DSHW-1996-002318 - 0901a0688013a4c4

ENVIRONMENTAL BASELINE ASSESSMENT
Bacchus Plant 3 ^?(P/^^^
Magna, Utah REGEIVFD
Hercules, Inc.
Hercules Plaza, 1313 Market Street
Wilmington, DE 19898-0001
UTAH DIVISION OF
SOLID & HAZARDOUS WASTE
30 September, 1996
ERM-Rocky Mountain, Inc.
102 West 500 South, Suite 650
Salt Lake City, Utah 84101-2334
[phone]
ERM

ENVIRONMENTAL BASELINE ASSESSMENT
Bacchus Plant 3
Magrui, Utah
Hercules, Inc.
Hercules Plaza, 1313 Market Street
Wilmington, DE 19898-0001
30 September, 1996
ERM-Rocky Mountain, Inc.
102 West 500 South, Suite 650
Salt Lake City, Utah 84101-2334
[phone]

TABLE OF CONTENTS
1.0 INTRODUCTION 1
1.1 SITE DESCRIPTION 1
1.2 SITE HISTORY AND PROJECT BACKGROUND 3
2.0 SCOPE OF WORK 4
2.1 COLLECTION OF SOIL, SURFACE WATER, AND SEDIMENT SAMPLES 4
2.1.1 Surface Soil Samples 4
2.1.2 Surface Water Samples 5
2.1.3 Sediment Samples 6
2.1.4 Soil-Gas Sample Collection 7
2.2 INSTALLATION AND SAMPLING OF GROUND WATER MONITORING 8
WELLS 8
3.0 FINDINGS 11
3.1 STANDARDS AND COMPARISON CRITERIA 11
3.1.1 Surface Soil Samples 11
3.1.2 Surface Water Samples 11
3.1.3 Sediment Samples 12
3.1.4 Soil-Gas Samples 12
3.1.5 Ground Water Samples 12
3.2 RESULTS 12
3.2.1 Surface Soil Samples 12
3.2.2 Surface Water Samples 13
3.2.3 Sediment Samples 13
3.2.4 Soil-Gas Samples 14
3.2.5 Ground Water Samples 14
4.0 CONCLUSIONS 15
5.0 REFERENCES 16

LIST OF TABLES
Table 1-1 Bacchus Pond Influent Summary
Table 2-1 Soil-Gas Analytes
Table 3-1 Ground Water Elevation Measures
Table 3-2 Surface Water Sample Results
Table 3-3 Judgmental Sediment Sample Results
Table 3-4 Statistical Sediment Sample Results
Table 3-5 Ground Water Sample Results
Table 3-6 Soil-Gas Survey Sample Results
LIST OF FIGURES
Figure 1-1 Bacchus Plant 3 Layout
Figure 1-2 Bacchus Pond
Figure 2-1 Soil-Gas Sampling Locations
Figure 2-2 Hydrogeological Cross Section
LIST OF APPENDICES
Appendix A Bacchus Lake Enviromnental Investigation Workplan
Appendix B Soil-Gas Borehole Logs
Appendix C Ground Water Monitoring Well Borehole Logs
Appendix D Laboratory Reports (Under Separate Cover)

1.0 INTRODUCTION
ERM, Inc. was retained by Hercules Incorporated (Hercules) to perform a
Baseline Enviroimiental Assessment at the Hercules Bacchus Plant 3 facility in
Magna, Utah. Because of its proximity to the subject property, ERM-Rocky
Mountain, Inc. of Salt Lake City, Utah performed the site investigation
described in this report under subcontract to ERM, Inc. This report has been
prepared jointly by ERM, Inc. and ERM-Rocky Mountam, Inc., which are
hereafter referred to as ERM. This assessment was conducted to provide an
environmental baseline, particularly for Bacchus Pond, at the time Bacchus
Plant 3 was sold by Hercules to Hexcel Corporation (Hexcel). The Baseline
Assessment consisted of soil, sediment, and surface water sampling and analysis
from Bacchus Pond; monitoring well installation, sampling, and analysis; and a
soil gas survey at select plant locations. This assessment was completed to
conform with the "Bacchus Lake Environmental Investigation Workplan"
(provided as Appendix A) and additional activities agreed to by Hercules and
Hexcel.
1.1 SITE DESCRIPTION
The layout of Bacchus Plant 3 (Plant 3) is shown in Figure 1-1. Plant 3 is
117.28 acres in size and houses graphite fiber and composite products
manufacturing operations.
Bacchus Pond was constructed in the early 1970s to contain non-contact cooling
water from the Plant 3 operations. The pond was constructed by placing an
earthen berm around a namral depression where the pond now exists. The pond
is approximately 500 feet long with an average width of 220 feet (approximately
2.5 acres in area) and has a maximum depth of approxunately 11 feet. A
discharge culvert is located at the north end of the pond. When water
discharges from the pond, it flows in a northeast direction onto property now
owned by Aliiant, where it evaporates or infiltrates into the subsurface. It is
reported that discharge from Bacchus Pond does not flow into any other body of
surface water.
Five influents to Bacchus Pond have been identified. These influents include:
four non-contact cooling water (CW) discharges (CW-1 through CW-4) and a
storm water discharge (CW-5). Although the storm water discharge does not
contain cooling water, it was designated as CW-5 by Plant 3 persormel for
consistency. The locations of CW-1 through CW-5 are shown in Figure 1-2.
All five influents originate on Bacchus Plant 3 property which is now owned by
Hexcel. Additional information regarding each influent is listed on Table 1-1.
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Table 1-1 Bacchus Pond Influent Summary
Influent Source Description
Flow
Characteristics
CW-1 Fiberlines 1, Discharges to Hexcel property from a heavily
2, and 3 silted corrugated metal pipe approximately 30 feet
south of Bacchus Pond. Flows beneath the fence
onto Hercules' property to the marsh area south
of the pond.
CW-2 Pilot Line Discharges to Hercules property from a 15-inch
diameter corrugated metal pipe approximately 50
feet from Bacchus Pond and then flows in an open
channel approximately 6 inches deep and 1 to 2
feet wide to Bacchus Pond.
Approximately
200 gpm*;
primarily laminar
flow.
Approximately 30
gpm*; primarily
laminar flow.
CW-3
CW^
CW-5
Fiberlines 4,
5, 6, and 7
Oil heater
cooling
water
(Building
2344)
Storm water
discharge
Flows through an open channel approximately 2
feet deep and 3 to 5 feet wide which is lined with
gravel and cobble.
Discharges to Hercules property though a heavily
silted 12-inch diameter iron pipe approximately
75 feet east of Bacchus Pond.
Discharges to Hercules property through a 30-
inch diameter corrugated metal pipe. Very low
flows of storm water were observed at the time of
this investigation, but the heavily eroded channel
(approximately 4 feet deep) below the outlet pipe
indicates that large flows have occurred from
CW-5 in the past.
Approximately
140 gpm*;
turbulent flow in
places.
Intermittent Flow.
Intermittent Flow.
* Approximate flow based on the average of three flows measured by Plant 3 personnel
(12/19/94, 2/23/94, and 9/5/95).
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1.2 SITE HISTORY AND PROJECT BACKGROUND
Plant 3 was originally part of the larger Hercules Bacchus Works. Bacchus
Works consisted of approximately 7,400 acres, which included Plant 1, Plant 3,
NIROP, and Bacchus West. In March 1995, Aliiant Techsystems (Aliiant)
purchased Plant 1 and Bacchus West from Hercules. Aliiant also became
responsible for the operation of NIROP at that time. Hercules retained the
ownership and operation of Plant 3 until June 1996 when it was sold to Hexcel.
Prior to the Aliiant transaction, numerous ground water monitoring wells were
installed within Bacchus Works. A total of 75 monitoring wells were installed
on property now owned by Aliiant. One well, GW-58, which is located on
Aliiant property approximately 300 feet downgradient from Bacchus Pond, has
shown low concentrations of 1,1,1 trichloroethane (TCA), 1,1-dichloroethene
(DCE) and 1,1-dichloroethane (DCA). Both DCE and DCA are believed to be
decomposition products of TCA. These chemicals were first identified in Well
GW-58 in the third quarter of 1993 after several quarters of monitoring without
detection. Installation of Well GW-58 was completed on 20 February 1988,
and quarterly sampling of GW-58 was begun during 1988. TCA concentrations
ranging from 6 to 12 part per billion (ppb), DCE concentrations ranging from 5
to 7 ppb, and a DCA concentration of 5 ppb have been detected in GW-58.
At the request of Mr. Bill Wallner of the Utah Department of Environmental
Quality (DEQ) Division of Solid and Hazardous Waste (DSHW), Hercules
submitted the "Bacchus Lake Enviroimiental Investigation Workplan" to the
DSHW on 2 August, 1995 to evaluate whether Bacchus Pond is the source of
ground water contamination detected in GW-58. This workplan outlined the
collection of 7 sedunent samples from Bacchus Pond. A copy of this workplan
is included as Appendix A. No written comments were received from the
DSHW regarding the workplan prior to the performance of this assessment.
However, when contacted regarding the Environmental Baseline Assessment,
Mr. Wallner commented that DSHW may require more work than that proposed
in the 2 August 1995 Workplan, but he had no objections to the planned
baseline activities.
At the request of Hercules, ERM performed a modified Phase I Environmental
Site Assessment of Plant 3 in February and March of 1996 in anticipation of a
potential sale of the facility. Plant 3 was purchased from Hercules by Hexcel in
June 1996, except for Bacchus Pond and some adjoining ground which was
retained by Hercules.
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2.0 SCOPE OF WORK
The scope of work for this assessment included 1) the collection of soil, surface
water, and sediment samples from Bacchus Pond and its influent streams; 2) the
collection of soil-gas samples; and 3) the installation of ground water
monitoring wells and the collection of ground water samples. These three tasks
are described in the following sections. All sampling was performed in
accordance with the "Bacchus Lake Environmental Investigation Workplan" and
ERM's "Standard Operating Procedures for the Collection of Environmental
Samples," (SOP) (Rev. February 1991).
2.1 COLLECTION OF SOIL, SURFACE WATER, AND SEDIMENT
SAMPLES
ERM collected soil, surface water, and sediment samples on 26 and 27 June
1996 from Bacchus Pond and its influent streams. Non-disposable equipment
used for the collection, preparation, preservation, and storage of samples was
cleaned prior to its use and after each subsequent use. The following
decontamination procedures were followed for all non-disposable equipment:
• manual scrub with a non-phosphate detergent;
• rinse with deionized/distilled water;
• rinse with 10%-dilute nitric acid;
• rinse with pesticide-grade methanol;
• triple rinse with deionized/distilled water; and
• air dry.
Samples were shipped ovemight by Federal Express to Lancaster Laboratories
Inc. (Lancaster) of Lancaster, Pennsylvania for analyses. The sample collection
procedures and the analyses performed are described in the following sections.
2.1.1 Surface Soil Samples
Three surface soil samples were collected within the fenced area of Bacchus
Pond to represent background soil conditions. These samples were identified as
Soil-1 through Soil-3. Approximate sample locations are marked in Figure 1-2.
Wooden stakes were placed at these locations for future reference. Samples
were collected 6-12 inches below ground surface using hand trowels which were
decontaminated prior to collection of each sample. A blind duplicate sample
(Soil-4) was collected from the same location as sample Soil-2. A hand trowel
rinsate blank was also collected.
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The three soil samples, the blind duplicate, and the rmsate blank were all
analyzed for the thirteen (13) Priority Pollutant Metals (antimony, arsenic,
beryllium, cadmium, chromium, copper, lead, mercury, nickel, selenium,
silver, thallium, and zinc), plus aluminum, barium, iron, and manganese using
methods SW-846 6010A and SW-846 7471A.
2.1.2 Surface Water Samples
Water samples were collected from four discharges to Bacchus Pond, from
"judgmental locations withm the pond," and from the Bacchus Pond outfall.
2.1.2.1 Discharge Water Samples
Discharge water samples (CW-1 DISC, CW-2 DISC, CW-3 DISC, and CW-5
DISC) were collected from the influents which discharge into Bacchus Pond at
locations unaffected by water in the pond. Approximate locations from which
these samples were collected are shown in Figure 1-2. A discharge water
sample could not be collected from CW-4 because there was no water flowing at
the tune of sampling. A sediment sample (CW-4 DISC) was therefore collected
in place of a water sample at the CW-4 discharge point. This sample (CW-4
DISC) was analyzed for the same parameters as the discharge water samples.
All discharge water samples were analyzed for the following parameters:
• Volatile Organic Compounds (SW-846 8240);
• Semi-Volatile Organic Compounds (SW-846 8270); and
• Thirteen (13) Priority Pollutant Metals, plus aluminum, barium, iron,
and manganese (SW-846 6010A and 7470 A).
2.1.2.2 Judgmental and Outfall Water Samples
Bacchus Pond water samples (CW-1 JUD through CW-4 JUD, and Outfall
JUD) were collected from a small boat prior to the collection of any sediment
samples to minimize disturbance of the pond sediment. These sample locations
were established where the influent streams discharge into Bacchus Pond as
described in the workplan submitted by Hercules to the DSHW. Samples were
collected approximately one foot beneath the water surface using the sample
bottles.
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Because of the proximity of discharges from CW-2 and CW-5 to Bacchus Pond
and limited access due to excessive vegetation, a single judgmental sample
(CW-2 JUD) was collected to represent both discharges.
Approximate locations where judgmental water samples were collected are
shown in Figure 1-2. Steel stakes were driven into the bottom of the pond at
the judgmental sample locations for fiiture reference.
All judgmental water samples were analyzed for the following parameters:
• Volatile Organic Compounds (SW-846 8240);
• Semi-Volatile Organic Compounds (SW-846 8270);
• Thirteen (13) Priority Pollutant Metals, plus aluminum, barium, iron, and
manganese (SW-846 6010A and 7470 A); and
• Pesticides and PCBs (SW-846 8081).
A blind duplicate (CW-6 JUD) was collected from the same location as sample
CW-2 JUD. A matrix spike sample (CW-1 JUD MS) and a matrix spike
duplicate sample (CW-1 JUD MSD) were also collected. No rinsate blanks
were collected because all water samples were collected directly into the sample
bottles, and no sampling equipment was used.
2.1.3 Sediment Samples
Sediment samples were collected from the judgmental locations (CW-1 JUD
through CW-4 JUD) and four "statistical locations" (STAT-1 through STAT-4).
The judgmental sediment samples were collected from the same locations
where the judgmental water samples were collected as described in Section
2.1.2. Statistical sediment samples were collected from four locations as
described in the workplan which Hercules submitted to the DSHW. The
statistical sampling locations (STAT-1 through STAT-4) and the sampling grid
are shown in Figure 1-2.
Two (2) sedunent samples were collected from each sampling location where
samples were reasonably attainable. The first sample was collected from the
top 2 to 3 mches of sediment on the bottom of the pond. The second sample
was collected from the bottom of the sediment profile (i.e., if the sediment
profile was more than 2 to 3 inches thick) or from the maximum depth to which
the sampling equipment could be advanced. The sediment samples were
collected from the bottom of Bacchus Pond using a small boat and a 3 inch
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diameter open bucket soil auger. Other sampling techniques were tested;
however, gravel and cobble at the bottom of the pond prohibited their
effectiveness.
2.1.4 Soil-Gas Sample Collection
ERM collected soil-gas samples during two soil-gas samplmg events. The first
event was conducted on August 5 and 6, 1996, during which time ERM
employed EarthProbe Environmental Services, Inc. (EarthProbe) to advance
Geoprobe® equipment to the appropriate sampling depths. However, the
Geoprobe equipment was not able to complete the soil-gas sampling at all
locations because of gravel and cobble in the subsurface. ERM ±en retained
Foundex Pacific, Inc. (Foundex) for the second event to provide drilling
services using their Becker-Hammer drilling equipment which had been adapted
for direct-push drilling to complete the soil gas sampling. This second sampling
event was performed on August 23 and 24, 1996.
The samples were collected from locations of historical solvent or coolant spills,
active and abandoned collection sumps, former underground storage tanks, and
above ground storage tanks. As shown in Figure 2-1, twelve (12) sample
locations were originally designated for sampling; soil-gas samples were
collected from seven locations. The other five locations were reviewed with
Hexcel personnel and not completed due to access and utility obstructions.
The soil-gas samples were collected from depths of 10, 15, 20 , and 30 feet
below ground surface (bgs) from accessible locations where penetration was
achievable. Samples were collected using the Geoprobe equipment from SG-1
and SG-3 where penetration to depths of 30 and 25 feet, respectively, where
accomplished. Samples were also collected at shallow depths from other
locations with the Geoprobe, but were not analyzed as it was anticipated that
deeper samples would later be obtained using other drilling techniques.
Samples were successfully collected from five additional locations (SG-4, SG-6,
SG-7, SG-10, and SG-12) usmg the Becker-Hammer drilling equipment. The
remaining five locations were inaccessible due of the size of the drilling rig and
the presence of overhead powerlines and underground utilities.
ERM's field representative classified the soil types for each borehole using the
Unified Soil Classification System (USCS) for development of borehole logs.
These borehole logs are mcluded as Appendix B.
Soil-gas samples were collected usmg disposable PVC tubing and a peristaltic
pump and were placed in 1 liter Tedlar Bags. Samples were also observed for
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evidence of volatile organics using a Photo Ionization Detector (PID).
Detectable PID readings were noted on the borehole logs. The samples were
shipped to Exton, Pennsylvania and tested by ERM's Field Analytical Services
Technology (ERM-FAST) for the parameters listed on Table 2-1. A bluid
duplicated and a field blank were also analyzed for each set of 20 samples (5 %
QA/QC).
Table 2-1 Soil-Gas Analytes
Carbon Tetrachloride
Chloroethane
Chloroform
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene (DCE)
cis-l ,2-Dichloroethene
trans-1,2-Dichloroethene
Dichloromethane (Methylene Chloride)
Tetrachloroethene (PCE)
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
1,1,1-Trichloroethane (TCA)
1,1,2-Trichloroethane
Trichloroethene (TCE)
Vinyl Chloride
Benzene
Toluene
Ethylbenzene
o-Xylene
m-, p-Xylene
Trichlorofluoromethane (Freon 11)
Dichlorodifluoromethane (Freon 12)
1,1,2-Trichloro-trifluoroethane
(Freon 13)
Methyl Ethyl Ketone (MEK)
After the soil-gas samples were collected and the drilling equipment was
removed from the borehole, each borehole was filled with bentonite.
Boreholes drilled through asphalt or concrete were patched with quick dry
concrete. All drilling equipment was steam-cleaned before each use.
2.2 INSTALLATION AND SAMPLING OF GROUND WATER MONITORING
WELLS
Three 2-inch diameter monitoring wells were installed adjacent to Bacchus
Pond. The approximate locations of these wells are shown in Figure 1-2.
Wells BP-1 and BP-3 were installed downgradient from Bacchus Pond based on
regional ground water flow information. During well construction, the
midpoint of the well screen interval was placed at the first water bearing zone.
Well BP-1 was installed in a perched ground water zone and Well BP-3 was
installed to a depth representative of the regional ground water table. Well
BP-2 was installed upgradient from Bacchus Pond to a depth consistent with the
regional water table. Wells BP-1 and BP-2 were installed between 30 July 1996
and 1 August 1996. Well BP-3 was installed between 21 and 23 August 1996.
Layne Christensen Company (Layne) and Foundex Pacific, Inc. (Foundex) were
retained to install and develop the wells.
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ERM's field representatives examined the drill cuttings to classify the soil types
for development of borehole logs. The borehole and well construction logs are
included as Appendix C. Borehole cuttings were observed for evidence of
volatile organics using a Photo Ionization Detector (PID). Detectable PID
measurements were noted on the borehole logs.
All drilling equipment was steam-cleaned before each use. Drill cuttings and
purge water were placed in 55 gallon drums and stored on Hercules' property.
Perched water tables were encountered at depths of 38 and 113 feet bgs during
installation of Well BP-1. Ground water samples were collected from each of
these depths. Disposable Teflon bailers were used to purge the borehole at each
of these depths, until no water could be collected in the bailer. After the
borehole recharged with ground water, a sample was collected using the bailer.
These samples were analyzed for the following parameters:
• Volatile Organic Compounds (SW-846 8240);
Semi-Volatile Organic Compounds (SW-846 8270); and •
• Thirteen (13) Priority Pollutant Metals, plus alununum, barium, iron, and
manganese (SW-846 6010A and 7470 A).
The samples analyzed for metals were collected in 1 liter polyethylene bottles
without preservatives. These samples were filtered by the laboratory prior to
analysis.
No perched ground water conditions were encountered in Wells BP-2 or BP-3.
Well BP-2 was sampled on 9 August 1996 and 5 September 1996. Well BP-3
was also sampled on 5 September 1996. These samples were analyzed for
VOCs using the analytical method listed above as requested by Hercules as part
of the monthly Bacchus Pond sampling program. Laboratory results for
samples collected on 5 September 1996 and subsequent sampling events will be
reported in the monthly sampling reports.
The depths to water were measured by ERM in Wells BP-1, BP-2, and BP-3 on
30 August 1996. The depth to water in Well GW-58 was measured by Allen
Lee of Aliiant on 27 August 1996. Measured ground water elevations are
presented on Table 2-2. Aliiant provided additional ground water monitoring
data which confirms that regional ground water flow is towards the north-
northeast. As shown on Table 2-2, ground water elevations downgradient from
Bacchus Pond (Wells BP-3 and GW-58) are higher than the elevation measured
upgradient in Well BP-2. Well BP-2 is referred to as the upgradient well based
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on the regional ground water flow direction as described in available literature
and data collected by Aliiant. The elevated ground water condition detected in
Wells BP-3 and GW-58 is believed to be due to recharge from Bacchus Pond to
the regional ground water flow. A cross section showing the screened intervals
and measured ground water elevations of Wells BP-2, BP-3, and GW-58 is
shown in Figure 2-2. No ground water was detected in Well BP-1 (perched
zone) at the time the measurements were performed. Based on the
potentiometric levels, as shown in Figure 2-2, it appears that these wells
monitor the same hydrologic zone. It should also be noted that borehole logs
for these wells show no confining layers.
Table 2-2 Ground Water Elevation Measurements
Ground
Ground Surface Screened Interval Top of Casing Depth to Water
Well Elevation Elevation* Elevation Water Elevation
Location (feet) (Feet-rounded) (feet) (feet) (feet)
GW-58 4967.79 4624 to 4608
(344 to 360)
4969.64 182.57 4787.07
BP-1 4968.42 4868 to 4848
(100 to 120)
4970.76
BP-2 4991.00 4777 to 4757
(214 to 234)
4993.31 210.90 4782.41
BP-3 4968.55 4784 to 4764
(185 to 205)
4970.47 153.42 4817.05
* The interval each well is screened is shown in parenthesis (feet below groimd surface).
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3.0 FINDINGS
The analytical results from the Environmental Baseline Assessment have been
summarized and separated into Tables 3-1 through 3-6 based upon the sample
media (i.e., soil, surface water, judgmental sediment, statistical sediment, soil-
gas, and ground water). These tables only present compounds detected above
method detection limits (MDLs). Copies ofthe laboratory analytical reports are
included as Appendix D. Monthly surface water and ground water sampling
results will be compared to these baseline data in later reports.
3.1 STANDARDS AND COMPARISON CRITERIA
The sample results are compared on the summary tables with applicable
standards or reference criteria which are described in the following sections.
These comparison standards and criteria are also briefly described at the bottom
of each table. The site concentrations exceeding any of these comparison
standards or criteria have been highlighted in bold text on the tables for easy
identification. Many of these values (bolded) are below lunits of quantitation
and are estimated ("J" values) or are representative of background conditions
and may not be site related.
3.1.1 Surface Soil Samples
The surface soil sample results are compared agamst the range of metals
concentrations typically found in westem U.S. soils (Shacklette, 1984). ERM
has used the results from the three background samples to develop a statistical
"Upper Background Liinit" for the soil near Bacchus Pond (90% one-tailed
upper tolerance limit). These limits are compared against the sediment sample
data.
3.1.2 Surface Water Samples
In the absence of applicable surface water standards for non-discharging
industrial water, the surface water sample results are not compared against any
standards or comparison criteria. The baseline surface water sample results will
be used to evaluate influent surface water quality during fiiture monthly
sampling events to identify changes in water quality.
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3.1.3 Sediment Samples
Sediment sample metals concentrations are compared against the "Upper
Background Limits" which were statistically calculated from the three
background soil samples collected near Bacchus Pond (90 % one-tailed upper
tolerance limit).
3.1.4 Soil-Gas Samples
The soil-gas sample results are not compared against any standards or criteria.
The soil-gas samples were analyzed for VOCs that do not namrally occur in the
subsurface. Detection of VOCs in the soil-gas samples represent migration of
VOCs in the vadose zone.
3.1.5 Ground Water Samples
The ground water sample results are compared against the Utah DEQ Ground
Water Quality Standards (GWQSs) (Utah R317-6).
3.2 RESULTS
The results from the Environmental Baseline Assessment are discussed in the
following sections.
3.2.1 Surface Soil Samples
Analytical results for the three surface soil (background) samples collected are
summarized on Table 3-1. As shown on Table 3-1, none of the metals
concentrations in the three samples exceeded the range of metals concentrations
typically found in westem U.S. soils.
The results from the three surface soil samples were used to develop a statistical
"Upper Background Limit" for the soil near Bacchus Pond (90% one-tailed
upper tolerance limit) for comparison with the sedunent sample data.
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3.2.2 Surface Water Samples
Surface water sample results are presented on Table 3-2. Low levels of certain
VOCs and SVOCs (acetone, bromodichloromethane, 2-butanone, and
chloroform) were detected in select surface water samples. The detection of
silver at a concentration of 646 ^ig/L in Sample CW-4 JUD is also noteworthy;
silver was not detected in any other water samples .
3.2.3 Sediment Samples
Analytical results for the sediment samples collected are suinmarized on Tables
3-3 and 3-4. As shown on Table 3-3, judgmental sample CW-1 (0-3")
contained barium and mercury concentrations which exceeded the background
concentrations established from the soil analytical data. Judgmental sample
CW-3 (0-3") contained copper, mercury, selenium, and zinc concentrations
which exceed background concentrations.
As shown on Table 3-4, statistical sample STAT-1 (0-3") contained arsenic
concentrations above the background level. STAT-3 (0-3") contained copper,
selenium, and zinc concentrations which exceeded background levels.
Low levels of certain VOCs, SVOCs, and pesticides/PCBs were also detected in
judgmental and statistical sediment samples (Tables 3-3 and 3-4). Acetone was
detected in all of the sediment samples except STAT-4 (6-10") in concentrations
ranging from 9J to 120 |ig/kg. Other compounds detected in sediment samples
include: benzene (IJ to 2J |ig/kg); 2-butanone (IOJ to 15J i^g/kg); methylene
chloride (3J to 5J |ig/kg); toluene (200 |ag/kg); bis (2-ethylhexyl) phthalate
(lOOJ to 1000 }ig/kg); di-n-butyl phthalate (41 to 46J iig/kg); gamma chlordane
(2J |ig/kg); and PCB-1260 (40J pg/kg). ERM reviewed the field blank and trip
blank results to assess whether these compounds may have been introduced
during sample collection or laboratory analysis; however, only methylene
chloride appeared in the blank samples.
CW-4 DISC, the soil sample collected in place of a water sample, is also
presented on Table 3-3 and compared against the same criteria as the sediment
samples. CW-4 DISC contained metals concentrations (arsenic, copper, iron,
lead, selenium, and zinc) which exceed background concentrations. Low levels
of the following VOCs and SVOCs were also detected in CW-4 DISC:
methylene chloride, bis (2-ethylhexyl) phthalate, di-n-butyl phthalate, and di-n-
octyl phthalate. Methylene chloride was detected in the trip blank and may be a
laboratory contaminant.
ERM-ROCKY MOUNTAIN, INC. 13 P:\U69005.Her\Report4.doc
3.2.4 Soil-Gas Samples
Analytical results for the soil-gas samples collected are presented on Table 3-5.
1,1-Dichloroethene was detected in SG-1 at depths of 10 and 30 feet and in SG-
3 at depths of 10, 20, and 25 feet in concentrations ranging from 7 to 78 ppm.
1,1,1-Trichloroethane was detected in SG-1 at depths of 10, 20 and 30 feet; SG-
3 at depths of 10, 20, and 25 feet; SG-6 at depths of 15 and 20 feet; and SG-7
at a depth of 20 feet in concentrations ranging from 1J to 270 ppm. None of the
other analytes were detected in any of the soil-gas samples analyzed.
3.2.5 Ground Water Samples
Analytical results for the ground water samples collected are presented on Table
3-6. The perched ground water samples BP-1:38 and BP-1:113 contained
certain dissolved metals concentrations which exceed the Utah GWQSs.
Chromium (113 and 523 |ag/L) and lead (31 and 260 |ig/L) were detected in
both samples at concentrations exceeding the Utah GWQSs. Barium (3,670
|j.g/L) was also detected in BP-1:38 at a level exceedmg the standard.
Low levels of certain VOCs and SVOCs were detected in the ground water
samples. None of the measured concentrations exceed Utah GWQSs.
Tetrachloroethene (4J )ag/L) was detected in BP-1:38. Acetone (30 |ig/L) and
bis (2-ethylhexyl) phthalate (5J )ig/L) were detected in BP-1:113. Acetone (7
|j.g/L), chloroform (1 |ig/L), 1,1-dichloroethene (6 |ig/L), and 1,1,1-
trichloroethane (8 lig/L) were detected upgradient from Bacchus Pond in BP-2.
The first sampling and analysis of ground water from Well BP-3 was conducted
on 5 September 1996. The results showed only estimated quantities (i.e., below
the laboratory Limits of Quantitation) of acetone (17 J ng/L) and 2-butanone
(4J ng/L) in the sample from this well. There were no detections of chlorinated
solvents.
Except for the presence of acetone (30 and 17 J|J.g/L) and possible presence of
2-butanone (4J ^g/L) and tetrachloroethene (4J |ig/L) at low concentrations in
the downgradient water samples, there is no evidence of impacts to ground
water from Bacchus Pond based on the current data. Monthly ground water
sampling of the monitoring wells should provide additional data regarding the
water quality downgradient from Bacchus Pond.
ERM-ROCKY MOIWTAJN, INC. 14 P:\U6900S.HrrVRcport4.diK
4.0 CONCLUSIONS
The main conclusion of the baseline study is that TCA and other chlorinated
compounds detected in the regional ground water were not detected in the
Bacchus Pond surface water, sediment, or ground water samples (BP-1:38, BP-
1:113 and BP-3). Bacchus Pond therefore is not considered a source of these
compounds because TCA or related chlorinated compounds were not detected in
the Bacchus pond surface water, sediment or ground water samples collected
north of the pond during this assessment.
The presence of chlorinated organic compounds in the soil gas and regional
ground water flow regime (i.e.. Well BP-2) suggest the presence of potential
sources of these compounds upgradient (south) from Bacchus Pond. The soil
gas data mdicate the presence of subsurface chlorinated compounds (TCA and
DCE) in the area of the TCA storage tank on the west side of the property
(Samples SG-1 and SG-3), were a release reportedly occurred in 1988. Lower
soil gas concentrations of TCA were detected within Plant 3 directly south of
Bacchus Pond in the vicinity of the TCA storage tanks near Building 2344.
ERM-ROCKY MOUNTAIN, INC. 15 P:\U69a05.Htr\Rtport4.doc
5.0 REFERENCES
Hercules Incorporated Composite Products Division; 1995. Bacchus Lake
Environmental Investigation Workplan.
Shacklette, H.T., and Boemgen, J.G.; 1984: Element Concentrations in Soils
and other Surficial Materials ofthe Conterminous United States. U.S.
Geological Surv. Professional Paper 1270. 105pp.
Utah Division of Water Quality; 1994: Administrative Rules for Ground Water
Quality Protection. R317-6 Utah Administrative Code.
ERM-ROCKY MOUNTAIN, INC. 16 P;\U69005.Her\Rcpan4.dac
TABLES
Table 3-1
Surface Soil Sample Results
Sample ID
Metals
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Silver
Thallium
Zinc
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Soil-1
10,000
ND
9.4
100
1,12
0.39 J
43.8
23.6
11,200
14
301
ND
11.5
ND
ND
ND
56
Soil-2
6,170
ND
9.7
84
0.76
0.57 J
14.6
34.6
7,840
22
342
ND
8.5
ND
ND
ND
60
Soil-3
6,630
ND
7.5
77
0.84
0.32 J
17.4
22.4
8,730
13
239
ND
10.2
ND
ND
ND
38
Standard*
29,000-116,000
0.22-1.01
2.8-10.9
337-998
0.30-1.56
0.01-2.0
19-90
10-43
10,800-41,000
9-31
192-752
0.02-0.11
7-32
0.09-0.56
0.01 -8
0.1-0.8
31-98
Mean
7,600
ND
9
87
0.91
0.43
25
27
9,257
16
294
ND
10
ND
ND
ND
51
Std. Dev.
2,091
ND
1
12
0.19
0.13
16
7
1,741
5
52
ND
2
ND
ND
ND
12
Limit"
12,859
ND
12
117
1.38
0.75
66
44
13,634
29
424
ND
14
ND
ND
ND
81
* standard = Normal Ranges of Elemental Concentrations in Soils of the Western United States (Shacklette, 1984)
** The "Limit" is the statistical Upper Background Limit based on a normal distribution of data using
a one-tailed t-test (t=1.886) where alpha = 0.1 (i.e., 90% confidence) and v (degrees of freedom) = 2.
ND = None Detected
J = Estimated Value
Table 3-2
Surface Water Sample Results
Sample ID
Total Metals
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Copper
Iron
Lead
Manganese
Mercury
Nickel
Sel^ium
Silver
Thallium
Zinc
VOCs
Acetone
Bromodichloromethane
2-Butanone
Chloroform
SVOCs
4-methylphenol
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
CW-1
JUD
18,600
ND
19
300
ND
ND
57
805
16,900
44 J
226
0.0105
36.3 J
6.0 J
ND
ND
767
ND
ND
ND
2J
ND
CW-2
JUD
141J
ND
3.4 J
93.0 J
ND
ND
ND
9.8 J
170
ND
34
ND
ND
ND
ND
ND
38
ND
ND
ND
6
ND
CW-3
JUD
370
ND
5.6 J
67.6 J
ND
ND
ND
39
480
ND
18
ND
7,7 J
ND
ND
ND
99
ND
ND
ND
2J
ND
CW-4
JUD
1,410
ND
8.5 J
91.7J
ND
ND
• 6.1J
78
1,370
ND
36
ND
ND
ND
646
ND
138
17J
ND
ND
3J
ND
Outfall
JUD
ND
ND
4.9 J
62.2 J
ND
ND
ND
6.7 J
69.8 J
ND
4.4 J
ND
ND
ND
ND
ND
22 J
ND
ND
ND
U
ND
CW-1
DISC
94 J
ND
7.6 J
66.0 J
ND
ND
ND
14.5 J
140
ND
4.9 J
ND
ND
ND
ND
ND
73
ND
3J
ND
11
ND
CW-2
DISC
65 J
ND
5.0 J
86.0 J
ND
ND
ND
10.5 J
69.7 J
ND
3.8 J
ND
ND
ND
ND
ND
49
ND
2J
ND
7
ND
CW-3
DISC
ND
ND
3.2 J
50.8 J
ND
ND
ND
11.3J
69.7 J
ND
6.0 J
ND
ND
ND
ND
ND
36
ND
ND
ND
2J
ND
CW-5
DISC
6,840
ND
12
200
ND
3.8 J
24.1 J
477
9,510
84 J
511
0.85
23.4 J
ND
ND
ND
4,610
23
ND
6J
ND .
2J
ND = None Detected; J = Estimated Value
JUD = Judgemental Sample Location; DISC = Discharge Sample Location
Table 3-3
Judgemental Sediment Sample Results
Sample ID
Depth (inches)
Petals
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
[Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Silver
Thallium
Zinc
VOCs
Acetone
Benzene
2-Butanone
Methylene Chloride
Toluene
Semivolatiles
bis (2-ethylhexyl) phthalate
di-n-butyl phthalate
di-n-octyl phthalate
Pesticides/PCBs
Gamma Chlordane
PCB-1260
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
CW-1
0-3
6,280
ND
4.8
118
0.85
0.54 J
1 14.7
31.5
6,850
8.2 J
55.6
0.18
10.4
0.56 J
ND
ND
49
40
2J
ND
4J
ND
ND
ND
ND
ND
40 J
CW-2
0-3
5,060
ND
5.5
56
0.82
0.36 J
12.1
32.5
7,080
14
41.2
0,111J
8.7
0,26 J
ND
ND
64
36
ND
ND
ND
ND
430 J
ND
ND
ND
ND
CW-2
15-18
6,360
ND
7.8
91
1.00
0.39 J
24.1
12.3
8,600
7.7
64.2
ND
8.4
ND
ND
ND
41
25
1 J
ND
ND
ND
ND
ND
ND
ND
ND
CW-3
0-3
9,060
ND
10.5
97
1.0
0.57 J
27.0
148
11,300
19.3 J
94.7
1.15
16.1
2.7
ND
ND
389
120
2J
15J
ND
200
1,000
ND
ND
ND
ND
CW-4
0-3
6,080
ND
4.4
65
0.86
0.36 J
17.7
23.3
8,240
8.5 J
40.4
0.070 J
9.6
ND
ND
ND
46
15J
1 J
ND
ND
ND
150 J
46 J
ND
2J
40 J
CW-4
9-12
7,330
ND
5.2
60
0.87
0.20 J
22.2
13.6
9,310
7.2 J
42.2
ND
10.6
ND
ND
ND
40
22 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
CW-4
DISC
7,220
3.2 J
21.7
106
0.85
ND
34.3
350
39,400
476
363
0.39
10.0
0.94
ND
ND
4,380
ND
ND
ND
3J
ND
2,700
81J
560
-
-
Back-
ground*
12,859
ND
12
117
1.38
0.75
66
44
13,634
29
424
ND
14
ND
ND
ND
81
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Blank (-) = Not Analyzed; NA = Not Available or Not Applicable; ND = None Detected; J = Estimated Value
* "Background" is the Upper Background Limit concentration calculated on Table 3-1
Table 3-4
Statistical Sediment Sample Results
Sample ID
Depth (inches)
Metals
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Silver
Thallium
Zinc
VOCs
Acetone
Benzene
2-Butanone
Methylene Chloride
Toluene
Semivolatiles
bis (2-ethylhexyl) phthalate
di-n-butyl phthalate
Pesticides/PCBs
Gamma Chlordane
PCB-1260
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
STAT-1
0-3
9,920
ND
20.4
84
0.98
0.35 J
21.5
27.8
13,300
19
118
0.050 J
11.9
ND
ND
ND
59
9J
ND
ND
ND
ND
ND
ND
-
-
STAT-i
6-9
6,490
ND
8.6
45
0.67
0.19 J
16
8.8
8,720
6.7 J
61.7
ND
9.4
ND
1.82 J
ND
37
13J
ND
ND
ND
ND
ND
41J
-
-
STAT-2
0-3
11,000
ND
10.1
89
1.12
0.46 J
21.5
21.7
13,200
12.1J
76.2
0.064 J
12.7
0.55 J
ND
ND
72
26 J
1J
ND
3J
ND
130 J
ND
-
-
STAT-3
0-3
8,950
ND
4.7
74
0.96
0.73 J
18.0
64.8
10,600
32
62.3
0.117J
10.9
1.61
ND
ND
88
84
2J
ND
ND
ND
100 J
ND
-
-
STAT-3
14-18
8,110
ND
5.2
57
0.88
0,35 J
18.6
19.8
9,720
13
52.3
0.041 J
9.8
0.54 J
ND
ND
50
17J
IJ
ND
ND
ND
130 J
ND
-
-
STAT-4
0-3
10,700
ND
5.5
84
1.14
0.53 J
20.5
42.2
13,400
17
71.0
0.106 J
12.9
0.65 J
ND
ND
70
67
2J
IOJ
5J
ND
ND
ND
-
-
STAT-4
6-10
10,400
ND
5.4
94
1.17
0.34 J
20.8
15.7
13,100
9,6 J
82.7
ND
11.9
ND
ND
ND
54
ND
2J
ND
ND
ND
200 J
47 J
-
-
Back-
ground*
12,859
ND
12
117
1.38
0.75
66
44
13,634
29
424
ND
14
ND
ND
ND
81
NA
NA
NA
NA
NA
NA
NA
NA
NA
Blank (-) = Not Analyzed; NA = Not Available or Not Applicable; ND = None Detected; J = Estimated Value
* "Background" is the Upper Background Limit concentration calculated on Table 3-1
Table 3-5
Soil-Gas Sample Results
Sample ID
SG-1:10
SG-1:15
SG-1:20
SG-1:30
SG-3:10
SG-3:15
SG-3:20
SG-3:25
SG-4:10
SG-4:15
SG-4:20
SG-4:30
SG-6:10
SG-6:15
SG-6:20
SG-7:10
SG-7:15
SG-7:20
SG-7:30
SG-10:9
SG-12:10
SG-12:15
SG-12:20
SG-12:30
Units
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
LOQ
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
1,1 -Dichloroethene 1,1,1 -Trichloroethane
27 61
ND ND
ND 5
63 270 J
7 11
ND ND
16 23
78 140
ND ND
ND ND
ND ND
ND ND
ND ND
ND 1 J
ND 2 J
ND ND
ND ND
ND 3 J
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
"J" = Estimated Value
"LOQ" = Limit of Quantitation
"ppm" = Parts Per Million
Table 3-6
Ground Water Sample Results
Sample ID
Date Collected
Dissolved Metals
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Silver
Thallium
Zinc
VOCs
Acetone
Benzene
Bromodichloromethane
2-Butanone
Chloroform
1,1-Dichloroethene
1,1,1-Trichloroethane
Trichloroethene
Tetrachloroethene
Semivolatiles
bis (2-ethylhexyl) phthalat
di-n-butyl phthalate
di-n-octyl phthalate
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
BP-1:38
7/30/96
307,000
ND
310
3,670
26
ND
523
526
632,000
260
19,000
1.19J
470
42
ND
ND
1,530
ND
ND
ND
ND
ND
ND
ND
ND
4J
ND
ND
ND
BP-1:113
7/31/96
43,400
ND
39
1,030
1.7 J
ND
113
87
55,800
31
1,380
ND
106
11
ND
ND
1,520
30
ND
ND
ND
ND
ND
ND
ND
ND
5J
ND
ND
BP-2
8/9/96
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
7J
ND
IJ
ND
6J
5J
8
ND
ND
-
-
-
BP-3
9/5/96
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
17J
ND
ND
4J
ND
ND
ND
ND
ND
-
-
-
Standard*
NA
NA
50
2,000
NA
5
100
1,300
NA
15
NA
2
NA
50
100
NA
5,000
NA
5
NA
NA
NA
7
200
5
NA
NA
NA
Blank (-) = Not Analyzed; NA = Not Available or Not Applicable; ND = None Detected; J = Estimated Value
* "Standard" is the Utah Ground Water Quality Standard - R317-6
FIGURES
F
N
S
LEGEND
© GROUND WATD? MONITORING WELL
0 WAIER TANK
—.c—-A— FENCE
APPROXIMATE SCALE-
I \ \ L_J
0 200" 400'
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SG-5
GROUND WATER MONITORING WIL
SOIL GAS SAMPLE LOCATION - SAMPLES COaECTED AT
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WATER TANK
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APPENDIXA
MHERCULES
Hercules Incorporated
Composite Products Division
P. O. Box 18748
Salt Lake City, Utah 84118-0748
[phone]
Mr. Dennis Downs
Director
Division of Solid and Hazardous "Waste
288 North 1460 West
Salt Lake City, Utah 84114-4810
Re: Bacchus Lake Investigation Workplan
Dear Mr. Downs:
August 2, 1995
HAND DELIVERED
DIVISION OF SOLID &
HAZARDOUS WASTE
. AUGo2 1996 ^^
AM '^"
7\8i9ill)iUil2ili2i3i4i5i6
Attached is a sampling/analytical investigation workplan for Bacchus Lake located
at the Hercules Incorporated Composite Products Facility. The workplan was requested
by Mr. Bill Wallner, of your staff, prior to us conducting the environmental investigation.
If you or your staff have comments, language changes or require any additional
infonnation please contact Mr. Shannon Stomid, of my staff, at 251-5006.
Sincerely,
1^ '-(-^
E. R. Anderson, Manager
Environmental, Safety and Hygiene
ERA\SJS
cc: File
BW-1000/0«8(REV 4/»1)
BHERCULES
BACCHUS LAKE
ENVIRONMENTAL INVESTIGATION
WORKPLAN
HERCULES INCORPORATED
COMPOSITE PRODUCTS DIVISION
SALT LAKE CITY, UTAH
AUGUST 1995
1.0 INTRODUCTION
Bacchus Lake was constructed in the mid 1970's, roughly elliptical in shape and has dimensions
of approximately 500 feet long with an average of 220 feet wide (about 110,000 sq. ft. or roughly
2.5 acres). The lake was constructed by placing an earthen berm around a natural depression in
a dry field north and adjacent to the present graphite manufacturing complex. The lake was
constructed for the sole purpose of controlling discharge waters resulting from the graphite fiber
manufacUiring process. Essentially a man-made pond unofficially named Bacchus Lake by
operations personnel.
By design, the only water supply to the lake is from non-contact cooling and rinse waters
resulting from the graphite fiber manufacturing process. The lake level fluctuates per
manufacturing demand intervals since the level is solely dependent on process discharge waters.
There are no, and never has been any, natural sources of water supplying the lake. Hercules has
a permit, issued by the State of Utah, Division of Water Quality (DWQ), to discharge the process
waters and to monitor the inflows and outflow of the lake for pH, temperature and ammonia on
a weekly basis. The results of the weekly monitoring are compiled and reported to the State of
Utah (DWQ) on a quarterly basis.
The lake has a discharge culvert at the northem end (when lake levels rise to that point). Any
discharge water passes through the culvert and generally flows in a north east direction. While
flowing northward, the water continually percolates into the sandy soil and eventually disappears
at approximately a half of a mile down flow. The water never leaves private property and does
not flow into any other bodies of water.
Over the last several years it has been Hercules intention to reduce or eliminate the flow of water
to Bacchus Lake, in fact, the Hercules Composite Products Division waste minimization/pollution
prevention program is actively working on eliminating discharges of water and ammonia to the
lake with the ultimate intention to either eliminate any water discharge to the lake or pipe the
discharge to the West Ridge Golf Course in West Valley City. Hercules has already approached
the golf course and the State Division of Water Quality. These actions will ultimately elhninate
the need for the Bacchus lake impoundment.
In the past, there have been small spills of chlorinated solvents (Dichloromethane and 1,1,1
Trichloroethane) and Mercury (from Mercury electrical switches which have since been replaced
with non-Mercury containing switches) which occurred within the operating buildings. Small
amoimts of residual contamination resulting from these spills may have been flushed to Bacchus
Lake during initial cleanup or by normal housekeeping operations .
Additionally, because of the volatile nature of the process solvents they are inevitably present in
small concentrations in the building's atmosphere. Because non-contact cooling waters and fiber
rinse waters are not enclosed (i.e. within pipes) and flow through open channels within the
buildings they are therefore exposed to the building atmosphere and subsequently may absorb
trace concentrations of process solvents (parts per billion).
To summarize:
Bacchus Lake is a small (P.S acres) man made earthen berm pond.
The water flow into Bacchus Lake is solely frorn a manufacturing process. There
are no natural water flows into the lake.
• The area where the lake is presently located was never a lake, wetland, creek,
tributary, ditch or stream.
When it occurs, water overflow discharges from Bacchus Lake do not flow into
any other body of water and do not leave the private property.
It is Hercules' full intention to eliminate or divert water discharges into Bacchus
lake as part of it's waste minimization/pollution prevention program.
• Residues of chlorinated solvents (1,1,1-Trichloroethane and Methylene Chloride)
and Mercury resulting from spills within the operating buildings could have been
flushed to Bacchus Lake in the past.
As illustrated on Plate I, Bacchus Lake is located along the northem boundary of Hercules'
property. The catalyst initiating the environmental investigation ofthe lake is chlorinated solvent
(specifically 1,1,1 -trichloroetheme) contamination evident tn groundwater taken from a monitoring
well (Aliiant Techsystems well # GW-58) downgradient and due north of Bacchus lake
(approximately 350 feet. See Plates I and II). Consequently, the first and most important step
toward mitigating groimdwater contamination is the attempt to identify and characterize the
contaminating source.
1.0 SITE WORK PLAN
Prior to conducting the sampling the site will be prepared as follows:
SITE PREPARATION
The lake will be sectioned in grids as illustrated on Figure I. Each grid will be on
seventy five (75) foot centers. Steel stakes (wooden stakes, 2 ft to 3 ft sections of rebar,
etc.) will be driven into the ground on the North, South, East and West banks ofthe lake.
The stakes will be driven on centerline of each ofthe 75 foot grids. As shown on Plate
II each intersection ofthe North/South and EastAVest lines will be numbered. Once each
intersection(s) has/Tiave been selected for sampling (selection and number defined below),
barrier tape, rope', cord or line etc. will be tied from North to South stakes and East to
West stakes to mark intersection location. Numbers from 1 to 9 will be written on
individual pieces of paper and placed in a container. One number will be randomly
drawn from the container which will specify the distance (in feet) the first North/South
and EastAVest grid line will start from the very northem and eastem boundary of Bacchus
Lake.
DETERMINATION OF NUMBER OF SAMPLES. LOCATION OF SAMPLES AND
LABORATORY ANALYTES
A combination of statistical and judgmental samples will be taken during the investigation.
Judgmental samples will be taken at all inflows into the lake since heavy.contaminants
may settle out of the flow once the inflow current slows down after contacting the main
body of the lake. Statistical sampling will be taken at grid intersection locations selected
at random. Statistical sampling should account for variability in contaminant distribution
induced by such aspects as inflow water volume and speed, wind and wave action and
fluctuating lake levels.
Judgmental sampling will be conducted at each of the three (3) inflows into the lake. One
inflow originates from fiberlines 1, 2 and 3 (named CW-1), the second inflow originates
from the pilot line (named CW-2) with the third inflow originating from fiberlines 4, 5,
6 and 7 (named CW-3). A single sample will be taken at each ofthe three inflows at a
location within ten (10) of where the inflow enters the lake. The ten (10) feet should
allow for heavy contaminants to fall out and settle on the bottom as the inflow current
slows upon entering the lake. Each inflow sartiple will be located in the centerline ofthe
flow pattem. Figure II displays the approximate locations of inflow sample locations.
FIGURE I N
FIGURE II
N
As explained in Phase I above, each ofthe intersections ofthe North/South and EastAVest
grid lines will be sequentially numbered from one (1) to the highest number of
intersections. Four (4) samples will be taken at randomly designated intersections ofthe
grid lines across Bacchus Lake. Four samples is the number of samples that is required
to achieve an analytical precision of ten percent (10%), a power of 90%, a confidence
level of 95%) and a standard deviation of 5% as defmed by Table 5-2 (Attachment A) of
EPA document #600/400-84-043, Soil Sampling Quality Assurance User's Guide.
A Hewlett-Packard HP-15C will be used to generate the random numbers which will
designate the selected grid intersection between zero (0) and one (1). To initiate the first
random number each number ranging from 0 through 9 will be written on individual
pieces of paper and placed in a container, from which four numbers will be drawn and
written down in sequence. These four numbers will serve as the "seed" for the random
number generator function, subsequent random numbers become the seed for the next
random number. Once each random number is generated it will be multiplied by the
highest number of intersections with the resultant of the multiplication being the
intersection to be sampled.
As illustrated on Figure I, there are fifteen (15) numbered grid intersections overlying the
physical outline of Bacchus Lake ( the exact number of intersections may be different
based on where the grid lines are started). As an example, assume 3,9,8 and 2 are
numbers drawn sequentially from a container and written dov,Ti as they are drawn, the
number 3982 is generated and therefore acts as the seed for the random number generator
with a resultant generated number of 0.4320. 0.4320 is multiplied by 15 (the number of
grid intersections) which results in the number 6.48 or 6. Grid intersection numbered six
(6) is now listed as one of the four intersections to sample. The process is repeated until
four (4) grid intersections are selected.
A small boat will be used to situate the sampling personnel at each of the selected grid
intersections on the surface of the lake. To prevent the boat from drifting it will be
anchored in place. Once the boat is in position the sampling crew will use a 12 foot
liquid/sludge coliwasa sampler to obtain lake bottom sludge and sludge surface water
samples. The sample will consist of approximately the bottom 1 inch of water at the
sediment/water interface and 2 inches of lake sediments below the interface. This
sampling zone should capture any heavy chlorinated solvents and heavy metals that would
be present at the sediment/water interface and below. The coliwasa will be
decontaminated between samples.
TABLE I
Analytical Method T«ble for Hazaj-Kioos C0ns«tue3>t5 iixW3t«ic!s/Sediitt^ts
Process Materials Used ^
Dichloromethane
1,1,1-trichloroethane
Sizing Emulsions
Sodium Hydroxide
Mercury Switches
1,1,1-Trichloroethane -
Dichloromethane Mixture
Hazard Constituents
Volatile Organics
Volatile Organics
Volatile Organics
pH
Heavy Metals-Mercury
Volatile Organics
Analytical Method
SW846-8240/8260
SW846-8240/8260
SW84 6-8240/8260
Field Test
SW846-8240/8260
SW846-8240/8260
As indicated by the Table, the water/sediments will be analyzed using analytical method SW846-
8240/8260 for volatile organics and SW846-6010 for metals. pH is also measured weekly as
part of the Bacchus Lake water quality monitoring program.
10
Four QA/QC samples will be taken during the sampling activities. The following is a
discussion on the number and type of QA/QC samples.
• A field blank fdled with distilled de-ionized water will be exposed during
sampling then analyzed to detect accidental or incidental contamination.
A trip blank will be filled with distilled de-iondzed water and carried with
the decontamination/sampling crew to HS-3. The trip blank bottles shall
be handled identically to the handling methods used for sample collection
and subjected to the same analyses as the wash/rinse waters.
The trip blank will serve to indicate (1) if a handling procedure alters the
analytical results (2) if interaction between the samples or samples and
container is occurring, and (3) if the sample botfles were properly
prepared and cleaned prior to use.
One (1) blind duplicate sample wUl be collected during the sampling
activity. Prior to the sampling activities, each sampling locafion (i.e.
judgmental and randomly drawn) will be numbered, the number will be
written on individual pieces of paper and placed in a container, one
number will then be drawn from the container. The number chosen will
then have a blind duplicate sample taken at that location.
One rinsate sample will be taken between one of the repetitive
decontamination procedures conducted on the sludge coliwasa. The
rinsate sample wUl indicate whether or not the decontamination procedure
is effective.
Table II displays the number of judgmental, grid-random and QA/QC samples.
The samples will be properly labeled, sealed and sent to a State of Utah certified
analytical laboratory for testing and all samples will be handled under chain-of-custody
protocols. Table III outlines sample packaging, handling and preservation.
ll
TABLE II
i:.:S|i|LiS||i
.iiiiiiiliiiiiiiiiil
iiiiiiiiiiiiiiii^
Judgmental
Grid - Random
mmmmmmm
iiiiiiiiiiiiiii
3
4
••••
mmmimmm:;^mmmm.
1 per sampling
activity
iiiilliiiiiiiiS
1 per sampling
activity
^^M
1 per sampling
activity
HB^BI
1 per sampling
activity
12
TABLE III
liiiiiiliiiiiiiiiilliiiii
M^mmMMrmmmmm
Water, Sediments and
Sludges
Water, Sediments and
Sludges
Water/Sediments
Samples
liiilBiliiiMiiiMiiiHjM
liiifliiistituciiiiii
Volatile Organics
Metais
pH
mffmimix:mmsmifmmMm-smmt
Glass jar with teflon lined
lid or 3 ea.40 mi vials
with teflon septum caps
Glass
Poly
liiiiiiiiiiiiiiil
Keep at 4°C
Keep at 4''C
N/A
Hlliiii
lOOg
lOg
N/A
:;;::;:;>;;::;:::;;;':::;o::-:::;::^^
Iiiiiiiiiiiiiiii^ iipiillipiilpilil
iiiiii^'iiRii^^iiii
14 Days
6 Months
During Sampling
13
APPENDIXB
ERM-Rockr Mounuin. Ine.
102 W«al 500 South
SuiLe 650
lliKM '°°'> 58b-8400
Project Numtier: U69005.2
Projecl: HERCULES
Locolion: MAGNA, UT
Owner: HEXCEL
Drilling Compony: EARTH PROBE
Drilling Melhod: DIRECT PUSH
Driller: M. TAGGERT
Log By: D. JOHNSTON
Dole Drilled: S/5/96
1
0
2
4
6
8
10
CP
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Jc:
D
GP
FNn
c o
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s
1
BOREHOLE
1
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41
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d
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SG-2:8
E
5.1
1
u
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LOG Borehole Number:
SG-2
Page 1 of 1
Totol Depth: 8.5'
Top of Casing Elv.:
Surfoce Elevotion:
Northing:
Eostinq
Borehole Diometer: 1.5"
Well Construction
Conductor Cosing:
type: dio: fm: to:
Blonk Casing;
lype; dio: fm: lo:
Screens:
type: size: dio; fm: to:
Annular Fill:
lype: fm: to:
type: fm: to:
Description/Soil Clossificotion
(Description Interval)
0-8.5' SAND/GRAVEL/COBBLES
(SG-2:8 NOT ANALYZED)
REFUSAL AT 8.5'
SECOND AIIEMPT - REFUSAL 2.5'
THIRD ATTEMPT - REFUSAL 7.5'
fefW Igi fflft
fffi • K
ERM-Rock; UounUlo. Inc.
102 Weal 500 South Suite 650
hjKIVl (»"" !'»5-840b
BOR;iHOLE
Project Number: U69005.2
Project: HERCULES
Location: I^AGNA, UT
Owner: HEXCEL
Drilling Compony: EARTH PROBE
Drilling Method: DIRECT PUSH
Driller: W. TAGGERT
Log By: 0. JOHNSTON
Dole Drilled: 8/5/96
0 _.
4
8
12
16
20
24
28
5
1
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GM
END
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SG-3:10
SG-3:15
SG-3:20
SG-3: 25
E a.
8.1
3.4
11.0
34.1
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3
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CD
C3 O
1
LOG Borehole Number;
SG-J
Poge 1 of 1
Totol Depth: 26.1'
Top of Casing Elv.:
Surface Elevalion:
Northing:
Eosling
Borehole Diameter: 1.5"
Well Construction
Conductor Cosing:
type: dio: fm: to:
Blonk Casing:
lype: dio: fm: lo;
Screens:
type: size; dio: fm: lo:
Annulor Fill:
type: fm: to:
type: fm: to:
Description/Soil Clossificotion
(Description Intervoi)
0-0.25' ASPHALT
0.25-6' SAND/GRAVEL/COBBLES
6-26' SAND/SILT/GRAVEL
REFUSAL AT 26.1'
1;
nrgwl m ul
CRU'Rocky Uouotala, Joe
102 Weal 500 South Suite 6S0
lllAlVl ^^°^'^ 595-8400
BOREHOLE
Project Number: U69005.2
Project: HERCULES
Locotion: MAGNA, UT
Owner; HEXCEL
Drilling Compony; FOUNDEX PACIFIC, INC.
Drilling Method: BECKER HAMMER
Driller: T. KUNIK
Log By: D. JOHNSTON
Dote Drilled: 8/24/96
! a.
0
4
8
12
16
20
L2i_
28
32
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GP
END
C
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5
SG-4:10
SG-4:15
SG-4: 20
SG-4:30
E
12.8
14.6
9.2
2.7
C
cS
ct
1
Ll
a:
LOG Borehole Number:
SG-4
Poge 1 of 1
Total Depth: 50'
Top of Casing Elv.:
Surface Elevotion:
Northing:
Eosling
Borehole Diometer: 5.5"
Well Construction
Conductor Casing:
lype: dio: fm: to:
Blank Cosing; 1
type; dio: fm: to;
Screens:
type: size: dio: fm; to:
Annulor Rll:
lype: fm: to;
lype: fm: to:
Description/Soil Clossificotion
(Description Intervoi)
0-30' SAND/GRAVEL/COBBLES
SAMPLE IDENTIFIED AS SG-4:25 WAS A BLIND
DUPLICATE FOR SG-4:20
T~ 1 ERU-Rocky UOUDUIQ, IDC
102 West 500 Soulh
1 Suile 6M
El KM '»"!) 505-a<00 BOREHOLE
Project Number: U69005.2
Project: HERCULES
Locotion; MAGNA, UT
Owner: HEXCEL
Drilling Compony: EARTH PROBE
Drilling Method: DIRECT PUSH
Driller: M. TAGGERT
Log 8y: 0. JOHNSTON
Dote Drilled: 8/5/96
0
2
4
6
8
o
CL
a
o
GP
END
c:
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6
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01
ca.
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SG-5: 7
Q.
8.0
c 3 O CJ
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CD
1
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LOG Borehole Number:
SG-5
Page 1 of 1
Totol Deplh: 7'
Top of Cosing Elv.:
Surfoce Elevotion;
Northing:
Eostinq
Borehole Diometer; 1.5'
Well Construction
Conductor Cosing:
type; dio: fm: lo:
Blonk Cosing:
type; dio; fm: lo:
Screens:
type; size; dio: fm: to:
Annular Fill;
lype; fm: to:
type: fm: to;
Oescriplion/Soil Clossificotion
(Description Intervoi)
0-7' SAND/GRAVEL/COBBLES
REFUSAL AT 7'
(SG-5: 7 NOT ANALYZED)
SECOND ATTEMPT - REFUSAL 3.5'
THIRD ATTEMPT - REFUSAL 1.5'
ERM-Rocky UounUlo. IDC.
Suite 650
EJX\]V1 *^°'* 595-^:400
Project Number: U69005.2
Projecl: HERCULES
Location: MAGNA, UT
Owner: HEXCEL
Drilling Compony: EARTH PROBE
Drilling Melhod; DIRECT PUSH
Driller: M. TAGGERT
Log By: 0. JOHNSTON
Dote Drilled: 8/6/96
0
2
4
5
8
10
3
O
t5
GP
END
C
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1
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ROREHOl E
1
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01
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XI
5
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Q.
C 3 O CJ
s o
OD
i
LO a Borehole Number:
SG-9
Poge 1 of 1
Totol Depth: 9'
Top of Casing Elv.:
Surfoce Elevation:
Northing:
Eostinq
Borehole Diameter: 1.5"
Well Construction |
Conductor Cosing:
lype: dio: fm:
Blank Casing:
type; dio: fm:
Screens:
lype: size: dio: fm:
Annulor Fill:
lype: fm:
lype: fm;
to:
to;
to:
to:
to:
Description/Soil Clossificotion
(Description Interval)
0-9' SAND/GRAVEL/COBBLES
NO SOIL-GAS SAMPLES COLLECTED
REFUSAL AT 9'
'"\
ERH-Rockr Mouniain. Inc.
JOa Heal 500 .South
Suite 550
EJXVJVI t^^*' 595-8400
Projecl Number: U69005.2
Projecl: HERCULES
Locotion: MAGNA, UT
Owner: HEXCEL
Drilling Compony; FOUNDEX PACIFIC, INC
Drilling Method; BECKER HAMMER
, Driller; T. KUNIK
Log By: D. JOHNSTON
Dote Drilled: 8/24/96
t
0
1 2
4
6
8
10
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Ic a. o
O
GP
END
c .9
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1
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1
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IJ VJ iVJL^ll VJ JLJJLIJ
3i a. E O to
d
z
01
a.
E
-O O
SG-10:9
E
15.6
g
CD
o
1 tl
LOG Borehole Number:
SG-10
Page 1 of 1
Total Depth: 9'
Top of Casing Elv.:
Surfoce Elevotion;
Northing;
Eostinq
Borehole Diometer: 5.5"
Well Construction
Conductor Cosing;
lype: dio: fm: lo;
Blonk Cosing:
type: dio: fm: to:
Screens:
type: size: dio; fm: to;
Annulor Rll;
type: fm: to:
type: fm: to:
Description/Soil Clossificotion
(Description Interval)
0-9' SAND/GRAVEL/COBBLES
VERY DENSE
REFUSAL AT 9' - POSSIBLE
ABANDONED STRUCTURE FOUNDATION
M 1 ERM-RoekT Uouolaln, Inc.
lOZ Weat 500 South
3 Suite 650
EJKM I™'' 505-8400
ROR^^f'Ol E LOG
Project Number; U69005.2
Project; HERCULES
Locotion; MAGNA, UT
Owner: HEXCEL
Drilling Company: EARTH PROBE
Drilling Method; DIRECT PUSH
Driller; U. TAGGERT
Log By: D. JOHNSTON
Dole Drilled: 8/6/96
1 a. Qt O
0
2
4
6
8
10
12
14
16
18
20
.3
GM
GP
FND
c
"CJ
3
17) c o CJ
"5
3
1
dj
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JC
01
a. E
X
X
d
z
01
Q.
cn
.o o
SG-n:10
SG-11:15
E
O.
8.1
7.2
o
S
C3
1 l_l 01 a:
Borehole Number:
SG-11
Poge 1 of 1
Totol Depth: 19.5'
Top of Cosing Elv.:
Surfoce Elevotion;
Northing:
Easting
Borehole Diometer: 1.5"
Well Construction
Conductor Cosing:
lype; dio: fm; to:
Blonk Cosing;
type: dio: fm; lo:
Screens;
type: size; dio: fm: to:
Annular Rll;
type: fm: to:
type: fm: to:
Description/Soil Clossificotion
(Description Interval)
0-13' SAND/GRAVEL/COBBLES
(SG-11:10 NOT ANALYZED)
13-19.5' SAND/GRAVEL/COBBLES
(SG-11:15 NOT ANALYZED)
REFUSAL AT 19.5'
1 l-'-fN
E
Pr
Pr
Lo
Ov
Dr
Ur
Dr
D
(
1
r
I
i
m ERM-RockT H
'^ ' '^ lOa Vl«at 500 So
h i aE Suite 650
ounUin. Inc.
uth
T-i^X Salt Lake Cilr. Utah 04101-2334
ID n O 17 un T L'
IJ VJiVJL'^liVJ JUJl^
oject Number; U69005.2
ojecl: HERCULES
cotion; MAGNA, UT
»ner: HEXCEL
illing Compony; FOUNDEX PACIFIC, INC.
illing Method; BECKER HAMMER
iller: T. KUNIK
)g By: D. JOHNSTON
]te Drilled: 8/24/96
? °
Sr o
13 O
3
4
3
2
6
10
IA
28
GP
52 END
C
•2
c
3
1
Ol
3
01 a. E
X
X
X
d
z
01 a. E o to .o o
SG-12:10
SG-12:15
SG-12:20
SG-12:3C
E
6.1
2.2
7.4
7.2
c 3 O <J
§
1
Oi.
LOG
Borehole Number:
SG-12
Poge 1 of 1
Totol Depth: 50'
Top of Cosing Elv.;
Surface Elevotion;
Northing:
Easting
Borehole Diameter: 5.5"
Well Construction
Conductor Casing:
type: dio: fm; to:
Blonk Casing:
lype; dio: fm: to:
Screens:
type: size: dio: fm: to;
Annular Rll:
lype: fm; to:
type: fm; to:
Description/Soil Clossificotion
(Description Interval)
0-30' SAND/GRAVEL/COBBLES
0-20' DENSE
20-30' VERY DENSE
APPENDIX C
ERM-Rockj UounUIn, Inc.
SMO South WItoa Drfta
ayiu too
ERM <i>i«»«i Vlllaal. (M»r»4» Will BOREHOLE LOG Borehole Number;
BP-01
Poge 1 of 7
Project Number; U69005.1
Projecl; Bocchus Pond
Location; Mogno, UT
Owner; Hercules
Drilling Compony; Layne Christensen
Drilling Method: Becker-Hammer
Driller; Blolne
Log By; P. Corbetto
Dole Drilled: 07/30/96 - 07/31/96
Totol Depth: 121.00"
Surface Elevotion:
Northing;
Eosling
Borehole Diometer: 9.50in
Well Construction
Conductor Cosing;
type: dia;0.00in fm: 0.00' to: 0.00'
Blank Casing:
type: PVC dia:2.00in fm;-0.5' lo; 100.60
Screens:
type: Slotted sizei010indio:2.00in fm; 100.60to: 120.60
Annulor Fill:
type; Concrete Grout
type: Bentonite
type; Sond Filter
fm: 0.00" to: 7.00'
fm; 7.00' to; 97.00'
fm: 97.00' to: 121.00
o
Description/Soil Clossiflcolion
(Description Intervoi)
1-
2
3
4-
5-
6-
7
8-
9-
10-
11-
12
13
14-1
15
16-j
17
U ppm
(0 - 5") SAND; little silt and grovel, light yellowish brown,
fine to coarse groin, subangular, dry, no stain, no odor.
(5 - 12') SAND; little silt ond grovel, brown, fine to coarse
groin, subongulor, dry to slightly moist, no stoin, no odor.
(12 - 17') SAND; little silt ond gravel, light yellowish
brown, fine to coorse groin, subongulor, dry, no stain/no
odor, quartzite cobbles up to 6 inches.
Em-Rockir MounUln, Inc.
HH SwU nilM DrM< suite KM
ERM itSTnt BOREHOLE LOG Borehole Number;
BP-01
Poge 2 of 7
Project Number: U69005.1
Project: Bocchus Pond
Locotion: Mogno, UT
Owner; Hercules
Drilling Compony: Layne Christensen
Drilling Method: Becker-Hammer
Driller; Blaine
Log By: P. Corbetto
Dote Drilled; 07/30/96 - 07/31/96
Totol Depth; 121.00"
Surfoce Elevation:
Northing:
Eosling
Borehole Diometer: 9.50In
Well Construction
Conductor Cosing:
type: dio:0.00in fm; 0.00" to: 0.00'
Blank Casing;
type: PVC dio;2.00in fm: -0.6' to; 100.60
Screens
type: Slotted size:010indio:2.00in fm: 100.60to: 120.60
Annulor Rll:
type; Concrete Grout
type: Bentonite
type: Sond Filter
fm: 0.00' to; 7.00'
fm; 7.00' to: 97.00
fm: 97.00' to: 121.00
o
Description/Soil Clossificotion
(Description Interval)
19-
20
21-[>
22-i'
23-^
24-
25-
26
27-1
28
29
30
31
32
33-
34-
35-
•^\Lf\J ••\^ • \.
O °
OO
O °
OO
o o
oo
O o
oo
O o
oo
o °
oo
0 °
oo
O o
o.o
O o
oo
Q o
oo
o °
oo.
0 °
oo
. 0 o
oo
O o
oo
0 °
oo
O o
oo
o
0
od
0
oa
0
od
o
OCl
0
oci
0
OCl
o
O0
0
0.0
o
o.d
o oa
o
Od
o
Od
0
Od
0
Od
0
Od
too o c
Ko ° o 'I
(17 0 20') SAND; little silt, troce grovel, brown, fine to
coarse groin, slightly moist, no stain, no odor.
(20 - 44") SANDY GIRAVEL; little silt, brown, slightly
moist, no stoin, no odor.
ERH-Rocky Mountain, Ino.
MM S«tk WlUota Ortn
suite no BOREHOLE LOG Borehole Number;
BP-01
Poge 3 of 7
Project Number; U69005.1
Projecl: Bacchus Pond
Location; Mogno, UT
Owner; Hercules
Drilling Compony; Layne Christensen
Drilling Method: Becker-Hammer
Driller: Bloine
Loq By: P. Corbetto
Dole Drilled: 07/30/96 - 07/31/96
Total Deplh; 121.00'
Surface Elevation:
Northinq;
Easting
Borehole Diameter: 9.50in
Well Construction
Conductor Casing:
lype; dio;0.00in fm; 0.00* to; 0.00'
Blank Casing;
lype: PVC dio;2.00in fm; -0.6' to; 100.60
Screens:
lype; Slotted size:010indio;2.00in fm; 100.60to: 120.60
Annular Rll:
lype; Concrete Grout
type; Bentonite
type: Sond Filter
fm: 0.00' to; 7.00'
fm; 7.00' to; 97.00'
fm: 97.00' to: 121.00
Description/Soil Clossificotion
(Description Interval)
At 38", water from 38 to 44.4.
(40 - 44") SANDY Gf^VEL, trace cloy, brown, fine
to coarse groin, subangulor, cobblers up to 4 inches,
slightly moist, no stoin, no odor.
(44 - 52') CLAY; trace grovel, greenish gray, trace
yellowish-red mottle, no stain, no odor.
ERM <sr^
ERH-RockJ UouoUin, Ine.
SHO Sralk •llteu Drtn &aia no
Vlllaca. Calorate 10111 BOREHOLE LOG Borehole Number;
BP-01
Poge 4 of 7
Project Number; U69005.1
Project; Bocchus Pond
Locotion; Mogno, UT
Owner: Hercules
Drilling Compony; Loyne Christensen
Drilling Method; Becker-Hommer
Driller: Bloine
Log By: P. Corbetto
Dote Drilled; 07/30/96 - 07/31/96
Totol Depth: 121.00"
Surface Elevotion;
Northing:
Easting
Borehole Diameter: 9.50in
Well Construction
Conductor Casing:
type: dia:0.00in fm; 0.00' to; 0.00"
Blonk Cosing;
type: PVC dio;2.00in fm: -0.6' to; 100.60
Screens;
type: Slotted sizeL010indio:2.00in fm: 100.60to: 120.60
Annulor Rll:
type; Concrete Grout
lype; Bentonite
type: Sand RIter
fm: 0.00' to: 7.00'
fm; 7.00' to: 97.00'
fm: 97.00' to: 121.00
01
Description/Soil Clossification
(Description Intervoi)
(52 - 77') CLAY; some grovel, strong brown, angulor
to subongulor. quartzite up lo 4 inches, wet to very
moist with depth, soft, no stain, no odor.
ERM-Roekr UounUIn. Ino.
SOM Soulk nUn Mn Suite aao
ERM issni^-BOREHOLE LOG Borehole Number;
BP-01
Poge 5 of 7
Project Number: U69005.1
Project; Bacchus Pond
Location; Mogno, UT
Owner: Hercules
Drilling Company: Loyne Christensen
Drilling Melhod: Becker-Hommer
Driller: Bloine
Log By: P. Corbetto
Dote Drilled: 07/30/95 - 07/31/96
Totol Depth; 121.00'
Surface Elevation:
Northing:
Eosling
Borehole Diameter; 9.50in
Well Construction
Conductor Cosing:
type: dio:0.00in fm;0.00' to: 0.00"
Blank Casing:
lype: PVC dia:2.00in fm; -0.6" to; 100.60
Screens;
type: Slotted size--010indio:2.00in fm; 100.60to: 120.60
Annulor Rll;
type: Concrete Grout
type: Bentonite
type; Sond Filter
fm; 0.00' to; 7.00"
fm: 7.00' lo; 97.00
fm; 97.00' to: 121.00
o
O-
:?
Description/Soil Clossificotion
(Description Intervoi)
(77 - 82") CLAY; trace sand ond gravel to gravely,
strong brown, sand is medium grain to coarse groin,
gravel is angulor to subangulor, quartzite, moist to very
moist (lift drill string to check water infiltration,no woter).
At 82"; CLAYEY SAND, strong brown, fine groin,
moist, no staining, no odor.
(82 - 90") SAND; troce cloy, fine to granular, slightly
moist, no stain, no odor.
ERM-RockT Mountain, Inc.
suite SOO Ttn\r cniu.i»< viiiMu. c»n>»<» aoiii
r>RM (*"> '«>-«<>»
BOREHOLE LOG Borehole Number:
BP-01
Page 6 of 7
Project Number: U69005.1
Project; Bacchus Pond
Locolion; Magna, UT
Owner; Hercules
Drilling Company; Loyne Christensen
Drilling Method; Becker-Hommer
Driller: Blaine
Log By: P. Corbetto
Dole Drilled; 07/30/96 - 07/31/96
Totol Deplh; 121.00'
Surfoce Elevotion:
Northing:
Easting
Borehole Diameter: 9.50in
Well Construction
Conductor Casing:
type: dio:0.00in fm: 0.00' to; 0.00'
Blank Cosing;
lype: PVC dia:2.00in fm: -0.6" to: 100.60
Screens:
type: Slotted size:010indio;2.00in fm: 100.60to: 120.60
Annular Fill:
lype; Concrete Grout
type; Bentonite
type: Sond Filter
fm: 0.00' to: 7.00"
Im; 7.00' to: 97.00'
fm; 97.00" to; 121.00
g"
Description/Soil Clossificotion
(Description Intervoi)
(90 - 95") CLAYEY SAND; some grovel lo gravely,
strong brown, medium to fine groin, subangulor
quartzite, andesite, slightly moist, no stoin. no odor.
At 93"; cobbles, subrounded.
(95 - 105') CU\YEY SAND; troce to some gravel,
brown, quartzite and sandstone grovel, moist to
very moist, strong reaction lo nitric acid.
(105 - 113') SAND; some gravel to gravely, trace
cloy, brown, coarse lo granular, subongulor to
subrounded, slightly moist, no stain, no odor.
1 IBMB ERU-Rockj MouoUitt. Ine.
1 IHillllffll f" SNia aiuni Mn 1 UgUUB sirite too
ERM ISOO) wi-ioS'^
EOREHOT.E LOG
Project Number; U69005.1
Projecl; Bacchus Pond
1 Location: Mogno, UT
Owner: Hercules
Drilling Compony: Loyne Christensen
Drilling Method: Becker-Hommer
1 Driller; Bloine
Log By: P. Corbetto
j Dole Drilled: 07/30/96 - 07/31/96
^^
-—^
I Q-
1 "^
• 109-
110-
j 111-
112-
Ill3-
.1 14-
115-
1 1 1 C ^
117-
|l18-
119-
120-
1121-
122-
|l23-
124-
'125-
o»
o
o x= o.
o
O o 0 "0
O O OO O
0 ° 0 o 0
OOOOO
0 o 0 o 0
ooooo
0, o 0 " 0
OOOOO.
0 ° 6 •» 0
OOOOO
0 o O o 0
oo ooo
O o 0 « 0
=
3
To
c o o
=:
S
=
1
—
—
^
—
=
^
irri
r-r=
z^^
•
>
i_
^
1
03
C
01
E
m
o
OJ
•o.
o tn
o
BP-OI:II?
Borehole Number:
BP-01
Page 7 of 7
Totol Depth: 121.00'
Surfoce Elevation:
Northing;
Easting
o a.
^
u c o
O
Borehole Diometer: 9.50in
Well Construction
Conductor Casing:
type; dio;0.00in fm; 0.00' to; 0.00'
Blank Casing:
type: PVC dia;2.00in fm: -0.6' to: 100.60
Screens;
lype; Slotted si2e:010irdio;2.00in fm; IOO.6OI0; 120.60
Annular Rll:
type; Concrete Grout fm: 0.00' to: 7.00"
type: Bentonite fm; 7.00' lo; 97.00'
lype; Sond niter fm; 97.00' lo: 121.00
Descriplion/Soil Classification
(Description Intervoi)
(113 - 116') SAND; coarse to granular, subangular
lo subrounded, water at 115'.
(116 - 121') SANO AND GRAVEL; gronulor. gravel is
angulor to subangulor up lo 5 inches, quortzite,
sandstone, conglomerote, increase in cobbles with
deplh, soturoted, no stoin. no odor.
ERM-Rock7 Mountain, Ine.
saw Smte nilnr Mo
Suite ao ERM <*•) '«!-««• BOREHOLE LOG Borehole Number;
BP-02
Poge 1 of 14
Projecl Number; U69005.1
Project: Bacchus Pond
Locolion: Mogno, UT
Owner Hercules
Drilling Company: Loyne Christensen
Drilling Melhod: Becker-Hommer
Driller: Blaine
Log By: P. Corbeiia
Dole Drilled: 08/01/96
Totol Depth; 235.00'
Surface Elevation:
Northing:
Easting
Borehole Diometer: 9.50in
Well Construction
Conductor Cosing;
type: dio;0.00in fm: 0.00' to: 0.00'
Blonk Cosing:
lype; PVC dio;2.00in fm; 0.0' lo; 214.01
Screens;
lype: Slotted size-.010india:2.00in fm:214.00to;234.0i
Annulor Rll;
type; Concrete Grout
type: Bentonite
type: Sond RIter
fm:0.OO' to: 1.00'
fm:1.00' to: 211.01
fm: 211.00'to: 235.01
rni fil
M
o.
E
a.
E
U ppm
Descriplion/Soil Clossificotion
(Description Inten/ol)
1-
(0 - M') SILTY SAND; some grovel to grovely,
pinkish groy, fine grain lo gronulor, ongular to
subongulor. quartzite, sandstone, gobbro, dry,
no odor, no stain.
(14 - 16') to stiff, moist, no odor, no stoin.
ERM '•'STU!
ERH-Rockr Uounlals. Inc.
UaO South nllou Drtn suite soo viiia(«. rmirm aoiii BOREHOLE LOG Borehole Number:
8P-02
Poqe 2 of 14
Project Number; U69005.1
Project; Bocchus Pond
Locolion; Mogno, UT
Owner: Hercules
Drilling Compony; Loyne Christensen
Drilling Method: Becker-Hommer
Driller: Bloine
Log By; P. Corbetto
Dote Drilled; 08/01/96
Totol Depth: 235.00'
Surfoce Elevotion:
Northing:
Easting
Borehole Diometer; 9.50in
Well Construction
Conductor Casing:
lype: dia:0.00in fm: 0.00' to; 0.00'
Blonk Cosing;
type; PVC dio;2.00in fm:0.0' to: 214.01
Screens:
type: Slotted sizei010indio:2.OOin fm: 214.00lo: 234.01
Annular Rll;
type; Concrete Grout
type: Bentonite
type: Sond RIter
fm;0.0O' to; 1.00'
fm: 1.00' lo: 211.01
fm; 211.00'lo; 235.01
E o t/l
ty< o
Description/Soil Clossification
(Description Intervoi)
(U - 25') CLAY; little sond ond grovel, trace silt, brown,
troce red streaking, grovel is angular to subrounded,
quortzite, sondstone, siltstone, soft
(25 - 33') CWYEY SAND; some gravel, reddish
brown, fine lo gronulor. subrounded, soft, moist to very moist,
wilh increasing depth moisture
decreoses and sond increoses.
0.9 ppm
(33 - 44') GIWVELY SAND; trace cloy, reddish brown.
fine to coarse groin, subrounded to rounded, moist, no odor, no stoir
ERH-Rocky Mountain, Inc.
gtU Soulh Wlllou Drhu Suite no
CmounU VllUfo, ruinio SOI II ERM SSr^-iSS' BOREHOLE LOG Borehole Number;
BP-02
Poge 3 of 14
Project Number; U69005.1
Projecl: Bocchus Pond
Location; Magna, UT
Owner; Hercules
Drilling Compony; Loyne Christensen
Drilling Melhod; Becker-Hommer
Driller: Blaine
Loq By; P. Corbetto
Dote Drilled; 08/01/96
Total Depth: 235.00'
Surfoce Elevotion:
Northing:
Easting
Borehole Diometer: 9.50in
Well Construction
Conductor Casing;
type; dia;O.00in fm: 0.00' to: 0.00'
Blank Casing;
type: PVC dia:2.00in fm; 0.0' to; 214.01
Screens;
lype: Slotted size-.01 Oindio: 2.00in fm;214.00to: 234.0i
Annular Rll:
type; Concrete Grout
type; Bentonite
type: Sond RIter
fm:0.00' to; 1.00'
fm;1.00' to; 211.01
fm; 211.00'lo: 235.01
o
e
o
Description/Soil Clossificotion
(Description Intervoi)
37
38
39
40
41
42
43 H
44
45
46-
47-
48-
49-
50
51
52-
53-
(44 - 50') SAND; little to some grovel, troce cloy, fine
groin to gronulor, subrounded quartzite, gravel up to 6
inches, slightly moist, carbonaceous, no stain, no odor.
ESU-Rock; Mouniain, Inc.
SHO South milou MM suite no r-iT-tif cioouoioj viiio(«, cm aeiii
LKM (SeS) 741-BOBO
BOREHOLE LOG Borehole Number:
BP-02
Poge 4 of 14
Project Number: U69005.1
Project; Bacchus Pond
Location; Magna, UT
Owner; Hercules
Drilling Compony; Loyne Christensen
Drilling Method: Becker-Hommer
Driller; Bloine
Log By: P. Corbetto
Dole Drilled; 08/01/96
Total Depth; 235.00'
Surface Elevotion;
Northing:
Eosling
Borehole Diometer: 9.50in
Well Construction
Conductor Casing;
type; dia;0.00in fm; 0.00' lo; 0.00'
Blank Cosing;
lype: PVC diQ;2.00in fm: 0.0" to:214.0C
Screens;
lype; Slotted size:010india;2.00in fm; 2U.00to: 234.0C
Annulor Rll;
type; Concrete Grout
type; Bentonite
type: Sond Filter
fm:0.00" to; 1.00'
fm;1.00" to: 21 l.OC
fm; 211.00'to; 235.0C
E o in
JO
6
Description/Soil Clossificotion
(Description Intervoi)
55-
56-
57-
58-
59-
60-
61-
62-
63-
64-
65-
66-
67-
68-
69-
70-
/1-
• . . . • ••.•.••.••
;•.;••'.;;•.:::;: :;•:•:
(50 - 66') SAND; some grovel to grovely, troce cloy, dork
reddish brown to reddish brown, subrounded, red and gray
sondstone grovel, corbonaceous, slightly moist, no stoin, no
odor, cobbles up lo 4 inches, difficult drilling from 50'.
(66 - 73') SAND; some grovel, brown, fine to gronulor,
subongulor to subrounded, cobbles up to 6 inches,
quortzite, gobbro, limestone, dry to slightly moist,
no odor, no stain.
ERM-Rockjr Mountain, Ine.
MM South niioi sum 100
ERM (SBTMI'-MM*
BOREHOLE LOG Borehole Number:
BP-02
Poqe 5 of 14
Project Number: U69005.1
Project; Bacchus Pond
Locotion; Mogno, UT
Ovner: Hercules
Drilling Compony: Loyne Christensen
Drilling Method: Becker-Hommer
Driller; Blaine
Log By; P. Corbetto
Dote Drilled: 08/01/96
Totol Depth: 235.00"
Surface Elevation:
Northing;
Easting
Borehole Diameter: 9.50in
Well Construction
Conductor Casing:
type: dio:0.00in fm: 0.00' lo; 0.00"
Blonk Cosing;
type; PVC dio;2.00in fm: 0.0" to;214.0C
Screens;
type; Slotted sizeiQl Oindio;ZOOIn fm:214.00(o;234.0C
Annular Rll;
lype: Concrete Grout
type; Bentonite
type; Sond RIter
fm;0.00' to: 1.00"
fm:1.00' to; 211.00
fm; 211.00'to: 235.00
o
e
Description/Soil Clossification
(Description Intervoi)
(73 - 75') SAND; trace cloy, reddish brown, slightly moist.
(75 - 77') SANOY CLAY; some grovel ond cobbles,
weok red, fine lo coarse groin, soft, slightly moist.
78 H
79
80-
81-
82
83-i
84
85-
86-
87
88-1
89
(77 - 84') SAND; medium groin to gronulor, light reddish
brown, subongulor lo subrounded, pebbles up to 1 inch, dry,
no odor, no stoin.
(84 - 102') SAND; some cloy, brown, fine to
coarse groin, pebbles up to 2 inches, subrounded.
slightly moist, no odor, no stain, interloyered cobbles,
subongulor to subrounded, quartzite, sandstone, limestone.
ERM iSSrH!
ERM-Rocky MounUln, Ine.
gOH South niteu Drtn &iite aoo Vlllo«o. coumo 10] 11 BOREHOLE LOG Borehole Numben
BP-02
Poqe 6 of 14
Project Number: U69005.1
Projecl: Bocchus Pond
Locotion: Mogno. UT
Owner: Hercules
Drilling Compony; Loyne Christensen
Drilling Method; Becker-Hommer
Driller; Blaine
Log By; P. Corbetto
Dole Drilled; 08/01/96
Total Depth: 235.00'
Surfoce Elevotion:
Northing:
Easting
Borehole Diometer: 9.50in
Well Construction
Conductor Cosing;
type; dio;0.00in fm: 0.00' to; 0.00'
Blank Cosing;
lype: PVC dio:2.00in fm;0.0' to: 214.0
Screens:
type; Slotted sizei010irdia:2.00in fm; 214.00to; 234.0
Annulor Rll;
lype; Concrete Grout
type: Bentonite
type: Sand RIter
fm:0.00' to: 1,00'
fm:1.00' to: 211.01
fm: 211.00'to: 235.01
OL
E 6
Description/Soil Clossificotion
(Description Intervoi)
(102 - 103') CLAY; little sand, fine grain to gronulor, red,
slightly moist, no odor, no stoin.
(103 - 105") Boulder, quartzite.
(105 - 110') SAND; troce cloy, strong brown, fine groin to
gronulor, pebbles, subongulor to subrounded, no odor, no slain.
ERH-Rock7 Mounuin, Ine.
H« South «Illo> Onn
Suite aee
T7>Tklf CulinuJ Vllloio. ruiini Mill
hiRM (*"> Mi-io"
BOREHOLE LOG Borehole Number:
BP-02
Poge 7 of 14
Project Number; U69005.1
Project: Bocchus Pond
Locolion; Magna, UT
Owner Hercules
Drilling Company: Loyne Christensen
Drilling Method; Becker-Hommer
Driller; Blaine
Log By: P. Corbetto
Dote Drilled; 08/01/96
Tofol Depth: 235.00'
Surface Elevation;
Northing;
Eosting
Borehole Diometer 9.50in
Well Construction
Conductor Casing;
type; dio:0.00in fm; 0.00' to; 0.00'
Blonk Cosing;
type: PVC dio;2.00in fm; 0.0' to; 214.0
Screens:
type; Slotted size-.010irdio;2.00in fm: 214.00to: 234.0
Annular Rll:
lype; Concrete Grout
type: Bentonite
type: Sond RIter
fm:0.00' to; 1.00'
fm:1.00' to: 21 l.Ol
fm; 211.00'to: 235.0
o
£
o.
E
Description/Soil Clossificotion
(Description Inten/ol)
113-1
114
115
116-
117-
118-
119
120-
121
122
123
124-1
125 V/.U O.U >-<
o °, O " o
oo oo o
(110 - 112') CLAY; some sond, little to some grovel,
reddish brown, medium grain lo gronulor, slightly moist.
(112 - 125') SAND; troce clay, little cobbles, strong brown,
fine groin to granular, cobbles up to 5 inches, no odor, no stain.
At 116', pinkish groy.
From 117 - 125', pebbles ond grovel increase.
Add water to borehole to advance borehole.
Al 125", CLAY, little sond. brown, fine groin to gronulor,
wet from odding woter -obove, no stoin, no odor.
ElUI-Rockr MouaUio. Inc.
HU South •liicra Mn Suite no nniM Cnouuoal niUfo. Colan^o Hill BOREHOLE LOG Borehole Number:
BP-02
Poge 8 of 14
Project Number; U69005.1
Project: Bocchus Pond
Locolion; Mogno, UT
Owner Hercules
Drillinq Company: Loyne Christensen
Drilling Method: Becker-Hommer
Driller Bloine
Log By; P. Corbetto
Dote Drilled: 08/01/96
Tofol Depth: 235.00'
Surface Elevotion:
Northing:
Easting
Borehole Diometer 9.50in
Well Construction
Conductor Cosing;
type; dio: O.OOin fm: 0.00' to; 0.00'
Blank Casing;
type; PVC diQ;2.00in fm; 0.0' to:214.0(
Screens:
type; Slotted sizeiOl Oindio: 2.00in fm; 214.00lo; 234.01
Annular Rll:
type; Concrete Grout
lype; Bentonite
type: Sond RIter
fm:0.00' lo:1.00'
fm:1.00" to:211.0(
fm:2n.00'to;235.0(
a
O
Description/Soil Clossificotion
(Description Inlen^ol)
(125 - 132") SANO ANO GRAVEL; ongulor to subangulor,
quartzite, sondstone, limestone, possible boulder, wet from
adding water, no odor, no stain.
(132 - 135') CLAYEY SAND; some grovel,
reddish brown, fine groin to gronulor, moist,
no odor, no stoin.
(135 - 142') SAND ANO GfWVEL; little to some
cloy, light reddish brown, gravel Is pebble size lo 4 inches,
subongulor to subrounded, slightly moist.
ERH-Rockr MounUln. loe.
HSO South nilov Mn
Suite no
Cmomilf nilofo. Counilo Hill ERM (SSTMI-MM BOREHOLE LOG Borehole Number
BP-02
Poge 9 of 14
Projecl Number U69005.1
Projecl: Bocchus Pond
Locolion: Mogno, UT
Totol Depth: 235.00'
Surface Elevation:
Northing:
Eosting
Borehole Diometer 9.50in
Ouinor* UWIiei. iicii^uicD
1 Drilling Compony: Loyne Christensen
j Drilling Method: Becker-Hommer
Driller Bloine
Log By: P. Corbetto
Dote Drilled; 08/01/96
"S" 1 ^—^ 1 -^ "S.
1 01 o
145-
146-
147-
148-
|l49-
150-
151-
152-
153-
1154-
155-
Il56-
157-
158-
159-
160-
j 161-
o*
—1
tl
•-=
o
o
oo o.b oj
O ° 0 o 0
oooo Ol
o ° o •» 0
OOOOOl
0 ° O ° 0
OOOOO'
O " OP 0
OOOOOi
0 9 0 ° 0
oooo O 1
0 " O o 0
oooo o-
O ° Q ° 0
oo o.o o
O " 0 " 0
ooobo
0 o 0 o 0
ooooo
0 ? 0 » 0
ooooo
O " 0 ° 0
ooobo
0 °. 0 "0
oo ooo
0 o 0 *• 0
oooo o OOQOO
ooobo
0 ° 0 ° 0
ooooo
0 o. 0 ".6
ooooo
O " O ». 0
ooooo
0 " Q o 0
loo ooo
O " O ° 0
po o.oo
0 " 0° 0
ooooo
0 ° O o 0
ooooo
0 " O ". Q
lO.o.ob o^
O o 0 o 0
Inn nnn
c
13
-s 1
O 1 O !
— (U *
^H
^H • ^H ^^ • • •
^J ^1
fcfe^a
^^
^^p 1 ^1
^^^3 ^^^3
•
•
1 1 1 1 1 1 1 1 ^H
~-1 ^1
)r Q»
•9 ' 3c
i 1
i 3 _c
01
Q.
E
o (/I
d '
z 01
E 1
o l/l
.o
o .3
& o-
> 1 ^o *c &
o
1.5 ppm
0.3 ppm
Well Construction
Conductor Casing;
type; dia:0.00in fm: 0.00' to: 0.00'
Blank Casing:
]ype;PVC dia;2.00in fm;0.0' to:214.0C
Screens;
type: Slotted size-.010india;2.00in fm: 214.00lo: 234.0(
Annulor Rll:
lype: Concrete Grout fm;0.00' lo: 1.00'
type; Bentonite fm: 1.00' to; 211 .OC
lype: Sond RIter fm: 211.00' to; 235.0C
Description/Soil Clossification
(Description Interval)
(142 - 170') SANO AND GIWVEL; trace cloy.
fine groin lo gronulor up lo 1 inch, slightly moist, no odor.
no stoin, interbedded grovel, cobbles, boulders, red and groy
sandstone, chert, limestone, quortzite, gobbro.
ERU-Rocky MounUln, Ine.
UOO South nllou Mn Suite no Cunuiiiil Vlllafo, ERM (SSTMI-I
BOREHOLE LOG Borehole Number
BP-02
Poge 10 of 14
Project Number; U69005.1
Project: Bocchus Pond
Locolion: Mogno, UT
Totol Depth; 235.00'
Surface Elevation;
Northing:
Eosting
Borehole Diameter 9.50in
Uor/-,,lse
Drilling Company: Loyne Christensen
Drilling Method; Becker-Hommer
Dniler Bloine
Log By; P. Corbetto
Dote Drilled: 08/01/96
c^
^-^
o
163-
164-
165-
166-
167-
168-
169-
170-
171-
172-
173-
174-
175-
176-
177-
178-
179-
O^ 3
u .c
o
0 o 0 o 0
OOOOO
0 ° 0 o 0
ooooo
0 o 0 o 0
oooo o
0 o 0 o 0
ooooo
0 ? 0 o 0
ooooo
0 o 0 " 0
oo ooo
OOQOO
ooooo 0 o 0 o 0
ooooo
0 o 0 o 0
OOOOO 0 o 0 o 0
OO ooo
Q o Q o 0
OOOOO
0 o 0 o Q
OOOOO
0 o 0 o 0
ooooo
0 o 0 o 0
oooo o 0 ? 6 o 0
ooooo 0 o 0 o 0
OOOOO
Q O 0 O 0
OOOO o
O ? 0 o 0
OOOOO
0 o 0 o 0
OOOOO
0 o 0 o 0
ooooo.
Q o 0 o 0
ooooo
OOQOO
ooooo 0 o o o 0
ooooo
c:
TJ
3
m
o (J
%
^d ^m
^==sq
B •
^^ ^^ 1 1 1 s ^^ ^9 I 1 1 I ^^s ^^^
1 1 1 H 1 1 1 1 1 1
S
^ ^^ ^^ ^^s
^B
^
5!
03
^_
*
? 03
_C
•o. E
to
z
03
to
J3
^
o o. i?
tl
c
o
0.3 ppm
Well Construction
Conductor Cosing;
type: dio;0.00in fm; 0.00' lo; 0.00'
Blonk Cosing:
type; PVC dio; 2.00in fm: 0.0" to: 214.0(
Screens:
type; Slotted size--010india;2.00in fm: 214.00to; 234.0
Annular Rll:
type: Concrete Grout fm;0.00' lo; 1.00'
type: Bentonite fm; 1.00' to; 211 .Of
type: Sond RIter fm: 211.00' to: 235.01
Description/Soil Classification
(Description Interval)
Al 162", boulder
Al 167"; dry.
(167 - 180') SAND ANO GRAVEL; light brownish groy, dry.
Project Number U69005.1
Project: Bocchus Pond
Location: Mogno, UT
Owner Hercules
Drilling Compony; Loyne Christensen
Drillinq Method: Becker-Hommer
Driller Bloine
Log By: P. Corbetto
Dole Drilled; 08/01/96
Total Depth: 235.00'
Surface Elevotion:
Northing:
Eosting
Borehole Diameter 9.50in
Well Construction
Conductor Cosing:
type: dio:0.00in fm: 0.00' to: 0.00'
Blonk Casing;
type; PVC dia;2.00in fm: 0.0" to; 214.0
Screens;
type: Slotted sizei010india;2.00in fm; 214.00to; 234.0
Annular Rll;
type; Concrete Grout
type: Bentonite
type: Sond RIter
fm:0.00' to; 1,00'
fm:1.00' lo: 211.01
fm: 211.00'to: 235.01
£
01
Cl.
E
Descriplion/Soil Classification
(Description Intervoi)
181
182
183
184-
185-
186
187-
188-
189
190-
191-
192
193-
194-
195-
196
197-1
(180 - 195') SAND; some grovel, brown lo light
brownish gray, sligh(/y moist, pebbles at 190'.
(195 - 203") SAND; interbedded gravel, light brownish gray lo
brown, fine groin lo gronulor, pebbles up to 1 inch, subrounded,
slightly moist lo dry wiih depth, no odor, no stoin.
ERU-Rocky Mounuin, Ine.
HH South nilou Prin
Suite no
Crn««iiiil VIIU(.. CiUnli Mill ERM (»?"•-»««> BOREHOLE LOG Borehole Number:
BP-02
Page 12 of 14
Project Number: U69005.1
Project: Bocchus Pond
Locotion: Mogno. UT
Owner Hercules
Drilling Compony: Loyne Christensen
Drilling Melhod: Becker-Hommer
Driller Blaine
Log By: P. Corbetto
Dote Drilled; 08/01/96
Total Depth; 235.00'
Surface Elevation:
Northing:
Easting
Borehole Diometer 9.50in
Well Construction
Conductor Cosing;
type; dio;0.00in fm: 0.00' lo: 0.00'
Blank Cosing:
type; PVC dia;2.00in fm: 0.0' to; 214.0
Screens;
type; Slotted sizeL010itTJio:2.00in fm: 214.00lo: 234.0
Annular Rll;
type: Concrete Grout
type: Bentonite
type; Sond RIter
fm:0.00' to: 1.00'
fm:1.00' to; 211.0
fm; 211.00'to; 235.0
i g.
O
Descriplion/Soil Clossificotion
(Oescriplion Intervoi)
199-
200-
201
202
203
204 H
205
206-1
207
208H
209
210
211-
212-
213-
214
215
1.4 ppm
0.7 ppm
(203 - 220') SAND; troce cloy, brown, fine lo medium groin,
slightly moist, no odor, no stoin.
At 210', troce grovel, interbedded.
m^9 MM South muo* Mn
IIIMIIIH SUte no
ERM tSOS) 741-HM
EiOREHOLE
Project Number: U69005.1
Project: Bocchus Pond
Locotion: Mogno, UT
Owner; Hercules
Drilling Company: Loyne Christensen
Drilling Method: Becker-Hommer
Dniler Blame
Log By: P. Corbetto
Dote Drilled; 08/01/96
^=-*—'
o.
o
217-
218-
219-
220-
221-
222-
223-
224-J
225-
226-
227-
228-
229-
230-
231-
232-
233-
3
o
^^ ^s 0 o 0 o 0
ooooo O o 0 o 0
o o ooo
O o 0 o 0
OOOO o
O o 0 o 0
OOOO o
Q o 0 o 0
OO O.O o
0 o 0 o 0
O O OOO OOQOO
OO OOO
O o 0 o 0
OOOOO
O o Q o 0
o o o.o o O o 0 o p
oo ooo
O o 0 o 0
oo. ooo
O o O o 0
ooooo
O o 0 o 0
oooo o Q o o o 0
oo oo o
0 o 0 o 0
ooooo
O o o o 0
c
3
Tn
o o
S
:=
=
-
^=
_i=
==.
^:=
5
i_
?
1
^
01
CL E
LO
z
•5. E
to
J3
—1
fe CL
^
U
c
o
LOG
nnrphnip Kinmhpr*
BP-02
Page 13 of 14
Totol Depth; 235.00'
Surfoce Elevotion:
Northing:
Easting
Borehole Diometer 9.50in
Well Construction
Conductor Casing:
lype; dio: O.OOin fm; 0.00" to: 0.00'
Blonk Casing;
type; PVC dio: 2.00in fm: 0.0" to; 214.0
Screens:
lype: Slotted size:010india:2.00in fm; 214.00lo: 234.0
Annulor Rll:
type; Concrete Grout fm;0.00' to; 1.00'
lype: Bentonite fm: 1.00' to: 211.0
type: Sand RIter fm: 211.00' to; 235.0
Description/Soil Clossificotion
(Descr
(220
brown
(221
(222
groin
ption Inten/ol)
- 221") CLAYEY SAND; trace to little grovel,
fine lo medium groin, moist, no odor, no stoin.
- 222") SANDY CLAY; brown, moist, no odor, no stoin.
- 235") SAND AND GRAVEL; brown, very fine
to granular, pebbles up lo 1 inch, gravel up to 4 inches.
ongular lo subrounded, soturoted, no odor, no stoin.
RBM-Rockr MounUiD.
MH South miou Mn
Suite an
Inc.
T<Tt1# Ciooououl TUIoio. ColonJo Hill ERM (SOS)M.-HH
ElOREHOLF LOG Borehole Number
BP-02
Page 14 of 14
Total Depth: 235.00'
Project Number: U69005.1 Surface Elevotion:
Project: Bacchus Pond J^^?'"^: ' Eosting
Location; Mogno, UT
Owner Hercules
Drilling Compony: Loyne Christensen
Drilling Method: Becker-Hommer
Driller Bloine
Log By: P. Corbetto
Dote Drilled: 08/01/96
235-
236-
237-
238-
239-
240-
241-
242-
243-
244-
245-
246-
247-
248-
249-
250-
251-
cn o —1
•§.
o
o
u u u u u
O o 0 o 0
gt.o o.ojD
c
.9
"§
.t= tn c
3
1
1
03 1
01
01
Q.
E
d
z
03 a. E
o to
J3
.3
o
a.
tl
"c o
S'
O
Borehole Diameter; 9.50in
Well Construction
Conductor Cosing;
type; dio:0.00in fm; 0.00' to: 0.00'
Blank Cosing:
type: PVC dio;2.00in fm; 0.0' to;2I4.0C
Screens:
lype: Slotted size-.010indio:2.00in fm; 214.00lo: 234.0C
Annulor Rll;
lype: Concrete Grout fm:0.00' lo: 1.00'
lype; Bentonite fm; 1.00' lo: 211 .OC
type: Sond RIter fm: 211.00' to: 235.0C
Description/Soil Clossiflcolion
(Description Interval)
Al 235', added woter to odvonce drilling.
ERM-Rocky MounUin, Ino.
MU South miou Mn
suite no
ERM <*»> Mi-M" Vlllaco. Cilj'oJi Hill BOREHOLE LOG Borehole Number:
BP-03
Poge 1 of 12
Project Number; U69005.0
Project: Bacchus Pond
Locolion: Magna UT
Owner: Hercules
Drilling Compony; Foundex Pacific, Inc
Drilling Method; Becker-Hommer
Driller; T. Kunik
Log By: D. Johnston
Dote Drilled: 08/21/96 - 08/23/96
Total Depth: 206.00'
Surfoce Elevotion; 100.00'
Northing; 764.89
Easting 572.34
Borehole Diometer; 9.50in
Well Construction
Conductor Casing:
lype: dio; O.OOin fm; 0.00' to: 0.00'
Blonk Cosing:
lype: PVC dio;2.00in fm; -2.0" lo: 185.00
Screens:
lype: Slotted 5ize:010indio;2.00in fm; 185.00to; 205.00
Annular Rll:
type: Concrete Grout
type; Bentonite
type: Bentonite Pellets
type; Filler Sond
fm: 0.00' to: 5.00"
fm: 5.00' to: 180.00
fm: 180.00'lo: 183.00
fm: 183.00'to: 206.00
rni fil
a. E o to o
Description/Soil Classification
(Description Intervoi)
1-
8-
9-
10
11-
12-
13-
14
15-
16-
17
2.3 ppm
(0 - 7.0') SILTY SAND; light groy, few gravel, fine lo
medium grains, subrounded to subangulor, dense, slightly
moisl lo dry. no stoining, no odor.
6-r^
7-
(7.0 - 18.0') SILTY SAND; light reddish brown, few
cobbles, little gravel, fine to medium subongulor grains,
dense, slightly moist, no staining, no odor.
4.9 ppm
ERM-Rocky MounUln, Inc.
MH South nUou Drtn
viuoao. riiiioii Hill ERM SST^-JS? BOREHOLE LOG Borehole Number
BP-03
Poqe 2 of 12
Project Number; U69005.0
Project; Bocchus Pond
Locotion: Mogno UT
Owner: Hercules
Drilling Company: Foundex Pocific, Inc
Drilling Melhod: Becker-Hommer
Driller T. Kunik
Log By; D. Johnston
Dale Drilled; 08/21/96 - 08/23/96
Totol Depth;
Surfoce Elevotion:
Northing:
Easting
Borehole Diometer:
206.00'
100.00'
764.89
572.34
9.50in
Well Construction
Conductor Casing;
type: dia:0.00in fm; 0.00' to: 0.00'
Blonk Casing;
lype; PVC dio:2.00in fm: -2.0' to: 185.00
Screens:
type: Slotted size:010india;2.00in fm; 185.00to: 205.00
Annular Rll;
type; Concrete Grout
type; Bentonite
type; Bentonite Pellets
type; Filter Sond
fm: 0.00' to; 5.00"
fm;5.00' to: 180.00
fm: 180.00'to; 183.00
fm: 183.00'to: 206.00
Description/Soil Clossification
(Description Interval)
19
20
21-1
22
23-
24-
25-
26-
27
28-
29
30-
31-
32
35
34
35
O.o
o o
oo
O o
ob
6 o
OO
0 o
ob
o o
oo
O o
ob.
o o
Ob.
O o
ob
O o
OO
Q o
OO
O o
o.do
O O Q
O.O o
0 ° o
o.o o
0 o o o.o o
0 o o o.o o
0 o o
ooo
0 o. 0 ooo
0 ° 0 ooo
0 ?. Q
ooo
O 9 0 ooo
O o o
ooo
a o o
,nn n
(18.0 - 27.0') GRAVELLY SAND: brown, few silt,
fine to medium groins, subangular, dense, slightly moist,
no stoining, no odor.
0.5 ppm
1.8 ppm
(27.0 - 39.0') SANDY GRAVEL: brown, few silt,
fine to coarse subangular grains, dense, slightly moist, no
stoining, no odor.
ERM-Rocky MounUln. Ine.
HH Soulh VIUou Drtn
ERM ^^-i!2r"—-'" BOREHOLE LOG Borehole Number
BP-03
Page 3 of 12
Project Number; U69005.0
Projecl; Bacchus Pond
Location; Mogno UT
Owner: Hercules
Drilling Compony: Foundex Pocific, Inc
Drilling Method: Becker-Hammer
Driller: T. Kunik
Log By; 0. Johnston
Dote Drilled: 08/21/95 - 08/23/96
Total Depth: 206.00'
Surfoce Elevotion: 100.00'
Northing: 764.89
Eosting 572.34
Borehole Diometer; 9.50in
Well Construction
Conductor Casing:
type: dio:0.00in fm: 0.00' lo: 0.00'
Blank Cosing:
type: PVC dio:2.00in fm:-2.0' to: 185.00
Screens:
type; Slotted size:010irdio;2.00in fm; 185.00to: 205.00
Annular Rll;
lype: Concrete Grout
type: Bentonite
type: Bentonite Pellets
type: RIter Sond
fm: 0.00' to: 5.00'
fm: 5.00' to; 180.00
fm: 180.00'to: 183.00
fm: 183.00'to; 206.00
Description/Soil Clossification
(Description Interval)
(39.0 - 43.0') SANDY GRAVEL: brown, few silt, fine to
coorse, subongulor groins, dense, wet, no stoining, no odor.
5.9 ppm
(43.0 - 48.0') CLAY; weok red, trace sond, trace gravel,
soft, moisl, plostic, no stoining, no odor.
(48.0 - 57.0') CUVY: weak red, little gravel, troce sand,
soft to medium stiff, moist, plostic, no staining, no odor.
ERM-Rocky MounUln. Ino.
MH Soulh WUM Mn suite uo
ERM <*»> «i-«<»»'
BOREHOLE LOG Borehole Number:
BP-03
Poge 4 of 12
Project Number: U69005.0
Projecl: Bacchus Pond
Localion: Mogno UT
Owner; Hercules
Drilling Company; Foundex Pacific, Inc
Drilling Method: Becker-Hommer
Driller T. Kunik
Log By: 0. Johnston
Dote Drilled; 08/21/96 - 08/23/96
Total Depth; 206.00'
Surface Elevotion; 100.00'
Northing; 764.89
Easting 572.34
Borehole Diometer; 9.50in
o
£
6.2 ppm
0.6 ppm
Well Construction
Conductor Casing;
type; dio; O.OOin fm: 0.00' lo; 0.00'
Blonk Cosing:
type: PVC dio:2.00in fm: -2.0' to: 185.00
Screens:
type: Slotted size--010indio;2.00in fm: 185.00to: 205.00
Annulor Rll:
type: Concrete Grout
lype; Bentonite
type; Bentonite Pellets
lype: Filler Sond
fm: 0.00' to: 5.00'
fm;5.00' to: 180.00
fm: 180.00* to: 183.00
fm: 183.00'to: 206.00
Description/Soil Classification
(Description Intervoi)
(57.0 - 72.0) CLAY: red to strong brown, little sand,
fine to medium groins, plostic, soft to medium stiff, very
moist, no stoining, no odor.
ERM-Rooky MounUio. Inc.
