DERR-2024-010105

WASATCH ENVIRONMENTAL, INC.
ENVIRONMENTAL SCIENCE AND ENGINEERING

2410 WEST CALIFORNIA AVENUE
SALT LAKE CITY, UTAH 84104
PHONE [phone]
FAX [phone]
e-mail: [e-mail]
www.wasatch-environmental.com

DRAFT QUALITY ASSURANCE PROJECT PLAN
SALT LAKE CITY INTERMODEL HUB
(VCP-C126)
200 SOUTH 600 WEST
SALT LAKE CITY, UTAH

Project No. 1574-080

To:

Utah Voluntary Cleanup Program
Mr. Bill Rees
195 North 1950 West
Salt Lake City, Utah 84114

Prepared by:

Wasatch Environmental, Inc.
2410 West California Ave.
Salt Lake City, Utah 84104

May 9, 2024
Quality Assurance Project Plan Salt Lake City Intermodal Hub VCP

Wasatch Environmental, Inc. Table of Contents
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TABLE OF CONTENTS

Section Page No.
1. INTRODUCTION .............................................................................................................................. 1
2. QUALITY ASSURANCE/QUALITY CONTROL ............................................................................... 1
3. PROJECT ORGANIZATION AND RESPONSIBILITIES ................................................................. 2
3.1 Voluntary Cleanup Program (VCP)/Utah Division of Environmental Response and
Remediation (DERR) Project Manager ............................................................................................ 2
3.2 Project Manager .................................................................................................................. 2
3.3 Field Staff ............................................................................................................................ 2
3.4 Health and Safety Manager ................................................................................................ 2
3.5 Laboratory QA Manager ..................................................................................................... 3
3.6 Third Party Data Validator ................................................................................................... 3
4. DATA GENERATION/ACQUISITION OBJECTIVE ......................................................................... 3
5. DATA QUALITY PARAMETERS AND OBJECTIVES ..................................................................... 3
5.1 Precision ............................................................................................................................. 3
5.1.1 Field Data Precision ............................................................................................... 3
5.1.2 Laboratory Data Precision ..................................................................................... 4
5.2 Accuracy ............................................................................................................................. 4
5.2.1 Field Data Accuracy ............................................................................................... 4
5.2.2 Laboratory Data Accuracy ..................................................................................... 4
5.3 Representativeness ............................................................................................................ 4
5.3.1 Field Data Representativeness .............................................................................. 4
5.3.2 Laboratory Data Representativeness .................................................................... 5
5.4 Completeness ..................................................................................................................... 5
5.4.1 Field Data Completeness ....................................................................................... 5
5.4.2 Laboratory Data Completeness ............................................................................. 5
5.5 Comparability ...................................................................................................................... 5
5.5.1 Field Data Comparability ........................................................................................ 5
5.5.2 Laboratory Data Comparability .............................................................................. 5
5.6 Sensitivity ............................................................................................................................ 6
5.7 Data Quality Objectives ...................................................................................................... 6
6. QA/QC PROCEDURES ................................................................................................................... 7
6.1 Field QA/QC ........................................................................................................................ 7
6.1.1 Matrix Spike (MS)/Matrix Spike Duplicate (MSD) .................................................. 7
6.1.2 Field Duplicate ....................................................................................................... 7
6.1.3 Equipment Blank .................................................................................................... 7
6.1.4 Trip Blank ............................................................................................................... 8
6.1.5 Spilt Samples ......................................................................................................... 8
6.1.6 Field Quality Control Checks ................................................................................. 8
6.1.7 Field Chain-of-Custody Procedures ....................................................................... 9
6.1.8 Field Logbook Records .......................................................................................... 9
6.1.9 Sample Labeling .................................................................................................. 10
6.1.10 Sample Handling and Transport .......................................................................... 10
6.1.11 Field Maintenance ................................................................................................ 10
6.2 Laboratory QA/QC Procedures ......................................................................................... 10
6.2.1 Laboratory QC Reporting Packages .................................................................... 11
6.2.2 Laboratory QC Checks ........................................................................................ 11
6.2.3 Laboratory Custody Procedures .......................................................................... 11
6.2.4 Laboratory Preventative Maintenance ................................................................. 12
6.2.5 Laboratory Equipment Maintenance .................................................................... 12
7. DATA REDUCTION, VALIDATION AND REPORTING ................................................................ 12
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7.1 Data Reduction ................................................................................................................. 12
7.1.1 Field Data Reduction ........................................................................................... 13
7.1.2 Laboratory Data Reduction .................................................................................. 13
7.2 Data Validation .................................................................................................................. 13
7.2.1 Procedures Used to Validate Field Data .............................................................. 13
7.2.2 Procedures Used to Validate Laboratory Data .................................................... 13
7.3 Data Reporting .................................................................................................................. 14
7.3.1 Field Data Reporting ............................................................................................ 15
7.3.2 Laboratory Data Reporting ................................................................................... 15
7.3.3 Document and Data Retention ............................................................................. 15
8. SPECIFIC PROCEDURES USED TO ASSESS DATA PRECISION, ACCURACY,
COMPLETENESS, AND COMPARABILITY.................................................................................. 15
8.1 Precision Assessment ....................................................................................................... 16
8.2 Accuracy Assessment ....................................................................................................... 16
8.3 Representativeness Assessment ...................................................................................... 17
8.4 Completeness Assessment .............................................................................................. 17
8.5 Comparability Assessment ............................................................................................... 17
9. CORRECTIVE ACTION ................................................................................................................. 17
9.1 Field Corrective Action ...................................................................................................... 18
9.2 Laboratory Corrective Action ............................................................................................ 18
9.3 Corrective Action During Data Validation and Data Assessment ..................................... 18
9.4 Immediate Corrective Action ............................................................................................. 19
9.5 Long-Term Corrective Action ............................................................................................ 19
10. QUALITY ASSURANCE REPORTS TO MANAGEMENT ............................................................. 19
10.1 Contents of a Project QA Report ...................................................................................... 19

TABLES

Table 1 – Summary of DQOs
Table 2 – Summary of Field QC Sample Types and Quantities by Matrix
Table 3 – Analytical Methods, Containers, Reporting Limits, and Holding Times
Table 4 – Calibration and Laboratory Quality Control Procedures – Lead and Arsenic
Table 5 – QC for Lead and Arsenic by Method 6020B
Table 6 – Sample Containers, Preservation, Reporting Limits, and Holding Times – PNAs SIM
Table 7 – Analytical Quality Control and Corrective Action – VOCs and PAHs SIM
Table 8 – Analytical Instrument Calibration – VOCs and PAHs SIM
Table 9 – VOCs Water Detection Limits
Table 10 – VOCs Soil Detection Limits
Table 11 – Sample Containers, Preservation, and Holding Times

APPENDIX

Appendix QAPP-A – Pace Laboratory Quality Manual
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QUALITY ASSURANCE PROJECT PLAN
SALT LAKE CITY INTERMODAL HUB VCP C126
200 SOUTH 600 WEST
SALT LAKE CITY, UTAH

1. INTRODUCTION

This Quality Assurance Project Plan (QAPP) describes the activities for collecting, handling, and
analyzing representative environmental samples at the Utah Transit Authority’s Salt Lake City Intermodal
Hub property (Property), located at approximately 200 South 600 West in Salt Lake City, Utah. The
Property has been accepted into the Utah Voluntary Cleanup Program (VCP-C126) to address
environmental impacts identified in the Property soils.

The Property consists of 15 acres and is within one of the oldest developed sections of downtown Salt
Lake City. The Property includes areas of former and current railroad infrastructures and railroad support
facilities. The history of the property includes a variety of land uses, but primarily commercial and light
industrial since the late 1800s, including railroad activities and three freight houses. The Denver & Rio
Grande Railroad owned and operated the site from the mid-1800s through approximately 1996, when the
railroad was acquired by Union Pacific. In 1997/1998, Union Pacific removed several railbeds. Salt Lake
City purchased at least some of the property in 1999. Two of the freight houses were removed in 2002.
The third warehouse was partially demolished and renovated in 2003 with additional demolition and
remodeling for an interstate bus depot in approximately 2012. UTA acquired the property in June 2007
and has operated the property since that time as an intermodal transit hub that has inclu ded local bus,
interstate bus, light-rail, interstate rail, and commuter rail bus services.

Prior to UTA acquiring the Property, Salt Lake City enrolled the Property in the Voluntary Cleanup
Program (VCP-C016) which received a Certificate of Completion (COC), dated February 21, 2007. The
COC described land use as a transit hub with commercial and retail operations. It excluded use that
included managed care facilities, hospitals, residential uses (including caretakers that live on the
Property), day care and school facilities that may expose children to hazardous constituents for extended
periods of time.

A Site Management Plan (SMP) dated January 8, 2007, is currently in place that requires:
• the property to be used in a manner consistent with the land use described on the COC,
• no groundwater use via wells, sumps or other means for the purpose of irrigation, drinking, or
bathing
• Ground cover to remain across the site in a manner consistent with the Remedial Action Plan,
dated September 24, 2003, and the SMP, and
• Compliance with the contingency plans described in the SMP in the event that impacted material
above the site cleanup goals in encountered.

Generally, the primary contaminants of concern identified during site investigation activities are lead,
arsenic and polynuclear aromatic hydrocarbons (PAHs). Additionally, isolated areas of volatile organic
compounds, mainly petroleum hydrocarbons were also identified in soil and groundwater samples.

All personnel involved with the collection and handling of environmental samples shall be required to read
this plan, and a copy of this plan will be available in the field during all sampling activities.

2. QUALITY ASSURANCE/QUALITY CONTROL

Quality assurance (QA) is a management system for ensuring that all information, data, and decisions
resulting from the investigation are technically sound and properly documented. Quality control (QC) is
the functional mechanism through which quality assurance goals are achieved. All QA/QC procedures
described in this QAPP are structured in accordance with applicable technical standards, agency
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requirements, regulations, and guidance. This QAPP is intended to be used in conjunction with the Site
Characterization Workplans and Remedial Action Plan (RAP) prepared for the Salt Lake City Intermodal
Hub VCP. The QAPP will serve as a controlling mechanism during the performance of the environmental
sampling and analysis activities to ensure that the technical data gathered are precise, accurate,
comparable, complete, and representative of actual field conditions , and meet the minimum QA/QC
requirements for the project. The following information is presented to ensure that QA/QC procedures for
environmental sampling and analysis are performed in accordance with the data quality objectives
(DQOs) for environmental sampling and analysis at the site.
3. PROJECT ORGANIZATION AND RESPONSIBILITIES
3.1 Voluntary Cleanup Program (VCP)/Utah Division of Environmental Response and
Remediation (DERR) Project Manager

The VCP Project Manager is responsible for regulatory oversight of the project and regulatory review and
approval of project planning documents and reports. The Wasatch Project Manager is responsible for
ensuring that the project meets the applicable regulatory requirements.
3.2 Project Manager

The Project Manager is responsible for implementing the project and has the authority to commit the
resources necessary to meet project objectives and requirements. The Project Manager's primary
function is to ensure that technical, financial, and schedul ing objectives are achieved successfully. The
Project Manager will serve as primary point of contact and control for all matters concerning the project.
The Project Manager will:
• Define project objectives,
• Establish project policy and procedures to address the specific needs of the project
as a whole,
• Acquire and apply resources as needed to ensure performance within budget and
schedule constraints,
• Review the work performed on each task to ensure its quality, responsiveness, and
timeliness,
• Review and analyze overall task performance with respect to planned requirements
and authorization,
• Approve all reports prior to their submission to agency representatives ,
• Ultimately responsible for the preparation and quality of interim and final report, and
• Represent the project team at meetings and public hearings.
3.3 Field Staff

The Field Staff includes technicians, geologists, hydrogeologists, and environmental scientists reporting
to, and working under the direction of, the Project Manager. The field staff are responsible for the
execution of the field work and direct oversight of subcontractors performing field tasks such as drilling.
The Field Staff are responsible for completing field work in accordance with the SAP, QAPP, Site -Specific
Health and Safety Plan, and work plans.
3.4 Health and Safety Manager

The project Health and Safety Manager will be responsible for the development of the Site-Specific
Health and Safety Plan and related training of Field Staff. The Health and Safety Manager is also
responsible for ensuring that health and safety procedures are understood and followed by all Field Staff
and for reporting and correcting any violations of policy or regulation.
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3.5 Laboratory QA Manager

The Laboratory QA Manager is responsible for validation of all laboratory analytical data prior to
submission of the data to the Project Manager.
3.6 Third Party Data Validator

The Third-Party Data Validator is responsible for validation of all laboratory analytical data, with respect to
the stated data quality objectives and parameters, prior to use of the data in final reports.

4. DATA GENERATION/ACQUISITION OBJECTIVE
The overall objective of this project is to acquire site data to design a Remedial Action Plan (RAP) to
address the known and not yet known environmental impacts, which may be present at the Site. The
number of samples and density of sampling is based on previously collected analytical data and is
designed to be representative of Site conditions to justify the remedial approach chosen. Each Sampling
and Analysis Plan discusses the specific number, type, and reason for the sample collection.

• investigate the nature and extent of on-site soil and/or groundwater impacts to identify the
contaminants of concern (COC) so that appropriate remedial alternatives may be identified and
evaluated; and the most feasible remedial alternative(s) selected and implemented.
• during implementation of the RAP, to identify, stockpile, characterize, and properly handle of soils
impacted by the COCs that are encountered during soil remediation activities, and
• document that the action levels are achieved after soil remediation activities by the collection of
confirmation soil samples and appropriate QA/QC samples.

5. DATA QUALITY PARAMETERS AND OBJECTIVES

The overall QA/QC objective for this project is to develop and implement procedures for field sampling,
chain-of-custody, laboratory analyses, and reporting that will provide results, which are valid and legally
defensible in a court of law. The purpose of implementing these procedures is to assess the data
obtained with respect to the data quality parameters of precision, representativeness, accuracy,
completeness, and comparability for both the laboratory analytical program and field sample collection
activities. The primary goal of the program is to ensure that the data generated are representative of
environmental conditions at the site. To achieve this goal, a combination of quantitative procedures and
qualitative evaluations will be used to assess the data quality. Precision, accuracy, representativeness,
completeness, and comparability (PARCC) will be computed in the manner described in the foll owing
paragraphs. A qualitative assessment of PARCC factors will be made and will be documented.

5.1 Precision

Precision is a measure of mutual agreement among individual measurements of the same property,
usually under prescribed similar conditions, and typically expressed in terms of the standard deviation or
relative percent difference (RPD).

5.1.1 Field Data Precision

Field precision will be assessed through the collection and analysis of field duplicates and
comparing the analytical results of the field duplicates to the analytical results of the
environmental samples.

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5.1.2 Laboratory Data Precision

Laboratory precision will be assessed through the calculation of RPD and/or relative standard
deviations (RSD) for duplicate samples. Analytical precision will be measured by comparing
analytical results for matrix spike (MS) and matrix spike duplicate (MSD) samples and internal
laboratory samples that may be analyzed according to analytical method or laboratory standard
operating procedure requirements. Acceptance criteria for analytical precision will be based on
established laboratory quality control limits for individual analytes. Applicable control limits are
based on statistically valid historical data compiled by the laboratory, which meet or exceed
precision requirements specified by the analytical method. Standard operating procedures are on
file with the selected project laboratory.

5.2 Accuracy

Accuracy is the degree of agreement of a measurement with an accepted reference or true value. The
accuracy of the analytical data will be assessed by examining possible sources of error that may bias the
analytical results.

5.2.1 Field Data Accuracy

Sources of the errors in the field can occur during sampling (i.e., cross contamination from
sampling equipment, etc.), field handling, and transportation. Accuracy in the field will be
assessed by documenting adherence to standard operating procedures (SOPs) for sample
collection, preservation, and handling; and through preparation and analysis of trip blanks and
equipment blanks. The SOPs for this Project are attached in the Remedial Action Plan.

5.2.2 Laboratory Data Accuracy

Sources of errors in the laboratory can occur during sample preparation and analysis, duplicate
and control sample preparation; and due to instrument and quantification errors. Laboratory
accuracy is assessed through the analysis of standard reference materials (SRMs) in laboratory
control samples, MSs, MSDs, and surrogate compounds and the determination of their recoveries
in terms of percentage. Control limits are established by the laboratory for each analyte based on
statistically valid historical recovery results, which meet or exceed the requirements specified by
the analytical method. In addition, the project laboratory will analyze method blanks to determine
the potential for contamination introduced at any stage of sample preparation or analysis.
Laboratory control limits and frequency for spike recovery and method blank analysis are
specified in standard operating procedures for each analytical method, which are on file with the
selected project laboratory.

5.3 Representativeness

Representativeness is a qualitative parameter that expresses the degree to which sample data accurately
and precisely represent a characteristic of a population, parameter variations at a sampling point, or an
environmental condition. As such, representativeness requires the selection of appropriate analytical
methods, sampling protocols, and sampling locations such that results are representative of the media
being sampled and conditions being measured.

5.3.1 Field Data Representativeness

Representativeness is dependent upon the proper design of the sampling program and will be
satisfied by ensuring that the SMP, and the specific procedures contained therein, is followed.

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5.3.2 Laboratory Data Representativeness

Representativeness in the laboratory is ensured by carefully following standard laboratory
analytical methods and procedures, meeting sample holding times, specifying detection limits that
are at or below regulatory standards, and analyzing method blanks to check for laboratory
contamination. Sample results will not be considered representative if contaminants are detected
in the method blanks, or if the reporting limits are above the specified screening levels.

5.4 Completeness

Completeness is an assessment of the number of valid measurements obtained in relation to the total
number of measurements planned for the successful achievement of the investigative objectives.
Completeness will be expressed as the percentage of valid measurements to the total number of
measurements. The closer the numbers, the more complete the measurement process.

5.4.1 Field Data Completeness

Field completeness evaluates the number of valid measurements obtained from all
measurements taken in the project. The intent of this program is to attempt to achieve a goal of
100 percent completeness. Realizing that under normal conditions this goal may not be
achievable, the completeness goal for this program is 90 percent. This completeness goal is
considered adequate to meet the DQOs for this site based on prior consideration of PARCC
parameters, the sampling plan designs, and data collection activities proposed for each medium.

5.4.2 Laboratory Data Completeness

Laboratory completeness evaluates the number of valid measurements obtained from all the
measurements taken in the project. The intent of this program is to attempt to achieve a goal of
100 percent laboratory completeness. Realizing that under normal con ditions this goal may not
be achievable, the laboratory completeness goal for this program is 90 percent.

5.5 Comparability

Comparability is a qualitative parameter expressing the confidence with which one data set may be
compared to another. Data sets will be compared only when precision and accuracy meet the specified
acceptance criteria established in this section. Samples will be collected, and analytical results will be
reported according to standard procedures and methods to ensure comparability with other similar data
and results. The comparability goal will be achieved by following the Sampling and Analysis Plan and the
Remedial Action Plan, and the specific procedures contained therein, and by collecting and analyzing
representative samples, specifying analysis by similar analytical procedures with comparable reporting
limits and by reporting analytical results in appropriate and consistent units.

5.5.1 Field Data Comparability

Comparability is dependent upon the proper design of the sampling program and will be satisfied
by ensuring that the Sampling and Analysis Plan and the Remedial Action Plans are followed and
that proper sampling procedures are used.

5.5.2 Laboratory Data Comparability

Analytical data will be considered comparable when similar sampling and analytical methods are
used and documented. Similar QA objectives will be used throughout the project to ensure
comparability. At the discretion of the Utah DERR, split samples may be collected for submittal to
a third-party analytical laboratory to assist in evaluation of comparability. The frequency at which
split samples are collected and analyzed will be specified by the U.S. EPA following the receipt
and approval of individual work plans for the project.
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5.6 Sensitivity
Sensitivity is the capability of a method or instrument to discriminate between measurement response(s)
representing differing levels of the variable of interest. The analytical laboratory as part of their standard
operating procedures follows published, approved analytical methods which validate the methods
including an evaluation of sensitivity, precision, and accuracy to ensure that the equipment can operated
the method properly prior to sample analysis.
5.7 Data Quality Objectives

DQOs are qualitative and quantitative statements that specify the quality of the data required to support
decisions made during project activities and are based on the end uses of the data to be collected. The
DQOs for soil samples collected for laboratory analysis during the Salt Lake City Intermodal Hub VCP are
summarized in Table 1.

Table 1
Summary of DQOs

QC Parameter DQO

Precision
Relative percent difference (RPD) of field and
laboratory duplicate (MS/MSD) samples. For
laboratory duplicates, the RPDs within established
laboratory control limits for each analyte are
acceptable. For soil and indoor air field duplicates, a
calculated RPD of 50% will be deemed acceptable.
For groundwater field duplicates, a calculated RPD of
20% will be deemed acceptable.

Accuracy
Spike recoveries from laboratory control samples
(LCSs), MS/MSDs, and surrogates within established
laboratory control limits for each analyte are
acceptable.

Representativeness
Environmental samples will be collected from locations
either reasonably believed to be, or established to be,
representative to identify source areas, evaluate the
nature of the release(s), and delineate the extent of
contamination. Standard field operating procedures will
be used, method blanks are to be free of target
analytes, sample holding times are not to be exceeded,
all samples are to be properly preserved, receiving
temperatures are not to be exceeded, 90% of all field
duplicates meet laboratory precision criteria, and
laboratory method detection limits must be below the
applicable screening levels.*

Completeness
An acceptable level of completeness will be defined as
90% of collected samples being deemed valid based
on precision, accuracy, representativeness, and
comparability acceptance criteria.

Comparability
Where feasible (where previous data exist as with
monitoring wells), analytical results for environmental
samples will be compared previous analyses for the
respective location. Measures of comparability will
include the use of standard analytical methods with
standard units of measure and consistent reporting
limits, and collection of field QC samples.

Sensitivity

Sensitivity is evaluated by the laboratory reporting
detection limit (RDL). The acceptable level of
sensitivity is 100% of RDLs are less than performance
standards.

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* The representativeness has been established requiring that that 90% of all field duplicates meet
the established precision criteria and detection limits will be below applicable screening levels.
However, if sample dilution occurs because of elevated analyte concentrations, the results will not
be rejected.

6. QA/QC PROCEDURES

QC checks will be performed for both field sampling and laboratory analysis of the environmental samples
to allow for the evaluation of data quality, documentation of data quality, and to help identify irregularities
in the field sampling or laboratory analyses that may require correction.
6.1 Field QA/QC

A variety of QC samples will be collected to facilitate the evaluation of the data quality parameters. An
explanation of each type of field QC sample is provided below. A summary of the quantity of each QC
sample type to be collected for each environmental medium (matrix type) is presented as Table 2.
6.1.1 Matrix Spike (MS)/Matrix Spike Duplicate (MSD)

MS/MSDs are QC samples collected in the field for use by the analytical laboratory. The
MS/MSDs are selected to be representative of the environmental matrix at the site. The
laboratory spikes the MS/MSDs with a known quantity of the analyte of interest. The MS and
MSD are then analyzed by the laboratory along with an un-spiked sample and the environmental
samples from the site to evaluate the accuracy and precision of the analytical method for that
specific sample. One MS/MSD will be collected for each matrix (soil and groundwater samples
only) for each sample delivery group.
6.1.2 Field Duplicate

A field duplicate is a QC sample collected from the same location as an environmental sample,
and collected simultaneously, or immediately following, the collection of the environmental
sample. Field duplicates are collected, handled, and analyzed in an identical manner to the
environmental samples. The sample labeling and chain of custody documentation will not
indicate that a sample is a field duplicate (they are blind duplicates) so the analytical laboratory is
not aware that the field duplicate is a QC sample. Field duplicates are analyzed by the laboratory
along with the environmental samples. The analytical results for the field duplicate are then
compared to the analytical results for the environmental sample as an indicator of the overall
sampling and analytical precision. One field duplicate will be collected for each matrix (soil,
groundwater, and indoor air samples only) for every 10 environmental samples for each matrix. A
minimum of one field duplicate per matrix will be collected for each sampling event.
6.1.3 Equipment Blank

An equipment blank (also referred to as an equipment rinsate blank) is a QC sample collected by
pouring deionized water over sampling equipment after the sampling equipment has been
completely decontaminated. Equipment blanks will only be collected when non-dedicated and
non-disposable sampling equipment is used. Equipment blanks will be analyzed for the same
analytes as the environmental samples. The analytical results for the equipment blanks are used
to evaluate the adequacy of the decontamination procedures used to prevent cross -
contamination between sampling locations. One equipment blank will be collected for each
matrix (soil and groundwater only) for every 20 environmental samples for each matrix.
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6.1.4 Trip Blank

A trip blank is a QC sample prepared by the laboratory consisting of a set of sample vials filled
with deionized water. Trip blanks are transported and stored with environmental samples (soil
and groundwater samples only) that are to be analyzed for volatile organic compounds (VOCs).
Trip blanks are analyzed for VOCs only. Trip blanks are collected and analyzed to evaluat e for
cross-contamination of VOC samples due to diffusion that may occur during transport and
storage of environmental samples. One trip blank will be included in each cooler used to
transport VOC samples. At this time, we do not anticipate collecting soil samples for VOC
analysis.
6.1.5 Spilt Samples

A spilt sample is a QC sample collected from the same location as an environmental sample, and
collected simultaneously, or immediately following, the collection of the environmental sample.
Spilt samples are transported and analyzed separately (by ChemTech-Ford) than the
environmental samples. The analytical results for the split sample are then compared to the
analytical results for the environmental sample as an indicator of the overall analytical accuracy
and precision. The Utah VCP may collect splits of soil and groundwater (if collected) samples at
their discretion.

Table 2
Summary of Field QC Sample Types and Quantities by Matrix

Environmental
Media (Matrix)
MS/MSD Field
Duplicate
Equipment
Blank
Trip Blank Split Samples
Soil 1 per sample
delivery
group, all
analytes
1 per 10
environmental
samples, all
analytes,
minimum of 1
per sampling
event
1 per 20
environmental
samples, all
analytes, only
if non-
dedicated
sampling
equipment is
used
1 in each
cooler
containing
VOC samples
At discretion
of Utah VCP
Groundwater
(if collected)
1 per sample
delivery
group, all
analytes
1 per 10
environmental
samples, all
analytes,
minimum of 1
per sampling
event
1 per 20
environmental
samples, all
analytes, only
if non-
dedicated
sampling
equipment is
used
1 in each
cooler
containing
VOC samples
At discretion
of Utah VCP
6.1.6 Field Quality Control Checks

Internal QC procedures are designed to ensure and document the overall quality of data. The
QC checks represent system checks and controlled samples introduced into the sample analysis
stream that are used to validate the data and calculate the accuracy and precision of the
chemical analysis program. Field quality control will also be checked by equipment blanks and
field duplicates.
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6.1.7 Field Chain-of-Custody Procedures

Custody is one of several factors which is necessary for the admissibility of environmental data as
evidence in a court of law. Custody procedures help to satisfy the two major requirements for
admissibility: relevance and authenticity. Sample custody is addressed in three parts: field
sample collection, laboratory analysis, and final evidence files. Final evidence files, including all
original laboratory reports, are maintained under document control in a secure area.

A sample or evidence file is under your custody if:
• the item is in actual possession of a person;
• the item is in the view of the person after being in actual possession of the person;
• the item was in actual physical possession, but is locked up to prevent tampering; or
• the item is in a designated and identified secure area.

A chain-of-custody form will be completed to record the custody of every sample collected for
laboratory analysis. A chain-of-custody form will accompany every delivery of samples to the
analytical laboratory in order to establish the documentation necessary to trace sample
possession from the time of sample collection through sample analysis.

The sample portion of the chain-of-custody form will include the following:
• project number, name, and location;
• sample identification;
• date and time of sample collection;
• sample type;
• number of containers;
• name of Project Manager, sampler, and recorder;
• sampling information (sampling area, depth, media type, type of sample, date, and
time of collection, etc.);
• analysis requested and specific analytical method;
• preservatives used, if any;
• filtering used, if any;
• signatures of persons involved in the chain-of-custody possession, including dates
and time; and
• condition of samples and sample bottles received by the laboratory.

When a chain-of-custody form is filled out, a copy is retained for the client file. The original form
accompanies the sample(s) until completion of laboratory analysis. The laboratory copies the
form and returns the original with the sample report. When the sample report is r eceived, it is
crosschecked with the chain-of-custody file record and both chain-of-custody pages and the
laboratory report are placed in the client file.

6.1.8 Field Logbook Records

A field log of daily activities will be used to record sampling activities on a daily basis. This book
will be bound and have consecutively numbered pages. Entries in the field logbook will be made
in ink and will include:
• the project name/number;
• name of the author/sampling team;
• date and time of entry;
• location of activity;
• chronological record of field activities;
• names and affiliations of personnel on site;
• sample collection or measurement methods;
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• number of samples collected;
• daily weather report;
• sample identification numbers;
• field observation and comments;
• sampling depth increment for field measurements;
• locations of photographs; and
• any deviations from the RAP, QAPP, or work plan.

All logbook entries will be signed, dated, and no erasures will be made. If an incorrect entry is
made, the information will be crossed out with a single strike mark, initialed, and dated by the
sampler. Each logbook will be assigned to a specific field team member and given a project
specific project documentation number.
6.1.9 Sample Labeling

Sample labels are necessary to prevent misidentification of samples. Each label will contain
space for the following information:
• name of the site,
• sample identification,
• date and time of sample collection,
• media sampled,
• name of sampler,
• type of preservative,
• type of filtering, and
• types of analyses to be performed.
6.1.10 Sample Handling and Transport

For transport, all soil and groundwater samples will be stored on ice or dry ice (depending on the
sample type and required cooling requirements) and packaged in such a manner as to prevent
damage or breakage during handling and transport to the laboratory. Samples delivered to the
laboratory will be delivered by sampling personnel. Sample containers will be labeled and placed
into suitable shipping containers. If samples are to be shipped, the containers will be sealed with
custody seals and taped closed. All sample holding times will be tracked and the COC form will
accompany the samples in a sealed plastic bag.

Custody seals will be placed on each sample cooler or container used to transport and/or store
samples.
6.1.11 Field Maintenance

Logs or field notebooks will be used to record maintenance, service procedures and schedules
for the field equipment. All maintenance records will be documented and traceable to the specific
equipment, instruments, tools, and gauges. Any items found to be inoperable will be tak en out of
use. Records shall be reviewed and maintained by the Project Manager and field staff when
equipment, instruments, tools, and gauges are used at the site.
6.2 Laboratory QA/QC Procedures

The laboratories which will be performing analyses of environmental samples for this project are certified
by the State of Utah and/or have National Environmental Laboratory Accreditation Program (NELAP)
accreditation. The Pace Laboratories Quality Manual is attached as Appendix QAPP-A. Pace
Laboratories QA/QC tables are attached as Table 3 through Table 9.

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The primary laboratories selected for this project are:

• Pace Laboratories for analysis of soil and groundwater samples, and
• Chemtech-Ford for analysis of split samples.

6.2.1 Laboratory QC Reporting Packages

All laboratories will be required to provide Level 3 QC reporting packages (or their equivalent).
For the purposes of this QAPP, a Level 3 QC package includes:
• Analytical results,
• COC records,
• Case narratives,
• Surrogate recoveries,
• Method blanks,
• Laboratory control samples (LCSs),
• Laboratory analysis of MS/MSDs collected from this project (not samples collected from
other projects included in the analytical batch), and
• Chromatograms for organic analyses and logbooks.
6.2.2 Laboratory QC Checks

Laboratory QC checks are accomplished through the use of system checks and QC samples that
are introduced into the same analysis stream as the environmental samples. Laboratory system
checks and QC samples for the inductively coupled plasma/mass spectrometer and gas
chromatograph/mass spectrometer are documented in the laboratory SOPs. An example of
laboratory system checks and QC samples for inorganics are defined below.
• Calibration Blank - A volume of acidified deionized water.
• Continuing Calibration Blank - Analytical standard run every 10 analytical samples or
every two hours, whichever is more frequent, to verify the calibration of the analytical
system.
• Instrument Calibration - Analysis of analytical standards for a series of different
specified concentrations; used to define the quantitative response, linearity, and
dynamic range of the instrument to target compounds.
• Preparation Blank - An analytical control that contains deionized water and reagents,
carried through the entire analytical procedures. An aqueous method blank is treated
with the same reagents as a sample with a water matrix; a solid method blank is
treated with the sample reagents as a soil sample.

Laboratory QC checks will be performed, and samples will be analyzed at a frequency
established by appropriate SW-846 and NELAP protocols for inorganics, organics, and the SOPs
for analytical methods used.
6.2.3 Laboratory Custody Procedures

Samples which are delivered by clients or received by courier are placed in a locked sample
control area immediately upon delivery. Coolers containing samples are unpacked within 1 hour
of receipt or placed in the walk-in cooler until unpacked. The COC accompanying the samples
will be signed by the Sample Custodian or their designee at the time of deliv ery by the client, or in
the case of courier delivery, where the COC is sealed inside the cooler, at the time the samples
are unpacked.

At the time of arrival and/or unpacking, coolers will be inspected for evidence of damage. They
will be unpacked carefully, and samples will be organized on the lab bench in numerical order or
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by sample sets and assigned a laboratory job number. The condition of the cooler(s) and sample
container(s) will be recorded on the COC form.

Information on the COC delivered with samples will be verified and recorded as to agreement or
non-agreement. Labels will be checked for notation of proper preservation. If there is an
apparent document non-agreement or incorrect preservation noted, the apparent problem will be
recorded, and the Project Manager notified. The samples will then by marked or labeled with
laboratory sample numbers. Laboratory project numbers are assigned serially, with each sample
numbered as a subset of the project number.

Finally, samples will be placed in appropriate storage and/or secure areas and the location will be
noted on the Service Request Form. Samples received for VOC analysis and samples known to
be highly contaminated are stored separately.

Sample volumes, extracts, and digestates will be disposed of by the laboratory. The volumes are
typically held for 30-60 days after the release of the final report. All samples are segregated by
matrix and solvent used (if applicable), then placed in appropriate waste disposal bins for pickup.
6.2.4 Laboratory Preventative Maintenance

To minimize the occurrence of instrument failure and other system malfunction, a preventative
maintenance program for laboratory instruments will be implemented. Equipment, instruments,
tools, gauges, and other items requiring preventative maintenance will be serviced in accordance
with the manufacture’s specified recommendations and written procedures developed by the
operators.
6.2.5 Laboratory Equipment Maintenance

The laboratory will be responsible for performing routine maintenance and will have available
tools and spare parts to conduct routine maintenance. Maintenance items that cannot be
performed by the laboratory technician will be performed by a person certified to repair the
instrument.

Manufacturer’s procedures identify the schedule for servicing critical items in order to minimize
the downtime for measurement system. It will be the responsibility of the laboratory to adhere to
this maintenance schedule and arrange any necessary and prompt service. In the absence of
any manufacturer recommended maintenance criteria, a maintenance procedure will be
developed by the operator based upon experience and previous use of the equipment. Service to
the equipment, instruments, tools, gauges, etc., shall be performed by qualified personnel.
Records shall be reviewed, maintained, and filed by the operators at the laboratories and will be
available upon request

7. DATA REDUCTION, VALIDATION AND REPORTING

All data collected will be reduced, managed, distributed, and preserved in a manner which substantiates
and documents that data are of known quality. An outline of the QC data handling process for data
collection, reduction, validation, transfer, reporting, and storage for both field and laboratory data is
described below.

7.1 Data Reduction

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7.1.1 Field Data Reduction

Field data collected with instruments such as pH, temperature, conductivity, Eh, specific
conductivity, dissolved oxygen, and photoionization detector (PID) are direct read devices. The
direct reading is recorded in the field logbook, or a groundwater/soil sampling form. No field data
reduction is anticipated.

7.1.2 Laboratory Data Reduction

Raw laboratory data will be recorded in a laboratory notebook along with other pertinent
information, such as the sample identification number. Other information to be recorded includes
laboratory procedure used, name of analyst, date of analysis, matrix sampled, reagent
concentrations and instrument settings. Copies of any strip chart printouts, such as gas
chromatograms, will be maintained on file. The laboratory QA Manager makes per iodic reviews
of these notebooks prior to final data reporting. Equations to be employed in the data reduction
are those outlined in the approved method. Data from laboratory quality control samples will be
compared to the method acceptance criteria. Unacceptable data shall be appropriately qualified
in the results report.

7.2 Data Validation

Technical data, including field data and results of laboratory sample analysis, will be validated to monitor
the performance of the investigation activities. Procedures for validating field and laboratory data are
described below.

7.2.1 Procedures Used to Validate Field Data

Validation of data obtained from field measurements will be performed by the Project Manager.
Field data requiring validation includes the daily calibration of field instruments. Other field
validation procedures include a review of logbooks and proofing data entered and imported into
the computer database for transcription errors.

7.2.2 Procedures Used to Validate Laboratory Data

The Laboratory QA Manager will review all analytical data to ensure that sample results meet all
method specified criteria.

The requirements to be checked in validation are:
• sample holding times,
• calibration,
• blanks,
• surrogate recovery,
• MS/MSDs,
• field duplicates,
• internal performance standards,
• target compound identification,
• interference check sample analysis,
• compound quantitation and reported detection limits,
• tentatively identified compounds,
• system performance,
• overall assessment of data,
• interference check sample analysis, and
• laboratory control sample analysis.

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The Laboratory QA Manager will be responsible for assessing data quality and advising
appropriate laboratory section supervisors of any data that are questionable or have notations
that would caution the data user of possible unreliability.

Data reduction, validation, and reporting by the laboratory will be conducted as follows:
• Raw data produced by the analyst will be turned over to respective supervisor.
• The supervisor will review the data for attainment of QC criteria as outlined in method
protocols and established EPA Methods.
• Upon acceptance of the raw data by the supervisor, a computerized report will be
generated and sent to the QA Manager.
• The QA Manager will complete a thorough audit of all reports.

The Laboratory QA Manager will conduct an evaluation of data reduction and reporting by the
laboratory. These evaluations will consider the finished data sheets, calculation sheets,
document control forms, blank data, duplicate data, and recovery data for matrix and surrogate
spikes. The material will be checked for legibility, completeness, and the presence of necessary
dates, initials, and signatures. The results of these checks will be assessed and reported, noted
any discrepancies and their effect upon acceptability of the data. In addition, the Laboratory QA
Manager will check for data consistency by assessing comparability of duplicate analyses,
comparability to previous criteria, transmittal errors, and anomalously high or low parameter
values.

The following is a description of the validation steps that will be used by the third-party data
validator, if it is determined that one is needed to independently validate the laboratory data
because of irregularities with the data. If performed, these validation results will be summarized
in the final report. The validation steps are listed below:
• Compile a list of all samples;
• Compile a list of all QC samples;
• Review laboratory analytical procedures and instrument performance criteria ;
• Review of chain-of-custody documents for completeness and correctness;
• Review transcription, calculation, completeness, and accuracy;
• Review of laboratory analytical procedures, appropriateness, and instrument
performance criteria;
• A data summary will be prepared and will include analytical results, media
identification, sample location and description, appropriate concentration units,
appropriate significant figures, data qualifiers, and definitions; and
• The laboratory data summary will be reviewed for potential data quality problems
including unexpected results, common laboratory contaminants, samples for which
dilution was necessary, and time and date of sample collection.

A sample data summary will be prepared to assess precision, accuracy, and completeness of the
analytical data. Laboratory records and data package requirements will be checked to assess the
completeness of the data package. The validation will be performed by personnel qualified and
experienced in the field of laboratory data validation.

Despite all efforts to achieve the objectives of the project, the potential for error exists in
laboratory chemical analyses and in the data reporting process. Every reasonable effort will be
made to compare and double-check data reported from the laboratory with data entered into the
data management system.

7.3 Data Reporting

Data generated will be summarized in reports and included in the final report. The Project Manager will
develop a data storage and information system to facilitate tracking, data calculations, and transfer of
data to various forms and reports.
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7.3.1 Field Data Reporting

Data reporting will be performed by the Project Manager. All data collected in the field will go
through data validation procedures and be put into a data management system in an organized
format so that intermittent and final summaries may be easily generated for data review and
project approval.

7.3.2 Laboratory Data Reporting

The laboratories will submit the following reports to the Project Manager. The laboratory reports
will also be included in the final sampling reports.

After laboratory data validation, the laboratory will prepare reports that will include at a minimum
the following components:
• Sample identification,
• Laboratory cross-reference numbers,
• Date of issuance,
• Analysis method numbers performed,
• Results from any analysis,
• Notation of any data qualifiers, and
• Quality control documentation.

Data validation packages are to be prepared for all samples submitted for laboratory analysis.
Sample results reported shall include:
• Summary page indicating dates of analyses for samples and laboratory QC checks;
• Cross referencing of laboratory sample to project sample identification numbers;
• Data qualifiers to be used should be adequately described;
• Sample preparation and analytical methods; and
• QC sample results including MS/MSD RPD, MS/MSD recoveries, laboratory control
sample spike recoveries, method blank results, and surrogate recoveries.
7.3.3 Document and Data Retention

The standard document and data retention policy at Wasatch Environmental, Inc. is to retain all
laboratory data and project deliverables indefinitely in both paper and electronic storage formats.
During execution of projects management of data and project deliverables is the responsibility of
the Project Manager. Following completion of projects, the responsibility for long-term storage of
data and deliverables shifts to an administrative assistant.

8. SPECIFIC PROCEDURES USED TO ASSESS DATA PRECISION, ACCURACY,
COMPLETENESS, AND COMPARABILITY

This section summarizes the QA/QC procedures used in assessing the quality of the chemical data and
the format for presenting the results of the QA/QC evaluations. The data evaluation procedures will be
used by the QA Manager for assessing duplicate and s pike samples and checking blank samples that are
submitted blind to the analytical laboratories from the field or generated internally by the laboratory. The
purpose of implementing these procedures is to assess the chemical data generated with respect to the
PARCC parameters for both the laboratory analytical program and field sample collection activities.

The primary goal of the program is to ensure that the data generated are representative of environmental
conditions at the site. To meet this goal, a combination of statistical procedures and qualitative
evaluations will be used to check the quality of data. Precision, accuracy, and completeness will be
computed in the manner described in the following paragraphs. A qualitative assessment of
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representativeness and comparability will be made and will be documented. Complex statistical data
verification and a significance evaluation will not be performed. If a problem arises and the data are
found to deviate from previous analyses or surrounding conditions, the data will be annotated. Sample
recollection and analysis will be used only in extreme cases where significant QC problems are identified.

Data will be evaluated with respect to the PARCC parameters for both the field sample collection
activities and laboratory analytical programs. The QA/QC program will evaluate data based on QC
sample types discussed in section 5. Because the QC samples are generated for analysis both in the
field and internally by the laboratories, a system of crosschecking has been established that provides
independent evaluations of chemical data on the project level and the laboratory level.

8.1 Precision Assessment

Spiked samples are prepared by choosing a sample at random from each sample set submitted to the
laboratory, dividing the sample into equal aliquots, and then spiking each of the aliquots with a known
amount of analyte. The duplicate samples are then included in the analytical sample set. The splitting of
the sample allows the analyst to determine the precision of the preparation and analytical techniques
associated with the duplicate sample. The RPD between the spike and the duplicate spike are calculated
and plotted.

In addition, RPD will be calculated and reported for field duplicate samples.

The RPD is calculated according to the following formula:

Where:
x = First duplicate or analytical value
y = Second duplicate or analytical value

For the present program, a calculated relative percent difference is that below the control limits
established by the laboratory will be deemed acceptable.

8.2 Accuracy Assessment

In order to ensure the accuracy of the analytical procedures, an environmental sample is randomly
selected from each sample set submitted to the laboratory and spiked with a known amount of the analyte
to be evaluated. In general, a sample spike should be included in every set of 10 samples tested on each
instrument. The spike sample is then analyzed. The increase in concentration of the analyte observed in
the spiked sample, due to the addition of a known quantity of the analyte, compared to the reported value
of the same analyte in the unspiked sample determines the percent recovery. Daily control charts are
plotted for each commonly analyzed compound and recorded. The percent recovery for a spiked sample
is calculated according to the following formula:

Where:
Ms = Amount (mass) of analyte recovered from the spikes sample
M = Amount (mass) of analyte recovered from the primary (non-spiked) sample
S = Known amount (mass) of analyte added to the spike sample

For the present program, control limits that have been established by the laboratory for individual spike
recovery percentages will be deemed acceptable.

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8.3 Representativeness Assessment

Representativeness is a qualitative parameter that expresses the degree to which sample data accurately
and precisely represents a characteristic of a population, parameter variations at a sampling point, or an
environmental condition. The design of and r ationale for the sampling program (in terms of the purpose
for sampling, selection of sampling locations, the number of samples to be collected, the ambient
conditions for sample collection, the frequencies and timing for sampling, and the sampling techniq ues)
ensure that environmental conditions have been sufficiently represented.

8.4 Completeness Assessment

Completeness is the ratio of the number of valid sample results to the total number of samples analyzed
with a specific matrix and/or analysis. Following completion of the analytical testing, the percent
completeness will be calculated by the following equation:

Where:
Zv = Number of valid measurements obtained
Zp = Number of measurements planned

A calculated completeness of 85% or greater will be considered acceptable.

8.5 Comparability Assessment

Comparability is a qualitative parameter expressing the confidence with which one data set may be
compared to another. Data sets will be compared only when precision and accuracy meet the specified
acceptance criteria established in this section. Samples will be collected, and analytical sample results
will be reported according to standard procedures and methods in order to be comparable with other
similar measurement data and sample results. The comparability goal will be achieved through the use of
standard procedures to collect and analyze representative samples, and by reporting analytical results in
appropriate and consistent units. Comparability will be maintained by consistency in sampling conditions,
selection of sampling procedures, sample preservation methods, analytical methods, and data reporting
units.

9. CORRECTIVE ACTION

The following procedures have been established to ensure that conditions adverse to quality, such as
malfunctions, deficiencies, deviations, and errors, are promptly investigated, documented, evaluated, and
corrected. When a significant condition adverse to quality is noted at the site, laboratory, or subcontractor
locations, the cause of the condition will be determined, and corrective action taken immediately. All
project personnel have the responsibility to promptly identify, solicit approved correctio n, and report
conditions adverse to quality. Conditions which warrant corrective action include:
• Predetermined acceptance standards are not attained,
• Procedures or data compiled are determined to be faulty,
• Equipment or instrumentation is found faulty,
• Samples and test results are questionably traceable,
• QA/QC requirements have been violated, and
• System and performance audits indicate problems.

The Project Manager is ultimately responsible for field and QA/QC corrective actions. Any associate has
the authority to stop work if serious QA/QC or field related issues arise. The Laboratory QA Manager will
be ultimately responsible for corrective actions concerning the laboratory.

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9.1 Field Corrective Action

The need for corrective action will be identified as a result of field audits. If problems become apparent
that are identified as originating in the field, immediate corrective action will take place. If immediate
corrective action does not resolve the problem, appropriate personnel will be assigned to investigate and
evaluate the cause of the problem. When a corrective action is implemented, the effectiveness of the
action will be verified such that the end result is elimination of the problem.

Corrective action in the field may be needed when the sample network is changed, or sampling
procedures and field analytical procedures require modification due to unexpected conditions. In general,
any project personnel may identify the need for corrective action. The field staff will recommend the
corrective action. The Project Manager will approve the corrective measure which will be implemented by
the field staff. It will be the responsibility of the Project Manager to verify that corrective action has been
implemented.

If the corrective action will supplement the existing sampling plan using existing and approved procedures
in the work plan, corrective action approved by the Project Manager will be documented. If a corrective
action will result in fewer samples being collected than was planned, alternate sample locations, etc.,
which may result in deviations from the DQOs; the corrective action should be reviewed and approved by
all levels of project management and the DERR Project Manager prior to implementation of the corrective
action.

Corrective action resulting from internal field audits will be implemented immediately if data may be
adversely affected due to unapproved methods or improper use of approved methods. The Project
Manager will identify deficiencies and mandate corrective action. Implementation of corrective actions will
be performed by the field staff. Corrective action will be documented in in field notes and made available
to the Project Manager.

Corrective actions implemented will be documented in the field notes. No staff member will initiate
corrective action without prior communication with the Project Manager.

9.2 Laboratory Corrective Action

The need for corrective action resulting from QA audits will be initiated by the Laboratory QA Manager.
The corrective actions will be performed prior to the release of data from the laboratory. The corrective
action will be documented in the logbook and submitted to the data validator. If the corrective action does
not rectify the problem, the laboratory will contact the Project Manager. If the nonconformance causes
project objectives not to be achieved, it will be necessary to inform all levels of man agement. Corrective
action may include, but is not limited to:
• Reanalyzing the samples, if holding time criteria permit;
• Evaluating and amending sampling and analytical procedures;
• Accepting data with an acknowledged level of uncertainty; and
• Resampling and analysis, if the completeness of the data set or intended use of the data is
recognized during a preliminary review to be insufficient to meet program DQOs.

If the above corrective actions are deemed unacceptable, an alternate laboratory will be selected to
perform necessary analyses.

9.3 Corrective Action During Data Validation and Data Assessment

The need for corrective action during either the data validation or data assessment may be identified.
Potential types of corrective action may include re-sampling by the field staff or re-injection/re-analysis of
samples by the laboratory. These actions are dependent upon the ability to mobilize the field staff,
whether the data to be collected is necessary to meet the required quality assurance objectives (e.g. the
holding time has not been exceeded, etc.). The Project Manager is responsible for identifying situations
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requiring corrective action, documenting the problem, determining the course of action, and implementing
the corrective action.

9.4 Immediate Corrective Action

Any equipment and instrument malfunctions will require immediate corrective actions. The laboratory QC
charts are working tools that identify appropriate immediate corrective actions to be taken when a control
limit has been exceeded. They provide the framework for uniform actions as part of normal operating
procedures. The actions taken should be noted in field or laboratory logbooks. A detailed description of
method-specific corrective action limits is provided in the appropriate method. Any deviatio n from the
prescribed control limits must be approved in writing by the Laboratory QA Manager (for laboratory
problems) or Project Manager (for field problems).

9.5 Long-Term Corrective Action

The need for long-term corrective action may be identified by standard QC procedures, control charts,
and system audits. Any procedural or data quality problem that cannot be solved by immediate corrective
action becomes a long-term corrective action. The essential steps in a corrective action system are as
follows:
• Identification and definition of the problem,
• Investigation and determination of the cause of the problem,
• Determination and implementation of a corrective action to eliminate the problem, and
• Verification that the corrective action has eliminated the problem.

Documentation of the problem is important in corrective action. The responsible person may be a
laboratory analyst, Laboratory QA Manager, Project Manager, or field staff. The Project Manager will
verify that the corrective action has been taken, appears effective, and that the problem has been
resolved.

10. QUALITY ASSURANCE REPORTS TO MANAGEMENT

10.1 Contents of a Project QA Report

Analytical results of samples analyzed by the laboratory will be submitted to the Project Manager
following a QA/QC review by the laboratory. The results will include a tabulation of the analytical data
and an explanation of any field conditions or laboratory QA/QC problems and their effects on data quality.
Proposed corrective action will be recommended in the event that QA problems are identi fied during
review of data quality.

The final report prepared for the project will contain a discussion of QA/QC evaluations summarizing the
quality of the data collected and/or used as appropriate to each activity of the project. The objective of
the QA/QC summary will be to ensure that the data are representative of site conditio ns and sufficient in
quality and quantity to support the field activities. The QA/QC summary will include:
• Tabulated results of all field and analytical data;
• A report from the Laboratory QA Manager evaluating the validity of the analytical data with
respect to accuracy, precision, completeness, and representativeness;
• A report from the Project Manager evaluating the results of field and office audits;
• A discussion of field and laboratory QA/QC including PARCC parameters and data
usability; and
• The laboratory’s Level 3 QC package (method blank results, surrogate recovery, laboratory
control sample results, and MS/MSD results).

A quality assurance report will be prepared by the Laboratory QA Manager upon receipt of sufficient QA
data from the laboratory. The report will be a summary of QA/QC results of the analytical work conducted
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and will be included as part of the final remedial action completion report, submitted to the DERR Project
Manager.

Figure

The use or reuse of this information is restricted to the referenced document unless otherwise authorized.
Wasatch Environmental Copyright 2006
UTA SLC INTERMODAL HUB WEI 1574-080
Figure 1 Vicinity Map
200 South
60
0

W
es
t
300 South
Project
Location

Tables

Analyte
Sample
Matrix Method
Number and Type
of Containers
Standard
Laboratory
Reporting Limit
Analysis
Holding Time
Total Arsenic Soil EPA SW-846 6020B One 2-oz clear wide-mouth jar 2.5 mg/kg
180 days following
collection
Total Lead Soil EPA SW-846 6020B One 2-oz clear wide-mouth jar 6.5 mg/kg
180 days following
collection
Dissolved Arsenic Soil EPA SW-846 6020B One 16-oz plastic with nitric acid 0.001 mg/L
180 days following
collection
Dissolved Lead Soil EPA SW-846 6020B One 16-oz plastic with nitric acid 0.002 mg/L
180 days following
collection
Table 3
Analytical Methods, Containers, Reporting Limits, and Holding Times
Analyte Method
Standard
Laboratory
Reporting Limit
MS/MSD Recovery
Limits (%)*
MS/MSD
RPD Limits (%)*LCS Limits (%)
Total Arsenic EPA SW-846 6020B 2.5 mg/kg 75-125 20 80-120
Total Lead EPA SW-846 6020B 6.5 mg/kg 75-125 20 80-120
Dissolved Arsenic EPA SW-846 6020B 0.001 mg/L 75-125 20 80-120
Dissolved Lead EPA SW-846 6020B 0.002 mg/L 75-125 20 80-120
Table 4
Calibration and Laboratory Quality Control Procedures
Table 5
QC for Lead and Arsenic by Method 6020B

Analytical Method: 6020B Measurement Performance
Criteria
Person Responsible/DQI
Laboratory QC Frequency/Nu
mber
Method/SO
P QC
Acceptable
Limits
Corrective
Action (CA)
Person(s)
Responsible for
CA
Data Quality
Indicator
(DQI)
Method Blank
(= Reagent
Blank)
After calibration
of every 10
samples
<RL Re-analyze. If it
fails again and
CCB is in control,
re-digest batch
Analyst, Inorganics
Supervisor, Quality
Assurance Officer
Contamination,
drift
ICB 1/run <RL Re-run. If it fails
again, recalibrate
Analyst, Inorganics
Supervisor, Quality
Assurance Officer
Contamination,
drift
Laboratory
Duplicates
(MS/MSD set)
1 per batch of
≤20 samples
20% RPD Qualify data Analyst, Inorganics
Supervisor, Quality
Assurance Officer
Precision
Laboratory
Matrix Spike
1 per batch of
≤20 samples
Recovery
75-125%
Qualify data Analyst, Inorganics
Supervisor, Quality
Assurance Officer
Matrix effects
ICV
TV=True Value
TV for As and
Pb= 0.010 mg/kg
1/run +/- 10 %
0.009-0.011
Re-run. If it fails
again, recalibrate
Analyst, Inorganics
Supervisor, Quality
Assurance Officer
Accuracy
Laboratory
Control Sample
(LCS)
TV for As and Pb
= 0.20 mg/kg
1 per batch of
≤20 samples
Recovery 85-
115%
Re-analyze. If it
fails again, re-
digest batch
Analyst, Inorganics
Supervisor, Quality
Assurance Officer
Method
performance

Analyte/Analyte Group Matrix Method /SOP Container(s) number, size
& type per sample Preservation Preparation Holding Time Analytical
Holding Time
Semivolatile Organics by GC/MS
using Capillary Column (EPA
Methods 8270C, EPA 8270D, EPA
Method 625, SM 6410B) Including
Provisions for Analysis in SIM Mode Water ENV-SOP-MTJL-0081
(2) 100 ml Amber glass
container w/Teflon lined lid None 7 days to extraction 40 day extract
Semivolatile Organics by GC/MS
using Capillary Column (EPA
Methods 8270C, EPA 8270D, EPA
Method 625, SM 6410B) Including
Provisions for Analysis in SIM Mode Soil ENV-SOP-MTJL-0081
(1) 4 ounce jar w/ Teflon lined
lid None 14 days to extraction 40 day extract
Analyte Analysis Method Detection Limit Reporting Detection Limit Method Detection Limit Reporting Detection Limit
ANTHRACENE 8270C-SIM 0.00060 0.00600 0.000019 0.00005
ACENAPHTHENE 8270C-SIM 0.00060 0.00600 0.000019 0.00005
ACENAPHTHYLENE 8270C-SIM 0.00060 0.00600 0.000017 0.00005
BENZ(A)ANTHRACENE 8270C-SIM 0.00060 0.00600 0.00002 0.00005
BENZO(A)PYRENE 8270C-SIM 0.00060 0.00600 0.000018 0.00005
BENZO(B)FLUORANTHENE 8270C-SIM 0.00060 0.00600 0.000017 0.00005
BENZO(G,H,I)PERYLENE 8270C-SIM 0.00060 0.00600 0.000018 0.00005
BENZO(K)FLUORANTHENE 8270C-SIM 0.00060 0.00600 0.00002 0.00025
CHRYSENE 8270C-SIM 0.00060 0.00600 0.000018 0.00005
DIBENZ(A,H)ANTHRACENE 8270C-SIM 0.00060 0.00600 0.000018 0.00005
FLUORANTHENE 8270C-SIM 0.00060 0.00600 0.000011 0.00005
FLUORENE 8270C-SIM 0.00060 0.00600 0.000017 0.00005
INDENO(1,2,3-CD)PYRENE 8270C-SIM 0.00060 0.00600 0.000018 0.00005
NAPHTHALENE 8270C-SIM 0.00200 0.02000 0.000128 0.0005
PHENANTHRENE 8270C-SIM 0.00060 0.00600 0.000018 0.00005
PYRENE 8270C-SIM 0.00060 0.00600 0.000017 0.00005
1-METHYLNAPHTHALENE 8270C-SIM 0.00200 0.02000 0.00002 0.0005
2-METHYLNAPHTHALENE 8270C-SIM 0.00200 0.02000 0.000012 0.0005
2-CHLORONAPHTHALENE 8270C-SIM 0.00200 0.02000 0.000028 0.0005
Table 6
Sample Containers, Preservation, Reporting Limits, and Holding Times
PNAs by 8270 SIM
Soil (mg/kg)Water (mg/L)
QC Sample Number/Frequency Method/SOP
Acceptance Critera Corrective Action (CA)Title/position responsible
for Corrective Action
Initial Calibration ICAL prior to sample analysis
Each analyte must meet on
of the three options listed:
RSD for each analyte ≤
15%; linear regression for
each analyte: r2 ≥ 0.99;
non-linear regression
(quadratic): r2 ≥ 0.99.
Correct problem, then repeat ICAL Analyst/Supervisor
Continuing Calibration
Verification
Before sample analisys, ater
every 10 field samples and at the
end of the analytical sequence
All reported analytes
within +/- 20% of true
value
Immediately analyze two
additional CCVs. If both pass,
samples may be reported without
reanalysis. If either fails or two
concescutive CCVs cannot be
performed, reanalyze all sample
since last acceptable CCV. Perform
ICAL if necessary.
Analyst/Supervisor
Laboratory Control
Sample (LCS)One per preparatory batch
Correct problem, then reprep and
reanalyze the LCS and all samples
in the associated analytical batch
for failed analytes, if sufficient
sample volume remains.
Analyst/Supervisor
Method Blank One per prepatory batch
No analytes detected 1/2
LOQ or > 1/10 the amount
measured in any sample.
Common contaminant
must be less than LOQ
Correct problem. If required,
reprep and reanalyze MD and all
QC samples and field samples
processed with the contaminated
blank
Analyst/Supervisor
Matrix Spike/Matrix Spike
Duplicate (MS/MSD)One per preparatory batch
Correct problem, then reprep and
reanalyze the LCS and all samples
in the associated analytical batch
for failed analytes, if sufficient
sample volume remains.
Analyst/Supervisor
Table 7
Analytical Quality Control and Corrective Action
VOCs by 8260 and PNAs by 8270 SIM
Instrument Calibration Procedure Calibration
Range Frequency Acceptance
Criteria Corrective Action (CA)
Title/position
responsible for
Corrective Action
Pace SOP Reference
GC/MS Initial Calibration (ICAL) Multipoint
calibration Refer to SOP At instrument setup; prior to
sample analysis
Each analyte must
meet on of the
three options
listed: RSD for each
analyte ≤ 15%;
linear regression
for each analyte: r2
≥ 0.99; non-linear
regression
(quadratic): r2 ≥
0.99.
Correct problem, then repeat
ICAL Analyst/Supervisor ENV-SOP-MTJL-0081
GC/MS Initial Calibration Verfication (ICV)Immediately after each ICAL ± 20 % of True
Value
Correct problem, Rerun ICV. If
reanlysis fails, repeat ICAL Analyst/Supervisor ENV-SOP-MTJL-0081
GC/MS Continuing Calibration Verification
(CCV)
Before sample analysis, after
every 10 samples and at the
end of the analytical sequence
Initial CCV ± 20% of
True Value; 50% at
the end of the
analytical sequence
Perform instrument
maintenance; recalibtrate if
necessary
Analyst/Supervisor ENV-SOP-MTJL-0081
GC/MS Calibration Blanks (ICB/CCB)Immediately after every CCV
The absolute values
of all analytes must
be < ½ LOQ or <
1/10th the amount
measured in any
sample.
Rinse and reanalyze once. All
samples following the last
acceptable Calibration Blank
must be reanalyzed.
Analyst/Supervisor ENV-SOP-MTJL-0081
GC/MS Tune Prior to ICAL and each 12 hour
period
Specific ion
abundance criteria
of DFTPP from
method
Retune instrument and verify.Analyst/Supervisor ENV-SOP-MTJL-0081
Table 8
Analytical Instrument Calibration
VOCs by 8260 and PNAs by 8270 SIM
Analyte
Reporting
Detection
Limit
LOD
Method
Detection
Limit
ACETONE 0.0113 0.025 0.05
ACROLEIN 0.00254 0.025 0.05
ACRYLONITRILE 0.000671 0.005 0.01
BENZENE 0.0000941 0.0005 0.001
BROMOBENZENE 0.000118 0.0005 0.001
BROMODICHLOROMETHANE 0.000136 0.0005 0.001
BROMOFORM 0.000129 0.0005 0.001
BROMOMETHANE 0.000605 0.002 0.005
N-BUTYLBENZENE 0.000157 0.0005 0.001
SEC-BUTYLBENZENE 0.000125 0.0005 0.001
TERT-BUTYLBENZENE 0.000127 0.0005 0.001
CARBON TETRACHLORIDE 0.000128 0.0005 0.001
CHLOROBENZENE 0.000116 0.0005 0.001
CHLORODIBROMOMETHANE 0.00014 0.0005 0.001
CHLOROETHANE 0.000192 0.002 0.005
2-CHLOROETHYL VINYL ETHER 0.000575 0.025 0.05
CHLOROFORM 0.000111 0.002 0.005
CHLOROMETHANE 0.00096 0.002 0.004
2-CHLOROTOLUENE 0.000106 0.0005 0.001
4-CHLOROTOLUENE 0.000114 0.0005 0.001
1,2-DIBROMOETHANE 0.000126 0.0005 0.001
1,2-DIBROMO-3-CHLOROPROPANE 0.000276 0.002 0.005
DIBROMOMETHANE 0.000122 0.0005 0.001
1,2-DICHLOROBENZENE 0.000107 0.0005 0.001
1,3-DICHLOROBENZENE 0.00011 0.0005 0.001
1,4-DICHLOROBENZENE 0.00012 0.0005 0.001
DICHLORODIFLUOROMETHANE 0.000374 0.002 0.005
1,1-DICHLOROETHANE 0.0001 0.0005 0.001
1,2-DICHLOROETHANE 0.0000819 0.0005 0.001
1,1-DICHLOROETHENE 0.000188 0.0005 0.001
CIS-1,2-DICHLOROETHENE 0.000126 0.0005 0.001
TRANS-1,2-DICHLOROETHENE 0.000149 0.0005 0.001
1,2-DICHLOROPROPANE 0.000149 0.0005 0.001
1,3-DICHLOROPROPANE 0.00011 0.0005 0.001
2,2-DICHLOROPROPANE 0.000161 0.0005 0.001
1,1-DICHLOROPROPENE 0.000142 0.0005 0.001
CIS-1,3-DICHLOROPROPENE 0.000111 0.0005 0.001
TRANS-1,3-DICHLOROPROPENE 0.000118 0.0005 0.001
DI-ISOPROPYL ETHER 0.000105 0.0005 0.001
ETHYLBENZENE 0.000137 0.0005 0.001
HEXACHLORO-1,3-BUTADIENE 0.000337 0.00075 0.0015
ISOPROPYLBENZENE 0.000105 0.0005 0.001
P-ISOPROPYLTOLUENE 0.00012 0.0005 0.001
2-BUTANONE (MEK)0.00119 0.005 0.01
METHYLENE CHLORIDE 0.00043 0.002 0.005
4-METHYL-2-PENTANONE (MIBK)0.000478 0.005 0.01
METHYL TERT-BUTYL ETHER 0.000101 0.0005 0.001
NAPHTHALENE 0.001 0.002 0.005
N-PROPYLBENZENE 0.0000993 0.0005 0.001
STYRENE 0.000118 0.0005 0.001
1,1,1,2-TETRACHLOROETHANE 0.000147 0.0005 0.001
1,1,2,2-TETRACHLOROETHANE 0.000133 0.0005 0.001
TETRACHLOROETHENE 0.0003 0.006 0.012
TOLUENE 0.000278 0.0006 0.0012
1,2,3-TRICHLOROBENZENE 0.00023 0.0005 0.001
1,2,4-TRICHLOROBENZENE 0.000481 0.001 0.002
1,2,3-TRIMETHYLBENZENE 0.000104 0.0005 0.001
1,2,4-TRIMETHYLBENZENE 0.000322 0.001 0.002
1,3,5-TRIMETHYLBENZENE 0.000104 0.0005 0.001
1,1,1-TRICHLOROETHANE 0.000149 0.0005 0.001
1,1,2-TRICHLOROETHANE 0.000158 0.0005 0.001
TRICHLOROETHENE 0.00019 0.0005 0.001
TRICHLOROFLUOROMETHANE 0.00016 0.002 0.005
1,1,2-TRICHLOROTRIFLUOROETHANE 0.00018 0.0005 0.001
1,2,3-TRICHLOROPROPANE 0.000237 0.001 0.0025
VINYL CHLORIDE 0.000234 0.0005 0.001
XYLENES, TOTAL 0.000174 0.0015 0.003
Table 9
VOCs Water Detection Limits
Values in milligrams per liter (mg/L)
Analyte Reporting
Detection Limit LOD MDL
ACETONE 0.0365 0.075 0.15
BENZENE 0.000467 0.001 0.002
BROMOCHLOROMETHANE 0.000564 0.0025 0.005
BROMODICHLOROMETHANE 0.000725 0.0015 0.003
BROMOFORM 0.00117 0.0125 0.025
BROMOMETHANE 0.00197 0.00625 0.0125
CARBON DISULFIDE 0.0007 0.005 0.0125
CARBON TETRACHLORIDE 0.000898 0.0025 0.005
CHLOROBENZENE 0.00021 0.00125 0.0025
CHLORODIBROMOMETHANE 0.000612 0.00125 0.0025
CHLOROETHANE 0.0017 0.005 0.01
CHLOROFORM 0.00103 0.0025 0.005
CHLOROMETHANE 0.00435 0.01 0.02
CYCLOHEXANE 0.00111 0.00125 0.0025
1,2-DIBROMOETHANE 0.000648 0.002 0.004
1,2-DIBROMO-3-CHLOROPROPANE 0.0039 0.0125 0.025
DICHLORODIFLUOROMETHANE 0.00161 0.005 0.01
1,1-DICHLOROETHANE 0.000491 0.00125 0.0025
1,2-DICHLOROBENZENE 0.000425 0.0025 0.005
1,3-DICHLOROBENZENE 0.0006 0.0025 0.005
1,4-DICHLOROBENZENE 0.0007 0.0025 0.005
1,2-DICHLOROETHANE 0.000649 0.002 0.004
1,1-DICHLOROETHENE 0.000606 0.00125 0.0025
CIS-1,2-DICHLOROETHENE 0.000734 0.0015 0.003
TRANS-1,2-DICHLOROETHENE 0.00104 0.0025 0.005
1,2-DICHLOROPROPANE 0.00142 0.005 0.01
CIS-1,3-DICHLOROPROPENE 0.000757 0.002 0.004
TRANS-1,3-DICHLOROPROPENE 0.00114 0.0025 0.005
ETHYLBENZENE 0.000737 0.002 0.004
2-HEXANONE 0.00336 0.0125 0.025
ISOPROPYLBENZENE 0.000425 0.00125 0.0025
2-BUTANONE (MEK)0.0635 0.15 0.3
METHYL ACETATE 0.003 0.0125 0.025
METHYL CYCLOHEXANE 0.00206 0.0025 0.005
METHYLENE CHLORIDE 0.00664 0.015 0.03
4-METHYL-2-PENTANONE (MIBK)0.00228 0.0125 0.025
METHYL TERT-BUTYL ETHER 0.00035 0.00075 0.0015
STYRENE 0.000229 0.00625 0.0125
1,1,2,2-TETRACHLOROETHANE 0.000695 0.002 0.004
TETRACHLOROETHENE 0.000896 0.002 0.004
TOLUENE 0.0013 0.003 0.006
1,2,3-TRICHLOROBENZENE 0.00733 0.015 0.03
1,2,4-TRICHLOROBENZENE 0.0044 0.01 0.02
1,1,1-TRICHLOROETHANE 0.000923 0.002 0.004
1,1,2-TRICHLOROETHANE 0.000597 0.00125 0.0025
TRICHLOROETHENE 0.000584 0.0015 0.003
TRICHLOROFLUOROMETHANE 0.000827 0.002 0.004
1,1,2-TRICHLOROTRIFLUOROETHANE 0.000754 0.002 0.004
VINYL CHLORIDE 0.00116 0.0025 0.005
XYLENES, TOTAL 0.00088 0.00325 0.0065
Table 10
VOCs Soil Detection Limits
Values in milligrams per kilograms (mg/kg)
Analyte/Analyte Group Matrix Method /SOP Container(s) number, size &
type per sample Preservation Preparation
Holding Time
Analytical
Holding Time
Volatile Organic Compounds (VOCs)Soil ENV-SOP-MTJL-0100
(1) 2 ounce jar, (1) 40 Amber
Vial/10ml MeOH MeOH 14 days 14 days
Volatile Organic Compounds (VOCs)Water ENV-SOP-MTJL-0100 (3) 40 ml VOA Vials HCL 14 days 14 days
Table 11
Sample Containers, Preservation, and Holding Times
VOCs by 8260

