DAQ-2024-010871

1

DAQC-996-24
Site ID 10725 (B5)

MEMORANDUM

TO: CEM FILE – CLEAN HARBORS ARAGONITE, LLC

THROUGH: Harold Burge, Major Source Compliance Section Manager

FROM: Rob Leishman, Environmental Scientist

DATE: October 1, 2024

SUBJECT: Source: Incineration System (INC)
Contact: William Simmons – 435-844-8351
Location: 11600 North Aptus Road, Aragonite, Tooele County, UT
Test Contractor: Alliance Technical Group
FRS ID#: UT00000049004500048
Permit/AO#: Title V operating permit 450004004 dated November 23, 2021
Subject: Review of RA/PST Report dated June 14, 2024

On June 21, 2024, Utah Division of Air Quality (DAQ) received a Relative Accuracy/Performance
Specification Test (RA/PST) report for the Clean Harbors Aragonite INC in Aragonite, Utah. Testing was
performed on May 8, 2024, to determine the relative accuracy of the THC, O2, CO2, NOX, SO2, and CO
monitoring systems. The DAQ-calculated test results are:

RA/PST EVALUATION:

INC Main Stack Primary System
NSPS RATA - Test Date - 5/8/2024
Primary
Channel Manufacturer Serial No. Units CEM
Value
RM
Value
Relative
Accuracy Status
SO2 Servomex - 4900 4021 ppm 0.697 0.558 0.5% Passed
CO2 Servomex 4900 653305 % 9.480 9.490 0.2% Passed
NOx Thermo 42i - HL 0836633949 ppm 139.094 133.408 5.8% Passed
lbs/hr 32.671 30.651 8.5% Passed
O2 Servomex - 4900 4021 % 8.910 9.030 1.8% Passed
CO Servomex 4900 653305 ppm 2.063 1.936 1.8% Passed
THC Thermo 5Li-TH 1203299855 ppm 0.161 0.190 2.0% Passed
Volumetric Flow Rate acfm 62604.89 59233.56 7.3% Passed
Stack Test Deviation Report
There were no deviations observed during testing.
Calibration gases were in date and met performance specifications.

1 8 2
2

INC Main Stack Secondary System
NSPS RATA - Test Date - 5/8/2024
Primary
Channel Manufacturer Serial No. Units CEM
Value
RM
Value
Relative
Accuracy Status
SO2 Servomex 4900 652525 ppm 0.697 0.558 0.5% Passed
CO2 Servomex 4900 653305 % 9.480 9.490 0.2% Passed
NOx Thermo 42i-HL 0614216783 ppm 139.094 133.408 5.8% Passed
lbs/hr 32.671 30.651 8.5% Passed
O2 Servomex 4900 652525 % 8.910 9.030 1.8% Passed
CO Servomex 4900 653305 ppm 2.063 1.936 1.8% Passed
THC Thermo 5Li-TH 1434964304 ppm 0.061 0.190 3.0% Passed
Stack Test Deviation Report
There were no deviations observed during testing.
Calibration gases were in date and met performance specifications.

INC Main Stack Backup System
NSPS RATA - Test Date - 5/8/2024
Primary
Channel Manufacturer Serial No. Units CEM
Value
RM
Value
Relative
Accuracy Status
SO2 Servomex - 4900 4022 ppm 0.033 0.461 0.7% Passed
CO2 Servomex 4900 653205 % 9.050 9.240 2.2% Passed
NOx Thermo 42i - HL 0614216782 ppm 137.094 133.408 4.4% Passed
lbs/hr 32.198 30.651 7.1% Passed
O2 Servomex - 4900 4022 % 8.800 9.010 2.7% Passed
CO Servomex 4900 653205 ppm 2.463 1.936 2.2% Passed
THC Thermo 5Li-TH 1203299856 ppm 0.108 0.190 2.5% Passed
Stack Test Deviation Report
There were no deviations observed during testing.
Calibration gases were in date and met performance specifications.

DEVIATIONS: No deviations were noted in this report.

CONCLUSION: Clean Harbors Aragonite operates the continuous emissions monitor
(CEM) on the INC stack to measure THC, O2, CO2, NOX, SO2, and CO
emissions. The CEM was audited by the DAQ and found to meet quality
assurance requirements found in 40 CFR Part 60, Appendix B,
Performance Specification 1, and R307-170, Continuous Emission
Monitoring System Program. Quarterly cylinder gas audits and an annual
relative accuracy test audit were conducted in accordance with the
procedures outlined in UAC R307-170.

RECOMMENDATION: The Clean Harbors Aragonite INC CEM system was operating as
required in R307-170 and 40 CFR 60.13 at the time of this evaluation.

HPV: No.