HM Soulh •Uteu Drtn suite no
T-IT-tlf e i Wllojo. Col»«o<o Hill BOREHOLE LOG Borehole Number;
BP-03
Poge 5 of 12
Projecl Number: U69005.0
Project: Bacchus Pond
Location: Magna UT
Owner; Hercules
Drilling Company; Foundex Pocific, Inc
Drilling Method: Becker-Hammer
Driller; T. Kunik
Log By: 0. Johnston
Dole Drilled; 08/21/96 - 08/23/96
Total Depth: 206.00'
Surfoce Elevotion: 100.00'
Northing; 764.89
Easting 572.34
Borehole Diometer: 9.50in
Well Construction
Conductor Casing:
type; dio:0.00in fm: 0.00' to: 0.00'
Blonk Cosing:
type: PVC dia:2.00in fm: -2.0' to; 185.00
Screens;
type: Slotted size:01 Oindio:2.00in Im: laS.OOto: 205.00
Annulor Rll;
type: Concrete Grout
type; Bentonite
type: Bentonite Pellets
type; Filter Sand
fm: 0.00' to; 5.00'
fm: 5.00' to: 180.00
fm: 180.00'to; 183.00
fm: 183.00'to: 206.00
E o to
0.5 ppm
o
1.9 ppm
Description/Soil Clossificotion
(Description Interpol)
(72.0 - 85.0') SANDY CLAY; strong brown, trace silt,
little grovel, few cobbles, subangulor, fine to coarse
sand groins, well graded, medium stiff, moisl to very moist,
no stoining, no odor.
(85.0 - 94.0') CLAYEY SAND; red, troce silt.
litlle grovel, fine to medium, angulor groins, very dense
moisl, no stoining, no odor.
ERU-Rocky Mountain, Inc.
MM SouU SUloo Mn Suite ne Cii.oi lli flUooo. Colons Mill ERM (Sr^-JSf
BOREHOLE LOG Borehole Number:
BP-03
Poge 6 of 12
Project Number: U69005.0
Project: Bocchus Pond
Locotion; Mogno UT
Owner: Hercules
Drilling Compony: Foundex Pocific, Inc
Drilling Method; Becker-Hammer
Driller T. Kunik
Log By: D. Johnston
Dole Drilled: 08/21/96 - 08/23/96
Total Depth: 206.00'
Surface Elevotion: 100.00'
Northing: 764.89
Easting 572.34
Borehole Diameter: 9.50in
Well Construction
Conductor Cosing;
lype; dia: O.OOin fm: 0.00' to: 0.00'
Blonk Cosing:
type: PVC dio:2.00in fm:-2.0' lo: 185.00
Screens;
type: Slotted size:010india:2.00in fm: 185.00to: 205.00
Annular Rll;
type: Concrete Grout
type; Bentonite
type; Bentonite Pellets
type: Filler Sond
fm: 0.00' to: 5.00'
fm; 5.00' to: 180.00
fm: 180.00'to: 183.00
fm: 183.00'to: 206.00
Descriplion/Soil Clossification
(Descripfion Intervoi)
2.3 ppm (94.0 - 96.0') CLAY; strong brown, little sond, trace
gravel, subongulor, fine to coarse sond grains, very dense,
very moist, no stoining, no odor
(96.0 - 102.0") CLAYEY SAND; reddish brown, trace
gravel, medium groins, subongulor, moist, no stoining, no odor.
1.9 ppm
(102.0 - 108.0") SILTY SAND: light groy, fine
grains, subrounded, slightly moist, very dense, no stoining,
no odor.
ERM-Rocky MounUln, Ine.
ERM t»>> «i-MM
BOREHOLE LOG Borehole Number;
BP-03
Poge 7 of 12
Projecl Number: U69005.0
Project; Bocchus Pond
Location: Mogno UT
Owner: Hercules
Drilling Compony: Foundex Pacific, Inc
Drilling Method: Becker-Hommer
Driller T. Kunik
Log By: D. Johnston
Dole Drilled: 08/21/96 - 08/23/96
Totol Depth; 206.00'
Surfoce Elevotion; 100.00'
Northing; 764.89
Easting 572.34
Borehole Diometer: 9.50in
109-
110
IIH
112
113
114-
115
116
117-
118-
119-
120
121
122
123-
124-
125-
o
£
E o to
E o to
ty \-O
0.4 ppm
Well Construction
Conductor Cosing:
type; dia; O.OOin fm; 0.00' lo; 0.00"
Blonk Casing:
type; PVC dio;2.00in fm; -2.0' to: 185.00
Screens;
type: Slotted size:010india:2.00in fm; 185.00to: 205.00
Annular Rll;
type: Concrete Grout
type: Bentonite
lype: Bentonite Pellets
type; Filter Sand
fm: 0.00' to: 5.00'
fm;5.00' to: 180.00
fm: 180.00'lo: 183.00
fm: 183.00'to; 206.00
Descriplion/Soil Clossificotion
(Description Interval)
(108.0 - 112.0') GRAVELY SAND: strong brown, trace silt,
fine to coorse groins, subrounded, slightly
moisl, no staining, no odor.
(112.0 - 115.0') SAND: reddish brow, trace silt, little
gravel, fine to medium grains, subrounded, very dense, moist,
no stoining, no odor
(115.0 - 122.0') GRAVELY SAND: reddish brown,
troce silt, fine to medium groins, subangular, very dense,
moist, no staining, no odor.
2.9 ppm
(122.0 - 128.0') SAND: light reddish brow, little gravel,
troce silt, fine groins, subrounded, very dense, moisl, no
stoining, no odor.
ERM-Rooky MounUln, Ino.
ERM Sw^-BOREHOLE LOG
Borehole Number:
BP-03
Poqe 8 of 12
Project Number; U69005.0
Project: Bacchus Pond
Locotion: Mogno UT
Owner; Hercules
Drilling Compony: Foundex Pocific, Inc
Drilling Method: Becker-Hommer
Driller: T. Kunik
Log By: D. Johnston
Dote Drilled: 08/21/96 - 08/23/96
Totol Deplh: 206.00'
Surfoce Elevation: 100.00'
Northing: 764.89
Eosting 572.34
Borehole Diameter; 9.50in
127H
128
129-
130-
131-
132-
^53-
134-
135
136
137-^)
138
139
140-
141-
142-
143-
OO Od
O ° 0
OO Od
O °. 0
oo Od o ° o
oo Od
O °. Q
OO Od
O o O
OO Od
O ° 0
OO Od
0 ° o
OO Od
Q ° 0
OO Od
O o o
OO Od
O ° c
f-t n—£
s
Well Construction
Conductor Cosing:
type: dio:0.00in fm: 0.00' lo; 0.00'
Blonk Cosing:
lype; PVC dio:2.00in fm:-2.0" to: 185.001
Screens:
type: Slotted size:010ift)io:2.00in fm: 185.00lo: 205.001
Annular Rll;
type: Concrete Grout
type: Bentonite
type: Bentonite Pellets
type; Rller Sand
fm; 0.00' to: 5.00"
fm: 5.00' to; 180.00
fm; 180.00-to: 183.00
fm;l 83.00'lo; 206.001
Description/Soil Classification
(Description Interval)
3.7 ppml
(128.0 - 138.0') SANDY GRAVEL: brown, troce silt.
fine to coarse gravel, subrounded, fine to medium sand groins,
very dense moisl, no stoining, no odor.
(138.0 - 142.0') GRAVELY SANO: reddish brown,
troce silt, fine lo coarse subongulor sond grains, subrounded
grovel, very dense, moist, no stoining, no odor.
ERU-Rooky MounUln. Ino.
MH South SUteu Mn Suite no mil ERM tSM) T4I-MM BOREHOLE LOG Borehole Number:
BP-03
Page 9 of 12
Projecl Number: U69005.0
Project; Bocchus Pond
Location; Mogno UT
Owner Hercules
Driiiing Compony: Foundex Pacific, Inc
Drilling Method: Becker-Hommer
Driller T. Kunik
Log By: 0. Johnston
Dote Drilled: 08/21/96 - 08/23/96
Totol Depth: 206.00'
Surface Elevation: 100.00"
Northing: 764.89
Easting 572.34
Borehole Diameter: 9.50in
Well Construction
Conductor Cosing;
type; dio: O.OOin fm; 0.00" to; 0.00"
Blank Cosing:
type: PVC dio:2.00in fm; -2.0" to: 185.00
Screens:
type: Slatted size:010irriio;2.00in fm: 185.00to; 205.00
Annulor Rll:
lype: Concrete Grout
type; Bentonite
type: Bentonite Pellets
lype: Filler Sond
fm; 0.00' lo: 5.00'
fm:5.00' to: 180.00
fm: 180.00'lo: 183.00
fm: 183.00'lo: 206.00
o
o
a.
E
E o
Description/Soil Clossificotion
(Description Inlerral)
145-
146-
147-
148-
149-
150-
151-
152-
153-
154-
155-
156-
157-
158-
159-
160-
161-
3.4 ppm
(142.0 - 154.0) GRAVEL SAND: light reddish brown,
trace sill, fine lo coarse subangular grains, fine
groin subrounded gravel, very dense slightly moisl lo moist,
no stoining, no odor.
0.5 ppm
(154.0 - 163.0') SANO: light reddish brown, little
gravel, troce silt, subangulor fine to medium grains, very
dense moist, no staining, no odor.
ERM <"»>«
ERM-Rooky MouoUin, Ine.
MH South nlou Dlin Aute no Mill BOREHOLE LOG Borehole Number:
BP-03
Poqe 10 of 12
Project Number; U69005.0
Projecl: Bocchus Pond
Locotion; Moqno UT
Owner: Hercules
Drilling Compony; Foundex Pocific, Inc
Drilling Method: Becker-Hommer
Driller T. Kunik
Log By: D. Johnston
Dote Drilled; 08/21/96 - 08/23/96
Tolol Deplh; 206.00'
Surfoce Elevotion: 100.00"
Northing; 764.89
Easting 572.34
Borehole Diameter; 9.50in
cx
167
168-
163 li o:o: <j \.
0 o o
164-|) OOOC
o o o
165-t> OOOC
o o. 0
166-b OO.Od
3 O ° O
_) OO. OC
0 o O
b od Od
169-
170-
171-
172
173
174
175
176-f
177
178-
179-
O o O
) O O OC
U ""0
) OOOC
o ° o
). oo OC
0 ° o
) OO OC
0 ° o
) OOOC
3 r, o f\
o
4.1 ppm
Well Construction
Conductor Cosing:
type: dio:0.00in fm: 0.00' to: 0.00'
Blank Casinq:
type: PVC dio:2.00in fm:-2.0' to: 185.00
Screens
type; Slotted sizei010indio:2.00in fm: 185.00to: 205.00
Annular Rll:
type: Concrete Grout
type: Bentonite
type; Bentonite Pellets
type: Rller Sond
fm: 0.00' to: 5.00'
fm: 5.00' to: 180.00
fm: 180.00" to: 183.00
fm; 183.00'lo: 206.00
Description/Soil Classificolion
(Description Interval)
03 ppm
(163.0 - 169.0') SANDY GRAVEL: brown, trace silt,
fine to coarse, subongulor grains, fine to coarse subangular
sond. well graded, slightly moist, no stoining, no odor.
(169.0 - 173.0') SAND: light reddish brown, fine to
coarse subangulor groins, well groded, very dense, slightly
moist, no stoining, no odor.
(173.0 - 177.0') SANDY GRAVEL; brown, fine
subrounded groins, fine subongulor sond groins, very dense,
slightly moist, no staining, no odor
(177.0 - 180.0') GRAVELY SAND: brown, fine to
coarse subrounded groins, fine subrounded grovel, well graded,
very dense slightly moist, no stoining, no odor.
1 kllllljtUU ERU-Haoky UounUIn. Ino.
1 mSI "" x*^ *<>i~ °**"
1 iimniiiiii &iiu no ERM p»»«i-MH^
BOREHOLE LOG
j Project Number: U69005.0
Project; Bocchus Pond
1 Locotion: Mogno UT
Owner: Hercules
1 Drilling Compony: Foundex Pocific, Inc
Drilling Method: Becker-Hommer
j Driller; T. Kunik
Log By: D. Johnston
1 Dote Drilled: 08/21/96 - 08/23/96
1 ^^
-—^ JZ . a.
1 o
, 181-
182-
|l83-
1 QA
Il85-
186-
187-
1188-
1 BQ —
|l90n
19H
'l92-
1193-
194-
|l95-
196^
'l97-
Oi
.3
o -c CL
o
3 O O O C
5 0 o O «
3 OOOC
= O o O <
) O OOC
3 O O Q <
) oo OC
3 O a Q «
3 O O Q <
) o0 oc
3 O o O <
) o boc
3 0 o Q <
) ob o.q
3 O ° 0 <
) oooo
3 O O Q C
) oo oc
3 O o 0 '
) ob. oc
' O °. O '
) oo oc
3 o o o *
) ob oc
3 Q o o <;
) ob OC
c
"o
•K
c o c_>
^
S-S i ss-s siss s°s
=
:
==
:=
.
^=
=
-z—
^=
^=
^
ssfs i "Sot sii sSsi
Hv^t
>
—1
^ _03
s
\/
"5
c
•QL E
«^
z
O-
tyl
XI
.3
Borehole Number:
BP-03
Page 11 of 12
Total Depth; 206.00'
Surfoce Elevotion: 100.00'
Northing; 754.89
Eosting 572.34
o o.
•y
o c o
o
0.4 ppm
0.6 ppm
Borehole Diomeler: 9.50in
Well Construction
Conductor Cosing;
lype; dio; O.OOin fm: 0.00" lo; 0.00'
Blank Cosing;
type: PVC dio:2.00in fm: -2.0' to: 185.00
Screens;
lype: Slotted size^OI Oindio: 2.00in fm: 185.00to: 205.00
Annulor Rll;
lype: Concrete Grout fm: 0.00' to; 5.00'
lype: Bentonite fm; 5.00' lo; 180.00
type: Bentonite Pellets fm; 180.00' to: 183.00
type; Rller Sand fm: 183.00' lo: 206.00
Descriplion/Soil Clossificotion
(Description Interval)
(180.0 - 184.0") SANOY GRAVEL: brown, fine
subrounded groins, fine to coarse subrounded sond groins.
very dense, slightly moist, no stoining, no odor
(184.0 - 187.0") SAND: brown, few grovel, fine lo medium
subrounded grains, slightly moist lo moist, no staining,
no odor.
(187.0 - 189.0") SAND: brown, little gravel, few cobbles.
fine to medium subrounded grains, very dense, moisl,
no staining, no odor.
(189.0 - 193.0") SANDY GRAVEL: brown, fine groin
rounded gravel, fine to coarse groin, subrounded sond, very
dense, moisl lo wet, stoining, odor.
ERM-Rocky HouaUIn, Inc.
MH South nitou IMn
ERM t*»> »««-"«•
BOREHOLE LOG Borehole Number;
BP-03
Poqe 12 of 12
Project Number: U69005.0
Project: Bocchus Pond
Locotion; Mogno UT
Owner: Hercules
Driiiing Company: Foundex Pacific, Inc
Drilling Method: Becker-Hommer
Driller T. Kunik
Log By; D. Johnston
Dole Drilled: 08/21/96 - 08/23/96
Totol Depth; 206.00'
Surface Elevotion: 100.00'
Northing: 764.89
Easting 572.34
Borehole Diameter: 9.50in
Well Construction
Conductor Cosing:
type; dio:0.00in fm: 0.00' lo: 0.00'
Blonk Cosing:
type: PVC dio:2.00in fm: -2.0' to: 185.00
Screens:
type; Slotted size-.010irdio;2.00in fm: 185.00to: 205.00
Annular Rll;
lype; Concrete Grout
type; Bentonite
type: Bentonite Pellets
type; Rller Sand
Im: 0.00' lo: 5.00
fm:5.00' to; 180.00
fm: 180.00'to: 183.00
fm: 183.00'to; 206.00
OO OC
CO 0
OOOC
o " o «
OOOC
O o 0
) oo oc
n ° n
Q. E o to
Description/Soil Classification
(Description Intervoi)
199-
200-
201-
202-
203-
204-
205--^
206----— -I
207-
208-
209-
210-
211-
212-
213-
214-
215-
(193.0 - 202.0') SANDY GRAVEL: brown, fine to
rounded gravel, fine to coarse subrounded sand grains, well
graded, very dense, wet to soturoted. no stoining.
(202.0 - 207.0") SILTY SAND; light reddish brown,
little cloy, fine subrounded groins, , medium dense,
soturoted, no stoining, no odor
0.5 ppm
b,,AFf I
BNVIRONMENTAL BASELINE
ASSESSMENT
Bacchus Plant 3
Magna, [Jtah
APPENDIX D
LABORATORY REPORTS
a=ffiffro
AUii I , lfln
uffit,o,W,o*
SOLID & HAZARDOUS WASTEPgHw-lqgb- ooa3B
Hercules, Inc.
Hercules Plaza,l3l3 Market Street
Wilmington, DE 19898-0001
30 September, 1996
ERM-Rocky Mountain, Inc.
102 West 500 South, Suite 650
Salt Lake city, utah 84101-2334
(801) ses-8400
ERM.
I b,*ilFr 1
ENVIRONMBNTAL BASBLINE
ASSESSMENT
Bacchus Plant 3
Mogna, Utah
APPENDIX D
LABORATORY REPORTS
Hercules, Inc.
Hercules Plaza, 1313 Market Street
Wilmington, DE 19898-0001
30 September,1996
ERM-Rocky Mountain, Inc.
102 West 500 South, Suite 650
Salt Lake City, Utah 84t01-2334
(801) s9s-8400I
I
I
I
I
T
I
t
I
tr
(I)Lancaster Laboratories Page: '1 of
A Thermo Analytical Laboratory
LLI sample No. ES 2538092cottected: 6/26/96 at 13:07 by Bn
Subnitted: 6/28/96 Reported: B/ 7/96Discard: 9/ 7/96
P. O.
Ret.
Soil.-1 Grab Soit Sampte
Hercutes: Bacchus Pond
SL'l -- SOG#; HBP02'15
T
Account No:06716
Hercutes, lncorporated
Envi ronmen!at Affa i rs
Uitmington DE 19894
AS RECEIVED
tffi
.646
1647
ltii
l65t+
tl:?,666
1672
Ii;
0111
I
I
I
I
I
I
I
I
I
I COPY
1 COPY
ANALYSIS NAHE
Thal.titrnt
A I umi num
Ant i mony
Barium
BeryI t i tnn
Cadnti um
Chromi um
Copper
I ron
Lead
Manganese
N i ckeI
Si Iver
Zi nc
Arsenic TR
Seteniurn TR
I'lercury
Moi sture
"lloisture'r lepfesents the Ioss
103 - '105 degrees CeIsius.
_ :j:j::::j.:,::::::ji::::qrE{rll Tc
.r.i.r.ilrrf,ri! i:ir.... lt . e '
I iii.:i::.'!.i:ii:il} ii.1u v,!
]::.::::::::,::,:::::I].:.],::i. o1,,1i!]!,!.]11]i'l!1,!,lp,,l: l:]:::,:,:::.:.:,:,:::::::::,::,.,:]i:, .,,^ -: ji..l:ij,j.rrrr:::::jl-ll, U,l :
j.:,...,i:..., ::lyii
HET HOO
DETECT!ON LII.IIT UNITS
13. ng/kg8.6 mg/kg?.1 mg/kg2.1 mslkg0.070 ms/ksi 0. 12 mslkg0.41 nts/kg0.LB mg/kg
DRY IJE I CHT
::,: :,..,:::::::::::::::::::::::::::,.::::-:',: :,1.::: METH0D; -r ".a..a1- ;.j!!rr: a. !-.a.! i tr"..r":. :a--. r|!
,,,,'.:,.ii.i.lit,i (Egtttt8..i.ii::ii DETECT I otl L I M I 1
. tt.: 11.:^.:: 1.6,, 2.6,, 0.087,,,.r 0.15,, 0. 55,,, 0.59,,. 4.C::.a 2.8
0.14,, 0. 54
U. >J':, 0.47
0. 29
0.71
0. 035
,,,i:ii ,r,:,','i,9;C60- 3.2 n1/'<g:.:.::::::.:'.:::.:::.:::::.:r1.q 23 ng/'Kg
.]:i:rill.:l:l:ll:i:::::?,+J:' ' C'1'1 mS/kS
:i:::::.: ::::.:::::::: i::: ::i:: :::. .? . 3 D . /4 4 mg / k S
:::.;ii:.:::.i:iii.:i.::::l:.l,'l:.u . o ' 0 ' 4 3 ms/ ke
,::::::::::::::::::::::::,::.::::.45. ] 0.38 mg/kg:.:::r:.:::::.:.::::::.t:::r:..7..C C.21. mg/kg
Lt. l7 mg/kg
:;,,..::i,,:',,,,,,,,::,t,:.,,,,,, lt.l. 0.028 nq/kg
,,,.,,,r,,:,,,:i,.,.,,',,'.,,,,::lt.g- Z C . 06 .'1 by wt .
in reight oi the sampte after oven drying at
TO
TO
Hercutes, I ncorpocated
ERM - Rocky Hountain
ATTtI: Yr. Joseph Kel Ier
ATTl.l: ilr. Erent Robinson
Questions? Contact your Ctient Services Representative
Rachel. L. Kreamer at (7'7) 656-2300
05:41:55 D 0002 23 REP 1261.36 52?739
3 1 0 25.00 00030400 ASR0o0
Larcaster Laboratori€s
2425 New Holland Prke
PO Box I2425
Lcncaster PA 17505-2125
717'656-2300 ;ar 717-556-2681
RespectfuL Ly Subnri tted
Ranlona V. Layman, GFoup Leader
ICP Metats/Leachates
i'pMEMBEFI
!ae re'/erse srCe io, explarlatro6 3f 5'7nr[615 and :DbrevraI'ofis 2215 P.e'.' 1013At95
!&&
(I)La ncaste r Laboratories Page:2ofA Thermo Analytical Labor4tory
LLI sample No. Es 2538092Cottected: 06/?6/96 at 13:07 by BR
Submi tted: 06/28/96
Account No: 06716
Hercutes, lncorporated - DE
Envi ronmentaI Affai rs
Uitmington 0E 19894
,I
I
I
I
I
Soi[-1 Grab Soit Sampte
Hercutes: Bacchus PondSL1-- SOG#: HBP02-13
CATilO ANALYSIS NAITIE
1625 ThaI t itrn
1643 Atuminum
164t+ Ant i rnony
1646 Earium
1647 Eeryttium
1649 Cadmiurn
1651 Chromium
1653 Copper
1651+ I ron
1 655 Lead
1658 Manganese
1661 N ickeL
1666 Si Lver1672 Zinc5708 SU StiB46 ICP Digest6935 Arsenic TR
6936 Setenium TR
0159 Hercury5711 SU S}JB46 Hs 0isest
01 11 l',loi stuie
I',tETHOD
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
srJ-846 60'l0A
su-846 6010A
su-846 6c10A
su - B4 6 60'l 0A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
srJ-846 3C50A
su-846 6010A
su-846 6010A
su-846 7471A
su-846 7471A Modified
EPA 160.3 (modified)
ANALYS I S
TRIAL DATE AND TIME
1 07/13/96 18331 07/13/96 18331 07/13/96 18331 07/13/e6 18331 07/13/96 18331 07/13/96 18331 07/13/96 18331 07/13/96 18331 07/13/96 18331 07/13/96 18331 07/13/96 18331 07/13/96 18331 07/13/96 18331 07/13/96 18331 07/0?/96 19341, 0t/13/96 1833i 07/17/96 09t+4
1 07/03/e6 16451 07/02/96 1506
1 07/02/96 15?0
ANALYST
Jotene M. Schietds
Jolene M- Schietds
Jotene I'1. SchieIds
Jotene M. SchieLcis
Jotene M. Schietds
Jotene I'1. SchieLds
JoIene M. Schietds
Jotene I{. Schietds
Jotene M. Schietds
Jotene M. Schields
Jotene M. SchieLds
Jo I ene I'1. Sch i e Lds
Jotene l'l. Schietds
JoIene M- SchieIds
Desi R. Carozza
Jotene M- Schiel.Cs
Nina C. HaIter
Hel.Li S. l'{arkaryan
Frances A. Demorest
Neetay B. l'{ehta
I
I
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t
I
I
I
I
I
I
I
MEMEtEFl,eriil
Lancagter LaborJtones
2425 New Holland Pike
PO Box 12425
Lancaster. PA 17605-2425
717-556-230O Fax: [phone] I {l
I,ABORATORY CHRONICLE
See reverse srde for erolanatron of symbois and abbre'/ratron!))16 Re.t 1A/3Ai95
QUALITY CONTROL REPORT
(iI)I La ncaster Laborato ries
A Thermo Analytical Laboratory
I LLr sample No. 2538092
l,:::.1":, ",::::.:T::
I
SampI e
UNITS
mg/ kg
mg,/ks
mg/ kg
mg/kg
mg/ ks
mg/ kg
mg/ks
mg/kg
mg/kg
mg/ks
ng/kg
ms/ks
mg/ kg
ms/ kg
both determ'inations llas tess
lras more than four times the
BLA}IK
Batch:961845708C03
N.D.
Batch:951845708003
I'l-D.
Batch: 961845708003
ll .0.
Batch:961845708C01
IJ.D.
Batch:961845708003
N.D -
Batch: 961845708C03
N.D.
Batch: 961845708C05
N.D.
Batch:961845708C03
N.0.
Batch:961845708001
7 -Z J mglks
Batch:961845708003
N.D.
Batch:961345708003
N.D.
Batch:961845708C03
N.D.
Batch: 961845708005
N.D.
Eatch:96'18457080030.80 J mg/kg
Batch: 951845708001
N.D.
Batch:961845708003
N.D.
Batch: 9618/1571 '1002
N.D.
Batch : 9618403163200034
crolp ruo. 5?2739
HerFuIes, I ncorporated
P age:5oi
DE
Sanp I e
l^"::,-,13.I Aluminum
l"!:i"*
i Barium
l"iri;;-'. iadmium
0.12
l[::-
0 .48
l"::,2.3
I'l:ii; Si Iver
t,.t,*t.
0.24
I"i"lil
0.028
r";:;:,."
m9/ kg
mg/ kg
mg/ kg
% by ut.
96
79
79
100
9B
99
10?
102
B9
94
94
96
9B
9?
93
B7
79
'1 00 100
L II'II TS
HIGH
150
165
?99
131
177
174
141
145
142
142
135
146
147
149
149
1lrq
157
101
DUP }IS LCS LCS LCSRPD }4S HSO RPD LCS DUP RPD LOU
?1
9
0
0
0
0
13
0
1',1
0
6
9
?
5
7
1
6
4
5
6
6
0
,l
0
93
2027
92
105
96
93
1?B
119
?452
96
116
97
102
108
91
92
92
B9
1645
95
97
91
88
131
109
2139
90
109
91
97
98
9?
94
92
(2)
50
50
21
70
23
26
54
57
ot
5l
69
55
50
54
52
26
'100
(1)
(1)
(1)
(1)
(1)
(1)
('l )
('1 )
(1)
(1)
(1)
(1)
(?)
TR
TR
I
I
I
The result for one or
lhe
bactsround result
than five times the Loo.
spike added.
MEMBEFlrem
Lancaster Laboratcres
2-125 New Hollani Prke
PO Bor 12425
Lanc.rsler, PA 11 5A5- 2 A 25
7 17 -656-230A F zt 7',7 -e16-2621 'rp r'.r:s€ sr<ie {o. erplaratron o{ syrSois d.d illb'iv'al.Dns 22rb Re, ro/ro/es d?
lof
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lar
f;li' .646
1647
G,\
1654
tii
7b7?
ti;
0111
I
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(I)La ncaster Laborato ries Page:
DRY IJE I GHT
LLI Sample No. ESCottected: 6/?6/96 at 13:50
Subritled: 6/28/96 Reported:Discard: 9/ 7/96
A Thermo Analytical Laboratsry
2538094
by BR
8/ 7/96
Account Ho:06716
HercuLes, Incorporated - DE
Envi ronmenrrI Affa i rs
uitmington DE 19894
P.0.
Ret.
! soi l. -2 Grab soi t Sanrpte
I ,"..r,".: Bacchus pond
SLz- - SoG#: HBP02- 15
AS RECE IVED
ANALYS I S NAI'IE
Thattium
A tumi num
Ant imony
Bar i um
Beryt t i um
Cadmi um
Chromi um
Copper
I ron
Lead
Manganese
NickeI
Si tver
ZincArsenic TR
Setenium TR
llercury
I'loi sturerrl'.loisturett represents the Ioss
103 - 105 degrees Celsius.
tn
MET HOO
DETECTION LIMIT UNITS
1/+. mg/kg
,;ii,ia'i:,::iii;i tESUUI6
METHOD
DETECTION LlI,IIT
16.
10.
2.5
?.5
0.085
0. 15
0. 54
0. 58
3.9
2.8
o.14
0. 53
0.52
0.46
0.29
o.21
0. 033
2216 Re,.,ro/lo/e5 d'9
8.7 mS/kS2.1 mslkg?.1 mg/kg0.C7? mg/ks0.13 ms/kg0.46 ms/kg0.49 ms/ks3.3 nrg/kgZ-3 ms/kg0.1? flrg/kgC.45 ms./kg0.ttl+ m9/kg0.19 mglkg0.24 ms/kg0.17 ms/ks0.023 mg/ks0.06 % by ur.
oven drying at
1 COPY TO
I
1 coPY To
Hercutes, Incorpocated
ERM - Rocky Mountain
Questions? Contact your Ctient
Rachel L. Kreamer
03:43:.?8 D 0002 ?3 REP
310 25.00 00030400 ASR000
ATTN: Mc. Joseph Ke[ [er
ATTN: Mr. Brent Robinson
Servi ces Representative
at (717) 656'23CC
126t 36 52?Ti9
:60:,i
Respectfu[ [y Submi tted
Ramona V. Layman, Group Leader
I CP I'leta I s/Leachates
I
I
I MEMBEFl7eilir
Lancaster Laboratofles
2425 Ne,r Holland Pike
PO tsox 12425
Lancaster, PA 17 505-2425
71 7-656-2 300 F ax. 7 \1 -655-2521
'::ai 3:iiiiiil!ii:i.i:.. .:
ueight of the sampte a{ter
See reverse side for explanairon oi svmbols end abbreYratlons
!&&
Soit-2 Grab SqiI Sampte
Hercutes: Bacchus PondSL2-- SDG#: HBP02-15
CATNO ANALYSI S }IAI.IE
1625 Thattium1643 Atuminum
1644 Antimony
1646 Barium
1647 Beryt I iun
1619 Cadmir.rn'1651 Chromi um
1651 Copper1654 I ron
1655 Lead
1658 Hanganese
1661 ll ickeI
1666 S i Iver
1672 Zinc
5708 SU SU846 ICP Digest6935 Arsenic TR
6936 SeLenium TR
0159 l.lercury
5711 SU SU846 Hg Digest
0111 l',loi sture
Account |lo: 06716
Hercutes, Incorporated - DE
Envi ronmentaI Affai rs
Uitmington DE 19894
I,ABORATORY CHRONICLE
Page: ? ol
ANALYST
Jotene M. Schietds
Jotene l{. Schiel.ds
JoIene M. Schiel.ds
Jotene H. SchieLds
Jotene M. SchieLds
Jotene M. Schietds
Jotene M- SchieLds
Jotene M. Schiel.ds
Jotene M. Schietds
Jotene M- SchieLds
Jotene M. Schiel.ds
Jotene H. Schiel.ds
Jotene M. SchieLds
Jotene M. SchieLds
Desi R. Carozza
JoIene l,l. SchieLds
Nina C. Hatter
Netti S. I'larkaryan
Frances A- Demorest
Neeiay B. I'lehta
ANALYS I SIRIAL DATE AND TIHE
I
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t
t
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t
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M ET HOO
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-816 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
srJ-816 6010A
su-846 6010A
su-846 6010A
su-846 3050A
su-846 6010A
su-846 6010A
su-8/.6 7471A
su-846 7471A l.lodi f ied
EPA 160.3 (modified)
07/13/96 1853
07/13/96 1853
07/13t96 1853
07/13/96 1853
07/13/96 1853
07/13/96 1853
07/13/96 1853
07/13/96 1853
07/13/96 1853
07/13/96 1853
07/13/96 1853
07/13/96 1853
07/13/96 1853
07/13/96 1853
07/02/96 1934
07/13/96 1853
07/17/96 100?
MEMBEFlrefia
Lancaster Laboratorres
2425 New Holland Pike
PO Box 12425
Lancasier. PA 17 605-2425
7 17 -655.2300 Fdx /l 7-656-2681
1 07/03/96 16501 07/0?/96 1506
1 07/0?/96 1520
(I)h?[HS^tFJ,^L*9,'.B1gl'et
LLf Sample No. ES 2538094cottected: a6/?6/96 at 13:30 by BR
Subni tted: 06/28/96
5ee reverse side for erplanation of symbols and abbrevratrons 2216 Rev lot3o/e5
jl
l"
QUALITY CONTROL REPORT(l)La ncaster Laborato ries
A Thermo Analytical Laboratory
2538094
Safip t e
UHiTS
mg/kg
mg/kg
mg/kg
ms/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/ks
mg/kg
mg/ ks
mg/kg
mg/kg
mg/ kg
mg/kg
T
t
t
I
Page:lof
LLI Sample No
Soi t -2 Grab Soi t SanrpLe
Hercutes: Bacchus Pond
Group No.
Hercu I es,
5?273e
lncorporated - DE
DUPRPD HS
LCS LCS LCSDUP RPD LOU
MS
HSO RPD
LII.IiTS
HIGHLCS
96
79
79
100
9B
99
102
102
89
94
94
96
98
92
93
R7
79
100
ms/ k9
mg/kg
% by ur.
BLANK
B atch : 96 1 845708003
N.D.
Batch: 961845708003
H.D.
Batch:961845708003
N .0.
Batch:961845708003
N.D.
Batch:961845708003
N.D.
Batch:961845708C03
N.D.
Batch:961845708003
N.D.
Batch:961845708003
N.D.
Batch: 961845708C037.2 J mg/kg
Eatch:96184570EC03
H.D.
Batch: 961845708003
N.D.
Batch: 961845708003
N.D.
Batch:961845708003
N.D.
Batch:9618457080030.80 J mslkg
Batch:961845708003
N.D.
Batch:961845708003
N.D.
Batch:961845711002
N.D.
Eatch : 961840316820003A
(1) 93
21 20?7
(1) 92
9 105
0 (1) 96
0 ('l ) 93
0 ('r ) 128
0 ('r ) 1'19
13 ?45?
0 (1) 96
11 116
0 (1) 97
(1) 102
0 (1) 105
0 (1) 91
0 (1) 9?
0 (1) 92
a
five times the LOO-
added -
89
1645 (2)
95
97
91
8B
131
'109
?139 (2)
90
109
91
97
98
9?
94
9?
50 150
50 165
21 299
70 131
23 177
?6 174
54 141
57 145
61 142
53 142
69 135
55 146
50 117
54 149
49 149
5? 1le
26 157
100 101
6
9
2
7
s
7
1
6
4
6
7
6
0
1
0
I
t
I
) The
l'n"
resutt for one or both determinations Has less than
background resutt was more than four times the spike
I Lancaster Laborato(es
2425 New Holland Prke
PO 8ox 12425
Lancastei PA 17 605 -2425
71 7-656-2100 I ax. 7 17 -656-2681
t?^t}B,!g>ee re,,,erse srde for axcianatron of ;ymbois and abbrevldtionS 2116 Rev. l0/10/95
I
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T
t
t
T
t
frfr
1647
ffii
1654
liii
1672
ffi;
0111
(iI)La ncaster Laborato ries
Account No:06716
Hercutes, lncorporated - DE
EnvironmentaI Affairs
fJi Imington 0E 19894
Page:lof
P.0.
Ret.
DRY IJE I GHT
,:::::,,,,,.:.1.;:,1,'.:,,:::i;,1!.::,,rt:,,:,,1,,::,:,t,i,a:,:i ME T HoD
,:,:.:.:iiii::l::,:::,::::ft't8tJtlEi':iii:::; DETECT I0ll L I 14I T
17.
11.
2.7
?.7
0.089
0.16
0.57
0.60
4. I
?.9
0.14
0.55
0.54
0. 48
0. 30
o.2?
0. 034
A Thermo Analytical Laboratory
LLI sampj-e No. ES 2538095Cottected: 6/26/96 at 13:40 by BR
Subnitted: 6/28/96 Reported: B/ 7/96Discard: 9/ 7/96
Soit-3 Grab Soit SampLe
Hercutes: Bacchus PondsL3-- SDG#: HBP02-16
I,t:
AS
i:::ii::::iX:iiil:8ge-t4Is
RECE IVEDt:::::: HETHOO
,,,,1,:.;t:, DETECT ION LIMIT UNI IS
.:.:l:i 1l+ - mg/kg,':.., 9. 0 m9/kg
,,.;ir 2.2 mg/kg
ii.',i ?.2 mg/kg
,,.,,,,, 0.074 mg/kg:: J U. rJ mg/(g,,1',,t 0.47 mg/ks
: , 0.50 ms/kg, 4 ng/kg
',,:,,, 2.4 mg/kg
,,:,: 0.12 mS/kg
,, 0.46 ms/kg,:,,,, 0.45 mS/kg
, ,, 0.40 m9/k9,.:: 0.25 ng/'<g
,,:i 0.18 ms/kst, 0.028 mg/ksi., 0.06 % by rt.after oven drying at
ANALYS I S NAI'IE
Thattium
Atuninun
Ant imony
Bar i um
Beryl. I i un
Cadmi um
Chromi un
Copper
I ron
Lead
Manganese
N i cket
Si Iver
Zinc
Arsenic TR
Seteniunr TR
I.lercury
Mo i s tureI'Moisture, represents the toss in
103 - 105 degrees Cetsius.I
I
I
I
I
t
I
I
I
1 COPY TO
1 COPY TO
Hercutes, Incorporated
ERl.l - Rocky l.lountai n
Questions? Contact your Ctient
Rachet L. Krearner
03:44:08 D 0002 ?3 REP
310 25.00 00050100 AsR000
ATTII: Mr. Joseph KeI ter
AITN: l'4r. Brent Robi nson
Services Representativear (7i7) 656-2100
126436 5?2739
RespectfuI Ly Submi tted
Ramona V. Layman, Group Leader
ICP Metats/Leachates
MEMBEFl7Nm
Lancaster Laboratones
2425 New Holland Pike
PO Box 12.125
Lancaster 7A 17 605 -242i
1 17 -656-2300 lax 7 17 -656-2681 2r16 Rp,: ro/ro/e' tft,See reverse srcje for exolanairon oi;','mbols Jni abbre'rdlrons
i&&
LLI Sample No.
Cottected: 06/26/96 at
Suhni tted: 06/28/96
Soit-3 Grab SoiI Sanpte
Hercutes: Bacchus PondSL3-- SDG#: HBP02-16
CATNO ANALYSIS NAME
1625 That t iun
1643 Atuminum
16t14 Antimony1646 Barium
1647 Beryttiun
1649 Cadmiurn
1651 Chromium'1653 Copper1654 I ron
1655 Lead'1658 ['langanese
1661 NickeI
1666 Si Iver
1672 Zinc
5708 SU SU8/+6 ICP Digest
6935 Arsenic TR
6936 Seteniw TR
0159 Hercury5711 SU SU8/+6 Hg Digest
0111 l,loisture
(I)La ncaste r Laborato ries
A Thermo Analytical Laboratory
ES 2538095
13:40 by 8R
METHOD
su-816 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
srJ-816 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 3050A
su-846 6010A
su-846 6010A
su-8t+6 7471A
SU'81r6 71.71A l,todi f i ed
EPA 160.3 (modified)
Account Uo: 06716
Hercutes, Incorporated - DE
Environmentat Affairs
uitmington DE 19894
ANALYS I S
TR tAL DATE AND TII'IE
1 07/13/96 18581 07/13/96 18581 07/13/96 18581 07/13/96 1B5B1 07/13/96 18581 07/13/96 18581 07/13/96 18581 07/13/96 18s81 07/13/96 18581 07/13/96 18581 07/13/96 18581 07/13/96 18581 07/13/96 18581 07/13/96 1B5B1 07/02/96 19341 07/13/96 18581 07/17/96 1006
1 07/03/96 16521 07/02/96 1506
1 07/02/96 1520
I,ABORATORY CHRONICLE
Page: 2 ol
ANALYST
Jotene itl- Schietds
JoIene 14- Schietds
Jotene M. Schiel.ds
Jotene M. Schietds
Jotene M. Schietds
Jotene M. SchietCs
Jotene M. Schietds
Jotene M. Sch i etds
Jotene I'l . SchieLds
Jotene M. Schietds
JoLene t'l . Schietds
Jotene l'1 . SchieIcis
Jotene l,l. SchieLCs
Jotene I't. SchieLCs
Desi R. Carozza
Jotene I'1. schieLds
Nina C. Hat ler
NetLi S, Markaryan
Frances A- Demorest
Neelay B. Mehta
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MEMBER
,KTTT
Lancaster Laboratones
2425 New Holland Prke
PO Box 12425
Lnncastet PA 17605-2425
7 1 7-656-2300 Fax. [phone] See reyerse srde ior explana:rcn oi symbols and abbrev at'o4s 2216 Rev 1ot3o/e5 dll
l"
I
t
(iI)Lancaste r Laboratories Page: 3 of
r LLI Sample No.
I s"i t -3 Grab'soi t Sampte
Hercutes: Bacchus Pond
I
I ffir'"
> Tha[ liurn
l4-
J'il;"",,.Ant I mony
2.?
l,::;t,-
0 -0749 Cadmium
l,{'ii..
3 copper
l,.hl',> Lead
A Thermo Ana lytica I Laboratory
2538095
I Group No-
I Hercutes,
BLANK
Batch: 96'1845708003
N.D.
Batch: 961845708003
N.D.
Batch: 961845708003
N.D.
Batch: 961845708003
N.D.
Batch:961845708003
N.D.
Batch:961845708003
N.D.
Batch:961845708003
N.0.
Batch: 961845708003
N.D.
Eatch: 961845708C057.2 J rW/kS
Batch: 90'1845708C03
N.D.
Batch: 961845708003
l,l.D.
Batch: 961845708003
N.D.
Batch:961845708003
[-D-
Batch:9618457080030.80 J mglkg
Batch:96'1845708003
N.D.
Batch:961845708003
N.D.
Eatch:961845711002
N.D.
Eatch : 961840316820001A
522739
lncorporated - DE
l:fir?
Samp I e
UN]TS
mg/kg
mg/kg
mg/kg
ms/kg
mglkg
mg/ks
mg/ kg
mg/kg
m9/ks
mg/kg
mg/kg
mg/ks
mg/kg
ms/ks
(1) 93
21 2A?7
(1) 92
9 105
0 (1) 96
0 (1) 93
0 (1) 123
0 (1) 119
13 U.52
0 (1) 96
11 ',l 16
0 (1) 97
(1) 102
0 (1) 108
0 (1) 91
o (t) 92
0 (1) 92
I
89
1645 (2)
95
97
91
BB
131
109
2139 (?)
90
109
91
97
98
92
94
92
LIMITS
HIGH
50 150
50 165
?1 299
70 131
?3 177
?6 174
54 141
,7 145
61 142
53 142
69 135
55 146
50 147
54 149
49 149
52 149
?6 157
100 10]
DUP IIS LCS LCS LCS
RPD MS I'ISD RPO LCS DUP RPD LOU
0.46
l,:iI;
0.40
i5 Arsenic
I'"iti:,.
i9 lrlercury
TR
TR
6
9
2
5
7
1
6
4
7
5
6
7
6
0
1
0
96
79
79
100
9B
99
102
102
89
94
94
96
9B
92
93
87
100l'"i:il:"
I
I
t
mg/kg
mg/kg
mg/kg
% by rJt.'100
lil: ;:]l:,m:::,ii both determinations pas tess than five tinres the 100.
Has more than four times the spike added.
Lancaster Laboratofles
2425 New Holland Prke
PO Box 12425
Lancaste( PA 17 605-2425r., -_rr a(r 1401
I MEMBEFt,Kriil d3
QUALITY CONTROL REPORT
<-^ ..,...<^ ..n^ i^. ^,^lrn:r,.n ni .r,m!rnl< ;rrr' .rhn16./,rr,^^<))16 Pc'i lO/lfr'q(
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fri' i646
1647
fr1
1654
ll:i
r 666
1672
Tie
0111
T
I
t"tt-4 Grab soit Sampte
HercuIes: Bacchus PondsL4-- SOG#: HBP02-14
ll: ANALYSTS NAHE
1 COPY
1 COPY
Account No:06716
Hercutes, lncorporated - DE
Envi ronmenraI Affa i rs
Uitmington DE ,l9894
AS RECEIVED
ME T HOD
iiiliii:::liii:iftEIlrrIs.,',.,',.,,, DETEcT I 0N L I I'l I T uN I rs
Page:
P.0.
Ret.
Respectf ut l-y Submitted
Rarnona V. Laynlan, Gcoup Leader
I CP I'lata I s/Leachates
DRY UEIGHT
.::.i:.::::i1:.::::ii:::::::::::::r:::::::.::::::::::i: : ttlETHoD..1.,|:..:.).j -, }|! | | i| j,,:,., |,, ! |.,, j I i !:!ij
i.:il.i:,:::iliiiiji;*Estjt.Isriii,,:,:i D E TECT I 0l{ L I ll I T
14.
8.8
?.2
2.2
0.orJ
0.13
0.46
0. 49
3.3
2.4
o.12
0.1r5
o.44
0. 39
0.25
0.18
0.o29
(l)La ncaster Laboratories
A Thermo Analytical Laboratory
LLr sample No. ES 2538093Cottected: 6/?6/96 at l3:30 by BR
Sutrnitted: 6/?8/96 Reported: 8/ 7/96Discard: 9/ 7/96
Thattitrn
A Iumi num
Ant i mony
Bar i um
Beryt t i un
Cadmi un
Ch rom i urn
Copper
I ron
Lead
Manganese
Nicket
Si Iver
Tinc
Arsenic TR
Setenium TR
Irlercury
I'loisture
"l'loisture[ represents the Ioss
105 - 105 deqrees Cetsius.
'.rr:::..i:iji:i.:ii:::t:v.ir :rr:
: !|li!|i. i!r".!!" l|ir a. ^.. i.a .' | : : :
::i:il-.:rliirl:i.:lrinr..lo r. . : I.:::.::.r":.:.:t:::r:.:-:.:.:l::::.:.:v; r 9 " _' J
i n r.rei ght of the sampt e
8.6 mg/kg2.1 mg/kg2.1 mg/ks0.070 ms/ks
0.1 2 mg/ks0.45 ns/Kg0.48 ms/kg3.2 ms/kg2.3 ms/kS
0. 11 rns/kg0.44 ns/kg0.43 ng/kg0-38 ng/\g0.U+ mg/kg0.17 mg/kg0.028 mg./kg0.C6 % by ut.
after oven drying at
TO
TO
t
I
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Hercutes, I ncorpotated
ERH - Rocky Mountain
Questions? Contact your Ctient
Rachet L. Kreamer
03:!r?:43 D 0002 ?1 REP
310 25.00 00010400 ASR000
ATTN: Mr. Joseph KeIter
ATTN: l'1r. Brent Robi nson
Services Repaesentativeat (7'^,7) 650-2300
126L36 5227i9
Lanca5ter Laooratofies
2425 Ne.r Holland Prke
PO Box '12.125
Lan(aster PA 17605-2425
7 11 -656-230A Fax [phone]
ii:i,.iii:lii ilr'; D'.
j,1
79:)>o
li;;;;,7
tif:ilo.i.,
,::,:,lt?L'l'?
MEMBER
See reverse slde for explan;!'c. oi !,'TaoiS.lnC dilo'e'.'ralrons
tt-
2ti5 Re, t.l.,lc/9: ?tP
LABORATORY CHRONICLE(I)La ncaster Laborato ries
TJETTIOO
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
srJ-846 3050A
su-846 60"t0A
su-846 6010A
sv-u6 7471A
su-846 7471A Modified
EPA 160.3 (modified)
ANALYS I S
TRIAL OATE AND TII4E
1 07/13/95 18481 07/13/96 18481 07/13/96 18/+81 07/13/96 1B4B1 07/13/96 1B4B1 07/13/96 18481 07/13/96 18481 07/13/96 1B4B1 07/13/96 18481 07/13/96 18481 07/13/96 1B4B1 07/13/96 18481 07/13/96 rB4B1 07/13/96 18481 07/0?/96 19341 07/13/96 18/-81 07/17/96 0958
1 07/03/96 16471 07/0?/96 1506
1 07/02/96 1520
Page:
ANATYST
Jotene M. Schields
Jotene I'1. Schietds
Jotene lll- Schields
Jotene M. Schietds
Jotene tl. Schields
Jotene M. Schi el.ds
Jotene M. Schiel.ds
Jotene ltl. Schietds
JoIene I'l. SchieLds
Jotene lil. Schiel.ds
Jotene M. SchieLds
Jotene M. SchieLds
Jotene M. SchieIcis
Jotene M- SchieLds
Desi R. Carozza
Jotene I'l- Schiel.ds
Nina C. Halter
Netti S. Harkaryan
Frances A. Demorest
Neetay B. I'lehta
?of I
I
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I
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I
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I
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I
A Thermo Analytica I Laboratory
LLI sample No. ES 2538093
Co(tected: 06/?6/96 at 15:30 by 8R
subni rted: 06/28/96
soit-4 Grab Soit Sampte
Hercutes: Eacchus PondSL4-- SDG#: HBP02-14
CAT
llo
16?5
1643
1644
1646
1647
1649
165 1
1 653
165t,
1 655
1 658
1661
1666
1672
5708
6935
6936
01 59
5711
011'l
ANALYSIS NAME
Thal, t ium
A I umi num
Ant imony
8ar i um
Beryt t i um
Cadmi urn
Ch romi um
Copper
I ron
Lead
l.langanese
N i cket
S i Iver
Z inc
SU SU846 ICP DigestArsenic TR
Setenium TR
I'lercury
SU SUB/i6 H9 Digest
I'loi sture
MEMBEFlrrcm
Lancaster Laboratofles
2425 New Hoiland Pike
PO 8ox 12425
Lancister, PA 17 505 -2 425
7 17 -656-2300 F ax. 7 17 -656'2681
I
iT
Account llo: 06716
Hercutes, lncorporated - DE
Environmental Affairs
Uilmington 0E 19894
5ee reverse srde fcr explanatron of s.vmbols ano 6bbr-oYratrons 2216 Re,r 10/10/95
J"
I
I
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) The resutt for one or
!rne
Uactsround resutt
3of
DUP MS LCS LCS LCS
RPO MS MSD RPD LCS DUP RPD LOU
(1) 93
?1 ?027
(1) 92
9 105
0 (1) 96
0 (1) 93
0 (1) 128
0 (1) 1',19
13 2452
0 (1) 96
11 116
0 ('1 ) 97
(1) 102
0 ('l ) ]08
0 (1) 91
0 (1) 92
0 (1) 92
B
five times the 100.
added.
B9
16/+5 (2)
95
97
9'1
8B
131
109
2139 (2)
90
109
91
97
98
9?
94
92
100
t
MEMBEFlriE'iilT
Lancaster Laboratones
2425 New Holland Pike
PO Box 12425
Lancastel PA 1 t- 605'2425
717-656-2100 Fax [phone]
QUALITY CONTROL REPORT
(I)La n caste r l*abo rato ries
A Thermo Analytical Laboratory
LLI sample No. 2538093I ::::.:"::.'.::::.:'::
I
Sampte Sampte
1,,:::,,_ u',rTs
13. mg/kg
It,il :il,
i6 Bariurn
l'"iii** ::;::
rl Cadmi rrn
0 -12 mq/kq
I chromium
I _ o.ts mg./kg, uopper0-48 mg/ks
l:":i mg/kg
?.3 mg/ks
II'iili-" :;::
i6 Sil.ver
l.'Hi :il:ri Arsenic TRO-24 mo/kqI s"t".irm TR
! o. rz ms/ks, 14etcuny0-028 mg/kg
I '"i:II,." Y. by ur.
BLA}JK
Batch: 9618/.5708003
N.D.
Batch:951845708003
}I.0.
Batch: 961845708003
N.0.
Batch:961845708003
N.D.
Batch: 961845708003
H.D.
Batch: 961845708003
N.D.
Batch:961845708003
N.D,
Batch:961845708C03
N.D.
Batch:961845708003
7 -? J mg,rkg
Eatch; 96'1845708005
N.D.
Batch:961845708003
N.D.
Batch: 961845708003
N.D.
Batch: 961845708003
N.D.
Batch: 961845708005
0 .80 J rnglkg
Eatch:96'1845708003
N .D.
Batch: 961845708001
N.D.
Batch:95184571100?
N.D.
Batch: 961840316820003A
both determinations xas Iess than
Has more than four times the spike
Group No. 52?739
Heccutes, Incorporated - DE
6
9
2
7
5
7
I
6
4
7
5
6
7
0
1
0
96
79
79
100
98
99
102
102
89
94
94
96
98
92
93
87
79
100
Page:
L II'IITS
HIGH
50 150
50 '165
21 ?99
70 131
23 177
26 174
54 141
57 145
61 142
55 142
69 135
55 146
50 1t7
54 149
49 149
52 149
?6 157
1 00 '101
22r5 Rev to/io/s5 d'}5ee re'/erse sroe ior explanatron of 5vmocls.;nc abbrevtatrons
I
t
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;
;
;
I
t
;
;
;
t
T
T
T
t
I
t
I
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T
1722
li,iii
1747
t:ii\1754
1755
litiii
1772
IH;
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Account No:067'!6
HercuIes, Incorporatecl - DE
EnvironmenraL Affairs
tJrtmrngton 0E 19894
AS RECEIVED
MFTHOD
iiii,SE;ql1gl5':'ir:.,., DE T ECI l :rl L t r'l I T ultl TS
Page:
P.0.
Ret.
Respectfu[ [y Subrni tted
Ranrona V. Layroan. Croup LeaCer
ICP Metats/Leachates
1of
2538099
by BR
B/ 7/96
I Soil. Eq Rinse Grab Uater Sampte
t Hercutes: Bacchus Pond
SOLER SDG#: HBP02-20EBr
I IlI ANALYSIS NAME
Tha[ [ ium
A I Lrni num
Ant i mony
Bar i um
Eeryl I i un
Cadmi um
Chromi um
Copper
I ron
Lead
i{anganese
NickeI
Si tver
ZincArsenic TR
Setenium IR
Mercury
.1B;i',:ir 170.
;;51.,'.,1;,1,': 57 ..i'1.. t()):^,,-u.:.: r.J
.,v, a. t
rlt:r':r' 4 '3--?o
'2, ).t)so
-) . to.
^ ,OtP t;Dr 5.44,,:',) 3.6,,',.,1 12.
r. 1a
.n ) 7
CSg , J 0.01+3
uS./ t
usl I
ug/ ''
u9/ [
uS./ t
,ig/'t
ug/ t
ug/ L
ug/ t
u9/ |
ug/ l.
ugl L
ug/ L
u9/ L
u9/ t
u9/ [
'rg/ I
i'{r. Joseph
,!1r- Er.rnt
1 COPY TO
I
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MEMBEFlKir
Hercutes, Incorporated
ERH - Rocky f'lounta in
Questions? Contact your Ctient
RacheI L. Kreanrer
03:48:46 D 0002 23 REP
l'10 '15.00 00027200 ASR000
Servi ces Representativeat (717) 656-2i00
12(,436 52?159
ATTN:
ATTN:
Ke[ [en
Robi nson
Lancaster Laboratones
2425 New Holland Pike
PO 8ox 12425
Lancaster PA 17 605 -2425
717-656-2300 Fax: [phone]
(I)La ncaste r Laboratories
A Thermo Analytical Laboratory
LLI Sample No. EL
Cottected: 6/?6/96 at 13:30
Subtli tted: 6/?8/96 Reported:Discard: 9/ 7/96
5ee rererse srde for erplanalron o{ symools and dbbrevlatlons 2216 Rev 1ot3o/es d}
LLr sample No. EL 2538099
CotIected: A6/26/96 at 13:30 by BR
Sutxni tted: 06/?8/96
soi t Eq Rinse Grab tJater Sampte
Hercutes: Bacchus Pond
soLER SDG#: HBP02-20E8*
I Account No: C6716 I
i Hercutes, Incorporated - DE II Envi ronmentai Affa i rs ii uitminston DE 19894 |
I,ABORATORY CI{RONICLE
Page: ? ol
ANALYST
Donna R. Sackett
Donna R. Sackett
Donna R. Sackett
oonna R. Sackett
Donna R. Sackett
Donna R- Sackert
Donna R. Sackett
Donna R. Sackett
Donna R. Sackett
Donna R- Sackett
Donna R, sackett
Donna R. Sackett
Donna R. Sackett
Donna R. Sackett
Chr-istine H. Contin
Donna R. Sackett
Donna R- Sackett
Netti S. Markaryantle[[r S. l'larkanyan
La ncaster Laborator"ies
A Thermo Analytical Laboratory I.l
I
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CAT
NO I!ET HOD
su-346 6010A
su-846.5010A
su-846 6010A
su-846 6010A
su-846 6C10A
su-846 6010A
su-846 6010A
SU-8/i6 6010A
su-316 60'10A
su-846 6C10A
su-846 6010A
su-846 6010A
su-846 6C10A
su-846 6010A
su-846 i005A
sU-84o 6010A
su-846 6310A
su-846 7470A
Su-gt 6 7q70A
Lancaster Laboratofles
2425 New Holland Pike
PO Box 12425
Lancastec PA 17 605-2425
7 17 -656-2300 F ax. 7 17 -655'268 1
ANALYS I S
DATE AND TIIIE
07/15/96 01ZC
07/15/96 AtZD
07/15/96 A4Zo
07/15/96 9420
07/15/9b C|?C
07/i5/96 C/.?0
07/15/96 04?0
07/15/96 04?A
07/15/96 01t?D
07/15/9$ Ct ?C
07/15/96 04?D
07/15/96 0/+20
07/15/95 04?0
07/1r/96 0420
07/14/96 12?8
07/15/96'0424
07/15/96 04?0
07/04/96 1353
07/03/96 ?213
1722
1743
1741
1746
1747
^,719
1751
1753
1754
1755
1 758
1761
1766
1772
1 848
7035
7036
AHALYS I S NAI.IE
Thattium
A I umi num
Ant i mony
Bar i um
BeryItium
Cadmi un
Ch romi um
Copper
I ron
L ead
I'tanganese
N i ckeI
Si tver
Zinc
UU SU8/i6 fCP Digest (tot rec)
Arseni c TR
Setenium TR
Hercury
UU SIJB46 Hg oigest
TRI AL
1
1
1
1
1
1
,1
1
i
1
i
1
1
1
1
1
,l
1
1
0?59
5713
Txtir
I
dlSee reverse srde for explanation of symbols and abbrevtatrons 2216 Rev.10l3O/95
ri"
I
I
La ncaster Laborato ries
A Thermo Analytical Laboratory
LLr sample No. 2538099
I ::::.::.:'^;;:: ::::"'*'"
BLANK
Batch:961921848002
N.D.
Eatch:9619218/*8002
N.D.
Eatch:951921848002
N.D.
Eatch:96'19218/+8002
N.D.
Barch:961921848002
0.0015 J mg/L
Batch:96192i848002
N.D.
Batch:951921848C02
li. D.
Batch:96192'1848002
N.0.
Batch:961921848002
0.0607 J mglL
Batch:961921e/+8002
N.D.
Batch:96'1921848002
N -D.
Batch:96i921848002
N.D.
Batch:96'1921848002
N.D.
Batch:96192'!848002
N.D.
Batch:95'1921848002
N.D.
Batch:961921848002
N.D.
Batch: 96185571300i
0.C00067J mg/ L
QUALITY CONTROL REPORT
(iI)Pag e:3of
Group No. 52229
HercuLes, lncorporated - DE
I
Sampt e
l,;,,,..
Sampt e
UNITS
u9/ t
u9/ |
u9/ t
ug./ t
u9/ |
us/ t
us/ t
ug/ t
us/ t
u9/ |
ug/ t
us,/ t
ug/ |
us/ t
u9,/ L
us/ t
us/ t
LlMITS
H I6H
LCS LCS LCSLCS DU!, RPD LOU
It!S
I'ISD RPD
D!.IP
RPD MS
i A[uminum
I ii:*',i Barium
l'"iii,,,.r Cadmium
2.7
r::i:"*
3.8
t;i
I l.langanese
I'i:i'
r Si Iver
(1) 101 't 03
174 -772 -7?9
(1) 1C5 106
0 (1) 87 88
(1) 97 97
(1) 9/+ 95
0 ('1 ) 78 79
0 (1) -?0'l -191
17/. '4,513 -14/.1
0 (1) 92 9i
0 (1) 59 61
0 (l) 9t+ 95
(1 ) 99 101
0 (1) -t,1 -34
0 (1 ) 101 102
0 (1) 101 102
0 (1) e5 90
(2)
1
24
1
1
0
1
2
9
34
1
3
1
1
q
1
1
6
102
108
107
10c
9B
97
107
101
111
102
103
104
100
103
103
101
95
80 120
80 1?0
B0 120
B0 12A
B0 120
B0 120
80 1?0
B0 120
80 120
80 120
B0 120
80 120
B0 120
80 , 1?0
B0 1?0
B0 120
B0 120
(2)
l^i,:^,.,-
2.7
l;:i:il'.
0.043
I
I
I
I
The resutt for one or
Je
Uactsround resutt
MEMElEFI7XmI
both determinations eas Iess than five times the LOo.
lras more than four tinres the spike adcled.
Lancaster Laboratories
2425 New Holland Pike
PO Box 12425
Lancaste( PA 17 605-2425
7 17 -656-2300 f ax. 7 17 -656-2681 d',See reverse srde for explanatron of symbols and abbrevratrons 22]6 Rev.10/30/95
T
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.ilo.
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I
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(I)Lancaster Laboratories
A Thermo Analytical Laboratory
Page:
P .0.
ReL.
nespectfuL Ly Submi tted
R;il!)co.r y. Llylrl.in, tl:orip Leader
LC2 i':eta ! s./l.eachat.:;
LLI sample No. FL 2531999CoLI.ected: 6/20/96 ar 12:05 by BR
subri tred: 6/28/96 Reponted: 8/ 1/96
0 i scarri: 8/ 9/96
CU-1 JUD Unspiked crab Uarer Sarnpl.e
HercuIes: Bacchus Pond
CUJUI SDG#: il6P01 -C3BKG
AIIALYS I S IIAME
ICL Votari tes by 3240 - !,are.
Tnal. I iunr
A Lunri nunr
An t i rrony
Bar iurn
Eeryr. I irnr
CaCnri um
Ch r onri unr
aoopcr
t ron
l- e:d
i,l a ng 3nei e
NickeI
gr lver
Tinc
/rrseni c TR
Seieniunt lR
!lc t c urY
TC! Pes(icides in Uaters
ICL SU846 Senivotati Les/Uaters
T!L S;346 SemlvoLati ies/};atecs
iAccounr ilo: 467':6
i itercuLes, ln.c.oorated - DE
. Errvi roftrlenra L Afia ! rs
.Ji lrfington OE j9{J94
A9 RECEIVED
l'rE T H00
OETE!Tl 9r- !-IMIT Ulll rS
459?
172?
1713
l/r5
)719
r/))
1 i58
lrCi
',756
^,77?
7b!5
7:30
czt9
t,678
1579
1 CCPY TO Hercur-es, lncorporatcd
1 CCPY T0 E?Y Roc(y l{o!:jta:n
7mm
Rachel. r-. Kr.-.:i:rer' art
0-1:?L:'J5 D Ct-)Z '15 sfn
i 10 I5 . 00 ,t! 1 ?6/1-i0 AsRCi!'
Lancaster Laboratofles
2425 New Holland Prke
PO Box l2rl25
Lancasler. PA 17 605-2425
7l7-656-2300 Fax 7tl-656 2o3l Seereversesrdeforexplanalronoi5ymboliandabbre,/ratrons 2216
t'^
n",, rOZ:OroS LJ
LLI Sarnp1e No. EL ?531999
Cotf.ected: 6/26/9o ar 12:05 by BR
suuritted: 6/28/96 Reported: 8/ 1/96giscard: Bl 9/96
r\ccount llo: 1671 6
l.lercutes, I ncf, rporated
Envi ronnrcntai. r1f f a i rs
Ui tmington DE ':9894
Page:
on
ReL.
RespectfuL ly Subrni tted
l,1i cire're i.!cCi.aIin, B.A.
6roup Leader, 6alHS Votati Ies
Lancaster Laboratories
A Thermo Analytical Laboratory 1l
ll
ll
il
ll
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xl
jl
:l
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9E
.i.:...it.i.,iiiji-jlESU!T S
Zof 14
CU-1 JUD Unspiked Grab !,ater Sampl"e
HercuIes: Bacchus Pond
CUJU0 SDG#: !19P01 -LilAKG
CATNO. AIIALYSIS NAME
TcL votatiles by 8240 ' lJater
1 258 Ch I orornethane1257 Brotnomethane3iqZ Vinyt Chtoride
3191 Chtoroethane3497 llethytene ChtoriCe3i9s Acelonei!,99 Carbon Disutfide3500 l,l'0ichtoroethene3501 1.1-DichLoroethane
i505 Chtoroform
i504'1,2-9ichLoroethane0316 2'Butanone3505 1,1,1-Tcichtoroethane1506 Carbon TetrachLoriCe3507 VinyI Acetate
i508 Eromodich(ot'ontethane1509 1,2-DichtoroProPane
3516 cis-1,3-DichtoroProPene
351 1 Trichtoroethenei5"i? DibroalochLoromethanei5'll 1,1,2-Trichtoroethane3515 Eenzene35i0 trans'1,3-DichloroPropene3513 Brornoform3521 4-l'lethyt-2-pentanone1920 2-Hexanonei522 Tet.achloroethenei523 1,1,2,2'ler.rachIoroethane352L Totuane
3525 ch Iorobenzenei525 Ethytbenzene3528 Styrene35?9 xytene (total)
,780 trans - 1,2-D i ch Ioroethene5363 cis'1,2-0ichIoroeti]eno
RECE I VEO,, l'!E'ia\9
,r : DETECIILTT Lll'(lI Ull!TS
jl
I
',1
ouest i ons? Contact
RacheL L. Kreanlef
your CI ient Servjces Representa!l'/e
ar (7";7) 656-2i00 I
,l
I
rxm
Lanca5ter Laboratones
2425 New Holland Prke
PO Box 12425
Ldrrcaster. PA 17 605-2 125
717-656'2300 Fax 717'656-2681 2216 Rev ,rr.rn, t 'if
See reverse srde ior exp{anatron of symbols and abbrevidtronS
I
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(iI)Lancaster Laboratories
A Thermo Analytica I Laboratory
Page:
P.0.
ReL.
Respectfu[ [y Submi tted
..ieniIe. E- Hess, B.S.
Grouo !eader Pesticides/PCBs
lof 14
2216 Rev ,O"rr* d?
LLI sample No. FL 2537999CotIected: 6/26/96 at 12:C5 by BR , A..ount llo: 05716
I li!'rcut es, : ncGrporated
I anvi ron:llenta. Af f a irs
] ;i Lrington DE 19u94
AS IECE I VED
,lZCl'-1! , DETECI:CrM1.,!lT ull IIS
DE
Srrbflritted: 6/23/96 Reported: 3/ 1/960iscard: 3/ 9/96
CU-1 Juo Unspiked Grab Uater Sampte
Hercules: Eacchus Pond
CIJJUD SDG#: llBPO'l -0i0(G
CATNO. AIIALYSIS }IAME
ICL Pesticides in Uaters
1600 Alpha BHC1601 geta BHc1603 oet ta BHC'1602 Gaoma 8HC - Lindane16C4 Heptachtor1605 ALdrin16C6 HeptachIor Epoxide1616 Endosulfan l'1o10 0ieldrin1607 DDE
loi I Lnorrn1615 Endosut{an t I1508 D0016i7 Endosut fan SuI fate1609 DDT0933 Endrin Ketone1860 I'lethoxychlo.'1361 Atpha Chtordane136? Garmra Ch Lordane
\613 Toxaphene'1613 Endrin Atdehyde1619 PCB - 10',161620 t,t:B - 12211621 PC3-12321622 PcB-12c216?3 PCB-r248162t PCB-125416?6 PrS-i260
il.r,.
lr.!,.
r{,:,.
ii.-..it.:.
u.'- ,
!t.!.
1!,-'.
:1.r,
il,!).
u.D-
N-l.
h,. :',
i{. :' .
ri. t;
ti.-r -
0.acz '-:s/ t
fa tarll ,,^ J ,uJi 'il 'r,ta ,..r / Ir!/ '
!-r . C:2 \r9/ '.
ll 11q t6t'
C. ir3c ,-rs/ i
r: rrr-.f . xr / '
r\ a1? t r.l:
,1. il! ue/ i
s.JLr JUl l
'-r . !35 u9/ ,.
i: nl !:.r/l
r'r .007 tc:/ ',
| .Ci)T ug/ [
D. !03 u9/ t
C.lil u9/ i.
rl .01 uq/ l.0.f05 u9/l
0. !Lr5 u9/ L
us/ i0.0i0 u9,/'.
C - !9 ug/|,
,l .2 u9/ L
Ll . rl9 ug/ t.
i-'.','5 !g/ i.
i 17 t6/
:r aA -.\/'
n '7 t'a/l
Due to insufficient samote size, we Here unab'.1'rio regorr our:sual
quantitation Limits. The values repocted reper-sr'nt la.'.oHes: quantirarion
Iirnirs obtainabLe-
Questions? Ccntacr your
RachrrL L. Krei,ner
CI iL.n: Ser\ ]ces Representa!!ve
at ( i'l) 5io-zil!
7Km
Lanca5ter Laboratofies
2425 New Holland Prke
PO Bor 12425
Lancast€r. PA l1 605 -2425
717-656-2100 Fax 717'65o'2631 5€e reverse 5roe lor e:pianatror ol s/mbol5 and abbrevlatlons
(I)Lancaster Laboratories
A The rmo Analytica I La boratory
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! Account No: 16716
ile.crles, lncorporatec ' 0E
Envi ronrncnra: Afta i fS
i Ui Imington 1E ']9tr94
AS RECEIVE9
METIIOO
DETECT! 3I{ L II'!!I UIII IS
q o? t4Page:
LtI Sampf e No. EL 2531>a99
Co[ [ectu.d: 6/26/96 at 12:05 by 8ll
gubflitted: 6/?8/96 Reported: S/ 1/95Oiscard: Bl 9/96
CU-1 JUD Unspiked Grab Uater Sampl.e
Hercutes: Eacchus Pund
CUJUo soG#: tlBPo l -0lBr(c
CATMO. AIIALYSI S llAl'lE
TCL SUB46 SemivoIari Ies,/Uaters
39'l 3 pheno L3867 bis (2-chloroethyt) ether
3!J74 2-ch IorophenoLi.183 1,3-dichiorobenzenel8g4 i,4-dichtorobenzene.3882 1,?-dichtorobenzerre46C0 2-methylphenoI/.631 2,2,oxybis ( l-chtoropropane)!,i2? 4-rnethyLphenotZ)15 N-nitrosodi'n-propytaminej.102 her{ach I oroethane1110 ni trobenzene
-',')04 isophorone1ti1.i 2-nitrophenoL3lri0 :,4-dinierhylphenol
3i16.6 bis (2-r:hlcroethoxy) fllethane3ita' 2,q-dichLorophenol,3931'1,2,4-trichlorobenzene3106 naphtha t eneir:il 4-ch(oroani lineitD0 hi:x;ich I orob'Jaad i ene
3!1,7? 4-chLoro-J-rrethyLphenoLarC5 2-methyLnaphthal.eneli01 hexachtorocyctopenradie'nei)23 2,4,5-tr-ichi.orophenol922 2,4,5-trichlorolllranDl.ii;tj 7-chloror,apirth;lene3t,07 ?--nitroani l.;ne
lg?1 climethy(Dh!hatete
-1[:8 acenophthylene
on
Rel.
ouestions? Contact yc:r CL ierrtlli,chl'.'-. Kr',::::r:r'
9erv i ces Rep|eseara ! i ve
a: (7"7) 65o'2:")')
iiHfi
Lancaster Laboratofles
2425 New Holland Prke
PO Box 12,J25
LJncasrel PA 11 605-2425
717-656-2100 tax 717"656-2581
Respe:t+uL !-y Submi tredCrristine lu!- itatc'-lii,C-cup:e:d:rr, GCll'15
5ee reverse srde for exFrlanatron oi symbol5 anci abbrevratrons {,1
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B.S
2216 Re! 10,'10195
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(I)La ncaster Laboratories Page: 5 o{ 14
A Thermo Analytical Laboratory
LLr sample No. EL 2531999cottecred: 6/26/96 at 12:05 by BR
Subflritted: 6/?3/96 Reported: A/ 1/96Discard: B/ S/96
CU-1 JUD Unspiked Grab uater Sampl.e
Hercules: Bacchus Pond
CUJUD sDG#: HBP0l -C33(G
CATIIO. AIIAI.YSIS IIAI,IE
fCL sU846 Semi voLati Ies,/uaters
:
I A..orn. No: !5716
j xercuLes, lncrrporated - 9E
I Envi ronment.rr Af iai rs
I ,/r l.orington lE '9894
REC! ! VE9
MET HOD. DETEC-TI,]i,] I-IM!T UI,IIIS
iel..
l:::::::::: 1|i:Sili Fq
1908
3857
i3t3
391 2
3579
:i39!.
ls95
3r87
_<893
3909
rc83
351 4
i?.69
i399
l9'1.5
3859
lE30
ia97
l?1 9
1E7q
18.50
zn:a
3876
lJ96
'ii)')3
inal
J-nitroani I ine
acenaph thene
2,4-dini rrophenot
4-nitrophenol
C i benzofulan
2,4 -di ni trototuene
2,o-Cini trotoLuene
dierhyL phrhaLate
4-chLorophenyL phenyI ether
f I uorene
4-nitroanitine
4,6-di ni tro-Z -methyt phenot
ll -n i trosodi pheny l- arni ne
4-brornophen'/|. phenyt ether
hexach I orobcnzene
pentach L or-opheno I
pirenanth rene
anthracene
carbazote
di -n-butyt phthal-ate
f iuoranthene
pyfene
buryt benzyt phthaLate
3,3' -di chiorobenzidi ne
benzo (a) anthTacene
bis (2-ethyLhexyL) phthalate
c h rysene
Ci -n-octyt phthalate
benzo (b) fLuoranthene
benzo (tl) f luora,nl:rene
bcnzo (a) pv.ene
indL'no (1,2,3-cC) pyrene .dibenz (ar,ir) arthrrcene . ..berrzo (9hri perylane
0ue to insufficrent sampl.e, the quenti ratiJn
sernivoL.iri te conrpouncls wcre rais.-C-
0uest i ons? Contact youc
lach.,l L. xrr:r!r.r
Selvi ces ReDresenlative
ar (j',/ ro16-Zlr.rD
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Lan(aster Laboratofies
2.125 New Holland Ptke
PO Box 12425
Lancaste( PA 17 605-2425
717-656-2100 Fax 717-65b'258 I
Respec:fu!. ty Subilr tted
Christine !l- RalcLif{,
6 i oup LeaCer, GCll'l:i
See reverse srde for explanatron of symbols and abbre'/ratrons d?Rev l0/lO/95
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(I)Lancaste r Laboratories T
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IABOS'}TORY CI{RONI CT E
Paqe: 6 of 1t
ANA'_YS'r
Susan A. l,!cilahon
Donna R. Sackett
0onna R. Sackerr
Donna R. Sacke:r
Donna R. SackL.tt
Don.a R. Sackett
Donna !i. Sackett
Conna R. Sackerr
!onna i. Sackort
Donno l. Sackert
Donna R. Sackett
Conne !?. Sacketr
0onna R. Sacke!t
oonna R. Sackett
Dooia R. SackettChristine tt. Contin
Donna R. Sackett
Donna R. Sackett
NeLLi S. !,larkaryanNelll S. Farkaryan
Hercie A. Natale
Dougias D. Seitz
lilacia A. Cavenport
Srepiranie I'1. Shenk
Sre2hanie H. Shenk
LLI Sampre No.
CoI tecred: A6/26/96 ar
Subori tted: 06/28/96
A Thermo Analytical Laboratory
EL 2531999
13:C5 by 8R , Account lio: 06716
, nelcutes, inco:90rrted
, Envirororcnt.l'- Af 'a ias,UiLmington .35 1r;394
CU-'l JUD Unspiked Grab Uater Sanlpte
Hercutes: Bacchus Pond
CIJUD SDG#: i1BP01 -03BriG
cAIIIO A}JALYSIS NAME
!.59? TCL Votari Les by 8240 uater
17?Z ThatLiern17\3 Aluminunt17!,4 Ant iflony
17t,6 Bar i urt
17/.7 BerytLiunr17t9 Cadrniunr
1751 Chrorniunr
',753 Copper175t, I ron
''755 Lead
1 753 llanganese17o'l N icke L1766 Silver177? Zinc
1848 llu SU846 ICP Disest (tot rec)
7C35 Arsenic IR
lUiC, SetenlLlll :l(
0259 ltercury
5713 UU 5!846 H9 Digest
0817 Uater SampLe Pest. Extraction
0937 TC: Pest'icides in lJaters
0B1l BNA lJater Extraction467A TC'- S18(6 Scmivol.ati tes/L!aters4679 TCL SUBlr6 SerrlvoLati Les/tJaters
llET!.t00
stJ-846 B?108
su-346 6il10A
su- 316 6,l lCA
su-846 60'10A
s'J-846 63-10t
Srr - 846 6C 1 rlA
SH-346 6il'10A
su-346 6-r10,1.
su-346 6li0A
SIJ-34o 6.''10A
sr - 846 6.11 0A
SrJ - 846 6il i LrA
SU- 346 6010i\
s,i-946 6C10A
slJ - 846 6,1i DA
sH-846 1005r,
s'r-346 6:110A
su- t46 6a't 0A
su-846 7470A
s,J-846 7i7'-'A
su-846 351C8
)H-DqO OJO,
st-846 i5 l0B
sl.'- 346 {i27C3
SU-52,6 327C,i
ANA'.Y S I SIRIAL DATE ANO TIME
1 07/01/96 A238
1 07/15/96 C256', 07;"t5/96,]2-\6'. 07/'5/e6 C?r6, 07/15/q6 A2S|-^ c7/15/9o C256', 07/15/96 A2551 07/15/55 C?56' a7 /1:' /96 a?-qb1 A7/',5/9o CTta': 07i',5/c6 0255'' q7/1'5i96 t2561 07/1i/96 C2-\51 A7/^t5/96 C25b', 07/15/96 f;?i61 07 / 1.0 / 96 12'??'. 07 / 1.5 /96 A?561 07/15/96 ti56
2 07/17/96 16123 C7/'^,6/96 21tr3
") 07/41/96 13301 97/15/96 0732
1. C7/C?./95 C93C'' t7/li/Ca' f;o061 C7/03/96 A6t,6
TeEiiI
Lancaster Laboratofles
2.125 New Holland Prke
PO 8ox 12425
Lancastel PA 11 605-2425
7 17-656-2300 t ax. 1 17 -656'2681 2216 Rev ,Orr.r* J-!
I
5ee re,/erse srde for erpianatlon ol symbols and abbrevratrons
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(I)Lancaste r Laboratories
A Thermo Analytical Laboratory
Sarrrp I e
!,t9 L
Sampte
UT]I TS
1258 chtoronrethane3. u9/ t
1 257 Brornomethanel. u9/ i
1a92 vinyt Chtoricie
2. u9/ |
1t rl1 Ch toroeth6ne3' us/t3;97 rterhyLene ChIoride?' ug/t
14?Z Acsttne6' u'lt
3499 Carbon Disutfide3. u!/ t
35C0 '1,1 -D i chtoroethene1. uglt
1501 'l, 1 -0rchtoroethane
2. ug/ I
3501 Ch I oroforn1' uq'/[3i04 1,2-DichLoroethane2' u,/t
O116 2-Butanone3' ug/L3)05 '1 ,'l ,1-Trichtoroethane1. u-q/t
3'-C6 Carbon TetrochLoride
1 . ug/ L
11A7 Vinyt AcerateZ. ug/ [ii0ll Brornodi ch lDroflrethane1. us/Llt09 1 ,2 -9 t ch l ocuprop.rne
'I ' ug/ll;16 cis-1,3-0ichtoropropene
'1 . ug,' L
35'11 Trichl.ocoerhene
LLI sample No. 2531999
CU-'l JUD Unspiked Grab Uater SemoLe
Hercules: Bacchus Pond
,croup No. 52?7?7
I liercuLes, :nc!r:poratcd ' DE
73
9n
t7
1 ,r;r
75
11.tt
1Cl
11t
9o
'; t,5
'1 1,
99
97
1C6
ol
a)
146
91
B LANI(
DUP YS
iPO MS I'1S9 RPD
LCS LCS
LCS DUP RPD
LCS LI}ttlS
iOU HICH
!,592 ICL Votatites by 3210 - ',Jater Batch: t96'1341AA
t.
2.
N.D.
ti.9.
N.t.
N.D.
N.).
N.!.
N.:'.
N.5.
N.!.
l,l.!.
N.D.
N.t.
N-1.
ri.,.
o
B
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9
j
3C
7
)
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l+
ti1
a
1
?7
5
2
t
1
1. l,
t6
0
75't\ Benzene'l ' us/t
39'10 trans-'!,J-Dichloroplopene
1 . uC/ t
MEMBEFT
7X-m
Lancasler Laboratofles
2425 New Holland Prke
PO Box 12425
Lancaiter. PA 17 605- )42c)
717-656-2100 tax 7 11 -656-2681
QL';\IITY CONTROL REPORT
See'ererse srce ioI e\olanalro4 o';ir.bols a.d dbbreYratronq 2216 Rev ,Or,Or* d}
I
(iI)La n caste r Laboratories
DUP
3.P9 !,!S MS3
LCS LCS LCS LII{ITS
LCS DUP RPO LOU H I GH
3oi
B0 120
80 120
8D 120
B0 12C
B0 120
80 '1?C
80 120
80 -12 0
80 120
B0 120
80 120
80 120
30 1?0
SLANK
Lancdster Laboratories
2425 New Holland Prke
PO Box 12425
Lancaste( PA 11 605-2425
7 17-656-2300 F ax: 1 11 -656-268 1
Pa_oe:
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LLI sample No. 2531999
CU-1 JUD Unspikad Grab Uater Sanrpr.e
llercutes: Bacchus Pond
'Group No. 522727
I HercuIes, Incoapofated OE
S.rmpt e
HDL
sampI e
UlI I TS
MS
RPO
z4
36
4i
26
I
c
2
1
0
5
'l
Ut
1
,l
0
1
?
I
,1
J
1
1
102
108
107
100
98
97
107
101
1i1
102
1Cl
1C1
10c
35'18 Bronrof orm1. us/t N.!. 71 90
3't?1 4-tlethyt -2'pentanonc-
5. u9/ t N.D. 65 9l
3520 2-Hexanone7. uq/L rl.9. 62 95
35?2 Ietrachtoroethene1. ug/t li.D. :05 105
i,?3 1, l, 2,2-Ietlachr-oror'thalte2. u9/\ r,l .!. 72 at
"2q rotuene2. ug/t N.!. 1i'! 1C5
i25 chtorobenzene1. ug/t N.f. ]Cl 101
J;25 Ethytbenzerie?.. u9/t r,r.!. 1!0 1!e
528 Styrene1. us/t N.1. 10? 102
;529 Xytene (totat)
'l . ug/t il.D. 10g 1Cgj780 trans-1,2-DichIoroethene2. ug,/L N.D. ,104 99
6268 ci s-1,2-Dichl.oroethene2. us/ | N -0. 1C6 1 02
l72Z Thattiurn Batcn:961921848102'170. ug./t N.g. (1) 1C' !03
174J Alunrinum Batch: 90192184810257. us/t ri-D. 174 -772 -729 (2)
171.4 Antimcny Batch: t6',192184B00215. us/t N.D. (1) 1C5 -'06
1740 Bar.iunr Batch: 961921843002Z.? uglt N.g- 0 (i) 87 83
1717 Beryt I iun Batch: 96i92134S;1021.3 uslt 0.00i6 J mgrl (') 97 97
1749 Csdrniuu 8.rtch:9b'192i341!022.7 ug,/t N.!. (1) g!. 95
1751 Chromi um Batch: 961921843i021.3 us.i t N.D. 0 (-1 ) 78 7c)
175i Coppcr Bal:ch:96'19218113C021.3 us/L N.!. 0 (1) '2C', -1Ci
1751, Iron 8;'tc!r:96i92181,3?325.9 uglt 0.0607 J mgll 174 '13',7'1111 (2)
1755 Lead Batch:9o192'18'48i10213. ug/t N.l. 0 (i) 9? 9i
'1753 l.liinganese 9atch: 9619218r.BC02
?.9 us/[ ri.D. 0 (1) 59 61
1761 Nicke!. Barch:96i92181.3:025.4 ug/t Ii.D. c (i) 91 ?5
'176,5 Sitver Eatch: 96192]B431023.6 u-o/t N-D. (1) 99 101
(1) Ihe result for one or both determinations uas less th.rn five tirnes the LoQ.(2) The backgrorrnd resuLt w:rs more than four tirnes tir: spite added.
Tmiir
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QI-'ALTTY CONTROI- P.EIORT
See reverse srde ior erolanatron of svmbols and abbreviattons 2216 Rev 10/10/95
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A Thermo Analytical La bo ratory
Page: 9 of 14
LCS L Ii{ITS
LOU IiIGTi
30 120
80 120
B0 120
B0 120
LLI sampl-e No . 2531999
CU-l JUD Unspiked Gcab Uater SamplL'
HercuI es: Bacchus Pond
r]roup tlo. 5?2727
hercuLes, !ncoroorateC
i
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DEI
I
II
Samp L e Samp l. el'!ot t,ll I TS
1772 Zinc1?. u9/ t
70f5 Ar:en'ic TR?.7 ug/t
7035 Setenium TR7.7 ugl t
0259 14ercury
0.0CC40 ug/ I
O9!7 IC'. Pesttcides in \.Jaters
LCS LCS
LCS DUP RPD
ouP t'!s
RP' I.1S MSD RPD
0 (1) -41
0 (1) lc']
0 (1) 1Cl
0 (1) 79
- _44
102
LA2
79
5
1
1
c
10i
i0l
'i 03
'r 08
'1500 Atpha BHc0.0D2 ug/l
1501 Eera BrlC0.00t u-ol L'1603 9elta 8Hc
0. trr15 u9/ t
1602 Ganura 8HC - Lindane0.002 us/t
1601 Heptachlor0.0C5 us/t'1o05 Atdrin0.004 ul/l
1eD6 Heptachtor Epoxide0.003 u9/ t
16'16 End!)sut f an I0.003 u9/ t
1610 Diel-drin0.005 ug/t1607 DDE
0. CC5 u9/ [
1611 EnCrin
C. 005 u9/ t15i5 EnccsuI fan I I0.01 uglt
1608 !00
0. CC7 u9/ t
r'61 7 Endosut fan suI fate0.0C2 u9/ t1i29 DDT0.008 trg/ [
0(/13 Encr in Ketonc
0 .004 u9/ t
1850 Methoz.ych Lor0.Ci us/t
1aL1 ALpha Chtorclane
0 .0C5 u9/ t'
1-1)? Garrrna Ch I orciana
0.0C5 us/ t
Eatch: 96:31000:.A
N _ir.
N.9.
N.]-
N.D.
N.!.
N.D.
N.9.
I.!.
!,1 .9 .
N.D.
N.9.
N.9-
l{ -t,
N-!-
u.D.
N.).
N.D.
N.!.
lt.D.
96
97
E5
76
g2
't :3
on
92
9!+
1tz
91
86
95
g7
.q5
76
86
33
33
i 14
91
!.9
9i
3?
r02
90
8o
0
1
0
C
1
I
c
2
0
l
1
,]
0
J
2
,]
2
0
67 122
74 12C
69 126
66 12C
5t, 120
42 1?0
64 120
60 120
66 120
60 121
73 1?9
67 120
A7 4)1
5l '123
71 ';20
76 120
57 1/,0
i5 120
75 120
9C
101
i00
9?
69
92
na
90
82
^.',2
97
95
97
98
94
101
91
(l) The resutt for one or bolh determir,"tions pas lts: thrn ;rve trmes the r-00
MEMBEFI,E6m
Lancaster Ldboratofle5
2425 New Holland Ptke
PO Box 12j25
Lancasrer PA 17 605- 242.>
717-656-2100 Fax 717 656'2651 2216 Rer,Orr.r* d3
QL]AI.fTY CONTROL REPORT
5ee reverse srce ior explanatron ol symbols and abbrevralrons
QI-IALITY CO}ITROL RtrPORT
(I)Lancaste r Laboratories Page: 10 o{ 11 t
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A Thermo Analytical Laboratory
LLr Sampl-e l{o . 253,1999
CiJ-1 JUD Unspiked 6rab lJater Sampi-e
Hcrcules: Bacchus Pond
; Group No. 523727
I Fercutc.s, ln.o.poratcd
;
Sampte Sampte
I'IDL UXITS
foxaphene1. us/t
Endrin AtCehyde0-010 us/t
PCB- 1016
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Pc! - 1 221
0. 2 uS-/ t
PC8 - 1 2i20.09 us./ t
PCts - 12120.C5 uglt
PCE - 1 2/'B0.07 ug/t
PCB - 1 254
0 .0r5 ug,r t
PCB- 1?600.07 us/ L
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3371, 2-ch toroprirenol2. uE/ t
i1133 1,3 -di ch Lorohenzene?' u9/ |i38,i 1 ,4 -C i clr t orobenzene
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Lancaster Ldbo.dtones
242 5 Nerv Holland Prke
PO Box 12425
LancJSrer PA 17605-2425
717-656-2300 tax 117-656 2631 2216 Rev ,rrr* J.l
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HercuLes: Bacchus Pond
Group No. 5?37?7
liL.rcJ L e5, I nccroorated
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3350 bis (2-chloroethoxy) methane2. ug/t
3386 2,4-d i ch torophenot1. rr9/ t
39?1 1,2,4-trichLorobenzeneZ. uglt
390o naphthaIene2. ug/t
3e71 4-chtoroaniline1. uq/ t
3900 hexachtorobutad'ienel. uq,/ L
347? 4-chlcro-J-methytphenott*. u9/ [liO5 2'methytnaphthaLeneZ. ug/t
3901 hexachtorocyctopentadiene6' us/|
3q23 2,4,6-tri chlorophenotZ. u9/ t
19?? 2,4,5'tt-ichtorophenoI2. u9/ tlSll 2-chlcronaphrhatene2. ugi'.3al7 2'nitroaniLine?' u9/ |3ttr1 dinrethyt phthaIate6' ug/L38i8 acenaphth/l.ene2. ug/ L
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3e91 ?,4-drni trotoIuene
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717-656-2300 Fax 7 1i -555-2621 ,orror$ d}
QIJALITY CCNTROL REPORT
See reverse srde lor erplanatron oi;:imbols and abbre,JratLons 2216 Rev
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3387 diethyt Phthatate1. u9/ t
3375 4-chtorophenyt phenyL ether4. u9/ t
35,il] f Ir-rorene2. u9/ t
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Qr-IALITY COI.ITtr-CL REPORT
Page: 1 2 o'f
AThermo
LLI sample No . 2531999
cU-1 JUD Un:piked crab tJater SanlplL'
HercuLes: Bacchus Pond
Sarnp I e
uillTs
[ - ni r rosodi phenytanri ne4" ug/L(-brornophcnyI preny'l ether4. ugl t
hexach I orobenzene2- u1/L
pent ac h I oloph eno L?' ug/L
phenanthreneZ. ug,/ [
anth racene2- ug/t
ca rbazo I e2. ug/t
di -n-butyl. phthaLate2- u-o/t
f Iuoranthene?' ug/t
pyrene2. us/ L
butyI benzyt phthalate4. usl !
3, 3' -cli ch iorobenzidineL. us/ t
benzo (a) anthfaceneZ. u9/ t
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bc.nzo (a) pyreneL. us/t
indeno ('l ,2,3-cC) P'lrene1. r.rg/ [
Labora
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52?727
In.D.porated ' DE
Lancaster Laboratoaes
2425 New Holland Prke
PO 8ox 12425
Lancaster. PA 17 605-2425
717-656-2100 Fax 7'17-656-2681
LCS LII!I'ISI.OU H I53
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1 191
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53 127
1 152
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(iI)La ncaster Laboratories Page: 13 ofA Thermo Analytical Laboratory
LLI Sampl e IIo . 2531 ,a99cu-'1 JriD ,Jnspiked Gr.:) uarer saopI e
flercul.es: Eacchus Pond
6roup No. 5327?7
llL:rcutes, lncOfDorated - ]E
Sampie Sanpte}I9L UN I TS
3881 di bernz ( a, h ) anthracene4. u9,/ t33i;l benzo (9hi) perytene4. ug/ t
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Lancaster Laborato(es
2425 New Holland Prke
PO 8ox 12425
Lancaster. PA 17 605-2425
71 7-656-2 300 t ax 1 17.'a55' 258 1
DUP MS
RP!' ,'15 MSD RPD LCS
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QUAI,ITY CCNTROL REPOF.T
5ee reverse stde for explanatron oi;vnbols and abbrevralrons 2216 Rev
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(il)La ncaste r Laborato ries
Q'JALITY CONTROL F.EPORT
Page: 14 of '.4 IA Thermo Analytical Laboratory
LLI sampl-e No . 2531999
CU-1 JUD Unspiked Grab tJater SanpLe
Hercules: Bacchus Pond
0937 TcL Pesticides in Uate.s
4592 ICL Votatites by 3240 - uarer
4678 ICL Su846 se.nrivoLati Les,/Uaters
1t79 ICL 9,J8lr6 SenrivoLati Ies/!Jaters
Group llo. 522727iiercuIes, :ncc.poratcd - DE
SURI]OCAIE SUIilMARY
TR!AL 1D S'.]RIIOGATE RqCCVERY Z
rcx 79
'Ja8 89
. c1- 1 ,Z-OCA 97
CS - to luene 103
JTU
2-Flphenol 52
Plrc'not -ci6 3i,2,q,6-\E? 75
\itrobz-C5 31,Z-fbignnyi 7q
T 2h eny I c 11, itl
SUNR96ATE L!MIlSLot lt ! 6H
6C 120
t.i 1 )i
76 1it,
33 1108'o 115
21 10Ci0 9110 123
35 1,1.L/i3 1 la,
MEMBEFtrem
Lancaster Laboratoiles
2425 New Holland Prke
PO Box 12425
Lancdsiet PA 17645 2425
7 I 7-656-2 100 F ax. 7 17 -656'263 1
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La ncaster Laboratories
A Thermo Analytica I Laboratory(I)
TO
TO
CAT
NO-
1592
17??
1743
174t
1746
1747
17!,9
1751
1753
1755
1758
1761
1766
1772
7Cl5
7036
0259
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$7A
1679
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LLI sample No. EL 25380CI7CoItecred: 6/26/96 at 11:55 by BR
Su&nitted: 6/28/96 Reported: 8/ 1/96Discard: 8/ 9/96
CU-2 JUD Grab Uater Sanpte
Hercutes: Bacchus Pond
C2JUD SDG#: HBPo'l -03
A}IALYS I S IIAME
TCL Votati les by 8240 - !,ater
Thattiunt
A ( ulri num
Ant inDny
8ar i um
Eeryt t ir-rnr
Cedrn i utn
Chromirnr
Copper
I ron
Le6d
Man9anese
Nickel
9 t Lver
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Arseni c TR
Seteniuri IR
i'!erEury
TCL Pesticides in Uaters
TCL StJ846 Se,nivoLat i Iesl!,aters
TCL SU846 Semivo!.ati Les,/Uaters
'I COPY
1 COPY
Heccut es, I ncorporated
ERI'l - Rocky 14ount.r in
Account No: C6716
lieccuIes, :ncorporated - 9Eqnviroffnental Aflairs
UrLmington ci !9894
Page:1of 14
P.0.
Re[.
Respectf ul. l-y Subrni tted
!?antrna V. Layllan, CIoup Leacer
I cP l'1eta ls,/Leachates
A5 RECEIVED
:t.td Sl l- I S'
,',r,, lI - D,;
'1 / 1
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:.:,:i,,, . ll,D.i
,, q.?
:,, i.1 70 -
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DETECI:9N LII.I!I UIIITS
See Page
170 - !9/t-
J 57 . ug/:
i5. u,j/!
) ) tnti
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J -1 .3 'rg/'.
5 .9 !9i'.'!S. uJ/ t'
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3 -6 ug/:.
'l 2. ui/ tJ ?.7 ugl i
i '7 'tg/ t'
0 . r43 ug/ l-
See Pagegee Pase
See Page
)
1
5
ATT!: l'1r. Joseph (eLLer
A'f 1!: i,1r - BrL-nr R!.ilinson
Qucstlons? Contact vour Ctienr: Serv'ccs Represcnrartve
RacheL L. Kcea[er a,: (i'i'l 656-2::1]0
03:40:40 D 0,JD2 15 R[2 i:5r,ji6 iZ?727
310 '15.00 00125700 ASR00,
74Cm
Lancaster Laboratofles
2425 New Holldnd Prke
PO Box 12425
Ldncaster. PA I 7605-2425
717-656-2300 Far 717-656 2581 seo rever5e 5,op lo'exola.dlron ct \ymccis and abb'e'.,ral ons 2216 Rev,Or,Or* d3
I
(iI)La ncaste r Laboratories
A Thermo Analytical Laboratory I
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Suhnitted: 6/?8/96 Reported: e/ 1/960iscard: 8/ 9/96
CH-z JUo 6rab llater Sample
Hercutes: Bacchus Pond
c2JUD SDG#: llBP0',l'03
CATIIO. ANALYSTS NAHE
TcL voiarites by 8?40 - uater
1258 Chloromethane1?57 6romoflethane3492 VinyI Chtorideit 94 Chtoloethane3i,97 l4ethytene chLorlde3,i98 Acetoneitr99 Car!:on D,isui.fiCe3500 1,1-DichIoroethene3501 1,1-DichLoroethane1503 Ch Ioroformisi)L 1,2-Dichl.ccoethane0316 2'Butanone3505 '1, 1,1 -TrichLoroethane
3506 Carbon TetrachIoriCe3507 vinyt Acetate3508 ErornodichLoromethane3509 1,?-DichLoropropane3516 cis-'1,1-9ichLoropropene3511 Trichtoroeri:erte1512 0ibroltochloromethane3513 1,1,2-TrichLot-oethane
35 1 5 Benzene35'10 tcans-1,5-Dichloropropene35'18 Brotnofocm3521 4-Hethyt-2-pentanone15?0 2'flexanone3532 Teteachtoroethen"-3521 1,1,2,2'Ierrachtoroethane3iZ4 ToIuene'3525 clr L orobenzene3't26 Ethytbenzcnei528 Styrene3529 xyl ene (1ota[ )5780 trans'1,2-Dichtoroethene6263 cis-1,2-0ichLoroethene
LLI Sample No. EL 2-53EC07
CotIected: 6/2b/96 at 11:55 by 8R
Page: 2 of 14
Account !,lo: C6716
fle.cutes, Incorporated - DE
Envi ronfllentaL Af fai rs
lJitminston 0E '19894
P.0.
Rel..
Respectfu[ !.y subori tted
lr!icoeLe l{c!larin, B.A.
Gcoup '-eader, cclHS VoLati Ies
AS RECEIVED
:1,:-,'.1,:.::]l;:::::il::::::.::j::,::::::::j:]:::] HETHoo
riii;;;:jli:r,::ii:.:i.l!EEU1-Ig,,r'r::::'i DETEcT I DN L I l'( I T Ull I Ts
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us/ t
u9/ t
us,/ L
UE/ I
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us/ L
u9/ |
ue/ L
ug/ [
us/ t
us/ t
u9/ l
ugl t
u9/ t
u9/ t
u9/ L
UCJ/,,,L!/'.
ugl I,r!/ |
u9/ t
u9/ t
u9/ L
u9/ |
uql t
usl I
u9/ l.
uql L
ug/ t.
us/ L
ug/ t'
u9/ L
u9/ t
us/ l.
u!/ i.
Questions? Contact your Cl ien:
RacheI L. Kre3rnnr
Servi cas Representat tve
at (7'7) 6i6-23CC
MEMBEFl7Xm
Lanca5ter Laboratores
2425 New Holland Prke
PO Box 12425
Lanca5ter PA 11 605-2425
7l 7-656-2100 Fax: [phone]E1
ilt!e
I
5ee reverse srde for explanatron ot symbols dnd abbrevratton5 2216 Rev l0/30/95
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(I)La ncaster Laboratories
LLI sampLe No. EL 2-538C07
ColtectL.d: 6/?6/90 at 11:55 by 8R
subilitted: 6/2e/96 Repo.ted: 8/ 1/96
0iscard: 3/ 9/96
CU-Z JUD Grab lJ3ter Samp[e
Ilercules: Bacchus Pond
C2JUD SDG#: HBP0l -08
CAT
IIO. AIIALYSIS IIAHE
I Account llo: 06716
' Hc'rcules, In.crporated - DE
' invi rorunenta', ;\f f a irs
il i i. rrr i ng ton 9E 19894
A9 qECS IVED
A Thermo Analytica I Laboratory Page: 3 of 14
2)15 Rev,Or,O,n, dt
P .0.
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DETECT:CI.I LI14IT UN!TS
TcL Pesticides in Uaters
1600 Atpha BHC .:t:,,,]1:.:i:lll l, '., rl.D. C.CCZ ug/t
1501 6era BHc ,. .'l ,, i1.:,. 0.9uS ug/\
1503 De[ta BHC . . ..,.. ]' l.l .0. 0.0C5 u9/!'1otl2 Gailrna BilC - Linderre . N.:. C.CC2 ui-l/t1{0! Hcprachtor , ',, i}.i'. 1r.005 uglL1005 Aiclrin , ,. l.rr. C.!f1* uglL'ia06 lregrachtor Eooxice :, :1,:-'. 0.0c1 ug/t-15!5 Endosul,ian I li.-r. ,1.0f3 ul/|1o10 Dieldrin ,,, , ,, ri.r--', 9.t!: ucJ/tio0z DDE ...::. '..,'i,0. 0.CC5 ugll
161 1 Endrin ... , .. ' , ){'.'ai. ' C.009 ug,/l1ci5 Endc:utf an Il . {.?, C.ijl ug/t
1608 090 ..,..,.: ' li.r. '1.007 ug/L..L17 Endosutfan Sutf,;te l,l.i. 1.107 u9/'-
DtiS En.lrin Ketone i.: , ,.i1.1. 0.!f4 ug/r.lab} ilarh.xycirr-L)r ...1.. N,!'. 0.13 u\/t-IiD1 ALpha chtordan" ',, , , l{.i. ?.!9! ,eZL
i-i52 Giirrr)r chLordJne :... 1i.:,'. C.345 ug/l'1,:11 Toi:3phene i! ,l: ;. 1 . u.i/ L'lcil-! End|in ALdehyd' .....' ll.:). tr-C10 ul/l
10.:9 pCB-i0.16 .,'. , ji.i, a.:}9 ug/|
1oz0 PC9-1221 ..:... rt.:',. , '1 .2 !!/i
1ol1 PCB-1232 .., v-r. ').t:? Lrg/''1,!12 ?cB-ftf7 .' ,',i. il .ir, Ii,35 Q9/\li3l Pc3-1?18 i\.;. i.!7 'J9/''iili ?a3-1?i'* .....,.. li .1,. C.Cr ug/'L
1526 PCs-1260 I .l.l'. C.:Z u-c/i.9!!'to ir)sufficiEnt sanple sizt, xe Here L::ab,.!-'tc rcpoi't our u::uaL
ri!.rntitation Lintits. Tic vnl,ues reporre'cl ::prL'surlt tlre LoHE's: q'-:antitation
Liliiis abtainai;Le-
TXim
OLrestions? C,lntsct vour Cti':::t Scri'ices Representatl'/e
Rachtl' L. Krclrrr3r .r: (7ll') 655-21'lc
Lanca5ter Laboratofle5
2425 New Holland Prke
PO 8ox 12425
Lancaster. PA 17 645'242\
717-656-2300 F3x 111-656 )\!'i
Respectfut Iy Submi tted
Jeni{er E. iiess, g.S.
6roup Leader Pesti c ides/PCBs
5ee reverse srde for explanaton ol symbols dnd abbrevlatlons
(l)La ncaster Laboratories
A Thermo Analytical Laboratory
I
i Account No: 06716
I tlercutes, Incorporated - DE
iEnviromntel Affairs
| ';'i tnrington oE '|9894
i
Page: /, of 14
.I
LLI sample No. EL 2538C,07co[[ected: 6/26/96 at 11:55 by 8R
Suhnitted: 6/28/C6 Reported: B/ 1/96
Oi scard: 8/ 9/96
CU-z JUD Grab Uater Sarnpte
Hercutes: Bacchus Pond
C2JUD SOG#: HBPO1.LT8
CAT}IO. ANALYSIS NAHE
TCL SU846 Semivotati Ies,/tJateFs
3918 phenoI
38,67 bis (2-chtoroethyt) ether
3871 2-chtorophenoL3B8l 1,3-dichLorobenzene
334/+ 1,4'dichLorobenzene1882 1,2-dichIoroE'enzene/168,0 2-methylphenoI4581 2,?'oxybis (l-chl.oroPropane)
15BZ 4-methyIphenoI3915 N-nitrosodi-n'propyLamine3902 hexach Ioroethane
3910 ni trobenzene3904 i sophorone391'l 2-ni rrophenot3890 2,4'dimethy!.phenoL
31166 bi s (2'chtoroethoxy) methane3836 2,4'dichtorophenoI3921 1,?,4-trichlorobenzene3905 naphthatene3371 4-chLoroani i. ine3900 hexachtorobutadiene3372 4-chLoro-i-nrethyLphenoLi905 2-rflethyr,naphthalerle3901 hexachtorocyctopentadiene3921 2,4,5-trichLorophenot39?? 2, q,5 - tr i ch torophenDL3873 2-chIoronaphrhatene3907 2-nitroanitinelB9'l dinrethytphthatate5858 acenaphthytenc'
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ar (7"7) 655-2i00
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AS RECEIVED
,:,.rii..j,i:i,,:,ft E StjlrTS.'.,
t'!ETH00
DETECTICN LTMIT UIJITS
u9/ [
u9/ i
u9/ t
us/ t
ug/ t
r9/ t-
ug/ L
us/ i
ug/ t
,Jg/ |
u9,/ t
us/ I
ugl I
ug/ t
u9/ L
u9/ t
u9/ L
ugl t
ugl t
u9/ !
ue/ L
u9/ I
u9/ 1-
u9/ i
us/'.u!/ [
ug/ L
rg/ t-
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ouestions? contact your ctient
RacheL L. Kao:t:)er
II
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Lan(aster Laboratofles
2425 New Holland Pike
PO Box 12425
Lancaster, PA 11 605-2425
717'656-2300 Fax 7'17'656-2681
RespectfuI Ly Submi ttedChristine l'!. i?arcLiff ,
GrouP LeadL'r, Gc/MS
See reverse srde lor explanatron of symbols and abbreviatrons
I
2216 Rev l0/10/95
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(iI)Lancaster Laboratories Pag e:
A Thermo Analytical Laboratory
5of 14
LLI Sample No. EL 2--5i8007
cot tected: 6/?c,/96 ar 'l 1:55 by 8R
subflritted: 6/28/96 Reported: 8/ 1/960iscard: 3/ 9196
cU-2 JUD Grab uater Sampte
ilercutes: Eacchus Pond
CZJDO SDG#: HBP01 -C3
CATIIO. AIIALYSIS NAI.IE
TcL SU846 Semivotati (es/tJatens
3908 3-nitroanitine3857 acenaphthene3893 2,4-dinitnophenoI3912 4-ni trophenoL3879 di benzofuran
!99!. 2,4-dinitrotoLuene3Aq5 2,6-dinitroroluene3n87 di erhyt phthatate
3375 4-chtolophenyt phenyI ether3893 f l. uoreneit09 4-nitcoanitine4633 4,5'dini tro-2-methylphenoI
3q11, N-nirrosodiphenyIantine
i869 +-bromophenyL phenyL ethcr3899 hexachlorobenzene!916 pentachtot'oohenol
3917 phenanthrene3159 anthracenc'
t h84 carbazote
3830 Ci -n-buryt phthatate
3397 f tuocanthene3tl9 pyrene3l:70 butyl benzyI phthatate
3835 J,3'-di ch Loeobenzidi ne
336D benzo (a) anthracene3868 bi s (2'ethyLhexyt;) phthaLate
2876 chryseneiB96 di -n-octyt phthaIate1361 benzo (b) iIuoranthene13,62 benzo (k) {'.uoranthene316!, benuo (a) pynene
3rt)3 indeno ( l,2,3-cd) pyrene3831 dibenz (a,h) anthracene
3163 ben:o (ghi ) perY[ene
Duu. to insufficienr sannpIe,
semi voLat i Ie cont2ouncls r.'rc'
I
lrrccount !lo: 057'16
I HeccuLes. lncorporated
i Envi ronqenta l. Af ia i rs
I Hi Lflrincton }E'1989/.
I
AS RECEIVED
:i::r:'::,i:,.::,::::r: : : HETIjOD
::1.:::::::,,:rlt!S:JLT9':, DETECl!olJ LIMII UNITS
DE
on
Ret.
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the q,..:anritarirn L it|its f or the Cc,/i'ig
TA ] SC1.
ouesti ons? contact your
Rache'. L. K.3arxer
CL 1..n! SL'r'vi cL's qepresel!:rt lve
ar (T-/ ) 6io.2_j!0
RespectfuL ty Submi tted
Cirristine Il. RatcLiff ,
E ro:p -eader , GC/l'lS
5ee reye.se srde for erplanatron oi 57mbol5 and abbrevlattons7Xm
Lancaster Laboratones
2425 New Holland Prke
PO Box 12425
Lancaster PA 11 6A5-242\
717-655-2100 Fdx 717 655 268 I d',2215 Rev t0/lor95
T
,E&&
(l)La ncaste r Laboratories ilPage: 6 of 11
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2216 Rev ,Orrr* i-il
A Thermo Ana lytica I Laboratory
EL 25330C7'l 1:55 by BR
LLI Sampl-e No.
