HomeMy WebLinkAboutDSHW-2024-007924ffi DEPARTMENT OF THE AIN FOHCE
HEADQUARTERS oGDEN AIB LOGISTICS CENTER (AFLC)
HILL AIR FORCE BASE, UTAH 84056-5990
Fqffifl}h;::i{Vry$fr,, €el
l,r0V 1 ? l99l
Bitltiur; *i $*li,j ',1 ltaa,;niuus hfust*
IJtsh ihper rr,*lit uf f,*rt;r"fts::trttl! [!us]lty
In accordance with the Utah ltest and Training Range, f,ithium
Battery Facility, hazardous waste permit number IrItO57oo9000L,Hill Air Force Base is subnitting for a permit renewal.
Suburitting the revised permit at this time will allow the Stateof Utah adequate tine to review and incorporate any necessary
changes before our current permit expires on
1-0 May 92.
Approval and reissuance of a new permit will be based on the factthat secondary containment and leak deteetion will be installedat the Lithiun Battery Facility. Until these are installed, thisfacility w111 not be authorized to operate or deactivate anylithium batteries. It is our intent to have this work started or
acconplished before 10 tlay 92.
If you have any question regardinqr this application for renewal,our point of contact is Bruce Oshita, Environmental Managenent,
(8011 777-69L8 or 69L9.
Jo^r,rru R. tJo-On^ r..o^^--
Bureau of Solid and Hazardous Waste
ATTN: Mr DOWNS
PO Box 1-6690
2BB North 1460 WestSaIt Lake City UT 84LL6-0690
Dear Mr Dourns
JAMES
Dir ec tor
R. VAN ORMAN .,TM
ol Environmental Management
J
1 Atch
Permit Renewal
".Ff,
N ffi srArE ". H:':#'-PR.,AL
A continued in accordance with R45G3-5(d).
ffi.
X signature: ,( - *Date: E/"/r,
X utalr r.r,::ffilff;N \W "*BJ'il,fl,i9,ilt:,rH,"
"B
-{<-v EPA Ideutification Numbei'IJr0570090001
tg
),N
$N hrrsrant to the Utah Solid and Hazardous Waste Act, (the Act), 26-14-1, et. seq.,
S Utah Code Annotated 1953, as arnended and the Utah Administrative Code (UAC)
Y G45G1 tbrough R45G13 and R450-50) as adopted by the Utah Solid and Hazardous
S Wasrc Commiftee, (the Comsrittee), a ptan apiroval (herein after talled "permit") is(fr issued to Hill Air Force Base - Utatr Test and Training Range(hereafter called the
N 'Permittee'), to operate a hazardous waste Research, Development, and
S) Demorutration (RD&D)treatment facility in Box Elder County, Utah. The U.S.
Ith Euvironmeutal Protection Agency (U.S. EPA) has authorized the Executive Sectetary
[Ill to issue such a permit under Section 3006(b) of the Resource Conservation and
U
Recovery Act (RCRA).
).t The Permittee mustl comply with all the terms and couditions of this permit. The
N permit corsists of the conditions contained herein (including the portions of the
O application attached and incorporated by reference), and the applicable portions of
,Y R450-1 through R45G13, R45G50, and R45&101 contained in the permit. Applicable,6 rules.are those which are in effect on the date of issuance of this permit.
ftt This permit is based on the premise that the inforcration submitted in the applicationr* dated September 23, 1986 as modified by a subsequent amendments dated November
tr 25, 1986 and June 5, 1987 (hereafter referred to as the application), is accurate andgil that the facility will be operated as specified in the referenced portions of the
Irll application, except as modified by the conditioru herein. Portioru of the application
V are attached and incorporated herein by reference, wherever noted, as part of this
2l permit. Any inaccuracies or misrepresentations found in the application may be
dfi grounds for the termination or modification of this permit (see R45S3-9.). TheyY. Permittee must inform the Executive Secretary of any deviation from, or changes in
lF the information in the application which would atreci the Permittee's ability td comply
g, with the applicable regulations or permit conditions.
Yl; This permit is effective as of March 30, 1990, and shall remain in effect until May 10,
#, 1992, unless revoked a.od reissued (R45G3-9.1(aXb)(c)) or terminated (R45G3-9.2.), orta continued in accordance with R45G3-5(d).
W^
6,
Y^
6,
N
#
$
x
$
!((
Dennis R. Dourns
Exentive Secretary
Utah Solid and Hazardous Waste Committee
a
A
B.
C.
D.
E.
F.
G.
H.
I.
J.
K
L.
M.
A
B.
C.
D.
E.
F.
G.
Fr.
I.
J.
K
TABLE OF CONTENTS
I,.sfl l.? tgg,
EIAZARDOUS WASTE PIA}I
MODULE I - STAI{DARD CONDITIONS
EFFECT OF PERMIT
ENFORCEABILITY
NO WAT\TER OF AUTI{ORITY
PERMIT ACTIONS
SEVERABILITY
DUTIES AND REOUIREMENTS
1. Duty to Comply; 2. Duty to Reapply; 3. Permit Expiration; 4. Need to
Halt or Reduce Activity not a Defense; 5. Duty to Mitigate; 6. Proper
Operation and Maintenance; 7. Dutv to Provide Information; 8. Inspection
and Entry; 9. Reponing Planned Changes; 10. Certification of Construction
or Modification; 1.1. Anticipated Noncompliance; 12. Transfer of Permits; 13.
Monitoring and Records; 14. Twentv-four Hour Reporting; 15. Compiiance
Schedules; 16. Biennial Report; 17. Other Noncompliance; 18. Other
Inforrration
SIGNATORY REOUIREMENT
CONFIDENTIAL INFORMATION
DOCUMEI.ITS TO BE MNNTAINED AT FACILITY S
PROTECTION OF HUMAN HEALTH AND THE ENVIRONMENT
DEFINTNONS
REOI.IIRED SUBMISSIONS UNDER THIS PERMIT
REOUIRED NOTIFICATIONS TTNDER THIS PERMIT
MODULE II - GENERAL CONDITIONS
APPLICABILITY
DESIGN AND OPERATION OF FACILITY
GENERAL WASTE ANALYSIS
SECURITY
GENERAL INSPECTiON REOUIREMENTS
PERSONNEL TRAINING
GENERAL REOUIREMENTS FOR IGNITABLE. REACTME. OR
INCOMPATIBLE WASTE
PREPAREDNESS AND PREVENTTON
CONTINGENCY PLql\
RECORDKEEPING AND REPORTiNG
cLosuRE/PosT-cLosuRE
ATTACHMENT II-1 - WASTE ANALYSIS PI-A}I
ATTACHMENT TI-2 - SECURITY PROCEDURES
Table of Contents - page 1
A
B.
C.
D.
EL.
F.
G.
H.
ATTACHMENT II.3 . INSPECTIONS
ATTACHMENT II4 - PERSONNEL TRAINING
ATTACHMENT II.5 . PREPAREDNESS A}ID PREVE}ITION
ATTACHMENT II.6 - CONTINGENCY PI-AI.I
ATTACHMENT TI.7 . CLOSURE
MODT'LE III - STORAGE IN CONTAINERS
NOT APPLICABLE
MODULE TV . STOR.A,GE AI{D TREATMENT IN TAI{IG
APPLICABILITY
WASTE IDENTIFICATION
TAhIK SYSTEM DESIGN A].ID CONSTRUCTION
GENERAL OPERATING COI.I TilONS
RESPONSE TO LEAKS OR SPILH
INSPECTION SC}TEDULES A]\ID PROCEDURES J.
RECORDKEEPING AND REPORTING
TA}IK CLOSURE
ATTACHMENT IV-l(A) - RESEARCH PI-Alr, RESEARCH
DESCRIPTION
ATTACHMENT IV-l(B) - RESE.ARCH PL-AI.I, DEACTIVATION
PROCESS DESCRIMON
Table of Contens - page 2
Module I -Standard Conditions
I.A.
I.B.
I.C.
r.D.
I.D.1.
uoDt LE r - sEtlrDeRD corIDIEroNs
EFFECT OF PERMTT
The Peraittee is allowed to research hazardous
waste treatment of lithiun batteries in tanks in
accordance with the condi.tions of this peruit.
Any treatuent or storage of hazardous waste not
auttrorized in this, or any other hazardous trastepermit is prohibited. Conpliance with thispemit constitutes coupliance, for purposes of
enforceuent, with the Utah Solid and Hazardous
Waste Act. Issuance of this pe:mit does not
convey property rights of any sort or any
exclusive privilegei nor does it authorize anyinjury to persons or property, any invasion ofother private rights, or any infringement ofState or loca1 1aw or regulations. Conpliancewith the terus of this pernit does notconstitute a defense to any order issued or anyaction brought under Section 3008 (a) , 3013 , or
7003 of RCRA; Sections 106 (a) , 104, oE 107 ofthe Conprehensive Environmental Response,
Compensation, and Liability Act of 1980 (42
U. S. C. 9501 g@-:-r commonly known as CERCLA)';or any other law providing for proteetion ofpublic health or the environment.
ENFORCEABILITY
Any violation of this pernit shall be consideredeither a Class I or a Class II violation 'as
outlined in the enforcement penalty policy
adopted by the Committee. Class I violationsduly docurnented thrcugh the enforcement prccess
and upheld through any appellate acti.on mayresult in penalties of up to S10,000 per day per
violation.
NO WATVER OF AT.'THORTTY
Other Authoritv. The Department of Healthexpressly reserves any right of entry provided
by law and any authority to order or perform
emergency or other response activities as
authorized by Iaw.
PERMIT ACTTONS
This permit may be nodified, revoked and
reissued, oE terminated for cause as specifiedin R450-3.9. The filing of a reqluest for a
Hodulel-page1
r.D.2.
r.D.3
I.E.
I.F.
r.F.L.
permit nodification, revocation and reissuance,or temination or the notification of planned
changes or ariticipated noncoupliance on the partof the Peruittee does not stay the applicabilityor enforceability of any perrnit condition. AI1perait conditions vithin this permit will
supersede conflicting stateroents, requirementsor procedures found within the Attachuents of
each Module.
This pernit uay be nodified at the request ofthe Peruittee according to the procedures of
R4so-3-e.1(d).
The Executive Secretary Day modify thls pemit
when the standards or rules on which the permit
was based have been changed by statute, amended
standards or regulations, or by judicial
decision after the effective date of the permit.
SE1/ERABTLITY
The provisions of this per:nit are severable, andif any provision of this permit, or theapplication of any provision of this permit to
any circumstance is held invalid, theapplication of such provision to other
circumstances and the remainder of this perrnit
shal1 not be affected thereby. Invalidation of
any state or federal statutory or regulatoryprovision which forms the basis for anycondition of this per:nit does not affect thevalidity of any other state or federal statutoryor regulatory basis for said condj.tion.
DUTIES AND REOUIREI'IENTS
Dutv to Cornplv. The Perurittee shaIl cornply withall conditions of this permit, except to theextent and for the duration such nonconplianceis authorized by an energency permit. Anypermit noncompliance, other than noncomplianceauthorized by an energency pernit, constitutes aviolation of the Utah Administrative Code and is
grounds for enforcenent action, permit r
termination, revocatj.on and rei.ssuance,rnodification, oE denial of a perrnit renewalapplication.
Dutv to Reaoplv. If the Permittee wishes to
continue any activities allowed by this permitafter the expiration date of this pernit, the
I.F.2
l,lodule f -page 2
r.F.3.
I.r.4
I.F.5.
I.F.5.
r.F.7
Permittee shall subroit an application for a newperrit at least 180 days before this pemit
ex5)ires
Pe::ait E:<oiration. This peruit wiII expire on
May 10, L992. This pemit and all conditions
herein will reuain in effeet beyond the pomitrs
orpiration date if the Peruittee has subaitted atinely, couplete applicatlon (see R450-3-3.1 and
R450-3-3.2.) and through no fault of the
Permittee, the Cournittee and/or Executive
Secretary has not issued a new pernit as setforth in R450-3-5(d).
Need to HaIt or Reduce Activitv Not a Defense.It shalI not be a defense for the Permittee in
an enforcement action that it would have been
necessary to halt or reduce the pernittedactivity in order to maintain compliance withthe conditions of this permit.
Dutv to l.titicrate. In the event of noncompliancewith the pennit, the Permittee shalI take all
reasonable steps to ninimize releases to the
environmentr''and shall carry out such measures
as are necessary to prevent significant adverse
impacts on human health or the environment.
Proper Oneration and Maintenance. The PermitteeshalI at dlI tirnes properly operate and maintainall.facilities and systems of treatment andcontrol (and related apparatus) which areinstalled or used by the Perurittee to achieve
compliance with the conditions of this perrnit.
Proper operation and maintenance incLudeseffective performance, adequate fundj.ng,
adequate operator staffing and training, and
adequate laboratory and process controls,including appropriate quality assuranceprocedures. This provision requires the
operation of back-up or auxiliary equiprnent orsinilar systems, only when necessary to achieve
compliance with the conditions of the perm5.t.
Dutv to Provide fnformation. The Permitteeshall furnish to the Committee and/or the
Executive Secretary, within a reasonable time,
any relevant infor:uation which the Committee
and/or Executive Secretary may request to
deterrnlne whether cause exists for urodifying,
revoking and reissuing, oE terminating thispernit, or to deteraine cornpliance with this
Modulef-page3
I.F.g.
f.F.8.E[.
r.F.g.b.
f.F.8.c.
r.F.g.d,.
TtrA..4'J
permit. The Pernittee shall also furnish to the
Conmittee and/or the Executive Secretary uponrequest, copies of records required to be-kept
by this permit.
fnspection and Entrv. The Per:uittee shall allowthe Couuittee and/or the Executive Secretary, or
an authorized representative, upon thepresentation of credentials and other documents
as Eay be required by lan to:
Enter at reasonable times upon the Pernitteets
premises where a regrulated facility and/oractivity is located or conductedr oE where
records nust be kept under the conditions ofthis permit r'
Have access to and copy, at reasonable times,
any records that must be kept under theconditions of this permit;
fnspect at reasonable times any facilities,
equipment (including nonitoring and control
equipnent) , practices, or .operations regulatedor required under this p€Errt; and
Sample or monitor, at reasonable times, for the
purposes of assuring per:nit compliance or as
otherwise authorized by the Utah Solid and
Hazardous Waste Act, any substances or
parameters at any location
Reportincr Planned Chanoes. The Perrnittee shallgive written notice to the Executive Secretarysixty (60) days prior to any planned physicalalterations or additions to any hazardous waste
management unit or systen being perroitted orpreviously perrnitted. Physical alterations or
additions shalI include a1l hazardous and solid
waste activities and any non-waste underground
storage tanks. Construction and/or operation of
new/modified hazardous waste units shall not
begin unless the provi.sions of R450-3-9. aremet. Failure to ccmply with this permit
condition may cons-,-itute a Cl.ass I violationduly documented through any appellate action.
Certification of Construction or Modification.
The Permittee may not conmence storage,treat:nent, or disposal of hazardous waste in a
new hazardous waste management unit or an
r.F.10.
ModuleI-page4
f.F.10.E[.
I.F.10.a'.i-.
f.f.10.E.ii.
r.F.10.b.
I.F.10.c.
r.F.]. 1.
I.F,L2
r.F.l_3.
I.F.13.a,.
existing unit being modified at the permitted
facility until:
The Petmittee has submitted to the Executive
Secretary:
A letter signed by the Per:uittee and a gualified
Utah registered professional engineer statingthat the unit has been constructed in compliancewith this permit; and
As built engineering plans and specifications;
and
The Executive Secretary has reviewed and
inspected the newly constructed facility and hasnotified the Permittee in writing that the unit
was found in conpliance with the conditions ofthis permit; or
The Executive Secretary has either waived the
inspection, or has not within fifteen (15) days
of the date of his receipt of the above
submission, notified the Pernittee of an intentto inspect
Anticipated Noncomoliance. The Perrnittee shallgive acivance notice to the Executive Secretaryof any planned changes in the perruitted facilityor activity which raay result in noncompliancewith permit requirements. Advance notice shall
not excuse any noncompliance.
Transfer of Permits. This pernit nay betransferred to a nehr owner or opera-,or only ifit is modified or revoked and reissued pursuant
to R450-3-8. and R45O-3-9. Before transferring
ownership or operation of the facility during
its operating life, the Pernittee shall notifythe new owner or operator, in writing, of the
requirenents of this permit.
Monitorinq and Records
Samples and measurernents taken for the purpose
of nonitoring shall be representative of the
monitored activity. The method used to obtain
representative samples must be the appropriate
nethod from R450-50-IH or an equivalent rnethodthat is approved by the Executive Secretary.
Laboratory methods must be those specified in
Test Methods for Evaluatinq Solid Waste:
Module I (- page 5
I.F.13.b.
I.F.13.c.
I . F. 13 . d.
-I.F.13.d,.i_.
r.F.13.d.ii.
r.F.13.d.iii.
f.F.13.d.iv.
I.F.13.d.v.
f.F.13.d.vi.
I.F.14.
Phvsical/Chemica1 Hethods SW-846, Third Edition,or the uost current edition, Standard Hethodsfor thP Examination of Water and Wastewater,
Sixteenth Edition.
A request for substitution of an analytical
uethod which is equivalent to the nethodspecifically approved for use in this pamitshall be submitted to the Executive Secretary in
accordance with R450-3-9. The request shallprovide infomation demonstrating that the
proposed uethod requested to be substituted is
equivalent or superior in ternrs of sensitivity,
accuracy, and precision (i.e., reproducibility) .
The Permittee sha1l retain at the Utah Test and
Training Range facility records of all
ruonitoring inforrnation, including allcalibration and maintenance recordsj copies ofall reports and records reguired by this pernit,
and records of all data used to conplete theapplication for this permit for three (3) years
frou date of measurement. This period may be
extended by request of the Executive Secretaryat any tiure and is automatically extended during
the course of any unresolved enforcement action
regarding this facility.
Records of rnonitoring at a ninimum shall
include:
The dates, exact place, and tirnes of sampling or'
measurements r'
The individuals who performed the sanpling or
measurements;
The dates analyses hrere performed;
The individuaLs who performed the analyses;
The analytical techniques or methods used; and
The results of such analyses.
firentv-four Hour Reportino. The Permittee shall
report to the Executive Secretary any
noncompliance with the pennit which rnay endanger
human health or the environnent. Any such
information shaIl be reported orally as soon as
possible, but not later than twenty-four (241
hours from the time the Permittee becomes aware
Modulef-page6
of the circumstances. This report shall includethe following:
f .F.14.a. Inforaation concetning the release of any
hazardous waste which may endanger public
drinking water supplies.
I.f.14.b. fnforuation concerning the release or dischargeof any hazardous waster or of a fire or
eqrlosion at the facility, which could threaten
the environment or human health. Thedescription of the occurrence and lts cause
shall include:
f.F"14.b.i. NaEe, address, and telephone number of the owneror operator;
f.F.14.b.ii. Name, address, and telephone number of thefacility i
I.F.14.b.iii. Date, time and type of incident;
f.F.14.b.iv. Name and quantity of materials involved;
I.F.14.b.v. The'extent of injuries, if anyi
f.F.14.b.vi. An assessment of actual or potential hazard tothe environment and human health outside thefacility, where this is applicable; and
f.F.14.b.vii Estimated quantity and disposition of recovered' material that resulted from the incident.
I.F.14.c. A written submissi.on shall also be providedwithin five (5) days of the time the Peruittee
becomes aware of the circumstances. The written
submission shall contain a description of the
noncompliance and its cause; the period of
noncompliance (including exact dates and tines);
whether the noncompliance has been correctedl
and if not, the anticipated tiure it is expectedto continuei and steps taken or planned to
reduce, eliminate, and prevent recurrence of t5e
nonconpliance. The Pernittee need not complywith the five (5) day written notice requireme:-.tif the Executive Secretary waives therequirement and the Permittee subrnits a rrritten
report within fifteen (15) days of the time the
Permittee becornes aware of the circumstances.
l'loduleI-page7
I.F.L4.d.
r.F.15.
r.F.16.
All applications, reports
reguest,ed by or submitted
Secretary shalI be signed
required by R450-3-3 . 3 .
I. H. CONFTDENTTAL TNFORMATTON
I.F.7-7.
I.F.18.
I.G.
The Permittee shall couply with the reporting
requirernents outlined in R450-9 in effect at thetime of the incident o '
Compliance Schedules. Reports of compliance or
noncorupliance with, or any progress reports on,
interiro and final requirements contained in any
coupliance schedule of this permit shall be
subuitted no later than fourteen (14) days
following each scheduled date.
Biennial Report. A biennial report shall be
subnitted covering facility activities during
odd nunbered calendar years. This report shall
be subnitted by March 1 of the following even
numbered year. (see R450-8-5.6.)
other Noncompliance. The Permittee shalI reportall other j.nstances of noncompliance not
otherwise required to be reported above, at the
time monitoring reports, as required by thispermit are submitted. Reporting sha1l not
excuse any noncornpliance.
other fnformation. ''Whenever the Permittee
becomes aware that be failed to subnit any
relevant facts in the pernit application, or
submitted incorrect inforrnation in a permit
application or in any report to the ExecutiveSecretary, the Pernittee shalL submit such factsor corrected inforrnation within seven (7)
working days.
SIGNATORY REOUTRE}TENT
or other informationto the Executive
and certified as
The Permittee nay claim confidential any
information require<i to be submitted by thispermit in accordance with R450-11.
I.I. DOCUMENTS TO BE MATNTATNED AT FACTLITY SITE
The Permittee shall naintain at the UTTRfacility, until closure is conpleted andcertified by an independent qualified Utahregistered professional engineer, the following
Modu1eIrpageB
documents and amendments, revisions anduodifications to these docunents:
f.I.1 Waste analysis plan as required by R45O- 8-2.4.'
and this pirmit.
f.I.2. Personnel training documents and records as
required by R450-8-2.7(d) and this pernit.
I.f.3. contingency plan as required by R45o-8-4.4(a)
and this permit.
f .f .4. Closure plan as requ5.red by R450-8-7. and thispermit.
I.f.S. Operating record as required by R450-8-5.3. andthis permit.
I.I. 5. InspectS-on schedules as required by
R450-8-2.6 (b) and this perrni.t.
f . f .7. A copy of the Pemittee I s waste nini:nization
staternent.
I.J. PRoTEcTToN oF HI,I{AN HEALTH AND THE EN TRONMENT
Pursuant to Section 3005(c)(3) of RCRA (Section
2]-2 of HSWA), codified as 40 CFR 270.32(b), and
R450-3-13(b) (2), this peruit contaj.ns those
terms and conditions determined necessary toprotect human health and the environment.
I.K. DEFINTTIONS
For purposes of this permit, terms used herein
sha1l have the same meaning as those in R450Parts 2, 3, 4, and 8 (40 CFR 124, 260, 264 and
27o), unless this perurit specifically provides
otherwise; vhere terms are not defined in the
regulations or the pernit, the meaning
associated with such terms shaLl be defined by a
standard dictionary reference or the generally
accepted scientific or industrial neaning of the
term
trApproved'r neans written approval from the
Executive Secretary of the Utah Solid and
Hazardous Wastes Cornmittee.
rrCommittee" means the Utah So1id and Hazardous
Wastes Comnittee.
Modu1eI-page9
ItComponenttr Deans either the tank or ancillary
equipuent of a tank systeu.
rrExecutive Secretatlzrt Eeans the Executive
Secretary of the Utah Solid and Hazardous l{astes
COrnrnittee.
rracility Plan Approvalrt Deans a written
approval (referred to as a pemit) to operate a
hazardous waste treatuent, storager ot disposalfacility within the State of Utah.
rrHazardous waste eonstLtuentrr means a
consti.tuent that caused the Coumittee to listthe hazardous saste in R450-2 of these
regulations or R450-50-1L of these regulations.
trQualified Utah .Registered Professional
Engineerrr means any individual who ispracticing in oners area of expertise and is
Iicensed as a Professional Engineer by the Utah
Department of Commerce.
trReleasetr Deans any spj.Iling, Ieaking, pour.ing,ernitting, emptying, dischargi.g, injecting,
puraping, escaping, leaching, dumping, or
disposing of hazardous wastes (including
hazardous waste constituents) into the
environrnent (including the abandonment or
discarding of barrels] containers, and other
closed receptacles containing hazardous wastesor hazardous waste constituents).
"Submit or Submissiontt means to be received by
hand delivery, certified nai1, maiI, expressnail, facsimile, and/or computer diskette as
required by this permit and logged in at theoffices of the Bureau of Solid and Hazardous
Waste.
ItWaste streamrr neans a waste that, is or should
be, identified as a line iteur on the Uniform
Hazardous Waste Manifest from the same source of
generation delivered with the same waste load.
ModuleI-page10
I.L. REOUTRED SUBMTSSTONS T'NDER THTS PERMIT
The Permittee sha1l subruit the following
documents - to the Executive Secretary asspecified by permit conditions:
Recnrired Submission Reference Date or event
1. If Peraittee wishes I.F.2. Subruit an applicationto continue an activity for a nen perDit at
allowed by this permit least 180 days beforeafter the opiration of the peruit expires
date of the peruit
2. Written submission of I.F.14. Provided within 5
noncoupliance which nay days of the tine the
endanger human health or Perznittee becoues
environment aware of the
circumstances unless
uaived by the
Executive Secretaryin which the tirne is
extended to 15 days
3. Prog.ess/Compliance I.F.15. Subnitted no later r
Reports than t4 daysfollowing each
scheduled date
4. Biennial report f.F.16. March 1 of thefollowing even
numbered year
5. Other noncompliance I.F.17. At tiure monitoringreports are
subnitted
6. Time schedule for fI.E.l. After initial 72 hourcorrecting deterioration period, submitor malfunction schedule to correct
problem
7. Copy of inspection If.E.4. Within 9O days offorms effective date of
permit
8. Submit schedule for II.H.2. within 90 days of
routine testing of effective date of
emergency equipnent permit
ModuleI-page11
I.}'. REOUTRED NOTIFICATIONS T'NDER THTS PERMIT
The Permittee shalI notify the Executive Secretary as
specif ied by permit conditions:
Recnrired Submiss ion Ref erence
Submit clo=rr" schedule -II.K.4 .with estinated tine to
conplete each closure
task
Date or event
Within 90 days ofeffective date ofpermit
Date or Event
60 days prior to
initiation of
changre
Advancenotification of
any change which
may result in
noncompl iance
Notify new owneror operator inwriting of
requirements of
R450
Report orallywithin 24 hours
Report all
instances of
noncompliance not
otherwise reguiredto be reported
written notification
180 days prior to
expected date for
flcilitywithin 24 hours c.rf
detection of sPi1l
( verba 1 )
t{ot i,f icat ion
1. Planned physical
change
2. Anticipated nor-
compliance
,'. Ownership, operation,permit transfer
Danger to humanhealth or the
environment
Other noncompliance
Notification of
c Iosure
Renoval of spilled
material that cannot
be accomplished
r.rithin 24 hours
5.
