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Home My WebLink AboutDAQ-2024-0112351 DAQC-1075-24 Site ID 10124 (B5) MEMORANDUM TO: CEM FILE – SILVER EAGLE REFINING THROUGH: Harold Burge, Major Source Compliance Section Manager FROM: Rob Leishman, Environmental Scientist DATE: October 21, 2024 SUBJECT: Source: Main Plant Fuel Gas Line Contact: Blaine Zwahlen – 435-319-6861 Location: 2355 South 1100 West, Woods Cross, Davis County, UT Test Contractor: Alliance Technical Group FRS ID#: UT0000004901100019 Permit/AO#: Approval Order (AO) DAQE-AN101240030-16 dated November 9, 2016 Subject: Review of RA/PST Report dated June 19, 2024 On July 1, 2024, Utah Division of Air Quality (DAQ) received a Relative Accuracy/Performance Specification Test (RA/PST) report for the Silver Eagle Refining main fuel line in Woods Cross, Utah. Testing was performed on May 31, 2024, to determine the relative accuracy of the H2S monitoring systems. The DAQ-calculated test results are: RA/PST EVALUATION: Silver Eagle - Fuel Gas RATA Test Date - 5/31/2024 Primary Channel Manufacturer Serial No. Units CEM Value RM Value Relative Accuracy Certification Status H2S Siemens Maxum II 3003955197 PPM -0.500 0.000 0.3% Passed H2S Siemens Maxum II HOU30075841370010 PPM -0.500 0.000 0.3% Passed Stack Test Deviation Report There were no deviations observed during testing. Calibration gases were in date and met performance specifications. DEVIATIONS: No deviations were noted in this report. CONCLUSION: Silver Eagle operates the continuous emissions monitor (CEM) on the Fuel Gas and Flare System to measure H2S emissions. The CEM was audited by the DAQ and found to meet quality assurance requirements found in 40 CFR Part 60, Appendix B, Performance Specification 1, and R307-170, Continuous Emission Monitoring System Program. Quarterly cylinder gas audits and an annual relative accuracy test audit were conducted in accordance with the procedures outlined in UAC R307-170. 1 8 2 2 RECOMMENDATION: The Silver Eagle Fuel Gas and Flare CEM system was operating as required in R307-170 and 40 CFR 60.13 at the time of this evaluation. HPV: No. ATTACHMENTS: RATA Review Spreadsheets and RATA Report. SilverFagle REFINING r,I ,,..'.r tr r ii/ .r... June 19,2024 Utah Department of Environmental Quality Division of Air Quality P.O. Box 144820 Salt Lake city, Utah 84114-4820 Attn: Mr. Rob Leishman _UTAH DJ:pARTtv,tFNT OFENVIRONMI.NTAL CLJALIIY JUL DIV,SION OF AIN Q(.:,iI ,T- Re: May 2024 H2S CEM Relative Accuracy Test Audit (RATA) Results Dear Rob: Enclosed are the results of the successful RATA test conducted on May 3 1,2023, by Alliance Source Testing. This report also includes the results from the RATA test conducted on May 15. The May l5 test was deemed not in compliance because the method-specified run times for the nine tests were too short. The following Continuous Emission Monitors (CEMs) were audited: Siemens Model: Serial Number: Range: Siemens Model: Serial Number: Range: Maxim II 30039ss197-000010 0 - 300 ppm Maxim II HOU3007s841370010 0 - 300 ppm The CEM's are located in the refinery adjacent to the control room. It appears all CEM monitors passed prescribed accuracy testing. If you have any questions about the enclosed information, please contact me at 435-319-6861 or by email at bzwahlen@silvereaglerefining.com. Sincerely,A.)' a ^ffiffiim for Silver Eagle Refining-Woods Cross Inc. Stephen Jeffs Mike Platz James Shupe Mike Klotovich Cc 2355 South 1100 West . Woods Cross, Utah 84087 AtAre it t., ili\r(),;':!l (lti(-)rrl' RATA Report Silver Eagle Refining Woods Cross Refinery 2355 S ll00 W Woods Cross, UT 84087 Source Tested: Flare/Fuel Gas Test Dates: May l5 & 31,2024 Project No. AST-2024-215 I UTAH OEPARTMENT OF ENVIBONMENTAL OUAIJTY JUL - 1 2024 DMSION OF AIR QUAUTV Prepared By Alliance Technical Group, LLC*I 3683 W 2270 S, Suite E .,ii West Valley City, UT T t t t Source Tesl Reporl Test Program Summary Resulatorv Information Permit No. Regulatory Citations Source Information DAQE-ANr01240030-16 40 CFR 60, Appendix B, Performance Specification 7 40 CFR 60, Subpart J I Source Name Flare/Fuel Gas Contact Information Target Parameter HzS I T I Test Location Silver Eagle Refining Woods Cross Refinery 2355S1100W Woods Cross, UT 84087 Facility Contact Blaine Zwahlen bzwah len@si lvereaglerefi ning.com (801) 298-321 I Test Company Alliance Technical Group, LLC 3683 W 2270 S, Suite E West Valley City, UT 84120 Project Manager Charles Horton charles.horton@all iancetg.com (352) 663-7568 Field Team Leader Alan Jensen alan jensen@alliancetg.com (847) 220-3949 QA/QC Manager Kathleen Shonk katie.shonk@all iancetg.com (812) 4s2-4785 Report Coordinator Delaine Spangler delaine.spangler@al liancetg.com Report Reviewer Sarah Perry sarah.perry@al liancetg.com I t I I I T I I I T T Silver Eagle - Woods Cross, UTAST-2024-2 I 5 I 2of54 Page i I AI Fla lrI Source Test Repon Certificotion Statement I Alliance Technical Group, LLC (Alliance) has completed the source testing as described in this report. Results apply only to the source(s) tested and operating condition(s) for the specific test date(s) and time(s) identified within this report. All results are intended to be considered in their entirety, and Alliance is not responsible for use of less than the complete test report without written consent. This report shall not be reproduced in full or in part without written approval from the customer. To the best of my knowledge and abilities, all information, facts and