DSHW-2024-006761

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6/14/2024 Relative Accuracy Test Audit (RATA) Report
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Banks, Kenneth <[e-mail]>Fri, Jun 14, 2024 at 11:00 AM
To: Rob Leishman Jr <[e-mail]>, dwmrcsubmit <[e-mail]>
Cc: "Simmons, William L" <[e-mail]>, "Kelley, Jennifer" <[e-mail]>, AG
Compliance <[e-mail]>, Boyd Swenson <[e-mail]>, "[e-mail]"
<[e-mail]>
Good morning and To Whom it May Concern,
Attached is a Relative Accuracy Test Audit (RATA) Final Report for Clean Harbors Aragonite, LLC.
EPA ID #: UTD 981 552 177
Title V Permit #: 4500048004
The RATA was conducted on May 8, 2024. A physical copy of this report is being sent to the Division of Air Quality (FedEx
Tracking # 8182 9436 4252). A physical copy is also being sent to the Environmental Protection Agency, Region VIII.
Thank you.
Safety Starts with Me: Live It 3-6-5
_________________________________
Kenneth Banks
Senior Environmental Compliance Manager
Clean Harbors Aragonite, LLC
(o) 435.884.8233
(c) 435.579.5193
[e-mail]
www.cleanharbors.com
2 attachments
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DSHW-2024-006761
AST 2024-1517 Clean Harbors Aragonite 2024 RATA_F.pdf
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6/14/24, 2:47 PM State of Utah Mail - 6/14/2024 Relative Accuracy Test Audit (RATA) Report
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RATA Report

Clean Harbors Aragonite LLC
11600 N. Aptus Road
Aragonite, UT 84029

Source Tested: Incinerator System (INC)
RATA – O2, CO2, SO2, NOx, CO & THC
Test Date: May 8, 2024

Project No. AST-2024-1517

Prepared By
Alliance Technical Group, LLC
3683 W 2270 S, Suite E
West Valley City, UT 84120

Source Test Report
Test Program Summary

AST-2024-1517 Clean Harbors – Aragonite, UT Page i

Regulatory Information

Permit No. Utah Department of Environmental Quality (DEQ), Division of Air Quality (DAQ)
Title V Operating Permit 4500048004
Regulatory Citations 40 CFR 60, Performance Specifications 2, 3, 4/4A, 6, and 8A

Source Information

Source Name Source ID Target Parameters
Incineration System INC VFR, O2, CO2, SO2, NOx, CO, THC

Contact Information

Test Location Test Company Regulatory Agency
Clean Harbors Aragonite LLC
11600 N. Aptus Road
Aragonite, UT 84029

Manager, Maintenance
Cody Parks
[e-mail]
[phone]
Alliance Technical Group, LLC
3683 W 2270 S, Suite E
West Valley City, UT 84120

Project Manager
Charles Horton
[e-mail]
[phone]

Field Team Leader
Alan Jensen
[e-mail]
[phone]

QA/QC Manager
Kathleen Shonk
[e-mail]
[phone]

Report Reviewer
Ryan Adam
[e-mail]

Utah DAQ
195 North 1950 West
Salt Lake City, UT 84116

Environmental Health Scientist
Rob Leishman Jr.
[e-mail]
[phone]
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Source Test Report
Certification Statement

AST-2024-1517 Clean Harbors – Aragonite, UT Page ii

Alliance Technical Group, LLC (Alliance) has completed the source testing as described in this report. Results
apply only to the source(s) tested and operating condition(s) for the specific test date(s) and time(s) identified within
this report. All results are intended to be considered in their entirety, and Alliance is not responsible for use of less
than the complete test report without written consent. This report shall not be reproduced in full or in part without
written approval from the customer.

To the best of my knowledge and abilities, all information, facts and test data are correct. Data presented in this
report has been checked for completeness and is accurate, error-free and legible. Onsite testing was conducted in
accordance with approved internal Standard Operating Procedures. Any deviations or problems are detailed in the
relevant sections in the test report.

This report is only considered valid once an authorized representative of Alliance has signed in the space provided
below; any other version is considered draft. This document was prepared in portable document format (.pdf) and
contains pages as identified in the bottom footer of this document.

Charles Horton, QSTI
Alliance Technical Group, LLC
Date

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6/13/2024

Source Test Report
Table of Contents

AST-2024-1517 Clean Harbors – Aragonite, UT Page iii

TABLE OF CONTENTS

1.0 Introduction ................................................................................................................................................. 1-1
1.1 Process/Control System Descriptions .......................................................................................................... 1-1
1.2 CEMS Descriptions ..................................................................................................................................... 1-1
1.3 Project Team ............................................................................................................................................... 1-2
1.4 Site Specific Test Plan & Notification ........................................................................................................ 1-2
2.0 Summary of Results .................................................................................................................................... 2-1
3.0 Testing Methodology .................................................................................................................................. 3-1
3.1 U.S. EPA Reference Test Methods 1 and 2 – Sampling/Traverse Points and Volumetric Flow Rate ........ 3-1
3.2 U.S. EPA Reference Test Method 3A – Oxygen/Carbon Dioxide .............................................................. 3-1
3.3 U.S. EPA Reference Test Method 4 – Moisture Content ............................................................................ 3-2
3.4 U.S. EPA Reference Test Method 6C – Sulfur Dioxide .............................................................................. 3-2
3.5 U.S. EPA Reference Test Method 7E – Nitrogen Oxides ........................................................................... 3-2
3.6 U.S. EPA Reference Test Method 10 – Carbon Monoxide ......................................................................... 3-2
3.7 U.S. EPA Reference Test Method 25A – Total Hydrocarbons ................................................................... 3-2
3.8 U.S. EPA Reference Test Method 205 – Gas Dilution System Certification .............................................. 3-3
3.9 Quality Assurance/Quality Control – U.S. EPA Reference Test Methods 3A, 6C, 7E and 10 ................... 3-3
3.10 Quality Assurance/Quality Control – U.S. EPA Reference Test Method 25A ....................................... 3-4

LIST OF TABLES

Table 1-1: Project Team ........................................................................................................................................... 1-2
Table 2-1: Summary of Performance Specification Test Results, O2 ....................................................................... 2-1
Table 2-2: Summary of Performance Specification Test Results, CO2 .................................................................... 2-1
Table 2-3: Summary of Performance Specification Test Results, SO2 ..................................................................... 2-2
Table 2-4: Summary of Performance Specification Test Results, NOx ................................................................... 2-2
Table 2-5: Summary of Performance Specification Test Results, CO ...................................................................... 2-3
Table 2-6: Summary of Performance Specification Test Results, THC ................................................................... 2-3
Table 2-7: Summary of Performance Specification Test Results, VFR ................................................................... 2-4
Table 3-1: Source Testing Methodology .................................................................................................................. 3-1

APPENDICES
Appendix A Sample Calculations
Appendix B Field Data
Appendix C Quality Assurance/Quality Control Data
Appendix D CEMS & CERMS Data

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Introduction

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Introduction

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1.0 Introduction
Alliance Technical Group, LLC (Alliance) was retained by Clean Harbors Aragonite, LLC (Clean Harbors) to
conduct performance specification (PS) testing at the Aragonite, Utah facility. Portions of the facility are subject to
provisions of 40 CFR 60, Appendix B, PS 2, 3, 4A, 6 and 8A and the Utah Department of Environmental Quality
(UDEQ) Title V Operation Permit No. 4500048004. Testing included conducting a relative accuracy test audit
(RATA) to determine the relative accuracy (RA) of the oxygen (O2), carbon dioxide (CO2), sulfur dioxide (SO2),
nitrogen oxides (NOx), carbon monoxide (CO) and total hydrocarbons (THC) primary, secondary and backup
continuous emissions monitoring systems (CEMS) and the volumetric flow rate (VFR) continuous emissions rate
monitoring system (CERMS) serving to monitor emissions from the incineration system (INC).
1.1 Process/Control System Descriptions
The permitted source is a commercial hazardous waste treatment, storage, and disposal facility (TSDF). Hazardous
waste is received from various sources including refineries, chemical manufacturing plants, and coke by-product
recovery plants. The off-site material management unit at the source includes sixteen liquid waste storage and
blending tanks, two sludge tanks, three bulk solids tanks, and several container management buildings. Waste from
the off-site material management unit is treated in an incinerator which includes primary and secondary chambers.
The incinerator control system includes a spray dryer, carbon injection, baghouse, saturator, and wet scrubber.
1.2 CEMS Descriptions
CEMS #1 (Primary)
Parameter: CO CO2 SO2 O2 NOx THC
Make: Servomex Servomex Thermo Thermo
Model: 4900 4900 42i-HL 51i-TH
Serial No.: 653204 4021 0836633949 1203299855
Span: 0-200 ppm (low) 0-20% 0-500 ppm 0-25 % 0-1,000 ppm 0-100 ppm

CEMS #2 (Secondary)
Parameter: CO CO2 SO2 O2 NOx THC
Make: Servomex Servomex Thermo Thermo
Model: 4900 4900 42i-HL 51i-TH
Serial No.: 653305 652525 0614216783 1434964304
Span: 0-200 ppm (low) 0-20 % 0-500 ppm 0-25 % 0-1,000 ppm 0-100 ppm

CEMS #3 (Backup - #2 Spare)
Parameter: CO CO2 SO2 O2 NOx THC
Make: Servomex Servomex Thermo Thermo
Model: 4900 4900 42i-HL 51i-TH
Serial No.: 653205 4022 0614216782 1203299856
Span: 0-200 ppm (low) 0-20% 0-1,000 ppm 0-100 ppm 0-1,000 ppm 0-100 ppm
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Introduction

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VFR FT2195
Parameter: Flow Rate
Make: Rosemount
Model: 3051
Serial No.: 036061752
Span: --
1.3 Project Team
Personnel involved in this project are identified in the following table.

Table 1-1: Project Team

Clean Harbors Personnel Cody Parks
Alliance Personnel
Alan Jensen
Supilani Mailei
Mitchell Manwaring
1.4 Site Specific Test Plan & Notification
Testing was conducted in accordance with the Site-Specific Test Plan (SSTP) submitted to UDAQ by Clean
Harbors.

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Summary of Results

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Summary of Results

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2.0 Summary of Results
Alliance conducted PS testing at the Clean Harbors facility in Aragonite, Utah on May 8, 2024. Testing consisted of
conducting a RATA to determine the RA of the O2, CO2, SO2, NOx, CO, and THC primary, secondary and backup
CEMS and the VFR CERMS serving to monitor emissions from the incineration system (INC).

Tables 2-1 through 2-7 provide summaries of the emission testing results with comparisons to the applicable relative
accuracy requirements. Any difference between the summary results listed in the following tables and the detailed
results contained in appendices is due to rounding for presentation.

Table 2-1: Summary of Performance Specification Test Results, O2

CEMS
Performance Test Data Relative Accuracy
Reference
Method
Data
CEMS
Data
Performance
Required
Performance
Demonstrated
Oxygen Data, AT2200A - 04900-C1-4021
Concentration, % (dry) 9.04 8.91 ≤ 20 % 1.81% 1
Oxygen Data, AT2200B - 04900-C1-4022
Concentration, % (dry) 9.04 8.91 ≤ 20 % 1.87% 1
Oxygen Data, AT2200C - 04900-C1-652525
Concentration, % (dry) 9.04 8.82 ≤ 20 % 2.77% 1
1 Calculated using the mean reference method.

Table 2-2: Summary of Performance Specification Test Results, CO2

CEMS
Performance Test Data Relative Accuracy
Reference
Method
Data
CEMS
Data
Performance
Required
Performance
Demonstrated
Carbon Dioxide Data, AT2198A - 04900-C1-653204
Concentration, % (dry) 9.38 9.39 ≤ 20% 0.34% 1
Carbon Dioxide Data, AT2198B - 04900-C1-653205
Concentration, % (dry) 9.37 9.37 ≤ 20% 0.25% 1
Carbon Dioxide Data, AT2198C - 04900-C1-653305
Concentration, % (dry) 9.25 9.05 ≤ 20% 2.38% 1
1 Calculated using the mean reference method.
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Summary of Results

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Table 2-3: Summary of Performance Specification Test Results, SO2

CEMS
Performance Test Data Relative Accuracy
Reference
Method
Data
CEMS
Data
Performance
Required
Performance
Demonstrated
Sulfur Dioxide Data, AT2208A - 04900-C1-4021
Concentration, ppmvd 0.56 0.70 ≤ 10% 0.63% 1
Concentration, ppmvd @ 7% O2 0.74 0.91 ≤ 10% 0.68% 1
Sulfur Dioxide Data, AT2208B - 04900-C1-4022
Concentration, ppmvd 0.46 0.45 ≤ 10% 0.54% 1
Concentration, ppmvd @ 7% O2 0.54 0.54 ≤ 10% 0.54% 1
Sulfur Dioxide Data, AT2208C - 04900-C1-652525
Concentration, ppmvd 0.46 0.033 ≤ 10% 0.82% 1
Concentration, ppmvd @ 7% O2 0.54 0.039 ≤ 10% 0.81% 1
1 Calculated using the applicable source standard for the pollutant. See Appendix B for the applicable standard used.

Table 2-4: Summary of Performance Specification Test Results, NOx

CEMS
Performance Test Data Relative Accuracy
Reference
Method
Data
CEMS
Data
Performance
Required
Performance
Demonstrated
Nitrogen Oxides Data, AT2202A - 08636633949
Concentration, ppmvd 133.47 139.09 ≤ 20% 5.72% 1
Emission Rate, lb/hr 30.65 32.67 ≤ 20% 8.42% 1
Nitrogen Oxides Data, AT2202B - 0614216783
Concentration, ppmvd 133.47 137.84 ≤ 20% 4.96% 1
Emission Rate, lb/hr 30.65 32.45 ≤ 20% 7.71% 1
Nitrogen Oxides Data, AT2202C - 0614216782
Concentration, ppmvd 133.47 137.09 ≤ 20% 4.31% 1
Emission Rate, lb/hr 30.65 32.20 ≤ 20% 6.97% 1
1 Calculated using the mean reference method.
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Table 2-5: Summary of Performance Specification Test Results, CO

CEMS
Performance Test Data Relative Accuracy
Reference
Method
Data
CEMS
Data
Alternative
Performance
Required
Performance
Demonstrated
Carbon Monoxide Data, AT2199A – 04900-C1-653204
Concentration, ppmvd 1.90 2.06 ≤ 5 ppm 1.81 ppm 1
Concentration, ppmvd @ 7% O2 2.25 2.25 ≤ 5 ppm 1.61 ppm 1
Carbon Monoxide Data, AT2199CL - 04900-C1-653205
Concentration, ppmvd 1.81 2.16 ≤ 5 ppm 2.05 ppm 1
Concentration, ppmvd @ 7% O2 2.35 2.54 ≤ 5 ppm 1.75 ppm 1
Carbon Monoxide Data, AT2199E – 04900-C1-653305
Concentration, ppmvd 1.90 2.46 ≤ 5 ppm 2.25 ppm 1
Concentration, ppmvd @ 7% O2 2.35 2.76 ≤ 5 ppm 1.92 ppm 1
1 Calculated using the average absolute difference plus the confidence coefficient.

Table 2-6: Summary of Performance Specification Test Results, THC

CEMS
Performance Test Data Relative Accuracy
Reference
Method
Data
CEMS
Data
Performance
Required
Performance
Demonstrated
Total Hydrocarbons Data, AT2207A - 1203299856
Concentration, ppmv (wet) 0.16 0.16 ≤ 20 % 3.30% 1
Concentration, ppmvd @ 7% O2 0.27 0.30 ≤ 10 % 3.34% 1
Total Hydrocarbons Data, AT2207B - 1434964304
Concentration, ppmv (wet) 0.16 0.061 ≤ 20 % 4.75% 1
Concentration, ppmvd @ 7% O2 0.27 0.11 ≤ 10 % 4.72% 1
Total Hydrocarbons Data, AT2207C - 1203299855
Concentration, ppmv (wet) 0.16 0.020 ≤ 20 % 5.56% 1
Concentration, ppmvd @ 7% O2 0.27 0.033 ≤ 10 % 5.59% 1
1 Calculated using the applicable source standard for the pollutant. See Appendix B for the applicable standard used.
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Table 2-7: Summary of Performance Specification Test Results, VFR

CERMS
Performance Test Data Relative Accuracy
Reference
Method
Data
CERMS
Data
Performance
Required
Performance
Demonstrated
Volumetric Flow Rate
High Load Flow Rate, acfm 59,077 62,605 ≤ 20 % 7.52% 1
1 Calculated using the mean reference method.

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Testing Methodology

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Source Test Report
Testing Methodology

AST-2024-1517 Clean Harbors – Aragonite, UT Page 3-1

3.0 Testing Methodology
The emission testing program was conducted in accordance with the test methods listed in Table 3-1. Method
descriptions are provided below while quality assurance/quality control data is provided in Appendix C.

Table 3-1: Source Testing Methodology

Parameter U.S. EPA Reference
Test Methods Notes/Remarks
Volumetric Flow Rate 1 & 2 Full Velocity Traverses
Oxygen / Carbon Dioxide 3A Instrumental Analysis
Moisture Content 4 Gravimetric Analysis
Sulfur Dioxide 6C Instrumental Analysis
Nitrogen Oxides 7E Instrumental Analysis
Carbon Monoxide 10 Instrumental Analysis
Total Hydrocarbons 25A Instrumental Analysis
Gas Dilution System Certification 205 --
3.1 U.S. EPA Reference Test Methods 1 and 2 – Sampling/Traverse Points and Volumetric Flow Rate
The sampling location and number of traverse (sampling) points were selected in accordance with U.S. EPA
Reference Test Method 1. To determine the minimum number of traverse points, the upstream and downstream
distances were equated into equivalent diameters and compared to Figure 1-2 in U.S. EPA Reference Test Method 1.

Full velocity traverses were conducted in accordance with U.S. EPA Reference Test Method 2 to determine the
average stack gas velocity pressure, static pressure and temperature. The velocity and static pressure measurement
system consisted of a pitot tube and inclined manometer. The stack gas temperature was measured with a K-type
thermocouple and pyrometer.

Stack gas velocity pressure and temperature readings were recorded during each test run. The data collected was
utilized to calculate the volumetric flow rate for comparison to the continuous emission rate monitoring system
(CERMS). The relative accuracy of the CERMS was determined based on procedures found in 40 CFR 60,
Performance Specification 6.
3.2 U.S. EPA Reference Test Method 3A – Oxygen/Carbon Dioxide
The oxygen (O2) and carbon dioxide (CO2) testing was conducted in accordance with U.S. EPA Reference Test
Method 3A. Data was collected online and reported in one-minute averages. The sampling system consisted of a
stainless-steel probe, Teflon sample line(s), gas conditioning system and the identified gas analyzer. The gas
conditioning system was a non-contact condenser used to remove moisture from the stack gas. If an unheated
Teflon sample line was used, then a portable non-contact condenser was placed in the system directly after the
probe. Otherwise, a heated Teflon sample line was used. The quality control measures are described in Section 3.9.

The relative accuracy of the O2 and CO2 CEMS was determined based on procedures found in 40 CFR 60,
Performance Specification 3.
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3.3 U.S. EPA Reference Test Method 4 – Moisture Content
The stack gas moisture content (BWS) was determined in accordance with U.S. EPA Reference Test Method 4. The
gas conditioning train consisted of a series of chilled impingers. Prior to testing, each impinger was filled with a
known quantity of water or silica gel. Each impinger was analyzed gravimetrically before and after each test run on
the same balance to determine the amount of moisture condensed.
3.4 U.S. EPA Reference Test Method 6C – Sulfur Dioxide
The sulfur dioxide (SO2) testing was conducted in accordance with U.S. EPA Reference Test Method 6C. Data was
collected online and reported in one-minute averages. The sampling system consisted of a heated stainless steel
probe, Teflon sample line(s), gas conditioning system and the identified analyzer. The gas conditioning system was
a non-contact condenser used to remove moisture from the source gas. If an unheated Teflon sample line was used,
then a portable non-contact condenser was placed in the system directly after the probe. Otherwise, a heated Teflon
sample line was used. The quality control measures are described in Section 3.9.

The relative accuracy of the SO2 CEMS was determined based on procedures found in 40 CFR 60, Performance
Specification 2.
3.5 U.S. EPA Reference Test Method 7E – Nitrogen Oxides
The nitrogen oxides (NOx) testing was conducted in accordance with U.S. EPA Reference Test Method 7E. Data
was collected online and reported in one-minute averages. The sampling system consisted of a stainless-steel probe,
Teflon sample line(s), gas conditioning system and the identified gas analyzer. The gas conditioning system was a
non-contact condenser used to remove moisture from the stack gas. If an unheated Teflon sample line was used,
then a portable non-contact condenser was placed in the system directly after the probe. Otherwise, a heated Teflon
sample line was used. The quality control measures are described in Section 3.9.

The relative accuracy of the NOx CEMS was determined based on procedures found in 40 CFR 60, Performance
Specification 2.
3.6 U.S. EPA Reference Test Method 10 – Carbon Monoxide
The carbon monoxide (CO) testing was conducted in accordance with U.S. EPA Reference Test Method 10. Data
was collected online and reported in one-minute averages. The sampling system consisted of a stainless-steel probe,
Teflon sample line(s), gas conditioning system, and the identified gas analyzer. The gas conditioning system was a
non-contact condenser used to remove moisture from the gas. If an unheated Teflon sample line was used, then a
portable non-contact condenser was placed in the system directly after the probe. Otherwise, a heated Teflon sample
line was used. The quality control measures are described in Section 3.9.

The relative accuracy of the CO CEMS was determined based on procedures found in 40 CFR 60, Performance
Specification 4A.
3.7 U.S. EPA Reference Test Method 25A – Total Hydrocarbons
The total hydrocarbons (THC) testing was conducted in accordance with U.S. EPA Reference Test Method 25A. Data
was collected online and reported in one-minute averages. The sampling system consisted of a stainless-steel probe,
heated Teflon sample line(s) and the identified gas analyzer. The quality control measures are described in Section 3.10.

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The relative accuracy of the THC CEMS was determined based on procedures found in 40 CFR 60, Performance
Specification 8A.
3.8 U.S. EPA Reference Test Method 205 – Gas Dilution System Certification
A calibration gas dilution system field check was conducted in accordance with U.S. EPA Reference Method 205.
Multiple dilution rates and total gas flow rates were utilized to force the dilution system to perform two dilutions on
each mass flow controller. The diluted calibration gases were sent directly to the analyzer, and the analyzer response
recorded in an electronic field data sheet. The analyzer response agreed within 2% of the actual diluted gas
concentration. A second Protocol 1 calibration gas, with a cylinder concentration within 10% of one of the gas
divider settings described above, was introduced directly to the analyzer, and the analyzer response recorded in an
electronic field data sheet. The cylinder concentration and the analyzer response agreed within 2%. These steps
were repeated three (3) times. Copies of the Method 205 data can be found in the Quality Assurance/Quality
Control Appendix.
3.9 Quality Assurance/Quality Control – U.S. EPA Reference Test Methods 3A, 6C, 7E and 10
Cylinder calibration gases used met EPA Protocol 1 (+/- 2%) standards. Copies of all calibration gas certificates can
be found in the Quality Assurance/Quality Control Appendix.