CoI lectiC: i:5/2i/96 at
Suhnitied:06/?3/96
1722 That t ium17t1 AIuminurn
17t,4 Ant irrony
17!"6 Bar i unr
17lr7 BerytIiultt
1 749 Cadrti ur
'1 75 1 Ch roil1i um
1753 copper
1754 I ron
1 755 Lead
1 756 14anganese1761 N i cket
1766 Sitver
1772 linc'1348 UU su846 lcP Digest (tot rec)
7015 Arserric TR
7036 Setenium TR
0259 ltercury
5713 'JU SiJ846 H9 C i grest
, Account No: 06716
i liercutes, Incorporated - DE
I Envi ronnrenta I Af;a i rsi ',,1i tmington DE 19394
!CU-a JUD Grab l.Jater SampLe
HercuI es: Bacchus Pond
C?Ju, S9G#: ll0P0'l -08
CATNO ANALYSIS IIAME !4ETHCO
1592 Tcl- Volatites by 8240 - Uater sU-846 82408
su-846 6010A
s,J-3q6 6.-'1CA
Sk - 846 61-1 1 0A
Sl,l - B46 o! l 0A
su-345 631DA
Sr-94o 63'1DA
su-345 6DtCA
SU-34.i 6l:t'lA
su-846,51',lCA
sl",J-ltl,6 6',li0A
s,J-845 6,11CA
SrJ'846 6'11 CA
su-845 5ri0A
s',,1-845 6J1r_1A
su-346 Lr05A
su-846 4:iCA
Sl,l-84o ,5;1'l:lL
su-845 71,70A
s,J-3,,6 7.,7CL
ANALY S I S
TRIAL OATE AND TII',!E
1 07/03/96 0747
1 07/15/96 03581 07/15/96 4353i 07/15/96 C353' r 07/15/96 C35E1 07/15/c.)6 C353\ a7/15/96 ?i,\g1 17/^'1/96 c355
1 nrl.cror n:ao. vtI,)Irv w-)-1 07/15/96 A31t1 07/15/96 C1581 07/15/96 0358'r 07/15/96 l35E1 C7/15/96 C3i31 A7/15/96 A3531 07/10/q6 1???1 07115196 C3551 07/15/96 C358
1 07/13/96 19171 07 /t2/96 ?1.22
1 07/01/96 13341 A7/A6/96 C951
1 O7/A?/e6 C93A't C7 /D4l9t 01'.21 !7/Ct+/9b tt ".2
ANALYST
susan A. McMahon
Donna R. Sackett
0onna R. Sacketl
Donna R. Sackett
Donna R.. Sackett
oonna R. Sackett
Donna R. Sackett
0onna R. Scrcketr
oonna R. Sackett
Donna R. Sackett
Donna R. sacketr
Donna R. Sackett
Donna R. Sackett
Donna R. Sackett
oonna R. Sackett
chcistine M. Con['in
Donna R. Sackett
Donna R. sackett
{eLti S. l'!arkaryan
lletLi s. l,lafkaryan
Marcie A. Natate
oougtas D. Seitz
Maria A. Davenport
l4ark A. RatcL if f
l'13rk A. Ratct i f f
0817 tJater Sampl,e Pest. E,rtraction sU-846 35108
Aq37 TcL Pestrcices in lJaters Sli-$Lb ?,121
0813 BNA. Harer Extraction SU-846 351C8
!.678 ICu Sl.i846 Semi','clati Iesl!aters S'J-31,6 32708
!,679 TC! SiJ946 Senivo',ati Ies/",]aters SU-846 S?708
Lancaster Laboratories
2425 New Holland Pike
PO Box 12425
Lancasteq PA 17605-2425
7 I 7-656-2300 t ax 7 1 7 -656-268 1
MEMBEFlKXII
U\BCRATORY CHRCNICLE
see reverse side for explanatron of symbols and abbrevratrons
I
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(I)Lancaster Laboratories Page: 7 ot 1t+A Thermo Analytical Laboratory
LLI sarnple No. 25i3007
CH-2 JUD Grcb Uater Sampte
Hercutes: Bacchus Pond
<)a7aa! uruuP ,ru. ,E!r L,
ce"c'Jt€.s, :ncJ.porated - DE
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Samp t e
MDL
Samp I e
UII.I TS
r-cs Lcs
LCS DUP RPD
OIJ? MS
RPD M5 HSO RPO
LCS LII'!ITS
LOV HIGH
1592 TcL Votatites by 8?40 ' lJater
1?58 chtoromethane3. trg/t
1257 Bromonethrnel. us/ |
3192 Vinyl. Chtoridez' us/ t
3494 ch t oroethane3. u9/ t
3497 merhytene Chloride2. tig/ tl/,98 Acetone6, uS./ t
3499 Caebon Di suLfide3. u9./ t
3500 1,1 -0ichIoroethene1. ug/l3501'l, 1-0ichLoroethane2. ug/ L150l Ch I orofornr
'l ' uglt
3504 1,2-Dichtoroethane2. ugl L0i16 2-Butanone3. u9/ L
3505 1,1,1-Trichtor-oethane1' u'/L
3506 Carbon Tetrachloridel. ug./t
3507 Vi rryt Acetate2. u9/ l-
l5ilo Eronrodi chtoromethane1. ug/t
3509 'l , 2'D i ch I oropropane1. tiS/L
3515 cis-'1,1-DichIocopropene1. ul/t
3511 TcichIoroethene1. Lrs/L
3512 D i brotnoch Lorcrriethanc2. u9/ t
3i1 3 1, 1,2-Trichl.oroeth.rnez' ug/t
1t l5 Senzene1' u,/l'
3510 tran$'1,1-0ichloropropene1. us/L
BLA iIK
Eatch: I96'1841AA
N.l.
N.D.
ri.D.
N.l.
l,i.!.
I'r.!.
N.l -
N.r-
N.0.
N -!.
N.0.
N.D.
IJ .D.
N.9.
N.D.
i{.0.
I-!.
!i.D.
N.0.
N.D.
l!,_1-
8
s
9
9
3
30
4
7
3
4
4
41
2
1
27
5
2
4
1
'6
0
12
73 68
38 31
90 82
oT 5l
1 !i? 93
67 9i
11!, 106
10i 190
115 109
95 r00
64 97
't'16 1ln
'l'r1 ]10
s4 110
9c) I 0,i
9g r01
97 : C]
116 1 05
e7 99
s2 96
q. 117
MEMBERTXrA
Laocas(er Ldboratofles
2425 New Holland Prke
PO Box 12425
Lancaster, PA 11 605-242,<
717-656-2100 tax 717-656 2r:Bl ,orrorn, d'f
QUALITY CCI{TROL RE PORT
sep revp,se srde,O. e.prarralroi oi Symbo'r dad aoorerratrons 2216 Rev
t
(l}La ncaster Laboratories
A Thermo Analytical Laboratory
QUALITY CONTROL REPORT
P age:
LIr{l'rs
HtGH
li
t
t
t
tl
t
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LCS ICS LCS
LCS OUP RPD LOU
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;ilercutes.i
II
DUP IlSRPD I4S I.1SD RPD
LLT samPre Itro. 2533007
CU-2 JUD Grab r,Jater Sarnpte
Hercutes: Bircchus Pond
5?2727
Inco.porated - DE
Sa'npte SamPte
MDL UIIITS
35,]8 Bromoform1. ug/t
3521 4-t4ethyt -2-pentanone
5. us/ |
3520 2-Hexanone7- uglt
3522 Tetrachtoroethene
'I . u9./ t
3523 1, 1,2,2-TetrachIoroethaneZ. u9/ t
3r?4 Totuene2. u9/ t
55?5 Ch I orobenzene1. uglf
552o Ethytbenzene2. u9/ |i528 Styrene1. ug/l
;529 Xytene (totat )1. ug/t
5780 trans- 1,2-D i chIocoethene
Z. u9/!
:158 cis-1,2-DichIoroethene?. trS/ t
t722 Thatti,'tm
1 70. u9/ t'i743 Al.uminum57. ul/t
1741, Antimony
15 . u9,/ t'1746 0ar ium2.2 trg/t
:247 EeryL L ium1.3 ug/t
174? Cadnrium?.7 u9/ t
'!75 i Chromi emt,.3 u9,/ t'1753 Copper3.8 u9/ t
1754 lrun5-q ug/L
:755 Leadlti. ug/t
l r'53 !tanganese2.9 u9/ t
'i51 tiicket5.\ ug/t
ll{.5 Sitv.'r1-5 uS/t
71 90
65 93
lrz 95
1C6 105
72 9t
1C5 iC5
101 101
1r0 109
102 102
-108 108
1C4 99
105 102
(1) 101 103
17/. -772 -729 (2'
(1) 115 106
o7 00u t ',
(1) 97 97
(i) 9t, 95
0 (1) 7e 79
0 (l) -?01 -191
171 -1513 -1441 (2)
0 (l) 92 93
0 (i) 59 61
0 (1) 94 95
(1) 99 101
lt4
36
I+i
2
0
c
?
,!
0
5
/4
'I
24
1
1
0
'l
2
9
3t
1
J
1
1
102
'103
107
'100
9B
97
107
101
'1 11
102
i03
i04
100
80 120
80 120
B0 120
80 120
B0 120
B0 120
80 120
B0 120
80 120
80 '120
80 120
B0 120
8C 1?C
,:'l) The resutt for one oc both determination:i Has Iess than five tinles the r-0o-
t2) The background resutt las more than four tir,res rhe spike aclded.
Lanca5ter Laboratofle5
2425 New Holland Prke
PO Box 12425
Lancastec PA 17 605-2425
7 17-656-2 300 F ax. 1 11'656-2681
MEMBER7rcm 5ee reverse srde for expldna0on oi symbols and abbrevratrons 2216 Rev l0/30/95
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(iI)La ncaster Laboratories
QUALITY CONTROL REPORT
P age:A Thermo Analytical Laboratory
LLr Sampfe No. 25-18007
Cu- 2 JUD 6r.,h Uater Sarrlrte
flercu!.L-s: Bacchus Pond
j Group No. 522727. liercuIes. lrccrporated - DE
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sarnpte SampteIIDL UN ! IS
1772 7\nc12. ug/t
7035 Arserric TR2.7 u9/ i
70J6 Seteniunt TRZ-7 ug/t
0259 llercury0.043 u-o,/ t
0937 Tc! Pe:ticides in uarer':i
DUPRP' fIS
MSI1SD RPD
c90
1 r01
0 10!
092
172
469
c9?
, ao
090
082
3 112
197
195
097
398
29t
1 103
291
086
LCS LII'IITSLOII H ! GH
B0 120
80 120
80 120
80 1?0
67 12?
74 120
69 126
66 120
54 120
42 ',120
64 120
60 1?O
66 120
60 120
73 1?9
67 120
67 121
53 12A
7i 120
57 "140
75 120
75 120
LCS LCsLCS DUP RPD
0 (1) -t1 -i4
0(1) '!01 102
0 (1) 101 102
0 (1) 79 79
5
1
,l
0
103
103
103
93
1500 Alpha BHc
0. tl32 us/ |
-1o01 Br-ra BllC0.005 u9/ t
1103 Del ta 8HC
0. C05 u9/ t
1502 Ganrna BilC - Lindane. 0. C,r1 u9/ t'!a0i Hepiachtor
0. CD5 u9,/ [1605 ALclin0.004 u9/ t
1606 Heptach tor Epoxi de0.OCi ugl ti415 EndosuI fan I0.0C3 u9/ t'!510 Die.Ldr in
0. CC5 ug/ I
1537 }:De
0. C05 ug/ t.
1611 Endrin0.,1C5 u9/ tir'15 Err('lc::uIf ar] I IC.C.l u9/[
i i03 DiD0.rlC7 us/t1617 Endusut fan Sutfate0-0ni' trg,/ t
1609 DDT
0. J05 'Ls/ |
0(-tlal Elcrin (ctonc
0. l]rr,i u9,/ L
I J:.l tiatl.);i).';h L eri.i: ug,, I1l;1 At1:r:ra Ch!.:rCane
0 . 0'-'t rr9/ L"iit,2 G:i;::ir; Ch i urileLe' C. Crls ug./ |
Batch: 9618iC00i.\
!,1.9.
!{-9.
N.!.
ti.9.
}i.9.
N.9.
N.C.
N.D.
N.C.
N.D.
N.!,.
N.l.
N.0.
ll .:r .
N.1.
r:.D.
r,i.c,.
85
96
97
to
a2
90
90
92
91!
Ol
102
91.
86
97
35
76
86
o?
8l
cq
91
89
E3
9Z
aa
102
90
36
r:) Tl,,; restrlt for one Dr b.lt!r clcter'frination:l ras L'-ji t'rar :l!'e tlntes the ,-O0.
iEHii
Lancaster Laboratofles
2425 New Holland Prke
PO 8ox 12425
Lancasler. PA 17605-2425
1 17 -656-230A Fax 7l;-656-2631
.!
,orron, ?aiSee rere'se srde ro'erpldnat:on of symbols and abbrevrdlrons
(l)La ncaste r Laboratories
Q'JALITY CONTROL REPORT
Page: 1 0 ofA Thermo Analytical Laboratory
14 I
LLI sampl-e No. 25380C7
clJ-2 JUo Grab Uater Sa,npte
Hercutes: Bacchus Pond
: Grouo No. 522727
; hercuIes, :ncoroorated - DE
I
I
Itcs r-cs Lcs
LCS OUP RPD LOU
DUP USRP9 MS ',ISD RPO
Sarnp[ e Sampt eI4DL UNITS
1613 foxaphene1. ug./t
1618 EMrin Atdehyde0.010 uslt
1619 PCB-10160.09 ug/ t
1620 PCB-12210.2 u9/ t
1621 PCB-123?0.09 u9/ t
1522 ?CB-121?0.05 u9/ t'ri23 Pc6-',I2480.07 us/t
ioZlr PC\-12510.06 !9/ L
5?6 PC8-12600.07 ug/t
ELANK
N.D.
N.D .
N.0.
N.D.
N.D.
!.t .0.
N.D.
N.D.
N.r.
LI}IITS
HI6H
1?6 I
-8 TCL SlJ846 Sernivotati Ies/Haters Batch: 96-lB/,HAA0Z6
1'7i B phenot?' ug/t
i367 bis (2-chloroethy[ ) ether
Z. u9/ I'337\ 2-ch IorophenoI2. u9/ t3ll3l 1,J-dichtorobenzenez' u,/t
38,J4 1,4-dichtorobenzene2. ug/t3882 i,2-dichtorobenzeneZ. us/t\LBn 2-methyLphenoL4. us/ [
-:81 2,2'oxybis (1-chtocopropane)t,. ug/ L
Lt32 4-metl'ryIpheooL'!+. uS/ L
39'15 il-ni trosodi -n-propylrnine
t+. us/t3t02 hexachtoroethane
l, . ug,/ t
3910 ni trobenzene?' ugl L
3904 i sophorone2. usl t
59^.1 2-ni trophcnol1. us/ t
19
91
38
ta
8fl
7q
67
o7
47
91
B9
62
82
&2
B3
1i 1,
7B
97
i0c
95
l
1
5
j
1
?
0
4
I
0
0
1
44
BS
B5
63
7C
71
77
6t,
7S
1C3
5l
9t,
97
9?
5
1?
?3
'!0
72
97
DC
94
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32
46
36
1
40
35
)1
29
1,12
158
134
172
t14
125
123
166
1q?
230
11i
'180
19o
182
MEMBEFlrrcm
Lancaster Laboralories
2425 New Holland Prke
PO Box 12425
Lancaster PA 17605'2'125
7 17-656-2300 F ax 7 17'656'263 1 il
I
5ee re!erse srde for erolandtron of symbols and abbrerratrons 2216 Rev l0/10/95
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(l)La ncaster Laboratories
A Thermo Analytical Laboratory
QIJALITY CONTRCL REPORT
LCS !_lr'ltrs:ou H I Gi.1
,'1
LLI sample No. 253300i
Cll-2 JUD Grnb lJater SarnpIe
Hercutes: Eacchus Pond
Sampte SampteMOL UH I IS
2,4-dimethytphenoL?- us,/t
bis (2-ch Loroethoxy) methane2. u9/ I'
2,4-dichtorophenol4- us/t
1, 2, 4- tr i ch Lorobenzene2. u!/t
naph tha L ene2. u9/ t-
4-chtoroani L ine1. ugll
hexachLorobutadieneZ. us/ L
4 -ch L oro-3 -ntethyI phenoI4. uC/ l.
2-nrethytnaphrhatene2. us/ t
hexach t orocyc I opentadi ene6. us/ t
2, 4, 6 - tr i ch t oropheno I2- ug/L
2,4,5 - tr i ch I oropheno L2' uglt'
2-chIoronaphthalene?' ug/[
2-ni troani l ine
Z. u9/ L
dimethyt phthaLate
6. u9,/ L
acenaphthyt ene2' u,/t'
iGroup !{o. 523727
ilercutes, lrcorporated nr
i
LC9 !-CS
lCS OUP RPI
OUP MS
RPD HS MSD RPD
I
3690
3886
392 1
390o
387 1
59C0
1A?a
3905
3901
3923
39??
JC/J
39'ol
1591
f 3-'i3
BLAUK
N.0.
N.9.
N.0.
N.0.
t .!.
N.D.
{.0.
N.D.
N.D.
N.D.
N.D,
N.D.
N.9.
N.g.
N.D.
N.0.
N-0.
N.D.
tl .D.
66
90
79
83
7?
65
91
51
89
39
9'1
o7
1)
92
70
9C
36
B,]
74
59
93
s7
53
87
88
90
s7
jI
93
7
0
0
3
C
?
7
1
1
5
l
1
'1
0
1
2
65
86
7A
B1
73
91
BO
11
91
90
8B
95
25
B6
3Z
33
39
/+4
21.
17
24
22
,o
1
37
39
60
53
IJ
119
lJ)
142
IJJ
116
1 '16
147
123
100
144
'151
118
t4J
11?
1t5
L679 IcL SU3/,6 SernivoIati Les/uaters Eatch: 95'184lr.r.C],5
l(t08 3-nitroaniIineZ. u9/ L
3357 acenaphtheneZ. u9/ t
3893 2,1+-dini tropher)oL10. ug/t
191? 4-ni trophenoL10. ug/L
2879 dibcnzofuran2' ug/ ,'
389c 2,4-dini trotoIuene/.. Ltg/t.
3tJ95 2,6-dini tTotoluene
Z. Lls,/r-
93 9l
41 37
s9 83
9\ ?6
9q 100
1
0
10
5
1
1
1
nn
fr7
92
55
B5
94
95
1I{J
145
191
132
131
139
158
7
47
,a
l9
50
7r6m
Lancaster Laboratofles
2425 New Holland Plke
PO Box 12425
Lancaster PA 17 605-242\
717-656-2300 Fax 7ll il5r lb3l 5ee reverse srde lor explanatroo of symbols and dbbre','atrons 2215 Fer,Orr.r* d3
(iI)La ncaster Laboratories
A Thermo Analytical Laboratory
Q'JAIITY CONTROI- RFPORT
Page: .lZ of 11
LCS LIMITS
LOU I] I Si1
;l
;lLLr sampl-e No. 25380C7
CiJ-2 JUC 0r;b U.1ter Sarnpte
Hercules: Bacchus PonC
Safipte SarnoleIIDL U}I I TS
diethyI phthal.atet-. ug/ L(-chlorophenyL phenyI ethert,. u9/ t
f tuorene
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i il
1l
il
jl
tl
il
;l
il
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LCS LCS
LCS DUI RPD
DUP TlSRPO I4S !'!SD IPO
3ZB7
;:J?8
3tD9
r,914
:169
131)9
;9 lo
1917
:a59
r58Jr
: a:)i)
1ar'l
a'.'',,-;
iitl)
157n
ieg6
?c i I
33tt,
l,),j j
2.us/ t
4 -ni troani t i ne/.. uS/t
4, 6-di ni tro-2-methytphenol
10 Ug/ [
N -n i irosodi phsnylanri ne
A . u-q,/ !
4-bromophenyI pheny!. ether
4-ug/ L
hexach lorobrnzene
?. u9/ |
pent3ch IorophenoI
?' ug/t
phenan t h rene
2- trg/ L
anthfacene?' ug/t
carbazote
2. uglL
di -n-bui7t phthat;te
?' u9/ t
f I uori:nthene7. u9/ t
py.ene
2. ugl L
buryl. ber:zyt phthatate
/, . ttcl/ \
3, J, -oi ch i.;rooenz i di ne4. uE/ |
bc-nzc (a) anl\.acenc)uq,/ t
A.u9/ t
ch rys c ne2' u!/|
di -n-ocryI phthalate
4.uq/'r
benzo (b) f luoranrhr-nei,. ug,'t
bcn:o (l) f Iuor-]nrhenL'
u9/ t
bis (2-L.rirytheir.yL ) .ohrhiii.atc
8 LAIIK
N-C.
ti-0.
N.9.
N.r.
N.!.
N.!.
li -D.
N.t.
N.D.
N.D,
1t.3.
N.0.
N.D.
N.D.
N.D.
N.9.
!.1.
lt.D -
N.D.
!(.t-
N-D-
64
103
1C2
85
67
oo
83
95
95
83
92
89
90
93
c)
35
1t2
91
100
9C
s1
76
65
1n,
98
51.
16
27
94
40
91
g7
90
89
9l
80
5
'c1
9i
i07
qq
95
o?
75
59
101
93
B6
B2
B4
B5
q5
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92
B9
B]
oa
9?
a1
77
B/-
sc
104
B9
9t,
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B2
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2
2
]I
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.l
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2
1
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1
25
59
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1
33
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5l+
27
40
,]
26
5Z
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4
?.4
11
17
1
111+
153
121
122
181
1,47
127
152
176
120
IJJ
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118
t:t
115
15?
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158
163
146
"t59
163
i63
171
MEMBEFl
TakfE
Lancaster Laboratones
2425 New Holland Prke
PO Box 12425
Lancaster, PA 17 605-2425
717-656-2300 Fax [phone] it
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5ee re',erse srde for explanatron oi symbois and dbbrevratrons Rev I 0/lC,'95
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QIJA:ITY CONTR.OL REPORT
Page: 13 of 1t+A Thermo Analytical Laboratory
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HIGH
227
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LLI sample No. 2538L107
Cll-Z JtJD Grab Uarer 9afl)pIe
Hercules: Bacchus Pond
broup No. )zJlJ/
I iiercutes, Incorporated - DE
SampI e
I'tD L
3881 d i benzt,.
3861 benzo
4.
Sar)pI e
UNIIS
(a,h) anthr6cene
ugl t
(ghi ) perytenc
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LCS I-CS LCS
LCS DUP RPD LOU
DUP I'iS
RPO !4S MSO RPDB L.'I NK
N.D.
N.D.
88 36
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Lancaster Laborato0es
2425 New Holland Prke
PO Box 12425
Lancaster. PA I 7605-242:;
717-656-2300 Fax 717-656'2531 5ee rc...re S,da 'o' exp.andr.ol ot syabo , and abb.ev.at,or.
(I)Lancaster Laboratories
A Thermo Analytical Laboratory
LLI samPre No. 2538007
CU-z JUD Grab fJater Sampte
HercuIes: Bacchus Pond
0937 lCL Pesticide:i in Uaters
4592 TCL Votatiles by 82r+0 - Uarer
4678 TCL Sl,J8/r6 Semi vol,ati les/Uatei's
167c) TCL Stj845 SenrivoIati Les/uare|s
Lancaster Laboratories
2425 New Holland Prke
PO Box 12425
Lan(aster. PA 1 1 605 -2425
1 r7 -656-2)00 Fax [phone]
Group No. 522727
i'1ercur.es, Incofporatgd - DE
QLIALITY CONTROL R-EPORT
Page: 14 of ':t+
SUNRCGATE L:}'!ITS
L!',i H I GI,I
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SUR?OG;\TE SUM!'!ARY
TRIAL !D SIRROGATE
TCX
DC8
c4-1,2-DCA
c8-toIuene
STB
2 - F '. plreno L
Fheno L -d6
?,t,,6-lS?
ilitrobz-d5
2-Fbiphnyt-lphenyldl4
60 12060 12C
RECOVERY %
58
99
1t2
91
_s1
tt,
77
72
53
83 11036 115
21.
10
35
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(iI)Lancaste r Laboratories
LLr sample No. EL 2531-fCCVlCottected: 5i?6/96 at 11:40 by BR
Suboritted: 6/29/96 neported: 8/ 1/960iscard: 8/ 9/96
CU-l JUo 6rab l/ater g.inpte
tlercutes: Bacchrrs Pond
CSJUD SDG#: HBP01 -05
CAINO. AIIALYSIS }IAME
inccount ilo: Ll67'16
; tiercutes, Incorporated - DE
i Envi ronrncntai Af fa i rs
i uiLrrrington ,E l9t]94
I
AS RECE IVED
A Thermo Analytical Laboratory Page: 1 of 14
2216 Rev,Or,.n, d,$
P.O.
ReL-
4592
1722
17L3
174\
17t 6
1717,,749
1751
1 a<7
175t+
1755
176i
17o6
177?
7035
7036
0259
0937
1679
170.
15.
2-2
2.7
!,.3
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2.7
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See Page
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See Page
Sce Paqe
TCL Votatites by tJ240 - Uarer
Thattiun
A i. ucr i nulr
Ant i fllony
Bar i um
Beryt tiun
Cad:rri urn
Ch romiurn
Copper
I ron
L ead
Itlanganese
NickeL
5 i tver
Zinc
Arseni c TR
Seteniuflr IR
11e r cury
TCL Pesticides in tlaterd
TCL SlJ846 SrrnivoIati Ies/Uaters
TCL StJ846 SenivoIati Ies/Uarers
Hercules, I ncoarjoratcd
tli!! - RocLy l'lorrrtr in
R.rchel L. Kra.rirrer
0i : iu, : 51 0 liJU2 15 Rti'i10 15-0! rr:_1'1267t,0 Asn0ca
ATI\: fl. - Josetlr Kel I ar
A-Il1: lir. BrenI RDbinton
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Pespectful Ly suhni tted
R"lnrona V. Layman, Croup Leaier
I Ct-' !eta l' 9/Leachatc:;
HETHOO
OETgCTiOlI LII.lIT UIIITSlTE9i.]LT S
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Qucstion:l? Cont.ict ycJr Ct lcnt Selzices Re,gresen!ative
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MEMBEFlTXrE
Lancaster Ldboratofles
2425 New Holland Pike
PO Box 12425
Ldn(astet PA 17 605-2425
7 l7'656-230A Fax: [phone]ee.everse srde Ior e\planat,on oi symbols anci abbrevrdtrons
(l)La ncaste r Laboratories
A Thermo Ana lytica I La bo rato ry ll
ilI
ilSubnritted: 6/28/96 Reported: 8/ 1/96
0iscard: g/ 9/96
CU-3 Juo Grab Uater Sarnpte
Hercutes: Bacchus Pond
C3JUD SDGI: HBP01'05
CAT
1,10. A$ALYSIS llAl4E
ICL VoLatites by 8240 - Uatec
1258 Chtoromethane1?57 Bromomethane3192 Vinyt ChLoride
149t+ Chtoroethane3i97 l.!erhytene c\l.oride
-1198 Acetone3199 Carbon Disur.fide
351r0 1,1'Dichtoroethene3501 1,1'Dichtoroethane
3503 Ch Ioroiotrn3504 1,2-0ichtoroethane
C3 16 2-Eutanone
3505'1,1,1-Trichloeoethanei506 Carbon TetrachLoriCe3507 VinyI Acc(ale
35 08 B l.ofllod i cl] i orome lhane3509 1,2-9ichtoroProPan.'
35'16 cis-1,1-Dichr-o.op,-opene3511 Trichtoroet:rene3512 D'i bronoch Ioromethane1513 1.1.,2-'lrichioroell't3ne
35 15 Berrzene3:10 trans-1,3-DichlolooroPene3518 9rcnroform3521, 4-Iethyl-2-pentancne3520 2 - Her.anonei51l Tetiachtoroethene3523 1,1,2,2-Ietrochloroethane15?1 ToIuene3525 Chtorobenzen€i516 E thytbenzcne3;28 Styrenci529 xy!. ene ( tota [ )5780 trans-1,2-0ichloroetheneirl55 cis-1,2-Dichtoloerherre
LLI sample No. EL 2533CO4Cottected: 6/26/96 at 11:40 by 3R I Account llo: 06715
; qercutes, !ncorporated - DE
r Environnenta !. Ai f a irs
j ,Ji L*ington DE l9B9/.
A9 RECEIVED
.:Ij: r:::::j:::: :j:rfi::.:-:': I'IET H00
iii,sutr!,.,,.:.:r: DETE:i!9ii LIiltT uMs
!,!ii.Ii: .:r::.: j:r,:n .::
:,,, : :::, :.:::::::, t',; :.'ta.:t. :
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Page:
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Rel..
RespectfuL ly Suboi tted
Hic.rc-le llcCl.arin, B-A.
6roup -eid.r, 6Cll/5; Volati Les
2of 11
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Questions? gontact )'ouf Clien!
Rachel r-. KrcaRer
Servi ces Representat i ve
ar (717) 65i,-23C0
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MEMBEFI7mm
Lancaster Laboratorres
2425 New Holland Prke
PO Box 12425
Lancaster, PA 17 605-2425
7 I 7-656-2100 F ax. 7 17 -656-2681 See reverse srde lor explanatron of svmbols and abb.evratrons.2216 Rev l0/10/95
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Account No:06716
r ,iercutes, :ncorporated - 9E
Environruentai. Af f aifs
r lr Lrningrton D'c 19{J9/'
AS RECE !VEO
, . MET TiCD
iTESI.JI-TS OETECI!CIi LIHIT U}I!]S
5of 14
^"r,Orr.r$ d}
P a9e:
LLr sample l.to. EL 2533ryJ4Cof"lected: 6/?6/96 at 11:40 by BR
Suhrri rted: 6/23/96 Reporred: 8,/ 1/96Discard: B/ 9/96
Cu-3 JUo Grab Uater sarnple
Hercutes: Bacchus Pond
C3JUD SDG#: tl8P01'05
CAT
TCL Pesticides in lJaters
P.0.
Ret.
1 600
1 601
i i,rl5
'1o02
160.{
I oC5
1 605
1615
16iD
toal
'c I I
lor)r, lq
U rl5
1tt60
1 151
1t1Z
'16't B
15'r 9
1 ilo
1611
1 i'J)
't623
'1b24
'l .:'15
TZKm
Lanca5ter Laborato(e5
2425 New Holland Prke
PO Box 12425
Lancaster. PA 17 605-2425
7l7-656-2100 tax 717-656 ).681
ResDectfu! Ly Submi tted
..lenifer E. Hess, B.S.
!fD!p ieaCer Pestic ides/PCB:;
See reverte srde lor explandtron oi s/mbols and abbreviatrons 22]6
(I)La ncaster Laborato ries
A Thermo Analytical Laboratory
; Account !lo: 05716
. |iercul.es, Incorporated - 0E
i Env i conrren:a i. Af fa i rs
i ui(nrington 9E 19894
Page:4ol 14
LLI sarnpl-e No. EL 253S0{XCotlected: 6/26/96 at 11:40 by 3R
Subflitted: 6/?g/96 .qeporteC: 8/ 1/56
Discard: 8/. 9/96
CU-3 JUD G|ab Uater Sampte
Hercutes: Bacchus Pond
CSJUf sOG#: tl8P01 -05
CAI!{0. AIALYSIS ]lAl'lE
ICL SU846 Semivotati tes/gaters
3918 ph€not
3867 bis (2-chloroethyl ) erher5871 2-chtocophenoI3383 1,3-dichLorobenzene3334 1,4-dichtorobenrenelB32 1.2-Cichlorobenzene/.69t-l 2-nrethyr,plrenollrj8l 2,2,oxvbis (1-ch'roropcopane),1j8? 4-nrethytpherrol3915 N-nitrosodi'n-propytamine
3!,)02 hexach I o|oetha{te3r'10 ni trobenzane
39C.4 i sophorcne
It)1 1 2-ni troghenoI3890 2,i-dimechyLphenot3866 bis (Z-chloroetroxy) methane
3C86 2,/r-dichtorophenuL39?1 1,2,4-trichlor.oben:ene391)6 naphthatene1d71, (-chtoroani I ine3i00 hexa;h Iorobutadi ene3S72 4-chLoro"3'tnerhy'.Phenoi,i905 2-methylnzrphtha'i.ene
39C1 hexachtorocyclopentadienei(.,?3 2.4,5-rrichLorophenrrL'5gZ? 2,4,5-t.ich!.orophanoIlSfi 2-chtoronaphthalene3i07 Z-ni troani I ineiJ?1 dirnethytphthaLatel3i8 acenaphthytene
ouestions? Contact y'o,J:
RJchal '-. KIu.riret
CL len! Sea'rrces Represcnti:lIlve
a: (7i 7l 65b-21!il
P.0.
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AS RECEIVE9 il
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19/ t
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MEMBEFl
7X-m
Lancaster Laboratofles
2425 New Holland Pike
PO Box 12425
Lan(asler. PA 17605-2425
7 11 -656-))00 Fax [phone]
nespecr:f u: Ly S,rbrni tted
C\r'is:inc I. Ratctiii, B.S.
6 f oup LeaCer, GCll'lS
5ee reverse srde ior explanatron of symbolS and abbrevratrong
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(iI)Lancaster Laboratories
LLI Sampie No. EL 253E/,'C4CoLtected: 6/26/96 ar 11;40 by BR
Sub{ilitted: 6/23/96 !leported: e/ 1/9o
0iscard: 3/ 9igo
CIJ-l JUD Grab later SampIe
Hercutes: Bacchus Pond
C3JLrD SDG#: HBP01 -05
CAT
No. ANALYSIS NAHE ',,. ,
ICL St,,B46 Semivotati Ies/lraters
Accouni No:'-i5716
ierc!Les, Inr::rperrated - 0E
anvi ronmcntr i ;1 ffa ! rs
j rtr lrrrington lE 'l'iS94
AS RECE IVED
:.::: : tlEiHCD
JtESlL]9: DETECT:!N I-!MI'I UN!IS
A Thermo Analytical Laboratory
Page: 5 of 14
2216 Rev ,Orr.rn, dt
Re! -
a.
2.
1r-',.
1C.
;'
t,_
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1.-..
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3879
3894
3395
3887
3u75
3898
l9Lr9
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:4t9
f899
39't5
i917
3859
163/.
3e30
3e97
3?1 9
f870
?caq
3860
1396
j?rll
lii3ljiol
3-nitroaniIine
ac enaph thene
2,4-dinitrophenot
4-nitrophenoI
d i benzofur:n
2,4-dinitrotoIuene2,6-dinitrotoi.uene
diethyL phthaLare
4-ch Lorophenyl phenyI ether
f L uorene4-nitronnitine
4,6 -di ni t ro-2 -methyIpheno L
N -n i trosod i plrenyL anri ne
4-brontophenyl. phenyt ether
hexach I oroDenzene
pentach t oropheno L
phenanth ceie
anth Tacene
carbazole
di -n-buryt phthalate
f I uc ranthene
pyrene
butyl benzyl. phthalate
3, J' -di ch Locobenzi dine
benzo (a) anthracene
bis (2-ethylhexyL) phthalate
c h iysene
Ci -rr-octyL phthat3te
benzo (b) fluoranthene
benzo (k) f L'roranihene
benzo (a) pyrene
inderro (1,2,l-cd) pyrene
Cibenz (a,h) anthracc.ne
ilerl:o ( gh r ) pery i. ene
lJe to iniutiia:ent safl,ple,
seili voL.lt i I.e corrrnounds sr:re
)1..;-
I-:.
it.:,.
*_t-
tl.,_t.
:' :: ;r - -].
thc' cluanr i!;t i )n I I : r :s iot' the I.lCll'lS
rais(.,i-
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Rachr.l !- Kri.r,ni.r
Cl i':nl Se"vrces ?epresentrtlve
ar r "l/) 5i6-?iLl'l
R..::pec t{rL Ly Subrni tlecl
aSriitrne 4- Earc'.iff ,
€.oup -erC.r,5ClMS
5ee reverse Stde for explanatLoo of symbol5 6nd abbrevrdtons
MEMBEFl
TXmr
Lancaster Laboratone5
2425 New Holland Prke
PO Box 12415
Lancaster PA 17 605-2425
7r7-656-2100 Fax 117 61c'26F'
B.S
&&&
LLI sample l{o. EL 25-lSC04
Col Iected: 05/26/9i, ar 'l 'l :40 by 3R
submi tted: 06/2C/96
fU-3 JUD Grab Uater Sa,rpte
tlercuIes: Bacchus Pond
C3JUD SDG#: H0P0'l -05
CATNO ANALYSIS NANE
4592 Tcl- Votati !.es by 3240 - uater
1722 Ihat t ium
1 74i A t umi n,:r
17t,4 Ant irnony
i 745 Bari unr
1 747 Beryt I i un
',71,9 Eadnt iutrr
1751 Chroo)i utn
1753 Coppei-
1751. I ron
1 755 Lead
i 758 Hanganesei761 i( ickeI
176.. Sr lver
1772 linc'1848 t+J SU846 ICP Digcr)t (tot rec)
7A35 A|senic IR
7036 S er- en i um TR
0259 I'lercury
5713 UU SL'845 H9 0iges!
0817 Uater SarnpIe Pest. Extraction
0937 Tcr- Pesircides in uate!'s
0815 EllA uater Extraction!+678 lCL sut46 Se!r,ivo'.ati Ies/r,JateIsr-579 TC. Sf346 Ser;ivol.ati l,es/!areis
i Account llo: 06716
ii'ir'r-cutes, IncL.rpocated - 0E
, Envi ronmentai aifai rs
I Ui imington iE '1989/'
I
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IABORATORY CHRCNICLE
Page: 6 of 14
ANAL Y ST
Susan A. Mclilahon
Donna R. sackett
Donna R. Sarckett
DLrnna R. Sackett
oonna R. sackett
Donna R. SacT.ert
Donna R. S;,ckett
ocnna R. Sacr,ett
tonna R. SackL.lt
lonna ii. sackett
!onna n. SackL'tt
Dcnna R. 9oc)(et!
Donna R, Sickert
Donna R. Silckett' ,onna R. Sacketr
Cnristine I'i. gontin
Donna R. Sackett
Conna R- S.lckett
Ne!!i S. l',!arkaryan
ilc'LLi S. l4a!'karyan
(il)La ncaste r Laborato ries
A Thermo Analytical Laboratory I1
I1
I1
I1
M5] HOD
su-346 r1l40B
su-8{6 6t10A
st-gt6 6J1CA
su-346 611'lA
sr.r-846 6! t 0rr
su- 3,16 6l',i CA
sr.'- 345 5i l LlA
sr-346 6-li!A
S 'J
- rl1r ": 5 l'l 0rr
SU'81,6 /r:l I LrA
s'J-3i6 6J1Crl
su-346 5,11 CA
s.J-s/,6 6l1CA
su'Zhb 6|"'at',
SU-8,{o 6ll0A
::.'-5qo J iulA
s',l-846 bii{-!A
S'J-846 6a': DA
su-316 7/,70A
:^U-846 7-i7!A
sil-845 35108
.ir c/l allr
su-846 35108
su-346 li2716
cr,-a/r t17,_,r
ANAI-YS IS.iR I AL DATE AIIS 'I I NE
1 07/D3/96 C531
1 07/15/96 0345i 07/15/c15 93t 5', c7/',5/96 9345., 07/15/96 A3!.51. 07 / ^.5 /96 a315', 07/15iC6 f;3tt^, 07 / ",5 /96 03t,5
^, 17/'5/9;r A3Li
'. A7 /',) /96 t3t 5'. 07/''5/'1b C345', D7!^,5/9e 13i5I t7/'.,5/96 01t,5". c7/',1/C6'J:4i1 07 / -,
-\ /9t t315't 07 /'.C/qb i???'t c7i1l/9c a3151. 07/j5/9t, C3L5
1 C7/03/96 1911'' 071'-t21c15 2122.
07/01/96 1330 l'larrie A" NataLe
D7/C6/95 A9^,7 Doug'.as 0. Sei tz
C7/c2/96 e93l Maria A. cavenPort
17/at,/9b ciD? l'lark A. Ratcliifg7/14/96 C-\79 I'lar( A. RatcLif f
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Lancaster Laboratofles
2425 New Holland Prke
PO Box 12425
Lancasre( PA 11 605-2425
717"656-2300 F ax: I 11 -656-268 1 2216 Rev ,rr* tfl'
t
5ee reverse stde for explanatron of symbol5 dnd abbre,/rations
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(iI)La ncaste r Labo ratories
A Thermo Analytical Laboratory
Q"]A:]TY CCNTROL RF'PORT
Page: 7 of '.4
LCS LI!ItTS
LOU HIGH
LLr sanpr e No. 25iS0Llul
C'J-l JUD Gr;,b U.,ter 9a,nol-1.
Hercules: Eacchus Pond
Crouc No. 522727herirLes, lncc:lorateo' - DE
Saflpl. e
HOL
Sanlo!. e
uilITS BLANK
I 96',! 84 l AA
DIJP lrts
RP? 'NS FS9 RPD
LCS LCSr-cs ou? RPo
t592 ICL volari t!'s by 8240 - uarer Batch:
12i8 chto|mlethane
l. ug/ t
1257 Brolnolnethane3. ug/ t3t92 vinyl. Chlorrde2. u9/ t
3!.94 chloroethrnel. u9/ L3497 [erhytene Clrl.oride?. u9/ t
1498 Acetone6. u9/ t'
3l,crq Carbon !isrrLf ide3. u-q/ |
350C 1,1-DichLoroethene1. r9/li:c'l 1,1 -9ichLoroethane
?' u9/ !35uli Ch I oroforrr1. ug/t
35il1t 1,2-Dichlorot'thaneZ. ug/ L011(, 2-Sulanone1. u9/ tltt,ti 1 , 1, 1 -Tr ich Loroethane1. ug/Ll:06 Canbon Te:rachloriCe1. us/tiit:7 Vinyt Acetate?- ug,l i15ilil 3roftrcdi ch loIorilethane1' ug'/l1:1.) 1,2-Dl:hLoropropane
1 . ug/'L
3515 cis-1,1-Dicirr.oroprcpene
1 ' uE/'t1t,11 Trichto.oL'thsne1. u!/t
it1 ! D ibiomocil l.orometharre
?' ug/ L
3113 1,'1,2'TrichlorDa!hane?. t-tg7 !
1-<'"i Bclllerle1. ug/llii0 tr:,n:;-1, J'DichLororrlooere1' u!'/l
Lancaster Laboraiones
2425 New Holland Prke
PO Box 12425
Lancastel PA 11 605-2425
717-656-2300 Fax [phone]
77 68
33 91
9C 32
L7 51
b7 91.
7t 72
1.1i " ,_ri
'1 15 ::9
64 97
'I 1 1le
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9t 'cl
97.'
',1:6 I 35
37 99
32 9o
c/' I !2
2215 Rev ,Orr,r* d'}
N.0.
N -ir -
ll ,:) .
N-l-
N.l.
r.l.
N.l.
!i.1.
N,1.
[-D.
N-!.
N.D.
r.t.t.
!i-!.
N.D,
ti.f-
ri.t.
lt.!.
B
B
9
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7
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(I)La ncaste r Laboratories
A Thermo Analytical Laboratory
alLr"fl"].(.
QI-'IALTTY COI'ITRCL RSPORT
Page:
l ac r tvtrc
':0U Hlcli
80 12A
80 120
80 12q
80 120
80 120
B0 120
80 12C
B0 120
3C 120
B0 ..2Q
80 'r 20
3t 120
30 120
q .I
LLI sample No. 25380.(}l
CU-3 Jt.rD Grc'rb l.later S,lnlpte
Hercut es: Eacchus Pond
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LCS LCS
LCS DUP RPD
?1
36
2
26
0
0
)
,l
0
5
I
1 -102
1 107
1 10C
098
197
z 107
9 101
al. 111
1 ',D2
3 101
i ^.0/.
1 100
DUP IlS
RF,,-] I{S MSD RPD
r Group No. 522727
iiierc'Jtes, lr:.o.Do!-ated - 9E
i
Sampte Sarilpteirol ux I is
3518 Bronufornr1. ug/t3521 4-l!ethyt -2-pentanone
5' us/t
35?0 2 -Hexanor)e
7- uslt
3522 TetrachIoroethene1. ug/t
1523 1,,t,2,2'Ietrachloroethane2. trg/ L15?1 To I u..ne2- us/[r525 ch Iorobenzerre1. ug/t526 EthyLbenzene2. u-a/ t:528 styrene
'l ' uglt529 Xy t ene ( tota t )'l ' ug/l,700 trans-1, 2-DichLoroethene2. ug/ L.2L3 cis-1,?-Dichloroetherre2' us/t2 Thaltium'170 . u9/ t,. 3 Aiuminum57. us/t' 4 Ant irrrony15. us/ti Barium?.2 u9/ L.7 BecyLlitrn1.1 ug/t
li49 Caclrnitsn2.7 ugl Il75l Chrolriunr4.3 u9/ t
1 7'53 Copper3-11 ug/t'r',q I ron5.9 ug/t.;> LeaC'18. ug,/L
I i58 l,t.rnqancse?.9 ugl I
1761 Nicketi.l. ugl t
1766 SiLver1.6 ugl t
SLANK
N.D.
N.0 -
N.!.
ti.c.
\.0.
N-.!.
!,1.1-
N -3.
!1.!.
N.D.
N.D.
Batch:951921848102
N.!.
Eatch: 96:92184e302
Batch:96'1921843302
N.D.sarch: 96':921843402
N-9.
Barch : 96'i9?18/,8n1120.C0:o J mglL
nlr^h- CArO?1r.1n'rn?
ii.!.
Srtcrr:96'i9213483C2
t,i .0.
8atcl. : 961921 8!ri1',.102
tl -0.
S.rtch:96192132.3 1C2
0.r_]6ltll J rrrE/ i
3ar.!r : 9bi92'1 5rl]102
Batch:95192181.$902
N.0.
3.rtch: t5192'lBd3l!2
Ii.9.
Batci, : 96192'l 31r3'l'12
li.l-
Lancaster Laboratofles
2425 New Holland Prke
PO Box 12425
Lancaster, PA 17605-2425
7 17 -656-2340 Faxr 71 7-656-268 l
,I
,orrorr, {I
0
0
0
0
0
(1)
(1)
(1)
(1)
(1)
rl)
(1)
(i)
(" )
(1)
(l )
90
93
95
'105
91
1C5
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102
10B
99
102
103
-7?9 (2)
106
ao
97
95
79
- ",4r+1 (?)
C,i
95
't c'1
i2)
Ilie result for orre on both Cetec;rinationJ HaJ tr'ssrira backitrouncl re:jrI r tras mlrc than f our t irr:s tlt.l
iEHfi 5ee reve.se srde lor explanatron ol syroo,s ano dbbrevrdtro.s 2216 Rev
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(iI)Lancaster Laboratories
A Thermo Analytical Laboratory
LLr sample No. 253S0tY
C'J-3 JUD Gratr Uater SdrpIe
i{ercutes: Eacchus Pond
Group No. 521727
FercuLes, !rccrDorateC - 0E
Page: 9 of '.!1
tCS Lli''lllSlol H I cil
8C 120
80 120
on 1rn
30 120
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1772 Tinc12. u9/ t
7035 Arsenic TR2-7 u9/ t
7036 SeteniL'rn TR2.7 us/ |
0259 Mercury
0 .043 us/ t
0937 TcL Pesticides in laters
8 LAIIK
gsrch: 96192'13r,8:!2!.0.
Batch:96192181.S092
N.).
Batch: 95192'1843402
ti.D.
Batch: 9618457'i 310'l!.0.
Batch:961B3CorJrl
Lancaster Laboratorres
2425 New Holland Prke
PO Box 12425
Lancaster. PA 17 605-2425
7 11 -656-23A0 Fax 717-656'2bB l
Dl]P \!S
RP? YS lSD FF'D
LCS !.CS,-CS DUP RTD
c (1)
c (1)
0 (1)
0 (1)
5
,]
'I
0
-41
:?1
79
- iat
,-0?
I3?
79
1C3
103
103
93
1500 Alpha 8HC
0. 002 ug/ t
1601 Beta BHc0.C2 us/L
1C,03 De!-ta BHC0.010 ug./t
1602 Gannn BHC - Lindane
0 .00/, us/ t
1bO1 tleptachtor0.010 u9/t
1t'O5 Atdrin
0. DC4 u9/ t
1606 |leprachIor Eooxide0.031 u9/ !
1616 EnclosuLfan I0.0C3 rig/ ['1610 Dietdr in0.005 us/ |
1607 DDE0.005 u9l t
1611 EndI in0.005 u9/ L
1o15 Endosutfan I I
0.0 1 u9/ t
1o08 0000-qC7 ue/t
1e17 Endr:suIfan Su'i{are0.CC7 ug/t
1C,09 DD T0-C08 uslt
C?iE Endr in Ketone
U.GCt, ug/ |'l8i>0 Methoxych Lor0.01 ug/ t-
llol AIpha ChLoF(lane
0 .0C5 us/ t
116? Garrnta Ch I orciane
0. CD5 us/ t
(1) Iire result for one or both deter'0tinetions xas l.t'ss t1-'an irve tijles t!',e'-0C-
0
1
0
,!
67 12?
7t, 120
69 126
66 120
5t, 1?0
42 120
64 120
60 1?C
66 120
73 129
67 120
5i i23
7"; 120
76 120
57 1{0
75 120
75 120
9C
101
100
92
72
69
92
oo
90
82
.,1.2
97
95
97
93
9i
13i
91
ta
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2
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0
3
1
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95 95
97 97
35 85
76 70
37 80
32 L1
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9.1 39
9?. ?3
q4 92
1CZ "42
91 9C
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QUALTTY CONTROL REPORT
See.everse srde for erplaoaiton of:trbols and abbrevlalrons 2216 Rev l0/30/95
(l)La ncaster Laboratories
A Thermo Analytical Laboratory
QUALTTY COI{TROL REPORT
Page: 10 of
LCS LIM!TS
LoW ti ! G:i
^4 ]t
tt
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CU-3 JLB Grab Ua(ef SarnpLe
Hercules: Bacchus Pond
6roup No. 522727
ileacul.es, lncorpora:ed - DE
SanpLe SampleIiDL UII]TS
Toxaphene1. us/t
Endrin Atdehyde0.U':0 us/ [
PCB - 10160.2 ug/t
PCE-12210.2 us/[
PCB - ',l 2320.2 uS/ t
PC8 - 1 242
0. 10 r,rgl I
PCB - 1 ?480.1 ug/ t
PC8 - '.!254
0. C6 ug/'.
PC3-1250
0. Lr7 ug/ I
DUPh'F3 lils
\19
t:s9 ii,9
LCS i_CS
LCS DUP RPO
92
1613
1518
1 410
'1o20
1 521
1L'JZ
B LANK
N.!.
ri-0.
N.!-
N.3.
u.9.
N.!.
N.].
ti_t-
ll.D.
N.D.
!{.D.
N.l.
N.C,.
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li -D.
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3 TCt- SU846 sefltivotatiLes,'uarers Eatclr: 951841iMC26
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49 17
91 91
33 39
73 82
30 83
7c) s2 .
g1 32
b7 oS
b1 83
1 10 11t
72 7a
q7 97
M :00
91, 95
,./18 phen; I?' uglt
fC57 bis (2-chto|oethyt) ether2- uo/t
3lr7,i 2.chtocopherroI?, t-rg./ tjf.::li 1,J-dichtorobenzene'!- ug/t
:i.,..1''1,4'diclrtor'obenzene?' u!/ L:!'j? 1,2-rlichLor'ube;rzene?. url,/ !l1lpt) 2-t:)e-thytpranoL
i - u!1./ t:.-:r1 ?,?'oxybis (1-chtorop.oParr.)r,. u!/i
/,''-82 4-methytl:irerol
q' u'!/(
1.1 l1; ll-ni rroscci i -n-propyl.-lr:ii ne
4. tc1/L
l;;C2 hexachtr-;roethan.1.. u!/t
l.--:1il ni ttot:c-nzrrne
2. uS,/ t
:t' -!1 ISD;-ll,)r'JI1C'
2- ar/t
191 1 2-rri t:irpn,:rt,t4. ug./ L
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5
l
1
2
!
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a
c
C
t,1
aa
B5
71
77
6!,
ao
101
53
9i,
97
92
5 112
12 158
23 13/+
1 17?
20 12t,
lz 129
t 5 123
3,5 166
5 15?
., 230
t10 111
35 180
21 196
?9 182
,AKIn
Lancaster Laboratofles
2425 New Holland Prke
PO Box 12425
Lancaster PA 17605-2425
717-656-2300 tax 1 17 -656-2681 iI
I,
5ee reverse srde for explanatron of symbols and abbrevratrons 2216 Rev 10/30/95
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(I)Lancaster Laboratories
QUALITY CONTROL REPORT
Page: 11 of ':1A Thermo Analytical Laboratory
LLI Sample No. 25lECC4
Ct/-l JUD Gr3b ilater SalnoIe
Hercutes: Eacchus Pond
Croup lJo. 52?727
eerc;Les, :nccrporated - DE
Sampte Sample
'{DL Uil 1'rS
3890 2,4-dimethytphenol.2' us/ t
3866 bis (2-chtoroethoxy) methane2- u9./ t
3386 2,4-dichtorophenot11. u9/t
3921 1,2,4-trichl.orobenzeneZ- us/t
1906 naghthatene2. ugl I
38t'1 4-chtoroaniIine/+. u9/!
3r00 hexachIoeobutadtene?' u9/ L
3877 4-chtoro-J-methyIphenot1. ugl t
3905 2'uethytnaplrthai.eneZ- ug/L
59C1 hexachtonocyclopentadiene
6 ' ul/|
39?3 2,4,5-tri chLoropherrol2. u9/ t
39?2 2,4,5-trichtoroDhendL?' u9/ t
3873 2'chLoronaphthaLene?' ug/t
3907 2'nitroan!tine2- ug/t
lS91 dinrethyt phthalateL. us/ t3ritB acenaphthylene2. u\/t
LCS LCS
LCS DUP RPD
ouP HsRPD MS HSD RPD
LCS LII!TSLOU H I GH
32 1'!9
33 18/4
)Y IJ)
44 11,2
?1 '1-13
17 116
?4 '116
?Z 1tt7
23 123
1 lnn
5t 144
39 151
60 113
53 143
1 112
33 1t5
7 143
1.7 145
1 _191
1 132
28 131
19 1ie
s0 158
5 LANK
N.3.
u-1.
N.].
N.D.
ri.i.
ll-1.
N.i.
N.).
N.D.
N.9.
0
0
3
0
2
7
1
1
5
I
,1
i
0
1
66 70
90 9C
95 83
7? 7i
61 59
9i 9l
36 B7
51 53
91 90
97 97
i2 il
92 93
65
o/
70
B1
t1
15
91
80
41
q1
90
95
l)
r679 TCL S!J81,6 Sernivolati l.es/!nters Eatch: 90'341JAA026
3908 3-nitroanitineZ- usl L35i7 acen;iphthcne2. u9/ t
3.-l9l 2,4-cini tropltenot!0. us/tiil? 4-nitrophcnoL10. ug/t
3379 di bcn:ofuranZ. uS,/ tia9i 2,4-clirti trotoIuenelr. ug/ l'
3395 2,6-dini tiotolu.'ne2. u9/ i.
7Xm
E0 s0
ct3 93
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95 90
9t 101
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Lancaster Laboratories
2425 New Holland Ptke
PO Box 12425
Lancaster. PA 17 605-2425
717-656-2100 Fax [phone] l See reve.se srde for explanatron oi symbol5 and abbre'lattons 2216 Rev ,Orr.r* d?
(il)La ncaste r Labo ratories
nvl.1 'l'.7mv an }\ITlen r DlTD/-\ Dm
Page: 1? olA Thermo Analytical Laboratory
r,LI sampf e No. 2538C0'4
CIJ-l JUD Gr;.b lJater sample
HerculL-s: Bacchus Pond
Group Io. 522727
liercuIes, Inccrporated - DE
il
ti
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DUP
RP9
SamPte gafilPLe
,.tDt UIi I TS
3887 diethyt phthaIate4. uS/ l
3875 4'chlorophenyl phenyt ether1. uE/ t
3595 f IuoreneZ- trg/ [
3909 4'ni troani I ine
l* . u-o/ t
4681 lr,6-dini tro-2-eethytohenot
1rl . us/ t
3911, N-ni trosodiphenytanrine4. u9/ |
lB59 4-brornr:phen1,t phenyL etherL. u9/ t
3399 hexach t orobenzeneZ. ugl t
3916 gentachtorophenoI2. u9/ t
39'l 7 phenanthceneZ. u9/',
3859 anthracene2. ug/L
455t, carbaloleZ- us/!
3330 di -n-butYt Phthatate2. us/t
3897 f Iuoranthene2. u9/ t
3919 pyrene?' us/l
:'170 butyl benzyL ohthatate4. u9/ t
38ii5 3,3''CichtorobenziCine4' ug/t
33o0 ben?,o (a) anth!'acene2. ug/ L
SioB bis (2'cthyiher.yt) phtilalate4. u-q/ |
357o chr1,s3t,"2. us/ t
3!tt)i, di -n-octyl. phr:haLalet,. u!/t
1351 ben:o (b) fl::oranthene4. ug/t,)\L2 benzo (k) fl-uoranthene!.- ug/L
3851, benzo (3) pyrene4. ug,/tlljol inderro (1,2.3-cd) pyrene
us/ I
MS !4S0
61 65
1e3 _'02
iDz 93
e6 36
67 5/.
8.3 86
33 87
95 9L
9i c)t
?,s s7
92 9C
9D 39
93 9',1
33 B0
79 79
35 35
1,?2 lCi
91 91
'1!i 1 D7
90 sB
q5 95
31 3l
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LC5 LCS L IMI TS
RPD LOU HIG|I
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RPD
LC5
DUPBL,qBK
N.!.
N.9.
ri.9.
(.!, .
[.D.
ri.l.
ri.c.
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N.D.
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285
295
11 90
492
135
289
283
183
292
382
034
1 1C2
090
6 1C4
28e
09d
c 81
132
1 11t.
25 158
59 121
33 12?
38 117
53 127
1 152
14 i76
27 113
t0 137
1 1'!B
?6 137
52 1 .15
1 i52
1 262
JJ iqJ
8 158
17 168
1 116
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11 167
17 163
1 171
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Lancaster Laboratone5
2425 Ne,, Holland Pike
PO Box 12425
Lancasier PA 11 6A5-2425
717-656'2300 F ax. 1 17 -656'258 1 2216 Rev ,rrr* df
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A Thermo Analytical Laboratory
AT'IIT,TMV'N}JMDAT Df.'D^DT
LCS LItI!1S
LO|J H:0il
LLf sampl-e No. 253304V1
CU-3 JIJD Gri,b Uater S3mple
HercuI es: Bacchus Pond
Sanrpr. "- S arnp L e
t'ltrL ulrlTs
dibenz (a,h) anthracenet,. ug/t
benzo (9hi) perytenc.
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LCS DI-'P R2D
9l+
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1 Z?7
1 219
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6 LANK
N.D.
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Lancasler I aboratoiles
2425 New Hollaod Pike
PO Box 12425
Lancasrer. PA 11 605-2425
7l7-656-2100 Fax [phone] ,orrorr, {*}
7L
86
5ee reverse srde for expldnatron oi symbols and abbrevrations 2216 Re'r
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QLTALITY CONTROL REPORT
Page: 1/+ ol
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103
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Group No. 522727
liercrIes, lncorporated - DE
sueRoGArE sultll.lLRY
IRIAL :D SURROCATE
TCX
0cs
d/+'1,2'DCA
cli-roluene
Brg
2-FLphenol.
Fheno I -C6,
?,1,6'r';F
Nitrobz-c5
2 - I'b i PhnT l.
I phr.ny'.d 11r
SUNRCCATE L!I'1ITSLAt) H I 6li
60 12050 120
76 11488 110
P/. 1lq
21 100
lC 12:i
35 11tt
33 1,li'.
TIKM
(I)La ncaste r Laboratories
A Thermo Analytical Laboratory
LLI samPre No. 2538004
CU-3 JUD 6rab Vater Samote
Hercutes: Eacchus Pond
0937 TCL Pesticides in Uaters
4592 IcL Votatile: by 8?10 - tJater
4678 ICL SU8{6 Senri voLati Ies/Uaters
1679 IcL 5U846 Serrivotati Les/\.laterr
Lancaster Laboratorles
2425 New Holland Pike
PO Box 12425
Lancasrei, PA 17 605-2425
717-656-2100 Fax: [phone] Seereversesrdeiorerplanatronoisymbolsandabbrevrat'ons. 2216 Rev 10/30/95
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A Thermo Analytical Laboratory
LLI Sanple No.
col Iecred:. b/?o/96 at
CU-4 JUD Grab Uater 9ampte
HercuIes: Bacchus Pond
C4JtiD 50G#: HBP0I-l0
6/?3/9b Reported: 3/ 1/q6t3/ 9/t)6
/\ccount r.o:357'16
rleIcul.e5, Inigrporated - DE
!r)vi.or.iex(:r. Af ;a i :-s
! i Inri ngron 1l: l9[J94
EL 25-13C09
il+:30 by BP
4592
1722
1744
1746
17t,7
1749
i75',
1 7ii
i75t
1 7:5
1751
70i5
70i6
0259
a93i
4578
4L79
,,71..
5-i.
i-<.
2.2,.j
? .i'
4.3
5 -1)
rJ-
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1t.i.7
2.7
AIIA!YS I S IIAME
TCL Volatites by 8240 - Uatef
ThaItiun
Aluninurn
Ant iilrony
Bar i unt
6eryttitrilt
Cadrni um
CirrDrniuilr
Coppcr
I ron
L ead
ItlanEanese!iicret
gi lver
1l nc
hrseni c TR
9eLeniuut lR
l'.lercury
TCL PesticiCes in llaters
TCL su84a, 9:rivotar i r.es,/Uaters
Ta'- SU8{4. Se:ni vol:r ! !..s/i/ateis
:, J
/':. -i l;'i.
.'?1 .7 i
fi.r.
'ar:5 .:::t_
, 1.i.9., ti-a'.
1 COPY
1CL)PY
Hercul es, I ricorporatec
ELY - Ro.ky )'1ct'.rnta i n
Racha['-. Klaa,incr,-ri:4:,:17 D Oi!-l 15 REP
110 15.00 D)1?57t0 ASRC:0
Respect fuI Ly subnri t ted
Ranrona V- I-ayfllan, 6roup Leader
I CP !'leta Is,/Le.rchate:;
7Xm
Lancaster Laboratorie5
2425 New Holland Prke
PO 8ox 12425
Lancdster PA 17 605-2425
711-656-230A tax 711-656 25E1 See revetse: ce lor exp,andtron ot symbols and dbbrevldlrons 2216 Rev,Orr'r* d3
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(il)La ncaste r Laboratories
A Thermo Ana lytical Laboratory Paqe:
Respec:f uL ly S,-ibmi tted
Hiche:-:- IcC'rarin, g.A.
Sroup l-eacjer, GC/'MS Volat i Ies
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Co[ [ectcd: 6/2;"196 at 14:00 by Bfl
sLrb{fli rted: 6/?3196 Repocred: 3/ 1/960iscard: g/ 9/96
CU-4 JUD Gr3b Uater SampLe
Herrutes: Eacchus Pond
C4JuO SDG#: IIBPC'l - 10
cATNO. AIIALYSIS llAl'lE
ICL Votatites by,8240 - tJater
Ch I oromethane
Eroxloflrethane
Vinyt ChtoriCe
Cll Ioroc-:hane
ii:r.h /1"'n3 Cr tbr i cle
,icetone
Carbon DisutfiCe
1,'!'D ichtoro.'thene
1, l -Dichtoroerhane
tilriorofo;nr
'I , l'D i ch Ioroethane
2-Butrrrone
l,1, I - fri"irlorocthan?
Crrbcn Tetrachlsriiie
VinyI Acc.ta !:
g c nltod i cli i. o.ome thane'l ,2-DichIercproprne
c i s - 1,3-0 icn Loripropene
-rri.htoacar-hanet i i:.rcxioch L oroniethane
1,'1, 2-Tr ich :.oroeanlne
B ii; r:tne
t,- ii ns - 1 , 3 -D ! ch !. oroprcpcne
8,'crrof o tnr
4 -r,lerhyl -2- pentanone
2 - 9eiianone
f e c rach 1.. oe t hef,e
1, !,2, 2 -1 *trachIoroelhane
I u'. udne
Cir L oIDbenzene
E [frytbenzane
5 lyr ene
X/lcr)c (totaL)
tIirns- 1, Z-D i ci: lo|octhena
c i s -'! ,2 -D r ch I arr;e!hrnt'
lA..orn, No: 06716
Hercules, lncrrpora!ed - DE
i Envi !-onmenta L Affa i rs
i lji lrnington DE'19u94
A9 REC3IVED
::::::i:-i:,:::::::.r.:.:::ir::ii:.. :: flETHOD
,;,.ii:i,::,.:if!!l.Ii i'1,,. DEIEcII0!i LIMIT urlITs
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u9/'l
u9/ |
un/ t-
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Lrr/ l
u!'/ I
u9/ t-
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uc-l i
ug/ t'
ug/ ''
Ug/ L
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u9/ t
u9/ \
usl t
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us/'.
uc/'-
ug/ L
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EGMT
Lancdster Laboraiories
2425 New Holland Pike
PO Box 12425
Lan(astet PA 17 605-2425
717-656,2300 Fax. [phone] Rev. ,rrr* dl
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see reverse srde tor explaaatron of symbols dnd dbbre,/tatrons
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(I)La ncaster Laboratories P age:A Thermo Analytical Laboratory
LLr sample No. EL 2533CC9
Cotf.ecred: 6/?b/96 at '14:00 by Bn
Subflri tted: 6/?3/96 Reported: g/ 1/96
Discard: 3/ 9/56
Cu-4 JUD Grab Uater Sarnpte
llercutes: gacchus Pond
CiJUD SOG#: H8901 - 1C
CATrlo. ANALYS IS llAxE ,,:.,;;'
IcL PeJticides in Uaters
Account No: 06716
!'1e.rcul c-S, I ncoegorated
Ervi ronrtcnta: Af ia i fs
!1 lmington lE 1939'4
AS ftEC: IVEO
HET }1CD
'IESILTS OETECT]Or' I-IIIlIT UNITS
P.0.
Rel.
1 600
160 l
1 601
1 oD2
'bua
1 605
1 oD6'16i6
'1.5'l D
1 o07
161 i
161 5
'l oL'\B
i 509
0933
1 360
lo I)
i D18
1o'19
1t?1
1r 22't:?i
'r 5?.1
1L26
ALpha BHcgera BHc
DeI Ta BflC
Cailnra BHC - Lindane
Heptach I or
Aliirin
tleptachIor Epoxide
EndosuI fan I
DiaLdrin
DDE
End| i n
Endosul fan ! I
D0n
EndosuI tan SuI fate
DDT
Endrin Ketone
l'lethokych L or
ALpha ChIordarle
0arora Chtoid-ine
T ox lph ene
Endr i n Ar.dehyde
PC8 -',l 016
2CB-122r
?t9 - i 23?
PCS - i2!,2
PCC'12t,8
PCS - 1 251,
?cB- 1?b0
Due to insufficient
cluant i ration L inri ts.
Lirnits obtainable.
N,D.
ii.l.ti:l.
li:l-
1i ',
0.cc2
0.0118
c. c02
D. CO5
c. c!3
0.:91
Ll -'l0,
C.!05
0"!1
0 .307
c .007i. cc5
0 . L'04
0.03
D .:C5
,l . !'ii
ug/ t'
uct / '.,;g/ I
u9/ I
rs/ |
us/ t
ugi t'
u9,/ i
us/ l'
!g/ l
Uq/ L
uo./ |
u9/ i
UE/ L
url I
u9/ i
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l:l/:
,sc. / ',
Nq/'.
u:1/ I
ug/ !.
,:-a/',
':r/1.u.'/ [
':i/ t
ResPeclful LY Submi tted
Jeni{er E. iless, B-S.
Croup LeaCer P.sticides/PcBs
See relerse srde lor exolanatron of symbols and dbbrevlatrons. 2216
ouest i ons? Cortac I
Rachel !. KTeaflref
7rcm
Lancaste. Laboratofle5
2425 New llolland Ptke
PO Box 12425
Lancasler PA 11605'242"
7 17'656-230a Fax: [phone] ,orrorn, do9Rer
(l)La ncaste r Laboratories Page: l. ol 14 ]lA The rm o Ana lyti ca I La bo rato ry
LLI sampl-e No. EI- 253tC09Cottected: 6/2o/96 at 14:00 by BR
Suhrritted: 6l2Z/96 Reported: 8/ 1/96Discard: 8/ 9/96
cu-4 JUo Grab Uater sanrpte
Heccutes: Bacchus Pond
CI,JUo SD6#: HBP01 - 1C
CATIIO. AIIALYSIS NAI'IE
ICL SlJ846 Semivotati Ies/uaters
3918 phenol
3867 bis (2-chloroethyt) ether
3874 2-chtorophenoti883 1,3-dichLorobenzene
5884'1,4-dichlorooenzene3882 1 ,2 -cli ch t orobenzenet+680 2-rnethylphenoI46il 2,2'oxy'bis (l -ch!.oropropane)i-632 4-rnethytPhenoI3915 tl-nitrosodi'n-propytamine3902 hexachloroethane
39i0 ni trobenzene39C4 i soplrorone-
191 1 2-ni trophcinoI3890 2,4-dim:thyiPhenot3665 bis (2-ch!.oroethoxy) methane3086 2,4'dichi.oroPhtnoLjr21 1,2,4-trichLorooenzene
i905 naph tha I ene1571 4-chi.oro;rniIine
39i10 hexach LorobutaCi ene
337? 4'chloro-3-methyLphenol3,)35 2-nrethytnaph!h3r.enel9Ci her(achlorocycIopentaCiene3ti?" 2,4,6-trichloroPhenoI
3st22 2,4,5-trichloropnenoI1873 2-chtorona.ohthal-ene3,,'07 2-nitroani i.ine
31,91 diilethyt pnthaiate
3318 acenaphthytene
1 A".ornt No: 06716
i llercules, Incorporated
I Envi ronrnenrai. Af f ai rs
I ui i.^ington DE '19894
9E
P.0.
Ret -
ll
iT
IT
AS RECEIVED
i ::j:.:::::::.::::'j::.r:::::::.: :: :: : :::.. :: : :::.:i M E T H G0..:::::i:::.::r:r:.,iESULTS :::1.:r 0ETECI : Llll L ! M ! T UN I IS il
il
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ouest i ons? ContJct
Rachel. r. (reinrcr ycur C I i cn! Su't'vi ces Represen:at i ve
ar (i:7) 656-2i!0
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Lan(a5ter Laboratones
2425 New Holland Pike
PO Box 12425
Lancaster, PA 11 603-2425
7 17 -656-2300 Fax: [phone] l
Respectful. ly 9ubmi tted
Christine il- Ratctiff,
G roup '-eader, Gc/1,1S
See reverse srde lor explanalrcn oi symbols and abbre'/rdtrons 2216 Rev 10/10/95 d
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(l)La ncaste r Lab oratories P a9e:5of 14A Thermo Analytical Laboratory
LLr sample No. EL 2-538C09
col. IectL.d: 6/26/96 at 14:D0 by Gi
suboritted: 6/28i96 Reported: 8/ 1/96Discrrd: 8/ 9/96
CU-4 JUD Grab Uater Sampte
Hercul.es: Bacchus Pond
c4JUo S0G#: !18P01 - 1 0
cAT ::::::::::.1::.NO. AHALYSIS NAI4E ..,:,,.,
fCL 5!846 Semivc'tati tes,/Uaters
Account tlo: 05716
f.ercuLes, Incoaporated
anvi ronnen!.1', Af f a i rs
Hilmington 'E
.:989/'
AS NECEIVED
:::'::.::.1:: .,: METI]oo
?ESJLTS ' DETECT!O:T L!!'IIT UN!TS
DE
P.0.
Rel.
3-ni troani i ine
acenaph thene
2,1 - cini t ropheno I
4-ni trophcnot
dii:enzof uran2,4-iini trototuene
Z, c.-di r,i'.rototuene
Ciethyt phtha[;te
4-chIoropilenyI phenyt ether
f L ucrenelr-nitro:rii L ine
4, 5-Ci ni rro'2 -rnethyl.phenot
ii - ni rroj.od i pheny L a:rti ne
4-!:comopheny l phenyI ether
irexach [,Jrobenzene
Psirrnch IoloPhenot
it.-r enarll h f eni'
anthrac+nc-
cllbalotc
Ci -n-butyl phth3Late
i Luor:in(h:ne
PYr etlet:i.rtyr. benzyt phtha[ate :,.,,,,.,,il,.j'-di::iurobenzidine 'i .. .
benzo ( -r ) anthf eatrne : ..., ..,
Li" (2'ctivlh::(yi) Phth.:l-ate ,,.....chrysene .. . .
cli -n ocryl phthalate :.:
benzo (b) fl-LJorant\cne ,.::lt,'ti::
'Jenz.) (?:) fi.,Jorsnttene ,.'tLenzo ( n) pyrene ....
ir,reno ir,2,J-cc1) pyrcne ...,(llJ,Jnz (a,lt) anitrfacelte ...
b.-n:o ( Jlr i ) pe r )/ L e, ,e .. ..
Cue to insufftc:ent sarp"s, the cuenti !:'-i'n
selrriviL;rt i te cotrtpounCs xu|e tais'-c.
2- ug/L?' r9/l
'10 . 19/ t.
10 . uc)/ t
?. 'Jg/ L
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:' u'l/i4- ug/i1i. ug/'l
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4. u9/ !
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1. u9/ i
a. 'x.)/,.1' utill
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for the 6ClYS
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;r .;.1 .ri-i.
L ir;r ts
ouestionj? C,)n!act yo!r
Raclre[ :. Kre:11'r'Jr'
Cl r:r' S,:ri'ces RL'p|esenietive
!'r :. - -): lll]:. .l l )
MEMBER7Xm
Lancaster Laboratofles
2425 New Holland Prke
PO Box 12425
Lancaster. PA 17 605-2425
717-656-2i00 Fax 717'655 2631
ResPectfuI LY Subrni tted
Ch|istine !- Rarctif{,
GrouP !-eader, GCl!'1S
see reverse srde for expianalron of symbols and abbrevratrons 2216 Rev l0/30/95 d3
It
,9&&
(iI)Lan caste r Laboratories
A Thermo Analytical Laboratory
, Account No: 06716
i Hu.rcutes, IncorDorated
i Envi ronmentaL i1f fa i rs
i uiLmington 9E 19894
i
Page: 6 of 14
LLI sampl-e No. EL 2538009
Co[tected: 0b/?6/96 at 14:C0 by BR
sulxni tted: 06/28/96
CIJ-4 JUD Grab Uater Sample
Hercutes: Eacchus Pond
C(JUD SDG#: HBPo1 - 1tr
CATTO ANALYSI S IIAIIE
459? TcL Votatil.es bv 8240 - Uater
1722 Thal I ium
1743 Atunlirr'Jrtl
17t,4 Ant iarony
1716 Eari un
1747 Becyt I ium
1749 Cadtn i r"nt
1751 Chrorni um175\ Coppu'r1754 I ron
1755 Lead1758 l'langanese1761 NickeL
1766 S i Iver1772 Zinc
1B4B UU SU846 ICP Digest (tot rec)
7035 Arsenic TR70lo SeIenium TR
0259 Mercury5713 U\J Su846 H9 Digest
0817 Uater SarnpLe Pest. Extraction
0937 TCL Pesticides in Uaters
0813 BIA Uater Extraction$7e TCL SUB/'5 SenivoLati Ies,/!Jaters
1679 TCL sil845 Sernivotati Ies/uarers
:'tE1H00
SU-8116 82406
su-316 6010A
s\J-845 6.lt0A
SiJ-546 6l'lCrl
srJ-3/i6 6liDA
s'r - 346 6J1C,\
Sll-945 6i1t;i
si,,-1r,46,5.1'l0A
s,;- a(6 6i'1CA
S\J-346 6-rlCA
stJ-845 6:'10A
su-846 501'-lA
sr - 846 5C',t 0A
su-346 6l'i0A
su-846 or'l'l0A
SlJ-84c,3i105A
su-346 6J10A
sU-Bi6 6tr10A
su-846 7470A
slJ-846 7jr7L1A
su-845 3510S
su-3(6 8t8:
su-816 35'l0D
s!.,r-846 SITCE
Sll- 3/*6 tJ.:TCS
ANATYS I S
TRIAL DAIE AI'IO IIT,!E
1 07/03/96 091tr
1 07/15/96 C107' 07/.,5/96 0407' 07/i5/96 t:117
i a7/15/95 t4071 07/'^,5/96 !4r71 07/15/96 CQ71 D7/15/96 t1a71. D7/i5/96 Cq'J7
', 07/'i5/96 D1l71 07/',5/96 A4D71 07/'t5/96 C4071 07/15/9a t4r71 07/15/96 e1071 A7/15/95 C4C71 07/1C/96 1?221. A7/15/96 C1n7': 07/15/96 A407
1 07/03/96 192?1 07/0?/96 ?1?2
1 07/01/96 1330't 07/06/96 i0?6
1 07/0?/96 CgiD1. C7/04/96 16"1i 07/0t,/96 cb17
ANAtYST
Tracey Neff
oonna R. Sackett
Donna A. Sackett
Donna R. Sackett
0onna i?. Sackert
oonna R. Sackett
conna,Q- S.rckert
Donna R. S.lcKelt
Donna R. S.1ci'.L.tt
Donna R. Sackert
Donna R. Sackett
Donna R. Sackett
Donna R- Sackerr
Donna R. Sackett
Donna R. sackertChristine 14. Conlin
Donna R. sackett
oonna R. sackett
Nel !. i S. MarkaryanNelLi S. Hankaryan
I'iarcie A. l'latate
Dougtas D. sei tz
Maria A. Davenport
Mark A. RatcLiff
Mark A. Retc L i ff
iI
1l
,l
il
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MEMBEFl7Xm
L:nca5ter Laboratofies
2425 New Holland Prke
PO Box 12425
Lancaste( PA 17645-2425
717-656-2100 F ax 7 17 -556-2631 ril
I
I
I,AEORATORY CHRONICLE
See reverse srde for explandtlon oi symllols and abbre'/ratrons ))16 Re, 1A/3O/95
I
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(iI)La ncaster Laboratories
1
t, Group No- 52?.727
llercutL's, Incorporated - DE
QT.IALITY CONTROL REPORT
Page: 7 of 11
LCS LIMI-I"S
tOL, H I CH
A Thermo Analytical Laboratory
LLI sampl-e No- 2538009
CU-4 JUD Grab Uater gample
HercuIes: Eacchus Pond
Sampte Sampte
Tlqt UN I IS 6LANK
t59? llt Votati tes by 8240 - rrater Barch: 196,i841.A4
MS
HSO RPD
DUPEPD MS
LCS I-CS
LCS DUP IIPD
l:58 Ch loromethane3. u9/ t
1257 Bromomethane3' ug'/L
3t9? Vinyt ChIorideZ. uq/t
3!9/, Ch toroethane1. us/ t
3497 Herhylene Chloride2. u9/ t
1498 Acetone6. uS/ t
34?9 Carbon Disulfide3. u9,/ t
3500 1,1-DichtoroethenE1. uglt
3501 1,1'DichIoroethaneZ. uq/l
3501 Ch I oroform1. ug/t
3504 1,2-Dichtocoethane2. u9/ |
0316 2-Sutanone3. ue./t
3505'1,1,1-Trtchtoroethane
'1 . ilg/ L
i505 Carbon TetrachIociCe1. us/t
3507 Vinyl. Acetate2. ug,/[3tte. BroncCichtorolnethane1. ug/t
3',05'1,2-DichIoropropan.'1. ug/L
3516 cis-'1,3'DichloroproPene1. ug,/t
3511 Trichtoroethcne1' rglt'35i? 0ibrcmochLorolnethaneZ. us,/ t
3511 1,1,2-Tiichioroethane?' us/|
35 1 5 Benzcne1. ug/L35'i0 r:rans-1,3'DichLoropropene1. ug/L
N.3..
ri.D.
r.t.!.
N.!.
ri.9.
N.D.
N.9-
N.D.
N.D.
i1.9.
N.D.
N.D.
N.D.
N.D.
N.!r.
N.D.
N.9.
8
I
I
3
3C
l+
7
l
4
4
l+1
?
1
27
5
2
4
1
1L
16
0
12
e3 8l
90 82
bt b I
icz 9B
75 7?
1 1r, 106
103 100
115 109
96 100
6r, 97
1 16 114
11t 110
3/. 1i0
99 101
98 101
97 i01
1u6 1 C5
s7 9e
8Z 96
1rr1, 1 04
91 102
,MIn
LancaSter Laboratories
2425 New Holland Prke
PO Box 12425
Lancaster PA 17 605-2425
717-656-2300 Fax [phone] See rev.,se rroe lor plplanalron ol t76gq,5 ard ,bbrev,a,rons 7ll5 Rev ,nrr.rn, dtP
'Il
o La ncaste r Laborato ries
A Thermo Analytical Laboratory
QI:]ALITY CONTROL REPORT
Page: 8 of '.1
I tvtYc
HI(]iI
]t
Il
]l
Il
il
ilLLI sample No. 2538009
C',J-4 Juo Grab i.';'ter Sampte
llercutes: Bacchus Pond
Group No.522727
llercutes, I ncorporated DE i
I
I
Sarnpte Sarnpte DUP.[,tDL UNITS BLANK IP' US M9D
f5 1 I Erornoform1. ug/t N-0. 71 90
1521 4-t4ethyt-?-pentanone5. us/t N.D. 65 93
352C 2-Hexanone
7 . us/ t N.). 62 95
3r?2 Tetrachtoioethene
1 . us/ t ri .9 . 106 105
3523 1,'1,2,2-TerrachLoroethane2. ug/t N.l. 77 9ri
:421, Totuene?. ug./t N.C" 'lC'5 105
'25 chlonobenzene1. ug/t l;.9. 'l0l 101:t:o Ethytbenzene2. ug./[ N.D. 11C 109-:28 Styrene1. ug/t N-'r. 1D2 iC?,29 Xylene (to(al)
1. us/t u.)- 103 lCB
730 trans-1,2-cichtoroethene?. us/ [ N.D. '104 99
.'58 cis-'1,2-Dichlocoe!hene2. ug,/L N-!. 1C6 102;-Z Thalt irrm 9atcn: 96''192'1343C02170. ug/t {.D. (!) lC1 103
,.:i rtumin,.Irt gatc5: I)6'192184:1002
57. r-rsll N.!. 17/. '772 -729 (2)
.:,:,i Anrimlrny Batch:96192184si10215. LrE,/[ ii.9. (!) 105 i05
iTl,L Brritm Batclr: 96i92'181t80022-2 ug,'t [-]. 0 (1) e7 88
17i? BeryitirLn Batch:96'19218/'!3Cz1.1 ug/L 0.LrC1,i J nr1r,'l (1) 97 97
'71.t cli]mi'ri Batch:96i9?13/,110022.7 u!l/t N-0. (-1 ) 91 95
17)'l rthrcnri,-rn aiich: 961921818']C21-3 uslt lt.D- 0 (1) 73 79lrq? c,\^dr.. Br,.ch:9,619218;,31!2.: rJ ettPl,vt3.3 us/t N.c. 0 ('1 ) -201 -191
., i{ I i^orr 0atch: 9619119+x'la?5.9 ug/l 0.06[)7,.1 'r]i'.il 174 -1513'14t+1 (?)
1:i5 tead Betch:9"19213ii1ri02
18. rrs/t i,l.D. 0 (1) 92 93' 55 t.lrngan.ise S,:tr:h: 9oi92'13u.:1'-t022-9 Lr!./t N.l. 0 (1) 5t 61
t7i.1 NickeL B.ltch:9r,19?]8/,31125.4 u9/ L tr.5. 0 ('1 ) 9t, 95
'..r1, Siivcr Bi,tch: ()b192181 n'llrz
\-b rlg./t 1i.0. (,1 ) 99 101
il) The result fcr orre 6r b0th deLernin3tionl; lcs letis than five tiles the r-Oc.
l:l) Tiie becl:3ior.rrrl resJIt !as more t!-,::n four tintes t:i,j spil(L'added.
Lancaster Laboratofles
2425 New Holland Pike
PO Box 12425
Lancaste( PA 17 605-2425
7 l7-656-2100 Fax: [phone]
llt
EP!
LCS !-CS LCS
LCS DUP RPD LOU
24
36
?
?6
0
0
2
1
0
5
I
1
1
1
0
,l
?
9
1
J
1
1
't 02
1C8
107
100
98
97
107
10',1
111
102
103
104
100
80 120
B0 120
80 120
30 120
80 '120
80 120
80 120
BC 12C
B0 120
80 120
80 120
80 120
80 120
it
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(l)La ncaster Laboratories
QUAL]TY CONTRCL REPORT
Page: 9 of 1t,
A Thermo Analytical Laboratory
I
LLI sample No. 2533009
CU-4 JUD Grab Uater SanrpLe
Hercutes: Bacchus Pond
I
I croup No. 522127
I itercuLes, inccrporated - DE
II
!
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Sarpte SampleMDL UIII IS
1772 Zinc12. uglt
7035 Arsenic TR2.7 u9/ t
7056 Seleniurn TR?.7 us./ L
0259 Mercury0.0t+1 u9/ t
0937 TCt Pesticides in lJaters
EI.ANK
Batch : 96'1921843r-r02
N-!.
Batch:96i921843Jc2
N,D.
Batch: 95'i9218i81C2
ti.D.
Batch: 961345713101
lt.D.
Ba rch : 961 830005,\
N.1.
ll !.
N.t.
N.9.
N-9.
ti.D.
N.!.
N.9.
N.9.
il-0.
N.D.
N.D.
ft.D.
N-D.
N.!.
N.t.
0 (1) -r+1. -34
n /1\ 1n1 1n)
0 (1) '101 102
c (1) 79 79
8,5 36
96 95
97 97
95 85
76 76
rc to
oa ot
92 8l
83 83
113 1',I/.
90 91,
90 39
92 93
'91 92
o/. a,
1C2 1C2
91 90
e6 86
times the Loo.
LCS
LCS DUP
OUP IlS
RPD IIS MSD RPD
1
0
103
101
101
!.CS LCS LII'IITS
RPD tOU HI6H
80 120
80 120
80 120
80 120
1600 AIpha 8HC
0 .002 us/ t'1601 Beta BHC0.003 u9/ t
1C,03 Det !a BrlC
0 . LrLl5 ug/ L1602 Gaflnra BHC - Lindane
0 .002 usl t
1 504 Hept ach L or0.CC5 u9/l
1505 Atdrin0.004 us/ |
1606 HeDtach Ior Epoxi de0.0C1 ue/ t'1615 Endosut f an I0.00l u9/ l
1610 Dietdrin0.0C5 ugl L
1507 D0E
0 .009 us,/ t
ILII LI]OTIN0.00i ug/ t
1615 EnrJostrtfan I I0.01 u'J/ |1608 DC,o0.007 usl lli17 Endosut fan Sut fate0.007 ug./ L
1609 DDl
0 .0C8 us/ t
0918 Endlin Xetone0.004 u9/ I
181C ltethoxychlor
0. 0l u9/ [1361 AlDha chLorcJ3ne0.005 u9/ t1362 Ganilla chLorCane0.005 us/'.
090
1 10-1
0 10c
092
172
169
, nq
090
082
3 1",2
197
195
0 97
393
294
1 ',101
2 91
086
67 1??
74 1?0
69 126
66 120
54 120
t+? 12C
61 120
60 120
66 120
60 120
T3 129
67 12C
67 121
53 128
76 120
57 140
75 120
75 i20
('l) The resutt for one or borh dererminations was tes; than flve
MEMBER
TaXm
Lancaster Ldborato0es
2425 New Holland Prke
PO Box 12425
Lancaster. PA 17 6A5-242')
717-656-2300 Fax [phone] See reverse srde for explanal on of symbois and abbrevratrons 77 l6 Rev ,arror$ d?
il3Ja(f
QIJA.LITY CONTRCL REFORT
Page: 10 of
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(I)La ncaster Laboratories
A Thermo Analytical Laboratory 14 ll
LLI sample No. 2538009
CU-4 JUD Grab Uater Sampte
Herculcs: Bacchus Pond
Sarnpt e
MDL
SampI e
UNITS
l51l Toxaphene1. us/t
1518 Endrin Atdehyde
0.01 0 u9/ t
1619 PCB-10160.09 u9/ t
1620 PCg-12210.2 ug/ t
1621 PCB - 12320.09 ug/ L
16?2 Pcl-1?t,Z
0. 05 us/ |
16?3 PCB-1268O.Cl ug/ t
1621 PC8-125i0.06 u9/ t
1b26 PcB - 12500.07 usl t
39 -t B phc.no L2. uS/t
3807 bis (2-chtoroethyt) ether
2. usl t
337( 2-chlorophenoI2. u9/t
3383 -1,3-tlichtorobenzene2. uglL
3aB1 1,4-dichtorobenzene2. uglt
-r332 1,2-dichIorobenzeneZ. u\/L
1630 2-methytphenoL4- us/t!.L!\1 2,2'oxybis (1 -chtoropropane)
4. uS/ [
1L8? 4-nEthytphenoI1.. uglt
3915 N-ni trosocll -n-propyLanri ne4. us/ t190: hexach Ioroethane4. ugl t
39'10 ni rrobenzene2. ug/t
190/t i sophorone7. us/ [
3911 2-nitrophc'ncrt1,. u9/ L
; Group No. 5227?7
I hercutes, in.ocDorated - 0E
i
;il
LCS LIi{!TSr_ou i{ I Ga
I
2216 Rev,OrrOrr, {l
ouP its
RP' I,IS I'!SD RPD
LCS LCS
LCS DlP RPD
-5lS lCL 5!346 Semivotatiles/Uaters Batch: 96184HAA025
GLANK
N.D.
N.D-
N.D.
N.D.
rl.D.
N.9.
N.9.
N.D.
N.9.
N.9.
NaD.
N.D.
N.9.
N.!.
N.D.
N.9.
N.).
I.D.
!{.!r.
I-D.
it
il
il
rl
T
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5 112
12 158
?3 13i+
1 172
20 124
3? 129
16 123
36 166
5 152
1. 210
40 113
55 180
2', 196
29 182
3 Lr1
-1 88
185
568
370
371
177
?64
078
4 103
853
0 9/,
a97
19?
t9 47
91 91
gs 39
7A O'
an aa
79 82
or a)
67 68
83 83
1]0 11(
aa 19
97 97
100 10c
9t 95
MEMBEFI7x-iil
Lancdster Laborato(es
2425 New Holland Prke
PO Box 12425
Lancaster PA 17 605-2425
7 I 7-656-2100 F ax 7 17 -656-2631
I
See reverse srde fo. explanatlon o{ symbols and abbrevutions
I
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(l)Lancaste r Laboratories
QUALITY CONTROL REPORT
Page: 1 'l of 1 l|A Thermo Analyti ca I La boratory
GLANK
N -!.
N.!.
N.3.
N.D.
N.3.
N-0.
N.D.
N.9.
t,i.).
IJ.D .
N.D.
rl .l-
N.D.
N.9.
i.!7.t'itt- SU84c Sadrivotati tes,/'Jiters Batch: 96184!.1/.(rl5
LtI sample No. 25330L\9Cl-4 JUD Gr:b 'Jater safipLe
HercuIes: Bacchus Pond
Sampte Sampte
FDL u[!Is
2,4-ditrrethytphenoI2- ug/t
bis (2-chioroethoxy) methaneZ- u9/ [
2,4 -di ch t orophenoI1. uS/t
'1, 2, 4- tri chtorobenzene2. ug,'t
naphthaLene?- ug/t
4-u:hIorcani i ine!*. ugi t
he;rach lorcbutadi eneZ. u.1/ [
4 - ch l. oro-3 -orethytphenoI
4. u:./t
2 -methylnapl-r tha Lene?' u'l I
herach I ococirc t open tadi enc6. Lrg,i I
2, /,, 6- tri chl orophenol
2 ' ugi'l
2,1,, 5 - rr-r ch Lorophenolz. ug.'|
? -ch l. oronirplrt ha t ene2. ug/ |
2'niiroanil.ine?. trEr".
dirlerilyL phthalatL.
6. u:1./ |
acen.ii,hth/i.ene?' ug/ |
I
j cloup uo. 522727
iHerc'..:les, Inaoeporated - DE
I
I
90 90
?6 36
79 31
33n 33
72 74
65 69
93 93
51 53
39 87
89 88
91 9C
97 97
32 l1
9? 9i
ec 3c
9i 93
47 1+5
q5 e6
9q 100
LCS tCS
LCS OUP RPD
DUP IISRPD MS MSD APO
LCS LI[lITSLOU HIGH
32 119
33 13!+
39 ]35
4/, 1/.2
21 133
17 116
2t, 1 16
22 147
23 123
1 ',100
5l lri4
59 151
60 1 '18
53 143
1 112
3t '1{,5
1r7 1/,5
1 19'l
1 112
23 1ll
l9 110
50 158
7
0
C
J
0
2
1
1
,q
l
1
1
0
1
2
65
B6
8l+
7A
n1
73
g1
80
4t
91
90
B8
95
25
36
jr.:rJ 3-nitroaniline
?' ug/i
i::5 / acenaiphth.'rre
Z. ug/ i
-'i93 ?,4-dirri tr'ophenoL
]u. u."l t-
:i ,Z 4-rti trophrnuI
lA. ug/L
:;.r,,'q cli b+n:oiur.irr
) ,.. _,1
jj9:r 2,4 -ii ni:rotc!.uene
11 . ui,/ t
lf?5 2,6-dini tr.rtol.uene
2. tl/t
1
0
1C
5
1
,]
1
BC
92
55
35
94
95
MEMBER
7X-m
Lancaster Laboratones
2425 New Holland Prke
PO Box 12425
LdncasteI PA 17 605-2425
717-656'2100 Fax: 7 I 7-65o.253 1 ,orrorrt d?)ee rp\e.)e \ qe tor e.old.dlron ol \y loor! aoo dbbre ldl,orrs 2216 Rev
jt
{lLf,3Jrr.
Q'-IALITY CONTROL REPORT
SanpLe SamPte
I.{Dt UN I'IS
3887 diethyt Phthatate4. uO/ t
5875 4-chtorophenyI Phenyt ether
1. u9/ [
i898 f tuorene?. u9./ t
3909 4'ni troani t i ne1. us./t
4683 4,6-dini tro-2-rtrethytphenoI
10. u9/ t
3914 il -ni trosodi phenyIanri nc'l.- ug/Llf59 4-brornophenyI Phenyt eth.'r
l, . u9/' i
;;?9 hexachLot.obenzenez. ug,/ r-915 pentach t oropheno I
Z. us/L)17 phenanthreneZ. us/li359 anthraceneZ. ug/t
1684 carbazoIeZ. ul/L
1880 di -n-butyt PhthaIate?. ug/t
3897 f I uoranthene2. Ltgl L39'i9 pyrene?- ug/ t
3570 butyl benzyl PhrhaIare1. u9/ t
3835 3,3' -dichLorobenzidinel.- u9/t
1a50 benzo (a) anthracene
?. us./ t
lurt bis (2-ethyiher.yL ) phthaIate
4 . tig/'.
3876 chrysene2. us/ L
3396 di -n-octYL Phthatate1. tJs/ t
39b1 benzo (b) fLuoranthene4. u9/ t
)152 benzo (k) ftuoranthenet+. u9/t
1364 benzo (a) Pyrenet,. u9/ t
59Cl indenc (1,2,3-cd) PYrene4. u9/ t
BLANK
Lancaster Labo.atofleS
2425 New Holland Prke
PO Box 12425
Lancaster PA 11 605-2425
717-656-2300 Fax [phone]
II, Group Io. 5227?7
: Hercul.es, Inco.porated - DE
i
i
6t+ 65
103 '.,02
]02 98
86 86
67 54
83 36
33 97
96 9!,
1,5 l+A
95 94
88 87
92 90
89 37
90 89
91 9',1
79 79
8r" 85
102 101
9'1 9',1
100 107
95 95
Da o?
76 75
Page: 12 oi 1t+
LCS LIIiIITS
LOU H i Gi1
?s 158
59 121
33 12?
1 181
33 117
>3 tl(
1 152
1t, 176
51 120
II IJJ
40 137
1 118
26 137
\2 115
i 152
1 262
JJ Iq)
8 153
17 168
4 iqo
24 159
11 161
17 163
1 171
<D Lancaster Laboratories
A Thermo Analytical Laboratory 1l
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II
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LLr sample No. 2538C09
CU-4 JUD Grab Uater sample
Hercutes: Bacchus Pond
OUP iqsRPD I45 T1SO RPC
I.CS LCS
LCS DUP RPO
259
I 10i
498
086
582
a olt
285
295
'r1 90
a92
185
289
283
'r 88
292
? n,
277
031
1 1.9?
090
6 i04
289
094
0 31
'1 82
7A<m 5ee re./e,se srde for exptdnatron or 5vmbols and abbre rratrons 2216 Rev 1 0/10/95
t
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I (I)Lancaster Laboratories
t
I
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I
I
I
I
I
I
I
t
I
I
LLI samp1e No- 2538C09
CU-4 JU0 Grab Uater Sarrrpte
Hercutes: Bacchus Pond
i tiroup No. 522727Ir'1r.rc!tes, lnccfooraleci - DE
A Thermo Analytical Laboratory
QL'AL]TY CO}.ITROL RNPORT
Pa-oe: 13 of ' t
LIMITS
ttt
219
SanpLe gampLe
MOL UIIITS
1381 dibenz (a,h) anthracene1. us/ t38i3 benzo (ghi) peryIene
l. . trg/ [
LCS LCS LCS
LCS DUP RPg LOI'
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Lancaster Laboratofles
2425 New Hotla^d Prke
PO Box 12425
Lancastei PA 11 505-2a25
717-o56-2atA Far 717 5!6 253'
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2425 New Holland plke
PO 8ox t2425
Lan(asret pA 17 605-2425
7 17 -656-230A tax I ti -656-26A1
Group No. 522727tlercutes, !,.]co.Dorated - 9E
SURRCGAIE SUII^IARY
TRIAL ID SURROGAIE RECOVERY i'
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Hercules: Bacchus pond
QUAIITY CONTROL RIIPORT
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TCL VotatiLes by 8240 - Uater
Thail.itll
A l. run i nurrt
Ant i mony
Bar i unr
BeryI t i unt
Cadnriurrr
Chrorni unr
C cppe r
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L ead
f'langanese
NickeI
Si Iver
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it;er cu.y
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Rachi.l. L. Kt'e:rrrrer
03:49:41 D OaJl 15 REP
310 I5.00 0012671'C ASiIILTU
Sefvi ctrs. ?eDrcsentat I ve
31 (7',i) 65.r-31'l!
1./ .t- <1aa')-
MEMBEFl7Fil
Lancaster Laboratories
2425 New Holland Prke
PO Box 12425
Lancasrer PA 11 605-2425
717-656-2300 Fax: [phone]
?espec:fuL Ly Subrni tted
il:(t!ana V. Layrnan, Croup Leacier
!iP fetaLs/r*eachates
5e* re;e.se stde for e(planalron of symDol5 and abbre,/tatrons 2215 Rev l0/30i95
La ncaster Labo ratories
A Thermo Analytical Laboratory
LLI Sample No. EL
Cottected: 6/?6/qd at 14:30
subli tted: 6/28/95 Reported:
Discard: Bl 9/96
OutfatL JUD Crab Uater SamP[e
Hercutes: Bacchus Pond
OUTFJ SOG#: HBPO1 - 1 2
CAT
}IO. ANALYSIS NAHE
'cL Vol.ati Les by 8240 - Hater
Ch t oromethane
B romorirethane
VinyL Chtoride
Ch Ioroethane
l.lethytene Cltoride
Acetone
Carbon DisuIfide
'i ,1 -Dichtoroethene
1,1 -DichIoroetnane
Ch Lorof orr,t
'l ,?-Dichloroethane
2 - But anone
1, 1,'1 -Tri chloroethane
Cacbon Tetrachtoricie
VinyI Acetate
Bronrodi ch I oromethane
1,2-Dichtoropropirne
c i s - 1,3-0i ch toropropene
Trrchtoroethene
D i brorrroch I oroolL'thane'!, 1, 2-Tri chi.oroethane
E enzene
trans -'l, 3-D i ch I oropropene
E lonrof ornt
4-HethyL'2-pentanone
2 - llexanone
Tetrachtocoethene
1, 1,2, 2-Tetrachtoroethane
ToIuene
Ch I rrrobenzene
E thytbenzene
S t yrene
Xytene (totat)
t rans - 1, 2-D i ch tocoethene
c i s - 1,2-C, i chtoroethene
g/ 1i96
Questions? Contact yoLlr
Rachei L. KTi:allL'l'
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253801 1
by SR
Page:2ol 14
' Account No: !5716
'HercuIes, lncorporated - DE
I Envirornlentat Afrai rs
! ,;i Lmington DE .19894
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AS RECEIVED
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I 258
1257
i492
5494
5i,97
5498
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5500
350 1
1501
55 D4
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3505
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35 rl7
3508
3509
35 t5
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Lancaster Laboratories
2425 New Holland Prke
PO Box 12425
Lancasler, PA 17605-2425
717-656-2300 Fax [phone]
RespectfuL Ly Submi tted
!!iche!.e i/cCLanin, B.A.
Group .eader, GC/'MS Votati Ies
See reverse srde for explanatron of symbols and abbrevratrons 2216
I
I (iI)La ncaste r Laborato ries Paqe: I of 14A Thermo Analytical Laboratory
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LLI Sample No. EL 253301
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I A]TALYSIS NA,,,!E
I:Account llo: C6716
, Hercutes, Incarporated - DE
i !nvi ronmenra L Affa i rs
i tJi lmington DE 19894
I
AS I?ECE I VED
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at (/1 7) 6:io-23Ctl
MEMBEFI7Xm
Lancasler Ldboratories
2425 New Holland Prke
PO Box 12425
Lancaster PA 17 605-2425
717-656-2100 Fax [phone] r-e ."...:e stde for exoldndtron of symoo s and abbrevratrons 2216 Rev lano/s5 dt8
La ncaste r Laborato ries
A Thermo Analytical Laboratory
253301 1
by BR
8/ 1/96
LLI Sainpl-e No. EL
Cot Iected: 6/?6196 at -14:30
Subori tted: 6/23/96 Reported:
0iscard: B/ 9/96
OutfatI JUD Grab Uater SamPte
Hercutes: Eacchus Pond
oUTFJ SDG#: HBP01 - 12
AI.JALYS I S NAI'IE
'CL SUB46 Semivotat i tes/Uatecs
t91B phenot
\967 bis (2-chtoroethy[) ether
,B7t+ 2-chLorophenoI
5383 1,3-dichtorobenzene
5384 1 ,4 -di ch Lorobenzene
iti32 1.2-dichIocobenzene
1680 2-rriethYtphenoli6B1 2,2'oxybis ('l-chtoropropane)
t,68,? 4-irrethytonenoI
i915 N-ni tros:ocli -n-propytanine
3902 hex"rch Iot oethane
39'10 nt rrobenzene
19,04 i scphorone
39'1 1 2-nitrophenoI
l3?0 2,4-dimethyLphenoI
i366 bis (2-chloroethoxy) melhane
-1880 2,4-dichIorophenoL
39?1 1,2,4-tricnlorobenzene
3A06 naphtha iene
3871 4-chtocoani t ine
3900 hexaclrtorobutadiene
787? 4-clrtoro-J-nrethytPhenoI
i905 2-methytnapi-rthai.ene
i901 hexachiorocyctopentadiene
3q23 2,4,6-trichLorophenot
i9?? 2,4,5-trichloroLl,-,enoI
3313 2-chLoronaphthalene
3ct07 2-ni troani I ine
33al dinrethyt phrhatatu'
3!-(3 acerraplr rhy I ene
i /rccount xo: ur6716
i tiercutes, !ncorporated - DE
! [nvi ronrnentai Aft'a i rs
I ililnrin9:on DE i9894
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Rachel. L. Xrcarriel
yor:r C L i enl Servi ces RepcesL'ntat 1 ve
a: (t'",7) 6i5-2100
MEMBEFt7Xm
Lancdster Laboratories
2425 New Holland Pike
PO Box 12425
Lancaster, PA 17 605-2425
7 17 -656-2)0A Fax 7 1l -656-2631
ResDcctf ut iy Sutrlni tted
Chr;st :nr' I'1. :?arcL iii,
Gr-oup -eader, GC/l'is
5ee reverse srde tor explanatron of symbols and abbre'riatrons.2216 Rev
i
I (iI)La ncaster Laboratories
l;,T:::,''
ILLI Sample No. ELCutIected: b/25/96 at 14:30
6/?B/96 Reported:B/ e/96
ANALYS t S NAI,,!E
I,::::: :.:",::::.:":::.'""' "
CUTFJ SDG#: HBP0l - 12
I Account No: C6716I HercuLes, !ncorporated - DE
I Envi ron,nentaL Af fai rs
I 'Ji trni ngton iE l9B9/+
I
I
RECE I VED
H E T i.iOD:' DEIE:TlCri Ll!'! lT UIIIS
A Thermo Analytical Laboratory
253801 1by 8n
B/ 1/9o
Respectfut Ly Subrni tted
Chiistine !1. Ratctitf, 3.S.
C roup !-eader, GC/l'1S
Page:5of 14
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* :;:$;;iH""3393 2,1-dinitrophenoI7912 4-ni troohenoL
]g di benzo'f uren
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5!.t')) l,o-drn: tf o:oLuenL.
3{lE7 diethyt phthatate
f5 4-chLoropirenyl phenyL etherDs f luoce.ef,C 4-nitroaniIine
468i 4,5'dinitro-2-nethytphenoI
fti xi*iili,i:f"irr*ri'i'n"'3q17 phenanthrene
ffi i?,:!;:li,ph,ha,are
3897 f luorantherr.'
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ouest i ons? Contact youn
Rachel. L. Krearrier
Client Servicesar (7 7)
Recf esentafIve
65o - 2,iC0
MEMBEFIzkm
Lancaster Laboratones
2425 New Holland Prke
PO Box 12425
Lancasret PA 17 605-2425
717-556-2300 Fax [phone]ee reverse srde tor explanatlon of rymbols and abbreviations 22l6 Rev 10/3ot9c,
I(&
253E1j11
by BR
Hercules: Bacchus Ptrnd
oUTtJ SDG#: HBP0l - 12
CAT
NO ANALYSIS NAf,IE
t592 TCL Volatites by 821+0 ' Uater
1722 ThaI t ium
1713 ri I unr i nurrr
1744 Ant i rrrony
174t, 0ari urt
17!17 Beryttiunr
17 t-9 Cadrrr i unt
1751 Clr romi',rtt
1 i53 Ccppen
175!. I ron17\5 Lead
175tJ l'lIlnganese
1761 lrickeL';756 Sitver1,77? Z inc'1843 uu SUg4,5 ! CP D igest ( tot rec )7015 Arsrn'ic TR
7*6 SeIenium'IR
0259 l.ler'cury57t3 r/rJ SiJ8l,6 il9 Digeir
A'IA!.Y S I S
IRI AL DA'TE AN' TI!'IE
i 07/03/96 1013
', 07/15t96 c4'61 A7/":5/96 e4',61 07/i5/96 04'^51 A7/15/96 At"^,6^' D7/1i/96 01,161 D7/15/96 Qtt':61 27/11/9'6 'Jt" 5
" 07/15/96 C/+',ii'i C7/15/95 f;4'.6
" 07/i5/96 A4',51 07/15/96 C416t. r)7/15/9b A41.b1 07/15/96 C415" 07 /15/96 ct,' 51 07/1'J/9o 12221 07/15t96 0!;:61 07.ti5/96 44",5
Page:
ANALYST
Tracey !{eff
Donna R. Sackett
Donna R. sackett
Sonna R. Sackett
Donna R. SacKett
0onna R. Sacketr
Donna R. SacKert
Donna R. SacKett
D Llnna li . Sac ke t t
0onna R. Sackett
Donna R. Sackett
Donna R. Sacketr
Donna R. Sackett
Donna R. SackL.tt
Donn.? R. Sacketr
Christine 14. Contin
Donna R. Sackett
Donna R. Sacke!t
Ne!.'. i S. ltarkaryan
tiei.Li S, I'larKaryarl
llaccie A. Natale
DougLas D. Sei tz
Haria A. Davenport
lrla!-k A. RatcLif lt
i,la!'( A. P.atc i i tf
(l)Lancaster Laboratories
A Thermo Analytical Laboratory 6of 14 il
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LLI Sample No. EL
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subrrirted: 06/29/96
Outfatt JUD Grab Uater Sampte
0817
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TCL SUl346 Senri vo'.at i iesllJat,:,r's
Lancaster Laboratofles
2425 New Holland Prke
PO Box 12425
Lancaster PA 11 605-2425
7 17-656-2300 F ax. 7 17 -656-2681
07 /03/96 1,931
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07/a,,/95 133C
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I,ABOPATORY CI.IRO}'I f CLE
See reverse srde for explanatron of symbols and abbrevratrons 2216 Rev
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I (il)Lancaste r Laborato ries
QIJALITY CONTR.OL RFPORT
7ot
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253801 1
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Il,, ,r.,,illo",nun.
I l,1-0ichtoroethane
?. u9/ iIch t orof oclr
f i.r-r,.ni'Lll".nunu2' us/ t
li ,:;l:l!(r...",n.^"1. uq/t-., Carbon Tetnach Lori de
l;,.,,, ^.::::"A. ue/t
3 BromcdichLorornerhane
Il'' '''-i:ii""o"^"
6 cis'1,3-Dictrtoropropene
1' u'/tI rrichtoccrrhene
! o, oro*o.Iioron,erhun"2. ug/ t
];"1:".'l[l) | "."o"'n"n"
1. ug/tril trnns - 1 . f -oi cl) Loroor ooeneI
I
MEMBEFl
7X-mI
Lanca5ter LdboratofleS
2425 New Holland Pike
PO 8ox 12425
Lancaster, PA 17 605-2425
717-656-2300 Fax. [phone]
l::;",,=n"
3' u'/t
l;:::..:H:'"
5ee reverse srde tor exoldnatron oi svmbols dnd abbrevratrons 2216 Rev 1o,3o,ss d?
(il)La ncaste r Laborato ries
Q:]A]' ITY COIITI1OL R.EPOF.T
Page: B of '.4
!CS
IIPD
L IYITS
lll cir
lt
Il
]l
ll
A Thermo Analytical Laboratory
LLr Sarnple No. 25-?8Ll1L
outf aI t JUD 6rai) uater Sar\pte
flercuIes: Bacchus Pond
Sanrpte SatnPleI'1DL UN I TS
8 Eronroform1. ug/L1 4-Hethyt -2 -pentanone
5. ugl tl0 2-Hexanone7- u1/t
12 Tet rach I oroetherre1. ug/t:i l, 1,2,2-Tetrachloroethane2. ug/ t
l4 Totuene2. ugl t
15 Chtorobenzetre1. ug/Llc Et!ty,tbenzene
2 ' ugr' t-
18 S ryrene1- ug/L!9 Xytene (totat)
1. ug/t-
JC trans-1,2'0ichioroethene2' ug/t
58 cis-1,2-Dichl.oroetht'ne?. rrs/ t
Thattium
1 70. us/ t
Aiuminum57. us/t
Ant iniorry
I
l Ccoup No. 523727
I iieccutes, lncorporated
I
DE
BL.'\NK
N.D.
N.t.
N.D .
H.3.
ri.!.
fr.]-
N .C.
N.D-
Batc;::96i921343102
fi-0.
Batch:961921e431C2
Batch : 95i 921 81'8102
!i.9.
Satch:96'1921843;'02
Batch: 96 192'l8qtl02
0.00t5 J mq/t
Batch : 96192'lfl4Str02
r".0.
G.r tclr : 951 921 81, 3'.-102
N.!.
6irtcl:: 9619213431D2
|l.D.
Bartcr : 96'19218rr3132
!'l Ill,r'7 t 'r,./l
Satch : 961 92'l 3t,li':il2
li.1.
8atch: r)5i921ZLit1D?
r.3.
Batc:r: 96i9218i 8.132
\ -0.
Batctr : 90.l Q21 3(3:lC2
', t
DUPRPD I,1S
lils
'ISD RPD
il
jl
II
LCS
l-0rJIac n, 'o
7n
L<
L1
1nl.
72
105
'1Ci
11C
'I Cr2
1C3
104
IUU
/ 1 \ 1'r1
.1 I 141
9C
93
95
105
94
rc5
:01
1C9
102
108
99
1n,
10i
-7?9 (2)
38
36
t+3
?
ai
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0
)
1
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5
lt
'I
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1
1
it
1Et)-
8.r'i ulr
2-2
Sery!.tiun
l-i
' C:Cnti unt
; Cooper_! ,1
r lTon
2.7 ug/ t
Chroirriurn
!, .3 ug/ t
us/ t
u9./ t
us/ L
ug/ t
u9/ !.
(' )
0 ('i )
(i)
(': )
0 (l)
0 (1)
102
l ne
1C7
100
98
97
1.07
lCt
1C3
'.ryi'
10c
BO
80
BO
80
BO
80
30
80
8C
30
80
80
80
120
120
120
120
1?0
120
lrQ
. f n
120
120
121)
120
120
105
iit
97 97
gtr 95
73 79
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rl
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i Leacl
Lrg/ t
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5-t
5 Silver3.o u!/t
'74 -'513 -''41+1
0 (1) 9? 93
0 ('l ) 59 b1
e {1) 94 95
(1) 9t I01
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lhe bac[:grotrnd resuLt cat n]ore :hitn f cur t lllL's th.] spi<e atlcled.
Lancaster Laboratories
2425 frlew Holland Prke
PO Box 12425
Lancaster. PA I 7605-2425
7 17 -656-230A F ax 7 17 -656-2681
MEMBEFt7Xm See reverse srde for explanatron of:ymbols and abbreviations 22 l6 Rev I0/30,'95
A Thermo Analytica I Laborato ry
Q';TALITY CONTROL REPORT
Page: 9 of '.4
LCS
101
1n-I
10i
LCS LCS LCS LII'1!TS
DUP RPD !-OU E i GH
90
i01
10Ll
9?
72
69
9?
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9C
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1..,2
97
95
97
93
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91
35
67 12?
74 12C
69 126
66 1?D
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42 1?0
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60 120
66 120
60 120
73 1?9
67 120
67 121
53 128
71 ',120
76 120
57 140
75 12C
75 .,20
(iI)Lancaster Laboratories
I
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r-I-f
i
r Grouo l{o.
I Ilr.rcu L es,
I
I
I
5??727
IncorDorated - DE
sample No. ?538C1 1
SanpI e
uIt rs
ug/ |
fls
ii?D
DUPRP! I,1S I,ISD
80
30
80
on
120
120
1?0
i?0
B L.r\NK
Batch : 96i9218/,8',r02
N.D.