ATTACHMENTS: RATA Review Spreadsheets.
Clean Harbors Aragonite, LLC
I1600 North Aptus Road
Aragonite, UT 84029
43s.884.8100
www.cleanharbors.com
Submitted via FedEx # 8182 9436 4252
Jvne 14,2024
Mr. Bryce Bird
Division of Air Quality (DAQ)
Department of Environmental Quality
195 North 1950 West
P.O. Box 144880
Salt Lake City, UT 84411-4880
RE: Relative Accuracy Test Audit (RATA) Report
Clean Harbors Aragonite, LLC
Title V Operating Permit 4500048004
Dear Mr. Bird,
In accordance with R307-170-7(5), Clean Harbors Aragonite,
Relative Accuracy Test Audit (RATA) Report. Enclosed is
copy was also sent to Mr. Robert Leishman Jr. via email.
UTAH DEPARTMENT OF
ENVIRONMENTAL OUALIW
JUii ? n ?i?4
DIVISION OF AIR QUALIW
LLC is submitting the May 8,2024,
a copy of the report for review. A
In accordance with Permit Condition I.K and Utah Administrative Code R307-415-5d,I certiff
under penalty of law that this document and all attachments were prepared under my direct
supervision in accordance with a system designed to assure that qualified personnel properly
gather and evaluate the information submitted. Based upon my inquiry of persons or persons who
manage the system, or those persons directly responsible for gathering the information submitted
is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are
significant penalties for submitting false information, including the possibility of imprisonment for
known violations.
Should you have any questions regarding this matter, please contact me at the number listed
below.
"People and Technologt Creating a Better Environment"
William Simmons
Facility GM III
Clean Harbors Aragonite, LLC
11600 North Aptus Road
PO Box 1339
Grantsville, Utah 84029 -1339
(o) 435.844.8351
(c) 870.310.6029
[e-mail]
www.cleanharbors.com
FAlHre
RATA Report
Clean Harbors Aragonite LLC
I1600 N. Aptus Road
Aragonite,UT 84029
Source Tested: Incinerator System GNC)
RATA - Oz, COz, SOz, NOx, CO & THC
Test Date: May 8,,2024
Project No. AST-2024-L 5 17
DIVISION OF AIR OUALITY
Prepared By
Alliance Technical Group, LLC
3683 W 2270 S, Suite E
West Valley City, UT 84120
pul6rpe
T[-CI]NICAL GROUP Source Test Rqnrt
Test Program Summary
Resulatorv Information
Permit No. Utah Department of Environmental Quality (DEQ), Division of Air Quality (DAQ)
Title V Operating Permit 4500048004
Regulatory Citations 40 CFR 60, Performance Specifications 2, 3, 4/4A,6, and 8A
Source Information
Source Narne
Incineration System
Contact Information
Source ID
INC
Target Parameters
VFR, Oz, COz, SOz, NOx, CO, THC
Test Location Test Company
Clean Harbors Aragonite LLC Alliance Technical Group, LLC
I 1600 N. Aptus Road 3683 W 2270 S, Suite E
Aragonite, W 84029 West Valley City, UT 84120
Manager, Maintenance
Cody Parks
Project Manager
Charles Horton
Regulatory Agency
Utah DAQ
195 North 1950 West
Salt Lake city, Lrf 84116
Environmental Health Scientist
Rob Leishman Jr.
[e-mail]
(801) 536-,{438
[e-mail] [e-mail]
(43s) 884-8242 (3s2) 663-7s68
Field Team Leader
Alan Jensen
alan j [e-mail]
[phone]
QA/QC Manager
Kathleen Shonk
katie. shonk@alliancetg. com
(8r2) 4s2-478s
Report Reviewer
Ryan Adam
[e-mail]
AST-2024-l 5 I 7
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Pagc iClcan Harbors - Aragonite, UT
Alliance Technical Group, LLC (Alliance) has completed the source testing as described in this report. Results
apply only to the source(s) tested and operating condition(s) for the specihc test date(s) and time(s) identified within
this report. All results are intended to be considered in their entirety, and Alliance is not responsible for use of lessthan the complete test report without written consent. This report shall not be reproduced in futt or in part without
written approval from the customer.
To the best of my knowledge and abilities, all information, facts and test data are correct. Data presented in thisreport has been checked for completeness and is accurate, error-free and legible. Onsite testing was conducted in
accordance with approved internal Standard Operating Procedures. Any deviations or problems are detailed in the
relevant sections in the test report.
This report is only considered valid once an authorized representative ofAlliance has signed in the space providedbelow; any other version is considered draft. This document was prepared in portable d-ocument format (pdf; and
contains pages as identified in the bottom footer of this document.
6113t2024
Charles Hortonn QSTI
Alliance Technical Group, LLC
Date
AST-2024-t517
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Page iiClean Harbors - Aragonitc, UT
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Source Test Report
l.l Process/Control System Descriptions.. ................ l_l
1.4 Site Specific Test Plan & Notification ................... ................... l_2
3.1 U.S. EPA Reference Test Methods I and2- Sampling/Traverse Points and Volumetric Flow Rate ........ 3-l
3.2 U.S. EPA Reference Test Method 3A. - Oxygen/Carbon Dioxide .................. 3-l
3.3 U.S. EPA Reference Test Method 4 - Moisture Content......... .......................3_2
3.4 U.S. EPA Reference Test Method 6C - Sulfur Dioxide......... .........................3_2
3.5 U.S. EPA Reference Test Method 7E - Nitrogen Oxides .........3_2
3.6 U.S. EPA Reference Test Method l0 - Carbon Monoxide..... ........................3_z
3.7 U.S. EPA Reference Test Method 25A - Total Hydrocarbons .......................3_2
3.8 u.s. EPA Reference Test Method 205 - Gas Dilution System certification.. ...................... 3-3
3-9 Quality Assurance/Quality Control - U.S. EPA Reference Test Methods 3A, 6C, 7E and 10................... 3-3
3.10 Quality Assurance/Quality control - u.s. EpA Reference Test Method 25A.......................................3-4
LIST OF TABLES
Summary of Performance Specification Test Results, Oz............... ............2_l
Summary of Performance Specification Test Results, COz ............ ............2_l
Summary of Performance Specification Test Results, SO2............. ............2_2
Summary of Performance Specification Test Results, NOx ........... ............2_2
Summary of Performance Specification Test Results, CO.............. ............2_3
Summary of Performance Specification Test Results, THC ........... ............2_3
Summary of Performance Specification Test Results, VFR........... ............2_4
Source Testing Methodology ............,.............3_l
APPENDICES
Appendix A Sample Calculations
Appendix B Field Data
Appendix C Quality Assurance/euality Control Data
Appendix D CEMS & CERMS Data
TABLE OF CONTENTS
AST-2024-1517
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fiCilNlcAt GTiC)UN Source Tesl Reporl
Introduction
1.0 Introduction
Alliance Technical Group, LLC (Alliance) was retained by clean Harbors Aragonite, LLC (clean Harbors) to
conduct performance specification (PS) testing at the Aragonite, Utah facility. Portions of the facility are subject to
provisions of 40 CFR 60' Appendix B, PS 2, 3, 4A,6 and 8A and the Utah Department of Environmental euality(UDEQ) Title V operation Permit No. 4500048004. Testing included conducting a relative accuracy test audit(RATA) to determine the relative accuracy (RA) of the oxygen (o2), carbon dioxide (Coz), sulfur dioxide (So2),
nitrogen oxides (NOx)' carbon monoxide (CO) and total hydrocarbons (THC) primary, secondary and backup
continuous emissions monitoring systems (CEMS) and the volumetric flow rate (VFR) continuous emissions rate
monitoring system (CERMS) serving to monitor emissions from the incineration system (INC).
l.l Process/ControlsystemDescriptions
The permitted source is a commercial hazardous waste treatment, storage, and disposal facilify (TSDF). Hazardous
waste is received from various sources including refineries, chemical manufacturing plants, and coke by-product
recovery plants' The off-site material management unit at the source includes sixteen liquid waste storage and
blending tanks, two sludge tanks, three bulk solids tanks, and several container management buildings. Waste from
the off-site material management unit is treated in an incinerator which includes primary and secondary chambers.
The incinerator confol system includes a spray dryer, carbon injection, baghouse, saturator, and wet scrubber.
1.2 CEMS Descriptions
CEMS #l (Primarv)
Parameter:CO COz SOz Oz NOx THC
Make:Servomex Servomex Thermo Thermo
Model:4900 4900 42i-HL 5li-TH
Serial No.:653204 4021 0836633949 12032998ss
Span:0-200 ppm (low) I 0-20%0-500 ppm I O-ZS N 0- 1.000 onm 0-100 oom
CEMS #2 (Secondarv)
-
Parameter:CO COr SOz I O,NOx THCMake:Servomex Servomex Thermo ThermoModel:4900 4900 42i-HL 5li-TH
Serial No.:653305 652525 0614216783 1434964304
Span:0-200 ppm (low) I O-20 o/o 0-500 ppm I O-25 o/n 0-1.000 oom 0-100 ppm
CEMS #3 (Backuo - #2 Soare)
Parameter:CO COr SOU Oz NOx THC
Make:Servomex Servomex Thermo ThermoModel:4900 4900 42i-HL 5li-TH
Serial No.:653205 4022 06142t6782 1203299856
Span:0-200 ppm (low) I 0-2\yo 0-l,000ppm I 0-l00nnm 0-1.000 oom 0-100 oom
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rE:CI]NICAL GNOUP Source Test Report
Introduction
VFR FT2195
Parameter:Flow Rate
Make:Rosemount
Model:305 I
Serial No.:036061752
Soan:
1.3 Project Team
Personnel involved in this project are identified in the following table.
Table 1-l: Project Team
1.4 Site Specific Test PIan & Notification
Testing was conducted in accordance with the Site-Specific Test Plan (SSTp) submitted to UDAe by Clean
Harbors.
Clean Harbors - Aragonite, UT
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Clean Harbors Personnel Cody Parks
Alliance Personnel
Alan Jensen
Supilani Mailei
Mitchell Manwaring
AST-2024-15t7 Page l-2
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2.0 Summary of Results
Alliance conducted PS testing at the Clean Harbors facility in Aragonite, Utah on May 8, 2024. Testing consisted of
conducting a RATA to derermine the RA of the Oz, COz, SOz, NOx, CO, and THC primary, secondary and backup
CEMS and the VFR CERMS serving to monitor ernissions from the incineration system (lNC).
Tables 2-1 through 2-7 ptovide summaries of the emission testing results with comparisons to the applicable relative
accuracy requirements. Any difference between the summary results listed in the following tables and the detailed
results contained in appendices is due to rounding for presentation.
Table 2-1: Summary of Performance Specification Test Results, Or
I Calculated using the mean reference method.
I Calculatcd using thc mcan rcttrcncc mcthod.
Table 2-2t Summary of Performance Specification Test Results, COz
Source Test Report
CEMS
Pcrformance Test Data Rehtlve Accurecy
Reference
Msthod
Iletr
CEMS
Date
Per{ormance
Required
Performance
Demonstrated
oxygen Data, AT2200A - 04900-cl-4021
Concentration , % (dry)9.04 8.91 <20 Yo l.8lo/" I
Oxygen Data, AT2200B - 04900-Ct-4022
Concentration , % (dry)9.04 8.91 <20Yo 1.87o/o I
Oxygen Data, AT2200C - 04900-Cl-652525
Concentration, % (dry)9.O4 8.82 <20Y"2.77o/o )
CEMS
Performance Test Dete Rehtive Accuracy
Reference
Method
Date
CEMS
Datr
Performence
Requlred
Performance
Demonstrated
Carbon Dioxide Data, AT2I98A - 04900-Cl-653204
Concentration , % (dry)9.38 9.39 120%0.34o/o t
Carbon Dioxide Data, AT2l98B - 04900-Cl-653205
Concentration , % (.dry)9.37 9.37
=20oA 0.250h I
Carbon Dioxide Data, AT2l98C - 04900-Cl-653305
Concentration , % (dry)9.2s 9.05 < 2oo/o 2.38yo I
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C CAL GROUP
Table 2-3: Summary of Performance Specification Test Results, SOz
I Calculated using the applicable source standard for the pollutant. See Appendix B for the applicable standard used.
Source Test Report
Table 2-4: Summary of Performance Specification Test Results, NOx
Sulfur Dioxide Data, AT220EA - 04900-Ct-4021
Concentration, ppmvd
Concentration, ppmvd @7% Oz
Sulfur Dioxlde Data, AT2208B - 04900-Ct-4022
Concentration, ppmvd
Concentration, ppmvd @7o/o Oz
0.54yol
0.54Yo I
Sulfur Dioxide Data, AT220EC - 04900-Cl-6S2525
Concentration, ppmvd
Concentration, ppmvd @ 7% Oz
0.82Yo I
0.glo I
Nitrogen Oxides Data, AT2202A - 08636633949
Concentration, ppmvd
Emission Rate, lb/hr
5.720 |
8.42Y.1
Nitrogen Oxides Datt, AT2202B - 0614216783
Concentration, ppmvd
Emission Rate, lb/hr
4.960/o I
7.7lYo l
Nitrogen Oxides Data, AT2202C .06142167E2
Concentration, ppmvd
Emission Rate, lb/hr
4.31yo I
6.97Yo I
I Calculated using the mean reference method.
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Page2-2Clean Halbors - Aragonite, UT
AItanoe
Test Repoft
Table 2-5: Summary of Performance Specification Test Results, CO
Table 2-6: Summary of Performance Specification Test Results, THC
L Calculated using the apphcabte source standard lor the pollutant. See Appendix B for the applicable standard used
CEMS
Performance Test Deta Reletive Accuracy
Reference
Method
Datr
CEMS
Data
Ntcrnative
Performance
Required
Performance
Demonrtrated
Carbon Monoxide Data, AT2199A - 04900-Cl-653204
Conccntration, ppmvd
Concentration, ppmvd @ 7% Oz
1.90
2.25
2.06
2.2s
<5oom
<5ppm
l.8l ppm I
l.6l ppm I
Carbon Monoxide Data, AT2199CL - 04900-Cl-653205
Concentration, ppmvd
Concentration, ppmvd @7% Oz
l.8l
2.3s
2.16
2.54
<5oom
<5ppm
2.05 ppm I
1.75 ppm I
Carbon Monoxide Data, AT2l99E - 04900-Cl-653305
Concentration, ppmvd
Concentration, ppmvd @7% Ot
1.90
2.3s
2.46
2.76
<5onm
<5onm
2.25 ppml
1.92 ppm I
rCalculatcd using thc avcragc absolute diff'crcncc plus the confidcncc cocfTicicnl
CEMS
Per{ormence Test Deta Reletlve Accuracy
Reference
Method
Dete
CEMS
Data
Performance
Requlred
Performance
Demonetrated
Total Hydrocarbons Data, AT2207 A - 1203299856
Concentration, pprnv (wet)
Concentration, ppmvd @ 7% Ot
0.16
0.27
0.16
0.30
<200
< l0Yo
3.30Yo I
334y. I
Total Hydrocarbons Datz, AT2207B - 1434964304
Concentration, ppmv (wet)
Concentration, ppmvd @) 7% Ot
0. l6
0.27
0.061
0.t I
<20Yo
<l0Yo
4.75Yo )
4.720h I
Total Hydrocarbons Data, AT2207C - 1203299855
Concentration, ppmv (wet)
Concentration, ppmvd @ 7% Oz
0. r6
0.27
0.020
0.033
:<20 Yo
< t0y,
5.560 |
5.59Yo I
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ECHNICAL GROUP Source Test Repor-t
Table 2-7: Summary of Performance Specification Test Results, Vf,.R
Volumetric Flow Rate
High Load Flow Rate, acfrn
I Calculated using the mean reference method.
AST-2024-15t7 Page24Clean Harbors - Aragonite, UT
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Source Tesl Repofi
Testins Methodolosv
3.0 Testing Methodology
The emission testing program was conducted in accordance with the test methods listed in Table 3-1. Method
descriptions are provided below while quality assurance/quality control data is provided in Appendix C.
Table 3-1: Source Testing Methodology
3.1 U.S. EPA Reference Test Methods I and 2 - Sampling/Traverse Points and Volumetric Flow Rate
The sampling location and number of traverse (sampling) points were selected in accordance with U.S. EPA
Reference Test Method l. To determine the minimum number of traverse points, the upstream and downstream
distances were equated into equivalent diameters and compared to Figure l-2 in U.S. EPA Reference Test Method l.
Full velocity traverses were conducted in accordance with U.S. EPA Reference Test Method 2 to determine the
average stack gas velocity pressure. static pressure and temperature . The veloc'ity and static pressure measurement
system consisted of a pitot tube and inclined manometer. The stack gas temperature was measured with a K-type
thermocouple and pyrometer.
Stack gas velocity pressure and temperature readings were recorded during each test run. The data collected was
utilized to calculate the volumetric flow rate for comparison to the continuous emission rate monitoring system
(CERMS). The relative accuracy of the CERMS was determined based on procedures found in 40 CFR 60,
Performance Specifi cation 6.
3.2 U.S. EPA Reference Test Method 3A - Oxygen/Carbon Dioxide
The oxygen (Oz) and carbon dioxide (COz) testing was conducted in accordance with U.S. EPA Reference Test
Method 3A. Data was collected online and reported in one-minute averages. The sampling system consisted of a
stainless-steel probe, Teflon sample line(s), gas conditioning system and the identified gas analyzer. The gas
conditioning system was a non-contact condenser used to remove moisture from the stack gas. If an unheated
Teflon sample line was used, then a portable non-contact condenser was placed in the system directly after the
probe. Otherwise, a heated Teflon sample linc was uscd. The quality control measures are described in Section 3.9.
The relative accuracy of the Oz and CO: CEMS was determined based on procedures found in 40 CFR 60,
Performance Specifi cation 3.
Clcan Harbors - Aragonitc, UT
Peremeter U.S. EPA Reference
Test Methods Notce/Remsrks
Volumetric Flow Rate t&2 Full Velocity Traverses
Oxygen / Carbon Dioxide 3A Instrumental Analysis
Moisture Content 4 Gravimetric Analysis
Sulfur Dioxide 6C Instrumental Analysis
Nitrogen Oxides 7E Instrumental Analysis
Carbon Monoxide l0 Instrumental Analysis
Total Hydrocarbons 25A lnstrumental Analysis
Gas Dilution System Certification 205
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Source Test Reporl
3.3 U.S. EPA Reference Test Method 4 - Moisture Content
The stack gas moisture content (BWS) was determined in accordance with U.S. EPA Reference Test Method 4. The
gas conditioning train consisted of a series of chilled impingers. Prior to testing, each impinger was filled with a
known quantity of water or silica gel. Each impinger was analyzed gravimetrically before and after each test run on
the same balance to determine the amount of moisture condensed.
3.4 U.S. EPA Reference Test Method 6C - Sutfur Dioxide
The sulfur dioxide (SO2) testing was conducted in accordance with U.S. EPA Reference Test Method 6C. Data was
collected online and reported in one-minute averages. The sampling system consisted of a heated stainless steel
probe, Teflon sample line(s), gas conditioning system and the identified analyzer. The gas conditioning system was
a non-contact condenser used to remove moisture from the source gas. If an unheated Teflon sample line was used,
then a portable non-contact condenser was placed in the system directly after the probe. Otherwise, a heated Teflon
sample line was used. The quality control measures are described in Section 3.9.
The relative accuracy of the SOz CEMS was determined based on procedures found in 40 CFR 60, performance
Specification 2.
3.5 U.S. EPA Reference Test Method 7E - Nitrogen Oxides
The nitrogen oxides (NOx) testing was conducted in accordance with U.S. EPA Reference Test Method 7E. Data
was collected online and reported in one-minute averages. The sampling system consisted of a stainless-steel probe,
Teflon sample line(s), gas conditioning system and the identified gas analyzer. The gas conditioning system was a
non-contact condenser used to remove moisture from the stack gas. If an unheated Teflon sample line was used,
then a portable non-contact condenser was placed in the system directly after the probe. Otherwise, a heated Teflon
sample line was used. The quality control measures are described in Section 3.9.
The relative accuracy of the NOx CEMS was determined based on procedures found in 40 CFR 60, performance
Specification 2.
3.6 U.S. EPA Reference Test Method 10 - Carbon Monoxide
The carbon monoxide (CO) testing was conducted in accordance with U.S. EPA Reference Test Method 10. Data
was collected online and reported in one-minute averages. The sampling system consisted of a stainless-steel probe,
Teflon sample line(s), gas conditioning system, and the identified gas analyzer. The gas conditioning system was a
non-contact condenser used to remove moisture from the gas. lf an unheated Teflon sample line was used, then a
portable non-contact condenser was placed in the system directly after the probe. Otherwise, a heated Teflon sample
line was used. The quality control measures are described in Section 3.9.
The relative accuracy of the CO CEMS was determined based on procedures found in 40 CFR 60, performance
Specification 4,A..
3.7 U.S. EPA Reference Test Method 25A - Total Hydrocarbons
The total hydrocarbons (THC) testing was conducted in accordance with U.S. EPA Reference Test Method 25A. Data
was collected online and reported in one-minute averages. The sampling system consisted of a stainless-steel probe,
heated Teflon sample line(s) and the identified gas analyzer. The quality control measures are described in Section 3.10.
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Source Test Report
The relative accuracy of the THC CEMS was determined based on procedures found in 40 CFR 60, performance
Specification 8A.
3.8 u.s. EPA Reference Test Method 205 - Gas Dilution System certification
A calibration gas dilution system field check was conducted in accordance with U.S. EpA Reference Method 205.
Multiple dilution rates and total gas flow rates were utilized to force the dilution system to perform two dilutions on
each mass flow controller. The diluted calibration gases were sent directly to the analyzer, and the analyzerresponse
recorded in an electronic field data sheet. The analyzer response agreed within 2Yo of the actual diluted gas
concentration' A second Protocol I calibration gas, with a cylinder concentration within 10% of one of the gas
divider settings described above, was introduced directly to the analyzer, and the analyzer response recorded in an
electronic field data sheet. The cylinder concentration and the analyzer response agreed within 2Zo. These steps
were repeated three (3) times. Copies of the Method 205 data can be found in the Quality Assurance/euality
Control Appendix.
3.9 Quatity Assurance/Quality Control - U.S. EPA Reference Test Methods 3A, 6C, 7E and l0
Cylinder calibration gases used met EPA Protocol I (+l- 2%) standards. Copies of all calibration gas certificates can
be found in the Quality Assurance/Quality Control Appendix.
Low Level gas was introduced directly to the analyzer. After adjusting the analyzer to the Low-Level gas
concentration and once the analyzer reading was stable, the analyzer value was recorded. This process was repeatedfor the High-Level gas. For the Calibration Error Test, Low, Mid, and High Level calibration gases were
sequentially introduced directly to the analyzer. All values were within 2.0 percent of the Calibration Span or 0.5
ppmv I %o absolute difference.
High or Mid Level gas (whichever was closer to the stack gas concentration) was introduced at the probe and the
timerequiredfortheanalyzerreadingtoreachg5percent or0.5ppmv/o/o(whicheverwaslessrestrictive)ofthegas
concentration was recorded. The analyzer reading was observed until it reached a stable value, and this value was
recorded. Next, Low Level gas was introduced at the probe and the time required for the analyzer reading to
decrease to a value within 5.0 percent or 0.5 ppmv/% (whichever was less restrictive) was recorded. If the Low-
Level gas was zero gas, the response was 0.5 ppmvloh or 5.0 percent of the upscale gas concentration (whichever
was less restrictive). The analyzer reading was observed until it reached a stable value and this value was recorded.
The measurement system response time and initial system bias were determined from these data. The System Bias
was within 5.0 percent of the calibration Span or 0.5 ppmvl%o absolute difference.
High or Mid Level gas (whichever was closer to the stack gas concentration) was introduced at the probe. After the
analyzet response was stable, the value was recorded. Next, Low Level gas was introduced at the probe, and the
analyzet value recorded once it reached a stable response. The System Bias was within 5.0 percent of the
Calibration Span or 0.5 ppmvl%o absolute difference or the data was invalidated and the Calibration Error Test and
System Bias were repeated.
Drift between pre- and post-run System Bias was within 3 percent of the Calibration Span or 0.5 ppmv/% absolute
difference. If the drift exceeded 3 percent or 0.5 ppmv/%, the Calibration Error Test and System Bias were repeated.
Clcan Harbors Aragonitc, UTAST-2024-'1517
l6 of 135
Pagc 3-3
fr
put6rpe
IiCIiNICAI G C)Source Test Report
An NOz - NO converter check was performed on the analyzer prior to initiating testing. An approximately 50 ppm
nitrogen dioxide cylinder gas was introduced directly to the Nox analyzer and the instrument response was recorded
in an electronic data sheet. The instrument response was within +/- l0 percent of the cylinder concentration.
A Data Acquisition System with battery backup was used to record the instrument response in one (l) minute
averages' The data was continuously stored as a *.CSV file in Excel format on the hard drive of a computer. At the
completion of testing, the data was also saved to the Alliance server. All data was reviewed by the Field Team
Leader before leaving the facility. once arriving at Alliance's office, all written and electronic data wasrelinquished to the report coordinator and then a final review was performed by the project Manager.
3.r0 Quality Assurance/euality control - u.s. EpA Reference Test Method 25A
cylinder calibration gases used met EPA Protocol I (+/- 2%) standards. Copies of all calibration gas certificates can
be found in the Quality Assurance/euality Control Appendix.
within two (2) hours prior to testing, zero gas was introduced through the sampling system to the analyzer. After
adjusting the analyzer to the Zero gas concentration and once the analyzer reading was stable, the analyzer value
was recorded. This process was repeated for the High-Level gas, and the time required for the analyzer reading toreach 95 percent of the gas concentration was recorded to determine the response time. Next, Low and Mid-Level
gases were introduced through the sampling system to the analyzer, and the response was recorded when it wasstable. All values were less than +/- 5 percent of the calibration gas concentrations.
Mid Level gas was introduced through the sampling system. After the analyzer response was stable, the value wasrecorded' Next, Zero gas was introduced through the sampling system, and the analyzer value recorded once itreached a stable response. The Analyzer Drift was less than +/_ 3 percent ofthe span value.
A Data Acquisition System with battery backup was used to record the instrument response in one (l) minute
averages' The data was continuously stored as a *.CSV file in Excel format on the hard drive of a computer. At thecompletion of testing, the data was also saved to the Alliance server. All data was reviewed by the Field Team
Leader before leaving the facility. once arriving at Alliance's office, all written and electronic data wasrelinquished to the report coordinator and then a final review was performed by the project Manager.
Clean Harbors - Aragonitc, UTAST-2024-1517
l7 of 135
Pagc 34
l8 of 135
FrarEE)AI Appendix A
Example Calculations
Locrtlon
Source
Project No.
Run No.
Psramter(r) 4JE
Meter Pre$ure (Pm), in. Hg
AHPm = Pb+-
where, 13'6
Ts
ps
BWSsal
Pb 25.32 = barometric pressure, in. HgAH 1.100 =pressurcdifferentialoforilice,inHlOPm 25.40 = in. Hg
Ab3olute Strck Grs Pres$ure (Ps), in. Hg
PoPs = Pb * 'o
where, 13'6
Pb 25.32 = barometric pressure, in. HgPg 0.21 : static prcssure, in. H2OPs 2534 =in. Hg
Strndsrd Meter Vdum (Vmstd), dscf
l7.636xVmxPmxYvmsro --------T;-
whcre,Y 0.995 = meter corection factorVm 39.210 = meter volume. cf
P. ---i,4L-- = absotute meter pressure, in. Hgfm ----36F- = absolute meter iemperature, .iVmstd 34.315 = dscf
Strndard Wet Volume (Vwstd), scf
Vwstd= 0.04706xMc
where,
Vlc 298.6 : Volume of H2O collected, ml
vwstd I-lT6:z--= r"1
Moisture Frrctiotr (BWSstt), direNiorless (theoreticrl 8t rttunted cotrditiotrs)
- -- / 2.827 \
10o r/-(E+36 /BWSsat =where,Da
151.3 = stack temperature, oF
25.3 : absolute stack gas pressurc, in. Hg0.3 - dimcnsionless
Moirture Frsction (BWS), direNiodes3
BWS Vwstd
whcre,fllvrctA t I/mcti\
Vwstd 14.052 = studard wet volure, scfVmstd 34.315 = standard meter volume, dscf
BWS ---l'f6T-= dimensionless
Moi6ture Fnctiotr (BWS), dimnrionlest
BWS = BWSmsd unless BWSsat < BWSmsd
where,
BWSsat 0-305 = moisture fiaction (theoretical at saturated conditions)BWSmsd 0.29t = moisture fraction (measured)BWS 0.291
Molecular Wclght (DRY-) (Md), lb^b-mte
. Md = (0.44 x o/oCO2) + (0.32 x o/oO2) *where,
CO, 9.3 : carbon dioxide concentration. yo
01 9.2 = oxygen concentmtion, yo
Md 29.85 : lb/lb mol
Moleculrr Weight (WET) (Ms), tb/ltsmte
(0.28 (100 - o/oCO2 - o/oO2))
Ms
wh€re,
= Md (1 - BWS) + 18.01s (BWS)
Md 29.85 = molecular wcight (DRy), lb/lb molBWS 0.291 = moisture fretion, dimcnsionlessMs 26.41 = Ib/lb mol
19 of 135
pu/tErre
Locrtlon
Source
Project No.
Run No.Par.mtcr(t) AJE
Aversge Veloclty (Vs), ftlsec
Vs = 85.49 x Cp x 1A p 1/21 avg x
whcre,
Cp 0.84 = pitot tube coemcient
A P'o 0.'727 = avcnge prc/post test velocity head ofstack gas. (i1.
fs ---?'ii]-= uverage pre/post test absolutc srack temperalure, "Rps ----7i5?-= absolute staik gas pressure, in. Hg
tnl. -f67I-: molecular wcighr of stack gas, lb/l-b molVs 49.9 : ff/sec
Averrge Strck Gr! Flow ra Stsck Conditiors (er), rcfm
Qa = 60x Vs x As
whera,
= stack gas velocity, fl/sec
= cross-sectional aea ofsack, ft1
Avcrege Stack Gar Flow rt Statrdard Condltiotrs (er), dscfm
Qsd= l7.616xQax(l -BWS)x Ps
Ts
Appendix A
Example Calculations
Itrol''
As
Qa
where,
Qa 58,763 = average stack gas flow at stack conditions, acfmBWS 0.291 = moisture fraction, dimensionless
Ps --T5Z--= ubsolute stack gas pressure, in. HgTs 610.9 = average prclpost test absolute stack temperature, oRqs--Jo-F-=ascrm
Dry Gri Meter Callbrrtlor Check (Yqr), dlmNlorlesg
Y-y'AH avg.
Yqa =
where,
Y 0.995 = meter corrcction factor, dimensionlessO 63 = run time, min.Vm 39.21 = total meter volume, dcfTm 509.3 : absolute metc. temperature, oR
AH@ 1.853 = orifice metercalibration coefiicient, in. H2OPb 25.32 =barometric prcssure, in. [Ig
AH avg I . I 00 = avcrage pressurc diffcrential ofori fice, in H2OMd 29.89 = molecular weight (DRY), lb/lb mol
(A H)r' 1.049 = average square root prcssue differential otorifice, (in. HrO)r/2Yqa 2.0 : dimensionless
(,+
x 100
20 of 135
pul6rrrce
I ir,l;,t,\ l,lrl
Location: Clean Harbors Aragonite LLC - Aragonite, UT
Appendix A
Example Calculations
where,
Source: Incinerator System (INC)
Project No.: AST-2024-15 17
Run No. /'lVlethodRun I / Method 3,A
Oz - Outlet Concentration (CoJ, o/o dry
Co,: (Cou,-Co)* ( dft;)
where,
Co.-:Tg-: Oz Concentration,oh dry
COz - Outlet Concentration (Cco), Y" dry
Cco,= (Cou,-Co)* ( **)
Cco, --=978- : COz Concentration, oh dry
Cob, 9.09 : average analyzer value during test, % dry
C" ---T?-: average of pretest & posttest zero response s,o/o dryCMA-TOF-: actual concentration of calibration gis,% dryCM-T038-: average of pretest & posttest calibration resjonses, % dry
Cob, 9.09 : average analyzer value during test, % dry
C"
-0Ttr-:
average of pretest & posttest zero response s,o/o dry
CMA
-TmO-
: actual concentration of calibration gis, % dry
CM
-T0:8-:
average of pretest & posttest calibration responses, oZ dry
2l of 135
pul6rrpE)
I I ii'.lll,/',i , (t ,ll'
Location: Clepn Harbors Aragonite LLC - Aragonite, UT
Source: Incinerafor Svstem /INC)
_ ProjgctPs.;ffi
Run No. /lVlethod Run I / Method l0
Appendix A
Example Calculations
CO - Outlet Concentration (Cco), ppmvd
where,
CO - Outlet Concentration (Cco"z), ppmvd @lyo O,
Cco"z: Ccox (ffi
where,Cco 5.07 : CO - Outlet Concentration, ppmvd
Co,
--:T9-
: oxygen concentration, %o
Cco"7
-j.-b-
: ppmvd @7 % o z
CO - Outlet Emission Rate (ER66), lb/hr
where,
Cco: (co6.-ce)x ( fri-rr)
Cob, 5.02 : average analyzer value during test, ppmvdC".-.0-: average of pretest & posttest zero responses, ppmvdCMA-25-i-0--: actual concentration of calibration gas, pp-rd-CM-74--: average of pretest & posttest calibration responses, ppmvdCco--:F: CO Concentration, ppmvd
ERco:CgsxMWxQsx60# x28.32 #
24.04 ;=;** 1.0E06 x453.592fl
Cco 5.07 : CO - Outlet Concentration, ppmvd
Mw
-28.01 -: CO molecular weight, g/g-mole
Qs :O[f-: stack gas volumehic fliw rate at standard conditions, dscfrnERco-038-: lb/hr
22 of 135
pul6rrrce)
NOx - Outlet Concentration (C*oJ, ppmvd
cNo*: (co6,-cs)x ( (*%J)
where,Cob, 109.49 : average analyzer value during test, ppmvdC"E:averageofpretest&posttestzeroresponses,ppmvd
CMA
-250TT--
: actual concentration of calibration gas, ppmvdCMw:averageofpretest&posttestcalibrationie.pons.,,ppmvd
C^,,-
-TITF-:
Nox Concentretinn nnmwd
Appendix A
Example Calculations
lil ' ,'\i , ll,,:,:
Location: Clean Harbors
Source: Incinerator
Project No.: AST-2024-l 5 17
Run No. /Method Run I / Method 7E
No*
-T|TZ--
: NOx Concentration, ppmvd
NOx - Outlet Concentration (Cro*"u), ppmvd @ 1yo O,
Cl.x.z: CxOrX (ffi
where,CNo* lll.24 : NOx - Outlet Concentration, ppmvd
Co, --l-9- : oxygen concentration, oZ
CNo*", ----lmD-: ppmvd @7% O,
NOx - Outlet Emission Rate (ERp6,), lb/hr
ED _ Cruo* x MW x Qs x 60 ff x28.32 #-,anO^ _
where.
CNo*lll.24 : NOx - Outlet Concentration, ppmvdMW 46.0055 _: NOx molecular weight, g/g-mole
Qs :0,+q -: stack gas volumetric flow rate at standard conditions, dscfrnERN.*--43-: lb/hr
23 of 135
pul6rrrcE)
1 .. i rl r,,\ i t, [1,,] iLocation: Clean Harbors te LLC -
Source: Incinerator
Project No.: AST-2024-1517
Run No. /Method Run I / Method 6C
SOr - Outlet Concentration (CsoJ, ppmvd
cso,: (cou,-co)*( tff.J
where,
Cso,
-0Jf-
: Soz Concentration, plmvd
SOz - Outlet Concentration (Cso..z), ppmvd @7o/o O,
LSo'c7 -- 20.9 -7Lso' x ( -or-)_
Appendix A
Example Calculations
Cob, 0.53 : average analyzer value during test, ppmvdC"-T-: average of pretest & posttest zero responses, ppmvd
CMA
-T0:0T-:
actual concentration of calibration gur, pp-ri'
CM
-T0T--:
average of pretest & posttest calibration i"rponr"r, ppmvd
where,Cso, 0.49 : SO, - Outlet Concentration, ppmvd
Co,
-9':I9-
: oxygen concentration, o%
Cro,",
-d33--:
ppmvd @7% o,
SOr - Outlet Emission Rate (ER56), lb/hr
ED _ Cso,xMWxQsx60ff x2832h
".rsor -
where,
Cso.
MW
0.49 = SOr - Outlet Concentration, ppmvd: SOz molecular weight, g/g-mole
Qs 30,491 : stack gas volumetric flow rate at standard conditions, dscfrnERso,-O:Ts-: lb/hr -
24 of 135
pul6rnclEr
. i.
Location: Clean Harbors Aragonite LLC - Araeonite. UT
Source: Ir"ir"Projectrys.;ffi
Run No. /lVlethod Run I / Method 25A
THC - Outlet Concentration (as C3H8) (Crsc), ppmvd
Cruc =Cr*.*
I-BWS
where,Cruc* 1.30 : THC - Outlet Concentration (as C3H8), ppmvw
BWS 0291 = moisture fraction, unitlessCrHC-T3-: ppmvd
THC - Outlet Concentration (as C3H8) (CrHc*), ppmvw
UTHCw -
lnt *.,
Cruc
where,
Crnc
MW
BWS 0.29 : moisture fraction, unitlessCrHC*-T30-: ppmvw
THC - Outlet Concentration (as C3H8) (Cruc"r), ppmvd @7V" O,
C"rHc"z : Crnc x 20.9 - 7[ 20.9 -O, )
Crrc 1.83 : THC - Outlet Concentration (as C3H8), ppmvd
Co,
-91T-
: oxygen concentration. o/o
Crnr"rT=ppmvd @7\oo,
Appendix A
Example Calculations
THC - Outlet Emission Rate (as C3H8) (ER1s6),lb/hr
rn C11s6 x MW x Qs x 60H x2n2#an rr-
where,
CrHcx(l -BWS)
1.83 : THC - Outlet Concentration (as C3H8), ppmvd
1.83 : THC - Outlet Concentration (as C3H8), ppmvd
44.1 : THC molecular weight, g/g-mole
Qs 30,491 : stack gas volumetric flow rate at standard conditions, dscfrnERrHc-i-8-: lb/hr
25 of 135
26 of 135
02 Summary
Location: Clean LLC-UT
Source: Incinerato. Syste- (tr{C
Project No.: AST -2024-1517
* Delimiter for runs not used in RA calculations
Conlidence Coefficient, CC
"=l#,,,1
where,
h.s:,s 2.306 = degrees of fieedom value
n 9 = number of runs selected for calculating the RA
Sd ---6lA- = srandard deviation of differenoe
CC --6.dJZ-- confidence coefficient
Relative Accuracy, RA
ldl+lcclRA = 73;;;;ix1oo
where,
d
CC
RM
RA
0.13
0n34
9.036
I .81
: average difference of Reference Method and CEMS: confidence coeflicient: reference meth od,, Yo dry
= relative accuracy,Yo
Run
No.Dete Time Reference Method
Or Concentration
Yo dn
CEMS - Primary
O, Concentration
%o dry
Average
Difference
Yo dryStartEnd
I
2
3
4
5
6
7
8
9
l0
1l
t2
5/8t24
5/8/24
518124
5t8/24
5t8/24
5t8/24
s/8/24
5t8/24
5/8/24
5/8/24
518/24
5/8/24
ll:28
I l:50
.2:ll
3:27
3:48
4:09
4:59
5:20
5:41
6:25
6:46
7:07
l:49
2:10
2:31
3:47
4:08
4:29
5: l9
5:40
6:01
6:45
7:06
7:27
9.19
8.67
8.31
9.05
8.93
9.63
8.79
9.64
9.13
8.77
9.73
10.38
9.09
8.62
8.21
8.87
8.77
9.46
8.68
9.47
8.99
8.56
9.52
l0.l I
0. l0
0.05
0. l0
0.18
0.16
0.17
0.1 I
0.17
0. l4
Averagr 9.O4 8.91 0. l3
Standard Deviation (Sd'0.044
Confi dence Coefficient (CC)0.034
Relative Accuracy (RA)l.El V"
Perforrnance Required - Mean Reference Method RA s 20%
Performance Specification Method PS3
27 of 135
pJ/lArEEr
Relative Accuracy, RA
ldl+lcclRA = 7r;;77:x1oo
where,
02 Summary
* Delimiter for runs not used id RA calculations
Confidence Coefficient, CC
cc = lto"t * ro;lVn I
where,
hs:,s 2.306 = degrees of fieedom value
n 9 : number of runs selected for calcutating the RA
Sd --d:O-r-: standard deviation of difference
CC - OIF-: confidence coefficient
d
CC
RM
RA
0. l30n44-
: average difference of Reference Method and CEMS: confidence coefficient9.036 : reference method, % dry1.87 : relative accuracy, 04
Locrtion: Clean Harbors Aragonite LLC - Aragonite, UT
Source: Incinerator System (INC)
Project No.: AST-2024-I 5 17
Run
No.Date Time Reference Method
Or Concentration
o/o drv
CEMS - Secondary
Or Concentration
Yo drv
Average
Difference
Yo drvStartEnd
I
2
3
4
5
6
7
8
9
l0
ll
t2
s/8/24
st8/24
518t24
5t8/24
518/24
5t8/24
s/8t24
5/8/24
5/8/24
5/8/24
5/8/24
5/8/24
tl:28
l:50
2:11
3:27
3:48
4:09
4:59
5:20
5:41
6:25
6:46
7:07
I l:49
l2:10
.2:31
3:47
4:08
4:29
5: l9
5:40
6:01
6:45
7:06
7:27
9.19
8.67
8.31
9.05
8.93
9.63
8.79
9.64
9.13
8.77
9.73
10.38
9. l0
8.64
8.24
8.84
8.82
9.46
8.65
9.49
8.96
8.52
9.50
10.09
0.09
0.03
0.07
0.21
0.1 I
0.17
0.14
0. l5
0.17
Averagr 9.04 8.91 0. l3
Standard Deviation (Sd'0.057
Confidence Coefficient (CC 0.044
Relative Accuracy (RA)t.E1 0h
Performance Required - Mean Reference Method RA<20Yo
Performance Specification Method PS3
28 of 135
FlaAI 02 Summary
Location: Clean Harbors Arasonite LLC - Arasonite. UT
Source: Incinerator Svstem (INC)
Project No.: AST-2024-1517
Run
No.Date Time Reference Method
Or Concentration
o/o d,rv
CEMS - Backup
Oz Concentration
Yo drv
Average
Difference
o/o dwStartEnd
I
2
J
4
5
6
7
8
9
l0
ll
t2
518/24
5/8/24
5/8124
5/8/24
5/8124
5/8/24
s/8/24
518/24
5/8/24
5/tl/24
5/8t24
5/8/24
.l:28
l:50
2:ll
3:27
3:48
4:09
4:59
5:20
5:41
6:25
6:46
7:07
l:49
2:10
2:31
3:47
4:08
4:29
5: l9
5:40
6:01
6:45
7:06
7:27
9.19
8.67
8.31
9.0s
8.93
9.63
8.79
9.64
9. l3
8.77
9.73
10.38
9.01
8.53
8.13
8.79
8.66
9.39
8.58
9.38
8.92
8.49
9.43
10.05
0.18
0.14
0. l8
0.26
0.27
0.24
0.21
0.26
o.2t
Average 9.04 8.82 0.22
Standard Deviation (Sd)0.045
Confidence Coefficient (CC'0.035
Relative Accuracy (RA 2.77 Vo
Performance Required - Mean Reference Method RA<20%
Performance Specifi cation Method PS3
* Delimiter for runs not used in RA calculations
Confidence Coefficient, CC
cc = ltoS'" sallVn I
where,
tonr, 2.306 : degrees offreedom value
n 9 : number ofruns selected for calcutating the RA
Sd -6.045-: standard deviation of differenceCC 0-0J-= confidence coefficient
Relative Accuracy, RA
ld I + lcclRA = -----:-----j----lx 100
where,
d, O.22 = average difference of Reference Method and CEMSCC 0.035 = confidence coeffrcient
RM 9.036 : reference method, % dryRA 237 : relative accuracy, o/o
29 of 135
COz Summary
Location: Clean Harbors Aragonite LLC - Arasonite. UT.JUUTCEa llur,ElaLUI JySLgm (Urt
'Project No.i AST-2024-| 5 17
Run
No.Date Time Reference Method
COr Concentration
%6 drv
CEMS - Primary
COr Concentration
V" drv
Average
Difference
Yo drvStrrtEnd
I
2
3
4
5
6
7
8
9
t0
u
t2
st8/24
5/8/24
5t8/24
s/8/24
5t8/24
5/8t24
518/24
s/8/24
5t8/24
5/8124
5/8/24
5/8/24
I l:28
I l:50
l2:ll
l3:27
L3:48
4:09
4:59
5:20
5:41
6:25
6:46
7:07
l:49
2:10
2:31
3:47
4:08
4:29
5:19
5:40
6:01
6:45
7:06
7:27
9.28
9.77
9.91
9.48
9.47
8.88
9.78
8.92
9.32
9.68
9.08
8.3 8
9.37
9.79
9.84
9.49
9.47
8.89
9.80
8.96
9.32
9.69
9.13
8.48
-0.02
-0.01
0.00
-0.01
-0.02
-0.04
0.00
-0.01
-0.05
Average 9.38 9.39 -0.02
Standard Deviation (Sd)0.018
Confidence Coefficient (CC)0.014
Relative Accuracv (RA)0.34 yo
Performance Required - Mean Reference Method RAs20%
Performance Specification Methoc PS3i Delimiter for runs not used in M calculations
Confi dence Coef{icient, CC
cc = ltolt, sallVn I
where,
t{s.s 2.306 = degrees offreedom value
n 9 : number of runs selected for calculating the RA
Sd -T"01 8- = standard deviation of difference
CC ---O'J-]T- : confi dence coeffi cient
Relative Accuracy, RA
ldl+lcclRA - 'x'l 0oAS or RM
where,
d -0.02 : average difference of Reference Method and CEMS
CC ---0TiA-: confidence coefficient
RM j-.liil: reference method, % dryRA 0.34 : relative accuracy, 7o
30 of 135
FTAA!'--t TEE!CO2 Summary
Location: Clean Harbors Aragonite LLC - Arasonite. UT
- Sor."",
Project No.: AST-2024-1517
Run
No.Date Time Reference Method
COr Concentration
o/o dn
CEMS - Secondary
COz Concentration
Yo drv
Averege
Difference
%o dryStartEnd
I
2
3
4
5
6
7
8
9
l0
1l
t2
5t8/24
5/8/24
st8t24
518/24
518/24
5/8/24
518/24
5/8124
5/8/24
5/8/24
5/8124
5/8124
t l:28
ll:50
t2:l l
l3:27
3:48
4:09
4:59
5:20
5:41
6:25
6:46
7:07
l:49
2:10
2:11
3:47
4:08
4:29
5:19
5:40
6:01
6:45
7:06
7:27
9.28
9.77
9.91
9.48
9.47
8.88
9.78
8.92
9.32
9.68
9.08
8.3 8
9.3 r
9.74
9.85
9.46
9.43
8.87
9.77
8.94
9.28
9.68
9.10
8.47
-0.03
0.03
0.02
0.04
0.01
0.01
-o.02
0.00
-0.02
Averaqt 9.37 9.37 0.00
Standard Deviation (Sd'0.024
Confi dence Coefficient (CC'0.019
Rehtive Accurrcy (RA)0,25 0
Perforrnance Required - Mean Reference Method RAs20%
Performance Specifi cation Method PS3* Delimiter for runs not used in RA calculations
Confidence Coeflicien! CC
cc=lff,sal
where,
h.es 2.306 = degrees of freedom value
n 9 .: number ofruns selected for calculating the RASd--6:0-'il-= standard deviation of differenceCC 0.019 : confidence coefficient
Relative Accuracy, RA
ld l+ lcctRA = ;i;;;#x1oo
where,
d 0.00 : average difference of Reference Method and CEMS
CC --l:dl!-= confidence coefficientRM 9.37 | = reference meth od, % dryRA 025 =relative accuracy,%o
31 of 135
FraAITEE
Location: Clean Harbors
Source: Incinerator
Project No.: AST-2024-1 51,7
COz Summary
Run
No.Date Time Reference Method
COr Concentration
%o drv
CEMS - Backup
COr Concentration
Yo drv
Average
Difference
o/" drvStartEnd
I
2
3
4
5
6
7
8
9
l0
ll
t2
5/8/24
5/8/24
518/24
5/8/24
5/8/24
s/8/24
s/8124
518/24
5/8/24
5/8/24
5/8/24
s/8t24
l:28
l:50
2:ll
3:27
3:48
4:.09
4:59
5:20
5:41
6:25
6:46
7:07
ll:49
l2:10
l2:31
'.3:47
4:08
4:29
5: l9
5:40
6:01
6:45
7:06
7:27
9.28
9.77
9.91
9.48
9.47
8.88
9.78
8.92
9.32
9.68
9.08
8.38
9.1 I
9.s6
9.66
9.25
9.24
8.65
9.57
8.72
9.07
9.47
8.88
8.22
0.17
0.21
0.23
0.23
0.21
0.20
0.21
0.20
0.16
Averase 9.25 9.05 0.20
Standard Deviation (Sd)0.023
Confidence Coefficient (CC)0.018
Relative Accurecv (RAl 2.38 0h
Perforrnance Required - Mean Reference Method RA<20%
Performance Specifi cation Method PS3t Delimiler for runs not used in RA calculations
Conlidence Coefficient, CC
..=lH",ol
where,
h.e1s 2.306 = degrees of freedom value
n 9 : number of runs selected for calculating the RASd 0.023 = standard deviation ofdifferenceCC 0.018 - confidence coefficient
Relative Accuracy, RA
ldl+lcclRA = 7r;;;7x1oo
where,
d 0.20 : average difference of Reference Method and CEMS
CC ---dIiT-= confidence coefficientRM 9249 : reference method, % dryRA- 238 : relative accuracy,yo
32 of 135
puIAnGe
Project No.: AST-2024-I 517
SO2 Summary
Locstiotr: Clean Harbors Aragonite LLC - Amgonite. UT
Source: Incinerator System (tr,Ic)
Run
No.Date Time Reference Method
SOr Concentration
DDmvd
CEMS - Primary
SOr Concentration
DPmvd
Average
Difference
oomvdStarlEnd
I
2
3
4
5
6
7
8
9
l0
ll
l2
st8/24
5/8/24
518/24
5/8/24
5/8/24
518/24
5/8/24
5/8/24
5/8/24
5/8/24
5/8/24
5/8t24
I l:28
I l:50
l2:ll
l3:27
t3:48
l4:09
L4:59
.5:20
5:41
6:25
6:46
7:07
I l:49
l2:10
12:31
l3:.47
l4:08
l4:29
l 5:19
l5:40
l6:01
l6:45
17:06
17:27
0.49
0.82
0.76
I .61
2.15
2.27
0.85
0.39
0.43
0.25
0. l3
0.05
t.02
0.62
1.59
0.87
1.06
0.66
0.68
0.50
0.54
0.50
0.73
0.8 r
-0.53
0.20
0.74
0. l7
-0.1 I
-0.1 I
-o.25
-0.60
-0.76
Average 0.s6 0.70 -0. 14
Standard Deviation (Sd)0.469
Applicable Source Standard (AS)78.4(\
Confi dcnce Coeffi cient (CC)0.360
Relative Accuracy (RA)0.63 o/o
Performance Required - Applicabte Source Standard RAs l0%
Performance Specification Method PS2
+ Dclimiter for runs not uscd in RA calculations
Conlidence Coellicien! CC
..:l#"rol
where,
to.czs
n
Sd
CC
2.306 = degrees offreedom value
number ofruns selected for calculating the RA0.469 : standard deviation ofdifference0.360 = confidencc coefficient
Relative Accuracy, RA
ldl+lcclne = 7s;;;#x1oo
where,
d -0. l4 : average diffcrcnce of Refcrence Mcthod and CEMS
CC --61e0-= confidence cocfficient
AS J-8J6-d-: applicabte source standard, ppmvdRA 0.63 =relative accuracy,yo
33 of 135
FIATEEAI SO2 Summary
Location: Clean Harbors LLC.UT
Source: Incinerator System (SiC)
Project No.: AST-2024-1517
* Delimiter for runs not usod in RA calculations
Conlidence Coefficien! CC
":lH"ol
where,
h.ns 2.306 = degrees of freedom valuen 9 : number of runs selected for calcutating the RASd--6'318-= standard deviation of differenceCC 0.444 : confidence coefficicnt
Relative Accuracy, RA
ldl+lcclM = 75;ffix 1oo
where,
d -0.17 - average difference of Refercnce Mcthod and CEMSCC 0.444 : confidcnce coeflicicnt
AS -I.0d0- = applicable source standard, ppmvd @ 7 o/o OzRA-- 0.68 -: relative accuracy, yo
Run
No.Date Time Reference Method
SOr Concentration
opmvd @.7 0h ot
CEMS - Primsry
SOr Concentration
ppmvd @7 %o O,
Averrge
Difference
ppmvd@7 %"O,Start End
I
2
3
4
5
6
7
8
9
l0
1l
t2
5/8124
5/8/24
518124
5/8124
5/8/24
5/8/24
518/24
5/8124
5/8/24
5/8t24
5/8/24
5/8/24
I l:28
I l:50
12:ll
l3:27
l3:48
l4:09
l4:59
l5:20
5:41
.6:25
6:46
7:07
ll:49
l2:10
l2:31
.3:47
4:08
4:29
5:19
5:40
6:01
6:45
7:06
7:27
0.s8
0.94
0.84
1.89
2.50
2.80
0.98
0.49
0.51
0.29
0. l6
0.06
1.27
0.67
1.78
0.99
t.2t
0.80
0.79
0.62
0.63
0.s7
0.91
l.0s
-0.69
0.27
-0.94
0.90
0.19
-0. l3
-0.12
-0.28
-0.75
Averagt 0-74 0.91 -0.17
Standard Deviation (Sd'0.578
Applicable Source Standard (ASl 9l
Confi dence Coeffi cient (CC)0.444
Relative Accuracy (RA)0.68 0h
Performance Required - Applicable Source Standard RA< l0%
Performance Specifi cation Method PS2