test data are correct. Data presented in this report has been checked for completeness and is accurate, error-free and legible. Onsite testing was conducted in accordance with approved internal Standard Operating Procedures. Any deviations or problems are detailed in the relevant sections in the test report. This report is only considered valid once an authorized representative of Alliance has signed in the space provided below; any other version is considered draft. This document was prepared in portable document format (.pdf) and contains pages as identified in the bottom footer of this document. t I I I T 6t12t2024 Charles Horton, QSTI Alliance Technical Group, LLC Date I I I t t I I t t t Silver Eagle - Woods Cross, UT t AST-2024-2 I 5 I 3 of54 Page ii AI Source Test Repon Table ofContents TABLE OF CONTENTS l.l Process/Control System Descriptions.. ...............' l-l 1.4 Site Specific Test Plan & Notification................... ................... l-l 3.1 U.S. EPA Reference Test Method 15 - Hydrogen Su1fide....... ....................... 3-l LIST OF TABLES Table 2- l: Summary of Performance Specification Test Results ...........2'l APPENDICES Appendix A Sample Calculations Appendix B RA Calculations & Field Data Appendix C Quality Assurance/Quality Control Data Appendix D CEMS Data FralEe l,il r Silver Eagle - Woods Cross, UT 4of54 5 of54 Fla I I AI Source Test Report Inlroduclion I I I I t I I T I I I t t I I I 1.0 Introduction Alliance Technical Group, LLC (Alliance) was retained by Silver Eagle Refining (Silver Eagle) to conduct performance specification (PS) testing at the Woods Cross Refinery. Portions of the facility are subject to provisions of the 40 CFR 60, Appendix B, PS 7, Subpart J, and the Utah Department of Environmental Quality, Division of Air Quality (UDAQ) Approval Order (AO) DAQE-AN101240030-16. Testing included conducting a relative accuracy test audit (RATA) to determine the relative accuracy (RA) of the hydrogen sulfide (H:S) continuous emissions monitoring system (CEMS) serving the Fuel Gas and Flare Gas. l.l Process/ControlSystemDescriptions Silver Eagle owns and operates a continuous monitoring system located downstream of the primary fuel mixing drum to determine compliance with the sulfur dioxide (SOz) and HzS limits of NSPS Subpart J. The facility records the output of the system, for measuring the H2S concentration in the plant fuel gas. SOz emissions are calculated assuming 100% of the Hu S in the plant fuel gas is combusted forming SOu at a ratio of 34lbs of H2S equals 64lbs of SOz. 1.2 CEMS Descriptions Pollutant HzS Siemens / Siemens Maxum II / Maxum II 3003955 197 / HOU30075841370010 0-300 ppm Parameter: Make: Model: Serial No.: Span: 1.3 Project Team Personnel planned to be involved in this project are identified in the following table. Table l-l: Project Team Silver Eagle Personnel Blaine Zwahlen Alliance Personnel Alan Jensen Finn Townsley 1.4 Site Specific Test Plan & Notification Testing was conducted in accordance with the Site Specific Test Plan (SSTP) submitted to UDAQ by Silver Eagle. 1.5 Test Program Notes The original RATA was conducted on May 15,2024. A retest was conducted on May 31,2024 due to insufficient run times during the original RATA. Silver Eagle - Woods Cross, UT I AST-2024-2 I 5 l 6 ot54 Page l-l 7 of54 I I I I I I I I I I I I I t I I t T I AI r TA ,11,.."' lEe i'l:i '' Source Test Report Summary of Results 2.0 Summary of Results Alliance conducted PS testing at the Woods Cross Refinery in Woods Cross, Utah on May l5 and 3l, 2024. Testing consisted of determining the RA of the HzS continuous emissions monitoring system (CEMS) serving the Fuel Gas and Flare Gas. Table 2-l provides a summary of the emission testing results with comparisons to the applicable RA requirements. Any difference between the summary results listed in the following table and the detailed results contained in appendices is due to rounding for presentation. Table 2-l: Summary of Performance Specification Test Results Calculatedusingtheapplicablesourcestandardforthepollutant. SeeAppendixBfortheapplicablestandardused. Silver Eagle - Woods Cross, UT Hydrogen Sulfide Performance Specification - Initial Test Hydrogen Sulfide Data Concentration, ppmvd Hydrogen Sulfide Performance Specification - Retest Hydrogen Sulfide Data Concentration, ppmvd AST-2024-2 l 5 l 8 of54 Page 2-l 9 of54 I t put6rpe Source Test Report Testing MethodologyTECI.l NICAL GROUP t 3.0 Testing Methodology The emission testing program was conducted in accordance with the test methods listed in Table 3-1. Method descriptions are provided below while quality assurance/quality control data is provided in Appendix C.I Table 3-l; Source Testing Methodology T I I 3.1 U.S. EPA Reference Test Method 15 - Hydrogen Sulfide The hydrogen sulfide testing was conducted in accordance with U.S. EPA Reference Test Method 15. The sampling system consisted of a heated Teflon probe, heated Teflon sample line, gas conditioning system, leak-free pump, unheated Teflon sample line, and a gas chromatogaph (GC) equipped with a flame photometric detector (FPD). Each test run consisted of 2 injections performed over a period of at least 30 minutes. The GCffPD was calibrated for each reduced sulfur compound (HzS, COS and CS2) with a certified calibration gas diluted with a dilution system validated in accordance with EPA Method 205 to produce three (3) or more concentration levels spanning the linear range of the FPD. Calibration