Appendix A
Pace Laboratory Quality Manual

ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Laurence Hayden Approved on 9/1/2022 1:01:26 PM
Robert Johnson Approved on 8/15/2022 4:06:20 PM
Elizabeth Turner Approved on 9/1/2022 7:55:17 PM
Rebecca King Approved on 9/2/2022 8:32:34 AM
Page 1 of 221
Title Page
Quality Manual
Pace Analytical Services, LLC
Prepared for:
ESC dba Pace® Analytical National Center for Testing and Innovation
12065 Lebanon Road
Mt. Juliet, TN 37122
Phone: [phone]
Parent Company: Pace® Analytical Services, LLC
Signatory Attestation: I attest the application of my electronic signature on this title page affirms my
management commitment and responsibility to uphold the requirements of the PAS Quality Management
System (QMS) described in this Quality Manual (manual) at each location for which this manual is prepared.
Refer to the Quality Manual Signatory Page to view the job title and physical address for each signatory.
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Page 2 of 221
Quality Manual Approval Signatories
The following individuals represent the PAS corporate and local management team responsible for
implementing the PAS Quality Management System (QMS) and upholding the requirements of this
manual at the location(s) for which this manual was prepared, at the time this version of the manual
was made effective, and that correlate with the electronic signatures shown on the title page of this
manual.
If these persons(s) change positions, leave the company, or are on extended leave of absence, the
approval of this manual automatically transfers to the person replacing the signatory or to the
signatory’s primary or alternate deputy until the manager is replaced and/or the manager returns to
work. The individual replacing the signatory automatically accepts the responsibilities associated with
the original signatory’s attestation. Refer to Section 4.1.5.1.1 of this manual for the deputies assigned
to key personnel job titles.
The manual is not revised and released under an updated version for the sole purpose of updating
personnel change(s). Personnel information is updated when the next revision of the manual is
released. See manual Sections 1.2.1 and 1.2.2 for more information about how this manual is
maintained.
Name Job Title Address, City, State, ZIP Phone
Laurence Hayden Vice President of Operations Texas [phone]
Eric Johnson Director of Lab Operations 12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
Elizabeth Turner Quality Program Manager 400 West Bethany Drive, Suite 190
Allen, TX 75013
[phone]
Rebecca King Quality Manager 12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Page 3 of 221
TABLE OF CONTENTS
1.0 PURPOSE AND SCOPE 7
1.1 PURPOSE 7
1.2 SCOPE AND APPLICATION 7
1.2.1 QUALITY MANUAL TEMPLATE 8
1.2.2 QUALITY MANUAL 9
1.2.3 REFERENCES TO SUPPORTING DOCUMENTS 9
2.0 REFERENCES 9
3.0 TERMS AND DEFINITIONS 10
4.0 MANAGEMENT REQUIREMENTS 11
4.1 ORGANIZATION 11
4.1.1 LEGAL IDENTITY 11
4.1.2 COMPLIANCE RESPONSIBILITY 11
4.1.3 SCOPE OF THE QUALITY MANAGEMENT SYSTEM 11
4.1.4 ORGANIZATION HISTORY AND INFORMATION 11
4.1.5 MANAGEMENT REQUIREMENTS 12
4.2 QUALITY MANAGEMENT SYSTEM 18
4.2.1 QUALITY MANAGEMENT SYSTEM OBJECTIVES 18
4.2.2 QUALITY POLICY STATEMENT 20
4.2.3 MANAGEMENT COMMITMENT: QUALITY MANAGEMENT SYSTEM 21
4.2.4 MANAGEMENT COMMITMENT: CUSTOMER SERVICE 21
4.2.5 SUPPORTING PROCEDURES 22
4.2.6 ROLES AND RESPONSIBILITIES 23
4.2.7 CHANGE MANAGEMENT 23
4.3 DOCUMENT CONTROL 23
4.3.1 GENERAL 23
4.3.2 DOCUMENT APPROVAL AND ISSUE 24
4.3.3 DOCUMENT REVIEW AND CHANGE 24
4.4 ANALYTICAL SERVICE REQUEST, TENDER, AND CONTRACT REVIEW 24
4.5 SUBCONTRACTING (INTERNAL AND EXTERNAL) 25
4.6 PURCHASING SERVICES AND SUPPLIES 26
4.7 CUSTOMER SERVICE 26
4.7.1 COMMITMENT TO MEET CUSTOMER EXPECTATIONS 26
4.7.2 CUSTOMER FEEDBACK 26
4.8 COMPLAINTS 27
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Page 4 of 221
4.9 NONCONFORMING WORK 27
4.9.1 DEFINITION OF NONCONFORMING WORK 27
4.10 CONTINUOUS IMPROVEMENT 29
4.11 CORRECTIVE ACTION 29
4.11.1 CAUSE ANALYSIS (AKA ROOT CAUSE ANALYSIS) 30
4.11.2 EFFECTIVENESS REVIEW 30
4.11.3 ADDITIONAL AUDITS 30
4.12 PREVENTIVE ACTION 31
4.12.1 CHANGE MANAGEMENT 31
4.13 CONTROL OF RECORDS 31
4.13.1 GENERAL REQUIREMENTS 31
4.13.2 TECHNICAL RECORDS 33
4.14 AUDITS 34
4.14.1 INTERNAL AUDIT 34
4.15 MANAGEMENT REVIEW 35
4.16 DATA INTEGRITY 36
5.0 TECHNICAL REQUIREMENTS 36
5.1 GENERAL 36
5.2 PERSONNEL 37
5.2.1 PERSONNEL QUALIFICATIONS 37
5.2.2 TRAINING (REQUIRED) 38
5.2.3 PERSONNEL SUPERVISION 42
5.2.4 JOB DESCRIPTIONS 42
5.2.5 AUTHORIZATION OF TECHNICAL PERSONNEL 43
5.3 ACCOMMODATIONS AND FACILITIES 43
5.3.1 FACILITIES 43
5.3.2 ENVIRONMENTAL CONDITIONS 43
5.3.3 SEPARATION OF INCOMPATIBLE ACTIVITIES 43
5.3.4 SECURITY 44
5.3.5 GOOD HOUSEKEEPING 44
5.4 TEST METHODS 44
5.4.1 GENERAL REQUIREMENTS 44
5.4.2 METHOD SELECTION 44
5.4.3 PAS DEVELOPED METHODS 45
5.4.4 NON-STANDARD METHODS 45
5.4.5 METHOD VALIDATION 46
5.4.6 MEASUREMENT UNCERTAINTY 48
5.4.7 CONTROL OF DATA 49
5.5 EQUIPMENT 50
5.5.1 AVAILABILITY OF EQUIPMENT 50
5.5.2 CALIBRATION 50
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Page 5 of 221
5.5.3 EQUIPMENT USE AND OPERATION 51
5.5.4 EQUIPMENT IDENTIFICATION 51
5.5.5 EQUIPMENT LISTS AND RECORDS 51
5.5.6 OUT OF SERVICE PROTOCOL 52
5.5.7 CALIBRATION STATUS 52
5.5.8 RETURNED EQUIPMENT CHECKS 53
5.5.9 INTERMEDIATE EQUIPMENT CHECKS 53
5.5.10 SAFEGUARDING EQUIPMENT INTEGRITY 53
5.6 MEASUREMENT TRACEABILITY 53
5.6.1 GENERAL 53
5.6.2 EQUIPMENT CORRECTION FACTORS 54
5.6.3 SPECIFIC REQUIREMENTS 54
5.6.4 REFERENCE STANDARDS AND REFERENCE MATERIALS 54
5.7 SAMPLING 57
5.7.1 SAMPLING PLANS AND SOPS 57
5.7.2 CUSTOMER REQUESTED DEVIATIONS 57
5.7.3 RECORDKEEPING 57
5.8 SAMPLE MANAGEMENT & HANDLING 57
5.8.1 PROCEDURES 57
5.8.2 UNIQUE IDENTIFICATION 59
5.8.3 SAMPLE RECEIPT CHECKS AND SAMPLE ACCEPTANCE POLICY 59
5.8.4 SAMPLE CONTROL AND TRACKING 61
5.8.5 SAMPLE STORAGE, HANDLING, AND DISPOSAL 61
5.9 ASSURING THE QUALITY OF TEST RESULTS 62
5.9.1 QUALITY CONTROL (QC) PROCEDURES 62
5.9.2 QC CORRECTIVE ACTION 66
5.9.3 DATA REVIEW 67
5.9.4 CALIBRATION CERTIFICATES 68
5.9.5 OPINIONS AND INTERPRETATIONS 68
5.9.6 SUBCONTRACTOR REPORTS 68
5.9.7 ELECTRONIC TRANSMISSION OF RESULTS 69
5.9.8 FORMAT OF TEST REPORTS 69
5.9.9 AMENDMENTS TO TEST REPORTS 69
5.10 REPORTING 69
5.10.1 GENERAL REQUIREMENTS 69
5.10.2 TEST REPORTS: REQUIRED ITEMS 69
5.10.3 TEST REPORTS: SUPPLEMENTAL ITEMS 70
6.0 REVISION HISTORY 71
7.0 APPENDICES 74
7.1 APPENDIX A: CERTIFICATION / ACCREDITATION LISTING 74
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Page 6 of 221
7.1.1 PAS-MT. JULIET 74
7.2 APPENDIX B: CAPABILITY LISTING 75
7.2.1 PAS-MT. JULIET 75
7.3 APPENDIX C: GLOSSARY 160
7.4 APPENDIX D: ORGANIZATION CHART(S) 175
7.4.1 PAS CORPORATE ORGANIZATION CHART(S) 175
7.4.2 PAS QUALITY SYSTEMS MANAGEMENT ORGANIZATION CHART 176
7.4.3 MT. JULIET – ORGANIZATION CHART 177
7.5 APPENDIX E: EQUIPMENT LISTING 182
7.5.1 PAS-MT. JULIET 182
8.0 ADDENDUM: PROGRAM REQUIREMENTS 211
8.1 DOD/DOE 211
8.2 ADDENDUM: AIHA-LAP, LLC 214
8.3 ADDENDUM: SOP REVIEW 216
8.4 ADDENDUM: RADIOLOGICAL REQUIREMENTS 217
8.4.1 ESTIMATE OF ANALYTICAL UNCERTAINTY 217
8.4.2 RADIOLOGICAL EQUIPMENT CALIBRATION 217
8.4.3 MATRIX SPIKE/MATRIX SPIKE DUPLICATE (MS/MSD) 217
8.5 ADDENDUM: QUALITY CONTROL CALCULATIONS 218
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Page 7 of 221
1.0 PURPOSE AND SCOPE
1.1 Purpose
This quality manual (manual) outlines the quality management system (QMS) and management
structure of Pace® Analytical Services, LLC. Pace® Analytical Services, LLC is referred to by brand
name Pace® Analytical Services and by the acronyms PAS or ENV. The acronyms PAS and ENV
are interchangeable.
The PAS QMS is also referred to as the quality program throughout this manual and other PAS
documents. The phrases “quality management system” and “quality program” are synonymous and
are referred to by the acronym QMS.
The QMS is the collection of policies and processes established by the senior leaders of PAS (top
management) to ensure the service and products provided by PAS consistently meet relevant
requirements and achieves the goal of Pace® to provide customers with high quality, cost-effective,
analytical measurements, and services.
The QMS is also planned to establish conformance1 and compliance with the current published
versions of the following international and national quality system standards:
ISO/IEC 17025: General requirements for the competence of testing and calibration laboratories
NELAC/TNI Standard Volume 1: Management and Technical Requirements for Laboratories Performing
Environmental Analysis
1The statement of conformity to these Standards pertains only to testing and sampling activities carried out by the laboratory
at its physical address, in temporary or mobile facilities, in-network, or by laboratory personnel at a customer’s facility.
In addition to the international and national standards, the QMS is planned to achieve regulatory
compliance with the various federal and state programs for which PAS locations provide compliance
testing and/or holds certification or accreditation. Federal or state requirements that do not apply to
all PAS locations, are provided in addendum to this manual or in other documents that supplement
the manual. Customer-specific project and program requirements are not included in the manual in
order to maintain client confidentiality.
A list of accreditation and certifications held by each location associated with this manual is
provided in Appendix A.
A list of analytical testing capabilities offered by each location associated with this manual is
provided in Appendix B.
1.2 Scope and Application
This manual applies to each location listed on the Title Page of this manual, including PAS
laboratories, satellite laboratories, service centers, and supporting business functions.
For purposes of the PAS QMS:
The term “location” used in this manual refers to laboratories and/or service centers.
The term “laboratory” refers to any PAS location, however named by Pace® that provides testing,
collects samples (sampling), or conducts field measurement services in a fixed building, mobile
unit, or in-situ (field).
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The phrase “service center” refers to any PAS location, however named by Pace® that does not
perform any testing, sampling, or field measurements.
The phrase “satellite laboratory” refers to a limited-service laboratory affiliated to a larger business
unit or location. Some PAS business groups, such as accounting, may refer to a satellite laboratory
as a “service center.” Irrespective of internal jargon or reference by any group, any PAS location
that generates a test result for external use is a “laboratory” and must comply with the
requirements specified in this manual for all analytical testing services.
PAS locations are defined by physical address. Laboratories are defined by physical address and
certification/accreditation ID except mobile units which may be defined by the address of the location
to which they are assigned, by VIN (vehicle identification number), or by certification/accreditation
ID. Laboratories that provide sampling and field testing are defined by the physical address of the
PAS location to which they are affiliated and that manages these activities.
1.2.1 Quality Manual Template
This manual was prepared using the PAS Quality Manual Template (template) created by the
PAS Corporate Quality Director (CQD).
The template, known as document ID ENV-TMP-CORQ-0007, specifies the minimum
requirements that every PAS location must abide by, regardless of scope of services or number
of personnel, to maintain a quality program that achieves the objectives of the PAS Quality
Policy (See Section 4.2.2).
The template is the mechanism used by top management to communicate to PAS personnel
their commitment to continuously develop and improve the QMS for effectiveness, to meet
customer expectations, and to comply with any statutory and regulatory requirements. Their
signature of approval on this template is the mechanism used to document this responsibility.
“Top Management” is the phrase used by the TNI Standard to refer to the leaders of an
organization that develop and/or release the PAS Quality Policy Statement and QMS under
their authority
For PAS, these managers include the Chief Executive Officer (CEO) and Chief Compliance
Officer (CCO) of Pace® and the President, CQD, Senior Vice President of Operations (Sr.
VPO), and the Chief Technical Officer (CTO) of PAS.
The template and instructions for use of the template are released by corporate quality
personnel to local quality managers responsible for each location (Local QM). The local QM
uses the template to prepare the location manual by following the instructions provided to
them. The local QM may not alter the font, structure, or content of the template, except where
specified by instruction to do so. As previously stated, program specific requirements unique
to each location are provided in addendum or in documents that supplement the manual.
The template is reviewed by corporate quality personnel annually and updated, if needed. More
frequent review and revision may occur to manage change, to maintain conformance and
compliance to relevant standards or to improve the QMS.
See standard operating procedure (SOP) ENV-SOP-CORQ-00015 Document Management and
Control for more information
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1.2.2 Quality Manual
The quality manual is created from template ENV-TMP-CORQ-0007 by local quality
personnel, who are also responsible for maintenance and management of the document.
PAS locations are not permitted to alter content of the template when preparing their
manual, except where specified in the template. Control of content in the manual is
necessary to ensure consistency of implementation of the PAS quality program across the
network.
If additions or changes to the manual are needed to maintain regulatory compliance or
conformance to relevant standards and these changes cannot be covered by addendum to
the manual, the need for change must be raised to the PAS Corporate Quality Director,
who will decide how to resolve the need.
The manual is approved for release by the management team listed on the Quality Manual
Approval Signatory Page. The manager’s electronic signature on the Title Page of the manual
affirms their commitment to implement and uphold the requirements, processes, and
procedures of the PAS QMS at each location for which the manual was prepared.
The manual is reviewed annually and updated with each release of a new version of the
template, and as needed to update appendices and addendum. More frequent review and
revision may be necessary when there are significant changes to the capabilities, and resources
of the laboratory during the calendar year
See SOP ENV-SOP-CORQ-00015 Document Management and Control for more information.
1.2.3 References to Supporting Documents
The template and the manual include references to other organization documents that support
the QMS such as policies and standard operating procedures (SOPs).
These references may include the document’s document control number (DC#) and the
document title. This information is subject to change at the discretion of PAS. The manual
and/or template are updated to reflect the editorial change during the manual’s next scheduled
review/revision cycle or the next time a version of the manual is released, whichever is sooner.
Each location maintains a current list of documents used by the location to support the QMS.
This list, known as the “Master List”, is readily available to personnel for their use and it
provides a cross reference to the legacy document ID, where applicable. Parties external to
PAS may contact the location of interest to obtain the most current version of the Master List
for their use as needed.
2.0 REFERENCES
References used to prepare this manual include:
“Guidelines Establishing Test Procedures for the Analysis of Pollutants Under the Clean Water Act.”
Federal Register, 40 CFR Part 136, most current version.
“Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods.” SW-846.
“Methods for Chemical Analysis of Water and Wastes,” EPA 600-4-79-020, 1979 Revised 1983, U.S.
EPA.
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U.S. EPA Contract Laboratory Program Statement of Work for Organic Analysis, current version.
U.S. EPA Contract Laboratory Program Statement of Work for Inorganic Analysis, current version.
“Standard Methods for the Examination of Water and Wastewater.” Current Edition APHA-AWWA-
WPCF.
“Annual Book of ASTM Standards,” Section 4: Construction, Volume 04.04: Soil and Rock; Building
Stones, American Society of Testing and Materials.
“Annual Book of ASTM Standards,” Section 11: Water and Environmental Technology, American
Society of Testing and Materials.
“NIOSH Manual of Analytical Methods,” U.S. Department of Health and Human Services, National
Institute for Occupational Safety and Health, most current version.
“Methods for the Determination of Organic Compounds in Finished Drinking Water and Raw Source
Water,” U.S. EPA, Environmental Monitoring and Support Laboratory – Cincinnati (Sep 1986).
Quality Assurance of Chemical Measurements, Taylor, John K.; Lewis Publishers, Inc. 1987.
Methods for Non-conventional Pesticides Chemicals Analysis of Industrial and Municipal Wastewater,
Test Methods, EPA-440/1-83/079C.
Environmental Measurements Laboratory (EML) Procedures Manual, HASL-300, US DOE, February
1992.
Requirements for Quality Control of Analytical Data, HAZWRAP, DOE/HWP-65/R1, July 1990.
Quality Assurance Manual for Industrial Hygiene Chemistry, AIHA, most current version.
National Environmental Laboratory Accreditation Conference (NELAC) Standard- most current
version.
ISO/IEC 17025, General requirements for the competence of testing and calibration laboratories, 2nd
Edition 2005-05-15; 3rd Edition 2017-11
The following are implemented by normative reference to ISO/IEC 17025:
o ISO/IEC Guide 99, International vocabulary of metrology –Basic and general concepts and associated terms
o ISO/IEC 17000, Conformity assessment – Vocabulary and general principles
Department of Defense Quality Systems Manual (QSM), most current version.
TNI (The NELAC Institute) Standard, 2009 and 2016 versions.
UCMR Laboratory Approval Requirements and Information Document, most current version.
US EPA Drinking Water Manual, most current version.
3.0 TERMS AND DEFINITIONS
Refer to Appendix C for terms, acronyms, and definitions used in this manual and in other documents
used by PAS to support the QMS.
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4.0 MANAGEMENT REQUIREMENTS
4.1 Organization
4.1.1 Legal Identity
Pace® Analytical Services, LLC (Pace® Analytical Services) is the responsible entity
authorized by the State of Minnesota to do business as a limited liability company, under the
parent company, PAS Parent, Inc.
4.1.1.1 Change of Ownership
If there is a change of ownership, if a location goes out of business, or if the entire
organization ceases to exist, PAS management is responsible to notify regulatory
authorities of the change within the timeframe required by each state agency for which
the location is certified or accredited.
Requirements for records and other business information are addressed in the
ownership transfer agreement or in accordance with appropriate regulatory
requirements, whichever takes precedence.
4.1.2 Compliance Responsibility
PAS management has the responsibility and authority to establish and implement procedures
and to maintain resources necessary to assure its activities are carried out in such a way to meet
the federal and statutory requirements in addition to the requirements of the PAS QMS. Also
See Section 1.1.
4.1.3 Scope of the Quality Management System
The QMS applies to work carried out at each location covered by this manual including
permanent facilities, at sites away from its permanent facilities, or in associated temporary or
mobile facilities.
The permanent and mobile facilities to which this manual applies are listed on the Title Page
of this manual.
4.1.4 Organization History and Information
Founded in 1978, Pace® Analytical Services, LLC (PAS) is a privately held scientific services
firm operating one of the largest full-service contract laboratory and service center networks
in the United States.
The business purpose of PAS is to deliver the highest standard of testing and scientific services
in the market. We offer the most advanced solutions in the industry, backed by transparent
data, a highly trained team, and the service and support that comes from over four decades of
experience.
4.1.4.1 Organization Structure
Each PAS location is led by a management team referred to as local management1.
Local management is responsible for making day-to-day decisions regarding the
operations of the facility and implementing, and sustaining the requirements, policies,
and procedures of the PAS quality program.
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The roles that make up the local management team include a Vice President of
Operations (VPO), a General Manager (GM) or Director of Laboratory Operations
(DLO), a Quality Program Manager (QPM), and the Quality Manager (QM).
1 The term “local management” does not mean “on-site” management. Some of the
roles that make up the local management team, work off site or from a different PAS
location. Refer to the Quality Manual Approval page at the beginning of this manual
for the physical address of each manager that comprises the local management team.
The local management team is supported by department specific supervisors and in
some PAS locations, a site supervisor or operations manager.
Local management and supervisors are supported by personnel from functional
groups that support the division, such as HR, IT, Sales & Marketing, Finance, and
EHS (Environmental Health & Safety).
Technical oversight for each location is provided by local personnel with support and
guidance from the PAS Chief Technical Officer (CTO), PAS corporate quality
personnel, and the Pace® compliance team. Locations that hold TNI accreditation,
also have personnel appointed to serve as the “acting technical manager for TNI,
however named” to perform the duties and responsibilities of this designation per the
TNI Standard. See Section 4.1.5.2.1 for more information on this TNI requirement.
The reporting relationships and responsibilities of quality personnel are independent
of operations in order to safeguard impartiality. See Section 4.1.5.2 for more
information.
Refer to the organization charts provided in Appendix D to view the organization
structure, reporting relationships, and the interrelationships between positions.
4.1.5 Management Requirements
4.1.5.1 Personnel
Each PAS location is staffed with administrative and/or technical personnel who
perform and verify work under the supervision of their direct line supervisor.
All personnel are expected to perform their duties in accordance with the policies and
processes outlined in this manual and in accordance with standard operating
procedures (SOPs) and other quality system documents. PAS policies and procedures
are designed for impartiality and integrity. When these procedures are fully
implemented, personnel remain free from undue pressure and other influences that
adversely impact the quality of their work or data.
4.1.5.1.1 Key Personnel
Key personnel are management positions that have the authority and
responsibility to plan, direct, and control activities related to the
QMS for the entire division (PAS Corporate), or for one or more
PAS locations (Local).
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PAS Key Personnel Positions & Deputy Assignments by Role
Job Title Acronym Primary / Alternate Deputy
Chief Executive Officer CEO President
Chief Compliance Officer CCO CQD
President NA CEO / Sr. VPO
Corporate Quality Director CQD CCO
Quality Program Manager QPM CQD / Peer QPM
Chief Technical Officer CTO CQD / CCO
Sr. VP of Operations Sr. VPO President / VPO
Vice President of Operations VPO Sr. VPO / Peer VPO
Director of Lab Operations1 DLO VPO / Peer GM or Sr. VPO
Health and Safety Director NA CCO
IT Director NA CTO
Quality Manager QM Direct QPM / Peer QPM
General Manager1 GM VPO / Sr. VPO or Peer GM
Operations Manager1 OM GM / DL or VPO
Technical Manager1 TM CTO / Peer TM
TNI Approved TM2 TNI TM Another Qualified Employee
1:Position is not in place at all locations.
2: The TNI TM is not a PAS position. See Section 4.1.5.2.1 for more information.
Some certification and accreditation programs require notification
when there is a change in key personnel. Notification requirements
and timeframes by agency, are tracked and upheld by the local QM,
when these requirements apply.
4.1.5.2 Roles and Responsibilities
The qualifications, duties, and responsibilities for each position at Pace® are detailed
in job descriptions maintained by the Pace® Human Resource personnel (HR).
The following sections provide a general overview of various management and
supervisory roles and are presented in no particular order.
Chief Executive Officer (CEO): Provides leadership for overall operations;
oversight of regulatory and compliance standards; development of growth strategies;
and long-range capital and strategic planning for Pace®.
Chief Compliance Officer (CCO): Has overall responsibility for statutory and
regulatory compliance and the environmental health and safety programs (EHS) for
Pace®.
President: Provides leadership for overall operations; oversight of regulatory and
compliance standards; development of growth strategies; and long-range capital and
strategic planning for PAS.
Chief Technical Officer (CTO): Provides technical oversight and leadership to all
PAS locations. Responsible for innovation and standardization of technical activities.
Corporate Director of Quality (CQD): Responsible for developing the PAS quality
program and the policies and procedures that support the QMS. The CQD leads the
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quality team, establishing functions, responsibilities, duties, and organization structure
for PAS.
Corporate Quality Program Manager (QPM): Responsible for helping local
management implement, monitor, maintain and improve the PAS quality program for
one or more locations in the network and for direct supervision of Quality
Manager(s).
Director of Information Technology: Oversees and delivers the systems and
processes of information technology used by PAS. These systems include Laboratory
Information Management Systems (LIMS); data acquisition, reduction, and reporting
software; virus-protection, communication tools, and ensuring the integrity, security
of electronic data, and associated policies and procedures.
Sr. Vice President of Operations (Sr VPO): Provides leadership, direction, and
insight necessary to achieve strategic initiatives. Develops and improves processes,
structure, and allocation of resources for operations for all of PAS.
Vice-President of Operations (VPO): Provides leadership, guidance, and
resources, including allocation of personnel, necessary to achieve the strategic goals
of the organization and the PAS quality program to one or more PAS locations.
Director of Laboratory Operations (DLO): See description for General Manager.
General Manager (GM): The GM is responsible for overall administration and
operation of one or more PAS locations and service centers. Although task duties
associated with this responsibility may be delegated, the GM is responsible for
ensuring all duties and activities of the locations they oversee comply with the PAS
QMS, the PAS EHS program, and with any applicable statutory, regulatory
requirements or program requirements.
Any GM of a NELAC/TNI Accredited laboratory is also responsible for the
designation of technical personnel to serve as acting technical managers for TNI for
the fields of accreditation held by the laboratory (See Section 4.1.5.2.1) and for
notifying the accreditation body (AB) of any extended absence or reassignment of
these designations.
Quality Manager (QM): The QM oversees and monitors the implementation,
compliance, and improvement of the QMS and communicates gaps, deviations, and
opportunities for improvement to local and corporate laboratory management. The
QM is independent of the operation and analytical activities for which they provide
oversight and has the authority to carry out the roles and responsibilities of their
position without outside influence.
The QM:
serves as the focal point for QA/QC protocol decisions and oversees review of
QC data for trend analysis;
evaluates data objectively and performs assessments without outside influence;
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has documented training and experience in QA/QC procedures and the PAS
quality system;
has a general knowledge of the analytical methods offered by the laboratory;
coordinates and conducts internal systems and technical audits;
notifies laboratory management of deficiencies in the quality system;
monitors corrective actions;
provides support to technical personnel and may serve as the primary deputy for
the acting TNI Technical Manager(s).
Manager-Client Services (CSM): This position is responsible for the training and
supervision of project manager(s) and/or shipping, receiving and courier personnel.
The primary responsibility of the CSM is to ensure projects are successfully managed
to meet the expectations and needs of PAS customers.
Department Managers / Supervisors / Team Lead): These positions are
responsible for administrative and operations management and implementation of
the QMS in the work area he/she oversees. These responsibilities include but are not
limited to: training and supervision of personnel, monitoring work activity to maintain
compliance with this manual, SOPs, policies and other instructional documents that
support the QMS; method development, validation and the establishment and
implementation of SOPs to assure regulatory compliance and suitability for the
intended purpose; monitoring QA/QC performance, proper handling and reporting
of nonconforming work, purchasing of supplies and equipment adequate for use,
maintaining instrumentation and equipment in proper working order and calibration,
and general maintenance of administrative and technical processes and procedures
established by the laboratory.
Operations Manager (OM): The OM is responsible for management of production
and/or other duties assigned by the GM.
4.1.5.2.1 Approved Technical Manager (TNI Accreditation Only):
The requirements in this subsection apply to only to PAS locations
that are NELAC/TNI accredited.
The TNI Standard specifies requirements for the qualification and
duties of technical personnel. The TNI Standard lists these duties
under the reference “technical manager(s), however named.”
At PAS, these duties closely correlate with the responsibilities and
duties outlined in the PAS job descriptions for managers,
supervisors, team leads, and/or scientist. However, these duties do
not need to be associated with any specific job title and can be
assigned to any one or more PAS employees that meets the
qualifications specified in the TNI Standard.
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Refer to the applicable version of the TNI Standard to view the
required qualifications for each discipline.
PAS locations that are TNI accredited must designate one or more
employees to perform these duties and submit these qualifications
to the TNI accreditation body (AB) for approval.
Employees approved by the TNI AB, to perform these duties retain
their Pace® assigned job title.
When TNI Accreditation Bodies (AB) refer to these employees as
‘technical manager’ or ‘technical director’ on the official certificate
or the scope of accreditation, this reference is referring to their
approval to perform duties of the ‘technical manager, however
named’ as specified in the TNI Standard and not to a PAS job title.
The duties of any approved technical manager for TNI, however
named, can be completed in person or remotely. If an employee that
is an approved technical manager for TNI is completely absent from
work or on a leave of absence for more than 15 calendar days, the
duties and responsibilities specified in the TNI Standard are
temporarily reassigned to another employee that meets the
qualifications for the technology or field of accreditation. If the
employee’s absence exceeds 35 calendar days, the local QM must
formally notify the TNI primary AB of the absence and the details
of reassignment of duties in writing.
4.1.5.3 Conflict of Interest
A conflict of interest is a situation where a person has competing interests that may
affect impartiality. It is the policy of Pace® to ensure business relationships, decisions
and transactions do not place personal interest ahead of the organization, customers,
colleagues, job responsibilities or the public we serve. Conflict of interest is avoided
by making personnel aware of circumstances that conflict or appear to conflict with
impartiality and/or designing process and procedures to include checks and balances
to prevent conflict and ensure impartiality.
See the current version of policy COR-POL-0004 Code of Ethics and Professional Conduct
for more information.
4.1.5.4 Confidentiality
PAS management is committed to preserving the confidentiality of Pace® customers
and confidentiality of Pace® business information.
Client information obtained or created during work activities is considered
confidential and is protected from intentional release to any person or entity other
than the client or the client’s authorized representative, except when Pace® is
required by law to release confidential information to another party, such as a
regulatory agency or for litigation purposes. In which case, Pace® will notify the client
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of the release of information and the information provided, unless notification is
prohibited by law.
When Pace® obtains information about the customer from a source other than the
customer, Pace® will keep the source of the information confidential unless
disclosure is agreed upon by the source.
The terms of client confidentiality are included in PAS Standard Terms and
Conditions (T&C). With the acceptance of the T&C and/or the implicit contract for
analytical services that occurs when the client sends samples to PAS for testing, the
client authorizes Pace® to release confidential information when required. Other
procedures used by PAS to maintain confidentiality include:
A Code of Ethics and Professional Conduct policy that covers this topic (COR-
POL-0004):
A Confidentiality Agreement which supervisory and sales personnel and other
positions are required to sign at the time of employment and abide by the
conditions of throughout employment;
Record retention and disposal procedures that assure confidentiality is
maintained;
Physical access controls and encryption of electronic data; and
See policy COR-POL-0004 Code of Ethics and Professional Conduct for more information.
4.1.5.5 Communication
Communication is defined as the imparting or exchanging of news and information.
Effective (good) communication occurs when the people included in the
communication gets the point and understands it.
4.1.5.5.1 Workplace Communication
Effective communication in the workplace is necessary to assure
work is performed correctly, efficiently, and in accordance with
client specifications.
Instructions for how to conduct testing and other work activities are
communicated to personnel via written policies, standard operating
procedures, and other work instructions.
Information about PAS performance (positive and negative) and
ideas for improvement are communicated to personnel using various
communication channels such as face to face meetings, video
conferencing, conference calls, email, memoranda, written reports,
and posters.
4.1.5.5.2 External Communication
Communication with external parties such as customers, vendors,
business partners, and regulatory agencies takes place every day.
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PAS management is responsible for training personnel to
communicate in professional and respectful ways to build strong
relationships and to avoid misunderstanding.
4.2 Quality Management System
4.2.1 Quality Management System Objectives
The objectives of the PAS QMS are to provide clients with consistent, exemplary professional
service, and objective work product that is of known and documented quality that meets their
requirements for data usability and regulatory compliance.
Objective work product is analytical services, data, test results, and information that is not
influenced by personal feeling or opinions. The quality of being objective is also known as
‘impartiality.’
4.2.1.1 Impartiality
PAS achieves and maintains impartiality by establishing an organizational structure
that safeguards impartiality (See 4.1.4.1) and implementing and adhering to the
policies and processes of the QMS outlined in this manual, which are based on
industry accepted standards and methodologies.
PAS procedures for handling nonconforming work (See 4.9), corrective and
preventive actions (See 4.11, 4.12) and management review (See 4.15) are the primary
mechanisms used to identify risk to impartiality and to prompt actions necessary to
eliminate or reduce the threat when risk to impartiality is suspected or confirmed.
4.2.1.2 Risk and Opportunity Assessment
Risks are variables that make achieving the goals and objectives of the QMS uncertain.
An opportunity is something that has potential positive consequences for the
organization.
PAS personnel manage risks and opportunities on a daily basis by following policies,
procedures and processes that support the QMS. Some ways in which the QMS is
designed to identify, minimize, or eliminate risk on a daily basis include but are not
limited to:
Capability and capacity reviews of each analytical service request to assure the
laboratory can meet the customer’s requirements;
Maintenance of accreditation and certification for test methods in multiple states
and programs to cover a broad range of jurisdiction for regulatory compliance;
SOPs and other controlled instructional documents are provided to personnel to
eliminate variability in the process. These documents include actions to counter
risk factors inherent in the process and are reviewed on a regular basis for on-
going suitability and relevancy;
Participation in proficiency testing programs and auditing activities to verify on-
going competency and comparability in performance;
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Provision of on-the-job training and established protocol for quality control (QC)
corrective action for nonconforming events;
An established program for ethics, and data integrity;
Tiered data review process;
Culture of continuous improvement;
Monitoring activities to assess daily and long-term performance; and
Annual critical review of the effectiveness of the QMS.
PAS also promotes a continuous improvement culture based on the principles of lean
manufacturing. These principles include 3P (Process, Productivity, Performance) and
Kaizen. 3P is a platform used by PAS to share best practices and standardization
across the network to achieve operational excellence. Kaizen is a team-based process
used to implement tools and philosophies of lean to reduce waste and achieve flow
with the purpose of improving both external and internal customer satisfaction. The
PAS lean program and activities help to mitigate risk because they generate a collective
understanding of vulnerabilities and utilize group-effort to develop and implement
solutions at all levels.
Risk and opportunities may also be formally identified using specific risk and
opportunity assessment methods such as SWOT Analysis (Strength, Weakness,
Opportunity, Threats) and 3-Stage Impact/Probability Grids.
4.2.1.3 Communication of the Quality Management System
This manual is the primary mechanism used by PAS management to communicate
the QMS to personnel.
To assure personnel understand and implement the quality program outlined in the
manual:
PAS personnel are required to sign a Read and Acknowledgement Statement to
confirm the employee has:
1) been informed of the manual by management,
2) has access to the manual,
3) has read the manual
4) understands the content of the manual, and
5) agrees to abide by the requirements, policies, and procedures therein.
Personnel are informed that the manual provides the “what” of the QMS. The
“how to” implementation of the QMS is provided in policy, SOPs, standard work
instructions, and other instructional documents.
This manual and supporting policies and procedures are made readily accessible
to personnel in the area where the work activity is performed.
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4.2.2 Quality Policy Statement
The quality policy of PAS is to provide customers with data of known and
documented quality fit for their intended purpose. PAS achieves this policy by
implementing the QMS defined in this manual, by following industry accepted
protocol for analytical testing and quality assurance and quality control (QA/QC)
activities, by conformance with published and industry accepted testing
methodologies, and by compliance with international and national standards for the
competency and/or accreditation of testing laboratories.
Intrinsic to this policy statement is each of the following principles:
PAS will provide customers with reliable, consistent, and professional service.
This is accomplished by making sure each PAS location has the resources
necessary to maintain capability and capacity; that staff are trained and competent
to perform the tasks they are assigned; that client-facing staff are trained and
prepared to find solutions to problems and to assist customers with their needs
for analytical services. Customer feedback, both positive and negative, is shared
with personnel and used to identify opportunities for improvement.
PAS maintains a quality program that complies with applicable state, federal, and
industry standards for analytical testing and competency.
PAS management provides training to personnel so that all personnel are familiar
with the QMS outlined in this manual and that they understand that
implementation of the QMS is achieved by adherence to the Pace® and PAS
policies and procedures.
PAS management continuously evaluates and improves the effectiveness of the
QMS by responding to customer feedback, and other measures of performance,
such as but not limited to the results of internal/external audits, proficiency
testing, metrics, trend reports, and annual and periodic management reviews.
4.2.2.1 Ethics Policy / Data Integrity Program
Pace® has established a comprehensive ethics and data integrity program that is
communicated to all Pace® employees so that they understand what is expected of
them. The program is designed to promote a mindset of ethical behavior and
professional conduct that is applied to all work activities.
The key elements of the Pace® Ethics / Data Integrity Program include:
Ethics Policy (COR-POL-0004);
Ethics Officer (Chief Compliance Officer);
Standardized data integrity training course taken by all new employees on hire
and a yearly refresher data integrity training course for all existing employees;
Policy Acknowledgement Statements that all Pace® personnel, including contract
and temporary, are required to sign at the time of employment and again during
annual refresher training to document the employee’s commitment and
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obligation to abide by the company’s standards for ethics, data integrity and
confidentiality;
SOPs that provide instructions for how to carry out a test method or process to
assure tasks are done correctly and consistently by each employee;
On the Job Training;
Data integrity monitoring activities which include, but are not limited to, primary,
secondary and completeness data reviews, internal technical and system audits,
data audits, data surveillance, and proficiency testing; and
Confidential reporting process for alleged ethics and data integrity issues.
All PAS managers and supervisors are expected to provide a work environment where
personnel feel safe and can report unethical or improper behavior in complete
confidence without fear of retaliation. Retaliation against any employee that reports a
concern is not tolerated.
Pace® has engaged Lighthouse Services, Inc. to provide personnel with an
anonymous reporting process available to them 24 hours a day/7 days per week. The
alert line may be used by any employee to report potential violations of the company’s
ethics and data integrity program. Reports are forwarded to the Pace® Ethics
Compliance Officer to investigate and resolve the matter. Investigations concerning
data integrity are kept confidential.
See COR-POL-0001 Compliance Alertline for more information.
Posters and flyers with the compliance alert line information must be prominently
posted in each PAS location for personnel reference.
Compliance Alert Line Information:
English Speaking US & Canada [phone]
Spanish Speaking North America [phone]
Internet www/lighthouse-services.com/pacelabs
Email [e-mail]
4.2.3 Management Commitment: Quality Management System
Evidence of management’s commitment for the development, maintenance, and on-going
improvement of the QMS is provided by the application of their signature of approval to the
template and/or manual. Their signature confirms they understand their responsibility to
implement the QMS outlined in this manual, to communicate the quality program to
personnel, and to uphold requirements of the program during work activities.
4.2.4 Management Commitment: Customer Service
Management communicates the importance of meeting customer and regulatory requirements
to personnel by training personnel on the QMS outlined in this manual, implementing the
QMS outlined in this manual, and upholding these requirements for all work activities.
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4.2.5 Supporting Procedures
References to processes and procedures that support the QMS are included throughout this
manual. The structure of the document management system is outlined in SOP ENV-SOP-
CORQ-0015 Document Management and Control and summarized in the following subsections.
4.2.5.1 Quality Management System Document Structure
Documents associated with the QMS are classified into document types that identify
the purpose of the document and establish how the document is managed and /or
controlled.
Examples: Types of PAS Internally Created Documents
Document Type Purpose
Quality Manual Outlines the PAS QMS and structure and how it works for a system
including policy, goals, objectives and detailed explanation of the system and
the requirements for implementation of system. Includes roles and
responsibilities, relationships, procedures, systems, and other information
necessary to meet the objectives of the system described.
Policy Provide requirements and rules for a process and is used to set course of
actions and to guide and influence decisions. Policy describes the “what,”
not the “how”.
Standard Operating
Procedure
Provide written and consistent set of instructions or steps for execution of a
routine process, method, or set of tasks performed. Assures that activities
are performed properly in accordance with applicable requirements.
Standard Work
Instruction
Provide step by step visual and/or written instruction to perform a specific
task to improve competency, minimize variability, reduce work injury and
strain, or to boost efficiency and quality of work (performance). SWI are
associated with an SOP unless the task described is unrelated to generation
of or contribution to environmental data or analytical results.
Template Pre-formatted document that serves as a starting point for a new document.
Guide Assists users in using a particular product; or a technical interpretation of a
method or process by which PAS locations must abide.
Form Used for a variety of purposes such as to provide a standardized format to
record observations, to provide information to supplement an SOP.
Guidance Non-binding advice used to explain internal policies, procedures, or
practices.
Example: Types of External Documents used by PAS
Certificate Lists parameters, methods, and matrices for which the location is
certified/accredited to perform within the jurisdiction of the issuing
regulatory agency or accreditation body.
Reference
Document
Provide information, protocol, instructions, and/or requirements. Issued by
the specifier. Examples include ISO/IEC, TNI, DoD and published
referenced methods such as Standard Methods, ASTM, SW846, EPA, and
federal and state regulatory bodies.
Project Document Provides requirements necessary to meet individual client expectations for
intended use of data. Examples include project quality assurance plans
(QAPP), client-program technical specifications, contracts, and other
agreements.
These document types are ranked to establish which documents takes precedence
when there is an actual or perceived conflict between documents and to establish the
hierarchal relationships between documents. The ranking system also provides
information to document writers and reviewers to assure downline documents agree
with documents of higher rank.
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PAS Document Hierarchy
Rank Document
1 Corporate Manual
2 Corporate Policy
3 Corporate SOP
4 Corporate SWI, Templates, Guides, Forms, Guidance
5 Local Manual
6 Local SOP
7 Local SWI, Templates, Guide, Forms, Guidance
Information and requirements from project documents are not incorporated into PAS
policy or SOPs in order to maintain client confidentiality. These documents are
managed as external documents and any requirements for work specified is followed
when work for the project is performed. Project Documents are reviewed and
maintained as part of the contract/incoming work review process (See Section 4.4).
If the project document is less stringent than the PAS QMS, policies, or SOPs, and/or
is less stringent than applicable federal or state requirements, PAS locations are still
required to meet the minimum requirements of the PAS QMS and any applicable
statutory or federal requirements in addition to the requirements specified in the
project document.
Reference documents are not ranked because all PAS created documents, processes
and procedures must be consistent with the applicable reference document(s) in
addition to higher-ranking PAS documents.
See SOP ENV-SOP-CORQ-0015 Document Management and Control for more
information.
4.2.6 Roles and Responsibilities
The roles and responsibilities for technical management and the quality manager is provided
in section 4.1.5.2.
4.2.7 Change Management
When significant changes to the PAS QMS are planned, these changes are managed by
corporate quality personnel to assure that the integrity of the QMS is maintained.
4.3 Document Control
4.3.1 General
PAS procedures for document control are provided in SOP ENV-SOP-CORQ-0015 Document
Management and Control.
PAS locations use electronic document management software (eDMS) to perform the
document control procedures of the SOP. This system provides centralized access to all
documents used by PAS locations across the network. All PAS locations are required to use
the eDMS system established for PAS (presently Qualtrax) unless an exemption has been
granted by the PAS Corporate Quality Director.
eDMS automates the process for unique document identification, version control, approval,
access, and archival and restricts access to archived documents except to authorized users to
prevent the use of obsolete documents.
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The local QM maintains a master list of controlled documents used at each location. The
master list minimally includes the document control number, document title, and current
revision status and is made available to personnel for their reference.
See SOP ENV-SOP-CORQ-0015 Document Management and Control for more information.
4.3.2 Document Approval and Issue
Documents that support the QMS are reviewed by qualified personnel and approved by
management prior to release for use.
Only the approved versions of documents are available to personnel for use unless use of a
draft document is authorized by management.
The managers responsible for authorization of each document is situation specific.
See SOP ENV-SOP-CORQ-0015 Document Management and Control for more information.
4.3.3 Document Review and Change
Unless a more frequent review is required by regulatory, certification or accreditation program
documents are reviewed at least every two years to ensure the documents remains current,
appropriate, and relevant.
Documents are also informally reviewed every time the document is used. Personnel are
expected to refer to and follow instructions in controlled documents when they conduct their
work activities. Consequently, any concerns or problems with the document should be caught
and brought to the attention of management on an on-going basis.
Documents are revised whenever necessary to ensure the document remains usable and
correct. Older document versions and documents no longer needed are made obsolete and
archived for historical purposes.
PAS does not allow hand-edits to documents. If an interim change is needed pending re-issue
of the document, the interim change is communicated to those that use the document using a
formal communication channel, such as change in progress form, email, or memorandum.
The document review, revision, and archival process is managed by quality personnel at the
location from which the document was released using the procedures established in SOP
ENV-SOP-CORQ-0015 Document Management and Control.
4.4 Analytical Service Request, Tender, and Contract Review
PAS management and/or client service personnel perform thorough reviews of requests and contracts
for analytical services to verify the location(s) performing the work has the capability, capacity, and
resources necessary to successfully meet the customer’s needs. These review procedures are described
in SOP ENV-SOP-MTJL-0009, Contract Review.
The procedures in this SOP(s) are established to ensure that:
The PAS locations performing the work understand the purpose of data collection in order to
ensure the test methods requested are appropriate for the intended use of the data and capable
of meeting the client’s data quality objectives;
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PAS locations and any external subcontractor(s) have the capability, capacity, and resources to
meet the project requirements and expectations within the requested time frame for delivery of
work product;
Any concerns that arise from review are discussed and resolved with the client;
Any discrepancies between the PAS QMS, statutory or regulatory requirements and the client
request are resolved; and
The results of review and any correspondence with the client related to this process and/or any
changes made to the contract are recorded and retained for historical purposes.
Capability review confirms that the PAS locations contracted to perform the work and any internal
or external subcontractors hold required certification/accreditation for the test method, matrix, and
analyte and verifies the location can achieve the client’s target compound list and data quality
objectives (DQOs) for analytical sensitivity and reporting limits, QA/QC protocol, and hardcopy test
report and electronic data deliverable (EDD) formats.
Capacity review verifies that the in-network locations and any potential subcontractors are able to
manage the sample load and deliver work production within the delivery timeframe requested.
Resource review verifies that the location and any potential subcontractors have adequate qualified
personnel with the skills and competency to perform the test methods and services requested and
sufficient and proper equipment and instrumentation needed to perform the services requested.
4.5 Subcontracting (Internal and External)
The terms ‘subcontract’ and “subcontracting” refers to analytical work done by an organization
external to Pace® (External Subcontracting) or by a Pace® location with an address different than
the address listed on the cover page of the test report (Internal Subcontracting).
The PAS network offers comprehensive analytical capability and capacity to ensure Pace® can meet
a diverse range of client needs for any type of project. If a PAS laboratory receives a request for
analytical services and it cannot fulfill the project specifications, the location’s client services team will
collaborate with the client to place the work within the PAS network.
When it is not possible to place the work within network, the location will, with documented client
approval, subcontract the work to a subcontractor that has the capabilities to meet the project
specifications and can meet the same commitment agreed on between the location and the client.
Whenever work is subcontracted, the PAS location responsible for management of the project verifies
each of these qualifications:
The internal or external subcontractor has the proper accreditation/certifications required for the
project and these are current; and
The use of the internal or external subcontractor is approved by the client and/or regulatory
agency when such approval is required by the customer. Record of customer approval is retained
in the project record.
External subcontractors selected by Pace® must be pre-qualified by quality personnel to verify their
QMS is similar to Pace® and complies with all relevant Standards such, as ISO/IEC 17025 and the
TNI Standard(s) and/or federal and state regulatory requirements. The list of approved
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subcontractors for each location is maintained by local quality personnel. Pre-qualification of a
subcontractor does not eliminate the requirement for the PAS location placing work to verify the
subcontractor has the certifications, capability, capacity, and resources to perform work on behalf of
Pace® on a project-specific basis.
For all subcontracted work, the PAS location placing the work internally or externally is responsible
to ensure project specifications are always communicated to and understood by the subcontractor.
4.6 Purchasing Services and Supplies
Vendors that provide services and supplies to PAS are qualified to meet the needs of Pace®. These
needs include but are not limited to competitive pricing, capacity to fill purchase orders, quality of
product, customer service, and business reputation and stability. Evidence of this qualification is the
availability to purchase services and supplies from the vendor in the corporate purchasing system.
PAS locations may purchase goods and services from any supplier in the purchasing system.
The specifications (type, class, grade, tolerance, purity, etc.) of supplies, equipment, reagents, standard
reference materials and other consumables used in the testing process are specified in SOPs. The SOP
specifications are based on the governing requirements of the approved reference methods and any
additional program driven regulatory specification, such as drinking water compliance.
All requisitions for materials and consumables are approved by local management who is responsible
to ensure the services and supplies procured and received are fit for intended use.
4.7 Customer Service
Project details and management is managed by PAS client services personnel.
4.7.1 Commitment to Meet Customer Expectations
PAS personnel collaborate closely with our customers to ensure their needs are met and to
establish their confidence in the capability of PAS to meet their needs for analytical services
and expectations for service.
The project manager (PM) is the customer’s primary point of contact for each analytical service
request (work order). The PM gathers information from the customer to ensure the details of
their request are understood. After samples are received, the PM monitors the progress of the
project and alerts the customer of any delays or excursions that may adversely impact data
usability. Supervisors are expected to keep the PM informed of project status and any delays
or key issues, so that the PM can keep the client informed.
PAS encourages customers to visit our locations to learn more about the capabilities, observe
performance and to meet personnel.
PAS customers expect confidentiality. Personnel will not divulge or release information to a
third party without proper authorization unless the information is required for litigation
purposes. See Section 4.1.5.4 of this manual and policy COR-POL-0004 Code of Ethics and
Professional Conduct for more information on the policy for client confidentiality.
4.7.2 Customer Feedback
PAS actively seeks positive and negative feedback from customers through surveys and direct
communication. Information from the client about their experience working with PAS and
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their satisfaction with work product is used to enhance processes and practices and to improve
decision making. Customer feedback is reviewed to identify risk and opportunity. Corrective,
preventive, or continuous improvement actions are taken based on nature of and/or feedback
trends.
Also see sections 4.9, 4.10, 4.11, 4.12, 4.14, and 4.15 for more information about how customer
feedback is managed by PAS and used to enhance the QMS.
4.8 Complaints
A complaint is a formal expression of dissatisfaction with the performance of a service or product
originating from a party external to Pace®. Complaints provide opportunities to improve processes