Low Level gas was introduced directly to the analyzer. After adjusting the analyzer to the Low-Level gas
concentration and once the analyzer reading was stable, the analyzer value was recorded. This process was repeated
for the High-Level gas. For the Calibration Error Test, Low, Mid, and High Level calibration gases were
sequentially introduced directly to the analyzer. All values were within 2.0 percent of the Calibration Span or 0.5
ppmv/% absolute difference.

High or Mid Level gas (whichever was closer to the stack gas concentration) was introduced at the probe and the
time required for the analyzer reading to reach 95 percent or 0.5 ppmv/% (whichever was less restrictive) of the gas
concentration was recorded. The analyzer reading was observed until it reached a stable value, and this value was
recorded. Next, Low Level gas was introduced at the probe and the time required for the analyzer reading to
decrease to a value within 5.0 percent or 0.5 ppmv/% (whichever was less restrictive) was recorded. If the Low-
Level gas was zero gas, the response was 0.5 ppmv/% or 5.0 percent of the upscale gas concentration (whichever
was less restrictive). The analyzer reading was observed until it reached a stable value and this value was recorded.
The measurement system response time and initial system bias were determined from these data. The System Bias
was within 5.0 percent of the Calibration Span or 0.5 ppmv/% absolute difference.

High or Mid Level gas (whichever was closer to the stack gas concentration) was introduced at the probe. After the
analyzer response was stable, the value was recorded. Next, Low Level gas was introduced at the probe, and the
analyzer value recorded once it reached a stable response. The System Bias was within 5.0 percent of the
Calibration Span or 0.5 ppmv/% absolute difference or the data was invalidated and the Calibration Error Test and
System Bias were repeated.

Drift between pre- and post-run System Bias was within 3 percent of the Calibration Span or 0.5 ppmv/% absolute
difference. If the drift exceeded 3 percent or 0.5 ppmv/%, the Calibration Error Test and System Bias were repeated.

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An NO2 – NO converter check was performed on the analyzer prior to initiating testing. An approximately 50 ppm
nitrogen dioxide cylinder gas was introduced directly to the NOx analyzer and the instrument response was recorded
in an electronic data sheet. The instrument response was within +/- 10 percent of the cylinder concentration.

A Data Acquisition System with battery backup was used to record the instrument response in one (1) minute
averages. The data was continuously stored as a *.CSV file in Excel format on the hard drive of a computer. At the
completion of testing, the data was also saved to the Alliance server. All data was reviewed by the Field Team
Leader before leaving the facility. Once arriving at Alliance’s office, all written and electronic data was
relinquished to the report coordinator and then a final review was performed by the Project Manager.
3.10 Quality Assurance/Quality Control – U.S. EPA Reference Test Method 25A
Cylinder calibration gases used met EPA Protocol 1 (+/- 2%) standards. Copies of all calibration gas certificates can
be found in the Quality Assurance/Quality Control Appendix.

Within two (2) hours prior to testing, zero gas was introduced through the sampling system to the analyzer. After
adjusting the analyzer to the Zero gas concentration and once the analyzer reading was stable, the analyzer value
was recorded. This process was repeated for the High-Level gas, and the time required for the analyzer reading to
reach 95 percent of the gas concentration was recorded to determine the response time. Next, Low and Mid-Level
gases were introduced through the sampling system to the analyzer, and the response was recorded when it was
stable. All values were less than +/- 5 percent of the calibration gas concentrations.

Mid Level gas was introduced through the sampling system. After the analyzer response was stable, the value was
recorded. Next, Zero gas was introduced through the sampling system, and the analyzer value recorded once it
reached a stable response. The Analyzer Drift was less than +/- 3 percent of the span value.

A Data Acquisition System with battery backup was used to record the instrument response in one (1) minute
averages. The data was continuously stored as a *.CSV file in Excel format on the hard drive of a computer. At the
completion of testing, the data was also saved to the Alliance server. All data was reviewed by the Field Team
Leader before leaving the facility. Once arriving at Alliance’s office, all written and electronic data was
relinquished to the report coordinator and then a final review was performed by the Project Manager.
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Appendix A

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Location
Source
Project No.
Run No.
Parameter(s)
Meter Pressure (Pm), in. Hg
where,
Pb 25.32 = barometric pressure, in. Hg
ΔH 1.100 = pressure differential of orifice, in H2O
Pm 25.40 = in. Hg
Absolute Stack Gas Pressure (Ps), in. Hg
where,
Pb 25.32 = barometric pressure, in. Hg
Pg 0.21 = static pressure, in. H2O
Ps 25.34 = in. Hg
Standard Meter Volume (Vmstd), dscf
where,
Y 0.995 = meter correction factor
Vm 39.210 = meter volume, cf
Pm 25.40 = absolute meter pressure, in. Hg
Tm 509.3 = absolute meter temperature, °R
Vmstd 34.315 = dscf
Standard Wet Volume (Vwstd), scf
where,
Vlc 298.6 = Volume of H2O collected, ml
Vwstd 14.052 = scf
Moisture Fraction (BWSsat), dimensionless (theoretical at saturated conditions)
where,
Ts 151.3 = stack temperature, °F
Ps 25.3 = absolute stack gas pressure, in. Hg
BWSsat 0.3 = dimensionless
Moisture Fraction (BWS), dimensionless
where,
Vwstd 14.052 = standard wet volume, scf
Vmstd 34.315 = standard meter volume, dscf
BWS 0.291 = dimensionless
Moisture Fraction (BWS), dimensionless
where,
BWSsat 0.305 = moisture fraction (theoretical at saturated conditions)
BWSmsd 0.291 = moisture fraction (measured)
BWS 0.291
Molecular Weight (DRY) (Md), lb/lb-mole
where,
CO2 9.3 = carbon dioxide concentration, %
O2 9.2 = oxygen concentration, %
Md 29.85 = lb/lb mol
Molecular Weight (WET) (Ms), lb/lb-mole
where,
Md 29.85 = molecular weight (DRY), lb/lb mol
BWS 0.291 = moisture fraction, dimensionless
Ms 26.41 = lb/lb mol
Vmstd =17.636 x Vm x Pm x Y
Tm
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
1
AJE
Vwstd = 0.04706 x Vlc
BWS =
Vwstd
(Vwstd +Vmstd)
Ms = Md (1 − BWS) + 18.015 (BWS)
Md = (0.44 × % COଶ) + (0.32 × % O2) + (0.28 (100 − % COଶ − % O2))
BWS = BWSmsd unless BWSsat <BWSmsd
BWSsat = 10଺.ଷ଻ି ଶ,଼ଶ଻
୘ୱାଷ଺
Ps
Ps = Pb +
Pg
13.6
Pm = Pb +
Δ H
13.6
Appendix A
Example Calculations
19 of 135
Location
Source
Project No.
Run No.
Parameter(s)
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
1
AJE
Average Velocity (Vs), ft/sec
where,
Cp 0.84 = pitot tube coefficient
Δ P1/2 0.727 = average pre/post test velocity head of stack gas, (in. H2O)1/2
Ts 610.9 = average pre/post test absolute stack temperature, °R
Ps 25.34 = absolute stack gas pressure, in. Hg
Ms 26.41 = molecular weight of stack gas, lb/lb mol
Vs 49.9 = ft/sec
Average Stack Gas Flow at Stack Conditions (Qa), acfm
where,
Vs 49.9 = stack gas velocity, ft/sec
As 19.63 = cross-sectional area of stack, ft2
Qa 58,763 = acfm
Average Stack Gas Flow at Standard Conditions (Qs), dscfm
Ps
Ts
where,
Qa 58,763 = average stack gas flow at stack conditions, acfm
BWS 0.291 = moisture fraction, dimensionless
Ps 25.34 = absolute stack gas pressure, in. Hg
Ts 610.9 = average pre/post test absolute stack temperature, °R
Qs 30,491 = dscfm
Dry Gas Meter Calibration Check (Yqa), dimensionless
where,
Y 0.995 = meter correction factor, dimensionless
Θ 63 = run time, min.
Vm 39.21 = total meter volume, dcf
Tm 509.3 = absolute meter temperature, °R
ΔH@ 1.853 = orifice meter calibration coefficient, in. H2O
Pb 25.32 = barometric pressure, in. Hg
ΔH avg 1.100 = average pressure differential of orifice, in H2O
Md 29.89 = molecular weight (DRY), lb/lb mol
(Δ H)1/2 1.049 = average square root pressure differential of orifice, (in. H2O)1/2
Yqa 2.0 = dimensionless
Qsd = 17.636 x Qa x (1 - BWS) x
Vs = 85.49 × Cp × (Δ P
ଵ/ଶ ) avg × Ts
Ps x Ms
Qa = 60 × Vs × As
Yqa =
Y −
Θ
Vm
0.0319 × Tm× 29
ΔH@ × Pb + Δ Havg.
13.6 × Md
ΔH avg.
Y × 100
Appendix A
Example Calculations
20 of 135
Location:
Source:
Project No.:
Run No. /Method
O₂ - Outlet Concentration (CO₂), % dry
CMA
( CM - C0 )
where,
Cobs 9.09 = average analyzer value during test, % dry
Co -0.04 = average of pretest & posttest zero responses, % dry
CMA 10.99 = actual concentration of calibration gas, % dry
CM 10.88 = average of pretest & posttest calibration responses, % dry
CO₂9.19 = O₂ Concentration, % dry
CO₂ = ( Cobs - C0 ) x
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run 1 / Method 3A

CO₂ - Outlet Concentration (CCO₂), % dry
C M A
( C M - C 0 )
where,
Cobs 9.09
Co 0.06
CMA 11.10
CM 10.86
CCO₂9.28
= average analyzer value during test, % dry
= average of pretest & posttest zero responses, % dry
= actual concentration of calibration gas, % dry
= average of pretest & posttest calibration responses, % dry
= CO₂ Concentration, % dry
CCO₂ = ( Cobs - C0 ) x
Appendix A
Example Calculations
21 of 135
Location:
Source:
Project No.:
Run No. /Method
CO - Outlet Concentration (CCO), ppmvd
CMA
( CM - C0 )
where,
Cobs 5.02 = average analyzer value during test, ppmvd
Co -0.05 = average of pretest & posttest zero responses, ppmvd
CMA 25.00 = actual concentration of calibration gas, ppmvd
CM 24.94 = average of pretest & posttest calibration responses, ppmvd
CCO 5.07 = CO Concentration, ppmvd
CO - Outlet Concentration (CCOc7), ppmvd @ 7% O₂
20.9 - 7
20.9 - O₂
where,
CCO 5.07 = CO - Outlet Concentration, ppmvd
CO₂9.19 = oxygen concentration, %
CCOc7 6.03 = ppmvd @7% O₂
CO - Outlet Emission Rate (ERCO), lb/hr
where,
CCO 5.07 = CO - Outlet Concentration, ppmvd
MW 28.01 = CO molecular weight, g/g-mole
Qs 30,491 = stack gas volumetric flow rate at standard conditions, dscfm
ERCO 0.68 = lb/hr
ERCO =CCO x MW x Qs x 60 x 28.32
24.04 x 1.0E06 x 453.592
CCOc7 = CCO x
CCO = ( Cobs - C0 ) x
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run 1 / Method 10

𝑚𝑖𝑛
ℎ𝑟
𝐿
𝑓𝑡ଷ
𝐿
𝑔−𝑚𝑜𝑙𝑒
𝑔
𝑙𝑏
Appendix A
Example Calculations
22 of 135
Location:
Source:
Project No.:
Run No. /Method
NOx - Outlet Concentration (CNOx), ppmvd
CMA
( CM - C0 )
where,
Cobs 109.49 = average analyzer value during test, ppmvd
Co 0.39 = average of pretest & posttest zero responses, ppmvd
CMA 250.00 = actual concentration of calibration gas, ppmvd
CM 245.57 = average of pretest & posttest calibration responses, ppmvd
CNOx 111.24 = NOx Concentration, ppmvd
NOx - Outlet Concentration (CNOxc7), ppmvd @ 7% O₂
20.9 - 7
20.9 - O₂
where,
CNOx 111.24 = NOx - Outlet Concentration, ppmvd
CO₂9.19 = oxygen concentration, %
CNOxc7 132.09 = ppmvd @7% O₂
NOx - Outlet Emission Rate (ERNOx), lb/hr
where,
CNOx 111.24 = NOx - Outlet Concentration, ppmvd
MW 46.0055 = NOx molecular weight, g/g-mole
Qs 30,491 = stack gas volumetric flow rate at standard conditions, dscfm
ERNOx 24.32 = lb/hr
ERNOx =CNOx x MW x Qs x 60 x 28.32
24.04 x 1.0E06 x 453.592
CNOxc7 = CNOx x
CNOx = ( Cobs - C0 ) x
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run 1 / Method 7E

𝑚𝑖𝑛
ℎ𝑟
𝐿
𝑓𝑡ଷ
𝐿
𝑔−𝑚𝑜𝑙𝑒
𝑔
𝑙𝑏
Appendix A
Example Calculations
23 of 135
Location:
Source:
Project No.:
Run No. /Method
SO₂ - Outlet Concentration (CSO₂), ppmvd
CMA
( CM - C0 )
where,
Cobs 0.53 = average analyzer value during test, ppmvd
Co 0.05 = average of pretest & posttest zero responses, ppmvd
CMA 10.00 = actual concentration of calibration gas, ppmvd
CM 10.02 = average of pretest & posttest calibration responses, ppmvd
CSO₂0.49 = SO₂ Concentration, ppmvd
SO₂ - Outlet Concentration (CSO₂c7), ppmvd @ 7% O₂
20.9 - 7
20.9 - O₂
where,
CSO₂0.49 = SO₂ - Outlet Concentration, ppmvd
CO₂9.19 = oxygen concentration, %
CSO₂c7 0.58 = ppmvd @7% O₂
SO₂ - Outlet Emission Rate (ERSO₂), lb/hr
where,
CSO₂0.49 = SO₂ - Outlet Concentration, ppmvd
MW 64.066 = SO₂ molecular weight, g/g-mole
Qs 30,491 = stack gas volumetric flow rate at standard conditions, dscfm
ERSO₂0.15 = lb/hr
ERSO₂ =CSO₂ x MW x Qs x 60 x 28.32
24.04 x 1.0E06 x 453.592
CSO₂c7 = CSO₂ x
CSO₂ = ( Cobs - C0 ) x
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run 1 / Method 6C

𝑚𝑖𝑛
ℎ𝑟
𝐿
𝑓𝑡ଷ
𝐿
𝑔−𝑚𝑜𝑙𝑒
𝑔
𝑙𝑏
Appendix A
Example Calculations
24 of 135
Location:
Source:
Project No.:
Run No. /Method
THC - Outlet Concentration (as C3H8) (CTHC), ppmvd
CTHCw
1 - BWS
where,
CTHCw 1.30 = THC - Outlet Concentration (as C3H8), ppmvw
BWS 0.291 = moisture fraction, unitless
CTHC 1.83 = ppmvd
THC - Outlet Concentration (as C3H8) (CTHCw), ppmvw
where,
CTHC 1.83 = THC - Outlet Concentration (as C3H8), ppmvd
BWS 0.29 = moisture fraction, unitless
CTHCw 1.30 = ppmvw
THC - Outlet Concentration (as C3H8) (CTHCc7), ppmvd @ 7% O₂
20.9 - 7
20.9 - O₂
where,
CTHC 1.83 = THC - Outlet Concentration (as C3H8), ppmvd
CO₂9.19 = oxygen concentration, %
CTHCc7 2.17 = ppmvd @7% O₂
THC - Outlet Emission Rate (as C3H8) (ERTHC), lb/hr
where,
CTHC 1.83 = THC - Outlet Concentration (as C3H8), ppmvd
MW 44.1 = THC molecular weight, g/g-mole
Qs 30,491 = stack gas volumetric flow rate at standard conditions, dscfm
ERTHC 0.38 = lb/hr
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run 1 / Method 25A
CTHC =
CTHCw = CTHC x (1 - BWS)
CTHCc7 = CTHC x
ERTHC =CTHC x MW x Qs x 60 x 28.32
24.04 x 1.0E06 x 454

