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HomeMy WebLinkAboutDERR-2024-011791 Johnston Leigh, Inc. 1820 S Palomar Ln Kanab, Utah 84741 (801) 726-6845 CommonCents/Reports/2024 SIR 10/22/2024 October 22, 2024 Mr. Mark Crim DERR Project Manager Division of Environmental Response and Remediation P.O. Box 144840 Salt Lake City, UT 84114-4840 RE: Subsurface Investigation August 2024 CommonCents, 907 N 400 E, Harrisville, Utah Facility Identification No. 1200401, Release MSB Dear Mr. Crim: On behalf of Moyle Petroleum (Moyle), operating CommonCents Stores in Utah, Johnston Leigh, Inc. (JLI) has prepared this Subsurface Investigation Report (SIR) for additional work at the. CommonCents Store located at 907 N 400 E in Harrisville, Utah (Figure 1). The Site includes an operating CommonCents convenience store, retail gasoline and diesel dispensers, and a car wash (Figure 2). This report was prepared in part to satisfy the requirements of the Utah Division of Environmental Response and Remediation (DERR) in their letter to Moyle Petroleum Company (Moyle) dated October 30, 2023 (Attachment A). The work performed at the Site included drilling and installation of three groundwater monitoring wells, soil sampling from the soil borings, groundwater sampling of DERR required monitoring wells, and top-of-casing (TOC) survey to measure the first encountered groundwater elevation. Soil Borings and Groundwater Monitoring Wells Three soil borings were drilled and converted to groundwater monitoring wells on August 16, 2024. The locations are shown in Figure 2. Prior to drilling, Blue Stakes of Utah were contacted, and subsurface utilities were marked. In addition to Blue Stakes, each soil boring was cleared of utilities to a depth of approximately 5 feet below grade using Hydrovac technology because of reconstruction activities performed by both the former owner Flying J Inc and the City of Harrisville. Soil boring MW15, MW16 and MW17 were advanced by ET Technologies Inc. (ET) using push probe techniques consisting of a track mounted 7842 Geoprobe® rig. Standard Operating Procedures (SOP) for soil sampling and groundwater monitor well installation is described in JLI SOPs included in Attachment B. Total depths were 20 feet in MW15, and 15 feet in wells MW16 and MW17. Well MW15 is located in the area where more backfill was used to raise the Site during reconstruction in late 1990’s. The drilling logs and well construction diagrams are presented in Attachment C. Subsurface Investigation Report October 2024 CommonCents, 907 N. 400 E., Harrisville, Utah Facility Identification No. 1200401, Release MSB CommonCents/Reports/2024 SIR/10/20/2024 2 Soil Sampling One soil sample was collected from each soil boring above first encountered groundwater. Soil was screened using a photoionization detector PID every 1-foot below the hydrovac interval to total depth of the soil boring. PID measurements were all zero. Soil samples were compacted into laboratory containers, bagged in bubble wrap baggies and placed into coolers with ice. The soil samples were delivered to Pace National Laboratory (Pace), a Utah certified laboratory in Mt. Juliet, Tennessee. The groundwater samples were analyzed for compounds of concern (COC) that include diesel range organics (DRO) and gasoline range organics (GRO) using EPA Method 8015B, and methyl tertiary butyl ether, benzene, ethyl benzene, total xylenes, and naphthalene (MBTEXN) using EPA Method 8260B . Soil lithology in boring MW15 consisted of 8 feet of engineered fill underlain by 12 feet of silty clay. Groundwater was encountered in MW15 at 7 feet and extended down to 9.5 feet. Soil lithology in boring MW16 consisted of 5 feet of engineered fill underlain by 1 foot asphalt surface, underlain by 1 foot of fill, underlain by 4 feet of sandy silt, and underlain by 4 feet of silty clay. Groundwater was encountered in MW16 at 7 feet and extended down to 10 feet. Soil lithology in boring MW17 consisted of 8 feet of engineered fill underlain by 1 foot asphalt surface and underlain by 6 feet of silty clay. 12 feet of silty clay. Groundwater was encountered in MW17 at 8 feet and extended down to 10 feet. Each well was constructed following the SOPs in Attachment B and consisted of 2-inch diameter PVC 0.010-inch well screen and blank riser pipe. Screen intervals consisted of 20-5 feet in well MW15, and 15-5 feet in wells MW16 and MW17. Each well was developed and allowed to set 24 hours prior to groundwater sampling. The TOC relative elevation was surveyed for each new well using existing well MW5 TOC elevations a base. Groundwater Elevation JLI measured the depth-to-water in all wells using a Solinst water level meter that reads accurately to 1/100th of a foot. The field data measurements are presented in Table 1. Field notes are provided in Attachment D. The depth-to-water measurements were subtracted from the surveyed TOC elevations (arbitrary datum of 100 feet) to calculate the relative groundwater elevation at the site. The groundwater elevation data for August 27, 2024, was gridded using the Kriging method and contoured using Surfer™ (Version 15) contour program (Figure 3). Potential groundwater highs near well MW7 and groundwater low near well MW11 generally produced an approximate hydraulic gradient of 0.025 feet per foot (ft/ft) to the west on 8/27/2024. Groundwater Sampling The groundwater monitoring wells sampled on August 28, 2024, included MW-3, MW-5, MW9, MW-11, MW15, MW16, and MW17. Well MW2 could not be accessed due to the car parked on the well all day and the driver was not present to move the car. Additionally as per the DERR request, underground storage tank (UST) basin monitor wells HNW, HNE, HSW, and HSE were sampled. JLI purged groundwater from each well using a Subsurface Investigation Report October 2024 CommonCents, 907 N. 400 E., Harrisville, Utah Facility Identification No. 1200401, Release MSB CommonCents/Reports/2024 SIR/10/20/2024 3 peristaltic pump and dedicated polyethylene tubing. The wells were either low-stress purged, generally following procedures in Low Stress (Low Flow) Purging and Sampling Procedure for the Collection of Groundwater Samples from Monitoring Wells (US EPA, 2017); or purged dry and sampled the following day using a peristaltic pump and dedicated polyethylene tubing. The groundwater samples were collected in 40-milliliter pre-acidified bottles, bagged in bubble wrap baggies, and placed into coolers with ice. The groundwater samples were delivered to Pace National Laboratory (Pace), a Utah certified laboratory in Mt. Juliet, Tennessee. The groundwater samples were analyzed for COCs that include DRO and GRO using EPA Method 8015B, and MBTEXN using EPA Method 8260B. Soil Analytical Results MW15, MW16, MW17 The soil analytical results were all below COC Tier 1 values. The cumulative soil analytical results at the site are presented on Table 2. Laboratory reports are included in Attachment E. All the soil samples collected at the site are below Tier I values. Groundwater Analytical Results August 2024 UST basin monitor wells were non-detect for all compounds of concern (COC). MTBE was slightly above Tier I values in MW3 and MW5. Cumulative groundwater analytical results are presented on Table 1. August 28, 2024, specific groundwater analytical results are presented on Table 2. The laboratory analytical reports are included in Attachment E. The approximate distribution of dissolved benzene and MTBE on August 28, 2024, is presented in Figure 3. Groundwater samples which contained a COC above RBCA Tier 1 levels on August 28, 2024, include MTBE in well MW3 and MW5. The individual analytes detected above Utah ISL in addition to the analytes identified above include: • MTBE at 0.694 mg/l in well MW3 and 0.59 mg/l in well MW5 • Benzene at 0.0403 mg/l in well MW5 • GRO at 1.42 mg/l in well MW3, and 1.67 mg/l in well MW5 • DRO at 1.33 mg/l in well MW5, 1.08 mg/l in MW15, and 2.83 mg/l in MW17. The groundwater benzene and MTBE concentration vs time and linear trend line is plotted on Table 3. The groundwater elevation and benzene and MTBE concentrations vs time, and linear trend, in wells MW3 and MW5 are plotted on Table 4. JLI will have the laboratory fractionate DRO at the next sampling event that is anticipated to occur in November 2024. Based on the information in this report, the dissolved COC’s above ISL in groundwater, apart from potentially DRO, appear to may remain onsite. Subsurface Investigation Report October 2024 CommonCents, 907 N. 400 E., Harrisville, Utah Facility Identification No. 1200401, Release MSB CommonCents/Reports/2024 SIR/10/20/2024 4 If you have questions or require additional information, please contact me by phone at (801) 726-6845, or email at leigh@johnstonleighinc.com. Sincerely, Leigh Beem, P.G., CC 0199 Johnston Leigh, Inc. CC: Mr. Jim Sachs, Moyle Petroleum Attachments: Figure 1 Site Location Map Figure 2 Site Map Figure 3 Groundwater Potentiometric Isoconcentration Map 8/28/2024 Table 1 Soil Boring Sample Results Table 2 Cumulative Groundwater Analytical Results and Field Parameters Table 3 DERR Required Well Groundwater Sampling August 2024 Table 4 Benzene and MTBE Groundwater Concentrations vs Time Table 5 Groundwater Elevation versus COC Concentrations Attachment A DERR letter to Moyle dated 10/30/2023 Attachment B JLI SOPs Attachment C Boring Logs MW15, MW16, MW17 Attachment D August 27-28 Field Notes Attachment E Laboratory Reports 8/28/2024 FIGURES © OpenStreetMap (and) contributors, CC-BY-SA Johnston Leigh Inc.(801) 726-6845 PREPARED BY:DATE:PJS 01/28/2022 FIGURE 1SITE LOCATION MAP CommonCents907 N 400 EHarrisville, Utah ± 0 0.25 0.50.125 Miles CommonCents !U !U !U !U !U !U !U !U !U !U !U !U !U !U !U MW9 MW8 MW7 MW6 MW5 MW4 MW3 MW2 MW1 MW17 MW16 MW15 MW14 MW11 MW10 Johnston Leigh Inc.(801) 726-6845 PREPARED BY:DATE: PJS 10/21/2024 FIGURE 2 SITE MAP CommonCents 907 N 400 EHarrisville, Utah ± 0 50 10025 Fe et MONITORING WELLS/SOIL BORINGS/UTILITIES !. !. !. !. !. !. !. !. !. !. !. !. !. !. !. 0 .4 0.5 0.6 0 . 0 1 0.020.030.04 0 .0 1 91 8 8 90 92 89 9 3 9 0 . 5 91.5 8 8 . 5 89.5 8 7 . 5 92.5 8 7 9 3 . 5 9 0 . 5 91.5 9 1 9 2 . 5 MW9 MW8 MW7 MW6 MW5 MW4 MW3 MW2 MW1 MW17 MW16 MW15 MW14 MW11 MW10 FACILITY #1200401, RELEASE MSB FORMER FLYING J "C" STORE DBA Common Cents HARRISVIL LE, UTAH GROUNDWATER POTENTIOMETRIC AND ISOCON CENTRATION MAP AUGUST 2024 FIGURE 3 Drawn By: Date: File: Joshns ton Leigh Inc. (801) 726-6845 Job No.: pjs 10/21 /2024 £ 10 0 10 20 30 405 Feet Legend !.Monitoring Well Locations Groundwater Elevation Benzene Isoconcentration (mg/l) MTBE Isoconcentration (mg/l) TABLES TABLE 1 SOIL BORING SAMPLE RESULTS CommonCents, 907 North 400 East, Harrisville, Utah Facility 1200401, Release MSB Boring Sample TPH GRO*TPH DRO*Ethyl Total ID ID Date (C6-C10)(C10-C28)*MtBE Benzene Toluene Benzene Xylenes Naphthalene (mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg) 1 SB-B1 10/05/10 No soil sample due to shallow groundwater and daylight procedure 2 SB-B2-6.5 10/05/10 <0.57 <4.6 <0.0057 <0.0057 <0.028 <0.0057 <0.017 <0.028 SB-B2-10 10/05/10 0.65 <4.9 0.028 <0.0061 <0.031 <0.0061 <0.018 <0.031 3 SB-B3-6.5 10/05/10 <0.56 <4.5 <0.005 <0.005 <0.025 <0.005 <0.005 <0.025 SB-B3-10 10/05/10 <0.72 <5.7 <0.0072 <0.0072 <0.036 <0.0072 <0.022 <0.036 4 SB-B4-7 10/05/10 <0.64 <5.1 <0.0064 <0.0064 <0.032 <0.0064 <0.019 <0.032 5 SB-B5-7 10/05/10 1.5 <4.4 0.022 <0.0055 <0.027 0.01 0.085 0.091 SB-B5-9 10/05/10 <0.6 <4.8 <0.006 <0.006 <0.030 <0.006 <0.018 <0.030 6 SB-B6-6 10/05/10 <0.62 <5.0 <0.0062 <0.0062 <0.031 <0.0062 <0.019 <0.031 SB-B6-9 10/05/10 <0.60 <4.8 <0.006 <0.006 <0.030 <0.006 <0.018 <0.030 7 SB-B7-7 10/05/10 <0.61 <4.8 0.047 <0.0061 <0.030 <0.0061 <0.018 <0.030 SB-B7-9 10/05/10 <0.59 <4.7 0.036 <0.0059 <0.030 <0.0059 <0.018 <0.030 8 SB-B8-6 10/05/10 <0.66 16 0.12 <0.0066 <0.033 <0.0066 <0.020 <0.033 SB-B8-9 10/05/10 2.6 77 0.078 <0.0075 <0.038 <0.0075 <0.022 <0.038 9 SB-B9-9 11/02/10 <0.61 <4.9 0.15 <0.0061 <0.030 <0.0061 <0.018 <0.030 10 SB-B10-10 11/02/10 <0.64 <5.1 <0.0064 <0.0064 <0.032 <0.0064 <0.019 <0.032 11 SB-B11-12 11/02/10 <0.62 <5.0 <0.0062 <0.0062 <0.031 <0.0062 <0.019 <0.031 12 SB-B12-10 11/02/10 <0.61 <4.9 0.058 <0.0061 <0.030 <0.0061 <0.018 <0.030 13 SB-B13-6 05/16/11 <0.62 <5.0 <0.0062 <0.0062 <0.081 <0.0062 <0.019 <0.081 14 SB-B14-7 05/16/11 <0.64 6.1 <0.0064 <0.0064 <0.082 <0.0064 <0.019 <0.082 15 SB-B15-9.5 11/17/11 <10 <10 <0.005 <0.005 <0.025 <0.005 <0.015 <0.025 16 SB-B16-5 11/17/11 <10 <10 <0.005 <0.005 <0.025 <0.005 <0.015 <0.025 16b SB-B16b 9-10 01/13/16 90.5 38 <0.005 <0.005 <0.0275 0.00591 <0.0165 0.121 17 SB-B17 12.5-13.5 01/13/16 <0.631 <252 0.00988 <0.00631 <0.0315 <0.00631 <0.0189 <0.0315 MW15 SB-MW15 6-7 08/28/24 <4.83 <5.01 <0.0242 <0.00193 <0.00966 <0.00483 <0.0126 <0.0242 MW16 SB-MW16 7-8 08/28/24 <9.65 50.3 0.00617 <0.00386 <0.0194 <0.00965 <0.0251 0.0844 MW17 SB-MW17 9-10 08/28/24 <5.39 <5.13 0.0205 <0.00216 <0.0108 <0.00539 <0.0140 <0.0270 RBCA Tier 1 Values mg/kg 1500 5000 0.3 0.9 25 23 142 51 Utah ISL Values mg/kg 150 500 0.3 0.2 9 5 142 51 GRO Gasoline Range Organics DRO Diesel Range Organics <0.001 Concentration was less than the detection limit shown NS Not Sampled mg/L Milligrams per liter MTBE Methyl tertiary butyl ether BOLD Indicates concentration exceeds the Tier I Screening Levels CommonCents Harrisville, UT Page 1 of 1 10/22/2024 TABLE 2 CUMMULATIVE GROUNDWATER ANALYTICAL RESULTS and FIELD PARAMETERS CommonCents, 907 North 400 East, Harrisville, Utah Facility 1200401, Release MSB Well TPH GRO*TPH DRO*Ethyl Total Benzene Total Mass Depth to Groundwater ID Date (C6-C10)(C10-C28)*MtBE Benzene Toluene Benzene Xylenes Naphthalene Mass Water Elevation DO ORP Conductivity pH Temperature (mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/l)(feet)(ft above datum)(mg/L)(mv)(ms/m)© or (F) Monitor Wells MW1 10/08/10 0.82 1.7 0.48 0.086 <0.005 0.0068 0.019 <0.005 0.086 3.11 5.61 93.50 MW1 11/02/10 1 0.66 0.21 0.091 <0.005 0.0076 0.019 0.48 0.091 2.47 5.51 93.60 MW1 05/18/11 0.52 0.21 0.087 0.02 0.0081 0.0012 0.0039 <0.005 0.02 0.85 6.50 92.61 MW1 10/31/11 1.4 0.54 0.15 0.16 <0.025 0.01 0.1 0.025 0.16 2.39 5.57 93.54 0.2 -220.0 2.6 20.5 MW1 04/05/12 0.74 1 0.078 0.033 0.005 0.0024 0.015 0.005 0.033 1.88 5.12 93.99 0.3 NA 1.96 7.16 14.2 MW1 11/08/12 1 0.91 0.09 0.073 <0.005 0.003 0.021 <0.005 0.073 2.10 5.50 93.61 MW1 06/26/13 <0.50 1.16 0.124 0.027 <0.002 <0.002 <0.006 <0.002 0.027 1.31 5.66 93.45 MW1 03/31/14 0.45 0.67 0.051 0.012 <0.005 <0.001 <0.003 <0.005 0.012 1.18 5.43 93.68 0.2 -119.0 12.7 6.9 13.3 MW1 11/07/14 0.54 0.51 0.11 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 1.16 6.98 92.13 1.0 -133.0 3.87 7.38 20.9 MW1 11/11/16 0.436 0.326 0.091 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.85 5.54 93.57 0.9 -135.0 5.2 6.6 21.4 MW1 11/16/2017 0.618 0.572 0.138 0.00533 <0.00100 <0.00100 <0.00300 <0.00500 0.00533 1.33 6.55 92.56 6.3 -112.0 1.8 7.64 18.6 MW1 06/14/2018 0.792 2.39 0.103 0.00698 <0.00100 <0.00100 <0.00300 <0.00500 0.00698 3.29 5.63 93.48 1.2 -8.0 2.33 7.28 17 MW1 12/20/2018 0.266 6.02 0.0688 <0.001 <0.001 <0.001 <0.003 <0.005 0.001 6.35 5.62 93.49 3.1 79.9 1.7 7.8 16.1 MW1 07/20/19 0.555 1.58 0.109 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 2.24 5.67 93.44 MW1 04/09/21 0.126 0.839 0.0185 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 0.98 5.43 93.68 1.7 104.0 2.41 7.35 13.6 MW1 12/08/21 0.351 0.518 0.0493 <0.001 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.92 7.09 92.02 1.9 114.0 2.85 7.16 13.8 MW1 07/12/22 0.328 0.57 0.0637 <0.001 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.96 6.80 92.31 1.0 4.48 7.92 22.2 MW1 11/17/22 0.127 0.3 0.103 <0.001 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.53 7.67 91.44 0.3 -64.0 2.05 6.85 18.5 MW1 08/27/24 Not on sampling list DERR 10/30/2023 6.54 92.57 MW2 10/05/10 0.15 0.58 0.012 <0.001 <0.005 <0.001 0.051 0.0051 0.001 0.80 8.64 90.01 4.1 -62 0.6 7.1 20 MW2 11/02/10 0.13 0.83 0.042 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 1.00 9.21 89.44 MW2 05/18/11 11 25 0.65 1.2 3.6 0.072 0.57 <0.50 1.2 42.09 8.22 90.43 MW2 10/31/11 0.8 <0.100 0.026 0.0093 <0.005 <0.001 <0.003 <0.005 0.0093 0.84 8.20 90.45 0.28 -218 1.03 15.9 MW2 04/05/12 <0.100 <0.100 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 4.32 94.33 8.2 NA 0.5 7.19 13.1 MW2 