and/or build stronger working relationships with clients.
The PAS complaint resolution process depends on the situation and the nature of the complaint.
Each complaint received is reviewed to determine if it is valid. If the complaint is valid, it is either
addressed immediately by the person receiving the complaint or the nature of the complaint is further
reviewed and investigated prior to resolution and follow up with the customer.
Complaints (and compliments) are recorded and reviewed during Annual Management Review (See
Section 4.15).
4.9 Nonconforming Work
4.9.1 Definition of Nonconforming Work
Nonconforming work is work that does not conform to customer requirements, standard
specifications, policies, and procedures, or that does not meet acceptance criteria.
The discovery of non-conforming work comes from various sources which include, but are
not limited to:
results of quality control samples and instrument calibrations;
quality checks on consumables and materials;
general observations of personnel;
data review;
proficiency testing;
internal and external audits;
complaints and feedback;
management review and reports; and
regulatory and certification and accreditation actions.
The way in which the laboratory or service center manages nonconforming work depends on
the significance and impact (risk) of the issue. Some issues may simply require correction,
others may require investigation, corrective action (See 4.11) and/or data recall (See 4.16).
When the location releases data and test results associated with nonconforming QC and
acceptance criteria, test results are qualified, or non-conformances are noted in the final
analytical report to apprise the data user of the situation. (See 5.10)
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Nonconforming work also includes unauthorized departure from l policies, procedures, and
test methods. Authorized departures are explained in the following subsections. Situations that
do not conform to these conditions are considered unauthorized departure(s).
4.9.1.1 Authorized Departure from SOPs
Departures from an SOP may sometimes be necessary to correct for an error in an
SOP or to resolve a complex problem. For example, to mitigate a complex matrix
interference.
An authorized departure from a test method SOP is one that has been reviewed and
approved by the department leader, however named, of the work area in which the
test method is performed. The leader, when authorizing a departure from an SOP,
accepts full responsibility to ensure the departure does not conflict with Pace® or
PAS policy or procedure, does not affect statutory, regulatory or program compliance
and does not adversely affect data integrity or usability.
Departure from administrative or process-oriented SOPs must be approved by the
local QM.
Documentation of the reason for the SOP departures must be retained with
management approval. Approved departures from test method SOPs should be noted
in the final test report to advise the data user.
See SOP ENV-SOP-CORQ-0016 SOP for SOPs and SWI, for more information.
4.9.1.2 Authorized Departure from Test Methods (Method Modifications)
When test results are associated to a published reference test method, the location’s
test method SOP must be consistent with the test method. If the test method is
mandated for use by a specific regulatory program such as drinking water, wastewater
or a certification or accreditation program, such as TNI/NELAC, the SOP must
comply with or include these requirements, or the resulting data and test results
cannot be used for regulatory compliance purposes.
If the procedures in the SOP are modified from the test method, these modifications
must be clearly identified in the SOP. The conditions under which the location may
establish an SOP that is modified from these reference method or regulatory program
and what is considered a modification are specified in ENV-SOP-CORQ-0011 Method
Validation and Instrument Verification.
Client requests to deviate from the test method are managed as client requests to
depart from the test method SOP since it is the SOP that the location follows when
performing work.
4.9.1.3 Stop Work Authority
Stop Work Authority provides PAS personnel with capability to stop work when there
is a perceived unsafe condition or behavior that may result in an unwanted event.
All personnel have the authority to request a stop work order when necessary to
preserve data integrity or safety of workers.
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The need for the stop work order and resolution of the problem must be confirmed
by subject matter experts and resumption of work must be approved as follows:
For stop work orders related to environmental health and safety (EHS) and/or
waste management, the decision to stop work may be made by any employee.
These decisions must often be made in real-time to protect the safety of the
worker. The decision to correct the problem, how, and/or to resume work after
stop work has been initiated may be made by the Chief Compliance Officer or
the EHS Director, or the deputies assigned to these positions.
Any employee may recommend a stop work order for concerns related to data
integrity. The need to stop work must be reviewed and affirmed by quality
personnel to confirm the concern is valid. The decision to uphold the stop work
order must minimally include the local QM, the QPM, and the Corporate Quality
Director. The President, the Sr. VPO, the VPO, the Chief Compliance Officer
and Chief Technical Officer may also be included in the decision making and
resolution process depending on the situation and/or needs for correction to
ensure protocols for investigation are followed. Resumption of work after
correction may be made by the Corporate Quality Director, or the Quality
Program Manager assigned to the location for which the stop work order was
issued or by the deputies assigned to these positions.
4.10 Continuous Improvement
The PAS QMS is designed to achieve continuous improvement through the implementation of the
quality policy and objectives outlined in this manual. Information about laboratory and service center
activities and performance is gained from sources such as customer feedback, audits, QC, trend
analysis, business analytics, management reports, proficiency testing, and management systems review.
This information is subsequently used during the corrective action (see section 4.11) and preventive
action (see section 4.12) processes and during annual review of the management system (see section
4.15) to establish goals and objectives for improvement.
PAS also promotes a continuous improvement culture based on the principles of lean manufacturing.
These principles include 3P (Process, Productivity, Performance) and Kaizen. 3P is a platform used
by Pace to share best practices and standardization across the network to achieve operational
excellence. Kaizen is a team-based process used to implement tools and philosophies of lean to reduce
waste and achieve flow with the purpose of improving both external and internal customer
satisfaction. All activities of 3P and Lean must conform with the requirements of this quality manual
and supporting policies and procedures.
4.11 Corrective Action
Corrective action is a process used to eliminate the cause of a detected nonconformity. It is different
from a correction. A correction is an action taken to fix an immediate problem but that does not
resolve the underlying cause of why the problem occurred. The objective of corrective action is to
find the underlying cause(s) of the problem and to put in place fixes to prevent the problem from
happening again. The corrective action process, referred to as CAPA, is one of the most effective
tools used by PAS to prevent nonconforming work, identify risk and opportunity, and improve service
to our customers.
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PAS has two general processes for corrective action, the application of which process is used depends
on the type of nonconformity:
Quality control (QC) exceptions (nonconformance) that occur during routine testing is investigated
through troubleshooting and required actions for correction is specified in policies and SOPs. When
action is not taken, cannot be taken, or is not successful, test results associated with the
nonconforming work are qualified in the final test report. Documentation of the nonconformance
and corrective action taken is documented in the analytical record.
A 7-stage corrective action process is used when there is a recurring problem. These problems are
identified through various activities such as but not limited to quality control trends, internal and
external audits, management review, customer feedback, and general observation.
The 7 Stage CAPA Process for PAS includes:
1) Identification and Containment
2) Evaluation
3) Investigation
4) Cause Analysis
5) Action Plan
6) Implementation
7) Follow Up and Effectiveness Review
PAS procedures for corrective action, are specified in corporate SOP ENV-SOP-CORQ-0018
Procedure for Corrective and Preventive Action. Some key concepts and activities related to the PAS
corrective action process is provided in the next three subsections.
4.11.1 Cause Analysis (AKA Root Cause Analysis)
Cause analysis is the process of investigation used to identify the underlying cause(s) of the
problem. After causal factors are identified, ways to mitigate the causal factors are identified
and action(s) most likely to eliminate these factors are taken.
PAS uses different methods to conduct cause analysis. The most common approach is 5-Why,
4M, Fishbone Diagrams, or brainstorming may be appropriate depending on the situation.
The method used is case specific and is documented in the CAPA record.
4.11.2 Effectiveness Review
Monitoring corrective actions taken for effectiveness is an essential part of the corrective
action process. Effectiveness means the actions taken were appropriate and sustainable.
Appropriate means the action(s) taken prevented recurrence of the problem since the time
corrective action was taken and sustainable means the actions taken are still in place.
The data from CAPA records are used by PAS to identify opportunities for preventive action
or to gain lessons learned when actions taken were not adequate to solve the problem. See
Section 4.12 (Preventive Action) and 4.15 (Management Review) for more information.
4.11.3 Additional Audits
When cause analysis and investigation of a problem casts doubt on compliance with PAS
policies, procedures, or to regulatory requirements; a special audit of the area of activity may
be performed as part of the corrective action process. These special audits are used to
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determine the scope of the problem and to provide information for the CAPA process.
Additional full-scale audits are done when a grave issue or risk to the business is identified.
4.12 Preventive Action
Preventive action(s) are actions taken to eliminate the cause of a potential nonconformity before it
happens.
Some examples of preventative action include, but are not limited to:
Routine instrument maintenance (Preventative maintenance)
Addition of Staff and Equipment
Professional Development Activities
Implementation of New Technology
PAS looks for opportunities for preventive action from a variety of sources including employee idea’s,
customer feedback, business partners input, trend analysis, business analytics, management reviews,
proficiency testing results, and risk-benefit analysis.
PAS management evaluates the success of preventive actions taken in any given year during annual
management review. See Section 4.15 for more information.
4.12.1 Change Management
Preventive actions may sometimes result in significant changes to processes and procedures
used by PAS locations. PAS management evaluates the risks and benefits of change and
includes in its implementation of change process, actions to minimize or eliminate any risk.
The types of changes for which risk are considered and managed include infrastructure change,
change in analytical service offerings, certification or accreditation status, instrumentation,
LIMS changes, and changes in key personnel.
4.13 Control of Records
A record is a piece of evidence about the past, especially an account of an act or occurrence kept in
writing or another permanent form. PAS records document activities and provide evidence of
conformity to the requirements established in the QMS. These records may be hardcopy or electronic
on any form of media.
4.13.1 General Requirements
4.13.1.1 Procedure
PAS requirements for control of records are specified in corporate policy ENV-POL-
CORQ-0013 Record Management.
The policy is established to assure quality and technical records are identified, retained,
indexed, and filed to allow for retrieval during the entire retention timeframe. During
storage, records are kept secure and protected from deterioration. At the end of the
retention time, the records are disposed of properly in order to maintain client
confidentiality and to protect the interests of the company.
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In general, records fall into three categories: quality, technical, and administrative.
Examples of each are provided in the following table:
Record Type Includes Records of:
Quality Document Types listed in SOP ENV-SOP-CORQ-0015
Audits: Internal and External
Certificates and Scopes of Accreditation
Corrective & Preventive Action
Management Review
Data Investigations
Method Validation
Instrument Verification
Training Records
Technical Raw Data
Logbooks
Certificates of Traceability
Analytical Record
Test Reports & Project Information
Technical Training Records & Demonstration of Capability
Administrative Personnel Records
Finance/Business
4.13.1.2 Record Legibility and Storage
Records are designed to be legible and to clearly identify the information recorded.
Manual entries are made in indelible ink; automated entries are in a typeface and of
sufficient resolution to be read. The records identify personnel that performed the
activity or entered the information. Records are archived and stored in a way that they
are retrievable. Access to archived records is controlled and managed.
For records stored electronically, the capability to restore or retrieve the electronic
record is maintained for the entire retention period. Hardcopy records are filed and
stored in a suitable environment to protect from damage, deterioration, or loss.
Hardcopy records may be scanned to PDF for retention. Scanned records must be
checked against the hardcopy to verify the scan is complete and legible.
Administrative records are kept for a minimum of 5 years and technical and quality
records are kept for 10 years unless otherwise specified by the client or regulatory
program.
The date from which retention time is calculated depends on the record. In general,
the retention time of technical records of original observation and measurement is
calculated from the date the record is created. If the technical record is kept in a
chronological logbook, the date of retention may be calculated from the date the
logbook is archived. The retention time of test reports and project records, which are
considered technical records, is calculated from the date the test report was issued.
The retention time of quality records is usually calculated from the date the record is
archived.
Refer to the record management policy and the location specific SOP for more
information.
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4.13.1.3 Security
PAS locations are secure facilities and access to records is restricted to authorized
personnel.
4.13.1.4 Electronic Records
The data systems used to store electronic records is backed up in accordance with
SOP ENV-SOP-MTJL-0058, Information Technology Processes and ENV-SOP-MTJL-
0010, Protection and Transfer of Laboratory Records.. Access to archived records stored
electronically is maintained by personnel responsible for management of the
electronic system.
4.13.1.5 Electronic Signature Policy
Work done by PAS locations include activities that require the application of a
signature. Some work product is in electronic format and signatures are applied
electronically.
The Electronic Signatures in Global and National Commerce Act (E-Sign Act)
clarifies that electronic signatures are legally valid and enforceable under United States
law.
The PAS policy for use and application of electronic signatures is specified in
corporate policy ENV-POL-CORQ-0014 Electronic Signature Policy.
All employees of PAS including temporary and contract personnel, must sign an
Electronic Signature Agreement to acknowledge that they understand and accept that
work activities performed by them may be authenticated with application of an
electronic signature and that electronic signature has the same validity as a
handwritten signature. Their signed agreement also confirms the individual has read
and understands the policy and agrees to abide by the requirements for use of
electronic signature stated in the policy.
4.13.2 Technical Records
In addition to the requirements specified in subsections 4.13.1.1 through 4.13.1.5, the
requirements in the following subsections also apply to technical records.
4.13.2.1 Description
Technical records are the accumulation of data and information generated from the
analytical process. These records may include forms, worksheets, workbooks,
checklists, notes, raw data, calibration records, final test reports, and project record.
The accumulated record needs to provide adequate detail to historically reconstruct
the process and identify the personnel that performed the tasks associated with a test
result.
4.13.2.2 Real Time Recordkeeping
Personnel are instructed and expected to always record observations, data, and
calculations at the time they are made. PAS managers are responsible to assure that
data entries, whether made electronically or on hardcopy, are identifiable to the task.
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4.13.2.3 Error Correction
Errors in records must never be erased, deleted, or made illegible. Use of correction
fluid, such as white-out is prohibited. In hardcopy records, the error is corrected by a
single strike through the original entry and the new entry recorded alongside or
footnoted to allow for readability. Corrections are initialed and dated by the person
making the correction. If the correction is not self-explanatory, a reason for the
correction is recorded.
For electronic records, equivalent measures of error correction or traceability of
changes made is kept. For example, audit trails provide records of change.
Maintenance of proper practices for error correction is monitored through the tiered
data review process described in Section 5.9.3. Records are reviewed throughout the
data review process. Individuals performing these reviews flag errors that are not
properly corrected and bring these to the attention of the department manager or
supervisor of the work area in which the record was generated so that the problem
may be addressed and corrected with the individual(s) that did not make the
correction properly.
4.14 Audits
Quality personnel, or their designees, perform internal systems and technical audits to assess
implementation of the QMS, compliance to this manual, policy, and procedures that make up the
QMS. Since the processes in this manual are based on the requirements from relevant and applicable
Standards for the operation and management of laboratories when operations are assessed against the
PAS QMS, compliance with regulatory program requirements and accreditation/certification program
requirements are also assessed.
PAS locations are also audited by external parties such as regulatory agencies, customers, consultants,
and non-government assessment bodies (NGAB).
Information from internal and external audits is used by local and corporate management to address
deficiencies and to identify opportunities to improve customer service and quality of work, including
reliability and usability of data and test results.
Deficiencies, observations, and recommendations from audits are managed by the local QM using the
CAPA process. See Section 4.11 for more information.
4.14.1 Internal Audit
The PAS internal audits are conducted to ensure practice matches what we say we do and what
we say we do is compliant with the PAS QMS and relevant standards and requirements.
The internal audit program is managed by the local QM who prepares an audit plan at the
beginning of each calendar year. The schedule is prepared to assure that all work areas are
reviewed over the course of the year and test methods are audited every two years, unless a
more frequent test method audit is required by program. Conformance to the schedule is
monitored on a monthly basis.
PAS management is responsible to ensure the audit schedule is maintained. PAS supervisors
are expected to cooperate with the quality personnel to provide them with complete access to
the work area, personnel, and records needed to conduct the audit.
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Internal audits may be performed by non-quality personnel when the auditor is approved by
the local QM. Non-quality personnel may not audit their own work activities unless it can be
demonstrated that an effective and objective audit will be conducted. The person conducting
the audit should be trained, qualified, and familiar enough with the objectives and policies of
the PAS QMS and knowledgeable with process and test method SOPs related to the activities
audited. The auditors should be trained in auditing practices in order to perform a thorough
and effective evaluation.
Test method audits include reviews of test reports to verify the product is consistent with
customer/project requirements, the work was conducted in accordance with policy and SOPs,
the SOP complies with the cited reference method, test results are accurate, and of known and
documented quality and properly qualified, when necessary.
Special audits are performed as needed to follow up on a specific issue such as a client
complaint, negative feedback, concerns of data integrity or ethics, or a problem identified
through other audits. Special audits may be scheduled or unscheduled. Unscheduled internal
audits are conducted whenever doubts are cast on compliance with regulatory requirements
or its own policies and procedures. These unscheduled internal audits may be conducted at
any time and may be performed without an announcement to the location or work area
audited.
When observations and findings from any audit (internal or external) cast doubt on the validity
of testing results, the location takes immediate action to investigate the problem and take
corrective action. (Also see 4.11 and 4.16)
4.14.1.1 Corporate Compliance Audit
PAS locations may also be audited by corporate personnel at discretion. The purpose
of the corporate compliance audit is to assess whether the location’s practices,
processes and procedures conform with the PAS QMS and to identify risk and
opportunity.
4.15 Management Review
Local management conducts an annual business review of each location under their purview to assess
performance and to establish goals, objectives, and action plans for the upcoming year.
The procedure used to conduct this review is specified in corporate SOP ENV-SOP-CORQ-0005
Management Review.
At a minimum, the following topics are reviewed and discussed during annual management review:
Changes in internal and external issues relevant to the location;
Fulfillment of objectives and initiatives;
suitability of policies and procedures, including EHS and waste management;
status of actions from previous performance reviews;
The outcome of recent internal audits;
Corrective and preventive actions;
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Assessments by external bodies;
The results of interlaboratory comparisons or proficiency tests;
Changes in the volume and type of the work;
Customer and personnel feedback, including complaints;
Effectiveness of improvements / preventive actions made since last review;
Adequacy of resources;
results of risk identification;
Proficiency testing performance and other measures related to the assurance of validity of test
results; other relevant factors, such as QC trends and training status.
The discussion and results of this review are documented in a report prepared by local management.
This report includes a determination of the effectiveness of the management system and its processes,
goals, and objectives for improvements in the coming year with timelines and responsibilities, and any
other need for change.
Goals and action items from annual management systems review are shared with local employees and
with corporate management to highlight focus areas for improvement in addition to areas in which
the location has excelled.
4.16 Data Integrity
PAS procedures for the investigation and response to events that may affect data integrity are
described in the corporate SOPs for data inquiries and data recall and corrective and preventive action,
however named.
Customers whose data are affected by these events are notified in a timely manner, usually within 30
days after the impact of the problem is understood. Some accreditation programs also require
notification to the accreditation body (AB) within a certain timeframe from date of discovery when
the underlying cause of the issue impacts accreditation. PAS locations must follow any program or
project specific client notification requirements for notification, when applicable.
5.0 TECHNICAL REQUIREMENTS
5.1 General
Multiple factors contribute to the correctness and reliability of the technical work performed by PAS.
These factors fall under these broad categories:
Human Performance
Facility and Environmental Conditions
Test Method Performance and Validation
Measurement Traceability
Handling of Samples
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The impact of each of these factors varies based on the type of work performed. To minimize negative
effects from each of these factors, PAS accounts for the contribution from each of these categories
when developing test method and process (administrative) SOPs, evaluating personnel qualifications
and competence, and in the selection of equipment and supplies used.
5.2 Personnel
5.2.1 Personnel Qualifications
The PAS program for personnel management is structured to ensure personnel are selected,
qualified, and competent to perform the roles and responsibilities of their position based on
education, experience, and training.
Qualifications, duties, responsibilities, and authorities of each position are specified in job
descriptions maintained by corporate HR (See Section 5.2.4). These job descriptions provide
the general basis for the selection of personnel for hire and are used by the location to
communicate to personnel the duties, responsibilities, and authorities of their position.
Qualification records may include but are not limited to diploma, transcripts, and curriculum
vitae (CV).
The term “personnel” refers to individuals employed by PAS directly as full-time, part-time,
or temporary, and individuals employed by PAS by contract, such as through an employment
agency. The term “personnel” is used interchangeably with the term “employee” throughout
this manual. For purposes of this manual, these terms are equivalent.
The personnel management program is structured to establish and maintain records for each
of the following:
Selection of personnel;
Training of personnel;
Supervision of personnel;
Authorization of personnel; and
Monitoring Competence of personnel.
5.2.1.1 Competence
Competence is the ability to apply a skill or series of skills to complete a task or series
of tasks correctly within defined expectations.
Competence for technical personnel authorized by PAS to provide opinion and
interpretation of data to customers also includes the demonstrated ability to:
Apply knowledge, experience, and skills needed to safely and properly use
equipment, instrumentation, and materials required to carry out testing and other
work activities in accordance with manufacturer specifications and location
SOPs;
Understand and apply knowledge of general regulatory requirements necessary to
achieve regulatory compliance in work product; and
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Understand the significance of departures and deviations from procedure that
may occur during the analytical testing process and the capability and initiative to
troubleshoot and correct the problem, document the situation and decision-
making process, and to properly qualify the data and analytical results.
PAS requirements for the competence of personnel (education, qualification, work
experience, technical skills, and responsibilities) are specified in job descriptions
created by management and kept by human resources (HR). The job description
provides the basis for the selection of personnel for each position.
An employee is considered competent when he/she has completed the required
training specified in Section 5.2.2 and documentation of training is complete.
5.2.2 Training (Required)
Pace® training requirements are outlined in Pace® policies COR-POL-0023 Mandatory
Training Policy and COR-POL-0004 Code of Ethics and Professional Conduct.
5.2.2.1 Required Training Requirements
The PAS training program includes these elements:
Scheduling
Execution
Documentation and Tracking
Evaluation of Effectiveness
Required training is scheduled by corporate training personnel, local quality
personnel, and the employee’s direct supervisor.
Training on required topics, processes and procedure is delivered using various
methods that incorporate techniques that appeal to the main learning styles: visual,
aural, linguistic, and kinesthetic. Techniques include, on-the-job, instructor-led, self-
study, eLearning, and blended.
The employee’s direct supervisor is responsible for oversight of completion of the
employee’s required training and for providing adequate time to the employee to
complete training assignments. The supervisor and employee are responsible to make
sure the employee’s training status and training records for all required training is
current, complete, and documentation of training is available.
Training status is tracked by the local QM, who provides the status to local
management at least monthly or more frequently, as necessary, to ensure required
training for personnel is complete and up to date.
The following subsections further describe the required PAS training program for
new hire training and on-going training.
5.2.2.1.1 New Hire Required Training
New hire training requirements apply to new personnel and to
existing employees starting in a new position or different work area.
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Required new hire training includes training on each of the
following:
Ethics and Data Integrity (See 5.2.2.1.3)
Quality Manual / Quality Management System (See 5.2.2.1.4)
Safety Manual and any training requirements specified in the
manual.
Policies & SOPs relevant to their job tasks
Technical personnel that prepare and test samples must also
successfully complete an initial demonstration of capability
(IDOC) for the test methods performed before independently
testing customer samples. (See 5.2.2.1.5). Independent testing
means without direct supervision of the work activity by the
supervisor or a qualified trainer.
All required training must be documented and verified complete by
the local QM before the employee is authorized to work
independently on client samples. Until then, the employee’s direct
supervisor is responsible for all work produced by the new employee
under their supervision.
5.2.2.1.2 On-Going Required Training
Personnel receive on-going training in each of the following topics:
Ethics and Data Integrity (See 5.2.2.1.3)
Quality Manual / Quality Management System (See 5.2.2.1.4)
Safety
Changes to Policies & SOPs, relevant to their job activities.
New Policies & SOPS, relevant to their job activities.
Technical personnel must also successfully complete on-going
demonstration of capability (CDOC) for all test methods
performed on an annual basis. (See 5.2.2.1.5)
All required training must be documented and verified complete by
the local QM with training records readily accessible in accordance
with the corporate policy for Record Management (ENV-POL-
CORQ-0013).
5.2.2.1.3 Ethics and Data Integrity Training
Data integrity training is provided to all new personnel and refresher
data integrity training is provided to all employees on an annual basis.
Personnel are required to acknowledge they understand that any
infractions of the PAS data integrity procedures will result in a
detailed investigation that could lead to profound consequences
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including immediate termination, debarment, or civil/criminal
prosecution.
Completion of data integrity training is documented using the
mechanism established by Pace® to provide evidence that the
employee has participated in training on this topic and understand
their obligations related to data integrity.
The following topics and activities are covered:
Policy for honesty and full disclosure in all analytical reporting;
Prohibited Practices;
How and when to report data integrity issues;
Record keeping. The training emphasizes the importance of
proper written documentation on the part of the analyst with
respect to those cases where analytical data may be useful, but
are in one sense or another partially nonconforming;
Training Program, including discussion regarding all data
integrity procedures;
Data integrity training documentation;
In-depth procedures for data monitoring; and
Specific examples of breaches of ethical behavior such as
improper data manipulations, adjustments of instrument time
clocks, and inappropriate changes in concentrations of
standards.
All PAS personnel, including contract and temporary, are required
to sign an “Attestation of Ethics and Confidentiality” at the time of
hire and/or during annual refresher training or as specified in the
ethics policy. This document clearly identifies inappropriate and
questionable behavior. Violations of this document result in
profound consequences, including prosecution and termination, if
necessary.
Also see SOP-ENV-COR-POL-0004 Code of Ethics and Professional
Conduct for more information.
5.2.2.1.4 Management System Documents Training
The Quality Manual policies, and SOPs are the documents used by
regulatory bodies and Pace® customers to verify capability,
competency, and compliance with their requirements and
expectations.
In addition to on-the-job training, employees must have a signed
Read and Acknowledgement Statement (R&A) on record for the
quality manual, and the policies and SOPs relating to his/her job
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responsibilities. This statement, whether signed by the employee
electronically or by wet signature, confirms that the employee has
received, read, and understands the content of the document, that
the employee agrees to follow the document when carrying out their
work tasks; and the employee understands that unauthorized change
to procedures in an SOP is not allowed except in accordance with
the SOP departure policy (See 4. 9.1).
See SOP ENV-CORQ-0016 Standard Operating Procedures and Standard
Work Instructions for more information.
5.2.2.1.5 Demonstration of Capability (DOC) Requirements
An initial demonstration of capability (IDOC) must be completed
and validated prior to authorization for the employee to work
independently on client samples for the test method. After
successful IDOC, the employee must demonstrate continued
proficiency (CDOC) for the test method on an annual basis. If more
than a year has passed since the employee last performed the
method; then capability must be re-established with an IDOC.
Successful DOC is one where the DOC replicate data has been
compiled, reviewed, and verified by the employee’s supervisor
and/or manager to be complete and to have met acceptance criteria
and the DOC record has been validated by quality personnel for
completeness and compliance, and placed in the employee’s training
file for accessibility and reference.
Demonstration of capability (DOC) procedures and requirements
vary by technology.
For example, a DOC for chemistry test methods where spiking is
appropriate, is based on the employee’s capability to achieve
acceptable precision and accuracy for each analyte reported by the
laboratory for the test method using the laboratory’s test method
SOP.
DOC procedures and requirements must be specified in the
laboratory’s test method SOP or a stand-alone SOP. Refer to these
SOPs for more information.
5.2.2.1.6 Effectiveness of Training
Effectiveness of individual employee training is measured by their
demonstrated ability to comprehend the training material and apply
knowledge and skills gained to their job task. Measurements include
but are not limited to:
Testing of the employee’s knowledge of the QMS, policies, and
technical and administrative procedures through various
mechanisms, such as quizzes, observation, and interviews.
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Demonstrated ability to convey information correctly and
factually in written and verbal communication to internal and
external parties.
Demonstrated ability to carry out tasks in accordance with SOPs
and other work instructions.
Demonstrated ability to make sound decisions based on
guidance and information available.
Demonstrated initiative to seek help or guidance when the
employee is unsure of how to proceed.
5.2.2.2 Supplemental Learning
Supplemental learning objectives may be established for newly hired personnel to aid
in their development of administrative and technical skills. These learning objectives
and materials, referred to as Learning Plans (LP), are created and maintained by the
PAS 3P program and managed by the employee’s direct supervisor.
Pace® also offers a wide variety of supplemental learning courses that are made
available to all employees for professional development. These learning materials,
maintained by Pace® corporate training personnel, are accessed via the company’s
employee portal, PaceConnect. The learning may be self-initiated based on an
employee’s interest or may be assigned to the employee at the discretion of
management as professional development as part of an employee’s annual goals.
Supplemental learning courses and learning plan activities are not prerequisites for
competency (Section 5.2.1.1) and are not considered part of the required PAS QMS
training program.
5.2.3 Personnel Supervision
Every employee is assigned a direct supervisor, however named, who is responsible for their
supervision.
General supervisory responsibilities may include but are not limited to:
Hiring Employees
Training Employees
Performance Management
Development, oversight, and execution of personnel training plans
Monitoring personnel work product to assure the work is conducted in accordance with
this quality manual, policies, SOPs, and other documents that support the QMS.
5.2.4 Job Descriptions
Job Descriptions that define the required education, qualifications, experience, skills, roles and
responsibilities, and reporting relationships for each Pace® position are established by top
management and kept by corporate HR. The job descriptions apply to employees who are
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directly employed by Pace®, part-time, temporary, technical, and administrative and by those
that are under contract with Pace® through other means.
The job descriptions include the education, expertise, and experience required for the position
and the responsibilities and duties, including any supervisory or managerial duties assigned to
the position.
5.2.5 Authorization of Technical Personnel
Technical personnel are authorized by local quality personnel to perform the technical aspects
of their position after quality personnel have verified that the employee meets the
qualifications for the position, has successfully completed required training (Section 5.2.2.1),
and the employee has completed initial demonstrated capability (Section 5.2.2.1.5). After initial
authorization, technical personnel are expected to maintain a current and complete training
record, demonstrate on-going capability at least annually for each test method performed, and
produce reliable results through accurate analysis of certified reference materials, proficiency
testing samples, and/or routine quality control samples in order to remain authorized to
continue to perform their duties.
Records to support authorization including, education, experience, training, and other
evaluations are kept by the location where the employee works.
5.3 Accommodations and Facilities
5.3.1 Facilities
PAS laboratories and service centers are designed to support the correct performance of
procedures and to not adversely affect measurement integrity or safety. Access to PAS facilities
is controlled by various measures, such as card access, locked doors, staffed main entry.
5.3.2 Environmental Conditions
Each location is equipped with energy sources, lighting, heating, and ventilation necessary to
facilitate proper performance of calibrations and tests. The location ensures that
housekeeping, electromagnetic interference, humidity, line voltage, temperature, sound, and
vibration levels are appropriately controlled to ensure the integrity of specific measurement
results and to prevent adverse effects on accuracy or increases in the uncertainty of each
measurement.
Environmental conditions are monitored, controlled, and recorded as required by the relevant
specifications, methods, and procedures. Operations are stopped if it is discovered that the
environmental conditions would jeopardize the integrity of analytical results or other work
product.
5.3.3 Separation of Incompatible Activities
The layout and infrastructure of each work area including air handling systems, power supplies,
and gas supplies of each work area is specifically designed for the type of analytical activity
performed. Effective separation between incompatible work activities is maintained. For
example, sample storage, preparation, and chemical handling for volatile organic analysis
(VOA) is kept separate from semi-volatile organic (SVOA).
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Samples known or suspected to contain high concentration of analytes are separated from
other samples to avoid the possibility for cross-contamination. If contamination is found, the
source of contamination is investigated and resolved in accordance with applicable SOPs.
5.3.4 Security
Security is maintained by controlled access to the building and by surveillance of work areas
by authorized personnel. Access is controlled to each area depending on the required
personnel, the sensitivity of the operations performed, and potential safety concerns.
5.3.5 Good Housekeeping
PAS locations must maintain good housekeeping practices in work areas to maintain a
standard of cleanliness necessary for analytical integrity and personnel health and safety.
5.4 Test Methods
5.4.1 General Requirements
The laboratory uses test methods and procedures that are appropriate for the scope of
analytical services the laboratory offers.
Instructions on the use and operation of equipment and sample handling, preparation, and
analysis of samples are provided in SOPs. The instructions in SOPs may be supplemented
with other documents including, but not limited to, standard work instructions (SWI),
manuals, guides, project documents and reference documents.
These documents are managed using the procedures described in SOP ENV-SOP-CORQ-
0015 Document Management and Control and SOP ENV-SOP-CORQ-0016 Standard Operating
Procedures and Standard Work Instructions.
5.4.2 Method Selection
The test methods and protocols used by the laboratory are selected to meet the needs of the
customer, are appropriate for the items tested, for the intended use of the data, and to conform
with applicable federal, statutory, or program requirements.
The test methods offered by PAS are industry accepted methods published by international,
regional, or national standards. Each PAS laboratory bases its procedure on the latest approved
edition of a method unless it is not appropriate or possible to do so, or unless regulatory
requirements specify otherwise.
The laboratory confirms that it can perform the test method and achieve desired outcome
before analyzing samples (see section 5.4.5). If there is a change in the published analytical
method, then the confirmation is repeated.
When a customer does not specify the test method(s) to be used, the laboratory may suggest
test methods that are appropriate for the intended use of the data and the type of samples to
be tested. The laboratory will also inform customers when test methods requested are
considered inappropriate for their purpose and/or out of date. This discourse takes place
during review of analytical service requests (See Section 4.4).
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5.4.3 PAS Developed Methods
A PAS developed method is a method developed from scratch (no published source method),
a procedure that modifies the chemistry from the source method, or a procedure that exceeds
the scope and application of the source method.
PAS developed methods must be validated prior to use (see section 5.4.5) and the procedure
documented in a test method SOP.
The requirements for non-standard methods (Section 5.4.4) also apply to PAS developed
methods.
5.4.4 Non-standard Methods
A non-standard method is a method that is not published or approved for use by conventional
industry standards for the intended purpose of the data. Non-standard methods must be
validated prior to use (see section 5.4.5) and the procedure developed and documented in a
test method SOP.
At a minimum, the following information must be included in the procedure:
Title / Identification of Method;
Scope and Application;
Description of the type of item to be analyzed;
Parameters or quantities and ranges to be determined;
Apparatus and equipment, including technical performance requirements;
Reference standards and reference materials required;
Environmental conditions required and any stabilization period needed; and
Description of the procedure, including:
o Affixing identification marks, handling, transporting, storing, and preparing of
items;
o Checks to be made before the work is started;
o Verifying equipment function and, where required, calibrating and/or adjusting
the equipment before each use;
o Method of recording the observations and results;
o Any safety measures to be observed;
o Criteria and/or requirements for approval/rejection;
o Data to be recorded and method of analysis and presentation; and
o Uncertainty or procedure for estimating uncertainty.
Use of a non-standard method for testing must be agreed upon with the customer. The
agreement, which is retained by the laboratory in the project record, must include the
specifications of the client’s requirements, the purpose of testing, and their authorization for
use of the non-standard method.
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5.4.5 Method Validation
5.4.5.1 Validation Description
Validation is the process of confirmation and the provision of objective evidence that
the stated requirements for a specific method/procedure are fulfilled.
The laboratory’s requirements and procedures for method validation are outlined in
SOP ENV-SOP-CORQ-0011 Method Validation and Instrument Verification.
5.4.5.2 Validation Summary
All test methods offered by the laboratory are validated before use to confirm the
procedure works and the data and results achieved meet the goals for the method and
repeated when there are major changes to the laboratory procedure.
Results of validation are retained are kept in accordance with method validation SOP
and the corporate policy ENV-CORQ-POL-0013 Record Management.
5.4.5.3 Validation of Customer Need
The validation process includes review of accuracy, precision, sensitivity, selectivity,
linearity, repeatability, reproducibility, robustness, and cross-sensitivity of the
procedure against general customer needs to ensure the laboratory’s procedure will
meet those needs.
The following subsections explain some concepts as they are applied to chemistry.
The applications of these same concepts may differ for other technologies such as
microbiology, radiochemistry, whole effluent toxicity (WET), and asbestos or other
validation concepts may apply to these disciplines. Refer to the laboratory’s test
method SOPs for more information.
5.4.5.3.1 Accuracy
Accuracy is the degree to which the result of a measurement,
calculation, or specification conforms to the correct value or a
standard. When the result recovers within a range from the known
value (control limit); the result generated using the laboratory’s test
method SOP is considered accurate.
5.4.5.3.2 Precision
Precision refers to the closeness of two or more measurements to
each other. It is measured by calculating the relative percent
difference (RPD) or relative standard deviation (RSD) from results
of separate analysis of the same sample. Precision provides
information about repeatability, reproducibility, and robustness of
the laboratory’s procedure.
5.4.5.3.3 Limits of Detection (LOD) (Chemistry)
The LOD is the minimum result which can be reliably discriminated
from a blank with a predetermined confidence level. The LOD
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establishes the limit of method sensitivity and is also known as the
detection limit (DL) or the method detection limit (MDL).
Values below the LOD cannot be reliably measured and are not
reported by the laboratory unless otherwise specified by regulatory
program or test method.
The LOD is established during method validation and after major
changes to the analytical system or procedure that affect sensitivity
are made.
The laboratory’s procedure for LOD determination is specified in
SOP ENV-SOP-MTJL-0016, Method Detection Limits (MDL), Limits
of Detection (LOD) and Limits of Quantitation (LOQ) and ENV-SOP-
MTJL-0340, Radiochemistry Method Performance Criteria.
For chemistry methodology, the local SOP must comply with the
current version of each of the following documents:
EPA document EPA-821-R-16-006 Definition and Procedure for the
Determination of the Method Detection Limit;
2016 TNI Standard V1M4; and
TNI GUID-3-109-Rev. 0, V1M4 2016 Standard Update Guidance
on Detection and Quantitation.
5.4.5.3.4 Limits of Quantitation (LOQ) and Reporting Limit (RL)
This section describes these concepts for chemistry. For non-
chemistry technologies, such as microbiology, refer to laboratory
SOPs.
The LOQ is the minimum level, concentration, or quantity of a
target analyte that can be reported with a specified degree of
confidence.
The LLOQ is the value of the lowest calibration standard included
in the calibration curve. The LLOQ establishes the lower limit of
quantitation; it is not the same concept as the LOQ, however, the
LOQ and LLOQ may be the same value.
The LOQ and LLOQ represent quantitative sensitivity of the test
method.
The LOQ must always be equal to or greater than the LLOQ
and the LLOQ must always be greater than the LOD.
Any reported value (detect or non-detect) less than the LLOQ
is a qualitative value.
The RL is the value to which the presence of a target analyte is
reported as detected or not detected. The RL is project-defined
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based on project data quality objectives (DQO). In the absence of
project specific requirements, the RL is usually set to the LOQ or
the LLOQ.
The laboratory’s procedures for LOQ determination must be
specified in the same SOP for LOD determination, (See Section
5.4.5.3.3) The LLOQ for each method must be specified in the test
method SOP.
Linearity is a mathematical concept applied to calibration models
that employ multiple points to establish a calibration range used for
quantitative analysis. Linearity is measured differently based on the
calibration model. In general, if linearity is demonstrated then the
slope of the response of standards are sufficiently close to one
another. The accuracy of the linear regression and non-linear curves
is verified by checking percent error or relative standard error (RSE),
which is the process of refitting calibration data back to the model
to determine if the results are accurate. For linear curves that use
average calibration or response factor, error is measured by relative
standard difference (RSD).
Linearity also establishes the range of quantitation for the test
method used which directly impacts the sensitivity of the test
method and uncertainty in measurement results. As previously
noted, the LLOQ establishes the lower limit of quantitation.
Similarly, the upper range of linearity establishes the upper limit of
quantitation. In general, results outside of this range are considered
qualitative values. However, inorganic test methods sometimes allow
for extension of the linear range above the upper limit of
quantitation when accuracy at this value is verified.
Linearity can also be used to establish repeatability, reproducibility,
and robustness of the laboratory’s test method. When linearity is
demonstrated using a specific calibration model during method
validation, then use of this same calibration model to achieve
linearity on a day-to-day basis confirms the laboratory’s method is
repeatable, reproducible, and robust.
5.4.5.3.5 Demonstration of Capability (DOC)
The DOC performed during method validation confirms that the
procedure demonstrated acceptable precision and accuracy.
5.4.6 Measurement Uncertainty
The location provides an estimate of uncertainty in testing measurements with analytical
results on request, or when required. For example, for radiochemistry uncertainty is always
reported with the test result
For chemistry methodologies, the uncertainty of the test method is reflected in the control
limits used to evaluate QC performance for the test method. (See 5.9.1.1.9). ISO/IEC states
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that when a well-recognized test method specifies limits to the values of the major source of
uncertainty of measurement and specifies the form of presentation of calculated results, the
laboratory has satisfied the requirements on analytical uncertainty by following the test method
and reporting instructions.
When measurement uncertainty cannot be satisfied through control limits, the location will
provide a reasonable estimation of uncertainty. A reasonable estimation is based on knowledge
of method performance and previous experience. When estimating the analytical uncertainty,
all uncertainty components which are of importance in the given situation are considered.
5.4.7 Control of Data
PAS has policies and processes in place to assure that reported data is free from calculation
and transcription errors, that quality control is reviewed and evaluated before data is reported,
and to address manual calculation and integration.
5.4.7.1 Calculations, Data Transfer, Reduction and Review
Whenever possible, calculations, transfer of data, and data reduction are performed
using validated software programs (See 5.4.7.2).
If manual calculations are performed, the results of these calculations are verified
during the data review process outlined in section 5.9.3.
5.4.7.1.1 Manual Integration
The PAS policy and procedures for manual integration are provided
in corporate SOP ENV-SOP-CORQ-0006 Manual Integration.
This SOP includes the conditions under which manual integration is
allowed and the requirements for documentation.
Required documentation of manual integration includes:
complete audit trail to permit reconstruction of before and after
results;
identification of the analyst that performed the integration and
the reason the integration was performed; and
identification of the individual(s) that reviewed the integration
and verified the integration was done and documented in
compliance with the SOP.
5.4.7.2 Use of Computers and Automated Acquisition
Whenever possible, PAS uses software and automation for the acquisition,
processing, recording, reporting, storage, and/or retrieval of data.
Software applications developed by PAS are validated by corporate IT for adequacy
before release for routine use. Commercial off the shelf software is considered
sufficiently validated when the location follows the manufacturer or vendor’s manual
for set-up and use. Records of validation are kept by the corporate information
technology (IT) group or by the group that performed the validation.
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The PAS process for the protection of data stored in electronic systems includes:
Individual usernames and passwords for Laboratory Information Management
Systems (LIMS) and auxiliary systems used to store or process data.
Employee Training in Computer Security Awareness
Validation of spreadsheets used for calculations to verify formulas and logic yield
correct results and protection of these cells to prevent unauthorized change.
Operating system and file access safeguards
Protection from Computer Viruses
Regular system backup; and testing of retrieved data
Verification the software application works as expected and is adequate for use
and fulfills compliance requirements, such as the need to record date/time of data
generation.
Change control to assure requests for changes are reviewed and approved by
management before the change is made.
Communication channels to assure all staff are aware of changes made.
Version Control and maintenance of historical records.
5.5 Equipment
5.5.1 Availability of Equipment
Each PAS location is furnished with all equipment and instrumentation necessary to correctly
perform the tests offered in compliance with the specifications of the test method and to
achieve the accuracy and sensitivity required.
When a regulation, program, or reference test method requires Class A glassware for
quantitative measurements, only Class A glassware may be used. Plastic graduated cylinders,
even if marketed by the vendor as comparable to Class A glassware, may not be used when
Class A glassware is specified because ASTM’s definition and tolerances for Class A glass
cannot be applied to other materials.
5.5.2 Calibration
Equipment and instrumentation are checked prior to use to verify it performs within tolerance
for its intended application.
5.5.2.1 Support Equipment
The location confirms support equipment is in proper working order, uniquely
identified, and meets the specifications for use prior to placement in service. Periodic
checks are performed to verify tolerance and accuracy are performed thereafter in
accordance with a support equipment maintenance scheduled maintained by local
quality personnel. Equipment that does not meet specifications is removed from
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service until repaired or replaced. Records of repair and maintenance activities are
maintained.
Procedures used to conduct and record these checks are outlined in SOP ENV-SOP-
MTJL-0374, Support Equipment, ENV-SOP-MTJL-0047 Lockout/Tagout as well as
ENV-SOP-MTJL-0056 Instrument Transport.
5.5.2.2 Analytical Instruments
Analytical instruments are checked prior to placement in service in accordance with
SOP ENV-SOP-CORQ-0011 Method Validation and Instrument Verification. After the
initial service date, the calibration of instruments and verification calibration is
performed in accordance with local test method SOPs.
The calibration procedures in the test method SOPs comply with the requirements
for acceptable calibration practices outlined in corporate policy ENV-POL-CORQ-
0005 Acceptable Calibration Practices, the reference methods, and any applicable
regulatory or program requirements.
5.5.3 Equipment Use and Operation
Equipment is operated and maintained by personnel that are trained on the test method SOP.
Up-to-date instructions and procedures for the use and maintenance of analytical equipment
are included in SOPs and/or supplemental documents such as standard work instructions
(SWI) or instrument manuals which are made readily accessible in the work area to all
laboratory personnel.
5.5.4 Equipment Identification
Each piece of equipment must be uniquely identified by serial number or any other unique ID
system. The identifier is included in the equipment list maintained by the quality department
and may not be reused or used interchangeably. New equipment and replacement equipment
must be assigned a new unique ID.
5.5.5 Equipment Lists and Records
5.5.5.1 Equipment List
Each PAS location maintains a list of equipment that includes information about the
equipment including a description, manufacturer, serial number, date placed in
service, condition when received, identity, and the work area where the equipment is
used. The date of purchase is tracked by the procurement record. The equipment
list(s) for each location covered by this manual is provided in Appendix E.
5.5.5.2 Equipment Records
In addition to the equipment list, the location maintains records of equipment that
include:
Verification that equipment conforms with specifications.
Calibration records including dates, results, acceptance criteria, and next
calibration dates.
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Maintenance plan and records
Records of damage, malfunction, or repair
The laboratory follows an equipment maintenance program designed to optimize
performance and to prevent instrument failure which is described in SOP ENV-SOP-
MTJL-0373 Instrument Maintenance, ENV-SOP-MTJL-0374 Support Equipment, Env-
