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DRC-2008-002301 - 0901a0688081b672
White Mesa Uranium Mill Groundwater Monitoring Report State of Utah Groundwater Discharge Permit No. UGW370004 4th Quarter (October through December) 2007 Prepared by: Denison Mines (USA) Corp. Suite 950, 1o5o lTth Street Denver CO 80265 Februaryr 2008 I I t t T t I I I I I I I T T T I I I 1. INTRODUCTION This is the Routine Groundwater Monitoring Report, as required under Part I.F.l of State of Utah Groundwater Discharge Permit No. 370004 (the "Permit"), and the Routine DMT Performance Standard Monitoring Report, as required under PartI.F.2 of the permit, for the 4th quarter of 2007 (the "Quart"i'; fo, Denison Mines (usA) corp,s. (..DUSA,s,,) White Mesa Uranium Mill (the "Mill"). As required under Parts I.E.1, LE.2 and,I.E.4 of the Permit, this Report includes all recorded field measurements and laboratory analyses for well monitoring conducted during the Quarter. In addition, and as required under part I.E.6 of the Permit, this report also presents the results of DMT Performance Standard monitoring for the Quarter. 2. GROUNDWATER MONITORING 2.1. Samples and Measurements Taken During the euarter A map showing the location of all groundwater monitoring wells, piezometers, existing wells and temporary chloroform contaminant investigation wells is attached under Tab A.During the Quarter, the following groundwater samples and measurements were taken during this reporting period (July through September). a) Groundwater Compliance Monitoring (i) QuarterlyGroundwaterComplianceMonitoring Quarterly Groundwater Compliance Monitoring is performed in the wells listed below, pursuant to Part I.E.1 . a) of the Permit. MW-l1 MW-14 MW-26 (formerly TW4- 1 5) MW-32 (formerly TW4-1 7) (ii) Semi-annual Groundwater Compliance Monitoring Semi-annual Compliance Monitoring is performed in the wells listed below, pursuant to Part I.E.I. a) of the Permit. MW-1 MW-2 MW-3 MW-5 MW-12 MW-l5 MW-17 MW-l8 MW-I9 I I t t T T I I I I T I I I I I I I t (iii) Accelerated Groundwater Monitoring. In addition to the routine quarterly monitoring referred to above, DUSA collected accelerated monthly samplings for select constituents at wells: MW-14, MW-26 and MW-32. Also, accelerated quarterly samples are collected at certain locations and for select constituents at wells: MW-l, MW-3, MW-5, MW-12, MW-I5, MW-17, MW-l8 and MW-l9. (iv) Quarterly Sampling for All New Wells Quarterly groundwater quality samples were collected from new monitoring wells in accordance with Part I.H. 4.of the Permit on October 23-31,2007. As such, the following monitoring wells were sampled on those dates: MW-3A MW-23 MW-24 MW-25 }|dW-27 MW-28 WM-29 MW-30 MW-31 The sample collection dates for monthly samples occurred on November 28,2007 and December 18-19, 2007. Routine quarterly, semi-annual and accelerated quarterly sample collection occurred on October 23-31,2007. (v) Parameters Analyzed All routine groundwater monitoring samples were analyzed for the parameters listed in Table 2 and Part I.E.l.c) 2)ii of the Permit. The accelerated monitoring samples were analyzed for the more limited specific parameters described in Section 2.4 of this report. b) Groundwater Head Monitoring Depth to groundwater was measured in the following wells andlor piezometers, pursuant to Part I.E.2 of the Permit: (i) (ii) (iii) The quarterly groundwater compliance monitoring wells listed in paragraph 2.1.a) above were measured on October 31, 2007 . Piezometers - P-l, P-2,P-3, P-4 and P-5, on November 2,2007; Existing monitoring well MW-4 and all of the temporary chloroform investigation wells, on October 10,2007; I I I I I I I t I I I I T I t T I t I (iv) In addition to the above, depth to water measurements are routinely observed in conjunction with sampling events for all wells sampled during monthly, quarterly and semi-annual monitoring efforts, regardless of the sampling purpose. 2.2 Field Data Sheets Attached under Tab B are copies of all field data sheets where field data were recorded in association with the quarterly and semi-annual sampling effort on October 23 through October 31, 2007 for the groundwater compliance monitoring wells listed in paragraphz.l(a) above. Attached under Tab C are copies of all field data sheets where field data were recorded in association with monthly accelerated monitoring and sampling efforts during the month of November for monitoring wells; MW-14, MW-26 and MW-32. Attached under Tab D are copies of all field data sheets where field data were recorded in association with monthly accelerated monitoring and sampling efforts during the month of Decernber for monitoring wells; MW-14, MW-26 and MW-32. 2.3 Laboratory Results -- Rout'ne Groundwater Monitoring 2.3.1 Copy of Laboratory Results All analytical results are provided by Energy Laboratories, the Mill's contract analytical laboratory (the "Analytical Laboratory). There are four sets of laboratory analytical results included in this Report. . Samples collected for the November accelerated sampling were reported on January 2, 2008 (Tab E) Also included under this Tab are the results of a duplicate sample of MW-26 (MW-65, lll28l07). Because the wells in the GWDP sampling program had been equipped with dedicated pumps by the November sampling an equipment rinsate sample was no longer necessary as of November, 2007. An analyses of a field blank was not included with this sample set. o Samples collected for the December accelerated sampling were reported on January 7, 2008 (Tab F). Also included under this tab are the results of analyses for a duplicate sample of MW-26 (MW-65, l2ll8l07). Because the wells in the GWDP sampling program had been equipped with dedicated pumps an equipment as of the Novernber, 2008 sampling, rinsate sample was no longer necessary in December. An analyses of a field blank was not included with this sample set. . Samples collected in October (l0l23lo7 through lOl3llOT) for the 4rth Quarter and Accelerated Quarterly samples under the Permit were reported in two data sets on January 9, 2008 and received by Denison on January 14,2008 (Tab G). Also I I I I I I I I I I I t I t I I I T I included under this tab are the results of analyses for duplicate samples of MW-26and MW-4 (Mw-65 and MW-70, respectively), a rinsate sample (Mw-63, 10130107) and a field blank (MW-60, t)l30l07). Note: Copies of laboratory QA/QC Summaries are included with the reported, data in corresponding Tabs E, F and G. 2.3.2 Analysis of Laboratory Results Under the Permit it is intended that background groundwater quality will be determinedon a well-by-well basis, as defined by the mean plus second standard deviation concentration. The Mill is currently in the process of working with the Utah Division ofRadiation Control and its consultant URS to establish background (including the meanplus second standard deviation) for all of the constituents b"ing'sampletunder thePermit. Toward this end, a report entitled Background Groundwater Quality Report:Existing Wells For Denison Mines (USA) Corp.'s White Mesa Uraniui mill Site, SanJuan County Utah, lntera lnc, 2006) was transmitted to UDEe on Decemb er 29, 2006. In response to UDEQ's review, a revised report was provided to UDEe on Octob jr 2007, Revised Background Groundwater Quality Report: Existing Wells For Denison Mines(USA) Corp.'s White Mesa (Jranium mill Site, San Juan County (Jtah, lntera Inc, 2007.In addition to the background report for existing wells, DIUSA Las transmitted to UDEetwo addenda to the background report, Evaluation of Available Pre-Operational andRegional Background Data (Intera, 4ll9/07) and Background Grouidwater quality Report, New Wells, For the Denison Mines (USA) Corp. White Mesa (Jranium Afu Siti, San Juan County, Utah (Iutera, 6/1107). Until such time as background is established,the Permit requires that constituent concentrations in each moniioring well shall notexceed the Groundwater Compliance Limits ("GWCLs") set out in Tablel of the permit. DUSA's review of the anallical results for the Quarter indicates that concentrations ofthe following constituents in the following monitoring wells exceeded their respective GWCLs in Table 2 of the Permit: Table 1- GwcL Exceedances for the euarterly and semi-Annual Sampting ' Monitorint W:eIl (Water Clasa) ConsfituCilt',:,GwcL.(ua/L), Sa.mp.le Resirlt (u.gll,) MW-3 (Class III) Manganese 400 1,950 Thallium 1.0 l. l5 Uranium 15 39.4MW-14 (Class ITI) Uranium l5 68.6 Manganese 400 2,120 MW-15 (Class III) Selenium 25 94 Uranium t5 5lMW-17 (Class III) I I I I I I I t I I I I t T I I I I T A separate Notice of these exceedances has been submitted to the Executive Secretary on February 13, 2008, pursuant to Part I.G.l.a) of the Permit. Unless the compliance status for any constituents in any wells is determined otherwise by the Executive Secretary, the Mill will, pursuant to Part I.G.1.b)1) of the Permit, coflrmence or continue, as the case may be, accelerated sampling of each of the foregoing constituents in its respective well on a monthly or quarterly basis, as applicable, as set forth below: Table 2 - Accelerated Monitoring Requirements as of January 13,2007 Mgnitofi4gWelI (Water ClnsS) Constitrient G-WC:Ir (us/L) Sainple'Result (ug1LJ Uranium l5 3l MW-18 (Class II) Uranium 7.5 39.2 MW-19 (Class II) Thallium 0.50 0.51 Manganese 200 219 MW-26 (Class III) Manganese 400 1.190 Uranium I5 47 Chloroform 35 820 Dichlormethane 2.5 9.0 MW-32 (Class III) Manqanese 400 5,170 Nickel 50 67 Iron 5.500 6,420 ' ,ConStituent,:. MW-1 (Class II) Tetrahydrofi,ran Semi-Annual Quarterly 4u Ouarter 2005 Manganese Semi-Annual Ouarterlv 1'r Ouarter 2006 MW-3 (Class III) Mansanese Semi-Annual Ouarterly 1"'Ouarter 2006 Selinium Semi-Annual Quarterly 3'o Ouarter 2006 Thallium Semi-Annual Ouarterly 4- Ouarter 2005 Uranium Semi-Annual Quarterly 4* Ouarter 2005 Tetrahvdrofuran Semi-Annual Ouarterly 3'" Ouarter 2006 MW-5 (Class II) Manganese Semi-Annual Ouarterly 4- Ouarter 2005 Fluoride Semi-Annual Quarterly 4- Ouarter 2005 Tetrahvdrofuran Semi-Annual Ouarterly l" Ouarter 2006 MW-12 (Class III) Manganese Semi-Annual Quarterly 4- Ouarter 2005 Uranium Semi-Annual Quarterly 4* Ouarter 2005 MonitoringWell fl{ater Class)Constituent , Normal ['requency of Samnline Accelerated Frequenc,y of Samnlins Commencement of Accelerated Monltonino Tetrahydrofuran Semi-Annual Ouartedy 4- Ouarter 2005 MW-14 (Class III) Mansanese Ouarterlv Monthlv June 2005 Uranium Quarterly Monthlv June 2005 MW-15 (Class III) Selenium Semi-Annual Quarterly 4- Ouarter 2005 Uranium Semi-Annual Quarterly 4* Ouarter 2005 MW-17 (Class III) Uranium Semi-Annual Quarterly 4- Quarter 2005 Thalium Semi-Annual Ouartedy l" Ouarter 2006 MW-18 (Class II) Thallium Semi-Annual Ouartedv 4* Ouarter 2005 Uranium Semi-Annual Quarterly 4- Ouarter 2005 MW-l9 (Class II) Fluoride Semi-Annual Quarterly l'' Ouarter 2006 Selenium Semi-Annual Quarterly {* Quarter 2005 Thallium Semi-Annual Quarterly 1"'Ouarter 2006 Uranium Semi-Annual Quarterly 4- Quarter 2005 MW-26 (Class III) Manganese Quarterlv Monthlv June 2005 Uranium Ouarterly Monthlv June 2005 Chloroform Quarterly Monthly June 2005 Dichloromethane'Ouarterlv Monthlv September 2005 Dichloromethane'Quarterlv Monthlv Seotember 2005 Tetrahydrofuran Ouarterly Monthlv March 2006 MW-32 (Class III) Cadmium Ouarterlv Monthlv June 2005 Iron Quarterly Monthly June 2005 Manganese Ouarterly Monthly June 2005 Nickel Quarterly Monthly June 2005 Gross Aloha Ouarterlv Monthly March 2007 The background constituent concentrations for all of the new monitoring wells (MW-3A, MW-23, MW-24, MW-25, MW-27, MW-28, MW-29, MW-30 and MW-31) through eight quarters of sampling pursuant to Part I.H.4 of the Permit has been evaluated and reported to UDEQ under the title Background Groundwater quality Report, New Wells, For the Denison Mines (USA) Corp. White Mesa (Jranium Mill Site, San Juan County, Utah (lntera, 611107). This report is currently under review at UDEQ and, as such, the GWCLs for these wells have not been determined and included in the Permit. Accordingly, it is premature to determine whether or not any of the sampling results for this Quarter exceed any Permit limits for any constituents in those wells. 7 I I 2.4Laboratory Results - Accelerated Monitoring I The analytical results for the accelerated monitoring of the various constituents in certainr monitoring wells for the months of November and December, 2007 are provided at Tabs I E and F respectively and for the 4tl' Quarter of 2007 are included in the analytical results I for that Quarter under Tabs G. t The following table summarizes the initial sample result that triggered accelerated I monitoring for each of the various constituents and the accelerated monitoring results to date. I Table 3 - Summary of Accelerated Monitoring Results to Date Monfto{4g,Well :::(WateirClass)''Constitue_nt GWCL,r* i,S.a.m le [.v6nt MW-l (Class II) Tetrahvdrofuran I 1.5 2* Otr 2005 85 4* Otr 2005 58 l* Otr 2006 48 2"" Otr2006 60 3'" Oh 2006 26 4- Otr 2006 t6 l* Otr 2007 t4 2"" Otr 2007 NA 3'" Otr 2007 l5 4* Otr2007 t6 Manganese 200 4* Otr 2005 215 l"'otr 2006 220 2* Otr 2006 230 3'otr 2006 216 4- Otr 2006 198 l"'otr 2007 229 2* Orr 2007 NA 3'," Otr2007 30 4* Ofr2007 15 MW-3 (Class III) Thallium 1.00 3'' Otr 2005 1.60 {* Qfr 2005 t.t4 1" otr 2006 r.13 2"" Ofi2006 0.99 3" Otr 2006 1.ll 4^ Otr 2006 1.16 l* Otr 2007 0.99 2"" Otr2007 NA 3* Otr 2007 l. l9 4* Q1tr2007 l.l5 Uranium t5 3'" Otr 2005 35.90 4'Otr 2005 30.90 l"'Qtr 2006 39.1 2* Qtr 2006 27.6 3" Otr 2006 32.0 4* Qtr 2006 28.2 I I I I I I I I I T I I I I I I I I I T I I t I T T I T t t I I MonitoringW.gtl (Water.Class) , Constituent GWCL (usltr-)SampleEv0nt Sample Result tue/L) MW-3 Contd.Uranium 15 1"'Otr 2007 30.2 2* Otr 2007 NA 3'" otr 200'7 17.4 4- Otr2007 39.4 Manganese 400 4- Otr 2005 732 1" Otr 2006 1,640 2"" Otr 2006 631 3'" Otr 2006 t,370 4- Otr 2006 682 l"'otr 2007 848 2"" Otr 2007 NA 3'" OjJ2007 t99 4* Otr2007 1.950 Selenium 25 2 01112006 25.4 3'Otr 2006 16.84 Orr 2006 27.9 1" otr 2oo7 20.1 2* Ofi2007 NA 3'" oft2007 33.6 4* Ofi2007 8.9 Tetrahydrofuran 23 2"" ofi 2006 26 3'," Otr 2006 46 4* Off2006 ll l" otr 2oo7 ll 2"" ofi 20a7 NA 3'," Ofi2007 ND 4* O1d2007 ND MW-s (Class II) Manganese 200 2^ Otr 2005 250 4- Otr 2005 280 l" Otr 2006 259 2"" Otx2006 228 3'o otr 2006 237 4* Otr 2006 228 l" otr 2oo7 281 2"" 01(2007 NA 4^ Otr 2007 t42 Fluoride 1.00 (ms/L)3'," Otr 2007 134 2^ Otr 2005 1.3 (me/L) 4* Otr 2005 1.0 (ms/L) l"'otr 2006 0.9 (mp/L) 2* OIr2006 1.0 (msll-) 3'o otr 2006 0.9 (ms/L) 4- Otr 2006 I 1(ms/L) l* otr 2007 l.l (ms/L ) 2"" Ofi2007 NA 3'" ofi2007 1.2 (msll\ 4* Otr2007 1.0 Tetrahvdrofuran 11.50 4* Otr 2005 l3 l" otr 2006 l0 2"" Otr2006 7.8 3'" Otr 2006 ND I I I I I t I I I I I I I T t I I T I Monitorlng,Well (Water Class)Constituent GWCL fuplf")Sample:Event Sample ReSuIt (uslt) MW-5 Contd.Tetrahydrofuran I t.s0 4* Oh 2006 ND l" oh 2oo7 ND 2* Otr 2007 NA 3," etr 2007 ND 4"'^Otr2007 10 MW-12 (Class III) Manganese 400 2" Otr 2005 420 4* otr 2oo5 27 l* Otr 2006 t7 3" Otr 2006 290 4^ Otr 2006 92 1* Otr 2007 279 2"" otr 2oo7 NA 3* Otr 2007 57 4^ Qfr2007 60 Uranium l5 2"" Otr 2005 15.30 4- Otr 2005 16.50 l"'otr 2006 ND 2* Ot 2006 20.9 3'" Otr 2006 23.5 4^ Otx 2006 19.8 l"'Otr 2007 19.4 2* Qtr 2007 NA 3'," Otr2007 8.68 4- Qff2007 19.2 Tetrahvdrofuran 23 2"" Ofi2005 24 4* Otr 2oo5 t2 l" otr 2006 ND 2"" Qfi2006 16 3'" Otr 2006 l8 4- Qfi2006 ND l"'otr 2007 38 2* Q1tr2007 NA 3'" Otr 2007 ND 4- Qtr 2007 NDMW-14 (Class III) Manganese 400 1" Otr 2005 1.860 June 2005 r.840 July 2005 2,000 Aue.2005 1,900 Sept.2005 2,tt0 Oct.2005 1.950 Nov.2005 1.880 Dec.2005 I,960 Jan.2006 2.060 Feb.2006 1.940 Mar.2006 2,070 Aoril2006 2.100 Mav 2006 2,000 June 2006 1,650 Julv. 2006 l,590 Aue..2006 I,870 10 t I I t I I T I I I I I I I I I t I I 11 Monitoring,,Well (Water,ClaCs)Coiistituent GWCL (us/Li Samglg.nvent , Sample Result , (us/L), MW-14 Contd.Manganese 400 Seot.2006 1,860 Oct.2006 1.960 Nov.2006 1,790 Dec.2006 1,960 Jan.2007 1.970 Feb.2007 1,940 Mar.2007 1.930 Aoril2007 2020 Mav 2007 t940 June2007 NA Julv 2007 NA Aueust 2007 2,010 Sentember 2007 2,060 October 2007 2.120 November 2007 2.380 December 2007 2.290 Uranium l5 1"'otr 2oo5 65. I June 2005 58.9 July 2005 65.s Aus. 2005 66.5 Sept.2005 67.5 Oct.2005 70.1 Nov.2005 69.7 Dec.2005 67.6 Jan.2006 74.8 Feb.2006 69.2 Mar.2006 69.4 April2006 64.0 Mav2006 70.3 June 2006 69.2 Julv. 2006 71.8 Aus.2006 64.7 Sept.2006 69.0 Oct.2006 66.4 Nov.2006 65.5 Dec.2006 68.4 Jan.2007 24.9 Feb.2007 43.8 Mar.2007 42.8 April2007 18.8 Mav2007 62.4 June 2007 NA Julv 2007 NA Auzust 2007 ND September 2007 70.5 October 2007 68.6 November 2007 6t.6 December 2007 60.7 MW-15 (Class III)Selenium 25 2* Qtr 2005 79 4." Otr 2005 92.s t't Qtr 2006 102 2^ Qtr 2006 tt7 I I I I t I T I I I I t T t I T I I t Monitoring W*ll (Water Class)Constituent GWCL (us/L)Sample Evqnt Sample Result(untLl MW-15 Contd.3'" Otr 2006 tt2 4* otr 2006 tt2 l" otr 2007 89.6 2* Otr 2007 NA 3'" Oft2007 94 4"',Otr 2007 94 Uranium t5 2* Otr 2005 45.3 4* otr 2005 47.7 l" otr 2006 50.42 Qtr 2006 47.8 3'" otr 2006 50.1 4"'Otr 2006 51.6 l* Otr 2007 46.5 2"" Otr 2007 NA 3* Ofr2007 28.6 4^ otr 2oo7 5l.0 MW-17 (Class III) Uranium 15 2"" otr 2oo5 23.4 4* Otr 2005 3t.2 1"'otr 2006 28.2 2"" Ofr2006 32.2 3'" otr 2006 30.6 4^ Ofi2006 30.2 l" Otr 2007 23.4 2"" Otr 2007 t8.2 3'" otr2oo7 20.1 4* Otr 2007 31.0 MW-18 (Class II) Thallium 0.5 2"" Otr 2005 1.0 4* otr 2oo5 0.95 l- Otr 2006 t.46 2"" otr 2006 1.3 3'," Otr 2006 0.83 4* Otr 2006 1.01 1" otr 2oo7 1.85 2* Qtr 2007 NA 3- Otr 2007 0.96 4- Qtr2007 0.89 Uranium 7.5 2"" Otr 2005 39 4* Otr 2005 39 l* Otr 2006 42.6 2"" Otr 2006 32.2 3'' Otr 2006 39.6 4* otr 2006 42.2 1" otr 2007 46.9 2"" otr 2oo7 NA 3'," OIr2007 36.5 4- Otr2007 39.2 MW-19 (Class II) Fluoride 1.0 (msll-)4- Otr 2005 1.1(mell.) 2"" otr 2006 1.1 (ms/L) 3- Otr 2006 1.1 (ms/L) l2 I I I I T I T I I t I t I I t I I I I Monitofing Well (Water C-lass)Constituent GWCL (us/L)Sample Event Sample Result hts.tL\ MW-19 Contd.Fluoride 1.0 (ms/L)4'" Otr 2006 1.3 (mplL\ l" otr 2007 1.4 (mslL\ 2* Otr 2007 NA 3'" otr 2007 1.3(mell.) 4"'Olr2007 l.l(ms/L) Selenium 12.5 2"" Otr 2005 l8 4* Otr 2005 2.3 l" otr 2006 4.3 2* Or 2006 2.0 3'o otr 2006 2.0 4* Otr 2006 1.2 l* Otr 2007 1.1 2"" Otr 2007 NA 3* Otr2007 l 1.9 4* Qtr2007 10.8 Thallium 0.5 4"',Otr 2005 0.57 1- Otr 2006 ND 2"" Otr 2006 0.7 3'o Otr 2006 0.55 4'," Otr 2006 0.68 l" Otr 2007 ND 2"" Otr2007 NA 3'" Otr 2007 0.53 4^ Otr2007 0.52 Uranium 7.5 2^ Otr 2005 1.6 4- Otr 2005 1.3 l" Otr 2006 2.8 2"" Otr2006 1.5 3'o otr 2006 8.s2 4* Otr 2006 t0. r 1" otr 2oo7 9.37 2"" Otr2007 NA 3'" olx2007 7.76 4* Otr2007 7.53 MW-26 (Class II) Manganese 400 1" otr 2005 1.3s0 June 2005 956 Julv 2005 1.100 Aue.2005 1.430 Sept.2005 1,160 Oct.2005 1.410 Nov.2005 949 Dec.2005 1.030 Jan.2006 95r Feb.2006 874 Mar.2006 1,210 April2006 l.100 Mav 2006 1,280 June 2006 1,300 Julv. 2006 95 Aue.2006 902 Sept. 2006 1,330 l3 I I I I I I I I I I I I I t I t I T I MonitorlngWell (Water Class)Constituept GW{t (usll,)SampleEvent SamlleResult : ,(uell,) MW-26 Contd.Mansanese 400 Oct..2006 1,610 Nov.2006 1.500 Dec.2006 1,080 Jan.2007 769 Feb.2007 979 Mar.2007 1.130 April.2007 1,410 Mav-2007 910 Jwe,2007 t.230 Julv 2007 1,280 4us.2007 728 Sept.2007 NS Oct.2007 r.190 Nov.2007 1.150 Dec.2007 1,410 Uranium l5 l"'otr 2005 22.4 June 2005 9.5 Julv 2005 12.6 Aue.2005 26.0 Seot.2005 17.4 Oct.2005 22.7 Nov.2005 t2.t Dec.2005 12.3 Jan. 2006 10.7 Feb.2006 9.9 Mar.2006 17.9 April2006 l4 Mav 2006 2.5 June 2006 24.6 Julv 2006 17.6 Aus.2006 r0.5 Sept. 2006 23.O Oct.2006 34.7 Nov.2006 32.6 Dec.2006 20.9 Ian.2007 22.6 Feb.2007 44.2 Mar.2007 42.8 April.2007 36.4 May,2007 ll9 June- 2007 24.5 Julv 2007 38.6 Aueust 2007 21.2 Seotember 2007 NS October 2007 47.0 November 2007 42.O December 2007 47.6 Chloroform 35 1* otr 2005 230 June 2005 430 Julv 2005 260 Aus.2005 780 Sept. 2005 810 t4 I I I I I t I I t I t T t I T I I I I t5 MonitoringWell fiVater,Class)Co-nstituent GWCL (us/L)Sample Event Sample Reiult , ,,,(ug&) MW-26 Contd.Chloroform 35 Oct.2005 960 Nov.2005 1,100 Dec. 2005 1,200 lat 2006 1.300 Feb.2006 860 Mar.2006 1,200 April2006 1.200 Mav 2006 1.100 June 2006 260 Julv.2006 7.800 Aus.2006 980 Sept.2006 1,200 Oct.2006 l,400 Nov.2006 950 Dec.2006 I.100 Ian.2007 5.700 Feb.2007 4.400 Mar.2007 1.600 April.2007 2,100 luf.ay,2007 2,400 June, 2007 660 Jnlv 2007 1.100 Aueust 2007 920 September 2007 NS October 2007 820 November 2007 1.400 December 2007 I.400 Dichloromethane 2.5 June 2005 5.4 Aue.2005 11.0 Seot.2005 5.9 Oct.2005 9.8 Nov.2005 7.6 Dec.2005 t2 Ian.2006 6.9 Feb.2006 4.8 Mar.2006 4.6 April.2006 t4 Mav.2006 l1 June.2006 2.5 Julv,2006 ND Aue. 2006 t2 Sept. 2006 25 Dichloromethane 2.5 Oct.,2006 3l Nov.2006 l5 Dec..2006 2.6 Jan.2007 ND Feb.2007 25 Mar.2007 26 April,2007 33 Mav.2007 28 June. 2007 37 Julv 2007 t4 I I I t t I I I I I I I t I T t T I I MonitoringWell (Water Class)Constituent GWCL :(us/f)Sample Event Sample Result (usil,) MW-26 Contd Dichloromethane 2.5 Auzust 2007 9.0 Seotember 2007 NS October 2007 1.2 November 2007 l8 December 2007 22 Tetrahvdrofuran 23 4- Otr 2005 55 Jan.2006 ND Feb. 2006 ND Mar.2006 ND April2006 ND Mav 2006 ND June 2006 ND Julv 2006 ND Aue.2006 ND Sept. 2006 ND Oct.2006 ND Nov.2006 ND Dec.2006 ND Iar.2007 ND Feb.2007 ND Mar.2007 ND Aoril.2007 ND Mav.2007 ND June. 2007 ND Julv 2007 ND Ausust 2007 ND September 2007 NS October 2007 ND November 2007 ND December 2007 ND MW-32 (Class III)Cadmium 2.5 1" Otr 2005 23.8 June 2005 t.7 Julv 2005 2.1 Aus.2005 2.75 Sept.2005 2.95 Oct.2005 2.16 Nov.2005 2.07 Dec.2005 1.0 Jan.2006 I.l4 Feb.2006 2.32 Mar.2006 2.58 April2006 2.96 Mav 2006 1.84 June 2006 0.8 Julv.2006 3.0 Aue.2006 1.44 Sept. 2006 0.96 Oct.2006 ND Nov.2006 0.9 Dec.2006 1.44 Jan.2007 3.0 Feb.2007 ND t6 I t I T T I I t I T I I I I T I I T I Moni{olingWetI (Water Class)Constituent GWCL (uslL)Sample Event Sample Result (ueltr,) MW-32 Contd.Cadmium 2.5 Mar.2007 2.42 Apm,2007 2.24 May,2007 6.18 June.2007 ND Julv-2007 2.83 Aurust.2007 1.82 September 2007 1.18 October 2007 1.20 November 2007 1.47 December 2007 1.8 I Manganese 400 l"'otr 2oo5 3,740 June 2005 4.220 Julv 2005 4,720 Aus.2005 4.670 Sept.2005 4.580 Oct.2005 4.590 Nov.2005 4,530 Dec.2005 4.340 Jan.2006 5,090 Feb.2006 4.160 Mar.2006 5.090 April2006 s.070 Mav 2006 4.840 June 2006 4.680 Julv. 2006 4.540 Aus.2006 5.160 Sept. 2006 4,690 Oct.2006 4.790 Nov.2006 4,830 Dec.2006 4.920 Jan.2007 5.040 Feb.2007 4,940 Mar.2007 4,920 Aoril.2007 5.450 Mau2007 4,920 h:lrie.2007 5.470 Julv 2007 5490 Ausust 2007 4,820 September 2007 4,790 October 2007 5.170 November 2007 5,583 December 2007 5.050 Nickel 50 1"'otr 2oo5 71.0 June 2005 54.0 Julv 2005 63.0 Aus.2005 64.0 Sept. 2005 67.0 Oct.2005 63.0 Nov.2005 62.0 Dec. 2005 51.0 Jan. 2006 69.0 Feb.2006 54.0 t7 I I I T I t I T I I T T T I I T T I I Based on the accelerated monitoring results to date, DUSA submits that accelerated monitoring should cease at this time for the following constituents in the following wells: Table 4 Constituents for Which Accelerated Monitoring Should be Disconfnued Well Location MW-5 MW-12 MW-26 Constituent Tetrahydorfuran Manganese Tetrahydrofuran DUSA will, however, continue accelerated monitoring of the foregoing constituents until advised otherwise by the Executive Secretary. 2.5 Depth To Groundwater Readings And Water Table Contour Map A listing of groundwater level readings for the Quarter (shown as depth to groundwater in feet) is included under Tab H. Also included under Tab H is a water table contour map, which provides the location and identity of all of the wells and piezometers listed in items 2.1O) above for which depth to groundwater was recorded during the Quarter, the groundwater elevation at each well and piezometer, measured in feet above mean sea level, and isocontour lines to delineate groundwater flow directions observed during the Quarter's sampling event. l8 MonitoiingWell (Water Class),Cortstituent GWCL(us/I)Sample Event Sample Result (us/L) MW-32 Contd.Nickel 50 Mar.2006 68.0 Aoril.2006 70.0 Mav.2006 64.0 June- 2006 52 Julv 2006 74 Aus.2006 59 Sept..2006 53 Oct..2006 t2 Nov.,2006 56 Dec.2006 62 Jan.2007 59 Feb.2007 51 Mar.2007 74 Aorll"2007 64 Mav.2007 127 June, 2007 94 Julv 2007 85 Aueust 2007 65 September 2007 62 October 2007 67 November 2007 5',? December 2007 66 I I I t I I I I I I t T I I I I I T I 2.6 Quality Assurance Evaluation And Data Validation Quality assurance evaluation and data validation procedures in effect at the time of sampling were followed. These involve three basic types of evaluations: field QC checks; Analytical Laboratory QA checks; and checks performed by DUSA personnel, as described below. 2.6.1 Field OC Checks The following QC samples were generated by Mill personnel and submitted to the Analytical Laboratory in order to assess the quality of data resulting from the field sampling program: a) October Sampling: -One field blank (MW-60, 10130107); -Two duplicate samples of MW-26 (MW-65 and MW-70,1012108 & 10/30/08, respectively) -One equipment rinsate sample (MW-63, 10130107 and, -One trip blank provided by the Analytical Laboratory and sent with the samples received by the Analytical Laboratory on 10126107. b) November Sampling: -One duplicate sample of MW-26 (MW-65, lll28l07,) and; -One trip blank provided by the Anallical Laboratory and sent with the samples received by the Analytical Laboratory on lll30/07. c) December Sampling: -One duplicate sample (MW-65, duplicate of MW-26 ); and; -One trip blank provided by the Analytical Laboratory and sent with the samples received by the Analytical Laboratory on 12120/07. Note: For monthly accelerated sampling in Novernber and December an equipment rinsate sample was not collected as these wells were equipped with dedicated pumps subsequent to the October quarterly sampling event. Due to a miscommunication a field blank was not included with the monthly sample batches, albeit field blanks are not required by either the GWDP or the QAP and are collected voluntarily by DUSA. The Environmental staff at the mill has been apprised of this oversight and will include a field blank with all monthly and quarterly samplings for future monitoring periods. These QC samples were sent blind to the Analytical Laboratory and analyzed for the same parameters as permit-required samples. l9 I t T I I I I I I t I I t I I t T I T 2.6.2 Analytical Laboratory QA/OC Procedures The Analytical Laboratory has provided summary reports of the analytical quality control/quality assurance (QA/QC) measurements necessary to maintain conformance with NELAC certification and reporting protocol. The Analytical Laboratory eA/eCSummary Reports, including copies of the Mill's Chain of Custody and Analytical Request Record forms for each set of Analytical Results, follow the analytical results under Tabs E to G. 2.6.3 Mill QA Manager Review The Mill QA Manager, which for the purposes of this Report was DUSA's Manager of Environmental Affairs, performed three types of reviews: a determination of whetherMill sampling personnel followed Mill sampling procedures; a review of the results from the Field QC Checks; and a review of the Analytical Laboratory QA/QC analysis. The results of the QA Manager's review are discussed below. a) Adherence to Mill Sampling SOPs On a review of adherence by Mill personnel to the existing sampling standard operating procedures (SOPs), the QA Manager observed that QA/QC requirements established in the Groundwater Monitoring Quality Assurance Plan wire being adhered to, (except that the field blanks were not included with the monthly samplings as mentioned above) and that the Sop's were implemented. b) Results fromfield QC checks (i) October Sampling The results of duplicate QC checks for the October sampling indicated three exceptions to the Relative Percent Difference goal of 2Ooh. The MW-26 sample and its duplicate MW-65 indicated acceptable duplication of analytical results except for nitrogen-ammonia, iron, selenium, uranium and gross alpha. Ho*",n"r, the results of the MW-4 and its duplicate MW-70 were all well within the acceptance criteria. The results of the Field Blank, Rinsate Sample and the evaluation of duplicate analyses are presented in the Table below. Table s-QC Evaluation October gth qtr.; Sampling Event Constituent MW-60 DI Blank MW-63 Rinsate Duplicate Evaluation I Duplicate Evaluation 2 MW-4 Dup MW-70 RPD % MW-26 Dup MW-65 RPD %Carbonate ND ND ND ND 0 ND ND 0Bicarbonate2ms/L ND 356mslL 358 ms/L -0.s6 4ll ms/l ,409mslL 0.48CalciumNDND273mp/L 276melL - 1.09 508 me/L 522 ms/\ .1.82ChlorideNDND46ms./L 45 ms/L 2.t9 55 mslL 55 mslL 0FluorideNDND0.3 me/L 0.3 me/L 0 0.2msll .0.2mslL 0MaenesiumNDND125 ms.lL 126mplL -0.80 179 mslL 177 me/L l.t2Nitrogen-Ammonia ND ND ND ND 0 0.27 ms/l .0.21 mplL 25.00 20 I I I I I T I I I I t I I I I t t T T * RPD Equation for Gross Alpha Satisfied if differential analysis of reported values and counting error is <2 In accordance with Section 10.1 of the Groundwater Monitoring Quality Assurance Plan (QAP) the nitrogen-ammonia, iron, selenium, uranium and gross alpha parameters are annotated here as falling outside of the QA specification for duplicate samplings. Denison has previously initiated a process to determine the root cause for duplication difficulties through extended discussions with the Laboratory and the Denison sampling technicians. While some duplicate analyses for MW-26 were outside of the 20% RPD specification, the results of duplicate analyses for MW-4 were all within specification. With regard to duplicate sampling of MW-26, this well is a pumping well and is subject to fluctuation in chemical parameters while sampling is underway. In accordance with Section 10.2 of the QAP Denison determined that duplicate analyses for MW-26 should be discontinued and that this pumping fluctuation is the root cause in failing RPD's on duplicate analyses for this well. Constituent MW-60 DI Blank MW-63 Rinsate Duplicate Evaluation I Duplicate Evaluation 2 MW-4 Dup MW-70 RPD % MW-26 Dup MW-65 RPD % Nitroeen-Nihate ND ND 6.0 ms/\.6.3 me/L 4.88 0.7 mslL 0.7 ms.L 0 Potassium ND ND 7.4melL 7.5 ms/L r.35 l0.2ms.lL 11.0 ms/L Sodium 0.9 melL 0.9 ms/L 89.6mplL 88.6 mell-t.t2 162m.lL 177 ms.L -s.99 Sulfate lmg/L ND 944ms.lL 919 2_68 1.930 me/L 1.850 me/L 4.23 pH 6.01 s.u.5.96 s.u.7.37 s.u.7.31 s.u.0.82 7.13 s.u.7.13 S.U.0 TDS ND ND 1"780 me/L 1.680 ms/L 5.78 3.180 me/L 3.200ms/L -0.63 Arsenic ND ND ND ND 0 ND ND 0 Bervlliurn ND ND ND ND 0 ND ND 0 Cadmium ND ND ND ND 0 ND ND 0 Chromium ND ND ND ND 0 ND ND 0 Cobalt ND ND ND ND 0 ND ND 0 Copper ND ND ND ND 0 ND ND 0 Iron ND ND ND ND 0 263 u,s.lL 332 us.lL -23.9 Lead ND ND ND ND 0 ND ND 0 Manganese ND ND ND ND 0 1.190 1.420 -17.62 Mercury ND ND ND ND 0 ND ND 0 Molybdenum ND ND ND ND 0 ND ND 0 Nickel ND ND ND ND 0 ND ND 0 Selenium ND ND 52.3 ue/L 53.9 :us/L -3.01 12.6 uelL 7.6rslL 124.75 Silver ND ND ND ND 0 ND ND 0 Thallium ND ND ND ND 0 ND ND 0 Tin ND ND ND ND 0 ND ND 0 Uranium ND ND 9.87 uslL 9.71 ts/L -0.016 47.0 uelL 52.2wL -58.24 Vanadium ND ND ND ND 0 ND ND 0 Zinc ND ND ND ND 0 ND ND 0 Gross Aloha ND ND ND ND NA 3.3 pCilL 1.9 oCtlL 1.65* Acetone ND ND ND ND 0 ND ND 0 Benzene ND ND ND ND 0 ND ND 0 Carbon tetrachloride ND ND 2.3 tts./L 2.4luslL -4.26 ND ND 0 Chloroform ND ND 2.700 us/l 2.700us./L 0 820 870 -5.92 Chloromethane ND ND ND ND 0 ND ND 0 MEK ND ND ND ND 0 ND ND 0 Methvlene Chloride ND ND ND ND 0 1.2 1.3 8.00 Naphthalene ND ND ND ND 0 ND ND 0 Tetrahydrofuran ND ND ND ND 0 ND ND 0 Toluene ND ND ND ND 0 ND ND 0 Xvlenes ND ND ND ND 0 ND ND 0 2t I I I I I I I t I I T T T t I t I I I (ii) November Sampling The results of duplicate QC checks for the November sampling indicated that manganese and methylene chloride exceeded the Relative Percent Difference goal of 20%. With regard to duplicate sampling of MW-26, this well is a pumping well andis subject to fluctuation in chemical parameters while sampling is underway. In accordance with Section 10.2 of the QAP Denison determined that duplicate analyses for MW-26 should be discontinued and that this pumping fluctuation is the root cause for failing RPD's on duplicate analyses for this well. As noted at2.6.l a) above, due to a miscommunication a field blankwas not included with the monthly sample batches. Rinsate samples were not required due to the use of dedicated pumping equipment. The Environmental staff at the mill have been apprised of this oversight and will include a field blank with all monthly and quarterly samplings for future monitoring periods. Table 6-QC Evaluation November Sampling Event Constituent Duplicate Evaluation MW-26 D.np MW-6s RPD o/o Manganese I.150 ue/L 840 us/L 31.16 Mercurv ND ND Uranium 42.0 u,s/L 39.0 us/L 7.41 Acetone ND ND 0 Benzene ND ND 0 Carbon tetrachloride ND ND 0 Chloroform l-490 lup/L 1.400 us/L 6.23 Chloromethane ND ND 0 MEK ND ND 0 Methylene Chhoride l8 us/L 14 us.lL 25.00 Napthalene ND ND 0 Tetrahydrofuran ND ND 0 Toluene ND ND 0 Xvlenes ND ND 0 (iii) DecemberSampling The results of duplicate QC checks for the December sampling indicated no exceptions to the Relative Percent Difference goal of 20%o. As noted at 2.6.1 a) above, due to a miscommunication a field blank was not included with the monthly sample batches. Rinsate samples were not required due to the use of dedicated pumping equipment The Environmental staff at the mill have been apprised of this oversight and will include a field blank with all monthly and quarterly samplings for future monitoring periods. 22 T I I ! T I I T I T I I I I t I I I I Table 7-QC Evaluation December Sampling Event Constituent Duolicate Evaluation MW.26 Dup MW;65 RPD % Manganese 1.410 us/L 1.450 -2.80 Mercury ND ND 0 Uranium 47.6w./L 51.6luc../L 8.06 Acetone ND ND 0 Benzene ND ND 0 Carbon tetrachloride ND ND 0 Chloroform 1.400 us/L 1-400 us/L 0 Chloromethane ND ND 0 MEK ND ND 0 Methylene Chhoride 22ts/L 24us/L -8.70 Naphthalene ND ND 0 Tetrahydrofuran ND ND 0 Toluene ND ND 0 Xvlenes ND ND 0 c) Review of Analytical Laboratory QA/QC Analysis The QA Manager reviewed the Analytical Laboratory's QA/QC Summary Reports and made the following conclusions; (i) Check samples were analyzed for all methods used in analyzirrg the groundwater samples. These methods were: Table 8 - Analytical Methods Ut:lized (ii) The check samples included at least the following: a method blank, a laboratory control spike, a matrix spike and a matrix spike duplicate, or the equivalent, where applicable. In this context, it should be noted that: o Laboratory fortified blanks are equivalent to laboratory control spikes, laboratory reagent blanks are equivalent to method blanks, post Carbonate as CO3. Bicarbonate as HCO3 Nitrate + Nitrite as N Z3 I I T I I I I T I I t I T I T I I I I digestion spikes are equivalent to matrix spikes and post digestion spike duplicates are equivalent to matrix spike duplicates; and o For method E900.1, used to determine gross alpha, a sample duplicate was used instead of a matrix spike duplicate; (iii) All qualifiers, and the corresponding explanations reported in the QA/QC Summary Reports for any of the check samples for any of the analytical methods were reviewed by the QA Manager. Some "D" qualifiers (reporting limit increased due to matrix interference) were observed for sulfate, chloroform and sodium. Sulfate limits have not been established under the permit and sodium is not a limited parameter. For chloroform, none of the detection limit modifications made in response matrix interference resulted in less than values above the required reporting level. (iv) A review of the Laboratory QA/QC summary reports indicated that the percent recovery and spiked duplicate results reported by the laboratory were acceptable with one exception (MW-14, 10129108 sample surrogate recovery at l32o/o for 1,2 Dibromfluoromethane compared to the RL guidance of 130%) attesting to the precision and accuracy of the measurement methods. The QA Manager noted that samples received and accepted by the Laboratory on November 30, 2008 were recorded at l4o C (but on ice), while all other samples for this reporting period were within the 4o C guidance. This subject was addressed in correspondence to UDEQ on February 2T, 2008. Further instances where samples are received by the laboratory in excess of the temperature requirement are not expected due to the acquisition of "5-day'' coolers for sample transport. (v) It was noted by the QA Manager that gross alpha results for MW-l, MW-2, MW-23, MW-26, NNV-27, MW-28, MW-32 and the MW-26 Duplicate (MW- 65) exceeded2} Yo vaiance for counting effor when compared to the reported analyical value. However, recent discussions with UDEQ, and corresponding drafted modifications to the GWDP, will modifii this requirement allowing that in these instances (<20% counting error) but when the precision effor is added to the reported value the resulting sum does not exceed the groundwater compliance limit the variance is acceptable. Accordingly, non-conformance is not indicated under the proposed modification to the GWDP. Once approved by UDEQ, these new conformance criteria for Gross Alpha will be incorporated into the QAP. 24 2.7 Electronic Data Files and Format DUSA has provided to the Executive Secretary an electronic copy of all laboratory results for groundwater quality monitoring conducted during the Quarter in Comma Separated Values (CSV). A copy of the transmittal e-mail is included under Tab I. 25 I I r r I I r I I I I l BOUNDARY I S/'f-(r.n\ =//I il // /t // l/ illw-01a MW.18a 1\ Nooto* T 0 3000 SCALE IN FEET EXPLANATION perched monitoring well temporary perched monitoring well perched piezometer perched monitoring well installed April, 2005 temporary perched monitoring well installed April,2005 new temporary perched monitoring well installed May,2O07 (locations approximate) 28 PIEZ-Ie MW.'19a \\ ,//// J'- MW-27+ It \\ t\\,/r'.---.-4 // tt/ /z . ,lJr-r, \r r\I \i \\t MW-20a // ,//MW-22a ,//,//,//,//// ,// I 1 lu*-roolrtr&rso PIEZ-1 MW-31+ TW4-20+ TWI-23* f wildlife oond \\ il lt // //\.\ rurLf$lifE CELL NO. 1 *8'oo#il, orw4-12/t//l// ll l1 l1 l1 ^lr-tl ql 1l gl 1l 1l 1l 1l gl 1l 1l 1l 1l 1l rlliiItl CELL NO. 4A SITE PLAN AND PERCHED WELL LOCATIONS WHITE MESA SITE HYDRO GEO CHEM,INC. IIIII III I I I I I t I I I I I T T I t t t T t Mill - Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) Description of SamPling Event: Date: 2.25 -O7 Revision: 2 Page4O of4l Location (wennane) tl4h) I mtil, in*iar il\a^, /*1,,,.e4 Date and Time for Purgi og lb ' .? I ' 0 7 *asampling (if different) Well Purging Equip Used: 4r*Oor -bailer Well Pump (if other noon"*retl-Delr iafu/ sampling Ev e,nt L'(lotlnl Nakf Prev. Well Sampled in sampling n*nt-.,S1L pHBuffer7.0 7.O pHBuffer4.0 4.0 Specific Conductance-ff *f-ulvfiIos/cm wettDeptrr . // (f2 DepttrtoWaterBefore P*{*e ( 7. 7Z CasingVolume(v)4' conduerince tunel lLtI .pIIof:Wdter welt water remp . <u"g)Lrz--Redpx Poten,*i dSIr*o rurr, 5 {, f Weather Con a. d# ,9 ..r-rt Ext'l Amb. Temp.