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Home My WebLink AboutDAQ-2024-0112671 DAQC-1093-24 Site ID 15938 (B4) MEMORANDUM TO: STACK TEST FILE – UINTA WAX OPERATING, LLC – North Randlett Compressor Station – Uintah County THROUGH: Rik Ombach, Minor Source Oil and Gas Compliance Section Manager FROM: Kyle Greenberg, Environmental Scientist DATE: October 24, 2024 SUBJECT: Source: Compressor Engine: Unit #3 Caterpillar G3516J; SN: N6W/JEF02569 Contact: Karen Pratt: 720-990-9927 Location: Remote location in Uintah County, UT Test Contractor: Oasis Emissions Consultants, Inc. Permit/AO#: DAQE-AN159380002-23, dated December 11, 2023 Action Code: TR Subject: Review of Stack Test Reports dated July 26, 2024 On August 15, 2024, DAQ received a test report for the above listed unit. Testing was performed on July 25, 2024, to demonstrate compliance with the emission limits found in Condition II.B.2 of Approval Order DAQE-AN159380002-23 and 40 CFR Part 60 Subpart JJJJ. The DAQ calculated test results are: Source Test Date Test Method Pollutant Tester Results DAQ Results Limits Unit ID: #3 SN: N6W/JEF025 69 July 25, 2024 320 NOx 0.41 g/bhp-hr 0.92 lb/hr 34.18 ppmvd @15% O2 0.404 g/bhp-hr 0.923 lb/hr 34.180 ppmvd @15% O2 1.0 g/bhp-hr 1.52 lb/hr 41 ppmvd @15% O2 320 CO 0.04 g/bhp-hr 0.08 lb/hr 5.17 ppmvd @15% O2 0.037 g/bhp-hr 0.085 lb/hr 5.167 ppmvd @15% O2 2.0 g/bhp-hr 1.37 lb/hr 61 ppmvd @15% O2 320 VOC 0.36 g/bhp-hr 0.82 lb/hr 31.52 ppmvd @15% O2 0.357 g/bhp-hr 0.815 lb/hr 31.517 ppmvd @15% O2 0.7 g/bhp-hr 2.13 lb/hr 60 ppmvd @15% O2 DEVIATIONS: None. CONCLUSION: The stack test report appears to be acceptable. RECOMMENDATION: The emissions from Unit #3 should be considered to have been in compliance with the emission limits of the AO and 40 CFR Part 60 subpart JJJJ during the time of testing on July 25, 2024. On June 20, 2024, Uinta Wax conducted a stack test on Unit #3; these test results showed that the NOx ppm @ 15% O2 AO limits were exceeded. 2 No recommended enforcement action for this exceedance - the current ppm @ 15% O2 limits are under an engineer review to reflect the limits of 40 CFR Part 60 Subpart JJJJ and the NOx ppm @ 15% O2 results were in compliance with Subpart JJJJ emission limits on June 20, 2024. See attached June 20, 2024, test report and Uinta Wax’s response to that test report. HPV: Not Applicable ATTACHMENTS: DAQ Stack Test Review Excel Spreadsheets; Uinta Wax Operating, LLC’s Stack Test Reports for July 25, 2024, and June 20, 2024; Uinta Wax Operating, LLC’s Response to June 20, 2024, Test Report Emissions CH4-Finley Operating, LLC North Randlett Compressor Station Uintah County, Utah Compressor Engine E1 SN: N6W/JEF02569 Test Date: 7/25/2024 Run # 1 2 3 Average Start Time 9:20 10:21 11:22 Stop Time 10:19 11:20 12:21 Sample Duration (minutes) 60 60 60 BHP Engine Load - Actual (bhp) 1035 1035 1035 1035 DS Stack Diameter (inches) 13.5 13.5 13.5 13.5 PAVG Average (Delta P)½ (" H2O)½0.9220 0.9220 0.9210 0.9217 CP Pitot Tube Constant (unitless) 0.84 0.84 0.84 0.84 TS Stack Temperature (°F) 621 623 626 624 Pbar Barometric Pressure (" Hg) 25.27 25.27 25.26 25.27 Ps Stack Pressure ('' H2O)0.33 0.32 0.34 0.33 O2%vd O2 (%vd)8.3 8.3 8.2 8.3 CO2%vd CO2 (%vd)7.3 7.3 7.3 7.3 N2%vd N2 (%vd)84.4 84.4 84.5 84.4 dry NOX (ppmvd)72.9 72.4 74.3 73.2 dry CO (ppmvd) 11.2 11.1 10.9 11.1 wet NMNEOC (ppmvd as C3H8)66.4 68.1 68.0 67.5 Run # 1 2 3 Average Bws Measured Moisture Content (%/100) 0.120 0.126 0.121 0.122 Bws Saturated Moisture Content (%/100) 143.009 145.001 148.070 145.360 Bws Actual Moisture Content (%/100) 0.120 0.126 0.121 0.122 MD Molecular Weight Dry (lb/lb-mole) 29.50 29.50 29.50 29.50 MA Molecular Weight Wet (lb/lb-mole) 28.12 28.05 28.10 28.09 VS Gas Velocity (ft/sec) 81.6 81.8 81.8 81.7 FACFM Gas Flow (acfm) 4869 4879 4877 4875 FDSCFM Gas Flow (dscfm) 1768 1756 1759 1761 FWSCFM Gas Flow (wscfm) 2010 2010 2003 2008 FKWSCFH Gas Flow (kwscfh) 121 121 120 120 FKWSCFM Gas Flow (kwscfm) 2222 lb/hr Gas Flow (lb/hr) 8801 8782 8767 8783 Fo Fo (unitless)1.726 1.726 1.740 1.731 wet O2 (%vw)7.3 7.3 7.2 7.3 wet CO2 (%vw)6.4 6.4 6.4 6.4 wet NOX (ppmvw)64.150 63.250 65.298 64.233 15 NOX (ppmvd @ 15% O2)34.131 33.883 34.527 34.180 41.0 lb/hr NOX (lb/hr)0.922 0.910 0.936 0.923 1.52 g/bhp-hr NOX (g/bhp-hr)0.404 0.399 0.410 0.404 1.0 wet CO (ppmvw) 9.831 9.694 9.603 9.709 15 CO (ppmvd @ 15% O2)5.230 5.193 5.078 5.167 61.0 lb/hr CO (lb/hr) 0.086 0.085 0.084 0.085 1.37 g/bhp-hr CO (g/bhp-hr) 0.038 0.037 0.037 0.037 2.0 dry NMEOC (ppmvd as C3H8)66.430 68.060 67.970 67.487 15 NMEOC (ppmvd as C3H8 @ 15% O2)31.106 31.869 31.577 31.517 60 lb/hr NMEOC (lb/hr as C3H8)0.805 0.820 0.820 0.815 2.13 g/bhp-hr NMEOC (g/bhp-hr as C3H8)0.353 0.359 0.359 0.357 0.7 Permit Limits Field Reference Method Data Reference Method Calculations Page 1 of 1 Source Test Report For Uinta Wax Operating, LLC North Randlett Compressor Station Uintah County, Utah Test Date: July 25, 2024 Report Date: July 26, 2024 UDEQ Permit: #DAQE-AN159380002-23 Engine: Caterpillar G3516J SN: N6W/JEF02569 Unit ID: #3 Prepared By: Oasis Emission Consultants, Inc. 2730 Commercial Way Rock Springs, WY 82901 July 26, 2024 Ms. Karen Pratt Uinta Wax Operating, LLC Dear Ms. Pratt: Re: Engine Emission Testing For Uinta Wax Operating, LLC, North Randlett Compressor Station, Unit #3, Permit #DAQE-AN159380002-23. An air emissions test program was conducted on a Caterpillar G3516J engine, operated by Uinta Wax Operating, LLC and designated as Unit #3, located at the North Randlett Compressor Station in Uintah County, Utah. The purpose of the testing was to demonstrate annual compliance with the emissions limits contained in UDEQ Permit #DAQE- AN159380002-23 and EPA 40 CFR 60, Subpart JJJJ, for oxides of nitrogen (NOx), carbon monoxide (CO) and volatile organic compounds (VOC). Oasis Emission Consultants, Inc. conducted the testing on July 25, 2024. UDEQ Permit #DAQE-AN159380002-23 Emission Levels The average recorded levels were found to comply with emission levels stipulated in the permit, as shown in the attached report and summarized below. Emission Unit Avg NOx Permit NOx Avg CO Permit CO Avg NMNEHC* Permit VOC ppm @ 15% O2 34.18 41 5.17 61 31.52 60 lbs/hr 0.92 1.52 0.08 1.37 0.82 2.13 *VOC levels reported as non-methane, non-ethane hydrocarbon on a propane basis (NMNEHC C3). EPA 40 CFR 60, Subpart JJJJ Emission Levels Emission Unit Avg NOx Permit NOx Avg CO Permit CO Avg NMNEHC* Permit VOC g/bhp-hr 0.41 1.0 0.04 2.0 0.36 0.7 Catalyst Parameters (Averaged Over 3 Test Runs) Inlet Temp (deg F) DP (in H2O) 733 N/A Engine Load (Averaged Over 3 Test Runs) Rated BHP Operating BHP % Load 1380 1035.0 75.0 Testing Protocol The attached report was generated using an extractive FTIR system using methodologies as required by and in accordance with EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320, as outlined in the submitted Source Test Protocol. Quality Assurance Oasis has performed a full review of the raw data and calculated results in this report. Any errors we have encountered have been listed in the body of this report. After performing the review, we are confident that this engine has met all requirements. If you have any questions or require further information, please contact the undersigned at (307) 382-3297. Yours truly, Oasis Emission Consultants, Inc. _________________________ _______________________ Charles A. Chapman Crystal Leonard Manager of Technical Services Senior EHS Specialist _________________________ Christopher N. Knott, P.Eng. Director, Engineering and Operations SOURCE EMISSION TEST REPORT UDEQ Permit #DAQE-AN159380002-23 Test Performed By: Oasis Emission Consultants, Inc. Test Company Contact: Chris Knott 2730 Commercial Way Rock Springs, WY 82901 307.382.3297 Owner/Operator: Uinta Wax Operating, LLC Owner/Operator Contact: Karen Pratt (720) 990-9927 Facility Name: North Randlett Compressor Station UTM Coordinates: 593,702 m Easting, 4,453,005 m Northing UTM Zone 12 Uintah County, Utah Emission Source: Caterpillar G3516J Unit #3 Date of Test: July 25, 2024 Date of Report: July 26, 2024 TABLE OF CONTENTS 1.1 Introduction .......................................................................................................................... 1 2.1 Stack Sampling Location ..................................................................................................... 2 3.1 Discussion of NOx, CO and VOC Test Results ................................................................... 3 3.1.1 Source Test 1 ............................................................................................................................................ 3 3.1.2 Source Test 2 ............................................................................................................................................ 3 3.1.3 Source Test 3 ............................................................................................................................................ 3 4.1 Stack Sampling Methods and Procedures ............................................................................ 4 4.2 Equipment Utilization .......................................................................................................... 5 4.3 Measurement of VOC (NMNEHC C3) ............................................................................... 6 4.4 Process Parameters............................................................................................................... 6 5.1 Quality Assurance ................................................................................................................ 7 List of Tables and Figures Figure 1 - Sample Port Location ............................................................................................................................. 2 Figure 2 - Sampling Train Schematic-Method 320 ................................................................................................ 5 Table 1 - Insertion Depths of Traverse Points for Stratification Test ..................................................................... 2 Table 2 - Test Matrix .............................................................................................................................................. 4 Table 3 - Concentrations and Interference .............................................................................................................. 5 APPENDIX A: NOx, CO and VOC Test Data APPENDIX B: Quality Assurance/Calibration Data APPENDIX C: Load Approximation APPENDIX D: Example Calculations and Summary APPENDIX E: Field Notes 1 1.1 Introduction An air emissions test program was conducted on a Caterpillar G3516J engine, operated by Uinta Wax Operating, LLC and designated as Unit #3, located at the North Randlett Compressor Station in Uintah County, Utah. The purpose of the testing was to demonstrate annual compliance with the emissions limits contained in UDEQ Permit #DAQE- AN159380002-23 and EPA 40 CFR 60, Subpart JJJJ, for oxides of nitrogen (NOx), carbon monoxide (CO) and volatile organic compounds (VOC) defined as non-methane, non-ethane hydrocarbons, reported as propane (NMNEHC C3). The facility is located five (5) miles west of Randlett, in Uintah County, Utah. Three one hour test runs were performed on July 25, 2024 to analyze NOx, CO and VOC emission levels. Test runs were performed according to methodologies outlined by EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320 as outlined in the submitted Source Test Protocol dated May 17, 2024. Each one hour test run consisted of 60 readings taken at one minute intervals. Process parameters were recorded during each test run in order to determine the load. Parameters include the engine panel load percent reading. The following key personnel were present during testing: TJ Schmidtberger, OEC 2 2.1 Stack Sampling Location The facility is located five (5) miles west of Randlett, in Uintah County, Utah. Testing was conducted on the Caterpillar G3516J engine. The sampling port for moisture, NOx, CO and VOC measurements was approximately 2.5 pipe diameters (34”) downstream from the nearest flow disturbance (Distance B) and 0.6 pipe diameters (7.5”) upstream from the nearest disturbance (Distance A), as seen in Figure 1. The stack sampling location was placed at approximately 50% insertion depth based on an O2 stratification check which demonstrated a non-stratified flow regime. The stratification was conducted according to EPA 40 CFR 75(A), §6.5.6.1 using 3 traverse points determined according to Table 1 below. Figure 1 - Sample Port Location Table 1 - Insertion Depths of Traverse Points for Stratification Test Traverse Point Insertion Depth (Percent of Stack Diameter) 1 16.6 2 50.0 3 83.3 13.5" A B Oxidation Catalyst 3 3.1 Discussion of NOx, CO and VOC Test Results Three, one hour test runs were performed on July 25, 2024 to analyze exhaust NOx, CO and VOC (NMNEHC C3) emission levels to demonstrate annual compliance with the emissions limits contained in the WDEQ Permit #DAQE-AN159380002-23 and EPA 40 CFR 60, Subpart JJJJ. Testing for NOx, CO and VOC were run concurrently with one another. Each test was performed at the maximum achievable load. Measured emissions were below permitted limits. Please refer to the Appendices for a listing of all raw data, calibration error response and calculations performed per EPA 40 CFR 60(A) requirements. 3.1.1 Source Test 1: Caterpillar G3516J, NOx, CO and VOC The first test was performed from 9:20 to 10:19 for NOx, CO and VOC. Based on operating parameters recorded during testing, the load was approximated at 1035.0 bhp, and the average NOx and CO levels were found to be 0.40 g/bhp-hr and 0.04 g/bhp-hr respectively, below limitations. The VOC level tested at 0.35 g/bhp- hr, which tested in compliance. 3.1.2 Source Test 2: Caterpillar G3516J, NOx, CO and VOC The second test was performed from 10:21 to 11:20 for NOx, CO and VOC. Based on operating parameters recorded during testing, the load was approximated at 1035.0 bhp, and the average NOx and CO levels were found to be 0.40 g/bhp-hr and 0.04 g/bhp-hr respectively, below limitations. The VOC level tested at 0.36 g/bhp- hr, which tested in compliance. 3.1.3 Source Test 3: Caterpillar G3516J, NOx, CO and VOC The third test was performed from 11:22 to 12:21 for NOx, CO and VOC. Based on operating parameters recorded during testing, the load was approximated at 1035.0 bhp, and the average NOx and CO levels were found to be 0.41 g/bhp-hr and 0.04 g/bhp-hr respectively, below limitations. The VOC level tested at 0.36 g/bhp- hr, which tested in compliance. Test Run NOx (ppmvd) NOx (g/bhp-hr) CO (ppmvd) CO (g/bhp-hr) VOC (ppmvd) VOC (g/bhp-hr) O2 (%) 1 72.89 0.40 11.17 0.04 66.43 0.35 8.3 Test Run NOx (ppmvd) NOx (g/bhp-hr) CO (ppmvd) CO (g/bhp-hr) VOC (ppmvd) VOC (g/bhp-hr) O2 (%) 2 72.36 0.40 11.09 0.04 68.06 0.36 8.3 Test Run NOx (ppmvd) NOx (g/bhp-hr) CO (ppmvd) CO (g/bhp-hr) VOC (ppmvd) VOC (g/bhp-hr) O2 (%) 3 74.32 0.41 10.93 0.04 67.97 0.36 8.2 4 4.1 Stack Sampling Methods and Procedures Testing followed EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320, with no exceptions. Table 2 - Test Matrix Method Title Parameter Reference EPA 40 CFR 60 Appendix A, Method 1 Sample and Velocity Traverses for Stationary Sources Sampling Point Determination https://www.epa.gov/ sites/production/files/ 2017- 08/documents/metho d_1_3.pdf EPA 40 CFR 60 Appendix A, Method 2 Determination of Stack Gas Velocity and Volumetric Flow Rate Exhaust Effluent Flow https://www.epa.gov/ sites/production/files/ 2017- 08/documents/metho d_2.pdf EPA 40 CFR 60 Appendix A, Method 3 Gas Analysis for the Determination of Dry Molecular Weight O2, CO2, Dry Volumetric Flow Rate https://www.epa.gov/ sites/production/files/ 2017- 08/documents/metho d_3.pdf EPA 40 CFR 63 Appendix A, EPA Method 320 Vapor Phase Organic and Inorganic Emissions by Extractive FTIR Nitrogen Oxides, Carbon Monoxide, Non- Methane Non- Ethane Hydrocarbons on a Propane Basis https://www.epa.gov/ emc/method-320- vapor-phase-organic- and-inorganic- emissions-extractive- ftir United States. U.S. Environmental Protection Agency. “EMC Promulgated Test Methods.” Air Emission Measurement Center (EMC). 31 August 2023. Web. 26 July 2024. <https://www.epa.gov/emc/emc-promulgated-test-methods>. ASTM International. “Standards & Publications.” All Environment Standards. Web. 26 July 2024. <https://www.astm.org/Standards/D6348.htm>. 5 4.2 Equipment Utilization The following equipment was used during the tests performed at this facility in conjunction with procedures outlined by EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320. • (1) MKS MultiGas 2030 FTIR Continuous Gas Analyzer (0.210 L/min sample flow, 0.014 atmosphere sample pressure, 1 atmosphere cell pressure, 191°C cell temperature) • (1) Laptop Computer for the FTIR Analyzer using MKS MG2000 Software • (1) 75ft or 100ft Heated Teflon Line w/ Heated Sample Probe and Spike Bypass Line • S-Type Pitot Tube c/w 20 ft. Heated Sample Line (coefficient 0.84) • (1) Enerac 500 Portable O2/CO2 Analyzer • (1) Fyrite O2/CO2 Analyzer • (5) EPA Protocol G1 Calibration Gas (NOx, CO, C3H8, C2H4 and NO2) The MKS Multigas 2030 FTIR Analyzer operated with a spectral resolution of 0.5 cm-1 and a scan time of 30 seconds. The FTIR spectrometer utilizes a multi-pass gas cell with a 5.11 meter effective pathlength. Figure 2 - Sampling Train Schematic-Method 320 Table 3 - Concentrations and Interference 6 The MKS 2030 software provides a Natural Gas Method that is designed to minimize all expected interferences by removing the regions in the quant region where they are most absorbed (i.e. picket fence approach). So, for example, all the water peaks that are greater than about 0.1 abs are removed from the quant region. Since the spectral noise measured (sample spectrum) is in the range of 0.001 absorbance, it is desirable to have any error within this range. The MKS software will match the water calibration spectrum to the sample spectrum at any 1 point in the spectrum to about 1% precision. So, 1% of 0.1 absorbance is 0.001 abs. This is why any peaks greater than this for interfering compounds are usually excluded so they do not interfere. To summarize, the MKS software and the method are designed to minimize any interferences by removing their largest interfering absorptions. 