Batch: 9619218/,BilC2ri.l.
Batch:96192'131,31C2
ti-D.
Batch : 9(.i 3/r57''3i01il.!,.
Batch: 96'13300C-.sA
0 ('1 )
0 (.l)
0 (1)
ti)gs t\an f tVe tinres
-3/,
1n,
79
s5 36
c)6 95
97 e7
35 85
76 76
78 76
a7 q(
32 83
83 83
8\ 8,4
1:8 11t1
90 91
90 39
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or aa
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tcl
1C1
79
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1
4
0
2
0
0
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3
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L
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l;ii:",:::", { 3
0 - 0t':J r-rg/ l li .,1 .'i.i,..]",,[;;,'*,^"
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0b HeptnchtL)t' Epoxide0.C01 t.:g/i N.r.
l,:;::"":;,1 N.D
0.C05 trg/t N.l.
i'u:::," 'lrs/t N'r'
0.0ri9 u9,/ [ li. ].
^i Endosul f ar'r I I
ll:lr, :;1, -;
17 6nciosut f an :lrtI f :rte
l,::il :;, ;.
'J8 Er:,.i:'in Ketc,re
0. Llt-lr r.rg/ L !t:.i'.
lo'.;in""u'i;l)i N.,,.
I rrty>ha ct,tJ,'ciir'e
0.0 j5 uJ/ r. l.l .!.
trliL;"'nl;i..l""" N.D.
The rr'sul t f or one or bc;th detertui n.:t ions was
T
Lancaster Laboratories
2425 New Holland Prke
PO Box 12425
Lancaster, PA 17605-2425
7'17-656-2300 Fax: [phone]
MEMBEFl7XmI
H.:::,:',":::..":::.sa
p c
I
Samp I e
[''12.
I"i,,,,',^*"2.7 u9/ t
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See reverse srde for explanatron of symbol! and abbreYrdtrons 22r5 Rev ro/ro/es d3
QL]A:ITY CONTR.OL REPORT(iI)Lancaster Laboratories
A Thermo Analytical Laboratory
LLI sample No. 253801 I0utfatt JUD Grab Uarer SampLe
Hercutes: Bacchus PonC
BLANK
I'1.D.
N.D.
N.l.
N.D.
x.l.
ri.D.
ti -D.
N-0.
t,l .D _
Ba:ch: 9,51341JM026
SarnpIe SampteITDL UN 1 TS
r13 Ioxaphene1. Lrg/tr18 Endrin Atciehyde
0.C1 0 u9/ t
r19 PCB-'10160.C9 ug/Li20 PCB-12210-2 ug/L,21 PC8-12320.09 ug/ [t?2 PC\-12t20.05 ug/ L
5?3 PCB-121,8
0 .07 ug./ t
5?t, PCB - 12540.06 u9/ L
5?6 PCB-12600.07 us/ [
Grouo No- 52?7?7'riercutes, !ncorporated - DE
Page: 10 of ':tt
LI!!ITS
HICH
5
a1
23
1
20
51
46
36
5
1
40
35
21
29
DUP I'IS
R;9 I,19 ISD RPD
LCS LCS LCSLCS DUP RP!) LCU
1l
il
il
ll
ll
ll
II
ll
n
I
'lI
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I
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11?
158
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172
124
129
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166
152
210
i13
'180
196
1Af
I
,o,3o,es fI'
86
3 TCL SU846 SerrrivoIat i Ie:;/U;rti,'rs
?18 phenoI?' ug/t
ScrT bis (2-chi.oroethyl ) ethe.?. uS./ t
874 2-chIoropnenot2. u9/ t8B 1,3-dichLorobenzene?' uo/t8B/, 1,4-dichIorobenzene2. ug/ t
331 1,2-dichtorobL'nzene2. u9/ L
oll0 2-rnethytphenot4. u9/ |
tg1 2,2'oxybis (1-chIoroProPane)tr. ug/ [
oB2 4-nrethytp:renoll+. uS/ti,l5 u-ni troso{!i -n-oropylarrrin.'
1.u9/ t
.9O? hexach l.oroethane
1r.u9/ t
;910 ni trobenzene?' u!/t
.rCA i sophort,ne
2-u9/ t;911 2-nitrophertoL
u9/ L
91
38
78
8C
79
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67
lr7
9!
89
82
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9)
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68.
8i
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97
100
95
l
1
1
5
l
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1
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4
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B5
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70
71
77
64
78
103
53
94
97
92
10
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MEMBEFlTXrE
Lancaster Laboratorie5
2425 New Holland Pike
PO Box 12425
Lan(aster, PA 17 605-2425
717-656-23O0 Fax: [phone] l
4.
5ee reverse srde for explanatron of symbols and abbrevratrons 2216 Rev
I
I
I
LLf S
[:.:,",
(I)Lancaste r Laboratories
A Thermo Analytical Laboratory
QI-TALITY CONTR.OL REPORT
Page: 1 1 of
amp)-e No . 2-53801 I
JUo Crab U'rer S.rn'ote
: Bacchus Pund
Samp I e
Group No. 5?2727
l-iL..cr..rIcs, ]nccrporated - DE
DL'P
R F:t
LCS LCS LIMITS
RPD LOU HISH
I
SampI e
^J::, .,,",J:,,::",?' ug/l'l;,
. l;.^ii;:,:"::,"
n'"rhane
?1 1,2,4- tri ch Ioroben:ene
B I-ANK
Batch: 9513/,1,.,u,C25
N.!.
N.:r.
N.!-J.
N.l.
Lancaster Laboratones
2425 New Holland Prke
PO Box 12425
Lancaster, PA 1 i605-2425
717-656-2300 Fax 7 17'656'2681
LCSLCS DUP
65
86
0q
7n
8l
73
l+5
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BO
41
91
9C
AQ
95
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ll:",'.^",ilii
71 4-chLoroani I ine
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72 l'-ch toro- j -nrerhylohenoI
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I {.::.::"li:i: i:,:::.., .""o. u9./ t
7.ri:' o:
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I ; ;;,.;;;,;;-
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1
37
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119
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116
116
147
123
100
144
151
118
143
112
115
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1 132
23 131
39 179
50 153
80
93
lr7
89
9i
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37
45
33
96
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37
92
55
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9/'
95
MEMBEFI7XTflI See re,ierse srde tor expianatron of sTmbors and abbreviatrons 22r6 Rev loBa/s(. d'8
(I)Lancaste r Laboratories
QI-TA],ITY COhITROL RI?FOR!
Page: 1 2 of '. t*t
I
I
A Thermo Analytical Laboratory
LL! Sample No. ?53801 I
Out{al t JUD urab Uarar Sanrc',e
Hercules: Bacchus Pond
SarnpIe Sanrpte
r'lD r- uLi I 'r s
37 diethyL phthatate
,. - t-tgrf t
75 4-chtor-ophenyI ohenyl. ethec
4. ug/ t
98 fluorene
?.ug/ L09 4'ni troani L ine1- ug/t
?.3 4,6-c!ini rlo-2-methylphet.tol
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11, tl -rii rrosociilheny'-an:tne
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Lancaster Laboratofles
2425 New Holland Prke
PO 8ox 12425
Lancaster. PA 17 605-2425
717-656-2i00 Fax [phone]
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See reverse srde for explanatron of symbols and abbrevratrons 22l6 Rev 10/3A/95
(iI)I Lancaster Laboratories
A Thermo Analytical Laboratory
Lta sarnple l{cr.
OutfatI JUD Crab Uater
1r..."u,." r Sacclrus Pond
I
253801 i
Sarnp L e i
r Cr-ouc \io. 52?727
. Herc'-lla-:,, :raoa.Dorated - DE
l
QUALITY CONTR.OL P.IPORT
Page: '! 3 of 1 4
LCS L I 14I'I'S
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BLAN(
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N. D.
Lancaster Laboratofles
2425 New Holland Ptke
PO Box 12425
Lancaster PA 17 605-2425
7 17 -656-23OO Fax 7l 7.656.2581 2216 Rev 1o/ro/es i'PSee reverse srde for explanatron of symbols and abbre,/ratrons
(iI}La ncaster Laborato ries
nI]a T TmrY' r.n\Tml)nr QFLT^I)m.zeriJ-- L --vr a\!rvtr\-
Page: 11, of 1.4A Thermo Analytical Laboratory t
I
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LLI sarnple No. 253E011Outfatt JUo 6rab Uater Samote
Hercutes: Bacchus Pond
11937 TCL Pest i c iclL.s in tJaters
459e TCL Votati Les by 8240 - Uater
r.678 ICL 5U8{6 SenlivoIati !.es/Uaters
4579 ICL SU846 Se.rrivoIat! Les/9atels
Croup No- 57?727
Hc.r-cuIes, inco.porated
SURROGAIE SU!4I'IARY
TRIAL '!D SURROCATE RECOVSRY Z
TCX 68
DC8 9?
c4-',l ,z-DCA 99
c5 - ro i. ueq€r iai
EfB !'2
?-Fipnenot 50
?iie'nol. -d5 ili.,t;,('-TS? 1,C
litfobl-C5 64
2- F5i phnyl 5i
Tpnenyld i4 66
SURROGATE LIM!TS
LOU
60
60
76
q,)
36
?1i0
10
l*i
HIGH
120
12C
114
110
115
'10c
() /+
I c)
11/+
tto
",4^t
MEMBEFI7Xm
Lancaster Laboratories
2425 New Holland PikP
PO Box 12425
Lancaster. PA 11 605-2425
7 17 -656-2300 Fax: 7l 7-656-268 I
T
I
I
I
I
I
I
I
I
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ro/jo,es t"
i5ee reverse srde for explanairon of symbols and abbreviatlons 2216 Rev
I
I (iI}La ncaste r Laborato ries
A Thermo Analytical Laboratory
ILLf Sampl-e No. EL
ffi ',.::'
uu''r'
r!,'ruu ::r::.".,Discard: 8/ 9/96
["::.:::: ::::^::'::":"*'"
ClOSC SDG#: HBP0l -04
I ANALYST. IrAHE
25i,8C03
by BR
B/ 1/9.5
i lt..ount llo: C6716
i Helcutes, Incorporated - DE
I Envi ronnenta L Affa i rs
r rJ i i nr i nc t on 1fi 19119/+
II
I
AS RECEIVED
F E'H C3
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Page:1 of 1'1
P.0.
Ret -
RespectfuI Ly Submi tted
R3nlona V.r-aynlan, Croup Leader
lr:? YetaIs/Leachates
3
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754
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ThaItiuor
11[uminunr
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Chl'orniunr
Copper
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Lead
llirnqsnege
liicii.eL
S i Iver
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Arsenic TR
5eteniurn IR
l,lecc ury
TCL SU846 Sernivolat i Ies,/l,aters
TCL SUB{C, Serni vol.at i Ies/!Jatecs
COPY
COP Y
See Page
170 - u9/ t
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Rachel. L- K.(:iirrer
0l:ll:04 D 0'iu1 15 REP
110 '15.00 C'110?7i10 AsRCru
ATIII: lrtr. Jos.--oh Ku,i. ler.
AITN:,!!r- 3r-cnl. Rr5inscn
Servrces Re!r esentettvear (717 ) 656- :l-1113
12t,4rio 52?7?/
MEMBEFl7Xm
Lancaster Laboratofles
2425 New Holland Pike
PO 8ox 12425
Lancaster, PA 17 605-Z 425
717-556.2300 Fax [phone] See'arerse stde for explanatron of svmbols and abbrevratrons 2216 Rev ,oi3o,es d.}
La ncaste r Laboratories
A Thermo Ana lytical Laboratory
LLI Sample No. EL
Cottected: 6/27/96 at 0S:00
Suhni tted: 6/28/96 Reported:Discard: B/ 9/96
CU-1 Disc. Grab Uater Sampte
Hercutes: Bacchus Pond
ClDSC SDG#: HBP0I -04
:ATIO, ANALYSIS NAME
:L Votati Les by 8240 - uater
158 Ch Ioromethane
157 Bromomerhane:92 Vinyl. Chtoride
i94 Ch Ir:roethane
l97 l,lethytene Chtocide
i98 Acetone
.99 Carbon Disutfide
t00 1,1-Dichtoroethene
;01 1 .1 -Dichtoroerhane
;03 Cir Iorofornt
504 1,2-Dichtoroethane
116 2-Butanone505 1,1,'1-Trichtoroelhane
506 Carbon Tetrachloride
5A7 Vinyl Acetate
508 Brotnodichloromethane509 1,2-DichLoropropane
516 cis-'1.i-Dich',ocoProPene511 Trichtoroethene
512 Dibroilochto.omethane513 1 ,1 ,2-Trich:.ocoethane515 Benzene510 trans-1,3-DichtoroPcoPene
513 Bromoform.5?1 4-llethyt-2-pentanone.520 2- l{exanone5?? Tet rach I oroethene.5?3 1,1,2,2'IerrachIoroethane,52t, To I uene;525 Ch Lcrobenzenei526 EthyIbenzene;528 Styrene;529 Xytene ( tota[ )i7B0 trans'1,2-DichLoroethene
'?oB cis' 1,2-DichIocoethene
Page:? o{ 11 II
T
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ouestions? Contact
,e.achel, r. Kaet:tner
Account No: 06716illeccuIes, Inco!'porated - DE
i Envi ronnrental. Af f a irs
I ui [*ineton DE .19894
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2538C03
by GR P.O.
Ret.
A9 RECEIVED
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your C|.ient Services Representativeat (7":7) 65o'2J14
MEMBEFI
7a<m
Lancaster Laboratofles
2425 New Holland Prke
PO Box 12425
Lancastet PA 17 605-2425
7 17 -656-2300 Fax: [phone]
Respectfut ty Submi tted
ui chel.e i',!cCiart n, B.A.
6roup Leader, GC/MS Vor.at'i Ies
See reverse side for explana:ron of symbols and abbre,rtattons. 22 1 6 Rev. 10/30/95
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il\ccolrnt t{o: 06716
i Hercules, .lnrorporated - DE
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AS RECEIVED
TES.JLTS. DETEC]]CI{ L!MIT UN!IS
P.0.
Re[ -
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l,o,a ohenolI rsoT ors (Z-cntoroetny[ ) etner
3P,74 2-ch Iorophenoti383 1-3-dichtorobenzenef iss+ .].4-drchtorobenzene
l;ssz 1.2-cilchtorosenzener u"au a-rernyIp.en.JL4631 2,7'oxyb\ s ('l -chIorooropane)r qo82 4-lnethvLoherroI
I lll: [t::;i;::J;t;::.,o''u''n"
39'10 nirrobenzene390t- i soohorone
I rst t 2-nr troohenoII 1;:: 3;: ?i:'EI?t:3::ffi1,, me,hane
3385 2,1-dichLorophenoI
liiii riri::i:r?;:::""'"*
1900 hexachLor-obutadiene
3e72 4-chtoro-3-methyLphr-nol
I :'vu5 Z-nlernvrnaorrna LeneI :;:t t:t:::i:iffr:::ffi![i'"'."19?? 2,4,5-tricnLorophenoI
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;lachei !-. Kl'ra$er
Ct i ent Serl i ce:-. Qelresenre'. ive
ar (7 17) c,tc-,llLl3
MEMBERKrIr
Lancaster Laboratones
2425 New Holland Prke
PO 8ox 12425
Lancaster, PA 11 605-2425
717-656-2300 Fa:r 717-656-268 I
Resoec!fuI ly Submi tted
Chris:ine I'1. Ratci. i fi
G.our Leadcr, GC/|4S
)ee reverse srcra ior exotarratrof ol svmbois and abbrevtattons
,.
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(I)La ncaste r Laborato ries
A Thermo Analytical Laboratory
LLI sampte No. EL 2538C03Cottecred: 6/?7/9o at 0B:00 by sR
Subrnitted: 6/23/96 Reported: B/ 1,/96
Discard: 3/ 9/96
CU-1 Disc. Grab Uater Satrple
Hercutes: Bacchus Pond
ClDSC SDG#: Il8P01 -04
cAT .r...N0, AIJALYSIS NAME :,:,,,
ICL SuB46 Semivotati Ies,/Uaters
Rev I0./30/9i
(iI)La ncaster Laboratories 4 of 11A Thermo Analytical Laboratory
LLI Sample No. EL
Cottected: L/?-l/96 at 011:!0
Subnri tted: 6/?8/96 Reported:Discard: B/ 9/96
CU.1 Grab Uater Sampte
Hercul.es: Bacchus Pond
C'IDSC SDG#: l{8P01-04
AIIALYSI S NAI4E
TCL SU846 Semivol.ati Iesluaters
39'08 3-ni troani t ine
:.?i7 ac:naphthene
3513 2,4-dinitlophenoIj.,)\2 4-nirrophenot
ii79 cii benzofurani391 2,L-dini t rototuene
18,?5 2,5-dinitr-otol.uene23.37 diethyL phtnatate
3a75 4-chIorophenyL phenyt ether
3393 f Iuorene
1909 4-nitroaniIine/.b23 4,5-dinitro'2-methyIphenoI
391!, N-nitrosodiphenytairrine
3859 4-bromophcnyt phenyl ether
3!c/9 he,rach I orcbenzene
=?16 penrachtorophenoI
i917 pirenanth I'ene
1a)9 a,lthracerle
4ri84 carbazote
33S0 di -n-butyt phthaLate
3bv7 f Iuoran,.henel9i9 p) renej370 brityt benzyl phthatate
-z$85 3,3' -dichtorobenzidinejg60 Lienzo (3) anthracene
:':ll,5B bi s (2-ethylhexyl ) phthatate
3375 chrysene
-'::i95 di-n-octyI phthatate
:')61 benzo (b) ftuoranthene
:'t5? benzo (k) fiuoranthene
l3o4 benzo (a) pyrenej9C3 inderro (', ,?,3-cd) pyrene
iaril ciicenz (a,h) anthracene
i833 benzo lghi) peryLene
253tCC3
by AR I A."ou.rt No: 06716
i I'ierc,-.rtes, !nccrporated
Envi romrenra i Af Ja irs
Uitnrington DE '19394
P.O.
Ret.
B/ 1/96 I
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ilachei. L. Kr..amer'
y,our C l. ierrt Services Representat iVeat (7''7 ) 556- ?l'-r0
Res:ectful Ly Subnri tted
Chiistrne 1.1. Rarctifi, S-S.
Crouo,eader, GC/l'1SLancaster Laboratofles
M E M B E Ii 2425 New Holland PrkeI4l-il l3^SliJiii',,u0,,.,,
rnn
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08,: 00
2533C03
by ER
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Account No: 067'16
i itercutes, :ncorporated - DE
I Errvironnrental Atf aiis
i'Ji i.nrington DE'19894
Page:5 of 1'1
Donna R. Sackett
Donna R. Sacke!t
Donna R. Sackett
Donna R. Sackett
Donna R. Sackett
Donna R. Sacketr
Donna R. Sackett
Donna R, Saci(ett
Donna R. Sackett
Donna R. Sackert
Donna R. Sackett
Donna R. Sackert
Donna R. Sa.kett
Donna R. Saakett
Christine 1,1. ConIin
Donna R. Sackett
Donna R, Saciiett
iletti S. 14arkaryan
lieL l i S. l',!af karyan
lilaria A. Davenport
I'iark A. RatcLiff
Hark A. Ratc L i ff
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?G
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CU-1 Disc. Grab Uater Sanipte
Heccutes: Bacchus Pond
C l DSC SD6#: HBPC'l - 04
CAT
NC AUnl'rSIS Urmr
459? TCL Volatiles by 8240 - lJater
17?2 Thattium
17 43 Ar. umi rrum
171.1 Ant inrony
1746 Bariun
1747 Bery[ [ ium
1749 Cadmi unr
1 75 1 Chromi um
1753 Copper
',754 I ron
1755 Lead
1 758 Manganese1761 N i ckeI
1766 Sitvc-r
1772 Z i nc
1813 UU SUB46 ICP Digest (tot rec)
7035 Arsenic -IR
7036 Selenium TR
0259 l'1ercur1,
5713 UU S'h'846 H3 Dlgest
IlET HCD
su-846 82408
su-846 6e10A
su-846 6l'l0A
s*-c46 6' :0,'\
su-845 6010A
sr.r-546 6i10Acr,_a,l 4r1n^
Sil-8q6 o:J104
sr]-346 6l'10A
Srr - 845 6110A
su-346 511CA
su - 846 6!a 1 ilAsu-346.'l'liiA
cl,-C1-i 4TrnA
srr-346 0110A
s';-8,16 3--r35A
sr^'-346 6llCA
su-s45 6l1CA
su-8.(5 7{7CA
Sl']-845 7,i7Ch
07/15/96 C340
07/15/96 C3!,0
07/15/96 Air,C
07/^,r/96 A14C
07/1.5/96 A3/.t
a7/":5/c)6 C3qt
07/i5/9'i, c34C
a7/^,5/c/6 0310
07/^,i/96 A3/t0a7/i5/96 A3!-A
c7/',5/96 C3.LC
07/15/9t C3!.A
A7/^'5/9to 11-l/tD
c7/15/96 Ci,1C
t\7 I ", t1 t Q^ 1)))
c7/',5/96 C3!+)
C7/'t5/96 C3aD
c7/ri/96 19AS
07/02/9b 21??
c7/02/96 A93C
07 /0/+/96 A?06
07/04/96 C?D6
ANALYS I S
TRIAL DATE AND TIME ANALYST
1 07/03/96 1047 Tracey Nef{
08'll BNA Uarer Extraction 5ll-846 351C8t,678 TCL SU8tr6 SerriivoIati IeslUaters SU-8(6 82708/,679 TCL SUBI'6 Semi votari IeslUaters Sl"'-545 827CB
Lancaster Laboralofles
2425 New holland Pr(e
PO Box 12i25
Lancasler PA 17505-2-il5
717-656-2100 Far 7i:-656-2bSl
I,ABORATOP.Y CI-IROI{ I CLE(I)La ncaste r Laboratories
A Thermo Analytical Laboratory
LLI Sampl-e No.
Co[ [ected: 06/?7/96 at
Suhrri tted: 06/28/96
MEMBER
5ee reverse stde ior exoianalron oi svmools and abbreviatrons 2216 Rev 10./10i95
(il)La ncaste r Laboratories
A Thermo Analytical Laboratory
QUALITY'::-*:
:'::' }I
Il
!CS
RPD
LLI samp]e No. 2533003
CU- 1 Di sc. Grab lJater S.rnrpIe
Hercutes: Bacchus Pond
I Grouo No. 522727
li,erc,..:tes. lncorporatec - iE
il
Samp I e
t4D r-
SampI e
UN]'TS
?18 Ch Iorornethane3' u'/t
257 Broflroflrethane3. us/ t492 VinyL Chtoride2. u9/ L/-9L Ch I oroethane3' us/L497 t'lethy t ene Ch I on i de2. us/ [498 Acetone6. us/ L
499 Canbon Disutfide3' ug/|
5C0 1,1 -Dichtoroethene
1. us/t
501 1,1-9ichtoroethane?' ug/ti503 Ch Iorofornr
1 ' u'/t
,5O4 '1 ,2-D i ch t oroethane?. u9./ ti316 2-Butanone3. uS,/ L;505 1, 1,1 -Trich'.oroethane
1 ' ug/t
;5C6 Carbon Tetrachloride1' us/ti't07 Vi nyI Acetate7. t-tg/ t
t508 Eromodichtocomethane1' u'/l
5509 1,2-Dichloropropane
'1 ' uglti51o cis-1,3-DichIoropropene
1 ' us/t
,51'1'f richtoroethene1. us./t
3512 Dibromochtolomethane?' u8/ t3;1i 1,'1,2-Trichtoroeth.ine?' us/L
35't 5 Benzene
'I ' ug/'t
351C trans- 1 ,3 -D ich Loropropene
U9/ L
LCSLCS DUP
DUP I.iS
RP] MS HSD RPD
LCS
LOIJ
LIMITS
H!CH
2 TCI- Votaril.es by 8240 - Uater Batch: !96134 1AA
N.D.
H.D.
N.D.
N.D.
N.D.
N.D.
N.C,.
l,J .lr .
N.D.
r,l.D.
I -D.
N.D.
Ulr
N.D.
N.!r.
N.9.
l':.D.
N. D.
r! n
R68
83 31
90 BZ
e,7 61
102 98
67 91
75 72
111 i 06
1C3 i00
1i5 109
9/r 100
('t, 97
116 11/l
1't 1 110
3/, 1 10
99 104
98 101
97 101
106 105
e7 99
s2 96
1C/, i 04
91 102
B
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9
9
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4
7
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4
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27
5
2
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1
11
16
0
12
Lancaster Laooratofles
2l2S New Holland Prke
PO Box 12415
Lancasler, PA 1 7605-2.125
717-650-1100 Far 7l?-55o,2681 ,ilree
MEMBEFl
1.
See reverse.rroa ior exotirdlroit oi svmDolj and abbr€vtatlons 2216 Rev 10/30,/95
l"
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3521 fotuene
I:: l,::;:,::rii
7., 9C
65 93
6? 95
1A6 1 05
7? 94
105 '1 C5
101 i0'1
ii0 109
'l 3? 102
1iB iCB
M99
146 1 02
.1r 1nr .n1
17t, -772 -729 (?)
(i) 1!5 1Co
3 (1) 97 38
(1) 97 97
('i ) 9t, 95
0 (1) 78 79
0 (1) -201 -191
17t, -1S13 -1441 (2)
0 (1) 92 93
c (1) 59 6^,
c (i) 9t, 95
(") 99 101
QLIALITY COITTROL REPORT
Page: 7 oI 11
LCS LIMIlS
LOIJ H I GH
B0 120
80 120
B0 120
80 "t20
30 ',120
B0 120
80 120
B0 120
B0 120
B0 170
80 120
B0 "120
B0 120
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r Croup No.
llercul. es,
I
5?2727
!nco.porated - DE
DUP
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LCS LCS
LCS DUP RPD
t:sI.ISD I1PD
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?4
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17
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26
0
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1
0
5
4
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1
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9
34
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98
97
107
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back3roirnC fL-si:i! irzrs rEore ti!an fou: tir:rr-s tl'rr sp!l<.. aCdeC.
Lancaster Labordtones
2425 New Holland Prke
PO Box 12425
Lancasler, PA 1 7605-2425
717 -656-2300 Fax [phone]r
MEMBEFIxmT o?i
(iI)Lancaster Laborato ries
A Thermo Analytical Laboratory
LLI SampJ-e No. 253,9003
CU-'l Disc. Grab Uarer saorpLe
Hercul.es: Bacchus Pord
BLANK
u.D_
N.D.
N.D.
N.D.
lt -D.
N.!.
N.i).
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N.!.
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N.D.
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Batch:96192181,31102
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9atch : 9c19218/t llll02
N.D.
Barch: 95i92'1843102
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Batcl::9619218/+UC02t.3.
Batch: 96'1921848102
0.0C16 J mgll
Batch: 9619218,/,8102
H.D.
Batch: 96192'!848-102
N.D.
83tch:95i92',l843C02
N.Cr .
Batch: 96'1921848302
0.04'07 J mg/ t
Satch : ;'51 92'l 51r3i102Irr
Batch:96i9?lg48l0l
li.cr.
Bitch:9619218{9102
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5ee reverse srde ior explanatron oi svmbols and abbrevratrons 22 16 Rev 10/30/95
(I)Lancaster Laboratories
A Thermo Analytical Laboratory
QLTALTTY CONTROI- REPORT
Page: 3 of 'l 1
LIM!TS
HICit
1l
LLI samprlg No. 2538003
CIJ- 1 D i sc. Crab Uarer Sanpte
Hercules: Bacchus Pond
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;I
I
I
I
I
I
I
I
I
112
158
I J.+
172
124
129
123
.,66
i)z
230
'1 13
180
1,96
182
119
135
142
113
Sanrp I e
l!!'t r_
iZinc
1?.
; Arsenic TR
a7
r Seleniurn TR
2.7
) l'lercucy
0.01,1
Samp I e
Ut: I TS
ug/ t
u9./ t
ugl t
u9/ I'
- _74
142
102
79
(+9 lr7
9i 91
s5 89
78 82
8C 33
79 32
81 32
67 63
s3 83
ttL : tq
7a aa
97 e7
100 r0c
9/. 95
65 70
90 90
86 86
79 B'1
oq oo
the LOo.
80 120
80 120
B0 ,,20
B0 120
f.:sMS! PPD
DUPRFD I,:S
LCS LCS LCS
LCS DUP RPD LOU
I TCL SU8/i6 Senrivotati Ies/Uaters
,18 phenoI
1 ' us/L
il:7 b'i s (2-chioroethyt) ether
1. ug/|.
\74 2-chtor-ophenot
1 ' u'ltl8l "!,3-CichIorobenzene
1 ' us/t161 1,4-dichtorobenzenc'
'1 . uglt
13? 1 ,2-di chtorobenzene
1 ' us/t
tB[] 2'orrthytphenoI?' u'/t
581 2,2'o:<ybis (1-chLoropropane)
?' u9/ [ttiz 4-methytphenol2- uS/ L)15 l.l-ni trosodi -n-propyIarnine
?' ug// titi2. hexachtoroethane2- u9/|)1C ni tcoben:.ene1. ug/[)0/. i sopirorone1' uE/l'911 2-n'i rrophenol.?. ug/ ttJr0 2,4 -drnrethytphenoL1' u'/t\Lb bis (2-chtoroethoxy) flrethane1' ug/L535 2,4 -Ci ch t orophenoIZ. ug/ Lt21 1 ,2,4 - tr i ch Locobenzene
1 ' u,/l90o naphthaIene1. ug/t
BLANK
Batch:96i9218/.8A0?
N.D.
Batch:951921848102
r".0.
Batch:96'1921848102
ti-.D.
Batch: 96'19457131C1
N.D.
Batch: 95'1841/A-A026
N.!.
N.D.
ri.D.
iln
N.D.
t,n
N.D.
t,l.!.
H.!t.
ti.t.
l,n
[_].
N.D.
N.D.
ll .D.
N.D.
N.D.
N.D.
c (1)
0 (1)
0 (1)
0 ('t )
103
103
1C3
93
- 4',]
101
1!i
a(r
5
1
1
0
3
'I
1
5
J
3
1
)
0
1.
a
0
0
1
7
0
C
J
0
4!
aa
o<
LA
7A
71
77
64
78
1C3
53
94
97
92
65
B4
7A
nl
5
1?
23
,1
20
32
46
36
5
1
l-0
35
2r,
29
3?
33
39
4t+
21
The cesut-t for one or both detecminations xas Iess than five tinres
MEMBEFlKriI
Lancaster LaDoralories
2425 New Hollano Pike
PO Bor 12^125
Lancasrer. PA 17605-2.i:5
717-6q6-rlnn Frr "ll-Ai;-?6R1 d
1""
t
I
I
I
(iI)Lancaster Laboratories Page:9of 11
A Thermo Analytical Laboratory
LLI sanple No. 25380C\3
Cl.J-'1 Disc. Grab Uater Sanrpte
Hercutes: Eacchus Pc,rrC
Sample SarnpLe
MDL UI'I]IS
4-chtoroani Iine
Group Nrr, 5??727
iiercuIes, !ncorporated - DE
LCS
iO'vJ
LCS
LCS DUP
DUP I'IS
R PD I'IS !4 SO RPD
I.CS
RPD
J,,
3900
JU"
3905
H]
J":
3907
]*,
3858
2.r-:S/ L
hexach Iorobtrtadi ene
1-u9/ t
/r - ch I oco - J -ruet hy I pheno t
2-u9,/ t
2 -nrethy t naph tha I ene
'1.us/ t
hexach Iorocyc Ioperrtodt ene3. us/ t
2,4, 6- tr i ch tonophenoI
1. trs/t
2 ,4 ,5'tr i ch I or opheno I1' ug/L
2-chIororuphthaLene
1. trg/t
2-nitroantLine
1. ug/t
dinrethyl. phthaiate
l. ugl/ L
acenaph rhy I, ene
1. us/L
79 TcL SUB/I5 SemivoIat i Les/uaters
ELANK
N -9.
N.D.
N.D.
N.l.
ti.! _
N.r.
N.D.
L! r,
ll .0.
Satch: 96'l84LAAC?6
ti.D.
N.D.
N.D.
ti.D.
Un
N.9.
t,t .D.
N.!.
e,5 69
91 93
36 87
51 53
89 B7
oa oo
9't 90
97 97
3? 31
9? 9-1
80
lr7
e9
9Et
99
64
101
102
2
1
1
5
3
1
,1
0
1
2
t)
45
91
QN
4l
91
90
B8
95
25
B6
LII'II TS
HIGH
17 116
2t+ 116
2? 147
28 123
1 100
37 144
39 151
60 118
53 143
1 ',',! 12
33 145
3903
t'u"
3893
t,n,,3s79
ffi:
t::,
1393
l,non
1683
I
I
3-nitroanitine
1.ug/ t
acenaph th ene
1.usl L
2,4-ciinitrophenoI
5-u9/ L
4-ni trophenoL5' us/l
d i benz ofur an1. rrg/[
2,4'd i ni t rc,tol uene
z-ug/ i'
2,6-clinitrototuene1' u9/[
diethyL phl:halate
?.uc/ |
4-chtorophenyL phenyL etherz' uslt
f I uorene1. uE/l
4-ni troani I ine?' ug/t
4, 6,-d'i ni t ro-2 -methyt phenoI5- u!l/t
80
93
37
45
8B
96
100
tc
1A2
98
B6
5/.
1
0
'10
)
,1
1
1
2
'1
4
0
5
B(l
87
9?
55
B5
94
95
59
101
9B
B6
Q)
1
,a
39
50
1
?5
59
33
1
tqJ
145
191
132
13'l
139
158
tt4
158
1)1
122
1Bl
7
47
1
a
?.I
Lancaster LaDoralofles
2425 New Holland Prke
PO Boi 12425
Lan(asier. PA 17605-2415
717-65o-2300 Fa\ 711-656-2681
QUALITY CONTROL REPORT
MEMBEFl
oe .everse srde ror e^pldnatron o1 symDors dno abbrevralrons 2216 Rev 10/30/95
(I)Lancaster Laboratories
A Thermo Analytical Laboratory
LLf sample No. 2533t103
Cl,l-'l Disc. Grab Uater Sarnpl.e
ilercutes: Eacchus Pond
Sarapt e SampL eI.iDL UIIIIS
N - ni ti'osodi ohenyI anri ne2. ug/ t
4-bromopheni,l. phenyt ether
2' ug/t
h exach I orcbenz ene
'1 ' ug/t
pentach I orophenoI
1 ' ug/[
ph enant lr re-ne1. ug/L
anth nacerru.
1 ' uglt
carbazole
'l . us,/ t
di -n-butyl phthatate
'1 ' us/i
f Iuoranrhene1. 'rS/L
'1 ' u'/L
butyL benzyt Dhthatote2' u,/t
3, 3' -d i ch I errobenz i d i ne2' ugii
benzo (a) anthracene1. uoltbis (2-ethylhexy[ ) phthat6re
2. uii/ t
c h r';'s =ne'1 , ug,/ t
di -rr-octyt phthatate
?' u'/t
ben:o (b) fluoranthene?' usll
benzo (k) ftuorantlrene?. ug,/ [
benzc (a) p.vrene
2. ug/ t
indeno (1,2,3-cd) p),rene
?. ug,/ l.
dibeaz (a,h) anthracene?' us/t
benzo (gi;i) perytene2- ug,/t
BLANK
N.D.
lJ . t,-
N.D.
trh
l,l.lr.
N.D .
N -0.
N.D.
N.D.
lt. !.
:( -D.
N-n.
N.D.
N.3.
N.D.
N. D.
N.3.
N.D.
N -D.
ri -0.
N.D.
I
i Group fto. 522727
i tier-c,,.:les, IncoiDotated - tJE
I
I
88 86
83 87
96 94
45 40
95 9t+
oo oa
e2 90
89 37
g'.J 39
91 91
aa, qn
79 78
oi oc
102 101
91 91
100 107
90 88
9-\ 95
3l 83
76 75
qq aL
7/. 7t,
QLIALITY CONTROL REPORT
Page: 10 of 'l 1
LCS LIMITSLOU HIGH
il
il
DUP I'IS
RPD i'ls MSD RPD
2
2
2
11
0
1
2
?
1
2
a
?
0
1
0
6
2
0
0
,]
2
1
Bt,
B5
95
90
92
B5
B9
83
ao
>a
B?
atq
102
9C
104
B9
gt1
B1
Q)
91.
J6
53
1
14
54
)7
40
1
26
\?
,1
I
33
8
17
?4
11
17
1
1
1
lt I
1)7
lsz
176
120
IJJ
151
118
t5(
il)
152
26?
143
158
168
tqb
''i59
'163
163
tl I
227
219
1l
1t
il
il
LCS LCSLCS DUP RPO il
.:L9
999
)16
)17
359
58t)
380
!197
919
370
335
n: n
3oS
rta;
..tc
11../ 1
n.')
;u3
ti,)l
1I
;l
I
I
I
I
I
I
I
MEMBEFlK-n
Lancasier Laboralofle5
2425 New Holland Prke
PO Box 12425
Lan(aster, PA 11 605-2425
7 11 -656-2300 F ax I 11 -656-2681 See reverse sto: ior explanatron of svmbois and abbrevratrons
I
I (I)La ncaste r Laboratories
A Thermo Analytical Laboratory
QIJALiTY CONTROL REPORT
11 of 11
LIHlTS
H I6H
111+
i10
115
100
94
12i
11/.
116
iu
"
1"", Sampl-e No. 253800-r
Gralb Uarer SanrpIs
Bacchus Pond
CU-1 Dlsc.
Hercut es:
: Grouo lio. 5??727I Fi.'.c,.,1es, lr:r orporated - DEI
I
I
I
I
t
I
I
I
I
I
t
I
I
T
I
S!C!:06ATE S'JM!.1,A.2Y
TRIAL :D S'JRROGATE RECOVERY Z
4592 TCL Volatites by 3240 - Uater d4-1,?-DCA j)t+
cii- tor.uene 99sr0 95
/i678 TCL StrlJ46 Senrivotati tes/Uaters 2-FLphenot 54
Phenol -d6, 36?,/,,6'IBP 77
l+679 ICL SU346 Senrivotati tes/,Jarers Nirrobz-C5 83?-l'ciphnyl 77Tplrenyldl4 77
Lancaster Laboralo(es
2425 New Holland PrKe
PO Box 12425
Lancdster. PA 1 7605-2.11:
717-65o-1300 Fa'. 7i;-655-268t
SURROGATE
76
qil
66
21
10
10
3\
d3
MEMBEFt
5er r everse srde for explanatron o{ svmbols ancl abbrevratrons 2215 Rev I 0/10/95
1l
nl
II
]l
]r
}T
tl
Il
II
1I
il
rl
1l
:;
I
I
I
I
I
ai'
T
I
I
I
I
1,59?
tliii1,7/.5
17/'7
llii\
1754
ttiii
1772
I i:i;
L.d7gt
C
ro/ro/e5 ?c
I
I
I
I
t
I
T
I
Lancaste r Laborato ries
A Thermo Analytical Laboratory
LLf samore No. EL 25i8C06
CUL Ie.:r ".d: i/2o/96 ar i 1 :DC by Di
Subrri tred: b/23/9D ReporreC: e/ 1/96Discard: B/ 9/96
CIJ-2 Disc. Grab Uater SamDte
Hercutes: Bacchus Pclnd
C2DSC SD6#: !lllPCl - 07
CAT
NO. ANALYSIS NA!'IE
TCL Vol..ir r ies by 822'0 - lJatec
Tha[ [ iurrr
A Iurni nuu
Ant i nony
Eiar ium
Bery[ [ ium
C adtn i urrr
Ch rom i unr
Copper
I ron
Lead
ManganeseIicket
S i Iver
Zinc
Arserr i c TR
Setc-niurr IR
l,lef cury
TCL SU*46 Senrivotali tes/Uaters
TCL SUSl+6 Se$ivoIati Ies/iate.s
1 COPY T0 Hercutes, lncorporated
1 CoPY TC [151 - Rocky i{ountain
RtciIVED. METI{CD, DETEITIlrr !-llllI UNIiS
See Pa!te170. w/ |
57 . Ng/,,
15 . ug/|?.2 u,J/ |1.3 ug/t?.7 us/ i.!..3 rg/',1.8 ug,/ L5.9 ug/l'13. u9/ i.2.9 ug/ |
:i .4 u9/ ii.6 ug/t
'I e'. ug/ t
2.7 ra/ i
1 7 tt^tlJ,-l .
r_1. t(l .Jgzl i
l.,e Page
See Page
I l\ c c our'\ t llo : C67i 6
, rleIcuit.s, inrc.roora!ed -
, lnvi lD't'rrt:nr.i. Aif a: rs
I .l t t lr i lc i.-)n Df '19894
P -O.
tsei-
3
lr
ResDectfuI Ly Sulmi tted
iian:cna V. Lzlynan, C.oup Leaier
I CP l'1eta l.s/Leachares
Page:i oI 11
:: i:::::ln I.
'::.::. ,r^ :.
l.:::.::. !r 1.: :: :: i,.r r
:.t.. ri n
:, .1 ,,:f,, l ! ij
t.;,,,,,,:,,,:,,:,.cg.
:..:r:rr':.::: 1t tr::r..::: 'r.:':: ...' .
:.:::t :t : :::.:. i,' . _ .
Quest i ons? Contacr yc.:lr CI i errrRachcl.,-. Xrcl:ir:er03;i!:1,9 D C"-,1 l5 Rf?lrC 'r5.tC Ct]l,l27-1 r.SRaat
ATril : t'lr'. Jo::('ph KelLer
l'.YTl:: Mf . 3rr'nr R.:linson
Serv i c,-':-. Replesen!e t i ve
a: t.1 7) tit,-2!,,.):i
1 ), i -l ). <a:7', 7
Lancasler Laboratoies
2425 Nerv Hollano Plke
PO Bor 12.ili
Lancaster P- 176C5-2425
717-65o-:i00 Fa). 717-655-26Et
MEMBEFI
5ee reverse srde lor exptanatton of svmbols and abbreviatrons 2215 Rev
Lancaste r Laboratories
A Thermo Analytical Laboratory Pag e:2 ol 11 Il
}T
]l
Il
LL,I sarnple l{o. EL 25ISOC'5
CoI lcctcd: Lizcr/91, ar l'1 :D0 by ER
Su5rli tt".d: 6/23/96 Reoortc'd: 3/ ligb
Discard: 8i 9/96
CU-2 Disc. Grab UaIer Sample
Hercutes: Bacchus Pond
C2DSC SDG/l: liEP!'l -07
CATrio. AiItLYSIS UAl.lE
Iii-. Volat'i Ies by 8240 - 'Jater
Cli t orotrrettrgne
B roltolnet.h aneVinr'i Chicride
Ch loroetlrane
l'lerhy I L-n€r C\ L or i de
lic e t one
li,;-bon DisuLf ide.
1,1-Dichlccoethene
1,1-Dichloriethane
Chloroforrit
1,2-DichLoroethane
2 - !l ut traola
'1 ,1 , 1 -T ri:lt'.oroe-thane
Crli Don Terrach l.oriae
\: i rr'/[ A.:ct:te
6 l circd i ct.i L oiomethane
i . 2 -D i ch !oroproD.rn.-
c i s -.1, J -D'i r:r-, Iorc,pl'cp:ne
T i'i clr I oroet h ene
! i broftroch L Droinethane
1, l, 2-T ri c!r'. oroe.rrrane
B a rr: *ne
t rani- 1, 3 -D i ch Loropropene
3 ictriol: orfll
4 -ilerhyt -2 -pentanone
2 - Hexanc,ne
let rach L iloetherre
1, , l ,2,2'I err ach I croethane
"' o l. uetre
Cii I olobelrzene
Et!-'yIberrzerr.'
I r)/.eric
iyr.ene (tcrat)
trans- 1, ?-D i ch loroethene
c i'i' 1,2'1 i ch L oroeti)=nx
Quesi ron;? Contact yc,Jl
Rache:r.'-. Kr(,:l,r<:
I
iAccount llo: 067'16
ili.,r;ul,es, incr:porated - DE
I Envi ronnent:il ,\lfa i ls
i !i lrnincron l-''! 198c4t-
I
P.U.
?ei.
AS RECEIVED
t1E T t-loD
,:,,,,,1i,,,,,,.,;i,,iiiif Si.i] s,,,,,, DETE cT I c''l L I r'1 I T ur ! I s ll
ll
il
rl
I
I
il
jl
I
I
I
2
,l
C L i er! Scrvi ces RepIes9n!al 1 \'e
at (7'.7) 6.5c-2:1..r0
Lancaster Laboratofles
2425 Nerv Holland Pike
PO Box 12125
Lan(asler. PA 1 7605-2425
7 17-556-iJ'00 Fax 7l 7-65b-2681
Respectiul Iy Submi tted
l''r clre'.e I'icC'.ari n, B.A.
6roup -eader, 5ClMS; Votati les
See reverse Srcie for exolanalron c' svmbois anci aobrevralons 22 1 6
I
Rev r0/30/e5 i t
l'
I
I
I
I
(iI)La ncaster Laboratories
A Thermo Analytical Laboratory Page: 3 of 11
LLI Sarnp)-e No. EJ.Cottecttd: o/?oi96 at 1'l :Cr(l
Subnritted: 6/28/96 Iieportc-cl:
D i scard: t1/ 9/9t,
CU-2 0isc. Grab Uater Sirnpl.e
rlercuIes: Eacchus Pond
C2DSC SDGI/: ll0P01 -07
ANALYSIS IIAHE
SlJ846 Serrri vol ati I es:/lJaters
3918 phenot
3gb7 bis (2-chtoroethyt) ether
3bl t" Z'ch ! orol.rheno i.
1383 1,J-dichlor.rbenzene
l3B1'1,4-dicniorobcnzene
iS82 1,2-Cichlorobenrcne
4oBC 2-ilethytphenoI
1o81 2,2'oxybis (1-chLoropropane)
1682 4-irrethylohenoI
39i5 ll-ni trosoCi -n-propy!aoline
JID? hexochIoroetharre
39'10 ni trobenuen.-l9A!, i sophorone
391 1 2-ni trophenolit90 2,4-dirr:erhyiphenot38.56 bi s (2-ch i.ocoethor.y,l rnethane
-'r85o 2,4-dicirior-cphenot':ri2', 1,2,4-trichtocobernzene39!6 ni.ph rha L ene
337", 4 -ch Loroani L inej;ilO hexach I cro5utad i ene
itJ72 4-chtoro-3-nrethy'tphenol
i905 2-fiiethyInaoirrhaLer]e
3i0i hexacirlorlcycLopentadierre19?5 2,4,6-trichiorophc'rrot
3q?2 2,r{,5-trichloroohenri3:t7i 2-chtolorrachthaiene
i907 2 rritro.:nilineiii9'l ciiiilethyt phthalatej!58 arcerraphthyiene
nccount No: C6716
i.tercules, !nco.pcIated - DE
Envi ronr)cnt.1 L Ai'ra i ts
l'i Lrlinqton !i 19lJ?1,
A9 RECE I VED
:::t:-::::.:..: : l'lETilcD
,,,jtE'SU'-l:i ", DETE:Tlr'l Lll'1lT Ull:IS
25i3C05
b)' Sii P.0.
Re[.
F. t 1 tO/,
I ral
TCL
I
t
I
I
t
I
I
I
I
I
I
I
I
'1.
?
ouestrons? Contarct yn':r
Rachr:l ',. Kac'a,r.3.
Cl reni Seivrces Repre:;en:rttve
a: t.7^ 7 : 6l;o- 21-r0
Respectfut ty Submi tted
Chr'rsrine :'l- Rarctif{, B.S.
6rcup -esder, CC/HSLancaster Laboratofles
2425 New, Holland Pike
PO Box 12425
Lancasrer. PI\ 17 645-2 425
717-65c-2100 Fax [phone]Ei
GMEMElEFt
5r'e reverse sroe ior exolanalron oi svmbois and abbrevratrons 22l6 Rpv lo/3o/gt ?G
ancaster Laboratories
A Thermo Analytical Laboratory Page: 4 of 1l Il
Il
Xl
]l
Il
xIt
.ri
LLI Samnre No. El, 25lS'336
cottectcd: 6/26/90 at 11:00 by 8R
Suboritted: t'/28/96 PeoorIsci: B/ 1i96
Di scard: t,/ 9/96
CtJ-2 Disc. Gt'ab Uater SatnPte
HercuIes: Bacchus Potrd
C20SC SDGII: ll3P01 -C7
CAT
lIO. AI,IALYSIS IIAME
TCL SU846 Senivotati tes/Uaters
3908 3-ni troani l ine
1tJ57 acen.rPhthL'ne
lll93 2,4-dinitroPhenoI
39i2 1r-ni troPhenot
3879 di benzof r-rran
itt94 2,ti-oinitrototuene
-18()5 2,5-dinitro!oLu€'ne
lt67 ciicthyL Pirthalate1875 4-chIorophenyL PaenYI ether
33911 1'!.uorene
1909 1,-nitroanitine
4e83 4,6'-dini t;'o-2-methy!phenoI
5914 ti-ni tros...rdiphenyialrt!ne
3569 4'brornophenyl phenyl ether
31199 hexachLorobinzerrs
:i9,!5 pentachloroolrenoL
1917 phenanthrene
38'59 anthracene
t b8! carbazoIe
3330 di -n-butyI phthatate
1397 f Iuorantltene
1t)^,9 pyrene
3fiA b,.:ryL benzyL Phthaiate1385 3,j' -dir:hIorobenzic{ine
:7r0 benzo (a) antir;1cene
liloE cis (2-ethvihexy'1.) phthaIate
3!7t' cliryiene
1995 cli -n-octyt phthatate
Jji,'l bcnzo (l)) f i.'-tocanthene
:jrl52 benzo (k) fluoranrrene
1'tJt4 berizo (er) PYt'ene3.-,trf i ncleno ( 1 ,? ,3-cd) py!'ene
:,1-{i dit,en: (i,h) anthracene
i3L3 beruo (ghr ) Peryten"'
ouest i ons? Contact
n3cheI r-- Kaeailei
llccount No: C57'16
i iiercui es, :lncocporated - DE
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AS RECEIVED
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Il
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at (7i7) 656-2lC,l
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Lancaster Laboratones
2425 New Holland Pike
PO Box 12i25
Lancasrer, PA 17605-2425
717-650-2100 Fax [phone]ee reverse srde lor explanatron ol symbors and abbrevtattons
MEMBER
2216 Rev ,OOOr* iJ
,!&&
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(I)La ncaste r Laboratories
Account No: "16,71 6
rielcu'r{rS, lnc:rpcrated' DE
! nvi rocncntilL ;1i{a: rs
!r Ltrrinstor .)!: lt'394
LABO!'}TOP.Y CHRONICLE
Page: 5 of 1'l
AIALYST
Susan A. Mcl'iahon
Donna R. Sackett
Donna R, S.ickert
Donn.1 R. Seckert
'-\onna il . Sac ke! (
Don.:a ,R. Sc.kett
Dcnna R. Sackert
Donna R. Sackett
Donna R. Sackert
Donia R. Sirci(ett
Donn.r R. Sack.,rt
Donna R. Sacxett
Donna R. Sarckett
Donna !1.. S,rckett
,-ionna k. Sackert
Christine l'1. Coni. in
Donna R. Sackett
0onna R. S!-1cke-.r
NelLi S. varkaryan
llel ii 5. l.i;riilaryan
l'!aria A. Davenport
David..i . Evans
0avid i. Ev3ns
f-rL
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A Thermo Analytical Laboratory
LLr Sampl-e No. EL 2533C'J5
Cot Itrcreil: Ab/2t'/96 art ]'l :'-'rl hy gR
Su!:rrr i t ted: tt!,i?B/96
CU-2 Disc- Grab Uater Santple
Hercul.es: Bacchus Pond
C2DSC SDG#: iIEI,I1.L17
CATlllr AIIALYSIS ll/rME f4FTtiOD
459? TC!- Votnt i Ies by 821.0 - f,'ater S';-81i,5 8?409
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17 !16 8 a;' i un17i7 8er-yt t iuln
17ati CeCrrrir-r:r
1 75 1 Ctrroriri ulr
1753 Coppc-r
1751 I coit
^,755 Leird
i 758 i'lanlranese
1751 N i cket
1766 Sitvu.r
1772 Z r nc'l3,itl 'JU SU346 ICP Digeit (Ior n.-c)
7ul5 /\feenic TR
TLri(, Seleniunr IR
0359 i,lcrcury57'\3 i",'.r 5i.,3.,6 59 rigest
ANAI-YS I S
TR I AL DATE AI'ID T IHE
1 07 /A3/9(, C71.?
,, 07/15/96 03531 07/''5/9f, C-",511 17/^,5/9o A3531 17 / 1 -\ /96 Cl53'i C7/"5,tc/6 Ci53^, Nl i'.51c1i, 015ii A7 /'.5 /96 l!'ii': C7/^,5/96 A35i', ,7/'i5,tt)6 0i53'. Cl/"5/96 al5i1 07/",:,/96 Cl5i1 a7ilS/96 C35l1. 07/^,5/9o 0353'. 07/1\/96 0:15:i1' a7/17/96 1???^, Lt7 / ":i /96 Ci-ili c7/'5/e6 c153
1 C7/C3/95 1915"r 17 /C2,rcic; 2"t??
1 C7/C?/96 09301 071i.r3/95 2i1'4i 07/t)1/96 213t,
SU-84(,6-llr-rA
5'^ - 34 6, 5l i Lr,\
st;-31r5 5llrA
Si,'-54c,.:'l1rJA
su-a146 6l;:..)A
Srj- -q4 6 (:l i i)A
S''J- 345 ,5li r--rri
s,-'-3,45 6:lirA
c!!-Qli ,1 11ni
si.,- tr/,6, 5: l DA
St,'-8qc 6tliaA
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(-r!-nl; ? rn( 1
sil-3jr{, 61-':,i
c!,-Qtl.11.,1,
S!-545 7i7,-1A
(-!,-i!ii , ?1..
0813 Bllir Herrer Extract i on SU-846 3tiCBt,L7B 'lu:- Sijli/i6 Seflilvoia!i Ies/uaters r,.-3,1r6, 5]7rr;t,b7t, lCl- SUli/ro Semivola:i t€.9/r,ra:ers ti,'-346 3j7Ctr
Lancaster Laboratofles
2425 New Holland Prke
PO 8ox 12425
Lancasler P!, 17 605 -242i
717-655-2300 Fax 717-65o'2681
MEMBEFIR-iI See reverse srde for explanatron oi symbols and abbrevratrons 2216 Rev l0/30/95
QUAI,fTY CONTROL REF'ORT(I)Lancaster Laboratories
A Thermo Analytical Laboratory 1l
]l
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Sa{Irp i e
M].} L
SalrpIe
utilIS
Vor.at i lc-s try 324C - 'JatL-r
5??7?7
I nr:or":.orateC
i53 Ch r. orornethane3. trg/ t
257 Brc,lloflreth"rne3. u9/ Lt*ct? V'i nyl. Chtoride?' ug/t
Aqq Ch Loroethanrl
t-97 MethyLene Chlorli.-
7. ug/ L/,98 n c€.tone6. ug/ [
1,99 Car'bon Dtsr.tLf ide
3.ug/ I
500 l, ! -DichILrroethene1. us/t
50'l 1,'l-Dtchloroetharle2. u9/ L
503 Ch I orof orrrt
1. trg/t.501 1,2-lt ich toruethatte
?' uglt'
:216 2 - Butar)one
3. ctg/ [
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t-u9/ t
i506, Carbon TetrachLoFlde1' u,/t
irOT Vi nyt Acetate
2.ug./ t
,9CB Brc,moclichIoron]ethane1. rg/Li5Jq 1.2-Dichlr,r'or)ropane
1.u,J,'L
,516 cis-'1,3-Dichl oroocoPene1- ug./t
J511'l"richtoroerh*ne
1- ug,/t
35 12 D i!:t'ornochIorottrethane
?. lg/t
ii1 5 1, 1,2-TrichLoIoethane
r.rg / t
ugl t
351C trans-'1,3-DichLoropt'o;'ene
L'S,/ I
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Lancaster Laboratones
2.125 Neu, Holland Prke
PO Box l2;15
Lancasler. Pi 1 7605-2.115
717-65c-:i0C Far 717-65c-2681
?.
35'l 5 Benzene
1.
7
cff
9a
,,|:?
67
75
11;
11i
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't"l1
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99
c)a
97
105
37
68
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91
72
106
iDC
109
100
97
1 ',10
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'1 01
101
101
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99
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5ee reverse side lor explanatron or symDols and abbrevratrons 2216 Rev 10/30/95
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(I)La ncaster Labo rato ries
A Thermo Analytical Laboratory
7.. 90
la d7
e,2 t5
''10{, 1 C5
7?. 91,
1Ci 1 05
101 ]rr'1
"! 10 "c9
icz - 1a?
't c3 103
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1!6 1C2
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-77? -7?9 (2)
1C5 1t6
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97 97
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78 79
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59 61
94 95
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Page: 7 of 11
B0 120
80 120
80 1?0
30 12C
80 120
B0 120
B0 1?0
80 120
80 120
B0 120
80 120
s0 120
80 120
LLf sample No- 2538C)C)6
CtJ-2 Drsc. 13r',ib Ua:er Sanrple
HercuIes: 0acch,.rs Pi,nrl
Sirtrn 1 e
trIlTc
f.ouo rir- 5??7?7
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E I.ANK
LCS
R:'D
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LCS
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MEMBERKrIrI
Ldncaster Laboratones
2425 New Hollaod Prke
PO 8ox 12425
Lan(aster, PA I 7605-2425
7l7-656-2300 Fax [phone]'t
o
?.
Qr_TALITY CONTROL R.EPOF{T
5e€ reverse srd€ for explanatron of svmbols and abbreviatlons 2216 Rev.10/30!95
(I)Lancaster Laboratories
QI-IAL]TY CONTR.OL REE'ORT
Page: B of 1'l
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A Thermo Analytical Laboratory
l,I-f Salnr,r e I.lo. 25lti0/,J5
Cll-? Dirc- r-';r iiii Uaatr Sarrrclr
Herct.rl.es: Biicchus Forrd
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7 !.lercury
!l .0ni ug/ t
I TCL S'.;8d6 SeinivoLal iLes;/laiers
]}1 q nlr,,nr, I
1 . r-rg/ tS:ol bis (2-clrloroethyL) ethet
'1 .ul,/ LtJ74 2-ch!.oropnvrruI
'l ' ui1/ L
!33 1,3-dichtt,ri;benzene
'1 . ug.i I
3a.4 i ,4 -dich Lolcherzen.
1' ug/i
lt:i2 1 ,2-d: chii.r'iibc'n:enr,
1. uE./L
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2. tE/ 1.
c.l:? lr-nlt:i!ri,lptr;r:oI
?. u-q/ t(,'t5 u-ni trosodi -n-oropylarrine
?. u9.'[,A2 hexaslrtocoelhane
?. Li:j/ L:)1.0 ni t roben:rrrc
1. rr!1 i:;i4 l sophr,!^one
'l ' ugr'L91I 2-rriirophenoI
2. ugz It')C 2, z, -di;us=rhyl phenoI
1. ug,/t,l:(' bir: (2 clrLcir';ethoxy) nrethane
1 . r"rgl L",r 2, l -Ci :frt;,roplrenoi2. ug.1 L'','?'l 1 ,? ,1, - t; t r:ii i or ob!,nzr:ti
1 . ttJ,/ L:ll): nalrlr r. ita L r', rt:
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DUP !,,IS
RFD I'1S I'JSD RPD
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tCS DUP RFD
LCS LIltlITS
LOW HICH
B0 120
B0 120
B0 120
80 120
5
i?
23
,1
?0
i2
l+6
36
5
1
lr0
35
21.
29
32
33
39
11
21
0 (i) -41
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0 (1) 101
0 (1) 79
-34
':02
102
79
103
1C3
'1C3
93
5
1
1
0
,i9 t'7
91 91
3!, 39
7s 32
tl L{3
79 82
?1 32
t= 4i
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1 10 '^,14
7? 73
c)7 97
'l crc 100
91 95
66 70
90 90
96 86
79 81
35 33
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0
1
7
0
0
l
0
114
B8
B5
63
7C
71
77
6ll
78
103
)J
94
92
65
B6
b4
7A
B1
11?
158
134
17)
129
123
166
152
230
'1 13
'lB0
196
1A)
'1 19
1Bl'
135
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Lancaster Laboralofles
2425 New Holland Prke
PO Box 12425
Lancaste( PA 176C5-2415
717-656-2100 Far 117-55c-2681 r)1( e6' ,n,ln,qq *!
MEMBEFI
ieo rpvcrse srcie ior exolan:tron nl <vmnni< ^n.i Ahhrpvretrnn<
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QUALTTY CONTROL REPORT
Page: 9 ol
Grcrup Ho- 5?2727
l-erc,tles;, Incoaporated DEi
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DUP !!s
RPO
2
7
1
,l
5
3
1
1
0
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2
LCS tCSLCS DUP RPD
LCS L IMITStOI/ HIGH
17 116
2t+ 116
?? 147
23 123
1 100
37 1t11
39 "!5 1
60 118
53 143
1 112
33 145
7
1
1
2B
39
50
1
25
59
38
1
[,,
3900
lu"
3905
l*'39'23
l"::
I;1
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4-chloroanitine)ug,/ t
hL.xach I orohutacil ene
1. ug,/t
4 - ch I oro- 3'nret hy I pht:no I
?. t-tql t
2 - fire thy I naph th a I ene
1.u9/ t
h exach I orocyc I opent ErC I ene3' u'/i
?, 4, 6- rr ich Ioropheno l.1. ug/t
2,4, 5 -trt ch LocophenoI
1-u9,/ L
2 - ch t oronaoh tha I ene
1 ' ug/t
2-ni troani I ine1. us/t
dinrethyt phthaiate3' ut/L
acena.)hrhy I ene
'1.u9/ L
65 69
91 93
86 87
51 53
39 87
99 38
9i 9C
97 97
5t il
92 93
80
93
41
oal
95
99
64
c3
n?
AL
67
73
45
91
80
41
91
9C
B8
95
25
B6
SU8l,6 Serrri vota: i IeslUaters
#:
t{"c)3
to,,
1179
Jnc3!j95
ffl
J:::
/,683
I
3-nitloaniIine1. u9/1,
ac enaph thene
1-ttg/ t
2,4-drnitrophenol5. u9/ |
4-ni trophenot).ug/ t
di benzofuran
1 ' uglt
2,4-Cin'i trotoIueneZ- us/ L
2,6-Cini trototuene
'1.us/ I
dicrhyt pnthaLate
2.ug/ t
Ir-chtorophenyt phenyt ether
?.
an
93
37
l+5
8B
96
100
L<
102
9B
B5
61.
1
0
'10
)
,l
,1
1
2
1
4
0
5
BO
87
92
55
B5
91
95
,9
101
98
B6
82
143
tq)
191
132
"t3't
139
158
1U+
158
121
122
181
1.
ug/ L
u9/'t
4-nitroan!line
ug./ I
4, 6-di ni t ro- 2'rnethyt phenoI
5. u9/1.
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Lancaster Laboratofles
2425 New Holland Prke
PO Box 12425
Lancaster. PA I 7605-2::25
717-656.110C Fa>. 71r-65o-2trri I
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{i\ La ncaster Laboratories7 A Thermo Analytical Laboratory
LLf SamF,re No. 25-1S0C)5C';-i Di9c. Lrzlb "iatel Saolete
HercutL's: B;rcchus Pond
San,pte Sampl e
i{r_LN K
ti.7 .
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MEMBEFt
5ee reverse srde ior exolana(ron of svmbols and abbrevratrons Rer 10./10/95
QUALITY CONTROL REPORT
LLI sample No. 25-180C6
Cil-2 Di sc. Grab Uater Sanrpte
Hercr.ttes: Bacchus Pond
'6roup llo. 522727
I iiercutes, lncc.Dorated - DE
38 86
83 87
96 94
45 40
9' 94
83 87
9? 90
39 87
90 39
93 91
o? cn
79 7g
8b 35
]02 10 !
91 91
1C0 107
90 83
95 95
83 83
76 75
88 86
7t4 7L
Page: 10 of 1 1
LCS LIMITS
LOU HICH
33 147
53 127
1 152
14 176
54 120
27 133
40 137
1 118
26 137
5? 115
1 152
1 262
33 143
B 158
17 168
4 146
2t+ 159
]',] 163
17 163
1 171
1 227
1 219
(il)Lancaster Laboratories
A Thermo Analytical Laboratory ]l
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Sampte SampteMDL UNITS
914 N-ni trosodiphenylarrrine
?' ug/t
8b9 4'bronrophenyt phenyl ether
2. u9./ L
899 hexachtorobenzene
'1 . ug/l
91o pentach IoroPhenoI1- ug/li)17 phenanthrene
'1 ' us/t
359 anthracene1. ug/t
|CA carbazote1. ug/t
830 di -n-butyt phthaIate1. u9/1.
,397 f tetoranthentr1' u,/L
,919 oyrene1. Lrg/t
;370 butyI benzy( phthatate?' us/ t
;3U5 J,3'-di cn IorobenziCine2. uS,/ t
i8,4.0 ben:o (a) anthracene1- trg/I
:868 bis (2-etlrythexyt) phthalate?' u!/Lt876 chnysene1. ug/t
';8,qi di -n-octyI phthatate2. uS,i t
3861 benzo (b) fluoranthene?. ug,/ L
3862 benzo (k) fIuoranthene2- ug/t
15L4 benzo (a) pyrene2. ug./ tl90l indeno (1,2,3-cd) pyrene2' u'/I'
3881 dibenz (a,h) anthracsne?' u9/ t
33,t1 benzo ( gh i ) oeryI enc:?. ur,/ t
8',ANK
r,t .3 -
N.l.
N.l.
N.',
t! n
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ti.!.
li.l.
N.C,-
N.3.
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N.l.
i\".9.
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I'.ISD RPD LCS DUP RPD
DUPRP3 I'1S
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2
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0
'1
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2
1
2
3
2
0
'1
0
6
2
C
0
1
?
,l
a/
85
I5
90
92
B5
B9
oaOJ
83
92
8?
B4
102
90
104
B9
94
B,]
82
94
77
Lan(aster Laboratofles
2425 Nen,Holland Prke
PO Box 12J15
Lancasler, Pf 1 7605'2-125
7ll-656-2r'00 Fa\ I 17-65c-2681 iIMEMBEFl
Se+ rsverse srcie io'exDlanatron ol svrbols dno dborevralrons 2216 Rev 10/30/95
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(iI)La ncaster Laborato ries
QLTALTTY CONTROL REPORT
Page: 1 'l of 1 IA Thermo Analytical Laboratory
LLI sample No. 25380C'16
CtJ'2 Disc. Crab U3rer S;rmpte
HercuLcs: Bacchus Pond
Group No. 5??.727
liercuLes, lncorporated - DE
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SURROGATE SUHI'lARY
TRIAL ID SURROGATE RECOVERY %
/+59? ICL Votatile.s by 8240 - Uater d4-1,2-DCA 102d8-toluene 10?EFB 97
t 678 TCL SU3{6 Senrivolari tes,/Uaters 2-Ftphenol 51,
Phenol -d6 33?,/,,t'-lBF 82
\679 ICL SlJ846 Senrivotati tes/Uaters Ni trobz-C5 8l
2-Fbi ohnyl BB
Tphenyld 14 SB
SURROGATE
L0u
76
oo
B6
21
't 0
10
15
jj
LIHITS
HIGH
114
'1'l 0
115
100
9lr
123
I l.+
116
1l+1
MEMBERrlir Lancaster Laboratones
2425 New Holland Prke
Po 8ox 12415 ,!-
Laniasrer PA 17605-2Jl: ?_;-i-.Eq:,':11 F:, ^ ::qi );"' ,^,,,",-,11-rr'a'.
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(iI)Lancaster Laboratories
LLI sample No. EL 2533C05Co[[ccted: 6/26/96 at 10:45 by BR
Subflitted: 6/28/96 Reported: S/ 1/96Discard: 8/ 9/96
CU-l Oisc. G.ab Uater SampLe
I Account No: C6716
I liercutes, In.o:porated - DE
i Envi :onnpn::. A{iairs
i ',Jr lmington rt !9994
l
A Thermo Analytica I Laboratory Page:
P.0.
Ret.
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Respect{ul ty submi tted
R;rrona V. Layrnnn, C|oup Leader
I rjq Me!a r, ::./Leacha tes
1 of 11
al-
2216 Rev ,Orrorr, ?aS
Hercutes: Bacchus Pond
C3DSc SOG#: HSP0 I -06
CATNO. AIIALYSIS IAME
1592 TCL Volatites by 3240 - !,ate!'17?2 ThaI t iur1713 AtumintLnr1714 Anc i nony1716 8ar i unr1717 Beryt I ium1749 Cadmiun1751 Chrorni un1753 Copper175L ! ron1755 Lead1758 14anganese1761. !l i c ke ti7o6 9i lver177? Zinc7035 Arsenic TR
7C'36 SeleniLxn rR0259 l.lercuryt'673 TCL SLJ846 SernivoIat i r.es,/Uarers
4b79 TCL S1,,8{6 Semi,;otatiLes/rJare!-s
YETI,iOD
DETECT:CI LI!1IT UTIITS
AS NE'E!VEO
See Page
uq/ t
u9/ L
u9/ L
u9/ |
us/ !.
19/ !-
uq/ i
19/ t
r9/ t-
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See 2age
!ue Pa.-je
1 COPY T0 HercuIes, lncoeoorated
1 CoPY I0 EllI Rccky l.iLrunliin
Al'-'l: l/r'- Joseph Ke:ler
AIT'i: rlr. Erent Robinson
Ouestioils? Contacl yolrr CLi:nt Servi.L': QecresL'n!al!ve
Rachet L. Kre3rner at (7 i) 6i6-2li)0
MEMBEFlrlkm
0l:i6:58 D 0';02 l5 REP "t?c/.|,s 5?2t i7110 15.00 3r:1027C0 ASRCI ar
Lancaster Laboratorie5
2425 New Holland Pike
PO Box 12425
Lan(aster. PA 11 605-242t
717-656-2100 Fax 7l 7-556-268 l 5ee re'rerse srde for explanatron oi symbols and abbrevidtrons
(il)La ncaste r Laboratories Page: 2 of 1'l
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A The rmo Analytical Laboratory
LLf sample No. EL 2538C05
cottected: 6/26/96 at '10:45 by 6R i Account Io: c67i6
i Hercutes, 1n:orporated ' DE
I Envi rorrnentc: Af fai rs
I ui lmington !5 19894
I
P:0.
Rel..
Submitted: 6/28196 Reported: 3/ 1/96Discard: B/ q/96
CU-3 0isc. Grab Uater Samote
Hercutes: Bacchus Pond
C3DSC S0G#: i{8P01 -06
CATi,IO. AIIALYSIS NAME
IcL Votati tes by 82(0 - I'later
1258 Chtoromethane1?57 Bromomethane3492 Vinyl ChtoriCr'1!91, Chtonoethane3497 i'lethytene chtDcide3498 Acetone3499 Carbon DisuLficle3500 1,1-0ichto!'oerhene3531 1,'l-DichLofoerhane3503 ChIoroforrt3504 1,2-0ichtoroethene0316 2-Butanone
3505'1,1,1-T.ichloroethane3506 Carbon TetrachtoriCe3507 Vinyl Acerate5508 Bromodi ch I oromethane
35Oq 1,2-DichloroproPane
35 15 c i s - 'l ,3 -0 i ch torop.oPene351'l Trichtoroethene!5i2 Dibrornochloroflrethane'a5',3 1,1,2-Trichloroethanel:15 Benzene3510 trans-1,3-0ichtoropeopene3518 Bromofornt3521 4-l',tethyt-2-pentanoneli20 2-Hexanone3523 TetrachIoroethene3513 1,1,2,2-Ietraclrtoroethane35ll- Tol.uenei525 ch Iorobenzene1525 Elhytbenzene3:23 Sryrcneli29 Xyl.ene ( cotar. )5780 trans-1,2-DichIoroethenec?58 cis-1,2-Dichlorserhenc
1lA9 RECEIVED
MET HOO
111i'..,,r1i1i1i!ui.I.s,r:r:.i;: DETEcT I 3ii L t !'! I r uN I rs
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ouestions? Contact yorr Cl.ient
Rachel- L. Kreirx,ll'
Senzices i?ep{ e:rentat ive
ar (7''17) 656'ZlC0
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TAkm
Lancaster Laboratofles
2425 New Holiand Prke
PO Box 12425
Lancaste( PA 17 645-2425
1 17 -655-2300 f ax 7 17 -6\6-2681
Respectfut Ly Submi tted
Ficrele !tcCiat'in, 5.A.
Sioup -eader, 5C/M9 Volati Ies
See reverse srde ior expiaoatlon oi symools and abbre'rratrons 2216 *"r,Orr.rr, {}
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(I)Lancaster Laboratories Pag e:
LLI Sampfe No.
Cot tsctBd: 6/?6/96 ar . Account flo: 0571,6
ljcrcutes, ll.lcorporatad - 95
I Snv i ronrnenra i. Al f a i rsili lrrinoron ,E l9U9i't_
AS RECE IVED
.,,,tE5!'.I5 DEIECTT9T{ LIr,!!T U}llTS
ugl i
'rg/ -
'Jgi i.
v9/ t-
!9/:-
,:t/t.
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uL-'l'-
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Serv i ces RLrPaeSentat i vL.
a. (1'7) 6!o-2llLr
EL 253St\C)5
1C:45 by 5R
A Thermo Analytica I Laboratory 3 of '11
2216 Rev,OOO,* d?
P-0.
liel.Subnitted: 6123/96 ReDorted: g/ 1/96Ciscard: 8/ 9/96
CU-3 Disc. Grab Uater Sampte
Hercutes: Sacchus Fond
CiDSC SDC#: llBPO'l -Co
CATNO, AHALYSIS NATE
Tcl- SL,846 Senrivol.ari Ier,/uate!-s
3918 phenoI
3867 rcis (2-chtoroethyt) ether
-i874 2-chLorophenoL3i83 1,3-dichLorobentene333/. 1,4-dichtoro;rL'nz*nefrl82 1 ,2 -cli ch Ioro:en:ene/,;8t-1 2-nre'thytphe:tol.4i,81 2,2'orybis (l.ifrr.oroprop:,ne)
4o:!2 4-rnethyIpirenor.l')15 N-niti'osoC1'n-prooylaminc
-:,tl.l? lrL:xaclli.!r,afIi:=
=t)iD ni trchenrene!;)C4 ioophorr-r.e
l?1 i 1'r:i troptsnoL-tL)c)D 2, ,i - d irr'el Iy: Dheno Iil,L6 bis (2-chio:-Jer:loxy) :retrrane1335 2,4-dicni.orccre:,.'.lCli 1,?,4-trich'!crolenzene39U6 naphth:Le:re1al1 4-chtoroani Line3QDd lie.\ach Iorobut!(: iilrr'3!t72 /r-chLoro-3-rneiirylohenol
:.:i05 2-;;e(hy(na35:ha:(:ne
-1tC I frexJch t orocyc L o.Jcn r:d i enr-3r?a 2,4,6'trichlolopheioI3r71 2,4,5- r''ir:lr'roropilrnDL:8iJ Z-chloron3ohrheiin"-jAD7 2-nitroaniLir:ei3.," diilerhyt phrhai3te!ni& ;rcen.rph chy I en:'
Ouestrons? Contact yo:r Cl. icr:
Rl:rr:1. L- (aE:lnei
Lancaster Laboratofles
2425 New Holland Prke
PO Box 12425
Lancasiei PA 17 605-2425
717 -656-23AA Fax: [phone]
Rescectfut Ly Submi ttedC:ristine )!. ?.ar:cLiff ,
C. o,]p :etC!'r , CC,/!1S
See reverse srde ior erplanahon of s/mcols dnd abbre',{atronsTIKTfT
(I)La ncaste r Laborato ries
A Thermo Ana lytica I La boratory
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EL 25-rSL}05
'I '-1: 45 by 6R
LLI Sample No.
coI tected: 6/?o/96 at I
i Account llo: :167'i6
I Hercuies, incorporated - DE
i Envi ronmentai. Af tai rs
i ti trnington ?: 19t194
i
Page: 4of 11
P.O.
ilet.Sub(ritted: 6/23/96 Repocted: S/ 1/96
Di scard: Bl 9/9t)
cU-3 Disc. Grab Uater gampte
tlercutes: Bacchus Pond
Closc SDG#: tl6P01 -t15
cATNO. A!.IALYSIS IIAHE
TCL SU846 SernivoIati Les/Uaters
3908 3-ni troani I inei857 acer,aphthLrneZ!393 2,4-dinitrophenot191? 4'ni trophenol3379 di Lrenzotut'an389/* 2,ti-dinitrototuenei895 2,6-dinit.otoLuene1387 diethyt phrha!.6ii3875 4-chtorophenyL phenyl eihec3399 f Iuorene3909 4-ni troani t i ne4583 4,6-dinitro-2-rrrerhyLphenoI39it, N-nrrrosodiphenyta,rrirre1869 4-bconrophcnyl p:renyl ether'1|\99 hexaclrtr:robcnzcn.-'7916 pu=ntach(oroDherroL3917 phenanthrene3859 anthracene1b8,4 carbazolei880 di -n-butyt phiha',ate3397 f Iuoranthene3419 pyrenelC70 butyl benzyl phthatate
i835 3,1'-dichl.orobenziCine5B6C benzo (a) anthracene1968 bis (2-et\Tthexyl) phthalate
337o clrrysene1396 di -n-ociyt phthalata38,11 benzo (b) fIuoranthene5tJt'2 benzo (k) fluoranthene38$1 br)r.zo (a) pyrenc'lgtll indeno (1,2,J-cd) pyrene
3E8l (iiDenz (a,h) anthracene3363 benzo (ghi) perytene
AS RECE!VED
METJICO
DETECI!O}I LII!IT UNI TS
ouestions? Contacr your CIient
Rachrl- L. Krcarnler
Servi ces !leFresenla! i ve
at (7',7 t Lt6'?.3.11
TAkm
Lancaster Laboratofles
2425 New Holland Prke
PO Box 12425
Lancaster. PA 17 605-2425
717-65&2300 tax: 717-656-2681
Sespecifut ly Submi ttedChr:s:ine !!- RarcLi ff ,Croup ieader, CCll'ts
See.everse srde ior explanalron of:Trbols and abbrevtations
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Rev 1060/95
08r3
/,678
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(iI)La ncaste r Labo rato ries
A Thermo Analytical Laboratory
L\BORATORY CHRONICLE
Page: 5 of II
AIJALY S T
Susan A. llcMahon
Donna R. Sackett
0onna R. Sackett
Donna R. Sackett
0onna R. Sackett
0onna R. Sackett
oonna R. Sackett
Donna R. Sackert
Donna R. Sackert
9onna il. Sackert
Conn3 R. Sacketr
9onna R. Sackettlcnna t:. Snckett
Conna R- Sacketi
Sonna R. Sackett
christine H. conlin
)Dnna R. Sackett
)on.ra 9. Sackert
lletii S. l,lackaryanNetLi S. ttarkaryan
l'!aria A, Davenport
Oavid i. Evans
David i. Evans
LLI Sample No. r'L
cottecred; 06/26/96 ar 10:45
Subnri tted: C6/?8/96
CU-3 0isc. Gcab Uater Sanple
HercutL.s: Eacchus Pond
C30SC SoG#: HBP0I-06
CATNO AIIALYSIS IIAME
2_s3SL$_s
by ER nccount !lo: 06716
He.c'Jtes, Inco.oorated - 0E
. Envirorrnenrar- ,\f ia irs
I Ji lmington DE 19094
I
t592 TCL voLari les by 8240 - uater su-846 82408
!,18 TH00
su-846 6C10A
s'J - 846 601 CA
su-846 bd'l0A
su-846 5'J i 0A
SU-346 6J'lCrA
su-346 6:1CA
su-316 6-10A
S,J-84€, o,llCA
S',.J-3',6 5.l1DA
c,' C-,i 1_lrrr
su-814,5C'lrlA
sr-345 0l1irA
S;-i1ro cl:!A
:i.'-i14ct 5i1lri
5i.8i5 l:r?5A
-sL,-3{i c,., t,lA
c!r-l/; -.\".r\
5'J - 84.4 74 70A
S'J-81,d 7"7C4
TR!AL
1
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:
ANALYS I S
DATE A[iI TIME
07/03/96 0604
07 / 1.5 /96 03t 9
07/15/96 03i9
07 / 1.5 /96 n3t-907/15/96
^3!+qc7/i5/c6 i349
07!".5/9t, C349e7/'5/9b CZ!,g
07J15/96 t349
07/15/9c, i3\9
)7/t5ic16 X3;9
'J7/1-\i9(, C3+9
t7/^,5/9o t34?
a1 ,lctaL n1 tdw'!.)11! .J.aa7!'r/94 f,5!,9
17/'.c/9d 1,222
a7/-. -\/16 t)a')
C7./ 15l95 t) jr?
C7 /l-a /96 i9':3
07/)?/95 21?2
07/c2/96 C93D
rt .r J:l1t aJ) |,17/13/90 2A31.
17?? Thattiun1743 Atuminurn
174t, Antimony17!.(' Bar i urr'1747 Beryt L ium17{9 Cadmitm
1751 Ch rorni urn
1 753 Copper
175/, I ron
1 755 Lead
1753 i4anganese1.761 Nickei
17or, siIver177? Zinc
1848 L,lJ 51.,1846 I CP D !gl's t ( tor r:c )7035 Arsanic TR
70-16 Sel.eniLril IR
0259 Mercury5713 UU SU846 H9 Disesr
BNA later Exrracr i on SU-846 ir 1 Cg
TC! SUg45 Serni./cr-ati les/'/a:ers SU-345 8?7,13
TCL SUs(6 Senrivolati !-es/fareri S,,t-8ri6 5:7J3
Lancasler Labo.atofles
2425 Nerv Hollaod Prke
PO Box 12425
Lancaster PA 17 605-2425
7 17 -656-2300 tdx: 717 656-2631iFHfi d35ee reverse sice ior explanat.on of symbols and abbre'/rations 2216 Rev lO/3O/95
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A Thermo Analytical Laboratory
QUALITY CONTROL REPORT
6o{
LCS LI!'IITS
!-CU H I CH
il
llLLr sanpLe No. 25380C),s
CiJ-3 Disc- G16b ,Jater Sarnpte
Hercutcs: Bacchus Pond
1 Group l,lo- 522727
i lie|cutes, Incorporatcd - DE
i
I
SaflpI e
}!DL
Saolp I e
UII ! IS ilLCS !-CS
LCS DUP RPO
DUP MSRPD !'1S I.ISO RPO
L592 ICL Votatites by 8240 - Uater Batch: Iq6]84':AA
1 258 Ch Ioromethane3' u9'/[
1 25 7 Eromomethene5' u,/l
3!,92 Vinyt Chl.orideZ. uS/t
3!+9! ch I oroethane3. ugl tf,'rt7 I'lethytene ChIol"ideZ. u!./ t
3498 Acetone6. ugl!
3499 Carbon Disulfide3- us/|
1500'1,'!-Dichtoroethtne1- us,/ti501 1,',],0'ichtocoerhaneZ. uglr
35C3 Chloroform!. uglt
35{J4 1,2-0 ichtoroethane
?' u9/ t
0115 2-B,Jtanone1. uS,/ t
39C5 1, 1,1 -Trichi.oroethane
1 ' u'/t
:1506 carbon Tetraclrloride1. ug/t3i07 Vinyl AcetareZ. u9/ t
3:r0l] grc'nlodich I Jroorethane1. ug/lliar', i, 2-D i r:l,tc'r'oprooane
'1 . u!/t
.11'15 cis-1,3-DicnIoropropene
1 ,,, tl
i:;'! I -lri(lioroefhq.ne
'1 . L'1./ i
:i I i 0ibror,fl.h l.ororliethane
2. ug,, IZ',1:'1, 1,2-Trichtoroethane2. us/ t-J: Ii llenrane
'1 ' ug/t3iiC tr;.ns- i,3-9 ichLoropr operr"-
1 . tjg,/ l-
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88 81
90 s2
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7t. ??
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103 100
i]5 :c9
96 100
64 97
111 11Ll
99 10/,
93 1 01
97 iC1
ic6 105
87 99
32 96
'I C4 144
91 1t2
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Lancaster Laboratories
2425 New Holland Pike
PO 8ox 12425
Lancaster. PA 17 665-1425
717-656-2300 Fax: [phone]ee reverse srde for explanatron of 5ymbols and abbrevrairons 2215 Rev
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(I)La ncaster Labo ratories Pa-oe: 7 ol 1'l
A Thermo Analytical Laboratory
LLI sample No. 25380t\5
CU-3 Disc. Gcab Uarer Sarnpte
tlercutes: Eacchus Pond
1
I
I croup No- 522727
i ile.rcuIes, inccrporated
i
i
Sampt e Sarnp[ etrDL u[ l Ts
3518 Eromofor-m
BLANK
LCS LCSLCS DUP RPO
102
108
107
r00
OR
97
1A7
1C'!
111
',02
103
10t,
1C0
i!sIISD RPD
DUPRPO MS
LCS LIi!tTS
LOU HIOH
I . ug/ t [.3. 71 9035?1 4-l.tethyt-2-pentanune5. ug/t N.D. 65 93
3520 ?-Hexanone7. us/t !i.!. C,? 95
3522 Tetrachtoroethene1. ug/L N.!. 1C6 i053521 1.1,2,?-1 e't.rachtoroethane2- us/ t N.D. 77 91
3521 fotuene?. u9/ t N.:,. 1C5 1 D5
3525 Ch I orobenzene1. ug/t [.0. 101 iC1
3526 Ethytbenzene?. u9/[ u.). 'l '10 1C93523 stynene1. ug/t N.r- i1z 102
35?9 xylene (tDtat)1. uc1/l N-0. 1CS 1CB
5780 tranr-'1,2-0ichtocoethene2. ug,/ t N.9. 1C1 99
6263 cis'1,2-Dichtoroethane2. us/ | N.9. 106 102
1722 Thal. t iurn satch: 961921818302170. ug/t N.r. (1) 101 rof
17(3 Atuminurn Barch: 96192.1848'.102
57 . us/ t !(.0. 174 -772 -729 (2)
1744 Antimony Satch: 961921848102.15. rrs,/[ N.D. (1) 105 1C6
1745 Bariunr Barch:96i92"!818t02?.2 ug/t ii.9. 0 (1) e7 38
1747 Beryl t iun Batch: 96'19218483C21.1 ug/L 0.0016 J nqi i. (i) 97 97
1749 Cadrnir-rm Batch:9.i1921e(93122.7 ul/t ri.). (1) 9/+ 95
1751 chromium Satcir:96192181,3r1C2tr-3 ug/t :i.9. 0 (1) 78 79
i753 copper Batch: 96'19213431C2i.S ug/l N.0. C (1) -2A1, -':91
1754 I ron Barch: 96192181,3,1025.9 uglt 0.0607 J m9/1. 174 -1313 -14t+1, 12)
1755 Lead Batch:951921t1,ti:rc218. us/t N.D. 0 ('l ) 92 93
1758 Manganese Batcir:961921843'lC22.9 uslt N.c. 0 (1) 59 51
1761 Nickel. Sarch:95:92181,8aC25-4 ug/t N.s. 0 (1) 94 95
1766 Sitver Batch: ?5]92]8{81023.6 ug/t l.l .). (1) e9 101
(1) Ihe resul.t for one or both dete.firnations ras Iesi than five tinps the r-CO.
(2) The background resutt xas more tr')an four tinres tn: spiie added.
Lancaster Laboratofles
2425 New Holland Pike
PO Box 12425
Lancaster. PA 11 605 - 2425
111-656-2300 tax:711 656 )AB1
z4
2
36
0
0
?
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5
4
1
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80 120
80 12C
80 1?O
8C 120
BC '120
Bt 120
80 120
80 i20
B0 120
80 n,20
80 120
7Xm
QUAL]TY CONTR.CL REPORT
See reverse srm for exolanatron of s/rbo,s and abbrevratrons 2216 Rev ,orror$ dtp
(l)ancaster L
A Thermo Analytical Laboratory
QL'AIITY CONTROL REPORT
Page: 3 of 11
tcs
101
1Cl
103
9l
LCS LCS LCS L1MITS
DUP RPD tOU H I GH
l+/,
oo
B5
70
71
77
64
101
53
9t
97
92
65
B4
7C
'31
5 1'12
12 158
?3 134
1 172
?D iz4
32 129
46 tt5
56 166
5 152
1 2i0
t+0 113
35 1BC
21 196
?9 ',182
3? ]',le
33 184
39 ',ll5
411 11.?
a1 aa1
il
il
Samp t e
HOL
177? Zinc
12.
7035 Arsenic)7
7036 Setenium
SarnpL e
UtI I TS
u9/ t
u9/ t
LLr sample No. 2538C05
CU-5 Disc. Grab Uarer scmpte
Hercutes: Bacchus Pond
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I Group lto. 522727
i HercuIes, lncorporated - DE
i
I
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DUP
RPD l'!SC
'31.
102
i02
79
0 (1) -41
c ('1 ) 101
0 (l) lc1
0 (1) 79
1+9 r+7
91 9',
83 89
78 82
80 8l
79 22
3! 82
67 68
83 83
1 1C 111
72 78
97 97
1C0 '1 CC
9t, 95
66 70
90 90
86 86
79 81
89 88
five tiflES the LCo.
!!s
iPD
1t
tI
2-7 uS/ t
0259 tlercury
0 .041 u9/ t-
5
1
,l
n
TR
TR
ELAIJK
Batch:961921848002
N -3.
Batch:961921848002
ti.9.
sarcir: 961921848102
N.D.
Batch:96-t8457-t3C01
!,1.9.
80 120
80 1?0
80 120
80 120
4673 TCL SU846 Seniivolati l-es/';aters Batch: 96i81'pM026
3918 phenot
'I ' us/t
3867 bis (2-chloroethyL) L'ther
1. u9/ L3871 2-chtorophenoI1. ug,/t3883 1,3-dichtocobenzene1' us/t
3884 1,4-dichlorobenzene1. ugJt
3S32'1,2-dichIorobenzene1. ug/t
4580 2-rlethytphe^ot
z.u9/ t
1631 2,2'oxybis (1 -chIoroPropane)
2. ug/ [
458? (-methytphenot
2. us/ |
3915 tl-ni trosodi -n-propytamine
2. ue/t39n2 hexachtoroethane?' ug/t
3t"10 ni trobenzene
'l ' ug/t
1904 i sophoronr.
1.ue/ t
3911 2'nitrophr'nol2. us/ t
1390 2,4-dimethylphenoi
'1 ' u9/ t'
:tlar bis (2-chloroethoxy) netir:ne1. us/L
1855 2,4-d'ichtorophenoL?. u9/ Lltll 1,2, 1r' trichtot-obenzenc'1. ug/t
3905 naphthaIene
u9l t
3
1
1
5
3
3
1
2
0
I
8
0
0
1
7
0
C
3
0
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I
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Lancaster Laboratorres
2425 New Holland Pike
PO Box 12425
Lancasle( PA 11 605-2425
717-656-2300 Fax [phone]
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QUALITY CONTROL REPORT
Page: 9 of 'l 1
A Thermo Analvtical Laboratory
LLI Sampf e I'ro. 2533CL.t5
CU-l Disc. GIi':b Uater sailpIe
Hercu!.es: Bacchus Pond
,i
I Crouo !,o. 52?7?7 l
1 Hercutes, lncorporated - D€ :
-t
I
Sample SampteI]IDL UN I TS
3?,71 4-chtoroani I ine?- ugl l
3903 hexachtorobutadiene1. u!/l
3372 4-chLoro-l-nrethytphenot2. ugl tl?35 2-rrrethyInaphthaIene'!' ug/L
3r,a1 he^acStorocyctopent adiene3. u9/ L
3923 2,4,6-trich Loropher,oL1. u9/!.
-ai-!? 2, 4, 5 - tI i L:lt !crophenot1. ug/ [
7.,77 2' rh loronapr'th.1iene
'l - us,' l
3707 2-ni troani I ine
'1 - uu/l
1Lr1 dirnerhyI phthalatel. u9/ t
i:jB acenaphthyl.ene1. us/t
1938 3-nitroanitine
1 ' u9/"
3857 acenaph thene1. ug,.[3Bri 2,4'dinitiophenoL5. uS/ Lir'i2 4-ni IroPtren3t
5 - Lrg,/ l.
l!-'? di benlof ur':,i'r
1' ug'/L-::.1!, 2,i-Cini trotoiuene2. ug/ iJ3t5 2,6-Cini trotoIuene
'1 . ug/tl::ir7 dieth)r!. phtiral.are2. u9/ I3\75 4-chLorophenyl pheny!. ethen2' ug/l:liti f Iucrcrre1. ug/t
If;)t 1,'ni rro;rri ! ine
2 . ugi'il.i,lj 1',6-dlnitro-
DUP I'!S LCS !.CS
RP9 MS MS! RP9 LCS DUP RP9
2
7
1
1
5
3
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'1
C
,]
2
t5
15
91
BO
1,1
91
90
8B
95
Z5
B6
180
a87
10 92
< qq
185
19!
195
?59
't 101
493
c86
582
LCS LII'IITS
LO|J HIGH
17 116
2t+ 116
2? 147
23 123
1 i00
5t rqq
39 15i
60 118
53 143
't 112
55 tq)
/ tq)
47 14\
1 191
1 132
23 131
39 139
50 158
1 114
25 158
59 121
?a 1))
1 1Sl1
3 LA NI(
H.!.
r,1.9.
N.i.
N.r.
N.9.
N.D.
N.l.
ti .9.
N.D-
l,l .9 .
N.D.
ri-].
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N.qr .
ri.!.
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N.D,
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65
93
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51
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t9
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97
32
9?
7l+
59
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97
5l
1/
tl3
97
ii
93
467q 1c'- su846 gemivotati Les/tarers Batch: 96i34UA!.026
93
41
t,7
39
95
99
6t1
105
1C2
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67
93
37
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88
9o
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65
102
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TXmI
Lan(aster Ldboratofie5
2425 New Holland Pike
PO Box 12425
Lancaster. PA 11 6A5-2425
717-656-2300 Fdx: 717-556 258l
5_
5ee re,rerse srde for explanairon of symbols and abbrevralrons 2216 Rev ,Orr.r* d?
391.i
3569
3E99
391 6
3917
3359
4.68t4
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39,19
3870
3335
3360
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3s76
3896
3851
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3t0i
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LLI sarnpl-e No. 253800-5
CU-l DiJc. 6rab Uarer Sampte
tlercuIes: Eacchus Pond
Sanpte SampleHOL UII I IS
N -ni trosodi phenyt ami neZ. us/t
4-bromphenyt phenyI ether2. ug/l
hexach I orobenzene1. ug/t
pentach I orophenot1' u'/t
phenan th rene1. us/l
ant h rac ene1. uglt
carbazote
'l ' ug/t
di -n-butyt phthaIate
'1 ' ug/L
f I uorJnthene1. ug./i
Pyrene'l' usllbutyt benzyl phthaLate2' u9/''
3,3' -di ch torobenz iCine2. u-q/ t
benzo (a) anthracene1. u!/tbis (2'erhylhexyt) phthatate2' u'/I
chrysene1. uglt
di -n-octyl phthaLate?' us/t
benzo (b) fIuorantheneZ. us/l
benzo (k) ftuoranthene2. uS/[
benzo (a) pyrene2. ugl L
indeno ('1,2,3-cd) pyrene2. u9,/ t
diLrenz (a,h) enthracene2. uel I
benro (9hl) pL..yLL.ne2. us/ [
I
I Group [o. 522727
i Hercutes- Incoroorated - CEI'
I
QUALITY CONTROL REPORT
P age:
LCS LI}IITS
LOU HIGH
]t
tl
]l
1l
]l
il
il
;l
il
,l
il
;l
I
I
I
t
I
LCS !_CS
LCS OUP RPO
115
!1S I.ISD RPD
96 94
45 40
95 ql1
33 27
c/2 90
3,i 97
9D 39
93 9_1
3l 80
79 76
ot- o<
1,rJ2 ioi
91 9]
100 107
90 88
95 95
83 33
76 75
oo n:
La ncaste r Lab oratories
A Thermo Analytical Laboratory(I)
SLANK
N.D.
N.D.
!.).
N.D.
N.D.
N.?.
N.D.
N.!.
N.D.
il.r.
N.!.
N.3.
N-)-
I.5.
N.D.
N.D.
N.0.
N.!.
N.l.
2
2
2
11
0
,]
?
1
?
j
2
c
1
0
6
2
0
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1
2
'l
B4
85
95
90
9?
B5
B9
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92
a,
77
81,
1C2
90
't04
69
9A
B1
B2
914
77
?a
53
1
14
54
27
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1
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152
176
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t) I
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-1 15
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168
It{b
159
163
163
2?7
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MEMEtERKIIE
Lancaster Laboratories
2425 New Holland Pike
PO Box 12425
Lancaster. PA 17 605-2425
1 17 -656-2300 Fax: [phone] i** I
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See.everse 5roe for e\Dldnatron of symbors and abbrevratroa:2216 Rev 10/10/95
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(I)La ncaste r laborato ries
A Thermo Analytical Laboratory
LLI sampLe No. 2538005
CU-3 Disc. Grab Uarer SampIe
Hercules: Bacchus Pond
459? ICL votatiles by 3240 - uater
4678 TCL SU846 SemivoLati Ies/Uaters
4679 ICL S1J846 Seqivotati Ies/Uaters
i 6roup No- 522727
, !lercutes, lnco.poraaed - DE
I
SURR06ATE SUNI'!ARY
SIRNOGATE RECCVERY ;{
i1,-1,2-DCA 102
c3 - to i. uene 1 ,t10
SFB ??
2-FtphenoL 49
ihenot -d6 3??,4,5-tB? 7D
I'l i t robz -d5 3t'Z-fr:iphnyt 79
I2neny'. d14 E7
SURROGATE LIHITS
LCU
76
QA
O^
21
'10
i0
35
i_<
HIGH
114'lic
'1 15
'!00
9t,
123
114
116
14'
MEMBEFl7Xm
Lan(aster Laboratones
2425 New Holland ftke
PO Box 12425
Lancaste( PA 17 605' 242\
717-656-2300 Fax 717'656 253r
,\D.
2216 Rev ,Orrorn, ?aS
QUALITY CONTROL REPORT
See reve'se s.de ior erplanatron of s/mools and abb,e'r,atrons
II
ll
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II
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1T
ll
li
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(I)Lancaster Laboratories Page: 1 of 11A Thermo Analytica I Laboratory
LLI sample No. EL 253800Scottected: 6/?7196 at 09:00 by BR
Subnitted: 6/28/96 Reported: 8/ 1/96Discard: 8/ 9/96
CU-5 Disc. 6rab Uater sanpIe
Hercules: Bacchus Pond
C50Sc SDG#: HBP01 '09
CATNO. AHALYSIS }IAME
1592 TcL Votatites by 82+0 ' llateri72? Tha[ [ ium1743 Aluminunt1744 Ant i mony174o Sar i um1717 Beryt I iuni7/-q Cadnriurn'1711 chromi uor1753 copper1751 I ron1755 LeaC1753 Nanganese17b1 N i cket1756 si lver
177?. Zi nc70i5 Arsanic TR
7036 Seleniunt TR
C259 ilefcury4o73 TcL 51J346 Senivolrti tes,/lJate!'s1579 TCL S'lB1c, sefl)ivotcr i Les,/uaters
I CCP'i T0 HercuL€.s, I ncorpo.ateC
I CoPY TO ERM - Rock'/ lnount:in
Acco,Jnt No: C6716
i llercul.es, :ncorporated - DE
r Envr conflren:.-,i. Af f air-s
i 'rt lrnrnston lE '19894
AS RSCE M'
P.0-
ReL -
,r?isrlTg
,.: ,, ' tl-!,
6,8+0.
20c -u.r: ,s-1.
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5,:-
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1; ,
!.1:
I'tE r ioo
DEIE'T I'.]Ii LIMIT UVIIS
See Page170. \t/ |
57 . u!/'.
15 . uE/ t
2.? u9,/ L
"' .3 u!/ iJ 4.7 u:/t-
j ".j ,t,]/L
: iI r:/ i
5 -',r trJl|
,tatl
Z-q \g/t
) 5.4 ugli
I .5 u9,/ L
11. Ng/r
? -7 's.i/ t_
a 7 t,,, ll
'i .'Jn3 '::-;i ''
)j< rd!le
see 2aqe
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AIr!: tlr. Jcseph Kclier
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Ouestions? Conrecr your Ctient Servrces Representarive
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RespectfuL Ly submi t t.-d
Rar:rerna V. Leynran, Croup Leaier
I cP lietal s./Lcachatcs
Txnir
Lanca5ter Laboratones
2425 New Holland Prke
PO Box 12425
Lancaster. PA 11 605-24)5
7 11 -656-23A0 Fax: 7'17'656-253 l d?I
t
See reverse srde for explanatron of symbols and abbreviations 2216 Rev l0/30/95
(I)La ncaste r Laboratories
A Thermo Ana lytica I Laboratory
I Account llo1. D6716
riercutes, lnccroorated - !E
I Env!ronxrenin', Atf a irsi';i Lrflinlron lE l9l!94
i
AS RECEIVED
l::ii::,:r;::ij:irli:i:iiil*i::.:::ir:ri:i::::: IIETHOD
:..:t::,i1,,,:,:i :::i?ESLrli g:i,:i. DETECT ! 3i',1 LM I T UN I IS
Page: ?ot 1'l ]l
LLI samp1e No. EL 25-1SCCSCotIecred: 6/27i96 ar 09:C0 by 6R
Subnitted: 6123/96 Reportec!: 8/ 1/96DiscarC: 8/ 9/96
CU-5 0isc. Grab Uater Sanpte
flercrites: Eacchus Pond
C5DSC SDG#: HSPDl -09
CATrJO. AlIALYSIS IIAME
TcL Votatites by 8240 - Uater
12i3 Chtoromeihane1?57 ErDnonethane
lrll \iiriyL Chioride
lqi,( C5!.oroethane
t\97 i!erh1,Ig;g Cl)l.oricie
iia3 lcetone
lii9 C:,ruLrn DisuLf ide
3:,,.,) 1,1-Dicirlorcethenc'j501'1,1-0ichtoro!"tn;ne
lt03 ch t ocoforrn
15o{ 1,2-Dichr-oroethane
Cii6 2-0irriirii-,ne
i'ii.s i, t,'l -trichloroerhane
itlS Ca!.bon Tetrachiorid.
l!07 Vinyt Acdt3te
1:,i8 Sronudicl',icromethane
3=,e') l,:-L)ichtorop.op:rnl.
35i6 cis-i,i-Dichlo.upropene't:,",', ll.ichtort,c::eng
lt',? Dr!:ronrochi.oronrerhane3i13 '1 .1, Z'TrichLoroetn3ne1l\5 Sclztnr.1i'10 rrans- 1,3-lichLorop.oilene
:.: 13 I r u;ilof orrn::,?1 1, -lr,rrhyt -2-pen!anone
i;::0 2-ile.xarrcne15?2 Totrachtcloethenej5:.3 1,1,2,2-'ferrachL(,r'oethane
li2\ Trlr-r.'ne
3'-?5 Cr t orobr.nzene
i--:15 Ethy'.LrEnzi.r.: -__,'l ( :\,..r^^
:--,:'.) ):,),1.r^e (tor.'l ),;30 tr'ar,s-1,2 iich',oroethcne1.i;:\ r is-1 ,2-,-: ic'r iorout.tdae
QL:Esriona? ConI.ia! \ol!T
Rr--hal .. Kr:,::;,:r
CL ien: Scrvi ces Represer'ltat ivL,
at (7:;) 656-2:i:li.)
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tlic:ele )'cCiarin, B-A.
CT,rro :e:Crrr, 5:,/MS Votatir.es
rcE
Lancaster Laboratories
2425 Neur Holland Prke
PO Box 12425
Lancaster. PA 17 605-2425
717-656-2300 Fax: [phone] $l'I 3'
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(iI)La ncaste r Laboratories Page:I of 11
A Thermo Analytical Laboratory
LLI sample No. EL 253SC0E
Cottected: 6/27/96 at 09:00 by SR
subritred: 6/28/96 Reported: 8/ 1/c)6Discard: 8/ 9/96
cU-5 Disc- 6rab lJater Sarple
t{ercutes: Bacchus Pond
c5DSC SOG#: HBP01 -09
CATIIO. A}IAtYSIS !IA!'IE
fcL SU846 Senivotati tes/Uarers
' Account llo: 067'16
l'lercul es, I ncsrrorated
Slrvi f oronenr: - ;\iia irs
ui Lnington 15 19894
AS ftECEIVED
tESI-,]LTS DETECI I 3\ !- !I.! I T UN I IS
}E
P.0.
i(eL.
391 I
3e,67
3874jsBS
J5J+
468U
I,D6 I
16eZ
391 5
39[,2
3q10
i9D4
39'r 1
i890
l806
1906
3911,1
3)05
3931
3923
392?
IU/J
3(/07
1891
38.5r1
:.; .1.
i,l " 4,, .
Il.:,.
.l
ti-:,
pheno t
bis (2-chIoroerh)"1 ) ether
2 - ch I oropheno L
1,3-dichtorobenzene
1.4-dichtorobcnzena
-1 ,2 dich I orobl-nzenL'
2-rnethytpheno i
2, 2'oxybis ( l.chtoropropane)
4 - nre thy I plteno I
t{-ni trosodr -n-propyIami ne
hL'xach i oroethane
ni riobenzene
i sophorone
2-rri trophenoL
2,4-dirnethyLphenoI
bis (2-chIoroethoxy) {nethane
2,4 -di cir IorophenoL
1, ?,4- tri ch l.orouenzene
naohtha L ene
4-chlorc'ani line
hex ach I o rol]ut ac i ene
1' - ch I oro-3 -rnethy L phenoI
2 -rrrethy I naphth a I ene
h ex ach |. o coc yc L opent ad i ene
2, 4, 5- tri chr.orophenoI
2,c, 5 - tr i chiorophenoI
2-ch !oronaphrha'.ene
2-nirroani I inedirrethyt lrlrtha',ate
ac endph t hy t enc'
1.
2.
Questions? Contact ycur
Ra.heI L- Krcarn(.r
3.
Cl iel: Ser.riie:i lleprasett?t1ve
at. ('/'.7 \ oj6-:lll_lLl
MEMBEFl7lr-ir
Lancaster Laboratoiles
2425 New Holland Pike
PO 8ox 12425
Laocaster PA 17 605-2425
717-656-2300 Fax: 717 656'2681
R?(;pectf uI l.Y Subrrritted
Chfistine ll. RatcIiii,
Group l-eaCer, CClfg
See reverse stde for explanatron ol symbols and abbrevraltons
b-5.
ol}
2li5 Pe'; ,.rrorrt {S
(iI)La ncaste r Laboratories Page:A Thermo Analytical Laboratory
r Account No: 06716
iii--rcui.es, lncorpcrated - 9E
i !nvi ronnrenrr,: Afrai rs
I ili'.irington !,E 19894
4 ol 1i
LLr SampLe No. EL 253:iC08cottected: 6/27/96 at 09:Llo by 5R
subnritted: 6/23/96 Reported: 3/ ",/96Discacd: 8/ 9/96
on
Rel-.
CU-5 0isc. Grab Uater Sarnpte
Hercutes: Eacchus Pond
c50sc sorif: HBP01 -c9
CAT}IO. ANALYSIS NAME
TCL SU846 Senivotati Ies/uaters
3908 3-ni troani t ine3857 acenaphthene3893 2.4-dinitrophenoL3912 4-ni trophenol3t;79 Cibenzofuran3594 2,4-dinitrorotuene3315 2,5-drnirrotoIuene3887 diethyt Dhrhalarei375 4-chLorophenyI phenyt erhar5898 f Iuorene3909 4-ni rroani I ine4C63 4,6-Cinitro-2-nerhyIphenoL391,L ll.ni tlosrrdiphenyinmine3669 4-brornophenyI phenyt erher3899 hexach I ocobenzene311,6 penr3chtoroohenoL39i7 phenrrnrhrene3859 anthracenelrtLl. carbazor.e3830 di -n-butyt phtha!ate3897 f Luorantirene39i9 pyrene3870 butyl benzyl phrhalate3335 3,3r -dichlorobenziciine3560 bcnzo (a) anthracsne3l,re bis (2-erhy!.hexy[ ) phthBlareit76 chrysene3l]95 di -n-octyI phthatatejgo1 ban:o (b) fluoranrhene3351 benzo (k) fl,uoranchene3ltLt, benzo (a) pyreneleJi i;deno (1,2,3-cd) pyrene338i dibenz (a,h) anthracene3t1b3 ben:o (ghi ) per'),tene
A5 AECS!VED
:::ii:i::::::::ii::iri:lr::r:r::i:::rii::::,:::.:;.:,i HE'IHOD
iii..1..iiii,i;.li;ftE,:f.!l9'i,ii,i:, DETECT 1 Di t !rl I r uN I rs
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ouest ions? Conr:act voLlf
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C'. ient Services Representative
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Lancdster Laborato(es
2425 Ne,r Holland Prke
PO Box 12425
Lancaster. PA 17 605 -2425
717-656-2100 Fax. [phone] See reverse srde for explanatron of symbol5 and abDrevrattons 22 l6 Rev l0/30/95
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(l)Lancaste r Laboratories
A The rmo Ana lyti ca I La bo rato ry
5 of 11
LLI Samp1e No. EL 25i3CC8
ColtectL.ci: C|iza/9o at 09:C0 iy ?R
Subnritted:06/?3/96
Account tlo:067!6
ttercut es, : ncorporated
lnvi ror,rnenra I Affa i nsti Lmington CE 19894
CU-5 0isc. Grab Uater Sompte
llercutes: Bacchus Pond
CSDSC S0GC: liBP0'l'C9
CATIIO AUALYSIS IIAHE
!i592 TCL Votati Les by 8240
!EIHOO
Uater sU-845 32(08
172? Thst I iLmr17t3 Aluminr:nr
'.741 Ant i niony'1746 llari urn
1 747 Bcryt t i um
',749 C adrri uli75i C!irorni Lrn17i3 fopper\75L I roni755 Lead
'l 75d Han.-ranc.sei76', l,i r cke I17irb Silvu'ri77Z Z inc
18/,3 HU SU8.1r, !CP Digcs( (tot rac)
7t')i5 .,\rsenic TR
7C36 Setenirrrr IR
0259 Mu'rcucy
5713 |,i-t"l SH8+6 i{g Di(,est
08'11 g{.t{ t-J;1ter Sv.tractiont67g TC! Sli346 Serr:ivoiat i Iesl1,Jalef s!,t7E TcL s'J816 senivotat ! l.s,'r-'a!ei's
su-346 5110A
5'J_346 6llr-r^
Si,'-8,,6 5.li CA
su-346 5t1,lA
SU-9/,o oJICAcrr-a4/ 4r.,1r
str-31,6 5_rlCi
r1r,_fI! ,'iir.
tu-rat "l'lil;\Jll-546 ol-r'-,;i
SU-345 5l-1iri,
cr,-i:/r /l !i,1,'
S*- J.ic 5l i'rn
.:!r-:l/^ .:1,_,\
Su- 41, llCtl
SIJ':i/.5 or r0A
9lJ-31a,5InA
su-9t,6 747c1
SU-345 7.'7.1^
su-9t,5 3510s
a'i-Q4r ,! )7ii.
su-3,"5:il7.,i
07/15/96 Cr,r?
07/15/96 C4CZ
07/15/96 CLo?
07/15/96 C4C2
c7/15/96 N4n?c7/',5/96 *q?
A7/1.5/95 C!*,)z
17,/^ 5 /96 t4l7
c7/15/96 C4t2tli/"5/9b c!-12
c7/'.5/91, C412
07,/i 5/9a ?r!-1:
c7/.5/9b C4':7
17i''5/')6,:$2t7/1i/c5 1.2??
