DAQ-2024-010991

1
DAQC-CI115900001-24
Site ID 11590 (B1)

MEMORANDUM

TO: FILE – MARTIN MARIETTA MATERIALS, INC. – Milford Quarry

THROUGH: Chad Gilgen, Minor Source Compliance Section Manager

FROM: Jared James, Environmental Scientist

DATE: August 28, 2024

SUBJECT: FULL COMPLIANCE EVALUATION, Minor, Beaver County

INSPECTION DATE: June 24, 2024

SOURCE LOCATION: 3.5 miles north of Milford on County Road 163
Milford, Utah.
DIRECTIONS: Approximately 5 miles northwest of Milford.
There is a sign for the source location close to mile marker #4 on
UT-257. Head west on the dirt road for 2.5 miles. Turn right and
head north for one mile to the crushing circuit and a second sign.
Turn left and head west for approximately 500 feet, to the office.

SOURCE CONTACTS: Brady Carter, Plant Manager
435-201-2355 [e-mail]

OPERATING STATUS: Down for repairs on the crusher.

PROCESS DESCRIPTION: Rock is blasted from a mountain quarry and 36" minus rock is
placed into a grizzly by a front-end loader that feeds the material
into a jaw crusher. A surge bin feeds 6" minus rock onto a long
conveyer belt to the crusher system. The aggregate is then
conveyed to a 3-deck scalping screen where the fines and
suitable size rock are separated and placed into separate piles,
one for road base and one for railroad ballast. The balance of the
material is conveyed to a cone crusher for further processing.
From the cone crusher the material is conveyed to a 3-deck
sizing screen. The material that passes through the screen is
stacked into one of three piles. The rock that does not pass
through the sizing screen is sent back through the cone crusher.
This source produces four products: 13/4-inch railroad ballast,
3/4-inch railroad ballast, fines for road base, and 4-inch rip rap
for railroad right of way. Rock used for railroad ballast is loaded
into railcars and shipped to its destination. Road base material is
trucked to local road crews. Water is obtained from a well and
must be conserved. The ballast is loaded onto railcars. Chipped
rock covers the yard and haul roads.

0 0
2
APPLICABLE REGULATIONS: Approval Order (AO) DAQE-AN115900006-16, dated March 3,
2016
NSPS (Part 60), OOO: Standards of Performance for
Nonmetallic Mineral Processing Plants
SOURCE EVALUATION:

Name of Permittee: Permitted Location:

Martin Marietta Materials, Inc. - Milford Quarry
7381 West 133rd Street, Suite 401 3.5 miles north of Milford on County Road 163
Overland Park, KS 66213 Milford, UT

SIC Code: 1429: (Stone, Crushed & Broken, NEC)

Section I: GENERAL PROVISIONS

I.1 All definitions, terms, abbreviations, and references used in this AO conform to those used in the
UAC R307 and 40 CFR. Unless noted otherwise, references cited in these AO conditions refer to
those rules. [R307-101]

I.2 The limits set forth in this AO shall not be exceeded without prior approval. [R307-401]

I.3 Modifications to the equipment or processes approved by this AO that could affect the emissions
covered by this AO must be reviewed and approved. [R307-401-1]

I.4 All records referenced in this AO or in other applicable rules, which are required to be kept by
the owner/operator, shall be made available to the Director or Director's representative upon
request, and the records shall include the two-year period prior to the date of the request. Unless
otherwise specified in this AO or in other applicable state and federal rules, records shall be kept
for a minimum of two (2) years. [R307-401-8]

I.5 At all times, including periods of startup, shutdown, and malfunction, owners and operators shall,
to the extent practicable, maintain and operate any equipment approved under this AO, including
associated air pollution control equipment, in a manner consistent with good air pollution control
practice for minimizing emissions. Determination of whether acceptable operating and
maintenance procedures are being used will be based on information available to the Director
which may include, but is not limited to, monitoring results, opacity observations, review of
operating and maintenance procedures, and inspection of the source. All maintenance performed
on equipment authorized by this AO shall be recorded. [R307-401-4]

I.6 The owner/operator shall comply with UAC R307-107. General Requirements: Breakdowns.
[R307-107]

I.7 The owner/operator shall comply with UAC R307-150 Series. Emission Inventories. [R307-150]
Status: In Compliance. No limits appear to have been exceeded. No modifications have been
made to equipment other than a replacement-in-kind screen which was granted (DAQE-GN115900007-24). Regular maintenance is conducted. No reportable breakdowns
have occurred since the previous inspection. A 2023 emission inventory was submitted to
DAQ.

3
Section II: SPECIAL PROVISIONS

II.A The approved installations shall consist of the following equipment:

II.A.1 Milford Quarry
II.A.2 Jaw Crusher Capacity: 660 TPH Manufacture Date: 2010 NSPS Applicable: Subpart OOO
II.A.3 Cone Crusher Capacity: 528 TPH Manufacture Date: 1997 NSPS Applicable: Subpart OOO
II.A.4 Cone Crusher (New Equipment) Capacity: 300 TPH Manufacture Date: 2001 NSPS Applicable: Subpart OOO
II.A.5 Grizzly Feeder Capacity: 750 TPH Manufacture Date: 2011 NSPS Applicable: Subpart OOO
II.A.6 Belt Feeder (New Equipment) Capacity: 250 TPH Size: 36" x 15' Manufacture Date: 1991 NSPS Applicable: Subpart OOO
II.A.7 Double-Deck Screen Size: 5' x 10' Manufacture Date: 2010 NSPS Applicable: Subpart OOO
II.A.8 Triple-Deck Screen Size: 8' x 20' Manufacture Date: 2011 or newer NSPS Applicable: Subpart OOO
II.A.9 Triple-Deck Wet Screen Size: 6' x 16' Manufacture Date: unknown NSPS Applicable: Subpart OOO
II.A.10 Triple-Deck Screen (New Equipment) Capacity: 650 TPH Size: 6' x 20' Manufacture Date: 2001 NSPS Applicable: Subpart OOO
II.A.11 Various Conveyors
Status: In Compliance. The equipment observed on site was consistent with that listed. The
triple-deck screen 8' x 20' was replaced with a replacement-in-kind
(DAQE-GN115900007-24). The shop also has a heater in the shop that burns used oil during colder months.
4
II.B Requirements and Limitations