(prior to sampling eve nq-{-- ve( t pn (,6f pn. (.7f , RedoxPoten ri*WJf3-- RedoxPotential (Hi 5q Z 2+.e r*iaq Lllo L {: , ATTACHMENT 1 WHITE MESA T'RANII'M MILL Gal. Purged-z r -corductance 17fi3 pn 6 JLt cona* lW pn f,. tz rr*p"rr* 13 ,eL . RedoxPotential (ED 5X0@ {qgRedox Potential Jsl t, ) Mill - Crroundwater Discharge Permit Crroundwater l\flonimring Quality Assurance Plan (QAP) DLte: ll.17.M Revision: I Page4l of{l Volume of WaterPurgcd When Field Parameters rnWur*a,V . V f*/Cg, Pumpin8 Rate Calculation ff#yrr=^*** Z. O I'9f,6":*fpfl**-* Number of casiqg volumes evacuated (if other than wa 2- U) If well evacuated to drymess, number of gallons evacuabd Name of Grtified Analytical Laboratory if Other Than Energy Labs IVneof Samnle Samnleffi rEuc'-r SainrileVolume (lndicatefioher Eiltered (circle) PreeeTTirtive Added (cir-ete) thfii assDedro VOCs N 3x4Oml Y HCX,2N Nutrients N l0Omt Y HrSOa N HtiawMetals N 250trlt (DN HNO.2NAll Other Non- Radiolocics UN 25Oml v'N NoPreservatirre Added GtossAloha VN 1.000 mt DN H+SOe V N Other (specify)tutry VN Samplevolume Yry Ifa preservative is use{ SpecifyTlpe and @antity of Prreservative: I t I T T t T t I I I I t I T t T t T Mill - Groundwater Discharge Permit Groundwater Monibring Qualiry Assurance Plan (QAP) Description of Sampling Date: 2.25.07 Revision: 2 Page4Oof 4l ATTACHMENT 1 WIIIIE MESA T]RANII]M MILL Loeation (wettnarre) lbtnt Z 'mJ:; RedoxPotential (Bh)-51%-- RedoxPotentialfrfrl .Sfrf Turbidity- Turbidity cordrrt^n ,3( /? c*a*t*u F / 3 L on 6.tlz pH,,, ,4,- ry , tr*pr^a* 13- 2 3 Ij Date andTime forPwgsng lb'23 'a? ,rdsampling(if different) Well Purging Equip Used: Au*nor -bailer Well Pump (rt *t,er frdnlr*rrrt))-du"#/ , l'l samplingEven, bfu 'll NorJot hv. well sampled in sampling Eventzht!-z? pHBuffer7.0 v.o pHBuffer4.o 4. 0 Specificconductance-fl*L uvlHos/cm wellDeptrr , IZf - Depth to Water Before P*srnLJl.O,SL- Casing Volume (V) 4" well: l0 - tltr (.653h) condue&rrcE <^"el <Lil pllof,grriter c*rr:;{:l','i":"ol WellwaterTemp .(*gJ|.-W- nAoip*o,rurOppflS-rtidity- weather con d. ClAn * (4 Ext.t Amb. Temp.(prior to sampling evenq L:--. e;la&Lctrace 3 S ff s L-'l/ t"rp"r"* | 2 ff Cnnrluctarice S(,32 ptt t"mproarn 12.89 - Redox Potential fehl--S t:L-l Redoxrot"otiaGn) d/i i Mill-GrormdwaterDischargePermit Date: ll.ll-M Revision: I &oundwarerMonitoring Quatity Assurance Plan (QAP)Page[l af4l rurbidity- r*iatv %& fr- Volume of IVa$uPurged PumBing Rate Calculation FlowRate(Q), in Eg,m. o ,S/50= = ' ).:)Time to evacuate tyo sasing.volumes (2V)T=2V|Q= {p/ *t,* Number of casing volumes evacuated (if other than rwo)-2 I I T I T I I t I I I I T I If well evacuated to dr5mess, number of gallons evacuated_ Name of Certified Analytical Lnboratory if OtherThanEnergyLabq I I Tvne of Srmple Sairnole "Tdkbn (ciiilAi. SpiniileV,pfu$e findii:rrtelf other Eiltered (cinclel P, rtserYative{dded (ciide) VOCs N 3x40ml Y HCI 2N Nutrients N lOOml Y HzSOa N EeawMetals N 2soihi IY) N IINO. TID NAll Other Non- Rediolosics @N a50ml VN NoPreservatirrc Added Gross Alpha UN I,m0 ml AN Hz.SOe W N Other (specify) he no Qfu,q; VN Samplevohrme Yey (y If apreservative is use4 SpecifyTlpe and Qrantity of Prreservative: ,l AqfrJ-/ S.{,;'r t I I t I I I I T I I I t I I I I T I Mill - Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) EIELD DAT Description of Sampling Date: 2.25 -O7 Revision: 2 Page a,O of 4l . ATTACHMENT 1 WTIITE MESA URATIIT]M MILL Location (well name) [Vl,{rr) 3 ffilila WellPurgingEquipUsed: du^oor-bailer WellPump(if otherthan e"*"D)-d,y- t;/ sampringEv enr b\umA Nelu Prev. Well Sampled in SamplingEvent- pHBuffer4.o 1, 0 Dare and Time forPurging /O' 3O' O+ *o Sampling (if different) f pHBuffer7.0 v.o Specific Conductance-fl'.f-ulvflIos/cm wellDepdn . 71 7 DepthtoWaterBefore p*errrL-BJL-CasingVolume(V)4"Well: (.653h) Condue&ince(urg) tSd pHo.flMater lVell Waier Temp .(ruOEL- Redox Potential WeatherCona.0*t t )"a1. Extl-Amb.Temp.(priortosamplingevent),/, , conductance S ?S3 pw (,% 'Tpmnerarrrte lL/. /L Tutbidiry , [3 Redox pot^ti* tr-D--!4! L - ,IL p Redox Potential An>-kS- Conductance s 7s3 pn t(.4 $ t"rp"ot r" ' []. E/ ' Redox Porential W-b]},--RedoxPoten ri*<r-al LZ€ - .lf (i MiIl-GroundwaterDischargePermit Date: 11.17-M Revision: I Groundumter hrtronitoring Quality Assurance PIan (QAP)Page4l of4l Turbidity- Tu6idity aa Volurne of WaterPurged PumBins RatE Calcula .qS' FlowRate (Q), in EFm. o -S/@= = ---r.)! Time to evacuate.two casrng volumes (2V) T =ZYIQ= 36 ,.;* Number of casing volumes evacuated (if other thmtwd--Z If well evacuafed to d4mess, number of gallons evacurted Name of Certified Analytical I"aboratory.if OtherThan Energy Labq T Tvpeof Sample Sqpi.le Take,n(tfnlelr Ei{speJr.qt,Esfindicatelf other ['iltered (circle) Prcsereative Added (dTcle) VOCs N 3x4Oml Y HCX-N Nutrients N lfiIml Y 6[)HrSOr 2N EeawMetals N 250hl"{DN TINO.2NAll Other Non- Radiolocics UN 25Oml VN No Preservatine Added Gross Alphf,s4N 1.m0 ml &N HzSOa V N Other (specify)furry VN Samplevolume Yry lf apraservative is use( SpecifyType and Quntity of heservative: Mill - Groundwater Discharge Pennit Groundwater Monitoring Quality Assurance Plan (QAP) FIELD DAT Description of Sampling Date: 2.25.07 Revision: 2 Page4O of 4l ATTACHMENT 1 WTIIIE MESA URANIT]M MILL t"roprrno 13 ,?L .,. Redoxeotential W Cl{u rrropr* 13.?O Redox Potentiar *, [Zl ' ' _ ,6r{ {: ' t; Location (wenname) kwt 3 a if ilu n*at 4^, /*/,,e4 pHBuffer7.0.7.O Specific Conductance-ff 'lf -uNftIOS/cm Depth to Water Before Pw$rrL ?{,t-1- Casing Volume (V) 4"tVel t € 7,/ | ,<rASSnl condueftince <nug S NZL, - pH of,wdter *r i' SI Z-t:'? WellwaterTemp .And--!3.il- n"ooxpot"n tirt4xQ%rubidity-g Extll'Amb. Temp.(prior to sampling event)-L'-- conawtance-L566 6 e.rlndr"tnao S E (/ pH S.7 pu S.?D , t" Wrot*-1a . LA t"*p"otrrr 13 '7 Z .1 , RedoxPotential @\ LZORedox Potenti ,l (BDJ, ZO- .3V .r/ Condurtnn." S gl 7 cordurtar"" S83f pH gJ 1,,nn 5J Date and Time for Purging h . 3t. O+ *d Sampling (if different) ' Well Purging Equip Used: fiu*Oor -bailer Well Pump (if other than nemetl-DALiafu/ samplingEven, b 'l NorLcr h:ev. Well Sampled in Sampling Eve* fUlU) ? pHBuffer4.o q, 0 w"[ P"p,r, /C Mill-GronndwaterDischargePermit DarE: lt.l7-M Revision: I Grounduater Monitoring Quality Assurance Plan (QAP) Volume of WaterPurged Page4l of47 PumpinF Rate Calculation FlowRate(Q),hBPm. ,e z5/60= =-----rl-i Time to evacuate tyo,castng volumes (2V) T=2VIQ = sf, Number of casingvolumes evacuated (if otherthan two) If well evacuated io drymess, number of gallons evacuated Name of Certified Analytical Laboratory if OtherThan Bnergy Labs Tvpeof Sample Sqqrle Taken (.f,rcIC) nilbred (circle) Preservative Added (citde) VOCs N 3x40ml Y HCX,N Nuffients N l0Oml Y IIalOe N EeawlUetals N 250hI DN IINOI NAll Other Non- Radiolosics @N 250ml VN NoPreservadve Added GrcssAlpha VN 1.m0 ml UN HzSOa V N Other(specfi) bonco^! {d, v N Samplevolume Y0y Ifa preservative is use{ SpecifyTlpe and Quantity of Prraservative: 0 I I I I I t I t I I I I I :l ..:, Mill - Groundwater Discharge Permit Grourdwater Monitoring Quality Assurance Plan (QAP) Description of Sampling Event: Date: 2.25.07 Revision: 2 Page 4O of4l ATTACHMENT 1 WHIIE MESA T'RANII]M MILL EIELD DATA WORI(.SIIEET FOR Location (wennarre). ( utt 9 iffi"'ilu intiar i\ya^t /*lr+e{-. Date and Time forPurging lb']O, O 7 and Sampling (if differen$ Wetl PurgingFauipused fir*Oor-baiter WetlPump (ifotherthan Isr*"|-fu k. Prev. Well Sampled in SamplingEvent- pHBuffer4 .o 4' 0 Well.Depth. rt/4. pHBuffer7.0 v.o Specific Conductnnce-ff*L uLfiIOS/"m DepthtoWaterBefore p*e*LL-t ):!-CasingVolume(V)4"Well: (.653h) pH of Water (avg)* *'-S-- RedoxPotentia tElflL n ruiai v ,Zf Condueance (avg) Well WaterTemp.(avg) Time:. . ,, Gal.Purged- conrrrrctence ZtS L ,"rp"** lS'?.i -, ldoH Y.tl temperaure /4'A - RedoxPotenti rtbal t{ f1l Redoxpotential (ED llZJ .23 ,ls weather cond.- Ext'l Amb. Temp.(prior to sampling eventl-!6 i'-(_, Time: - Gal. Ptrged---'- Time: Gal. Purged_ Crranr*tarrc LlS t/ Time:-;-Gal.Purged- condu"t*", 26 # nr 7'/V Redox Potential (Fh)RedoxPotential (Eh) .ll+ Ij Mill - Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) Turbidi64 Date: 11.17.06 Revision: I Pageal of 41 T I I I I I I T I T I Turbidity Volume of Water Purged When Field Parameters are Measured Pumpins Rate Calculation Flow Rate (Q), in $m.Time to evacuate two casing volumes (2V)-4, T=2VlQ= Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labs. T I I I I T I T Tvpeof Samole Sartrnle Taken (cirele) SimpleVotume finffcateif other thiiri as specified Eiltered (circle) PreseHrative Added (eifcle) below) voG N 3x40 ml Y HCX,,N Nuffients N l0Oml Y IIzSOa 7N HeawMctals N 250mI I\D N HNO, 110 NAll Other Non- Radioloeics UN 25Oml VN NoPreservative Added Gross Alpha VN 1.000 mI EN IIzSOa V N Other (specify) Ur^il"!4f VN Samplevolume YoY (y lf apreservative is use4 SpecifyTypeand Quantity of heservative: T I I T I t I I I I I I I I I I T I T Mill - Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) FIELD DATA Date: 2.25.07 Revision: 2 Page40 of4l ATTACHMF}IT 1 WIIIIE MESA URANIT]M MILL GROT]ND WATER Description of Sampling - ffil1, dinitiats Z'rc,- DAi,^..4 Date and Time forPurging l6'?n'6? and Sampling (if different) Welt Purging Equip Used: dr*por -bailer Well Pump (if other than B"*$Ln)rr** SamplingEven, 0 UrnJ,^l atq Brev. Well Sampled in SamptingEvent pHBuffer7.0.7,0 pHBuffer4.0 Vct Specific Conductance-Z-{ uh,fiIos/cm wellDeptdn. xt/A - Casing Volume Of) 4" Well: (-653h) 3" WeIl: (.367h) Depth to Water Before Purgmg-Z__ Condrictance (avg)- Well WaterTemp.(avg)- pH o.f .Wdter (avg)- Redox Potential (Ehl-futidity -WeatherCond.Ext'l.Anrb. Temp.(prior to sampling event)------- '--(:, Time:-Gal. Purged -Conductariee . p Temoerahrre Time: . Gal.Purged_ Conductance Redox Potential (Eh)_Redox Potential (Eh) T[rbidity Time:- Gal. Purged_Time: ; Gal.Purged- Conductance Conductance RedoxPotential (Fh)RedoxPotential (Eh)_ pH Temoerature | .', }a,r- { ruN Lt Mill - Groundwater Discharge Permit Groundwater Modtoring Quality Assurance Plan (QAP) Datg- 11.17.06 Revision: I Page4l of41 Volume of WaterPurged When FieldParameters areMeasured_ Pumnine Rate Calculation FlowRate (Q), ingPm.Time to evacuate two casi4g volumes (2Y)S/CI= =:T=2VlQ= Number of casing volumes evacuated (if other than two) If well evacuated to drlmess, number of gallons evacuated Name of Certified Analytical Laboratory if Orher Than Energy Labq IVpeofiSamrle Sqmnle TFken (eirrte), SriihiileVolume finfieteffolLct Eiltered (circle) Pneseryative Added (ciTde) VOCs &N 3x40ml Y/[05 HCX, Cgl N Nutrients fi_N l0Oml Y@ HzSOa (D N Hriawlfietals ry- N 250hI CDN IING M NAll Other Non- Radioloeics VN 250mI v'N NoheservatiGtdded Gross Alpha V.N I.0m ml $N HzSOa - @ N Other (specify)@ aN Samplevolume Yg Ifa preservative is use( SpecifyType and Quantity of Prreservative: I I I I I I I I I t I I I I T I I I I I Mill - Groundwater Discharge Permit Groundwater Molitoring Quality Assurance Plan (QAP) Date: 2.25.07 Revision: 2 Page40 of 4l ATTACHMENT 1 WHITE MESA T'RANIT'M MILL Description of Sampling Loeation (welt narne) Iilal S iffi'il, Date andTime torYwgtngl0- 21' 6? and Sampling (if different) WeatherCond. conductne Z/t f { s 1./l (l;,Llz.y -- - Well Purging Equip Used: 4r*ror -bailer Welt Pump (if other nonn"runet)-D&Lidfu/ Sampting Even , bf 'd NrurJdf Prev. well Sampled in sampting Eve*- aL pHBuffer7.0.7_O pH Buffer4 .o--3,-0- Extll=Amb. Temp{prior to sampling even0--6 j- Specificconductance-f'.L ul[Hos/cm w"ttp"pm l3F. S Depth to WaterBefore pweur1l-El.,3Y-- Casing Volume (v) 4' wett:.4.321 (.653h) conduc&rnce (nvg pH of -wdter r*r1f-'t"g - ll* weltwaterTemp .(^ug)3,fu-- RedoxPotenterrfrnil turbidity 1At e,loa*t*n 261{ condu"tnin 2?b3 , -ps (..?f pn ?,1( , * r"rp"ot* l7 .SY remperature 14. 0 I I , Redox potentiaf (prr) 5? ) Redox Potential fehl ,S ?{) Tnrrbidiry-3V'U r,*iaiw 31-L ri"urtt?tt aa.p\re.d&SafT Ttue: 6E7l Gar.PurgeilEitLZ ,or*r*n ZL?T pw l -9E rc^w* 'l3.tt - Redox Potential (tu) -5 7 Y--RedoxPotentiatgxl 9E { ' 4 o,t a ti\, '..' MIt - Groudwater Discharge Permit Cnoundumter Monitoring Quality Assurance Plan (QAP) Turbidity. Date: 11.17.06 Revision: I Page4l of41 I I I I Turbidity Volume of WaterPurgedWhen FieldParameers r*U"urrna 31, C ^ Puqline Rate Calculation FlowRate(Q), ingpm. Number of casing vohrmes evacuated (if other than two) Irvw rw \Y.I .g oY*. ., ,5/60= = ,-) J Time to evacuate.Qro^casi4g volumes (2V) T=ZYIQ= l?3 lf well evacuated to drymess, number of gallons evacuated Name of Certified Analytical Labbratory if Other Than Energy Labs t I I I T T I I I I I T T I I t lVneof Samde Qqdtp& Takeh(tfnfle)'' EifltlilcV.duqc finifcateif other fftered (circle) PrreserYrtive Added "ry VOCs N 3x40ml Y .HCL N Nutrients N l00mI Y IIzSOT N HdawlV[etals N 250hI tp N HNOr )N Alt other N6h: Radiolosics AN 250mI VN No Preservatine Addod Gross Alnha UN 1.m0 ml DTU HrSO, V N Other (specify) br^rt^lQqf VN S4mplevolume ry (y If a preservative is used, Specify"ype and Quantity of Prreservative: T I I I I I I I I I I I t I I T I T t Mill - Grormdwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) Date: 2.25 -O7 Revision: 2 Page 40 of 4l SamplingEve ATTACHMENT 1 WHITE MF^SA T'RANII'M MILL Description of Sampling Event: Location (wennarre) lll$) ll *HJn, Date and Time for Purging f 0'? -? andSampling(if different) Well Purging Equip Used: 4r*Oor -bailer Well Pump (if other than s"*r"q)JZAt&./ Prev. Well Sampled in Sampling nn*r--,LL puBuffer4.o 4) Specificconductance-fl*f-ult&I0s/cm WeWepn , 130 Depth to waterBefo nP*giog ? Z. 3 7-casing volume (v) 4" well: Z\ -Y0? (.6s3h) conduerrhce (^ug 26|ttr. werr water remp . AuglS-LZ*41 weatherCon o.(rrr, CL. ( + Ext'l Amb. Temp.(ptiortosampling even0-196-::- C*t Bioo pHBuffer7.0. {:, , ellnd*r^n 26 7 / ps v.7{",on*"r*u ? [ {? ,, ,,,-p, ?.1( , RedoxPotential (ED 3 (D /. 97 Time: 1233 art cnnrtrctance 2 L< f conductmc.e Zf L{ [ r"rp"o* /5'56 Redox Potential 6nhrjeQ--RedoxPotential W Z?? ' Redox Potential @_337__ t.qsTurbidity. w 7.42 LI, U 2,5? { ', MilI - Groundwater Discharge Permit Grounduater Ivtronitoring Quality Assurance Plan (QAP) Dare: 11.17.06 Revision: I Page4l of4l I I I I I I I I I I I I I I T I t T t Volumeof WaterPurged Pumping Rafe Calculation FlowRate (Q), in EPn. a z5/60= = ----r?J Time to evecuate tw.o. cjglng volumes (2Y)r=2VlQ= lyy' ----' Numberof casingvolumesevacuated(if otherthan wa /. 8 U If well evacuated to dr5mess, number of gallons evacuated Name of Certified Analytical Laboratoryif Other Than Energy Labs Tvoeof Sample Saimnle TrB* (rfit!e). Eiltered (circle) Prreservafive Added - (citrle) VOCs N 3x40ml Y HCL 2N Nrilrients N f00ml Y6D HzSO+N EdawMetals N 250ihl ON IINOI 2NAll Other Non- Radioloeics UN 25Oml v'N NoPneservative Added GrossAlpha [4N l.m0 ml DN HzSOa V N Other(spec$) bonro^.0 fi*r*tt VN Samplevolume Yry Ifa praservative is use{ Specify Type and @antity of Prreservative: 0 I I I I I I I I I t I I I I t t I t t Mill - Crroundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) Date: 2.25.07 Revision: 2 Page 40 of 4l ATTACHMENT 1 WIIITE MESA URANIT]M MILL FOR Well Purging Equip Urd, $"mp or bailer Well Pump (if other nannenneq-DALbfud Prev. Well Sampled in Sampling nvent UIbLZ3 pHBuffer4.o 4. 0 wettoepth , l3 O. { Depth to Water Before p*ernEJ-AI . ZS- Casing volume (v) +" w"n, 13.81 llf <.6s3h) Condue&ince (avg)12 rJVelt WaterTemp .<ur$-UrtL Bedoxpotenriat eOsturbidity , 7 / flELD DAT Description of Sampling Event: Sampler Location(wellname) ltTlhJ lZ Nameandinitials. Redox Potential (Eh) c {-' I .'.L:j. ,41 sampringEv *, b(nmA No,lcr Date andTime torYwgng I b' ? 3' 07 anasampling (if differenO- pHBufferT.Q v_o Specific Conductanct-ff' .L uI/ffIOS/cm WeatherCond.Extzl''Amb. Temp.(pnor to wmPlin1 ev ent) .2L1'' cnnrfircrance 7?gC> n, g'P'ffi [.t/? r"pr** 17'6) '" , Redox potential (Eh) SSF-- Redox Potential Ceh)--Sff Trrrbidity--' trg .qJ cordu.*"" 3f,50 ,,,,au.o^n 818.2 en L.,L{1 pH C.W r"rp"*tor, ,/1.01 .' ,"rowrr*n ll,l9 - 5b" ' , RedoxPotenti"l(8h)-ts-q.{ ,8L MilI - Groundwater Discharge Permit Ciroundwaer Monitoring Quality Assurance Plan (QAP) Dare: 11.17.06 Revision: I Page4l of41 t I I I I I I I t I I I I I I t I T I VolumeofWaterPurgedWhenFieldParamerers *.Wt"uur"A 27 . Q +a/Ls Pumpine Rate Calculation FlowRate(Q),in gq.m.. o -S/fl)= =----, .) )Time to evacuate twp castqg volumes (2V) T=2VlQ = *q Numbei of casing volumes evacuated (if other than two) If well evacuated to drlmess, number of gallons evacuated Name of Certified Analytical Laboratoryif Other Than Bnergy Labs I Tvpeof Samnle Sailio,le'Tfkfn (cirde)' SriihbleVolume (inffcateif otrer Preeervative Added(dltfe) VOCs N 3x40ml Y HCX,'N Nutrients N l0Omt Y HzSOe N HtiiwMetals N 25$bl DN TINO.NAtl Other 'I{on- Radioloeics AN 25OmI v'N NoPrreservative Added CirossAloha [4N 1-m0 ml EN HrSOe V N Other (specify) Ltonro^.0 fr,$t; V'N Sampl6iolume Yry (y If apreservative is used, SpecifyType and Quantity of Prreservative: 0 I I I I I I I I I I T t I I I T T I T Mill - Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) AT'TACHMENT 1 WHITE MESA URANIT]M IVflLL Description of Sampling Sampler Location (wellnarnd W ll Nameand Date and Time for Purgi ng f 0 'Ll ' A 7 arrd Sampting (if different) pHBuffer7.0. Date: 2.25.07 Revision: 2 Page40 of4l v.o t\" Well PurgingEquip Used: 4"^ror-bailer Well Pump (if otherthan n"*rt>)fAtii/ hrev. Well Sampled in Sampting Eve* fhet K pHBuffer4.o 4. 0 Specific Conductance-fl*f-uh[g6s/cm W"ttO.pth . I Z*, ? , Depth to WaterBefore P*srnL&--!-L/-Casing volume (ulo wett: K.f,?{ (.653h) Lp.*_-- z c/ ?t _ J,,!pll:__(.36i/h) Conductance (avg)3 Well Water Temp. tuue)-Js./5f-nuoo* po,*r* er,ffi* iaity'SOi Iveather Cond @t1''Amb. Temp.(pnor to sampling e venq-U:- e,,nd*t^"' 3t1?q cooau"'$n 3 td 3 ,'o, t,zs , Redox Pot"o,i"r @h)--S U---Redox Potential *r', s?r Turbidity.t3 Tiwe: ILI { Gal.Ptnged]fJ.!-- Tine: l2?r\ Gal. PurgedJ--2-Z- conau"t*n 9t33 c*a*t *"JEF/ Temperatuq t5.L\t"*p"*tor" 1.5 ,J .D - RedoxPotential (ED-S?1 -- RedoxPotential W> f W .?1 ,'[7 f; MilI - Grourdwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) Date: 11.17.06 Revision: I Page4l of41 I I T I I I I I I I t I I I I I I I T FlowRate(Q), in BW. o - 5/60 = =-----rl f,Time to evacuate_two castng volumes (2V) T=2VIQ = 4d ,;- Volume of WaterPurged When FieldParameters are Measured Pumpine Rate Calculation Number of casing volumes evacuated (if other than two) If well evacuated to dr5mess, number of gallons evacuated Name of Certified Analytical Laboratory.if OtherThan BnergyLabs TYpeof Sample Spirrrle Tlken (drcle) Etlte,red (drcte) Presemative AddedM-- VOCs N 3x40ml Y HCX,2N Nufrients N l0Oml Y HrSOr N Htiawltfetals N 250frt IlD N HNO.2NAll other Non- Radiolocics UN a5Oml VN NoPrreservative Added GrossAloha UN l.m0 ml DN HrSO. V N Other (specify) @ VN Samplevolume Y0y (9 Ifa preservative is use4 SpecifyTpeand Quantity of Prreservative: I I I I I I I I t I I I I I T I I I T Mill - Cuoundwater Discharge Permit Groufldwater Monitoring Quality Assurance Plan (QAP) Description of Sampling Event: Date: 2.25.07 Revision: 2 Page 4Oof 4l <,ATTACHMENT 1 WIIITE MESA I]RANIT]M MILL DateandTimeforPurgne t(:'21'67 ndSampling(ifditrerenti -/ WellPurgingEquip usu ("mpor-bailer WellPump(ifother nanBemeO-Delbfu/ "/ Prev. Well Sampled in Sampting Frvern l4NS pHBuffer4 .o 4. 0 sampringEven, bf ' 'rd Nater pHBuffer7.0.7.0 Specificconductance-fl'.L g1ftIgs/cm WettO"pn, 137 Depth to water Before p*gine-ld?r"3Y casing volume (v) 4' w"il/F.31/,5 (.6s3h) condueurce <r"g qlq?,pH oJrWdter (avg) - (,, Well water remp . <^w>A,-LZ-Redox Potentirr rrinPr*u,o,r,' S/ WeatherCond.Ext'"I'Amb. Temp.(prior to sampling "n"ot)--8-o.:* {: , cnnrlrcrnnee q l8f Temperature lL gr< Redoxfot"nti"f fnr'l S ?/ . z1 c,,na*ann t/ZO 3 -n t"-p"otor" / Y.ES - (Eh) -ssq.6sRrdoxPotential Turbidity cooau"t^*l2ll c*a*t^n tll tl t .. RedoxPotential tj +-z\ RedoxPotential(Eh) I S U MilI - Crroundwater Discharge Permit CroundwaEr Moniroring Quality Assurance Plan (QAP) Dare: 11.17.06 Revision: I Page4l of4l I I I t I I I I Volurne of Water Purged When Field Parameters are Measured_ Pumuinc Rate Calculation FlowRate (Q), in Epm. o . 5/60 = =--------r-I Time to evacuate lvqo casing volumes (2V) T =ZYIQ= U7 Numberof cdsingvolumes evacuated (if otherthan two) If well evacuated to dryness, number of gallons evacueted Name of Certilied Analytical Laboratory-if Other firan Energy Labq -____--_l I I t I t I I I I r I Tvre of Samnle S.amole T,[kb4 (cfutl6)i SFiiFIeVp"Ipne findii:ntoif o&er X'lltered (circle) Preservttive Addcd (ciFle) VOCs N 3x40ml Y H(x,2N Nutrients N l0Oml Y HaSOr 2N IleawMetals N 250lm,[DN HNO3 2NAll Othei Non- Radiolosics UN 250mI VN Noheservatine Added GrossAloha a4N 1.000 ml UN HzSOa_ I N Other(speci8)@ry VN SaEplevolume ry (9 Ifa preservative is use4 SpcifyT)ryeand Quntity of heservative: I I I I I I T I I I T t t I T I T T t Mill - Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) Date: 2.25.07 Revision: 2 Page 4O of 4l Location (*"nnur*) hN t1 iiffirtllu initiar i\yao /*ln+et-. Date and Time forPurging ll', - ? f ' 0l r"d Sampling (if different) ATTACHMENT 1 WIIITE MESA URANIT]M MILL Description of Sampling Event: Wedther Cond . ha{r\ *V , XXO*tExtll'Amb. Temp.(pnor to sampling e *rO--U-.:- Well Purging Equip Used: 4r*Oor -bailer Well Pump (if other than nr*"t>)tli&/ samplingEven r (n 'il NalOf Prev. Well Sampled nsamplineEventJ/l4lLL!-{ pH Buffer ?. o 7. O pH Buffer 4 .o 1, 0 Specific Conductance-fl'lf-ulvfiIos/cm WeIl Depth , // Z Depth to lVaterBefore p*srrrL-? E- tl- Casing Volume (v) 4" wat,Z l.LZ t653h) pII of Wdter Well WaterTemp. (avg)Redox Potenti"r fpnfffr*uiaity JS cn a*t^n lW condu"txu lI f 7 -pH L.Y7 p f"rp*to* / 7.4 RedoxPotent irtW-Slj- Redox Potential (Eh) SA y r*idiry ,f,f ru,oidi* Y/ conductance qll l{Conductance y Llk3 pu L.t{{ pw e.}s aGt"rperator" /S,77 - Redox Potential fW-61f '- Redox Potential feh) 66. < {:, .23 , bg t; Mill - GrounfuaterDischarge Permit Grounduater lfionitoring Quality Assruance Plan (QAP) Volume of WaterPurged Pumnine RatE Calculation Date: 11.17.06 Revision: I Page4I of41 t I I I I I I I t I I I t I t T I I T FlowRate (Q), in EFm. o ,s/60= =_______r_2 I Time to evacuate tryo-castng volumes (2V) r =ZYIQ= I 3l Numberofcasingvolumesevacuated(if other n*wa l. f 0V If well evacuated to drymess, number of gallons evacuated Name of Certified Analytical Iaboratoryif Other Than Energy Labs T Tvoeof Samrle Sflimnle Takph (circle). SiBiile,.V,o,lu4e (lniffcate'if oher Eiltered (circle) Preserrntive Added below) VOCs N 3x40ml Y "0u ..;Hcr ,N Nutrients N l0Omt Y HaSOr N HriawMetals N 250ht fr)N HNOr TNAtl Other Non- Radioloeics UN 250mI WN No Preservatine Addsd Gtoss Aloha q(N 1.m0 ml Dt[HrSOa' V N Other (specify) LtoncU*! fr*rut VN Samplevolume Yry ey If i ireservative is urcd, SpecifyType and qnntity of Preservative: 0 Yl I I I I I I I I t t I T T I I I I T I Mill - Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) FIELD DAT Description of Sampling Dats: 2.25 -07 Revision: 2 Page 40of 4l ATTACHMENT I WIIITE MESA I'RANIT]M MILL FOR Location (*"nnur*rWWtN (C ff#.Jll, *rtiar ilrva* /*l,re4 Specific Conductance-?' .L uLffIOS/cm sampringEven, b{ ','ll, Nalu' DenthtoWaterBeforePursins TJ. I I conductrince <*ng 2472 well waterremp .t ng)bL-g-RedoxPotenr* enfll ,* iaity '/ L ^6Ext''t-Anrb. Temp.(prior to sampling event)-7 ' ' -{_' Date and Time for Purging 16' 7 O ' 0? nasampling (if different) WeltPurgingEquipUsed 4r ror-bailer WetlPump (ifotherthan s"*r"D)d;^fr/ hev. Well Sampled in SamplingEvent pHBuffer4.o 4J \Me[ Depth /,? { pH Buffer 7. o 7. O e ?3 . 1 / casing volume (v) 4" wrn 37. 7f, <.6s3h) pII of Water ( uoao"reon 21/2 Redox pcltelrti*gn €(3 RedoxPotential(Eh) (yZ 7 ,ZL r*iai," b. () cood*^n 2(75 c*,a*r^n 217 Z pn L. ll *, pH L,N ,, . OL RedoxPotential li Mill-GroundwaterDischargeFermit Date: ll.l?.06 Revision: I Groundwater Monitoring Quality Assurance Plan (QAP)Page 4l of 41 I I I I I t I t I I I I I t I I Volume of WaterPurg ea Pumping Rate Calculation FlowRate(Q), in Wn. o .5/60= = , )J Time to evacuatq two casing volumes (2V) T=2VIQ = 2V0 Numberofcasingvolumesevacuared(iforher tnnnwil I LV If well evacuated to dryness, number of gallons evacuate Name of Certified Analytical Laboratoryif Other Than Energy Labq I I T IVpeof Sample Sahnle Talien (eincle) Sninrile Volume (indicateif other Filtered (circle) Pneservative Added lcifcle) thilh as specified below) VOCs N 3x4Oml Y HCI,,N Nutrients N l0Oml Y HiSoa 2N HeawMetals N 250mI fiDN IINOr 2NAll Other Non- Radiolopics @N 250mI VN NoPreservative Added GmssAlnha [4N 1,000 ml VN IIzSOa V'} N Other (specify) boneh.l t"w; VN Samplevolume Yry (y E a prcservative is used, SpecifyType and Quantity of Preservative: 0 osso I I I I I I I I I I I t t I I I I t I Mill - Groundwater Discharge Permit Groundwater Monimring Quality Assurance Plan (QAP) FIELD DAT Description of Sampling Event: Date: 2.25.07 Revision: 2 Page4O of 4l Location (wettnane) /lll/J fl ATTACHMENT 1 WHIIE MESA URANIT'M MILL EO Date and Time forPurgi"g 10. ig' 07 *nd Sampling (if differen$ Well Purging Equip Used: Ar*nor -bailer Well Pump (if other than n"lrlnt>)tl,y#d Sampling Even , b( ' 'qA NrurJC,f " Prev. well Sampled in sampling e** fu-* pHBuffer7.0.v.o pHBuffer4 o l/. 0 wen*pn , ll 1Specific Conductance-ff ' .f -uhrHos/cm Depth to Water Before p*sr"L->0-83- casing Volume (v) 4" wen: L t{. I 0 S (.653h) CondueHnce t*gl 3" IVel[: (.367h) pHofwater (ruil 6- {-' Well Water Temp . <une\-b.]-Turbidity .al WeatherCond.C Extl-Amb. Temp.(prior to sampling e*nO-$-?' cooao.hr." /?0S coo;du"rxu l3(1 , ,,,- pH (.s7 w (..Y3 , Temperature t3.w Redox Potential (BDJ 0 - Redox Potential Gr-n> A / L Conductance Tvrbidiq 'n Turbidity ,57 irre-du r.-Gtl.Pweed 33.7 7 Tirc: 6f,,2Y Cal. Pureed-3C-ZZ- c*ar**n IKL ps A .3? ,* (, 9'{ t"*p"ot* 1 3. ?6 - RedoxPotential RedoxPotential glil (: .7L Mill-GroundwaterDischargePermit Date: lt.l7.M Revision: I Cnoundwater Monitoring Quality Assuance PIan (QAP)Page4l of4l Volume of Water Purgcd When Field Parame ters arcMeaswd 3 L E Puqpine Rate Calculation FlowRate(Q),hgpm. ,a z 5/60 = =-----.ll Time to evacuate tyo casi4g volumes (2V) T =ZYIQ= 3 88 - Numberbf casing volumes evacuated (if other than t If well evacuated to d4mess, number of gallons evacuated Name of Certified Analytical Laboratoryif OtherThan Bnergy Labs. IVreofSamule Samnle Takeh (clrtlB). Eiltered (circlel P+rservptive-Added(ci4de) Hb*) VOCs N 3x4Oml Y ,H(L N Nutrieirts N l00ml Y 'Hz'SO4 (9 N Eriawltfietals N 250'tr,1,N IINO.NAll Other l{on- Radiolosics @N 250mI VN Nohqservative Added GrcssAloha N l.m0 El D[IIuSOa 2N Other (specify) (anco o fr*rrr^ VN Samplevolume Yry (y Ifa preservative is use4 SpocifyTlpe and Quantity of heservative: 0 I I t T I I I ,l :ilia:, Mill - Groundwater Discharge Pennit Groundwater Monitoring Quality Assurance Plan (QAP) Dats'- 2.25.O7 Revision: 2 Page4O of 4l ATTACHMENT 1 WHITE MESA T'RANIT]M MILL {,.',. ' eH (. =zf , t"rrry"t* f{ L{ ' " ., RedoxPotentialCh) S Y/ ?.32 FIELD DATA WORXSIIEET FOR GROTIhID,WATEB Description of Sampling n*rrt I^ (lu*fie{ hlound Nr&l pHBuffer7.0 v.o Specific Conductance-ff'lf-ulvfiIoS/cm W"tt O"ptf, | .} Z Depth to water Before p*g,ne-J-YJ-1- casing volume (v) 4" well: conductar.rce a"el,,C7 tr7,,', pHofwdter *rr'::t':-VT-""' Well Water Temp . (^ng$+-gedoxPotentiar t-Et$S{flTurb rurr, Z . Z f Weathir Cond W Ext'*Amb. r"*p tpri* to sampling r:toa*t^n 37il ps (.// r. prua* f 4"5 I Redox Potenti"l (ED-55Q.- s.z7 Location(w"rrnu*") Il4w ZE ffi:'H, ntiar i\ynt /elrue4 Dare and Time forPurgi rg l0'27' O? *asampling (if different) Welt purgingEquip Used: $r*Oor-baiter Wetl Pump (if other tnansenrre|)-drr*/ samplingEven, bn 'r' Noln Prpv. Well Sampled in Sampling P*"t&Jrl ZB pHBuffer4a 4.0 . Gal. conara^"" S?il cona*w"" 3788 ps 1" .27 t"mp"raqtre l,{ f53 " Temperaturq tL{.fu Redox Potentiat (ft)-{LYS--Redoxrotential eal 6lif ' 'i., !*,on, -?*o; 1,,e1il,+7 Mi[ - Groundwater Discharge Permit Crroundwater l\donitoring Quality Assurance Plan (QAP) Date: 11.17.06 Revision: I Page 4l of41 Volume of WaterPurged / Pumoine Rate Calculation Number of casing volumes evacuated (if other than two) FlowRate(CI, in gpn a z5/60= =--., ).1 Time to e\racuate trvg casrng volumes (2V) T=2VIQ = w If well evacuated to dr5mess, number of gallons eiacunted Name of Certified Analytical Laboratory if Other Than Bnergy I-abs. IVoe of Samule I Saimfile Tirlien(dqdf), Siihfile,,Volume(ffiiiteffdther f,Ittertd (cirde)@ryq$y,eAd4ed "ry VOCS N 3i40ml Y HCL 2N Nutrients N lOOml Y IIdSO 2N IleawMEtttls N 25fi.fr|TDN IINO.NAll Other ' Non Radiolosics gN 25Oml 9'N NoPreservative Added Gross Alphr [(N 1.000 ml DN HrSO. V N Other (specify) he ,rO^l.foq', (v N Samplevolume YCy (9 Ifa preservative is use{ SpecifyType and Quantity of Prreservative: T I I T I I I ''1 I I I I t t I T T t T Mill - Crroundwater Discharge Permit Grourdwater Monitoring Quality Assurance Plan (QAP) EIELD DAT Description of Sampling Event: Date: 2.25.07 Revision: 2 Page4Oof 4l ATTACHMENT 1 WHITE MESA URANIT]M MILL i#Jil, io*i,tr i\ya^t /*1,,,.e4 Date and Time for Purgine lb2)10L andsampling (if different) €d: Ar*Oor-bailer WellPumP(ifotheWellPurgingEqurpused 4"*or-bailer WellPump (ifotherthan g"*r"tl]Ddv e./ Prev. Well Sampled in Sampling Frverc!!-N-L pHBuffer4 .o 4, 0 sampringEventb 'd NAtff pHBuffer 7 o 7"O Specific Conductance-ff' .f-ulttrIOs/cm WeU n"pth I Z 0 Depth to Water Before p*s,n&-lJ6-!-g- Casing Volume (V) 4' wet: 2.?€ I t653h) 3" lVell: (.367h) Well WaterTemp.(avg)-Redox Poteirtiai tEf.t)-turtiaity weather con a Cl col i b ( Extl'Amb. Temp.(prior to sampling even D- ( "':-(: , ( conductance--93L3 s s.Z'l t"rp"rotur" 13, FO Redox Potenti rt tsri-fC L-- Temperafure '. - Redox Potential (Eh)- Conductatiee - p Tem.oerature , Redox Potential (Eh)- Turbidity Conductanceconductance- nH pH Temperahre - i; Mill - Grormdwater Discharge Permit Groundunter Monibring Quality Assurance Plan (QAP) Date: 11.17.05 Revision: I Page4l of4l T I T I I T T I I I I I I I I t t t T Volume of WaterPurged Pumpine Rate Calculation NumbEr of casing volumes evacuated (if other than two) FlowRate(Q),in Epm.. a z5/60= =---, ).1 Time to evacuate_two casrng volumes (2V) T=2VlQ= I? ,,",.i*. If well evacuated to dr5mess, number of gallons evacuated Name of Certified Analytical Labomtory if Other Than Energy Labq Tvneof Sample Salrole Taken (drc!e), filtered (cirde) PruersrdveAdded (ciFle) th{it iir gpeciffd VOCs ,N 3x40ml Y HCX,N Nutrients N fOOml Y HrSOr N Eriawlfietals N 250ffi,MN HNO. M NAll Other Non- Radiolocics @N 250ml g'N NoPnqservatirrc Added GrossAlphe q4N 1.fit0 mI DN HISO. V N Other (specify) br;rl^!futf VN Samplevolume YCy (y lfa preservative is used SpecifyType and Quantity of Preservative: I I t I I I I I I I I I I I I I I I I Mill - Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) T'IELDDAT Date: 2.25 -O7 Revision: 2 Page4A of 4l ATTACHMENT 1 WIIITE MESA UMNIT]M MILL Description of SamPling samPrer i?\ "' /*l*rt,Location (wellnarre) /hlN Z{ Nameandinitials-, pHBuffer7.0 v.o Specific Conductance-77''L ulvfiIos/cm Prev. Well Sampled in Sampling Event:fuadlZ pHBuffer4 .o- '4) w"tro.pm- / I f Dare andTime torYwging h.?E'(* and Sampling (if differenO- well purging Bquip ur..dl 4"*r- -raiter well Pump (if other *aneenrr*tbl); b/ sampring Even,I4 *' qA Noter Depth to water Before putan*-?7 i-/-- casins volu-" t"l1'#il1'295,.!:;il1' conduetrir.rce (unel 3 lg ! - pHoJWdter toue) ,-[:-37-'- wellwaterTemp.t"neil3-EZ- ri.c*pur"ni"r(EhftL,*iotv' f9 weathercon a (]ler t , bt,l Ext'{ Amb.Temp.(priortosamPlingevenq-V r' .:- ps L.?7 p Redox Potenti ,t (Ek)J3-33-- Tffiidity '% RedoxPotenti"rGh) 3 Y 3 Tvrbidir ' q tr (.' cono*t",i"" 3/ &/ ,, , ,,', , coodu.t nr" 31 73 conductancq 3t?s pH clb eH (-w Temnerature '' ,lt, 6Z . Tentwra, re 16' g"l' ,' Reddx Potdnrt t @h)-3 "E 3 t MiII - Grounduater Discharge Permit Groundwater l\rlonimring Quality Assurance Plan (QAP) Date: 11.17.06 Revision: I Page4l of41 Volume of Water Purged When Field Paralneters are Pumpine Rate Calculation Flow Rate (Q), in gW. a , Time to evacuatg' two caslng volumes (2V) s/oo= = ,S i*=zie=-[47 - - i: Nuuiberof ttasingvolumesevacuated(if otherthan *A I . ft ,04 \).'{,r^* If well evacuated to d4mess, number of gallons evacuatr/' Name of Certified Analytical Labomtory if Other Than Bnergy l,abs Tvoes[SamPle Sqmile Takdir (cirdB), SlmfleV,qlupe(lnffcatoifottet f,'iltered (cimJeI Pneservative Added (cirde) VOCs )N 3x40ml Y HCX,, V N Nutrients N lfi)ml Y HrSOr 7N HdawMetits N 2s0tid tDN IINO. M N All Other Non- Rodiolocics UN 250ml 9N No Prbservati\re Added Gross Alpha UN l.mO ml DN HrSO. V N Other (specify) Upto | fr*n' VN $auplevolume YW (y If aprcservative is use{ SpecifyType and *Ulof Preservative: I I I {: ' T t I I ,l ::.'il il ',...:".1 ll .t 'I I I I I I I I I I I Mill * GroundwaterDischarge Permit Groundwater Monibring Quality Assurance Plan (QAP) Date: 2.25 -O7 Revision: 2 Page40 of 4l ATTACHMENT 1 WHITE ME.SA URANIT'M MILL FOR Description of SamPling E Location (w ell namd -fu,JLZL Sampler pHBuffer7.0.7.O . Ztr Dare and Time for Purging | 0 ' ?3 ' 6 7 *d Sampling (if different) Well Purging Equip U r*, 4r*or -bailer Well Pump (if other than n"*rq -fu C'*. samptingEven, b '\A Nortc,f Prev. Well Sampled in Sampling nvent]}//!L*!-!Z pHBuffer4 .o 4' 0 SpecificConductance-ff'.L u}fiIos/cm lyettDepth I Z /. 3 ? DepthtoWaterBeforePrrryirne //4 CasingVolume(V|4"Well: (.653h) conduetdnce <r"r> ?3/ 7 ,- pHof,writer*r.i"#l'i'--:'? Well lVater Temp. (ure)--[S.-?5-Redox Poten titt Gflttlturbidity, 3 7 trreather cond Wff1t Amb. Temp.(prior to sawtins "nenit227- Time:, . .. Gal.Purged-- - Titne: ,--Gal.PurgeC--- . - -corao.t.o* 33 [3 c^'*r"*in , ] 377 -pa L. 7 tr n* , c'85-' , ^t"^protrn /(, 0, Z RedoxPotenti"f (Eht S5 a- T"p"o* 16,37- ' Time:- Gal. Purged- cooa*r*n SS 13 pH ( t(l t"^poutrn /l ,76 ' Time: ; Gal.Purged- Conductance 3LI3S* f,,rf, r"*r-ryorry , l'{'(Z- RedoxPotential ff:rl tlt 7 RedoxPotential(Eh),'..t': "73 MII - Grourdwater Discharge Permit Crrounds/at€r l/trof, ibring Quality Assurance Plan (QAP) Turbidity Date: 1t.17.06 Revision: I Page4l of41 T T I I I t I t I I I T I Turbidity Volume of WaterPurged When FieldParameters arcMeasured_ Prrmnine Rate Calculation FlowRate(Q),ingpm. o -5/60= =---' ) )Time to evacuate two casmg vohunes (2Y) T=ZVIQ = Numtier of casing volumes evacuated (if other than two)- If well evacuated to dqmess, nurrber of gallons evacuated Name of Certified Analytical Laboraiory if OthEr Than Bnergy Labg I I t I T I Tvneof Samde Sairiple Trikeh(ciry), FIttercd (circle)Fespwative Adriled (drcfe) VOCs N 3i40ml Y HCI.N Nutrients N r00tlil Y HrSO.7N EdawIvleals N 2solhl TID N IINO. M NAll Other Non- Radiolocics UN 250ml VN NoPreservatirre Added Gross Aloha [(N t.m0 mI DN HrSOr V N Other (specify) boncl^! frh; VN Samplevolume Yry (y Ifa preservative i$ use{ SpecifyTypeand Qranti$ of Prreservative: 0 I I I I I I I I I I I I I T I I I I T Mill - Gmundwater Discharge Perrnit Groundwater Monitoring Quality Assurance Plan (QAP) FIELI}DA Description of Sampling Event: Date: 2.25.07 Revision: 2 Page 4A of 4l ATTACHMENT 1 WIIITE MESA URANIT]M MILL Location (*"nnur*) lflN lS mJn, initia, Qya,*> Aol*.a^ A Well Purging Equip Used: $r*por -bailer Well Pump (if other than Bennet) [2-T. SamplingEvent brZou, ) a:oleL hev. Well Sampled Date and Time for Purgi "s I rt . Z3 ' 6l *d Sampling (if different pHBuffer7.0.a.o pHBuffer4.0 Specificconductance-ZU*Lumlos/cm wellDe4h . ) Zl- 33 Depth to WaterBefore Purgrn&-Casing Volume (V) 4'Well: (.653h) 3" IVell: (-367h) pHof,Water(avg) ,. Well WaterTemp.(avg)- Redox Potential (Eh)-turUidity -Weather Cond.Ext'lAnrb.Temp.(priortosamplingevent)---- - in Samplifrg Event tvTtJ lZ 4.o ft ' , ,' Time:--- Gal. Purged- *n6ugianOe Redox Potential (Ett)- Turbidity- Trme:- , ,,. -Gal.Purged-- -Conductruiee Redox Potential (Ett)- Turbidiry - pH Temperahre- Time:-Gal. Purged- Conductance- Redox Potential (Ht)- Time: ; Gal.Purged- Conductance pH Temperature RedoxPotential (Eh)- L^pr,;^^a t fi4N zt MII - Groudwater Discharge Permit Ciroundmrarer ldonitoring Quality Assurance Plan (QAP) Date: 11.17 -M Revision: I Page4l of4l Volume of lVater hrged When Field Parameters are Measured Pumpine Rate Calculation FlowRate (Q), ingpm.Time to evaeuate two casr4g volumes (2V) 5/60 =T=2VlQ= Number of casing volume.e evacuated (if other than two) lf well evacuated to dr;mess, number of gallons evacuated Name of Certifiod Analytical Laboratoryif OtherThan EnergyLabS IYpeofSapple Samole Taken (circle). SaihtilIe V-olume findieateif other f,Iltercd (cirde) PresefvativeAdded (tfr-de) VOCs N 3x4Oml YN5.HCX, & N Nufrierts N f00ml YN HrSOe @ N Eriaw lfietalg N 250frI 6DN IINO. C? NAll Other Non- Radioloeics vN 25Oml &N NoPreservatftre Added GrossAloha qN 1-m0 ml c9N HzSOa - ry N Other (specify) b^rrrtr 5n) AN Samplevolume YN If a preservative is use( SpecifyTypeand qrantity of Prreservative:-_ :l- I I I I t I T I I I I I I T I T T I T Mill - Groundwater Discharge Pennit Grourdwater Monitoring Quality Assurance Plan (QAP) Date: 2.25.07 Revision: 2 Page4O of 4l ATTACHMENT 1 WHITE MESA T]RANII]M MILL FIELD DAT Description of SamPling Event: Location (*"ttour*\ fWN 27' 'iffi% Date and Time for Purgi ng / rt ' ZZ- 6 7 arrd Sampling (if different) Well Purging Equip Used: 4r* * -oailer Well Pump (if other than Eenn et))d)&/ ll sampringEven, bf ,qA Nakr hev.wett sampted insampting Event */h pHBuffer7.0.v.o pHBuffer4.0 1"0 SpecificConAuctance ?f'.S ulvntoSlcm WellDepth, 7S Depth to lyater Before P*g,ng-.,$-115- Casing Volume (v) 4' walrZ( - ll< 7 (.653h) Condrl0trtnce t".ug PH of,Water ( I.t ".' coodo"t o"" 14 f 7 I .:t ..: p t".p"ot* /Y-56 ,i RedoxpotentiatGr,) 5 75r RedoxPotential (Eh) S7? . cordu"tuo""--1!-5J w L.\K pH (.si t"ropranrc l1.8L ' Redox Potential (Et )-*5JL- Reilox Potential @h :*;tilr. Mill - Groundwater Discharge Perrnit Groundwater Monitoring Quality Assurance Plan (QAP) Date: 1t.17.06 Revision: I Page 41 of 4.1 I I I I votumeofwaterPurged , W sSZ(Aful Pumpine Rate Calculation Flow Rate (Q), in gPm. If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labs 5/60 =33 Number of casing volumes evacuated (if other than Time to evacuate two casing volumes (2V)T=2VIQ= [S 5 I I I I I I I I I T t I t I Tvpe of Sample Sample Taken (circle) SriiniileVolume Cudisatcrf other Filtered (circle) Preservative Added (ciTcle) thdil as specifred helow) voG )N 3x40 nl Y HCL v)N Nutrients N l00ml Y HzSOc N lleaw Metals N 25Oml frDN HNO3 M NAll Other Non- Radiolocics UN 25Oml (,N NoPreservative Added Gross Alpha a(N 1,000 ml DN HrSO, I N Other (specify)@ry VN Sample volume Y0y (9 lf a preservative is used, Specrfy Type and Quantity of Preservative: i ,61 o,od*t^n 3v6? pn S.5? l" I I I I I I I I I I I t T I I I I I Mill - Gmundwater Discharge Pennit Groundwater Monitoring Quality Assurance Plan (QAP) Date: 2.25.07 Revision: 2 Page40of 4l ATTACHMENT 1 WIIIIE MESA I]RANIIIM MILL SamPler Location (wettnaw)j44U 2{ Nameandinitials Date and Time for Purging /rt - 7 " - O7 *asampling (if different) Well Purging Equip Used drr*nor-bailer Well Pump (if ofirer than n"rn tl]Dflvob/ FIELD DAT Description of Sampling Event: SamplingEvent LAILUTWA W0&( , pHBuffer 7.o 7. O Prev. Well Sampled in Sampling E**illd-?LI pHBuffer4 o 4) Specific Conouctance-fl,.f-u6toslcm ryetl Depth , / 1 0 DepthtoWaterBefore prrerrr*-7?. !!