SOP-MTJL-0047 Lockout/Tagout as well as ENV-SOP-MTJL-0056 Instrument
Transport and/or in individual test method SOPs.
The maintenance program includes routine maintenance activities which are
performed as recommended by the manufacturer at the frequency recommended and
non-routine maintenance, which is performed to resolve a specific problem such as
degradation of peak resolution, shift in calibration relationship, loss of sensitivity, or
repeat failure of instrument performance checks and quality control samples.
Maintenance is performed by PAS personnel or by outside service providers.
All maintenance activities performed by PAS personnel are recorded by the
individual(s) that performed the activity at the time the maintenance was performed
in an instrument maintenance log.
The maintenance record minimally includes the date of maintenance, the initials of
the person(s) performing maintenance, a description of the activity performed, why
(when the maintenance is non-routine), and the return to analytical control. When
maintenance is performed by an external vendor, the service must be maintained and
accessible for easy retrieval. The location must provide personnel with unrestricted
access to instrument maintenance logs in order to promote good instrument
maintenance and recordkeeping practices.
If an instrument must be moved, the location will use safe practices for handling and
transport to minimize damage and contamination.
5.5.6 Out of Service Protocol
Equipment that has been subjected to overloading, mishandling, gives suspect results, has
been shown to be defective, or is performing outside of specified limits is taken out of service
and either removed from the work area or labeled to prevent accidental use until it has been
repaired and verified to perform correctly.
When analytical equipment is taken out of service because it no longer meets tolerance
specifications, the potential effect of the nonconformance may have had on previously
reported analytical results should be evaluated. (See section 4.9).
5.5.7 Calibration Status
The location labels support equipment to indicate calibration status, whenever practicable or
otherwise maintains the calibration status in a visible location in the work area. These
procedures are described in SOP ENV-SOP-MTJL-0373 Instrument Maintenance, ENV-
SOP-MTJL-0374 Support Equipment, Env-SOP-MTJL-0047 Lockout/Tagout as well as ENV-
SOP-MTJL-0056 Instrument Transport.
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The calibration status of analytical instruments is documented in the analytical record. Analysts
verify on-going acceptability of calibration status prior to use and with instrument
performance check standards. These procedures are described in test method SOPs.
5.5.8 Returned Equipment Checks
When equipment or an instrument is sent out for service, the location using the equipment
ensures that the function and calibration status of the equipment is checked and shown to be
satisfactory before the equipment is returned to service.
5.5.9 Intermediate Equipment Checks
The location performs intermediate checks on equipment to verify the on-going calibration
status. For example, most test methods require some form of continuing calibration
verification check, and these procedures are included in the test method SOP. Periodic checks
of support equipment are also performed; see ENV-SOP-MTJL-0373 Instrument Maintenance,
ENV-SOP-MTJL-0374 Support Equipment, Env-SOP-MTJL-0047 Lockout/Tagout as well as
ENV-SOP-MTJL-0056 Instrument Transport for more information.
5.5.10 Safeguarding Equipment Integrity
The location safeguards equipment integrity using a variety of mechanisms that include but
are not limited to:
Adherence to manufacturer’s specification for instrument use so that settings do not
exceed manufacturer’s recommendation or stress the performance of the equipment.
Established maintenance programs.
Transparent maintenance records and unrestricted access to maintenance logs.
Validation and approval of software before use.
Audits to confirm instrument settings are consistent with SOPs.
On-the-job training for safe and proper use of laboratory equipment.
5.6 Measurement Traceability
5.6.1 General
Measurement traceability refers to a property of a measurement result whereby the result can
be related to a reference through an unbroken chain of calibration, each contributing to the
measurement uncertainty. Traceability requires an established calibration hierarchy of
equipment (instruments) used during testing including equipment used for subsidiary
measurements. The location assures this equipment is calibrated prior to being put into service
and that the reference standard and materials used for calibration are traceable to the
international standard of units (SI) or national measurement standard.
When strict traceability to SI units cannot be made, the location establishes traceability with
the use of reference standards and equipment obtained from competent suppliers that provide
calibration certificates and/or certificates of analysis (COA).
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5.6.2 Equipment Correction Factors
When correction factors are used to adjust results the PAS personnel will assure that results
in computer software are also updated.
5.6.3 Specific Requirements
5.6.3.1 Requirements for Calibration Laboratories
The laboratory does not offer calibration services to customers; therefore, ISO/IEC
and TNI requirements for calibration laboratories do not apply.
5.6.3.2 Requirements for Testing Laboratories
The laboratory has procedures in place to verify equipment is calibrated prior to being
put into service (See 5.5.2) and ensures the reference standard and materials used for
calibration are traceable to the international standard of units (SI) or national
measurement standard. When strict traceability to SI units cannot be made, the
laboratory establishes traceability with the use of reference standards and equipment
obtained from competent suppliers that provide calibration certificates and/or
certificates of analysis (COA).
5.6.4 Reference Standards and Reference Materials
5.6.4.1 Reference Standards
The laboratory uses reference standards of measurement to verify adequacy of
working weights and thermometers. The working weights are the weight(s) used for
daily balance calibration checks and the working thermometers are used for daily
temperature measurements.
Working weights and thermometers must be periodically checked to verify on-going
adequacy for use between calibrations performed by an external calibration laboratory
using reference standards traceable to SI or a national standard and that are used solely
for verification purposes.
For example:
An acceptable reference standard to check working thermometers against include
a NIST Certified Thermometer or a NIST Traceable Thermometer that is not
used for any other purpose than to check the adequacy of the working
thermometer.
An acceptable reference standard for the working weights is a set of Class S
weights that is not used for any other purpose than to verify the weights used
daily.
The working weights must be checked against the reference standard annually and all
weight sets must be recertified by an ISO accredited calibration body every 5 years.
In this application, “annually” means within thirteen (13) months from the date of
the last check.
Working thermometers must be checked against the reference thermometer prior to
placement in service to establish a correction factor (CF)1 and then re-checked
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annually (±13 months from date of last check) or if battery operated, every three (3)
months (±100 days from date of last check).
Exceptions to the 3-month recheck for battery operated sensors are allowed when
the sensor is embedded in a unit and the manufacturer/vendor has evidence to show
that the accuracy of the sensor is not affected by battery life.
Liquid in Glass NIST Certified reference thermometers must be recertified by an
ISO/IEC accredited calibration laboratory every 5 years. If the reference
thermometer is NIST Traceable or is a digital NIST Certified thermometer, the
reference thermometer must be recertified annually by an ISO/IEC 17025 accredited
calibration laboratory or service provider that provides traceability to a national
standard.
If criteria for the intermediate checks or recertification is not acceptable, the impact
on previously reported results is evaluated using the process for evaluation of
nonconforming work (See 4.9).
See SOP ENV-SOP-MTJL-0373 Instrument Maintenance, ENV-SOP-MTJL-0374,
Support Equipment, Env-SOP-MTJL-0047 Lockout/Tagout as well as ENV-SOP-MTJL-
0056 Instrument Transport for more information.
5.6.4.2 Reference Materials
The location purchases chemical reference materials (also known as stock standards)
from vendors that are accredited to ISO 17034 or Guide 34. Purchased reference
materials must be received with a Certificate of Analysis (COA) where available. If a
reference material cannot be purchased with a COA, it must be verified by analysis
and comparison to a certified reference material and/or there must be a
demonstration of capability for characterization. COA are reviewed for adequacy and
retained by the laboratory for future reference.
All prepared standards, reference materials, and reagents are verified to meet the
requirements of the test method through routine analyses of quality control samples.
The laboratory procedure for traceability and use of these materials is provided in
SOP ENV-SOP-MTJL-0041 Standards Logger-Tree Operation, ENV-SOP-MTJL-0023
Storage of Consumables, and ENV-SOP-MTJL-0042 Standards Recertification.
This SOP includes each of the following requirements:
Procedures for documentation of receipt and tracking. The record of entry
includes name of the material, the lot number, receipt date, and expiration date.
Storage conditions and requirements. Reference materials must be stored
separately from samples, extracts, and digestates.
Requirements to assure that preparations of intermediate or working solutions
are recorded and assigned a unique identification number for tracking. Records
of preparation include the lot number of the stock standard(s) used, the type and
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lot number of the solvent, the formulation, date, expiration date, and the
preparer’s initials. The lot number of the working standards is recorded in the
analytical record to provide traceability to the standard preparation record. The
preparation record provides traceability to the COA, which is traceable to SI or
the national measurement standard.
A requirement that the expiration dates of prepared standards may not exceed
the expiration date of the parent standard. Standards, reference materials, and
reagents are not used after their expiration dates unless it is not possible to
procure a new standard and the reliability of the expired material is verified and
documented by the location using a procedure approved by corporate quality
personnel. Otherwise, the expired material is promptly removed from the work
area or clearly labeled as acceptable for qualitative/troubleshooting purposes
only.
The second source materials used for verification of instrument calibration are
obtained from a different manufacturer or may be a different lot from the same
manufacturer.
Procedures to check reference materials for degradation and replacement of
material if degradation or evaporation is suspected.
Procedures for labeling. At a minimum, the container must identify the material,
the ID of the material and the expiration date. Original containers should also be
labeled with date opened.
5.6.4.3 Intermediate Checks
Checks to confirm the calibration status of reference standards and materials must be
included in test method SOPs. These checks include use of second source standards
and reference materials reserved only for the purpose of calibration checks.
5.6.4.4 Transport and Storage
The location handles and transports reference standards and materials in a manner
that protects the integrity of the materials. Reference standard and material integrity
is protected by separation from incompatible materials and/or minimizing exposure
to degrading environments or materials. Standards and reference materials are stored
separately from samples, extracts, and digestates. All standards are stored according
to the manufacturer’s recommended conditions. Temperatures colder than the
manufacturer’s recommendation are acceptable if it does not compromise the
integrity of the material (e.g., remains in liquid state and does not freeze solid). In the
event a standard is made from more than a single source with different storage
conditions, the standard will be stored according to the conditions specified in the
analytical method.
See the applicable analytical SOPs for specific reference material storage and transport
protocols.
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5.7 Sampling
Sampling refers to the field collection of samples and to subsamples taken by the laboratory for
analysis from the field collected sample.
Subsampling procedures are included in each test method SOP or a stand-alone SOP to assure the
aliquot used for testing is representative of the field collected sample.
The requirements in the following subsections apply when field sampling is performed by PAS.
5.7.1 Sampling Plans and SOPs
When PAS performs field collection of samples, sampling is carried out in accordance with a
written sampling plan and sampling SOPs. These documents are made readily accessible at
the sampling location. Sampling plans and SOPs are, whenever reasonable, based on
appropriate governing methods and address the factors to be controlled to ensure the validity
of the analytical results.
5.7.2 Customer Requested Deviations
When the customer requires deviations, additions, or exclusions from the documented
sampling plan and/or procedure, the laboratory records the client’s change request in detail
with the sampling record, communicates the change to sampling personnel, and includes this
information in the final test report.
5.7.3 Recordkeeping
PAS assures the sampling record includes the sampling procedure used, any deviations from
the procedure, the date and time of sampling, the identification of the sampler, environmental
conditions (if relevant), and the sampling location.
5.8 Sample Management & Handling
5.8.1 Procedures
The location’s procedures for sample management and handling are outlined in SOP
ENV-SOP-MTJL-0045 Sample Dilution Policy, ENV-SOP-MTJL-0060 Sample Receiving,
ENV-SOP-MTJL-0061 Sample Storage, Disposal and Sample Control Technicians, ENV-SOP-
MTJL-0064 Sample Shipping, and ENV-SOP-MTJL-0066 Cold Storage Management.
The procedures in these SOPs are established to maintain the safe handling and integrity of
samples from transport, storage, to disposal and during all processing steps to maintain client
confidentiality, and to protect the interests of PAS and its customers.
5.8.1.1 Chain of Custody
All samples received by the location must be accompanied with a Chain of Custody
(COC) record. The COC provides information about the samples collected and
submitted for testing and documents the possession of samples from time of
collection to receipt by the location.
The COC record must minimally include the following information:
Client name, address, phone number;
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Project Reference;
Client Sample Identification (Client ID);
Date, Time, and Location of Sampling;
Sampler’s Name or Initials;
Matrix;
Type of container, and total number collected for each sample;
Preservatives;
Analyses Requested;
Mode of collection;
Any special instructions; and
The date and time and signature of each sample transfer from time of collection
to receipt in the location. When the signature field on CoC includes company.
Personnel relinquishing and/or receiving samples are expected to record this
information. When the COC is transported inside the cooler, independent
couriers do not sign the COC and the shipping manifests and/or air bills are the
records of possession during transport. The shipping manifest must be retained
as part of the COC record and included in the test report when required (See
Section 5.10.3).
A complete and legible COC is required. If the location observes that the COC is
incomplete or illegible, the client is contacted for resolution. The COC must be filled
out in indelible ink. Personnel correct errors by drawing a single line through the initial
entry, so the entry is not obscured, entering the correct information, and initialing,
and dating the change.
5.8.1.2 Legal Chain of Custody
Legal chain of custody is a chain of custody protocol used for evidentiary or legal
purposes. The protocol is followed by the location when requested by customer or
when mandated by a regulatory program.
Legal chain of custody (COC) protocol establishes an intact, continuous record of the
physical possession*, storage, and disposal of “samples” which includes sample
aliquots, and sample extracts/digestates/distillates.
Legal COC records account for all time periods associated with the samples and
identifies all individuals who physically handled individual samples. Legal COC begins
at the point established by legal authority, which is usually at the time the sample
containers are provided by the location for sample collect or when sample collection
begins.
*A sample is in someone’s custody if:
It is in one’s physical possession;
It is in one’s view after being in one’s physical possession;
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It has been in one’s physical possession and then locked or sealed so that no one
can tamper with it; and/or
It is kept in a secure area, restricted to authorized personnel only.
Refer to SOP ENV-SOP-MTJL-0060 Sample Receiving for more information.
5.8.2 Unique Identification
Each sample is assigned a unique identification number (Lab ID) after the sample has been
checked and accepted by PAS in accordance with the PAS sample acceptance policy (See
5.8.3). The Lab ID is affixed to the sample container using a durable label.
The unique identification of samples also applies to subsamples, and prepared samples.
The lab ID is linked to the field ID (client ID) in the receipt and log-in record. Both IDs are
linked to the testing activities performed on the sample and the documentation records of the
test.
Also see 5.8.4.
5.8.3 Sample Receipt Checks and Sample Acceptance Policy
The location checks the condition and integrity of samples on receipt and compares the labels
on the sample containers to the COC record. Any problem or discrepancy is recorded. If the
problem impacts the suitability of the sample for analysis or if the documentation is
incomplete, the client is notified for resolution. Decisions and instructions from the client are
maintained in the project record.
5.8.3.1 Sample Receipt Checks
The following checks are performed:
Verification that the COC is complete and legible.
Verification that each sample’s container label includes the client sample ID, the
date and time of collection and the preservative in indelible ink.
The container type and preservative are appropriate for each test requested.
Adequate volume is received for each test requested.
Visual inspection for damage or evidence of tampering.
Visual inspection for presence of headspace in VOA vials. (VOA = volatile
organic analysis).
Thermal Preservation: For chemical testing methods for which thermal
preservation is required, temperature on receipt is typically considered acceptable
if the measurement is above freezing but <6°C unless otherwise specified by
federal, statutory, program or test method requirements. Refer to the location’s
SOP for sample receipt for specific thermal preservation requirements.
For samples that are hand-delivered to the location immediately after sample
collection, there must be evidence that the chilling process began immediately
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after sample collection and prior to delivery of the samples to the laboratory or
service center, such as arrival of the samples on ice.
Chemical Preservation
Holding Time: Sample receiving personnel are trained to recognize tests where
the holding time is 48 hours or less and to expedite the log-in of these samples.
Except for tests with immediate holding times (15 minutes from time of
collection or less), when samples are received out of hold, the location will notify
the client and request instruction. If the decision is made to proceed with analysis,
the final test report will include notation of this instruction.
5.8.3.2 Sample Acceptance Policy
PAS maintains a sample acceptance policy in accordance with regulatory guidelines to
clearly establish the circumstances in which sample receipt is accepted or rejected.
When receipt does not meet criteria for any one of these conditions, the location must
document the noncompliance, contact the customer, and either reject the samples or
fully document any decisions to proceed with testing. In accordance with regulatory
specifications, test results associated with receipt conditions that do not meet criteria
are qualified in the final test report.
All samples received must meet each of the following criteria:
Be listed on a complete and legible COC;
Be received in properly labeled sample containers;
Be received in appropriate containers that identify preservative;
The COC must include the date and time of collection for each sample;
The COC must include the test method requested for each sample;
Be in appropriate sample containers with clear documentation of the
preservatives used;
Be received within holding time. Any samples received beyond the holding time
will not be processed without prior customer approval;
Have sufficient sample volume to proceed with the analytical testing. If
insufficient sample volume is received, analysis will not proceed without customer
approval; and
Be received within appropriate temperature ranges unless program requirements
or customer contractual obligations mandate otherwise.
Samples that are delivered to the location immediately after collection are
considered acceptable if there is evidence that the chilling process has been
started. For example, by the arrival of the samples on ice. If samples arrive that
are not compliant with these temperature requirements, the customer will be
notified. The analysis will NOT proceed unless otherwise directed by the
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customer. If less than 72 hours remain in the hold time for the analysis, the
analysis may be started while the customer is contacted to avoid missing the hold
time. Data associated with any deviations from the above sample acceptance
policy requirements will be appropriately qualified.
5.8.4 Sample Control and Tracking
The samples are controlled and tracked using the Laboratory Information Management
System (LIMS). The LIMS stores information about the samples and project. The process of
entering information into the LIMS is called log-in and these procedures are described in SOP
ENV-SOP-MTJL-0060 Sample Receiving. After log-in, a label is generated and affixed to
each sample container. Information on this label, such as the lab ID, links the sample container
to the information in LIMS.
At a minimum, the following information is entered during log-in:
Client Name and Contact Information;
The laboratory ID linked to the client ID;
Date and time of sample collection;
Date and time of sample receipt;
Matrix; and
Tests Requested.
5.8.5 Sample Storage, Handling, and Disposal
The location procedures for sample storage, handling and disposal are detailed in SOPs
ENV-SOP-MTJL-0061 Sample Storage, Disposal and Sample Control Technicians and ENVSOP-
MTJL-0066 Cold Storage Management as well as test method SOPs.
5.8.5.1 Sample Storage
The samples are stored according to method and regulatory requirements as per test
method SOPs. Samples are stored away from all standards, reagents, or other potential
sources of contamination and stored in a manner that prevents cross contamination.
Volatile samples are stored separately from other samples. All sample fractions,
extracts, leachates, and other sample preparation products are stored in the same
manner as actual samples or as specified by the analytical method.
Refrigerated storage areas are maintained at (but not frozen) and freezer storage
areas are maintained at <-10°C, unless otherwise required per method or program.
The temperature of each storage area is checked and documented at least once for
each day of use. If the temperature falls outside the acceptable limits, then corrective
actions are taken and appropriately documented.
The location is operated under controlled access protocols to ensure sample and data
integrity. Visitors must register at the front desk and be properly escorted while on-
site. Samples are taken to the appropriate storage location immediately after sample
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receipt and log-in procedures are completed. All sample storage areas have limited
access. Samples are removed from storage areas by designated personnel and returned
to the storage areas as soon as possible after the required sample quantity has been
taken.
5.8.5.2 Sample Retention and Disposal
The procedures used by the location for sample retention and disposal are detailed in
SOP ENV-SOP-MTJL-0061 Sample Storage, Disposal and Sample Control Technicians and
ENV-SOP-MTJL-0066 Cold Storage Management.
In general, unused sample volume and prepared samples such as extracts, digestates,
distillates and leachates (samples) are retained by the location for the timeframe
necessary to protect the interests of the location and the customer.
Samples may be stored at ambient temperature when all analyses are complete, the
hold time is expired, the report has been delivered, and/or when allowed by the
customer or program. Samples requiring storage beyond the minimum sample
retention time due to special requests or contractual obligations may be stored at
ambient temperature unless the location has a capacity, and their presence does not
compromise the integrity of other samples.
After this period expires, non-hazardous samples are properly disposed of as non-
hazardous waste. The preferred method for disposition of hazardous samples is to
return the excess sample to the customer.
5.9 Assuring the Quality of Test Results
5.9.1 Quality Control (QC) Procedures
The location monitors the validity and reliability of test results using quality control (QC)
samples that are prepared and analyzed concurrently with field samples in the same manner as
field samples. QC results are always associated to and reported with the field samples they
were prepared and analyzed with from the same preparation or analytical batch. See the
glossary for definition of preparation and analytical batch.
The results of QC performed during the testing process are used by the location to assure the
results of analysis are consistent, comparable, accurate, and/or precise within a specified limit.
When the results are not within acceptance criteria or expectations for method performance,
correction and corrective action(s) are taken. These actions may include retesting or reporting
of data with qualification to alert the end user of the situation.
Other QC measures performed include the use of certified reference materials (see 5.6.4),
participation in interlaboratory proficiency testing (see 5.9.1.2), verification that formulae used
for reduction of data and calculation of results is accurate (see 5.9.3), on-going monitoring of
environmental conditions that could impact test results (see 5.3.2), and evaluation and
verification of method selectivity and sensitivity (see 5.4.5).
QC results are also used by the location to monitor performance statistical trends over time
and to establish acceptance criteria when no method or regulatory criteria exist. (See 5.9.1.1.9)).
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5.9.1.1 Essential QC
Although the general principles of QC for the testing process apply to all testing, the
QC protocol used for each test depends on the type of test performed.
QC protocol used by the location to monitor the validity of the test are specified in
test method SOPs. The SOP includes QC type, frequency, acceptance criteria,
corrective actions, and procedures for reporting of nonconforming work.
These requirements in the SOP conform to the reference method and any applicable
regulations or certification and accreditation program requirement for which results
of the test are used. When a project requires more stringent QC protocol than
specified in the SOP, project specification is followed. When the project requires less
stringent QC protocol, the project specification may be followed as an authorized
departure from the SOP when the project specifications meet the requirements in the
mandated method and any regulatory compliance requirements for which the data
will be used.
The following are examples of essential QC for chemistry. These concepts may not
apply to other technologies and disciplines such as microbiology, radiochemistry,
whole effluent toxicity, and/or asbestos. For essential QC for these disciplines, refer
to test method SOPs.
5.9.1.1.1 Second Source Standard (ICV/QCS)
The second source standard is a standard obtained from a different
vendor than the vendor of the standards used for calibration, or
from a different lot from the same vendor, when only one vendor is
available. It is a positive control used to verify the accuracy of
instrument calibration relative to the purity of the standards used for
calibration. This check may be referred to in published test methods
and quality system standards as the initial calibration verification
(ICV) or a quality control sample (QCS). The second source
standard is analyzed immediately after the calibration and before
analysis of any samples. When the ICV is not within acceptance
criteria, a problem with the purity or preparation of the standards
may be indicated. The source of the problem should be investigated
and corrected prior to further use of the calibration/instrument for
sample analysis.
5.9.1.1.2 Continuing Calibration Verification (CCV)
The CCV is used to determine if the analytical response has
significantly changed since calibration. If the response of the CCV is
within criteria, the calibration is considered valid. If not, there is a
problem that requires further investigation and correction. Actions
taken are technology and method specific.
5.9.1.1.3 Method Blank (MB) / Other Blanks
The MB is a negative control used to assess for contamination during
the prep/analysis process. The MB consists of a clean matrix, similar
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to the associated samples that is known to be free of analytes of
interest. The MB, unless otherwise specified by the test method, is
processed with, and carried through all preparation and analytical
steps as the associated samples.
The criteria used to assess for contamination depends on the
intended use of data. In general, detections in the MB above the RL
or ½ the RL indicate contamination. When contamination is evident,
the source is investigated, and corrections are taken to reduce or
eliminate it. Analytical results associated with MB that does not meet
criteria are qualified in the final test report.
Other types of blanks that serve as negative controls in the process
may include:
Trip Blanks (VOA)
Storage Blanks
Equipment Blanks
Field Blanks
Calibration Blanks
Cleanup Blanks
Instrument Blanks
5.9.1.1.4 Laboratory Control Sample (LCS)
The LCS is a positive control used to measure the accuracy of
process in a blank matrix. The LCS is spiked by the laboratory with
a known amount of analyte. The spike is a standard solution that is
pre-made or prepared from a certified reference standard. Like the
MB, unless otherwise specified in the test method, the LCS is
processed with and carried through all preparation and analytical
steps as the associated samples.
When the percent recovery (%R) of the LCS is within the established
control limit, sufficient accuracy has been achieved. If not, the
source of the problem is investigated and corrected, and the
procedure may be repeated. Analytical results associated with LCS
that does not meet criteria are qualified in the final test report.
5.9.1.1.5 Matrix Spike (MS) and Matrix Spike Duplicate (MSD)
The MS and MSD are replicates of a client sample that is spiked with
known amount of target analyte. Matrix spikes measure the effect
the sample matrix has on precision and accuracy of test results.
Matrix spike results mostly provide information on the effect of the
matrix to the client whose sample was used and on samples of the
same matrix from the same sampling site, during the same sampling
event. Consequently, matrix spikes should be client designated.
When there is not a client-specified MS for any sample in the batch,
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the location randomly selects a sample from the batch; the sample
selected at random is called a “batch” matrix spike.
The MS/MSD results for percent recovery and relative percent
difference are checked against control limits. However, because the
performance of matrix spikes is matrix-dependent and specific to the
customer whose sample was used as the MS/MSD, the results of
matrix spikes are not used for quality control on the batch.
5.9.1.1.6 Sample Duplicate (SD)
A sample duplicate is a second replicate of sample that is used to
measure precision.
The relative percent difference between replicates are evaluated
against the established acceptance criteria for relative percent
difference (RPD) when this criterion is applicable. If RPD is not met,
associated test results are reported with qualification.
5.9.1.1.7 Surrogates
Surrogates are compounds that mimic the chemistry of target
analytes but are not expected to occur naturally in real world
samples. Surrogates are added to each sample and matrix QC
samples (MS, MSD, SD) at known concentration to measure the
impact of the matrix on the accuracy of method performance.
Surrogates are also added to the positive and negative control
samples (MB, LCS) to evaluate performance in a clean matrix, and
included in the calibration standards and calibration check standards.
The percent recovery of surrogates is evaluated against method-
specified limits or statistically derived in-house limits. Project-
specific limits and/or program-specific limits are used when
required. Results with surrogate recovery out of limits in samples are
reported with qualification. Samples with surrogate failures can also
be re-extracted and/or re-analyzed to confirm that the out-of-
control value was caused by the matrix of the sample and not by
some other systematic error.
5.9.1.1.8 Internal Standards
Internal Standards are compounds not expected to occur naturally
in field samples. They are added to every standard and sample at a
known concentration prior to analysis for the purpose of adjusting
the response factor used in quantifying target analytes. The location
follows specific guidelines for the treatment of internal standard
recoveries and further information can be found in the applicable
test method SOP.
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5.9.1.1.9 QC Acceptance Criteria and Control Limits
The QC acceptance criteria are specified in test method SOPs. The
criteria in the SOP are based on the requirements in the published
test method or regulatory program. When there are no established
acceptance criteria, the location develops acceptance criteria in
accordance with recognized industry standards.
Some methods and programs require the location to establish
control limits for LCS, MS/MSD, and surrogate evaluation using
historical data. PAS developed limits are referred to as “in-house”
control limits. In-house control limits represent ± 3 Standard
Deviations (99% confidence level) from the average recovery of at
least 20 data points generated using the same preparation and
analytical procedure in a similar matrix.
See SOP ENV-SOP-MTJL-0017 Generation of Control Limits for more
information about the procedures used to establish in-house control
limits.
5.9.1.2 Proficiency Testing (PT)
PAS locations participate in interlaboratory proficiency testing (PT) studies to
measure performance of the test method and to identify or solve analytical problems.
PT samples measure location performance through the analysis of unknown samples
provided by an external source.
The frequency of PT participation is based on the certification and accreditation
requirements held by the laboratory. The PT samples are obtained from accredited
proficiency testing providers (PTP) and treated as field samples which means they are
included in the location’s normal analytical processes and do not receive extraordinary
attention due to their nature.
PAS locations do not share PT samples with other PAS locations, does not
communicate with other PAS locations regarding current PT sample results during
the duration of the study, and does not attempt to obtain the assigned value of any
PT sample from the PT provider.
PT results scored unacceptable are investigated and correction action taken, when
necessary.
Refer to corporate policy ENV-POL-CORQ-0002 PT Policy for more information.
5.9.2 QC Corrective Action
When the results of QC are not within acceptance criteria or expectations for method
performance, correction and corrective action(s) are taken per the specifications in the test
method SOP. These actions may include retesting or reporting of data with qualification to
alert the end user of the situation.
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5.9.3 Data Review
PAS locations use a tiered system for data review. The tiered process provides sequential
checks to verify data transfer is complete; manual calculations, if performed, are correct,
manual integrations are appropriate and documented, calibration and QC requirements are
met, appropriate corrective action was taken when required, test results are properly qualified,
process and test method SOPs were followed, project specific requirements were met, when
applicable, and the test report is complete.
The sequential process includes three tiers referred to as primary review, secondary review,
and administrative/completeness review.
Detailed procedures for the data review process are described in SOP ENV-SOP-MTJL-0038
Data Review. The general expectations for the tiered review process are described in the
following sections:
5.9.3.1 Primary Review
Primary review is performed by the individual that performed the task. All PAS
personnel are responsible for review of their work product to assure it is complete,
accurate, documented, and consistent with policy and SOPs.
Checks performed during primary review include but are not limited to:
Verification that data transfer and acquisition is complete
Manual calculations, if performed, are documented and accurate
Manual integrations, if performed, are documented, and comply with SOP ENV-
SOP-CORQ-006 Manual Integration
Calibration and QC criteria were met, and/or proper correction and corrective
actions were taken, and data and test results associated with QC and criteria
exceptions are properly qualified
Work is consistent with SOPs and any other relevant instructional document such
as SWI, program requirements, or project QAPP
5.9.3.2 Secondary Review
Secondary review is performed by a qualified peer or supervisor. Secondary review is
a repeat of the checks performed during primary review by another person. In
addition to the checks of primary review, secondary review includes chromatography
review to check the accuracy of quantitative analyte identification.
5.9.3.3 Completeness Review
Completeness review is an administrative review performed prior to release of the test
report to the customer. Completeness review verifies that the final test report is
complete and meets project specification. This review also assures that information
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necessary for the client’s interpretation of results are explained in the case narrative
or footnoted in the test report.
5.9.3.4 Data Audits
Test reports may be audited by local quality personnel to verify compliance with SOPs
and to check for data integrity, technical accuracy, and compliance with the PAS QMS
and any applicable federal, statutory, and program requirements. The reports chosen
for the data audits are selected at random and these audits are not usually done prior
to issuance of the test report to the customer.
If any problems with the data or test results are found during the data audit, the impact
of the nonconforming work is evaluated using the process described in Section 4.9.
Also see Section 4.14 for internal audits.
5.9.4 Calibration Certificates
PAS does not perform calibration activities for its customers and calibration certificates are
not offered or issued.
5.9.5 Opinions and Interpretations
The location provides objective data and information to its customers of sufficient detail for
their interpretation and decision making. Objective data and information are based solely on
fact and does not attempt to explain the meaning (interpret) or offer a view or judgement
(opinion). Sometimes the customer may request the location provide opinion or interpretation
to assist them with their decisions about the data.
When opinions and interpretations are included in the test report, the location will document
the basis upon which the opinions and interpretations have been made and clearly identify this
content as opinion or interpretation in the test report.
Examples of opinion and interpretation include but are not limited to:
A viewpoint on how a nonconformance impacts the quality of the data or usability of
results.
Recommendations for how the customer should use the test results and information.
Suggestions or guidance to the customer for improvement.
5.9.6 Subcontractor Reports
When analytical work has been subcontracted to an organization external to PAS, the test
report from the subcontractor is included in its entirety as an amendment to the final test
report.
Test results performed by multiple locations within the PAS network (internal subcontracting)
may be merged into a single test report so long as the test report issued clearly identifies the
location and address of each network location that performed testing, and which tests each
PAS location performed. (See 5.10.2)
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5.9.7 Electronic Transmission of Results
When test results and/or reports are submitted to the customer through electronic
transmission, the procedures established in this manual for confidentiality and protection of
data apply.
5.9.8 Format of Test Reports
The test formats offered by PAS are designed to accommodate each type of analytical test
method performed and to minimize the possibility of misunderstanding or misuse of analytical
results. The format of electronic data deliverables (EDD) follows the specifications for the
EDD.
5.9.9 Amendments to Test Reports
Test reports that are revised or amended by the location after date of release of the original
final test report to the customer are issued as a new test report that is clearly identified as an
amendment or revision and that includes a reference to the originally issued final test report.
The customer is the organization doing business with PAS external to PAS.
Changes made to test results and data before the final test report is issued to the customer are
not amendments or revisions, these are corrections to errors found during the location’s data
verification and review process.
The procedure for report amendments and revision are outlined in SOP ENV-SOP-MTJL-
0014 Data Handling and Reporting and ENV-SOP-MTJL-0033 Report Revision.
5.10 Reporting
5.10.1 General Requirements
PAS offers a wide variety of test report formats to meet project needs of Pace® customers
and that comply with federal and state regulatory programs.
The type and level of deliverable, including the electronic data deliverable (EDD) format are
established between PAS and the customer during the contracting process. The report
specifications include the test report format, protocol for the reporting limit (RL), conventions
for the reporting of results less than the limit of quantitation (LOQ), and specification for the
use of project or program specific data qualifiers. Information about review of analytical
service requests is provided in Section 4.4.
5.10.2 Test Reports: Required Items
Regardless of deliverable or report requested, every test report issued by the location includes
each of the following items:
a) A Title
b) The name and address of the location issuing the test report and for each location where
testing was performed if different than address of the location issuing the report. When
testing is done at multiple PAS locations, the report must clearly identify which PAS
location performed each test method;
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c) Unique identification of the test report and on each page an identification number to link
each page to the test report, and clear identification of the end of the report.
d) The name and address of the customer
e) Identification of test methods used
f) Cross reference between client sample identification number (Sample ID) and the
identification number for the sample (Lab ID) to provide unambiguous identification of
samples.
g) The date of receipt of samples, condition of samples on receipt, and identification of any
instance where receipt of the samples did not meet sample acceptance criteria.
h) Date and times of sample collection, receipt, preparation, and analysis.
i) Test results and units of measurement, and qualification of results associated with QC
criteria exceptions, and identification of reported results outside of the calibration range.
j) All chains of custody (COC) including records of internal transfer between locations
within PAS,
k) Name, title, signature of the person(s) authorizing release of the test report and date of
release.
l) A statement that the results in the test report relate only to the items tested.
m) Statement that the test report may not be reproduced except in full without written
approval from PAS.
5.10.3 Test Reports: Supplemental Items
5.10.3.1 Supplemental Requirements
The following items are included in the test report when required or relevant:
a) Shipping manifests / bill of ladings as applicable when common couriers are
utilized for shipment of samples,
b) Explanation of departure from test method SOPs including, what the departure
was and why it was necessary.
c) Statistical methods used. (Required for Whole Effluent Toxicity)
d) For solid samples, specification that results are reported on a dry weight or wet
weight basis.
e) Signed Affidavit, when required by client or regulatory agency.
f) A statement of compliance / non-compliance with requirements or specifications
(client, program, or standard) that includes identification of test results that did
not meet acceptance criteria.
g) When requested by the client, statement of estimated measurement uncertainty.
In general, for environmental testing, estimated uncertainty of measurement is
extrapolated from LCS control limits. Control limits incorporate the expected
variation of the data derived from the laboratory’s procedure. When the control
limits are specified by the test method or regulatory program, the control limits
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represent the expected variation of the test method and/or matrices for which
the test method was designed.
h) Opinions and Interpretations
i) If a claim of accreditation/certification is included in the test report, identification
of any test methods or analytes for which accreditation/certification is not held
by the location if the accrediting body offers accreditation/certification for the
test method/analyte. The fields of accreditation/certification vary between
agencies, and it cannot be presumed that because accreditation/certification is
not held that it is offered or required.
j) Certification Information, including certificate number and issuing body.
For PAS locations accredited to ISO/IEC 17025:2017:
Data included in the test report provided by a customer should be clearly
identified. The test report should also include a statement that the test results
apply only to the samples as received.
5.10.3.2 Test Reports: Sampling Information
The following items are included in the test report when samples are collected by PAS
or when this information is necessary for the interpretation of test results:
a) Date of Sampling.
b) Unambiguous identification of material samples.
c) Location of sampling including diagrams, sketches, or photographs.
d) Reference to the sampling plan and procedures used.
e) Details of environmental conditions at time of sample that may impact test
results.
f) Any standard or other specification for the sampling method or procedure, and
deviations, additions to or exclusions from the specification concerned.
6.0 REVISION HISTORY
This Version (Version 2):
Section Description of Change
Header / All Added registered trademark after Pace as required by branding guidelines
Header Updated the years associated with the copyright.
Signature Page Removed Cover Page applied by MasterControl eDMS
Approval Signatory Changed name of this page to “Management Personnel” and updated Job Titles.
All Changed references to “laboratory” with PAS or location, where appropriate.
All Replaced stand-alone acronym “ENV” with “PAS” except where “ENV” is
embedded in document control numbers.
All Corrected spelling, typographical, and format errors.
Various
Added language to clarify the examples in the manual are provided for chemistry,
these examples may not apply in the same way to other disciplines such as
radiochemistry, microbiology, asbestos, or whole effluent toxicity (WET).
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1.0 Corrected Parent Company Information.
1.2 Added definitions for “location,” “laboratory” and “service center” for QMS and
compliance purposes.
1.2.1 Updated job titles to match current structure.
1.2.2 Revised language for clarity.
1.2.3 Removed specificity to allow for more options
4.1.4 Updated to describe current scope of organization
4.1.4.1 Updated to describe current organization structure
4.1.5.1.1 Updated to match new organization structure and job titles
4.1.5.2 Updated to match new organization structure and job titles
4.1.5.2.1 Updated to clarify qualifications and meaning of “absent”
4.1.5.3 Updated to clarify impartiality
4.1.5.4 Reorganized section for clarity
4.2.1.1 Added statement that the organization structure is designed to safeguard impartiality
4.2.2.1 Added requirement to post compliance alertline posters in work area.
4.2.1.3 Added requirement for policies and procedures to be available in work area
(previously implied but not explicitly stated)
4.2.5.1 Clarified hierarchy and application of project documents
4.5 Updated requirements for internal and external subcontracting
4.8 Updated complaint handling requirements to clarify that only valid complaints are
acted on with corrective action.
4.9.1.3 Added roles responsible for authorizing return to work after stop work order.
4.11 Main and subsections updated for clarity
4.14 Main and subsections updated for clarity
5.2.2 Subsections
Content reorganized and language related to documentation of training and
authorization of personnel revised to clarify expectations. Requirements of DOCs
modified to clarify procedure described in manual pertains to chemistry
methodology; other approaches to DOC acceptable for other disciplines such as
microbiology, radiochemistry, asbestos, whole effluent toxicity.
5.4.5.3.3 Added reference documents for which the local SOP for LOD must comply with.
5.5 Added language to clarify existing requirements.
5.6.4
Clarified requirements for reference standards for working weights and
thermometers and defined meaning of terms “annual” and “quarterly.” Included
examples of acceptable reference standards for adequacy checks.
5.8.1
Added recommendation for Pace® personnel to add “Pace®” next to their
signature on the CoC when receiving samples since the CoC form has
signature/company, implying the company affiliation must be added.
5.10.3.1 Included ISO/IEC 17025:2017 to add disclaimer to test reports (applies to
laboratories accredited to ISO/IEC 17025:2017 only).
Addendum Added AIHA, Radiological and Calculation addendums
This document supersedes the following documents:
Document Number Title Version
ENV-MAN-MTJL-0001 Quality Manual 02
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7.0 APPENDICES
7.1 Appendix A: Certification / Accreditation Listing
Disclaimer: The certifications / accreditation lists provided in this Appendix are those that were held by the
PAS location on the effective date of this manual. This information is subject to change without notice and
must not be considered valid proof of certification or accreditation status. This manual is not updated with each
change made. Current certificates are accessible via the eDMS Portal for PAS employees. External parties should
contact the location for the most current information.
7.1.1 PAS-Mt. Juliet
Authority ID Authority ID
Alabama 40660 North Carolina Env375
Alaska UST-080 North Dakota R-140
Arizona AZ0612 Ohio EPA/VAP CL0069
Arkansas 88-0469 Oklahoma 9915
California 2932 Oregon TN200002
Colorado None Pennsylvania 68-02979
Connecticut PH-0197 Rhode Island 221
Florida E87487 South Carolina 84004
Georgia DW 923 South Dakota Pending
Georgia None Tennessee DW 2006
Idaho TN00003 Tennessee DW Micro 2006
Illinois 200008 Texas-Env.T 104704245-07-TX
Indiana C-TN-01 Texas-Mold LAB0152
Iowa 364 Utah TN000032019-9
Kansas E-10277 Vermont VT2006
Kentucky DW 90010 Virginia VELAP 460132
Kentucky UST 16 Washington C1915
Kentucky WW 90010 West Virginia 233
Louisiana Agency ID 30792 West Virginia Crypto 9966 M
Louisiana DW LA150002 Wisconsin 998093910
Maine TN0002 Wyoming A2LA
Maryland 324 A2LA 1461.01
Massachusetts M-TN003 AIHA-LAP 100789
Michigan 9958 DOD 1461.01
Minnesota 047-999-395 EPA TN00003
Mississippi None EPA Region 8
Missouri 340 USDA S-67674
Montana CERT0086
Nebraska NA
Nevada TN-03-2002-34
New Hampshire 2975
New Jersey-NELAP TN002
New Mexico None
New York 11742
North Carolina
Aquatic Tox.
41
North Carolina DW DW21704
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7.2 Appendix B: Capability Listing
The capabilities listed in this Appendix were held by the location referenced on the effective date of
this manual. This information is subject to change without notice. External parties should contact the
location for the most current information.
Table Legend:
Air = Air
DW = Drinking Water
NPW = Non-Potable Water
SCM = Solid and Chemical Materials
Waste = Non-Aqueous Phase Liquid (NAPL), Oil
Tissue = Biota and Tissue
7.2.1 PAS-Mt. Juliet
MatricesParameterMethod
Air DW NPW SCM Waste Tissue
1,1,1,2-Tetrachloroethane EPA 5030 X
1,1,1,2-Tetrachloroethane EPA 624.1 X
1,1,1,2-Tetrachloroethane EPA 8260B X X
1,1,1,2-Tetrachloroethane EPA 8260C X X
1,1,1,2-Tetrachloroethane EPA 8260D X X
1,1,1,2-Tetrachloroethane SM 6200 B-2011 X
1,1,1,2-Tetrachloroethane EPA 524.2 X
1,1,1-Trichloroethane EPA 624.1 X
1,1,1-Trichloroethane EPA 8260B X X
1,1,1-Trichloroethane EPA 8260C X X
1,1,1-Trichloroethane EPA 8260D X X
1,1,1-Trichloroethane EPA TO-15 X
1,1,1-Trichloroethane
EPA TO-15 GC/MS
SIM X
1,1,1-Trichloroethane SM 6200 B-2011 X
1,1,1-Trichloroethane EPA 524.2 X
1,1,2,2-Tetrachloroethane EPA 624.1 X
1,1,2,2-Tetrachloroethane EPA 8260B X X
1,1,2,2-Tetrachloroethane EPA 8260C X X
1,1,2,2-Tetrachloroethane EPA 8260D X X
1,1,2,2-Tetrachloroethane EPA TO-15 X
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1,1,2,2-Tetrachloroethane
EPA TO-15 GC/MS
SIM X
1,1,2,2-Tetrachloroethane SM 6200 B-2011 X
1,1,2,2-Tetrachloroethane EPA 524.2 X
1,1,2-Trichloro-1,2,2-
trifluoroethane (Freon 113)EPA 624.1 X
1,1,2-Trichloro-1,2,2-
trifluoroethane (Freon 113)EPA 8260B X X
1,1,2-Trichloro-1,2,2-
trifluoroethane (Freon 113)EPA 8260C X X
1,1,2-Trichloro-1,2,2-
trifluoroethane (Freon 113)EPA 8260D X X
1,1,2-Trichloro-1,2,2-
trifluoroethane (Freon 113)EPA TO-15 X
1,1,2-Trichloro-1,2,2-
trifluoroethane (Freon 113)SM 6200 B-2011 X
1,1,2-Trichloroethane EPA 624.1 X
1,1,2-Trichloroethane EPA 8260B X X
1,1,2-Trichloroethane EPA 8260C X X
1,1,2-Trichloroethane EPA 8260D X X
1,1,2-Trichloroethane EPA TO-15 X
1,1,2-Trichloroethane
EPA TO-15 GC/MS
SIM X
1,1,2-Trichloroethane SM 6200 B-2011 X
1,1,2-Trichloroethane EPA 524.2 X
1,1'-Biphenyl (BZ-0) (Biphenyl)EPA 8270C X X
1,1'-Biphenyl (BZ-0) (Biphenyl)EPA 8270D X
1,1-Dichloroethane EPA 624.1 X
1,1-Dichloroethane EPA 8260B X X
1,1-Dichloroethane EPA 8260C X X
1,1-Dichloroethane EPA 8260D X X
1,1-Dichloroethane EPA TO-15 X
1,1-Dichloroethane
EPA TO-15 GC/MS
SIM X
1,1-Dichloroethane SM 6200 B-2011 X
1,1-Dichloroethane EPA 524.2 X
1,1-Dichloroethene EPA 524.2 X
1,1-Dichloroethylene EPA 624.1 X
1,1-Dichloroethylene EPA 8260B X X
1,1-Dichloroethylene EPA 8260C X X
1,1-Dichloroethylene EPA 8260D X X
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1,1-Dichloroethylene EPA TO-15 X
1,1-Dichloroethylene
EPA TO-15 GC/MS
SIM X
1,1-Dichloroethylene SM 6200 B-2011 X
1,1-Dichloropropene EPA 524.2 X
1,1-Dichloropropene EPA 624 (extended) X
1,1-Dichloropropene EPA 624.1 X
1,1-Dichloropropene EPA 8260B X X
1,1-Dichloropropene EPA 8260C X X
1,1-Dichloropropene EPA 8260D X X
1,1-Dichloropropene SM 6200 B-2011 X
1,1-dimethylethyl ester (tert-
Butyl Formate)EPA 8260B X X
1,1-dimethylethyl ester (tert-
Butyl Formate)EPA 8260C X
1,1-dimethylethyl ester (tert-
Butyl Formate)EPA 8260D X
1,2,3,4-Tetrachlorobenzene EPA 8270C X X
1,2,3,4-Tetrachlorobenzene EPA 8270D X X
1,2,3,4-Tetrachlorobenzene EPA 8270E X X
1,2,3,5-Tetrachlorobenzene EPA 625.1 X
1,2,3,5-Tetrachlorobenzene EPA 8270C X X
1,2,3,5-Tetrachlorobenzene EPA 8270D X X
1,2,3,5-Tetrachlorobenzene EPA 8270E X X
1,2,3-Trichlorobenzene EPA 524.2 X
1,2,3-Trichlorobenzene EPA 624 (extended) X
1,2,3-Trichlorobenzene EPA 624.1 X
1,2,3-Trichlorobenzene EPA 8260B X X
1,2,3-Trichlorobenzene EPA 8260C X X
1,2,3-Trichlorobenzene EPA 8260D X X
1,2,3-Trichlorobenzene SM 6200 B-2011 X
1,2,3-Trichloropropane EPA 504.1 X
1,2,3-Trichloropropane EPA 624.1 X
1,2,3-Trichloropropane EPA 8260B X X
1,2,3-Trichloropropane EPA 8260C X X
1,2,3-Trichloropropane EPA 8260D X X
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1,2,3-Trichloropropane SM 6200 B-2011 X
1,2,3-Trichloropropane EPA 524.2 X
1,2,3-Trimethylbenzene EPA 624.1 X
1,2,3-Trimethylbenzene EPA 8260B X X
1,2,3-Trimethylbenzene EPA 8260C X X
1,2,3-Trimethylbenzene EPA 8260D X X
1,2,3-Trimethylbenzene EPA TO-15 X
1,2,4,5-Tetrachlorobenzene EPA 625.1 X
1,2,4,5-Tetrachlorobenzene EPA 8270C X X
1,2,4,5-Tetrachlorobenzene EPA 8270D X X
1,2,4,5-Tetrachlorobenzene EPA 8270E X X
1,2,4-Trichlorobenzene EPA 624.1 X
1,2,4-Trichlorobenzene EPA 625.1 X
1,2,4-Trichlorobenzene EPA 8260B X X
1,2,4-Trichlorobenzene EPA 8260C X X
1,2,4-Trichlorobenzene EPA 8260D X X
1,2,4-Trichlorobenzene EPA 8270C X X
1,2,4-Trichlorobenzene EPA 8270D X X
1,2,4-Trichlorobenzene EPA 8270E X X
1,2,4-Trichlorobenzene EPA TO-15 X
1,2,4-Trichlorobenzene SM 6200 B-2011 X
1,2,4-Trichlorobenzene EPA 524.2 X
1,2,4-Trimethylbenzene EPA 624.1 X
1,2,4-Trimethylbenzene EPA 8260B X X
1,2,4-Trimethylbenzene EPA 8260C X X
1,2,4-Trimethylbenzene EPA 8260D X X
1,2,4-Trimethylbenzene EPA TO-15 X
1,2,4-Trimethylbenzene SM 6200 B-2011 X
1,2,4-Trimethylbenzene EPA 524.2 X
1,2-Dibromo-3-chloropropane EPA 504.1 X
1,2-Dibromo-3-chloropropane EPA 524.2 X
1,2-Dibromo-3-chloropropane
(DBCP)EPA 624.1 X
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1,2-Dibromo-3-chloropropane
(DBCP)EPA 8011 X X
1,2-Dibromo-3-chloropropane
(DBCP)EPA 8260B X X
1,2-Dibromo-3-chloropropane
(DBCP)EPA 8260C X X
1,2-Dibromo-3-chloropropane
(DBCP)EPA 8260D X X
1,2-Dibromo-3-chloropropane
(DBCP)SM 6200 B-2011 X
1,2-Dibromoethane EPA 504.1 X
1,2-Dibromoethane EPA 524.2 X
1,2-Dibromoethane (EDB,
Ethylene dibromide)EPA 624.1 X
1,2-Dibromoethane (EDB,
Ethylene dibromide)EPA 8011 X X
1,2-Dibromoethane (EDB,
Ethylene dibromide)EPA 8260B X X
1,2-Dibromoethane (EDB,
Ethylene dibromide)EPA 8260C X X
1,2-Dibromoethane (EDB,
Ethylene dibromide)EPA 8260D X X
1,2-Dibromoethane (EDB,
Ethylene dibromide)EPA TO-15 X
1,2-Dibromoethane (EDB,
Ethylene dibromide)
EPA TO-15 GC/MS
SIM X
1,2-Dibromoethane (EDB,
Ethylene dibromide)SM 6200 B-2011 X
1,2-Dichloro-1,1,2,2-
tetrafluoroethane (Freon-114)EPA TO-15 X
1,2-Dichlorobenzene EPA 624.1 X
1,2-Dichlorobenzene EPA 625.1 X
1,2-Dichlorobenzene EPA 8260B X X
1,2-Dichlorobenzene EPA 8260C X X
1,2-Dichlorobenzene EPA 8260D X X
1,2-Dichlorobenzene EPA 8270C X X
1,2-Dichlorobenzene EPA 8270D X X
1,2-Dichlorobenzene EPA 8270E X X
1,2-Dichlorobenzene EPA TO-15 X
1,2-Dichlorobenzene SM 6200 B-2011 X
1,2-Dichlorobenzene EPA 524.2 X
1,2-Dichloroethane EPA 524.2 X
1,2-Dichloroethane (Ethylene
dichloride)EPA 624.1 X
1,2-Dichloroethane (Ethylene
dichloride)EPA 8260B X X
1,2-Dichloroethane (Ethylene
dichloride)EPA 8260C X X
1,2-Dichloroethane (Ethylene
dichloride)EPA 8260D X X
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1,2-Dichloroethane (Ethylene
dichloride)EPA TO-15 X
1,2-Dichloroethane (Ethylene
dichloride)
EPA TO-15 GC/MS
SIM X
1,2-Dichloroethane (Ethylene
dichloride)SM 6200 B-2011 X
1,2-Dichloropropane EPA 624.1 X
1,2-Dichloropropane EPA 8260B X X
1,2-Dichloropropane EPA 8260C X X
1,2-Dichloropropane EPA 8260D X X
1,2-Dichloropropane EPA TO-15 X
1,2-Dichloropropane
EPA TO-15 GC/MS
SIM X
1,2-Dichloropropane SM 6200 B-2011 X
1,2-Dichloropropane EPA 524.2 X