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07/03/96 192r
t7/12/96 ?'.2?
n7ln2lCA ^Qin,)7/tl/96 C'--'l5
A7 /C'/-/96 ,)5'.5
ANALYS t 5
TRIAL DATE A}ID TIME AIIALYST
1 07/03/96 CgZl Susan A. !,lcHahon
Donna R. Sackett
Donna R. Sackert
oonna R. Sackett
Donna R. Sacket(
Donna R. Sackert
Donna R. Sackett
Donna R. Sackett
Donna R. Sacieta
conna R- Sackert
Dorna R. Sackett
qonna R. Sackett
Donna R. sacke!t
Donna R. Saciert
9onne R. S.rcketr
Chcistine Il. contin
Donna R. Sacketl
Donna R. Sacketr
Nel i. i S- llarkaryan
tiet i. i S, Markaryan
''iaria A. 9avenpol.t
Mark A. R:tc'-i{f
l4ai( A. Ratci.iff
7Fn
Lancaster Laboratofles
2425 New Holland Prke
PO Box 12425
Lancaste( PA 17605-242 -\
117-656-2300 tax:717 656 2631
I.ABORATORY CI]RONICLE
5ee reverse srde fo'expidndtrcn oi symDols aad abbrevrdtro45 2216 Rev ,orror$ dt
(I)La ncaste r Laboratories Page:
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A Thermo Analytical Laboratory
Sarpl, e
HDL
Samp L e
UNITS
'1258 chtocomethanel. us,/ t
1257 Brooomethane3. uq/t
3192 Vinyt Chtoride2. us/t
3191, Ch I oroethane3. u9/ [
3497 Methytene Chloride2. ug/t
3498 Acetone6. trg/t3499 Carbon 0isuLfi.re3' ug"L3500 1,1-DichIoroethene
'! . ue./ t
3501 1,'!-0ichtor oethane2. u9/ |5i01 Chtoroforrr
'1 ' uglt3iA4 1,2-0ichtoroethane?' us/l
0315 2-Butanone'3. trg/ t
3505 1,1,1-Trichtoroethanei. ug/L3506 Carbon Tetrachi.oride
1 ' us/t3507 Vinyt Acetate2. u9/ tf50B Bromodichlonon)ethane1. ug/[3509 1,2-DirhIoropropane1. us,/t
35'16 cis'1,3-Dichtoropropene1. trg/t
3511 Trichtoroethene1. uE./[
35'12 Di brcurochtorornethane2. trgr'tll li 1, 1,2- Trich toroethane2. ug/t
3115 BLlnzerre1. us/t1510 trans-1,3-Dichtoropropene
1 ' u'/t
LLI sample No. 2538008
CrJ-5 Disc. Crab Uater Samp!.e
Hercutes: Bacchus Pond
I
iI Grouo No. 522727
i liercutes, lnco!-porated - DE
6B
81
32
61
98
9.:
72
00
09
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97
10
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DUP I'ISRPI lIS MSD F.PO
LC9 !.CS
LCS OV'? RPo
LCS LII'IITS
LOU H I6i{
1592 IcL Votarites by 8240 - Uater Batch: I9618414A
N.D.
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N.9.
N.D.
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ll-D.
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N.! .
N.:r .
N.D.
N.D.
N.D.
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N.D.
73
90
67
1C2
67
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1.01
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96
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116
1',1 1
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106
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MEMBEFI,e-m
Lancaster Laborato0es
2425 New Holland Prke
PO Box 12425
Lancaster. PA 11 605 - 2425
7 17 -656-2300 f ax 1 17 -656-268 1
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QUALITY CONTROL RE!'ORT
5ee reverse s'de tot explaq61lgq si trmbols dnd abb'evrdlrons 2216 Rev 10/30/95
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Sarpte Sarpte DUPI.IDI UII I TS BLANK RPO iIS HSD
3518 Bromofocnt'l . uslt [.9. 71 90
35?1 4-Methyt -2-pentanone5. u9/ t N.D. 65 93
3520 2 - l'lexanone7- ug/t ll.D. 62 95
357? Tetrachtoroethene1. ug/i. N.0. 106 1053525 1, 1,2,2-Terrachtoroethane2. us/t N.3. 72 9435?!, TotLrene?. ug/t N.D. 105 105i525 Ch I orobe,]zene1. ug/[ N.9. 101 101
35?6 EthyIbenzene?. ug/t N.9. 1i0 109
35?e styrene1. us./L N.!. 1AZ 1C23529 Xytene (total )1. ug/L N.r. lCS 1035730 trans-1,2-0 ich'.oroethene?. us/t N-D. 'lC4 99
6258 ci s-1,2-9ichtocoethena2. ug/t N.0. 1C6 '102
1722 Thattium Batch:96.1t2'18l.8302170. u9/ t N. C. ( 1 ) 1C'l 1C3
174i Atuminum 6a!ch:96i92'13/+8102
57 . uE/ l. N.D. 17t -772 -7?9 (2)
1744 Antimony Batch: 95192:34BilD2':5. uE/t N.9. ('l ) 105 136
1745 Baciunr Batch:96192181,8102?.? uE/t ri.o. 0 ('l) el 38
1747 Seryl L iun Batch: 95192'18131021.1 ug/t 0.0016 J m!,/l (") 97 97'!7/r!r Cadrniun Bat.ch:96192'i32.!1022.7 us/t \.9. (1) 94 95
1751 Chlonrium 6.ircx: 95i92'181,81024.3 us,/t N.D. 0 (1) 78 79
1753 Copper 0arch:96192184!.-rC23.8 us/[ !{.0- 0 (1) -2i,1 -191
1754 Iron Barch:96192131,81025.9 u9/1. 0.t)6C7 J t(.:/ 17t -151\ -1!.t,1 (?)
1755 Lead 6atch:96192'1313.'lD2i8,. us/t ri.9. 0 (1) 92 9l
1758 tlanganese Ba!c5: 96'192181.111022.9 us/L ti.!. 0 (1) 59 L1
176'1 t{icket Eatch:9o19218:,-qll25.\ tJg/t l.D. 0 (1) 94 95'!766 S i tvec Sarcfr: 9,rl92lg43ll23.6 ug/t r(.9. (',] ) 99 10]
(1) The resuLt for one or both dctefnrinations ras less than fivc !inles thc'-00.(2) Thr'background resutt p:rs more than four tilnes the spi(c ad.,ied.
I Grouo No. 522727
i i'iercJIes, lncorporaled
i
QUAL]TY CONTROL .R.EPORT
Page: 7 ol 'l 'l
LIi!ITS
H I G'rl
80 -120
80 120
80 120
30 120
80 1?D
B0 120
80 120
80 120
80 120
80 12t)
80 120
80 'rzc
80 1?C
MS
RPD
LCS tCS LCS
LCS DUP RPD LOU
21
16
43
2
26
0
0
2
'1
c
5
4
1
?1
1
1
c
1
2
9
1
J
1
1
1C2
108
107
100
93
97
107
101
'I 11
102
101
1C4
10c
MEMBEFI7mm
Lanaaster Laboratores
2425 New Holland Prke
PO Sox 12425
Lancaste( PA 17 605-24)3
717-656-2300 Fax [phone]
(I)Lancaster Laboratories
A Thermo Analytical Laboratory
LLI sample No. 25381')08
Cu-5 Disc. Grab l,arer Sampr.e
HercuIes: Bacchus Pond
See re'/e'se s,de for e.crdnal on of symoois and abbrerratroos 2216 Rev ,orror,, dos
1l
il
1l
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5 112
1Z 158
25 tJ4
1 172
?0 124
3? 129
46 123
36 166
5 15?
1 230
A0 i 13
15 180
2" n96
29 162
3? 119
33 184
39 135
t-/. 11?
21 113
ZIL Lancaster Laboratories\lZ A Thermo Anaiytical Laboraiory
Page: 8 of
LLr sample No. 25330C)8
Ctl-5 Drsc. Grab'Jarer safltpte
Hercules: Eacchus Pond
I Group No.
Htsrc'-ites,
5Z?7?i
! ncoeporated
Sarrrpte SarnpIeIrtoL u[! rs
1772 Zinc12. ug/t
7015 Arsenic TR2.7 ug/t
7036 Seteniurn TR
Z .7 u9,/ t
0259 tlercu.y
0 . 0/ti u9/ [
4673 lCL SUB/'6 SenrivoLati 1Es/'laters
3918 phenot1. ug/t3867 bis (2-ch'.o|oethyll ether'1. uS,/t
3e74 2 -ch Iorophenol'l . us/t3elll 1,5-dichtorob"'nzene
'l ' ug/t
33.Ji'1,4-dichLorobenzenE1. ug,/t
1'482 1,2-Cichtorobenzene'l' ug/t4580 ?-rrethytphenoI2. ug./ t(a:11 2,2'oxybis (l-chLoropropane)
2 . uo-,/ t-
4a:2 /+-r:ath;,l.pherrot2. ug/t
3q l5 ll-ni trosodi -n-propytarnine
2. u9/ tli,ll he;,.ach t oroethane2- u9/ t
3t,10 ni rr.rbenzene
'1 ' uglt
3i.:i't!. i soJ-.i:ocone1' ug'/[ii'i I ?-niti'uphcnol2. rs/L
1,:)0 2,4-d!mcthyiphenol1' uEi'i
-:IJ85 bis (2-cirLorosthoxy) rnethE.rti
1 ' ug/'t
13.15 2,l,-dichtorophr.noil. ue/ t::1,:1 l,2,r, riicliLorcbenz:rte
1 . ug/ t
3r,i'-tf, naphthatene
'1 . rrg/ I
6LANK
Batch:961921848302
N.D.
Batcn:951921848C02
IJ.D.
Barch:95'i92':848C02
N.r.
Earch: 96184 5713X01
ti.).
Batch: 96'134uAA026
N.!.
ti.5-
N.!.
ll 9-
N.!.
N.D.
N.?.
!i.9.
N.D.
N.D.
N.l.
ti.!.
!'r.9.
N.!.
q9 47
91 91
3.8 89
73 82
30 83
79 82
31 8?
67 58
8i 8i
1 !0 114
72 73
97 97
1CC 10C
9t, 95
66 72
90 90
o<
79 S1
s8 3B
than f ive r intes the l-00.
DUP lISRF9 !,!S FS9 RPO
!-cs Lcs
LCS OUP RPD
LCS LIlIIITSLOU HIGH
80 12C
80 120
30 120
30 120
0 (1)
0 (1)
0 (1)
0 (i)
- l+1
".c',
1C1
79
-34
1D2
1e2
79
'!03
103
103
93
5
,l
!
n
2
c
I
C
0
7
C
0
J
1\
8B
u5
68
71
77
64
103
)J
911
92
65
86
8/,
70
{1) Tire resi.:tt for one or both rjeterrninations xas Iess I
diI
!
mtr Lancaster Laborator,es
2425 New Holland Prke
PO Box 12425
Lancastet PA 17605-2425
7r7'656-2300 Fax T 11 -656-2681
Q',IA],ITY CONTROL REPOF.T
see reverse srde for explanatron of symools and abbrevrairons 2216 Rev tot30/95
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(il)Lancaster Laboratories
QUAI]TY CONTROL REPORT
1l9ofA Thermo Analytica I La bo ratory
LLI Sarnpl-e No. 25380t\ti
CU-5 Disc. Grab Uater Sampte
Hercules: Bacchus Pond
6roup No. 522727
tercul.es, In.c,'pora!ed - DE
Sarple SampteIIOL UII I TS
3871 4-chtoroani IineZ. ul/l
3900 hexachtorobutadiene
1 ' ug/t
3872 4 -ch Loro-l -methytphenot
?. tJg/ t
3905 2-methytnaphthatene1. ug/t
3901 hexachtorocyclopentadiene3. ugl t
3921 2,4,6' trichtorophenol1. ug/t
3922 2,4,5-trichlorophenot1. ugll
3ST3 2-chIoronaphthaterre
1 - ug/t
3907 ?'ni tro.rni I ine
1 ' us/t
3891 dinrethyI phthatate
3. ugll
3858 acenaphth';Lene1' uqlt'
OUP MS
RP9 !4S IISD RPD
LCS LCS
I.CS DUP RPD
LCS LII'ltTS
LOU HIGHBLAIIK
N.C.
N.D .
Ir.9.
N.9.
N.D.
N.r.
N-9-
N.!.
N.9.
N.!.
17 115
24 116
?? 147
23 123
1 100
39 151
60 118
s3 143
1 112
33 145
73
15
9l
BO
41
91
90
oo
95
?5
B6
0
'I
2
72 74
65 69
93 93
35 87
51 53
_s? s7
99 88
0' 9e
97 97
i2 3l
92 93
7 143
47 1/t5
1 191
1 132
28 131
39 139
50 158
1 11/'
25 158
59 121
38 12?
1 181
'1 B0
087
10 92
55s
r o<
19t
195
'1 101
498
086
< n,
grl B0
93 93
41 37
47 l+5
g9 88
Y) Yt)
99 100
'6+65
1^? tn,
102 9B
s6 36
67 61)
1679 lcL SU8(5 Sernivoiatites/uaters Batch: 96184HAA!26
3908 3-nitroanitine
1 ' us/[
-2857 acenaphthr.ne
1 ' uglt
3891 2,4-dini trophenoL5. ug/ t
3912 4-ni trophenot5. u9/ t
J579 dibenzofura,n1. uglt
1394 2,4'dinitrotoIuene?' us/t
3895 2,6' dinitIototuene0. us/t1387 diethyI phrhal-ate?' us/tlE75 4-chl.orophenyt phenyt ether2. ug/[l89B f t uorene0. us/ t
3909 4-nitroaniIine?' ug/t
1L83 4,6-di ni tro-2-methyLphenol5' uslt
7Fn
Lancaster Laboratories
2425 New Holland Prk?
PO Box 12425
Lancastec PA 17 605-2425
71 7-656-2300 Fax.'7 17 -556-7581 2216 Rev.,Orr.rr d?See re,rerse srrie for explanatron oi symbol5 and abbrevralrons
II
L
LLI sanrpLe No. 2538008
CU-5 Disc. Grab uarer Sanpte
Hercutes: Bacchus Pond
' croup l,lo. 522727
, i.lc-rcutes, lncorporated
I
Page: 10 of 1'l
38 147
53 127
1 152
14 176
54 1?0
?7 i33
10 137
1 118
t6 t) I
52 115
1 152
1 262
33 143
8 158
17 168
t+ 146
21, 159
11 163
17 163
1 171
i ?27
1 719
(I)La ncaste r Laboratories
A Thermo Analytica I Laboratory
DE
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Sampte sanDteHDL UN i IS
3911 I-ni trosodiphenytanineZ. ug/l
3369 4-bromophenyl. phenyt erherZ. ug/l
1899 hexachtocobenrene
'1 . trs/ t
3916 pentachIorophenoI
'l ' ug/t
39i7 phenanthrene1. ug./l
3359 anthracene
:' u!/L
t-68,1 carbazote
'1 . ug/t
3880 di -n-butyl phthatate1. ug/t
3897 f Iuoranthene
'I . ug/t
39'19 pyrene1' usll
3870 butyI benzyl. phthaLotez' us/t
3S85 3,3''di ch lorobenzidine2' uglt
3860 benzo (a) anthracene'l ' us/t3868 bis (2'ethythe.xyt ) ph!halate?' ug/t
3876 chrysene1. ug,/t
3{,96 di -n-octyI phthatateZ. us/t
3851 benzo (b) ftuoranthene7' u9/|
1362 benzo (k) ftuoranthene?.. us/ L!2e!. benzo (a) pyrenez' ug/ t
3901 indenc ('1,2,3-cd) pycene2. ugl t
388'l dibe,rz (a,h) anthracene?' uc/t
33L3 ben:o (shi) perytene
2. usr't
US!'1S IISD RPD LCS
DUP
RPO
LCS I-CS LCS LIiIITS
9UP RPD LOU II I GHgLANK
11.9.
N.0.
r'i.0.
N.9.
N.0.
N.!.
N-9-
N.0.
t,n
N.D.
N.0 .
N.D.
N.D.
N.D.
N.D.
N.!-
N.t-
il.D.
N.9.
N.?.
88 86
o a na
96 94
4s 4a
95 94
c2 9C
e9 87
9C E9
93 91
s3 80
79 7A
85 85
'102 101
91 91
'r c0 107
90 88
95 95
33 8l
76 75
74 74
2
2
2
11
C
,j
?.
2
'1
2
J
2
0
1
6
?
C
c
84
B5
95
90
9Z
35
39
B]
92
84
102
9C
'I C4
B9
94
Q1
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9tr
77
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MEMBER
TXTTI
Lancaster Laboratories
2425 New Holland Pike
PO Box 12425
Ldncaster PA 11 605- 2425
7l 7-656-2300 Fax. [phone]
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Q'r'ALITY CONTROL REPORT
See reverse srde ior explanatron of symbols and abbrevratrons 2216 Rev I0/30/95
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A Thermo Analytical Labo ratory
QUAIITY CONTROL REFORA
Page: 'l 1 of 11
SURRC6ATE LI!i,IITSLO'; H I6H
76 114qi t l n
86 115
21 10010 9110 123
35 11t+t-3 't 16
LLI Samr:le l'to. 2538CL18
Cil-5 0 isc. G-r'rb UateI Saillple
Hercutss: Bacchus Pond
4r9? ICL Votatiles by 8240 - Uarer
4678 ICL SU8lr6 Semivotari les,/Uaters
t+679 ICL SU846 Se$ivoIari Les/Uarers
i Group No. 522727
i HercuLes, lncorporated - DE
r
SI-'RROCAIE SUM!!ARY
TR!AL ID SURRO6AIE
c4- 1 ,2 -9CA
c! ' tol. uene
5rb
Z-F!.phenoL
FhcnoL-d6
2,1.,6'TEP
N i trobz-d5
2 I'D i phny I
I pir.n / !.d1 4
RECOVERY %
104
1C3
91
56
37
36
69
71'
MEMBER
'Kil
Lanca5ter Laboratofles
2425 New Holland Prke
PO Box 12425
Lancastec PA 17605-2425
717-656-2300 Fax: [phone] I See re'rerse srde ior expianatron of symbols and abbrevidtrons 2216 Re!,orrorn, d*s
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A Thermo Analytica I La bo ratory
Page:
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Respr.c: {ur. l.y Subxi tted
R;-::o:a V-'.nyrlra, rifoup Leader
! aP :1e!a Is,/."'acha f es
lof 14
LLr sampl-e No. EL 253E000Cottected: 6/26/96 at 1?:C5 by BR
suunitted: 6l?8196 Reported: 8/ 1/960iscacd: 8/ 9/96
CU-1 JUo t'latrix Spike Grab Llarer Sanple
iAccount llo: C6716
; !ercuIes, Inconporated ' OE
i Envi cor-rpnte!. Af fai rs
i ui lmington !E 19u9r'
I
AS NECE IVED
Hercutes: Bacchus Pond
CUJUO SDG#: H8PD1 -03MS
CATIIO. AIIALYSIS IIAHE
4592 TCL Votatites by 8240 - Uater1722 Thattiur
171+3 Aluninun1711 Anrimony1T+6 8ar ium1747 Bery[ [ iunr1749 Cadnrium1751 Chcomi Lxn1753 Copper175L I ron1755 Lead1758 I'langanese1761 Hici(eI1766 Si tver17TZ Zinc7035 Arsenic TR7036 SeLenium fR0259 tlercury0937 TCL Pest ic ides in l.,latsrs4678 TCL 51846 SemivoIati les/Uaters4679 ICL 5',J346 senivotati Les/uaters
ME T HOO
OETEC]]3ii I.IMIT U!ITS
See Page
17C . -r9/ t
t7 . u..t/'.i5. ug/i
: I t,^t'
^. .3 ,rr/ i.
? .7 u9/ i.
1-3 ,L=q/t
i.a u.j/ls.!. !g!t'13. re/ |2.9 t:+)/'-
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2.7 !S/'l
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SL-c Fa!L'
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::::,.i:::,i:,,, \E-}Uf I :
::::::,i c,UlU-,
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I coPY T0 Hercutes, lncorporated
1 CoPY T0 ERM - eockv Mountarn
ATTN: Mr. Joseph Kel ler
ATI\: I'lr. lirenr Rdcinson
ouestions? Cont:ict your Ctient Se, vjccs Rep't'esu.n:ittive
RachcI L- Krean]er ar (7'1 /) 650-z]ilri
MEMBEFI
7ztrm
0l:28:06 D 0C02 15 REP 1?C436 5i2727I1C r5_00 0c',t267D0 ASRooC
Lancaster Laboratories
2425 New Holland Prke
PO Box 12425
Lan(aste( PA 17 605-24)5
717-656-2100 Fax: [phone] See reverse srde for erplan;iron ol 5';mools and abbrevratrons 2216 Rev.,Orr'r* d'9
I
I
(I)La ncaster Laborato ries I
ILLI Sample No. ELCotlected: 6/26/96 at 12:05
Subflritted: 6/?8/96 Reporred:Discard: 9/ 9/96
A Thermo Ana lytica I Laboratory
2538C00
by BR
8/ 1/96
I
i Account lto: 057n6Ir Hercutes, !ncorporared - DE
I Env'i roruenreL Affai rs
i uitnington DE 19894
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Ret.
Respeclful. iy Subrnj ttedFicner.r YcClarin, B.A.
Sroup -eader, CCl!4S; Volari Ies
Page: 2 of 14
CU-'l JUo fiarrix Spike G.ab Uater SampLe
Hercutes: Bacchus Pond
CUJUD SoG#: HBP0'l -0lltS
CAI}IO. ANALYSIS NAHE
TCL Votatites by 8240 - Uater
1258 Chtoronrethane1?57 Bronpmethane3492 vinyt ChLoride3494 Chtoroethane3497 Methytene Chloride3498 Acetone3499 Carbon DisuIfide3500 1 ,1 -D i ch Ioroethene3501 1 ,1 -0i ch !oroethane3503 Ch Ioro{orm350t+ 1,2-Dichic.oethane0316 2-Butanone3505 1 ,1 ,'1 -Trichioroethane
3506 Cacbon Tetrachr,oride3507 VinyI Acetare3508 Eronrodichtoromethane
3509'1,2-0ichtoroprooane3516 cis-1,1-Dichi.oropropene3511 TnichIoroethene35i2 Dibromochto.omethane3513 1,1,2-Trich'Loroethane3515 Benzene1510 trans-.l,3-Dichtoropropene3518 Brornoform3521 4-l,lethyt-2-pentanone3520 2-He,ranone35?Z Tetrachtoroethene3523 1,1,2,2-Te!rachLoroethane35?t Totuene3525 Ch Iorobenzene3526 Ethytbenzene1528 Styrene3529 XyIene (tota[ )5780 trans-1,2-DichIoroethene6268 cis-1,2-Dichtoroerhene
AS RECEIVED
, HETINN
ii:i,,,:,;i:ililliF,l!!ISli:. ii;'i . DETE c I : 1ri L I I{ I T u}r I Is
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AaaheL r,. Kreaner
Servi ces Represenlaiivear (717) 6t6-21i3
TIKIIT
Lancaster Laboratories
2425 New Holland Pike
PO Box 12425
Lancaster. PA 17605-2425
717-656-2300 Fax: [phone] ,orror$ d?5ee reverse slde for explanatron of symbois and abb.evtations 22 l6 Rev
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(I)La ncaster Laboratories
A Thermo Analytical Laboratory
LLI Sample No. EL 2538CC0cotlected: 6/26/96 at 12:05 by BR
Su&nitted: 6/28/96 Reported: S/ 1/960iscard: 8/ 9/96
CU-1 JUo Matrix Spike Grab lJater Sernpte
:i Account [o: 06716
i t'tercuLes, Incorporated - gE
: Envi ronoental ,\fia i rs
I Ui lmington !E ',:9894
AS RECEIVED
P.0.
Ret.
PesDect{ul Iy Subm! tted
,.ieniJer E. Hess, ts-S.
C.oup Le:der P.sr !ciCes/PCBs
Page: f of 14
Hercutes: Bacchus Pond
CUJI,D SDG#: HBP01-03t'!S
CATIIO. A}IAIYSIS IIAME
ICL Pestic ides in Uaters
I{E I HOD
OETECT:3Ii LIId!T UNITS
1600 Atpha BHc ,i,:'i:.i::':j".. :: "' 0,21 C.CCZ ug/l1601 Beta BHC Iti:1,::tt:::i:l::tl:.::t: O-:i l.,lig uq/t1603 getra BHc ,....' ,'. 0..',. C.at5 !g/ j.
lbOZ Garrma BilC - t-indane ':,,t.j, . . C..-r i.il't u.l/:']60/, lleptachlor :'.',' . *-,V i-f;5 ,a,tl16os Ardrrn l,.. ' !..9 ;.;i; ;i/i1606 Heptachtor Epoxide :::,i,i,,:::: :, i, ::0-Z-) C.,ji3 \!/.,'1616 Endosutfan t ,:... !-:.J r-::'l ,r/t1610 eierdrin i a.-i ;.;;; ;;i,i6o7 DoE :r,'. ,9,a- L1.c!5 u9/:
161 1 Endrin ,i....::.,, :, . .0,:c C.,l0i u,)/t-1615 Endosutfan lt ,,.,...... . :,.-l !.!.1 ,t!/.1603 DOD ,.,,,,.,,.,:...,:,
',, l..i u.'lCZ ,ti/,,1617 EMosutfan Sul.frte ,,.r... .. 'l. j 0.f!7 Ji/,.1609 DDT ,'. ).:, 'j.t!:j ug/,i0938 Endrin Ketone :t:::t.t,,::,t,:. , U-.- . 0.3!,i ug/i'1800 ttethoxychl.or ::..':.'.,.' (:-iii l.i3 !9/ -1361 Alpha Chi.ordane ',i:i.ii.i ,li,, J.?l 1..1105 .tg/t1J6Z Gamna Chtordane 'i.tiiii:t,:i. ,, ,.:',0- : . t.C,,r5 ,Lg/:,1613 Toxaphene .',,., r,. N.,:,. I . ui/ r1618 Ende in Atdehyd" ..,.', .., 0-l C.01C ,rg/,-1619 PCB-'101d, ,:'itl:.,:,,,iiii'il: . N,q, O.CC uS/t1620 PCB'1221 :.i,:,:.i1i :ttil,.:., il,g. 0.? uS/t1621 PCB'1232 :.,:,.:,'i:' U.O. 0.J9 u'/l1622 PC8-1212 .,..,';.:.:. g.i. 0.C5 Lrg/l1623 PCB-12/,8 iirl.:i;i;rr,;i.. .i ,r.!,. 0.t7 us/t16?t- PCB-1254 ',,..'..:::,::,. r.r. i. 0. C6 t9/ t1026 PcB-1260 :.i'::.: : .],.0., C.:T ug/,.
Due to insufficient sampLe sjze, ce cere unable !o feport our usuaIquantitation Linrits. The vaLues reported.eprr.sont rne !oHest ouantita!ion
L irrrits ootainabl.e.
Quesflons? Contact your Ctienr SerVices ?epresen:drjve
Rachel ,-. Kreimer at (7:7) 656-2j.l,J
Laocaster Labordtoie5
2425 New Holland Prke
PO Box 12425
Lancastet PA 1 7605-2425
717-656-2300 tax: 717-656-268 l
MEMBER7XilI a]D.?.#See reverse srde ior explanairon of symbois and abbre,rratrons 2216 Rev l0/10,'95
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j Sercutes, IncJ.oorated - 0E
i Envi ronflc.nta . ..1{ia i rs
i Ui tmington lE l9ll9/+
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I
Page: 4 of 11
2216 Rev 10/lo/rs d?
ll
P.0-
Rel.
1I
}IAS RECEIVED
XE T H39
.,.i:,;i*tfi:{rpl:t-s.;.:i; 0ETEcT : 3s L !r't I T uN I Ts
!s/ t
u9/ t
ut)l'-
u9/ I
u!/'-
uc/ l
ug/r.
u9/ L
rg/ t'
tJg / 'r
!g/ t-
ug,/ I
tg/ |
u9/'-
ugl I
uJ/ I
ucJ / t-
Ut-,/'.
ugl i
u9/ l.
u9/'r
!9/ |
\J5/ t-
ugl i'
u9/ i
u9/ |
'r9/ t.
il
z.
2.)
2.
z.
Tour Ct ient Serriccs Represen:ativeat ( 7'7) 656- 2110
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MEMBEREKtit
Lancaster Laboratores
2425 New Holland Pike
PO Box 12425
Ldn(aster PA 11 605-2425
717-655'2100 Fax [phone]
Resoec: fuL ly Sutrmi tted
Crrrisilne il. Aaacl- ii+, 5.S.
Sroup !eacier, 5Cl!{S
See reve.se Stde for explanatron of s/mcols and abbrevratrons
(|)h*t**..,r,H?,qr.*gr'.t
LLI sample No. EL 253SC00coltected: 6/?6/96 at 12:05 by 3R
Suhnitted: 6/28/96 Repocted: 8/ 1/96Discard: 8/ 9/96
CU-'l JUD |latrix Spike Grab iJater Sampte
Hercutes: Bacchus Pond
CsJUo SDG#: HBP01-C31.!S
CAT}IO. ANALYSIS UAHE
TcL SU846 Semivotati Ies/Uaters
3918 phenol3867 bis (2-chIoroethyt) ether3A71 2-chtorophenoL3BB3 1,3'dichtorobenzene3884 1,4-dichtorobenzene3882 1,2'dichtoroben:ene46B0 2-orethylphenol4o81 2,2'oxybis (i'chtoropropane)4682 4-methytphenol39'15 N-ni trosodi -n-propylamine
3902 hexachtocoetirane39!0 ni trobenzene390/. i sophorone
39'l 1 2-nitrophenoI3890 2,4 -dimethy iphenot3866 bis (2'chtoroethoxy) methane1386 2,4-dichlorophenoi.3921 i,3,4-trichtorobenzene3906 naphtha Iene3871 4-chIoroanil,ine3900 hexach Iorobutadi ene387? 4-chtoro-3-nErhyl,ghenot3905 2-methytnaphlhatene3901 hexach I orocyc I opentad i ene3921 2,1r,5-trichlorophenol3922 2,4,5'trichtoropilenot3875 2-chtoronaohthalene3907 2-nitroan'i Iine3891 dinrethytphrhatate3853 acenaph thyI ene
ouest ions? Contact
Rachel r-. Kreanler
DE
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(I)Lancaster Laboratories
A Thermo Analyti ca I La boratory 5of 14
LLI Sample No. EL 2533C,,t\0Cottected: 6/?6/9o at 12:05 by BR
suhnitted: 6/28/96 Repor-ted: Bl 1/96oiscard: 8/ 9/96
JUD itatrix Spike Grab [,ater SafilPLe
i A..ount lto: c5716i ftercutes, lncofporated
i Envi rorulentaL Affai r:
i ,;r [mington DS :9094
i
AS RECEII/ED
MET HCO
RESULIS, " OETECTICN LI!1IT UIIITS
P.0.
ReL.
llercutes: Bacchus Pond
CUJUo SDG#: ll8P0l -03HS
CATNO. AIIALYSIS NAHE
fCL SU846 Semivotati tes/Uaters
3908
3857
3893
3912
3879
3894
3395
3887
3e7S
3898
3909
4583
391 4
3869
3899
39r6
3917
3859
1(fii.
3880
3897
3919
3870
3885
1860
3868
3376
3896
3361
3862
3864
3903
3881
3863
3 -ni troani t i ne
ac enaph thene2,4-dini trophenot
4-nitrophenol
di benzofuran
2,4-dini trotoluene
2,6-dinitrotoIuenediethyt phrhirlate
4-chtorophenyl prenyI ether
f Iuorene4-nitroanitine
4, 6 - d i n i tro- Z-methytpheno I
N -ni trosodi phenyt anr i ne
4-brornophenyl phenyt ether
h exach t orobenzene
pentach I orophenoI
phenanth rene
ant h rac ene
carbazot e
di -n-butyL phthatate
f luoranthene
Pyrenebutyt benzyt phthatate
1,3' -di ch Lonobenzidine
benzo (a) anthracenebis (2-ethyl.hexytl phthatate
82..
18u,
Servi ccs Rcpresentnt!veat (i^7) 656-2iCU
2.
2.
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4.
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1,.
2-t..
+.
for the CClYS
u9/ t
u9/ t
,tg/ i
us/ i
!9/ |
u9/ t
'Jg/'-ug/ t
u9/ t
trg/ :
uqt/ L
N<:/'l
u,i/ t.
ug/ t
ug/ ''
u9/ I
ut) / '-ug/ !
u9/ i
ugr/ i.
u9/ :
usl I
'.,:<) / 1.
u1/ t.
u9,/ |
'J9/'.
u,!/ i-
u1:/ L
u.)/'.
u\/'-
u9/ 1.
uc)/',
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chrysene i,'i ,,i':
di -n-octy[ phthalate ', .,.,
benzo (b) f'.uoranthene ,', '.
benzo (k) f',uoranthene ..
benzo (a) pyrene :.: . :
inde,no ( 1 ,2,3 -cd) pyrene :, ,:
dibenz (a,h) anthraccne :.'
benzo (ghi ) perytene : .,1..
oue to insufficient sampie, the quantitaticn liilits
senrivotati Ie coflrpounds xc.re raiscc.
Questrons? Contact youc Ctient
Rachet L- xrEaner
Ldncaster Laboratofles
2425 New Holland Prke
PO Box 12425
Lancaster, PA I 7605-2425
1 17 -656-2300 Fax: [phone] I
Respectf ul ly S,Jbrli tted
Chrisrin.- l\1, Rntcl::f ,Croup _cader, CCl,/S
5ee reverse slde for explanatron of sym,cois aod abbrevtairons7Xm
8.S.
22 l6 Rev. l0/30/95 i'g
&&&
Page: 6 of 14
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I Hercules, Inccrporated
I invironnrentar- lf f a irs
j ui Lnrineton DE 198q/.
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ANALYS I S
TRlAL DAIE AN9 TIIE ANALYST
1, 07iC3/96 llZZ Susan A. McMahon
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Il
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1722 Thattium174f Atuminun
1744 Antimony
1716 Bariun
1747 Seryt t iun17\9 cadmiun
1751 Chromium
1753 copper
175r, I ron
1755 Lead
1758 I'langanese176i Nicket'l766 SiLver
177? Zrnc
1848 ulJ sU846 lcP oigest (tot rec)
7035 Arseni c TR
7036 Setenium TR
0259 lilercury
5713 utJ SHBI,6 Hq 0igest
srJ-845 6C l0A
su-846 6110A
su-946 6a'.i0A
su-846 6,1'l0A
SU.846 6J1CA
su-846 6'llCA
su-846 6i',10/,
sr'-846 6ilirA
Sr''846 6,1'l0A
s*-846 6llCt\
srr-846 6J !0A
su-846 6J10A
StJ-846 6l'lr-rA
su-846 6iiiCA
slJ-846 3105A
su-846 6C'l,lA
s!/-846 6C i0A
su-846 747CA
sL,-8/,6 7i7DA
D7/i5/96 D3n9
071't5/96 A3l9
07/15/96 C3CC
c7/15/96 C3)9
07/.,5/96 C3,Jq
c7/',5/96 A3t)9
07/15/95 l3i.l'g7ii5/';b C!i9
07 / 1.5 /96 0iA9
07l15/96 0iC9
D7 / 15 /96 ,:i09
t7/^.5/95 t3);
D7/':5/9b A3)g
{Jl / 15 /9t, litl
07.!.c/96 i?Z?
n 7 /. < ,n; ntnnut I )t ,v uJv,
c7/15/96 A3tq
07/17/96 1617
O7/'t5/96 ?i4E
07/01/96 133A
07 /a5/96 A807
07/02/96 C930
07/a3/96 C7t9
07 /t3/96 07A9
Donna R. Sackett
Don,ra R. Sackett
Donna R. S.lckert
Donna g. Sackett
9onna il. sackett
Conna R. gackett
Donna R. Sackert
Donna R. Sackelt
Donna R. Sackett
Donna R. Sackett
0onna,t.. Sackett
9onna R. Sackett
Donna R. Sackett
Donna R. Sackert
christine l.t. Conlin
Conna R. Sacke(t
Donoa R. SacLett
Netli S. Harkaryan
NeLIi S. Markaryan
uarrie A. Natate
DougIas D. Seitz
Ha.ia A. Davenport
Stephanie M. Shenk
SreDhanie H. Shenk
ilI
081 3
4678
1679
08!7 uater Sample Pest. Extraction SU-846 35108
0937 TcL Pesticides in Uaters sU-8/.5 8C3l
BNA Uater Extraction sU-846 35108
ICL SU846 Sernivotati Ies/Uaters SU'846 327C8
TCL su846 SernivoIati tes/uare'rs sU-845 32708
Lancaster Ldboratofles
2425 New Holland Pike
PO Box 12425
Ldncastet PA l7 605-2425
717-656-2300 Fax: 7 17'656-2631
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TXmE 2216 Rev. ,Orrorn, dJ
LABORATORY CHRONICLE
(|)hgn:**ff,^hgP,o,'"*9i,"
LLI samp1e No. EL 2538000
Cottected: n6/26/96 at l2:05 by ER
submitted: 06/28/96
CU-1 JUo Matrix Spike 6rab Uater Sanrple
Hercutes: Eacchus Pond
CUJUo SDG#: tlBPO1-03r'tS
CATIIO AUALYSI S NAME I,(ETHOO
159? TCL Votatites by 8240 - Uater SU-846 82108
5ee rever5e sde lor explandtion of symbols and abbrevrations
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(iI)Lancaster Laboratories
A Thermo Analytical La boratory
QLTALITY COI.TTROL REPORT
Page: 7 ot
LCS LIiIITSLOU H I G'd
LLr sampl-e No. 25380CfJ
CU-1 JUD Matrix Spike Grab r"later Semote
Hercutes: Bacchus Pond
Group l{o. 522727
!'iencutes, !nco.porated - DE
Sanp I e
nDt
Samp I e
UII I TS
1258 Chtoromethane5. u9/ t
1257 Brornomethane3. ugl t
349? VinyI ChIoride?. us/l
3494 Ch t oroethane3. u9./ t
3497 HethyIene ChLoride?. us/ L
J498 Acetone6. us,/ [
349C Carbon 0isul.fide3. us/ t3500 1,'l -D ich loroethene1. us/t
3501 1,1 -Dich toroethane2. u9./ t3503 Ch Loroforrn
1 ' ug/t3504 1,2-0ichtoroethane?. u-o/ |
0J16 2-Butanone3' us/[3505 1,1,1 -Tr ichtoroerhane1. uslL3506 Carbon TetrachloriCc1. ug/t
3507 Vi nyt Acetare2' us/ L3508 Bronpdichtoromethane1- ug,iL3509 1,2-0ichIoropropane1. ug/L1516 cis-1,3-Dichtoropropene
1 ' us/t3511 frichtoroethene1. uglt
3512 Dibromochtoromerhane2. ug/t351i 1,1,2-TrichLoroerhane2. ugl L
3515 Benzene1. ug/t
3510 trans-,l,3-0ichIoropIopene'l ' ug/t
S LAIJK
DUP MSRF9 I{S IiSD ITPD
LCS LCS
LCS DUP RPD
4592 TCL votatites by 8240 - uater Batch: 196184lAA
N.9.
N.9.
N.9.
N.!.
N.9.
ri.i.
N.D.
N.!-
i!.!.
N.D.
N.9.
t(.0.
!{.9.
t.D.
N.9.
N..!.
N -C.
ti.9.
x.D.
N.9.
8
8
9
9
J
30
4
7
3
l,
4
l+1
2
'l
5
?
l,
1
i4
'16
0
12
73 58
33 31
9C 32
67 51
102 98
67 9'l
75 7?
',1!, 1 06
191 1 CC
115 i09
96 10C
(,1, 97
1' ltr 1 14
1',: 1 :10
99 10q
9Z 1 rl'l
97 101
',c5 105
-q7 99
82 96
1D/. 10/,
f i02
MEMBEFlTXrE
Lancaster Laboratofles
2425 New Holland Pike
PO Box 12425
Lancaster. PA 17 605-2425
717-656-2300 Fax [phone] Rev ,OOOr* d?'>:: reverse srco'or elpanat,on c'i/Tools anc dbbrevratron\
LLI sample No. 2538CCCI
CU-1 JUD Hatrix Spike 6rab Uater Sampte
flercutes: Bacchus Pond
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LCS
LCS DUP
102
108
107
i00
98
97
107
,1 0'1
i11
102
'1 03
104
'1 00
DUP ItlS
RPC MS I.ISO R2D
Lancaster Laborato ries
A Thermo Ana lytica I Laboratory(il)
Group No- 52?727
Hercutes, !ncorporated - 0E
Paqe: B of
LCs LCS LIIIIITS
PPC LOU HIGiI
Safipte
UII TS 6LANK
3518 Bromofocm1. us/l N.0. 7i 90
3521 4-Methyt'2-pentanone5. ug/l N.D- 65 93
3520 2.Hexanone7. uslt N.D. 62 95
352? TetrachIoroethene
1 . u9/ t N.c . 1Db '105
3523 1,1,2,2-ferrachtoroethane2. us/t l,i.D- 72 94
35?4 Totuene?. u9/ t r( -3 . 1C5 1e5
3525 Chtorobenzene1. uS./t N.9" 101 10i
3526 Ethytbenzene?- u9/ t N.9. :10 1C9
3528 styrene1. us/t H.0. 1C2 '123529 Xytene (total.)1. ug/t N.D. lCB 103
5780 trans- 1,2-Di chtoroe:hene2. ug/t N.0. 1c4 9E
6268 cis-1,2-Dichtocoethene2. us-/L N.D. ",16 102
1722 Thattiun Barch:961921848002170. ug/t N.0. (1) i01 101
1743 ALuminuo Batch: 961921843C0257. ug/t N.D. 17t, -772 -7?9 (2)
'1744 Anrinnny Barch: 96192184830215. uslt N.D. (1) 1JS 106
1746 Earium Batch: 961921848002Z.? us/l N.D- 0 ('l ) g7 38
1747 BerytLium Batch: 9619218480C21.5 us/t 0.0016 J rE,/l (1) 97 97
1749 Cadmium Batch: 961921843002
?.7 ug/L N.9. (1) 94 95
1751 Chrornium Batch: 96',:92184BCC2/..3 uglt N.D. 0 (1) 78 79
1753 Copper Batch: 96192',184BC023.8 ug/t N.D. 0 (1) -201 '191
1754 tron Satch: 96i921848CC25.9 us/t 0.0607 J mg/t 171, -1513 -1t,41 (?)
1755 Lead Batch: 96',192134300218- uslL N.D. 0 (1) 92 95
1758 Manganese Satch: 96'19218483022.9 uslt N.D. 0 (1) 59 61
176'1 tticket satch:96'192181i39025.4 uglt N.g. 0 (1) 94 95
1766 Si tver Eatch: 961921e1'B3023.6 ug/t N.0. ('1 ) ?9 :C]
(1) The result for one or both deterilinations was !,ess than five tintes the'-0c.(Z) The background resuIt ras more than four tinres tha spike acided.
Sallpte
IIDL
Lancaster Laboratofles
2425 New Holland Pike
PO Box 12425
Lancasler, PA 11 605-2425
7l 7-656-2100 F ax: 7 11 -656-2681
80 1?0
B0 120
80 120
80 120
80 120
80 120
80 120
8C 120
cn 1)O
80 1?.0
80 120
80 120
B0 120
alD_
2216 Rev ,OUOrr, ?a#
?1
t+3
)
26
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2
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0
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24
1
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MEMBEFI
reET
QLIA],ITY CONTROL REPORT
5ee reverse srde for expianatron of sTmbois 6nd abbreuations
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(iI)La ncaster Labo ratories
QI.]ALITY CONTROL REPORT
Page: 9 of 11A Thermo Analytica I Laboratory
LLI sarnple No. 25380C0
CU-1 JUD Matrix Soiie Grab tJater Sanpte
tlercutes: Bacchus Pond
Group tlo. 522727iiercules, !ncorpocated - DE
Sarpte Safl.roteI,IDL UII I TS
1772 Tinc12. ug/t
7035 Arsenic TR?-7 us/|
7036 SeLenium TR2.7 ug/t
0259 llercury0.43 uslt
0937 TCL Pesticides in Uaters
BLAIIK
Batch: 96i9218/+8C02
ri.D.
Batch: 96,1921848002
N.D.
Satch:96',!9218(BCC2ll.0.
Batch: 96:985713001
ll.D.
Batch: 96-183C005.1
!i.9 -
N.D.
N.D.
N .9.
N.r.
N.D.
N.D.
N.0.
N.D .
N .D.
N.D.
I.0.
t{.0.
N.!.
N.D.
N.9.
ll.D.
N.5.
0(1) -41 -34
0 (1) 101 't02
0 (1) '101 102
0 (1) 79 79
OUP HSRPC !'IS IISD RPE
LCS LCStCS DUP RPD
LCS LI[IITSLOU fl t Gil
80 120
80 r20
B0 120
80 120
5
'I
1
0
101
'!03
103
108
1600 Atpha BHC0.002 ug/t1601 Beta BHC0.008 uslt
1503 Del ta BHC0.005 ug/t
1602 Gailnla 8HC - Lindane0.002 ugl I1604 Heptach Ior0.005 u9/ t1605 ALdrin0.004 u9/t
1606 Heptachtoc Epoxide0.003 u9/ l'1616 Endosutfan I0.003 uglt.1610 Dietdrin0.005 us/ t
1607 DoE0.005 u9/t
1511 Endrin0.0C5 ug/t1615 Endosutfan I I
0. Cl u9/ t1608 DoD0.007 us/t
1617 Endosutfan Sut fa'te0-007 us/ t,I609 DD I0.008 u9/ t0938 Endrin Ketone
0. C0/. rrgl L1860 Hethoxychtor
0 .03 rrs/ t
1361 Atpha Chtordane0.00t us/ t1362 Gannra ChIordane0.005 us/ t
96
97
s5
76
73
87
o,
o2
11q
9D
90
C)?
94
d/
'l112
91
86
95
97
85
76
76
86
33
83
g4
i14
39
93
9?
aa
1C2
90
8c
67 122
7t+ 120
69 126
66 120
54 120
42 120
6!, 120
60 1?0
66 12C
60 1?O
71 1.29
67 120
67 121
53 128
7', 120
76 120
57 110
75 120
75 120
90
0'r
00
92
72
69
92
BB
9C
o,
',2
97
95
97
93
94
cl
91
0
't 1
01
0
1
4
c
2
0
(1) The result for one or both deterfinations xas Iess tharr frve rines the !00-
LanCaster LaboratOfleS
2425 New Holland Prke
PO Box 12425
LancasteL PA 17 605-2425
717-656-2300 Fax: [phone]
MEMBER7Xm ,orror,, dop5ee reverse srde for expianarron of symbols aod abbreytattons 22 16 Rev
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Group No. 522727
llercutes, Incofporated - DE Il
Sanp I e
I'(DL
Samote
UNITS
9UP
?.?)
14s
RPO
tCS LCS LCS LIIIITS
DtiP RPD LOU illcH 1l
1613 Toraphene
1 ' u,/l
1618 Endrin Atdehyde
0.0 10 u9/ t
1619 PCB-10160.09 usl t
1620 Pcs-12210.2 us/ t
1621 PCB-12520.09 ugl t
162? PCB-12t+?0.05 u9/ t
1623 PCB -',l248
0.07 ug/l
1624 PCB-12540.06 u9/ t
1626 PcB-1260O.07 ug/l
12659
LCS
9?
ilsD
31
MS
36
'11
4678 TCL SU846 Semivotatiles/uaters Eatch: 96'13/+uM025
3918 phenoI2. us./ t
1867 bis (2-chIoroethyt) etherz. ugr!3371 2-chtorophenoI2. us/t38B3 1,3 -di ch Iorobenzene2. ug/t3884 1,4-dichtorobenzene2. ug/t3882 1,2'dichlorobenzene2' us/[
4680 2-methytphenot4. u9/ t1681 2,2'oxybis (1-chtoroprooane)
4.ug/ t
4682 4-methytphenoL1. us/ t
3915 N-ni trosodi -n-propytamine
L.ugl t
3902 hexachtor-oethane1. ug/ t3910 ni trobenzene?. ug,/ t3904 i sophorone
?.u9/ t
391'l 2-ni trophenoI
Lan(aster Laboratofles
2425 New Holland Pike
PO Box 12425
Lancaster PA 17605-2425
717-656-2300 Fax: [phone]
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12 158
?3 134
1 172
20 i?4
32 129
46 123
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5 152
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40 1',13
35 i8C
21 196
29 132
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QI-IALITY CONTRCL REPORT
(il)La ncaste r Laboratories
A Thermo Analytical Laboratory
I,LI Sarnple No. 25380C0
CtJ-1 JUo Hatrix SpiKe 6rab UaEer Sampte
Hercutes: Bacchus Pond
S LAH(
N.9.
il.!.
iI.9.
N.!.
N -D.
[.!'r.
N.3.
N.9.
N.0.
1.u9/ t
see reverse srde for explanatroo oi symbols and abbrevratrons
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LLr sampl-e No. 253E0C0
CU-1 JUD Matrix Spike Grab !Jater SarnoIe
Hercutes: Bacchus Pond
i
, Grouo No. 52?727
ilercutes, lnc:olJorated - ![
I
9C 90
79 81
33 83
65 69
91, 9_1
86 97
) | ))
39 &7
Be s8
9^, 90
97 97
32 31
92 93
30
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37
115
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Page: 1'l of 14
LCS LI14ITS
LOIJ H I 6H
3Z 119
33 184
39 135
21 133
t/ I i6
24 116
?? 147
23 123
1 100
37 141
19 151
60 118
1 112
33 11.5
Sampte SamDteMDL UNITS
3890 2,4-dimethytphenot2. us/ t
3866 bis (2-chLoroethoxy) merhanez' us/l
3886 2,4-dichIorophenoL4. u9/ t
=921 1,2,4'trichtorobenzene2. u9/ t3905 naphthaLene2. us/ t
3871 4-chlocoanitine4. ugl t
3900 hexach Iorobr:tadi ene2. u9/ L
3872 4-chIoro-3'methytchenot4. u9/ t
3905 2-nlethytnaphthatene?' u'/t
3901 hexachtorocyctopentaCiene6. u9/ |
3923 2,4.5-trichIorophenot2' u,/l
3922 2,4,5-trichtorophenol.?' us/ t
3873 2-chto.onaphthaLene2. ug/t
3907 2-nitroani Iine?' usl t3891 dinrethyL phtha'.ate6' ug/L
3858 ac enaph thy t eneZ. ugl t
LC9 LCS
LCS DUP RPD
DUP TSRP9 MS MSD RPDBLAI.IK
,,i -9.
ll.D.
}I .0.
H.D.
N.D.
il.9.
N.!.
N.D.
N.D.
N.C.
N.9.
N.0.
ti.0.
N.D.
7
0
0
J
0
2
7
.1
1
5
J
1
'1
0
'1
2
65
a/
7t
B1
t)
t+5
91
t,,,
91
90
BB
95
?5
B6
4679 ICt- Su846 SemivotatiLes/Uarers Barch: 96-184HM026
3908 3-ni troani t inez' ug/t3857 ace.naphthene?. ug/ L
3891 2,4-dinirrophenoI10. us/l
3912 4-ni trophenot10. ug/L3879 d i benzofuran2' usl I
3391 2,4-dini trotoLuene/,. ugl I
3395 2,6 -di ni t rotoI uene?' ug/t
8C
91
41
1,7
c)5
9<)
1
0
5
1
1
80
92
55
B5
9/1
95
17 ,"(5
1 191
1 132
23 111
39 119
50 158
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Lan(aster Laboratofies
2425 New Holland Prke
PO 8ox '12425
Lancdsrer PA I 7605-2425
717-656-2300 Fax: [phone] ,orrorn, d3
Qr_TALITY CONTROL P.EPORT
Se" e./e,)e Srde for e<p anat,or ol symbols ano abbrev drron5 2216 Rev
QUALITY CONTRCL REPORT(I)
LLr sample No. 25380CO
CU-1 JUD Marcix Spike Grab uater Sanpte
Hercutes: Bacchus PoM
Lancaster Laboratori
.A Thermo Analytical Laboratory t
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Page: 1? ol
LCS LCS LIIIITS
RPD LO''J II I GiI
Group *o- 52?727
HercuIes, Incorporated - D€
Sampte
IiD L
Saflp I e
UNITS
3887 diethyt phthatate4. uglt
3875 4-chIorophenyI phenyt ether1' uE/t
3898 ftuorene2. uglt
3909 4-ni troani I inet - ug,/t
4683 4,6-dini tro-2'methylphenoL10. u9/[
391t, N-ni trosodiphenyIanrine4. uS/ t
5869 4-broorophenyr. ohenyr. ether1. uS/ L
3899 hexachLorobenzene2. us/t
3916 pentach IorophenoIZ. ug/ t
3917 phenanthrenez' u9/ t
3859 anthracene2. uglt
468t, carbazote?' ug/t
3880 di-n-butyt phthatate2. u9/ t
3897 ftuorantheneZ. ugl I
3919 pyrene?' ug/t
3870 butyt benzyt phthatare4. uq/t
5885 3,5' -dichLorobenzidine1.. uglt
1350 benzo (a) anthracene2' us/t
3868 bis (2-ethythe.(yt) phthaIate1.. u9/ t
3375 chryseneZ. ug/t
389b di -n-octyt phthatate4. usl t
3861 benzo (b) fl.uoranthene4. ug/ t
3862 benzo (k) ftuorantheneq. ug/L
3864 benzo (a) pyrenet,. ug,, t
3901 indeno (1,2,3-cd) pyrene
OUP
RPDB LAIIK
N.0.
,i.0-
ll-D.
N.9 .
N.9.
ri.9.
li .9.
,r'-9 .
N.9.
N.D.
N.D.
N.D.
N -0.
N.0.
N.C.
N.D.
N.0.
N.D.
ti -!.
t'.D.
N -9.
!i-3-
N.).
61, 65
1C3 iO?
102 98
67 61
oo aa
96 94
!4 -a 4C
95 9t
if, Dt
92 9!
39 37
90 g9
91 91
81 80
79 73
36 g5
91 91
l CC ',C7
90 38
95 95
cl 3l
/,\ l\
LCS
259
1 !01
198
086
s82
2A4
285
295
11 9C
c92
185
289
2Bi
292
382
277
0 B1,
'I 102
c9c
6 10/.
094
c 8i
,' !2
1 1111
?5 158
59 121
3B 122
38 1t7
53 127
'I "152
14 175
5t+ 120
?7 133
40 137
1 118
26 137
52 115
1 l<t
1 114
33 143
B 158
17 168
4 t40
?4 159
11 161
17 163
I 141
7Xm
Lancaster Laboratories
2425 New Holland Pike
PO Box 12425
Ldncaster. PA 17 605-2425
717-656-2300 F ax: 7 11 -656-2681
,1 il)rl5 Rev 1O/10/q5 Ylt
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(il)La ncaste r Labo ratories
A Thermo AnalVtical Laboratory
LLr sanpre No. 2538000
CU-1 JUD [arrix Spiie Gcab tJater sanlcte
Hercutes: Bacchus Pond
Grouo No.
. liL-t'cuteS,
I
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5Z?.7?7
lncrrDoratL.d ' 0E
sarrp t e
TlD L
3881 dibenz
4.
3863 benzo
1..
Samp t e
UNIIS
(a,h) anthracene
u9/ t
(ghi ) perytene
u9/ t
!ls
TPD
OUP
RPD LCS
LCS LIMI-IS
LOU H I C.l
227
?19
S LANK
t{.3 .
N.D.
Lancaster Laboratories
2425 Ne,{ Holland Prke
PO Box 12425
Lancaster PA 11 605-2425
717-656-2300 Fax [phone] Rev ,Orr.r* d}
BB
7l+
B6 2
1
9l+
MEMBEFl
TaKm
QLTALITY CONTROL REPORT
5ee re'ierse side for exoianatroo oi symools and abbrevratrons
{>La ncaster Laboratories
A Thermo Analytical Laboratory
QUALITY CCNTRCL REPORT
SUNROGATE L!MITS
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LLI sample No. 2538000CU-l JUD Matrix Spike crab Uarer Safltote
Hercutes: Bacchus Pond
0937 TCL Pesticides in Uaters
4592 TCL Votatiies by 8240 - uarer
4678 TCL 9U846 SenrivoLati les,/Uaters
t+679 lCl SU3,i6 Senri votat i Les/',.'ate.s
I
ii Group llo. 522727
i l'lercuIes, !ncorporated - DE
SURROGAIE SUM!'1A.RY
TRIAL IO SURROGATE RECOVERY Z
TCX 70
DCB 90
c4-1,2-DCA 9.3
c3 - to i. uene 1 D4BrB :'10
?-FlphenoL 6:
Ph ene i - C5 !.?
2,4,6-T9? 36
N: trobz-C5 9?2-fbipl-rnyl 9-\Tpireny'.C]4 35
60
6C
76
!o
B6
)1
10,: Ll
l5
43jj
H I6H
'120
120
114
110
I15
1C0
91
116
it,1
iEffif,i
Lan(aster Laboratores
2425 New Holland Pike
PO Box 12.125
Lancasiei PA 11 605-2425
7 17 -656-2300 Fax 7l 7'656-268 l ,orror$ d'}5ee reverse stde {or expldnatron of symbols and abbreviatrons
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(I)Lancaster Laboratories
A Thermo Analytical Laboratory
LLI sample No. EL 2538C01Co[[ected: 6/26/9i, ar 12:05 by gR
suBnitted: 6/28/96 Reporred: 8/ 1/960iscard: 8l 9/96
CU-1 JUo Matrix Spike Dupticate Grab Uater Sarnpte
Hercutes: Eacchus Pond
CUJUD 506#: HBP0l -031'tSD
CATIIO. A}IALYSIS NAITIE
4592 TCL Votatites by 8240 - Uater17ZZ Thattir.nn1713 Atuninunr174/. Ant inlony1746 Bar i um1747 Beryt I ium1719 Cadmium'1751 Chromium1753 Copper175t I ron1755 Lead1753 I'langanese1761 N i ckeI1766 Si Iver1772 Zinc7035 Arsenic TR7036 Seteniunr TR0?59 ilercury0937 TCL Pesticides in Uatcrs4678 TCL 5U84o Semi vol at i Ies/!Jarers4679 TCL 5U846 SerrlvoLari tes,/'Jaters
1 COPY TO Harcules, Incorporated
1 CoPY T0 ERl.l - Rocky Moulrrain
Account tlo: 06716
llercutes, Inco.porated - DE
Envi ronoEntn i r.f f a i !'s
t,li tmington CE 19894
A9 RECEIVEl
.I:::::::::.::1.:+:j:rr.:i::.::..-:::.: r:r:.r: l!EIHOO
ri;niiil;,;r:i:i.ii:REs?Lls ,!, DETECT! 3{ L!Mlr uNl rs
See Pa_qe
l7q . ug/t-57. \s/ |15. ug/l2.2 ug,/ i
: -l ug/'.?.7 u9/
".4.i u!;,/,.
5.9 ug/i
1S - ug/ 1,
2 O t'd-tl
= .t, us/ L
I .6 'tg,t '.12. us/l?.7 ug/ :-
2.7 u!/ |
!) . i3 u9,/ !
see Page
tr-e 2a9a
aso O,r-:
Page: 1 of 14
P .0.
Ret -
AITN; !1r - Joseph Ket ier
ATTJ,I : Yr- Brent R0binson
Ouejtlons? Cont.rct your Cl icn: SL'rvicu: ReDreseniative
Rachel L. Kreamer ar (7' t') 556-2_i30
0l:3C:22 D 0002 15 REP 1J61.lb \?2727
I
lro ts.oo ocl26roo ASRooo
Lancaster Laboratorres
2425 New Holland Pike
PO 8ox 12425
Lancastet PA 17 6A5-2425
717-656-2300 Fax: 717 656,2681
Reseectful 1y submi rted
Rarona V- Layrra:t, 6roup Leader
: C? lie:e I s:,/l-eaclraresI
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7Xm ,orror$ d3Se reverse srde for erptanatron of srmoorS ano abbrevratrons 2216 Rev
Hercules: Eacchus Pond
CUJUD SDG#: HBP01 -03MSD
CAT[O. AI,IALYSIS IIAHE
TCL Votatil,es by 8240 - Uater
1258 Chtoromethane1257 Bromomethane3492 VinyL chLoride349tt Ch Ioroethane3497 t{ethytene ChtoriCe3/.98 Acetone3499 Carbon Disul.fide3500 1 ,1 -D i ch Ioroethene3501 1,.l-oichLoroethane3503 chtoroform3504'1,2-0ichtoroethane0315 2-Butanonel5C5 1,!,'1-TrichLoroethEne3506 Carbon Ierrachtoride3507 Vinyt Acetate3508 Eromodichi.oromethane3509 1,2-0ichtoropropane3516 .cis- !,1-DichIoropropene1511 Trichtoroethene3512 0ibro{oochtoromerhane35i3 1,1,2-TrichLoroethane3515 Benzene1510 trans-'1,3-Dichtoeopropene35'13 Brornofo.m3521 4-ltethyL-2-pentanone3520 2-liexanone15?? TetrachIoroethene35?3 1,1,2,2-Tetrachtoroethane3524 Totuene3525 Chtocobenzene3526 EthyIbenzene3528 styrene3529 xytene (totat)
5780 trans-1,2-Dichtoroethene6268 cis-1,2-Dichtoroe!hene
AS RECETVEO
:.rij.j:..ii:.:!.:.sii:j:i::i:::::::r: :i.::ii1:ii !'( E I H OC
'iiill:,: iiir?g.q!i.F'IFiiil:.:: oETECTrcN LIMIT uNrIs
Page:
P.0.
Ret.
Rea;pecifuL ly S:bnri tteci
liiaire',c t'c!'.arin, 8.A.
Croup ;e.cler, C:/1,1! Volat'i Les
?of 1L
2216 Rev lo/3o/rs d},
(l)La ncaste r Laboratories
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A Thermo Analytica I Laboratory
LLI sample No. EL 2538001cottected: 6/26/96 at 12:05 by BR
Suhnitted: 6/28/96 Reported: 8/ 1/960iscard: 8/ 9/96
CU-1 JUD l,latrix Spike Duoticate Grab tJater Sampte
' :r,,,.j,: :,:,:::::,i:.,r:,:':::,jr;.: :,,:,,.: :,::r:,:,:::::.::.1 ::::i.!:i.::. :!.::.t9, !: :..
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ouestions? Contact your Client
RacheI r-. Krearner
Servi ces Reoreseniat i ve
ar (7':7) 656'2i10
Krril
Lancaster Latro.atofl es
2425 New Holland Prke
PO Box 12425
Lancaster, PA 17 6A5-2425
7 17 -656-2)00 Fax: [phone]
I
I Accou^t llo: 067'15
I Hercutes, lncoroorated - DE
i EnvironmentaL Af fairs
j uitmington 0E I9894
I
See reverse srde for explanatron oi ;/mools and dbbre'.1atrons
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(iI)La ncaster Laboratories
! Account llo: 06716
i tlercutes, !n;orporated - DE
I Envi rormenral Af fai rs
: '.ilminoton DE 19894i'
P.0.
Ret.
Respecr:iut ly 9,rbrri t ted.jenife.:. liess, B.S.
6roup rerdcr Pesticides/PCBs
Page: 3 of 14
A Thermo Analytica I La boratory
LLI Sample No. EL 2538Cr01Cottected: 6/26/96 at 12:05 by BR
Suboritted: 6/28/96 Reported: 8/ 1/96Discard: B/ 9196
CU-l JUD Matrix Spike oupticate 6rab lJate. Samole
Hercutes: Eacchus Pond
CUJUO SoG#: HBP01 -0lMsD
CATNO. ANALYSIS IIAME
TCL Pesticides in Uaters
A9 NECE!VED. t'lETlt9o
;tisuurs,, , ogTEctrcir LIHIT u$lIs
1600
1601
1603
1602
'1604
1605
1006
1615
'1610
1607
151 1
1615
,1608
i617
1 509
0938
1860
1361
1362
1615
16lB
1619
1 620
16?1
16?Z
1623
1624
1626
c.i|10rl ,rG
u.2r' aa
0.t5
c.f;i'
u9/ |
ug/t-
u -a,/ t-
ug/t
,tg/ t
':g/ t
us/ i
urJ/ i
rg/ t.
ugl I
u,f,, i,
ur,/'.
u9/'.
ucj/ t
ug/ i
u?/',
ug/:'
,rsl i
u.) / ',
'Jg/
"u3/ L
u9/ t'
19/ t
u9/ 1.
,r9/'\
ur/ t.
Al.pha 8HC
Beta 8HC
DeLta BHC
Ganma BHC - l-indane
l{ ept ach I or
Aidrin
Heptachtor Eloxide
Endosut fan I
Die!.drin
CDE
Endr i n
Endosut fan I I
00D
EndosuL fan SuI fate
DDl
Endrin Ketone
I'lethoxych'.or
Ar.pha Ch !ordane
Gaftna ChLoriane
Toxaphene
Endrin Atdehyde
PC6-1016
PCB - 1221
PCB - 1 232
PCE - 17t+2
PCB - 1 218
PC8 - 1 254
0"2(
L\: l9:.
c.2l
! - :..j
PCe-]2oC :::::r::ii:::.:i:.!:i::.:'::: '.' ll.!:: C.:7
Due to insufficient sanrpte size, le were urable':o regort our usual
quantitation r.iflrits. The vatues reported.epcL:s,:'nt rlle Ioeest quantitation
t imi ts obta inable.
0uestions? Contact your Ctie.i Ser!ices ?epIeser:ative
Raahe! '-. KFearfler ar (7:;l 65f,-21!:0
Txnir
Lancaster Laboratones
2425 New Holland Pike
PO Box 12425
Lancaste( PA 11 605-2425
1 17 -656-2300 F ax'l 11 -656' 256 1 d?5ee reverse stde for explanatron of symbols and abbrevratrons 22 16 Rev l0/30/95
(iI)Lancaste r Laboratories Page:l+ of 1L
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]lA Thermo Analytical Laboratory
LLI sample No. EL 2538001Cottected: 6/?6/96 at 12:05 by BR
suhritted: 6/?8/96 Repor(ed: 3/ 1/96
oiscard: 8/ 9/96
CU-1 JUo ilatrix Spike 0upticate Grab Uater Samcle
rll
Hercutes: Eacchus Pond
CUJLO SDG#: llBPO1 -03MSD
CAINO- ANALYSIS UAHE
TCL SUB46 Semivotati tes/iJaters
3918 phenol3867 bis (2-chloroethyl I "91t..387!, 2-chtorophenoIj883 1,3-dichtorobenzene3834 1,4-dichtorobenzene3832 1,2'dichlorobenzene4680 2-methyIphr'not4581 2,2'oxybis (1'chIoropropanel
t+682 4-nrethytphenoI3915 l.l-ni trosodi -n-propytamine
3902 hexachtoroethane
3910 n i rrobenzene3901 isophorone
391 1 2-ni trophenot3890 2,4-dimethytphenoL3866 bis (2-chIoroethoxy) methane3886 2,4-dichl,orophenot392f i,2,4-trichr.orobenzene3906 naphtha I ene3871 4-chtoroanilinef900 hexach Iorobutadi ene3372 4-chloro-3-methyLphenoI3905 2-methytnaphthaLene3901 hexachtorocycLopentadiene3923 2,4,6-trichlorophenoI392?. 2,4,5 - tr i ch IorophenoI3815 2-chtoronaphthiriene3907 2-nitroanitine3891 dirnerhytphthatate3358 acenaphihyLene
; Account No: C6716
I tlercuIes, !ncc.porated " 0E
i lnvi ronmcnrai Aliai !'s
I HiLnringtcn 3E 191]94
AS TSCEIVEO
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ouestions? Contac! you!' cIient Servrces Represelltatlve
Rachul !-. Krearnar at (717) 656-?-{10
MEMBER,Ekm
Lan(aster Laboratones
2425 New Holland Prke
PO 8ox 12425
Laocasrer PA 17 605 -2425
717-656-2300 Fax [phone]
ResDectf ui':y S,]bm! tteC
Christine u. RatcLif+, B.S.
c.ou, -eader, 6C/149
See reverse side for explanalron oi svmool5 anC abbrevratton!Rev,0,30,e5 i? l'
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(iI)La ncaste r Labo ratories
Account llo: C6716
Hercutes, incorporateC - DE
6nvi rormentat Alf airs
llltnington !'E 19894
Page: 5 of 14
2216 Rev,Orr.rn, d3
A Thermo Analytical Laboratory
LLr sample No. EL 253800!Col.tected: 6126/96 at 12:05 by BR
Suboitted: 6/28/96 Reported: 8/ 1/96Discard: El 9/96
CU-1 JUD xatrix Spike oupticate Grab Uater Sampte
P.0.
ReL.
Hercutes: Bacchus Pond
CUJUD SDG#: HBPO1 -03MSD
CATItO, AIIALYSIS }IAI(E
TCL SUB46 Sernivotat i Ies/Uarers
AS RECEIVED
3908 3-nitroani Iine tiii.ii::r::l:...:.',..i'1d]0.: . :::13857 acenaphthene ii.:,:::i::l:.',,.::.,.,,.1(rd. '
3893 Z,4-dinitrophenot .ii':,:,j..: .: 7!'. '.
3912 4-ni trophenot ::,:tii::,it::,:'!i:, i, B).3879 dibenzofuran i,':..':t:,:,,.', ,'.,fgU-.389/. 2,4-dinitrototuene .',:i,,.:;:,.1:,,'. .,.1?C.3895 2,6-dinitrototuene :i::,::i:,itri, ,,...,2,,".]887diethyl.phthal'ate....1,',;.;1;;,'..,iJ'.3875 4-chlocopnenyt phenyL erher ;:.:.:..,,.':,,., :,?lC,i. . .,'3398 f I uorene l.i.:':::,.i.':, ., 200 .3909 4-nitroaniIine ,.,i:::,'i.:' "1zP-
1683 4,6'dinitro-2-methyr.phenot .i::'::.::.:, ..'llil.3911 tt-nitrosodiohenylamine i,t,t,t,tiir:.:..", .,,':;'0.3869 A-bromophenyi. phenyl ether i:ii:::il::,::],: ..:::'17C.3899 hexachtorobenzene ii,,l..ii:' ,it,J.3916 pentach locophenol :::::'::,i,:: : 80.i917 phenanthrene .i':':,ii :, i ,.i.Jl.3859 anthracene 'ir.,...,.'.'. ,tn.4084 carbazote tii.;.i:,r,,t. .lrc.
3880 di-n'buty[ phthatate ,l;::,::.:, ',7'a.3897 f luocanthene .; ;',,;:,,,,, i ,, r31:-
39'i9 pyrene .i:..,iii:.:', i., ,1311.
3e7D butyt benzyt phthar.are ..;i.,:ti1il, l''', ,U,.3885 3,3,-dichLorobenzidine t.:,',.i.,.., ,. :.,tr,;_
-1860 benzo (a) anthr6cene ti:j...i.,,:,t,t':,ji' 'i7!.3853 bis (2-ethylhexyi) phtha!.ate',',.;',,..." .',2r:D-'3876 chrysene :i,,':.:::1,i.,:,:::. 1.9J,.3896 Ci -n-octyl. phthal.ate :;,rt.;,,,,,,1.iir,:,:,',,.:::it..3801 benzo (b) fLuoranthene i::..:.:' 1UU.3862 benzo (k) fluoranthene ,:...,,"' ',;',386/- benro ( a) pyrene ..'.'i. i Z:.3903 i;rdeno ('l ,2,3-cd) pyrene .':'..,..: 15,r.3381 dibenz (a,h) anthracene .:.1:::!::. 1.7i.3861 benzo (ghi ) peryLene ::"''.., r 1qa.
3ue to insufficient samp(e, the qranti!atjcn .rrn:rs
semivo[;.ti Ie conpounds were raisec.
li!':::.1::.i.!'!: rlrca,r rc l,lE T 5CD
DETECTIq{ LIi{!T !IIIIS
z' ugliZ. u-o/ i
1C . ULJ/ |
'I r-1. ugl t3' usli4. ug,/i2. ug/':4' ugil'
!, . !.-J/ i2. ug/t1. utJl'l
10 . t:c/ '.
4. ,tg/:
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1 . u._r,, -t-, ,sg/t-
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for the C!./!{!:
Questions? Contact youe Cti..ni
RacheI L. (reamef 5..ryi ceS lleDresen!a t i ve
at (7'.i ) c,.r6-2l(JD
iEHii
Lancaster Labolatofles
2425 New Holland Prke
PO 8ox 12425
Lancaster, PA 17 605-2425
717-656-2300 Fd\. 1 11 -656-26a1
Respectf,-rt ly Srbr! tted
Chrisrine U. &n:cliff, 8.S.
i.ouD -ead."r, 6ClUS
5ee reverse srde for explanatrcn oi synbols and abbrevratrons
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I,ABORATORY CIIRONf CLE
(il)La ncaste r Laboratorieb Page: 5 of 11 ]l
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A Thermo Analytical Laboratory
LLI Sampie No. EL 2538CC1
Cottected: 05i2cl96 at 12:05 by 8R
submi tted: 06/?8/96
j A."oun. No: 067'16
i HercuIes, Inccrporated - DE
: Envi ronqrc.ntsi Affai cs
iili!.mingron 3E 19J94
CU-1 JUo Matrix Spike Dupticate Grab'ieter Sar":[e
Hercu[es: Eacchus Pond
C'JJUD SDG#: HBP01 -0lrSD
CAT,IO AIIALYSIS NAME
L59Z TCL votatites by 8240 - Ll.rter
I!ETHOO
su-845 82408
su-945 6310A
st-3/,5 6110A
su- 8j.,5 6J I CA
SU-845 6,--l'lDA
s,;-8l,6 6-110,1.
5f-3{5 6,!l0r'r
,qrJ-845 6l'l0A
9:i- 3i6 5-l lDA
:rt-S4C,5-rlCA
5';-346 i)illi-]n
:u-3.46, o)1tA
S,J-84o cli:rri
sr-345 6li,lA
s',i- 8{5 5]1'-14
c.i-ir - :a'14^
Su-3(6 cllLlA
.rr,E/! r11.1i
su-845 7r,70A
S';- .lq6. 7.''7lA
s'j-845 ii'l0B
Sii'846 !j.i31
S'J'B4i' l) 1 C0
SU-32;{, 52700
s":-tt,4.J:7q.3
ANA'.YSI5
TRIAL DATE AIIO TII.IE
1 O7/C3/96 ltSE
AI{A!.YST
Susan A. Mcllahon
oonna R. Sackett
oonna R. Sackett
oonna R, Sackett
Donna R. Sackett
Donna R. Sackett
Donna R, Sackett
0onna F.. Sackett
Dona3 ?. Sacketr
lonna R. Sackett
0onna t. sacketr
Oon.a R. Sacketr
Donna R. Sacke!t
Do:ina R. sackert
Dcnna R. Sackett
Christine I't. conlin
oonna R. Sackett
oonna R. Sacketr
NelLi S. tlarkaryan
xc=1. i. i S. Harkaryan
Harcie A- NataIe
0ou9[as 9. Seitz
l{aria A. 0avenpor:
Saeplran!e l!. Shenk
Siephenie l!. Shenk
172?
1743
174t,
1746
1747
1749
1 751
1753
175t+
1 755
i 758
1761
1756
177?
1 848
7U35
7016
Thattit-un
A t umi nurn
An t i mony
Bar i un
Bery[ [ i run
Cadlni sr
Chrcrni um
Copper
I ron
Lead
I'lan9anese
t{ i cketSitver
Tinc
',{u SU846 M Digest (tot rec)
Arsenic TR
seLPniuin TR
1 A7 t',5 /951 D7/1-</961 07/15/961 27/:5t96i 07/15/t)61 07/.,5/961 07 /"5/e61 A7/15/901 07 /1,i /q61 D7/15/96' t)7/i5/ci6
i O7/15/ctL1 07/15/96't Q7.r i5 /96i C71:91c161 A7/15/961 t-17 /',5 /96
0259 tlercury
5 7'13 UU S'i845 Hg D i 0e: t
0817 uater Samp!.e Pest- Extraction
C937 TcL Peiticides in Uatecs
0813 BIA Uater Exrraction
4b7E TCL Su346 Serrri vol.at i Iesluaters
1579 TCi- SUSl,f, Semivol.ati !.es,/'Ja:ers
?
'2
,1
,]
1
1
1
07/17/96 1619
D7/16t96 Zltg
07./01/96 1jio
a7/16/96 cB12
07/02/96 A930
a7/03/96 f;E',z07/!3/')6 08.2
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Lancaster Laboratories
2425 New Holland Prke
PO Box 12425
Lancastet PA 11 605-2425
717-656-2300 Fax: [phone]
!
fil'
Rev to/30/95 Ya! j
ll
5ee reverse side for explanatton of symbols and abbrevratons 2)16
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A Thermo Analytical Laboratory
LLI sampl-e No. 25380Lr1
CU-1 JUD Ha(rix Spike oupticate 6rab Uater Sarncle
Hercules: Bacchus Pond
Q5AL]TY CONTROL REPORT
Page: 7 of 14
LCS LII'IITSLOU HI 6H
(iI)Lancaster Laboratories
I Cr-oup rlo. 522727
r liercutes, Inco.porated - 0E
SarpI e
MDL
SamoI e
UNITS BLANK
I961841A4
ouP ltsRP' MS I'1SO RPD
LC9 LCS
LCS DUP RPD
1592 lCL Votatites by 8210 - Uater Batch:
1 258 Ch t ononrethane5. u9/ L'1257 8rofllomethane3. u9/ t3192 Vinyl ChLoride2. u9/ t'
3t,91 ch I ofoethane3. u!/L
5497 Hethy(ene ChLoriCe?' ug/ [3498 Acetone6. u9/ [
3499 Carbon Disutfide3. us/ |
3500 1,1 -0ichIorocthene
1' ug'/t3501 1,.1-Dichtor-oethane7. ug/ !l50l Ch t oroforrr
'l ' ug/t
3504 1,2-Dichtoroethane2. u9/ |
0-"16 2-Butanone3- ug/l3i05 1,1, 1-TrichIoroethane1. ug./l
350o carbon TctrachloriCe1. ug/t
3507 Vinyt Ac!'!ate2. us/ti103 SrorrodichLoronethanc1. u9/[350,; 1,2-DichLoropropane1. us./t35'lo c'is-1,3-Dichloroprcpene
1 , Llg,i I1511 Trichtcrocthene'I' u'l[35]i2 Dibrornochtoronethane?' us/ [
35 !3 1,1,2-Trichloroethane2. u!/ L
3515 Benzene1. ug/t
3516 trans-1,3-DichLoropropene1. uS/ |
N.!.
N.!.
\.:,_
t{.1.
l.l.D,
r.l.?.
ri.).
3
B
9
9
J
3C
l+
7
3
t,
t
2
,l
5
2
I,
1
'1.1,
tb
C
12
73 68
88 3i
90 82
t7 6i
1rt? OA
67 91
1C3 110
i15 ',109
96 100
6!, 97
116 ',14
i i 1 110
99 10(
t5 101
97 101
_105 1 05
B7 99
s2 96
1')t* 101'
91 102
7X-TI
Lancaster Laboratoile5
2425 New Holland Ptke
PO 8ox 12.125
Lancaster. PA 17605-2425
717-656-230A Fax: [phone]
,E,
,nr,nro, ?aE'See reverse 5rde for explanation of symbols and abbre'/railons 2216 Rev
QI-IAI,fTY CONTROL REPORT(I)La ncaster Laboratories IA Thermo Analvtical Laboratory
LLI sample No. 25-18C0i
ctJ-1 JUo Matrix Spike Dupticate Grib Uater SarnDle
HercuIes: BacchLls Pond
ii___^_i Grouo lto- ,ZJfZ(
I tiercutes, Incorporated ' DE
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Sampte SampteI{DL UII I TS
3518 Bronroform
BLANK
Lancaster Laboratories
2425 New Holland Pike
PO Box 12425
Lancaster PA 17 605-2425
717-656-2300 Fax: [phone]
OUPRPD MS
LCS LCS LCS
LCS DUP RPD LOU
MS
MSD EPD
LII!ITS
HI6H
1. uglt li.D. 71 90
3521 4-Methyt'2-pentanone5. us/ t N -1. 65 93
3520 2'Hexanone7. ug/t N.D. 6z 95
35?2 retrachtoroethene
'l . u9/[ N.0. 1f:6 i05
3523 1,1,?,7'l ettachtoroethane2. us/t N.3. 72 94
3524 ToIuene?. us/t N.3. 115 1C5
1"25 Chtorobenzene
'l . us,/t N.:,. i1l 10i
3526 Ethytbenzene?. ug/t N-D. :10 1C9
3528 styrene1. usll N.c. ::2 1C:
3529 xyt.ene (totat)1- ug/L N.3. ]i3 103,
5780 trans-1,2-Dichioroethene2. us/t N.r. 134 99
6?.68 cis-'1,2-Dichtoroethene?. u9/ t N.0. 1 C6 1 02
1722 Thal.l.ium Batch:9619218113902170. u-u/t N.D. (1) lC1 'l0i
1743 Alrrnrinun Batch:961921843,-102
57 . usl t li.D. 17t4 -772 '7?9 (2)
174j, Antimony Batch: 96'1921348002]5. ug/t ri.!. (1) 1C5 106
171,5 Earitrn Batch:96192'13/'8lL\2?.? ug/l N.9. 0 (i) 37 BB'li{7 Eery!. I i'-rnr Batch: 96192'!848:rT 2
'l .3 us/l 0.00i5 ,.i nrg,rt (1) 97 97
'1749 cadmiun Batch:96.19?134.3-1022.7 ug/l N.9. (1) 9t, 95
'!751 chrooiunr Barch:96'i9213/,311024.3 us/t N.D. 0 (1) 78 79
1753 cupper Eatclr: 9619218/r83C21.8 ug./t N.l. 0 (1) -201 '191
1754 lron Batch: 9619218483025.9 ug/t a.A5!7 J ng/t ',74 -1513 -1411 (2)
1759 Lead Srtch: 96i921t r:ti;1C2
18. ug/t ll.0. 0 (1) 92 93
17!3 I'ianganese B3tch: 95'19218/131322.9 ug/t N.l. 0 (i) 59 6^'
1791 lickel. Batch:95'192'18q8 1025.4 ug/t N.!'. 0 (1) 9t' 95
1765 si iver Batclr: 95192181:11102i.6 ug/t N.D. (1) 99 1C1
(!) The result for one or both deteflrinations las less than five times tne'-O0.
(2) rhe background resuLt las more than four times ti)e spike aCcled.
il
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B0 1?.0
80 120
8C 1?0
80 120
80 120
B0 120
BC 1?0
80 120
8C 120
80 120
80 120
80 120
B0 120
?4
36
43
a
?6
0
0
2
1
0
I
1 102
1/ 1nO
1 i07
'l 100
098
197
? 107
9 101
31 11l
't 1c2
3 103
't I04
1 100
MEMBER
7a<fn ,1lvg5See reverse side for explanatron of symbols and abbrevaations 2215 Rev. l0/10/95
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Q!_"\LrTY CCNTROL REPORT(I)Lancaster Laboratories 149of
A Thermo Analytical Laboratory
LT,f Sainpl-e No. 2538C01
CLr-1 JUo i'tatrix Spike oupIicare Grab Uater Sarrcle
Hercutes: Bacchus PonC
Grouo !io. 522727
rercuLes, lnco.aorated
Sampte Samplei'IDL UI,IITS
1772 Zinci2. us/t
7035 Arsenic TR2.7 us/ t
7034 setenium TR?.7 uS/ t
C2',9 Fercuryu.43 ug/ t
SLATiK
Batch:9619218(3102
N.r-
Batch: 96192'1848302
N.0.
Batch:951921848102
N,9.
aatch: q61985711-101
N.9.
Eatch: 96133C0C5.1
il.D.
N.9.
r,i-1.
N.D.
h'.i.
t(.?.
!i.1.
N.D.
N.9.
!t.9.
t,l.!.
!i -0.
N-:r.
N.D.
!.0.
N.l.
l.?.
LanCaSter LabOratOnes
2425 New Holland Prke
PO Box 12425
Lancaste( PA 17 605- 2425
711-656-2300 Fax [phone]E1
DUPRP9 lns
lils
MSD RPD
LgS LCS
LCS DUP RPD
LCS LIi!ITSLou l.l(G!{
B0 120
30 120
80 120
80 '120
0 (1 ) 't't -i4
0 (1) 1C1 1A?
0 (1) 131 102
c 1'l) 79 79
5
'1
1
C
103
1D3
103
108
0917 lcL Pesticides in Uaters
'1500 AlFha sl1C
0 -CCz ug/ t'!601 Bet-i Bllc
0. Lr03 rr9/ !
iA0l DeI ra gilc
0. C05 u9/ L
io02 6anna BHC - Lindane
0.0C2 ue/ L
1tJ!, HeDtach r-or
0. lai us/ t
lar:1 A L3r in
0. !C1, u9/ [
'14-'")5 fier;rachIor Epoxide0.OCi u,J/ |'iliS Encl:suL fa;r !
0 . CUI Li!/ L'1:,:il Diel.liin
0. CG' u9/ |
.i tr.l DDE
0
1
0
C
,]
la
0
?
0
3
1
1
0
j
2
!
2
C
96 e5
97 97
s5 85
7;r 76
7t 70
83 8i
a'Lt L\
113 1';t+
9! 9i
91 3e
ci? 93
94 )2
llia 1!2
t: cl
?b ?,1'
9C
101
100
s2
1)
69
9?
BB
90
32
1 ",2
95
97
,3
9t,
101
91,
u6
67
71.
o9
66
12
64
.60
66
60
'67
67
53
71
76
57
75
75
122
120
1?6
12C
124
1?A
.,zo
lZC
'120
129
i?D
121
1r11
120
140
1?C
120
0. iJa5 u9/ |
Er:.ii i n
0. 005 u9/ t
EndosuI fan I I
0 .01 u9,/ [
0 9c,
0.0C-,' ug/ [
Endcs.rt fan Sul fate
0 - CCjT ug/ t
DIT
0. c'-,3 q/',
En.r|in Kctc:re
o ''Jol u'-r'r L
Iti L. I h oxyc h L ,r ILr.Cl ur/ t
A i.1'1.: Clr' ,:r'-l^n"
,.-r.0i I u!./ ].
G:rrv,ra Cir I orC:'.re
0 .'lrr5 u!./ i.
(i) l.l:c cesult for one or both cleternrirration$ vas Les:: lhan flv: tines t!re LO0-
MEMBEFl7Xm ,orror,, dt$See reverse srde for explanatlon of symbols and abbrevlatlons 2216 Rev
(iI)Lancaster Laboratories Page: 10 of 11
LCS LII'!ITSLot ir I cH
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LLI sampLe No. 2538001
cu-1 JUD uerrix SpiKe Dupiicare Grab tJarer SaD)te
Hercules: Bacchus Pond
Grouo No. 52?727
!iercu'.es, !ncorporated - DE
Saqnte SarilpleIIDL U[ T IS
1613 Toxaphene
'l ' ug/l'1618 Endrin AtCehyde0.010 us/ t
1619 PCB-10160.C9 u9/ t
1620 PC8-1221
0. 2 us/ t'1o?1 ?cB-173?0.li9 u9/ t
16?? PC8-12/'2
0 .05 uSl t
16?3 PCs-12430.07 us,, t
1a2\ PcB'1ZtL
0. 06 u9./ t
16?6 PC1-12600.07 ug,/t
ilsIIS9 RPO
OUPRPl HS
r ac I ac
I-CS DUP RPDSLAilK
u.D.
N.D.
ti.9.
N.D.
!J.0"
!{ -9.
[.D.
N.0.
N.D.
4678 TCt- SUB46 Semivotatites/!/aters Satch: 96'184uM026
3913 phenot?. us/t
33o7 bis (2-chtoroethyt ) etherZ. us/ t3t7!, 2-chtofophenot?- ug/L
3883 1,3-dichtorobenzene?. u9,/ t
3334 1,4'di ch IorobenzeneZ- ug/ l.
3932 1,2-dichtorobenzenc'2. ug/t
4680 2'rnethytphenol.L. us/ t
LLB1 2,2'oxybis ('1-chtoroProPane)t. us/t(63? 4-rlethytphenot/+. u9/[
3915 N-ni trosodi -n-propytamine
4. uS./t
3C{i? hex.achloroethane
l. . u9,/ t3?i0 ni trob,cnzencZ- u-q/t3r0\ i sophororre2. ug/ [
391 1 2-ni trophcrrolq. ug/ t
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23 134
1 172
20 124
32 1?9
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36 166
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Lancaster Laboratories
2425 New Holland Prke
PO Box 12425
Lancastet PA 17605-2425
717-656-2100 Fax [phone]
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22r6 Rev l0/30/95 Yllt
QUALITY CONTROL REFORT
See reverse side ior explanatron of symbols dnd abbrevrations
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(il)Lancaster Laboratories 1'1 of '.4
A Thermo Ana lytica I La bo ratory
LLI sample No. 2538001
Cri-'l JUo ilatrix Spike oupLicare Greb Uater Sarnote
Hercutes: Bacchus Pond
Grouo No. 521727
l!ercutes, ln,:c.porated - DE
lUP lISaP9 FS :,rS3 aFo
LCS
LCS Aliir
LCS LIMITS
LOU
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3890
3856
3886
3921
3906
3871
3900
3372
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390 1
3923
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3571
3r07
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3358
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2,4 -d i ch Ioropheno I4. us/ t
'1, 2, 4 - tr i ch Lorobenzene?.. uglt
naoh tha t eneZ. ug/t
4-chtocoanitine4. uE/|.
hexachtorobutadiene?' ug/t
4 - ch I oro -J -uethyI pheno tt,. us/l
2 - rret hy I naph tha L ene2. ug/t
hexach I orocyc t opentadi ene5' ug/t
2, 4, 6- tr i ch t orophenol2. u9/ t
2,4, 5- tri ch lorcohenol.2. ug/t
2-chtoronaphthalene2' uslt
2-nitroaniIine2. ug/t
dinrelhyt phthaLate6' u'/t
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l?i.)g 3-ni:roanitine?' u9/ L35i7 acenaph thene2. u9/ tlS?f 2,t,-dini trophenoI10. ug/t3912 4-nitrophen,rl
10 . ug,/ t
3379 di benzofuran2. ug/L
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2425 New Holland Prke
PO Box 12425
Lancaster. PA 17 605-2425
117-656-2300 Fax 717'656 2681 2216 Rev.,Orr.r* d?
QUALITY CONTROL REPORT
5ee re,rerse srde for explanatron of symbols and abbre'/rairons
(il)Lancaster hboratories Page: 12 o( itt
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LLi sampl-e No. 2538001
CU-l ..luD Ma(rix spi(e Dupticate crab Uater Sampte
lrercutes: Bacchus Pond
Sroup No. 52?727
,iercutes, Incorporated - DE
Sampte SampteIIDL UIiiTS
3337 diethyt phthatater+. ug/t
3875 4-chLorophenyt phenyt ether1.. uS/t
189D ftuorene2. uglt
=?Aq 4'nitroani Iine!,- us/l
46ti3 4,6-di ni tro-2-nrethylpherrot'!0. u9./ t
3]1t l,l-ni trosodiphenytanrine
4 - u.i,/ L
1869 4-brortrophenyt phenyt erhert,. uc/ Lf999 hexachtorobenzene2. ug/t
39t16 pentachtorophenol?. u9/ L
3917 plrenanthrene?' ugll
3859 anthraceneZ- us,/ t
1,:84 ca;'ba:ote2. u9/ [l8;lil di-n-but)/[ phthalate7. u9/ tlJ97 f I uorantnane?. uglt.j;,i9 Dyre:re?' ug/tiitlC buiyt berrzyr, Phtha ltrte4. ug./Llr..:5 3,f ' -dichto|obenzidine4. uSl tf.!:,0 benzo (a) arrthracene2. us/ tli,-:l b'is (2-etlrythexy[ ) plrrhatate1. u9/ t
3!7,1 chr,.'sene2. us/t:i.li).i di'n-octyt phthatate
4 ' ug/'tJijt'l bcnzo (b) fluoranther',e1. ug/ |
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2425 New Holland Pike
PO Box 12425
Lancaster. PA 17 605-2425
717-656-2300 ta\. 7 17-656-2681
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91 91
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QTJALITY CONTROL REPORT
4-
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A Thermo Analytical Laboratory
LLI sample No. 2533001
CU-1 JUD Matrix Spire oupLicate Gcab Hate,- Safl,D!.e
HercuIes: Bacchus Pond
Q'JAIITY CONTROL REPORT
LCS LIY!TS
LOU NIGA
(I)La ncaste r Labo ratories 1.4
Group No. 512727
rlerc-rl-es, lnacrporated - DE
SarnpIe 9amp'.eHDL UiI I TS
3881 dibenz (a,h) anthracene4' u,/t'
3861 benzo (9hi) oerTtenc4. u0/ t
8LA IK
li.D.
Lancaster Laboratofles
2425 New Holland Pike
PO Box 12425
Lancaster. PA 17 605-2425
71 7-656-2300 Fax. 7 t7 -6i6 )681
DUP MSP.P) HS IIS9 RPO
LCS LCS
LCS DUP RPO
7t,
94
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2
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1 ?19
MEMBERECM ,orrorn, d*B5ee reverse srde for explanatron of symbols and abbrevralons 22 16 Rev
(iI)Lancaster Laboratories
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A Thermo Analytical Laboratory
LLI sample No. 2538001
cU-1 JUD Matrix spike Dupticate 6rab Uater Samote
HercuIes: Bacchus Pond
0937 IcL Pesticides in tJaters
159? lcL VolatiLes by 8240 - Uater
1lt78 lCL I'J846 sefiiivoIati Ies/'Uaters
4679 IcL 9U845 SenrivoIati Ies,/Uaters
Lan(aster Laborator€l
2425 New Holland Pike
PO 8ox 12425
Lancaster PA 17 605-2425
1 11 -656-2300 Fax [phone]
i
Grouo No.
i ttercut es,
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522727
!nco,'porated - DE
RECOVERY:{
od
101
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QUALITY CONTROL RFPORT
srdeiorerplanatronofsymbolsandabbrevtatrons 2216 Rev 10/10/95
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Lancaster LaboratoriesA Thermo Analytical Laboratory Page: 1 of 14
LLr sample No. ES 2538088Cottected: 6/?6/96 ar '16:30 by BR
Suboitted: 6/?E/96 Reported: gl 6/96Discard: 9/ 6/96
CU-2 JUO (15-18',) 6rab Soit Sampt.e
Hercutes: Bacchus pond
1J015 S0G#: tlBP0Z-09
CATIIO. ANALYSIS IIAITIE
1593 TCL Votatites by 82401625 ThaL t iun1643 AtLrninun1644 Anti,oony1616 Barim1iA7 Beryt I iuun1619 Cadmim1651 Chromium1653 Copper1654 I ron1655 Lead1658 Manganese
166:1 NickeI1666 Si tver
tott Ltnc6935 Arsenic TR6936 Seteniurn IR0159 I'lercury1??5 TCL Pesticides in Sotids4688 TCL SU846 SemivotariLes Soit4689 TCL sr.J846 Semivotari Les/Soii.0.111 l,loisturerrl.loisture,, represents the Ioss103 - 105 degrees Cetsius.
1 CoPY I0 HercuIes, Incorporated
1 CoPY T0 ERH - Rocky ttountain
AS RECEIVED
:li:lii:lij+r:::j:;rr:::i:,:r:i:,1i:::::::.::r:.:i Ii(ETHOD
i:ii:ii:i:ii:ri,tSSUr.f s ..,.,',' DETECT I0N L lH I T Ull I TS
ORY UEIGHT
::::;: l::i:jiii;::l:il:,ij::.::::::i::':i:::r:i:i: i::.::::::: l{ETll00
::::.::j..::: .:::.::,:::::fttsutTS,:'.':t,,,i DETECT I Otl L I I't I T
t6.
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0. 087
0. 15
0. 55
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0. z1
0.034
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I Hercutes, Incorporated - DE
I Envi ronnentaI Af fairs
I ur tminsron oE 19894
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Ret.
3I
5
RespectfuI ty Subrni tred
Ramona V. Layman, Group Leader
ICP MetaLs/Leachates
14.
d.5
2.2
See Page
m9/k9
m9/ks
ng/ <g
m9/ k90.!73 m9/k9
0. l3 ms/kg0-46 m9/k90.49 mg/ks
ng/'<9
m9/ks0.12 ms/kg0.45 m9/kg0.4!+ II9/k90.39 ng/<g0.25 m9/kg
0. i8 mg,zkg0.028 ns/kg
See Page
See Page
See PaSe0.06 L by ut.rn Height of the sample after oven dr-yin9 at
ATTN: Hr. Joseph KeI Ler
AITtI : l'1r. Erent Robinson
3.3
2.4
Questions? Contact youc Ctient Services Repr.esentativeRachel L. (reaflEc at (7,.7) 656-23C0'I 5 : 56: 29 D 0002 23 REP 1261.16 5ZZT'593'10 25.00 00138400 AsR000
Lancaster Laboratories
2425 New Holland Prke
PO 8ox 12425
Lancasie( PA 1i 6A5-2125
7l7-656-2i00 t at i i7 -5tb. i6e t
MEMBEFl
5ee ie'.,er;e : ci -:,.:?3iaa;i:C. Ci SymDctS d|C Abbrevrahons 2)'t6, 9.e't iOi)ii9\
(I)La ncaster Laborato ries 2ot 14
P.0.
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DRY UE I 6HT
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LLI sample No. ES 2538088Cotlected: 6/26/96 at 16:30 by BR
Subflitted: 6/28/96 Reported: 8/ 6/96Discard: 9/ 6/96
CU-2 JUD (15-18') 6rab SoiI sample
Hercutes: Bacchus Pond
1 JD15 SDG#: HBP02-09
CATNO. A}IALYSIS I,IAME
ICL Votatil.es by 8240
3t34 Chtorornethane3435 Sromomethane3436 VinyI Chl.ocide3437 Ch t oroethane
34t D l'1ethyI ene Ch t or ide407L Acerone4076 Carbon Disutfide1'180 1,1-Dichtoroethene3442 I , l'0ichtoroethane34iL Chtocoform3145 1,2-Dichtoroethane4085 2-Butanone3446 1,1, ! -TrichLoroethane
3447 Carbon TetrachIoriCe4091 VinyI Acetare3448 BromodichIoromethane3150 1,2-Dichloropropane3151 cis-1,3-Dichl,oropcopene1181 Irichtoroethene3452 0ibrontochtoromethane3455 1,1,2'Trichtoroethane
1 182 Benzene3451 trans-1,5-0ichtoropropene3456 Bromoform4108 4-Methyt-2-pentanone
t 107 2-Hexanone3157 Tetrach I oeoethene
34t+9 1,1,2.2-TetrachIoroethane
1 lBl Totuene
'I 184 Ch (orobenzene
3458 Ethytbenzene4117 Styrene3355 Xytene (totat)
6187 trans-1,2-Dichtoroethene6277 cis- 1,2 -0i ch loroethene
A Thermo Analytical Laboratary
AS RECEIVED
r:::.:::.:::j:::::.:;:r.::1-::::::l:::.:-:::.:j:.:.1:1:i:r.:.:r: llET HOD
,.ii:iiiiit',.:.' ts,ltft.qiir,i DETEcT ! oN L I r,r I T uN I Ts
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7 - uglks3. uglkg?' ug/kg1. ug/kg1. u9l(9?. uglks7. u9/i9'r. u9lk91. ug/kS3. u9/k9?' uglxq3- uz/kg
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RacheL L. Krearner
your CIient Services Representative
at [phone]
MEMBEFl
ffig'lq
Lancaster Laboratories
2425 New Holland Prke
PC Box 12a25
Lancasle.. PA I 7505-2.1:S
717-655-2i00 Fax 7li-6i5-2661
RespectfuI ty Submi tted
I,ricnete ucclarin, B.A.
Group r-eader, GCll'15 VoLatiLes
jee:everse:rce iC, :tolanat on oi S/mo,tr a.d Jbor?ytatton., 22j6
Account llo: 06716
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(iI)La ncaste r Lab o ratoriesA Thermo Analytical Laboratory
LLI sample No. ES 2538088Cottected: 6/26/96 at 16:30 by BR
I
I Account No: 06716
I Hercutes, !ncorpoaated - DE
i Envi roflnentaI Af fairs
I lJi Lmingron DE 19894
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Page: 3 of 11
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ReL.Suhnitted: 6/?8/96 Repocted: gl 6/96Discard: 9/ 6/96
CU-? JUD (15-18,') Grab Soit Sampte
llercules: Eacchus Pond
1J015 SDG#: tlBPO2-09
CATIIO. AIIALYSIS IIAIIE
TCL Pesticides in Solids
1981 Atpha 8HC198? Eeta Bfic1983 0el.ta gHC
1?1A Gama BtlC - Lindane1219 Heprachtor1220 Atdrin1984 tleptachIor Epoxide1989 Endosu[fan I1?Z? DieLdrin1985 ooE
I ZZ.5 tndr I n1990 Endosut fan I I1985 DDo1991 EndosutfanSutfare12?1 oDT3017 Endrin Ketone1859 I'tethoxychtor'3025 ALpha Chtordane30?6 Garnm Chtordane1988 Toxaphene1992 Endrin Atdehyde1995 PC8-10161991 PCB-12211995 PcB-12321996 ?cB-1?121997 PC8-12481998 PC8.',]2541999 PCS-1260
AS RECEIVED DRY UEIGHT
ii:.::::t i:::j:'i:,:i:iti::i:,:::,:t;:::::,,::, .::'rt:::;,. :::.::. ilE T H00
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ug/k9
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ug/\g
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ouestrons? Contact your CIiant Services Repcesenrative
Rachel. L. Kreamer a. (7.7 ) 656-2f01)
MEMBER
7reilE
Lanca5ler Laboratofles
2425 New Holldnd Prke
PO 8ox 12425
Ldncaster PA 17 605-2425
717-656-2100 t.rx 7l7.ii56.2aB l
tB
,o. ,arrnrnt ?a*
Respectfut Ly Submi tted
Jeni fer E. Hess, B. S.
croup Leader pest i c ides/pcgs
See reverse slde ior ejolana(ron oi symbols and abbre,rratrons 2216
La ncaster Labo rato riesA Thermo Analytical Laboratory
LLI sample No. ES 2538088Cottected: 6/26/96 at 16:30 by BR
subnitted: 6/29/96 Reported: gl 6/960iscard: 9/ 6/96
C!l-2 JUO (15-18") Grab SoiL sampLe
Hercutes: Bacchus Pond
1J015 S0c#: HBP02-09
CATiIO. AHALYSIS }IAI'IE
TCL SU8/+6 SemivotatiLes Soit
1185 phenol
3753 bis (2-chIocoerhy[) ether1185 2-chl.orophenot4751 1.3-dichto.obenzene1187 1,4-dichtorobenzene3755 1,2-dichtonobenzene4690 2-me[hyiphenot4691 2,2'-oxybis (1-chloropropane)4692 4-methylphenol.1188 N-nitrosodi-n-propytamine3757 hexach Ioroethane3758 ni trobenzene3759 isophorone3716 2-ni trophenot3747 2,4-dirnethytphenoI3760 bis (2-chtorcerhoxy) methane3718 2,4-dichtorophenoL1189 1,2,4-trichl.orobenzene3761 naphthatene1.693 4:chloroani t ine3762 hexachIorobutadiene'119C 4-chLoro-3-rn€thytphenot1694 2-methyl.naphthaIene3763 hexachtorocyclopentadiene3749 2,4,6-trichtocophenol4695 ?,4,5-trichiocophenot3764 2-chtoronaphthatene4696 2'ni troani t i ne3766 dimethyI phthaIate3765 acenaphthytene
ouestions? Contact your
RacheI L. Kreamer
j A."otrnt tlo: 06716j Hercul.es, Incorporated
I Envi rorrnentaL Af fai rs
i UiLminston DE 19894
4 of 1/,
DRY IJEI GHT
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80.
80.
40.
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80.
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AS RECEIVED
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C I i ent Servi ces Repcesenta r i ve
at (7i7) 656-2300
u9/k9
u9l kg,
u9lk9
u9lk9
u9/k9
u9/ <9
ug/k9
ugl (9
u9lkg
u9/ kg
trglks
ug/ <9
uslk9
us/k9
us/kg
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us/kg
ug/k9
ugl <9
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u9/kg
uglkqug/kg
tg/ <9
u9/'<g
u9/ K9
u9/ k9
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Lancaster Laboratories
2425 New Holland Prke
PO 8ox 12J25
Lancasier PA I 7605-1J25
717-655-2i00 Fax r-17-65o-258i
Respecrful Ly Submi tted
Chr-istine i{. R:tct if f , I
6roup Leadq.r, GClHs
5ee 'ever;e s;ce icr erplaratron oi svmbcrs and abbreyratrons
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2216 Rev
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LLI sample No. ES 2538083Coltected: 6/26/96 at 15:30 by BR
suhnitted: 6/28/96 Reporred: 8/ 6/96Oiscard: 9t 6/96
I Account tlo: 06716
I xercutes, Incorporated - DE
I Envi rormenrat Af fai rs
I Ui [ringron DE 19894
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DRY UE I GHT
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AS RECEIVED
iliii:i:li::::::::::i::::::i::::i::::::::,: :,::;:r HETHoo
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RacheI L. Kreamer
your CI ient Services Representativear (7'7) 65o.2500
Respec!fut Ly Slbmi ttedChrisrine tt. tiarct'i ii, B.S.
6coup :eade!-, cClMSLancaster Ldboratories
2425 New Holland Prke
PO Bor 12425
Lan(asrer PA I7605-?J:5
il7-655-2300 F,\x ,11:-a-a )6Al
,B
l2l5 Fer lC/ro,95 lf;
hncaster LaboratoriesA Thermo Analytical Laboratory
CU-2 JUD (15-18'.) Grab Soit Sampte
Hercutes: Bacchus pond
1 JD15 SDG#: H8p02-09
CATHO. ANALYSIS }IAI4E
TCL SU8/+6 semivotari Les/Soi L
4697 3-ni troani I ine
1 191 acenaphthene3750 2,4-dinitrophenot1192 4-ni trophenol.4698 dibenzofuran1193 2,4-dinitrotoLuene4699 2,6-dinirrorotuene3770 diethyt phrhal.are3769 4-chtorophenyI phenyI ether3768 fluorene1700 4-nitroanitine4701 4,6-dini tro-2-methyIphenot.3772 [-ni rrosodiphenyl.arnine3773 4-bromophenyL phenyt ether3771. hexach I orobenzene1191. pentach I or-ophenoI3775 phenanthrene3776 anrhracene4702 carbazole3777 di -n-butyt phrhal.ate3778 ftuor-anthene
1 195 pyrene3780 butyt benzyt phthatate3783 3,3' -dichl.orobenzidine
3781 benzo (a) anthracene3784 bis (2-ethythexyt) phthatate378? chcysene3785 di -n-octyI phthatate3786 benzo (b) fl.uoranthene3787 benzo (k) ftuoranthene3788 benzo (a) pyrene3789 indeno (,],2,3.cd) pyrene3790 dibenz (a,h) anrhracene3791 benzo (9hi) peryl.ene
usl k9
us/kg
u9/ k9
u9/k9
Ug/ICJ
u9l (s
us/k9
ugl k9
us/ kg,tg/\g
u9/ <g
u9/ kg
u9/'<g
u9/'<9
!,j/ K9
ue/'rg
ug/'<g
19/19
ugl k9
rr9l kg
uslkg
uglk9
ug/'<9
u9/'<9
ug/ k9
ugl <9
u9/'<g
ugl <9
u9/ <9
u9/'<g
u9/ks
uslkg
u9/ ks
u9/ t9
MEMBEFl
.co re\,,erse i,de tat 2,.c!;tt Z:_,)- )- ', tf;.i1i\ .jatl aitCrey ation,
&&&
LLI sample No. ES 2538088
Suuni tted: 06/?8/96
CU-2 JUO (15-18,,) Grab Soit Sanrpte
I Account tlo: 06716
i Hercutes, lncorporated - DEI Envi ronrnentaI Affai rs
I,ABORATORY CHRONTCLE
Page: 5 of 1t,
AIIAI-YST
Rick S. Rodgers
Jotene M. SchieLds
JoIene t!. SchietCs
Jolene fl. Schietcs
Jotene M. SchieLcis
JoLene fl. Schie!.dsJotene ltl. Schields
Jotene !1. SchieIds
Jotene !t. SchietCs
JoIene !!. ScI i etds
JoLEne I'1. SchielcsJotene !t. Schiel.CsJol.ene t!|. SchieIcs
Jotpne I- SchieLcs
JoLene I'1. SchieIcisDesi R. Carozza
.iolene i!. ScnietCsNina C. Halier
lleL l. i S. HarkaryanIrances A. Demot"est
MattheH U. Kofroth
Michel.e 0. Uack
Sherry Lynn Devtin
Joseph I'1. GambLer
Joseph I'1. Gambter
Neelay 8. Hehca
(I)hfl 1ffi,r,#3,?,o,r,Blgli.t Il
lt
I ui tminston DE 19894 it
]lHercules: Bacchus pond
1J015 SDG#: HBp02-09
CATi{O AiIALYSIS IIAIIE
t+593 TCL Votari tes by 8240
16?5 That t iun
1543 Aturninurn
'! 644 Ant inony
'! 646 Bar i unr1647 Beryttiurn1649 Cadnriun
165 I Chromi um
1 653 Coppe.1651 I ron
1 655 LeadI658 lt{anganese
1661 ilicket
1666 Si Iver
tot I I tnc5708 su SU84o lcp Digesr6915 Arsenic TR6936 Sel.enim TR
01 59 Mercury5711 sU SUB46 Hg Digest
08'19 Sotid Sampte pesticide Extract1?25 TcL Pesricides in sot ids
0381 BNA Soi I Exrraction45BB lCL SU8/+6 Semivotatites Soit4689 TCL SU846 Semivotatr Les,zSoi L
0111 I'toisture
METHOO
su-846 82408
su-846 6010A
su-846 6C10A
su-846 6010A
su-816 6C,r0A
su-846 6C10A
su-846 6J10A
srJ-346 6C10Asu-3/i6 6010A
su-846 6010A
su-346 601CA
SU-8/+6 60'l0A
su-846 60icA
su-846 6110A
su-845 6C10A
su-346 f050A
su-846 60i0A
su-846 6010A
Su-Btt6 7471A
SU-846 717iA !'!odif ied
su-846 3550A
su-846 8981
su-346 3550A
su-846 82708
su-846 82708
EPA 160.3 (modiried)
ATIALYSI STRIAL OATE A}IO TIME
1 07/03/96 0859
1 07/13/e6 1813i 07/13/96 18i3i 07/13/96 18131. 07/13/96 18131 07/1i/96 1Bi3't 07 /1.3/96 131.31 07/^,3/9b 1Bi3'. 07/13/96 13i31 07/i3/96 1,3.,31 C7/1,1/9o i813't 07/13/95 181.31 07/1i/96 13':11 a7/13/96 18"31 07/i3/96-13..31 07/0?/95 i9311 07/13/95 18131 C7/17/96 0927
1 07/03/96 16361 07/02/96 15n6
1 07/01/96 14CO1 07/18/96 0757
1 07t01/96 1c3a1 07/05/96 16,t41 07/05/96 16t 4
1 07/0?/96 1520
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MEMBEFlrffiiE
Lan(aster Labord{o.ies
2425 Ne'e Holtand Prke
PO Bor 12a25
LJrcaster, PA I7605-2425
717-556-2100 Fax: 717-E5d-i5Sl
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Lancaster Laboratories
A Thermg Analytica I Laboratory
QUALITY CONTROL REPORT
Page: 7 of 1/,
LLI sample No. 2538088CU'2 JUD (15-18,,) Grab Soit Sanpte
Hercutes: Bacchus Pond
Group l,lo. 522139Hercutes, lncorporated - DE
I
Samp t e
HDL
SampI e
UNITS LCS LCSLCS DUP RPD
DUP MsRPD HS MSD RPD
LCS LII{ITS
LOU H I6iI
4593 rcL votarites by 8240
BLA NK
Eatch: E96'183.1A8
N.D.
N.D .
N.D.
N-0.
2. J ug,/kg
N.D.
N.D.
N-0.
N.D.
il.D.
N.D.
N.D.
N.D.
N.D.
[.0.
N.D.
N.0.
N.0.
N.9.
N.D.
N.D.
N.0.