II.B.1 The Milford Quarry shall be subject to the following:

II.B.1.a The owner/operator shall notify the Director in writing when the new equipment listed in this AO
has been installed and is operational. To ensure proper credit when notifying the Director, send
your correspondence to the Director, attn: Compliance Section.

If the owner/operator has not notified the Director in writing within 18 months from the date of
this AO on the status of the construction and/or installation, the Director shall require
documentation of the continuous construction and/or installation of the operation. If a continuous
program of construction and/or installation is not proceeding, the Director may revoke the AO.
[R307-401-18]

Status: In Compliance. Previous inspection memos report notification being made by email
on June 13, 2018.
II.B.1.b The owner/operator shall not produce more than 15,840 tons of aggregate material, including
bank-run material, per day. [R307-401-8]
II.B.1.b.1 Records of production shall be kept for all periods when the plant is in operation. Production
shall be determined by belt scale records, scale house records, and/or sales records. The records
of production shall be kept on a daily basis. [R307-401-8]
II.B.1.b.2 The owner/operator shall weigh and account for all aggregate material prior to the aggregate
material leaving the site or being used in another process on site. [R307-401-8]
Status: In Compliance. Records reviewed on site indicated that the daily high production
was 12,226 tons.
II.B.1.c Unless otherwise specified in this AO, the owner/operator shall operate the Milford Quarry only
between 5:00 am and 9:00 pm each day. [R307-401-8]
II.B.1.c.1 Hours of operation shall be determined by supervisor monitoring and maintaining of an
operations log. The records of operation shall be kept on a daily basis and shall include the time the aggregate processing plant starts operation and the time the aggregate processing plant ceases
operation. [R307-401-8]
Status: In Compliance. Standard operation hours are from 6:30 am to 4:00 pm.

II.B.1.d Unless otherwise specified in this AO, the owner/operator shall not allow visible emissions from any source on site to exceed 20 percent opacity. [R307-201-3]

II.B.1.d.1 Unless otherwise specified in this AO, opacity observations of emissions from stationary sources shall be conducted according to 40 CFR 60, Appendix A, Method 9. [R307-201-3]

Status: In Compliance. No significant visible emissions were observed during the inspection.
II.B.2 All Crushers, Screens, and Conveyors on site shall be subject to the following:
II.B.2.a The owner/operator shall not allow visible emissions from any crusher on site to exceed 15 percent opacity, and any crusher on site manufactured on or after April 22, 2008 to exceed 12 percent opacity. [40 CFR 60 Subpart OOO]
Status: Not Observed. The crushing circuit was down for repair.

5
II.B.2.b The owner/operator shall not allow visible emissions from any screen on site to exceed 10 percent opacity, and any screen on site manufactured on or after April 22, 2008 to exceed 7 percent opacity. [40 CFR 60 Subpart OOO] Status: Not Observed. The crushing circuit was down for repair. II.B.2.c The owner/operator shall not allow visible emissions from any conveyor transfer point on site to exceed 10 percent opacity, and any conveyor transfer point on site with the conveyor manufactured on or after April 22, 2008 to exceed 7 percent opacity. [40 CFR 60 Subpart OOO] Status: Not Observed. The crushing circuit was down for repair. II.B.2.d The owner/operator shall not allow visible emissions from any conveyor drop point on site to exceed 10 percent opacity. [R307-401-8] Status: Not Observed. The crushing circuit was down for repair. II.B.2.e The owner/operator shall install water sprays on all crushers and screens on site. Water sprays shall be installed on the conveyor transfer points on site as needed to control fugitive emissions. Sprays shall operate as required to maintain the opacity limits listed in this AO. [R307-401-8] Status: In Compliance. Water sprays are installed as outlined. II.B.2.f Within 60 days after achieving the maximum production rate but not later than 180 days after initial startup, the owner/operator shall conduct an initial performance test for all crushers, screens, and conveyor transfer points on site. Performance tests shall meet the limitations specified in Table 3 to Subpart OOO. Records of initial performance tests shall be kept and maintained on site for the life of the equipment. [40 CFR 60 Subpart OOO] II.B.2.f.1 Initial performance tests for fugitive emissions limits shall be conducted according to 40 CFR 60.675(c). The owner or operator may use methods and procedures specified in 40 CFR 60.675(e) as alternatives to the reference methods and procedures specified in 40 CFR 60.675(c). [40 CFR 60 Subpart OOO] II.B.2.f.2 The owner/operator shall submit written reports to the Director of the results of all performance tests conducted to demonstrate compliance with the standards set forth in 40 CFR 60.672. [ 40 CFR 60 Subpart OOO] Status: In Compliance. The source supplied initial OOO observations via email. The source was directed to maintain those records on site. The new screen is scheduled to have initial observations conducted October 7, 2024. II.B.3 The Bulldozing Operations on site shall be subject to the following: II.B.3.a The following bulldozer operational limits shall not be exceeded: A. 8 hours of operation combined for all bulldozers on site per day. B. Operation shall only occur between 7:00 am and 3:00 pm each day. [R307-401-8]