Reference
r.F.g.
I.F.11.
r.F.L2
I . F. 14
r.F.17
Ir.K.3
rv.E.1.b.
Module
Notif ication
8. Occurrence of leakor spill to the
environnent
9. Report of leak tothe environnent
10. Sched,ule ofsubmitting samplingresults if cannot be
accomplished within
30 days
Reference
IV.G.1.
IV.G.3.
IV.G.3.c.
Date or, Event
Within 24 hours of
detec€ion of spill(verbal)
Within 30 days of
detection of release
Within 30 days of
detection of release
Modu1eI-page13
Module II - General Conditions
1 TTODI'LE II - GENERAIJ FACILItrY COITDITIONS
rT.A. APPLTCABTLTTY
The reguirements of this permit module pertain
to all hazardous waste manageuent unitsidentified within Module IV.
II.B. DESTGN AND OPERATTON OF FACTLITY
The Permittee shall uaintain and operate the
storage and treatment tanks and surrounding
areas to uiniuize the possibility of a fire,
erqllosion, or any sudden or non-sudden releaseof hazardous waste constituents to air, soilr oE
surface water vhich could threaten human heaLthor the environment.
II.C. GENERAL WASTE ANALYSTS
II.C.1. The Permittee shal1 follow the procedures
described in the Waste Analysis Plan, AttaehnentII-1. In addition, the Permittee shall courplywith the conditions of rI.C. and any other.- conditions involving waste analysiS in Module
IV.
II.C.2. The Perrnittee shall perform analys5.s on the
water in the tanks after each use before being
. II.c.3. The Per:nittee shalL perform analysis on dried
sludges in evaporation pond before sludges are
removed.
fI.C.4. The Pernittee shall perform analysi.s on allsolids removed from tanks.
If.C.s. All analysis will be for pH, EP Toxic Metals,
and Tota1 Metals. Metals analysis includes:
Ag, As, BE, Cd, Cr, Ni, Pb, Hg, S€, and T1.
rI.D. SECURITY
The Per:nitiee shall comply with security
conditions and procedures as outlined in their
application and ccntained in this permit as
Attachment II-2.
Modu1e II - page 1
II.E. GENERAL TNSPEETION REOUTREITTENTS
The Peruittee -shall follow the inspection
schedule found in Attachment ff-3. In addj.tion,
the Permittee shall cornply with the f,ollowing
conditions as veIl as conditions pertaining to
inspections in Module IV:
II.E.l. The Petmittee shall remedy any deterioration orualfunction discovered by an inspection as
required by R450-8-2.6(c) within seventy-two
(721 hours. If the renedy reguires raore tinethe Permittee shall subroit to the ExecutiveSecretary, before the expiration of the
seventy-two (721 hour period, a proposed tine
schedule for correcting the probLem.
II.E.2. Records of inspections shall be kept as required
by R450-8-2.6(d). All annual tests for tankcorrosion, foundation integrity, and secondary
containment integrity must be certified by an
independent, qualified, Utah registeredprofessional engineer.
ff.i.g. " Any problern which could endanger human heaLth orthe environment (tank rupture, dike failure,transportation spilIs, etc. ) shaIl be corrected
as soon as possible, but no later thantwenty-four (24) hours from the tine the problem
is discovered.
II.E.4. The Permittee shall, within ninety (90) days
from the effective date of the permit, submit to
Executive Secretary an acceptable inspectionform'that, upon approval, shalI become a part of
Attachnent II-3.
II.E.S. Problens found during periodic inspections
conducted under this Module shall be correctedwithin the time frame stipulated in ConditionsII.F.1 and 3. If, upon determination by the
Executive Secretary or the Perroittee, continued
operation of the waste management unit involvedin the inspection could endanger hunan health
and the environment, the Permittee shall cease
operation of the unit until the problen hai been
corrected.
IT.F. PERSONNEL TRATNING
The Permittee shaLl conduct personnel training
as required by R45o-a-2.7. This training
Modu1e II - page 2
rr. G.
II. G. 1.
rI. G.2.
rI.H.
rI.H.1.
Ir. H.2.
II.H.3.
II.H.4.
prograu shall follow the attached outline foundin Attachment II-4. The Peruittee shallnaintain training docrrments and records asrequired by nCSo:8.2.7(d) and (e). New
personnel working with or around the hazardous
waste areas shaIl couplete the reguired
personnel training within six (6) months oftheir hire date. These records sha1l indi.catethe tlpe and amount of training received.
GENERAL REOUTRE!,TENTS FOR TGNITABLE. REACTIVE, OR
INCOIITPATTBLE WASTE
The Peraittee shall eornply with the requirenentsof R450-8-2.8. and the requirements of all
applieable National Fire Protection Association
(NPPA) codes.
In addition to the requireuents of R450-8-2.8.,the Permittee shall comply with the conditionsof Module IV pertaining to ignitable, reactive,or incompatible waste.
PREPAREDNESS AND PBE\TENTTON
Reouired nquiprneni. of a minimum, the Per:mitteeshal] equip and naintain in good operatingcondition at the facility the equipment setforth in Attachment II-5 as required by
R450-8-3.3.
Testincr and !,laintenance of Equipment. ThePermittee shall submit a schedule for testingthe eguipnent specified in Condition II.J.1.
Access to Communications or A1arm Svstem. thePernittee shall naintain access to the
co"munications or alarm system as required by
R450-8-3 .5.
Arranoe:nents with Loca1 Authorities. ThePermittee shal1 atteurpt to nake arrangementswith State and 1ocal authorities as required byR450-8-3.7. ff State or local officials refuseto enter into preparedness and prevention
arrangements with the Permittee, the Permittee
must document this refusal in the Operating
Record.
Module fI - page 3
II.I. CONTTNGENCY PI,AN
II.I.1.- frnplementation of Plan. When dictated by the
Contingency PIan the Permittee shall imnediatelycarry out the provisions of Attachment II-6, andfolIos the euergeney procedures described by
R450-8-4.7. whenever there is a fire, explosion,or release of hazardous waste or hazardous wasteconstituents whlch threatens or could threaten
human health or the environment. The Pemitteeshall cornply with R450-9 in reporting releasesto the Executive Secretary.
II.I.2. Copies of PIan. The Permittee shall comply withthe requirements of R450-8-4.4.
fI.I.3. Amendments to Plan. The Permittee shall review
and immediately anend, if necessary, the
contingency pIan, as required by R450-8-4.5.
II.J. RECORDKEEPTNG AND REPORTTNG
II.J.1. The Permittee shalI maintain a written Operating
Record at the facility in accordance with
R450-8-5.3. and R450-50-1D.
fI.J.l.a. Within the Operating Record the Permittee shaIlnaintain at the facility, a written wasteninimi.zation certificati.on in accordance with
R450-8-5. 3 .
' If.J.1.b. The Permittee shall comply with the biennialreport requirements of R450-8-5.6, by March 1 of
each even numbered reporting year. The reportshall include wastes generated, treated and/orstored, 6t the Permitteers facility during theprevious odd number year as requi.red byCondition f.F.16.
II.K. CLOSITRE/POET-CLOST,IRE
II.K.1. Performance Standard. The Perrnittee shaI1 closethe facility as required by R45O-B-7. and
Attachment ll-7.
II.K.2. Amendment to Closure/Post-Closure P1an. The
Permittee shall amend the closure/post-closureplan in accordance with R450-8-7. whenever
necessary, or when required to do so by the
Executive Secretary.
Modu1e ff - page 4
rI.K.3
rI .K.4.
Ir.K.5.
rI.K.6
Notifieation of Closure. The Petmitt,ee shallnotify the Executive Seeretary at Ieast 180 daysprior to the comnencement of closure. Uponnotification of closure, which shall be in thefora of rrritten correspondence addressed to the
Executive Secretar-y, the closure plan containedin Attachnent II-7 will be nodified as necessary
and resubnitted to the Executive Secretary for
approval for each hazardous waste nanageuentunit undergoing closure.
The Peraittee shall subnit withln ninety (90)
days of the effective date of the permit, a
schedule that gives the estiuated tine toperfora each closure activity
Time Allowed for Closure. After receiving thefinal volume of hazardous waste, the PermitteeshalI treat or remove from the site all
hazardous waste in accordance with the schedule
specified in Attachment fI-7. After receivingthe final volume of hazardous naste, the
Permittee shall conplete closure activities in
accordance with the schedule specified in
Attachruent II-7
Certification of Closure. The Permittee shallcertify that the facj.lity has been slosed in
accordance with the specifications in Attachment
TJ:7 as required by R450-8-7., and provide acertification by an independent, qualified, Utah
registered professional engineer.
l{odule II - page 5
AITACHMENT II . 1
Waste Analysis PIan
SECTION 1 . PROJECTDESCRIPTION
1-1. The lithium battery disposal facility is designed to deactivate battery pou,er
supplies used in the MinuteEran Extended Survivable Pourer Sptem.
t-2. General objectives of research conducted under the permit are evaluation of the
prosess and characterization of the waste generated. More specifically, the waste
generated will be tested for extraction procedure leachable metals, total metals content
corrosivity, and free liquids. These data will help determine any environmental or safety
hazards associated with the waste produced. In addition these data may help in the
development of better prooesses for deactivating lithium batteries.
1-3. The general objectives of sampling and analysis conducted under this plan are:
collection of representative samples, accurate analysis of samples, ond evaluation of
sample results based on quality assurance guidelines. These goals will be accomplished
by using the EPA sampling and analysis methods outlined in Technical Order (TO)
35F13-8-1 and Table I of this Waste Analysis Plan.
SECTION 2 - PROJECT ORGAI.IIZATION
2-1. The Aerospace Vehicle Equipment Division (LtrIA) at Hill AFB has overall
responsibility for operation of the facility. Day to day operation will be accomplished by
a crew of 4 people, one supervisor and three technicians, in the Propulsion Unit
(LMAP). These people will accomplish the following tasls as outlined in Technical
Order 35F13-8-1.
a. Discharge batteries.
b. Burst batteries.
c. Circulate water through the burst batteries until the chemicals they contain
fully react.
d. Analpe the water for pH using an electronic pH meter and neutralize the
water.
e. Sample the water for corrosivity and metals analyses by the Science and
Engineering and Technical Chemical Laboratory (TIEL,IC).
f. hmp the water to the evaporation pond when analyses are complete.
L- 1.
L
g. Sample the dried sludge in the evaporation pond.
h.
analyzed.
Remove and dispose of the dried sludge when the samples have been
The Precision Measurement Equipment Laboratory Unit, TTWL, will calibrate the pH
meters and SOZ detectors used by field personnel. Equipment calibration will take place
monthly.
2-2. After samples are taken by LMAP personnel the samples will be transported to
Hill AFB for analysis in the Chemical I-aboratory (TIELC) by the following people.
Laboratory Supenrisor: The I-aboratory Supervisor, oversees the Project Analyst
and Quality Assurance Manager, reviews the datq and gives final approval to the
report. He/She ilssrues the project goals and objectives are recogntzed and that
efforts necessary to their attainment are implemented. A position description is
attached (Attachment 1).
Project Analyst: The Project Analyst is responsible for performing and
overseeing all testing connected with the project. As part of his/her duties, the
Chemist will calibrate the instruments, prepare b1anl6 and samples, run
standards, blanls, and samples, calculate results, and draft laboratory reports. A
position description for the Project Analyst is attached (Attachment 2).
Ouality Assurance Manager: This individual has the responsibility to ensure tlat
i, all reported data meets the quality assurance objectives associated with the
project. When problems arise that have the potential to adversely affect data
quality, the manager will make recommendations to the project analyst or
management to ensure appropriate corrective actions are taken. The Quality
Assurance Manager will be independent of the project analyst. A position
description for the Quality Assurance Manager is attached (Attachment 3).
2-3. The Directorate of Environmental Management (EM) has responsibility for
overseeing compliance with environmental laws throughout the ICBM Product
Directorate including LMAP. As part of this mission they will review all laboratory
reports on the facilities wastes and insure the waste is handled within the provisions of
the permit, EPA laws, and state regulations. In addition they will perform an initial on-
site compliance inspection followed by quarterly inspections.
2-4.The Directorate of Environmental Management (EM) also has responsibility for
base wide environmental compliance. They are the authors of the permit application
and are the point of contact for any permit related issues.
L-2
2-5. The ICBM Product Directorate (LM) is responsible for procuring new batteries
and provided the engin-eering support, through a contractor, for design of the facility.
The contractor who designed the facility was GTE.
SECTION 3 . OA OBJECTIVES
The overall objective of the testing described herein is to evaluate the potential
hazard to the environment of waste generated from deactivation and neutralization of
lithium batteries. Materials generated during the disposal operation will be tested using
established EPA methods. These materials will be handled as hazardous waste until
testing proves them to be nonhazardous as set forth in the permit.
Accuracy is the degree of agreement of a measurement,or avetage of
the salient pointsmeasurements, with an accepted or true value. Listed below are
affecting the accuracy of the proposed measurements.
a. Reference Materials - Only the highest quality materials will be used for
standard reference materials. The standard solutions used in testing will be made from
certified standard solutions.
b. Instrument Performance - The instrument performance will meet those
listed in EPA publication SW-846 for hazardous waste testing. The frequency of
calibration and re-calibration procedures will follow those set forth in the analytical
section of this document.
c. Analytical Performance - The overall performance of the analysis will be
monitored through the regular use of blank samples and surrogate standards. Each
sample will be spiked with a surrogate standard (not already in the sample) containing
each of the metals being tested. The surrogate recovery will be calculated from the
following equation.
Vo recovew = ppm of metal found in sample * l00Vo" ppm of metal added to sample
Surrogate recovery will meet those guidelines set forth in the analytical section of this
document.
L-3
3-3. Precision is a measurement of agreement among individual measurements of a
partiorlar sarnple property. Precision goals for the analyses are for the relative percent
difference (RPD) to be < 20 percent. For the initial calibration the RPD for the analyte
concentration will be < 20 percent over the full range of calibration. The surrogate
recovery will have a RPD < 20 percent.
34. Completeness is the number of samples taken for which results will be obtained.
It is the goal of this project to obtain results for at least 95 percent of all samples taken.
This goal will be attained by adhering strictly to chain of custody procedures, taking
appropriate precautions to preserre samples, and by following the laboratory procedures
set forth in SW-846.
3-5. The major issues of representative samples are addressed in the sampling portion
of this document. The chief concern in laboratory testing is that the sub-samples
subjected to test procedures be representative of &e bulk sample. All samples will be
thoroughly mixed prior to taking an aliquot for analysis.
3-6. Corrosivity samples from this project will be reported in pH units. Total metals
analysis of sludge will be reported in mg/Kg on a dry basis along with percent moisture.
EP toxicity and water sample results will be reported in units of. mg/L. Results from the
analysis of all similar matrices for a given analyte will be reported with each set of
samples.
SECTION 4 - SAMPLING PROCEDURES
4-7. The sampling procedures to evaluate waste from the lithium battery disposal
facility are surlmaized in Table 1. The table indicates sampling frequencies, locations,
methods, responsible sampling personnel, and analysis method.
4-2. Prior to sampling, as indicated in Table 1, the circulation pumps will be run for
at least 15 minutes. This procedure will thoroughly mix the tank and provide a
representative sample of the burst battery and acid water. Samples taken for field pH
analysis will be split and an aliquot placed in a labeled and precleaned 500 ml wide
mouth bottle for duplicate analysis by TIElf. The residual samples from the field pH
test will also be placed in labeled and precleaned 500 mI wide moutl sample bottles for
transport to TIEIf. At the time of sampling a chain of orstody documents will be
initiated for all sanples. It will follou, the sample throughout analysis.
l-4
4-3. Sampling of solid and sludge material deposited in the evaporation ponds and
tanl$ will be accomplished using scoop/shovels in accordance with Table 1. At no point
in time will the solid and sludge material be allowed to accumulate more than 18 inches
in depth. Samples will be taken at three random points tno feet from the perimeter of
the pond and at three random points in the center of the pond. These separate samples
will be combined to form one aliquot for analysis. The sample container will be a
labeled precleaned wide mouth 500 ml bottle.
44. Any free liquids in the evaporation pond will be sarnpled. These samples will be
taken at four random points around the perimeter of the area wetted by free liquids.
Two additional points near the center of the area will be sampled. These six samples
will be combined to form one aliquot for analysis. The sample container will be a
labeled precleaned wide mouth 500 mI bottle.
4-5. Between each sannpling event sarrpling tools will be thoroughly decontaminated.
The sampler will be scrubbed with detergent water using a soft bristle brush, followed by
a rinse with copious amounts of water.
SECTION 5 . SAMPLE CUSTODY
5-1. A sample custody document, Figure 1, will be initiated with each sample. The
document will follow the sample through all phases of transport, storage, ond analysis.
In addition the sample will be logged into the lab and each analyst will sign the log when
they take possession of the sample.
SECTION 6 - CALIBRATION PROCEDURES
6-1. New standards containing each analyte as described in SWS 646 Method 6010
will be prepared quarterly, except silver, which will be prepared monthly.
6-2. The instrument will be set to proper operating parameters as specified by the
manufacturer.
6-3. The instrument will be allowed to become thermally stable before beginning
(this requires at least 30 minutes of operation prior to calibration).
1-5
64. The instnrment will be profiled and calibrated according to the instnrment
manufacturer's recornmended procedures using the calibration standards described in
Step 6-1.
6-5. The solution will be flushed by the calibration blank between standards.
6-6. The average intensity of at least three multiple exposrues of the standards will be
used to generate calibration curves.
6-7. The instrument will be normalized using the manufasturer's recommended
procedures at least once a day.
6-8. Before beginning a sample run, the highest mixed calibration standard will be
run as if it were a sample.
6-9. Concentration values should deviate by less than or equal to 5 percent (or the
established control limit whichever is lower). If not, the instnrment manufacturer's
recommended procedure should be followed to correct for this condition.
6-10. For pH measurements, the calibration procedure will involve the use of nvo pH
buffers which bracket the sample pH. The two buffers solutions will be tested
successively until the two buffer solutions read within 0.05 pH units. The pH meter used
will have an automatic temperature compensator.
SECTION 7 . A}{ALYTICALPROCEDURES
7-1. The deactivation and neutralization tank samples will be tested using an ICP and
an electronic pH meter using procedures set forth in EPA methods: 9040, 6010, 9095,
and 1310 as described in EPA manual "Test Methods for Evaluation of Solid Waste.
Physical/Chemical Methods," 3rd Edition. The test will be run without deviation from
the procedures as outlined.
L-6
SECTION 8 . DATA REDUCTION. VALIDATION. A}.ID REPORTING
8-1. At each stage of the analysis data will be reviewed for completeness and, based
upon previous experience, reasonableness. Any missing data will be provided and
unusual results verified. As much as possible, data reduction will be by computer and
scientific calculator. \Uhere manual data menipulation procedures are required, the
utmost care will be exercised to reduce the resuls. Data reduction will follow relevant
EPA reference methods.
8-2. These tests involve the performance of chemical analpes by one or more
chemists and technicians. For this reason, data validation and coordination are
important. Internal tracking has been addressed elsewhere in the sample orstody
section. At the conclusion of the analyses, the data will be checked against the original
furnished information and the analysis requests to be sure the required tests and analyses
have been performed. The validity of the data will be tested througb the analysis of
blank duplicate and when needed matrix samples. The blank sample results will
demonstrate the absence of laboratory contamination in the samples. Duplicate analyses
glve a measure of analytical precision. Analysis of matrix spike samples permit accuracy.
8-3. The data will be reported as components identified and the quantities present.
The final report will include example calculations where needed and descriptions of the
equipment and procedures. Complete data packages of raw sample and calibration data
will be furnished upon request. A sample report forrr is shown in Figure 2. Field
analysis data witl bL reported on the form shbrvn in Figure 3.
SECTION 9 - INTERNAL OUALITY CONTROL CHECKS
9-1. For each set of samples, a check standard sample containing a knorvn amount of
each analyte will be tested. Its concentration will be in the range normally encountered
during testing. The check standards will constitute a minimum of 10 percent (at least 1)
of the test samples run.
9-2. If the standard does not read to + 10 percent of the known value of each
analyte, the instrument will be renormalized and the samples and standards retested. If
the standard does not read back within the above limits, the instrument will be re-
calibrated. If the problem persists, corrective action procedures will be initiated.
1-7
SECTION 10 - PEPS'oRMANCE AtlD SYSTEM AUDITS
1S1. Performance and system audits wil be performed semi-annually by the project
ual),sq quality assurance man4ger, and/or the laboratory supervisor. Sptem audits will
be conducted before the beginning of the project. This will include verifrcation that the
instnrments are in proper operating conditions and that adequate supplies and spare
parts are on-hand for the project.
lG2. Laboratory performance audits are conducted prior to the implementation of any
new protocol and periodically during the performance of analpes. When available, audit
samples from outside sources are used to measure system performance. Otherwise, in-
house audit samples are prepared and analped.
SECTION 11 - PREVENTATIT/E I,IAINTENAI.ICE
11-1. The preventative maintenance schedule recommended by the instrument
manufacturer will be followed except as noted below.
ll-2. On the ICP, the vacuum system pump oil will be changed as needed with a
minimum of one oil change per year.
11-3. The nebulizer flow rate will be checked daily to ensure it is within the optimum
range as specified by the instrument manufacturer. The nebulizer will be cleaned and
back flushed at least once a week.
ll4. The nebulizer tip wash slntem will be checked weekly, and witl be used to clean
the nebulizer tip after daily analyses.
SECTION 12 . SPECIFIC ROIJTINE PROCEDURES USED TO ASSESS
DATA PRECISION. ACCURACY. AT.ID COMPLETENESS
l2-1. The precision of the analpes will be tested by the following two methods.
a. The first method involves duplicate analysis of each sample mn on the ICP.
Unless the duplicate analyses yield a reproducibility of t 5 percent (or 0.3 ppm
whichever is greater) for each analyte the sample will be re-nrn after re-normalization.
1.-8
b. The second method iryolves the use of duplicate spike samples. For each
set of sa^mples at least 10 percent of the test samples will be run as duplicate spike
samples. For sets of samples numbering less than 10 at least 1 duplicate spike will be
run per set. The duplicate spike samples will be required to have yields of t 5 percent
(or 03 ppm whichever is greater) of their tnre value or they will be re-nm. If re-running
of the samples does not yield the required analytical precision, then the corrective action
procedures will be instituted.
l2-2. The acanracy of the analpis will be verifred by testing a calibration check
standard solution containing knoum concentrations of each analyte. The number of
check standards will be 10 percent of the test sample with 3 minimum of 1. A minimum
of nro field blanls, a trip btantq and an equipment blanh wil be used to check for
transportation and sampling device contaninates, respectively. The calibration check
standard must read t 10 percent (or 0.5 ppm whichever is greater) of its tnre value or
corrective action procedures must be initiated.
t2-3. The completeness of testing will be determined by making a check sample
consisting of a spiked distilled/deionized water solution 6pstaining 5 times the
quantification limit of each analyte being tested. The percent recovery of the spike must
be t 40 percent or corrective action procedures will be undertaken.
124. Field pH measurements will have split samples returned to TIEI-C for duplicate
analysis. If a duplicate analysis varies by more than t 15 percent from the field analysis,
corrective action will be taken.
SECTION 13 - CORRECTIVE ACTION
13-1. Any sample not analped by the specified method will be considered
unacceptable and will be rejected. Re-analysis by the approved method will be the only
acceptable way. Equipment found to be out of calibration or operating improperly will
be repaired or replaced before analpes proceed. Data generated under these
circumstances will be thoroughly examined to determine what repeat measurements are
needed to assure data quality.
l3-2. If weaknesses or problems become apparent during system or performance
audits, corrective action will be taken to remedy the condition. Examples of corrective
actions include re-calibration, maintenance of instnrmentation, replacement of reagents
when analysis blanls are unacceptable, etc.
1-9
13-3. The project analyst and co-workers will be responsible for initiating corrective
action and the quality assurance manager will be responsible for determining if this
action has resolved the problem.
SECTION 14 - OUALITY ASSURANCE REPORTS TO MANAGEMENT
L4-L. Quality assurance reporting and documentation are important elements of final
project reports. Reports provided to customers will contain sections which describe the
quality assurance/quality control activities and criteria relevant to the project. Such
reports will address the impact of these results on disposal, etc.
14-2. The quality assurance procedures used in the analytical prograrns will generate
sufficient documentation to indicate data quality. Assurance results will be included in
the final report. All data generated including the reports will be reviewed by
management, as indicated by Figure 4. All aspects of the project will be discussed
regularly by the appropriate laboratory personnel.
L4-3. All sampling and analysis data and reports will be reviewed, as a further QA
check, by TIELC before submission to the Propulsion Unit or to regulatory agencies.
L4-4. The quality assurance manager will make independent checks of data quality and
reports them to management.