-CasingVolume(V)4' Welt, -Zl,l{ldSSln'1 weatherCon u.ClA , (l ( , Extll'Amb. Temp.(pnortosamplingevent)--& 1-' - , condueance <rng 3tr0?- ,, : - Well Water Temp . (rvg,\]!,-E Z- Tempera$rc tq. Ll I 3" Well: (.367h) pHof water(n"gl S.7-',, BsdorPoten drrt t*>lLLt,*iairy . Z I conarcrs;u , Sfl O ,, ,- pn S.t) , ternprutlue 14- tZ , ' .', Redox pt ntirt<W Y4? RedoxPotential (ED q [ tr ' .3L . Turbidi Gal. Condrctance 36(), ,IL\.-- Redox Potential fW \61 : Redox Potentiur fen) ' tl ?J ( ., , ,_ Mill - Groundwater Discharge Permit Groundrvater Monitoring Quality Assurance PIan (QAP) Date: ll.17.O6 Revision: I Page4l of4l I I I I Volume of WaterPurge A Pumoine Rate Calculation FlowRate(Q), ingpm. .o -5/60 = =-:.}) Time to evacuate two casmg volumes (2y) T=2VIQ = l7o - Number of casing volumes evacuated (if other than two If well evacuated to dqmess, number of gallons evacuated_ Name of Certified Analytical Laboratory' if Other Than Energy Labs ,I Tvreof Samnle Saimnle T$en (circIc) SriihiilleVolnme findicateif other Eiltered (circlel Preservafive Added (dFIe) VOCs N 3x40ml Y HCL,.N Nutrients N 100mI Y HzS-Or N Heaw llfletals t N 25Oiilt MN IINO3 2NAtl Other Non- Radiolosics @N 25Oml UN No Presenatine Added Gtoss Alpha q(N l.mO mI UN HzSOa- I N Other (spocify) '(aonco^.0 fr***l VN Samplevolume Yry (9 If a preservative is use{ SpecifyTlpe and Quantity of Prre.servative: 0 Mill - Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) FIELD DAT Description of Sampling Event: Date: 2.25.07 Revision: 2 Page 4O of 4l ATTACHMENT T WTtrTE MESA T'RANII]M MILL Loeation @arndrnet [YlN 21 m'il, nitar i2ynt /4/,r,,e4 Date and Time for Purgi "e liJ!,-fi-*dsampling (if differen0 pHBuffer 7.0 7.O Well Purging Equip Used: 4r Oor-bailer Well Pump (if other U*e"rrre0-DlAbfu/ sampringEv *t b4unA No,er Prev. Well Sampled in Sampling gnrrfiW2/ pHBuffer4 .o 4, 0 Specific Conductance-fl'.L ulr,fiIgs/cm WAI n"ptf, , / 27 Depth to Water Before p*srng--l-}s .8'l- Casing Volume (V) 4" w.tt l< 01fr (.653h) conduetrince (rng, {try 7 pHo.frvater*rr 1",H"7-.1''? Well Water Temp. (urgt-J*L-1.I-Redox Poten tiil G$'llJ_rrtuidiry 1,, 8 I weathercond.DaOf Ext1l.'Amb. Temp.(pdor to sampling even[--!l:-' ' - (.' conauctance f $*Sf s 5.77 Temperature / j. d3 Redox Pot"ntid 1en) JE q - 3 "(7 c*a*tur." l S9L pn S.87 t"rp"*trr" f3'$O ' RedoxPotential (Eh) ? 3 Y Turbidiry 2.-s2- RedoxPotential 6Eb " i conduct;llrce Lf S.< tr ,ro*",rr*- l3'{'? . Redox Potential L, A7 @,% i; Mill - Groundwater Discharge Permit Groundwater lfi oritoring Quality Assurance Plan (QAP) Date: 11.17.06 Revision: I Page4l of 47 I I I I I I I I I I t I t I T I t I t VolumeofWaterPurgedWhenFieldParamerers araWensard 30 eJh.T Pumpine Rat€ Calculation FlowRare(Q),ingPm. o ,5/60= = , )J Time to evacuate Eyo casr4g volumes (2V)T=2VIQ= ?l n,;* Number of casi4g volumes evacuated (if other than two) If well evacuated to dqmess, number of gallons evacuated Name of Crrtifisd Analytical Laboratory if OtherThan Energylabs TvpeofSamole SairrpleTir* (drgP): SiihfleVdume(fuficiteffother fftered (circle)rPruserrrltive Added tdple) flif;iias specified VOCs )N 3x40ml Y(p5 HCX,zN Nutrients N l0Oml Y HrSOr N Itreaw l\,ietals N 250lhl.(DN IINO,VNAlt Other Noi- Radiolocics @N 250dl v"N No Preservative Added CrtossAloha UN l.mO ml DN HaSOe V N Other (specify) brnco^.l d"r,r; VN Samplevolume Y0y Ifa praservative is use4 SpecifyType and Quantity of heservative: 0 I I I I t I I I I I I I T T T I t I I Mill - Crroundwater Discharge Permit Groundwater Moniforing Quality Assurance Plan (QAP) Description of Sampling Dats: 2.25 -07 Revision: 2 Page 40 of4l ATTACHMENT 1 WIIITE MESA T]RANII]M MTLL Location (wennane) tlN BO ilffiX'ilu i^tiar Q\au /*l,ue{-. Date and Time for Furgi oe l0 ' Z'l' 6 V *d Sampling (if differenO- pHBuffer7.0 v.o WellPurgingEquipUsed: ("*or-bailer WellPump (ifotherthan s"*"tl)-dr; h./ sampring Ev ent L,(At^qA Nat*(hev. Well Sampled in Sampling n**AlLLl pHBuffer4 .o 4. 0 Specificconductance-ff'lf-uNftIos/cm WellDepth . // b ps (.3? rr prruwn lZ'7L (.' e^rau"wnn Z06D ,, ,, , p t"*p"o* /3-72 i, Redox Potcnti * gnlJ '17--Redox Potential @D 3 7L Turbidity..07 cona*t^n 26{{ pH /.s3ps 6.3K t"^pr*t* 3,b4 . . r"rrrprrro* 17. Vl' Redox Potential fW E 0{ \ RedoxPotential fea> 3 V0 ' *L _0( t ..lt.; Mill - Grouduater Discharge Permit Grounduater Monitoring Quality Assurance Plan (QAP) DatE: ll.l7-M Revision: I Page4l of 41 I I I I I t I I I I I t I I I I I t T Turbidity. Volume of Water Purged Pumnine Rate Calculation Number of cabihg volumes evacuated (if other than two) FlowRate(Q), in Wm. + z5/60= = -. )J Time to evscuate_two casipg volumes (2V) T=2VlQ = lzo * If well evacuated to d4mess, number of gallons evacuated Name of Certified Analytical Labomtoryif Other Than Energy Labs- TvpeofSrmnle WdeTakeir (ciirl&)' X'Ittered (circlet Preservative Added Gir-Aet VOCs N 3x40ml Y H(x,2N Nutrients N l0Oml Y HzSOr N I*iawItfietals N 250,mt DN TINO.2NAll Other Non- Radioloeics UN 25Oml VN NoPrreservative Addcd CrrcssAlohl s(N 1.m0 ml UN IIaSOT VN Other (specify) bonch,! fr'm; VN Sauplevolume Yry (9 If apreservative is use4 Specify[rpe and Qnntity of Prreservative: 0 I T I t I I t I I I I I I I I t I t t Mill - Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) Description of Sampling Date:2.25.07 Revision:2 .' Page4Oof 4l ATTACHMENT 1 WIIITE MESA URANIIJM MILL Date andTime forPurging I b' I I' frX md Sampling (if different) Well Purging Equip Used: Au*ror -bailer Well Pump (if other than n"m"tl]Dtittrt/ SamplingEven, b( ;nll Norlq( pHBuffer 7.o 7. O Prev. Well Sampled in Sampling event2lb)-;C) pHBuffer4.O 4.0 Specific Conductance-fl'.f-ultvtrIos/cm WeU p"pth I 3O Depth to Water Before p*ernL1,W- Casing Volume (V) 4" wen:3tr161f1-(.653h) CondueElcet"re)L pHo.f,Wdter(a WeatherCond. Well Water Temp. ("rel-L!L,f-Itedox Poteirt *, f*b>127r*ron,.3L Ext'*Arnb. Temp.(pnor to sampling even q-! 3::-(_' Location (wenname) ll4tt 3l ii#r'ilu innu, il\aa /,4lue4 coodo"t*n l719 ps L,8? c*ra*t^n l7/0 -P, L,F , rr p"o* l{.Zf , - . Redox toterrti*fgrl 1l ti RedoxPotential @D q30 Turbidity .03 o" [,1L. ,"rp"r"*r. /Y.37 .' conrlrrctance l+ lq condurt^"" I ?08 on (-?7 ,"rrr*.^* 11'87 - '{32RedoxPotential@tt, .l lu t.:Redox Potential (Fh) ,3L Mitl - Gronnfiiater Discharge Permit GroundwaEr Monitoring Quality Assurance Plan (QAP) DatE: ll.r7.M Revision: I Page4l of4l I I T I I T t I I I I I I I I I I I T Volume of Ttrater Purged Pumoine Rate Calculation Number of casing volumes evacuated (if other than FlowRate(Q), in EFm. o .5/60= =- . t Timeto evacuaQql,o castng volumes (2V)?l ^r.\T =ZYIQ= 2LSU *-i,,- If well evacuated to drlmess, number of gallons evacuated Name of Certified Analytical Laboratoryif Other Than BnergSr Labs Tvpeof Samole Sqqple Takbh(4{ttp} S*niileVp.Iuqe findicateif other filtered (circte) hservptiveAdded (circle) VOCs )N 3x40ml Y HCX"zN Nutrients N l0Oml Y Hr.SOe N II6ew ltfiefals N 250frt DN HNOJ M NAll Other Non- Radiolocics AN 250ml [a'N No Preservative Added CrrossAlpha VN l.mO ml DN HzSOe- V N Other (specify) (i, no o.tuV' VN Samplevolume ry Y. If apreservative is use4 SpecifyType and Quantity of Preservative: t I I t I ,'l -,1 ;: ,l '. :.4,, ;l il .'f,i r: iil Location (*ennarue) il4t*t 3Z ilHl'ilu initia, i2ynt /nln+e{. Date andTime tofiwgrng lh' Z<l' 6? rrd Sampling (if different) Welt Purging Equip Used: 4r^ror -bailer Well Pump (if other than n*rro>)di&d samplingEven, bf ', 'ql- N\rkt Prev. well Sampled in samplingEvent- pHBuffer 7.0 7. O pHBuffer4.O 4.0 SpecificConductance-fl*f-u}rfiIos/"m W"Un"ptn /3 Z.( Depth to Water Before p*r-*fut. fl- Casing votume (V) +" w.n= 9{. Zif (.653h) .r4 Oa 3" pell: (.367h) Conductance(wil \l l [ . pHofWater(avs). 6.S() Well Watrcr?emp. furgl-l S.3r5-n"or* pot"n rr* <n+f6*iairv I d .t 3 Mill - Crroundwater Discharge Permit Groundwater Monibring Quality Assurance Plan (QAP) FIELD DAT Description of SamPling Event: Page 4O of 4l ATTACHMENT 1 WHITE MESA T]RANIIJM MILL ( r,,od*t^n 348L r,,t;drrc"nnn 3f E y : s A/? p t"rp"** /?. 7 rrmp"oarn ff,?0," , Redox Potentiat (Eh)-!LL - Redox Potential fer,) ZY,C Turbidity 13^,L Turbidity 4.*z conductance 3q ft ps A.s? t"rp"otnr /S.2? -Redox Potentiat Gh) Z?L c*d*t*"" 3qUN, L,LY ,,rrrrWotrn . I {,-, 0L -- Redox Potential ftO Z '{8 ' , t0 'tI*b._Jb ,I ,', Mill - Grounduater Discharge Permit Groundwater hfionitoring Quality Assurance Plan (QAP) Date: 11.17.06 Revision: I Page4l of4l I I I t I I I T I I I I I I I I T I T VolumeofWaterPurgedWhenFieldParameters u*Wt*rna S ?, / Pumnine Rat€ Calculation FlowRate(Q),ingpm. o ,5/60= =---= ) )Time to evacuate t T=2VlQ= Number of casing volumes evacuated (if other than two If well evacuated to dryness, nrmber of gallons evacuated Name of C-e.rtified Analytical Laboratory if OtherThan Energylabs. TYpeof Samole Sarrple T*"Nn (cirrlet. nilbped (circle) Presenative Added (ciTcle)ffia VOCs N 3x40ml Y HCL 7N Nutrients N l0Oml Y H,SOI N HriawMetals N 250riii M.N IINO"2NAtl Other Non- Radiolosics U N 250mI v N'NoPreserv'ative Added GrossAlpha UN l.mO ml MN H,So. V N Other (specify)tu4r VN Famplevolume Yry (y Ifa preservative is use4 Specify[ryeand qlantity of Prreservative: I I I I I I t I I I I I I I I t I T t Mill - Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) T'IELDDA Descripion of Sampling Event: Date: 2.25.07 Revision: 2 Page4Aof 4l ATTACHMENT 1 WHITE MFfA I,RAT{IT]M MILL Location (wennarue) fuus I O iffi'il, initiats (lao/et Oc,L Date and rime forPurging l?'.U'O7 and sampling (if different) Well Purging Equip Used: -pump or _bailer Well Pump (if other than Bennet)- SamplingEven t (.%-/ w-fr Prev. Well Sampledin SamplingEvent- pHBuffer7.0 ? ,tl pH Buffer4 .o qi Specificconducr*nc"-f7^1ulrfiIos/cm WellDepth Depth to Water Before Purerng-- Casing Volu*" ,urrf #i1:____,:Hl}) Conductrince (avg) , , PII of Water Well WaterTemp. (avg)- Redox Potentiat Ghl-tuOidity -Weather Cond.- Ext'l'Amb. Temp.(prior to sampling event)------ ' - t Time: . , Gal.Purged- Conductance Redox Potential (Eh)- Turbidity- Titne:-- ,,- - Gal. Purged----. --Conductarice Redox Potential (Eh)- Turbidity pH Temperature- Time:-Gal. Purged- Conductance Time: ; Gal. Purged- Conductance pH Temperahrte- RedoxPotential (Eh)- L*;; > T, BL,,-K RedoxPotential (Eh) Mill - Groundwater Discharge Permit Groundunter Monitoring Quality Assurance Plan (QAP) Turbidity. Date: ll.ll.M Revision: I Page4l of4l Turbidity Volume of Water Purged When Field Parameters areMeasured_ Pumping Rate Calculation Flow Rate (Q), in gpm.Time to evacuate two casing volumes (2V) 5/60 =T= 2VlQ = Number of casing volumes evacuated (if other than two If well evacuated io drymess, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labs lYneof Samde $qmole Taken (clmle), Ssin6le Votume finffcatelf olher nftered (cinclel h,esersstive Added (dTcto) VOCs d)N 3x40ml Y6D5 HCX, (Yz N Nutrients 7^N lOOml Y(P Hz$Or (b N Ileaw tVfietalg N 250ftI U)N ffi;-------ffiAll Other Non- Radioloeics gN 25Oml ff/' N NoPreservative Added GrossAlphs AN 1.m0 ml fr)N HrSO, @ N Other (specify)UN Samplevolume Y(y If apreservative is use{ SpecifyType and Quantity of heservative: I T I I I I I I I I I I t t I I T I t T I Mill - Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) Description of Sampling Date: 2.25 -07 Revision: 2 Page40 of47 ATTACHMENT 1 WHITE MESA URANIT'M MILL Locarion (wetrname) ML,J f 3 irffi'il, irrt^t CLek Oao;* * {* /-L Date and Time forPurging )tl')O'Of *d Sampling (if differenO Well Purging Equip Used: 6rr*Oor -bailer Well Pump (if other than Bennet)- Sampling en*t Aa^.--/o-^4 Prev.Well Sampledin SamplingEvent pH Buffer4.0 ?.o Specific Corau"t^r"lf , {rilufrlosl"^ Welt Depth Depth to WaterBefore Purgmg- Conductrince (avg)- lVell Water Temp. (avg)- weather cond.- Extt Amb. Terrp.(prior to sampling ev ent\ tLZ''-- Casing Volume (V) 4" Well: (.653h) 3" Well: (.361h) pII o,f ,Water (avg)- RedoxPotentfuiFh) tu6idity- t\ ".' Time: . . . Gal.Purged- Conductance- Time: Gal. Pureed- -Conductatice Temperature RedoxPotential @h)-Redox Potential (Eh)- Turbidity ?.() Time:-Gal. Purged- Conductance RedoxPotential (Ett). Time: ; Gal. Purged- L-onrftrcfence Temperature RedoxPotential (Eh) pH Temperahrre- L';t*'fr, aiv,CMrN MilI - &ormdwater Disctarge Permit Groundwater Monitoring Quality Assurance Plan (QAP)Page4l of4l Turbidity Turbidity Volume of lVater Purged When Field Parameters are Measured_ Pumuine Rate Calculation FlowRate(Q), inelpm.Time to evacuate two castng volumes (2V) T = 2VlQ= Date: 11.17 -06 Revision: I Number of caslng volumes evacuated (if other than two) If well evacuated to drymess, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Iabs. Tvneof Samnle Sqmole Taken (cirde) SriiFiileVolume findicatelf ofter Eittered (cincle) Preservative Added "ry VOCs &N 3x40ml Y(II)HCI, ftI N Nutsients g/N lO0ml YGD IIz*lO+ /:V N I*iawMetals dlN 250mI WN HNG lTD NAII Other Non- Radioloeics VN 250mI 4'N Noheservatine Added GrossAloha XN 1.000 ml U/N HaSOr Of N Other (speciff) /orrr*l mo*no gN .-5 { & B a preserv"ative is used, SpeciffTypeand @antity of Prreservative: -qt '.. -l t I I II t:: il il I I I I I I I t T T I I T T T I I Mill - Groundwater Discbarge Pennit Groundwater Monitoring Quality Assurance Plan (QAP) Description of Sampling Date: 2.25.W Eevision: 2 Page4Qof 4lt ATTACHMENT 1 WIIITE MESA URANIT'M MILL (Y!w ltt m.'il. in*iutr P,fu P*herLocation (well niame)-.! Date andTime torparsrrrg ll'?t'07 and Sampling (if different) Wrff frrginsF4uipUsed: n(u*por-bailer WellPump(if other than}lenne0-0cd[;^t/ €gl Specific conductance-7 Z-uItEIoS/cm Sampliigrven$k**hl k,ta"*r{,*,ff,. frev. Well Sampled in sampling EventtNt{- pHBufferT.Q 7"il pH Buffer4.O.A, r) w.tto"pn , lZt ] Casing Volume (V) 4" Wett: lt,$ZA? (.653h) 3" Well:_(.367h) pHof Water(uu$ .<{ . S? Depth to Water Before pursrne-l-U.2/ L- Well WaterTe ^p.(uuil-J3-a-L. Redox Potential (Ettllrrrbidity -"S Weather Con O.Br&tt, lOtl t Ext't Amb. Temp.(prior to sampling .u"rq-d!-, Time:0?30 Gal.T ime:E-84-Gal. Purged--ZS,ll8- nH €.\4 ,.tpH b'ffi Temperature 13.36 Temperature r3.3) RedoxPotential@hl 44{ RedoxPotential fen>--!!} Turbidity " rll Turbidity ,EL Time: &38 Gal.Pwged 14 . ) 7 Time: rl??f cat.pwged,-16 -tZ-- crndu"tan"" 3t7-0 cnnrtrrcrance 3 g Z7 on s.63 ,r****",i'ilT"*poutu." 11.3 D RedoxPotential eED q qb Redox potentiat@D 3 ! 3 t 0fzt & - SEZo ..5. f5 t2.7tr tu7 T PL,TwaL 1,.0tr I ';t- t, I I I t I I I I t I I I t t I I I I I Mill - Groundwater Discharge Pennit Groundwater Monitoring Quality Assurance Plan (QAP) Dats: 2.25.07 Revision: 2 Page40of 4l ATTACHMENT 1 WHITE MF"SA T]RAMT]M MILL FIELD DAT Description of Sampling Event: Location (wettname) ltN 3L i##rinitials DateandTimeforPurging U' L8'07 arrtdSampling(if Weather Cond Ext'l-Amb. Temp.(pnor to sampling event)-f *- Specific Conductance-AZ-ulvffIos/cm Depth to WaterBefore P*Srng-17, J1-- Conductance (rn1') SfSLl welr waterrem p.(u"$ lL33--Redox Porenrial <BafiLtr*iaity 75S croa*tuon 343L enndr"t^i".31{8 , ,: ps y-En ,, 5.58 , tr^pr^t* l?.4V t,np"** | 2# RedoxPotentirt Ch) 60 L- Ttfridfty 7 ,gS Redox Potential (Eh)-3J1- Time: 12 40 cat. purgeal3-t- Time: B# Gal. Purged .?f,. d ,3Sr 47. ***** l3-0? RedoxPotential $.h', Ll A6- :* - q'zl-- Well PurgingEquip Use* lcpump or-bailer Well Pump (if otherthan B"*e|-NiuL^t / SamplingEven, il4o*+t4 /nO *rt , l, Prev. Well Sampled in SamplingEvent-.t&i4riL-.1 fl pHBuffer7.o a -O pHBuffer4 \MellDepth, llZ-f Casing Volume (V) 4' Wetl: EzZ-(.653h) Turbidity. s.7y t3. lL ::ry,,,ffi {.' ll, y c*au"t*n % E16t 5$3 pn S't{Z ,r 5'?( RedoxPotential fenl,-28$- 'Ti,sb tss ,ff L--,; I I I I I I I t I I I I T I I t T I I Mill - Groundwater Discharge Penait Groundwater Monitoring Quality Assurance Plan (QAP) Description of Sampling Event: arraeEMEllIlL WHITE MESA URAMTIM MILL Date: 2.25.O7 Revision: 2 Page 40 of41 WATER Locarion (wettnane) NN ZL iffi:Yr. initiats \ya,,t lal,qtrr (. 1 [.tt {. Date and Time forPurging / l' Z ?'O7 and Sampling (if different)- Well Purging Equip Used: l-pump or -bailer Well Pump (if other than neno"$ Wtl (^.,;',*,^a sampling e"*t'(Wn*Ll hglu"/$.fr Prev. well sampled in samptingEventlfu&-fr, pHBuffer7.0 7.0 pHBuffer4.o I 0 Specific Conductance-4. L-uIffIOS/cm Wett O"pttr , / Z I .33 , Depth to Water Before Purgin Casing Volume (V) 4'Well: (.653h) conductance <nnel 3\U pHof water Well Water Temp . (un e\--!Zt t-Y-RedoxPoten iatg;n>581r*rurr, l. L WeatherCon d. - Ext'tAmb. Temp.(priortosampling "u"nt) cona*t*"" 54111 conductaiee_9{ $,2 pr (./c I t"*p" r*" l?. 7 FTemnerature lZ- f f Redox potentiat(BD-36-)- RedoxPotential (ED 3 E4 Time l4l1 Gal. Purged y'"r A ru*iditv ,19 ru*iaity 9.8 Time: l1?0 Gal. Purged---l^r A -.ooor"r*"" ffi B3?7 ,, (.t? r" w,,r*" vg'19 t3-15r"*p"ruw" IZ. (a3 RedoxPotential @D35-+- RedoxPotential Crndr",*"" 3 ?6 Z {*b {*ob -!-1 " I I t t I I t I I t I I I I t I I I I Well Purging Equip Used: [pump or -bailer Well Pump (if other than gerrret)Co1* sampling pvent [Yl*#4h hoon/4*.h Prev. well sampted in samplingErent- pH Buffer4.0 ?-o Specific Conductance-? Z-uh,trIOs/cm Welt Depth Mill - Groundwater Discharge Pennit Groundwater Monimring Quality Assurance Plan (QAP) Date: 2.25.M Revision: 2 Page 40 of 4l ATTACHMENT 1 WHITE MESA T]MNIT]M MILL FIELD DATA WORKSIIEET FOR GBOUI\D WATER Description of Sampling Event: Alhftruhef h aon,r/ua-h Location (w ett name) -t/tltl -:6 S Sampler Name and Date andTimeforPurging I l' Z t'6? anasampling(ifdifferent)' Depth to Water Before Purgtng- Conductance (avg)- Well WaterTemp. (avg)- Weather Cond. Casing Volume (V) 4" Well: (.653h) 3" WeIl: (367h) pH of water (avg)- Redox Potential (Eh)-Turbidity -Ext'l' Amb. Temp.(prior to sampling event)---.--j, -{''' Time: , Gal.Purged- Conductance- Time: Gal.Purged-----. --Conductalic" Temperature TemperatuIq Redox Potential (Eh)Redox Potential @h) Turbidity Time:-Gal. Purged- Conductance- Time: : Gal. Purged- Conductance Temperature Temperature Redox Potential (Eh)- Redox Potential (Eh)- ti .}^f L'.J, f rVtv Z( 6 rl ';" I I T I I I I I I T I t T I Mill - Groundwater Discharge Penmit Groundwater Monitoring Quality Assurance Plan (QAP) Description of Sampling Event: Date: 2.25.07 Revision: 2 Page40 of4l ATTACHMENT 1 WHITE MESA URAMT]M MILL Locarion (weuname) luN 14 i,ffitilu1r#r,,fi /-% Date and Time for Purg Ug I 2 -fi' I V u"d Sampling (if differenO well PurgingEquip used: /numn or-baiter well Pump (if orherrhan e"nnt)iDdLJ? Sampling Evenq pHBuffer 7.0 7- c) Specific Conductance 7 7 urflIos/cm w.tto"ptn 12 & J Depth to Water Before PwstneJlS--03_ Casing Votume (V) 4, wafl,,,r0LE!(.653h) conductance <uug g tr63 pH of water Or*, 1" E'l'? - t 1'? Well water Temp. Gve)-13 .-L-RedoxPotentiai W-%16"*idty . d( Ext'l Amb. Temp.(prior to sampling "n"nt1-{' * condr"toor" .<T?? condrr"tuir"-$3ZL pn s,73 p r".p"** /3. 0f T"*p"ruwr" l7 .7 L Redoxeotentiat(sh) Yll Redoxporentiat (ED Ll?S Turbidity,,)7 WeatherCond._[ ...i Prev. Well Sampled in SamplingEvent ft//+ Time: [blU Gal.Purged IS.JL conductance 3{6 L Time l/0 0 Gal. Pursed conducrance 37 tO <>lapH >.b/ T"*p"r",u* 15 'Z O Redox Potentiar (Eti --Ll -tz I; ,( pH S .A:/ ,- Fi ]l t t I I t I I t t t I I I I I I I Mill - Groundwater Discharge Permit Groundwater Monitoring Qualiry Assurance Plan (QAP) Date: 2.25.M Revision: 2 Page 4O of 4L ATTACHMENT 1 WHITE MESA URANIT]M MILL specific Conductance-flZ-ulvfi{os/cm Depth to Water Before Purgin conducrance r"rgl {0ut. s- W S,Z8 r"rp"*t* (3. {1 t.t1,' Redoxpor"*i"r(rh)=E Eg- RedoxPotential (Hi 3t Z Turbidity 90.0 Turbidity t(.v corar"^n 34 5 1 crnd*t*"" 3? 3 Z rr p"rrtrn 13,63 ,"rnp"o*" 13. 5 3 RedoxPotential (ED-211 - FIELD DAGA WORKSIIEET FOR GROTIND WATER Description of Sampling e*rrt l)r i ir,t+h^/ -il1fr17( he"urnft-, f.r Location (wettnamil ftw 3Z Name andinitiah PYa* /*lrucr Date and Time for Purging I 2 . t7 . O? a"aSampling (if different) , Well Purging Equip Used: Xpump or -bailer Well Pump (if other than ngr*a>h&)& Sampting eu*, hrrr,rt Prev.WellsampledinSamplingEvent-.|1(-- pHBuffer 7.0.7.0 pH Buffer4.O U. rv weu n"ptn IJZS Casing Volume (V) 4' Well:9.6W(.653h) 3" WeIl: (.367h) nHofWater(ave) S.73 Ao Weather Cond. /t t t* Ext'l Amb. Temp.(prior to sarnpling event)-----ll --:--- Well WaterTem p: (uue\-\b .3'l-Red-ox Potenttni teF)38lrurbidity %Jf conductance lILL p:n, @ 5,7/ -t"rrrprr^trn 12' 4 7 lrb.L: iriIrti I t I t I T T I I I I t I T T t I Mill - Crromdwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) Date: 2.25.A7 Revision: 2 Page4A of4l ATTACHMENT 1 WIIITE MESA T'RANITIM MILL FOR G Description of SamPling Location (well narrc)-Wlw 4 Sampler Name and i Date andTime forPurging 12' t"-6? *d Sampling (if different) Well Purging Equip Used: 1$ump or -tailer Well Pump (if other than Bennet) SamplingEven, h, , I * hev.IVell Sampled in SamplingEven tlUN 3.2 pHBuffer 7.a '7 ,0 pHBuffer4.O LI,D Specific unuctancelLLr*mtosrcm W.tto"ptt . l Z ( . 3 ? WeatherCond. Depth to Water Before Purgrng-I}- Casing Volume (v) 4' weil: il , 21[? (.653h) 3" lVell: (.367h) Conductance- (avg) WellWaterTemp.(avg)- RedpxPotential(Eh)-Turbidity Ext'l Amb. Temp.(priortosampling "n"nq-Z t -.--- (, Conductarice ou [.3L p r. wru* l?.31 . Redox Potential (ED-3 ? Z Turbidity..7r Turbidity Temoerature Redox Potential (Eh)- Time:-Gal. Purged Conductance Temnerahre Time: Gal. Pureed Conductance pH . Temperature - RedoxPotential (Eh) .[;Redox Potential (Ett)- I t I T I I t I I I I I I I I I I I I Mill - Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) FIELD DA Date: 2.25.07 Revision: 2 Page40 of4l ATTACHMENT 1 WHITE MESA URANIT'M MILL Description "tr$ Location (well name) in SamplingEvent_ V.opHBufferT.Q| +- tJ pHBuffer4.Q-Io Date and Time forPurging l7 . lk .67 ,nd Sampling (if different)- Well PurgingEquip Used: *-pump or-bailer Well Pump (if otherthan e"*tl kL+, SamplingEven , hr1, ,1, . -' prev. Well Sampled Specific Conductanen-l(. L u\&IOStcm Well Depth Depth to water Before Purgrng- casing volume (v) 4" well: (.653h) 3" Well:_(.367h) Conductance (avg) - pH of Water (avg) Well WaterTemp. (avg)- RedoxPotential (Eh) Turbidity WeatherCond.Ext'l Amb. Temp.(prior to sampling event)______::_ i.t ..i Time:-Gal. Purged_ Conductance- Time:- Gal. Purged-__ _ Conductariee , Redox Potential (Eh) Temperaturc Redox Potential (Eh)_ TurbidiwTurbidity. Temnerature Temperature RedoxPotential (Eh)_ Time:_Gal. Purged ' - Conductance- Time: Gal. Pursed Conductance Redox Potential (Eh)- )^O K**u ( tww ZL I I I t , , /.-,iqffi_l6+ev; ENERGYLABORAfiORIES,INC..2S9SSa/tCreekHrghway(8260/) " PO.9ox3258. Caspe; WY82602:!trWii|f'Y WFrce888.235.05/5 , 307.235.05/5 . Fax307.234./639 . caspe@energ4ab.mm . w,weneryy/ab.comtgE@tmw LABORATORYANA Denison Mines (USA)corp / November Groundwater /c07111275-oo1 vMW 14 LYTICAL REPORT Glient: Project: Lab lD: Client Sample lD: Revised Date: Report Date: Collection Date: DateReceived: Matrix: 02t22t08 01to2t08 11128107 09:26 tt3at07 Groundwater Result Units Qualafiers RL MCUACL Method Analysis Date / By 10 0.30 2380 ug/L 61 .6 ug/L I I I I I I t METALS. DISSOLVED Manganese Uranium E200.8 E200.8 12lO3lO7 16:01 / sml 12103107 16:01 / sml T T T t I I I I Report RL - Analyte reporting limit Definitions: eCL - eualig control limit. MCL - Maximum contaminant level. ND - Not detected at the reporting limit. CO7111275 R1 Page 1 of4 I I ..r:' ryt:tr. E _ENERGY LABORATORIES, tNC " 2393 Sa/t Cnek Highway (8260/) . PO. &ox 3258 " Caspe5 WY s2602s {f.ffiA effi 7?il/fiee888.235.05/5 , 307.235.05/5 . Fax307.234./639 . casp@energ14ab.mm . u,tuuenergy/ab.mmEEEWEV LABORA REPORT I Client: Denison Mines (USA) CorpI Project: November Groundwater Lab lD: C07111275-002 I client Sample ID: MW 26t TORY ANALYTICAL / / Revised Date: 42122108 Report Date: O1lQ2l08 Collection Dale:. 11128107 14:3A DateReceived: 11 130107 Matrix: Groundwater I MCU Result Units Qualifiers RL QcL Method Analysis Date / By METALS - DISSOLVED I u,*flr* T I I I I I I 150 ug/L 42.0 ug/L 10 E200.8 12lO3lO7 16:09lsml0.30 E200.8 12lO3lO7 16:09 / sml I I T T I I T Report RL - Analyte reporting limit Definitions: eCL - euality control limit. MCL - Maximum contaminant level. ND - Not detected at the reporting limit. C07111275 Rl Page 2 of 4 T I ffi!EEE@ EilEEAyLAEOfrAfAfiEq_ttE '_sJsr.ftrt qqdf Hfignway($ffitJ,EO. turiffiE . tasfrt WyiEFEW Free 8t8,ffi.45$, il7tt5.0515 . ftr frlltH,tsg . carpa.@ana4fa,t mm . ww,eircryyBhwn t I I LABOEATORY AI1IAIYTICTL REFO RT Gll+nt: Prolcat Lab lD: ClhntSamFIE IDt lDrnlron Uhc+ {UEA} Corp t,lo,rembar Grgundwai6f corl 1 1 lIE-002 MW lE Eopott Dale: 01fl2/DE Oollcctlort Oaftl Il/Jgfi7 14:40 DilsR+cclwdr t l/-+0rET Hatrlx: Gloundrrrater Anrlytrc Result Unlt*Qualtllcrt RL HCUotrL m6th0d Jlnrl]|Els DrfB I Ey D I I I I t I I I I I METTL$. EIS$OLVED ManEuncse VOLATILE OOTGAIUE CO IilPOUHD$ Areione Benaeng Caftrr tclratfilorlds ChhnDform Chhrpmothane MsthF dhyr IoHnB H€ihyl€r€ shloilds l{sF'rlhel.rrre TEIr*ryi}ofu.on Tol'xne XtlcrtoB. Tol8l Bm; 1,2-Dlol"lcIabEl:d'.8{4 $ur: olbnonoflmfirmHfrhs Surr: F-BronoiuorobErdnH S'Jrr:Tdlsh+d$ 1150 rrgtL l-Jl '4rLNJ r.,E/LND Ug/L 1400 ug/LHD t5lLHE ugll1E Ug,rLItD ut'rtND upulHD udlHD Ull/L96.{ riEREC r1s l6REc96,0 trBEClct t4REc t0 20 1,0 't,0 EO 1,0 zfl 1,f, t,0 10 i.0 1.0 8il,tt0 ?s130 80.120 80.t20 Ee00,8 UIUI{716:08I sml SYirE26flE {1fi507 15:38/ jh sw6t6cB tl/utm7 fi:36 /Jh SIYAEEDB lt'!01tt 1S:16 t jlr 5Vr82638 t?'fotel 17:35 lllr SVfESSB IA,U&t71i:lElllrSW5163B l2i01OI 15:36 / llr6r/,ltce0E felfl3,itl7 1f:.X6 /ltr SWflft6,fi8 th[i,tt] 1S:SB l]h SWa*e0B lerE&tr 16:$6 I irrEWa2&lB t2fith? 15:S$ /Ilr SW€XAJB t3'BilUIlS:38/llr $wflaEffi l2JEi,trt5:38Ilh Elryf,AEoB 1zrotrur15i3E/Ih $WflA60B 1Zr!0iltl 1i:38 tllrSW&alB 12AtrOI 1S:16 lllr EEport EEllnllloflr:I t I RL. Analytn rE0ortlng llmlt OoL - Qualtty otrttrnl Imit. D ' FIL hotep+eC dus ta BFtr.dT tnstrfr lnterf+rence : I'iCL. lrtaximum oontamhant lcr€, NO - Hot deledsd El thE r€pqfhg llmit. TRHCIT# C07lIrA75 I I ffi@@w EnEf,elLAEOfrAIIIFTEEiltE ..ffs,Snf C;rgitl,tig#'/.dyfiffiil.EO.tuxlllfl . Casryt,WY82i02 fut+ftgieEt4if$.*5in,$1fr505r5.ft{J0IFt4,lffi,rgqafreneryylalddr?.tt40fiarl4$}r'Ed.trE t I I LAEORATtrRY AHALYTI CAt RE PORT f liurt: Prulech Lab tD: Cllent Sample lD: Denison lllnoe {USA) Corp Novenrber G..ou nd'rrrater c071 t,1175.003 tiw 3,2 Faport Eele: 01/t2ltl$ Collectlon Data: 1l#fiI07 14:00 DateEPatlved; 1 lI30,U7 Itlelrlx: Cttundrater RBarlt Unlti Euallflrrr RL HCU QCt- lllethod lnllysls Dnte I Ey 0.s3 3g IE 2i 1Al ugrl 746X u6iLsl$x uSiLS? ugit I I I t I t I I I I I IIIETTLs. EISSOLVEE Cadm unt lrm ManEtn€tE Nlc'<el Et0c.B E20tr.7 E20t-E E200.8 lftlo3,tlt 16:15 / Eml 1l/tEi0l l8:E6Ico 11lb3,l07 16:16 J sml l?,BStI 16:'lG J eml T T ne$'fit EL - A,nalytE Frpodrg llmlt Ddlnltlonrl OCL.Ous1tryo'r.rd rmp l/CL - Maxtilum coilefilirent le,v'€|, m. Uot decotrd nt tfie mporllrq linlt -4- TEICK# C0?111275 T I t I I LABORATORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp November Groundwater co7111275-004 MW 65 Revised Date: Report Date: Collection Date: DateReceived: Matrix: 02t22t08 01102t08 1112810714:30 11130107 Groundwater I Analyses Result Units Qualifiers RL MCUQCL Method Analysis Date / By ug/L ug/LI I I I I I I t I T I I METALS. DISSOLVED Manganese Uranium VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Mdhyl ethyl ketone Mdhylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surr: 1,2-Dichlorobenzen+d4 Surr: Dibromof luoromethane Surr: p-Bromofluorobenzene Surr: Toluened8 846 39.0 10 0.30 20 1.0 1.0 50 1.0 20 1.0 1.0 10 1.0 1.0 8G.120 7&,130 80-120 80-120 ND ug/L ND ug/L ND ug/L 1400 ug/L ND ug/L ND ug/L 14 ug/L ND ug/LND ug/L ND ug/L ND ug/L 101 %REC 103 %REC 97.0 %REC 98.0 %REC E200.8 E200.8 SW82608 SW82608 SW82609 SW82608 SW8260B sw82608 SW82608 sw82608 sw82608 SW82608 SW82608 SW82608 SW82608 SW82608 SW82608 12103107 16:24 / sml 1A$lO7 '16'.24 lsml 12103107 16:15 /jlr 12J03107 16:15 /jlr 'l2l03lo7 16:15 / jlr 12103107 18:17 lji 12103107 16:15 / jlr 12103107 16:15 / jlr 1A$107 16:15/jlr 12103107 16:15 / jlr 12103107 16:15 ljtr 12103107 16:15 / jlr 12103107 16:15 / jlr 'l2l0slo7 16:15 /jlr 't2l03lo7 16:15 / jlr 12103107 16:15 / jlr 12103107 16:15 ljtr Report Definitions: RL - Analyte reporting limit. QCL - Quality cmtrol limit. D - RL increased due to sample matrix interference MCL - Maximum contaminant level. ND - Not detected at the reporting limit. t I t I EnEfrEEtnaog,,IufrrEfl fiUE 'r,sg,fff fiwf tu'Elhryrrffifl-F.Otur#5t , CElFat, W5ffi2 ToiffietfifiElffflfl' . r07.fr5ffil5 , Far307,E34.tit9' ea4pr@mep,phf.comr.ruaranrry,fahmm t t I Cllenl: Prolect: t:b lD: Cllent SarrFle lDr LAEO RATORY Afi ALYTIEAL REPO ET / Eenlson l+ther{U.SA} Corp / Irlo,rember Grsund'rvelsr , /o07111r75.00n v Tdp Ehnh EaEonEilcr 0l/IIzrUg Eoll+ctloh triltE: 1ln8€r t4:30 DatgFlr+lvrd: 11/30O7 JrIatrlx: Grrrrrndwater Analylor REEUIT Un|tr Quallfnrr RL lIICUACL Hethod Analyrlr D*t+ I EyI t I I I I I I t I t UOUTTI LE TIEGII'IIG COilIPOUHTIS J\E+l4ne Eeorena C€rtqn tstrBitlorld+ Chlnm{om Chlsrf,ft*tltns Itllalhyl e,lhy. hotore Melhylene chlorlds Hrptrtralene Tet'BhydrofurEn TofueEe Xylenes. Total Sunl 1J-OichlcrDUslz.rlD{4 Suri: D bronroirrorsHletlatru S url D-Brprroil.r+robgrra€nc Bunl To:uBfid.d8 ND USILNE UEtr NU UgtrH0 uElLND u6,LNE ulllND uA/L ND uxlLND u3IL fi'tr ug,l"l,lD USJL cs,o v,HEc1Vt vrREC 101 16REC SE.O JEREC 2[ 1.0 t.o .t.0 t,0 2C 1.0 1.0 ID 1-O 1-0 E0- I ro 70.180 8{-t20 80..t2{r S|VEaEEL tlr$,l0? T4t6# /Jilr SIVB?EoB lz,tx0? 1a:SE / lksrrsffiDB l?,sx0l1tl:59/lk SftrB20OE l2'trxbll4:SfiJltr slTEe60B t2,r]107 14:58 ' ItrStAr6260s 1rfi5107 14:54 /llrsw0I60B 1lJol,t7 t4:58 Jltf SIII0ZEE 1E{Eij0I14:58tllr s1il8260$ {:/81,07 14:38I llrEw828E le&&'[7t4;50/itr SW8260E l2lEg,UI 14:56 /l1r BWge6,0B lZAl]iUT t4:58 /It/ SW*2E0B lliE.t'u7 l4:58 Ilhswfi2608 t!E3,uI 14;58I ltrSW0,aGOE rrlE3flI f4:58 y'flr I t Erport RL.Ansl$trr€EorllrUlimlt Dsflnl0m=; eCL - iluallty66rttrq I mlr, lflcL . !,radmum mntrflt'ftrnt Jovd. Ho. tlotdetsclEd Ellhs repsring lhll. -6- TRTCK+ CC7I11275 I I I I I I ffi fiFE{,iHEilW##;,f trH?frr!ffiryffis:,;#fi,#r,ffi ;fH#ffi ffi* AAISG Summary Report Ellant Denlson Mhoe (USA) Corp Fr+lec* Nov6:rter Cmundumter Eoport Dah: OldJz{)B Worlr Otdar: CU71l1E75 E ReruJt Uhlt* llt ttEEE lon llrnlt High ltlttlr EFII EPDLIm|T truat i I ilgthsdi EZU0'7 Eatrfi: R9d{e2 $anrplr lo: lFE.thl LEho'ahry ForElndBlank Runi |EP2-E_0I1Z1EA 12j12/07 12:OElron t,ss fiE/L o.iBo 9t 85 tls f,anph lf: C0t1l11e0{0SCl,lS $ample Ltlahix Spi}.e Euru ICPt D_07l2ltA lA'?.117 17:00lrqn 0.sil2 tflslL 0.0ut) ${ 70 130 Srrnph lE: Col'ltllf,o{orcilSE Surrrpls lulalrix,Ephe truflicalru Rurr; lCPl.C_C?lElEA ttil?Jl7 17:OXlrsn 0,€f,0 mEIL 0-lKi0 St ?0 t30 2,1 2C. HEthod; EIID.E BiltEh: R93666 Run: ICPHSI-E_0?'1203A tt.,[51D7 19:46 I t I I EamplelD: LEB I nlilngsnscs Nl*.El f Ermph lor Lr.E I crdmtum Mrtgrnese Nlc8sl ,l1elhod Hrr* Htr thst o.0lIL"J HD mgIL 3E{5 d.floffi ,0tL tE{E Lf, berfl lor/ Fcflff ad Elsrk Fffln: l6PllSl-C_071201A 12E3iU7 1l:€4 0.84H lr:St 0.0010 clt t5. 115 0-0499 m$t 0,0m0 I00 E[ l1S 0.0510 {nSL S,00lo l0I 85 lts ftrn: lGPlll8l-G 071!ntA l2/03/o7 'l?i00 0,flSEG r,gtt 0,010 101 70 lefflvlrrgancso 0.057t mst 0.u10 107 ?0 130I Ntc*,et o.E$tl msrL o.ffio rs ?o 1so I Etmnh lllr coflZ00t+EoaEilEq4 F6t qHBEl.rEn sllts Dupt EalE Eunr ICFHEl-C-0?12fi44 firt1r07 1?:S9 0.050G rttgil- 0.010 t0l ?0 t30 0-4 20 0.05'm mdL 0.tll0 100 70 130 s.4 lD 0,s418 nEa o.tEo 84 70 130 0.0 t0 I ssmns lo, c0flrffi1&oollElrls{ Pwt D$esllor spllcICadmlum 0.fl5t16 rr,n{ CsdmlumI Lil:l"*' t T I t I Oudifl+rs: RL - Anelyle lepor [rtg llmlt.NE . Not detcdad rt lh€ repoflng lldl. -?- TEAC!(# C07111375 I T I ffi@@r EtlEfrEf LtB0frAfCIftIfl$/ LlIf. . 4trr,5#,1 *epk Hghway (8Pt0U , EO, tux fli9 ' fs4rsfi WAEiFtra#Frrllfrtfl?li.Wn . mr.fiSffi$ , Fil( ffiLfit ffiie aaflr,,r+r,rs.efls'ifHf.f,wrr I t QA/{lc Surnmary Report Gll+trt Uonlmn filines (USA]trorp ProJrrtl Ns'rsrnber Gtoundwaier Eepon D6t+! olrEznlE Work Ordrn C07l112IE I t I I I I T I I I T I lrlgrhod: gwEIA0B $*mpls ID:'l2050rlcE_: .4cglarre 0ctrctu Carbon lstiacldordd Chioroforrrt Cltlolotre{hane mrF-xilenca Llethll stftyl ketong Hathllem rJrtorlde tuo0hfinlGDq ofiylsne Tefahyrlrsfurarr Tolrrens ,g,tsrio6. TEEI Sun: 1,l.Elcf,Embenzened4 Sur. I Orlrrotnol.rcmtnsl,tune Surr: rEilx+fl uorsbonfr n c $urr: TuluenadB EmrFla lDi ll0i0I_hELK_s AoElotrs EsrzEae gsr!ffi t€trfiohlorldE Cirloroform Chlonnrclha-.o nr{F.)slenes tUlgtrll etryt helpne Httrllfirc cfilcddd NsChlhEIsn+ o-Xyhoe TctlehlEmfulen Toluor+ lujeflrE, Talel Gurr I-t Elnhhmbenmne{4 Eulfi EfrEmsllusf 0mEila! lE Sum Ftnrmo,firomGsE€nr Sun:Toltrrrtg{8 ErmFtl IDi Gq?rr,lrrl-o0tsirE Emzsrs Carbon bttchhrldo LEharotorf oont'ol $em plr56 u{ul,5-2 u#LE-4 riS/L 5,2 uE/L 5.5 ug.L 1l uElL t.5 uglL. {s ugfl.4.S udl 6.1 udl 50 uilL +,4 ug+L 1E ug{L . Mnihod Ehd( t{0 ug,iL Dll'l ug,iL HD 'iSLND ]flL MD UEL ND ,qg'l- ll0 .rr#L llD '€lLlE 'ISJLND urvL ND UE,L ND U6,L ND ugL Bsault Unltr 6arElf, MFtixSFlko i1E0 USIL 1100 uslL ID 110'l,o 1081,0 ioE{.0 10$1,0 r101.{r t0620 t15 1,0 s8 ?o1,0 grr r0,r,0 103 ?o10 eB ?0ll) i07 rrl1.0 'rxi mr.0 lus E0t-o 'lld ttr,l_c cft ti Run: SA?URl,rlGA_071 ztr34 70 t30 ?0 13{70 t30?0 t30 7E T3O 70 13070 130 RL t(EEe Lor,r Llmlt Htgh Ltmtt RPo EPDUmlt Qurl 'l.c 101 8X 120 - Ons rnCilE k Eul#s ol HCF,lArOtr.nga, Thc lEnplr msatr tha .rrn6lrdEr otlhr GAErtltdr,lhrEhrB l1ts EsEh h eFptErtC t30 130 130 13n 1A0 1SE 1?t 13C I r4t Run : 8ATUft lilcA_dIl ?034 120 1 l{l 140 r20 Rr rn: SATURNCIT_o71 20OAtE 'r t07t 133 Ealch: R$6730 12t3OT 10:42 12/tr+rEl 12:37 llEiior a0:t I 0.5 0.5 0.5 o.E o.$ 0-5 tl,6 0.5 0.5 O,E n 0-s 0.E 100 B0'111 r0s4 80lEo m 50 tli8 50 1lt T I T Qurllllcrc; EL . Anrlrte rcpEr{no llfilt.lD - I'ltt deh+hil ill tlr6 rEporttrE {tmtt. -B-TRicl(+ c0?i11175 rEilEfiffi]iliE@ E tEfrE rtISf,E,4 IOEIfq flr0,' EJ4? Sdf treer rtghway {Pffi il, PO. Eor SlSi . 6d,in# W Wfd[Ft9ilfififr.I1',frfE,Aff!J5.05l5,FaxJlE.?Jdlffit.caqper@erxprg/rEA*m,wu*xwtyfiat,mn QA/QC Sumrnary Report Ellenl: DoniEDn ft'lines (ltSA] Corp Frolocu NovHmbdr Grou ndYrdt€r Feport Date: 01,II2J08 WcrkordcE C07111u75 IErlyti EOiUII UfiI]E RL TTftEG LtrV' LIMII TISh UMII RPD EFDL]MII trUAI Hrttrod: glfl[IE0E Slmplr tD: C0IlllfI6,0EEBuf 5ampl6 tr4sy,* $r'n"Chlrrrlorm t600 {rgJLrlr+p-Xllenes 2CnO udL t-xylrrrg 1m0 ugrlTolusns 1m0 uc.L XtlGrlc6, TolEt 3m0 ug{ suri l.2.[IlEhfoft,t#trcnG-d{ 5urfl OlbfurEfl uo!am€fi4ft6 Sun: p*rumollmrohmzans $uni Ttlufio.da Run: S/lTURttCfi_[? I e0#rsfl 1!, 7t 13150 sfl 70 lso50 101 r0 rso50 10,1 I0 1*050 rls m 1301.0 108 00 1201.0 tui, IU lJUr.0 ts 80 1t01,0 103 80 rto Run: EATUEHCA_ffJ I 2tI3A50 gE 70 130 s.550 't05 I0 t30 r.050 s0 70 t30 11Et st z[ t:ro 8,0E0 Cl i0 t30 10i0 9s ?0 fi0 E.s5d Sf 7D t30 tt1,0 0B s0 ,tzo 0.0i,0 sB I0 tso 0.81,0 0s 80 120 0.01,0 100 80 120 u_o . HEK r{rgEnt*lr 0'r.r lc€ctsJno$1lrut+ slncE lhg LE$ tnd fia EPodtre hls/HEp FrFls Dcl{pHh{, n) t+llsti+tr lE rEsEssil/ Bamplo lE: EoflllZf!{loIEll$D SanlFls hlaku Sptlrl Duplicale Batch: RE3r3o 14ru3/D7 20:11 lZtngIOI 20:49 10 EU e0 t0 20 20 20 to Itr t0 t0 Bgrrcne CtrEon tc,tmdrlortde ClilsglErrx m+9-Xylenes 0-trylcns Toluenq I{yfgnss, Tntel guf r: l,?+;chlorotolEch6.d4 Surr: Ctmmot'lu,rum chans Surt: pBroncf rlorEb+ntEno $u,r: TolucncdE gEO lgll 10X0 UCL 2300 USL 18fl0 ugils'ro ugiL 580 ugiL 27IJE {rg/t loofFlilEllru$, Tr|oarln:plEI,lcslrlhc$rntlfi{drEltoO c:Ii.c,llrerEbryt}i5gltehtrapprorr+{t. Quil[flenr: FL - AJElIte iqportlflg l|mlt,h D - [J{t Cetoctad al tte reporfrrg lmrt -9-TFiltr# C07111275 T I ffi@E EilqH6fl.i{g0ll/1ruF/Et tiYC .-.Pl4lSatq,!4irt$n*y/d6$f,I/.ffl.8*rJ4frf ' f,effi Wrt26tr Erfr.EIiE df,tglI4f tS ' ,l$Ir,r5. 0516 , Fw ,9P/234, 1fl19 , ' isspfn$grrr,flrl,rEama ; m+rrJ,i+,if+*,1oorr - t;IEIBl=LEId;'ii Erd EdlE .l|E Hr# 3 E,EU_ GBtg .E.E PG-IE'-'f, u .E s;II E=fiE'H EF{; EES EE# }EEEE EEEgE= J''ri F.Eg.gl ttEgEEHE EEE gEH {=s sg El E*nEl E o*E*.i cllt}EI FI EE EIoE.,Hu# EHEd+{ts HE:EE>il s fdEE E ts EE ft.+E +-4EttE *u ir, \IE \f,'o\ $tl 'r"'fi1 iH "l /l# [u'{ lE =lEEIE EIE EErLE "gEEEEo;1€UIE #.8EL EElIr0loao-AEgHr!tEs IEfllE EI+lrt El= fiHErfitrtr trtr Ell = rFJ*itrtrtrtrtr r'lN trfiEt+Eho-# I 0 Ig .d0- TILoo{ltr rl{gto ETlu IE E .g-Fr -rBtrr{ttrtE L,()*tr E f! ff G) T T I T T I t T I I I I I I T T Jut{4- z. .tHi. Ec T I I I EIIfflOf IdEOf,,{ fOEilEB rrtG . fiffi JEf Creeir tlhhway (&tittJ . EO, tu iflti , frsa:x tvy sfrtr. Tadftcrfiffi'ffi,ffiIi ' il71fi.0515 . Far frr,ei4jnH ' lasper6*ug),Ffrnrrn.nr*uaringffi.caz I T I I I t I t I I I t I I I T Energy Lahoratories lnc Workorder Receipt Ghecklist lffiDenison Mines (USA) Corp Legi' crmpletdl h; Knrherty Huniiston Dat6 and firne Received: tlj3tjl20o7 g:30 Al,rlRevie/Ed by: ReOelVeU by: Jn Roviu'/ved Date: Canier nams Next Day Alf $hipptng containsr/sr0 +r ln Ecod cEnditicn? yor fi |rh E Hot pres+nt fJ cuEtody E+Els rntFct on ehlrEinfl Efiltolroricqerer? yes @ H= E N,rt presunt I cusl<ruy reph inlEcl Err rtrnph Eo[ta6? yer E Np E H6t ftErE't E Chlr,rof eust:rdyF-Eaent? yer g Hq E CLs'n olcUrtrdl +rgnrdg#o:r rethqulEl,EC and ro.;€ived? y** EJ yo E Cl',E n o'custo{I +gr+orui:h sornph lEhcta? yer fl 1lo E $arrp.es Ur proper 2qnlslnsrlElaf.€? ysE E Ng ESemplccontairerrintacr? yes @ No fl $Jlrci0nte€mllf ,rOlJmsforindicrtedte*t? y€r E No [f All sflnpl€e rcEst,JEd errthtn hotdrng:iE? yea E No J Corllflitler,.TE{tip BleFktsmpEruture ;n scnp ianco? yer fl Ho ] 1 ,l}C On ls! 