1,2-Diphenylhydrazine EPA 625.1 X
1,2-Diphenylhydrazine EPA 8270C X X
1,2-Diphenylhydrazine EPA 8270D X X
1,2-Diphenylhydrazine EPA 8270E X X
1,3,5-Trimethylbenzene EPA 524.2 X
1,3,5-Trimethylbenzene EPA 624.1 X
1,3,5-Trimethylbenzene EPA 8260B X X
1,3,5-Trimethylbenzene EPA 8260C X X
1,3,5-Trimethylbenzene EPA 8260D X X
1,3,5-Trimethylbenzene EPA TO-15 X
1,3,5-Trimethylbenzene SM 6200 B-2011 X
1,3,5-Trinitrobenzene (1,3,5-
TNB)EPA 625.1 X
1,3,5-Trinitrobenzene (1,3,5-
TNB)EPA 8270C X X
1,3,5-Trinitrobenzene (1,3,5-
TNB)EPA 8270D X X
1,3,5-Trinitrobenzene (1,3,5-
TNB)EPA 8270E X X
1,3,5-Trinitrobenzene (1,3,5-
TNB)EPA 8330 X X
1,3,5-Trinitrobenzene (1,3,5-
TNB)EPA 8330A X X
1,3,5-Trinitrobenzene (1,3,5-
TNB)EPA 8330B X X
1,3-Butadiene EPA 624.1 X
1,3-Butadiene EPA 8260B X
1,3-Butadiene EPA 8260C X
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1,3-Butadiene EPA 8260D X
1,3-Butadiene EPA TO-15 X
1,3-Dichlorobenzene EPA 624.1 X
1,3-Dichlorobenzene EPA 625.1 X
1,3-Dichlorobenzene EPA 8260B X X
1,3-Dichlorobenzene EPA 8260C X X
1,3-Dichlorobenzene EPA 8260D X X
1,3-Dichlorobenzene EPA 8270C X X
1,3-Dichlorobenzene EPA 8270D X X
1,3-Dichlorobenzene EPA 8270E X X
1,3-Dichlorobenzene EPA TO-15 X
1,3-Dichlorobenzene SM 6200 B-2011 X
1,3-Dichlorobenzene EPA 524.2 X
1,3-Dichloropropane EPA 624 (extended) X
1,3-Dichloropropane EPA 624.1 X
1,3-Dichloropropane EPA 8260B X X
1,3-Dichloropropane EPA 8260C X X
1,3-Dichloropropane EPA 8260D X X
1,3-Dichloropropane SM 6200 B-2011 X
1,3-Dichloropropane EPA 524.2 X
1,3-Dichloropropene EPA 624 (extended) X
1,3-Dinitrobenzene (1,3-DNB)EPA 625.1 X
1,3-Dinitrobenzene (1,3-DNB)EPA 8270C X X
1,3-Dinitrobenzene (1,3-DNB)EPA 8270D X X
1,3-Dinitrobenzene (1,3-DNB)EPA 8270E X X
1,3-Dinitrobenzene (1,3-DNB)EPA 8330 X X
1,3-Dinitrobenzene (1,3-DNB)EPA 8330A X X
1,3-Dinitrobenzene (1,3-DNB)EPA 8330B X X
1,3-Hexachlorobutadiene EPA 8260B X
1,3-Hexachlorobutadiene EPA 8260C X
1,3-Hexachlorobutadiene EPA 8260D X
1,3-Hexachlorobutadiene EPA 8270D X
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1,3-Hexachlorobutadiene EPA 8270E X
1,3-Hexachlorobutadiene EPA TO-15 X
1,4-Dichlorobenzene EPA 624.1 X
1,4-Dichlorobenzene EPA 625.1 X
1,4-Dichlorobenzene EPA 8260B X X
1,4-Dichlorobenzene EPA 8260C X X
1,4-Dichlorobenzene EPA 8260D X X
1,4-Dichlorobenzene EPA 8270C X X
1,4-Dichlorobenzene EPA 8270D X X
1,4-Dichlorobenzene EPA 8270E X X
1,4-Dichlorobenzene EPA TO-15 X
1,4-Dichlorobenzene
EPA TO-15 GC/MS
SIM X
1,4-Dichlorobenzene SM 6200 B-2011 X
1,4-Dichlorobenzene EPA 524.2 X
1,4-Dinitrobenzene EPA 625.1 X
1,4-Dinitrobenzene EPA 8270C X X
1,4-Dinitrobenzene EPA 8270D X X
1,4-Dinitrobenzene EPA 8270E X X
1,4-Dioxane (1,4-
Diethyleneoxide)EPA 624.1 X
1,4-Dioxane (1,4-
Diethyleneoxide)EPA 625.1 SIM X
1,4-Dioxane (1,4-
Diethyleneoxide)EPA 8260B X X
1,4-Dioxane (1,4-
Diethyleneoxide)EPA 8260B SIM X X
1,4-Dioxane (1,4-
Diethyleneoxide)EPA 8260C X X
1,4-Dioxane (1,4-
Diethyleneoxide)EPA 8260C SIM X X
1,4-Dioxane (1,4-
Diethyleneoxide)EPA 8260D X X
1,4-Dioxane (1,4-
Diethyleneoxide)EPA 8260D SIM X X
1,4-Dioxane (1,4-
Diethyleneoxide)EPA 8270C X
1,4-Dioxane (1,4-
Diethyleneoxide)EPA 8270C SIM X
1,4-Dioxane (1,4-
Diethyleneoxide)EPA 8270D X
1,4-Dioxane (1,4-
Diethyleneoxide)EPA 8270D SIM X
1,4-Dioxane (1,4-
Diethyleneoxide)EPA 8270E X
1,4-Dioxane (1,4-
Diethyleneoxide)EPA TO-15 X
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1,4-Dioxane (1,4-
Diethyleneoxide)SM 6200 B-2011 X
1,4-Naphthoquinone EPA 625.1 X
1,4-Naphthoquinone EPA 8270C X X
1,4-Naphthoquinone EPA 8270D X X
1,4-Naphthoquinone EPA 8270E X X
1,4-Phenylenediamine EPA 625.1 X
1,4-Phenylenediamine EPA 8270C X X
1,4-Phenylenediamine EPA 8270D X X
1,4-Phenylenediamine EPA 8270E X X
1-Chloronaphthalene EPA 625.1 X
1-Chloronaphthalene EPA 8270C X X
1-Chloronaphthalene EPA 8270D X X
1-Chloronaphthalene EPA 8270E X X
1-Methylnaphthalene EPA 610 (HPLC) X
1-Methylnaphthalene EPA 625.1 SIM X
1-Methylnaphthalene EPA 8260B X X
1-Methylnaphthalene EPA 8260C X X
1-Methylnaphthalene EPA 8260D X
1-Methylnaphthalene EPA 8270C X X
1-Methylnaphthalene EPA 8270C SIM X X
1-Methylnaphthalene EPA 8270D X X
1-Methylnaphthalene EPA 8270D SIM X X
1-Methylnaphthalene EPA 8270E X X
1-Methylnaphthalene EPA 8270E SIM X X
1-Methylnaphthalene EPA 8310 X X
1-Methylnaphthalene SM 6200 B-2011 X
1-Naphthylamine EPA 625.1 X
1-Naphthylamine EPA 8270C X X
1-Naphthylamine EPA 8270D X X
1-Naphthylamine EPA 8270E X X
2,2,4-Trimethylpentane
(Isooctane)EPA 624.1 X
2,2,4-Trimethylpentane
(Isooctane)EPA 8260B X X
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2,2,4-Trimethylpentane
(Isooctane)EPA 8260C X X
2,2,4-Trimethylpentane
(Isooctane)EPA 8260D X X
2,2,4-Trimethylpentane
(Isooctane)EPA TO-15 X
2,2,4-Trimethylpentane
(Isooctane)SM 6200 B-2011 X
2,2-Dichloropropane EPA 524.2 X
2,2-Dichloropropane EPA 624 (extended) X
2,2-Dichloropropane EPA 624.1 X
2,2-Dichloropropane EPA 8260B X X
2,2-Dichloropropane EPA 8260C X X
2,2-Dichloropropane EPA 8260D X X
2,2-Dichloropropane SM 6200 B-2011 X
2,2'-Oxybis(1-chloropropane),
bis(2-Chloro-1-EPA 625.1 X
2,2'-Oxybis(1-chloropropane),
bis(2-Chloro-1-EPA 8270C X X
2,2'-Oxybis(1-chloropropane),
bis(2-Chloro-1-EPA 8270D X X
2,2'-Oxybis(1-chloropropane),
bis(2-Chloro-1-EPA 8270E X X
2,3,4,6-Tetrachlorophenol EPA 625.1 X
2,3,4,6-Tetrachlorophenol EPA 8270C X X
2,3,4,6-Tetrachlorophenol EPA 8270D X X
2,3,4,6-Tetrachlorophenol EPA 8270E X X
2,3-Dichloroaniline EPA 625.1 X
2,4,5-T EPA 8151A X X
2,4,5-T SM 6640 B-2001 X
2,4,5-T SM 6640 B-2006 X
2,4,5-Trichlorophenol EPA 625.1 X
2,4,5-Trichlorophenol EPA 8270C X X
2,4,5-Trichlorophenol EPA 8270D X X
2,4,5-Trichlorophenol EPA 8270E X X
2,4,6-Trichlorophenol EPA 625.1 X
2,4,6-Trichlorophenol EPA 8270C X X
2,4,6-Trichlorophenol EPA 8270D X X
2,4,6-Trichlorophenol EPA 8270E X X
2,4,6-Trinitrotoluene (2,4,6-
TNT)EPA 8330 X X
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2,4,6-Trinitrotoluene (2,4,6-
TNT)EPA 8330A X X
2,4,6-Trinitrotoluene (2,4,6-
TNT)EPA 8330B X X
2,4-D EPA 8151A X X
2,4-D SM 6640 B-2001 X
2,4-D SM 6640 B-2006 X
2,4-DB EPA 8151A X X
2,4-Dichlorophenol EPA 625.1 X
2,4-Dichlorophenol EPA 8270C X X
2,4-Dichlorophenol EPA 8270D X X
2,4-Dichlorophenol EPA 8270E X X
2,4-Dimethylphenol EPA 625.1 X
2,4-Dimethylphenol EPA 8270C X X
2,4-Dimethylphenol EPA 8270D X X
2,4-Dimethylphenol EPA 8270E X X
2,4-Dinitrophenol EPA 625.1 X
2,4-Dinitrophenol EPA 8270C X X
2,4-Dinitrophenol EPA 8270D X X
2,4-Dinitrophenol EPA 8270E X X
2,4-Dinitrotoluene (2,4-DNT)EPA 625.1 X
2,4-Dinitrotoluene (2,4-DNT)EPA 8270C X X
2,4-Dinitrotoluene (2,4-DNT)EPA 8270D X X
2,4-Dinitrotoluene (2,4-DNT)EPA 8270E X X
2,4-Dinitrotoluene (2,4-DNT)EPA 8330 X X
2,4-Dinitrotoluene (2,4-DNT)EPA 8330A X X
2,4-Dinitrotoluene (2,4-DNT)EPA 8330B X X
2,6-Dichlorophenol EPA 625.1 X
2,6-Dichlorophenol EPA 8270C X X
2,6-Dichlorophenol EPA 8270D X X
2,6-Dichlorophenol EPA 8270E X X
2,6-Dinitrotoluene (2,6-DNT)EPA 625.1 X
2,6-Dinitrotoluene (2,6-DNT)EPA 8270C X X
2,6-Dinitrotoluene (2,6-DNT)EPA 8270D X X
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2,6-Dinitrotoluene (2,6-DNT)EPA 8270E X X
2,6-Dinitrotoluene (2,6-DNT)EPA 8330 X X
2,6-Dinitrotoluene (2,6-DNT)EPA 8330A X X
2,6-Dinitrotoluene (2,6-DNT)EPA 8330B X X
2,6-Toluenediisocyanate EPA 8270C X
2,6-Toluenediisocyanate EPA 8270D X
2,6-Toluenediisocyanate EPA 8270E X
2-Acetylaminofluorene EPA 625.1 X
2-Acetylaminofluorene EPA 8270C X X
2-Acetylaminofluorene EPA 8270D X X
2-Acetylaminofluorene EPA 8270E X X
2-Amino-4,6-dinitrotoluene (2-
am-dnt)EPA 8330 X X
2-Amino-4,6-dinitrotoluene (2-
am-dnt)EPA 8330A X X
2-Amino-4,6-dinitrotoluene (2-
am-dnt)EPA 8330B X X
2-Butanone (Methyl ethyl
ketone, MEK)EPA 624.1 X
2-Butanone (Methyl ethyl
ketone, MEK)EPA 8260B X X
2-Butanone (Methyl ethyl
ketone, MEK)EPA 8260C X X
2-Butanone (Methyl ethyl
ketone, MEK)EPA 8260D X X
2-Butanone (Methyl ethyl
ketone, MEK)EPA TO-15 X
2-Butanone (Methyl ethyl
ketone, MEK)SM 6200 B-2011 X
2-Chloroethyl vinyl ether EPA 624.1 X
2-Chloroethyl vinyl ether EPA 8260B X X
2-Chloroethyl vinyl ether EPA 8260C X X
2-Chloroethyl vinyl ether EPA 8260D X X
2-Chloroethyl vinyl ether SM 6200 B-2011 X
2-Chloronaphthalene EPA 625.1 X
2-Chloronaphthalene EPA 8270C X X
2-Chloronaphthalene EPA 8270C SIM X
2-Chloronaphthalene EPA 8270D X X
2-Chloronaphthalene EPA 8270D SIM X
2-Chloronaphthalene EPA 8270E X X
2-Chloronaphthalene EPA 8270E SIM X
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2-Chlorophenol EPA 625.1 X
2-Chlorophenol EPA 8270C X X
2-Chlorophenol EPA 8270D X X
2-Chlorophenol EPA 8270E X X
2-Chlorotoluene EPA 524.2 X
2-Chlorotoluene EPA 624 (extended) X
2-Chlorotoluene EPA 624.1 X
2-Chlorotoluene EPA 8260B X X
2-Chlorotoluene EPA 8260C X X
2-Chlorotoluene EPA 8260D X X
2-Chlorotoluene EPA TO-15 X
2-Chlorotoluene SM 6200 B-2011 X
2-Hexanone EPA 524.2 X
2-Hexanone EPA 624.1 X
2-Hexanone EPA 8260B X X
2-Hexanone EPA 8260C X X
2-Hexanone EPA 8260D X X
2-Hexanone EPA TO-15 X
2-Hexanone SM 6200 B-2011 X
2-methyl-2-butanol (tert-Amyl
alcohol)EPA 624.1 X
2-methyl-2-butanol (tert-Amyl
alcohol)EPA 8260B X X
2-methyl-2-butanol (tert-Amyl
alcohol)EPA 8260C X X
2-methyl-2-butanol (tert-Amyl
alcohol)EPA 8260D X X
2-methyl-2-butanol (tert-Amyl
alcohol)SM 6200 B-2011 X
2-Methyl-2-pentanol EPA 8260B X X
2-Methyl-2-pentanol EPA 8260C X X
2-Methyl-2-pentanol EPA 8260D X
2-methyl-2-pentanol (ethyl tert-
butyl alcohol)EPA 8260B X X
2-methyl-2-pentanol (ethyl tert-
butyl alcohol)EPA 8260D X
2-methyl-2-pentanol (ethyl tert-
butyl alcohol)SM 6200 B-2011 X
2-Methyl-4,6-dinitrophenol
(4,6-Dinitro-2-methylphenol)EPA 625.1 X
2-Methyl-4,6-dinitrophenol
(4,6-Dinitro-2-methylphenol)EPA 8270C X X
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2-Methyl-4,6-dinitrophenol
(4,6-Dinitro-2-methylphenol)EPA 8270D X X
2-Methyl-4,6-dinitrophenol
(4,6-Dinitro-2-methylphenol)EPA 8270E X X
2-Methylaniline (o-Toluidine)EPA 625.1 X
2-Methylaniline (o-Toluidine)EPA 8270C X X
2-Methylaniline (o-Toluidine)EPA 8270D X X
2-Methylaniline (o-Toluidine)EPA 8270E X X
2-Methylnaphthalene EPA 610 (HPLC) X
2-Methylnaphthalene EPA 625.1 X
2-Methylnaphthalene EPA 625.1 SIM X
2-Methylnaphthalene EPA 8260B X X
2-Methylnaphthalene EPA 8260C X X
2-Methylnaphthalene EPA 8260D X X
2-Methylnaphthalene EPA 8270C X X
2-Methylnaphthalene EPA 8270C SIM X X
2-Methylnaphthalene EPA 8270D X X
2-Methylnaphthalene EPA 8270D SIM X X
2-Methylnaphthalene EPA 8270E X X
2-Methylnaphthalene EPA 8270E SIM X X
2-Methylnaphthalene EPA 8310 X X
2-Methylnaphthalene EPA TO-15 X
2-Methylnaphthalene MADEP EPH X X
2-Methylnaphthalene SM 6200 B-2011 X
2-Methylphenol (o-Cresol)EPA 625.1 X
2-Methylphenol (o-Cresol)EPA 8270C X X
2-Methylphenol (o-Cresol)EPA 8270D X X
2-Methylphenol (o-Cresol)EPA 8270E X X
2-Naphthylamine EPA 625.1 X
2-Naphthylamine EPA 8270C X X
2-Naphthylamine EPA 8270D X X
2-Naphthylamine EPA 8270E X X
2-Nitroaniline EPA 625.1 X
2-Nitroaniline EPA 8270C X X
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2-Nitroaniline EPA 8270D X X
2-Nitroaniline EPA 8270E X X
2-Nitrodiphenylamine EPA 8270C X X
2-Nitrodiphenylamine EPA 8270D X X
2-Nitrodiphenylamine EPA 8270E X X
2-Nitroguanidine
(Nitroguanidine)
EPA 8330A
(extended) X X
2-Nitroguanidine
(Nitroguanidine)
EPA 8330B
(extended) X X
2-Nitrophenol EPA 625.1 X
2-Nitrophenol EPA 8270C X X
2-Nitrophenol EPA 8270D X X
2-Nitrophenol EPA 8270E X X
2-Nitropropane EPA 624.1 X
2-Nitropropane EPA 8260B X X
2-Nitropropane EPA 8260C X X
2-Nitropropane EPA 8260D X X
2-Nitropropane SM 6200 B-2011 X
2-Nitrotoluene EPA 8330 X X
2-Nitrotoluene EPA 8330A X X
2-Nitrotoluene EPA 8330B X X
2-Picoline (2-Methylpyridine)EPA 625.1 X
2-Picoline (2-Methylpyridine)EPA 8270C X X
2-Picoline (2-Methylpyridine)EPA 8270D X X
2-Picoline (2-Methylpyridine)EPA 8270E X X
2-Sec-butyl-4,6-dinitrophenol
(DNBP, Dinoseb)EPA 8151A X
3,3'-Dichlorobenzidine EPA 625.1 X
3,3'-Dichlorobenzidine EPA 8270C X X
3,3'-Dichlorobenzidine EPA 8270D X X
3,3'-Dichlorobenzidine EPA 8270E X X
3,3-dimethyl-1-butanol EPA 624.1 X
3,3-dimethyl-1-butanol EPA 8260B X X
3,3-dimethyl-1-butanol EPA 8260C X X
3,3-dimethyl-1-butanol EPA 8260D X X
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3,3-dimethyl-1-butanol SM 6200 B-2011 X
3,3'-Dimethylbenzidine EPA 625.1 X
3,3'-Dimethylbenzidine EPA 8270C X X
3,3'-Dimethylbenzidine EPA 8270D X X
3,3'-Dimethylbenzidine EPA 8270E X X
3+4 Methylphenol EPA 625.1 X
3+4 Methylphenol EPA 8270C X X
3+4 Methylphenol EPA 8270D X X
3+4 Methylphenol EPA 8270E X
3-Methylcholanthrene EPA 625.1 X
3-Methylcholanthrene EPA 8270C X X
3-Methylcholanthrene EPA 8270D X X
3-Methylcholanthrene EPA 8270E X X
3-Methylphenol (m-Cresol)EPA 625.1 X
3-Nitroaniline EPA 625.1 X
3-Nitroaniline EPA 8270C X X
3-Nitroaniline EPA 8270D X X
3-Nitroaniline EPA 8270E X X
3-Nitrotoluene EPA 8330 X X
3-Nitrotoluene EPA 8330A X X
3-Nitrotoluene EPA 8330B X X
4,4'-DDD EPA 608.3 X
4,4'-DDD EPA 8081A X X
4,4'-DDD EPA 8081B X X
4,4'-DDE EPA 608.3 X
4,4'-DDE EPA 8081A X X
4,4'-DDE EPA 8081B X X
4,4'-DDT EPA 608.3 X
4,4'-DDT EPA 8081A X X
4,4'-DDT EPA 8081B X X
4,4'-Methylenebis(2-
chloroaniline)EPA 8270C X X
4,4'-Methylenebis(2-
chloroaniline)EPA 8270D X X
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4,4'-Methylenebis(2-
chloroaniline)EPA 8270E X
4-Amino-2,6-dinitrotoluene (4-
am-dnt)EPA 8330 X X
4-Amino-2,6-dinitrotoluene (4-
am-dnt)EPA 8330A X X
4-Amino-2,6-dinitrotoluene (4-
am-dnt)EPA 8330B X X
4-Aminobiphenyl EPA 625.1 X
4-Aminobiphenyl EPA 8270C X X
4-Aminobiphenyl EPA 8270D X X
4-Aminobiphenyl EPA 8270E X X
4-Bromophenyl phenyl ether EPA 625.1 X
4-Bromophenyl phenyl ether EPA 625.1 SIM X
4-Bromophenyl phenyl ether EPA 8270C X X
4-Bromophenyl phenyl ether EPA 8270D X X
4-Bromophenyl phenyl ether EPA 8270E X X
4-Chloro-3-methylphenol EPA 625.1 X
4-Chloro-3-methylphenol EPA 8270C X X
4-Chloro-3-methylphenol EPA 8270D X X
4-Chloro-3-methylphenol EPA 8270E X X
4-Chloroaniline EPA 625.1 X
4-Chloroaniline EPA 8270C X X
4-Chloroaniline EPA 8270D X X
4-Chloroaniline EPA 8270E X X
4-Chlorophenyl phenylether EPA 625.1 X
4-Chlorophenyl phenylether EPA 8270C X X
4-Chlorophenyl phenylether EPA 8270D X X
4-Chlorophenyl phenylether EPA 8270E X X
4-Chlorotoluene EPA 524.2 X
4-Chlorotoluene EPA 624 (extended) X
4-Chlorotoluene EPA 624.1 X
4-Chlorotoluene EPA 8260B X X
4-Chlorotoluene EPA 8260C X X
4-Chlorotoluene EPA 8260D X X
4-Chlorotoluene SM 6200 B-2011 X
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4-Dimethyl aminoazobenzene EPA 8270C X
4-Dimethyl aminoazobenzene EPA 8270D X
4-Dimethyl aminoazobenzene EPA 8270E X
4-Ethyltoluene EPA 8260B X
4-Ethyltoluene EPA TO-15 X
4-Isopropyltoluene EPA 524.2 X
4-Isopropyltoluene (p-Cymene)EPA 624 (extended) X
4-Isopropyltoluene (p-Cymene)EPA 624.1 X
4-Isopropyltoluene (p-Cymene)EPA 8260B X X
4-Isopropyltoluene (p-Cymene)EPA 8260C X X
4-Isopropyltoluene (p-Cymene)EPA 8260D X X
4-Isopropyltoluene (p-Cymene)SM 6200 B-2011 X
4-Methyl-2-pentanone (MIBK)EPA 624.1 X
4-Methyl-2-pentanone (MIBK)EPA 8260B X X
4-Methyl-2-pentanone (MIBK)EPA 8260C X X
4-Methyl-2-pentanone (MIBK)EPA 8260D X X
4-Methyl-2-pentanone (MIBK)EPA TO-15 X
4-Methyl-2-pentanone (MIBK)SM 6200 B-2011 X
4-Methylphenol (p-Cresol)EPA 625.1 X
4-Methylphenol (p-Cresol)EPA 8270C X X
4-Methylphenol (p-Cresol)EPA 8270D X X
4-Methylphenol (p-Cresol)EPA 8270E X X
4-Nitroaniline EPA 625.1 X
4-Nitroaniline EPA 8270C X X
4-Nitroaniline EPA 8270D X X
4-Nitroaniline EPA 8270E X X
4-Nitrophenol EPA 625.1 X
4-Nitrophenol EPA 8270C X X
4-Nitrophenol EPA 8270D X X
4-Nitrophenol EPA 8270E X X
4-Nitroquinoline 1-oxide EPA 625.1 X
4-Nitroquinoline 1-oxide EPA 8270C X X
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4-Nitroquinoline 1-oxide EPA 8270D X X
4-Nitroquinoline 1-oxide EPA 8270E X X
4-Nitrotoluene EPA 8330 X X
4-Nitrotoluene EPA 8330A X X
4-Nitrotoluene EPA 8330B X X
5-Nitro-o-toluidine EPA 625.1 X
5-Nitro-o-toluidine EPA 8270C X X
5-Nitro-o-toluidine EPA 8270D X X
5-Nitro-o-toluidine EPA 8270E X X
7,12-Dimethylbenz(a)
anthracene EPA 625.1 X
7,12-Dimethylbenz(a)
anthracene EPA 8270C X X
7,12-Dimethylbenz(a)
anthracene EPA 8270D X X
7,12-Dimethylbenz(a)
anthracene EPA 8270E X X
7h-Dibenzo(c,g) carbazole EPA 8270C X X
7h-Dibenzo(c,g) carbazole EPA 8270D X X
7h-Dibenzo(c,g) carbazole EPA 8270E X X
96-hour LC50 EPA 2000 X
a-a-Dimethylphenethylamine EPA 625.1 X
a-a-Dimethylphenethylamine EPA 8270C X X
a-a-Dimethylphenethylamine EPA 8270D X X
a-a-Dimethylphenethylamine EPA 8270E X X
Acenaphthene EPA 610 (HPLC) X
Acenaphthene EPA 625.1 X
Acenaphthene EPA 625.1 SIM X
Acenaphthene EPA 8270C X X
Acenaphthene EPA 8270C SIM X X
Acenaphthene EPA 8270D X X
Acenaphthene EPA 8270D SIM X X
Acenaphthene EPA 8270E X X
Acenaphthene EPA 8270E SIM X X
Acenaphthene EPA 8310 X X
Acenaphthene MADEP EPH X X
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Acenaphthylene EPA 610 (HPLC) X
Acenaphthylene EPA 625.1 X
Acenaphthylene EPA 625.1 SIM X
Acenaphthylene EPA 8270C X X
Acenaphthylene EPA 8270C SIM X X
Acenaphthylene EPA 8270D X X
Acenaphthylene EPA 8270D SIM X X
Acenaphthylene EPA 8270E X X
Acenaphthylene EPA 8270E SIM X X
Acenaphthylene EPA 8310 X X
Acenaphthylene MADEP EPH X X
Acetaldehyde EPA TO-15 X
Acetone EPA 624.1 X
Acetone EPA 8260B X X
Acetone EPA 8260C X X
Acetone EPA 8260D X X
Acetone EPA TO-15 X
Acetone SM 6200 B-2011 X
Acetone EPA 524.2 X
Acetonitrile EPA 624.1 X
Acetonitrile EPA 8260B X X
Acetonitrile EPA 8260C X X
Acetonitrile EPA 8260D X X
Acetonitrile EPA TO-15 X
Acetonitrile SM 6200 B-2011 X
Acetophenone EPA 625.1 X
Acetophenone EPA 8270C X X
Acetophenone EPA 8270D X X
Acetophenone EPA 8270E X X
Acetylene
EPA RSK-175
(GC/FID)X X
Acid Digestion of Aqueous
samples and Extracts for Total EPA 3010A X
Acid Digestion of Oils for
Metals Analysis or ICP EPA 3031 X
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Acid Digestion of Sediments,
Sludges, and soils EPA 3050B X
Acid Digestion of waters for
Total Recoverable or Dissolved EPA 3005A X
Acidity, as CaCO3 SM 2310 B-2011 X
Acrolein (Propenal)EPA 624.1 X
Acrolein (Propenal)EPA 8260B X X
Acrolein (Propenal)EPA 8260C X X
Acrolein (Propenal)EPA 8260D X X
Acrolein (Propenal)EPA TO-15 X
Acrolein (Propenal)SM 6200 B-2011 X
Acrylonitrile EPA 624.1 X
Acrylonitrile EPA 8260B X X
Acrylonitrile EPA 8260C X X
Acrylonitrile EPA 8260D X X
Acrylonitrile EPA TO-15 X
Acrylonitrile SM 6200 B-2011 X
Acute toxicity
EPA 2002
Ceriodaphnia dubia X
Alachlor EPA 507 X X
Aldrin EPA 608.3 X
Aldrin EPA 8081A X X
Aldrin EPA 8081B X X
Alkalinity as CaCO3 EPA 310.2 X
Alkalinity as CaCO3 SM 2320 B-2011 X X
Allyl chloride (3-
Chloropropene)EPA 624.1 X
Allyl chloride (3-
Chloropropene)EPA 8260B X X
Allyl chloride (3-
Chloropropene)EPA 8260C X X
Allyl chloride (3-
Chloropropene)EPA 8260D X X
Allyl chloride (3-
Chloropropene)EPA TO-15 X
Allyl chloride (3-
Chloropropene)SM 6200 B-2011 X
Alpha Emitting Radium
Isotopes EPA 9315 X X
alpha-BHC (alpha-
Hexachlorocyclohexane)EPA 608.3 X
alpha-BHC (alpha-
Hexachlorocyclohexane)EPA 8081A X X
alpha-BHC (alpha-
Hexachlorocyclohexane)EPA 8081B X X
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alpha-Chlordane EPA 608.3 X
alpha-Chlordane EPA 8081A X X
alpha-Chlordane EPA 8081B X X
alpha-Terpineol EPA 625.1 X
alpha-Terpineol EPA 8270C X X
alpha-Terpineol EPA 8270D X X
alpha-Terpineol EPA 8270E X
Alumina Clean-Up EPA 3610B X
Alumina Clean-Up EPA 3611B X
Aluminum EPA 200.7 X X
Aluminum EPA 200.8 X X
Aluminum EPA 6010B X X
Aluminum EPA 6010C X X
Aluminum EPA 6010D X X
Aluminum EPA 6020 X X
Aluminum EPA 6020A X X
Aluminum EPA 6020B X X
Amenable cyanide EPA 9010B X
Amenable cyanide EPA 9010C X X
Amenable cyanide EPA 9012B X X
Amenable cyanide EPA 9014 X X
Amenable cyanide
SM 4500-CN¯ B-
2011 X
Amenable cyanide
SM 4500-CN¯ G-
2011 X
Americium-241
EPA 907 Modified
(ENV-SOP-MTJL-X X X X
Ammonia
SM 4500-NH3 B-
2011 X
Ammonia as N EPA 350.1 X X X
Ammonia as N
SM 4500-NH3 B-
2011 X
Ammonia as N
SM 4500-NH3 G-
2011 X
Aniline EPA 625.1 X
Aniline EPA 8270C X X
Aniline EPA 8270D X X
Aniline EPA 8270E X X
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Anthracene EPA 610 (HPLC) X
Anthracene EPA 625.1 X
Anthracene EPA 625.1 SIM X
Anthracene EPA 8270C X X
Anthracene EPA 8270C SIM X X
Anthracene EPA 8270D X X
Anthracene EPA 8270D SIM X X
Anthracene EPA 8270E X X
Anthracene EPA 8270E SIM X X
Anthracene EPA 8310 X X
Anthracene MADEP EPH X X
Antimony EPA 200.7 X X
Antimony EPA 200.8 X X
Antimony EPA 6010B X X
Antimony EPA 6010C X X
Antimony EPA 6010D X X
Antimony EPA 6020 X X
Antimony EPA 6020A X X
Antimony EPA 6020B X X
Aramite EPA 625.1 X
Aramite EPA 8270C X X
Aramite EPA 8270D X X
Aramite EPA 8270E X X
Aroclor-1016 (PCB-1016)EPA 600/4-81-045 X
Aroclor-1016 (PCB-1016)EPA 608.3 X
Aroclor-1016 (PCB-1016)EPA 8082 X X
Aroclor-1016 (PCB-1016)EPA 8082A X X
Aroclor-1016 (PCB-1016) in
Oil EPA 8082A X
Aroclor-1221 (PCB-1221)EPA 600/4-81-045 X
Aroclor-1221 (PCB-1221)EPA 608.3 X
Aroclor-1221 (PCB-1221)EPA 8082 X X
Aroclor-1221 (PCB-1221)EPA 8082A X X
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Aroclor-1221 (PCB-1221) in
Oil EPA 8082A X
Aroclor-1232 (PCB-1232)EPA 600/4-81-045 X
Aroclor-1232 (PCB-1232)EPA 608.3 X
Aroclor-1232 (PCB-1232)EPA 8082 X X
Aroclor-1232 (PCB-1232)EPA 8082A X X
Aroclor-1232 (PCB-1232) in
Oil EPA 8082A X
Aroclor-1242 (PCB-1242)EPA 600/4-81-045 X
Aroclor-1242 (PCB-1242)EPA 608.3 X
Aroclor-1242 (PCB-1242)EPA 8082 X X
Aroclor-1242 (PCB-1242)EPA 8082A X X
Aroclor-1242 (PCB-1242) in
Oil EPA 8082A X
Aroclor-1248 (PCB-1248)EPA 600/4-81-045 X
Aroclor-1248 (PCB-1248)EPA 608.3 X
Aroclor-1248 (PCB-1248)EPA 8082 X X
Aroclor-1248 (PCB-1248)EPA 8082A X X
Aroclor-1248 (PCB-1248) in
Oil EPA 8082A X
Aroclor-1254 (PCB-1254)EPA 600/4-81-045 X
Aroclor-1254 (PCB-1254)EPA 608.3 X
Aroclor-1254 (PCB-1254)EPA 8082 X X
Aroclor-1254 (PCB-1254)EPA 8082A X X
Aroclor-1254 (PCB-1254) in
Oil EPA 8082A X
Aroclor-1260 (PCB-1260)EPA 600/4-81-045 X
Aroclor-1260 (PCB-1260)EPA 608.3 X
Aroclor-1260 (PCB-1260)EPA 8082 X X
Aroclor-1260 (PCB-1260)EPA 8082A X X
Aroclor-1260 (PCB-1260) in
Oil EPA 8082A X
Aroclor-1262 (PCB-1262)EPA 600/4-81-045 X
Aroclor-1262 (PCB-1262)EPA 8082 X X
Aroclor-1262 (PCB-1262)EPA 8082A X X
Aroclor-1262 (PCB-1262) in
Oil EPA 8082A X
Aroclor-1268 (PCB-1268)EPA 600/4-81-045 X
Aroclor-1268 (PCB-1268)EPA 8082 X X
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Aroclor-1268 (PCB-1268)EPA 8082A X X
Aroclor-1268 (PCB-1268) in
Oil EPA 8082A X
Arsenic EPA 200.7 X X
Arsenic EPA 200.8 X X
Arsenic EPA 6010B X X
Arsenic EPA 6010C X X
Arsenic EPA 6010D X X
Arsenic EPA 6020 X X
Arsenic EPA 6020A X X
Arsenic EPA 6020B X X
Atrazine EPA 507 X X
Atrazine EPA 625.1 X
Atrazine EPA 8141A X
Atrazine EPA 8141B X
Atrazine EPA 8270C X X
Atrazine EPA 8270D X X
Atrazine EPA 8270E X X
Azinphos-methyl (Guthion)EPA 1657 X
Azinphos-methyl (Guthion)EPA 8141A X X
Azinphos-methyl (Guthion)EPA 8141B X X
Barium EPA 200.7 X X
Barium EPA 200.8 X X
Barium EPA 6010B X X
Barium EPA 6010C X X
Barium EPA 6010D X X
Barium EPA 6020 X X
Barium EPA 6020A X X
Barium EPA 6020B X X
Barium-133 DOE 4.5.2.3 X
Barium-133 EPA 901.1 X
Barium-133 HASL 300 Ga-01-R X
Benzal chloride EPA 8270C X X
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Benzal chloride EPA 8270D X X
Benzal chloride EPA 8270E X X
Benzaldehyde EPA 625.1 X
Benzaldehyde EPA 8270C X X
Benzaldehyde EPA 8270D X X
Benzaldehyde EPA 8270E X X
Benzene EPA 602 X
Benzene EPA 624.1 X
Benzene EPA 8021B X X
Benzene EPA 8260B X X
Benzene EPA 8260C X X
Benzene EPA 8260D X X
Benzene EPA TO-15 X
Benzene
EPA TO-15 GC/MS
SIM X
Benzene IDNR OA-1 X X
Benzene LUFT GCMS X X
Benzene MADEP VPH X X
Benzene OK DEQ GRO X X
Benzene SM 6200 B-2011 X
Benzene EPA 524.2 X
Benzenethiol EPA 625.1 X
Benzenethiol EPA 8270C X X
Benzenethiol EPA 8270D X X
Benzenethiol EPA 8270E X
Benzidine EPA 625.1 X
Benzidine EPA 8270C X X
Benzidine EPA 8270D X X
Benzidine EPA 8270E X X
Benzo(a)anthracene EPA 610 (HPLC) X
Benzo(a)anthracene EPA 625.1 X
Benzo(a)anthracene EPA 625.1 SIM X
Benzo(a)anthracene EPA 8270C X X
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Benzo(a)anthracene EPA 8270C SIM X X
Benzo(a)anthracene EPA 8270D X X
Benzo(a)anthracene EPA 8270D SIM X X
Benzo(a)anthracene EPA 8270E X X
Benzo(a)anthracene EPA 8270E SIM X X
Benzo(a)anthracene EPA 8310 X X
Benzo(a)anthracene MADEP EPH X X
Benzo(a)pyrene EPA 610 (HPLC) X
Benzo(a)pyrene EPA 625.1 X
Benzo(a)pyrene EPA 625.1 SIM X
Benzo(a)pyrene EPA 8270C X X
Benzo(a)pyrene EPA 8270C SIM X X
Benzo(a)pyrene EPA 8270D X X
Benzo(a)pyrene EPA 8270D SIM X X
Benzo(a)pyrene EPA 8270E X X
Benzo(a)pyrene EPA 8270E SIM X X
Benzo(a)pyrene EPA 8310 X X
Benzo(a)pyrene MADEP EPH X X
Benzo(b)fluoranthene EPA 610 (HPLC) X
Benzo(b)fluoranthene EPA 625.1 X
Benzo(b)fluoranthene EPA 625.1 SIM X
Benzo(b)fluoranthene EPA 8270C X X
Benzo(b)fluoranthene EPA 8270C SIM X X
Benzo(b)fluoranthene EPA 8270D X X
Benzo(b)fluoranthene EPA 8270D SIM X X
Benzo(b)fluoranthene EPA 8270E X X
Benzo(b)fluoranthene EPA 8270E SIM X X
Benzo(b)fluoranthene EPA 8310 X X
Benzo(b)fluoranthene MADEP EPH X X
Benzo(e)pyrene EPA 8270D SIM X X
Benzo(e)pyrene EPA 8270E SIM X X
Benzo(g,h,i)perylene EPA 610 (HPLC) X
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Benzo(g,h,i)perylene EPA 625.1 X
Benzo(g,h,i)perylene EPA 625.1 SIM X
Benzo(g,h,i)perylene EPA 8270C X X
Benzo(g,h,i)perylene EPA 8270C SIM X X
Benzo(g,h,i)perylene EPA 8270D X X
Benzo(g,h,i)perylene EPA 8270D SIM X X
Benzo(g,h,i)perylene EPA 8270E X X
Benzo(g,h,i)perylene EPA 8270E SIM X X
Benzo(g,h,i)perylene EPA 8310 X X
Benzo(g,h,i)perylene MADEP EPH X X
Benzo(j)fluoranthene EPA 8270C X X
Benzo(j)fluoranthene EPA 8270D X X
Benzo(j)fluoranthene EPA 8270E X X
Benzo(k)fluoranthene EPA 610 (HPLC) X
Benzo(k)fluoranthene EPA 625.1 X
Benzo(k)fluoranthene EPA 625.1 SIM X
Benzo(k)fluoranthene EPA 8270C X X
Benzo(k)fluoranthene EPA 8270C SIM X X
Benzo(k)fluoranthene EPA 8270D X X
Benzo(k)fluoranthene EPA 8270D SIM X X
Benzo(k)fluoranthene EPA 8270E X X
Benzo(k)fluoranthene EPA 8270E SIM X X
Benzo(k)fluoranthene EPA 8310 X X
Benzo(k)fluoranthene MADEP EPH X X
Benzoic acid EPA 625.1 X
Benzoic acid EPA 8270C X X
Benzoic acid EPA 8270D X X
Benzoic acid EPA 8270E X X
Benzotrichloride EPA 8270C X X
Benzotrichloride EPA 8270D X X
Benzotrichloride EPA 8270E X X
Benzyl alcohol EPA 625.1 X
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Benzyl alcohol EPA 8270C X X
Benzyl alcohol EPA 8270D X X
Benzyl alcohol EPA 8270E X X
Benzyl chloride EPA 8270C X X
Benzyl chloride EPA 8270D X X
Benzyl chloride EPA 8270E X X
Benzyl chloride EPA TO-15 X
Beryllium EPA 200.7 X X
Beryllium EPA 200.8 X X
Beryllium EPA 6010B X X
Beryllium EPA 6010C X X
Beryllium EPA 6010D X X
Beryllium EPA 6020 X X
Beryllium EPA 6020A X X
Beryllium EPA 6020B X X
beta-BHC (beta-
Hexachlorocyclohexane)EPA 608.3 X
beta-BHC (beta-
Hexachlorocyclohexane)EPA 8081A X X
beta-BHC (beta-
Hexachlorocyclohexane)EPA 8081B X X
Biochemical oxygen demand SM 5210 B-2011 X
Biphenyl (1,1'-Biphenyl)EPA 625.1 X
Biphenyl (1,1'-Biphenyl)EPA 8270C X X
Biphenyl (1,1'-Biphenyl)EPA 8270D X X
Biphenyl (1,1'-Biphenyl)EPA 8270E X X
bis(2-Chloroethoxy)methane EPA 625.1 X
bis(2-Chloroethoxy)methane EPA 8270C X X
bis(2-Chloroethoxy)methane EPA 8270D X X
bis(2-Chloroethoxy)methane EPA 8270E X X
bis(2-Chloroethyl) ether EPA 625.1 X
bis(2-Chloroethyl) ether EPA 8270C X X
bis(2-Chloroethyl) ether EPA 8270D X X
bis(2-Chloroethyl) ether EPA 8270E X X
Bis(2-Chloroisopropyl) ether EPA 625.1 X
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Bis(2-Chloroisopropyl) ether EPA 8270E X X
Bis(2-Chloroisopropyl) ether
(2,2-oxybis(1-chloropropane))EPA 8270C X X
Bis(2-Chloroisopropyl) ether
(2,2-oxybis(1-chloropropane))EPA 8270D X X
bis(2-Ethylhexyl)adipate EPA 625.1 X
bis(2-Ethylhexyl)adipate EPA 625.1 SIM X
Bolstar (Sulprofos)EPA 1657 X
Bolstar (Sulprofos)EPA 8141A X X
Bolstar (Sulprofos)EPA 8141B X X
Boron EPA 200.7 X X
Boron EPA 200.8 X
Boron EPA 6010B X X
Boron EPA 6010C X X
Boron EPA 6010D X X
Boron EPA 6020 X X
Boron EPA 6020A X X
Boron EPA 6020B X X
Bromide EPA 300.0 X X X
Bromide EPA 9056 X X
Bromide EPA 9056A X X
Bromide SM 4110 B-2011 X X
Bromoacetic acid EPA 552.2 X
Bromobenzene EPA 524.2 X
Bromobenzene EPA 624 (extended) X
Bromobenzene EPA 624.1 X
Bromobenzene EPA 8260B X X
Bromobenzene EPA 8260C X X
Bromobenzene EPA 8260D X X
Bromobenzene SM 6200 B-2011 X
Bromochloromethane EPA 524.2 X
Bromochloromethane EPA 624.1 X
Bromochloromethane EPA 8260B X X
Bromochloromethane EPA 8260C X X
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Bromochloromethane EPA 8260D X X
Bromochloromethane SM 6200 B-2011 X
Bromodichloromethane EPA 624.1 X
Bromodichloromethane EPA 8260B X X
Bromodichloromethane EPA 8260C X X
Bromodichloromethane EPA 8260D X X
Bromodichloromethane EPA TO-15 X
Bromodichloromethane SM 6200 B-2011 X
Bromoethane (Ethyl Bromide)EPA 624.1 X
Bromoethane (Ethyl Bromide)EPA TO-15 X
Bromoform EPA 624.1 X
Bromoform EPA 8260B X X
Bromoform EPA 8260C X X
Bromoform EPA 8260D X X
Bromoform EPA TO-15 X
Bromoform SM 6200 B-2011 X
Bromoform EPA 524.2 X
Butachlor EPA 507 X X
Butyl benzyl phthalate EPA 625.1 X
Butyl benzyl phthalate EPA 8270C X X
Butyl benzyl phthalate EPA 8270D X X
Butyl benzyl phthalate EPA 8270E X X
Cadmium EPA 200.7 X X
Cadmium EPA 200.8 X X
Cadmium EPA 6010B X X
Cadmium EPA 6010C X X
Cadmium EPA 6010D X X
Cadmium EPA 6020 X X
Cadmium EPA 6020A X X
Cadmium EPA 6020B X X
Calcium EPA 200.7 X X
Calcium EPA 200.8 X
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Calcium EPA 6010B X X
Calcium EPA 6010C X X
Calcium EPA 6010D X X
Calcium EPA 6020 X X
Calcium EPA 6020A X X
Calcium EPA 6020B X X
Calcium hardness as CaCO3 EPA 200.7 X
Calcium hardness as CaCO3 EPA 200.8 X
Calcium hardness as CaCO3 EPA 6010B X
Calcium hardness as CaCO3 EPA 6010C X X
Calcium hardness as CaCO3 EPA 6010D X
Calcium hardness as CaCO3 SM 2340 B-2011 X
California Waste Extraction
Test
CCR Chapter 11,
Article 5 Appendix II X
Caprolactam EPA 625.1 X
Caprolactam EPA 8270C X X
Caprolactam EPA 8270D X X
Caprolactam EPA 8270E X X
Carbazole EPA 625.1 X
Carbazole EPA 8270C X X
Carbazole EPA 8270D X X
Carbazole EPA 8270E X X
Carbon dioxide ASTM D1946-90 X
Carbon dioxide
SM 4500-CO2 D-
2011 X X
Carbon disulfide EPA 624.1 X
Carbon disulfide EPA 8260B X X
Carbon disulfide EPA 8260C X X
Carbon disulfide EPA 8260D X X
Carbon disulfide EPA TO-15 X
Carbon disulfide SM 6200 B-2011 X
Carbon disulfide EPA 524.2 X
Carbon monoxide ASTM D1946-90 X
Carbon tetrachloride EPA 624.1 X
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Carbon tetrachloride EPA 8260B X X
Carbon tetrachloride EPA 8260C X X
Carbon tetrachloride EPA 8260D X X
Carbon tetrachloride EPA TO-15 X
Carbon tetrachloride
EPA TO-15 GC/MS
SIM X
Carbon tetrachloride SM 6200 B-2011 X
Carbon tetrachloride EPA 524.2 X
Carbon-14
EPA EERF Method
C-01 X X X X
Carbonaceous BOD, CBOD SM 5210 B-2011 X
Carbophenothion EPA 8141A X
Carbophenothion EPA 8141B X
Ceriodaphnia dubia EPA 1002 X
Ceriodaphnia dubia
EPA 2002
Ceriodaphnia dubia X
Ceriodaphnia dubia EPA 2002.0 X
Cesium-134 DOE 4.5.2.3 X
Cesium-134 EPA 901.1 X X
Cesium-134 HASL 300 Ga-01-R X
Cesium-137 DOE 4.5.2.3 X
Cesium-137 EPA 901.1 X X
Cesium-137 HASL 300 Ga-01-R X
Chemical oxygen demand EPA 410.4 X
Chemical oxygen demand SM 5220 D-2011 X
Chlorate EPA 300.0 X
Chlordane (tech.)EPA 608.3 X
Chlordane (tech.)EPA 8081A X X
Chlordane (tech.)EPA 8081B X X
Chloride EPA 300.0 X X X
Chloride EPA 9056 X X
Chloride EPA 9056A X X
Chloride SM 4110 B-2011 X X
Chlorine EPA 9076 X
Chlorine SM 4500-Cl G-2011 X X
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Chloroacetic acid EPA 552.2 X
Chlorobenzene EPA 624.1 X
Chlorobenzene EPA 8260B X X
Chlorobenzene EPA 8260C X X
Chlorobenzene EPA 8260D X X
Chlorobenzene EPA TO-15 X
Chlorobenzene SM 6200 B-2011 X
Chlorobenzene EPA 524.2 X
Chlorobenzilate EPA 625.1 X
Chlorobenzilate EPA 8270C X X
Chlorobenzilate EPA 8270D X X
Chlorobenzilate EPA 8270E X X
Chlorodibromomethane EPA 524.2 X
Chlorodibromomethane
(dibromochloromethane)EPA 624.1 X
Chlorodibromomethane
(dibromochloromethane)EPA 8260B X X
Chlorodibromomethane
(dibromochloromethane)EPA 8260C X X
Chlorodibromomethane
(dibromochloromethane)EPA 8260D X X
Chlorodibromomethane
(dibromochloromethane)EPA TO-15 X
Chlorodibromomethane
(dibromochloromethane)SM 6200 B-2011 X
Chloroethane EPA 524.2 X
Chloroethane (Ethyl chloride)EPA 624.1 X
Chloroethane (Ethyl chloride)EPA 8260B X X
Chloroethane (Ethyl chloride)EPA 8260C X X
Chloroethane (Ethyl chloride)EPA 8260D X X
Chloroethane (Ethyl chloride)EPA TO-15 X
Chloroethane (Ethyl chloride)
EPA TO-15 GC/MS
SIM X
Chloroethane (Ethyl chloride)SM 6200 B-2011 X
Chloroform EPA 624.1 X
Chloroform EPA 8260B X X
Chloroform EPA 8260C X X
Chloroform EPA 8260D X X
Chloroform EPA TO-15 X
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Chloroform
EPA TO-15 GC/MS
SIM X
Chloroform SM 6200 B-2011 X
Chloroform EPA 524.2 X
Chloromethane EPA 524.2 X
Chloroprene (2-Chloro-1,3-
butadiene)EPA 624.1 X
Chloroprene (2-Chloro-1,3-
butadiene)EPA 8260B X X
Chloroprene (2-Chloro-1,3-
butadiene)EPA 8260C X X
Chloroprene (2-Chloro-1,3-
butadiene)EPA 8260D X X
Chloroprene (2-Chloro-1,3-
butadiene)SM 6200 B-2011 X
Chlorpyrifos EPA 1657 X
Chlorpyrifos EPA 8141A X X
Chlorpyrifos EPA 8141B X X
Chromium EPA 200.7 X X
Chromium EPA 200.8 X X
Chromium EPA 6010B X X
Chromium EPA 6010C X X
Chromium EPA 6010D X X
Chromium EPA 6020 X X
Chromium EPA 6020A X X
Chromium EPA 6020B X X
Chromium VI EPA 218.6 X X
Chromium VI EPA 3060A X
Chromium VI EPA 7196A X X
Chromium VI EPA 7199 X X
Chromium VI SM 3500-Cr B-2011 X X
Chromium VI SM 3500-Cr C-2011 X X
Chromium VI Digestion EPA 3060A X
Chrysene EPA 610 (HPLC) X
Chrysene EPA 625.1 X
Chrysene EPA 625.1 SIM X
Chrysene EPA 8270C X X
Chrysene EPA 8270C SIM X X
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Chrysene EPA 8270D X X
Chrysene EPA 8270D SIM X X
Chrysene EPA 8270E X X
Chrysene EPA 8270E SIM X X
Chrysene EPA 8310 X X
Chrysene MADEP EPH X X
cis-1,2-Dichloroethene EPA 524.2 X
cis-1,2-Dichloroethylene EPA 624.1 X
cis-1,2-Dichloroethylene EPA 8260B X X
cis-1,2-Dichloroethylene EPA 8260C X X
cis-1,2-Dichloroethylene EPA 8260D X X
cis-1,2-Dichloroethylene EPA TO-15 X
cis-1,2-Dichloroethylene
EPA TO-15 GC/MS
SIM X
cis-1,2-Dichloroethylene SM 6200 B-2011 X
cis-1,3-Dichloropropene EPA 524.2 X
cis-1,3-Dichloropropene EPA 624.1 X
cis-1,3-Dichloropropene EPA 8260B X X
cis-1,3-Dichloropropene EPA 8260C X X
cis-1,3-Dichloropropene EPA 8260D X X
cis-1,3-Dichloropropene EPA TO-15 X
cis-1,3-Dichloropropene
EPA TO-15 GC/MS
SIM X
cis-1,3-Dichloropropene SM 6200 B-2011 X
cis-1,4-Dichloro-2-butene EPA 624.1 X
cis-1,4-Dichloro-2-butene EPA 8260B X X
cis-1,4-Dichloro-2-butene EPA 8260C X X
cis-1,4-Dichloro-2-butene EPA 8260D X X
cis-1,4-Dichloro-2-butene SM 6200 B-2011 X
cis-Diallate EPA 8270C X
cis-Isosafrole EPA 8270C X
Closed-System Purge-and-Trap
and Extraction for Volatile EPA 5035A X
Cobalt EPA 200.7 X X
Cobalt EPA 200.8 X
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Cobalt EPA 6010B X X
Cobalt EPA 6010C X X
Cobalt EPA 6010D X X
Cobalt EPA 6020 X X
Cobalt EPA 6020A X X
Cobalt EPA 6020B X X
Cobalt-60 DOE 4.5.2.3 X
Cobalt-60 EPA 901.1 X X
Cobalt-60 HASL 300 Ga-01-R X
Color SM 2120 B-2011 X X
Conductivity EPA 120.1 X X
Conductivity EPA 9050A X X
Conductivity SM 2510 B-2011 X X
Copper EPA 200.7 X X
Copper EPA 200.8 X X
Copper EPA 6010B X X
Copper EPA 6010C X X
Copper EPA 6010D X X
Copper EPA 6020 X X
Copper EPA 6020A X X
Copper EPA 6020B X X
Corrosivity (langlier index)SM 2320 B-2011 X X
Corrosivity (pH)EPA 9040B X
Corrosivity (pH)EPA 9040C X
Corrosivity (pH)EPA 9045D X
Coumaphos EPA 1657 X
Coumaphos EPA 8141A X X
Coumaphos EPA 8141B X X
Cyanazine EPA 8141A X X
Cyanazine EPA 8141B X X
Cyanide EPA 335.4 X X
Cyanide EPA 9010B X X
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Cyanide EPA 9010C X X
Cyanide EPA 9012A X
Cyanide EPA 9012B X X
Cyanide EPA 9013 X
Cyanide EPA 9013A X
Cyanide EPA 9014 X X
Cyanide
SM 4500-CN¯ B-
2011 X X
Cyanide
SM 4500-CN¯ C-
2011 X X
Cyanide
SM 4500-CN¯ E-
2011 X X
Cyanide
SM 4500-CN¯ G-
2011 X
Cyclohexane EPA 624.1 X
Cyclohexane EPA 8260B X X
Cyclohexane EPA 8260C X X
Cyclohexane EPA 8260D X X
Cyclohexane EPA TO-15 X
Cyclohexane SM 6200 B-2011 X
Cyclohexanone EPA 624.1 X
Cyclohexanone EPA 8260B X X
Cyclohexanone EPA 8260C X X
Cyclohexanone EPA 8260D X X
Cyclohexanone SM 6200 B-2011 X
Dalapon EPA 8151A X X
Dalapon SM 6640 B-2001 X
delta-BHC EPA 608.3 X
delta-BHC EPA 8081A X X
delta-BHC EPA 8081B X X
Demeton EPA 1657 X
Demeton EPA 8141A X X
Demeton EPA 8141B X X
Demeton-o EPA 8141A X X
Demeton-o EPA 8141B X X
Demeton-s EPA 8141A X X
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Demeton-s EPA 8141B X X
Di(2-ethylhexyl) phthalate
(bis(2-Ethylhexyl)phthalate, EPA 625.1 X
Di(2-ethylhexyl) phthalate
(bis(2-Ethylhexyl)phthalate, EPA 8270C X X
Di(2-ethylhexyl) phthalate
(bis(2-Ethylhexyl)phthalate, EPA 8270D X X
Di(2-ethylhexyl) phthalate
(bis(2-Ethylhexyl)phthalate, EPA 8270E X X
Diallate EPA 625.1 X
Diallate EPA 8270C X X
Diallate EPA 8270D X X
Diallate EPA 8270E X X
Diazinon EPA 1657 X
Diazinon EPA 8141A X X
Diazinon EPA 8141B X X
Dibenz(a, h) acridine EPA 625.1 X
Dibenz(a, h) acridine EPA 8270C X X
Dibenz(a, h) acridine EPA 8270D X X
Dibenz(a, h) acridine EPA 8270E X X
Dibenz(a, j)acridine EPA 625.1 X
Dibenz(a, j)acridine EPA 8270C X X
Dibenz(a, j)acridine EPA 8270D X X
Dibenz(a, j)acridine EPA 8270E X X
Dibenz(a,h)anthracene EPA 610 (HPLC) X
Dibenz(a,h)anthracene EPA 625.1 X
Dibenz(a,h)anthracene EPA 625.1 SIM X
Dibenz(a,h)anthracene EPA 8270C X X
Dibenz(a,h)anthracene EPA 8270C SIM X X
Dibenz(a,h)anthracene EPA 8270D X X
Dibenz(a,h)anthracene EPA 8270D SIM X X
Dibenz(a,h)anthracene EPA 8270E X X
Dibenz(a,h)anthracene EPA 8270E SIM X X
Dibenz(a,h)anthracene EPA 8310 X X
Dibenz(a,h)anthracene MADEP EPH X X
Dibenzo(a,e)pyrene EPA 8270C X X
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Dibenzo(a,e)pyrene EPA 8270D X X
Dibenzo(a,e)pyrene EPA 8270E X X
Dibenzo(a,h) pyrene EPA 8270C X X
Dibenzo(a,h) pyrene EPA 8270D X X
Dibenzo(a,h) pyrene EPA 8270E X X
Dibenzo(a,i) pyrene EPA 8270C X X
Dibenzo(a,i) pyrene EPA 8270D X X
Dibenzo(a,i) pyrene EPA 8270E X X
Dibenzofuran EPA 625.1 X
Dibenzofuran EPA 8270C X X
Dibenzofuran EPA 8270D X X
Dibenzofuran EPA 8270E X X
Dibromoacetic acid EPA 552.2 X
Dibromomethane EPA 524.2 X
Dibromomethane (Methylene
bromide)EPA 624.1 X
Dibromomethane (Methylene
bromide)EPA 8260B X X
Dibromomethane (Methylene
bromide)EPA 8260C X X
Dibromomethane (Methylene
bromide)EPA 8260D X X
Dibromomethane (Methylene
bromide)SM 6200 B-2011 X
Dicamba EPA 8151A X X
Dicamba SM 6640 B-2001 X
Dichlorobromomethane EPA 524.2 X
Dichlorodifluoromethane EPA 524.2 X
Dichlorodifluoromethane
(Freon-12)EPA 624.1 X
Dichlorodifluoromethane
(Freon-12)EPA 8260B X X
Dichlorodifluoromethane
(Freon-12)EPA 8260C X X
Dichlorodifluoromethane
(Freon-12)EPA 8260D X X
Dichlorodifluoromethane
(Freon-12)EPA TO-15 X
Dichlorodifluoromethane
(Freon-12)SM 6200 B-2011 X
Dichloroeacetic acid EPA 552.2 X
Dichloroprop (Dichlorprop)EPA 8151A X X
Dichlorovos (DDVP,
Dichlorvos)EPA 1657 X
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Dichlorovos (DDVP,
Dichlorvos)EPA 8141A X X
Dichlorovos (DDVP,
Dichlorvos)EPA 8141B X X
Dichlorvos EPA 507 X
Dicyclopentadiene EPA 8260B X
Dicyclopentadiene EPA 8260C X
Dicyclopentadiene EPA 8260D X
Dicyclopentadiene EPA TO-15 X
Dieldrin EPA 608.3 X
Dieldrin EPA 8081A X X
Dieldrin EPA 8081B X X
Diesel range organics (DRO)CA LUFT GCMS X
Diesel range organics (DRO)EPA 8015B X X
Diesel range organics (DRO)EPA 8015C X X
Diesel range organics (DRO)EPA 8015D X X
Diesel range organics (DRO)EPA 8270C X X
Diesel range organics (DRO)EPA 8270D X X
Diesel range organics (DRO)EPA 8270E X
Diesel range organics (DRO)IDNR OA-2 X X
Diesel range organics (DRO)LUFT GC X X
Diesel range organics (DRO)LUFT GCMS X
Diesel range organics (DRO)MADEP EPH X
Diesel range organics (DRO)MO-DRO X X
Diesel range organics (DRO)NWTPH-Dx X X
Diesel range organics (DRO)OA-2 X
Diesel range organics (DRO)OK DEQ DRO X X
Diesel range organics (DRO)OK DEQ GRO X
Diesel range organics (DRO)WI(95) DRO X X
Diethyl ether EPA 624.1 X
Diethyl ether EPA 8260B X X
Diethyl ether EPA 8260C X X
Diethyl ether EPA 8260D X X
Diethyl ether SM 6200 B-2011 X
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Diethyl phthalate EPA 625.1 X
Diethyl phthalate EPA 8270C X X
Diethyl phthalate EPA 8270D X X
Diethyl phthalate EPA 8270E X X
Di-isopropylether (DIPE)
(Isopropyl ether)EPA 624.1 X
Di-isopropylether (DIPE)
(Isopropyl ether)EPA 8260B X X
Di-isopropylether (DIPE)
(Isopropyl ether)EPA 8260C X X
Di-isopropylether (DIPE)
(Isopropyl ether)EPA 8260D X X
Di-isopropylether (DIPE)
(Isopropyl ether)SM 6200 B-2011 X
Dimethoate EPA 1657 X
Dimethoate EPA 625.1 X
Dimethoate EPA 8141A X X
Dimethoate EPA 8141B X X
Dimethoate EPA 8270C X X
Dimethoate EPA 8270D X X
Dimethoate EPA 8270E X X
Dimethyl phthalate EPA 625.1 X
Dimethyl phthalate EPA 8270C X X
Dimethyl phthalate EPA 8270D X X
Dimethyl phthalate EPA 8270E X X
Di-n-butyl phthalate EPA 625.1 X
Di-n-butyl phthalate EPA 8270C X X
Di-n-butyl phthalate EPA 8270D X X
Di-n-butyl phthalate EPA 8270E X X
Di-n-octyl phthalate EPA 625.1 X
Di-n-octyl phthalate EPA 8270C X X
Di-n-octyl phthalate EPA 8270D X X
Di-n-octyl phthalate EPA 8270E X X
Dinoseb (2-sec-butyl-4,6-
dinitrophenol, DNBP)EPA 625.1 X
Dinoseb (2-sec-butyl-4,6-
dinitrophenol, DNBP)EPA 8151A X X
Dinoseb (2-sec-butyl-4,6-
dinitrophenol, DNBP)EPA 8270C X X
Dinoseb (2-sec-butyl-4,6-
dinitrophenol, DNBP)EPA 8270D X X
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Dinoseb (2-sec-butyl-4,6-
dinitrophenol, DNBP)EPA 8270E X X
Dinoseb (2-sec-butyl-4,6-
dinitrophenol, DNBP)SM 6640 B-2001 X
Diphenyl ether (Diphenyl
Oxide)EPA 625.1 X
Diphenyl ether (Diphenyl
Oxide)EPA 8270C X X
Diphenyl ether (Diphenyl
Oxide)EPA 8270D X X
Diphenyl ether (Diphenyl
Oxide)EPA 8270E X X
Diphenyl ketone
(Benzophenone)EPA 8270C X
Diphenyl ketone
(Benzophenone)EPA 8270D X
Diphenyl ketone
(Benzophenone)EPA 8270E X
Diphenylamine EPA 625.1 X
Diphenylamine EPA 8270C X X
Diphenylamine EPA 8270D X X
Diphenylamine EPA 8270E X X
Dissolved Carbon SM 5310 B-2011 X
Dissolved organic carbon
(DOC)EPA 9060 X
Dissolved organic carbon
(DOC)EPA 9060A X
Dissolved organic carbon
(DOC)SM 5310 B-2011 X
Dissolved organic carbon
(DOC)SM 5310 C-2011 X
Disulfoton EPA 1657 X
Disulfoton EPA 8141A X X
Disulfoton EPA 8141B X X
Disulfoton EPA 8270C X X
Disulfoton EPA 8270D X X
Disulfoton EPA 8270E X X
Endosulfan I EPA 608.3 X
Endosulfan I EPA 8081A X X
Endosulfan I EPA 8081B X X
Endosulfan II EPA 608.3 X
Endosulfan II EPA 8081A X X
Endosulfan II EPA 8081B X X
Endosulfan sulfate EPA 608.3 X
Endosulfan sulfate EPA 8081A X X
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Endosulfan sulfate EPA 8081B X X
Endrin EPA 608.3 X
Endrin EPA 8081A X X
Endrin EPA 8081B X X
Endrin aldehyde EPA 608.3 X
Endrin aldehyde EPA 8081A X X
Endrin aldehyde EPA 8081B X X
Endrin ketone EPA 608.3 X
Endrin ketone EPA 8081A X X
Endrin ketone EPA 8081B X X
Enterococci ASTM D6503-99 X
Enterococci Enterolert® X
EPH Aliphatic >C10-C12 MADEP EPH X X
EPH Aliphatic >C12-C16 MADEP EPH X X
EPH Aliphatic >C16-C35 MADEP EPH X X
EPH Aliphatic C19-C36 MADEP EPH X X
EPH Aliphatic C9-C18 MADEP EPH X X
EPH Aromatic >C10-C12 MADEP EPH X X
EPH Aromatic >C12-C16 MADEP EPH X X
EPH Aromatic >C16-C21 MADEP EPH X X
EPH Aromatic >C21-C35 MADEP EPH X X
EPH Aromatic C11-C22 MADEP EPH X X
EPH Aromatic C11-C22
Unadjusted MADEP EPH X X
EPN EPA 1657 X
EPN EPA 8141A X X
EPN EPA 8141B X X
Escherichia coli SM 9223 B-2004 X X
Ethane
EPA RSK-175
(GC/FID)X X
Ethanol EPA 624.1 X
Ethanol EPA 8015 X
Ethanol EPA 8015B X X
Ethanol EPA 8015C X X
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Ethanol EPA 8015D X X
Ethanol EPA 8260B X X
Ethanol EPA 8260C X X
Ethanol EPA 8260D X X
Ethanol EPA TO-15 X
Ethanol SM 6200 B-2011 X
Ethene
EPA RSK-175
(GC/FID)X X
Ethion EPA 8141A X
Ethion EPA 8141B X
Ethoprop EPA 1657 X
Ethoprop EPA 507 X
Ethoprop EPA 8141A X X
Ethoprop EPA 8141B X X
Ethyl acetate EPA 624.1 X
Ethyl acetate EPA 8260B X X
Ethyl acetate EPA 8260C X X
Ethyl acetate EPA 8260D X X
Ethyl acetate EPA TO-15 X
Ethyl acetate SM 6200 B-2011 X
Ethyl methacrylate EPA 624.1 X
Ethyl methacrylate EPA 8260B X X
Ethyl methacrylate EPA 8260C X X
Ethyl methacrylate EPA 8260D X X
Ethyl methacrylate SM 6200 B-2011 X
Ethyl methanesulfonate EPA 625.1 X
Ethyl methanesulfonate EPA 8270C X X
Ethyl methanesulfonate EPA 8270D X X
Ethyl methanesulfonate EPA 8270E X X
Ethylbenzene CA LUFT GCMS X X
Ethylbenzene EPA 524.2 X
Ethylbenzene EPA 602 X
Ethylbenzene EPA 624.1 X
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Ethylbenzene EPA 8021B X X
Ethylbenzene EPA 8260B X X
Ethylbenzene EPA 8260C X X
Ethylbenzene EPA 8260D X X
Ethylbenzene EPA TO-15 X
Ethylbenzene
EPA TO-15 GC/MS
SIM X
Ethylbenzene IDNR OA-1 X X
Ethylbenzene MADEP VPH X X
Ethylbenzene OK DEQ GRO X X
Ethylbenzene SM 6200 B-2011 X
Ethylene glycol EPA 8015B X X
Ethylene glycol EPA 8015C X X
Ethylene glycol EPA 8015D X X
Ethyl-t-butyl ether (ETBE) (2-
Ethoxy-2-methylpropane)EPA 624.1 X
Ethyl-t-butyl ether (ETBE) (2-
Ethoxy-2-methylpropane)EPA 8260B X X
Ethyl-t-butyl ether (ETBE) (2-
Ethoxy-2-methylpropane)EPA 8260C X X
Ethyl-t-butyl ether (ETBE) (2-
Ethoxy-2-methylpropane)EPA 8260D X X
Ethyl-t-butyl ether (ETBE) (2-
Ethoxy-2-methylpropane)SM 6200 B-2011 X
Extractable organics halides
(EOX)EPA 9023 X
Extractable Petroleum
Hydrocarbons (EPH)CT ETPH X
Extractable Petroleum
Hydrocarbons (EPH)IDNR OA-2 X X
Extractable Petroleum
Hydrocarbons (EPH)MADEP EPH X X
Extractable Petroleum
Hydrocarbons (EPH)NJDEP EPH 10/08 X
Extractable Petroleum
Hydrocarbons (EPH)TN EPH X X
Extractable Total Petroleum
Hydrocarbons NJDEP EPH 10/08 X
Famphur EPA 625.1 X
Famphur EPA 8141A X
Famphur EPA 8141B X
Famphur EPA 8270C X X
Famphur EPA 8270D X X
Famphur EPA 8270E X X
Fecal coliforms EPA 1681 X X
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Fecal coliforms SM 9223 B-2004 X
Fensulfothion EPA 1657 X
Fensulfothion EPA 8141A X X
Fensulfothion EPA 8141B X X
Fenthion EPA 1657 X
Fenthion EPA 8141A X X
Fenthion EPA 8141B X X
Flash Point ASTM D93 X X
Flash Point ASTM D93-07 X X
Florisil Clean-up EPA 3620 X
Florisil Clean-up EPA 3620C X
Fluoranthene EPA 610 (HPLC) X
Fluoranthene EPA 625.1 X
Fluoranthene EPA 625.1 SIM X
Fluoranthene EPA 8270C X X
Fluoranthene EPA 8270C SIM X X
Fluoranthene EPA 8270D X X
Fluoranthene EPA 8270D SIM X X
Fluoranthene EPA 8270E X X
Fluoranthene EPA 8270E SIM X X
Fluoranthene EPA 8310 X X
Fluoranthene MADEP EPH X X
Fluorene EPA 610 (HPLC) X
Fluorene EPA 625.1 X
Fluorene EPA 625.1 SIM X
Fluorene EPA 8270C X X
Fluorene EPA 8270C SIM X X
Fluorene EPA 8270D X X
Fluorene EPA 8270D SIM X X
Fluorene EPA 8270E X X
Fluorene EPA 8270E SIM X X
Fluorene EPA 8310 X X
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Fluorene MADEP EPH X X
Fluoride EPA 300.0 X X X
Fluoride EPA 9056 X X
Fluoride EPA 9056A X X
Fluoride SM 4110 B-2011 X X
Fluoride SM 4500-F¯ B-2011 X
Fluoride SM 4500-F¯ C-2011 X
Fractional Organic Carbon
(FOC)ASTM D2974 X
Free cyanide EPA 9014 X
Free liquid EPA 9095A X
Free liquid EPA 9095B X X
Gamma Emitters DOE 4.5.2.3 X X
Gamma Emitters EPA 901.1 X X X
Gamma Emitters HASL 300 Ga-01-R X X X X
gamma-BHC (Lindane, gamma-
Hexachlorocyclohexane)EPA 608.3 X
gamma-BHC (Lindane, gamma-
Hexachlorocyclohexane)EPA 8081A X X
gamma-BHC (Lindane, gamma-
Hexachlorocyclohexane)EPA 8081B X X
gamma-Chlordane EPA 608.3 X
gamma-Chlordane EPA 8081A X X
gamma-Chlordane EPA 8081B X X
Gasoline range organics (GRO)CA LUFT GCMS X
Gasoline range organics (GRO)EPA 8015B X X
Gasoline range organics (GRO)EPA 8015C X X
Gasoline range organics (GRO)EPA 8015D X X
Gasoline range organics (GRO)EPA 8260B X X
Gasoline range organics (GRO)EPA 8260C X X
Gasoline range organics (GRO)EPA 8260D X X
Gasoline range organics (GRO)EPA TO-15 X
Gasoline range organics (GRO)IDNR OA-1 X X
Gasoline range organics (GRO)LUFT GC X X
Gasoline range organics (GRO)LUFT GCMS X
Gasoline range organics (GRO)MADEP VPH X
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Gasoline range organics (GRO)MO-GRO X
Gasoline range organics (GRO)NWTPH-Gx X X
Gasoline range organics (GRO)OK DEQ GRO X X
Gasoline range organics (GRO)TN GRO X
Gasoline range organics (GRO)WI(95) GRO X X
Gross alpha-beta EPA 900 X
Gross alpha-beta EPA 9310 X X
Gross-alpha EPA 900 X
Gross-alpha EPA 900.0 (GPC) X X X
Gross-alpha EPA 9310 X X X
Gross-alpha Radium EPA 900.1 X
Gross-beta EPA 900 X
Gross-beta EPA 900.0 (GPC) X X X
Gross-beta EPA 9310 X X X
Guanidine Nitrate EPA 9056 X X
Guanidine Nitrate EPA 9056A X X
Hardness EPA 130.1 X X
Hardness SM 2340 B-2011 X X
Hardness (calc.)EPA 200.7 X X
Hardness (calc.)EPA 200.8 X
Hardness (calc.)SM 2340 B-2011 X X
Helium ASTM D1946-90 X
Heptachlor EPA 608.3 X
Heptachlor EPA 8081A X X
Heptachlor EPA 8081B X X
Heptachlor epoxide EPA 608.3 X
Heptachlor epoxide EPA 8081A X X
Heptachlor epoxide EPA 8081B X X
Heterotrophic plate count
SM 9215 B 2000
(PCA) X X
Hexachlorobenzene EPA 608.3 X
Hexachlorobenzene EPA 625.1 X
Hexachlorobenzene EPA 625.1 SIM X
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Hexachlorobenzene EPA 8081A X X
Hexachlorobenzene EPA 8081B X X
Hexachlorobenzene EPA 8270C X X
Hexachlorobenzene EPA 8270C SIM X X
Hexachlorobenzene EPA 8270D X X
Hexachlorobenzene EPA 8270D SIM X X
Hexachlorobenzene EPA 8270E X X
Hexachlorobenzene EPA 8270E SIM X
Hexachlorobutadiene EPA 624.1 X
Hexachlorobutadiene EPA 625.1 X
Hexachlorobutadiene EPA 8260B X X
Hexachlorobutadiene EPA 8260C X X
Hexachlorobutadiene EPA 8260D X X
Hexachlorobutadiene EPA 8270C X X
Hexachlorobutadiene EPA 8270D X X
Hexachlorobutadiene EPA 8270E X X
Hexachlorobutadiene EPA TO-15 X
Hexachlorobutadiene SM 6200 B-2011 X
Hexachlorobutadiene EPA 524.2 X
Hexachlorocyclopentadiene EPA 625.1 X
Hexachlorocyclopentadiene EPA 8270C X X
Hexachlorocyclopentadiene EPA 8270D X X
Hexachlorocyclopentadiene EPA 8270E X X
Hexachloroethane EPA 624.1 X
Hexachloroethane EPA 625.1 X
Hexachloroethane EPA 8260B X X
Hexachloroethane EPA 8260C X X
Hexachloroethane EPA 8260D X X
Hexachloroethane EPA 8270C X X
Hexachloroethane EPA 8270D X X
Hexachloroethane EPA 8270E X X
Hexachloroethane SM 6200 B-2011 X
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Hexachlorophene EPA 625.1 X
Hexachlorophene EPA 8270C X X
Hexachlorophene EPA 8270D X X
Hexachlorophene EPA 8270E X X
Hexachloropropene EPA 625.1 X
Hexachloropropene EPA 8270C X X
Hexachloropropene EPA 8270D X X
Hexachloropropene EPA 8270E X X
Hydroquinone EPA 625.1 X
Hydroquinone EPA 8270C X
Hydroquinone EPA 8270D X
IC25 (ON) Growth
EPA 1000.0 - Fathead
minnow, 7-day X
IC25 Reproduction
EPA 1002.0 -
Ceriodaphnia dubia, X
IC25 Survival
EPA 1000.0 - Fathead
minnow, 7-day X
IC25 Survival
EPA 1002.0 -
Ceriodaphnia dubia, X
Ignitability EPA 1010 X X
Ignitability EPA 1010A X X
Indene EPA 625.1 X
Indene EPA 8270C X X
Indene EPA 8270D X X
Indene EPA 8270E X X
Indeno(1,2,3-cd)pyrene EPA 610 (HPLC) X
Indeno(1,2,3-cd)pyrene EPA 625.1 X
Indeno(1,2,3-cd)pyrene EPA 625.1 SIM X
Indeno(1,2,3-cd)pyrene EPA 8270C X X
Indeno(1,2,3-cd)pyrene EPA 8270C SIM X X
Indeno(1,2,3-cd)pyrene EPA 8270D X X
Indeno(1,2,3-cd)pyrene EPA 8270D SIM X X
Indeno(1,2,3-cd)pyrene EPA 8270E X X
Indeno(1,2,3-cd)pyrene EPA 8270E SIM X X
Indeno(1,2,3-cd)pyrene EPA 8310 X X
Indeno(1,2,3-cd)pyrene MADEP EPH X X
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Inorganic Carbon SM 5310 B-2011 X
Iodomethane (Methyl iodide)EPA 624 (extended) X
Iodomethane (Methyl iodide)EPA 624.1 X
Iodomethane (Methyl iodide)EPA 8260B X X
Iodomethane (Methyl iodide)EPA 8260C X X
Iodomethane (Methyl iodide)EPA 8260D X X
Iodomethane (Methyl iodide)EPA TO-15 X
Iodomethane (Methyl iodide)SM 6200 B-2011 X
Iron EPA 200.7 X X
Iron EPA 200.8 X
Iron EPA 6010B X X
Iron EPA 6010C X X
Iron EPA 6010D X X
Iron EPA 6020 X X
Iron EPA 6020A X X
Iron EPA 6020B X X
Iron-(II) (Ferrous Iron)SM 3500-Fe B-2011 X
Isobutyl alcohol (2-Methyl-1-
propanol)EPA 624.1 X
Isobutyl alcohol (2-Methyl-1-
propanol)EPA 8260B X X
Isobutyl alcohol (2-Methyl-1-
propanol)EPA 8260C X X
Isobutyl alcohol (2-Methyl-1-
propanol)EPA 8260D X X
Isobutyl alcohol (2-Methyl-1-
propanol)SM 6200 B-2011 X
Isodrin EPA 625.1 X
Isodrin EPA 8270C X X
Isodrin EPA 8270D X X
Isodrin EPA 8270E X X
Isophorone EPA 625.1 X
Isophorone EPA 8270C X X
Isophorone EPA 8270D X X
Isophorone EPA 8270E X X
Isopropyl alcohol (2-Propanol,
Isopropanol)EPA 624.1 X
Isopropyl alcohol (2-Propanol,
Isopropanol)EPA 8260B X X
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Isopropyl alcohol (2-Propanol,
Isopropanol)EPA 8260C X X
Isopropyl alcohol (2-Propanol,
Isopropanol)EPA 8260D X X
Isopropyl alcohol (2-Propanol,
Isopropanol)EPA TO-15 X
Isopropyl alcohol (2-Propanol,
Isopropanol)SM 6200 B-2011 X
Isopropylbenzene EPA 524.2 X
Isopropylbenzene (Cumene)EPA 624 (extended) X
Isopropylbenzene (Cumene)EPA 624.1 X
Isopropylbenzene (Cumene)EPA 8260B X X
Isopropylbenzene (Cumene)EPA 8260C X X
Isopropylbenzene (Cumene)EPA 8260D X X
Isopropylbenzene (Cumene)EPA TO-15 X
Isopropylbenzene (Cumene)SM 6200 B-2011 X
Isosafrole EPA 8270C X X
Isosafrole EPA 8270D X X
Isosafrole EPA 8270E X X
Isotopic uranium
ASTM D3972-09
Modified (ENV-SOP- X
Isotopic uranium ASTM D3972-97 X
Kepone EPA 625.1 X
Kepone EPA 8270C X X
Kepone EPA 8270D X X
Kepone EPA 8270E X X
Kjeldahl nitrogen - total EPA 351.2 X
Kjeldahl nitrogen - total
SM 4500-NH3 B-
2011 X
Kjeldahl nitrogen - total
SM 4500-NH3 C-
2011 X
Kjeldahl nitrogen - total
SM 4500-Norg B-
2011 X
Kjeldahl nitrogen - total
SM 4500-Norg C-
2011 X
Kjeldahl nitrogen - total
SM 4500-Norg D-
2011 X X
LC50 Survival
EPA 2000.0 - Fathead
minnow, 48-hr Acute, X
LC50 Survival
EPA 2002
Ceriodaphnia dubia X
Lead EPA 200.7 X X
Lead EPA 200.8 X X
Lead EPA 6010B X X
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Lead EPA 6010C X X
Lead EPA 6010D X X
Lead EPA 6020 X X
Lead EPA 6020A X X
Lead EPA 6020B X X
Lead-210 DOE 4.5.2.3 X
Lead-210 Eichrom OTW01 X
Lead-210
EICHROM PBS01-
12 X X X X
Lead-210 HASL 300 Ga-01-R X
Legionella Legiolert X X
Lithium EPA 200.7 X X
Lithium EPA 6010B X X
Lithium EPA 6010C X X
Lithium EPA 6010D X X
Lithium EPA 6020 X
Lithium EPA 6020A X
Lithium EPA 6020B X
LOEC Survival EPA 2000 X
m+p-xylene EPA 602 X
m+p-xylene EPA 8021B X X
m+p-xylene EPA 8260B X X
m+p-xylene EPA 8260C X X
m+p-xylene EPA 8260D X
m+p-xylene EPA TO-15 X
m+p-xylene IDNR OA-1 X
m+p-xylene MADEP VPH X X
m+p-xylene SM 6200 B-2011 X
Magnesium EPA 200.7 X X
Magnesium EPA 200.8 X
Magnesium EPA 6010B X X
Magnesium EPA 6010C X X
Magnesium EPA 6010D X X
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Magnesium EPA 6020 X X
Magnesium EPA 6020A X X
Magnesium EPA 6020B X X
Malathion EPA 1657 X
Malathion EPA 8141A X X
Malathion EPA 8141B X X
Manganese EPA 200.7 X X
Manganese EPA 200.8 X X
Manganese EPA 6010B X X
Manganese EPA 6010C X X
Manganese EPA 6010D X X
Manganese EPA 6020 X X
Manganese EPA 6020A X X
Manganese EPA 6020B X X
MCPA EPA 8151A X X
MCPP EPA 8151A X X
Mercury EPA 245.1 X X
Mercury EPA 7470A X
Mercury EPA 7471A X
Mercury EPA 7471B X
Merphos EPA 1657 X
Merphos EPA 507 X
Merphos EPA 8141A X X
Merphos EPA 8141B X X
Methacrylonitrile EPA 624.1 X
Methacrylonitrile EPA 8260B X X
Methacrylonitrile EPA 8260C X X
Methacrylonitrile EPA 8260D X X
Methacrylonitrile SM 6200 B-2011 X
Methane ASTM D1946-90 X
Methane
EPA RSK-175
(GC/FID)X X
Methanol EPA 8015 X
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Methanol EPA 8015B X X
Methanol EPA 8015C X X
Methanol EPA 8015D X X
Methanol EPA 8260B X
Methanol EPA 8260C X
Methanol EPA TO-15 X
Methanol SM 6200 B-2011 X
Methapyrilene EPA 625.1 X
Methapyrilene EPA 8270C X X
Methapyrilene EPA 8270D X X
Methapyrilene EPA 8270E X X
Methoxychlor EPA 608.3 X
Methoxychlor EPA 8081A X X
Methoxychlor EPA 8081B X X
Methyl acetate EPA 624.1 X
Methyl acetate EPA 8260B X X
Methyl acetate EPA 8260C X X
Methyl acetate EPA 8260D X X
Methyl acetate SM 6200 B-2011 X
Methyl acrylate EPA 624.1 X
Methyl acrylate EPA 8260B X X
Methyl acrylate EPA 8260C X X
Methyl acrylate EPA 8260D X X
Methyl acrylate SM 6200 B-2011 X
Methyl bromide
(Bromomethane)EPA 624.1 X
Methyl bromide
(Bromomethane)EPA 8260B X X
Methyl bromide
(Bromomethane)EPA 8260C X X
Methyl bromide
(Bromomethane)EPA 8260D X X
Methyl bromide
(Bromomethane)EPA TO-15 X
Methyl bromide
(Bromomethane)SM 6200 B-2011 X
Methyl chloride
(Chloromethane)EPA 624.1 X
Methyl chloride
(Chloromethane)EPA 8260B X X
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Methyl chloride
(Chloromethane)EPA 8260C X X
Methyl chloride
(Chloromethane)EPA 8260D X X
Methyl chloride
(Chloromethane)EPA TO-15 X
Methyl chloride
(Chloromethane)
EPA TO-15 GC/MS
SIM X
Methyl chloride
(Chloromethane)SM 6200 B-2011 X
Methyl ethyl ketone EPA 524.2 X
Methyl iodide EPA 524.2 X
Methyl isobutyl ketone EPA 524.2 X
Methyl methacrylate EPA 624.1 X
Methyl methacrylate EPA 8260B X X
Methyl methacrylate EPA 8260C X X
Methyl methacrylate EPA 8260D X X
Methyl methacrylate EPA TO-15 X
Methyl methacrylate SM 6200 B-2011 X
Methyl methanesulfonate EPA 625.1 X
Methyl methanesulfonate EPA 8270C X X
Methyl methanesulfonate EPA 8270D X X
Methyl methanesulfonate EPA 8270E X X
Methyl parathion (Parathion,
methyl)EPA 1657 X
Methyl parathion (Parathion,
methyl)EPA 625.1 X
Methyl parathion (Parathion,
methyl)EPA 8141A X X
Methyl parathion (Parathion,
methyl)EPA 8141B X X
Methyl parathion (Parathion,
methyl)EPA 8270C X X
Methyl parathion (Parathion,
methyl)EPA 8270D X X
Methyl parathion (Parathion,
methyl)EPA 8270E X X
Methyl tert-butyl ether EPA 524.2 X
Methyl tert-butyl ether (MTBE)EPA 602 X
Methyl tert-butyl ether (MTBE)EPA 624.1 X
Methyl tert-butyl ether (MTBE)EPA 8021B X X
Methyl tert-butyl ether (MTBE)EPA 8260B X X
Methyl tert-butyl ether (MTBE)EPA 8260C X X
Methyl tert-butyl ether (MTBE)EPA 8260D X X
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Methyl tert-butyl ether (MTBE)EPA TO-15 X
Methyl tert-butyl ether (MTBE)IDNR OA-1 X X
Methyl tert-butyl ether (MTBE)LUFT GCMS X X
Methyl tert-butyl ether (MTBE)MADEP VPH X X
Methyl tert-butyl ether (MTBE)OK DEQ GRO X X
Methyl tert-butyl ether (MTBE)SM 6200 B-2011 X
Methyl-2,4,6-
trinitrophenylnitramine (tetryl)EPA 8330 X X
Methyl-2,4,6-
trinitrophenylnitramine (tetryl)EPA 8330A X X
Methyl-2,4,6-
trinitrophenylnitramine (tetryl)EPA 8330B X X
Methylcyclohexane EPA 624.1 X
Methylcyclohexane EPA 8260B X X
Methylcyclohexane EPA 8260C X X
Methylcyclohexane EPA 8260D X X
Methylcyclohexane EPA TO-15 X
Methylcyclohexane SM 6200 B-2011 X
Methylene bromide EPA 524.2 X
Methylene chloride EPA 524.2 X
Methylene chloride
(Dichloromethane)EPA 624.1 X
Methylene chloride
(Dichloromethane)EPA 8260B X X
Methylene chloride
(Dichloromethane)EPA 8260C X X
Methylene chloride
(Dichloromethane)EPA 8260D X X
Methylene chloride
(Dichloromethane)EPA TO-15 X
Methylene chloride
(Dichloromethane)SM 6200 B-2011 X
Metolachlor EPA 507 X X
Metribuzin EPA 507 X X
Mevinphos EPA 1657 X
Mevinphos EPA 507 X
Mevinphos EPA 8141A X X
Mevinphos EPA 8141B X X
Microextraction of Organics in
Water EPA 3511 X X
Microwave Assisted Acid
Digestion of Aqueous Samples EPA 3015A X
Microwave Assisted Acid
Digestion of Sediments, EPA 3051 X
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Microwave Assisted Acid
Digestion of Sediments, EPA 3051A X
Microwave Assisted Acid
Digestion of Sediments, EPA 3052 X
Microwave Extraction EPA 3546 X
Mirex EPA 8270C X
Mirex EPA 8270D X
Molybdenum EPA 200.7 X X
Molybdenum EPA 200.8 X X
Molybdenum EPA 6010B X X
Molybdenum EPA 6010C X X
Molybdenum EPA 6010D X X
Molybdenum EPA 6020 X X
Molybdenum EPA 6020A X X
Molybdenum EPA 6020B X X
m-Xylene EPA 624.1 X
m-Xylene EPA 8021B X X
m-Xylene EPA 8260B X X
m-Xylene EPA 8260C X X
m-Xylene EPA 8260D X X
m-Xylene EPA TO-15 X
m-Xylene EPA 524.2 X
Naled EPA 1657 X
Naled EPA 8141A X X
Naled EPA 8141B X X
Naphthalene EPA 610 (HPLC) X
Naphthalene EPA 624.1 X
Naphthalene EPA 625.1 X
Naphthalene EPA 625.1 SIM X
Naphthalene EPA 8021B X
Naphthalene EPA 8260B X X
Naphthalene EPA 8260C X X
Naphthalene EPA 8260D X X
Naphthalene EPA 8270C X X
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Naphthalene EPA 8270C SIM X X
Naphthalene EPA 8270D X X
Naphthalene EPA 8270D SIM X X
Naphthalene EPA 8270E X X
Naphthalene EPA 8270E SIM X X
Naphthalene EPA 8310 X X
Naphthalene EPA TO-15 X
Naphthalene MADEP EPH X X
Naphthalene MADEP VPH X X
Naphthalene OK DEQ GRO X X
Naphthalene SM 6200 B-2011 X
Naphthalene EPA 524.2 X
n-Butane EPA TO-15 X
n-Butyl alcohol (1-Butanol, n-
Butanol)EPA 624.1 X
n-Butyl alcohol (1-Butanol, n-
Butanol)EPA 8260B X X
n-Butyl alcohol (1-Butanol, n-
Butanol)EPA 8260C X X
n-Butyl alcohol (1-Butanol, n-
Butanol)EPA 8260D X X
n-Butyl alcohol (1-Butanol, n-
Butanol)SM 6200 B-2011 X
n-Butylbenzene EPA 524.2 X
n-Butylbenzene EPA 624 (extended) X
n-Butylbenzene EPA 624.1 X
n-Butylbenzene EPA 8260B X X
n-Butylbenzene EPA 8260C X X
n-Butylbenzene EPA 8260D X X
n-Butylbenzene EPA TO-15 X
n-Butylbenzene SM 6200 B-2011 X
n-Decane EPA 625.1 X
n-Decane EPA 8270C X X
n-Decane EPA 8270D X X
n-Decane EPA 8270E X X
Neptunium-237
EPA 907 Modified
(ENV-SOP-MTJL-X X X X
n-Heptane EPA 624.1 X
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n-Heptane EPA 8260B X
n-Heptane EPA 8260C X
n-Heptane EPA 8260D X
n-Heptane EPA TO-15 X
n-Hexane EPA 624.1 X
n-Hexane EPA 8260B X X
n-Hexane EPA 8260C X X
n-Hexane EPA 8260D X X
n-Hexane EPA TO-15 X
n-Hexane SM 6200 B-2011 X
n-Hexane Extractable Material
(O&G)EPA 1664A (HEM) X X
n-Hexane Extractable Material
(O&G)
EPA 1664A (SGT-
HEM) X
n-Hexane Extractable Material
(O&G)EPA 1664B X
n-Hexane Extractable Material
(O&G)EPA 9070A X
n-Hexane Extractable Material
(O&G)EPA 9071A X
n-Hexane Extractable Material
(O&G)EPA 9071B X
Nickel EPA 200.7 X X
Nickel EPA 200.8 X X
Nickel EPA 6010B X X
Nickel EPA 6010C X X
Nickel EPA 6010D X X
Nickel EPA 6020 X X
Nickel EPA 6020A X X
Nickel EPA 6020B X X
Nitrate as N EPA 300.0 X X X
Nitrate as N EPA 353.2 X
Nitrate as N EPA 9056 X X
Nitrate as N EPA 9056A X X
Nitrate as N SM 4110 B-2011 X X
Nitrate as N
SM 4500-NO3¯ F-
2011 X X
Nitrate-Nitrite EPA 300.0 X X X
Nitrate-Nitrite EPA 353.2 X X
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Nitrate-Nitrite EPA 9056 X X
Nitrate-Nitrite EPA 9056A X X
Nitrate-Nitrite SM 4110 B-2011 X X
Nitrate-Nitrite
SM 4500-NO3¯ F-
2011 X X
Nitrite as N EPA 300.0 X X X
Nitrite as N EPA 353.2 X
Nitrite as N EPA 9056 X X
Nitrite as N EPA 9056A X X
Nitrite as N SM 4110 B-2011 X X
Nitrite as N
SM 4500-NO3¯ F-
2011 X