SECTION 15 . DOCUMENT CUSTODY AND FILING
15-1. Copies of all lab reports, chain of custody documents, permits, log books,
operating instructions, and this sampling plan will be maintained for five years by LMAP
at UTTR. These documents will be available for inspection by State or Federal
regulatory agencies upon request. In addition, copies of all lab reports will be routed
from TIELC to LMAP, LMMRO, and EM.
1,-L0
rIfl,RE 1.
CHAIN OT CUSTODY
HII.L AIR FORCE BASE, UTAII - TIELC IAB
(please prlnt all except s lgnatures )
Sanple number:
Collector's
Duty Phone:
Nane:
Date of Sanple: /
Offlce Synbol:
Tlne of Sample:Hours
Process & Locatlon Sampled:
Sampling Method:
Suspected Courpos ition :
Field Information:
Collector's Signature & Date:
CHAIN OF POSSESSION:
S ignature Title
1-11.
Sanple Nunber:
Free Liqulds Present (Palnt filter Test):
FIG1IRE 2
ANALYSIS REPORT FOR}I
rOR TEE
LITHIT'U BATTERY DISPOSAT trACILITY
Analyst:
Yes No
pH of Llqulds:
I{etals :
Tota1 Concentration Standard Check
Ba ppm
Actual
JPXN
PPN
PPN
PPN
Pm
PPM
Ppm
PPN
PPM
ppm
PPM
PPN
t{easured
Ag
As
cd
Cr
Ni
Pb
Hg
T1
As
Ba
Ag
As
Ba
Cd
Cr
Ni
Pb
Hg
PPN PPN
PPN Pm
Pn
PnPPN
PPM
PPtrI
PPM
PPMSe ppm
PPM
PPM
PPM
Ppm
PPN
PPM pPm
PPM Ppm
PPN PPM
Percent recovery of spike:
Extraction Procedure Toxic Metals :
Extract Concentration
Spike element:
Standard Check
Actual Measured
PPN PPtrI
ppm PPtrI
pPm PPM
PPM PPM
PPtrI PPM
PPMPPM
Pm PPM
-PPM
PPN
Splke element:
PPM
pPm
PPM
Ppm
PPN
PPM
PPM
PPM
Percent recovery of spike:
Notes :
Analyst Signature & Date
QA Officer Signature & Date
Lab l{anager Signature & Date
L-12
FIGI'RE 3
DATA SHEET
FIELD PH T,IEASI'REUENTS FOR THE LITHTUU BATTERY DTSPOSAT FACILITY
Analysts Nane:
Date:
Sanp1e Number:
Phone:
Tlne:Hours
Calibration
Buffer
Buffer
Buffer
Standards :
pH Reading
Reading
Reading
pH
pH
pH Analysis:Tank Nrrmber:
pH Reading Approx. lbs
Carbonate
of Sodium
Added
1-1.3
E
t/
r
F
l
H
;J
r
I
1
O
z-
H
r
l
l
cfr
l
()
B
H
HH
d
hH
(
)
O
fr
l
El
d&
o
ladt
r
1
u
)
*I
N
E
1
()
;
J
t
r
{
H
dOB
H
HE
]
f
r
O(
J
H
O
J&
i
d
l
r
l
H&
&
o
u)
2r
I
1
HP
{
F{
(
)
=
3
Ac
h
()
r
d
rd
!4H
BHH&
=H
o
rd
r
I
I
d&
r{Ff
tr
{
qU
lr
1
=
u)
()
O
4
u
)
Y
FI
H
ch
El
Z
HO
Z
E
.
I
J
F{
l
{
O
Fl
E
()
V)Hdotr
{
rI
1&a2u)
fr
l
FI
tr
{?ahoHd-arr
{uBoFl
Fr
r
$rI
1dPC'HlH
oHEl
lr
l
O
u,
H9
{
d
3'
f;
=
=
3{&
1-
14
a
v,
JC)oe,
hJ4-C)-lr
,
.
d*<F
lr
J
€
t{
.
rp
o
It
t
=
3/
t
>-
(J
(u
r
.
a
3/
'
En
--
oo
(t
)
(-
)
-
-c
t
d<
T
E
L
Lr>J
-
tF
r
>t
.p
)-
-
d,
-O=
-
I.
L
L
>-
c)
l-
d,
-l
a
l
-
<l
-
E
,
-F
L
)
4<
,
Oc
o
t
6|
U
>-
00
-d
,
lr
J
tr
l
-
lr
l
>
O
@l
r
r
<
a/
,
|-
.
<,
v1
tr
t
-t
r
r
<
)-
l-
=
..
r-
tr
.
l
(/
l
J-
J
-
j-
1
c)
FU-
(
/
)
-
t!
O
lr
J
!-
.
6
U'
)
g
lr
J
o<
-
IT
J
NJ
F
-<E
:t
r
I.
L
oc
)
Eu
?
Q4
a
Z
,
lr
J
C)
CL
lr
,
J
r<
FF
lr
,
q/
,
<
CE
I
<
d
!t
-
J-J(
/
,
l
4
,
t
|-
r
-
L)
Io
-
-o
tg
3r
,
Q
-E(
9
J
J=
<
CL
x
F
-F
O
<,
.r
,
j-
31
,
vlF
CI
'
JC
>
((
,
1
t
r
-
x
tl
'
l
FI
r
J
F
aJ
U
r
,
--
t
*
)
Fr
=
F
I
t*
+t
{
.
6
-O
Lr
.
J
-
-F(u
r
--
F(
O
(,
l
rt
lr
l
@
FI
-ar
'
,
lt
)o)
(,
CD
-
e,
lr
tFlr
,--CL
\:-a
.a
-
CL
o
tt
,
J
CD
LJ
Qx
o)
l
!
.d
ll
l
EO
E
tr
,
lr
.
rl
l
lr
J
lr
,
J
I-
l
<
CL
-
--
<
e,
<
.t
l
o
'F
J
H
-J
Cl
-r
-Gu
)
<
-e
:t
r
Ft
oG
o
rl
,
r
o
oo
t?
f
(
)
-
t
.
o
o)
ct
t
tt
t
o)
o
a
J
.
r|
-
at
.
(l
l
le
J
od
J
-
xl
r
J
(
=F
l
-
J
9u
r
rr
J
<
E-
-
F
JO
-3
J
l
-
tr
l
G
x
L,
,(
I
E\
O
r
E'
F
i
-o
-F
la-
C
L
o
rl
,
ro
oo
t?
lf
!
-t
.
oc
D
r
?
,
.
.
.
t
,
CD
O
d
J
r
o|
r
Ul
.
Ul
l
lr
l
E_
e
J
-
xl
r
J
(
=F
F
J
gl
r
,
r
t
l
J
<
XE
-
F
JO
-C
)
F
lr
l
CL
-t
lr
,
}(
l
E\
.
O
r
E}
F
T
-O
-F
aeo
-
e
tr
,
fO
oo
tt
U
)
r
t
-
EC
D
(
Y
'
(
/
}
Cr
l
(,
Fr
J
-
-F
ar
)
;
Ql
)
l*
l
OE
J
-
xl
r
l
(
=F
F
J
qE
J
E'
<
r-
r
E
-
F
JO
-(
.
)
F
lr
J
CL
r.
.
r
lr
,
}(
{
t
E\
.
O
{
3
E}
F
*
3t
)=ot-
aFc)d,Ftt
)-t-
aJl-
a(-
)
t!
,CL
at
)
=t
-
()
O
(
,
-r
>
r
(
OF
t
r
J
-(
JCJ
J
<=
F
L)
<
tL
EQ-
Z
(J
=
1r
)
d,
lr
'
E
J
tr
J
tr
J
CL
F
>
-l
r
<
<<
-
.
.r
'
,
-
d
tt
'
t
a
lr
,
lr
t
EL
-
\Z
F
-
F-
4
-
r
;
1/
l
rt
o.
-
-
-=
l
f
,
OE
-
-
t
HF-
F
=O
t
r
'
)
U-
J
-
r
(
OO
F
I
T
J
a<
,
J
3J
)
J
lr
.
l
O
=
t-
JI
r
J
C
)
<
CL
T
{
E
fr
-
r
s
l
<J
G
)
=
!t
1
<,
d,
GE
,
lr
J
F
l&
f
tr
J
tz
=
F
>
(r
r
r
!
L
<
F-
<
-
-
QA
U
O-
-
-5
r
n
OC
L
-
t
t-
a
l-
-
F
=C
r
t
r
1
lr
J
-
{
OO
F
t
T
J
./
t
<,
J
1r
7
J
tr
J
C
l
=
F
Jt
r
r
C
J
<
CL
h
I
E
El
r
g
!
(-
t
c
)
=
an
<.
d,
do
'
,
lr
J
F
tr
J
lr
J
\4
=
F
>
(
tr
.
l
tr
<
F-
<
-
.n
-
-c
)
c)
tl
e,
<
,
t-
r
O
ll
J
lr
J
l-
l-
<,
e
r
-
u
.
t
(-
,
lr
,
O
L
J
-
OF
C
f
(
J
E
J
Tr
J
-
GE
I
-<
l
r
r
-
L
r
J
Er
r
C
E
-
O
-
r
OC
E
l-
C
J
C
L
C)
lr
,
t
(Y
)
-
dl
r
J
-
-
r(
/
l
Cl
p|
(v
r
t
-
O
-
O
.
-O
tr
J
tr
J
(
3
O
F
.
u
V
J=
C
L
F
-
<
o-
=
<F
-
-O
l
r
J
L
)
<t
r
<
-
O
l
r
-
O
3n
<
,
t
-
J
o
F
(9=l-
{-F't-oEC)=lr
Jolr
Jdu-
Y,=
.<
l
r
J
{
(
>-
F
-
J
F}
I
--
=
oL
)
o
<
<F
F
>-
lr
j
d,
a=
l4
J
lr
J
tr
J
O
j-
d,
CL
-t
FO
-
F
<t
J
.
=
<
E
lr
J
CL
hl
co
H
F
.,
,
1
J
v1
lg
'
l
F
.
<
pr
J
d,
CL
J
I
-
E,
-
J
=
O<
=
u
.
J
u-
tf
,
tL
-
1r
,
Y,
F
-
>-
=
dC
J
E
rl
.
J
<
o
l-
tr
J
O
F
?,
"
<EEl
u,
lJ
-
FC
)
>
tL
tr
,
E<
-
l
-
lr
l
O<
>>
t
r
,
x
1
3
lr
J
J
l
-
O
4r
*
C
D
e,
-
t
r
!
E
o<
o
<
Lt
-
v,
<
L)
!l=
-
<u
.
J
F
.F
E
rt
6
Fl
lr
r
-
*
>.
F
(
)
O
c<
<
F
o
tr
r
>
l
.
l
,
J
=
)-
t
AO
IT
J
F
U
J
t
r
J
A
L)
E
O
.
o<
o
-
=
zl
l
J
u
-
=
o
<6
l
r
l
C
L
r
<
CO
F
F>
-
(,
t
<
,
tl
1
&l
r
J
s
g
pl
L
r
J
J
O
FC
L
J
C
L
e,
j
-
-
J
<
o<
<
=
>
lr
.
El
(,
t
E
tl
J
ll
'
J)-
=
3n
o
(>
r
-F(9
CE
-o1<
t
!
c)
>
Eu
r
lr
JCl
a
fr
J
.!
Ir
J
F
d,o-
a
lr
O
z
:
Ir
r
E
O
co
l
!
o
.
=lr
J
\Z
(.
'
)
t-
cEo
(t
1OD
FT
C\
J
JOD
Aa
J
.t
1
J}
Z<=
lr
l
F
JCL
-
-o<,
d,
q,
tL
Jtr
l==()U'
d,
lr
jCL
=oq,
JcL
l-
O
t-
t
d,
-
Cl
-
=
-oFa
1,
f
,
JCL
F
Fl
r<
e=
CL
=
=o!-
a
.t
)
JCL
F
Q>
r
d,
=a.
=
=c)
lrar
)
JCL
F
Q-
r
c,
=
cL
=
-o!-
a3t
'
,
JCL
F
it
Ed,
=
cL
=
=oF'FC)oJ
y-=<(
a
Fr
h
-aO:
z
-.
(
F^<
-t
</
)
>r
h
c
f
EHl-
.
n
=
L)
!
l
o
(Z
r
-
.
lr
r
<
J
6
F:
z
Y,-F-oF'FhI
^
r-
.
ar
'
l
JG
J
O
(t
-
r
d,
=
i-
Y
,
O
DZ
:
.
r
lr
J
<
J
-J
-
v
J-F-oF'Fhl
a
'
F.
lt
JG
'
O
(t
:
-
e,
=
t-
1
4
O
D2
:
r
lr
J
<
J
-)
-
v
A
3"
C'
'
Ci
lr
J
=t
0oo
e-
=
J
-
.t
,
oEo
!
F4
tt
t
doQ:
r
CL
J
<o>.
n
lg
i,
-oE(
a
E
cl
a-
tr
,
<
O-
Ec
t
l4
J
d,
.
Fa
v)aq
t
H)
Z
J-o<
in
l-
3J
)oc)+l-
F
L^
J
lr
J
=
:C
D==
-'
CL-j/
,
1-
15
Attaehnent 1
IABORATORY SUPERVISOR
Ttre purpose of this posltlon ls to provlde supenrlston over the Chenlcal
Scl.ences Section. Ttre manager asslgned to thls positlon ls responslble for
effective and efflclent utlllzatlon of resources whlch lnclude: hlgh-value
egulpnent, complex and sensl.tlve measurlng devices, conputers, lnstrunents,
facllities, manporrer, and approprlate firnds. Ttrle supenrlslon ls responslble
for individual and cumulatlve actlons of a staff of approxlnately flfteen
section persormel.
l{aior Duties and Responsibilities
1. Responsible for the fuLl and effective utlllzatlon of persorurel within the
unit. Establishes quallty and quantlty objectives, prloritles, and work
standards. Assures that ernpJ.oyees are complylng wlth establlshed standards in
accomplishment of their asslgned rnisslon. Counsels employees, or takes action
for reassignments or removal. Reconmends personnel aetlons; schedules and
approves annual/slck leave, evaluates perfornanee of subordlnates, and assigns
performance ratings. Assures compliance with security reguirements.
Inplenents afflrnative action/EEo and other prograns. Aceounts for tlne
expenditures and certifles tine cards.
2. Reviews work requests submitted to the section end deternines the lntent
of the work necessary. Assigns projects to appropriate staff personnel,
reviews laboratory operations, and approves the results. Incrrmbent ls
norroally available for consultation and assistance as required by subordinate
personnel to solve problens of nonrecurring nature. llhen guldellnes are not
avaiLable, assigns problens to specialists, to devise better nethods.
Resolves problens when there ls a confllct of opinlon on the approach to be
used. Directs the establishnent of new t1pes of investigations and assures
the validity of the information obtained. Prepares work schedules; develops
quallty and guantity perfornance standards; spot checks; work operations; and
revlews of conpleted uork and reports to assure that performance standards and
goals are met. Coordinates work operations as needed with the superrrisors of
other organizatlons and functions.
3. Investigates new trends and eguipuent advertlsed to determlne potentlal
improvements ln automated nethods of analyses, greater efflcl€DClr and reduced
cost. Dlscusses findlngs and eoncluslons wlth superrzlsors ln shops and
lnspection organizations. Investigates new developments Ln processes and
nethods of inspectlon that utllize the equipment on hand. Insures that an
adeguate supply of equlpnent, spare parts, and other materials are uaintalned
to perform the anticlpated sectlon workload. Justlfy all additional items of
equipnent and expedltes procurement of approved items.
l-16
4. llanages the personnel program of the section, includlng posltlon
developnent and asslgnnent of dutles. Encourages the professional developneat
of personnel by arranglng for tralnlng classes, requesting support for
professlonal seminars, technlcal meetings, and conferences. Recrults
personnel when authorlzed and dlrects the assignlng of personnel when reguired
by changes ln workload. Prepares workload estlEates as well as equlpment,
facllltles, and personnel proJectl.ons. Provldes for effective safety by
preparlng and enforclng safety SOPs, by conductlng safety meetlngs for all
asslgned persormel at least nonthly, and by frequent personal tnspectlons of
all section operatlons and storag,e areas to deter:nlne the adequacy of safety
preeautlons taken.
Controls Over Work
1. Receives general dlrection of the Branch Chief, who establlshes overall
policy, procedural requlreroents, and results expected.
2. I{ritten guidelines consist of various broad policies and proeedures from
this and higher headquarters. Established principles, teehnlques, theorles
and philosophles relating to Quality Assurance and prevlously mentloned
disciplines, do not always cover the sltuations encountered. Initiatlve is an
intrerent attrlbute of the incr.rmbent.
3. Ttrrough discusslons and meetlngs keeps the Branch Chlef lnformed of work
progress; problems encountered whlch reguire higher level lntenrention,
declsions and co'n-itment; and subnits nethods-improvenents for Branch
endorsernent -
1-17
Attachnent 2
PROJECT AI{ALYST
1. Trains, tests, and certlfies personnel ln speeiallzed lndustrial
processes.
2. Perfonns chernical analysls of materlal.
3. Provldes chenical englneerlng support and review of chenlcal processes,
equlpnent, and probleus.
4. Provldes laboratory support for accident lnvestlgatlons, materlal reviews,
and preplanning.
5. Provides technical advise and laboratory serrrices for uetals analysis,
processing and substitutlon and supports the netallurglcal laboratory as
required.
5. Provides analysls for contamlnation lnvestlgatlon lncluding chemlcal,
environnental, partlculate, etc., lncludlng photonicrographlc analysis.
7. GontroLs and certifies electroplatlng, painting, chenlcal nllllng, and
eleaning processes, and develops new processes and assures an adequate program
of tralning for operetors.
8. Provides engineering support for Service Englneering, Bioenvironnental,
Safety, Disaster Preparedness, Civil Engineerlng, and other ALC nlssions.
9. Provides USAF conrnands and DOD wlth laboratory support lncludlng
engineering evaluations and tests, prototJrplng, materlal investigatlons and
analysis, and corrosion prevention and control programs.
10. Prototypes and/or dlrects reclamation of high value or critical supply
ehenicals, Daterlals, and petroleum products.
Knowledee Reouired bv Position
1. Professional knowledge of chenical principles, theories, practices, and
established methodology to perforn the full renge of duties involved ln the
chenical and physlcal analysis and testlng of varlous substances and to
provide lnfornatlon pertlnent to a varlety of programs and problens lnvolving
chemical analysls for whlch established nethods are not completely avallable.
Knowledge to edopt and uodlfy technlques to speelal probleus and requlrements.
2. Professlonal knowledge of the prlnciples of eallbrating and operatlng
scientific equlprnent and evaluatlon of data generated from such equlpnent.
1-18
Elemental analytical equipnent such as atomic absorption spectrometers,
electron microprobes, emission spectometers, etc. Compound analysis equipment
such as liquid and gas chromatograph, infrared and visible spectroscopy and
such specLalized equipment as nuclear magnetic resonance spectrometry, mass
spectrometry, and microcoulombmetric techniques.
3. Professional knowledge in methods of chemical analysis of water, waste
water, and pollution control; analytical methods in quality control and
accuracy; analytical method in toxic substance and safety; analytical methods
in plating and cleaning, analytical methods for drugs and narcotics; and
knowledge in general standard analytical methods for routine work.
4. Skil1 in determining the specific data required to answer specific
questi.ons or solve problems related to broad program requirements. Skill in
searching technical data, nicrofiln, and directives, and selection of analysis
techniques, methods, and procedures which rnay be applied to new and
unprecedented reguirements
Suoervisorv Controls
The supervisor assigns the programs to the chemist by setting the overall
objectives, priorities, and resources available. The chemist, having several
years of experience in the work, is responsible for planning, scheduling, and
carrying out the assignments;'selecting the specific approach, methods, and
procedur6s to use; and coordinating the work with other ineluding chemists and
physieal science technicians. The supervisor is kept informed of progress and
major problems. The test report is reviewed from an overall standpoint for
being feasible and effectively fulfilling the assignment's requirements.
s
Guidelines
The chemist is provided the general test directive, manuals of established
laboratory procedures and practices, various standard chemical and engineering
references, and agency policies and practices. Current chemieal and
engineering literature is also available to the chemist. Ihe guidelines are
not completely applicable nor specific to the work. Therefore, the chemist
must use judgenent to select, adapt, and modify the guidelines to solve
specific chemical and scheduling problems and to meet specialized test
requirements that are speeified in the general test directive.
Comolexitv
1. The assignments consi-st of planning and carrying out testi-ng programs. It
involves a large variety of complex analysis which may range from organic and
gaseous analysis through i.norganic analysis and plating. Established methods
L-lg
and practices must be eval-uated to select the most appropriate. Ihis process
involves the evaluation and interpretation of information found in the
scientific and trade literature, the information provided by the serviced
activity, and the data produced in the laboratory. Frequently, modification
of the established methods and practlces is necessary to eomplete the work.
2. The assignnents may consist of projects that involve evaluating,
nodifying, and performing lnstrtrurental nethods that are used to anaLyze
materials, metal alloys, and rel-ated products.
3. The assi-gnnrents consist of a variety of requests from the serviced
activities for data and for sol-ucion of chemical problems. Typically, only
the general nature of the problems of the work is known. Ihe work includes
complexities such as scanty infornation as to what a sample may eonsist of,
unusual analytical requirements, and lack of specific scientific literature
concerning the work. Some assignments consist of applying new and advanced
analytical procedures developed for other substances in order to determine the
validity and applicability of the procedures for the analysis of toxic
chemieals, muni.ti.ons, or other related materials.
l-20
Attachment 3
QUALITY AS SURAI{CE MANAGER
The chemist responsible for the Quality Assurance Program of the Chemical
Science Section, oversees and maintains a high level- of Quality Assurance as
it applies to State Certification. This person docunents, controls, and
validates data for laboratory customers.
The Quality Assurance chemist has the ultimate responsibility of establishing,
overseei.ng, and auditing specific procedures for documenti.ng, eontrolling, and
validating data quality. This position is established to provide chemical
sciences support to the D/M, the D/MM, and ALC, and in certain circumstances,
the locaL civilian conmunity. Specific work elements of this position are:
I"lai or Duties
1. Training and
analytical prior
4. Ensuring that all data Standard
logs, proj eet plans , and analytical
fashion.
qualifyirg personnel in specified laboratory QC and
to receiving samples.
2. Monitoring the Quality Assurance (QA) and Quality Control (QC) activities
of the laboratory to ensure.laboratory practices; and recommending
improvements as necessary.
3. Assisting the data requestor in specifying the QA/QC procedures to be used
during a program.
Operating Proeedures (SOPs) , records,
results are rnai-ntained in a retrievable
5. Ensuring that SOPs and project QA/QC plans are available to al-l
appropriate laboratory personnel.
6. Informing the specific projects manager of noncompliance with the approved
QA program.
7. Establishing the procedures and criteria for evaluating whether analytical
performance is both acceptable and in control.
8. If problems are detected, naking recoumendations to the data requestor
and/ot upper management to ensure appropriate corrective actions are
undertaken.
9. Maintaining documentation of correctlve actions and ensuring chat analysis
implement and documenc corrective actions as they become necessary.
I0. Reviewing laboratory data before the data is released, verifying that
data was collected properly and was in control.
L-2L
11. Ensuring that sample logs, instrument 1ogs, and all QC documents are
properly maintained.
L2. Submitting audit samples to assist in review of QA/QC procedures.
13. Assunes complete technical responsibility for complex long term chemicaL/
analytical projects and in-depth organLzaxional and analytical skills.
L4. Directs chemists and other personnel in complex projects where several
analytical spercialties are required. Provides procedural guidance and
nethodoLogy on such projects.
15. Prototypes new project workloads and wri-tes standard procedures for use
by other 1ab personnel. Trains lower grade personnel in state-of-the-art
methods, chemical safety, data acquisition, and interpretation.
16. Develops methods by which analytical instruments are used for complex
proj ects.
L7. Reconmends instrunent and equipment purchases needed to enhance
analytical capabilities in the laboratory and solve reliability and
maintainability problems in the shops. Writes technical specifications for
such equipment.
18. lJrites reports which are not linited to analytical data but often
includes detailed interpretation of data, recommendations to improve froductsafety, maintainability and reliability, product qualifications to urilitary
specifications, etc.
Re spons ib i 1i t ie s
Ihe inctrmbent chemist is responsible for the Laboratory Quality Assurance
Progrem and State Certification. the individual is responsible for developing
a modifying methods, Infrared Photo Spectrometry, Inductive Coupled Plasma
Spectrometry, and Atomic Absorption Spectrometry equipment. The incumbent
will also train laboratory personnel in the use of such instruments and
methods.
Factors
1. Knowledge Required by the Position:
a. Know EPA and State of Utah procedures and protocols for sampling
testing and handling of Environmental samples. This knowledge is required to
ensure the l-aboratories obtaining reliable results which can be compared with
any other laboratory doing EPA testing. This will enable the laboratory to be
certified ln these test procedures.
L-22
b. Know what ls entalled by good laboratory practlces as well as
analytlcal chemlstry technlques. Ttrls w111 allow Lnproper praetices or
procedures to be corrected and will ensure the leboratory ls nalntained ln
certlflable condltion.
c. Have a lcnowledge of statlstical and dLnenslonal analysis. Sktll in
accuracy and preclsion control llnits of laboretory processes.
d. Knowledge of how laboratory lnstrunentatlon works and the theory
behlnd the analysis.
e. Professional knowledge of the prlnciples of chenlstry, chemlcal
theory, and uodern practl.ces. A thorough knowledge of establlshed nethodology
for perforrning the full range of dutles lnvolved ln analysls, ldentiflcatlon,
and testing of naterlal sueh as platlng solutlons, toxic and hazardous
chenicals, drugs, environnental pollutants, unknown chenlcals, and petroleun,
products.
f. Practical knowledge of industrlal processes; the chenlcal products
used ln conJunctlon wlth alrcraft and aerospace ground equlpnent; and the
industrial use of chenicals and control. of such products in harmony wlth
environmental and reclamation concepts.
g. Sklll in nodlfylng and developing nethods of analyzlng and ldentlfying
chemlcals, chernical eompounds, and derlvatlves. Such skills would be acqulred
through some conblnatlon of professlonal laboratory experience and either a
bachelors, nasters, or doctors degree ln chemistry.