4.3 Measurement of VOC (NMNEHC C3) The algorithm currently used for NMNEHC C3 and developed for natural gas fired applications by Dr. Spartz and MKS instruments in accordance with EPA standards, is the following: (2.4*c8/(1+exp((2-c8)/0.2))+1.9*c11/(1+exp((2-c11)/0.2))+6*c12/(1+exp((0.5-c12) /0.2))+2.85*c13/(1+exp((2-c13)/0.2))+3*c14/(1+exp((1-c14)/0.2)))/3 c8= acetylene c11= ethylene c12= hexane c13= propylene c14= propane Note: The constants in front of each of the compounds listed represents the FID response factor when calibrated with Propane. As with any CEMS analyzer, the FTIR may demonstrate a negative zero bias. The “exp” functions listed in the algorithm above are intended to mathematically filter out any negative biases and set them to approach zero. 4.4 Process Parameters Process parameters were recorded during each test run in order to determine the load. Parameters include the engine panel load percent reading. Results are provided in Appendix C. 7 5.1 Quality Assurance The MKS Multigas 2030 FTIR Analyzer was used to measure NOx, CO and VOC on a dry basis. A pre Direct and System calibration measurement was made on compounds of NOx, CO, C3H8 and C2H4. In addition, post System calibrations were made on compounds of NOx, CO, C3H8 and C2H4. Compounds of CO2 and C3H8 were measured for the quality assurance spiking requirements. Levels for calibrations and zeroes must be within +/- 5% of the certified calibration gas or response to zero gas, respectively. CTS procedures were followed according to EPA requirements for both pre and post testing. Similarly, QA spiking procedures were followed. Analysis of the CO2 exhaust effluent was used to determine the dilution factor. Steady levels of the CO2 were observed and a sufficient duration of time was allowed to elapse for a representative average. The calibration gas was spiked into the effluent stream using a bypass line at approximately 10% of the sampling rate. The dilution factor was obtained from observation of the stack CO2 behavior using the following equation: CO2AVG – CO2SPIKE DF = ------------------------ CO2 AVG Where: CO2AVG = The average undiluted CO2 stack gas concentration of spike measurements CO2SPIKE = The average diluted CO2 stack gas concentration when spiked The sample recovery was then obtained from the following equation: % REC = (Spike MEAS – Stack MEAS)* (1 – DF) --------------------------------------------------------- CS * DF Where: Spike MEAS = The average diluted stack gas concentration when spiked Stack MEAS = The average undiluted stack gas concentration DF = Dilution factor CS = Certified concentration of calibration standards The Sample Recovery average level for C3H8 was found to be 72.3%, which was within the allowable tolerance of Method 320 (70% to 130%). A summary of all spiking procedures/results can be found in Appendix B. APPENDIX A NO Dry (ppm) NO2 Dry (ppm) NOx Dry (ppm) CO Dry (ppm) NMNEHC C3 Dry (ppm) H2O% (High) 191C Time 1 59.397453 13.58417 72.981623 11.372611 66.015957 9.802151 9:20:09 07/25/2024 2 59.895811 13.977793 73.873604 11.367461 66.011398 10.15439 9:21:09 07/25/2024 3 59.790369 13.875888 73.666257 11.35345 66.426444 10.70357 9:22:09 07/25/2024 4 59.363701 13.724757 73.088458 11.250843 66.579572 11.371182 9:23:09 07/25/2024 5 58.844572 13.609996 72.454568 11.252568 66.274161 11.561841 9:24:09 07/25/2024 6 59.410852 13.755733 73.166585 11.300633 66.614299 12.064459 9:25:09 07/25/2024 7 59.425062 14.035214 73.460276 11.226981 66.528758 12.096047 9:26:10 07/25/2024 8 59.076235 14.210439 73.286674 11.306945 65.788544 12.130042 9:27:10 07/25/2024 9 58.583127 14.259911 72.843038 11.205928 66.382331 12.062909 9:28:10 07/25/2024 10 58.209043 14.145754 72.354797 11.222419 66.379953 12.06748 9:29:10 07/25/2024 11 59.185682 14.468278 73.65396 11.272719 66.101693 12.039816 9:30:10 07/25/2024 12 58.643023 14.55186 73.194883 11.17628 66.279436 12.053993 9:31:10 07/25/2024 13 59.657059 14.910972 74.568031 11.182086 65.705691 12.292298 9:32:10 07/25/2024 14 59.132825 14.728901 73.861726 11.165547 66.269349 12.465166 9:33:10 07/25/2024 15 59.057079 14.735345 73.792424 11.148839 65.971474 12.488406 9:34:10 07/25/2024 16 59.544015 14.947552 74.491567 11.225075 65.121282 12.301866 9:35:11 07/25/2024 17 58.819888 14.904281 73.724169 11.184294 65.721075 12.357452 9:36:11 07/25/2024 18 59.286042 15.047419 74.333461 11.22292 65.466024 12.31232 9:37:10 07/25/2024 19 59.304713 15.129621 74.434334 11.227443 65.366355 12.316383 9:38:11 07/25/2024 20 59.95503 15.265598 75.220628 11.221956 64.862687 12.404196 9:39:11 07/25/2024 21 59.637776 15.100282 74.738058 11.199936 65.917351 12.502278 9:40:11 07/25/2024 22 59.665634 15.143893 74.809527 11.086939 65.831087 12.522033 9:41:11 07/25/2024 23 59.587805 15.233346 74.821151 11.13443 66.030929 12.523943 9:42:11 07/25/2024 24 60.160871 15.373036 75.533907 11.163244 65.063093 12.306627 9:43:11 07/25/2024 25 59.113497 15.083286 74.196783 11.082092 65.730316 12.195938 9:44:11 07/25/2024 26 59.338685 15.163468 74.502153 11.138156 65.718088 11.940112 9:45:11 07/25/2024 27 58.730875 14.782872 73.513747 11.035751 65.929369 11.783404 9:46:11 07/25/2024 28 59.209509 14.975201 74.18471 11.187471 65.658477 11.926643 9:47:13 07/25/2024 29 58.34853 14.950803 73.299333 11.173964 66.370422 11.98264 9:48:12 07/25/2024 30 58.164795 14.775478 72.940273 11.098225 66.381235 11.81882 9:49:12 07/25/2024 31 58.231334 14.746923 72.978257 11.070971 66.409096 12.428975 9:50:13 07/25/2024 32 57.482793 14.57442 72.057213 11.076496 66.164014 12.529787 9:51:13 07/25/2024 33 57.53887 14.534253 72.073123 11.102527 66.262932 12.364727 9:52:13 07/25/2024 34 58.263194 14.826846 73.09004 11.169436 66.487074 12.194632 9:53:13 07/25/2024 35 58.116334 14.780092 72.896426 11.137266 66.159295 12.285946 9:54:13 07/25/2024 36 57.819236 14.828222 72.647458 11.108317 65.810515 12.28377 9:55:13 07/25/2024 37 57.026609 14.630312 71.656921 11.183611 65.936592 12.199654 9:56:13 07/25/2024 38 57.130799 14.531036 71.661835 11.093672 65.746843 11.926706 9:57:13 07/25/2024 39 57.234957 14.654163 71.88912 11.149593 66.090344 11.545416 9:58:13 07/25/2024 40 56.186379 14.462734 70.649113 11.134376 66.423105 11.633721 9:59:13 07/25/2024 41 56.639784 14.600359 71.240143 11.052584 66.255438 11.696955 10:00:13 07/25/2024 42 57.126724 14.938455 72.065179 11.141123 66.474881 11.781575 10:01:14 07/25/2024 43 56.630201 14.73836 71.368561 11.040144 66.108785 11.738762 10:02:14 07/25/2024 44 57.512854 15.008636 72.52149 11.192636 66.310910 11.773701 10:03:14 07/25/2024 45 57.01082 14.780956 71.791776 11.109248 66.628788 11.98652 10:04:14 07/25/2024 46 56.325269 14.631953 70.957222 11.066031 67.072043 12.174352 10:05:14 07/25/2024 47 56.920632 14.812525 71.733157 11.124776 66.614064 12.205136 10:06:14 07/25/2024 48 56.16962 14.561937 70.731557 11.053502 67.454056 12.30573 10:07:14 07/25/2024 49 56.614502 14.682398 71.2969 11.164604 67.799525 12.307329 10:08:14 07/25/2024 50 56.447879 14.727784 71.175663 11.032523 67.564897 12.24578 10:09:14 07/25/2024 51 57.010833 14.853956 71.864789 11.076845 67.373565 12.177891 10:10:14 07/25/2024 52 57.044235 14.945137 71.989372 11.186379 67.340711 12.139631 10:11:14 07/25/2024 53 57.427881 15.047313 72.475194 11.18591 67.384204 11.880116 10:12:15 07/25/2024 54 57.171297 14.865729 72.037026 11.14912 67.815509 11.724534 10:13:15 07/25/2024 55 56.968752 14.878831 71.847583 11.127122 67.526375 11.606431 10:14:15 07/25/2024 56 57.91903 15.213732 73.132762 11.137798 67.542924 11.638009 10:15:15 07/25/2024 57 57.394766 15.170412 72.565178 11.15849 67.594852 11.792757 10:16:15 07/25/2024 58 56.812346 14.961111 71.773457 11.187273 68.631823 12.011275 10:17:15 07/25/2024 59 57.204004 14.917845 72.121849 11.169497 68.123910 12.052395 10:18:15 07/25/2024 60 57.208602 15.075029 72.283631 11.188551 68.157034 12.070424 10:19:15 07/25/2024 AVG 58.19 0.00 72.89 11.17 66.43 11.99 ppm@15% O2 34.13 5.23 31.11 NOx (g/bhp-hr) NOx (lbs/hr) CO (g/bhp-hr) CO (lbs/hr) NMNEHC C3 (g/bhp-hr) NMNEHC C3 (lbs/hr) 0.40 0.92 0.04 0.09 0.35 0.81 #3 FTIR Measurements Calculated Emission Levels Uinta Wax Operating, LLC North Randlett Compressor Station Run 1 Record Date EPA REFERENCE METHOD 1 EPA REFERENCE METHOD 2 Stack Diameter 13.5 Inches Kp=85.49 ft/sec Cp=0.84 Traverse Points 16 Port Point Insertion Depth dP Ts Stat P sqrt dP Ports 2 (inches)(in h2O)(deg R)(in H2O) EPA REFERENCE METHOD 3 A 1 0.50 0.82 1080 0.33 0.906 Average O2 8.3 (% dry)A 2 1.42 0.85 0.922 Average CO2 7.3 (% dry)A 3 2.62 0.84 0.917 Average N2 + CO 84.4 (% dry)A 4 4.36 0.88 0.938 Dry Molecular Weight 29.50 lb/lbmol A 5 9.14 0.81 0.900 Wet Molecular Weight 28.12 lb/lbmol A 6 10.88 0.89 0.943 EPA REFERENCE METHOD 320 A 7 12.08 0.89 0.943 Barometric Pressure 25.27 in Hg A 8 13.00 0.82 0.906 Moisture Content 11.99 %A 9 EPA REFERENCE METHOD 320 A 10 Average Analyzer NOx Level 72.89 ppm A 11 Calculated NOx Mass Output 0.92 lbs/hr A 12 Calculated NOx Output 0.40 g/bhp-hr A 13 EPA REFERENCE METHOD 320 A 14 Average Analyzer CO Level 11.17 ppm A 15 Calculated CO Mass Output 0.09 lbs/hr A 16 Calculated CO Output 0.04 g/bhp-hr B 1 0.50 0.83 1080 0.33 0.911 EPA REFERENCE METHOD 320 B 2 1.42 0.85 0.922 Average Analyzer NMNEHC Level 66.43 ppm B 3 2.62 0.86 0.927 Calculated NMNEHC Mass Output 0.81 lbs/hr B 4 4.36 0.85 0.922 Calculated NMNEHC Output 0.35 g/bhp-hr B 5 9.14 0.84 0.917 LOAD APPROXIMATION B 6 10.88 0.87 0.933 Estimated Engine Load 1035.0 BHP B 7 12.08 0.88 0.938 B 8 13.00 0.82 0.906 B 9 B 10 B 11 B 12 B 13 B 14 B 15 B 16 Averages 0.9 1080 0.3 0.922 Average Stack Gas Velocity 81.57 ft/sec Average Dry Flowrate 1769.69 dscfm TEST RUN # 1 NO Dry (ppm) NO2 Dry (ppm) NOx Dry (ppm) CO Dry (ppm) NMNEHC C3 Dry (ppm) H2O% (High) 191C Time 1 58.023712 15.295377 73.319089 11.245158 66.552805 11.698857 10:21:15 07/25/2024 2 57.735407 15.201734 72.937141 11.188899 66.472522 11.533576 10:22:15 07/25/2024 3 57.460032 15.275943 72.735975 11.111807 66.754227 11.659542 10:23:15 07/25/2024 4 57.789134 15.375981 73.165115 11.225713 66.608973 11.580115 10:24:15 07/25/2024 5 57.963313 15.464447 73.42776 11.14498 66.398698 11.896068 10:25:15 07/25/2024 6 57.441923 15.271766 72.713689 11.039673 66.275049 11.974514 10:26:16 07/25/2024 7 57.783801 15.387237 73.171038 11.132349 66.816766 11.715201 10:27:16 07/25/2024 8 57.220803 15.163876 72.384679 11.058445 67.095851 11.735618 10:28:16 07/25/2024 9 57.524785 15.360597 72.885382 11.13902 66.757481 11.454405 10:29:16 07/25/2024 10 57.082276 15.163657 72.245933 11.104098 67.599237 11.883793 10:30:16 07/25/2024 11 57.475105 15.407528 72.882633 11.083068 66.903724 12.997796 10:31:16 07/25/2024 12 57.723923 15.377335 73.101258 11.049278 66.996035 13.83428 10:32:16 07/25/2024 13 58.418432 15.662323 74.080755 11.038364 67.108053 14.351001 10:33:16 07/25/2024 14 58.328422 15.673617 74.002039 11.079686 67.451460 14.514427 10:34:16 07/25/2024 15 56.756033 15.197445 71.953478 11.047578 67.545669 14.76286 10:35:16 07/25/2024 16 56.825715 15.228995 72.05471 11.057199 67.964430 14.912619 10:36:17 07/25/2024 17 57.475228 15.500127 72.975355 11.059202 68.096989 15.005573 10:37:16 07/25/2024 18 57.351362 15.643754 72.995116 11.049393 68.617777 14.802255 10:38:17 07/25/2024 19 58.347882 15.587681 73.935563 11.155136 68.542274 14.607821 10:39:17 07/25/2024 20 57.841469 14.907521 72.74899 11.071007 67.925016 13.690105 10:40:17 07/25/2024 21 56.766408 14.130317 70.896725 11.100755 68.080982 13.071939 10:41:17 07/25/2024 22 57.520034 14.473973 71.994007 11.111601 68.303561 13.231361 10:42:17 07/25/2024 23 56.644525 14.342422 70.986947 11.058994 67.686989 13.014062 10:43:17 07/25/2024 24 57.494032 14.648582 72.142614 11.108315 67.040516 12.918256 10:44:17 07/25/2024 25 57.916163 14.80786 72.724023 11.100917 66.576002 12.897461 10:45:17 07/25/2024 26 58.409468 14.861606 73.271074 11.151214 66.512650 12.727451 10:46:17 07/25/2024 27 57.101673 14.331691 71.433364 11.111711 67.633194 12.859336 10:47:18 07/25/2024 28 57.973975 14.610225 72.5842 11.083921 66.572142 12.748563 10:48:17 07/25/2024 29 57.095622 14.423628 71.51925 11.11203 67.494249 12.715386 10:49:17 07/25/2024 30 56.724876 14.489218 71.214094 11.054362 67.784658 12.623926 10:50:18 07/25/2024 31 57.608149 14.862523 72.470672 11.107676 67.415114 12.588879 10:51:18 07/25/2024 32 57.9612 15.091739 73.052939 11.063257 67.253139 12.518991 10:52:18 07/25/2024 33 57.942143 14.984948 72.927091 11.159157 67.789063 12.392276 10:53:18 07/25/2024 34 57.779643 14.975543 72.755186 11.156369 68.630978 12.315109 10:54:18 07/25/2024 35 55.640295 14.551017 70.191312 11.092758 68.820440 12.355117 10:55:18 07/25/2024 36 56.216857 14.700298 70.917155 11.056172 68.953859 12.360229 10:56:18 07/25/2024 37 56.899777 14.826995 71.726772 11.082827 68.605250 12.337733 10:57:18 07/25/2024 38 56.152444 14.638914 70.791358 11.07053 69.047503 12.360452 10:58:19 07/25/2024 39 56.818451 14.897796 71.716247 11.123721 68.240169 12.309976 10:59:18 07/25/2024 40 57.483893 15.022603 72.506496 11.170761 68.444301 12.190449 11:00:18 07/25/2024 41 56.48364 14.807122 71.290762 11.173669 68.620813 12.169603 11:01:19 07/25/2024 42 57.986315 15.269033 73.255348 11.081858 67.699034 12.16804 11:02:19 07/25/2024 43 56.879284 15.00661 71.885894 11.063048 68.987375 12.1235 11:03:19 07/25/2024 44 55.965439 14.790937 70.756376 11.076354 68.749834 12.167575 11:04:19 07/25/2024 45 56.404936 14.813523 71.218459 11.03179 68.654005 12.244512 11:05:19 07/25/2024 46 57.273055 15.057295 72.33035 11.098112 68.715066 12.236643 11:06:19 07/25/2024 47 56.897864 14.991403 71.889267 11.044915 68.597789 12.154837 11:07:19 07/25/2024 48 56.424021 14.757569 71.18159 11.068074 69.244141 12.141942 11:08:19 07/25/2024 49 56.536139 14.894715 71.430854 11.07138 68.761211 12.129549 11:09:20 07/25/2024 50 56.531607 14.904632 71.436239 11.127629 69.531986 12.14819 11:10:20 07/25/2024 51 56.636836 14.927512 71.564348 11.036571 69.697811 12.175823 11:11:19 07/25/2024 52 55.28238 14.545996 69.828376 10.9994 69.918882 12.161412 11:12:20 07/25/2024 53 56.196236 14.791603 70.987839 11.056946 69.403060 12.175337 11:13:20 07/25/2024 54 56.343419 14.841224 71.184643 10.99591 69.423703 12.095523 11:14:20 07/25/2024 55 59.294196 15.692046 74.986242 11.129825 68.598987 12.051305 11:15:20 07/25/2024 56 58.494478 15.635722 74.1302 11.051419 69.062930 11.986198 11:16:20 07/25/2024 57 59.0843 15.693805 74.778105 11.092061 69.464165 11.983774 11:17:20 07/25/2024 58 58.47566 15.590988 74.066648 11.102613 69.360787 11.942615 11:18:20 07/25/2024 59 58.044124 15.441455 73.485579 11.032658 69.416634 12.017154 11:19:20 07/25/2024 60 57.325582 15.064863 72.390445 11.046646 70.262797 12.098789 11:20:20 07/25/2024 AVG 57.32 0.00 72.36 11.09 68.06 12.59 ppm@15% O2 33.88 5.19 31.87 NOx (g/bhp-hr) NOx (lbs/hr) CO (g/bhp-hr) CO (lbs/hr) NMNEHC C3 (g/bhp-hr) NMNEHC C3 (lbs/hr) 0.40 0.91 0.04 0.08 0.36 0.82 Calculated Emission Levels Record Date Uinta Wax Operating, LLC North Randlett Compressor Station Run 2 #3 FTIR Measurements EPA REFERENCE METHOD 1 EPA REFERENCE METHOD 2 Stack Diameter 13.5 Inches Kp=85.49 ft/sec Cp=0.84 Traverse Points 16 Port Point Insertion Depth dP Ts Stat P sqrt dP Ports 2 (inches)(in h2O)(deg R)(in H2O) EPA REFERENCE METHOD 3 A 1 0.50 0.84 1082 0.32 0.917 Average O2 8.3 (% dry)A 2 1.42 0.86 0.927 Average CO2 7.3 (% dry)A 3 2.62 0.87 0.933 Average N2 + CO 84.4 (% dry)A 4 4.36 0.89 0.943 Dry Molecular Weight 29.50 lb/lbmol A 5 9.14 0.84 0.917 Wet Molecular Weight 28.05 lb/lbmol A 6 10.88 0.85 0.922 EPA REFERENCE METHOD 320 A 7 12.08 0.84 0.917 Barometric Pressure 25.27 in Hg A 8 13.00 0.83 0.911 Moisture Content 12.59 %A 9 EPA REFERENCE METHOD 320 A 10 Average Analyzer NOx Level 72.36 ppm A 11 Calculated NOx Mass Output 0.91 lbs/hr A 12 Calculated NOx Output 0.40 g/bhp-hr A 13 EPA REFERENCE METHOD 320 A 14 Average Analyzer CO Level 11.09 ppm A 15 Calculated CO Mass Output 0.08 lbs/hr A 16 Calculated CO Output 0.04 g/bhp-hr B 1 0.50 0.82 1082 0.32 0.906 EPA REFERENCE METHOD 320 B 2 1.42 0.86 0.927 Average Analyzer NMNEHC Level 68.06 ppm B 3 2.62 0.89 0.943 Calculated NMNEHC Mass Output 0.82 lbs/hr B 4 4.36 0.89 0.943 Calculated NMNEHC Output 0.36 g/bhp-hr B 5 9.14 0.85 0.922 LOAD APPROXIMATION B 6 10.88 0.87 0.933 Estimated Engine Load 1035.0 BHP B 7 12.08 0.82 0.906 B 8 13.00 0.79 0.889 B 9 B 10 B 11 B 12 B 13 B 14 B 15 B 16 Averages 0.9 1082 0.3 0.922 Average Stack Gas Velocity 81.78 ft/sec Average Dry Flowrate 1758.68 dscfm TEST RUN # 2 NO Dry (ppm) NO2 Dry (ppm) NOx Dry (ppm) CO Dry (ppm) NMNEHC C3 Dry (ppm) H2O% (High) 191C Time 1 57.230165 15.133816 72.363981 11.094414 69.740571 12.225354 11:22:20 07/25/2024 2 57.498416 15.11451 72.612926 