precision, sample line loss, and calibration drift test values were maintained in accordance with EPA Method l5 requirements. The relative accuracy of the HzS CEMS was determined based on procedures found in 40 CFR 60, Appendix B, Performance Specification 7. I I I T T I t I I I I Silver Eagle - Woods Cross, UT T AST-2024-2151 l0 of54 Page 3-l I I T I I t t t t I t I I t I I t I I al6rce Example Calculations Corrected Concentration, PPmvd Crr, = CorrxRF where, Coas RF Cnzs 0.00 : average H2S concentration observed during test, ppmvd 1.05 : system recovery correction factor, unitless 0.0 = average H2S concentration during test, ppmvd l3 of54 I I I t I I t I I I I t I I I I I I t l4 of54 I,Fr Aliarue I souRCE rESrtNG H2S Summary Location: Silver Eagle Refining - Woods Cross Refinery I I I I I t I I I Confidence Coeflicient, CC,lcc :l'o= x sdr I "ln I where, hsts 2.306 = degrees of freedom n T= number of runs selected for calculating the RAI Sd CC 0.00 : standard deviation ofdifference I 0.0000 = confidence coefficient I Relative Accuracy, RA Lt I umn <tiferarc el+l :F *tVi If,t= lr/rt lrlgg AS q RL{ where, mean difference 0.50 = average difference of Reference Method and CEMS h szs 2.306 = degrees of freedom n -T= number of runs selected for calculating the RA Sd 0"00 = standard deviation of difference AS 162 : applicable standard RA 0^00 : relative accuracy T t I t Run No.Date Time Reference Method H25 ppmvd CEMS H2S ppmvd Average Difference ppmvdStartEnd I 2 3 4 5 6 7 8 9 5/15/24 5lt5l24 5/t5124 5lt5l24 5n5124 5lt5l24 5lt5l24 sil5124 5ltsl24 7:30 7:53 8: l3 8:33 8:56 9:16 9:36 9:59 l0: l9 7:50 8:l I 8:31 8:53 9:14 9:34 9:56 l0: l7 l0:37 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 -0.50 -0.50 -0.50 -0.s0 -0.50 -0.50 -0.50 -0.50 -0.50 0.50 0.50 0.50 0.50 0.50 0.s0 0.s0 0.s0 0.50 Average 0.00 -0.50 0.50 Standard Deviation (Sd)0.00 Applicable Source Standard (AS)t62 Confi dence Coeffi cient (CC)0.000 Relative Accuracy (RA)O.3lo/" Acceptability Criteria - Applicable Source Standard < 100 Performance Specification Method PS 7 (RM l5) l5 of54 a6ard\oet=NLz Ar 6 r ;i ^ r vi l l r Ql e o hl n <6 6 ltQlo + ui - f ) <6 0 \ (: { l o c h Y- t :i <€ o , $CJ o o hn Y l <€ a CJ O - h- f ] <a € d- . -h- i :: <r € sQr o o vi 1_ 1 Yl <F - r ooFF :E 3 qoqqOAAU) N!tddFaz'=A o=rl .odLca toqdeQI=u,=ooEt6o:U) 't6 c!6gnav)v)E] O: 9* -- \i E ; =1 (: ttITTIItIIITItIIIII l6 of 5 4 I T I t I I anErrce Run I Data Location: Silver Eagle Refining - Woods Cross Refinery Source: Flare/Fuel Gas Project No.: AST-2024-2151 Date: 511512024 I I 2 3 4 5 6 7 8 9 l0 7:30 7:32 7:35 7:37 7:39 7:41 7:44 7:46 7:48 7:50 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00t I I I I I I I I I t T Injection Start Time l7 of54 T t T T T T T T I t t t t T I T T t I AlErrce sr)L_|ir)L I ts I rNo Run 2 Data Location: Silver Eagle Refining - Woods Cross Refinery Source: Flare/Fuel Gas Project No. : AST-2024-ZI 5 I Date: 5115/2024 I 2 J 4 5 6 7 8 9 7:53 7:55 7:57 7:59 8:02 8:04 8:06 8:08 8:l I 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 Injection Start Time Parameter H,S Uncorrected Run Average (Coo")0.00 Corrected Run Average (Corr)0.00 l8 of54 T T I T I I I I t T T t I t T t I T I l t=Al6trce.j.)L_|tCt I LS rrNai Run 3 Data Location: Silver Eagle Refining - Woods Cross Refinery Source: Flare/Fuel Gas Project No.: AST-2024-21 5l Date: 511512024 I 2 J 4 5 6 7 8 9 8:13 8:15 8:17 8:20 8:22 8:24 8:26 8:29 8:3 I 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 Injection Start Time l9 of54 Injection Start Time FAIErrces()u8cL IIsriN(;Run 4 Data l Location: Silver Eagle Refining - Woods Cross Refinery Source: Flare/Fuel Gas Project No.: AST-2024-2151 Dile: 511512024 I I T I I 2 J 4 5 6 7 8 9 l0 8:33 8:35 8:38 8:40 8:42 8:44 8:47 8:49 8:5 I 8:53 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 I I I T Parameter H,S Uncorrected Run Average (Co6.)0.00 Corrected Run Averaqe (Corr)0.00 t I I I I I I t I I I I I I I I T I T rutErrce Run 5 Data Location: Silver Eagle Refining - Woods Cross Refinery Source: Flare/Fuel Gas Project No.: AST-2024-21 5 I Datez 511512024 I 2 3 4 5 6 7 8 9 8:56 8:58 9:00 9:02 9:05 9:07 9:09 9:l I 9:14 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 2l of 54 FAllanrce Run 6 Data Location: Silver Eagle Refining - Woods Cross Refinery Source: Flare/Fuel Gas Project No.: AST-2024-2151 Datez 511512024 I T I I I 9:16 9:18 9:20 9:23 9:25 9:27 9:29 9:32 9:34 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 T t I I Injection Start Time Parameter H,S Uncorrected Run Average (Coo,)0.00 Corrected Run Average (Corr)0.00 F:Alianrce sr_)t., )a)L lLsrlNo Run 7 Data Location: Silver Eagle Refining - Woods Cross Refinery Source: Flare/Fuel Cas Project No.: AST-2024-215 | Datez 511512024 T I I T I I 2 3 4 5 6 7 8 9 l0 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 9:36 9:38 9:41 9:43 9:45 9:47 9:50 9:52 9:54 9:56 T I t I Injection Start Time Parameter H,S Uncorrected Run Average (C.5.)0.00 Corrected Run Average (Corr)0.00 I I I r t I T t I t T I T I I T T t I F:Allarce Run 8 Data Location: Silver Eagle Refining - Woods Cross Refinery Source: Flare/Fuel Gas Project No.: AST-2024-215 I Date: 511512024 0.01 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 9:59 l0:01 l0:03 l0:05 l0:08 l0:10 l0:12 l0:14 l0:17 Injection Start Time 24 of 54 Run 9 Data FAliarrce I I I T T t T I T I t I I I T I T I t Location: Silver Eagle Refining - Woods Cross Refinery Source: Flare/Fuel Gas Project No.: AST-2024-215 | Date: 511512024 l0: l9 