6
II.B.3.a.1 Hours of operation shall be determined by supervisor monitoring and maintaining of an operations log. The records of operation shall be kept on a daily basis. Records shall include the following: A. The time each bulldozer starts operation each day B. The time each bulldozer ceases operation each day C. The total hours of operation for all bulldozers each day. [R307-401-8] Status: In Compliance. Records reviewed at the time of inspection indicated that bulldozer operation is less than 8 hours per day and between the hours specified. II.B.4 All Drilling and Blasting Operations on site shall be subject to the following: II.B.4.a The owner/operator shall conduct wet drilling when drilling holes for explosive blasting. [R307-401-8] Status: Not Observed. Drilling was not being conducted at the time of inspection. However, Mr. Carter stated that wet drilling is conducted. II.B.4.b The owner/operator shall not blast more than 478,600 square feet per rolling 12-month period. [R307-401-8] II.B.4.b.1 To determine compliance with a rolling 12-month total, the owner/operator shall calculate a new 12-month total for each day of the previous month by the twentieth day of each month using data from the previous 12 months. The area blasted shall be determined by supervisor monitoring and maintaining of an operations log. The log shall contain the following: A. The date of each blast B. The area of each blast C. The rolling 12-month total of the area blasted [R307-401-8] Status: In Compliance. Records reviewed at the time of inspection indicated that the 12-month rolling total was 269,406 square feet. II.B.4.c The owner/operator shall not use more than 1,597 tons of explosives per rolling 12-month period. [R307-401-8] II.B.4.c.1 To determine compliance with a rolling 12-month total, the owner/operator shall calculate a new 12-month total by the twentieth day of each month using data from the previous 12 months. Amount of explosives used shall be determined by purchasing records or maintaining an operations log. [R307-401-8] Status: In Compliance. Records reviewed at the time of inspection indicated that 221 tons of explosives had been used during the 12-month period. II.B.5 All Haul Roads and Fugitive Dust Sources on site shall be subject to the following: II.B.5.a The owner/operator shall not allow visible emissions from any storage pile on site to exceed 10 percent opacity. [R307-401-8] Status: In Compliance. No visible emissions were observed from the storage piles during the inspection.
7
II.B.5.b The owner/operator shall not allow visible emissions from haul roads and other fugitive dust sources on site to exceed 20 percent opacity. [R307-205-4] II.B.5.b.1 Visible emission determinations for fugitive dust emissions from haul-road traffic and mobile equipment in operational areas shall use procedures similar to Method 9. The normal requirement for observations to be made at 15-second intervals over a six-minute period, however, shall not apply. Visible emissions shall be measured at the densest point of the plume but at a point not less than 1/2 the vehicle length behind the vehicle and not less than 1/2 the height of the vehicle. [R307-205-4] Status: In Compliance. Only minimal dust was observed from haul traffic and operational areas during the inspection. A water truck was in operation throughout the inspection. II.B.5.c The owner/operator shall use a chemical dust suppressant on all haul roads and operational areas on site. The owner/operator shall use water application to supplement the chemical dust suppressant and maintain opacity limits listed in this AO. The owner/operator may stop applying water to the haul roads and operational areas on site when the temperature is below freezing. [R307-401-8] II.B.5.c.1 Records of chemical suppressant and water application shall be kept for all periods when the plant is in operation. The records shall include the following items: A. Date and time treatments were made B. Dilution ratio and quantity of water/chemical suppressant applied C. Rainfall amount received, if any D. Records of temperature, if the temperature is below freezing. [R307-401-8] Status: In Compliance. Records of watering were made available for review during the inspection. The source has a 4,000-gallon water truck on site. MgCl was applied to the haul roads on May 24, 2024, with another application scheduled for August 31, 2024. II.B.5.d The owner/operator shall apply water from conveyor sprays and water trucks to all storage piles on site to control fugitive emissions. Sprays shall operate as required to maintain the opacity limits listed in this AO. [R307-401-8] Status: In Compliance. The water truck is equipped with a side cannon which is used to wet storage piles as well as conveyor sprays. II.B.5.e The owner/operator shall comply with all applicable requirements of R307-205 for fugitive emission and fugitive dust sources on site. [R307-205] Status: In Compliance. All observed visible emissions were within outlined limits.

Section III: APPLICABLE FEDERAL REQUIREMENTS

In addition to the requirements of this AO, all applicable provisions of the following federal programs
have been found to apply to this installation. This AO in no way releases the owner or operator from any
liability for compliance with all other applicable federal, state, and local regulations including UAC
R307.

NSPS (Part 60), OOO: Standards of Performance for Nonmetallic Mineral Processing Plants

Status: In Compliance. See conditions II.B.2.e and II.B.2.f.
8
MACT (Part 63), Subpart CCCCCC: National Emission Standards for Hazardous Air Pollutants for
Source Category: Gasoline Dispensing Facilities

Status: In compliance. During the 12-month period the source had 3,250 gallons of gasoline
throughput.

AREA SOURCE RULES EVALUATION:

The following Area Source Rules were evaluated during this inspection:

Emission Standards: Sulfur Content of Fuels [R307-203]

Status: In Compliance. Used fuel oil used in the shop heater meets the sulfur content standard. See
attached.