'dv{ter - VOA v als harar rern hradspare? yeu fl Ho tr Ho UOA rristr r,ubmlttcd ! Weter - DH B.tcoptAtle rgon rEcolpt? yer [f ilo tr iJdtAf,F,llcscte = C.01tFct End Co,recllr.EArilon Cr.xnm*nts: ilone rffirrflilllffiililfftilIffiltffilil c071 1 1 275 - 11- :*** cr?1r.1275 T I EI#EEEE I;d,gOFttIEfIffi 4y6- ,rsg9$d.40,uE+ lttgtqiy{rtMil,po.Estit5E . c.f,jfldrt lyf ffii)tToliFtw0t8/f,6fl5l5 . id7.21L05ti , Fa,{ Jfitrj/.rd}p . aaqoer@ersgrdaf,qrn,wr1/t|.e+-+isllab.na T Dah: 0l.Ja,t08 I t I t I I I t I I t t T T T t CLIEHT: Frolem: Deni++n lrlirres 1954, *u* i'lovEmbur Groundwahr Samplt Ecllv*ryGroupr C0?1{l2TE CASE hIARRATIVE THIS IS TI.IE FIHAI. PAGE OF THE LABORATORY AI'IALYTICAL REFOET O RIGINAL S,\t,IPLE $UEMITTAL( S) All orfuinul sample zubr1ffie haue ha+n rBtumtd with lho data pacltagc. A copy of tha u bmlttat{e} har been incluoedend lraEksd h lh$ dsta Ftckagc, SAITIPLE TE hIPE RATUEE GO[,tpLtAl'lCE: 4"C {iZ'C)Tamp6rElure of semples rocelrd qay not bu cotteldered propeily presorvad by accepled Bt rnddrds, samf,oe trct ar,hand delhEted lrtrrt-ediahlv oter colieEtlqn sha!l be oonddarctl oiicptru" ii th;.u ts ilvidencd rhsiir,a "riilr'i,ii prooe*rhas begun. sotL/soLtu €AinPLE$ All $gmplgg reporttd on an af, r*Crrrrd bmi+ unhs€ sthanylee ltElcgtEd_. PCB AT,IALI43]S USING EPA 505 -og$ gtorle-d try EL! 9;ing EFA method 505 rsllscE thE ItETJIE tur €etren lndivldrol Aroclora. when lhE resutts tcr alEsvEfl ar€ NO {not dshfil€d}, lh6 csraplo meeh EPA compEcrlce crilerln for l-CAhonitcring. SUEEO}ITEA#TING ANALY5IS Suboontrdoflng of srnple efi4yes to an crilslde laborahry.n-ray bs. rsqulnrd, Il ezr, ENEftGy LAEoRAToRlEs rrlll udizelh branch hboralur{m flrqr ra;16"6 crntsact laboml+rles rqiHs lervlcei nny ruci rirboririrret niiiEilnllcarro u$rrn rhclaborabry Anatythal Fepurt, EEAHGH LAEOFATOFIT LOCNTIONS cli-b . Eneqy Letqrutoiler, lnc. - Blflrngr, flTctlg - Ercqy Lahomtorlee. tnc. - $l[Ette. t{y cll-h - E16r[ir Labrahriar, Inc- - I lal6na, MT etl.r - -Energy Laboratortee, lnc. - ReFtd City. SDeti-t. Energy l.ebonatorles, tnc. - Ooliege S-tatf,rn, fX CERTFICATION$: u$EPAr wYEo0m; FL-DoH NEt Ac: Egr641; Arizonar Az0Eg0r cEl,Ioril€:0zr |SEAOrcEtrt: WY2000011 Utah: 30723E05tS: \4rglnh: 00osr; t rEshingtJni Ci SCI -- tso 17025DISC| {!MEE: The resulEqf thla Anahfical Report relate only tn tho ftems submlttpd furanalplo. ENERGY LqBOFATORIES. lNC. -CAEPER.WYocfli+stlrat caftaln mothod setection$Gontatned ln thls renortmeetrgqulmmsnts as B6rtlilh bytho arow acqEildnq author{ttar. Eomi rsilrG mqtEr"i-uifru-citar;ffi;ffifi.coy€rsdundcr licro oettlfca0ons. A[ BnEl]rsJt dEtE to b6 Huhmtted for.r.egutatory anron[rngnt ;'lirr]d Hiltild ilfl;;;,,]ri;E'ltta of olEln. t'loaso varlry ELt'B cerilficrfion coveraga hy vtstflnfr nrnrur,Lnaryd-aL.com ELI appreclahe the oppo(unlty tc prudde yuu willr this anutytlcal eEryice, Fcr addtflongl hlorma[on afid scruiocs vidt ourneb page vrr,,r,energylub,com Tm fttal Iumbcr of paEes of lhas rcfott HIs lndlcsted Uy ttr€ FHge nurnbsr lffiflt€d in the lo111161 dght cater. -L2-EEtrcKf c071112?5 L1#4 qB;-:*.::t:._.::_i! t:::: :.:,::t:..aaaa; : UEWT Glient: Denison Mines (USA) Corp Project: November Groundwater QA/QC Summary Report Revised Date:02122108 Report Date: 01102108 Work Order: C47111275 I I I I I I I I I I I I T T I T I I T Analyte Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: E200.8 Sample lD: LRB Uranium Sample lD: LFB Uranium Sample lD: C07120016{03BMS4 Uranium SamplelD: C07120016{l03BMStX Uranium Method Blank ND mg/L Laboratory Fortified Blank 0.0505 mg/L Post Digestion Spike 0.0506 mg/L Post Digestion Spike Duplicate 0.051 1 mg/L 0.00030 0.00030 101 98 990.00030 Run: ICPMSl-C_071203A Run: ICPMSl-C_071203A 85 115 Run: ICPMS'l -C_071 203A 70 130 Run: ICPMSl-C_0712O3A 70 130 Batch: R93696 12103107 12:46 12lO3lO7'12:54 1ZA3|O7 17:09 1ZO3l07 17:39 201.0 RL - Analyte reporting limit.ND - Not detected at the reporting limit. CO7111275 R1 Page 3 of4 T I "ffi:::i';:: s,*i!i.'YA"i:w{-e-'#W ENERGY LABORAqORIES, tNC. . 2393 Sa/t Creek Hrghway (5260/) " PO. Box 3258 . Casper WY 82602 Wfiee888.2j5.05/5"307.235.05/5"Fax307.234./639"caspe@energlab.com"www.enetgytab.com Date: 22-Feb-08IDenison Mines (USA) CorP November Groundwater CASE NARRATIVEIProject: Sample DeliverY GrouP: C07111275 T I I I t I I I I t I T T I rHIS IS THE FINAL PAGE OF THE LABORATORY ANALYTICAL REPORT REVI SED/SUPPLEMENTAL REPORT The attached analytical report has been revised from a previously submitted report due to the addition of Uranium on samples MW14 and MW26 per request from Steve Landau 212212008. oRt Gr NAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. A copy of the submittal(s) has been included and tracked in the data Package. SAMPLE TEMPERATURE COMPLIANCE: 4'C (t2'C) Temperature of samples received may not be considered properly preserved by accepted standards- Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. PCB ANALYSIS USING EPA 505 Data reported by ELI using EPA method 505 reflects the results for seven individual Aroclors. When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTI NG ANALYSI S Subcontracting of sample analyses to an outside laboratory may be required. lf so, ENERGY LABORATORIES will utilize its branch laboratories or qualiiied contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical RePort. BRANCH LABORATORY LOCATI ONS eli-b - Energy Laboratories, lnc. - Billings, MT eli-g - Energy Laboratories, lnc. - Gillette, \tr/Y eli-h - Energy Laboratories, lnc. - Helena, MT eli-r - Energy Laboratories, lnc. - Rapid City, SD eli-t - Energy Laboratories, lnc. - College Station, TX CERTFICATIONS: USEPA: WY00002; FL-DOH NELAC: E87641 ; Arizona: 420699; California: 0211ACA Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, lNC. - CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certifled in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit out web page www. energylab. com. The total number of pages of this report are indicated by the page number located in the lower right corner. I C07'111275 Rl Page 4 of4 t I t I ENEROY LABORA\ORIES, lNC. - 2393 Sa/t Creek Hrghway (8260/) " PO. Box 3258 ' Caspet WY 82602 lb//FbeSSS.Zj5.05/5,307.235.05/5.Fax307.234./639.casp@ererglab.@n"wu44ler@tgy/ab.com Glient: Project: Lab lD: Client Sample lD: Denison Mines (USA) CorP December Groundwater c07121013-001 MW 14 Revised Date: Report Date: Collection Date: DateReceived: Matrix: 02t22108 0'1109/08 12119107 09:08 12t20t07 Aqueous LABORATORY ANALYTICAL REPORT Result Units Qualifiers RL MCUQCL Method Analysis Date / By E200.8 E200.8 10 0.30 2290 ug/L 60.7 ug/L I I t I I I t I I METALS - DISSOLVED Manganese Uranium 12126107 15:07/sml 12126107 15:07 / sml I T t T I T Report RL - Analyte reporting limit. Definitions: eCL - euality conhol limit. MCL - Maximum contaminant level. ND - Not detected at the reporting limit C07'12'10'13 R1 Page 1 of 4 I I I I ENERGYLABORAfiORIE_S, lNC " 2393 Sa/t Crcek Hrghway (5260J) " PO. Box 3258 , Caspe4 WyB2602lb//Free 88823505/s " *r*1!!,.y: ,* *rrl r05s . ix;spedenersiiamn " u,u4uenerwr/ao.con Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp December Groundwater c071 21 01 3-003 MW 26 Revised Date: Report Date: Collection Date: DateReceived: Matrix: 02t22t08 01t09t08 12118107 14:25 12120t07 Aqueous LABORATORY ANALYTICAL REPORT I Analyses Result Units Qualifiers RL MCU QCL Method Analysis Date / By I I I I I I I I T T I METALS. DISSOLVED Manganese Uranium VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromof luorobenzene Surr: Toluene-d8 1410 ug/L 47.6 ug/L ND ug/L ND ug/LND ug/L 140,0 ug/L ND ug/LND ug/L 22 ug/L ND ug/LND ug/LND ug/L ND ug/L 98.0 %REC108 06REC 96.0 %REC99.0 %REC 10 0.30 20 1.0 1.0 50 1.0 20 1.0 1.0 10 't.0 1.0 80-120 70-130 80-120 80-120 E200.8 E200.8 SW826OB SW826OB SW826OB sw8260B SW8260B sw8260B SW826OB sw8260B sw8260B SW826OB sw8260B SW826OB sw8260B sw8260B SW826OB 12126107 l5:15 / sml 12126107 15:15 / sml 12121107 17:38 / dkh 1212'1107 17:38 / dkh 12121107 17:38 / dkh 12t21107 18:17 ldkh 12121107 17:38 / dkh 12121107 17:38 / dkh 12121107 17:38 / dkh 1221107 17:38 I dkh '1212'llO7 17:38 / dkh 12121107 '17:38 / dkh 12,21107 17:38 / dkh 12121107 17:38 / dkh 12121107 17:38 / dkh 12121107 17:38 / dkh 1212'lll7 17:38 / dkh t T T Report RL - Analyte reporting limit. Definitions: ecl - euality control limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant level. ND - Not detected at the reporting limit. C071210'13 Rl Page 2 of 4 I I ffi/ErrffiilE@ . iattftEflflffi,afl5;ct 15 . .ffHe$f,Oftt . Fff J07flJ4.t$lf . c*apertPenerg;r+*Ucum.rfln+.ana'g/aI,.6n0, t I I.ABORATOEIY fiHAt L f,EPORT Gll+nt: ' Fmfect: Lab lD: CllenlEample lDr Denis+m lrtlnee {USAJ Corl Eegember Groundruatsr c07t2t01s.002 M[i 3? Eepod[ater 01JDg,t]8 Eollortlsn Erts; 12/18I[I 1{:fi0 trfilDl-{occlvad: 12ll0lli7 fialrl* Aqrr+ous I Re$ult unltE Qualifhrr kL ldctrod Annlysh Dnto, By fiicu clcL E?mx 81U0,7 E20c.B E200.8 0.rn 30 1,) ZJ 1.Bl rrfl,L 787E tIgl,L S0S0 usrtfi6 uErL I I I I I I I T I t I IIETALS. trlSSOLVEtr tr6dritium lrtrt iilangan€ee Nlcftel r?lllldl 04BA / G 0t$,ll{13 22:0G I cp tlllT,tr 04133 J lE {znl,Ul O1:3$ I rr FrPqt Do,llnlllCnr: ru - fulElltE rererllng ],lnlt. ECU- austtg oontd l,nrtt. MCL . Hadrhunt contrnlnsnl teTEl. NO - Hot Celeclod nt fir r€tf,rting limit,I I -4.-.vtB,rtEr# c0?1AI01r T I I I T LABORATORY ANALYTICAL REPORT Client: Proiect: Lab lD: Client Sample lD: Denison Mines (USA) Corp December Groundwater c07121013-004 MW 65 Revised Date: Report Date: Collection Date: DateReceived: Matrix: 021221o8 01/09/08 12118107 14:25 12120t07 Aqueous MCU QCL MethodIAnalysesResult Units Qualifiers RL Analysis Date / By 10 0.30I I t I I t I I T t I METALS. DISSOLVED Manganese Uranium VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Mdhyl ethyl ketone Mdhylene chloride Naphthalene TetrahFrofuran Toluene Xylenes, Total Surr: 1,2-Dichlorobenzen+d4 S urr: Dibromof luoromethane Surr: FBromof luorobenzene Surr: Toluens.d8 1450 ug/L 51.6 ug/L ND ug/L ND ug/L ND ug/L 1400 ug/L ND ug/L ND ug/L24 ug/L ND ug/L ND ug/L ND ug/L ND ug/L 1OO %REC108 %REC 1OO %REC100 %REC 20 1.0 't.0 50 1.0 20 1.0 1.0 10 1.0 1.0 80-120 70-130 80-120 80-120 E200.8 E200.8 SW82608 SW82608 SW82608 SW82608 SW82608 SW8260B SW82608 SW82608 sw82608 SW82608 SW8260B sw82608 SW82608 SW82608 SW8260B 12126107 15:22 lsml 12126107 15t22 lsrr'l '12121107 18:58 / dkh 12121107 18:58 / dkh 1212'lll7 18:58 / dkh '12J21107 19:40 / dkh 12121107 18:58 / dkh 1212'1107 18:58 / dkh 'l2l21lO7 '18:58 / dkh 12121107 '18:58 / dkh 1212'1107 18:58 / dkh 'l2l21l1l 18:58 / dkh 12121107 18:58 / dkh 1212'llo7 18:58 / dkh 12121107 18:58 / dkh 1A21lO7 18:58 / dkh 1212'1197 18:58 / dkh I I I Report RL - Analyte reporting limit. Definitions: eCL - euality control limit. D - RL increased due to sample matrix interference MCL - Maximum contaminant level. ND - Not detected at the reporting limit. EllEfrolLAEofr'lIHFrEsr_4tlE trqqqqry.rHgh*ayl4tffitJ 'Ffl &rsefd . frqmr wyht60xlolfrzcffi.tffi.lilf , iflZ.AyfAili . FEX fr14$C.1659 ,'citsrydmergyhncon . nulr+eie,.gria&,car IJIEORATUEY AHAIYTI CAL REPO RT cllffit: PnilE+fl . Leb lD; Client Srmple ltr; Dcnlson Mino€ (ttSAI Bory D€cefi hcr Oroundtrvqlcr [0r1?1 013-00s Trip Blank Repofi EiltEr 0lfll$/tl8 Sollocllqn Este: 12i18/07 l4;28 DeEEoc*lved; 1tl20,t? l.iatrlx Aqtleo:re Aneljr.r Rrsull tJrtlh 4lurliflers nL HGUOCL HEthod Analy:sls trf,?s/ By UOLf,tLE ORGf, H lC CO t'rtFOUl{OS 14cefone E+EErle Certon letgohlorlde Chlorrl'orm Chlommcfiam lul#lryl elhfl heknr ltlellrlrns chloddE Haphtralerre TELEhrdrpfumn Tolusne )t$enae, Totar fiun: I,2-0lCrlbmbensene.d4 Surn t,2tlEfi hmsthfl n€.dl $un: El5nrrofl uolomslhrnc Sun: p-Ero6ofl uorqbmrcnE liun:Ttluenodf, l.ltr USL flf ugrLHE lrptfiD ugrlND us,t- NE u$[HE LglLI'lD ugLHD uS,'LND ugil.NI] USLIO1 ?ERECIO8 '[REC'105 ?[R5C SB.O 'JLREC180 fikEc 2D 1.8 l-3 La r_0 20 1_0 I_0 t0 1.0 t,0 6+1t0 TJ-l 30 Ifi19r) 8+110 6tr120 swlizEoE lerEtult3la:!/dkh SW02E0ll lttItEfl$:S$/dhh BllIGef,IB l2r2tIET liri0tdirtr srtJE!fiflE 1e2ilU713:3gidrrsrrEa60E 12,tt/8713:3EldhhElIIslEoE 1?JE1tg7 15:i€ t dthSW82dflB tltil]7 i$;ig f dkhSlrft,zmE 12I21/W,t3:i€ldrrlr SWEIEIB l!j2l/o7 tg:3Bf dkh EwEe60E tl,tltr ts:ag,dhhsltEeE0E l?,?tfft1$:ssJdkhstl{s26[E lztltUI .t3:Ss r dkh SWE2t[D r?l21fl7 13:sH I rlkhsv1ffi263E 12iI1O713;sEIdth EWAI60E 1AElflrr1l:Sgrdkh SIn AtBIB 12& Uof ffi:J3,'dth Erporl FL . ffralyto mpnllng ll[rft. Dcflnllloce: g1CL -OrrHtiS mfihrl llmlt, MCL. l/.arlmum cofiicflrhant tftlel. HO - Nat detesbd al h+ ruFor{ng flnrlt -6- IEACI#.' C0712t013 I lr Ill ri I, _Ery4ffEr ,,/,F!EA!frEE_f,fiC,._2,tr{,sr,t4lsa,f W*yarlalffiil,EO,Eoxtrffi. Gaspq l?rffiEuE lirflFtsedflFLlrl0515 , 307,!35.Nti . F& 307,E31.tdtg . cd,idc.6ffe,Ij4€f,0*; . sr+lrerrrg,fr&oom f, ffAlfTlcilIt 8 Uilfil4TFY FEFOFT January 00, ?008 Denisofl Minrs IUSft] Corp 6415 S Hury 191 Elandlng, UT 84511 WorkErdEtr No.: t07121013 PruJcnt Nam+ becfilhhsrGmundu{EtBrIt' Il' ErlEmy LeboretoflEE, lnc. rBc€i{Ed lho Hlo|*irrg U E€mples lrom Eenison Mines IUSA} Corp on i?r20E00? tor analyaiu. Samplc !D Cllrnl Sample lD Collea Dilr E.c6lvr Df,iE Hilirlfi Test c07121019001 tr/tw 14 ,rsilg/07ilssE 1lir0i07 Aqt €oils lr'lelals by ICPITCFMS, Dlssolwd trtlft2i013.00? M1n 52 12/18rEI t4il0 12fl0fl7 Aqutoue Sarne fu Aho,rc I I I I I I I I t I t t07l2t0t3-DD3 HV{ Zts l2/1&[T 14:15 {2t?0107 Aqueous Hctat* by lcpacpMs, ltesotved E$fE260B VoCa, Srenderd LIal Ct?ll'1013{04 l'ltriJ EB 12fiAIDI l1:e$ l7J?qrc7 AquHous fiBtr'B tfi AbovE C07121O1.4.005 T$F BIHnF 12/5 0OI l4:ES 12/8tr07 Aqumlls SWBZEIIB ltlf,Cs, Stgndad t-let Themlttoro no pmtlgmq wlh llr englyues and ull data frr ae;uiluisd qC nst EPA or laborahry epeclfico,ilonseruept rvhem n+,tsd in lhe Care Harrclive ur HapnrL l[ ytu ha'ro any queeUore regarding t]rese tsste rceults, ploaso catl. n Report Approved By #*#r* -r- TF,BCH# C071er013 ffi f#Ftr#Xf*lTflr#m,;'#*T[ffi;H$vlffi#$#Hf:;,,ffi,f#ffi* QAIQC Summary Eeport Cllant: Denls+n rvlinat (US) C0rp FloJttt: Dicember Gmunfirfiter Report Dala: 01/Ug/09 lrllbrk f, rdtr: C0712r013 Rrrult Unltt BL STEEC Lonlimlt tllghllflrh RFO EfDl-rrnlt Ouat f,lEftod: EzE[,? Ermple lO; LF8-Tlll lrsr €rmpfu lD: LEE lmn Eqmple l0i C0?llEail4illDuS lrqn SrrrflB lh GEItltHa.oftlDllBD lron kloHkry Fsrtllod Blrr* ?.m mg,t Lalorelory Reagnt iila*ND rag,il $amds Mrl'lx Sfikr t't$ !n'+l SnmplB h'lfiFt[ Ep'ko ouptir,ltoS.dl mEiL fttrn: lG?24_O&11008ts rzs Run: lCFl-C. pstrtosE o0 Rtru ICPI-E-08010387r0 1i4 Fm: loFz.c-llgdlolE?0 1E[ 0.0{E 0.046 94 06 Eal+h: HOSTEB 01/0#08 10;07 01filaE$ 1011? 01,ts4I0E t5:38 {ll/s{lS$ 15;42 eo I t I I I I T I I I T I I T I T I t I LlErhod: El00.t 8rmplo lD: LEA Llingane€E Srmph lO: lfE UIEJFTgEnEEE $emFlolE,: f,trtrl0ro-0Efrlisir [rortgil,:6EE trrllptd tE: cE?tt'lotE.[olil,rso{ Mangc.':cee MElhcd Bldnl ,'IE mE,L L*5rEuy Foalliod BlEnk 0.0498 ngll P&{ B,lge€IlEn SFlke 0S47 {ngL F{t+ nherhnh sF,I* l}lDllcsle 0,011 mgL R$r: !GFl,.l6t -c_0T12264 Run: ICPMSt-C_0711264 55 f1t Eun: ICPMSI'C-0IttZfi m 180 turn: ICFM$l.C-0.I1?264 t0 130 0.8 3E{5 o.E0'lE t00 Eatch: IlS47B3 1?126/07 r1:36 r7./26/rt? r1:{3 l2J?61U7 tlt:dS l?fiBl0l 74:52 20 gt 0, 0,o{0 0J'tc Qtrallfiert: BL. finrlytt rEFodrd frldt, -8-Tns.cK# co? I41013 HD . Hcl delc(tud at lhc r€pJrtlnE lhn't. I I I _ElEJifrf 4F:OFA!OEtfi,-{$,E"t{r,trft*EliH$t}r,s/fffffif U.pAftsr*zil . {aqwa/|]fE,?tIatr+Fe#ff/3f,ffi15.301,fr1,4f1J. &,r fl?,234,t€59 . prryefiwrgyhh.m.w,rwfiatgrt*mm I I I eruQC $urnmary Repor1 Cllent Benison [4lnes (USA]0orp Fruled: OerembsrEruund,,wter f,eport Dat+: 01/ESm8 Work Ordsrl CO7121013 Hethsd: E?{0,8 Srnpls lD; LRE cadmJum l*engnnens Fllckd Cedmlum lrtrnBfl[c]E Hlttel RtEiIlt Unltr 0jlElh,o'd Elonh ItD trg,il- $ttr mg,t I'lO rtrg,'L 0-0448 mgdL 5-38 mglI. O,I l5 nqrl Run: t5FI,iS2-C_0? I dSA ft un ; lcPltd$e4_07 t2eaAfls l1ae5 1,t5e3 l1f +r'1: lcP us!-c_o7i ezs,{F0 1.!0it 1JO?E {90 Runt lCFlvlS+C_fiI1 ezEAtu t30I0 lSOT0 130 Bakh: RErl8{}2 l2f26iOI ltl35 121l6r'{}7 t2:42 1z,iEilo7 04:.10 A {flz?ruf OE:irt e020A u0 Rt ttftEE Lsw Lhntt HISh Umll RFtr EfrDllmlr qurl I I I I I I I I I I I I Sihrpl! lljj LFE LliborChsy t-rs|!,llE,d EEfikC*drlum 0,0405 mFL?#,rflOar;s*t 0,0'lEt mflvLNi=lf]6l 0.0488 rr:Utl €lmplolDt Gu7le10l3.ooaAilE4 FnettllllErhlnSFtkACaJrrrlrnt 0,0490 .Trg/LM*rganme 5,2! ;nEdLNrckei O-ltZ mg/L $soFlo lD: OfllflDIr.tUIAilED4 Port Dqartion Sdhp Our,icste 1E45 EE45 {_{lt0? 0.[u10 s?0,c010 s3[,001t s4 $.+ b{ 39 E8 0.010 0.010 0.050 0,010 ll.ul0 0,0i0 r.2 J.L' 2.6 Qtrrllflere; RL. Amtyle repofing flmlt, t{D. tlol delected etlho rBptrilng lftrlt t\ -Tie enslb laEl *Es lrcflErllidn h[rti.tsr rhE sFtkE tBvrEl, Irrecerdsroo w{lh the ntgilred q{ lsce+try ls nrol calcrilaisd, ..9- TTBCTS# C0rt2to13 I I I I I ffi #Ffl!{,iiffi flv#F%!fr ;rof#f#ffi Y#ffiffi/#,$,frl#r;ffi,f#ffi 0A/ftC $urrmary Hepart Cll+nt Denleon lllnet (USA] Corp Proh Et Oecentber G round',r*t+r Eeport DaE: 01,U9ru8 Wo* Order: C07i?1o13 I T t I I I I I I t T I Ar{lF, Ilath+d: SWiEE0E SamphlE: ltilrc.o7.LEg_l AEatdrrE EFn4ne Garbm tetrachlorlrle Chlonrll'rfi ChlcrcmE*Eils g1t+p-Xt/tne$ airlof,rylothyl kGhrr lvlcfiy'€rE c[toride Naphtralene s-rq{ene Istrehtdrofursn Tr'uenr Xl,1sn6t, Tf,taI Sunr t,3{rohtonborucno-d;[ S urr; Dtrornofi uqtm+lhgl1€ Sun: pErrmdlufff, b€nrefh, SurrTElucnodg 8{mDls lDi llDsr.0r:ilBtlLf, AEclffie BsnrEne (hfion klm+ftlurldt Cfuloruiorm ChloltflrEtrfiE nr.ll.Xyfanus Hcthyl oilrrl lttoet ,Iethyltrrc dlondr hhphthglerE o'$tlaor Tsutfiydrofur€n Toluclre XylencaTobl Sur: 1.X-0lohhr0bcnffiio{+ gurr DrEmmoiluErgmelhrne Strr: p'Hrrmllrmmhenanre Eurr: Toluolf{8 Ermple lD; Cllil?1015{O4EH! Benzrra Ciltonteucdlliilde ChtorEhrtn EL tdREf LowLklrlr tHf,fi Llmll RPD RFTILlmtr Qual Lfr bora tot ) Crtrrlml Sarrple 48 ud!- E.E UdL 5,7 trgtl.5.4 ugIL 5.? ug.L10 uf,rlr+B udL E.5 uilL 3,6 uS.t S.'i $Eit {5 r,EiL5,2 u*,L16 USL htethod BlenhND u6[ ND UIJLND u!/L ND WLND UCLTtr u#Ll\D udL ND UfiJIND UCL NE ug{L NE UdLHO ugIL tl0 $slL g7 1.t fidr.c T 1{1.0 rcg f ,0 1f,i1.0 1'J{ 2C 851J lio1.0 rur.c 1E sc 1,0 103 1.0 103r.fi 9I r.0 toll,o s?r.0 gs 9,5 0,5 0.!I 0.5 0.5 0,3 0.5 0.6 fiI 0,6 0,$ flB 180 s8 100 50 102 50 1t2 6U 121 E0 t20 ?0 tgo 80 rJo 80 I20 Runl GChlSl_Er1EzlA E0 'tz0?E ,tst 80 tlo8x 118 Runr GEHSI_III122lASanrlo inerft Splls 1000 us,'L 1lU0 u$JL ?800 ugJL tun: Gcll/f$e.0r1til1A Bf TEhr R$,II?E 12rEl/0? 11:01 1281/U? 1tsE r2,21J07 e0iz0 70 IO 70 70 ?fl 70 ?[ ?'tr IE ]c' 7D T!I] 1ilE lfld 130 t30 1S0 138 1ld 1$C 130 130 ts0 1CD 130 If, 70 ?0 130 r30 ,t3{ T T I Qusllfiq!$r ftL . Arulyle rcprthg llmit - 10- [BACrCf C07l]rDl3 ND - Not deHt€d ilr fi6 l1lpotrhs llrtllt, I I ffiffi@EEi@ ?Di'trEs eff8,i,ffi 0El5 . fiO4,Eiaffil' ' l+1r En7.Efi4,tflfr ' arqaer8.mclryfn twn ' nww.cmrgyffi.twtt I I QAJQG Sunrmary Raport Ellsnfl Oonlnm ,"line* {USA} Corp Prsl+st; EotDTfibtrI Em1nditotdr Report EalE: 0lflrSfi8 WorlrOrdar: C07131013 1$0 1?o 1?0 70 00 s{} t I I t I I I I T T I I rlrrnlyte ilEthod: gtlltl[EE Eamplo loi E0IlIl0l3{06EMS rn +p.Xy{enoe q-Xylene Tf,luene ](ll€nf,E. rOHl 5un: 1.2.ElchhrobenrflFd4 S trn: Dlhramoluommeftane ' Suri p. Emnno,ftroruEsnecne sun: Tolusnr{E Srmpls lD: C!?12'l0{A.004EllED Bsn!€ns OFftorr hlrsEhloridE ChlorofuEn rt+trXyl€nEE o-Xyfel:e Tolrttnc Xylems, Totrl Surr: 1,2.DlGhlfftbffi tffi r"ill Eor; DltromcIucrohl6t}Eud 6 urE o{rcmalluorotefi rEfl E Su[: Tcluon€.d6 Eerull lrn lr$ Sr:rnh HahhSpiko S41 u$,L S41 URIL A4O rrltl 1800 sqtL Eamfle tllatrr Spilm Dupllcatu i10tl ugrL 1300 ugfl- 3700 tJgrl 1100 uoIL lICO UEIL 1fE0 uSIL 22C0 ugt!- Rrrrr : GCItrEi2_071 221 A70 .t3n /u 130 It 13it)m 150E0 1?0 IE i3O B0 '12080 120 Run: EiCHS2-0?1211A rfl 13i: 7fl 133 7i 131 70 134 ?0 t3{ to 130?D 130 8O TTO EL !+REC Lm*Llmlt HIUHL|fiJI BFD RpDltmtt Orfrt E0 *f E0 e4 E0 s4 50 g1 'l O 1no1tr 1r1.l_[ 9Br,E sts 5C 112 5C. 127 s3 lirs S0 1os 5t 105 lo lrE r.0 05t,0 115 1.0 f3 l.t, 100 9.? 12 3.8 1+ 16 1t 1g s.0 0.0 0.0 0.0 EitEh: Rgr{7?0 71r2tt07 ?,t:IJ lIJZlrtt glilJl 20 ?0 zfr lo ?o ?o r0 l0 tu 10 r0 t I I Ouallflore: ItL . Arra[fa roporfng llrttt H0 - l'Iot dElsslsd et l}ra repartlrq lm,n. +rTR.ec# Cg?121013 ffitrErrffiErt?il EltEfrtrV/,/EOfrlTOfrlES,i,LE,.f3flg$df C{g[,ttint*Eytfgtrit|,EOEottlfi. ,fasus: FtyaemplilFlffif,ifi,lflfl,ffifF , fr1135.fffl5 , Faf t07,2.1639. caqperdanei,pfai,anfi.[au,+-Ffq;,I,k].cu#r ;El8l5lrlol.s r# IEIrlcI H+S I figE I ISE I EF; I HlE I EEf i E$E I *+EI E#E IEEE I gEE trq h *EEl E$HJE€t $Ef6Ec Er# EEEilf,:-aF.{E> d*. H EI E Ed E .E $ nrOrEI #Ego. frg? tr i+ tr 6tI. I o I'(rlhfl Eouf,ltr {J UDo -tEToE h TEo ThIEEt{,IErEilE.l Eol-tt (}do Ftt.F la(J trEUI- Ub,Il pumrulnl MxloN oSHSVrrH 33s lEe 'T s= #.8rtE-t}EilEo TFEo Fg gr fil H ,.1>.. f,H $HEtrtr trtr LII =-EJJutrtrtrtr 0EAELlr rdlredrrrueuFuof lE taqllthfl I I Eflt?csEdf,.?3f,d#r$ ".t[Ifa5.4rr$ . FaE 30r,2s1.lt3g , casdEt€e{$E}tuhtom,wrnene.rgilab,ma I t I I I I I t t Energy Laboratories lnc Workorder Receipt Checklist Denison Mines (USA) Corp Login completed hy: Kirnb+rty Humiehn Reviewed b'1r: Revieled Date: ShipFlng wntgrrnerlcoilFr rn S([d urildrlion? Yer 6[l Cu{iod} eeils i,EEt en shlrJlng ooilrlncrJEootur? Ves I?l curlody rerla in$ct Ell gcrEt! xollss? Yer I thaln of cuEJsCy plesattt? Yer p[ Chgin ol cucltCy tinerl urrun tt.irrgulsrred end receluEd? Y€r 7 Ehain ol arl'lody sgreri *ilh EamFle letEls+ Yor ;il StmplhB[lFrEE+recnlahe'rD0u1c? YEr E Sample oontalners htrct? Yer E Suffi:lrrt namlrlevclume for lndlc{trd t€rfi ter $ 4ll EE,nFlei tpc#+Ed wlthin holding l,lmr? Yea [f ComrhBrITcmF Blanx tsrEFErFlure inoomplance? Vof fl uJhtdr .uoA vlsh Faue mto lreedsQ*.-? Ys E lrhicr 'pl'l EcrGF,trhld upon rEcElp4? Y* E 1ililllilll:fiillIIft1flfi'ffililU c07121 D 1 3 Date End Tirne Received: 12/20r20t7 10138 AM Recelved by: kh Carrier narno Noxt Eay Ajr HctFruscil E !'lotFrE€ent U NntPftEent EI HOE {uE HoE HOE xoJ l'lu,I HoE Hs lf htc E NoE Nc f-] Non f,lu E 1,4rC Ofi 106 HEVOAil.IE$ubrr.ttted E tl*.Applhauh glI T I I I T T I conltrt rnd corlEctiaAH?rr 0ofiF6nE: None - 1t- 1IRACIHA C]?121013 EfiEEEYL"ABflEATPffIEq IJlffi 'Xil3.sr,t *eetff'ghrr+$ffiU'PO. tuxffi'i ' f,*ga*; WYffia Wftee0u,2I5.05t5,3fffr5,4il5,&rJ0iai4.tfr!.caup*@eruryrl&h,r0,tr'rfl#64€rgFrd,dflr': t t t I T I I I I I I I t T t t T Ef,te: o3Jan-EE ELIEI{T; Pmpct: Denison lJinas (USAI Corp ftstrmhsr Ertundlrnaler CAEE HAERATIUESample tlollverf Gnoup: 0o7l2fol9 TH!8 IS THE FINAL PAGE OF I'HE I-ABOffATORYAIIATYTICAI REPORT OHIGIilAL EAII1FLE SUETdITTAIIS} trJl orlglnal sample 6tr[mfitals harm been rotumed uiti tlte dala pachage. A copy of [Ie Eubml]tsl(E] hc$ bc.qn lutuded and tracked in lhe dale packEge. SAMPLE TEMPERATURE cOtlFtlAI\CE: a'C (t2'C) TBHltEnElurE of turnplcs recclved nrsf not bt crneldflE{, pmperl} preserved by accepted stendertlu. $amphs lhat stE hEnC d6ll'/erEd lmmarlialely afier collsction shall ha conelderpd ccro:htrla lf theru ls euldencp fiet ths chlllng Etress haE hegun, SOIUSOLID EAlti{PtES A,ll EamFlse ]€Fortod on rfl ss reDoivdd haels unlcse othgndl€E indl+eted. PEE ANALYSIS USTIIE EI+ 505 Eela rcporEd bI ELI urhg EPA firshod flI5 tef,ectg the reEulta loi ssverr ln,Jiuidual Aroclor*. Whon ho rucuhs frr sll seson gm ND [not detechd]. ihe sample meeh EFA psrnpliarrrr crlluria fu PCB monlloinq, SUBCOI{IRACII NG AiIALY$ IS Subcontractlng otsarufllg enillmee to an outsjdc laharatory mq/ bo ntquirod. lf s0, ENERGY |-ABtrRATORIES will ut'lim lle bnanch labfratorios 0r qusliliod oonmct laEoratori6s hr lhiB rnryiEE. Any su6h lf,borEtDrlds rdll be lndicah{ u,ltlilrr tlls Ls borshry AnEtldEEl F{Eps{t, B RANCH I.AEORATOEY LOCATIO]IIS eti-b - Eilergy Lahontories, lnc. - Bltllngs, MT €11{ - ErBrgy LehoHtdlse, Inq. - Gillott6. wY ell$ - Energy Lsborthdae, tnc. - Ho?ano. MT olFr - EnHrEy LEboratoficq. tnr. - Eapld Clty, St) oli{ - En6rgf l.ab0ralEris$, InE - collogo Slatlon, T]t CERTFiCATIOi{S: UgEPe trtrY00002; FL.DOH NElSc; Effr61{;ArfE6ra:AZ0609: Cslllofilh:02118Cr1 OregonI VrrYz0O0O1i UtEh: 307ffiS0i15; VlGlnla: 00o57: t\iashlngton: G1903 tso 17t26 Dtscu[,HER: The results oflhls *nalylical Fepoft mlate only h tha rlenrs subrnltled fcr analyslr, EHERGY LTqEOFATORIEE. !NC.. CASFER,V|IYoerti,f,asthatce(ain mellcd E€lecllofie rcnlElnsd ln lhis mpoil mcct tsquhEfllsnb ari EEt fortfi by tlls aborue accredltlng gulhorllleE. Scrns rEillh 16qtJB6ted by lhe Elhnt may mt bs corered undar theae cBrtlflcailons, Atl snalltls dslE to bo subrtittcd ftr rEguhtory cnfc.EEmflil thould ba cediliod ln thc ramPlo atate ol orlgln. Pl66Eo vBfiry EU'g osrtifiEolion soytrflgs by vlrl[ru wtrv.efleEytab.eorn ELI apprtclates th6 oFptrdunlty to Frwk 6 you with lhlt malyticd servic6- Foradditlorral lnlormallon and *ervhoe v{elt our weh ptge wr*vr,enargy'ab,com, Tlre total rrurnber of psge* ol lHr r€pod ar€ lndlealed bytho paga n.JrrbEr locdcd ln Hs lowff rlohI6orner, T T - 14- 'rfl.frcr# c0?J.21013 :7.r;.::r."1:.i.,jj t);:'|il.r,l:,i|. tti, -&&ttrLfrlltu!,gEgEgIEEW ENEROY LABORATORIES, lNC. " 2393 Sa// Creek Hrghway (8260A . PO. Box 3258 " Caspes WY 82602 7b/1Free888.235.05/5,307.235.05/5.Fax307.234./639-caspe@energylab.ffim.w4weneej4ab.em QA/QC Summary Report Client: Denison Mines (USA) Corp Project: December Groundwater Revised Date: O2D2l08 Report Date: 01/09/08 Work Order: c47121413 I I t I t I I I I I I I I T t T t I I Analyte Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: Sample lD: Uranium Sample lD: Uranium Sample lD: Uranium Sample lD: Uranium E200.8 LRB LFB c07120802{04EMS4 c07120802{XXEMSIX Method Blank ND mglL Laboratory Fortifled Blank 0.0460 mg/L Post Digestion Spike 0.0660 mg/L Post Digestion Spike Duplicate 0.0639 mg/L 1 E-05 0.00030 0.00030 0.00030 92 106 101 Run: ICPMS2-C_071226A Run: ICPMS2-C_0712264 115 Run: ICPMS2-C_071226A 70 130 Run: ICPMS2-C 0712264 130 3.3 Batch: Rgz8o2 12126107 12:35 1Z26107 12142 '12126107 16:00 12126107 16:07 20 Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. C071210'13 R1 Page 3 of4 t I *,gt :,*, ;""ffifl: 7:NERGYLIB_O-EAIaTES! tNC " 239! Sa/t Crcek Hrghway (s260/) , PO. Box 3258 " Casper; WYs2002:1;_*-ffi lZtl/fiee888.235.05/5 ' 307.235.05/5 . Fax307.234./6i9 . baspr@energylab.com " w,uuenefolrtaO.mi Date: 22-Feb-08I I Project: Sample Delivery croup; C07121013 Denison Mines (USA) Corp December Groundwater CASE NARRATIVE I I T I I I I I I I T I t I THIS IS THE FINAL PAGE OF THE LABORATORY ANALYTICAL REPORT REVI SED/SUPPLEMENTAL REPORT The attached analytical report has been revised from a previously submitted report due to the addition of Uranium onsamples MW14 and MW26 per request from Steve Landau 212212A09. oRr Gt NAL SAMPLE SUBMTTTAL(S) All original samplesubmittalshavebeenreturnedwiththedatapackage. Acopyofthesubmittal(s) hasbeenincluded and tracked in the data package. SAMPLE TEMPERATURE COMPLIANCE: 4.C (t2.C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that arehand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. PCB ANALYSIS USING EPA 505 Data reported by ELI using EPA method 505 reflects the results for seven individual Aroclors. When the results for allseven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTI NG ANALYSIS subcontracting of sample analyses to an outside laboratory may be required. lf so, ENERGY LABoRAToRIES will utilizeits branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within theLaboratory Analytical Report. BRANCH LABORATORY LOCATI ONS eli-b - Energy Laboratories, lnc. - Billings, MT eli-g - Energy Laboratories, lnc. - Gillette, WY eli-h - Energy Laboratories, Inc. - Helena, MT eli-r - Energy Laboratories, lnc. - Rapid City, SD eli-t - Energy Laboratories, lnc. - College Station, TX CERTFICATIONS: USEPA: \A/Y00002; FL-DOH NELAC: E87641; Arizona: ,420699; California: 0211BCA Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, lNC. - CASPER,WY certifies that certain method selections contained in this report meetrequirementsassetforthbytheaboveaccreditingauthorities. Someresultsrequestedbytheclientmaynoibecovered under these certifications. All analysis data to be submitted for regulatory enforcement should be certifiid in the samplestate of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit ourweb page www. energylab. com. The total number of pages of this report are indicated by the page number located in the lower right corner. T C07121013 Rl Page 4 of 4 ENEEGYLABORATORIES,lNC. .2S9SSaltCreekHlghway(82ffi1).P.O. Box3258 . Casper, WY82602 TollFreeffi.235.05l5 " 307.2''n515. Fax307.234.1639 " casper@energylab.cot 'ru,w.energylab.mm LABORATORY ANALYTICAL REPORTI I Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp / 4th Qtr Groundwater/Semi-Annualy' co711oo77-014 /MW1 I/ Report Date: Collection Date: DateReceived: Matrix: 01t07t08 10131107 08:53 fit0a07 Aqueous I Analyses Result Units Quallfiers RL MCU QCL Method Analysls Date / By D pCi/L pCi/L I I I I I I I I t t T I t MAJOR IONS darbonateas Co3 /Bicaoonate as HCO3/ c^t iu^l/ crrrrioeV Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium dodium Auffate II / PHYSTCAL PROPERTTES VpHSolids, Total Dissolved TDS @ 180 C METALS . DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt fcooo.,I honI rcaa ! u"n9rn"." Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium hin" II I RADTONUCLTDES - DTSSOLVED , I Gross Alpha minus Rn & U V Gro"" Alpha minus Rn & U Precision (*) ND mg/L 300 mg/L176 mg/L 17 mg/L0.3 mg/Lil.2 mg/L 0.27 mg/LND mg/L8.2 mg/L171 mg/L 753 mg/L 7.79 s.u. 1390 mg/L ND ug/LND ug/L ND ug/LND ug/LND ug/LND ug/LND ug/L ND ug/L15 ug/LND ug/LND ug/L ND ug/LND ug/LND ug/L ND ug/L ND ug/L0.94 ug/LND ug/LND ug/L 1.2 0.6 1 1 0.5 1 0.1 0.5 0.05 0.1 0.5 0.5 30 0.01 10 5.0 0.50 0.50 25 10 10 30 1.0 10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 1.0 A232OB 423208 E200.7 44500-Ct B A4500-F C E200.7 A45OO-NH3 G E353.2 E200.7 E200.7 44500-504 E 11106107 16:10 / bas 11tO6iO7 16:10 / bas 11115107 19:02 / ts 11107107 12:45llil 11105107 14:01 / bas 11115107 19:02 / ts 11lOOl07 12:43ljal 11108107 14'i2lial 11115107 19:02 / ts 11115107.'19:02 I ts 11lOOlO7 12:59 lzd A4500-H B 11lOSl07 10:45 / rw A2540 C 11105107 14:15 I rvv E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E900.1 E900.1 11l0gl07 21:47 lbwsfillili7 21:47 lbws 11l0gl07 21;47 I bws 11l0gl07 21:47 lbws lll0gl0l 21:47 lbws 11l0gl07 21:47 lbws 1'1115107 19:02 / ts 11l0gl07 21:47 lbws 11109107 2'l:47 lbws 11109107 21:47 lbws 11l0gl07 21;47 lbws 11109107 21:47 lbws 11109107 21:47 lbws 11109107 21:47 lbws 11109107 21;47 lbws 11l0gl07 21:47 I bws 11l0gl07 21:47 ttus 11109107 21:47 lbws 11l0gl07 2'l:47 lbws 11116107 16:02 / cnrrr 11116107 16:02 / clw I T Report RL - Analyte repofting limit. Definitions: eCL - euality control limit. D - RL increased due to sample matrix interference. MCI- - Maximum contaminant level. ND - Not detected at the reporting limit. -28-TPAcT(# cn'7 11nn11 ENERGY LABORATOEIES, lNC. . 2393 Salt Creek Highway (82601) . P.O. Box 3258 " Caspet W82602 Toll Free 888.235.0515 , 3022' - ',515 . Fax 302234.1639 , caspr@energylab.m: 'vww:energylab.com I I Client: Project: Lab lD: Client Sample lD: LABORATORY ANALYTICAL REPORT Denison Mines (USA) Corp 4thQtrGroundwater/Semi-Annual,/ co711oo77-014 /MW1 v Report Date: 01/07/08 Collection Date: 10/31/07 08:53 DateReceived: 1 1 102107 Matrix: Aqueous I Analyses Result Unlts Qualifiers RL MCUQCL Method Analysis Date / ByI I T I I I T I I I I T t DATA QUALITY /RrC eatance (r s) / Rrions I / cationsV Solids, Total Dissolved Calculated TDS Balance (0.80 - 1.20) VOLATILE ORGANIC COMPOUNDS Acetonet flenzene^ Carbon tetrachlorideI\ /cttororo-Vchloromethane Methyl ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Sun: 1,2-Dichlorobenzene-d4 Sun: Dibromofl uoromethane Sun: p-Bromofl uorobenzene Surr: Toluene-d8 1.45 o/o 2'1.1 meq/L 21.7 meq/L 1340 mg/L 1.04 dec. Yo ND ug/L ND ug/LND ug/LND ug/L ND ug/L ND ug/LND ug/LND ug/L16 ug/L ND ug/L ND ug/L104 %REC127 %REC115 %REC 97.0 %REC 20 't.0 1.0 1.0 1.0 20 1.0 1.0 10 1.0 1.0 80-120 70-1 30 80-120 80-120 Calculation Calculation Calculation Calculation Calculation SW826OB SW8260B SW826OB SW8260B SW826OB SW826OB SW826OB sw8260B SW826OB SW826OB sw8260B SW826OB sw8260B SW826OB SW826OB 11116107 14:39 / bws 11116107 14:39 / bws 11116107 14:39 / bws 11t16107 14:39 / bws 11116107 14:39 / bws 11105107 23:30 / dkh 11105t07 23:30 / dkh 1 1/05/07.23:30 / dkh 11lOSl07 23:30 / dkh 11105107 23:30 / dkh 11105107 23:30 / dkh 11l1gl07 23:30 / dkh 11lO5lO7 23:30 / dkh 11lgslo7 23:30 / dkh 11t05t07 23:30 / dkh 11105107 23:30 / dkh 11105107 23:30 / dkh fi105fi7 23:30 / dkh 11105107 23:30 / dkh 11105107 23:30 / dkh Report Deftnitlons: RL - Analyte reporting limit. QCL - Quality control limit. MCL - Maximum contaminant level. ND - Not detected at the repofting limit.I T -29- TRACK# C07110077 ENERGY L/|BORATORqES, tNC. , 2393 Salt Creek Highway (8260U . PO. Box 3258 . Casper; WY82602 fitt fbe AA.ZeS.1,l, , 307.i 1515 , Fax 307.234./d?9 ' casper@energylab.co 'aww.energylab.com I I I LABORATORYANA ,YTICAL REPORT Client Denison Mines (USA) Corp Report Date: 01/07/08 Collection Date: 10123107 O7:31 DateReceived: 10126107 Matrix: Aqueous Project: Lab lD: Client Sample lD: 4th Quarter/Semi-Annual Groundwater c071013/.1-oo2 MW2 Analyses Result Units Qualifiers RL MCUOCL Method Analysis Date / ByI I I I I I I I I I t I I MAJOR IONS Carbonate as CO3 #carbonate as HCO3 /c^t"iu^ / ctrtoriae'/ ruorioe Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N METALS. DISSOLVED Arsenic Beryllium Cadmium c{romiumI Sobalt\ 0opper \r/r,on Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium ; Vanadium i i Zinc tt I neoroxucLtDEs - DrssoLVEDI \fGross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (t) 7.41 3100 1 1 0.5 1 0.1 0.5 0.05 0.1 0.5 0.5 30 5.0 0.50 0.50 25 10 10 30 1.0 10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 1.0 ND mg/L 396 mg/L 337 mg/L 6 mg/L 0.3 mg/L100 mg/L ND mg/LND mg/L 10.5 mg/L460 mg/L 1990 mg/L A2320 B A232OB E200.7 A4500-Ct B 44500-F C E200.7 A45OO-NH3 G E353.2 E200.7 E200.7 A4500-SO4 E E200.8 E200.8 E200.8 E200,8 E200.8 E200.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E900.1 E900.1 fil02lA7 22:02lbas 11102107 22:02lbas 11106107 18:28 / ts 11101t07 14:22lljt 10131107 21:14 lbas filA6l07 18:28 / ts 11105107 10:00 / jal 10129107 09:02 / jal 11106107 '.t8..24 tts 1110G107.18.24 I ls 11lOSlO7 12:58 lzd 10E1lO7 18:59 / bws 10l31l0l 18:59 / bws 10131107 18:59 / bws 10131107 18:59 / bws 10131107 18:59 / bws 10131107 18:59 / bws 11106107 18:24lts 10131107 18:59 / bws 10131107 18:59 / bws 10l31l0l 18:59 / bws 1Ol31lO7 18:59 / bws 10131107'18:59 / bws 1Ol31lO7 18:59 / bWs 10R1lO7 18:59 / bws 'l0l31l07 18:59 / bws 10131107 18:59 / bws 10131107 18:59 / bws 10131107 18:59 / bws 1Ol31lO7 18:59 / bws 11113107 '16:56 / crw 11l13l0l 16:56 / crw 0.0'l 10 s.u. mg/L 44500-H B 10127107 11:15 / bas A2540 C 1Ol28lO7 13:42lbas ND ug/LND ug/L ND ug/LND ug/L ND ug/LND ug/LND ug/L ND ug/L ND ug/LND ug/L ND ug/LND ug/L8.1 ug/LND ug/L ND ug/LND ug/L10.3 ugrll-ND ug/L 14 ug/L 1.3 0.5 pCi/L pcru I T Report RL - Analyte reporting limit. Definltions: eCL - euality control limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant level. ND - Not detected at the reporting limit. -4- TRACK# C07101341 ENEBGY LABORATORIES, lNC. " 2393 Salt Creek Hlghway (8260A , P.O. Box 3258 , Caspe4, W82602 TollFree888.235.05l5 " 302[ 't515 , Fax 307.234./639 , casper@energylab.cc www:energylab.com I I I LABORATORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp 4th Quarter/Semi-Annual Groundwater c07101341-002 MW2 Report Date: Collection Date: DateReceived: Matrix: 01t07t08 10123107 O7:31 10t26t07 Aqueous Result Units Qualifiers RL MCUQCL Method SW826OB s\ 182608 SW826OB SW826OB SW826OB SW8260B SW826OB SW8260B SW826OB SW826OB sw8260B SW826OB sw8260B SW826OB SW8260B I I t I t I I T I t I t TA QUALITY A/C Balance (t 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 - 1.20) VOLATILE ORGANIC COMPOUNDS -2.96 48.1 45.3 31 10 1.00 o/o meq/L meq/L mg/L dec. o/o Calculation Calculation Calculation Calculation Calculation Analysis Date / By 11107107 13:57 / bws 1'1107107 13:57 / bws 11107107 13:57 / bws 11107107 13:57 / bws 11107107 13:57 / bws 10129107 14:59ljtr 1Ol29lO7 14:59ljtr 10129t07.14:59 tjlr '10129107 14:59 / jlr 10ngt07 14i5s tjt 10129107 14:59 I jn 10nst07 14:59 / jlr 1Ol29lO7 14:59ljlr 10129t07 14:59 / jk 1Ol29lO7 14:59 I jk 10129107 '14:59 / jk loDglOT 14:59 t jk 10129107 14:59 I jlr 10129107 14:59 / jlr 10129107 14:59 / jlr /cetone /B"n .n / C^rAontetrachloride / ctrloroform 1 Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Sun: 1,2-Dichlorobenzened4 Surr: Dibromofluoromethane Surr: p-Bromofl uorobenlene Sur: Toluene-d8 ND ug/LND ug/LND ug/L ND istLND ug/LND ug/L ND ug/L ND ug/L ND ug/LND ugA ND ug/L 96.0 %REC95.0 %REC103 %REC101 o/oREC 20 1.0 1.0 1.0 1.0 20 1.0 1.0 10 1.0 1.0 80-120 70-130 80-120 8G.120 t I T Report RL - Analyte reporting limit. Deflnftlons: eCL - euallity control limit. MCL - Maximum contaminant level. ND - Not deteded at the reporting limit. -5- TRACK# C07101341 ENERCY LABOBATORIE/ lNC. . 2393 Saft Creek Htghway (82601) . P.O. Box 3258 . Caspet W82602 Tol/Free888.235.05/5 , 307.2' t5l5 " Fax 307.234.1639 , casper@energylab.cc ,uwwehergylab.com I I T LABORATORYANAL REPORT Client: Project: Lab lD: Glient Sample lD: Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual c07110077-011 MW3 Report Date: 01/07/08 Collection Date: 10/31/07 0T:10 DateReceive d: 1 1 lo2l07 Matrix: Aqueous Analyses Result Units Qualifiers RL MCU QCL Method Analysis Date / ByI li / I MAJOR IONS $*onateas Co3 .Cicarbonate as HCO3 /crt"iu Chloride Fluoride Magnesium Nitrogen, Ammonia as N PHYSICAL PROPERTIES pH Solids, Total Dissolved TDS @ METALS. DISSOLVED ND 516 482 63 0.4 246 0.07 0.1 23.3 8U 3120 6.95 5150 ND pCi/L ND ug/LND ug/L0.98 ug/LND ug/LND ug/LND ug/LND ug/LND ug/L 1950 ug/LND ug/LND ug/L21 ug/L8.9 ug/L ND ug/L 1.15 ugAND ug/t39.4 ug/LND ug/L13 ug/L E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E900.1 1 1 0.5 1 0.1 0.5 0.05 0.1 0.5 0.6 30 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L A232OB 423208 E200.7 A4500-Ct B A4500-F C E200.7 A45OO.NH3 G E353.2 E200.7 E200.7 44500-S04 E 11106107 15:12 I bas 11106107 15:12 tbas 11115107 18:35 / ts 11107107 12:30lljl 11lOSlO7 13:50 / bas 11115107 18:35 / ts 11106107 12:33ljat 11108107 13:47 liat 11115107 18:32 / ts 1 1/15/07.18:35 / ts 11lOOl07 12:54 lzdI s.u. mg/L I T I I T I I I I 180 C 0.01 10 5.0 0.50 0.50 25 10 10 30 1.0 10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 1.0 A4500-H B 11105107 10:41 / rw A2540 C 11105107 14:14 t rw Arsenic B/ryltium dadmium 6hromium lcoo^tt.f copw,V lron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium 11109107 21:26 lbuvs 11109107 21:26 / bws 11109107 21:26 I bws 11l09lll 21:26 tbrus 11109107 21:26 / bws 11109107 21:261bws 11115107 18:32 / ts 11109107 21:26 / bws 11109107 21:261bws 11109107 21:26 / bws 11109107 21:26 / bws 11109107 21:26lbws 11109107 21:26 / bws 11109107 21:26 lbws 11109107 21:26 tbws lll0gl0l 21:26 / bws 11109107 21:26 / bws 11109107 21;26 tbws 11109107 21:26 tbws 11116107 14:24 I emt . DISSOLVED Alpha minus Rn & U Pq{assium S6dium ulfate Report Definltions: RL - Analyte reporting limit. QCL - Quallty control limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant level. ND - Not detected at the reporting limit.I I _22_ rFPArrr{# ?a1 11nn'l1 ENEflGY LABORATORIES, lNC. , 2393 Salt Creek HlThway (82601) "PO. Box 3258 , Casper; W82602 TollFree888.235.05l5 , 307.? ',515 . Fax 307.234.1639 , casper@energylab.cc www.energylab.com LABORATORYANAL REPORTI I Glient: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual c07110077-011 MW3 Report Date: 01/07/08 Collection Date: 10/31/07 O7:1O DateReceived: 1 1 102107 Matrix: Aqueous MCURL QCL Method t I I I I I I I I I I I t T Result Unlts Qualifiers Calculation Calculation Calculation Calculation Calculation sw8260B SW826OB SW826OB SW826OB sw8260B sw8260B SW826OB SW826OB sw8260B sw8260B SW826OB sv\r82608 SW826OB SW8260B SW8260B Analysis Date / By 11116107 14:38 / bws 11t16i0714:38 / bws 11116107 14:38 / bws 11116107 14:38 / bws 11116107 14:38 / bws 1110510719:31/dkh 11l0st0l'19:31 / dkh 11105107.19:31 ldkh 1110510719:31/dkh 11105107 19:31 / dkh 11105107 19:31 / dkh 11lO5lO7 19;31 / dkh 11105107 19:31 / dkh 11105107 19:31 / dkh 1110510719:31/dkh 11105107 '19:31 / dkh 11105107 19:31 / dkh 11105107 19:31 / dkh 11105107 19:31 / dkh 11105107 19:31 / dkh A QUALITY Balance (t 5) Solids, Total Dissolved Calculated TDS Balance (0.80 - 1.20) VOLATILE ORGANIG COMPOUNDS Rcedne Bg(zene darbon tetrachloride ,6hbroform /chloromethane [/ ttt tnytethyt ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surr: 1,2-Dichlorobenzene-d4 Sur; Dibromofl uoromethane Sun: p-Bromofluorobenzene Sun: Toluene-d8 2.99 75.3 80.0 5010 1.03 o/o meq/L meq/L mg/L dec. o/o ND ug/LND ug/L ND ug/L ND ug/LND ug/LND ug/LND ug/L ND ug/LND UgAND ug/L ND ug/L 102 %REC125 %REC115 %REC99.0 %REC 20 1.0 't.0 1.0 1.0 20 1.0 1.0 10 1.0 't.0 80-120 70-130 80-120 80-120 Report Definltions: RL - Analyte reporting limit. QCL - Qualig control limit. MCL. Maximum contaminant level. ND - Not detected at the reporting limit.I I -23- TRACK# eO71 1 0077 T ENERGY LABORATORIES, INC '-2393 *a/t Creek Highway (82ffi1) . P.O. Box S2SS . Casper Wya2602rott Free 8fi.23s.0515 . s07.i 15ff : Fax sbifu4,;;5b :b;;i;;6r;;6yffi;:*,r"r;;;;;;s;Lb.:rm T I LABOMTORY ANALyTTCAL REPORT Glient: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual c07110077-012 MWSA Report Date: Collection Date: DateReceived: Matrix: 01to7t08 10131107 07:51 11t02t07 AqueousI Analyses MCU QCL MethodResult Unlts Qualifiers RL . DISSOLVED Gross Alpha minus Rn & U Analysis Date / By mg/L mga mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L METALS. DISSOLVED Arsenic Q'erylltum 6admium rbhromium /cou"tt, i / Copper V lron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium t I t I I I I t T Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium 6uffateII/ PHYSTCAL PROPERTTES ./ pH V Sotid., Totat Dissolved TDS @ 180 C ND 324 479 60 1.4 310 ND 1.2 29.3 741 3470 6.92 s.u. 5490 mg/L ND ug/L1.32 ug/L1.23 ug/LND ug/LND uglLND ug/LND ug/LNO ug/L142 ug/LND ug/LND ug/LND ugA73.9 ug/LND ug/L1.01 ug/LND ugrl-22.9 ug/LND ug/L40 ug/L pCi/L 1 1 0.5 1 0.1 0.5 0.05 0.1 0.5 0.6 3o 0.01 1o 5.0 0.50 0.50 25 10 10 30 1.0 10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 1.0 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E900.1 D D F232O B 11tO6tO7 15:19 / basA232OB 11to6i}71S:19/basE200.7 11t1it1t18:42lts 44500-Cl B lll|Zt|t 12:34 t tjt A4500-F C lltOStOZ 13:53 / basE200.7 11t1SlO7 18:42 tts 44500-NH3 G 11106/07 ,12:38 t jatE353.2 11lOBtO713:50 / jatE200.7 1lt1ltlt 18;39 / tsE2O0.7 11t11tOt.18:42 t ts A4500-SO4 E 11tO6tO7 12:i7 tzd 44500-H B 11lOStO7 10:42 t rw 42540 C lltOStOZ 14:14 I rw 11109107 21;33 / bws 11109107 21:33 / bws 11109107 21:33 / bws 11109107 21:33 / bws 11109107 21:33 / bws 11109107 21:33 / bws 11115107 18:39 / ts 11t09tQ7 2,t:33 / bws 11109107 21:33 / bws 11109107 21:33 / bws 11109107 21:33 / bws 11109107 21:33 / bws 11109107 21:33 / bws 11109107 21:33 / bws 11109107 21:33 / bws 11109107 21:33 / bws 11109107 21:33 / bws 11ligl07 21:33 / bws 11109107 21:33 / bws 11116107 16:02 t cwv I Report Definltions: RL - Analyte reporting limit. QCL - Quality control timit. D - RL increased due to sample matrix interference MCL - Maximum contaminant level. ND - Not detected at the reporting limit.I T -24-rf.ELnw+ rrn.111^.r.11 ENEEGY LABORATORI-ES, tNC , 239! Salt Creek Highway (82601) " PO. Box 32SB . Caspet; W 82602Tott Free 888.235.0515 ' 30zZ'- nsts , Fax sni.iat.io1i ;-ciipeideitirsylai.