11/08/12 1.6 0.21 0.045 0.03 0.013 0.0016 0.0042 <0.005 0.03 1.90 9.78 88.87 13.1 MW2 06/26/13 <0.50 <0.50 0.017 0.0147 0.003 <0.002 <0.006 <0.002 0.0147 0.03 8.85 89.80 13.1 MW2 03/31/14 1.6 2.4 0.22 0.13 <0.005 0.0045 0.0078 <0.005 0.13 4.36 9.62 89.03 0.35 -141 2.8 7.1 11.7 MW2 11/07/14 2.1 0.84 0.24 0.056 <0.025 <0.005 <0.015 <0.025 0.056 3.24 9.88 88.77 0.87 -155 1.96 7.23 18.3 MW2 11/11/16 0.743 0.553 0.0691 0.0035 <0.005 <0.001 <0.003 <0.005 0.0035 1.37 9.71 88.94 0.5 -135 3.45 6.51 19 MW2 11/15/2017 0.466 <0.100 0.00895 <0.001 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.47 9.62 89.03 4.01 -114 0.36 7.32 15.4 MW2 06/14/2018 0.182 0.141 <0.00100 <0.001 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.32 8.13 90.52 0.62 -58 0.38 7.41 17.2 MW2 12/19/2018 0.301 0.497 0.0252 <0.001 <0.001 <0.001 <0.003 <0.005 0.001 0.82 9.59 89.06 0.73 14 0.88 7.33 12.9 MW2 07/20/19 0.5 <0.100 <0.001 <0.001 <0.001 <0.001 <0.003 <0.005 0.001 0.50 8.87 89.78 MW2 04/09/21 0.22 1.11 0.0556 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 1.39 9.55 89.10 2.13 102 2.46 7.54 15.1 MW2 12/08/21 0.301 0.845 0.0753 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 1.22 9.87 88.78 2.02 98 2.54 7.35 14.9 MW2 07/12/22 0.253 0.451 0.0904 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.79 7.33 91.32 3.81 1.47 7.89 20.5 MW2 11/17/22 0.162 0.486 0.0248 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.67 9.60 89.05 0.39 -55 0.86 7.11 16.5 MW2 08/27/24 Not accessible day of sampling, car parked on well all day 9.17 89.48 MW3 10/05/10 2.8 1 4.4 <0.001 <0.050 <0.010 0.03 0.05 0.001 8.28 8.22 90.08 MW3 11/02/10 1.3 1.9 3.8 0.0012 <0.005 <0.001 <0.003 <0.005 0.0012 7.00 8.40 89.90 MW3 05/18/11 4.1 1.7 1.1 0.48 0.29 <0.10 <0.30 <0.050 0.48 7.67 7.58 90.72 MW3 10/31/11 6.8 0.53 2 0.52 1.4 0.033 0.25 <25 0.52 11.53 7.89 90.41 0.15 -207 5.32 19.6 MW3 04/05/12 19 0.5 0.06 0.4 2.4 0.34 2.7 0.03 0.4 25.43 4.93 93.37 0.24 NA 0.79 7.16 13.5 MW3 11/08/12 4 1.8 1.2 0.25 <0.025 0.05 0.59 <0.025 0.25 7.89 8.43 89.87 MW3 06/26/13 0.94 1.96 0.605 0.169 <0.004 <0.004 0.331 <0.004 0.169 4.01 8.34 89.96 MW3 03/31/14 2.3 2.7 0.48 0.13 <0.005 0.063 0.14 <0.005 0.13 5.81 8.25 90.05 0.21 -101 14.7 6.6 12.3 MW3 11/07/14 2.1 1.3 1.3 0.12 <0.025 0.026 0.24 <0.025 0.12 5.09 8.78 89.52 1.07 -143 9.53 6.95 20.4 MW3 11/11/16 1.25 0.61 1.28 0.0337 <0.005 <0.001 <0.00831 <0.005 0.0337 3.17 8.69 89.61 1 -134 10.35 6.31 20.1 MW3 11/16/2017 2.13 1.4 1.05 0.0772 0.00137 <0.00100 0.00856 <0.00500 0.0772 4.67 8.69 89.61 3.99 -137 2.37 7.14 17.6 MW3 06/14/2018 2.29 1.66 0.936 0.0647 <0.0100 <0.0100 <0.0300 <0.0500 0.0647 4.95 8.16 90.14 0.9 -56 3.5 7.11 18.3 MW3 12/20/2018 0.956 16.3 0.586 0.0115 <0.0100 <0.0100 <0.0300 <0.0500 0.0115 17.85 8.64 89.66 5.02 82.7 2.72 7.36 13.3 MW3 07/20/19 2.132 9.52 0.51 0.0203 <0.0100 <0.0100 0.00318 <0.0500 0.0203 12.19 8.37 89.93 MW3 04/09/21 0.649 1.27 0.754 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 2.67 8.48 89.82 1.21 61 2.81 7.23 14.2 MW3D 04/09/21 0.688 1.21 0.648 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 2.55 8.48 89.82 1.21 61 2.81 7.23 14.2 MW3 12/08/21 1.01 1.09 0.726 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 2.83 8.79 89.51 1.33 58 2.71 7.39 13.8 MW3 07/12/22 1.54 0.424 0.715 0.00661 <0.00100 <0.00100 <0.00300 <0.00500 0.00661 2.69 8.18 90.12 0.69 3.92 7.9 21.1 MW3 11/17/22 1.00 0.978 0.394 <0.025 <0.025 <0.025 <0.075 <0.125 0.001 2.37 8.61 89.69 0.87 -92 2.72 6.83 16.8 MW3 08/27/24 1.42 0.848 0.694 <0.0200 <0.0200 <0.0200 <0.0600 <0.100 0.02 2.96 8.65 89.65 3.57 1.7 6.85 26.05 CommonCents Harrisville Page 1 of 4 10/22/2024 TABLE 2 CUMMULATIVE GROUNDWATER ANALYTICAL RESULTS and FIELD PARAMETERS CommonCents, 907 North 400 East, Harrisville, Utah Facility 1200401, Release MSB Well TPH GRO*TPH DRO*Ethyl Total Benzene Total Mass Depth to Groundwater ID Date (C6-C10)(C10-C28)*MtBE Benzene Toluene Benzene Xylenes Naphthalene Mass Water Elevation DO ORP Conductivity pH Temperature (mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/l)(feet)(ft above datum)(mg/L)(mv)(ms/m)© or (F) MW4 10/08/10 <0.10 2.6 0.082 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 2.68 8.76 89.80 MW4 11/02/10 <0.10 4.2 0.01 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 4.21 5.58 92.98 MW4 05/18/11 <0.10 2 0.0064 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 2.01 4.39 94.17 MW4 10/31/11 <0.10 0.78 0.01 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.79 5.73 92.83 0.4 -177 1.69 13.6 MW4 04/05/12 <0.10 0.4 0.033 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.43 5.52 93.04 0.36 NA 2.07 7.18 9.7 MW4 11/08/12 <0.10 1.1 0.027 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 1.13 5.89 92.67 MW4 06/26/13 <0.5 <0.5 0.032 <0.002 <0.002 <0.002 <0.006 <0.002 0.002 0.03 6.15 92.41 MW4 03/31/14 <0.1 1.5 0.031 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 1.53 6.64 91.92 0.25 -113 7.65 7.1 9.3 MW4 11/07/14 <0.1 0.78 0.038 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.82 7.50 91.06 MW4 11/11/16 <0.1 0.967 0.0276 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.99 7.44 91.12 MW4 11/16/2017 <0.100 1.01 0.0159 <0.001 <0.00100 <0.00100 <0.00300 <0.00500 0.001 1.03 7.10 91.46 MW4 06/14/2018 <0.100 0.868 0.0151 <0.001 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.88 6.08 92.48 4.87 -9 0.99 7.22 20.7 MW4 12/20/2018 <0.100 0.84 0.0122 <0.001 <0.001 <0.001 <0.003 <0.005 0.001 0.85 7.86 90.70 MW4 07/20/19 <0.100 0.402 0.01121 <0.001 <0.001 <0.001 <0.003 <0.005 0.001 0.41 6.18 92.38 MW4 04/09/21 <0.100 0.541 0.00721 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 0.55 6.70 91.86 6.9 127 2.17 7.67 11.9 MW4 12/08/21 <0.100 0.531 0.0102 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.54 7.87 90.69 5.2 136 2.48 7.27 12.6 MW4 07/12/22 <0.100 0.311 0.00455 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.32 5.87 92.69 2.98 1.59 8.02 17.6 MW4 11/17/22 <0.100 0.335 0.00618 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.34 7.47 91.09 0.28 -41 1.53 7.2 14.2 MW4 08/27/24 Not on sampling list DERR 10/30/2023 6.74 91.82 MW5 11/02/10 0.24 1 1.2 0.0022 <0.005 <0.001 <0.003 <0.005 0.0022 2.44 8.59 89.22 MW5 05/18/11 2.8 3.9 0.97 0.42 2.5 0.12 1.1 <0.10 0.42 11.81 7.62 90.19 MW5 10/31/11 7.7 0.53 0.71 0.62 0.6 0.13 1.2 0.007 0.62 11.50 7.73 90.08 0.53 -173 1.25 18.5 MW5 04/05/12 3.5 0.58 0.68 0.52 0.17 0.006 0.044 <0.005 0.52 5.50 4.68 93.13 0.26 NA 1.72 7.16 13.1 MW5 11/08/12 3.2 0.56 1.2 0.21 <0.025 0.044 0.25 <0.025 0.21 5.46 9.29 88.52 MW5 06/26/13 0.63 1.5 0.419 0.315 0.007 <0.004 0.08 <0.004 0.315 2.95 8.20 89.61 MW5 03/31/14 1.9 6 0.34 0.16 <0.005 0.001 0.035 <0.005 0.16 8.44 NA MW5 11/07/14 2.5 0.73 0.45 <0.025 <0.005 0.074 <0.025 0.45 3.75 9.43 88.38 MW5 11/11/16 2.42 0.647 0.714 0.129 <0.050 <0.010 <0.030 <0.050 0.129 3.91 9.29 88.52 MW5 11/16/2017 1.42 0.687 0.772 0.146 0.00306 <0.00100 0.0133 <0.00500 0.146 3.04 9.17 88.64 MW5 06/14/2018 1.62 2.17 0.29 0.17 <0.00500 <0.00500 <0.0150 <0.0250 0.17 4.25 8.13 89.68 0.58 -20 2.06 7.4 18.9 MW5 12/20/2018 0.929 1.06 0.585 0.0398 <0.005 <0.005 <0.0150 <0.0250 0.0398 2.61 9.28 88.53 MW5 07/20/19 1.18 1.86 0.0856 0.0399 0.00108 <0.00100 0.00306 <0.00500 0.0399 3.17 8.26 89.55 MW5 04/09/21 0.737 6.96 0.0676 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 7.76 8.86 88.95 1.65 52 4.69 7.09 14.1 MW5 12/10/21 2.06 0.738 0.762 0.0422 0.00113 <0.00100 <0.00300 <0.00500 0.0422 3.60 9.50 88.31 1.54 41 3.97 7.12 13.7 MW5 07/12/22 1.78 0.282 0.223 0.0624 <0.005 <0.005 <0.00300 <0.025 0.0624 2.35 7.90 89.91 1.58 2.07 8.18 22.2 MW5 11/18/22 3.03 0.653 0.686 0.0519 <0.005 <0.005 <0.0150 <0.025 0.0519 4.42 9.32 88.49 1.74 -54 2.22 7.44 10.6 MW5 08/27/24 1.67 1.33 0.59 0.0403 <0.0100 <0.0100 <0.0300 <0.0500 0.0403 3.63 6.08 91.73 1.08 2.5 7.34 19.5 MW6 11/02/10 <0.1 0.48 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.48 6.65 92.17 4 -1 1.3 7.72 17.9 MW6 05/18/11 <0.1 0.34 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.34 5.76 93.06 MW6 10/31/11 <0.100 <0.100 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 7.56 91.26 0.35 -210 1.46 20.4 MW6 04/05/12 <0.100 <0.100 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 6.82 92.00 0.36 NA 1.75 7.14 12.6 MW6 11/08/12 <0.100 <0.400 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 7.84 90.98 MW6 06/26/13 <0.5 <0.5 <0.002 <0.002 <0.002 <0.002 <0.006 <0.002 0.002 0.00 6.99 91.83 MW6 03/31/14 <0.1 0.34 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.34 7.29 91.53 0.36 -137 3.27 7.1 13.1 MW6 11/07/14 <0.1 0.29 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.29 8.29 90.53 2.01 -118 2.36 7.29 20.5 MW6 11/11/16 <0.1 0.358 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.36 8.03 90.79 1.37 -138 3.62 6.42 20 MW6 11/15/2017 <0.100 0.264 <0.00100 <0.001 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.26 7.98 90.84 4.49 -72.5 0.97 6.7 19.4 MW6 06/14/2018 <0.100 0.35 <0.00100 <0.001 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.35 6.88 91.94 0.52 -72 1.3 7.5 16.2 MW6 12/20/2018 <0.100 0.433 <0.001 0.00135 <0.001 <0.001 <0.003 <0.005 0.00135 0.43 8.08 90.74 3.46 89.7 7.21 7.55 15.2 MW6 07/20/19 <0.100 0.275 <0.001 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 0.28 7.04 91.78 MW6 04/09/21 <0.100 0.29 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 0.29 6.92 91.90 3.27 120 1.51 7.62 14.8 MW6 12/08/21 <0.100 0.376 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.38 8.20 90.62 3.01 118 1.98 7.49 13.9 MW6 07/12/22 <0.100 0.231 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.23 6.83 91.99 2.43 0.841 7.66 22.2 MW6 11/18/22 <0.100 0.255 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.26 7.84 90.98 1.63 51 1.16 7.44 13.9 MW6 08/27/24 Not on sampling list DERR 10/30/2023 6.71 92.11 CommonCents Harrisville Page 2 of 4 10/22/2024 TABLE 2 CUMMULATIVE GROUNDWATER ANALYTICAL RESULTS and FIELD PARAMETERS CommonCents, 907 North 400 East, Harrisville, Utah Facility 1200401, Release MSB Well TPH GRO*TPH DRO*Ethyl Total Benzene Total Mass Depth to Groundwater ID Date (C6-C10)(C10-C28)*MtBE Benzene Toluene Benzene Xylenes Naphthalene Mass Water Elevation DO ORP Conductivity pH Temperature (mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/l)(feet)(ft above datum)(mg/L)(mv)(ms/m)© or (F) MW7 11/02/10 <0.1 0.45 <0.001 0.0011 <0.005 <0.001 <0.003 <0.005 0.0011 0.45 5.80 94.00 MW7 05/18/11 <0.1 <0.10 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 5.35 94.45 MW7 10/31/11 <0.100 <0.100 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 6.71 93.09 0.52 -136 1.34 17.7 MW7 04/05/12 <0.100 <0.100 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 5.21 94.59 2.4 NA 1.52 7.15 12 MW7 11/08/12 <0.100 <0.100 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 6.78 93.02 MW7 06/26/13 <0.5 <0.5 <0.002 <0.002 <0.002 <0.002 <0.006 <0.002 0.002 0.00 5.97 93.83 MW7 03/31/14 <0.1 <0.1 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 5.48 94.32 3.62 -15 3.41 7.1 11.5 MW7 11/07/14 <0.1 <0.1 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 7.53 92.27 MW7 11/11/16 <0.1 0.166 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.17 6.89 92.91 3.27 -20 3.55 6.53 19 MW7 11/16/2017 <0.100 0.12 <0.00100 <0.001 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.12 7.58 92.22 3.34 -61 1.09 7.88 15.8 MW7 06/14/2018 <0.100 <0.100 <0.00100 <0.001 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.00 4.92 94.88 MW7 12/20/2018 <0.100 0.103 <0.001 <0.001 <0.001 <0.001 <0.003 <0.005 0.001 0.10 7.14 92.66 5.83 96.3 1.02 7.86 12.3 MW7 07/20/19 <0.100 <0.100 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 0.00 6.03 93.77 MW7 04/09/21 <0.100 0.105 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 0.11 5.92 93.88 5.86 128 1.66 7.68 11.7 MW7 12/08/21 <0.100 0.119 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.12 7.60 92.20 4.27 136 1.87 7.61 10.8 MW7 07/12/22 <0.100 <0.100 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.00 7.27 92.53 4.14 2.1 7.39 21.1 MW7 11/18/22 <0.100 0.126 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.13 7.47 92.33 4.26 -60 1.45 7.37 11.4 MW7 08/27/24 Not on sampling list DERR 10/30/2023 6.06 93.74 MW8 11/02/10 <0.10 0.12 0.011 <0.005 <0.005 <0.001 <0.003 <0.005 0.005 0.13 6.70 91.81 MW8 05/18/11 <0.10 <0.10 0.0014 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 5.93 92.58 MW8 10/31/11 <0.100 <0.100 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 7.27 91.24 2.31 175 1.47 14.6 MW8 04/05/12 <0.100 <0.100 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 5.58 92.93 0.7 NA 1.8 7.23 11.2 MW8 11/08/12 <0.100 <0.100 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 7.33 91.18 0.7 MW8 06/26/13 <0.5 <0.5 <0.002 <0.002 <0.002 <0.002 <0.006 <0.002 0.002 0.00 7.20 91.31 0.7 MW8 03/31/14 <0.1 <0.1 0.0011 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 6.75 91.76 NA -138 2.46 7.8 11.8 MW8 11/07/14 <0.1 <0.1 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 6.75 91.76 MW8 11/11/16 <0.1 0.35 0.0565 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.41 7.59 90.92 MW8 11/16/2017 <0.100 <0.100 <0.00100 <0.001 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.00 7.94 90.57 12.4 49 1.26 8.32 14.7 MW8 06/14/2018 <0.100 <0.100 <0.00100 <0.001 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.00 7.21 91.30 8.8 4 1.8 7.74 13.6 MW8 12/20/2018 <0.100 <0.100 <0.001 <0.001 <0.001 <0.001 <0.003 <0.005 0.001 0.00 7.87 90.64 3.75 116 1.33 8.18 13.5 MW8 07/20/19 <0.100 <0.100 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 0.00 7.25 91.26 MW8 04/09/21 <0.100 <0.100 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 0.00 6.64 91.87 2.7 114 1.44 7.93 11.2 MW8 12/08/21 <0.100 0.138 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.14 8.21 90.30 2.9 154 1.84 7.74 10.5 MW8 11/18/22 <0.100 0.138 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.14 7.97 90.54 2.27 34 1.32 7.57 11.1 MW8 08/27/24 Not on sampling list DERR 10/30/2023 98.51 MW9 11/17/11 <0.5 <0.5 0.599 <0.002 <0.004 <0.002 <0.006 <0.002 0.002 0.60 8.07 90.66 MW9 05/18/11 0.44 0.13 0.77 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 1.34 7.12 91.61 MW9 10/31/11 0.42 <0.100 0.83 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 1.25 9.41 89.32 0.5 -152 2.08 16.3 MW9 04/05/12 0.35 0.19 0.46 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 1.00 6.47 92.26 0.41 NA 2.54 7.12 11.6 MW9 11/08/12 0.35 0.14 0.68 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 1.17 8.85 89.88 MW9 06/26/13 <0.5 <0.5 0.403 <0.001 <0.002 <0.002 <0.006 <0.002 0.001 0.40 9.18 89.55 MW9 03/31/14 <0.1 0.3 0.29 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.59 8.14 90.59 0.35 -114 4.1 6.9 12 MW9 11/07/14 0.15 0.13 0.3 <0.005 <0.025 <0.005 <0.015 <0.025 0.005 0.58 10.37 88.36 MW9 11/11/16 <0.100 0.194 0.0877 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.28 9.10 89.63 2.77 -90 11.32 6.76 17 MW9 11/16/2017 <0.100 0.165 0.0418 <0.001 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.21 9.27 89.46 7.42 -86 2.45 7.47 14.4 MW9 06/14/2018 0.107 0.221 0.134 <0.001 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.46 10.00 88.73 2.11 4.8 3.7 7.2 14.4 MW9 12/20/2018 <0.100 0.1 0.0383 <0.001 <0.001 <0.001 <0.003 <0.005 0.001 0.17 9.35 89.38 5.23 123.9 3.21 7.49 14.1 MW9 07/20/19 0.2 0.1 0.1260 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 0.43 9.22 89.51 MW9 04/09/21 0.101 <0.200 0.0914 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 0.19 7.77 90.96 2.18 141 2.26 7.25 13.6 MW9 12/08/21 <0.100 0.132 0.0195 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.15 9.97 88.76 1.68 154 2.36 7.29 12.7 MW9 07/12/22 0.13 0.136 0.0793 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.35 8.44 90.29 1.06 3.67 6.87 25 MW9 11/17/22 0.2 0.115 0.1 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.42 9.12 89.61 1 -31 1.74 6.96 16.5 MW9 08/27/24 <0.100 0.125 0.0474 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.17 8.24 90.49 0.44 2.95 7.33 17.9 CommonCents Harrisville Page 3 of 4 10/22/2024 TABLE 2 CUMMULATIVE GROUNDWATER ANALYTICAL RESULTS and FIELD PARAMETERS CommonCents, 907 North 400 East, Harrisville, Utah Facility 1200401, Release MSB Well TPH GRO*TPH DRO*Ethyl Total Benzene Total Mass Depth to Groundwater ID Date (C6-C10)(C10-C28)*MtBE Benzene Toluene Benzene Xylenes Naphthalene Mass Water Elevation DO ORP Conductivity pH Temperature (mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/l)(feet)(ft above datum)(mg/L)(mv)(ms/m)© or (F) MW10 05/20/11 0.14 0.25 0.075 <0.001 <0.005 0.0036 0.032 <0.005 0.001 0.50 9.81 88.41 MW10 10/31/11 <0.100 <0.100 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 8.28 89.94 0.74 -95 2.93 14.6 MW10 04/05/12 <0.100 <0.100 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 6.27 91.95 1.22 NA 3.61 7.19 10.1 MW10 11/08/12 <0.100 <0.100 0.081 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.08 8.19 90.03 MW10 06/26/13 <0.5 <0.5 0.072 <0.001 <0.002 <0.002 <0.006 <0.002 0.001 0.07 8.54 89.68 MW10 03/31/14 <0.1 <0.1 0.067 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.07 7.62 90.60 0.84 -123 3.2 7.4 10.8 MW10 11/07/14 <0.1 0.19 0.066 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.26 9.24 88.98 1.22 -140 2.67 7.39 13.9 MW10 11/11/16 <0.1 <0.30 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 8.34 89.88 5.47 -129 10.07 6.41 14.1 MW10 11/15/2017 <0.100 0.123 0.0412 <0.001 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.16 8.59 89.63 MW10 06/14/2018 <0.100 <0.100 0.0397 <0.001 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.04 8.71 89.51 MW10 12/20/2018 <0.100 <0.100 0.0406 <0.001 <0.001 <0.001 <0.003 <0.005 0.001 0.04 8.71 89.51 4.06 102.5 2.04 8.09 12.9 MW10 07/20/19 <0.100 <0.100 0.0233 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 0.02 8.59 89.63 MW10 04/09/21 <0.100 <0.100 0.0247 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 0.02 7.54 90.68 2.98 78 1.44 7.72 9 MW10 12/08/21 <0.100 0.139 0.0193 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.16 8.98 89.24 2.51 83 1.32 7.54 9.2 MW10 07/12/22 <0.100 0.139 0.0248 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.16 8.05 90.17 1.74 3.35 7.18 25.5 MW10 11/18/22 <0.100 <0.100 0.028 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.03 8.65 89.57 2.48 -72 1.83 7.61 8.6 MW10 08/27/24 Not on sampling list DERR 10/30/2023 7.21 91.01 MW11 05/20/11 <0.10 0.81 <0.001 <0.001 <0.0050 <0.001 0.0056 <0.005 0.001 0.82 13.46 79.57 MW11 10/31/11 <0.100 <0.100 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 6.15 86.88 0.3 -230 1.95 15.4 MW11 04/05/12 <0.100 <0.100 0.0065 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.01 4.95 88.08 0.39 NA 1.76 7.2 10 MW11 11/08/12 <0.100 0.14 0.0045 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.14 6.20 86.83 MW11 06/26/13 <0.5 <0.5 <0.002 <0.002 <0.002 <0.002 <0.006 <0.002 0.002 0.00 6.51 86.52 MW11 03/31/14 <0.1 <0.1 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.00 5.43 87.60 0.36 -181 2.4 7.9 10.5 MW11 11/07/14 <0.1 0.2 <0.001 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.20 7.08 85.95 MW11 12/20/2018 <0.100 0.29 <0.001 <0.001 <0.001 <0.001 <0.003 <0.005 0.001 0.29 6.49 86.54 MW11 07/20/19 <0.100 <0.100 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 0.00 6.55 86.48 MW11 04/09/21 <0.100 0.26 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 0.26 5.81 87.22 2.52 71.8 1.37 7.63 10.3 MW11 12/08/21 <0.100 0.181 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.18 6.26 86.77 2.41 79 1.27 7.21 9.8 MW11 07/12/22 <0.100 <0.100 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.00 5.58 87.45 0.6 3.51 8.27 21.6 MW11 11/17/22 <0.100 0.125 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.13 7.93 85.10 2 -152 1.57 7.62 15 MW11 08/27/24 <0.100 <0.100 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.00 6.24 86.79 0.81 3.03 7.2 20 MW14 11/11/16 <0.1 0.311 0.0206 <0.001 <0.005 <0.001 <0.003 <0.005 0.001 0.33 10.08 88.95 2.46 -132 1.1 8.09 12.4 MW14 11/16/2017 <0.100 0.199 0.0128 <0.001 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.21 10.11 88.92 7.6 -66 0.72 7.91 13.1 MW14 06/14/2018 <0.100 <0.100 0.00157 <0.001 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.00 8.38 90.65 1.8 -2.5 0.4 7.81 13.3 MW14 12/20/2018 <0.100 0.184 0.0094 <0.001 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.19 9.99 89.04 6.64 106.4 0.78 8.25 12.3 MW14 07/20/19 <0.100 <0.100 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 0.00 9.99 89.04 MW14 04/09/21 <0.100 0.148 0.00643 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 <0.00100 0.15 9.80 89.23 2.29 127 1.41 7.82 10.4 MW14 12/08/21 <0.100 0.117 0.00293 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.12 9.57 89.46 2.29 127 1.41 7.82 10.4 MW14 07/12/22 <0.100 <0.100 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.00 8.28 90.75 2.75 0.323 7.52 18.8 MW14 11/18/22 <0.100 0.105 0.00324 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.11 9.56 89.47 2.16 78 0.831 7.72 9.6 MW14 08/27/24 Not on sampling list DERR 10/30/2023 9.08 89.95 MW15 08/27/24 0.18 1.08 0.139 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 1.40 11.77 87.28 2.09 5.01 7.85 16.6 MW16 08/27/24 <0.100 0.529 0.033 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.56 8.77 88.59 0.45 1.48 7.45 21.1 MW17 08/27/24 <0.100 2.83 0.0322 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 2.86 8.57 89.10 0.38 2.23 7.27 21.4 RBCA Tier 1 Values mg/L 10 10 0.2 0.3 3 4 10 0.7 Utah ISL Values mg/L 1 1 0.2 0.005 1 0.7 10 0.7 GRO Gasoline Range Organics C6-C10 mg/L Milligrams per liter DRO Diesel Range Organics C10-C28 ms/m Micro semens per meter <0.001 Concentration was less than the detection limit shown DO Dissolved Oxygen mv Millivolts Blank Not sampled not measured GRO Mass DERR Wells 8-24 3.3 mg/l Benzene Mass DERR Wells 8-24 0.044 mg/l CommonCents Harrisville Page 4 of 4 10/22/2024 TABLE 3 DERR REQUIRED WELL SAMPLING GROUNDWATER ANALYTICAL RESULTS and FIELD PARAMETERS CommonCents, 907 North 400 East, Harrisville, Utah Facility 1200401, Release MSB Well TPH GRO*TPH DRO*Ethyl Total Benzene Total Depth to Groundwater ID Date (C6-C10)(C10-C28)*MtBE Benzene Toluene Benzene Xylenes Naphthalene Mass Mass Water Elevation DO ORP Conductivity pH Temperature (mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(feet)(ft above datum)(mg/L)(mv)(ms/m)(Fahrenheit) Monitor Wells HNW 08/27/24 <0.100 <0.100 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.53 6.20 0.23 1980 7.54 76.9 HNE 08/27/24 <0.100 <0.100 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0 0.00 6.20 0.08 1969 7.53 77.5 HSW 08/27/24 <0.100 <0.100 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.80 6.31 0.17 2029 7.49 79.2 HSE 08/27/24 <0.100 <0.100 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 1.00 6.29 0.11 1770 7.44 75.2 MW2 08/27/24 Not accessible day of sampling, car parked on well all day 9.17 89.48 MW3 08/27/24 1.42 0.848 0.694 <0.0200 <0.0200 <0.0200 <0.0600 <0.100 0.02 2.96 8.65 89.65 3.57 1.7 6.85 26.05 MW5 08/27/24 1.67 1.33 0.59 0.0403 <0.0100 <0.0100 <0.0300 <0.0500 0.0403 3.63 6.08 91.73 1.08 2.5 7.34 19.5 MW9 08/27/24 <0.100 0.125 0.0474 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.17 8.24 90.49 0.44 2.95 7.33 17.9 MW11 08/27/24 <0.100 <0.100 <0.00100 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.00 6.24 86.79 0.81 3.03 7.2 20 MW15 08/27/24 0.18 1.08 0.139 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 1.40 11.77 87.28 2.09 5.01 7.85 16.6 MW16 08/27/24 <0.100 0.529 0.033 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 0.56 8.77 88.59 0.45 1.48 7.45 21.1 MW17 08/27/24 <0.100 2.83 0.0322 <0.00100 <0.00100 <0.00100 <0.00300 <0.00500 0.001 2.86 8.57 89.10 0.38 2.23 7.27 21.4 RBCA Tier 1 Values mg/L 10 10 0.2 0.3 3 4 10 0.7 Utah ISL Values mg/L 1 1 0.2 0.005 1 0.7 10 0.7 GRO Gasoline Range Organics C6-C10 mg/L Milligrams per liter DRO Diesel Range Organics C10-C28 ms/m Micro semens per meter <0.001 Concentration was less than the detection limit shown DO Dissolved Oxygen mv Millivolts Blank Not sampled or not measured HNW HNE HSW HSE Tank Basin monitoring wells CommonCents Harrisville Page 1 of 1 10/22/2024 TABLE 4 BENZENE and MTBE GROUNDWATER CONCENTRATIONS vs TIME CommonCents, 907 North 400 East, Harrisville, Utah Facility 1200401, Release MSB -0.1 0 0.1 0.2 0.3 0.4 0.5 0.6 10 / 0 5 / 1 0 11 / 0 2 / 1 0 05 / 1 8 / 1 1 10 / 3 1 / 1 1 04 / 0 5 / 1 2 11 / 0 8 / 1 2 06 / 2 6 / 1 3 03 / 3 1 / 1 4 11 / 0 7 / 1 4 11 / 1 1 / 1 6 11 / 1 6 / 2 0 1 7 06 / 1 4 / 2 0 1 8 12 / 2 0 / 2 0 1 8 07 / 2 0 / 1 9 04 / 0 9 / 2 1 04 / 0 9 / 2 1 12 / 0 8 / 2 1 07 / 1 2 / 2 2 11 / 1 7 / 2 2 08 / 2 7 / 2 4 To t a l G R O D R O M B T E X N m g / l MW3 Groundwater Benzene Mass vs Time Benzene Linear (Benzene) 0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 5 10 / 0 5 / 1 0 11 / 0 2 / 1 0 05 / 1 8 / 1 1 10 / 3 1 / 1 1 04 / 0 5 / 1 2 11 / 0 8 / 1 2 06 / 2 6 / 1 3 03 / 3 1 / 1 4 11 / 0 7 / 1 4 11 / 1 1 / 1 6 11 / 1 6 / 2 0 1 7 06 / 1 4 / 2 0 1 8 12 / 2 0 / 2 0 1 8 07 / 2 0 / 1 9 04 / 0 9 / 2 1 04 / 0 9 / 2 1 12 / 0 8 / 2 1 07 / 1 2 / 2 2 11 / 1 7 / 2 2 08 / 2 7 / 2 4 To t a l G R O D R O M B T E X N m g / l MW3 Groundwater MTBE Mass vs Time MtBE Linear (MtBE) -0.1 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 11 / 0 2 / 1 0 05 / 1 8 / 1 1 10 / 3 1 / 1 1 04 / 0 5 / 1 2 11 / 0 8 / 1 2 06 / 2 6 / 1 3 03 / 3 1 / 1 4 11 / 0 7 / 1 4 11 / 1 1 / 1 6 11 / 1 6 / 2 0 1 7 06 / 1 4 / 2 0 1 8 12 / 2 0 / 2 0 1 8 07 / 2 0 / 1 9 04 / 0 9 / 2 1 12 / 1 0 / 2 1 07 / 1 2 / 2 2 11 / 1 8 / 2 2 08 / 2 7 / 2 4 To t a l G R O D R O M B T E X N m g / l MW5 Groundwater Benzene Mass vs Time Benzene Linear (Benzene) 0 0.2 0.4 0.6 0.8 1 1.2 1.4 11 / 0 2 / 1 0 05 / 1 8 / 1 1 10 / 3 1 / 1 1 04 / 0 5 / 1 2 11 / 0 8 / 1 2 06 / 2 6 / 1 3 03 / 3 1 / 1 4 11 / 0 7 / 1 4 11 / 1 1 / 1 6 11 / 1 6 / 2 0 1 7 06 / 1 4 / 2 0 1 8 12 / 2 0 / 2 0 1 8 07 / 2 0 / 1 9 04 / 0 9 / 2 1 12 / 1 0 / 2 1 07 / 1 2 / 2 2 11 / 1 8 / 2 2 08 / 2 7 / 2 4 To t a l G R O D R O M B T E X N m g / l MW5 Groundwater MTBE Mass vs Time MtBE Linear (MtBE) CommonCents Harrisville Page 1 of 1 10/22/2024 TABLE 5 GROUNDWATER ELEVATION VERSUS COC CONCENTRATIONS CommonCents, 907 North 400 East, Harrisville, Utah Facility 1200401, Release MSB 87.00 88.00 89.00 90.00 91.00 92.00 93.00 94.00 0 0.1 0.2 0.3 0.4 0.5 0.6 10 / 0 5 / 1 0 11 / 0 2 / 1 0 05 / 1 8 / 1 1 10 / 3 1 / 1 1 04 / 0 5 / 1 2 11 / 0 8 / 1 2 06 / 2 6 / 1 3 03 / 3 1 / 1 4 11 / 0 7 / 1 4 11 / 1 1 / 1 6 11 / 1 6 / 2 0 1 7 06 / 1 4 / 2 0 1 8 12 / 2 0 / 2 0 1 8 07 / 2 0 / 1 9 04 / 0 9 / 2 1 04 / 0 9 / 2 1 12 / 0 8 / 2 1 07 / 1 2 / 2 2 11 / 1 7 / 2 2 08 / 2 7 / 2 4 GW E l e v a t i o n Groundwater Elevation Versus Benzene Concentration MW3 Benzene Groundwater Elevation Linear (Benzene) 85.00 86.00 87.00 88.00 89.00 90.00 91.00 92.00 93.00 94.00 -0.1 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 11 / 0 2 / 1 0 05 / 1 8 / 1 1 10 / 3 1 / 1 1 04 / 0 5 / 1 2 11 / 0 8 / 1 2 06 / 2 6 / 1 3 03 / 3 1 / 1 4 11 / 0 7 / 1 4 11 / 1 1 / 1 6 11 / 1 6 / 2 0 1 7 06 / 1 4 / 2 0 1 8 12 / 2 0 / 2 0 1 8 07 / 2 0 / 1 9 04 / 0 9 / 2 1 12 / 1 0 / 2 1 07 / 1 2 / 2 2 11 / 1 8 / 2 2 08 / 2 7 / 2 4 GW E l e v a t i o n Be n z e n e m g / l Date Groundwater Elevation Versus Benzene Concentration MW5 Benzene Groundwater Elevation Linear (Benzene) 87.00 88.00 89.00 90.00 91.00 92.00 93.00 94.00 0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 5 10 / 0 5 / 1 0 11 / 0 2 / 1 0 05 / 1 8 / 1 1 10 / 3 1 / 1 1 04 / 0 5 / 1 2 11 / 0 8 / 1 2 06 / 2 6 / 1 3 03 / 3 1 / 1 4 11 / 0 7 / 1 4 11 / 1 1 / 1 6 11 / 1 6 / 2 0 1 7 06 / 1 4 / 2 0 1 8 12 / 2 0 / 2 0 1 8 07 / 2 0 / 1 9 04 / 0 9 / 2 1 04 / 0 9 / 2 1 12 / 0 8 / 2 1 07 / 1 2 / 2 2 11 / 1 7 / 2 2 08 / 2 7 / 2 4 GW E l e v a t i o n MT B E m g / l Date Groundwater Elevation Versus MTBE Concentration MW3 MtBE Groundwater Elevation 85.00 86.00 87.00 88.00 89.00 90.00 91.00 92.00 93.00 94.00 0 0.2 0.4 0.6 0.8 1 1.2 1.4 11 / 0 2 / 1 0 05 / 1 8 / 1 1 10 / 3 1 / 1 1 04 / 0 5 / 1 2 11 / 0 8 / 1 2 06 / 2 6 / 1 3 03 / 3 1 / 1 4 11 / 0 7 / 1 4 11 / 1 1 / 1 6 11 / 1 6 / 2 0 1 7 06 / 1 4 / 2 0 1 8 12 / 2 0 / 2 0 1 8 07 / 2 0 / 1 9 04 / 0 9 / 2 1 12 / 1 0 / 2 1 07 / 1 2 / 2 2 11 / 1 8 / 2 2 08 / 2 7 / 2 4 GW E l e v a t i o n Be n z e n e m g / l Date Groundwater Elevation Versus MTBE Concentration MW5 MtBE Groundwater Elevation Linear (MtBE) CommonCents Harrisville Page 1 of 1 10/22/2024 ATTACHMENT A 195 North 1950 West • Salt Lake City, UT Mailing Address: P.O. Box 144840 • Salt Lake City, UT 84114-4840 Telephone (801) 536-4100 • Fax (801) 359-8853 • T.D.D. (801) 536-4284 www.deq.utah.gov Printed on 100% recycled paper State of Utah SPENCER J. COX Governor DEIDRE HENDERSON Lieutenant Governor Department of Environmental Quality Kimberly D. Shelley Executive Director DIVISION OF ENVIRONMENTAL RESPONSE AND REMEDIATION Brent H. Everett Director ERRL-0394-23 October 30, 2023 CERTIFIED MAIL RETURN RECEIPT REQUESTED Jim Sachs Moyle Petroleum Company 2504 West Main Street Rapid City, South Dakota 57702 Re:Additional Sampling Requirements Following Site Closure Review Common Cents, located at 907 North 400 East, Harrisville, Utah Facility Identification No. 1200401, Release Site MSB Dear Mr. Sachs: The Division of Environmental Response and Remediation (DERR) completed a site closure review of the Common Cents, leaking underground storage tank (LUST) site, located at the above- referenced facility. The review included historic reports in the case file, including the Johnston Leigh, Inc. (JLI) Subsurface Investigation Report 2016 and 2022 Groundwater Monitoring Results, No Further Action Review report, submitted to the DERR in February 2016 and March 2023, respectively. The review indicates that historic soil sampling data is below the DERR’s Initial Screening Level (ISL) cleanup standard, while groundwater contamination remains at the site exceeding the ISL standard. Conclusions drawn from the DERR review are: 1. Dissolved-phase petroleum-impacted groundwater (Plume) above the ISL remains for total petroleum hydrocarbons, gasoline range organics (TPH-GRO), benzene and methyl-tertiary butyl-ether (MTBE) in and about monitoring wells (MWs) MW3 and MW5. The depth to groundwater is about 8-9’ below grade (see enclosed Figure 1, Site Map with Groundwater Monitoring Well Locations, DERR, 2023). 2. The Plume has an undefined southwestern boundary, and a western boundary that is defined between MW-5 and MW-11, with more than 160’ between them. The undefined Plume area appears to be on third party land. According to the Weber County Recorder’s Office, Common Cents is on Parcel 110270126 and owned by Common Cents Harrisville, LLC, while Parcel 110270123, bounding Common Facility ID# 1200401 Page 2 Cents on the south and west, is owned by Flying J Inc. (see enclosed Figure 2, Weber County Parcel Map). Therefore, more work is needed before site closure can be considered: 1. Determine the limits of the Plume. Install additional MWs as needed and obtain soil samples from the MW borings. Samples collected shall be analyzed for total petroleum hydrocarbons, diesel range organics (TPH-DRO), TPH-GRO, benzene, toluene, ethyl-benzene, xylene, naphthalene (BTEXN) and MTBE. 2. Obtain one round of samples from underground storage tank observation wells HNW, HSW, HNE and HSE. Collected groundwater samples shall be analyzed for TPH-DRO, TPH-GRO, BTEXN and MTBE. 3. Continue groundwater monitoring from MW2, MW3, MW5, MW9, MW11 and newly placed MWs for four quarters. Samples collected shall be analyzed for TPH- DRO, TPH-GRO, BTEXN and MTBE. 4. Provide a report of the findings from Items 1 and 2 above as well as the results from the first round of quarterly groundwater monitoring as identified in Item 3 above, in accordance with Utah Admin. Code R311-211 and R311-202. Individual reports shall also be submitted following the subsequent quarterly monitoring events referenced in Item 3. According to Utah Code R311-202 and R311-211, the DERR requires that Moyle Petroleum Company provide a report of findings for Item 4 above, within 120 days of receipt of this letter. Subsequent quarterly groundwater monitoring will follow, with reports due 30 days following the respective field events. If you have any questions, please contact Mark Crim, the DERR project manager, at (801) 536-4100. Sincerely, Brent H. Everett, Director Division of Environmental Response and Remediation BHE/MEC/rr Enclosure(s): Figure 1, Site Map with Groundwater Monitoring Well Locations, DERR, 2023 Figure 2, Weber County Parcel Map cc: Brian Cowan, B.S., M.P.H., Director, Weber-Morgan Health Department Leigh Beem, Johnston Leigh, Inc. Figure 1: Site Map with Groundwater Monitoring Well Locations (from Johnston Leigh Inc., Figure 2, 2022) Jofinston L eigli foe. (801) 72 6-6845 "l r,IE1 uo ,,, C."500\•r-., 0 ;,,FOC FIGURE 2 SITE MAP MONITORING W ELLS/SO IL BORINGS/UTILITIES CommonCents go7 N400 E Harrisville Utah Figure 2: Weber County Parcel Map 11 PART OF N.E. 1/4 SECTI ON 8, T .6N.,R.1 W., S.L .B.