Suoervisory Controls
ltre supervisor assigns the requests fron the senriced activities by defining
the overall objectives and setting the resources available. Ttre superlisor
and chemist discuss the general approach to be taken and the extent and
inplications of the problems involved. Belng a specialist, the chemist ls
conpletely responsible for planning and carrying out assl.gnments; resolving
almost all technlcal problens; coordinating work with englneers, chemlsts,
technicians, and shop employees; and determine the approach and nethods to
use. The work and conclusions of the chenist are accepted as technlcaLLy
authoritatlve and are reviewed only for ueetlng the asslgnment obJectlves.
Comolexitv
The asslgnments consist of analyzing, identlfying, or testlng varlous
substances to provlde a wlde varlety of lnformatlon or solve cornplex problens.
Ttre asslgnments t)lplcally lnvolve noveL or unlque requests for lnfornation
about substances that are new on the market or substances for which the
chenical cornposltlon ls a trade secret. Often there are several approaches
that can be taken, the nethods and procedures are not establlshed, and the
interpretation of the data ls inconcluslve. t{odification of established
approaches and developrnent of new nethods, techniques, or preeedents are
freguently requlred to plan and carry out assignments.
r-23
Seope and Effect
Ttre work lnvolves developlng and nodifying analytlcal nethods and provldlng
expertise for chenical processes; special projects; aglng crlteria; speclal
test prograns; hazards, toxlc, bioenvlronnental problems; and other loglsties
center sclentlfic functlons. Ttre work nay lnclude developnent of crlterla,
procedures, processesr or lnstructlons for the laboretory or the logistlcs
center operatlons. The results of this work affect a wlde range of actlvltles
wlthln the loglstlc center, wlthln AEII, and on occaslon, the clvlllan
comunlty.
L-24
ATTACHMEI.{T II - 2
SECT]RITT PIAI{
SECURITY PI-A}.I
Surveillance System
The UTIR has a Z-hour seanrity s]rstem to control unauthorized access to the DOD
land. It has an 8-foot high 6fo1ia link fence with a locked gate to prevent unauthorized
access to the LBDF.
The main entrance to UTIR is controlled by a seority gate which is manned Z hours
per day. There are also security police on call 24 hours per day. Although the searrity
police do not patrol the entire facility, they do patrol the compound area and the
perimeter fence around the storage/discharge building and deactivation facility. The
lithium battery submodule storage and treatment facilities are both within sight of the
main compound area. The road leading to the LBDF passes the discharge 6uilding and
through a second locked gate before it ends at the deactivation site. OnIy authorized
UTIR personnel have access to the keys which unlock these gates.
All security personnel have access to telephone or radio equipment at all times.
Warnins Sisns
Warning signs have been placed on all roads leading into the UTIR. These signs
identiff the area as having restricted access and potentially hazardous materials or
activities. In addition, there is a sign posted on the gate leading to the discharge
building, another on the gate leading to the deactivation facility. A thfud sign is on tle
treatment facility itself. The sign on the main gate reads:
,DATIGER AUTHORIZED PERSONNEL ONLY"
The sign on the LBDF fence reads:
,DANGER HAZARDOUS WASTES AUTI{ORIZED PERSONNEL ONLY'
Barriers and Means to Control Entry
The UTIR covers several hundred square mils5 and there are roads and dirt trails
throughout the area. Because the operations at the site are hazardous, efforts are
continually berng made to prevent unauthorized entrance to the facility and to keep
those who are present away from hazardous areas.
2-l
ATTACHMENIT II .3
INSPECNON SCHEDULE
GEI{EBAL INSPE-CTION PI-A}.I
The purpose of the facility inspections is to determine if there are or have been any
malfunctions, operator errors, physical deterioration, or discharges which may lead to the
release of hazardous waste or its constituents to the environment, or pose a threat to
human health. Inspection of the LBDF \ilitl be done on an as-needed basis. Inspections
will take place daily during periods of operation and storage of batteries and
immediately after use of the facility.
Inspection of the LBDF is governed by various written regulations of Hill AFB. The
following is a summary of such regulations which cumulatively comply urith UHWMR
8.6.2 and 40 CFR 264.15.
Inspection Schedule
The following schedule of inspections of the LBDF shall be made by the identified
parties:
1. Security devices, including locks on the submodule storage buildings and locls on
the fence gate which allows road access to the lithium battery area, will be
inspected on a monthly basis by the Building C\rstodian Facility Manager to ensure
that they are in working order. Any searity devices not functioning properly will
be reported to the Range Security Officer and Range Civil Engineering on the
date of inspectioq and will be repaired or replaced within a ?A-hour period.
2. Areas subject to discharge of waste materials (e.g. areas around the deactivation
tanks) will be inspected by someone from the base civil engineering office, on a
daily basis to determine whether any spills have occurred. In the case of those
facilities which operate only on an occasional basis, such inspections shall be
conducted only when such facilities have been operating. Any discharges of waste
discovered will be reported to Range Civil Engineering and the f,,ange Fire
Department who will be responsible for immediate cleanup.
3. While in use, the operating and structural equipment wil be inspected by the
ranking offrcer working in the LBDF areas as follows:
a. Above ground structural materials of the tanl$ will be examined for leaks
and corrosion. While in service, the ground around the tanks will be
examined for wet spots or dead vegetation that would indicate an
underground leak.
3-1
b.Discharge control equipment on each tank will be inspected daily to ensure
that the equipment is in good operating condition.
The waste level in the tanls will be inspected daily during operations to
avoid overtopping.
Confinement stnrctures, including dikes, wiU be inspected weekly for
substantial erosion, cracks, or indication of leals.
The evaporation pond will be inspected weekly while in use and after all
stontrs to detect:
1) Spillage on the ground surrounding the impoundment.
2) Sudden drops in the level of the contents.
3) Presence of liquid in leak detection systems.
4) Tears, punctures, or blisters on the lins1, and if all joints and sea^ms are
tight.
5) Any leaks that have occurred which are evident from the leak detection
taP.
I-evels of liquid in tanls will be inspected daily during operations to ensure
adequate free board and avoid overtopping by wind, wave action,
precipitatio& etc.
Any other operating or structural equipment not specified above will be
inspected on a daily basis when operations occur.
If any operational or structural equipment is found to be operating improperly,
damaged, inadequate, or exceeding its capacity, it will be reported immediately to
Range Civil Engineering, and operations which affect that equipment will be shut
down immediately until problem is corrected.
The pH and gas meters which monitor for SO2 in the storage and discharge
buildings, and any other monitoring equipment installed will be inspected weekly
during operations by the ranking officer in charge of LBDF to ensure it is
functioning properly. Any malfunctions will be reported 6 f,,ange Civil
Engineering within 8 hours and will be repaired or replaced within a24 hour
period.
AII containers, including the battery submodules, will be inspected by the ranking
officer in charge of lithium battery storage to detect leals or corrosion. Any leals
e.
g.
4.
5.
or corrosion noted will be reported to the Uthium Bauery Emergency Response
Team at Hill AFB for disposition. If the submodule has not been discharged, it
should be discharged immediately or disposed of with explosives at the UTIR
munitions burn pit after an emergency permit has been sought and approved by
the Utah Solid and Hazardous Waste Committee.
All emergency and safety equipmenq including fire extinguishers, soda ash supply,
eyewash, deluge shower, rinse water, and the first aid kit will be inspected monthly
by the f,engo Safety Offrcer for adequate quantities and proper function Any
equipment found to be not functioning properly wiU be reported to Range Civil
Engineering and will be repaired or replaced within Z hours. Any supplies found
to be inadequate will be reported to the Base Supply and will be replaced within
24 hours.
A log of all inspections made as called for above will be maintained at the LBDF. The
log will include:
- The date and time of inspection
The item(s) inspected
- The name of the inspector
- Observations made
- The date and nature of any repairs made or remedial action taken
These records shall be kept on file in the Range Civil Engineering Office for at least 3
years after the expiration of this permit.
Tanks
The deactivation and neutralization tank inspections will include an annual leak
assessment as required in Module IV of this permit.
The equipment used in battery discharge will be inspected prior to each use for damages
that may result in injury. The equipment requiring inspection prior to use includes sulfirr
dioxide meter, insulated tools, load cables, and discharge metering devices.
The pH meter used to determine the efEuent water pH will be checked for adequate
battery charge prior to calibration or use in analping the water pH.
The pump house equipment, all piping and hoses, tanls, discharge equipment, and
circulation lines shall be inspected for damages prior to each use.
A record of the equipment inspections shall be kept as part of the inspection record.
Any equipment found to be damaged or inoperative shall be corrected or replaced prior
to battery discharge or deactivation.
Reporting and Record Keeping
In addition to correcting all detected problems as described in this attachment and
required by 40 CFR 264.15(c) and UHWMR 8.10.5.(c)(1), applicable reporting
requirements required by permit Part I, Section I, shall be met.
All inspection records must be maintained at the UTIR facility.
34
ATTACHMENT II I 4
PERSONNEL TRAINING PROGRAM
PERSONNEL TRAINING PROGRAM
All personnel that work in the LBDF must pass a basic instruction course prior to their
work assignment. This training course includes, but is not limited to, the areas of lithium
battery construction, proper destruction techniques, ffid proper storage and
transportation of the batteries. Lithium battery personnel are also trained in the proper
emergency response techniques, as are all base personnel. Current training programs
ensure that the facility personnel are able to respond effectively to emergencies,
specifically in the areas of communications and alarm systems, to fires and explosions,
and shutdown of operations. Additional training of UTTR facility personnel will be
implemented, to insure that the personnel are aware of all emergency procedures
outlined in tle Contingency Plan, and that the proper record keeping procedures for the
UHWMR are instituted.
The job title of the personnel who will operate this facility is "Minuteman Missile
Maintenance Specialist" with the military specialty code of 411X1A Attached is the job
description for the personnel working at this facility. Documentation of training and job
experience, training requirements, and personnel filli"g such positions in the LBDF are
available at Hill AFB upon request.
U.S. Air Force Training Program
The Air Force has a very extensive training program in place where all personnel receive
extensive training in the areas of their assigned duties and responsibilities.
Training aids (videos, hardware, and manuals) have been developed to assist in training.
This training focuses on learning and following the procedures of the technical order for
deactivation. This training includes procedures to operate and maintain this facility in a
safe manner. On-the-job training will be used to maintain proficiency and to train new
personnel.
Hazardous Waste Management Training
All employees who work at the discharge or deactivation facility, or directly implement
any part of this permit, shall participate in a minimum 7 hour annual hazardous waste
management training. The training must cover the handling of reactive and corrosive
wastes and all the terms and conditions of this permit (with attachments). In addition to
providing the training yearly, the training must be provided to all new employees of the
discharge and deactivation facility.
4-l
The training shall be taught by a qualified individual(s). Information which verifies the
instructor(s) qualifications shall be kept as part of the record. A record must also be
kept of the names of individuals panicipating in the training, ffid the times of the
participation.
4-2
AF* ..=9- 1 (C71
2. DUTIES AND
ir. Alvscs ott trr'ltttic'ol probknts relorcd nt ccttr.liXurotiotr.
('lr(('lroitt. tru,tsilott, o\Scrrihl), ittstttllotnn, oiltl in\lrcctto,t o/
t,ttJrr/cs oni ttttssilr suh5.1 5vrnrJ. atttl relot(cl sttPport equtP'
t,t('tt!. sol\ cs unusu.rl nroblems enL'ountcrcul in thc
lr.rri)irort.rnd J\\cnrhlr ol'nttssiler ut olrerJtl()n:rl or lest
5ltt. Pr€l1uf r.r l.rultr,h cn111l.,r-Cnlcnt iJre.t lor filultnr:. u rth
ntls:ilc L:ndr.tIcs nrisr:lc .rn..l ion]lton?nt p.rrls. l)er[urrn:
i n r irc(t t(rns. :r nr.l .r\\e I':r h Ic> n'i I \rr lc. coml.r()nc n [ [i.t rl 5. u ncJ
:.,t'r\ \iJ:::l [i'::':];r'. C'S C'r .titi'!rt'' PfCSs'[\:llt\ C5. tJCSiC'
(.:iir. JnJ ccl\er.i ltcrr:o\e:.rnd tnsl.rll> tcsi lrnCs. cillc:.
nl.rtt.r. und firtrrrcr. Joins ntr\:ilc s3t'tions lnJ m:,Ites
nlt:.:iu to luunr.h ll.ru Pc:l('rnt: sJhcduleJ l'rg\enlltr'
[1].:rnie!':.rn(e in>1\gctrr!n\ [r:rlu:rtc: insPcctton reslrlts
.t",i! n-..:k,:: dect:it,n. ttU.!rtJ;ng ci:mPoncnt tclrl.tccmcnt.
1i;!i',i.,,nt'i: rcp:rrr. :rnJ rel-:r rtr()i:iJurc5. I)r.rgn('5cS
o. -'r "''- .' n'1.:li t;r.,.'l:.t1,5 .tiJ ICr,'nn'.n;cnds C(lrrt. :lVjr I \ r, I | .. a a
.r. i-,,F, bi tntir.rlipn r.l Lr,5.:ll5t-r.t(rr)' fClrq,rt:. l.r:lurC rC.
l1',il:. Of p;O11.,:CJ i1';oJ;li.'.:liOn:- SCfriCC:. Ii-.5le(:S.
ir i'.::i). mJtn::irir. Ch:'i.\. tCSl5. and OI)CrulcS rClllcd
).:;';' l:i C'Gt;;iminl
h l'r'rt(,rttt5 Ot;tl .\tt7 'rl'ltr'i J('rt'r;!ttlL' O.l tttt55,lt x:tl: ltiCl.
f;?\t'5. Ot:rl ltthrt. ut:t\. \i.-;r,F:o:'s re=1ote conl:'rrilc'i "r.j
i't'..:r,t..!! sri'.icil':1 o!'nti:5ric urlh [r.tel unci g-:cS .{scc;'
[.:u'r- i l-,.:l pr(':"jr sui:;.1:e s Cr[ [ucl, EJses. ilnd lubrri.rlits Jre
.l r..l ,1.:l.lu .rt l.ruF,r'h ei',l:i.:r,C!"i1Cnl iJnd uCll:t'Ci'll Si()rJ'i3
.lfC.:S \lOnitcrrS .rnd c\ulu..:ttS inSlrum\:nts .rntJ 5.rirSeS
dur:r:u COurltdu\^n ()l\'lI.:trori: r\1 ClnrtOIS an,J ln:3rf\;c:S
nlet h.: nra.ll consclg 0.lhcl> to lo;;le :rn,J isol.:te f'r'..rllunc-
ttot> [)(l(:ri:tt'lcs scolr3 .rn:j complc rri.r ol' nl.tllL:fi,-'lt()ils
A21.i.S
AFSC 1117i
t
RESPON SIB ILITIES
by' consuttinE techni';el publicutions. rneih.l;ri.;l Cr.:
ings. or enginecring rnslructions. Eslrni.:13s :ine req,-i;
to fix mull'unctions i,lnd coordrn.rtcs u iti: ol!-.:r counl.i:.,'
OpcrJtionS. AScert:rinS prt,pcr oi::r;iir.;'. Of rn3;i-..:i.:.
consoles. Suncrvises Jnd Fcrforms renor;i. tesi. .:t'rtt ;a
lacement or mech.ro,.;l cofisolu- coii;f.:,,a;i:s P;;.'i;a
and supervises s:[ct1 procedures t(r bc.fclll(,r*ctj in I
hundlinE of lrguid o\) $.-'!1. ni:r:c :lcir!. hcilr;:'.: . ri:r:'c!:
and hi'droCJibon [uc!> uoJ-;r .sriia:'i:r.!1 i..oi. f :r!:-i-;.
c. Records attd sltft'rvtsei tl:e tnc:rttnc.'.'.r- oj r,:;-(i.'.
lntssile cotnpan(',tts. cttd surFutt ?ett:7tr:ct:t his:oi,:c; C-
Nl.rintuitts anJ sut',3t'\ ;s3-1 t!':c mJrn:3r.::n:'- t!' l'.:st(ri:.
recOrds peftuininS tO rt-l51rL'Ct!OnS. ftfe:ir. feniu.-3Ix3
lesis. und mul['uncttons of n:issll=s. rntsg'1.; i(rrr,i::r':.
and supnort eq'.;i;m3r,i. Reu.';is:(roi: z:':.! re.-c.:L-: c';i
ericS ;,:nC e.\f:nJrluIc ol g:j.-'i. l'uC::. ij:,L{ !';:'tri-flS
d .Sttpt'rl'r5c5 tt;:S.ltit n:i!til.t t:J 't.'(' laf t5 ,''i:t(' I':-:1. -
Schedulcs \A orl. J-\.(tj=-:lni: Lr:.:bl:sl.r'! \r (,ii.. r :: -.(
produciic:n coiilrtti:. ::r.J i,-'i ! c : L--,.:n(-: Si--.j-: jr [l i.: ..'
a\ Jillhiliil (rI sr.i'i"'.rII .. (1.:;-:-':i:: iin.: S;'.''r l-:'i: ! -;
viscs thc lc,:r.iiir!. c(,r-.li!..Jr:r.:. .:r.i ('ii-lr--..::.' .-! r:-..-
rr ith requtrec! sr l;-.4:'t gctr:;'x,..'il. .is:.i -: ['.;,:.::.-...:
and tc13;' [un.'litrts to sur):',7'; r.:13S. e-<:-::.-.,t1'- ;':..:
O[ u C,t i. tO bS :j.Cr-,np!rS i^.:C. ;lnd I'! r,i rC:'.. ]ul - l'. :::a.:
l'ollo\\ up to cnsure Q!.r:':ti:.r:ir c ci.i.i Qu;i,i.:l:r r.' i^.'.,,:
IlJrrr.-C fcSultS. [itaiu;la: Sul'..)iU:ri.,! l'j i1.']:'.':.:,:: l: i::'
of complru!'.ce' r^'ii n of,cr-:,lr-..:l l(':.iri:. n-::.: -.-.r -
cjrrcctir e:. tg'.'l:nic., I tnsiiLrr.'l:i'ri--. an;l St;L:. '-' (,''-',.:.
procedureS Coo --.'.. , '.the-Job Ii'.:in!nL' i-:oi]:r-.-i
A:tEchmenl 21 15 March 1985 EHectivo 30 April 1985.1
AIRMAN AIR FORCE SPECIALTY
MISSILE MAINTENANCE TECHNICIAN
I. SPECIALTY SUMMARY
Assenrbtc>. rcp.rirs. nuintuins. nro<Jifies. configurcs. inspects. and servic:s missilcs. missile subsl'stenrs. anC ri:rti
support equtpnlcnr: and supef iscs missilc nliunlenJnce rctivitics. Rc'lotcd DOD Ocaryorionol Sviirp1,,-.'1'-11
3. SPECIALIY OUALIFICATIOT{S
a. Ancx/edgr. Knoulcdg: of thc follouing is mardaton': oneration. and assentrlr ol ;'::-.srlc s\stc=: an( ti
propcnics and charac:cris:rcs of missilc oxidizcrs and fucls. supFort equiprn:nt is riltnd:tc'rr
basic hydraulics. pneudraulics. rne:hanics. and electricirr':
end principles of milsilc proSrulsion. Possession of
c. Tro intng
(l) .ComFIelion of Prcscribcd 7-lerc!
mandatorl' Lno,*lcCgc uill bc dctcrmined according to coursc is mandatory.
AFR ]5.I (?) Cg*pletion of an advanccd pir;'lr
__b_._frf!r!!rr. 9u-._][qrt,o_l_a: .a !v'tissil:_l.lrinl:l"ncc aoujsc is-desirablc-
Spccialrst tt ms ndator). In edd ition. cxperience in d. Other. A Sccret secunt)'clearance rl
p<rforming or rupcn'ising functrons ruch as inrpcction, tcst. as'ard and rctcntion of this AFSC.
f.r. J n j _:.1 rt l.a i
4-3
A2r 1.1C Effective 3o April 1985 AFR 39- 1(c7) Anrchmcns 21.1 1s trtarc
O 4. 'SPECIALTY SHREDOUTS
Punton o/ A FS to H'hil h Rclotr.,l
\\'s- I J3A' Nl. \\',S- t 338
BGM-109 Ground L:unchcd Crur:,
r ilc
LG M.25
SulIi t
A
c
D
a
4-4
ATTACHMET{T II .5
PREPAREDNESS AI\TD PREVETVNON PIAhI
L.
PREPAREDNESS AI{D PRE\IENTION PI-AI{
Maintenance and Ooeration
The purpose of this section is to describe the plan used by LBDF personnel in case of
emergency. The LBDF has been desigued and will be operated in a manner to prevent
accidents which might occur from the presence of hazardous wastes, and to minimize the
seriousness of any problems that should occur.
Reouired Equioment
The following equipment is available for the purpose(s) specified:
For purposes of internal communications and alarm systems for providing
immediate emergency instruction to facility employees, and for summoning
external emergency assistance from law enforcement agencies, fire departments, or
emergency response teams, the following equipment is available:
- Hand-held, Z-way radios with central dispatch are in the possession of each
team chief and the range safety officer. All vehicles also contain Z-way
radios.
- Telephones are available at the LBDF which tie into the base telephone
system.
- A manual fire alarm is located at the facility which is coded to the alarm at
the range fire department.
2. The Range Fire Department is within 5 minute response time to the facility and
has the following equipment:
- Structural pumper, self-contained, with 400 gallons of water, 500 gpm pump.
- 1,500 gallon water nurse truck.
- 400 gallon 'kater buffalou truck with pump.
- Ramp patrol vehicle with halon and dry chemicals for engine fires.
This equipment is inspected daily after each use, and receives maintenance on a
quarterly basis.
5-L
3.Safety Equipment. General safety equipment and safety procedures at the UTTR
Complex available for use and practices at the LBDF include:
- Protective equipment for all fire fighters (e.g.pants, boots, hood helmets,
gloves, coats, respirators, etc.)
- Ambulance (paramedic unit)
Safety Officer
A medical technician is on-site 5 days a week, 24 hours a day, and on
weekends the fire department provided emergency medical services.
All range personnel receive first-aid and CPR instruction annually.
A paramedic unit is stationed at the UT[R.
Safety equipment maintained at the facility specific to the possible hazards
include: deluge shower, eyewash, wash down and rinse water, pH meters, SO2
meters (stationary and portable), and a first-aid kit.
5. Decontamination equipment available includes soda ash to neutralize the acids
resulting from the deactivation process, and water truck to dilute and hydrolyze
the liquids.
*6. Discharge control equipment includes soda ash water trucks and heavy equipment,
including road graders, backhoes, and dump trucks.
7. The range water supply system seryes the facilities and can supply adequate water.
All of the required equipment is periodically tested and maintained to assume proper
working condition in case of emergency use.
Access to Communications
All personnel who serve at the LBDF have immediate access at all times by hand-held,
Z-way radios and those installed in the UTIR vehicles, as well as the telephone located
at the LBDF. The facility never operates without at least two persons on-site. All
emergency vehicles have immediate access to all parts of the facility.
4.
5-2
Arrangements for Emergency Assistance
The UTfR compound is essentially self-suffrcient in terms of law enforcement,
emergency services, and safety. The compound has its own security force and safety
ofEcer, and is serviced by Hill AFB Hospital, with which it maintains direct
communication. A helicopter is available at Hill AFB to transfer personnel to IIAFB
Hospital and to LDS Hospital in Salt kke City or Humana Hospital in Davis County.
The UTIR does have several emergency assistance agreements with other agencies. An
agreement exists with the Utatl State Highway Patrol to evacuate base personnel in case
of emergency. The Higbway Patrol personnel have been acquainted with the UTIR
layout and activities at the facility including the properties of hazardous waites handled
at the rang€ and their associated hazards, places at the facility where personnel would
normally be working, road access to the facility, emergency equipment and facilities at
the range, and evacuation routes. A mutual aid agreement exists between the UTIR
and the BLM for fire protection, and BLM personnel are also familiar with the Range
and its facilities. LDS Hospital in Salt Lake City maintains Ufe Flight capability to take
UTIR personnel to that hospital in an emergency situation. An agreement also exists
with Humana Hospital for airlifting of patients in case of accidents at the UTIR.
Personnel at these hospitals have also been familiarized with the properties of hazardous
wastes at the facilities and the potential injuries which could result from them.
ATTACHMEIIIT II - 6
CONNNGENCY PI"AhI
EMERGENCY RESPONSE PIA}I
General
In addition to this plan, the Ogden Air hgistics Center has developed otler contingency
plans for responses to disasters of all tlpes including: Air Force Regulation 93-2 ard
operating plans (HiIl AFB PI-AN 355-1). A Lithium Battery Emergency Response Tea:n
has also been formed to respond to an incident at any of the missile sites, including
6ansportation to and from an installation, and also to an incident at the UTTR.
Scooe
The timely and effective response to spills or niishaps involving hazardous materials is
mandatory in order to provide counter-measures which will eliminate or reduce the
possibility of exposure and contamination of people and resources. This section is aimed
at providing the procedures, instructions, and management structure to achieve this end.
Faciliw Emersencr/ Coordinator
The Emergency Coordinator or his alternate will be available at all times to coordinate
emergency response measures, and will have a copy of this contingency plan. The
primary Emergency Coordinator is in charge of all activities at the UTIR. As such he is
intimately familiar with the facilities and operations of the LBDF. and has the authority
to commit resources ils necessary to carry out this contingency plan. The Emergency
Coordinator will be responsible for insuring that the emergency procedures outlined in
Section 8.4.7 of the Utah Hazardous Waste Management Regulations (UHWMR) and 40
CFR 264.56 are followed. The Emergency Coordinator and his alternate are as
identified below.