11.138427 69.066564 12.265878 11:23:21 07/25/2024 3 58.670784 15.610609 74.281393 10.951737 68.897922 12.257115 11:24:21 07/25/2024 4 58.016702 15.37841 73.395112 11.090155 68.761946 12.282097 11:25:21 07/25/2024 5 57.988557 15.254184 73.242741 11.142515 69.012822 12.277388 11:26:21 07/25/2024 6 57.930985 15.242128 73.173113 11.082476 69.028626 12.327542 11:27:21 07/25/2024 7 58.349545 15.416164 73.765709 11.10468 68.694547 12.291735 11:28:21 07/25/2024 8 58.144408 15.46536 73.609768 11.073321 68.475618 12.292722 11:29:21 07/25/2024 9 59.437309 15.702979 75.140288 11.110491 68.124743 12.329298 11:30:21 07/25/2024 10 58.612263 15.58524 74.197503 11.112379 67.953938 12.273089 11:31:21 07/25/2024 11 58.774733 15.831153 74.605886 11.021252 67.676807 12.266427 11:32:22 07/25/2024 12 59.178627 15.798279 74.976906 11.124994 67.681501 12.285845 11:33:21 07/25/2024 13 58.888962 15.757643 74.646605 11.090257 67.753009 12.23517 11:34:21 07/25/2024 14 58.345203 15.613411 73.958614 10.989239 67.435048 12.220516 11:35:22 07/25/2024 15 58.946984 15.623777 74.570761 11.071607 67.166774 12.289105 11:36:22 07/25/2024 16 59.611058 15.80944 75.420498 11.239692 67.343274 12.324223 11:37:22 07/25/2024 17 59.561794 15.717275 75.279069 11.148733 67.223481 12.28104 11:38:22 07/25/2024 18 59.441661 15.798514 75.240175 11.039421 67.310074 12.271775 11:39:22 07/25/2024 19 59.501942 15.764076 75.266018 11.127012 67.728514 12.274715 11:40:22 07/25/2024 20 58.627057 15.52013 74.147187 11.030714 67.932355 12.252707 11:41:22 07/25/2024 21 58.584866 15.503111 74.087977 11.0272 68.169888 12.206999 11:42:22 07/25/2024 22 59.493977 15.837637 75.331614 11.073573 67.605025 12.204375 11:43:22 07/25/2024 23 59.060095 16.009659 75.069754 11.023045 67.782860 12.100718 11:44:22 07/25/2024 24 57.094393 15.479506 72.573899 10.858134 68.677441 12.145749 11:45:23 07/25/2024 25 59.0062 16.08456 75.09076 10.997823 67.678125 12.213305 11:46:22 07/25/2024 26 58.843457 16.029236 74.872693 10.981897 68.327770 12.145238 11:47:22 07/25/2024 27 57.738989 15.601698 73.340687 10.913084 69.064755 12.091616 11:48:22 07/25/2024 28 58.594412 15.825153 74.419565 10.879564 68.572281 12.054035 11:49:23 07/25/2024 29 58.196305 15.939088 74.135393 10.879908 68.535798 11.939517 11:50:23 07/25/2024 30 58.782198 16.103191 74.885389 10.825582 68.120533 11.896554 11:51:23 07/25/2024 31 58.629362 15.966207 74.595569 10.872009 68.570446 12.085847 11:52:23 07/25/2024 32 58.42256 15.933085 74.355645 10.889852 68.129530 12.169734 11:53:23 07/25/2024 33 58.914439 16.122976 75.037415 10.844397 67.342934 12.110514 11:54:23 07/25/2024 34 59.159754 16.242773 75.402527 10.866297 67.716843 12.085358 11:55:23 07/25/2024 35 57.821639 15.90618 73.727819 10.813563 67.741201 12.116847 11:56:24 07/25/2024 36 59.041162 16.189004 75.230166 10.851588 67.351762 12.071746 11:57:23 07/25/2024 37 58.446072 15.966805 74.412877 10.796478 67.861316 12.018149 11:58:23 07/25/2024 38 58.588354 15.989125 74.577479 10.82587 67.914264 11.99292 11:59:23 07/25/2024 39 58.432879 15.971735 74.404614 10.886177 68.104520 12.081997 12:00:23 07/25/2024 40 59.422298 16.115838 75.538136 10.90585 67.832861 12.087812 12:01:24 07/25/2024 41 59.431628 16.012057 75.443685 10.954976 67.757218 12.074547 12:02:24 07/25/2024 42 59.363885 16.14224 75.506125 10.896344 68.128356 12.050736 12:03:24 07/25/2024 43 58.920894 16.136995 75.057889 10.909744 68.295299 11.943619 12:04:24 07/25/2024 44 58.318422 15.870058 74.18848 10.786565 68.588336 11.91541 12:05:24 07/25/2024 45 57.888212 15.92812 73.816332 10.777198 68.297696 11.917097 12:06:24 07/25/2024 46 58.836898 16.151006 74.987904 10.862787 67.524989 11.95853 12:07:24 07/25/2024 47 57.698345 15.939366 73.637711 10.734966 67.941719 11.95471 12:08:24 07/25/2024 48 58.040029 15.974779 74.014808 10.807773 67.617405 11.995422 12:09:24 07/25/2024 49 57.552351 15.709902 73.262253 10.740015 67.885964 12.0172 12:10:25 07/25/2024 50 57.869582 15.670787 73.540369 10.764777 67.630625 12.094823 12:11:24 07/25/2024 51 58.509223 15.995641 74.504864 10.782636 67.042707 12.116483 12:12:25 07/25/2024 52 57.516378 15.631412 73.14779 10.738282 67.676752 12.105235 12:13:25 07/25/2024 53 58.362105 16.020555 74.38266 10.697463 67.057430 12.110687 12:14:25 07/25/2024 54 58.602246 15.988113 74.590359 10.747242 67.154810 12.06542 12:15:25 07/25/2024 55 58.463791 16.106764 74.570555 10.759301 67.120681 12.086296 12:16:25 07/25/2024 56 56.786799 15.440039 72.226838 10.748836 68.128067 12.234385 12:17:25 07/25/2024 57 58.41145 15.877396 74.288846 10.752465 67.327509 12.262561 12:18:25 07/25/2024 58 58.603879 15.929387 74.533266 10.86936 67.136947 12.048261 12:19:25 07/25/2024 59 58.548334 15.974227 74.522561 10.810903 67.686181 12.061504 12:20:25 07/25/2024 60 58.152414 15.913773 74.066187 10.842289 68.208439 12.171055 12:21:26 07/25/2024 AVG 58.52 15.81 74.32 10.93 67.97 12.14 ppm@15% O2 34.53 5.08 31.58 NOx (g/bhp-hr) NOx (lbs/hr) CO (g/bhp-hr) CO (lbs/hr) NMNEHC C3 (g/bhp-hr) NMNEHC C3 (lbs/hr) 0.41 0.94 0.04 0.08 0.36 0.82 FTIR Measurements #3 Calculated Emission Levels Uinta Wax Operating, LLC North Randlett Compressor Station Run 3 Record Date EPA REFERENCE METHOD 1 EPA REFERENCE METHOD 2 Stack Diameter 13.5 Inches Kp=85.49 ft/sec Cp=0.84 Traverse Points 16 Port Point Insertion Depth dP Ts Stat P sqrt dP Ports 2 (inches)(in h2O)(deg R)(in H2O) EPA REFERENCE METHOD 3 A 1 0.50 0.81 1085 0.34 0.900 Average O2 8.2 (% dry)A 2 1.42 0.85 0.922 Average CO2 7.3 (% dry)A 3 2.62 0.89 0.943 Average N2 + CO 84.5 (% dry)A 4 4.36 0.88 0.938 Dry Molecular Weight 29.50 lb/lbmol A 5 9.14 0.87 0.933 Wet Molecular Weight 28.10 lb/lbmol A 6 10.88 0.84 0.917 EPA REFERENCE METHOD 320 A 7 12.08 0.83 0.911 Barometric Pressure 25.26 in Hg A 8 13.00 0.81 0.900 Moisture Content 12.14 %A 9 EPA REFERENCE METHOD 320 A 10 Average Analyzer NOx Level 74.32 ppm A 11 Calculated NOx Mass Output 0.94 lbs/hr A 12 Calculated NOx Output 0.41 g/bhp-hr A 13 EPA REFERENCE METHOD 320 A 14 Average Analyzer CO Level 10.93 ppm A 15 Calculated CO Mass Output 0.08 lbs/hr A 16 Calculated CO Output 0.04 g/bhp-hr B 1 0.50 0.84 1085 0.34 0.917 EPA REFERENCE METHOD 320 B 2 1.42 0.87 0.933 Average Analyzer NMNEHC Level 67.97 ppm B 3 2.62 0.88 0.938 Calculated NMNEHC Mass Output 0.82 lbs/hr B 4 4.36 0.88 0.938 Calculated NMNEHC Output 0.36 g/bhp-hr B 5 9.14 0.84 0.917 LOAD APPROXIMATION B 6 10.88 0.85 0.922 Estimated Engine Load 1035.0 BHP B 7 12.08 0.82 0.906 B 8 13.00 0.81 0.900 B 9 B 10 B 11 B 12 B 13 B 14 B 15 B 16 Averages 0.8 1085 0.3 0.921 Average Stack Gas Velocity 81.71 ft/sec Average Dry Flowrate 1760.89 dscfm TEST RUN # 3 APPENDIX B Date Time NO 191C span NO2 191C span H2O% (high) 191C Formaldehyde 191C Ethylene 191C TE span Propane 191C span Acetaldehyde 191C span CO ppm 191C (1of2) span CO ppm Dry CO2% 191C NOx Wet NOx Dry NM NE HC C3 Temp ( C )Pressure (atm) 7/25/2024 9:03:16 0.024558 -0.023755 0.001202 -0.011169 0.294871 0.032636 0.116186 -0.12726 -0.127262 -0.004198 0.000803 0.000803 0.004357 190.833237 1.137776 7/25/2024 9:03:24 0.105395 -0.141942 0.00218 0.065084 0.215859 -0.131908 0.093034 0.154524 0.154527 0.001521 -0.036548 -0.036548 -0.001021 190.829773 1.13997 7/25/2024 9:03:31 0.087703 -0.038683 -0.002365 -0.084698 -0.210506 0.069617 0.15538 0.027675 0.027674 0.005423 0.04902 0.049019 0.003736 190.682602 1.132505 7/25/2024 9:03:39 0.170661 0.004721 -0.00127 -0.060854 0.05816 0.260284 -0.106854 0.014909 0.014909 0.009647 0.175382 0.175379 0.017756 190.697128 1.093856 7/25/2024 9:04:17 0 0 0 0 0 0 0 0 0 0 0 0 0 190.682159 1.068342 7/25/2024 9:04:31 -0.099678 0.059635 -0.004842 -0.012668 -0.169353 0.090678 0.104775 -0.146476 -0.146469 0.000727 -0.040043 -0.040041 0.008308 190.664429 1.06501 7/25/2024 9:04:39 -0.054538 0.059412 -0.004221 0.059681 0.490235 0.08713 -0.024904 0.119296 0.119291 0.000905 0.004874 0.004874 0.0095 190.638992 1.074347 7/25/2024 9:04:46 -0.009637 0.022011 -0.001253 -0.187524 0.062617 0.019111 -0.247967 0.126415 0.126414 0.000434 0.012374 0.012374 0.013892 190.682602 1.06815 7/25/2024 9:04:53 0.038426 0.05905 -0.00253 0.084872 0.165468 -0.194578 0.605651 0.085625 0.085623 0.008973 0.097476 0.097473 0.002242 190.726212 1.06939 7/25/2024 9:05:01 -0.180824 -0.041915 -0.003307 -0.046536 -0.30308 -0.215737 0.115939 0.057775 0.057773 0.005852 -0.222739 -0.222731 0.017062 190.697128 1.064478 7/25/2024 9:05:08 -0.035239 -0.041207 -0.002679 -0.043052 0.215015 0.390107 0.647568 0.047387 0.047386 0.008192 -0.076446 -0.076444 0.014864 190.682602 1.071639 7/25/2024 9:05:16 0.078106 -0.026265 -0.000627 -0.055611 0.124837 -0.072976 -0.195197 0.025448 0.025448 0.004631 0.051842 0.051841 -0.000869 190.626266 1.070044 7/25/2024 9:05:23 -0.163317 0.071336 -0.003838 -0.052215 0.045814 0.153631 -0.543498 -0.042298 -0.042297 0.008704 -0.091981 -0.091977 -0.000991 190.638992 1.06509 7/25/2024 9:05:31 -0.035925 -0.052425 -0.00096 0.003963 -0.420559 0.167997 0.301532 0.010854 0.010854 -0.007619 -0.08835 -0.088349 0.003375 190.624451 1.066452 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm) 7/25/2024 9:05:51 518.331851 490.880643 491.12721 190.596588 1.077166 7/25/2024 9:07:18 98.13731 190.596588 1.066402 7/25/2024 9:05:58 525.203951 501.08664 498.94399 190.580841 1.075219 7/25/2024 9:07:25 99.267444 190.624451 1.06916 7/25/2024 9:06:05 524.587723 501.34809 497.825403 190.609924 1.076367 7/25/2024 9:07:33 99.990869 190.609924 1.064799 7/25/2024 9:06:13 524.314253 500.250205 496.171994 190.566315 1.078065 7/25/2024 9:07:40 99.324289 190.595383 1.069068 7/25/2024 9:06:20 522.983918 499.699203 493.950349 190.624451 1.080039 7/25/2024 9:07:48 99.561059 190.566315 1.071593 7/25/2024 9:06:28 526.580097 502.96008 500.596145 190.66806 1.072832 7/25/2024 9:07:55 99.938404 190.580841 1.070032 7/25/2024 9:06:35 524.611896 501.338571 498.648563 190.580841 1.077698 7/25/2024 9:08:03 99.456813 190.575394 1.068718 7/25/2024 9:06:43 525.031103 500.932761 495.835892 190.58812 1.07876 7/25/2024 9:08:10 99.88311 190.609924 1.066452 7/25/2024 9:06:50 524.847749 500.773111 498.150322 190.595383 1.078892 7/25/2024 9:08:18 100.183837 190.580841 1.067554 7/25/2024 9:06:58 521.317921 497.910822 495.327497 190.624451 1.085869 7/25/2024 9:08:25 99.15143 190.580841 1.065626 Date Time NO2 191C span Temp ( C )Pressure (atm) 7/25/2024 9:08:46 121.342084 190.675995 1.082802 7/25/2024 9:08:54 137.732547 190.638992 1.09097 7/25/2024 9:09:01 140.614086 190.624451 1.094131 7/25/2024 9:09:09 142.248429 190.638992 1.089954 7/25/2024 9:09:16 143.188604 190.66806 1.094223 7/25/2024 9:09:24 143.910647 190.566315 1.091606 7/25/2024 9:09:31 144.611545 190.580841 1.09156 7/25/2024 9:09:39 144.943564 190.562683 1.094223 7/25/2024 9:09:46 145.182763 190.551773 1.095738 7/25/2024 9:09:54 145.614056 190.566315 1.093947 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm) 7/25/2024 9:10:14 6.604911 102.377477 7.995207 190.562683 1.028487 7/25/2024 9:11:49 80.569929 190.702591 1.025341 7/25/2024 9:10:22 360.585889 376.062809 321.206319 190.580841 1.023717 7/25/2024 9:11:56 99.363636 190.624451 1.020274 7/25/2024 9:10:29 506.95282 492.081065 491.241724 190.551773 1.021835 7/25/2024 9:12:04 99.224215 190.653519 1.026792 7/25/2024 9:10:37 508.412633 491.538584 492.903188 190.609924 1.022891 7/25/2024 9:12:11 98.603863 190.697128 1.024773 7/25/2024 9:10:44 509.958013 492.931597 495.095857 190.595383 1.022661 7/25/2024 9:12:19 99.798525 190.726212 1.021789 7/25/2024 9:10:52 507.41993 490.937361 493.585403 190.551773 1.023809 7/25/2024 9:12:26 100.053952 190.697128 1.025369 7/25/2024 9:10:59 509.872145 493.090606 493.828785 190.664429 1.022489 7/25/2024 9:12:34 100.030967 190.653519 1.026563 7/25/2024 9:11:07 509.117822 492.355279 493.059784 190.653519 1.02491 7/25/2024 9:12:42 100.757003 190.651703 1.022288 7/25/2024 9:11:14 512.364839 494.283956 495.625693 190.624451 1.023809 7/25/2024 9:12:49 99.116142 190.66806 1.024359 7/25/2024 9:11:22 512.85675 495.274419 500.367994 190.638992 1.02055 7/25/2024 9:12:56 100.010721 190.638992 1.021743 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Ethylene 191C TE Temp ( C )Pressure (atm) 7/25/2024 9:13:34 0.140873 0.123219 0.474953 0.529762 190.638992 1.070164 7/25/2024 9:13:41 0.078389 0.116397 0.149898 0.145346 190.706818 1.07082 7/25/2024 9:13:49 0.064275 0.01503 -0.025893 -0.212518 190.689865 1.070847 7/25/2024 9:13:57 0.189927 0.170959 -0.205755 0.051937 190.726212 1.069298 7/25/2024 9:14:04 -0.003828 0.271205 0.042159 0.552537 190.71167 1.069068 Raw Calibration Data BACKGROUND / PRE DIRECT ZERO PRE DIRECT CAL NO2 CAL PRE SYSTEM CAL PRE SYSTEM ZERO Date Time CO2% 191C Propane 191C span Temp ( C )Pressure (atm) 7/25/2024 9:16:19 6.649826 44.622186 190.698349 1.023694 7/25/2024 9:16:27 6.627961 44.181633 190.769806 1.025232 7/25/2024 9:16:34 6.610544 42.601877 190.66806 1.02693 7/25/2024 9:16:49 6.603569 43.984382 190.681839 1.026949 7/25/2024 9:16:57 6.638751 44.30726 190.638992 1.021766 7/25/2024 9:17:04 6.58416 44.152376 190.66806 1.028307 7/25/2024 9:17:12 3.990706 35.114293 190.664429 1.026465 7/25/2024 9:17:19 1.035491 290.808514 190.609924 1.028123 7/25/2024 9:17:27 0.807366 411.205629 190.638992 1.030419 7/25/2024 9:17:34 2.692 250.33807 190.66806 1.025691 7/25/2024 9:17:42 6.201254 70.236502 190.638992 1.030281 7/25/2024 9:17:50 6.276082 65.218024 190.624451 1.027022 7/25/2024 9:17:57 6.265815 66.748659 190.71167 1.026333 7/25/2024 9:18:04 6.016118 82.267648 190.651703 1.02755 7/25/2024 9:18:19 5.979163 83.821319 190.676483 1.024565 7/25/2024 9:18:27 5.97122 83.522045 190.689865 1.028192 7/25/2024 9:18:34 6.009723 83.085576 190.71167 1.022799 7/25/2024 9:18:42 6.376329 58.687806 190.798889 1.027068 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm) 7/25/2024 12:25:22 485.799645 462.711688 463.249946 190.978149 1.067286 7/25/2024 12:23:54 54.806417 190.969681 1.064046 7/25/2024 12:25:29 506.22251 485.45081 484.20735 190.987854 1.071088 7/25/2024 12:24:02 97.770194 191.00238 1.061219 7/25/2024 12:25:36 509.76839 489.217091 487.598765 190.958771 1.069252 7/25/2024 12:24:09 98.982543 190.958771 1.059658 7/25/2024 12:25:44 515.139355 492.049745 489.197 190.944244 1.067875 7/25/2024 12:24:17 99.213845 190.958771 1.058694 7/25/2024 12:25:51 516.741057 493.579229 492.184832 190.958771 1.067416 7/25/2024 12:24:24 98.781656 190.958771 1.061357 7/25/2024 12:25:59 515.915698 493.525867 493.176787 190.987854 1.067737 7/25/2024 12:24:32 99.060034 190.944244 1.059429 7/25/2024 12:26:06 517.573159 495.05129 493.312872 190.987854 1.067921 7/25/2024 12:24:39 99.181758 190.987854 1.054058 7/25/2024 12:26:14 518.88728 496.065762 496.265035 190.982391 1.067353 7/25/2024 12:24:47 98.885008 190.982391 1.059039 7/25/2024 12:26:21 520.865077 497.391415 495.34156 190.987854 1.064157 7/25/2024 12:24:54 99.330491 190.944244 1.060898 7/25/2024 12:26:29 520.993868 498.158598 495.134919 190.973312 1.064799 7/25/2024 12:25:02 98.595033 190.987854 1.061311 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm) 7/25/2024 12:24:09 -0.296917 0.102869 0.280603 190.958771 1.059658 7/25/2024 12:27:04 0.16463 190.987854 1.072465 7/25/2024 12:24:17 -0.143859 0.193783 0.134847 190.958771 1.058694 7/25/2024 12:27:12 0.549351 190.944244 1.078111 7/25/2024 12:24:24 -0.099721 0.199139 0.170121 190.958771 1.061357 7/25/2024 12:27:19 0.426954 190.987854 1.079213 7/25/2024 12:24:32 -0.5091 -0.023854 -0.479066 190.944244 1.059429 7/25/2024 12:27:27 0.296584 191.00238 1.076321 7/25/2024 12:24:39 -0.316119 0.024572 0.045332 190.987854 1.054058 7/25/2024 12:27:34 0.644581 190.958771 1.082334 7/25/2024 12:24:47 -0.105193 0.114667 -0.481256 190.982391 1.059039 7/25/2024 12:27:42 -0.084961 190.931519 1.080487 7/25/2024 12:24:54 -0.417637 0.006529 -0.105484 190.944244 1.060898 7/25/2024 12:27:49 0.52694 190.961197 1.081906 7/25/2024 12:25:02 -0.141876 0.064269 -0.763533 190.987854 1.061311 7/25/2024 12:27:57 0.035306 190.969681 1.079081 SAMPLE SPIKE RECOVERY POST SYSTEM CAL POST SYSTEM ZERO PRE TEST 1 495.6 6.6 44.3 6.0 83.8 0.099 72.3% Sensor Analyzer Cal Zero Cal Zero Response (ppm)Level (ppm)Response (ppm)Error (%)Error (%) NOx 497.9 493.4 0.0 0.91 -0.01 CO 521.3 520.2 0.0 0.21 0.01 Propane 495.3 495.6 0.0 -0.05 0.01 Ethylene 99.2 101.9 0.1 -2.70 0.08 Sensor System Cal Zero Cal Zero Response (ppm)Level (ppm)Response (ppm)Recovery (%)Error (%) NOx 495.3 493.4 0.1 0.38 0.03 CO 512.9 520.2 0.1 -1.41 0.02 Propane 500.4 495.6 0.1 0.96 0.02 Ethylene*100.0 101.9 0.2 -1.85 0.21 Sensor System Cal Zero Cal Zero Cal Zero Response (ppm)Level (ppm)Response (ppm)Recovery (%)Error (%)Drift Error (%)Drift Error (%) NOx 498.2 493.4 0.1 0.96 0.02 0.58 0.01 CO 521.0 520.2 -0.3 0.15 -0.05 1.56 0.07 Propane 495.1 495.6 -0.1 -0.09 -0.01 1.06 0.03 Ethylene*98.6 101.9 0.4 -3.24 0.41 1.39 0.20 *CTS Scans are conducted with Ethylene through the sample line. Lf 5.11 Lr Cr Tr Pr Lr/Lf 4.92 99.2 190.6 1.1 0.96 Ls Cs Ts Ps Ls/Lf 5.09 100.0 190.6 1.0 1.00 Pathlength Stack Propane Concentration Stack + Spike CO2 Concentration Stack + Propane Concentration DF Calculated POST SYSTEM CAL PRE SYSTEM CAL % Recovery Propane PRE DIRECT CAL FTIR QA/QC SUMMARY SAMPLE RECOVERY CALCULATIONS Period Spike #Concentration of Propane Cylinder Stack CO2 Concentration UWO – North Randlett 7-25-2024 UWO – North Randlett 7-25-2024 UWO – North Randlett 7-25-2024 Instrument Resolution – FWHH – 0.4687 cm-1 which is < 0.55 cm-1 (therefore meets manufacturer specifications) Water Frequency – Freq – 3920.0938 cm-1 which is +/- 0.075 of 3920.0952 cm-1 (therefore meets ASTM) Please note: FWHH is the Full Width at Half Height of the resolution. The frequency position is only calculating the center line for one water line in the spectrum. MKS uses 3920.0952 cm-1 since it is a single water line. Spectral Fit Run 1 Spectral Fit Run 2 Spectral Fit Run 3 Analysis Validation Report Sample Filename: C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000126.LAB Filename for noise: C:\OLT\2024 Data\Hilcorp\South Moxa E2 6-4-24\SOUTH MOXA E2 6-4-24_000011.LAB Interferences Filenames: C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000068.