&M. T AXINC UNIT! 20 I t-I H ARRI SVlll.£ CI TY SCAL.£ 1M = 100' SEE PAGE 27 -1 GR EE NLAN D SUB S EE PAGE 2 7 -1 CINNAMON PARK 10 5 0 NORTH ST. SU BD IVISIO N NO. 2 SEE PAG ES 140 , 14 1 ,---------<-SEE PAGE 2 CIN NAMON PARK 1000 NORTH SUBD IVISION NO. SEE PAGE 28 ST. P. :58 7 SEE PAGE 2 7 -2 •f'~ l ~X PURPOSE$ mil yt ; ci > _J (D I i i ~ I-'-' • z n :i: (/) ~ • : ~ .. w g ! ., . ,._ N 8 N g 27-5 SEE PAGE 27-1 \'LG 1-9!1 ATTACHMENT B 2024 JOHNSTON LEIGH INC LEIGH BEEM Johnston Leigh Inc. Standard Operating Procedure DERR 2024 Page 1 SOP 1 Sample Documentation ___________________________________________________ 2 SOP 2 Surface and Subsurface Soil Sampling _______________________________________ 3 SOP 3 PRE-PACK WELL INSTALLATION AND SAMPLING _______________________________ 5 SOP 4 Slug Test _______________________________________________________________ 9 SOP 5 Sub-Slab Air Sampling ___________________________________________________ 10 SOP 6 Decontamination _______________________________________________________ 11 SOP 7 FIELD SCREENING PHOTO IONIZATION DETECTOR (PID) ________________________ 12 SOP 8 EQUIPMENT CALIBRATION _______________________________________________ 13 SOP 9 SAMPLING MANAGEMENT CHAIN OF CUSTODY ______________________________ 14 SOP 10 INVESTIGATION DERIVED WASTE _________________________________________ 16 Johnston Leigh Inc. Standard Operating Procedure DERR 2024 Page 2 SOP 1 Sample Documentation 1.0 Sample Data Point The Sample Data Point (SDP) is the unique ID for a sample location. An individual SDP may include surface soil samples, soil boring samples and groundwater sample(s). Having one SDP allows management; retrieval and query of analytical results under one XYZ coordinate for multiple samples and media type collected at an individual SDP. Each SDP will be designated as “S” for “soil”; and a sequential number indicating the location where the sample(s) were collected. For instance, S1-1 is SDP number 1 at soil boring 1. The individual sample ID for surface soil, subsurface soil and groundwater samples are described below. 2.0 Surface Soil The surface soil sample designation will consist of a string of letters and numbers. The letters “SS” is the designation for “surface soil”. Following the “SS”, the soil boring number will be listed. For instance, SS1-1 would designate surface soil sample #1 collected at SDP #1 at soil boring 1. 3.0 Subsurface Soil Sample The subsurface soil sample designation will consist of a string of letters and numbers similar to the formatting for surface soil. The letters “SB” is the designation for soil boring. Following the “SB”, the soil boring number will be listed. Following the soil boring number will be the SDP number at that location. Lastly the final number in the sample ID will be the depth of the sample. For instance, SB1-1-5 would designate a soil sample collected from soil boring at SDP #1 at soil boring 1 and at a depth of 5 feet below ground surface (BGS). 4.0 Groundwater Sample A groundwater sample collected from the well will be designated using the following letters and numbers. The letters “GW” is the designation for groundwater. Following the “GW”, the well ID will be listed followed by the date. For instance, GW1-010121 would designate a groundwater sample collected from well 1 on 01/01/2021. 5.0 Slug Test A slug test performed at a well will be referenced in the database management system in the same manner as the soil and groundwater samples. This will allow the selection of the calculated K value derived from the slug test from the same XYZ data management system and contouring the results. The letter “K” is the designation for hydraulic conductivity value, followed by the well number and date. For instance, K1-010121 would designate a slug test K at well 1 on 01/01/2021. Johnston Leigh Inc. Standard Operating Procedure DERR 2024 Page 3 SOP 2 Surface and Subsurface Soil Sampling 1.0 Surface Soil Surface soil samples are designated as those samples collected no more than 0.5 feet in depth. A one-foot square area will be located on the ground surface and any debris or vegetation will be removed from within the area. The surface soil sample will be collected with a decontaminated stainless steel or aluminum trowel and placed directly in the sample containers. No mixing of the soil will occur. If more than one sample container is filled, then the soil aliquot will be evenly distributed to all the containers from the sample depth within the one foot area. A label with the subsurface soil sample ID will be attached to the glass jars and placed inside a labeled ziplock baggie. The sample will be retained inside a cooler containing ice enclosed in a plastic bag. After the surface soil sample is collected, the sampling trowel will be decontaminated using the three-bucket wash system consisting of washing the trowel in low phosphate soap with tap water, followed by a triple rinse in tap water and one final triple rinse in deionized water. The trowel will be allowed to air dry before proceeding to the next soil sample location. 2.0 Subsurface Soil The Geoprobe® Dual Tube 35 (DT35) soil sampling system will be used to collect soil samples. The DT35 system will collect continuous soil core samples from ground surface to total depth of each soil boring. A 3.5-inch outside diameter (OD) rod is driven into the ground as an outer casing. The outer rods receive the driving force of the hammer. The second smaller set of 3.25-inch OD rods is placed inside the outer casing through which the soil samples are recovered. A cutting show is treaded into the leading end of the outer rod string. When the outer rods are driven into the subsurface, the cutting shoes shears a 2.125-inch OD soil core inside a clear plastic liner that is attached to the smaller inner rods. Once filled, the liner with the soil sample is removed from the bottom of the outer casing by lifting the inner rods. Sampling soil from a cased hole is advantageous in that there is no side wall slough into the open boring. Additionally, perched groundwater is isolated from the soil core eliminating potential cross contamination of soil with perched water. Each boring will be advanced to first encountered groundwater. The final depth most likely will be 15-20 feet below ground surface. The sample depth may be determined by the results of the Laser Induced Fluorescence (LIF) and PID measurements. The SOP for LIF is included in SOP 2. The SOP for PID screening is included in SOP 6. The LIF results will be used to identify the greatest concentration of petroleum hydrocarbons in the soil borings. The highest RE% value for each boring will be collected for analytical testing. The LIF target sample depth will be removed from the 2.125-inch diameter clear plastic sleeve by cutting the sleeve along the axis and placing the sample depth into sample jars. The sample jar(s) will be labeled and placed inside a labeled ziplock baggie. The sample will be retained inside a cooler containing ice enclosed in a plastic bag. The soil exhibiting the highest PID value for each boring may be collected if the depth does not coincide with the highest %RE. The PID target sample depth will be removed from the 2.125- inch diameter clear plastic sleeve by cutting the sleeve along the axis and placing the sample depth into sample jars. The sample jar(s) will be labeled and placed inside a labeled ziplock Johnston Leigh Inc. Standard Operating Procedure DERR 2024 Page 4 baggie. The sample will be retained inside a cooler containing ice enclosed in a plastic bag. Decontamination of the DT35 outer and inner rods will be accomplished following decontamination procedures outline in SOP 6. Johnston Leigh Inc. Standard Operating Procedure DERR 2024 Page 5 SOP 3 PRE-PACK WELL INSTALLATION AND SAMPLING 1.0 Well Installation The DT35 dual casing system will also be used to install small diameter pre-pack well screen and blank riser for the purpose of collecting groundwater samples and measuring groundwater levels (calculating hydraulic gradient. An expendable cutting shoe will be used which allows setting prepacked well screen and blank riser through the DT35 outer casing. After the collection of the continuous soil core samples to the total depth, a 2-inch diameter prepack well screen five feet in length is lowered to the bottom of the outer casing. Blank casing is flush threaded to the pre-pack screen up to the ground surface. Pressure is exerted on the well riser while the outer casing is slowly raised. This dislodges the expendable cutting show and the well stays at the total depth while the outer casing is removed. The well head will be protected by either placing a 6-inch OD stove pipe casing over the well pipe and cementing it into a 12-inch OD hole excavated by hand using a shovel; or surface completion of well head inside a 8-inch diameter circular vault sealed with a concrete apron. 2.0 Groundwater Sampling This SOP provides a description of field procedures related to collection of groundwater samples. Sampling activities performed in the monitoring wells shall be conducted in an order of least-to-most contaminated to minimize the potential for cross-contamination. If free product is encountered in a monitoring well, a groundwater sample at that location will not be collected. Specific field information regarding general activities, water level measurement, and sampling activities will be recorded in the field on specific forms. Forms for recording field information include: • Form A Daily Field Log, • Form B Groundwater Gauging Log, and • Form C Groundwater Sampling Log. 3.0 Well Gauging Procedures for groundwater level measurements and LNAPL thickness measurements in monitoring wells are provided in this section. Based on the background information (if present) on the monitoring wells, it is known which wells have or have had measurable LNAPL in the past. These wells will only be gauged using an oil/water interface probe. The following procedure shall be used for a well with potential LNAPL: • Lower the probe of a decontaminated electronic sounding oil/water interface meter into the monitoring well until the meter indicates the probe has contacted the oil/groundwater surface. • Measure the depth to product and depth to water from the survey reference mark (on the polyvinyl chloride [PVC] well casing) to the nearest 0.01 foot. If no mark is present, measure the depth to product and depth to water to the north side of the casing. • Record the oil and water level measurements and total well depth on Form B. • Decontaminate the probe and tape in accordance with the decontamination procedures outlined in SOP 5. Johnston Leigh Inc. Standard Operating Procedure DERR 2024 Page 6 The following procedure shall be used for a well with no LNAPL: • Begin with the wells that historically have had the lowest concentration of dissolved BTEX (i.e, clean to dirty). Lower the decontaminated electronic water level meter into the monitoring well until the meter indicates the probe has contacted the groundwater surface. • Measure the depth to water from the survey reference mark (on the PVC well casing) to the nearest 0.01 foot. If no mark is present, measure the depth to water to the north side of the casing. • Record the water level measurements and total well depth on Form B. • Decontaminate the probe and tape in accordance with the decontamination procedures outlined in SOP 5. 4.0 Groundwater Sampling A groundwater sample collected from the well will be designated using the following letters and numbers. The letters “GW” is the designation for groundwater. Following the “GW”, the well ID will be listed followed by the date. For instance, GW1-010121 would designate a groundwater sample collected from well 1 on 01/01/2021. Groundwater purging and sampling may be performed utilizing a disposable bailer, a dedicated bladder pump, or a peristaltic pump. These data are recorded on Form C. 4.1 Field Equipment Calibration Field equipment is used during sampling activities to measure groundwater elevations, collect samples, and measure field parameters. Calibration of the multi-meter is done each day prior to collecting groundwater parameters. In general, calibration and operation of all equipment used for collection of samples and field parameters from monitoring wells will conform to the respective manufacturer’s specifications. Instrument calibrations and calibration checks shall be recorded on Form C. Field equipment function checks shall be performed in accordance with procedures described in this section. Calibration of pH meters shall be performed to pH standards (4, 7, or 10 standard units) bracketing the actual field measured value. The specific conductivity meter shall be calibrated to one of three standards, 2,000, 6,000, or 10,000 micro Siemens per centimeter (mS/cm), whichever is closer to the field measured value. Dissolved oxygen is calibrated using the barometric pressure method outlined by the manufacturer. ORP calibration standard is 220 mv at 25○C. 5.0 Peristaltic Pump Sampling Procedures The ¼-inch polyethylene tubing used to purge the groundwater is set in the mid-screen level in each well. These wells will be sampled in accordance with EPA SOP Low Stress (Low Flow) Purging and Sampling Procedure for The Collection of Groundwater Samples from Monitoring Wells (US EPA, 1996 and 2010). The well purging process for a monitoring well using a peristaltic pump consists of the following steps: 1. Measurements of DO, SC, temperature, pH, and ORP will occur by way of probes that are installed in a clear flow through cell. The pumps flow rate will be set to an approximate flow rate of between 100-200 milliliters per minute (mL/min). The flow rate Johnston Leigh Inc. Standard Operating Procedure DERR 2024 Page 7 will be adjusted for long pulses of water, so one pump cycle will deliver a minimum of 40 mL of water as recommended by EPA Low-Stress Standard Operating Procedure (US EPA, 2010). 2. Purge groundwater from the monitoring well into a bucket to check for potential sheen. 3. Record the parameters DO, SC, temperature, pH, and ORP at a frequency of 5 minute intervals. Stabilization is considered to be achieved when three consecutive readings are within the following limits: • DO. 10% for values greater than 0.5 mg/L; if three DO values are less than 0.5 mg/L, consider the values stable; • SC. 3%; • Temperature. 3%; • pH +- 0.2 unit; and • ORP. +- 100 millivolts (mV). 4. Fill the sample bottles for BTEX first. Sample bottles for these analytes must be filled such that there is no headspace in the bottle. 5. Continue to collect groundwater to fill all other sample bottles filling the VOC bottles first (no headspace), SVOC second (no Headspace), metals third and any remaining COCs fourth. 6. Purge water is containerized and transported to the refinery process wastewater treatment system. 7. Record the sample description and required information on the chain-of-custody form. 6.0 Bailer Purging and Sampling Procedures Well purging and sampling procedures will be performed using disposable bailers in wells that do not contain dedicated sampling pumps. The procedure for sampling using disposable bailers is provided below. The purge and sample data is recorded on Form C. The well purging process for a monitoring well using a disposable bailer consists of the following steps: 1. Attach new nylon rope to a disposable bailer before well evacuation activities. Discard the nylon rope after the monitoring well has been sampled. 2. Purge groundwater from the monitoring well into a bucket to gauge the volume of water recovered. After purging each well volume, take field parameter measurements by following these directions. Pour well water directly from the bailer into a sample cup and measure temperature, pH, and specific conductance, dissolved oxygen and ORP with the multi parameter meter. Record the groundwater parameter measurements on Form C, after the readings on the meter have stabilized. 