@7-- "t44i,:;;;;biiab.@n I t I I Client: Project: Lab lD: Glient Sample lD: LABORATORY ANALYTICAL REPORT Denison Mines (USA) Corp ,/ 4th Qtr Groundwater/Semi-Annuat /co711oo77-012 /MW3A V Report Date: Collection Date: DateReceived: Matrix: 01t07t08 10131107 07:51 11t02t07 Aqueous Result Unlts Quallfiers RL MCUQCL Method I I t I I I T I I I I TA QUALITY Balance (* 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.90 - 1.20) VOLATILE ORGANIC COMPOU NDS fcetone ,,BenzeneI / Carbon tetrachloride f Chloroform / Chloromethane { Utettrylettryt ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Sun: 1,2-Dichlorobenzened4 Sun: Dibromofluoromethane Surr: p-Bromofl uorobenzene Sur: Toluene-d8 1.83 79.4 82.4 5270 1.04 o/o meq/L meq/L mg/L dec. o/o Calculation Calculation Calculation Calculation Calculation sw8260B SW826OB SW8260B sw8260B SW826OB SW8260B SW826OB sw8260B SW826OB SW8260B SW826OB SW826OB sw8260B SW8260B SW8260B Analysis Date / By 11116107 14:38 / bws 11116107 14:38 / bws 11116107 14:38 / bws 11116107 14:38 / bws 111'16107 14:38 / bws 11105107 22:10 tdkh 11105107 22:1A I dkh 11105107.22:10 I dkh 11105107 22:10 I dkh 'i,1105107 22:10I dkh 11105107 22:10 I dkh 11l05l0l 22:10 I dkh 11105107 22:10I dkh 11105107 22:10 tdkh 11l05lOZ 22:10I dkh 11l05lOZ 22:101 dkh 11lOSl07 22:10I dkh 11105107 22:10I dkh 11105107 22:10 I dkh 11lO5tO7 22:10 t dkh ND ug/LND ug/LND ug/LND ug/L ND ug/LND ugAND ug/LND ug/tND ug/LND ug/LND ug/L102 ToREC125 %REC113 %REC99.0 %REC 20 1.0 1.0 1.0 1.0 20 1.0 1.0 10 1.0 1.0 80-'t20 70-130 80-120 80-120 T I I Report Definltions: RL -Analyte reporting limit. QCL - Quality control limit. MCL - Maximum contaminant ldvet. ND - Not detected at the reporting limit. _25_ .ITRACT{# Afi7 11no1-7 _ENERGY LABoRAToB_l^Es, tmc ._239! satt Qr gf rylgQway (s2601) . po. Box 32i8 . caspet; w a2602TottFree888.235.05t5 " a1z{ '0s15, Faxa07.234.b3e .'cisperaieneigyEi.i---r4r*.;;;isiiab.'@n I I T Client Denison Mines (USA) Corp /Projec* 4th Qtr Groundwater/Semi-Annuat / Lab ID: CO711OOZ7-OO7 / CtientSample lD: MW4 V LABORATORY ANALYTICAL REPORT Report Date: 01/07/08 Collection Date: 10/30/07 14:35 DateReceived: 1 1 102t07 Matrix Aqueous Analyses Result Unlts Qualifiers RL MCU QCL Methodt I t t I I I I I I MAJOR IONS C{rbonateas CO3 ficarbonate as HCo3 /crt";u /:*;:: Magnesium ND 356 273 46 0.3 125 ND 6.0 7.4 89.8 944 7.37 s.u. 1780 mg/L ND ug/LND ug/LND ug/LND ug/LND ug/LND ugAND ug/LND ug/tND ug/LND ug/LND ug/LND ug/L52.3 ug/LND ug/LND ug/LND ug/L9.87 ug/L ND ug/LND ug/L ND pCi/L 1 1 0.5 1 0.1 0.5 0.05 0.2 0.5 0.5 30 0.01 10 5.0 0.50 0.50 25 10 10 30 't.0 10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 1.0 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.E E200.8 E200.8 E200.8 E900.1 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 42320 B 11tO6tOZ 13:41 / bas 42320 B 11tO6tOZ 13:41 / bas8200.7 l1t1\tot 18:06 / tsA4500-ClB 1llOilOZ 10:41 iljt 44500-F C l1tOStO7 13:33 / basE200.7 11t1StO718:06/ts 44500-NH3 c 11tffit\t 12:19 ljatE353.2 11tOBtO7 13:32 t jatE200.7 11t15t07 18:02 / tsE200.7 11t1StOZ .18:02 tts 44500-504 E 11t}6t1t 12:Oi lzd A4500-H B lltOStOZ i0:33 / rw 42540 C 11tOStO7 14:12 t rw l/ Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate PHYSICAL PROPERTIES pH Solids, Totat Dissolved TDS @ 1BO C METALS. DISSOLVED Arsenic Beryllium CTdmium Ohromium louatt , fcopp",vH. Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc I f muilff ',P,ii; D'!ssoLVED lll0gl17 20:45 / bws 11109107 20:45 / bws 11l0gl07 20:45 / bws 11109107 20:45 I bws 11109107 20:45 / bws 11loglo7 20:45 I bws 11115107 18:02 / ts 11109107 20:45 / bws 11109107 20:45 I bvts 11109107 20;45 / bws 11109107 20:45 / bws 11109107 20:45 / bws 11109107 20:45 / bws lll0gl0l 20:45 / bws 11109107 20:45 / bws 11l0gl07 20:45 / bws 11109107 20:45 / bws 11l09lol 20:45 / bws 11109107 20:45 / bws 11116107 14:24 I clt I Analysis Date / By Report Deflnltions: RL - Analyte reporting lirnit. QGL - Quality control limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant level. ND - Not deteded at the reporting limit.I t _t4_ rTrpLnta# f A't11rr[-r1 ENEEGY LABORATOHEA NC. , 2393 Salt Creek Highway (52601) " P.O. Box 3258 . Caspet W82602TollFree888.235.05l5 ' 307.? 'q5ff " Fax 307.234.1ffi9 , casper@energylab.cc wtwuehergylab.mn I LABORATORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp , 4th Qtr Groundwater/S emi-Annual/co711OO77-OO7 ^/MW4 I/ Report Date: Gollection Date: DateReceived: Matrix: 0'lto7t08 10130107 14:35 11t02t07 Aqueous I T I I t I Result Units Qualifierc RL MCU QCL Method ND ND 2.3 2700 ND ND ND ND ND ND ND 105 128 115 99.0 I T I I t I I t I I DATA QUALITY tuC Balance (t 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 - 1.20) VOLATILE ORGANIC COMPOUNDS Acgtone B#zene drOon tetrachloride lhloroform I /ChloromethaneV U"ttyt ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Sun: 1,2-Dichlorobenzene-d4 Sun: Dibromofl uoromethane Sun: p-Bromofl uorobenzene Sun: ToluenedS 1.46 27.2 28.0 1700 1.05 % meq/L meq/L mg/L dec. % ug/L ug/L ug/L ug/L ug/L ug/L ug/L uga ug/L ug/L ug/L %REC o/oREC %REC %REC 20 1.0 1.0 100 1.0 20 1.0 1.0 10 1.0 1.0 80-120 70-130 80-120 80-120 Calculation Calculation Calculation Calculation Calculation SW826OB SW8260B SW826OB SW8260B SW826OB SW826OB SW826OB sw8260B SW826OB SW8260B SW826OB SW826OB SW826OB SW8260B sr E260B Analysis Date / By 11116107 14:37 / bws 11116107 14:37 / bws 11116107 14:37 I bws 11116107 14:37 / bws 11116107 14:37 tbws 11lOOlO7 00:11 / dkh 11106107 00:11 / dkh 11/06/07-00:11 / dkh 11106107 00:52 / dkh 11106107 00:11 /dkh 11106107 00:11 / dkh 11106107 00:11 / dkh 11lOOlO7 00;11 / dkh 11lOOl07 00:11 / dkh 11106107 00:11 / dkh 11106107 00:1't / dkh 11106107 00:'11 / dkh 11106107 00:11 / dkh 11106107 00:11 / dkh 11106107 00:11 / dkh Report Deftnltions: RL - Analyte reporting limit. QCL - Quality control timit. D - RL increased due to sample matrix interference. MCL - Maximum contiaminant level. ND - Not detected at the reporting limit. I _ 15_ryPAcra* ool 11nn'l1 ENERGY LABORATOBIES, lNC. . 2393 Salt Creek Highway (82601) , P.O. Box 3258 . Caspq W82602 Toll Free 888.235.0515 " 307.' - 0515 , Fax 307.234.1639 , casper@energylab.c wwwehergylab.com t I I LABORATORY YTICAL REPORT Client: Project: Lab lD: Client Sample tD: Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual c07110077-001 MW5 Report Date: Collection Date: DateReceived: Matrix: 01t07t08 10129107 08:30 11t02t07 Aqueous Analyses Result Unlts Qualifiers RL MCU QGL Method Analysis Date / By D I I t I I I I I T I t I I M^JOR IONS Oarbonate as CO3 lbrc.arlonateas HCO3I calcium ./ chloriae/ Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N ND mg/L 378 mg/L138 mg/L 50 mg/L1.0 mgA39.3 mg/L 0.43 mg/LND mg/L8.4 mg/L476 mg/L 1130 mg/L 8.09 s.u. 1880 mg/L ND ug/LND ug/L ND ug/LND ug/LND ug/LND ug/LND ug/L ND ug/L142 ug/LND ug/LND ug/LND ug/LND ug/LND ugAND ug/LND ug/L0.61 ug/LND ug/LND ug/L 1 1 0.5 1 0.1 0.5 0.05 0.1 0.5 0.5 30 0.01 10 5.0 0.50 0.50 25 10 10 30 1.0 10 0.s0 10 20 5.0 10 0.50 1oo 0.30 15 10 1.0 423208 Ac32OB E200.7 44500-Ct B A4500-F C E200.7 A45OO-NH3 G E353.2 E200.7 E200.7 44500-504 E 11106107 02:41 lbas 11106107 02:41 I bas 11115107 16:52 / ts 11107107 10:11 iljt 11lOSlO7 13:07 / bas 11115107 16:52 / ts 1110610712:O1l jat 11lO8lO7 13:'t0 / jal 11115107 16:52 / ts 11115107.16:$2 I ts 11106107 11:53 t zd ,tassium odium Sulfate PHYSICAL PROPERTIES pH Solids, Total Dissolved TDS @ 1SO C METALS. DTSSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper lron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium 44500-H B 11t05t07 10:251 wv 42540 C lltOStOZ t411 I tw ND pci,tL E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200..7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E900.1 11109107 '19:31 / bws 11109107 19:3't / bws 11109107 19:31 / bws 11l0gl07 19:31 / bws 11l0gl07 19:31 / bws 11l0gl07 19:31 / bws 11115107 16:52 / ts 11109107 19:31 / bws 1110910719;31 / bws 11l0gl07 19:31 / bws 11l0gl07 19:31 / bws 11109107 lg:31 / bws 11llgl07 19:31 / bws 11109107 19:31 / bws 11109107 19:31 / bws 11109107 19:31 / bws 11109107 19:31 / bws 11l0gl07 19:31 / bws 11109107 19:31 /bws 11116107 14:24 I crw Report Deflnltlons: RL, Analyte reporting limit. QCL - Quality control limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant level. ND - Not detec{ed at the reporting limit.t I -2-rFDaa!a4 rrl't11nn11 ENERCYLABORATORIES,INC .2SgSSaltCreekHiThway(8260t).PO. Boxl?fi , Casper, WY82602 TollFree888.235.05l5 , 307.f -0515 . Fax 307.234.16,39 " casper@energylab.q wwwehergytab.com I I I Client: Project: Lab lD: Glient Sample lD: LABORATORY ANALYTICAL REPORT Denison Mines (USA) Corp /' 4th Qtr Groundwater/Semi-Annual /co711oO77-OO1 /MWs / Report Date: 01/07/08 Collection Date: 101291O7 08:30 DateReceive d: 1 1 ll2tO7 Matrix: Aqueous Analyses TA QUALITY A/C Balance (r S) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 - 1.20) VOLATILE ORGANIC COMPOUNDS Quallfiers MCURL QCL MethodI tr, I -0.316 31.3 31.1 2040 0.920 o/o meq/L meq/L mg/L dec. % Calculation Calculation Calculation Calculation Calculation SW8260B SW826OB SW826OB SW826OB SW826OB sw8260B SW826OB SW826OB SW826OB SW826OB sv\82608 SW826OB sv\a2608 SW826OB SW826OB Analysis Date / By 111161p7 14:34 / bws '11116107 14:34 / bws 11116107 14:34 / bws 11116107 14:34 / bws 11116107 14:34 / bws 11105107 13:38 / dkh 11105107 13:38 / dkh 1 1/05/07'1 3:38 / dkh 11105107 13:38 / dkh 11105107 13:38 / dkh '11105107 13:38 / dkh 11105107 13:38 / dkh 11lOSl07 13:38 / dkh 11105107 13:38 / dkh 11105107 13:38 / dkh 11105107 13;38 / dkh 11105107 13:38 / dkh 11105107 13:38 / dkh 11105107 13:38 / dkh 11105107 13:38 / dkh I I I I I t T I T t T /Acetone f a"n."n" 1 Carbon tetrachloride / chloroform V Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Sun: 1,2-Dichlorobenzene-d4 Sun: Dibromofl uoromethane Sur: p-Bromofl uorobenzene Sun: ToluenedS ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L10 ug/L1.4 ugAND ug/L100 ToREC125 %REC111 %REC99.0 %REC 20 1.0 1.0 1.0 1.0 20 1.0 1.0 10 1.0 1.0 80-120 70-130 80-120 80-120 t Report Deftnltlons: RL.- Analyte reporting timit. QCL - Quality control timit. MCL - Maximum contaminant level. ND - Not detected at the reporting limit. -3-iFPAcra# ..al 11an'7'l t ENERGYLABonAToRtES,_tNC. .239ssattcre,gf ltlqQway(s2601).p.o. Boxs2sS , casper wse602rott Free 888.23i.0s15 " snzz' - nirc-. -Fi ibiiin. id1b ;'dlriiidriiisyE:i;i* ,r,,,;;;;;;s;LL.:*, I I LABORATORY ANALYTIGAL REPORT Glient: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual c07110077-013 MW 11 Report Date: 01/07l0g Collection Date: 10/30/07 14:10 DateReceived: 11102t02 Matrix: Aqueous MCURL QGL Method D D mg/L mg/L mglL mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L I t I I I I I Analyses IONS as CO3 Bicarbonate as HCO3 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Qualifiers ND 378 40.3 29 0.5 11.1 0.65 ND 7.5 580 1020 8.08 s.u. 1770 mg/L ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L 141 ug/LND ug/L80 ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ugA E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E900.1pCi/L 1 1 0.5 1 0.1 0.5 0.05 0.1 0.5 0.6 30 0.01 10 5.0 0.s0 0.50 25 10 10 30 1.0 10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 1.0 Analysis Date / By 12320 8 lltlit}Z l5:46 / bas423208 t1t}6t1715:46/bas8200.7 11t1il\7 18:46 / ts A4500-Cl B 11t07l\t 12:40 ttl44500-FC 11tOStO713:57lbasE200.7 11t1StO7 18:46 / ts A4500-NH3 c 11tO6tOZ 12:31 tjatE353.2 11tOAtO7 13:52 t jatE200.7 11t1SlOZ iB:46 / tsE200.7 11tlStOV t8:49 / ts A4500-SO4 E 11tO6tO7 12:58 t zd A4500-H B llt1ltlt 10:43 / rw 42540 C 11tOStO7 14:14 t tw ryI Potassium Sodium AurateI /rr"r,.o, pRopERrrES t/ o* Solids, Total Dissolved TDS @ lBO C METALS. DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper lron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc I /m:il[",hllli; D'|ssoLVED 11109107 21:40 I bws 11109107 21:40 t bws 11109107 21;40 / bws 11109107 21:40 / bws 11lO9lO7 21:40 tbws 11109107 21:40 tbws 11115107 18:46 / ts 11109107 21:40 tbws 11109107 21:40 tbvts 11109107 21:40 I bvts 11109107 21:40 / bws 11109107 21:40 tbws 11109107 21:40 / bws 11l09lll 21;40 / bws 11109107 21:40 tbws 11l0gl07 21:40 I bws 11109107 21:40 / bws 11l0gl07 21:40 / bws 11109107 21:40 t bws 11116107 16:02 t crw I I I I Report Definltions: RL - Analyte reporting limit. QCL - Quality controt limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant level. ND - Not detected at the reporting limit.I I -26- ENERGY'LABOBATORIEE lNC. . 2393 Saft Creek Hjghway (82601) . P.O. Box 3258 . Casper; W 82602 Toll Free 8fi.235.05/5 , 307.2:'"1515 , Fax 307.234.1639 , casper@energylab.mr 'vww.energylab.com LABORATORY ANALYTIGAL REPORTI T Client: Projeet: Lab lD: Client Sample lD: Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual c07110077-O1s MW 11 Report Date: Collection Date: DateReceived: Matrix: un7t08 10130107 14:10 11t02t07 Aqueous I Analyses Result Units Qualifiers RL MCU QCL Method Analysis Date / ByI I I I t I I I t I I T T DA/TA QUALITY {p Bahnce (r 5) y'nions . / CationsW solidr, Total Dissolved Catculated TDS Balance (0.80 - 1.20) VOLATILE ORGANIC COMPOUNDS Acetone 86nzene $arilon tetrachloride ,Dhloroform lchbromethanety/ Methyl ethyl ketone- Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Sun; 1,2-Dichlorobenzene-d4 Surr: Dibromofl uoromethane Sun: p-Bromofl uorobenzene Sun: Toluene-d8 0.131 % 28.3 meq/L 28.4 meq/L 1890 mg/L 0.940 dec. o/o ND ug/LND ug/LND ug/L ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LlU %REC128 %REC114 %REC100 %REC 20 1.0 1.0 1.0 1.0 20 1.0 1.0 10 1.0 1.0 80-120 7G.130 80-120 80-120 Calculation Galculation Calculation Calculation Calculation SW826OB SW826OB SW826OB SW826OB SW826OB SW826OB SW826OB SW8260B SW826OB st /82608 SW826OB sw8260B SW8260B SW826OB sw8260B 11116107 14:38 / bws 111161b714:38 / bws 11116107 14:38 / bws 11116107 14:38 / bws 11116107 14:38 / bws 11105107 22:50 / dkh 11105107 22:50I dkh 11105107 22:50ldkh 11lOSl07 22:50 t dkh 11lOSl07 22:50ldkh 11105107 22:50I dkh 11105107 22:50 I dkh 11105107 22:50ldkh lll05l0l 22:50I dkh 11105107 22:50 / dkh 11lO5lO7 22:50I dkh 11lOSl07 22:501 dkh 11105107 22:50I dkh 11105107 22:50I dkh 11105107 22:50I dkh Report Definltlons: RL - Analyte reporting limit. QCL - Quality control limit. MCL - Maximum contaminant level. ND - Not detec-ted at the reporting limit.t T -27 - TRACK# CO1LLOOl1 ENEnGy LABORATORIES, lNC. " 2393 Saft Creek HiThway (82601) , P.O. Box 3258 , Casper, W 82602To11Free888.235.0515,3022 '515 " Fax307.234.1639, casper@energylab.co 'uww:ehergytab.com t T I LABORATORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp / 4th Quarter/Semi-AnnualGroundwater /c07101341-006 / MW12 / Report Date: 01/07/08 Gollection Date: 10/23/07 14:22 DateReceive d: 10126107 Matrix: Aqueous Analyses Result Unlts Qualifiers RL MCU QCL Method Analysis Date / ByI I I I I I iae.lon torus / Carbonateas Co3 / Bicarbonate as HCO3/ c"t"irtt Y Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium METALS. DISSOLVED ND 439 524 58 0.2 224 ND ND 13.2 282 2290 7.30 s.u. 3800 mg/L ND ug/LND ug/LND ug/LND ug/LND ugAND ug/L68 ug/LND ug/L60 ug/LND ug/L ND ug/LND ug/L 10.7 ug/LND ug/L ND ug/LND ug/L19.2 ug/LND ug/L 10 ug/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L pCirL 1 1 0.5 1 0.1 0.5 0.05 0.1 0.5 0.5 30 0.01 10 5.0 0.50 0.50 25 10 '10 30 1.0 10 0.50 10 20 5.0 10 0.50 100 0.30 15 '10 1.0 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E900.1 423208 423208 E200.7 44500-Ct B A4500-F C E200.7 A45OO.NH3 G E353.2 E200.7 E200,7 A4500-SO4 E 11103107 12:08 / bas 1110310712;08 / bas 11106107 19:11 / ts 11t01107 15:04 t tjt 10131107 21:4Q lbas 11106101 19:11 / ts 11105107 10:08 / jal 10129107 09:20 / jat 11106107 19:08 / ts 1 1/06/07.19:08 / ts 11lOSlO7 13:07 lzd A4500-H B 1Ol27tO7 11:26 /.bas 42540 C 1Ot28lO7 13:43 / bas I T I ND I r/ Arsenic Beryllium :Cadmium Chromium Cobalt Copper lron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium 10131107 19:26 / bws 10131107 19:26 / bws 10131107 19:26 / bws 10131107 19:26 / bws 1Ol31lO7 19:26 / bws 10131107 19:26 / bws 11rc6rc719:08/ts 10131107 19:26 / bws 10131107 19:26 / bws 10131107 19:26 / bws 10131107 19:26 / bws 10131107 19:26 / bws 10131107 19:26 / bws 10131107 19:26 / bws 10131107 19:26 / bws 1Ol31lO7 19:26 / bws 10131107 19:26 / bws 10131107 19:26 / bws 1Ol31lO7 19:26 / bws 11113107 16:56 / env Vanadium Zinc RADIONUCLIDES . DISSOLVED Gross Alpha minus Rn & U t Report Definltlons: RL - Analge reporting limit. QCL - Quality control limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant level. ND - Not detected at the reporting limit.I I -L2-rFPAcra4 rnl 1 i1 ?A 1 ENERGY LABORATOBIES, lNC. , 2393 Salt Creek Hlqhway (SZ60t) . P.O. Box 3258 , Casper. W A2602 Toll Free 88t1.235.0515 " 307.2' 'rl5 , Fax 302234.1639 .'casper@energylab.cor r*vw.iheigylab.con T I Client: Project: Lab lD: Client Sample lD: LABORATORY ANALYTICAL REPORT Denison Mines (USA) Corp 4th Quarter/Semi-Annual Groundwate/-C07101341-OOO ,/ MW 12 ,/ Report Date: Collection Date: DateReceived: Matrix: 01t07t08 10123107 14:22 10t26t07 AqueousI t I T I I t I I I I T T T I T Result Unlts Qualifiers RL MCU QCL Method TA QUALITY A/C Balance (t 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 - 1.20) VOLATILE ORGANIG COMPOUNDS 0.623 56.5 57.2 3630 1.05 % meq/L meq/L mg/L dec. o/o Calculation Calculation Calculation Galculation Calculation Analysis Date / By 11107107 13:58 / bws 1110710713:58 / bws 11107107 13:58 / bws 11107107 13:58 / bws 11107107 13:58 / bws 10129107 17:32 t itr 10t29t07 17:32 t jk 10129107'17:32 t jtr 10r29n7 17:32ljtr 10129107 17:32 tjtr 10129t07 17:32 t jtr 10129107 17:32 tjtr 10129107 17:32 t itr 10129107 17:32 t itr 10129107 17:32 t itr 10129107 17:32 t itr 1ODgl07 17:321jtr 10129107 17:32 t jtr 10t29107 17:32 tjtr 10129107 17:32 tjk 4r,etone henzene I C",tontetrachloride / chtoroform / chloromethaneI u"il y ethyr ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Sun: 1,2-Dichlorobenzene-d4 Sun: Dibromofl uoromethane Sun: p-Bromofl uorobenzene Sun: Toluene.dS ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L ND ug/L ND ug/LND ug/LND ug/LND ug/L 1O1 o/oREC 1O2 o/oREC 1O4 o/oREC 100 %REC 20 1.0 1.0 1.0 1.0 20 1.0 1.0 10 1.0 1.0 80-120 70-130 80-120 80-120 SW826OB SW8260B SW826OB SW826OB SW8260B SW826OB SW826OB SW826OB SW826OB sw8260B sw8260B SW826OB sw8260B sWB26oB sw8260B Report Definitions: RL. Analyte reporting limit. QCL - Quality control limit. MCL - Maximum contaminant level. ND - Not detected at the reporting limit. - 13-|FPAr'ra# nn?1nt 2r1 ENEBGY LABORATORIES, lNC. , 2393 Salt Creek HlThway (82601) " PO. Box 32s8 . Casper W A2602 Toll Free 888.235.0515 , 307.? ' 0515 " Fax 3022a4.1639 ,'cisper@energylab.ct www.eheigytab.con I I LABOMTORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual c07110077-003 MW 14 Report Date: 01/07/08 Collection Date: 10129107 13:2i DateReceive d: 1 1 l02l0l Matrix: AqueousI Analyses Result Units Qualifiers RL MCU QCL Method mg/L mg& mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L METALS. DISSOLVED Arsenic Beryllium Cadmium /chromium /courtt / "orr",/ IronIi;l Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc I I I I I I I I t I I Analysis Date / By tyAJoR toNS rtarbonateas CO3 /Bicarbonate as HCO3/ c^t"irn,. / ctrtoriaeI Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium ND 474 520 18 0.2 158 0.05 ND 11.9 302 2180 7.03 s.u. 3490 mg/L ND ug/LND ug/L0.89 ug/LND ug/LND ug/LND udLND ug/LND ug/L 2120 ug/LND ug/LND ug/LND ug/LND ug/LND ug/L ND ug/LND ug/L68.6 ug/LND ug/L10 ug/L ND pCilL 1 1 0.5 1 0.1 0.5 0.05 0.1 0.5 "0.5 30 0.01 10 5.0 0.s0 0.50 25 10 10 30 1.0 10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 1.0 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E900.1 AA320B A232OB E200.7 44500-Ct B A450&.F C E200.7 A45OO.NH3 G E353.2 E200.7 E200.7 44500-so4 E 11106107 02:56 / bas 11lOOl07 02:56 / bas 11115107 17:23 tts 11107107 10:23 t lil 11105107 13;12 / bas 11115107 17:23lts 11106107 12:05 tjat 11108107 13:15 t jat 11115107 17:19 / ts 11115107 17:19 / ts 11106107 11:55 I zd Solids, Total Dissotved TDS @ 1BO C 44500-H B 11l0StO7 IOiZB t rw 42540 C llt}St}t 14:11 t rw ; / s3J:ixx"'.','if '-; DrssoLVED 11109107 19:44 / bws 11109107 19:44 / bws 11109107 19:44 / bws 11109107 19:44 / bws 11109107 19:44 / bws 11109107 19:44 / bws 11115107 17:'19 / ts 11109107 19:44 t bws 11109107 19:44 / bws 11109107 19:44 / bws 11109107 19:44 / bws 11109107 19:44 / bws 11109107 19:44 / bws 11109107 19:44 / bws 11109107 19:44 / bws 11l0gl07 19:44 / bws 11109107 19:44 / bws 11109107 19:44 / bws 11109107 19:44 / bws 11116107 14:24 I crw I Report Definitlons: RL - Analyte reporting limit.. QCL - Quality control limit. D - RL increased due to sample matrlx lnterference. MCL - Maximum contaminant tevel. ND - Not detected at the repoffng limit.t I -5- TRACK# CA7LLOO77 ENERCY LABORATOBIES, lNC. . 2393 Saft Creek Hfighway (52601) , PO. Box 32i8 , Caspet W 82602TollFreefi8.295.05l5,30Z? 7515 " Fax302234.1639, casper@energylab.a wvwehergylab.mn LABOMTORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sampte lD: Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual c071 10077-003 MW 14 Report Date: 01/07/08 Collection Date: 10129t07 13:25 DateReceived: 1 1 102107 Matrix: Aqueous Result Unlts % meq/L meq/L mg/L dec. o/o Quallfiers RL MCU QCL Method TA QUALITY A/C Balance (r 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 - 1.20) vorrATtLE oRGAN|C COMPOUNDS Ace{one Behzene rbon tetrachloride -1.04 53.6 52.s 3430 1.02 Calculation Calculation Calculation Calculation Calculation Analysis Date / By 11116107 14:35 / bws 11116107 14:35 / bws 11116107 14:35 / bws 11116107 14:35 / bws 11116107 14:35 / bws ND ug/L 20 sw826OB 11t0510714:56 / dkhND ug/L 1 .O SW826OB lll}Stot t 4:56 / dkhgarbon tetrachloride ND ug/L 1.0 sw826oB llroirov 14:56 / dkhdhloroform ND ug/L 1.0 sw826oB 11tosroz14:56 / dkhIGhloromethane ND ug/L 1.0 sw826oB 11rostoz 14:56 / dkhMethyl ethyl ketone ND ug/t 20 sw826oB 1lrostor 14:s6 / dkhMethylene chloride ND ug/L 1.0 s\ /82608 11tosro714:s6 / dkhNaphthalene ND ug/L 1.0 sw826oB 1lrosroz 14:s6 / dkhTetrahydrofuran ND ug/L ro sw826oB 11rosror 14:56 / dkhToluene ND ug/L 1.0 sw826oB 11rostor l4:s6 / dkhXylenes, Total ND ug/L 1.0 sw826oB 11t05t0714:56 / dkhsun:1'2-Dichlorobenzene-d4 105 %REc BG12o sw826oB 11tosroz14:56/dkhSun: Dibromofluoromethane B2 %REC S 70-130 SWB26OB 1,ltOSlOl14:56 / dkhsurr: p-Bromofluorobenzene 1$ %REc 80-120 svv826oB 11tosro714:56 / dkhsurr: Toluene'd8 98.0 %REc 80-120 sw,26oB 11rosror 14:56 / dkh-sunwate response Is above standard QA limit rhis could indicate a high bias for the sample resutb. since there were no detectable analyte rcsponses,and the remainder of the run QA is witrin acceptance range, thrs batch r"-"pprri,J -- - Report Definltions: RL - Analyte reporting timit. QCL - Quality control limit. S - Spike recovery outside of advisory limits. MCL - Maximum contaminant level: ND - Not detected at the reporting limit. -7-TRACK# eo711oo77 I ENERGY LABOilATORI-ES, lNC '-239Q Saft Cre9( H!7-Qway (s2601) . PO. Box S2SB , Caspet Wa2602Toll Free 888.235.0i1i . s07.,. ' 05ti . Fax a02.2a4. tobs .biipiiaienergytai.b:--- *,*.iiibiirb.ro, I I LABOMTORY ANALYTICAL REPORT Client Denison Mines (USA) CorpProject 4th etr Groundwater/S emi,Annuat /Lab lD: CO711OOZ7-OO2 /ClientSampletD: MWIS / Report Date: OilAtfig Collection Date: 1Ol29t0Z 10:51 DateReceive d: 1 1 tl2tO7 Matrix: Aqueoust Analyses Result Units Quallfiers RL MCUQCL MethodI I I I I I I I MAJOR IONS parbonate as CO3 /Bicarbonate as HCO3/ Calcium / ctrtoriaeI V Ftuoride' Magnesium Nitrogen, Ammonla as N. Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate I /envsrcel pRopERTtES lpn y/ Sorio., Totat Dissotved TDS @ METALS - DISSOLVED Arsenic Beryllium Cpdmium Ohromium /cot^tt/ copper V lron Lead 180 C 1 1 0.5 1 0.1 0.5 0.05 0.1 0.5 0.5 30 0.01 10 5.0 0.50 0.50 25 10 10 30 1.0 10 0,s0 10 20 5.0 10 0.50 100 0.30 15 10 1.0 ND 454 440 36 0.2 165 ND 0.1 10.6 457 23/;0 7.21 s.u. 3660 mg/L ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L94.0 ug/LND ug/LND ug/LND ug/L51.0 ug/LND ugtrND ug/L E200.8 E200.8 E200.S E200.8 E200.8 E200.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E900.1 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L PA320B 11lO6tOZ 02:49 tbas A2320 B 11tO6tOZ 02:49 t basE200.7 11t15t0717:16 / ts 44500-Cl B 11to7t|t 10:18 iljt 44500-F C lllOStOZ i3:10 / basE200.7 11t15t1t.t7:16 / ts A4500-NH3 G 11tO6tOZ 12:04 tjatE353.2 lltOBtOZ 13:12 t jatE200.7 11t1StO7 1t:12 t tsE200.7 |1t11lot 17:12 tts A4500-SO4 E 11t}6t1z 11:54 t zd 44500-H B llt}Stlt i0:27 I rwA254OC 11lOSlO7 14:11 trw ManganeseI il:r;;n",* Selenium T iiF;,I ffi::,T,I lzinc I I / HJ:ilX"'*l?ii; DrssoLVED pCi/L 11l1gll7 19:38 / bws 11109107 19:38 / bws 11l1gt07 19:38 / bws 11109107 19:38 / bws 11109107 19:38 / bws 11109107 19:38 / bws 11115107 1t:12 t ts 11109107 19:38 / bws 11109107 19:38 / bws 11109107 19:38 / bws 11109107 19;38 / bws 11109107 19:38 / bws 11l0gl07 19:38 / bws 11109107 19:38 / bws 11109107 19:38 / bws 11109107 19:38 / bws 1110910719:38 / bws 11109t07 19;38 / bws 11109107 19:38 / bws 11116107 14:24 I ctw I Analysis Date / By Report Definltions: RL - Analyte reporting limit. QCL - Quality control limit. MCL - Maximum contaminant level. ND - Not detected at the reporting limit.T I -4- TRACK# CO7110077 D - RL increased due to sample matrix interfercnce- T ENERGY LABORATOilE-9, INC ' 2393 Salt Creek Highway (52601) . PO. Box i2S8 , Casper WyAz602TottFreeaffi.23i.a,t5 "snzr -lits .Faxs0zfia.i63i :r;;i;;6";;6rh;;***;r;tr;b;Lb.*, t I LABORATORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual c07110077-002 MW 15 Report Date: 01107t09 Collection Date: 10/29i07 10:Sl DateReceive d: 1 1 t02tO7 Matrix: Aqueous MCURL QCL Method I T I I I I t I I I t T T T Analyses TA QUALITY Balance (r S) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 - 1.20) VOLATILE ORGANIC COMPOUNDS Qualifiers -1.30 57.2 55.7 3690 0.990 o/o meq/L meq/L mg/L dec. o/o Calculation Calculation Calculation Calculation Calculation SW826OB SW8260B SW826OB SW826OB SW826OB SW826OB SW826OB sw8260B SW826OB SW826OB SW826OB SW826OB SW826OB sw8260B SW826OB Analysis Date / By 11116107 14;35 / bws 11t16i07 14:35 / bws 11116107 14:3S / bws 1'll16to7 14:35 / bws 11116107 14:35 / bws 11105107 14:17 t dkh lllOSlOZ 14:12 t dkh 11105107.14:12 tdkh 11105107 14:17 ldkh 11105107 14:17 I dkh 11lO5lO7 14:11 I dkh 11105107 14:17 I dkh 11lOSlO7 14:11 tdkh 11105107 14:12 I dkh 11105107 14:17 I dhh 11lOSlO7 14:11 t dkh 11105107 14:1t t dkh 11t05107 14:11 I dkh 11105107 14:17 I dkh 11105107 14:17 tdkh Acgtone Blnzene farAontetrachloride /chlorotorm 1,/ chloromethanev Methyr ethyr ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Sun: 1,2-Dichlorobenzene_d4 Sun: Dibromofluoromethane Sun: p-Bromofl uorobenzene Sun; Toluenedg ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND uglLND ug/LND ug/L103 o/oREC 127 %REC116 %REC100 %REC 20 1.0 1.0 1.0 1.0 20 1.0 1.0 10 1.0 1.0 80-120 70-130 80-120 80-120 Report Definltions: RL . Analyte reporting limit. QCL - Quality control limit. MCL - Maximum contaminant level. ND - Not detected at the reporting limit.t t -5-rRACK# eO7110077 I ENERGY LABORAT0R!^Eji2 tNC .,_239! satt Qr99( Hyg-lway (s260t) " p.o. Box 3pi8 . caspq wy82602TollFree888.235.05/s, a0z.? 'tsts ,Fax302.234.fi3s. c;sper@enerwtai."i' -www.iiiigiiab.:@, I I LABORATORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual c07110077-OO4 MW17 Report Date: 01107108 Gollection Date: 10t29101 15:40 DateReceived: 1 1 l02l07 Matrix: AgueousI Analyses Result Units Qualifiers RL MCU QCL Method D D I I I I I I I t T I t I t Analysis Date / By MAJOR IONS drbonate as Co3 ficarbonate as HCO3 /c^t"iu.,./ cnnna" 11/ ruoriae' Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N ND mg/L521 mg/L37'l mg/L28 mg/L0.3 mg/L 188 mg/LND mg/L0.4 mg/L13.0 mg/L624 mg/L 2510 mg/L 7.07 s.u. 3980 mg/L ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L73 ug/LND ug/LND ug/t ND ug/L5.4 ug/LND ug/LND ug/LND ug/L31.0 ug/LND ug/LND ug/L 1 1 0.5 1 0.1 0.5 0.05 0.1 0.5 0.6 30 0.01 10 5.0 0.50 0.50 25 't0 10 30 1.0 10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 1.0 AQ32OB pc320B E200.7 44500-Ct B 44500-F C E200.7 A45OO.NH3 G E353.2 E200.7 E200.7 44500-S04 E 11106107 03:04 / bas 11106107 03:04 / bas 11115107 17:29 tts 11107107 10:30 / tjt 11105107 13:15 / bas 11115107 17:29 tts 11lOOl07 12:14 tjat 11lOBl07 13:25 t jat 11115107 17:26 lts 11115107_17:29 tts 11106107 11:58 tzd Pbtassium odium ulfate PHYSICAL PROPERTIES pH Solids, Total Dissolved TDS @ lBO C METALS. DTSSOLVED Arsenic $eryllium 6admium /chromiu,/ coaatl/ copp", lron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium r llniI Uranium I Vanadium \ zin" IIJ RADIONUCLIDES. DTSSOLVED Gross Alpha minus Rn & U A4500-H B 11t0StO7 10:29 trw A2540 C 11t0StOZ 14:12 t ruv ND pCi/L E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E900.1 11l1gl07 20:05 / bws 11llgl07 20:05 / bws 11l1gl07 20:05 / bws 11109107 20:05 / bws 11109107 20:05 / bws 11109107 20:05 / bws 11115107 17:26 I ts 11l0gl07 20:05 / bws 11109107 20:05 / bws 11l0gl07 20:05 / bws 11109107 20:05 / bws 11/09/07 20:05 / bws 11109107 20:05 / bws 11109107 20:05 / bws 11109107 20:05 / bws lll0gl0l 20:08 / bws 11109107 20:05 / bws 11l0glo7 20:05 / bws 11109107 20:05 / bws 11116107 14:24 I crw Report Definltions: RL - Analyte reporting limit. QCL - Quality control limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant level. ND - Not detected at the reporting limit.t T -8- TRACK# C07110077 ENERGY L/IBORATOHEA NC. . 2393 Salt Creek Hishway (A260t) . pO. Box SpiB . Casper. Wy A2602TollFree888.235.05l5 ' 307.2 1515 , Fax 307.234.1639 ,'casper@energylab.u rtww.eieigytab.con t T LABORATORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sampte lD: Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual c07110077-o04 MW 17 Report Daie: 01t07t08 Collection Date: 10t29t07 15:4A DateReceived: 1 1 102107 Matrix: Aqueous MCU QCL Method I I I I t t I T t t t I I T Result Units Quallfiers RL TA QUALITY Balance (r 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 - 1.20) VOLATILE ORGANIC COMPOUNDS -0.155 61.7 61.5 4000 1.00 o/o meq/L meq/L mg/L dec. % Calculation Calculation Calculation Calculation Calculation SW826OB SW826OB SW826OB SW826OB SW826OB sw8260B sw8260B SW826OB sv\a2608 SW826OB SW8260B SW826OB sv\r82608 SW826OB sw8260B Analysis Date / By 11116101 14:35 / bws 11116107 14:35 / bws 11116107 14:35 / bws 11116107 14:3S / bws 11116107 14:35 / bws 11105107 15:36 / dkh 11105t07 15:36 / dkh '11105/07.15:36 / dkh 11105107 15:36 / dkh 11105t07 15:36 / dkh 11105107 15:36 / dkh 11105107 '15:36 / dkh 11lOSl07 '15:36 / dkh 11105107 15:36 / dkh 11lOSl07 15:36 / dkh 11105107 15:36 / dkh 11105107 15:36 / dkh 11lOSl07 15:36 / dkh 11105107 15:36 / dkh 11105107 15:36 / dkh Acetone f"nr"n" /Carbon tetrachloride /chloroform,y/ Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surr 1,2-Dichlorobenzened4 Surr: Dibromofl uoromethane Sun: p-Bromofluorobenzene Sun: Toluene-d8 ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L103 o/oREC 129 %REC118 %REC98.0 %REC 20 1.0 1.0 1.0 1.0 20 1.0 1.0 10 1.0 1.0 80-'t20 70-130 80-120 80-120 Report Definitions: RL - Analyte reporting limit, QCL - Quality control limit. MCL - Maximum contaminant level. ND - Not detected at the reporting limit.T T -9- TRACK# C07LLO077 ENERGY LABORATORIES, lNC. , 2393 Salt Creek Htjghway (82601) . PO. Box 32.q8 . Cas@r, W82602 TollFree888.235.05l5 , 307.2' 1515 ' Fax 307.234.1639 , casper@energylab.m vww:energylab.com LABORATORY ANALYTICAL REPORTI I Glient: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp / 4th Qtr Groundwater/Semi-Annual /co711oo77-oo6 /MW18 v Report Date: 01/07/08 Collection Date: 10/30/07 10:50 DateReceived: 1 1 lo2l07 Matrix: Aqueous I Analyses Result Units Qualifiers RL MCU QCL Method Analysis Date I By mg/L mg/L mg/L mg/L mg/L mg/L mga mg/L mg/L mg/L mg/L I I t I I MAJOR IONS Carbonate as CO3 /icarbonate as HCO3 /c.t iu^ / ctrtorioeI Ftuoriae V Magnesium ND 429 501 48 0.2 104 0.17 ND 9.5 196 1700 7.03 s.u. 2840 mg/L ND ug/LND ug/LND ug/LND ug/LND ug/L ND ug/L 509 ug/LND ug/L219 ug/LND ug/L ND ug/LND ugAND ug/LND ug/L 0.89 ug/LND ug/L39.2 ug/LND ug/L 19 ug/L 1.7 0.6 A232OB 423208 E200.7 44500-Ct B A4500-F C E200.7 A45OO-NH3 G E353.2 E200.7 8200.7 A4500-SO4 E A4500-H B A2540 C E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E900.1 E900.1 1'1106107 11:30 / bas '11106107 11:30 / bas 11l15lOZ 17:52 tts 11107107 10:41 il1t 11105107 13:20 tbas 11115107 17:49 tts 11106107 12:17 ljat 11108107 13:30 / jat 'l1l15lo7 17:49 tts 11115107 17:49 I ts 11106107 12:03 lzd 11105107 10:31 / rw 11105107 14:12 I rw 11109107 20:39 / bws 1'll0gl07 20:39 / bws 11l09lll 20:39 / bws 11ligl07 20:39 / bws 11109107 20:39 / bws 11109107 20:39 / bws 11115107 17:49 lts 11109107 20:39 / bws 11109107 20:39 / bws 11l0gl07 20:39 / bws 11l0gl07 20:39 / bws 11l0gl07 20:39 / bws 11l09lOZ 20:39 / bws 11109107 20:39 / bws 11/09/07 20:39 / bws 1'llOglOT 20:39 / bws 11109107 20:39 / bws 11109107 20:39 / bws 11109107 20:39 I bws 11116107 14:24 I crw 11116107 14:24 I crw 1 1 0.5 1 0.1 0.5 0.05 0.1 0.5 0.5 30 0.01 10 5.0 0.50 0.50 25 10 10 30 1.0 10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 1.0 Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium ,Sulfate PHYSICAL PROPERTIES pH Solids, Total Dissolved TDS @ 180 C I 1*="r*o - DrssoLVED Berylliumr fi:;"jr;ffi / copp", l,/ H.f Manganese T ilffi* SeleniumI iiFr, Uranium I vanadium pCi/L pCitL rJ I RADIONUCLIDES . DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (r) Report Deflnitions: RL - Analyte reporting limit. QCL - Quality control limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant level. ND - Not detected at the reporting limit.I I -L2-.IPACT<# r.nTt 1nn7? ENERGY LABoRAroqlE_q.NC.,_239s saft qrqg\ Hlg-hway (a2601) . p.o. Box s2<4 . caspq wya2602TollFreeffi9.21i.2sts . a02.2' 15t5, Faxs0Z2a4.ff3e.biiwdenergytaici. ,r*.iiiibiiro.o, T I I LABORATORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual c071 10077-006 MW 18 Report Date: 01/07/0g Collection Date: 10/30/07 10:S0 DateReceived: fifi2t07 Matrix: Agueous Analyses Result Unlts Qualiflers RL MCU QCL MethodI T flere oualrw y'/C Batance (r s) ^ /Anion. \r/ c"tio* Solids, Total Dissolved Calculated -1.77 o/o 43.9 meq/L42.3 meq/L 2780 mg/L 1.O2 dec. Vo ND ug/LND ug/LND ugAND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ugAND ug/L104 %REC128 ToREC116 %REC99.0 %REC Methyl ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofl uoromethane Sun: p-Bromofluorobenzene Sun: Toluene-d8 20 1.0 1.0 1.0 1.0 20 1.0 1.0 10 1.0 1.0 80-120 70-130 80-120 8o-120 Calculation Calculation Calculation Calculation Calculation sw8260B SW826OB sw8260B SW8260B SW826OB SW826OB SW8260B SW826OB sw8260B SW826OB SW826OB SW826OB sua260B SW826OB SWE26OB 11116107 14:37 / bws 11116t07 14:37 lbws 11116107 14:37 / bws 11116107 14:37 / bws 11116107 14:S7 / bws 11105107 16:54 / dkh 11105107 16:54 / dkh 1 1/05/0716:54 / dkh 11lOSl07 16:54 / dkh 11lOSl07 16:54 / dkh 11105107 16:54 / dkh 11105107 16:54 / dkh 11105107 16:54 / dkh 11105t07 16:54 / dkh 11lOSl07 16:54 / dkh 11105107 16:54/dkh 11105107 16:54 / dkh 11105107 16:54 / dkh 11105107 16:54 / dkh 11105107 16:54 / dkh T t t t t t T t t Analysis Date / By RL - Analyte reporting limit. QCL - Quality control limit. MCL - Maximum contaminant level. ND - Not detected at the reporting limit.T I -13_ TRACK# CO7110077 ENERGY LABORATORIES, ltlC. " 2393 Salt Creek Highway (5260A , P.O. Box 32c8 , Casper WyA2602 TollFree888.235.05l5 , 307.2' t5l5 , Fax 307.234.1639 ,-casper@energytab.a awueher!1ylab.mn LABOMTORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample tD: Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual c07110077-005 MW 19 Report Date: 01/07/08 Collection Date: 10/30/07 08:35 DateReceive d: 1 1 lO2l07 Matrix: Aqueous Analyses Result Unlts Qualifiers RL MCUQCL Method Analysis Date / By MAJOR IONS C/rbonate as CO3 #carbonate as HCO3 6alcium /ctrtorioe r / Fluoride V Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium ND 270 140 26 1.1 46.5 ND 2.4 5.0 121 509 7.54 s.u.982 mg/L ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ugA10.8 ug/LND ug/L0.52 ug/LND "ug/L7.53 ug/LND ug/LND ug/L 1 1 0.5 mg/L mga mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L pCi/L 1 0.1 0.5 0.05 0.1 0.5 0.5 10 0.01 10 5.0 0.50 0.50 25 10 10 30 1.0 10 0.50 10 20 5.0 10 0.50 100 0.30 l5 10 1.0 E200.8 E200.8 E200.8 E2oO.8 E200.8 E200.