Emission Standards: Fugitive Emissions and Fugitive Dust [R307-205]

Status: In Compliance. All visible emissions were within set limits. National Emission Standards for Hazardous Air Pollutants [R307-214] Status:

EMISSION INVENTORY:
Listed below are the Actual Emissions Inventory provided from Martin Marietta Materials, Inc. - Milford
Quarry. A comparison of the estimated total potential emissions (PTE) on AO: DAQE-AN115900006-16,
is provided. PTE are supplied for supplemental purposes only.

Criteria Pollutant PTE tons/yr Actuals tons/yr
CO2 Equivalent 311.00
Carbon Monoxide 53.50 13.364
Nitrogen Oxides 13.57 15.912
Particulate Matter - PM10 60.99 7.587
Particulate Matter - PM2.5 7.67 1.729
Sulfur Dioxide 1.60 0.227

PREVIOUS ENFORCEMENT
ACTIONS: No enforcement actions in the past five years.

COMPLIANCE STATUS &
RECOMMENDATIONS: In regards to Approval Order (AO) DAQE-AN115900006-16,
dated March 3, 2016, the overall status is: In Compliance.
Records were made available for review at the time of inspection
except for the used oil analysis which was emailed after. The
facility appeared to be properly maintained and operated.

HPV STATUS: Not Applicable.

RECOMMENDATION FOR
NEXT INSPECTION: Inspect as normal.