Primarv Emersency Coordinator
Major Stephen Smith
2849 Support Squadron Commander/SU 171550 (777-L550 from off base) during
duty hours, or 71524 (Range Controller during off-duty hours).
Alternate Emergency Coordinator
Rick Bruce
UTTR Fire Department - 2849 SS (R)/SLJF /71555 (777-L555 from off base) or
71524 (Range Controller).
6-L
Emersens/ Eouioment
The following emergency equipment is available at the LBDF and at the UTTR. This
equipment is stored at the facility or held in readiness at a remote location within 5
minutes response distance from the LBDF.
L. Portable fire extinguishers at the facility and individual backpack style fire
extinguishers on vehicles (as remote location).
2. Fire fighting equipment from UTIR fire department (remote location).
a. Structural pumper - 400 gallon storage capacity, 500 gpm pump
b. 1500 galton water distributor (nurse truck)
c. 400 gallon "Water Buffalo" (truck w/pump)
d. Rarnp patrol vehicle - halon & d.y chemicals
e. Brush truck - 280 gallon capacity w/small pump
3. Self contained positive pressure respirators (6) w/(tZ) tanks each at 30 minute
continuous supply (stored at fire department).
4. Protective equipment: suits for each fire fighter including hood helmets (stored at
fire department).
5. Hand tools (shovels, picks, etc.) at remote location.
6. First aid equipment at facility and remote location.
7. Heary equipment at UTTR (remote location).
a. Front end loaders
b. Backhoes
c. Graders
d. Dump trucks
8. Two-way radio communication system (hand held and in vehicles).
9. AmbulancefParamedic unit (remote location).
6-2
LL.
L0.
L2.
13.
L4.
Soda ash for neutralization battery fluid (at facility).
Water for flushing and rinse (at facility).
Deluge showers and eyewash showers (at facility).
Manual fire alarm (at facility).
pH meter (at facility).
L5. SOZ meters (at facility).
Arrangements for Outside Emergency Services
The UTTR complex has its own security police force. However, an assistance agreement
has been entered into with the Utah Highway Patrol to provide on-base assistance to
UTIR security personnel, if required. The UTTR fire department has a fire fighting
agreement with the Bureau of I-and Management (BLM). This agreement allows for
mutual aid betrveen the UTIR fire department and BLM fire fighting personnel. A
medical technician is on site at the UTIR Security Building 5 days a week 24 hours a
day along with a paramedic team. Instant communication can be established with
doctors at Hill AFB Hospital. Emergency ambulance services can be provided by Air
Force helicopters from Hill AFB or Life Flight from LDS Hospital in Salt I-ake City.
Response Procedures
The LBDF includes a storagefdischarge building where serviceable batteries are stored
before deactivatior\ and a deactivation facility where used batteries are neutralized
before disposal. During the deactivation and neutralization process of the batteries,
access to the area is controlled and the entire operation closely monitored. The
batteries arc hazardous due to lithium in the batteries which is reactive (D003) and the
sulfurous acid and hydrochloric acid electro$te which is corrosive (D002).
In the event of a spill or exposure to personnel during battery discharge or during
deactivation of the batteries, the Emergency Coordinator will be notified immediately.
The first action of the Emergency Coordinator would be to assess the extent of the spill
or exposure and to insure first aid is provided to exposed personnel. The next step
would be to notiff personnel at the UTIR complex of the emergency and dispatch the
paramedic unit and needed equipment to the site. Any spill of hazardous materials in
the I-BDF would be confined by using earthwork equipment to build berms or dig
trenches. A spill in the storage/discharge building would be confined to the
storage/discharge building. Soda ash present at either site would be used to neutralize
any spill materials. If personnel were exposed, immediate showers would be applied and
6-3
consultations with Hill AFB doctors and an on-site evaluation by emergency medical
personnel would establish if emergency ambulance procedures would be required. If so,
the exposed personnel would be transported via helicopter to Hill AFB Hospital or LDS
Hospital in Salt I-ake City. After any exposed or injured personnel were under care, the
Emergency Coordinator would transfer neutralized spill material to the evaporation pond
and begin clean-up procedures.
An explosive disposal method has been developed and tested in case a battery cannot be
deactivated following the established procedures. It is not anticipated that this method
will ever be used. However, if it is needed, an emergency permit would be requested
from the Utah Bureau of Solid and Hazardous Wastes and the explosives would be
placed as shown in Figure E1. The UTTR has an interim status munitions open burning
RCRA treatment facility and erperienced Explosive Ordnance Disposal personnel in the
2701E;OD Squadron would perform this task.
Evacuation Plan
It in the opinion of the emergency coordinator, an evacuation of the LBDF is required,
the Emergency Coordinator would notiff the UTfR complex by telephone or by two-way
radio and the evacuation would proceed. Personnel in the LBDF area would be notified
of the evacuation by voice signal and vehicle siren.
The evacuation has two possible routes. The main route would be over the main access
road to the site back to the southwest to the UTTR complex. If for some reason this
route was blocked, evacuation could proceed over land to the south to the UTIR
complex.
The LBDF is remote and the hazardous materials present are such that any emergency
would most likely not require evacuation of facilities outside the UTTR area.
6-4
.TEH (10) SATCHELS OF C4 EXPLOSIVES REEUIRED
. EACH CdNTTIHIHG ZO PoUHDS (TOTAL ZOO POUXDS
.
TCgHfIGURATIOH: 2 SATCHELS 0ll EACH SIDE, TOP
1 SATCHEL OH EACH END
T:H I}lU 11 )
3 B 0 TT0lr
r+-TYPICAL SAFETY FUSE
(BURHS AT SPECIFIC
COHFIGURATIOH
RATE )
Figure E1
Explosive Placement on Submodule
6-5
Post Emersencv Procedures
Immediately after the emergency condition is over, the Emergency Coordinator or his
alternate shall ensure that any material from the lithium batteries still considered
hazardous are placed in the facilities for treatment. All emergency equipment will be
cleaned and restored before operations are resumed. No additional treatment
operations will begin until all clean-up procedures have been completed and all
emergency facilities are restored to working order. The Emergency Coordinator shall
notrff the Utah Hazardous Waste Committee and other appropriate state, federal, and
local authorities, that the facility has been cleaned up and is ready to resume operation.
The Emergency Coordinator shall record in the operating record, the time, date, and
nature of any incident that requires implementing the contingency plan. Within L5 days
after the incident, he shall submit a written report on the emergency to the Utah
Hazardous Waste Management Committee and EPA The report shall include:
L. Name, address, and telephone number of the owner or operator.
2. Name, address, and telephone number of the facility.
3. Date, time, and type of incident (e.g. fire, discharge).
4. Name and quantity of material(s) involved.
5. The extent of injuries, if any.
6. An assessment of actual or potential hazards to the environment on human health,
where this is applicable.
7. Estimated quantity and disposition of recovered material that resulted from the
incident.
Maintenance of Contingency Plan
Copies of the contingency plan and all revisions to the plan will be maintained at the
UTIR and Hill AFB and by the Emergency Coordinator and his alternate. This
contingency plan will be reviewed on an annual basis and updated as required as
required'by 40 CFR 264.54 and UHWMR. The plan shall be submitted to all police and
fire departments, hospitals, and emergency response teams that may be called upon to
provide emergency services.
6-6
ATTACHMENT II .7
CLOSLIRE PLAI{
CLOSURE PI-AI.I
Lithium Batterv Facilities Ooeration
Batteries are stored in the designated storage buildings. During the discharge phase of
the treatment, the batteries are remotely monitored for voltage readings. The batteries
are not stored longer than 90 days prior to deactivation. After complete discharge,
batteries are transported by truck to the nearby deactivation facility. The deactivation
facility has the capacity to deactivate four batteries at a time. There are two, double-
walled polyethylene tanks, where the batteries are placed, submerged in water, and the
battery casings pressured and burst. The battery casings are then flushed by continuously
pumping the water in the tails through the burst casings. The water is then transferred
to a third polyethylene tank where soda ash is added to neutralize the battery fluid and
tank liquids. The burst casings are flushed for approximately 48 hours.
Once the flushing is completed and the fluid is transferred to the neutraltzation tank, the
sludge in the tank is tested for pH, EP toxic, and total metals. The total metal analysis
will include all EP toxic metals and nickel and thallium. Should this sludge be found to
be hazardous it will be treated to be non-hazardous or disposed of as a hazardous waste.
If applicable, the hazardous waste will also be disposed of in a manner consistent with
RCRA Section 3004(d) land disposal restrictions.
The remaining aluminum battery sa5ings are landfilled. Residue from the deactivation
and neutralization tanks is disposed of in accordance with the Waste Analysis and
Research Plans. Sludge in the evaporation pond is loaded into barrels and hauled to
landfill.
Inventorv of Wastes
The initial contents of the batteries before discharge and deactivation is lithium and
thionyl chloride.
Deactivating 12 to 40 submodules per year will require 33,300 to 222,000 gallons of water
(depending upon single or multiple submodule deactivations) and will generate
corresponding volumes of effluent from the deactivation facility. After the battery
submodules have been burst, hydrolyzed and the water (liquid) neutralized, the
remaining water will be pumped into the evaporation pond. According to GTE, the
water and sediments removed from the deactivation of one submodule will contain the
following:
7-l
1. Uthium is present in the fluid distributed betrneen two salts approximately as:
UZSOE 78 lbs.LiHCO3 112 lbs.
2. Aluminum is distributed betrneen two salts approximately as:
Alz(SOg)r 52 lbs.AI(HCO3)3 74 lbs.
3. Nickel is present as Ni3S2 which forms in the acid media to the extent of 54 lbs.
None of the materials identified above are listed by EPA as hazardous waste. The
neutrdized water solution will have a pH of 6.0 to 7.5 Glightly acidic and is non-
hazardous).
The deactivated battery submodule casing will consist of:
1. Metallic aluminum in the submodule frame: 60lbs.
2. Metallic nickel in buss bars, hold downs, and terminals: 9 lbs.
3. Stainless steel case, covers, wires, etc: 65 lbs.
4. Tefzel rails and shims: 21 lbs.
5. Epoxy and carbon remain unchanged: 10 lbs. and 13.3 lbs. respectively.
These deactivated submodule casings will be disposed of as solid waste (non-hazardous).
With the material involved there should be no impact on water qudity from their
ultimate disposition.
The evaporation pond residue and liquid and the submodule casings will be landfilled
off-site. Therefore, no solid wastes will be stored on site.
Events kading to Closure
It is reasonable to assume that the lithium batteries udll be used by the Air Force for a
long time, and as such that the LBDF will remain in operation indefinitely, unless the
Air Force discontinues the use of the batteries, the UTIR is closed doum completely.
The anticipated closure procedure for LBDF is described in the following section.
7-2
Facility Closure
Once the operation on the LBDF oease, no hazardous wastes will remain on the site.
All remaining non-hazardous waste, the battery submodule designs, and the sludge in the
evaporation pond will be landfilled off-site. Clean water will be pumped through the
deactivation facility. The effluent water from this process will be analped. When no
hazardous wastes are detected the deactivation plant will be nashed down and cleaned
with soda ash solution and the last effluent water evaporated in the evaporation ponds.
The LBDF will require no closure activities other than a wash doum once all the lithium
batteries are removed. Since the only hazardous wastes at the site during operation were
immediately neutralized during the plant processes, no major slganing or
decontamination of the site will be required.
Once closure is completed, a certification must be submitted to the state veri$ing that
closure has been completed in accordance with the approved closure plan.
Decontamination of the Facility
No hazardous wastes will remain at the site once operation ceases. Decontamination of
the facility will be outlined under the facility closure plan.
Closure Schedule
No specific date for closure can be established. When closure is anticipated, at least 180
days before closure begins, this closure plan will be submitted to the Utah Solid and
Hazardous Waste Committee. The schedule for final closure is to be completed in detail
for this submission. Closure of the facility will be as described in this closure plan.
Closure is expected to take no more than2 weels, and will be completed within 90 days
of the last operation of the facility. Within 90 days after final closure, physical data
(location, dimensions, contents, etc.) will be submitted to the appropriate county
recorder as directed by Section 8.7.10 of the Utah Hazardous Waste Management
Regulations.
Post-Closure
Since no hazardous wastes will remain at the facility after closure, post-closure
requirements do not apply to the hazardous waste operations at the UTIR LBDF. As
Iong as the Air Force owns the property, access will be restricted. This restriction is
consistent with the overall mission of the UTIR. Sectrity Police would be routinely
monitoring the area whether or not the LBDF site had existed.
7-3
Closure Time Frame
Day 0 The State of Utah is notified of the intention to close the Uthium Battery
Facility.
Day 7 AIt Solid Wastes @attery casings) have been removed from the facility.
Day 2l All System Tanls and lines have been flushed and the flushing liquid has
been placed in the evaporation ponds.
Day 35 The plant has been washed down and scnrbbed with a Soda ash solution.
The cleaning solution has been placed in the waporation ponds.
Day 150 Evaporation complete. Sludge from the evaporation ponds has been placed
in a landfill.
Day 180 Certification of closure issued to the State of Utah.
Day 240 Site location data is provided to Box Elder County as required by 40 CFR
264.119.
Closure Performance Standard
The Closure Plan will be carried out to meet the requirements of 40 CFR 164.1L1,
264.114, and 264.197.
74
MODULE III - STORAGE IN COT{TAINERS
Not Applicable
MODULE fV - STORAGEA}ID WENT IN TAhIIG
.T{ODULE TV - TREATT,TETflT A}ID STORAGE TN TE}IKS
IV.A.
IV. B.
rv. B. ]. .
IV. C.
rv. D.
rv.D.1.
IV .D.2
IV. D.3.
IV. E.
IV.E.1.
IV.E.
APPLICABTLTTY
The requirements of this pernit Module pertainto the storage and treatment of hazardous wastein the tank systeus.
WASTE IDENTIFICATION
The Perrrj.ttee uay treat and store the foJ.lowing
wastes in tanks at the facility, subject to the
terms of this permit:
RCRA Wasteg
D002 and Do03
TANK SYSTEM DESIGN AND CONSTRUCTION
RESERVED
GENERAL OPERATTNG CONDTTTONS
Subject to the teras of this per:nit, the
Permittee shall treat only the hazardous wastes
as specified in peruit Condition IV.B.1.
The Permittee shall
treabment reagents,tank systems if theyancillary equipmentor otherwise fail.
not place hazardous wast€s,
or other materials in the
could cause the tank or its
to rupture, leak I corrod€,
The Permittee shall prevent spil1s and overflows
from the tank or containment system.
RESPONSE TO LEAKS OR SPTLLS
In the event of a leak or a spill from a tank
system, or a secondary containment system, or if
a system becomes unfit for contj.nued use, the
Permittee shall remove the system from serrrice
irnrnediately and complete the following actions:
Stop the flow of
and inspect thethe release.
Remove all hraste
f our (24 ) hours
hazardous hlaste into the system
system to deternine the cause of
from the system within twentY-
of the detection of the leak to
IV.E.
Module fV - page L
rv.E.2.
IV.8.2.a.
rv. E. 2.b.
fV.E.2.c.
IV.E.3
IV. F.
IV. F. l- .
prevent further rel.ease and alLow inspection andrepair of the system. If the Pemittee findsthat it will be-inpossible to meet this tideperiod, the Permittee shall verbally notify the
Executive Secretary and demonstrate that the
longer tine period is required.
The Petmittee shall close any tank system thatis unfit for contLnued use or any tank systemthat is leaking in accordance with the Closure
Plan specified in Attachnent II-7 unless thefollowing actions are taken:
For a release caused by a spill that has not
danaged the integrity of the system, the
Petmittee shall remove the released waste and
make any necessary repairs to ful1y restore theintegrity of the system before returning the
tank system to senrice;
For a release caused by a leak from the primary
tank system to the secondary containment system,
the Petmittee shall repair the prinary systemprior to returning it to se;rrice; and
If the Perraittee replaces a component of a tank
system to eliminate a leak, that component mustsatisfy the requirements for new tank systems or
components in R450-8-10. (40 CFR Sections
264.192 and 264.193 incorporated by reference).
For all major repairs to elirninate leaks or
restore the integrity of the tank system, the
Pennittee shall obtain a certification by an
independent, gualified, Utah registered,professional engineer that the repaired systemis capable of handling hazardous wastes without
release for the intended life of the system
before returning the system to serrrice.
Examples of najor repairs are: repair of a
ruptured tank or repair or replacement of a
secondary containment vau1t.
INSPECTTON SCHEDULES AND PROCEDURES
The Perurittee shall inspect the tank systems in
accordance with the fnspection Schedulespecified in Attachrnent II-3.
The Permittee shall conduct an assessment of the
deactivation and neutralization tank systemsintegrity on an annual basis. The assessment
IV.F.2.
Modu1e IV - page 2
which is reviewed and certified by an
independent, qualified, registered professional
engineer, Dust be kept on file at the UTTRfacility. The assessnent nust be conductedprior to the first operation of the units each
calendar year. If as a result of the
assessuent, a tank systeu conponent is found to
be leaking or unflt for use, the Pemittee mustueet the requireroents of R450-8-10.
rV. G . RECORDKEEPING AIIID REPORTTNG
IV.G.1. The Peruittee shall verbally notlfy the
Executive Secretary rithin twenty-four (24)
hours of detection, when a leak or spill occurs
from the tank system or secondar? containnent
system to the environment.
fV.G.2. Releases from a tanl< system that are containedwithin a secondary containment system need not
be reported as required in IV.G.I. However,said release shall be recorded in the Operating
Record.
rv-G.3- In addition to cornplying with Condition rV.G.1.,within thirty (30) days of detecting a releaseto the environnent from the tank system or
secondary containment system, the Perrnitteeshall subrnit the following information to the
Executive Secretary:
Iv.G.3.a. Like1y route of migration of the release;
fv.G.3.b. Characteristics of surrounding soil (includingsoil composition, geology, hydrology, and
climate) ;
Iv.G.3.c. Results of any rnonitoring or sampling conductedin connection with the release. If the
Perrnittee finds it will be iupossible to rneetthis tirne period, the Permittee shall subrnit to
the Executive Secretary a schedule of when theresults will be available. This schedule shal1
be suburitted before th.e required thirty (30)
days subnittal period expires;
IV.G.3.d. Proxinity of downgradient drinking uater,
surface water, and populated areasi and
Iv.G.3.e. Description of response actions taken or
planned.
Modu1e IV - page 3
rv.G.4.
IV.G.5.
rv.G.6.
rV. H.
rv. H. ]_ .
The Pemittee shall naintain at the Facility a
record of the results of annual tank assessmenttests condueted in accordance with Condition
IV.F.2.
The Petmittee shall docuoent and record theresults of the waste analysis of each spill and
any subsequent treatnent reguired by the Waste
Analysis Plan, Attachroent II-1, in the Operating
Record.
The Petmittee shall subnit to the Executive
Secretary all certif,ications of najor leakswithin seven (7) days from returning the tank
systems to serlrice.
TANK CIPSURE
The Petrrittee shall close the Tank Systems in
accordance with the approved Closure Plan,
Attachurent II-7.
Module fV - page 4
ATTACHMENT fV. 1(A)
RESEARCH PIAI{ & DESCRIPilON
SECTIONl - RESEARCHDESCRIPTION
In order to extend their survival under standby power, the Minuteman Mssile sites on a
scheduled basis will exchange existing lithium thionyl chloride batteries for new ones. As
part of this scheduled exchange, the batteries are treated to be non-hazardous utilizing
existing facilities at UTfR. The treatment involves discharge and deactivation of ttre
batteries.
The batteries are discharged to 7.0 or 0.7 volts (depending upon manufacturer) in a
designated area of the battery storage building. Following their discharge, the batteries
are transported to the Deactivation Facility where the battery cell fillports are opened
and hydraulic lines are connected. The lithium batteries are then placed inside a water-
filled, double walled polyethylene, in ground tank. Using nitrogen and pressurized water,
each of the three cells in a battery submodule is hydrostatically burst so that an opening
is created at the bottom of the battery.
Water is then circulated through the cells. This process hydrolpes the thionyl chloride
and forms sulfurous acid and hydrochloric acid. Several cycles of water are circulated
through the battery. Between each cycle, the water is pumped to a neutralization tank
(center tank) where sodium carbonate is added and the water is mixed until a pH of 6 to
7.5 is measured.
The neutralized water and salt solution is pumped out of the neutralization tank to the
evaporation pond. The evaporation pond is not considered a hazardous waste
management facility because the equilibrium constant for the lithium and acids
neutralization reactions $eatly favor tle neutral products. The liquid and solid matter
in the treatment tanls is non-hazardous after the neutralization process. These
substances will be analyzed to insure they are indeed non-hazardous (see the Waste
Analysis Plan), prior to discharge to the evaporation pond. The salts in the evaporation
pond and sludges in the polyethylene tanls will be recycled if economical, or disposed of
at a solid waste landfill. The remaining aluminum battery casings will be disposed of in
a solid waste in a landfill. Disposal at the UTIR landfill will not occur until permission
for such disposal has been approved by the Bureau.
Deactivation and disposal techniques for the batteries were developed parallel to the
development of the lithium battery by GTE s Wyle I-aboratories, Norco, California. The
chemical steps required in the deactivation and disposal are as follows:
Step 1:
Full discharge to 7.0 or 0.7 volts to remove as much lithium as possible - the chemical
reaction for this electrical discharge is:
1-1
4U + 2SOCI2 = 4UCl + SOZ + S
(Uthium) (Thionyl Chloride) (Lithium Chloride) (Sultur Dioxide) (Sultur)
Step 2:
Hydrolysis of remaining electrolyte - the chemical reaction for this hydrolpis is:
SOCI2 +H2O = SOZ + 2HCl
(Thionyl Chloride) Water (Lithium Ctloride) (Hydrochloric Acid)
and:
SOZ +HZO = HZSOg
(Sultur Dioxide) (Water) (Sulturous Acid)
Step 3:
Neutralization of resulting solution - the chemical reaction for this neutralization is:
H2SO3 + Na2CO3 = HZO+ 2Na2SO3 + COZ
(Sulturous Acid) (Sodium Carbonate) (Water) (Sodium Sulfite) (Carbon Dioxide)
and:
2HCl + Na2CO3 = H2O+ 2NaCl + COZ
(Hydrochloric Acid)(Sodium Carbonate) (Water)(Sodium Chloride) (Carbon Dioxide)
If the submodules should vent through the internal venting system described in
Attachment G, the thionyl chloride (SOCI2) will hydrolyre io the presence of any
moisture to SO2 and HCl, which would be neutralized by the internal scrubber. When
the cell fillports on the submodules are first opened after electrical discharge, small
quantities of gas can escape. However, it is estimated that the total space available for
gas to accumulate is about five liters per submodule; therefore, volumes of emissions
from this source will be extremely small. The gas will be mostly hydrogen (50 to 60
percent) but will also include small quantities of nitrogen, sulfur dioxide, argon, and
helium.
L-2
AITACHMEhTT fV. 1(B)
RESEARCH PI"AN
DEACTWATION PROCESS DESCRIPilON
LITHIUM BATTERY SPECFICATIONS
The submodule is the basic deliverable battery section of the lithium module (Figure G-
1). It consists of three cells housed in an aluminum weldment. The submodule case is
0.187 inches thick and is made from 5083 aluminum sheet stock. The packaging of the
cells in the submodule housing constitutes a pressure vessel. The cells are centered in
the housing and then completely potted in place by the use of a slmtactic epory foam.
This forms a composite stnrcture that is able to withstand internal pressures without
exceeding the material yield stren,gth of either the cell case or the submodule housing.
This composite constnrction also allows the stainless steel case and the aluminum
housing to work together in resisting shock and vibration The epoxy foam electrically
insulates the cell case from the submodule case as well as providing structural support.
Additional electrical isolation is obtained from plastic buttons that are pressed into the
sides and bottom of the submodule, and the combination of the foam and plastic buttons
eliminates differential motion between cell cases. Hazardous wastes associated with
these batteries are lithium (D003) and sulfurous and hydrochloric acids (D002).
Each cell is equipped with a pressure relief valve that will permit the cell to vent if a
malfunction or external heating causes the pressure to increase above 30 to 33 psig
(Figure G-2). If venting occurs, these emissions are to be routed through Teflon tubing
into a chemical scnrbber on the end of the submodule which neutralizes the emissions.
The scrubber is an unpainted stainless steel box which houses soda lime in a liquid
trap/distribution manifold that is made of nylon. The manifold, in turn, houses three
packets of sodium carbonate (soda ash) to neutralize any electrolyte that is ejected. The
elemental lithium in the battery is hazardous. Once the lithium is converted to an
inorganic salt it is non-hazardous. This occurs as the battery is discharged. The acids
are corrosive and are neutralized with soda ash in the deactivation process to render
them non-hazardous.
G-1,
a\q
ri
I
]Dcro.cn?rfiS n Lncl'.ur '
Figure G-l MESP Ortline Drawings of Submodule Assembly
!7.5o
G-2
PRESSURE
RELIEF.
VALVE
INLET TUBE
(TEFL0N )
COVER
T9
))
,'r7"./
FILLED TO
TOP I,JI TH
SODA LIME
PAC KETS O F
SOD I UM
CARBONATE
LIQUID TRAP/
MAN I FOL D
(ruvLoN)
VENT INDICATOR
MOUNTED HERE
Figure G-2 Scrubber Assembly Detail
//'
G-3
ATTACHMENT H
SECTION 1 - DEACIWATION AI{D I{EIJTRALIZATION TAI\K SPECIFICATIONS
SECTION 2 . FACILITY DESIGN SPECIFICATIONS
SECTION 3. FACILITY I,OCATION INFOR]\{ATION
SECTION 1 . DEACTTVATION A}.ID NEUTRALIZATION TAT.IK SPECIFICATIONS
The Lithium Battery Deactivation Facility is a concrete pad, with three subsurface one
inch thick polyethylene tanla (Figure H-1). Secondary containment is provided by a
second polyethylene tank and each tank rystem includes leak detection. Pad
containment is provided by a six inch reinforced concrete wall which surrounds the pad.