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E900.1 423208 423208 E200.7 44500-CtB A4500-F c E200.7 A45OO-NH3 G E353.2 E200.7 E200.7 44500-so4 E 11128107 14:07 lbas 11128107 14:07 tbas 11115107 17:42 tts 11107t07 10:34ltjt 11105107 13:18 / bas 11115107 17:42 I ts 11106107 12:15 t jat 11108107 13:27 tjat 11115107 17:42 tts 11115107 .17:42 fts 11106107 12:O4 t zd Solids, Total Dissolved TDS @ 1gO C A4500-H B 11l0StO7 10:30/rw 42540 C 11t0StO7 14:12 I rw METALS. DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt Copper lron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc MDIONUCLIDES . DISSOLVED Gross Alpha minus Rn & U 11l0gl07 20:12 t bws 11lO9lO7 20:12 tbws 11109107 20:12 / bws 11109107 20:12 / bws 11llgl07 20:12 tbvts 11109107 20:12 / bws 11115107 17:42 t ts 11l0gl07 20:12 tbws 11109107 20:12 / bws 11109107 20:12 t bws 11109107 20:12 lbws 11logl07 20:12 tbws 11109107 20:12 tbws 11109107 20:12 tbws 11109107 20:12 t bws 11l0gl07 20:12 I bws 11l0gl07 20:12 tbws 11109107 20:12 I bws 11109107 20:12 I bws 11116107 14:24 I cwv Report Deftnitions: RL - Analyte reporting limit. QCL - Quality control limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant level. ND - Not detected at the reporting limit. H - Analysis performed past recommended holding time. - 10- rRAcK# c07t]-0077 ENEBGYLAB0RAT0RI^E9,.1NC ,2sgisattcreekHlqhway(s2601).p.o. BoxSpca . caspet; ws260zTollFree@8.235.0515 , 307.1' 1515 , Fax 30Z234.tObS ,'cisperdenergytai.ci vww.iiiigyAO.con I I Client: Project: Lab lD: Client Sample lD: LABORATORY ANALYTICAL REPORT Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annyaf c07110077-005 ,/ MW le t/ Report Date: 01/07/08 Collection Date: 10/30/07 0g:35 DateReceive d: 1 1 t02t07 Matrix: Aqueous MCU QCL Method I I t I I I t I I t I I T t Result Units Qualifierc RL TA QUALITY Balance (t 5) Cations Solids, Total Dissolved Calculated TDS Balance (0.S0 - i.2O) .VOLATILE ORGANIC COMPOUNDS I Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surr: 1,2-Dichlorobenzene{4 Sun: Dibromofl uoromethane Sun: p-Bromofl uorobenzene Sun: Toluene-d8 0.709 16.0 16.2 1 000 0.980 o/o meq/L meq/L mg/L dec. o/o Calculation Calculation Calculation Calculation Calculation sw8260B SW826OB sw8260B sw8260B SW826OB SW826OB sw8260B sw8260B sw8260B sw8260B SW826OB SW826OB SW826OB SW826OB SW8260B Analysis Date / By 1112910713:0S / bws 1112910713:05 / bws 11129107 13:05 / bws 11129107 13:05 / bws 11129107 13:05 / bws 1110510716:15 / dkh 11105107 16:15 / dkh 1 1/05/07-16:15 / dkh 11105107'16:1S / dkh 'l1l11l07 16:1S / dkh 11105107 16:1S / dkh 11105107 16:18 / dkh 11105107 16:15 / dkh 11105107 16:1S / dkh 11lOSl07 16:tS / dkh 11105107 16:15 / dkh 11105t07 16:15 / dkh 11105107 16:15 / dkh 11105107 16:1S / dkh 11lO5lO7 16:1S / dkh ND ug/LND ug/LND ug/LND ug/LND ug/LND ugAND ug/LND ug/LND ug/LND ug/LND ug/L102 %REC127 %REC115 %REC97.0 %REC 20 1.0 1.0 1.0 1.0 20 1.0 1.0 10 1.0 1.0 8G.120 70-130 8G120 80-120 Report Deflnltlons: RL - Analyte reporting limit. QCL - Quality control limit. MCL - Maximum contaminant level. ND - Not detected at the reporting limit. T T _1 1_ TRACK# CO7LLOOT7 ENERQY LABOEATORIE_S, ltlc ._2i9s saft creek H@hway (a2601) . po. Box J2i8 , caspec wya2602TottFree&&g.2?5.2sti , azze 'iff .Fax30z.2l4.ds :-cAipeidriirsyt.d:l;.:r;:--.r,*i;;;;;giirb.:*, I I t LABOMTORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp ./ 4th Quarter/Semi-Annual Groundwaler,/co71o1s41-005 /MW23 / Report Date: Collection Date: DateReceived: Matrix: 01t07to} 1Al23lO7 12:45 10t26t07 Aqueous Analyses Result Units Qualifiers RL MCU QCL Methodt I IONS as CO3 as HCO3 ND 162 475 7 0.2 164 ND 0.3 11.1 343 2310 1 1 0.5 1 0.1 0.5 0.05 0.1 0.5 0.5 30 0.01 10 5.0 0.50 0.50 25 10 10 30 1.0 10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 1.0 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L A232OB A232OB E200.7 A4500-ctB 44500-F C E200.7 A45OO-NH3 G E353.2 E200.7 E200.7 44500-so4 E 11102107 22:32 I bas 1110A07 22:32 t bas 11106107 19:04 / ts 11t01107 14:59 iljt 10131107 21:37 lbas 11106107 19:04 / ts 1110510710:06 / jat 10129107 09:17 ljat 11106107 19:01 / ts 11106107 19:01 / ts 11105107 13:06 tzd 6.94 3520 s.u. mS/L A4500-H B 10t2il07 11:23lbas 42540 C 10t2BtO7 13:42 lbas I T I T I I [T#t'DrssoLVED Beryllium Cadmium Cfrombm Qbbaltpopper hron /rc.a 1r/ Mrng"n"." Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc I ffJ:ilff*,',',:'*; l',i'o"=' / Gross Alpha minus Rn & U precision (*) T ND ug/LND ug/LND ug/LND ug/LND uS/LND ug/LND ug/LND ugA337 ug/LND ug/L ND ug/LND ug/LND ug/LND ug/L1.24 ug/LND ug/L19.6 ug/LND ug/L 41 ug/L 1.3 0.5 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200,8 E900.1 E900.1 1Ol31lO7 19:19 / bws 10131107 19:19 / bws ,10131107 19:19 / bws 10131107 19:19 / bws 10131107 19:19 / bws 10131107 19:19 / bws 11106107'19:01 / ts 10131107 19:i9 / bws 1Ol31lO7 19:19 / bws 1Ol31lO7 19:19 / bws 10131107 19:19 / bws 10l31l0l 19:19 / bws 10131107 19:19 / bws 10131107 19:19 / bws 10131107 19:19 / bws 1Ol31lO7 19:19 / bws 10l31l0l 19:19 / bws 10131107 19:19 / bws 10l31l1l 19:19 / bws 11113107 16:56 / qw 11113107 16:56 / cnr pCi.tL pCi/L Analysis Date / By Report Definltlons: RL - Analyte reporting limit. QCL - Quality control limit. D - RL inceased due to sample matrix interference. MCL - Maximum contaminant level. ND - Not detected at the reporting limit.I I _ 10_ TRACK# C071 n1 ?41 ENEROY LABORATORIES, lNC. . 2393 Salt Creek Hrghway (82601) . PO. Box 3258 . Caspet; WY A2602 Toll Free 888.235.0515 , 307.2 '515 , Fax e07.234.1639 , casper@energylab.cot 'ww.ehergytab.com I I T LABORATORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp /4th Quarter/Semi-Annual Groundwater /c07101341-Oo5 /MW23 v Report Date: 01107108 Collection Date: 10/23107 12:45 DateReceived: 10126107 Matrix: Aqueous Analyses TA QUALITY Balance (* 5) Cations Solids, Total Dissolved Calculated Methyl ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Sun: 1,2-Dichlorobenzened4 Sun: Dibromofl uoromethane Sur: p-Bromofl uorobenzene Sur: ToluenedS Qualifiers MCURL QCL MethodI I 1.29 51.1 52.4 3410 1.03 o/o meq/L meq/L mg/L dec. To Calculation Calculation Calculation Calculation Calculation SW8260B SW8260B SW826OB SW826OB SW826OB SW826OB SW826OB SW8260B sw8260B SW826OB SW826OB SW826OB SW8260B SW826OB sw8260B Analysis Date / By 11107107 13:58 / bws 11107107 13:58 / bws 11107107 13:58 / bws 11107107 13:58 / bws 11107107 13:58 / bws 'lill29l07 16:54 tjtr 10Dgt07 16:54 tjtr 10129107"16:54 I itr 10129107 16:54 tjtr 10129107 16:54ljlr 10l29lol 16:54 ljlr 10129107 16:54 t ik 10t29107 16:54 t ik 10129107 16:541jlr 1ol29l|l 16:54 / jlr 10129107 16:54 titr 10129107 16:54 tik 10129107 16:54ljtr 10129107 16:54 / jlr 10t29t07 16:54lilr I I t I I I I T T ND ug/L ND ugAND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ugAND ug/L ND ugA99.0 o/oREC 96.0 %REC101 %REC101 ToREC 20 1.0 1.0 1.0 't.0 20 1.0 1.0 10 1.0 1.0 80-120 70-130 80-120 80-120 Report Deflnitions: RL - Analyte reporting limit. QCL - Quality control limit. MCL - Maximum contaminant level. ND - Not detected at the reporting limit.t T - 11-,T'RACK# Cn71n1?41 ENEBGY L/IBORATOR-IE_9t INC '_2393 Satt Creek Hrghway (5260t) . PO. Box 32i8 . Casper, W A2602Tol Free 8o8.23s.0its . soz.{ 75ts . Fax 907.234.16b9 .'cisperGienergylab.q- - wn+y.iiiieiiao.bon I I t LABORATORY ANALYTIGAL REPORT Client: Project: Lab lD: Client Sample !D: Denison Mines (USA) Corp 4th Quarter/Semi-Annual Groundwater c07101341-003 MW 24 Report Date: 01/07/08 Collection Date: 10123t07 08:05 DateReceived: 10126t07 Matrix: Aqueous Analyses Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Result Units Qualifiers MCURL QCL MethodI I I I t T ND 300 509 45 0.1 183 0.86 ND 14.5 495 2620 6.97 s.u. 4180 mg/L ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L 2320 ug/LND ug/L 2770 ug/LND ug/l- ND ug/LND ug/LND ug/LND ug/L ND ug/LND ug/L 1.78 ug/LND ug/LND ugtr mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L pCi/L 1 1 0.5 1 0.1 0.5 0.05 0.1 0.5 0.6 30 0.01 10 5.0 0.50 0.50 25 10 10 30 1.0 ',0 0.50 10 20 5.0 10 0.50 100 0.30 15 't0 1.0 E200.8 E200.8 E200.8 E200.8 E200.8 E2oO.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E900.1 D D 42320 B PA320B E200.7 A4500-CtB A4s00-F c E200.7 A45OO-NH3 G E353.2 E200.7 E200.7 A4500-so4 E Analysis Date / By 11102107 22:1Q lbas 'nl0il07 22:10 tbas 11106107 18:34 / ts 11101107 14:29 iljt 10131107 21:16 / bas 11106107 18:34 / ts 11lOSl07 10:02 t jat 10129107 09:12 tjat 11lOOl07 18:31 /ts 1 1/06/07.18:34 / ts 11105107 12:53 lzd$ulfate I /puysrclr- pRopERTTES lrn / Sotior, Totat Dissotved TDS @ l8o C METALS. DISSOLVED Arsenic A4500-H B 10l27t!t 11:20 tbas n2540 C 10128t07 13:42 t bas BdrvlliumI E;m'* /couatt l/[i:" Manganeset ilff;n,,* Nickel I *T; TinI Y;::il', 10131107 19:06 / bws 1Ol31lOZ 19:06 / bws 1Ol31lO7 19:06 / bws 10131107 19:06 / bws 10131107 19:06 / bws 10131107 19:06 / bws 11lOOl07 18:31 / ts 10131107 19:06 / bws 1Ol31lO7 19:06 / bws '|.0131107 19:06 / bws 10131107 19:06 / bws 10131107 19:06 / bws 10131107 19:06 / bws 10131107 19:06 / bws 10131107 19:06 / bws 10131107 19:06 / bws 10131107 19;06 / bws 10131107 19:06 / bws 10131107 19:06 / bws 11113107 16:56 / crwI ffiJ?ilr'"',','.',!i; DrssoLVED 'll' Report Definltions: RL -Analyte reporting limit. QCL - Quality control limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant level. ND - Not detected at the rcporting limit.! I -6- TRACK# C07101341 ENERGY LABORATOB-I-E_S! INC "_2393 Satt Creek Highway (52601) . PO. Box 3258 . Caspet; W82602Toll Free 888.235.05/5 . 30zz liti , Fax 907.294.1639 ,'cf,sperdenerwai.n--- ,*,w:;;;;biii)@n I I t LABORATORY ANALYTICAL REPORT Client: Project: [-ab !D: Client Sample lD: Denison Mines (USA) Corp 4th Quarter/Semi-Annual Groundwat c07101341-003 MW 24 Report Date: 01/07/08 Collection Date: 10/23/07 08:05 DateReceived: 10126t07 Matrix: Aqueous Analyses Result Units Qualiflens RL MCU QCL Method Analysis Date / ByI I t I T I I I I I T T T dlra oueury /NCBatane (ts) .,/ Aniontl/ c"tio^ Solids, Total Dissolved Calculated TDS Balance (0.80 - 1.20) VOLATILE ORGANIC COMPOUNDS Acetone B/nzene darAontetrachloride /chloroform r / ChloromethaneV vi"tnytethyr ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Sun: 1,2-Dichlorobenzened4 Sun: Dibromofluoromethane Sun: p-Bromofluorobenzene Sur: ToluenedS 1.64 %60.7 meq/L 62.7 meq/L4030 mg/L1.04 dec. Yo ND ug/LND ugAND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L99.0 %REC99.0 ToREC1U %REC104 %REC 20 1.0 1.0 1,0 1.0 20 1.0 1.0 10 1.0 1.0 8o-120 70-130 80-120 80-120 Calculation Calculation Calculation Calculation Calculation sw8260B sw8260B SW826OB sw8260B SW826OB SW8260B SW8260B sw8260B sw8260B SW8260B sw8260B SW826OB SW8260B sw8260B SW826OB 1110v107 13:57 / bws 11107107 13:87 / bws 1110710713:57 / bws 11107107 13:57 / bws 11107107 13:57 / bws 1012910715:38 / jtr 10t29t0715:38 / jtr 10t29t07'15:38 tik 10129107 15:38 / jtr 10129107'15:38 / jtr 10t29107 15:3g tik 1012910715:38 / jtr 10n9lit 15:38 / jh 10t29t07 15:38 / jtr 10129107 15:38 / jtr 10DglO7 15:38 / jtr 1ill29lll 15:38 / jtr 10l29tll 15:38 / jk 10t29107 15:38 / jtr 10129107 1s:38 / jtr Report Deflnitions: RL - Analyte reporting limit. QCL - Quality control limlt. MCL - Maximum contaminant level. ND - Not detec{ed at the reporting limit.t T -7- TRACK# C07101341 ENERGY LABOEATORIEA NC. , 2393 Salt Creek Hffiway (52601) . P.O. tux 3258 . Caspq bW 82602TollFreeffi8.235.05l5 , 307.2 Yl5 , Fax 307.294.1639 ,'cisper@energytab.m vwweheigytab.con I I I LABORATORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp 4th Quarter/Semi-Annual Groundwater c07101341-013 MW25 Report Date: 01/07/08 Goflection Date: 10125t07 08:20 DateReceive d: 10126t02 Matrix: Aqueous Analyses Result Units Quallfiers RL MCUQCL Method Analysls Date / By D D I I I I I I MAJOR IONS Carbonate as CO3 Bjtxrbonate as HCO3 palcium /Chloride/ rtuoriae V Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate I/ PHYSTCAL PROPERTTES/onV Solids, Total Dissotvect TDS @ 1BO C METALS - DISSOLVED ND 410 392 32 0.3 115 0.54 ND 10.1 272 1710 7.30 2750 ND ND 1.37 ND 10 ND ND ND 1670 ND 11 ND ND ND 0.98 ND 6.02 ND 11 ND mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L s.u., mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L u9/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L uga pCi/L 1 I 1 ,| 0.1 0.5 0.05 0.1 0.5 0.5 30 0.01 10 5.0 0.50 0.50 25 10 10 30 1.0 10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 1.0 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E2AA.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 8900.1 423208 423208 E200.7 A4500-CtB A4500-F C E200.7 A45OO.NH3 G E353.2 E200.7 E200.7 A4500-SO4 E 11103107 13:16 / bas 11103107 13:16 / bas 11110107 13:57 / ts 11101107 16:26 iljt 10131107 21:59 / bas 11106107 20:12 tts 11lOSl07 10:34 tjat 10129107 09:50 / jat 11106107 2Q:12 I ts 111Q6107'20:12 I ts 11105107 13:33 / zd 44500-H B 11t27t0t 11:54 / bas 42540 C 1Ol2A0t 13:45 / bas ArsenicI ffffirr t'[ r#I il:f#; NickelI ;lf;; TinI vn:tl, 7n" I /muilff 1,,,,,!i; D,s s o LVE D I 10131107 20:47 I bvts 10131107 20:47 t bws 10131107 20:47 I bws 10131107 20i47 tbws 10131107 20:47 lbws 10131107 20:47 tbws 11t0t6t07 20:12 t8 '10131107 2O:47 I bvts 10131107 20:41 I bws 10131107 2Q:41 lbws 10131107 20:47 I bws 10131107 20:41 I bws 10131107 20:47 I bvts 10131107 20:41 lbws 10131107 20:47 lbrt'ts 10131107 20:47 I bws 10/31107 20:47 tbws 10131107 20:47 I bws 10131107 20:47 I bws 11113107 18:49 / crw t I RL - Analyte reporting limit. QCL - Quality control limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant tevel. ND - Not deteded at the reporting limit. _26_ Ehi ^?,1 ENERGY LABOBATOBIES, lNC. . 2393 Salt Creek Hishway (82ffi1) . PO. Box 3258 . Casper WY 52602 TollFree888.235.05l5 . 307.2 't515 , Fax 302234.1639 ,-cisper@energylab.co .rwueherfiytab.on I I t LABORATORY ANALYTICAL REPORT Client Denison Mines (USA) Corp Project: Lab lD: Client Sample lD: 4th Quarter/Semi-Annual Groundwater c07101341-013 MW25 Report Date: 01/07/08 Collection Date: 10/25107 08:20 DateReceive d: 10126107 Matrix: Aqueous Result Units Qualifiers RL MCU QCL MethodI I t I I t I t I t t I T TA QUALITY Balance (t 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 - 1.20) VOLATILE ORGANIC COMPOUNDS -2.35 43.3 41.3 2740 1.00 % meq/L meq/L mg/L dec. o/o Calculation Calculation Calculation Calculation Calculation SW8260B sw8260B SW8260B SW826OB sw8260B SW826OB SW826OB SW826OB SW826OB SW826OB sw8260B sw8260B SW826OB SW826OB SW826OB Analysis Date / By 11112107 13:23 / bws 11112107 13;23 / bws 11112107 13:23 / bws fihA07 13:23 / bws '11112107 '13:23 / bws 1Ol29lO7 22:391ik 1Ol29lO7 22:39 ljb 10129107'22:39 I jtr 'l0l29l|7 22:39 tjtr 10l29l0l22:39 ljtr 10129107 22:39 I itr 10129t07 22:39 t ik 10129107 22:39 tjk 1Ol29lO7 22:39 tjtr 1Ol29lO7 22:39 ljh 10129107 22:39 tjtr 10129107 22:39 tjtr 10129107 22:39 I jlr 10129107 22:39ljtr 10129107 22:39ljtr Acetone 6"nr"n" /Crrt ntetrachloride " / chtoroformv Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Sur: 1,2-Dichlorobenzene-d4 Sun: Dibromofluoromethane Sun: pBromofluorobenzene Surr: ToluenedS ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L ND ugA ND ug/LND ug/LND ug/L96.0 %REC100 %REc103 %REC100 %REC 20 1.0 1.0 1.0 't.0 20 1.0 1.0 10 1.0 1.0 80-120 70-130 80-120 80-120 Report Definltions: RL - Analyte reporting limit. QCL - Quality control limit. MCL - Maximum contaminant level. ND - Not detected at the reporting limit.I t _27_ TRACK# e07101341 ENERGY LABORATOR!-Ej9! lNC.,_239! Salt Creek Highway (52601) 'P.O. Box 32iB . Caspe4 WA2602TollFree888.205.05l5 ' 307.1 'rl5 " Fax 307.234.t03s .'cisperAienergytai.co-- vww.ifriigiiat.com I t I LABORATORY ANALYTICAL REPORT Glient: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp 4th Quarter/Semi-Annual Groundwater c07101341-007 MW26 Report Date: 01107t08 Collection Date: 10123t07 1 S:00 DateReceive d: 10126t02 Matrix: Aqueous Analyses Result Units Qualifiers RL MCUQCL Method Analysis Date / ByIMAJOR IONS Srbonate as CO3 I frnlr""asHco3 _ ./ ChlorideV Fluoride I ffi::::koniaasN Nitrogen, Nitrate+Nitrite as Nt liffr" I f,irsrcAL pRopERnEs 'y/ Sorias, Torat Dissotved TDS @ 1BO C I ffi* - DrssoLVED BerylliumI f;HffiI cobatt ll/ [ifl"' ManganeseI il:i;ffi.,, Nickel I ;l;:# TinI ;itJ'T' I ArJ:il,',T,',',:i; ll"o"=o'y/ Gross Alpha minus Rn & U precision (r) ND 411 500 55 0.2 179 0.27 0.7 10.2 162 1930 7.13 31 80 1 ,| 0.5 1 0.1 0.5 0.05 0.1 0.5 0.5 30 mg/L mg/L mg/L mg/L mgll- mg/L mg/L mg/L mg/L mg/L mg/L s.u. mg/L 4C320 B 423208 E200.7 44500-Ct B 44500-F C E200.7 A45OO-NH3 G E35s.2 E200.7 E200.7 A4500-SO4 E 11103107 12:31 tbas 11103107 12:31 tbas 11106107 't9:18 / ts 11t01107 15:11 iljt 10131107 21:43 tbas filAdli7 19:18/ts 11lO5lO7 10:16 t jat 10129107 09:22ljat 11lOGl07 19:15 / ts 11 lOOl07 ,t g: 1 5 / ts 11105107 13:08 / zd 0.01 10 A4500-H B 10t27tOZ 11:29 t bas42540C 10128t0213:43lbas ND ND ND ND ND ND 263 ND 1 190 ND ND ND 12.6 ND ND ND 47.0 ND ND ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L uga ug/L ug/L ug/L uga ug/L ug/L ug/L ug/L ug/L 5.0 0.50 0.50 25 10 10 30 1.0 10 0.50 10 20 5.0 10 0.50 't00 0.30 15 10 1.0 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E20o.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200,8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E900.1 E900.1 10l31lll 19:33 / bws 10131107 19:33 / bws 10131107 19:33 / bws 10131107 19:33 / bws 10131107 19:33 / bws 10131107 19:33 / bws 1110/i,107 19:1S / ts 10131107 19:33 / bws 10131107 19:33 / bws 1Ol31lO7 19:33 / bws 10131107 lg:33 / bws 10131107 19:33 / bws 10131107 19:33 / bws 10131107 19:33 / bws 10131107 19:33 / bws 1Ol31lO7 19:33 / bws 10131107 19:33 / bws 1Ol31lO7 19:33 / bws 10131107 19:33 / bws 11l13lOZ '16:56 / cnnr 11113107 16:56 / crw 3.3 pCi,/L0.7 pCirlI I t RL - Analyte reporting limit. QCL - Quality control limit. D - RL increased due to sample matrix interference. MCL - Maximium contaminant level. ND - Not detected at the reporting limit. -L4- TBACK# C07101341 ENEPGY LABOBATORI^ES, INC .'_239p Saft Creek Highway (5260t) . PO. Box 3258 . Casper Wy A2602Tolt Free 888.23s.0s1s " a2zz 'its , Fax a0z.2a4.t63s .-c[spercieiergytal;.*-- ,,*.ifiiibiirb.ro, I I I LABORATORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Gorp 4th Quarter/Semi-Annual Groundw c07101341-007 MW26 Report Date: 01/07108 Collection Date: 10t23t07 1S:00 DateReceive d: 10126t07 Matrix: Aqueous Result Units Quallfiers RL D I t I I I t t I T I t T I ,TA QUALITY Balance (* 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 - 1.20) VOLATILE ORGANTC COMPOUNDS -1.13 48.6 47.5 3060 1.U o/o meq/L meq/L mg/L dec. o/o Calculation Calculation Calculation Calculation Calculation sw8260B SW826OB SW826OB SW826OB SW826OB sw8260B sw8260B SW826OB SW8260B SW826OB SW8260B SW8260B SW826OB sw8260B SW8260B Analysis Date / By 11107107 13:58 / bws 11107107 13:58 / bws 11107107 13:58 / bws 11107107 13:58 / bws 11107107 13:58 / bws 10129107 23:55 titr 10129t07 23,s5 t jk 1012910723:55 I jtr 1ongt07 23:11 I jk lODglOT 23:55 / jk 10129107 23:55 / jtr 10129107 23:55 t itr 10129107 23:55 tjtr 10129107 23:SS / jtr 10t29107 23:55 / jtr 10t29t07 23:55 / jlr 10129107 23:55 titr 10129107 23:55 / jtr 1Ol29lO7 23:55 tjtr 10129107 23:55 tltr lAcetone /B"n "n"/ CrOon tetrachtoride I chloroform \ chtoromethane Methyl ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surr: 1,2-Dichlorobenzened4 Sun: Dibromofluoromethane Sun: p-Bromofl uorobenzene Surr: Toluene-d8 ND ugAND ug/LND ug/L820 ug/LND ug/LND ug/L 1.2 ug/LND ug/LND uglLND ug/LND ug/L98.0 ToREC95.0 %REC104 o/oREC 101 %REC 20 1.0 1.0 100 1.0 20 1.0 1.0 10 1.0 1.0 80-120 7o-130 80-120 80-120 Repod Definltlons: RL - Analyte reporting limit. QCL - Quality control limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant level. ND - Not detected at the reporting limit.I T _15_ TRACK# C07101341 ENERGY LABORATORI^ES, INC ' 2393 Salt Creg( Hlg-lway (52601) . PO. Box S2iO . Caspet; Wy 82602TollFree888.235.05l5 ' 307.[ 1515 , Fax 307.234.t03s .'cispertienergytao.cb. - www.ifiiibiao.on I I t Client: Project: Lab lD: Client Sample lD: LABORATORY ANALYTTCAL REPORT Denison Mines (USA) Corp 4th Quarter/Semi-Annual Groundwater.z c07101341-Ool /Mw27 / Report Date: 01107108 Collection Date: 10122107 1 4:1 S DateReceived: 10126fi7 Matrix: Aqueous Analyses Result Units Qualifiers RL MCUQCL Method Analysis Date / ByI parbonate as CO3 I f:",:ffi""" as HCo3 t / **$,*,onaasN Nitrogen, Nitrate+Nitrite as N ND 448 170 37 0.7 73.2 ND 5.2 4.3 74.1 406 7.44 1010 ND ugAND ug/LND ug/LND ug/L ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L 10.6 ug/LND ug/LND ug/LND ug& 32.2 ug/LND ug/LND ug/L 1.0 0.5 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 1 1 0.s 1 0.1 0.5 0.05 0.1 0.5 0.5 7 0.0'l 10 5.0 0.50 0.50 25 10 10 30 1.0 10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 1.0 A2320 B M32OB E200.7 A4500-Cr B 44500-F C E200.7 A45OO.NH3 G E353.2 E200.7 E200.7 A4500€O4 E fil0A07 21:54 tbas 11102107 21:54 I bas 11106107 18:13 / ts 11101107 14:14 I t1t 10131107 21:11 lbas 1110610718:13/ts 11105107 09:52ljat '10129107 09:00 / jat 11lOOl07 18:13 / ts 1 1/06/07 .1 8: 1 3 / ts 11105107 12:48 lzd s.u. mg/L I I t t I I I Potassium Sodium Sulfate PHYSIGAL PROPERTIES pH Solids, Total Dissolved TDS @ 180 C METALS. DISSOLVED Arsenic Beryllium Cadmium Chromium Cobalt 44500-H B 1Ol27lO7 11:'t3/bas 42540 C 1Ol28lO7 13:4i / bas I /1iil"' E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 .E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E900.1 E900.1 10131107 18:52 / bws 1Ol31lO7 18:52 / bws 10131107 18:52 / bws 10l31l0l 18:52 / bws 1Ol31lO7 18:52 / bws 10131107 18:52 / bws 11106101 18:13 / ts 10131107 18:52 / bws 10131107 18:52 / bws 1Ol31lO7 18:52 / bws 10131107 18:52 / bws 10131107 18:52 / bws 1Ol31lO7 18:52 / bws '10t31107 18:52 / bws 10131107 18:52 / bws 1Ol31lO7 18:52 / bws 10131107 18:52 / bws 10R1107 18:52 / bws 10131107 18:52 / bws 11l13l\l 16:56 / cnrv 11113107 16:56 / cnr Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc RADIONUCLIDES . DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U precision (t) r/ I pCi/L pCi/L Report Definltions: RL - Analyte reporting limit. QCL - Quality control limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant level. ND - Not detec-ted at the reporting limit.I I -2- TRACK# C07101341 ENERGY LABOBATO$I^Eji! INC '-239! Satt Creek Highway (52601) .PO. Box J258 , Casper WyS2602Tbtl Free 888.235.0515 " 307.{ 1515 ' Fax 307.234. toSs "cisper@energylai.m--- ww*.ifreisiiab.'con I t LABORATORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp 4th Quarter/Semi-Annual Groundwater c07101341-001 MW 27 Report Date: 01107108 Collection Date: 10122t07 14:15 DateReceived: 10126107 Matrix: Aqueous MCU QCL Method I t I I I t I I t t t I I T Result Unlts Quallfiers RL TA OUALITY Balance (t 5) Cations Solids, Total Dissolved Calculated TDS Balance (0.80 - 1.20) V9LAT|LE ORGANTC COMPOUNDS Aietone arbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surr: 1,2-Dichlorobenzened4 Sun: Dibromofl uoromethane Sun: p-Bromofl uorobenzene Sun: Toluene-d8 1.68 17.2 17.8 1020 0.990 o/o meq/L meq/L mg/L dec. %o Calculation Calculation Calculation Calculation Calculation SW8260B SW826OB SW826OB SW826OB SW8260B SW826OB SW826OB SW826OB sw8260B SW826OB st^r8260B SW826OB SW826OB SW826OB SW8260B Analysis Date / By 11107107 13:56 / bws 11107107 13:56 / bws 11107107 13:56 / bws 11107107 13:56 / bws 11107107 13:56 / bws 10129107 '14:19 tjn 10t29107 't4:19 t ih 10129107'14:19 t jh 10129107 14:19 t jtr 10t29107 14:19 tjtr 10t29107 M:19ljV 10t29107 14:19 tjtr 10129t07 14:19 t jtr 1Ol29lO7 14:19 tih 10129107 14:19 t lh 10129107 14:19 tjtr 10n9rc7 M:19 tlk 10t29107 14:19 tjk 10t29107 14:19 titr 10n9rc7 M:19 tih ND ug/LND ug/LND ug/LND ug/L ND ug/LND ug/LND ugAND ug/LND ug/LND ug/LND ug/L93.0 %REC93.0 %REC106 %REC100 %REC 20 1.0 1.0 1.0 1.0 20 1.0 1.0 10 1.0 1.0 80-120 70-130 80-120 8G120 Report Definltlons: RL - Analyte ieporting limit. QCL - Quality control limit. MCL - Maximum contaminail byel. ND - Not detected at the reporting limit.I T -3- TRACK# C07101341 ENERGY LABORATOilIES, INC "_239! Salt Creek Highway (82ffi1) . PO. Box 3258 , Caspet WYA2602Toll Free 888.235.05ff , e07.2 \iti . Fax a02.294.rc3e , cisper@energytab.a, - .*r;.eieisyi;0.:Nn I I I LABORATORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp .,4thQuarter/Semi-AnnualGroundwater,/ c07101341-OO4 /MW28 / Report Date: 01/07/08 Collection Date: 10/23107 10:50 DateReceived: 10126107 Matrix: Aqueous Analyses Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate rfnYsrcru pRopERTtESI /pHSolids, Total Dissolved TDS @ 180 C METALS. DISSOLVED Result Units Qualifierc MCURL QCL Method 6.40 3600 t I I T I I t t T I T I ND 162 538 99 0.6 1U ND o.2 11.4 282 2370 1 1 0.5 1 0.1 0.5 0.05 0.1 0.5 0.5 30 0.01 10 5.0 0.50 0.50 25 10 10 30 1.0 10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 1.0 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 4C320 B 423208 E200.7 A4500-Ct B A4500-F C E200.7 A45OO-NH3 G E353.2 E200.7 E200.7 A4500-SO4 E Analysis Dale / By 1lrcA0l 22:25 I bas 11102107 22:25 tbas 11106107 18:41 / ts 11101107 14:48 lgt 10131107 21:29 lbas 11t06107 18:41 / ts 11105107 10:04 tiat 10129107 09:15 /jat 11106107 18:38 / ts 11106107 18:38 / ts 11105107 12:56lzd s,u. mg/L 44500-H B 10127107 11;21 I bas FA54O C 10128t07 13:42 I bas Arsenic Beryllium Cadmium Chromium Cpbalt @opper 1,onI LeadV M"ng"n"r" Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium 17.9 ug/LND ug/t 3.36 ug/LND ug/L31 ug/LND ug/L43 ug/LND ug/L 1480 ug/LND ug/LND ug/L29 ug/L5.0 ug/LND ug/L0.90 ug/LND ug/L 3.40 ug&ND ug/L48 ug/L 1.2 0.5 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E900.1 E900.1 10131107 19:13 / bws 10131107 19:13 / bws 10131107 19:13 / bws 10131107'19:13 / bws 10131107 19:13 / bws 10131107 19:13 / bws '11106,/07 18:38 /ts 10131107 19:13 / bws 10131107 19:13 / bws 10131107't9:13 / bws 10131107 19:13 / bws 10131107 19:13 / bws 1Ol31lO7 19:13 / bws 10131107 19:13 / bws 10131107 19:13 / bws 1Ol31lO7 19:13 / bws 10131107 19:13 / bws 10131107 19:13 / bws 1Ol31lO7 19:13 / bws 11l13lll 16:56 / crw 11113107 16:56 / crw RADIONUCLIDES . DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U precision (r) pCi/L pCi/L Report Deflnltlons: RL - Analyte reporting limit. QCL - Quality control limit. D - RL lncreased due to sample matrix interference. MCL - Maximum contaminant level. ND - Not detected at the reporting limit.I I -8- TRACK# C07101341 ENERQY LABOBATOR!-EA tNC . 2093 saft creg( Hlg_hway (a2601) . p.o. Box 3258 . casper, w 82602TollFreeffi.235.05l5 , 3022 'its , Fax slz.2g4.tfre ,'cbsperaieneigytat.co- -.ww.ifrir:gitab)con I t I Client: Project: Lab lD: Client Sample lD: LABORATORY ANALYTICAL REPORT Denison Mines (USA) Gorp 4th Quarter/Semi-Annual Groundwater,"c07101341-OO4 ,/MW28 ,/t/ Report Date: 01/07/08 Collection Date: 10123t07 10:50 DateReceived: 10126101 Matrix: Aqueous Analyses Result Unlts Qualiflers RL MCU QCL Method Analysis Date / By _ TDS Balance (0.80 - 1.20) I /ounle oRGANrc coMpouNDS fenton" lV Ei['""lL"n,ono" -0.134 o/o 54.8 meq/L54.6 meq/L 3570 mg/L 1.01 dec. o/o ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L ND ug/LND ug/LND ug/LND ug/LND ug/L99.0 %REC96.0 %REC104 %REC99.0 %REC Calculation Calculation Calculation Calculation Calculation sw82608 SW826OB SW826OB SW826OB SW826OB SW8260B SW826OB SW826OB sw8260B SW826OB SW826OB SW826OB SW826OB sw8260B SW826OB 11107107 13:57 / bws 11107107 13:57 / bws 1110710713:57 / bws 11107107 13:57 / bws 11107107 13:57 / bws 1012910716:16 / jtr 10129107 16:16ljtr 10129107'16:16 I jtr 10t29t07 16:16ljk 10t29107 16:16 tjtr 1012910716:16 / jh 1Ol29lO7 16:16 / jlr 10129107 16:16 / jtr 10129107 16:16 / jk 1ol29lo7 16:16 / jtr 10129107 16:16 / jtr 10129107 16i16 I jtr 10129t0716:16 / jtr 1ot29107 16:16 / jtr 10nsl07 16:16 / jtr I T T I t I T I Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surr 1,2-Dichlorobenzene-d4 Sun: Dibromofl uoromethane Sun: pBromofl uorobenzene Sun: Toluene{8 20 1.0 't.0 1.0 1.0 20 1.0 1.0 10 1.0 1.0 80-'t20 70-130 80-120 80-120 T. Report Deflnitlons: RL - Analyte reporting limit. QCL - Quality control limit. MCL - Maximum contaminant tevel. ND - Not detecled at the reporting llmit.I T -9- TRACK# C07101341 ENERCY LABORATOilEA NC. , 2S9S Satt Creek Hishway (52il1) . p.O. Box i2S8 , Casper WA2602TollFree888.235.05l5 " 3022' '515 , Fax 302234.1639 .'cisper@energytab.mr :{ww.eherbytab.con I I I LABOMTORY ANALYTICAL REPORT Client: Project: Lab lD: ClientSample lD: MW29 Denison Mines (USA) Corp 4th Quarter/Semi-Annual Groundwater c07101341-009 Report Date: Collection Date: DateReceived: Matrix: 01t07t08 10124107 08:01 10t26t07 Aqueous Analyses Result Units Qualifiers RL MCUQCL Method Analysis Date / ByI t I I MAJOR IONS ;"l0arbonate as CO3 ,/ Bicarbonate as HCO3 / Cal"im . / ChlorideV Ftuoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate ND 338 510 37 0.8 240 0.79 ND 17.3 425 2790 1 1 0.5 1 0.1 0.5 o.bs 0.1 0.5 0.5 30 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 42320 B 4.23208 E200.7 44500-CtB 44500-F C E200.7 A45OO.NH3 G E35s.2 E200.7 E200.7 A4500-SO4 E 11103107 12:46 tbas 11103107 12:46 tbas 11106107 19:32 / ts 11101107 15:44 iljt 10131107 21:49lbas 11106107 19:32 / ts 11105107 'lO,,20ljat 10129107 09:32 tjat 11106107 19:28 / ts 11106107.19:28 t ts 11105107 13:21 tzd l r/mvsrcer- pRopERnES / So[Os, Totat Dissotved TDS @ 1Bo C t METAL' - DrssoLVED Arsenic BervlliumI fft#rfr lcoa"t l,lrr;il- ManganeseI ililfio",,, Nickelr f#; TinI y:#il, I /m*ilff 'Li,!i; D'|ssoLVED 6.87 4370 s.u. mg/L 0.01 10 5.0 0.50 0.50 25 10 10 30 1.0 10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 1.0 A4500-H B 10t27t0t 11:33/bas 42540 C 10t2$l!t 13:43 / bas ND ug/LND ug/LND ug/LND qS/LND ug/LND ug/L 1110 ug/LND ug/L 4930 ug/LND ug/L ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L11.1 ug/LND ug/L 15 ug/L E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E900.1 10131107 19:46 / bws 10131107 19:46 / bws 10131107 19:46 / bws 10131107 19:46 / bws 10131107 19:46 / bws 10131107 19:46 / bws 11106107 19:28 / ts 10131107 19:46 / bws 10131107 19:46 / bws 1013110719:46 / bws 10131107 19:46 / bws 1013110719:46 / bws 10131107 19:46 / bws 10131107 19:46 / bws 10131107 19:46 / bws 10l31lil 19:46 / bws 10131107 19:46 / bws 10131107 19:46 / bws 1013110719:46 / bws 11113107 16:56 / cnrrrNDpCi/L I Report Definitlons: RL - Analyte reporting limit. QCL - Quality controt limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant level. ND - Not detected at the reporting limit.t T _ 18_ TRACK# C07101341 ENERGYLABOBATORIES, INC ,2393 SaltCregkH!1_Qway(52601) . PO. Box3258 . Casper; WYB2602TollFree888.235.05l5 ' 307.2 'rl5 ' Fax 302234.1639 "'c)sper(ienergytab.ca, ,ywiifreiCyAO.con I I I Client: Project: Lab lD: Client Sample lD: LABORATORY ANALYTICAL REPORT Denison Mines (USA) Corp 4th Quarter/Semi-Annual Groundwaterc07101341-009 ,/MW29 /V Report Date: Collection Date: DateReceived: Matrix: 01t07t08 10124107 08:01 10t26t07 Aqueous Analyses TA QUALITY Balance (r 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 - 1.20) VOLATILE ORGANIC COMPOUNDS Acetone fB"n."n" Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Sun: 1,2-Dichlorobenzened4 Sur: Dibromofluoromethane Sur: p-Bromofl uorobenzene Sur: ToluenedS Qualifiers MCURL QCL MethodI t I I I I I I I t t T I -0.082 64.6 64.5 4200 1.04 % meq/L. meq/L mg/L dec. Yo Calculation Calculation Calculation Calculation Galculation SW826OB SW826OB SW826OB SW826OB SW8260B sw8260B SW826OB SW826OB SW826OB SW826OB SW8260B sw82608 sw8260B SW826OB SW826OB Analysis Date / By 11107107 13:59 / bws 11107107 13:59 / bws 11lO7lO7 13;59 / bws 11107107 13:59 / bws 'l1ll7l07 13:59 / bws 10129107 20:04 t jtr 10l29lOZ 20:04ljtr 10129107'20:04 I jh 10129107 20:04 tjtr 10129107 20:04 t jtr 10129107 2A:04lik 10129107 20:041jtr 10129107 20:O4 t jtr 10129107 20:04 titr 10129107 20:M I itr 10129107 20:A4litr 10129t07 20:041jtr 10129107 20:04lik 10129107 20:04ljtr 10t29107 20:04ljk ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L ND ug/L ND ug/LND ug/L97.0 %REC97.0 ToREC104 %REC101 70REC 20 1.0 1.0 1.0 1.0 20 1.0 1.0 10 1.0 1.0 80-120 70-130 80-120 80-120 Report Definltions: RL - Analyte reporting limit. QCL - Quality control limit. MCL - Maximum contaminant level. ND - Not detected at the reporting limit.I T _ 19_ TRACK# eo71 01 ?41 ENERGY LABORATOR_I_EE INC .'_239! Satt Creek Highway (52601) , P.O. Box 32i8 , Caspet; ,W A2602TollFreeffi8.235.05t5 , 30zz liti ' Fax s02.204.ff3e ,'cisper(trenergytab.co;--.yww.ifriibyao.con I T I LABORATORY ANALYTIGAL REPORT Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp 4th Quarter/Semi-Annual Groundwater c07101341-010 MW30 Report Date: Collection Date: DateReceived: Matrix: 01t07t08 10124107 10:24 10t26t07 Aqueous Analyses Result Units Qualifiers RL MCUQCL Method Analysis Date / ByI I I I I I I I t t T I I MAJOR IONS datonateas Co3 hie.arbonateas HCO3I cd"iu . / q,o,ta" Y Ftuoriae Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate / PHYSTCAL PROPERTTES IoH V So,,o", Total Dissolved TDS @ 1Bo C METALS. DISSOLVED Arsenic Beryitium Cddmium thromium Aobalt ,f crpp",I iron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin lUranium f Vanadium I Z,tnc I I \l nnotolrucLtDES - DtssoLvED Gross Alpha minus Rn & U ND mg/L197 mg/L294 mg/L 122 mg/L0.3 mg/L72.9 mg/L ND mg/L 14.9 mg/L8.1 mg/L110 mg/L871 mg/L 7.43 s.u. 1660 mg/L ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L125 ug/LND ug/L54 ug/LND ug/LND ug/L ND ug/L29.8 ug/LND ug/L ND ug/LND ug/L6.88 ugAND ug/LND ugA 1 1 0.5 1 0.1 0.5 0.05 0.2 0.5 0.5 30 0.01 10 5.0 0.50 0.50 25 10 10 30 1.0 10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 1.0 423208 A232AB E200.7 A4500-Ct B A4500-F C E200.7 A45OO-NH3 G E353.2 E200.7 E200.7 44500-S04 E 11103107 12:53 lbas 11103107 12:53 / bas 11lOOl07 19:48 / ts 11101107 15:53 / tjt 10131107 21:51 tbas 11106107 19:44 / ts 11105107 10:22 tjat 10129107 09:35 / jat 11lOGl07 19:44 / ts 11lOGl07 19:44 tts 11105107 13:22 tzd 44500-H B 10t2il0111:3S/bas l254O C 1Ol28tOZ t3:43 / bas ND pCi.rL E200.8 E200.8 E200.8 E200.8 E200.8 E200.6 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E900.1 10131107 20:21 lbws 10131107 20:27 I bws 10131107 20:27 tbws 10131107 20:27 tbws 10131107 20:27 I bws 10131107 20:27 lbws 11106107 19:44 / ts 10131107 20:27 lbws 10131107 20:27 I brus 10131107 20:27 I bws 10131107 20:27 I bws 10131107 20:27 tbws 10131107 20:27 tbws 10131107 20:27 lbws 10131107 20:27 / bws 1Ol31lO7 20:27 tWts 10131107 20:27 I bws 10131107 20:27 I bws 10131107 20:27 I bws 11113107 16:56 / crw Report Deflnltions: RL - Analyte reporting limit. QCL - Quality control limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant level. ND - Not detec{ed at the reporting limit.T I _20_ TRACK# r.07101?41 ENEflGY LABOilATORIES, lNC. .2393 Salt Creek Highway (82601) , PO. Box 3258 " Casper W82602 TollFree888.205.05l5 " 307.2 '515, Fax307.234./639 " casper@energylab.m,, .vwwehergytab.com I I t I LABORATORY ANALYTICAL REPORT Client: Project: Lab lD: Glient Sample lD: Denison Mines (USA) Corp 4thQuarter/Semi-AnnualGroundwater r/'c07101341-010 ,/MW3o v Report Date: 01/07/08 Collection Date: 10124107 10:24 DateReceived: 10126107 Matrix: Aqueous Analyses Result Units Qualifiers RL MCU QCL Method Analysis Date / By T DATA QUALITY /Nceaaneesl 1/ Rnionsv cations Solids, Total Dissolved Calculated -0.433 o/o 25.9 meq/L 25.7 meq/L 1650 mg/L1.01 dec. Yo ND ug/L NO ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/tND ug/LND ug/L98.0 %REC96.0 %REC107 %REC 99.0 %REC Calculation Calculation Calculation Calculation Calculation 11107107 13:59 / bws 11107107 13:59 / bws 11107107 13:59 / bws 11107107 13:59 / bws 11107107 13:59 / bws 10t29107 20:41 tjtr 10129107 20:41 ljtr 10t29t07-20:41 litr 10t29107 20:41 ljtr 10t29t07 20:41 ljtr 1onil07 20:41 ljtr 10t29107 20:41 ljtr 10129107 20:41 ljlr 10t29107 20:41 t itr 10129107 20:41 I ik 10129107 20:41 ljk 1ol2gl07 20:41 tih 10129107 20i41 ljlr 10t29107 20:41 tjlr 10t29107 20:41 titr _ TDS Balance (0.80 - 1.20) I voLArLE oRGANrc coMpouNDS Acetone I !ll'illu*n"*" A;ntorotorm. / Chloromethanel' u:llll""i:Li:r"J: Naphthalene - Tetrahvdrofurant I;i::::,",", Surr 1,2-Dictrlorobenzene-d4I :rx;38l:ffi1il::ffill:t: Sun: ToluenedS I T t 20 1.0 1.0 1.0 1.0 20 1.0 1.0 10 1.0 1.0 80.120 70-130 80.120 80-120 SW8260B sw8260B SW8260B SW8260B SW826OB SW826OB sw8260B SW8260B SW826OB SW826OB SW826OB sw8260B sw8260B SW826OB sw8260B I I I Report Definltlons: RL - Analyte reporting limit. QCL - Quality control limit. MCL - Maximum contaminant level. ND - Not detec{ed at the repoding limit.T T _2L_ TRACK# C07101341 ENEBGYLABORATORIES,INC. .2SgSSaltCreekHighway(8260/)'P.O. Box3258 , Caspet W82602 Ton Free 888.235.0515 . 307.2 1515 . Fax a02.2a4.1639 ,'chsper@energytab.co. .vtwueheigytab.on I I I LABORATORY ANALYTICAL REPORT Client: Denison Mines (USA) CorpProject 4th Quarter/Semi-Annual erounawafi Lab lD: C07101341-011 / Client Sample lD: MW 31 V Report Date: 01/07/08 Collection Date: 10124107 12:35 DateReceived: 10126107 Matrix: Aqueous Analyses Result Unlts Qualifiers RL MCUQCL Method Analysis Date / By 1 1 0.5 1 0.1 0.5 0.05 0.2 0.5 0.5 10 I t I I I t MAJOR IONS Carbonate as OO3 Bjlarbonate as HCO3 Oalcium TChloride/ FluorideI \rl Magnesium' Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodium Sulfate / pxYstcll pRopERTtES /o* l/ sotias, Totat Dissotved TDS @ 1Bo c METALS. DISSOLVED Arsenicr ##ffi tobalt l/",r{i" ManoaneseI il:,i,*'fl",, NickelI ;;T; TinI Y:il:;x, . Zinc I / muh,".*,,",f i; D,ssoLVED I ND mg/L 2Og mg/L172 mg/L 122 mg/L0.8 mg/L83.8 mg/L ND mgA 24.6 mg/L6.4 mg/L93.3 mg/L497 mg/L 7.62 s.u. 1150 mg/L ND ug/LND ug/LND ug/L ND ug/L ND ug/LND ug/LND ugrll.ND ug/L ND ug/LND ug/LND ug/l- ND ug/L 56.6 ug/LND ug/L ND ug/LND ugA7.20 ug/LND ug/L10 ug/L 42320 B FA320B E200.7 A4500-Ct B 44500-F C E200.7 A45OO.NH3 G E353.2 E200.7 E200.7 A4500-SO4 E 44500-H B 42540 C E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 8200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E900.1 11103107 13:01 / bas 11103107 13:01 / bas 1'1106107 19:51 /ts 11101107 16:03 / ljl 10131107 21:54 lbas 1110610719:51/ts 11lOSlO7 10:24 ljat 10129107 09:37 / jat 1110610Z 19:51 /ts 11/06/07'19:51 / ts 11105107 13:28 lzd 10127107 11:38 / bas 1Ol28lO7 13i44 I bas 10131107 20:34 / bws 1Ol31lO7 20:34 I bws 10131107 20:34 / bws 10131107 20:34 / bws 10131107 20:34 / bws 1Ol31lO7 20:34 / bws 11lOOlO7 19:51 / ts 10t31107 20:34 / bws 10131107 20:34 / bws 10l31l0l 20:34 / bws 10131107 20:34 / bws 1Ol31lO7 20:34 / bws 10R1107 20:34 / bws 'l0l31l0l20:34 / bws 10131107 20:34 / bws 1Ol31lO7 20:34 / bws 'l0l31l07 2O34 / bws 1Ol31lO7 20:34 / bws 1Ol31lO7 20:34 / bws 11113107 18:49 / crwpCi/L 0.01 10 5.0 0.50 0.50 25 10 10 30 1.0 '10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 1.0 Report Definltlons: RL - Analyte reporting limit. QCL - Quality control limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant level. ND - Not detected at the reporting limit.I T -22- TRACK# e071 01 ?41 ENEROY LABORATOBIES, lNC. . 