34ofl35
SO2 Summary
FTATEE)
' : n ,.' :1
AI
Location: Clean Harbors Amgonite LLC - Aragonite. UT
Source: lncinerator System (INC)
Project No.: 4ST-2O24-1517
Run
No.Date Time Reference Method
SOr Concentration
oomvd
CEMS - Secondary
SOz Concentration
pomvd
Average
Difference
oomvdStortEnd
I
2
3
q
5
6
7
8
9
l0
1l
t2
5/8/24
5/8t24
st8/24
5/8/24
5/8t24
st8/24
5/8124
5t8/24
5/8t24
5t8/24
s/8124
518/24
l:28
l:50
2:ll
3:27
3:48
4:09
4:59
5:20
5:41
6:25
6:46
7:07
l:49
2:10
2:31
3:47
4:08
4:29
5:19
5:40
6:01
6:45
7:06
7:27
0.49
0.82
0.76
l .61
2.t5
,11
0.85
0.39
0.43
0.25
0. l3
0.05
0.07
0.07
0.86
0.30
0. l3
0.3s
0.34
0.20
0.30
0.57
0.84
0.80
0.42
0.75
-0. l0
0.51
0. l9
0.t3
-0.32
-0.71
-0.75
Average 0.46 0.45 0.01
Standard Deviation (Sd)0.529
Applicable Source Standard (AS)78.46
Confi dence Coefficient (CC)0.40't
Relative n".r."., {*,0.54 0/"
Performance Required - Applicable Source Standard RAs l0%
Performance Speci fi cation Methor PS2
* Delimitcr for runs nol used in RA calculations
Confi dence Coefficient, CC
cc = ltogs x sdllVn I
where,
h.qzs
n
Sd
CC
2.306 = degrees offreedom value
9 : number ofruns selected for calculating the RA0.529 = standard deviation ofdifference
0.407 : confidcnce coefficicnt
Relative Accuracy, RA
ldl+l6clRA = 7s;;TM:x loo
where,
d 0.01 : averagc differcnce of Rcfcrence Method and CEMS
CC -d70r- = confidence coefficientAS 78.460 : applicable source standard, ppmvdRA 0.54 : relative accuracy,%o
35 of 135
FraAT SO2 Summary
Location:
Source:
Project No.:
Harbors
Incinerator
AST-2024-l 5 I 7
te, UT
Run
No.Date Time Reference Method
SOr Concentration
ppmvd@7 YoO,
CEMS - Secondary
SOr Concentration
ppmvil @7 %o Ot
Average
Difference
pgmvd (D,7 o/o OzStartEnd
I
2
3
4
5
6
7
8
9
l0
1l
t2
5/8/24
518t24
518/24
5t8/24
s/8t24
5t8/24
sl8t24
5/8/24
518t24
518124
5/8/24
518t24
t l:28
I l:50
t2:11
.3:27
3:48
4:09
4:59
5:20
5:41
6:25
6:46
7:07
tl:49
l2: l0
l2:31
.3:47
4:08
4:29
5:19
5:40
6:01
6:45
7:06
7:27
0.58
0.94
0.84
1.89
2.50
2.80
0.98
0.49
0.51
0.29
0. l6
0.06
0.07
0.08
0.99
0.35
0.15
0.43
0.38
0.24
0.36
0.64
1.04
1.02
0.51
0.86
-0. l5
0.60
0.25
0.15
-0.35
-0.8E
-0.96
Averaq(0.54 0.54 0.00
Standard Deviation (Sd'0.639
Applicable Source Standard (AS'9l
Confi dence Coefficient (CC)0.491
Relative Accuracv (RA)0-54 o/o
Performance Required - Appticable Source Standard RAs t0%
Performance Specifi cation Method PS2
* Dclimiter for runs not uscd in RA calculations
Confidence Coefficient, CC
cc = lto'Is x sdllVn I
where,
he75 2.306 : degrees offreedom valuen 9 : number of runs selected for calculating the RASd 0.639 = standard deviation ofdifferenceCC 0.491 = confidence cocfficicnt
Relative Accuracy, RA
ldl+lcclna = 7s;;;r:x1oo
where,
d 0.00 : average differcnce of Referencc Method and CEMSCC 0.491 : confidencs coefficientAS 9l .000 : applicable source standard, ppmvd @ 7 o/o OzRA 0.54 : relative accuracy,yo
36 of 135
SO2 Summary
', f; t- it I
Location: Clean Harbors Aragonite LLC - Aragonite, UT
Source: Incinerator System (INC)
Project No.: AST -2024-15 17
Run
No.Date Time Reference Method
S0r Concentration
nnmvd
CEMS - Backup
SOr Concentration
nnmvd
Average
Difference
oomvdStartEnd
I
2
3
4
5
6
7
8
9
l0
ll
t2
5/8/24
5l8l24
s/8/24
5/8124
s/8t24
5/8/24
518/24
518/24
5/8/24
5/8124
5t8t24
518/24
l:28
l:50
2:ll
3:27
3:48
4:09
4:59
5:20
5:41
6:25
6:46
7:07
ll:49
l2:10
l2:31
l3:47
t4:08
',4:29
.5: l9
.5:40
6:01
6:45
7:06
7:27
0.49
0.82
0.76
I .61
2.15
2.27
0.85
0.39
0.43
0.25
0. l3
0.05
0.000
0.000
0.200
0.000
0.010
0.000
0.030
0.000
0.000
0.070
0.000
0.000
0.49
0.82
0.56
0.82
0.39
0.43
0.18
0. l3
0.05
Averag(0.46 0.033 0.43
Standard Deviation (Sd)0.280
Applicable Source Standard (AS)78.46
Confidence Coefficient (CC'0.216
Relative Accuracv (RA 0.82 o/o
Performance Required - Applicable Source Standard RA < l0%
Performance Specifi cation Method PS2
* Delimiter lor runs not used in RA calculations
Conlidence Coeflicient, CC
cc = ltoIt, sally'n I
where,
hq,s 2.306 : degrees of freedom value
n 9 : number of runs selected for calculating the RA
Sd -lfE6-: standard deviation of differenceCC 0.216 : confidence coefficient
Relative Accuracy, RA
ldl+lcclRA = lqsorRM xloo
where,
d 0.43 : average differencc of Rcfcrcncc Method and CEMSCC 0.216 : confidcnce coeffrcientAS 78.460 = applicable source standard, ppmvd
RA 0.82 : relative accuracy, To
37 of 135
SO2 SummaryTEE!FlaAI
Location: Clean Harbors
Project No.: AST-2024-1517
Run
No.Date Tlme Reference Method
SOr Concentration
ppmvd@1 YoOz
CEMS - Backup
SOr Concentrrtion
Averege
Difference
opmyd @.7 Yo O,Starl End ppmvd@7 o/oOz
I
2
3
4
5
6
7
8
9
l0
lt
l2
5/8/24
5/8/24
518t24
5/8/24
5/8/24
5/8/24
5/8/24
5/8124
518t24
5/8/24
5/8t24
5/8/24
I l:28
I l:50
12:11
l3:27
l3:48
l4:09
14.,59
l5:2O
I 5:41
l6:25
l6:46
17:07
ll:49
l2: l0
l2:31
l3:47
.4:08
4:29
5:19
5:40
6:01
6:45
7:06
7:27
0.58
0.94
0.84
1.89
2.50
2.80
0.98
0.49
0.51
0.29
0. l6
0.06
0.000
0.000
0.230
0.000
0.010
0.000
0.040
0.000
0.000
0.080
0.000
0.000
0.58
0.94
0.61
0.94
0.49
0.51
0.21
0.16
0.06
Average 0.54 0.039 0.50
Standard Deviation (Sd 0.3ls
Applicable Source Standard (AS 9t
Uontldence Coclticicnt (CC'0.242
Relative Accuracv fRA'0.81 yo
reno[nance Kequlred - Applicable Source Standard RA< t0%
Performance Specifi cation Method PS2* Dclimitcr for runs not uscd in RA calculations
Conlidence Coefficient, CC
.. =l#,*l
where,
to.sr: 2.306 = degrees offreedom value
Relative Accuracy, RA
ld I + lcclRr6\ : 7r;;*7x 1oo
where,
d 0.50 - average difference of Referencc Method and CEMSCC-IZA- = confidencc coefficientAS 9l "000- = applicable source standard, ppm vd (@ 7 yo OzRA 0f l -:riLtive acatracy,yo
n 9 : number of runs selected for calculating the RA
Sd O.3 I 5 : qtandard /aviatia- ^fiiff-- -^^Sd 0.315 : standard deviation ofdifferenceCC 0.?42 : confidence coefficicnt
38 of 135
NOx Summary
Location: Clean Harbors Arasoni UT
Source:
Project No.: AST -2024-1 5 17
Run
No.Date Time Reference Method
NOx Concentration
oomvd
CEMS - Primary
NOx Concentration
oomvd
Averuge
Difference
pDmvdStartEnd
I
2
3
4
5
6
7
8
9
l0
ll
t2
5/8/24
518124
518/24
5/8/24
5/8/24
5t8/24
5/8124
5/8/24
5/8/24
5/8/24
5/8/24
s/8/24
ll:28
I l:50
l2:l I
l3:27
l3:48
l4:09
l4:59
l5:20
l5:41
l6:25
l6:46
17:07
ll:49
l2:10
l2:31
l3:47
t4:08
l4:.29
t5:19
5:40
6:01
6:45
7:06
7:27
11.24
16.99
36.54
36.51
26.77
44.61
43.77
73.45
87.93
44.12
32.44
15.13
I14.t7
t2t.9t
I 47.80
t41.83
.34.20
54.07
55.49
82.68
r00.39
48.88
37.20
16.91
-2.93
-4.92
-s.32
-7.43
-9.46
-9.23
-4.76
-4.76
-1.78
Average 3.47 39.09 5.62
Standard Deviation (Sd 2.626
Confidence Coefficient (CC)2.01 8
Relative Accuracy (RA)5.72 yo
Performance Required - Mean Reference Method RA<20%
Performance Specifi cation Method PS2
' Delimiter for runs not used in RA calculations
Confidence Coefficient, CC
cc = ltol'x sallVn I
where,
t{.s1s 2.306 = degrees offreedom valuen 9 = number of runs selccted for calculating the RA
Sd -Z;U-= standard deviation of diflerenccCC 2.018 = confidence coefficient
Relative Accuracy, RA
ldl+lcclRA = 7s;;Tr:x1oo
where,
d -5.62 - average difference of Reference Method and CEMSCC 2.018 : confidence coefficientRM 133.47 4 : reference method, ppmvd
RA 5J2 : relative accuracy, Zo
39 of 135
AI FTANGE
,r i:iL' :
NOx Summary
Location: Clean Harbors
Source: lncinerator
Project No.: AST-2024-| 5 17
Run
No.Date Tlme Reference Method
NOx Emission Rate
lb/hr
CEMS - Primary
NOx Emission Rate
lb/hr
Average
Difference
lb/hrStartEnd
I
2
3
4
5
6
7
8
9
l0
ll
t2
5/8/24
5t8t24
s/8/24
518/24
5/8/24
518/24
518/24
5t8/24
5/8/24
st8/24
5t8/24
5/8t24
I l:28
I l:50
t2:l I
l3:27
l3:48
l4:09
.4:59
5:20
5:41
6:25
6:46
7:07
I l:49
l2:10
l2:31
l3:47
l4:08
l4:29
l5: l9
l5:40
l6:01
l6:45
17:06
17:27
24.32
25.08
28.92
29.64
27.96
31.85
30.89
38.42
44.35
29.37
2E.62
25.63
25.79
26.67
32.75
31.77
30.39
34.52
34.63
41.47
45.37
33.20
31.25
26.81
-t.47
-l.59
-2.13
-2.43
-2.67
-3.05
-1.02
-2.63
-r. l8
Average 30.65 32.67 -2.02
Standard Deviation (Sd)0.730
Applicable Source Standard (AS)44.2
Confidence Coefficient (CC)0.561
Relative Accuracv (R 4,'8.42 Yo
Performance Required - Mean Reference Method RA s 20%
Performance Specification Method PS2* Delimiter for runs not uscd in RA calculations
Confi dence Coefficient, CC
cc = ltogs x sdllVn I
where,
h91s 2.306 : degrees of freedom value
n 9 : number of runs selected for calculating the RASd lJ30-: standard deviation of difference
CC -lEl-: confidencc coeflicient
Relative Accuracy, RA
ldl+lcclRA = 7s;;;r:x 1oo
wheren
d -2.02 = average differencc of Rcference Method and CEMS
CC -l3T-= confidcnce coefficicntRM 5-652 = reference method, lb/hr
RA --TA- : relative accuracy, yo
40 of 135
NOx Summary
Location: Clean Harbors Aragonite LLC - Afagonite, UT
Source: Incinerator Svstem (INC)
Project No.:
Confidence Coeflicient, CC
cc=1ff*sal
where,
to.ns 2.306 = degrees of freedom value
n 9 : number ofruns selected for calculating the RA
Sd --t 0- = standard deviation of differenceCC--di- - confidence cocfficicnt
Relative Accuracy, RA
ld I + lcclRA = 7s;;Tr:x1oo
where,
d 4.37 : average difference of Reference Method and CEMSCC 2.245 : confidence coefficientRM 133.474 - reference method, ppmvdRA 4.96 = relative accuracy, Zo
Run
No.Date Time Reference Method
NOx Concentration
opmvd
CEMS - Secondary
NOx Concentration
Averege
Difference
pDmvdStartEndDDmvd
I
2
3
4
5
6
7
8
9
l0
ll
t2
5/8/24
5/8/24
sl8l24
5/8/24
518/24
5t8/24
518/24
5/8/24
5/8/24
5/8/24
5/8t24
5/8t24
I l:28
I l:50
t2:l I
l3:27
3:48
4:09
4:59
5:20
5:41
6:25
6:46
7:07
l:49
2:10
2:31
3:47
4:08
4:29
5: l9
5:40
6:01
6:45
7:06
7:27
ltt.24
16.99
36.54
36.51
26.77
44.61
43.77
73.4s
87.93
44.t2
32.44
15.t3
I13.33
t20.79
t45.72
t41.28
t33.20
t54.04
154.32
180.45
99.82
45.94
36.44
15. l3
-2.09
-3.80
-4.77
-6.43
-9.43
-7.00
- 1.82
4.00
0.00
Averasr 33.47 37.84 -4.3'1
Standard Deviation (Sd'2.920
Confidence Coefficient (CC'2.245
Relative Accuracv (RA 4,96 0/o
Performance Required - Mean Reference Method RA < 20o/o
Performance Specification Method PS2* Delimiter for runs not uscd in RA calculations
4l of 135
NOx Summary
Location:
Source:
Project No.:
Clean Harbors
lncinerator
Run
No.Date Time Reference Method
NOx Emission Rate
CEMS - Secondary
NOx Emission Rate
Averoge
Difference
lb/hrStartEndlb/hr lb/hr
I
2
J
4
5
6
7
8
9
t0
ll
t2
s/8/24
5/8124
s/8/24
5/8/24
5/8/24
5/8/24
5/8/24
5/8/24
5/8/24
518124
s/8/24
5/8t24
ll:28
Il:50
I2:l I
l3:27
l3:48
4:09
4:59
5:2O
5:41
6:25
6:46
7:07
l:49
2:10
2:31
3:47
4:08
4:29
5:19
5:40
6:01
6:45
7:06
7:27
24.32
25.08
28.92
29.64
27.96
31.85
30.89
38.42
44.35
29.37
28.62
25.63
25.60
26.43
32.29
31.65
30.1 6
34.51
34.37
40.97
45.24
32.55
3 1.08
26.40
-1.28
-t.3s
-2.01
-2.20
-2.66
-2.55
-0.89
-2.46
-0.77
Average 30.65 32.45 1.80
Standard Deviation (Sd)0.736
Applicable Source Standard (AS)44.2
Confi dencc Coeffi cient (CC)0.566
Relative Accuracy (RA)7.71 yo
Performance Required - Mean Reference Method RA < 20%
Performance Specification Method PS2
* Dclimitcr for runs not uscd in RA calculations
Confidence Coefficient, CC
cc : lto't" , sallVn I
where,
h.ns 2.306 = degrees of freedom value
n 9 = number ofruns selected for calculating the RASd--l7JZ-= standard deviation of differenceCC 0.566 = confidence coefficient
Relative Accuracy, RA
ldl+lcclrut = rrt;up:xloo
where,
d -1.80 = averagc differcnce of Referencc Mcthod and CEMS
CC
-.5G6- = confi dcnce cocfficicntRM 30-652 = reference method, lbihrRA 7Jl = relative accuracy,yo
42 of 135
FlaAI NOx Summary
Location: Clean Harbors
Source: Incinerator
Project No.: AST.
Run
No.Date Time Reference Method
NOx Concentretion
pomvd
CEMS - Backup
NOx Concentration
PPmvd
Average
Difference
oomvdStartEnd
I
2
3
4
5
6
7
8
9
l0
ll
t2
5t8/24
5t8/24
518t24
5t8/24
5t8/24
5t8/24
s/8/24
5/8124
518/24
5/8124
5/8124
518/24
L l:28
I 1:50
l2:ll
l3:27
3:48
4:09
4:59
5:20
5:41
6:25
6:46
7:07
l:49
2:10
2:31
3:4'l
4:08
4:29
5: l9
5:40
6:01
6:45
7:06
7:27
1.24
t6.99
36.54
36.51
26.77
44.61
43.'77
73.45
87.93
44.12
32.44
l5.l 3
I I 1.88
I19.99
145.56
140.33
r 32. l0
r52.00
t53.43
t80.9 r
.97.97
47.30
34.89
14.45
-0.64
-3.00
-3.82
-s.33
-7.39
-7.46
-3.18
-2.45
0.68
Averagt 33.47 137.09 -3.62
Standard Deviation (Sd'2.768
Confi dence Coefficient (CC'2.t28
Relative Accuracv (RA'4.31 Yo
Perlormance Required - Mean Reference Methoc RA<20%
Performance Specifi cation Method PS2
r Delimiter for runs not used in RA calculations
Confidence Coefficient, CC..=lH,'l
where,
h gzs
n
Sd
CC
2.306 : degrees of freedom value: numbcr ofruns sclccted for calculating the RA
= standard dcviation ofdifference: confidcnce coefficicnt
9
2168
2.t28
Relative Accuracy, RA
ldl+lcclRA = 7s;;Tr:x1oo
where,
d -3.62 - average difference of Reference Method and CEMS
CC -lrI-= confitlence coefficientRM IEIZ : refererice method, ppmvdRA- 431 :relative
^"ur^"y,;/o
43 of 135
FTAAI NOx Summary
Location: Clean
Source: lncinerator
Project No.: AST-2024-l 5 I 7
te LLC.
Run
No.Date Time Reference Method
NOx Emission Rate
lb/hr
CEMS - Backup
NOr Emission Rate
lb/hr
Average
Difference
lb/hrStariEnd
I
2
3
4
5
6
7
8
9
l0
ll
t2
518/24
518t24
5t8124
5/8/24
5/8/24
5/8/24
s/8/24
5/8124
5/8/24
5/8/24
5/8/24
5/8/24
ll:28
I l:50
l2:11
l3:27
13:48
l4:09
l4:59
l5:20
l5:41
l6:25
l6:.46
17:07
ll:49
l2:10
l2:31
l3:47
l4:08
l4:29
t 5:19
L5:40
6:01
6:45
7:06
7:27
24.32
25.08
28.92
29.64
27.96
3 1.85
30.89
38.42
44.35
29.37
28.62
25.63
25.27
26.25
32.25
31.43
29.91
34.06
34.17
41.07
44.82
32.85
30.72
26.25
-0.95
-1.t7
-1.79
-1.95
-2.21
-2.65
-0.47
-2.t0
-o.62
Average 30.65 32.20 1.55
Standard Deviation (Sd)0.769
Applicable Source Standard (AS)44.2
Confi dence Coefficient (CC)0.591
Relative Accuracv (RA)6.97 0/o
Performance Required - Mean Reference Method RA s 20%
Performance Specifi cation Method PS2I Dclimiter for rus no( used in RA calculations
Confi dence Coeflicient, CC..:lH,*l
where,
he:,s 2.306 : degrees offreedom value
n 9 : number of runs selected for calculating the RA
Sd -l%t-: standard deviation of differenceCC 0.591 : confidencc coefficicnt
Relative Accuracy, RA
ldl+lcclRA = 7s;;;r:x 1oo
where,
d -1.55 = avcrage differcnce of Referencc Method and CEMSCC 0.591 = confidencc coefficient
RM -30.8t-: reference method. lb/hrRA 6.97 = relarive accuracy,7o
44 of 135
pull6noEr
Location:
Source:
Project No.:
ai
Clean
Incinerator
AST-2024-1517
te LLC -
CO Summary
Run
No.Date Time Reference Method
CO Concentmtion
DDmvd
CEMS - Primrry
CO Concentration
Dpmvd
Average
Difference
onmvdStartEnd
I
2
3
4
5
6
7
8
9
l0
u
t2
5t8t24
5/8/24
sl8l24
s/8/24
5t8/24
5/8/24
st8/24
5/8/24
5t8124
5/8/24
5/8t24
5/8124
I l:28
l l:50
2:11
3:27
3:48
4:09
4:59
5:20
5:41
6:25
6:46
7:07
l:49
2:10
2:31
3:47
4:08
4:29
5: l9
5:40
6:01
6:45
7:06
7:27
5.07
2.30
r.02
1.23
5.92
1.35
5.86
l .33
1.30
6.72
1.30
1.40
I Ll9
1.76
0.3s
0.50
15.01
0.83
1.73
0.86
0.80
13.20
0.80
0.94
0.54
0.67
0.73
0.52
-5.87
0.47
0.50
0.50
0.46
Averapr 1.90 2.06 -0. l6
Standard Deviation (Sd 2.14t
Confidence Coeffrcient (CC'1.645
Alternative Relative Accurecv (RA 1.8 I DDM
Alternative Performance Required (d + CC <5opm
Performance Specifi cation Method PS 4Ai Delimiter for runs not used in RA calculations
Conlidence Coefficient, CC
cc=ltoI'xsally'n I
where,
b'js 2.306 : degrees of freedom valuen 9 = number ofruns selected for calculating thc RASd 2.141 - standard deviation ofdiffercnccCC 1.645 = confidcnce coefficicnt
45 of 135
FraAI CO SummarylEeri-/l
Location: Clean Harbors
Source: Iocinerator
Project No.: AST
Run
No.Date Time Reference Method
CO Concentration
ppmvd@7 YoO,
CEMS - Primary
CO Concentration
ppmvd @7 %o O,
Average
Difference
oomYd (4.7 Vo O,Start End
I
2
J
4
5
6
7
8
9
l0
1l
t2
5t8/24
5/8/24
5t8124
5/8124
518/24
5/8/24
5/8/24
5/8124
5/8/24
5/11/24
5/8/24
5/8/24
tl:28
I l:50
t2:l I
l3:27
L3:48
4:09
.4:59
5:20
5:41
6:25
6:46
7:07
l:49
2:10
2:31
3:47
4:08
4:29
5: l9
5:40
6:01
6:45
7:06
7:27
6.03
2.61
l.l3
1.44
6.88
t.67
6.73
1.64
I .53
7.70
1.62
1.85
t2.24
1.86
0.39
0.57
15.80
1.00
12.28
1.05
0.93
13.33
0.98
1.22
0.75
0.74
0.87
0.67
-5.55
0.59
0.60
0.64
0.5f
Average 2.25 2.25 -0.01
Standard Deviation (Sd)2.081
Applicable Source Standard (AS)100
Confi dence Coefficient (CC)1.600
Relative Accuracv (RA)l.6l o/o
Performance Required - Applicable Source Standarc RASS%
Alternative Relative Accurrcy (RA r .61 DDM
Alternative Performance Required (d + CC)S5oom
Performance Specifi cation Mcthod PS 4A
* Delimiter for runs not used in RA calculations
Confi dence CoeIlicient, CC
cc = lto'gzs t ta;ly'n I
where,
h'ts 2306 = degrees of freedom valuen 9 = number ofruns sclected for calculating thc RA
Sd -581- = standard deviation of difference
CC -i ;00- = confidence coefficient
Relative Accuracy, RA
ld I + lcclRA =;s;;Tr:xloo
where,
d -0.01 : average difference of Reference Method and CEMSCC 1.600 = confidence coefficient
AS --T66ldd-: applicable source standard, ppmvd (q) 7 o/o OzRA l.6l :relative accuracy,o/o
46 of 135
AI FtalEE>CO Summary
Location: Clean Harbors Aragonite LLC - Aragonite, UT
Source: Incinerator System (INC)
Project No.: AST-2024-1517
Run
No.Date Time Reference Method
CO Concentretion
oomvd
CEMS - Secondary
C0 Concentration
Average
Difference
pomvdStarlEndDomvd
I
2
3
4
5
6
7
8
9
10
ll
t2
518124
518/24
5t8124
5/8/24
5/8124
5/8/24
5t8/24
5/8t24
5/8/24
5/8124
5/8/24
5t8/24
I l:28
I l:50
l2:11
l3:27
l3:48
l4:09
l4:59
l5:20
I 5:41
l6:25
l6:46
17:.O7
ll:49
2:10
.2:31
3:47
4:08
4:29
5:19
5:40
6:01
6:45
7:06
7:27
5.O7
2.30
t.o2
1.23
5.92
I .35
5.86
l .33
1.30
6.72
1.30
1.40
11.32
1.95
0.68
0.82
14.28
0.93
11.7 I
0.90
0.93
13.23
0.90
1.04
-6.25
0.3 5
0.34
0.41
0.42
0.43
0.37
0.40
0.36
Averagr l.8l 2.t6 -0.35
Standard Deviation (Sd'2.210
Confi dence Coefficient (CC 1.699
Alternative Relative Accurecv (RA 2.05 ppm
Alternative Performance Required (d + CC)<5oom
Performance Specifi cation Method PS 4A
* Delimiter for runs not used in RA calculations
Confidence Coefficient, CC
cc = lto?t x sallVn I
where,
hezs 2.306 : degrees offreedom valuen 9 : number ofruns selscted for calcutating the RA
Sd --7T0 : srandard dcviation of diffcrence
CC --176t-= confidence cocfficient
47 of 135
CO Summary
FralEeAI
Location:
Source:
Project No.:
Clean Harbors
Inc
Run
No.Date Time Reference Method
CO Concentration
ppmvd @7 o/o Oz
CEMS - Secondary
CO Concentration
oomvd (d.7 o/o Oz
Average
Difference
ppmvd @7 o/o OzStartEnd
I
2
3
4
5
6
7
8
9
l0
ll
t2
5/8t24
5/8/24
5/8t24
5t8/24
5/8t24
5/8/24
5/8/24
5/8124
5/8/24
5/8124
5/8t24
5/8/24
l:28
l:50
2:ll
3:27
3:48
4:09
4:59
5:20
5:41
6:25
6:46
7:07
l:49
2:10
2:31
3:47
4:08
4:29
5: l9
5:40
6:01
6:45
7:06
7:27
6.03
2.61
I .13
1.44
6.88
1.67
6."t3
1.64
l .53
7.70
1.62
1.85
13.30
2.tt
0.75
0.94
15.19
I .13
12.41
l.09
1.08
13.31
1.09
1.34
0.50
0.38
0.50
0.54
0.55
0.45
-5.61
0.53
0.51
Average 2.35 2.54 -0.t8
Standard Deviation (Sd)2.035
Applicable Source Standard (AS)100
Confi dcnce Coeffrcient (CC)1.564
Reladve Accuracy (RA)1.75 yo
Performance Required - Applicable Source Standarc RAS 5%
Alternative Relative Accurrcy (RA,1.75 oom
Alternative Performance Required (d + CC.55oom
Performancc Specifi cation Methoc PS 4A.
t Delimiter for runs not used in RA calculations
Confidence Coefficient, CC
"=lH,.*l
where,
h.ejs 2.306 : degrees of freedom value
n 9 = number ofruns selectcd for calcutating the RA
Sd ---t63-: standard deviation of differenceCC 1.564 = confidence coeflicient
Relative Accuracy, RA
ldl+lCClRA = 7s;;;r:x1oo
where,
d -0. I 8 : average difference of Reference Method and CEMS
CC --J6Z-= confidence coefficientAS l0-6.000- - applicable source standard, ppmvd @ 7 yo OzRA 1.75 : relative accuracy,,'/o
48 of 135
AI Fla CO Summary
Source:
Project No.: AST-2024-I 517
Run
No.Date Time Reference Method
CO Concentration
nomvd
CEMS - Backup
CO Concentration
nomvd
Averrge
Difference
oomvdStartEnd
I
2
3
4
5
6
7
8
9
l0
il
t2
5t8124
5/8/24
518124
5t8/24
5t8/24
5t8/24
s/8/24
5/8124
5/8/24
5/8/24
5/8/24
5/8/24
I l:28
I l:50
l2:11
l3:27
3:48
4:09
4:59
5:20
5:41
6:25
6:46
7:07
l:49
2:10
2:11
3:47
4:08
4:29
5:19
5:40
6:01
6:45
7:06
7:27
5.O7
2.30
t.o2
t.23
5.92
1.35
5.86
I .33
1.30
6.72
1.30
1.40
I 1.78
2.26
0.89
0.92
15.97
l.l6
12.28
l.l8
Ll3
13.20
l.l6
l.l9
0.04
0.13
0.31
0.t9
-6.42
0.r5
0.17
0. l4
0.21
Averagr L90 2.46 -0.56
Standard Deviation (Sd)2.196
Confidence Coeffrcient (CC 1.688
Alternative Relative Accumcv (RA'2.25 r:om
Alternative Performance Required (d + CC.<5ppm
Performance Specifi cation Method PS 4At Delimiter for runs not used in RA calculations
Note: Sincc abs(d) < CC. the systcm passcs tle bias tcst
Confidence Coeflicient, CC
cc = ltol'x sally'n I
where,
h.qs
n
Sd
CC
= degrees of freedom value: numbcr of ms selectcd for calculating the RA: standard deviation ofdifference
= confidencc coefficient
2.306
9
2.t%
1.688
49 of 135
CO Summary
Location: Clean Harbors Aragonite LLC - Arasonite. UT
Source: Incinerator
Project No.: AST -2024- | 5 17
Run
No.Date Time Reference Method
CO Concentration
oomvd @7 o/o O,
CEMS - Backup
CO Concentration
ppmvd @7 %o O,
Average
Difference
ppmvd @7 o/" OtStartEnd
I
2
J
4
5
6
7
8
9
l0
lt
t2
5t8124
518/24
s/8124
5/8/24
5/8/24
5/8/24
s/8/24
5/8/24
5t8124
5/8/24
5/8/24
5/8124
Il:28
I l:50
12:ll
l3:27
L 3:48
4:09
4:59
5:20
5:41
6:25
6:46
7:07
ll:49
l2:10
l2:11
l3:47
l4:08
l4:.29
L 5:19
5:40
6:01
6:45
7:06
7:27
6.03
2.6t
l.l3
t.44
6.88
t.67
6.73
1.64
1.53
7.70
1.62
1.85
12.59
2.41
0.97
1.05
16.73
1.40
12.8 r
1.43
l.3l
13.36
L40
I.s3
0.20
0.16
0.39
0.27
0.21
o.22
-5.66
0.22
0.32
Average 2.3s 2.76 -0.41
Standard Deviation (Sdl t.970
Applicable Source Standard (AS)100
Confi dence Coeflicient (CC)t.514
Relative Accuracv (RA)1.92 o/o
Performance Required - Applicable Source Standard RA<5%
Alternative Relative Accuracv (RA l 1.92 nom
Alternative Performance Required (d + CCI <5nom
Pcrformancc Specifi cation Mcthod PS 4,A
* Delimiter for run$ not used in RA calculations
Confidence Coeflicient, CC..:lH"*l
where,
h975 2.306
n9
sd---1176--cc-1ffi-
Relative Accuracy, RA
ldl+lcclRA - 'x 100AS or RM
where,
= degrees of freedom value: numbcr of runs selected for calculating the RA: standard deviation ofdifference: confidence coefficient
d -0.41 - average difference of Reference Method and CEMSCC 1.514 :confidencecoeflicienr
AS I 00.000 : applicable source standard, ppmvd, (@ 7 yo OzRA 1.92 = relative accuracy,Yo
50 of 135
THC Summary
Location: Clean Harbors Aragonite LLC - Arasonite. UT
Source: Incinerator System (INC)
Project No,: AST-2024-1517
Run
No,Date Time Reference Method
THC (as CrIL) Concentration
CEMS - Primary
THC (as C:Hr) Concentration
Average
Difference
oDml,tilStartEndDDMVWDDMVW
I
2
J
4
5
6
7
8
9
10
ll
t2
5/8/24
5/8/24
518124
5/8t24
5/8/24
5/8t24
5/8/24
5/8/24
518t24
5/8/24
5t8t24
5/8t24
l:28
l:50
2:ll
3:27
3:48
4:09
4:59
5:20
5:41
6:25
6:46
7:07
l:49
2:10
2:31
3:47
4:08
4:29
5: l9
5:40
6:01
6:45
7:06
7:27
1.30
1.04
0.78
0.57
0.59
0.1 8
0. l9
0. l8
-0.03
-0.t2
-0.t0
-0.06
0.18
0.15
0.1 8
0. l6
0.23
0. l5
0.23
0. l6
0.14
0.20
0.1 I
0. t0
0.41
0.36
0.03
-0.04
0.02
-0.17
-0.32
-0.21
-0. l6
Average 0. l6 0. l6 -0.01
Standard Deviation (Sd'0.253
Applicable Source Standard (AS 6. l3
Confidence Coefiicient (CCl 0.1 94
Relative Accuracy (RA 3.3 Yo
Performance Required - Applicable Source Standard RA< t0%
Performance Specifi cation Method PS2
t Delimiter lbr runs not used in RA calculations
Confidence Coeflicient, CC
cc = ltolu x sallVn I
where,
to.s1s 2.306 : degrees offreedom value
n 9 : number of runs selected for calculating the RASd-d'Bt-: standard deviation of differenceCC 0.194 : confidcncc coe{ficicnt
Relative Accurecy, RA
ldl+lcclRA =;s;;;r:x1oo
where,
d -0.01 : averagc differencc of Referencc Mcthod and CEMSCC 0.194 = confidcnce coelficicnt
AS ---6.tJ6-: applicable source standard, ppmr.w
RA 3.30 = relative accuracy,%o
5l ofl35
THC SummaryrEeFtaAI
Location:
Source:
Project No.:
arbors
Incinerator
AST-2024-1s17
Run
No.Date Time Reference Method
THC (as CrHr) Concentration
CEMS - Primary
THC (as CrHr) Concentration
Average
DilTerence
ppmvd @.7 Yo OzStart End oomvd @,7 o/o O,opmvd @.7 Yo Oz
I
2
J
4
5
6
7
8
9
t0
ll
t2
5/8/24
5/8/24
518124
5/8/24
5/8/24
s/8/24
518124
5/8/24
5t8t24
5/8/24
5t8t24
5/8/24
l:28
l:50
2:ll
3:27
3:48
4:09
4:59
5:20
5:41
6:25
6:46
7:07
l:49
2:10
2:31
3:47
4:08
4:29
5:19
5:40
6:01
6:45
-l:06
7:27
2.17
1.67
t.21
0.94
0.96
0.32
0.31
0.31
-0.05
-0. l4
-0. l3
-0.08
0.33
0.26
0.30
0.29
0.41
0.28
0.40
o.29
0.26
0.35
0.21
0.20
0.65
0.55
0.04
-0.09
0.02
-0.31
-0.49
-0.34
-0.28
Averast 0.27 0.30 -0.03
Standard Deviation (Sd)0.397
Applicable Source Standard (AS l0
Confi dencc Coefl icient (CCl 0.305
Relative Accuracy (RA)3.34 Vo
Performance Required - Applicable Source Standard RA< l0%
Performance Specification Method PS2
* Delimiter lor runs not used in RA calculations
Confi dence Coeflicient, CC
..=lH,'ol
where,
h.e1s 2.306 = degrees of freedom value
n 9 : number of runs selected for calculating the RA
Sd -03t-: standard deviation of differenceCC 0.305 : confidencc coefficicnt
Relstive Accuracy, RA
ldl+lcclRA = dsorRM xloo
where,
d -0.03 = average diffcrcnce of Rcfcrence Method and CEMSCC 0-305 = confidencc cocfficientAS 10.000 = applicable source standard, ppmvd@7 yoOz
RA 334-: relative accuracy,o/o
52 of 135
AT FIA THC Summary
Location: Clean Harbors
Source: Incinerator
Project No.: AST-2024-1 5 17
Run
No.Date Time Reference Method
THC (as CrHr) Concentration
CEMS - Secondary
THC (as CsHr) Concentration
Averege
Difl'erence
DDM}\ryStartEndPDmYwDDrnVW
I
2
J
4
5
6
7
8
9
l0
ll
t2
518124
518/24
5/8/24
5/8/24
s/8/24
5/8/24
5/8t24
s/8/24
5/8/24
5/8t24
5/8/24
5/8t24
I l:28
I l:50
t2:l I
l3:27
l3:48
i4:09
.4:59
5:20
5:41
6:25
6:46
7:07
ll:49
l2:10
l2:31
l3:47
t4:08
l4:29
t5: l9
5:40
6:01
6:45
7:06
7:27
l.30
1.04
0.78
0.57
0.59
0.1 8
0. l9
0.t8
-0.03
-0.t2
-0.10
-0.06
0.070
0.060
0.080
0.040
0.1 50
0.030
0.r l0
0.050
0.050
0.1 00
0.020
0.000
0.53
0.44
0.15
0.08
0.13
-0.08
-0.22
-0.t2
-0.06
Average 0. l6 0.061 0.09
Standard Deviation (Sd 0.256
Applicable Source Standard (AS 6. l3
Confidence Cocffi cient (CCl 0.1 96
Relative Accuracy (RA 4.75 yo
Performance Required - Applicable Source Standard RAs l0%
Performance Specifi cation Method PS2* Dclimitcr for runs not used in RA calculations
Confidence Coeflicient, CC
..=l#,rol
where,
h91s 2.306 : degrees of fieedom valuen 9 = number of runs selected for calculating the RASd--d'f5G-: standard deviation of difference
CC -L l %- = confidencc coefficient
Reletive Accuracy, RA
I d.l + lcclM = 7ri;ffix loo
where,
d 0.09 : average diffcrcnce of Refcrence Method and CEMS
CC -l:ir6-= confidence coefficient
AS ---6JJ6- = applicable source standard, ppmwRA 4.75 : relative accuracy,oh
53 of 135
THC SummaryFIATEE!AI
Location:
Source:
Project No.:
Clean Harbors
Incinerator
'-2024-1517
Run
No.Date Time Reference Method
THC (as CrHr) Concentration
CEMS - Secondary
THC (as C:Hr) Concentration
Average
Difference
pomvd @7 Yo OzStartEndoumvd@7 YoO,pomvd (4.7 Yo O,
I
2
3
4
5
6
7
8
9
t0
ll
t2
518124
5/8/24
518124
5/8/24
518124
5/8/24
5/8/24
5/8/24
5/8/24
518/24
5/8/24
5/8/24
l:28
l:50
2:ll
3:27
3:48
4:09
4:59
5:20
5:41
6:25
6:46
7:07
ll:49
12:10
l2:31
13:47
l4:08
4:29
5: l9
5:40
6:01
6:45
7:06
7:27
2.17
1.67
r.2t
0.94
0.96
0.32
0.31
0.31
-0.05
-0. t4
-0.13
-0.08
0.t2
0.1 I
0. l4
0.07
0.26
0.05
0.20
0.09
0. l0
0.t7
0.03
0.00
0.87
0.70
0.27
0.1 I
0.22
-0. l5
-0.31
-0. l6
-0.08
Average 0.27 0.1 I 0.16
Standard Deviation (Sd'0.402
Applicable Source Standard (AS l0
Confidence Coefticient (CCl 0.309
Relative n..o"""" {*,4.72 0h
Performance Required - Applicable Source Standard RA< l0%
Performance Soecification Method PS2
' Delimiter for runs not used in M calculations
Confidence Coefficient, CC
CC : lto'"t x sdllVn I
where,
toels 2.306 : degrees offreedom value
n 9 = number ofruns selected for calcutating the RASd-670r-: standard deviation of difference
CC --dj-6t- = confidence coefficicnt
Relative Accuracy, RA
I dl + lcclRA = 7r;ffix loo
where,
d 0.16 : averagc diffcrence of Reference Mcthod and CEMSCC 0.309 : confidcncc cocfficieltAS 10.000 : applicable source standard, ppmvd @ 7 o/o OzRA 4.72 : relative accuracy,yo
54 of 135
THC Summary
Location:
Source:
Project No.:
Clean
Incinerator
'-2024-1517
Run
No,Date Time Reference Method
THC (as CrHs) Concentration
CEMS - Beckup
THC (as C.H*) Concentrrtion
Averrge
Difference
DOml,rtrStartEndDDltrVWDDInYW
I
2
3
4
5
6
7
8
9
l0
1l
t2
5/8t24
5t8/24
518124
5/8t24
518124
5t8t24
s/8t24
5t8/24
5/8/24
5/8/24
s/8/24
5/8/24
l:28
I:50
2:ll
3:27
3:48
4:09
4:59
5:20
5:41
6:25
6:46
7:07
ll:49
12:10
l2:31
l3:47
L4:08
4:29
.5:19
5:40
6:01
6:45
7:O6
7:27
1.30
1.04
0.78
0.57
0.59
0.1 8
0. l9
0.18
-0.03
-0.t2
-0.10
-0.06
0.020
0.000
0.000
0.000
0.060
0.000
0.080
0.000
0.000
0.040
0.000
0.000
0.57
0.53
0.18
0.1 I
0. l8
-0.03
-0. l6
-0. l0
-0.06
Average 0.16 0.020 0.14
Standard Deviation (Sd'0.266
Applicable Source Standard (AS 6.13
Confi dence Coeffi cient (CC'0.20s
Relative Accuracv (RA 5.56 0
Performance Required - Applicable Source Standard RA< l0%
Performance Specification Method PS2* Delimitcr for runs not used in RA calculations
Confidence Coefficient, CC
"=lH"*l
where,
to.s:s 2.306 = degrees offreedom value
n 9 : number ofruns selected for calculating the RASd 0.266 = standard deviation ofdifferenceCC 0.205 : confidence cocfficient
Reletive Accuracy, RA
ld I + l6clRA = 7s;;;r:x 1oo
where,
d 0. l4 : average differencc of Rcfercncc Method and CEMSCC 0.205 = confidence coeflicientAS 6.130 : applicable source standard, ppm!.\ilRA 5.56 : relative accuracy,o/o
55 of 135
THC Summary
Location:
Source:
Project No.:
Clean Harbors
Run
No,Date Time Reference Method
THC (as CrHr) Concentration
CEMS - Beckup
THC (as C:Hr) Concentration
Average
Difference
ppmvd@.7 ohO,Start End opmvd @7 Yo Oz opmvd @7 %o O,
I
2
3
4
5
6
7
8
I
10
ll
t2
5/8/24
5/8124
518/24
5/8/24
5/8t24
5/8/24
5/8t24
5t8/24
5/8/24
5/8/24
5/8/24
5/8/24
t l:28
I l:50
.2:11
.3:27
3:48
4:09
4:59
5:20
5:41
6:25
6:46
7:07
ll:49
l2: l0
l2:31
l3:47
4:08
4:29
5: l9
5:40
6:01
6:45
7:06
7:27
2.t7
1.67
t.2l
0.94
0.96
0.32
0.31
0.31
-0.05
-0. l4
-0. l3
-0.08
0.040
0.000
0.000
0.000
0.110
0.000
0.1 30
0.000
0.000
0.060
0.000
0.000
0.94
0.8s
0.32
0.18
0.31
-0.05
-0.20
-0.13
-0.08
Averagr 0.27 0.033 0.24
Standard Deviation (Sd'0.41 8
Applicable Source Standard (ASl l0
Confidencc Coefficient (CC)0.321
Relative Accuracy (RA)5.59 V"
Performance Required - Appticable Source Standard RAs l0%
Performance Specifi cation Method PS2
+ Delimiter for runs not used in RA calculations
Confi dence Coefficient, CC
cc = ltogs x sdllVn I
where,
to.sts 2.306
n9
sd ---i:zlI-
CC-J'I-
Relative Accuracy, RA
ldl+lcclRA = 7s;;Tr:xloo
where,
= degrees of freedom value
= number of runs selected for calculating the RA: standard deviation ofdifference
= confidencc coc{ficicnt
d 0.24 : averagc diffcrcncs of Relercnce Method and CEMSCC 0.321 : confidence cocffrcicntAS 10.000 :applicablesourcestandard, ppmvd@1 yoO,RA 5.59 : relative accuracy,o/o
56ofl35
AI
,f
FrarEe VFR Summary
Loc8tion: Clean Harbors AEgonite LLC - Amgonire, UT
_ _Sou-rce' Inlilrqrgpr$yflem (rNC)
ProJect No.: 4!J-2024-l 5 I 7
* Delimiler Ibr runs nor uscd h RA calculanons
NoE: run time came from VFR shect
Confidence Coeflicient, CC
.. = lt"=" rollVn I
where,
\.y5 2.306 = degrees of freedom value
n 9 : number of ms selected for calculating the RASd fit234 = standmd dcviation of differcnceCC 916.82 = cotrfidence coefficient
Relatiye Accurscy, RA
ldl+lcctRA = -----:-----:---=x 100
where,
,J -3,528.22 = average difference of Reference Method and CEMSCC 916.82 : confidence coefficientRM 59,076.67 = rcferencc method, acfinRA 7.52 : relative accuacy, 04
Bias Test Results, BA
BA Required it ldl > CC
where.
d -3528.222 = avcmge differcncc ofRefercnce Mcthod and CEMSCC 916.821 = confidence coefficient
BA R"qri.cd? ---i6-
Bias Adjustment Factor, BAF
'd
f,{P=-a1cEMSavs -
where,
d -3528.222 = average difference ofReference Method and CEMSCEMS",, 62604.889 = avoage of CEMS valucs
BA-F 1.000 = bias adjutmcnt factor
Run
No.Date Time Refercnce Method
Flow Rrte
acfm
CEMS
Flow Rst€
acfm
Averagc
Difference
rcfmStartEnd
I
2
J
4
5
6
?
8
I
l0
il
t2
5t8/24
5lEt24
5/8/24
s/8/24
5/8124
5/8124
5/8/24
5/8124
5/8/24
518/24
5/8/24
518124
I l:28
I l:50
12:12
L3:2'1
l3:49
l4:10
l4:59
l5:20
l5:41
l6:25
l6:45
17:06
I l:49
l2:ll
t2:31
l3:48
l4:09
L4:30
5:19
5:40
6:01
6:44
7:05
7:26
58,763
51,792
57,094
58, I 55
59,075
58,998
57,150
58,9s9
62,822
55,t24
58.283
60.032
61,843
60,905
61,882
62,445
63,117
62,650
62,953
63,574
63,639
62,827
63,726
63.389
-3,080
-3,1 l3
-4,788
-4,290
-4,042
-3,652
-4,615
-817
-).1) I
Avemge 59,077 62,605 -3.528
Stildard Deviation (Sdl r,193
Confidence Coefficient (CC 916.82 I
Relative Accurrcv /RA 7.52 yo
Acceptability Criteria - Mean Refcrence Method s20%
Perfomnce Specifi cation Method PS6
57 of 135
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LOCATION OF TRAVERSE POINTS
Nunbcf of ltoieru poidtt oD a dicil&t
I
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rPer.enl oJ stoc* diameterliom i[\ide Mll to traverse point.
Stack Diagm
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Deplh ofDucl - 60 in.
Coss Seclio@l Area
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Upstream
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59
pllt6rre Cyclonic tr'low Check
Location Clean Harbors A
Source Incinerator
Project No. AST-2024-1517
Date 518124
Sample Point Angle (AP=0)
8
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Average
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60 of 135
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62 of 135
pulIATEE!
- i .' i'': .1
Location: Clean Harbors A
.q1.1 ,-
Runl-RMData
LLC-A
Source: Incinerator
Project No.: AST
Date: 5/8/24
Time
Unit
Status
Uncorrected Run Average (Co6.)
Cal Gas Concentration (Cya)
Pretest System Zero Response
Posttest System Zero Response
Average Zero Response (Co)
Pretest System Cal Response
Posttest System Cal Response
Average Cal Response (C6,a)
Corrected Run A
Or - Outlet COr - Outlet CO - OutletYodry %odry ppmvdValid Valid Valid
NOx - Outlet SOr - Outlet THC - Outletppmvd ppmvd ppml'rtrValid Valid Valid
109.49
250.00
0,12
0.66
0.39
244.3r
246.83
245.s7
1tl.24
9.09
10.99
0.01
-0.09
-0.04
10.95
10.80
10.88
9.09
I I.l0
0.06
0.06
0.06
10.8 I
10.91
10.86
9.28
5.02
25.00
0.09
-0.1 9
-0.05
24.96
24.92
24.94
5.0'7
0.03
0.06
0.05
9.96
10.08
10.02
0.49
10.00
0.00
0.00
0.00
10.33
10.13
10.23
NA
1.50
0.9r
0.90
0.91
0.96
0.86
0.31
0.00
0.00
0.63
1.79
2.25
2.t6
2.17
1.89
1.72
1.81
1.57
1.64
1.58
1.52
t.46
0.53
10.00
I l:28
1l:29
I l:30
1 l:31
l1:32
I l:33
I 1:34
I l:35
I l:36
I l:37
I l:38
i t:lg
I l:40
l1:41
ll:42
I 1:43
l1:44
I l:45
I l:46
1l:47
I l:48
l1:49
10.13
8.41
8.06
8.86
12.27
12.06
9.82
t0.62
10.20
9.42
8.65
9.19
8.84
8.08
8.s7
7.',?1
8.33
7.98
8.07
8.s0
8.25
7.98
8.3 l
9.65
9.91
9.50
6.57
6.78
8.51
7.92
8.24
8.85
9.49
9.12
9.28
9.89
9.51
10.02
9.58
9.88
9.83
9.51
9.70
9.95
1.04
1.0
6.28
50.00
32.15
3.06
l.35
1.1 5
l.l4
l.l0
1.04
0.95
0.93
0.92
1.08
1.60
0.94
0.95
0.94
0.97
0.98
0.96
120.76
I16.05
I I 1.59
107.s6
101.32
82.52
85.71
95.27
99.80
l13.51
123.03
124.29
I t4.72
109.82
I I 1.02
110.75
102.69
105.56
113.97
I14.79
l2 1.86
122.t5
0.28
0.37
0.44
0.18
0.26
0.50
0.s0
0.55
0.40
0.46
0.44
0.47
0.55
0.60
0.59
0.67
0.63
0.78
0.71
0.67
0.80
0.89
63 of 135
Run2-RMDataIEE}FraAI
Location: Clean Harbors
Source: Incinerator Svstem (INC
Project No.: AST -2024-1 5 17
Dttez 518124
Time
Unit
Status
0u - Outlet COr - Outlet
o/o dry Yo dry
Valid Valid
NOx - Outlet SOr - Outlet THC - Oufletppmvd ppmvd ppmvwValid Valid Valid
CO - Outlet
ppmvd
Valid
Uncorrected Run Average (Coor)
Cal Gas Concentration (Csn)
Pretest System Zero Response
Posttest System Zero Response
Average Z,ero Response (Co)
Pretest System Cal Response
Posttest System Cal Response
Average Cal Response (Cy)
Corrected Run A
8.57
10.99
0.01
-0.09
-0.04
10.95
10.80
10.88
8.67
9.57
I l.l0
0.06
0.06
0.06
10.81
10.91
r0.86
9.77
2.25
25.00
0.09
-0.19
-0.05
24.96
24.92
24.94
2.30
250.00
0.t2
0.66
0.39
244.31
246.83
245.s7
0.87
10.00
0.03
0.06
0.05
9.96
10.08
10.02
0.82
1.04
r 0.00
0.00
0.00
0.00
10.33
10.13
10.23
NA
I l:53
11:54
I l:55
I l:56
l:50
l:51
l:52
8.20
7.79
8.06
8.07
8.63
9.65
9.59
10.20
9.40
9.68
t0.22
8.69
7.92
8.09
8.23
8. l3
7.90
7.52
8. l5
7.95
7.82
9.77
10.21
9.97
10.02
9.58
8.81
8.84
8.38
8.99
8.80
8.32
9.41
10.05
9.95
9.80
9.81
9.98
10.27
9.85
9.99
l0.l I
0.96
0.93
0.93
0.96
0.98
0.97
0.94
0.93
0.91
0.92
0.92
0.97
0.96
0.99
0.96
0.95
t.12
25.24
3.66
r.05
0.99
t24.10
122.91
122.60
I18.91
121.93
122.57ll7.lt
I I 1.37
104.25
104.59
r 10.00
106.44
108.42
107.84
109.88
n7.41
I 18.68
I 17.58
I 15. l5
I t4.t4
121.76
0.89
0.77
0.80
1.06
1.27
1.22
1.3 I
1.40
1.37
1.20
0.84
0.70
0.77
0.s2
0.43
0.40
0.51
0.74
0.63
0.70
0.69
1.43
t.42
t.26
1.27
1.s2
1.49
1.29
0.86
1.38
l.3l
0.73
0.78
0.75
0.87
0.80
0.81
0.79
0.77
0.77
0.78
0.78
l:57
l:58
l:59
l2:00
l2:01
l2:02
l2:03
l2:04
l2:05
l2:06
l2:07
l2:08
l2:09
l2:10
64 of 135
pllaATEE)
Location: Clean Harbors Aragonite LLC - Arasonite. UT
Source: Incinerator Svstem (INC)
Run3-RMData
Project No.: AST-2024-t517
Date: 518124
Time
Unit
Status
Uncorrected Run Average (Co6")
Cal Gas Concentration (Cyn)
Pretest System Zero Response
Posttest System Zero Response
Average Zero Response (Co)
Pretest System Cal Response
Posttest System Cal Response
Average Cal Response (Cy)
Corrected Run A
0r - Outlet
Y, dry
Valid
10.99
0.01
-0.09
-0.04
10.95
10.80
10.88
8.3 t
COr - Outlet
Y, dry
Valid
9.70
I l.l0
0.06
0.06
0.06
10.81
10.91
10.86
9.91
CO - Outlet
ppmvd
Valid
NOx - Outlet
ppmvd
Valid
SOz - Outlet
ppmvd
Valid
THC - Outlet
ppmvw
Valid
0.97
25.00
0.09
-0.19
-0.05
24.96
24.92
24.94
1.02
0.98
l.0l
1.00
1.00
0.96
1.00
0.96
0.9s
0.96
0.96
0.98
0.99
0.99
0.97
0.98
0.96
0.94
0.91
0.94
0.97
0.97
134.30
250.00
0.12
0.66
0.39
244.31
246.83
245.57
136.54
I r5.65
1t5.44
127.98
123.t8
132.72
133.52
I 35.61
137.55
132.45
137.44
136.06
141.08
I 39.50
l3 6.84
t32.04
139,08
139.s2
142.13
137.28
l4l .l 8
t44.09
0.80
10.00
0.03
0.06
0.05
9.96
10.08
10.02
0.76
0.78
10.00
0.00
0.00
0,00
10.33
10.13
t0.23
NA
12:l I
l2:12
l2:13
l2:14
l2: l5
12:16
l2:17
l2: l8
l2:19
l2:20
l2:21
l2:22
12:23
l2:24
l2:25
12:26
12:27
l2:28
l2:29
l2:3O
l2:31
7.72
7.40
7.25
7.34
7.77
8.04
7.78
7.99
8.03
8.08
8.43
8.33
8.27
8.45
8.53
8.88
8.72
8.35
8.87
9.17
9.01
10.15
10.41
10.48
10.40
10.05
9.82
10.02
9.91
9.83
9.80
9.57
9.61
9.65
9.50
9.47
9.27
9.29
9.55
9. l8
8.87
8.97
0.82
0.83
0.73
0.68
0.66
0.91
0.87
0.91
0.66
0.49
0.78
0.67
0.83
0.82
0.71
0.60
0.44
0.66
0.79
1.23
1.76
0.78
0.72
0.68
0.74
0.93
0.79
0.79
0.79
0.77
0.76
0.77
0.84
0.77
0.73
0.75
0.76
0.76
0.76
0.80
0.80
0.82
65 of 135
Run4-RMDataAI
-i
Location:
Source:
Project No.r
Date:
Clean Harbors
Incinerator
AST-2024-15 I 7
5t8/24
Time
Unit
Status
Uncorrected Run Average (Co6")
Cal Gas Concentration (Cya)
Pretest System Zero Response
Posttest System Zero Response
Average Zero Response (Co)
Pretest System Cal Response
Posttest System Cal Response
Average Cal Response (Cy)
Corrected Run A
Oz - Outlet
Yo dry
Valid
COz - Outlet
Y, dry
Valid
CO - Outlet
ppmvd
Valid
NOx - Outlet
ppmvd
Valid
135.04
250.00
0.66
l. t0
0.88
246.83
246.34
246.59
136.5 I
SOr - Outlet
ppmvd
Valid
THC - Outlet
ppmvw
Valid
8.83
10.99
-0.09
-0.20
-0.15
10.80
10.7 I
10.76
9.05
9.35
I l.r0
0.06
0.05
0.06
10.91
10.95
10.93
9.48
1.00
2s.00
-0. l9
-0.28
-0.24
24.92
24.67
24.80
t.23
1.64
10.00
0.06
0.03
0.05
10.08
9.88
9.98
1.27
1.39
1.69
1.49
1.45
1.36
1.45
1.48
1.24
1.55
1.74
1.87
1.87
1.72
1.70
1.94
1.90
l.8l
1.87
I "84
1.91
0.57
10.00
0.00
0.02
0.01
10.13
10.01
10.07
NA
l3:27
I 3:28
l329
l3 :30
13:31
l3:32
l3:33
13:34
l3:35
l3:36
l3:37
13:3 8
I 3:39
l3:40
l3:41
l3:42
13:43
l3:44
I 3:45
l3:46
l3:47
9.28
9.21
8.81
8.54
8.48
8.24
8. l2
8.03
7.88
7.55
7.89
8.2s
8.01
8.76
9.29
9.60
10.95
10.t5
9.51
9.47
9.37
9.04
9.08
9.36
9.55
9.60
9.75
9.80
9.87
10.00
10.33
10.t0
9.74
9.99
9.41
9.06
8.82
7.79
8.32
8.86
8.88
8.94
0.81
0.80
0.80
0.82
0.83
0.90
0.93
0.93
0.89
2.76
1.09
0.94
0.94
0.90
0.90
0.88
0.88
0.90
0.97
0.98
1.05
142.28
150.07
144.63
l4 I .55
140.29
l3 9.48
132.74
132.28
137.42
l3 l .16
t24.54
122.97
135.44
139.72
135.30
136.02
134.99
129.14
l2 1.80
135.07
128.98
0.t2
0.70
I .17
1.32
t.32
1.24
1.00
0.62
0.37
0.35
0.41
0.42
0.43
-0.24
-0.30
-0.30
0.17
0.71
0.92
0.84
0.78
66 of 135
Run5-RMData
Location: Clean Harbors
Source: Incincrator System (INC
Project No.: AST-2024-l 5 I 7
Date: 5/8124
Oz - Outlet CO: - Outlet CO - OufletY'dry Y'dry ppmvdValid Valid Valid
8.72
10.99
-0.09
-0.20
-0.15
10.80
10.71
10.76
8.93
NOx - Outlet SOr - Outlet THC - Oufletppmvd ppmvd ppmvwValid Valid Validt25.47 2. I 8Uncorrected Run Average (Co6.)
Cal Gas Concentration (Cya)
Pretest System Zero Response
Posttest System Zero Response
Average Zero Response (Co)
Pretest System Cal Response
Posttest System Cal Response
Average Cal Response (Cp)
Corrected Run A
Time
Unit
Status
9.33
0.06
0.05
0.06
10.91
10.95
10.93
9.4'1
5.69
25.00
-0. l9
-0.28
-0.24
24.92
24.67
24.80
5.92
250.00
0.66
l.l0
0.88
246.83
246.34
246.s9
126.77
10.00
0.06
0.03
0.05
10.08
9.88
9.98
2.15
0.59
10.00
0.00
0.02
0.01
10. l3
10.01
10.07
NA
I 3:48
13:49
l3:50
l3:5 I
l3:52
l3 :53
l3:54
I 3:55
I 3:56
l3:57
l3:58
I 3:59
l4:00
14:01
14:02
14:03
l4:04
14:05
l4:06
l4:07
l4:08
9.25
9.34
9.26
9.17
9.04
8.75
8.89
8.88
8.82
8.t4
7.73
7.72
7.51
7.92
9.63
9.4s
8.66
8.43
8.44
8.89
9.1 I
9.02
8.94
9.03
9.09
9.t4
9.31
9.22
9.21
9.19
9.69
r 0.03
10.04
10.20
9.89
8.65
8.68
9.30
9.50
9.50
9.24
9.03
1.06
1.02
1.06
1.05
1.07
1.05
L08
1.l0
l l3
l. t8
1.17
1.20
34.88
49.65
12.90
2.23
l.6l
L39
r.32
1.22
l t8
127.08
130.07
132.06
128.31
128.59
l2s.0l
124.57
123.42
132.63
t22.64
l 15.69
I 18.87
I I 1.90
I I 1.40
l I 1.58
134.23
t20.62
125.78
130.92
139.08
140.38
1.84
1.82
1.90
1.88
2.08
2.20
2.20
2.18
2.18
2.28
2.41
2.32
2.24
2.29
2.42
2.15
2.01
2.31
2.40
2.52
2.19
0.80
0.78
0.75
0.66
0.34
0.69
0.30
0.30
2.79
0.42
0.74
0.86
0.75
0.42
0.24
0.23
0.26
0.27
0.28
0.29
0.28
67 of 135
Run6-RMData
Location: Clean Harbors
Source: Incinerator
Project No.: AST-2024-1517
Date:518124
Time
Unit
Status
Or - Outlet COr - Outlet CO - Outlet
Yo dry Y, dry ppmvdValid Valid Valid
NOx - Outlet SOr - Outlet THC - Outtetppmvd ppmvd ppmvwValid Valid Valid143.01 2.30Uncorrected Run Average (Co5.)
Cal Gas Concentration (Cya)
Pretest System Zero Response
Posttest System Zero Response
Average Zero Response (Co)
Pretest System Cal Response
Posttest System Cal Response
Average Cal Response (C1s)
Corrected Run A
9.40
r 0.99
-0.09
-0.20
-0.l5
10.80
10.7 |
t0.76
9.63
8.76
I l.l0
0.06
0.05
0.06
10.91
10.95
10.93
8.88
25.00
-0.1 9
-0.28
-0.24
24.92
24.67
24.80
1.35
1.12
1.08
1.07
1.04
1.09
Ll0
t.07
l.l0
l.l I
l.l3
t.t7
l.l9
t.t2
1.08
1.05
l.l I
1.07
l.l I
l.l9
1.32
l.l6
250.00
0.66
l.l0
0.88
246.83
246.34
246.s9
141.87
141.04
134.40
r37.21
140.09
137.41
138.56
136.46
t29.65
124.22
133.52
152.82
160.76
152.06
144.69
144.56
l5l. l l
I 50.80
t43.62
r 50.66
157.61
10.00
0.06
0.03
0.05
10.08
9.88
9.98
2.27
0. 18
10.00
0.00
0.02
0.01
10.1 3
10.01
10.07
NA
l4:09
14: l0
l4:l I
l4:12
14:13
l4:14
l4:15
l4:16
l4:17
l4:18
l4:19
14:20
l4:21
l4:22
l4:23
l4:24
l4:25
l4:26
l4:27
l4:28
l4:29
9.13
9.26
9.15
9.32
9.68
9.69
9.82
9.88
9.97
9.98
9.89
9.66
9.26
9.03
9.17
9.09
9.01
9.16
9.04
8.99
9.26
8.99
8.90
8.94
8.85
8.58
8.53
8.44
8.39
8.31
8.34
8.40
8.53
8.83
9.02
8.90
8.96
9.04
8.94
9.0s
9. l0
8.8s
1.98
2.02
2.36
2.34
2.27
2.14
2.15
2.09
2.36
2.31
2.34
2.46
2.46
2.23
2.25
2.41
2.41
2.48
2.37
2.34
2.63
0.27
0.26
0.25
0.26
0.22
0.22
0.24
0.24
-0.28
-0.50
-0.05
0.41
0.56
0.63
0.65
0.46
0.07
0.03
0.00
-0.01
-0.08
68 of 135
Run7-RMDatar"taAIlEE)
Location: Clean Harbors
Source: Incinerator
Project No.: AST-2024-l5l 7
Date: 5/8124
Time
Unit
Status
Ou - Outlet,h dry
Valid
COr - Outlet
Y, dry
Valid
9.68
I l.l0
0.05
0.09
0.07
10.95
10.99
10.97
9.78
CO - Outlet
ppmvd
Valid
NOx - Outlet
ppmvd
Valid
SOz - Outlet
ppmvd
Valid
THC - Outlet
ppmvw
Valid
0.19
r 0.00
0.02
-0.40
-0.19
10.01
9.92
9.97
NA
Uncorrected Run Average (Co6.)
Cal Gas Concentration (C,ya)
Pretest System Zero Response
Posttest System Zero Response
Average Zero Response (Co)
Pretest System Cal Response
Posttest System Cal Response
Average Cal Response (Cy)
Corrected Run A
8.s8
10.99
-0.20
-0.04
-0.12
10.71
10.8 I
10.76
8.79
5.55
25.00
-0.28
-0.33
-0.3 r
24.67
24.67
24.67
5.86
t42.29
250.00
l.l0
l.l6
I .13
246.34
246.8s
246.60
t43 -77
119.r3
t26.2t
145.12
I 5l .69
139.27
138.23
143.37
147.33
144.25
135.13
143.77
l4s.8l
137.05
118.44
1t0.26
I t 6.85
144.s5
150.81
163.59
192.62
174.61
1.02
10.00
0.03
0.35
0.19
9.88
10.06
9.97
0.8s
r.09
0.62
0.61
0.55
0.59
0.49
0.74
0.90
0.99
L02
1.04
1.02
l. t0
1.13
1.27
1.08
t.4s
t.62
1.70
1.39
l.t2
14:59
1 5:00
l5:01
I 5:02
I 5:03
l5:04
l5:05
I 5:06
l5:07
I 5:08
l5:09
15:10
15:l I
l5:12
l5:13
15:14
l5:15
15:16
15: l7
l5:18
l5:19
8.34
8.72
8.1 I
7.83
8.02
8.75
8.66
8.1 l
8.54
8.69
8.75
8.34
7.59
7.75
8.62
9.03
9.1 I
9.s3
8.98
9.30
9.39
9.73
9.46
9.91
10. l6
10.06
9.54
9.57
10.04
9.75
9.73
9.62
9.95
10.55
10.50
9.76
9.39
9.26
8.92
9.30
9.07
8.98
l.t4
1.16
1.22
l.l 8
t.t8
l.l6
Lt8
1.20
1.25
1.38
1.35
2.18
46.81
42.24
4.74
1.40
1.20
1.21
l.l 8
l.l I
l.ll
0.34
0.59
0.29
0.28
0.25
0.22
0.24
0.20
0.21
0.20
0.20
0.19
0.17
0.09
-0.04
-0.01
0.1 1
0. l3
0.21
0.18
0.00
69 of 135
AI
Location: Clean Harbors
Source: Incinerator
Project No.: AST -2024-t 517
Fra Run8-RMData
Date: 518124
Time
Unit
Status
Uncorrected Run Average (Cos.)
Cal Gas Concentration (Cra)
Pretest System Zero Response
Posttest System Zero Response
Average Zero Response (Co)
Pretest System Cal Response
Posttest System Cal Response
Average Cal Response (Cy)
Corrected Run A
Oz - Outlet COz - Outlet!"dry YodryValid Valid
NOx - Outlet SO: - Outlet THC - Outtetppmvd ppmvd ppmvwValid Valid Valid
CO - Outlet
ppmvd
Valid
l5:20
15,'21
l5:22
l5:23
l5:24
l5:25
l5:26
l5:27
I 5:28
l5:29
I 5:30
l5:31
l5:32
15:33
l5:34
l5:35
15:36
l5:37
l5:38
l5:39
l5:40
9.32
9.52
9.62
10.08
10.18
9.63
9.59
9.45
9.22
9.42
9.35
9.s3
9.40
9.46
9.20
9.14
9.r7
9.37
9.16
8.94
9_O4
9.00
8.87
8.76
8.38
8.29
8.68
8.71
8.80
8.92
8.78
8.83
8.67
8.78
8.71
8.92
9.01
9.04
8.88
9.04
9.19
9.17
L09
0.99
0.65
0.53
0.55
0.69
0.46
0.39
0.41
0.48
0.66
0.68
0.37
0.29
0.49
0.48
0.65
0.58
0.60
0.42
0.62
-0.05
0.00
0. l0
0.l8
0.2t
0.20
0.0r
-0.l3
-0.20
-0.31
0.28
0.56
0.s3
0.48
0.49
0. l4
1.12
0.35
0.01
0.00
-0.1 I
9.42
10.99
-0.20
-0.04
-0.12
10.71
t 0.81
10.76
9.64
8.83
I l.l0
0.05
0.09
0.07
10.95
10.99
10.97
8.92
t.02
25.00
-0.28
-0.33
-0.31
24.67
24.67
24.67
1.33
1.09
1.09
1.07
1.07
l.l I
r.08
l.09
1.04
0.97
0.93
0.97
0.99
L03
0.98
I .01
0.99
0.95
0.98
0.96
l.0l
1.02
250.00
1.10
l l6
l.l3
246.34
246.85
246.60
173.45
169.55