𝑚𝑖𝑛
ℎ𝑟
𝐿
𝑓𝑡ଷ
𝐿
𝑔−𝑚𝑜𝑙𝑒
𝑔
𝑙𝑏
Appendix A
Example Calculations
25 of 135
Appendix B
26 of 135
O2 Summary
Location:
Source:
Project No.:
Reference Method CEMS - Primary Average
O₂ Concentration O₂ Concentration Difference
Start End % dry % dry % dry
1 5/8/24 11:28 11:49 9.19 9.09 0.10
2 5/8/24 11:50 12:10 8.67 8.62 0.05
3 5/8/24 12:11 12:31 8.31 8.21 0.10
4 5/8/24 13:27 13:47 9.05 8.87 0.18
5 5/8/24 13:48 14:08 8.93 8.77 0.16
6 5/8/24 14:09 14:29 9.63 9.46 0.17
7 5/8/24 14:59 15:19 8.79 8.68 0.11
8 5/8/24 15:20 15:40 9.64 9.47 0.17
9 5/8/24 15:41 16:01 9.13 8.99 0.14
10 5/8/24 16:25 16:45 * 8.77 8.56
11 5/8/24 16:46 17:06 * 9.73 9.52
12 5/8/24 17:07 17:27 * 10.38 10.11
9.04 8.91 0.13
0.044
0.034
1.81 %
RA ≤ 20%
PS 3
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.044 = standard deviation of difference
CC 0.034 = confidence coefficient
Relative Accuracy, RA
where,
d 0.13 = average difference of Reference Method and CEMS
CC 0.034 = confidence coefficient
RM 9.036 = reference method, % dry
RA 1.81 = relative accuracy, %
Relative Accuracy (RA)
Performance Required - Mean Reference Method
Performance Specification Method
* Delimiter for runs not used in RA calculations
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
27 of 135
O2 Summary
Location:
Source:
Project No.:
Reference Method CEMS - Secondary Average
O₂ Concentration O₂ Concentration Difference
Start End % dry % dry % dry
1 5/8/24 11:28 11:49 9.19 9.10 0.09
2 5/8/24 11:50 12:10 8.67 8.64 0.03
3 5/8/24 12:11 12:31 8.31 8.24 0.07
4 5/8/24 13:27 13:47 9.05 8.84 0.21
5 5/8/24 13:48 14:08 8.93 8.82 0.11
6 5/8/24 14:09 14:29 9.63 9.46 0.17
7 5/8/24 14:59 15:19 8.79 8.65 0.14
8 5/8/24 15:20 15:40 9.64 9.49 0.15
9 5/8/24 15:41 16:01 9.13 8.96 0.17
10 5/8/24 16:25 16:45 * 8.77 8.52
11 5/8/24 16:46 17:06 * 9.73 9.50
12 5/8/24 17:07 17:27 * 10.38 10.09
9.04 8.91 0.13
0.057
0.044
1.87 %
RA ≤ 20%
PS 3
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.057 = standard deviation of difference
CC 0.044 = confidence coefficient
Relative Accuracy, RA
where,
d 0.13 = average difference of Reference Method and CEMS
CC 0.044 = confidence coefficient
RM 9.036 = reference method, % dry
RA 1.87 = relative accuracy, %
* Delimiter for runs not used in RA calculations
Relative Accuracy (RA)
Performance Required - Mean Reference Method
Performance Specification Method
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
28 of 135
O2 Summary
Location:
Source:
Project No.:
Reference Method CEMS - Backup Average
O₂ Concentration O₂ Concentration Difference
Start End % dry % dry % dry
1 5/8/24 11:28 11:49 9.19 9.01 0.18
2 5/8/24 11:50 12:10 8.67 8.53 0.14
3 5/8/24 12:11 12:31 8.31 8.13 0.18
4 5/8/24 13:27 13:47 9.05 8.79 0.26
5 5/8/24 13:48 14:08 8.93 8.66 0.27
6 5/8/24 14:09 14:29 9.63 9.39 0.24
7 5/8/24 14:59 15:19 8.79 8.58 0.21
8 5/8/24 15:20 15:40 9.64 9.38 0.26
9 5/8/24 15:41 16:01 9.13 8.92 0.21
10 5/8/24 16:25 16:45 * 8.77 8.49
11 5/8/24 16:46 17:06 * 9.73 9.43
12 5/8/24 17:07 17:27 * 10.38 10.05
9.04 8.82 0.22
0.045
0.035
2.77 %
RA ≤ 20%
PS 3
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.045 = standard deviation of difference
CC 0.035 = confidence coefficient
Relative Accuracy, RA
where,
d 0.22 = average difference of Reference Method and CEMS
CC 0.035 = confidence coefficient
RM 9.036 = reference method, % dry
RA 2.77 = relative accuracy, %
* Delimiter for runs not used in RA calculations
Relative Accuracy (RA)
Performance Required - Mean Reference Method
Performance Specification Method
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
29 of 135
CO2 Summary
Location:
Source:
Project No.:
Reference Method CEMS - Primary Average
CO₂ Concentration CO₂ Concentration Difference
Start End % dry % dry % dry
1 5/8/24 11:28 11:49 * 9.28 9.37
2 5/8/24 11:50 12:10 9.77 9.79 -0.02
3 5/8/24 12:11 12:31 * 9.91 9.84
4 5/8/24 13:27 13:47 9.48 9.49 -0.01
5 5/8/24 13:48 14:08 9.47 9.47 0.00
6 5/8/24 14:09 14:29 8.88 8.89 -0.01
7 5/8/24 14:59 15:19 9.78 9.80 -0.02
8 5/8/24 15:20 15:40 8.92 8.96 -0.04
9 5/8/24 15:41 16:01 9.32 9.32 0.00
10 5/8/24 16:25 16:45 9.68 9.69 -0.01
11 5/8/24 16:46 17:06 9.08 9.13 -0.05
12 5/8/24 17:07 17:27 * 8.38 8.48
9.38 9.39 -0.02
0.018
0.014
0.34 %
RA ≤ 20%
PS 3
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.018 = standard deviation of difference
CC 0.014 = confidence coefficient
Relative Accuracy, RA
where,
d -0.02 = average difference of Reference Method and CEMS
CC 0.014 = confidence coefficient
RM 9.375 = reference method, % dry
RA 0.34 = relative accuracy, %
Relative Accuracy (RA)
Performance Required - Mean Reference Method
Performance Specification Method
* Delimiter for runs not used in RA calculations
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
30 of 135
CO2 Summary
Location:
Source:
Project No.:
Reference Method CEMS - Secondary Average
CO₂ Concentration CO₂ Concentration Difference
Start End % dry % dry % dry
1 5/8/24 11:28 11:49 9.28 9.31 -0.03
2 5/8/24 11:50 12:10 9.77 9.74 0.03
3 5/8/24 12:11 12:31 * 9.91 9.85
4 5/8/24 13:27 13:47 9.48 9.46 0.02
5 5/8/24 13:48 14:08 9.47 9.43 0.04
6 5/8/24 14:09 14:29 8.88 8.87 0.01
7 5/8/24 14:59 15:19 9.78 9.77 0.01
8 5/8/24 15:20 15:40 8.92 8.94 -0.02
9 5/8/24 15:41 16:01 * 9.32 9.28
10 5/8/24 16:25 16:45 9.68 9.68 0.00
11 5/8/24 16:46 17:06 9.08 9.10 -0.02
12 5/8/24 17:07 17:27 * 8.38 8.47
9.37 9.37 0.00
0.024
0.019
0.25 %
RA ≤ 20%
PS 3
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.024 = standard deviation of difference
CC 0.019 = confidence coefficient
Relative Accuracy, RA
where,
d 0.00 = average difference of Reference Method and CEMS
CC 0.019 = confidence coefficient
RM 9.371 = reference method, % dry
RA 0.25 = relative accuracy, %
* Delimiter for runs not used in RA calculations
Relative Accuracy (RA)
Performance Required - Mean Reference Method
Performance Specification Method
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
31 of 135
CO2 Summary
Location:
Source:
Project No.:
Reference Method CEMS - Backup Average
CO₂ Concentration CO₂ Concentration Difference
Start End % dry % dry % dry
1 5/8/24 11:28 11:49 9.28 9.11 0.17
2 5/8/24 11:50 12:10 9.77 9.56 0.21
3 5/8/24 12:11 12:31 * 9.91 9.66
4 5/8/24 13:27 13:47 * 9.48 9.25
5 5/8/24 13:48 14:08 9.47 9.24 0.23
6 5/8/24 14:09 14:29 8.88 8.65 0.23
7 5/8/24 14:59 15:19 9.78 9.57 0.21
8 5/8/24 15:20 15:40 8.92 8.72 0.20
9 5/8/24 15:41 16:01 * 9.32 9.07
10 5/8/24 16:25 16:45 9.68 9.47 0.21
11 5/8/24 16:46 17:06 9.08 8.88 0.20
12 5/8/24 17:07 17:27 8.38 8.22 0.16
9.25 9.05 0.20
0.023
0.018
2.38 %
RA ≤ 20%
PS 3
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.023 = standard deviation of difference
CC 0.018 = confidence coefficient
Relative Accuracy, RA
where,
d 0.20 = average difference of Reference Method and CEMS
CC 0.018 = confidence coefficient
RM 9.249 = reference method, % dry
RA 2.38 = relative accuracy, %
* Delimiter for runs not used in RA calculations
Relative Accuracy (RA)
Performance Required - Mean Reference Method
Performance Specification Method
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
32 of 135
SO2 Summary
Location:
Source:
Project No.:
Reference Method CEMS - Primary Average
SO₂ Concentration SO₂ Concentration Difference
Start End ppmvd ppmvd ppmvd
1 5/8/24 11:28 11:49 0.49 1.02 -0.53
2 5/8/24 11:50 12:10 0.82 0.62 0.20
3 5/8/24 12:11 12:31 * 0.76 1.59
4 5/8/24 13:27 13:47 1.61 0.87 0.74
5 5/8/24 13:48 14:08 * 2.15 1.06
6 5/8/24 14:09 14:29 * 2.27 0.66
7 5/8/24 14:59 15:19 0.85 0.68 0.17
8 5/8/24 15:20 15:40 0.39 0.50 -0.11
9 5/8/24 15:41 16:01 0.43 0.54 -0.11
10 5/8/24 16:25 16:45 0.25 0.50 -0.25
11 5/8/24 16:46 17:06 0.13 0.73 -0.60
12 5/8/24 17:07 17:27 0.05 0.81 -0.76
0.56 0.70 -0.14
0.469
78.46
0.360
0.63 %
RA ≤ 10%
PS 2
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.469 = standard deviation of difference
CC 0.360 = confidence coefficient
Relative Accuracy, RA
where,
d -0.14 = average difference of Reference Method and CEMS
CC 0.360 = confidence coefficient
AS 78.460 = applicable source standard, ppmvd
RA 0.63 = relative accuracy, %
Relative Accuracy (RA)
Performance Required - Applicable Source Standard
Performance Specification Method
* Delimiter for runs not used in RA calculations
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Applicable Source Standard (AS)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
33 of 135
SO2 Summary
Location:
Source:
Project No.:
Reference Method CEMS - Primary Average
SO₂ Concentration SO₂ Concentration Difference
Start End ppmvd @ 7 % O₂ ppmvd @ 7 % O₂ ppmvd @ 7 % O₂
1 5/8/24 11:28 11:49 0.58 1.27 -0.69
2 5/8/24 11:50 12:10 0.94 0.67 0.27
3 5/8/24 12:11 12:31 0.84 1.78 -0.94
4 5/8/24 13:27 13:47 1.89 0.99 0.90
5 5/8/24 13:48 14:08 * 2.50 1.21
6 5/8/24 14:09 14:29 * 2.80 0.80
7 5/8/24 14:59 15:19 0.98 0.79 0.19
8 5/8/24 15:20 15:40 0.49 0.62 -0.13
9 5/8/24 15:41 16:01 0.51 0.63 -0.12
10 5/8/24 16:25 16:45 0.29 0.57 -0.28
11 5/8/24 16:46 17:06 0.16 0.91 -0.75
12 5/8/24 17:07 17:27 * 0.06 1.05
0.74 0.91 -0.17
0.578
91
0.444
0.68 %
RA ≤ 10%
PS 2
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.578 = standard deviation of difference
CC 0.444 = confidence coefficient
Relative Accuracy, RA
where,
d -0.17 = average difference of Reference Method and CEMS
CC 0.444 = confidence coefficient
AS 91.000 = applicable source standard, ppmvd @ 7 % O₂
RA 0.68 = relative accuracy, %
Relative Accuracy (RA)
Performance Required - Applicable Source Standard
Performance Specification Method
* Delimiter for runs not used in RA calculations
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Applicable Source Standard (AS)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
34 of 135
SO2 Summary
Location:
Source:
Project No.:
Reference Method CEMS - Secondary Average
SO₂ Concentration SO₂ Concentration Difference
Start End ppmvd ppmvd ppmvd
1 5/8/24 11:28 11:49 0.49 0.07 0.42
2 5/8/24 11:50 12:10 0.82 0.07 0.75
3 5/8/24 12:11 12:31 0.76 0.86 -0.10
4 5/8/24 13:27 13:47 * 1.61 0.30
5 5/8/24 13:48 14:08 * 2.15 0.13
6 5/8/24 14:09 14:29 * 2.27 0.35
7 5/8/24 14:59 15:19 0.85 0.34 0.51
8 5/8/24 15:20 15:40 0.39 0.20 0.19
9 5/8/24 15:41 16:01 0.43 0.30 0.13
10 5/8/24 16:25 16:45 0.25 0.57 -0.32
11 5/8/24 16:46 17:06 0.13 0.84 -0.71
12 5/8/24 17:07 17:27 0.05 0.80 -0.75
0.46 0.45 0.01
0.529
78.46
0.407
0.54 %
RA ≤ 10%
PS 2
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.529 = standard deviation of difference
CC 0.407 = confidence coefficient
Relative Accuracy, RA
where,
d 0.01 = average difference of Reference Method and CEMS
CC 0.407 = confidence coefficient
AS 78.460 = applicable source standard, ppmvd
RA 0.54 = relative accuracy, %
Performance Specification Method
* Delimiter for runs not used in RA calculations
Relative Accuracy (RA)
Performance Required - Applicable Source Standard
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Applicable Source Standard (AS)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
35 of 135
SO2 Summary
Location:
Source:
Project No.:
Reference Method CEMS - Secondary Average
SO₂ Concentration SO₂ Concentration Difference
Start End ppmvd @ 7 % O₂ ppmvd @ 7 % O₂ ppmvd @ 7 % O₂
1 5/8/24 11:28 11:49 0.58 0.07 0.51
2 5/8/24 11:50 12:10 0.94 0.08 0.86
3 5/8/24 12:11 12:31 0.84 0.99 -0.15
4 5/8/24 13:27 13:47 * 1.89 0.35
5 5/8/24 13:48 14:08 * 2.50 0.15
6 5/8/24 14:09 14:29 * 2.80 0.43
7 5/8/24 14:59 15:19 0.98 0.38 0.60
8 5/8/24 15:20 15:40 0.49 0.24 0.25
9 5/8/24 15:41 16:01 0.51 0.36 0.15
10 5/8/24 16:25 16:45 0.29 0.64 -0.35
11 5/8/24 16:46 17:06 0.16 1.04 -0.88
12 5/8/24 17:07 17:27 0.06 1.02 -0.96
0.54 0.54 0.00
0.639
91
0.491
0.54 %
RA ≤ 10%
PS 2
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.639 = standard deviation of difference
CC 0.491 = confidence coefficient
Relative Accuracy, RA
where,
d 0.00 = average difference of Reference Method and CEMS
CC 0.491 = confidence coefficient
AS 91.000 = applicable source standard, ppmvd @ 7 % O₂
RA 0.54 = relative accuracy, %
Relative Accuracy (RA)
Performance Required - Applicable Source Standard
Performance Specification Method
* Delimiter for runs not used in RA calculations
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Applicable Source Standard (AS)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
36 of 135
SO2 Summary
Location:
Source:
Project No.:
Reference Method CEMS - Backup Average
SO₂ Concentration SO₂ Concentration Difference
Start End ppmvd ppmvd ppmvd
1 5/8/24 11:28 11:49 0.49 0.000 0.49
2 5/8/24 11:50 12:10 0.82 0.000 0.82
3 5/8/24 12:11 12:31 0.76 0.200 0.56
4 5/8/24 13:27 13:47 * 1.61 0.000
5 5/8/24 13:48 14:08 * 2.15 0.010
6 5/8/24 14:09 14:29 * 2.27 0.000
7 5/8/24 14:59 15:19 0.85 0.030 0.82
8 5/8/24 15:20 15:40 0.39 0.000 0.39
9 5/8/24 15:41 16:01 0.43 0.000 0.43
10 5/8/24 16:25 16:45 0.25 0.070 0.18
11 5/8/24 16:46 17:06 0.13 0.000 0.13
12 5/8/24 17:07 17:27 0.05 0.000 0.05
0.46 0.033 0.43
0.280
78.46
0.216
0.82 %
RA ≤ 10%
PS 2
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.280 = standard deviation of difference
CC 0.216 = confidence coefficient
Relative Accuracy, RA
where,
d 0.43 = average difference of Reference Method and CEMS
CC 0.216 = confidence coefficient
AS 78.460 = applicable source standard, ppmvd
RA 0.82 = relative accuracy, %
Performance Specification Method
* Delimiter for runs not used in RA calculations
Relative Accuracy (RA)
Performance Required - Applicable Source Standard
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Applicable Source Standard (AS)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
37 of 135
SO2 Summary
Location:
Source:
Project No.:
Reference Method CEMS - Backup Average
SO₂ Concentration SO₂ Concentration Difference
Start End ppmvd @ 7 % O₂ ppmvd @ 7 % O₂ ppmvd @ 7 % O₂
1 5/8/24 11:28 11:49 0.58 0.000 0.58
2 5/8/24 11:50 12:10 0.94 0.000 0.94
3 5/8/24 12:11 12:31 0.84 0.230 0.61
4 5/8/24 13:27 13:47 * 1.89 0.000
5 5/8/24 13:48 14:08 * 2.50 0.010
6 5/8/24 14:09 14:29 * 2.80 0.000
7 5/8/24 14:59 15:19 0.98 0.040 0.94
8 5/8/24 15:20 15:40 0.49 0.000 0.49
9 5/8/24 15:41 16:01 0.51 0.000 0.51
10 5/8/24 16:25 16:45 0.29 0.080 0.21
11 5/8/24 16:46 17:06 0.16 0.000 0.16
12 5/8/24 17:07 17:27 0.06 0.000 0.06
0.54 0.039 0.50
0.315
91
0.242
0.81 %
RA ≤ 10%
PS 2
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.315 = standard deviation of difference
CC 0.242 = confidence coefficient
Relative Accuracy, RA
where,
d 0.50 = average difference of Reference Method and CEMS
CC 0.242 = confidence coefficient
AS 91.000 = applicable source standard, ppmvd @ 7 % O₂
RA 0.81 = relative accuracy, %
Relative Accuracy (RA)
Performance Required - Applicable Source Standard
Performance Specification Method
* Delimiter for runs not used in RA calculations
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Applicable Source Standard (AS)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
38 of 135
NOx Summary
Location:
Source:
Project No.:
Reference Method CEMS - Primary Average
NOx Concentration NOx Concentration Difference
Start End ppmvd ppmvd ppmvd
1 5/8/24 11:28 11:49 111.24 114.17 -2.93
2 5/8/24 11:50 12:10 116.99 121.91 -4.92
3 5/8/24 12:11 12:31 * 136.54 147.80
4 5/8/24 13:27 13:47 136.51 141.83 -5.32
5 5/8/24 13:48 14:08 126.77 134.20 -7.43
6 5/8/24 14:09 14:29 144.61 154.07 -9.46
7 5/8/24 14:59 15:19 * 143.77 155.49
8 5/8/24 15:20 15:40 173.45 182.68 -9.23
9 5/8/24 15:41 16:01 * 187.93 200.39
10 5/8/24 16:25 16:45 144.12 148.88 -4.76
11 5/8/24 16:46 17:06 132.44 137.20 -4.76
12 5/8/24 17:07 17:27 115.13 116.91 -1.78
133.47 139.09 -5.62
2.626
2.018
5.72 %
RA ≤ 20%
PS 2
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 2.626 = standard deviation of difference
CC 2.018 = confidence coefficient
Relative Accuracy, RA
where,
d -5.62 = average difference of Reference Method and CEMS
CC 2.018 = confidence coefficient
RM 133.474 = reference method, ppmvd
RA 5.72 = relative accuracy, %
Relative Accuracy (RA)
Performance Required - Mean Reference Method
Performance Specification Method
* Delimiter for runs not used in RA calculations
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
39 of 135
NOx Summary
Location:
Source:
Project No.:
Reference Method CEMS - Primary Average
NOx Emission Rate NOx Emission Rate Difference
Start End lb/hr lb/hr lb/hr
1 5/8/24 11:28 11:49 24.32 25.79 -1.47
2 5/8/24 11:50 12:10 25.08 26.67 -1.59
3 5/8/24 12:11 12:31 * 28.92 32.75
4 5/8/24 13:27 13:47 29.64 31.77 -2.13
5 5/8/24 13:48 14:08 27.96 30.39 -2.43
6 5/8/24 14:09 14:29 31.85 34.52 -2.67
7 5/8/24 14:59 15:19 * 30.89 34.63
8 5/8/24 15:20 15:40 38.42 41.47 -3.05
9 5/8/24 15:41 16:01 44.35 45.37 -1.02
10 5/8/24 16:25 16:45 * 29.37 33.20
11 5/8/24 16:46 17:06 28.62 31.25 -2.63
12 5/8/24 17:07 17:27 25.63 26.81 -1.18
30.65 32.67 -2.02
0.730
44.2
0.561
8.42 %
RA ≤ 20%
PS 2
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.730 = standard deviation of difference
CC 0.561 = confidence coefficient
Relative Accuracy, RA
where,
d -2.02 = average difference of Reference Method and CEMS
CC 0.561 = confidence coefficient
RM 30.652 = reference method, lb/hr
RA 8.42 = relative accuracy, %
Relative Accuracy (RA)
Performance Required - Mean Reference Method
Performance Specification Method
* Delimiter for runs not used in RA calculations
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Applicable Source Standard (AS)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
40 of 135
NOx Summary
Location:
Source:
Project No.:
Reference Method CEMS - Secondary Average
NOx Concentration NOx Concentration Difference
Start End ppmvd ppmvd ppmvd
1 5/8/24 11:28 11:49 111.24 113.33 -2.09
2 5/8/24 11:50 12:10 116.99 120.79 -3.80
3 5/8/24 12:11 12:31 * 136.54 145.72
4 5/8/24 13:27 13:47 136.51 141.28 -4.77
5 5/8/24 13:48 14:08 126.77 133.20 -6.43
6 5/8/24 14:09 14:29 144.61 154.04 -9.43
7 5/8/24 14:59 15:19 * 143.77 154.32
8 5/8/24 15:20 15:40 173.45 180.45 -7.00
9 5/8/24 15:41 16:01 * 187.93 199.82
10 5/8/24 16:25 16:45 144.12 145.94 -1.82
11 5/8/24 16:46 17:06 132.44 136.44 -4.00
12 5/8/24 17:07 17:27 115.13 115.13 0.00
133.47 137.84 -4.37
2.920
2.245
4.96 %
RA ≤ 20%
PS 2
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 2.920 = standard deviation of difference
CC 2.245 = confidence coefficient
Relative Accuracy, RA
where,
d -4.37 = average difference of Reference Method and CEMS
CC 2.245 = confidence coefficient
RM 133.474 = reference method, ppmvd
RA 4.96 = relative accuracy, %
Performance Specification Method
* Delimiter for runs not used in RA calculations
Relative Accuracy (RA)
Performance Required - Mean Reference Method
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
41 of 135
NOx Summary
Location:
Source:
Project No.:
Reference Method CEMS - Secondary Average
NOx Emission Rate NOx Emission Rate Difference
Start End lb/hr lb/hr lb/hr
1 5/8/24 11:28 11:49 24.32 25.60 -1.28
2 5/8/24 11:50 12:10 25.08 26.43 -1.35
3 5/8/24 12:11 12:31 * 28.92 32.29
4 5/8/24 13:27 13:47 29.64 31.65 -2.01
5 5/8/24 13:48 14:08 27.96 30.16 -2.20
6 5/8/24 14:09 14:29 31.85 34.51 -2.66
7 5/8/24 14:59 15:19 * 30.89 34.37
8 5/8/24 15:20 15:40 38.42 40.97 -2.55
9 5/8/24 15:41 16:01 44.35 45.24 -0.89
10 5/8/24 16:25 16:45 * 29.37 32.55
11 5/8/24 16:46 17:06 28.62 31.08 -2.46
12 5/8/24 17:07 17:27 25.63 26.40 -0.77
30.65 32.45 -1.80
0.736
44.2
0.566
7.71 %
RA ≤ 20%
PS 2
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.736 = standard deviation of difference
CC 0.566 = confidence coefficient
Relative Accuracy, RA
where,
d -1.80 = average difference of Reference Method and CEMS
CC 0.566 = confidence coefficient
RM 30.652 = reference method, lb/hr
RA 7.71 = relative accuracy, %
Performance Specification Method
* Delimiter for runs not used in RA calculations
Average
Standard Deviation (Sd)
Applicable Source Standard (AS)
Confidence Coefficient (CC)
Relative Accuracy (RA)
Performance Required - Mean Reference Method
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
42 of 135
NOx Summary
Location:
Source:
Project No.:
Reference Method CEMS - Backup Average
NOx Concentration NOx Concentration Difference
Start End ppmvd ppmvd ppmvd
1 5/8/24 11:28 11:49 111.24 111.88 -0.64
2 5/8/24 11:50 12:10 116.99 119.99 -3.00
3 5/8/24 12:11 12:31 * 136.54 145.56
4 5/8/24 13:27 13:47 136.51 140.33 -3.82
5 5/8/24 13:48 14:08 126.77 132.10 -5.33
6 5/8/24 14:09 14:29 144.61 152.00 -7.39
7 5/8/24 14:59 15:19 * 143.77 153.43
8 5/8/24 15:20 15:40 173.45 180.91 -7.46
9 5/8/24 15:41 16:01 * 187.93 197.97
10 5/8/24 16:25 16:45 144.12 147.30 -3.18
11 5/8/24 16:46 17:06 132.44 134.89 -2.45
12 5/8/24 17:07 17:27 115.13 114.45 0.68
133.47 137.09 -3.62
2.768
2.128
4.31 %
RA ≤ 20%
PS 2
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 2.768 = standard deviation of difference
CC 2.128 = confidence coefficient
Relative Accuracy, RA
where,