3434 Chtoromethane7. ug/kg
3435 Broflomethane
1 - us/ks3136 vinyt Chtor-ide?. ug,/kg
3437 Chtoroethane3. uglkg
3t t O Methytene ChLoride2. uglkg4074 Acetone7. uglkg
4076 Carbon DisuLfide3. ug/kg1180 1, 1-0ichtoroethene2. ug/kg341? 1, 1 -Dichtoroe!hane
1. ug/ks
3/+14 ChLoroform
1 - us/kg3145 1,2-DichtoroethaneZ. us,/ k94085 2-Butanone7. us/kg3446 1,1,1-TrichLoroethane1. ug/kg3447 Carbon letrachIoride1. ug/kg1091 Vinyt Acetare3. uglkg
31/+8 Bromodi ch Loromethane2- ug/kg
3450'1,2-Dichtocopropane3. uglks3154 cis-1,3-Drchtoropropene1. ug/kg1181 Trichtoroethene1. uglkg345? D ibcomoch Ioromethane1. uglks
3/+53'1,'l, 2-TnichLoroerhane2. ug/ks
1 1 82 Benzene1. u9lk9
3/,51 trans-1,3-0 ichLoropr-opene
1 . u9,/ k9
90 37
99 98
104 1 0C
91 101
1C2 99
83 78
1C2 100
107 101
99 95
96 95
93 92
102 84
106 105
104 100
99 31
92 90
95 98
96 98
1 09 107
90 87
94 92
93 96
93 q?
395
255
5 102
1q 89
196
,r oo
2 103
,5 105
495
295
191
20 95
1 105
I 103
20 't 05
295
0 101
2 10?
2 lil
396
298
2 104
198
1 272
1 241
't0 251
1 )11
19 150
24 188
1 233
5e 155
51 138
49 155
2? 167
52 152
70 '!4 0
19 190
35 155
1 ?09
1 ?26
71 157
53 149
5? 150
37 151
17 aO?
Lancaster Laboratofles
2425 New Holland Prke
PO 8ox 12425
Lancasrer PA I 7605-2.125
717-556'2100 Fax 717-556 l13l
aBl.iRcv I0/:'0/95
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LLr sample No. 2538088cu-2 JUo (15-18") Gfab soit sampte
Hercutes: Eacchus Pond
QLTALITY CONTROL REPORT
Page: 3 of 14
LCS LIIIIITS
LOU HIGH
Group No. 522259llercutes, Incorporated
Lancaster Laborato(es
2425 New Holland Prke
PC 8ox j2325
LJncaster PA 17605-2415
7 l;-655-2 100 Fax. / 1 7'656-:53 r See re,rs15" t,6" lor
"xoianauon of symnois .;nd abirre,.,rarrons
DUP t'lsRPD I.1S I.ISO RPD
LCS LCS
LCS DUP RPD
1 . ug/kg tl.D. Bg Bj4108 4-Methyt -2-penranonel. us/kg N.D. 98 9i4107 2-Hexanone3. uslks N.D. 1 01 903457 Tetrach t oroethene1. u9lk9 N.D- .l 15 110
34t q 1, 1;2,2'Tetrachtoroethane1. uglkg N.9. 100 941.183 Tol uene1. us/ks H-0. 105 '103
'1 1 84 Ch Iorobenzene
'l . uslkg N.D. 96 963458 Ethytbenzene1. us/ks N.0. ,,07 104
41 17 Styrene
1 - uq/Y.s N.D. 99 923355 Xytene (tocat)
1 . us/ks N.9. 1 05 1 036187 trans- 1,2-DichloroerheneZ. u9/k9 tt-D. 1U 986277 cis-1,2-DichIoroerheneZ. u9lk9 N.D. 105 101
1625 Thal. t iurn Batch: 96184570e00314. mglks N.9. ( 1 ) 93 89.1643 Atuminum Batch: 9,518457080038.8 ms/ks N.D. 21 zc?i 1615 (?)
1644 Antimony Batch: 9618457080032.2 mg/ks N.D. (1) 92 951646 Barium Satch: 9619457080032.2 mg/ks N-0. 9 105 97
1547 Beryttim Batch: 9618457080030.0rJ mg/ks N.D. 0 (1) 96 91'1649 Cadmiurn Eatch: 9618457080030.13 mg/ks N,0. 0 (t) 93 88
1551 Chromiun Batch: 96'1845708!03'0.46 ms/ks N.D. 0 (t) 1ZB ljl
1653 copper Batch: 9618457080030.49 mg/kg N.D. 0 (1) -1
'19 109
1654 lron Batch: 9618457080013.3 m9/k9 7.2 J mglks 13 Zt52 21.39 (2)
1655 Lead Eatch: 96',1845708C012.4 ms/kg N.9. 0 ('1 ) 96 90
1658 l,,tanganese Batch: 961945708C0j0.12 mg/ks N.D. il 't 16 t09'1661 Nicket Batch:96',1845708!Cl0.45 ms/kg ti.9. 0 (1) 9T 911656 Si tver Batch: 9618457080030.44 mg/ks N.0. (1) 1AZ 97
(1) The resutt for one or both determinations cas tess than five times the LOO.(2) The background resutt ras more than four times the spike added.
45 169
50 124
52 140
64 148
46 157
47 150
37 160
37 162
t4 tjo
30 200
54 156
54 156
50 150
50 165
21 2e9
70 131
23 177
26 17t,
5t+ 111
57 115
61, 142
53 142
69 135
)) l.io
50 147
693
790
12 91
4 115
797
1 10'l
r97
3 108
2 105
6 101
4 102
696
979
279
7 100
598
799
1 '102
6 102
1Bq
791
594
696
798
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Sarple SanrpteI.(DL UNITS
3455 Bromoform
22 16 9e,r 14t30/95
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Lancaster Laboratories
A Thermo Analytical Laboratory
QUAiITY CONTROL REPORT
Page: 9 of 14
LLr sarnple No. 2538088
Cu-Z JUo (15-18,,) Grab Soit Sarpte
Hercules: Bacchus Pond
I
I
i Group llo. 522159
i Hercutes, Incorporated - DE
!
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L
Sarpte SanpteI1OL UH I TS
1672 Zinc0.39 mglks
6935 Arsenic TR0.25 m9/ks
6936 Setenitun TR0.18 m9/k9
0159 ltercury0.028 ms/ks
ELANK
Batch: 9618457080030.80 J mslkS
Batch:961845708!03
N.D.
Batch:961845708!03
N.D.
Barch: 9618457'1 1002
lt.D.
Batch:961830103A
N.0.
N.D .
N.C.
N -9.
N.9.
ll.3.
N .0.
N.0.
N.D.
[.D.
N.D.
N.r.
[.0.
N.D.
N.D.
N.t.
0(1) '108 98
0 (1) 9'r 92
0 (1) 92 91
0(1 ) 92 92
LCS LCSLCS DUP RPO
DUP itsRPo !{s Hso RPD
LCS LIMITS
LOU HIGH
54 149
49 149
5Z 149
26 157
65 127
50 137
07 120
T3 120
69 1?0
67 I,Z0
60 120
60 120
79 120
7? 120
68 126
62 120
7? 1?3
6? 120
ot lzt
7s 125
57 141
75 125
75 125
1225 TCL Pesticides in Sot ids
69?
093
187
079
ll
16
19
'1981 Atpha 8HC5. us/ks1982 Bera BHC3. uglkg
1981 Det ta 8Hc1. u9lk9
1218 Garma BHC - Lindane1. us/ks1219 Heptachtor1. uglkg1220 Atdrin1. uslkg
1984 lteptachtor Epoxide3. ug/kg1989 Endosul.fan I4. ug/kg12?? Dietdrin4. ug/ks
1985 DoE1. ug./kg1?23 Endrin6. ug/ks1990 Endosut fan I I9. ug/kg1986 DDOl. ug/kg1991 Endosut fan Sut fate
1 0. us/ kg1221 DDT
'l . us/kg5017 Endrin Ketone5. uglks1859 MerhoxychIor10. u9/k9
1325 Alpha Chtordanelt. ug/kg30?6 caflma Chlordane1. uslks
69
76
73
70
71
71
T7
79
87
82
o/
69
79
81
7=
85
89
B9
85
83
86
9?
ot
95
94
105
93
95
101
97
57
95
89
)n
19
19
io
16
1B
17
10
19
'15
18
tz
2C
19
l)
2C
76
82
85
76
70
78
85
81
89
83
98
B7
93
91
90
58
B1
B1
(1) rhe resutt for one or both dererminations Has tess than five times the Loo-
Lan(aster Laborato.res
2425 New Holland Prke
PO Box 12425
Ldn(Jsiel oA 17505.2-l::
7 17-556-2340 Fax I ii-o!'j 25-: l
t9?.f
MEMElER
jee'e'.e.ss ;cp'c, :,c'dadirol D: tt-.Jct> t^: iro,e/ral,cn;22 l6 Rev l0/10/95
La ncaster Laboratories
A Thermo Analytical Laboratory
QUALITY CONTROL REPORT
Page: 10 of
LCS LCSDUP RPD
.Il
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Sarpl.e Sanpt eIIOL UIIITS
1988 Toxaphene
1 , 000.uglks
LLr sample No. 2538088
CU-z JUO (15-18r1 Grab Soit. Sampte
llercuIes: Eacchus Pond
Group llo- 522739
Hercutes, Incorporated - DE
DUP
RPO
72 82
75 84
69 78
T1 79
7/. 78
72 77
69 80
62 70
3/+ 97
74 34
ac. aa
77 83
83 92
7{, 82
6 LANK
N.D .
lr.0 .
r.t. D .
N.D.
N.9.
N.0.
N.r.
!,1.0 .
N.D.
t4s
RPO
95159279
LCS LIMITS
LOU iI t GH
57 123
5 112
1? 158
23 134
1 172
z0 1?4
32 129
46 123
36 166
5 152
1 ?30
40 111
35 180
21 195
?9 182
1992 Endrin Atdehyde10. us/kg
1993 PCB-101630. uglks
1994 Pc8-122130. ug/kg1995 ?cB:1?3?50. -ug/kg1996 PCS-124?50. ug/ks
1997 PCB-121810. ug/kg
1998 PCB-1?5430. us/ ks1999 PCB-126030. us/ks
il
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4688 TCL SU846 Seflrivotatites Soit Batch:961giSLBoZ5
1185 phenol35. ug/kg3753 bis (2-chloroethyt) ether
67 - ug/kg
I 1 86 2-ch t orophenol.31. ug/kg
3754 1,3-dichtorobenzene31. us/kg1187 1,4-dichtorobenzene33. us/kg3755 1,2-dichIocobenzene33. ug/ks4690 2-nrethyl.phenot67. uslkg4691 2,2' -oxybi s ( 1 -ch Locopropanel100. u9lk9469? 4-methytptrenoI
100 .u9/ ks'l'l88 ll-ni trosodi -n-pcopyIamine
67 - ug/kg
3757 hexach t ocoerhane67. ug/kg3758 ni trobenzenell. ug/ks3759 isophorone
67 - ug/ks
3746 2-ni trophenot
Lrq/kg
I.0.
N.D.
N .9.
N.D.
N.9.
N.D.
N.D.
N.D.
N.9.
N.C.
N.C.
N.0.
N.D.
N.D.
t5
11
1)
5
5
6
15
11
1t,
13
'10
1C
9
76
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76
71
62
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76
MEMElEFlreis
Lancaster Laboratorre!
2425 New Holland Prke
PO Bor 12425
Lancaller. PA I 7505-.2.125
717-656-?ioo Far: 7 I l-556-:68 l
{tslni
67-
:ee rele.i: .'tre'or:\rrda6trol of symtors ;rc abore,rrar,cns 2 2 l5 Re,, i 0,'1O95
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Lancaster Laboratories
A Thermo Analytical Laboratory
QUALITY CONTROL REPORT
Page: 1 1 of
LLr sample No. 2538088
CU-2 JUO (15-1E',) Grab Soit Sampl.e
Hercutes: Bacchus Pond
Group !,1o. 522239
hercutes, Incorporated - DE
Sanpt e Sarnpl eMDL UII I TS
3747 ?,4-dinethytphenol67. us/kg
3760 bis (2-chtoroethoxy) methane13. uS/kS
3748 2,4- dichtorophenoI33. uS/kg1189 1,2,4-trichLorobenzene31. uglkg
3761 naphthatene53. u9/k9
1693 4-chtoroani t inei00. ug/kg
3762 hexachtocobutadiene
67 - uslkg
1190 4-chLoro-3-nrethytphenoL67. ug/ks4691 2-methytnaphthal.ene33. ug/ks
3763 hexachtorocyctopentadiene170. ug/kg
3749 2,1,6- trichtorophenoI67. ug/kg
4695 2,4,5-trichtorophenot67. ug/kg3761 2-chtoronaphthatene33. us,/kg4696 2-ni troani t ine57. uglks
3766 direthyt phthatate33. us/kg
3765 acenaphthytene13. us/kg
DUPRPO HS
LCS i.CS
LCS DUP RPO
MSI.!S9 RPD
LCS LI}IIlSLou fitcit
32 119
31 184
39 13s
44 11?
21 '13i
17 116
24 116
2Z 147
)a a17
1 100
37 141
39 151
50 'l 18
53 143
i 112
33 145
BLANK
u.D.
rJ.9 .
N.D.
N.0.
[.0.
N.9.
N.0.
[.9.
N.D.
H.D.
N.9.
N.0.
N.D.
N.D.
[.D.
r,l. D .
't7
11
IJ
6
5
5
I
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i0
11
10
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48 57
T3 81
71 81
77 82
73 77
14 15
B0 87
75 86
74 82
17 16
81 90
80 8e
79 35
72 78
79 87
75 81
41
75
77
75
43
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62
82
82
75
80
4589 TCL SU846 Senrivotat i Les,/soi t Batch: 96.!83S18026
4697 3-ni troani I i ne67. ug/kg119'l acenaphthene33. u9/ ks
3750 2,4-dini trophenot17O. us/kg
119? 4-ni trophenol.170. ug/ks1698 dibenzofuran13. us/kg
'l 191 2,1-dint trotoluene67. ug/ks1699 Z,t'- dini trototuene67. us/kq
10 56
973
863
675
876
790
10 85
36 40
71 78
59 65
n77
74 80
82 89
7 143
1,7 '145
1 191
1 132
2B 131
39 139
50 t58
MEMBER7reiir
Lancaster Laboralones
2425 New Holland Prke
PO Box 12425
Ldncastel PA I 7605-:l:1
717-656'2344 izx l1i'i:o 262:
tD}.;See 'ere'se :,ca 'c. :j(oldn;iroi oi ; rrggt5 666 abbre.;,;l ons ll I o ?e';
QLTALTTY CONTROL REPORT
Page: 12 oi
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i itercutes, :ncoroorated - DE
Sanpte SampteIiDL UII I TS
3T7O diethyt phthatate67. u9/k9
3769 4-chtoropheny( phenyI ether67. us,/kg
3768 ftuorene53. us/kg4700 4-ni troani I ine
r00.uglk9
4701 4,6-dini tro-2-methytphenot
170.u9/ k9
377? [-ni trosodiphenytanrine67. u9lk9
3773 4-bromophenyt phenyl ether'100. ug/ks
3771, hexachtorobenzene
100 -ug/kg
1 191 pentach IorophenoI
170 .u9/ kg
3775 phenanthrene33. us/V-g3776 anthracene33. uS/kS
47OZ carbazote33- ug/ks377 di -n-butyI phthatate33. us/ks
3778 ftuoranthene53. us/kg
1 195 pyrene
67 - uS/kg
3780 butyl benzyI phthatate67. ug/ks
3783- 3.3t -dichLorobenz idi ne130. uglkg
5781 benzo (a) anrhracene
33 . ug/ l,:g
378/. bis (2-ethythe.{yl.) phrhatate67. u9/k9
378?. chrysene33. ug/ks
3785 di -n-octyt phthaIare67. ug/kg
3786 benzo (b) ftuoranthene67. u9/k9
3787 benzo (k) {tuoeanthene130. us/kg
3788 benzo (a) pyrene67. u9/k9
3789 indeno (1,2,3-cd) pyrene67. uglkS
DUP
RPO
ils
RPO
10
10
7
L
9
1?
IJ
13
2
10
9
7
11
9
'10
1?
5
7
9
IJ
10
10
10
8
LCS
RPD
tcs
DUP
LCS LII'llTSLOU HIGH
', 114
25 158
59 121
38 122
'! 181
33 147
53 127
1 152
"t4 176
34 120
27 133
35 '133
1 118
26 137
52 115
1 152
1 262
JJ lr{)
8 158
17 168
tl 116
2t+ 159
11 163
17 163
1 171
MS I.ISD
79 33
79 S7
74 30
59 52
65 72
74 34
81 92
83 9t,
/4 t6
75 8l
7+ 81
7t+ 79
30 90
T3 80
83 92
86 97
55 58
77 8i
93 101
82 39
31 92
73 80
77 85
74 81
e2 89
LCS
83
B4
79
76
66
73
BO
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63
10
86
77
91
95
68
BO
103
101
BO
B6
7B
82
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Lancaster Laboratones
2425 New Holland Prke
PO Box 12.125
Lancastel PA 1 7505-2.125
717-656-2100 F.ir 117-655-1631
t'!)l.i
(I)La ncaste r Laborato ries
A Thermo Ana lytica I Laboratory
LLI sample No. 2538088
CU-2 JUD (15-16"1 Gcab SoiI Sarnpte
Hercutes: Bacchus Pond
8 LAIIK
[ .0.
N.9.
il.0.
N.D.
[.0.
N -0.
N.D.
N.D.
N.D.
N -3.
r.l. D .
N.D.
N.0.
N.D.
n.D-
N .9.
N.0.
ll.D.
N.0-
N.D.
N.D.
il.D-
N.9 .
N.D.
N.0.
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QUALITY CONTROL REPORT
LLI sample No. 2538088CU-2 JUO (15-18") Grab Soi t Sanpte
llercu(es: Bacchus pond Group No. 922739
Hercutes, lncorporated - 0E
BLANK
N.9.
[.0 .
Earch : 96184C31 6320C03A
l'1s
83
79
9
8
LCS LCSLCS DUP RPD
az
75
r00 100
LCS LII'IITS
LOU H I6H
1 ?27
1 219
100 101
MEMBERtrerm
LanCaster Laboratones
2425 New Holland P,l,.e
PO Box 12425
Ld.(asr:t FA'ai_<-:r-:l
711-a56-2)Aa :.^ -'' .
,t
nr,nro, laJ,
(I}heffiq*FfiLs?gr*eri,'
Sarple SampteI.IDL U[ I TS
3790 dibenz (a,h) anthracene67. ug/ks
3791 benzo (ghi) perytene67. uglkg
01 11 lloisrure0.05 % by lt.
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il(l}La ncaste r Laboratories
A Thermo Analytica I Laboratory
QUALITY CONTROL REPORT
Page: 1( of 11
SURROGATE L!UITSLOI] H I GH
50 12C50 120
70 121
117
74 i2",
Zt+ 1i325 i2',
LLI sample No. 253808E
C!-2 JUo (15-18") Grab Soit SampLe
Hercutes: Bacchus Pond
1225 TCL Pesticides in Sotids
4593 ICL Votatites by 8?40
4688 TcL su346 semivotatites Soit
4689 TCL St,845 Semivotati les/Soi L
Gcoup No. 522739
Hercutes, lncorporated ' 0E
SURROGATE StJI'IMAIIY
TRIAL ID SURROGATE
TCX
DC3
dt,-1,2-9CA
dB - toIuene
Br8
Phc'no['d6
2-ftphenoI
2,t*,6-f BP
Ni trobz'C5
2-Fbiphnyt
TphenyLdl4
23 12030 1'5
1B 137
RECOVERY Z
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95
88
91
93
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92
68
19 1?Z
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Lancaster Laboratores
2425 New Holland Prke
PO Box 12425
Lancasier. PA 17505-1.125
ltl-oio-L)at rdr / t/.4_a--:::
tt
,o,,rorn, ?aiSee .erea:e r,c3 lcr :toEnii: ra rrr :rrbols dic actaelrairons 2216 ie,.
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16?5
1643
1614
1646
1647
i649
165 1
1 651
1654
1655
1 658
t66 I
1666
1672
6955
6936
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4689
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0 .45
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See Page
m9/ k9
ms/k9
m9/k9
m9lk9
m9/k9
mg/ k9
n9/'<g
mglkg
ntg/ <g
m9/ks
m9lkg
mglks
m9/i(9
mg/k9
ms/k9
m9/ k9
tfrg/ R9
See Page
see Page
See Page
LLr sample No. ES 2538091Cottected: 6/26/96 ar 15:00 by BR
Suhoitted: 6/28/96 Reported: g/ 6/96oiscard: 9/ 6/96
CU-3 JUD Grab Soit Sampte
Hercutes: Eacchus Pond
SSJUD SDG#: HBP02- 12
I
I
Account l{o: 06716
Hercutes, Incorpotated - DE
Envi rorynental Affa i rs
Ui Imington 0E 19894
AS RECETVED
IiIE T HOO
0ETECTI0N LL,ltT UItIS
Pag e:
l
Respectfu[ [y Subnri tted
Ramona V. Layman, Group LeaCer
ICP MetaLs/Leachates
'I of 11
DRY UEIGHT
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4.3
0.'t5
0. 26
0.93
1.0
6.7
4.7
0.24
0.91
0. 89
0. 79
0. 49
0. 35
0. c56
[-a ncaste r Labo ratories
A Thermo Analyical Laboratory
P.0.
Ret.
CAT
l,lo.AIIALYSIS llAtlE
TCL Votatites by 8240
Thal. t im
Aluminurn
Ant i mony
Bac i un
BeryL t iurn
Cadmi urn
Ch romi urn
Copper
I ron
Lead
I'langanese
l,l i c'<e I
S i Iver
Zinc
Arseni c TR
Seteniunr TR
I'lercury
TCL Pesticides in Sol.ids
TcL sUB46 Semivotati Ies Soi L
TCL Su846 !e..Livotati tes/soiL
l''lo isture
3
4
50.05 % by ur.,l'loistucerr represents the toss in veight of the sarnpLe after oven drying at'103 105 desrees Cetsius.
1 COPY T0 Hercutes, lncorporated'l CoPY T0 ERl4 - Rocky Mounra in
AITN: Mr. Joseph KeI ler
ATTII: !1r. BIent Robinson
ouestions? Contact your Ctieni Services RepresentativeRachet L. Kreamer a.. (7"7\ 556-230016:34:40 D 0002 23 REp 126136 52ZTi9310 25.00 00138400 ASR000
MEMBER
7FE5I1E
Lancdster Ldborato.es
2425 Ne', Holland Prke
PO Bor 12J25
laocjrsi-o. Pa I /505-2Jl:
717-655-llco Fat 1ii.1,>i ii).1
ar.TT.'''i or;-..11.!i a{,
LLI Sample No. ES 2538091
Cottected: 6/26/96 at 15:00 by 8R Account tto: 06716
Heccutes, lncorporated ' DE
Envi rorvnentai Af fa i rs
Uitmington DE 19894
AS RECEIVEO
ME 1 HOO
iljiiri:1ii 8r,s.utls.,;r,i oETEcr I 0N L I r'! I T uN I Ts
Page:2ol 14
DRY UE I GIIT
.. :::::i::::i:i:j:::::: ::::::.::ir::.:. ::i...:::. ::: ItETH00
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Ret.Suhnitted: 6/28/96 Reported: 81 6/96Discard: 9/ 6/96
CU-3 JUO Grab Soi t Sampte
Hercules: Bacchus Pond
S3JU0 SOG#: HBP02-'12
CATr,10. AIIALYSIS tlAlilE
TCL Votatiles by 8240
3434 Chtoromethane3435 Brornomethane3136 Vinyt Chtoride3437 Chtoroethane3410 I'lethytene Chtoridel.O7lt Acetone4076 Carbon Disut fide1180 1,'l-0ichtoroethene
3412'1,1-0ichtoroethane3144 Chtoroform3445 ,],2-0ichIoroethane
/1085 2-Butanone3446 1,1,1-Trichtoroethane3417 Carbon Tetrachtoride4091 Vinyl Acetate3448 BromodichIoromerhane3450 1,2-0ichtoropeopane3454 cis'1,3-DichLoropropene1181 Trichtoroethene3452 0ibromochloromethane3453 1,1,2-TrichLoroethane
1 182 Senzene3451 trans-1,3-0ichtocopropene3456 Bromoform4'108 4-Hethyt-2-pentanone1107 2'Hexanone3457 Tetrachtoroethene
3449'1,'1,2,2-TetrachLoroethane
1 183 Totuene
'l 18/- Ch Iorobenzene3458 Erhytbenzene4117 9tyrene3355 xyLene (tota[ )6187 trans-1,2-DichIocoethene6277 cis-1,2-DichLoroethene
?.
T,
7
2.
7.
1
2.
1.
2.
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2.i.
us/kg
u9/kg
u9/ k-o
ug/'<9
ugl ks
u9/(g
ug/ k9
uglk9
ug/k9
u9/ ks
ugl kg
u9/k9
ugl kg
u9/kg
u9/k9
u9lks
ug/ kg
u _a/'<9ugl(g
u9/k9
ugl ks
ugl <g
u9/k9
ugl kg
u9/ kg
ug/'<g
u9l kg
u9/kg
u9/ <g
u9/ (9
ug/'<9
\Jg/'<g
ug/kg
u<J/ <cJ
'Jg/'<g
1
2.J 1.
3.
0uestions? Contact your Ctient
RacheI L. Kreamer
Servi ces Representat i ve
at (717) 656-23C0
Ldncaster Ldboratofle5
2425 New Holland Prke
PC Bor l2{25
Ldrr.aiie. F{ 17505-2d25
717-6;ii-1 100 Fa\ 717-a5o-2631
I
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Respectfut ly submi tted
MicheLe YcCLarin, B.A.
Croup :eader, GClHS VoIati Ies
See reg-o.ga r:: iCr eroianai,Or Oi :vrori:.r,'.i ra;,:'j,alroas 2!ia
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(I)Lancaste r Laboratories Page:3of 14A Thermo Ana lytical Laboratory
LLI sample No. ES 2538091Cottected: 6/?6/96 at 15:00 by BR
SuHritted: 6/2E/96 Reported: 8/ 6/960iscard: 9/ 6/96
CIJ-3 JUD Grab Soil. Sampte
lieccutes: Eacchus Pond
S3JUD SDG#: HBP02-12
I o.rorn. Io: 067']6
I Hercutes, Incocporated - DE
I EnvirormentaL Affai rs
I uiLmington DE 1989/+
AS RECEIVED
r,,tETHOo
DETECTIOX LIMIT UIIIISANALYSIS IIAI4E i.!:::::::.. .orctil lc
DRY UEIGHT
.:,;i,.i:iji:ii]..,:j::,.:i,:,,r,.,,;...',.::.:,,.,iii ItETHOD
.';';;...;';.;.;i;;j;.;,;.,$[StJUIS :i.'j,"" DETECT IOfl L I tl I T
TCL Pesticides in Sotids
1981 Atpha BHci98Z Beta BHC1983 DeLta BHC1218 Garma EtlC - Lindane1219 Heptachtor
12?O ALdrin1984 Heptachtor Epoxide1989 Endosutfan I12?? 0ietdrin'1985 0081223 Endrin1990 Endosul fan I I1986 D001991 EndosuI fan Sut fare
122 1 DoT1017 Endrin Ketone1859 Methoxychtor'3025 Al.pha Ch[ordane3026 Ganma Chiordane1988 Toxaphene199? Endrin ALdehyde'1993 PCB-10161994 PCB - 1 2? ',l
1995 PCB-1.?3?1996 PCB-12421997 PC8-I2481998 ?cB-12511999 PCB - ',t 260
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Questions? Contact your CIien: Services Representative
Rachet L. Kreamer at [phone]
Respectfu[ !.y Submi ttedJenifer E. i]ess, B.S.
Group Leadec Pesticides/PCBsLan(aster Laoor3tofies
M E M Ef E R 2425 Ne,, Horlancj Prke
PO 8or l2Jl5
Larr(a;iea P: I 15,15-:J25
7t ;,555_.r:it0 ;;( :l:-ara-:a.l I -)Ea ae'.,e'5e 1de io. e.t an,ritca ot jrmool5 d.rj aarc.eyrairons
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(l)La ncaste r Laborato ries
A Thermo Analytical Laboratory
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LLI sample No. ES 2538091cottectedr 6/26/96 at 15:00 by BR
Subtritted: 6/28tg6 Reported: 8/ 6/960iscard: 9/ 6/96
cU-3 JUo Grab soi t Sampte
Hercutes: Bacchus Pond
53JUD SDG#: HBP02-12
CATIIO. AIIALYSIS IIAI'IE
IcL SU846 Sanivotatites soit
1 185 phenoI3753 bis (2-chtoroethy[) ether
1 186 2-chtorophenot
375/.'1,3-dichIorobenzene1187 1,4-dichtorobenzene
3755'1,2-dichlorobenzene4690 2-methytphenot4o91 2,2'-oxybis (1'chtoropropane)
4692 4-methytphenot
1'188 N-ni trosodi -n-propytamine3757 hexach Ioroetnane3758 ni tcobenzene3759 isophorone3716 2-ni trophenot3747 2,4-dimethylphenot3760 bis (2-chIoroethoxy) methane3748 2,4-dichtorophenoI1189 1,2,4-trichLorobenzene3761 naphthatene4693 4-chtoroant Iine3762 hexach Iorobutadi ene1190 4-chtoro-3-methytphenot1694 2-methylnaphthatene3763 hexachtorocyctopentadjene3749 2,4,6'tnichLorophenot4695 2,4,5-tcichlorophenoI3764 2-chloronaphthatene4696 2-ni troani I ine3766 dimethyt phthatate3765 acenaphthytene
II Account No: 067'16
I Hercutes, Inco.porated - DEi Environmentai Af fairs
luitminoton DE 19894
I
I
P.0.
Ret.
AS RECEIVED
IlET HOD
jiiiir.::'fi:tgc!,!:I5'.iiil DETEcT I oir L IH I T ulr I Ts
ugl kg
ugl ks
r.tg/kg
ug/ kg
ug/ <g
u9/ks
u9/kg
ug/kg
ug/ <9
tJg/ kS
ugl k -c
ug/ K9
u9l k9
ug/ (9
ug/ (g
ugl (g
t)g/ <9
u9/ <g
u9/ K9
u9/ tg
u9/ <9
ug/ <g
uslks
u9/ <9
us/ (9
ug/ <')
ugl k9
rgl kg
ug/ tg
ug/'<9
ORY UEIGHT
:1;.iir.r,;,:,i,:ilii.i:iijrili:.::lrr:i:j:::i:: l'iETHoo
,;irrrr:::!:i:li;,.'..8.EfiJl:l:E iil:::,: 0ETECT I 0N L ! r.,l I T
66.
110.
66.
66.
66.
66.
130 .
200.
200.
IJU .
130.
66.
130 .
130.
1?n
66.
66.
66.
66,
zcl.
130.
130.
66.
3i0.
130 .
lJu.
66.
130 .
65.
66-
ouestions? Contact your ct ient
Rachet L. Krealner
Services Reoresentatlveat (717) 656-Z3Du
Lancaster Laboratofles
2425 New Holland Pike
PO Box 12425
Lrnca;le( P\ 17605-2-125
717-555-2100 Fex 7l i'656'2681 ,oirc,e-< {*9
Respectfu[ [y Submi ttr.dCrristine ltl. Ratc'.iff , B.S,
GrouD Leader, Gc/Ms
See aq..?.te jioe tcr:!oiar:;;..r. ^i .'_rla,i'allrl aagfi\rtiitLrn: 2-
MEMBER
I
I
I (I}Lancaster Laboratories
LLI Sample No.
Co( [ected: 6/?6/96 ar
sut)(nitted: 6/?8/96Discard: 9/ 6/96
CU-3 JUD Gcab Soi l. SampLe
Hercutes: Bacchus Pond
S3JUD SDG#: llBPO2-12
A Thermo Analytica I La bo ratory
ES 2538091
15:00 by BR
5of 14
ORY UEI6HT
:ii:;liii:t:il:,::::ii:i:+i!:jiiii.,::iir:,.:,! llETHoo
,iitiiiii,;.:.,r1gsu1'"IGii:iil DETEcT IoN L I ut T
Account No: 067'16
Hercutes, Inco.porated - DE
Envi ronmenral. Af fai rs
Uilmington DE 1989/+
8/ 6/96t
I
I
I
I
I
I
I
I
I
I
t
I
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I
AS RECEIVED
CAT[o.ANALYSIS IIAI'IE ,:irll]l]:,,,::ocel tr,ld
METHOD
DETECIION LIII{II UNI TS
TCL SUB46 Semivotati tes/Soi t
4697 3-ni troani t ine
'l 191 acenaphthene3750 2,4-dinitrophenoL1192 4-ni trophenoI4698 di benzofuran
1 193 2,4-di ni trorotuene4699 2,6-dinitrototuene3770 diethyL phthaIare3769 4-chtocophenyI phenyt ether3763 f Iuorene4700 4-ni troani I i ne1701 4,6-dini tro-2-methytphenol.377? N-ni trogodipheni-Lamine37Tj 4-bromophenyt pheny( erher3nq hexachtorobenzene1194 oentachtoropher,oI3775 phenanthrene
3776 anthracene470? carbazote3777 di -n-butyt phthatate3778 f Iuoranrhene
1 195 pyrene3780 butyl benzyt phthalate3783 3,3'-dichtorobenzidine3781 benzo (a) anrhracene3784 bis (2-erhyl.hexyL) phthatate378? chrysene3785 di -n-octyt phrhatare3786 benzo (b) ftuoranthene3787 benzo (k) ftuoranthene37U. benzo (a) pyrene3789 indeno (1,2,3-cd) pyrene3790 dibenz (a,h) anrhracene3791 benzo (ghi ) perytene
: r.ii::r:.!:..:::::ri:::::i:r:li;?r;t:i:i:i 130.
,i,:1.',,,,,:1,,],,,,.,it:::,:,ii:,v:tD,:,1'', 130.
ti,:ir.: .t:t::,,ii i'j,.,:t,r:,i:11;D-]',. ?60.
,;i', i.:.. ., 1 tCCqti,jti....,..i,,t, 130.:.:':': ..: :,, N.0..',.. 66.
,,.i ::,,: ,, r:,:.ii:.,.lj:.D;,::li 130,, ,:.,:: ,.:,:::,i:!i:D..:, 130.. :i: :. : :v..D. , 260.,,: ,. ::.'' :: t{.D:,:, 1j0.. i, ... lI.D.. 110., 1, ,,,.i,, ,.,,, . ,-",,1,;.9;,'::"1 130.
: ... :: ,.. . i{.0. .. , 130,
:]i.::::i:::ill ; O i
,.i.,,,, N.0,
i.::i::i:.:.Il: a .]
':.:j:r. N; r.
|]:.::::]N. [;:...tt-D.
,,,,,,l.J.r',,
,',.,,, 11 ., ,
.r . ,'.tr1 - c, :,
1'1'..1,1t{, I :
,,,,.,i,V.D:
.,'.,,.t;. I -,i.'t{.f,.
'u.!.
' , N;D:
', .. ...1i,, ua .':i,, .,U. r.
:,,,.[.9.
.,, '1,,,,'}J.9 '',',',"N.!,
,,i,. ,, $, D,
lzo-,,, ,'., ,.H.J.
':::i:.rM , i:;.
,.,. N,D.
,'.',,, 1.,1.!.'
.' ,,;N . 0..:: ::]llJ - }:
67.
170.
17C .
JJ-
67.
67.
o7.
b7.li.
'100.
170.
67.
1 frn
'r00.
'!7C .
f i -
3i.
iJ -
67.
67.
110.??
67.
Ji -
67.
67.
1i0.
07.
o7.
07-
07.
u9lk9
uq/k9
u9/<9
ugl (9
u9/ <9
u9l k9
u9/ <g
u9l <g
ugl k9
u9/(gtj!/'<9
u9,/k9
u9,/ kg
19/ <g
u9/k9
u9/kg
'r9/'19
u5l I(9
u9/ Kg
u9/ks
u9/ k9
ti9/k9
u9/ k9
ug/ <g
ug/ ks
19/ <g
us/ (9
r9l ks
u9/ k(J
u9/'<9
u9/ ks
u9l <9
,J.i,/kg
u9/ <g
,'r : i,1,,,,, ,}f . $,:
130.
66.
530.
330.
66.
130 .
130 .
'130.
1i0.
66.
200.
330..130.
2.:0.
200.
5JU.
66.
66.
66,
66.
66.
;]:,:"t:'::t'i:l ;.: :l::'i::t::.tlir'D.l':i:t.'
r: .::,::...:::: ::.::r: :.::::::::::::.lI jD ir:::i::i,:.rr,^. :
:,;;.;,;:,'..,;,',;,."1.".'..1P.q..:,..
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^:
,:
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.' i,,,'.:. ' ,,.i',: .' ]' i'.1 li ;'D;.',,,i
.i,i.'.,,,:.'l::,:,:i..t. ,l ,l i:.:.;,|l,i D:i: l:.:;.1..:_jlrrft,::r :
,ii]t :l:jl::.i. :::::i ,:.1{:;a; ti::':l
,.,,.;,..'. :.:,,:,.i,:,,.:, :i,ti:D:,::.:.,:,:
..'t'l.,:.,i,,it,,,.'',,i,:,'t,,.,i::'.1'I,D.,]',,:: 1 ,.' ,l! ts,,
' ... :..'u:6.1 1l
, :r::l,: :'.i:.i:.]:i::l i:l::r.ll ;Cr :.: :.
., . i.,'..l....',i.,,:;,,l',,,,. ,li . D : .i.i'
.. i i: t..i.: ',1,:, i.': ii: r:N -D ; :,:,:
ri::." :rr : :r: rr ::::ljr:!). : :.
0uestions? Contact your Client
RacheI L. Kreamer
Servi ces Rep|L.sentat ivear (7r7) 656-2j00
RespectfuI l-y Subffii t redChristine i'!" Ratci.iff , B.S.
Grouo Leader, CC,/HSLancaSter Laboratc0es
2.125 Ne,r Hoilano Prke
PO 0or 12-125
La.(isie,. PA 11 605 -)12.
1 1 :' -5 -<6-2300 ia, 7 17 -aiD'264 ){"*
&&&
I
i Account lto: 06716
i Hercutes, Inccrpocated - 0E
I Envi rormen:ai. lf ta i rs
iUiImington 0E i9B9/.
I
Paqe: 6 of 14
:i'6 Re' l'ill/-r5 dt;
ll
CU-3 JUD Grab soiI Sample
Hercules: Bacchus Pond
SSJUD SDG#: ttBPO2-12
CATIIO AIIALYSI S IIAIIE
4593 ICL Votatites by 8240
1625 That t iLrn
1643 Aluminum
1544 Antimony
1646 Barium
1647 Beryt t ium
1649 cadmiurn
165 'l ch romi um
1653 Copper'1654 I ron
1655 Lead
165E I'langanese1651 ll i cke t
1666 SiLver1.672 Z\nc5708 sU SU846 lcP Digest
6935 Arsenic TR6936 Sel.eniun TR
0159 l,tercucy
3711 su SU846 H9 oigest
0819 sotid Sampte Pesticide Extract
1?25 TcL Pesticides in Sotids
0381 BtlA Soi I Extract i on4688 TCL sU846 SemivoLati les Soi I
/+689 TCL SU846 SenrivoIati tes/Soi I
0111 lloisture
METHOO
SU-8/'5 821*08
su-846 6010A
su-346 6Cl0A
su-846 6Cl0A
su-846 60r0A
su-845 6910A
su-846 60'l0A
su-846 6010A
sr,J- 846 6010A
su-846 6010A
su-846 6C10A
su-846 6010A
su-845 6010A
srJ-846 6C10A
su-s46 60'l0A
su-845 3050A
su-846 60',I0A
s!j-346 6C10A
su-846 7471A
su-846 7471A l'!odif ied
su-845 3550A
su-816 8031
su-846 3550A
su-846 82708
su-946 82708
EPA 160.3 (moCified)
ATALYS I S
TRIAL DATE ANO TII{E
1 07/03/96 1104
1 07/13/96 18231 07/13/96 18?51 07/13/96 18ZB't 07/13/96 15231 07/13/96 18281 07/13/96 18?81 07/13/96 15281 07/13/96 18281 07/13/96 18?e
', a7!13/96 18ZE't 07/13/96 1EZ81 07/13/96 13?31 07/1_\/96 1823i 07/13/9b'.829i 07/0?/96 1934'. 07/13/96 182E1 07/i7/96 C94A
', 07/03/96 16t,3', c7/02/96 15n6
1 07/01/96 14041 07/18/96 17t)8
1, 07/01/96 19301 07/05/96 1C",91 07/05/96 i9..9
1 07/0?/96 1520
ANALYSI
Rick S. Rodgers
Jotene I'1. Schiel.ds
Jotene. M- Schietcs
Jolene I'1. Schietcs
Jotene M- Schietds
JoIene l'!. SchieICs
JoIene i{. SchieLds
Jotene tl. SchieLas
Jotene M. Schi eLcs
Jotene il. Schietis
Jotene i,i. schieLis
Jotene t. SchietCs
JoLene t'!. Schier.Cs
JotL.ne ltl. schietcs
JoLene !'1. SchieLds
Desi R. Ca.ozza
,.lotene I'1. Schietds
Nrna c. Hal.ter
Helti S. Mackaryan
Frances A. Deflorest
Matthew U. Kofroth
Michete o. llack
Sheery Lynn Devtin
Joseph lrl.6ambIer
Joseph ll. Gambter
!eetay B. Mehta
ll
rl
tt
rl
I
I
I
I
:l
I
I
,I
jl
jl
Lan(aster Laboratoles
2425 New Hotland Prke
PO Box 12425
Ldn.a;ier PA 17605-2J25
7]].656_2jLro Eix rt ;-656,2881
LABORATORY CHRONICLE
(I)h?n*r^tFJ.hg?,qn,gI,"
LLI Sample No. ES 2538091
Cottected: 06/?6/96 at 15:00 by BR
subili rted: 06/28/96
MEMBER
F!SI4S iISD RPD
I
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T
t
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(iI)Lancaster Laboratories 7of 14A Thermo Analytical Labciratory
LLI sample No. 2538091
CU-3 JUD crab Soi t Samote
Hercutes: Bacchus Pond
Sampte SarnpteI'IDL UNITS
Group llo. 522139Hercutes, !ncorporated - DE
LCS LCS
LCS OUP RPO
LCS LIl\IITSLOV iIIGH
4593 TCL Votati les by 82a0
gLANK
gatch: E96'185'lAB
3434 Chlororn€thane
?.3435 I u9/ kg3435 Eromomethane3. ug/ks3tB6 Vinyt Chtorid3436 Vinyt Chtoride?' uslkg3437 Chtoroethane
?' uslkg3437 Chtoroethane3. uglkg
31/+0 l!ethytene Chl.oridet!ethytene chL?. uslke
90
99
104
91
ln,
aa
102
107
99
96
93
102
106
104
99
92
98
96
109
9C
9t,
93
93
87
98
100
101
99
1C0
10',l
95
95
92
u
105
100
81
90
98
98
107
87
92
?6
q2
3
2
5
10
3
'1 1
)
6
4
z
1
20
,1
J
2
0
2
?
J
I
2
,I
95
95
102
89
96
38
103
105
95
95
91
95
105
103
105
95
'101
'I 02
'l 11
96
98
101
98
1
'1
1
10
'I
19
z4
'I
59
51
49
?z
52
70
'19
35
,1
i
53
5Z
.5t
?72
241
zso
254
?21
't5 0
188
233
155
138
155
167
162
110
190
155
209
226
157
149
'15 0
15'1
4071 Acetone7. uglkg
4076 Carbon 0isuLiide3. ug/kg
1180 1, 1-Dichtoroerhene2. ug/tg341? 1, 1-Oichtoroethane
'l ' ug/kg3444 Chtorofornr1. uglkg
3t+45 1,2-0ichtocoethane2. u9/k9
4085 2-Butanone7. uslks31tt6 1,1,1-Trichtoroethane
1 . uslk.g
31t47 Carbon TetrachIocide
1 . uslkg4091 VinyI Acerate5. us/ks3448 Eromodichtocomethane?- us/kg3450 1,2-Dichlocopropanel. uglkg3454 cis-1,3-9ichLoropropene
1 . ug/k.g1181 Trichtoroethene1. trg/kg
3452 DibcorcchIorcmethane1. ug/kg
3453 1,1,2-Trichl.oroethane?' us/kg
1 '182 Eenzene
'l . ug,u kg
3451 trans- 1,J-0ichLoropropene1. ug/kg
2. J ug/k!
N.D.
N.9.
N.D.
I-D.
N.D.
I.D.
|1.0.
fl.0.
N.0.
N.0.
[.D.
N.D.
N.D.
N.0.
N.D.
N.9.
N.D.
N.9.
Lanca5ter Laboratofles
2425 Ne,l Hoilaod Pike
PC 8ox l2'125
l-aniasr... Pn i 7605-2425
:l;'556'2i00 rax 7l:-'656'253 l a..,Or,O,'r, d'9
QIJALITY CONTR.OL REPORT
MEMBEFl
:ee rever;e, d?' at a t.)1 aa a...,. :i :. - a.Jr' aI .l a35.e,,ralroas
LLr sample No. 2538091
CU-3 JUo Grab Soi I Sampte
Hercutes: Bacchus Pond
I
j ccoup tto- 522759
i HercuIes, Inso.porated - OE
i
I
Page: 8 of 14
LCS LIi'tITSLow il t oir
15 169
50 124
52 140
64 118
46 157
47 150
37 160
37 16?
74 156
30 200
54 156
54 156
50 150
50 155
?', 79e
70 131
23 177
?5 174
54 141
57 145
6" 112
53 14?
69 135
55 146
50 147
(I)La ncaster Laboratories
A Thermo Analytical Laboratory
I
I
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:l
TI
T
LCS LCS
LCS DUP RPO
Sampte SampteIIDL UNITS
3456 Bromoform
DUP I|ISRP9 ils MSD RPO
'l . ug/kS il.D. 83 8l4108 4-Methyt-2-pentanone3. u9lk9 ll.D. 98 91
4107 2-Hexanone3. uglkS N.D. 101 90
3457 Tetrachtoroethene1. uglkg N.D. '1 15 1103449 1,1,2,2-TerrachIoroethane1. us/kg N.D. 1C0 94
1 183 Totuene1. u9.1k9 N.D. 105 101
1 l84 Ch Lorobenzene
1 . us/ks N.D. 96 96
3458 Ethytbenzene1. ug/kg N-0. 107 104
41 17 Styrene1. u9/k9 N.D. 99 92
3355 xytene (totat )'l . us/ks N.D. 105 103
6187 trans-'1,2-0ichtoroethene2. ug/kg ll.D. 1C4 98
6277 cis-1,?-DichIoroethene2. uslkg N.9. 1 C5 1 01
1625 Thaltium Barch: 96'184570800314- ns/kg N.D. (1) 93 89
1643 Atuminum Batch: 9618457C80C39.0 ms/kg N.D. 21 2927 1645 (2)
1644 Antirnony Batch: 961845708003?.2 mg/kg N .0 . ( -1 ) 92 95
1646 Earium Eatch: 961845708C032.2 mg/kg N.D. 9 105 97'1647 Becyt t iun Batch: 9618457080030.074 ms/ks N.D. 0 (1) 96 9l
1649 Cadmiun Batch: 9618/r57C80030.13 m9,/k9 x.D. 0 (1) 93 38
1651 Chromium Batch: 95'18/*5708C03O.\7 nrg/ks N.o. 0 (1) 123 i31
1653 copper Eatch: 961845708C010.50 ns/l:.s N.D. 0 (1) 'l'19 109
1654 leon Batch:95181'57083033.4 mg/ks 7.2 J mg/r.! 13 2t'52 2139 (?)
1655 Lead Batch; 9518457080032.4 mg/ks N.D. 0 (1) 96 90
1558 Manganese Eatch: 9618457080030.12 mg/kg r1.9. 11 116 109
1661 [ickel Batch:9618/+57080030.16 mg/ks N.D. 0 (1) 97 91'1666 Si tver Eatch: 96'!8457030030.45 ms/ks N.D. ( 1 ) 1AZ 97
(1) The result for one or both determinations xas less than five times the LOo.(2) The background result ras more than four times the spi<e added.
Lancd5ter Laboratofles
2425 l.le,./ Hollan.i Prke
PO 9cr 12 125
Li.(r;,'e. P{ 1 7405-ldl :
.- \ ,- -6 _\6-2)Cl i"" ,.',: -; -:6-)411
ovJ
790
12 91
4 115
797
'l 101
097
3 108
7 101
2 106
6 ',101
4 102
696
979
?79
7 100
593
799
1 102
5 102
t89
794
5 9t,
696
79e
I
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I
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"0,')1,2' d?
QUALTTY CONTROL REPORT
MEMBER
QUALITY CONTROL REPORT
I (iI)Lancaste r Laboratories Page: 9 of 14A Thermo Analytical Laboratory
LCS LCS
LCS OUP RPC
DUP MS
RPD MS I'SD RPO
I
I
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I
LLr sampJ-e No. 2538091
CU'3 JUD Grab Soit Sampte
Hercules: Bacchus Pond
I
i croup No. 522739
I xercutes, lncorporared - OE
l
I
Sanpte SampLeHDL UtI I TS
1672 Zinc0.40 mg/ks
6935 Arsenic TR0.25 mg/kg
6956 Seteniun TR0.18 mg/ks
0159 l,lercury0.023 ng/kg
BLANK
Batch:9618457083C10.80 J mglkg
Batch: 96184570B001
N.0-
Eatch: 96',I845708003
ti.9-
8a tch : 96 1 84571 1 002
N.D.
0 (1) 108
0 (1) 91
0 (1) 92
0 (i) 92
98
92
9t,
92
6
0
1
0
92
93
aa
79
LCS LII'IITSLOU HIGH
54 149
49 149
92 119
26 157I
I
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I
I
I
t
1225 TCL Pesticides in Sotids Batch:961850103A
N.D .
N.0 .
N.D.
I,1.9.
N.D.
N.D.
N.0.
N.D.
[.0.
N.9.
[.0 .
N.D.
,,1.D.
N.r.
N.9.
N.D.
N.9.
N.D -
1981 Atpha BHc5. uglkg1982 Beta BHc3. ug/kg
1983 Det ta BHC1. uglkg
1218 Garma 8HC - Lindane
'l . uslks
1219 Heptach Ior1. ug/kg1220 Atdrin1. uglks
19B1 Heptachtor Eooxide3. ug/ks
1989 Endosutfan I
t, . ug/ks
1222 Dietdrin4. us/kg
1985 DDE1. ug/kg
1223 Endcin6. ug/ks1990 Endosutfan I I9. uglkS
1985 DOD3. ug/kg
1991 Endosutfan Sutfate10. ug/ks
1221 00r
1 - ug/kg3012 Endrin Kerone5. ug/kg'1859 t'tethoxych t or40. uslkg
3O?5 Atpha Chtordane
t . ug/kg3026 Gannra Chto.dane1. ug/kg
69
76
ii
70
72
71
79
79
o/
77
A)
69
79
t7
t5
85
89
39
35
oo
86
92
88
95
9t,
105
9i
95
101
aa
97
57
95
39
21
16
19
2C
19
13
16
17
18
19
15
'18
12
20
i9
15
za
76
82
85
76
7A
1A
35
8'l
39
BB
98
87
93
911
83
9C
5B
B1
S,]
55
50
67
t5
69
67
60
60
79
72
68
62
72
62
61
t)
57
75
75
1?7
137
120
120
120
120
120
120
120
120
tz6
120
123
120
lz I
1?5
111
ar<
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for one or both determinations xas tess than five tinres the LOo.
Lancaster Laboralofies
2425 Ne,! Holland Prke
PO Box l2Ii5
Lan.;5tel PA I i605-2425
71i.556-21C0 ia, 711-i5o )".]1 O.',rr,a,n, d?
MEMBER
(l)La ncaste r Labo rato ries
.l'l
=l
LLI Sample No. 2538091
clJ-3 JUo crab soi t Sampte
Hercutes: Bacchus Pond
Group llo. 522759Hercutes, Incorporated - DE
A Thermo Analytical Laboratory
QUAL]TY CONTROL REPORT
Page: '10 of 11
LCS LII'IITSLOU HIGiI
I
.l
Sampte SarnpteI.IDL UNITS
1988 Toxaphene1,000. uglkS
1992 Endrin Atdehyde'10- ug/kg'1993 PCB - 101610. uglkg
1994 PCS-122130. ug/ks
19-o5 PCB-123250. ug/kg
1996 PcB-121?50. ug/kg
1997 PCB-124840- ug/kg
1998 PCB-1?5430. uslks'1999 PCB - 126030. us/ ks
its
r,r s0 RPo
DUPRPD fiS
LCS LCS
LCS OUP RPD
,l
,l
I
I
6LANK
N.D.
r{.0.
[.0.
N.D.
N.D.
N.9.
N.D.
N.D.
N.D.
123
4688 Tcl- su846 seorivotati tes Soi I Batch: 96'183s18026
1 185 phenoI53. ug/kg
3751 bis (2-chtoroethyt) ether67. us/kg
1 186 2-chtorophenoI53. ug/kg3754 1,3-dichtorobenzene53. ug/kg1187 1,4-dichtorobenzene33. us/kg3755 ,l,2-dichtorobenzene
33. ug/ks
4690 2-nrethytphenoI
67.ug/ kg
4691 2,2' -oxybis ( 1 -chIoropropane)
1 00 . ug/ks4692 4-methytphenot
1 00. ug/ ks
1 188 {-nitrosodi -n-propytamine
67.ug/ kg
3757 hexachloroethane
67-uslks3758 ni tcobenzene33. uslks
3759 isophorone67. uglks
3746 2-ni trophenoL
67.u9/ k9
7? 32
75 84
69 78
75 79
74 78
72 77
69 80
62 70
B4 97
748/"
75 8l
77 85
93 92
7t+ Bz
13
1'1
12
5
5
6
15
11
It{
1l
'10
7
10
9
77
76
73
1,6
t6
74
71
62
90
77
AN
76
5 112
12 158
23 134
1 17?
20 124
3? 1?e
46 123
36 166
5 152
1 230
40 113
35 180
zi 196
?9 182
T
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I
I
I
I
I
il
MEMBEFIffiiE
Lan(aster Laboratoles
2425 l'Jew Holl;nd Pike
PO Bor 12125
Lanca5rer PA 176C5-2425
7 l7-b55-2lrl0 te^'1 17 -a -\6-2631 ,.r,OrrOrnU {3See re.,e.se jrde ior erpianatrcr ci rymccis ,.c lcbi:.';i:,o:r5
DUP itsRPD MS MSO RPD
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QUALITY CONTROL REPORT
Page: '11 of
LLI sampte No. 2538091CLl-3 JUD Grab Soit SampLe
Hercutes: Bacchus Pond
Sarpte Sampte
lrD t UII I TS
, Gfoup Io. 52?759Heccutes, Incorporated - DE
i
3747 2,1-dinethytphenoI67. u9/k9
3760 bis (2-chtoroethoxy) methane31. ug/kg
3748 2,4-dichtorophenol.33. uglkg1189 1,2,4-trichtorobenzene33. ug,/kg
3761 naphthaterle33. ug/kg
1.693 4-chIoroani I ine100. ug/ks3762 hexachlorobutadiene67. ug/ks
1190 4-chtoro-3-nrerhytphenot
67 - uglks
4691 2-methytnaphthatene33. uglkg3763 hexach Iorocyctopentadiene170. ue/kg
3719 2,4,6- trich locophenot67. uglkg
1695 2,4,5-trichtocophenot
67 - uS/kg3764 2 -ch toconaph tha I ene13. ug/kg4696 ?-ni troani I ine
67 - u9/k9
3766 dimethyl. phthaLate35. uslkg
3765 acenaphthytene33. us/kg
BLAHK
N.'.
N.9.
I.D.
N.9.
N.C.
N.0.
N-9.
N.D.
N.D.
N.0 .
N.D.
[.D.
[ .0.
N.D.
N.0.
N.D.
48
73
71
77
73
75
7L
ci
80
72
79
I>
57
81
81
32
77
aa
R')
16
90
39
85
78
37
Q1
17
11
13
6
5
5
9
15
10
7
1l
10
o
o
'10
o
LCSLCS DUP
41
t>
77
a9
75
4l
81
82
6?
oa
82
79
75
80
LCS LCS LI!,IITSRPO LOV HIGii
3? 119
33 184
39 135
4t+ 142
21 133
17 116
24 116
)) 1ta
2a 1)a
'1 100
J( l.+4
39 151
60 118
55 143
1 11?
33 1/t5
4689 TCL SUB46 Senrivotati tes/Soi l. Barch: 95i83SLB025
4697 3-ni troani I ine67. u9/k9
1 191 acenaphthene35. ug/k.g3750 2,4-dini trophenoI170. ug/ks1192 4-ni trophenot
1 70. u9lk94698 dibenzofuran13. u9/k9l'193 ?,1-dinitrorotuene67. ug/ksl+699 2,6-dini troroIuene67. u9/k9
Lancaster Laboratoftes
2425 New Holland P'ke
PO gc\ i2-r25
l-ar(.rsie.. PA 17605-21:5
717".:;c-:l,l0 F:x ill-c5:i i53l
36 /+0
71 78
59 65
73 77
74 80
8? 89
g1 89
7 143
47 145
i 19't
1 132
28 '131
39 119
50 158
10
9
6
8
7
10
56
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63
75
76
90
85
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Pa,, lO,'10,/g5 aA-t
MEMBER
'.1
(I}La ncaste r Laboratories
A Thermo Analytical Laboratory
QUALITY CONTROL REPORT
Page: 12 ol
LCS LII!ITS
LOU fltGA
't 1.14
?5 158
59 121
38 122
1 181
J5 ltI
51 127
1 152
14 176
51 120
27 133
15 133
1 118
zb t5t
52 115
1 152
1 262
33 143
8 158
17 168
4 t46
24 159
I I IOJ
17 165
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LLI sample No. 2538091
CU-3 JUD 6rab Soi I Sampte
Hercutes: Eacchus Pond
Group l,lo. 522739tiercutes, lncorporated - DE
Sampte SarpleI{DL UII I TS
3n0 diethyt phthatate67. ug/kg
3769 4-chtorophenyt phenyI ether67- ug/kS
3768 ftuorene33. ug/kg4700 4-ni troani I ine100. ug/kg
1701 4,5-dinitro-2-methyIphenoI170. ug/ks
3772 tJ-ni trosodiphenyIanrine
67 - ug/kg
3773 4-bromophenyt phenyl ether100- uglkg
3774 hexachlorobenzene100. ug/kg
1194 pentachtorophenot
1 70. us/kg3 75 phenanthrene33. us/ks3776 anthracene33. ug/ks
47OZ carbazote33. uslkg3n7 di-n-butyI phthatate31. u9ll:9
3778 ftuoranthene33. us/kg
1 195 pyrene67. ug/ks
3780 butyl benzyl phthatate67. ug/ks3783 3,3' -dichtorobenzidine130. uglkg
3781 benzo (a) anthcacene33. ug/kg
3784 bis (2-ethythexyt) phthatate67. us/kg
3782 chrysene33. ug/kg3785 di -n-octyI phrhatate67. ug/kg
3786 benzo (b) ftuo.anthene67. ug/kg
J7B7 benzo (k) ftuoranthene130. u9/k9
37BB benzo (a) pyrene67. uglks
3789 indeno (1,2,3-cd) pyrene67. u9lk9
LCS t_CSLCS DUP RPO
DUP MSRPD i4S MSO RPDBLANK
N .0.
H.D.
N.D.
u.0 .
N.D.
N.D.
N.D.
N.9.
il .9.
N.D.
N.D.
N.0.
il.0.
N.D.
N.0.
tl D.
il .9.
N.D.
N -9.
r{.0.
N.0.
N.0.
N.D.
N.0.
N-9.
10 83
10 B4
779
476
966
12 73
13 80
13 82
263
'10 77
977
778
11 86
977
10 91
12 95
568
780
9 '103
885
13 103
10 80
10 86
10 78
a c,
79 88
79 87
74 80
5e 62
66 7?
7t, s4
8': 92
83 94
7!r 76
75 83
7t, 79
80 90
73 80
8t 92
86 97
55 58
7? 3l
93 103
82 39
81 92
73 80
77 35
7t, 81
82 8o
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Ldncaster laborato(es
2425 l'lew Holland Prke
PO 8ox I2.r25
Ldncaitei PA I ;605-2125
717-556-li0L1 Fax 7ll-65s-158 ]
o?a'cc:., ro/lc;9: 'lf
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(I)Lancaster Laborato ries 13 of
A Thermo Analytical Laboratory
LLl sarnpLe No. 2538091
CU-3 JUD crab SoiI Sampte
Hercutes: Bacchus Pond
Croup llo. 522239
Hercutes, lncoroorated - DE
Saflpte sampLel.lDL UN I TS
3790 dibenz (a,h) anth.acene67. ug/kg
3791 benzo (ghi) perytene67. u1/kg
01 11 lloistuce0.06 % by ur.
ELANK
I.0.
r,i.0.
Batch: 96184C3'16820003A
DUP
RP9
MS LCS LCSMS MSD RPO LCS DUP RPD
83
79
83
75
1 00 100
LCS LIIIITS!-0\J it: G il
1 227
1 219
0 100 101
91
85
9
8
ffiiIfl
Lan(aster Laboratofles
2425 New Holland Prke
PO Box 12425
Lancdsrer PA 1 7 605 - 2t2t
717-556-2100 lax 7\i'6>6 2521
QUAL]TY CONTROL REPORT
5ee le're.5e s,Ce ior exor;.r:r(n oi syftroois ana.Otr?.r,4-'nn;"cttir.;..)9a ,leg
(I}La ncaster Laborato ries
A Thermo Analytical Laboratory
LLI Sarnple No. 2538091
CU-3 JUO Grab Soi I Sampte
llercutes: Bacchus Pond
1225 TCL Pesticides in Sol.ids
4593 TCL Votatites by 8240
4688 TCL SU846 Semivotatiles SoiI
4689 TCL SU8/+6 Semivotatites/Soil
TRIAL ID
i Hercutes, lncorporated - 0E
QIJALITY CONTROL REPORA
Paqe: 14 o( 11
SURROGATE LIMITSLOU HIGH
50 12090 120
70 12181 11774 121
24 11l25 12i":9 122
23 120i0 115'18 137
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SURROGAT E
SURROGATE
TCX
0c8
d1-1,Z-DCA
ci8-totuene
BFB
Phenot -d6
2-Ftphenot
3,4,6-iBF
lJ i trobz-d5
Z- Fbi phnyL
Tphenyldi4
SUMMARY
RECOVERY Z
69
79
89
93
5U
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1',r2
9?
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Lancaster LaboratofleS
2425 New Holland Pike
PO Box 12425
Lancajier PA 17605-2.r25
ill--65b-2j00 Far 717'65o.168I ft+lililil.?! Yct
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(I)La ncaster Laboratories
A Thermo Analytical Laboratory
I o..orn. tlo: 06716
Environmen(aL Affairs
Ui Imington 0E 19894
AS RECEIVED
1of 14
2216 Rev ,Orr.r* dt
Page:
LLI sample No. ES 2538080Cottected: 6/27/96 at 09:05 by BR
Subritted: 6/28/96 Reported: 8/ 6/96Discacd: 9/ 6/96
CIJ-4 JUo Unspiked Grab Soit Sampte
Hercules: Bacchus Pond
S4JUD SDG#: tlBPO2-D4BKG
CAIiIO. AIIALYSIS IIAIIE
DRY tJEIGHT
,,i.i:i:ili'ti,:.tl:iiirii:,::.i:;:ii.:.ii:i11.:.:l.ii,i l,lETHoD
.i:r.rXi.,. :iiil:;ltSlll.li:r:iri..: DETEcT I0r L I M I T
,,,:':"'::::::i:l::l::'::::;iirl,:0:,.,,, 18.,r.,.i...:.t,'.5,C80i,,r,:::iiiij.j1: 1?.
. r ,',tr i': , ii:it::l:'i jl , : ,.,,i.iill.;0.;,.'i:ir 2 . 8. ..:.:.j,,..,,.,.165:,,.,.::::.,, 2.8
l.;:,.,i.i':;..',,,"':::l',i,:.,0.;'86:i;,i.:.,: 0.095
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tlt.l.t.:.,.t't.::: . i, ..t,:.$i.5l.::,,i.:rit,J 3 . 1
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::.::: : .i:.::::: :::::::. .9! 6.' .. i:: :: 0 . 59.r-.4"a.::..:.::.A:r:,.:.. U.5gr rr ' : ]::.:ii j. 46:r ..:r:i.: 1 0. 5 1::--::||.: --': : ':-:-:- , -:--i- -::-:,-::-,, , :: 1.:'.:' ,::::.t| r4i,,:: I U .
'z,,:,,,,1,.ri,.1i:i,,,i1:r,i:ii:::lilg':.[r:;,ii,,:,: 0.23
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P.0.
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DETECIION LIIt!IT UIIIIS
4593 TCL Votatites by 8240 See Page1625 Tha[ t iun ::,,:ii:ii., .i.:.,,,.:,..,.,:,,. n.O. 1r,. rq/kg16L3 Atumintrm ,i::;'i:':i.t:.ii4,rdg0;.::,,,..,li , 8.9 mglkg1644 Anr inpny ii:iijiii:':t:.i.:.ir:.: ;: . N . D. .' ?.2 ms/ (9
1646 Barium ::::!it':i:i.:::t:::t':::t::::::lu9':7 " : z'? mglkgiU; i"'viii.- :,:.ii..:ii,:.,ii..,i.,..,,,,r-6.i,.0 o.oz ms/ie1649 Cadmiuun :iir.:jiti :,i:.,,,., :: o.:S I 0.'13 mg/;(g1551 Chromiun i.:.,:.'.,., i.,.:, .....,I3.o . 0.17 ng/'<g1653 Copper .,i :.,. . .. 17.9 0.50 mol<s1654 lron :::::,:j,ii ,,,'6.340: ,.,,,,, 3.4 m9/<91655 Lead ..:.:',i:':':,, , :.. , 6,5 . t 2.4 rx9/k91658 Mansanese :iittr.tii,,,'i..:,;i;,t 3I:.1 .,. 0.12 mg/<s1661 Nicket ,:.:, ,:,'., .....' ..'7:4 A.16 ng/'<g1666 sitvec ::.i.:l.i:.:.t.,'i.t.: u.o, 0.45 nlg/kg1672 Zinc ..,:,':::. ,:,,, 35.3: 0.10 ng/<g6935 Arsenic TR :.,,: :,.': :... 3,1. , 0.25 n<11tg6936 Seteniun TR ..'",',;';,., ',,.'. il.D. 0.19 mg/<g0159 l.lercury ..i: l':.:.'.. ,i .0:C54,,,.,'J C-028 ms/kg12ZS TCL Pesticides in SoLids See Page4688 TCL SU846 Semivotatites Soi[ See Paoe4689 TCL SUB46 Semivotatites/Soil suu e"i"0111 Moisture ::::::::.:i. ..: .'.2J-0 0.06 7, by wr.rrl{oisturerr represents the toss in ueight of the sampte after^ oven drying at101 - 105 degrees cetsius.
l
5
'l CoPY T0 HercuIes, lncorporated
1 CoPY T0 ERI'! Rocky Hountain
ATTN: Mr . Joseph KeL ter
ATTl,l: Mr. Brent Robinson
Questions? Contact your Ctient Services Representativeat (717) 656-23C0RacheL L. (reamer
13:29:20 D 0002 ?3 REP 12tl.i6 52?739
I 1 0 25 . 00 00 1 384 00 ASR000
Lancaster Laboratofles
2425 New Holland Prke
PO 8ox 12425
Lancaner. PA 17605-2425
7 1l -656-230A Fdx: 71 7-556-2 tr8 l
RespectfuL Ly Submi tted
Ramona V. Layman, Grcup Leader
I CP l'1eta t s/Leacnates
wm 5eo,e./e.se s,de for e,o:;ratron ot;./rbol5 ano dbore,.,rat.onS
I1
(l)La ncaste r Laboratories Page:?ol 14
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LLI sarnple No. ES 2538080cotlected: 6/27/96 at 09:05 by 8R
Subrnitted: 6/2A/96 Reported: 8/ 6/96Discard: 9/ 6/96
A Thermo Analytical Laboratory
I Account llo: 06715
I xercuLes, lncorporated - DE
! Envi rorrnental. Affa i rs
P.0.
Ret.
cu-4 JUo Unspiked ccab soit Sampte
Herctites: Bacchus Pond
S4JU0 sDG#: hBP02-04BKG
CATIIO. A}IALYS tS HAI.IE
IcL votati Les by 8240
3431, Chtocomethane3435 Eromomethane3436 VinyI Chtoride3437 Ch Ioroethane3410 Melhytene Chloride4074 Acetone4076 Carbon Disutfide1180 1,1-0ichIoroethene
3t+42 1,1-0ichloroethane3t+41 Chtoroform3445 1,2'Dichtoroethane4085 2-Butanone3446 1,1,1-Trichloroethane3447 Carbon Tetrachtoride4091 vinyt Acetate344A Bromodi ch I oromethane3150 1,2'Dichtoropropane3454 cis-1.3-0ichl,oropropene
1 181 Tri ch Ioroethene3452 Dibromochto.ornethane3453 1,1,2-TrichLoroethane
1 182 Benzene3151 trans- 1,3-D i chtoropropene3456 Eromofocm/+108 4-MethyL-2-pentanone4107 Z-Hexanone3457 Tetrachtoroethene3149 1,1,?,2-Tetrachtoroethane
1 183 To(uene
1 184 Ch(orobenzene3458 EthyIbenzene4117 styrene3355 xytene ( tota[ )6187 trans- 1,2-D ich Loroethene6277 cis-1,2-0ichtocoethene
j
uitminston oE 1e8e4
AS RECEIVEO
METHOO
,iriii.:.iiiljirnt,{urls' ..,,,, DETEcr I cN LIt'tI T utl I Ts
DRY UEIGHT
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ug/'<9
uglkg
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ug/ks
ug/ <g
u9l kg
u9/ ks
ug/kg
us/ k9
ug/ kg
u9/ ks
ug/ k9
ug/kg
u9/k9
uglkg
ug/ ks
ug/'<g
ug/kg,tg/kg
u9/ (9
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Questions? Contact your Ctient
RacheL L. Kreamer
Servi ces ReDresenta!ive
ai (7',7) 656-2300 I
I
Re, ,0,30/es d"i I
Lancaslea Laboratores
2425 New Holland Prke
PO Box 12425
Lancasie( PA 1 76C5-2.125
117-656-230A aax 7 I 7-b56-268
RespectfuI ty submi tted
ItlicheIe l4cCLarin, 8.A.
Group leader, 6ClMS Votati Les
I
MEMBEFI
See 'a,erse srcie for e (oiandlron oi sTmoo s and abbrevrat:ons :2j6
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(I}Lancaste r Labo rato ries Page:A Thermo Analytical Laboratory
LLI sarnple No. ES 2538080Cottected: 6/27/96 at 09:05 by BR
Suhnitted: 6/28196 Reported: 8/ 6/96Discard: 9/ 6/96
Account llo: 05716
Hercutes, Incorporated - 0E
EnvironmentaI Affairs
Hitmington 0E 19894
AS RECEIVED
METHOD
DETECTI OI'I LII{IT UIJI IS
P.0.
Ret.
CU-4 JUo Unspiked Grab Soit Sampte
Hercutes: Bacchus Pond
S4JUD SDG#: HBP02-04BKG
CAIilo. AIALYSIS [AitE
TCL Pesticides in Sotids
1981 ALpha BHc1982 Bera BHc1983 oetra BHc1218 Ganrna BHC - Lindane1219 Heptachtor1220 ALdrin1984 Heptachtoc Epoxide1989 Endosutfan I1222 Die(drin1985 0081223 Endrin1990 Endosutfan I I1986 0001991 Endosutfan Sutfate1??1 0073017 Endrin (etone'1859 I'lethoxych Ior3025 Atpha Chtordane30?5 Ganma Chlordane1988 Toxaphene199? Endrin Atdehyde1993 PCB-10161994 PCg-1?211995 PC8-12321996 PCg-121?1997 PCB-1?481998 PCB-125/+1999 PCB-1260
riiiriri:,, i.i ir r':irIEEUtTs
DRY UEI GHT
::i:::i:::::::iji:::rl:i.iir:i::r:ji:::l:::i::::r:i::j:.. HETIIOO
ii:iiiilijiiltl!fiE*i,_tls,r::iii DETEcT ror L I l.t r T
6.
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3.
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6.
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70.
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3.
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uglk9
u9./kg
u9/k9
u9/kg
us/kg
u-olk9
ug/kc!
u9/ kcJ
uq/ ks
ug/Yg
t9/ks
u9/k9
u9/ <s
us/kg
'19/ k!
u9/ kg
u9/k9
us/ k9
u9/ kg
u9/'<g
u9/kg
u9l (9
u9/k9
us/ k9
u9/kg
ug/'<g
ug/kg
u9l k9
Questions? Contact your Ctient Services Representative
RacheI L. Krearner ar (7"t7) 656'2304
MEMBERrkm
Lancasler Laboratofle5
2425 Nerv Holland Prke
PO Box 12425
Lancdster PA I 7605-2-125
717'555-2i00 Far 717 656 2i,lll
Respectful ty Submi ttedJeniier E. Hess, B.S.
Group :eader Pesticides/PCBs
5eereve.seirdeloreyol6naironofsr'mboisa.debbre,,,ra(rons 2216 Re,, l0/30/95
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(l)La ncaste r Laborato ries
A Thermo Ana lytica I La boratory
Pag e:
Respectfu[ [y Subrni ttedchristine M. Rarcr.iff, B.S.
Group Leader, GC/MS
4of 14
P.0.
ReL -
DRY IJE I GHT
liiil:iiiiiir.:iill:iililiii:iii.i:i:1:i:riiiii:ij rlETHoo
il ;,i ir:i.iillliREEUl-ISitri:!:i1 DETECT I 0tl L I I'l I T
43.
a7
43.
13.
43.
43,
87.
110.
130.
87.
87.t3.
o1
e7.
9a
43.
45.
43.
43.
130.
87.
43.
2?0.
87.
43.oa
4J.
13.
1l
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it
ll
Il
LLI sample No. ES 2538080Cottected: 6/27/96 at 09:05 by 8R
Suhnitted: 6/28/96 Reported: 8/ 6/96
Discard: 9/ 6/96
CU-4 JUo Unspiked Grab Soit sampte
Hercutes: Bacchus Pond
s4JUD SDG#: HSP02-04BKG
CAIIIO. AXALYSIS IIAti{E
TCL SU846 Semivotatites SoiI
1185 phenot
3753 bis (2-chtoco'ethyt) ether1186 2-chtorophenoI
3714'1,3'dichtorobenzene1187 1,4-dichtorobenzene3755 1,2'dichtonobenzene4690 2'methytphenol4691 2,2'-oxybis (1 -chtoropropane)
4692 4-methytphenoL1188 t'l-ni trosodi -n-prooytamine
3757 hexach Ioroethane3758 ni trobenzene3759 isophorone3746 2-ni tropnenot3747 2,4-dimethyl.phenoI3760 bis (2-chtoroethoxy) methane3748 2,4'dichlorophenoI1189 1,2,4-trichtorobeozene3761 naphthatene4693 4-chtoroani Iine
376? hexachtorobutadiene1190 4-chlot'o-i-methYtphenoI4691 2'methytnaphthatene3763 hexachtorocyctopentadiene3749 2,4,5-trichtoroPhenoi4695 2,4,5-trichLorophenot3764 2'chtoronaphthatene4696 2-ni troani I ine3766 dimethyI phthatate3765 acenaphthytene
Quest i ons? Contac t
Rachet L. Kreamer
Account tlo: 06716
lleccules, .lncorporated - DE
EnviconmentaI Affairs
Uitmington 0E 19894
AS RECEIVED
I.4 ET HOD
jti+ii:i:,r:i:;8$Slilligi,iir, DEIEcT I 0N L I M I I un I rs
aa
oi.
33.
33.3i.
67.
100 .
10c .
67.
67.
13.
67.
67.
67.
31.Ji.
33.
100 .
67.
67.??
17C .
67.
67.
33.
67.
31.
JJ.
u9/kg
u9/kg
ug/kg
us/k9
tr9/kS
'Jg/kg
ugl k9
u9/ K9
,.tg/k9
ug/ <g
u9/ ks
ug/(g
usl k9
ug/<9
u9lks
,Jg/ <g
ug/ks
ugl k9
ug/ <g
u9lkg
ugllg
ugl k9
u9lk9
uglkg
ug/'<g
rg/'<9
uglkg
u9/kg,tg/k9
ug/'<g
il
1l
1l
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your Ctient Services Representatlvear (7"7) 656-2300
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MEMBEFlrrcIil
Lan(aster Laboratofle5
2425 New Holland Prke
PO Box 12425
Lancaster PA l,- 605- 2d?5
717'656-2300 Fax: [phone] Seereve.sesrdeforerplanrronofsymbolsandabbre,,latrons 22i6 Fe,r lCil0/95
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(iI)Lancaste r Labo r:ato ries
A Thermo Analytical Laboratory
Page: 5 of 14
ar-
1216 Rer ,Orrorr, ?ai
LLI sample No. ES 2538080
Cottecred: 6/27/96 at 09:05 by BR
subnitred: 6/28/96 Reported: 8/ 6/96Discard: 9/ 6/96
CU-4 JUD Unspiked Grab Soit Sampte
i Account llo: 05716
I xercuIes, Incc.porated - DE
I EnvirormentaI Affai rs
I uitmington DE 19894
I
AS RECEIVED
Hercutesl Bacchus Pond
S4JUD SoG#: HBP02-048KG
CAIIIO. AHALYSIS IIAME
fcL SU846 Semivotati tes/Soi I
4697 3-nitroani I ine
1 191 acenaphthene3750 2,4-dinitrophenoI1192 4-ni trophenoI4698 di benzofuran1193 2,4-dinitrototuene4699 2,5-dinitrotol"uene3770 diethyt phthatate
3769 4-chtorophenyt phenyI ether3768 ftuorene4700 4-ni troani I i ne
4701 4,6-dini tro'2-methytphenot3nZ N-nitrosodiphenytamine37Tj 4-bromophenyI phenyI ether3774 hexachtorobenzene
1 194 pentach IorophenoI3775 phenanthrene3776 anthcacene470? carbazoIe
3n7 di -n-butyt phthal.ate
3n8 f Iuoranthene
1 195 pyrene3780 butyL benzyl phthatate37Bl 3,3'-dichtorobenzidine3781 benzo (a) anthracene
3784 bis (2-ethythexyt) phthatate
3782 chrysene3785 di -n-octyt phthal.ate
3786 benzo (b) ftuo.anthene3787 benzo (k) f[uoranthene3788 benzo (a) pyrene3789 indeno (1,2,3-cd) pyrene3790 dibenz (a,h) anthracene3791 benzo (9hi) perytene
MET HOD
DETECTION LIMIT UI,IITS
ORY UEI GHT
:ti:::,:,::::::,::i:i,i:,:i:ir::,:i:ii::,::::l,ii:::i::i.,.;:;i,: llET HOD
:;jiii:,,:,:,,;,,ir1RgfltIsi,l.il:, 0ETEcT I otl L I r't I T
:'::-:, ::: ::j-,1 ::r:lN;'D't,.,:':I 87.
.::i.:ii,::i:,:tili,:i.:::,i;l.:.NiiD1;:j,,iiil 43.
. :,'ii :.:'jli.', !i: :ii1.:i:ij:i iii:,llllQii'ii:l.i, 22O .
:,l::i:i ,l:!, : '', : : i'l :ii',ll ,,: l'i ,,Il'; D ;,:::,i, 220 .
tl:.t:::,.:,t.,:tlilt.:.'ltltitlt,:i:litl:.!ii,a.,rtl:,,.t., 43'
: it:r:i:,,:::,. ::i :. :::., :.:ii::,t::,1, I l{,iD , i,::: it 87 ,
'i',:ii.. i,..:,:i:iti,::,:::::ti,)ii:Dii'::,iit 87.
,,:.:,i,,:i:..,:,.,,iii.:.i.1.,,iNiD;i.;,., 37.
..: . ::': .. .:N..:o;rj:.: 87.:;:;..:..,::'r:;::::;':::11,;9..:: 43.
.:::, i:,: :,::i ::;:::i:. t.::,l:;ll::..}{:::ci:::i'irli:, 1 30 ,
i :.,':,. :.:,: .ll:.' l: :,l:":,,,:,;1,. .: fl . b., . . . ,'' 2ZO .
; , 1: .;:i ., ,:,.,:',:,t,,::1,,,,,1 ,, ,i tt ,;Q -,,,.,,,,, 87 .
t::l.:li,:i:1.:lr: i:it::l:r:::ii::,t::i,ll ;:D ; i.:::.t 1 30.
, i,,,'i'i,.!',,,' ,'.:i':i:tii i'iili;0.;.1;,1:,' 1 10 .
:,,,,l:t:t,::,':,ti'i.:!iti:,i:i::,|:i:iill,:Dr':li:::,i ??0,
. . . .: . 1 1: ::ll,u.: :- q).
,ii.rii:.i::t:it,i!t:itttitti::iii:,i:tt.l,Ii.Di :.,,: 43.
,,. :.r':.:'.,, ,:,,:,',:i,' j.N::0.,,. 43.
:.: :' .i:.::.:i: :::,. .::.:i{ o; : :. : .l:::.::': J q J .
:::i'ii.ii.i::ii,ti,::1,:i:i:,i:iii:i:f:l{iq.:i,l',i1.. 43.
ii.,l,l::,i,1..,::i:i:,::i],i::i::i.t[:i'o;:.::]:li 87.
::ri,iii,;i.,.,;:i:t::::,t.tii.ii:'ii:i,'),ltitD:iiit,ii 87.j: :::::.::.1: :: :N.D.: 170.
i:,:,:: :;,',',:.'..,':;.:,;,31.P.;,,- 43.
,i:iii,,,..ririi.::,.ilil5q. ili:,,r:::.'J 87.
:: .:::::. j:.::::'.i: : . .i:: ll:0 ::. : 43.
,,,,:, :,,,,, N.,U;::,,
,:it:tll'l::.t:1,.,,i:!:,],:'i,:,|,:t.11,]O:.,'l:it::: 87.
11.,.,:r. '. 1;.:ii'.,iil'I,D.:.',.... 170.
,.,..,,:,,',,",,.,i,'ii,,,,.,':,lIr'9li':,,,' 87.
1i,, i,.,'',,.,,',:i.,:,,,:,,ii.it,! N r O - . 87 .
:. .,.t..:,:...:,':.....;,.,. i .:,,X,; O. , , 87 .
:ii:::..,..,:., ::::.:::'i:r,':..:::iI: li: ::::., 87 .
:i:i+:.1,::: :ociclti lc
,,,,,N,D,
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170 .
67.
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1 70.
3i.
3-1.
67.
67.
130.
31.
67.
67.
07.
130.
67.
67.
67.
67.
ug/kg
u9/ k9
u9lk9
u9/k9
uglk9
ug/ks
ugl(g
u9/ <9
ugl ig
u9l ks
u9/ ks
u9/ <9
,J9/ <g
usl kg
u9/ <9
u9l (g
u9/ <g
u9/ 19
u9/ (9
u9l kg
u9/i(g
u9/k9
us/ kg
u9/ <9
u9/'<9
ug/ kg
ug/<g
ug/ks
u9/ k9
ug/.<g
u9/ !9
ug/kg
ug/ k9
u9/'Kg
Questions? Contact your Ctienl
Rachet L. Kreamer
Services Representat tve
at (7'7) 656-23C0
Ek-lir
Lancaster Laboratofles
2425 New Holland Prke
PO Box 12425
Lancaster PA 17 605-2,1r.5
717-656-2300 rar 1i t-.,)t6'2b81
Respectfu[ [y Submi tted
christtne !l- Ratctiif, B.s.
GrouP l-eader, GC/l'1S
See .everse side ior elolanairln oi r /mbols and abbrevratrons
&&&
lt
rl
Il
It
(l)La ncaste r Labo ratories
A Thermo Ana lytica I La borato ry
Account llo: 06716
Hercutes, lncorporated - DE
EnvironmentaI Affairs
Uitmington DE 19894
Page: 6 of 11
1t
ll
]lLLr sample No. ES 2538080
cottected3 06/27/96 ar 09:05 by BR
Suhnitted: 06/28/96
cU-4 JUo Unspiked Grab SoiI Sampl.e
Hercutes: Bacchus Pond
S4JU0 SDG#: HBP02-04BKG
CATI'IO A}{ALYSIS }IAME
4593 TCL Votatites by 8240
1525 Tha l. t i un
1643 Atuminum
1644 Antinony1646 Baritl'Ir1647 Beryttiun1649 cadmiun
1651 Chromiun
1653 Copper
1654 I.on
1 555 Lead
1558 lt{anganese
1661 Nicket
1666 Si tver
t6tt Ltnc
5708 sU SU846 ICP oigest
6935 Arsenic TR
6935 sel.enium TR
0159 Meccury
5711 SU SU846 Hg Digest
0819 Sotjd SanpLe Pesticide Extract
12?5 TcL Pesticides in Sol.ids
0381 B|'lA soi I Extract'ion4688 TcL SU846 SemivoIati Ies Soi t
4689 TcL SU846 Sentivotati Les/Soi t
0111 ttoisture
;l
METHOD
su-846 82408
su-846 6010A
sr,-346 60'10A
su-816 6010A
su-846 6010A
su-846 6C10A
su-3r.6 6010A
sri-846 6l)10A
su-846 5!10A
su-846 6C10A
su-346 6010A
su-846 6010A
su-846 5010A
srJ-846 6ill0A
su-346 5C10A
su-846 1050A
siJ-846 6010A
su-846 6010A
su-846 7471A
SU-8/.6 7471A laodi f ied
su-846 3550A
su-846 8081
su-846 3550A
su-846 82708
su-846 BZ70B
EPA 150-3 (modified)
ANALYS I S
TRIAL DAIE AIID TII'IE
1 07/03/96 0??3
1 07/13/96 16591 07/13/96 16591 t)7/13/96 1659
', 07/13/96 165e1 07/13/96 i6591 07/13/96 16591 07/11/96 16591 A7/13/96 16591 07/13/96 16591 07/13/96 16591 07/13/96 16591 07/13/96 1659i 07/13/96 16591 07/13/96 16591 07/0?/96 19341 07/13/96 1659i 07/17/96 0821
1 07/03/96 16151 07/02/96 1506
1 07/01/96 14001 07/18/96 0450
1 07/01/96 19301 07 /t)4/96 10311 07/04/96 1031
1 07/02/96 1520
AIIAI-YST
Ctark A. Dougherty
Jotene M. Schiel.ds
JoIene ll. Schiel.ds
Jotene l.l. Schields
JoLene M. Schietcs
JoLene irt. Schiel.Cs
JoIene !. Sch i etcs
Jolene M. Schielcis
JoLene M. SchietCs
Jotene Fl. SchietCs
Jotene M. Schietds
JoLene M. Schietds
JoIene M. schieLds
Jolene M- SchieIcis
Jotene itl. schietds
Desi F. Carozza
Jotene M. Schietds
llina C. HatIer
Netti S. Markaryan
frances A. Demorest
MattheH U. Kofroth
trtichete 0. Mack
Shecry Lynn Devtin
Joseph l'1. 6ambler
Joseph it. Gambter
Neetay B. I'lehta
II
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7i€lTil
Lancaster Laboratories
2425 New Holland Prke
PO Box 12425
Lancaster. PA l7 505-?725
717-656-2100 F:x 717-656"25E1 d} 5r
I
T,ABORATORY CHRONICLE
See reverse srde ior erplaodtroo of symbols and abbrevrations 22 l6 F.av lCi -r'i.'95
I
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(I)Lancaste r Laboratories
A Thermo Analytical Laboratory
7of
LCS LCS LII.ItTSRPD LOU HIGH
LLI sample No. 2538080cu-4 JUD unspiked Grab Soit Sampte
llercutes: Bacchus Pond
6roup No. 52269
Hercutes, lncorporated - DE
Sarpt e
I{D L
Sa,npt e
UII I TS LCS
95
95
102
B9
96
88
103
105
95
95
91
95
105
103
105
95
101
102
111
96
98
104
9B
LC9
DUP
t
I
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I
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t
I
t
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4593 TCL Votatiles by 8240
ELANK
Batch: E961831A8
N.D.
[.0 .
N.0.
N.D.
?. J us/kg
l.l. D .
N -0.
N.D.
ll.D.
N.D.
N.D .
[-D.
N.0.
1,1.9.
il .9.
N.C.
[.0.
il.0.
N.r.
N.0.
N.D.
[.0.
N-0.
34\4 Chtoromethane2. us/ks3435 Eromomethane3. ug/kg
3436 vinyt Chtoride2- us/ks3437 Chtoroethanel- uglkq
3440 flethytene Chtocide2. ug/kg
4074 Acetone7. ug/kg4075 Carbon DisuLfide5. uslkg
1180 1,1'0ich(oroethene2. uglks
3442 1,1-0ichtoroethane1. uglkg
3441 Chtoroform1. uslks
3445 1,2-Dichtoroethane?' us/kg4085 2-Butanone7. ug/kg
1146 1,1, 1-Trichtoroethane1. us/kg
3447 Carbon Tetrachtoride
'I . ug/kg
4091 Vinyl Aceratel - us/ks3448 Eromodichloromethane2. uglks
3450 1,2-0ichtoropropanel. u9/k9345/, cis-1,3-DichLoropropene1. us/ks1181 frichtoroethene
1 ' ug/ks3152 Dibromochtoromethane1. u9lk9
31.53 1.'1,2-Trichtoroethane2. ug/kg
1 182 Eenzene1. uslkg
3451 trans-1,3-Dichtoropnopene
90
99
104
91
102
88
't 02
107
99
96
93
102
'105
10/+
99
92
98
96
109
90
94
98
93
87
98
100
'10'l
99
aa
100
101
95
95
97
81
r05
100
81
90
98
98
107
87
92
96
92
3
2
5
10
)
'I 1
2
6
I
2
1
z0
1
J
20
2
0
?
2
J
2
2
1
'l
I
10
'l
'19
?4
1
59
51
49
22
5Z
70
19
35
1
71
53
52
5l
17
)7)
241
250
?5/.
)a1
150
188
233
155
138
155
tdI
162
140
190
'15 5
209
226
157
149
150
151
183u9/k g
MEMBERrkmr
Lancaster Laboratones
2425 New Holland Prke
PO 8ox 12425
Lancasier. PA 1 7 60 _\ -24 2,:
717-656-2300 Fax 717 ar',5-2631
,l}l.J
QUALITY CONTROL REPORT
t.
See re,rerse srde for explanatron of;ymcols and abbrevrdtions 1116 Re'r l0/30/95
Il
tl
ll
tl
}ILCS
Dt-,JP
Page: 8 of 11
Group No. 522239
Hercutes, !ncorporated - 0E
Sampte sarpteIIDL UNITS
f456 Brornoform1. u9/k9
4108 4-l,tethyt'2-pentanone3. us/ks
4107 2-Hexanone3. ug/kg
3457 Tetrachtoroethene1. ug/ks
3449 1,1,2,2-f etrachtoroethane1. uq/ks
1 183 Totuene1. us/kg
1 l 84 Ch I orobenzene
'I . u9/k9
3458 Ethytbenzene
1.u9/k9
41'17 Styrene1. uglks
5355 xytene (totat )
1.us/ks
OUPRPD I4S IiSD
oo a?
98 9-1
101 90
115 110
100 94
105 -101
96 96
107 1 04
99 92
'105 1 03
104 98
105 101
(1) 93 89
?1 ZCZI lOtS tZl
(1) 9Z 95
9 ',105 97
0 (1) 96 91
0 (1) 93 88
0 (1) 1?8 13',1
0 (1) 119 109
13 2452 21.39 (2)
0 (1) 96 90
11 116 109
0(1) 97 9',1
(1) 102 97
LCS LCS LII',IITS
RPO LOU H IGH
6
7
12
4
ils
RPD LCS
93
90
91
't 15
97
10'1
97
108
't 01
106
101
102
96
79
79
100
98
99
102
'r 02
B9
94
g4
95
98
45 169
50 124
52 140
64 148
46 157
47 150
37 160
37 162
74 116
30 200
54 ',156
54 156
50 150
50 155
?1 299
70 131
?3 177
26 171
54 141
57 145
61 142
53 142.
69 135
5s 146
50 147
ll
'il
il
it
ll
I
:l
,I
I
I
I
5187 trans-1,2-Dichloroethene2- u9lk9
6277 cts'1.2'Dichtoroethene2. us/kg
1625 Thattium14. mg/ks
1643 Atuninun8.9 ms/ks
1644 Antirnony2.? mS/kg
1646 Bariutr2.2 ms/ks
1647 EeryLtium0.073 mg/ke
1649 Cadmium
0.1 3 mS/ks
1651 Chromium0.47 mg/kg
1653 Copper0.50 m9/ ks
1654 I ron3.1 mS/kg
'1655 Lead2.1 mg/ks
1658 l'{anganese0.12 mg/ks
1651 tlickeL0.46 ms/ks
1666 Si tver0.15 ms/ks
7
,l
0
l
7
2
6
4
6
9
2
7
5
7
1
6
4
7
5
5
('l) The resutt for one or both determinations uas less than five tinles the L00.
(2) The background result was more than four times the spike aCded.
Lan(a5ter Laboratorre5
2425 New Holland Prke
PO Box 12425
Lancaster PA 17605-2.125
717-556-2300 Fdx: 717-656.268I7xffin 2216 Rev ,.rrrr$ dlil
QUAL]TY COI.ITROL REPORT
(I)h#t1*,.,r,*?,?,0,,"*gr'.!
LLI sample No. 2538080
CIJ-4 JUD Unspiked Grab soiL SampLe
Hercutes: Bacchus Pond
BLANK
N.D.
fl.0.
N.D .
N.0.
N.0 .
N.D.
N.D.
N.0.
N.D .
N.D .
N.0.
N.D.
Batch:961845708003
N.D.
Eatch:96i845708003
N.0.
Batch:951845708003
il.D.
Eatch:961845708003
t',t.0.
satch:961845708C01
lr-D-
Batch:961845708003
N.D.
Satch:961845708003
N.D.
Batch:961845708003
N.0.
Eatch:96'18457083037.2 J mglkg
Batch:961845708C03
R.0 .
Batch:961845708C05
N-0.
Eatch: 96'1845708C01
N.0-
Batch:961845708003
[.D.
5es rq,/gr5p 5,69 lor eloler 6: !n of svmtlols d.c abbrevtatrons
T
I
I
I
I
t
I
I
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I
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I
I
T
I
I
I
I
I
I
(il)Lancaster Laboratories
A Thermo Analytical Laboratory Page: 9 of 14
LLr sample No. 2538080
CU-4 JUD Unspiked Grab Soit Sampl.e
Hercutes: Bacchus Pond
I
I
,6roup llo. 522259j tiercutes, lncorporated - DE
I
i
Sampt e
H0L
1672 Tinc
0 .40 tnglkg
6935 Arsenic TR0.25 mg/kg
6936 Sel.eniurn TR0.18 mglkg
0159 ttercury0.028 melkg
B LANK
Batch:961845708001
0 .80 J rng/ k9
Earch:961845708J03
N.D.
Batch: 961845708C03
N.D.
Ba tch : 96 1 845 71 1 C02
rl.D.
Batch:96'185C103A
N.D.
N.D.
T.D.
11.0.
N.!.
N.0.
N.D.
N.0.
r,l .0.
N.0.
N.9.
{.9.
N.D"
N.D.
N.D.
N.l.
N.D.
N.D.
N.0.
DUP MSRPD IJS MSD RPO
Samp I e
UII I TS
LCS LCS
LCS OUP RPD
LCS LIIITTSLCV IIIGH
5t+ 149
49 149
5Z 149
?6 157
0 (1)
0 (1)
0 (1)
0 (1)
692
093
187
079
'!03 98
91 92
92 94
92 92
1225 lCL Pesticides in Sot ids
1981 Atpha BHC5. uglkg
1982 Eera BHC3. ug/ks'198J Del.ta 8HC1. ug/kg'12'18 Ganma BHC - Lirdane1. u1/ks
I 21 9 Heptach t or1. ug/kg
1220 Atdrin1. u9lk91984 Heptachtor Epoxide3- uglkg
1989 Endosutfan I4. ug/kS
1?22 Dietdrin1. ug/kg1985 DoE1. ug/kg1??3 Endrin6. uslkg
1990 Endosutfan I t9. ug/kg'1986 DDo3- ug/kg
199'l Endosulfan suIfate
1 0. ug/kg1221 DDT1. uglkg3017 Endrin Ketone5. ug/kg
1859 ltlethoxych t or10. ug/kg
5025 AIpha Chtordane1. uglkg
3026 Gannra Chtordane
l - ug/ks
6s 127
50 137
67 120
T3 '120
69 120
67 120
60 'r20
60 120
79 120
72 120
5g 126
6? 120
72 123
62 120
61 1?1
75 125
57 141
75 125
75 1?5
21 76
16 82
19 85
z0 76
19 70
19 78
to oc
16 81
18 89
17 88
18 9B
'19 87
15 93
'18 94
12 83
?0 90
19 58
15 8'l
2A 81
69 85
76 89
73 89
70 85
72 88
71 86
77 92
71 88
79 95
79 94
87 105
77 93
32 95
34 101
t9 78
79 97
4l )t
31 95
73 89
(1) The resutt for one or both determinations rlas Less than five times the LOo
Lancasier Laboratofles
2425 New Holland Prke
PO Box 12425
Ldn(dsier PA 17505.2d::
717-656-2300 Fax:7li o:6 2ilE
at}
2l'6 Rav ,Orrorn, ?ai
QIJALITY CONTROL REPORT
MEMBEFI
5ee :everse lice ior erpldndl,on oi :!,rbol;,1.d ;obrevratrons
Page: 10 of 14
LCS LIMITS
LOU HIGH
1t
'll
1l
tl
tl
1I
Il
il
Group llo. 522759
Hercutes, lncorporated ' DE
Sarpte Sampl.eMDL UN I TS
1988 Toxaphene
1 , 000. u9lk9
1992 Endrin Atdehyde10. ug/kg
1993 PCB-101630. uq/ks
1994 PCB-122130. ug/kg
1995 ?C8-123250. ug/kg
1996 PCB-121?50. us/kg
1997 PCB-1?4810. us/ks
1998 PCB-125130. us/kg
1999 PCB-126050. us/ks
ilS
IISO RPD
DUPRPD MS
LCS LCS
LCS OUP RPO
1235715
il
4688 TcL su846 Semivol.ati'.es SoiI Batch:96183s1S026
1185 phenol33. us/kg
3753 bis (2-chloroethyt) erher57. uq/kg
1 186 2-ch Iocophenot33. uglks
375t, 1,3'dichtorobenzene33. u9/k9
1 187 1,4-dichtorobenzene33. us/ks
3755 1,2-dichtorobenzene55. ullkg4590 2-methytphenoI67. us/ks
1691 2,2' -oxybts (1 -chLoropropane)
100. trg/kg
4692 4-nrethytphenoI100. us/kg
1 188 N-ni trosodi -n'propytarnine
67. us/kg
3757 hexachtoroethane67. ug/ksf758 ni trobenzene53. uq/kg
3719 i sophorone67. ug/ks
3746 Z'ni trophenoL67. uglkg
72 82
75 84
69 78
75 79
7!1 78
72 77
69 g0
6? 70
84 97
74 BL
75 83
77 83
e3 92
7t, 82
il
I
I
I
'l
I
I
I
5 112
12 158
?3 134
1 172
20 124
32 129
46 123
36 166
5 152
1 230
40 113
l5 180
21 196
29 182
1l 77
'11 76
12 73
s76
576
674
15 71
11 62
11 90
t5 I t
'r0 80
10 87
976
miil
Lancaster Laboratones
2425 New Holland Prke
PO Box 12425
Lancaster PA 1 7605-?d25
717-656-?l0O Fax: [phone]
QUALITY CONTROL REPORT
dL La ncaster Laboratories\17' A Theimo Analytical Laboratory
LLI sample No. 2538080
CU-4 JUD Unspiked Grab SoiI Sampl.e
Hercutesi Bacchus Pond
BLAIIK
ll.D -
N.D.
N.D.
il-D.
N.0.
N.D.
il .0.
rl.D .
N.0.
See reve15e srcje for e(pranatton of 5ymbols and abbreviallons 2216 Rev ,t"^"t tl'.i, I
I
I
I
I
I
I
I
I
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I
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I
I
DUPRPD l,1S
MS LCS LCS
HSD RPD LCS DUP RPD
Page: 11 of 14
LCS LIMITS
LOU HIGH
Sampte SarpLeI4DL UX I IS
3747 2,4-dinethyLphenot67. u9lk9
3760 bis (2-chtoroethoxy) methane31. us/kg
1748 2,4-dichtorophenoI33. uslkgI189 1,2,4-trichLorobenzene55. uglkS
3761 naphthalene13. ug/kg
4693 4-chlonoani I iJ 4-chlonoani I ine100. uo,/kqu9lks
376? hexachtorobutadiene67. uglkg1190 4-chloro-3-methytphenot67. ug/kg
4694 2-methytnaphthatene33. uglks
3763 hexachtorocyctopentadi ene170. ug/ks
3749 2,4,6- ttichtorophenoL67. us/kg4595 2,4,5-trichtorophenot67. ug/ks
3764 2-chtoronaphthaIene33. uglkg
4696 Z-nitroani t ine67. us/ks3766 dimethyt phthal.ate
53. uglks
3765 acenaphthytene33. u9lk9
B LAN(
N.0.
N.D.
[.c-
I'1.0.
N.D.
N.9.
I.D.
N.D.
I.9.
N.3.
11.9.
il.0.
N.D.
N.D.
N.D.
N.D.
Lancaster Laborato.res
2425 New Holland Prke
PO 8ox 12425
Lan(aster PA 1 7 605- 2 42,\
717-656-2100 Fax 7li 55;o 2o3i
17 41
11 75
13 77
678
57s
543
981
13 82
10 78
762
'11 82
10 82
879
e75
10 80
48 57
73 81
71 81
77 82
73 77
1tr i5
80 87
75 36
17 16
81 90
80 89
79 85
72 78
79 87
75 81
32
33
39
44
21
17
?1
22
28
1
)l
39
60
53
1
3l
119
184
135
142
IJJ
tlo
116
l4 I
123
100
144
151
1 '18
lqJ
112
145
33.
3761 n
4689 TCt SU846 Semivotari Ies/Soi I Batch: 96183s18026
4697 3'ni troani t ine67. us/ks
1 1 91 acenaphthene33. u9lk93750 2,4-dinitrophenoI170. us/ks1192 4-ni trophenoI170. us/ks4698 dibenzofuran13. u9/k9
1193 2,4-dinitrorotuene67. us/ks
4699 2,6-dinitrototuene67. ug,rkg
MEMBEFlTmft!
36 40
71 78
59 65
73 77
74 80
e2 89
81 89
7
1
I
28
l9
50
10 56
973
361
675
876
790
10 85
145
191
132
131
1f9
'158
a'
to/roies ?a;
QUALITY CONTROL REPORT
(iI)La ncaster Laboratories
A Thermo Analytical Laboratory
LLI sarnple No. 2538080
CU-4 JUD Unspiked Grab Soit Sampte
tlercutes; Bacchus Pond
i
i
I Group t'lo. 522139
I Hercutes, lncorporated - 0E
I
See reverse stde for exoianatron of:rmbois dno aobrevratlons 2216 Rev
(I}La ncaste r Laboratories
A Thermo Analytical Laboratory
REPORT
Page: 12 of 11
LCS LII'IITS
tOU HIGH
,11
il
il
LLI sample No. 2538080
CU-4 JUD Unspiked crab Soit Sampte
Hercutes: Bacchus Pond
6roup No. 522239
Hercutes, lncorporated - 0E
1t
Sarp t e
MDL
Sarpte
u[ITS
LCS
RPD
LCS
DUP
MS
RPO
DUP
RPD
3770 diethyt phthatate67. ue/ks
3769 4-chtorophenyI phenyI ethec67. ug/kg
3768 ftuorene33. u9/k9
4700 4-ni troani I i ne100. ug/kg
4701 4,6-dini tro-2-methytphenol
170.ug/ kgJ772 I -ni trosodi phenyI amr ne
67.ugl Y.9
3715 4-bcomophenyt phenyt ether100. uglkg
3774 hexachtorobenzene100. uS/kg
1194 pentachtoroFhenoI170. uslkg3n5 phenanthrene33. u9lk9326 anthracene53. uqlks
470? carbazote33. uslkq3n7 di-n-butyI phthatate
33. uslkg3nB f Iuoranthene33. us/ks
1195 pyrene67. ug/kg
3780 butyI benzyt phthaIate67. u9/k9
3783 5,3''dichtocobenzidine130. ug/ks
3781 benzo (a) anthracene33. us/ks
3784 bis (2-ethythexyL) phthatate67. ug/kg
3782 chrysene33. ug/k g
3785 di-n-octyt phthal.ate
67 , ug,/kg
3786 benzo (b) ftuoranthene67. ug/kg
3787 benzo (k) fIuocanthene'130. uslkg
3788 benzo (a) pyrene67. ug/ks
1789 indeno (1,2,3-cd) pyrene67. us/kg
BLANK
ll .0.
[.0 .
t{ .0.
l.r.D.
N,D.
11.9.
N.D.
ll .D.
N.D.
N.0.
N.D.
N.D.
[.D.
}t.9.
N.D.
N.0.
N .0.
N.D.
N.0.
N.D.
N.D.
ll.D.
N.D.
N.D.
N.D.
t1s MSO
79 88
79 87
74 80
59 62
66 72
7+ 34
81 92
83 9t,
7/+ 76
75 83
74 79
30 90
73 80
83 9?
86 97
55 58
77 Cl
93 101
32 89
8'r 92
73 80
77 85
7r, 8'l
8Z 39
10
10
7
4
9
12
13
IJ
2
10
9
7
11
9
10
5
7
I
I
13
'10
10
10
8
LCS
83
84
79
76
66
It
BO
82
63
77
aa
86
77
91
95
68
80
103
B5
103
80
36
78
1
?5
59
3B
,]
l8
53
1
14
5l+
?7
35
,l
26
52
,1
1
17
4
2/'
11
17
l
114
'158
121
lZZ
18i
ltt I
127
15?
176
120
135
I JJ
118
137
115
152
?62
141
158
168
1l+6
159
I6J
'163
171
il
,l
I
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I
I
I
t
I
MEMBER
r&m-l
Lancaster Laboratorie5
2425 New Holland Pike
PO Box 12425
Ldncaster, PA 17 605-2,125
717-656-2300 Fax 717'656-2631
T
2216 Rev ,rrr* d'i I
I
QUALITY CONTROL
See ,e'rerse:rcie {or eio doatron o's;mcols lnd iboreyrahons
I
t
t
I
I
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(I)Lancaste r Laboratories
QUALITY CONTROL REPORT
Page: 1l of 14A Thermo Analytica I Laboratory
LLr sample No. 2538080
CU-4 JUD Unspiked Grab SoiI Sampl.e
tlercutes: Bacchus Pond
522739
lncorporated - DE
Sarpte SarpteI.{DL UII I TS
3790 dibenz (a,h) anthracene67. us/kg
3791 benzo (ghi) perytene
67 - ug/kg
0111 l,loisture0.06 Z by !,t.
BLANK
H.D .
ll.D.
Eatch: 9618401'16820003A
Lan(aster Laboratofles
2425 New Holland Prke
PO Box '12425
Lancaster, P.A 17605-2425
717-656-2-100 Fax: 7l 7 6:o-253 l
MS
RPO
DUP
RPD
91
8679
9
o
LCS LCS
LCS DUP RPO
LCS LI!lITSLOil HIGi.I
1 ZZ7
1 ?19
0 100 101
83
75
1 00 100I
I
I
T
I
I
I
I
I
I
I
I
TFHii t!'
,or,orrt ?a*5ee re?e:se',.oe 'or e\p n.di.o_ ,;{ ;ymg911 a_o .,obrpvrai,or:
(I)La ncaste r Laborato ries 14 o{l4
,i1
1l
'jl
1l
11
ll
Il
'i1
ll
ll
rl
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A Th e rmo Ana lyti ca I La bo rato ry
LLI sample No. 2538080
CU-4 JUD Unspiked G.ab Soit Sarpte
Hercutes: Bacchus Pond
'1225 IcL Pesticides in Sotids
4593 TcL Vo(atites by 8240
4688 ICL SU846 Semivotatiles SoiI
4689 TCL SU846 SemivotatiIes/Soit
Group No. 522239
Hercutes, Incorporated ' DE
SURROCATE SUt'JMARY
TRIAL ID SURROGATE
TCX
DCB
d4-1,2-DCA
c8- totuene
8rB
Phenot -d6
2-Ftphenot
2,4 ,6-f8P
lli trobz-ci5
2-Fbiphnyt
TphenYtdl 4
RECOVERY Z
75
92.
89
95
92
69
65
71
73
80
SURROGATE LII.IITSLCU HI6H
50 '120
50 120
70 121ol
7/+ 121
Ur 11325 12',
19
23
iB
12?
'r 20
115
137
MEMEtEFI
Tikim
Lancaster Laboratones
2425 New Holland Prke
PO 8ox 12425
Lancaster. PA 17 605-2425
717-656-2300 Fax 7 17'656'2581
,t?.i
QUALITY CONTROL REPORT
5ee .?rer:e iioe ror eroranat on cf symoolS and Jbbrcvratrcns 2216 Rev 10i30/95
;l
CAT
N0.
4593
1625
1643
1b4\
1645
l04/
1649
1651
1653
1651
1655
1658
1 661
1600
167?
6935
6936
01 59
12?5
4688
4689
0'l 1'l
I
I
t
I
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I
I
I
I
I
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(I)La ncaste r Laboratories
A Thermo Analytica I La boratory
LLI sanple No. ES 2538084Cottected: 6/27/96 at 09:05 by BR
Suhflitted: 6/28/96 Reported: 8/ 6/96Oiscard: 9/ 6196
CU-4 JUo (9-12tr) crab SoiI Sample
Hercules: Bacchus Pond
s4JD9 SDG#: tl8P0?-05
, Account llo: C5716
, Hencutes, Incc.porated - DE
I Envr ronnentai Af fai rs
I uitringron rE 1989/.
Page:1of 14
P.0.
Ret -
ORY UEI GHT
ii:::iiliii:,,,,':::l-:,,:,,'I:::..:1,,iii::,;, ilETHOo
i r;ir,:,: :.:, :i:,FEsu.tils:1:..;;11' 0ETECT I 0N L I M I T
17.
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0.039.,r,J 0. 16.r. 0. 57t:,,,. 0. 60,...,.q. i
r'i:.J ?'9t:i.. 0.14,,:,' 0 - 55
0.54
0 .48
0.30
0.?2
0 .035
AIIALYSIS }IAIIE
TcL votatites by 8240
Thattiunr
A I uni nul
Ant i mony
Bar i um
Beryt t i un
Cadni un
ghromi Lflr
Copper
: r'on
Lead
I'langanese
Iti cket
Si Iver
Z inc
Arsenic TR
SeteniLfi TR
Fler cury
TcL Pesticides in sotids
TcL su846 Semivotati tes Soi t
TCL SU846 Semivotati tes/Soi t
Itloi sture
ME I HC'
OEIECl I ON !- II.,II T UN I IS
See Page
1t,. nglkg8.3 ,ns/ks
?.2 mg/kgZ.? m9/k9t'.!73 m9/k9
!_.. i3 ngl <g
!-' .4o nt/ <gC.,1', n(j/r:g
3.3 m!r,/<g2.n nql <g4.12 mg/<gf.i5 nr3/<9
I'r!, r Ji. l9 mg/ (9
D.:5 mg/i9!_'.1e ng/ <9
0.028 rllq/(g
s.e ; age
See PegE
See ?age
d dL o/ k, ,,+.r Jf ,t.
A9 RECEIVEO
,:::::i::::::l j,:,,,,,,o E,s || Tc
rrtloisturel represents the toss in weight oi rhe sampte after oven drying ar
103 105 deqrees Ce(sius.
1 COPY TO Hercutes, lncorporated
1 CoPY IO ERM - Rocky I'lountain
ATTII: Mr. Joseoh Ker- Ler
ATIN: f1r. BrenI Rrbin5on
Ouestions? Contact your Ctien: Services q.ept'esectative
at (7:7) 656'214aRacheL L. Krearner'14:29:11 D 0002 ?3 REP 126tti6 522719310 25.00 00158400 ASRCCg
Lancaster Laboratones
2425 New Holland Ptke
PO Box 12425
r-ancasier PA I 7605-2r.1:
7l7-555"2100 F;t. i:' 61c lti
Resoectf ul. Ly Sub,nitred
Ramona V.r-0yrn.1n, Ceoup Leacer
! :F Yetr'- S/':cacrates
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MEMBEFI
.1l
(il}La ncaste r Laboratories Page:ilA Thermo,Analvtical Labo ratory
I
i Account No:- 06716
j Hercutes, lncorporated - DE
i Envi rornrenrat Af fai rs
i Ui tmington DE 19894
2ot 14
2.