3. Bail three well casing volumes and record the volume bailed on Form C. Because the wells are completed with a 2-inch casing, the following equation can be used to calculate one casing volume: (TD – DTW) X 0.163 = 1 casing volume in gallons Where: TD = total well depth DTW = depth to water 4. Discharge purged water into an approved polyethylene drum. The purge water will be discharged to the refinery process wastewater treatment system. 5. If the well is bailed dry before three well casing volumes have been evacuated, then Johnston Leigh Inc. Standard Operating Procedure DERR 2024 Page 8 record the volume bailed on Form C and allow the well to recover (no longer than 24 hours). 6. Once three well volumes have been removed (or purged dry and recovered 24 hours) and the field parameters have been recorded, slowly lower the bailer into the monitoring well to avoid agitation of the groundwater. Fill the sample bottles for VOC first (no headspace), SVOC second (no Headspace), metals third and any remaining COCs fourth. Sample bottles for these analytes must be filled such that there is no headspace in the bottle. 7. Record the sample description and required information on the chain-of-custody form. Johnston Leigh Inc. Standard Operating Procedure DERR 2024 Page 9 SOP 4 Slug Test 1.0 Slug Test A 10 PSI pressure transducer is threaded through a 2-inch well cap with rubber grommet that seals the inside of the well. The pressure transducer is placed near the center of the well screen (approximately 12 feet BGS). The well cap is fitted with a bicycle tire type valve to allow pressurizing in inside of the well. 2.0 Pneumatic Test Apparatus In pneumatic slug testing, the well head is sealed and air pressure or vacuum is used to change the static water level. As air pressure in the well is increased or decreased, the water level changes until the water pressure "up" and the air pressure "down" are equal. Once the water level is stable, a release valve is quickly opened, instantaneously releasing the air pressure or vacuum. The water level recovers without splashing and the pressure transducer and data logger/computer record the changes in water level and time. A slug test performed at a well will be referenced in the database management system in the same manner as the soil and groundwater samples. This will allow the selection of the calculated K value derived from the slug test from the same XYZ data management system. The letter “K” is the designation for hydraulic conductivity value, followed by the well number and date. For instance, K1-010121 would designate a slug test K value calculated from well 1 on 01/01/2021. Johnston Leigh Inc. Standard Operating Procedure DERR 2024 Page 10 SOP 5 Sub-Slab Air Sampling 1.0 Installation Select the locations for installation of brass pre-constructed Vapor Pin®. Divide the building into thirds, place one sub-slab vapor pin near the center of each third, if possible. The depth of the vapor pin is determined by the depth of the concrete slab; however, each Vapor Pin® is to be installed just below the concrete slab such that the potential vapors immediately below the concrete slab are being sampled. A 1.5-inch diameter hole will be drilled to a depth of approximately 1.75-inches deep. This is to allow the Vapor Pin® to be recessed below the concrete surface. Set the supplied drill bit flange in the 1.75-inch diameter hole as a guide to drill a 5/8-inch diameter Vapor Pin® hole through the concrete slab. Extend the drill bit a couple of inches below the concrete slab to verify the Vapor Pin® hole is completely through the concrete slab. Fit the supplied silicon sleeve over the Vapor Pin® and insert it inside the 5/8- inch diameter hole using the supplied tap and cover that protects the barbed fitting on top of the Vapor Pin®. Set the supplied stainless steel cap flush to the floor to cover the Vapor Pin®. 2.0 Sampling Each brass Vapor Pin® will be purged of vapor after installation and then allowed to set undisturbed for 48 hours before collecting a grab sample from each Vapor Pin®. Rather than purging three volumes of air from the Vapor Pin® and tubing before collecting a sample, each Vapor Pin® will be purged using a PID and O2 meter at a rate <= 0.2 liters per minute and collect the air sample after the PID and O2 levels have stabilized. A grab sample will be collected from each Vapor Pin® by attaching one end of Tygon™ and Nylaflow LM ¼-inch diameter tubing to the Vapor Pin® and the other end to a 1 liter Summa TO-CAN. The grab sample is collected by opening the sampling valve of the pre-evacuated canister and allowing the canister to fill to ambient pressure (typically a minute or less). One grab sample will be collected from each Vapor Pin® weekly for four consecutive weeks following EPA SOPs (EPA ERT #2042, 2001). The atmospheric pressure, wind speed, precipitation and temperature at the site the days samples are collected will be recorded. The soil gas samples will be shipped overnight delivery to and analyzed by Pace Laboratory for VOCs using EPA Method TO-15. Johnston Leigh Inc. Standard Operating Procedure DERR 2024 Page 11 SOP 6 Decontamination 1.0 Hand Tools and Equipment Hand tools and equipment will be decontaminated between each sample location by using a three-bucket wash and rinse system. The sampling equipment will be washed in the first bucket using low-phosphate detergent and tap water, followed by a triple rinse in bucket two containing tap water and lastly a triple rinse in bucket three containing deionized/distilled water. The sampling equipment will then be allowed to air dry before proceeding to the next sampling grid. One equipment rinseate sample per day may be collected by pouring distilled water over the decontaminated field equipment and collecting the rinseate water into the sample containers. The equipment rinseate sample will be submitted to the laboratory for analyses of COCs in the work plan. 2.0 Push Probe/Drilling Equipment All down hole drilling equipment and associated tools will be pressure-washed between boreholes. Pipe racks or similar will be used to elevate the drilling equipment (e.g., rods and augers) during pressure washing. Decontamination of the DT35 outer and inner rods may be accomplished using a mobile decontamination pad (MDP) constructed in an open double axel trailer, or on bermed plastic placed over an asphalt pavement surface. The outer and inner rods would be pressured washed within the MDP and the fluids would be contained in the MDP or plastic bermed area and allowed to evaporate. Johnston Leigh Inc. Standard Operating Procedure DERR 2024 Page 12 SOP 7 FIELD SCREENING PHOTO IONIZATION DETECTOR (PID) 1.0 Objective This procedure describes the field-screening method of analyzing organic vapors emitted from within the pore spaces of a soil sample. Following appropriate techniques, the real-time data can be used to estimate relative levels of organic contamination in the soil. In addition to providing assessment information, headspace analysis can be used for health and safety purposes. 2.0 EQUIPMENT AND SUPPLIES The following equipment and supplies are necessary to conduct field headspace testing: • Photoionization detector (PID) • Calibration gas standards for PID of known concentrations (SOP 8) • DT35 Dual tube sampling system. • Ziplock plastic baggies. 3.0 PROCEDURE The following procedure will be used for field headspace testing of soil samples: 1. The PID is calibrated daily to a standard of 100 parts per million (PPM) isobutylene (SOP 8). 2. When the outer rods are driven into the subsurface, the cutting shoes shears a 2.125- inch OD soil core inside a clear plastic liner that is attached to the smaller inner rods. Once filled, the liner with the soil sample is removed from the bottom of the outer casing by lifting the inner rods. 3. Cut the plastic sleeve length wise to expose the sample and remove the soil to be tested with the PID. Granular soils should be broken apart and cohesive soils should be broken by crushing the sample as it is placed in the ziplock plastic bag. Place approximately 100-500 grams of soil in the ziplock plastic bag. Place the ziplock plastic bag in the sun to warm or on the dashboard of the truck to warm the sample for approximately 5-10 minutes. 4. Turn the PID on before opening the ziplock plastic bag. Open one end of the ziplock bag just enough to insert the PID probe and then pinch the plastic bag around the PID probe tip. Take a PID reading, results will be PPM. 5. Record the PID reading on the boring log at the depth of the sample tested. Repeat this process for any sampled depth of interest. Johnston Leigh Inc. Standard Operating Procedure DERR 2024 Page 13 SOP 8 EQUIPMENT CALIBRATION 1.0 Objective Parameters which would be likely to change with time prior to delivery to the laboratory are generally measured in the field. Because of the potential for temporal differences in measured values, laboratory measurements of these parameters, although potentially more precise, would be less accurate than measurements collected in the field. In addition, field measurements can serve as an initial screening tool to evaluate relative degree of physical properties of samples. Field measurements are typically performed for the following parameters: (1) total volatile organic vapors in soil, (2) fluid pH, (3) fluid specific conductance (Cond), (4) fluid temperature (T),fluid oxidation/reduction potential (ORP), and dissolved oxygen (DO). The equipment to be used for the above parameters include, a Photoionization detector (PID) total organic vapors in soil and groundwater, a YSI 6500 Water Quality Meter for pH, T, Cond, ORP and DO. JLI uses a Geopump® peristaltic pump connected to a flow through cell to collected groundwater samples when the depth to groundwater is less than 20 feet. The calibration and maintenance history, as appropriate, of all equipment used to make measurements will be recorded in the field note book. In general, equipment must be checked for calibration on a daily basis and according to manufacturer's equipment operation procedure. 2.0 CALIBRATION 2.1 Photoionization Detector (PID) The PID must be calibrated in order to display concentration in units’ equivalent to PPM. First a supply of clean air, which contains no off gases or vapors, is used to set the zero point. Then, isobutylene at 100 PPM (span gas), is used to set the reference standard. The cylinder of span gas and flow regulator needed for calibration is included with the PID instrument. 2.2 YSI 6500 Water Quality Meter The YSI meter is calibrated daily for pH, T, Cond and DO. The YSI meter is factory calibrated for T and ORP and this calibration is updated every 6 months. The YSI meter is calibrated for ph, Cond and DO by turning on the instrument and selecting the calibration function. The screen displays the calibration steps the user follows using the following standards: • pH – calibrated to 4, 7 and 10 • Cond – calibrated to known solution of 10,000 microsiemens per centimeter (ugS/cm) • DO – calibrated by entering the local barometric pressure in mm/hg. Johnston Leigh Inc. Standard Operating Procedure DERR 2024 Page 14 SOP 9 SAMPLING MANAGEMENT CHAIN OF CUSTODY 1.0 Objective This section describes sample handling and shipping documentation requirements to ensure the integrity of the samples collected and submitted to the laboratory for analysis, and to provide the laboratory with explicit instructions for the analytical services required. The following general procedures are summarized in this section: • Sample labeling, • Sample packaging and shipping, and • Chain-of-custody. 2.0 Sample Labeling All sample containers will be labeled using waterproof ink with the following information on labels: • Client or project name, • Sample identification number, • Date and time of collection, • Requested analysis, and • Container type and type of preservation used. All groundwater samples collected each day are to be listed on the Daily Field Log (Form A). Duplicate samples will be labeled with a “D” after the well ID. A fictitious sample ID number is not needed since the internal QAQC laboratory report serves as additional checks on the laboratory QAQC policy. 3.0 Sample Packaging and Shipping The following procedures apply to all groundwater samples packed for transport to the laboratory: • Place each sample into an individual laboratory supplied bubble wrap bag. • Each sample from the well will be comprised of 4-40milliliters (mL) vials for BTEX and GRO, and 4-40 mL vial for DRO. These are all placed into a 1-liter sealable baggie and labeled on the outside of the baggie with the sample name, date, and sample time. This is performed to verify the sample during preparation of the chain of custody, and to assist the laboratory personnel at the log in procedure at the laboratory. • Place bubble wraps on the inside bottom of the cooler. • Line the cooler with a laboratory supplied 6-millimeter thick clear plastic bag (plastic bag) that extends above the cooler at least 18-inches so the bag can be sealed with a zip-tie strap. • Place the samples inside the plastic bag and pack the plastic bag with the contents of one bag of crushed ice. Spread the ice evenly over the entire contents of the plastic bag. Zip tie the plastic bag shut. • Place the completed chain of custody inside a 1-liter sealable baggie and tape the baggie to the inside lid of the cooler. • Remove any expired shipping label for the cooler. Place the laboratory supplied overnight priority shipping label on the cooler. Remove the receipt of the shipping label and attach it to the copy of the chain of custody that is inside the cooler. • Attach two signed custody seals over the cooler lid where it seals to the body of the Johnston Leigh Inc. Standard Operating Procedure DERR 2024 Page 15 cooler. Tape the cooler shut by wrapping shipping tape around the cooler lid and base and over the custody seals at least two layers thick. • Ship the coolers using Federal Express or United Parcel Service only from a distribution location that is staffed by company personnel. No shipping cooler is ever to be left unattended at a drop location. 4.0 Chain-of-Custody Chain-of-custody is a mechanism employed to ensure that data resulting from laboratory analysis are credible and defensible. Chain-of-custody begins at the time and point of sample collection. Documentation of sample possession and chain-of-custody is provided by the use of sample labels and chain-of-custody forms. The chain-of-custody record will be initiated in the field and will accompany each sample during shipment to the laboratory. The chain-of-custody record allows transfer of custody of a sample or group of samples in the field to any laboratory. Information listed on the chain-of-custody includes: • Sample Identification; • Project name, location, and number; • Sampling dates and times; • Name of sampling technician(s); • Media being tested for each sample; • Number of containers per sample; • Signature of person relinquishing and receiving custody; • Requested analyses for each sample; and • Special requirements/comments for project or analysis. The sampler relinquishing the samples will keep one copy of the chain-of-custody forms and send the remaining copies with the samples. The chain-of-custody form shall be sealed in a waterproof plastic bag and placed inside the shipping container. Johnston Leigh Inc. Standard Operating Procedure DERR 2024 Page 16 SOP 10 INVESTIGATION DERIVED WASTE 1.0 Classification Investigation derived waste (IDW) will include soil, groundwater, and personal protection equipment (PPE). The following IDW rules will apply for the SAP. 2.0 Soil Soil is generated from core samples recovered from the push probe plastic sleeves. The unused soil is considered deminimus and will be broken into fine media and remain onsite. If required by MT DEQ, a Waste Profile Sheet will be completed with the required analytical documentation for offsite transportation and disposal. This will be further discussed in the work plan if required by the site-specific conditions. 3.0 Groundwater Groundwater purged from the wells using low flow procedure is considered deminimus and will l first be containerized in a bucket to document the volume of water removed. The groundwater will then be discharged to an asphalt surface away from storm drains and allowed to evaporate. 