d -3.62 = average difference of Reference Method and CEMS
CC 2.128 = confidence coefficient
RM 133.474 = reference method, ppmvd
RA 4.31 = relative accuracy, %
Performance Specification Method
* Delimiter for runs not used in RA calculations
Relative Accuracy (RA)
Performance Required - Mean Reference Method
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
43 of 135
NOx Summary
Location:
Source:
Project No.:
Reference Method CEMS - Backup Average
NOx Emission Rate NOx Emission Rate Difference
Start End lb/hr lb/hr lb/hr
1 5/8/24 11:28 11:49 24.32 25.27 -0.95
2 5/8/24 11:50 12:10 25.08 26.25 -1.17
3 5/8/24 12:11 12:31 * 28.92 32.25
4 5/8/24 13:27 13:47 29.64 31.43 -1.79
5 5/8/24 13:48 14:08 27.96 29.91 -1.95
6 5/8/24 14:09 14:29 31.85 34.06 -2.21
7 5/8/24 14:59 15:19 * 30.89 34.17
8 5/8/24 15:20 15:40 38.42 41.07 -2.65
9 5/8/24 15:41 16:01 44.35 44.82 -0.47
10 5/8/24 16:25 16:45 * 29.37 32.85
11 5/8/24 16:46 17:06 28.62 30.72 -2.10
12 5/8/24 17:07 17:27 25.63 26.25 -0.62
30.65 32.20 -1.55
0.769
44.2
0.591
6.97 %
RA ≤ 20%
PS 2
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.769 = standard deviation of difference
CC 0.591 = confidence coefficient
Relative Accuracy, RA
where,
d -1.55 = average difference of Reference Method and CEMS
CC 0.591 = confidence coefficient
RM 30.652 = reference method, lb/hr
RA 6.97 = relative accuracy, %
Performance Specification Method
* Delimiter for runs not used in RA calculations
Average
Standard Deviation (Sd)
Applicable Source Standard (AS)
Confidence Coefficient (CC)
Relative Accuracy (RA)
Performance Required - Mean Reference Method
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
44 of 135
CO Summary
Location:
Source:
Project No.:
Reference Method CEMS - Primary Average
CO Concentration CO Concentration Difference
Start End ppmvd ppmvd ppmvd
1 5/8/24 11:28 11:49 * 5.07 11.19
2 5/8/24 11:50 12:10 2.30 1.76 0.54
3 5/8/24 12:11 12:31 1.02 0.35 0.67
4 5/8/24 13:27 13:47 1.23 0.50 0.73
5 5/8/24 13:48 14:08 * 5.92 15.01
6 5/8/24 14:09 14:29 1.35 0.83 0.52
7 5/8/24 14:59 15:19 5.86 11.73 -5.87
8 5/8/24 15:20 15:40 1.33 0.86 0.47
9 5/8/24 15:41 16:01 1.30 0.80 0.50
10 5/8/24 16:25 16:45 * 6.72 13.20
11 5/8/24 16:46 17:06 1.30 0.80 0.50
12 5/8/24 17:07 17:27 1.40 0.94 0.46
1.90 2.06 -0.16
2.141
1.645
1.81 ppm
≤ 5 ppm
PS 4A
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 2.141 = standard deviation of difference
CC 1.645 = confidence coefficient
Performance Specification Method
* Delimiter for runs not used in RA calculations
Alternative Relative Accuracy (RA)
Alternative Performance Required (d + CC)
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
45 of 135
CO Summary
Location:
Source:
Project No.:
Reference Method CEMS - Primary Average
CO Concentration CO Concentration Difference
Start End ppmvd @ 7 % O₂ ppmvd @ 7 % O₂ ppmvd @ 7 % O₂
1 5/8/24 11:28 11:49 * 6.03 12.24
2 5/8/24 11:50 12:10 2.61 1.86 0.75
3 5/8/24 12:11 12:31 1.13 0.39 0.74
4 5/8/24 13:27 13:47 1.44 0.57 0.87
5 5/8/24 13:48 14:08 * 6.88 15.80
6 5/8/24 14:09 14:29 1.67 1.00 0.67
7 5/8/24 14:59 15:19 6.73 12.28 -5.55
8 5/8/24 15:20 15:40 1.64 1.05 0.59
9 5/8/24 15:41 16:01 1.53 0.93 0.60
10 5/8/24 16:25 16:45 * 7.70 13.33
11 5/8/24 16:46 17:06 1.62 0.98 0.64
12 5/8/24 17:07 17:27 1.85 1.22 0.63
2.25 2.25 -0.01
2.081
100
1.600
1.61 %
RA ≤ 5%
1.61 ppm
≤ 5 ppm
PS 4A
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 2.081 = standard deviation of difference
CC 1.600 = confidence coefficient
Relative Accuracy, RA
where,
d -0.01 = average difference of Reference Method and CEMS
CC 1.600 = confidence coefficient
AS 100.000 = applicable source standard, ppmvd @ 7 % O₂
RA 1.61 = relative accuracy, %
Relative Accuracy (RA)
Performance Required - Applicable Source Standard
Performance Specification Method
* Delimiter for runs not used in RA calculations
Alternative Relative Accuracy (RA)
Alternative Performance Required (d + CC)
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Applicable Source Standard (AS)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
46 of 135
CO Summary
Location:
Source:
Project No.:
Reference Method CEMS - Secondary Average
CO Concentration CO Concentration Difference
Start End ppmvd ppmvd ppmvd
1 5/8/24 11:28 11:49 5.07 11.32 -6.25
2 5/8/24 11:50 12:10 2.30 1.95 0.35
3 5/8/24 12:11 12:31 1.02 0.68 0.34
4 5/8/24 13:27 13:47 1.23 0.82 0.41
5 5/8/24 13:48 14:08 * 5.92 14.28
6 5/8/24 14:09 14:29 1.35 0.93 0.42
7 5/8/24 14:59 15:19 * 5.86 11.71
8 5/8/24 15:20 15:40 1.33 0.90 0.43
9 5/8/24 15:41 16:01 1.30 0.93 0.37
10 5/8/24 16:25 16:45 * 6.72 13.23
11 5/8/24 16:46 17:06 1.30 0.90 0.40
12 5/8/24 17:07 17:27 1.40 1.04 0.36
1.81 2.16 -0.35
2.210
1.699
2.05 ppm
≤ 5 ppm
PS 4A
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 2.210 = standard deviation of difference
CC 1.699 = confidence coefficient
Alternative Performance Required (d + CC)
Performance Specification Method
* Delimiter for runs not used in RA calculations
Alternative Relative Accuracy (RA)
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
47 of 135
CO Summary
Location:
Source:
Project No.:
Reference Method CEMS - Secondary Average
CO Concentration CO Concentration Difference
Start End ppmvd @ 7 % O₂ ppmvd @ 7 % O₂ ppmvd @ 7 % O₂
1 5/8/24 11:28 11:49 * 6.03 13.30
2 5/8/24 11:50 12:10 2.61 2.11 0.50
3 5/8/24 12:11 12:31 1.13 0.75 0.38
4 5/8/24 13:27 13:47 1.44 0.94 0.50
5 5/8/24 13:48 14:08 * 6.88 15.19
6 5/8/24 14:09 14:29 1.67 1.13 0.54
7 5/8/24 14:59 15:19 * 6.73 12.41
8 5/8/24 15:20 15:40 1.64 1.09 0.55
9 5/8/24 15:41 16:01 1.53 1.08 0.45
10 5/8/24 16:25 16:45 7.70 13.31 -5.61
11 5/8/24 16:46 17:06 1.62 1.09 0.53
12 5/8/24 17:07 17:27 1.85 1.34 0.51
2.35 2.54 -0.18
2.035
100
1.564
1.75 %
RA ≤ 5%
1.75 ppm
≤ 5 ppm
PS 4A
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 2.035 = standard deviation of difference
CC 1.564 = confidence coefficient
Relative Accuracy, RA
where,
d -0.18 = average difference of Reference Method and CEMS
CC 1.564 = confidence coefficient
AS 100.000 = applicable source standard, ppmvd @ 7 % O₂
RA 1.75 = relative accuracy, %
Alternative Performance Required (d + CC)
Performance Specification Method
* Delimiter for runs not used in RA calculations
Relative Accuracy (RA)
Performance Required - Applicable Source Standard
Alternative Relative Accuracy (RA)
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Applicable Source Standard (AS)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
48 of 135
CO Summary
Location:
Source:
Project No.:
Reference Method CEMS - Backup Average
CO Concentration CO Concentration Difference
Start End ppmvd ppmvd ppmvd
1 5/8/24 11:28 11:49 * 5.07 11.78
2 5/8/24 11:50 12:10 2.30 2.26 0.04
3 5/8/24 12:11 12:31 1.02 0.89 0.13
4 5/8/24 13:27 13:47 1.23 0.92 0.31
5 5/8/24 13:48 14:08 * 5.92 15.97
6 5/8/24 14:09 14:29 1.35 1.16 0.19
7 5/8/24 14:59 15:19 5.86 12.28 -6.42
8 5/8/24 15:20 15:40 1.33 1.18 0.15
9 5/8/24 15:41 16:01 1.30 1.13 0.17
10 5/8/24 16:25 16:45 * 6.72 13.20
11 5/8/24 16:46 17:06 1.30 1.16 0.14
12 5/8/24 17:07 17:27 1.40 1.19 0.21
1.90 2.46 -0.56
2.196
1.688
2.25 ppm
≤ 5 ppm
PS 4A
Note: Since abs(d) < CC, the system passes the bias test
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 2.196 = standard deviation of difference
CC 1.688 = confidence coefficient
Alternative Performance Required (d + CC)
Performance Specification Method
* Delimiter for runs not used in RA calculations
Alternative Relative Accuracy (RA)
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
49 of 135
CO Summary
Location:
Source:
Project No.:
Reference Method CEMS - Backup Average
CO Concentration CO Concentration Difference
Start End ppmvd @ 7 % O₂ ppmvd @ 7 % O₂ ppmvd @ 7 % O₂
1 5/8/24 11:28 11:49 * 6.03 12.59
2 5/8/24 11:50 12:10 2.61 2.41 0.20
3 5/8/24 12:11 12:31 1.13 0.97 0.16
4 5/8/24 13:27 13:47 1.44 1.05 0.39
5 5/8/24 13:48 14:08 * 6.88 16.73
6 5/8/24 14:09 14:29 1.67 1.40 0.27
7 5/8/24 14:59 15:19 * 6.73 12.81
8 5/8/24 15:20 15:40 1.64 1.43 0.21
9 5/8/24 15:41 16:01 1.53 1.31 0.22
10 5/8/24 16:25 16:45 7.70 13.36 -5.66
11 5/8/24 16:46 17:06 1.62 1.40 0.22
12 5/8/24 17:07 17:27 1.85 1.53 0.32
2.35 2.76 -0.41
1.970
100
1.514
1.92 %
RA ≤ 5%
1.92 ppm
≤ 5 ppm
PS 4A
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 1.970 = standard deviation of difference
CC 1.514 = confidence coefficient
Relative Accuracy, RA
where,
d -0.41 = average difference of Reference Method and CEMS
CC 1.514 = confidence coefficient
AS 100.000 = applicable source standard, ppmvd @ 7 % O₂
RA 1.92 = relative accuracy, %
Alternative Performance Required (d + CC)
Performance Specification Method
* Delimiter for runs not used in RA calculations
Relative Accuracy (RA)
Performance Required - Applicable Source Standard
Alternative Relative Accuracy (RA)
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Applicable Source Standard (AS)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
50 of 135
THC Summary
Location:
Source:
Project No.:
Reference Method CEMS - Primary Average
THC (as C₃H₈) Concentration THC (as C₃H₈) Concentration Difference
Start End ppmvw ppmvw ppmvw
1 5/8/24 11:28 11:49 *1.30 0.18
2 5/8/24 11:50 12:10 *1.04 0.15
3 5/8/24 12:11 12:31 *0.78 0.18
4 5/8/24 13:27 13:47 0.57 0.16 0.41
5 5/8/24 13:48 14:08 0.59 0.23 0.36
6 5/8/24 14:09 14:29 0.18 0.15 0.03
7 5/8/24 14:59 15:19 0.19 0.23 -0.04
8 5/8/24 15:20 15:40 0.18 0.16 0.02
9 5/8/24 15:41 16:01 -0.03 0.14 -0.17
10 5/8/24 16:25 16:45 -0.12 0.20 -0.32
11 5/8/24 16:46 17:06 -0.10 0.11 -0.21
12 5/8/24 17:07 17:27 -0.06 0.10 -0.16
0.16 0.16 -0.01
0.253
6.13
0.194
3.3 %
RA ≤ 10%
PS 2
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.253 = standard deviation of difference
CC 0.194 = confidence coefficient
Relative Accuracy, RA
where,
d -0.01 = average difference of Reference Method and CEMS
CC 0.194 = confidence coefficient
AS 6.130 = applicable source standard, ppmvw
RA 3.30 = relative accuracy, %
Relative Accuracy (RA)
Performance Required - Applicable Source Standard
Performance Specification Method
* Delimiter for runs not used in RA calculations
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Applicable Source Standard (AS)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
51 of 135
Location:
Source:
Project No.:
Reference Method CEMS - Primary Average
THC (as C₃H₈) Concentration THC (as C₃H₈) Concentration Difference
Start End ppmvd @ 7 % O₂ppmvd @ 7 % O₂ ppmvd @ 7 % O₂
1 5/8/24 11:28 11:49 *2.17 0.33
2 5/8/24 11:50 12:10 *1.67 0.26
3 5/8/24 12:11 12:31 *1.21 0.30
4 5/8/24 13:27 13:47 0.94 0.29 0.65
5 5/8/24 13:48 14:08 0.96 0.41 0.55
6 5/8/24 14:09 14:29 0.32 0.28 0.04
7 5/8/24 14:59 15:19 0.31 0.40 -0.09
8 5/8/24 15:20 15:40 0.31 0.29 0.02
9 5/8/24 15:41 16:01 -0.05 0.26 -0.31
10 5/8/24 16:25 16:45 -0.14 0.35 -0.49
11 5/8/24 16:46 17:06 -0.13 0.21 -0.34
12 5/8/24 17:07 17:27 -0.08 0.20 -0.28
0.27 0.30 -0.03
0.397
10
0.305
3.34 %
RA ≤ 10%
PS 2
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.397 = standard deviation of difference
CC 0.305 = confidence coefficient
Relative Accuracy, RA
where,
d -0.03 = average difference of Reference Method and CEMS
CC 0.305 = confidence coefficient
AS 10.000 = applicable source standard, ppmvd @ 7 % O₂
RA 3.34 = relative accuracy, %
Relative Accuracy (RA)
Performance Required - Applicable Source Standard
Performance Specification Method
* Delimiter for runs not used in RA calculations
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Applicable Source Standard (AS)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
THC Summary
52 of 135
Location:
Source:
Project No.:
Reference Method CEMS - Secondary Average
THC (as C₃H₈) Concentration THC (as C₃H₈) Concentration Difference
Start End ppmvw ppmvw ppmvw
1 5/8/24 11:28 11:49 *1.30 0.070
2 5/8/24 11:50 12:10 *1.04 0.060
3 5/8/24 12:11 12:31 *0.78 0.080
4 5/8/24 13:27 13:47 0.57 0.040 0.53
5 5/8/24 13:48 14:08 0.59 0.150 0.44
6 5/8/24 14:09 14:29 0.18 0.030 0.15
7 5/8/24 14:59 15:19 0.19 0.110 0.08
8 5/8/24 15:20 15:40 0.18 0.050 0.13
9 5/8/24 15:41 16:01 -0.03 0.050 -0.08
10 5/8/24 16:25 16:45 -0.12 0.100 -0.22
11 5/8/24 16:46 17:06 -0.10 0.020 -0.12
12 5/8/24 17:07 17:27 -0.06 0.000 -0.06
0.16 0.061 0.09
0.256
6.13
0.196
4.75 %
RA ≤ 10%
PS 2
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.256 = standard deviation of difference
CC 0.196 = confidence coefficient
Relative Accuracy, RA
where,
d 0.09 = average difference of Reference Method and CEMS
CC 0.196 = confidence coefficient
AS 6.130 = applicable source standard, ppmvw
RA 4.75 = relative accuracy, %
Relative Accuracy (RA)
Performance Required - Applicable Source Standard
Performance Specification Method
* Delimiter for runs not used in RA calculations
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Applicable Source Standard (AS)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
THC Summary
53 of 135
Location:
Source:
Project No.:
Reference Method CEMS - Secondary Average
THC (as C₃H₈) Concentration THC (as C₃H₈) Concentration Difference
Start End ppmvd @ 7 % O₂ppmvd @ 7 % O₂ ppmvd @ 7 % O₂
1 5/8/24 11:28 11:49 *2.17 0.12
2 5/8/24 11:50 12:10 *1.67 0.11
3 5/8/24 12:11 12:31 *1.21 0.14
4 5/8/24 13:27 13:47 0.94 0.07 0.87
5 5/8/24 13:48 14:08 0.96 0.26 0.70
6 5/8/24 14:09 14:29 0.32 0.05 0.27
7 5/8/24 14:59 15:19 0.31 0.20 0.11
8 5/8/24 15:20 15:40 0.31 0.09 0.22
9 5/8/24 15:41 16:01 -0.05 0.10 -0.15
10 5/8/24 16:25 16:45 -0.14 0.17 -0.31
11 5/8/24 16:46 17:06 -0.13 0.03 -0.16
12 5/8/24 17:07 17:27 -0.08 0.00 -0.08
0.27 0.11 0.16
0.402
10
0.309
4.72 %
RA ≤ 10%
PS 2
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.402 = standard deviation of difference
CC 0.309 = confidence coefficient
Relative Accuracy, RA
where,
d 0.16 = average difference of Reference Method and CEMS
CC 0.309 = confidence coefficient
AS 10.000 = applicable source standard, ppmvd @ 7 % O₂
RA 4.72 = relative accuracy, %
Relative Accuracy (RA)
Performance Required - Applicable Source Standard
Performance Specification Method
* Delimiter for runs not used in RA calculations
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Applicable Source Standard (AS)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
THC Summary
54 of 135
Location:
Source:
Project No.:
Reference Method CEMS - Backup Average
THC (as C₃H₈) Concentration THC (as C₃H₈) Concentration Difference
Start End ppmvw ppmvw ppmvw
1 5/8/24 11:28 11:49 *1.30 0.020
2 5/8/24 11:50 12:10 *1.04 0.000
3 5/8/24 12:11 12:31 *0.78 0.000
4 5/8/24 13:27 13:47 0.57 0.000 0.57
5 5/8/24 13:48 14:08 0.59 0.060 0.53
6 5/8/24 14:09 14:29 0.18 0.000 0.18
7 5/8/24 14:59 15:19 0.19 0.080 0.11
8 5/8/24 15:20 15:40 0.18 0.000 0.18
9 5/8/24 15:41 16:01 -0.03 0.000 -0.03
10 5/8/24 16:25 16:45 -0.12 0.040 -0.16
11 5/8/24 16:46 17:06 -0.10 0.000 -0.10
12 5/8/24 17:07 17:27 -0.06 0.000 -0.06
0.16 0.020 0.14
0.266
6.13
0.205
5.56 %
RA ≤ 10%
PS 2
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.266 = standard deviation of difference
CC 0.205 = confidence coefficient
Relative Accuracy, RA
where,
d 0.14 = average difference of Reference Method and CEMS
CC 0.205 = confidence coefficient
AS 6.130 = applicable source standard, ppmvw
RA 5.56 = relative accuracy, %
Relative Accuracy (RA)
Performance Required - Applicable Source Standard
Performance Specification Method
* Delimiter for runs not used in RA calculations
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Applicable Source Standard (AS)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
THC Summary
55 of 135
Location:
Source:
Project No.:
Reference Method CEMS - Backup Average
THC (as C₃H₈) Concentration THC (as C₃H₈) Concentration Difference
Start End ppmvd @ 7 % O₂ppmvd @ 7 % O₂ ppmvd @ 7 % O₂
1 5/8/24 11:28 11:49 *2.17 0.040
2 5/8/24 11:50 12:10 *1.67 0.000
3 5/8/24 12:11 12:31 *1.21 0.000
4 5/8/24 13:27 13:47 0.94 0.000 0.94
5 5/8/24 13:48 14:08 0.96 0.110 0.85
6 5/8/24 14:09 14:29 0.32 0.000 0.32
7 5/8/24 14:59 15:19 0.31 0.130 0.18
8 5/8/24 15:20 15:40 0.31 0.000 0.31
9 5/8/24 15:41 16:01 -0.05 0.000 -0.05
10 5/8/24 16:25 16:45 -0.14 0.060 -0.20
11 5/8/24 16:46 17:06 -0.13 0.000 -0.13
12 5/8/24 17:07 17:27 -0.08 0.000 -0.08
0.27 0.033 0.24
0.418
10
0.321
5.59 %
RA ≤ 10%
PS 2
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 0.418 = standard deviation of difference
CC 0.321 = confidence coefficient
Relative Accuracy, RA
where,
d 0.24 = average difference of Reference Method and CEMS
CC 0.321 = confidence coefficient
AS 10.000 = applicable source standard, ppmvd @ 7 % O₂
RA 5.59 = relative accuracy, %
Relative Accuracy (RA)
Performance Required - Applicable Source Standard
Performance Specification Method
* Delimiter for runs not used in RA calculations
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Applicable Source Standard (AS)
Confidence Coefficient (CC)
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝐴𝑆 𝑜𝑟 𝑅𝑀× 100
THC Summary
56 of 135
VFR Summary
Location:
Source:
Project No.:
Reference Method CEMS Average
Flow Rate Flow Rate Difference
Start End acfm acfm acfm
1 5/8/24 11:28 11:49 58,763 61,843 -3,080
2 5/8/24 11:50 12:11 57,792 60,905 -3,113
3 5/8/24 12:12 12:31 57,094 61,882 -4,788
4 5/8/24 13:27 13:48 58,155 62,445 -4,290
5 5/8/24 13:49 14:09 59,075 63,117 -4,042
6 5/8/24 14:10 14:30 58,998 62,650 -3,652
7 5/8/24 14:59 15:19 * 57,150 62,953
8 5/8/24 15:20 15:40 58,959 63,574 -4,615
9 5/8/24 15:41 16:01 62,822 63,639 -817
10 5/8/24 16:25 16:44 * 55,124 62,827
11 5/8/24 16:45 17:05 * 58,283 63,726
12 5/8/24 17:06 17:26 60,032 63,389 -3,357
59,077 62,605 -3,528
1,193
916.821
7.52 %
≤ 20%
PS 6
Note: run time came from VFR sheet
Confidence Coefficient, CC
where,
t0.975 2.306 = degrees of freedom value
n 9 = number of runs selected for calculating the RA
Sd 1,192.74 = standard deviation of difference
CC 916.82 = confidence coefficient
Relative Accuracy, RA
where,
d -3,528.22 = average difference of Reference Method and CEMS
CC 916.82 = confidence coefficient
RM 59,076.67 = reference method, acfm
RA 7.52 = relative accuracy, %
Bias Test Results, BA
where,
d -3528.222 = average difference of Reference Method and CEMS
CC 916.821 = confidence coefficient
BA Required?No
Bias Adjustment Factor, BAF
where,
d -3528.222 = average difference of Reference Method and CEMS
CEMSavg 62604.889 = average of CEMS values
BAF 1.000 = bias adjustment factor
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Run
No.Date Time
Average
Standard Deviation (Sd)
Confidence Coefficient (CC)
Relative Accuracy (RA)
Acceptability Criteria - Mean Reference Method
Performance Specification Method
* Delimiter for runs not used in RA calculations
BA Required if 𝑑 > 𝐶𝐶
CC = t଴.ଽ଻ହ
n × 𝑆d
RA = d +𝐶𝐶
𝑅𝑀× 100
BAF = d
CEMSୟ୴୥
 +  1
57 of 135
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58 of 135
Method 1 Data
Location
Source
Project No.
Date:
Vertical
Circular
67.50 in
7.50 in
60.00 in
19.63 ft2
2
1
60.0 ft
12.0 (must be ≥ 0.5)
50.0 ft
10.0 (must be ≥ 2)
12
16
Measurer (Initial and Date):MDM 5/8/24
Reviewer (Initial and Date):SPR 5/8/24
2 3 4 5 6 7 8 9 10 11 12
1 14.6 -- 6.7 -- 4.4 -- 3.2 -- 2.6 -- 2.1 1 3.2 1.92 9.42
2 85.4 -- 25.0 -- 14.6 -- 10.5 -- 8.2 -- 6.7 2 10.5 6.30 13.80
3 -- -- 75.0 -- 29.6 -- 19.4 -- 14.6 -- 11.8 3 19.4 11.64 19.14
4 -- -- 93.3 -- 70.4 -- 32.3 -- 22.6 -- 17.7 4 32.3 19.38 26.88
5 -- -- -- -- 85.4 -- 67.7 -- 34.2 -- 25.0 5 67.7 40.62 48.12
6 -- -- -- -- 95.6 -- 80.6 -- 65.8 -- 35.6 6 80.6 48.36 55.86
7 -- -- -- -- -- -- 89.5 -- 77.4 -- 64.4 7 89.5 53.70 61.20
8 -- -- -- -- -- -- 96.8 -- 85.4 -- 75.0 8 96.8 58.08 65.58
9 -- -- -- -- -- -- -- -- 91.8 -- 82.3 9 -- -- --
10 -- -- -- -- -- -- -- -- 97.4 -- 88.2 10 -- -- --
11 -- -- -- -- -- -- -- -- -- -- 93.3 11 -- -- --
12 -- -- -- -- -- -- -- -- -- -- 97.9 12 -- -- --
*Percent of stack diameter from inside wall to traverse point.
A = 60 ft.
B = 50 ft.
Depth of Duct = 60 in.
Number of traverse points on a diameter
Stack Diagram
Cross Sectional Area
Distance
from
outside of
port
LOCATION OF TRAVERSE POINTS
Traverse
Point
% of
Diameter
Distance
from inside
wall
No. of Test Ports:
Number of Readings per Point:
Distance A:
Distance A Duct Diameters:
Distance B:
Distance B Duct Diameters:
Minimum Number of Traverse Points:
Actual Number of Traverse Points:
CIRCULAR DUCT
Cross Sectional Area of Duct:
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
05/08/24
Stack Parameters
Duct Orientation:
Duct Design:
Distance from Far Wall to Outside of Port:
Nipple Length:
Depth of Duct:
Upstream
Disturbance
Downstream
Disturbance
B
A
59 of 135
Cyclonic Flow Check
Location
Source
Project No.
Date
Sample Point Angle (ΔP=0)
1 0
2 0
3 0
4 5
5 5
6 5
7 5
8 0
9 5
10 5
11 0
12 0
13 0
14 5
15 5
16 5
Average 2.8
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
5/8/24
60 of 135
Me
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2