2393 Salt Creek Highway (82601) , P.O. Box 3258 . Cas@r, WY82602TollFree888.235.05l5,30Zq '5/5 " Fax307.234.1639 , casper@energylab.m .uww.ehergylab.com T I Client: Project: Lab lD: Client Sample lD: LABORATORY ANALYTICAL REPORT Denison Mines (USA) Corp 4thQuarter/Semi-AnnualGroundwater / co71o1u1-011 /MW31 lr/ Report Date: 01/07/08 Collection Date: 10124107 12:35 DateReceived: 10126107 Matrix: AqueousI I I I I I I I I I I I T T T I Result Unlts Qualifierc RL MCU QCL Method TA QUALITY Fy'C Balance (r 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 - 1.20) VOLATILE ORGANIC COMPOUNDS Acetone Benzene 1.70 19.0 19.7 1200 0.960 o/o meq/L meq/L mg/L dec. o/o Calculation Calculation Calculation Calculation Calculation Analysis Date / By 11107107 13:59 / bws 11107107 13:59 / bws 11107107 13:59 / bws 11107107 13:59 / bws 11107107 13:59 / bws 10129107 21:20 I jlr 10129t07 21:20 tjtr 10129107'21:20 I jtr 10129107 21:20 t jlr 10t29107 21:20litr 10129107 21:20I jh 10t29107 21:20 lik 1Ol29lO7 21:20 I jlr 10129107 21:20ljlr 10t29107 21:20ljlr 10129107 21:20I jlr 1Ol29lO7 21i20 lih 10n9rc7 21:20 tjk 10l29tOZ 21:20 lilr 10129107 21:20ljlr Cgrbon tetrachloride phbroform rChloromethane | / uetfrvrethyl ketone7 Methyl"ne chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofl uoromethane Surr: p-Bromofl uorobenzene Surr: ToluenedS ND ug/LND ug/LND ug/L ND ug/L ND ug/LND ug/LND ug/L ND ug/LND ug/LND ug/LND ugA 97.0 %REC 96.0 o/oREC 100 %REC101 %REC 20 1.0 1.0 1.0 1.0 20 1.0 1.0 10 1.0 1.0 80-120 70-130 80-120 80-120 SW826OB SW826OB sw8260B SW826OB sua260B SW8260B SW826OB SW826OB sw8260B sw8260B SW826OB SW826OB sw8260B SW826OB SW826OB Report RL - Analyte reporting limit. Definltions: eCL - euality control limit. MCL - Maximum contaminant level. ND - Not detected at the reporting limit. -23- 'FPArrra# cn71n1?a1 ENERGY LABORATOBIES, lNC. ' 2393 Salt Creek Hiqhway (52tu1) . PO. 1ox 3258 , Casper WYS2O02TollFree888.235.05l5 , 307.1 t5l5 " Fax 307.234.1639 ,-casper@energytab.m ,ww.einrl1ytab.con I I I Client: Project: Lab lD: Client Sample lD: LABORATORY ANALYTICAL REPORT Denison Mines (USA) Corp 4th Quarter/Semi-Annual Groundwater c07101341-012 MW32 Report Date: 01/07/08 Collection Date: 10124107'14:48 DateReceive d: 10t26107 Matrix: Aqueous Analyses IONS as CO3 as HCO3 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium METALS. DISSOLVED Arsenic Beryllium Cadmium Chromium Gobalt Copper lron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc RADIONUCLIDES . DISSOLVED Gross Alpha minus Rn & U Gross Alpha minus Rn & U Precision (t) Result Units Qualifiers MCURL QCL Method s.u. mg/L t I I I I I I t I I ND 434 539 33 0.2 247 0.78 ND 14.6 212 2400 6.75 3780 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 1 1 0.5 1 0.1 0.5 0.05 0.1 0.5 0.5 30 0.01 10 5.0 0.50 0.50 25 10 10 30 1.0 10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 1.0 ND ug/LND ug/L 1.20 ug/L ND ug/L55 ug/LND ug/L 6/.20 ug/LND ug/L 5170 ug/LND ug/L10 ug/L 67 ug/LND ug/LND ug/LND ug/LND ug/L 3.91 ug/L ND ugA143 ug/L Analysis Date / By 42320 B 11103t07 13:09 / basA232OB 11t03t02 13:09 / bas8200.7 11t06107 20:01 / ts 44500-Cl B 11101107 16:23lt1t A4500-F C 10131t07 21:i7 lbasE200.7 11lOGl07 20:01 fts A4500-NH3 c 11l05llt 10:32 tiatE353.2 10129107 09:40 / jat E200.7 11106t07 19:58 / tsE2OO.7 11106/07-19:88/ts 44500-504 E 11105107 13:32 tzd 44500-H B 10l27tlt 11:40/bas 42540 C 10128107 13:44 t bas E200.8 10B1io7 20:41 / bwsE200.8 10131t07 20:41 / bwsE200.8 10131107 20:41 I bwsE200.8 10131107 20:41 / bwsE200.8 10131107 20:41 / bwsE200.8 10131107 20:4't / bwsE200.7 11106rc7 19:58 / tsE200.8 10131t07 20:41 I bwsE200.8 10131107 20:41 / bwsE200.8 10/31107 20;41 / bwsE200.8 10131107 20:41 / bwsE200.8 10131107 20:4i / bwsE200.8 10131107 20:41 / bwsE200.8 1Ol31tO7 20:41 / bwsE200.8 10131107 20:41 / bwsE200.8 10131107 20:41 / bwsE200.8 10131107 20:41 / bwsE200.8 10131107 20:41 / bwsE200.8 10131107 20:41 / bws E900.1 E900.1 11113107 18:49 / cnrv 11113107 18:49 / crw T rJ I 3.0 pCi/L 0.7 pCi/L Report Definitlons: RL - Analyte reporting limit. QCL - Quality control limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant level. ND - Not detected at the reporting limit.I I _24_ TRACK# eO71 01 ?41 ENERGY LABOflATOHES, lllC. . 2393 Salt Creek Highway (82601) . P.O. Box 3258 . Casper W 82602 To11Free888.235.0515,307.4 1515, Fax307.234.16,?9 . casper@energylab.m 'vww.energylab.on T I I Client: Project: Lab lD: Glient Sample lD: LABORATORY ANALYTIGAL REPORT Denison Mines (USA) Corp 4th Quarter/Semi-Annual Groundwater/ c07101341-012 /MW32 V Report Date: 01/07/08 Gollection Date: 10124107 14:45 DateReceived: 10126107 Matrix: Aqueous Analyses TA QUALITY A/C Balance (t 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 - 1.20) VOLATILE ORGANIC COMPOUNDS Quallfiers MCURL QCL Method SW8260B SW826OB SW826OB SW8260B sw8260B SW826OB SW826OB sw8260B sw8260B sw8260B SW826OB sw8260B SW826OB SW826OB SW826OB t T I t I I I I I t I T T I t -0.491 58.1 57.5 3670 1.03 % meq/L meq/L mg/L dec. o/o Calculation Calculation Calculation Calculation Calculation Analysis Date / By 11107107 13:59 / bws 11l07l0l 13:59 / bws 11107107 13:59 / bws 11107107 13:59 / bws 1'll07lO7 13:59 / bws 10t29107 21:59ljtr 10129107 21:59 tjn 10129107"21:59 tjE 10129107 21:59 ljn 10129107 21:59ljlr 10129107 21:59 lilr 1Ol29lO7 21:59ljtr 10129107 21:59 tjh 10129107 21:59ljlr 10129107 21:59 tjk 10129107 21:59ljh 10t29t07 21:59ljk 10129t07 21:59 I jtr 10129107 21:591jk 10129107 21:59lin Acetone dlnzene /Carbon tetrachloride/ Chloroform V chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Sun: 1,2-Dichlorobenzene{4 Sun: Dibromofl uoromethane Sun: p-Bromofluorobenzene Surr: Toluene-d8 ND ug/L ND ug/L ND ug/LND ug/L ND ug/L ND ug/LND ug/LND ugA ND ug/L ND ug/L ND ug/L100 %REC98.0 %REC103 ToREC100 %REC 20 1.0 1.0 1.0 1.0 20 1.0 1.0 10 1.0 1.0 80-120 70-130 80-120 80-120 Report RL - Analyte reporting limit. Definltlons: eCL - euality control limit. MCL - Maximum contaminant level. ND - Not detected at the reporting limit. _25_ mAeK# eo7101?41 ENERGYLABOBATOHEA INC ,2S9SSaltCreekHighway(52601).P.O. Box3258 , Caspet WA2602 Toll Free 888.235.0515 , 307.2 '1515 , Fax 302234.1639 ,'cisper@energytab.cc vwnueheigytab.con I I I LABORATORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample lD:/ Report Date: Collection Date: DateReceived: Matrix: 01t07t08 10130107 14:18 11t02t07 Aqueous Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual c071 10077-009 MW60 Analyses Result Unlts Qualifiers RL MCU QCL Method Analysis Date / By ND mg/L 2 mglLND mg/LND mg/LND mgAND mg/LND mg/L ND mg/LND mg/L0.9 mg/L 1 mg/L 1 1 0.5 1 0.'l 0.5 0.05 0.1 0.5 0.5 1 A232OB 423208 E200.7 A4500-Ct B 44500-F C E200.7 A45OO.NH3 G E353.2 E200.7 E200.7 A4500-SO4 E 11106107 14:59 / bas 11106107 14:59 / bas 11115107 18:25 / ts 11107t07 11:27 ttit 11105107 13:44 lbas 11115107 18:2S / ts 11106107 12:29 tiat 11108107 13:42 tiat 11115107 18:25 / ts 11115107.18:25 tts 11lOGlO7 12:55 tzd Solids, Totat Dissolved TDS @ 180 C t [1tn* ' DrssoLVED BerylliumI fi:#ffi ,#fil*" I il:ffifl",." SeleniumI ;ffi,. Tint y,lH'T' 6.01 ND 0.01 10 s.u. mg/L 44500-H B 11lOStO7 10:36 / niv A2540 C 11t0SlO7 14:131 rw ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/l-ND ug/LND ug/LND ug/L 5.0 0.50 0.50 25 10 10 30 1.0 10 0.50 10 20 5.0 't0 0.50 100 0.30 15 10 1.0 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E900.1 11109107 20:59 / bws 11109107 20:59 tbws 11109107 20:59 / bws '11109107 20:59 / bws 11109107 20:59 / bws 11109107 20:59 / bws 11115107 18:25 / ts 11l0gl07 20:59 / bws 11l0gl07 20:59 / bws 11logl07 20:59 / bws 11l09l|l20:59 / bws 11109107 20:59 / bws 11l0gl07 20:59 / bws 11logl07 20159 / bws 11l0gl07 20:59 / bws 11l0gl07 20:59 / bws 11109107 20:59 / bws 11109107 20:59 / bws 1 1/09/07 20:59 / bws 11116107 14:24 I crwI T . DISSOLVED Gross Alpha minus Rn & U pCi/L Report Definitions: RL - Analyte reporting limit. QCL - Quality control timit. MCL - Maximum contaminant level. ND - Not detected at the reporting limit.I t _1 8_ TRACK# CO7LLOO77 EilIERCY LABOBATORIES, lNC. .2393 Salt Creek Highway (82601) .P.O. Box 3258 . Caspr, W82602 TollFree888.235.05l5 " 307.? 't515 " Fax307.234.1639 , casper@energylab.cc www.energylab.om I I I LABORATORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Anrydf' co711OO77-OO9 ,/MW6o / Report Date: 01/07/08 Collection Date: 10/30/07 14:18 DateReceive d: 1 1 l12l07 Matrix: Aqueous Analyses Result Units Quallfiers RL MCU QGL Method Analysis Date / By o/o meq/L meq/L I T I I I I t I I T T t oNfa ouaury y'JCeaaneeg.s1 V Anions Cations -5.02 0.061 0.056 Calculation Calculation Calculation 11116107 14:38 / bws 11116107 14:38 / bws 11116107'14:38 / bws 11lOSl07 18:13 / dkh 11105107 18:13 / dkh 11lOSl07 18:13 / dkh 11/05/0718:13/dkh 11lOSl07 18:13 / dkh 11105107 18:13 / dkh 11lO5lO7 18:13 / dkh 11lOSlO7 18:13 / dkh 11lOSl07 18:13 / dkh 11105107 18:13 / dkh 11105107 18:13 / dkh 11lO5lO7 18:13 / dkh 11105107 18:13 / dkh 1110s107 18:13 / dkh 11105107 18:13 / dkh - The ion balance is not appropriate for near blank results. volATtLE oRGANIC COMPOUNDS Ac€tone {n."n" Iarbon tetrachloride /chloroformy' Chbromethane Methyl ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surr; 1,2-Dichlorobenzened4 Sun: Dibromofl uoromethane Sun: p-Bromofl uorobenzene Surr: ToluenedE ND ug/LND ug/LND ug/L ND ug/LND ug/LND ug/L ND ug/LND ug/LND ug/LND ug/LND ug/L102 o/oREC 121 %REC114 o/oREC 97.0 %REC 20 1.0 1.0 1.0 1.0 20 1.0 1.0 10 1.0 1.0 80-120 70-130 8G.120 80-120 SW826OB SW826OB SW826OB SW826OB SW826OB SW826OB SW826OB sr /82608 sw8260B SW8260B SW826OB SW826OB SW826OB SV\E26OB sw8260B T t T Report Deftnltions: RL - Analyte reporting limit. QCL - Quality control limit. MCL - Maximum contaminant level. ND - Not detected at the reporting limit. - 19- rRACK# C07110077 I ENERG, LABORATOB-,-EE rNC ' 2393 Satt Crryf ltlqQway (s2ffi1) . p.o. Box 3258 . Caspq bw82602rott Free 888.23i.0i15 " s1zi - 0i$-: Fax s0rhi:i6ib :r;;r;;ar;;E Etr;'* *,r;;;;;;s;;rL:*, I I LABORATORY ANALYTICAL REPORT Client: Project Lab lD: Client Sample lD: Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual c07110077-010 MW63 Report Date: 01/07/08 Collection Date: 10/30/07 1S:00 DateReceive d: 1 1 l02lOZ Matrix: AqueousI I I I I I Analyses roNs as CO3 as HCO3 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sgdium d rrt"/ /nnvsrcel pRopERTTES "l pn I Soros, Totat Dissolved TDS @ 1Bo C Qualifiers MCURL QCL Method ND mg/LND mg/LND mg/LND mg/LND mg/LND mg/LND mg/LND mg/LND mg/L0.9 mg/LND mg/L 1 1 0.5 1 0.1 0.5 0.05 0.1 0.5 0.5 1 Ae32OB AC320B E200.7 A4500-ctB 44500-F C E200.7 A45OO-NH3 G E353.2 E200.7 E200.7 44500-504 E Analysis Date / By 11106!07 1S:04 / bas 11106107 iS:04 / bas 11115107 18:29 / ts 11t07107 12:24 tgt 11lOSl07 13:41 t bas 11115107 1B:29 / ts 1'110610712:31t jat 11108107 13:45 tjat 11115107 18:29 / ts 11115107.18:29 tts 11106107 12:56lzd 5.96 s.u.ND mgA ND ug/LND ug/LND ug/LND ug/LND ug/LND ugAND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ugA 0.01 10 5.0 0.50 0.50 25 10 10 30 1.0 10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 1.0 A450G.H B lltOStOt 10:38 / rw 42540 C 11lOSlO7 14:13 I ruv I ffmt. - DrssoLVED BerylliumI :Iffiffi CoooerI 'fr, /Manganese l/ g#n,,, SeleniumI ;ffi, TinI y,iF'T', E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E.200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 . E200.8 E200.8 E200.8 E200.8 E900.1 11t09107 21:06 / bws 11109t07 21:06 / bws 11l09l0t 21:06 / bws 11109107 21:06 tbws 11l0gl07 21:06 / bws 11109107 21:06 / bws 11115107 18:29 / ts 11l09lOZ 21:06 / bws 11109107 2.t:06 / bws 11109107 21:06 / bws 11l0gl07 21:06 / bws 11109107 21:06 / bws 11109107 21:06 / bws 11109107 21:06 / bws 11109107 21:06 I bws 11l0gl07 21:06 / bws 1 1/09/07 21:06 / bws 11l0gl07 21:06 / bws 11109107 21:06 / bws 11116107 14:24 I crw I/:u,xx"',','"',1'-;DrssoLVED I ND pCi/L Report Definltions: RL -Analyte reporting limit. QCL - Quality controt timit. MCL -tiaximum contaminant level. ND - Not detected at the repofting limit.t I -20-.FPAnr4 r'n111nn.11 ENERGYLABOBATOHEE lNC. .2393SaftCreekHffiway(52601).PO. Box3258 . Casper W82602 Toll Free ffi.235.0515 . 302, 't515 , Fax 307.234.1639 . casper@energylab.cc wwueitergylab.com LABORATORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample ID: Denison Mines (USA) Corp 4th Qk Groundwater/Semi-Annual c07110077-010 MW63 Report Date: 01/07/08 Collection Date: 10/30/07 1S:00 DateReceived: 1 1 102107 Matrix: Aqueous Result Units Qualifiers RL MCU QCL Method DATA QUALITY A/C Balance (t 5) Anions Cations AcEtone Bqhzene darbon tetrachloride 6hloroform . /ChloromethaneY tt"tt'yt ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Sun: 1,2-Dichlorobenzened4 Sun: Dibromofl uoromethane Surr: p-Bromdfl uorobenzene Sur: ToluenedS 44.4 0.020 0.053 o/o meq/L meq/L Calculation Calculation Calculation Analysis Date / By 11116107 14:38 / bws 11.n6n7 14:38 / bws 11116107 14:38 / bws 1'1105107 18:52 / dkh 11105107 18:52 / dkh 11105107 18:52 I dkh 11105107 18:52 / dkh 11105107'18:521 dkh 11105107 18:52 / dkh 11105107 18:52 / dkh 11lOSl07 18:52 / dkh 11105107 1E:52 / dkh 11105107 18:52 / dkh 11105107 18:52 / dkh 11lOSlO7 18:52 / dkh 11105107 18:52 / dkh 11105107 18:52 / dkh 11105107 18:52 / dkh - The ion balance is not appropriate for near blank results. VOLATILE ORGANIC COMPOUNDS ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L ND ug/tND ug/LND ug/L103 %REC125 %REC111 o/oREC 98.0 o/oREC 20 1.0 1.0 1.0 1.0 20 't.0 't.0 10 1.0 1.0 80-120 70-130 80-120 80-120 SW826OB SW826OB SW826OB SW826OB SW826OB SW826OB SW826OB SW8260B SW826OB sw8260B SW826OB SW826OB sw8260B SW826OB SW826OB Report Definltions: RL - Analyte reporting limit. QCL - Quality control limit. MCL - Maximum contaminant level. ND - Not detected at the reporting limft. -2L- TRACK# CO7LLOO77 ENERGY LABORATOR-IE-5, INC ' 2393 Satt Cregk HlgQway (5260t) . PO. Box S2S8 . Casper WyA2602rott Free 8ffi.23i.0s1i ' s02.1 .itt : -Fax sbr.iii:165b":L;;i;;dr;;6y/Zl;.,;i-- *;r:;;;;bii,b.'*, I I I LABORATORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sampte lD: Denison Mines (USA) Corp 4th Quarter/Semi-Annual Groundwater c07101341-008 MW65 Report Date: 01/07/08 Coltection Date: 1Ol23lOZ 15:00 DateReceive d: 10126t07 Matrix: Aqueous Analyses Result Units Qualifiers RL MCU QCL Method 1 1 0.5 1 0.1 0.5 0.05 0.1 0.5 0.5 10D s.u. mg/L I I I I I T I I I T I Analysls Date / By ruAdon rous C/rbonateas CO3 picarbonate as HCO3 /catclum r / chtortoeV Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N Potassium Sodiufit sur/e IHYS|CAL PROPERTTES , /oH / sotio", TotatDissotved TDS @ 1Bo C METALS. DISSOLVED Arsenic Bbryllium Cadmium Chromium Cobalt Copper lron Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zinc ND mg/L409 mg/L522 mg/L 55 mg/L0.2 mg/L177 mg/L0.21 mg/L0.7 mg/L11.0 mg/L177 mg/L 1850 mg/L 423208 42320 B E200.7 A4500-Ct B 44500-F C E200.7 A45OG,NH3 G E353.2 E200.7 E200.7 A4500-SO4 E 11103107 12:39 / bas 11103107 12:39 / bas 11106107 19:2S / ts 11t01107 15:18 / tjt 10131107 21:46 tbas 11106t07 19:25 / ts 11lOSlO7 10:18 /jat 10129107 09:30 / jat 11106107 19:21 / ts 11106107-19:21 t E 11lOSl07 13:09 / zd 7.13 3200 0.01 5.0 0.50 0.50 25 10 10 30 1.0 10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 1.0 A4500-H B 10t27t0711:31 /bas42540C 1Ot2BtO713:43/bas I /RADToNUcLTDES - DrssoLVEDf / Gross Alpha minus Rn & U I Gross Alpha minus Rn & U precision (*) ND uglLND ug/LND ug/LND ug/LND ug/LND ug/L332 ug/LND ug/L 1420 ug/LND ug/LND ug/LND ug/L7.6 ug/LND ug/LND ug/LND ug/L 52.2 ug/LND ugtLND ugA E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E2oO.8 E900., E900.1 10131107 19:40 / bws 10131107 19:40 / bws 1Ol31lO7 19:40 / bws 10131107 19:40 / bws 10131107 19:40 / bws 10131107 19:40 / bws fil0dl0719;21lrs 10131107 19:40 / bws 10131107 19:40 / bws 10131107 19:40 / bws 10131107 19:40 / bws 10131107 19:40 / bws 10131107 19:40 / bws 10131107 19:40 / bws 10131107 19:40 / bws 1Ol31lO7 19:40 / bws 10131107 19:40 / bws 10131107 19:40 / bws 10131107 19:40 / bws 11113107 16:56 / crw 11113107 16:56 / crw 1.9 pCi/L 0'6 Pci/LI Report Definitlons: RL - Analyte reporting limit. ' QCL - Quality control limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant level. ND - Not detec{ed at the reporting limit.I I -1 6_.I|PAaTa+ 11o.t.t i1 2 A'l ENEROY LABO4ATO|IE-\ lilC " 2393 Saft Creek HigQway (82601) , P.O. Box 3258 , Casret W A2602rott Free fi8.23s.0sts " s0z2 'its " rax eoi.an.iale :risr;;6rii6yt :i;.*V-- ,*iiiiibiii6*, I T I LABOMTORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp 4th Quarter/Semi-Annual Groundwater c07101341-008 MW65 Report Dafc; 01t07t08 Gollection Date: 10t23107 1 S:00 DateReceive d: 10t26t07 Matrix: Aqueous Analyses TA QUALITY Balance (t 5) Anions Cations Solids, Total Dissolved Calculated TDS Balance (0.80 - 1.20) vgLATtLE ORGANIG GoMPOUNDS tone Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surr: 1,2-Dichlorobenzened4 Sun: Dibromofl uoromethane Sun: pBromofluorobenzene Sur: Toluened8 Quallfiers MCURL QCL MethodI I T t I I I t I t I I T 1.99 46.8 48.7 3010 1.06 % meq/L meq/L mg/L dec. % Calculation Calculation Calculation Calculation Calculation sw8260B SW8260B SW826OB SW826OB SW8260B sw8260B sw8260B SW826OB sw8260B sw826oB SW826OB sw8260B SW826OB sw8260B SW826OB Analysis Date / By 11107107 13:58 / bws 11107107 13:88 / bws 11107107 i3:SB / bws 11107107 13:SB / bws 11107107 13:58 / bws 10129107 18:10 t jk 10129107 18:10 t jk 10129107 18:10 t ltr 10131107 21:41 tjtr 10t29107 18:10 t jh 10129107 18:10 / jk 10t29t07 18:10 tik 10129107 18:10 /itr 10129107 18:10 / jtr 10129107 18:10 / jtr 102gt07 18;10 / jtr 10fr29107 18:10 / jk 10n9rc7 18:10 / jtr 10t29107 18:10 / jtr 10t29107 18:10 tjtr ND ug/LND ug/LND ug/L870 ug/LND ug/LND ug/L1.3 ug/LND ug/LND ug/LND ug/LND ug/L98.0 %REC101 %REC105 %REC101 %REC 20 1.0 1.0 100 1.0 20 1.0 1.0 10 1.0 1.0 80-120 70-130 80-120 8G120 Report Definitlons: RL -Analyte repoiling limit. QCL - Quality control limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant level..' ND - Not detected at the reporting limit.T I -17 -.FpAaraJl na1 1a1 aA1 I ENERGYLABonAToR-lE-s! INC'2393Saltcregf ltlg-Qway(s2601).Po. Boxs2SB , Casrer Wa2602rott Free 888.23s.0i15 . azzi 'qits-:-Fi ibi2ii:;'6ib"7c;;i;;A";;;syE;;'* *,r;:;;;;b;LL.'*, I I LABORATORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual c07110077-008 MWTO Report Date: Collection Date: DateReceived: Matrix: 01t07t08 10130107 14:35 11t02t07 AqueousI t I t I I Result Unlts Quallfiers RL Analysis Date / By l€3208 11t06rc7 fi:54 tbasA232OB 11tO6tOZ 14:54 tbasE200.7 11tlStOZ 1A:22 tts 44500-Ct B 11tOZlO7 11:09 i tjt A4500-F C 11tOStOt 13:4i / basE200.7 11llSlOZ 18:22 tts A4500-NH3 c 11t}6t}t 12:21 t jatE353.2 11tOAtOt 13:35 / jatE200.7 11tl1to7 18:09 / tse200.7 11l15/0718:09 / ts A4500-SO4 E 11tO6tO7 12:50 tzd 44500-H B 11tOStO7 10..34 I rw 42540 C llt}St}t 14:1J t rw MCUQCL Method IONS Carbonate as CO3 Bicarbonate as HCO3 Calcium Chloride Fluoride Magnesium Nitrogen, Ammonia as N Nitrogen, Nitrate+Nitrite as N ND 358 276 45 0.3 126 ND 6.3 7.5 88.6 919 7.31 s.u.1680 mg/L ug/L u9/L uglL ug/L ug/L ug/L ug/L ug/L ug/L ug/L uga ug/L ug/L ug/L ug/L uga ug/L ug/L uglL pCi/L 1 1 0.5 1 0.1 0.5 0.05 0.2 0.5 0.5 30 0.01 10 5.0 0.50 0.50 25 10 10 30 1.0 '10 0.50 10 20 5.0 10 0.50 100 0.30 15 10 1.0 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.7 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.8 E200.E E200.8 E200.8 E200.8 E900.1 mg/L mg/L mg/L mga mg/L mg/L mg/L mga mg/L mg/L mg/t Potassium Sodiumtr" /r".,"o. pRopERrES t/31,"r, rotarDissorved rDS @ 180 c I ffilft - DrssoLVED BerylliumI frffi; fobatt l/d;" ManganeseI ffi;Tn,,, SeleniumI ;ffi, Tin I I,IH'Ll IJH:ilffi:i;D'|ssoLVED ND ND ND ND ND ND ND ND ND ND ND ND 53.9 ND ND ND 9.71 ND ND 11109t07 20:52 / bws 1'll09t07 20:52 tbws 11109t07 20;52 / bws 11109107 20:i2 t bws 11l0gl07 2O:52 t bws 11l0gl07 20;52 / bws 11l15tlt i8:09 / ts 11109107 20:52 t bv,ts 11109101 20:52 t bws 11l0gl}7 20:52 / bws 11ligt07 20:52 / bws 11109107 20:52 / bws 11109107 20:52 / bws 11109107 20:52 / bws 11109107 20:52 lWts 11l0gl07 20:f2 / bws 11l0gl07 20:52 / bws 11109107 20:52 / bws 11l0gl07 20:52 / bws 11116107 14:24 I cwv I Report Definitlons: RL - Analyte reporting limii. QCL - Quality control timit. MCL - Maximum contaminant level. ND - Not detected at the reporting limit.I I _ 15_frDiivJl ^A11 a D - RL lncreased due to sample matrix interference. ENERGY LABOflATORIES, lNC. , 2393 Satt Creek Hr?hway (5260t) . pO. Box 3258 . Casper Wy A2602TollFree888.235.05/5 ' 307... -0515 , Fax 307.234.1639 ,-cisper@energytab.a wnnu.iheri\yho.conT I I Client: Project: Lab lD: Client Sample lD: LABORATORY ANALYTICAL REPORT Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual /c07110077-008 /MWTo v/ Report Date: 01/07i08 Collection Date: 10130/02 14:JS DateReceived: 1 1 llltll Matrix: Aqueous Analyses Result Units Qualifiers RL MCUQCL Method T I I I I I I I I I I t I t I ory{a ouar-lw 4/6 Bahnce 1* sy fnionsi,/cations 2.69 o/o 26.7 meq/L28.2 meq/L 1680 mg/L1.00 dec. Yo ND ug/LND ug/L2.4 ugA 2700 ugAND ug/LND ug/LND ug/LND ug/L ND ug/LND ug/LND ug/L102 %REC126 ToREC113 %REC100 %REc Solids, Total Dissolved Calculated TDS Balance (0.80 - 1.20) ivol_ATtLE ORGANTC COMPOUNDS Acdtone Be{rzene ClrUon tetrachloride\ dhbroform Vchloromethane Methyl ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Surr: 1,2-Dichlorobenzened4 Sun: Dibromofl uoromethane Sun: p-Bromofl uorobenzene Sun: ToluenedS 20 1.0 1.0 50 1.0 20 1.0 1.0 10 1.0 1.0 80-120 70-130 8G120 8G120 Calculation Calculation Calculation Oalculation Calculation SW8260B SW8260B sw8260B SW826OB SW826OB SW8260B SW826OB SV\A26OB sw8260B SW826OB SW826OB SW826OB SW8260B sw8260B SW826OB 11116107 14:37 tbws 11116107 14:31 I bws 11116107 14:31 tbws 11116107 14:37 / bws 11116107 14:37 tbws 11105107 17:341 dkh 11105107 17:341 dkh 1110510717:34 t dkh 11106107 15:11 /dkh 11105107 17:341 dkh 11105107 17:341 dkh 11105107 17:34 t dkh 11105t07 17:34 t dkh 11lOSlO7 17:i4 t dkh 11105107 17:341 dkh 11105107 17:34 / dkh 11105107 17:34 / dkh 11105107 17:341dkh 11lOSlO7 17:34 I dkh 11105107 17:34 t dkh Ahatysis Date / By Report Definltions: RL - Analyte reporting limit. QCL - Quality controt limit. D - RL increased due to sample matrix interference. MCL - Maximum contaminant levei. ND - Not detected at the reporting limit. I -1 1_LT ..lmi dtt-Il ^6q. n ^^-- -ENERGY LABOBATORI^E-5, INC ' 2393 Saft Creek Highway (82601) . PO. Box 3258 , Caspq WA2602TottFree888.235.05t5 .307.1 'jtr ,Faxs0rfu4.i63e :ci{riidei,irgytal;.;* ,";;;;;;;iirb.'*, I I T LABORATORY ANALYTICAL REPORT Client: Project: Lab lD: Client Sample lD: Denison Mines (USA) Corp 4th Quarter/Semi-Annual Groundwater c07101341-014 Trip Blank Report Date: 01/07i09 Collection Date: 10t25t07 Og:20 DateReceive d: 10lZ6t0Z Matrix: Aqueous Analyses Result Unlts Qualifiers RL MCU QCL MethodI I I I I I I I T t I I VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Sun: 1,2-Dichlorobenzene-d4 Surr: Dibromofl uoromethane Sur: pBromofluorobenzene Sun: ToluenedS ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L94.0 %REC93.0 %REC104 %REC100 %REC 20 1.0 1.0 1.0 1.0 20 1.0 1.0 10 't.0 1.0 80-120 70-130 80-120 80-120 SW8260B SW826OB SW826OB SW826OB SW826OB SWE260B sw8260B SW826OB SW826OB SW826OB SW826OB SW826OB sw8260B SW826OB sw8260B 1ot29lo7 13:39 / jtr 10129107't3:39 / jk 1o2gt07 13:39 / jtr 10129t0713:39 /jtr 10129107 t3:39 / jtr 10t29107 13:39 / jk 10129t07 13:39 / jtr 10129t07 13:39 /jk 10129t07 13:39 / jtr 1012910713:39 t jtr 10129t07 13:39 / jk 10129107 13:39 / jtr 10t29t07 13;39 / jtr 10129107 13:39 / jtr 10t29t07 13:39 / jtr Analysls Date / By I t T Report Deflnitlons: RL - Analyte reporting iimit. QCL - Quality controt limit. MCL - Maximum contaminant level. ND - Not detected at the reporting limit. _28_ TPAl.lT.lJA ttn.1 1n1 aA1 t -ENERGY LABOilATOR-|ES, lNC'-2393 Saft Creek HBlway (52601) . PO. tux 3258, Casret; W 82602rott Free M.Bi.asti " s0z1' .tsts . rax ao/iit.ifri :casrni6ei,iiwElii'* iifii]ibiiii*, I T Client: Project: Lab lD: Client Sample lD: LABOMTORY ANALYTICAL REPORT Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual c07110077-015 Trip Blank Report Date: 01/07/08 Gollection Date: 10/31/01 0l:51 DateReceive d: 1 1 t0Zt07 Matrix: Aqueoust Analyses Result Unlts Qualifiers RL MCU QCL Method Analysis Date I ByI I I I I t t I I I T t I VOLATILE ORGANIC COMPOUNDS Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methyl ethyl ketone Methylene chloride Naphthalene Tetrahydrofuran Toluene Xylenes, Total Sun: 1,2-Dichlorobenzened4 Surr: Dibromofl uoromethane Surr: p-Bromofluorobenzene Surr: ToluenedS ND ug/LND ug/LND uglLND ug/LND ug/LND ug/L ND ug/LND ug/LND ug/LND ug/LND ug/L102 %REC120 %REC120 %REC98.0 %REC 20 1.0 1.0 1.0 1.0 20 1.0 1.0 10 1.0 1.0 80-120 70-1 30 80-120 80-120 SW826OB sw8260B SW826OB sw8260B SW826OB sw8260B SW8260B SW826OB SW8260B SW826OB SW8260B SW826OB SW826OB SW826OB sw8260B 11lOSl07 12;59 / dkh 11t05i07 12:59 / dkh 11lOSl07 12:S9 / dkh 11105107 12:59 / dkh 11105107 12:59 / dkh 11105107 12:59 / dkh 11105107 12:59 / dkh 11105107 12:59 / dkh 11lO5lO7 12:59 / dkh 11lO5lO7 .12:59 t dkh 11105107 12:59 / dkh 11105107 12:59 / dkh 11105107 12:59 / dkh 11lOSl07 12:59 / dkh 11105107 12:59 / dkh Report Deftnltions: RL - Analyte reporting limit. QCL - Quality control limit. MCL - Maximum contaminant level. ND - Not detected at the reporting limit. T I _30_ TRACK# C07LL}O77 ENERGY LABoRAToR-l^Ejt! tMc ._zssa satt Qrgg[ Hlg-lway (s2601) . po. Box B2s8 , casper; w a2602TollFreeffi.235.05t5. s07., riti, Fax302.294.1639 co: vww,i6iigiao.'com I t I t N{ALWI CN- S U M MARY REPO RT January 07, 2008 Denison Mines (USA) Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: G07101341 ProjectName: 4thQuarter/Semi-AnnualGroundwater Energy Laboratories, lnc. received the following 14 samples from Denison Mines (USA) Corp on 1Ol26t2OOT for analysis. Sample lD Glient Sample lD Gollect Date Receive Date Matrlx Test JAN 1 4 20$8 L:;-""-"tt" ""'G' T I I c07101341-001 nfiN 27 10122107 14:15 10126107 Aqueous Metals by ICP/ICPMS, Dissolved Alkalinity QA Calculations Chloride Fluoride Nitrogen, Ammonia Nitrogen, Nitrate + Nitrite pH Gross Alpha minus Rn222 and Uranium Solids, Total Dissolved Sulfate SW8260B VOCs, Standard ListI co?1o1s41{02 MW 2 10123107 07:31 10126107 Aqueous Same As Above c07101341-003 MW24 10123107 08:05 10/26/07 Aqueous SameAsAboveIC07101341-004 lrrw 28 10123107 1O:50 10126107 Aqueous SameAsAbove c07101341-005 MW23 10123107 12:45 1O126107 Aqueous SameAsAbovetC071013/.1406 tvlw 12 10123107 1 4:22 10126lO7 Aqueous Same As Above C07101341-007 IvlW 26 1 0 l23l$7 1 5:OO 1o126107 Aqueous SameAsAbove t c07101341408 MW65 10l23lOT 15:00 10126107 Aqueous SameAsAbove c07101341-009 MW29 10124107 08:01 10126107 Aqueous SameAsAbove c07101341-010 MW30 10l24lOT 10:24 1012610l Aqueous SameAsAbovetc07101341-011 MW31 10l24lOT 12:35 10126107 Aqueous SameAsAbove c07101341{12 MW 32 1Ol24lO7 1 4:45 1O126lO7 Aqueous SameAsAbove I co?rols4iola nrw rE 10125107 08:20 10DBl07 Aqueous Same As Above C07101341-014 Trip Blank 10125107 08:20 10126lOT Aqueous SW8260B VOCs, Standard ListI I There were no problems wilh thg analyses and all data for associated QC met EPA or laboratory specificationsexcept rvftere noted ln the Case Nanative or Report. lf you have any questions rcgarding these tests results, ptease ca[. I ReportApprovedBy I -1-.nPArtra# r'n'tt n1 ?,a.1 nh:Rasrq^r.H (gpcorrqm/ ENERGYLABORATORES,INC. .2SgSSaftCreekHighway(52601)'P.O. Box3258 , Caspq WA2il2TollFree 888.235.05t5 ' 307.fu! 15 . Fax 307.2s4.1639 "'cisperaienergytai.coi- .w.iiiisiiab.con I I QA/QC Summary Report Glient Denison Mines (USA) Corp Project 4th Quarter/Semi-Annual Groundwater Report Date: 01/07/08 Work Order: C07101341 Result Unlts RL %REC Low Llmit High Limit RpD RpDLimit euatI I t t I Method: A?,3208 Sample lD: MBLK-I Alkalinity, Total as CaCO3 Carbonate as CO3 Bicarbonate as HCO3 Sample tD: LGS-{ Alkalinity, Total as CaCO3 Sample lD: G0710149E-00lAtlS Alkalinity, Total as CaCO3 Sample lD: C07101498-00lAi,tSD Alkalinity, Total as CaCO3 Method Blank ND mg/L ND mg/L ND mdl Laboratory Conhol Sample 5090 mg/L Sample Matrix Spike 300 mS/L Sample Matrix Spike Duplicate 301 mg/L Run: MANTECH_O71102A Run: MANTECH_071102A 90 110 Run: MANTECH_071102A 90 110 Run: MANTECH_071102A 90 110 0.2 1 1 Batctr: R92237 11102107 08:27 11102107 08:36 11102107 08:59 11102107 O9:OB 10 1021.0 1.0 1.0 105 t I I t Method: A23208 Sample tD: MBLK-I Alkalinity, Total as CaCO3 Carbonate as CO3 Blcarbonate as HCO3 Sample lD: LGS-I Alkalinlty, Tohl as CaCO3 Sample !D: C07101341-006BMS Alkalinity, Total as CaCO3 Sample lD: G07101341-006Bl,tSD Alkallnity. Total as CaCOS Method Blank ND mg/L ND mS/L ND mS/L Laboratory Conhol Sample 5120 mg/L Sample Mafix Spike 478 mg/L Sample Matrix Spike Duplicate 477 mg/L Run: MANTECH_071109A Run: MANTECH_071103A 102 90 110 Run: tu|ANTECH_O711034 90 110 Run: MANTECH_07l103A 0.2 1 1 Batch: R92251 1110310711245 11103107 11:53 11103107 12:16 1'110310712:23 1.0 1.0 1.0 90 110 0.2 10 101 101 10 I I I T Method: A2540C Sample !D: MBLK1-071028 Method Btank Solids, Total Dissolved TDS @ 1S0 C ND mg/L Sample lD: LCS1_071028 Laboratory Contol Sample Solids, Total Dissolved TDS @ 180 C 968 mS/L Sample !D: C07101341-001BMS Sample Mabix Spike Sollds, Total Dissolved TDS @ 180 C 3O4O mg/L Sample lD: G071013414018MSD Sampte Mabtx Spike Duplicate Solids, Total Dissolved TDS @ 180 C gO2O mg/L Run: BAL-1_0710288 Run: BAL-1_0710288 90 110 Run: BAL-1_07'|O28B 90 110 Run: BAL-1_0710288 90 110 Batch: 071 028_1_SLDS-TDS-W 10P810713:41 1012810713:41 102il0713:4,1 10128t07 13:410.5 10 t T Qualifiers: RL - Analyte reporting limit.ND - Not detected at tre reportng limlt -29- ENERoY LABORATORIES, lNC ,_2e% saft creek Hlg_hway (s260r) , po. Box J2iB , casper w a2602rottFreeaffi.21s.q5ts .s07.23! 'ts .Faxeoiiit.roSi :dirii6ei66yEli.,ii- .riiiiiisiirb.ro, T Glient: Project: QA/QC Summary Report Denison Mines (USA) Corp 4th Quarter/Semi-Annual Groundwater Report Date: 01/07/08 Work Order: C07101341 Resurt unrts RL %REc Low Lrmrt High L.mrt RpD RpDLimrt Quar i[ethod: Sample lD: Chloride Sample lD: Chloride Sample lD: Chloride Sample lD: Chloride 44s00-ct B MBLK9.O71,IO,lA c07101312.003AMS co7t01312.{,03AltSD LCS35.071101A Method Blank ND mg/L Sample Matrix Spike 104 mg/L Sample Matix Spike Duplicate 104 mg/L Laboratory Control Sample 3440 mg/L Run: TITMTION_071i01D Run: TITMTION_071101D 90 110 Run: TITMTION_O71101D 90 110 Run: TITMTION_071101D 90 110 Batch: 071 101A-CL-TTR-W - 1'110110712:42 11101t07 13:iO 11101t07 13:SSo.7 10 11lO1l0t 15:33 0.4 1.0 1.0 t t I I t I t I I t I I I I I Msthod: Sample lD: Fluoride Sample lD: Fluorlde Sample lD: Fluoride Sample lD: Fluoride A4500-F C MBLK.I LCS-2 c0710{341{'04BMS c07101341-004BMSD Method Blank ND mg/L Laboratory Conhol Sample1.00 mg/L Sample Maflx Splke 1.50 mg/L Sample Matrix Splke Duplicate 1.50 mg/L Run: MANTECH_O71031A Run: MANTECH_071091A 90 110 Run: MANTECH_07.|0glA 90 110 Run: MANTECH_07l031A 90 110 Batch: R92081 10131107 17:19 1013110718:44 1Ol31lO7 21:32 10131107 21:35 10 0.05 0.10 0.10 0.'t0 100 iilethod: Sample lD: pH A4SOO-H B lcvl_071027_1 lnitial Calibration Verlfi caton Standard 6.81 s.u.0.010 99 Analytlcal Run: ORIONSESA O71O2ZA 1Ql27lO710:48 10298 illethod: Sample lD: pH 44500-H B c07r01341-002BDUP Sample Duplicate 7.44 s.u.0.0't0 Run: ORIONSS 5A_07 1027 A Batch: 071027_1_pH-W 1012710t 11:180.4 10 I T Quallfters: RL - Analyte reporfng limlt ND - Not detected at the reporting limlt. -30- ENERQY LABORATOR!-EA -lNC .'_2393 Saft Creek Hiqhway (52601) . P.O. Box 3258 , Caspq W A2602TollFree8ffi.235.05t5 . J0z.2s -ts , Fax30z.2a4.fi3e .'cispeiaienergytai.co;- w*:;fr;;siab.'@* Glient: Project: QA/QC Summary Report Denison Mines (USA) Corp 4th Quarter/Semi-Annual Groundwater Report Date: 01/07/08 Work Order: C07101341 Result Unlts RL %REG Low Ltmlt Htgh Llmlt RpD RpDLlmit eua! Method: Alt500-NH3 G Sample lD: MBLK-1 Nitrogen, Ammonia as N Sample lD: LCS-2 Nitrogen, Ammonla as N Sample lD: G07101341-001CriS Nitrogen, Ammonla as N Sample lD: C07101341-001ClrSD Nitrogen, Ammonia as N Method Blank ND mg/L Laboratory Control Sample 21.3 mS/L Sample Matrix Spike 2.12 mg/L Sample MaEix Spike Duplicate 2.Og mg/L Run: TECHNICON_071 I 0SA Run: TECHNICON_071 1 05A80 120 Run: TECHNICON_071't 05A 80 120 Run: TECHNICON_071 1 05A80 120 Batch:A2007-11-05 1 NHg 01 11105/07 09:10 11l05lol09:12 1'1105107 09:54 11/05107 09:561.4 '20 0.02 0.20 0.050 106 59 15 I t T I I I t t I I I I I I t T T T Itlethod: A4500€O4 E Sample lD: LCS-i_071105 Sulfate Sample lD: MBLK-1_071105 Sulfate Sample lD: G07l0l3{1-O0lBMS Sulfate Sample lD: G07101341-001BMSD Sulfate Laboratory Control Sample 4880 mg/L Mehod Blank 0.8 msA Sample Mabix Splke 889 mg/L Sample Mablx Spike Duplicate 889 mg/L Run; TURB-2_071105A 102 90 110 Run: TURB-2_071105A Run: TURB-2_071105A 101 90 110 Run: TURB-2_071108A 101 90 110 Batch: 071 1 05_1_SO4-TURB-W 11105107 12:21 1110it07 12:26 'l1l06l0t 122i0 11lO5lOT 12:51 0.0 10 Qualifiers: RL - Analyte reportng limit. -31-fio^ a1v4 d/a11 i1 ) i 1 ND - Not detec{ed at the reportng llmlt. ENEflGY LABORATOBIES, lNC. '2393 Salt Creek Hrghway (52ffi1) . PO. Box 3258 . Casper nWA260ZTollFree888.235.0st5 , 3022e 'ts , Fax 302.2a4.r639 ,'chsper@energytab.coi- ,vw.iiiibiao.mn I ctient: Denison Mines (USA) Corp I Proiect: 4th Quarter/Semi-Annuat Groundwater - QA/QC Summary Report Report Date: 01/07/08 Work Order: C07101341 Result units RL %REc Low Limit Hlgh Ltmlt RpD RpDLtmit euatI I I t I I I I T Method: E200.7 Sample lD: LFB-1CP25315 Calcium lron Magnesium Potassium Sodium Sample lD: LRB Calclum lron Magnesium Potassium Sodium Sample lD: G07101309-019CIttS Calcium lron Magnesium Potassium Sodium Sample lD: G07101309-019CMSD Caldum lron Magneslum Potasslum Sodium Laboratory Fortified Blank 52.6 mg/L 1.93 mS/L 52.5 mS/L 49.5 mg/L 50.8 mg/L Mehod Blank ND mS/L ND mg/L ND mg/L ND mS/L ND mg/L Sample Matix Spike 98.1 ms/L 0.787 mg/L 60.6 mg/L 146 mg/L 94.8 mS/L Sample Mabix Spike Duplicate 97.2 mg/L 0.777 mS/L 60.0 mg/L 146 mg/L 97.4 mg/L Run: lCPl-C_071106A 0.50 0.030 0.50 0.50 0.50 0.04 0.002 0.04 0.08 0.06 0.50 0.030 0.s0 0.50 0.50 0.50 0.030 0.50 0.50 0.50 105 85 97 85 105 85 99 85 102 8s 94 70 91 70 98 70 101 70 80 70 93 70 89 70 96 70 100 70 85 70 Run: lCPl-C_071106A Run: lCPl-C_07110GA Batch: R92430 1110610713:49 11106107 14:02 11lOGlO717:57 11/06/07 18:00 20 20 20 20 20 125 125 125 125 125 Run: lCPl-C_071'106A 130 130 130 130 130 130 't30 130 130 130 0.9 1.3 1.0 0.3 2.7 ilethod: E200.7 I Xil:: rD: LFB-tcp253r5 I H]::rD: LRB Sample lDz C07110270{19BMS I c"uu, Sample lD: C07 1 10270-{rt gBIrlSD I Galcium Laboratory Forfffi ed Blank 51.1 mg/L Method Blank mS/L Sample MaEix Spike 1140 mgA Sample Makix Spike Duplicate 1130 mg/L Run: lCPl-C_0t1110A 102 85 125 Run: lCPl-C_071110A Run: lCPl-C_071110A 104 70 130 Run: lCPl€_0t1110A 103 70 130 2.3 Batc*r: R92662 11110107 07:47 11110107 08:01 11110107 13:27 11h0107 13:31 20 RL - Analyte reportlng limit ND - Not detected at ttre reporting limit. 0.7 -32- I *,",t "* T ENEBGY LABORATORIES, lNC. , 2393 Salt Creek Hi!,lhway (S?ffit) . pO. Box 32i8 , Casper yWA2602 Toll Free 888.235.05t5 ' 307.23,' -ts . Fax s02.234.fi3e .'cisper@energytab.coi wv.ifrirbiao.mn I I oient Denison Mines (USA) Corp Report Date: 01/07/08 Work Order: C07101341 QA/QG Summary Report Project: 4th Quarter/Semi-Annual Groundwatert t I I I I I Itlethod: E200.8 Sample lD: LRB Arsenic Cadmlum Chromlum Cobalt Copper Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Tin Uranium Vanadium Zlnc Mehod Blank ND mg/L ND mS/L ND mg/L ND mg/L ND mdL ND mg/L ND mg/L ND mS/L 6E-05 mg/L ND mg/LND mg/L 0.0003 mg/L ND mS/L 0.0001 mg/L ND mg/L ND mS/L 0.001 mg/L Laborabry Fortified Blank 0.0507 mg/L 0.0513 mg/L 0.0495 mS/L 0.0486 mg/L 0.0516 mg/L 0.0502 mg/L 0.0483 mS/L 0.00509 mg/L 0.0544 mgA 0.0508 mg/L 0.0491 mS/L 0.0212 mg/L 0.0504 mgA 0.0507 mg/L 0.0490 mg/L 0.0499 mdL 0.0521 mg/L Post Digestion Spike 0.0509 mg/L 0.0527 mg/L 0.0492 mg/L 6E-05 1E-05 4E-05 2E45 7E-05 3E-05 5E-05 8E-05 5E-05 0.0007 0.0002 3E-05 1E-05 6E-05 1E-05 3E-05 0.0003 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.00030 0.00't0 0.0010 0.0010 0.0't0 0.010 Run: ICPMS2-C_071031A Run: ICPMS2-C_071031A 85 11585 115 85 115 85 .t15 85 115 85 115 85 115 85 11585 115 85 115 85 11585 1158s '!15 85 115 85 115 85 115 85 115 Run: ICPMS2€_071031A 70 130 70 .t30 Batch: R92083 10131107 11:03 1Ol31lO7 11:10 1013'llo718-.11 I ffi:'o: LFB Cadmiumt 3ffi*' Copper I [":[T*" MolybdenumI }:ff:,, Sllver I I';:: I I;:""' Sample lD: G07101372-0itDilS4 T trfi,'; Cadmium 101 103 99 97 103 100 97 102 109 102 98 105 101 101 98 100 101 101 105 98 Result Units RL o/oREG Low Limit Htgh Ltmlt RpD RpDLimit Qual t ff:tr""ft."