4.0 PPE PPE does not warrant any special disposal. PPE will be disposed of in trash receptacles. ATTACHMENT C ATTACHMENT D FIELD NOTES GROUNDWATER SAMPLING 08/27-28/2024 CommonCents, 907 North 400 East, Harrisville, Utah Facility 1200401, Release MSBCommon Cents Harrisville DTW Date Well Water DTP DTW Well DO ORP COND pH TEMP Sample 08/27/24 Elevation Elevation (feet)(feet)I.D.(mg/L)(mv)(ms/cm)C Time Sample Date 99.11 92.57 6.54 MW1 98.65 89.48 9.17 MW2 08/28/24 98.30 89.65 8.65 MW3 5.57 1.70 6.85 78.9 1100 GW-MW3 98.56 91.82 6.74 MW4 08/28/24 97.81 91.73 6.08 MW5 1.08 2.50 7.34 19.5 1030 GW-MW5 98.82 92.11 6.71 MW6 99.80 93.74 6.06 MW7 98.51 MW8 08/28/24 98.73 90.49 8.24 MW9 0.44 2.95 7.33 17.9 1200 GW-MW9 98.22 91.01 7.21 MW10 08/28/24 93.03 86.79 6.24 MW11 0.81 3.03 7.20 20.0 1130 GW-MW11 99.03 89.95 9.08 MW14 08/28/24 99.05 87.28 11.77 MW15 2.09 5.01 7.85 16.6 1000 GW-MW15 08/28/24 97.36 88.59 8.77 MW16 0.45 1.48 7.45 21.1 930 GW-MW16 08/28/24 97.67 89.10 8.57 MW17 0.38 2.23 7.27 21.4 900 GW-MW17 MW-2 accessible on 8/27/2024 but a car was parked on the well all day on 8/28/2024 and owner could not be located Sample Name Common Cents Harrisville, UT Page 1 of 1 08/27-28/2024 ATTACHMENT E ANALYTICAL REPORT August 31, 2024 Johnston, Leigh, Inc. Sample Delivery Group:L1768962 Samples Received:08/17/2024 Project Number: Description:Site Investigation Site:HARRISVILLE, UT Report To:Leigh Beem 1820 S Palomar Ln Kanab, UT 84741 Entire Report Reviewed By: August 31, 2024 [Preliminary Report] John Hawkins Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received. Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 mydata.pacelabs.com 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 08/31/24 18:29 1 of 16 September 03, 2024 John Hawkins Project Manager ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 09/03/24 07:43 1 of 16 TABLE OF CONTENTS Cp: Cover Page 1 Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results 5 SB-MW15 6-7 L1768962-01 5 SB-MW16 7-8 L1768962-02 6 SB-MW17 9-10 L1768962-03 7 Qc: Quality Control Summary 8 Total Solids by Method 2540 G-2011 8 Volatile Organic Compounds (GC) by Method 8015D/GRO 10 Volatile Organic Compounds (GC/MS) by Method 8260B 11 Semi-Volatile Organic Compounds (GC) by Method 8015 12 Gl: Glossary of Terms 14 Al: Accreditations & Locations 15 Sc: Sample Chain of Custody 16 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 08/31/24 18:29 2 of 16 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 09/03/24 07:43 2 of 16 SAMPLE SUMMARY Collected by Collected date/time Received date/time SB-MW15 6-7 L1768962-01 Solid Leigh Beem 08/15/24 14:45 08/17/24 08:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG2348064 1 08/22/24 10:14 08/22/24 10:23 CMB Mt. Juliet, TN Volatile Organic Compounds (GC) by Method 8015D/GRO WG2350876 33.5 08/15/24 14:45 08/27/24 02:56 NCD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260B WG2348794 1.34 08/15/24 14:45 08/24/24 11:22 DWR Mt. Juliet, TN Semi-Volatile Organic Compounds (GC) by Method 8015 WG2352560 1 08/29/24 14:14 08/30/24 02:21 KKS Mt. Juliet, TN Collected by Collected date/time Received date/time SB-MW16 7-8 L1768962-02 Solid Leigh Beem 08/16/24 09:00 08/17/24 08:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG2348065 1 08/22/24 09:47 08/22/24 09:54 CMB Mt. Juliet, TN Volatile Organic Compounds (GC) by Method 8015D/GRO WG2350876 61.8 08/16/24 09:00 08/27/24 03:15 NCD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260B WG2348794 2.47 08/16/24 09:00 08/24/24 11:41 DWR Mt. Juliet, TN Semi-Volatile Organic Compounds (GC) by Method 8015 WG2352562 5 08/29/24 15:03 08/30/24 16:31 KKS Mt. Juliet, TN Collected by Collected date/time Received date/time SB-MW17 9-10 L1768962-03 Solid Leigh Beem 08/16/24 10:00 08/17/24 08:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG2348065 1 08/22/24 09:47 08/22/24 09:54 CMB Mt. Juliet, TN Volatile Organic Compounds (GC) by Method 8015D/GRO WG2350876 36.5 08/16/24 10:00 08/27/24 03:35 NCD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260B WG2348794 1.46 08/16/24 10:00 08/24/24 12:01 DWR Mt. Juliet, TN Semi-Volatile Organic Compounds (GC) by Method 8015 WG2352562 1 08/29/24 15:03 08/30/24 01:54 KKS Mt. Juliet, TN 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 08/31/24 18:29 3 of 16 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 09/03/24 07:43 3 of 16 CASE NARRATIVE All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. [Preliminary Report] John Hawkins Project Manager 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 08/31/24 18:29 4 of 16 John Hawkins Project Manager ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 09/03/24 07:43 4 of 16 SAMPLE RESULTS - 01 L1768962 SB-MW15 6-7 Collected date/time: 08/15/24 14:45 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 79.8 1 08/22/2024 10:23 WG2348064 Volatile Organic Compounds (GC) by Method 8015D/GRO Result (dry)Qualifier RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) Low Fraction ND 4.83 33.5 08/27/2024 02:56 WG2350876 (S) a,a,a-Trifluorotoluene(FID)87.5 77.0-120 08/27/2024 02:56 WG2350876 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg date / time Benzene ND 0.00193 1.34 08/24/2024 11:22 WG2348794 Toluene ND 0.00966 1.34 08/24/2024 11:22 WG2348794 Ethylbenzene ND 0.00483 1.34 08/24/2024 11:22 WG2348794 Total Xylenes ND 0.0126 1.34 08/24/2024 11:22 WG2348794 Methyl tert-butyl ether 0.0718 0.00193 1.34 08/24/2024 11:22 WG2348794 Naphthalene ND J3 0.0242 1.34 08/24/2024 11:22 WG2348794 (S) Toluene-d8 105 75.0-131 08/24/2024 11:22 WG2348794 (S) 4-Bromofluorobenzene 93.0 67.0-138 08/24/2024 11:22 WG2348794 (S) 1,2-Dichloroethane-d4 95.4 70.0-130 08/24/2024 11:22 WG2348794 Semi-Volatile Organic Compounds (GC) by Method 8015 Result (dry)Qualifier RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) High Fraction ND 5.01 1 08/30/2024 02:21 WG2352560 (S) o-Terphenyl 46.6 18.0-148 08/30/2024 02:21 WG2352560 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 08/31/24 18:29 5 of 16 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 09/03/24 07:43 5 of 16 SAMPLE RESULTS - 02 L1768962 SB-MW16 7-8 Collected date/time: 08/16/24 09:00 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 71.4 1 08/22/2024 09:54 WG2348065 Volatile Organic Compounds (GC) by Method 8015D/GRO Result (dry)Qualifier RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) Low Fraction ND 9.65 61.8 08/27/2024 03:15 WG2350876 (S) a,a,a-Trifluorotoluene(FID)95.1 77.0-120 08/27/2024 03:15 WG2350876 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg date / time Benzene ND 0.00386 2.47 08/24/2024 11:41 WG2348794 Toluene ND 0.0194 2.47 08/24/2024 11:41 WG2348794 Ethylbenzene ND 0.00965 2.47 08/24/2024 11:41 WG2348794 Total Xylenes ND 0.0251 2.47 08/24/2024 11:41 WG2348794 Methyl tert-butyl ether 0.00617 0.00386 2.47 08/24/2024 11:41 WG2348794 Naphthalene 0.0844 J3 0.0483 2.47 08/24/2024 11:41 WG2348794 (S) Toluene-d8 106 75.0-131 08/24/2024 11:41 WG2348794 (S) 4-Bromofluorobenzene 93.7 67.0-138 08/24/2024 11:41 WG2348794 (S) 1,2-Dichloroethane-d4 97.0 70.0-130 08/24/2024 11:41 WG2348794 Semi-Volatile Organic Compounds (GC) by Method 8015 Result (dry)Qualifier RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) High Fraction 50.3 28.0 5 08/30/2024 16:31 WG2352562 (S) o-Terphenyl 47.0 18.0-148 08/30/2024 16:31 WG2352562 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 08/31/24 18:29 6 of 16 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 09/03/24 07:43 6 of 16 SAMPLE RESULTS - 03 L1768962 SB-MW17 9-10 Collected date/time: 08/16/24 10:00 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 77.9 1 08/22/2024 09:54 WG2348065 Volatile Organic Compounds (GC) by Method 8015D/GRO Result (dry)Qualifier RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) Low Fraction ND 5.39 36.5 08/27/2024 03:35 WG2350876 (S) a,a,a-Trifluorotoluene(FID)86.4 77.0-120 08/27/2024 03:35 WG2350876 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg date / time Benzene ND 0.00216 1.46 08/24/2024 12:01 WG2348794 Toluene ND 0.0108 1.46 08/24/2024 12:01 WG2348794 Ethylbenzene ND 0.00539 1.46 08/24/2024 12:01 WG2348794 Total Xylenes ND 0.0140 1.46 08/24/2024 12:01 WG2348794 Methyl tert-butyl ether 0.0205 0.00216 1.46 08/24/2024 12:01 WG2348794 Naphthalene ND J3 0.0270 1.46 08/24/2024 12:01 WG2348794 (S) Toluene-d8 103 75.0-131 08/24/2024 12:01 WG2348794 (S) 4-Bromofluorobenzene 95.0 67.0-138 08/24/2024 12:01 WG2348794 (S) 1,2-Dichloroethane-d4 96.1 70.0-130 08/24/2024 12:01 WG2348794 Semi-Volatile Organic Compounds (GC) by Method 8015 Result (dry)Qualifier RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) High Fraction ND 5.13 1 08/30/2024 01:54 WG2352562 (S) o-Terphenyl 58.6 18.0-148 08/30/2024 01:54 WG2352562 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 08/31/24 18:29 7 of 16 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 09/03/24 07:43 7 of 16 QUALITY CONTROL SUMMARYWG2348064 Total Solids by Method 2540 G-2011 L1768962-01 Method Blank (MB) (MB) R4110627-1 08/22/24 10:23 MB Result MB Qualifier MB MDL MB RDL Analyte %%% Total Solids 0.00200 L1768962-01 Original Sample (OS) • Duplicate (DUP) (OS) L1768962-01 08/22/24 10:23 • (DUP) R4110627-3 08/22/24 10:23 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte %%%% Total Solids 79.8 80.6 1 0.939 10 Laboratory Control Sample (LCS) (LCS) R4110627-2 08/22/24 10:23 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte %%%% Total Solids 50.0 50.0 99.9 90.0-110 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 08/31/24 18:29 8 of 16 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 09/03/24 07:43 8 of 16 QUALITY CONTROL SUMMARYWG2348065 Total Solids by Method 2540 G-2011 L1768962-02,03 Method Blank (MB) (MB) R4110408-1 08/22/24 09:54 MB Result MB Qualifier MB MDL MB RDL Analyte %%% Total Solids 0.00100 L1768962-02 Original Sample (OS) • Duplicate (DUP) (OS) L1768962-02 08/22/24 09:54 • (DUP) R4110408-3 08/22/24 09:54 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte %%%% Total Solids 71.4 66.2 1 7.62 10 Laboratory Control Sample (LCS) (LCS) R4110408-2 08/22/24 09:54 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte %%%% Total Solids 50.0 50.0 100 90.0-110 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 08/31/24 18:29 9 of 16 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 09/03/24 07:43 9 of 16 QUALITY CONTROL SUMMARYWG2350876 Volatile Organic Compounds (GC) by Method 8015D/GRO L1768962-01,02,03 Method Blank (MB) (MB) R4113094-2 08/27/24 01:42 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg TPH (GC/FID) Low Fraction 1.09 J 0.543 2.50 (S) a,a,a-Trifluorotoluene(FID)89.8 77.0-120 Laboratory Control Sample (LCS) (LCS) R4113094-1 08/27/24 00:35 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% TPH (GC/FID) Low Fraction 5.00 5.76 115 72.0-127 (S) a,a,a-Trifluorotoluene(FID) 97.6 77.0-120 L1769545-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1769545-04 08/27/24 07:29 • (MS) R4113094-3 08/27/24 08:08 • (MSD) R4113094-4 08/27/24 08:27 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% TPH (GC/FID) Low Fraction 186 ND 213 214 114 114 37.3 10.0-151 0.468 28 (S) a,a,a-Trifluorotoluene(FID) 102 98.0 77.0-120 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 08/31/24 18:29 10 of 16 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 09/03/24 07:43 10 of 16 QUALITY CONTROL SUMMARYWG2348794 Volatile Organic Compounds (GC/MS) by Method 8260B L1768962-01,02,03 Method Blank (MB) (MB) R4111532-3 08/24/24 04:41 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Benzene U 0.000467 0.00100 Toluene U 0.00130 0.00500 Ethylbenzene U 0.000737 0.00250 Total Xylenes U 0.000880 0.00650 Methyl tert-butyl ether U 0.000350 0.00100 Naphthalene U 0.00488 0.0125 (S) Toluene-d8 104 75.0-131 (S) 4-Bromofluorobenzene 91.4 67.0-138 (S) 1,2-Dichloroethane-d4 95.9 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R4111532-1 08/24/24 03:05 • (LCSD) R4111532-2 08/24/24 03:24 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% Benzene 0.125 0.118 0.124 94.4 99.2 70.0-123 4.96 20 Toluene 0.125 0.130 0.133 104 106 75.0-121 2.28 20 Ethylbenzene 0.125 0.136 0.135 109 108 74.0-126 0.738 20 Total Xylenes 0.375 0.407 0.399 109 106 72.0-127 1.99 20 Methyl tert-butyl ether 0.125 0.124 0.129 99.2 103 66.0-132 3.95 20 Naphthalene 0.125 0.121 0.148 96.8 118 59.0-130 J3 20.1 20 (S) Toluene-d8 105 100 75.0-131 (S) 4-Bromofluorobenzene 91.3 91.1 67.0-138 (S) 1,2-Dichloroethane-d4 103 102 70.0-130 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 08/31/24 18:29 11 of 16 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 09/03/24 07:43 11 of 16 QUALITY CONTROL SUMMARYWG2352560 Semi-Volatile Organic Compounds (GC) by Method 8015 L1768962-01 Method Blank (MB) (MB) R4114082-1 08/30/24 00:20 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg TPH (GC/FID) High Fraction U 0.769 4.00 (S) o-Terphenyl 56.3 18.0-148 Laboratory Control Sample (LCS) (LCS) R4114082-2 08/30/24 00:33 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% TPH (GC/FID) High Fraction 50.0 28.6 57.2 50.0-150 (S) o-Terphenyl 55.0 18.0-148 L1768920-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1768920-01 08/30/24 18:22 • (MS) R4114082-3 08/30/24 18:35 • (MSD) R4114082-4 08/30/24 18:49 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% TPH (GC/FID) High Fraction 60.7 532 562 598 49.4 107 10 50.0-150 V 6.24 20 (S) o-Terphenyl 76.2 94.5 18.0-148 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 08/31/24 18:29 12 of 16 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 09/03/24 07:43 12 of 16 QUALITY CONTROL SUMMARYWG2352562 Semi-Volatile Organic Compounds (GC) by Method 8015 L1768962-02,03 Method Blank (MB) (MB) R4113997-1 08/30/24 00:20 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg TPH (GC/FID) High Fraction U 0.769 4.00 (S) o-Terphenyl 63.5 18.0-148 Laboratory Control Sample (LCS) (LCS) R4113997-2 08/30/24 00:33 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% TPH (GC/FID) High Fraction 50.0 34.7 69.4 50.0-150 (S) o-Terphenyl 68.9 18.0-148 L1768924-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1768924-05 08/30/24 00:47 • (MS) R4113997-3 08/30/24 01:00 • (MSD) R4113997-4 08/30/24 01:14 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% TPH (GC/FID) High Fraction 50.0 ND 30.3 27.1 60.6 54.2 1 50.0-150 11.1 20 (S) o-Terphenyl 55.9 51.4 18.0-148 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 08/31/24 18:29 13 of 16 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 09/03/24 07:43 13 of 16 GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions (dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils]. MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit. RDL (dry)Reported Detection Limit. Rec.Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. (S) Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. Dilution If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. Limits These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. Qualifier This column provides a letter and/or number designation that corresponds to additional information concerning the result reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. Result The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL” (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry)Confidence level of 2 sigma. Case Narrative (Cn) A brief discussion about the included sample results, including a discussion of any non-conformances to protocol observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control Summary (Qc) This section of the report includes the results of the laboratory quality control analyses required by procedure or analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. Sample Chain of Custody (Sc) This is the document created in the field when your samples were initially collected. This is used to verify the time and date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. Sample Results (Sr) This section of your report will provide the results of all testing performed on your samples. These results are provided by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description J The identification of the analyte is acceptable; the reported value is an estimate. J3 The associated batch QC was outside the established quality control range for precision. V The sample concentration is too high to evaluate accurate spike recoveries. 