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61 of 135
Location
Source
Project No.
Parameter(s):
Console Units / Method ft3 M4
Run No.
Date
Status
Start Time
End Time
Run Time, min (θ)
Meter ID
Meter Correction Factor (Y)
Orifice Calibration Value (ΔH @)
Max Vacuum, in. Hg
Post Leak Check, ft3/min (at max vac.)
Meter Volume, ft3
Total Meter Volume, ft3 (Vm)
Meter Probe Filter Vacuum Imp. Exit Meter Probe Filter Vacuum Imp. Exit Meter Probe Filter Vacuum Imp. Exit Meter Probe Filter Vacuum Imp. Exit
48 -- -- 3 54 56 -- -- 3 56 59 -- -- 3 51 59 -- -- 3 52
48 -- -- 3 50 56 -- -- 3 56 59 -- -- 3 51 59 -- -- 3 52
49 -- -- 3 50 56 -- -- 3 56 59 -- -- 3 51 59 -- -- 3 52
49 -- -- 3 50 56 -- -- 3 56 59 -- -- 3 51 59 -- -- 3 52
49 -- -- 3 49 56 -- -- 3 56 59 -- -- 3 52 60 -- -- 3 52
49 -- -- 3 49 56 -- -- 3 57 59 -- -- 3 52 60 -- -- 3 52
49 -- -- 3 49 57 -- -- 3 57 59 -- -- 3 52 60 -- -- 3 52
50 -- -- 3 49 57 -- -- 3 58 60 -- -- 3 52 60 -- -- 3 52
50 -- -- 3 48 57 -- -- 3 58 60 -- -- 3 52 59 -- -- 3 52
50 -- -- 3 49 57 -- -- 3 58 60 -- -- 3 52 59 -- -- 3 52
51 -- -- 3 49 57 -- -- 3 58 60 -- -- 3 53 59 -- -- 3 52
51 -- -- 3 49 56 -- -- 3 58 60 -- -- 3 53 59 -- -- 3 52
51 -- -- 3 49 58 -- -- 3 58 60 -- -- 3 53 59 -- -- 3 52
51 -- -- 3 49 58 -- -- 3 58 60 -- -- 3 54 59 -- -- 3 52
Average Temperature, °F (Tm)50 -- -- 3 50 57 -- -- 3 57 60 -- -- 3 52 59 -- -- 3 52
Average Temperature, °R (Tm)509 -- -- -- -- 516 -- -- -- -- 519 -- -- -- -- 519 -- -- -- --
Minimum Temperature, °F 48 -- -- 3 48 56 -- -- 3 56 59 -- -- 3 51 59 -- -- 3 52
Maximum Temperature, °F 51 -- -- 3 54 58 -- -- 3 58 60 -- -- 3 54 60 -- -- 3 52
Barometric Pressure, in. Hg (Pb)
Meter Orifice Pressure , in. WC (ΔH)
Meter Pressure, in. Hg (Pm)
Standard Meter Volume, ft3 (Vmstd)
Analysis Type
Impinger 1, Pre/Post Test, g 765.6 948.6 183.0 751.2 939.6 188.4 768.7 945.6 176.9 763.4 948.1 184.7
Impinger 2, Pre/Post Test, g 748.5 848.7 100.2 763.3 870.2 106.9 772.3 865.1 92.8 777.9 881.3 103.4
Impinger 3, Pre/Post Test, g 676.0 681.3 5.3 681.3 686.0 4.7 686.0 691.3 5.3 691.3 696.2 4.9
Impinger 4, Pre/Post Test, g 889.6 899.7 10.1 899.7 911.2 11.5 911.2 923.3 12.1 923.3 934.7 11.4
Volume Water Collected, mL (Vlc)
Standard Water Volume, ft3 (Vwstd)
Moisture Fraction Measured (BWS)
Gas Molecular Weight, lb/lb-mole (dry) (Md)
DGM Calibration Check Value (Yqa)
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
BWS
1 2 3 4
5/8/24 5/8/24 5/8/24 5/8/24
VALID VALID VALID VALID
11:28 13:27 14:59 16:25
12:31 14:30 16:02 17:28
63 63 63 63
M5-27 M5-27 M5-27 M5-27
0.995 0.995 0.995 0.995
1.853 1.853 1.853 1.853
3 3 3 3
.001@6 .001@5 .001@5 .001@5
0 121.405 160.875 203.661 244.520
5 124.544 164.635 207.015 247.770
15 130.215 171.350 213.425 254.270
10 127.525 167.885 210.365 251.020
20 133.875 174.630 216.635 257.500
181.455 223.010 263.960
25 136.985 178.030 219.820 260.730
35 143.000 184.895 226.220 267.180
30 140.170
40 146.475 188.340 229.415 270.365
194.910 235.885 276.840
45 149.585 191.635 232.630 273.665
55 155.450 197.960 239.145 280.050
50 152.835
60 158.660 201.475 242.265 283.265
65 160.615 203.483 244.195 285.335
39.210 42.608 40.534 40.815
Temperature, °F
0
5
10
15
20
25
30
35
40
45
50
55
60
65
25.32 25.32 25.32 25.32
1.100 1.100 1.100 1.100
25.40 25.40 25.40 25.40
34.315 36.783 34.800 35.056
Gravimetric Gravimetric Gravimetric Gravimetric
H₂O H₂O H₂O H₂O
H₂O H₂O H₂O H₂O
Empty Empty Empty Empty
Silica Silica Silica Silica
298.6 311.5 287.1 304.4
14.052 14.659 13.511 14.325
0.291 0.285 0.280 0.290
2.0 9.1 4.2 4.9
29.89 29.85 29.86 29.83
62 of 135
Run 1 - RM Data
Location:
Source:
Project No.:
Date:
Time O₂ - Outlet CO₂ - Outlet CO - Outlet NOx - Outlet SO₂ - Outlet THC - Outlet
Unit % dry % dry ppmvd ppmvd ppmvd ppmvw
Status Valid Valid Valid Valid Valid Valid
Uncorrected Run Average (Cobs)9.09 9.09 5.02 109.49 0.53 1.30
Cal Gas Concentration (CMA)10.99 11.10 25.00 250.00 10.00 10.00
Pretest System Zero Response 0.01 0.06 0.09 0.12 0.03 0.00
Posttest System Zero Response -0.09 0.06 -0.19 0.66 0.06 0.00
Average Zero Response (Co)-0.04 0.06 -0.05 0.39 0.05 0.00
Pretest System Cal Response 10.95 10.81 24.96 244.31 9.96 10.33
Posttest System Cal Response 10.80 10.91 24.92 246.83 10.08 10.13
Average Cal Response (CM)10.88 10.86 24.94 245.57 10.02 10.23
Corrected Run Average (Corr)9.19 9.28 5.07 111.24 0.49 NA
11:28 10.13 8.31 1.04 120.76 0.28 1.50
11:29 8.41 9.65 1.0 116.05 0.37 0.91
11:30 8.06 9.91 6.28 111.59 0.44 0.90
11:31 8.86 9.50 50.00 107.56 0.18 0.91
11:32 12.27 6.57 32.15 101.32 0.26 0.96
11:33 12.06 6.78 3.06 82.52 0.50 0.86
11:34 9.82 8.51 1.35 85.71 0.50 0.31
11:35 10.62 7.92 1.15 95.27 0.55 0.00
11:36 10.20 8.24 1.14 99.80 0.40 0.00
11:37 9.42 8.85 1.10 113.51 0.46 0.63
11:38 8.65 9.49 1.04 123.03 0.44 1.79
11:39 9.19 9.12 0.95 124.29 0.47 2.25
11:40 8.84 9.28 0.93 114.72 0.55 2.16
11:41 8.08 9.89 0.92 109.82 0.60 2.17
11:42 8.57 9.51 1.08 111.02 0.59 1.89
11:43 7.71 10.02 1.60 110.75 0.67 1.72
11:44 8.33 9.58 0.94 102.69 0.63 1.81
11:45 7.98 9.88 0.95 105.56 0.78 1.57
11:46 8.07 9.83 0.94 113.97 0.71 1.64
11:47 8.50 9.51 0.97 114.79 0.67 1.58
11:48 8.25 9.70 0.98 121.86 0.80 1.52
11:49 7.98 9.95 0.96 122.15 0.89 1.46
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
5/8/24
63 of 135
Run 2 - RM Data
Location:
Source:
Project No.:
Date:
Time O₂ - Outlet CO₂ - Outlet CO - Outlet NOx - Outlet SO₂ - Outlet THC - Outlet
Unit % dry % dry ppmvd ppmvd ppmvd ppmvw
Status Valid Valid Valid Valid Valid Valid
Uncorrected Run Average (Cobs)8.57 9.57 2.25 115.13 0.87 1.04
Cal Gas Concentration (CMA)10.99 11.10 25.00 250.00 10.00 10.00
Pretest System Zero Response 0.01 0.06 0.09 0.12 0.03 0.00
Posttest System Zero Response -0.09 0.06 -0.19 0.66 0.06 0.00
Average Zero Response (Co)-0.04 0.06 -0.05 0.39 0.05 0.00
Pretest System Cal Response 10.95 10.81 24.96 244.31 9.96 10.33
Posttest System Cal Response 10.80 10.91 24.92 246.83 10.08 10.13
Average Cal Response (CM)10.88 10.86 24.94 245.57 10.02 10.23
Corrected Run Average (Corr)8.67 9.77 2.30 116.99 0.82 NA
11:50 8.20 9.77 0.96 124.10 0.89 1.43
11:51 7.79 10.21 0.93 122.91 0.77 1.42
11:52 8.06 9.97 0.93 122.60 0.80 1.26
11:53 8.07 10.02 0.96 118.91 1.06 1.27
11:54 8.63 9.58 0.98 121.93 1.27 1.52
11:55 9.65 8.81 0.97 122.57 1.22 1.49
11:56 9.59 8.84 0.94 117.11 1.31 1.29
11:57 10.20 8.38 0.93 111.37 1.40 0.86
11:58 9.40 8.99 0.91 104.25 1.37 1.38
11:59 9.68 8.80 0.92 104.59 1.20 1.31
12:00 10.22 8.32 0.92 110.00 0.84 0.73
12:01 8.69 9.41 0.97 106.44 0.70 0.78
12:02 7.92 10.05 0.96 108.42 0.77 0.75
12:03 8.09 9.95 0.99 107.84 0.52 0.87
12:04 8.23 9.80 0.96 109.88 0.43 0.80
12:05 8.13 9.81 0.95 117.41 0.40 0.81
12:06 7.90 9.98 1.12 118.68 0.51 0.79
12:07 7.52 10.27 25.24 117.58 0.74 0.77
12:08 8.15 9.85 3.66 115.15 0.63 0.77
12:09 7.95 9.99 1.05 114.14 0.70 0.78
12:10 7.82 10.11 0.99 121.76 0.69 0.78
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
5/8/24
64 of 135
Run 3 - RM Data
Location:
Source:
Project No.:
Date:
Time O₂ - Outlet CO₂ - Outlet CO - Outlet NOx - Outlet SO₂ - Outlet THC - Outlet
Unit % dry % dry ppmvd ppmvd ppmvd ppmvw
Status Valid Valid Valid Valid Valid Valid
Uncorrected Run Average (Cobs)8.21 9.70 0.97 134.30 0.80 0.78
Cal Gas Concentration (CMA)10.99 11.10 25.00 250.00 10.00 10.00
Pretest System Zero Response 0.01 0.06 0.09 0.12 0.03 0.00
Posttest System Zero Response -0.09 0.06 -0.19 0.66 0.06 0.00
Average Zero Response (Co)-0.04 0.06 -0.05 0.39 0.05 0.00
Pretest System Cal Response 10.95 10.81 24.96 244.31 9.96 10.33
Posttest System Cal Response 10.80 10.91 24.92 246.83 10.08 10.13
Average Cal Response (CM)10.88 10.86 24.94 245.57 10.02 10.23
Corrected Run Average (Corr)8.31 9.91 1.02 136.54 0.76 NA
12:11 7.72 10.15 0.98 115.65 0.82 0.78
12:12 7.40 10.41 1.01 115.44 0.83 0.72
12:13 7.25 10.48 1.00 127.98 0.73 0.68
12:14 7.34 10.40 1.00 123.18 0.68 0.74
12:15 7.77 10.05 0.96 132.72 0.66 0.93
12:16 8.04 9.82 1.00 133.52 0.91 0.79
12:17 7.78 10.02 0.96 135.61 0.87 0.79
12:18 7.99 9.91 0.95 137.55 0.91 0.79
12:19 8.03 9.83 0.96 132.45 0.66 0.77
12:20 8.08 9.80 0.96 137.44 0.49 0.76
12:21 8.43 9.57 0.98 136.06 0.78 0.77
12:22 8.33 9.61 0.99 141.08 0.67 0.84
12:23 8.27 9.65 0.99 139.50 0.83 0.77
12:24 8.45 9.50 0.97 136.84 0.82 0.73
12:25 8.53 9.47 0.98 132.04 0.71 0.75
12:26 8.88 9.27 0.96 139.08 0.60 0.76
12:27 8.72 9.29 0.94 139.52 0.44 0.76
12:28 8.35 9.55 0.91 142.13 0.66 0.76
12:29 8.87 9.18 0.94 137.28 0.79 0.80
12:30 9.17 8.87 0.97 141.18 1.23 0.80
12:31 9.01 8.97 0.97 144.09 1.76 0.82
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
5/8/24
65 of 135
Run 4 - RM Data
Location:
Source:
Project No.:
Date:
Time O₂ - Outlet CO₂ - Outlet CO - Outlet NOx - Outlet SO₂ - Outlet THC - Outlet
Unit % dry % dry ppmvd ppmvd ppmvd ppmvw
Status Valid Valid Valid Valid Valid Valid
Uncorrected Run Average (Cobs)8.83 9.35 1.00 135.04 1.64 0.57
Cal Gas Concentration (CMA)10.99 11.10 25.00 250.00 10.00 10.00
Pretest System Zero Response -0.09 0.06 -0.19 0.66 0.06 0.00
Posttest System Zero Response -0.20 0.05 -0.28 1.10 0.03 0.02
Average Zero Response (Co)-0.15 0.06 -0.24 0.88 0.05 0.01
Pretest System Cal Response 10.80 10.91 24.92 246.83 10.08 10.13
Posttest System Cal Response 10.71 10.95 24.67 246.34 9.88 10.01
Average Cal Response (CM)10.76 10.93 24.80 246.59 9.98 10.07
Corrected Run Average (Corr)9.05 9.48 1.23 136.51 1.61 NA
13:27 9.28 9.04 0.81 142.28 1.27 0.12
13:28 9.21 9.08 0.80 150.07 1.39 0.70
13:29 8.81 9.36 0.80 144.63 1.69 1.17
13:30 8.54 9.55 0.82 141.55 1.49 1.32
13:31 8.48 9.60 0.83 140.29 1.45 1.32
13:32 8.24 9.75 0.90 139.48 1.36 1.24
13:33 8.12 9.80 0.93 132.74 1.45 1.00
13:34 8.03 9.87 0.93 132.28 1.48 0.62
13:35 7.88 10.00 0.89 137.42 1.24 0.37
13:36 7.55 10.33 2.76 131.16 1.55 0.35
13:37 7.89 10.10 1.09 124.54 1.74 0.41
13:38 8.25 9.74 0.94 122.97 1.87 0.42
13:39 8.01 9.99 0.94 135.44 1.87 0.43
13:40 8.76 9.41 0.90 139.72 1.72 -0.24
13:41 9.29 9.06 0.90 135.30 1.70 -0.30
13:42 9.60 8.82 0.88 136.02 1.94 -0.30
13:43 10.95 7.79 0.88 134.99 1.90 0.17
13:44 10.15 8.32 0.90 129.14 1.81 0.71
13:45 9.51 8.86 0.97 121.80 1.87 0.92
13:46 9.47 8.88 0.98 135.07 1.84 0.84
13:47 9.37 8.94 1.05 128.98 1.91 0.78
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
5/8/24
66 of 135
Run 5 - RM Data
Location:
Source:
Project No.:
Date:
Time O₂ - Outlet CO₂ - Outlet CO - Outlet NOx - Outlet SO₂ - Outlet THC - Outlet
Unit % dry % dry ppmvd ppmvd ppmvd ppmvw
Status Valid Valid Valid Valid Valid Valid
Uncorrected Run Average (Cobs)8.72 9.33 5.69 125.47 2.18 0.59
Cal Gas Concentration (CMA)10.99 11.10 25.00 250.00 10.00 10.00
Pretest System Zero Response -0.09 0.06 -0.19 0.66 0.06 0.00
Posttest System Zero Response -0.20 0.05 -0.28 1.10 0.03 0.02
Average Zero Response (Co)-0.15 0.06 -0.24 0.88 0.05 0.01
Pretest System Cal Response 10.80 10.91 24.92 246.83 10.08 10.13
Posttest System Cal Response 10.71 10.95 24.67 246.34 9.88 10.01
Average Cal Response (CM)10.76 10.93 24.80 246.59 9.98 10.07
Corrected Run Average (Corr)8.93 9.47 5.92 126.77 2.15 NA
13:48 9.25 9.02 1.06 127.08 1.84 0.80
13:49 9.34 8.94 1.02 130.07 1.82 0.78
13:50 9.26 9.03 1.06 132.06 1.90 0.75
13:51 9.17 9.09 1.05 128.31 1.88 0.66
13:52 9.04 9.14 1.07 128.59 2.08 0.34
13:53 8.75 9.31 1.05 125.01 2.20 0.69
13:54 8.89 9.22 1.08 124.57 2.20 0.30
13:55 8.88 9.21 1.10 123.42 2.18 0.30
13:56 8.82 9.19 1.13 132.63 2.18 2.79
13:57 8.14 9.69 1.18 122.64 2.28 0.42
13:58 7.73 10.03 1.17 115.69 2.41 0.74
13:59 7.72 10.04 1.20 118.87 2.32 0.86
14:00 7.51 10.20 34.88 111.90 2.24 0.75
14:01 7.92 9.89 49.65 111.40 2.29 0.42
14:02 9.63 8.65 12.90 111.58 2.42 0.24
14:03 9.45 8.68 2.23 134.23 2.15 0.23
14:04 8.66 9.30 1.61 120.62 2.01 0.26
14:05 8.43 9.50 1.39 125.78 2.31 0.27
14:06 8.44 9.50 1.32 130.92 2.40 0.28
14:07 8.89 9.24 1.22 139.08 2.52 0.29