-*,*, T ND - Not detected at the reporting limit -33-ryPAnT{* r.n'71n,1 ?r,1 ENERGYLABOBATOBIEi lNC. ,2S9SSaltCreekHighway(52601) ,P.O. tux5258 . Caspu WA2602TollFree 8ffi.235.0515 ' 307,23 -/5 ' Fax 302234.1639 ,'casper@energytab.con ww.eheigylab.mm I I Gtient: Denison Mines (USA) Corp QA/QG Summary Report r ProJect 4thQuarter/Semi-AnnualGroundwater Report Date: 01/07/08 Work Order: C07101341 t Batch: R92083 10131107 18:11Sample lD: C07101372-011DMS4 I ::ffi" Copper LeadI il:HT""" MolybdenumI $:::,, ThalliumI vi* Anc Post Digestion Spike 0.0500 mg/L 0.0491 mg/L 0.0488 mg/L 0.0510 mg/L 0.0819 mg/L 0.00520 mg/L 0.0529 mg/L 0.0489 mg/L 0.0477 mg/L 0.0515 mg/L 0.0511 mS/L 0.0530 mg/L 0.0512 mg/L 0.0503 mg/L 0.0496 mg/L 0.0508 mg/L 0.0484 mg/L 0.0482 mg/L ..0.0472 mdL 0.0481 mg/L 0.0496 mg/L 0.0796 mg/L 0.00518 mS/L 0.0522 mg/L 0.0463 mS/L 0.0471 mg/L 0.0498 mg/L 0.0502 mgr1- 0.0522 mS/L 0.0495 mg/L 0.0501 mg/L 0.050 100 0.010 98 0.010 97 0.050 ,t02 0.010 97 0.0010 104 o.1o 103 0.050 98 0.0010 95 0.10 103 0.10 102 0.00030 106 0.10 102 0.010 94 0.0010 980.010 102 0.010 970.050 960.010 s40.010 95 0.050 990.010 92 0.0010 104 0.10 102 0.050 930.0010 94 0.10 100 0.10 100 0.00030 1u 0.10 99 0.010 94 1013110718:18 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Run: ICPMS2-C_071031A 70 130 70 130 70 130 70 130 70 130 70 ,t30 70 .t30 70 130 70 130 70 130 70 130 70 130 70 130 70 130 Run; ICPMS2€_071031A 70 13070 13070 13070 13070 13070 13070 13070 13070 13070 130 70 13070 130 70 130 70 13070 13070 13070 130 I Sample lD: C07101372-011DMSD4 Post Dlgeston Spike Duplicate Arsenlc t trHffi CobaltI :JJ* Manganeset ffffir,,, Nickel I il"""rrT UraniumI I,::"0'" 2.7 3.6 1.7 0.0 3.8 't.6 0.0 2.8 0.4 0.0 0.0 1.4 0.0 0.0 1.6 0.0 0.4 I I Result units RL %REc Low Limit High Llmit RpD RpDlimit euat I fftr""ffi,"-*"' I ND - Not detected at ttre reporting limlt. -34-rrrDa,1l.J6 f rl't1A1 al,1 ENERQY LABORATORIES, lNC, ,_2393 Salt Creek Highway (52601) , P.O. Box 3258 . Caspet WYS2602 TollFree888.235.05l5 " 307.23 -15 , Fax 307.234.1639 ,-casper@energytab.cotT wwehergytab.om Client: Project: QA/QC Summary Report Denison Mines (USA) Corp 4th Quarter/Semi-Annual Groundwater Report Date: 01/07/08 Work Order: C07101341 iilethod: E353.2 Sample lD: MBLK-I Nltrogen, Nltrate+Nibite as N Sample lD: LCS-2 Nitrogen, Nitrate+Nitrite as N Sample lD: G07101341-002CMS Nitrogen, Nitrate+Nitrite as N Sample !D: G07101341-002CMSD Nitrogen, Nitrate+Nifite as N Method Blank ND mg/L Laboratory Conhol Sample 2.37 mg/L Sample Mafix Splke 2.11 mg/L Sample Mabix Splke Duplicate 2.14 mg/L Run: TECHNICON_O7I 029A Run: TECHNICON_071 029A 90 110 Run: TECHNICON_O71029A 90 1,t0 Run: TECHNICON_0710294 90 110 0.03 0.10 0.10 0.10 10129107 o8:47 10/29/07 08:50 10129/07 09:05 10'29107 09:07 10 Result unlts RL %REG Low Limit High Limit RpD RpDlimtt eual Batch: 42007-1 0-29_1_NO3_01 T I I I I I I I I I I I t I T T T T Method: 8900.1 Sample lD: LCS-GA.0081 Gross Alpha minus Rn & U Sample lD: RB-GA-0081 Gross Alpha mlnus Rn & U Sample lD: C07101341.002A!,lS Gross Alpha mlnus Rn & U Sample lD: G07101341-OO9ADUP Gross Alpha minus Rn & U Laboratory Confol Sam pte 20.6 pCi/L Method Blank ND pCi/L Sample Matix Splke 15.4 pCi/L Sample Duplicate 1.13 pCi/L Run: TENNELEC-3_071 109A 98 70 130 Run: TENNELEGS_071 109A Run: TENNELEG3_O71 109A 86 70 130 Run: TENNELEG3_071 1 09A 1.0 Batch: GA-0081 1111310716:56 11/13/07 16:56 11/13/07 16:56 1111310716:56 104.20.0 1.0 3.8 Quallfienr: RL - Analyte reporting limlt. -35-TPAflTa# rrn71n1?al ND - Not detected at the reporting limlt ENERGY LABonAToB-l-E:rllNC. ._2393 satt creek Htghway (s2601) " po. Box 32i8 , caspr, w ez60eTollFree888.235.05/5 , 307.2q :ff " Fax 9022a4.t639 ,'cAsper@energytab.mq ww,eheigytab.com I I dient Denison Mines (USA) Corp QA/QC Summary Report r ProJect: 4th Quarter/Semi-Annual Groundwater Report Date: 01/07/08 Work Order: C07101341 t Sample lD: 102907_LCS_2 - Benzene I Carbontetr:achlorider chbroform I ilffit#'-"." Methylene chlorideI }il::1""" Tehahydrofuran t .tliilxlh,orobenzened4 Sun: Dibromofl uoromethane I *x;i;ilH:"robenzene I ::Hi"Jr,,02e07_i'rBLK_5I Carbon tehachloride ChloroformI ::'il;#"" Methyl ethyl ketone I ff;llT:*'"n." o'Xylene I n'Hil*" Sun: 1,2-Dichlorobenzene{4 T :Hffi:Hl:::ffi:il: Sun: ToluenedS I ;f*D: co7lor34i'oozEltrs Carbon tetacftloridet ::HIn" o-Xylene Laboratory Gontrol Sample 5.3 ug/L 5.4 uS/L 5.1 udl 6.4 udL 10 ug/L 49 ug/L 4.8 ug/L 4.6 ug/L 5.0 ug/L 52 ug/L 5.2 udL 15 udL Method Blank ND ug/L ND ug/L ND ug/L ND ug/L ND udl ND us/L ND ug/L ND ug/L ND ug/L ND ug/L ND udL ND ug/L Run: SATURNCA_O71029A 70 130 70 130 70 13070 130 70 130 70 130 70 130 70 130 70 130 70 130 70 130 70 130 80 120 70 130 80 .t30 80 120 Run: SATURNCA_07l029A 1.0 106 1.0 107 1.0 102 1.0 129 1.0 100 20 98 1.0 96 1.0 91 1.0 101 10 105 1.0 105 1.0 101 1.0 96 1.0 95 1.0 102'1.0 102 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 5 0.5 0.5 10129107 12:44 10/30/07 00:33 120 130 120 120 97 80 98 70 104 80 102 80 Sample Matix Splke 2300 ugA 2100 ug/L 3200 ug/L 22W ug/L 220fJ ug/L 100 114100 103100 115100 109100 109 Run: SATURNCA 071029A70 13070 130 70 130 70 130 Result Units RL %REC Low Llmtt High Llmit RpD RpDlimit eual I ",**-RL - Analyte reporting limit T ND - Not detected at tre reporting llmit -3 6- ENERGY LABORATOBIES, firtC. , 2393 Satt Creek Hiqhway (A260t) . pO. Box 3258 . Casoer. W A2602 Toll Free 888.235.0515 , 307.2€ rfi " Fax 30Z2s4. /639 .'chsper@energytab.or ,,ww.eheigytab.con QA/QC Summary Report Denison Mines (USA) Corp 4th Quarter/Semi-Annual Groundwater T I I I t I I t I T I t T T T Client: Project: Sample lD: G07101341-007EMS Toluene Xylenes, Total Sur: 1,2-Dichlorobenzene-d4 Sur: Dibromofl uoromethane Sur: p-Bromofluorobenzene Surr: ToluenedS Sampld lD: C07l0l34l-007EMSD Benzene Carbon tetrachloride Chloroform 6+p-Xylenes o-Xylene Toluene Xylenes, Total Sun: 1,2-Dichlorobenzene-d4 Sun: Dibromofl uoromethane Surr: p-Bromofl uorobenzene Sun: Toluene-d8 Sample Matrix Spike2200 ug/L 4400 ug/L Sample Matrix Spike Duplicate2300 ug/L 2000 ug/L3100 ug/L 2200 ug/L 2300 ug/L 2300 ug/L 4500 ug/L 100 111 100 109 1.0 98 1.0 91 1.0 100 1.0 100 100 117100 10r'too 110100 111100 116 100 114 100 1141.0 1051.0 , 91 1.0 103 1.0 100 Run: SATURNCA_O7I029A 70 130 70 130 80 120 70 130 80 120 80 120 Run: SATURNCA_O7I029A 70 130 70 13070 13070 13070 13070 13070 13080 12070 13080 12080 't20 2.8 2.O 2,8 2.2 6.4 2.8 4.3 0.0 0.0 0.0 0.0 Batch: R92018 10/30/07 00:33 1Ol3OlO7 01:11 20 20 20 20 20 20 20 10 10 10 10 Report Date: 01/07/08 Work Order: C07101341 RL %REC Low Ltmit High Limit RpD RpDLimit euat T T -41 -J' mraltz aAtlA{^rr RL - Analyte reporting limit.ND - Not deteded at the reporting limit. ENEBGY LABOHATORI^ES, -INC. '_2393 Salt Creek Hphway (52601) . PO. Box 32SB . Caspet W A2602Toll Free 888.235.05/5 , 302.2,( it5 . Fax 902.2a4.1639 , biswdenergyai.roi-- ,,t*.iii;siiab.con I I I I I I I I I I T I I I T I t E o7 tr oo E 9E E 3e,H -*EG rdEEP E#EE 8?sE s Fs$ $l $t h,hir.J- --, \$Jj ;sI iFi,g ea rcffiIesseo1fr uoneteOan' spltoSrsfloS-JatBffirry ' O g A S 14y :eitr{l qdueg sraulquo9Io Joqunil lEiIOlalo,l* la| '-ot->Idlcl(uloIr lol6lolE oI orl.I ok.trl:sEI O- aUtlr(U -IicEI .=E 6lpE;I o=5I 6 6qI 8.tst€b8I =1f, 6 I gfif I E 8E I EFEI 6E 5I O(Dc,I P.(l!'I Tr- -I EEEE.e 6E.E EoeF €EE EEge+EE6E .e<E iisEtE -ct ()l EEEJ €rHJE CI>: ql B3 EI EEE' fr e#E S-oE*sdur=s€!-a,-.9tr> a6o a;oIgoE =g(, Efoog grelclolEItxtxl>tllEJt,<> E lU<( dHEEgND trE tlf-o(,o E, {.aoo-'.J ETo&,-;(Eo.IE EE:<,tlre,(El>iE.oiHotJ C' $.o tra-oF -c) zotr otrFzUIo TUJo- =a) IE'l.ol!Elaii,lLe l3El(/,6 Eo -!JrrJ bl* trEtrEE-ct-o=lL q,Eooto.FeE .Ee8: EE. t,l{{ w 'g, U'o EE o.9os ENERGY LABOBATORIEE lNC. ' 2393 Salt Creek Htjghway (8260t) . PO. Box 3258 " Caspil WY A2602 Toll Free 888.235.0515 ' 307.2i 'tl| , Fax 307.234.t639 .'casper@energytab.orywwc,iieigytaO.con EP 9^E P Ee# -*Eo rdEEe E#EE8Esf; eIgiL o\a E66ctr rcffir(esseofiuolepEol spltoSBtps-tqeijm'rtY OgASlyly :ed[lepueg sroulEluoc Io EqunN o ul"\ \ .I s-S 0o ri G\A d ,4 IE,o6'1'!t o -9oc gr ol€letEIIIJ I 5..1>.. fiHEEEtrD frtr l!,t0)l=Ieii, leEgE Eo --curbt= f;qtrEE-cto5lL ItEooto.EfH Ee8x 8'E ldlo lotoI=lrlot;|'7tl>ldIcl(I,lol.c lol6lcl-lE {tI oP;< IEB;lb"kl (t, -l:gEl'-firol.8E;I o== I giEl€b8I -o o I Efi*IEsE ;FEE3Eooo€oE!t- -O= cf,3c,EsEEEE €EE 3EE.cloo>-AEcr=t,E 6Eita=dg ElEIt 9I € gEl EBHHra blJE CI>: aI H3 EI EEE' fre#E k-o EEgtoa'=sf:EF gIE>q,o dC'cgoE e(, E E(D(,c t,Lo()ot*.ooJ CToE, -(Eoa-f Gtr t,GG E'oi*!,a =o tl;o trt-G.Cc) oq) (U(L lu t ttL sE, HIJ H E C C E Eo C.cf HH E -\. ooo E' eeogi6= (U -= e.EL= 6)o (,,- ab Q)'E-q, EP P - cL'" | [d E 9csH;EEE =(,)E O =8?sEE $J..NHNrfrb\s-E r\o- lc\l do'l.E+ga- ovro(E66ctr+$ oc,oc(L -,v fitsEl-6trJ4o, r-o)'6t '=,a1 .re qp- Iesseo rfi uolgtoqo1- sprlosFlros rolBM ltv OgASlyly:ad{lepueg s.roulE0uoc lo FqunN urO*\S oo r- tts\A "- dT o.9 9 ii,LC 8E (,!;i JFEo J-rrJ bl*oQ?=o.=trE =_oO=tL(,ttsoaE-rreds E98xA-=(/)o- G.rilol.eIcl9lEIul I h ..1>.. 1b'Ed3 TftEE5trtr trtr =sE#s E Hf EitE -t- A tigo(l):f(, E .a aD Ec(U o ;(l)aEoo-.,=o x.Ee#eb'Blt(d^so(,,eE cc-li'-do6E; c,=f E g.Eo -G€b8-D (I)!2(l)(l,gE; E.8Ee >\EuE Ii-9Eoo=o(t,o-oDE'_oE c-lo(u(E=i =dE g EEo)E6ooc-ooO>.AE(UEEEEEg< b=gF EI €Erl E iil(B.!g otJ-C Cl>: 0llPo =loo=lfi H:loEtu-,^ot x{ ..i=o'-o.E {loc<d)EF=il;= aEE-ats,,2tr>(d6 U;ooc(UoEf .g()c.G too E ENEBGY LABoRAToBtEs,.tNC ._2393 satt creek HigQway (s260t) , po. Box s2s8 . casper, w a2602TottFree&B4.2?i.^,ts .sLz.z 'i/s .Faxeoi.ieaio1e :-d;r;;6r;;6rh6.r*-- ,,*;;;;;siirb.** t T I I T I I T I I I I I T t T T Workorder Receipt Checklist Energy Laboratories lnc Denison Mines (USA) Corp Login completed by: Amber Entrekin Reviewed by: Reviewed Date: Shipping container/cooler in good condition? Custody seals intac,t on shipping container/coolep Custody seals intac{ on sample botfles? Chain of custody present? Chain of custody signed when relinquished and received? Ghain of custody agrees with sample labels? Samples in proper container/botfle? Sample containers intac-t? Sufficient sample volume for indicated test? All samples received within holding time? Container/Temp Blank temperature in compliance? Water - VOA vials have zero headspace? Water - pH acceptable upon receipt? tilililililflfl iltilflil Itilf,ilililtrilffi flil c07101341 Date and Time Received: 1012612007 10:15 AM Received by: jm Carrier name: Next DayAir Yes fl Yes fl Yes I Yes [f Yes [l Yes fl Yes fl Yes fl Yes [f Yes fl Yes [l Yes I Yes [f No fI No fl No fI NoE NoI No fI No fI NoE No fl NoE NoE NoE NoE NotPresent I Not Present fl Not Present [l 0.2'C On lce NoVOAvials submitted NotApplicable tr g Contact and Conec{ive Action Comments: None -40- ENEROY LABoRAToB_lEs, tNC .2393 satt creek Highway (s2601) , po. Box 32iB , caspe4, wya260zTotlFree888.235.05t5 . 3022'-'15ts " Fax s022s4.fi3e , casperdenergltai."l--- *r*w.iiiibiab.bon Dale: 07-Jan-08 I I I I I I I t I I I GLIENT:Denison Mines (USA) Corp Projec* 4th Quarter/Semi-AnnualGroundwater Sample DeliveryGroup: CO71O1g41 CASE NARRATIVE THIS IS THE FTNAL PAGE OF THE LABORATORYANALYTICAL REPORT oRlctNAL SAMPLE SUBMTTTAL(S) Alloriginal sample submittals hav6 been returned with the data package. A copy of the submittal(s) has been includedand tracked in the data package. SAMPLE TEMPEMTURE COMPLTANCE: 4.C (r2.C) Temperature of samples received may not be coirsideie{ groogrly presgrye! by accepted standards. Samples that arehand delivered immediately after collection shall be considereo a6ceptaore if thlre is lvioence that the chilling processhas begun. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. PCB AMLYSIS USING EPA 505 Data reported by ELI using EPA method 505 reflects the results for seven individual Aroclors. when the results for allseven ane ND (notdetected), the sample meets EPA compliance criteria foiFfB;;;i#ft. SUBCONTMCTING ANALYSIS subcontracting of sample analyses to an outside laboratory may be required. lf so, ENERGY LABoMToRIES will utilizeits branch labor:atories-or qualified contract laboratories toittris service. Any such laboratories wilt be indicated wlthin theLaboratory Analytical Report. BRANCH LABOMTORY LOCAT]ONS eli-b - Eneqy Laboratories, Inc. - Billings, MT eli-f - Energy Laboratories, lnc. - ldaholalb, lDelig - Energy Laboratories, lnc. - Gillefte, Wyeli-h - Energy Laboratories, lnc. - Helena, MTeli-r- Energy Laboratories, lnc. - Rapid Cifu. SDeli-t - Energy Laboratories, lnc. - Coilege Siation, TX CERTFICATIONS: UsEPA: wYo0002; FL-DoH NELAC: EBt 641 ;Arizona: M0699; catifomia: oz1 lBcAOregon: WY200001 ; Utah: 307235051i; Mrginta: 00057; Wast i'ngton, C19Og ISO 17025 DISCLAIMER: The results of this Analyticat Report relate only to the items submifted for anatysis. ENERGY LABoMToRIES, !.Nc.- CASPER,WY certifies that certain method selections contained in this report meetrcqulrements as set forth by the above accrediting authorities. somJ results r"qu".t"o oi g,e client may not be coveredunder these certifications. All analysis data to be-submitted r-ol resuratorv enforiement sliorio Le certined in the samplestate of origin. Please veriff ELI's certificafion coverage by visitini www.bnergylab.com ELI appreciates the opportunity to provide you with ttris analytical service. For additional information and services visit ourweb page www.energylab.com. The total number of pages of this report are indicated by the page number located in the lower right comer. I I T I t I T -4L-rFptrrrTal6 rrA1 1rr.t1A1 o ;l ldl(l)l6toljluloILl.qlat>lqILl(Ulol-c lol6lolEoI 8f EI Oo--IPc)Y I q)- (Elod!oU)9E EF >F'-(UogE; o--l EiE-o!o(deu, =ro o) B E.EE19 o I =.8EE 8E3Eo(t,o-oEo-oE Ex30EEEE.Iq Eoe!gEE(,,E6qroEo ().o> A.ts(d=o E 6H 9t a=gP EI €EII E Fdrd .g olJ.C Cl>: ql B3 =lfi fi:loEiu E e,H E ff{-o EEgt-'n =E €,:EF.9tr>(6o g;6)oc(d o EJ .go '6 EoC) C tr oz tr ao Eooo ! t_ EEgEO E i6= E 9.E eEe# p _ o_." I (L d E BgsEJ E=6 5H;#E s Fs$ iN UN) $$r"ht,t rt^+il. {\r{t ( 6g i*,\: ,g *a fiyg punoreu]n1 leuloN O=HCVIIV =I3S rc qp- {esseo rfr' uo gep6el- sprros6lroS :apffi'rrY OEASlly:edlleldueg sloulBluog lo JoqunN t\4 lsulstlIrl^z.\')t:'q.5joA 6o E E (U to CLoIT IJ {t V) oo EI,1' oo'6 tr Br.olcI9l8IulILl>[J ..r- ---E Ed3 E-,HE,gtrn trr ii, L =o6 o ! Lo E 'E -oJoo CL E(U U'o o Lo- EoEoE o)-o o) E J TU I U' (U E oILEoo.otE (d'6oo-U) I Itf-o E Ect E -(tr E. C !, F H = B Ef ENERGY L/IBORATOilEE NC. " 2393 Salt Creek Highway (82601) . PO. Box 3258 . Caspec WY 82602 TollFree888.235.05l5 " 3071 -0515 " Fax 307.234.1639 " casper@energylab.c www.energylab.com ANALWICN- S U MMARY REPORT I January07,20oB T I Denison Mines (USA) Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C07110077 ProjectName: 4thQtrGroundwater/Semi-Annual I Energy Laboratories, lnc. received the following 15 samples from Denison Mines (USA) Corp on 11l2l2OO7 for analysis. Sample lD Cllent Sample lD Gollect Date Receive Date Matrix Test JAN i 4 2$00 -t-G-- ---r-----t*-----a' I I I c07110077-O01 MW 5 10129107 08:30 1 1102107 Aqueous Metals by ICP/ICPMS, Dissolved Alkalinity QA Calculations Chloride Fluoride Nitrogen, Ammonia Nitrogen, Nitrate + Nitrite pH Gross Alpha minus Rn222 and Uranium Solids, Total Dissolved Sulfate SW8260B VOCs, Standard ListIc07110077-002 MW 15 1$l29lo7 1o:57 11 102107 Aqueous Same As Above co7110077-O03 MW 14 1Ol29lO7 13:25 1 1 lo2l07 Aqueous SameAsAboveICO7110077-004 IvIVV 17 1Ol29lO7 15:40 1 1 l02lOT Aqueous SameAsAbove c07110077405 trrvv 19 1Ol3OlO7 08:35 11 102107 Aqueous SameAsAbove I c07110077-006 MW 18 10l30lo7 10:50 1 1l02l07 Aqueous SameAsAbove c07110077407 MW 4 1Ol3OlO7 14:35 1110?/07 Aqueous Same As Above c07110077408 MW70 1Ol3OlO7 14:35 1 1 lo2l07 Aqueous Same As AboveIc07110077-009 MW60 1Al3Ol07 14:18 1 1 lO2lOT Aqueous SameAsAbove c07110077-010 [/lvv63 1Ol3Ol07 1 5:OO' 1 1 102107 Aqueous SameAsAbovetc07110077.o11 MW3 10131 107 07 :10 1 1 102107 Aqueous Same As Above c07110077412 MW 3A 10131 107 07:51 1 1 102107 Aqueous Same As AbovetYo7ttoozzql3 Mw 11 1Ol3OlO7 14:10 11 l02to7 Aqueous SameAsAbove :,tr10077-014 MW 1 11tg1t}7 08;53 11t02tol Aqueous Same As Above @711 S,:Tfrpahnk . :g}tqi #,*mg,91/07 0T:51 11to2t07 Aqueous SW8260B VOCs, Standard ListI T I-ff ,Xfl:,.:""3[:'fl T$::I"-:ffiffi u'ffi:H lf you have any questions regarding these tests results, Olease iffi QC met EPA or laboratory specifications t ReportApprovedBy: I *.o, ze:*ffiT,Hf*./ -1-TRA(-K# co71 1 oo77 ENERCY LABORA1OHES, INC , 2393 Satt Creek Highway (52601) . P.O. tux 3258 , Caspq WA2602TollFreeffi8.235.05l5 ' 3022' t5l5 , Fax 302234.1639 .'cisperdenergytab.a. --,urw.ifiiigiat.@n I t QA/QC Summary Report Glient Denison Mines (USA) Corp Project 4th Qtr Groundwater/Semi-Annual Report Date: 01/07/08 Work Order: CO711O07Z I I I t I Method: A2320 B Sample lD: MBLK-I Alkalinity, Total as CaCO3 Carbonate as CO3 Bicarbonate as HCO3 Sample lD: LCS-I Alkalinity, Total as CaCO3 Sample lD: C0710098+002BMS Alkalinity, Total as CaCO3 Sample lD: G07100984-002BMSD Alkalinity, Total as CaCO3 Method Blank ND mg/L ND mg/L ND mg/L Laboratory Control Sample 5140 mg/L Sample Matrix Spike 277 mg/L Sample Matrix Spike Duplicate 280 mg/L Run: MANTECH_0711OSC Run: MANTECH_O7110SC 90 110 Run: MANTECH_O711OSC 90 110 Run: MANTEGH_0Z1iOSC 90 110 0.2 1 1 Batch: R92339 11105107 16:18 1110510716:26 1110510716:49 1110510716:57 100.9 1.0 1031.0 1.0 Result units RL %REc Low Lrmrt High Lrmrt RpD RpDlim* euar I I t t I I I T T Method: A23208 Sample lD: MBLK-I Alkalinity, Tohl as CaCOg Carbonate as CO3 Bicarbonate as HCO3 Sampte lD: LCS-I Alkallnity, Total as CaCOg Sample lD: G07110072.006AmS Alkallnlty, Iotal as CaCOg Sample lD: G07110077.006Att[SD Alkalinlty, Total as CaGO3 Mehod Blank ND mg/L ND mdL ND mS/L Laboratory Conbol Sample5060 mg/L Sample Matlx Splke 467 mg/t- Sample Mabix Spike Duplicate 468 mS/L Run: MANTECH_O71106A Run: [vIANTECH_071 1 06A 90 110 Run: MANTECH_0711064 90 110 Run: MANTECH_O711064 s0 110 0.2 1 1 Batch: R92418 11106107 11:09 lllO0lol 11:16 '1110610711:38 1110610711:45 10 1.0 1001.0 1.0 T T Quallflers: RL -Analyte reporting limit. -3 1- TRACK# C07110077 ND - Not detected at the reporting limit. ENERGY LABOEATORIES, INC " 2393 Salt Creek Highway (s2601) . PO. Box 32iB . Caspu W a2602TotlFree888.?J.i.0s/i , s0z2 1it5 " Fax s022a4.ff3e :-ciipeidenerg[al;.:r;-**rr;;;fr;;siirb.'*, I I QA/QC Summary Report Client: Project: Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual Report Date: 01/07/08 Work Order: C07110077I t I t t Method: A€,3208 Sample lD: MBLK-I Alkalinig, Total as CaCO3 Carbonate as CO3 Bicarbonate as HCO3 Sample lD: LCS-I Alkalinlty, Total as CaCO3 Sample lD: G07{10980-001AMS Alkalinity, Total as CaCO3 Sample lD: G07110980-001AMSD Alkalinity, Total as CaCO3 Method Blank ND mg/L ND mg/L ND mg/L Laboratory Control Sample 4980 mg/L Sample Mafix Spike 306 mg/L Sample Matsix Spike Duplicate 306 mS/L Run: MANTECH_071128A Run: MANTECH_O711284 90 110 Run: MANTECH_071128A 90 110 Run: MANTECH_071128A 90 110 0.2 1 1 Batch: R93480 1112810710:13 1'1128107 10:20 11128107 10:42 1112810710:51 100.1 1001.0 1.0 1.0 Resurt units RL %REc Low Lrmrt High Limit RpD RpDLlmit Quar 98 100 99 10 10 10 I I I I Method: A2540C Sample lD: MBLKI_071i05 Solids, Total Dissolved TDS @ 1BO C Sample lD: LCSl_07tt0E Solids, Total Dissolved TDS @ 180 C Sample lD: C07100984-002BMS Solids, Total Dlssolved TDS @ 1BO C Sample !D: C071009E4-002BMSD Solids, Total Dissolved TDS @ 180 C Method Blank ND mdL Laboratory Control Sample 984 mg/L Sample Mahix Splke 2280 mg/L Sample Mafix Spike Dupllcate 2230 mg/L Run: BAL-1_0711058 Run: BAL-1_07110S8 90 110 Run: BAL-1_07110SB 90 110 Run: BAL-1_07110S8 90 110 Batch:071105_1-SLDS-TDS-W 1110510714:08 1110510714i09 1110510714:10 11105N714:10 10 101 101 1.0 1.0 1.0 T I I I I Method: A[500-Cl B Sample lD: MBLKS-011107A Chloride Sample lD: C07110077{05AMS Chlorlde Sample lD: C0711007Z.0OSAilSD Chlorlde Sample lD: LGS3$071107A Chloride Mehod Blank ND mS/L Sample Maflx Spike 97.9 mS/L Sample Matix Spike Duplicate97.9 mg/L Laboratory Contol Sample 3510 mg/L Run: TITMTION_071107A Run: TITMTION_O71107A 90 110 Run: TITMTION_O7I107A 90 110 Run: TITMTION_071107A 90 110 Batch: 071 1 07A-CL-TTR-W 1,t/02/07 09:38 11l0tte7,tO:iS 11l07l0t 10:580.0 10 11107107 13:21 T I Qualifiers: RL - Analyte reporting limit. -32-.I|RAl:rT{# Anl 11nO'7.7 ND - Not detected at tre reportng limit. EilERGY LABORATOHEA lNC. ' 2393 Salt Creek Hrlqhway (82601) . P.O. Box 32i8 , Caspu ttw A2602TollFree888.235.05l5 " 307.2 't515. Fatr307.234.1639,-cisprdenergytab.cq yww.ifreisylaO.con QA/QC Summary Report Gllent: Project: Denison Mines (USA) Corp 4th Qk Groundwater/Semi-Annual Report Date: 01/07/08 Work Order: C07110077 Result Unlts RL %REc Low Limit High Lrmit RpD RpDLlmrt euar Method: Sample lD: Fluoride Sample lD: Fluoride Sample lD: Fluoride Sample lD: Fluoride M500-F C MBLK.I LCS.2 c0711005S,006A1rs c07110055.006AMSD Method Blank ND mS/L Laboratory Conbd Sample 1.06 mg/L Sample Makix Spike 1.59 mg/L Sample Matix Spike Duplicate'1.59 mg/L Run: MANTECH_O7I10SA Run: MANTECH_O7110SA 90 110 Run: MANTECH_O7110SA 90 110 Run: MANTECH_O7110SA 90 110 Batc*r: R92313 1 1/05/07 09:10 1110510710:38 1110510712:52 11105107 12:55 10 0.05 0.10 0.10 0.'t0 106 105 0.0 Method: Sample lD: pH A4sOO.H B !cvt_071105_1 lnltial Calibration Verifi cation Standard 6.92 s.u. 0.010 98101 Analytical Run: ORIONSSSA 0711OSA 1110510710:22 102 I I I I I t t I I T I t t T T T I I It[ethod: Sample lD: pH A4sOO.H B c07110077-010ADUP Sample Duplicate 5.96 s.u.0.010 Run: ORION555A_071 10SA Batch: 071105_1_PH-W 1110510710:40 0.0 10 tlethod: Adlt00-NH3 c Sample lD: MBLK-I Nltrogen, Ammonia as N Sample lD: LCS-2 Nibogen, Ammonia as N Sample !D: G0711005$00SEMS Nibogen, Ammonia as N Sample lD: G07110055-O05EilSD Nihogen, Ammonia as N Batch: 42007-1 1 -06_1_NH3_01 Mehod Blank 0.03 mg/L Laboratory Conbol Sample . 20.8 mg/L Sample Mabix Splke 2.41 mdl Sample Mabix Splke Duplicate 2.43 mg/L Run: TECHNICON_O71 1 06A Run: TECHNICON_O7I 1 06A80 120 Run: TECHNICON_07l 1 06A 80 120 Run: TECHNICON_O71 1 06A80 120 0.8 0.20 0.050 11lOGl07 11:07 11/06/07 11:09 111061071'l:51 11/06/07 11:53 2099 Qualifiers: RL - turalyte reporting limlt. -33- TRACK# COlLLOO77 ND - Not detected at the repoiling limit. ENERGY LABORATORIES, lllC. . 2393 Salt Creek Highway (5260t) , PO. Box S2i8 , Casoer W A2602TolFree884.235.05ts , a07.i 't1ts . Fax g0z.ea4.t639 .-cisper@energytab.a ,,vww.eherbytao.con I I QA/QC Summary Report Glient: Project: Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual Report Date: 01/07/08 Work Order: C07110077 1.5 59 ND T I I t I Method: Sample lD: Sulfate Sample lD: Sulfate Sample lD: Sulfate Sample lD: Sulfate 44500-504 E LCS-1_071106 MBLK-1_071106 c07fi0077.004A!rs G07110077.004AMSD Laboratory C;onhol Sam ple 5030 mg/L Method Blank mg/L Sample Matrix Spike 4600 mg/L Sample Mabix Spike Duplicate 4530 mS/L Run: TURB-2_071106A't05 90 110 Run: TURB-2_0711064 Run: TURB-2_071106A 109 90 110 Run: TURB-2_071106A 105 90 1'to Batch: 071 106_1_SO4TURB-W 11t06t07 10:14 1110610710:15 11106/07 11:59 11106107 12:01 10 Result units RL %REc Low Llmtt High Limit RpD RpDLtmit eual 84 87 90 96 89 t I I I T I I I I Method: Sample lD: Calcium Magnesium Potassium Sodium Sample lD: Calcium Magnesium Potassium Sodium Sample lD: Calcium lron Magnesium Potassium Sodlum Sample lD: Calcium lron Magnesium Potassium Sodium E200.7 LFB-ICP25315 c07{10330-002DMs c07r10330{02DMSD Laboratory Fofffied Blank 57.4 mg/L 56.2 mS/L 52.8 mg/L 54.6 mg/L Method Blank ND mg/L ND mg/L 0.2 mg/L ND mg/L Sample Matix Spike 145 mS/L 0.437 mdL 70.3 mg/L 146 mS/L 70.5 mg/L Sample Matrlx Splke Duplicate 146 mdL 0.463 mg/L 70.6 mg/L 147 mg/L 70.7 mS/L 0.50 0.50 0.50 0.50 0.04 0.04 0.08 0.06 0.50 0.030 0.50 0.50 0.50 0.50 0.030 0.50 0.50 0.50 '115 112 105 109 Run: lGPl-C_071115A 70 13070 13070 130 70 130 70 130 Run: lCP14_071115A 8s 70 13092 70 13091 70 .t3o 96 70 130 89 70 130 Run: lCPl-C_071115A 85 125 85 125 85 125 85 125 Run: lCPl-C O71115A Batch: R92939 1111510711:42 11115107 11:56 11115107 19:12 11115107 19:15 20 20 20 20 20 0.3 6.0 0.4 0.1 0.3 I I Quallfters: RL - Analyte repordng limit. -34- TR,ACK# CO7LLOO7l ND - Not detected at the reporting limlt. ENERGY LABORATOEI_ES, INC '-2393 Saft Creek Hfighway (52601) . PO. Box 3258 , Caspec W 52602Toll Free 888.235.0515 ' 307.i ',515 , Fax 307.234. /639 .'cisperdenergytaO.ct- - tvvw.iiiibiaO.mn I I Glient Denison Mines (USA) Corp Project 4th Qtr Groundwater/Semi-Annual QA/QC Summary Report Report Date: 01/07/08 Work Order: C07110077 I I ;"*";,,;; ArsenicI ::H"'# Chromium I dff:, ManganeseI #:ifrI"",* NickelI ilT; I Ji::,; Znc I ffi,;.,: LFB l#ffi CobaltI ::j;- Manganese t il:rfr;"",, Seleniumt ffi;,,, Tln T Yfl';,T, Zlnc I ru;.: D: Go7r1oo4e-{,o2Drs4 Method Blank ND ND ND ND ND ND ND ND ND 5E45 ND ND 0.0006 ND 0.0001 ND ND 0.001 mg/L mg/L mg/L mdL mdL mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L m9/L mg/L mdL mdL Laboratory Fortifi ed Blank 0.0496 mg/L 0.0486 mdL 0.0508 mg/L 0.0496 mg/L 0.0497 mg/L 0.0499 mg/L 0.0514 mg/L 0.0497 mg/L 0.00519 mg/L 0.0509 mg/L 0.0497 mS/L 0.(M95 mg/L 0.0195 mdL .0.0514 mg/L 0.05'15 m/L 0.0512 mdL 0.0498 mg/L 0.0515 mg/L Post Digestion Splke 0.0524 mg/L 6E-05 3E-05 1E{5 4E-05 2E-05 7E-05 3E-05 5E45 8E-05 5E-05 0.0007 0.0002 3E-05 1E-05 6E-05 1E-05 3E-05 0.0003 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.00030 0.0010 0.0010 0.0010 99 97 102 99 99 100 103 99 104 102 99 99 94 103 103 142 100 101 102 Run: ICPMS2-C_071109A 1110910713:04 1110910713:10 11109107'19:04 Run: ICPMS2€_071109A 85 115 85 115 85 115 85 115 85 115 85 1.t5 85 115 85 115 85 115 85 115 85 115 85 1,t5 85 115 85 115 85 115 85 115 85 115 85 115 Run: ICPMS2-C_071109A 70 130 Result Units RL %REC Low Limit High Llmit RpD RpDltmlt eual Batch: R92603 I ff-"lffi; reportns rimit. t -35- TR,ACK# CO7LLOO17 ND - Not detec-ted at the reporting limlt. ENERGY LABOBATOR-I-E-5, INC " 2393 Satt Creek Highway (52il1) . PO. Box J2i8 , Caspet WyA2602TollFree8ffi.235.05t5 , 307.i 't5/5 . Fax gq7.274.tObs "'cispeicienergylai.i- - w*w.;;;ii1ia:b.:@n I I Glient. Denison Mines (USA) Corp Project: 4th Qtr Groundwater/Semi-Annual QA/QC Summary Report Report Date: 01/07/08 Work Order: C07110077 I I I I I I I Sample lD: C0711004$002DMS4 Beryllium Cadmium Chromlum Cobalt Copper Lead Manganese Merorry Molybdenum Nickel Selenium Silver Thallium Tln Uranium Vanadium Zinc Post Digestion Spike 0.0537 mS/L 0.0517 mg/L 0.0502 mS/L 0.0483 mg/L 0.0480 mg/L 0.0522 mg/L 0.0565 mg/L 0.00531 mg/L 0.0524 mg/L 0.0472 mg/L 0.0510 mS/L O.O2O2 mS/L 0.0524 mS/L 0.0518 mS/L 0.0549 mg/L 0.0505 mg/L 0.0516 mg/L Run: ICPMS2-C_071109A Batch: R92603 11fi9107 19:04 0.010 0.010 0.050 0.010 0.010 0.050 0.010 0.0010 0.10 0.050 0.0010 0.010 0.10 0.10 0.00030 0.10 0.010 107 70 103 70 99 70 96 70 95 70 104 70 98 70 106 70 104 70 94 70102 70101 70 105 70103 70108 70101 7097 70 130 130 130 130 130 130 130 130 130 130 130 130 130 130 130 130 130 I Sample lD: G07110049.002DMSIN post Digestion Spike DuplicateI Arsenic O.OS31 mg/L O.OO1OI Beryllium O.OsIE mg/L O.O1OCadmlum O.OS13 mS/L O.OIO I Chromlum O.oSO3 mg/L 0.OSOI Cobalt 0.0491 mg/L O.O1Ocopper 0.0487 mg/L o.o,to I Lead 0.0528 mS/L 0.050 I Manganese O.OS73 mg/L O.OIOMercury O.O0s41 mg/L O.OOIO I Molybdenum O.OO2S mS/L O.1OI Nickd 0.0481 mg/L O.OSOI Selenium O.oSO9 mg/L O.OOIOSilver 0.0199 mg/L O.O1O I Thanlum 0.0031 mg/L 0.10I Tin 0.0513 mg/L o.1oUranlum O.OSOZ mg/L O.OOO30 I Vanadium 0.0511 mg/L O.1O ! Zinc 0.0529 ms/L o.O1o 103 109 103 99 98 97 105 99 108 104 96 102 99 106 142 109 102 99 1.3 1.1 0.9 0.1 1.6 1.4 1.1 1.4 1.8 0.0 0.0 0.2 1.8 0.0 0.0 1.4 0.0 2.6 Run: ICPMS2-C_071109A 70 130 70 130 70 130 70 130 70 130 70 130 70 130 70 130 70 130 70 13070 130 70 130 70 130 70 130 70 ,t30 70 .t30 70 13070 130 11l09lOl 19:11 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 I Result Untts RL %REC Low Limit High Limlt RpD RpDllmlt eual I ff:Ifffireporrinsrim*. _36_ TRACK# CO7ttOO77 I ND - Not detected at the reporting limtt. ENERGY LABORATORIES, lNC. . 2393 Salt Creek Highway (52601) , PO. Box 3Ps8 . Casper W e2602TollFree888.235.05l5 " 307.{ ',s15,Fax902.2?4./fr9 "cisper@energytab.a wwwifiiigytao.mm QA/QC Summary Report Client: ProJect: Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual Report Date: 01/07/08 Work Order: C07110077 Method: E353.2 Sample lD: MBLK-I Nitnogen, Nitrate+Nitrite as N Sample lD: LCS-2 Nitrogen, Nihate+Nitrite as N Sample lD: C071100774038MS Nitrogen, Nitrate+Nitdte as N Sample !D: C07110077-003BilSD Nitrogen, Nitrate+Nitrite as N Mehod Blank ND mg/L Laboratory Confol Sample 2.43 mg/L Sample Matrix Spike 2.11 mg/L Sample Mabix Splke Duplicate 2.13 mS/L Run: TECHNICON_O7'I 1 08A Run: TECHNICON_O71 108A 90 110 Run: TECHNICON_071 1OeA 90 110 Run: TECHNICON_O71 108A 90 110 0.9 Batch: A2007-1 1 -08_1_NO3_ol 11/08/07 13:00 1110810713:03 1110810713:17 11108107 13:20 10 0.03 0.10 0.10 0.10 Result Unlts RL %REC Low Limit High Ltmlt RpD RpDLlmit eual T t I I I I t I I I T I I T T T T t Method: E900.t Sample lD: LGS-GA.0082 Gross Alpha minus Rn & U Sample lD: MB-GA-0082 Gross Alpha minus Rn & U Sample lD: C07110077-003DMS Gross Alpha minus Rn & U Sample lD: C07110077-0llDDUP Gross Alpha minus Rn & U Laboratory Control Sample21.9 pCi/L Method Blank ND pCi/L Sample Matix Spike19.'l pCl/L Sample Duplicate 1.10 pCi/L Run: TENNELEG3_O71 1't gD 103 70 130 Run: TENNELEG3_O71 1 13D Run: TENNELEG3_O71 1 I 3D91 70 130 Run:TENNELEG3 071119D 1.0 Batch: GA-0082 1111610714:24 1111610714:24 1111610714:24 11t16107 16:02 129.6 1.0 1.0 Quallflers: RL - Analyte reporting limit. -37 - TRACK# A.O7 11o.n.17 ND - Notdetected atffre reporting limit. ENERGY LAB0RATORI^E9, INC . 239J satt creek Hlghway (a2601) . po. Box i2s8 , caspet w 82602TollFreeffi8.21s.1sti . 30zi ?sts 'Faxs0z2g4.to3e :-c;swdeneriyhi.a -*,r*:;;;;giiab.:rom I QA/QC Summary ReportI I I Client: Denison Mines (USA) Corp Projecft 4th Qtr Groundwater/Semi-Annual Method: SW8260B Sample lD: 0$Nov.07_MBLK_2 Run: GCMS2_07110SA Report Date: 01/07/08 Work Order: C07110077 11105107 10:23 11/06/07 03:36 s Acetone I 3llfflln""n,"no" ChloroformI fiffitiffi;* Methylene chlorideI |.T;I1""" Tetrahydrofuran I lilti[,"o, Sun: 1,2-Dlchlorobenzene-d4t :;l[#:]::r"Jil: I lHfl:"'',', 05'Nov''tt7-LGS-3 I $mff:"" m+p.XylenesI il:ilffi:H::ff Naphthalene I ffi[,*,"" XMenes. TotalI :il;ffi:fliffi:T:ff# Sun: pBromofl uorobenzene l t"-r"'ri "il',oorrror.n,Benzene I Carbon tetrachtortde Mehod Blank ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND udLND uS/LND ug/LND ug/LND ug/LND ug/L Laboratory Conhol Sample 47 ug/L 4.6 ug/L 5.8 udL 5.2 uS/L 5.8 ug/L 8.8 ug/L 52 ug/L 5.7 ug/L 3.5 ug/L 4.8 ug/L 52 ug/L 5.1 ug/L14 ugru 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 5 0.5 0.5 10'l 80 ,120 118 70 130112 80 120 96 80 120 Sample Matix Spike 2100 ug/L 2800 uS/L 5200 ug/L Run: GCMS2_071105A 70 130 70 130 70 13070 130 70 130 70 130 70 130 70 130 70 130 70 13070 130 70 13070 130 80 120 70 130 80 130 80 120 Run: GCMS2_07110SA 70 130 70 130 70 130 20 1.0 1.0 1.0 1.0 1.0 20 1.0 1.0 1.0 10 1.0 1.0 1.0 1.0 1.0 1.0 94 93 117 105 1't7 88 103 114 70 95 104 't02 90 106 118 118 99 106 138 128 100 100 100 Result Units RL %REC Low Limit High Limit RpD RpDLlmit eual I ffffi;:reportinsrimrt. S - Spike recovery outslde of advisory limlts. I ND - Not detected at the reporting limit. -38_ TRACK# eO711no71 ENERCY LABOBATORIES, lNC. . 2399 Salt Creek Highway (52601) . PO. Box 3ts8 " Caspet; W A2602TollFree888.235.05l5 , 302; ?515 , Fax 302234.1639 ,'cisper@energylab.ci wwwehergytab.mn QA/QC Summary Report I T I t I I I I I t I I I t t Client: Project: Denison Mines (USA) Corp 4th Qtr Groundwater/Semi-Annual Report Date: 01/07/08 Work Order: C07110077 Sample lD: G07110077-007EMS m+p-Xylenes o-Xylene Toluene Xylenes, Total Sun: 1,2-Dichlorobenzene-d4 Sun: Dibromofl uoromethane Sun: p-Bromofl uorobenzene Sun: ToluenedS - Spike recovery ls high for saveral ana$es. Sample lD: C07110077-007EMSD Benzene Carbon tetrachloride Chloroform 6+p.Xylenes o-Xylene Toluene Xylenes, Totral Sun: 1,2-Dichlorobenzene{4 Sun: Dibromofl uorome0rane Sun: p-Bromofluorobenzene Sun: Toluene-d8 - Splke recovery ls high for several analytes. Sample Makix Spike 1800 ug/L 2000 ug/L 2000 ug/L 3700 ug/L 100 88 70 100 98 70 100 100 70 100 93 70 130 130 130 130 11106107 04:17130 4.2 20 130 0.3 20 s 1.0 102 80 1201.0 124 70 1301.0 111 80 1201.0 100 80 120 This is a matrix related bias since the MS MSD pak both exhibit thls samE behavior y€t have an acceptable RpD. Sample Mahix Spike Duplicate 2000 ug/L 2800, ug/L 5200 ug/L 1900 ug/L 2100 ug/L 21oo udL 4000 ug/L 130 6.6 2070 130 Run: GCMS2 071105A 100 102 70 100 138 70 100 128 70 100 95 70 100 106 70 100 107 70 100 101 1.0 102 80 120 1.0 127 70 130 0.0 20 7.9 20 7.4 20 7.6 20 0.0 10 0.0 101.0 112 80 120 0.01.0 98 80 120 0.0 This ls a matrix related bias slnce the MS MSD pair both exhlbit this same behavior lrot havo an acceptable RpD, 10 10 RL %REC Low Limlt High Llmtt RpD RpDLimit euat Method: SW8260B Run: GCMS2 071105A 130 130 130 Batch: R92366 11106/07 03:36 T T Quallfiers: RL - Analyte reporting limlt. S - Spike recovery oubide of advlsory limits. _39_ TRACK# CO7ITOO77 ND - Not detected at the reporting limit. ENERGY LABORATORIES. tNC. '2393 Salt Creek Highway (52601) "PO. Box 3ze8 , Casper WA2602Toll Free 888.235.0515 , 307., ?sti , Fax 907.2s4. tobs , cisperdenergytab.a www.ifiiibiiab.con ld flgI: rf$ i$l# srEl* od i-lirs I O- lEs g ili FE [* i s [€ ef $IEEE rIfFq ]EE E trEE € JEE EitEa€llei E ilE$€ lE$$lfis b l;Is lf is l*--F tI5 =aLrB EsIPEt Eoo E -$ Es CL a \- C.oE*EI E + gEEle \g r{ -ts-lo r do uvo punoeurnlHsnu 6cI.9 orU)E C5sE T FElJ =-cgE 0a- g, s/to'Et Fti s.l N N\o $ J \3a sre rcseeqE uogqaoen sflp8/qlog rerBm.4yg g 71 9114y:edIleldtueg $eulBluoc lo JequlnN 00t.\:s H-t ,A/\tX tr =o 0(L E =Ebb€o.o LoIL E .g ETou.too-otr o ECIEo-ELI sg -OEii)J :iJllulE n#t sEu NE*"vtsOE &.8 aE-9 ()?to-d6tr JeE2 EEfig5u=u, TR.'ACK# CO7LLOO77 "lo -loo,(U(L dEHLo OH 8qt3,gP anCOP.JgcrEoH'T,E(, -^tET .g# haE-trf -OEO<a E€(EEl >Eltr6lo=lgElhsl =€ IoEltroloE IeE I.=G I .EH Iod'I HH I I T I I I I I I I t I I T I T I I ^lo Noo)o(L orr.El-oo* EE T,E*r9OYOP =EEEO sr*'tr,E(JI^c:oe'j= fl )o; --TE€ -oLO<frtr5CH(EE >€tr6A=1vEl{JLI'o8l -ol6EttroloE I?8, '.=r I .EH IoH I HH ENERGY LABORATORIES. tNC. ,2393 Salt Creek Highway (82601) ,PO. Box,an<4 , Caspu WY82O02TollFree888.235.05l5 " 307. 9515 " Fax 302234.16,19 .'cisper@energylab.c. www.eherfiytab.con sPn tlEcss' oEE.9 orAE c,.B:dEE^.'-o;ef;EEg I:E tu= 1..d€ s l€gf PIE:g€18 _o (lvl) punoreunl HSnu N\$ k+ v.slt3r ;4 -!m IBsseqE Xuom€GensprcSFtpgretegrly fr ueqquogprequnp = Bri r:(rF ^c+d{4 o ECLE€tr oE oEiiJ :E?En €g 5Ee N5€<u-(U =EOEo-=&EOE-9 (JEq< ,BE =d coiEo E.Eo'o 6 Efio EEfiB6u=o -41- tdrlo ilEIB ils:01 E'tr1 6 El# €EIT ;.lgps I O- tEg € tigfr il* e* *IHEE iIEBE 'lE;:{a=.E IE; E IEE € triE EU6rgilEo!, ilg= E ilEg€ I8E E l3s$ IEE E IEEE lf iH l*er elE =OL EE Ee Eo Eotoo E ENERGY LABORATOBIES tNC. . 2393 Salt Creek Highway (82601) . PO. Box 3^"8 . Caspet WY82602 Toll Free 8ffi.235.0515 , 307. 2515 , Fax 307.234.1639 . casper@energylab.a wwwenergylab.mm I I I I I I I I I I I I I I I I t Energy Laboratories lnc Wo rko rder Recei pt C h ecklist Denison Mines (USA) Corp Login completed by: Edith McPike Reviewed by: ReMewed Date: Shipping container/cooler in good condilion? yo M Qrstody seals intact on shipping container/cooler? yes M Grstodysealshtactonsanplebottles? yes ! Chainofcustodypresent? y* M Chain of custody signed w hen relinquished and received? yeu M Chainofcustodyagreeswittrsanplelabels? yes M Sarples inpropercontainer/bottle? yes M Sanplecontainers htact? yeu M Sufficientsanplevolureforindicatedtesl? yes M Allsanplesreceivedwi0rinhoHingtine? yes M Oontainerfferp Blankte[perature in conplhnce? ye fl Water-VoAvialshavezeroheadspace? yes M Water-pHacceptableuponreceipt? yeu EI tr IIIililffi !ilflffi ilil[IIffi flIffiIililil c07110077 Date and Time Receir,ed: 111212002 9:45 AM Receir,ed by: jm Canier name: Next Day Air llo E NoD t{o E Non NoE llo tr t{o tr t{o tr Nlo I tlo tr I{o E I'lo fI tlo E l.lot Flesent n l,lot Resent ! Nlot ftesent EJ 0.6'C On lce tlo VOA vials subnrtted tlotApplicabh tr Oontact and Oorrective Actbn @rrrents: None -42- TR,ACK# CO7LLOO77 ENERCYLABORATOBIES Toll Free 8ffi.235.0515 . 302 rNC. . 2393 Salt Creek Htghway (82601) . PO. Box ."^"8 , Caspet W 82602 0515 ' Fax 307.234.1639 " casper@energylab.c www:energylab.com Date: 07-Jan-08 I t T I T T I I t T I T I I t t t CLIENT: Denison Mines (USA) Corp ProJect: 4th Qtr Groundwater/Semi-Annual Sample Delivery Group: C07110077 CASE NARRATIVE THIS IS THE FINAL PAGE OF THE LABORATORYANALYTICAL REPORT oRIG|NAL SAMPLE SUBMTTTAL(S) All original sample submiftals have been returned with the data package. A copy of the submittal(s) has been includedand tracked in the data package. SAMPLE TEMPEMTURE COMPLTANCE: 4"C (r2.C) Tempgrature of samples rgcer-ved may not be considered properly preserved by accepted standards. Samples that arehand delivered immediately after collection shatl be considered atieptable if th-ere is evidence that the chifjlng pio;Lsshas begun. SOIUSOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. PCB ANALYSIS USING EPA 505 Data reported by ELI using EPA method 505 reflects the results for seven individualAroclors. When the results for allseven are ND (not detected), the sample meets EPA compliance criteria for pCg monitoring. SUBCONTRACTING ANALYSIS subcontracting of sample analyses to an outside laboratory may be requir.ed. lf so, ENERGY LABoRAToRIES will utilizeits branch laboratories or gualified contract laboratories foittris iervice.' Any such laboratories will be indicated within theLaboratory Analytical Report. BMNCH LABOMTORY LOCATIONS eli-b - Energy Laboratories, lnc. - Billings, MT eli-f - Energy Laboratories, lnc. - ldaho Falls, lDelig - Energy Laboratories, lnc. - Gillette, Wy eli-h - Eneryy Laboratories, lnc. - Helena, MT eli-r- Energy Laboratories, lnc. - Rapid Clty, SD eli-t - Energy Laboratories, lnc. - College Station, TX CERTFICATIONS: USEPA: WY00002; FL-DOH NELAC: E87641; Arizona: A20699; Catifomia: O2118CA Oregon: WY200001; Utah: 307235051S; Virginia: 00057; Washington: C1909 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submifted for analysis. ENERGY LABORATORIES, lNC. - CASPER,WY certifies that certain method selections contained in this report meetrequirements as set forth by the above accrediting authorities. Some results requested by the client may nol Oe covlieOunder these certifications. -All ?nalysis data to be submitted for regulatory enforiement sliould be certifi6d in ne iampfestate of origin. Please veriff ELI's certification coverage by visiting www.-energytab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit ourweb page www.energylab.com. The total number of pages of this report are indicated by the page number located in the lower right comer. _43_ TRACK# eO7110077 ,&g;,8 e Hgcss' Ya 6E mE ..+ ,itfi, qlr\bi{ (n :Fl \i: f-6 Jto'.v ll,M3 t,p- ' l \1 H\' (ElclL9 oltnE E I . AEEI Y 4 EEgI E t gE $lE \s \izHtl6 l o (lvD punorBunl HsnH s.l NIN N\o t, fv5 =- eta oEEdE: Js$O ^PsseolE X uollqaoenspilosFlosrelBm4Y g sJaulEluocloJsqurnN = ($\ Hu 00t.\o_$ aiFJ\A \ \u {st !a : o .9Lo-!tgtr oE o.,)ti.J L> =6ulIE ns9?iE= JCg NE.o < LE -EotrcLx&EAE-9 (J'6q< 8.H durin z o Efio gEEB rio oo,(to po a!trGo oo-o E9E;8.so E6 b.Ec-b;E.9 .EbiEgo-tb E.|€EEOoLolt o.!-coEEet o'=EiEa!E1tosC'"-o6oes$>46lE3 g< 6=o=Ello'aE8oa. €-sJ-c OEooE"IIJ Eo9 E8to=oE>abdoo9OEcF Et!6 oto(, E6o E5a,:() E.EEoo E I N o l-l o lE lPfr dH EE gF o EE Et<a E€IEE EEOEgE Eg F;?E -A CH I HH| dE6otALo oL tro U'ootrg, E,5eooLLooo Loou. )d .ctoooeoNco o Eo .co J E ID(E op oLo Fzeo. UJo IIJ o. N o 1.1 0) lfl lPo s E,g ei E E(ri F]oigr Ei FiFA -a EI I HE zzzsP* illgcgs' I 5*l8qtE:IaI u\ - or{E+diLlr$gE :[ /),- h z o (El -.5o,1s, H.E I EEE I eEEI ;E fi I* EEEIEt-o (lvD punoJBurnl Hsnu Aoll,-\$ k J.slt3r ,4 roqlo ^esseotE XuolletoEsn spttosFllosJetel rlv g OgnSMV:edlleldureg k \F58,Ltr-- \)t; ^x+dto, _5at\O o oLo.EgD oE (,QiiJ -I =oYE npP <a!= JEg NE€ o II (Uvtotro-x &H n EEfiB6E=o I I I I I T t T I I I T I I t 4th Quarter 2007 Water Level Measurements t0l3u07 - MWI - 67.92 MW2 - tt0.s2 MW3 - 83.69 MW3 (A) - 85.87 MW4 - 68.t4 MW5 - 107.38 MWl1 -92.33 MW12 - t09.25 MW14 - 104.68 MW15 -107.35 MWl7 - 78.89 MW18 -73.1r MWl9 - 50.83 MW23 -714.39 l|'{W24 - 115.48 MW25 -77.81 MW26 - Unable to get depth, measurement pipe is broken, needs replaced. MW27 - s4.93 MW28 -79.14 MW29 - 103.89 MW30 -79.44MW3t -7t.78 MW32 -78.54 tv02lo7 - MW20 -79.25 NNV22 - 67.97 Pt - 64.75 P2 - 12.66 P3 - 30.75 P4 - 52.37 Ps - 46.61 rolrot|T - MW4 -7s.t3 TW4-1 - 64.70 TW4-2-72.52 TW4-3 - 48.74 TW4-4 - 66.27 TW4-5 - 53.90 TW4-6 - 54.24 TW4-7 -70.77 TW4-8 -70.64 TW4-9 - 52.t7 TW4-10 - s5.20 TW4-11 - 66.49 TW4-12 - 37.55 TW4-13 - 54.tt TW4-14 -94.64 TW4-15 -74.t2 TW4-16 - 65.00 TW4-t7 -72.28 TW4-18 - 54.38 TW4-19 -71.66 TW4-20 -73.68 TW4-2r - 55.90 TW4-22 - 57.01 TW4-23 - 68.57 TW4-24 - 57.33 TW4-25 - 43.02 I I I I I I I I I PROPERTY r,J BOUNDARY \\ \\o) TUu ls /,/t- (,u)\rr, )- =( \/r///(, -1L( MW-18 45584 PtEZ-1 e 5591 2 f' PtEZ-3 e 5607 --: l[ .. //\\ /tll /t\\ /t- -;- _;1/ojis18 +5s35 TW4-23 33 PIEZA c 5538 J ''/ PtEZ-s c 5538 .:-+:-:-s: -r,/ Sszo -""'' 7 ,il,-,, 11 1\ 1\ $ \\\r MW-20\ a5461 54eo (N { + \\\ 0 SCALE IN FEET EXPLANATION perched monitoring well showing elevation in feet amsl temporary perched monitoring well showing elevation in feet amsl perched piezometer showing elevation in feet amsl perched monitoring well installed April, 2005 showing elevation in feet amd temporary perched monitoring well installed April, 2005 showing elevation in feet amsl temporary perched monitoring well installed May, 2007 showing approximlte elevation Mw-22 //-{5450 .//,//,//,// ,/,/,//,/l ofrj\6 MW.2O O saor O ssso //,//.// PtEZ-1e 559'l MW-31f ssrs $ sstz fr ssas NorES: Locations and elevations for Tw4-2g,Tw4-24, ana rw+-zs are approximate';Water level for TW4-6 is from the third quarter, 2007 // // //\\ -=ll 1l 1l 1l 1l ;l 1l 1l 1l 1l gl 1l 1l 1l 1l ;l 1l HYDRO GEO CHEM,INC. KRIGED 4th QUARTER, 2OO7 WATER LEVELS WHITE MESA SITE H :/7 1 8000/feb08/wt 1 007.srf III IITIIITII