l0:21 l0:23 l0:26 l0:28 l0:30 l0:32 l0:35 l0:37 0.00 0.00 0.00 0.00 0.00 0.00 0.01 0.00 0.00 I 2 3 4 5 6 7 8 9 Injection Start Time Parameter HzS Uncorrected Run Average (Co6"l 0.00 orrected Run Average (Corr)0.00 25 of 54 I I I t t I t T I t t t I I I t I I I ! ___=- AlilarrcE) I souRCE rESrrNG Location: Silver Eagle Refining - Woods Cross Refinery - Retest H2S Summary * Delimiter for runs not used in RA calculations Confidence Coefficient, CC cc : l:r*=. rrllJn Iwhere, I I I t I I I I T I I t I t I I bqzs 2.306 : degrees of freedom n --il= number of runs selected for calculating the RA Sd 0J0 = standard deviation ofdifference CC 00000 = confidence coefficient Relative Accuracy, RA Ll I nean diferer el*l +J, (&O I .p-r = l{n |,rm .15 or RM where, mean differen."10.:50: average difference of Reference Method and CEMS tosz: 2.306 : degrees of freedom n T= number of runs selected for calculating the RA Sd 0.00 : standard deviation ofdifference AS 162 : applicable standard RA 000 : relative accuracy 27 of 54 Run No.Date Time Reference Method H2S ppmvd CEMS H2S ppmvd Average Difference ppmvdStartEnd I 2 J 4 5 6 7 8 9 l0 5/3 5/3 st3 5t3 5t3 5t3 st3 513 5t3 513 t24 124 124 124 124 124 124 124 t24 /24 l0:46 I l:21 I l:56 l2:31 l 3:13 l3:48 l4:23 l4:58 l5:33 l6:08 l:17 l:52 2:27 3:02 3:44 4:19 4:54 5:29 6:04 6:39 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 -0.50 -0.50 -0.50 -0.50 -0.50 -0.50 -0.50 -0.s0 -0.50 -0.s0 0.50 0.s0 0.50 0.50 0.50 0.50 0.50 0.50 0.s0 Average 0.00 -0.s0 0.50 Standard Deviation (Sd)0.00 Applicable Source Standard (AS)t62 Confi dence Coeffi cient (CC)0.000 Relative Accuracy (RA)0.3l%o Acceptability Criteria - Applicable Source Standard <l0Yo Performance Specifi cation Method PS 7 (RM l5) acIa&rE\o&idEe&z ;i @ 6 io 6 -\ o \ o \6 O6h \ o ii o o ;i € o . X- o Ia e a! ! Xo s ; -i a.i N€ r 6o - ooFF gE r 46 6 C6GCU oot(- )0.o./ ) NdNFozoLA. 6rl?eo6I!Loa oo&hoo&e(JoBu.Eogd€L! )o:E*,l CEcioao(a ) (a ) rdo;t)I I \l g =( IIIIItItIIIIIIIIIII 28 of 54 anErrce T I Run I Data Location: Silver Eagle Refining - Woods Cross Refinery - Retest Source: Flare/Fuel Gas Project No.: AST-2024-215 I Date: 5/3112024 I 2 3 4 5 6 7 8 9 l0 T I I l0:46 l0:49 l0:53 l0:56 I l:00 I l:03 I l:07 I l:10 I l:14 I l:17 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 I I I I Injection Start Time Parameter H,S Uncorrected Run Average (C"n.)0.00 Corrected Run Average (Corr)0.00 29 of 54 I I I u=Allanrce!;()UBcL IL.9rrN(i Run 2 Data Location: Silver Eagle Refining - Woods Cross Refinery - Retest Source: Flare/Fuel Gas Project No.: AST-2024-2151 Date: 513112024 I I 2 3 4 5 6 7 8 9 t0 I l:21 ll:24 I l:28 I l:31 I l:35 I l:38 ll:42 I l:45 I l:49 ll:52 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00I I I I I I I I I I I Injection Start Time 30 of 54 I I FAIiarrce Run 3 Data Location: Silver Eagle Refining - Woods Cross Refinery - Retest Source: Flare/Fuel Gas Project No.: AST-2024-21 5l Date:5/3112024 I I 2 3 4 5 6 7 8 9 l0 I l:56 I l:59 l2:03 l2:06 l2:10 l2:13 l2:17 l2.,20 l2:24 l2:27 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00t I I I I I t I I I Injection Start Time Parameter H,S Uncorrected Run Average (Co6.)0.00 orrected Run Average (Corr)0.00 3l ot54 Al6rce Run 4 DataI t t I Location: Silver Eagle Refining - Woods Cross Refinery - Retest Source: Flare/Fuel Gas Project No.: AST-2024-21 5 I Datez 5l3l/2024 I 2 J 4 5 6 7 8 9 l0 l2:31 l2:34 l2:38 l2:41 l2:45 l2:48 l2:52 l2:55 l2:59 l3:02 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 I I t I Parameter H,S Uncorrected Run Average (Co6.)0.00 Corrected Run Averase (Corr)0.00 I 2 3 4 5 6 7 8 9 l0 I T I T t I I I I t I I I I I I I I I =AIIalrce Run 5 Data Location: Silver Eagle Refining - Woods Cross Refinery - Retesl Source: Flare/Fuel Gas Project No.: AST-2024-21 5l Date: 5/31/2024 l3: l3 l3: l6 13:20 13:23 13:27 I 3:30 l3:34 13:37 l3:41 l3:44 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 Injection Start Time Parameter H,S Uncorrected Run Average (Co6r)0.00 Corrected Run Average (Corr)0.00 33 of54 I 2 3 4 5 6 7 8 9 l0 I I I I I I T T I I t t I I I t t I T Aliarrce !irJUfrof I Ll.j1!N(;Run 6 Data Location: Silver Eagle Refining - Woods Cross Refinery - Retest Source: Flare/Fuel Gas Project No. : AST-2024-21 5 I Date: 513112024 I 3:48 l3:51 l3:5 5 l3:58 l4:02 l4:05 l4:09 l4:12 l4: l6 l4: l9 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 Parameter S Uncorrected Run Average (Co6,)0.00 Corrected Run Average (Corr)0.00 34 of 54 I T t T T t T T T t t I I T T I I I I Al6rce Run 7 Data Lo."tion, Source: Flare/Fuel Gas Project No. : AST-2024-21 5 I Date: 513112024 I 2 J 4 5 6 7 8 9 l0 l4:23 l4:26 l4:30 l4:33 l4:37 l4:40 l4:44 l4:47 l4:5 I l4:54 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 Parameter H Uncorrected Run Average (Co6,)0.00 Corrected Run Average (Corr)0.00 T I T t I I I t T T I I t I I I I I T FAlIanrce Run 8 Data Location: Source: Project No.: Silver Eagle Refining - Woods Cross Refinery - Retest Flare/Fuel Gas AST-2024-2151 Date:513112024 I 2 J 4 5 6 7 8 9 l0 l4:58 l5:01 I 5:05 I 5:08 l5:12 l5:15 l5: l9 l5:22 l5:26 l5:29 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 Injection Start Time 36 of 54 T I I 4AIlarce Run 9 Data Location: Silver Easle Refining - Woods Cross Refinery - Retesl Source: Flareffuel Gas Project No.: AST-2024-21 5l Dile:5/3112024 t I 2 J 4 5 6 7 8 9 l0 I 5:33 I 5:36 l5:40 I 5:43 l5:47 I 5:50 I 5:54 I 5:57 l6:01 l6:04 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 T I I t I t t I I I I