14:08 9.11 9.03 1.18 140.38 2.19 0.28
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
5/8/24
67 of 135
Run 6 - RM Data
Location:
Source:
Project No.:
Date:
Time O₂ - Outlet CO₂ - Outlet CO - Outlet NOx - Outlet SO₂ - Outlet THC - Outlet
Unit % dry % dry ppmvd ppmvd ppmvd ppmvw
Status Valid Valid Valid Valid Valid Valid
Uncorrected Run Average (Cobs)9.40 8.76 1.12 143.01 2.30 0.18
Cal Gas Concentration (CMA)10.99 11.10 25.00 250.00 10.00 10.00
Pretest System Zero Response -0.09 0.06 -0.19 0.66 0.06 0.00
Posttest System Zero Response -0.20 0.05 -0.28 1.10 0.03 0.02
Average Zero Response (Co)-0.15 0.06 -0.24 0.88 0.05 0.01
Pretest System Cal Response 10.80 10.91 24.92 246.83 10.08 10.13
Posttest System Cal Response 10.71 10.95 24.67 246.34 9.88 10.01
Average Cal Response (CM)10.76 10.93 24.80 246.59 9.98 10.07
Corrected Run Average (Corr)9.63 8.88 1.35 144.61 2.27 NA
14:09 9.13 8.99 1.12 141.87 1.98 0.27
14:10 9.26 8.90 1.08 141.04 2.02 0.26
14:11 9.15 8.94 1.07 134.40 2.36 0.25
14:12 9.32 8.85 1.04 137.21 2.34 0.26
14:13 9.68 8.58 1.09 140.09 2.27 0.22
14:14 9.69 8.53 1.10 137.41 2.14 0.22
14:15 9.82 8.44 1.07 138.56 2.15 0.24
14:16 9.88 8.39 1.10 136.46 2.09 0.24
14:17 9.97 8.31 1.11 129.65 2.36 -0.28
14:18 9.98 8.34 1.13 124.22 2.31 -0.50
14:19 9.89 8.40 1.17 133.52 2.34 -0.05
14:20 9.66 8.53 1.19 152.82 2.46 0.41
14:21 9.26 8.83 1.12 160.76 2.46 0.56
14:22 9.03 9.02 1.08 152.06 2.23 0.63
14:23 9.17 8.90 1.05 144.69 2.25 0.65
14:24 9.09 8.96 1.11 144.56 2.41 0.46
14:25 9.01 9.04 1.07 151.11 2.41 0.07
14:26 9.16 8.94 1.11 150.80 2.48 0.03
14:27 9.04 9.05 1.19 143.62 2.37 0.00
14:28 8.99 9.10 1.32 150.66 2.34 -0.01
14:29 9.26 8.85 1.16 157.61 2.63 -0.08
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
5/8/24
68 of 135
Run 7 - RM Data
Location:
Source:
Project No.:
Date:
Time O₂ - Outlet CO₂ - Outlet CO - Outlet NOx - Outlet SO₂ - Outlet THC - Outlet
Unit % dry % dry ppmvd ppmvd ppmvd ppmvw
Status Valid Valid Valid Valid Valid Valid
Uncorrected Run Average (Cobs)8.58 9.68 5.55 142.29 1.02 0.19
Cal Gas Concentration (CMA)10.99 11.10 25.00 250.00 10.00 10.00
Pretest System Zero Response -0.20 0.05 -0.28 1.10 0.03 0.02
Posttest System Zero Response -0.04 0.09 -0.33 1.16 0.35 -0.40
Average Zero Response (Co)-0.12 0.07 -0.31 1.13 0.19 -0.19
Pretest System Cal Response 10.71 10.95 24.67 246.34 9.88 10.01
Posttest System Cal Response 10.81 10.99 24.67 246.85 10.06 9.92
Average Cal Response (CM)10.76 10.97 24.67 246.60 9.97 9.97
Corrected Run Average (Corr)8.79 9.78 5.86 143.77 0.85 NA
14:59 8.34 9.73 1.14 119.13 1.09 0.34
15:00 8.72 9.46 1.16 126.21 0.62 0.59
15:01 8.11 9.91 1.22 145.12 0.61 0.29
15:02 7.83 10.16 1.18 151.69 0.55 0.28
15:03 8.02 10.06 1.18 139.27 0.59 0.25
15:04 8.75 9.54 1.16 138.23 0.49 0.22
15:05 8.66 9.57 1.18 143.37 0.74 0.24
15:06 8.11 10.04 1.20 147.33 0.90 0.20
15:07 8.54 9.75 1.25 144.25 0.99 0.21
15:08 8.69 9.73 1.38 135.13 1.02 0.20
15:09 8.75 9.62 1.35 143.77 1.04 0.20
15:10 8.34 9.95 2.18 145.81 1.02 0.19
15:11 7.59 10.55 46.81 137.05 1.10 0.17
15:12 7.75 10.50 42.24 118.44 1.13 0.09
15:13 8.62 9.76 4.74 110.26 1.27 -0.04
15:14 9.03 9.39 1.40 116.85 1.08 -0.01
15:15 9.11 9.26 1.20 144.55 1.45 0.11
15:16 9.53 8.92 1.21 150.81 1.62 0.13
15:17 8.98 9.30 1.18 163.59 1.70 0.21
15:18 9.30 9.07 1.11 192.62 1.39 0.18
15:19 9.39 8.98 1.11 174.61 1.12 0.00
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
5/8/24
69 of 135
Run 8 - RM Data
Location:
Source:
Project No.:
Date:
Time O₂ - Outlet CO₂ - Outlet CO - Outlet NOx - Outlet SO₂ - Outlet THC - Outlet
Unit % dry % dry ppmvd ppmvd ppmvd ppmvw
Status Valid Valid Valid Valid Valid Valid
Uncorrected Run Average (Cobs)9.42 8.83 1.02 171.43 0.58 0.18
Cal Gas Concentration (CMA)10.99 11.10 25.00 250.00 10.00 10.00
Pretest System Zero Response -0.20 0.05 -0.28 1.10 0.03 0.02
Posttest System Zero Response -0.04 0.09 -0.33 1.16 0.35 -0.40
Average Zero Response (Co)-0.12 0.07 -0.31 1.13 0.19 -0.19
Pretest System Cal Response 10.71 10.95 24.67 246.34 9.88 10.01
Posttest System Cal Response 10.81 10.99 24.67 246.85 10.06 9.92
Average Cal Response (CM)10.76 10.97 24.67 246.60 9.97 9.97
Corrected Run Average (Corr)9.64 8.92 1.33 173.45 0.39 NA
15:20 9.32 9.00 1.09 169.55 1.09 -0.05
15:21 9.52 8.87 1.09 169.66 0.99 0.00
15:22 9.62 8.76 1.07 178.89 0.65 0.10
15:23 10.08 8.38 1.07 183.07 0.53 0.18
15:24 10.18 8.29 1.11 182.28 0.55 0.21
15:25 9.63 8.68 1.08 186.85 0.69 0.20
15:26 9.59 8.71 1.09 194.35 0.46 0.01
15:27 9.45 8.80 1.04 192.59 0.39 -0.13
15:28 9.22 8.92 0.97 187.96 0.41 -0.20
15:29 9.42 8.78 0.93 170.79 0.48 -0.31
15:30 9.35 8.83 0.97 162.45 0.66 0.28
15:31 9.53 8.67 0.99 155.45 0.68 0.56
15:32 9.40 8.78 1.03 151.81 0.37 0.53
15:33 9.46 8.71 0.98 162.22 0.29 0.48
15:34 9.20 8.92 1.01 164.52 0.49 0.49
15:35 9.14 9.01 0.99 171.06 0.48 0.14
15:36 9.17 9.04 0.95 170.25 0.65 1.12
15:37 9.37 8.88 0.98 157.11 0.58 0.35
15:38 9.16 9.04 0.96 145.19 0.60 0.01
15:39 8.94 9.19 1.01 173.00 0.42 0.00
15:40 9.04 9.17 1.02 171.07 0.62 -0.19
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
5/8/24
70 of 135
Run 9 - RM Data
Location:
Source:
Project No.:
Date:
Time O₂ - Outlet CO₂ - Outlet CO - Outlet NOx - Outlet SO₂ - Outlet THC - Outlet
Unit % dry % dry ppmvd ppmvd ppmvd ppmvw
Status Valid Valid Valid Valid Valid Valid
Uncorrected Run Average (Cobs)8.92 9.22 0.99 185.65 0.61 -0.03
Cal Gas Concentration (CMA)10.99 11.10 25.00 250.00 10.00 10.00
Pretest System Zero Response -0.20 0.05 -0.28 1.10 0.03 0.02
Posttest System Zero Response -0.04 0.09 -0.33 1.16 0.35 -0.40
Average Zero Response (Co)-0.12 0.07 -0.31 1.13 0.19 -0.19
Pretest System Cal Response 10.71 10.95 24.67 246.34 9.88 10.01
Posttest System Cal Response 10.81 10.99 24.67 246.85 10.06 9.92
Average Cal Response (CM)10.76 10.97 24.67 246.60 9.97 9.97
Corrected Run Average (Corr)9.13 9.32 1.30 187.93 0.43 NA
15:41 9.31 8.92 0.94 169.11 0.55 -0.11
15:42 9.67 8.69 0.95 165.13 0.68 -0.03
15:43 9.65 8.67 1.01 168.28 0.56 -0.12
15:44 9.28 8.94 1.05 191.07 0.34 0.00
15:45 8.56 9.52 1.00 197.14 0.48 0.05
15:46 8.91 9.27 0.94 194.41 0.58 0.06
15:47 9.00 9.21 0.94 175.78 0.81 -0.19
15:48 9.12 9.06 0.97 183.29 0.53 -0.18
15:49 8.71 9.39 0.99 181.65 0.62 -0.63
15:50 8.96 9.17 1.00 190.00 0.71 0.04
15:51 9.04 9.11 1.03 182.05 0.90 0.09
15:52 8.77 9.35 1.02 208.82 0.76 -0.17
15:53 8.91 9.25 0.96 217.51 0.70 -0.21
15:54 8.88 9.26 1.00 189.57 0.70 -0.02
15:55 8.55 9.50 0.97 192.11 0.57 0.13
15:56 8.48 9.51 1.01 185.41 0.63 0.08
15:57 8.54 9.47 0.99 173.47 0.63 0.09
15:58 8.59 9.43 1.01 173.06 0.45 0.20
15:59 8.92 9.22 1.02 186.63 0.58 0.32
16:00 8.83 9.30 1.04 188.23 0.32 0.19
16:01 8.69 9.36 1.00 186.01 0.68 -0.18
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
5/8/24
71 of 135
Run 10 - RM Data
Location:
Source:
Project No.:
Date:
Time O₂ - Outlet CO₂ - Outlet CO - Outlet NOx - Outlet SO₂ - Outlet THC - Outlet
Unit % dry % dry ppmvd ppmvd ppmvd ppmvw
Status Valid Valid Valid Valid Valid Valid
Uncorrected Run Average (Cobs)8.61 9.60 6.38 142.65 0.44 -0.12
Cal Gas Concentration (CMA)10.99 11.10 25.00 250.00 10.00 10.00
Pretest System Zero Response -0.04 0.09 -0.33 1.16 0.35 -0.40
Posttest System Zero Response -0.08 0.08 -0.35 1.16 0.03 -0.26
Average Zero Response (Co)-0.06 0.09 -0.34 1.16 0.19 -0.33
Pretest System Cal Response 10.81 10.99 24.67 246.85 10.06 9.92
Posttest System Cal Response 10.78 11.01 24.67 246.34 10.17 9.96
Average Cal Response (CM)10.80 11.00 24.67 246.60 10.12 9.94
Corrected Run Average (Corr)8.77 9.68 6.72 144.12 0.25 NA
16:25 8.07 10.06 1.29 145.16 1.03 -0.12
16:26 8.29 9.89 1.42 148.17 0.98 -0.20
16:27 7.08 10.83 48.41 148.93 0.72 -0.15
16:28 8.02 10.08 36.11 144.50 0.53 -0.08
16:29 8.95 9.34 3.27 121.98 0.70 -0.09
16:30 8.82 9.44 1.50 135.75 0.37 -0.13
16:31 8.50 9.67 1.36 139.34 0.39 -0.13
16:32 8.33 9.79 1.25 152.00 0.26 -0.11
16:33 8.78 9.41 1.16 156.01 0.23 -0.08
16:34 9.32 9.02 1.11 155.67 0.43 -0.06
16:35 9.01 9.26 1.07 165.42 0.41 -0.08
16:36 8.85 9.38 1.03 162.95 0.36 -0.12
16:37 9.03 9.24 0.99 153.04 0.62 -0.23
16:38 9.16 9.13 0.97 149.45 0.33 -0.04
16:39 9.29 9.04 1.00 145.79 0.20 -0.11
16:40 8.94 9.31 0.95 146.33 0.21 -0.12
16:41 8.52 9.64 0.90 147.72 0.18 -0.06
16:42 8.01 10.07 16.16 142.68 0.12 -0.23
16:43 8.04 10.07 11.98 122.86 0.38 -0.21
16:44 8.43 9.76 1.13 103.95 0.51 -0.16
16:45 9.30 9.18 0.96 107.87 0.32 -0.08
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
5/8/24
72 of 135
Run 11 - RM Data
Location:
Source:
Project No.:
Date:
Time O₂ - Outlet CO₂ - Outlet CO - Outlet NOx - Outlet SO₂ - Outlet THC - Outlet
Unit % dry % dry ppmvd ppmvd ppmvd ppmvw
Status Valid Valid Valid Valid Valid Valid
Uncorrected Run Average (Cobs)9.55 9.01 0.96 131.19 0.32 -0.10
Cal Gas Concentration (CMA)10.99 11.10 25.00 250.00 10.00 10.00
Pretest System Zero Response -0.04 0.09 -0.33 1.16 0.35 -0.40
Posttest System Zero Response -0.08 0.08 -0.35 1.16 0.03 -0.26
Average Zero Response (Co)-0.06 0.09 -0.34 1.16 0.19 -0.33
Pretest System Cal Response 10.81 10.99 24.67 246.85 10.06 9.92
Posttest System Cal Response 10.78 11.01 24.67 246.34 10.17 9.96
Average Cal Response (CM)10.80 11.00 24.67 246.60 10.12 9.94
Corrected Run Average (Corr)9.73 9.08 1.30 132.44 0.13 NA
16:46 9.75 8.78 0.93 130.25 0.41 -0.08
16:47 9.70 8.82 0.91 139.53 0.58 -0.24
16:48 9.67 8.86 0.90 137.44 0.25 -0.41
16:49 9.31 9.21 0.92 138.46 0.42 -0.25
16:50 9.53 9.05 0.92 144.81 0.58 -0.04
16:51 9.93 8.77 0.92 141.23 0.39 -0.22
16:52 10.25 8.47 0.86 139.07 0.23 -0.20
16:53 10.15 8.55 0.86 129.53 0.39 -0.26
16:54 10.27 8.49 0.87 128.11 0.22 -0.29
16:55 10.19 8.53 0.90 129.36 0.21 -0.31
16:56 9.95 8.68 0.92 129.69 0.19 -0.18
16:57 8.57 9.72 0.94 132.79 0.29 -0.11
16:58 8.21 10.05 0.95 120.18 0.27 -0.05
16:59 8.47 9.85 1.00 111.25 0.45 -0.07
17:00 8.72 9.69 1.06 121.48 0.34 -0.07
17:01 8.92 9.54 1.07 127.24 0.17 -0.16
17:02 9.24 9.27 1.06 128.07 0.15 -0.15
17:03 9.40 9.18 1.06 131.86 0.26 -0.06
17:04 9.69 8.90 1.03 129.51 0.40 0.02
17:05 10.42 8.34 1.04 132.59 0.14 0.39
17:06 10.24 8.44 1.04 132.46 0.37 0.58
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
5/8/24
73 of 135
Run 12 - RM Data
Location:
Source:
Project No.:
Date:
Time O₂ - Outlet CO₂ - Outlet CO - Outlet NOx - Outlet SO₂ - Outlet THC - Outlet
Unit % dry % dry ppmvd ppmvd ppmvd ppmvw
Status Valid Valid Valid Valid Valid Valid
Uncorrected Run Average (Cobs)10.19 8.33 1.06 114.19 0.24 -0.06
Cal Gas Concentration (CMA)10.99 11.10 25.00 250.00 10.00 10.00
Pretest System Zero Response -0.04 0.09 -0.33 1.16 0.35 -0.40
Posttest System Zero Response -0.08 0.08 -0.35 1.16 0.03 -0.26
Average Zero Response (Co)-0.06 0.09 -0.34 1.16 0.19 -0.33
Pretest System Cal Response 10.81 10.99 24.67 246.85 10.06 9.92
Posttest System Cal Response 10.78 11.01 24.67 246.34 10.17 9.96
Average Cal Response (CM)10.80 11.00 24.67 246.60 10.12 9.94
Corrected Run Average (Corr)10.38 8.38 1.40 115.13 0.05 NA
17:07 10.18 8.48 1.05 127.17 0.37 0.03
17:08 9.91 8.66 1.05 124.34 0.29 -0.02
17:09 9.74 8.80 1.06 125.72 0.28 -0.02
17:10 9.87 8.69 1.05 127.49 0.38 -0.19
17:11 10.05 8.54 1.05 124.21 0.28 -0.21
17:12 10.18 8.40 1.08 122.21 0.28 -0.23
17:13 9.86 8.60 1.06 116.82 0.38 -0.19
17:14 10.16 8.38 1.06 117.85 0.39 -0.23
17:15 10.35 8.20 1.05 114.86 0.32 -0.25
17:16 10.51 8.07 1.01 113.09 0.15 -0.21
17:17 10.52 8.03 0.99 112.32 0.07 0.95
17:18 10.87 7.74 1.03 108.80 0.07 0.53
17:19 11.08 7.56 1.01 106.92 0.14 -0.13
17:20 10.68 7.88 1.01 105.39 0.12 -0.19
17:21 10.85 7.77 1.04 106.63 0.21 -0.20
17:22 10.98 7.65 1.08 107.85 0.15 -0.20
17:23 10.75 7.81 1.12 103.63 0.20 -0.14
17:24 10.02 8.36 1.17 108.01 0.23 -0.09
17:25 9.29 8.97 1.20 114.52 0.13 -0.14
17:26 9.34 8.99 1.16 105.20 0.23 0.02
17:27 8.83 9.32 0.96 104.98 0.30 -0.23
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
5/8/24
74 of 135