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2215 F.er ,Orrorr, ?ai
ilLLI sample No. ES 2538084Cottected: 6/27/96 at 09:05 by BR
Suhnitted: 6/28/96 Reported: 8/ 6/96Discard: 9/ 6/96
CU-4 JUD (9-12r') Grab soii Sampte
Hercutes: Bacchus Pond
S4JD9 SDG#: HBP02-05
CATNO. AIIALYSIS IIAI.IE
ICL votatites by 8240
1134 Chtoromethane3135 Brqnomethane3436 Vinyt Chtoride
3437 Chtocoethane3440 Methytene Chtoride4074 Acetone1076 Carbon 0isutfide1180 1,1'Dichtoroethene344? 1,1-0ichtoroetnane
3441 Chtoroform3,i45 1,2-DichIoroethane4085 2-Eutanone
3416'1,1,1-Trichtoroethane3417 carboo Tetrachloride4091 vinyt Acetate3448 Eromodichtoromethane3450 1 ,2 -0 i ch I orooropane3454 cis-1,3-0ichioropropene1'l81 Trichtoroethene3452 DibromochIocomethane3453 I,1,2-TrichLoroethane
1 182 Benzene3151 trans-1,3-Dichtoropcopene3456 Bromoform4108 4-l'tethyt-Z-pentanone4107 2'Hexanone3457 Terrachtoroethene3149 1,1,2,2'Tetrachtoroethane
1 185 To I uene
1 184 Ch Iorobenzene3458 Ethytbenzene4117 styrene3155 xytene (tota[ )6187 trans-1,2'Dichtoroethene6277 cis-1,2-0ichtoroethene
AS RECEIVED
t:.:.i:;:r::::::::.:::i::!.:.:.:::::r::i.r: ::::.::: HETHCO
.i:iii:i:ji;ii'ftEFUUIt::il; DETEcT r cH L I r't I T ux t rs
DRY UEIGHT
,,i.lrii:,,:l:,i.ii,iiii.i:tii1:l:;!;,i:iiii:ti:r: METHoo
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1l
1l
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u9/ (9
u9/ kg
u9/ <g
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'.rgl k,l
u-q/ kJ
u3/ <!J
,.]L)/ <c),
ut:/ <tJrl/ iE
u!/ <g
N!/ <'!
ugl <g
u9/ is
ug/':'9
t2/'<9
u9/ (g
ug/ ig
uglk9
ug/'<9
u9/k9
u9/t9
ug/ <g
u9/ Kg
u9/kg
u9/kg
u9/ k9
,rg/'<g
uil <9
'r2/ <g
!g/ks
u9/ (9
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)
oueetions? Contact your Client Services Represen:ative
RacheL L. Krear0e. al (717) 656'233c
Lancaster Laboratofles
2425 New Holland Prke
PO 8ox 12.125
r-dncaster, PA I 7505'2.125
7 17 -555'2300 Fax /17-656-2531
Respec!ful ly Submi tted
!ichL.Le lccLarin, 6.A.
GrouD :eader, G!/!r9 VoLati tes
See.e,.e,5p,,ie'o. 7tri.a|. r' c: ;ymbois lnd abb.eTratrons
on
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(iI)La ncaste r Labo rato ries Page:3ot 14
LLI sample No. ES 2538084Cottected: 6/?7/96 at 09:05 by BR
Suhnitted: 6/28/96 Repocted: 8/ 6/960iscard: 91 6196
A Thermo Analytical Laboratory
I Account No: 06716
I hencutes, !ncorporated - DE
I Envi cornrentat Af iai rs
i Ui Imington DE '19894
I
I
AS RECEIVED
r::::r:::i:::iit::::::::::::1rr:::::r:.:r::r. -: I"ETHOO
iirtiii::,,t::,trsuLIs:r : DETEcr:cli L!HtT url!Ts
CU-4 JUO (9-1?il, Grab Soi t Sampte
Hercutes: Bacchus Pond
S4J09 SOG#: HBP02-05
CATXO. A}IALYSIS }IAI.IE
TcL Pesticides in Sotids
1981 Atpha BHc
1982 Bera Etlc1983 Detra gHc
12'18 Garma 8Hc - LinCane1219 Heptachtor1220 ALdrin1984 Heptachtor Epoxide1989 Endosutfan i122? Dietdrin,1985 DDE1223 Endrin':990 Endosutfan !l1986 DDo1991 Endosutfan SuIfate1221 DDT3017 Endrin Ketone1859 Methoxychtor3025 Atpha ChIordane3026 GarmE Chtordane1983 Toxaphene1992 Endrin Atdehyde1993 PCS-10161994 PCB - 1 22 11995 PCS-1252'1996 PCB-1?t+?1997 Pc8-12481998 PCA-12541999 PC8-1260
:,',,, , lI .0 ;':,, .tt.a.
:l{. E.
.. .i N,r,
...' N.a..
r,r,::: u.!.
,,,:,,.,,V.D.
,',::'l,:'. li.f''
,,, ,,, u i,
::lln
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,,,,:,,.,, lJ.!.
s-!-
:::u:.
s
qr- -
4.
'1.
1 nnn
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5D.
4i.
3t).
ugl (g
!9/ <g
u9/ <g
,Jg/'< g
ug,/ kg
t9/'<g
J')/ <9
)9/'-':
':g/ <9
ug,/ k E
!1/'t:9
ug/ (9
u!/ <g
i!/ <g
ri) / <,)
19/ <.)
,t'l/ <9
u9,/ k9
'J9l <g
u9/ <9
r!/ <9
ur)/ <9
u9/'kg
u'-il kil
ug/ (g
19/ <e:
DRY UE I GHI
RespectfuL iy Subnii tted
.ienifer a. Hess, B.s.
Group 'eader Pr-st icides/PCBs
:it:i:iiili.ii,l.i,:i';'iiiii;ir,:iii::,:i:,: |1ETH00
r,::r ::,r:,,iili8Esut:Isiiiii,: DEr E cT I oN L I l.t t r
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Questions? Contact your CIient Services Representat!ve
RacheI L. Xrearner at (7'7) 656-2]C0
Lancaster Laboratoies
2425 I'le.d Holland Prke
PO Box 12425
Lan(asier PA 1i6i5-).J2t
717-,i;6-210C Far ; l7-r;ic l:rd
a'!)
1216 Rev ,O,rO,n, l-J
MEMBEFI
(I}Lancaste r Laboratories
A Thermo Analytical Laboratory Page:4of 14 Il
}I
II
Il
ll
il
d*I
T,LI sample No. ES 2538084Cottected: 6/27/96 at 09:C5 by BR
Subnritted: 6/Z8196 Repo|ted: 8/ 6/96Discard: 9/ 6/96
CU-4 JUD 19-12) Grab soit Sanrpte
tlercuIes: Bacchus Pond
S4JD9 SDG#: HBP02-05
CATlto. AllALYsIs llAt'lE
TCL s!J846 Semivotatites SoiL
1185 phenoI3753 bis (2-chloroethyt) ether1186 2-chtorophenoI3754 1,3-dichtorobenzene1187 1,4-dichLorobenzene
3755'1,2-dichtorobenzene4690 2-nlethytphenot4691 2,2'-oxybis (1-chtoropropane)
46S2 4-methytphenot1183 N-nitrosodi-n'propytamine3757 hexachtoroethane375A ni trobenzene3759 i scphorone3746 2-ni trophenol37t7 2,4-drmethytpheno'.3760 bis (2-chtoroerhoxy) methane3743 2,4 -di ch Iorophenol1189 1,2,4-trichiorobenfene376', naphthatene4693 4-ch(oroani I ine3762 hexach t ocobutadi ene
'1 190 4-chtoro'3'methylphenol.L69t 2'methytnaphthaIene3763 hexach torocyc Iopentadi ene3749 2,4,6-trichtorophenoI4695 2,4,5-trichiorophenoI3764 2-chtoronaphthaLene4696 2-ni troani I ine3766 dirnethyt phthatate
3765 acenaphthylene
I Account No: C67'16'ilercules, Incorporated ' DE
I Envi ronnlentaL Af f a i rs
I uiLmington DE 19894
I
P.0.
Ret.
Il
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AS RECEIVED
:::::::t:#i:rjrir::'.::i:i:::::i-::ja HETHOo
filiiii. !,'illliiri: DETEcrl0N Ltt'!lr urllTs
67.'li
li.
07.
1CC.
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67.
67.
l:1 .
o7.
67.
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11r0.
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67.
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b7.
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u9/\g
u9l t9
us/ ks
ug/ (9
u9/kg
,r9/ 79
u-cl (9
ug/ig
u9/ <9
ug/ (g
u:/(g
u9l <g,'g/ <\!
ug/ <')
U:],/(E
u!/t9
,ri/ <g
N9/Nq
t1/'r.J
u9/'rg
ug/ (g
u9/ (g
u9/ (g
a9/ <g
ugl k9
ug/ <cJ
ug/ <g
'Jg!'^rJ
'r9/'-g
ut/'<9
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0ucstions? Contact your Ctieni
R3cheL ,-- KreaNer
Se!.'r; ces llepresenlotive
ar (7'.7) 65b-23!5
I
T
I
I
I
Lancaster Laboratones
2425 New Holland Prke
PO 8ox 12.125
Ldncasief, PA. 17505.1J25
717-655-2100 F;i: 71 i-ii56-15€
Resoec:fuL Iy Submi tted
Chrlstine itl. RaicLif{, 8.S.
6roup !-eader, 6ClMS
5eere,,er:a,dea.rr:,aanarronci;7moo5.tnd.rbbre,/idlrons 2216 ie, l0/30i95
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(I)La ncaster Lab o rato ries Page: 5 of 14A Thermo Analytical Laboratory
LLI sample No. ES 2538084Cottected: 6/27/96 at 09:05 by BR
Suunitted: 6/28/96 Reporred: S/ 6/96oiscard: 9/ olCb
CU-4 JUD (9-12") 6rab Soit Sampte
Hercules: Bacchus Pond
S4J09 506#: HBP02-05
CATilo. AIALYSI S [Ar{E
TCL SU846 Semivotati les/Soi I
4697 3-ni troani t ine'119'l acenaphthene3750 2,4-dinitrophenot119? 4-ni trophenol.4698 dibenzofuran
1 193 2,4-dini trototuene4699 2.5-dirritrototuene3770 diethyl. phthalare3769 4-chtoropherryl phenyI ether3768 ftuorene
47OO 4-nitroani L inet+701 4,6-dinitro-2-methytphenot37-l? ll-nitcosodiphenytanine3773 4-brornophenyt phenyI ether3771 hexach I orobenzene1194 pentachIocophenor,3775 phenanrhrene3776 anthracene4702 carbazo(e3777 di -n-butyL phthatare3T7A f!.uoranthene
1 195 pyrene3780 butyt benzyt phthatate3783 3,3' -dichtorobenzidine
3781 benzo (a) anthracene3784 bis (2-ethythexyL) phthatate378? chrysene3785 di -n-octyt phthatate3786 benzo (b) fIuoranthene1787 benzo (k) f'.uoranthene3788 bcnzo (a) pyrene3789 incieno (l,2,3-cd) pycene
3790 dibenz (a,h) anthracene3791 benzo (ghi) perytene
Ij Account No: 06716
i Hercutes. !nccrporated - DE
I Envi romrentaL Affa i rs
1 ,,liLmington DE '19894
on
Ret.
AS RECE IVED
t{ETHOo
DETECTION LII,(II UHIIS
DRY UEIGHT
i:it:,i:ii:r.:,:xiiiii;iiiiiiii,ii:!:,i',:l;:.:,, ilETflo0
u,il'li;ilii'$salls,j,,i ;i oerecr t or t- t x t r
::,i':'tti,ij:!i.!rirtit..:t::,i:i.'.,j:j}{l;0,itii:: 82.
,,, :.,1. i :',t...,:. i:..:: t,, ,lt,j,D il:::i:, 41 .:; ' ;;,,.;,1g,j1i.',,;,, ZCO.
,itr::,.,i,i: '''ti,,:i.:r.t,i:,.i..l*iD,l't,.:.i 200..,,. i .i'\..&::t: !1
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.:t: ::.:l ' :'r:,:: " tr:U j}..:,,:::' 92.
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Cuest i ons? Contact you.
RacheI L. Kreamer
CL ient Services Represeniative
ar (71 7) 656-23C!
rr,siifl
Laocasiel Laboratofle5
2425 I'lew Holland Prke
PO Bor 12125
Lnnc;;ier. PA I :6a5-;ti.l_s
717.655-:iC0 :r^ lt ;.,i)a,la,i
PespectfuI ly Submi ttedChris!ine !1. Rarclii+, 3.S.
croup Leader, GCIHS
:ee e,.,e::e;:CeiDr:,11-i.a:!onali/ruoi.r.aaDrr.g'.i:!O.5 2:t5 Re.. l0;10/95
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LLI sample No. ES 2538084cottected: 06/27/96 at 09:05 by 8R
subnitted: 06/28/96
Account llo: 06716
Hercutes, :ncorporated - DE
Envi ronnEntai Affai rs
Uitmington 0E 19894
Page: 6 of 14
ANALYST
ctark A. Dougherty
Jo I ene I'1. Sch i etds
Jotene M. SchieLcs
JoIene ltl. Schietcis
Jotene M. Schielos
Jotene iq. Schietcs
JoIene M. Schielcs
Jotene il. Schietis
-otene tl. Schi elds
JoLene ltl. Schieids
Jotene tl. Schieics
JoLene M. SchieIcs
iolene 11. Sch'i eids
Jotine,{. Schietis
Jo L ene lil. Sch i elcs
0esi R. Catozza
..loIene I'1. schieLis
Nina C. HaLLer
tletLi s. Markaryan
Frances A. Demorest
tlattheH u. Kofroth
Michete D. l,lack
(I)Lancaster hboratories
A Thermo Analytical Laboratory
CU-6 JUD (9-12") Grab SoiI Sanpte
llercutes: Bacchus Pond
54J09 SDG#: HBP02-05
CAT[O AiIALYSIS IIAI|E
t593 TCL Votatites by 8240
1625 Thatlium
1643 Atuminun
1644 Antinony
1546 Bariun
1647 Beryt t iLnn
l6119 Cadrriunr
1 65 1 Chromi urn1553 copperi65!+ I ron
1655 Lead
1658 Manganese
1661 NickeI
1666 si Lver
167? Zinc
5708 su su846 IcP Digest69f5 A.senic TR
6936 seteniun TR
0159 Mercury
5711 sU sU846 Hs Digest
0819 sol.id Sampte Pesticide Extract
1?25 TCL Pesricides in Sotids
038'1 8l,lA soi I Extraction
468g TCL StJ846 Semivol.ati les Soi t
4689 TCL sU346 Serrrivotati Les/Soi L
0111 lloisture
METHOO
su-846 82408
SU-8/.6 6C10A
s'r-846 6010A
sr-846 6C1CA
su-846 6010A
su-846 601CA
su-846 6010A
su- 846 6C'i 0A
su-3/,5 60i0A
su-846 6010A
su-846 6,J10A
su-946 6010A
su-846 6C',l0A
su-846 5.110A
s"J-815 60',t0A
su-846 3050A
su-8,{6 6.:10A
su-846 6ClCA
su-816 7171A
su-845 747iA Modified
su-846 3550A
SU-8/+6,8C81
sU'8/i6 3550A
su-846 82708
su-846 82703
EPA 160.3 (modified)
AiIALYS I S
TRIAL DATE AND T!I.IE
1 07/03/96 0428
1 A7/13/96 17511 07/11/96 175t+1 07/13/96 175t,1 07/"3/95 175t+1 A7/13/96 173t+1 07/1,3/96 17541 07ii3/96 1754i !7/13/96 1754., a7/13/96 1754i 17 / 13 /96 17 -<4't 07/i3/96 17511. 17/.,3/96 175tt1 D7/13/95 175+1 07/i3/q6 1751
'. 07/02i96 193t,', 07/1:/96 175rr1 07/17/96 0909
1 07/03/96 16241 07/02/96 1506
1 07/01/96 14001 07/18/96 0642
Lancaster Laboratones
2425 New Holland Prke
PO Bor 12.:25
Ldn(asret PA 17605-ll:5
717-656-210C i.rr li7 656-2581
1
1
1
1
07/01/96 19\0 sherry Lynn Devtin
07/05/96 1319 Joseph H. Gambter
07/05/96 13''9 Joseph l.1.6ambter
07/0?/96 15Zo Neetay B. I'lehta
tt
,1115 F..', 'Or-,Or* L"
I,ABORATORY CHRONICLE
5ee re,/ease ,de:or:(iriaatoa tl /mool; dno nborevrat:oo!
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(iI)La ncaste r Labo ratories
A Thermo Analytical Labqratory
QIJALITY CONTROL REPORT
Page: 7 ol 14
LLI sample No. 2538084
CU-4 JUD (9-12") crab Soit Sampte
Hercutes: Eacchus Pond
I
1
i croup xo. 522159
I nercutes, lncorporated - DE
I
I
I
SarrpIe
}lD L
Samp t e
UII I TS
DUP MSRPD FS I.ISO RPO
LCS LCSLCS CUP RPD
LCS LIitITS
LOU H I GiI
4593 TcL Votatites by 8240
3431 ChIoromethanez. uglkg
3435 gromomethane
3. ug/k.s5436 Vinyl. Chtoride2. ug/kg
3437 Chtoroethane3. us/ks
3440 l{ethytene ChLocide2. ul/ks4074 Acetone7. ug/kg
4076 Carbon Disul.fide3. ug/kg
1'lB0 i, 1-Dichtoroethene?. ug/kg3442 i, l'Dichtoroerhane1. u\lkg
3441 chIoroform1. ug/ks
3/,45 1,2-DichLocoethane2- uglkg
4085 2-Butanone7. ug/kg3446 1, 1,1-Tf ichtoroethane1. uslks
3447 Carbon Tetrachtoride1. uglkg
4491 vinyL Acetatel. us/kgf448 Broopdi chtoromethano?. uslks3450 1 ,2 -D i ch I oropropane3. ug/kg
3451 cis-1,3-0ichtoropropene1. us/ks
1181 TrichIoroetnene1. uglkg
3152 Dibcomochtoromethane
1 . uglkg
3453 1, 1,2-Trichtoroethanez. ug/kg
1 1 82 Eenzene1. uglkg
3451 trans - 1 ,3-0 i ch Ioropropene
1 . us/ks
ELANK
Eatch: E961 831A8
N.D.
il.0.
N.D .
N.D.
?. J ug/kq
N.D.
N.!.
N.0.
N.D.
r'1.0 .
N.D.
N.D.
il.9.
N.9.
N.D.
N.D.
I.0.
H.D.
ti.D.
il.0.
I.0.
N.9.
N.D.
1 ?7?
1 241
1 250
10 254
1 2?1
19 150
?4 188
1 233
59 155
51 138
19 155
Zl lO r/
52 162
70 140
19 190
55 155
1 209
1 226
71 157
53 1t9
5? 150
37 151
17 183
395
?95
5 102
'!0 39
396
11 88
2 10J
6 105
495
295
1 9't
20 95
1 105
3 101
20 105
295
0 101
z 102
2 111
396
29e
2 104
19B
90 87
99 98
!04 100
9i 101
rcz 99
o0 70
1C2 100
1t7 101
99 95
96 95
93 9?
102 84
106 105
104 100
99 81
92 90
98 98
96 98
109 107
90 87
9t, 92
98 96
93 q2
Lan(aster Laboratones
2425 New Holland Prke
PO Box 12425
Ldncdsiet PA i7645-2x.:
1i7-656-2)40 Fax 7ll.6!c 153'
tl'
t",ao,n, l-ESee reverse r,ce for eroianarron of 5rmbcl5 Jnd Jbbrev,atioos
(iI)Lancaster Labo rato ries
QUALITY CONTROL REPORT
Page: 8 of 11
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A Thermo Analytical Laboratory It
:II
tl
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LLI sample No. 2538084
cu-4 JUo (9-12() G.ao soit sampte
llercutes: Bacchus Pond
sarTpte sarnpteMDL U}IITS BLANK
3456 Erornoform
croup tlo- 522739
He.cutes, Incorporated - DE
1. uglkg N.D. 88 83
41OB 4'llethyt'2'pentanone3. u9lk9 N -D - 98 91
4107 2'Hexanone5. ug/kg tl.D. 101 90
3457 Tetrachtoroethene1. u9lk9 N.D. I'15 !10
3149 1, 1,2,2-Tetrachtoroethane
1 . ug/ks |,1 .0. 100 94
'I 1 83 To I uene1. uglkg tl.D. 105 103
1 184 Ch lorobenzene
1 . u9/k9 N.D. 96 96
3458 EthyIbenzene1. ug/ks li-D. '187 101
/+1 17 Styrene
1 . uglkg N.D. 99 92
3355 xylene (totat)1. us/ks N.0. 105 103
6187 trans-1,2'0ichtoroethene?. ug/kg N.D. 104 98
6277 cis' 1,2-DichtoroetheneZ. us/kg tl.D. 105 101
1625 Thattiurn Batch:96184570800314. ms/ks N.D. ( 1 ) 93 89
1643 ALuminum Batch: 9518457080038.8 ms/ks N.D. 21 2a?7 16t+5 (?)
1644 Anrim,ony Batchr 961845708003
2.2 mg/ks 1,1.0. (1) 92 95
1646 Bariunr Batch: 961845708003Z.? ms/ks N.D. 9 105 97
'1647 Eeryttium Batch: 9618457080030.0fi mg/kg N.D. 0 (1) 96 91
1649 cadmiun Batch: 961845708003
o. 13 mg/kg N.o. 0 ( 1 ) 93 88
1651 chrornium Batch: 9613457080030.46 ms/kg N.D. 0 (1) 1?8 131
1653 Copper Batch: 96184570B003
0.49 mg/ks Ll-o. 0 ('l ) 119 109
1654 lron Eatch: 9618457080031.3 mg/ks 7.2 J $slks '11 ?452 2139 (2)
1555 Lead Eatch: 9618457C33032.4 mg/ks N.D. 0 (11 96 90
1658 Manganese Batch: 961845703003
0.12 mg/ks N.D. 11 116 109
1661 Iicket Sarch:9618457C8!4030.45 mg/kg tl.D. c (1) 97 91
'1666 SiLver garch:96'1845708C01
0.44 ms/kg N.D. ( 1 ) 1DZ 97
(1) The resutt for one or both determinations uas tess than five times the 100-
(2) The background result Has more than fouc times the sPike added.
:Il
Il
il
it
rl
DUP I'IS LCS LCS
RPO I,IS ilSO RPD LCS DUP RPO
6
7
12
I
7
1
0
3
2
6
4
6
9
z
7
5
1
6
i,
7
5
6
7
93
90
91
1 ',l5
97
101
97
'r 08
i0l
105
101
102
96
79
79
100
98
99
1n,
'102
89
94
94
96
98
LCS LIIIITS
LOU HIGH
45 169
50 124
52 140
6/+ 148
46 157
47 150
37 160
37 162
T4 IIO
30 200
54 156
s4 156
50 150
50 165
21 299
70 131
21 177
lb ll4
54 141
57 145
61 142
53 142
69 135
55 116
50 1A7
i1
rl
]l
t
I
,l
Lancaster Laboratones
2425 New Holiand Plke
PC 8ox 12a25
Linrdster ?A I7605-212'l
717-b56-:100 Frr 717-6:o-r631 see re,/c.5e s,qc fcr explanai:on oi ;rrio.i aic;bijie/rjirons i?. i:l/lCi95 dl 'l
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(iI}La ncaste r Laboratories
A Thermo Analytical Laboratory
QUALITY CONTROL REPORT
Page: 9 of 14
LCS LII'IITSLOU HICH
92
93
87
79
54
49
(,
26
LLI sample No. 2538084
CU-4 JUo (9-12rr) Grab Soil. Sampl.e
Hercutes: Bacchus Pond
i
Ii Grouo No. 522159
I nercul,es. tncorporated - DE
I
I
Saflpte SampLeMDL UN I TS
1672 Zinc0.39 n9/kg
6935 Arsenic TR
0.25 . m9/k9
6936 setenilllll TR0.18 mg/kg
0159 Hercury0.028 ms/kg
BLANK
Batch:9618457080010.80 J mglkggatch: 961845708C03
!{-D.
Eatch:961845708C03
il.D.
Barch: 96184571 1002
N.C.
Eatch:961830103A
N.9.
N.0.
r.D.
N-C.
ll.D.
N.D.
N.D.
N,D.
ll.D.
ll.D .
lt.0 .
N.0.
N.D.
N.0.
N.0.
N.D,
N.D.
N.1.
N.9.
0 (1) 108 98
0 (1) 91 92
0 (1) 92 9t
0 (1) 9? 92
87 105
77 93
82 95
84 ',10',1
69 73
79 97
t+7 57
81 95
73 89
times the loo.
I'rs
HSO F.PO
OUPRPD I'1S
LCS LCSLCS OUP RPD
15V
12?5 lCL Pesticides in Sol,ids
1981 Atpha BHc5. ug/kg
1982 Eeta BHc3. ug/kg
1983 Detta 8HC1. ug/ks
1218 Ganma BHC - Lindane1. ug/kg
1219 Heptachtorl. ug/kg
1220 Atdrin1. uslkg
1984 Heptachtor Epoxide3. uS/kg1989 Endosutfan I4. ug/ks
1222 Dietdrint . ug/kg
1985 DOE
'l ' uglkg1223 Endrin6. ug/kg1990 Endosut fan I I9. ug/kg
1986 DDo
l ' us/kg
1991 Endosulfan Sutfate
1 0. uslkg1221 DDT1. ug/kgfO]7 Endrin Ketone5. us/kg
1859 Methoxychtor40. ug/kg
3025 Atpha Chtordane1. us/ks
3026 Ganrna Ch tordane1. u9/k9
6s 85
76 39
7i 89
70 35
7? 88
71. 85
77 92
74 88
79 95
79 9t,
al
'16
20
19
19
ao
Ib
10
17
18
19
15
12
20
'19
15
20
76
oa
aq
76
70
78
85
81
B9
B8
98
aa
93
94
B]
90
5e
B1
81
65 127
50 137
67 120
73 120
69 120
67 120
60 120
60 120
79 120
72 1?0
68 126
6? 120
72 1?3
6? 120
61 121
75 125
57 141
75 12'
75 125
(1) The nesutt for one or both determinations Has tess than ftve
rffiilil
Lancaster Laboratofles
2425 New Holland Prke
PO 8ox 12425
Lancnsier. ?A i76C5'lil:
1 t: -636-23q0 Fax 7l l-o!5.-e-i i 'Oc.,1.d aDbre\.'r;i cn3 '0. ii/i5
tt).?.#
(iI}La ncaster LaboratoriesA Thermo Analytical Laboratory
QUALITY CONTROL REPORT
Page: 10 of 11
LCS LIMITSLO\./ H I Gi{
57 123
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LCS LCSLCS DUP RPD
95
MS
I.ISD RPD
'10
9
DUPRPO MS
LLI sample No. 2538084
CU-4 JUD (9-12t) crab SoiI Samp[e
Hercutes: Bacchus Pond
I
I
1 Group No. 52269
i Hercutes, lncorporated - DE
I
I
I
Sanpte SampteI'IDL UI{ I T5
1988 Toxaphene
1 ,000. us/kg
1992 Endrin Atdehyde10. uS/kS
1993 PC8-101630. ug/ks1994 PCB-12?130. ug/kg
1995 PcB"123250. us/ks
1996 PCg-1?4250. ug/kg
1997 Pc8-124840. ug,/kg1998 PC8 - 125430. ug/kg
1999 PCB-125030. ug./kg
8 LANK
[.0 .
il.D .
N .0.
N.0.
N.D.
N.0.
H.D.
N.D.
il.9.
4688 TCL SU846 Sernivotatites soiI Eatch:95183s18025
'1185 phenoI31. ug/kg3753 bis (2-chtoroethyt) ether67. ug/kg
'I 1 86 2-ch Iorophenot33. u9/k93754 1,3-dichtorobenzene33. uslks
1187 1,4-dichtorobenzene33. ue/ks3755 1,2-dichtorobenzene33. ug/kg4590 2-rnethytphenot67. u9lk94691 2,2' -oxybis (1 -chLoropcopane)
1 00. ug/kg
4692 4'methytphenoI
100 .uslkg
1 188 N-ni trosodi -n-propyIarnine
57. uglkg
3257 hexach I oroethane67. uglks3758 ni trobenzene31. ug/kg3759 isophorone67. uglkg
3746 2-nitrophenoI67. uslks
r.l. D.
N.D.
N.D.
[ -0.
t{.D.
N .0.
ti.D.
N.l.
N.0.
[ .0.
N.0.
N.0.
N.D.
N.0.
72 82
75 8/.
69 78
75 79
7t- 78
72 77
69 80
62 7C
81 97
71 U
75 85
77 8l
83 9?
71 32
IJ
11
lz
5
5
6
'15
11
11
13
10
7
76
T3
76
76
71
6?
90
77
BO
aa
t6
s 112
12 158
?3 134
1 17?
20 izL
12 129
46 123
36 166
5 15?
1 230
40 113
35 180
?1 196
29 182
,l
Lancasler Laboratories
2425 New Holland Prke
PO 8or 12425
LJncasie( PA I 7605.1115
717-556-2300 Fax 717-6!6-163 I
t]Dl.i
MEMBER
See 'e'.,er:e .,.ce ' jt ?!u'anal$n ci :tmbots aid ;borevrdtrons )) 16 ?.ev \ABC/95
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QL]ALITY CONTROL REPORT
Page: fi of 11
I Grouo No. 522739
Hercutes, Incorporated - DE
I
Sampl e Sarnpl eilDL UII] TS
5747 2,4'dinethytphenol.67. u9/k9
3760 bis (2-chtoroethoxy) methane33. uslks
3748 2,4-dichtorophenot33. ug./ks'1189 1,2,4-rrichtorobenzene33. u9lk9
3761 naphthatene13. ug/ks
4693 4-chloroaniline
1 00. uglks
3762 hexachIorobutadiene67. u9/k9
1 190 4-chtoco-J-nrethytphenot67. u9lk91694 2-methytnaph(haLene33. ugl k9
3763 hexachtorocyclopentadiene
'l 70 . u9/ ks
3749 2,4,6-trichLorophenoI67. ug/ks/.695 2,4,5-trichl.orophenot67. us/kg
3764 2-ch loronaphrhatene33. u9/k9
4696 2-ni troani I ine67. ug/k.s
3766 dimethyt phthatate33. us/kg3765 acenaphthytene31. us/ks
ilstlSD R?O
DUPRPO MS
LCS LCS
LCS DUP RPD
LCS Lll'llTSLOU HIGH
32 119
33 184
39 135
4t 1tz
21 133
17 116
?!r 116
?2 147
)e 1r?
1 ',100
37 144
3e 151
60 118
51 143
, 112
7 143
t 7 1/.5
1 191
I t5z
28 131
39 139
50 158
17 41
l',I 75
13 77
678
575
5 /,i
9 B't
13 82
1C 78
11 q'
1n aa
875
1C 80
877
48 57
73 81
71 81
77 82
73 77
14 15
80 37
7': 86
7ti 32
t/ ic
81 90
8C 89
79 g5
tz tb
79 87
75 81
4689 TCL SU846 Semivolati Ies/Soi I Eatch: 96183sr-8026
4697 3-ni troani t ine67. u9/k9
1191 acenaphthene13. us/kg
3750 2,4-dlni trophenoL
1 20. uSlkg119? 4 -ni trophenot
1 70. us/kg4698 di benzofuran33. u*/ks
1193 2,4-dinitrototuene67. trglkS
1699 ?,6-dinitrototuene67. uslks
16 40
7i 7P,
59 65
73 77
74 B0
s2 89
8,1. 89
i0
I
6
a
7
10
56
73
OJ
75
90
85
Lancasler Laboratofie5
2425 flew Holland PLke
PO 8oi 12.125
l;.(Jt:er PA',- 1C5. 2 1 )
")i7-6ta 23CA ?+ ::t 616.!45
(iI)Lancaster Laboratories
A Thermo Analytical Laboratory
LLI sample No. 2538084
CU-4 JUD (9-12r') Grab SoiI Sampte
llercutes: Bacchus Pond
ELAIIK
N.D.
[.0.
N.C.
N.D.
N-C.
N-0.
N.9.
t{.0.
N.D.
N.t.
N.D .
N.D.
N.9.
N.9.
N.).
sce,Erei;e jlcg r,-i a.crdnai.cn,); :;rbc ;aal daDre';r;i,c.r
,Il
I1
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t
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I
Sample SaopteIIDL UIII TS
3n0 diethyt phthatate
. 67 - us/kg
5769 4-chtorophenyt phenyt ether67. ug/ks
5768 ftuorene35. ug/ks
47OO 4-ni troani t i ne
1 00. ug/kS
4701 4,6-dinitro-2-methytphenot170. uglks
37'12 !l-ni trosodi phenytami ne67. u-o./kg
3773 4-bromophenyt phenyl ether100- ug/kg
3774 hexachIorobenzene100. ug/k.s
1191 pentachIorophenoI
1 70. ug/kS5n5 phenanrhrene33. uglkg
3776 anthracene33. ug/kg
4702 carbazote33. uslks3n7 di-n-butyt phtha(ate13. ul/kg3ng ftuocanthene33. ug/kg
1 195 pyrene67. u9/k9
3780 butyI benzyt phthatate
67. uglks
3781 3,3''dichtorobenzidine130. uSlkg
3781 benzo (a) anthracene35. ug/kg
3784 bis (2-ethythexyt) phthatate
67. u9/k9
37BZ chrysenell. ug/ks
3785 di -n-octyt phthatate
67. us/kg
37B6 benzo (b) fluoranthene67. uslkg
3787 benzo (k) fluoranthene130. ug/ks
3788 benzo (a) pyrene67. ug/kg
3789 indeno (1,2,3-cd) pyrene67. uslks
N.0 .
fl.D.
N.0.
[.0 .
N.0.
N .D.
N.D.
N.D.
[.D .
N .0.
N.D.
N.D.
N.D.
N.9.
N.D.
N.D.
N.D.
* N.D.
N .0.
ll .0.
tl.D.
ll-D.
Lancdster Laboratories
2425 New Holland Prke
PO Bor 12425
LJncJsre( PA 1 75;5-:J25
7 17-556-1100 F at I l] -o->6-2tts
BLANK
Group [o. 522739
Hercutes, lnco.oorated ' 0E
QLTALITY CONTRCL REPORT
Paqe: 1? ol 1.4
LCS LIHITSLOU HIGiI
1 114
25 158
59 121
38 1?2
1 181
38 147
53 127
1 152
1.1 176
54 120
27 133
35 133
1 118
26 137
52 115
1 152
1 262
5J 'CJ
I 158
17 i68
4 lrro
21 i59
11 163
17 163
i 171
tts
I{SD F.PO
DUPRPD FlS
LCS LCSI-CS DUP RPO
.ll
ll
ll
Il
ip
Iil
i;
li]l
il
rl
ll.D.
N.D.
I.0-
8l
84
79
76
66
73
a)
6l
78
86
91
95
68
BO
103
85
101
BO
B6
78
82
10
10
7
4
9
12
tl
'.3
2
10
9
7
11
79 83
79 87
74 30
59 62
66 7?
71 84
31 92
35 9\
74 76
75 33
7L 79
30 90
7i 80
83 92
36 97
55 58
a1 qa
93 103
z2 39
81 92
7i 80
77 85
71 81
e2 89
9
'10
12
5
7
I
I
13
10
10
't0
8
t!
n..,,rn, ?OU
iI
il
ill
(|)L+n:**ff.1*P,o,t1tgI,n'
LLI sarnple No. 2538084
CU-4 JUo (9'12") Grab Soit SampLe
Hercules: Bacchus Pond
MEMBEFl
12 r6 R:,,
I
I
I (I)Lancaster Laboratories
QUAiTTY CONTROL REPORT
Page: 13 of 14A Thermo Analytical Laboratory
MS
RPO
OUP
RP9
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T
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T
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LLI sample No. 2538084
CU-4 JUD (9'12") Grab Soi I Sarnpl.e
Hercutes: Bacchus Pond
Group No. 522759
Hercutes, lncorporated - DE
Ilt
I
Sarpte SampteIIOL UNI TS
3798 dibenz (a,h) anthracene67. ug/kg
3791 benzo (ghi) perytene57. ug/kg
0111 tiloisture0.06 I by xt.
BLANK
}I. D.
x.D.
Barch : 95',I84051 65200C3A
83 91
79 86
I
LCS LCSLCS OUP RPO
B3
'! 00 100
LCS LII'IITS
LOTJ H I GH
1 227
1 219
0 100 101
9
o
Lan(aste. Laboraio.re5
2425 Ne,r Hoil.tnd Prke
PC lox 12425
Ldocas:et 2A l,'5C5-:i
11 r--63irZ),Clt ia, i'
MEMBEFl
)ee.r/e",f : r'.. ptC a-;_.!r,i',yrco ;.,crl l5c'i/rdl,ons
(I)La ncaste r Laboratories
A Thermo Analytical Laboratory
LLr sample No. 2538084
CU-4 JUD (9-12") Grab SoiI Sampte
Hercutes: Bacchus Pond
1225 TcL Pesticides in Sotids
4593 TCL Votatites by 8240
4688 IcL SU846 Semivotatites Soit
4589 IcL SU846 Sernivotati tes/Soi I
I
l
I Group xo. 522759
I HercuLes, lncoeporated . DE
I
I
QTIALITY CONTROL REPORT
Page: 11 of 14
SURROGATE LITIITS
LOU HIGH
$l
]l
ll
Il
SURROGATE SUM[.'!ARY
TRIAL ID SURROGATE
TCX
DCB
d4-1,2-oCA
o3-toLuene
Br0
Phenot -d6
Z-FIphenot
2,1 ,6-tsP
N i trobz -d5
2-Fbiphnyt
Tpheny!.d14
70 121
RECOVERY %
53
85
89
92
91
73
78
39
78
66
?4 113?5 121
19
2330 115
50
50
al
120
120
il
il
'I1
il
117
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120
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Lancaster Laboratories
2425 New Holldnd Prke
PO 8,:r 12J25
Laocrster PA I 76C5-2d:5
7l7-556'2300 Fax 71 i-616')r-31 dtt,l
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CU-1 JUD Dupticate Grab Uater SanEte
llercutes: Eacchus Pond
CUJU! SDG#: HBP01 -CJDL.;P
CATNO. AIIALYSI S IIAME
172? That t iurn17t3 Aluninun17/.1 Ant inrony1i'16 8ar i um1747 Bery[ [ iun
t t4Y Lamtm1751 Chlaniunr1753 Copper1714 I ron1755 LeaC1758 l{anganese1761 N i ckeL1766 Si t,rec1772 Zinc7035 Arsenic TR7436 Scteniurn TRC?59 [ieicury
LLI sample No. EL 2538002cotIected: 6126/96 at 1?:95 by Bn
Suhnitted: 6/28/96 Reported: 8/ 1/96Discard: 8/ 9/96
I Account No: 067i6j tercul.es, lncorporareC - !Ej Envi rorrrcnta I Affa i rs
I ui Lmington )E i9{J94
AS RECE!VED
r,tET H0c
DETECI:3I.I LIHIT !NITS
17t. !s/ Lti - u!/',
15 . ug/'rJ :.2 ug/t-1.3 ugll?.7 u9/ |J 4.1 !g/i1.3 u9/!
5 .9 ug/'.13. tr!/'.2.9 u?/ t
J 5.i '.sg/'.I .6 uL:/ '.1:. uJ/LJ ? .7 u:.:/'.
? -7 ug/',
t .43 ug/ i
P.0-
Rel-
Resoectful Ly submi tted
Ranrona V. laynan, Group LeaCer
ICP i{er:a Ls/'-eachates
A Thermo Analytical Laboratory Page: 1 of l
2216 Rev ,Orr.rn, d*3
1 CoPY T0 Hercutes, lncorporateCI coPY I0 ERt'{ - Rock }, t',ourr r i n
ATTl.l: qr- Joseph Ker.Lr'rATIiI: Y.- Brent Rooinson
Questrons? Corltact ycur CIient Sc,rvjces RepresenrJt!ve
Ractet L. Kroamcr a'(. (7',7) 65o-2il]0
MEMBER7Xm
03:ll:it, D irii2 '15 Rir 1?c4io 52?7?7310 0.30 0iC00Ct0 ASRCU',1
Lanca5ler Laboratofle5
2425 New Holland Prke
PO Box 12425
Lancaste( PA 17 695-)a25
717-655-2100 Fax [phone]ee reverse 5rde for explan;:.on of symools and abbrevrattons
&&&
LLI sampJ.e No. EL 2538C02
cottected: 06/26/96 ar 12:05 by 8R
suuni rted: 06/23/96
CU-1 JUo Dupticate Grab Warer SampIe
I
; Account tlo: 06716
, Hercules, Incorooraaed - DEI EnvironnenraL Aifai rs
i ui tminqton 9E 19894
LABORATORY CHRONICLE
Page: ? ol
AIIALY ST
Donna R- Sackett
Donna R. Sackett
Donna R- Sacke(t
oonna R, Sackett
oonna R. sackett
Donna R. sackett
Donna R. Sackett
Donna R. Saci(ett
Donna R. sackett
oonna R. Sackett
Donna R. sackett
Donna R. Sackett
oonna R. Sackett
Donns R. Sacketr
Christine H, ConLin
oonna R- Sackett
Donna R. Sackett
NetIi s. Mal.karyan
Ie!.Li S. tiarkanyan
(I)Lancaster Laboratories
A Thermo Analytical Laboratory Il
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Hercutes: Bacchus Pond
CUJUD SDG#: tlBP0'l -03cUP
CATNO A}{ALYSI S IIAHE
1722 ThaLIim'1743 Atumintrrn
1 744 Ant i nrony
1 746 Bar i unr
1 747 EeryI t i um1749 cadmiul
1751 Chromium1753 ccpper1754 I ron
1755 Lesd
1758 l'(anganese
1761 N icket
1766 Sitver
1772 Zinc
1848 uu SUe46 IcP 0igest (tot rec)
7035 Arsenic TR
7036 Selenium TR
0259 ltercury
5713 UU Su846 H9 Digest
FETHOO
su-846 6010A
SU-846 5110r1
su-846 6',''lCA
SU-346 6!'':CA
srJ-846 6n1r1A
sl/-34o 501CA
srJ-346 6010A
su-846 6i',i0r\
su-846 6:13A
St,-846 6,r':r'14
sr-846 6110A
sr-346 6,lr0A
SU- 345 6il'l LlA
su-846 5'li0A
su-845 3,'rD-sA
su-84,5 5:.110,\
s'J-846 5'-110A
su-346 7470A
su-346 7i7CA
ANAI-YS I SIRIAL DAIE AIJD TIME
1 07/15/96 s3051 07/',5/e6 f;3.!5', n7/15/96 t3A5I !7/:5/96 0j05
" 07 /,.5 /96 C3C51 07/:5/96 03'_15
'' A7 /':5/96 f;3t5', c7 /',5 /96 0315
" t7t'.51e5 s3g5'. )7/';5/95 C3l5': C7!"5/96 A305': 07/^,5/96 t3i5', D7/.5/96 030-<,' t7/1.5/96 93051 D7/'..9/96 12721 Lr7l 15,/96 03051 07./1 5/96 0305
2 07/17 /96 16152 D7!'6t96 21t3
Temt
Lancaster Laboratofles
2425 New Holland Pike
PO 8ox 12425
Lan(astet PA 17 505-2425
7 11 -656-2300 F ax 7 1'1 -656'2681
Il
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A Thermo Analytical Laboratory
QUALTTY CONTROL REPORT
LIi'IITS
HIGH
3of
LLI sample No. 2538002
CU-1 JUD Dupticate G|ab Uater satrpte
Hercutes: Eacchus Pond
: Group No. 522727
| ;teccutes, Inco.porated - DE
Sanp L e
I,ID L
1722 Thattium
170.
1743 ALuminun
1744 Antimony
15.
1746 Bariun
)7
1747 BeryLtiurn
1.3
1749 Cacirniunr
2.7
1751 Chronrium/.4
1753 Coppec
3.8
1754 I ron
5.9
1755 Lead
18.
1758 ltanganese
2.9
175'1 llicket
5.4
i766 Sitver
1772 Zinc
12.
7035 Arsenic TR
2.7
7036 Setenium IR
)7
0259 t!ercury
0-43
SamoI e
UNITS
Ug,/ t
us/ t
u9/ t
ugl t
ug/ |
u9/ t
ugl I
u9/ |
ugl t
u9/ t
u9/ |
u9/ t
ug/ t
us/ |
u9/ t
u9/ |
ugl t
103
-7?9 (2)
105
s3
97
95
- 191
-1411 (?)
93
t!
95
1C1
-34
1n,
79
1 102
3 103
1 104
1 100
5 101
1 103
1 103
0 108
DUP ]i
RP9 HS MSD RPD
LCS LCS LCS
'.CS DUP RPO LOUBLANK
Eatch:96'192'18431C2
N.9.
satch: 96i92 1348102
{.0.
Batch:96'1921843:32
N.D.
Barch: 96i9218.4.9:02
N.9.
Eatch:9619218r.B:C2
0.C0'16 J n:g/t
Batch:951921ts43!C2
N.D.
Batch: 961921848:02
N.C'.
Batch:96'192'1818102
N.D .
Batch: 961921848032
C.C6t:,7 J ng/l
Eatch : 96.192't 3461C2
Barch: 96192 !8/.3i02
N.1.
Barch : 95',I92.',l8431C2
1i.3.
Batch:9619218433C2
t{.0.
Batch; 96192'18/*8!02
H.D.
Eatch: 96 1921843!02
N.9.
Batch: 961921843:C2
N.D.
Eatch:95':985711'101
N.D.
(1)
111
0 (1)
(1)
(1)
0 (1)
0 (_1 )
c (1)
0 (1)
0 (1)
0 (1)
0 (i)
c (1)
'101
-77?
1C5
97
94
78
-20'l
l) lJ
92
59
99
-L1
1
0
'l
2
9
80 120
80 1?0
80 1?0
80 1?0
80 120
80 1?O
80 120
80 120
B0 '120
80 120
80 120
80 120
80 120
80 't2 0
80 120
80 120
80 120
102
108
107
100
98
97
.07
101
111
1
26
1
'l 01
1C1
The resutt for one oc both d".terminations Has Less than frve times
The background resuLt uas more than ioltr t!nles rh::;pi<.: aCCed.
MEMBEFI7Xm
Lancaster Laborato(es
2425 New Hoiland Prke
PO 8ox 12425
Lancaster PA 11 605-2421
7 17 -656-2300 Fax 717.o56-i681 5ee re,rerse stde ior erpianatron of svmbols and abbre,/ratrons 2216 Rev ,orror$ d.j
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(I}Lancaster Laboratories Page:'1 of 6A division of Thermo Analytical lnc.
LLI Sample No. EL
CoI tected:2538 330
Suhnitred: 6/28/96 Repocted: 7/10/96Discard: 8/10/96
Trip Btank Uate. Sampte
Hercutes: Bacchus Pond
TBHBP SDG#: HBP01 - 13I6
CATI{0. AIIALYSIS NAI.IE
459? TcL Vol.atites by 8?40 - Uarer
Account No: 06716
HercuIes, !ncorporated - 0E
EnvirormentaL Affairs
Ui tminston, DE 19894-0001
AS RECE IVED
:..::i:i:ii:ij:.::,ft !SlJtTS : lt'tt DETECT I Ctl L I U I T UII I TS
See Page 2
P.O. /BR
Rel..
TO
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,I COPY
1 COPY
Hercules, Incorporated
ERM ' RockT Mountain
ouestions? Contact your CIien!
Rachet L. KFeamer
07:38:02 D 0002 1s90 0. 00 0c026000 ASR000
SL'rv i c L.s Represen !a t i ve
ar /.7:7 ) 656-Zilu
ltL,q)b )!11I /
ResFec!fuL lY Submi ttedt'lichele YcCLarin, B-/i.
Croue -eaCer, 6C,/liS VL.lati les
ffiil,Tfl
Lancaster Labora!ofiet
2425 Ne,ry Holland Prke
PO 8ox 12425
Lancdsier. PA 17503-2.125
717 -656-D0a Fax [phone]e 'eyerse sroe icr i{tlenatro. or symcols and abbre,/ratron5 2216 Peu stolte6 i3
ll
(I)La ncaster Laborato ries
A division of Thermo Analytical lnc.
2538330
7 /10/96
I
i A..ount No: 06216
i Hercutes, Incorporated - DE
i Envi ronmenraL Af f ar rs
I ui tmington. lE 19894"0001
I
Page:2ol
P.O. /BR
Ret.
ResDectfut Ly Submi tted
ilicneLe llcclarin, B.A.
Group !eader, 6Cllis VoIati ies
]l
llLLI Sample No. EL
co[ [ected:
subritted: 6/?a/96 RePorted:Discard: 8/10/96
Tcip Etank Uater sarnpte
Hercutes: Bacchus Pond
TBHBP SDG#: HBP01 - 13T8
CATIIO. ANALYSIS IIATIE
TcL votatjtes by 8240 - Uater
1258 Chtocomethane1257 Bromomethane3492 V iny l. Ch t or ide3494 chtoroethane3497 I'tethytene Chtoride3498 Acetone3499 Carbon Dis.uLfide
3500 1,1-Dichtoroethene
3501'1,1'Cichtoroethane3503 Chtoroform3504 1,2-DichLoroethane0316 2-Butanone3505 1,1,1-Triclitoroethane3506 carbon TetrachLoride3507 vinyt Acetate3508 BromodichIoromethane
3509'1,2-oichIorooropane3516 cis-1,f-DichLoropropene3511 Trichtonoethene
3512 Dibromochloromethane3513 1,1,2-Trichtot-oethane3515 Benzene3510 trans-1,3-Dichloropropene3518 Bromoform35?1 4-t'lethyt-2-pentanone
3520 2-Hexanone352? Tetrachtocoethene3521 1,1,2,?'Tetrachtoroethane35?4 Totuene3525 Chtorobenzene3526 Ethytbenzene3528 Styrene35?9 xytene (totat)
5780 trans-1,2'Dich(oroethene6268 cis-1,2-0ichLoroethene
AS RECEIVED
!:;ir:rI::i::::::i!::::i:::::::::::i::;::: j I r::ri:::r M E I H00
:ti:;i,i:ii;ii;ftFsg1S :,r,::iir DETEc T : 0N L I H I T utl I Ts
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RacheI L. Kneamer
Servi ces Representative
ar. (7i7) 656-2100
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Lancaster Laboratones
2425 New Holland Prke
PO 8ox 1242!
Lancaster PA 1 7605-2+25
717-656-2300 Fax [phone]
tl'
??16 nev. 5/01/96 ?: J'
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See reverse srde for elJlaaa:,c. of 5ymbois a.o abbre'/ratlcns
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LABORATORY CHRONICLE
(iI)La ncaste r Labo rato ries
A division of Thermo Analytical lnc.
LLI sample No. EL 2538330
Cot Iected:
Submi tted: 06128/96
Trip Btank Uater Sa[p[e
Hercutes: Bacchus Pond
TBHBP SDG#: HBP0'l -13T8
CATIIO AIIALYSI S IIAHE
4592 TcL votariles by 8240 - uater
METHOO
su-846 821.08
Lancaster Laboratorres
2425 l.le6, Holland Pike
PO 8ox 12425
Lan(astet PA rT 635-2425
717-656-2100 ta\ 7 1,1'6t6'26?' 1
Accounr ilo: 06716
Hercutes, Incorpoaated - DE
Envirornentai Affairs
ui Lmington, DE 19894-0001
ANAI-YS I S
TRIAL OATE AIID TIlIE AIIAI.YST
1 07/03/96 0659 susan A.
see re'/erse srde for eroiara: or cf symcol5 aod ;boreviatroas 2216 Rev 5/01i9o
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ll(iI)La ncaster Laboratories Page: 1 ot
A division of Thermo Analytical lnc.
LLI sample No. 2538330Trip Btank tlater Sarnpte
Hercutes: Bacchus Pond
I
I
i Croup tto.
i xercutes,
I
II
ll
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I',ID L
Sarnp t e
UII I TS
1258 Chtoromethane3. uglt
1257 Brc*nomethane3' u,/t
3192 Vinyt Chtocide2. us/t
3494 ch Ioroethane3. uSlt
3497 l,lethytene chtocideZ. ug/t
3498 Acetone6. us/t
3499 Carbon 0isutfide3. u9/ t
3500 1,1-DichIoroethene1. ug/t3501 1,1-Dichtoroerhane?' uglt
3503 Ch toroform1. uq/l3504 1,2-Dichtoroethane?' us/t
0516 2-Butanone3. us/t
3505 1,'1,1-Trichtoroethane1. uS/t
3506 Carbon Tetrachloride1. ug/t
3507 vinyt Acetate2' us/t
3508 Bronrodichtoromethane1. ug/[
3509 1,2-0ichIoropropane1. ug/t
3516 cis-1,f-DichLoropropene'l ' us/t3511 Trichtoroethene1. ug/t
3512 Dibronochtoromethane2. ug/[ t
3513 1,1,2'Trichtoroethane2. ug./ t
3515 Benzene
'I . uS/t
3510 trans-1,3-DichIoropropene1. uslt
BTANK
4592 lcL Votatites by 8240 - uater Eatch: 1961841M
522777
!ncorporated - DE
ilsMSO RPD
OUPRPo MS
LCS LCS
tCS OUP RPD
LCS LIMITS
LOU HIGiI :il
N.D.
N,D.
N.D.
N.!t-
N.9.
N.D.
H.!.
8.0.
N .0.
N.9"
N.9.
N.D.
N.0.
N.D.
N.D.
N.D.
N.D.
N.D.
N.0.
N.ir .
il.D.
r'1.D.
N.9.
1l
il
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;l
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jl
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3
9
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1.1
2
1
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5
2
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1
1t,
16
0
.,?
73 68
oo al
90 82
6t ot
iaz 98
67 9i
75 72
11t, 106
1 15 109
96 ',t00
64 97
116 1'.!(
111 1',10
84 'l 10
99 104
98 1 0',1
97 l0l
1 06 ',l05
87 99
82 96
104 104
91 102
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Lancaster Laboratories
2425 flew Holland Pike
PO Bor 12425
Lancaster PA 17 605-2425
1 17 -656-2)00 Faxr 71 7-655-?68 l
QUALITY COITTROL REPORT
5ee reverse srde for erolanat,on of svmooi5 dnd aborevratroas
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QUALITY CONTROL REPORT
Page: 5 oJA division of Thermo Analytical lnc.
LLr sample No. 2538330Trip Btank Uater Sampte
Hercutes: Bacchus Pond
i Group No. 52277
, Hercutes, Incorporated - DE
I
Sanpte SampleHDL UII I IS
35'18 Eromoform
1 ' ug/l
1521 4-l.lethyt -2-pentanone
5' ug/t
3520 2-Hexanone7. ug/t352? fetrachtoroethene'l ' ugll35?3 1, 1,2,2'Ietrachtoroethane2. ug/t
35?4 TotueneZ. ug/t
3525 Chtorobenzene
1 ' uslt
3526 Ethytbenzene?' us/t
3528 Styrene1. ug/l3529 xytene (totaL)
1. ug/t
5780 trans-,l,2-DichIocoethene2. ug/t
6268 cis-1,2-DichIoroetheneZ. us/ t
!tsMS }ISO APO
LCS
LCS DUP
ICS LCS LII{ITSRPD LOU HIGH
x.D.
N.9.
il.9.
[.9.
N.D.
N.D.
N.9.
N.D.
N.D.
N.D.
N.D.
N.!.
71 90
65 93
6? 9s
106 105
72 94
1C5 1 05
't 01 't 01
110 109
1C2 10?
108 1C8
i1L 99
]06 .,02
2\
43
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0
2
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Lan(J5ter Laboralo(es
2425 l.lew Holiand Pike
PC Box 12425
Lancasier. PA i7 605-2425
7 1i -556-2300 Fax 117 -65a'268:
rE.
?*oF5ee re'/erse srde for erpiaral cn oi 5/rbolt and abbreniatrons 2216 Rev 5iO1/95
I
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(iI)La ncaster Laboratories
A division of Thermo Analytical lnc.
QUALITY CONTROL R.EPORT
Pa-qe: 6 of
SURRCGATE LIHITS
LCU HIGH
LLI sample No. 2538330Trip Btank Uater Sampte
llercutes: Bacchus Pond
4592 TcL votatites by 8240 - Uater
SURROGAIE SUHI'IARY
TRIAL ID SURROGATE RECOVERY Z
d4 .1 , 2 -DCA 98i8-totuene 1023rB 91
1l
II
1I
1l
76
8B
36
114
'l 10
115
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MEMBEFl
fa@i-n
Lan(aster Laboralofles
2425 New Holland Prke
PO gox 12425
Lancastel PA 176C5-2{25
1 17 -556-2200 ? ax 1 17 -656-2681 O"u.Ur.,rnu d}
I Group No. 52277
I xercutes, Incorporated
See rever:e srde lor e.iplanatron oi;/r:or: and abbre,rrtrons 22l,6
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1644
1646
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1649
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1653
165r,
1655
':658
1661
1666
i672
6935
6916
0.159
1??5
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4689
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d-t11
,1
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3.1
?.3
0 .4r.
0. 3J'a.i7
0.328
see Page
mg/ k9
xlg/k-o
m9/k9
ns/\g
mg/i9
m9/i9
nrg/ <9
ng/ <g
mg/'(-q
n9/ k9
n9/<g
mg/ <9
n9/ <!
mg/ (9
ne/kg
ne/<s
ngl kg
See Page
See 2age
See Page
LLI sample No. ES 2538087cottecred: 6/26/96 at 17:10 by BR
Suhnitted: 6/25/96 Reported: 8/ 6/96Discard; 9/ 6/96
CU-1 JUo 6rab SoiI Sample
Heccutes: Bacchus Pond
S l JUD SDG#: HBP02-08
A}IALYSIS IIAME
TCL Votatites by 8240
ThaLtiun
Aluninm
Ant irnony
Bar i um
Beryt L i ern
Cadmi w
Chromi w
Copper
I ron
Lead
,i! an9 anes e
rtickeI
Si Iver
ztnc
Arsenic TR
Setenium TR
l.lercury
TcL Pesticides in SoL ids
TCL St/646 Semivotatl tes Soi L
TCL SU846 Semivotari Ies/soi I
Account No: C6716
Hercutes, lncorporated - DE
Envi rorrnental Af f a i fs
Ui lmingron DE 19894
A Thermo Analytical Laboratory Page;
P.0.
Ret.
Respec!IuI Ly Subtrri tteC
Rc-irona Y. Layman, Group r-eacer
ICP Fe!als/Leacnates
'! of 14
AS RECEIVED
r::::t::f:::j:i:ir::ri::::::1:::::::::::::r,:: tlETHO0
iiliji:.::r,r,rr SlsUrrsr:.,,i.:,. DETECT : 0rl L Il"l I T Ull I Ts
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HercuLes, Incorporated
ERI'l - Rocky Mountain
Quest i ons? Contact yotrr C L i ent Servi ces Represen!a: i ve
Rachel i-. Kreailrcr at (7")T) 556-2iIJ0
15:36:43 D 0002 23 REP 12b136 -\??7'39310 25.00 00138100 AsR000
Lancaster Laboratofles
2425 New Holland Prke
PO Bor 12425
idn.aster PA 17605-:J.U,q
711-656-23AA Fa\ 717 'l:c-1631
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lllo Rs. ,r.n-* iaJ
A Thermo Analytical Laboratory
2538087
by 8R
.8/ 6/96
i Account No: 057'16
I Hercutes, lncorporated
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i iJitmington 0E 191194
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LLI Samp1e No. ES
Cot Iected: 6126/96 at 17:'10
Subrni tted: 6/28/96 Reported:Discard: 9/ 6/96
CU-'l JUD Grab SoiI Sampte
Hercutes: Bacchus Pond
S1JUO SDG#: HBP02-08
CATIIO. ANALYSIS IIAME
TcL vot at i t es by 8240
343/+ Ch torornethane3435 Eromomerhane3,.36 Vinyt ChtoIide3437 chtoroethane3140 YethyIene chtoride1071 Acetone4076 Carbon Disutfide
'1 180 1 ,1 -D i ch toroethene
344?'1,1'Dichtoroethane31t-4 Ch Ioroform3445 1,2'0ichtoroethane4085 2-Butanone3446 'l ,1,'1 -TrichLoroethane3t,/.7 Carbon fetrachloride4091 vinyI Acetare3418 Brornodi ch Loromethane3450 1,2-DichtoroproPane3451 cis-1,3-DichIoroProPene1181 Trichtoroethene
31,52 Dibromochtorotnethane3453 1,1,2'TrichLoroethane
1 1 82 Benzene3151 trans-1,3-DichIocoProPene3\56 Eromoform4'103 1r'l,lethyt'2-pentanone
4107 2-Hexanone3457 TetrachLoroethene3419 1,1,2,2-TetrachLoroethane
1 185 Totuene
1 184 ch I orobenzene3458 Ethytbenzene4117 Styrene3155 xytene ( totat )6187 trans-'1,2-Dichtoroethene6277 cis-1,2-Dichtoroe!nene
(il)La ncaster Laboratories
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oues t i ons? Contac t
Rachet L. Kreanrer
your Ctient Services Representa:ive
ar (7'.7) 656-230'
Lancaster Ldboratofles
2425 New Holland Prke
PO Eox 12425
Lanc6;rer. PA I 7605- 212-s
717-650-2100 rar 717-c56-lE,l
Respecrfut Iy Su.mi tted
Itlichele llcclarin, B-A.
6roup -eeCar, GC/Ms Votati l.es
t-"7'-=.1,,..::":-,cari':--,'tl1rc(tisd..l;ilbrerat..s l:16 9e., iC/10/95 d:l
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lg,qcaste r Lab o ratoriese t nermo Analytical Laboratolt Page:3of 14
LLr sample No. ES 253g0g7Cottected: -6/26/96 ac 17:10 O, in-"-",
subnitted: 6/2g/96 Reported: g/ 6/96Drscard: 9/ 6/96
CtJ-1 JUO Grab Soit Sampte
flercutes: Bacchus pond
SIJUD SDG#: HBp0Z-08
rtccount l{o: C6716dercutes, .:ncc,-porated - DEEnviconmenrai AffairsUi tmington CE i9B9/.
AS RECEIVED
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CAT[o. AIALYSIs ilAilE
TCL pesticides in Sotids
1981 Atpha BHC198? Beta BHC1983 De( ta BHC
]i]9 cama 8Hc - Lindanett tV Heprach I or1220 Atdrin1984 Heprachtor Epoxide1989 EndosuLfan I''2?2 0ietdrin1985 DoE1223 Endrin1990 Endosutfan ll]986 oDO1991 Endosut fan Su[ fate1?21 Dor3017 Endrin Ketone'1859 Nerhoxych(or3025 Atpha ChLordane3026 Ganma Chlordane'1988 Toxaphene1992 Endrin Al.dehvde1993 PC8. I0161994 PCB-12211995 ?cB-123?1996 PCB-12121997 PCB-12481998 P$- 125t1999 PC8-1260
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Respeclful ly Subrni rted.renifer E. Hess, B.S.Gfoup,_eader pest jc icjes/pcgs
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2425 Ne, Holland prke
PO Box 12425
Lan(dsrer. pA I75tS_-1.i25
i ii -656-2lA0 F,rr 7t7.5ii-l€B ,!}till0/10/95 vat
MEMBEFI
(l)Lancaster Laboratories
A Thermo Analytical La borato ry
P.0.
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Page:
1l
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LLI sample No. ES 2538087cottected: 6/26/96 at 17:10 by 8R
Suhnitted: 6/28/96 Reported: 8/ 6/960iscard: 9/ 6/96
CU-1 JUD Grab Soit Sampte
Hercutes: Eacchus Pond
S1JUO SDG#: HBP02-03
CATI.IO. AIIALYSIS IIAI'IE
TCL su846 Semivolati Ies Soi t
1 185 phenot
3753 bis (2-chIoroethyt) ether'1186 2-chtorophenoI375t, 1,3-dichIorobenzene1187 1,4'dichtorobenzene3755 1,2'dichtorobenzene1590 2'nrethyIphenoL4691 2.2'-oxybis ('1'chl.oropropane)
1692 4-methytphenot1188 N-nitrosodi -n-propyIamine
3757 hexach Iocoethane3758 ni trobenzene3759 isophorone374o 2-ni trophenoI3717 2,4 -di methytphenot
3760 bis (2'chloroethoxy) methane3718 2,4-dichtorophenol1189 1,2,4-trichtorobenzene3761 naphthatene4693 4-chtoroani t ine376? hexachtorobutadiene1190 4-chtoro-3-methylphenoI469t, 2-methytnaphthaLene3763 hexachIorocyctopentadiene3749 2,4,6-trichlorophenoIt+695 2,1,5-trichl,oroolenoI3764 2-chIoronaphthaIene4696 2-ni troani I ine3766 dimethyl phthatate3755 acenaphthytene
I
I Account No: 06716
i tlercuLes, Incorporated - DE
I Envi ronnenta i. Af f a i rs
i uitmincton DE 19894t'
I
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A9 RECEIVEO
,!.,!:1,:!.':!:n|irnlirl::'',.'''i :, l,lETli00:ji;;i::i..:;:,:':[g5Eart' 0ETEcTtcN !-rMtT u*rrs
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RacheI L. Kreailrer
Services Representativeat (71 7) 656-2300
MEMElERrrem
Lancaster Laboratorres
2425 New Holiaod P,ke
pO Box t2rr25
Lancasre( PA I ;605-:i:5
717-655-2i00 Far 7l;-656-258 i
Respectful !y submi rted
Chcrstine 14. RatcI i+f,
Group LeaCer, GCIMS
See ie,/Frse !oe icr e,9.;-3g,3n 9i :.tritr, aro aborivlattcns {:l
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Subni tted: 6/?8/96 Reported: 8/ 6/96Discard: 9/ 6/96
CU-l JUD Grab SoiI Sampte
Hercutes: Bacchus Pond
S1JUO SOG#: HBP02-08
CATlro. AltALYsts [Al'.tE
TCL SU846 Semivotati Les/Soi I
4697 3-ni troani I ine
1 191 acenaphthene3750 2,4-dinitrophenoI
'1 192 4-nitcophenoIL698 dibenzoiuran
1 193 2,4-dini trototuene4699 2,6-dinitrototuene3770 di ethyt phthaLate3769 4-chLorophenyt ptrenyI ether3768 ftuorene4700 4-ni troani t ine1701 4,5-dini tro-2-rnethytphenot3772 tt -ni tcosodi phenyI arni ne3TTj 4-bromophenyI phenyI ether3774 hexachtorobenzene
1 1 94 pentach I oropheno t3775 phenanrhrene3776 anthracene47OZ carbazote3777 di'n-butyl. phthatate3778 f Iuoranthene
1 1 95 pyrenc3780 butyI benzyI phthatare3783 3,j'-dichtocobenzidine3781 benzo (a) anthracene3784 bi s t2- ethylhexyt ) phthatate3782 chrysene3785 di -n-octyI phthatate1786 benzo (b) f',uoranthene3787 benzo (k) fluoranthene3788 benzo (a) py!'ene
3739 indeno (1,2,3-cd) pyrene3790 dibenz (a,h) anthracene3791 benzo (9hi) perylene
LLI sample No. ES 2538087cottecred: 6/?5/96 at 17:10 by 8R I n..ornt tto: 06716
Hercutes, lncorporaied - DE
r Envi ronmental, Af fai rs
I pilminston DE l9B9/.
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AS RECEIVED
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DETECTION LIMIT UNITS
A Thermo Analytical Laboratory Page: 5 of 1t+
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RacheI L. Kreamea
Ctient Services Represen!at ive
at (7'.7 ) 616-2311)
ffifiil
Lancasler Laboratores
2425 New Hoiland Prke
PO 8ox l2{25
Lan(aster PA 17505-2jr-:
717-656-2100 Fax :l; ;56-:aa
Respectful ty Suhni tted
Christine H. Rarctif+,
Group Leader, GC/MS
Se: .grerse srde ior !rc;anarron of svmbcls arrd abbrevr.rrrons
B.S.
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LABORATORY CHRONICLE
Page: 6 of 1tA Thermo Analytical Laboratory
LLI sampLe No. ES 2538087
cottected: 06/?6/96 at 17:10 by BR
Subori tted: 06/?8/96
I
I Account No: 06716j Hercutes, !ncorporated - DE
i Envi rorvrrenta i. Af f a i rs
i Ur inrington DE l9B9/+
I
CU-1 JUD Grab Soit Sampte
llercutes: Bacchus Pond
SlJUD SDG#: HBP02-08
CATHO ANALYSIS IJATTE
4593 TcL voLatites by 8240
'1525 That Iium
1643 Aturninunt
1644 Antimony'1646 BaritIIr
1647 Eeryttitrn
1649 cadmium
1651 Chroniunt1653 copper165t, I ron
1 655 Lead
1558 llanganese
1661 llicket
1666 S i tver167? Zioc
5708 SU SU846 ICP 0igest
6935 Arsenic TR
6916 SeIeniun TR
0159 ltercury5711 Su SU846 H9 Digest
0819 Sotid SampLe Pesticide Extract
1225 TCL Pesticides in Sot.ids
0381 BtlA Soit Extraction4688 Tc!- SU846 Semivotati Ies soi t
4689 TCL stJ846 Senrivotati tes/Soi I
0111 lloisture
A}IALYS I S
TRIAL DATE AND TIME AIIALYSTMETTIOD
su-846 82408
su-846 6010A
su-846 6010A
su-846 60'l0A
su-346 6010A
su-846 6010A
su-846 5010A
su-846 6010A
sr/-846 6010A
su-846 6010A
su-346 6010A
su-845 6010A
su-846 ,5010A
sH-846 6J10A
sr-846 6C10A
su-846 3C50A
su-846 6010A
su-846 60i0A
su-846 7471A
su-846 747iA Modi fied
srJ-846 3550A
su-845 8081
su-846 3550A
su-846 8?708
su-846 82708
EPA 160.3 (modified)
1 07/03/96 08',9
1 C7/13/96 13031 07/13/96 18081 07/13/96 18021 07/13/96 18031 ,J7/13/96 18081 07115/96 1803i 07,/13/96 1803
" c7/13/96 18CE'I 07l1i196 18LrB1 07/13/95 13051 07/13/96 1et)g1 A7/i3/96 18f;31 07/',3/96 lBOg1 07/13/96 18t)81 07/02/96 19311 D7/13/96 1A0g1 07/i7/96 092?
1. !l/t):,i?6 16131 07/0?/96 1506
1 07/01/96 14CCi 07/18/96 07'9
1 07/01/96 19301 C7/05/96 15531 07/C5/96 1553
1 07/02/e6 1520
Rlck S. Rodgers
Jotene I'l- Schietds
JoLene I'1. Schietds
Jo(ene ll. SchieLCs
Jotene iI. SchieLds
JoIene il. Schietcis
Jotene I'1. Schietds
JoLene iY. Schietds
..lotene i\|. Schie[ds
JoIene M. Sch'ields
Jotene M. Schietds
JoIene il. SchieIds
iotene M. SchietCs
JoLene ltl. Schietds
Jolene I'1. Schietcis0esi R. Earozza
JoLene H. SchietCs
Nina c. Hatr,er
Nclti S. ilarkaryan
Frances A. Dernorest
MattheH g. Kofroth
t'lichete D. Hack
Sherry Lynn Devtin
Joseph M. 6ambter
Joseph l'1. Gambter
NeeIay B. Mehta
reiii
Lancaster Laboratones
2425 New Holland Prke
PO Box 12J25
Lancasier PA 17505-2c29
717-556-:i00 Fax i17-o:o-253 !d?l22 '6 8ev I 0./10/95
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(iI)La ncaste r Laboratories
A Thermo Analytical Laboratory
QUALTTY CONTROL REPORT
Page: 7 of 14
LCS LII.IITS
LOU HIGH
LLI sample No. 25-18087CU-1 JUD Grab Soit Sampte
llercutes: Bacchus Pond
Sanpte
I.{D L
Samp t e
UNITS
DUP ils Lcs LcsRPO MS I'ISO RPD LCS DUP RPD
4593 TCL Votatites by 8240
BLANK
Batch: E95183lAB
N.D.
H.0.
N.D.
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I.D.
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N.0.
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N.0.
3434 Chtoromethane2. uq/ks
1435 Bromomethanel. ug/kS3436 Vinyt ChtorideZ. uglkg3437 Chtoroethane3. uglV.g
3440 Hethyl.ene ChIoride2- ug/ks4074 Acetone7. uslks
4076 Carbon Disutfide3. ug/kg
1'180 1,1 -DichIoroethene
z. ug/kg3442 1,1 -0ichtoroethane
1 - uglks
31.114 ChIoroform
1 . uglkg
3445 1,2-0ichtoroerhane2. uglkg
4085 2-Butanone7. uglkg34t+6 1,'l ,1-Tri ch toroethane1. ug/ks3447 Carbon TetrachIoride
1 - ug/ks4091 Vinyt Acetate3. ug/kg3448 Bromodi chtoromethane2. ug/1..93450 1,2-Dichtoropropane3. ug/ks
3t 5t cis-1,3-DichLoropropene
1 - ug/kg118'l Trichtoroethene
1 . ug/ks
J452 DibromochIoromethane
1 . ug,/ k9
3453 1,1,2-IrichLoroethane2. uglks
1 182 Benzene
1 . ul/k.s
3451 trans-1,5-0ichto.opropene
'1 . ug/kg
90 87
99 98
104 100
91 101
102 99
oo a0
1C2 100
107 '10 r
99 95
96 95
93 92
102 84
106 105
144 100
99 81
9? 90
98 98,
96 98
'! c9 107
90 87
9t, 92
93 96
93 92
3
2
5
10
)
11
2
6
4
2
1
20
1
J
2A
?.
0
2
?
I
2
2
1
95
95
102
B9
96
88
103
105
95
95
91
95
105
103
105
95
101
102
111
96
98
104
98
1 272
1 241
1 250
10 254
1 2?1
19 150
24 188
1 233
59 155
51 138
49 155
2? 167
52 16?
70 140
19 190
15 15s
1 ZO9
1 2?6
I I t)t
53 119
52 '150
37 151
17 183
retr
Lan(asler Laboratones
2425 New Holland Prke
PO 8or 12,125
Lan(a5iet PA 17605-2Ji :
71;-656-21A0 Fdx 7t1-ile )i2
lncorporated - DE
;: ::' :ro anai:o. ci ;vmior.. j,td dobrevtations
,*
))lr R.r,nr-rnrq, ?a*
(l}La ncaste r Laborato ries
A Thermo Analytical La borato ry
QUALITY CONTROL RNPORT
Page: 8 of 14
LCS LCS LCS LIiIITSDUP RPD LOU HIGH
Il
Il
1t
1l
"11
]T
il
tl
il
t
I
I
I
I
I
I
I
693
790
LLI sample No. 2538087
CU-1 JUo 6rab SoiI SamPte
[ercutes: Bacchus Pond
Group No. 522159
Hercutes, Incorporated - DE
Sarpte SamP[e
I.IDL UtI 1 TS
3456 Bromoform
'l . ug/ks
4'108 4-ltethyt-2-pentanone3. uglkg
4107 2'Hexanone3. us/ks
3457 TetrachIoroethene
l.u9lkg
3419 1, 1,2,2-Ietrachtoroethane
ug/kg
BLAIIK
lr.D.
N.D.
[.D .
}I.D.
lr.D.
ll.D.
N.D .
N.D .
N.0.
t{.0.
N.D.
N.D.
Batch:961845708003
N.D.
Barch:961845708003
il.D.
Batch : 961 845708003
It.D.
Batch:961845708003
N .0.
Barch:961845708C03
N.0.
Batch:961845708003
N.D.
Eatch:96',1845708003
N.D.
Batch;961845708C03
ri.0.
Batch:9618457080037.? J ms/kq
Eatch: 961845708003
N.D.
Batch:961845708003
[.0.
Eatch: 961845708003
N.0.
Earch: 961845708003
N.D -
1-
DUP
RPD
HS
RPOMS
oo
98
101
1 '15
'100
105
96
'107
99
105
101.
105
93
2027
9?
105
96
93
128
119
245?
96
'l 16
97
(1)
?1
(1)
9
0 (1)
0 (1)
0 (1)
0 (1)
1l
0 ('l )
11
0 (1)
(1)
MSD
83
91
90
110
94
103
96
104
92
103
98
101
89
16t+5 (?\
95
97
91
88
151
109
2139 (?)
90
109
91
97
12 91
4 115
797
1 101
097
3 108
7 101
2 106
6 101
4 102
696
979
279
7 100
598
799
1 102
6 102
189
791
591
696
798
45 169
50 124
5Z 140
61 148
46 157
t+7 '150
37 160
37 162
74 136
30 200
54 156
54 156
50 150
50 165
?1 ?99
70 131
21 177
25 174
54 141
57 145
61 142
53 142
69 135
55 146
50 147
1 '1Bi To I uene
1 , ug/k.s
1 1 84 Ch Iorobenzene
'I . u-olkg
3458 Ethytbenzene1. ug/kgl+117 Styrene
1 . uglkg
3355 xytene (totat)1. uS/kg
6187 trans-1,2-0ichtocoethene2- ug/kg
6277 cis-1,2-DichIonoethene2. ug./k9
1625 ThaL t ium13. ms/ks
1543 Atuminun8.7 ms/kg
1644 Antimony2.1 mg/ks
1646 Baciun?.1 mg/ks
1547 geryttiLdn
0.071 m9/ks
1649 Cadmiun0.'13 mg/kg
1651 Ch rom i urn
0. /.5 mg/ks
1653 Copper0.48 mg/kg
1654 I ron
3 .3 ms/ kg
'1655 Lead2.3 mg/kg
1658 t'langanese0.]2 mg/kq
166'l N ickeL0.44 mg/ks
1666 Si tver
0. /.3 ms/kg
(1) The resutt for one or
(2) The background resuIt
both detecminations ras less than five times
las more than four times the spike added.
't 02
the Loo.
Lancaster Laboratones
2425 New Holland Prke
PO Box 12425
L3ncasrer PA 17605-2r25
117-516-230A Fa\ rl;-d56'268r i';l
.l
5ee .e',,er,i . ::E .e1r : (Cialalrei 2' : i nb?e a.a i -Ot a I at tOaS :l j6 i.,, l0r10/95
I
I
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I
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I
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I
I
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I
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I
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QUALTTY CONTROL REPORT
Page: 9 of 14
i
I
I
, Group llo. 52229
I Hercutes. lnco.oorated - DEt'
I
l
l
Sanpte SampteI.IDL UII I TS
1672 Zinc0.38 mg/kg
6935 Arsenic TR0.24 mg/kg
6936 Setenium TR0.17 ms/ks
0159 Mercury0.028 ms/ks
1225 lCL Pesticides in Sotids
1981 Atpha BHC5. u9/k91982 Bera BHc3. uglks1983 Detta 8Hc1. us/kg
1218 Ganma BHC - Lindane
'1 . uglkg
1219 tieptachtoc1. u9/k91220 Atdrin
1 . uglkg
1984 Heptachtor Epoxide5. us/kS1989 Endosul.fan I4. us/kg1222 Dietdrin1. us/kg'1985 D0E1. uslkg
1223 Endrin6. ug/kg
1990 Endosul fan I I9. ug/kS
19B6 000
3 . ug./kg1991 EMosut f an SuI f ate
1 0. u9lk9
12?1 DoT
1 . u9/k9
3017 Endrin Ketone5. us/ks
1859 t'tethoxychtor40. ug/ks
3025 Atpha Chlordane
L - us/ks3026 Garma Chtordane1. ug,/kg
0 (1) 108 98
0 (1) 91 9?
0(1) 9? 9t
0(1) 92 92
MS
RPO
6
0
1
0
DUPRPD MS MSO
LCS LCS
LCS DUP RPO
LCS LI[IITSLOU HI6H
54 119
49 149
52 149
26 157
92
93
79
69
76
73
70
7?
71
79
79
87
77
82
81
69
79
47
81
73
I
a<
89
35
88
86
92
88
95
9lt
05
9l
95
01
7B
97
57
95
89
zt
l6
19
20
19
19
18
t6
18
tt
18
19
15
18
12
20
19
15
20
76
a)
76
70
B5
81
89
88
98
87
s3
94
B3
90
58
B1
B1
65 127
50 137
67 120
T3 120
69 120
67 1?0
60 120
60 120
79 120
7? 1?O
58 126
62 120
7? 123
62 120
61 17-1
75 125
57 141
75 125
75 125
('l) The result for one or both determinations xas Iess rhan flve times the L00.
Lancaster Laboratofles
M E M B E R 2425NewHollandPrke
t'!D
"., ,Ol:C,SS ?Gi
(I)Lancaste r Laboratories
A Thermo Analytical Laboratory
LLr Samp]e No. 2538087
Cl,- l JUo Grab Soi L Sampte
Hercutes: Eacchus Pond
BLAIIK
Batch:9618457080030.80 J nrg/ks
Eatch:961845708003
N.0.
Eatch:961845708003
N.D.
Eatch: 96184571',l002
N.D.
Eatch:9618301ofA
N.0.
rl.D.
[-D.
[.9.
N.9.
N.9.
x.0.
N.0.
N.D.
N.9.
N.D.
N.D.
N.0.
N.D.
N.0.
N.D.
N.0.
il.0.
N,D.
rl
DUP MS LCS LCS
RPD MS HSD RPD LCS OUP RPO
QUALITY CONTROL REPORT
Page: I0 of 14
LCS LIMITS
IOIJ H I GiI
'lr
1l
lt
ll
ll
il
I
d:i
Sampte Sampter,tot u[ I TS
-1988 Toxaphene1,000. ug/ks
1992 Endrin Atdehyde10. ug/kg
1993 PCB-101630. ug/ks
1994 ?CB-12?130. uslkg
1995 PcB-123250. ug/ks
1996 PCS-124250. uslkq
1997 PCS-124840. ug/ks
1998 PCB'125/.30. ug/kg
1999 PC8-126030. us/ks
57
4688 TcL SU846 Semivolatites soit Eatch:96183518026
1 185 phenoI33. ug/kg
3753 bis (2-chIoroethy[ ) ether
67. uglks
1 186 2 -ch Iorophenot13. us/kg
3754 1,5-dichIorobenzene51. ug/kg
1187 1.4-dichtot'obenzene33. ug/ks
3755 1,2-dichlorobenzene33. u9/k9
4690 2-methytphenot67. ug/ks
4691 2,2' -oxybi s (1 -chtoropropane)
1 00. uslkg
469? 4-methytphenoI
1 00. ug/ks
'l 188 fl'ni trosodi -n-propytamine
67 - ug/kg
3757 hexach t oroethane67. us/ks
3758 ni trobenzene33. uslkg
3759 isophorone67. ug/kg
3746 ?-nitrophenot
67.
il
(il)La ncaster Laborato ries
A Thermo Analytical Laboratory
LLI sampte No. 2538087
CU-1 JUo Grab soiI Sampte
Hercutes: Bacchus Pond
BLAIIK
|l .0.
l,t.D.
[.0.
N .D.
ll.D.
[.0.
N -0.
N.0.
N.D.
ilI orouo tto. 5227J9 I
I Hencutes, lncorporated - DE I
72 82
75 84
69 78
75 79
72 77
69 80
6? 70
84 s7
7t, 81
75 83
T7 83
83 92
74 82
il
,l
I
I
I
T
I
T
I
5 117.
12 158
23 134
1 172
z0 124
32 129
t+6 123
36 166
5 152
1 230
40 111
35 180
21 196
29 182
Lancaster Labordto0e5
2425 New Holland Prke
PO Box 12J25
Lancasrea PA i750!'l.l2-r
717456'1100 irr lll-ii5o-16.6 I
'11 77
11 76
12 73
576
576
674
15 71
11 6?
1t 90
t) ( /
10 80
778
10 87
976
MEMBEFl
, ar) ilti'i1,,i.1 Irons 2ilrr qe: l0/lC,'95
14
I
I
I
I
La ncaste r Labo ratories
A Thermo Analytical Labbratory
QI-IALTTY CONTROL REPORT
L I ]"II TS
HIGH
LLr sample No. 2538087
CU-1 JUD Grab SoiI Sampte
Hercutes: Bacchus Pond
l
IjGroup l,lo-
I Hercutes,
I
522739
I ncorporated
I
I
I
I
I
I
T
I
t
I
T
I
I
I
Sanpte Samptel.lDL UHITS
3747 ?,4-dinethytphenot67. uslks
3760 bis (2-chtoroethoxy),nethane53. ug/ks3748 2,4-dich Lorophenol.33. uslkg1189 1,2,4-trichLorobenzene33. ug/ks
3761 naphthatene33. uslkg
4693 4-chloroani I ine'100. uglks3762 hexachtorobutadiene67. ug/ks
1 190 4-chtoro-3-methytphenot67. us/ks
4694 2-methytnaphthatene31. ug./kg
3763 hexach Iococyctopentadi ene170. uS/kg3719 2,4,6-trichLorophenol67. uslks4695 2,4, 5-tcich LorophenoI67. ug/kg
3764 2-chloronaphthatene33. uglks4696 2-nitroanitine67. us/kg3755 dimethyt phrhatate33. u9/k9
3765 acenaphthytene33. us/kg
4697 3-nitroanitine67. uglks1191 acenaph thene33. uslks
3750 2,4'dinitrophenoI
1 70. ug/ks1192 4-ni trophenoL
1 70. ug/ks
4698 dibenzofuran33. uslks
'I 193 2,4-dini trototuene67. uglkg
4699 2,6-dinirrototuene67. us/kg
fisI'lS0 RPD
DUPRPO MS
LCS rCS LCSLCS DUP RPO LOUBLANK
N.D.
r{.0.
N.D.
N.D.
N.9.
N.D.
N.D.
N.D.
N.D.
N.D.
il.0.
N.D.
t{.0.
N.D.
N.D.
N.D.
48 57
73 81
71 31
n82
73 77
14 '15
80 87
75 86
711 82
17 16
81 90
80 89
79 85
72 78
79 87
36 40
71. 78
59 55
73 77
74 80
82 39
81 89
17
11
IJ
6
5
5
9
13
10
7
11
'10
8
I
10
o
41
77
78
75
43
81
82
6?
82
A)
79
75
an
3? 119
33 184
39 135
44 14?
)1 tz?
17 116
?4 116
22 117
28 123
1 '100
37 144
39 151
60 118
53 143
1 112
33 145
4689 TCL SUB46 Semi vot at i Les/Soi t Batch: 95'183S18026
[.0.
N.D.
N.0.
N.D.
N.D.
N.D.
N.D.
t0
9
8
6
I
7
10
56
73
6i
75
76
90
B5
{ tq)
47 1{.5
1 191
1 13?*
?8 131
39 139
50 't 53
MEMBERyreTs
Lancasler Laboratofles
2425 New Holldnd Prke
PO Box 12425
Ldncasret PA 176C5-2-1i :
7r7-555-2i00 iax 7il-o:6.liJ - ?rt\ a. a rbbr? rrat,ons l2l6 R,". lCli0l95
ancaster Laboratories
A Th ermo Ana lyti ca I La bo rato ry
QT-'ALITY CONTROL REPORT
Page: 1? of 14
LCS
83
B4
79
76
66
73
80
82
63
7A
86
91
95
68
80
103
B5
103
BO
85
to
82
LCS LCS LII'IITS
RPO LOU HIGiI
1l
1tLLr sarnple No. 2538087
CU-1 JUD Grab SoiI Sampte
HercuIes: Bacchus Pond
I
!
IlGrouo tlo.
I Hercul.es.
I
I
I
I
522739
lncorporated - 0E
MS t!s0
79 38
79 87
74 30
59 62
66 72
7t, s4
81 92
83 91
74 76
75 83
7t+ 81
74 79
80 90
7i 80
8t 92
86 97
55 58
77 83
93 103
3Z 89
81 92
73 80
77 85
71 81
E2 89
1 114
25 158
59 121
58 122
1 181
38 147
53 1?7
1 152
14 176
54 120
27 133
35 133
1 118
?6 137
5? 115
1 152
1 262
JJ Iq)
8 158
17 168
4 146
z1 159
11 163
17 161
1 171 i
2216 5e! ,.rr.r* dl L'
il
SanpI e
I'IDL
SanpL e
UNITS
MS
RPD
10
10
7
4
9
12
'13
IJ
2
'10
9
7
1l
9
10
1?
5
I
8
13
10
10
10
8
ELAI{K
T.D .
N.D.
N. D.
[ .0.
N.D.
N.D.
N.0.
ll.D.
N.0.
N.D.
N.D.
N -0.
N.D.
N.D.
iI.0.
N.0.
[.0.
il.D.
N.0.
N.0.
N.D.
N.D.
fl.0.
N.D.
il.0.
LCS
DUP
DUP
RP3 1l
il3n0 diethyt phthatate
67.uglkg
3769 4-chtorophenyt phenyt ether67. ug/ks
3768 ftuorene33. ug/kst7O0 4-nitroanitine
'100 . ug/kg
1701 4,6-dini tro-2-methytphenoI
170 .uslkg
3T7Z tl-ni trosodiphenYtamine
67.ug,/ kg
3773 4'bromophenyl phenyI ether
100. ue/kg
3774 hexachIorobenzene100. uslks
1194 pentachtorophenot
170.u9/ kg3Tl5 phenanthrene33. ug/kg
3776 anthnacene33. us/kg
47OZ carbazote33- ug/kg
3n7 di-n-butyl. phthalate33. ug/kg
3ng ftuoranthene33. us/kg
1 195 pyrefle67. ug/kg
3780 butyt benzyt phthatate
67. us/kg
3783 3,3''dichl.orobenzidine
130 .ug/ks
3781 benzo (a) anthracene33. ug/kg
3784 bis (2-ethythexyt) phthaIate
67. uglkg
3782 chrysene33. ug/kg
3785 di'n-octyt phthaIate67. us/ks
3786 benzo (b) ftuoranthene
67 - ug/kg
3787 ber,zo (k) ftuoranthene110. ug/ks
3788 benzo (a) Pyrene67. us/kg
3789 iMeno (1,2,3-cd) pyrene
ug/ kg
,l
I
I
I
T
I
I
I
Lan(aster Laboralofies
2425 New Hoiland Prke
PO 8ox 12425
Lan(asreL PA 11 |at-2J)a
7li-656-2300 Far il7'5!6-163 I
il
MEMBEFl
67.
i-o.lbbrevrailoos
I
I
I
I
I
I
I
I
I
I
I
I
I
I
t
I
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I
QUALITY CONTROL REPORT
Page: 13 of 1t
Sarpt e
IIDL
3790 dibenz
67.
3791 benzo
67.
01'11 l{oisture
0 .06
Samp t e
UII I TS
(a,h) anthracene
uslk9
ighi ) perytene
u9./ k9
Z by pt.
LCS LCS
LCS DUP RPD
DUP MSRPO MS MSD RPD
LCS LII'I I TS
LOU HIGH
1 ?27
1 219
1 00 101
BLANK
N.D.
N.D.
Eatch : 95184C3 1 6320003A
o?
79
9
8
83
75
100
91
86
1C0
MEMBER
EGTTil e!+?.i
(I}Lancaster Laboratories
A Thermo Analytical Laboratory
LLr sample No. 2538087
CU-1 JUo Grab Soil Sampte
Hercutes: Bacchus Pond
Ldncasier Laboratores
2425 lJev/ Holland Prke
PC Bo, :242t
Lancasiec PA I 7505.:tr, l
7l:--655-DCt) i,:r -1 :l: lil
I croup uo.
Hercut es,
I
I
L
522739
Incorporated - 0E
t d.d .ltlD.:.., itro,,,i ;e. 'C/lO/?5
A Thermo Analytical La bo rato ry
LLI Sample No. 2538087
Cu-1 JUD Grab Soit SampLe
Hercutes: Bacchus Pond
SURR06ATE SUMI'IARY
TRIAL ID SURROGATE RECOVERY Z
1225 ICL Pesticides in Sotids TCX 66DC8 83
4593 TCL Votatites by 8240 d4-1,2'DCA 90C8-totuene 99
8FB 90
4688 TCL SU846 Semivo(atites Soi[ Phenol-d6 792-Fipheno[ 762,4,6-TEP 93
/1689 ICL Su846 semivotati tes/Soi t Nitrobz-d5 91
2 - Fbi PhnYt 79TphenyLdl4 65
(iI)La ncaste r Laborato ries
Lancaster Laboratore5
2425 New Holland Pike
PO Box 12-125
LJn(dslei PA 1 7505-1tr25
717-556-llOC tax i :i -61c-ii?1
rl
]l
Page: '14 of 14 "ll
ll
SURROGATE L IITII TS
LOU HIGH
50 '120
'll
il
120
121
11771 121
ii il1 .l
19 122
50
70
31
il
?3
30
18
't20
'I 15
141 ,l
I
il
,l
I
I
I
I
I
d:i
QUALITY CONTROL RXPORT
see ,g,.,e.se 5lo€ ior e:rpianat,cr oi;ymbol5 .i.i abori',,ratrons 22',6 ".t'. Ci)A/9i
t
t
I
I
I
I
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I
I
I
I
I
I
I
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I
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I
I
(I)La ncaste r Laboratories
LLr sample No. ES 2538090Cottected: 6/26/96 at 16:20 by 8R
Suboritted: 6/28/96 Reporred: 81 6/960iscard: 9l 6/96
CU-Z JUD Grab Soi I Sampte
Hercules: Bacchus Pond
S2JUD SDG#: HBP02'1 1
cAT .:::ir:: :ll0. AIIALYSIS IIAME ,.,,,:,:i,:',
1 CoPY IO Hercutes, lncocporated
1 CoPY IO El(t't - Rocky Hountain
I Account llo: 05716
. Hercutes, lncorporated - DE
i Envr ronmenral. Af fai rs
i lJr tmington 0E 19894
1
A Thermo Analytical Laboratory Pag e:
P.0.
Ret.
DRY UEIGHT
::.:i::::::::ii::::::::i::i:i:.:::r..::::::: :: METHoD
ri:*ll;i:tii:l.lfsut tli:,::iii DETEcT I otl L I L I T
AS RECEIVEO
1of 14
18.
ta.
?.8
a.o
0 .095
0.17
0. 60
0.6/,
4.1.
J.l
0.15
0. 59
0. 58
0.51
0.32
0.23
0. 038
,E
,orrorr, ?ai
i(Ebfl I i
I!ET HOD
DETECTI OI'I LII.tIT UIIIIS
459J TCL Votati Les by B2(0 See page
1625 Thattiun :::r::ltitt:t1::::i:. ,..,tt.r. 13. nrq/kg1643 Alurninun i.iti.iili,r:r:tr:r5,,7.c9. -. r' 3.6 mglkg164t, Antimony ,r,ii:,ii;.,,i.,.,.,,'.,.',1{,r. . 2.1 mglkg1646 Earium 'i:,'.i ,. ': (1:,:5 :, 2.1 nEl<g1617 EerytLir..rn i:.:.:i'..,,.,, ,,,O,ta't . 0.C70 mg/<g
161,9 Cadnriun ...,, , 0-?: ) i.1? mg/kg'1651 Chromiun ......:. u.? C.45 ltg/<g1651 Copper ., ' ,' , .:' 2t ."' C . (g mg/ <91651 I ron ':,. .. . ,5,:+1. 3.2 nq/ tg1655 Lead i,,:... ... ., 10.1 , 2;3 mg/ <s1658 Manganese ;1.;,,;';';; ;;;.';,.1;.;;50,5 . D.l'l mg,/kg1661 Nickel ,,,.,..:,. ;i.6.i C.44 m9/<91666 Si lver :,:,..' . . iJ.). C.45 ng/<g1672 Zinc ,,::t,' , ,: ;!7,! . ,-1.13 mg/kg6935 Arsenic TR ,i',.,: q.' C.3r, ng/<g6936 Seteniun IR :,,i,. ,,9.1-9 :.. 1 O-17 ng/kg0159 ltlercury ,',.,,.,::. ,, ',,...., Lt . C53 , J 0. C23 mq/k,J1?25 TCL Pesticides in Solids S.e Page4638 TCL SU846 Semivolatites Soil see Faoe4689 TCL 5U846 Semivolarites/Soit see cale0111 Moisture ::::.i:i:::. :' .25.C 0.e6 Z by cr.
"l'loisturerr repcesents the toss in r.reight of the sanrpLe after oven drying at
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ATIII : l4r. Joseph (etLer
ATTN: i"tr - grenr RoLrinson
ouesticns? Contact your CLient Services Representative
Rache!. L. (rearner at (717 ) 65o-:i30C
16:22:43 D 0002 23 REP 12cL3b 5?2fi9310 25.00 C01l84L)0
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Respectf ul. !.y Submitred
I?anrona V. Lay$an, Group LeaCer
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7ikilfxil
Lancaster Laborator!es
2425 New Holland Prke
PO 8or 12425
Lancaster PA 1 i 603-2 !,) <.
717-556-2100 Fax 71t ;:1o-25at 5ee :ere..,e ;rde for trolanatroo oi :ynrbols ano abbrevrattons 2216 Rev
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A Thermo Analytical Laboratory
LLI sample No. ES 253E090Cottected: 6/26/96 at 16:20 by BR
Sutxnitted: 6/?3/96 RepoFted: 8/ 6/96Discard: 9/ 6/96
CU-2 JUo Grab SoiI Sampte
Hercutes: Bacchus Pond
s2JUD SOG#: ltBPOZ- 1 1
AIIALYS I S }IAIIIE
Votatiles by 8240
: Account lto: 06716j uercul.es, Inccrporated
i Envi ronmenrai rffai rs
i uitmington cE I9894
II
Page:2ot 14
DRY UE!GHT
ii.:r,iiiii:r.ii:,i!,i:i,tri:iii;!,iii':il;i:,,t, METHoo
:Iiii:ii::::ili::i$gg!1t-I.F:i::,iii 0 ETEcr I otl L I M I 1
3431 Ch I orornethane3L35 Eromomethane3i,36 Vinyt Chlor ide
3437 Chtoroethane3440 rernytena chIoride1071 Acetone1076 carbon Disutfide1180 1,1'0ichtoroetherre31.42 1,'l-DichLoroet.,rane3!41 Ch I ot-of orm3445 1,2'0ichtoroethane4085 2-Butanone3446 i,'l,i-Trichtoroethane3147 carbon Tetraciltoride4091 VinyI Acetate3448 BromodichLofomethane3450 1,2-DichloroProPane3154 cis-1,j-Crichioropropene'1181 Trichtocoethene3t52 Dibromochlorofielhane3153 I ,1 ,2-Tri chIoroethane
1 182 Benzene3151 rrans'1 ,3-D i ch I oropropene
3156 Eromoform4103 4-Methyl'2-oentanone4107 2-Hexanone
3157'letrachLo[oerhene3419 1,1,2,?-letrachIoroethane
1 1 8l Totuene1184 Chtorobenzene3455 Ethytbenzene4117 Styrene3i55 YyLene (total)
6'187 trans-,l,2-0ichloroerhene6277 cis-1,2-DichLorocthene
AS RECEIVED
:iii::.j:;jf,i::::::f::::*::::::::::rr:::.:r :: M E T H OD
,i;ii;i,ii:i:i:,1E iq.u, 1s,,,,,,:t D ETEcr : cN L t H I T uN I TS
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Ouestions? Contact your Cl ient
RacheL L- Kreamer
Servi ces Representa! i ve
at (7'7\ 656'Z3,JD
Lancaster Laboratoftes
2425 New holland Prke
PO Box l2J:5
Lancaste( 9A 1 7605-212:
lr7-656-2100 Far 7i7-5!o-2531
I
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Respecifrl ly SuLlmi tted
tiche',e vc!l.arin, 8.A.
Croup -eader, 6C/l4S Volati les
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A Thermo Analytical Laboratory
LLI sample No. ES 2538090Cottected: 6/?6/96 at 16:20 by 9R
subnitted: 6/28/96 Reported: 81 6/960iscard: 9/ 6/96
CU-z JUD Grab SoiI Sampte
Hercu(es: Eacchus Pond
S2JUD SDG#: tl8P02-11
Account llo: 067-'6
i iiercu(es, lnccroorated - DEI Enviaornlenlai. Af ia irs
i !j lmington DE 1989/+
A9 RECEIVEO
I.IET HCD
DETECTICN LITIT UIIIIS
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AIIALYSIS IIAME
DRY UEIGI.IT
i:1i::i1..jii::i::i::i:i::::iji:i:::i::,:::::::::::1:i::i: llET'r100
i:iiii iiiiiliiEsuil si:iii,,'i D ETEc : r cN L I I't I T
TCL Pesticides in Solicls
1981 Atpha BHc1982 Beta 8HC1983 Detra 8Hc1218 Garmla BHC - l-indane1219 Heptach I or1220 Atdriri1984 Heptachlor Epoxide1989 Endosu[ fan I1??2 Dietdrrn'1985 00E1?23 Endrin1990 Endosut fan I I198,6 DDO'1991 EndosuI fan Sul fate1221 DoT3017 Endrin Ketone1859 t'lerhoxych Ior3025 Atpha Chlordane3C26 Garma Chtordane1988 Toxaphene1992 Endrin Al.dehyde'199t PC8-1016'199/+ PcB - t2211995 PcS-1232'1996 PCB - 1?121997 PCS-1?481998 PCS - 1?5t+1999 PCB -',l 260
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ouestions? Contact your CIient Se'evices RepreseatJ!ive
RacheL L. Kreamer ar (7'7) 6;6-2i0C
Lancasler Laboratores
2425 New Hoiland Prke
PO 8oi 12-125
Lanc;srer PA I 76C5-l-;.15
717-555-;iCO F,r^ :'::i6 l.'.6
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Respecrful Ly Subrni :tedieni+er E' lless' B'S'
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MEMBEFI
LLI sample No. Es 2538090Cottectedi 6/26/96 at 16:20 by BR
Suunitted: 6/2A/96 Repocted: 8/ 6/96Discard: 9/ 6/96
CU-2 JUD 6rab Soi t Sampte
Hercutes: Bacchus Pond
S2JUD SDG#: HBP02-11
CAT}IO. ANALYSIS NAME
TcL sU846 Semivotati tes Soi I
1185 phenot
3713 bis (2-chtocoelhyt) ether
1 186 2-chlorophenoi3754 1,3-dichIorobenzene1187 1,4-dichtorobenzene3755 1,2 -dich Ioroben:ene4690 2-rnethytphenoL1691 2,2'-oxybis (1-chloropropane)
l+692 4-rnethyIphenoI1188 N-nitrosodi-n-prooytamine3757 hexachloroethane3758 ni trobenzenei759 i soplrorone3746 2-ni trophenot3747 2,4-dirnethytohenot3760 bis (2-chtoroethoxy) methane37tB 2,4'dichlorophenoL1139 1,2,4-trichLorobenzene3761 naphtha I ene
t 693 4-chtoroani I ine376? hexach Loroburadi ene'1190 4-chtoro-3-methytphenot4694 2-rnethytnaphihalene3763 hexach lorocyc l.openradi ene3749 2,4,5-trichtorophenoI4595 2,4,5-trichi.oroohenot3764 2-chLoronaohthaIene4696 2-ni troani I ine3766 dimethyt phthalare3765 acenaphrhytene
ouest i ons? Corltacl
Rachel. L. (reailrer
Account tlo: C67'16
tlercutes, lncorporated ' DE
Envi rornrenta i. Af ia i rs
lli tmingron DE ,'9894
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AS RECEIVED
HE T H09
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DRY UE I 6IIT
MF IHOO
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your Ct ient Services ReDresentative
at (7'7) 556-23C0
Lancaster Laboratotes
2425 New Holland Prke
PO 8ox 12425
LJncasier. PA I 7605-1125
717-656-2ioo Far ;ll-5a6-i531
Respectful Iy Subni tted
Christrne U. natcliff, B-S.
G(.oup :eader, Cc,/Ms
5e: ,rterse i ae 'rl. ilulir;i aa ci lveoor, iafl iLcre'/ral,on5 .l:1 6
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(I)Lancaster Laboratories Page: 5 of 14A Thermo Analytical Laboratory
LLI sample No. ES 2538090Cottected: 6/26/96 at 16:20 by 8R
Suhnitted: 6/28/96 Reported: 8/ 6/96Discacd: 9l 6/96
CU-z JUD Grab Soi t Sampte
llercutes: Bacchus Pond
SAJUO SDG#: HBP02-11
CATIIO. AIIALYSIS IIAME
TCL SU846 Sernivotatj |.es/Soi I
4697 3-nitroanitine
1 191 acenaphthene3750 2,1-dinitrophenot1192 4-ni trophencl4698 dibenzofuran
1 193 2,4 -di ni trorotuene4699 2,6-dinitro(or-uene377A diethyt phrhaLare3769 4-chtorophenyt phenyt ether3763 f Iuorene
t 700 4-ni troani t ine4701 4,6-dini tro-2-rnethytphenoI3772 N'ni trosodipherrylomine3773 4-beomophenyI phenyI ether3774 hexachtocobenzene119/. pentachIoroonenol3775 phenanthrene
3n6 anthracene4707 carbazote3777 di -n-buryI phthatate3778 ftuoranthene
1 195 pyrene3780 buryt benzyl phthatate
l78l 3,3r -dichtorobenzidine
3781 benzo (a) anthracene3784 bis (2-ethyIhexy{.) phthaLate378? chrysene3785 di -n-octyI phthaIate3786 benzo (b) ft,uoranthene3787 benzo (k) fLuoranthene3738 benro (a) pyrene
3789 indeno (1,2,3-cd) pyrene3790 dibenz (a,h) anthracene3791 benzo (ghi) perytene
ouestions? Contact ycur
Rachet L. Kreafftef
Account No: 06716
llercutes, Incorporated
Envi ronmentai Affai rs
Ur Lmington DE 19894
AS RECEIVED
tqsuLTS . DETECT!Cr'l ttt"!tI U[lTS
DRY UEIGHT
..:.::r:j:::::::....I::i:.::::..:ii..:.. IIETHoO
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Cl. ien! Services Represen:ative
a.. (7'/) 556-21C0
RespecrfuI LY Subnri tted
Christine !4. RatcLifi,
G.oup Leader, GC/FS
iee.:re::! irCe.or ;rr:ianauoo oi r'lnf,ols ;.c :bbrevra(ror;
Lanca5ter Laboratofle:
2425 New Holland Prlir
PO 8or 12425
Ldncasier, PA I 75\15':i: a
717-656-2-z0O ia, -.- :
oe?--,!;l
B.S
2? 15 ?:. 'Ail1i ,4'-)
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(I)La ncaster, Laborato ries Page: 6 ol 14
'11
A Thermo Ana lytical Laboratory
LLI sanpl-e No. ES 2538090
cotlected: A6/?6/96 at 16:20 by BR
Suhritted: 06/28/96
CU-2 JUD Grab Soi I Sampte
Hercutes: Bacchus Pond
S2JUD SDG#: il8P02-11
CATI,IO AIIALYSI S I'IAME
4593 TCL Votati les by 8240
1 625 That t ium'1643 Atuminum'1544 Antimony
1 646 Bari unr'1047 Beryt tium
1 649 Cadnr i trr'1651 Chromium'1655 Copper
1654 I ron
1 655 Lead
1 658 trianganese'166'l Nicket
1666 Sitver
1672 Zinc
5708 SU Su846 ICP Digest
6935 Arseni c TR
6936 Setenium TR
0159 I'lercucy
5711 5U SU846 H9 Disest
Account llo: 06716
Hercutes, lncorporated - DE
Envi ronmental. Aff a i rs
Uitmington 0E 19894 1l
II
HETIIOD
su-846 82408
su-816 6010A
su-846 6010A
su-346 6010A
su-846 6010A
su-546 6010A
su-846 601CA
su-846 6010A
su-345 6C10A
su-846 6010A
su-546 6010A
su-846 6010A
su-s46 6C10A
su-84,5 6Cl0A
su-346 6010A
su-846 3t50A
s.r,l-8r,6 6010A
5U-846 6l lCA
s\t-846 7471 A
s'*-846 7471A Modified
AIIALYS I S
TRIAL OATE ANO TIftIE
1 07/03/96 1026
1 07/13/96 18231 07/1i/96 13?31, A7/13/96 18?31 C7/13/96 182:i 07/',3/96 18?31 07 /'t3/96 18?31 D7/..3/96',i323', c7/13/96 1e23., 07/13/96 1373\ 07/13/96 1B?31 07/13/96 1821": 07/13/96 1A231 C7 /1i/9o 18231 07/13/95 18231 07/02/96 193t', 07/13/96 18?31 C7/17/96 0935
1 07 /03/96 16t-11 07/0?/96 1506
1 07/01/96 14001 07/13/96 15>3
1 07t01/96 19301 A7/05/96 1827., 07/q5/95 1927
1 07/02/96 15ZA
ANALYST
Rick s. Rodgers
JoIene M. Schiel.is
JoLene tl. scirietcs
Jotene t'l. SchieLCs
Jotene M. Schietds
JoIene il- Sch'i etds
Jotene M. schiel.is
Jo(ene li. Schietcs
JoIene ]rl. SchieLcs
Jotene I'l- Sch ieLCs
Jotene I'1. Schiel.ds
iotene M. SchieIds
Jolane !l- Sch i etcs
JoLene ltl. Schielcis
..loLene Y. Schiel-ds
Desi R. Catozza
Jotene M. Schietds
Nrna c. HatLer
NetLi S. Markaryan
Frances A. Denrorest
llattheH U. Kof.oth
i,tichele D. l'lack
sherry Lynn Devl.in
Joseph i(. Gambter
Joseph l'!- Gambter
Heetay B. llehta
il
0819 Sotid Sampte Pesticide Extract sU-846 3550A
1225 TcL Pesticides in Solrds su-846 8131
0381 StlA Soi t Extraction sU-846 3550A
/.688 TCL SU845 SerrrivoIatites Soil. Sf,-546 82708
4689 TCL 5!,1846 SenrivoLati les/Soi L SU-346 82708
0111 t'loisture EPA'160.3 (modified)
Lancaster Laboratofles
2425 New Holland Prke
PO Box 12425
Lencaste( PA i 7505'irl:5
71/-656-2l00 tar ll7-655-268
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RevllriiD,'95 fil
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I"ABORATORY CHRONICLE
Sea.e./er5e :ide for :ro';ratron of 5vmbo,; ;1rd ;bi)revratron5 2lt6
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(I)Lancaste r Labo ratories
A Thermo Analytical Laboratory
QUALITY CONTROL REPORT
LCS LIMI TSLOU HIGH
147oi
LLI sample No. 2538090
CU-z JUD Grab Soit Sampte
Hercutes: Eacchus Pord
' 6roup llo- 52289
i Hercutes, :ncorporated - DE
i
I
Samp I e
HDL
Samp I e
UII I TS
LCS LCS
LCS OUP RPO
OUP I'IS
RPD MS ',1S0 RPo
4593 TcL Votatites by 8240
3l$1 Chlorom€thane?' ug/ks
1135 Sronpmethanel. ug/kS3436 vinyt chtoricie?' us/ks
3437 Chtoroethane3. ug/Y.g
3440 Methytene chl.ocideZ. ug/ks
1074 Acetone7. ug/kg4075 Carbon Disutfidel. us/ks'1'180'1, 1-DichtoroetheneZ- ug/kg
3442 1, 1 -Dichtoroethane
'l . ug/kg
3444 Chtoroform
'I . uglkg
3445 1,2-0ichtoroethane?. u9/k9
40BS 2-Butanone
7 - us/kg3446 1, 1,1-Trichtoroethane1. ug/kg
3447 Carbon Tetrachto{'ide1. us/kg
4091 Vi nyI Acetate5. ug/ kg
311+8 BromodichLoromethane2. ug/kg
3450 1,2-DichIoropropane3. us/ks
31,5t, cis-1,3-DichLoropropene
1 - ug/kg
11B1 Trichtoroethene1. us/kg3452 Dib.omochtoromethane1. ug/kg
3453 1, 1,2'Trichl.oroethane2- ug/kg
1 1 82 Benzene1. us/ks
3451 trans-'1,3'Dichtoropropene
I . ug/kg
BLANK
Batch : E96l 83'lAB
N .0.
N.D.
r{.0.
N.9.
?- J us/kg
N.D.
N.D.
I.D.