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000069.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000070.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000071.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000072.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000073.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000074.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000075.LAB Recipe path: C:\OLT\RECIPES\NEW TEST.MGRCP Gas calibration NameConc MDC3 MDC2 MDC1 MAU FMU*R OCU ~ DL ~ CL ~ Bias Sigma Range Span Comment NO 191C 50.53 2.06 -0.77 1.05 2.8 2.8 -1.01 --0-2795 1.02 Good NO2 191C 12.58 0.36 -0.08 0.09 0.38 0.38 -0.25 --0-488 1.02 Good N2O 191C 0.13 0.39 0.1 0.09 0.11 0.45 0.45 0.14 0.31 0.04 0.03 0-200 -Close to DL NH3 TE 191C -0.21 20.4 10.69 10.86 18.54 34.82 34.82 11.81 11.81 1.12 3.56 0-2995 -Close to DL H2O% (HIGH) 191C12.19 0.18 -0.04 0.07 0.3 0.3 -0.24 --0-40 -Good FORMALDEHYDE 191C5.98 0.81 5.01 0.62 0.7 0.92 0.92 5.58 5.58 0.56 1.67 0-69 -Close to DL FORMIC ACID 191C TE1.19 13.78 1.29 3.65 4.27 16.13 16.13 1.56 10.19 0.28 0.43 0-466 -Close to DL CH4 2900 CM-1 191C746.16 14.33 -3.84 5.58 27.61 27.61 -14.92 --0-3143 0.98 Good PROPANE 191C43.31 1.71 -0.55 0.65 2.05 2.05 -0.87 --0-4976 0.95 Good PROPYLENE 191C TE-1.49 12.91 1.62 3.86 4.57 15.28 15.28 1.72 9.1 0.11 0.54 0-194 -Close to DL ETHANE 191C 80.25 3.65 -1.26 1.96 5.69 5.69 -1.61 --0-1004 -Good ETHYLENE 191C TE11.72 19.22 12.65 5.17 6.38 23.71 23.71 14.66 14.66 2.01 4.22 0-900 -Close to DL CO PPM 191C (1OF2)9.85 0.93 -0.44 0.96 1.73 1.73 -0.28 --0-5010 0.99 Good CO2% 191C 6.43 0.24 -0.03 0.04 0.33 0.33 -0.13 --0-23 -Good CO% 191C (2OF2)0 0 0 0 0 0 0 0 0 0 0 0-8 -Close to DL ACETALDEHYDE 191C0.87 2.21 1.19 1.67 2.15 2.84 2.84 1.41 1.41 0.21 0.4 0-186 1.04 Close to DL ACETYLENE 191C0.08 1.84 0.44 1.83 2.42 2.43 2.43 0.48 0.48 0.04 0.15 0-1016 -Close to DL SO2 191C 2.26 3.41 1.27 1.02 1.24 4.15 4.15 1.85 2.47 0.58 0.42 0-964 -Close to DL HEXANE 191C 3.82 1.07 4.07 0.32 0.43 1.45 1.45 4.58 4.58 0.51 1.36 0-1000 -Close to DL Analysis Validation Report Sample Filename: C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000183.LAB Filename for noise: C:\OLT\2024 Data\Hilcorp\South Moxa E2 6-4-24\SOUTH MOXA E2 6-4-24_000011.LAB Interferences Filenames: C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000068.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000069.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000070.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000071.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000072.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000073.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000074.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000075.LAB Recipe path: C:\OLT\RECIPES\NEW TEST.MGRCP Gas calibration NameConc MDC3 MDC2 MDC1 MAU FMU*R OCU ~ DL ~ CL ~ Bias Sigma Range Span Comment NO 191C 48.9 1.98 -0.77 1.05 2.69 2.69 -0.98 --0-2795 1.02 Good NO2 191C 12.23 0.37 -0.08 0.09 0.39 0.39 -0.24 --0-488 1.02 Good N2O 191C 0.1 0.38 0.1 0.09 0.11 0.44 0.44 0.14 0.3 0.04 0.03 0-200 -Close to DL NH3 TE 191C -0.34 19.62 10.69 10.86 18.54 33.49 33.49 11.81 11.81 1.12 3.56 0-2995 -Close to DL H2O% (HIGH) 191C12.62 0.18 -0.04 0.07 0.29 0.29 -0.25 --0-40 -Good FORMALDEHYDE 191C6.05 0.77 5.01 0.62 0.7 0.87 0.87 5.58 5.58 0.56 1.67 0-69 -Close to DL FORMIC ACID 191C TE1.2 13.39 1.29 3.65 4.27 15.68 15.68 1.56 9.81 0.28 0.43 0-466 -Close to DL CH4 2900 CM-1 191C709.22 13.02 -3.84 5.58 25.09 25.09 -14.18 --0-3143 0.98 Good PROPANE 191C43.39 1.65 -0.55 0.65 1.99 1.99 -0.87 --0-4976 0.95 Good PROPYLENE 191C TE-1.14 12.63 1.62 3.86 4.57 14.94 14.94 1.72 8.83 0.11 0.54 0-194 -Close to DL ETHANE 191C 76.98 3.6 -1.26 1.96 5.6 5.6 -1.54 --0-1004 -Good ETHYLENE 191C TE11.94 18.88 12.65 5.17 6.38 23.3 23.3 14.66 14.66 2.01 4.22 0-900 -Close to DL CO PPM 191C (1OF2)9.71 0.95 -0.44 0.96 1.75 1.75 -0.29 --0-5010 0.99 Good CO2% 191C 6.43 0.23 -0.03 0.04 0.32 0.32 -0.13 --0-23 -Good CO% 191C (2OF2)0 0 0 0 0 0 0 0 0 0 0 0-8 -Close to DL ACETALDEHYDE 191C0.87 2.17 1.19 1.67 2.15 2.79 2.79 1.41 1.41 0.21 0.4 0-186 1.04 Close to DL ACETYLENE 191C0.19 1.83 0.44 1.83 2.42 2.42 2.42 0.48 0.48 0.04 0.15 0-1016 -Close to DL SO2 191C 2.31 3.56 1.27 1.02 1.24 4.33 4.33 1.85 2.62 0.58 0.42 0-964 -Close to DL HEXANE 191C 4.14 1.05 4.07 0.32 0.43 1.42 1.42 4.58 4.58 0.51 1.36 0-1000 -Close to DL Analysis Validation Report Sample Filename: C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000245.LAB Filename for noise: C:\OLT\2024 Data\Hilcorp\South Moxa E2 6-4-24\SOUTH MOXA E2 6-4-24_000011.LAB Interferences Filenames: C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000068.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000069.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000070.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000071.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000072.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000073.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000074.LAB C:\OLT\2024 Data\Uinta Wax\N Randlett #3 7-25-24\N RANDLETT #3 7-25-24_000075.LAB Recipe path: C:\OLT\RECIPES\NEW TEST.MGRCP Gas calibration NameConc MDC3 MDC2 MDC1 MAU FMU*R OCU ~ DL ~ CL ~ Bias Sigma Range Span Comment NO 191C 50.92 1.97 -0.77 1.05 2.69 2.69 -1.02 --0-2795 1.02 Good NO2 191C 13.56 0.35 -0.08 0.09 0.37 0.37 -0.27 --0-488 1.02 Good N2O 191C 0.12 0.39 0.1 0.09 0.11 0.45 0.45 0.14 0.31 0.04 0.03 0-200 -Close to DL NH3 TE 191C -1.56 19 10.69 10.86 18.54 32.43 32.43 11.81 11.81 1.12 3.56 0-2995 -Close to DL H2O% (HIGH) 191C12.09 0.17 -0.04 0.07 0.28 0.28 -0.24 --0-40 -Good FORMALDEHYDE 191C5.88 0.79 5.01 0.62 0.7 0.9 0.9 5.58 5.58 0.56 1.67 0-69 -Close to DL FORMIC ACID 191C TE1.83 13.68 1.29 3.65 4.27 16.01 16.01 1.56 10.07 0.28 0.43 0-466 -Close to DL CH4 2900 CM-1 191C703.18 12.84 -3.84 5.58 24.74 24.74 -14.06 --0-3143 0.98 Good PROPANE 191C44.18 1.72 -0.55 0.65 2.06 2.06 -0.88 --0-4976 0.95 Good PROPYLENE 191C TE-1.06 12.86 1.62 3.86 4.57 15.21 15.21 1.72 9.05 0.11 0.54 0-194 -Close to DL ETHANE 191C 78.35 3.69 -1.26 1.96 5.75 5.75 -1.57 --0-1004 -Good ETHYLENE 191C TE11.84 19.03 12.65 5.17 6.38 23.48 23.48 14.66 14.66 2.01 4.22 0-900 -Close to DL CO PPM 191C (1OF2)9.61 0.89 -0.44 0.96 1.64 1.64 -0.25 --0-5010 0.99 Good CO2% 191C 6.46 0.23 -0.03 0.04 0.32 0.32 -0.13 --0-23 -Good CO% 191C (2OF2)0 0 0 0 0 0 0 0 0 0 0 0-8 -Close to DL ACETALDEHYDE 191C0.82 2.18 1.19 1.67 2.15 2.8 2.8 1.41 1.41 0.21 0.4 0-186 1.04 Close to DL ACETYLENE 191C0.18 1.8 0.44 1.83 2.42 2.37 2.42 0.48 0.48 0.04 0.15 0-1016 -Close to DL SO2 191C 2.4 3.4 1.27 1.02 1.24 4.15 4.15 1.85 2.46 0.58 0.42 0-964 -Close to DL HEXANE 191C 4.3 1.08 4.07 0.32 0.43 1.46 1.46 4.58 4.58 0.51 1.36 0-1000 -Close to DL APPENDIX C Test Run Load %Site Rated Load, bhp Load Approx., bhp 1 75 1380 1035.0 2 75 1380 1035.0 3 75 1380 1035.0 Engine Load Approximation based on Panel Levels APPENDIX D Test Run Flowrate dscfm Approx. BHP Avg O2 % NOx ppmvd NOx g/bhp-hr NOx lbs/hr CO ppmvd CO g/bhp-hr CO lbs/hr NMNEHC ppmvd NMNEHC g/bhp-hr NMNEHC lbs/hr Moisture Content % 1 1769.69 1035.0 8.3 72.89 0.40 0.92 11.17 0.04 0.09 66.43 0.35 0.81 11.99 2 1758.68 1035.0 8.3 72.36 0.40 0.91 11.09 0.04 0.08 68.06 0.36 0.82 12.59 3 1760.89 1035.0 8.2 74.32 0.41 0.94 10.93 0.04 0.08 67.97 0.36 0.82 12.14 1035.0 8.3 73.19 0.41 0.92 11.06 0.04 0.08 67.49 0.36 0.82 12.24 Summary Average Levels Example Calculations: Uinta Wax Operating, LLC, North Randlett Compressor Station, #3 The following is a step-by-step calculation for the first test run conducted on the North Randlett Compressor Station #3. Test Parameters • Stack Diameter = 13.5 inches • Traverse Points = 16 • Ports = 2 • Barometric Pressure = 25.27 in Hg • Average O2 = 8.3% • Average CO2 = 7.3% • Load Approximation = 1035.0 bhp • Moisture Content = 11.99% EPA 40 CFR 60(A) Methods 1-3: Determination of Stack Gas Velocity and Flow Rate Dry Molecular Weight (lb/lbmol) = (0.44 * %CO2) + (0.32 * %O2) + ((0.28 * (%N2 + %CO)) Where: %CO2 – Carbon Dioxide Content Of The Gas = 7.3% %O2 – Oxygen Content Of The Gas = 8.3% %N2 – Nitrogen Content Of The Gas %CO – Carbon Monoxide Content Of The Gas (%N2 +%CO) = (100 - %O2 - %CO2) = (100 – 8.3 – 7.3) = 84.4% Dry = (0.44 * %CO2) + (0.32 * %O2) + ((0.28 * (%N2 + %CO)) = (0.44 * 7.3) + (0.32 * 8.3) + (0.28 * 84.4) = 29.50 lb/lbmol Wet Molecular Weight (lb/lbmol) = MD * (1-BWS) + (18) * BWS Where: MD – Molecular Weight Of The Dry Gas (lb/lbmol) = 29.50 lb/lbmol BWS – Moisture Content Of The Gas (%/100) = 11.99% = MD * (1-BWS) + (18) * BWS = 29.50 * (1 – (11.99/ 100)) + (18 * (11.99/ 100)) = 28.12 lb/lbmol Average Stack Gas Velocity (ft/sec) = Cp * (85.49) * ∆PAVG * (TS / (((PS / 13.6) + PB) * MA)) Where: CP – Pitot tube constant (unitless) = 0.84 ∆PAVG – Average square root of the stack gas pitot DP (inches water) = 0.922 in H2O TS – Average stack temperature (R) = 1080 R PB – Barometric pressure (in Hg) = 25.27 in Hg PS – Stack pressure relative to barometric pressure (inches water) = 0.3 in H2O MA – Molecular weight of the wet gas (lb/lbmol) = 28.12 lb/lbmol = Cp * (85.49) * ∆PAVG * (TS / (((PS / 13.6) + PB) * MA)) = 0.84 * (85.49) * 0.922 * ( 1080 / (((0.3/ 13.6) + 25.27) * 28.12)) = 81.57 ft/sec Average Dry Flowrate (dscfm) = 60 * (1-BWS) * VS *  * (((DS / 2) / 12))2)* TSTD / TS * (PB + (PS / 13.6)) / 29.92 Where: DS – Diameter of the stack (inches) = 13.5 inches BWS – Moisture content of the gas (%) = 11.99% TSTD – Standard temperature (528R) TS – Average stack temperature (R) = 1080 R PB – Barometric pressure (in Hg) = 25.27 in Hg PS – Stack pressure relative to barometric pressure (inches water) = 0.3 in H2O VS– Average Stack gas velocity (ft/sec) = 81.57 ft/sec = 60 * (1-BWS) * VS *  * (((DS / 2) / 12))2)* TSTD / TS * (PB + (PS / 13.6)) / 29.92 = 60 * (1 - (11.99/ 100)) * 81.57 *  * (((13.5 / 2) / 12))2) * 528 / 1080 * (25.27 + (0.3 / 13.6)) / 29.92 = 1769.69 dscfm Conversion of Dry Flowrate to m3/hr = Q * 60 * 2.83168*10 -2 Where: Q – Volumetric Flowrate = 1769.69 dscfm 2.83168*10 -2 – Conversion factor for cubic feet to cubic meter 60 – Minutes in an hour = Q * 60 * 2.83168*10 -2 = 1769.69 *60 * 2.83168*10 -2 = 3006.72 m3/hr ASTM D 6348-03: Determination of NOx, CO and VOC Emissions From Stationary Sources NOx Emission Rate (g/Bhp-hr) = (Cd * 1.912*10 -3 * Q * T) / HP-hr Where: Cd – Measured NOx concentration in ppm = 72.89 ppm 1.92*10 -3 - Conversion constant for ppm to g/m3 NOx Q – Volumetric Flowrate = 3006.72 m3/hr T – Time in Hours of Test Run = 1 hr HP-hr – Unit Brake Horsepower = 1035.0 Bhp = (Cd * 1.912*10 -3 * Q * T) / HP-hr = (72.89 * 1.912*10 -3 * 3006.72 * 1) / 1035.0 = 0.40 g/Bhp-hr NOx Emission Rate (lbs/hr) = g/Bhp-hr / 454 * Bhp Where: g/Bhp-hr = 0.40 g/Bhp-hr 454 – Conversion factor for g to lbs Bhp - Unit Brake Horsepower = 1035.0 Bhp = g/Bhp-hr / 454 * Bhp = 0.40 / 454 * 1035.0 = 0.92 lbs/hr CO Emission Rate (g/Bhp-hr) = (Cd * 1.164*10 -3 * Q * T) / HP-hr Where: Cd – Measured CO concentration in ppm = 11.17 ppm 1.164*10 -3 - Conversion constant for ppm to g/m3 CO Q – Volumetric Flowrate = 3006.72 m3/hr T – Time in Hours of Test Run = 1 hr HP-hr – Unit Brake Horsepower = 1035.0 Bhp = (Cd * 1.164*10 -3 * Q * T) / HP-hr = (11.17 * 1.164*10 -3 * 3006.72 * 1) / 1035.0 = 0.04 g/Bhp-hr CO Emission Rate (lbs/hr) = g/Bhp-hr / 454 * Bhp Where: g/Bhp-hr = 0.04 g/Bhp-hr 454 – Conversion factor for g to lbs Bhp - Unit Brake Horsepower = 1035.0 Bhp = g/Bhp-hr / 454 * Bhp = 0.04 / 454 * 1035.0 = 0.09 lbs/hr VOC Emission Rate (g/Bhp-hr) = (Cd * 1.833*10 -3 * Q * T) / HP-hr Where: Cd – Measured VOC concentration in ppm = 66.43 ppm 1.833*10 -3 - Conversion constant for ppm to g/m3 VOC Q – Volumetric Flowrate = 3006.72 m3/hr T – Time in Hours of Test Run = 1 hr HP-hr – Unit Brake Horsepower = 1035.0 Bhp = (Cd * 1.833*10 -3 * Q * T) / HP-hr = (66.43 * 1.833*10 -3 * 3006.72 * 1) / 1035.0 = 0.35 g/Bhp-hr VOC Emission Rate (lbs/hr) = g/Bhp-hr / 454 * Bhp Where: g/Bhp-hr = 0.35 g/Bhp-hr 454 – Conversion factor for g to lbs Bhp - Unit Brake Horsepower = 1035.0 Bhp = g/Bhp-hr / 454 * Bhp = 0.35 / 454 * 1035.0 = 0.81 lbs/hr APPENDIX E FTIR Engine Test Sheet Company Name j)//J/~ 1RJe Location! Unit 1.0. A! JC,t,y)/kf/ ~S -:t:t ;$ Type of Test Completed 3-/A".. #?)/ Field Technician (s) TJ Schrnidtberuer Client Rep and/or State Rep Date 7-.16 ~ .23 Stack Diagram Jt:-:j."19Non-Resettable Run Time Hours C~fe.rr?; //c,rEnqine Make .en 5:"5-/{,::r -Encine Model .-....... #6'L-t// .J/;of-OZ5 b '1Engine SIN Verified: ' ..1--5'"Port Distance A T....... ." Port Distance B exhaust Diameter (inches) !---< !Calibration Gas INO (ppm) CO (ppm) t A']:'! /"J. s: . ConcentrationCviinder # .~tl 493.4CC453965 . ~ CC453965 520.2 495.6CC453965Propane (corn) 1 B'" 1143 ... jN02 (ppm) CC168787 101.9 lCC173895Ethylene (ppm) 499.4 "G""",F""""CC453965Methane (ppm) 196.7'CC321163Acetaldehyde (ppm) 01/24/2025 Test 1 Test 2 Test 3 I ime of Readinq Atm Pressure (in Hq)J Atm Temp CF) I. t:t:Zo' ;25'. :z."1 1-7 Aj,';( ! 2.~ . .,:i ~() /1,";... :.( 2S:7-{, X's Encine RPM /:;---.... /292. l;}.c;3 /2~X' *Manifoid Pres. Vac(") or Boost(p~ or Boost (psia) 3'2,/7 5'2.1 3/. 'i< Manifold Temp CF) Psuction (psi) Stage 1 Tsuction (OF) Staqe 1 I"'J.<:.'J ;;2<;' - /4/2s /'-1/ 7,::, --Pdischarge (psi) Stage 1 Psuction (psi) Stage 2 Tsuction p.) Stage 2 'J5cJTSC~arge (psi) Stage 2 (00 \. ./ »<. ,.L9S? lou \./, 2C; ry 7'51 , .... -~. ~3 Psuction (psi) Staqe 3 Tsuction CF) Stage 3 P_~~charge (psi) Stage 3 \. -/"'"7co / \/ .......... • s7 x.> »<. CJbC> !Psuction (psi) Staqe 4 I suction ('F) Stage 4 Pdischarge WSi) Stage 4 \Jas fhroug put (mmcfld) or ( ) li/A/ -';"71:7 2«{>< :2'Xh Pre Cat Temp ('F) ~3C7 7"3\ Post Cat Temp CF) ~;?o 62J.b)..S Cat Differe':!tiai Pres. (" of _H2O) Il/o 7IAJ..e-e, /VA. 77/F If f4 Humidity % .:L5t' ..:z~ /'/ 02% ~3 <;7.3 2 .J... C02 % Dry ~3 ;1. .3 7.l..J LOAD % (e-an~ or (Estimated) C34::1-=t5 ~5' :;~ Ignition Timinq CF) 2'1.7_ ~'f. I ;:LL.J.l l\FR setnno mV (Left Bank) AFR Setting mV (Right Bank) '3/.2.. r/. /.3/. 'j - Rev 8 • Some units show boost In inches of Hg. In this situation please indicate if It is positive (+) or negative(-) Eg: (+12") or (- 5") Worksheet: O2 Stratification Client:Uinta Wax Location:N Randlett #3 Date:7/25/2024 PD:13.5 DD:34 YES Method 1 Criteria Met UD:7.5 YES Method 1 Criteria Met Port Point Insertion Depth Reading (inches)(%) A 1 2.24 8.30 A 2 6.75 8.30 A 3 11.25 8.30 A 4 A 5 A 6 A 7 A 8 A 9 A 10 A 11 A 12 Average 8.30 Notes: To demonstrate non-stratified flow and utilize one sampling location O2 may not deviate by more than +/- 0.3% of the average O2 concentration. EPA REFERENCE METHOD 3A (Determination Of Stratification) COMPANY NAME:Uinta Wax COMPANY LOCATION:N Randlett #3 DATE:7/25/2024 STACK DIAMETER (inches):13.5 TRAVERSE POINTS:16 2 TEST RUN #1 TEST RUN #2 TEST RUN #3 AVERAGE O2:8.3 AVERAGE O2:8.3 AVERAGE O2:8.2 AVERAGE CO2:7.3 AVERAGE CO2:7.3 AVERAGE CO2:7.3 BARO PRESSURE:25.27 BARO PRESSURE:25.27 BARO PRESSURE:25.26 Point Insertion DepthDP (H2O)Ts (deg F)Stat P (H2O)Point Insertion DepthDP (H2O)Ts (deg F)Stat P (H2O)Point Insertion DepthDP (H2O)Ts (deg F)Stat P (H2O) 1 0.5 0.82 620 0.33 1 0.5 0.84 622 0.32 1 0.5 0.81 625 0.34 2 1.4175 0.85 2 1.4175 0.86 2 1.4175 0.85 3 2.619 0.84 3 2.619 0.87 3 2.619 0.89 4 4.3605 0.88 4 4.3605 0.89 4 4.3605 0.88 5 9.1395 0.81 5 9.1395 0.84 5 9.1395 0.87 6 10.881 0.89 6 10.881 0.85 6 10.881 0.84 7 12.0825 0.89 7 12.0825 0.84 7 12.0825 0.83 8 13 0.82 8 13 0.83 8 13 0.81 9 9 9 10 10 10 11 11 11 12 12 12 13 13 13 14 14 14 15 15 15 16 16 16 1 0.5 0.83 620 0.33 1 0.5 0.82 622 0.32 1 0.5 0.84 625 0.34 2 1.4175 0.85 2 1.4175 0.86 2 1.4175 0.87 3 2.619 0.86 3 2.619 0.89 3 2.619 0.88 4 4.3605 0.85 4 4.3605 0.89 4 4.3605 0.88 5 9.1395 0.84 5 9.1395 0.85 5 9.1395 0.84 6 10.881 0.87 6 10.881 0.87 6 10.881 0.85 7 12.0825 0.88 7 12.0825 0.82 7 12.0825 0.82 8 13 0.82 8 13 0.79 8 13 0.81 9 9 9 10 10 10 11 11 11 12 12 12 13 13 13 14 14 14 15 15 15 16 16 16 From:Kaitlin Meszaros To:Dylan Frederick; Alan Humpherys Cc:Rik Ombach; Kyle Greenberg; Karen Pratt; Josh Morgan Subject:[EXTERNAL] Follow-up to Uinta Wax meeting on proposed BACT for North Randlett Compressor Station Date:Tuesday, August 13, 2024 8:26:35 AM Attachments:image001.pngimage002.pngimage003.pngimage004.png Good morning, Dylan and Alan, We appreciate you taking time to meet with us on August 2, 2024, to discuss the engine ppm limits that were placed into the permit on 02/18/2019. As we mentioned, our literature review resulted in 4 separate UDAQ BACT analyses provided to the original applicant (Crescent Point) by Spencer Nelson dated 09/08/2018, 11/27/2018, 12/07/2018 and 02/18/2019. Each of these BACT analysis included a lb/hr and g/bhp-hr limit, which are appropriate BACT for the compressor engines at North Randlett. It is unclear under what circumstance the ppm limits were added to the permit nor the calculation method from which the specific ppm limits in the permit were generated. Based on correspondence with