Appendix C

75 of 135
QA Data
Location
Source
Project No.
O₂ - Outlet CO₂ - Outlet CO - Outlet NOx - Outlet SO₂ - Outlet THC - Outlet
Make Servomex Servomex Thermo Thermo Ametek Thermo
Model 1400 1440 48C 42C-HL 9900 55i-2
S/N 1420-4 1415C-2 48CTL-74507-376 42CHL-59778-324 9900-S1562-1 1209052150
Operating Range 25 25 50 500 25 20
Cylinder ID
Zero NA NA NA NA NA NA
Mid RR04251 RR04251 EB0097304 EB0011606 SG9170578BAL EB0091184
High CC749479 CC749479 EB0097304 EB0011606 SG9170578BAL EB0091184
Cylinder Certifed Values
Zero NA NA NA NA NA NA
Mid 10.99 11.1 50.39 501 50.39 29.72
High 23.02 22.93 50.39 501 50.39 29.72
Cylinder Expiration Date
Zero NA NA NA NA NA NA
Mid 9/19/31 9/19/31 10/20/30 9/16/31 10/18/30 2/20/25
High 1/16/31 1/16/31 10/20/30 9/16/31 10/18/30 2/20/25
Type of Sample Line Heated Sample Line
Parameter
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
76 of 135
Calibration Data
Location:
Source:
Project No.:
Date:
O₂ - Outlet CO₂ - Outlet CO - Outlet NOx - Outlet SO₂ - Outlet THC - Outlet
Expected Average Concentration 10.00 10.00 10.00 250.00 5.00 10.00
Span Between
Low 10.00 10.00 10.00 250.00 5.00 15.00
High 50.00 50.00 50.00 1250.00 25.00 25.00
Desired Span 23.02 22.93 50.00 500.00 20.00 20.00
Low Range Gas
Low NA NA NA NA NA 5.00
High NA NA NA NA NA 7.00
Mid Range Gas
Low 9.21 9.17 20.00 200.00 8.00 9.00
High 13.81 13.76 30.00 300.00 12.00 11.00
High Range Gas
Low NA NA NA NA NA 16.00
High NA NA NA NA NA 18.00
Actual Concentration (% or ppm)
Zero 0.00 0.00 0.00 0.00 0.00 0.00
Low NA NA NA NA NA 6.00
Mid 10.99 11.10 25.00 250.00 10.00 10.00
High 23.02 22.93 50.00 500.00 20.00 17.00
Response Time (seconds)30.00 30.00 30.00 60.00 60.00 60.00
Upscale Calibration Gas (CMA)Mid Mid Mid Mid Mid Mid
Instrument Response (% or ppm)
Zero -0.06 0.02 -0.03 0.09 0.03 0.00
Low NA NA NA NA NA 6.19
Mid 10.98 10.87 25.04 249.57 9.96 10.33
High 23.01 22.98 49.99 497.52 20.09 17.02
Performance (% of Span or Cal. Gas Conc.)
Zero 0.26 0.09 0.06 0.02 0.15 0.00
Low NA NA NA NA NA 3.05
Mid 0.04 1.00 0.08 0.09 0.20 3.18
High 0.04 0.22 0.02 0.50 0.45 0.00
Status
Zero PASS PASS PASS PASS PASS PASS
Low NA NA NA NA NA PASS
Mid PASS PASS PASS PASS PASS PASS
High PASS PASS PASS PASS PASS PASS
Incinerator System (INC)
Clean Harbors Aragonite LLC - Aragonite, UT
Parameter
5/8/24
AST-2024-1517
77 of 135
Bias/Drift Determinations
Location:
Source:
Project No.:
O₂ - Outlet CO₂ - Outlet CO - Outlet NOx - Outlet SO₂ - Outlet THC - Outlet
Pretest System Zero Response 0.01 0.06 0.09 0.12 0.03 0.00
Posttest System Zero Response -0.09 0.06 -0.19 0.66 0.06 0.00
Pretest System Upscale Response 10.95 10.81 24.96 244.31 9.96 10.33
Posttest System Upscale Response 10.80 10.91 24.92 246.83 10.08 10.13
Pretest System Zero Response 0.01 0.06 0.09 0.12 0.03 0.00
Posttest System Zero Response -0.09 0.06 -0.19 0.66 0.06 0.00
Pretest System Upscale Response 10.95 10.81 24.96 244.31 9.96 10.33
Posttest System Upscale Response 10.80 10.91 24.92 246.83 10.08 10.13
Pretest System Zero Response 0.01 0.06 0.09 0.12 0.03 0.00
Posttest System Zero Response -0.09 0.06 -0.19 0.66 0.06 0.00
Pretest System Upscale Response 10.95 10.81 24.96 244.31 9.96 10.33
Posttest System Upscale Response 10.80 10.91 24.92 246.83 10.08 10.13
Pretest System Zero Response -0.09 0.06 -0.19 0.66 0.06 0.00
Posttest System Zero Response -0.20 0.05 -0.28 1.10 0.03 0.02
Pretest System Upscale Response 10.80 10.91 24.92 246.83 10.08 10.13
Posttest System Upscale Response 10.71 10.95 24.67 246.34 9.88 10.01
Pretest System Zero Response -0.09 0.06 -0.19 0.66 0.06 0.00
Posttest System Zero Response -0.20 0.05 -0.28 1.10 0.03 0.02
Pretest System Upscale Response 10.80 10.91 24.92 246.83 10.08 10.13
Posttest System Upscale Response 10.71 10.95 24.67 246.34 9.88 10.01
Pretest System Zero Response -0.09 0.06 -0.19 0.66 0.06 0.00
Posttest System Zero Response -0.20 0.05 -0.28 1.10 0.03 0.02
Pretest System Upscale Response 10.80 10.91 24.92 246.83 10.08 10.13
Posttest System Upscale Response 10.71 10.95 24.67 246.34 9.88 10.01
Pretest System Zero Response -0.20 0.05 -0.28 1.10 0.03 0.02
Posttest System Zero Response -0.04 0.09 -0.33 1.16 0.35 -0.40
Pretest System Upscale Response 10.71 10.95 24.67 246.34 9.88 10.01
Posttest System Upscale Response 10.81 10.99 24.67 246.85 10.06 9.92
Pretest System Zero Response -0.20 0.05 -0.28 1.10 0.03 0.02
Posttest System Zero Response -0.04 0.09 -0.33 1.16 0.35 -0.40
Pretest System Upscale Response 10.71 10.95 24.67 246.34 9.88 10.01
Posttest System Upscale Response 10.81 10.99 24.67 246.85 10.06 9.92
Pretest System Zero Response -0.20 0.05 -0.28 1.10 0.03 0.02
Posttest System Zero Response -0.04 0.09 -0.33 1.16 0.35 -0.40
Pretest System Upscale Response 10.71 10.95 24.67 246.34 9.88 10.01
Posttest System Upscale Response 10.81 10.99 24.67 246.85 10.06 9.92
Pretest System Zero Response -0.04 0.09 -0.33 1.16 0.35 -0.40
Posttest System Zero Response -0.08 0.08 -0.35 1.16 0.03 -0.26
Pretest System Upscale Response 10.81 10.99 24.67 246.85 10.06 9.92
Posttest System Upscale Response 10.78 11.01 24.67 246.34 10.17 9.96
Pretest System Zero Response -0.04 0.09 -0.33 1.16 0.35 -0.40
Posttest System Zero Response -0.08 0.08 -0.35 1.16 0.03 -0.26
Pretest System Upscale Response 10.81 10.99 24.67 246.85 10.06 9.92
Posttest System Upscale Response 10.78 11.01 24.67 246.34 10.17 9.96
Pretest System Zero Response -0.04 0.09 -0.33 1.16 0.35 -0.40
Posttest System Zero Response -0.08 0.08 -0.35 1.16 0.03 -0.26
Pretest System Upscale Response 10.81 10.99 24.67 246.85 10.06 9.92
Posttest System Upscale Response 10.78 11.01 24.67 246.34 10.17 9.96
Run 9
Run 10
Run 11
Run 12
Run 3
Run 4
Run 5
Run 6
Run 7
Run 8
Run 2
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Parameter
Run 1
78 of 135
Bias/Drift Determinations
Location:
Source:
Project No.:
O₂ - Outlet CO₂ - Outlet CO - Outlet NOx - Outlet SO₂ - Outlet THC - Outlet
Run 1 Date 5/8/24
Span Value 23.02 22.93 50.00 500.00 20.00 20.00
Initial Instrument Zero Cal Response -0.06 0.02 -0.03 0.09 0.03 0.00
Initial Instrument Upscale Cal Response 10.98 10.87 25.04 249.57 9.96 10.33
Pretest System Zero Response 0.01 0.06 0.09 0.12 0.03 0.00
Posttest System Zero Response -0.09 0.06 -0.19 0.66 0.06 0.00
Pretest System Upscale Response 10.95 10.81 24.96 244.31 9.96 10.33
Posttest System Upscale Response 10.80 10.91 24.92 246.83 10.08 10.13
Bias (%)
Pretest Zero 0.30 0.17 0.24 0.01 0.00 NA
Posttest Zero -0.13 0.17 -0.32 0.11 0.15 NA
Pretest Span -0.13 -0.26 -0.16 -1.05 0.00 NA
Posttest Span -0.78 0.17 -0.24 -0.55 0.60 NA
Drift (%)
Zero -0.43 0.00 -0.56 0.11 0.15 0.00
Mid -0.65 0.44 -0.08 0.50 0.60 -1.00
Run 2 Date 5/8/24
Span Value 23.02 22.93 50.00 500.00 20.00 20.00
Instrument Zero Cal Response -0.06 0.02 -0.03 0.09 0.03 0.00
Instrument Upscale Cal Response 10.98 10.87 25.04 249.57 9.96 10.33
Pretest System Zero Response 0.01 0.06 0.09 0.12 0.03 0.00
Posttest System Zero Response -0.09 0.06 -0.19 0.66 0.06 0.00
Pretest System Upscale Response 10.95 10.81 24.96 244.31 9.96 10.33
Posttest System Upscale Response 10.80 10.91 24.92 246.83 10.08 10.13
Bias (%)
Pretest Zero 0.30 0.17 0.24 0.01 0.00 NA
Posttest Zero -0.13 0.17 -0.32 0.11 0.15 NA
Pretest Span -0.13 -0.26 -0.16 -1.05 0.00 NA
Posttest Span -0.78 0.17 -0.24 -0.55 0.60 NA
Drift (%)
Zero -0.43 0.00 -0.56 0.11 0.15 0.00
Mid -0.65 0.44 -0.08 0.50 0.60 -1.00
Run 3 Date 5/8/24
Span Value 23.02 22.93 50.00 500.00 20.00 20.00
Instrument Zero Cal Response -0.06 0.02 -0.03 0.09 0.03 0.00
Instrument Upscale Cal Response 10.98 10.87 25.04 249.57 9.96 10.33
Pretest System Zero Response 0.01 0.06 0.09 0.12 0.03 0.00
Posttest System Zero Response -0.09 0.06 -0.19 0.66 0.06 0.00
Pretest System Upscale Response 10.95 10.81 24.96 244.31 9.96 10.33
Posttest System Upscale Response 10.80 10.91 24.92 246.83 10.08 10.13
Bias (%)
Pretest Zero 0.30 0.17 0.24 0.01 0.00 NA
Posttest Zero -0.13 0.17 -0.32 0.11 0.15 NA
Pretest Span -0.13 -0.26 -0.16 -1.05 0.00 NA
Posttest Span -0.78 0.17 -0.24 -0.55 0.60 NA
Drift (%)
Zero -0.43 0.00 -0.56 0.11 0.15 0.00
Mid -0.65 0.44 -0.08 0.50 0.60 -1.00
Parameter
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
79 of 135
Bias/Drift Determinations
Location:
Source:
Project No.:
O₂ - Outlet CO₂ - Outlet CO - Outlet NOx - Outlet SO₂ - Outlet THC - Outlet
Run 4 Date 5/8/24
Span Value 23.02 22.93 50.00 500.00 20.00 20.00
Instrument Zero Cal Response -0.06 0.02 -0.03 0.09 0.03 0.00
Instrument Upscale Cal Response 10.98 10.87 25.04 249.57 9.96 10.33
Pretest System Zero Response -0.09 0.06 -0.19 0.66 0.06 0.00
Posttest System Zero Response -0.20 0.05 -0.28 1.10 0.03 0.02
Pretest System Upscale Response 10.80 10.91 24.92 246.83 10.08 10.13
Posttest System Upscale Response 10.71 10.95 24.67 246.34 9.88 10.01
Bias (%)
0.13 0.17 0.32 0.11 0.15 NA
0.61 0.13 0.50 0.20 0.00 NA
0.78 0.17 0.24 0.55 0.60 NA
1.17 0.35 0.74 0.65 0.40 NA
Drift (%)
-0.48 -0.04 -0.18 0.09 -0.15 0.10
-0.39 0.17 -0.50 -0.10 -1.00 -0.60
Run 5 Date 5/8/24
Span Value 23.02 22.93 50.00 500.00 20.00 20.00
Instrument Zero Cal Response -0.06 0.02 -0.03 0.09 0.03 0.00
Instrument Upscale Cal Response 10.98 10.87 25.04 249.57 9.96 10.33
Pretest System Zero Response -0.09 0.06 -0.19 0.66 0.06 0.00
Posttest System Zero Response -0.20 0.05 -0.28 1.10 0.03 0.02
Pretest System Upscale Response 10.80 10.91 24.92 246.83 10.08 10.13
Posttest System Upscale Response 10.71 10.95 24.67 246.34 9.88 10.01
Bias (%)
0.13 0.17 0.32 0.11 0.15 NA
0.61 0.13 0.50 0.20 0.00 NA
0.78 0.17 0.24 0.55 0.60 NA
1.17 0.35 0.74 0.65 0.40 NA
Drift (%)
-0.48 -0.04 -0.18 0.09 -0.15 0.10
-0.39 0.17 -0.50 -0.10 -1.00 -0.60
Run 6 Date 5/8/24
Span Value 23.02 22.93 50.00 500.00 20.00 20.00
Instrument Zero Cal Response -0.06 0.02 -0.03 0.09 0.03 0.00
Instrument Upscale Cal Response 10.98 10.87 25.04 249.57 9.96 10.33
Pretest System Zero Response -0.09 0.06 -0.19 0.66 0.06 0.00
Posttest System Zero Response -0.20 0.05 -0.28 1.10 0.03 0.02
Pretest System Upscale Response 10.80 10.91 24.92 246.83 10.08 10.13
Posttest System Upscale Response 10.71 10.95 24.67 246.34 9.88 10.01
Bias (%)
0.13 0.17 0.32 0.11 0.15 NA
0.61 0.13 0.50 0.20 0.00 NA
0.78 0.17 0.24 0.55 0.60 NA
1.17 0.35 0.74 0.65 0.40 NA
Drift (%)
-0.48 -0.04 -0.18 0.09 -0.15 0.10
-0.39 0.17 -0.50 -0.10 -1.00 -0.60
Zero
Mid
Mid
Pretest Zero
Posttest Zero
Pretest Span
Posttest Span
Pretest Zero
Posttest Zero
Pretest Span
Posttest Span
Zero
Posttest Zero
Pretest Span
Posttest Span
Zero
Mid
Parameter
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Pretest Zero
80 of 135
Bias/Drift Determinations
Location:
Source:
Project No.:
O₂ - Outlet CO₂ - Outlet CO - Outlet NOx - Outlet SO₂ - Outlet THC - Outlet
Run 7 Date 5/8/24
Span Value 23.02 22.93 50.00 500.00 20.00 20.00
Instrument Zero Cal Response -0.06 0.02 -0.03 0.09 0.03 0.00
Instrument Upscale Cal Response 10.98 10.87 25.04 249.57 9.96 10.33
Pretest System Zero Response -0.20 0.05 -0.28 1.10 0.03 0.02
Posttest System Zero Response -0.04 0.09 -0.33 1.16 0.35 -0.40
Pretest System Upscale Response 10.71 10.95 24.67 246.34 9.88 10.01
Posttest System Upscale Response 10.81 10.99 24.67 246.85 10.06 9.92
Bias (%)
0.61 0.13 0.50 0.20 0.00 NA
0.09 0.31 0.60 0.21 1.60 NA
1.17 0.35 0.74 0.65 0.40 NA
0.74 0.52 0.74 0.54 0.50 NA
Drift (%)
0.70 0.17 -0.10 0.01 1.60 -2.10
0.43 0.17 0.00 0.10 0.90 -0.45
Run 8 Date 5/8/24
Span Value 23.02 22.93 50.00 500.00 20.00 20.00
Instrument Zero Cal Response -0.06 0.02 -0.03 0.09 0.03 0.00
Instrument Upscale Cal Response 10.98 10.87 25.04 249.57 9.96 10.33
Pretest System Zero Response -0.20 0.05 -0.28 1.10 0.03 0.02
Posttest System Zero Response -0.04 0.09 -0.33 1.16 0.35 -0.40
Pretest System Upscale Response 10.71 10.95 24.67 246.34 9.88 10.01
Posttest System Upscale Response 10.81 10.99 24.67 246.85 10.06 9.92
Bias (%)
0.61 0.13 0.50 0.20 0.00 NA
0.09 0.31 0.60 0.21 1.60 NA
1.17 0.35 0.74 0.65 0.40 NA
0.74 0.52 0.74 0.54 0.50 NA
Drift (%)
0.70 0.17 -0.10 0.01 1.60 -2.10
0.43 0.17 0.00 0.10 0.90 -0.45
Run 9 Date 5/8/24
Span Value 23.02 22.93 50.00 500.00 20.00 20.00
Instrument Zero Cal Response -0.06 0.02 -0.03 0.09 0.03 0.00
Instrument Upscale Cal Response 10.98 10.87 25.04 249.57 9.96 10.33
Pretest System Zero Response -0.20 0.05 -0.28 1.10 0.03 0.02
Posttest System Zero Response -0.04 0.09 -0.33 1.16 0.35 -0.40
Pretest System Upscale Response 10.71 10.95 24.67 246.34 9.88 10.01
Posttest System Upscale Response 10.81 10.99 24.67 246.85 10.06 9.92
Bias (%)
0.61 0.13 0.50 0.20 0.00 NA
0.09 0.31 0.60 0.21 1.60 NA
1.17 0.35 0.74 0.65 0.40 NA
0.74 0.52 0.74 0.54 0.50 NA
Drift (%)
0.70 0.17 -0.10 0.01 1.60 -2.10
0.43 0.17 0.00 0.10 0.90 -0.45
Pretest Span
Posttest Span
Zero
Mid
Pretest Span
Posttest Span
Zero
Mid
Pretest Zero
Posttest Zero
Posttest Zero
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Parameter
Pretest Zero
Posttest Zero
Pretest Span
Posttest Span
Zero
Mid
Pretest Zero
81 of 135
Bias/Drift Determinations
Location:
Source:
Project No.:
O₂ - Outlet CO₂ - Outlet CO - Outlet NOx - Outlet SO₂ - Outlet THC - Outlet
Run 10 Date 5/8/24
Span Value 23.02 22.93 50.00 500.00 20.00 20.00
Instrument Zero Cal Response -0.06 0.02 -0.03 0.09 0.03 0.00
Instrument Upscale Cal Response 10.98 10.87 25.04 249.57 9.96 10.33
Pretest System Zero Response -0.04 0.09 -0.33 1.16 0.35 -0.40
Posttest System Zero Response -0.08 0.08 -0.35 1.16 0.03 -0.26
Pretest System Upscale Response 10.81 10.99 24.67 246.85 10.06 9.92
Posttest System Upscale Response 10.78 11.01 24.67 246.34 10.17 9.96
Bias (%)
0.09 0.31 0.60 0.21 1.60 NA
0.09 0.26 0.64 0.21 0.00 NA
0.74 0.52 0.74 0.54 0.50 NA
0.87 0.61 0.74 0.65 1.05 NA
Drift (%)
-0.17 -0.04 -0.04 0.00 -1.60 0.70
-0.13 0.09 0.00 -0.10 0.55 0.20
Run 11 Date 5/8/24
Span Value 23.02 22.93 50.00 500.00 20.00 20.00
Instrument Zero Cal Response -0.06 0.02 -0.03 0.09 0.03 0.00
Instrument Upscale Cal Response 10.98 10.87 25.04 249.57 9.96 10.33
Pretest System Zero Response -0.04 0.09 -0.33 1.16 0.35 -0.40
Posttest System Zero Response -0.08 0.08 -0.35 1.16 0.03 -0.26
Pretest System Upscale Response 10.81 10.99 24.67 246.85 10.06 9.92
Posttest System Upscale Response 10.78 11.01 24.67 246.34 10.17 9.96
Bias (%)
0.09 0.31 0.60 0.21 1.60 NA
0.09 0.26 0.64 0.21 0.00 NA
0.74 0.52 0.74 0.54 0.50 NA
0.87 0.61 0.74 0.65 1.05 NA
Drift (%)
-0.17 -0.04 -0.04 0.00 -1.60 0.70
-0.13 0.09 0.00 -0.10 0.55 0.20
Run 12 Date 5/8/24
Span Value 23.02 22.93 50.00 500.00 20.00 20.00
Instrument Zero Cal Response -0.06 0.02 -0.03 0.09 0.03 0.00
Instrument Upscale Cal Response 10.98 10.87 25.04 249.57 9.96 10.33
Pretest System Zero Response -0.04 0.09 -0.33 1.16 0.35 -0.40
Posttest System Zero Response -0.08 0.08 -0.35 1.16 0.03 -0.26
Pretest System Upscale Response 10.81 10.99 24.67 246.85 10.06 9.92
Posttest System Upscale Response 10.78 11.01 24.67 246.34 10.17 9.96
Bias (%)
0.09 0.31 0.60 0.21 1.60 NA
0.09 0.26 0.64 0.21 0.00 NA
0.74 0.52 0.74 0.54 0.50 NA
0.87 0.61 0.74 0.65 1.05 NA
Drift (%)
-0.17 -0.04 -0.04 0.00 -1.60 0.70
-0.13 0.09 0.00 -0.10 0.55 0.20
Pretest Span
Posttest Span
Zero
Mid
Pretest Span
Posttest Span
Zero
Mid
Pretest Zero
Posttest Zero
Posttest Zero
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
Parameter
Pretest Zero
Posttest Zero
Pretest Span
Posttest Span
Zero
Mid
Pretest Zero
82 of 135
Balance
Red Ball Technical Gas Service
555 Craig Kennedy Way
Shreveport, LA 71107
800-551-8150
Accreditation #62754 PGVP Vendor ID # G12023
EPA PROTOCOL GAS CERTIFICATE OF ANALYSIS
Cylinder Number:CC749479 Certification Date:01/18/2023
Product ID Number:125372 Expiration Date:01/16/2031
Cylinder Pressure:1900 PSIG MFG Facility: - Shreveport - LA
COA #CC749479.20230103-0 Lot Number:CC749479.20230103
Customer PO. NO.:Tracking Number:103899767
Customer:Previous Certification Dates:
This calibration standard has been certified per the May 2012 EPA Traceability Protocol, Document EPA-600/R-12/531,
using procedure G2.
Do Not Use This Cylinder Below 100 psig (0.7 Megapascal).
Certified Concentration(s)
Component Concentration Uncertainty Analytical Principle Assayed On
Carbon Dioxide 22.93 %±0.09 %FTIR 01/18/2023
Oxygen 23.02 %±0.05 %MPA 01/10/2023
Nitrogen
Analytical Measurement Data Available Online.
Reference Standard(s)
Serial Number Lot Expiration Type Balance Component Concentration Uncertainty(%)NIST Reference
CC738486 CC738486.20211012 05/01/2030 GMIS N2 O2 19.98 %0.128 SRM 2659a
EB0097897 EB0097897.20210412 05/18/2030 GMIS N2 CO2 19.46 %0.15 C1847810.03
Analytical Instrumentation SMART-CERT
Component Principle Make MPC Date
O2 MPA Thermo 12/23/2022
CO2 FTIR MKS 01/17/2023
Serial
1162980025
017146467
This is to certify the gases referenced have been calibrated/tested, and verified to meet the defined specifications. This
calibration/test was performed using Gases or Scales that are traceable through National Institute of Standards and
Technology (NIST) to the International System of Units (SI). The basis of compliance stated is a comparison of the
measurement parameters to the specified or required calibration/testing process. The expanded uncertainties use a coverage
factor of k=2 to approximate the 95% confidence level of the measurement, unless otherwise noted. This calibration certificate
applies only to the item described and shall not be reproduced other than in full, without written approval from Red Ball
Technical Gas Services. If not included, the uncertainty of calibrations are available upon request and were taken into account
when determining pass or fail.
Jasmine Godfrey
Analytical Chemist
Assay Laboratory: Red Ball TGS
Version 02-J, Revised on 2018-09-17
Model
410i
MKS 2031DJG2EKVS13T
83 of 135
Balance
Red Ball Technical Gas Service
555 Craig Kennedy Way
Shreveport, LA 71107
800-551-8150
Accreditation #62754 PGVP Vendor ID # G12023
EPA PROTOCOL GAS CERTIFICATE OF ANALYSIS
Cylinder Number:RR04251 Certification Date:09/21/2023
Product ID Number:125371 Expiration Date:09/19/2031
Cylinder Pressure:1900 PSIG MFG Facility: - Shreveport - LA
COA #RR04251.20230831-0 Lot Number:RR04251.20230831
Customer PO. NO.:Tracking Number:107549718
Customer:Previous Certification Dates:
This calibration standard has been certified per the May 2012 EPA Traceability Protocol, Document EPA-600/R-12/531,
using procedure G1.
Do Not Use This Cylinder Below 100 psig (0.7 Megapascal).
Certified Concentration(s)
Component Concentration Uncertainty Analytical Principle Assayed On
Carbon Dioxide 11.1 %±0.11 %FTIR 09/21/2023
Oxygen 10.99 %±0.03 %MPA 09/18/2023
Nitrogen
Analytical Measurement Data Available Online.
Reference Standard(s)
Serial Number Lot Expiration Type Balance Component Concentration Uncertainty(%)NIST Reference
CC737012 CC737012.20230228 07/09/2031 GMIS N2 O2 20 %0.112 SRM 2659a
EB0022021 EB0022021.20180323 07/15/2026 GMIS N2 CO2 14.9 %0.777 101001
Analytical Instrumentation SMART-CERT
Component Principle Make MPC Date
O2 MPA Thermo 09/18/2023
CO2 FTIR MKS 09/21/2023
Serial
1162980025
017146467
This is to certify the gases referenced have been calibrated/tested, and verified to meet the defined specifications. This
calibration/test was performed using Gases or Scales that are traceable through National Institute of Standards and
Technology (NIST) to the International System of Units (SI). The basis of compliance stated is a comparison of the
measurement parameters to the specified or required calibration/testing process. The expanded uncertainties use a coverage
factor of k=2 to approximate the 95% confidence level of the measurement, unless otherwise noted. This calibration certificate
applies only to the item described and shall not be reproduced other than in full, without written approval from Red Ball
Technical Gas Services. If not included, the uncertainty of calibrations are available upon request and were taken into account
when determining pass or fail.
Jasmine Godfrey
Analytical Chemist
Assay Laboratory: Red Ball TGS
Version 02-J, Revised on 2018-09-17
Model
410i
MKS 2031DJG2EKVS13T
84 of 135
CERTIFICATE OF ANALYSIS
Grade of Product: EPA PROTOCOL STANDARD
Part Number: E03NI99E15A01D0 Reference Number: 153-402560601-1
Cylinder Number: EB0097304 Cylinder Volume: 144.0 CF
Laboratory: 124 - Tooele (SAP) - UT Cylinder Pressure: 2015 PSIG
PGVP Number: B72022 Valve Outlet: 660
Gas Code:CO,NO,NOX,BALN Certification Date: Oct 20, 2022
Expiration Date:Oct 20, 2030
Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA
600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical
uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a
mole/mole basis unless otherwise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval of the laboratory. Do
Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals.