I I I lnjection Start Time Parameter HzS Uncorrected Run Average (Co6.)0.00 Corrected Run Average (Corr)0.00 37 of 54 FAliarrce Run 10 Data I 2 3 4 5 6 7 8 9 l0 I I T T I I I I T T I I T I T I t Location: Source: Project No.: Silver Eagle Refining - Woods Cross Refinery - Retest Flare/Fuel Gas AST-2024-2151 Datez 5l3l/2024 l6:08 l6:l I l6: l5 l6:18 l6:22 l6:25 l6.,29 l6:32 l6:36 l6:39 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 Parameter HzS Uncorrected Run Average (Co5.)0.00 Corrected Run Average (Corr)0.00 *'.'O* OF AIR OUALITY 39 of54 pJ/lTarEE! SOURCE TESTING Locetion: Silver Eagle Refining - Woods Cross Refinery QA/QC Source: FlardFuel Gas Project No.: AST-2024-2 I 5 I Dcvice GC-FPD Meke SRI Modci 8610c i/N N 12148 Compound Bonle lD Concentration ExDirution Date Mol.htt. H2S cc475645 481.9 r/3t2026 34.08 - I Allarrce Cal QA Location Silver Eagle Refining - Woods Cross Refinery Source Flare/Fuel Gas- JUUII t Project No. AST-2024-2151 Date: 5/1512024 Time: 7:30 Notes: ***Calibration injections are reanalyzed using the calibration curve "**No injeciton can vary from the mean of all 3 injections by >5% "**Chromatograms from calilbration injections are contained in the appendix H2S Conc. (ppm) High Level Calibration Standard 100.00 Conc. (ppm) Mid Level Calibration Standard 50.00 Injeclion RT AC 94 l'ariation RT AC 96 Variation I 1.519 19676.8 l.4o/o 1.558 t3t02.7 l.lo/o 2 1.518 20056.4 0.5%1.560 12845.8 0.9Yo J 1.517 20128.6 0.9%1.559 t2920.5 0.3Yo Mean 1.518 19953.92 1.559 12956.36 4l of54 I I I I I t I I I I I I I I I I I I I Al6rrce Recovery-Drift QA Location: Silver Eagle Refining - Woods Cross Refinery Source: Flare/Fuel Gas Project No.: AST-2024-2 I 5 I Recoverv Correction Factor I S.Sl GC Drift (Using H25 Gas) Pre-Test Post-Tesl Date 5^512024 Date 5n5t2024 Time 8:10 AM Time I l:50 AM Injection #Measured Concentration (ppm)% l'ariation Measured Concentration (ppm)% Variation % Drift I 6.84 2.60/o 12.14 3.5o/o 43.7% 2 6.22 ll.4Yo 2.45 l.lo/o 50.0o/o 3 8.00 14.0%3. l6 4.60/o 39.2% Mean 7.02 2.58 44.30h Pre Test System Recovery (Using H2S Gas) Date s/1st2024 Time 8:10 AM Injection #Measured Concentration (ppm)94 l'ariation Gas Concentration 7o Recovery I 6.84 2.60/o 50.00 3.7o/o ,6.22 lt.4%2.4o/" 3 8.00 14.0o/o 6.0o/o Mean 7.02 4,00 Post Test System Recovery (Using H2S Gas) Datr 5il5/2024 Timr I l:50 AM Iniection #Measured Concentration (ppm)o% l'ariation Gas Concentration 7o Recoverv I t2.14 3.5o/o 50.00 24.3o/o 2 12.45 l.lo/"24.9o/o 3 13.t6 4.60/o 26.3% Mean 12.58 25.2v, 42 of 54 CERTIFICATE OF ANALYSIS Grade of Product: EPA ALLIANCE SOURCE TESTING LLC, E02Nt99E15A2965 cc475645 124 - Pasadena (SG06) - TX 432023 H2S,BALN I I I I I I I T I I t I I I I t I I I Aitgas an Air Liquide company Airgas Specialty Gases Airgas USA LLC 98ro BAYAREA BLVD Pasadena, fi 75o7 Airgas.com Customer: Part Number: Cylinder Number. Laboratory: PGVP Number: Gas Code: PROTOCOL STANDART) Reference Number: 163-402877350-1 Cylinder Volume: 144.0 CF Cylinder Pressure: 2015 PSIG Valve Outlet: 330 Certification Date: Nov 03, 2023 Expiration Date: Nov 03, 2026 Certification performed in accordance with "EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)' document EPA 6OO/R-1 2/531 , using the assay procedures listed. Analytical Methodology does not require correclion for analytical interference. This cylinder has a total analytical mole/mole basis unless otherwise noted. The results relate only to the items tested. The report shall nol be reproduced except in full withoul approval of the laboratory. Do Not Use This Cylinder below 100 psig, i.e. 0.7 Triad Data Available Upon Request Sianatrrre on file ANALYTICAL RESULTS Actual Protoco! Total RelativeConcentration Method Uncertaanty HYDROGEN SULFTDE 500.0 PPM 487.9 PPM G"l +l- 1.4o/o NIST Traceable 1012712023, 1110312023 NITROGEN Balance CALIBRATION STANDARDS Type Lot lD Cylinder No Concentration NTRM 12010315 ND.{6373 304.5 PPM HYDROGEN SULFIDE/NITROGEN +I.1.OO/O MAT22,2026 ANALYTICAL EQUIPMENT lnstrumenUMake/Model Analytical Principle Last Multipoint Calibration AAI OMA-406H NDUV Oct 19,2023 Approved for Release 43 of 54 Page 1 of 1 plllfarpe SOURCE TESTING QA/QC Locetion: Silver Eagle Refining - Woods Cross Re Sourcc: Project No.: AST-2024-21 5l Device GC-FPD Make SRI Model 8610c i/N N 12148 Compound Boule ID Concentration EtDiration Dale Mol./wt. H2S DT002 I 67 I 298 4/19/202s 34 08 I I FAllanrcesirirrroL rLriirN,, CaleA Location Silver Eagle Refining - Woods Cross Refinery - Retest Source Flare/Fuel GasI Juur I Project No. AST-2024-2151 D*e: 5/3112024 Time: 9:53 I t I I I I t I I I T I I I I I ***Calibration injections are reanalyzed using the calibration curve **"No injeciton can vary from the mean of all 3 injections by >5% '**Chromatograms from calilbration injections are contained in the appendix H2S Conc. (ppm) High Level Calibration Standard 50.00 Conc. (ppm) Mid Level Calibration Standard 25.00 lniection RT AC o% Variation RT AC ?5 Variation I 566 7134.3 0.0%1.568 1975.6 0.8o/o 2 567 7143.5 0.lo/o 1.568 195 l .0 0.4o/o J 568 7127.0 0.lYo 1.569 1950.4 0.4o/o Mean .567 7134.96 1.568 195 8.99 45 of54 I t I I I I T T t I I I I I T I I I I FAl6rrcesolrncF r:sr NG ReCOVefy-Dfift QA Location: Silver Eagle Refining - Woods Cross Refinery - Retest Source: Flare/Fuel Gas Project No.: AST-2024-215 I Correction Factor I 1.05 GC Drift (Using H25 Gas) Pre-Test Post-Test Date 5t3v2024 Date 5t3v2024 Time l0:04 AM Time 5:00 PM Iniection #Measured Concentration (ppm)o% l'ariation