An overhead monorail crane provides a means of lifting submodules off tnrck beds and
lowering them into the water-frlled tanls. The mechanical elements of the facility are
utilities providing water, compressed nitrogen storage tanl6, and recirculation pumps to
circulate water througb the submodules.
Figure H-2 is a sectional diagram of the facility and shows the containment taoks, pump
houses, overhead crane, and concrete pad.
The tar* construction specifications shdl be in accordance with Figure H-3 for the
primary containment tank and Figure H-4 for the secondary containment tank.
H-L
SECTION 2 - FACILITY DESIGN SPECIFICATIONS
The discharge of the lithium batteries is considered to be a form of treatment and is an
integral part of the RD&D operation. Therefore, the storage building which includes the
battery discharge area is part of this RD&D treatment facility. Discharged batteries will
not be stored over 90 days so a storage permit is not required. The submodules are
discharged to a voltage of 7.0 volts or 0.7 volts depending upon battery manufacturer.
The design of the discharge building is shown in Figure H-5 (attachment).
The Facility Design Specifications discuss volume markers in the evaporation ponds and
a berm and collection system around the deactivation area. The pond markers are
necessary to assure that adequate capacity exists in the pond prior to additional liquid
introduction and the existence of adequate freeboard to prevent overtopping by wind or
precipitation. The berm and collection system's purpose is to contain and collect any
spilIs, leaks, splashes, etc. that may occur during operation and prevent runoff onto the
surrounding soil.
A.EVAPORATION PONDS
The Uthium Battery Disposal Facility has two evaporation ponds. The small pond has a
volume capacity of 7800 gallons and the large pond has a volume capacity of 255,000
gallons. Permanent volume indicators shall be marked in each evaporation pond that
indicates the pond level that can safely contain the liquids generated from an additional
battery disposal. Additionally, a marker shall be placed 18 inches (I-UZ feet) from the
top of the pond to show when the pond contains the maximum allowable capacity. Each
pond is constructed with double liners and each have inspection areas that show when
the primary liner has been compromised. Figures H-6 and }I-7 (attachments) shows the
construction of the evaporation ponds.
B. CONCRETE PAD AREA
The concrete pad which houses the pumphouses, recycle pipes, and deactivation and
neutralization tanks is bermed with a 6 inch reinforced concrete wall. The berm was
designed to meet the following performance standards:
The berm must be designed and constructed to prevent runoff from spills,
drips, splashes, breaks in pipes or hoses, valve lea}s, etc. The berm must be
high enough to contain one tank volume.
H-2
The concrete pad and berrr must be lined or coated with a material that is
compatible with the characteristic waste and chemicals used in treatment
and will prevent absorption or degradation of tle conctete.
The concrete pad and berm must be free of crack.
C. COLLECTION SYSTEM
A collection system has been designed and construced to collect liquid that may
acctrmulate in the bermed area of the concrete pad. Precipitation tlat is colleoed must
be pumped to the evaporation ponds. Water collected from leals, spills, breals, etc.,
must be neutralized to a pH benreen 6 and 7.5 prior to pumping to the evaporation
ponds.
H-3
SECTION 3 - FACILIY I,OCAIIQIN INFORI\{ATION
The Utah Test and Training Renge (UTIR), EPA ID #IJT570[Pr0001, is located
approximately 55 mils5 west of Salt lake City, Utah and north of Interstate 80 (Figures
H-8 and H-9). The facility is onmed and operated by the United States Air Force. It is
used as a practice bombing and gunnery range for pilots and is used for storage of
necessary Air Force materials.
TRAFFIC PATTERNS AT UTIR
Except for the county road (Box Elder County) that runs from north to south on the east
side of the UTfR, traffic on all roads in controlled areas must be authorized. Traffic at
the site is extremely light, even on the county road, and it is difficult to envision a
situation when traffic movement will hinder the operation of either facility or emergency
vehicles if they are required.
FLOOD PI-AIN INFORIT{ATION
FIA flood plain maps for the LBDF are not available. Although these maps are not
available, it is believed that these facilities are not within the l0Gyear flood plain. The
Great Salt Lake is the nearest body of water, approximately 3 miles from the MBP site,
and about 8 miles from the range complex. The highest water level of the lake during
recorded history is 4217 msl. This will not threaten the LBDF which is at elevation 4400
msl.
Although it is unlikely that either a 24-hour or aZ1-year storm event would adversely
effect the LBDF, this faciliry has been designed so that very little damage would occur
due to unexpected flash flooding. The LBDF facility is constructed with foundation walls
which extend above ground. All mechanical equipment is above ground and the finish
grade slopes away from all the facility to insure good drainage.
H-4
CLIMATE
The climate in the area is considered to be arid. The winters are moderate to severely
cold, and the surnmers are hot and dry. The diurnal range of temperature is great.
During the summer, temperatures from 80 to 105"F are common. During the winter the
temperature varies from about -?5" to +55"F. The precipitation in the area is meager,
about 5 inches or less per year. Precipitation is chiefly from rain and snow during
December, January and February. Very little rain falts in the summer with some rain
during the spring and fall. Precipitation is will vary geatly from year to year. The
relative humidity is about 50 percent, and is lower during the summer than in the winter.
The average wind speed during tle summer is 5 to 10 milg5 per hour. In the spring and
fall, winds up to 50 miles per hour have been recorded. The prevailing winds duriug the
summer are generally from southwest to northeast, and during the winter they are mostly
from north to south.
H-5
I
NlTO EVAPORAT ION
POND
Figure H-t
Lithium Battery Disposal Facitity
Supplemental Deactivation Process Flow
TANK 2 TAHK 3
H-6
:{
I
or
r
;
r
r
Ii
.B
('
t
-,
l
\
\
ic{\
1t
l.t,oa
Eri
{ro\
S*E0n
O)-
'ElU(
UP
r-
I
T8
a-
'-
r
$*
oo
r.
!
II
t
r{
o<
</
t
U
il
btr
UT
,
'*
l
b
JI
ilrlul
i3Jd
-tL\-
r3r
J3o2oT
-!
9
hUa
.
)
-
o
I:
'
l
t
il
I
gl
t
*
i
$
\'
_
I
I
v
B
\i
t
i
r
#
h
d
__
l
__
Itg
)-sia"i
l\ol
\J?L
O.
Ol
,,
u
.0
L]
/
T
o
-t
3{
t
tF
a
er
t
$
i
tl
>\
+r
r
.t
s
Ff
.E
()cg
fJ
.
-
-
qE
'*
,
cg
q
Eh
o
IE
.?
.
9
o
oo
.$
u.
E
=
=E
rE
E
Ftr-).-FF+)
.l
-J
TT.
Pf
r
3(
lr
f
-f
!-
r
8T
n
O-
L.
,l
a
(I
t
(
t
(-
dt,
-
.r
*
,
JIUorl
qJrt
L)5r1'
trUve2r'
i($
t
o!i{t\Jll
)-
S
tt
7
r-
o
-
r
S
l
o
,t
s
'
t
2
t
i
t
l
Jf
r
u
H-
'
l
Figure H-3
H-8
!,C'
t
e.
(F
T
t-
tt
-
!
r
u
c
ry
t
r
.
g
80
,
Li
,
-'
6
.c
U'
;
:
R
T
TL
,
;
Ec
l
.
c.
F
-.
>
f
:r
\
f-
t?
8f
0
-E
:
tf
i
TL
L
'
-n
\)
c.
c
,
c
'o
3s
LL
.xuIl.
)
u7=OogF(r
)J0.J{ll'g
t.Jon.a
-
JJ
J]
-==
NJ
=-
rE
{
N
o]
r
J
z,
sz
==
lr
J
O
cr
F
==
o
Lr
J
-
CO
NJ
OU
-
FL
L
o
>zZ,
F
FC
J
oC)€Fl
A1?1
tscgF+.
,
?1Ftq)
t+
t
r
r'
l
E
*(
'E
EE
=o
.3
0
u
Er
'
cl
g
lF
l
L,
t1Ho(Jq)
V)
lr
t
C5=Ju-
al
-
LJ
.
l
<
az
,
r-
r
d
3
tr
lF-)
-1
,$
t-
t
(/
,=oJJ(5
,+
-
Lr
-
-
C)
N
N
I
OO
(
n
-
oD
t\
t(
f
o)
aa
aa
a
F
uJ
=
..
_=
(-
)
tr
,
>Z
F
(J
O
ar
.
,
J
ToO--r\
;.
.l
C\
J
-or
oc)
t\NJ
H-
g
-JIr-. L7r-.Or 3t l*,c, rc\.ar-g-r,
5o.tv ISBO( Qc,-.42 a3tg-t33 $o-ffi..'i;;E;3'i:a?,ti:3.:7io
l,rr,,; cirtt 4i 4,5 r-zg- g : c 4t trt 4.gej92^-? Et4= (- fl .yCt- EC14ry. j&lgtralr.l a{c+l, -e 54C..ecsa&+tl)-\\
:[;;
'E ria<, c-uO:z
I r--t:1rF-)l 3-9?tZ
Lt.t: tr,ts C @q,g,S
41'C-g-3 l' 2?',3
tide--=e :z
?, /:
Orz
f
'er, gt*,draag
:
II
I
i
I
a
I
dte.tl:z
tiztc-sot?
!'a- 2 ),3
qe'O'Zt 12
lzoc,-2,)tO
iL-zq i2 acc
I O t2, L?-1
Rgc,ortrtge? TrdseFtt?uR3s FrotlCt,lCU:? ,, F?oR?g7 1
llz'c- tarZ
E;,:JTDJC
F,qraTtilGn-EftT
D.l R@|silr rrrr! g
S7o&rGt Eax
11grulfi ell7E4
,Erc-zrr2rAgo f E
l?'c- 2'lz
lfzl.'=
I -l.€Ca.teg37 7q!38! Ft/? e?s) sPot
i")of;'. \
-g,e--
,r\/
a.,\'.
I
ls2'c-2e 12
Eb,-2?:Z
.9?,)3,*35
l.O-beQlZrtO
lS7?^re ?*E=TF,ICA-EdJtftr=^ff To U REDEa
\2,8,
\\-Q x y- ?s;a' b{rAg, Lo w =<wrrH a@? Gfr? c"r4
(ztc-+o lz
liltc'2"r2
P€*JfiE CCIiTIA.g*t?Cd, P€9 -l
1L-1t J 614,-2,1,c,c.p
UO.t'r?tG PA^;E:..
,Eg:2olU !o rr;gr? ,lo-. 91, , a q
ltc
?e
lCc-* tz
(z'c- z'iz /,
y':;
/'
l,il
.t
!,stf!,;tl,RCS-Z
-\\
- FliZ,g/.- 1,9.5
SUILDING b22O
Figrue H-5
Electrical Discharge Building
i- . X
-$2'c'2't2,
asc t?tz
iA 1\ N--- CCttf',',,- , HaNfTosin Ljl. -ffrto..,fn
r=" n'Y=nz
{ei*'r,s s=cueriv fi*a!6aa frrg:- (-5l;E;l:7 e-\
1.c- S . t1 ,' O. tZ t 4 5:tns2!,
?.2"12 a== l'tizrl!-lo r
CTSEJT f- tE e,.CJ|T t=2,%cc=
I
lR'&,IVt+tozo
H-I.O
,r*3i ?r
!.3 na. Trlr*LtHq, (*E speca
.t' _rt_ _li rsi arrEAa,3fr-
l+ Q, to',
tt'rr*rtc
,o-ao
E'EL C^ID
'O PI"H??n. *,etGutr..cc
tz'lpu^ac
rac L^Y.a2et,{^l- \
o+tnO
S ErcA,OS C ot a'.A'
,t.i O PtsC rlrrga.d?z,rLs9,fi3 3.1
F3 22p9frf,,4=
PLAA/---2'. lt €o
3
er3r,roac.e'll-oo
l-.)e
3&,rtE,lN3-
1'C
C,,fi67aJ5
AFII,|,
f )t FL-^Ca
.DETA,'L /Nl- t ,\o' El
ttl'oo atryLitL,i-*i*ffi8
a t
-ae
.i of
alYri,
!'^r-cLort ert{rrcrY-E r.t? ,---aul j rytgE1-AL17
s€c7/oN /6-\
Figure H-6
Small Evaporation Pond
H-Ll.
U-41
t'Qrve
'"?'FC;
NOTESz--r-D
t lra, LE,tE,.i?torlt l,\rJo t g.*tcna. t}CErrLg;gl tX art5rlrecaJttaHa ?r{ ,tlr,s J^.rO tE O, t>tafD,trLatl F?Sra lAll..hril, X ), ^CCOIiyr^/C:CUtt tG }wEigasrlb ac@t-t4ra^lro4j 4uO?rt frcna, qtng ffi ta
'..Sira/E^lTC*Zru3Tr(,tl }lAArAc,a1.
a.al;r,,tfi*lgi ,n ,LL X Cr ar,rQ$, A.VxrL ?fFg- nt$onr.L )t9 U, CrElrneruA8 g7 c.agri,rl?u*cE ?tcL,o rynarts,
FCAT gtatxcass
ETCUL r^3 C*tl
lrta4lAygTltL A^rcr€t
Lrr{
,c*,rt3 Satp
s,ECzc,N €\
9'. li-o' E/
,'pvc tl-c >tl
7s129;gCD '
PLUs
sEcTtoN 6\
l' t l"oo E/I
,oa.3 tr6rC GC'g !rPr*jx
Figure H-6 (Cont'd)
Sma1l Evaporation Pond
& tEtc et,
DETA, IL A\
H.T2
IIII 1
I
EVAPORATION POND PLANrca!. T';E
arlca
9 ?tAro Qt.Qtfl.tl
o20Jrloli4n/,ttala
1,
-5eel
tlEn 6717-)c7 to.E*7ofu,.tb
Figure H-7
Large Evaporation Pond
sEcrroN
@
'fup7lprccwr
Sruoc grw, a*nwtu ogaFAntGrx 70 .j5, crsts
H-13
,It/-r.f l?mr,aritqB 3rr 0
LEAK. DETECTION TRAP
Figure H.7 (Cont'd)
Large Evaporation Pond
TYPICAL PIPE PENETRATION
Cctt,erGla
j.il*r.r,
&,irrtIEl
DOUBLE LINER AND LEAK DETECTION SYSTEM
H-14
UTAH TEST AI
I#ll,jNGRA^H=t
WENDOVER I- -
6\/
SCALE t" - lO ttttES
C EDAR
CITY
-
LOGAN
OGOEN
SALT LAKE CITY
+
I
I
I\
PROVO
Figure H-8
Closure PLanIRCRA-Part B
VicinitY MaP
H-15
aIel lles
oF
.J
...
o ,ffi
Fz-Jo
C)
l-z
Joo
rlJJ
UJool-
ffiF,o\ dl
Figure H-9
Closure Plan/RCRA-Part B
UTIR Site Topography
H-16
8 Novenber 1991
I. DISCHARGE OF BATTERY P01{ER SUPPLIES. Dlseharge battery power supplles
which have been categoxLzed as category II or have been depleted through
normal use as follows:
a. Request Securlty Alarm Systeu Swltch to nA' (OfF) posltlon.
b. Enter Mechanical Roon and verify UAIN POIJER clrcult breakers (1
through L6, 24, 25, 27 through 33) are ln ON posltlon.
T|ARNING
Sulfur dioxide (SOz) concentration of 2 ppn or
greater presents a hazardous condition.
The envi,ronment of any confined area contalnlng
battery power supplies shall be sanpled for
sulfur dioxide (S0z) prior to entry. Fallure to
comply could result ln injury or death to
personnel .
c. Refer to manufacturer's lnstructlons for checkout and operation of
the Neotox SO2 detector.
d. UnLock outer door to Bay #2 and, uslng SOz detector, sample for
presence of SO2 as entry ls made to the Discharge Room Control and
Voltage Monitor Station (DRC\ruS).
e. If SOz ls detected, secure the area. Notify the Energency Response
Team (OO-ALC/IMET) to lnvestlgate and essess the source of the
problen.
f. At DRCWS (Figure 1), ser ROo!.t LIGHTS swltch (1, Figure 1) to ON
posltion. Llghts will cone on and ventllatlon fan will start.
g. Turn ON or verlfy that System Power Switch (5, Figure 1) ls ln the
ON (switch ilh.rnlnates) posltlon.
h. Depress LED test switch (2, Flgure 1) and verify all SUBMODIIIJ
ITOADED lights (3, Figure 1) llluninare.
1. If all SUBM0DITLE LOADED Lights illurnlnate, proceed to 6tep k.
J. If any llght falls to llltrnlnate, AUTOMATIC CUTOFF clrcult
nalfunction has occurred and shall be reported for correction prior
to proceeding.
CAUTION
Do not enter the Discharge Bay while batterles
are being discharged. ltre BATTERY DISCHARGE
EMERGENCY SHUTDOWN button shall always be
depressed prlor to Dlscharge Bay entry.
NOTE
If batteries are on dlscharge and only battery
monitoring ls required, proceed to step al.
k. If any batteries are being discharged, SUBI.iODULE IOADED ltght(s)
wiLL be llluninated. If access lnto the Dlscharge Bay ls required,
depress BATTERY DISCHARGE EMERGENCY SHUTDOIflII button (4, Flgure 1)
to trlp clrcuit breakers before entering.
1. Select or verlfy AUTOUATIC CUT0FF SWITCH (6, Figure 1) is in proper
set positlon (either GTE 0.7 Volt or Altus 7.0 Volts).
!^TTERY OISCH^R6E NOOll
ROL ANO IONITOR S?A?I
loor. L l6HTs
*-ll +o . ooo llrHr
-
m
A0roI^?rc gu?orF
tr trcx
ROOI{ LIGHTSAENTTI^A,TION SWTTCH
LED TEST SIfiTCH
SUBI{ODULE LOADED LIGHT
BATTERY DISCHARGE ET{ERGENCY SHUTDOIN BUTTON
AUTOMATIC SYSTEM POWER SWITCH
AUTOMATIC CUTOFF SELECTION SWITCH
VOLTT'IETER SELECTOR SWITCH
BATTERY VOLTAGE INDICATOR
OVERRIDE SWITCH
Figure 1
Dlscharge Roon Control and Voltage llonitoring Statlon (DRCWS)
NOTE
Gloudlng or smoking ln discharge roorn indlcates
a discharge circuit nalfunction and shall be
reported for repatrs.
m. Perfotm vlsual check for cloudlng or snoklng through wlndow of
dlscharge room door prlor to entry of dlscharge room.
n. Open door lnto battery porer supply dlscharge room.
o. Uslng SO2 detector, proceed through door and sanple lnterlor of
discharge room.
TTARNING
Do not subj ect battery porrer supplles to rough
handling in loading and transporting. Case
rupture or puncture or damage to scrubber or
battery power supply piping could release toxic
vapors and corrosive naterials hazardous to
personnel in the area.
Battery power supplies shaIl be placed in an
upright position to insure maximr:m discharge of
lithiun in battery power supply. Failure to
conply eould result ln lnjury or death to
personnel.
Battery power supplles from different
manufacturers eannot be dlseharged
slmultaneously. Battery manufacturer can be
determined by battery part nrrmber:
03 - 1340540 - 1 GTE manufactured
0875 - 0001 Altus manufactured
P.Transport crated battery porrer supplles to the dlseharge room and
posltlon one battery power supply, ln uprlght positlon, ln each
dlscharge statlon as narked on floor.
Remove battery power supply shlpptng contalner covers. Leave
battery power supplles on thelr shipplng contalner base.
NOTE
g.
Initiate Discharge and Deactlvation Log (flgure 2)
WARNTNG
A battery power supply has potential to draw
thousands of a,mperes current across a short.
Failure to use insulated hand tools could
result in equipment damage and injury or death
to personnel.
Stepsrthroughyshall
battery power supply at
be perforned on one
a time.
accomplish this procedure .Ensure tools are
remove termlnal cover fron battery powert.
Use insulated tools to
eompletely insulated.
Using insulated tools,
suPPly.
Inspect and, lf
cable pos ltive
required, use 80
(red) and negative
grit sandpaper, to clean load
(black) connectors .
PART I: DISCTIARGE
Date Received:
Discharge Bay Location:
Voltage Cut-Off Switch
Part No.Serlal No.
7.0V
lteasured
Voltage By
Locatlon:0. 7V
Date
Predischarge:
Discharge:Tlne:
Time:
Time:
Time:
Time:
Time
Tine
Time
Tirne
Time
Tine
Time:
Post Discharge:
Post Discharge (+t Hour) :
Diseharge ( If Required) :
Post Discharge (1 Hour-If Required):
OCV:
Load V:
Load V:
Load V:
Load V:
Load V:
Load V:
Load V:
Load V:
Load V:
Load V:
Load V:
Load V:
Load V:
OCV:
Load V:
OCV:
Signature:
Note: Upon Log completlon, send copy to OO-ALC/IUI'IRO
FIGIIRE 2. DISCHARGE A}.ID DEACTIVATION LOG
PART II: -DEACTIVATION
Battery
Voltage:
Part No.Battery Serlal No.
Burst Date:
Cell Burst Location:
-Cell 1: End:
-CelI 2: End:
-GelI 3: End:
Top:
Top:
Top:
Bottom:
Bottom:
Botton:
Side:
Slde:
Slde:
Quantity of Sodiurn Carbonate Added to Neutrallzation Tank
NeutralLzation Tank pH (following each
Start/Finish
pH Readins Tine /Date
t.
flush and as required)
Serial No. (s)
of Flushed Batteries
Serial No. (s)
of Flushed Batteries
2.
3.
4.
5.
Following
Rec ireulation
2Hr
8Hr
Final
Start/Finish
Time/Date
Deactivation Conpleted :
Battery Power Supp1y Discarded:
Date:
Date:
S ignature :
Note: Upon Log conpletion, send copy to OO-ALC/LMI'IRO
FIGURE 2. DISCHARGE AI{D DEACTIVATIoN LOG (CoNT',D)
v. Set discharge roon VOLTI{ETER SELECTOR SWITCH (2, Flgure 3) to
correspondlng battery power supply.
SARNTNG
Connecting a load to the battery power supply
may cause severe arclng. Ensure clrcult
breaker for corresponding discharge station ls
in OFF posltlon. Fellure to comply could
result ln lnjury or death to personnel.
w. Ensure that clrcult breaker (ST) (Figure 3) for correspondlng
station is in OFF position.
CAUTION
The load cable connectors are of different
sizes to aid ln proper mating to battery power
supply terminals. Connecting cable to rnrong
terminal may cause damage to equlpnent.
x. Attach posltive (red) and negatlve (black) load cables to battery
po\rer supply ternlnals and secure terninal bolts.
y. Observe discharge roon BATTERY VOLTAGE INDICATOR (1, Flgure 3) and
record open clrcuit voltage (OCV) on Discharge and DeactLvatl.on
Iog.
z. Repeat steps r through y for battery polrer supplles in renainlng
stations.
Yq.?ftll arLtcTrolart?ct{
l.
2.
3.
A,.
5.
6.
1.
B.
BATTERY VOLTAGE I ND I CATOR
VOLTMETER SELECTOR SW I TCH
C IRCU IT BREAI<ER ST I
C IRCLJ IT BREAKER ST2
CIRCUIT BREAKER ST3
CIRCUIT BREAKER ST4
CIRCUIT BREA}<ER ST5
CIRCUIT BREAKER ST6
Flgure 3
Battery Power Supply Dlscharge Room Details
GAUTTON
-ltre AUTOI'{ATIC Ct T-OFF SWITCH detetmlnes the
battery voltage level for automatlc dlscharge
terminatlon and prevents battery over-
dlscharge. Itre AUTOMATIC CUT-OFF SI{ITCH must
be ln the proper posltlon for the partlcular
battery manufacturer or a battery exploslon may
occur.
CAUTION
Electrical discharge of batteries from
different manufacturers cannot be perfor:med
s imultaneously .
NOTE
Connect battery power supplies to discharge
load one at a tlme. Start wlth battery power
supply located furthest from door.
OnIy one person shall remain ln dlscharge room
when eircuit breakers are set on. The other
person shall exlt to the DRC\MS area to nonitor
voltage and obsenre events in discharge room.
Electrlcal actlvatlon of the Dlscharge
Circuitry is a two man operatlon. One person
statlon at the Control Panel and the other at
the Circuit Breaker.
Discharge clrcultry can be
press ing BATTERY DISCHARGE
switch on DRCWS.
deenergLzed by
EI-{ERGENCY SHUTDO!ilN
10
aa.Verify AUTOI{ATIC CUTOFF SWITCH (5, Figure 1) ls in the proper
posltlon to prevent over-dlscharglng of batterles. Set AUTOUATIC
CUTOFF SI{ITCH to posltlon "0.7 V" for GTE manufactured batterles
and "7.0 V" for Altus uanufactured batterles.
ab. Set DRC\NS VOLffiETER SELECTOR SI{ITCH to correspondlng battery pot er
supply station.
ac,Note tlne, observe BATTERY VOLTAGE INDICATOR (8, Flgure 1), depress
and hold OVERRIDE SWITCH (9, Flgure 1), and set clrcult breaker
(ST) (Figure 3) for corresponding statlon to ON posltlon. (If
circuit breaker has been trlpped, reset by noving handle to extreme
OFF position. ) Voltage drop indicates appllcatlon of load.
Release OVERRIDE SWITCH on the Control Panel.
ad. Verify SUBII0DULE IOADED light (3, Figure 1) for corresponding
station ilh.rmlnates.
ae. Repeat steps
is connected
ab
to
and ad until last battery power supply (Station L)
discharge load.
af. Depart and secure discharge room.
NOTE
Allow battery power supplles to
mi.nutes before proceeding wlth
discharge 10- t5
steP ag.
ag.Set DRCV!{S VOLTMETER SELECTOR
position and record discharge
Discharge and Deactivatlon Log.