169.66
I 78.89
183.07
182.28
186.85
194.3 5
192.59
187.96
170.79
162.45
155.45
l5l.8l
162.22
164.52
t7 t .06
170.2s
l 57.1 I
145.19
173.00
17 t.07
0.58
10.00
0.03
0.35
0.19
9.88
10.06
9.97
0.t8
10.00
0.02
-0.40
-0.19
10.01
9.92
9.97
NA
70 of 135
FIATEE!',E L r-
Run9-RMDataAI
Location: Clean Harbors
Source: Incinerator S
Project No.: AST -2024-1 5 I 7
Date: 5/8/24
Time
Unit
Status
Oz - Outlet
o/o dry
Valid
COr - Outlet
%, dry
Valid
9.22
I l.l0
0.05
0.09
0.07
10.9s
10.99
r0.97
9.32
CO - Ouflet
ppmvd
Valid
NOx - Outlet
ppmvd
Valid
SOz - Outlet
ppmvd
Valid
THC - Outlet
ppmvw
ValidUncorrected Run Average (Co6")
Cal Gas Concentration (Crn)
Pretest System Zero Response
Posttest System Zero Response
Average Zero Response (Co)
Pretest System Cal Response
Posttest System Cal Response
Average Cal Response (Cp)
Corrected Run A
8.92
10.99
-0.20
-0.04
-0.12
10.71
10.8 r
10,76
9.13
0.99
25.00
-0.28
-0.33
-0.31
24.67
24.67
24.67
1.30
185.65
250.00
1.10
l.r6
l l3
246.34
246.85
246.6A
187.93
0.61
10.00
0.03
0.35
0. l9
9.88
10.06
9.97
0.43
-0.03
10.00
0.02
-0.40
-0. l9
10.01
9.92
9.97
NA
l5:41
15:42
l5:43
l5:44
l5:45
l5:46
15:47
I 5:48
l5:49
l5:50
l5:5 I
15:52
I 5:53
15:54
l5:55
l5:56
l5:57
l5:58
15:59
l6:00
l6:01
9.31
9.67
9.65
9.28
8.56
8.91
9.00
9.12
8.71
8.96
9.04
8.77
8.91
8.88
8.55
8.48
8.54
8.59
8.92
8.83
8.69
8.92
8.69
8.67
8.94
9.52
9.27
9.21
9.06
9.39
9.17
9.t I
9.35
9.25
9.26
9.50
9.51
9.47
9.43
9.22
9.30
9.36
0.94
0.95
l.0l
1.05
1.00
0.94
0.94
0.97
0.99
1.00
1.03
1.02
0.96
1.00
0.97
L0l
0.99
l.0l
1.02
r.04
1.00
169.1 I
165. l3
168.28
191.07
197.14
194.41
17 5.7 8
183.29
l8 1.65
190.00
182.05
208.82
217.51
189.57
192.|
I 8s.41
173,47
173.06
186.63
188.23
I 86.01
0.55
0.68
0.56
0.34
0.48
0.58
0.81
0.53
0.62
0.71
0.90
0.76
0.70
0.70
0.57
0.63
0.63
0.45
0.s8
0.32
0.68
-0.1 I
-0.03
-0.12
0.00
0.0s
0.06
-0.19
-0.18
-0.63
0.04
0.09
-0.17
-0.21
-0.02
0. l3
0.08
0.09
0.20
0.32
0.19
-0.18
7l of 135
AI
Locatiorl: Clean Harbors A
Source: Incinerator S
Project No.: AST -2024-1 517
FIATEE)Run 10 - RM Data
Dile:5/8/24
Time
Unit
Ststus
Oz - Outlet
%o dry
Valid
COu - Outlet
'/, dry
Valid
CO - Ouflet
ppmvd
Valid
NOx - Outlet
ppmvd
Valid
SOr - Outlet
ppmvd
Valid
THC - Outlet
ppmvw
ValidUncorrected Run Average (Coo.)
Cal Gas Concentration (Cya)
Pretest System Zero Response
Posttest System Zero Response
Average Zero Response (Co)
Pretest System Cal Response
Posttest System Cal Response
Average Cal Response (Cy)
Corrected Run A
8.61
10.99
-0.04
-0.08
-0.06
10.81
10.78
10.80
8.77
9.60
Il.t0
0.09
0.08
0.09
10.99
I l.0l
I1.00
9.68
6.38
25.00
-0.33
-0.35
-0.34
24.67
24.67
24.67
6.72
142.65
250.00
l.l6
l.t6
l.t6
246.85
246.34
246.60
t44.12
145.16
148.17
t 48.93
1M.50
l2l.98
135.75
139.34
152.00
156.01
ts5.67
165.42
162.95
153.04
149.45
145.79
146.33
147.72
142.68
122.86
103.95
t07.87
0.44
10.00
0.35
0.03
0. l9
10.06
10.1 7
10.t2
0.25
-0.12
r 0.00
-0.40
-0.26
-0.33
9.92
9.96
9.94
NA
16:25
l6,,26
l6:27
l6:28
l6:29
l6:3 0
16:3 I
l6:32
l6:33
l6:34
l6:35
16:36
l6:37
l6:38
l6:39
16:40
l6:41
l6:42
l6:43
l6:44
l6:45
8.07
8.29
7.08
8.02
8.9s
8.82
8.50
8.33
8.78
9.32
9.01
8.85
9.03
9.16
9.29
8.94
8.s2
8.01
8.04
8.43
9_30
10.06
9.89
10.83
10.08
9.34
9.44
9.67
9.79
9.41
9.02
9.26
9.38
9.24
9. l3
9.04
9.31
9.64
10.07
10.07
9.76
9.1 8
1.29
|.42
48.4t
36.1 I
3.27
1.50
l 36
1.25
1.16LlI
1.07
l.03
0.99
0.97
l.00
0.95
0.90
16,16
I 1.98
I .13
0,96
1.03
0.98
0.72
0.53
0.70
0.37
0.39
0.26
0.23
0.43
0.41
0.36
0.62
0.33
0.20
0.21
0.18
0.12
0.38
0.51
0.32
-0.t2
-0.20
-0.15
-0.08
-0.09
-0.13
-0. l3
-0.1 I
-0.08
-0.06
-0.08
-0.t2
-0.23
-0.04
-0.t I
-0.12
-0.06
-0.23
-o.21
-0. l6
-0.08
UTAH DEPARTMENT OF
ENVIRONMENTAL QUALITY
DIVISION OF A.IR QIJALITY
72 of 135
Run 11 - RM Data
Location: Clean Harbors
Source: Incinerator
LLC - Ar
Project No.: AST -2024-15 l7
Date:518124
Time
Unit
Status
Oz - Outlet
oh dry
Valid
COr - Outlet
Y" dry
Valid
9.01
I l.l0
0.09
0.08
0.09
10.99
I 1.01
1 1.00
9.08
CO - Outlet
ppmvd
Valid
0.96
25.00
-0.33
-0.35
-0.34
24.67
24.67
24.67
1.30
NOx - Outlel
ppmvd
Valid
SOz - Ouflet
ppmvd
Valid
THC - Outlet
ppmvw
Valid
-0. l0
10.00
-0.40
-0.26
-0.33
9.92
9.96
9.94
NA
Uncorrected Run Average (Coo.)
Cal Gas Concentration (Cra)
Pretest System Zero Response
Posttest System Zero Response
Average Zero Response (Co)
Pretest System Cal Response
Posttest System Cal Response
Average Cal Response (Cy)
Corrected Run A
9.55
10.99
-0.04
-0.08
-0.06
10.81
10.78
10.80
9.73
l3l .19
250.00
l.l6
l.t6
1.16
246.85
246.34
246.60
132.44
t30.2s
139.53
137.44
138.46
144.81
141.23
139.07
129.53
l28.ll
129.36
129.69
132.79
I 20.1 8
I I 1.25
tzt.48
t27.24
128.07
I 3 1.86
129.51
132.59
t32.46
0.32
10.00
0.3s
0.03
0.19
10.06
t 0.17
10.12
0. l3
l6:46
16:47
l6:48
l6:49
16:50
l6:51
l6:52
16:53
16:54
l6:55
l6:56
l6:57
16:58
16:59
l7:00
l7:01
17:02
l7:03
17:04
l7:05
17:06
9.75
9.70
9.67
9.3 I
9.53
9.93
10,25
10.15
t0.27
I0.19
9.95
8.57
8.21
8.47
8.72
8.92
9.24
9.40
9.69
10.42
10.24
8.78
8.82
8.86
9.21
9.05
8.77
8.47
8.55
8.49
8.s3
8.68
9.72
10.05
9.85
9.69
9.54
9.27
9.r8
8.90
8.34
8.44
0.93
0.91
0.90
0.92
0.92
0.92
0.86
0.86
0.87
0.90
0.92
0.94
0.95
1.00
1.06
1.07
1.06
1.06
1.03
1.04
1.04
0.41
0.58
0.25
0.42
0.58
0.39
0.23
0.39
0.22
0.2t
0. l9
0.29
0.27
0.45
0.34
0.17
0.ts
0.26
o.40
0.14
0.37
-0.08
-0.24
-0.41
-0.25
-0.04
-0.22
-0.20
-0.26
-0.29
-0.3 r
-0. l8
-0.1 1
-0.0s
-0.07
-0.07
-0.16
-0.15
-0.06
o.02
0.39
0.58
73 of 135
Run 12 - RM DataAI
-i
Location:
Source:
Project No.:
Date:
Clean Harbors A
Incinerator System (INC)
AST-2024-1517
Time
Unit
Status
Or - Outlet
'/" dry
Valid
10.19
10.99
-0.04
-0.08
-0.06
10.8 I
10.78
10.80
r 0.38
l0.l 8
9.91
9.74
9.87
10.05
10.18
9.86
10.16
10.35
10.5 t
10.s2
1 0.87
I 1.08
10.68
10.85
10.98
10.75
t0.02
9.29
9.34
8.83
COr - Outletth dry
Valid
CO - Outlet
ppmvd
Valid
NOx - Outlet
ppmvd
Valid
I 14.19
250.00
l.l6
Ll6
Ll6
246.8s
246.34
246.60
I 15.13
SOz - Outlet
ppmvd
Valid
THC - Outlet
ppmvw
Valid
Uncorrected Run Average (Co6")
Cal Gas Concentration (Cp1a)
Pretest System Zero Response
Posttest System Zero Response
Average Zero Response (Co)
Pretest System Cal Response
Posttest System Cal Response
Average Cal Response (Cy)
Corrected Run A
8.33
l l.l0
0.09
0.08
0.09
10.99
I l.0l
I 1.00
8.38
8.48
8.66
8.80
8.69
8.54
8.40
8.60
8.38
8.20
8.07
8.03
7.74
7.56
7.88
7.77
7.65
7.81
8.36
8.97
8.99
9.32
1.06
25.00
-0.33
-0.35
-0.34
24.67
24.67
24.67
1.40
1.05
L0s
l.06
1.05
1.05
1.08
1.06
1.06
1.05
I .01
0.99
1.03
I .01
l.0l
1.04
1.08
t.t2
1.17
1.20
t.l6
0.96
0.24
10.00
0.35
0.03
0. l9
10.06
l0.l 7
I 0.12
0.05
0.37
0.29
0.28
0.38
0.28
0.28
0.38
0.39
0.32
0. l5
0.07
0.07
0. l4
0.t2
0.2t
0.15
0.20
0.23
0.13
0.23
0.30
-0.06
10.00
-0.40
-0.26
-0.33
9.92
9.96
9.94
NA
17:07
17:08
17:09
l7:10
17:ll
17:12
17:13
l7:14
l7:15
l7:l 6
l7:17
17:18
17:19
17:20
l7:21
l7 22
17:23
l7:24
17:25
17,,26
17:27
127.17
124.34
125.72
127.49
124.21
122.21
I 16.82
l 17.85
I14.86
113.09
tt2_32
l 08.80
106.92
I 05.3 9
t 06.63
107.85
I 03.63
I 08.01
114.52
r05.20
104.98
0.03
-0.02
-0.02
-0.19
-0.21
-0.23
-0. l9
-0.23
-0.25
-0.21
0.95
0.53
-0.13
-0.19
-0.20
-0.20
-0.14
-0.09
-0. l4
o.02
-0.23
74 of 135
75 of 135
QA Data
Location Clean Harbors
Source Incinerator
Project No. AST-2024-15
Parameter O, - Outlet COr - Outlet CO - Outlet NOx - Outlet SOz - Outlet THC - OutletlvlIKE
Model
s/N
Operatins Ranse
Servomex
1400
14204
25
Servomex
1440
1415C-2
25
Thermo
48C
48CTL-74507-376
50
Thermo
42C.HL
42CHL-59778-324
500
Ametek
9900
9900-s I 562- I
25
Thermo
55i-2
1209052150
20Cylinder ID
Zero
Mid
Hish
NA
RR0425 r
cc749479
NA
RR0425l
cc749479
NA
E80097304
E80097304
NA
EB00 l r 606
EB00l 1606
NA
tG9l70578BAI
iG9l70578BAr
NA
EB009l r 84
EB009 I I 84Cylinder Certifed Values
Zero
Mid
Hish
NA
10.99
23.02
NA
I l.l
22.93
NA
50.39
50.39
NA
501
501
NA
s0.39
50.39
NA
29.72
29.72Cylinder Expiration Date
Zero
Mid
Hish
NA
9/19/31
1n6/3t
NA
9/19t31
U16t3l
NA
10t20/30
lo/20/30
NA
9/t6/3t
9t16/31
NA
t0/l 8/30
l0/l 8/30
NA
2/20/2s
2t20/25fvpe of Samole Line Line
76 of 135
IEE}FraAI
Calibration Datai
Locationl
Source:
Project No,:
Drte:
Clean Harbors LLC-A
Incinerator
AST-2024-1517
st8t24
Parameter Or - Outlet COr - Outlet CO - Outlet NOx - Outlet SOr - Outlet THC - Outlet
Expected Averase Concentration 10.00 10.00 10.00 250.00 5.00 10.00
Span Between
Low
High
Desired Span
10.00
50.00
23.02
10.00
50.00
22.93
10.00
50.00
50.00
250.00
t 250.00
500.00
5.00
25.00
20.00
15.00
25.00
20.00
Low Range Gas
Low
Hiph
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
5.00
7.00Mid Range Gas
Low
Hish
9.21
13.81
9.17
13.76
20.00
30.00
200.00
300.00
8.00
r 2.00
9.00
I 1.00High Range Gas
Low
Hish
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
r6.00
18.00Actual Concentration (7o or ppm)
Zero
Low
Mid
Hish
0.00
NA
t 0.99
23.02
0.00
NA
I l.l0
22.93
0.00
NA
25.00
50.00
0.00
NA
250.00
500.00
0.00
NA
10.00
20.00
0.00
6.00
10.00
17.00
ResDonse Time (seconds)30.00 30.00 30.00 60.00 60.00 60.00
Upscale Calibration Gas (C Mid Mid Mid Mid Mid Mid
Instrument Response (% or ppm)
Zero
Low
Mid
Hish
-0.06
NA
10.98
23.01
0.02
NA
10.87
22.98
-0.03
NA
25.04
49.99
0.09
NA
249.s7
491.52
0.03
NA
9.96
20.o9
0.00
6.19
10.33
17.02Performance (7o of Span or Cal. Gas Conc.)
Zero
Low
Mid
Hieh
0.26
NA
0.04
0.04
0.09
NA
1.00
o.22
0.06
NA
0.08
0.02
0.02
NA
0.09
0.50
0.t5
NA
0.20
0.45
0.00
3.05
3.l8
0.00
Zero
Low
Mid
Hieh
PASS
NA
PASS
PASS
PASS
NA
PASS
PASS
PASS
NA
PASS
PASS
PASS
NA
PASS
PASS
PASS
NA
PASS
PASS
PASS
PASS
PASS
PASS
77 of 135
FralEeAI Bias/Drift Determinations
Location:
Source:
Project No.:
Parf,meter Or - Outlet COr - Outlet CO - Outlel NOx - Outlet SOr - Outlet THC - Outlet
Run I
Pretest System Zero Response
Posttest System Zero Response
Pretest System Upscale Response
Posttest Svstem IJnscale Resnonse
0.01
-0.09
10.95
10.80
0.06
0.06
10.8 I
10.91
0.09
-0, l9
24.96
24.92
0. l2
0.66
244.3t
246.83
0.03
0.06
9.96
10.08
0.00
0.00
10.33
10. l3
Run 2
)retest System Zero Response
)osttsst Systcm Zcro Response
'retcst System Upscale Responsc
'osttest Svstem I lnscalc Resnonsc
0.01
-0.09
10.95
I 0_80
0.06
0.06
10.8 I
10.91
0.09
-0,19
24.96
24.92
0.12
0.66
244.3t
246 R1
0.03
0.06
9.96
10.08
0.00
0.00
10.33
10.13
Run 3
Pretest System Zero Response
Posttest System Zero Response
Pretest System Upscale Response
Posttest Svstem IJnscale Resnons,
0.01
-0.09
10.95
I 0.80
0.06
0.06
10.8 |
10.91
0.09
-0.19
24.96
24.92
0.12
0.66
244.31
246.83
0.03
0.06
9.96
10.08
0.00
0.00
10,33
10. l3
Run 4
Pretest System Zero Response
Posttesl Systcm Zero Response
Prctcst System Upscalc Rcsponse
Posttest Svstem Unscale Resnonse
-0.09
-0.20
10.80
10.71
0.06
0.05
I 0.91
I0.9s
-0.19
-0,28
24.92
24.67
0.66
l.l0
246.83
246.34
0.06
0.03
10.08
9.88
0.00
0.02
I 0.13
10.01Run 5
Pretest System Zero Response
Posttest System Zero Response
Pretcst System Upscale Responsc
Posttest Svstcm Upscale Resoonse
-0.09
-0.20
I 0.80
I 0.71
0.05
0.05
10.91
10.95
-0. l9
-0.28
24.92
24.67
0.66
t.l0
246.83
246.34
0.06
0.03
10.08
9.88
0.00
0.02
10.13
10.01Run 5
)retest System Zero Response
)osttest System Zero Response
'retest Systcm Upscale Responsc
)osttest Svstcm UDscalc Rcsnonse
-0.09
-0.20
I 0.80
10.71
0.06
0.0s
10.91
I0.95
-0. l9
-0.28
24.92
24.67
0.66
l.l0
246.83
246.34
0.06
0.03
10.08
9.88
0.00
0.02
I0. l3
I0_01Run 7
Pretest System Zero Response
Posttest System Zero Response
Pretest System Upscale Response
Posttest Svqlcm I Inscalc Recnnnc.
-0.20
-0.04
10.7 I
10.8t
0.05
0.09
t 0.95
10.99
-0.28
-0.33
24.67
24.67
l.l0
l.l6
246.34
246.85
0.01
0.35
9.88
t0 06
0.02
-0.40
10.0 t
9.92
Run 8
Pretest System Zero Response
Posttest System Zero Response
Pretest System Upscale Response
Posttest Svstem Unscale Resnonse
-0.20
-0.04
10.71
10.81
0.05
0.09
10.95
t0 99
-0.28
-0.33
24.67
24.67
l.l0
l.l6
246.34
246 85
0.03
0.3 5
9.88
10.06
0.02
4.40
10.01
992Run 9
Pretcst System Zcro Responsc
Posttest System Zero Response
Pretest System Upscale Response
Posttest System Upscale Resoonse
-0.20
-0.04
10.71
10.81
0.05
0.09
10.9s
10.99
-0.28
-0.33
24.67
24.67
l. t0
l.l6
246.34
246.8s
0.03
0.35
9.88
10.06
0.02
-0.40
10.01
9.92Run l0
Pretest System Zero Rcsponse
Posttest System Zero Response
Pretest System Upscale Response
Posttest Svstem Uoscale Resoonse
-0.04
-0.08
10.81
l0 78
0.09
0.08
10.99
I l.0l
-0.33
-0.35
24,6'7
24.67
l. t6
I .16
246.8s
246.34
0.35
0.03
t0.06
lo.l7
-0,40
-0.26
9.92
9.96Run ll
Prctest Systcm Zero Rcsponse
Posttcst Systcm Zcro Rcsponsc
Pretest System Upscale Response
Posttest Svstem Uoscale Resnonse
-0.04
-0.08
10.8 I
I 0.78
0.09
0.08
10.99
I l.0l
-0.33
-0.3s
24.61
24.67
I .16
I .16
246.85
246.34
0.35
0.03
r0.06
10.17
-0.40
4.26
9.92
9.96Run I
Pretest System Zero Response
Posttest System Zcro Responsc
Prctcst System Upscale Rcsponsc
Posttest Svstem IJnscale Resnonse
-0.04
-0.08
t0.8I
| 0.78
0.09
0.08
10.99
I l.0l
-0.33
-0.35
24.67
24.67
l.l6
t.t6
246.85
246.34
0.35
0.03
10.06
10.t7
-0.40
-0.26
9.92
9.96
78 of 135
Bias/Drift Determinations
FralEeAI
Location:
Sourcel
Project No.:
Clean Harbors
Incinerator System (INC)
AST-2024-1517
Parameter Or - Outlel COz - Outlel CO - Outlet NOx - Outlet SOr - Outlet THC - Outlet
Run I Date 518124
Span Valuc
Initial ]nstrument Zeto Cal Response
Initial Instrument Upscale Cal Response
Pretest System Zero Response
Posttest System Zero Rcsponse
Pretest System Upscale Response
Posttest Svstem Uoscale Resnonse
23.02
-0.06
t 0.98
0.01
-0.09
10.9s
l 0.80
22.93
0.02
10.87
0.06
0.06
10.81
I0.91
50.00
-0.03
25.04
0.09
-0. l9
24.96
24.92
500.00
0.09
249.s7
0. l2
0.66
244.3t
246.83
20.00
0.03
9.96
0.03
0.06
9.96
10.08
20.00
0.00
r0.33
0.00
0.00
10.33
10.t3
Bias (%)
Pretest Zero
Posttest Zero
Pretest Span
Posttest SDan
0.30
-0. l3
-0.13
-0.78
0.17
0.17
-0.26
0.17
0.24
-0.32
-0.16
-0.24
0.01
0.1 I
-1.05
-0.55
0.00
0.t5
0.00
0.60
NA
NA
NA
NADrift (%)
Zero
Mid
-0.43
-0.65
0.00
o.44
-0.56
-0.08
0.1 I
0.50
0. l5
0.60
0.00
-1.00Run 2 Dste 518124
Span Value
Instrument Zero Cal Response
lnstrument Upscale Cal Response
Pretest System Zero Response
Posttest System Zero Response
Pretest System Upscale Response
Posttest Svstem Uoscale Resnonse
23.02
-0.06
10.98
0.01
-0.09
r0.95
I 0.80
22.93
0.02
I 0.87
0.06
0.06
10.81
10.91
50.00
-0.03
25.04
0.09
-0.19
24.96
24.92
500.00
0.09
249.57
0.12
0.66
244.3t
246.83
20.00
0.03
9.96
0.03
0.06
9.96
t 0.08
20.00
0.00
10.33
0.00
0.00
10.33
10. l3
Bias (%)
Pretest Zero
Posttest Zero
Pretest Span
Posttest S6an
0.30
-0.1 3
-0. l3
-0.78
0. l7
0.17
-0.26
0.17
0.24
-0.32
-0. l6
-0.24
0.01
0.1 I
- 1.05
-0.5s
0.00
0.15
0.00
0.60
NA
NA
NA
NADrift (%)
Zero
Mid
4.43
-0.65
0.00
0.44
-0.56
-0.08
0.tI
0.50
0. l5
0.60
0.00
-1.00
Run 3 Date 518124
Span Value
Instrument Zero Cal Response
Instrument Upscale Cal Rcsponse
Pretest System Zero Response
Posttest System Zero Response
Pretest System Upscale Response
Posttcst Svstem Uoscalc Resoonsc
23.02
-0.06
10.98
0.01
-0.09
10.95
10.80
22.93
0.02
10.87
0.06
0.06
10.8 I
10.91
50,00
-0.03
25.04
0.09
-0.t9
24.96
24.92
500.00
0.09
249.57
0. l2
0.66
244.31
246.83
20.00
0.03
9.96
0.03
0.06
9.96
10.08
20.00
0.00
10.33
0.00
0.00
10.33
t0. l3
Bias (%)
Pretest Zero
Posttest Zero
Pretest Span
Posttest Snan
0.30
-0. l3
-0. l3
-0.78
0.t7
0.17
-0.26
0.t7
0.24
-0.32
-0. l6
-0.24
0.01
0.tI
- 1.05
-0.55
0.00
0.15
0.00
0.60
NA
NA
NA
NADrift (%)
Zero
Mid
4.43
-0.65
0.00
0.44
-0.56
-0.08
0.1 I
0.50
0. l5
0.60
0.00
-1.00
79 of 135
FTA
t\
AI lEe Bias/Drift Determinations
Location: Clean Harbors
Source: Incinerator
Project No,: AST-2024-l5l
Paremeter Or - Outlet COr - Outlet CO - Outlet NOx - Outlel SOr - Outlel THC - OutletRun 4 Date 5nn4
Span Valuc
Instrument Zero Cal Response
lnstrument Upscale Cal Response
Pretest System Zero Response
Posttest System Zero Rcsponsc
Pretest System Upscale Response
Posttest System UDscale Resoonse
23.02
-0.06
10.98
-0.09
-0.20
10.80
10.71
22.93
0.02
10.87
0.06
0.05
10,91
10.95
50.00
-0.03
25.04
-0. l9
-0.28
24.92
24.67
500.00
0.09
249.57
0.66
l.l0
246.83
246.34
20.00
0.03
9.96
0.06
0.03
10.08
9.88
20.00
0.00
10.33
0.00
0.02
10. l3
r0.0tBias (%)
Pretcst Zero
Posttest Zero
Pretest Span
Posttest Snan
0. l3
0.61
0.78
l.t7
0.1'1
0. l3
0.17
0.35
0.32
0.50
0.24
0.74
0.1 I
0.20
0.55
0.65
0.ls
0.00
0.60
o.40
NA
NA
NA
NALrnfi (70
Zero
Mid
-0.48
4.39
-0.04
0.t7
-0, l8
-0.50
0.09
-0. l0
-0.15
-1.00
0. l0
-0.60Run 5 Date SlAl24
Span Value
Instrument Zero Cal Response
Instrument Upscale Cal Response
Pretest Systcm Zero Response
Posttest System Zero Response
Pretest System Upscale Response
Posttest Svstem Unscale Resnonse
23.02
-0.06
10.98
-0.09
-0.20
10.80
10.71
22.93
0.02
l 0.87
0.06
0.05
10.91
10.95
50.00
-0.03
25.04
-0. l9
-0.28
24.92
24.67
500.00
0.09
249.57
0.66
1.10
246.83
246.34
20.00
0.03
9.96
0.06
0.03
10.08
9.88
20.00
0.00
10.33
0.00
0.02
10.13
10.0 lBias (%)
Pretest Zero
Posttest Zero
Pretest Span
Posttest Soan
0. l3
0.61
0.78
r. l7
0.17
0. l3
0.17
0.3s
0.32
0.50
0.24
0.74
0.1 I
0.20
0.55
0.65
0. l5
0.00
0.60
0.40
NA
NA
NA
NA
Zero -0.48
-0.39
-0.04
o.t7
-0. l8
-0.50
0.09
-0.10
-0.r5
- 1.00
0. t0
-0.60Run 6 Date 518124
Span Value
Instrument Zero Cal Response
Instrumcnt Upscale Cal Response
Pretest System Zero Response
Posttest System Zero Response
Pretest System Upscale Response
Posttest Svstem Unscale Resnonse
23.02
-0.06
I0.98
-0.09
-0.20
1 0.80
10.71
22.93
0.02
10.87
0.06
0.0s
10.91
t0.95
50.00
-0.03
25.04
-0. l9
-0.28
24.92
24.67
500.00
0.09
249.57
0.66
l.l0
246.83
246.34
20.00
0.03
9.96
0.06
0.03
10.08
9.88
20.00
0.00
I 0.33
0.00
0.02
10. l3
10.01Bias (%)
Pretest Zero
Posttest Zero
Pretest Span
Posttest Span
0. l3
0.61
0.78
t.t7
0.1'1
0. l3
0.t7
0.35
0.32
0.50
0.24
0.74
0.1 I
0.20
0.5s
0.65
0.r5
0.00
0.60
0.40
NA
NA
NA
NADnft (%)
Zero
Mid
-0.48
-0.39
-0.04
0.t7
-0.18
-0.50
0.09
-0.10
-0.15
-1.00
0. l0
-0.60
80 of 135
FTAAI Bias/Drift Determinations
Location: Clean Harbors
Source: lncinerator
Proiect No.: AST-2024-| 5 17
Prrameter O, - Outlel COr - Outlet CO - Outlet NOx - Outlel SO, - Outlel THC - OutletRun 7 Date Sl8l24
Span Valuc
lnstrument Zero Cal Response
Instrument Upscale Cal Response
Pretest System Zero Response
Posttcst System Zcro Responsc
Pretest System Upscale Response
Posttest System Upscale Resoonse
23.02
-0.06
10.98
-0.20
-0.04
10.7 I
10.81
22.93
0.02
10.87
0.05
0.09
10.9s
r0.99
50.00
-0.03
25.04
-0.28
-0.33
24.67
24.67
500.00
0.09
249.s7
t.l0
l.l6
246.34
246.85
20.00
0.03
9.96
0.03
0.35
9.88
r 0.06
20.00
0.00
10.33
0.02
-0.40
10.01
9.92Bias (%)
Pretest Zero
Posttest Zero
Pretest Span
Posttest Sban
0.61
0.09
t.t7
0.74
0. l3
0.31
0.35
0.52
0.s0
0.60
0.74
0.74
0.20
0.21
0.65
0.54
0.00
1.60
0.40
0.50
NA
NA
NA
NADrift (%)
Zero
Mid
0.70
0.43
0.17
0.17
-0. l0
0.00
0.01
0. l0
1.60
0.90
-2.t0
-0.45
Run E Date 5lEl24
Span Value
Instrument Zero Cal Response
Instrument Upscale Cal Response
Pretest System Zcro Response
Posttest System Zero Response
Pretest System Upscale Response
Posttest Svstem Unscale Resnonse
23.02
-0.06
10.98
-0.20
-0.04
lo.7t
10.81
22.93
0.02
10.87
0.05
0.09
10.95
10.99
50.00
-0.03
25.04
-0.28
-0.33
24.67
24.67
500.00
0.09
249.57
l. t0
1.16
246.34
246.8s
20.00
0.03
9.96
0.03
0.35
9.88
10.06
20.00
0.00
10.33
0.02
-0.40
10.01
9.92Bias (%)
Prelest Zero
Posttest Zero
Pretest Span
Posttest SDan
0.61
0.09
t.t7
0.74
0. l3
0.3 I
0.35
0.s2
0.50
0.60
0.74
0.74
0.20
o.2t
0.65
0.54
0.00
1.60
0.40
0.s0
NA
NA
NA
NADrift (%)
Zeto
Mid
0.70
o.47
0.17
0.17
-0.1 0
0.00
0.01
0. l0
1.60
0.90
-2.10
-0.45
Run 9 Date 518124
Span Value
Instrument Zero Cal Response
Instrument Upscale Cal Response
Pretest System Zero Response
Posttest System Zero Response
Pretest System Upscale Response
Posttest Svstem Uoscalc Resnonse
23.O2
-0.06
10.98
-0.20
-0.04
10.71
10.81
22.93
0.02
10.87
0.0s
0.09
I 0.95
10.99
50.00
-0.03
25.04
-0.28
-0.33
24.67
24.67
500.00
0.09
249.57
l.l0
I .16
246.34
246.85
20.00
0.03
9.96
0.03
0.35
9.88
t0.06
20.00
0.00
10.33
0.02
-0.40
10.01
9.92
Bias (%)
Prelest Zero
Posttest Zero
Pretest Span
Posttest Snan
0.61
0.09
t.t7
0.74
0. l3
0.3 l
0.3s
0.52
0.50
0.60
0.74
0.74
0.20
0.2t
0.6s
0.54
0.00
L60
0.40
0.50
NA
NA
NA
NADrift (%)
Zero
Mid
0.70
0.43
0.17
0.17
-0.10
0.00
0.0 r
0. l0
1.60
0.90
-2.10
-0.45
8l of 135
Bias/Drift Determinations
Location:
Source:
Project No.:
Clean Harbors ite LLC - A
Ilcinerator
AST-2024-t5t7
Parameter Oz - Outlet COr - Outlet CO - Outlet NOx - Outlet SOr - Outlet THC - Outlet
Span Valuc
lnstrument Zero Cal Response
Instrument Upscale Cal Response
Pretest System Zero Response
Posttest System Zero Rcsponsc
Pretest System Upscale Response
Posttest System Uoscale Resoonse
23.02
-0.06
10.98
-0.04
-0.08
10.81
l 0.78
22.93
0.02
10.87
0.09
0.08
10.99
I l.0l
50.00
-0.03
25.04
-0.33
-0.35
24.67
24.67
500.00
0.09
249.57
l.l6
l.l6
246.85
246.34
20.00
0.03
9.96
0.35
0.03
10.06
10.17
20.00
0.00
10.33
-0.40
-0.26
9.92
9.96Bias (%)
Prctest Zero
Posttest Zero
Pretest Span
Posttest Sban
0.09
0.09
0.74
0.87
0.31
0.26
0.s2
0.61
0.60
0.64
0.74
o.74
0.21
0.2t
0.54
0.65
1.60
0.00
0.50
1.05
NA
NA
NA
NA
Zeto
Mid
4.17
-0. l3
-0.04
0.09
-0.04
0.00
0.00
-0.10
-1.60
0.55
0.70
0.20
Span Value
hstrument Zero Cal Response
Instrument Upscale Cal Response
Pretcst System Zcro Rcsponsc
Posttest System Zero Response
Pretest System Upscale Response
Posttest Svstem Unscale Resnonse
23.02
-0.06
10.98
-0.04
-0.08
10.81
10.78
22.93
0.02
10.87
0.09
0.08
10.99
I r.0l
50.00
-0.03
25.04
-0.33
-0.35
24.67
24.67
500.00
0.09
249.5't
t. t6
l.l6
246.85
246.34
20.00
0.03
9.96
0.35
0.03
r0.06
10.t7
20.00
0.00
10.33
-0.40
-0.26
9.92
9.96Bias (%)
Pretest Zero
Posttest Zero
Pretest Span
Posttest SDan
0.09
0.09
0.74
0_87
0.31
0.26
0.s2
0.61
0.60
0.64
0.74
0.74
0.21
0.21
0.54
0.6s
1.60
0.00
0.50
1.05
NA
NA
NA
NA\'/o )
Zero
Mid
-0. l7
-0. l3
-0.04
0.09
-0.04
0.00
0.00
-0. t0
-t.60
0.55
0.70
0.zoRun 12 Date 5nD4
Span Value
lnstrument Zero Cal Response
Instrumcnt Upscale Cal Response
Pretest System Zero Response
Posttest System Zero Response
Pretest System Upscale Response
Posttcst System Upscale Resoonse
23.02
-0.06
10.98
-0.04
-0.08
10.81
10.78
22.93
o.o2
10.87
0.09
0.08
10.99
I 1.01
50.00
-0.03
25.04
-0.33
-0.35
24.67
24.67
500.00
0.09
249.57
r.l6
I .16
246.85
246.34
20.00
0.03
9.96
0.35
0.03
10.06
10.1 7
20.00
0.00
r 0.33
-0.40
-0.26
9.92
9.96Bias (%)
Pretest Zero
Posttest Zero
Prctcsl Span
Posttest Span
0.09
0.09
0.74
0.87
0.31
0.26
0.52
0.61
0.60
0.64
0.74
0.74
0.2t
0.2r
0.54
0.65
1.60
0.00
0.50
l.0s
NA
NA
NA
NADrift (o/o)
Zero
Mid
-0.17
-0.13
-0.04
0.09
-0.04
0.00
0.00
-0. l0
-1.60
0.55
0.70
0.20
82 of 135
&*"J!f,**
Accroditation #62754
Red Ball Technical Gas Service
555 Craig Kennedy Way
Shreveport, LA 71,107
800.5514150
PGVP Vendor lO # c12023
EPA PROTOCOL GAS CERTIFICATE OF ANALYSIS
Cylinder Number:
Product lD Number:
Cylinder Pressure:
coA#
Customer PO. NO.:
Customsr:
)c749479
25312
t900 PStGrctMMoro
Certification Date:
Expiration Date:
MFG Facility:
Lot Number:
Tracking Number:
)1t18t2023
)1t16t2031IEErevepor-iI
cc749419.20230't03
1 03899767
Previous Certification Dates:
Conc.ntmdon Uncrrttmy Anrtytcel prlnclpte
cc738486.20211012
E40097897.20210/.12
1 16298002s 12t2312022017146467 01t17t2023
SMART.CERT
This is to certify the gases referenced have been calibrated/tested, and verified to meet the delined speciflcations. Thiscalibration/test was performed using Gases or Scales that are traceable through National lnstitute of Standards andTechnology (NIST) to the lnternational System of Units (Sl). The basis of compliance stated is a comparison of themeasurement parameters to the specified or required calibration/testing process. The expanded uncertainties use a coveragefactor of k=2 to approximate the 95% confidence level of the measurement, unless otheruise noted. This calibration certificateapplies only to the item described and shall not be reproduced other than in full, without written approval from Red BallTechnical Gas Services. lf not included, the uncertainty of calibrations are available upon request and were taken into accountwhen determlning pass or fail.
Jasmine Godfrey
Analytical Chemist
AssayLaboratory: Red Ball TGS
Version 02-J, Revised on 2018-0$1 7
83 of 135
-..*l.yij12-ffi &*iilf,*
Accreditation #62754
Red Ball Technical Gas Service
555 Craig Kennedy Way
Shreveport, LA 71{07
800.551€.t s0
PGVP Vendor lD # c12023
EPA PROTOCOL GAS CERTIFICATE OF ANALYSIS
Cylinder Number:
Product lD Number:
Cylinder Pressure:
coA#
Customer PO. NO.:
Customer:
RR04251
125371
r900 PS|G
KU4Zf,I.ZUZJUUJI-U
Certification Date:
Expiration Date:
MFG Facility:
Lot Number:
Tracking Number:
Previous C€rtification Dates:
)9t21t2023
l9/19/2031
- Snreveoon - LA
(KU4ZC t.ZUZJUdJI
IO/549/1 E
s calibration standard has been certified per the May 2012 EPA Traceability Protocol, Document EPA-600/R-12531,
1.
I
Certifi ed Concentration(s)
SMART.CERT
Conc.r*reilonW
10.99 %
Unc.ri.lnty Analy{cal Pdndplc
FTIR
MPA
A!..y.d et
Dloxide r0.11%
*0.03 %
o9n1PO23
0p,|18t2023
Belance
Analytical Measurement Data Available Online.
Analytical !nstrumentation
02
co2 FTIR
Thermo
MKS
410i
MKS 2O31OJG2EKVS13T
1 162980025 0911U2023017146467 09t21t2023
This is to certify the gases referenced have been calibrated/tested, and verified to meet the defined specilications. This
calibration/test was performed using Gases or Scales that are traceable through National lnstitute of Standards and
Technology (NIST) to the lnternational System of Units (Sl). The basis of compliance stated is a comparison of the
measurement parameters lo the specifled or required calibration/testing process. The expanded uncertainties use a coverage
factor of k=2 to approximate the 95% confidence level of the measurement, unless otheMise noted. This calibration certificate
applies only to the item described and shall not be reproduced other than in full, without written approval from Red Ball
Technical Gas Seruices. lf not included, lhe uncedainty of calibrations are available upon request and were taken into account
when determining pass or fail.
" ,, -.
Jasmine Godfrey
Analytical Chemist
Assay Laboratory: Red Ball TGS
Ve6ion 02-J. Revised on 2018-09-17
84ofl35
Airgas.
an Air Liquide company
Airgas Specialty Gases
Airgas USA LLC
5e5 North Industrial toop Road
Tooele, UT 84o74
Airgre.com
Part Number:
Cylinder Number:
Laboratory:
PGVP Number:
Gas Code:
Reference Number:
Cylinder Volume:
Cylinder Pressure:
Valve Outlet:
Certification Date:
153-402560601-1
144.0 CF
2015 PStc
660
Oct20,2022
ation Date: Oct
Certification performed in accordance with "EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May ZOtZ),'OocumEntEFi600/R-12/531 ' using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analyticaluncertainty as stated below with a confidsnce level of 95%. There are no signiflcant impurities which affect th6 uie of this calibration mixture. All concentrations ire on amole/mole basis unless otherwise noted. The results relate only to the itemsiested. The report shall not be reproduced except in full without approval of the laboratory. Do
Siqnature on file
CERTIFICATE OF ANALYSIS
Grade of Product: EPA PROTOCOL STANDARI)
E03Nt99E15A01D0
E80097304
124 -Tooele (SAP) - UT
872022
CO,NO,NOX,BALN
Not Use This below 100 psiq. i.e. 0.7
ANALYTICAL RESULTSActual Protocol Total Relative
Concentration Method Uncertainty
Component Requested
Goncentration Assay
Dates
NOX
CARBON MONOXIDE
NITRIC OXIDE
NITROGEN
50.00 PPM
50.00 PPM
50.00 PPM
Balance
+l- 1.4o/o NIST Traceable
+l- 0.8o/o NIST Traceable
+l- 1.4% NIST Traceable
1 0 I 1 0 I 2022, 1 0 I 20 I 2022
10t10t2022
1 0 I 1 0 12022, I 0 I 20 I 2022
49.91 PPM
50.39 PPM
49.85 PPM
G1
G1
G1
CALIBRATION STANDARDSType Lot !D Cylinder No Concentration Uncertainty Expiration Date
Aug 31,2024
Feb 20,202O
Sep 21,2O25
Feb O2,2022
Sep 24,2025
Feb 01,2023
Apr 30,2024
CC5OO959 5.074 PPM NITROGEN DIOXIDE/NITROGEN 2.1%
EBO13OO55 4.81 PPM NITROGEN DIOXIDE/NITROGEN 2.Oo/oTheSRM,NTRM'PRM,o'RG@totheGMlSusedintheassayandnotpartoftheanalysis.
NTRM 120'11221PRM 12386NTRM 210607-24
PRM 12395
NTRM 21060713GMIS 401648675102
GMIS 1534002020104
KALOO4127 49.24PPMCARBONMONOXIDE/NITROGEN O.6YOD685025 9.91 PPM NITROGEN DIOXIDE/AIRCC7O8O8O 48.41 PPM NITRIC OXIDE/NITROGEND887660 9.91 PPM NITROGEN DIOXIDE/AIR
CC7O8O49 48.41 PPM NITRIC OXIDE/NITROGEN
2.Oo/o
1.2%
2.0%
1.2%
lnstrumenUMake/Model
ANALYTICAL EQIIIPMENT
Analytical Principle Last Multipoint Galibration
Nicolet iS50 AUP21 '10269 CO LCO
Nicolet iS50 AUP2110269 NO LNO
Nicolet iS50 AUP211O269 NO2 impurity
FTIR
FTIR
FTIR NO2 impurity
Oct 05,2022
Oct'13,2022
Ocl 12,2022
Triad Data Available Upon Request
Approved for Release
85 of 135
Page 'l of 1
Red Ball Technical Gas Service
555 Craig Kennedy Way
Shreveport, LA 71107
800-551{150
PGVP Vendor lD # G12023
EPA PROTOCOL GAS CERTIFICATE OF ANALYSIS
Cylinder Number:
Product lD Number:
Cylinder Pressure:
coA#
Customer PO. NO.:
Customer:
:tJUo1 1 606
24235
t900 PStG
:8001 1 606.20230906-0
Certification Date:
Expiration Date:
MFG Facility:
Lot Number:
Tracking Number:
)g1ata)23
)9/16/2031
- Shreveport - LA
-8001 1606.20230906
)25274E39
SMART-CERT
This is to certify the gases referenced have been calibrated/tested, and verified to meet the defined specifications. Thiscalibration/test was performed using Gases or Scales that are traceable through Nalional lnstitute of Standards andTechnology (NIST) to the lnternational System of Units (Sl). The basis of compliance stated is a comparison of themeasurement parameters to the specified or required calibration/testing process. The expanded uncertainties use a coveragefactor of k=2 to approximate the 95% confidence level of the measuremenl, unless otherwise noted. This calibration certificateapplies only to the item described and shall not be reproduced other than in full, without wriflen approval from Red BallTechnical Gas Servlces. lf not included, the uncertainty of calibrations are available upon request and were taken into accountwhen determlning pass or fail.
,h,r/r, W*At-
Aaron Varelas
Analltical Chemist
Assay Laboratory: Red Ball TGS
Version 02-J, Revased on 2018-09-17
Previous Csdification Dates:
Conc.nbatlon Uncrrtalnty &ralyd6l pdndpL AmryrdOn
501 PPM *3 PPM Chemiluminescence
41-M-50
E80059947.202301 17
sx32691.20230'r'1 7
1152610017 08t29t2023
86 of 135
Airgas
an Air Liquide company
Airgas Specialty Gases
Airgas USA LLC
S25 North Industrial hop Road
Tooele, UT 84o74
Airgas.com
Part Number:
CylinderNumber: SGg170578BAL
Reference Number:
Cylinder Volume:
Cylinder Pressure:
Valve Outlet:
Certification Date:
1 53-402560600-1
144.0 CF
2015 PS|G
660
Oct 18,2022
Laboratory:
PGVP Number:
Gas Code:
Expiration Date: Oct 18, 2030
Certification performed in accordance with "EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)" document EPA
600/R-12/531, using the assay procedures listed. Analytical Methodology does not require coffection for analytical interference. This cylinder has a total analytical
uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixturo. All concentrations are on amole/mole basis unless otherwise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval ofthe laboratory. Do
Triad Data Available Upon Request
Sionature on file
CERTIFICATE OF ANALYSIS
Grade of Product: EPA PROTOCOL STANDARI)
E02N199E15A0350
124 - Tooele (SAP)- UT
872022
S02,BALN
Not Use This below 100 psiq, i.e. 0-7
Component Requested
Concentration
ANALYTICAL RESULTS
Actual Protocol Total Relative Assay
DatesConcentrationMethod Uncertaingr
SULFUR DIOXIDE 50.00 PPM 50.39 PPM Gl +l- 0.9o/o NIST Traceable 10t1112022, 10t18t2022NITROGEN Balance
CALIBRATION STANDARDSType Lot lD Cylinder No Concentration Uncertaintyr Expiration Date
NTRM 16010207 KALOO3179 97.69 PPM SULFUR DIOXIDE/NITROGEN 0.8%Nov 01, 2027
InstrumenUMake/Model
ANALYTICAL EQIIIPMENT
Analytical Principle Last Multipoint Galibration
Nicolet iS50 AUP2110269 SO2 LSO2 Oct 12,2022FTIR
Approved for Release
87 of 135
Page 1 of I
Airgas"
an Air Liquide company
Airgas Specialt5r Gases
Airgas USA LLC
525 North Industrial Loop Road
Tooele, UT 84o74
Airgas.com
Part Number:
Cylinder Number:
Laboratory:
PGVP Number:
Gas Code:
Reference Number:
Cylinder Volume:
Cylinder Pressure:
Valve Outlet:
Certification Date:
153-124604653-1
144.4 CF
2015 PS|G
350
Feb 20,2017
Feb
Cerlification performed in accordance with 'EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards lUaV ZOf ZI Oocr"'o't epa600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This c/i;der has a total analyticaluncertainty as stated below with a confidence level of g5%. There are no significant impuritios which affect the uae of this celibration mixture. All concentrations ire on amole/mole basis unless otherwise noted. The results relate only to the items tested. The report shall not be reproduced exoept in full without approval of lhe laboratory. Do
Sionature on file
CERTIFICATE OF ANALYSIS
Grade of Product: EPA PROTOCOL STANDARI)
E02Nr99E15A0930
E80091 184
124 -Tooele (SAP)- UT
872017
PPN,BALN
Not Use This below 100 psio. i.e. 0.7
Component Requested
Concentration
ANALYTICAL RESULTS
Actual ProtocolConcentration Method
Total Relative
Uncertainty
Assay
DatesPROPANE 3O.OO PPM 29.72PPMNITROGEN Balance
G1 +l- 0.6% NIST Traceable 0212012017
Type
CALIBRATION STANDARDS
Lot lD cylinder No concentration uncertainty Expiration Date
NTRM/C3H8 08061008 CC262362 49.62 ppM PROPANE/A|R +t- o.3oL May 14,2018
lnstrumenUMake/Model
ANALYTICAL EQI.IIPMENT
Analytical Principle Last Multipoint Calibration
Nicolet 6700 AMP09001 19 C3H8 LC3H8 FTIR Feb 02.2017
Triad Data Available Upon Request
Approved for Release
88 of 135
Page I of 1
plll6rrrcEr
' .l i.r'L
Location: Clean Harbors_A14gg!4gll-C - Aragonite, UT
NOx Converter Efficiency Check
Project No.: AST-2024-1517
NO2 Converter Check - Outlet
Analyzer Make Thermo3"Tll'ffHX"', ;mCytinderlDNumber @CylinderExp.Date @
Cyfinder Concentration, ppm T
Pre-Test Date 518124 Time 7:20
Pre-Test ConcentETiilppm 46A
Pre-Test Efficiencv, 7o %
Post-Test Date 5/8124 Time 17:53
Post-Test CorceniEEi-, ppm W
Post-Test Efficiencv, 7o 9l
ired Efliciencv is > 90 96.
89 of 135
&*PJ**, *
Accreditation #62754
Red Ball Technical Gas Service
555 Craig Kennedy Way
Shreveport, LA 71107
800-551{150
PGVP Vendor lD I G12O24
EPA PROTOCOL GAS CERTIFICATE OF ANALYSIS
Cylinder Number:
Product lD Number:
Cylinder Preasure:
coA#
Customer PO. NO.:
Customer:
ccllot26
124t31
1800 PS|G
)c770726.20240212-0
Certification Datc:
Expiration Dat6:
MFG Facility:
Lot Number:
Tracking Number:
)4t23t2024
)4t23t2027
- Shrevepon - LA
-ut lut26.2tJ240212
r oEE93184
SMART-CERT
This is to certify the gases referenced have been calibrated/tested, and verified to meet the defined specifications. Thiscalibration/test was performed using Gases or Scales that are traceable through Nalional lnstitute of Standards andTechnology (NIST) to the lnternational System of Units (Sl). The basis of compliance stated is a companson of themeasurement parameters to the specifled or required calibration/testing process. The expanded uncertainties use a coveragefactor of k=2 to approximate the g5% confidence level of the measurement, unless otherwise noted. This calibration certificateapplies only to the item described and shall not be reproduced other than in full, without written approval from Red BallTechnical Gas Seruices. lf not included, the uncertainty of calibrations are available upon request and were taken into accountwhen determining pass or fall.
,/arrdrt W*e4-
Aaron Varelas
Analytical Chemlst
Assay Laboratory: Red Ball TGS
Version 02-J, Revised on 2018-09-17
Previous Csrtification Datas:
Certafi ed Concentration(s)
Gonccrdradonffi Urc.rt Inty
i0ffim An lytcd Pdnclplo A.my.d On
Dloxide FTIR ou 1 6 t2024, U I 1 612024, 04 I 2A 2A24
Balance
Analytical Measurement Oata lvi
E80055436.20201 021
EB0080844.20201020
E80097551.20201 021
c2190301.02
c21 90301.02
c2190301.02
MKS 2O31DJG2EKVSl3T
MKS 2O31GPPP1A5ZK1XX
90 of 135
F EPA Method 205
lalaE}g Fietd Calibration of Dilution System
,tiont
Dme: InlilrgBlor iyst_en (INC)
AI
Locrtion:
Source:
Projcct No.:
Date
Uethod Criteria EPA
Parametel o)
Makr
Mode
s/N
Soar
Deruomcx
1400
14204
250
3vlinder Number lD
Zeto
Mid
Hloh
8ts0089907
cc4587R8
lylinder Certified Vslues
Zero
Midgioh
u.u
10.99
23 97
Instrument Resoonre (7o or oon
Zeto
Mid
[Iioh
10.9
24.O
Crlibrrtion Ges Selection (9/o of SDrn)
Mid
IIioh 95.9
Crlibmtion Error Performanc€7o of Soan)
Zero
Mid
Hioh
v.t
-0.3
0.0
Linerity (70 of R8nse)
.o.6
Alalyzer Make:
Analyzer Model:
Analyzer SN:
Environics ID:
ComponenL/Balancc Gas:
Cylinder Gas tD (Dilution):
Cylinder Gas Concenration (Dilution), %:
Cylinder Gas ID (Mid-lrvel):
Cylinder Gas Concentration (Mid-Lcvel), %:
Analyzer
Concentration
to/^\
lnjection 1
Error
I *2 y.\
Injection 2
Error
I +2./"\
Injection 3
Error(+2%l
t9.22 0.tv")Yo 4.1%
I 1.99 tJ. I"/n lYo 0.0%
4.81 tJ.2'/o .o.2yo
2.43 0.sro 50/6 |.lYo
Mid-L€vel Supply Gas Calibration Direct to A
Calibrstion
Gas
Concentrrtion
lo/^\
ruecnon I
Analy4r
Conc€ntretion
lo/^\
Injection 2
Anslyzer
Concentratlon
Injection 3
Atrrlyzer
Conc€ntratiotr(o/^r
Average
Amlyrer
Cotrcentration
to/^\
Differcncc
Average
Error
( *2./ol
t0.99 I 1.0 tt)t.0 il.0 t 0.o2 o.20k
91 of 135
,:AlElrce
SOURCE AESTING
Mass Flow Controller Calibration
Note: Themassflowcontroller'scalibrationvaluesareusedbythedilutionsystem'soperatingsoftwaretoimproveaccuracy. Thesecalibrationsarenotnecessarily indicative of the systems overall performance. Performance is verified by conducting a Method 205 prior to each field use.
Calibration Performed By Ryan Lyons
Dilution System Make:
Dilution System Model:
Dilution System S/Ni
Calibration Equipment Make:
Calibration Equipment Modet:
Calibration Equipment S/N:
Flow Cell S/N:
Flow Cell S/N:
Calibration Gas:
Barometric Pressure, mmHt:
Ambient Temperature,'F:
4040
8025
Scientific
-10sLPD/sMM-D/sM, M-15LPM-D/st
797206
797206
t97208
Nitrogen
25.s
7
Mass Flow Controller lD
size, ccm:
Make:
Model:
s/N:
#L
10,000
Environics
4040
455242077
#2
10,000
Environics
4040
455242012
fl3
1,000
Environics
4040
455238005
Set Flow True Flow Difference
cclmin cc/min
Set Flow True Flow Difference
cc/min cc/min
Set Flow True Flow Difference
cclmin cc/min
5%
LOlo
20%
30%
40%
50%
60%
70%
SOYo
90%
too%
500 502 0.4%
1,000 L,077 7.7%
2,000 2,os7 2.9%
3,000 3,083 2.8%
4,000 4,106 2.7%
5,000 5,L22 2.4%
6,000 6,748 2.5%
7,000 7,764 23%
8,000 8,t82 2.3%
9,000 9,198 2.2%
10,000 70,227 2.2%
500 502 0.4%
1,000 1,012 7.2%
2,OOO 2,040 2.0%
3,000 3,0s9 2.o%
4,000 4,078 2.0%
5,000 5,095 L.9%
6,000 6,1L4 t.9%
7,000 7,L34 L.9%
8,000 8,152 7s%
9,000 9,773 1.9%
10,000 10,195 2.O%
50 49 2.4%
100 99 7.5%
200 r99 0.7%
300 299 0.2%
400 400 0.I%
500 502 0.5%
600 504 0.6Yo
700 706 0.9%
800 810 L.3%
900 916 7.8%o
1,000 7,024 2.4%
Dare 4/27/23
92 of 135
Airga$
an Air Liquide company
Airgas Specialty Gases
Airgas USA LI,C
525 North Industrial Loop Road
Tooele, UT 84o74
Airgas.com
CERTIFICATE OFANALYSrc
Grade of Product: EPA PROTOCOL STANDARD
Part Number:
Cylinder Number
Laboratory:
PGVP Number:
Gas Code:
E03N152E15A38Q7
cc458788
124 - Tooele (SAP) - UT
872023
C02,02,BALN
Reference Number:
Cylinder Volume:
Cylinder Pressure:
Valve Outlet:
Certification Date:
Feb 13. 2031
1 53-402661 01 0-1
164.0 CF
2015 PStc
296
Feb 13,2023
Cerlification performed in a@ordanc€ witir 'eea fraceaOif ity ftotoool fo, A";
.ff;]?31]:.51r^,!j:XI1*^:1T,,:l-T:*..lff, fgooologvaSs 19t,eoui'e coreaionLianaryricar interrerence. rhis oyrinder has a totat anatyricatuncettainty as stated below with a conlldence l€vel of g5o/o. Thore are no silnifcant impu;tiss which *r"a tir. ,G oi tiri" *irur":u-"i i-n i,l,i. il ;;;;;;;'ilf,;^ "mole/mol€ basis unless olheMlse noted- The rosults relate only to the itemsiested. Tne report snai not be raproduc€d except tn fuit without approvat ot th6 laboratory. DoUSe IhrS below 100 psiE, i.e.0.7
Component Requested
Concentration
ANALYTICAL RESULTS
Actual - - ProtocolConcentration Method
Total Relative
Uncertainty Assay
Dates
CARBON DIOXIDE
OXYGEN
NITROGEN
24.OO o/n
24.00 0a
Balance
23.62 yo
23.97 0/o
G2
G2
+l- 0.8o/o NIST Traceeble
+l- 0.5% NIST Traceable
02t13t2023
02n3na23
CALIBRATION STANDARDSType Lot lD Cylinder No Concentration Uncertainty Expiration Date
NTRM
NTRM
1 3060802
09061434
cc41 5397
cc282492
24.04 O/O CARBON OIOXIDUNITROGEN
22.53 o/n OXYGEN/NITROGEN
0.60/o
0.4%
Dec 1 1, 2025
May 1 3. 2025
lnstrumenUMake/Model
-
ANALYTICAI EQUIPMENT
Analytical Principle Last Multipoint Calibration
Horiba MA-510 SV4MEUTJ CO2
Horiba MPA-510 VV603MM58 02
CO2 NDIR (Dixon)
02 P?ramagnetic (Mason)
Feb 09, 2023
Feb 09, 2023
Triad Data Available Upon Request
93 of 135
Page I of 1
&*PJlf*
Accreditation #62754
Red Ball Technical Gas Service
555 Craig Kennedy Way
Shreveport, LA 71107
800-551{150
PGVP Vendor lD # c12023
EPA PROTOCOL GAS CERTIFICATE OF ANALYSIS
Cylinder Number:
Product lD Number:
Cylinder Pressure:
coA#
Customer PO. NO.:
Customer:
:80O89907
1253t1
1900 PStG
E80089907.202301 04-0
Certification Oate:
Expiration Date:
MFG Facility:
Lot Number:
Tracking Number:
)'v11t2023
J1tog12031
:SEreveport -IA---
:B0089907.20230,t 04
952894',t6
Previous Certification Dates:
Concsntrdon Uncertalnty Anely{lc.l prlnclple
cc722672.202104't 2
cc738496.20211012
E80089841.20't9101 7
EB0097A97.20210412
11.94 0/.
19.98 %
12.O3 %
19.46 %
1162980025 12t23t2022
1 162980025 12t14t2022
SMART.CERT
This is to certify the gases referenced have been calibrated/tested, and verified to meet the defined specitications. Thiscalibration/test was performed using Gases or Scales that are traceable through National lnstitute of Standards andTechnology (NIST) to the lnternational System of Units (Sl). The basis of compliance stated is a comparison of themeasurement parameters to the specified or required calibration/testing process. The expanded uncertainties use a coveragefaclor of k=2 to approximate the 95% confidence level of the measurement, unless otherwise noted. This calibration certificateapplies only to lhe item described and shall not be reproduced other than in full, without written approval from Red BallTechnical Gas Services. lf not included, the uncertainty of calibrations are available upon request and were taken into accountwhen determining pass or fail.
--7 a
(
LYI:,]1
Timothy Davis
Analytical Chemist
Assay Laboratory: Red Ball TGS
Version 02-J, Revised on 2O1B-09-1 7
94 of 135
trlarEeAI QA Data
Location Clean Harbors
Source Incinerator
Project No. AST-2024-1517
LLC-
Parameter(s): VFR
Date Pitot ID Evidence of
damase?
Evidence of
mis-alisnment?
Calibration or
Repair required?5t8t24 P-867 no no no
Date Probe or
Thermocouple ID
Reference
Temp. (oF)
Indicated
Temp. (oF)Difference Criterie
5/8/24 P-867 141.0 l4 1.0 0.0%+ 1.5 yo
Date 05108t24
Balance ID:SCALE 22
Test Weieht ID:SLC-I KG-I
Certifieid Weisht (s):1000.0
Measured Weight (e):999.7
Weight Dilference (e):0.3
Date Barometric
Pressure
Evidence of
damase?
Reading
Verified
Calibration or
Repair reouired?Weather Station Location
5t8/24 Weather Station NA NA NA Salt Lake City UT
Date Meter Box ID Positive Pressure Leak Check
s/8124 M5-27 Pass
95 of 135
DGN,1 Calibration-Orifices
Document ll:624.044
Revisior 23.0
Effective Dat€1/25/23
issuinq Department Tech Seryices Paqr 1of1
Console lD: M5-21
Meter S/N: 20035543
Critical Orifice S/N. 1330
Calibration Detail
lnitial Barometric Pressure, n. Hg (pb)
Final Barometric Pressure, in. Hg (pbr)
Averaqe Barometric Pressure, in. Ho /ph)
25.07
25.07
25.01
lrLlcdt ulltce tu (y)
K' Factor, ftr R1/2 / in. wc.min (K)
Vacuum Pressure, in. Hg U,
lnitial DGM Volume, ftr (Vm)
Final DGM Volume, ftr (Vm,)
Total DGN,I Volume, ft3 (Vm)
1330-31
4.8429
13.0
541.924
512781
10 857
1330-31 i330-25
0.6728
15.0
s28.098
536.765
8.667
1330-25 1330-19
0.5186
17.0
548.287
5 55.093
6.806
1330-19
0.8429 0.673 0.519
130
512.781
523.688
14.907
15.0
536.76s
545.420
8.65 5
17.0
555 093
561.889
6.796Ambient Temperature, "F (Ia)
lnitial DGM Temperature, "F (Tm)
Final DGM Temperature, 'F (Tm-)
Average DGM Temperature, 'F ( Tm)
64
63
63
63
64
63
64
64
63
64
65
65
63
65
64
65
63
64
64
64
63
64
65
65Elapsed Time (O)
Meter Orifice Pressure, in. WC (AH)
Standard Meter volume, fti (Vmstd)
Standard Critical Orifice Volume, ftr (Vcr)
Meter Correction Factor (y)
Tolerance
Orifice Calibrat on Value (AH @)
Tole.ance
Orrfice Cal Cneck
10 00
3.20
9 2724
9 2341
0.996
0.001
1.803
0.051
10.00
3.24
9.3058
9.2341
0.992
0 003
1.80'l
0.052
10.00
2.10
7 3570
1.3777
1.003
0.008
1.842
0.011
10.00
2.10
7.3468
7.3777
1.004
0.009
1.842
0 011
10 00
1.30
s.7693
5.6868
0 986
0.009
1.917
0.063
10 00
1.30
5 7553
5 6868
0.988
0 007
1.915
0.062
094 168 1.66
\4eter Corrertlon Fad6r rn
frifice Calibration Value ( H @)
0.995
)ositive Pressure Leak Check Yes
Reference Calibrator Make: OMEGA
Reference Calibrator Model: CL23A
Reference Calibrator S/N: T-]97207
Calibration Detail
Reference Temp Display Temp Accuracv Difference
uF oR oR oF
0
68
100
4bu
528
560
2
69
102
462
529
562
-0.4
-0.2
-0.4
2
1
2
223
248
273
683
708
133
225
250
274
68s
710
734
-0
0
-0
2
2
1
300
400
500
600
7AA
800
900
1,000
1,100
1,200
760
860
960
1,060
1,160
1,260
1,360
1,460
1,560
1,660
301
401
501
600
700
800
900
999
1,100
1,199
761
861
961
1,060
1,160
1,260
1,360
1,459
1,560
1,659
-0.1
-0 1
-0 1
00
0.0
00
0.0
0.1
0.0
0.1
1
i
1
0
0
0
0
,1
0
1
Personnel
Stacey Cunningham
96 of 135
Calibration By
Calibration Date
Rev ewed By:
RYAN LYONS
2/2/2024
FTAIEE!AI
1..,i
Location:
Source:
Project No.:
Clean Harbors
Incinerator
AST-2024-1517
Datez 51812024
Traverse Point Time o2
(o/"\
CO,
(o/"\
CO
(ppm)
NOx
(nnm)
Soz
(oom)
A-l
2
J
B-1
2
J
ll:17
1 1:19
l1:21
ll:23
l1:25
ll:27
9.73
8.60
8.06
9.04
9.84
10.85
9.4
8.69
9.62
9.90
9.22
8.55
7.73
9.0
1.04
1.03
t.02
0.98
0.97
0.98
1.0
238.96
131.57
118.79
118.92
131.72
126.35
144.4
0.49
0.06
0.25
0.22
0.r7
0.34
0.3Average
Criteria Met I Z Polnt l2 Point Srngle Point l2 Point slngle Polnt
97 of 135
98 of 135
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13
5
-uIT5r-PARTMENT oF
ENVIRoNMENIA!-qqaLI
JUN 20 2024
DIVISION OF AIR OUALTTY
135 of 135
Clean Harbors Primary CEM THC RATA RM 25A (Tested 5-8-2024)
Reference Methods 25 A & B
Compromised
Source Information
Company Name Clean Harbors CEMS #1 Incinerator Stack
Company Contact:Willian Simmons
Contact Phone No.435-844-8351
Point Source:Clean Harbors CEMS #1
Test & Review Dates
Test Date:5/8/2024 Tabs Are Shown
Review Date: 10/1/2024
Observer:Not Observed
Reviewer:Rob Leishman
Emission Limits Emission Rates
VOC VOC
mg/L gas
10.0
lbs./hr.
%O2 Correction as a whole #7.00
Test Information
Stack I.D. inches
As ft^2 Y Dl H @ Cp Pbar Pq (static)
Ps
Stack Pressure
60.0 19.6 0
Contractor Information
Contact:
Contracting Company:
Address:
Phone No.: Btu/hr Selected
Project No.:

Division of Air Quality
Instrumental Reference Methods - Gaseous Measurements
Round
ppm
Method 19 - F factors for Coal, Oil, and Gas
Fd Fw Fc
dscf/MMBtu wscf/MMBtu scf/MMBtu
Diluent
F factor used
O2
CO2
Anthracite 2
Bituminous 2
Lignite
Natural
Propane
Butane
10100
COAL
OIL
GAS
9780
9860
9190
8710
8710
8710
10540
10640
11950
320
10610
10200
10390
1970
1800
1910
1420
1040
1190
1250
Wet CEM
Correct For O2 Yes
Yes
Clean Harbors Primary CEM THC RATA RM 25A (Tested 5-8-2024)
D$I$v$I$s$I$on of A$I$r Qual$I$ty
NSPS Relat$I$ve Accuracy Performance Spec$I$f$I$cat$I$on Test - CEMS Cert$I$f$I$cat$I$on
Clean Harbors CEMS #1 Incinerator Stack
Clean Harbors CEMS #1
VOC/THC Analyzer:Thermo 5Li-TH Serial No.:THC - 1434964304
O2 Analyzer:Serial No.:
Acquisition System:Serial No.:
Acquisition System: Serial No.:
Equivalent Emission Limit:10 I & J
Test Date VOC Dry VOC Test Date % O2 Dry
5/8/2024 ppm lbs/hr 9/30/2014 RM CEMS Diff
Run#Start
Time
End
Time RM CEMS Diff RM CEMS Diff Run#
Start
Time End Time %c %c
1 11:28 11:49 1.30 0.18 1 11:28 11:49 10.0
2 11:50 12:11 1.04 0.15 2 11:50 12:11 8.7
3 12:11 12:32 0.78 0.18 3 12:11 12:32 8.4
4 13:27 13:48 Y 0.57 0.13 0.44 4 13:27 13:48 9.0
5 13:48 14:09 Y 0.59 0.23 0.36 5 13:48 14:09 9.0
6 14:09 14:30 Y 0.18 0.15 0.03 6 14:09 14:30 9.7
7 14:59 15:20 Y 0.19 0.23 -0.04 7 14:59 15:20 8.8
8 15:20 15:41 Y 0.18 0.16 0.02 8 15:20 15:41 9.6
9 15:41 16:02 Y 0.00 0.14 -0.14 9 15:41 16:02 9.1
10 16:25 16:46 Y 0.00 0.2 -0.20 10 16:25 16:46 8.8
11 16:46 17:07 Y 0.00 0.1 -0.11 11 16:46 17:07 9.7
12 17:07 17:28 Y 0.000 0.1 -0.10 12 17:07 17:28 10.4
13 13
14 14
15 15
16 16
Average = 0.2 0.16 0.03 Average =
Sd Standard Deviation = 0.22 Sd Standard Deviation = Sd Standard Deviation =
Confidence Coefficient = 0.17 Confidence Coefficient = Confidence Coefficient =
RA - Relative Accuracy =105.70%RA RA - Relative Accuracy =
n = 9 0 n = 0 or RA of 1%
t0.975 = 2.306 t0.975 =
E.L. Relative Accuracy = 2.01%
a For steam generators;b Average of three samples;
c Make sure that RM and M data are on a consistent basis either wet or dry.
40 CFR 60 Performance Specification 2 For SO2 and NOx Continuous Emission Monitoring Systems
13.2 Relative accuracy Performance Specification. The RA of the CEMSS must be not greater than 20 percent when RM is used in the denominator of Eq. 2-6
(average emissions during test are greater than 50 percent of the emission standard)or 10 percent when the applicable emission standard is used in the
denominator of Eq. 2-6 (average emissions during test are less than 50 percent of the emission standard).
Up dated January 17, 2006
40 CFR 60 Performance Specification 3 For O2 and CO2 Continuous Emission Monitoring Systems
13.2 CEMS Relative Accuracy Perfromance Specification.
The RA of the CEMS must be no grater than 20 percent of the mean value of the reference method (RM) data. 1 percent O2 or CO2.
The results are also acceptable if the absolute value of the difference between the mean RM value and the mean CEMS value is less than or equal to 1.0 percent O2 (or CO2).
Up dated September 14, 2016
40 CFR 60 Performance Specification 6 For Continuous Emission Rate Monitoring Systems (CERMS)
13.2 CERMS Relative Accuracy. The RA of the CERMS shall be no greater than 20 percent of the mean value of the RM's test data in terms of the nits of the emission
standard, or 10 percent of the applicable standard, which err is greater.
Up dated January 17, 2006
Ac
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Passed
State of Utah CalError Page 5
VOC K3
(Propane)O2
Span Value 20.00 Span Value 23.02
Units ppm Units %
Cylinder No.
Expiration
Date Cylinder Value: Response Difference CAL. ERROR Status Cylinder No.
Expiration
Date
Cylinder
Value:Response Difference CAL. ERROR Status
Zero Gas 0.00 0.00 0.00 0.00%Passed Cal.Zero Gas 0.00 -0.06 0.06 0.26%Passed Cal.
Low-level Cal. Gas 6.00 6.19 0.19 0.95%Passed Cal.Mid-level Cal. Gas 10.99 10.98 0.01 0.04%Passed Cal.
Mid-level Cal. Gas 10.00 10.33 0.33 1.65%Passed Cal.High-level Cal. Gas 23.02 23.01 0.01 0.04%Passed Cal.
High-level Cal. Gas 17.00 17.02 0.02 0.10%Passed Cal.
<0.25% of span value Zero Gas 0.00%
<0.10% of span value Zero Gas 0.00%40 to 60% of span value Low-level Cal. Gas 47.7%
25 to 35% of span value Low-level Cal. Gas 30.00%80 to 100% of span value Mid-level Cal. Gas 100.00%
45 to 55% of span value Mid-level Cal. Gas 50.00%
80 to 90% of span value High-level Cal. Gas 85.00%
VOC K4
(Butane)CO2
Span Value Span Value 22.93
Units ppm Units %
Cylinder No.
Expiration
Date Cylinder Value: Response Difference CAL. ERROR Status Cylinder No.
Expiration
Date
Cylinder
Value:Response Difference CAL. ERROR Status
Zero Gas Zero Gas 0.000 0.020 0.02 0.09%Passed Cal.
Low-level Cal. Gas Mid-level Cal. Gas 11.100 10.870 0.23 1.00%Passed Cal.
Mid-level Cal. Gas High-level Cal. Gas 22.930 22.980 0.05 0.22% Passed Cal.
High-level Cal. Gas
<0.25% of span value Zero Gas 0.00%
<0.10% of span value Zero Gas 40 to 60% of span value Low-level Cal. Gas 48.4%
25 to 35% of span value Low-level Cal. Gas 80 to 100% of span value Mid-level Cal. Gas 100.00%
45 to 55% of span value Mid-level Cal. Gas
80 to 90% of span value High-level Cal. Gas
0.00
VOC K2 (Ethane)
0.00
Span Value 0.00
Units ppm
Cylinder No.
Expiration
Date Cylinder Value: Response Difference CAL. ERROR Status
Zero Gas
Low-level Cal. Gas
Mid-level Cal. Gas
High-level Cal. Gas
<0.10% of span value Zero Gas
25 to 35% of span value Low-level Cal. Gas
45 to 55% of span value Mid-level Cal. Gas
80 to 90% of span value High-level Cal. Gas
Page 5
Clean Harbors Primary CEM THC RATA RM 25A (Tested 5-8-2024)
Division of Air Quality
NSPS Relative Accuracy Performance Specification Test - CEMS Certification
Clean Harbors CEMS #1 Incinerator Stack
Clean Harbors CEMS #1
Average Emission
Dry
VOC
(Propane)
VOC
(Butane)
VOC
(Ethane)Average % concentration
lbs./hr.CO2 O2
ppm 0.40 8.61 9.25
Run 1
Dry
VOC
(Propane)
VOC
(Butane)
VOC
(Ethane)
Molecular Weight 44.1 58.1 30.1
Qs dscf min CO2 O2
ppm 1.30 10.11 10.00
lbs/hr #VALUE! 9.90 9.90
Run 2
Dry
VOC
(Propane)
VOC
(Butane)
VOC
(Ethane)
Molecular Weight 44.1 58.1 30.1
Qs dscf min CO2 O2
ppm 1.04 9.73 8.73
lbs/hr #VALUE!9.57 8.57
Run 3
Dry
VOC
(Propane)
VOC
(Butane)
VOC
(Ethane)
Molecular Weight 44.1 58.1 30.1
Qs dscf min CO2 O2
ppm 0.78 0.66 8.36
lbs/hr #VALUE!0.70 8.21
Run 4
Dry
VOC
(Propane)
VOC
(Butane)
VOC
(Ethane)
Molecular Weight 44.1 58.1 30.1
Qs dscf min CO2 O2
ppm 0.57 9.49 9.04
lbs/hr #VALUE!9.35 8.83
Run 5
Dry
VOC
(Propane)
VOC
(Butane)
VOC
(Ethane)
Molecular Weight 44.1 58.1 30.1
Qs dscf min CO2 O2
ppm 0.59 9.45 8.97
lbs/hr #VALUE!9.33 8.72
Run 6
Dry
VOC
(Propane)
VOC
(Butane)
VOC
(Ethane)
Molecular Weight 44.1 58.1 30.1
Qs dscf min CO2 O2
ppm 0.18 8.87 9.66
lbs/hr #VALUE!8.76 9.40
Corrected Value
Raw Value
mg/Liter of gasoline
Corrected Value
Corrected Value
Raw Value
Corrected Value
Raw Value
Corrected Value
Raw Value
Raw Value
Corrected Value
Raw Value
Wet CEM
Yes
Correct For O2 Yes
Clean Harbors Primary CEM THC RATA RM 25A (Tested 5-8-2024)
Division of Air Quality
NSPS Relative Accuracy Performance Specification Test - CEMS Certification
Clean Harbors CEMS #1 Incinerator Stack
Clean Harbors CEMS #1
Wet CEM
Yes
Correct For O2 Yes
Run 7
Dry
VOC
(Propane)
VOC
(Butane)
VOC
(Ethane)
Molecular Weight 44.1 58.1 30.1
Qs dscf min CO2 O2
ppm 0.19 9.79 8.78
lbs/hr #VALUE!9.68 8.58
Run 8
Dry
VOC
(Propane)
VOC
(Butane)
VOC
(Ethane)
Molecular Weight 44.1 58.1 30.1
Qs dscf min CO2 O2
ppm 0.18 8.90 9.57
lbs/hr #VALUE!8.83 9.42
Run 9
Dry
VOC
(Propane)
VOC
(Butane)
VOC
(Ethane)
Molecular Weight 44.1 58.1 30.1
Qs dscf min CO2 O2
ppm 0.00 9.30 9.07
lbs/hr #VALUE!9.22 8.92
Run 10
Dry
VOC
(Propane)
VOC
(Butane)
VOC
(Ethane)
Molecular Weight 44.1 58.1 30.1
Qs dscf min CO2 O2
ppm 0.00 9.68 8.77
lbs/hr #VALUE!9.60 8.61
Run 11
Dry
VOC
(Propane)
VOC
(Butane)
VOC
(Ethane)
Molecular Weight 44.1 58.1 30.1
Qs dscf min CO2 O2
ppm 0.00 9.07 9.74
lbs/hr #VALUE!9.01 9.55
Run 12
Dry
VOC
(Propane)
VOC
(Butane)
VOC
(Ethane)
Molecular Weight 44.1 58.1 30.1
Qs dscf min CO2 O2
ppm 0.00 8.38 10.39
lbs/hr #VALUE!8.33 10.19
Run 13
Dry
VOC
(Propane)
VOC
(Butane)
VOC
(Ethane)
Molecular Weight 44.1 58.1 30.1
Qs dscf min CO2 O2
ppm
lbs/hr
Corrected Value
Corrected Value
Corrected Value
Raw Value
Corrected Value
Raw Value
Corrected Value
Raw Value
Corrected Value
Raw Value
Raw Value
Corrected Value
Raw Value
Raw Value
Clean Harbors Primary CEM THC RATA RM 25A (Tested 5-8-2024)
Division of Air Quality
NSPS Relative Accuracy Performance Specification Test - CEMS Certification
Clean Harbors CEMS #1 Incinerator Stack
Clean Harbors CEMS #1
Wet CEM
Yes
Correct For O2 Yes
Run 14
Dry
VOC
(Propane)
VOC
(Butane)
VOC
(Ethane)
Molecular Weight 44.1 58.1 30.1
Qs dscf min CO2 O2
ppm
lbs/hr
Run 15
Dry
VOC
(Propane)
VOC
(Butane)
VOC
(Ethane)
Molecular Weight 44.1 58.1 30.1
Qs dscf min CO2 O2
ppm
lbs/hr
Run 16
Dry
VOC
(Propane)
VOC
(Butane)
VOC
(Ethane)
Molecular Weight 44.1 58.1 30.1
Qs dscf min CO2 O2
ppm
lbs/hr
Corrected Value
Raw Value
Corrected Value
Raw Value
Corrected Value
Raw Value
Clean Harbors Primary CEM RATA RM 1, 2, 3A, 6C, 7E, 10, & 19 (Tested 5-8-2024)
Reference Methods 2, 3A, 6C, 7E, 10, & 19
Source Information
Company Name Clean Harbor cems-#2b
Company Contact:Tyler Lee
Contact Phone No.435-884-8122
Stack Designation:Main Stack
Test & Review Dates
Test Date:5/8/2024
Review Date: 9/27/2024
Observer:Not Observed
Reviewer:Rob Leishman
Emission Limits Emission Rates
SO2 NOX CO SO2 NOX CO
lbs./MMBtu
lbs./hr. 44.2 30.446
ppm 91.0 100.00 0.854 2.933
%O2 Correction as a whole #7.00 7.00
Test Information
Stack I.D. inches
As ft^2 Y Dl H @ Cp Pbar Pq (static)
Ps
Stack Pressure
60.00 19.635 0.9950 13885 0.84 25.32 0.21 25.335441
Contractor Information
Contact:Austin Keough
Contracting Company: Alliance Source Testing
Address: 2855S 500 W Sutie A, Salt Lake City, Utah 84115
Phone No.: [phone]
Project No.:

Division of Air Quality
Instrumental Reference Methods - Gaseous Measurements
Round
Method 19 - F factors for Coal, Oil, and Gas
Fd Fw Fc
dscf/MMBtu wscf/MMBtu scf/MMBtu Diluent
F factor used
O2
CO2
Anthracite 2
Bituminous 2
Lignite
Natural
Propane
Butane
10100
COAL
OIL
GAS
9780
9860
9190
8710
8710
8710
10540
10640
11950
320
10610
10200
10390
1970
1800
1910
1420
1040
1190
1250
Wet CEM
Correct For O2
CO2 Interference w/CO
Yes
Yes
Yes
Clean Harbors Primary CEM RATA RM 1, 2, 3A, 6C, 7E, 10, & 19 (Tested 5-8-2024)
Company Clean Harbor cems-#2b
Point Source Main Stack
Test Date 5/8/24
Start
Time
End
Time Run
O2
%
CO2
%
SO2
PPM
SO2
PPM@7%
O2
NOx
PPM
NOx
lb/hr CO
PPM
CO
PPM@7%
O2
THC
PPM
THC
PPM@7%
O2
Flow
ACFM
Headers
Here
11:28 11:49 1 9.1 9.31 1.02 1.27 114.17 25.79 11.19 12.24 0.18 0.33 61843
11:50 12:11 2 8.64 9.74 0.62 0.67 121.91 26.67 1.76 186 0.15 0.26 60905
12:11 12:32 3 8.24 9.85 1.59 1.78 147.8 32.75 0.35 0.39 0.18 0.3 61882
13:27 13:48 4 8.84 9.46 0.87 0.99 141.83 31.77 0.5 0.57 0.16 0.29 62445
13:48 14:09 5 8.82 9.43 1.06 1.21 134.2 30.39 15.01 15.8 0.23 0.41 63117
14:09 14:30 6 9.46 8.87 0.66 0.8 154.07 34.52 0.83 1 0.15 0.28 62650
14:59 15:20 7 8.65 9.77 0.68 0.79 155.49 34.63 11.73 12.28 0.23 0.4 62953
15:20 15:41 8 9.49 8.94 0.5 0.62 182.68 41.47 0.86 1.05 0.16 0.29 96574
15:41 16:02 9 8.96 9.28 0.54 0.63 200.39 45.37 0.8 0.93 0.14 0.26 63639
16:25 16:46 10 8.52 9.68 0.5 0.57 148.88 33.2 13.2 13.33 0.2 0.35 62827
16:46 17:07 11 9.5 9.1 0.73 0.91 137.2 31.25 0.8 0.98 0.11 0.21 63726
17:07 17:28 12 10.09 8.47 0.81 1.05 116.91 26.81 0.94 1.22 0.1 0.2 63389
13
14
15
16
Clean Harbors Primary CEM RATA RM 1, 2, 3A, 6C, 7E, 10, & 19 (Tested 5-8-2024)
Division of Air Quality
NSPS Relative Accuracy Performance Specification Test - CEMS Certification
Clean Harbor cems-#2b
Main Stack
SO2 Analyzer:Serial No.:
CO2 Analyzer:Serial No.:
Acquisition System:Serial No.:
Acquisition System: Serial No.:
Equivalent Emission Limit:91
Test Date SO2 Dry SO2 Dry SO2 Test Date % CO2 Dry
5/8/2024 RM CEMS Diff RM CEMS Diff RM CEMS Diff 5/8/2024 RM CEMS Diff
Run#Start
Time
End
Time ppm lbs./MMBtu lbs./hr. Run#
Start
Time End Time %c %c
1 11:28 11:49 Y 0.5 1.02 -0.53 0.15 1 11:28 11:49 Y 9.3 9.31 -0.03
2 11:50 12:11 Y 0.8 0.62 0.19 0.24 2 11:50 12:11 Y 9.7 9.74 -0.01
3 12:11 12:32 0.7 1.59 0.22 3 12:11 12:32 Y 9.9 9.85 0.01
4 13:27 13:48 Y 1.6 0.87 0.74 0.48 4 13:27 13:48 Y 9.5 9.46 0.03
5 13:48 14:09 2.2 1.06 0.67 5 13:48 14:09 Y 9.5 9.43 0.02
6 14:09 14:30 2.3 0.66 0.71 6 14:09 14:30 Y 8.9 8.87 0.00
7 14:59 15:20 Y 0.9 0.68 0.17 0.25 7 14:59 15:20 Y 9.8 9.77 0.02
8 15:20 15:41 Y 0.2 0.5 -0.26 0.07 8 15:20 15:41 8.9 8.94
9 15:41 16:02 Y 0.3 0.54 -0.27 0.09 9 15:41 16:02 Y 9.3 9.28 0.02
10 16:25 16:46 Y 0.3 0.5 -0.25 0.07 10 16:25 16:46 Y 9.7 9.68 0.00
11 16:46 17:07 Y 0.3 0.73 -0.44 0.09 11 16:46 17:07 9.1 9.1
12 17:07 17:28 Y 0.2 0.81 -0.60 0.06 12 17:07 17:28 8.4 8.47
13 13
14 14
15 15
16 16
Average = 0.6 0.70 0.14 Average = 9.490 9.480 0.005
Sd Standard Deviation = 0.43 Sd Standard Deviation = Sd Standard Deviation = Sd Standard Deviation = 0.02
Confidence Coefficient = 0.33 Confidence Coefficient = Confidence Coefficient = Confidence Coefficient = 0.013
RA - Relative Accuracy = RA RA RA - Relative Accuracy =0.18%
n = 9 0 0 n = 9 or RA of 1%0.01%
t0.975 = 2.306 t0.975 = 2.306
E.L. Relative Accuracy = 1% 0.52%
a For steam generators;b Average of three samples;9
c Make sure that RM and M data are on a consistent basis either wet or dry.
40 CFR 60 Performance Specification 2 For SO2 and NOx Continuous Emission Monitoring Systems
13.2 Relative accuracy Performance Specification. The RA of the CEMSS must be not greater than 20 percent when RM is used in the denominator of Eq. 2-6
(average emissions during test are greater than 50 percent of the emission standard)or 10 percent when the applicable emission standard is used in the
denominator of Eq. 2-6 (average emissions during test are less than 50 percent of the emission standard).
Up dated January 17, 2006
40 CFR 60 Performance Specification 3 For O2 and CO2 Continuous Emission Monitoring Systems
13.2 CEMS Relative Accuracy Perfromance Specification.
The RA of the CEMS must be no grater than 20 percent of the mean value of the reference method (RM) data. 1 percent O2 or CO2.
The results are also acceptable if the absolute value of the difference between the mean RM value and the mean CEMS value is less than or equal to 1.0 percent O2 (or CO2).
Up dated September 14, 2016
40 CFR 60 Performance Specification 6 For Continuous Emission Rate Monitoring Systems (CERMS)
13.2 CERMS Relative Accuracy. The RA of the CERMS shall be no greater than 20 percent of the mean value of the RM's test data in terms of the nits of the emission
standard, or 10 percent of the applicable standard, which err is greater.
Up dated January 17, 2006
PassedPassed
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Servomax - XENTRA 4900 04900 - CL - 652525
04900 - C1-653305 #2bServomaex Model # 4900
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Clean Harbors Primary CEM RATA RM 1, 2, 3A, 6C, 7E, 10, & 19 (Tested 5-8-2024)
Division of Air Quality
Relative Accuracy Test Audit of
Clean Harbor cems-#2b
Main Stack
NOX Analyzer:Serial No.:
O2 Analyzer:Serial No.:
Acquisition System:Serial No.:
Acquisition System: Serial No.:
Equivalent Emission Limit:44.18
Date NOx Dry NOx Dry NOx Test Date % O2 Dry
5/8/2024 RM CEMS Diff RM CEMS Diff RM CEMS Diff 9/30/2014 RM CEMS Diff
Run#Start
Time
End
Time ppm lbs./MMBtu lbs./hr. Run#
Start
Time End Time %c %c
1 11:28 11:49 Y 111.3 114.17 -2.9 Y 24.37 25.79 -1.42 1 11:28 11:49 Y 9.2 9.1 0.083
2 11:50 12:11 Y 116.3 121.91 -5.7 Y 25.02 26.67 -1.65 2 11:50 12:11 Y 8.7 8.64 0.087
3 12:11 12:32 135.7 147.8 29.26 32.75 3 12:11 12:32 Y 8.4 8.24 0.112
4 13:27 13:48 Y 136.5 141.83 -5.3 Y 29.64 31.77 -2.13 4 13:27 13:48 Y 9.0 8.84 0.199
5 13:48 14:09 Y 126.8 134.2 -7.4 Y 27.95 30.39 -2.44 5 13:48 14:09 Y 9.0 8.82 0.155
6 14:09 14:30 Y 144.7 154.07 -9.4 Y 31.84 34.52 -2.68 6 14:09 14:30 Y 9.7 9.46 0.203
7 14:59 15:20 143.8 155.49 30.88 34.63 7 14:59 15:20 Y 8.8 8.65 0.126
8 15:20 15:41 Y 173.3 182.68 -9.4 Y 38.31 41.47 -3.16 8 15:20 15:41 Y 9.6 9.49 0.084
9 15:41 16:02 187.7 200.39 Y 44.49 45.37 -0.88 9 15:41 16:02 Y 9.1 8.96 0.105
10 16:25 16:46 Y 144.1 148.88 -4.8 29.36 33.2 10 16:25 16:46 8.8 8.52
11 16:46 17:07 Y 132.6 137.2 -4.6 Y 28.58 31.25 -2.67 11 16:46 17:07 9.7 9.5
12 17:07 17:28 Y 115.3 116.91 -1.7 Y 25.65 26.81 -1.16 12 17:07 17:28 10.4 10.09
13 13
14 14
15 15
16 16
Average = 133.4 139.1 5.687 30.65 32.67 2.02 Average = 9.030 8.910 0.128
Sd Standard Deviation = 2.67 Sd Standard Deviation = Sd Standard Deviation = 0.780 Sd Standard Deviation = 0.05
Confidence Coefficient = 2.049 Confidence Coefficient = Confidence Coefficient = 0.599 Confidence Coefficient = 0.036
RA - Relative Accuracy =5.80%Relative Accuracy = Relative Accuracy =8.50%RA - Relative Accuracy =1.81%
n = 9 0 9 n = 9 or RA of 1%0.12%
t0.975 = 2.306 t0.975 = t0.975 = 2.306 t0.975 = 2.306
E.L. Relative Accuracy = EMRA EMRA 69%
a For steam generators;b Average of three samples;
c Make sure that RM and M data are on a consistent basis either wet or dry.
40 CFR 60 Performance Specification 2 For SO2 and NOx Continuous Emission Monitoring Systems
4. Performance and Equipment Specifications
4.3 Relative accuracy. The RA of the CEMSS shall be no grater than 20 percent of the mean value of the RM test data in terms of the
units of the emission standard or 10 percent of the applicable standard, whichever is greater
For SO2 emission standards between 0.30 and 0.20 lbs./MMBtu use 15 Percent of the applicable standard;
For SO2 emission standards below 0.20 lbs./MMBtu use 20 Percent of the emission standard;
40 CFR 60 Performance Specification 3 For O2 and CO2 Continuous Emission Monitoring Systems
12. Calculate the arithmetic difference between the RM and the CEMSS output for each run. The average of the nine (of more) data sets constitute the RA.
13.2 Relative accuracy. The RA of the CEMSS must be no grater than 1 percent O2 or CO2.
40 CFR 60 Performance Specification 6 For Continuous Emission Rate Monitoring Systems (CERMS)
13.2 CERMS Relative Accuracy. The RA of the CERMS shall be no greater than 20 percent of the mean value of the RM's test data in terms of the nits of the emission
standard, or 10 percent of the applicable standard, which err is greater.
Up dated January 17, 2006
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614216782 #2bThermo Electron Corp 42i - HL
Servomex - XENTRA 4900 04900 - C1 - 652525 #3
Clean Harbors Primary CEM RATA RM 1, 2, 3A, 6C, 7E, 10, & 19 (Tested 5-8-2024)
Division of Air Quality
Relative Accuracy Test Audit of
Clean Harbor cems-#2b
Main Stack
CO Analyzer:Serial No.:
Acquisition System:
Acquisition System: Serial No.:
Equivalent Emission Limit:100.00
Date CO Dry CO Dry CO
5/8/2024 RM CEMS Diff RM CEMS Diff RM CEMS Diff
Run#Start
Time
End
Time ppm lbs./MMBtu lbs./hr.
1 11:28 11:49 5.07 11.19 0.68
2 11:50 12:11 Y 2.42 1.76 -0.66 0.32
3 12:11 12:32 Y 1.13 0.35 -0.78 0.15
4 13:27 13:48 Y 1.22 0.5 -0.72 0.16
5 13:48 14:09 5.98 15.01 0.80
6 14:09 14:30 Y 1.40 0.83 -0.57 0.19
7 14:59 15:20 Y 5.86 11.73 5.87 0.77
8 15:20 15:41 Y 1.35 0.86 -0.49 0.18
9 15:41 16:02 Y 1.32 0.8 -0.52 0.19
10 16:25 16:46 6.72 13.2 0.83
11 16:46 17:07 Y 1.31 0.8 -0.51 0.17
12 17:07 17:28 Y 1.41 0.94 -0.47 0.19
13
14
15
16
Average = 1.94 2.06 0.13
Sd Standard Deviation = 2.16
Confidence Coefficient = 1.657
RA - Relative Accuracy =
n = 9 0 0
t0.975 = 2.306
E.L. Relative Accuracy = 2%1.79%
a For steam generators;b Average of three samples;
c Make sure that RM and M data are on a consistent basis either wet or dry.
40 CFR 60 Performance Specification 4 For Carbon Monoxide (CO) Continuous Emission Monitoring Systems
applicable emission standard is used to calculate RA.
40 CFR 60 Performance Specification 4A For Carbon Monoxide (CO) Continuous Emission Monitoring Systems
13.2 Relative accuracy. The RA of the CEMSS must be no greater than 10 percent when the average RM value is used to calculate RA, 5 percent when the applicable
emission standard is used to calculate RA, or within 5 ppmv when the RA is calculated as the absolute average difference between the RM and CEMSS plus the 2.5
percent confidence coefficient.
40 CFR 60 Performance Specification 6 For Continuous Emission Rate Monitoring Systems (CERMS)
13.2 CERMS Relative Accuracy. The RA of the CERMS shall be no greater than 20 percent of the mean value of the RM's test data in terms of the nits of the emission
standard, or 10 percent of the applicable standard, which err is greater.
Up dated January 17, 2006
13.2 Relative accuracy. The RA of the CEMSS must be no grater than 10 percent when the average of the RM value is used to calculate RA or 5 percent when the
Passed
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Servomex XEMTRA 4900 4900 - C1 653305
Division of Air Quality
NSPS Relative Accuracy Performance Specification Test - CEMS Certification
Dry Volumetric Flow
dscfh
Run Date Start Time End Time RM CEM Diff
1 5/8/24 11:28 11:49 1,833,843.87
2 5/8/24 11:50 12:11 1,801,920.62
3 5/8/24 12:11 12:32 1,804,926.30
4 5/8/24 13:27 13:48 1,817,608.41
5 5/8/24 13:48 14:09 1,845,711.70
6 5/8/24 14:09 14:30 1,842,836.22
7 5/8/24 14:59 15:20 1,798,275.92
8 5/8/24 15:20 15:41 1,851,227.94
9 5/8/24 15:41 16:02 1,984,119.53
10 5/8/24 16:25 16:46 1,705,204.59
11 5/8/24 16:46 17:07 1,804,833.52
12 5/8/24 17:07 17:28 1,862,924.31
13 5/8/24
14 5/8/24
15 5/8/24
16 5/8/24
Average =
Standard Deviation
Confidence Coefficient =
RA - Relative Accuracy =
n = 0
t0.975 =
Dry Volumetric Flow
dscfm
Run Date Start Time End Time RM CEM Diff
1 5/8/24 11:28 11:49 30,564.06
2 5/8/24 11:50 12:11 30,032.01
3 5/8/24 12:11 12:32 30,082.11
4 5/8/24 13:27 13:48 30,293.47
5 5/8/24 13:48 14:09 30,761.86
6 5/8/24 14:09 14:30 30,713.94
7 5/8/24 14:59 15:20 29,971.27
8 5/8/24 15:20 15:41 30,853.80
9 5/8/24 15:41 16:02 33,068.66
10 5/8/24 16:25 16:46 28,420.08
11 5/8/24 16:46 17:07 30,080.56
12 5/8/24 17:07 17:28 31,048.74
13 5/8/24
14 5/8/24
15 5/8/24
16 5/8/24
Average =
Standard Deviation
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Clean Harbor cems-#2b
Main Stack
Division of Air Quality
NSPS Relative Accuracy Performance Specification Test - CEMS Certification
Clean Harbor cems-#2b
Main Stack
Confidence Coefficient =
RA - Relative Accuracy =
n = 0
t0.975 =
Actual Volumetric Flow
acfm
Run Date Start Time End Time RM CEM Diff
1 5/8/24 11:28 11:49 Y 58,763.63 61843 (3,079.37)
2 5/8/24 11:50 12:11 Y 57,891.83 60905 (3,013.17)
3 5/8/24 12:11 12:32 Y 57,997.86 61882 (3,884.14)
4 5/8/24 13:27 13:48 Y 58,186.36 62445 (4,258.64)
5 5/8/24 13:48 14:09 Y 59,105.28 63117 (4,011.72)
6 5/8/24 14:09 14:30 Y 59,022.81 62650 (3,627.19)
7 5/8/24 14:59 15:20 57,184.97 62953
8 5/8/24 15:20 15:41 Y 58,916.78 63574 (4,657.22)
9 5/8/24 15:41 16:02 Y 63,146.16 63639 (492.84)
10 5/8/24 16:25 16:46 55,146.86 62827
11 5/8/24 16:46 17:07 58,198.14 63726
12 5/8/24 17:07 17:28 Y 60,071.32 63389 (3,317.68)
13 5/8/24
14 5/8/24
15 5/8/24
16 5/8/24
Average = 59,233.56 62,604.89 3,371.33
Standard Deviation 1,208
Confidence Coefficient = 929
RA - Relative Accuracy =1 7.3%
n = 9
t0.975 =2.306
WET VOLUMETRIC FLOW
wscfh
Run Date Start Time End Time RM CEM Diff
1 5/8/24 11:28 11:49 2,579,160.23
2 5/8/24 11:50 12:11 2,534,262.63
3 5/8/24 12:11 12:32 2,538,489.89
4 5/8/24 13:27 13:48 2,543,834.77
5 5/8/24 13:48 14:09 2,583,166.75
6 5/8/24 14:09 14:30 2,579,142.37
7 5/8/24 14:59 15:20 2,498,426.77
8 5/8/24 15:20 15:41 2,571,995.42
9 5/8/24 15:41 16:02 2,756,627.77
10 5/8/24 16:25 16:46 2,404,290.55
11 5/8/24 16:46 17:07 2,544,764.55
12 5/8/24 17:07 17:28 2,626,670.94
13 5/8/24
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Division of Air Quality
NSPS Relative Accuracy Performance Specification Test - CEMS Certification
Clean Harbor cems-#2b
Main Stack
14 5/8/24
15 5/8/24
16 5/8/24
Average =
Standard Deviation
Confidence Coefficient =
RA - Relative Accuracy =
n = 0
t0.975 =
Wet Volumetric Flow
wscfm
Run Date Start Time End Time RM CEM Diff
1 5/8/24 11:28 11:49 42,986.00
2 5/8/24 11:50 12:11 42,237.71
3 5/8/24 12:11 12:32 42,308.16
4 5/8/24 13:27 13:48 42,397.25
5 5/8/24 13:48 14:09 43,052.78
6 5/8/24 14:09 14:30 42,985.71
7 5/8/24 14:59 15:20 41,640.45
8 5/8/24 15:20 15:41 42,866.59
9 5/8/24 15:41 16:02 45,943.80
10 5/8/24 16:25 16:46 40,071.51
11 5/8/24 16:46 17:07 42,412.74
12 5/8/24 17:07 17:28 43,777.85
13 5/8/24
14 5/8/24
15 5/8/24
16 5/8/24
Average =
Standard Deviation
Confidence Coefficient =
RA - Relative Accuracy =
n = 0
t0.975 =
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Clean Harbors Primary CEM RATA RM 1, 2, 3A, 6C, 7E, 10, & 19 (Tested 5-8-2024)
Test Overview
NSPS Relative Accuracy
Performance Specification Test -
CEMS Certification Clean Harbor cems-#2b
Point Source Main Stack
Contact Phone No.Tyler Lee
Stack Designation:Main Stack
Project No.:0
Run Run # 1 Run # 2 Run # 3 Run # 4 Run # 5 Run # 6 Run # 7 Run # 8 Run # 9 Run # 10 Run # 11 Run # 12
Test Date 5/8/2024 5/8/2024 5/8/2024 5/8/2024 5/8/2024 5/8/2024 5/8/2024 5/8/2024 5/8/2024 5/8/2024 5/8/2024 5/8/2024
Start Time 11:28 11:50 12:11 13:27 13:48 14:09 14:59 15:20 15:41 16:25 16:46 17:07
Stop Time 11:49 12:11 12:32 13:48 14:09 14:30 15:20 15:41 16:02 16:46 17:07 17:28
Run Time 0:21 0:21 0:21 0:21 0:21 0:21 0:21 0:21 0:21 0:21 0:21 0:21
Stack I.D. (inches)60.00 60.00 60.00 60.00 60.00 60.00 60.00 60.00 60.00 60.00 60.00 60.00
As ft^2 19.64 19.64 19.64 19.64 19.64 19.64 19.64 19.64 19.64 19.64 19.64 19.64
Cp (Pitot Tube Coefficient)0.84 0.84 0.84 0.84 0.84 0.84 0.84 0.84 0.84 0.84 0.84 0.84
Yd Meter Y Factor (unit less)0.9950 0.9950 0.9950 0.9950 0.9950 0.9950 0.9950 0.9950 0.9950 0.9950 0.9950 0.9950
Pbar Barometric Pressure ("Hg)25.32 25.32 25.32 25.32 25.32 25.32 25.32 25.32 25.32 25.32 25.32 25.32
Pq (Static Pressure)0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21
Ps (Pressure of the Stack)25.34 25.34 25.34 25.34 25.34 25.34 25.34 25.34 25.34 25.34 25.34 25.34
Ts Stack Temp Avg. oF 151.20 152.80 152.90 153.60 153.80 153.90 154.00 154.50 154.50 155.30 153.50 153.50
Tm Meter Temperature oF 49.00 49.00 49.00 56.00 56.00 56.00 59.00 59.00 59.00 59.00 59.00 59.00
CO2 (carbon dioxide)9.28 9.73 9.86 9.49 9.45 8.87 9.79 8.90 9.30 9.68 9.07 8.38
O2 (oxygen)9.18 8.73 8.35 9.04 8.97 9.66 8.78 9.57 9.07 8.77 9.74 10.39
Md Molecular Weight Dry 29.85 29.91 29.91 29.88 29.87 29.81 29.92 29.81 29.85 29.90 29.84 29.76
Ms Molecular Weight Wet 26.43 26.47 26.47 26.49 26.48 26.44 26.58 26.50 26.53 26.44 26.40 26.34
N2 (nitrogen)81.54 81.54 81.79 81.47 81.58 81.47 81.44 81.53 81.64 81.56 81.19 81.23
Vm Sample Volume (cf)39.21 39.21 39.21 42.61 42.61 42.61 40.53 40.53 40.53 40.82 40.82 40.82
Vm std Standard Volume (dscf)34.24 34.24 34.24 36.70 36.70 36.70 34.71 34.71 34.71 34.95 34.95 34.95
Vlc Moisture (g)295.60 295.60 295.60 311.50 311.50 311.50 287.10 287.10 287.10 304.40 304.40 304.40
Vwstd Moisture Volume (scf)13.91 13.91 13.91 14.66 14.66 14.66 13.51 13.51 13.51 14.33 14.33 14.33
Bws Moisture Content (%100)28.90%28.90%28.90%28.55%28.55%28.55%28.02%28.02%28.02%29.08%29.08%29.08%
S Bws (saturation moisture)30.82%32.05%32.13%32.68%32.84%32.92%33.00%33.41%33.41%34.06%32.60%32.60%
AvgSqrtDlp √∆P 0.727 0.716 0.717 0.719 0.730 0.729 0.708 0.728 0.781 0.680 0.718 0.741
Vs. Gas Velocity (ft./sec)49.88 49.14 49.23 49.39 50.17 50.10 48.54 50.01 53.60 46.81 49.40 50.99
Qa (stack actual flow rate) acfm 58,764 57,892 57,998 58,186 59,105 59,023 57,185 58,917 63,146 55,147 58,198 60,071
Qs (stack std. flow rate) dscfm 30,564 30,032 30,082 30,293 30,762 30,714 29,971 30,854 33,069 28,420 30,081 31,049
Qsd (stack std. flow rate) dscfh 1,833,844 1,801,921 1,804,926 1,817,608 1,845,712 1,842,836 1,798,276 1,851,228 1,984,120 1,705,205 1,804,834 1,862,924
Qw (stack flow rate) wscfm 2,579,160 2,534,263 2,538,490 2,543,835 2,583,167 2,579,142 2,498,427 2,571,995 2,756,628 2,404,291 2,544,765 2,626,671
Clean Harbors Primary CEM RATA RM 1, 2, 3A, 6C, 7E, 10, & 19 (Tested 5-8-2024)
Test Overview
NSPS Relative Accuracy
Performance Specification Test -
CEMS Certification Clean Harbor cems-#2b
Point Source Main Stack
Contact Phone No.Tyler Lee
Stack Designation:Main Stack
Project No.:0
Run Run # 1 Run # 2 Run # 3 Run # 4 Run # 5 Run # 6 Run # 7 Run # 8 Run # 9 Run # 10 Run # 11 Run # 12
Test Date 5/8/2024 5/8/2024 5/8/2024 5/8/2024 5/8/2024 5/8/2024 5/8/2024 5/8/2024 5/8/2024 5/8/2024 5/8/2024 5/8/2024
Heat Input - BTU/hr.
F factor - scf/MMBtu
Fuel Analysis - ft3/min 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0 1050.0
Fuel Flow - ft3/min 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0
Heat Input - BTU/hr.
SO2 Concentrations
Uncorrected 0.53 0.87 0.80 1.64 2.18 2.30 1.02 0.58 0.61 0.44 0.32 0.24
Dry Corrected 0.49 0.81 0.74 1.61 2.18 2.31 0.85 0.24 0.27 0.25 0.29 0.21
Wet Corrected
NOx Concentrations
Uncorrected 109.49 115.13 134.30 135.04 125.47 143.01 142.29 171.43 185.65 142.65 131.19 114.19
Dry Corrected 111.25 116.25 135.72 136.51 126.78 144.66 143.77 173.26 187.73 144.12 132.59 115.25
Wet Corrected
CO Concentrations
Uncorrected 5.02 2.25 0.97 1.00 5.69 1.12 5.55 1.02 0.99 6.38 0.96 1.06
Dry Corrected 5.07 2.42 1.13 1.22 5.98 1.40 5.86 1.35 1.32 6.72 1.31 1.41
Wet Corrected
CO2 Concentrations
Uncorrected 9.09 9.57 9.70 9.35 9.33 8.76 9.68 8.83 9.22 9.60 9.01 8.33
Dry Corrected 9.28 9.73 9.86 9.49 9.45 8.87 9.79 8.90 9.30 9.68 9.07 8.38
Wet Corrected
O2 Concentrations
Uncorrected 9.09 8.57 8.20 8.83 8.72 9.40 8.58 9.42 8.92 8.61 9.55 10.19
Dry Corrected 9.18 8.73 8.35 9.04 8.97 9.66 8.78 9.57 9.07 8.77 9.74 10.39
Wet Corrected
Clean Harbors Primary CEM RATA RM 1, 2, 3A, 6C, 7E, 10, & 19 (Tested 5-8-2024)
Division of Air Quality
NSPS Relative Accuracy Performance Specification Test - CEMS Certification
Clean Harbor cems-#2b
Main Stack
Average Emission
Dry SO2 NOX CO
lbs./MMBtu Average % concentration
lbs./hr.30.45 CO2 O2
ppm or % 0.85 138.99 2.93 9.32 9.19
Run 1 Enter O2 or CO2
Dry SO2 NOX CO CO2 O2
Atomic Weight 64 46 28
lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d))
lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d)
lbs./cu.ft 8.077E-08 1.329E-05 3.688E-07
lbs./hr.0.15 24.37 0.68 9.28 9.18
ppm or %0.49 111.25 5.07 9.09 9.09
Run 2
Dry SO2 NOX CO CO2 O2
Atomic Weight 64 46 28
lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d))
lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d)
lbs./cu.ft 1.343E-07 1.389E-05 1.757E-07
lbs./hr.0.24 25.02 0.32 9.73 8.73
ppm or %0.81 116.25 2.42 9.09 8.57 Raw Value
Run 3
Dry SO2 NOX CO CO2 O2
Atomic Weight 64 46 28
lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d))
lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d)
lbs./cu.ft 1.228E-07 1.621E-05 8.190E-08
lbs./hr.0.22 29.26 0.15 9.86 8.35
ppm or %0.74 135.72 1.13 9.70 8.20 Raw Value
Run 4
Dry SO2 NOX CO CO2 O2
Atomic Weight 64 46 28
lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d))
lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d)
lbs./cu.ft 2.667E-07 1.631E-05 8.865E-08
lbs./hr.0.48 29.64 0.16 9.49 9.04
ppm or %1.61 136.51 1.22 9.35 8.83 Raw Value
Run 5
Dry SO2 NOX CO CO2 O2
Atomic Weight 64 46 28
lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d))
lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d)
lbs./cu.ft 3.628E-07 1.514E-05 4.349E-07
lbs./hr.0.67 27.9520 0.80 9.45 8.97
ppm or %2.18 126.78 5.98 9.33 8.72 Raw Value
Corrected For Cal. Drift
Raw Value
Corrected For Cal. Drift
Corrected For Cal. Drift
Corrected For Cal. Drift
Corrected For Cal. Drift
O2
CO2
Clear
lbs./MMBTU
Clean Harbors Primary CEM RATA RM 1, 2, 3A, 6C, 7E, 10, & 19 (Tested 5-8-2024)
Division of Air Quality
NSPS Relative Accuracy Performance Specification Test - CEMS Certification
Clean Harbor cems-#2b
Main Stack
O2
CO2
Clear
lbs./MMBTU
Run 6
Dry SO2 NOX CO CO2 O2
Atomic Weight 64 46 28
lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d))
lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d)
lbs./cu.ft 3.831E-07 1.728E-05 1.020E-07
lbs./hr.0.71 31.8443 0.19 8.87 9.66
ppm or %2.31 144.66 1.40 8.76 9.40 Raw Value
Run 7
Dry SO2 NOX CO CO2 O2
Atomic Weight 64 46 28
lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d))
lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d)
lbs./cu.ft 1.411E-07 1.717E-05 4.261E-07
lbs./hr.0.25 30.88 0.77 9.79 8.78
ppm or %0.85 143.77 5.86 9.68 8.58 Raw Value
Run 8
Dry SO2 NOX CO CO2 O2
Atomic Weight 64 46 28
lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d))
lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d)
lbs./cu.ft 3.939E-08 2.070E-05 9.816E-08
lbs./hr.0.07 38.31 0.18 8.90 9.57
ppm or %0.24 173.26 1.35 8.83 9.42 Raw Value
Run 9
Dry SO2 NOX CO CO2 O2
Atomic Weight 64 46 28
lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d))
lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d)
lbs./cu.ft 4.454E-08 2.242E-05 9.598E-08
lbs./hr.0.09 44.49 0.19 9.30 9.07
ppm or %0.27 187.73 1.32 9.22 8.92 Raw Value
Run 10
Dry SO2 NOX CO CO2 O2
Atomic Weight 64 46 28
lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d))
lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d)
lbs./cu.ft 4.188E-08 1.722E-05 4.884E-07
lbs./hr.0.07 29.36 0.83 9.68 8.77
ppm or %0.25 144.12 6.72 9.60 8.61 Raw Value
Run 11
Dry SO2 NOX CO CO2 O2
Atomic Weight 64 46 28
lbs./MMBtu (O2)E=Cd x Fd x (20.9/(20.9-%O2d))
lbs./MMBtu (CO2)E=Cd x Fc x (100 / % CO2d)
lbs./cu.ft 4.753E-08 1.584E-05 9.517E-08
lbs./hr.0.09 28.58 0.17 9.07 9.74
ppm or %0.29 132.59 1.31 9.01 9.55 Raw Value
Corrected For Cal. Drift
Corrected For Cal. Drift
Corrected For Cal. Drift
Corrected For Cal. Drift
Corrected For Cal. Drift
Corrected For Cal. Drift
Clean Harbors Primary CEM RATA RM 1, 2, 3A, 6C, 7E, 10, & 19 (Tested 5-8-2024)
Calibration Error Test
Test Date May 8, 2024 O2
CS - Cal. Span 23.02
Units %
Cylinder No. Expiration
Date Cal. Gas CV- Certified
Concentration
CDir or CS -
Measured
Concentration
Difference
ACE Eq. 7E-1
Analyzer Cal.
Error
Status
Low-level 0.00 -0.06 0.06 0.26% Passed Cal.
Mid-level 10.99 10.98 0.01 0.04% Passed Cal.
High-level 23.02 23.01 0.01 0.04% Passed Cal.
% of Span Sec. 8.2.1 Cal Gas Verification
0 to 20% of CS - Cal. Span Low-Level 0.00%
40 to 60% of Cal. Span Mid-level 47.74%
100% of Cal. Span High-level 100.00%
Test Date May 8, 2024 CO2
CS - Cal. Span 22.93
Units %
Cylinder
No.
Expiration
Date Cal. Gas CV- Certified
Concentration
CDir or CS -
Measured
Concentration
Difference
ACE Eq. 7E-1
Analyzer Cal.
Error
Status
Low-level 0.00 0.02 0.02 0.087% Passed Cal.
Mid-level 11.10 10.87 0.23 1.003% Passed Cal.
High-level 22.93 22.98 0.05 0.218% Passed Cal.
% of Span Sec. 8.2.1 Cal Gas Verification
0 to 20% of Cal. Span Low-Level 0.00%
40 to 60% of Cal. Span Mid-level 48.41%
100% of Cal. Span High-level 100.00%
Test Date May 8, 2024 SO2
CS - Cal. Span 20.00
Units ppm
Cylinder
No.
Expiration
Date Cal. Gas CV- Certified
Concentration
CDir or CS -
Measured
Concentration
Difference
ACE Eq. 7E-1
Analyzer Cal.
Error
Status
Low-level 0.00 0.03 0.03 0.150% Passed Cal.
Mid-level 10.00 9.96 0.04 0.200% Passed Cal.
High-level 20.00 20.09 0.09 0.450% Passed Cal.
% of Span Sec. 8.2.1 Cal Gas Verification
0 to 20% of Cal. Span Low-Level 0.00%
40 to 60% of Cal. Span Mid-level 50.00%
100% of Cal. Span High-level 100.00%
Test Date May 8, 2024 NOx
CS - Cal. Span 500.00
Units ppm
Cylinder
No.
Expiration
Date Cal. Gas CV- Certified
Concentration
CDir or CS -
Measured
Concentration
Difference
ACE Eq. 7E-1
Analyzer Cal.
Error
Status
Low-level 0.00 0.09 0.09 0.018% Passed Cal.
Mid-level 250.00 249.57 0.43 0.086% Passed Cal.
High-level 500.00 497.52 2.48 0.496% Passed Cal.
% of Span Sec. 8.2.1 Cal Gas Verification
0 to 20% of Cal. Span Low-Level 0.00%
40 to 60% of Cal. Span Mid-level 50.00%
100% of Cal. Span High-level 100.00%
Test Date May 8, 2024 CO
CS - Cal. Span 50.00
100 Units ppm
Cylinder
No.
Expiration
Date Cal. Gas CV- Certified
Concentration
CDir or CS -
Measured
Concentration
Difference
ACE Eq. 7E-1
Analyzer Cal.
Error
Status
Low-level 0.00 -0.03 0.03 0.060% Passed Cal.
Mid-level 25.00 25.04 0.04 0.080% Passed Cal.
High-level 50.00 49.99 0.01 0.020% Passed Cal.
% of Span Sec. 8.2.1 Cal Gas Verification
0 to 20% of Cal. Span Low-Level 0.00%
40 to 60% of Cal. Span Mid-level 50.00%
100% of Cal. Span High-level 100.00%
Clean Harbors Secondary CEM THC RATA RM 25A (Tested 5-8-2024)
Reference Methods 25 A & B
Compromised
Source Information
Company Name Clean Harbors CEMS #2 Incinerator Stack
Company Contact:Willian Simmons
Contact Phone No.435-844-8351
Point Source:Clean Harbors CEMS #2
Test & Review Dates
Test Date:5/8/2024 Tabs Are Shown
Review Date: 10/1/2024
Observer:Not Observed
Reviewer:Rob Leishman
Emission Limits Emission Rates
VOC VOC
mg/L gas
10.0
lbs./hr.
%O2 Correction as a whole #7.00
Test Information
Stack I.D. inches
As ft^2 Y Dl H @ Cp Pbar Pq (static)
Ps
Stack Pressure
60.0 19.6 0
Contractor Information
Contact:
Contracting Company:
Address:
Phone No.: Btu/hr Selected
Project No.:

Division of Air Quality
Instrumental Reference Methods - Gaseous Measurements
Round
ppm
Method 19 - F factors for Coal, Oil, and Gas
Fd Fw Fc
dscf/MMBtu wscf/MMBtu scf/MMBtu
Diluent
F factor used
O2
CO2
Anthracite 2
Bituminous 2
Lignite
Natural
Propane
Butane
10100
COAL
OIL
GAS
9780
9860
9190
8710
8710
8710
10540
10640
11950
320
10610
10200
10390
1970
1800
1910
1420
1040
1190
1250
Wet CEM
Correct For O2 Yes
Yes
Clean Harbors Secondary CEM THC RATA RM 25A (Tested 5-8-2024)
D$I$v$I$s$I$on of A$I$r Qual$I$ty
NSPS Relat$I$ve Accuracy Performance Spec$I$f$I$cat$I$on Test - CEMS Cert$I$f$I$cat$I$on
Clean Harbors CEMS #2 Incinerator Stack
Clean Harbors CEMS #2
VOC/THC Analyzer:Thermo 5Li-TH Serial No.:THC - 1203299856
O2 Analyzer:Serial No.:
Acquisition System:Serial No.:
Acquisition System: Serial No.:
Equivalent Emission Limit:10 I & J
Test Date VOC Dry VOC Test Date % O2 Dry
5/8/2024 ppm lbs/hr 9/30/2014 RM CEMS Diff
Run#Start
Time
End
Time RM CEMS Diff RM CEMS Diff Run#
Start
Time End Time %c %c
1 11:28 11:49 1.30 0.07 1 11:28 11:49 10.0
2 11:50 12:11 1.04 0.06 2 11:50 12:11 8.7
3 12:11 12:32 0.78 0.08 3 12:11 12:32 8.4
4 13:27 13:48 Y 0.57 0.04 0.53 4 13:27 13:48 9.0
5 13:48 14:09 Y 0.59 0.15 0.44 5 13:48 14:09 9.0
6 14:09 14:30 Y 0.18 0.03 0.15 6 14:09 14:30 9.7
7 14:59 15:20 Y 0.19 0.11 0.08 7 14:59 15:20 8.8
8 15:20 15:41 Y 0.18 0.05 0.13 8 15:20 15:41 9.6
9 15:41 16:02 Y 0.00 0.05 -0.05 9 15:41 16:02 9.1
10 16:25 16:46 Y 0.00 0.1 -0.10 10 16:25 16:46 8.8
11 16:46 17:07 Y 0.00 0.0 -0.02 11 16:46 17:07 9.7
12 17:07 17:28 Y 0.000 0.0 0.00 12 17:07 17:28 10.4
13 13
14 14
15 15
16 16
Average = 0.2 0.06 0.13 Average =
Sd Standard Deviation = 0.22 Sd Standard Deviation = Sd Standard Deviation =
Confidence Coefficient = 0.17 Confidence Coefficient = Confidence Coefficient =
RA - Relative Accuracy =156.30%RA RA - Relative Accuracy =
n = 9 0 n = 0 or RA of 1%
t0.975 = 2.306 t0.975 =
E.L. Relative Accuracy = 2.97%
a For steam generators;b Average of three samples;
c Make sure that RM and M data are on a consistent basis either wet or dry.
40 CFR 60 Performance Specification 2 For SO2 and NOx Continuous Emission Monitoring Systems
13.2 Relative accuracy Performance Specification. The RA of the CEMSS must be not greater than 20 percent when RM is used in the denominator of Eq. 2-6
(average emissions during test are greater than 50 percent of the emission standard)or 10 percent when the applicable emission standard is used in the
denominator of Eq. 2-6 (average emissions during test are less than 50 percent of the emission standard).
Up dated January 17, 2006
40 CFR 60 Performance Specification 3 For O2 and CO2 Continuous Emission Monitoring Systems
13.2 CEMS Relative Accuracy Perfromance Specification.
The RA of the CEMS must be no grater than 20 percent of the mean value of the reference method (RM) data. 1 percent O2 or CO2.
The results are also acceptable if the absolute value of the difference between the mean RM value and the mean CEMS value is less than or equal to 1.0 percent O2 (or CO2).
Up dated September 14, 2016
40 CFR 60 Performance Specification 6 For Continuous Emission Rate Monitoring Systems (CERMS)
13.2 CERMS Relative Accuracy. The RA of the CERMS shall be no greater than 20 percent of the mean value of the RM's test data in terms of the nits of the emission
standard, or 10 percent of the applicable standard, which err is greater.
Up dated January 17, 2006
Ac
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i
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a
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e