experts in the stack testing field and the engine leasing field, the ppm numbers in the permit are not equal to the engine make/model pedigree for the guaranteed catalyst outlet emissions rates. Without these data deriving the ppm limits UDAQ has placed in the permit, the ppm limits have no justification or basis for inclusion. As noted in each of the 4 separate UDAQ BACT analysis, mass emission limits (lb/hr, tons/yr, g/bhp-hr) represent a complete measurement of all the engine’s operational attributes and combined stack flow rate. Mass emission rates are used in dispersion modeling and other SIP plans making a 1:1 compliance comparison with state plans, NAAQS evaluations, and increment consumption. Concentration limits (ppm) only represent the amount of pollution in a fixed volume of gas. These values only represent part of the emissions picture as they exist independent of stack flow rates. For example, 100 ppm in a stack exhaust flow rate of 10,000 acfm has a lower emissions rate than the same 100 ppm in a stack exhaust flow rate of 100,000 acfm because the total gas out of the 100,000 acfm stack is higher and therefore the 100 ppm has more mass than the same 100 ppm in the lower exhaust flow. PPM concentrations out of a stack cannot be compared without additional information (namely stack flow rates), to state plan limits, NAAQS thresholds, and increment values. Per our discussion on August 2, 2024, including both a g/bhp-hr and lb/hr limit in the permit provides unique and effective NSR and BACT protections from an emission limit standpoint. A g/bhp-hr limit sets compliance expectations independent of compression output or load. A lb/hr limit sets compliance expectations incorporating of the power output of the engine and limits the mass emissions to the atmosphere. A limit of 0.5 g NOx/bhp-hr and 1.52 lb NOx/hr can be proposed as BACT for a 1,380-horsepower engine. During emission stack testing, it is possible, should the engine’s normal operating load not be 100%, that the test rate could be 0.7 g NOx/bhp-hr and be less than the lb NOx/hr limit. For example, 0.7 g NOx/bhp-hr * 1380 hp * 70% /453.6 g/lb = 1.49 lb NOx/hr. This in turn means that compliance with one limit does not necessarily mean compliance with the other making the g/bhp-hr and lb/hr limits not equal. Including both limits provides a multi-layer approach to emission limitations for the engine. Therefore, we request a g/bhp-hr and lb/hr limit are used as BACT thresholds for the compressor engines at the North Randlett Compressor Station, rather than lb/hr and ppm limits. Let us know if you have any questions or would like to discuss. Thank you, Kaitlin Meszaros Air Quality & Noise Specialist 3222 S Vance St Suite 200 Lakewood, CO 80227 P: 303.980.5200 | D: 720.614.5598 E: meszaros@pinyon-env.com asdfrewq CAUTION: This email originated from outside of the organization. Do not click links or open attachments unless you recognize the sender and know that the content is safe. If you believe that this email is suspicious, please forward it to support@fluiditservices.com. Source Test Report For Uinta Wax Operating, LLC North Randlett Compressor Station Uintah County, Utah Test Date: June 20, 2024 Report Date: July 24, 2024 UDEQ Permit: #DAQE-AN159380002-23 Engine: Caterpillar G3516B SN: N6W/JEF02569 Unit ID: #3 Prepared By: Oasis Emission Consultants, Inc. 2730 Commercial Way Rock Springs, WY 82901 July 24, 2024 Ms. Karen Pratt Uinta Wax Operating, LLC Dear Ms. Pratt: Re: Engine Emission Testing For Uinta Wax Operating, LLC, North Randlett Compressor Station, Unit #3, Permit #DAQE-AN159380002-23. An air emissions test program was conducted on a Caterpillar G3516B engine, operated by Uinta Wax Operating, LLC and designated as Unit #3, located at the North Randlett Compressor Station in Uintah County, Utah. The purpose of the testing was to demonstrate annual compliance with the emissions limits contained in UDEQ Permit #DAQE- AN159380002-23 and EPA 40 CFR 60, Subpart JJJJ, for oxides of nitrogen (NOx), carbon monoxide (CO) and volatile organic compounds (VOC). Oasis Emission Consultants, Inc. conducted the testing on June 20, 2024. UDEQ Permit #DAQE-AN159380002-23 Emission Levels The average recorded levels were found to comply with emission levels stipulated in the permit, as shown in the attached report and summarized below. The average recorded level for NOx ppm@15% O2 were found to be non-compliant with emission levels stipulated in the permit. Emission Unit Avg NOx Permit NOx Avg CO Permit CO Avg NMNEHC* Permit VOC ppm @ 15% O2 44.54 41 53.00 61 38.94 60 lbs/hr 1.19 1.52 0.86 1.37 1.00 2.13 *VOC levels reported as non-methane, non-ethane hydrocarbon on a propane basis (NMNEHC C3). EPA 40 CFR 60, Subpart JJJJ Emission Levels Emission Unit Avg NOx Permit NOx Avg CO Permit CO Avg NMNEHC* Permit VOC g/bhp-hr 0.57 1.0 0.41 2.0 0.48 0.7 Catalyst Parameters (Averaged Over 3 Test Runs) Inlet Temp (deg F) DP (in H2O) 912 6.7 Engine Load (Averaged Over 3 Test Runs) Rated BHP Operating BHP % Load 1380 947.6 68.7 Testing Protocol The attached report was generated using an extractive FTIR system using methodologies as required by and in accordance with EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320, as outlined in the submitted Source Test Protocol. Quality Assurance Oasis has performed a full review of the raw data and calculated results in this report. Any errors we have encountered have been listed in the body of this report. After performing the review, we are confident that this engine has met all requirements. If you have any questions or require further information, please contact the undersigned at (307) 382-3297. Yours truly, Oasis Emission Consultants, Inc. _________________________ _______________________ Charles A. Chapman Crystal Leonard Manager of Technical Services Senior EHS Specialist _________________________ Christopher N. Knott, P.Eng. Director, Engineering and Operations SOURCE EMISSION TEST REPORT UDEQ Permit #DAQE-AN159380002-23 Test Performed By: Oasis Emission Consultants, Inc. Test Company Contact: Chris Knott 2730 Commercial Way Rock Springs, WY 82901 307.382.3297 Owner/Operator: Uinta Wax Operating, LLC Owner/Operator Contact: Karen Pratt (720) 990-9927 Facility Name: North Randlett Compressor Station UTM Coordinates: 593,702 m Easting, 4,453,005 m Northing UTM Zone 12 Uintah County, Utah Emission Source: Caterpillar G3516B Unit #3 Date of Test: June 20, 2024 Date of Report: July 24, 2024 TABLE OF CONTENTS 1.1 Introduction .......................................................................................................................... 1 2.1 Stack Sampling Location ..................................................................................................... 2 3.1 Discussion of NOx, CO and VOC Test Results ................................................................... 3 3.1.1 Source Test 1 ............................................................................................................................................ 3 3.1.2 Source Test 2 ............................................................................................................................................ 3 3.1.3 Source Test 3 ............................................................................................................................................ 3 4.1 Stack Sampling Methods and Procedures ............................................................................ 4 4.2 Equipment Utilization .......................................................................................................... 5 4.3 Measurement of VOC (NMNEHC C3) ............................................................................... 6 4.4 Process Parameters............................................................................................................... 6 5.1 Quality Assurance ................................................................................................................ 7 List of Tables and Figures Figure 1 - Sample Port Location ............................................................................................................................. 2 Figure 2 - Sampling Train Schematic-Method 320 ................................................................................................ 5 Table 1 - Insertion Depths of Traverse Points for Stratification Test ..................................................................... 2 Table 2 - Test Matrix .............................................................................................................................................. 4 Table 3 - Concentrations and Interference .............................................................................................................. 5 APPENDIX A: NOx, CO and VOC Test Data APPENDIX B: Quality Assurance/Calibration Data APPENDIX C: Load Approximation APPENDIX D: Example Calculations and Summary APPENDIX E: Field Notes 1 1.1 Introduction An air emissions test program was conducted on a Caterpillar G3516B engine, operated by Uinta Wax Operating, LLC and designated as Unit #3, located at the North Randlett Compressor Station in Uintah County, Utah. The purpose of the testing was to demonstrate annual compliance with the emissions limits contained in UDEQ Permit #DAQE- AN159380002-23 and EPA 40 CFR 60, Subpart JJJJ, for oxides of nitrogen (NOx), carbon monoxide (CO) and volatile organic compounds (VOC) defined as non-methane, non-ethane hydrocarbons, reported as propane (NMNEHC C3). The facility is located five (5) miles west of Randlett, in Uintah County, Utah. Three one hour test runs were performed on June 20, 2024 to analyze NOx, CO and VOC emission levels. Test runs were performed according to methodologies outlined by EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320 as outlined in the submitted Source Test Protocol dated May 17, 2024. Each one hour test run consisted of 60 readings taken at one minute intervals. Process parameters were recorded during each test run in order to determine the load. Parameters include the engine panel load percent reading. The following key personnel were present during testing: David Martinez, OEC Kyle John 2 2.1 Stack Sampling Location The facility is located five (5) miles west of Randlett, in Uintah County, Utah. Testing was conducted on the Caterpillar G3516B engine. The sampling port for moisture, NOx, CO and VOC measurements was approximately 2.5 pipe diameters (34”) downstream from the nearest flow disturbance (Distance B) and 0.6 pipe diameters (7.5”) upstream from the nearest disturbance (Distance A), as seen in Figure 1. The stack sampling location was placed at approximately 50% insertion depth based on an O2 stratification check which demonstrated a non-stratified flow regime. The stratification was conducted according to EPA 40 CFR 75(A), §6.5.6.1 using 3 traverse points determined according to Table 1 below. Figure 1 - Sample Port Location Table 1 - Insertion Depths of Traverse Points for Stratification Test Traverse Point Insertion Depth (Percent of Stack Diameter) 1 16.6 2 50.0 3 83.3 13.5" A B Oxidation Catalyst 3 3.1 Discussion of NOx, CO and VOC Test Results Three, one hour test runs were performed on June 20, 2024 to analyze exhaust NOx, CO and VOC (NMNEHC C3) emission levels to demonstrate annual compliance with the emissions limits contained in the WDEQ Permit #DAQE-AN159380002-23 and EPA 40 CFR 60, Subpart JJJJ. Testing for NOx, CO and VOC were run concurrently with one another. Each test was performed at the maximum achievable load. Measured emissions were below permitted limits. Please refer to the Appendices for a listing of all raw data, calibration error response and calculations performed per EPA 40 CFR 60(A) requirements. 3.1.1 Source Test 1: Caterpillar G3516B, NOx, CO and VOC The first test was performed from 11:52 to 12:51 for NOx, CO and VOC. Based on operating parameters recorded during testing, the load was approximated at 938.4 bhp, and the average NOx and CO levels were found to be 0.58 g/bhp-hr and 0.42 g/bhp-hr respectively, below limitations. The VOC level tested at 0.52 g/bhp- hr, which tested in compliance. 3.1.2 Source Test 2: Caterpillar G3516B, NOx, CO and VOC The second test was performed from 12:53 to 13:52 for NOx, CO and VOC. Based on operating parameters recorded during testing, the load was approximated at 952.2 bhp, and the average NOx and CO levels were found to be 0.52 g/bhp-hr and 0.41 g/bhp-hr respectively, below limitations. The VOC level tested at 0.48 g/bhp- hr, which tested in compliance. 3.1.3 Source Test 3: Caterpillar G3516B, NOx, CO and VOC The third test was performed from 13:54 to 14:53 for NOx, CO and VOC. Based on operating parameters recorded during testing, the load was approximated at 952.2 bhp, and the average NOx and CO levels were found to be 0.62 g/bhp-hr and 0.42 g/bhp-hr respectively, below limitations. The VOC level tested at 0.45 g/bhp- hr, which tested in compliance. Test Run NOx (ppmvd) NOx (g/bhp-hr) CO (ppmvd) CO (g/bhp-hr) VOC (ppmvd) VOC (g/bhp-hr) O2 (%) 1 107.90 0.58 127.57 0.42 100.84 0.52 6.0 Test Run NOx (ppmvd) NOx (g/bhp-hr) CO (ppmvd) CO (g/bhp-hr) VOC (ppmvd) VOC (g/bhp-hr) O2 (%) 2 103.59 0.52 132.81 0.41 99.33 0.48 6.0 Test Run NOx (ppmvd) NOx (g/bhp-hr) CO (ppmvd) CO (g/bhp-hr) VOC (ppmvd) VOC (g/bhp-hr) O2 (%) 3 125.94 0.62 141.15 0.42 94.85 0.45 6.0 4 4.1 Stack Sampling Methods and Procedures Testing followed EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320, with no exceptions. Table 2 - Test Matrix Method Title Parameter Reference EPA 40 CFR 60 Appendix A, Method 1 Sample and Velocity Traverses for Stationary Sources Sampling Point Determination https://www.epa.gov/ sites/production/files/ 2017- 08/documents/metho d_1_3.pdf EPA 40 CFR 60 Appendix A, Method 2 Determination of Stack Gas Velocity and Volumetric Flow Rate Exhaust Effluent Flow https://www.epa.gov/ sites/production/files/ 2017- 08/documents/metho d_2.pdf EPA 40 CFR 60 Appendix A, Method 3 Gas Analysis for the Determination of Dry Molecular Weight O2, CO2, Dry Volumetric Flow Rate https://www.epa.gov/ sites/production/files/ 2017- 08/documents/metho d_3.pdf EPA 40 CFR 63 Appendix A, EPA Method 320 Vapor Phase Organic and Inorganic Emissions by Extractive FTIR Nitrogen Oxides, Carbon Monoxide, Non- Methane Non- Ethane Hydrocarbons on a Propane Basis https://www.epa.gov/ emc/method-320- vapor-phase-organic- and-inorganic- emissions-extractive- ftir United States. U.S. Environmental Protection Agency. “EMC Promulgated Test Methods.” Air Emission Measurement Center (EMC). 31 August 2023. Web. 2 July 2024. <https://www.epa.gov/emc/emc-promulgated-test-methods>. ASTM International. “Standards & Publications.” All Environment Standards. Web. 2 July 2024. <https://www.astm.org/Standards/D6348.htm>. 5 4.2 Equipment Utilization The following equipment was used during the tests performed at this facility in conjunction with procedures outlined by EPA 40 CFR 60(A) Methods 1-3 & EPA 40 CFR 63(A), Method 320. • (1) MKS MultiGas 2030 FTIR Continuous Gas Analyzer (0.210 L/min sample flow, 0.014 atmosphere sample pressure, 1 atmosphere cell pressure, 191°C cell temperature) • (1) Laptop Computer for the FTIR Analyzer using MKS MG2000 Software • (1) 75ft or 100ft Heated Teflon Line w/ Heated Sample Probe and Spike Bypass Line • S-Type Pitot Tube c/w 20 ft. Heated Sample Line (coefficient 0.84) • (1) Enerac 500 Portable O2/CO2 Analyzer • (1) Fyrite O2/CO2 Analyzer • (5) EPA Protocol G1 Calibration Gas (NOx, CO, C3H8, C2H4 and NO2) The MKS Multigas 2030 FTIR Analyzer operated with a spectral resolution of 0.5 cm-1 and a scan time of 30 seconds. The FTIR spectrometer utilizes a multi-pass gas cell with a 5.11 meter effective pathlength. Figure 2 - Sampling Train Schematic-Method 320 Table 3 - Concentrations and Interference 6 The MKS 2030 software provides a Natural Gas Method that is designed to minimize all expected interferences by removing the regions in the quant region where they are most absorbed (i.e. picket fence approach). So, for example, all the water peaks that are greater than about 0.1 abs are removed from the quant region. Since the spectral noise measured (sample spectrum) is in the range of 0.001 absorbance, it is desirable to have any error within this range. The MKS software will match the water calibration spectrum to the sample spectrum at any 1 point in the spectrum to about 1% precision. So, 1% of 0.1 absorbance is 0.001 abs. This is why any peaks greater than this for interfering compounds are usually excluded so they do not interfere. To summarize, the MKS software and the method are designed to minimize any interferences by removing their largest interfering absorptions. 