SWITCH to each battery stati.on
load voltage on corresponding
1t
Complete dlscharge
supply may take as
NOTE
of a fresh battery power
long as 22 days.
aJ
ah. At DRCWS,set ROOM LIGHTS swlteh to OFF positlon.
lock outer door.ai. Secure and
Request SECITRIIY AIARl.l SYSTEI{ SWITCH to 'Str (ON) positlon.
ak. To gain reentry into the Mechanical Roon and Discharge Bay, repeat
steps a through o and monltor battery power supply discharge as
required.
NOTE
Battery discharge is automatically terminated
when the battery voltage reaches 7 .O VDC or 0 .7
VDC depending upon automatic cutoff switch
Position.
al. Observe if any SUBIIODULE IOADED lights (3, Figure 1) are
illtrninated. If not illunlnated, proceed to step ao for batteries
being dlscharged to 7.0 volts (Altus) or step aq for batteries
being discharged to 0.7 volts (GTE). If llghts are llluminated,
proceed to step am.
am. Set DRC\,!IS VOLruETER SELECTION SWITCH for each illuninated
SUBMODULE LOADED light and record voltage on corresponding
Discharge and Deactlvatlon Log.
L2
er1. Repeat steps ah through ak.
NOTE
Wtren a clrcuit breaker has trlpped at a battery
dlscharge station, the voltage shown on the
BATTERY VOLTAGE INDICATOR wlll be the Open
Clrcult Voltage (OCV). To determlne the aetual
state of battery discharge, the battery must be
placed under a loaded condltlon.
ao. Perforrn step ac to reset statlon clrcuit breaker. Set DRCWS
VOLTMETER SELECTOR SI{ITCH to approprlate statlon (subnodule)
position. Obsenre BATTERY VOLTAGE INDICATOR and record voltage on
corresponding Discharge and Deactivation Log.
(t) If load voltage of the battery power supply ls greater than
7.0 vdc then drops quickly xo 7.0 vdc and the clrcult breaker
trips, proceed to step as.
(2) If load voltage is greater than 7.0 vdc, and the voltage does
not drop appreciably ln t hour, a discharge circuit
nalfunctlon has occurred and shall be reported for correction.
After correctlons are conplete, a1low discharge to continue.
Monitor as required to insure discharging ls occurring.
ap. Repeat steps ah through ak.
NOTE
I{tren a circult breaker has tripped at a battery
discharge station, the voLtage shown on the
BATTERY VOLTAGE INDICATOR r.rilI be the Open
Circuit Voltage (OCV) . To determlne the actual
state of battery discharge, the battery must be
placed under a loaded condition.
13
aq. Perform step ac to reset statlon clrcult breaker. Set DRCWS
VOLffiETER SELECTION SITITCH to approprlate statlon (subnodule)
posltlon. Obsenre BATTERY VOLTAGE lndicator and record voltage on
correspondlng Dlscharge and Deactlvatlon Log.
(1) If load voltage of each battery power supply ls greater than
0.7 vdc, then drops quickly to 0.7 vdc and the clrcult breaker
trips, proceed to step as.
(2) If load voltage ls greater than 0.7 vdc and the voltage does
not drop appreclably ln t hour, a dlscharge clrcult
nalfunction has occurred and sha1l be reported for correctl.on.
After correctlons are conplete a1low diseharge to eontlnue.
Monitor as regulred to insure discharglng ls occurrlng.
er. Repeat steps ah through ak.
as. Press BATTERY DISCHARGE EMERGENCY SHUTDOI{N button on DRCVI{S to
assure circuit breakers (1 through 5, Figure 3) are in OFF
position.
at. Allow t hour to elapse. Set DRCWS VOLT!,IETER SELECTION SWITGH to
approprlate station (subnodule) posltlon. Observe BATTERY VOLTAGE
lndicator and record post discharge +1 hour on corresponding
Discharge and Deactlvatlon Log.
au. Reset clrcuiE breakers for those battery statlons stlIl undergolng
electrlcal dlscharge.
L4
NOTE
It is not necessary to remove a single battery porrer
supply lmediately after electrlcal dlscharge. If
lt is more convenlent, additlonal power supplles can
be dlscharged and then several batterles can be
removed slnultaneously.
av. Turn off SYSTE!,! POIJER (5, Figure 1) on DRCV!{S.
ew. Uslng insulated tools, discorurect negative and posltive load cables
fron battery power supply tenninals in the station(s) that have
conpleted electrical discharge and lnstalI terninal covers on
battery power supplies.
ax. l,[ark "electrlcally discharged" on battery and shipplng contalner
exterior.
ay. Install battery power supply shipplng container covers.
NOTE
Deactivation of discharged battery power
supplies shalI commence wlthin 90 days of
complete discharge.
az. Transport created battery power supplies to deactlvatlon area or
return to storage to await deactlvation.
ba. Position, connect, and dlscharge additlonal battery(les) of the
same Eanufacturer lf required by performing steps p through ad.
bb. Perform steps ah through aJ to exit and secure Mechanical Room.
15
II. DEACTMTIONT/DISPOSAL 0F BATTERY POIIER SUPPLIES. Deactivatlon of
discharged battery polrer supplles is accompllshed as follows:
a. Inspect all tanks, plplng and valves to be used in the deactlvatlon
for defects such as cracks, tears, fractures, etc.
b. Check level of evaporatlon ponds to insure ponds ean handle
discharge \rater fron deactivation operations. Ttre inflow plpes
have tvo marks for level control. ltre upper nark represents the
maximr:m pond leve1 that must not be exceeded (18 lnches of
freeboard). The lower nark slgnlfles the ulnlntrm volune requlred
for battery deactlvatlon uslng one deactlvation tank.
(1) Verify that the pond level is below the lower mark prlor to
operation or the naximum pond level w111 be exceeded.
(2) Remove caps from lnspectlon pipes at the base of both
evaporation ponds and check for presence of water. If water
is present, liner ls leaklng and shall be reported for
correction. Environmental ManageBent shall be contacted for
sanpltng of leaklng fluid and 6ivlL Engineerlng shal1 be
contacted for llner repalr.
c. Open }IAIN POWER breaker box and switch main breaker to the ON
position.
d. Verify nonorall breaker box switch is ln the ON position.
e. Turn on lnterior llghts in each pump house.
NOTE
Steps f through i are performed at each
deactlvation tank and pump house. Start at
Pr-tmp House #L .
15
f. Attach monorail hoist cable hook to llftlng eye of deactlvatlon
tank eover and unfasten cover frorn tank.
rAR}.{ING
No one shall be under suspended monorall load.
Failure to conply could result ln lnJury or
death to personnel.
Exerclse eautlon while working
deactivation tank. Falls lnto
in injury to personnel.
Hardhats must be worn by all
the monorail crane. Failure
result in lnjury or death to
near uncovered
tank may result
personnel
to conply
personnel,
using
could
g-Using monorail hoist,Ilft cover off deactlvatlon tank.
(1) Position cover to slde of tank (covers nay be stacked)
(2) Disconnect monorail hoist hook from llfting eye.
CAUTTON
Under no cirer:mstances shall any pump be
operated when lts suetlon intake sereen ts
nisslng or danaged.
Examine interior of deactlvation tank:h.
L7
(1) Verlfy that a long
at valve V22 and e
lnlet valve V23.
suctlon l1ne ls attached to the punp lnlet
short suetton llne ls attached at pump
a1.
(2> If suction lntake acreen appears do-aged or is nisslng,
replaee acreen before proceeding.
(3) Clean any debrls from botton of deactlvation tank. Ttre debrls
uust be disposed of ln a uanner conslstent with state and
federal regulatlons.
Close or verify that valves V4 through V25, V28, and Y29 are
closed.
Repeat steps f through I for Pump House #3 lf lt ls to be used.
k. Open nain lrater supply Ilne Vl located behind Pump House #2.
Open inlet and outlet valves (V3) on backflow preventer.
Open deactivation tank water fill valve V6 at Pump House #1 and
monitor water 1evel as tank ls fllllng to prevent overflow.
I{hen water level reaches second ladder rung fron top of
deactlvation tank, close deactlvatlon tank water f111 valve V5.
Repeat steps m and n et Pump House #3 if lt is to be used.
SARNING
Do not subj ect battery power supplies to rough
handling ln loadlng and transportlng. Case
rupture or puncture or danage to scrubber of
battery power supply plping could release toxic
n.
TARNING (CONT'D\
vapors and corrosive naterial hezardous to
personnel ln the area. Fallure to conply could
result ln lnjury or death to personnel.
NOTE
A maxlmum of four discharged batterles can be
deactivated at a tlme, tvo battertes ln each
tank.
p. Transport the crated battery power supplles to monorail pickup at
end of access road turnaround.
q. Remove battery power supply shlpping container cover and plaee near
deactlvatlon tank.
r. Verify serial nrrmber on battery polrer supply and Discharge and
Deactivatlon Log (Figure 2) agree.
s. Attach cable liftlng sllng to battery power supply llfting eyes.
t. Connect monorail holst cable hook to sllng eye Loop.
u. Insure personnel are clear of innedlete area and, uslng uonorail
holst, ralse battery porrer supply fron shipplng contalner base and
move it to a posltlon adJacent to deactivatlon tank to be used, and
parallel to shlpplng container cover.
v. Lower battery polrer supply to the gror:nd next to shlpping container
cover.
19
y.
Discorurect monorall holst cable hook fron cable sllng eye loop.
Disconnect cable llftlng sling fron battery power supply llftlng
eyes.
For renaining battery porrer supplies, repeat steps q through
positloning a ma:rlnnrm of two battery power supplles adJacent
each deactivatlon tank, parallel to thelr shipplng contalner
covers.
TIARNING
x,
to
Don face shield prlor to
ePoxy from battery Power
ePoxy may cause danage to
drilling or chipping
supply. Partlcles of
eyes .
Steps z through
be perforned on
disposed. Start
#1 .
Terminal end of fillport
aid in proper positionlng
suPPly.
NOTE
az (battery preparation) shall
each of the batteries to be
with batteries at Pr,rnp House
locator is marked to
on battery power
z. Don face shield. Use chlsel- to carefully pry G-10 cover (thin
layer of epoxy) from top of battery power supply. Dlscard epoxy.
aa. Place fil-lport locator (Flgure 4) on top of battery power supply
and secure with L/2 - 20 x L/2 lnch cap screws.
20
Figure 4
FillPort Locator
2L
ab. Using variable speed drlll and 2 lnch hole saw, eut through
openlngs provided by flllport locator.
ac. Remove fillport locator fron battery pouer supply.
TIARNING
Exercise cautlon when chlpplng epoxy to avold
danage to scrubber tublng located on top of
battery power supply or to the eell cans,
located approxlmately L/2 lnch below the epoxy.
Damage to the scrubber tublng or cell cans may
result in release of SOe.
Sulfur dioxlde (SOz) concentration of 2 ppm or
greater presents a hazardous conditlon.
Failure to evacuate all above ground personnel
2000 ft. upwind, or provide approved personnel
protection as required could result ln lnjury
or death to personnel.
ad. Position SO, detector in close proxinity to battery power supply.
Don resplrators lf presence of SO2 ls lndicated prlor to contlnulng
with procedure.
ae. IJtrile wearing face shield, rubber epron, and gloves, use a hr"'-er
and chlsel to clear area approxlmately 3n x 3" around each ce1l
fillport. If necessary, use utlllty knife to cut and remove cell
intercormect cabling.
af. Using a utlllty knlfe and/or chlsel, cut and renove plastic caps
covering fillport plugs.
22
ag. Install flllport plug renoval flxture (Figure 5) along one side of
bettery power supply.
(1) Allgn hole ln tool over flllport plug and attach to side of
battery power supply vLtJ}: L/2 - 20 x L/2 LI]lc}j. cap screws.
(2) Tighten screws securely.
TARNING
Removal of fillport plugs nay release vapors
hazardous to personnel. Protective clothing
shal1 be worn untll all hose-to-cell
connections are completed. Fallure to comply
could result in injury or death to personnel.
ah. A11 personnel lnvolved ln fillport plug renoval shall don rubber
gloves, rubber apron, and resplrator.
al. Insert 5/15 inch Allen wrench through hole in removal flxture and
slowly loosen fillport plug to relieve cell pressure.
aj. After venting stops, renove flllport pLug removal fixture, and
repeat steps ag through al for renaining celI fillport plugs along
same side of battery power supply.
ak. If wrench opening in a flIlport plug strlps out, repeat steps ag
through ai for fillport plug on opposite side of that celL and
perforn steps an through ar.
a1. After venting stops, reuove fillport plug removal fixture. Uslng
5/16 inch Allen wrench, remove three cell fillport plugs from
opposite side of battery power supply.
23
HOL=
Figure 5
Use of FlII Plug Removal Fixture
1 a=t I '?
I !.-
-(-
I
aa --. . -1 L:,LL 1
? ?=t r i
t-tt----
L iR3\Ci{ IIIS:RTION
'
CTP SCREi
6 SCRE'i SLOTS
N\
24
Steps am through aq are
wrench openlng in celI
out and plug cannot be
NOTE
perforned only lf
flllport has strlpped
renoved from ce1l.
Fqr. Using a metal prick prrnch and
center of fillport plug to be
ftamrnss, stanp drlll start point
drlIled through.
1n
If both fillport plugs
stripped out, cell will
Drilling into f lllport
hazardous vapors.
TIARNING
in the seqe ceII have
be under pressure.
plug nay release
an. Don rubber gloves , rubber apron, and respirator.
ao. Using variable speed drllI with 3/8 tnch drlll blt and drIll stop
set at one inch fron tip of drill, drIll through flllport plug.
ap. Garefully brush array any metal chips that result frorn drilling.
aq. Insert treasy-out" in fiLlport plug end remove p1ug.
NOTE
Vented scrubber shall be deactivated along wlth
battery power supply. Non-vented scrubber
shall be removed and disposed of prlor to
deactivation of battery power supply.
25
ar. Inspect vent lndlcator on scrubber.
(1) If lndicator has blackened, battery power supply has vented
through scrubber. Perforn steps as and at.
(2) If indicator ls turchanged, perforn steps au and av.
as. Using a utllity knlfe, cut scrubber tublng above flttlng uor.urted on
scrubber. Rernove insulated sleevlng.
at. Using an offset #2 Philllps head screwdrlver, renove top plate of
scrubber. Cut serubber tubing below top plate and dispose of top
plate.
au. Using utility knife, cut and remove scrubber tubing.
av. Using 3/t6" Allen wrench, remove four screws securing scrubber to
battery power supply. Remove and dispose of scrubber and tubing
according to Iocal procedures.
arr. Place deactivation flxture (Figure 6) on lts side parallel to the
top of battery power supply shlpping cover.
CAUTTON
Do not drag flush hose assemblies over ground
or pavement. Abusive treatment to flush hose
assemblies tray result ln damage to plated
surfaces of the flttlngs.
26
9 --4>
e*af
'ir F-.'.A
i
/
r7/3
1
2
3
4
5
6
7
8
9
BATTERY POt.JER SUPPLY
BA TT E RY POI.J E R SUP PLY
FLUSH HOSE ASSEIVIBI.Y
FLUSH HOSE ASSEMBLY
FLUSH HOSE ASSEIUIBLY
DEACTIVATION FIXTURE
FLUSH HOSE ASSEIUIBLY
FLUSH HOSE ASSETUIBLY
FLL' SH HOSE ASSEFIBLY
1
2
FH2-1
FH2-?
FH2-3
FH1 -1
FH1 -2
F H1 - 3
Flgure 5
Flush Hose Assernblies to CeII Connection
27
NOTE
To aid in proper flush hose assenbly to cell
conneetlon, the batterles are referred to as
battery power supply 1 and battery power supply
2.
Cells of the battery power supply are nrrmbered
sequentially (1, 2, and 3) from scrubber end of
battery power supply.
Care must be taken not to over-tighten flush
hose assenbly to cell filIport.
ax. Pass ends of flush hose assenbly (7, 8, and 9, Figure 5) through
deactivatlon fixture (5, Flgure 6) of battery power supply 1.
Connect ends of flush hose assenbly to ee1l fillports. Tighten
with wrench until washer makes contact with cell fillport, then
turn an addltlonaJ- L/4 to L/2 turn. Connect in the following
sequence:
(1) FHl-l to ceIl #1.
(2) FItl-2 to ceII *2.
(3) FItl-3 to cell #3.
ey. If required, pass ends of flush hose assenbly (3, 4, and 5, Flgure
5) through deactlvatlon flxture (5, Figure 6) of battery porrer
supply 2. Gonnect ends of flush hose assenbly to ceIl fllIports.
Tighten wlth wrench untll washer makes contact with ce1l flIlport,
then turn an addltional L/4 to L/2 turn. Connect ln the following
sequence:
( 1) Ftl2 - 1 to ceIl #1 .
(2) Fttz -2 to ceIl #2 .
(3) FIl2-3 to cell #3.
28
a::2. Carefully llft deactlvatlon flxtures fron the shipplng contalner
covers and place over top of battery power supplles 1 and 2.
(1) Adjust fixture clamps to engege botton edge of battery power
supply upper attachnent pads.
(2) Equally tlghten each clamplng assenbly untll fixture ls flrnly
secured to bettery power supply and ln total contact with top
of battery. (Move hoses sllghtly lf clearance is needed to
tighten clanps.)
ba. Attach cable llfting sling to battery power supply lifting eyes and
connect monorall holst cable hook to sllng eye loop.
bb. Using monorail hoist, ralse and suspend battery power supply
approximately 5 lnches above ground.
bc. Obtaln t.wo 7-L/2 foot lengths of 1/8" plastic coated wlre and
prepare as follows:
(1) Make 4-inch loop at each end of both cables.
(2) Secure loops with cable clamps.
bd. Install a shackle (2, Figure 7) in each eye of deactivation
fixture.
be. Connect deactivation cables (4, Flgure 7) to shackles on one slde
of deactivation flxture.
bf. Route deactivatlon cables dlagonally under battery polrer supply and
connect to shackles on opposlte slde of deactlvatlon flxture.
bg. Raise and suspend battery power supply over deactivatlon tank.
29
N \
L.
2.
3.
4.
5.
DEACTIVATION FIXTURE
SHACKLES
BATTERY POWER SUPPLY LIFTING EYE
DEACTIVATION CABLES
BATTERY POWER SUPPLY
Figure 7
Use of Deactivation Fixture and Deactivation
30
CabIes
CAUTION
I{tren placlng battery power supply ln
deactivation tank prlor to burstlng, posltlon
battery power supply 1n tarrls on opposlte slde
of tank from suctlon lntake plplng, and secure
llfting sllng to ladder.
bh.Slowly lower and posltion battery polrer supply lnto deactlvatlon
tank.
(1) Position battery power supply on opposlte slde of tank fron
suction lnteke plplng.
(2) Disconnect monorall hoist cable hook fron sllng eye loop.
(3) Tie cable lifting sling to slde of tank with a two foot
sectlon of L/8" plastlc coated wire so that sling eye loop can
be retrieved at conpletlon of deactlvation cycle.
bi. Repeat steps ba through bJ for battery power supply 2 lf
applicabLe.
bj Pass the single ends of two flush hose assenblies through the wal-l-
openlngs ln Pr:np House #2. Connect one hose to V8 and the other to
vll.
Steps bk through
performed on two
and deactlvation
Punp House #L.
ck (battery bursting) are
batterles at each punp house
tank. Start wlth batteries at
bk. Verify burst valve V7 ln the punp house ls closed.
bI. Turn nitrogen gas
counterclochrise
(GNz) regulator valve control
several turns untll knob feels
knob
loose to the touch.
bm. Open
than
Don
vent
GNz
750
ualn tank valve and verlfy pressure gauge lndlcates greater
pslg. If less than 750 pslg replace GN2 tarrk.
bn. Insure valve V15 at the bottorn of the accumulatlon tank is closed.
TIARNING
Don face shield prior to openlng accunulator
tank vent valve due to posslble hydraulic
pressure bulIdup. Fallure to comply eould
result in lnjury to personnel.
bo.faee shield and rubber gloves ,
valve V5.
and slowly open aecumulator tank
IIARNING
Do not add water to accunulator tank if
pressure in tank is 15 psig or greater.
Failure to conply coul,d result ln inj ury or
death to personnel.
bp. Slowly open eccunulator tank inlet water valve V4.
( 1) I{hen water begins
V5, close V5.
(2) Close accumulator
spraylng out of accunulator tank vent valve
tank inlet water valve V4.
slowly turn
to 500 pslg.
GNe regulatorbg. I{hile obserrrlng regulator pressure gauge,
valve cloclcwise and regulate GNz pressure
ITARNTNG
Clear immediate area of personnel before
attempting to burst battery power supply cells.
Failure to conply could result in injury or
death to personnel.
NOTE
Battery power supply eells shall be burst ln
the following order: celI 3, ceIl 1, cell 2.
Burst is detected by a fast drop on burst
pressure gauge. Start with battery power
supply 1.
Periodically monitor bursting gauge during
bursting activity. If gauge lndicates an
i.ncrease ln hydraul-ic pressure when burst valve
V7 is closed, open bleed valve V26 to release
pressure and enable connectlon of flush hose
assembly. (Ensure bleed valve V26 is closed
once pressure ls released. )
33
br. Connect flush hose assenbly Ffl1-3 to burst valve qulck dlsconnect.
(1) Iltrile monitorlng burst pressure gauge, slowly open burst valve
v7.
(2) lltren ceII has burst, close burst valve V7.
bs. Disconnect flush hose assenbly Fttl-3 fron burst valve qulck
discormect. Corurect flush hose assenbLy FlIl-3 to fLush valve V10.
bt. Obsenze accumul-ator tank water leve1 lndlcator llght.
(1) If low water level lndlcator 1lght ls off, proceed to step bx.
(2) If low water level lndlcator llght ls on, proceed to step bu.
bu. Turn nitrogen gas (GN2) reguLator valve control knob
counterclockwlse several turns untll knob feels loose to the touch.
bv. Don face shield and rubber gloves. Slow1y open eccunulator tank
vent valve V5. Allow accumulator tank pressure to bleed down below
15 psig.
bw. Repeat steps bp and bq to reflll and pressurize acctrmulator tank.
bx. Connect fLush hose assenbly FHl-1 to burst valve quick disconnect.
(1) Wtrile monltorlng burst gauge, elowly open burst val-ve V7.
(2) I{tren cell has burst, close burst valve V7.
by. Disconnect flush hose assenbly Flll-l fron burst valve qulck
dlsconnect. Connect flush hose assenbly Fttl-l to flush valve V8.
34
bz. Observe aceumulator tank water leve1 lndicator llght.
(1) If low water level
leve1
lndlcator light is
lndicator llght ls
off, proceed to step ca.
oD, repeat steps bu(2) If low water
through bw.
ca. Connect flush hose assenbly f'HL-2 to burst vaLve guick disconnect.
( 1 ) Wtri le moni tor lng burs t gauge ,slowly open burst valve V7.
(2) Wtren cell has burst,close burst valve V7.
cb. Disconnect flush hose assenbly Fttl-2 fron burst valve qulck
disconnect. Connect flush hose assenb).y Fttl-2 to flush valve V9.
cc. Obsenre accr.unulator tank water 1evel indlcator Ilght.
(1)
(2)If low water level indicator ltght is on, repeat steps bu
through bw.
NOTE
If only one battery ls to be burst, proceed to
step cl. If a second battery ls to be burst,
Proceed to steP cd.
cd. Connect flush hose assenbly FH2-3 to burst valve quick dlsconnect.
(1) lltrile nonltoring burst gauge, slowly open burst valve V7.
If low water level indicator llght ls off, proceed to step cd.
(2) Wtren cell has burst, close burst valve V7 .
ce. Disconnect flush hose assenbly FH2-3 frou burst valve qulck
dlscorurect. Corurect flush hose assenbly Ftt2-3 to flush valve V13.
cf. Obsenre acctrmulator tank water leveI lndlcator llght.
(1) If 1ow water leve1 lndlcator llght ls off, proceed to step cg.
(2) If low water level lndlcator llght ls on, repeat eteps bu
through bw.
cg. Connect flush hose assenbly Ftl2-1 to burst valve qulck dlscorurect.
(1) lltrile monltorlng burst gauge, slowly open burst valve V7.
(2) I{tren cell has burst, close burst valve V7.
ch. Disconnect flush hose assenbly FlI2-1 fron burst valve qulck
disconnect. Connect flush hose assenbly FII2-1 to flush valve Vll.
ci. Observe accumulator tank water level lndlcator llght.
(1) If low water level lndlcator llght is off, proceed to step cJ.
(2) If low water 1evel lndicator llght ls on, repeat steps bu
through bw.
cJ. Connect flush hose assenbly FH2-2 to burst valve quick dlsconnect.
(1) Whl1e monltorlng burst geuge, slowly open burst valve V7.
(2> I{tren cell has burst, close burst valve V7.
ck. Dlsconnect flush hose assenbly FIt2-2 fron burst valve qulck
di.sconnect. Connect flush hose assenbly Ftl2-2 to flush valve V12.
cl. Verlfy that valves V18 through V25, V28, and \129 are closed.
36
cm. Slowly open pump prining valve V15 untll water stops flowlng at the
flow indicator. Close V15 and alIow alr fron suctlon Ilne to rise
lnto upper piping (approxinately 1-2 ninutes). Reopen V15.
cn. Slowly open flush valve V8. Allow prining water to flow through
purnp and to battery power supply 1. Verlfy t ater fLow through flow
lndicator.
NOTE
If flow is not established, slowly close V15
and reopen VL5 slowly allowing lines to prop-
erly flood. If flow is stiIl not established,
close V15 and VB and repeat steps cm and crl .
co. Set recirculatlon punp *1 breaker to ON position and press puup
START button.
cp. Slow1y elose pump priming valve V15.
cq. Slow1y open flush valves V9 and V10.