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 08/31/24 18:29 14 of 16 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 09/03/24 07:43 14 of 16 Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122 Alabama 40660 Nebraska NE-OS-15-05 Alaska 17-026 Nevada TN000032021-1 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey–NELAP TN002 California 2932 New Mexico ¹TN00003 Colorado TN00003 New York 11742 Connecticut PH-0197 North Carolina Env375 Florida E87487 North Carolina ¹DW21704 Georgia NELAP North Carolina ³41 Georgia ¹923 North Dakota R-140 Idaho TN00003 Ohio–VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LAO00356 Kentucky ¹ ⁶KY90010 South Carolina 84004002 Kentucky ²16 South Dakota n/a Louisiana AI30792 Tennessee ¹ ⁴2006 Louisiana LA018 Texas T104704245-20-18 Maine TN00003 Texas ⁵LAB0152 Maryland 324 Utah TN000032021-11 Massachusetts M-TN003 Vermont VT2006 Michigan 9958 Virginia 110033 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 998093910 Montana CERT0086 Wyoming A2LA A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2LA – ISO 17025 ⁵1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA–Crypto TN00003 ACCREDITATIONS & LOCATIONS ¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable * Not all certifications held by the laboratory are applicable to the results reported in the attached report. * Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical. 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 08/31/24 18:29 15 of 16 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1768962 09/03/24 07:43 15 of 16 ANALYTICAL REPORT September 12, 2024 Johnston, Leigh, Inc. Sample Delivery Group:L1772744 Samples Received:08/29/2024 Project Number: Description:Site Investigation Site:HARRISVILLE, UT Report To:Leigh Beem 1820 S Palomar Ln Kanab, UT 84741 Entire Report Reviewed By: September 12, 2024 [Preliminary Report] John Hawkins Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received. Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 mydata.pacelabs.com 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 1 of 28 September 12, 2024 John Hawkins Project Manager ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 1 of 28 TABLE OF CONTENTS Cp: Cover Page 1 Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 5 Sr: Sample Results 6 HNW L1772744-01 6 HNE L1772744-02 7 HSW L1772744-03 8 HSE L1772744-04 9 MW17 L1772744-05 10 MW16 L1772744-06 11 MW15 L1772744-07 12 MW9 L1772744-08 13 MW11 L1772744-09 14 MW13 L1772744-10 15 MW14 L1772744-11 16 Qc: Quality Control Summary 17 Volatile Organic Compounds (GC) by Method 8015D/GRO 17 Volatile Organic Compounds (GC/MS) by Method 8260B 19 Semi-Volatile Organic Compounds (GC) by Method 3511/8015 21 Gl: Glossary of Terms 25 Al: Accreditations & Locations 26 Sc: Sample Chain of Custody 27 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 2 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 2 of 28 SAMPLE SUMMARY Collected by Collected date/time Received date/time HNW L1772744-01 GW Leigh Beem 08/27/24 15:15 08/29/24 08:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC) by Method 8015D/GRO WG2357830 1 09/07/24 02:10 09/07/24 02:10 CDD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260B WG2355536 1 09/03/24 20:49 09/03/24 20:49 JCP Mt. Juliet, TN Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2357908 1 09/09/24 09:00 09/10/24 22:57 DMG Mt. Juliet, TN Collected by Collected date/time Received date/time HNE L1772744-02 GW Leigh Beem 08/27/24 15:45 08/29/24 08:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC) by Method 8015D/GRO WG2357830 1 09/07/24 02:32 09/07/24 02:32 CDD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260B WG2355536 1 09/03/24 21:09 09/03/24 21:09 JCP Mt. Juliet, TN Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2357908 1 09/09/24 09:00 09/10/24 23:17 DMG Mt. Juliet, TN Collected by Collected date/time Received date/time HSW L1772744-03 GW Leigh Beem 08/27/24 13:00 08/29/24 08:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC) by Method 8015D/GRO WG2357830 1 09/07/24 02:54 09/07/24 02:54 CDD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260B WG2355536 1 09/03/24 21:30 09/03/24 21:30 JCP Mt. Juliet, TN Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2357908 1 09/09/24 09:00 09/10/24 23:37 DMG Mt. Juliet, TN Collected by Collected date/time Received date/time HSE L1772744-04 GW Leigh Beem 08/27/24 14:00 08/29/24 08:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC) by Method 8015D/GRO WG2357830 1 09/07/24 03:16 09/07/24 03:16 CDD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260B WG2355536 1 09/03/24 21:50 09/03/24 21:50 JCP Mt. Juliet, TN Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2357908 1 09/09/24 09:00 09/10/24 23:58 DMG Mt. Juliet, TN Collected by Collected date/time Received date/time MW17 L1772744-05 GW Leigh Beem 08/28/24 09:00 08/29/24 08:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC) by Method 8015D/GRO WG2357830 1 09/07/24 03:38 09/07/24 03:38 CDD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260B WG2355536 1 09/03/24 22:11 09/03/24 22:11 JCP Mt. Juliet, TN Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2358514 1 09/09/24 09:19 09/09/24 21:08 DMG Mt. Juliet, TN Collected by Collected date/time Received date/time MW16 L1772744-06 GW Leigh Beem 08/28/24 09:30 08/29/24 08:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC) by Method 8015D/GRO WG2357830 1 09/07/24 04:00 09/07/24 04:00 CDD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260B WG2355536 1 09/03/24 22:31 09/03/24 22:31 JCP Mt. Juliet, TN Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2358514 1 09/09/24 09:19 09/10/24 19:10 DMG Mt. Juliet, TN 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 3 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 3 of 28 SAMPLE SUMMARY Collected by Collected date/time Received date/time MW15 L1772744-07 GW Leigh Beem 08/28/24 10:00 08/29/24 08:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC) by Method 8015D/GRO WG2357830 1 09/07/24 04:22 09/07/24 04:22 CDD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260B WG2355536 1 09/03/24 22:52 09/03/24 22:52 JCP Mt. Juliet, TN Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2358514 1 09/09/24 09:19 09/09/24 21:48 DMG Mt. Juliet, TN Collected by Collected date/time Received date/time MW9 L1772744-08 GW Leigh Beem 08/28/24 12:00 08/29/24 08:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC) by Method 8015D/GRO WG2357830 1 09/07/24 04:44 09/07/24 04:44 CDD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260B WG2358717 1 09/09/24 14:12 09/09/24 14:12 DWR Mt. Juliet, TN Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2358514 1 09/09/24 09:19 09/10/24 18:50 DMG Mt. Juliet, TN Collected by Collected date/time Received date/time MW11 L1772744-09 GW Leigh Beem 08/28/24 11:30 08/29/24 08:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC) by Method 8015D/GRO WG2357990 1 09/07/24 16:14 09/07/24 16:14 ACG Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260B WG2358717 1 09/09/24 14:30 09/09/24 14:30 DWR Mt. Juliet, TN Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2358544 1 09/11/24 06:45 09/12/24 00:20 DMG Mt. Juliet, TN Collected by Collected date/time Received date/time MW13 L1772744-10 GW Leigh Beem 08/28/24 10:30 08/29/24 08:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC) by Method 8015D/GRO WG2357990 10 09/07/24 20:36 09/07/24 20:36 ACG Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260B WG2358717 10 09/09/24 16:43 09/09/24 16:43 DWR Mt. Juliet, TN Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2358544 1 09/11/24 06:45 09/12/24 00:40 DMG Mt. Juliet, TN Collected by Collected date/time Received date/time MW14 L1772744-11 GW Leigh Beem 08/28/24 11:00 08/29/24 08:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC) by Method 8015D/GRO WG2357990 10 09/07/24 20:59 09/07/24 20:59 ACG Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260B WG2358717 20 09/09/24 17:02 09/09/24 17:02 DWR Mt. Juliet, TN Semi-Volatile Organic Compounds (GC) by Method 3511/8015 WG2358545 1 09/09/24 10:36 09/10/24 09:36 TJD Mt. Juliet, TN 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 4 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 4 of 28 CASE NARRATIVE All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. [Preliminary Report] John Hawkins Project Manager Sample Delivery Group (SDG) Narrative pH outside of method requirement. Lab Sample ID Project Sample ID Method L1772744-07 MW15 3511/8015 L1772744-08 MW9 3511/8015 L1772744-09 MW11 8015D/GRO, 3511/8015 L1772744-10 MW13 8015D/GRO, 3511/8015 L1772744-11 MW14 3511/8015 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 5 of 28 John Hawkins Project Manager ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 5 of 28 SAMPLE RESULTS - 01 L1772744 HNW Collected date/time: 08/27/24 15:15 Volatile Organic Compounds (GC) by Method 8015D/GRO Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) Low Fraction ND 0.100 1 09/07/2024 02:10 WG2357830 (S) a,a,a-Trifluorotoluene(FID)99.4 78.0-120 09/07/2024 02:10 WG2357830 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Benzene ND 0.00100 1 09/03/2024 20:49 WG2355536 Toluene ND 0.00100 1 09/03/2024 20:49 WG2355536 Ethylbenzene ND 0.00100 1 09/03/2024 20:49 WG2355536 Total Xylenes ND 0.00300 1 09/03/2024 20:49 WG2355536 Methyl tert-butyl ether ND 0.00100 1 09/03/2024 20:49 WG2355536 Naphthalene ND 0.00500 1 09/03/2024 20:49 WG2355536 (S) Toluene-d8 106 80.0-120 09/03/2024 20:49 WG2355536 (S) 4-Bromofluorobenzene 96.3 77.0-126 09/03/2024 20:49 WG2355536 (S) 1,2-Dichloroethane-d4 104 70.0-130 09/03/2024 20:49 WG2355536 Semi-Volatile Organic Compounds (GC) by Method 3511/8015 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) High Fraction ND 0.100 1 09/10/2024 22:57 WG2357908 (S) o-Terphenyl 76.3 52.0-156 09/10/2024 22:57 WG2357908 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 6 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 6 of 28 SAMPLE RESULTS - 02 L1772744 HNE Collected date/time: 08/27/24 15:45 Volatile Organic Compounds (GC) by Method 8015D/GRO Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) Low Fraction ND 0.100 1 09/07/2024 02:32 WG2357830 (S) a,a,a-Trifluorotoluene(FID)100 78.0-120 09/07/2024 02:32 WG2357830 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Benzene ND 0.00100 1 09/03/2024 21:09 WG2355536 Toluene ND 0.00100 1 09/03/2024 21:09 WG2355536 Ethylbenzene ND 0.00100 1 09/03/2024 21:09 WG2355536 Total Xylenes ND 0.00300 1 09/03/2024 21:09 WG2355536 Methyl tert-butyl ether ND 0.00100 1 09/03/2024 21:09 WG2355536 Naphthalene ND 0.00500 1 09/03/2024 21:09 WG2355536 (S) Toluene-d8 105 80.0-120 09/03/2024 21:09 WG2355536 (S) 4-Bromofluorobenzene 94.5 77.0-126 09/03/2024 21:09 WG2355536 (S) 1,2-Dichloroethane-d4 105 70.0-130 09/03/2024 21:09 WG2355536 Semi-Volatile Organic Compounds (GC) by Method 3511/8015 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) High Fraction ND 0.100 1 09/10/2024 23:17 WG2357908 (S) o-Terphenyl 76.8 52.0-156 09/10/2024 23:17 WG2357908 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 7 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 7 of 28 SAMPLE RESULTS - 03 L1772744 HSW Collected date/time: 08/27/24 13:00 Volatile Organic Compounds (GC) by Method 8015D/GRO Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) Low Fraction ND 0.100 1 09/07/2024 02:54 WG2357830 (S) a,a,a-Trifluorotoluene(FID)102 78.0-120 09/07/2024 02:54 WG2357830 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Benzene ND 0.00100 1 09/03/2024 21:30 WG2355536 Toluene ND 0.00100 1 09/03/2024 21:30 WG2355536 Ethylbenzene ND 0.00100 1 09/03/2024 21:30 WG2355536 Total Xylenes ND 0.00300 1 09/03/2024 21:30 WG2355536 Methyl tert-butyl ether ND 0.00100 1 09/03/2024 21:30 WG2355536 Naphthalene ND 0.00500 1 09/03/2024 21:30 WG2355536 (S) Toluene-d8 106 80.0-120 09/03/2024 21:30 WG2355536 (S) 4-Bromofluorobenzene 95.8 77.0-126 09/03/2024 21:30 WG2355536 (S) 1,2-Dichloroethane-d4 106 70.0-130 09/03/2024 21:30 WG2355536 Semi-Volatile Organic Compounds (GC) by Method 3511/8015 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) High Fraction ND 0.100 1 09/10/2024 23:37 WG2357908 (S) o-Terphenyl 77.4 52.0-156 09/10/2024 23:37 WG2357908 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 8 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 8 of 28 SAMPLE RESULTS - 04 L1772744 HSE Collected date/time: 08/27/24 14:00 Volatile Organic Compounds (GC) by Method 8015D/GRO Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) Low Fraction ND 0.100 1 09/07/2024 03:16 WG2357830 (S) a,a,a-Trifluorotoluene(FID)99.7 78.0-120 09/07/2024 03:16 WG2357830 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Benzene ND 0.00100 1 09/03/2024 21:50 WG2355536 Toluene ND 0.00100 1 09/03/2024 21:50 WG2355536 Ethylbenzene ND 0.00100 1 09/03/2024 21:50 WG2355536 Total Xylenes ND 0.00300 1 09/03/2024 21:50 WG2355536 Methyl tert-butyl ether ND 0.00100 1 09/03/2024 21:50 WG2355536 Naphthalene ND 0.00500 1 09/03/2024 21:50 WG2355536 (S) Toluene-d8 106 80.0-120 09/03/2024 21:50 WG2355536 (S) 4-Bromofluorobenzene 96.9 77.0-126 09/03/2024 21:50 WG2355536 (S) 1,2-Dichloroethane-d4 105 70.0-130 09/03/2024 21:50 WG2355536 Semi-Volatile Organic Compounds (GC) by Method 3511/8015 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) High Fraction ND 0.100 1 09/10/2024 23:58 WG2357908 (S) o-Terphenyl 80.0 52.0-156 09/10/2024 23:58 WG2357908 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 9 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 9 of 28 SAMPLE RESULTS - 05 L1772744 MW17 Collected date/time: 08/28/24 09:00 Volatile Organic Compounds (GC) by Method 8015D/GRO Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) Low Fraction ND 0.100 1 09/07/2024 03:38 WG2357830 (S) a,a,a-Trifluorotoluene(FID)99.8 78.0-120 09/07/2024 03:38 WG2357830 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Benzene ND 0.00100 1 09/03/2024 22:11 WG2355536 Toluene ND 0.00100 1 09/03/2024 22:11 WG2355536 Ethylbenzene ND 0.00100 1 09/03/2024 22:11 WG2355536 Total Xylenes ND 0.00300 1 09/03/2024 22:11 WG2355536 Methyl tert-butyl ether 0.0322 0.00100 1 09/03/2024 22:11 WG2355536 Naphthalene ND 0.00500 1 09/03/2024 22:11 WG2355536 (S) Toluene-d8 106 80.0-120 09/03/2024 22:11 WG2355536 (S) 4-Bromofluorobenzene 95.9 77.0-126 09/03/2024 22:11 WG2355536 (S) 1,2-Dichloroethane-d4 104 70.0-130 09/03/2024 22:11 WG2355536 Semi-Volatile Organic Compounds (GC) by Method 3511/8015 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) High Fraction 2.83 0.100 1 09/09/2024 21:08 WG2358514 (S) o-Terphenyl 94.2 52.0-156 09/09/2024 21:08 WG2358514 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 10 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 10 of 28 SAMPLE RESULTS - 06 L1772744 MW16 Collected date/time: 08/28/24 09:30 Volatile Organic Compounds (GC) by Method 8015D/GRO Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) Low Fraction ND 0.100 1 09/07/2024 04:00 WG2357830 (S) a,a,a-Trifluorotoluene(FID)98.9 78.0-120 09/07/2024 04:00 WG2357830 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Benzene ND 0.00100 1 09/03/2024 22:31 WG2355536 Toluene ND 0.00100 1 09/03/2024 22:31 WG2355536 Ethylbenzene ND 0.00100 1 09/03/2024 22:31 WG2355536 Total Xylenes ND 0.00300 1 09/03/2024 22:31 WG2355536 Methyl tert-butyl ether 0.0330 0.00100 1 09/03/2024 22:31 WG2355536 Naphthalene ND 0.00500 1 09/03/2024 22:31 WG2355536 (S) Toluene-d8 106 80.0-120 09/03/2024 22:31 WG2355536 (S) 4-Bromofluorobenzene 95.8 77.0-126 09/03/2024 22:31 WG2355536 (S) 1,2-Dichloroethane-d4 101 70.0-130 09/03/2024 22:31 WG2355536 Semi-Volatile Organic Compounds (GC) by Method 3511/8015 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) High Fraction 0.529 0.100 1 09/10/2024 19:10 WG2358514 (S) o-Terphenyl 74.7 52.0-156 09/10/2024 19:10 WG2358514 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 11 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 11 of 28 SAMPLE RESULTS - 07 L1772744 MW15 Collected date/time: 08/28/24 10:00 Volatile Organic Compounds (GC) by Method 8015D/GRO Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) Low Fraction 0.180 0.100 1 09/07/2024 04:22 WG2357830 (S) a,a,a-Trifluorotoluene(FID)99.7 78.0-120 09/07/2024 04:22 WG2357830 