9
NSR RECOMMENDATIONS: Update equipment list to show the replacement-in-kind granted
by DAQE-GN115900007-24.

ATTACHMENTS: VEO Form, Used Oil Analysis and Email, Initial OOO
Observations and Email, Gasoline Throughput Email.
#=CL#
May 08, 2023
LIMS USE: FR - JAMES NICHOLSON
LIMS OBJECT ID: 60427001
60427001
Project:
Pace Project No.:
RE:
James Nicholson
Martin Marietta Aggregates
7381 West 133rd St.
Suite 401
Overland Park, KS 66213
MILFORD L/T OIL ANALYSIS
Dear James Nicholson:
Enclosed are the analytical results for sample(s) received by the laboratory on April 24, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Kansas City
• Pace Analytical Services - New Orleans
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Jennifer Haley
[e-mail]
PM Lab Management
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9608 Loiret Blvd.
Lenexa, KS 66219
[phone]
Page 1 of 37
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
60427001
MILFORD L/T OIL ANALYSIS
Pace Analytical Services New Orleans
Florida Department of Health (NELAC): E87595
Illinois Environmental Protection Agency: 0025721
Kansas Department of Health and Environment (NELAC):
E-10266
Louisiana Dept. of Environmental Quality (NELAC/LELAP):
02006
Texas Commission on Env. Quality (NELAC):
T104704405-09-TX
U.S. Dept. of Agriculture Foreign Soil Import: P330-10-
00119
Pace Analytical Services Kansas
9608 Loiret Boulevard, Lenexa, KS 66219
Missouri Inorganic Drinking Water Certification #: 10090
Arkansas Drinking Water
Arkansas Certification #: 22-031-0
Illinois Certification #: 2000302021-3
Iowa Certification #: 118
Kansas/NELAP Certification #: E-10116
Louisiana Certification #: 03055
Nevada Certification #: KS000212023-1
Oklahoma Certification #: 2022-057
Florida: Cert E871149 SEKS WET
Texas Certification #: T104704407-21-15
Utah Certification #: KS000212022-12
Illinois Certification #: 004592
Kansas Field Laboratory Accreditation: # E-92587
Missouri SEKS Micro Certification: 10070
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9608 Loiret Blvd.
Lenexa, KS 66219
[phone]
Page 2 of 37
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
60427001
MILFORD L/T OIL ANALYSIS
Lab ID Sample ID Matrix Date Collected Date Received
60427001001 MOS-4-20-23 Non Aqueous 04/20/23 09:15 04/24/23 09:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9608 Loiret Blvd.
Lenexa, KS 66219
[phone]
Page 3 of 37
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
60427001
MILFORD L/T OIL ANALYSIS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
60427001001 MOS-4-20-23 EPA 6010 1 PASI-NAJS
EPA 6010 4 PASI-KMA1
EPA 9076 1 PANLOH
ASTM D240 1 PANCRB
ASTM D92 1 PASI-KRKA
Moisture 1 PASI-NGGG1
PAN = Pace National - Mt. Juliet
PASI-K = Pace Analytical Services - Kansas City
PASI-N = Pace Analytical Services - New Orleans
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9608 Loiret Blvd.
Lenexa, KS 66219
[phone]
Page 4 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
60427001
MILFORD L/T OIL ANALYSIS
Sample:MOS-4-20-23 Lab ID:60427001001 Collected:04/20/23 09:15 Received:04/24/23 09:10 Matrix:Non Aqueous
Liquid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical Services - New Orleans
6010 Metals, Total
Sulfur 504 mg/kg 04/28/23 11:3904/27/23 07:4510.1 1
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical Services - Kansas City
6010 MET ICP Red. Interference
Arsenic ND mg/kg 05/01/23 15:58 7440-38-204/27/23 10:110.49 1
Cadmium ND mg/kg 05/01/23 15:58 7440-43-904/27/23 10:110.24 1
Chromium ND mg/kg 05/01/23 15:58 7440-47-304/27/23 10:110.24 1
Lead 0.54 mg/kg 05/01/23 15:58 7439-92-104/27/23 10:110.49 1
Analytical Method: EPA 9076
Pace National - Mt. Juliet
Wet Chemistry 9076
Total Organic Halides ND mg/kg 05/02/23 10:2105/02/23 10:215005
Analytical Method: ASTM D240 Preparation Method: D240
Pace National - Mt. Juliet
Wet Chemistry D240
BTU 19700 BTU/lb 05/01/23 22:35 BTU05/01/23 19:001
Analytical Method: ASTM D92
Pace Analytical Services - Kansas City
Flashpoint, Open Cup
Flashpoint >212 deg F 05/08/23 14:36 N378.0 1
Analytical Method: Moisture
Pace Analytical Services - New Orleans
Percent Moisture
Percent Moisture 3.1 %05/01/23 11:080.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2023 02:44 PM
Pace Analytical Services, LLC
9608 Loiret Blvd.
Lenexa, KS 66219
[phone]
Page 5 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
60427001
MILFORD L/T OIL ANALYSIS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
284756
EPA 3050
EPA 6010
6010 MET
Laboratory:Pace Analytical Services - New Orleans
Associated Lab Samples:60427001001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1365168
Associated Lab Samples:60427001001
Matrix:Solid
Analyzed
Sulfur mg/kg ND 10.0 04/28/23 10:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1365169LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfur mg/kg 9221000 92 81-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1365170MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
20275882001
1365171
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfur mg/kg M1962-190 75-125-424 13 20877170001520013300
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2023 02:44 PM
Pace Analytical Services, LLC
9608 Loiret Blvd.
Lenexa, KS 66219
[phone]
Page 6 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
60427001
MILFORD L/T OIL ANALYSIS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
843953
EPA 3050
EPA 6010
6010 MET
Laboratory:Pace Analytical Services - Kansas City
Associated Lab Samples:60427001001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3344673
Associated Lab Samples:60427001001
Matrix:Solid
Analyzed
Arsenic mg/kg ND 1.0 05/01/23 15:30
Cadmium mg/kg ND 0.50 05/01/23 15:30
Chromium mg/kg ND 0.50 05/01/23 15:30
Lead mg/kg ND 1.0 05/01/23 15:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3344674LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 91.9100 92 80-120
Cadmium mg/kg 100100 100 80-120
Chromium mg/kg 99.5100 100 80-120
Lead mg/kg 100100 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3344675MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
60427148001
3344676
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 96.2 90 75-12589 1 2096.2ND 86.5 85.8
Cadmium mg/kg 96.2 96 75-12596 0 2096.22.9 93.0 92.6
Chromium mg/kg M196.2 91 75-125-106 11 2096.27970 1890 1700
Lead mg/kg 96.2 97 75-12596 1 2096.2ND 93.2 92.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2023 02:44 PM
Pace Analytical Services, LLC
9608 Loiret Blvd.
Lenexa, KS 66219
[phone]