4.3 Measurement of VOC (NMNEHC C3) The algorithm currently used for NMNEHC C3 and developed for natural gas fired applications by Dr. Spartz and MKS instruments in accordance with EPA standards, is the following: (2.4*c8/(1+exp((2-c8)/0.2))+1.9*c11/(1+exp((2-c11)/0.2))+6*c12/(1+exp((0.5-c12) /0.2))+2.85*c13/(1+exp((2-c13)/0.2))+3*c14/(1+exp((1-c14)/0.2)))/3 c8= acetylene c11= ethylene c12= hexane c13= propylene c14= propane Note: The constants in front of each of the compounds listed represents the FID response factor when calibrated with Propane. As with any CEMS analyzer, the FTIR may demonstrate a negative zero bias. The “exp” functions listed in the algorithm above are intended to mathematically filter out any negative biases and set them to approach zero. 4.4 Process Parameters Process parameters were recorded during each test run in order to determine the load. Parameters include the engine panel load percent reading. Results are provided in Appendix C. 7 5.1 Quality Assurance The MKS Multigas 2030 FTIR Analyzer was used to measure NOx, CO and VOC on a dry basis. A pre Direct and System calibration measurement was made on compounds of NOx, CO, C3H8 and C2H4. In addition, post System calibrations were made on compounds of NOx, CO, C3H8 and C2H4. Compounds of CO2 and C3H8 were measured for the quality assurance spiking requirements. Levels for calibrations and zeroes must be within +/- 5% of the certified calibration gas or response to zero gas, respectively. CTS procedures were followed according to EPA requirements for both pre and post testing. Similarly, QA spiking procedures were followed. Analysis of the CO2 exhaust effluent was used to determine the dilution factor. Steady levels of the CO2 were observed and a sufficient duration of time was allowed to elapse for a representative average. The calibration gas was spiked into the effluent stream using a bypass line at approximately 10% of the sampling rate. The dilution factor was obtained from observation of the stack CO2 behavior using the following equation: CO2AVG – CO2SPIKE DF = ------------------------ CO2 AVG Where: CO2AVG = The average undiluted CO2 stack gas concentration of spike measurements CO2SPIKE = The average diluted CO2 stack gas concentration when spiked The sample recovery was then obtained from the following equation: % REC = (Spike MEAS – Stack MEAS)* (1 – DF) --------------------------------------------------------- CS * DF Where: Spike MEAS = The average diluted stack gas concentration when spiked Stack MEAS = The average undiluted stack gas concentration DF = Dilution factor CS = Certified concentration of calibration standards The Sample Recovery average level for C3H8 was found to be 83.6%, which was within the allowable tolerance of Method 320 (70% to 130%). A summary of all spiking procedures/results can be found in Appendix B. APPENDIX A NO Dry (ppm) NO2 Dry (ppm) NOx Dry (ppm) CO Dry (ppm) NMNEHC C3 Dry (ppm) H2O% (High) 191C Time 1 92.689169 16.00645 108.695619 128.676058 101.440401 11.203826 11:52:39 06/20/2024 2 91.970828 15.948155 107.918983 128.648014 100.234820 11.226931 11:53:39 06/20/2024 3 91.63064 16.096632 107.727272 128.576853 100.438803 11.227104 11:54:39 06/20/2024 4 91.071615 16.179072 107.250687 128.49718 101.253560 11.243336 11:55:39 06/20/2024 5 91.989683 16.269161 108.258844 128.05215 101.481788 11.22215 11:56:39 06/20/2024 6 91.59807 16.158855 107.756925 127.548723 101.186699 11.243346 11:57:40 06/20/2024 7 91.871254 16.328323 108.199577 127.284736 100.229626 11.270435 11:58:39 06/20/2024 8 90.886889 16.305018 107.191907 127.439996 101.980683 11.290885 11:59:39 06/20/2024 9 92.080309 16.437213 108.517522 127.766722 99.883727 11.29068 12:00:39 06/20/2024 10 90.758453 16.243039 107.001492 127.854861 101.618574 11.297466 12:01:40 06/20/2024 11 90.828445 16.383933 107.212378 127.671828 100.852467 11.308071 12:02:40 06/20/2024 12 91.74088 16.408139 108.149019 127.552234 100.219300 11.292946 12:03:40 06/20/2024 13 92.393295 16.464719 108.858014 127.218051 100.984056 11.323686 12:04:40 06/20/2024 14 93.083677 16.593183 109.67686 127.61055 100.607968 11.318372 12:05:40 06/20/2024 15 92.656944 16.587962 109.244906 127.950874 100.364020 11.344246 12:06:40 06/20/2024 16 93.717219 16.793078 110.510297 128.198452 100.522585 11.309721 12:07:40 06/20/2024 17 91.541611 16.629812 108.171423 128.056979 101.361110 11.323959 12:08:40 06/20/2024 18 92.289754 16.67196 108.961714 128.015531 100.567424 11.335912 12:09:41 06/20/2024 19 92.402705 16.54614 108.948845 127.852839 101.987901 11.299067 12:10:40 06/20/2024 20 88.978758 16.085107 105.063865 126.650613 101.287156 11.287 12:11:40 06/20/2024 21 92.145119 16.419134 108.564253 127.751039 101.395023 11.323609 12:12:41 06/20/2024 22 90.702784 16.372521 107.075305 127.282215 101.221838 11.317367 12:13:41 06/20/2024 23 93.198455 16.845604 110.044059 127.973884 101.008274 11.304378 12:14:41 06/20/2024 24 90.805255 16.635471 107.440726 127.315538 100.659598 11.295408 12:15:41 06/20/2024 25 91.277212 16.576048 107.85326 126.899272 100.776145 11.30798 12:16:41 06/20/2024 26 92.54068 16.600318 109.140998 127.018037 101.570088 11.339417 12:17:41 06/20/2024 27 89.881943 16.303244 106.185187 126.705884 101.590970 11.32096 12:18:41 06/20/2024 28 90.236419 16.448732 106.685151 127.085822 101.098208 11.351507 12:19:41 06/20/2024 29 91.649314 16.75089 108.400204 127.735032 100.080139 11.356529 12:20:41 06/20/2024 30 91.97781 16.815311 108.793121 127.856897 100.590332 11.354472 12:21:42 06/20/2024 31 91.103494 16.772576 107.87607 127.701704 101.766318 11.364815 12:22:41 06/20/2024 32 91.314347 16.635085 107.949432 128.154317 101.056052 11.360884 12:23:41 06/20/2024 33 91.52 16.530024 108.050024 127.962963 101.526326 11.34202 12:24:42 06/20/2024 34 89.090664 16.253839 105.344503 127.25061 103.100073 11.328733 12:25:42 06/20/2024 35 90.733586 16.531341 107.264927 127.8398 101.463696 11.364345 12:26:42 06/20/2024 36 91.060111 16.558008 107.618119 128.190145 100.571673 11.367088 12:27:42 06/20/2024 37 90.893278 16.699269 107.592547 128.108897 101.299201 11.368201 12:28:42 06/20/2024 38 92.255306 16.778455 109.033761 127.855721 100.876084 11.348249 12:29:42 06/20/2024 39 92.566937 16.748994 109.315931 127.331979 100.591147 11.340481 12:30:42 06/20/2024 40 91.716445 16.609677 108.326122 127.299974 100.893111 11.3683 12:31:42 06/20/2024 41 91.308894 16.64533 107.954224 127.201972 99.411231 11.347241 12:32:43 06/20/2024 42 92.009544 16.858874 108.868418 127.817426 101.509178 11.393986 12:33:42 06/20/2024 43 92.332839 16.998593 109.331432 127.844994 99.861402 11.374687 12:34:42 06/20/2024 44 90.416158 16.834139 107.250297 127.656955 99.414224 11.373093 12:35:43 06/20/2024 45 92.316628 16.918291 109.234919 127.630933 100.298085 11.378184 12:36:43 06/20/2024 46 93.514475 16.949078 110.463553 127.635552 100.662454 11.371181 12:37:43 06/20/2024 47 90.108022 16.551312 106.659334 126.342214 101.037156 11.334088 12:38:43 06/20/2024 48 91.106442 16.840115 107.946557 127.141793 99.245339 11.355278 12:39:43 06/20/2024 49 91.49777 16.986106 108.483876 127.474672 100.430832 11.313656 12:40:43 06/20/2024 50 90.153525 16.889067 107.042592 127.518814 100.564244 11.347977 12:41:43 06/20/2024 51 92.165413 17.10706 109.272473 127.613034 100.721349 11.336021 12:42:43 06/20/2024 52 92.322118 16.995137 109.317255 127.181621 101.125490 11.305742 12:43:43 06/20/2024 53 90.72386 16.592592 107.316452 126.458217 99.721983 11.312989 12:44:43 06/20/2024 54 91.142697 16.801018 107.943715 127.132899 100.482833 11.311667 12:45:43 06/20/2024 55 92.855847 17.008718 109.864565 128.03256 99.728635 11.333545 12:46:44 06/20/2024 56 87.837616 16.461174 104.29879 127.32038 102.063840 11.318905 12:47:44 06/20/2024 57 81.995223 15.715733 97.710956 126.211186 102.171723 11.327995 12:48:44 06/20/2024 58 90.064654 16.701771 106.766425 127.491011 100.579011 11.380205 12:49:44 06/20/2024 59 90.771452 16.660059 107.431511 126.943699 99.737524 11.378072 12:50:44 06/20/2024 60 92.055366 16.832312 108.887678 127.064171 99.770640 11.38236 12:51:44 06/20/2024 AVG 91.33 0.00 107.90 127.57 100.84 11.32 ppm@15% O2 42.72 50.51 39.93 NOx (g/bhp-hr) NOx (lbs/hr) CO (g/bhp-hr) CO (lbs/hr) NMNEHC C3 (g/bhp-hr) NMNEHC C3 (lbs/hr) 0.58 1.19 0.42 0.86 0.52 1.07 #3 FTIR Measurements Calculated Emission Levels Uinta Wax Operating, LLC North Randlett Compressor Station Run 1 Record Date EPA REFERENCE METHOD 1 EPA REFERENCE METHOD 2 Stack Diameter 13.5 Inches Kp=85.49 ft/sec Cp=0.84 Traverse Points 16 Port Point Insertion Depth dP Ts Stat P sqrt dP Ports 2 (inches)(in h2O)(deg R)(in H2O) EPA REFERENCE METHOD 3 A 1 0.50 0.79 1424 0.3 0.889 Average O2 6.0 (% dry)A 2 1.42 0.82 0.906 Average CO2 7.1 (% dry)A 3 2.62 0.85 0.922 Average N2 + CO 86.9 (% dry)A 4 4.36 0.89 0.943 Dry Molecular Weight 29.38 lb/lbmol A 5 9.14 0.88 0.938 Wet Molecular Weight 28.09 lb/lbmol A 6 10.88 0.88 0.938 EPA REFERENCE METHOD 320 A 7 12.08 0.86 0.927 Barometric Pressure 24.91 in Hg A 8 13.00 0.87 0.933 Moisture Content 11.32 %A 9 EPA REFERENCE METHOD 320 A 10 Average Analyzer NOx Level 107.90 ppm A 11 Calculated NOx Mass Output 1.19 lbs/hr A 12 Calculated NOx Output 0.58 g/bhp-hr A 13 EPA REFERENCE METHOD 320 A 14 Average Analyzer CO Level 127.57 ppm A 15 Calculated CO Mass Output 0.86 lbs/hr A 16 Calculated CO Output 0.42 g/bhp-hr B 1 0.50 0.81 1424 0.3 0.900 EPA REFERENCE METHOD 320 B 2 1.42 0.82 0.906 Average Analyzer NMNEHC Level 100.84 ppm B 3 2.62 0.84 0.917 Calculated NMNEHC Mass Output 1.07 lbs/hr B 4 4.36 0.88 0.938 Calculated NMNEHC Output 0.52 g/bhp-hr B 5 9.14 0.89 0.943 LOAD APPROXIMATION B 6 10.88 0.87 0.933 Estimated Engine Load 938.4 BHP B 7 12.08 0.85 0.922 B 8 13.00 0.86 0.927 B 9 B 10 B 11 B 12 B 13 B 14 B 15 B 16 Averages 0.9 1424 0.3 0.924 Average Stack Gas Velocity 94.60 ft/sec Average Dry Flowrate 1545.91 dscfm TEST RUN # 1 NO Dry (ppm) NO2 Dry (ppm) NOx Dry (ppm) CO Dry (ppm) NMNEHC C3 Dry (ppm) H2O% (High) 191C Time 1 93.905581 17.313746 111.219327 127.695835 99.447504 11.394739 12:53:44 06/20/2024 2 89.854348 16.852355 106.706703 126.91472 99.403191 11.401773 12:54:45 06/20/2024 3 91.087466 16.960755 108.048221 127.431383 98.671298 11.402495 12:55:44 06/20/2024 4 91.699465 16.857985 108.55745 126.47626 98.499621 11.401337 12:56:45 06/20/2024 5 91.25291 16.767412 108.020322 126.133711 99.864014 11.416597 12:57:45 06/20/2024 6 90.968294 16.805875 107.774169 125.843728 98.743982 11.425033 12:58:45 06/20/2024 7 92.315008 16.998293 109.313301 126.484599 97.895820 11.461848 12:59:45 06/20/2024 8 92.069942 17.118885 109.188827 126.535604 98.030618 11.443673 13:00:45 06/20/2024 9 93.803076 17.375567 111.178643 127.269528 98.427086 11.471355 13:01:45 06/20/2024 10 102.534092 18.399479 120.933571 129.355129 95.829942 11.497935 13:02:45 06/20/2024 11 86.014748 16.368408 102.383156 125.650566 99.675677 11.401323 13:03:45 06/20/2024 12 88.319485 16.579324 104.898809 126.372877 99.928233 11.419645 13:04:45 06/20/2024 13 98.741187 17.844582 116.585769 128.925419 98.956748 11.483079 13:05:46 06/20/2024 14 87.118257 16.651458 103.769715 126.290322 100.970435 11.437999 13:06:45 06/20/2024 15 90.225438 17.073238 107.298676 127.636043 99.266852 11.463248 13:07:45 06/20/2024 16 91.798547 17.148742 108.947289 127.734396 99.705455 11.453998 13:08:45 06/20/2024 17 91.788139 17.006261 108.7944 127.200513 98.722584 11.449862 13:09:46 06/20/2024 18 91.308025 16.76771 108.075735 126.716426 99.681623 11.46433 13:10:46 06/20/2024 19 92.709801 16.964292 109.674093 127.285181 99.398911 11.484397 13:11:46 06/20/2024 20 92.437367 17.086333 109.5237 127.323419 98.892296 11.487591 13:12:46 06/20/2024 21 91.342295 17.195338 108.537633 127.728396 99.123048 11.474194 13:13:46 06/20/2024 22 91.384908 17.450774 108.835682 128.171442 99.312124 11.4838 13:14:46 06/20/2024 23 91.926807 17.405326 109.332133 127.768483 100.609813 11.478809 13:15:46 06/20/2024 24 92.939408 17.491663 110.431071 127.468727 98.356130 11.508743 13:16:46 06/20/2024 25 87.33164 16.711183 104.042823 125.873841 101.638369 11.507045 13:17:46 06/20/2024 26 76.692001 15.449413 92.141414 124.030187 102.303208 11.421202 13:18:47 06/20/2024 27 78.61158 15.656126 94.267706 124.533461 101.897035 11.456657 13:19:47 06/20/2024 28 74.352613 15.185549 89.538162 123.980156 102.698347 11.408007 13:20:47 06/20/2024 29 74.29608 15.074723 89.370803 124.364685 103.836131 11.411086 13:21:47 06/20/2024 30 66.891195 13.883939 80.775134 122.187821 105.434191 11.349935 13:22:47 06/20/2024 31 42.848793 12.390559 55.239352 117.330974 112.550394 11.167098 13:23:47 06/20/2024 32 36.561823 11.939483 48.501306 128.153045 113.976508 11.135953 13:24:47 06/20/2024 33 43.054207 11.667856 54.722063 134.255317 110.442769 11.16495 13:25:47 06/20/2024 34 46.797111 12.208847 59.005958 135.617312 108.416520 11.191174 13:26:47 06/20/2024 35 47.894606 12.516329 60.410935 136.539719 109.097499 11.23674 13:27:47 06/20/2024 36 45.107364 12.040462 57.147826 135.615857 108.403571 11.221515 13:28:47 06/20/2024 37 45.48503 12.106951 57.591981 135.468018 109.294933 11.23622 13:29:47 06/20/2024 38 47.132248 12.220169 59.352417 135.591236 106.037819 11.220103 13:30:48 06/20/2024 39 67.422657 15.396379 82.819036 141.125764 101.422600 11.343479 13:31:48 06/20/2024 40 93.094345 19.344451 112.438796 147.41122 95.373542 11.462235 13:32:48 06/20/2024 41 76.064879 17.145515 93.210394 142.999713 97.996112 11.399344 13:33:48 06/20/2024 42 75.013037 17.06393 92.076967 142.86915 99.049343 11.409865 13:34:48 06/20/2024 43 74.743827 17.087707 91.831534 142.925762 99.286418 11.423569 13:35:48 06/20/2024 44 75.672077 16.98106 92.653137 142.266924 97.364100 11.437915 13:36:48 06/20/2024 45 103.669316 20.094933 123.764249 144.081489 93.220219 11.582799 13:37:48 06/20/2024 46 106.534639 20.065575 126.600214 140.470174 92.214228 11.594752 13:38:48 06/20/2024 47 107.011065 20.40397 127.415035 140.645678 93.744693 11.575497 13:39:48 06/20/2024 48 108.061604 20.707007 128.768611 141.199414 93.875198 11.623214 13:40:48 06/20/2024 49 107.590917 20.652836 128.243753 141.067705 93.954953 11.610871 13:41:48 06/20/2024 50 106.105191 20.327628 126.432819 140.290175 93.556630 11.654497 13:42:48 06/20/2024 51 107.387505 20.248654 127.636159 140.460829 92.240575 11.668873 13:43:49 06/20/2024 52 105.226293 20.063192 125.289485 140.060739 93.324205 11.644833 13:44:49 06/20/2024 53 107.585815 20.520398 128.106213 141.003346 92.577359 11.658682 13:45:49 06/20/2024 54 106.891622 20.736304 127.627926 140.988293 93.667684 11.661676 13:46:49 06/20/2024 55 107.183553 20.70194 127.885493 140.969572 93.320557 11.673467 13:47:49 06/20/2024 56 105.370257 20.608456 125.978713 140.767773 94.295668 11.678963 13:48:49 06/20/2024 57 106.096318 20.666977 126.763295 140.316378 94.629259 11.673154 13:49:49 06/20/2024 58 106.158574 20.358228 126.516802 139.925796 93.092536 11.662031 13:50:50 06/20/2024 59 107.04447 20.631993 127.676463 140.274286 93.541257 11.658405 13:51:49 06/20/2024 60 104.96297 20.36553 125.3285 140.274828 94.356068 11.657501 13:52:49 06/20/2024 AVG 86.42 0.00 103.59 132.81 99.33 11.46 ppm@15% O2 41.02 52.59 39.33 NOx (g/bhp-hr) NOx (lbs/hr) CO (g/bhp-hr) CO (lbs/hr) NMNEHC C3 (g/bhp-hr) NMNEHC C3 (lbs/hr) 0.52 1.09 0.41 0.85 0.48 1.00 Calculated Emission Levels Record Date Uinta Wax Operating, LLC North Randlett Compressor Station Run 2 #3 FTIR Measurements EPA REFERENCE METHOD 1 EPA REFERENCE METHOD 2 Stack Diameter 13.5 Inches Kp=85.49 ft/sec Cp=0.84 Traverse Points 16 Port Point Insertion Depth dP Ts Stat P sqrt dP Ports 2 (inches)(in h2O)(deg R)(in H2O) EPA REFERENCE METHOD 3 A 1 0.50 0.73 1427 0.31 0.854 Average O2 6.0 (% dry)A 2 1.42 0.75 0.866 Average CO2 7.2 (% dry)A 3 2.62 0.78 0.883 Average N2 + CO 86.8 (% dry)A 4 4.36 0.81 0.900 Dry Molecular Weight 29.39 lb/lbmol A 5 9.14 0.84 0.917 Wet Molecular Weight 28.09 lb/lbmol A 6 10.88 0.79 0.889 EPA REFERENCE METHOD 320 A 7 12.08 0.76 0.872 Barometric Pressure 24.91 in Hg A 8 13.00 0.75 0.866 Moisture Content 11.46 %A 9 EPA REFERENCE METHOD 320 A 10 Average Analyzer NOx Level 103.59 ppm A 11 Calculated NOx Mass Output 1.09 lbs/hr A 12 Calculated NOx Output 0.52 g/bhp-hr A 13 EPA REFERENCE METHOD 320 A 14 Average Analyzer CO Level 132.81 ppm A 15 Calculated CO Mass Output 0.85 lbs/hr A 16 Calculated CO Output 0.41 g/bhp-hr B 1 0.50 0.71 1427 0.31 0.843 EPA REFERENCE METHOD 320 B 2 1.42 0.74 0.860 Average Analyzer NMNEHC Level 99.33 ppm B 3 2.62 0.78 0.883 Calculated NMNEHC Mass Output 1.00 lbs/hr B 4 4.36 0.82 0.906 Calculated NMNEHC Output 0.48 g/bhp-hr B 5 9.14 0.85 0.922 LOAD APPROXIMATION B 6 10.88 0.81 0.900 Estimated Engine Load 952.2 BHP B 7 12.08 0.77 0.877 B 8 13.00 0.74 0.860 B 9 B 10 B 11 B 12 B 13 B 14 B 15 B 16 Averages 0.8 1427 0.3 0.881 Average Stack Gas Velocity 90.33 ft/sec Average Dry Flowrate 1470.65 dscfm TEST RUN # 2 NO Dry (ppm) NO2 Dry (ppm) NOx Dry (ppm) CO Dry (ppm) NMNEHC C3 Dry (ppm) H2O% (High) 191C Time 1 104.24461 20.478542 124.723152 140.902279 94.835463 11.633347 13:54:50 06/20/2024 2 104.348929 20.284778 124.633707 140.453217 94.913914 11.622384 13:55:50 06/20/2024 3 105.337833 20.526758 125.864591 140.03632 95.895592 11.571835 13:56:50 06/20/2024 4 105.947009 20.524688 126.471697 139.882357 95.414431 11.571734 13:57:50 06/20/2024 5 102.461038 20.102557 122.563595 139.921047 95.016711 11.572313 13:58:50 06/20/2024 6 106.314101 20.639807 126.953908 140.863892 92.656443 11.661122 13:59:50 06/20/2024 7 107.471469 20.853173 128.324642 141.488812 93.358650 11.681174 14:00:50 06/20/2024 8 106.109359 20.726683 126.836042 141.040644 93.852401 11.66677 14:01:50 06/20/2024 9 105.36493 20.449669 125.814599 140.590062 93.523674 11.668075 14:02:50 06/20/2024 10 106.310107 20.483803 126.79391 140.198504 93.008149 11.672288 14:03:51 06/20/2024 11 106.33332 20.486604 126.819924 140.124628 92.552297 11.64262 14:04:51 06/20/2024 12 105.687876 20.519974 126.20785 140.385466 91.938047 11.648237 14:05:50 06/20/2024 13 105.189053 20.753425 125.942478 140.869524 94.877719 11.562293 14:06:51 06/20/2024 14 105.031292 20.723159 125.754451 141.362117 94.723392 11.579716 14:07:51 06/20/2024 15 104.118822 20.432044 124.550866 140.921851 94.398063 11.543187 14:08:51 06/20/2024 16 102.665005 20.199215 122.86422 140.302357 94.779749 11.540208 14:09:51 