Measured Concentration (ppm)ok l'ariation o/o Drift I 25.46 O.5o/o 25.59 l.9o/o 0.50/o 2 25.28 0.2%26.02 0.30/o 2.8% 3 25.28 0.2%26.68 2.20/o 5.3o/o Mean 25.34 26.10 2.90/. Pre Test System Recovery (Using HrS Gas) Date 5/31t2024 Time l0:35 AM Iniection #Measured Concentration (ppm)% l'ariation Gas Concentration 7o Recovery I 22.41 l.5o/o 25.00 89.60/o 2 22.92 0.8%9t.7% 3 22.91 0.7o/o 91.60/o Mean 22.15 9l.Oo/" Post Test System Recovery (Using HrS Gas) Datt 5t3U2024 Timt 4:46 PM Iniection #Measured Concentration (ppm)% l'ariation Gas Concentration 7o Recovery I 23.34 t.5% 25.00 93.4o/o 2 23.85 0.60/o 95.4o/o 3 23.92 0.9o/o 95.70h Mean 23.71 94.8Y. 46 of 54 I Linde Gas & Equipment lnc. 5700 S. Alameda Street Los Angeles CA 90058 Tel: 323-585-21 54 Fax: 714-5426689 PGYP lO: F22022tDocNumber: 462215 I CERTIFICATE OF ANALT,SI.S / EPA PROTOCOL GAS t Customer &. Order Informilion NEXAIR 1 385 CORPORATE AVE MEMPHIS TN 3A132.1723 Ce iilicate lssuance Date : 0412012022 Ltnde Otdet Numbq 65563707 Pad Numbet Nl HS300E-AS Cuslomet PO Number 8565536 Fiil Date:0312912022 Lot Nutubet 70086208802 Cylindet Style & Outlet AS CGA 330 CylinderPrcssurc and volume 2oOOpsig 140tt3 Cer Concenlration ProSpec EZ Cert g.qIExpiration Date: Cylinder Number: o4t19t2025 oT0021671 Nt5 I traceaore Expanded Uncertainty 298 ppm Balance Hydrogen sulfide Nitrogen t4ppm I T Certifi ca t i o n I nformatio n :Ceftification Date.0411912022 Term. 36 Months Expiration Date. 0411912025 Thrscylinderwascentfeda@ordingtothe20l2EPATraceabrlityProtocol,Document#EPA-600/R-12/531 usrngProcedureGl Un@rtarntyaboversexpressedasabsoluteexpanded unertainty at a level of @nfiden€ of approximalely 95% with a coverage factor k = 2 Do Nol Use thrs Standa.d rf Pressure is less than 100 PSIG I Analvticsl Data: 1, Componena: (R=Releren@ Standard Hydrogen sullide Z=Zero Gas C=Gas Candidale) I Requested Concentratronr 300 ppm Cenified Concentration 298 ppm Referonce Standard: fype I Cyli^de. t GMIS / DT0009254 Con€ntratron / Uncertarnty 251 ppm t2 ppm Expiration Date 07117/2024 lnstrument Used Ametek Senes 9900 S/N ZW-9900-S1330-1 Traceable to:SRM # / Sample # / Cyhnder # PR|\il l C21 O34O1 1 0547 47 4 SRM Concentration/Un@rtainty 4004 ppm /132 ppm SRM Expirairon Date O5l2Ol2O24 Analyti€l Method UV Spectrometry Last Mulhpornt Calibelion 0312812022 I : Date 0411212022 Zt o R: 251 C: 298 Conc: 298 R: 251 Zt O C: 297 Conc: 297 Zi O C: 297 R: 252 Conc: 297 UOM: ppm Mean Test Assay: 297 PPm Second Analysi3 Data; Date 0411912022 Z: O R: 251 C: 300 Conc: 300 R: 251 Zi O C; 300 Concr 300 Zt O C: 301 R: 252 Conc: 301 UOM: ppm Mean Tesl A33ay: 300 ppm I r I,lr ].' A, I Analyzed By Jo3e Va3quez Certilied By I I t I I T of the use of the infomatron contarned herein exceed the fee established for providing such infomalion I 47 ol 54 t I I t 48 of54 T I I I I I t t T t t I t I I t T T t 49 of54 .l q I I Q I q 9. 9 9. 9 9 9 9 9.9 9 9 9.9 I S !!! ! s ! 3 9 3 S ! 3 ! 3 3 ! ! ! ! r ! 9! 9 9 ! ! ! ! 9 ! ! 9 ! 9 ! 9 9 9 ! 9 ! 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" 9 " 9 + + 9 q " " " " e 9 9 9 " q 9 9 9 66 n 6 6 n 6 h h 6 6 6 6 6 6 6 0 6 n n 6 h 6 h 6 6 6 h n n o n e" + e e + + + + e i e i + + + + e e + + + e + + + + + e + + + 66 6 6 6 n O 6 6 6 6 6 6 4 h n 6 h h h 6 6 6 0 6 4 6 6 n 6 6 6 ee e e + + + + e e Q + e e e e + e + e e " Q e + e + e Q e " e d6 o d N d c n @ N @ o o d d 6 t n 9 F @ o o d N 6 q 6 o F 6 o < e 66 o 6 l,l n 6 h 6 !i OO oo Oo o oo O d d H d d d d d H i di li i # di di di # di di di di di , U { .U + s { + s + r + r $ s e s + s € e i:: a * H d d d d d H t i i d d d d d d H d d d i i d d d d d qs s s q q gs s s s s s s s s s s s s $ s q s < s 9 9 s 9 9 s dN N N N N N d N N N N N N N N N N N N N N N N N N N N d N N d Fa i - i - F i d H d d H d d i d d d d d d d d i H d d d d d il d H d i o6 6 0 0 6 0 m 6 m 6 m 6 6 m 6 6 m O m O m O 6 m 6 6 6 6 m 6 m \< \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ > \ \ \ \ 66 6 6 6 6 6 6 6 6 6 6 h 6 0 6 6 6 n n h n 6 6 6 6 6 6 h 4 0 6 o 9 o o N @ o o d N m v 6 @ N @o o i N o s 6 @ r: a o Q n q{ . ! s .i : i : d : AN Nd d d N N N N N o m m m o m m 6 o m < s $ q I # di di di di di di di di di di di ri i ii di di di di di di di di di di ii di di di di di di di dH d H H d d d d d d d i i d d d d i H i i d a ss s q s s 9 9 9 q s s 3 9 q s 9 9 s s v s $ t 9 $ 9 9 s s $ $ N. i d N N N NN NN N N Nd N N N N N NN NN N n q r y n n N N N d_ i l d d i H Hd d H a d d d d HH H i H d dd d i d H H H Hd d 6m m m 6 6 6 0 m 6 m m 6 0 6 m 6 6 0 m m 6 6 0 !< < < ! ! \ < < \ \ \ \ \ \ \ \\ \ \ \ \ \ \ 66 6 6 4 6 6 6 6 6 0 6 6 6 6 6 0 0 4 0 0 6 6 6 h 6 6 6 4 4 6 6 iN o < n @ N o o o d N o s 6 @ r @ o o d N o s o @ r @ o o F d ry ] q? ry 1 qr q': * * qr ' t + !! T T I S .: q ' : q r T I n Y) n n n 9l Yl n Yl n ? I 9 Nd N N d N N N N N N N N N N N d N d N N N d N N N N N N O M M .a d dd HH d H Hd d d i d d d dd d dH di dd Hd H H i l a i 9S C I 9S S9 I t S g* t 9t 9 $ S S S 9q I $ tti 9q S S9 dd d N NN N N N N N N N N N N N N N d N N N N N N N N 6m d 6 m 6 6 d m d m d 6 0 0 6 6 6 0 0 6 m o d 6 6 m o o o o o h6 h 6 6 6 6 6 6 6 6 6 6 6 0 6 6 6 6 6 6 6 0 6 4 h 6 n 6 6 6 6 Nl-l E ol r 6 h6 6 n 6 6 6 6 6 4 4 4 6 6 6 6 h O 6 6 4 6 6 6 6 6 6 6 6 0 h 6 €l ; i e" p e Q + " ? 