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n
?
Ac
t
i
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e

R
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Ac
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Passed
Clean Harbors Secondary CEM RATA RM 1, 2, 3A, 6C, 7E, 10, & 19 (Tested 5-8-2024)
Reference Methods 2, 3A, 6C, 7E, 10, & 19
Source Information
Company Name Clean Harbor cems-#2
Company Contact:Tyler Lee
Contact Phone No.435-884-8122
Stack Designation:Main Stack
Test & Review Dates
Test Date:5/8/2024
Review Date: 9/27/2024
Observer:Not Observed
Reviewer:Rob Leishman
Emission Limits Emission Rates
SO2 NOX CO SO2 NOX CO
lbs./MMBtu
lbs./hr. 44.2 30.446
ppm 91.0 100.00 0.854 2.933
%O2 Correction as a whole #7.00 7.00
Test Information
Stack I.D. inches
As ft^2 Y Dl H @ Cp Pbar Pq (static)
Ps
Stack Pressure
60.00 19.635 0.9950 13885 0.84 25.32 0.21 25.335441
Contractor Information
Contact:Austin Keough
Contracting Company: Alliance Source Testing
Address: 2855S 500 W Sutie A, Salt Lake City, Utah 84115
Phone No.: [phone]
Project No.:

Division of Air Quality
Instrumental Reference Methods - Gaseous Measurements
Round
Method 19 - F factors for Coal, Oil, and Gas
Fd Fw Fc
dscf/MMBtu wscf/MMBtu scf/MMBtu Diluent
F factor used
O2
CO2
Anthracite 2
Bituminous 2
Lignite
Natural
Propane
Butane
10100
COAL
OIL
GAS
9780
9860
9190
8710
8710
8710
10540
10640
11950
320
10610
10200
10390
1970
1800
1910
1420
1040
1190
1250
Wet CEM
Correct For O2
CO2 Interference w/CO
Yes
Yes
Yes
Clean Harbors Secondary CEM RATA RM 1, 2, 3A, 6C, 7E, 10, & 19 (Tested 5-8-2024)
Company Clean Harbor cems-#2
Point Source Main Stack
Test Date 5/8/24
Start
Time
End
Time Run
O2
%
CO2
%
SO2
PPM
SO2
PPM@7%
O2
NOx
PPM
NOx
lb/hr CO
PPM
CO
PPM@7%
O2
THC
PPM
THC
PPM@7%
O2
Flow
ACFM
Headers
Here
11:28 11:49 1 9.1 9.31 0.07 0.07 113.33 25.6 11.32 13.3 61843
11:50 12:11 2 8.64 9.74 0.07 0.08 120.79 26.43 1.92 2.11 60905
12:11 12:32 3 8.24 9.85 0.86 0.99 145.72 32.29 0.68 0.75 61882
13:27 13:48 4 8.84 9.46 0.3 0.35 141.28 31.65 0.82 0.94 62445
13:48 14:09 5 8.82 9.43 0.13 0.15 133.2 30.16 14.28 15.19 63117
14:09 14:30 6 9.46 8.87 0.35 0.43 154.04 34.51 0.93 1.13 62650
14:59 15:20 7 8.65 9.77 0.34 0.38 154.32 34.37 11.71 12.41 62953
15:20 15:41 8 9.49 8.94 0.2 0.24 180.45 40.97 0.9 1.09 96574
15:41 16:02 9 8.96 9.28 0.3 0.36 199.82 45.24 0.93 1.08 63639
16:25 16:46 10 8.52 9.68 0.57 0.64 145.94 32.55 13.23 13.31 62827
16:46 17:07 11 9.5 9.1 0.84 1.04 136.44 31.08 0.9 1.09 63726
17:07 17:28 12 10.09 8.47 0.8 1.02 115.13 26.4 1.04 1.34 63389
13
14
15
16
Clean Harbors Secondary CEM RATA RM 1, 2, 3A, 6C, 7E, 10, & 19 (Tested 5-8-2024)
Division of Air Quality
NSPS Relative Accuracy Performance Specification Test - CEMS Certification
Clean Harbor cems-#2
Main Stack
SO2 Analyzer:Serial No.:
CO2 Analyzer:Serial No.:
Acquisition System:Serial No.:
Acquisition System: Serial No.:
Equivalent Emission Limit:91
Test Date SO2 Dry SO2 Dry SO2 Test Date % CO2 Dry
5/8/2024 RM CEMS Diff RM CEMS Diff RM CEMS Diff 5/8/2024 RM CEMS Diff
Run#Start
Time
End
Time ppm lbs./MMBtu lbs./hr. Run#
Start
Time End Time %c %c
1 11:28 11:49 Y 0.5 1.02 -0.53 0.15 1 11:28 11:49 Y 9.3 9.31 -0.03
2 11:50 12:11 Y 0.8 0.62 0.19 0.24 2 11:50 12:11 Y 9.7 9.74 -0.01
3 12:11 12:32 0.7 1.59 0.22 3 12:11 12:32 Y 9.9 9.85 0.01
4 13:27 13:48 Y 1.6 0.87 0.74 0.48 4 13:27 13:48 Y 9.5 9.46 0.03
5 13:48 14:09 2.2 1.06 0.67 5 13:48 14:09 Y 9.5 9.43 0.02
6 14:09 14:30 2.3 0.66 0.71 6 14:09 14:30 Y 8.9 8.87 0.00
7 14:59 15:20 Y 0.9 0.68 0.17 0.25 7 14:59 15:20 Y 9.8 9.77 0.02
8 15:20 15:41 Y 0.2 0.5 -0.26 0.07 8 15:20 15:41 8.9 8.94
9 15:41 16:02 Y 0.3 0.54 -0.27 0.09 9 15:41 16:02 Y 9.3 9.28 0.02
10 16:25 16:46 Y 0.3 0.5 -0.25 0.07 10 16:25 16:46 Y 9.7 9.68 0.00
11 16:46 17:07 Y 0.3 0.73 -0.44 0.09 11 16:46 17:07 9.1 9.1
12 17:07 17:28 Y 0.2 0.81 -0.60 0.06 12 17:07 17:28 8.4 8.47
13 13
14 14
15 15
16 16
Average = 0.6 0.70 0.14 Average = 9.490 9.480 0.005
Sd Standard Deviation = 0.43 Sd Standard Deviation = Sd Standard Deviation = Sd Standard Deviation = 0.02
Confidence Coefficient = 0.33 Confidence Coefficient = Confidence Coefficient = Confidence Coefficient = 0.013
RA - Relative Accuracy = RA RA RA - Relative Accuracy =0.18%
n = 9 0 0 n = 9 or RA of 1%0.01%
t0.975 = 2.306 t0.975 = 2.306
E.L. Relative Accuracy = 1% 0.52%
a For steam generators;b Average of three samples;9
c Make sure that RM and M data are on a consistent basis either wet or dry.
40 CFR 60 Performance Specification 2 For SO2 and NOx Continuous Emission Monitoring Systems
13.2 Relative accuracy Performance Specification. The RA of the CEMSS must be not greater than 20 percent when RM is used in the denominator of Eq. 2-6
(average emissions during test are greater than 50 percent of the emission standard)or 10 percent when the applicable emission standard is used in the
denominator of Eq. 2-6 (average emissions during test are less than 50 percent of the emission standard).
Up dated January 17, 2006
40 CFR 60 Performance Specification 3 For O2 and CO2 Continuous Emission Monitoring Systems
13.2 CEMS Relative Accuracy Perfromance Specification.
The RA of the CEMS must be no grater than 20 percent of the mean value of the reference method (RM) data. 1 percent O2 or CO2.
The results are also acceptable if the absolute value of the difference between the mean RM value and the mean CEMS value is less than or equal to 1.0 percent O2 (or CO2).
Up dated September 14, 2016
40 CFR 60 Performance Specification 6 For Continuous Emission Rate Monitoring Systems (CERMS)
13.2 CERMS Relative Accuracy. The RA of the CERMS shall be no greater than 20 percent of the mean value of the RM's test data in terms of the nits of the emission
standard, or 10 percent of the applicable standard, which err is greater.
Up dated January 17, 2006
PassedPassed
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Servomax - XENTRA 4900 04900 - CL - 4022
04900 - C1-653205 #2Servomaex Model # 4900
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Clean Harbors Secondary CEM RATA RM 1, 2, 3A, 6C, 7E, 10, & 19 (Tested 5-8-2024)
Division of Air Quality
Relative Accuracy Test Audit of
Clean Harbor cems-#2
Main Stack
NOX Analyzer:Serial No.:
O2 Analyzer:Serial No.:
Acquisition System:Serial No.:
Acquisition System: Serial No.:
Equivalent Emission Limit:44.18
Date NOx Dry NOx Dry NOx Test Date % O2 Dry
5/8/2024 RM CEMS Diff RM CEMS Diff RM CEMS Diff 9/30/2014 RM CEMS Diff
Run#Start
Time
End
Time ppm lbs./MMBtu lbs./hr. Run#
Start
Time End Time %c %c
1 11:28 11:49 Y 111.3 114.17 -2.9 Y 24.37 25.79 -1.42 1 11:28 11:49 Y 9.2 9.1 0.083
2 11:50 12:11 Y 116.3 121.91 -5.7 Y 25.02 26.67 -1.65 2 11:50 12:11 Y 8.7 8.64 0.087
3 12:11 12:32 135.7 147.8 29.26 32.75 3 12:11 12:32 Y 8.4 8.24 0.112
4 13:27 13:48 Y 136.5 141.83 -5.3 Y 29.64 31.77 -2.13 4 13:27 13:48 Y 9.0 8.84 0.199
5 13:48 14:09 Y 126.8 134.2 -7.4 Y 27.95 30.39 -2.44 5 13:48 14:09 Y 9.0 8.82 0.155
6 14:09 14:30 Y 144.7 154.07 -9.4 Y 31.84 34.52 -2.68 6 14:09 14:30 Y 9.7 9.46 0.203
7 14:59 15:20 143.8 155.49 30.88 34.63 7 14:59 15:20 Y 8.8 8.65 0.126
8 15:20 15:41 Y 173.3 182.68 -9.4 Y 38.31 41.47 -3.16 8 15:20 15:41 Y 9.6 9.49 0.084
9 15:41 16:02 187.7 200.39 Y 44.49 45.37 -0.88 9 15:41 16:02 Y 9.1 8.96 0.105
10 16:25 16:46 Y 144.1 148.88 -4.8 29.36 33.2 10 16:25 16:46 8.8 8.52
11 16:46 17:07 Y 132.6 137.2 -4.6 Y 28.58 31.25 -2.67 11 16:46 17:07 9.7 9.5
12 17:07 17:28 Y 115.3 116.91 -1.7 Y 25.65 26.81 -1.16 12 17:07 17:28 10.4 10.09
13 13
14 14
15 15
16 16
Average = 133.4 139.1 5.687 30.65 32.67 2.02 Average = 9.030 8.910 0.128
Sd Standard Deviation = 2.67 Sd Standard Deviation = Sd Standard Deviation = 0.780 Sd Standard Deviation = 0.05
Confidence Coefficient = 2.049 Confidence Coefficient = Confidence Coefficient = 0.599 Confidence Coefficient = 0.036
RA - Relative Accuracy =5.80%Relative Accuracy = Relative Accuracy =8.50%RA - Relative Accuracy =1.81%
n = 9 0 9 n = 9 or RA of 1%0.12%
t0.975 = 2.306 t0.975 = t0.975 = 2.306 t0.975 = 2.306
E.L. Relative Accuracy = EMRA EMRA 69%
a For steam generators;b Average of three samples;
c Make sure that RM and M data are on a consistent basis either wet or dry.
40 CFR 60 Performance Specification 2 For SO2 and NOx Continuous Emission Monitoring Systems
4. Performance and Equipment Specifications
4.3 Relative accuracy. The RA of the CEMSS shall be no grater than 20 percent of the mean value of the RM test data in terms of the
units of the emission standard or 10 percent of the applicable standard, whichever is greater
For SO2 emission standards between 0.30 and 0.20 lbs./MMBtu use 15 Percent of the applicable standard;
For SO2 emission standards below 0.20 lbs./MMBtu use 20 Percent of the emission standard;
40 CFR 60 Performance Specification 3 For O2 and CO2 Continuous Emission Monitoring Systems
12. Calculate the arithmetic difference between the RM and the CEMSS output for each run. The average of the nine (of more) data sets constitute the RA.
13.2 Relative accuracy. The RA of the CEMSS must be no grater than 1 percent O2 or CO2.
40 CFR 60 Performance Specification 6 For Continuous Emission Rate Monitoring Systems (CERMS)
13.2 CERMS Relative Accuracy. The RA of the CERMS shall be no greater than 20 percent of the mean value of the RM's test data in terms of the nits of the emission
standard, or 10 percent of the applicable standard, which err is greater.
Up dated January 17, 2006
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61613-332 #2Thermo Environmental 42C - HL
Servomex - XENTRA 4900 04900C1-4022 #2
Clean Harbors Secondary CEM RATA RM 1, 2, 3A, 6C, 7E, 10, & 19 (Tested 5-8-2024)
Division of Air Quality
Relative Accuracy Test Audit of
Clean Harbor cems-#2
Main Stack
CO Analyzer:Serial No.:
Acquisition System:
Acquisition System: Serial No.:
Equivalent Emission Limit:100.00
Date CO Dry CO Dry CO
5/8/2024 RM CEMS Diff RM CEMS Diff RM CEMS Diff
Run#Start
Time
End
Time ppm lbs./MMBtu lbs./hr.
1 11:28 11:49 5.07 11.19 0.68
2 11:50 12:11 Y 2.42 1.76 -0.66 0.32
3 12:11 12:32 Y 1.13 0.35 -0.78 0.15
4 13:27 13:48 Y 1.22 0.5 -0.72 0.16
5 13:48 14:09 5.98 15.01 0.80
6 14:09 14:30 Y 1.40 0.83 -0.57 0.19
7 14:59 15:20 Y 5.86 11.73 5.87 0.77
8 15:20 15:41 Y 1.35 0.86 -0.49 0.18
9 15:41 16:02 Y 1.32 0.8 -0.52 0.19
10 16:25 16:46 6.72 13.2 0.83
11 16:46 17:07 Y 1.31 0.8 -0.51 0.17
12 17:07 17:28 Y 1.41 0.94 -0.47 0.19
13
14
15
16
Average = 1.94 2.06 0.13
Sd Standard Deviation = 2.16
Confidence Coefficient = 1.657
RA - Relative Accuracy =
n = 9 0 0
t0.975 = 2.306
E.L. Relative Accuracy = 2%1.79%
a For steam generators;b Average of three samples;
c Make sure that RM and M data are on a consistent basis either wet or dry.
40 CFR 60 Performance Specification 4 For Carbon Monoxide (CO) Continuous Emission Monitoring Systems
applicable emission standard is used to calculate RA.
40 CFR 60 Performance Specification 4A For Carbon Monoxide (CO) Continuous Emission Monitoring Systems
13.2 Relative accuracy. The RA of the CEMSS must be no greater than 10 percent when the average RM value is used to calculate RA, 5 percent when the applicable
emission standard is used to calculate RA, or within 5 ppmv when the RA is calculated as the absolute average difference between the RM and CEMSS plus the 2.5
percent confidence coefficient.
40 CFR 60 Performance Specification 6 For Continuous Emission Rate Monitoring Systems (CERMS)
13.2 CERMS Relative Accuracy. The RA of the CERMS shall be no greater than 20 percent of the mean value of the RM's test data in terms of the nits of the emission
standard, or 10 percent of the applicable standard, which err is greater.
Up dated January 17, 2006
13.2 Relative accuracy. The RA of the CEMSS must be no grater than 10 percent when the average of the RM value is used to calculate RA or 5 percent when the
Passed
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Servomex XEMTRA 4900 4900 - C1 653205
Division of Air Quality
NSPS Relative Accuracy Performance Specification Test - CEMS Certification
Dry Volumetric Flow
dscfh
Run Date Start Time End Time RM CEM Diff
1 5/8/24 11:28 11:49 1,833,843.87
2 5/8/24 11:50 12:11 1,801,920.62
3 5/8/24 12:11 12:32 1,804,926.30
4 5/8/24 13:27 13:48 1,817,608.41
5 5/8/24 13:48 14:09 1,845,711.70
6 5/8/24 14:09 14:30 1,842,836.22
7 5/8/24 14:59 15:20 1,798,275.92
8 5/8/24 15:20 15:41 1,851,227.94
9 5/8/24 15:41 16:02 1,984,119.53
10 5/8/24 16:25 16:46 1,705,204.59
11 5/8/24 16:46 17:07 1,804,833.52
12 5/8/24 17:07 17:28 1,862,924.31
13 5/8/24
14 5/8/24
15 5/8/24
16 5/8/24
Average =
Standard Deviation
Confidence Coefficient =
RA - Relative Accuracy =
n = 0
t0.975 =
Dry Volumetric Flow
dscfm
Run Date Start Time End Time RM CEM Diff
1 5/8/24 11:28 11:49 30,564.06
2 5/8/24 11:50 12:11 30,032.01
3 5/8/24 12:11 12:32 30,082.11
4 5/8/24 13:27 13:48 30,293.47
5 5/8/24 13:48 14:09 30,761.86
6 5/8/24 14:09 14:30 30,713.94
7 5/8/24 14:59 15:20 29,971.27
8 5/8/24 15:20 15:41 30,853.80
9 5/8/24 15:41 16:02 33,068.66
10 5/8/24 16:25 16:46 28,420.08
11 5/8/24 16:46 17:07 30,080.56
12 5/8/24 17:07 17:28 31,048.74
13 5/8/24
14 5/8/24
15 5/8/24
16 5/8/24
Average =
Standard Deviation
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Clean Harbor cems-#2
Main Stack
Division of Air Quality
NSPS Relative Accuracy Performance Specification Test - CEMS Certification
Clean Harbor cems-#2
Main Stack
Confidence Coefficient =
RA - Relative Accuracy =
n = 0
t0.975 =
Actual Volumetric Flow
acfm
Run Date Start Time End Time RM CEM Diff
1 5/8/24 11:28 11:49 Y 58,763.63 61843 (3,079.37)
2 5/8/24 11:50 12:11 Y 57,891.83 60905 (3,013.17)
3 5/8/24 12:11 12:32 Y 57,997.86 61882 (3,884.14)
4 5/8/24 13:27 13:48 Y 58,186.36 62445 (4,258.64)
5 5/8/24 13:48 14:09 Y 59,105.28 63117 (4,011.72)
6 5/8/24 14:09 14:30 Y 59,022.81 62650 (3,627.19)
7 5/8/24 14:59 15:20 57,184.97 62953
8 5/8/24 15:20 15:41 Y 58,916.78 63574 (4,657.22)
9 5/8/24 15:41 16:02 Y 63,146.16 63639 (492.84)
10 5/8/24 16:25 16:46 55,146.86 62827
11 5/8/24 16:46 17:07 58,198.14 63726
12 5/8/24 17:07 17:28 Y 60,071.32 63389 (3,317.68)
13 5/8/24
14 5/8/24
15 5/8/24
16 5/8/24
Average = 59,233.56 62,604.89 3,371.33
Standard Deviation 1,208
Confidence Coefficient = 929
RA - Relative Accuracy =1 7.3%
n = 9
t0.975 =2.306
WET VOLUMETRIC FLOW
wscfh
Run Date Start Time End Time RM CEM Diff
1 5/8/24 11:28 11:49 2,579,160.23
2 5/8/24 11:50 12:11 2,534,262.63
3 5/8/24 12:11 12:32 2,538,489.89
4 5/8/24 13:27 13:48 2,543,834.77
5 5/8/24 13:48 14:09 2,583,166.75
6 5/8/24 14:09 14:30 2,579,142.37
7 5/8/24 14:59 15:20 2,498,426.77
8 5/8/24 15:20 15:41 2,571,995.42
9 5/8/24 15:41 16:02 2,756,627.77
10 5/8/24 16:25 16:46 2,404,290.55
11 5/8/24 16:46 17:07 2,544,764.55
12 5/8/24 17:07 17:28 2,626,670.94
13 5/8/24
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Division of Air Quality
NSPS Relative Accuracy Performance Specification Test - CEMS Certification
Clean Harbor cems-#2
Main Stack
14 5/8/24
15 5/8/24
16 5/8/24
Average =
Standard Deviation
Confidence Coefficient =
RA - Relative Accuracy =
n = 0
t0.975 =
Wet Volumetric Flow
wscfm
Run Date Start Time End Time RM CEM Diff
1 5/8/24 11:28 11:49 42,986.00
2 5/8/24 11:50 12:11 42,237.71
3 5/8/24 12:11 12:32 42,308.16
4 5/8/24 13:27 13:48 42,397.25
5 5/8/24 13:48 14:09 43,052.78
6 5/8/24 14:09 14:30 42,985.71
7 5/8/24 14:59 15:20 41,640.45
8 5/8/24 15:20 15:41 42,866.59
9 5/8/24 15:41 16:02 45,943.80
10 5/8/24 16:25 16:46 40,071.51
11 5/8/24 16:46 17:07 42,412.74
12 5/8/24 17:07 17:28 43,777.85
13 5/8/24
14 5/8/24
15 5/8/24
16 5/8/24
Average =
Standard Deviation
Confidence Coefficient =
RA - Relative Accuracy =
n = 0
t0.975 =
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Clean Harbors Backup CEM THC RATA RM 25A (Tested 5-8-2024)
Reference Methods 25 A & B
Compromised
Source Information
Company Name Clean Harbors CEMS #2B Incinerator Stack
Company Contact:Willian Simmons
Contact Phone No.435-844-8351
Point Source:Clean Harbors CEMS #2B
Test & Review Dates
Test Date:5/8/2024 Tabs Are Shown
Review Date: 10/1/2024
Observer:Not Observed
Reviewer:Rob Leishman
Emission Limits Emission Rates
VOC VOC
mg/L gas
10.0
lbs./hr.
%O2 Correction as a whole #7.00
Test Information
Stack I.D. inches
As ft^2 Y Dl H @ Cp Pbar Pq (static)
Ps
Stack Pressure
60.0 19.6 0
Contractor Information
Contact:
Contracting Company:
Address:
Phone No.: Btu/hr Selected
Project No.:

Division of Air Quality
Instrumental Reference Methods - Gaseous Measurements
Round
ppm
Method 19 - F factors for Coal, Oil, and Gas
Fd Fw Fc
dscf/MMBtu wscf/MMBtu scf/MMBtu
Diluent
F factor used
O2
CO2
Anthracite 2
Bituminous 2
Lignite
Natural
Propane
Butane
10100
COAL
OIL
GAS
9780
9860
9190
8710
8710
8710
10540
10640
11950
320
10610
10200
10390
1970
1800
1910
1420
1040
1190
1250
Wet CEM
Correct For O2 Yes
Yes
Clean Harbors Backup CEM THC RATA RM 25A (Tested 5-8-2024)
D$I$v$I$s$I$on of A$I$r Qual$I$ty
NSPS Relat$I$ve Accuracy Performance Spec$I$f$I$cat$I$on Test - CEMS Cert$I$f$I$cat$I$on
Clean Harbors CEMS #2B Incinerator Stack
Clean Harbors CEMS #2B
VOC/THC Analyzer:Thermo 5Li-TH Serial No.:THC - 1203299855
O2 Analyzer:Serial No.:
Acquisition System:Serial No.:
Acquisition System: Serial No.:
Equivalent Emission Limit:10 I & J
Test Date VOC Dry VOC Test Date % O2 Dry
5/8/2024 ppm lbs/hr 9/30/2014 RM CEMS Diff
Run#Start
Time
End
Time RM CEMS Diff RM CEMS Diff Run#
Start
Time End Time %c %c
1 11:28 11:49 1.30 0.12 1 11:28 11:49 10.0
2 11:50 12:11 1.04 0.11 2 11:50 12:11 8.7
3 12:11 12:32 0.78 0.14 3 12:11 12:32 8.4
4 13:27 13:48 Y 0.57 0.07 0.50 4 13:27 13:48 9.0
5 13:48 14:09 Y 0.59 0.26 0.33 5 13:48 14:09 9.0
6 14:09 14:30 Y 0.18 0.05 0.13 6 14:09 14:30 9.7
7 14:59 15:20 Y 0.19 0.2 -0.01 7 14:59 15:20 8.8
8 15:20 15:41 Y 0.18 0.09 0.09 8 15:20 15:41 9.6
9 15:41 16:02 Y 0.00 0.1 -0.10 9 15:41 16:02 9.1
10 16:25 16:46 Y 0.00 0.17 -0.17 10 16:25 16:46 8.8
11 16:46 17:07 Y 0.00 0.0 -0.03 11 16:46 17:07 9.7
12 17:07 17:28 Y 0.000 0.0 0.00 12 17:07 17:28 10.4
13 13
14 14
15 15
16 16
Average = 0.2 0.11 0.08 Average =
Sd Standard Deviation = 0.21 Sd Standard Deviation = Sd Standard Deviation =
Confidence Coefficient = 0.16 Confidence Coefficient = Confidence Coefficient =
RA - Relative Accuracy =129.60%RA RA - Relative Accuracy =
n = 9 0 n = 0 or RA of 1%
t0.975 = 2.306 t0.975 =
E.L. Relative Accuracy = 2.46%
a For steam generators;b Average of three samples;
c Make sure that RM and M data are on a consistent basis either wet or dry.
40 CFR 60 Performance Specification 2 For SO2 and NOx Continuous Emission Monitoring Systems
13.2 Relative accuracy Performance Specification. The RA of the CEMSS must be not greater than 20 percent when RM is used in the denominator of Eq. 2-6
(average emissions during test are greater than 50 percent of the emission standard)or 10 percent when the applicable emission standard is used in the
denominator of Eq. 2-6 (average emissions during test are less than 50 percent of the emission standard).
Up dated January 17, 2006
40 CFR 60 Performance Specification 3 For O2 and CO2 Continuous Emission Monitoring Systems
13.2 CEMS Relative Accuracy Perfromance Specification.
The RA of the CEMS must be no grater than 20 percent of the mean value of the reference method (RM) data. 1 percent O2 or CO2.
The results are also acceptable if the absolute value of the difference between the mean RM value and the mean CEMS value is less than or equal to 1.0 percent O2 (or CO2).
Up dated September 14, 2016
40 CFR 60 Performance Specification 6 For Continuous Emission Rate Monitoring Systems (CERMS)
13.2 CERMS Relative Accuracy. The RA of the CERMS shall be no greater than 20 percent of the mean value of the RM's test data in terms of the nits of the emission
standard, or 10 percent of the applicable standard, which err is greater.
Up dated January 17, 2006
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Passed
Clean Harbors Backup CEM RATA RM 1, 2, 3A, 6C, 7E, 10, & 19 (Tested 5-8-2024)
Reference Methods 2, 3A, 6C, 7E, 10, & 19
Source Information
Company Name Clean Harbor cems-#2b
Company Contact:Tyler Lee
Contact Phone No.435-884-8122
Stack Designation:Main Stack
Test & Review Dates
Test Date:5/8/2024
Review Date: 9/27/2024
Observer:Not Observed
Reviewer:Rob Leishman
Emission Limits Emission Rates
SO2 NOX CO SO2 NOX CO
lbs./MMBtu
lbs./hr. 44.2 30.446
ppm 91.0 100.00 0.854 2.933
%O2 Correction as a whole #7.00 7.00
Test Information
Stack I.D. inches
As ft^2 Y Dl H @ Cp Pbar Pq (static)
Ps
Stack Pressure
60.00 19.635 0.9950 13885 0.84 25.32 0.21 25.335441
Contractor Information
Contact:Austin Keough
Contracting Company: Alliance Source Testing
Address: 2855S 500 W Sutie A, Salt Lake City, Utah 84115
Phone No.: [phone]
Project No.:

Division of Air Quality
Instrumental Reference Methods - Gaseous Measurements
Round
Method 19 - F factors for Coal, Oil, and Gas
Fd Fw Fc
dscf/MMBtu wscf/MMBtu scf/MMBtu Diluent
F factor used
O2
CO2
Anthracite 2
Bituminous 2
Lignite
Natural
Propane
Butane
10100
COAL
OIL
GAS
9780
9860
9190
8710
8710
8710
10540
10640
11950
320
10610
10200
10390
1970
1800
1910
1420
1040
1190
1250
Wet CEM
Correct For O2
CO2 Interference w/CO
Yes
Yes
Yes
Clean Harbors Backup CEM RATA RM 1, 2, 3A, 6C, 7E, 10, & 19 (Tested 5-8-2024)
Company Clean Harbor cems-#2b
Point Source Main Stack
Test Date 5/8/24
Start
Time
End
Time Run
O2
%
CO2
%
SO2
PPM
SO2
PPM@7%
O2
NOx
PPM
NOx
lb/hr CO
PPM
CO
PPM@7%
O2
THC
PPM
THC
PPM@7%
O2
Flow
ACFM
Headers
Here
11:28 11:49 1 9.01 9.11 0 0 111.88 25.27 11.78 12.59 61843
11:50 12:11 2 8.53 9.56 0 0 119.99 26.25 2.26 2.41 60905
12:11 12:32 3 8.16 9.66 0.2 0.23 145.56 32.25 0.89 0.97 61882
13:27 13:48 4 8.79 9.25 0 0 140.33 31.43 0.92 1.05 62445
13:48 14:09 5 8.66 9.24 0.01 0.01 132.1 29.91 15.97 16.73 63117
14:09 14:30 6 9.39 8.65 0 0 152 34.06 1.16 1.4 62650
14:59 15:20 7 8.58 9.57 0.03 0.04 153.43 34.17 12.28 12.81 62953
15:20 15:41 8 9.38 8.72 0 0 180.91 41.07 1.18 1.43 96574
15:41 16:02 9 8.92 9.07 0 0 197.97 44.82 1.13 1.31 63639
16:25 16:46 10 8.49 9.47 0.07 0.08 147.3 32.85 13.2 13.36 62827
16:46 17:07 11 9.43 8.88 0 0 134.89 30.72 1.16 1.4 63726
17:07 17:28 12 10.05 8.22 0 0 114.45 26.25 1.19 1.53 63389
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Division of Air Quality
NSPS Relative Accuracy Performance Specification Test - CEMS Certification
Clean Harbor cems-#2b
Main Stack
SO2 Analyzer:Serial No.:
CO2 Analyzer:Serial No.:
Acquisition System:Serial No.:
Acquisition System: Serial No.:
Equivalent Emission Limit:91
Test Date SO2 Dry SO2 Dry SO2 Test Date % CO2 Dry
5/8/2024 RM CEMS Diff RM CEMS Diff RM CEMS Diff 5/8/2024 RM CEMS Diff
Run#Start
Time
End
Time ppm lbs./MMBtu lbs./hr. Run#
Start
Time End Time %c %c
1 11:28 11:49 Y 0.5 0 0.49 0.15 1 11:28 11:49 Y 9.3 9.11 0.17
2 11:50 12:11 Y 0.8 0 0.81 0.24 2 11:50 12:11 Y 9.7 9.56 0.17
3 12:11 12:32 Y 0.7 0.2 0.54 0.22 3 12:11 12:32 Y 9.9 9.66 0.20
4 13:27 13:48 1.6 0 0.48 4 13:27 13:48 9.5 9.25
5 13:48 14:09 2.2 0.01 0.67 5 13:48 14:09 Y 9.5 9.24 0.21
6 14:09 14:30 2.3 0 0.71 6 14:09 14:30 Y 8.9 8.65 0.22
7 14:59 15:20 Y 0.9 0.03 0.82 0.25 7 14:59 15:20 9.8 9.57
8 15:20 15:41 Y 0.2 0 0.24 0.07 8 15:20 15:41 Y 8.9 8.72 0.18
9 15:41 16:02 Y 0.3 0 0.27 0.09 9 15:41 16:02 9.3 9.07
10 16:25 16:46 Y 0.3 0.07 0.18 0.07 10 16:25 16:46 Y 9.7 9.47 0.21
11 16:46 17:07 Y 0.3 0 0.29 0.09 11 16:46 17:07 Y 9.1 8.88 0.19
12 17:07 17:28 Y 0.2 0 0.21 0.06 12 17:07 17:28 Y 8.4 8.22 0.16
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Average = 0.5 0.03 0.43 Average = 9.240 9.050 0.189
Sd Standard Deviation = 0.25 Sd Standard Deviation = Sd Standard Deviation = Sd Standard Deviation = 0.02
Confidence Coefficient = 0.19 Confidence Coefficient = Confidence Coefficient = Confidence Coefficient = 0.016
RA - Relative Accuracy = RA RA RA - Relative Accuracy =2.21%
n = 9 0 0 n = 9 or RA of 1%0.19%
t0.975 = 2.306 t0.975 = 2.306
E.L. Relative Accuracy = 1% 0.68%
a For steam generators;b Average of three samples;9
c Make sure that RM and M data are on a consistent basis either wet or dry.
40 CFR 60 Performance Specification 2 For SO2 and NOx Continuous Emission Monitoring Systems
13.2 Relative accuracy Performance Specification. The RA of the CEMSS must be not greater than 20 percent when RM is used in the denominator of Eq. 2-6
(average emissions during test are greater than 50 percent of the emission standard)or 10 percent when the applicable emission standard is used in the
denominator of Eq. 2-6 (average emissions during test are less than 50 percent of the emission standard).
Up dated January 17, 2006
40 CFR 60 Performance Specification 3 For O2 and CO2 Continuous Emission Monitoring Systems
13.2 CEMS Relative Accuracy Perfromance Specification.
The RA of the CEMS must be no grater than 20 percent of the mean value of the reference method (RM) data. 1 percent O2 or CO2.
The results are also acceptable if the absolute value of the difference between the mean RM value and the mean CEMS value is less than or equal to 1.0 percent O2 (or CO2).
Up dated September 14, 2016
40 CFR 60 Performance Specification 6 For Continuous Emission Rate Monitoring Systems (CERMS)
13.2 CERMS Relative Accuracy. The RA of the CERMS shall be no greater than 20 percent of the mean value of the RM's test data in terms of the nits of the emission
standard, or 10 percent of the applicable standard, which err is greater.
Up dated January 17, 2006
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Servomax - XENTRA 4900 04900 - CL - 652525
04900 - C1-653305 #2bServomaex Model # 4900
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Clean Harbors Backup CEM RATA RM 1, 2, 3A, 6C, 7E, 10, & 19 (Tested 5-8-2024)
Division of Air Quality
Relative Accuracy Test Audit of
Clean Harbor cems-#2b
Main Stack
NOX Analyzer:Serial No.:
O2 Analyzer:Serial No.:
Acquisition System:Serial No.:
Acquisition System: Serial No.:
Equivalent Emission Limit:44.18
Date NOx Dry NOx Dry NOx Test Date % O2 Dry
5/8/2024 RM CEMS Diff RM CEMS Diff RM CEMS Diff 9/30/2014 RM CEMS Diff
Run#Start
Time
End
Time ppm lbs./MMBtu lbs./hr. Run#
Start
Time End Time %c %c
1 11:28 11:49 Y 111.3 111.88 -0.6 Y 24.37 25.27 -0.90 1 11:28 11:49 Y 9.2 9.01 0.173
2 11:50 12:11 Y 116.3 119.99 -3.7 Y 25.02 26.25 -1.23 2 11:50 12:11 Y 8.7 8.53 0.197
3 12:11 12:32 135.7 145.56 29.26 32.25 3 12:11 12:32 Y 8.4 8.16 0.192
4 13:27 13:48 Y 136.5 140.33 -3.8 Y 29.64 31.43 -1.79 4 13:27 13:48 Y 9.0 8.79 0.249
5 13:48 14:09 Y 126.8 132.1 -5.3 Y 27.95 29.91 -1.96 5 13:48 14:09 9.0 8.66
6 14:09 14:30 Y 144.7 152 -7.3 Y 31.84 34.06 -2.22 6 14:09 14:30 Y 9.7 9.39 0.273
7 14:59 15:20 143.8 153.43 30.88 34.17 7 14:59 15:20 Y 8.8 8.58 0.196
8 15:20 15:41 Y 173.3 180.91 -7.7 Y 38.31 41.07 -2.76 8 15:20 15:41 Y 9.6 9.38 0.194
9 15:41 16:02 187.7 197.97 Y 44.49 44.82 -0.33 9 15:41 16:02 Y 9.1 8.92 0.145
10 16:25 16:46 Y 144.1 147.3 -3.2 29.36 32.85 10 16:25 16:46 Y 8.8 8.49 0.276
11 16:46 17:07 Y 132.6 134.89 -2.3 Y 28.58 30.72 -2.14 11 16:46 17:07 9.7 9.43
12 17:07 17:28 Y 115.3 114.45 0.8 Y 25.65 26.25 -0.60 12 17:07 17:28 10.4 10.05
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16 16
Average = 133.4 137.1 3.687 30.65 32.20 1.55 Average = 9.010 8.800 0.210
Sd Standard Deviation = 2.82 Sd Standard Deviation = Sd Standard Deviation = 0.820 Sd Standard Deviation = 0.05
Confidence Coefficient = 2.164 Confidence Coefficient = Confidence Coefficient = 0.631 Confidence Coefficient = 0.034
RA - Relative Accuracy =4.40%Relative Accuracy = Relative Accuracy =7.10%RA - Relative Accuracy =2.70%
n = 9 0 9 n = 9 or RA of 1%0.21%
t0.975 = 2.306 t0.975 = t0.975 = 2.306 t0.975 = 2.306
E.L. Relative Accuracy = EMRA EMRA 69%
a For steam generators;b Average of three samples;
c Make sure that RM and M data are on a consistent basis either wet or dry.
40 CFR 60 Performance Specification 2 For SO2 and NOx Continuous Emission Monitoring Systems
4. Performance and Equipment Specifications
4.3 Relative accuracy. The RA of the CEMSS shall be no grater than 20 percent of the mean value of the RM test data in terms of the
units of the emission standard or 10 percent of the applicable standard, whichever is greater
For SO2 emission standards between 0.30 and 0.20 lbs./MMBtu use 15 Percent of the applicable standard;
For SO2 emission standards below 0.20 lbs./MMBtu use 20 Percent of the emission standard;
40 CFR 60 Performance Specification 3 For O2 and CO2 Continuous Emission Monitoring Systems
12. Calculate the arithmetic difference between the RM and the CEMSS output for each run. The average of the nine (of more) data sets constitute the RA.
13.2 Relative accuracy. The RA of the CEMSS must be no grater than 1 percent O2 or CO2.
40 CFR 60 Performance Specification 6 For Continuous Emission Rate Monitoring Systems (CERMS)
13.2 CERMS Relative Accuracy. The RA of the CERMS shall be no greater than 20 percent of the mean value of the RM's test data in terms of the nits of the emission
standard, or 10 percent of the applicable standard, which err is greater.
Up dated January 17, 2006
614216782 #2bThermo Electron Corp 42i - HL
Servomex - XENTRA 4900 04900 - C1 - 652525 #3
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Clean Harbors Backup CEM RATA RM 1, 2, 3A, 6C, 7E, 10, & 19 (Tested 5-8-2024)
Division of Air Quality
Relative Accuracy Test Audit of
Clean Harbor cems-#2b
Main Stack
CO Analyzer:Serial No.:
Acquisition System:
Acquisition System: Serial No.:
Equivalent Emission Limit:100.00
Date CO Dry CO Dry CO
5/8/2024 RM CEMS Diff RM CEMS Diff RM CEMS Diff
Run#Start
Time
End
Time ppm lbs./MMBtu lbs./hr.
1 11:28 11:49 5.07 11.78 0.68
2 11:50 12:11 Y 2.42 2.26 -0.16 0.32
3 12:11 12:32 Y 1.13 0.89 -0.24 0.15
4 13:27 13:48 Y 1.22 0.92 -0.30 0.16
5 13:48 14:09 5.98 15.97 0.80
6 14:09 14:30 Y 1.40 1.16 -0.24 0.19
7 14:59 15:20 Y 5.86 12.28 6.42 0.77
8 15:20 15:41 Y 1.35 1.18 -0.17 0.18
9 15:41 16:02 Y 1.32 1.13 -0.19 0.19
10 16:25 16:46 6.72 13.2 0.83
11 16:46 17:07 Y 1.31 1.16 -0.15 0.17
12 17:07 17:28 Y 1.41 1.19 -0.22 0.19
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Average = 1.94 2.46 0.53
Sd Standard Deviation = 2.21
Confidence Coefficient = 1.699
RA - Relative Accuracy =
n = 9 0 0
t0.975 = 2.306
E.L. Relative Accuracy = 2%2.23%
a For steam generators;b Average of three samples;
c Make sure that RM and M data are on a consistent basis either wet or dry.
40 CFR 60 Performance Specification 4 For Carbon Monoxide (CO) Continuous Emission Monitoring Systems
applicable emission standard is used to calculate RA.
40 CFR 60 Performance Specification 4A For Carbon Monoxide (CO) Continuous Emission Monitoring Systems
13.2 Relative accuracy. The RA of the CEMSS must be no greater than 10 percent when the average RM value is used to calculate RA, 5 percent when the applicable
emission standard is used to calculate RA, or within 5 ppmv when the RA is calculated as the absolute average difference between the RM and CEMSS plus the 2.5
percent confidence coefficient.
40 CFR 60 Performance Specification 6 For Continuous Emission Rate Monitoring Systems (CERMS)
13.2 CERMS Relative Accuracy. The RA of the CERMS shall be no greater than 20 percent of the mean value of the RM's test data in terms of the nits of the emission
standard, or 10 percent of the applicable standard, which err is greater.
Up dated January 17, 2006
4900 - C1 653305
13.2 Relative accuracy. The RA of the CEMSS must be no grater than 10 percent when the average of the RM value is used to calculate RA or 5 percent when the
Passed
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Servomex XEMTRA 4900