Page 7 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
60427001
MILFORD L/T OIL ANALYSIS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2048280
EPA 9076
EPA 9076
Wet Chemistry 9076
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:60427001001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3920133-1
Associated Lab Samples:60427001001
Matrix:Solid
Analyzed
Total Organic Halides mg/kg ND 100 05/02/23 08:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3920133-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Halides mg/kg 102100 102 85.0-115
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3920133-3MATRIX SPIKE SAMPLE:
MSSpike
Result
L1609804-01
Total Organic Halides mg/kg 171167 102 80.0-120ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2023 02:44 PM
Pace Analytical Services, LLC
9608 Loiret Blvd.
Lenexa, KS 66219
[phone]
Page 8 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
60427001
MILFORD L/T OIL ANALYSIS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2052039
D240
ASTM D240
Wet Chemistry D240
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:60427001001
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3919650-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3919650-2
BTU BTU/lb 1150011400 101 85.0-11510211600 0.544 20
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
60427001001
R3919650-3SAMPLE DUPLICATE:
BTU BTU/lb 19600 0.385 2019700
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2023 02:44 PM
Pace Analytical Services, LLC
9608 Loiret Blvd.
Lenexa, KS 66219
[phone]
Page 9 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
60427001
MILFORD L/T OIL ANALYSIS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
845704
ASTM D92
ASTM D92
Flashpoint, Open Cup
Laboratory:Pace Analytical Services - Kansas City
Associated Lab Samples:60427001001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3351222
Associated Lab Samples:60427001001
Matrix:Solid
Analyzed
Flashpoint deg F >212 78.0 N305/08/23 14:36
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
60426931003
3351223SAMPLE DUPLICATE:
Flashpoint deg F >212 N3>212
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2023 02:44 PM
Pace Analytical Services, LLC
9608 Loiret Blvd.
Lenexa, KS 66219
[phone]
Page 10 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
60427001
MILFORD L/T OIL ANALYSIS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
284992
Moisture
Moisture
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - New Orleans
Associated Lab Samples:60427001001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
20274561001
1366546SAMPLE DUPLICATE:
Percent Moisture %ND 20ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2023 02:44 PM
Pace Analytical Services, LLC
9608 Loiret Blvd.
Lenexa, KS 66219
[phone]
Page 11 of 37
#=QL#
QUALIFIERS
Pace Project No.:
Project:
60427001
MILFORD L/T OIL ANALYSIS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
SAMPLE QUALIFIERS
Sample: 60427001001
Wet Chemistry by Method 9076 - Dilution due to matrix.[1]
Sample: L1609804-01
Wet Chemistry by Method 9076 - Dilution due to matrix.[1]
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Accreditation is not offered by the relevant laboratory accrediting body for this parameter.N3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2023 02:44 PM
Pace Analytical Services, LLC
9608 Loiret Blvd.
Lenexa, KS 66219
[phone]
Page 12 of 37
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
60427001
MILFORD L/T OIL ANALYSIS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
60427001001 284756 284836MOS-4-20-23 EPA 3050 EPA 6010
60427001001 843953 844131MOS-4-20-23 EPA 3050 EPA 6010
60427001001 2048280MOS-4-20-23 EPA 9076
60427001001 2052039 2052039MOS-4-20-23 D240 ASTM D240
60427001001 845704MOS-4-20-23 ASTM D92
60427001001 284992MOS-4-20-23 Moisture
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2023 02:44 PM
Pace Analytical Services, LLC
9608 Loiret Blvd.
Lenexa, KS 66219
[phone]
Page 13 of 37
Page 14 of 37
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#=CL#
May 08, 2023
LIMS USE: FR - JENNIFER HALEY
LIMS OBJECT ID: 20275827
20275827
Project:
Pace Project No.:
RE:
Jennifer Haley
PASI Kansas
9808 Lorient Blvd.
Lenexa, KS 66219
60427001/Martin Marietta
Dear Jennifer Haley:
Enclosed are the analytical results for sample(s) received by the laboratory on April 26, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - New Orleans
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Brian Rhode
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1000 Riverbend Blvd - Suite F
St. Rose, LA 70087
[phone]
Page 1 of 11Page 16 of 37
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
20275827
60427001/Martin Marietta
Pace Analytical Services New Orleans
Florida Department of Health (NELAC): E87595
Illinois Environmental Protection Agency: 0025721
Kansas Department of Health and Environment (NELAC):
E-10266
Louisiana Dept. of Environmental Quality (NELAC/LELAP):
02006
Texas Commission on Env. Quality (NELAC):
T104704405-09-TX
U.S. Dept. of Agriculture Foreign Soil Import: P330-10-
00119
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1000 Riverbend Blvd - Suite F
St. Rose, LA 70087
[phone]
Page 2 of 11Page 17 of 37
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
20275827
60427001/Martin Marietta
Lab ID Sample ID Matrix Date Collected Date Received
60427001001 MOS-4-20-23 Solid 04/20/23 09:15 04/26/23 08:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1000 Riverbend Blvd - Suite F
St. Rose, LA 70087
[phone]
Page 3 of 11Page 18 of 37
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
20275827
60427001/Martin Marietta
Lab ID Sample ID Method
Analytes
ReportedAnalysts
60427001001 MOS-4-20-23 EPA 6010 1AJS
Moisture 1GGG1
PASI-N = Pace Analytical Services - New Orleans
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1000 Riverbend Blvd - Suite F
St. Rose, LA 70087
[phone]
Page 4 of 11Page 19 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
20275827
60427001/Martin Marietta
Sample:MOS-4-20-23 Lab ID:60427001001 Collected:04/20/23 09:15 Received:04/26/23 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical Services - New Orleans
6010 Metals, Total
Sulfur 504 mg/kg 04/28/23 11:3904/27/23 07:4510.1 1
Analytical Method: Moisture
Pace Analytical Services - New Orleans
Percent Moisture
Percent Moisture 3.1 %05/01/23 11:080.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2023 11:47 AM
Pace Analytical Services, LLC
1000 Riverbend Blvd - Suite F
St. Rose, LA 70087
[phone]