9 9 9 9 e e e 9 " 9 " 9 9 q 9 ? e e + e e e + q 6l > flrl @N 6 6 0 H N 6 < h@ N 6 0 0 H N 6 < h@ F @ O o i N 6 S 6 9 N h6 h 6 o o o o o o o o o o H d NN N d N N N N J J ; J ri n 6i 6i ^i Ai ni ^i ^i n ^i ^i n ^i ^i ^i ^i ^i ^i ^i ^i 6i . i . . i Fi 6i Fi ^i iii H d H d d d d d i d H i i i d d d d d d H d H d i qs 9 s 9 { s < n 9 < 9 s < s q q s $ 9 s 9 $ s s 9 { 9 $ s s s AN d N N N N N N N N d N d N N N N N N N N N N N N N N d d N N \\ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ dd H H d H d d i d d d d H i d d d d H d H H H d d d d d d H H mm d 6 m 6 m m o 6 m m o 6 6 6 6 6 0 0 6u i 6 6 6 6 6 6 6 h 66 6 6 6 n h 66 66 6o h4 4 h 46 6 4 6 Hd 6t 6@ r € OO dN ot 6@ F 6O O i N m I o @ N QO O El N q! c'i I q! c, l |1 n e c! q- r q! q! ql c! e e e ry ] e I g a a : I 9 a I T Y! n n dd d i d H d d d d d d H d d d d H H H H A d d d H d i d d d H Hd d i H d H d d d i l d i d d d d d d d < d d d H H d d d d d d s9 r 9 { t t n $ $ s 3 $ $ $ q s q s c s t t t s s 9 t 9 9 c s NA N d N N N N N N N N N N N N N d N N d N N N N N N N N N N N \\ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ d- i l - i - H H d d H H H d d d H d d d d d d H d i < H d d d d d d d 6m m m i l d m 6 m m m m m 6 0 6 0 6 d o o m o o << < < < < < < < < < < < < \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ 66 6 6 6 6 n 4 n 6 6 h h 6 6 6 h O 6 6 6 6 6 6 6 6 n 6 6 6 6 6 @N Q O O d N m S 6 A r @ O O d N m 9 6@ r 6 O O d d m q 6 @ N I :C I I q1 Y- l Yt ql Y) !1 Y) Y- l !n Yr I I I I I 9 I I C I n n n n n n n n oo o o o o o o o o o o o o d d H d d d d d d d i d d d d d H H Fid H H H H i H H d H d i H d H d H H H H H H d i d d i d i i gq 9 r $ s 9 i q 9 q s q s { $ 9 t $ $ s $ 9 s s s s $ q + ( s NN N N N N N N N N N N d N d N N N N N N d N N N N N N N N d d \\ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ dH d H d d H H d d d d d d d H d H H d H d d d H d d d i H d i o6 6 6 0 m 6 6 m O m 6 0 0 6 0 6 0 6 0 6 m O 6 0 m m f i md d 6 \\ \ \ \ \ \ \ \\ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ 66 6 h 6 6 6 0 h O O O O 4 6 6 h 6 6 6 h h h O O 6 0 6 0 6 6 h Nl-l EEI * E El > ro t ,i l tr l d El 3[ EEs*es rl E .E l * 3 El = tr l El cl d El 3xEE dJdxAE EI E .E | 3 E El = sf l ,i l cl d El 3xEEsi e5 EI E .f l * I EI E NI EI cl d El 3XEE fies NIEI E6l * ts El > t{ l ,? l cl d El 3: EE <JdxPE III 6h n 6 0 6 6 6 6 6 6 h 6 4 n 6 6 6 6 n 6 6 n 4 6 0 h n 6 6 6 6 e+ + " + + e " + e " " + e e + + e + " + + + + + e e e e + ? e f} . ! lcl :r lEI o(9c,)lJ -Ol F{ 6t n8B63 6OEo n o-ot 2 o.t ri o - cFcfEXau ( ! E> (U g bD Jl ,I g !( EgoEf , d,<tNoN(!E (! , .>( , ;(L5 fies 52 ol 5 4 66 6 6 6 6 6 6 6 h 6 6 6 6 6 6 6 6 6 6 6 6 0 4 6 6 0 6 0 6 n O c; c, c, ci ct ci o o d c, cj o o o c, c, c, cj o o o o o o c, cj cj d I e o d -li i - - i i 60 4 6 6 6 4 6 6 6 6 4 6 6 6 6 06 h h 6 0 6 6 6 6 6 h h 0 0 0 d ci ci ci d ci ct ci o o o o d ct c, o o o o d ci d d ci ct ci o d o o d o -i- i iN m * 6 6 N @ 6 O d N 6 < 6 @ r @ O O H d O 9 6 @ F 6 O O d N ni \ i N ^ l - - N - N o o 6 6 . a o m md m g g st + q q q <{ 66 6 n ^i ^i ^i ^i & Fi Fi 6i .,, i 6i 6i .. i ", i 6i & .i ^i ^i ^i ^i n .i n n .i .i ^i & .. i 6i 6i i- : ; i ; H H d H d d d d H d H i i d d d i H d d i < d d H d dc a a s < s v q s v s s s s 9 s s s s s s s s s s s q q s s s NN N N d d d d N d N d d N d N N N N N N N N N N N N N N N N N ui ui 6- ui 6- ui 4- 6- 6- si 6- 6 6 h h 6 6 6 h h 6 n 6 6 h 6 6 6 o 6 n h -- - - - d i H H H d d d H d d d H d d i d H d d d d d d i d H 6- h - 6 - 6 - 6 - 6 6 n h 6 n 6 0 6 6 6 0 6 6 0 6 6 4 6 6 6 0 0 6 n 6 6 oH N m < 6 @ N 6 O O H N O $ 6 Q F @ O O d N 6 S 6 @ F 6 O O i 6o o o c , o o o o o dH d d d d dd H d d N N N d N d N N N m o ^: 6i 6i ri "i 6i ^i ^i ^i ^i ^i ^i .i 6i 6i 6i 6i ^i ^i ^: .i ^i .. i ^i ^i ^i 6i ^i .i .i ^i .i dd H d d d i d d H d H i d d d d H H a d H d i d d d d d i d d 9q { 9 S S < 9 S 9 9 S t S S S S q S S 9 9 q 9 S 9 9 S S 9 9 9 N NN N ' ! NN N N N NN N N N N N N N d Nd N dN d N i N N N d ;; ; ; ; ; . ; ; ; ; ; ; ; ; ; ; . ; ; ; ; ; ; ;; . ; ; ; ; ; > ; ; dH H d d d d d d d a H H H H d i H H d d d d d i H d d i d d i \< \ < \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ > \ \ \ \ \ \ \ \ \ \ \ \ rih 6 n 6 6 oo h6 6 6 64 64 6h o6 6 h 6 6 4 66 6 4 6 6 6 @o o d N m t n @ r o o o d N o s 6 9 r @ o o d N o $ 6 @ r a o 9 I a n n n n n :1 n n n .i n c !! c! q! cl * * |! e q] e q. 1 n ql e q] ql ql @@ @ @ @ a @ @ @ @ @ @ @ @ @ @ @ @ @ @ @ 9 0 @ @ @ a @ @ @ @ @ iid H d d d d H H H H H d H d d d H H H d H d d d d d H i d H {s 9 s s s s 9 s s € 9 q 9 { t s $ s $ s t s q q 9 9 t $ c $ $ dd N N N N N N N N N N N N N N N N d N N N N N N N d N d N N N d- H - H - H - d - d d d d H H d i d d d d d d H H i H d H d d d d d d H 6 m d o6 o o 6 m m 6m m 6 o6 6 o om 6d 6 o 6 om o ! n o 6 6 << < \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ fi6 - 6 - 6 - h - 6 _ 6 6 6 6 n h 6 6 0 n O O n h h O 6 6 6 6 n 6 6 h 6 h ss H S h n s g + s 9 s ss 5 s g 3 f i fr 33 R t s h 3 s 8 3 3 3 3 r; J' i 6 ra d, i i. i r; fi {; fi fi ,. i l; d'i fi fi r; r; r; fi th , i ' i , i ' i .; d' i fi fi 6 .b 6 6 li i dH H d d a d r H d H d H d d d d d H H H d H d d H d d d d d d $q 9 9 9 q 9 $ 9 q S 9 S q q S 9 9 q S 9 9 S < $ 9 q 9 S S 9 q NN N d N N d N N N N N N N d N N N d N N d N d N N N N N N N N did d H d d H H d i d H H i d H d i H H H d d d d d i mm m m 6 m 6 m 6 0 0 m m o 6 m m 6 6 0 0 0 0 6 6 m m m 6 6 d o \\ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \\ \ \ \ \ \ \ > > > \ 44 6 6 6 6 6 6 h 4 6 0 6 6 h h 6 h 4 4 6 6 6 6 6 6 6 6 6 6 6 4 @6 O H N O $ 6 @ F € O O H N 6 9 6 @ F @ O O d N m 9 6 @ r 6 O 66 O O O O O O O O O O H H d d d d d H H i N N N N N N N N N N .