Nitrobenzene EPA 625.1 X
Nitrobenzene EPA 8270C X X
Nitrobenzene EPA 8270D X X
Nitrobenzene EPA 8270E X X
Nitrobenzene EPA 8330 X X
Nitrobenzene EPA 8330A X X
Nitrobenzene EPA 8330B X X
Nitrocellulose EPA 353.2 Modified X X
Nitrocellulose
US Army
#ADA067081 X X
Nitroglycerin EPA 8330 X X
Nitroglycerin EPA 8330A X X
Nitroglycerin EPA 8330B X X
Nitroguanidine EPA 8330 X X
Nitroguanidine EPA 8330A X X
Nitroguanidine EPA 8330B X X
n-Nitrosodiethylamine EPA 625.1 X
n-Nitrosodiethylamine EPA 8270C X X
n-Nitrosodiethylamine EPA 8270D X X
n-Nitrosodiethylamine EPA 8270E X X
n-Nitrosodimethylamine EPA 625.1 X
n-Nitrosodimethylamine EPA 625.1 SIM X
n-Nitrosodimethylamine EPA 8270C X X
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n-Nitrosodimethylamine EPA 8270C SIM X X
n-Nitrosodimethylamine EPA 8270D X X
n-Nitrosodimethylamine EPA 8270D SIM X X
n-Nitrosodimethylamine EPA 8270E X X
n-Nitrosodimethylamine EPA 8270E SIM X
n-Nitroso-di-n-butylamine EPA 625.1 X
n-Nitroso-di-n-butylamine EPA 8260B X
n-Nitroso-di-n-butylamine EPA 8260C X
n-Nitroso-di-n-butylamine EPA 8260D X
n-Nitroso-di-n-butylamine EPA 8270C X X
n-Nitroso-di-n-butylamine EPA 8270D X X
n-Nitroso-di-n-butylamine EPA 8270E X X
n-Nitrosodi-n-propylamine EPA 625.1 X
n-Nitrosodi-n-propylamine EPA 8270C X X
n-Nitrosodi-n-propylamine EPA 8270D X X
n-Nitrosodi-n-propylamine EPA 8270E X X
n-Nitrosodiphenylamine EPA 625.1 X
n-Nitrosodiphenylamine EPA 8270C X X
n-Nitrosodiphenylamine EPA 8270D X X
n-Nitrosodiphenylamine EPA 8270E X X
n-Nitrosomethylethylamine EPA 625.1 X
n-Nitrosomethylethylamine EPA 8270C X X
n-Nitrosomethylethylamine EPA 8270D X X
n-Nitrosomethylethylamine EPA 8270E X X
n-Nitrosomorpholine EPA 625.1 X
n-Nitrosomorpholine EPA 8270C X X
n-Nitrosomorpholine EPA 8270D X X
n-Nitrosomorpholine EPA 8270E X X
n-Nitrosopiperidine EPA 625.1 X
n-Nitrosopiperidine EPA 8270C X X
n-Nitrosopiperidine EPA 8270D X X
n-Nitrosopiperidine EPA 8270E X X
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n-Nitrosopyrrolidine EPA 625.1 X
n-Nitrosopyrrolidine EPA 8270C X X
n-Nitrosopyrrolidine EPA 8270D X X
n-Nitrosopyrrolidine EPA 8270E X X
n-Nonane EPA TO-15 X
n-Octadecane EPA 625.1 X
n-Octadecane EPA 8270C X X
n-Octadecane EPA 8270D X X
n-Octadecane EPA 8270E X X
n-Octane EPA 8260B X X
n-Octane EPA 8260C X X
n-Octane EPA 8260D X X
n-Octane SM 6200 B-2011 X
NOEC (ON) Growth
EPA 1000.0 - Fathead
minnow, 7-day X
NOEC Reproduction
EPA 1002.0 -
Ceriodaphnia dubia, X
NOEC Survival
EPA 1000.0 - Fathead
minnow, 7-day X
NOEC Survival
EPA 1002.0 -
Ceriodaphnia dubia, X
NOEC Survival
EPA 2002
Ceriodaphnia dubia X
non-Polar Extractable Material
(TPH)EPA 1664A (HEM) X
n-Pentane EPA TO-15 X
n-Propane
EPA RSK-175
(GC/FID) X
n-Propylbenzene EPA 524.2 X
n-Propylbenzene EPA 624 (extended) X
n-Propylbenzene EPA 624.1 X
n-Propylbenzene EPA 8260B X X
n-Propylbenzene EPA 8260C X X
n-Propylbenzene EPA 8260D X X
n-Propylbenzene EPA TO-15 X
n-Propylbenzene SM 6200 B-2011 X
o,o,o-Triethyl
phosphorothioate EPA 625.1 X
o,o,o-Triethyl
phosphorothioate EPA 8270C X X
o,o,o-Triethyl
phosphorothioate EPA 8270D X X
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o,o,o-Triethyl
phosphorothioate EPA 8270E X X
Octahydro-1,3,5,7-tetranitro-
1,3,5,7-tetrazocine (HMX)EPA 8330 X X
Octahydro-1,3,5,7-tetranitro-
1,3,5,7-tetrazocine (HMX)EPA 8330A X X
Octahydro-1,3,5,7-tetranitro-
1,3,5,7-tetrazocine (HMX)EPA 8330B X X
Odor SM 2150 B X X
Oil & Grease EPA 1664A (HEM) X X
Oil & Grease EPA 1664B X X
Oil & Grease
EPA 1664B (SGT-
HEM) X
Oil & Grease EPA 9070A X
Oil & Grease EPA 9071B X
Oil-Range Organics (ORO)EPA 8015B X X
Oil-Range Organics (ORO)EPA 8015C X X
Oil-Range Organics (ORO)EPA 8015D X X
Organic nitrogen EPA 350.1 X
Organic nitrogen EPA 351.1 X
Organic nitrogen EPA 351.2 X
Organic nitrogen
EPA 351.2 minus
EPA 350.1 X
Organic nitrogen EPA 351.3 X
Organic nitrogen EPA 351.4 X
Organic nitrogen
SM 4500-Norg D-
2011 minus SM 4500- X
Organic nitrogen
TKN minus
AMMONIA X
Orthophosphate EPA 9056A X
Orthophosphate as P EPA 300.0 X
Orthophosphate as P EPA 365.2 X X
Orthophosphate as P EPA 9056 X
Orthophosphate as P EPA 9056A X
Orthophosphate as P SM 4500-P E-2011 X X
Oxidation Reduction Potential SM 2580 B X
Oxygen ASTM D1946-90 X
Oxygen, dissolved SM 4500-O C-2011 X
Oxygen, dissolved SM 4500-O G-2011 X
o-Xylene EPA 602 X
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o-Xylene EPA 624.1 X
o-Xylene EPA 8021B X X
o-Xylene EPA 8260B X X
o-Xylene EPA 8260C X X
o-Xylene EPA 8260D X X
o-Xylene EPA TO-15 X
o-Xylene IDNR OA-1 X
o-Xylene MADEP VPH X X
o-Xylene OK DEQ GRO X
o-Xylene SM 6200 B-2011 X
o-Xylene EPA 524.2 X
Parathion, ethyl EPA 1657 X
Parathion, ethyl EPA 625.1 X
Parathion, ethyl EPA 8141A X X
Parathion, ethyl EPA 8141B X X
Parathion, ethyl EPA 8270C X X
Parathion, ethyl EPA 8270D X X
Parathion, ethyl EPA 8270E X X
p-Dimethylaminoazobenzene EPA 625.1 X
p-Dimethylaminoazobenzene EPA 8270C X X
p-Dimethylaminoazobenzene EPA 8270D X X
p-Dimethylaminoazobenzene EPA 8270E X X
Pentachlorobenzene EPA 625.1 X
Pentachlorobenzene EPA 8270C X X
Pentachlorobenzene EPA 8270D X X
Pentachlorobenzene EPA 8270E X X
Pentachloroethane EPA 624.1 X
Pentachloroethane EPA 625 (extended) X
Pentachloroethane EPA 625.1 X
Pentachloroethane EPA 8260B X X
Pentachloroethane EPA 8260C X X
Pentachloroethane EPA 8260D X X
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Pentachloroethane EPA 8270C X X
Pentachloroethane EPA 8270D X X
Pentachloroethane EPA 8270E X X
Pentachloroethane SM 6200 B-2011 X
Pentachloronitrobenzene EPA 625.1 X
Pentachloronitrobenzene EPA 8270C X X
Pentachloronitrobenzene EPA 8270D X X
Pentachloronitrobenzene EPA 8270E X X
Pentachlorophenol EPA 625.1 X
Pentachlorophenol EPA 8151A X X
Pentachlorophenol EPA 8270C X X
Pentachlorophenol EPA 8270D X X
Pentachlorophenol EPA 8270E X X
Pentaerythritoltetranitrate EPA 8330 X X
Pentaerythritoltetranitrate EPA 8330A X X
Pentaerythritoltetranitrate EPA 8330B X X
Percent ash ASTM D482 X
Perchlorate EPA 314.0 X X X
Petroleum Organics CT ETPH X
Petroleum Organics FL PRO X
Petroleum Organics LUFT GC X
Petroleum Organics NWTPH-HCID X X
Petroleum Organics Texas 1006 X X
Petroleum Volatile Organic
Compounds (PVOC)WI(95) GRO X X
pH EPA 150.1 X X
pH EPA 9040B X X
pH EPA 9040C X X
pH EPA 9045C X X
pH EPA 9045D X X
pH SM 4500-H+ B-2011 X X
Phenacetin EPA 625.1 X
Phenacetin EPA 8270C X X
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Phenacetin EPA 8270D X X
Phenacetin EPA 8270E X X
Phenanthrene EPA 610 (HPLC) X
Phenanthrene EPA 625.1 X
Phenanthrene EPA 625.1 SIM X
Phenanthrene EPA 8270C X X
Phenanthrene EPA 8270C SIM X X
Phenanthrene EPA 8270D X X
Phenanthrene EPA 8270D SIM X X
Phenanthrene EPA 8270E X X
Phenanthrene EPA 8270E SIM X X
Phenanthrene EPA 8310 X X
Phenanthrene MADEP EPH X X
Phenol EPA 420.4 X
Phenol EPA 625.1 X
Phenol EPA 8270C X X
Phenol EPA 8270D X X
Phenol EPA 8270E X X
Phenols EPA 420.1 X
Phenols EPA 420.4 X
Phenols SM 3500 D-2005 X
Phorate EPA 1657 X
Phorate EPA 625.1 X
Phorate EPA 8141A X X
Phorate EPA 8141B X X
Phorate EPA 8270C X X
Phorate EPA 8270D X X
Phorate EPA 8270E X X
Phosmet (Imidan)EPA 8141A X
Phosmet (Imidan)EPA 8141B X
Phosphorus EPA 200.7 X X
Phosphorus EPA 6010B X
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Phosphorus EPA 6010C X X
Phosphorus EPA 6010D X
Photon Emitters DOE 4.5.2.3 X
Photon Emitters EPA 901.1 X
Photon Emitters HASL 300 Ga-01-R X
Phthalic anhydride EPA 625.1 X
Phthalic anhydride EPA 8270C X X
Phthalic anhydride EPA 8270D X X
Phthalic anhydride EPA 8270E X
Pimephales promelas EPA 1000 X
Pimephales promelas EPA 2000 X
Plutonium-238
EPA 907 Modified
(ENV-SOP-MTJL-X X X X
Plutonium-239/240
EPA 907 Modified
(ENV-SOP-MTJL-X X X X
Plutonium-241
EPA 907 Modified
(ENV-SOP-MTJL-X X X X
Polonium-210
DOE EML Po-02-
RC X
Polonium-210 HASL 300 Po-02-RC X X X X
Potassium EPA 200.7 X X
Potassium EPA 200.8 X
Potassium EPA 6010B X X
Potassium EPA 6010C X X
Potassium EPA 6010D X X
Potassium EPA 6020 X X
Potassium EPA 6020A X X
Potassium EPA 6020B X X
Preparation/Extraction EPA 200.2 X
Pronamide (Kerb)EPA 625.1 X
Pronamide (Kerb)EPA 8270C X X
Pronamide (Kerb)EPA 8270D X X
Pronamide (Kerb)EPA 8270E X X
Propane
EPA RSK-175
(GC/FID)X X
Propionitrile (Ethyl cyanide)EPA 624.1 X
Propionitrile (Ethyl cyanide)EPA 8260B X X
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Propionitrile (Ethyl cyanide)EPA 8260C X X
Propionitrile (Ethyl cyanide)EPA 8260D X X
Propionitrile (Ethyl cyanide)SM 6200 B-2011 X
Propylene EPA TO-15 X
Propylene Glycol EPA 8015B X X
Propylene Glycol EPA 8015C X
Propylene Glycol
EPA 8015C
(extended) X X
Propylene Glycol EPA 8015D X X
Purge and trap for aqueous
phase samples EPA 5030 X
Purge and trap for aqueous
phase samples EPA 5030A X
Purge and trap for aqueous
phase samples EPA 5030B X
Purge and trap for aqueous
phase samples EPA 5030C X
p-Xylene EPA 624.1 X
p-Xylene EPA 8021B X X
p-Xylene EPA 8260B X X
p-Xylene EPA 8260C X X
p-Xylene EPA 8260D X X
p-Xylene EPA TO-15 X
Pyrene EPA 610 (HPLC) X
Pyrene EPA 625.1 X
Pyrene EPA 625.1 SIM X
Pyrene EPA 8270C X X
Pyrene EPA 8270C SIM X X
Pyrene EPA 8270D X X
Pyrene EPA 8270D SIM X X
Pyrene EPA 8270E X X
Pyrene EPA 8270E SIM X X
Pyrene EPA 8310 X X
Pyrene MADEP EPH X X
Pyridine EPA 625.1 X
Pyridine EPA 8270C X X
Pyridine EPA 8270D X X
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Pyridine EPA 8270E X X
Quinoline EPA 625.1 X
Quinoline EPA 8270C X X
Quinoline EPA 8270D X X
Quinoline EPA 8270E X X
Radium-226 EPA 903.0 X
Radium-226 EPA 903.1 X X
Radium-226 EPA 9315 X
Radium-226 HASL 300 Ra-04-RC X
Radium-226
SM 7500 Ra B
Modified X X X X
Radium-226 SM 7500-Ra B X X
Radium-226 SM 7500-Ra B (GPC) X X
Radium-228 EPA 904 X
Radium-228 EPA 904.0 X X X
Radium-228 EPA 9320 X X
Radon SM 7500-Rn B X X
RDX (hexahydro-1,3,5-trinitro-
1,3,5-triazine)EPA 8330 X X
RDX (hexahydro-1,3,5-trinitro-
1,3,5-triazine)EPA 8330A X X
RDX (hexahydro-1,3,5-trinitro-
1,3,5-triazine)EPA 8330B X X
Reactive Cyanide EPA 9010C X
Reactive Cyanide EPA 9014 X
Reactive sulfide EPA 9034 X X
Residue-filterable (TDS)SM 2540 C-2011 X
Residue-nonfilterable (TSS)SM 2540 D-2011 X
Residue-nonfilterable (TSS)USGS I-3765-85 X
Residue-settleable SM 2540 F-2011 X
Residue-total SM 2540 B-2011 X
Residue-volatile EPA 160.4 X
Residue-volatile SM 2540 E-2011 X
Ronnel EPA 1657 X
Ronnel EPA 8141A X X
Ronnel EPA 8141B X X
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Safrole EPA 625.1 X
Safrole EPA 8270C X X
Safrole EPA 8270D X X
Safrole EPA 8270E X X
Salinity SM 2520 B-2011 X
sec-Butylbenzene EPA 524.2 X
sec-Butylbenzene EPA 624 (extended) X
sec-Butylbenzene EPA 624.1 X
sec-Butylbenzene EPA 8260B X X
sec-Butylbenzene EPA 8260C X X
sec-Butylbenzene EPA 8260D X X
sec-Butylbenzene EPA TO-15 X
sec-Butylbenzene SM 6200 B-2011 X
Selenium EPA 200.7 X X
Selenium EPA 200.8 X X
Selenium EPA 6010B X X
Selenium EPA 6010C X X
Selenium EPA 6010D X X
Selenium EPA 6020 X X
Selenium EPA 6020A X X
Selenium EPA 6020B X X
Separatory Funnel Liquid-liquid
extraction EPA 3510C X
Silica as SiO2 EPA 200.7 X X
Silica as SiO2 EPA 6010B X
Silica as SiO2 EPA 6010C X
Silica as SiO2 EPA 6010D X
Silica Gel Clean-up EPA 3630C X X
Silica Gel Treated n-hexane
Extractable Material (SGT-EPA 1664A (HEM) X X
Silica Gel Treated n-hexane
Extractable Material (SGT-EPA 1664B X
Silica Gel Treated n-hexane
Extractable Material (SGT-EPA 9071B X
Silica-dissolved EPA 200.7 X
Silicon EPA 200.7 X
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Silicon EPA 6010B X
Silicon EPA 6010C X
Silicon EPA 6010D X
Silver EPA 200.7 X X
Silver EPA 200.8 X X
Silver EPA 6010B X X
Silver EPA 6010C X X
Silver EPA 6010D X X
Silver EPA 6020 X X
Silver EPA 6020A X X
Silver EPA 6020B X X
Silvex (2,4,5-TP)EPA 8151A X X
Silvex (2,4,5-TP)SM 6640 B-2001 X
Silvex (2,4,5-TP)SM 6640 B-2006 X
Simazine EPA 507 X X
Simazine EPA 8141B X
Sodium EPA 200.7 X X
Sodium EPA 200.8 X
Sodium EPA 6010B X X
Sodium EPA 6010C X X
Sodium EPA 6010D X X
Sodium EPA 6020 X X
Sodium EPA 6020A X X
Sodium EPA 6020B X X
Solid-Phase Extraction (SPE)EPA 3535A X
Soxhlet Extraction EPA 3540C X
Specific Gravity (Relative
Density)SM 2710 F-2011 X
Specific Gravity of Sludge SM 2710 F-2011 X
Stirophos EPA 1657 X
Stirophos EPA 8141A X X
Stirophos EPA 8141B X X
Strontium EPA 200.7 X X
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Strontium EPA 200.8 X
Strontium EPA 6010B X X
Strontium EPA 6010C X X
Strontium EPA 6010D X X
Strontium EPA 6020 X X
Strontium EPA 6020A X X
Strontium EPA 6020B X X
Strontium-89 DOE EML Sr-01-RC X
Strontium-89 EPA 905.0 X X
Strontium-89
HASL 300 Sr-01-RC
(GPC) X
Strontium-89, 90 EPA 905 X X
Strontium-90 DOE EML Sr-02-RC X
Strontium-90 EPA 905 X X
Strontium-90 EPA 905.0 X X
Strontium-90
HASL 300 Sr-02-RC
(GPC) X
Styrene EPA 624.1 X
Styrene EPA 8260B X X
Styrene EPA 8260C X X
Styrene EPA 8260D X X
Styrene EPA TO-15 X
Styrene SM 6200 B-2011 X
Styrene EPA 524.2 X
Sulfate EPA 300.0 X X X
Sulfate EPA 9056 X X
Sulfate EPA 9056A X X
Sulfate SM 4110 B-2011 X X
Sulfide EPA 9030A X
Sulfide EPA 9030B X X
Sulfide EPA 9034 X X
Sulfide SM 4500-S2¯ D-2011 X
Sulfite-SO3
SM 4500-SO3¯ B-
2011 X
Sulfotepp EPA 1657 X
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Sulfotepp EPA 625.1 X
Sulfotepp EPA 8141A X X
Sulfotepp EPA 8141B X X
Sulfotepp EPA 8270C X X
Sulfotepp EPA 8270D X X
Sulfotepp EPA 8270E X X
Sulfur EPA 6010B X
Sulfur EPA 6010C X
Sulfur EPA 6010D X
Sulfur Clean-Up EPA 3660B X X
Sulfuric acid/permanganate
clean-up EPA 3665A X X
Surfactants - MBAS SM 5540 C-2011 X X
Synthetic Precipitation
Leaching Procedure EPA 1312 X X
T-amylmethylether (TAME)EPA 624.1 X
T-amylmethylether (TAME)EPA 8260B X X
T-amylmethylether (TAME)EPA 8260C X X
T-amylmethylether (TAME)EPA 8260D X X
T-amylmethylether (TAME)SM 6200 B-2011 X
Technetium-99 DOE EML Tc-02-RC X X X X
Temperature, deg. C SM 2550 B-2000 X X
Terbufos EPA 8141A X
Terbufos EPA 8141B X X
tert-Amyl-ethyl ether (TAEE)
EPA 8260B
(extended) X X
tert-Amyl-ethyl ether (TAEE)EPA 8260C X X
tert-Amyl-ethyl ether (TAEE)EPA 8260D X
tert-Amyl-ethyl ether (TAEE)EPA TO-15 X
tert-Amyl-ethyl ether (TAEE)SM 6200 B-2011 X
tert-Butyl alcohol EPA 602 X
tert-Butyl alcohol EPA 624.1 X
tert-Butyl alcohol EPA 8260B X X
tert-Butyl alcohol EPA 8260C X X
tert-Butyl alcohol EPA 8260D X X
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tert-Butyl alcohol EPA TO-15 X
tert-Butyl alcohol SM 6200 B-2011 X
tert-Butyl formate EPA 624.1 X
tert-Butyl formate EPA 8260B X X
tert-Butyl formate EPA 8260C X X
tert-Butyl formate EPA 8260D X
tert-Butyl formate SM 6200 B-2011 X
tert-Butylbenzene EPA 524.2 X
tert-Butylbenzene EPA 624 (extended) X
tert-Butylbenzene EPA 624.1 X
tert-Butylbenzene EPA 8260B X X
tert-Butylbenzene EPA 8260C X X
tert-Butylbenzene EPA 8260D X X
tert-Butylbenzene EPA TO-15 X
tert-Butylbenzene SM 6200 B-2011 X
Tetrachloroethene EPA 524.2 X
Tetrachloroethylene
(Perchloroethylene)EPA 624.1 X
Tetrachloroethylene
(Perchloroethylene)EPA 8260B X X
Tetrachloroethylene
(Perchloroethylene)EPA 8260C X X
Tetrachloroethylene
(Perchloroethylene)EPA 8260D X X
Tetrachloroethylene
(Perchloroethylene)EPA TO-15 X
Tetrachloroethylene
(Perchloroethylene)
EPA TO-15 GC/MS
SIM X
Tetrachloroethylene
(Perchloroethylene)SM 6200 B-2011 X
Tetrachlorovinphos EPA 8141B X
Tetraethyl pyrophosphate
(TEPP)EPA 1657 X
Tetraethyl pyrophosphate
(TEPP)EPA 8141A X X
Tetraethyl pyrophosphate
(TEPP)EPA 8141B X X
Tetrahydrofuran EPA 524.2 X
Tetrahydrofuran (THF)EPA 624.1 X
Tetrahydrofuran (THF)EPA 8260B X X
Tetrahydrofuran (THF)EPA 8260C X X
Tetrahydrofuran (THF)EPA 8260D X X
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Tetrahydrofuran (THF)EPA TO-15 X
Tetrahydrofuran (THF)SM 6200 B-2011 X
Thallium EPA 200.7 X X
Thallium EPA 200.8 X X
Thallium EPA 6010B X X
Thallium EPA 6010C X X
Thallium EPA 6010D X X
Thallium EPA 6020 X X
Thallium EPA 6020A X X
Thallium EPA 6020B X X
Thionazin (Zinophos)EPA 625.1 X
Thionazin (Zinophos)EPA 8270C X X
Thionazin (Zinophos)EPA 8270D X X
Thionazin (Zinophos)EPA 8270E X X
Thorium EPA 200.8 X
Thorium EPA 6020 X X
Thorium EPA 6020A X X
Thorium EPA 6020B X X
Thorium-228
LANL ER200
Modified X X X X
Thorium-230
LANL ER200
Modified X X X X
Thorium-232
LANL ER200
Modified X X X X
Tin EPA 200.7 X X
Tin EPA 200.8 X X
Tin EPA 6010B X X
Tin EPA 6010C X X
Tin EPA 6010D X X
Tin EPA 6020 X X
Tin EPA 6020A X X
Tin EPA 6020B X X
Titanium EPA 200.7 X X
Titanium EPA 200.8 X
Titanium EPA 6010B X X
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Titanium EPA 6010C X X
Titanium EPA 6010D X X
Titanium EPA 6020 X X
Titanium EPA 6020A X X
Titanium EPA 6020B X X
Tokuthion (Prothiophos)EPA 1657 X
Tokuthion (Prothiophos)EPA 8141A X X
Tokuthion (Prothiophos)EPA 8141B X X
Toluene EPA 602 X
Toluene EPA 624.1 X
Toluene EPA 8021B X X
Toluene EPA 8260B X X
Toluene EPA 8260C X X
Toluene EPA 8260D X X
Toluene EPA TO-15 X
Toluene IDNR OA-1 X X
Toluene LUFT GCMS X X
Toluene MADEP VPH X X
Toluene OK DEQ GRO X X
Toluene SM 6200 B-2011 X
Toluene EPA 524.2 X
Total coliforms SM 9223 B-2004 X X
Total Cyanide EPA 335.4 X
Total Cyanide EPA 9010B X
Total Cyanide EPA 9010C X X
Total Cyanide EPA 9012A X X
Total Cyanide EPA 9012B X X
Total Cyanide EPA 9014 X X
Total Cyanide
SM 4500-CN¯ B-
2011 X
Total Cyanide
SM 4500-CN¯ C-
2011 X
Total Cyanide
SM 4500-CN¯ E-
2011 X
Total Dissolved Solids SM 2540 C-2011 X
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Total Haloacetic Acids EPA 552.2 X
Total hardness as CaCO3 EPA 130.1 X
Total hardness as CaCO3 EPA 200.7 X
Total hardness as CaCO3 EPA 200.8 X
Total hardness as CaCO3 EPA 6010B X
Total hardness as CaCO3 EPA 6010C X X
Total hardness as CaCO3 EPA 6010D X
Total hardness as CaCO3 SM 2340 B-2011 X
Total hardness as CaCO3 SM 2340 C-2011 X
Total Nitrate+Nitrite EPA 300.0 X
Total Organic Carbon ASTM F1647-02A X
Total Organic Carbon EPA 9060 X
Total Organic Carbon EPA 9060A X
Total Organic Carbon SM 5310 B-2011 X X
Total Organic Carbon SM 5310 C-2011 X
Total Organic Carbon USDA LOI X
Total Organic Carbon
Walkley-Black
Method X
Total Organic Halides (TOX)EPA 9020B X
Total Organic Halides (TOX)EPA 9076 X
Total Organic Halides (TOX)SM 5320 B-2010 X
Total Petroleum Hydrocarbons
(>C12-C28)TNRCC 1005 X X
Total Petroleum Hydrocarbons
(>C28-C35)TNRCC 1005 X X
Total Petroleum Hydrocarbons
(Aviation Gasoline Range)EPA 8015B X X
Total Petroleum Hydrocarbons
(Aviation Gasoline Range)EPA 8015C X X
Total Petroleum Hydrocarbons
(Aviation Gasoline Range)EPA 8015D X X
Total Petroleum Hydrocarbons
(C6-C12)TNRCC 1005 X X
Total Petroleum Hydrocarbons
(C6-C35)TNRCC 1005 X X
Total Petroleum Hydrocarbons
(C8-C40)EPA 8015B X X
Total Petroleum Hydrocarbons
(C8-C40)EPA 8015C X X
Total Petroleum Hydrocarbons
(C8-C40)EPA 8015D X X
Total Petroleum Hydrocarbons
(Gasoline Range)TN GRO X
Total Petroleum Hydrocarbons
(Jet Fuel Range)EPA 8015B X X
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Total Petroleum Hydrocarbons
(Jet Fuel Range)EPA 8015C X X
Total Petroleum Hydrocarbons
(Jet Fuel Range)EPA 8015D X X
Total Petroleum Hydrocarbons
(Oil Range)EPA 8015B X X
Total Petroleum Hydrocarbons
(Oil Range)EPA 8015C X X
Total Petroleum Hydrocarbons
(Oil Range)EPA 8015D X X
Total Petroleum Hydrocarbons
(TPH)EPA 8015B X X
Total Petroleum Hydrocarbons
(TPH)EPA 8015C X X
Total Petroleum Hydrocarbons
(TPH)EPA 8015D X X
Total Petroleum Hydrocarbons
(TPH)FL PRO X
Total Petroleum Hydrocarbons
(TPH)TNRCC 1005 X X
Total Phenolics EPA 420.1 X X
Total Phenolics EPA 420.2 X
Total Phenolics EPA 420.4 X
Total Phenolics EPA 9066 X X
Total Phenolics SM 5530 D X
Total Phosphorus EPA 365.1 X
Total Phosphorus EPA 365.4 X X
Total Phosphorus EPA 6010B X
Total Phosphorus EPA 6010C X
Total Phosphorus EPA 6010D X
Total Phosphorus SM 4500-P B 5-2011 X
Total Phosphorus SM 4500-P H-2011 X
Total Purgeable Hydrocarbons
(C5-C12)MADEP VPH X X
Total radium EPA 903.0 (GPC) X X
Total radium EPA 9315 X X
Total radium SM 7500-Ra B (GPC) X
Total radium
SM 7500-Ra B
(GPC)-2001 X
Total residual chlorine SM 4500-Cl G-2011 X
Total Suspended Solids SM 2540 D-2011 X
Total Trihalomethanes EPA 524.2 X
Total, Fixed, and Volatile
Residue SM 2540 G X X
Total, Fixed, and Volatile
Residue SM 2540 G-2011 X
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Toxaphene (Chlorinated
camphene)EPA 608.3 X
Toxaphene (Chlorinated
camphene)EPA 8081A X X
Toxaphene (Chlorinated
camphene)EPA 8081B X X
Toxicity Characteristic Leaching
Procedure (TCLP)EPA 1311 X X
trans-1,2-Dichloroethene EPA 524.2 X
trans-1,2-Dichloroethylene EPA 624.1 X
trans-1,2-Dichloroethylene EPA 8260B X X
trans-1,2-Dichloroethylene EPA 8260C X X
trans-1,2-Dichloroethylene EPA 8260D X X
trans-1,2-Dichloroethylene EPA TO-15 X
trans-1,2-Dichloroethylene SM 6200 B-2011 X
trans-1,3-Dichloropropene EPA TO-15 X
trans-1,3-Dichloropropene EPA 524.2 X
trans-1,3-Dichloropropylene EPA 624.1 X
trans-1,3-Dichloropropylene EPA 8260B X X
trans-1,3-Dichloropropylene EPA 8260C X X
trans-1,3-Dichloropropylene EPA 8260D X X
trans-1,3-Dichloropropylene EPA TO-15 X
trans-1,3-Dichloropropylene
EPA TO-15 GC/MS
SIM X
trans-1,3-Dichloropropylene SM 6200 B-2011 X
trans-1,4-Dichloro-2-butene EPA 624.1 X
trans-1,4-Dichloro-2-butene EPA 8260B X X
trans-1,4-Dichloro-2-butene EPA 8260C X X
trans-1,4-Dichloro-2-butene EPA 8260D X X
trans-1,4-Dichloro-2-butene SM 6200 B-2011 X
trans-Diallate EPA 8270C X
trans-Isosafrole EPA 8270C X
Trichloroacetic acid EPA 552.2 X
Trichloroethene EPA 524.2 X
Trichloroethene
(Trichloroethylene)EPA 624.1 X
Trichloroethene
(Trichloroethylene)EPA 8260B X X
Trichloroethene
(Trichloroethylene)EPA 8260C X X
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Trichloroethene
(Trichloroethylene)EPA 8260D X X
Trichloroethene
(Trichloroethylene)EPA TO-15 X
Trichloroethene
(Trichloroethylene)SM 6200 B-2011 X
Trichlorofluoromethane EPA 524.2 X
Trichlorofluoromethane
(Fluorotrichloromethane, Freon EPA 624.1 X
Trichlorofluoromethane
(Fluorotrichloromethane, Freon EPA 8260B X X
Trichlorofluoromethane
(Fluorotrichloromethane, Freon EPA 8260C X X
Trichlorofluoromethane
(Fluorotrichloromethane, Freon EPA 8260D X X
Trichlorofluoromethane
(Fluorotrichloromethane, Freon EPA TO-15 X
Trichlorofluoromethane
(Fluorotrichloromethane, Freon SM 6200 B-2011 X
Trichloronate EPA 1657 X
Trichloronate EPA 8141A X X
Trichloronate EPA 8141B X X
Triclosan EPA 8270C X
Triclosan EPA 8270D X
Triclosan EPA 8270E X
tris-(2,3-Dibromopropyl)
phosphate (tris-BP)EPA 8270C X X
tris-(2,3-Dibromopropyl)
phosphate (tris-BP)EPA 8270D X X
tris-(2,3-Dibromopropyl)
phosphate (tris-BP)EPA 8270E X
Tritium EPA 906 X X
Tritium EPA 906 (Modified) X
Tritium EPA 906.0 X
Turbidity EPA 180.1 X X
Turbidity SM 2130 B-2011 X X
Ultrasonic Extraction EPA 3550B X
Ultrasonic Extraction EPA 3550C X
Uranium ASTM D5174-02 X X
Uranium
ASTM D5174-07
Modified (ENV-SOP-X X X
Uranium ASTM D5174-97 X X
Uranium DOE EML U-02-RC X
Uranium EPA 200.8 X X
Uranium EPA 6020 X X
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Uranium EPA 6020A X X
Uranium EPA 6020B X X
Uranium HASL 300 U-02-RC X
Uranium-234
ASTM D3972-09
Modified (ENV-SOP-X X X
Uranium-234 DOE EML U-02-RC X
Uranium-234 HASL 300 U-02-RC X
Uranium-235
ASTM D3972-09
Modified (ENV-SOP-X X X
Uranium-235 DOE EML U-02-RC X
Uranium-235 HASL 300 U-02-RC X
Uranium-238
ASTM D3972-09
Modified (ENV-SOP-X X X
Uranium-238 DOE EML U-02-RC X
Uranium-238 HASL 300 U-02-RC X
UV254 SM 5910 B-2011 X
Vanadium EPA 200.7 X X
Vanadium EPA 200.8 X X
Vanadium EPA 6010B X X
Vanadium EPA 6010C X X
Vanadium EPA 6010D X X
Vanadium EPA 6020 X X
Vanadium EPA 6020A X X
Vanadium EPA 6020B X X
Vinyl acetate EPA 624.1 X
Vinyl acetate EPA 8260B X X
Vinyl acetate EPA 8260C X X
Vinyl acetate EPA 8260D X X
Vinyl acetate EPA TO-15 X
Vinyl acetate SM 6200 B-2011 X
Vinyl bromide (Bromoethane)EPA 624.1 X
Vinyl bromide (Bromoethane)EPA 8260 X
Vinyl bromide (Bromoethane)EPA 8260B X X
Vinyl bromide (Bromoethane)EPA 8260C X X
Vinyl bromide (Bromoethane)EPA 8260D X X
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Vinyl bromide (Bromoethane)EPA TO-15 X
Vinyl bromide (Bromoethane)SM 6200 B-2011 X
Vinyl chloride EPA 624.1 X
Vinyl chloride EPA 8260B X X
Vinyl chloride EPA 8260C X X
Vinyl chloride EPA 8260D X X
Vinyl chloride EPA TO-15 X
Vinyl chloride
EPA TO-15 GC/MS
SIM X
Vinyl chloride SM 6200 B-2011 X
Vinyl chloride EPA 524.2 X
Volatile Petroleum
Hydrocarbons (VPH)
MADEP VPH
(modified) X
Volatile suspended solids SM 2540 E-2011 X
VPH Aliphatic >C6-C8 MADEP VPH X X
VPH Aliphatic >C8-C10 MADEP VPH X X
VPH Aliphatic C5-C8 MADEP VPH X X
VPH Aliphatic C5-C8
Unadjusted MADEP VPH X X
VPH Aliphatic C9-C12 MADEP VPH X X
VPH Aliphatic C9-C12
Unadjusted MADEP VPH X X
VPH Aromatic >C8-C10 MADEP VPH X X
VPH Aromatic C9-C10 MADEP EPH X
VPH Aromatic C9-C10 MADEP VPH X X
Waste Dilution EPA 3580A X X
Waste Dilution EPA 3585 X
Weak Acid Dissociable Cyanide SM 4500-CN I X
Xylene (mixed isomers, total)EPA 524.2 X
Xylene (total)EPA 602 X
Xylene (total)EPA 624.1 X
Xylene (total)EPA 8021B X X
Xylene (total)EPA 8260B X X
Xylene (total)EPA 8260C X X
Xylene (total)EPA 8260D X X
Xylene (total)EPA TO-15 X
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Xylene (total)IDNR OA-1 X X
Xylene (total)LUFT GCMS X X
Xylene (total)MADEP VPH X
Xylene (total)OK DEQ GRO X X
Xylene (total)SM 6200 B-2011 X
Zinc EPA 200.7 X X
Zinc EPA 200.8 X X
Zinc EPA 6010B X X
Zinc EPA 6010C X X
Zinc EPA 6010D X X
Zinc EPA 6020 X X
Zinc EPA 6020A X X
Zinc EPA 6020B X X
Zinc-65 DOE 4.5.2.3 X
Zinc-65 EPA 901.1 X
Zinc-65 HASL 300 Ga-01-R X
1 = Laboratory does not hold TNI Accreditation for this test method.
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7.3 Appendix C: Glossary
This glossary provides common terms and definitions used by PAS. It is not intended to be a
complete list of all terms and definitions used. The definitions have been compiled mostly from
the TNI Standard and DoD QSM. Although this information has been reproduced with care, errors
cannot be entirely excluded. Definitions for the same term also vary between sources. When the
meaning of a term used in a PAS document is different from this glossary or when the glossary does
not include the term, the term and definition is included or defined in context in the laboratory
document.
Term Definition
3P Program The continuous improvement program used by PAS that focuses on Process, Productivity, and
Performance.
Absence Inability to perform assigned duties due to lack of physical presence and connectivity.
Acceptance Criteria TNI- Specified limits placed on characteristics of an item, process, or service defined in requirement
documents.
Accreditation TNI- The process by which an agency or organization evaluates and recognizes a laboratory as meeting
certain predetermined qualifications or standards, thereby accrediting the laboratory.
DoD- Refers to accreditation in accordance with the DoD ELAP.
Accreditation Body (AB)TNI- The organization having responsibility and accountability for environmental laboratory
accreditation, and which grants accreditation under this program.
DoD- Entities recognized in accordance with the DoD-ELAP that are required to operate in accordance
with ISO/IEC 17011, Conformity assessment: General requirements for accreditation bodies accrediting conformity
assessment bodies. The AB must be a signatory, in good standing, to the International Laboratory
Accreditation Cooperation (ILAC) mutual recognition arrangement (MRA) that verifies, by evaluation
and peer assessment, that its signatory members are in full compliance with ISO/IEC 17011 and that its
accredited laboratories comply with ISO/IEC 17025.
Accuracy TNI- The degree of agreement between an observed value and an accepted reference value. Accuracy
includes a combination of random error (precision) and systematic error (bias) components that are due
to sampling and analytical operations; a data quality indicator.
Activity, Absolute TNI- Rate of nuclear decay occurring in a body of material, equal to the number of nuclear
disintegrations per unit time. NOTE: Activity (absolute) may be expressed in becquerels (Bq), curies (Ci),
or disintegrations per minute (dpm), and multiples or submultiples of these units.
Activity, Areic TNI- Quotient of the activity of a body of material and its associated area.
Activity, Massic TNI- Quotient of the activity of a body of material and its mass; also called specific activity.
Activity, Volumic TNI- Quotient of the activity of a body of material and its volume; also called activity concentration.
NOTE: In this module [TNI Volume 1, Module 6], unless otherwise stated, references to activity shall
include absolute activity, areic activity, massic activity, and volumic activity.
Activity Reference Date TNI- The date (and time, as appropriate to the half-life of the radionuclide) to which a reported activity
result is calculated. NOTE: The sample collection date is most frequently used as the Activity Reference
Date for environmental measurements, but different programs may specify other points in time for
correction of results for decay and ingrowth.
Aliquot DoD- A discrete, measured, representative portion of a sample taken for analysis.
American Society for
Testing and Materials
(ASTM)
An international standards organization that develops and publishes voluntary consensus standards for a
wide range of materials, products, systems, and services.
Analysis DoD- A combination of sample preparation and instrument determination.
Analysis Code (Acode)All the set parameters of a test, such as Analytes, Method, Detection Limits and Price.
Analysis Sequence A compilation of all samples, standards and quality control samples run during a specific amount of time
on a particular instrument in the order they are analyzed.
Analyst TNI- The designated individual who performs the “hands-on” analytical methods and associated
techniques and who is the one responsible for applying required laboratory practices and other pertinent
quality controls to meet the required level of quality.
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Analyte TNI- A substance, organism, physical parameter, property, or chemical constituent(s) for which an
environmental sample is being analyzed.
DoD- The specific chemicals or components for which a sample is analyzed; it may be a group of
chemicals that belong to the same chemical family and are analyzed together.
Analytical Method DoD- A formal process that identifies and quantifies the chemical components of interest (target
analytes) in a sample.
Analytical Uncertainty TNI- A subset of Measurement Uncertainty that includes all laboratory activities performed as part of the
analysis.
Aliquot DoD- A discrete, measured, representative portion of a sample taken for analysis.
Annual (or Annually)Defined by PAS as every 12 months ± 30 days.
Assessment TNI - The evaluation process used to measure or establish the performance, effectiveness, and
conformance of an organization and/or its system to defined criteria (to the standards and requirements
of laboratory accreditation).
DoD- An all-inclusive term used to denote any of the following: audit, performance evaluation, peer
review, inspection, or surveillance conducted on-site.
Atomic Absorption
Spectrometer
Instrument used to measure concentration in metals samples.
Atomization A process in which a sample is converted to free atoms.
Audit TNI- A systematic and independent examination of facilities, equipment, personnel, training, procedures,
record-keeping, data validation, data management, and reporting aspects of a system to determine
whether QA/QC and technical activities are being conducted as planned and whether these activities will
effectively achieve quality objectives.
Batch TNI- Environmental samples that are prepared and/or analyzed together with the same process and
personnel, using the same lot(s) of reagents. A preparation batch is composed of one to 20
environmental samples of the same quality systems matrix, meeting the above-mentioned criteria and
with a maximum time between the start of processing of the first and last sample in the batch to be 24
hours or the timeframe specified by the regulatory program. An analytical batch is composed of
prepared environmental samples (extracts, digestates or concentrates) which are analyzed together as a
group. An analytical batch can include prepared samples originating from various quality system matrices
and can exceed 20 samples.
Batch, Radiation
Measurements (RMB)
TNI- An RMB is composed of 1 to 20 environmental samples that are counted directly without
preliminary physical or chemical processing that affects the outcome of the test (e.g., non-destructive
gamma spectrometry, alpha/beta counting of air filters, or swipes on gas proportional detectors). The
samples in an RMB share similar physical and chemical parameter, and analytical configurations (e.g.,
analytes, geometry, calibration, and background corrections). The maximum time between the start of
processing of the first and last in an RMB is 14 calendar days.
Bias TNI- The systematic or persistent distortion of a measurement process, which causes errors in one
direction (i.e., the expected sample measurement is different from the sample’s true value).
Blank TNI and DoD- A sample that has not been exposed to the analyzed sample stream in order to monitor
contamination during sampling, transport, storage, or analysis. The blank is subjected to the usual
analytical and measurement process to establish a zero baseline or background value and is sometimes
used to adjust or correct routine analytical results (See Method Blank).
DoD- Blank samples are negative control samples, which typically include field blank samples (e.g., trip
blank, equipment (rinsate) blank, and temperature blank) and laboratory blank samples (e.g., method
blank, reagent blank, instrument blank, calibration blank, and storage blank).
Blind Sample A sub-sample for analysis with a composition known to the submitter. The analyst/laboratory may know
the identity of the sample but not its composition. It is used to test the analyst’s or laboratory’s
proficiency in the execution of the measurement process.
BNA (Base Neutral Acid
compounds)
A list of semi-volatile compounds typically analyzed by mass spectrometry methods. Named for the way
they can be extracted out of environmental samples in an acidic, basic, or neutral environment.
BOD (Biochemical
Oxygen Demand)
Chemical procedure for determining how fast biological organisms use up oxygen in a body of water.
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Calibration TNI- A set of operations that establish, under specified conditions, the relationship between values of
quantities indicated by a measuring instrument or measuring system, or values represented by a material
measure or a reference material, and the corresponding values realized by standards. 1) In calibration of
support equipment, the values realized by standards are established through the use of reference
standards that are traceable to the International System of Units (SI); 2) In calibration according to test
methods, the values realized by standards are typically established through the use of Reference Materials
that are either purchased by the laboratory with a certificate of analysis or purity, or prepared by the
laboratory using support equipment that has been calibrated or verified to meet specifications.
Calibration Curve TNI- The mathematical relationship between the known values, such as concentrations, of a series of
calibration standards and their instrument response.
Calibration Method A defined technical procedure for performing a calibration.
Calibration Range DoD- The range of values (concentrations) between the lowest and highest calibration standards of a
multi-level calibration curve. For metals analysis with a single-point calibration, the low-level calibration
check standard and the high standard establish the linear calibration range, which lies within the linear
dynamic range.
Calibration Standard TNI- A substance or reference material used for calibration.
Certified Reference
Material (CRM)
TNI- Reference material accompanied by a certificate, having a value, measurement uncertainty, and
stated metrological traceability chain to a national metrology institute.
Chain of Custody An unbroken trail of accountability that verifies the physical security of samples, data, and records.
Chain of Custody Form
(COC)
TNI- Record that documents the possession of the samples from the time of collection to receipt in the
laboratory. This record generally includes: the number and type of containers; the mode of collection, the
collector, time of collection; preservation; and requested analyses.
Chemical Oxygen
Demand (COD)
A test commonly used to indirectly measure the amount of organic compounds in water.
Client (referred to by
ISO as Customer)
Any individual or organization for whom items or services are furnished or work performed in response
to defined requirements and expectations.
Code of Federal
Regulations (CFR)
A codification of the general and permanent rules published in the Federal Register by agencies of the
federal government.
Comparability An assessment of the confidence with which one data set can be compared to another. Comparable data
are produced through the use of standardized procedures and techniques.
Completeness The percent of valid data obtained from a measurement system compared to the amount of valid data
expected under normal conditions. The equation for completeness is:
% Completeness = (Valid Data Points/Expected Data Points)*100
Confirmation TNI- Verification of the identity of a component through the use of an approach with a different
scientific principle from the original method. These may include but are not limited to second-column
confirmation; alternate wavelength; derivatization; mass spectral interpretation; alternative detectors; or
additional cleanup procedures.
DoD- Includes verification of the identity and quantity of the analyte being measured by another means
(e.g., by another determinative method, technology, or column). Additional cleanup procedures alone are
not considered confirmation techniques.
Conformance An affirmative indication or judgment that a product or service has met the requirements of the relevant
specifications, contract, or regulation; also, the state of meeting the requirements.
Congener A member of a class of related chemical compounds (e.g., PCBs, PCDDs).
Consensus Standard DoD- A standard established by a group representing a cross-section of a particular industry or trade, or a
part thereof.
Continuing Calibration
Blank (CCB)
A blank sample used to monitor the cleanliness of an analytical system at a frequency determined by the
analytical method.
Continuing Calibration
Check Compounds
(CCC)
Compounds listed in mass spectrometry methods that are used to evaluate an instrument calibration from
the standpoint of the integrity of the system. High variability would suggest leaks or active sites on the
instrument column.
Continuing Calibration
Verification
DoD- The verification of the initial calibration. Required prior to sample analysis and at periodic intervals.
Continuing calibration verification applies to both external and internal standard calibration techniques, as
well as to linear and non-linear calibration models.
Continuing Calibration
Verification (CCV)
Standard
Also referred to as a Calibration Verification Standard (CVS) in some methods, it is a standard used to
verify the initial calibration of compounds in an analytical method. CCVs are analyzed at a frequency
determined by the analytical method.
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Continuous Emission
Monitor (CEM)
A flue gas analyzer designed for fixed use in checking for environmental pollutants.
Continuous
Improvement Plan (CIP)
The delineation of tasks for a given laboratory department or committee to achieve the goals of that
department.
Contract Laboratory
Program (CLP)
A national network of EPA personnel, commercial labs, and support contractors whose fundamental
mission is to provide data of known and documented quality.
Contract Required
Detection Limit (CRDL)
Detection limit that is required for EPA Contract Laboratory Program (CLP) contracts.
Contract Required
Quantitation Limit
(CRQL)
Quantitation limit (reporting limit) that is required for EPA Contract Laboratory Program (CLP)
contracts.
Control Chart A graphic representation of a series of test results, together with limits within which results are expected
when the system is in a state of statistical control (see definition for Control Limit)
Control Limit A range within which specified measurement results must fall to verify that the analytical system is in
control. Control limit exceedances may require corrective action or require investigation and flagging of
non-conforming data.
Correction DoD- Action taken to eliminate a detected non-conformity.
Corrective Action DoD- The action taken to eliminate the causes of an existing non-conformity, defect, or other
undesirable situation in order to prevent recurrence. A root cause analysis may not be necessary in all
cases.
Corrective and
Preventative Action
(CAPA)
The primary management tools for bringing improvements to the quality system, to the management
of the quality system’s collective processes, and to the products or services delivered which are an
output of established systems and processes.
Critical Value TNI- Value to which a measurement result is compared to make a detection decision (also known as
critical level or decision level). NOTE: The Critical Value is designed to give a specified low probability
of false detection in an analyte-free sample, which implies that a result that exceeds the Critical Value,
gives high confidence (1 – ) that the radionuclide is actually present in the material analyzed. For
radiometric methods, is often set at 0.05.
Customer DoD- Any individual or organization for which products or services are furnished or work performed in
response to defined requirements and expectations.
Data Integrity TNI- The condition that exists when data are sound, correct, and complete, and accurately reflect
activities and requirements.
Data Quality Objective
(DQO)
Systematic strategic planning tool based on the scientific method that identifies and defines the type,
quality, and quantity of data needed to satisfy a specified use or end user.
Data Reduction TNI- The process of transforming the number of data items by arithmetic or statistical calculation,
standard curves, and concentration factors, and collating them into a more usable form.
Definitive Data DoD- Analytical data of known quantity and quality. The levels of data quality on precision and bias meet
the requirements for the decision to be made. Data that is suitable for final decision-making.
Demonstration of
Capability (DOC)
TNI- A procedure to establish the ability of the analyst to generate analytical results of acceptable
accuracy and precision.
DoD- A procedure to establish the ability of the analyst to generate analytical results by a specific method
that meet measurement quality objectives (e.g., for precision and bias).
Department of Defense
(DoD)
An executive branch department of the federal government of the United States charged with
coordinating and supervising all agencies and functions of the government concerned directly with
national security.
Detection Limit (DL)DoD- The smallest analyte concentration that can be demonstrated to be different than zero or a blank
concentration with 99% confidence. At the DL, the false positive rate (Type 1 error) is 1%. A DL may be
used as the lowest concentration for reliably reporting a detection of a specific analyte in a specific matrix
with a specific method with 99% confidence.
Detection Limit (DL) for
Safe Drinking Water Act
(SDWA) Compliance
TNI- Laboratories that analyze drinking-water samples for SDWA compliance monitoring must use
methods that provide sufficient detection capability to meet the detection limit requirements established
in 40 CFR 141. The SDWA DL for radioactivity is defined in 40 CFR Part 141.25.c as the radionuclide
concentration, which can be counted with a precision of plus or minus 100% at the 95% confidence level
(1.96 where is the standard deviation of the net counting rate of the sample).
Deuterated Monitoring
Compounds (DMCs)
DoD- SIM specific surrogates as specified for GC/MS SIM analysis.
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Diesel Range Organics
(DRO)
A range of compounds that denote all the characteristic compounds that make up diesel fuel (range can
be state or program specific).
Digestion DoD- A process in which a sample is treated (usually in conjunction with heat and acid) to convert the
target analytes in the sample to a more easily measured form.
Document Control The act of ensuring that documents (and revisions thereto) are proposed, reviewed for accuracy,
approved for release by authorized personnel, distributed properly and controlled to ensure use of the
correct version at the location where the prescribed activity is performed.
Documents DoD- Written components of the laboratory management system (e.g., policies, procedures, and
instructions).
Dry Weight The weight after drying in an oven at a specified temperature.
Duplicate (also known as
Replicate or Laboratory
Duplicate)
The analyses or measurements of the variable of interest performed identically on two subsamples of the
same sample. The results of duplicate analyses are used to evaluate analytical or measurement precision
but not the precision of sampling, preservation, or storage internal to the laboratory.
Electron Capture
Detector (ECD)
Device used in GC methods to detect compounds that absorb electrons (e.g., PCB compounds).
Electronic Data
Deliverable (EDD)
A summary of environmental data (usually in spreadsheet form) which clients request for ease of data
review and comparison to historical results.
Eluent A solvent used to carry the components of a mixture through a stationary phase.
Elute To extract, specifically, to remove (absorbed material) from an absorbent by means of a solvent.
Elution A process in which solutes are washed through a stationary phase by movement of a mobile phase.
Environmental Data DoD- Any measurements or information that describe environmental processes, locations, or conditions;
ecological or health effects and consequences; or the performance of environmental technology.
Environmental
Monitoring
The process of measuring or collecting environmental data.
Environmental
Protection Agency
(EPA)
An agency of the federal government of the United States which was created for the purpose of
protecting human health and the environment by writing and enforcing regulations based on laws passed
by Congress.
Environmental Sample A representative sample of any material (aqueous, non-aqueous, or multimedia) collected from any source
for which determination of composition or contamination is requested or required. Environmental
samples can generally be classified as follows:
Non-Potable Water (Includes surface water, ground water, effluents, water treatment
chemicals, and TCLP leachates or other extracts)
Drinking Water - Delivered (treated or untreated) water designated as potable water
Water/Wastewater - Raw source waters for public drinking water supplies, ground waters,
municipal influents/effluents, and industrial influents/effluents
Sludge - Municipal sludges and industrial sludges.
Soil - Predominately inorganic matter ranging in classification from sands to clays.
Waste - Aqueous and non-aqueous liquid wastes, chemical solids, and industrial liquid and
solid wastes
Equipment Blank A sample of analyte-free media used to rinse common sampling equipment to check effectiveness of
decontamination procedures.
Extracted Internal
Standard Analyte
Isotopically labeled analogs of analytes of interest added to all standards, blanks and samples analyzed.
Added to samples and batch QC samples prior to the first step of sample extraction and to standards and
instrument blanks prior to analysis. Used for isotope dilution methods.
Facility A distinct location within the company that has unique certifications, personnel, and waste disposal
identifications.
False Negative DoD- A result that fails to identify (detect) an analyte or reporting an analyte to be present at or below a
level of interest when the analyte is actually above the level of interest.
False Positive DoD- A result that erroneously identifies (detects) an analyte or reporting an analyte to be present above
a level of interest when the analyte is actually present at or below the level of interest.
Field Blank A blank sample prepared in the field by filling a clean container with reagent water and appropriate
preservative, if any, for the specific sampling activity being undertaken.
Field Measurement Determination of physical, biological, or radiological properties, or chemical constituents that are
measured on-site, close in time and sPAS to the matrices being sampled/measured, following accepted
test methods. This testing is performed in the field outside of a fixed-laboratory or outside of an enclosed
structure that meets the requirements of a mobile laboratory.
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Field of Accreditation TNI- Those matrix, technology/method, and analyte combinations for which the accreditation body
offers accreditation.
Field of Proficiency
Testing (FoPT)
TNI- Matrix, technology/method, analyte combinations for which the composition, spike concentration
ranges and acceptance criteria have been established by the PTPEC.
Finding TNI- An assessment conclusion referenced to a laboratory accreditation standard and supported by
objective evidence that identifies a deviation from a laboratory accreditation standard requirement.
DoD- An assessment conclusion that identifies a condition having a significant effect on an item or
activity. An assessment finding may be positive, negative, or neutral and is normally accompanied by
specific examples of the observed condition. The finding must be linked to a specific requirement (e.g.,
this standard, ISO requirements, analytical methods, contract specifications, or laboratory management
systems requirements).
Flame Atomic
Absorption Spectrometer
(FAA)
Instrumentation used to measure the concentration of metals in an environmental sample based on the
fact that ground state metals absorb light at different wavelengths. Metals in a solution are converted to
the atomic state by use of a flame.
Flame Ionization
Detector (FID)
A type of gas detector used in GC analysis where samples are passed through a flame which ionizes the
sample so that various ions can be measured.
Gas Chromatography
(GC)
Instrumentation which utilizes a mobile carrier gas to deliver an environmental sample across a stationary
phase with the intent to separate compounds out and measure their retention times.
Gas Chromatograph/
Mass Spectrometry
(GC/MS)
In conjunction with a GC, this instrumentation utilizes a mass spectrometer which measures fragments of
compounds and determines their identity by their fragmentation patterns (mass spectra).
Gasoline Range Organics
(GRO)
A range of compounds that denote all the characteristic compounds that make up gasoline (range can be
state or program specific).
Graphite Furnace
Atomic Absorption
Spectrometry (GFAA)
Instrumentation used to measure the concentration of metals in an environmental sample based on the
absorption of light at different wavelengths that are characteristic of different analytes.
High Pressure Liquid
Chromatography
(HPLC)
Instrumentation used to separate, identify, and quantitate compounds based on retention times which are
dependent on interactions between a mobile phase and a stationary phase.
Holding Time TNI- The maximum time that can elapse between two specified activities.
40 CFR Part 136- The maximum time that samples may be held prior to preparation and/or analysis as
defined by the method and still be considered valid or not compromised.
For sample prep purposes, hold times are calculated using the time of the start of the preparation
procedure.
DoD- The maximum time that may elapse from the time of sampling to the time of preparation or
analysis, or from preparation to analysis, as appropriate.
Homogeneity The degree to which a property or substance is uniformly distributed throughout a sample.
Homologue One in a series of organic compounds in which each successive member has one more chemical group in
its molecule than the next preceding member. For instance, methanol, ethanol, propanol, butanol, etc.,
form a homologous series.
Improper Actions DoD- Intentional or unintentional deviations from contract-specified or method-specified analytical
practices that have not been authorized by the customer (e.g., DoD or DOE).
Incremental Sampling
Method (ISM)
Soil preparation for large volume (1 kg or greater) samples.
In-Depth Data
Monitoring
TNI- When used in the context of data integrity activities, a review and evaluation of documentation
related to all aspects of the data generation process that includes items such as preparation, equipment,
software, calculations, and quality controls. Such monitoring shall determine if the laboratory uses
appropriate data handling, data use and data reduction activities to support the laboratory’s data integrity
policies and procedures.
Inductively Coupled
Plasma Atomic Emission
Spectrometry (ICP-AES)
Analytical technique used for the detection of trace metals which uses plasma to produce excited atoms
that emit radiation of characteristic wavelengths.
Inductively Coupled
Plasma- Mass
Spectrometry (ICP/MS)
An ICP that is used in conjunction with a mass spectrometer so that the instrument is not only capable of
detecting trace amounts of metals and non-metals but is also capable of monitoring isotopic speciation
for the ions of choice.
Infrared Spectrometer
(IR)
An instrument that uses infrared light to identify compounds of interest.
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Initial Calibration (ICAL)The process of analyzing standards, prepared at specified concentrations, to define the quantitative
response relationship of the instrument to the analytes of interest. Initial calibration is performed
whenever the results of a calibration verification standard do not conform to the requirements of the
method in use or at a frequency specified in the method.
Initial Calibration Blank
(ICB)
A blank sample used to monitor the cleanliness of an analytical system at a frequency determined by the
analytical method. This blank is specifically run in conjunction with the Initial Calibration Verification
(ICV) where applicable.
Initial Calibration
Verification (ICV)
DoD- Verifies the initial calibration with a standard obtained or prepared from a source independent of
the source of the initial calibration standards to avoid potential bias of the initial calibration.
Injection Internal
Standard Analyte
Isotopically labeled analogs of analytes of interest (or similar in physiochemical properties to the target
analytes but with a distinct response) to be quantitated. Added to all blanks, standards, samples, and batch
QC after extraction and prior to analysis.
Instrument Blank A clean sample (e.g., distilled water) processed through the instrumental steps of the measurement
process; used to determine instrument contamination.
Instrument Detection
Limits (IDLs)
Limits determined by analyzing a series of reagent blank analyses to obtain a calculated concentration.
IDLs are determined by calculating the average of the standard deviations of three runs on three non-
consecutive days from the analysis of a reagent blank solution with seven consecutive measurements per
day.
Interference, spectral Occurs when particulate matter from the atomization scatters incident radiation from the source or when
the absorption or emission from an interfering species either overlaps or is so close to the analyte
wavelength that resolution becomes impossible.
Interference, chemical Results from the various chemical processes that occur during atomization and later the absorption
characteristics of the analyte.
Internal Standard TNI and DoD- A known amount of standard added to a test portion of a sample as a reference for
evaluating and controlling the precision and bias of the applied analytical method.
International
Organization for
Standardization (ISO)
An international standard-setting body composed of representatives from various national standards
organizations.
Intermediate Standard
Solution
Reference solutions prepared by dilution of the stock solutions with an appropriate solvent.
International System of
Units (SI)
The coherent system of units adopted and recommended by the General Conference on Weights and
Measures.
Ion Chromatography
(IC)
Instrumentation or process that allows the separation of ions and molecules based on the charge
properties of the molecules.
Isomer One of two or more compounds, radicals, or ions that contain the same number of atoms of the same
element but differ in structural arrangement and properties. For example, hexane (C6H14) could be n-
hexane, 2-methylpentane, 3-methylpentane, 2,3-dimethylbutane, 2,2-dimethylbutane.
Laboratory A body that calibrates and/or performs testing.
Laboratory Control
Sample (LCS)
TNI- (also known as laboratory fortified blank (LFB), spiked blank, or QC check sample): A sample
matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material
containing known and verified amounts of analytes and taken through all sample preparation and
analytical steps of the procedure unless otherwise noted in a reference method. It is generally used to
establish intra-laboratory or analyst-specific precision and bias or to evaluate the performance of all or a
portion of the measurement system.
Laboratory Duplicate Aliquots of a sample taken from the same container under laboratory conditions and processed and
analyzed independently.
Laboratory Information
Management System
(LIMS)
DoD- The entirety of an electronic data system (including hardware and software) that collects, analyzes,
stores, and archives electronic records and documents.
Learning Management
System (LMS)
A web-based database used by the laboratories to track and document training activities. The system is
administered by the corporate training department and each laboratory’s learn centers are maintained by a
local administrator.
Legal Chain-of-Custody
Protocols
TNI- Procedures employed to record the possession of samples from the time of sampling through the
retention time specified by the client or program. These procedures are performed at the special request
of the client and include the use of a Chain-of-Custody (COC) Form that documents the collection,
transport, and receipt of compliance samples by the laboratory. In addition, these protocols document all
handling of the samples within the laboratory.
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Limit(s) of Detection
(LOD)
TNI- The minimum result, which can be reliably discriminated from a blank with predetermined
confidence level.
DoD- The smallest concentration of a substance that must be present in a sample in order to be detected
at the DL with 99% confidence. At the LOD, the false negative rate (Type II error) is 1%. A LOD may
be used as the lowest concentration for reliably reporting a non-detect of a specific analyte in a specific
matrix with a specific method at 99% confidence.
Limit(s) of Quantitation
(LOQ)
TNI- The minimum levels, concentrations, or quantities of a target variable (e.g., target analyte) that can
be reported with a specified degree of confidence.
DoD- The smallest concentration that produces a quantitative result with known and recorded precision
and bias. For DoD/DOE projects, the LOQ shall be set at or above the concentration of the lowest
initial calibration standard and within the calibration range.
Linear Dynamic Range DoD- Concentration range where the instrument provides a linear response.
Liquid chromatography/
tandem mass
spectrometry
(LC/MS/MS)
Instrumentation that combines the physical separation techniques of liquid chromatography with the
mass analysis capabilities of mass spectrometry.
Lot TNI- A definite amount of material produced during a single manufacturing cycle and intended to have
uniform character and quality.
Management Those individuals directly responsible and accountable for planning, implementing, and assessing work.
Management System System to establish policy and objectives and to achieve those objectives.
Manager (however
named)
The individual designated as being responsible for the overall operation, all personnel, and the physical
plant of the environmental laboratory. A supervisor may report to the manager. In some cases, the
supervisor and the manager may be the same individual.
Matrix TNI- The substrate of a test sample.
Matrix Duplicate TNI- A replicate matrix prepared in the laboratory and analyzed to obtain a measure of precision.
Matrix Spike (MS)
(spiked sample or
fortified sample)
TNI- A sample prepared, taken through all sample preparation and analytical steps of the procedure
unless otherwise noted in a referenced method, by adding a known amount of target analyte to a specified
amount of sample for which an independent test result of target analyte concentration is available. Matrix
spikes are used, for example, to determine the effect of the matrix on a method’s recovery efficiency.
Matrix Spike Duplicate
(MSD) (spiked sample or
fortified sample
duplicate)
TNI- A replicate matrix spike prepared in the laboratory and analyzed to obtain a measure of the
precision of the recovery for each analyte.
Measurement
Performance Criteria
(MPC)
DoD- Criteria that may be general (such as completion of all tests) or specific (such as QC method
acceptance limits) that are used by a project to judge whether a laboratory can perform a specified activity
to the defined criteria.
Measurement Quality
Objective (MQO)
TNI- The analytical data requirements of the data quality objectives are project- or program-specific and
can be quantitative or qualitative. MQOs are measurement performance criteria or objectives of the
analytical process. Examples of quantitative MQOs include statements of required analyte detectability