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Benzene ND 0.00100 1 09/03/2024 22:52 WG2355536 Toluene ND 0.00100 1 09/03/2024 22:52 WG2355536 Ethylbenzene ND 0.00100 1 09/03/2024 22:52 WG2355536 Total Xylenes ND 0.00300 1 09/03/2024 22:52 WG2355536 Methyl tert-butyl ether 0.139 0.00100 1 09/03/2024 22:52 WG2355536 Naphthalene ND 0.00500 1 09/03/2024 22:52 WG2355536 (S) Toluene-d8 106 80.0-120 09/03/2024 22:52 WG2355536 (S) 4-Bromofluorobenzene 95.6 77.0-126 09/03/2024 22:52 WG2355536 (S) 1,2-Dichloroethane-d4 102 70.0-130 09/03/2024 22:52 WG2355536 Semi-Volatile Organic Compounds (GC) by Method 3511/8015 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) High Fraction 1.08 0.100 1 09/09/2024 21:48 WG2358514 (S) o-Terphenyl 56.8 52.0-156 09/09/2024 21:48 WG2358514 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 12 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 12 of 28 SAMPLE RESULTS - 08 L1772744 MW9 Collected date/time: 08/28/24 12:00 Volatile Organic Compounds (GC) by Method 8015D/GRO Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) Low Fraction ND 0.100 1 09/07/2024 04:44 WG2357830 (S) a,a,a-Trifluorotoluene(FID)99.8 78.0-120 09/07/2024 04:44 WG2357830 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Benzene ND 0.00100 1 09/09/2024 14:12 WG2358717 Toluene ND 0.00100 1 09/09/2024 14:12 WG2358717 Ethylbenzene ND 0.00100 1 09/09/2024 14:12 WG2358717 Total Xylenes ND 0.00300 1 09/09/2024 14:12 WG2358717 Methyl tert-butyl ether 0.0474 0.00100 1 09/09/2024 14:12 WG2358717 Naphthalene ND 0.00500 1 09/09/2024 14:12 WG2358717 (S) Toluene-d8 93.9 80.0-120 09/09/2024 14:12 WG2358717 (S) 4-Bromofluorobenzene 94.3 77.0-126 09/09/2024 14:12 WG2358717 (S) 1,2-Dichloroethane-d4 95.9 70.0-130 09/09/2024 14:12 WG2358717 Semi-Volatile Organic Compounds (GC) by Method 3511/8015 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) High Fraction 0.125 0.100 1 09/10/2024 18:50 WG2358514 (S) o-Terphenyl 55.8 52.0-156 09/10/2024 18:50 WG2358514 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 13 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 13 of 28 SAMPLE RESULTS - 09 L1772744 MW11 Collected date/time: 08/28/24 11:30 Volatile Organic Compounds (GC) by Method 8015D/GRO Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) Low Fraction ND 0.100 1 09/07/2024 16:14 WG2357990 (S) a,a,a-Trifluorotoluene(FID)93.3 78.0-120 09/07/2024 16:14 WG2357990 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Benzene ND 0.00100 1 09/09/2024 14:30 WG2358717 Toluene ND 0.00100 1 09/09/2024 14:30 WG2358717 Ethylbenzene ND 0.00100 1 09/09/2024 14:30 WG2358717 Total Xylenes ND 0.00300 1 09/09/2024 14:30 WG2358717 Methyl tert-butyl ether ND 0.00100 1 09/09/2024 14:30 WG2358717 Naphthalene ND 0.00500 1 09/09/2024 14:30 WG2358717 (S) Toluene-d8 91.5 80.0-120 09/09/2024 14:30 WG2358717 (S) 4-Bromofluorobenzene 94.9 77.0-126 09/09/2024 14:30 WG2358717 (S) 1,2-Dichloroethane-d4 98.4 70.0-130 09/09/2024 14:30 WG2358717 Semi-Volatile Organic Compounds (GC) by Method 3511/8015 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) High Fraction ND 0.100 1 09/12/2024 00:20 WG2358544 (S) o-Terphenyl 90.5 52.0-156 09/12/2024 00:20 WG2358544 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 14 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 14 of 28 SAMPLE RESULTS - 10 L1772744 MW13 Collected date/time: 08/28/24 10:30 Volatile Organic Compounds (GC) by Method 8015D/GRO Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) Low Fraction 1.67 B 1.00 10 09/07/2024 20:36 WG2357990 (S) a,a,a-Trifluorotoluene(FID)94.2 78.0-120 09/07/2024 20:36 WG2357990 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Benzene 0.0403 0.0100 10 09/09/2024 16:43 WG2358717 Toluene ND 0.0100 10 09/09/2024 16:43 WG2358717 Ethylbenzene ND 0.0100 10 09/09/2024 16:43 WG2358717 Total Xylenes ND 0.0300 10 09/09/2024 16:43 WG2358717 Methyl tert-butyl ether 0.590 0.0100 10 09/09/2024 16:43 WG2358717 Naphthalene ND 0.0500 10 09/09/2024 16:43 WG2358717 (S) Toluene-d8 92.5 80.0-120 09/09/2024 16:43 WG2358717 (S) 4-Bromofluorobenzene 99.2 77.0-126 09/09/2024 16:43 WG2358717 (S) 1,2-Dichloroethane-d4 95.8 70.0-130 09/09/2024 16:43 WG2358717 Semi-Volatile Organic Compounds (GC) by Method 3511/8015 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) High Fraction 1.33 0.100 1 09/12/2024 00:40 WG2358544 (S) o-Terphenyl 109 52.0-156 09/12/2024 00:40 WG2358544 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 15 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 15 of 28 SAMPLE RESULTS - 11 L1772744 MW14 Collected date/time: 08/28/24 11:00 Volatile Organic Compounds (GC) by Method 8015D/GRO Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) Low Fraction 1.42 B 1.00 10 09/07/2024 20:59 WG2357990 (S) a,a,a-Trifluorotoluene(FID)93.8 78.0-120 09/07/2024 20:59 WG2357990 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time Benzene ND 0.0200 20 09/09/2024 17:02 WG2358717 Toluene ND 0.0200 20 09/09/2024 17:02 WG2358717 Ethylbenzene ND 0.0200 20 09/09/2024 17:02 WG2358717 Total Xylenes ND 0.0600 20 09/09/2024 17:02 WG2358717 Methyl tert-butyl ether 0.694 0.0200 20 09/09/2024 17:02 WG2358717 Naphthalene ND 0.100 20 09/09/2024 17:02 WG2358717 (S) Toluene-d8 93.6 80.0-120 09/09/2024 17:02 WG2358717 (S) 4-Bromofluorobenzene 94.8 77.0-126 09/09/2024 17:02 WG2358717 (S) 1,2-Dichloroethane-d4 91.4 70.0-130 09/09/2024 17:02 WG2358717 Semi-Volatile Organic Compounds (GC) by Method 3511/8015 Result Qualifier RDL Dilution Analysis Batch Analyte mg/l mg/l date / time TPH (GC/FID) High Fraction 0.848 0.100 1 09/10/2024 09:36 WG2358545 (S) o-Terphenyl 127 52.0-156 09/10/2024 09:36 WG2358545 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 16 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 16 of 28 QUALITY CONTROL SUMMARYWG2357830 Volatile Organic Compounds (GC) by Method 8015D/GRO L1772744-01,02,03,04,05,06,07,08 Method Blank (MB) (MB) R4117820-2 09/06/24 22:46 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l TPH (GC/FID) Low Fraction U 0.0314 0.100 (S) a,a,a-Trifluorotoluene(FID)100 78.0-120 Laboratory Control Sample (LCS) (LCS) R4117820-1 09/06/24 21:53 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/l mg/l %% TPH (GC/FID) Low Fraction 5.00 5.28 106 72.0-127 (S) a,a,a-Trifluorotoluene(FID) 103 78.0-120 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 17 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 17 of 28 QUALITY CONTROL SUMMARYWG2357990 Volatile Organic Compounds (GC) by Method 8015D/GRO L1772744-09,10,11 Method Blank (MB) (MB) R4118407-2 09/07/24 13:56 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l TPH (GC/FID) Low Fraction 0.0621 J 0.0314 0.100 (S) a,a,a-Trifluorotoluene(FID)92.9 78.0-120 Laboratory Control Sample (LCS) (LCS) R4118407-1 09/07/24 10:54 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/l mg/l %% TPH (GC/FID) Low Fraction 5.00 5.22 104 72.0-127 (S) a,a,a-Trifluorotoluene(FID) 104 78.0-120 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 18 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 18 of 28 QUALITY CONTROL SUMMARYWG2355536 Volatile Organic Compounds (GC/MS) by Method 8260B L1772744-01,02,03,04,05,06,07 Method Blank (MB) (MB) R4117160-3 09/03/24 19:23 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Benzene U 0.0000941 0.00100 Toluene U 0.000278 0.00100 Ethylbenzene U 0.000137 0.00100 Total Xylenes U 0.000174 0.00300 Methyl tert-butyl ether U 0.000101 0.00100 Naphthalene U 0.00100 0.00500 (S) Toluene-d8 104 80.0-120 (S) 4-Bromofluorobenzene 96.8 77.0-126 (S) 1,2-Dichloroethane-d4 103 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R4117160-1 09/03/24 18:22 • (LCSD) R4117160-2 09/03/24 18:42 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% Benzene 0.00500 0.00503 0.00503 101 101 70.0-123 0.000 20 Toluene 0.00500 0.00528 0.00515 106 103 79.0-120 2.49 20 Ethylbenzene 0.00500 0.00538 0.00536 108 107 79.0-123 0.372 20 Total Xylenes 0.0150 0.0163 0.0159 109 106 79.0-123 2.48 20 Methyl tert-butyl ether 0.00500 0.00498 0.00491 99.6 98.2 68.0-125 1.42 20 Naphthalene 0.00500 0.00387 0.00393 77.4 78.6 54.0-135 1.54 20 (S) Toluene-d8 105 105 80.0-120 (S) 4-Bromofluorobenzene 97.7 97.0 77.0-126 (S) 1,2-Dichloroethane-d4 105 105 70.0-130 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 19 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 19 of 28 QUALITY CONTROL SUMMARYWG2358717 Volatile Organic Compounds (GC/MS) by Method 8260B L1772744-08,09,10,11 Method Blank (MB) (MB) R4118240-2 09/09/24 13:29 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l Benzene U 0.0000941 0.00100 Toluene U 0.000278 0.00100 Ethylbenzene U 0.000137 0.00100 Total Xylenes U 0.000174 0.00300 Methyl tert-butyl ether U 0.000101 0.00100 Naphthalene U 0.00100 0.00500 (S) Toluene-d8 92.4 80.0-120 (S) 4-Bromofluorobenzene 98.6 77.0-126 (S) 1,2-Dichloroethane-d4 97.6 70.0-130 Laboratory Control Sample (LCS) (LCS) R4118240-1 09/09/24 12:51 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/l mg/l %% Benzene 0.00500 0.00560 112 70.0-123 Toluene 0.00500 0.00507 101 79.0-120 Ethylbenzene 0.00500 0.00464 92.8 79.0-123 Total Xylenes 0.0150 0.0141 94.0 79.0-123 Methyl tert-butyl ether 0.00500 0.00539 108 68.0-125 Naphthalene 0.00500 0.00462 92.4 54.0-135 (S) Toluene-d8 90.7 80.0-120 (S) 4-Bromofluorobenzene 98.9 77.0-126 (S) 1,2-Dichloroethane-d4 100 70.0-130 L1773226-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1773226-01 09/09/24 17:21 • (MS) R4118240-3 09/09/24 22:46 • (MSD) R4118240-4 09/09/24 23:05 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% Benzene 1.00 1.98 3.07 3.13 109 115 200 17.0-158 1.94 27 Toluene 1.00 8.67 9.40 9.31 73.0 64.0 200 26.0-154 0.962 28 Ethylbenzene 1.00 1.97 2.96 2.91 99.0 94.0 200 30.0-155 1.70 27 Total Xylenes 3.00 11.8 14.6 14.4 93.3 86.7 200 29.0-154 1.38 28 Methyl tert-butyl ether 1.00 ND 1.15 1.18 107 110 200 28.0-150 2.58 29 Naphthalene 1.00 ND 1.96 1.96 105 105 200 12.0-156 0.000 35 (S) Toluene-d8 92.3 91.6 80.0-120 (S) 4-Bromofluorobenzene 97.5 96.6 77.0-126 (S) 1,2-Dichloroethane-d4 95.1 96.1 70.0-130 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 20 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 20 of 28 QUALITY CONTROL SUMMARYWG2357908 Semi-Volatile Organic Compounds (GC) by Method 3511/8015 L1772744-01,02,03,04 Method Blank (MB) (MB) R4117693-1 09/10/24 06:16 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l TPH (GC/FID) High Fraction U 0.0247 0.100 (S) o-Terphenyl 83.0 52.0-156 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R4117693-2 09/10/24 06:36 • (LCSD) R4117693-3 09/10/24 06:56 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% TPH (GC/FID) High Fraction 1.50 1.12 1.13 74.7 75.3 50.0-150 0.889 20 (S) o-Terphenyl 77.0 76.0 52.0-156 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 21 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 21 of 28 QUALITY CONTROL SUMMARYWG2358514 Semi-Volatile Organic Compounds (GC) by Method 3511/8015 L1772744-05,06,07,08 Method Blank (MB) (MB) R4117638-1 09/09/24 20:07 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l TPH (GC/FID) High Fraction U 0.0247 0.100 (S) o-Terphenyl 76.0 52.0-156 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R4117638-2 09/09/24 20:27 • (LCSD) R4117638-3 09/09/24 20:48 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% TPH (GC/FID) High Fraction 1.50 1.11 1.08 74.0 72.0 50.0-150 2.74 20 (S) o-Terphenyl 85.0 84.0 52.0-156 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 22 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 22 of 28 QUALITY CONTROL SUMMARYWG2358544 Semi-Volatile Organic Compounds (GC) by Method 3511/8015 L1772744-09,10 Method Blank (MB) (MB) R4118814-1 09/11/24 23:19 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l TPH (GC/FID) High Fraction U 0.0247 0.100 (S) o-Terphenyl 81.5 52.0-156 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R4118814-2 09/11/24 23:39 • (LCSD) R4118814-3 09/12/24 00:00 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l %%%%% TPH (GC/FID) High Fraction 1.50 1.61 1.64 107 109 50.0-150 1.85 20 (S) o-Terphenyl 111 112 52.0-156 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 23 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 23 of 28 QUALITY CONTROL SUMMARYWG2358545 Semi-Volatile Organic Compounds (GC) by Method 3511/8015 L1772744-11 Method Blank (MB) (MB) R4118054-1 09/10/24 08:55 MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mg/l mg/l TPH (GC/FID) High Fraction U 0.0247 0.100 (S) o-Terphenyl 126 52.0-156 Laboratory Control Sample (LCS) (LCS) R4118054-2 09/10/24 09:16 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/l mg/l %% TPH (GC/FID) High Fraction 1.50 1.56 104 50.0-150 (S) o-Terphenyl 142 52.0-156 L1774813-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1774813-06 09/10/24 14:01 • (MS) R4118054-3 09/10/24 14:21 • (MSD) R4118054-4 09/10/24 14:42 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mg/l mg/l mg/l %%%%% TPH (GC/FID) High Fraction 1.43 0.353 1.93 1.88 110 107 1 50.0-150 2.62 20 (S) o-Terphenyl 107 109 52.0-156 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 24 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 24 of 28 GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit. Rec.Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. (S) Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. Dilution If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. Limits These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. Qualifier This column provides a letter and/or number designation that corresponds to additional information concerning the result reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. Result The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL” (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry)Confidence level of 2 sigma. Case Narrative (Cn) A brief discussion about the included sample results, including a discussion of any non-conformances to protocol observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control Summary (Qc) This section of the report includes the results of the laboratory quality control analyses required by procedure or analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. Sample Chain of Custody (Sc) This is the document created in the field when your samples were initially collected. This is used to verify the time and date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. Sample Results (Sr) This section of your report will provide the results of all testing performed on your samples. These results are provided by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description B The same analyte is found in the associated blank. J The identification of the analyte is acceptable; the reported value is an estimate. 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 25 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 25 of 28 Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122 Alabama 40660 Nebraska NE-OS-15-05 Alaska 17-026 Nevada TN000032021-1 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey–NELAP TN002 California 2932 New Mexico ¹TN00003 Colorado TN00003 New York 11742 Connecticut PH-0197 North Carolina Env375 Florida E87487 North Carolina ¹DW21704 Georgia NELAP North Carolina ³41 Georgia ¹923 North Dakota R-140 Idaho TN00003 Ohio–VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LAO00356 Kentucky ¹ ⁶KY90010 South Carolina 84004002 Kentucky ²16 South Dakota n/a Louisiana AI30792 Tennessee ¹ ⁴2006 Louisiana LA018 Texas T104704245-20-18 Maine TN00003 Texas ⁵LAB0152 Maryland 324 Utah TN000032021-11 Massachusetts M-TN003 Vermont VT2006 Michigan 9958 Virginia 110033 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 998093910 Montana CERT0086 Wyoming A2LA A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2LA – ISO 17025 ⁵1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA–Crypto TN00003 ACCREDITATIONS & LOCATIONS ¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable * Not all certifications held by the laboratory are applicable to the results reported in the attached report. * Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical. 1 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 Gl 8 Al 9 Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 10:39 26 of 28 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Johnston, Leigh, Inc.L1772744 09/12/24 13:08 26 of 28