+ - ii ' h ri i, i rh fi ni U, i di fi fi 'r ' i fi fi 6 fi ri i 6 Ji di Ji fi fi ,i ii 6 fi 6 ii fi fi iii H H H d d d d d H d d H d H d d i i d d d d i H i H d H d si q s 9 9 9 s q s t s { $ s ( 9 { $ q t s n t € t < 9 s € q 9 NN N N N N N N N N N d N N N d N N N N N N N N N NN N N N N N \< \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ d- i - J d - t - l - i - d - d H d d H d i a d H il i i d d H H t d d d d d d m6 6 6 m m m m m m m 6 m o o o o m 6 m 6 6 0 0 6 m 6 m m m m m !< < < < < < < < < < \ < \ \ \ \ \ \ \ \ \ \ \ \\ \ \ 6 6- 6 6 h h 66 66 66 6 h 66 6 6 6 6 6h 66 6 6h 6 6 h6 h mq 6 @ r @ o o d N 6 9 6 @ N Q O O H N m S 6 @ r @ O O d d m q I. l c J q ! n l c ! * q 1 q1 q: q l q l q ) r y ) e r y ' ) r 9 I * S I S * I S S Y - 1 g) ! 1 Y- 1 9l {9 q q q 9 9 9 $ t $ ( $ 9 S q q 9 S 9 g $ $ t S 9 $ $ $ 9 t S iH i H d d d i d H i i H d d d d d d H d d i d H H d d H H d d s9 { q 9 s q 9 s s 9 q t s q g 9 9 9 s s s 9 q q 9 t $ 9 9 t 9 NN N N N N N N N N N d d N N N N N N N N N N N N N N N Hd i H H H d d d H d d H A d d H H H H H d d H m6 6 6 0 6 0 0 0 6 0 0 m o m 6 6 6 6 0 0 0 0 d 6 0 6 6 6 d m m \\ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \\ \ \ \ \ \ \ 66 6 6 6 6 6 6 0 h 6 h O 6 6 6 h 6 6 6 6 6 6 6 6 6 h O 6 6 h 6 Nlrl EEI * E sl El = tr l 9u ; a i3E=fies -l E .E l * $ EI E =l El El Xg al E: E=fiPS II dlrl E .E l 3 ts 3t El = El ie sl E;Ei es -l E6l * $ al E or t al cl d El 3x F<c4fioS e1 dlrl eEI * E al > @r il -tst c ,El 3: EE fie= -l esl : ts -r l = r\ l ,? l tr l d El 3: EEsi eg 66 6 6 6 h 6 6 6 6 6 h h O 6 S h h 6 6 6 6 4 h O 6 n 6 6 6 6 6 e+ + + e e + e + " + e + + + + + e e ? + e e " + + e + " e + + 6t! (9o))ILOr F{ vl l n 9l n eo i 63 6OE, od o-ot2o r dD - CFEJ i= xsg (U s EE ,I g t( Ego6g E,<lot! 66 4 0 6 6 6 6 4 h 6 6 0 6 6 6 6 6 6 6 6 6 6 6 h 6 6 6 6 6 6 6 ci d ci d ci ci o c, c, o o o ci o d ct c, c, ci o ci ci o d o o d d d c, ci ci 4u ! u l u l s _ 1 u- l 4u - l 4u . ! v l v l u ' l u : u l v 1 v! v ) u l 4q r ) 4 u l 4u - 1 sl u : u ? u l 4s ) ?9 9 9 9 e 9 9 ? 9 9 9 9 9 ? 9 9 9 9 9 ? ? 9 9 9 9 9 9 9 ? ? 9 j=r$OE>os5 cl -a S i! pB3 oFE3 EE s eI u t u l 4u ! 4 q 4 u _ l u) u ) 4 ' 4 v ) 4 4 u - 1 ul u l 44 4 u l 44 u ) 4 u ) u ) 4 4 ?9 9 9 9 ? ? ? 9 9 ? 9 ? 9 9 9 9 9 9 9 9 e 9 ? 9 9 P 9 ? ? ? ? 53 ol ' 5 1 LJTAH DEPARTMENT OF E NVI Ro N tvlE NTAL OUALITr JUL - 1 n24 DIVISION OF AIR QUALITY 54 of 54 Division of Air Quality Performance Specification Test - CEMS Certification SO2 Analyzer:Serial No.:3003955197/HOU30075841370010 Acquisition System:Serial No.: Acquisition System:Serial No.: Emission Limitations:162 Test Date Enter Use TRS SO2 H2S Enter Use TRS SO2 Enter Use TRS SO2 5/31/2024 RM CEM Diff RM CEM Diff RM CEM Diff Run#Time End Time 1 10:46 11:17 Y 0.00 -0.50 0.5 2 11:21 11:52 Y 0.00 -0.50 0.5 3 11:56 12:27 Y 0.00 -0.50 0.5 4 12:31 13:02 Y 0.00 -0.50 0.5 5 13:13 13:44 Y 0.00 -0.50 0.5 6 13:48 14:19 Y 0.00 -0.50 0.5 7 14:23 14:54 Y 0.00 -0.50 0.5 8 14:58 15:29 Y 0.00 -0.50 0.5 9 15:33 16:04 Y 0.00 -0.50 0.5 10 16:08 16:39 0.00 -0.60 11 12 13 14 15 16 Average = 9 0.00 -0.51 0.5 0 0 Confidence Coefficient =0.0 Confidence Coefficient = Confidence Coefficient = RA - Relative Accuracy =N/A RA - Relative Accuracy =RA - Relative Accuracy = n = 9 t0.975 =2.306 E.L. Relative Accuracy => % of E.L.0.0%0.3%% of E.L. % of E.L. a For steam generators;b Average of three samples;c Make sure that RM and M data are on a consistent basis either wet or dry. 40 CFR 60 Performance Specification 2 For SO2 and NOx Continuous Emission Monitoring Systems 4. Performance and Equipment Specifications 4.3 Relative accuracy. The RA of the CEMS shall be no grater than 20 percent of the mean value of the RM test data in terms of the units of the emission standard or 10 percent of the applicable standard, whichever is greater For SO2 emission standards between 0.30 and 0.20 lb./MMBtu use 15 Percent of the applicable standard; For SO2 emission standards below 0.20 lb./MMBtu use 20 Percent of the emission standard; Title 40: Protection of Environment PART 60—STANDARDS OF PERFORMANCE FOR NEW STATIONARY SOURCES Subpart J—Standards of Performance for Petroleum Refineries § 60.105 Monitoring of emissions and operations. % O2 Correction (iii) The performance evaluations for this SO2monitor under §60.13(c) shall use Performance Specification 2. Methods 6 or 6C and 3 or 3A shall be used for conducting the relative accuracy evaluations. Method 6 samples shall be taken at a flow rate of approximately 2 liters/min for at least 30 minutes. The relative accuracy limit shall be 20 percent or 4 ppm, whichever is greater, and the calibration drift limit shall be 5 percent of the established span value. Siemens Maxum II Make Selection Select Concentration (ppm) Used Clear Selection ppm dv C ppmdv Division of Air Quality Reference Methods 15 - Determination of Hydrogne Sulfide, Carbonyl Sulfide, & Carbon Disulfide Performance Specification Test Source Information Company Name:Silver Eagle Stack Designation:Fuel Gas Company Contact:Blaine Zwahlen Contact Phone No.801-298-3211 Test & Review Dates Test Date:5/31/2024 Review Date:10/21/2024 Observer:Not Observed Reviewer:Rob Leishman Emission Limits Under Construction form 15 ppm 162 Test Information Y Dry Gas Meter Yc Combustion Meter Dl H @ Pbar Contractor Information Contracting Company:Alliance Source Testing Contact:Charles Horton Phone No.:801-269-0550 Project No. F factors for Coal, Oil and Gas #REF! Diluent UsedMethod 19 - F factors for Coal, Oil, and Gas Fd Fw Fc scf/MMBtu scf/MMBtu scf/MMBtu Clear F-factor Used 10100 9780 9860 9190 8710 8710 8710 10540 10640 11950 320 10610 10200 10390 1970 1800 1910 1420 1040 1190 1250