ANALYTICAL RESULTS
Component Requested Actual Protocol Total Relative Assay
Concentration Concentration Method Uncertainty Dates
NOX 50.00 PPM 49.91 PPM G1 +/- 1.4% NIST Traceable 10/10/2022, 10/20/2022
CARBON MONOXIDE 50.00 PPM 50.39 PPM G1 +/- 0.8% NIST Traceable 10/10/2022
NITRIC OXIDE 50.00 PPM 49.85 PPM G1 +/- 1.4% NIST Traceable 10/10/2022, 10/20/2022
NITROGEN Balance
CALIBRATION STANDARDS
Type Lot ID Cylinder No Concentration Uncertainty Expiration Date
NTRM 12011221 KAL004127 49.24 PPM CARBON MONOXIDE/NITROGEN 0.6%Aug 31, 2024
PRM 12386 D685025 9.91 PPM NITROGEN DIOXIDE/AIR 2.0%Feb 20, 2020
NTRM 210607-24 CC708080 48.41 PPM NITRIC OXIDE/NITROGEN 1.2%Sep 21, 2025
PRM 12395 D887660 9.91 PPM NITROGEN DIOXIDE/AIR 2.0%Feb 02, 2022
NTRM 21060713 CC708049 48.41 PPM NITRIC OXIDE/NITROGEN 1.2%Sep 24, 2025
GMIS 401648675102 CC500959 5.074 PPM NITROGEN DIOXIDE/NITROGEN 2.1%Feb 01, 2023
GMIS 1534002020104 EB0130055 4.81 PPM NITROGEN DIOXIDE/NITROGEN 2.0%Apr 30, 2024
The SRM, NTRM, PRM, or RGM noted above is only in reference to the GMIS used in the assay and not part of the analysis.
ANALYTICAL EQUIPMENT
Instrument/Make/Model Analytical Principle Last Multipoint Calibration
Nicolet iS50 AUP2110269 CO LCO FTIR Oct 05, 2022
Nicolet iS50 AUP2110269 NO LNO FTIR Oct 13, 2022
Nicolet iS50 AUP2110269 NO2 impurity FTIR NO2 impurity Oct 12, 2022
Triad Data Available Upon Request
Airgas Specialty Gases
Airgas USA LLC
525 North Industrial Loop Road
Tooele, UT 84074
Airgas.com
Signature on file
Approved for Release Page 1 of 1
85 of 135
Balance
Red Ball Technical Gas Service
555 Craig Kennedy Way
Shreveport, LA 71107
800-551-8150
Accreditation #62754 PGVP Vendor ID # G12023
EPA PROTOCOL GAS CERTIFICATE OF ANALYSIS
Cylinder Number:EB0011606 Certification Date:09/18/2023
Product ID Number:124235 Expiration Date:09/16/2031
Cylinder Pressure:1900 PSIG MFG Facility: - Shreveport - LA
COA #EB0011606.20230906-0 Lot Number:EB0011606.20230906
Customer PO. NO.:Tracking Number:025274839
Customer:Previous Certification Dates:
This calibration standard has been certified per the May 2012 EPA Traceability Protocol, Document EPA-600/R-12/531,
using procedure G1.
Do Not Use This Cylinder Below 100 psig (0.7 Megapascal).
Certified Concentration(s)
Component Concentration Uncertainty Analytical Principle Assayed On
Nitric Oxide 501 PPM ±3 PPM Chemiluminescence 09/11/2023, 09/18/2023
Total Oxides of Nitrogen 503 PPM
Nitrogen
Analytical Measurement Data Available Online.
Reference Standard(s)
Serial Number Lot Expiration Type Balance Component Concentration Uncertainty(%)NIST Reference
FF55464 41-M-50 04/13/2025 SRM N2 NO 996.7 PPM 0.501 SRM 1687b
EB0059947 EB0059947.20230117 04/18/2031 GMIS N2 NO 280 PPM 0.658 SRM 1687b
SX32691 SX32691.20230117 08/28/2031 GMIS N2 NO 279.8 PPM 0.557 SRM 1687b
Analytical Instrumentation SMART-CERT
Component Principle Make MPC Date
NO Chemiluminescence Thermo 08/29/2023
Serial
1152610017
This is to certify the gases referenced have been calibrated/tested, and verified to meet the defined specifications. This
calibration/test was performed using Gases or Scales that are traceable through National Institute of Standards and
Technology (NIST) to the International System of Units (SI). The basis of compliance stated is a comparison of the
measurement parameters to the specified or required calibration/testing process. The expanded uncertainties use a coverage
factor of k=2 to approximate the 95% confidence level of the measurement, unless otherwise noted. This calibration certificate
applies only to the item described and shall not be reproduced other than in full, without written approval from Red Ball
Technical Gas Services. If not included, the uncertainty of calibrations are available upon request and were taken into account
when determining pass or fail.
Aaron Varelas
Analytical Chemist
Assay Laboratory: Red Ball TGS
Version 02-J, Revised on 2018-09-17
Model
42i-HL
86 of 135
CERTIFICATE OF ANALYSIS
Grade of Product: EPA PROTOCOL STANDARD
Part Number: E02NI99E15A0350 Reference Number: 153-402560600-1
Cylinder Number: SG9170578BAL Cylinder Volume: 144.0 CF
Laboratory: 124 - Tooele (SAP) - UT Cylinder Pressure: 2015 PSIG
PGVP Number: B72022 Valve Outlet: 660
Gas Code:SO2,BALN Certification Date: Oct 18, 2022
Expiration Date:Oct 18, 2030
Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA
600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical
uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a
mole/mole basis unless otherwise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval of the laboratory. Do
Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals.
ANALYTICAL RESULTS
Component Requested Actual Protocol Total Relative Assay
Concentration Concentration Method Uncertainty Dates
SULFUR DIOXIDE 50.00 PPM 50.39 PPM G1 +/- 0.9% NIST Traceable 10/11/2022, 10/18/2022
NITROGEN Balance
CALIBRATION STANDARDS
Type Lot ID Cylinder No Concentration Uncertainty Expiration Date
NTRM 16010207 KAL003179 97.69 PPM SULFUR DIOXIDE/NITROGEN 0.8%Nov 01, 2027
ANALYTICAL EQUIPMENT
Instrument/Make/Model Analytical Principle Last Multipoint Calibration
Nicolet iS50 AUP2110269 SO2 LSO2 FTIR Oct 12, 2022
Triad Data Available Upon Request
Airgas Specialty Gases
Airgas USA LLC
525 North Industrial Loop Road
Tooele, UT 84074
Airgas.com
Signature on file
Approved for Release Page 1 of 1
87 of 135
CERTIFICATE OF ANALYSIS
Grade of Product: EPA PROTOCOL STANDARD
Part Number: E02NI99E15A0930 Reference Number: 153-124604653-1
Cylinder Number: EB0091184 Cylinder Volume: 144.4 CF
Laboratory: 124 - Tooele (SAP) - UT Cylinder Pressure: 2015 PSIG
PGVP Number: B72017 Valve Outlet: 350
Gas Code:PPN,BALN Certification Date: Feb 20, 2017
Expiration Date:Feb 20, 2025
Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA
600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical
uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a
mole/mole basis unless otherwise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval of the laboratory. Do
Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals.
ANALYTICAL RESULTS
Component Requested Actual Protocol Total Relative Assay
Concentration Concentration Method Uncertainty Dates
PROPANE 30.00 PPM 29.72 PPM G1 +/- 0.6% NIST Traceable 02/20/2017
NITROGEN Balance
CALIBRATION STANDARDS
Type Lot ID Cylinder No Concentration Uncertainty Expiration Date
NTRM/C3H8 08061008 CC262362 49.62 PPM PROPANE/AIR +/- 0.3%May 14, 2018
ANALYTICAL EQUIPMENT
Instrument/Make/Model Analytical Principle Last Multipoint Calibration
Nicolet 6700 AMP0900119 C3H8 LC3H8 FTIR Feb 02, 2017
Triad Data Available Upon Request
Airgas Specialty Gases
Airgas USA LLC
525 North Industrial Loop Road
Tooele, UT 84074
Airgas.com
Signature on file
Approved for Release Page 1 of 1
88 of 135
Location:
Project No.:
Analyzer Make Thermo Pre-Test Date 5/8/24 Time 7:20
Analyzer Model 42C-HL Pre-Test Concentration, ppm 46.4
Serial Number 42CHL-59778-324 Pre-Test Efficiency, %93
Cylinder ID Number CC770726 Post-Test Date 5/8/24 Time 17:53
Cylinder Exp. Date 4/23/27 Post-Test Concentration, ppm 45.19
Cylinder Concentration, ppm 49.9 Post-Test Efficiency, %91
*Required Efficiency is ≥ 90 %.
Clean Harbors Aragonite LLC - Aragonite, UT
AST-2024-1517
NO2 Converter Check - Outlet
NOx Converter Efficiency Check
89 of 135
Balance
Red Ball Technical Gas Service
555 Craig Kennedy Way
Shreveport, LA 71107
800-551-8150
Accreditation #62754 PGVP Vendor ID # G12024
EPA PROTOCOL GAS CERTIFICATE OF ANALYSIS
Cylinder Number:CC770726 Certification Date:04/23/2024
Product ID Number:124731 Expiration Date:04/23/2027
Cylinder Pressure:1800 PSIG MFG Facility: - Shreveport - LA
COA #CC770726.20240212-0 Lot Number:CC770726.20240212
Customer PO. NO.:Tracking Number:108893184
Customer:Previous Certification Dates:
This calibration standard has been certified per the May 2012 EPA Traceability Protocol, Document EPA-600/R-12/531,
using procedure G2.
Do Not Use This Cylinder Below 100 psig (0.7 Megapascal).
Certified Concentration(s)
Component Concentration Uncertainty Analytical Principle Assayed On
Nitrogen Dioxide 49.9 PPM ±0.5 PPM FTIR 02/16/2024, 04/16/2024, 04/23/2024
Air
Analytical Measurement Data Available Online.
Reference Standard(s)
Serial Number Lot Expiration Type Balance Component Concentration Uncertainty(%)NIST Reference
EB0055436 EB0055436.20201021 07/14/2025 GMIS AIR NO2 29.22 PPM 1.026 C2190301.02
EB0080844 EB0080844.20201020 05/04/2026 GMIS AIR NO2 94.5 PPM 1.029 C2190301.02
EB0097551 EB0097551.20201021 05/05/2025 GMIS AIR NO2 63.3 PPM 1.074 C2190301.02
Analytical Instrumentation SMART-CERT
Component Principle Make MPC Date
NO2 FTIR MKS 01/19/2024
NO2 FTIR MKS 04/15/2024
Serial
017146467
112428254
This is to certify the gases referenced have been calibrated/tested, and verified to meet the defined specifications. This
calibration/test was performed using Gases or Scales that are traceable through National Institute of Standards and
Technology (NIST) to the International System of Units (SI). The basis of compliance stated is a comparison of the
measurement parameters to the specified or required calibration/testing process. The expanded uncertainties use a coverage
factor of k=2 to approximate the 95% confidence level of the measurement, unless otherwise noted. This calibration certificate
applies only to the item described and shall not be reproduced other than in full, without written approval from Red Ball
Technical Gas Services. If not included, the uncertainty of calibrations are available upon request and were taken into account
when determining pass or fail.
Aaron Varelas
Analytical Chemist
Assay Laboratory: Red Ball TGS
Version 02-J, Revised on 2018-09-17
Model
MKS 2031DJG2EKVS13T
MKS 2031GPPP1A5ZK1XX
90 of 135
Location:
Source:
Project No.:
Date
EPA
O2
Servomex
1400
1420-4
25.0
Cylinder Number ID
Zero NA
Mid EB0089907
High CC458788
Cylinder Certified Values
Zero 0.0
Mid 10.99
High 23.97
Instrument Response (% or ppm)
Zero 0.2
Mid 10.9
High 24.0
Calibration Gas Selection (% of Span)
Mid 44.0
High 95.9
Calibration Error Performance (% of Span)
Zero 0.7
Mid -0.3
High 0.0
Linearity (% of Range)
-0.6
(%)lpm (%)(%)(%)(%)(%)(%)(%)( ± 2 %)
10L/5L 80.0 5.0 19.2 19.2 19.2 19.2 19.2 19.22 0.02 0.1%
10L/5L 50.0 5.0 12.0 12.0 12.0 12.0 12.0 11.99 -0.01 -0.1%
10L/1L 20.0 4.0 4.8 4.8 4.8 4.8 4.8 4.81 0.01 0.2%
10L/1L 10.0 4.0 2.4 2.4 2.4 2.4 2.4 2.43 0.03 1.1%
(%)( ± 2 %)( ± 2 %)( ± 2 %)
19.22 0.1%0.0%-0.1%
11.99 0.1%-0.1%0.0%
4.81 0.2%0.0%-0.2%
2.43 0.5%0.5%-1.1%
Mid-Level Supply Gas Calibration Direct to Analyzer
Calibration Injection 1 Injection 2 Injection 3 Average
Gas Analyzer Analyzer Analyzer Analyzer
Concentration Concentration Concentration Concentration Concentration
(%)(%)(%)(%)(%)(%)( ± 2 %)
10.99 11.0 11.0 11.0 11.01 0.02 0.2%
Analyzer Make: Servomex
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
5/9/24
Parameter
Make
Model
S/N
Span
Method Criteria
Analyzer Model: 1400
Analyzer SN: 1420-4
Environics ID: 8026
Component/Balance Gas: O2/N2
Cylinder Gas ID (Dilution): CC458788
Cylinder Gas Concentration (Dilution), %: 23.97
*Not all AST Environics Units have 2-10L Mass Flow Controllers. For these units the 90% @ 7lpm and 80% @ 7lpm injections will not be conducted.
Cylinder Gas ID (Mid-Level): EB0089907
Cylinder Gas Concentration (Mid-Level), %: 10.99
Target Mass Flow
Contollers
Target
Dilution
Target Flow
Rate
Target
Concentration
Actual
Concentration
Injection 1
Analyzer
Concentration
Injection 2
Analyzer
Concentration
Injection 3
Analyzer
Concentration
Average
Analyzer
Concentration Difference Average Error
Average
Analyzer
Concentration
Injection 1
Error
Injection 2
Error
Injection 3
Error
Difference
Average
Error
EPA Method 205
Field Calibration of Dilution System
91 of 135
Dilution System Make:
Dilution System Model:
Dilution System S/N:
Calibration Equipment Make:
Calibration Equipment Model:
Calibration Equipment S/N:
Flow Cell S/N:
Flow Cell S/N:
Calibration Gas:
Barometric Pressure, mmHg:
Ambient Temperature, °F:
Mass Flow Controller ID
Size, ccm:
Make:
Model:
S/N:
Set Flow True Flow Difference Set Flow True Flow Difference Set Flow True Flow Difference
cc/min cc/min cc/min cc/min cc/min cc/min
5%500 502 0.4%500 502 0.4%50 49 2.4%
10%1,000 1,017 1.7%1,000 1,012 1.2%100 99 1.5%
20%2,000 2,057 2.9%2,000 2,040 2.0%200 199 0.7%
30%3,000 3,083 2.8%3,000 3,059 2.0%300 299 0.2%
40%4,000 4,106 2.7%4,000 4,078 2.0%400 400 0.1%
50%5,000 5,122 2.4%5,000 5,095 1.9%500 502 0.5%
60%6,000 6,148 2.5%6,000 6,114 1.9%600 604 0.6%
70%7,000 7,164 2.3%7,000 7,134 1.9%700 706 0.9%
80%8,000 8,182 2.3%8,000 8,152 1.9%800 810 1.3%
90%9,000 9,198 2.2%9,000 9,173 1.9%900 916 1.8%
100%10,000 10,221 2.2%10,000 10,195 2.0%1,000 1,024 2.4%
Date
4040 4040
67
Environics
8026
#1
10,000
Environics
4040
Alicat Scientific
197206
197206
197208
Nitrogen
25.5
Calibration Performed By Ryan Lyons
4/27/23
455242011
Mass Flow Controller Calibration
Note: The mass flow controller's calibration values are used by the dilution system's operating software to improve accuracy. These calibrations are not
necessarily indicative of the systems overall performance. Performance is verified by conducting a Method 205 prior to each field use.
M-10SLPD/5MM-D/5M, M-1SLPM-D/5M
4040
10,000
# 2 # 3
Environics
455242012
1,000
Environics
455238006
92 of 135
93 of 135
Balance
Red Ball Technical Gas Service
555 Craig Kennedy Way
Shreveport, LA 71107
800-551-8150
Accreditation #62754 PGVP Vendor ID # G12023
EPA PROTOCOL GAS CERTIFICATE OF ANALYSIS
Cylinder Number:EB0089907 Certification Date:01/11/2023
Product ID Number:125371 Expiration Date:01/09/2031
Cylinder Pressure:1900 PSIG MFG Facility: - Shreveport - LA
COA #EB0089907.20230104-0 Lot Number:EB0089907.20230104
Customer PO. NO.:Tracking Number:095289418
Customer:Previous Certification Dates:
This calibration standard has been certified per the May 2012 EPA Traceability Protocol, Document EPA-600/R-12/531,
using procedure G1.
Do Not Use This Cylinder Below 100 psig (0.7 Megapascal).
Certified Concentration(s)
Component Concentration Uncertainty Analytical Principle Assayed On
Carbon Dioxide 10.90 %±0.06 %NDIR 01/11/2023
Oxygen 10.99 %±0.03 %MPA 01/09/2023
Nitrogen
Analytical Measurement Data Available Online.
Reference Standard(s)
Serial Number Lot Expiration Type Balance Component Concentration Uncertainty(%)NIST Reference
CC722672 CC722672.20210412 05/18/2030 GMIS N2 CO2 11.94 %0.245 C2190301.03
CC738486 CC738486.20211012 05/01/2030 GMIS N2 O2 19.98 %0.128 SRM 2659a
EB0089841 EB0089841.20191017 01/07/2028 GMIS N2 O2 12.03 %0.139 SRM 2659a
EB0097897 EB0097897.20210412 05/18/2030 GMIS N2 CO2 19.46 %0.15 C1847810.03
Analytical Instrumentation SMART-CERT
Component Principle Make MPC Date
O2 MPA Thermo 12/23/2022
CO2 NDIR Thermo 12/14/2022
Serial
1162980025
1162980025
This is to certify the gases referenced have been calibrated/tested, and verified to meet the defined specifications. This
calibration/test was performed using Gases or Scales that are traceable through National Institute of Standards and
Technology (NIST) to the International System of Units (SI). The basis of compliance stated is a comparison of the
measurement parameters to the specified or required calibration/testing process. The expanded uncertainties use a coverage
factor of k=2 to approximate the 95% confidence level of the measurement, unless otherwise noted. This calibration certificate
applies only to the item described and shall not be reproduced other than in full, without written approval from Red Ball
Technical Gas Services. If not included, the uncertainty of calibrations are available upon request and were taken into account
when determining pass or fail.
Timothy Davis
Analytical Chemist
Assay Laboratory: Red Ball TGS
Version 02-J, Revised on 2018-09-17
Model
410i
410i
94 of 135
Location
Source
Project No.
Parameter(s):
5/8/24 P-867 no no no
Date Probe or
Thermocouple ID
Reference
Temp. (°F)
Indicated
Temp. (°F)Difference Criteria
5/8/24 P-867 141.0 141.0 0.0%
Date 05/08/24
Balance ID:SCALE 22
Test Weight ID:SLC-1 KG-1
Certifieid Weight (g):1000.0
Measured Weight (g):999.7
Weight Difference (g):0.3 --------
5/8/24 Weather Station NA NA NA
5/8/24 M5-27
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
VFR
Salt Lake City UT
Pass
Date Pitot ID Evidence of
damage?
Evidence of
mis-alignment?
Calibration or
Repair required?
Date Meter Box ID
± 1.5 %
Field Balance Check
Date Barometric
Pressure
Evidence of
damage?
Reading
Verified
Calibration or
Repair required?Weather Station Location
Positive Pressure Leak Check
QA Data
95 of 135
Document ID 620.004
Revision 23.0
Effective Date 1/25/23
Issuing Department Page 1 of 1
Console ID:
Meter S/N:20035543
Critical Orifice S/N:
(PbI)
(PbF)
(Pb)
(Y)1330-31 1330-31 1330-25 1330-25 1330-19 1330-19
(K')0.8429 0.8429 0.6728 0.673 0.5186 0.519
(VP)13.0 13.0 15.0 15.0 17.0 17.0
Initial DGM Volume, ft3 (VmI)501.924 512.781 528.098 536.765 548.287 555.093
Final DGM Volume, ft3 (VmF)512.781 523.688 536.765 545.420 555.093 561.889
Total DGM Volume, ft3 (Vm)10.857 10.907 8.667 8.655 6.806 6.796
Ambient Temperature, °F (Ta)64 64 63 63 63 63
Initial DGM Temperature, °F (TmI)63 63 64 65 64 64
Final DGM Temperature, °F (TmF)63 64 65 64 64 65
Average DGM Temperature, °F ( Tm)63 64 65 65 64 65
Elapsed Time (Θ)10.00 10.00 10.00 10.00 10.00 10.00
Meter Orifice Pressure, in. WC (ΔH)3.20 3.20 2.10 2.10 1.30 1.30
Standard Meter volume, ft3 (Vmstd)9.2720 9.3058 7.3570 7.3468 5.7693 5.7553
Standard Critical Orifice Volume, ft3 (Vcr)9.2341 9.2341 7.3777 7.3777 5.6868 5.6868
Meter Correction Factor (Y)0.996 0.992 1.003 1.004 0.986 0.988
Tolerance --0.001 0.003 0.008 0.009 0.009 0.007
Orifice Calibration Value (ΔH @)1.803 1.801 1.842 1.842 1.917 1.915
Tolerance --0.051 0.052 0.011 0.011 0.063 0.062
Orifice Cal Check --
Meter Correction Factor (Y)
Orifice Calibration Value (ΔH @)
Accuracy Difference
oF oR oF oR %oF
0 460 2 462 -0.4 2
68 528 69 529 -0.2 1
100 560 102 562 -0.4 2
223 683 225 685 -0.3 2
248 708 250 710 -0.3 2
273 733 274 734 -0.1 1
300 760 301 761 -0.1 1
400 860 401 861 -0.1 1
500 960 501 961 -0.1 1
600 1,060 600 1,060 0.0 0
700 1,160 700 1,160 0.0 0
800 1,260 800 1,260 0.0 0
900 1,360 900 1,360 0.0 0
1,000 1,460 999 1,459 0.1 1
1,100 1,560 1,100 1,560 0.0 0
1,200 1,660 1,199 1,659 0.1 1
Calibration Date:
0.94 1.68 1.66
DGM Calibration-Orifices
Tech Services
25.07
25.07
25.07
K' Factor, ft3·R1/2 / in. WC·min
CL23A
Vacuum Pressure, in. Hg
Initial Barometric Pressure, in. Hg
Final Barometric Pressure, in. Hg
Average Barometric Pressure, in. Hg
Critifcal Orifice ID
Calibration Detail
M5-27
1330
Positive Pressure Leak Check
Equipment Detail - Dry Gas Meter
0.995
1.853
Yes
Personnel
Reference Calibrator Make:
Reference Calibrator Model:
Reference Calibrator S/N:
Calibration Detail
Equipment Detail - Thermocouple Sensor
Reference Temp.Display Temp.
OMEGA
T-197207
Stacey CunninghamReviewed By:
RYAN LYONSCalibration By:
2/2/2024
96 of 135
Location:
Source:
Project No.:
Date:
Time O2 CO2 CO NOx SO2
(%) (%) (ppm) (ppm) (ppm)
A-1 11:17 9.73 8.69 1.04 238.96 0.49
2 11:19 8.60 9.62 1.03 131.57 0.06
3 11:21 8.06 9.90 1.02 118.79 0.25
B-1 11:23 9.04 9.22 0.98 118.92 0.22
2 11:25 9.84 8.55 0.97 131.72 0.17
3 11:27 10.85 7.73 0.98 126.35 0.34
9.4 9.0 1.0 144.4 0.3
12 Point 12 Point Single Point 12 Point Single Point
Average
Criteria Met
Traverse Point
Clean Harbors Aragonite LLC - Aragonite, UT
Incinerator System (INC)
AST-2024-1517
5/8/2024
97 of 135

Appendix D

98 of 135
04
9
0
0
-
C
1
-
4
0
2
1

0
4
9
0
0
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2
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A
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2
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A
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1
9
8
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2
1
9
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B

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1
9
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A
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2
2
0
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2
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0
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2
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A
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#1

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(
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)
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