and the uncertainty of the analytical protocol at a specified radionuclide activity, such as the action level.
Examples of qualitative MQOs include statements of the required specificity of the analytical protocol,
e.g., the ability to analyze for the radionuclide of interest given the presence of interferences.
Measurement System TNI- A method, as implemented at a particular laboratory, and which includes the equipment used to
perform the test and the operator(s).
DoD- A test method, as implemented at a particular laboratory, and which includes the equipment used
to perform the sample preparation and test and the operator(s).
Measurement
Uncertainty
DoD- An estimate of the error in a measurement often stated as a range of values that contain the true
value within a certain confidence level. The uncertainty generally includes many components which may
be evaluated from experimental standard deviations based on repeated observations or by standard
deviations evaluated from assumed probability distributions based on experience or other information.
For DoD/DOE, a laboratory’s Analytical Uncertainty (such as use of LCS control limits) can be reported
as the minimum uncertainty.
Method TNI- A body of procedures and techniques for performing an activity (e.g., sampling, chemical analysis,
quantification), systematically presented in the order in which they are to be executed.
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Method Blank TNI- A sample of a matrix similar to the batch of associated samples (when available) that is free from
the analytes of interest and is processed simultaneously with and under the same conditions as samples
through all steps of the analytical procedures, and in which no target analytes or interferences are present
at concentrations that impact the analytical results for sample analyses.
Method Detection Limit
(MDL)
TNI- One way to establish a Detection Limit; defined as the minimum concentration of a substance that
can be measured and reported with 99% confidence that the analyte concentration is greater than zero
and is determined from analysis of a sample in a given matrix containing the analyte.
Method of Standard
Additions
A set of procedures adding one or more increments of a standard solution to sample aliquots of the same
size in order to overcome inherent matrix effects. The procedures encompass the extrapolation back to
obtain the sample concentration.
Minimum Detectable
Activity (MDA)
TNI- Estimate of the smallest true activity that ensures a specified high confidence, 1 – , of detection
above the Critical Value, and a low probability of false negatives below the Critical Value. For
radiometric methods, is often set at 0.05. NOTE 1: The MDS is a measure of the detection capability
of a measurement process and as such, it is an a priori concept. It may be used in the selection of
methods to meet specified MQOs. Laboratories may also calculate a “sample specific” MDA, which
indicates how well the measurement process is performing under varying real-world measurement
conditions, when sample-specific characteristics (e.g., interferences) may affect the detection capability.
However, the MDA must never be used instead of the Critical Value as a detection threshold. NOTE 2:
For the purpose of this Standard, the terms MDA and minimum detectable concentration (MDC) are
equivalent.
Minimum Reporting
Limit (MRL)
the lowest concentration of standard used for calibration – Drinking Water Manual
MintMiner Commercial software program used to scan large amounts of chromatographic data to monitor for errors
or data integrity issues.
Mobile Laboratory TNI- A portable enclosed structure with necessary and appropriate accommodation and environmental
conditions for a laboratory, within which testing is performed by analysts. Examples include but are not
limited to trailers, vans, and skid-mounted structures configured to house testing equipment and
personnel.
National Environmental
Laboratory Accreditation
Conference (NELAC)
See definition of The NELAC Institute (TNI).
National Institute of
Occupational Safety and
Health (NIOSH)
National institute charged with the provision of training, consultation, and information in the area of
occupational safety and health.
National Institute of
Standards and
Technology (NIST)
TNI- A federal agency of the US Department of Commerce’s Technology Administration that is
designed as the United States national metrology institute (or NMI).
National Pollutant
Discharge Elimination
System (NPDES)
A permit program that controls water pollution by regulating point sources that discharge pollutants into
U.S. waters.
Negative Control Measures taken to ensure that a test, its components, or the environment do not cause undesired effects,
or produce incorrect test results.
Nitrogen Phosphorus
Detector (NPD)
A detector used in GC analyses that utilizes thermal energy to ionize an analyte. With this detector,
nitrogen and phosphorus can be selectively detected with a higher sensitivity than carbon.
Nonconformance An indication or judgment that a product or service has not met the requirement of the relevant
specifications, contract, or regulation; also, the state of failing to meet the requirements.
Not Detected (ND)The result reported for a compound when the detected amount of that compound is less than the
method reporting limit.
Operator Aid DoD- A technical posting (such as poster, operating manual, or notepad) that assists workers in
performing routine tasks. All operator aids must be controlled documents (i.e., a part of the laboratory
management system).
Performance Based
Measurement System
(PBMS)
An analytical system wherein the data quality needs, mandates or limitations of a program or project are
specified and serve as criteria for selecting appropriate test methods to meet those needs in a cost-
effective manner.
Physical Parameter TNI- A measurement of a physical characteristic or property of a sample as distinguished from the
concentrations of chemical and biological components.
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Photo-ionization
Detector (PID)
An ion detector which uses high-energy photons, typically in the ultraviolet range, to break molecules into
positively charged ions.
Polychlorinated
Biphenyls (PCB)
A class of organic compounds that were used as coolants and insulating fluids for transformers and
capacitors. The production of these compounds was banned in the 1970’s due to their high toxicity.
Positive Control Measures taken to ensure that a test and/or its components are working properly and producing correct
or expected results from positive test subjects.
Post-Digestion Spike A sample prepared for metals analyses that has analytes spike added to determine if matrix effects may be
a factor in the results.
Power of Hydrogen (pH)The measure of acidity or alkalinity of a solution.
Practical Quantitation
Limit (PQL)
Another term for a method reporting limit. The lowest reportable concentration of a compound based
on parameters set up in an analytical method and the laboratory’s ability to reproduce those conditions.
Precision TNI- The degree to which a set of observations or measurements of the same property, obtained under
similar conditions, conform to themselves; a data quality indicator. Precision is usually expressed as
standard deviation, variance, or range, in either absolute or relative terms.
Preservation TNI and DoD- Any conditions under which a sample must be kept in order to maintain chemical,
physical, and/or biological integrity prior to analysis.
Primary Accreditation
Body (Primary AB)
TNI- The accreditation body responsible for assessing a laboratory’s total quality system, on-site
assessment, and PT performance tracking for fields of accreditation.
Procedure TNI- A specified way to carry out an activity or process. Procedures can be documented or not.
Proficiency Testing (PT)TNI- A means to evaluate a laboratory’s performance under controlled conditions relative to a given set
of criteria, through analysis of unknown samples provided by an external source.
Proficiency Testing
Program (PT Program)
TNI- The aggregate of providing rigorously controlled and standardized environmental samples to a
laboratory for analysis, reporting of results, statistical evaluation of the results and the collective
demographics and results summary of all participating laboratories.
Proficiency Testing
Provider (PT Provider)
TNI- A person or organization accredited by a TNI-approved Proficiency Testing Provider Accreditor to
operate a TNI-compliant PT Program.
Proficiency Testing
Provider Accreditor
(PTPA)
TNI- An organization that is approved by TNI to accredit and monitor the performance of proficiency
testing providers.
Proficiency Testing
Reporting Limit (PTRL)
TNI- A statistically derived value that represents the lowest acceptable concentration for an analyte in a
PT sample, if the analyte is spiked into the PT sample. The PTRLs are specified in the TNI FoPT tables.
Proficiency Testing
Sample (PT)
TNI- A sample, the composition of which is unknown to the laboratory, and is provided to test whether
the laboratory can produce analytical results within the specified acceptance criteria.
Proficiency Testing (PT)
Study
TNI- a) Scheduled PT Study: A single complete sequence of circulation and scoring of PT samples to all
participants in a PT program. The study must have the same pre-defined opening and closing dates for all
participants; b) Supplemental PT Study: A PT sample that may be from a lot previously released by a PT
Provider that meets the requirements for supplemental PT samples given in Volume 3 of this Standard
[TNI] but that does not have a pre-determined opening date and closing date.
Proficiency Testing Study
Closing Date
TNI- a) Scheduled PT Study: The calendar date by which all participating laboratories must submit
analytical results for a PT sample to a PT Provider; b) Supplemental PT Study: The calendar date a
laboratory submits the results for a PT sample to the PT Provider.
Proficiency Testing Study
Opening Date
TNI- a) Scheduled PT Study: The calendar date that a PT sample is first made available to all participants
of the study by a PT Provider; b) Supplemental PT Study: The calendar date the PT Provider ships the
sample to a laboratory.
Protocol TNI- A detailed written procedure for field and/or laboratory operation (e.g., sampling, analysis) that
must be strictly followed.
Qualitative Analysis DoD- Analysis designed to identify the components of a substance or mixture.
Quality Assurance (QA)TNI- An integrated system of management activities involving planning, implementation, assessment,
reporting and quality improvement to ensure that a process, item, or service is of the type and quality
needed and expected by the client.
Quality Assurance
Manual (QAM)
A document stating the management policies, objectives, principles, organizational structure and
authority, responsibilities, accountability, and implementation of an agency, organization, or laboratory, to
ensure the quality of its product and the utility of its product to its users.
Quality Assurance
Project Plan (QAPP)
A formal document describing the detailed quality control procedures by which the quality requirements
defined for the data and decisions pertaining to a specific project are to be achieved.
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Quality Control (QC)TNI- The overall system of technical activities that measures the attributes and performance of a process,
item, or service against defined standards to verify that they meet the stated requirements established by
the customer; operational techniques and activities that are used to fulfill requirements for quality; also the
system of activities and checks used to ensure that measurement systems are maintained within
prescribed limits, providing protection against “out of control” conditions and ensuring that the results
are of acceptable quality.
Quality Control Sample
(QCS)
TNI- A sample used to assess the performance of all or a portion of the measurement system. One of
any number of samples, such as Certified Reference Materials, a quality system matrix fortified by spiking,
or actual samples fortified by spiking, intended to demonstrate that a measurement system or activity is in
control.
Quality Manual TNI- A document stating the management policies, objectives, principles, organizational structure and
authority, responsibilities, accountability, and implementation of an agency, organization, or laboratory, to
ensure the quality of its product and the utility of its product to its users.
Quality System TNI and DoD- A structured and documented management system describing the policies, objectives,
principles, organizational authority, responsibilities, accountability, and implementation plan of an
organization for ensuring quality in its work processes, products (items), and services. The quality system
provides the framework for planning, implementing, and assessing work performed by the organization
and for carrying out required quality assurance and quality control activities.
Quality System Matrix TNI and DoD- These matrix definitions shall be used for purposes of batch and quality control
requirements and may be different from a field of accreditation matrix:
Air and Emissions: Whole gas or vapor samples including those contained in flexible or rigid
wall containers and the extracted concentrated analytes of interest from a gas or vapor that are
collected with a sorbant tube, impinger solution, filter, or other device
Aqueous: Any aqueous sample excluded from the definition of Drinking Water or
Saline/Estuarine. Includes surface water, groundwater effluents, and TCLP or other
extracts.
Biological Tissue: Any sample of a biological origin such as fish tissue, shellfish, or plant
material. Such samples shall be grouped according to origin.
Chemical Waste: A product or by-product of an industrial process that results in a matrix
not previously defined.
Drinking Water: Any aqueous sample that has been designated a potable or potentially
potable water source.
Non-aqueous liquid: Any organic liquid with <15% settleable solids
Saline/Estuarine: Any aqueous sample from an ocean or estuary, or other saltwater source
such as the Great Salt Lake.
Solids: Includes soils, sediments, sludges, and other matrices with >15% settleable solids.
Quantitation Range DoD- The range of values (concentrations) in a calibration curve between the LOQ and the highest
successively analyzed initial calibration standard used to relate instrument response to analyte
concentration. The quantitation range (adjusted for initial sample volume/weight, concentration/dilution,
and final volume) lies within the calibration range.
Quantitative Analysis DoD- Analysis designed to determine the amounts or proportions of the components of a substance.
Random Error The EPA has established that there is a 5% probability that the results obtained for any one analyte will
exceed the control limits established for the test due to random error. As the number of compounds
measured increases in a given sample, the probability for statistical error also increases.
Raw Data TNI- The documentation generated during sampling and analysis. This documentation includes, but is
not limited to, field notes, electronic data, magnetic tapes, untabulated sample results, QC sample results,
print outs of chromatograms, instrument outputs, and handwritten records.
Reagent Blank (method
reagent blank)
A sample consisting of reagent(s), without the target analyte or sample matrix, introduced into the
analytical procedure at the appropriate point and carried through all subsequent steps to determine the
contribution of the reagents and of the involved analytical steps.
Reagent Grade Analytical reagent (AR) grade, ACS reagent grade, and reagent grade are synonymous terms for reagents
that conform to the current specifications of the Committee on Analytical Reagents of the American
Chemical Society.
Records DoD- The output of implementing and following management system documents (e.g., test data in
electronic or hand-written forms, files, and logbooks).
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Reference Material TNI- Material or substance one or more of whose property values are sufficiently homogenized and well
established to be used for the calibration of an apparatus, the assessment of a measurement method, or
for assigning values to materials.
Reference Method TNI- A published method issued by an organization generally recognized as competent to do so. (When
the ISO language refers to a “standard method,” that term is equivalent to “reference method”). When a
laboratory is required to analyze by a specified method due to a regulatory requirement, the
analyte/method combination is recognized as a reference method. If there is no regulatory requirement
for the analyte/method combination, the analyte/method combination is recognized as a reference
method if it can be analyzed by another reference method of the same matrix and technology.
Reference Standard TNI- Standard used for the calibration of working measurement standards in a given organization or at a
given location.
Relative Percent
Difference (RPD)
A measure of precision defined as the difference between two measurements divided by the average
concentration of the two measurements.
Reporting Limit (RL)The level at which method, permit, regulatory and customer-specific objectives are met. The reporting
limit may never be lower than the Limit of Detection (i.e., statistically determined MDL). Reporting limits
are corrected for sample amounts, including the dry weight of solids, unless otherwise specified. There
must be a sufficient buffer between the Reporting Limit and the MDL.
DoD- A customer-specified lowest concentration value that meets project requirements for quantitative
data with known precision and bias for a specific analyte in a specific matrix.
Reporting Limit
Verification Standard
(RLVS)
A standard analyzed at the reporting limit for an analysis to verify the laboratory’s ability to report to that
level.
Representativeness A quality element related to the ability to collect a sample reflecting the characteristics of the part of the
environment to be assessed. Sample representativeness is dependent on the sampling techniques specified
in the project work plan.
Requirement Denotes a mandatory specification; often designated by the term “shall.”
Retention Time The time between sample injection and the appearance of a solute peak at the detector.
Revocation TNI- The total or partial withdrawal of a laboratory’s accreditation by an accreditation body.
Sample Portion of material collected for analysis, identified by a single, unique alphanumeric code. A sample may
consist of portions in multiple containers, if a single sample is submitted for multiple or repetitive
analysis.
Sample Condition Upon
Receipt Form (SCURF)
Form used by sample receiving personnel to document the condition of sample containers upon receipt
to the laboratory (used in conjunction with a COC).
Sample Delivery Group
(SDG)
A unit within a single project that is used to identify a group of samples for delivery. An SDG is a group
of 20 or fewer field samples within a project, received over a period of up to 14 calendar days. Data from
all samples in an SDG are reported concurrently.
Sample Receipt Form
(SRF)
Letter sent to the client upon login to show the tests requested and pricing.
Sample Tracking Procedures employed to record the possession of the samples from the time of sampling until analysis,
reporting and archiving. These procedures include the use of a chain-of-custody form that documents the
collection, transport, and receipt of compliance samples to the laboratory. In addition, access to the
laboratory is limited and controlled to protect the integrity of the samples.
Sampling TNI- Activity related to obtaining a representative sample of the object of conformity assessment,
according to a procedure.
Selected Ion Monitoring
(SIM)
A mode of analysis in mass spectrometry where the detector is set to scan over a very small mass range,
typically one mass unit. The narrower the range, the more sensitive the detector.
DoD- Using GC/MS, characteristic ions specific to target compounds are detected and used to quantify
in applications where the normal full scan mass spectrometry results in excessive noise.
Selectivity TNI- The ability to analyze, distinguish, and determine a specific analyte or parameter from another
component that may be a potential interferent or that may behave similarly to the target analyte or
parameter within the measurement system.
Sensitivity TNI- The capability of a method or instrument to discriminate between measurement responses
representing different levels (e.g., concentrations) of a variable of interest.
Serial Dilution The stepwise dilution of a substance in a solution.
Shall Denotes a requirement that is mandatory whenever the criterion for conformance with the specification
requires that there be no deviation. This does not prohibit the use of alternative approaches or methods
for implementing the specification as long as the requirement is fulfilled.
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Should Denotes a guideline or recommendation whenever noncompliance with the specification is permissible.
Signal-to-Noise Ratio
(S/N)
DoD- A measure of signal strength relative to background noise. The average strength of the noise of
most measurements is constant and independent of the magnitude of the signal. Thus, as the quantity
being measured (producing the signal) decreases in magnitude, S/N decreases and the effect of the noise
on the relative error of a measurement increases.
Source Water TNI- When sampled for drinking water compliance, untreated water from streams, rivers, lakes, or
underground aquifers, which is used to supply private and public drinking water supplies.
Spike A known mass of target analyte added to a blank sample or sub-sample; used to determine recovery
efficiency or for other quality control purposes.
Standard (Document)TNI- The document describing the elements of a laboratory accreditation that has been developed and
established within the consensus principles of standard setting and meets the approval requirements of
standard adoption organizations procedures and policies.
Standard (Chemical)Standard samples are comprised of a known amount of standard reference material in the matrix
undergoing analysis. A standard reference material is a certified reference material produced by US NIST
and characterized for absolute content, independent of analytical test method.
Standard Blank (or
Reagent Blank)
A calibration standard consisting of the same solvent/reagent matrix used to prepare the calibration
standards without the analytes. It is used to construct the calibration curve by establishing instrument
background.
Standard Method A test method issued by an organization generally recognized as competent to do so.
Standard Operating
Procedure (SOP)
TNI- A written document that details the method for an operation, analysis, or action with thoroughly
prescribed techniques and steps. SOPs are officially approved as the methods for performing certain
routine or repetitive tasks.
Standard Reference
Material (SRM)
A certified reference material produced by the US NIST or other equivalent organization and
characterized for absolute content, independent of analytical method.
Statement of
Qualifications (SOQ)
A document that lists information about a company, typically the qualifications of that company to
compete on a bid for services.
Stock Standard A concentrated reference solution containing one or more analytes prepared in the laboratory using
an assayed reference compound or purchased from a reputable commercial source.
Storage Blank DoD- A sample of analyte-free media prepared by the laboratory and retained in the sample storage area
of the laboratory. A storage blank is used to record contamination attributable to sample storage at the
laboratory.
Supervisor The individual(s) designated as being responsible for a particular area or category of scientific analysis.
This responsibility includes direct day-to-day supervision of technical employees, supply and instrument
adequacy and upkeep, quality assurance/quality control duties and ascertaining technical employees have
the required balance of education, training, and experience to perform the required analyses.
Surrogate DoD- A substance with properties that mimic the analyte of interest. It is unlikely to be found in
environmental samples and is added to them for quality control purposes.
Suspension TNI- The temporary removal of a laboratory’s accreditation for a defined period of time, which shall not
exceed 6 months or the period of accreditation, whichever is longer, in order to allow the laboratory time
to correct deficiencies or area of non-conformance with the Standard.
Systems Audit An on-site inspection or assessment of a laboratory’s quality system.
Target Analytes DoD- Analytes or chemicals of primary concern identified by the customer on a project-specific basis.
Technical Director Individual(s) who has overall responsibility for the technical operation of the environmental testing
laboratory.
Technology TNI- A specific arrangement of analytical instruments, detection systems, and/or preparation techniques.
Test A technical operation that consists of the determination of one or more characteristics or performance of
a given product, material, equipment, organism, physical phenomenon, process, or service according to a
specified procedure. The result of a test is normally recorded in a document sometimes called a test
report or a test certificate.
Test Method DoD- A definitive procedure that determines one or more characteristics of a given substance or
product.
Test Methods for
Evaluating Solid Waste,
Physical/ Chemical (SW-
846)
EPA Waste’s official compendium of analytical and sampling methods that have been evaluated and
approved for use in complying with RCRA regulations.
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Test Source TNI- A radioactive source that is tested, such as a sample, calibration standard, or performance check
source. A Test Source may also be free of radioactivity, such as a Test Source counted to determine the
subtraction background, or a short-term background check.
The NELAC Institute
(TNI)
A non-profit organization whose mission is to foster the generation of environmental data of known and
documented quality through an open, inclusive, and transparent process that is responsive to the needs of
the community. Previously known as NELAC (National Environmental Laboratory Accreditation
Conference).
Total Petroleum
Hydrocarbons (TPH)
A term used to denote a large family of several hundred chemical compounds that originate from crude
oil. Compounds may include gasoline components, jet fuel, volatile organics, etc.
Toxicity Characteristic
Leaching Procedure
(TCLP)
A solid sample extraction method for chemical analysis employed as an analytical method to simulate
leaching of compounds through a landfill.
Traceability TNI- The ability to trace the history, application, or location of an entity by means of recorded
identifications. In a calibration sense, traceability relates measuring equipment to national or international
standards, primary standards, basic physical conditions or properties, or reference materials. In a data
collection sense, it relates calculations and data generated throughout the project back to the requirements
for the quality of the project.
Training Document A training resource that provides detailed instructions to execute a specific method or job function.
Trip Blank This blank sample is used to detect sample contamination from the container and preservative during
transport and storage of the sample. A cleaned sample container is filled with laboratory reagent water
and the blank is stored, shipped, and analyzed with its associated samples.
Tuning A check and/or adjustment of instrument performance for mass spectrometry as required by the
method.
Ultraviolet
Spectrophotometer (UV)
Instrument routinely used in quantitative determination of solutions of transition metal ions and highly
conjugated organic compounds.
Uncertainty, Counting TNI- The component of Measurement Uncertainty attributable to the random nature of radioactive
decay and radiation counting (often estimated as the square root of observed counts (MARLAP). Older
references sometimes refer to this parameter as Error, Counting Error, or Count Error (c.f., Total
Uncertainty).
Uncertainty, Expanded TNI- The product of the Standard Uncertainty and a coverage factor, k, which is chosen to produce an
interval about the result that has a high probability of containing the value of the measurand (c.f.,
Standard Uncertainty). NOTE: Radiochemical results are generally reported in association with the Total
Uncertainty. Either if these estimates of uncertainty can be reported as the Standard Uncertainty (one-
sigma) or as an Expanded Uncertainty (k-sigma, where k > 1).
Uncertainty,
Measurement
TNI- Parameter associated with the result of a measurement that characterizes the dispersion of the
values that could reasonably be attributed to the measurand.
Uncertainty, Standard TNI- An estimate of the Measurement Uncertainty expressed as a standard deviation (c.f., Expanded
Uncertainty).
Uncertainty, Total TNI- An estimate of the Measurement Uncertainty that accounts for contributions from all significant
sources of uncertainty associated with the analytical preparation and measurement of a sample. Such
estimates are also commonly referred to as Combined Standard Uncertainty or Total Propagated
Uncertainty, and in some older references as the Total Propagated Error, among other similar items (c.f.,
Counting Uncertainty).
Unethical actions DoD- Deliberate falsification of analytical or quality control results where failed method or contractual
requirements are made to appear acceptable.
United States
Department of
Agriculture (USDA)
A department of the federal government that provides leadership on food, agriculture, natural resources,
rural development, nutrition, and related issues based on public policy, the best available science, and
effective management.
United States Geological
Survey (USGS)
Program of the federal government that develops new methods and tools to supply timely, relevant, and
useful information about the Earth and its processes.
Unregulated
Contaminant Monitoring
Rule (UCMR)
EPA program to monitor unregulated contaminants in drinking water.
Validation DoD- The confirmation by examination and provision of objective evidence that the particular
requirements for a specific intended use are fulfilled.
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Verification TNI- Confirmation by examination and objective evidence that specified requirements have been met. In
connection with the management of measuring equipment, verification provides a means for checking
that the deviations between values indicated by a measuring instrument and corresponding known values
of a measured quantity are consistently smaller than the maximum allowable error defined in a standard,
regulation, or specification peculiar to the management of the measuring equipment.
Voluntary Action
Program (VAP)
A program of the Ohio EPA that gives individuals a way to investigate possible environmental
contamination, clean it up if necessary and receive a promise from the State of Ohio that no more
cleanup is needed.
Whole Effluent Toxicity
(WET)
The aggregate toxic effect to aquatic organisms from all pollutants contained in a facility’s wastewater
(effluent).
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ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
7.5 Appendix E: Equipment Listing
The equipment listed represents equipment were held by each location on the effective date of this
manual. This information is subject to change without notice. External parties should contact the
location for the most current information.
7.5.1 PAS-Mt. Juliet
Equipment List: PAS-Mt. Juliet
Description Manufacturer Model Serial Number Service
Date
Condition Location Internal
ID
Manual
Location
GC/FID Agilent 6890N US10137006 As
Needed
Used Air Lab AIRGC2 Online
GC/FID Agilent 6890N US10137006 As
Needed
Used Air Lab AIRGC2 Online
Gas
Chromatograph
HP 6890N TCD US10726007 As
Needed
Used Air Lab AIRGC3 Online
GC/FID Agilent 7890B CN14513033 As
Needed
Used Air Lab AIRGC4 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 7890A/5975 CN13231014
US50680012
As
Needed
Used Air Lab AIRMS1 Online
Preconcentrator Entech 7200 1683 As
Needed
Used Air Lab AIRMS1 Online
Canister
Autosampler
Entech 7016D 1708 As
Needed
Used Air Lab AIRMS1 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 6890N/5975 CN10551083
US61332744
As
Needed
Used Air Lab AIRMS2 Online
Preconcentrator Entech 7200 1005 As
Needed
Used Air Lab AIRMS2 Online
Tedlar
Autosampler
Entech 7032A 1017 As
Needed
Used Air Lab AIRMS2 Online
Canister
Autosampler
Entech 7016D 1871 As
Needed
Used Air Lab AIRMS2 Online
Gas
Chromatograph
Agilent 6890 US000011333 As
Needed
Used Air Lab AIRMS3 Online
Injector Agilent G2614A CN40327743 As
Needed
Used Air Lab AIRMS3 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 6890/5973 US00024695
US82311265
As
Needed
Used Air Lab AIRMS4 Online
Preconcentrator Entech 7200 1174 As
Needed
USED Air Lab AIRMS4 Online
Canister
Autosampler
Entech 7016D 1870 As
Needed
Used Air Lab AIRMS4 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 6890/5973 GCUS00039611
MSUS0340681
As
Needed
Used Air Lab AIRMS5 Online
Preconcentrator Entech 7200 1162 As
Needed
Used Air Lab AIRMS5 Online
Canister
Autosampler
Entech 7016D 1741 As
Needed
Used Air Lab AIRMS5 Online
Tedlar
Autosampler
Entech 7032AB 1044 As
Needed
Used Air Lab AIRMS5 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 7890A/5975C GCUS10831022
MSU91732329
As
Needed
Used Air Lab AIRMS6 Online
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Description Manufacturer Model Serial Number Service
Date
Condition Location Internal
ID
Manual
Location
Canister
Autosampler
Entech 7016D 1505 As
Needed
Used Air Lab AIRMS6 Online
Preconcentrator Entech 7200 1322 As
Needed
Used Air Lab AIRMS6 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 6890/5975C US00024616
US71236615
As
Needed
Used Air Lab AIRMS7 Online
Preconcentrator Entech 7200 1720 As
Needed
Used Air Lab AIRMS7 Online
Canister
Autosampler
Entech 7016D 1991 As
Needed
Used Air Lab AIRMS7 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 8890/5977B US2008A003
US2007M007
As
Needed
Used Air Lab AIRMS8 Online
Preconcentrator Entech 7200A 00118 As
Needed
Used Air Lab AIRMS8 Online
Canister
Autosampler
Entech 7016D 1869 As
Needed
Used Air Lab AIRMS8 Online
Canister
Autosampler
Entech 7016D 1828 As
Needed
Used Air Lab AIRMS8 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 8890/5977B US2007A038
US2006M061
As
Needed
Used Air Lab AIRMS9 Online
Preconcentrator Entech 7200A 00117 As
Needed
Used Air Lab AIRMS9 Online
Canister
Autosampler
Entech 7016D 1872 As
Needed
Used Air Lab AIRMS9 Online
Canister
Autosampler
Entech 7016D 1990 As
Needed
Used Air Lab AIRMS9 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 8890/5977B US2209A075
US2201R007
As
Needed
Used Air Lab AIRMS10 Online
Preconcentrator Entech 7200A 00145 As
Needed
Used Air Lab AIRMS10 Online
Canister
Autosampler
Entech 7016D 2000 As
Needed
Used Air Lab AIRMS10 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 8890/5977B US2209A079
US2202R013
As
Needed
Used Air Lab AIRMS11 Online
Preconcentrator Entech 7200A 00146 As
Needed
Used Air Lab AIRMS11 Online
Canister
Autosampler
Entech 7016D 2001 As
Needed
Used Air Lab AIRMS11 Online
Canister
Autosampler
Entech 7016D 2002 As
Needed
Used Air Lab AIRMS11 Online
Canister
Autosampler
Entech 7650-01 0130 As
Needed
Used Air Lab AIRMS11 Online
Precision Diluter Entech 4700 0371 As
Needed
Used Air Lab Online
Dynamic Diluter Entech Model 4600A 1086 As
Needed
Used Air Lab Online
TO Canister Restek/Entec
h
TO-
CAN/SiloniteCan
N/A As
Needed
Used Air Lab 3024 cans
owned
Online
Passive Sampling
Kit
Restek/Entec
h
N/A As
Needed
Used Air Lab 2218
owned
Online
Field hand held
PID
RAE Systems MiniRAE3000 592-929317 As
Needed
Used Air Lab Online
Canister Cleaner Entech 3100A 1178 As
Needed
Used Air Lab Oven 1 Online
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Description Manufacturer Model Serial Number Service
Date
Condition Location Internal
ID
Manual
Location
Oven Entech 3513ENT 1482050570384 As
Needed
Used Air Lab Oven 1 Online
Oven Entech 3513ENT 1482060344515 As
Needed
Used Air Lab Oven 1 Online
Canister Cleaner Entech 3100A 1473 As
Needed
Used Air Lab Oven 2 Online
Oven Entech 3513ENT 1482060344518 As
Needed
Used Air Lab Oven 2 Online
Oven Entech 31-350ER B33ER-01180 As
Needed
Used Air Lab Oven 2 Online
Canister Cleaner Entech 3100A 1448 As
Needed
Used Air Lab Oven 3 Online
Oven Entech 31-350 B33-02663 As
Needed
Used Air Lab Oven 3 Online
Oven Entech 31-350ER B33ER-01142 As
Needed
Used Air Lab Oven 3 Online
Canister Cleaner Entech 3100D 1741 As
Needed
Used Air Lab Oven 4 Online
Oven Entech 31-350ER B33ER-01654 As
Needed
Used Air Lab Oven 4 Online
Oven Entech 31-350ER B33ER-01652 As
Needed
Used Air Lab Oven 4 Online
Canister Cleaner Entech 3100D 2214 As
Needed
Used Air Lab Oven 5 Online
Oven Entech 09-OV6L8 0134 As
Needed
Used Air Lab Oven 5 Online
Oven Entech 09-OV6L8 0135 As
Needed
Used Air Lab Oven 5 Online
Canister Cleaner Entech 3100A 1154 As
Needed
Used Air Lab Oven 6 Online
Oven Entech 3513ENT 1482060344516 As
Needed
Used Air Lab Oven 6 Online
Oven Entech 3513ENT 1003-4123 As
Needed
Used Air Lab Oven 6 Online
Canister Cleaner Entech 3100D 1154 As
Needed
Used Air Lab Oven 7 Online
Oven Entech 09-OV6L12 0212 As
Needed
Used Air Lab Oven 7 Online
Oven Entech 09-OV6L12 0213 As
Needed
Used Air Lab Oven 7 Online
Description Manufacturer Model Serial Number Service
Date
Condition Location Internal
ID
Manual
Location
Analytical
Balance
Mettler XSE 105 Dual
Range
B634906554 Annual Used Aquatic
Tox Lab
002929 Biomon
Class “I” weights
(2)
Troemner SN #67812 67812 Annual Used Aquatic
Tox Lab
000565 UKN
Stereoscope Olympus SZX2-ILLD 7D48897 Annual Used Aquatic
Tox Lab
N/A Biomon
Oven (2)Fisher 655F 30400142 Annual Used Aquatic
Tox Lab
304 UKN
Cold Room Thermo-Kool Walk-In
Refrigerator
49409 Annual Used Aquatic
Tox Lab
1800 UKN
Stir plate Fisher 170 US HHKF65010 Annual Used Aquatic
Tox Lab
N/A Biomon
Stir plate Fisher 120 US HBKF63004 Annual Used Aquatic
Tox Lab
N/A Biomon
Stir plate VWR 151211003 Annual Used Aquatic
Tox Lab
N/A Biomon
Stir plate VWR 97042-626 151211016 Annual Used Aquatic
Tox Lab
N/A Biomon
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Description Manufacturer Model Serial Number Service
Date
Condition Location Internal
ID
Manual
Location
Chlorine meter Hach DR300 19110A002361 Annual Used Aquatic
Tox Lab
P0148 Biomon
Hardness meter Orbeco-
Hellige
942 2444 Annual Used Aquatic
Tox Lab
N/A Biomon
Conductivity
Probe
ZW1-10283 ZW1-10283 Annual Used Aquatic
Tox Lab
N/A Biomon
Hood 4 Labconco 6963401 111151057 12-1-21 Used Micro 2329 Biomon
pH probe Thermo
Scientific
ZY1-18044 ZY1-18044 Annual Used Aquatic
Tox Lab
N/A Biomon
Incubator-I9 Thermo
Scientific
Precision
Annual Used Aquatic
Tox Lab
2355 Biomon
Incubator I8 Thermo
Scientific
Precision
MH400-S 42499233 Annual Used Aquatic
Tox Lab
N/A Biomon
Incubator-I4 Thermo
Scientific
Precision
02010320 Annual Used Aquatic
Tox Lab
N/A Biomon
Stereoscope Olympus SZX2-ILLD
(ESCP0004)
7B49859 Annual Used Aquatic
Tox Lab
P0004 Biomon
pH meter Orion VersaStar X61072 Annual Used Aquatic
Tox Lab
X61072 Biomon
Waterbath 1 Lindberg/Bl
ue
WB1130A X05R-220204-
XE
Annual UKN Aquatic
Tox Lab
000601 N/A
Stereoscope Olympus SZH-ILLD
(ESC125)
711005 Annual Used Aquatic
Tox Lab
N/A Biomon
Stereoscope Olympus SZXz-ILLD 9B49874 Annual Used Aquatic
Tox Lab
Biomon
Waterbath Thermo
Scientific
C1R89 300253242 Annual Used Aquatic
Tox Lab
P0131 UKN
Refrigerator True 63366 909935 Annual UKN Aquatic
Tox Lab
UKN
Water Purifier ELGA Pure
Lab
4LXXXSCM2 ULT00002887 N/A Used Aquatic
Tox Lab
2628 Biomon
Mini fridge Haier HC27SG42RG BS0882E1G00B
KFCH0426
Annual Used Aquatic
Tox Lab
n/A N/A
RDO Probe Thermo
Scientific
Orion
VSTAR-RD 15762 Daily Used Aquatic
Tox Lab
N/A Biomon
Oven (1)Thermoscient
ific
Heratherm
OGS400
41831936 Annual New Aquatic
Tox Lab
2809 Biomon
Freezer Kenmore 198.8130582 P20949206 Annual Used Aquatic
Tox Lab
N/A UKN
Incubator Crown Tonka Walk-In 260333-01 J01 Annual New Aquatic
Tox Lab
N/A Biomon
Description Manufacturer Model Serial
Number
Service Date Condition Location Internal
ID
Manual
Location
Balance - Top
Loading
Mettler
Toledo
PB3002-S 1121462199 See
KanbanFlo
w
Used Metals
Prep
METBAL3 Supervisor's
Office
Balance - Top
Loading
Mettler
Toledo
PB3002-S 1119070828 See
KanbanFlo
w
Used Metals
Prep
METBAL2 Supervisor's
Office
Balance - Top
Loading
Torbal AGN100 701001026 See
KanbanFlo
w
Used Metals
Prep
METBAL5 Supervisor's
Office
Balance - Top
Loading
Mettler
Toledo
PB3002-S 1128150150 See
KanbanFlo
w
Used TCLP METBAL1 Supervisor's
Office
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Description Manufacturer Model Serial
Number
Service Date Condition Location Internal
ID
Manual
Location
Balance - Top
Loading
Mettler
Toledo
XSR1202S C20129128 See
KanbanFlo
w
Used TCLP TCLPBAL
2
Supervisor's
Office
Balance - Top
Loading
Mettler
Toledo
XS40025 B712847753 See
KanbanFlo
w
Used TCLP METBAL4 Supervisor's
Office
Balance - Top
Loading
Mettler
Toledo
XS40025 B410367932 See
KanbanFlo
w
Used Mercury HGBAL1 Supervisor's
Office
Hotblock Environment
al Express
SC154 9062CECW39
53
See
KanbanFlo
w
Used Metals
Prep
MPE Supervisor's
Office
Hotblock Environment
al Express
SC154 2015CECW42
78
See
KanbanFlo
w
Used Metals
Prep
MPF Supervisor's
Office
Hotblock Environment
al Express
SC154 2015CECW43
38
See
KanbanFlo
w
Used Metals
Prep
MPG Supervisor's
Office
Hotblock Environment
al Express
SC154 2018CECW49
65
See
KanbanFlo
w
Used Metals
Prep
MPO Supervisor’s
Office
Hotblock Environment
al Express
SC154 9062CECW39
54
See
KanbanFlo
w
Used Mercury HG1 Supervisor's
Office
Hotblock Environment
al Express
SC154 9062CECW39
56
See
KanbanFlo
w
Used Mercury HG2 Supervisor's
Office
Hotblock Environment
al Express
SC154 3994CEC1880 See
KanbanFlo
w
Used Mercury MPC Supervisor's
Office
Hotblock Environment
al Express
SC154 missing See
KanbanFlo
w
Used Mercury MPD Supervisor's
Office
Hotblock Environment
al Express
SC154 See Kanban
Flow
Used Mercury MPN Supervisor’s
Office
Microwave CEM Mars 5 Xpress MD7441 See
KanbanFlo
w
Used Metals
Prep
MD7441 Supervisor's
Office
Microwave CEM Mars 5 Xpress MD4692 See
KanbanFlo
w
Used Metals
Prep
MD4692 Supervisor's
Office
Microwave CEM Mars 6 MJ2771 See
KanbanFlo
w
Used Metals
Prep
MJ2771 Supervisor's
Office
Microwave CEM Mars 6 MJ9747 See
KanbanFlo
w
Used Metals
Prep
MJ9747 Supervisor's
Office
Microwave CEM Mars 6 MJ9726 See
KanbanFlo
w
Used Metals
Prep
MJ9726 Supervisor's
Office
Centrifuge Thermo
Fisher
Sorvall ST 40 42496720 See
KanbanFlo
w
Used Metals
Prep
N/A Supervisor's
Office
Turbidimeter Hach TL2300 2019060C0080 See
KanbanFlo
w
Used Metals
Prep
N/A Supervisor's
Office
Turbidimeter HACH 2100N 2020060C0093 See
KanbanFlo
w
Used Metals
Prep
N/A Supervisor’s
Office
Water Purifier ELGA Purelab Ultra ULT00002665 See
KanbanFlo
w
Used Metals
Prep
N/A Supervisor's
Office
Mercury Analyzer Leeman Hydra II AA 4049 See
KanbanFlo
w
Used Mercury CVAA 5 Supervisor's
Office
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Description Manufacturer Model Serial
Number
Service Date Condition Location Internal
ID
Manual
Location
Mercury Analyzer Teledyne QuickTrace 7600 US17016008 See
KanbanFlo
w
Used Mercury CVAA 6 Supervisor's
Office
Mercury Analyzer PerkinElmer FIMS 100 101S18111401 See
KanbanFlo
w
Used Mercury CVAA 7 Supervisor's
Office
ICP OES Thermo ICAP 7400 Duo IC74DC14180
1
See
KanbanFlo
w
Used ICP ICP 12 Supervisor's
Office
ICP OES Thermo ICAP 7400 Duo IC74DC14380
4
See
KanbanFlo
w
Used ICP ICP 13 Supervisor's
Office
ICP OES Thermo ICAP 7400 Duo IC74DC15110
3
See
KanbanFlo
w
Used ICP ICP 14 Supervisor's
Office
ICP OES Thermo ICAP 6500 DUO ICP-20074614 Used Metals
Lab
ICP15 Supervisor’s
Office
ICPMS Agilent 7900 G8403A JP16281469 See
KanbanFlo
w
Used ICPMS ICPMS 8 Supervisor's
Office
ICPMS Agilent (1) 7900
G8403A
JP14400452 See
KanbanFlo
w
Used ICPMS ICPMS 9 Supervisor's
Office
ICPMS Agilent 7900 G8403A JP14080164 See
KanbanFlo
w
Used ICPMS ICPMS 10 Supervisor's
Office
ICPMS Agilent 7900 G8403A JP17472096 See
KanbanFlo
w
Used ICPMS ICPMS 11 Supervisor's
Office
Refrigerator Maxx Cold MXM2-48RBHC 36031 Used TCLP P0136 On Line
TCLP Freezer Danby
Designer
DUFM043A1WDD 4315093419531 See
KanbanFlo
w
Used TCLP Missing Supervisor’s
Office
Stirrer/Hot Plate Thermo Cinarec+C301001311514
115
See
KanbanFlo
w
Used TCLP 1 Supervisor's
Office
Stirrer/Hot Plate IKA RT15 3.492224 See
KanbanFlo
w
Used TCLP 2 Supervisor's
Office
Stirrer/Hot Plate IKA RT15 3.503438 See
KanbanFlo
w
Used TCLP 3 Supervisor's
Office
Stirrer/Hot Plate IKA RT15 3.503438 See
KanbanFlo
w
Used TCLP 4 Supervisor's
Office
Stirrer/Hot Plate IKA RT15 3.527246 See
KanbanFlo
w
Used TCLP 5 Supervisor's
Office
Tumbler Environment
al Express
12 Position N/A See
KanbanFlo
w
Used TCLP A Supervisor's
Office
Tumbler Environment
al Express
12 Position N/A See
KanbanFlo
w
Used TCLP E Supervisor's
Office
Tumbler Environment
al Express
12 Position N/A See
KanbanFlo
w
Used TCLP I Supervisor's
Office
Tumbler Environment
al Express
12 Position N/A See
KanbanFlo
w
Used TCLP L Supervisor's
Office
Tumbler Environment
al Express
12 Position N/A See
KanbanFlo
w
Used TCLP O Supervisor's
Office
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Description Manufacturer Model Serial
Number
Service Date Condition Location Internal
ID
Manual
Location
Tumbler Environment
al Express
12 Position N/A See
KanbanFlo
w
Used TCLP S Supervisor's
Office
Tumbler Environment
al Express
12 Position N/A See
KanbanFlo
w
Used TCLP 1 Supervisor's
Office
Tumbler Environment
al Express
12 Position N/A See
KanbanFlo
w
Used TCLP 2 Supervisor's
Office
Tumbler Environment
al Express
12 Position N/A See
KanbanFlo
w
Used TCLP G Supervisor's
Office
Tumbler Environment
al Express
12 Position N/A See
KanbanFlo
w
Used TCLP H Supervisor's
Office
Tumbler Environment
al Express
12 Position N/A See
KanbanFlo
w
Used TCLP R Supervisor's
Office
Tumbler Environment
al Express
12 Position N/A See
KanbanFlo
w
Used TCLP B Supervisor's
Office
pH Meter Thermo OrionVerastar V04967 See
KanbanFlo
w
Used TCLP V04967 Supervisor's
Office
pH Meter Thermo OrionVerastarPro V11227 See
KanbanFlo
w
Used TCLP V11227 Supervisor's
Office
pH meter Thermo Orion VersastarPro V13429 See
KanbanFlo
w
Used TCLP V13429 Supervisor's
Office
Description Manufacturer Model Serial Number Service
Date
Condition Location Internal
ID
Manual
Location
Analytical
Balance
Mettler
Toledo
XSE1050DU B634906554 Annual New Microbiology
Lab
002929 Biomon
Class “I” weights (1 set)
Troemner
000565 Annual New Microbiology
Lab
N/A UKN
Autoclave Barstead Harvey 1277061222472 Annual New Microbiology
Lab
1708 Biomon
Water Bath Themo
Scientific
Precision CIR89 300380862 Annual Used Microbiology
Lab
UKN
Quantitray Sealer IDEXX 2X QTP13172302569 Monthly Used Microbiology
Lab
2803 Biomon
Incubator I10 Thermo
Scientific
Precision
PR505755L 300303584 Annual Used Microbiology
Lab
30T8 Biomon
Colony Counter Quebecor 3325 222649 N/A Microbiology
Lab
Stereoscope Olympus SZXZ-ILLD 9B48439 Annual Used Microbiology
Lab
P0125 Biomon
UV light; short
and long wave
Entela UVP-56 F122708 Quarterl
y
Used Microbiology
Lab
F122708 Biomon
Autoclave SterileMax Harvey 1277061222472 Annual Used Microbiology
Lab
1708 Biomon
pH meter/
Conductivity
meter/LDO
Thermo
Scientific
Orion
VStar pro V16919 Annual New Aquatic Tox
Lab
V16919 Biomon
Incubator I7-2 Thermo
Scintific
IGS100 42408345 Annual Used Aquatic Tox
Lab
P0141 Biomon
Incubator I7-1 Thermo
Scintific
IGS100 42408448 Annual New Aquatic Tox
Lab
P0132 Biomon
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Description Manufacturer Model Serial Number Service
Date
Condition Location Internal
ID
Manual
Location
Analytical
Balance
Mettler PL602-S 1125081657 Annual Unk Bacteriology
Lab
N/A Mold Lab
cabinet
Autoclave Tuttnauer 2540EK 2906170 Annual New Bacteriology
Lab
N/A Mold Lab
cabinet
Biolog
MicroStation
Biolog, Inc. Microlog 3 203222 Annual New Bacteriology
Lab
1676 Mold Lab
cabinet
BOD Skalar 2000 Skalar 2000 8123 Annual New BOD 1931 Mold Lab
cabinet
Class I BSC AirFiltronix AirFiltronix HS
4500
41031 Annual New Mold Lab 1505 Mold Lab
cabinet
Class II BSC Labconco Labconco 36209 30706555 Annual USed Bacteriology
Lab
1374 Mold Lab
cabinet
Class II BSC Labconco Labconco 36213 60554894 Annual USed Mold Lab N/A Mold Lab
cabinet
COD Reactor HACH 45600 900903221 N/A New BOD N/A Mold Lab
cabinet
YSI ProOBOD
LDS Probe
YSI 21C103980 N/A New BOD N/A Mold Lab
cabinet
YSI ProOBOD
LDS Probe
YSI 21C103978 N/A New BOD N/A Mold Lab
cabinet
YSI ProOBOD
LDS Probe
YSI 21G103335 N/A New BOD N/A Mold Lab
cabinet
Fisher Scientific
Vortex(q?)
Fisher
Scientific
80109016 N/A New Mold N/A No
Incubator Precision
Scientific
30M 309100 N/A New Bacteriology
Lab
1826 Mold lab
cabinet
Incubator Precision
Scientific
ER505755R 300245487 N/A New BOD P0127 Mold lab
cabinet
Incubator Thermo
Scientific
Precision
3721 233089-3323 N/A New BOD 2617 Mold Lab
cabinet
Incubator SHEL-LAB SR120P 09000719 N/A New BOD 3079 BOD lab
Incubator SHEL-LAB SR120P 09000819 N/A New BOD 3079 BOD Lab
Incubator SHEL-LAB SR120P 11003819 N/A New BOD N/A BOD Lab
Incubator VWR 2030 1000499 N/A New BOD 0902 Mold Lab
cabinet
Incubator Quincy Lab 10-100 I11-2454 N/A New Mold Lab N/A Mold lab
cabinet
Incubator Thermo
Precision
PR505755R 300207736 N/A New Mold Lab P0092 Mold lab
cabinet
Microscope NIKON LABOPHOT 230064 Annual Used Mold Lab N/A UKN
Microscope NIKON LABOPHOT 235267 Annual Used Mold Lab N/A UKN
Microscope Olympus CH2 9G0216 Annual Used Mold Lab N/a UKN
Microscope Olympus BH-2 200733 Annual Used Mold Lab 1597 UKN
Microscope Leitz Laborlux 512663 Annual Used Mold Lab N/A UKN
pH meter Thermo
Scientific
Orion Star A211 X59095 N/A New BOD N/A BOD lab
Refrigerator Frigidaire FRT17G4BW9 BA703033306 N/A NEW Mold Lab N/A UKN
Refrigerator Whirlpool EL88TRRWS03 442001106 N/A New Mold Lab N/A UKN
Refrigerator Whirlpool EL7ATRRMQ07 EWR4973976 N/A New Mold Lab N/A UKN
Refrigerator Whirlpool EL05PPXMQ EEP3524864 N/A NEW Bacteriology
Lab
N/A UKN
Spectrophotomet
er
Hach DR900 192180001065 N/A New BOD N/A BOD
Stereoscope VWR
Scientific
VWRS1 V168430 Annual Used Mold Lab N/A Mold lab
cabinet
Stir Plate VWR DYLA-DUAL 120202001 N/A New Bacteriology
Lab
N/A UKN
Stir Plate IKA Big Squid 102 N/A New Bacteriology
Lab
N/A UKN
Stir Plate VWR 7x7 AL4
HOT/STIR
180605003 N/A New BOD N/A UKN
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Description Manufacturer Model Serial Number Service
Date
Condition Location Internal
ID
Manual
Location
Stir Plate VWR 205 7852 N/A New BOD N/A UKN
Turbidimeter Biolog, Inc.21907 06093898 Annual New Bacteriology
Lab
N/A Mold lab
cabinet
Vortex Genie2
Mixer
VWR G-560 2-223236 N/A New Bacteriology
Lab
N/A UKN
Waterbath Fisher Sci FSGPD20 300302839 N/A New Bacteriology
Lab
N/A Mold lab
cabinet
Waterbath Precision Circulating 260 21-AJ11 N/A New BOD N/A Mold lab
cabinet
Description Manufacturer Model Serial Number Service
Date
Condition Location Internal
ID
Manual
Location
Flow control
valve
Plast-o-matic FC050B SA55CXFJN352 Semi-
annual
New Protozoan
Lab
N/A UKN
Centrifugal pump Jabsco 18610-0271 0562309-MA Semi-
annual
Unk Protozoan
Lab
N/A Crypto
Lab
Graduated
container
Nalgene 20 Liter Carboy N/A Semi-
annual
New Protozoan
Lab
N/A UKN
Laboratory
shaker
Lab-Line 3587-4 0105-2679 Annual New Protozoan
Lab
N/A Crypto
Lab
Laboratory
shaker side arms
Lab-Line 3589 0105-2679 Annual New Protozoan
Lab
N/A Crypto
Lab
1500 XG swinging
bucket centrifuge
Damon/IEC
Division
CRU-5000 23453388 Annual Unk Protozoan
Lab
1863 Crypto
Lab
1500 XG swinging
bucket centrifuge
Damon/IEC
Division
CRU-5000 23453744 Annual Unk Protozoan
Lab
1863 Crypto
Lab
1500 XG swinging
bucket centrifuge
Damon/IEC
Division
CRU-5000 2345497 annual unk Protozoan
Lab
1863 Crypto
Lab
Sample
mixer/rotator
DYNAL Car#: 947.01 1004-3765 Annual Unk Protozoan
Lab
RT1 UKN
Magnetic Particle
Concentrator
DYNAL MPC-1 N/A N/A Protozoan
Lab
N/A UKN
Magnetic Particle
Concentrator
DYNAL MPC-S N/A N/A Protozoan
Lab
N/A UKN
Magnetic Particle
Concentrator
DYNAL MPC-6 N/A N/A Protozoan
Lab
N/A UKN
Flat-sided sample
tubes
DYNAL Cat#: 740.03 74003 N/A New Protozoan
Lab
N/A UKN
Epifluorescence/
differential
interference
contract
microscope
Olympus BX-40 9E09944 Annual Protozoan
Lab
1554 Crypto
Lab
Excitation/ band
pass microscope
for fluorescein
isothiocyanate
(FTIC)
C-squared UN3100 023355 Annual Protozoan
Lab
1924 Crypto
Lab
Excitation/ band
pass filters for
4’6-diamidino-2-
phenylindole
(DAPI)
C-squared UN41001 8H2122 Annual Protozoan
Lab
N/A Crypto
Lab
Masterflex pump Cole Parmer 7553-50 Protozoan
Lab
Crypto
Lab
Balance Denver
Instrument
MXX-412 19053216 Annual Protozoan
Lab
Crypto
Lab
Biosafety Cabinet Labconco Cat#: 36208043726 050J372 Annual Protozoan
Lab
1557 Crypto
Lab
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Description Manufacturer Model Serial Number Service
Date
Condition Location Internal
ID
Manual
Location
Gas
Chromatograph 2
HP 6890 HP 6890 US00004397 As needed Used SVOC svcompa
Online
Gas
Chromatograph 3
Agilent 6890 Agilent 6890 US00002051 As needed Used SVOC svcompo
Online
Gas
Chromatograph 7
Agilent 6890 Agilent 6890 US10350064 As needed Used SVOC Svcompe
Online
Gas
Chromatograph 8
Agilent 6890 Agilent 6890 DE00022534 As needed Used SVOC svcompp Online
Gas
Chromatograph 9
HP 6890 HP 6890 US00029095 As needed Used SVOC Svcompj
Online
Gas
Chromatograph
10
Agilent 6890 Agilent 6890 US00039655 As needed Used SVOC Scvompk
Online
Gas
Chromatograph
11
Agilent 6890 Agilent 6890 US00040550 As needed Used SVOC Svcompn
Online
Gas
Chromatograph
12
Agilent 6890 Agilent 6890 US00034155 As needed Used SVOC Svcompaf
Online
Gas
Chromatograph
13
HP 6890 HP 6890 US00010364 As needed Used SVOC Svcomps
Online
Gas
Chromatograph
14
HP 6890 HP 6890 US00020581 As needed Used SVOC svcompt
Online
Gas
Chromatograph
16
Agilent 6890 Agilent 6890 US10212071 As needed Used SVOC Svcompv
Online
Gas
Chromatograph
17
Agilent 6890 Agilent 6890 US10344078 As needed Used SVOC Svcompw
Online
Gas
Chromatograph
18
Agilent 6890 Agilent 6890 US10351038 As needed Used SVOC Svcompd
Online
Gas
Chromatograph
19
Agilent 6890 Agilent 6890 CN10516070 As needed Used SVOC Svompaa
Online
Gas
Chromatograph
20
Agilent 6890 Agilent 6890 CN10543031 As needed Used SVOC Svcompa
b Online
Gas
Chromatograph
21
Agilent 7890 Agilent 7890 CN10730070 As needed Used SVOC Svcompa
e Online
Gas
Chromatograph
22
Agilent 7890 Agilent 7890 CN10730081 As needed Used SVOC svcompa
d Online
Gas
Chromatograph
23
Agilent 6890 Agilent 6890 CN92174366 As needed Used SVOC Svcompa
g Online
Gas
Chromatograph
24
Agilent 6890 Agilent 6890 CN92174369 As needed Used SVOC Svcompa
h Online
Gas
Chromatograph
25
Agilent 7890 Agilent 7890 CN10091009 As needed Used SVOC Svcompaj
Online
Gas
Chromatograph
26
Agilent 7890 Agilent 7890 CN11501138 As needed Used SVOC Svcompar
Online
Gas
Chromatograph
27
Agilent 7890 Agilent 7890 CN11501139 As needed Used SVOC Svcompas
Online
Gas
Chromatograph
28
Agilent 7890 Agilent 7890 US11521018 As needed Used SVOC Svcompat
Online
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Gas
Chromatograph
29
Agilent 7890 Agilent 7890 CN11521077 As needed Used SVOC Svcompa
u Online
Gas
Chromatograph
30
Agilent 7890 Agilent 7890 US11521020 As needed Used SVOC Svcompa
v Online
Gas
Chromatograph
31
Agilent 7890 Agilent 7890 CN13503096 As needed Used SVOC Svcompb
a Online
Gas
Chromatograph
32
Agilent 7890 Agilent 7890 CN14423060 As needed Used SVOC Svcompb
c Online
Gas
Chromatograph
33
Agilent 7890 Agilent 7890 CN15033026 As needed Used SVOC Svcompb
d Online
Gas
Chromatograph
34
Agilent 7890 Agilent 7890 CN15033027 As needed Used SVOC svcompb
e Online
Gas
Chromatograph
35
Agilent 7890 Agilent 7890 US10838014 As needed Used SVOC svcompb
h Online
Gas
Chromatograph
36
Agilent 7890 Agilent 7890 US10205134 As needed Used SVOC svcompbi
Online
Gas
Chromatograph
38
Agilent 7890 Agilent 7890 US10142052 As needed Used SVOC svcompb
k Online
Gas
Chromatograph
41
Agilent 7890 Agilent 7890 CN16123059 As needed Used SVOC svcompb
m Online
Gas
Chromatograph
42
Agilent 7890 Agilent 7890 US1952A007 As needed Used SVOC svcompb
p Online
Gas
Chromatograph
43
Agilent 7890 Agilent 7890 US1951A023 As needed Used SVOC svcompb
q Online
Gas
Chromatograph
45
Agilent 8890 Agilent 8890 US2016A022 As needed Used SVOC svcompb
x Online
Gas
Chromatograph
46
Agilent 7890 Agilent 7890 CN13443001 As needed Used SVOC svcompb
y Online
Gas
Chromatograph
47
Agilent 7890 Agilent 7890 CN10301152 As needed Used SVOC svcompb
z Online
Gas
Chromatograph
48
Agilent 6890 Agilent 6890 CN10344042 As needed Used SVOC svcompca
Online
Gas
Chromatograph
49
Agilent 7890 Agilent 7890 CN10814061 As needed Used SVOC svcompc
b Online
Gas
Chromatograph
50
Agilent 8890 Agilent 8890 US2119A057 As needed Used SVOC svcompcc
Online
Gas
Chromatograph
Detectors 2
FID Detector FID Detector N/A As needed Used SVOC scvompa
Online
Gas
Chromatograph
Detectors 3
NPD/NPD
Detectors
NPD/NPD
Detectors
N/A As needed Used SVOC Svcompo
Online
Gas
Chromatograph
Detectors 7
FID Detector FID Detector N/A As needed Used SVOC Svcompe
Online
Gas
Chromatograph
Detectors 8
FID Detector FID Detector N/A As needed Used SVOC Svcompp
Online
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Gas
Chromatograph
Detectors 9
FID Detector FID Detector N/A As needed Used SVOC Svcompj
Online
Gas
Chromatograph
Detectors 10
FID Detector FID Detector N/A As needed Used SVOC Svcompk
Online
Gas
Chromatograph
Detectors 11
ECD/ECD
Detectors
ECD/ECD
Detectors
F) U11750
B) U12481
As needed Used SVOC svcompn
Online
Gas
Chromatograph
Detectors 12
FPD/FPD
Detectors
FPD/FPD
Detectors
N/A As needed Used SVOC Svcompaf
Online
Gas
Chromatograph
Detectors 13
Detectors Detectors N/A As needed Used SVOC Svcomps
Online
Gas
Chromatograph
Detectors 14
ECD/ECD
Detectors
ECD/ECD
Detectors
F) U3113
B) U2620
As needed Used SVOC Svcompt
Online
Gas
Chromatograph
Detectors 16
FID Detector FID Detector N/A As needed Used SVOC Svcompv
Online
Gas
Chromatograph
Detectors 17
FID Detector FID Detector N/A As needed Used SVOC Svcompw
Online
Gas
Chromatograph
Detectors 18
ECD/ECD
Detectors
ECD/ECD
Detectors
F) U11613
B) U13988
As needed Used SVOC Svcompd
Online
Gas
Chromatograph
Detectors 19
ECD/ECD
Detectors
ECD/ECD
Detectors
F) U6632
B) U8422
As needed Used SVOC Svcompa
a Online
Gas
Chromatograph
Detectors 20
ECD/ECD
Detectors
ECD/ECD
Detectors
F) U13989
B) U0418
As needed Used SVOC Svcompa
b Online
Gas
Chromatograph
Detectors 21
FID Detector FID Detector N/A As needed Used SVOC Svcompa
e Online
Gas
Chromatograph
Detectors 22
ECD/ECD
Detectors
ECD/ECD
Detectors
F) U12039
B) 12038
As needed Used SVOC Svcompa
d Online
Gas
Chromatograph
Detectors 23
ECD/ECD
Detectors
ECD/ECD
Detectors
F) U2621
B) U8104
As needed Used SVOC Svcompa
g Online
Gas
Chromatograph
Detectors 24
ECD/ECD
Detectors
ECD/ECD
Detectors
F) U8423
B) U12482
As needed Used SVOC Svcompa
h Online
Gas
Chromatograph
Detectors 25
FID Detector FID Detector N/A As needed Used SVOC Svcompaj
Online
Gas
Chromatograph
Detectors 26
FID Detector FID Detector N/A As needed Used SVOC Svcompar
Online
Gas
Chromatograph
Detectors 27
FID Detector FID Detector N/A As needed Used SVOC Svcompas
Online
Gas
Chromatograph
Detectors 28
ECD/ECD
Detectors
ECD/ECD
Detectors
F) U26768
B) U26237
As needed Used SVOC Svcompat
Online
Gas
Chromatograph
Detectors 29au
ECD/ECD
Detectors
ECD/ECD
Detectors
F) U20277
B) U20299
As needed Used SVOC Svcompa
u Online
Gas
Chromatograph
Detectors 30
ECD/ECD
Detectors
ECD/ECD
Detectors
F) U20425
B) U20424
As needed Used SVOC Svcompa
v Online
Gas
Chromatograph
Detectors 31
FID Detector FID Detector N/A As needed Used SVOC Svcompb
a Online
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Gas
Chromatograph
Detectors 32
FID Detector FID Detector N/A As needed Used SVOC Svcompb
c Online
Gas
Chromatograph
Detectors 33
FID Detector FID Detector N/A As needed Used SVOC Svcompb
d Online
Gas
Chromatograph
Detectors 34
FID Detector FID Detector N/A As needed Used SVOC Svcompb
e Online
Gas
Chromatograph
Detectors 35
FID Detector FID Detector N/A As needed Used SVOC Svcompb
h Online
Gas
Chromatograph
Detectors 36
FID Detector FID Detector N/A As needed Used SVOC Svcompbi
Online
Gas
Chromatograph
Detectors 38
ECD/ECD
Detectors
ECD/ECD
Detectors
F) U14736
B) U16284
As needed Used SVOC Svcompb
k Online
Gas
Chromatograph
Detectors 41
NPD/NPD
Detectors
NPD/NPD
Detectors
N/A As needed Used SVOC Svcompb
p Online
Gas
Chromatograph
Detectors 42
ECD/ECD
Detectors
ECD/ECD
Detectors
F) U37659
B) U37661
As needed Used SVOC Svcompb
p Online
Gas
Chromatograph
Detectors 43
FID Detector FID Detector N/A As needed Used SVOC Svcompb
q Online
Gas
Chromatograph
Detectors 45
FID Detector FID Detector N/A As needed Used SVOC Svcompb
x Online
Gas
Chromatograph
Detectors 46
ECD/ECD
Detectors
ECD/ECD
Detectors
F) U39219
B) U39356
As needed Used SVOC Svcompb
y Online
Gas
Chromatograph
Detectors 47
FID Detector FID Detector N/A As needed Used SVOC Svcompb
z Online
Gas
Chromatograph
Detectors 48
FID Detector FID Detector N/A As needed Used SVOC Svcompc
a Online
Gas
Chromatograph
Detectors 49
FPD/FPD
Detectors
FPD/FPD
Detectors
N/A As needed Used SVOC Svcompc
b Online
Gas
Chromatograph
Detectors 50
FID Detector FID Detector N/A As needed Used SVOC Svcompc
c Online
Gas
Chromatograph/
Mass
Spectrometer 1
Agilent
6890GC
5973 MSD
Agilent 6890GC
5973 MSD
GC CN10335001
MS US33220022
As needed Used SVOC Svcompf
Online
Gas
Chromatograph/
Mass
Spectrometer 2
Agilent
6890GC
5973 MSD
Agilent 6890GC
5973 MSD
GC US10409048
MS US35120400