06/20/2024 17 104.287475 20.456115 124.74359 140.333891 95.230774 11.513663 14:10:51 06/20/2024 18 103.253368 20.338803 123.592171 140.250016 95.629705 11.492405 14:11:51 06/20/2024 19 103.077781 20.616787 123.694568 140.603236 94.733887 11.517755 14:12:51 06/20/2024 20 103.951633 20.748317 124.69995 140.794397 95.850543 11.493449 14:13:51 06/20/2024 21 101.980387 20.601778 122.582165 140.611291 95.923166 11.472801 14:14:52 06/20/2024 22 102.879401 20.630143 123.509544 140.627093 94.955966 11.401582 14:15:52 06/20/2024 23 102.355124 20.203035 122.558159 139.906633 95.186093 11.491855 14:16:51 06/20/2024 24 103.374028 20.400185 123.774213 140.274147 95.729324 11.592305 14:17:52 06/20/2024 25 104.293084 20.630865 124.923949 141.046213 96.284304 11.709814 14:18:52 06/20/2024 26 102.89476 20.414753 123.309513 141.31805 95.599585 11.685105 14:19:52 06/20/2024 27 105.107321 20.657214 125.764535 142.267654 95.581963 11.666792 14:20:52 06/20/2024 28 105.440883 20.497828 125.938711 141.718835 95.022387 11.604155 14:21:52 06/20/2024 29 103.461415 20.442887 123.904302 140.747735 95.935626 11.540144 14:22:52 06/20/2024 30 105.594064 20.660997 126.255061 140.798947 95.501837 11.531853 14:23:52 06/20/2024 31 105.750527 20.636617 126.387144 141.079544 95.311114 11.45835 14:24:53 06/20/2024 32 105.229359 20.669892 125.899251 141.544622 94.836038 11.568973 14:25:52 06/20/2024 33 106.471627 20.870005 127.341632 142.249468 94.943052 11.682828 14:26:52 06/20/2024 34 107.474861 20.94167 128.416531 141.846172 93.934629 11.613141 14:27:52 06/20/2024 35 106.368071 20.897085 127.265156 141.206889 94.837324 11.566105 14:28:53 06/20/2024 36 105.213114 20.544916 125.75803 140.617182 94.690897 11.572153 14:29:53 06/20/2024 37 106.57143 20.722128 127.293558 140.973021 94.813053 11.581017 14:30:53 06/20/2024 38 106.634436 20.844388 127.478824 141.649591 93.932195 11.594936 14:31:53 06/20/2024 39 106.118087 20.783855 126.901942 141.844644 95.746934 11.595327 14:32:53 06/20/2024 40 102.742426 20.482837 123.225263 141.312958 96.193412 11.577031 14:33:53 06/20/2024 41 103.864315 20.573571 124.437886 141.323551 96.056180 11.537657 14:34:53 06/20/2024 42 106.069771 20.756603 126.826374 141.541515 95.415113 11.578066 14:35:53 06/20/2024 43 106.719124 20.713294 127.432418 140.960335 95.406818 11.550905 14:36:53 06/20/2024 44 106.424595 20.823656 127.248251 140.96656 94.812677 11.559302 14:37:53 06/20/2024 45 105.641059 20.624191 126.26525 141.17123 94.634686 11.554797 14:38:53 06/20/2024 46 106.534606 21.003607 127.538213 141.934677 94.612894 11.57681 14:39:54 06/20/2024 47 105.672136 20.959594 126.63173 141.709467 94.527326 11.598559 14:40:54 06/20/2024 48 107.198206 21.01712 128.215326 141.475221 94.734514 11.59311 14:41:54 06/20/2024 49 105.79551 20.645327 126.440837 141.128856 95.013093 11.560792 14:42:54 06/20/2024 50 106.66767 20.793534 127.461204 141.45165 94.609639 11.574104 14:43:54 06/20/2024 51 105.975985 20.753344 126.729329 141.699164 96.104723 11.572228 14:44:54 06/20/2024 52 104.434668 20.776262 125.21093 141.762608 95.478412 11.564726 14:45:54 06/20/2024 53 105.099434 20.908338 126.007772 142.227444 95.884762 11.581191 14:46:54 06/20/2024 54 106.384785 20.95697 127.341755 142.418335 93.979116 11.604256 14:47:55 06/20/2024 55 106.94998 20.900514 127.850494 141.981549 94.223519 11.586507 14:48:55 06/20/2024 56 106.593268 20.779256 127.372524 141.695784 94.943137 11.62002 14:49:54 06/20/2024 57 107.830442 20.93302 128.763462 141.860446 94.833861 11.624359 14:50:54 06/20/2024 58 106.882588 20.998577 127.881165 142.096983 94.890558 11.619981 14:51:55 06/20/2024 59 107.721587 21.154973 128.87656 142.771277 93.440059 11.623284 14:52:55 06/20/2024 60 104.835978 20.85006 125.686038 142.017046 95.207896 11.639798 14:53:55 06/20/2024 AVG 105.28 20.66 125.94 141.15 94.85 11.58 ppm@15% O2 49.87 55.89 37.56 NOx (g/bhp-hr) NOx (lbs/hr) CO (g/bhp-hr) CO (lbs/hr) NMNEHC C3 (g/bhp-hr) NMNEHC C3 (lbs/hr) 0.62 1.29 0.42 0.88 0.45 0.93 FTIR Measurements #3 Calculated Emission Levels Uinta Wax Operating, LLC North Randlett Compressor Station Run 3 Record Date EPA REFERENCE METHOD 1 EPA REFERENCE METHOD 2 Stack Diameter 13.5 Inches Kp=85.49 ft/sec Cp=0.84 Traverse Points 16 Port Point Insertion Depth dP Ts Stat P sqrt dP Ports 2 (inches)(in h2O)(deg R)(in H2O) EPA REFERENCE METHOD 3 A 1 0.50 0.66 1432 0.29 0.812 Average O2 6.0 (% dry)A 2 1.42 0.70 0.837 Average CO2 7.2 (% dry)A 3 2.62 0.73 0.854 Average N2 + CO 86.8 (% dry)A 4 4.36 0.77 0.877 Dry Molecular Weight 29.39 lb/lbmol A 5 9.14 0.80 0.894 Wet Molecular Weight 28.07 lb/lbmol A 6 10.88 0.76 0.872 EPA REFERENCE METHOD 320 A 7 12.08 0.76 0.872 Barometric Pressure 24.91 in Hg A 8 13.00 0.72 0.849 Moisture Content 11.58 %A 9 EPA REFERENCE METHOD 320 A 10 Average Analyzer NOx Level 125.94 ppm A 11 Calculated NOx Mass Output 1.29 lbs/hr A 12 Calculated NOx Output 0.62 g/bhp-hr A 13 EPA REFERENCE METHOD 320 A 14 Average Analyzer CO Level 141.15 ppm A 15 Calculated CO Mass Output 0.88 lbs/hr A 16 Calculated CO Output 0.42 g/bhp-hr B 1 0.50 0.69 1432 0.29 0.831 EPA REFERENCE METHOD 320 B 2 1.42 0.72 0.849 Average Analyzer NMNEHC Level 94.85 ppm B 3 2.62 0.76 0.872 Calculated NMNEHC Mass Output 0.93 lbs/hr B 4 4.36 0.80 0.894 Calculated NMNEHC Output 0.45 g/bhp-hr B 5 9.14 0.83 0.911 LOAD APPROXIMATION B 6 10.88 0.78 0.883 Estimated Engine Load 952.2 BHP B 7 12.08 0.74 0.860 B 8 13.00 0.71 0.843 B 9 B 10 B 11 B 12 B 13 B 14 B 15 B 16 Averages 0.7 1432 0.3 0.863 Average Stack Gas Velocity 88.66 ft/sec Average Dry Flowrate 1436.40 dscfm TEST RUN # 3 APPENDIX B Date Time NO 191C span NO2 191C span H2O% (high) 191C Formaldehyde 191C Ethylene 191C TE span Propane 191C span Acetaldehyde 191C span CO ppm 191C (1of2) span CO ppm Dry CO2% 191C NOx Wet NOx Dry NM NE HC C3 Temp ( C )Pressure (atm) 6/20/2024 11:32:35 0.182914 -0.024404 0.006066 0.107092 1.00063 -0.460761 0.433238 -0.105383 -0.105389 -0.011882 0.15851 0.158519 0.834823 191.850967 0.992948 6/20/2024 11:32:43 0.08739 -0.067754 0.003622 0.100976 0.010762 -0.408351 -0.696483 0.11757 0.117574 -0.018462 0.019635 0.019636 0.05251 191.857025 0.996402 6/20/2024 11:32:50 0.246265 -0.129605 0.002949 0.03 0.776321 -2.088321 0.197708 -0.052693 -0.052694 -0.00152 0.11666 0.116663 2.631924 191.886093 0.993143 6/20/2024 11:32:57 0.062281 0.032139 0.004248 0.068565 0.350629 -0.241498 -0.109228 -0.014325 -0.014326 -0.010865 0.09442 0.094424 0.232529 191.857025 0.993556 6/20/2024 11:33:35 0 0 0 0 0 0 0 0 0 0 0 0 0 191.916489 0.993189 6/20/2024 11:33:49 -0.034813 0.076813 -0.001947 0.102995 1.191266 0.834743 -0.443761 0.099458 0.099456 0.012701 0.042 0.041999 1.280159 191.961197 0.993189 6/20/2024 11:33:56 0.017525 -0.012519 0.004217 0.004612 -0.669234 1.522345 -0.410264 -0.01529 -0.015291 -0.001023 0.005006 0.005006 1.406507 192.00238 0.997274 6/20/2024 11:34:04 0.101477 -0.060277 0.004834 0.08345 -0.53141 0.512231 -0.385813 -0.112278 -0.112284 0.006206 0.0412 0.041202 0.037848 192.00238 0.996402 6/20/2024 11:34:11 -0.174058 0.028948 0.001649 0.025963 0.849184 -0.254508 -0.760525 -0.076999 -0.077001 -0.001576 -0.14511 -0.145113 0.018195 192.00238 0.996172 6/20/2024 11:34:18 0.243706 0.003424 -0.000332 -0.018359 0.076942 -0.1626 0.594419 0.080921 0.080921 0.011452 0.247131 0.24713 0.017711 191.987854 0.995162 6/20/2024 11:34:26 -0.338938 -0.02969 0.002 0.06461 0.32824 -0.046315 0.897137 0.133968 0.133971 0.00292 -0.368628 -0.368635 0.013731 192.04599 0.999018 6/20/2024 11:34:34 -0.040287 -0.061358 0.010419 0.085338 0.882331 -0.765118 0.198714 -0.045343 -0.045348 -0.004149 -0.101645 -0.101656 0.056953 192.033264 0.994434 6/20/2024 11:34:41 0.266123 0.076829 -0.001742 -0.061049 0.098261 0.837339 -0.344879 -0.285171 -0.285166 0.014335 0.342951 0.342945 0.313458 192.031448 0.996815 6/20/2024 11:34:49 -0.094432 0.042848 -0.001567 -0.197853 -0.084103 0.509479 -0.147423 0.059537 0.059536 0.007694 -0.051584 -0.051583 0.034646 192.031448 0.993097 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm) 6/20/2024 11:35:20 517.793113 493.139057 497.934949 192.020554 1.002748 6/20/2024 11:38:46 98.286927 192.054474 0.991555 6/20/2024 11:35:27 516.487792 492.40244 493.677949 192.016922 1.005353 6/20/2024 11:38:53 97.888852 192.04599 0.991261 6/20/2024 11:35:35 517.13011 492.227465 492.860082 191.958771 1.007464 6/20/2024 11:39:01 97.84851 192.016922 0.990939 6/20/2024 11:35:42 515.775882 491.771662 492.202897 192.031448 1.008245 6/20/2024 11:39:08 98.143722 192.060532 0.993831 6/20/2024 11:35:50 518.24486 493.571703 494.02793 191.987854 1.005582 6/20/2024 11:39:16 99.487093 192.031448 0.988369 6/20/2024 11:35:57 519.309289 493.76369 499.473587 191.987854 1.005536 6/20/2024 11:39:23 98.724265 192.00238 0.990021 6/20/2024 11:36:04 518.583226 495.166045 496.240353 191.987854 1.003746 6/20/2024 11:39:31 97.703538 191.995117 0.99351 6/20/2024 11:36:12 519.221949 494.914484 493.393857 191.969681 1.003993 6/20/2024 11:39:38 97.339662 192.031448 0.992638 6/20/2024 11:36:20 519.479889 494.360945 493.977199 191.987854 1.003792 6/20/2024 11:39:46 98.474843 192.04599 0.990021 6/20/2024 11:36:27 519.389562 493.97972 496.424082 191.958771 1.00549 6/20/2024 11:39:53 97.774691 192.04599 0.991949 Date Time NO2 191C span Temp ( C )Pressure (atm) 6/20/2024 11:37:05 143.563831 192.054474 0.987646 6/20/2024 11:37:12 144.391491 192.04599 0.988185 6/20/2024 11:37:20 144.718527 192.031448 0.991536 6/20/2024 11:37:27 145.662326 192.031448 0.989103 6/20/2024 11:37:35 145.898468 192.060532 0.987543 6/20/2024 11:37:42 145.305228 192.04599 0.99122 6/20/2024 11:37:50 145.499802 192.016922 0.992684 6/20/2024 11:37:58 145.981364 192.075058 0.989975 6/20/2024 11:38:05 145.725922 192.0896 0.991674 6/20/2024 11:38:12 146.305998 192.075058 0.990297 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm) 6/20/2024 11:40:26 338.730281 282.461286 327.620041 192.088379 0.908334 6/20/2024 11:42:08 75.447492 192.181656 0.955782 6/20/2024 11:40:33 481.630705 473.556368 480.879078 192.133209 0.903358 6/20/2024 11:42:15 97.748354 192.205887 0.974093 6/20/2024 11:40:41 513.737577 490.823639 489.080567 192.162277 1.004802 6/20/2024 11:42:23 98.74989 192.133209 0.995438 6/20/2024 11:40:48 517.432805 493.825272 494.784128 192.104126 1.009163 6/20/2024 11:42:30 99.098478 192.118668 0.995346 6/20/2024 11:40:56 520.860735 496.878602 497.457259 192.176819 1.004435 6/20/2024 11:42:37 97.941935 192.147736 0.997733 6/20/2024 11:41:03 518.550151 495.240932 496.838641 192.133209 1.007694 6/20/2024 11:42:45 98.652689 192.185898 0.992907 6/20/2024 11:41:11 519.6694 493.889844 492.089412 192.147736 1.009937 6/20/2024 11:42:52 99.305792 192.181656 0.994849 6/20/2024 11:41:18 518.913898 494.519975 496.574972 192.176819 1.009667 6/20/2024 11:43:00 99.754903 192.211334 0.994193 6/20/2024 11:41:26 520.705121 494.951423 498.20596 192.205887 1.008153 6/20/2024 11:43:07 98.745276 192.162277 0.994336 6/20/2024 11:41:33 521.327286 496.910579 495.362878 192.147736 1.007326 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Ethylene 191C TE Temp ( C )Pressure (atm) 6/20/2024 11:43:38 -0.001949 0.104134 0.463178 -0.075561 192.133209 0.99553 6/20/2024 11:43:45 -0.028626 0.119009 0.238039 -0.642198 192.060532 0.998421 6/20/2024 11:43:52 0.202582 0.277979 0.876804 0.409384 192.104126 0.993602 6/20/2024 11:44:00 0.317424 0.24872 1.197772 -0.166887 192.191345 0.992684 6/20/2024 11:44:08 0.23107 0.054011 0.610702 1.219568 192.160461 0.99359 6/20/2024 11:44:15 0.067533 0.328803 0.337982 -0.05354 192.133209 0.991949 6/20/2024 11:44:23 0.261042 0.072145 0.793143 0.29484 192.176819 0.993923 6/20/2024 11:44:30 -0.108875 0.148714 0.30656 0.688261 192.133209 0.991536 Raw Calibration Data BACKGROUND / PRE DIRECT ZERO PRE DIRECT CAL NO2 CAL PRE SYSTEM CAL PRE SYSTEM ZERO Date Time CO2% 191C Propane 191C span Temp ( C )Pressure (atm) 6/20/2024 11:47:53 6.376701 41.333843 192.096863 0.97972 6/20/2024 11:48:00 6.399998 40.396131 192.060532 0.979051 6/20/2024 11:48:07 6.388173 41.340522 192.104126 0.98107 6/20/2024 11:48:15 6.357272 42.150785 192.118668 0.984329 6/20/2024 11:48:22 6.384379 40.536618 192.075058 0.991628 6/20/2024 11:49:07 6.379959 40.069799 192.084656 0.995746 6/20/2024 11:49:15 6.379748 41.914403 192.084656 0.995746 6/20/2024 11:49:23 6.356361 39.464703 192.075058 0.992684 6/20/2024 11:49:30 5.460076 34.931353 192.071426 0.997044 6/20/2024 11:49:38 4.405368 31.919602 192.060532 1.003562 6/20/2024 11:49:45 4.380937 157.471722 192.133209 0.997641 6/20/2024 11:49:53 4.370349 183.363315 192.147736 1.001359 6/20/2024 11:50:00 4.060245 203.590399 192.147736 1.000298 6/20/2024 11:50:08 4.229959 189.819317 192.162277 0.997411 6/20/2024 11:50:15 5.780509 83.820307 192.104126 0.993464 6/20/2024 11:51:00 5.86736 78.621452 192.10704 0.992824 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm) 6/20/2024 15:05:46 522.00099 496.492876 493.43442 192.020554 1.004194 6/20/2024 15:04:05 97.294986 192.164703 0.993001 6/20/2024 15:05:53 522.803982 496.389593 490.489258 192.00238 1.005858 6/20/2024 15:04:13 98.573325 192.249496 0.998192 6/20/2024 15:06:01 523.219001 498.176273 498.643841 192.016922 1.00471 6/20/2024 15:04:21 98.615999 192.191345 0.994979 6/20/2024 15:06:08 521.28052 496.539479 498.185968 191.973312 1.0093 6/20/2024 15:04:28 99.472582 192.191345 0.992867 6/20/2024 15:06:16 525.819772 498.007121 496.278395 191.915161 1.005307 6/20/2024 15:04:36 99.004484 192.173172 0.992425 6/20/2024 15:06:23 526.116 499.696155 500.787869 191.900635 1.00448 6/20/2024 15:04:43 98.126699 192.130783 1.000311 6/20/2024 15:06:31 523.580294 497.442036 492.049052 191.886093 1.006408 6/20/2024 15:04:51 98.940092 192.104126 0.992546 6/20/2024 15:06:38 523.971118 498.225908 497.516185 191.893372 1.00564 6/20/2024 15:04:58 98.918466 192.160461 0.995478 6/20/2024 15:06:46 525.81493 498.920524 496.357474 191.900635 1.004251 6/20/2024 15:05:06 99.791038 192.075058 0.993923 6/20/2024 15:06:53 524.689038 497.883161 494.324124 191.929703 1.009989 6/20/2024 15:05:13 99.019164 192.0896 0.992959 Date Time CO ppm 191C (1of2) span NOx Wet Propane 191C span Temp ( C )Pressure (atm)Date Time Ethylene 191C TE Temp ( C )Pressure (atm) 6/20/2024 15:04:21 -0.370364 0.070762 -0.040605 192.191345 0.994979 6/20/2024 15:08:08 -1.393683 191.900635 0.991169 6/20/2024 15:04:28 -0.473053 0.108975 0.379022 192.191345 0.992867 6/20/2024 15:08:16 -0.296539 191.900635 0.992959 6/20/2024 15:04:36 -0.558235 0.235341 -0.826647 192.173172 0.992425 6/20/2024 15:08:23 -1.097376 191.915161 0.992729 6/20/2024 15:04:43 -0.530259 0.114766 -1.384532 192.130783 1.000311 6/20/2024 15:08:31 -0.394724 191.886093 0.991536 6/20/2024 15:04:51 -0.351511 0.094302 0.649854 192.104126 0.992546 6/20/2024 15:08:38 0.137739 191.982391 0.992506 6/20/2024 15:04:58 -0.541776 0.24587 -0.38659 192.160461 0.995478 6/20/2024 15:08:46 -1.047298 191.929703 0.99227 6/20/2024 15:05:06 -0.577382 0.455435 -0.138642 192.075058 0.993923 6/20/2024 15:08:53 0.394419 191.929703 0.98892 6/20/2024 15:05:13 0.077561 0.124158 -1.232036 192.0896 0.992959 6/20/2024 15:09:01 -0.161166 191.929703 0.991215 SAMPLE SPIKE RECOVERY POST SYSTEM CAL POST SYSTEM ZERO PRE TEST 1 495.6 6.4 40.5 5.8 83.8 0.095 83.6% Sensor Analyzer Cal Zero Cal Zero Response (ppm)Level (ppm)Response (ppm)Error (%)Error (%) NOx 494.0 493.4 0.0 0.12 0.00 CO 519.4 520.2 0.0 -0.16 -0.01 Propane 496.4 495.6 0.3 0.17 0.06 Ethylene 99.5 101.9 0.3 -2.37 0.27 Sensor System Cal Zero Cal Zero Response (ppm)Level (ppm)Response (ppm)Recovery (%)Error (%) NOx 496.9 493.4 0.2 0.71 0.03 CO 521.3 520.2 0.1 0.22 0.03 Propane 495.4 495.6 0.6 -0.05 0.13 Ethylene*98.7 101.9 0.1 -3.10 0.14 Sensor System Cal Zero Cal Zero Cal Zero Response (ppm)Level (ppm)Response (ppm)Recovery (%)Error (%)Drift Error (%)Drift Error (%) NOx 497.9 493.4 0.2 0.91 0.04 0.20 0.00 CO 524.7 520.2 -0.5 0.86 -0.09 0.65 0.12 Propane 494.3 495.6 -0.2 -0.26 -0.05 0.21 0.18 Ethylene*99.0 101.9 -0.6 -2.83 -0.60 0.27 0.74 *CTS Scans are conducted with Ethylene through the sample line. Lf 5.11 Lr Cr Tr Pr Lr/Lf 5.32 99.5 192.0 1.0 1.04 Ls Cs Ts Ps Ls/Lf 5.34 98.7 192.2 1.0 1.04 % Recovery Propane PRE DIRECT CAL FTIR QA/QC SUMMARY SAMPLE RECOVERY CALCULATIONS Period Spike #Concentration of Propane Cylinder Stack CO2 Concentration Pathlength Stack Propane Concentration Stack + Spike CO2 Concentration Stack + Propane Concentration DF Calculated POST SYSTEM CAL PRE SYSTEM CAL CERTIFICATE OF ANALYSIS Grade of Product: EPA PROTOCOL STANDARD Part Number:E02NI99E15W0051 Reference Number:153-402577489-1 Cylinder Number:CC486070 Cylinder Volume:144.0 CF Laboratory:124 - Tooele (SAP) - UT Cylinder Pressure:2015 PSIG PGVP Number:B72022 Valve Outlet:660 Gas Code:NO2,BALN Certification Date:Nov 08, 2022 Expiration Date:Nov 08, 2025 Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA 600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a mole/mole basis unless otherwise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval of the laboratory. Do Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals. ANALYTICAL RESULTS Component Requested Actual Protocol Total Relative Assay Concentration Concentration Method Uncertainty Dates NITROGEN DIOXIDE 150.0 PPM 146.6 PPM G1 +/- 2.0% NIST Traceable 11/01/2022, 11/08/2022 NITROGEN Balance CALIBRATION STANDARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date GMIS 15340120215 CC511005 59.52 PPM NITROGEN DIOXIDE/NITROGEN 1.4%Dec 17, 2024 PRM 12397 D887665 74.2 PPM NITROGEN DIOXIDE/AIR 1.3%Feb 02, 2022 The SRM, NTRM, PRM, or RGM noted above is only in reference to the GMIS used in the assay and not part of the analysis. ANALYTICAL EQUIPMENT Instrument/Make/Model Analytical Principle Last Multipoint Calibration MKS FTIR NO2 018143349 FTIR Nov 01, 2022 Triad Data Available Upon Request PERMANENT NOTES:OXYGEN ADDED TO MAINTAIN STABILITY Airgas Specialty Gases Airgas USA LLC 525 North Industrial Loop Road Tooele, UT 84074 Airgas.com Signature on file Approved for Release Page 1 of 1 CERTIFICATE OF ANALYSIS Grade of Product: PRIMARY STANDARD Part Number:X02NI99P15AD524 Reference Number:153-402622613-1 Cylinder Number:CC173895 Cylinder Volume:140.0 CF Laboratory:124 - Tooele (SAP) - UT Cylinder Pressure:2015 PSIG Analysis Date:Dec 22, 2022 Valve Outlet:350 Lot Number:153-402622613-1 Expiration Date:Dec 22, 2025 Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials. ANALYTICAL RESULTS Component Req Conc Actual Concentration Analytical (Mole %)Uncertainty ETHYLENE 100.0 PPM 101.9 PPM +/- 1% NITROGEN Balance Airgas Specialty Gases Airgas USA LLC 525 North Industrial Loop Road Tooele, UT 84074 Airgas.com Signature on file Approved for Release Page 1 of 1 Finley – North Randlett 6-20-2024 Finley – North Randlett 6-20-2024 Finley – North Randlett 6-20-2024 Instrument Resolution – FWHH – 0.4936 cm-1 which is < 0.55 cm-1 (therefore meets manufacturer specifications) Water Frequency – Freq – 3920.0915 cm-1 which is +/- 0.075 of 3920.0952 cm-1 (therefore meets ASTM) Please note: FWHH is the Full Width at Half Height of the resolution. The frequency position is only calculating the center line for one water line in the spectrum. MKS uses 3920.0952 cm-1 since it is a single water line. Spectral Fit Run 1 Spectral Fit Run 2 Spectral Fit Run 3 Analysis Validation Report Sample Filename: C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000142.LAB Filename for noise: C:\OLT\Data\Golden Spectrum 10-31-23\GOLDEN SPECTRUM 10-31-23_000004.LAB Interferences Filenames: C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000068.