NOTE
Perform steps cr through cv if a second battery
is being flushed. If a second battery will not
be burst, proceed to step cw.
cr. Slowly open prinlng punp valve V17 untll weter stops flowlng at the
flow lndicator. Close V17 and al1ow air fron suction llne to rlse
into upper piping (approximate).y 1-2 ninutes). Reopen V17.
37
cs. Slowly open flush valve V11. Allow prlnlng rrater to flow through
punp and to battery power supply 2. Verlfy water flow through flow
lndicator.
NOTE
If flow ls not establlshed, slowly close VL7
and reopen V17 slowly allowlng llnes to
properly flood. If flow ls stlII not
establlshed, close VL7 and Vl1 and repeat steps
er and cs.
ct. Set reclrculation pr.rnp #2 breaker to ON position and press pump
START button.
cu. Slowly close pr:np prlmlng valve V17.
ev. Slowly open flush valves V12 and V13.
cw. Perform steps cx through di to ensure proper burstlng of the
battery ceIIs.
ITARNING
Exercise care while working near uncovered
deactivation tank. Falls lnto water may result
ln lnjury to Personnel.
Water in deactivatlon tank ls acidie. Fallure
to don protectlve face shleld, rubber gloves,
and rubber apron could result in lnJury to
Personnel.
38
cx. Attaeh nonorall hoist hook to eye loop of battery power supply
cable sling and untie holdlng wlre fron tank ladder.
CAUTION
Jagged metal edges that result fron cell burst
could damage deactlvatlon tank llner.
cy. Using monorall holst, ralse battery power supply approxlmately 5
lnches above deactlvatlon tank water level and observe water flow
through ce11s of battery power supply.
(1) If all three cells have properly burst, proceed to step dg.
(2> If flush hose(s) have burst lnstead of battery polrer supply
cell(s), proceed to step cz.
cz. Press appropriate recirculatlon punp swltch STOP button.
da. Close flush valves in ptrnp house and allow water to drain fron
battery power supply.
db. Don protective Eear. Uslng nonorait hoist, posltlon battery power
supply at side of deactlvation tank and lower to pavement.
dc. Replace danaged flush hose assenbly(ies).
dd. Using monorall holst, return battery porrer supply to botton of
deactivation tank.
de. Repeat applicable steps bn through cm to burst renaining ceIl(s).
39
df. Perfonn steps cn through cv to restart reclrculatlon pumps.
dg. Return battery power supply to botton of deactlvation tank and
repeat steps cx through cy to check reuaining pot er supply if
applicable.
NOTE
Steps di and dj through dl can be performed
durlng forced water clrculation.
dh. Maintaln forced water circulatlon contlnuously for two hours.
After two hours, press appropriate punp STOP button to ternlnate
circulation. Obtain sample and measure pH in accordance with Waste
Analysis Plan.
di. Repeat steps z through di for battery porrer supplles at Punp House
#3 if applicable.
dj. Attach monorall holst cable hook to lifting eye of the
neutrallzation tank cover and unfasten cover fron tank.
TIARNING
No one shall be under suspended monorail load.
Failure to conply could result ln lnjury or
death to personnel.
Exercise care while worklng near uncovered
deactivation tank. Falls lnto tank may result
ln lnjury to personnel.
40
dk. Using monorail hoist, llft cover off neutrallzatlon tank.
(1) Posltion cover to side of tank (covers nay be stacked).
(2) Disconnect uonorall holst hook fron lifting eye.
CAUTION
Under no clrcr-rmstances shall any punp be
operated when tts suctlon lntake screen ls
known to be nlssing or danaged.
dl . Examine interior of neutr alization tank:
(1) Verify that a long suctlon Ilne ls attached to V23 and a short
suctlon line is attached to 1122.
(2) If suction intake screen appears da.naged or is mlssing,
replace screen before proceeding.
(3) Clean any debris from botton of neutrallzation tank. The
debris must be disposed of ln a uanner conslstent with state
and loca1 regulatlons.
dn. After cornpletion of forced water reclrculatlon, press appropriate
pr:np STOP button to terninate eirculatlon.
CATTTION
I'lre voltrne of the neutr a]izatlon tank is the
same as each of the deactlvatlon tanks.
Neutr al,Lzatlon of each deactlvatlon tank must
be performed tndivldually.
4L
NOTE
Use of one pump ls adequate to pump the
contents of the deactivatlon tank to the
neutralLzatlon tank. Operate appropriate
valves for the punp destred for use.
dn. Verify that valves VB through V13 ,
are closed.
VL8 through V25, V28, and V29
do. Slowly open pump prinlng valve VL6NL7 to fill suction llne and
slightly open \24f\125 to bleed out air. Close V24/\125 when water
begins to leak fton \124f\125.
dp. Set ptunp switch #1 or #2 breaker to ON positlon and press
appropriate punp START button.
NOTE
If flow is not established, slowly reopen
VL5fiL7 and V24N25 allowing lines to properly
flood. If flow is still not established, close
V15 NL7 and repeat steps do and dp.
dq. Slowly open V28/V29 and slowly close punp prining valve VL6/VL7.
dr.Monltor water level as deactivation tank dralns. tltren water level
is below suctlon filter, press recirculatlon pump STOP button.
ds. close valves v28N29.
dt. Refill deactivatlon tank wlth water by perfornlng steps m and n.
du. Repeat steps cI through cq to restart rrater reclrculation and also
steps cr through cv lf water reclrculatlon through a second battery
is requlred.
dv. Maintain forced water clrculatlon for eight hours.
dw. Neutrallze the neutrallzatlon tank eontents by perfornlng steps d:r
through el.
d:(. Transport bags of sodlun carbonate and the sodlum carbonate hopper
to the nonorail plckup at end of access road turnaround.
dy. Don face shield and load 150 pounds of soditrm carbonete per battery
deactivated lnto the hopper.
dz. Attach monorall hoist cable hook to llfting sllng of sodium
carbonate hopper.
ea. Using monorail hoist, raise sodium carbonate hopper approxlmately 1
foot above ground. Move hopper to a position approxinately 1 foot
above neutralizatlon tank.
WARNTNG
I{ater in neutralLzation tank may be acidic.
Failure to don protectlve face shleld, apron,
and rubber gloves could result in lnjury to
personnel.
eb. Slowly dispense sodium carbonate from the hopper into
neutralization tank. Stop sodium carbonate addition when no more
sodium carbonate w111 dlssolve ln the tank. Record anount of
sodiuur carbonate added on data sheets.
43
ec. Move sodir:n
access road
carbonate hopper
turnaround.
to monorail plckup area at end of
monorall holst hook from llftlng eye of sodium carbonateed. Disconnect
hopper.
Ensure that the ends
assenblies connector
dlscharging into the
NOTE
of the flush hose
to valves V8 and Vll are
neutralization tank.
eg.Perform steps cl through cv to recirculate contents of
neutralizatlon tank and mlx the sodlum carbonate for at l-east 15
minutes.
ef . IJtren the solid soditrm carbonate ls dlssoLved, press punp ST0P
buttons #1 and *2 and obtaln rrater samples in a clean contalner
from several- areas of the neutralizatlon tank ln accordance with
Waste Analysis Plan.
NOTE
Only add enough sodium carbonate to raise the
solution pH between 5.0 and 7 .5. Care nust be
used to not add excessive sodirrm carbonate or
the 7 .5 pH limit w111 be exceeded.
eg. Using lltmus
(1) If pH is
samPles ,
paper or a pH meter, determine the pH of the liquld.
greater than 6 and less than 7.5 ln all of the
record pH on data sheets and proceed to step ej .
44
(2>
(3)
If pH is 6 or less ln any of the sanples, proceed to step eh.
pH is greater than 7.5, open V6 to add dilutlon water to
tank. Repeat step eg.
NOTE
It may be requlred to restart the reclrculatlon
punps (steps c1 through cv to agltate the
additional sodir:m carbonate .
If
the
eh. S1owly dispense (by hand) 25 pounds
neutralLzation tank. Allow 2 hours
water sanple. Record pH and amount
data sheets.
of sodium carbonate lnto the
to elapse and obtain additlonal
of sodir:m carbonate added on
ei. Repeat step eg as required untll a pH greater than 5 and less than
7.5 is obtalned.
ej Obtain f.iquid sample ln accordance with lJaste Analysis PIan.
Discharge neutrallzed water solution fron the neutrallzatlon tank
to the evaporatlon ponds by perfornlng steps ek through es.
ek. Verify that the correct discharge valve is opened to allow punping
to the desired evaporatlon pond. 0pening valve V30 allows fluld to
be ptuped to the snall pond, opening valve V31 allows fluid to be
pumped to the large pond.
NOTE
Ptrmping of solution from the neutr al'Lzatlon
tank to the evaporation ponds ls acconplished
at Punp House #2.
45
eI . Verlfy that valves V8 through V25 are closed.
NOTE
Use of one punp to draln the neutr al,Lzatlon
tank ls adequate. Steps em through es
describes the use of punp #L for tank dralnlng.
em. Slowly open valve V16 to prlne punp #1.
en. Slightly open V24 to bleed out alr. Close V24 when rrater begins to
leak fron V24.
eo. Set recirculatlon punp switch #1 breaker to ON posltlon and press
punp START button.
NOTE
If flow is not established, swltch ptrnp to OFF
and perforxn steps em through ep.
ep. Open valve V18 in Ptrnp House #2 and close V15.
eq. Verify liquid flow lnto appropriate evaporatlon pond.
er. ttonitor draining of neutrallzatlon tarrk lnto evaporatlon pond.
I{hen suctlon fllter becomes exposed, press recirculatlon prrnp #1
STOP button.
es. Close valve V18.
46
et. After elght hours of clrculatlon of the batteries ln the
deactivation tank, collect another llquid sample ln accordance with
I{aste Analysis Plan. Repeat steps d,n through ds to puup fluld to
neutrallzatlon tank.
eu. Refl1l deactlvation tank by perforning steps u and n.
ev. Repeat steps cl through cv to perforn addltlonal battery flushing.
ew. Repeat steps dy through es to neutrallze and pump water to
evaporatlon pond.
ex. llalntaln forced lrater circulation for L-L/2 to 2 days.
ey. Following the thlrd flushing operatlon, attach monoraiL hoist hook
to eye loop of battery power supply cable sllng.
CAUTION
Jagged rnetal edges that result fron cell burst
could darnage deactivation tank li.ner.
ez. Using rnonorail hoist, ralse battery power supply approxinately 5
inches above deactivation tank rrater 1evel.
fa. Press recirculatlon pr:rnp STOP button and close correspondlng flush
valves.
fb. Using a hose connected to the water llne
house, rinse the battery and flush hoses
fc. Allow water to drain from battery power
on the outside of the punp
wlth rrater.
suPPly.
47
fd. Keeplng battery power supply et least 6 lnches above tank, move
battery power supply frou tank to area adJacent to tank.
fe. Lower battery porrer supply adJacent to tank and disconnect monorail
holst cable hook fron cable sllng eye 1oop.
ff. Disconnect cable llfting sllng fron battery power supply llftlng
eyes.
fg. Disconnect flush hose assernblles from eell flIlports.
fh. Disconnect and remove shackles and deactlvation cables from eyes of
deactivation fixture. Retaln shackles and deactivatlon cables for
reuse.
fi. Loosen clamping assenblies and renove deactivatlon fixture from
battery power supply. Retain flxture for reuse.
fj. Collect a liquid sanple ln accordance wlth Waste Analysls Plan.
Repeat steps dn through ds to pump contents of deactlvation tank to
neutralization tank.
fk. Perforn steps eh through es to neutralize and pr-rnp fluid to
evaporatlon pond(s).
fl. Cornplete Deactivatlon and Dlscharge Log and malntain as reguired.
fro. Discard battery power supply in accordance with Waste Anal-ysls
Plan.
fn. Repeat steps ey through fk to remove renainlng batteries from
deactl.vatlon tanks.
fo. If no additlonal batteries w111 be disposed of for 30 days, proceed
to Section III, C1ean-up of Deactlvatlon Facility.
48
III. CLEAI{-UP OF DEACTIVATION FACILIIY .
NOTE
ltre post-deaetlvatlon procedures ln steps
through ad are conmon for both Punp House
and #3. Start wlth Punp House #L.
a
#1
a.Verffy that flush hoses
place loose ends of all
tank(s ) .
are attached to valves
flush hose assemblles
V8 through V13 and
lnto deactlvation
b.
NOTE
Perform steps b through
house at a time.
h on one side of punp
Insure that valves VB through V13, V16 or V17, V20 or V21, Y22 and
V23, V24 or V25, and V28 or V29 are closed.
ITARNING
Exercise care whlle worklng near uncovered
deactlvation tank. Falls into water may result
ln lnjury to personnel.
I{ater ln deactlvatlon tank may be acldic.
Splashes of water may cause lnJury to
personnel.
49
c. Slow1y open fresh water prlnlng valves V16 and V17.
d. Slowly open flush valves V8 through V13 and obserrre flow of rrater
fron all flush hose assenblles lnto deactlvatlon tank. Detenline
lf pressure ls equal frou each hose assenbly.
(1) If water flow fron any flush hose asseubly ls Iow, proceed to
steP e.
(2) If water flow Is equal, proceed to step h.
e. Close flush valve (V8 through V13) controlling flow to flush hose
assenbly wlth low pressure.
f. Disconnect flush hose assenbly fron qutck disconnect and connect e
known free running flush hose assenbly ln lts place.
E. Slowly open flush valve controlling flow (V8 through V13) to newly
installed flush hose assenbly. 0bsenre water flow.
(1) If water flow fron thls hose ls nornal, clean or replace
original hose as necessary.
(2) If water flow from this hose ls still low, a blockage exlsts
in inlet nanifold and sha1l be reported and corrected.
h. Allow fresh rrater to flow through each hose for 5 mlnutes. Close
valves V16 and V17 and flush valves V8 and V13. Dlscorurect al.l
flush hose assenblies fron qulck disconnects. Store hoses to dry.
i. Slow1y open pump prlnlng valve V16 or V17 unttl rrater stops flowlng
at the flow indicator.
50
Set reclrculatlon punp SI{ITCH #L
press punp START button to punp
neutralization tank.
Slowly open valve V28 or V29 .
Do not allow pumps to
deactivation tank has
filter. Danage to the
or #2 breaker to ON posltion
deactlvatton tank contents to
and
the
k.
1.Check for flow lnto neutrallzatlon tenk.
(1) If flow ls not establlshed, slowly close V16 or V17 end reopen
V16 or V17 slowly allowlng llnes to properly flood. If flow
ls still not establlshed, slowly close rite ot V17 and V28 or
V29, then reopen V15 or V17 and Y28 or Y29.
CAUTION
continue runnlng once
emptied below suction
PUnP Can OCCtrT.
Monitor water leveL as deactlvatl.on tank drains. tlhen water Ievel
ls below suctlon filter, press reclrculatlon pump #1 or #2 OFF
button. Close valve V28 or V29.
Open water flush vaLves V16 and V17 ln both Pr.rnp Houses *1 and #3
to f ill Punp #1 and Pr.rnp #2 plping rrlth water.
Open valves V28 and V29 ln both Pr.rmp Houses #1 and #3 to flush
overhead lines leadlng to the neutrallzation tank.
P.A1low water flush of llnes to contlnue for L0 mlnutes.
sL
TIARNING
Exercise care whlle working near uncovered
neutralLzatlon tank. Falls lnto tank may
result ln lnJury to personnel.
Water belng dlscharged lnto tank may be acldtc.
Wear faeeshield, rubber apron, and rubber
gloves. Splashes of acldlc water may lnjure
personnel.
q. Obtain a sample of water belng dlscharged lnto the neutrallzation
tank.
r. Measure pH of line flush water wlth pH Eeter.
s. Continue water flush of Ilnes until a pH of 5 or greater Ls
obtalned.
t. Close valves V15, V17, V28, and V29.
u. At pump houses #l and #3, open prlnp line draln valves Y22 andtl23
and open high point vent valves V20, V21, V24, and V25 to drain
water frorn punps.
v. Open valves V8 through V13 to draln dlscharge Ilnes.
TIARNING
Face shield, rubber apron, and rubber gloves
shal1 be worn when rinstng acld contamlnated
objects. Splashes of acldlc rrater may lnjure
Personnel.
52
Uslng a hose attached to the faucet on the outsldes of the punp
houses, open faucet and water Bpray the lnterior of the
deactivatlon tank.
Using shovel and buckets, renove residue water and partlcles fron
bottom of deactivation tarrk and transfer to neutralization tank.
y. Glean pump suctlon lIne fllter screens ln the deactivatlon tank.
Uslng a cLean cloth, wlpe down deactlvatlon tank wall. If
necessary, use a paint scraper or nlld abraslve to remove
particles.
aa. Inspect deactlvatlon tank for leaks, cracks, corrosion, or erosion
which nay lead to cracks.
ab. Inspect all fittlngs lnside and outslde of deactlvation tank for
leaks and corrosion.
ac. Attach monorail holst cable hook to llftlng eye of deactivation
tank cover.
TTARNING
No one shall be under suspended monorail load.
Failure to conply could result ln lnjury or
death to personnel.
Hardhats must be urorn by all personnel uslng
the monorail crane. Fallure to conply could
result in inJury or death to personnel.
53
ed. Uslng rnonorall holst, lift cover and place on deactivation tank.
Secure cover to deactlvatlon tank. Dlsconnect monorall holst hook
fron llftlng eye.
ae. Repeat steps w through ad at Punp House #3 lf required.
af. Don face shield, epron, and rubber gloves.
ag. Uslng pH neter, Deasure pH of resldual rater ln the neutrallzatlon
tank.
(1) If pH ls greater than 6, proeeed to step al.
(2> If pH ls 6 or Iess, proceed to step ah.
ah. Slowly dispense (by hand) 25 pounds of sodirlm carbonate into
neutralization tank. Mix contents wlth paddle for at least 15
minutes. Repeat step ag.
ai. Perform steps aj through ap to pr.rJrp neutralizatlon tank contents
with Purnp *1 to evaporation pond.
aj. Examine the suctlon lntake screen on the long suetion llne (Punp
#1) to verify that it is lntact and not danaged. Replace screen if
required prior to proceeding.
ak. Verify that valves V8, V9, V10, V18, V20, V23, V24, and V28 are
closed.
al. Slowly open pump prlnlng valve V16 to f111 suctlon llne and
slightly open V24 to bleed out alr. Glose V24 when water begl.ns to
leak fron V24.
am. Set reclrculation punp srritch #1 breaker to ON position and press
punp START button.
54
an. Slowly open V18 and slowly close prrltrp prlnlng valve V15.
NOTE
If flow ls not establlshed, slowly close V15
and V18 and reopen V15 allowing llnes to
properly flood. If flow ls still not
establlshed, close V16 and repeat steps aI and
an.
ao. Monitor
leve1 is
button.
water level as
below suction
neutr a].Lzation
filter, press
tank drains. Wtren water
recirculation punp STOP
ap. Close valve V18.
aq. Perforn analysis of residue as reguired by the Waste Analysls Plan.
Using shoveL and buckets, renove resldue water, partlcles, and
sodium carbonate from bottom of neutrallzatlon tank. Place ln 55
gallon llned drrrm. Disposition as directed by envlronnental
engineering, EM.
ar. Cleanup of the solids ln the evaporatlon pond is requlred prlor to
sollds reaching a depth of 18 inches. Sanples of the soLld
residues shall be collected ln accordance wlth the Waste Analysis
P1an.
55
IV. WINTERIZATION OF LITltIlrM BATTERY DISPOSAL FACILIIY. lfinterlzatlon of
the Lithlun Battery Dlsposal Faclllty urtrst be perforned to prevent
darnage to facillty equipnent and plping and is acconplished as follows:
e. Transport 4, 55 galIon druns of antlfreeze, barrel stand, and 2
sets of flush hose assenblles to the monorall plckup at the access
road tur:raround.
b. Open I{AIN POI{ER breaker box and swltch naln breaker to the ON
position.
c. Verify monorail breaker box swltch is ln the ON position.
d. Turn on interior lights ln each prrmp house.
NOTE
Steps e through o are performed at each
deactivatlon tank and acconpanying pump house.
Start at Punp House #1 .
e. Attach monorall hoist cable hook to llfting eye of deactivation
tank cover and unfasten cover fron tank.
TIARNING
No one shall be under suspended monorall load.
Failure to comply could result ln injury or
death to personnel.
Exerclse cautlon whlle working near uncovered
deactlvatlon tank. Falls lnto tank may result
in injury to personnel.
s5
Hardhats must be worn by all personnel uslng
the monorail crane. Failure to conply could
result tn lnjury or death to personnel.
f. Uslng nonorall hoist, lift cover off deactlvatlon tank.
(1) Position cover to side of tank (covers nay be stacked).
(2) Dlsconnect nonorall holst hook fron llfting eye.
CAUTION
Under no circr.mstances shall any punp be
operated when its suction intake screen is
missing or danaged.
g. Examine interior of deactivation tank:
(1) Glean any debris from bottom of deactivation tank. Itre debrls
must be disposed of ln a manner conslstent with state and
federal regulatlons.
h. Close or verify that valves V5 through V29 are closed.
NOTE
Addition of antifre eze is performed at each
punp and assoclated piplng separately.
i. Open vent valves V?ONZL ln punp house.
57
J. Transport one barrel of antlfteeze to the pump house.
k. Pour antifreeze lnto valves V20/V2L to f111 plplng and prrmps.
1. Obse:rre flow meters on valves V8, V9, VLO/LL, V12, V13 to ensure
antlfreeze addltlon. If no entlfreeze ls obsenzed, add antlfteeze
through approprlate valves V8, V9, V10411 , VLz, V13.
n. Al1ow antifreeze to drain through Punp *L/#2 and lnto the
deactlvatlon tank.
n. Open valves V8 through V10411 through V13 when draining is
complete.
o. Repeat antlfreeze addition to remaining pump and plping.
p. Perform steps e through o at Pump House #3.
q. Transport barrels of antlfreeze to neutralizatlon tank.
r. In Punp House #2, verlfy that a long suction line ls attached to
the pr:mp #1 inlet at valve V23 and that the suction lntake screen
is not danaged.
s. Open vent valve V21 tn Prlmp House #2.
t. Pour antifreeze lnto V21 to fill piplng and punp #2.
rl. Obsenze fl-ow meters on valves V1l , V12, end V13 to ensure
antlfreeze additlon. If no antifreeze ls observed, add antlfteeze
through approprlate valves V11, V12, or V13.
v. Al1ow antifreeze to draln through punp #2 and lnto neutrallzation
tank.
s8
t . Open valves V11, VLz, and V13 when drainlng ls conplete.
x. Pour all remalnlng antlfreeze lnto neutrallzatlon tank except for
approxinateIy one half barrel.
y. Verlfy that valves V6 through V10, V15, V17, V19, V20, V22 through
V24, V26, V27, V28 and V30 are closed.
z. Verlfy V31 ls open.
ea. Note liquld leve1 ln the neutrallzatlon tank. If liquld level ls
above the suctlon lntake screen, proceed to step af. Perform step
ab if the llquid level ls below the suctlon lnlet screen.
ab. Open nain water supply llne Vl.
ac. Open lnlet and outlet valves V3 on backflow preventer.
ad. Open neutralization tank water fill valve V5 to add water to tank.
ae. Close valve V5 when tank liquid level ls above the suction lnlet
screen.
af. Slowly open pump prfunary valve V15 until water stops flowing at the
flow lndicators. Close valve V15 to allow alr frorn suction lines
to rise into upper plping. Reopen valve V16.
NOTE
If flow ls not establlshed, sIowly close V16
and reopen slowly allowlng llnes to properly
flood. If flow ls stlll not establlshed, close
V15 and repeat step af.
59
ag. Set reclrculatlon punp #1 breaker to ON positlon and press ptrmp
START button.
ah. Slowly close punp prlning valve V16.
al. Slowly open valve V18 to punp llquld to the large evaporatlon pond.
CAUTION
Do not allow punp to contlnue runnlng once
neutraLLzatlon tank has enptled below suction
filter. Danage to the punp can occur.
aj. Monitor dralnlng of neutrallzatlon tank lnto evaporatlon pond.
I,ltren suctlon fllters becone exposed, press punp #1 STOP button.
ak. Open valves V8 through V10, V20, V23, and Y24 to drain pr:np #1
piping.
al. I{tren drainlng ls conplete (when no liquid leaks from the suction
line), close valves V8 through V10, and V24.
am. Pour antlfreeze lnto valve Y24 to f111 plping and ptrmp #1.
an. Observe flow meters on valves V8, V9, and V10 to ensure antifreeze
addition. If no antlfreeze ls observed add antifreeze through
appropriate valves V8, V9, or V10.
ao. Allow antifreeze to drain through punp #1 and lnto the
neutrallzatlon tank.
ap. Open valves V8 through V10 when dralnlng ls complete.
50
TIARNING
Exercise caution whlIe working near uncovered
deaetlvat ion/neutrallzation tanks . Falls lnto
tanks may result ln lnjury to persorurel.
eq. Obtaln plastic tarps and cover all deactlvatlon and neutralLzatlon
tank openings.
WARNTNG
No one shalI be under suspended monorall load.
Failure to conply could result in injury or
death to personnel.
ar. Using monorail hoist, llft covers and place on tanks.
covers to tanks.
Secure
as. Drain overhead lines at all three pr.rnp houses by unscrewing llnes
on the discharge side of the six check valves.
at. Reconnect overhead llnes to check valves when draining ls complete.
au. Close main water valve Vl.
av. Open water line draln valve V2.
aw. Operate emergency eyewash statlon to draln water.
ax. Open outside water faucets at each puup house. Close faucets when
draining is conplete.
51
ay. Open aecr.uulator valves V4 and V5 at all three pump houses.
az. Set all punp breakers ln the three pump houses to the OFF posltlon.
ba. furn off llghts ln punp houses and secure entry doors.
bb. Set monorall breaker ewlteh to OFF posltlon.
bc. Open IIAIN POI{ER breaker box and srrltch maln breaker to the OFF
positlon.
\
62