As needed Used SVOC Svcompc
Online
Gas
Chromatograph/
Mass
Spectrometer 4
Agilent
6890GC
5973 MSD
Agilent 6890GC
5973 MSD
GC CN10403067
MS US35120308
As needed Used SVOC Svcomph
Online
Gas
Chromatograph/
Mass
Spectrometer 7
Agilent
6890GC
5973 MSD
Agilent 6890GC
5973 MSD
GC US00023180
MS US03940745
As needed Used SVOC svcompm
Online
Gas
Chromatograph/
Mass
Spectrometer 9
Agilent
6890GC
5973 MSD
Agilent 6890GC
5973 MSD
GC CN10344042
MS US33220158
As needed Used SVOC Svcompx Decomm
issioned
and
repurpos
ed as
SVGC48
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Gas
Chromatograph/
Mass
Spectrometer 10
Agilent
6890GC
5973 MSD
Agilent 6890GC
5973 MSD
GC CN10340045
MS US33220183
As needed Used SVOC Svcompy
Online
Gas
Chromatograph/
Mass
Spectrometer 11
Agilent
6890GC
5975 MSD
Agilent 6890GC
5975 MSD
GC CN10509031
MS US60532657
As needed Used SVOC Svcompa
c Online
Gas
Chromatograph/
Mass
Spectrometer 12
Agilent
7890GC
5975 MSD
Agilent 7890GC
5975 MSD
GC CN10728074
MS 12-0706-1325
As needed Used SVOC Svcompai
Online
Gas
Chromatograph/
Mass
Spectrometer 13
Agilent
7890GC
5975 MSD
Agilent 7890GC
5975 MSD
GC CN10301081
MS US10313621
As needed Used SVOC Svcompa
k Online
Gas
Chromatograph/
Mass
Spectrometer 14
Agilent
7890GC
5975 MSD
Agilent 7890GC
5975 MSD
GC CN11031022
MS US11093726
As needed Used SVOC Svcompal
Online
Gas
Chromatograph/
Mass
Spectrometer 15
Agilent
7890GC
5975 MSD
Agilent 7890GC
5975 MSD
GC CN10301081
MS US10313621
As needed Used SVOC Svcompa
m Online
Gas
Chromatograph/
Mass
Spectrometer 16
Agilent
7890GC
5975 MSD
Agilent 7890GC
5975 MSD
GC CN10301152
MS US10313616
As needed Used SVOC Svcompa
n
Decomm
issioned
and
repurpos
ed as
SVGC47
Gas
Chromatograph/
Mass
Spectrometer 17
Agilent
7890GC
5975 MSD
Agilent 7890GC
5975 MSD
GC CN11191064
MS US11363807
As needed Used SVOC Svcompa
o Online
Gas
Chromatograph/
Mass
Spectrometer 18
Agilent
7890GC
5975 MSD
Agilent 7890GC
5975 MSD
GC CN11401093
MS US11403903
As needed Used SVOC Svcompa
p Online
Gas
Chromatograph/
Mass
Spectrometer 19
Agilent
7890GC
5975 MSD
Agilent 7890GC
5975 MSD
GC CN 11391051
MS US11383838
As needed Used SVOC Svcompa
q Online
Gas
Chromatograph/
Mass
Spectrometer 20
Agilent
7890GC
5975 MSD
Agilent 7890GC
5975 MSD
GC CN12031161
MS US11503941
As needed Used SVOC Svcompa
w Online
Gas
Chromatograph/
Mass
Spectrometer 21
Agilent
7890GC
5975 MSD
Agilent 7890GC
5975 MSD
GC CN12031160
MS US11513903
As needed Used SVOC Svcompa
x Online
Gas
Chromatograph/
Mass
Spectrometer 22
Agilent
7890GC
5975 MSD
Agilent 7890GC
5975 MSD
GC CN11521157
MS US12023909
As needed Used SVOC Svcompa
y Online
Gas
Chromatograph/
Mass
Spectrometer 23
Agilent
7890GC
5975 MSD
Agilent 7890GC
5975 MSD
GC CN12031114
MS US11433926
As needed Used SVOC Svcompa
z Online
Gas
Chromatograph/
Mass
Spectrometer 24
Agilent
7890GC
5977 MSD
Agilent 7890GC
5977 MSD
GC CN14163165
MS US92043581
As needed Used SVOC Svcompb
b Online
Gas
Chromatograph/
Mass
Spectrometer 25
Agilent
7890GC
5975 MSD
Agilent 7890GC
5975 MSD
GC CN10906031
MS US11343905
As needed Used SVOC Svcompbf
Online
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Gas
Chromatograph/
Mass
Spectrometer 26
Agilent
7890GC
5975 MSD
Agilent 7890GC
5975 MSD
GC CN10021075
MS US10143111
As needed Used SVOC Svcompbl Online
Gas
Chromatograph/
Mass
Spectrometer
(QQQ) 27
Agilent
7890GC
7010 MSD
(QQQ)
Agilent 7890GC
7010 MSD (QQQ)
GC US18373018
MS US1730V003
As needed Used SVOC Svcompb
n
Transferr
ed to
IDEA
Lab.
Gas
Chromatograph/
Mass
Spectrometer 28
Agilent
7890GC
5977 MSD
Agilent 7890GC
5977 MSD
GC CN13483185
MS US1349M227
As needed Used SVOC Svcompb
o
Online
Gas
Chromatograph/
Mass
Spectrometer 29
Agilent
8890GC
5977 MSD
Agilent 8890GC
5977 MSD
GC US1951A019
MS US1952M030
As needed Used SVOC Svcompbr Online
Gas
Chromatograph/
Mass
Spectrometer 30
Agilent
8890GC
5977 MSD
Agilent 8890GC
5977 MSD
GC US1947A006
MS US2040M022
As needed Used SVOC Svcompb
s
Online
Gas
Chromatograph/
Mass
Spectrometer 31
Agilent
8890GC
5977 MSD
Agilent 8890GC
5977 MSD
GC US2014A033
MS US2041M031
As needed Used SVOC Svcompb
u
Online
Gas
Chromatograph/
Mass
Spectrometer 32
Agilent
8890GC
5977 MSD
Agilent 8890GC
5977 MSD
GC US2016A007
MS US2041M015
As needed Used SVOC Svcompb
v
Online
Gas
Chromatograph/
Mass
Spectrometer 33
Agilent
8890GC
5977 MSD
Agilent 8890GC
5977 MSD
GC US2014A035
MS US2040M015
As needed Used SVOC Svcompb
w
Online
Liquid
Chromatograph/
Mass
Spectrometer
(QQQ)
LCMSMS1
Agilent
1290/1290/
1290LC
6470 MSD
(QQQ)
Agilent 1290LC
6470 MSD (QQQ)
Multisampler
DEBAS01954
MS/MS
SG1846G104
Pump
DEBA202992
MCT
DEBA404366
As needed Used SVOC LCMSMS
1
Online
Liquid
Chromatograph/
Mass
Spectrometer
(QQQ)
LCMSMS2
Agilent
1260/1200/
1200LC
6460 MSD
(QQQ)
Agilent 1260/1200/
1200LC
6460 MSD (QQQ)
Multisampler
DEAAC40230
MS/MS
SG11477210
Pump
DEAB715448
TCC
DEACN42876
As needed Used SVOC LCMSMS
2
In
develop
ment
High
Performance
Liquid
Chromatography
(HPLC1)
Agilent 1100
Series
DAD/FLD
Agilent 1100 Series
DAD/FLD
DAD de01608402
FLD de23904489
As needed Used SVOC Hplc1
Online
High
Performance
Liquid
Chromatography
(HPLC2)
Agilent 1100
Series
DAD/FLD
Agilent 1100 Series
DAD/FLD
DAD de30518420
FLD de92001880
As needed Used SVOC Hplc2
Online
High
Performance
Liquid
Chromatography
Agilent 1100
Series
DAD
Agilent 1100 Series
DAD
DAD us64400711 As needed Used SVOC Hplc3
Online
High
Performance
Liquid
Chromatography
Agilent 1100
Series
DAD
Agilent 1100 Series
DAD
DAD de43623013 As needed Used SVOC Hplc4 Online
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Analytical
Balance
Mettler-
Toledo XS204
1122411619 As needed Used Ext. Lab Book
shelf
Automated
Soxhlet
Gerhardt
Soxtherm
2951 As needed Used Ext. Lab #1 In lab on
shelf next
to
instrume
nt
Automated
Soxhlet
Gerhardt
Soxtherm
2952 As needed Used Ext. Lab #2 In lab on
shelf next
to
instrume
nt
Automated
Soxhlet
Gerhardt
Soxtherm
2953 As needed Used Ext. Lab #3 In lab on
shelf next
to
instrume
nt
Automated
Soxhlet
Gerhardt
Soxtherm
2954 As needed Used Ext. Lab #4 In lab on
shelf next
to
instrume
nt
Centrifuge Sorvall ST-41 2225 As needed Used Ext. Lab Book
shelf in
lab
Centrifuge Sorvall ST-41 2227 As needed Used Ext. Lab Book
shelf in
lab
Microwave CEM MARS
6
MJ2518 As needed Used Ext. Lab #3 Book
shelf in
lab
Microwave CEM MARS
6
MJ6367 As needed Used Ext. Lab #4 Book
shelf in
lab
Microwave CEM MARS
6
MJZ868 As needed Used Ext. Lab #2 Book
shelf in
lab
Microwave CEM MARS
6
MARS 6 MY2163 As needed New Ext. Lab #5 Book
shelf in
lab
Microwave CEM MARS
6
MARS 6 MY2132 As needed New Ext. Lab #6 Book
shelf in
lab
O&G Solvent
Evaporator
Horizon
Speed-Vap
III
04-2020 As needed Used Ext. Lab #1 Book
shelf in
lab
O&G Solvent
Evaporator
Horizon
Speed-Vap
III
03-1001 As needed Used Ext. Lab #3 Book
shelf in
lab
O&G Solvent
Evaporator
Horizon
Speed-Vap IV
15-0055 As needed Used Ext. Lab #4 Book
shelf in
lab
O&G Solvent
Evaporator
Horizon
Speed-Vap IV
15-0056 As needed Used Ext. Lab #2 Book
shelf in
lab
O&G SPE
Extractor
Horizon
SPE-DEX
3100
15-0113 As needed Used Ext. Lab Disk in
lab
O&G SPE
Extractor
Horizon
SPE-DEX
3100
15-0116 As needed Used Ext. Lab Disk in
lab
O&G SPE
Extractor
Horizon
SPE-DEX
3100
15-0117 As needed Used Ext. Lab Disk in
lab
O&G SPE
Extractor
Horizon
SPE-DEX
3100
15-0118 As needed Used Ext. Lab Disk in
lab
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Oven Fisher 00700127 As needed Used Ext. Lab Bookshel
f in lab
Oven Fisher 1000594
F210266022FD
As needed Used Ext. Lab Bookshel
f in lab
Ring & Puck Mill SPEX
ShatterBOX
8530
10191 As needed Used Ext. Lab Bookshel
f in lab
Sonicator Qsonica Q700 92183M-16-16 As needed Used Ext. Lab Bookshel
f in lab
Sonicator Qsonica Q700 92186M-10-16 As needed Used Ext. Lab Bookshelf
in lab
Sonicator Qsonica Q700 92189M-10-16 As needed Used Ext. Lab Bookshelf
in lab
Sonicator Qsonica Q700 9219M-10-16 As needed Used Ext. Lab Bookshelf
in lab
Sonicator Qsonica Q700 Q700 120131U-05-21 As needed New Ext. Lab #5 Bookshelf
in lab
Sonicator Qsonica Q700 Q700 120137U-05-21 As needed New Ext. Lab #6 Bookshelf
in lab
Water Bath ThermoScien
tific
2033602-102 As needed Used Ext. Lab Bookshelf
in lab
Water Bath Gant VH1535002 As needed Used EXT. Lab Bookshelf
Microwave CEM MARS
Xpress
MD2861 As needed New EXT. Lab #1 Decommi
ssioned
Centrifuge Sorvall ST-41 42498357 As needed Used EXT. Lab Bookshelf
Concentrator Buchi Buchi Syncore
Plus
1100082324 As needed New EXT. Lab #1 Bookshelf
Concentrator Buchi Buchi Syncore
Plus
1100082473 As needed New EXT. Lab #2 Bookshelf
Concentrator Buchi Buchi Syncore
Plus
1100084062 As needed New EXT. Lab #3 Bookshelf
Concentrator Buchi Buchi Syncore
Plus
1100084063 As needed New EXT. Lab #4 Bookshelf
Concentrator XcelVap Horizon
Technologies
17-5548 As needed Used EXT. Lab On Disc
in Lab
Concentrator XcelVap Horizon
Technologies
19-5688 As needed Used EXT. Lab On Disc
in Lab
Concentrator XcelVap Horizon
Technologies
17-5564 As needed Used EXT. Lab On Disc
in Lab
Concentrator XcelVap Horizon
Technologies
17-5686 As needed Used EXT. Lab On Disc
in Lab
Concentrator XcelVap Horizon
Technologies
19-5687 As needed Used EXT. Lab On Disc
in Lab
Concentrator XcelVap Horizon
Technologies
17-5549 As needed Used EXT. Lab On Disc
in Lab
Concentrator XcelVap Horizon
Technologies
17-5541 As needed Used EXT. Lab On Disc
in Lab
Concentrator XcelVap Horizon
Technologies
17-5545 As needed Used EXT. Lab On Disc
in Lab
Concentrator XcelVap Horizon
Technologies
17-5547 As needed Used EXT. Lab On Disc
in Lab
Concentrator XcelVap Horizon
Technologies
18-5619 As needed Used EXT. Lab On Disc
in Lab
O/G SPE
Extractor
Horizon
Technologies
15-0104 As needed Used EXT. Lab On Disc
in Lab
O/G SPE
Extractor
Horizon
Technologies
16-0169 As needed Used EXT. Lab On Disc
in Lab
O&G Solvent
Evaporator
Horizon
Speed-Vap IV
Horizon Speed-
Vap IV
10-0778 As needed Used EXT. Lab Bookshelf
in Lab
O&G Solvent
Evaporator
Horizon
Speed-Vap IV
Horizon Speed-
Vap IV
04-2020 As needed Used EXT. Lab Bookshelf
in Lab
Analytical
Balance
Rad Wag 552935 As needed Used EXT. Lab EXTBAL
#4
Bookshelf
in Lab
Analytical
Balance
Rad Wag 537906 As needed Used EXT. Lab EXTBAL
#3
Bookshelf
in Lab
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Analytical
Balance
Rad Wag 552941 As needed Used EXT. Lab EXTBAL
#5
Bookshelf
in Lab
Analytical
Balance
Rad Wag 545380 As needed Used EXT. Lab EXTBAL
#7
Bookshelf
in Lab
Analytical
Balance
Rad Wag 537906 As needed Used EXT. Lab EXTBAL
#9
Bookshelf
in Lab
Description Manufacturer Model Serial Number Service
Date
Condit
ion
Location Internal
ID
Manual
Location
Gas
Chromatograph
Hewlett
Packard
5890 Series II 3336A60095 As Needed Used Volatiles VOCGC1
FID1A= FID
FID2B= PID
Online
Gas
Chromatograph
Agilent 6890 CN10609095 As Needed Used Volatiles VOCGC2
FID1A= FID
ELC2B= PID
Online
Gas
Chromatograph
Hewlett
Packard
5890 Series II 3336A50614 As Needed Used Volatiles VOCGC4
FID1A= FID
FID2B= PID
Online
Gas
Chromatograph
Hewlett
Packard
5890 Series II 3027A29678 As Needed Used Volatiles VOCGC5
FID1A= FID
FID2B= PID
Online
Gas
Chromatograph
Hewlett
Packard
5890 Series II 2950A27895 As Needed Used Volatiles VOCGC6
FID1A= FID
FID2B= PID
Online
Gas
Chromatograph
Hewlett
Packard
5890 Series II 3336A55283 As Needed Used Volatiles VOCGC7
FID1A= FID
FID2B= PID
Online
Gas
Chromatograph
Agilent 6890 US00022519 As Needed Used Volatiles VOCGC10
FID1A= FID
FID2B= PID
Online
Gas
Chromatograph
Agilent 6890 US00040221 As Needed Used Volatiles VOCGC12
FID1A= FID
FID2B= PID
Online
Gas
Chromatograph
Hewlett
Packard
5890 Series II 2921A23548 As Needed Used Volatiles VOCGC13
FID1A= FID
FID2B= PID
Online
Gas
Chromatograph
Agilent 6890 CN10406054 As Needed Used Volatiles VOCGC14
FID1A= FID
ELC2B= PID
Online
Gas
Chromatograph
Agilent 6890 US10232130 As Needed Used Volatiles VOCGC15
ELC1A= FID
ELC2B= PID
Online
Gas
Chromatograph
Agilent 8890 GC GC US2120A021 As Needed Used Volatiles VOCGC16
FID1A=FID
FID2B=PID
Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 6890 GC
5975 MSD
GC CN10517046
MS US63234371
As Needed Used Volatiles VOCMS2 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 6890 GC
5973 MSD
GC US00023465
MS US82311257
As Needed Used Volatiles VOCMS4 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 6890 GC
5973 MSD
GC CN10343037
MS US44647141
As Needed Used Volatiles VOCMS6 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 6890 GC
5973 MSD
GC CN10339006
MS US33220045
As Needed Used Volatiles VOCMS13 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 6890 GC
5973 MSD
GC US00006479
MS US82321899
As Needed Used Volatiles VOCMS16 Online
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Description Manufacturer Model Serial Number Service
Date
Condit
ion
Location Internal
ID
Manual
Location
Gas
Chromatograph/
Mass
Spectrometer
Agilent 6890 GC
5975 MSD
GC CN621A4367
MS US469A4832
As Needed Used Volatiles VOCMS20 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 6890 GC
5975 MSD
GC CN621A4368
MS US469A4833
As Needed Used Volatiles VOCMS21 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 7890 GC
5975 MSD
GC CN99205324
MS US54441572
As Needed Used Volatiles VOCMS22 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 7890 GC
5975 MSD
GC CN10728068
MS US71236616
As Needed Used Volatiles VOCMS23 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 6890 GC
5975 MSD
GC CN10728074
MS US98003634
As Needed Used Volatiles VOCMS25 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 6890 GC
5975 MSD
GC CN11381060
MS US11383834
As Needed Used Volatiles VOCMS26 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 7890 GC
5975 MSD
GC CN10301155
MS US10313619
As Needed Used Volatiles VOCMS27 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 6890 GC
5973 MSD
GC US10208101
MS US10442380
As Needed Used Volatiles VOCMS28 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 6890 GC
5973 MSD
GC US000034135
MS US94240103
As Needed Used Volatiles VOCMS30 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 7890 GC
5975 MSD
GC CN13113015
MS US92013978
As Needed Used Volatiles VOCMS32 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 7890 GC
5975 MSD
GC CN11351165
MS US63810153
As Needed Used Volatiles VOCMS33 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 7890 GC
5975 MSD
GC CN10849077
MS US83131017
As Needed Used Volatiles VOCMS35 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 7890 GC
5975 MSD
GC CN13153007
MS US83141150
As Needed Used Volatiles VOCMS36 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 7890 GC
5977 MSD
GC CN15333012
MS US1534M407
As Needed Used Volatiles VOCMS37 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 7890 GC
5975 MSD
GC CN11281031
MS US1713D003
As Needed Used Volatiles VOCMS38 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 7890A GC
5977A MS
GC CN10151020
MS US1417L240
As Needed Used Volatiles VOCMS39 Online
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Description Manufacturer Model Serial Number Service
Date
Condit
ion
Location Internal
ID
Manual
Location
Gas
Chromatograph/
Mass
Spectrometer
Agilent 7890B GC
5977A MSD
GC CN15133171
MS US1542L427
As Needed Used Volatiles VOCMS40 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 7890B GC
5977B MS
GC CN10940090
MS US1705M027
As Needed Used Volatiles VOCMS41 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 7890B GC
5977B MS
GC CN17010001
MS US1706M049
As Needed Used Volatiles VOCMS42 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent Intuvo 9000 GC
5977HES MS
GC CN17040005
MS US1714D003
As Needed Used Volatiles VOCMS44 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 7890B GC
5973 MSD
GC US14453011
MS US1451L418
As Needed Used Volatiles VOCMS52 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 8890B GC
5977B MS
GC US1946A049
MS US1945M023
As Needed New Volatiles VOCMS53 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 8890B GC
5977B MS
GC US1946A050
MS US1946M007
As Needed New Volatiles VOCMS54 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 8890B GC
5977B MS
GC US1946A054
MS US1946M008
As Needed New Volatiles VOCMS55 Online
Gas
Chromatograph/
Mass
Spectrometer
Agilent 8890B GC
5977B MS
GC US1946A056
MS US1945M026
As Needed New Volatiles VOCMS56 Online
as
Chromatograph/
Mass
Spectrometer
Agilent 8890 GC
5977B MS
GC US1947A068
MS US2040M031
As Needed New Volatiles VOCMS57 Online
as
Chromatograph/
Mass
Spectrometer
Agilent 8890 GC
5977B MS
GC US2014A037
MS US2041M011
As Needed New Volatiles VOCMS58 Online
as
Chromatograph/
Mass
Spectrometer
Agilent 8890 GC
5977B MS
GC US2014A036
MS US2040M033
As Needed New Volatiles VOCMS59 Online
Centurion
Autosampler
PTS/EST Centurion CENTS385091214 As Needed Used Volatiles VOCGC2 Online
Centurion
Autosampler
PTS/EST Centurion CENTS368051214 As Needed Used Volatiles VOCMS6 Online
Centurion
Autosampler
PTS/EST Centurion CENTS500041117 As Needed Used Volatiles VOCMS13 Online
Centurion
Autosampler
PTS/EST Centurion CENTW80106212
1
As Needed Used Volatiles VOCMS16 Online
Centurion
Autosampler
PTS/EST Centurion CENTS396112014 As Needed Used Volatiles VOCMS21 Online
Centurion
Autosampler
PTS/EST Centurion CENTW80306212
1
As Needed Used Volatiles VOCMS22 Online
Centurion
Autosampler
PTS/EST Centurion CENTS386091214 As Needed Used Volatiles VOCMS23 Online
Centurion
Autosampler
PTS/EST Centurion CENTS754102820 As Needed Used Volatiles VOCMS25 Online
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Description Manufacturer Model Serial Number Service
Date
Condit
ion
Location Internal
ID
Manual
Location
Centurion
Autosampler
PTS/EST Centurion CENTS170072010 As Needed Used Volatiles VOCMS26 Online
Centurion
Autosampler
PTS/EST Centurion CENTS375071714 As Needed Used Volatiles VOCMS30 Online
Centurion
Autosampler
PTS/EST Centurion CENTS163052610 As Needed Used Volatiles VOCMS33 Online
Centurion
Autosampler
PTS/EST Centurion CENTW80206212
1
As Needed Used Volatiles VOCMS36 Online
Centurion
Autosampler
PTS/EST Centurion CENTW80406212
1
As Needed Used Volatiles VOCMS37 Online
Centurion
Autosampler
PTS/EST Centurion CENTS171072010 As Needed Used Volatiles VOCMS39 Online
Centurion
Autosampler
PTS/EST Centurion CENTS338112213 As Needed Used Volatiles VOCMS40 Online
Centurion
Autosampler
PTS/EST Centurion CENTS395112014 As Needed Used Volatiles VOCMS42 Online
Centurion
Autosampler
PTS/EST Centurion CENTS499041117 As Needed Used Volatiles VOCMS44 Online
Centurion
Autosampler
PTS/EST Centurion CENTS667111119 As Needed Used Volatiles VOCMS53 Online
Centurion
Autosampler
PTS/EST Centurion CENTS664110519 As Needed Used Volatiles VOCMS54 Online
Centurion
Autosampler
PTS/EST Centurion CENTS673120319 As Needed Used Volatiles VOCMS55 Online
Centurion
Autosampler
PTS/EST Centurion CENTS674120319 As Needed Used Volatiles VOCMS56 Online
Centurion
Autosampler
PTS/EST Centurion CENTS756102820 As Needed Used Volatiles VOCMS57 Online
Centurion
Autosampler
PTS/EST Centurion CENTS755102820 As Needed Used Volatiles VOCMS58 Online
Centurion
Autosampler
PTS/EST Centurion CENTW80006212
1
As Needed Used Volatiles VOCMS59 Online
Autosampler Varian Archon 13809 As Needed Used Volatiles VOCGC1 Online
Autosampler Varian Archon 13999 As Needed Used Volatiles VOCGC4 Online
Autosampler Varian Archon 13454 As Needed Used Volatiles VOCGC5 Online
Autosampler Varian Archon 14157 As Needed Used Volatiles VOCGC6 Online
Autosampler Varian Archon 14599 As Needed Used Volatiles VOCGC7 Online
Autosampler Varian Archon 13391 As Needed Used Volatiles VOCGC10 Online
Autosampler Varian Archon VOLARCHON1 As Needed Used Volatiles VOCGC12 Online
Autosampler Varian Archon 13827 As Needed Used Volatiles VOCGC14 Online
Autosampler Varian Archon 13810 As Needed Used Volatiles VOCGC15 Online
Autosampler Varian Archon 15261 As Needed Used Volatiles VOCGC16 Online
Autosampler Varian Archon 14143 As Needed Used Volatiles VOCMS2 Online
Autosampler Varian Archon 14605 As Needed Used Volatiles VOCMS27 Online
Autosampler Varian Archon 14233 As Needed Used Volatiles VOCMS28 Online
Autosampler Teledyne Centurion CENTS317080513 As Needed Used Volatiles VOCMS4 Online
Autosampler Teledyne Atomx US14330003 As Needed Used Volatiles VOCMS52 Online
Autosampler OI Analytical 4100 D645410849 As Needed Used Volatiles VOCMS20 Online
Autosampler OI Analytical 4100 D627410770 As Needed Used Volatiles VOCMS32 Online
Autosampler OI Analytical 4100 D649410582 As Needed Used Volatiles VOCMS35 Online
Autosampler OI Analytical 4100 D619410106 As Needed Used Volatiles VOCMS38 Online
Autosampler OI Analytical 4100 D705410973 As Needed Used Volatiles VOCMS41 Online
Purge and Trap OI Analytical Eclipse 4660 D833466009P As Needed Used Volatiles VOCGC6 Online
Purge and Trap OI Analytical Eclipse 4660 F023466618P As Needed Used Volatiles VOCGC16 Online
Purge and Trap OI Analytical Eclipse 4660 D726466961P As Needed Used Volatiles VOCMS2 Online
Purge and Trap OI Analytical Eclipse 4660 D742466578P As Needed Used Volatiles VOCMS16 Online
Purge and Trap OI Analytical Eclipse 4660 F026466142P As Needed Used Volatiles VOCMS26 Online
Purge and Trap OI Analytical Eclipse 4660 F024466460P As Needed Used Volatiles VOCMS27 Online
Purge and Trap OI Analytical Eclipse 4660 F026466139P As Needed Used Volatiles VOCMS28 Online
Purge and Trap OI Analytical Eclipse 4760 21J102730 As Needed Used Volatiles VOCMS32 Online
Purge and Trap OI Analytical Eclipse 4660 D736466413P As Needed Used Volatiles VOCMS33 Online
Purge and Trap OI Analytical Eclipse 4660 D713466087P As Needed Used Volatiles VOCMS35 Online
Purge and Trap OI Analytical Eclipse 4660 E851466095P As Needed Used Volatiles VOCMS39 Online
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Description Manufacturer Model Serial Number Service
Date
Condit
ion
Location Internal
ID
Manual
Location
Purge and Trap OI Analytical Eclipse 4760 21J102729 As Needed Used Volatiles VOCMS20 Online
Purge and Trap OI Analytical Eclipse 4760 21J102727 As Needed Used Volatiles VOCMS25 Online
Purge and Trap OI Analytical Eclipse 4760 A627447776 As Needed Used Volatiles VOCMS37 Online
Purge and Trap OI Analytical Eclipse 4760 21J102728 As Needed Used Volatiles VOCMS38 Online
Purge and Trap OI Analytical Eclipse 4760 A620447864 As Needed Used Volatiles VOCMS40 Online
Purge and Trap OI Analytical Eclipse 4760 A703447399 As Needed Used Volatiles VOCMS41 Online
Purge and Trap OI Analytical Eclipse 4760 A707447491 As Needed Used Volatiles VOCMS42 Online
Purge and Trap OI Analytical Eclipse 4760 A942447703 As Needed Used Volatiles VOCMS53 Online
Purge and Trap OI Analytical Eclipse 4760 A031447210 As Needed Used Volatiles VOCMS54 Online
Purge and Trap OI Analytical Eclipse 4760 A946447334 As Needed Used Volatiles VOCMS55 Online
Purge and Trap OI Analytical Eclipse 4760 A946447333 As Needed Used Volatiles VOCMS56 Online
Purge and Trap OI Analytical Eclipse 4760 A039447237 As Needed Used Volatiles VOCMS57 Online
Purge and Trap OI Analytical Eclipse 4760 A041447860 As Needed Used Volatiles VOCMS58 Online
Purge and Trap OI Analytical Eclipse 4760 A946447335 As Needed Used Volatiles VOCMS59 Online
Purge and Trap PTS/EST Encon 301082903P As Needed Used Volatiles VOCGC1 Online
Purge and Trap PTS/EST Encon 269050803P As Needed Used Volatiles VOCGC2 Online
Purge and Trap PTS/EST Encon 273052803P As Needed Used Volatiles VOCGC4 Online
Purge and Trap PTS/EST Encon 156053001 As Needed Used Volatiles VOCGC5 Online
Purge and Trap PTS/EST Encon 213073102E As Needed Used Volatiles VOCGC7 Online
Purge and Trap PTS/EST Encon 271051903P As Needed Used Volatiles VOCGC10 Online
Purge and Trap PTS/EST Eclipse D719466252P As Needed Used Volatiles VOCGC12 Online
Purge and Trap PTS/EST Encon 302082903E As Needed Used Volatiles VOCGC14 Online
Purge and Trap PTS/EST Encon 280062503P As Needed Used Volatiles VOCGC15 Online
Purge and Trap PTS/EST Evolution EV577051214 As Needed Used Volatiles VOCMS6 Online
Purge and Trap PTS/EST Evolution EV504082713 As Needed Used Volatiles VOCMS4 Online
Purge and Trap PTS/EST Evolution EV831041117 As Needed Used Volatiles VOCMS13 Online
Purge and Trap PTS/EST Evolution EV642112014 As Needed Used Volatiles VOCMS21 Online
Purge and Trap PTS/EST Evolution EV643112014 As Needed Used Volatiles VOCMS22 Online
Purge and Trap PTS/EST Evolution EV618091214 As Needed Used Volatiles VOCMS23 Online
Purge and Trap PTS/EST Evolution EV594071714 As Needed Used Volatiles VOCMS30 Online
Purge and Trap PTS/EST Evolution EV832041117 As Needed Used Volatiles VOCMS44 Online
Purge and Trap PTS/EST Evolution II EV20174062121 As Needed Used Volatiles VOCMS36 Online
Description Manufacturer Model Serial Number Service
Date
Condit
ion
Location Internal
ID
Manual
Location
Analytical
Balance
Mettler XP205 1129420141 As Needed Used Wet Lab Balance 3 Online
Analytical
Balance
Mettler
Toledo
AG204 1120381348 As Needed Used Wet Lab WetBal 1 Online
Analytical
Balance
VWR 403B 5262015128 As Needed Used Wet Lab WetBa8 Online
Analytical
Balance
VWR 403B 5262015102 As Needed Used Wet Lab WetBa7 Online
Balance RADWAG WTC600 603664 2019 New Wet Lab WetBal 13 Online
Balance Scout Pro B513752877 As Needed Used Wet Lab WetBal 9 Online
Analytical
Balance
Mettler
Toledo
MS204TS/00 B820869344 As Needed Used Wet Lab WetBal 10 Online
Autoanalyzer OI Analytical FS 3100 301831056 (NH3)
251833391 (CN)
As Needed Used Wet Lab FS 3100-1 Online
Distillation Unit-
TKN/PT
Seal
Analytical
BD50/28 5146001504 2021 New Wet Lab Block D Online
Distillation Unit-
TKN/PT
Lachat
Instrument
BD40 1018420580 2022 New Wet Lab Block C Online
Autoanalyzer OI Analytical FS 3100 407831164
(NO2NO3)
403833925 (PHT)
Wet Lab FS 3100-3 Online
Autoanalyzer Lachat Quikchem 8000 A83000-1027 As Needed Used Wet Lab Lachat 2 Online
Autoanalyzer Lachat Quikchem 8000 A83000-1638 As Needed Used Wet Lab Lachat 3 Online
Autoanalyzer Lachat Quikchem 8500 60900000341 As Needed Used Wet Lab Lachat 4 Online
Autoanalyzer Lachat Quikchem 8500 60900000342 As Needed Used Wet Lab Lachat 5 Online
Autoanalyzer Lachat Quikchem 8500 70500000452 As Needed Used Wet Lab Lachat 6 Online
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Description Manufacturer Model Serial Number Service
Date
Condit
ion
Location Internal
ID
Manual
Location
Autoanalyzer-
digestor
Lachat BD-46 100700000-982 As Needed Used Wet Lab DIG1 Online
Autoanalyzer-
digestor
Lachat BD-46 1800-871 As Needed Used Wet Lab DIG1 Online
Autoanalyzer-
digestor
Lachat BD-46 1000700000-982 As Needed Used Wet Lab DIG2 Online
Autoanalyzer-
digestor
Lachat BD-46 1800-872 As Needed Used Wet Lab DIG2 Online
Autoanalyzer-
digestor
Lachat BD-40 HTLC1018420580 As Needed Used Wet Lab DIG3 Online
Automated
Titrator
Metrohm 855 titrosampler 3256 As Needed Used Wet Lab Titrando Online
Automated
Titrator
Metrohm 855 titrosampler 3315 2021 New Wet Lab Titrando Online
Automated
Titrator
Metrohm 855 titrosampler 3319 2021 New Wet Lab Titrando Online
Balance RADWAG WTC600 603642 2019 New Wet Lab WetBal 11 Online
Balance RADWAG WTC600 603657 2019 New Wet Lab WetBal 12 Online
Balance RADWAG WTC600 603639 2019 New Wet Lab WetBal 14 Online
Bomb
Calorimeter
Parr 1108 Oxygen Bomb 5424 Used Wet Lab Parr Bomb Online
Bomb
Calorimeter
Parr 1108 Oxygen Bomb 6420-1112-24696 2021 New Wet Lab Parr Bomb Online
Centrifuge Thermo ST40 41179863 As Needed Used Wet Lab Centrifuge
Online
Centrifuge Damon HNSII 23557225 As Needed Used We Lab Centrifuge Cabinet
Class “I” weights Troemner Serial # 7944 4057 As Needed Used Wet Lab Online
COD Reactor Environment
al Express
B3000 2016CODW101 As Needed Used Wet Lab COD Reactor Online
Conductivity
Meter
ORION Model 170 32470051 As Needed Used Wet Lab ATI Orion Online
Conductivity
Meter
Thermo
Fisher
Orion VersaStar V02971 As Needed Used Wet Lab Orion VS-2 Online
Discrete Analyzer Seal AQ400 141032 2017 New Wet Lab Seal 1 Online
DI Water Dionex IC Pure 42034291 As Needed Used Wet Lab Nanopure Online
Distillation Unit-
Cyanide
Environment
al Express
Distillation 1 2270 As Needed Used Wet Lab LMD1920-106 Online
Distillation Unit-
Cyanide
Environment
al Express
Distillation 2 2271 As Needed Used Wet Lab LMD1920-106 Online
Distillation Unit-
Cyanide
Environment
al Express
Distillation 3 2272 As Needed Used Wet Lab LMD1920-106 Online
Distillation Unit-
Phenol
Westco
Scientific
Model EASY-
DIST
1062 As Needed Used Wet Lab Dist 1 Online
Distillation Unit-
Phenol
Westco
Scientific
Model EASY-
DIST
1198 As Needed Used Wet Lab Dist 2 Online
Drying Oven VWR 1390 FM 501202 As Needed Used Wet Lab 103-105 Online
Drying Oven Shel Lab FX28-2 12006713 As Needed Used Wet Lab 178-182 Online
Drying Oven Shel Lab SM028-2 8041917 As Needed Used Wet Lab 178-182 Online
Drying Oven Shel Lab --As Needed Used Wet Lab 178-182 Online
Flash Point
Tester
Koehler Pensky-Martens
K16200
R07002693B As Needed Used Wet Lab Manual Cabinet
Flash Point
Tester
Koehler Pensky-Martens
K16204
R070022328D As Needed Used Wet Lab Manual Cabinet
Automated Flash
Point Ignitability
Tester
Tanaka APM-8FC 34352 2019 New Wet Lab Automated Online
Automated Flash
Point Ignitability
Tester
Tanaka APM-8FC 34394 2020 New Wet Lab Automated Online
Hot Block TDS Environment
al Express
TDS024 2017TDSW101 2018 New Wet Lab TDS Hot
Block
Cabinet
Hot Plate Cole Parmer HS19 C-P 50000073 As Needed Used Wet Lab Hot Plate Unknow
n
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Description Manufacturer Model Serial Number Service
Date
Condit
ion
Location Internal
ID
Manual
Location
Hot Plate Thermo
Fisher
Type 2200 C1707140516473 As Needed Used Wet Lab Hot Plate Unknow
n
Hot Plate Cole Parmer HS19 CP 50002676 As Needed Used Wet Lab Hot Plate Unknow
n
Hot Plate Cole Parmer HS19 CP 50002447 As Needed Used Wet Lab Hot Plate Unknow
n
Hot Plate Cole Parmer HS19 CP 50002557 As Needed Used Wet Lab Hot Plate Unknow
n
Ion
Chromatograph
Dionex ICS-2000 6050731 As Needed Used Wet Lab IC5 Online
Ion
Chromatograph
Dionex ICS 1500 8100010 As Needed Used Wet Lab IC6 Online
Ion
Chromatograph
Dionex ICS 2000 8090820 As Needed Used Wet Lab IC8 Online
Ion
Chromatograph
Dionex ICS 2100 10060822 As Needed Used Wet Lab IC9 Online
Ion
Chromatograph
Dionex ICS 2100 10091285 As Needed Used Wet Lab IC10 Online
Ion
Chromatograph
Dionex ICS 2100 11012204 As Needed Used Wet Lab IC11 Online
Ion
Chromatograph
Dionex ICS 2100 12020460 As Needed Used Wet Lab IC12 Online
Ion
Chromatograph
Thermo
Fisher
ICS 1600 13031204 As Needed Used Wet Lab IC13 Online
Ion
Chromatograph
Thermo
Fisher
ICS-2100 15030082 As Needed Used Wet Lab IC14 Online
Ion
Chromatograph
Thermo
Fisher
ICS-2100 15071973 As Needed Used Wet Lab IC15 Online
Ion
Chromatograph
Thermo
Fisher
ICS-2100 15071973 As Needed Used Wet Lab IC16 Online
Ion
Chromatograph
Thermo
Fisher
(1) ICS-
1600
15110462 As Needed Used Wet Lab IC17 Online
Ion
Chromatograph
Thermo
Fisher
ICS-2100 15120139 As Needed Used Wet Lab IC18 Online
Ion
Chromatograph
Thermo
Fisher
Integrion 16070510 As Needed Used Wet Lab IC19 Online
Ion
Chromatograph
Thermo
Fisher
Integrion 16090734 As Needed Used Wet Lab IC20 Online
Ion Chromato
Ion
Thermo
Fisher
Integrion 19050436 2019 New Wet Lab IC21 Online
Ion
Chromatograph
Thermo
Fisher
Integrion 19040421 2019 New Wet Lab IC22 Online
Ion
Chromatograph
Thermo
Fisher
Integrion 19050752 2019 New Wet Lab IC23 Online
Ion
Chromatograph
Thermo
Fisher
Integrion 19050751 2019 New Wet Lab IC24 Online
Muffle Furnace Thermolyne 30400 23231 As Needed Used Wet Lab FURNACE Online
Muffle Furnance Cole Parmer CE3749 As Needed Used Wet Lab FURNACE Online
ORP Meter YSI ORP15 JC000114 As Needed Used Wet Lab ORP Online
pH Meter Fisher AB15 AB92329028 As Needed Used Wet Lab AB 15+Online
pH Meter Orion 410A 58074 As Needed Used Wet Lab Orion Online
pH Meter Thermo
Fisher
Orion VersaStar V00659 As Needed Used Wet Lab Orion VS-1 Online
pH Meter Thermo
Fisher
Orion Starfall 1 J13992 As Needed Used Wet Lab PH1 Online
pH Meter Thermo
Fisher
Orion Star A222 K12005 2018 New Wet Lab PH Online
pH Meter Thermo
Fisher
Orion Star A111 J21101 As Needed Used Wet Lab PH Online
pH Meter Thermo
Fisher
Orion Star A111 J21983 2019 New Wet Lab pH Online
Refrigerated
Recirculator
Polyscience Recirculator 1282 As Needed Used Wet Lab Recirculator 1 Online
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Description Manufacturer Model Serial Number Service
Date
Condit
ion
Location Internal
ID
Manual
Location
Refrigerated
Recirculator
Polyscience Recirculator 1608 As Needed Used Wet Lab Recirculator 2 Online
Shaker GlasCol 099A LC1012 11325052 As Needed Used Wet Lab Shaker Online
SimpleDist Env. Express SC154 8940CECW3871 As Needed Used Wet Lab SimpDist1 Online
SimpleDist Env. Express SC155 9062CECW3952 As Needed Used Wet Lab SimpDist2 Online
SimpleDist Env. Express SC156 9062CECW3955 As Needed Used Wet Lab SimpDist3 Online
SimpleDist Env Express MDI 2019MDISW159 2019 New Wet Lab SimpD4 Online
SimpleDist Env Express MDI 2019MDISW162 2019 New Wet Lab SimpD 5 Online
Spectrophotomet
er
Hach DR6000 1646676 As Needed Used Wet Lab DR6000-1 Online
Spectrophotomet
er
Hach DR6000 1646781 As Needed Used Wet Lab DR6000-2 Online
Spectrophotomet
er
Hach DR6000 1894098 2019 New Wet Lab DR6000-3 Online
Spectrophotomet
er
Hach Dr6000 1893736 2022 New Wet Lab DECSP02 Online
Stir Base Env. Express STIR 2019 STIR132 2019 New Wet Lab STIR Online
TOC Analyzer Shimadzu Model TOC-VWS 39830572 As Needed Used Wet Lab TOC2 Online
TOC Analyzer Shimadzu TOC-VCPH H51304435 As Needed Used Wet Lab TOC3 Not in
Sevice
TOC Analyzer Shimadzu TOC-L H54335232035 As Needed Used Wet Lab TOC5 Online
TOC Analyzer Shimadzu TOC H51725600306 As Needed Used Wet Lab TOC6 Online
TOC Analyzer EST TE Xplorer 2019.154 2019 New Wet Lab TOC8 Online
TOC Analyzer Shimadzu TOC-L H54215000551 2021 Used Wet Lab TOC10 Online
TOX Analyzer EST TE Xplorer 2017.287 2017 New Wet Lab TOX5 Online
TOX Analyzer EST TE Xplorer 2017.286 2017 New Wet Lab TOX6 Online
TOX Analyzer EST TE Xplorer 2015-184 2015 New Wet Lab TOX3 Online
TOX Analyzer EST TE Xplorer 2016202 2016 New Wet Lab TOX4 Online
Turbidimeter Hach TL2300 2017070C0008 2018 New Wet Lab TURB1 Online
Description Manufacturer Model Serial Number Service
Date
Condit
ion
Location Internal
ID
Manual
Location
Chemchek KPA-
11 Kinetic
Phosphorescence
Analyzer w/
Gilson Sample
Changer and
Gilson Dilutor
401 Syringe Pump
Chemchek KPA-11 1418986;
649025031; 91-
5050024
As Needed Used Rad Lab At the
Instrument
Canberra 2404
Alpha/Beta
Counter
Canberra 2404 1090352; 988600/
787196; 488584
As Needed Used Rad Lab At the
Instrument
Packard Tri-Carb
2200CA Liquid
Scintillation
Counter
Packard 2200CA 102180 As Needed Used Rad Lab At the
Instrument
Canberra LB4100
Alpha/Beta
Counter
Canberra LB4100U2 1300001; 1300002;
1300000; 117
As Needed Used Rad Lab At the
Instrument
Canberra Genie
2000 Alpha
Spectrometer
System
Canberra Genie 2000 See Description As Needed Used Rad Lab At the
Instrument
Canberra Genie
2000 Gamma
Spectrometer
System
Canberra Genie 2000 See Description Clean
Chambers
monthly,
Vacuum
pump-6
months.
As needed.
Used Rad Lab At the
Instrument
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Description Manufacturer Model Serial Number Service
Date
Condit
ion
Location Internal
ID
Manual
Location
LSC 8000 Liquid
Scintillation
Counter
Hitachi LSC-8000 GR30025119 As Needed New Rad Lab At the
Instrument
Hot Plate Presto 703016 NA As Needed Used Rad Lab G1 Online
Hot Plate Presto NA NA As Needed Used Rad Lab G2 Online
Hot Plate Presto 703016 NA As Needed Used Rad Lab G3 Online
Hot Plate Bella TSK-2470P NA As Needed Used Rad Lab G4 Online
Hot Plate Bella TSK-2470P NA As Needed Used Rad Lab G5 Online
Hot Plate Presto TSK-2470P NA As Needed Used Rad Lab G6 Online
Hot Plate Presto 703016 NA As Needed Used Rad Lab G7 Online
Hot Plate Bella TSK-2470P NA As Needed Used Rad Lab G8 Online
Hot Plate Presto 703016 NA As Needed Used Rad Lab G9 Online
Hot Plate Mainstays NA NA As Needed Used Rad Lab G10 Online
Hot Plate Mainstays NA NA As Needed Used Rad Lab G11 Online
Furnace Fisher
Scientific
550-126 902NOO12 As Needed Used Rad Lab M1 Online
Furnace Barnstead FB1415M 7.46951E+11 As Needed Used Rad Lab M2 Online
Centrifuge Beckman TJ-06 96006 As Needed Used Rad Lab C1 Rad Lab
Centrifuge Beckman TJ-06 9A010 As Needed Used Rad Lab C2 Rad Lab
Centrifuge Beckman TJ-06 8953 As Needed Used Rad Lab C3 Rad Lab
Centrifuge Fisher
Scientific
ST-40 42502680 As Needed Used Rad Lab C4 Rad Lab
Hot Water Bath Oster NA NA As Needed Used Rad Lab HB1 Online
Hot Water Bath Mainstays NA NA As Needed Used Rad Lab HB2 Online
Hot Water Bath Sunbeam
Products
CKSTR51B-VHD-
D
192847 As Needed Used Rad Lab HB3 Online
Sonicator CD FCC
RoHS
PS-30A 20150720 As Needed Used Rad Lab So1 Online
Hot Plate Troemner,
LLC
984VWOAHPUSS 171027003 As Needed Used Rad Lab HP1 Online
Hot Plate Troemner,
LLC
984VWOAHPUSS 161026002 As Needed Used Rad Lab HP2 Online
Hot Plate Troemner,
LLC
984VWOAHPUSS 161026001 As Needed Used Rad Lab HP3 Online
Hot Plate Troemner,
LLC
984VWOAHPUSS 160927002 As Needed Used Rad Lab HP4 Online
Shaker Eserbach NA NA As Needed Used Rad Lab Sh1 Online
Shaker NA 6000 NA As Needed Used Rad Lab Sh2 Online
Hot Plate/Stirrer NA NA NA As Needed Used Rad Lab St1 Online
Hot Plate/Stirrer Labline
Insruments
1287 NA As Needed Used Rad Lab St2 Online
Hot Plate/Stirrer Labline
Instruments
1287 3055447 As Needed Used Rad Lab St3 Online
Hot Plate/Stirrer NA NA NA As Needed Used Rad Lab St4 Online
Hot Plate/Stirrer NA NA NA As Needed Used Rad Lab St5 Online
Hot Plate/Stirrer NA NA NA As Needed Used Rad Lab St6 Online
Hot Plate/Stirrer NA NA NA As Needed Used Rad Lab St7 Online
Hot Plate/Stirrer NA NA NA As Needed Used Rad Lab St8 Online
Hot Plate/Stirrer NA NA NA As Needed Used Rad Lab St9 Online
Hot Plate/Stirrer NA NA NA As Needed Used Rad Lab St10 Online
Hot Plate/Stirrer Labline
Instruments
1268 NA As Needed Used Rad Lab St11 Online
Hot Plate/Stirrer Labline
Instruments
1268 NA As Needed Used Rad Lab St12 Online
Hot Plate/Stirrer Labline
Instruments
1268 8039816 As Needed Used Rad Lab St13 Online
Hot Plate/Stirrer Labline
Instruments
1268 0185 As Needed Used Rad Lab St14 Online
Hot Plate/Stirrer SYMA HJ6A NA As Needed New Rad Lab St15 Online
Hot Plate/Stirrer SYMA HJ6A NA As Needed New Rad Lab St16 Online
Hot Plate/Stirrer SYMA HJ6A NA As Needed New Rad Lab St17 Online
Hot Plate/Stirrer SYMA HJ6A NA As Needed New Rad Lab St18 Online
Oven Binder NA NA As Needed Used Rad Lab O1 Online
ENV-MAN-MTJL-0001 v03_Quality Manual
Effective Date: 8/15/2022 3:09:53 PM
COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Description Manufacturer Model Serial Number Service
Date
Condit
ion
Location Internal
ID
Manual
Location
Oven Shel Lab 1326 5057405 As Needed Used Rad Lab O2 Online
Sealer Automatic
Canning
NA 3108 As Needed Used Rad Lab S1 Rad Lab
Grinder Straus Co. 4E NA As Needed Used Rad Lab GR1 Rad Lab
Grinder Arthur H.
Thomas Co.
NA 4352 As Needed Used Rad Lab GR2 Rad Lab
Tumbler US Stoneware NA CN12005 As Needed Used Rad Lab T1 Rad Lab
Tumbler US Stoneware NA CN32108 As Needed Used Rad Lab T2 Rad Lab
Balance RADWAG PS360R2 530077 As Needed Used Rad Lab RADBAL
1
Rad Lab
Balance RADWAG PS4500R2 544404 As Needed Used Rad Lab RADBAL
2
Rad Lab
Balance RADWAG AS60/220R2 415543 As Needed Used Rad Lab RADBAL
3
Rad Lab
Balance RADWAG PS4500R2 544401 As Needed Used Rad Lab RADBAL
4
Rad Lab
Pipettor/Repeate
r
RAININ EDP3-PLUS C040040E Quarterly Used Rad Lab E-31 Rad
Lab/Online
Pipettor/Repeate
r
RAININ EDP3-PLUS K0203177E Quarterly Used Rad Lab E-44 Rad
Lab/Online
Pipettor/Repeate
r
RAININ EDP3 J0400734E Quarterly Used Rad Lab E-33 Rad
Lab/Online
Pipettor/Repeate
r
RAININ EDP3-PLUS H0300753E Quarterly Used Rad Lab E-63 Rad
Lab/Online
Pipettor/Repeate
r
RAININ EDP3-PLUS A00978 Quarterly Used Rad Lab E-41 Rad
Lab/Online
Pipettor/Repeate
r
RAININ EDP3-PLUS J0400699E Quarterly Used Rad Lab E-43 Rad
Lab/Online
Pipettor/Repeate
r
RAININ EDP3-PLUS J0300147E Quarterly Used Rad Lab E-54 Rad
Lab/Online
Pipettor/Repeate
r
RAININ EDP3-PLUS G0200223E Quarterly Used Rad Lab E-32 Rad
Lab/Online
Pipettor/Repeate
r
RAININ EDP3-PLUS H0000585E Quarterly Used Rad Lab E-53 Rad
Lab/Online
Pipettor/Repeate
r
RAININ EDP3-PLUS B0200477E Quarterly Used Rad Lab E-42 Rad
Lab/Online
Pipettor/Repeate
r
OXFORD MACRO SET NA Quarterly Used Rad Lab 102 Rad
Lab/Online
Pipettor/Repeate
r
OXFORD NA Quarterly Used Rad Lab 130 Rad
Lab/Online
Pipettor/Repeate
r
Ward Science 2.5-30 NA Quarterly Used Rad Lab RP-1 Rad
Lab/Online
Pipettor/Repeate
r
RAININ EDP3-PLUS F200510E Quarterly Used Rad Lab E-34 Rad
Lab/Online
Pipettor/Repeate
r
RAININ EDP3-PLUS D1100091E Quarterly Used Rad Lab E-64 Rad
Lab/Online
Survey Meter 9 79445 Annually Used Rad Lab Rad Lab
Survey Meter 3 156503 Annually Used Rad Lab Rad Lab
Survey Meter 12 88002 Annually Used Rad Lab Rad Lab
Survey Meter 3-98 71211 Annually Used Rad Lab Rad Lab
Survey Meter 3-98 455984 Annually Used Rad Lab Rad Lab
Survey Meter 3 292175 Annually Used Rad Lab Rad Lab
Survey Meter 3 292202 Annually Used Rad Lab Rad Lab
Survey Meter 177 287820 Annually Used Rad Lab Rad Lab
Survey Meter 2221 172021 Annually Used Rad Lab Rad Lab
Survey Meter 19 156438 Annually Used Rad Lab Rad Lab
Survey Meter 9 74528 Annually Used Rad Lab Rad Lab
Survey Meter 3 156232 Annually Used Rad Lab Rad Lab
Survey Meter 3 156193 Annually Used Rad Lab Rad Lab
Survey Meter 3 56439 Annually Used Rad Lab Rad Lab
Survey Meter 12 63765 Annually Used Rad Lab Rad Lab
Survey Meter 177 96337 Annually Used Rad Lab Rad Lab
Survey Meter 12 47797 Annually Used Rad Lab Rad Lab
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Description Manufacturer Model Serial Number Service
Date
Condit
ion
Location Internal
ID
Manual
Location
Survey Meter 12 87918 Annually Used Rad Lab Rad Lab
Survey Meter 2221 154201 Annually Used Rad Lab Rad Lab
Survey Meter 19 499190 Annually Used Rad Lab Rad Lab
Survey Meter 19 156468 Annually Used Rad Lab Rad Lab
Survey Meter 3-98 155387 Annually Used Rad Lab Rad Lab
Survey Meter 3 156193 Annually Used Rad Lab Rad Lab
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COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
Description Manufacturer
e
Model Serial Number Service
date
Conditi
on
Location Internal
ID
Manual
Location
Centrifuge Eppendorf 5424R 5404IR839716 As needed New PCR PCR Lab
Centrifuge Thermo
Scientific
Sorvall Legend
Micro 21R
42930526 As needed New PCR PCR Lab
Galaxy Tablet
with PLatr
Samsung SM-T510 R52MA0T1C5E As needed New PCR PCR Lab
Heat Block Thermo
Scientifc
Dry bath Standard
1 Blck 100-120V
KABT70001011 As needed New PCR PCR Lab
Isotemp Large
Oven
Fisherbrand 3511FSQ 300403777 As needed New PCR PCR Lab
Mini Centrifuge Fisherbrand SPROUT PLUS HSG04861 As needed New PCR PCR Lab
Mini Centrifuge Fisherbrand SPROUT PUS HSG04753 As needed New PCR PCR Lab
Mini Vortex
Mixer
Fisherbrand Mini Vortex Mixer
(Variable Speed)
200020151 As needed New PCR PCR Lab
Mini Vortex
Mixer
Fisherbrand Mini Vortex Mixer
(Variable Speed)
200020151 As needed New PCR PCR Lab
Minus 80 Freezer SCIENTEMP 86-01A S8008781 As needed New PCR PCR Lab
Precisiom CIR 89
Water Bath
Thermo
Scientific
TSCIR89 300399766 As needed New PCR PCR Lab
Refrigerator Frigidaire FRT18L4JW5 BA92344749 As needed PCR PCR Lab
Repeater Pipette Eppendorf Repeater E3 N296671 As needed PCR PCR Lab
Repeater Pipette Eppendorf Repeater E4 H40109J As needed PCR PCR Lab
RT-PCR Machine Applied
Biosystems
by Thermo
Scientific
QuantStudio5 272531538 As needed New PCR PCR Lab
RT-PCR Machine Applied
Biosystems
by Thermo
Scientific
QuantStudio7 278872930 As needed New PCR PCR Lab
Refrigerator Danbury
Designer
DAR110A1WDD 4320043102086 As needed New PCR PCR Lab
Oven Quincy Lab
Inc
10-100 I11-2454 As needed Used PCR PCR Lab
Sorvall X Pro
Centrifuge
ThermoFishe
r Scientific
SorvallX4R Pro-
MD
42632360 As needed New PCR PCR Lab
UPS (Surge
Protector/Power
Backup
CyberPower CP1500PFCLCDa CXXJY2002934 As needed New PCR PCR Lab
UPS (Surge
Protector/Power
Backup
CyberPower CP1500PFCLCD CXXJY2002934 As needed New PCR PCR Lab
Incubator Fisherbrand Isotemp 300403777 As needed New PCR PCR Lab
Plate Shaker Fisherbrand 88861023 K4CF61023014 As needed New PCR PCR Lab
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COPYRIGHT © 2019-2022 Pace® Analytical Services, LLC.
8.0 ADDENDUM: PROGRAM REQUIREMENTS
Section 8.0 provides additional requirements the locations covered by this manual are required to follow
when performing work under the program. Only requirements that are not covered by the main body of
the manual are listed in addendum.
8.1 DoD/DOE
PAS-Mt. Juliet maintains accreditation for DoD/DoE Environmental Laboratory Approval
Program (ELAP)
This addendum outlines additional policies and processes established by this laboratory to maintain
compliance with DoD/DOE program specific requirements as outlined in the DoD/DOE
Consolidated Quality Systems Manual (QSM) for Environmental Laboratories. The QSM
incorporates ISO/IEC 17025 and the TNI Standard and includes additional program-specific
requirements for laboratories that perform analytical testing services for DoD and DOE, and which
must be followed for DoD / DOE projects.
Section 4.2.5: Supporting Documents
In addition to the requirements specified in Section 4.2.5, technical SOPs used for DoD/DOE
testing must also include instructions for equipment and instrument maintenance, computer
software/hardware, and troubleshooting.
The review frequency for technical SOPs used for DoD/DOE testing is annual, instead of every 2
years.
Section 4.4: Review of Analytical Service Requests
If the DoD/DOE customer requests a statement of conformity, the standard used for the decision
rule must be communicated to and agreed on with the customer and identified in the final test report.
Laboratory requests to deviate from the requirements specified in the DoD/DOE QSM must be
requested on a project-basis and include technical justifications for the deviation. These requests are
submitted to and approved by the DoD/DOE project chemist or contractor, however name, in
addition to the PAS client.
For DoD / DOE projects, will also seek clarification from the customer when the customer has
requested an incorrect, obsolete, or improper method for the intended use of data; the laboratory
needs to depart from its test method SOP in order to meet project-specific data quality objectives;
information in project planning documents is missing or is unclear,
Section 4.5: Subcontracting
In addition to written client approval of any subcontractor for testing, the customer is notified of
the laboratory’s intent to use a subcontractor for any management system element (such as data
review, data processing, project management or IT support) and consent for subcontracting is
obtained approved in writing by the DoD/DOE customer and record of consent kept in the project
record.
Section 4.6: Purchasing and Supplies
The laboratory procedure for records of receipt of materials and supplies used in testing also include
a specification to record the date opened (DOE only).
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Section 4.9.3: Nonconforming Work
The laboratory’s procedure for client notification includes the 15-business day DoD /DOE
timeframe for notification of the problem and the 30-business day timeframe for submission of the
corrective action plan or corrective actions taken. This procedure also includes the DoD/DOE
requirement for AB notification of discovery.
Section 4.13: Control of Records
Technical Records: The laboratory’s procedure for logbooks includes measures to prevent the
removal of or addition of pages to the logbook (applies to both hardcopy and electronic). Hardcopy
logbooks are version controlled, pre-numbered and bound. Initials and entries are signed or initialed
and dated by the person making the entry and the entry is made at the time the activity is performed
and in chronological order. Each page of the logbook must be closed by the last person making the
entry on the page. Closure is recorded by the initial and date of the person making the last entry.
Section 5.4.5.3.3: Limit of Detection
For DoD/DOE the LOD is an estimate of the minimum amount of an analyte that can be reliably
detected by an analytical process. For clarification, the LOD is the analyte concentration necessary
to distinguish its presence from its absence. The LOD may be used as the lowest concentration for
reliably reporting a non-detect (ND). The LOD is specific to each suite of analyte, matrix, and
method including sample preparation.
After each DL determination, the laboratory establishes the LOD by spiking a quality system matrix
at a concentration of least 2X but no greater than 4X the DL (i.e., 2X DL LOD Spike 4X DL).
The spike concentration establishes the LOD and the concentration at which the LOD is verified.
The LOD is established during method validation and after major changes to the analytical system
or procedure that affects sensitivity of analysis or how the procedure is performed.
An LOD study is not required for any component for which spiking solutions or quality control
samples are not available. Additionally, an LOD study is not required if the laboratory does not
report data below the LOQ.
The LOD must be verified on a quarterly basis. Each preparation method listed on the scope of
accreditation must have quarterly LOD verifications; however, verification of all possible
combinations of preparation and clean-up techniques is not required. Where LOD verifications are
not performed on all combinations, the LOD verification is based on the worst-case combination
(preparation method with all applicable cleanup steps).
The laboratory’s procedure for LOD determination and verification is detailed in SOP ENV-SOP-
MTJL-0016 Method Detection Limits (MDL), Limits of Detection (LOD) and Limits of Quantitation (LOQ)
and ENV-SOP-MTJL-0340 Radiochemistry Method Performance Criteria.
Section 5.4.5.3.4: Limit of Quantitation
For DoD/DOE, the LOQ is established for each analyte-matrix-method combination, including
surrogates. When an LOD is determined or verified by the laboratory, the LOQ must be above the
LOD [DL<LOD<LOQ].
At a minimum, the LOQ must be verified quarterly; however, verification of all possible
combinations of preparation and clean-up techniques is not required. Where LOQ verifications are
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not performed on all combinations, the LOQ verification on the worst-case combination
(preparation method with all applicable cleanup steps).
The laboratory’s procedure for LOQ determination and verification is detailed in laboratory SOP
ENV-SOP-MTJL-0016 Method Detection Limits (MDL), Limits of Detection (LOD) and Limits of
Quantitation (LOQ) and ENV-SOP-MTJL-0340 Radiochemistry Method Performance Criteria.
Section 5.4.7: Control of Data
The laboratory will assure LIMS passwords are changed at least once per year.
An audit of the LIMS will be incorporated into the laboratory’s annual internal audit schedule.
The laboratory will have procedures in place to notify DoD/DOE customers of changes to LIMS
software or hardware configurations that may impact the customer’s integrity of electronic data
Section 5.9.1: Quality Control
For DoD/DOE, storage blanks are essential QC to monitor the storage of samples for volatile
organic analysis (VOA). The SOP for storage of VOA samples must include a contamination
monitoring program based on the performance of storage blanks. (See QSM 5.3.3)
Section 5.8.5: Sample Disposal
For DOE projects, the record of disposal must also include how the sample was disposed and the
name of the person that performed the task.
Appendix E: Support Equipment Calibration
Mechanical Volumetric Pipette: In addition to the quarterly verification check, pipettes used for
DoD/DOE projects are checked daily before use using the same procedure and criteria specified
for the quarterly check.
Water Purification System: The performance of the water purification system is checked daily prior
to use in accordance with SOP ENV-SOP-MTJL-0366 Reagent Water Quality.
Radiological Survey Equipment: The performance of the radiological survey equipment is checked
daily prior to use in accordance with SOP ENV-SOP-MTJL-0344 Radiation and Contamination Surveys.
Additional: (DOE): Section 6.0 of the QSM outlines additional management system requirements
for the management of hazardous and radioactive materials management and health and safety
practices. The laboratory, if approved for DOE, will consult with the PAS Health and Safety Director
to establish plans, policies and procedures that conform to these comprehensive specifications and
incorporate these documents into the QMS.
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8.2 ADDENDUM: AIHA-LAP, LLC
Section 4.1.5.4: Confidentiality
While the laboratory does not typically make client information public, the customer will be informed
in advance if the laboratory intends to place any client-identifying information in the public domain.
Information about the customer obtained from sources other than the customer (e.g., complainant,
regulators) will remain confidential between the customer and the laboratory. The source of the
information will remain confidential to the laboratory and will not be shared with the customer,
unless agreed by the source.
Personnel, including any committee members, contractors, personnel of external bodies, or
individuals acting on the laboratory’s behalf, shall keep confidential all information obtained or
created during the performance of laboratory activities, except as required by law.
All personnel of the laboratory, either internal or external, that could influence the laboratory
activities shall act impartially, be competent and work in accordance with the laboratory’s
management system.
Section 4.2.1.2: Risk and Opportunity Assessment
Actions taken to address risks and opportunities shall be proportional to the potential impact on the
validity of laboratory results.
Section 4.3.1: Document Control – General
All documentation, processes, systems, records, related to the fulfilment of the requirements of
ISO/IEC 17025 are included in, referenced from, or linked to the management system. All
personnel involved in laboratory activities have access to the parts of the management system
documentation and related information that are applicable to their responsibilities.
Section 4.4: Analytical Service Request, Tender, and Contract Review
If a contract is amended after the work has commenced, the contract review shall be repeated and
any amendments shall be communicated to all affected personnel.
Section 4.13.2.3: Error Correction
Amendments to technical records can be tracked to previous versions or to original observations.
Both the original and amended data and files are retained as applicable, including the date of
alteration, an indication of the altered aspects and the personnel responsible for the alterations.
Section 4.14.1: Internal Audit
Quality System Audits: A review of all management system requirements of ISO/IEC 17025
and any other regulatory or applicable policy document (e.g., AIHA-LAP, LLC). These
audits are also performed annually per a pre-determined schedule.
Section 5.5.2: Calibration
Laboratory staff performing in-house calibrations and verifications shall have received documented
training.
Section 5.5.7: Calibration Status
Measuring equipment shall be calibrated when:
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The measurement accuracy or measurement uncertainty affects the validity of the reported
results, and/or
Calibration of the equipment is required to establish the metrological traceability of the
reported results
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8.3 ADDENDUM: SOP Review
DoD and drinking water SOPs are reviewed annually.
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8.4 ADDENDUM: RADIOLOGICAL REQUIREMENTS
8.4.1 Estimate of Analytical Uncertainty
Radiological tests often report uncertainty and the manner in which it is derived are in
accordance with Multi-Agency Radiological Laboratories Analytical Protocols Manual
(MARLAP) and Evaluation of Measurement Data – Guide to the Expression of Uncertainty
in Measurement (GUM). The means by which these criteria are applied can be found in the
method SOPs.
8.4.2 Radiological Equipment Calibration
Radiological calibrations may follow one of several methodologies based on technology of
the counting; these can include efficiency curves, energy calibrations and quench curves. The
various calibrations should ensure that the range chosen encompasses the activities expected
in the client samples.
Radiological Equipment should be calibrated at the appropriate frequency and whenever the
equipment undergoes maintenance. In the case of liquid scintillation counters the equipment
shall be recalibrated when a significant move has taken place.
Calibrations can vary with equipment; in the case of gas flow proportional counters standards
that range the expected residue range for gross alpha and beta shall be used, with efficiency
curves developed to encompass the range of client sample residues. Any samples outside of
this range shall be evaluated and the aliquot changed to accommodate the curve if necessary.
Beta emitters, or isotopes that are shown to have less than a 2% efficiency change with residue
that are known to not experience self attenuation may be calibrated by using a least 3
standards of known activity and comparing the efficiency results to ensure all agree to a
relative standard deviation of less than 5%.
Quench factors for liquid scintillation counters shall be prepared by adding varied amounts
of quenching agent. Any sample displaying a quench factor outside of the curve shall be
evaluated. If the quench factors are shown to not vary in efficiency by greater than 2% then
an efficiency calibration can be established using at least 3 standards of known activity and
comparing the efficiency results to ensure all agree to a relative standard deviation of less
than 5%.
Cross talk factors must also be evaluated when samples are known to contain more than one
beta or an alpha and beta emitter.
All detectors must pass various daily tests depending upon the technology. The criteria of
these various tests should be known to the analyst. Any detector that does not pass the daily
check must be re-checked.
If the daily test fails a second time the detector must be taken out of service for that day. Any
detector that fails two daily checks must be evaluated and serviced if required. In most
instances two passing daily checks are required to put a detector back into service.
8.4.3 Matrix Spike/Matrix Spike Duplicate (MS/MSD)
For radiochemical analyses, tests that do not incorporate the use of a carrier or tracer for
yield assessment must contain an associated MS and MSD (or sample duplicate) using the
same matrix collected for the specific DOD project. Gamma spectroscopy analyses are
excluded from the MS/MSD requirement as the test does not require chemical processing of
samples for analysis
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8.5 ADDENDUM: QUALITY CONTROL CALCULATIONS
PERCENT RECOVERY (%REC)
=100
NOTE: The SampleConc is zero (0) for the LCS and Surrogate Calculations
PERCENT DIFFERENCE (%D)
=100
where:
TrueValue = Amount spiked (can also be the CF or RF of the ICAL Standards)
Measured Value = Amount measured (can also be the CF or RF of the CCV)
PERCENT DRIFT
=
RELATIVE PERCENT DIFFERENCE (RPD)
=+100
where:
R1 = Result Sample 1
R2 = Result Sample 2
CORRELATION COEFFICIENT (R)
CorrCoeff =
With: N Number of standard samples involved in the calibration
i Index for standard samples
Wi Weight factor of the standard sample no. i
Xi X-value of the standard sample no. i
X(bar) Average value of all x-values
Yi Y-value of the standard sample no. i
Y(bar) Average value of all y-values
N
i
iii YYXXW
1
)(*)(*
N
i
ii
N
i
ii YYWXXW
1
2
1
2 )(**)(*
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CALIBRATION FACTOR (CF)
CF =
A
where:
As = Average Peak Area over the number of peaks used for quantitation
Cs = Concentration of the analyte in the standard
RESPONSE FACTOR (RF)
)Area)(.(Conc
)Area)(.(Conc=RF
IStdanalyte
AnalyteIStd
where:
As = Response for analyte to be measured
Ais = Response for the internal standard
Cis = Concentration of the internal standard
Cs = Concentration of the analyte to be measured
LINEAR CALIBRATION MODEL
=+
where:
m = Slope of the line
b = The y intercept
QUADRATIC CALIBRATION MODEL
=2 ++
where:
c = The y intercept
STANDARD DEVIATION (S)
=
=
()
where:
n = number of data points
Xi = individual data point
X = average of all data points
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AVERAGE (X)
==1
where:
n = number of data points
Xi = individual data point
RELATIVE STANDARD DEVIATION (RSD)
=100
where:
S = Standard Deviation of the data points
X = average of all data points
PERCENT ERROR
=
'
100
where:
x´i = Measured amount of analyte at calibration level i
xi = True amount of analyte at calibration level i
RELATIVE STANDARD ERROR (RSE)
=100 ×
=1
[']
2
where:
xi = True amount of analyte at calibration level i
x´i = Measured amount of analyte at calibration level i
p = Number of terms in fitting equation (Average = 1, Linear = 2, Quadratic = 3)
n = Number of calibration points
AVERAGE RESPONSE 1/X FOR MASS HUNTER INSTRUMENTS
1
= =1
1
=1(())
where:
As = Response for analyte to be measured
Ais = Response for the internal standard
Cis = Concentration of the internal standard
Cs = Concentration of the analyte to be measured
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MINIMUM DETECTABLE ACTIVITY (MDA)
The MDA is used for radiochemical analysis and is calculated with the following equations:
MDA with Blank Population

3.29
+
3
MDA =
Where:
K = E × V × R × Y × F × 2.22
E = efficiency
V = sample volume
R = tracer recovery
Y = gravimetric carrier recovery
F = ingrowth or decay factor
2.22 = conversion from dpm to pCi
Ts = count time of sample in minutes
Sb = standard deviation of the blank population
MDA without Blank Population

3.29 +
+
3
MDA =
Where:
b = background count rate in cpm
Tb = Count time of background in minutes
Relative Error Ratio (RER)/Normalized Absolute Difference (NAD)/Duplicate Error Ratio (DER)
RER, NAD, and DER are used for radiochemical analysis and are calculated by the following:
Where:
S = Sample Value
US = Sample Uncertainty (at 2 sigma)
R = Replicate Value
UR = Replicate Uncertainty (at 2 sigma)