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000069.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000070.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000071.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000072.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000073.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000074.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000075.LAB Recipe path: C:\OLT\RECIPES\STEPHEN PYER TEST.MGRCP Gas calibration NameConc MDC3 MDC2 MDC1 MAU FMU*R OCU ~ DL ~ CL ~ Bias Sigma Range Span Comment NO 191C 81.33 3.9 -0.24 0.33 5.31 5.31 -2.05 --0-2795 1.05 Good NO2 191C 16.05 0.4 -0.03 0.03 0.42 0.42 -0.32 --0-488 1.05 Good N2O 191C -0.01 0.37 0.07 0.03 0.03 0.42 0.42 0.07 0.34 0 0.02 0-200 -Close to DL NH3 TE 191C 6.27 39.05 8.02 4.14 7.06 66.64 66.64 10.41 34.94 2.39 2.67 0-2995 -Close to DL H2O% (HIGH) 191C11.31 0.26 -0.02 0.03 0.42 0.42 -0.23 --0-40 -Good FORMALDEHYDE 191C31.14 1.13 -0.24 0.27 1.3 1.3 -0.62 --0-69 -Good FORMIC ACID 191C TE2.38 12.58 3.3 1.56 1.83 14.73 14.73 3.45 11.01 0.16 1.1 0-466 -Close to DL CH4 2900 CM-1 191C729.39 23.78 -1.69 2.46 45.83 45.83 -14.59 --0-3143 1 Good PROPANE 191C40.72 1.55 -0.22 0.27 1.87 1.87 -0.82 --0-4976 0.95 Good PROPYLENE 191C TE5.41 12.9 3.32 1.57 1.86 15.26 15.26 3.53 11.2 0.22 1.11 0-194 -Close to DL ETHANE 191C 70.18 3.71 -0.55 0.85 5.77 5.77 -1.77 --0-1004 -Good ETHYLENE 191C TE53.3 21.82 56.6 2.07 2.55 26.23 26.23 63.52 63.53 6.92 18.87 0-900 -Close to DL CO PPM 191C (1OF2)112.65 3.89 -0.26 0.56 8.01 8.01 -2.27 --0-5010 1.04 Good CO2% 191C 6.39 0.17 -0.01 0.02 0.23 0.23 -0.13 --0-23 -Good CO% 191C (2OF2)0.01 0 -0 0 0 0 -0 --0-8 -Good ACETALDEHYDE 191C3.11 2.36 4.01 0.64 0.82 3.04 3.04 4.63 4.63 0.62 1.34 0-186 1 Close to DL ACETYLENE 191C-0.07 4.47 0.86 0.79 1.05 5.91 5.91 1.07 3.72 0.21 0.29 0-1016 -Close to DL SO2 191C 2.63 2.2 2.22 0.26 0.32 2.68 2.68 2.23 2.23 0.01 0.74 0-964 1.02 Close to DL HEXANE 191C 5.03 1.14 5.5 0.13 0.18 1.54 1.54 6.09 6.09 0.59 1.83 0-1000 -Close to DL Analysis Validation Report Sample Filename: C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000203.LAB Filename for noise: C:\OLT\Data\Golden Spectrum 10-31-23\GOLDEN SPECTRUM 10-31-23_000004.LAB Interferences Filenames: C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000068.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000069.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000070.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000071.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000072.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000073.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000074.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000075.LAB Recipe path: C:\OLT\RECIPES\STEPHEN PYER TEST.MGRCP Gas calibration NameConc MDC3 MDC2 MDC1 MAU FMU*R OCU ~ DL ~ CL ~ Bias Sigma Range Span Comment NO 191C 92.49 3.96 -0.24 0.33 5.39 5.39 -2.09 --0-2795 1.05 Good NO2 191C 18.9 0.43 -0.03 0.03 0.45 0.45 -0.38 --0-488 1.05 Good N2O 191C 0.01 0.36 0.07 0.03 0.03 0.41 0.41 0.07 0.33 0 0.02 0-200 -Close to DL NH3 TE 191C 4.67 38 8.03 4.14 7.06 64.86 64.86 10.41 33.95 2.39 2.68 0-2995 -Close to DL H2O% (HIGH) 191C11.6 0.26 -0.02 0.03 0.41 0.41 -0.23 --0-40 -Good FORMALDEHYDE 191C32.63 1.17 -0.24 0.27 1.35 1.35 -0.65 --0-69 -Good FORMIC ACID 191C TE1.92 11.68 3.3 1.56 1.83 13.67 13.67 3.45 10.12 0.16 1.1 0-466 -Close to DL CH4 2900 CM-1 191C713.08 21.18 -1.69 2.46 40.82 40.82 -14.26 --0-3143 1 Good PROPANE 191C34.97 1.45 -0.22 0.27 1.75 1.75 -0.73 --0-4976 0.95 Good PROPYLENE 191C TE6.17 12.4 3.32 1.57 1.86 14.67 14.67 3.53 10.67 0.22 1.11 0-194 -Close to DL ETHANE 191C 63.8 3.53 -0.55 0.85 5.5 5.5 -1.68 --0-1004 -Good ETHYLENE 191C TE53.98 17.35 56.6 2.07 2.55 20.88 20.88 63.52 63.53 6.92 18.87 0-900 -Close to DL CO PPM 191C (1OF2)123.82 4.1 -0.26 0.56 8.44 8.44 -2.48 --0-5010 1.04 Good CO2% 191C 6.42 0.16 -0.01 0.02 0.22 0.22 -0.13 --0-23 -Good CO% 191C (2OF2)0.01 0 -0 0 0 0 -0 --0-8 -Good ACETALDEHYDE 191C2.91 2.48 4.01 0.64 0.82 3.18 3.18 4.63 4.63 0.62 1.34 0-186 1 Close to DL ACETYLENE 191C0.07 4.56 0.86 0.79 1.05 6.03 6.03 1.07 3.81 0.21 0.29 0-1016 -Close to DL SO2 191C 2.09 2 2.22 0.26 0.32 2.43 2.43 2.23 2.23 0.01 0.74 0-964 1.02 Close to DL HEXANE 191C 3.9 1.06 5.5 0.13 0.18 1.43 1.43 6.09 6.09 0.59 1.83 0-1000 -Close to DL Analysis Validation Report Sample Filename: C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000264.LAB Filename for noise: C:\OLT\Data\Golden Spectrum 10-31-23\GOLDEN SPECTRUM 10-31-23_000004.LAB Interferences Filenames: C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000068.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000069.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000070.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000071.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000072.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000073.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000074.LAB C:\OLT\Data\Finley Resources\NR CS E4 6-20-24\FINLEY NR CS E4 6-20-24_000075.LAB Recipe path: C:\OLT\RECIPES\STEPHEN PYER TEST.MGRCP Gas calibration NameConc MDC3 MDC2 MDC1 MAU FMU*R OCU ~ DL ~ CL ~ Bias Sigma Range Span Comment NO 191C 91.96 3.93 -0.24 0.33 5.34 5.34 -2.07 --0-2795 1.05 Good NO2 191C 19.52 0.48 -0.03 0.03 0.51 0.51 -0.39 --0-488 1.05 Good N2O 191C -0.05 0.35 0.07 0.03 0.03 0.4 0.4 0.07 0.33 0 0.02 0-200 -Close to DL NH3 TE 191C 7.36 37.21 8.02 4.14 7.06 63.5 63.5 10.41 33.07 2.39 2.67 0-2995 -Close to DL H2O% (HIGH) 191C11.61 0.24 -0.02 0.03 0.38 0.38 -0.23 --0-40 -Good FORMALDEHYDE 191C32.95 1.21 -0.24 0.27 1.4 1.4 -0.66 --0-69 -Good FORMIC ACID 191C TE0.96 12.02 3.3 1.56 1.83 14.07 14.07 3.45 10.49 0.16 1.1 0-466 -Close to DL CH4 2900 CM-1 191C709.77 20.65 -1.69 2.46 39.8 39.8 -14.2 --0-3143 1 Good PROPANE 191C35.95 1.48 -0.22 0.27 1.78 1.78 -0.74 --0-4976 0.95 Good PROPYLENE 191C TE5.46 12.69 3.32 1.57 1.86 15.02 15.02 3.53 10.98 0.22 1.11 0-194 -Close to DL ETHANE 191C 64.49 3.64 -0.55 0.85 5.68 5.68 -1.75 --0-1004 -Good ETHYLENE 191C TE54.34 21.13 56.6 2.07 2.55 25.43 25.43 63.52 63.53 6.92 18.87 0-900 -Close to DL CO PPM 191C (1OF2)125.47 4.18 -0.26 0.56 8.6 8.6 -2.51 --0-5010 1.04 Good CO2% 191C 6.44 0.16 -0.01 0.02 0.22 0.22 -0.13 --0-23 -Good CO% 191C (2OF2)0.01 0 -0 0 0 0 -0 --0-8 -Good ACETALDEHYDE 191C3.22 2.43 4.01 0.64 0.82 3.12 3.12 4.63 4.63 0.62 1.34 0-186 1 Close to DL ACETYLENE 191C-0.16 4.83 0.86 0.79 1.05 6.38 6.38 1.07 4.07 0.21 0.29 0-1016 -Close to DL SO2 191C 1.86 2.05 2.22 0.26 0.32 2.5 2.5 2.23 2.23 0.01 0.74 0-964 1.02 Close to DL HEXANE 191C 4.26 1.09 5.5 0.13 0.18 1.48 1.48 6.09 6.09 0.59 1.83 0-1000 -Close to DL APPENDIX C Test Run Load %Site Rated Load, bhp Load Approx., bhp 1 68 1380 938.4 2 69 1380 952.2 3 69 1380 952.2 Engine Load Approximation based on Panel Levels APPENDIX D Test Run Flowrate dscfm Approx. BHP Avg O2 % NOx ppmvd NOx g/bhp-hr NOx lbs/hr CO ppmvd CO g/bhp-hr CO lbs/hr NMNEHC ppmvd NMNEHC g/bhp-hr NMNEHC lbs/hr Moisture Content % 1 1545.91 938.4 6.0 107.90 0.58 1.19 127.57 0.42 0.86 100.84 0.52 1.07 11.32 2 1470.65 952.2 6.0 103.59 0.52 1.09 132.81 0.41 0.85 99.33 0.48 1.00 11.46 3 1436.40 952.2 6.0 125.94 0.62 1.29 141.15 0.42 0.88 94.85 0.45 0.93 11.58 947.6 6.0 112.48 0.57 1.19 133.84 0.41 0.86 98.34 0.48 1.00 11.46 Summary Average Levels Example Calculations: Uinta Wax Operating, LLC, North Randlett Compressor Station, #3 The following is a step-by-step calculation for the first test run conducted on the North Randlett Compressor Station #3. Test Parameters • Stack Diameter = 13.5 inches • Traverse Points = 16 • Ports = 2 • Barometric Pressure = 24.91 in Hg • Average O2 = 6.0% • Average CO2 = 7.1% • Load Approximation = 938.4 bhp • Moisture Content = 11.32% EPA 40 CFR 60(A) Methods 1-3: Determination of Stack Gas Velocity and Flow Rate Dry Molecular Weight (lb/lbmol) = (0.44 * %CO2) + (0.32 * %O2) + ((0.28 * (%N2 + %CO)) Where: %CO2 – Carbon Dioxide Content Of The Gas = 7.1% %O2 – Oxygen Content Of The Gas = 6.0% %N2 – Nitrogen Content Of The Gas %CO – Carbon Monoxide Content Of The Gas (%N2 +%CO) = (100 - %O2 - %CO2) = (100 – 6.0 – 7.1) = 86.9% Dry = (0.44 * %CO2) + (0.32 * %O2) + ((0.28 * (%N2 + %CO)) = (0.44 * 7.1) + (0.32 * 6.0) + (0.28 * 86.9) = 29.38 lb/lbmol Wet Molecular Weight (lb/lbmol) = MD * (1-BWS) + (18) * BWS Where: MD – Molecular Weight Of The Dry Gas (lb/lbmol) = 29.38 lb/lbmol BWS – Moisture Content Of The Gas (%/100) = 11.32% = MD * (1-BWS) + (18) * BWS = 29.38 * (1 – (11.32/ 100)) + (18 * (11.32/ 100)) = 28.09 lb/lbmol Average Stack Gas Velocity (ft/sec) = Cp * (85.49) * ∆PAVG * (TS / (((PS / 13.6) + PB) * MA)) Where: CP – Pitot tube constant (unitless) = 0.84 ∆PAVG – Average square root of the stack gas pitot DP (inches water) = 0.924 in H2O TS – Average stack temperature (R) = 1424 R PB – Barometric pressure (in Hg) = 24.91 in Hg PS – Stack pressure relative to barometric pressure (inches water) = 0.3 in H2O MA – Molecular weight of the wet gas (lb/lbmol) = 28.09 lb/lbmol = Cp * (85.49) * ∆PAVG * (TS / (((PS / 13.6) + PB) * MA)) = 0.84 * (85.49) * 0.924 * ( 1424 / (((0.3/ 13.6) + 24.91) * 28.09)) = 94.60 ft/sec Average Dry Flowrate (dscfm) = 60 * (1-BWS) * VS *  * (((DS / 2) / 12))2)* TSTD / TS * (PB + (PS / 13.6)) / 29.92 Where: DS – Diameter of the stack (inches) = 13.5 inches BWS – Moisture content of the gas (%) = 11.32% TSTD – Standard temperature (528R) TS – Average stack temperature (R) = 1424 R PB – Barometric pressure (in Hg) = 24.91 in Hg PS – Stack pressure relative to barometric pressure (inches water) = 0.3 in H2O VS– Average Stack gas velocity (ft/sec) = 94.60 ft/sec = 60 * (1-BWS) * VS *  * (((DS / 2) / 12))2)* TSTD / TS * (PB + (PS / 13.6)) / 29.92 = 60 * (1 - (11.32/ 100)) * 94.60 *  * (((13.5 / 2) / 12))2) * 528 / 1424 * (24.91 + (0.3 / 13.6)) / 29.92 = 1545.91 dscfm Conversion of Dry Flowrate to m3/hr = Q * 60 * 2.83168*10 -2 Where: Q – Volumetric Flowrate = 1545.91 dscfm 2.83168*10 -2 – Conversion factor for cubic feet to cubic meter 60 – Minutes in an hour = Q * 60 * 2.83168*10 -2 = 1545.91 *60 * 2.83168*10 -2 = 2626.51 m3/hr ASTM D 6348-03: Determination of NOx, CO and VOC Emissions From Stationary Sources NOx Emission Rate (g/Bhp-hr) = (Cd * 1.912*10 -3 * Q * T) / HP-hr Where: Cd – Measured NOx concentration in ppm = 107.90 ppm 1.92*10 -3 - Conversion constant for ppm to g/m3 NOx Q – Volumetric Flowrate = 2626.51 m3/hr T – Time in Hours of Test Run = 1 hr HP-hr – Unit Brake Horsepower = 938.4 Bhp = (Cd * 1.912*10 -3 * Q * T) / HP-hr = (107.90 * 1.912*10 -3 * 2626.51 * 1) / 938.4 = 0.58 g/Bhp-hr NOx Emission Rate (lbs/hr) = g/Bhp-hr / 454 * Bhp Where: g/Bhp-hr = 0.58 g/Bhp-hr 454 – Conversion factor for g to lbs Bhp - Unit Brake Horsepower = 938.4 Bhp = g/Bhp-hr / 454 * Bhp = 0.58 / 454 * 938.4 = 1.19 lbs/hr CO Emission Rate (g/Bhp-hr) = (Cd * 1.164*10 -3 * Q * T) / HP-hr Where: Cd – Measured CO concentration in ppm = 127.57 ppm 1.164*10 -3 - Conversion constant for ppm to g/m3 CO Q – Volumetric Flowrate = 2626.51 m3/hr T – Time in Hours of Test Run = 1 hr HP-hr – Unit Brake Horsepower = 938.4 Bhp = (Cd * 1.164*10 -3 * Q * T) / HP-hr = (127.57 * 1.164*10 -3 * 2626.51 * 1) / 938.4 = 0.42 g/Bhp-hr CO Emission Rate (lbs/hr) = g/Bhp-hr / 454 * Bhp Where: g/Bhp-hr = 0.42 g/Bhp-hr 454 – Conversion factor for g to lbs Bhp - Unit Brake Horsepower = 938.4 Bhp = g/Bhp-hr / 454 * Bhp = 0.42 / 454 * 938.4 = 0.86 lbs/hr VOC Emission Rate (g/Bhp-hr) = (Cd * 1.833*10 -3 * Q * T) / HP-hr Where: Cd – Measured VOC concentration in ppm = 100.84 ppm 1.833*10 -3 - Conversion constant for ppm to g/m3 VOC Q – Volumetric Flowrate = 2626.51 m3/hr T – Time in Hours of Test Run = 1 hr HP-hr – Unit Brake Horsepower = 938.4 Bhp = (Cd * 1.833*10 -3 * Q * T) / HP-hr = (100.84 * 1.833*10 -3 * 2626.51 * 1) / 938.4 = 0.52 g/Bhp-hr VOC Emission Rate (lbs/hr) = g/Bhp-hr / 454 * Bhp Where: g/Bhp-hr = 0.52 g/Bhp-hr 454 – Conversion factor for g to lbs Bhp - Unit Brake Horsepower = 938.4 Bhp = g/Bhp-hr / 454 * Bhp = 0.52 / 454 * 938.4 = 1.07 lbs/hr APPENDIX E FTIR Engine Test Sheet Company Name Location / Unit 1.0. Type of Test Completed Field Technician (5) Client Rep and/or State Rep Date 3x1hr Y'l-V David Martinez '\vie ( (Kvl~. Non-Resettable Run Time Hours Engine Make I,. A Engine Model {¥I ~[ 1(.. 13, Port Distance B 3,t.I'\ Exhaust Diameter (inches) \:S,S Calibration Gas Cylinder # NO (ppm CC453965 CO (ppm CC453965 Propane ppm) CC453965 N02 (ppm) CC486070 Ethylene (ppm CC173895 Methane (ppm CC453965 Acetaldehyde ppm) CC321163 Concentration 493.4 520.2 495.6 146.6 101.9 499.4 196.7 Stack Diagram Test 1 Test 2 Test 3 Time of Reading \\~Sll \}'~~1 1: 3.i Atm Pressure (in Hg) ~c.t. tt ~c.Le1J d.-'t , ~\ Atm Temp CF) ., ~~ ~"'l Engine RPM ~ \\1, \t/S \d..d-~ *Manifold Pres. Vac(") or E(oost(pgi) or Boost (psia) ~, ~I. d...~ Manifold Temp CF) r~c;( '3 '! '~Gr Psuction (psi) Stage 1 ~~ q..3 -;}.~ Tsuction CF) StaQe 1 -..,. ~ --,. Pdischarae (psi) Staae 1 It ct3 ctd-. Psuction [psi) Stage 2 \ \ Tsuction OF) Stage 2 I I Pdischarc e (psi) Staae 2 ~1~ d-.q'). 0.'1\ Psuction (psi) Stage 3 , 1\ \ Tsuction OF) Staae 3 , \ \ Pdischarc e (psi) Staae 3 ~ b 'Co \\ )(>Ie::. Psuction (psi) Stage 4 , Tsuction OF) StaQe 4 t Pdischarge (psi) Stage 4 \ Gas Throuahput (mmcf/d) or ( V\'\ F F\ LP-.. 'hI'" ~\.IO d-.L rl.c.:,5, Pre Cat Temp CF) qoCl 11 \ ~ \5 Post Cat Temp CF) G{ 6 It( C-fbl q)). Cat Differential Pres. (" of H2O) b. "l Humidity % .01 \O.~ q.L-f 02% 6.{/ l.6 '1. a C02 % Dry ....-.. 7,1 .d. I,d, LOAD % (fanel)or (Estimated) l.~ 6t7t hOI Ignition Timing CF) 0.,\ \\ 'd-1. \ 1,\ AFR Setting m~~~) 3.{).q "'!:> f:), 'I :'0. '1 AFR Settinl1 mV fR' ,. k) ---. -.,,,. Rev 8 * Some units show boost in inches of Hg. In this situation please indicate if it is positive (+) or negative(-). Eg: (+12") or (·5") 9/17/2019 Worksheet: O2 Stratification Client:Finley Location:North Randlett E4 Date:6/20/2024 PD:13.5 DD:34 YES Method 1 Criteria Met UD:7.5 YES Method 1 Criteria Met Port Point Insertion Depth Reading (inches)(%) A 1 2.24 6.00 A 2 6.75 6.00 A 3 11.25 6.00 A 4 A 5 A 6 A 7 A 8 A 9 A 10 A 11 A 12 Average 6.00 Notes: To demonstrate non-stratified flow and utilize one sampling location O2 may not deviate by more than +/- 0.3% of the average O2 concentration. EPA REFERENCE METHOD 3A (Determination Of Stratification) COMPANY NAME:Finley COMPANY LOCATION:North Randlett E4 DATE:6/20/2024 STACK DIAMETER (inches):13.5 TRAVERSE POINTS:16 2 TEST RUN #1 TEST RUN #2 TEST RUN #3 AVERAGE O2:6 AVERAGE O2:6 AVERAGE O2:6 AVERAGE CO2:7.1 AVERAGE CO2:7.2 AVERAGE CO2:7.2 BARO PRESSURE:24.91 BARO PRESSURE:24.91 BARO PRESSURE:24.91 Point Insertion DepthDP (H2O)Ts (deg F)Stat P (H2O)Point Insertion DepthDP (H2O)Ts (deg F)Stat P (H2O)Point Insertion DepthDP (H2O)Ts (deg F)Stat P (H2O) 1 0.5 0.79 964 0.3 1 0.5 0.73 967 0.31 1 0.5 0.66 972 0.29 2 1.4175 0.82 2 1.4175 0.75 2 1.4175 0.7 3 2.619 0.85 3 2.619 0.78 3 2.619 0.73 4 4.3605 0.89 4 4.3605 0.81 4 4.3605 0.77 5 9.1395 0.88 5 9.1395 0.84 5 9.1395 0.8 6 10.881 0.88 6 10.881 0.79 6 10.881 0.76 7 12.0825 0.86 7 12.0825 0.76 7 12.0825 0.76 8 13 0.87 8 13 0.75 8 13 0.72 9 9 9 10 10 10 11 11 11 12 12 12 13 13 13 14 14 14 15 15 15 16 16 16 1 0.5 0.81 964 0.3 1 0.5 0.71 967 0.31 1 0.5 0.69 972 0.29 2 1.4175 0.82 2 1.4175 0.74 2 1.4175 0.72 3 2.619 0.84 3 2.619 0.78 3 2.619 0.76 4 4.3605 0.88 4 4.3605 0.82 4 4.3605 0.8 5 9.1395 0.89 5 9.1395 0.85 5 9.1395 0.83 6 10.881 0.87 6 10.881 0.81 6 10.881 0.78 7 12.0825 0.85 7 12.0825 0.77 7 12.0825 0.74 8 13 0.86 8 13 0.74 8 13 0.71 9 9 9 10 10 10 11 11 11 12 12 12 13 13 13 14 14 14 15 15 15 16 16 16