Page 5 of 11Page 20 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
20275827
60427001/Martin Marietta
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
284756
EPA 3050
EPA 6010
6010 MET
Laboratory:Pace Analytical Services - New Orleans
Associated Lab Samples:60427001001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1365168
Associated Lab Samples:60427001001
Matrix:Solid
Analyzed
Sulfur mg/kg ND 10.0 04/28/23 10:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1365169LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfur mg/kg 9221000 92 81-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1365170MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
20275882001
1365171
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfur mg/kg M1962-190 75-125-424 13 20877170001520013300
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2023 11:47 AM
Pace Analytical Services, LLC
1000 Riverbend Blvd - Suite F
St. Rose, LA 70087
[phone]
Page 6 of 11Page 21 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
20275827
60427001/Martin Marietta
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
284992
Moisture
Moisture
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - New Orleans
Associated Lab Samples:60427001001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
20274561001
1366546SAMPLE DUPLICATE:
Percent Moisture %ND 20ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2023 11:47 AM
Pace Analytical Services, LLC
1000 Riverbend Blvd - Suite F
St. Rose, LA 70087
[phone]
Page 7 of 11Page 22 of 37
#=QL#
QUALIFIERS
Pace Project No.:
Project:
20275827
60427001/Martin Marietta
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The Nelac Institute
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2023 11:47 AM
Pace Analytical Services, LLC
1000 Riverbend Blvd - Suite F
St. Rose, LA 70087
[phone]
Page 8 of 11Page 23 of 37
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
20275827
60427001/Martin Marietta
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
60427001001 284756 284836MOS-4-20-23 EPA 3050 EPA 6010
60427001001 284992MOS-4-20-23 Moisture
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2023 11:47 AM
Pace Analytical Services, LLC
1000 Riverbend Blvd - Suite F
St. Rose, LA 70087
[phone]
Page 9 of 11Page 24 of 37
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ANALYTICAL REPORT
May 03, 2023
Pace Analytical - Lenexa, KS
Sample Delivery Group:L1609434
Samples Received:04/26/2023
Project Number:60427001
Description:MILFORD L/T OIL ANALYSIS
Site:001
Report To:Jennifer Haley
9608 Loiret Boulevard
Lenexa, KS 66219
Entire Report Reviewed By:
May 03, 2023
[Preliminary Report]
Nancy McLain
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Pace Analytical - Lenexa, KS 60427001 L1609434 05/03/23 09:05 1 of 11
May 03, 2023
Nancy McLain
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Pace Analytical - Lenexa, KS 60427001 L1609434 05/03/23 09:12 1 of 11
Page 27 of 37
TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
MOS-4-20-23 L1609434-01 5
Qc: Quality Control Summary 6
Wet Chemistry by Method 9076 6
Wet Chemistry by Method D240 7
Gl: Glossary of Terms 8
Al: Accreditations & Locations 9
Sc: Sample Chain of Custody 10
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Pace Analytical - Lenexa, KS 60427001 L1609434 05/03/23 09:05 2 of 11
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Pace Analytical - Lenexa, KS 60427001 L1609434 05/03/23 09:12 2 of 11
Page 28 of 37
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MOS-4-20-23 L1609434-01 Solid 04/20/23 09:15 04/26/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Wet Chemistry by Method 9076 WG2048280 5 05/02/23 10:21 05/02/23 10:21 LOH Mt. Juliet, TN
Wet Chemistry by Method D240 WG2052039 1 05/01/23 19:00 05/01/23 22:35 CRB Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Pace Analytical - Lenexa, KS 60427001 L1609434 05/03/23 09:05 3 of 11
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Pace Analytical - Lenexa, KS 60427001 L1609434 05/03/23 09:12 3 of 11
Page 29 of 37
CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Nancy McLain
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Pace Analytical - Lenexa, KS 60427001 L1609434 05/03/23 09:05 4 of 11
Nancy McLain
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Pace Analytical - Lenexa, KS 60427001 L1609434 05/03/23 09:12 4 of 11
Page 30 of 37
SAMPLE RESULTS - 01
L1609434
MOS-4-20-23
Collected date/time: 04/20/23 09:15
Wet Chemistry by Method 9076
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TOX U 150 500 5 05/02/2023 10:21 WG2048280
Sample Narrative:
L1609434-01 WG2048280: Dilution due to matrix.
Wet Chemistry by Method D240
Result Qualifier Dilution Analysis Batch
Analyte BTUs/lb date / time
BTUs 19700 1 05/01/2023 22:35 WG2052039
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Pace Analytical - Lenexa, KS 60427001 L1609434 05/03/23 09:05 5 of 11
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Pace Analytical - Lenexa, KS 60427001 L1609434 05/03/23 09:12 5 of 11
Page 31 of 37
QUALITY CONTROL SUMMARYWG2048280
Wet Chemistry by Method 9076 L1609434-01
Method Blank (MB)
(MB) R3920133-1 05/02/23 08:21
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TOX U 30.0 100
Laboratory Control Sample (LCS)
(LCS) R3920133-2 05/02/23 08:29
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TOX 100 102 102 85.0-115
L1609804-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1609804-01 05/02/23 09:36 • (MS) R3920133-3 05/02/23 09:42
Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier
Analyte mg/kg mg/kg mg/kg %%
TOX 167 U 171 102 5 80.0-120
Sample Narrative:
OS: Dilution due to matrix.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Pace Analytical - Lenexa, KS 60427001 L1609434 05/03/23 09:05 6 of 11
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QUALITY CONTROL SUMMARYWG2052039
Wet Chemistry by Method D240 L1609434-01
L1609434-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1609434-01 05/01/23 22:35 • (DUP) R3919650-3 05/01/23 22:35
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte BTUs/lb BTUs/lb %%
BTUs 19700 19600 1 0.385 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3919650-1 05/01/23 22:35 • (LCSD) R3919650-2 05/01/23 22:35
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte BTUs/lb BTUs/lb BTUs/lb %%%%%
BTUs 11400 11500 11600 101 102 85.0-115 0.544 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Page 33 of 37
GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Page 34 of 37

Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Page 35 of 37
Page 36 of 37
Pa
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e

3
7

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f

3
7
Jared James <[e-mail]>
Milford Used Oil Sample 04-20-2023.pdf
2 messages
James Nicholson <[e-mail]>Tue, Jul 9, 2024 at 2:49 PM
To: Jared James <[e-mail]>
Cc: Brady Carter <[e-mail]>, Erin Kunkel <[e-mail]>
Jared,
This was stuck in my Outbox. Sorry!!! Please find attached the used oil sample obtained in 2023. I apologize for the
document not being available during today’s inspection. Please let me know if any other documents are needed.

Thanks
James Nicholson
Manager Environmental Services

7381 W 133rd St, Suite 100, Overland Park, Kansas 66213
t. [phone] m. [phone] f. [phone]
e. [e-mail]
www.martinmarietta.com
P Please consider the environment before prinng this email.

This email (including aachments) is intended solely for the use
of the individual to whom it is addressed and may contain informaon
that is privileged, confidenal or otherwise exempt from disclosure
under applicable law. If you are not the intended recipient, please do
not read, copy or re-transmit this communicaon. If you have received
this message in error, please contact the sender immediately by return
email and delete the original message and any aachments from your
system. Thank you in advance for your cooperaon and assistance.

Milford Used Oil Sample 04-20-2023.pdf
3716K
8/28/24, 5:03 PM State of Utah Mail - Milford Used Oil Sample 04-20-2023.pdf
https://mail.google.com/mail/u/0/?ik=2b4d965f6e&view=pt&search=all&permthid=thread-f:1804135987008591138&simpl=msg-f:180413598700859113…1/2
Jared James <[e-mail]>Tue, Jul 9, 2024 at 2:55 PM
To: James Nicholson <[e-mail]>
Received, thank you.
[Quoted text hidden]
--
Jared James | Environmental Scientist | Minor Source Compliance
Phone:[phone] email: [e-mail]
195 North 1950 West, Salt Lake City, UT 84116
8/28/24, 5:03 PM State of Utah Mail - Milford Used Oil Sample 04-20-2023.pdf
https://mail.google.com/mail/u/0/?ik=2b4d965f6e&view=pt&search=all&permthid=thread-f:1804135987008591138&simpl=msg-f:180413598700859113…2/2
Jared James <[e-mail]>
NSPS Milford Quarry
2 messages
James Nicholson <[e-mail]>Tue, Sep 24, 2024 at 11:55 AM
To: "[e-mail]" <[e-mail]>
Jared,
As we discussed last week, please find the NSPS testing conducted years ago at the Milford Quarry. 3 hour tests had
to be brutal. The replacement screen is scheduled to be tested the week of October 7th. Sorry for the delay. Please call
with any questions.

Thanks
James Nicholson
Manager Environmental Services

7381 W 133rd St, Suite 100, Overland Park, Kansas 66213
t. [phone] m. [phone] f. [phone]
e. [e-mail]
www.martinmarietta.com
P Please consider the environment before prinng this email.

This email (including aachments) is intended solely for the use
of the individual to whom it is addressed and may contain informaon
that is privileged, confidenal or otherwise exempt from disclosure
under applicable law. If you are not the intended recipient, please do
not read, copy or re-transmit this communicaon. If you have received
this message in error, please contact the sender immediately by return
email and delete the original message and any aachments from your
system. Thank you in advance for your cooperaon and assistance.

UT - Milford - Item B - NSPS Performance Tests - 1998.pdf
2268K
Jared James <[e-mail]>Tue, Sep 24, 2024 at 12:49 PM
To: James Nicholson <[e-mail]>
9/24/24, 1:05 PM State of Utah Mail - NSPS Milford Quarry
https://mail.google.com/mail/u/0/?ik=2b4d965f6e&view=pt&search=all&permthid=thread-f:1811101006912885397&simpl=msg-f:181110100691288539…1/2
Thanks for getting those to me, James. You might want to make sure they have a copy of these at the quarry since the
Approval Order states that records shall be kept for the life of the equipment. Thanks again!
[Quoted text hidden]
--
Jared James | Environmental Scientist | Minor Source Compliance
Phone:[phone] email: [e-mail]
195 North 1950 West, Salt Lake City, UT 84116
9/24/24, 1:05 PM State of Utah Mail - NSPS Milford Quarry
https://mail.google.com/mail/u/0/?ik=2b4d965f6e&view=pt&search=all&permthid=thread-f:1811101006912885397&simpl=msg-f:181110100691288539…2/2
Jared James <[e-mail]>
12 Month Gasoline Dispensing
2 messages
Sheri Wiseman <[e-mail]>Tue, Oct 1, 2024 at 12:12 PM
To: "[e-mail]" <[e-mail]>
Cc: Brady Carter <[e-mail]>, James Nicholson <[e-mail]>
Good Afternoon,

Our gasoline usage for the period of 10/01/23 – 09/30/24 = 3,250 gallons.
Please let me know if you need further details.

Thank you and Stay Safe,

Sheri Wiseman
Office Manager | Milford Quarry

Martin Marietta
4.5 Miles N. County Rd. 163,
P.O. Box 880, Milford, UT 84751
t. [phone] m. [phone]
e. [e-mail]
www.martinmarietta.com

From: James Nicholson <[e-mail]>
Sent: Tuesday, September 24, 2024 3:52 PM
To: Brady Carter <[e-mail]>; Sheri Wiseman <[e-mail]>
Subject: Fwd: One Last Thing

You guys on this?
10/1/24, 1:30 PM State of Utah Mail - 12 Month Gasoline Dispensing
https://mail.google.com/mail/u/0/?ik=2b4d965f6e&view=pt&search=all&permthid=thread-f:1811736265029038129&simpl=msg-f:181173626502903812…1/2
EXTERNAL SENDER – PLEASE ASSESS AND VERIFY

James Nicholson
Martin Marietta-Central
Begin forwarded message:
From: Jared James <[e-mail]>
Date: September 24, 2024 at 3:32:37 PM EDT
To: Brady Carter <[e-mail]>, James Nicholson <James.Nicholson@
martinmarietta.com>
Subject: One Last Thing

Brady/James

Can I also get the gasoline monthly throughput for the last 12 months for your gasoline dispensing facility
for 40 CFR Subpart 63, CCCCCC requirements? This should be the last thing I need from you. Thanks!

--
Jared James | Environmental Scientist | Minor Source Compliance
Phone:[phone] email: [e-mail]
195 North 1950 West, Salt Lake City, UT 84116
Jared James <[e-mail]>Tue, Oct 1, 2024 at 1:26 PM
To: Sheri Wiseman <[e-mail]>
Cc: Brady Carter <[e-mail]>, James Nicholson <[e-mail]>
Got it, thank you.
[Quoted text hidden]
10/1/24, 1:30 PM State of Utah Mail - 12 Month Gasoline Dispensing
https://mail.google.com/mail/u/0/?ik=2b4d965f6e&view=pt&search=all&permthid=thread-f:1811736265029038129&simpl=msg-f:181173626502903812…2/2