N.0.
N.9.
N.D.
N.0.
ti.0.
tl o.
x.D.
N.D.
N.0.
N.D.
N.0.
N.D.
N.D.
N.D.
1 ?72
1 241
1 250
J0 254
1 ??1
19 150
24 188
I ZJ5
59 155
51 138
49 155
?2 167
5? 162
70 140
19 190
35 155
1 209
1 2?6
71 157
53 149
5? 150
37 151
17 181
395
295
5 102
'10 B9
i96
'r 1 88
2 101
495
295
191
20 95
1 105
3 101
20 105
295
0 101
2 102
2 111
396
298
2 10t,
't 98
90 87
99 98
104 100
9r i01
102 99
83 78
ioz 100
1.C7 I01
99 95
96 95
93 92
102 8L
106 105
1C4 10o
99 31
9? ?0
98 98
96 99
109 107
90 87
91 92
98 90
93 92
Lanca5ter Laboratofle5
2425 New Holldnd Prke
PO 8or 12425
Lixc.r!re. PA r 76r-15-:-:.'5
7 1 7-655-2 100 F;x 7 I r -5:,o'.-'ri I
tB
n., rO.':OzeS L*
MEMBER
-:ol; J.d abt.p: a:rcns
ll
(l)La ncaste r Laborato ries
A Thermo Ana lytica I Laboratory
QUALITY CONTROL REPORT
Paqe: 8 of 14
LCS
93
90
91
115
97
101
97
108
101
106
10',I
102
96
79
79
100
98
99
102
'I 02
B9
9t,
94
96
9B
LCS LCS LCS L I I'I I TS
DUP RPD LOU H ! GH
ll
1lLLI samp]e No. 2538090
CU-Z JUo Grab Soi I Sampte
Nercules: Eacchus Pond
Gcoup No. 522139tiercutes, Incorporated ' DE 'trI
Sampt e
I'tDL
Sanp I e
UNITS
DUP
RPD
ils
RPD
6
7
ta
4
7
1
0
J
7
2
6
4
6
I
)
7
5
7
,1
6
4
7
5
6
7
ttsDMSBTANK
3456 Bromofocm
1 . uglkg N.D. 88 83
4108 4-ilethyt'2-pentanone3. uslkg N.o. 98 9 !
4107 2-Hexanone3. us/ks N.D. 101 90
3457 Tetrachl.oroethene
'I . ug/kg N.O. 115 110
3149 1,1,?,2-I etrachloroethane1. u9/k9 N.D. 100 94
1 183 Totuene1. uglkg N.c. 105 101
1 1 84 ch lorobenzene
1 . ug/ks N.D. 96 96
3458 Ethytbenzene
'I . u9/k9 N.D. 107 104
41 17 styrene1. rrg/ks ll.r. 99 92
3355 xytene (tota[ )1. us/ks N.D. 105 103
6'187 trans-1,2-Dichtoroethene2. ug/ks rl .D . '104 9e
..6?77 ci s'1,2-Di chl.ocoethene2. ug/ks N.D. 105 101
1625 Thattitln Eatch:961845708C0513. ms/ks N.D. (1) 93 89
1643 Atuminum Barch: 961845708C038.6 mg/ks N.D. ?1 ?!27 1645 (2)
'1644 Antirnony Batch: 961845708C032.1 mg/ks N.D. (1) 92 95
1646 Bariun Barch: 9618457080032.1 ms/ks li.D. 9 1C5 97
1647 EeryLtir.rn Batch:9618457080030.070 mg/kg N.0. 0 (i) 96 91
1649 Cadmitm Batch: 9518457080030.12 mg/kg N.D. 0 (1) 93 38
'1651 chromium Batch: 9518/+570BC030.45 ms/kg N.9. o (1) 123 131
1653 Copper Barch: 9618457080030.18 mg/kg N.D. 0 (1) 'l19 109
1654 I ron Batch : 96',1 8457080033.2 mg/kg 7.? ) ns/kg 13 2452 2139 (2)
1655 Lead Earch: 96',18457080032.3 mg/kg N.0. 0 (1) 96 90
1658 llanganese Eatch: 961845708C030.1i ms/kg N.D. 11 116 109
1661 flicket Earch:961845708C030.14 mg,/kg N.D. 0 (1) 9i 91
1666 S i Lver Batch: 9618457080030.(3 mglkg N.0. ('l ) 102 97
(1) The resutt for one or both determinations Has tess than five times the 100.(2) The background result cas more than four times the spike added.
Lancaster Laboratoles
2425 Nelv Holland Prke
PC 8ox 12425
Ldnci;iei. PA :75,15-2j25
7 1,7 -6"0- il]i rar 7l 7-65c'i6i i
45 169
50 124
52 140
64 148
46 157
17 150
37 160
37 162
74 136
30 200
)4 156
54 156
50 150
50 165
21 ?99
70 111
23 177
2b 174
54 141
57 11s
61 14?
s3 142
69 135
55 146
50 147
I
;216 ie,.,.rrr* d:'l
I
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MEMBEFIrffit3 '.ee ,e;e.s: ; :: -oa e toiaee-. a' ot :,i:r)cr, .lno abilrey(dtionS
LCS LCSLCS DUP RPD
DUP MSRPD MS MSD RPO
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(l}Lancaster Laboratories
QUALITY CONTROL REPORT
Page: 9 of t&A Thermo Analfiical Laboratory
LLI sarnple No. 2538090
CiJ-z JUD Grab SoiI Sampte
Hercutes: Bacchus Pond
Group No. 522139
Hercutes, IncorporateC - DE
Sanpte SampleI'rDt uillrs
16T2 Zinc0.18 taq/kg
6935 Arsenic TR0.24 mglkg
6936 Seteniun TR0.17 mg/kg
0159 ltercury
0 .028 m9/kS
B LANK
Eatch: 9618457080030.80 J mslks
Eatch:961845708003
N.0.
Eatch: 96'1845708001
N.D.
Batch: 96184571 ',1002
r,I .0.
Satch:96183C103A
0 (1) 1C8
0 (1) 91
0 (1) 92
0 (1) 9?
98
9?
94
9?
69 85
75 39
73 89
70 35
72 88
71 86
77 92
at
79 95
79 94
87 105
77 9l
82 95
84 101
69 78
79 97
47 57
81 95
71 89
Iess th6n flva times the 100.
6
0
1
0
9?
87
79
LCS Lll,ltTSLOU HI6H
5tr 149
19 119
52 119
26 157
65 1?7
50 137
67 120
73 1?O
69 120
67 120
60 120
60 120
79 120
72 120
68 126
62 '.120
72 123
62 120
61 121
75 125
57 141
75 125
75 125
1225 ICL Pesticides in Sotids
1981 Atpha BHC5. uS/kS
1982 Beta BHc3. ug/kg
1983 Detta 8Hc
'l . ugl kg
1218 Ganrna BHC - Lindane1. ug/kg
12'19 Heptachtor1. us/ks
1220 Atdrin1. ug/ks
1984 Heptachtor Epoxidei. ug/ks
1989 Endosutfan I4. ug/kg
1Z?2 DieIdrinL. ug./kg
1985 D0E1. uglks
1?23 Endrin6. ug/kg
1990 EndosuI fan I t9. ug/kg
1986 DDDl. ug/kg
199'l Endosutfan Sutfate'10. ug/kg
1221 Dor
'1 ' ug/kg
3017 Endrin Ketone5. ug./kg
1859 l,tethoxychtor40. ug/ kg
3025 Atpha Ch Iordane1. ug/kg
3026 Garrna Ch Lordane
'l . uglkg
(1) The result for one or both determinations uas
21
16
i9
20
19
19
18
16
aa
17
'18
19
15
'18
12
20
19
15
20
76
6Z
85
7A
a<
B1
89
B3
98
93
94
B3
90
58
B1
B1
Lancaster Laboralofles
2425 New Hoiland PrkP
PO Box 12425
Ldncas(ec 2A 1 7605'2.1: :
1\i-656-2300 td\,1 1..)',;,)a):a. leert.:r:::rr:'ti:,rlar];l:o.or;,:.corSanda:ocrevrdllont
t]D
,ar,o,r, ?ai
MEMBER
ll
(I)La ncaste r Laborato ries
A Thermo Ana lytical Laboratory
QLTALITY CONTROL REPORT
Paqe: 10 of
'll
LCS LIi,IITSLou x i cir
5 112
12 158
23 134
1 17?
20 124
3Z 129
46 tl5
36 166
5 152
1 230
t+O 113
35 180
21 196
29 182
I
2216 Re'r ,.rr* d: i
Il
Il
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12357
LCS
RPD
LLI sample No. 2538090
CU-z JUo Grab SoiI Sampte
Hercules: Eacchus Pond
I
I
i croup uo. 522259
I tlercutes, lncorporated - 0E
I
Sanp I e
r,tDt
Sampt e
UN ITS
1988 Toxaphene
1 , 000. uglks
1992 Endrin Atdehyde10. ug/kg
1993 PC8-101630. ug/kg
1994 PCg-12?130. tts/k s1995 PCS-121250. uS./kg
1996 PCS-1U+250. ug/kg
1997 PCB-124840. ug/kg
1998 PCB-125450. ug/kg
1999 PCB-126030. uslkg
1 1 85 phenot33. u9/k93753 bis (2-chtoroethyt) erher67. ug/ks
1 186 2-chtorophenoI33. ug/kg3754 ,l,3'dichtorobenzene
33. ug/kg'1187 1,4'dichtorobenzene33. uslkg3755 1, z'dichto.obenzene33. ug/ks
4690 2-methytphenot
67 - ug,/kg4691 2,2' -oxybis (1-chIoropropane)
100 .ug/kg
1692 4-nrethytphenoI100. uS/kg
1188 N-nitrosodi'n-proPytamine57. us/kg
5757 hexach to.oethane67. ug/kg3758 ni trobenzene13. usl ks3759 i sophorone
6-l .us/k9
1746 2-ni trophenoL
uslk9
DUP IISRP9 I,!S MSO RPO LCS
tcs
DUPB LAIK
[.D.
N.0.
N.D.
t{.0 .
[.D.
l,t .0.
N.D.
N.D.
N.D.
N.D.
lr.D .
11.9.
H.D.
N.0.
N.D.
N.D.
N.0.
N.0.
N.D.
I.D.
N.D.
N.D.
lr.D.
72 82
75 84
69 78
75 79
74 78
72 77
69 80
62 70
e4 97
74 84
75 83
77 83
33 92
7t, 82
951592
4588 TcL SU846 Senrivotatites Soil. Batch: 96183s18026
13
11
1)
5
5
6
15
tl
lq
1l
10
7
76
/J
76
76
tt
62
90
77
BO
78
76
10
I
ti.Hfi
Lan(asler Laboratones
2425 New Holland Pike
PO Box 12425
Lancasier, PA 17 5O5-2425
7 17 -556-23A0 Far: 717-656-258 1
il
67.
5ee re,rerse srCe ior e:ioianai'o. ci;!rbci';6.d abbrevratrons
7
47
1
1
28
39
50
LCS LCS
LCS DUP RPD
10 56
973
863
675
876
790
10 85
MS
MSD RPO
48 57
T3 31
71 81
77 82
73 77
1{, 15
80 87
75 36
7/. 82
17 16
81 90
80 89
79 85
7? 78
79 87
75 31
35 /+0
59 55
74 80
32 89
s1 89
DUPRPD I,IS
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(iI)Lancaster Laboratories
QUALITY CONTROL REPORT
Page: 11 of 14A Thermo Analytical Laboratory
LLI sample No. 2538090
CU-z JUD Grab Soi I Sampte
Hercutes: Bacchus Pond
sanpte Sampte
IIIDL UII I TS
II 6roup No. 522139
I Hercutes, Incol.porated - DE
I
II
3747 2,1' dinethytphenot67. uslks
3760 bis (2-chloroethoxy) methane33. us/ks
3748 2,4-dichIorophenoI33. ug/kg
1189 1,2,4-trichIorobenzene33. uglkg
3761 naphthatene33. us/kg
4693 4-chtoroani Iirre100. ug/ks
3762 hexachlorobutadiene67. ug/ks
1 190 4-chtoro-3'methytphenol.
67 - ug/kg
4691 2-rlethytnaphihateneJ3. ug/ks
3763 hexachlorocyctopentadi ene170. uslkg
3749 2,4, 6-trichl.orophenoI67. ul/kg
4695 2,4,5-trichlorophenoI67. us/ks
3764 2'chtoconaphthatenell. us/kg
1696 2-ni troani I i ne67. ug/ks
5766 dimethyt phthaLate
33. ug/kg
3765 acenaphthytene33. ug/kg
BLANK
N.D.
N.D.
N.9.
N.D.
ri.D.
N.9.
h'.9.
N.0 .
N.D.
[.0.
N.0.
N.D.
N.0.
N.D.
N.9.
'1 1
13
6
5
5
9
IJ
10
7
11
't0
8
8
10
41
t>
77
73
75
43
81
a)
7B
62
8?
82
79
75
80
77
LCS LII'IITSLog Htcil
32 119
33 181
39 135
44 142
21 133
17 116
24 116
22 147
28 123
1 100
)( t4+
39 151
50 118
53 143
1 112
33 1/,5
4589 TCL sU846 SemivoLati Ies/Soi t Batch: 96183S18025
4697 3-ni troani t ine67. ug./kg
1191 acenaphthene
33 . us./ ks
3750 ?,4-dinitrophenoI170. ug/kg
1192 4-ni trophenoI
1 70. ug/ks
4598 dibenzofuran33. ug/kg
1191 ?,4-dinitrototuene
67 - uglkg
4699 2,6-dinitrototuene67. ug/kg
tq)
't91
131
139
158
tB
,orrorn, ?au!e: .eve.ra :;te :or :.,pbn:i on or ::,'mcoic. dnd abbrevrdtron5
(l)Lancaster Laboratories
1l
"]tA Thermo Analytical Laboratory
QUALITY CONTROL REPORT
Page: 12 of 14
LCS
83
84
79
tb
66
73
BO
82
63
77
77
B6
77
91
95
68
101
B5
r03
BO
B6
7A
82
LCS lcs Lll'IITSRPD LOU HIGH
]l
Sample SatrpteMDL UHITS
3770 diethyl. phthatate67. ug/kg
3769 4-chtorophenyt phenyt ether67. ug/ks
3768 ftuorene33. u9lk9
4700 4-nitroani Iine'100. uglkg
1701 4,6-dini tro-2-methytphenot170. ug/ks
3772 !.1-ni trosodiphenytamine
67.ug/kg3 73 A-bromophenyL phenyl ether100. uglks
3771 hexachtorobenzene100. ug/kg
1194 pentachtorophenoI170. uslkg3nt phenanthrene
53. uglkg
3776 anthracene33. ug/kg
47OZ carbazole33. ug/kg3777 di-n-butyt phthatate
33. ug/kg
3778 ftuoranthene
13.L,g/ k9
1 195 pyrene67. us/kg
3780 butyt benzyt ph!hatate
67. ug,i kg
3783 3,3' -dichtorobenzidine
130.us/ks
3781 benzo (a) anthracene33. us/ks
37BL bis (2'ethythexyL) phthatate
67. ug/kg
3782 chrysene33. ug/kg
3785 di -n-octyI phthatate67. uslkg
3786 benzo (b) ftuoranthene67. uS/kg
3787 benzo (k) ftuoranthene130. u9/k9
3788 benzo (a) pyrene67. us/kg
37Bq indeno (.l,?,f-cd) pyrene
LLI sample No. 2538090
CU-Z JUD Grab SoiI Sample
Hercutes: Bacchus Pond
I
i Group No. 522239
I ttercutes, lncofporated - DE
I
MS r,rsD
79 88
79 87
7t1 80
59 62
66 72
7!. 84
8'1 92
33 94
7r+ 76
75 83
74 81
74 79
80 90
73 80
35 92
86 97
55 58
77 83
93 103
32 89
81 92
T3 80
77 85
74 8-1
32 89
Lancaster Laboratones
2425 New Holland Prke
PO Box 12125
L.rn(airer. PA i 7605-2,i:5
;- 1 ,- -656-2)iC lax 7: ; '656-)-631
1 111+
25 158
59 121
JO t.l
1 181
J6 t4t
53 127
1 15?
14 176
54 120
27 135
35 133
1 118
?6 137
s2 115
1 152
1 262
33 143
8 158
17 168
4 116
?4 159
11 163
17 163
1 171
t':l
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(I}La ncaste r Labo ratories
A Thermo Analytical Laboratory
QLIAL]TY CONTROL REPORT
Page: 13 of 14
LLr sample No. 2538090
Cu-Z JUD Grab SoiI Sampte
Hercutes: Sacchus Pond
Group llo. 52269
Hercutes, lncocporated - 0E
Sample SampteI(DL UN I TS
3790 dibenz (a,h) anthracene67. u9lk9
3791 benzo (ghi) pery[ene
67 - uq/ks
0111 l',loisture0.06 7" by trt.
BLANK
[.0 .
[.0 .
Barch : 96184C3'1 68200034
DUP {SRPD l'!S HSo RPD LCS
LCS LCSOUP RPO
100 0
LCS LII'IITS
LOU HIGH
1 227
1 ?19
100 10 1
83 91
tv 5b
9
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83
75
100
MEMBEFI
_ot:: :41 d!o.9. r,l: on!
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feu IOU:O,SS Li
(l)La ncaster Labo rato ries
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cu-z Juo Grab soit SampLe
Hercutes: Bacchus Pond
1225 ICL Pesticides in Sotids
4593 TCL Votatites by 8240
4688 Tct sU846 Semivotati Ies Soi L
4689 TCL SU846 Semivotati tes/soi I
I
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I croup tlo. 522159
i tlercutes. Incoroorated ' DEI'
I
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A The rmo Analytical Laborato ry
Page: 14 ot
SURROGATE LII.IITSLOU HIGH
50 12050 120
70 12181 1177t+ 1?i
24 I1325 121
i9 122
23 12030 115
18 137
SURROGATE SUMitARY
TRIAL ]D SURROGATE
TCX
DC8
d/r'1,2-DCA
ci8-toIuene
BFB
PhenoL -d6
2-FtphenoL
2,4,6.T8P
Nitrobz-d5
2-rbiPhnYL
Tpheny Id1 4
RECOVERY Z
65
84
91
98
84
86
30'l0l
91
77
63
r:6iir
Lancaster Laboratorte5
2425 New Holland Prke
PO Box 12425
Ld.crsier PA I 7505-2 J25
717-656-2100 Frx i17-6:;-:i3l
oR
ro/ro/9s ?ai
QUAI,ITY CONTROL REPORT
5ee.?verse 9,de ior eyDlarrd[10. ot:,/mbots aiq abb.e./ratrois ))15 9.zt
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CAT
NO-
Account llo: 067'i6
r tieccutes, :ncorporated ' DE
Envi rorrrenra: Affa i rs
ui lmington )E 19894
AS RECS!VED
xE.]-00
CETECT:'\i LI!1!T U!]IIS
Paqe: 1 of 1i
P.0.
Ret.
Respectfut ly Subflri tted
Ram.rna V. Layrnan, CIoup LeaCL.r
I Cl', ileta I s/Leacha tes
459? TCL Vo(ati les by 82r'0 - uater17?2 That t ium1713 A I Lr/rtinum1744 Anr imony1746 9ar ium1747 Bery[ [ itnr1749 Cadrniurn1751 Chromi um1753 Ccpper1754 I ron1755 Lead1755 Hanganese1761 N ici<el.1766 Si lver1772 Zinc7035 Arseni c TR7036 Setenium TR0219 iilercury4678 lCt 51846 Seflrivotat i Ies,/Uarers4679 TCL SiJe46 Semivotat i tes,/Uatecs
ANALYSIS HAME
1 CoPY TO Hercutes, lncorporated
1 CCPY TO EIM - Rocky lrountain
AI'N: v.. ioseDh (e! i.er
AT'!i 11r. Srent Robinson
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see Page
170.
57.
15.
4.2
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2.7
?.7
ouestions? Contact yo,Jr CLiCr)t Ser!ices ReorcsentJtive
Rache[ :. Kre.3mea at (1"7) 65o-?1"1'l
MEMBEFI
7x-lie
0l:24:21 D 0Ct? 15 Ra!, l2c,r.l5 i?2727
3'r c 1 5 . 0c c0 'l 027cc ASRc0l
Lancaster Laboratores
2425 New Holland Prke
PC 8ox 12425
Lancastet PA 1l 605-2425
717-656'2:00 Fa^ 71i'6,\a )aZi d-P
(|}h+ffiq*..,r,}.9,?,0,r"*gi'o
LLI sampLe No. EL 2537998Cotlecred: 6/?7/96 at 08:25 by 8R
SuEnitted: 6/28/96 Reported: 3/ 1/960iscard: 8/ 9/96
fietd Etank Crab lJa(er Sampte
Heccutes: Bacchus Pond
FBHBP SDG#: HBPo1 -02F8
See re'rerse srde ior ?rplanation of symbols dnd abbrevratrons 2216 Re'; l0/10/95
il
A Thermo Analytical Laboratory
253'7998
by SR
8/ 1/96
Page: 2ol 1I
P.0.
Ret.
RespectfuI Ly Submi tted
YicreIe rcClaiin, B.A.
C.oup LeaCe., 6C/l''!9 VoLatites
LLf Sample No. EL
coI Lected: 5/27/96 at 08:25
subni tted: 6/?8/96 Reported:Discard: 8/ 9/96
FieLd Etank Grab Hater Sample
Hercutes: Bacchus Pond
FgHBP S0G#: nSP0l -02r8
CATIIO. AIIALYSIS NAME
TcL votatites by 8240 Uater
1258 Chtoromethane1?57 Bronpmethane3/.92 vinyI ChIoride3494 ChtoroethaneY,q7 HethyIene Clrtoricle3{98 Acetone1499 Carbon Disutfide3500 i, l -0ichtoroethene
35C1 1;1-0ichLo!'oethane1503 Ch Iorofolmi504 1,2'Dichloroethane
Ci 16 2 -9utanone
3505 i,i, l'Irichr,oroethatre1506 carbon Terrachi.oriCe3507 Vinyt Acet3te
35CS BromodichLoromethane
3509'1,2-DichIocoptopane3516 cis-1,3-Diu-htoroPropene1511 TrichIoroethene3512 9ibeomochlocomethane3513 -1,1,2-Trichtoroelhane
35 15 Benzene3510 trans-'1,3-Dichtoropcopene3518 B{'oolof orm3121 4-Methyi'2'Pentanone1520 2'Hexanone352? Tetrachtoroethene3523 1,1,2,2'Tetrachtoroethane3521 Totuene1i25 Chlorobenzene3526 Ethytbenzene352C Styrene3529 x.ytene (totat)
5780 trans-1,2-Dichloroethene6263 cis-1,2'Dichtoroethcne
i Account tlo: 35716
I ilercutes, !ncorporated - lE
, Fnvironmenta', Af +a i .s
I ti tmington !E 19u94
AS NECE IVED
METr.100
DETE'TION LIHIT UNITS
(I)La ncaste r Laborato ries
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Rachel. L. KrEaxrer
Servi ces Represen:at ive
.rr (7'7) 6,5o-z-jl0
MEMBEFI,e-i-l
Lan(aster Lairoratones
2425 New Holland Prke
PO Box 12425
Lancaster. PA 17605'2425
717-656-2100 F ax 7 17 -655'2661
I
5ee reverse srCe for e,ctarairon of symools and abbrerratloo5 2216 Rev l0/30/95
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(iI}La ncaster Laboratories Page:3 of 1-1
A Thermo Analytical Laboratory
LLI Samp)-e No. EL 2537993Cottected: 6/27/96 at 03:25 by BR
Subni tted: 6/28/96 Repocted: 8/ \/96Discacd: B/ 9/96
..rccount No: t6716
liercules, :nccfporatec - D:
invi ron'rlenta: ,\f ia i rs
;i'rmington ::: 'i9894
AS REIEIVED
:rEt H!0?ZSUL.'S OETEIT:1T L!II!T U\I'IS
P.0.
Fiel.d Btank crab Hater Sampte
HercuIes: Bacchus Pond
FBHBP SDG#: il8P0'i -02F8
CATI,IO. AXALYSIS HAME
TCL SU845 SemivoIat i Ies/uaters
3918 phenoI
3B67 bis (2-chtoroe!hyL) ether3374 2'chtorophenoLie83 1,3'dichlorobenzerrei884 1,+-dichtoroben:ene3882 1,2-dichlorobenzene/.680 2-methylphenoll.68'' 2,2'oxybis ('1 -chlorooropane)
/+o82 4-fllethyipnenoI
3915 N -nj trosodi 'n-propyL ami ne3902 hexachtoroethanef910 ni trobenzene3904 i sophorone3911 2-niqrophenoti390 2,4-dimethylphenot!ea,6 bis (2-chIoroerhoxy) me.hane3656 2,1 -d i cn L oropheno L
1921 1,2,4-trichtorobenzene3906 naph tha t ene3871 4-chl.oroani t ine1900 hexachtorobutadiene3877 4-chloro-3-nrethyLpl)enoI3905 2 -methytnaph tha i ene3901 hexachtorocycLopentadiene39?3 2,4,6-trichLoropnenoL3922 2,4,5-trichlorophenoI3873 Z-chloronaphthelene3907 2-nitcoaniline5391 dimerhytphtnalate3858 acenaphthyr.ene
,, ll .'-1 . ,: li-:,.
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0ueslions? Contacr your Clienl Scrv d('s ?L:prcsel:3!lve
Rachel L. Kleonref a! (7"7) 6to'Z3lA
MEMEiEFl
TARffi
Lancasier Laboratoiles
2425 New Hoiland Prke
PO Box 12425
Lancastet PA \7605-2425
1 17'656-2304 F ax /- 11 -6t6')6E1
Re5pect ful ly Submi ttedChristire i!- Ratc l.'i;{,
Croup LeaCer. 6ClMS
See rever:e s de for exolana: on of ;Tmoois and dbbre'/ratrons d's22 l5 Re,r 10/10/95
I
'Account !lo: C5716
I Hercutes, !nc.,.porated - DE
: Envi conmenta,. A:iai rs
: ui Lmingt,;n oE '19U9/,
AS RECE!VE9
MET!AN
i:,ii:iii:,:,i:ir3,Es!!Ie::.r :: DE'rEcT I 1ri '- ! !i l't uN I rs
4 of 11
B.S.
a]}
2216 Rev ro/30/e5
'IE'
Page:ll
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ouestions? Conract
Rachi.t L. Krdamef
your CI ienl Selrices Representariveat (7'7) 656-2310
Txtir
Laocaster Labo.atofles
2425 New Hollard Prke
PO 8ox 12425
Ldncasrer. PA \1 605-2425
7l7'656-2100 Fdt 1 11'656'2531
RespectfuI ty Submi tted
chrisrine i"l. Rarctift,
Group Leader, GCIMS
See reve.se s,ce rcr e\pld4;:,or\ oi i/moois dnd dobrevralrons.
(I)L+ffiq*ff.1*?,0,t*9['tt
LLI sample IIo. EL 25i7998Cottected: b/?7lsb ar 03:25 by on
Subnitted: 6/?3196 Reported: 8/ 1/96Discard: 8/ 9/C6
Field Blank Grab lJater Sampte
tlercutes: Bacchus Pond
FBhBP sDG#: tlBPO1'02f8
cATIIO, AIIAI.YSIS NAME
IcL sU846 Seoivolati Ies./lJaters
3908 3-ni troani t i ne3857 acenaphthene1893 2,4-dinitrophenot3912 4-ni trophenoIi379 dibenzofuran3994 2,4-dinitrotoIuene3395 2,6-dinitrorotuenei887 diethyI phthalate3875 4'chIorophenyl phenyl ether3898 ftuorene3909 4-nitroani Iine4683 4,5-dini tro-2-rnethyi.phenol5914 N'nr trosodiphenylamine3859 4-bronlophenyt phenyt ether3899 hexachtorobenzene19',6 pentachtorophenoli9,i7 phenanrhrene3359 anthcacenet 681 carbazo l. e3880 di'n'butyL phthatate3897 ftuoranthene3919 pyrene3870 buryt benzyI phthatate1385 3,3'-dichLorobenzidine3360 benro (a) anthraccne3868 bis (2-ethylhexyL) phthetate
38i5 chrysenelE96 di -n-octyt phthatare3361 benzo (b) ftuoranrhene36c2 benzo (k) {Luoranthene
3E6lr benzo (a) pyrene3901 indeno (1,2,3-ccl) pyrene
3881 dibenz (a,h) anthracene3863 benzo (9hi) perytene
ug/ l
'ts/',,:ct/ i.
.s9/t.
'jg/ t-
ug/ !.
u?/ t'
ugl'.
rg/'.
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ug/ t'
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(iI)Lancaster Laboratories Page: 5 of l1A Thermo .Analytical Laboratory
LLI Sample No. EL 2537998
Cottected: C6/27/96 at 08:25 by BR
submi tted: D6/28/96
j Account No: C6716
, fleecutes, Incorporated - DEi Envi ronnrentaL Atfa i rs
i ti tmington 0E '19894
lFietd Btank Grab Uater Samote
Hercutes: Eacchus Pond
FBHBP S0G#: ilBP0l -02F8
CATIIO AMALYSI S NAIIE
459? TCL Votarites by 8240 - Uate.
17ZZ ThatLium
1 743 A t umi nuni74/, Ant irnony
1746 Bariunr1747 Berytl.itrm
'I 7d9 C adnr itn
1 75 1 Chromi umi753 Copper
175t, I ron
1755 Lead17i8 uanganese1751 NicIeI176o S i [.rer
1772 Zinc
1848 Lv SU8l,o '! CP D i gest ( tot rec )7035 Arsenic TR7036 Seteniun TR
0259 Hercury5713 gu srJ8l,6 H9 oigest
0813 8NA uater Extracrion
4678 TCL SU846 Senrivotati tes/lJaters1.679 1t:L 5*345 Sellivol.ati Ies/'Jaters
H ET HO!
5U-846 3l4LrB
s'J-846 6! i 0A
s'J-846 6,l t,.lA
su-346 6J t 0A
su-346 6-rt 0A
su-346 6110A
su-8r,6 611cA
S,J-846 6:)iCA
clr-u,'; 4l-,11
cr.-O/i (r1a\
S'J-845 5ll C;1.
SiJ-8/r6 i.,'llA
5';-940 5rl1!i\
s',,f -3(5 5l:4,1.
s;'-E16 5ll ia
crr-e/l i:o(n
Sr-C4o 6,l1LrA
sl.,-846 5t10A
SU-846 71r70A
sr-u46 7;70A
su-846 35'r05
su-S46 81708
su-846 It2706
AIIAI.YS I S
TRIAL OATE ANI T!}|E
., 07/03/96 0311
1 A7/i5i96 C327') 07/15/96 CaZT't C7/'.5i9c N327', 07/"5/95 43271. 17/15/95 ?3?7', D7/'5/9'_.03271 A7/',5i96 N1?71 C7i'^5/9t C3?7i a7/'.5/9o t327' 27/".5/95 l1Z7
', 17/1'.,/95 0327'. c7/',-</95 D3?71 97i15/9i C127
', c7/',5/95 l1?7L t7/.C/9i, 12?Z" n7l1s/c/, n1?7
', 07t15/9. 0327
1 07/A3/95 18,52., g7/c?/95 21??
1 07102,/95 C9l01 07/11/96 01gL1 07/t!,/96 01A4
AIIALYST
Susan A. l'lcitahon
oonna R. Sackett
oonna !1. Sacket!
Donna R. Sacke:t
!onna R. Sackett
Donna R. sackett
}onna R. Sacke!t
Donna ii. Sacketr
Donni R- Sackert
Donna R. Saciet!
0onna R. S.lckett
Donna R. Secketr
lonna R. 5.1ckett
Donna R. Sa.kert
0onna R. Sackett
Christine H. Conl,in
Conna R. Sackert
oonna R. Sackett
Nel. li S. l,(arkaryan
NeLLi S. ltarkaryen
!!aria A. Davenport
l4ack A. RatcL if f
Ma.i( A. Ra(.Liff
7Rril
Lancaster Laboratofles
2425 New Holland Prke
PO 8ox 12425
Lancasrer. PA 17605-2425
717-656-2300 Fax [phone] i 2216 Rev,Orr,r* d?
LABORATORY CHRONICLE
5ee reve.se s,oe for explanat,on oi :7-ools and aDbrevrdi ons
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A Thermo Analytical Laboratory
Pa-oe: 5 of '11
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Hercutes: Bacchus Pond
SarnpI e
MDL
Sampl e
UII I IS
!.59? IcL Votarites by 8240 - Uater Batch:
1?58 Chtoromethane3. ug/ t
1257 Brooornethane3. u9/ t
3492 Vinyt Chtocide2- uglt
3494 Chtoroethane3. us/ [
3497 t'!ethytene ChLocideZ. ug/t
3498 Acetone6. u9/ t
3499 Carbon Disutfide3' u'/L3500 1,1-DichLoroethene
'1 . uslt
3501 ,l,1-Dichtorc,erhane
Z. ug/t
1503 Ch Iorofocnr1. uglt1501 1,2-Dichtoroethane2. uo./ t'
0316 2-Eutanone3. uq/t350i 1, 1,1'Irichtoroethane
I Group No- 5227?7
; Hercutes, lncorporated - DE
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7i 58
83 81
9C 32
67 61
1C2 c8
6i 9i
75 72
1.14 i 06
'r 03 100
115 1C9
96 1C0
64 97
116 't 14
'l 11 110
99 I04
98 ',l 01
97 1C1
10t- 1 nq
97 c9
82 95
1 C/. 101
9', '.,Dz
OUPB L.,1TK
t961 84 1AA
usl t
3506 Carbon Tetrachtoride
1 ' us/t
3507 Vinyt Acetate?' u9/ L
3508 Bromodi ch Iocomethane1. ug/t3509 1,2-Dichtoropropane
1-
1.
1.
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N.9.
N.3.
N.l.
N.9.
N.!.
r.l .9 .
N.0.
N.9.
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N.D.
N.!.
I.0.
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N.1.
N.3.
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1
?7
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2
4
1
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ug/ ti511 Trich(oroerhene
1 ' u9/[
3512 DibronpchLoromethane2. u9/ [3t13 1,1,2-TrichtoroethaneZ. ug/ |'
35 15 0enzene1. uglt
35'10 trans-'l,J-D ichIoropropene1. ug/t
MEMBEFl
TXEIir
Lancaster Labo.atones
2425 New Holland Prke
PO 8ox 12425
Lancasrer PA I 7605'2,f25
717-556-2300 Fdxr 717-555-2681 d'r.il
;T
QTJALiTY CCNTROL R.EPORT
5ee re,/erse;tde fo. ?xplandtron of symbols aod dbbre,/ralrons 2216 Rev l0/10/-05
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(I)Lancaster Laboratories Page: 7 of ilA Thermo Analytical Laboratory
LLI Sarnple No. 2537998Fietd Btank Grab Uo(er Sarnpte
Hercutes: Eacchus Pond
Sroup No. 5227?7llercutes, !r:corporated OE
Samp I e
tlDL
Sampte
UilITS
DUP
RPD
JIIS
RPO
21
36
4J
2
26
0
0
z
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5
4
1
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1
1
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1
2
9
34
1
3
,1
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LCS LCSDUP RPD
LCS LIMITSLOU HIGH
80 120
80 120
80 120
80 1?0
30 120
B0 120
80 120
80 120
80 120
80 120
80 120
80 120
80 120
3518 Eromform1. uglt [.]. T1 905521 4-llethyt -Z -pentanone
5. u-olt !'1.D. 65 933520 2-Hexanone7. ug/t rl.D. 62 953522 Tetrachtoroethene
'I . ug/L [.0. 105 10S3523 1, !,2,2-TerrachIoroerhaneZ. ug/t N.o. 72 943521 fotueneZ. ug/t lJ.D. 105 105
35?5 Chtorob€nzene1. ug/l N.9. 101 1013526 Ethytbenzene?. us/t N.9. 1 10 1C93528 styrene1. ug/t N.9. 1C? 1.A2
3529 Xytene (rorat)
1. uglt N.9. 1C8 r085780 trans-1,2-Dichtocoerhene2. uS/t N.3. 1.04 996268 cis-1,2-Dichtoroethene?. uslt N-0. 1C6 1C2
1722 That Liw Eatcn: 96192!843J02170- uslt H.D. (i) 101 103'1743 Atuminurn Batch:96192'!848!0257. ug/i N.9. 174 -772 -729 (?)
1744 Antimony eatch: 96192194800215. us/t N.D. ('t ) 1C5 1061746 Eariurn Batch:95192'18483022.2 us/t N.c. 0 (1) 87 83
1747 Ber-ytl.iurn Eatch: 9619218480021.3 uS/t 0.0016 J mgTL (1) 97 97
1 749 Cadmi um Batch: 9o'1921&8C022.7 ug/t N.9. (1) 9/, 95
.t751 Chromium Batcn: 961921848C021.3 ug/t t1.0. 0 ('1 ) 78 79
1753 Copper Barch: 9619218480023.8 u9/[ N.9. 0 (1) -201 -191
1754 tron Batch:96192184|!025.9 uglt 0.0607 J nrg,/l 174 -'i513 -1141 (2)
1755 Lead Batch: 96192teq8tC213. us/l N.C,. 0 (1) 92 931758 Manganese Batch:96192184SqC22.9 ug/t N-0. 0 (1 ) 59 61175'l Nicket Batch:96192'1843!02S.tt u9/[ N.9. 0 ('1 ) 9/. 95
1766 sitver Batcrr: 9019218r,31023.5 us/t N.c. ('t) 99 101
(1) The resutt for one or both deletminatioos r,las [ess than five times the LOo.(2) The background resutt Has mo.e than four titnes the spi<e acided.
BLANK
Lancagter Labordtofles
2425 New Holland Prke
PO Box 12425
Lancastet PA 11 605-2425
717-656-2100 tax 7 17-656' 2631
MS HSD
1C2
107
lCC
98
97
107
1 0'l
1',I1
102
101
101
'1 00
MEMBEFlzkm
QI,'ALITY CONTROL REPORT
See reverSe srde for erp,anatron of svmDots and abbre'/rat,cns 22 16 Rev l0/10/-05
,I1
1l
(l)La ncaste r Laborato ries
A Thermo Analytical Laboratory
r.lllaT.TmVYv.fJ5+ !
'I03
IUJ
103
Pa-oe: 3 of i1
LCS LI}IITS
LOU HIGiI
120
120
120
120
'Il
LLI sampLe No. 2531995
Fietd Btank Grab lJater Sanrpte
Heccutes: Bacchus Pond
Group llo. 522727
Hercutes, lncocporated ' DE
ll
ll
Sanpte
MDL
177? Tinc12. usll
7035 Arsenic TR2.7 uglt
7035 SeLenium TR2.7 u9/ |
0259 ltercury0.043 ugl t
Sampl e
UNITS
ouP i4s
RPD MS I.IS9 RPD
LCS LCS
LCS DUP RPD ]l
it
ELANK
Batch:961921848C02
N.D.
Eatch:96'1921348C02N.!.
Earch: 961921843C02
ri -D.
Eatch: 961845713C01
N.9.
(1 ) -41
(': ) '101
(1) 79
0
0
0
0
5
1
1
80
80
80
80
-J4
102
102
4678 TCt- Sr"8(5 Se.mivoLari tes/lJaters 6atch: 96184UM025
!ril
il
I
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I
I
I
5 112
12 158
?3 13t+
1 172
20 1?4
32 129
46 123
J6 tOO
5 152
1 230
40 115
7C 4 0n
24, 196
29 182
3? '! 19
Ii l8,i
39 135
l+/+ 11,?
?1 13i
31t
i88
185
563
170
371
?6t
4 103
853
094
097
765
086
084
37C
t+9 47
91 91
33 39
78 \2
80 83
79 82
81 82
67 58
o? az
11C r11
7? 78
97 97
1!0 100
ct4 95
66 70
90 90
36 S6
79 31
e3 38
3918 phenoL
'l ' ug/t
1867 bis (2-chloroethy[) ether
'l . ug,i t
387t, 2-ch(orophenot1. us/t
3831 1 ,3-di ch L orobenzene1' u'lt
3B!1,;'1,4-dichlocobenzene1. ue/t7!12 1,2'Cichlorobenzene
'1 . ug/t(590 2'methytphenoL2. uglL/.r31 2,2,oxybis ('l -chtoroproDane)
2. us/t
1,6!2 4-methyLphenoI2. ugl t
3S15 N-ni trosodi -n'propytamine
?' us/t
39DZ hexach ioroethaneZ. us/ t
3910 ni trobenzene1. u9/ t1|r1 isophorone1. ugltit'l 1 2-ni trophenot?. us./ L
3l\';7 2.4' dinethyLphenoI1. ug/t
ll16 bis (2-chIocoethoxy) rnethane1' usltl!.j5 2,4-dichlocophenoIZ. ugl tit;?1 1,2,4-trichtorobenzene
'l . u9/ t'
39C5 naphthaIene1. ug/[
N.9.
N.D.
N.1.
N.9.
!l.r.
N.C.
N.9.
N.9.
N.D.
N.D.
H.l.
N..1.
N.9.
N.!.
N.2.
N.D.
ri-1.
N.3.
('l) Ihe resutt for one or both determinations Has Less then five !illes the LCo.
Lancaster Laboratones
2425 New Holland Prke
PO 8ox 12.125
Lancastei PA 11 605-2,125
717-656-2300 Fax 7 17'556'2631
MEMBEFlrrcm t]}
,nrrorn, ?al
I
CCNTROL REPORT
Seg.ere.se sroe'or explanatron oi symbols and abbrevratrons 22 l6 Rev
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(l)Lancaster Laboratories Page:
A Thermo Analytical Laboratory
LLI sample No. 2537998
Fietd sLank 6rab Uarec Saarple
Hercutes: Bacchus Pord
Sanrpte Sampte
I.tDL uilIrs
i
I Group lio. 522727
!lercutL.s. lnccrcoratedt'
LCS LCS
LCS DUP RPD
!!stlsD RPo
DUPRPO VS
3871 4-chtor-oani Iine?. t,g/ t
3900 hexachlorobutadiene
'I . us/t
3972 4-chtor-o'3 -npthyIohenoI
?' us/t
3905 2'methytnaphthatane1. ug/t
3901 hexachtorocyctopentadiene3. u9./ t
3923 2,(,6-trichIorophenot
'l ' ug/t
39?2 2,4, 5-tr ichtorophenoI1. ug/t
3873 Z-ch Ioronaphthal.ene1. us/t
3907 2-ni troani t ine
1 ' uglt
3891 dinrethyt phthatate3. u9/ l.
3858 acenaphthy(ene1. us/l
B LANK
N-9.
H.l.
[.0 -
N.9.
N.D.
N.D.
[.c.
N.!.
N.9.
N.D.
72 74
,55 5e
93 93
5: 53
g') 37
g9 38
91 90
97 97
32 31
92 93
1
0
1C
5
1
on
93 93
4 r 5t
t+7 45
39 38
95 e5
99 10C
L) L<
10i r02
1A? 93
o.
n
91
80
t,1
91
90
88
95
25
85
80
92
55
85
94
95
101
98
86
B2
LCS LIl|IITS
LOU HIGH
17 116
Ztr 116
?2 147
23 1?3
1 100
37 114
39 151
60 118
)J IqJ
1 112
33 145
7 143
47 145
't 191
1 132
23 131
t9 119
50 158
1 114
?5 158
59 121
?a 1))
1 181
a'.
,orrorn, ?aJ
4679 lcL su845 semivotatites/uaters Batch: 96i84uM025
i908 3'ni troani t ine1. us/t
3357 acenaphthene1. ug/t3893 2,4-dini trophenoI5. u9/ t
3912 4'ni trophenol5. ugl t
3379 di benzofuran1. uglt
3894 2,4'dini trotoluene
?' ug/t
3895 2,6-dini trototuene1. u9/[
3887 diethyt phthatateZ. ugl t
3875 4-chtorophenyl phenyI etherZ. ug/tlS98 f Iuorene1. us/[
3909 4-nitroani t ine2- u9/ t
t bB3 4,5-dini tro'2-rnethytphenoL5. us/t
Krfl
Lancaster Laboratones
2425 New Holland Prke
PO Box 12425
Lancastet PA 17 605'2425
1 11 -656-2100 Fax. 7 f i'656 2531
QIJALITY CONTROL R-EPOR.T
See /e\erse Srde io. erpia-;-c. Of STmaorS d.d dbbrevrdt,ons 2216 Rev
(iI)La ncaster Laborato ries
A Thermo Analytical Laboratory
QUALITY CONTROL REPORT
Page: 10 of I
LCS LIMITS
LOU HIGH
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LLI sample No. 2531998tietd Etank Grab lJater Sa$p'.e
HercuIes: Bacchus Pond
Sampte Sampte
UUITS
I
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: Group No. 522727
I i{ercutes, lncccporaied - DE
!rsMS9 R29
DUPRP9 i{S
LCs LCS
LCS DUP RPO
,I
IIDL
3914 l,l -ni trosodiphenyLamine2. u9/ t
3869 4-bromophenyI phenyt ether2' us/t
3899 hexachl.ocobenzene1. ug/t
3915 pentachtorophenoI1. uglt
3917 phenanrhrene
'1 . ug/tf859 anrhracene
'I . ug/t
1684 carbalole1. us,/t
3880 di -n-butyL phthatate1. ug/t
3897 ftuoranthene1. ug/t
3919 pyrene
'I . ug/t
3870 butyL benzyt phthatate
z' u9/ L
-1885 5,3' -dichlorobenzidine
?. ug/L
3850 benzo (a) anthracene1. us/t
31168 bis (2-ethyLhexyt) phthatate
?. ug/L
3876 chrysene1. ug/t
1396 di -n-octyl phthatate2. uglt
3361 benzo (b) ftuoeanthenez' us/ [
3862 benzo (k) ftuoranthenez' ug/l
3B!4 benzo (a) pyrene
?' us/t390i indeno ('1,2;3-cd) pyrene7. ug/ [
3331 dibenz (a,h) anthracene2. usll186l benzo (9hi) pL'rytene
Z. u9/ t
B LANK
H.D.
ll.D.
N.0 ,
N.).
N.D.
N.D.
N.D.
Il.D.
ti.c.
N.t.
N.D.
N.D.
N.D-
N.r.
N.C.
N.D.
!1.1.
N.D.
It.9.
,{ .D.
N.D.
38 147
53 127
1 15?
t4 tl6
5/. 120
?7 133
t+0 137
'1 118
26 137
52 115
1 152
1 262
33 143
8 158
17 153
4 1t,6
24 159
11 163
17 163
1 171
1 227
1 ?19
284
285
?95
1'1 90
492
185
289
283
188
292
182
?77
1 102
090
5 104
289
0 91,
081
182
2 St,
177
88 86
88 87
96 94
15 40
95 94
g3 g7
92 90
89 87
9C 89
93 91
79 78
36 85
102 10',1
9i 9!
100 1a7
90 38
95 95
3i c3
75 75
38 e6
,45TiI
Lancas{er Laboratofles
2425 Ne.r Holland Prke
PO 8ox 12425
Lancasrer PA 17 605-2t24
7 1 7-655-2 300 F ax i 17 -6\6-262 1 2216 Rev ,rrr* d? |
I
see rever5e Sroe Ior explana: c- 3r ;ymbols anc dbble'/'dlrons
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(I)Lancaster Laboratories
A Thermo Analytical La bo ratory
11
_t\
2216 Re.. 'Orrorn,
?aE
SURRCGATE TIHITS
Page: 1 1 of
HIGH
114
1i0
115
'100
94
123
114
116
lq
LLI sample No. 2537995
Fietd Btank crab Uater Samote
rlercutes: Eacchus Pond
459? TCL Votatites by 8240 - Uater
4678 IcL StJ81r6 Semivotat i Ies,/lJaters
4679 llt- StJ846 SemivoLati tes/uarers
Group No- 52?777
HcrcuIes, Incorporated - DE
SUIlROGAIE SUMI'!ARY
TRIAL ]D SURROGATE
ci1*-1,2-DCA
c8-:oLuene
bi L
2-FLphenoL
theno t -d6
?,4 ,6-f8P
tt itrobz'C5
?-t--bietrnyI
TDlren/1 C14
RECOVERY Z
100
i0c
55
)(
,t'i
79
3",
31
LOU
76
3u
36
?1':0
10
35
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Lancaster Laboralofles
2425 New Holldnd Prke
PO 8ox 1242S
Lancasrer. PA 11 605-2.12t
717-656-2100 Fax 717 6-<o 2681
QLIALITY CONTROL REPORT
See re'rer;e ;rde lor exo ;ra: on oi lymbols dnd abbre,/ratrons
,il
3l
il
1l
1l
'11
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(I)Lancaster Laboratories Pag e:A Thermo Analytical Laboratory
LLI sample No. EL 1533010Cottccted: ii?5/9o at 14:C5 by 8R
Sub{nrrted: 6/?g/96 Reoorted: 8/ 1/96
D iscard: 3/ 9/96
CU-6,iuo Grab U6ter Saflrotc
Hercutes: Eacchus Pond
CSJUD SOG#: llEPDl - 1 1
ANALYSIS HAME
TCL Votari les by 82{0 - !,ater
That L iun
Atsninrrrtt
Ant i[]ony
6ai i ian
?ci'y[ [ iuor
Cadui ul
Ch rorn i um
goppec
I !-on
Lead
Manganese
NirxeL
Si Iver
Zinc
Arsenic TRieleniurr:R
l.le rcury
TCL Peiric ides in t,'atersTtL Slu/ro SenrivoLati Les/Uaters
TC!- Sl5.i6 Scmi voL3t i les/iiitsrs
Accolnt \lo: 05716
I lercules, lnccroorated - DE
Envi romrcnrar, lfiai rs
IJt !.min9ton cg 1989q
AS RECEIVED
Mqrtrnn
IESJl.TS, DETE'II3:( L!I'1IT UIIIlS
P.0.
Rel
4592
1722
i7!,6
1719
1751
l,'))'t7it
17'.:5
1758
1loh
1 1a)
7lll5
02590irl/
Li78
t,.79
,!7.; ,
. :l -:'-
5,7
il.l.
r: af -
i.L.
. i,,.i..
..., . . ii.l.
See Page
'rg/ ''
u9/ ''
t,l/'-
r9./ L
r'il'/:
,:c)/ t-
1,3 u!,':
S.le Page
See Page
t.'e Pa:e
iJ I'170 -
?.2'.i
2.i.;.)
:a
5.q
:.a
1il.
:.7
L-, -'l
Orc.st ions? C.rnt6ct vorrr CL l atr SL'T! i re: Qecresee:aI !ve
lrlli,r; o*ii;J" ,, ^0,
"',!1,,1] tZl.?i'r'
I
ilo l',.cc cl12570c ^sRcll
Respeciiut Ly Submi tted
iiariDn3 Y. Laynin, 6roup Leadef
l:!,iletaLs/Leachares
I
I
rxTiil
Ldoca5ter Laboratones
2425 New Holland Prke
PO 8ox 12425
LancasteL PA 17 605-2425
7 17 -656-2100 Fax: 7l 7'656 2631 See reve'se ;,ce tc':.prano:'o^ oi ;vrbri' ano oobrerrolrons
t]}
7)16 Rev,Orrorr, ?af
(l)Lancaste r Laborato ries
A Thermo Analvtical Laboratory
I
, Account No: !5715
i tiercutes, !n.orporated - DE
i Env i ronnrenta. ;\f f: i rs
1 lJi lmington lE :939/.
P.0.
Ret -
Respectfut r.y Suhmi tred
t" :crete l'lcciarin, g-A.
GIoup -eaC:r, GC/':{5 Vol.ati'.es
Page: 2 ol 1l+il
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2.:.
LLr sampLe No. EL 2533010
cot tected: h/25/96 at 14:05 by BR
Subritted: 6/28/96 Reported: 8/ 1/960iscard: 3/ 9/96
Cu-6 JUD Grab 'Jater SamDte
Hercutes: Dacchus Pond
C6JUD SD6#: HBP0'l -1 1
CATilO. AIIALYSIS IIAME
TCL Votatites by 8240 - t,ater
1253 Ch Ioromerhane1257 6romoroerhane34qZ Vinyt ChLoride349!- ch Ioroerhane3497 Merhytene Chtoride3498 Acetone1t99 carbon DisuIfide3500 i,l-Dichtoroethene3501 1,'l-Dichtoroethane3503 Chi.orofo{'m350/- 1,2-DichIocoethane0315 2-Butan.ene
i505'1,1,1'Trichtoroethsne3505 Carbon Tetraclriorida3507 VlnyI Acetate1508 grornodichlDromethane
3599'1,2-9ichtoropropane
i5 16 c i s-'l,3-Di ch LoroDropene3511 Trichtoroethene3512 0ibromochLoromethane3513 1,1,2-Tricntoroethane
3515 Bcnzene35'10 trans-'1,3-DichtoroProPene1518 Bromoform3521 4-Merhyt-2-pentanone3520 2-Hexatrone3522 Tetrachtoroethene35?3 1,1,2,2-Tetrachtoroethanei521 Totuene
157-5 Chtorobenzene3126 Ethytbenzrlne35?8 Siyrenc352q )(yl.ene ( tot3l )t7B0 trani-1,2-Dichtoroethene63JB cis-1,2-Dichloroethc,rc
AS fIECE!VED
rii*:j:::::::::::.':::::::.:::::-'r: llET'rlCD
!'iil:ii!q!!!=15.,,'. :r DETECT I lrl LIil tT url I Is
oueitions? contact
RichrI L. Kr+irrer
.,:i.;,',: i..i'i i,i.,.t "' . tt.
:,::,. .,:,,]:1::'::::],]:.U . n.
your Cl ient: Serv!ces Re=resen:a:tve
ar (7" 7) 65o'2iLl0
MEMBEFl
'KNTI
Lancaster Labordtofies
2425 New Holland Ptke
PO 8ox 12425
Lancasrer, PA I 7605-2425
7 17 -656-2300 Fax [phone]
T
di l'
t
5ee reverse 5,ce jor erpla.alon of symbols and abbrevtatrons 2216 Rev 10/30/95
I
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3of 14
Account No: 05716
iercutes, lncc.pora!ed - DE
!nvl ronflenr.l r. Af ;a irs
'JrLflirrgton ,n 19894
Suhnitted: o/?8/9o Reported: 8i 1/96Discard: 8/ 9/96
CU-6 JUD Grab i;ater Sarnpte
Hercutes: Sacchus Pond
C6JU0 S0GII: hBP01-11
CATIIO. ANALYSIS IIAME
ICL Pesticides in Uaters
1c00 Atpha 8HC'1501 Bera BHC'i601 0e L ta 8HC'l'502 Gamna BHC - ! indane'1504 Heptach I or'1o05 LLdrin1605 Heptachtor Epoxide16'16 EnciusuIfan I161C 0ieLdcin1607 DDE1611 Endrin1615 Endosutfan I I1608 DOD1617 Enclosutfan Sutfate1609 DoT0933 Endrin Ketone1860 ltlethoxychLoc136'l A'.pha Chlordane.,i62 Ganrna Chlorciane1513 Toxaphene
-1618 Endr in AIdehyCe1619 PCS-10',101620 ?Cs-12211021 PCE-I2J21b?? PCB-12/r216?l Pc8 -',r 2iB162\ PCS-12541626 PCE- r260
AS RECEIVEO
I
:+:::::;.:.:.. iiEsll T J
I'' ET HOD
DETECIICT.J Ltl!T UNI IS
f .002 ug/ i-
n n^(r ,,|) / .
rl ll( ,,,r/i
n n4) ttttl
C.l:;! ut:/ !.
,J . Di4 ug/ L
^ rla<-:/ '
'l 'r:? ,^ t -'-!/.
0. rl05 ug/ :
0 . CD5 l_tg/ 1-
n -i; t,atl
0-!1 !g/t
C. 137 u$/ |
a . ii!7 u.:r/ IC.,-r,J8 u!/ t,
L). Ji4 uf/i-
'j. rl j :!/ t-
n ,riq ,r,tl
r' .li5 N9/ t
1' u'/l0.C10 us,/t
0. 19 ue/ ID.Z ugl L
C .'.19 u9/ t
0. C5 us/ t
0 . '17 uq/ !.
0. C6 u!r,/ L
C .i7 ug/ t
I
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ii .,-r -
Dur'to insufficient sampte size, Ee Here uaabLe ro report our usuatquantitatron linrits. Tne val,uc,s reporteaj -f.octs..ar the torest quanritation
Lirni!:s cbrainabte-
Questions? Contact your Clicnr Se:-"icr.s ?epresentalive
ll.ichel L. Krea,ne.
Respectf,JL Ly Subn[ ttedJeniier E" Hejs, B.S.
Croup Lerder- Pest ic iCes/PCBs
rciTr
Lan(aster Laboratorres
2425 Ne'd Holland Prke
PO Box l:425
Ldncasrer. PA 17 6A5 - 2425
111-656-23AA Fat 711-a56 )a;),2216 Re.r,0r30lr5 d3
(iI)Lancaster Laboratories
A Thermo Analytical Laboratory
LLI sample No. EL 2533010Cottected: 6l?5/9o ar 14:05 by ER
See 'ever5e .. de fOr exp'Jnat,On of Symour5 dno abOre/alronS
(I)La ncaste r Laborato ries Paqe: l+ of 14
A Thermo Ana lytical Laboratory
LLI Sample No. EL
co[ [Ectcd: 6126/96 at !4:05
Subrni tted: 6/29196 Repocted:Discard: 8/ 9/96
CU-6 JUD Grab lJater Si]flpte
Hercutes: Eacchus Pond
C6JUD S0G#: HBP0'1 '1 1
CATNO. AIIALYSIS IIAME
ICL SUg46 Semivot ati tes/Uaters
8/ 1/96
Oues:trons? Coritact )'oul
Raahcl r-. Ire:.roer
nccount No: 167'16
iiercutes, inco.poratcd ' DE
Envi ronmenrai. Af f a i rs
Yitmington 9E 19894
25330 i0
'ry 8R P.0.
lleL.
AS RECEIVED
r'1ETHC0
DETECTICN L!I.!IT UNITS
phenoI
ois (2-chtoroethyt) ether
Z - ch I orol rheno L
'l ,3 -d i ch Iorobenzene
i,c-ciichlo.ooenzene
1,1-ciichlorobenzene
2 - methyt pheno L
2,2,oxyt:is ( 1 -chtoropropane)
4 - rilet hy t pheno t
li - n i rrosodi -n- pnopyt alrri ne
he:<ach lorcernane
n i r iobcriene
i scphoror:e
Z-ni trophenoI
2, ri -di rnethy !. pheno tbis (2-chtoroeEhoxy) methane
2-1-t!icnIoropherroI
1, 2, 4 -tr i ch Lorobenzene
naphrhatene
4-chIoroaniiine
he;..ich t orobutaCi ene(- ch I oro-] -fiethyIohenot
2 - rncthy t nsph tha I ene
h exach I o rocyc I ope.nt ad i ene
2, {, 6- tr i ch i orophcnc-.I
2,4,5-tri ch Lorophenol
l-dhlorcnaphthatene
2-ni troani t ined:;:ethyI phrhatarc
ac.naDh thy L ene
1-
a
)
)
)
6.
a.
)
)
C t i enr Se!'v1 ces Represertat i ve
ar (7-' 7 .t 6:;6 - 2ll'-'
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Lancaster Laboratoftes
2425 New Hoiland Prke
PO Box 12425
Lancastet PA 17605-2J25
717-656-2300 Fax: [phone]
Respecl:fut Ly srbmi ttedChristine U. S:alctii{, B.S
6roap:-eader, GC/'14S
See reverse srde for explanatron of symbols and abbrevrdtlons
at
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(iI)Lancaste r Laboratories Page:A Thermo Analytical Laboratory 5 of lt,
LLi Sample No. EL
CoI tecred: 6/26/96 a! lrr:C5
suhni tred: 6/29/96 Reported:0iscard: 8/ 9/96
CU-6 JUD Grab Uater gampte
HercuIes: Bacchus Pond
C6JUD SDG#: HBP01 '1 1
CAT},IO. AIIALYSIS NAI'IE
fCL SU846 Semivotati te9/uaters
3908 3-nitroanitine3857 acenaphthene3893 2,4-dtnitrophenoI3912 1-ni trophenol3879 dibenzofuran389t, 2,4-dinirrototuenei895 2,S-dinitrotol.uene5837 diethyt ptrthaLate3875 4-ch'-oropnenyt phenyt ether3i98 f Iuorene3909 4-nitroanitine1683 4,6-dinitfo-2-methytphenoti9lJ, lr-rritrosodiphenylarnina3869 4-bcornophenyL phenyL ether1899 hexach I orobenzene3916 pentachtoroghenoI3917 phenanthrene3859 snthracener.684 carbazoIe3880 di'n-butyt phthatate3897 f I uoranttrene3919 pyrene3970 butyt benzyl phthatare
33E5 3,3' -CichLorooen:idine
la60 benzo (a) anthraceneZe$ cis (2-erhylhexyL) phthaIare16f6 chrysene1996 di -rr-octyt phthatarel5L1 benzo (b) fLuor;.nthene336? benzo (() Jl.uoranthene3gir4 be.nzo (a) pyrene
39Cl indeno (1 ,2,3-cd) ?yrene3i131 dibenz (a,h) anthracene3863 benzo (ghi) perytene
Due to insufficient sanpte,
selrivoLati Ie corrrpounCs uere
/\cco'Jn( lio:357'o
:iercuIes, :nl-orporated - DE
:nv i rorYilenr3 ,- A{ +a ! rs
'^ ilrrrinqron DE i9894
AS NECE!VE9
::. t{EIt1oD
ItESLiLTS. 0ETE!Il3^- Ltl{l'r UNIIS
25i8010by SR P .0.
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4-
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u-:,/ l
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19/'.
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ug,/:
.rgl I
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N9/ t
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ug,/ I
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u'J/'-
us/ i
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usl I
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oLrestions? Contact
Rach€:L L- KrEir(!ee
yo,Jr C.l. r en: 5er';i ces.rt (7"1)
for the
Rep.esen!3 t i ve
51o - 2i:lC
Respectfut Ly Submi tted
Chris::ne q. ta!cr.iff ,
GrouD -eader', r:C/l''1S
5ee reverse;toe ior explanatron of symbols and abbrevration5
B.S
Lancaster Laboratofles
2425 New Holland Prke
PO Box 12425
Lancaster. PA 17 605-24) a
717-656-2300 Fa\ 1 17 -656 )5e1 d'}
MEMBEFl
2216 Rev l0/10/95
&&&I
(I)La ncaster Laborato ries Page: 6 of 14A Thermo Analytical Laboratory
LLI Sarnple No. EL 25i8010
CoLIected; 06/2b/96 at 14:05 bY 8R
Subnitred:06123/96
: Account No: 367'6
. llerc'Jles, lnco.porateC
Envi ronnrenra :.,tira i rs
i .,,;r lmingron 3E 19{J94
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Hercutes: Bacchus Pond
C6JUD SDG#: tlSPDl - l'l
CATUO ANALYSIS IIAME
459? TCL VoLatites by 3240 - Uater
17?? Thattitmr
1743 ALumrnum
1714 Anriruny
1 746 Bar i ,.an
1747 Beryttiurrr
'I 7/,9 Cadn i unr
1751 Chromitfn'1753 Copper
1754 I con
1755 Lead
1758 l{anganese'1761 Nici(el.176b sil.ver177? ? inc
1848 Uu SUB46 ICP Digest (tot .ec)
7035 Arsenic TR
7036 Seteniutn IR
0259 Hercucy5713 uU SU846 tls Digest
0817 Hater SampIe Pest. Extraction
0917 TCL Peslicides in Uaters
0B'13 BNA tJater Extraction
4679 jCl SU34i> Sem!vor:ari Ies/,]aterS
4679 TcL StiS/,6 Sernivotati Ies/'Jaters
TT
I'IE T HOD
slJ-816 82408
Su_846 6,-rj0A
s'r - 346 5J',l 0A
sll-84,5 6-r'111A
su-946 6J'l0A
su- s{6 6.,'1rJA
su-!40 6i:r1A
s',J- 546 Cl l LrA
Sr,-346 611L1A
S'w--84f, 4ii JA
su-346 5,110A
:,'rJ-845 6'li0A
srJ-3do 6.1'lcA
sr-31i6 6.lt,Jn
St-Sr',5 6.l1Ci\
su-846 l-r05A
S!'316 5,l1CA
su-31.5 6.',1'.!DA
su-345 7{70A
su-846 7i70A
su- 346 35 1 08
su-846 3!81
su-846 3510S
su-846 82708
sH-8,/.6 8?708
Lancaster Laboratofles
2425 New Holland Prke
PO Box 12425
Lancastet PA 11 6A5-2425
7 17 -656-2304 t ax. 7 17 -656-2681
AIIALYS ! 5
TRIAL DATE ANB T!I4E ANA!.YSI
1 07/A3/96 A939 Tracey l,le{f
a7/03/95 192C
D7/n?/96 ?'..?2
c7/D\/96 133f,
c7/c6/96 11r.,
07/42t96 C93A
C7/11/9o A7?l
07/f;4/96 \TZC
Donna R. Sackett
0onna R. Sacke!t
Donn3 R. S.rcketE
0cnna !1. Sackett
Conna i. Sac,tett
CLlnna R. Sacl,ett
conna ll. Sackett
Donna R. SacLetr
)onna R. Sirckett
Donna R. Sackert
9Dnna R. Sackett
)onna :1, Sacketr
Conna R. Sacketr
Donna R. Sackerr
Chcistine {. ConIin
0G:]na q. Seckett
tonni R. Sacketr
lletli s.:r'a.ke.yan!.leIii S. liarkaryen
Harcie A. xatate
)ougl.as D. 9ei rz
Mari a A. Davenport
l'{ark A. R3tct i{f
!,!ar{ A- Ratct i f f
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MEMBERTXIII
LABCRATCRY CI{RONTCLE
5ee re..erSe Srde for e t?ta.,aitcf; 9i 5fr,oal5 ind abtirey,airons 22 l6 Rev 10/30/95
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(I)La ncaster Laboratories
A Thermo Analytical Laboratory
QUALITY CONTROL REPORT
Page: 7 ol
LCS L IMITS
Lou Ht6H
LLI sample No . 253801tJ
CU'6 JUo Grab r,Jater SailiDle
ilcfcul.s: Bacchus Pond
6rouo i,lo- 5i2727ilL'.c!tes, incor-forateC - 9E
S arry: I e
ilD L
Sampte
UI.iIIS
LCS LCS
LCS DIJP RPD
DUP IS
RP9 ,',!S MSg RPO
i592 TCL Volariles by 8240 - Uater
1258 Chtoroilreth;nel. ugl t.I257 Bromornethane5' u'/t3t92 VinyL ChtorideZ. u9/ t
3494 ChIoroethanel. u!,i t
31'97 Methytena Chto!-ide?' ug/t
31.98 Acetone6. us/t
-?499 Caibon 0isuIiide3' ug/'tlt00 1,1 -D i clr loroet\ene
'l . us./ t
35D1 1, I -9 i chIocoethane?- us/ l3503 ch torofonn1. ug/ti':t\ 1,2-, ichtoroethane2. u0/ t
O3''6 2-But;nonr.3. u9/ L
3505 'l , !,'1 -Trichtoroelhane
1. ug/i
35D6 Carborr Tc-trechloride1. ug/t
3:,ir7 \t inyl Acerare2. uc/ t3ii.itl Erorlodich l rlomethanel. ug/t31.D 1,2-0 i':htcropropane
'I . rr9./ Ij: 15 cis- l,l-9ich!.ofop.oprrne1' usli
3t'1 1 Triclil.oroe:irene
1 . ug,'!'3:1?- t i b.onpchi.oromethaneZ. ug/tli ll 1. 1,?-Trichioroethiinez' usr't
3i 1,'. 6cnze le1. ug,/titl0 trans-1, J-ti':htorcpropene1. ug,/t
6 Lp.trK
Earch: l?61341AA
ti-D.
N.3.
N.t.
(.9-
N.:.
\.1.
\.3-
N.-1.
N-0.
tt.!.
N.r-
N.D,
u.0.
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t,t.t.
N.9.
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4
4
l+1
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4
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16
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1,?
73 68
aq a 1
90 82
57 51,
\12 93
67 91
1't -105
1C3 rDC
115 1D9
96 100
6/1 97
1'16 ',: 14
i'11 '!'10
99 104
93 101
97 101
1r5 105
92 96
llh 101
91, '.,Cz
MEMBER
TTEM
Lancaster Laboratorres
2425 Ne,a Holland Prke
PO tsox 12425
Lancaste( PA 1? 645-2425
717-556-2i00 Fat 111-6\'c 256t see reverse;rde ior explanatron of si,mbol5 and abbrevtdttons 2216 Rev ,Orr.rn, {}
LCS LI!.IITS
LOU H I G'd
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(l)Lancaster Laboratories
QI-]ALITY CONTROL REPORT
Pa_oe: 3 of
A Thermo Ana lytical Laborato ry
LLI sample No. 253ELri0
CU-6 JUo 6rab Uater $atnpte
Hercutes: Bacchus Pond
,
; Aeoup lto. 52?7?7
I Hercutes, Inco.porated
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Sarpt e Saopr. e
l.lDL Utl I IS
35'18 Bromo{orml.
1.
SLANK
DUP
RPD l!sD
LCS
DUP
LCS
RPO
us/ t
3521 4-l4ethyt -2'pentanone
5.
3520 2
ug/ t
2'Hexanone7- uq7. ug/t
3522 Tetrachtoroethene1. ug/t
3523'1,1,2,2'IetlacStoroeth.ineZ- ugl I
312t, Totuene2. u9/ t
3525 Ch I orobenzene
7., 9C
65 9l
02 95
1C6 i05
72 9t,
1C5 105
'l L.r1 1 C1
1i0 :09
1A? i 02
1C3 108
104 99
106 1q2
'101 i 0l
.772 -7?9 (2)
105 1f6
97 97
9/' 95
79 79
'71'. - I q1
''.51i '',t,+1 (?)
92 93
59 5!
9t, 95
c)9 101
the LCc.
3b
43
2
26
0
0
2
1
0
5
4
1 ',102
2t 108
'l '!07
1 '10C
098
197
? 1A7
I 101
3t 'l il
1 102
3 rOJ
1 10(
't 100
ugl I
3525 Ethytbenzene?' u9/!
3528 styrene1. uS/t
3529 xyl.ene (toEat)
1. ug/t
5780 trans- 1,2-Dichtoroethene2. ug/L
6258 cis-'1,2-Dich'.oroethene
u9/ t
1722 Tha[ [ iun170. ug/t
'174f Atuminum57. ug/t
17lr4 Antimony15. ug/t
1745 Bariunr?.2 u9/ t
1747 Beryt I iumI.J ug/t
1749 Cadmirmt2-7 u9/|
1751 Chrornium4.3 trg/ t
1753 Copper3.8 ug/t
1751. Tron5.9 us/ |
'1755 Lead18. ug,/ t
175ii !'iangane:e2.9 u9/ t
1761 tl!cket
1766 Si tver
u9./ I
(1)
171,
(1)
c (1)
(1)
(1)
0 {'l)
0 (1)
c ('t)
c (1)
0 (')
(1)
80 120
80 1?O
80 i20
80 120
80 120
an 1?n
B0 120
80 120
80 120
80 '120
80 120
80 120
80 120
I
I
I1.5 ug/t
(1)
(2)
Ihe resuLt for
Thc background
Has tesstines tlte
than five tiotes
spi <e acced.
Lancaster Laboratories
2425 New Holland Prke
PO Box 12425
Lancastet PA 17 605-2425
717-656-2100 Fax. [phone]
I
2216 Rev ,rrr* dt;-fiEHii
I
See re./erse srce ior eroranairon o{::rmbolS and abbrevratrons
I
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(I)Lancaster Laboratories
A Thermo Analytical Laboratory
LLI Sample No. 253301/-\
!U-5 JtlD Grab tJ3ter Samote
Hercutes: Bacchus Pond
Group !,1o.
Ierc!!es,
DUP ltsTFD :'1S HSD RP5I I ac I fq
LCS 9UP RP)
t
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Sarpte SampteI,IDL UXITS
1777 Zinc
1 2. Lrg/ t
7035 Arsenic TR2.7 uglt
7035 Selenium TR2.7 us/ t
0259 hercury0.041 ugl t
0937 ICL Pesticides in garers
BLANK
Eatch: 96'19?1848!02
ti -D.
9atch: 951921818C02ti.!.
8a:ch: 96192 1849C!2ti.r.
Batch:96'1845713tl0l
I,i.D.
Batch: 96i8300rJ5A
N.9.
N.9.
\.i-
N.l.
N.r.
{.9.
ll.D.
N.9.
li.l.
N.?.
N.1.
N.!.
!,t.r.
ll .l-
li.i.
N.D.
N.:, .
0 ( 1) -41 -3/.
0 (.) 1el 102
0 ('l ) 10i 102
0 (-1 ) 79 79
5
,l
1
0
09c
1 101
0 10c
092
172
tt 69
092
283
c9c
082
I 112
197
195
097
l9s
2 9t,
1 lci
291
r_' 86
LCS LIII!TS
LC'YJ H ! 6H
80 120
80 129
80 120
80 120
67
69
66
54
4?
64
60
66
60
67
67
53
71
76
57
75
75
'r 03
103
lCl
93
1600 Atpha 8HC0.0c2 u9/ L1601 Bera gHC
0 .003 u9/ t.1601 9elta Bilc
0 .0C5 ug/ I
1602 Garrna 8HC - Lindane
0 .002 u9,/ t
'I 504 Haptach I or0.085 us/ t
1605 Atdrin
0 .004 ug,/ t1605 Heptachtoc Epcxide0.001 u9/ t
10^tc Endosutfan I
0 .003 us/ '.'16'10 DieLdrin
C .005 ug/ t1607 008
0 .005 ue/ t
1511 EMrin0.005 us/ t1515 Endosulfan I I0.01 u!1/ Ileg8 000
0. CC7 trg/ t
1617 EndosuLfan Strtfate
0 .307 us/ t'16C9 9Dr
0. CUB u9/ t
0.738 Endrin Ketone0.004 ug/ t
1350 r.1e!hoxychi.or0.Ci us./L
13.11 Alpha Chtordane
0 .0C5 0s/ |
13oZ 0arr:ra ChLordane
0. CCs us/ t
96 95
97 a7
85 35
76 76
73 76
87 36
9't 3-1
83 8l
84 8t)
90 a'l
9C g9
92 ?3
9!t 9?
102 102
g'., 9C
86 0-6
12?
120
1?6
120
120
120
12C
120
i20
120
129
120
12't
1?8
121
''20
11D
'120
120
(1) The resutt for one or both detarminations p;s Le:;l thtn irve times the Loo.
KTfN
Lancaster Laboratofies
2425 New Hoildnd Prke
PO Box 12425
Lancastet PA i7 605-24)5
7l 7-656-2100 | ax. 1 11 -5ia ) a?. 1 ,orror$ d'}
QtJz\LrTY CONTP.OL REPORT
See rer€r:e s,cje for exo,anat,on of 5vrco,s ancl abbrevraltons 2215 Rev
QUALJTY CONTROL REPORT
(il)La ncaste r Laborato ries Page: !0 of
A Thermo Analytical Laboratory
LLI sampl-e No. 253,q010
cr-6 JUD Grab'Jater 9alrpte
Hercutes: gacchus Pond
Sarrrpte Sarnpte
HDL UN I iS
Yoxaphene1. us/t
Endrin Atdehyde0.010 us/l
PCB - i 0.160.09 u9/ L
PCB- 12210.2 us/t
PcB - 1 2320.09 us/ t
PCS - 1 14?
0. C5 us/ t
PC3- 1248O.tr/ u.l/t
PC8 - 1 2540.06 us/ t
PC8 - ',l260
A -07 ug/ t
Grouo No. 522727
iiL'rcutes, !ncoiporated - DE
.I
I
LCS LCSLCS DUP RPO
ouP rls
RFD MS I{SD RPD
LCS LII'IITS
LOU HI6H T
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'1o13
1110
1 619
16?0
ioi I
1a?z
I c23
15?L
6 L.ANK
N.9 -
H.D.
N.i' .
[.9.
N.!.
t(.1.
N.!-
ri.D.
N .D.
N.D.
,,t.D.
N.3.
r-,.
N.D.
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r.!.
N.!.
L'.!.
{.!.
N.t.
N_1_
T
I!,67!. ICL SU84o Serrivotari Le./rJarers Batch: 96',]84i.'M026
3918 phenotZ. ul/l
3957 bis (2'chLoroethyt ) etherZ. u9/ t
3'L7 ! 2'ch r.orophencrt
2- ugl t
358i'1,3-dichtocobenzene2. u-c/ t
-i::l)( i,4'dichlorobenzene?' ug//LiSiil '1,2 -di chtorobenzene2- ug./t
4540 2-m'rthytphenol4. ug/ t(i;j 2,2'cx;zbis (1-chIocopropane)
4. ug/t
Lai:Z 4-nrt:thytpherrcl4. ugl tir15 N-ni rrosorji -n-oronylatnine
4. ua.r tar02 hexachlorcettrana
t, . ug,'t
39'10 ni t rcbenzene2' ug'/t32i:! i sopnorone7. ug/ [311i 2-nitr,rphcnott . ug/l
5 112
1? 158
?3 13,i
1 17?
20 i24
32 129
45 1?3
36 166
q 1s2
1 230
40 113
55 180
?1 196
29 182
3 4r,
188
185
170
371
177
2 6/,
078
4 103
851
c94
097
1. 92
t9 47
91 91
83 80
78 32
30 s3
79 82
o,
tL,7 63
83 83
1 10 1'.t1
77 7g
97 97
rc0 100
gt 95
TKrrr
Lancasler Laboralofles
2425 New Holland Prke
PO Box 12425
Lancaslei PA 17 605-2425
717-656-2300 Fax: [phone] Rev ,rrr$ d?' l
I
See revelse srde for explanalron oi:!mbols and dbore?rdtroos
I
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(l)La ncaster Laboratories
QLIALITY CCNTROL REPORT
Paqe: 11 of ',tA Thermo Analytical Laboratory
LLI Sample No. 253E010
CU-6 JUD Grab uate| Saopte
Hercules: Bacchus Pond
MDL
(irouo No. 522727
l-rerc!teJ, incceporated
DUP MSiI?, MS I1S3 RPD
I ac I ac
LCS DUz RP9
3390 2,4-dinrethytphenotZ. usl I
1860 bis (2-chtoroethoxy) nlethane2. ug/ L
3886 2,4-dichLorophenot1. u9/ L
3921 1,2,4-tcichtorobenzene2. ug/ t
3906 naphthatene2. ug,/ t
3871 4-chl.oeoan'i t ine4- ug/tf900 hexachIorobutadieneZ. ug/l
3872 4-chtoro-l -rnerhyl,phenol
1. ug/ l
1905 2-r,tethytnaphthatene?' ug/t
3901 hexach I orocyc t opentad j ene6. ug/l
5921 2,4,6-trichlorophenolZ. us,/ L
i9?2 2,4,5-trichLorophanoL2. u9/ t
3873 2-chLo.onaphthaIene2- uq/ L
3907 2-ni troani I ineZ. ul/t
1891 dimethyt phthalate6' us/ t3858 acenaph thyt eneZ. ug/t
B LANX
N.!.
N.t.
N.D.
ri.].
N.!.
li .'J .
N-!.
N.D.
N.D.
N.D.
N.D.
66 70
90 9C
s6 36
79 31
83 38
65 69
93 93
) I >J
89 Z7
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9., 90
97 97
32 3.1
92 9l
65
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73
BC
41
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95
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LCS LIi'II"IS
LOU HIGH
3? ',r1e
33 184
39 135
ZI IJJ
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2L ',t 16
22 1t7
?9 123
1 100
5 t t\t+
39 151
60 113
53 143
1 112
33 145
7 113
1 191
1 112
38 111
19 rl9
50 15e
4579 TCL SU846 Semivol.ati tes/tJaters Barch: 96184"JAA0?6
3908 3-ni lroani I i neZ. uS/ t
3857 acenaphthene?' usl L
3893 2,4-dini tr'ophenoI10. u9/ !
3912 4-nirrophenot'10. ug/L
3{179 di benzofuran2. t:g/ [
3894 2,4-drni !rotoLuene4. us/ t
3895 2,6-dini trorol.uene2. u9/ [
MEMBEFI
TAEffi
g0 8c
93 9l
t1 i7
95 96
99 10C
1
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Lancaster Laboratones
2425 New Holland Prke
PO 8ox 12425
Lancasle( PA 11 6A5-2425
111-656-2300 tax 711 556')6e :€: re,.,e'se srde ior erplanatron of symbols and abbre,rai;ons 2216 Rev
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(il)Lancaste r Laboratories
A Thermo Ana lytica I Laboratory
^rri\r,Tmv r.nYrrlRnIJ REPoRT
Page: 12 of 14 I
LLI sample No. 25380iC
clJ-6 Jtro Greb Uater garflple
Hercutcs: Bacchus Pond
I Group llo. 522727
I rercu(es, !ncorporated - DE
i
Sanpte SampleM9L UN I TS
3887 diethyl phthaLate14. ug/t
3875 4-chtorophenyt phenyl ethec4. u9/ Ll89B f Iuorene2. us/t
l9C9 /'-nitroan!tine't,. ucl t
trb13 4,5-dini tro'2'methylphenoI10. ug/ t
3911, N-ni trosoCiphenyLarline
l, . u9/'.
3869 4-bcornophenyt PhenYL etherl+. ug/l
3l!99 hexachLoroben:ene?. u!/ L
3t1o pentachIorophenol2. ul.l t
3?17 phenanthrene2. u9/ t
5359 anthracene2. us,/ t
1,631 carbazoteZ. us/ t
3SB0 di -n-butyt phthaIate7. u3l t
7ti97 f ttroranthc'ne2. u9/ t
191.9 pyrene2. u9/ t
3':70 butyt benzyt phthaIatelt. uS/[l3u5 3,3' -dichtorobenzidinc'!4. uglt
3Si,0 benzo (a) anthracerre2. trg/ [
3868 bis (2-ethythexyt) phthaIatc
1' us/t
3875 chry:;ene?. ug/ L
3S96 di -n-octyt phthal-ate
l+ . LIC/ t
3351 benzo (b) f luoeanthene
4. ugl t
3U6? benzo (k) ftuoranthene
1. us/ t
3!'LL benzo (a) Pyrene1- ug/i
3rl0l indeno (1,2,3-cd) pyrene
l, . u9,/ l'
Lancasier Laboratories
2425 New Holland Prke
PO Box 12425
Lancdsrer PA 17 6A5-2425
7 11 -656-2300 lax 7 11 -656-26E1
LCS LIIIITS
LOU HI6H
1 114
25 158
59 1?1
33 122
1 i81
38 1(17
53 "t27
1 1,52
14 176
54 120
?7 i33
/.0 137
1 118
25 137
52 115
1 152
1 )A)
33 143
8 158
17 158
4 1t)6
?r, 159
11 163
17 163
1 171
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DUPRF! !'S
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LCS OUP RPO
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122 98
a:, io
95 0L
9t 94
83 37
92 9C
39 87
90 89
ct3 91
79 73
1C2 101
91 91
90 3S
3l 33
7(, 75
-1 101
/. 98
c86
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285
295
1'1 9A
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289
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084
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6 1C1
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(I}Lancaster Laborato ries
A Thermo Analytical Laboratory
Q'-TALITY CONTROL REPORT
Page: 13 of 'L
LCS LIMITS
LOIJ H ! GH
1 2?7
1 219
LT,f sample No. 25334'lC
CN-L J|)O G|ab :,,;irer g:l0nr,e
Hercu!.c's: Bacchus Pond
SalnpLe S;rnrp[eMDL UII ! TS
3831 dibenz (a,h) anthracene4' us/[
38f,1 benzo (9hi) peryLene
4. uq/ t
DUP !1S
IPl TiS MSD E2D
LCS LCSLCS DUP RPD
94
77
6 LAf.'K
fl.D.
rrcTr
Ldncaster Laborato.es
2-125 Ne.a Holland Prke
PO Box 12425
Laxasrer PA 17605-242t
717-656'2i00 Fax [phone]i31
2
1
5e: .ere ra S de ror gxprJndtron Of 5yTbO.S dnd abOrevratrons 2216 Rev ,arorrt d?
(I)La ncaster Laboratories
LOI
60
60
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A Thermo Analytical Laboratory
LLI sampl-e !.ro. 253801C
CU-6 JUo Grab lJater :iarrpIe
HeccuIes: Bacchus Pond
0937 TcL Pesticides in lJa(ers
4592 TCL votatites bv 8210 - vJirer
/.678 ICL S'tJ346 Spnlivotati Ies,/!aters
4679 ICt- SU346 Senrivolati [3s/'uarars
SURftOGATE SUXI'AAY
IR!AL !D SURROGATE
TCX
D'i0
d1.-1 )-\r1
c9 - rol uene
2-FLphenoI
2henol -C5
2,,'r,6'I82
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2 - i:c i pirny l.
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SUIIRO6ATE LII'!ITS
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79
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LancaSter Laboratofles
2425 New Holland Pike
PO Box 12425
Lancasler, PA 17605-2425
717-656-2300 Fax: [phone]
I
QLIAIITY CONTROL REPORT
see reverse sroe for erplanalon o{ symbols and abbre'/ratrons 2216 Rev.,OOOrn, d3
CAT
[0.
1593
16?5
161,3
1644
1616
1617
1649
IO) :
1 65i
1555
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1666
167?
6935
6936
01 59
4683
4689
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(iI)Lancaster Laboratories
LLr sample No. Es 2538086Cottected: 6127/96 at 10;35 by BR
Subfiitted: 6/?8/96 Reported: 8/ 6/96Discard: 9/ 6/96
Stat 1(18) (6-9r') Grab Soi I Sampte
Hercutes: Bacchus Pond
SI186 sDG#: HBP02-07
I
I Account No: C6716
r HercuLes, !ncorporated - 0E
i Envi rom1enta t Affa i rs
I lJr [mington 0E '19894
I
I
A Thermo Analytical Laboratory P age:
RespectfuI ty Submi tted
Ramona V. Layflan, Croup Leader
ICP He!aLs/Leachates
P.0.
AIIALYS I S IIAME
TCL Votati tes by 8240
Thatl.ium
A I r.rni nr.un
Ant i nony
Bar i um
Beryt t itrn
cadniurn
Chromi um
Copper
I ron
Lead
Manganese
Nicket
s i Iver
zi nc
Arsenic TR
Seleniunr IR
Ile rcury
TcL SU846 Semivotatites SoiI
TCL 5U845 Semivotati tes,/Soi t
Mo i s ture
AS RECEIVED
MET HCD
t:i::,tlii:i,:,,intsur"rs,,:,,,,,, DETEcTt cll L !il I T uN I Is
DRY UEIGHI
:.ii.i:,illil:ir:,iiii::riiirii:iiiliirii rlErHoD
r:. ::.::j.::l :ri::ii8(!.u-Llg,i:::iii: 0ETEC"l' I 0[ L I l'l I I
16.
10.
2,6t.6
0. 086
0.15
0.55
0 .58).v
2.8
0.14
0 .53
0. 52
0. 46
0.29n ,1
0.034
See Page1t-. fle/ks8.7 m9/<9
2 .1 ,ngl <g2.1 nr9/k90.072 ne/kg0.1i mgli9C.46 nrg/(9C.q9 rg/<gi. i :x-alkg2.3 n9/(9
0. 1 2 $g/Kg0.45 ng/<gC.4+ mgl tg
0 .39 nq/ <g
D. :4 irg,/kgC.i7 ng/<g
0. !28 nl/ <n
See Pa-oe
see Page0.05 li by rr.
3
4
"iloisture" repcesents the toss in veight of the sampLe after oven drying at
103 - 105 degeees Celsius.
1 COPY TO
1 COPY TO
Hercutes, Incorporated
ERr.l - Rocky Mountain
ATTN: !'!r. Joseph Ke', Ler
ATTl,l :1,,1r. Brent Rocinson
Questions? Contacl your Ctient Services Representa!ive
Rachel L. Krearner at (7'7) 556-ZlC0
15:29:06 D 0002 ?3 REP 126di6 522fi9510 25.00 001 r2400 AsR000
Lancaster Laborato(es
2425 Ne,ru Holland Pike
PO 8ox 12.125
Ld.ca:ie. 5A ii6C5'.r'r2!
7l:-556-:100 irx ll/.i:r: lirll
tt
il1b ce,., ,Orrorn, ?a j-ilJ(, =, a Aca.e,lAltntj
(I)Lancaster Laboratories I
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Re[.
LLI sanple No. ES 2538086
Cottected: 6/?7/96 at 10:35 by BR
Subnitted: 6/28/96 Reported: 8/ 6/96Oiscard: 9/ 6/96
stat 1(18) (6'9") Grab Soit Sarnpte
Hercutes: Bacchus Pond
S1186 SOG#: HSP9Z'97
CATtio. AIIALYSIS tlAl'lE
TcL votatites by 8240
3431 Chtoromethane3435 Bromoilethane3116 Vinyl. Chtoride3437 chIoroethane3140 Methytene chtoride
4071 Acetone4076 Carbon Disutfide
1'180'l,l'Dichtoroethene3442 1,'l-Dichtoroethane3444 ch Ioroform3145 1,2-0ichtoroethane4085 2-Sutanone3416 1,1,1-Trichtor.oethane3447 Carbon TetrachIoride4091 vinyI Acetare
31,48 BromodichIoromerhane3450 1,2-0ichtoropeopane3t54 cis'1,f-DichLoropropene1181 Trichtoroethene345? 0ibromochloromethane3\53 1,1,2'Trichl.oroethane
1 'l82 Eenzene3151 trans'1,3-Dich(oropropene3156 Bcomofornt4108 4-Methyt-2-pentanone4107 2'He(anone3457 Tetrachtoroethene3449 1,1,2,2'Tetrachtoroethane
1 185 Totuene1184 Chtorobenzene3458 Ethytbenzene4117 Styrene3355 Xytene (tota[)6187 trans-1,2-Cichtoroethene6277 cis-i,2-0ichtoroethene
A Thermo Analytical Laboratory
ui lmington DE '19894
AS RECEIVED
.:,.,.!:l::.:,.i:,.,::i Dddri rc::.|.:il
METHOO
OETECTION LtI.IIT U}IITS
?. ug/kg3. uS/Rg?. uglkg3. ug/'<g2. ug/'<g7. 'Jg/kgl. ugltg?' ugl<g
'.. u9/(9
'l . uglkSZ. ug/kg7. ug/(q1. ug/<g1. ug/\c)3. uglkS7' \g/<gi. uglkq1. ugl<g
1 . ue/kg1. ug/ks2- uglks
1 . u9/k9
'i. ug/kg
1 . u9./ <9l. ug/'Kg
i . 'L9/ <91. u9lk9
1 . u9/k9
1 . uS/kg
1 . u9l(9i. u9l(9
'1 . ,Jq/'<g
2 - u9 /'<g2. usl ks
ORY UEI6HT
:.:.1:r...:.::.::.i:::.:.::...1:.:r.."1.::..:r. .:: r: l{F T H 0D
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,:,:,,,:.j,,. :.'jr,:, :,::,'',:,,.'il.U t:.,,,,
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::.::::,:::::i:i::i:::l :,ij:...M. 3.
ouest i ons? Contact
Rachet'-. Kreamer
your CI ient Services Representative
ar (7i7) 556-2300
Lancaste. Laboraiortes
2425 New Holland Prke
PO 6ox l2ll5
La.casier PA I l;q5-li25
71i-655-:j00 lax i:l-n5i-1531
RespectfuL l.y Submi tted
l'licne[". IcCIarin, 8.A.
Group !-eader, GC/l'1S VoLatites
;ee.e,/:.._i::Cerori,c,.ta;:t.oi:yr.i)c,i-,indaborgyliltons 2:I6
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Account |lo: 06716
i Hercutes, Incorporated - OE
i Envi rormentat Af fai rs
MEMBER
!.er l0/lCi95
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(l)Lancaster Laboratories
LLI Sarnple No. ES 2538086Cottected: 6/?7/96 at 10:35 by BR
Suboitted: 6/?8/96 Reported: 8/ 6/96Discard: 9/ 6/96
Stat 1(18) (6-9'r) Grab Soit Sampte
Heccutes: Bacchus Pond
S1 186 SDG#: HBP02-07
CATIIO. AIIALYSIS IIAME
TCL SU845 Semivotatites SoiI
"1185 phenol
3753 bis (2-ch(oroethyt) ether
1 186 2-ch torophenoI375t 1,J-dichtorob€nzene
1187'1,4-drchl.orobenzene3755 1,2-dichtoroberrzene4690 2-methytphenot4691 2.2'-c.rybis (l-chtoropropane)
1692 4-methytphenot
1 188 N-ni trosodi -n-propyIamine
3757 hexachtoroethane3758 ni trobenzene3759 isophocone3716 2'ni trophenoI37tr7 2,4.dimethytphenot3760 bis (2-chtoraethoxy) methane3748 2,4-dichlorophenot1189 1,2,4-rrichLorobenzene3761 naphtha lene4693 4-chtoroani Iine376? hexachtorobutadienei190 (-chtoro-3-methyl.phenot
469t 2-methytnaphthaIene3763 hexachtorocycLopentadiene3719 2,4,6-trichtorophenoIl+695 2,4,5-trichLorophenol3764 2-chIoronaphthatenet+696 2-ni tcoani t ine3766 dimethyt phthatate3765 acenaphthytene
I Account No: 06716
j xercutes, !ncorporated - DElFnviroruntaL Affaics
I urtminoton OE 19894I'
I
AS RECEIVEO
I{ET HOOftEs'Jtrs::r DETECTIoN tttilT uNlTs
A Thermo Analytical Laboratory Page: 3 of 11
P.0-
Ret.
DRY UEIGHT
,:r!,iiii,:.:r.r:iiiiii'iii:::::,,',i!1i:i,:,.:j: llETHO0
j:iiiii:iii:l.:r;REsUtIs'i.'11:.1' DETECT I oll L I M I T
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:::.::::i:::1::::.j::::;::. :::::li.::D.::::i:: 200.
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ouestions? Contact you. cIient
Rachet L. K.eanrer
Servr ces Repteseotat lveat (/1 7) 650-2iC0
Respectiul Ly submi tied
Christine It. Ratclif{, B.S.
6roup Leader, GC,/l$S
ffiaiE
LanCaster Ldboratofle5
2425 tlew Holland Prxe
PO 8oY lji25
r-dn(a-)i:. PA I :ea:-: rr:l
;r;'a:o-l;00 ii( ;'; '-:'i'f-3
e2
... ?.o:.:F f?
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(l}La ncaste r Laborato ries Pag e:
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A Thermo Analvtical Laboratory
Servi ces Representat i ve
at (7'7) 656-2300
P-0.
Re[.
Respectfut ty Submi tted
C5l-istine :1. Rarclif{,
Group !eaCer, GClMS
. - a.a \ ,a.a:, ar:rerral,ons
4 of 11
LLI sample No. Es 2538086Cottected: 6/?7/96 at '10:35 by 8R
Subnritted: 6/28/96 Reporred: 8/ 6/96Discerd: 9/ 6/96
stat 1(18) (6-9") Grab SoiI Sampte
Hercules: Bacchus Pond
S1186 SDG#: HBP02-07
CATNO. AIIALYSIS }IAI{E
TCL SU846 Semivotati tes/Soi t
4697 3-ni troani t ine
1 19'l acenaphrhene3750 2,4'dinitrophenot119? 4-ni trophenot4698 dibenzofuran1193 2,4-dinitrotoIuene4699 2,5-dinitrototuene3 70 diethyt phrhaLare
3769 4-chlorophenyL phenyI ether3768 fluocene4700 4-ni troani I ine
4701 4,6'dini tro-2-methytphenoI3nZ N-ni trosodiphenyLamine3773 4-bromophenyl phenyl erher3771 hexachtorobenzene
1 194 pentach Lorophenot3775 phenanthrene3776 anthcacene4702 carbazote37Tf di -n-butyt phthaIate
3778 ftuoranthene
1 195 pyrene3780 butyt benzyt phthatate
3783 3,3' -dichIorobenzidine
3781 benzo (a) anthracene1784 bis (2-ethythe,(yt) phthatate37BZ chrysene3785 di -n-octyI phthal.ate3786 benzo (b) ftuoranthene3787 benzo (k) ftuoranthene3788 benzo (a) pyrene
3789 indeno ('1,2,i-cd) pyrene
3790 dibenz (a,h) anthracene3791 benzo (ghi) perytene
AS RECEIVED
:r:::i:ii1t:j:::i:i+:::::i:r::ai::::i.::.::i::::ii: I'(ETH00
iii:.:n::iliil:|i*g8t II,qt:,* DETECTI0ll LIr,rIr uNtrs
DRY UE!GHT
;::::::.:::ii:;:i.i:::ir::;::::j::::ir:.:.::::::..::: METH00
ili:iili:i;:8!ilEis ;';:rii: o Er ec r t oN r- t u I r
40.
200.
200.
40.
80.
80.
80.
80.
40.
120.
2C0.
1?0.
120.
?00.
10.
40.
40.
40.
40.
80.
80.
'150 .
40.a,t
40.
80.
80.
t6u .
80.
30.
Io/ .
33.
17C.
17C.
33-
6i.
67.
67.
67.i5.
101r.
174.
't00.
'100 -
17Ll .3i.
13.
33.
??
il .
67-
67.
110.
13.
67.li.
67.
130 .
67.
67.
67.
67.
u9/k9
uglkg
ug/ks
us/k9
u9/ (g
rr9l (g
,rgl <9
u9/ is
uo./ <g
ug/ <g
'J9l <g
19/ <9
ug/ kg
u-o/ iq
ug/ <9
u9/ (g
u9,/ (9
ug/(g
ug/kg
u9/?g
u9/'<g
ug/ kS
ug/<9
u9/ (9
ug/kg
ug/kg
ugl k9
ugl<g
u9/'<9
ugl <9
u9l <g
'tg/ <g
.g/ <g
u9/ (g
Questions? Contac! your Ct ient
RacheL L- Krea(ner
Lanca5ter Laboratofles
2425 New Horland Prke
PO 8or I2425
Laocastea PA I 7509-:j125
717-656-2100 Fdr 717-a-ia-2ria I r:: ilMEMBEFI
)ee aev9t5;l2 l6 ie., l0/r'ilrg:
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(D Lancaste r Laboratories
LABORATORY CHRONICLE
Page: 5 of 1-1A Thermo Analytical Laboratory
LLI sample No. ES 2538086CoItected: A6/?7/96 ar '10:35 by BR
Suboirred: 06/28/96
Stat 1(18) (6-9") crab Soit Sanpte
Hercutes: Bacchus Pond
Sl 186 SDG#: HBP02-07
CATiIO AIIALYSI S NAME
4595 TCL Votatites by 8240
i Account tlo: 067'16
i ttercutes, lncorporated - OE
r Envi l.onitental Affai rs
I ur lmington DE '19894
I
ANALYS I S
TR: AL DATE ANO T IIIIE ANAI.YST
1 07/03/96 C611 Ctark A. Dougherty
1625
1643
1611
16t,6
1647
'1649
155',l
1 653
I b)4
1 655
1 558
rool
1 600
\672
5708
6935
6936
ThaLLium
Atuminum
Ant i mony
Bar i urn
EeryLLium
Cadnri urn
Ch romi um
CDpper
I ron
Le3d
t{angane$ e
N i cket
Si tver
Zirrc
SU 5l.1846 I CP 0 i ges t
Arseni c TR
seIeniun TR
07 /13/96
07/',3/96
a7 / 13/96
07 / 13 /96
0T / 1.3 /96
07 / 11 /e6
07 / 13 /96
A7 /':i/96
07 i 13/96
07 i',3/9b
07 / ",3 /96
07 /':3 / 96
C7 / ''i1c16
07 /'3/96
07 /02/95
a7 /..3/95
07 / 17 /96
1 803
1B0l
1803.1803
'1803
'1801
1 303
1 805
18113
1 803
1303
1303'r801
193t,
1 803
091 E
07/0t+/96 11t+8
07/02/96 lAUl
07/01/96 193A
07/05/96 150?
a7/05/96 150?
07/10/e6 1355
JoLene 14. SchieLCs
Jotene 11. SchietCs
Jotene itl. Schietcis
JoLene i!. Sch ietds
JoLene il. Schietds
JoLene l'1. SchietCs
Jo L ene i!. Sch i e Lcis
JoLene ll- Schielcis
JoLene itl. SchieIds
JoLene tl. Schiel.ds
Jotene ltl. Schietcis
Jotene H. Schieids
Jotene ll. Schietds
Jotene rl. SchieLcis
0esi R- Carozza
-ro L ene iY. Sch i e tds
llrna C. HaIter
NetLi S. Markaryan
Desi R. Carozza
Sherry Lynn Devtin
Joseph tl. Gambter
Joseph M. GambLer
Neetay 8. Mehta
METHOO
su-846 82408
su-846 6010A
su-846 6010A
su-346 6!r0A
su-846 6C10A
su-846 6rl't0A
su-346 6010A
su-846 6010A
su-846 60't0A
su-346 6010A
su-346 60 r0A
su - 846 6l 't 0Acrr-n/i ()r,a^
su-346 601CA
su-346 6C't 0A
su-846 10504
sil-846 60i0A
su-845 6C10A
su-846 747iA
SU'846 7471A itodified
su-846 3550A
su-846 82708
su-846 82708
EPA 160.1 (modified)
0'159 t''tercury
5711 SU SlJ846 99 Digest
0381 BNA Soi I Extraction4688 TCL Su846 Serni votat i Les Soi t1689 TCL SU846 Senrivotati Les/Soi t
0'l 11 l{oisture
t9?oJ
L6n(aster Laboratofles
2425 New Holland Prke
PO Box 12d25
Ldlcrsier PA 11605-iJl::il-5i5-2:'00 Far 71i.::5,r -l5dl
MEMBEFl
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RPDLCS
HS
RPD
La ncaste r Laboratories
A Thermo Analytical Laboratory(I)QUALITY CONTROL REPORT
Page: 6 of
LLI sample No. 2538086Stat 1(18) (6-9") Grab Soit Sarnpte
Hercutes: Bacchus Pond
I
i Gcoup |,1o. 522739
i Hercutes, incorpoaated
I
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OE
Sampt e
MDL
Sampt e
UHITS
DUP
RPD lsD
LCS
DUP
LCS LIIIITS
LOU HI6ii
4595 TcL Votatites by 8240
BLANK
Batch: E96183148
N.D ,
N.D.
N.D.
ll.D -
3434 ChIoromethanez- uslks
3135 Bromomethanel. us/kg
3436 vinyl. Chtoride2. uglkg
5437 Chtoroethane3. ug/kg
3440 Methytenc ChLoride. 2. ug/ks
4074 Acetone7. uglkg
4076 Carbon Disutfide3. us./ks
1 1 80 1,1 -Di ch IoroetheneZ. us/ks
344? 1,1 -0 i chtoroethane
2.
N.0.
N.D.
N.0.
N.D.
t{.0.
H.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.0.
N.D.
N.D.
N.D.
il.0.
N.0.
J uqlkg
90 37
99 98
104 100
91 ':01
142 99
oo ao
1C2 ',l 00
107 101
99 95
96 95
93 92
'102 84
't05 105
104 ',t 00
99 81
9? 90
9B 98
96 98
'lc9 107
90 87
9t, 92
98 A6
93 9?
1 27?
1 241
1 250
'10 254
i 221
19 150
24 188
1 233
59 155
51 138
49 155
2? 1b7
52 162
70 140
19 190
35 155
1 209
1 226
71 157
53 149
52 150
37 151
17 l8i
et_
)215 ?er'.,r0'r, ?ti
3
2
5
10
3
a1
2
6
4
?
1
20
1
3
20
2
0
2
2
J
2
2
1
95
95
1,02
B9
95
QO
't 0i
105
95
95
91
95
105
101
105
95
'101
1C2
111
g6
98
'104
98
uslk9
3441 chtoroform
'1 . ug,/kS
3l+15'1,2-Dichtoroethane2. us/kg/.085 2-Butanone7. ug/kg3446 1,1, 1-IrichIoroethane1. uglkg
341+7 Carbon Terrachtoride
'1 . us/kg
4091 Vinyt Acetate3. u9lk9
3448 Bromodi ch IoromethaneZ. u9/k9
3450 1,2-Dichtocopropane
3 . u9/ k.9
3454 cis- 1,3-0ichtoroP.opene
't.
1.
1.
'1 .
1
us/ kg
1 1 81 Tr i ch Ioroerhene
ug/kg
3152 DibrornochLoromethane
us/k9
3453 1,1,2-TrichtoroethaneZ. u9/k9
'l 182 genzene
1. ug/kg3451 trans'1,J-DichIoropropene
ug/k9
Lancaster Laborato(es
2425 New Holland Prke
PC 8ox 12115
Ldncaslei PA 1 7505-:J:5
lrl-655-ll0C Far ill'c5b-i53i ,ee 'e re';: :,t-a :Or i\Plaria ;;,rool;..ii:.j 3c;.e"tairo;r5
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Group llo. 522259
, Hercutes, lncoroorated - DEi
I
QI-IALITY CONTROL REPORT
Page:
LCS LIA{ITS
LOU HIGH
45 169
50 124
52 140
61 143
46 157
17 150
37 160
37 162
74 136
30 200
54 156
54 156
50 150
50 15s
21 299
70 131
?3 177
Zb 17t
54 141
57 145
53 112
69 115
55 116
50 147
'1 1
SampLe SampteI'!DL UH I TS
31.56 Bromoform
1 . u9/k9 N.D - 8S 834108 4-Hethyt -2-pentanone
3. u9/k9 N.o. 9g 914107 2-Hexanone3. uslkg N.c. lot 903457 Tetrachtoroethene1. us/kg N.D. 'l 15 't l03449 1 , 1 ,2,2-Tet rach I oroethane1. ug/kg ll .D. '100 9/.
1 183 ToIuene1. uslkg N.D. rC5 101
1 1 84 Ch I orobenzene
1 . ug/ks [.0. 96 963458 Erhytbenzene1. us/ks N.D. 107 104
41 17 styrene
'l . u9lk9 N.D. 99 923355 xylene (tota[ )1. us/ks N.D. .lD5 1015187 trans-1,2-Dichr.oroetheneZ. us/ks I.9. 104 986277 cis-1,2-Dichtoroethene?. u9/k9 N.O. 105 1011625 ThaLtir.rn Eatch:96.1845708!0314. mg/kg r{.0. (t) 93 89
1643 Atuminun Barch: 9618457000038.7 ms/ks N.0. 21 2A27 16t5 (2)
1644 Anrirrony Barch: 9618457080032.1 ng/kg N.0. (l) c;? 95
1546 Baritin Barch:961845708.1032.1 m9/k9 N.D. 9 I 05 97
1647 EeryLtiun Barch: 9618457033030.072 mg/ks N.D. 0 (1) 96 91
1649 Cadmitrn Batch: 961845708C030.13 mg/ks N.r. 0 (1 ) 93 38
1651 Chromiun Batch:96'1845708110l0.46 m9/k9 N-0. 0 (1) 1?g 1ll
1653 Copper Eatch:961845708C03i).tq m9/k9 N.0. 0 (r) 119 109
1654 Iron Barch: 96184570e8011.3 ms/kg 7.2 ) ffs/k) 13 2152 2',39 (2)
1655 Lead Batch: 9613457031012.3 m9lk9 N.D. 0 (1) gtJ 90
1658 Manganese Batch: 961845708t030-12 m9/k9 N.D. lj 116 109
1661 lickel Batch:961845708!030.45 ms/kg N.9. 0 (1) 9i 9t
1666 Si lver Earch: 9618457081010.44 ng/kg \.D. (1) t.:2 97
(1) The result for one or both determinations uas tess than five times the Loo.(2) Ihe background result uas mofe than four times the spike ac]ded.
Lancaster Laboratoiler
2425 New Holland 2rk€
PO 8ox l2J"-5
LdncJlie. PA l;5lr :l-,':7t7-6;a,:l0Lr ;.:, - -.:i,: ,r-i!
OUP TS
RPD MS I'SO RPO
LCS LCS
LCS DUP RPO
693
790
12 91
/t 't 15
797
1 101
c97
3 108
7 101
2 106
6 101
4 102
696
979
279
7 100
598
799
't 102
6 1D2
489
794
591
696
798
e!'
r,tl": L;
(il)La ncaste r Laboratories
A Thermo Analytical La bo ratory
LLI SampleStar 1( 1B) (6-9'r)
l{ercutes: Bacchus
No. 2538086
Grab SoiI Satnpte
Pond
MEMBEFl
't::'1--',: :"''r:rC : a iat)te\! a|:a-
(iI)La ncaste r Laborato ries
QUALITY CONTROL REPORT
Page: 8 oiA Thermo Analytica I Laborato ry
LCS L ITIITSLOU HIGH
5t, 149
49 149
5? 149
?3 157
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LLI sample No. 2538036Stat'l(18) (6-9") C.ab Soil. Sampte
Hercutes: Bacchus Pond
Group No. 52289
liercutes, lncorpofated ' 9E
Sarpte SampteITIDL UII I TS
1672 Zinc0.39 mg/ks
6935 Arsenic TR0.21 mg/ks
6936 Seteniun TR0-17 mg/ks
0159 ttercury0.028 ms/ks
BLANK
Batch:9518457080030-80 J rF.g/kg
Batch:961845708003
N.D.
Satch:961845708C03
N.D.
Batch:9618457'11003
t,l.D.
0(1) 108 98
0 (1) 91 92
0 (1) 92 94
0 (1) 83 81
LCS LCS
LCS DUP RPD
ouP t'ls
RPD MS IISD RPD
6
0
,l
2
92
93
66
4688 rcl sLE45 semivoLatites SoiI Batch: 96i83s16025
1 1 85 phenot31. ug/kg
3751 bis (2'chto.oethyt) ether67. ug/ks
1 186 2-chtorophenoL33. uglks
3754'1,3'dichtorobenzene33. ug,/kS
1 '1 87 '1 , 4 'd i ch t ocobenzene31. ug/ks
5755'1,2-dichtorobenzene33. uslkg
4690 2-methytphenotir7. ug/ksl+691 2,2' -oxybis ('l -chtoropropane)
1 00. uglkg
4692 4-methytphenot100. ug/ks
1188 il-nitrosodi -n'propytamine
67. ug/kg
3757 hexachtoroethane
67 - uglkg
3758 ni trobenzenell. uslkg
3759 isophocon..67. ug/ks
3746 2-ni tcophenoI67. ug/kg
3717 2, t*-diarethyl.phenoL
67. ug/ks
3760 bis (2-ch(oroethoxy) methane33. ug/ks
3748 2,4-ijichtorophenoI31. ug/ks'l'l89'1,2,4-trichtorobenzene
3l- ug/kg
3761 naphthalene31. ug/kg
N.0.
N.D.
N.D.
7Z
75
69
75
74
72
69
62
7L
75
77
aa
pl
84
78
79
to
77
80
70
97
8l
9Z
82
57
ot
81
82
13
'1 1
12
6
15
11
111
13
'10
10
9
17
11
'11
6
5
76
IJ
76
76
71
62
90
80
78
87
76
t,1
75
78
75
5
la
t5
i
,n
32
46
36
5
1
40
35
?1
?9
32
53
39
l+1
)l
112
158
t)4
1?t+
129
1?3
160
152
230
I l)
196
1A)
119
184
135
1 /.)
IJ)
q8
T3
71
77
(1) The resutt for one or both determinations gas less than five the 100.
Lan(aster Labo.ato.e5
2425 New Holland Prke
PO Box 12425
Lancasre( PA 17605'2415
71;-655-2300 Fcx 717-656-.1561
MEMBEFl
Sez,et"';i -::'a'..a.a' al01 )r i/ :'c: ;a_c idcririlt.cns :, :;,/ltj. ?-<
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(il}Lancaste r Laboratories
A Thermo Analytica I Laboratory
QUALITY CONTR.OL REPORT
Page: 9 of 11
L IMITS
NIGH
LLI sarnple No. 2538086Stat 1(18) (6-9,,) Grab Soit Sampl.e
Hercutes: Bacchus Pond
i 6rouo l,lo. 5227J9
I hercuLes, Incorporated - DE
i
I
Safpte SafipteI.IDL UII I TS
4693 4-chtoroanitine100. ug/kg
376? hexachtorobutadiene67. ug/kg
1190 4-chloro-3-methytphenot67. ug/kg
4691 2-methylnaphthatene35. uslkg
3763 hexachtorocyc(opentadi ene170. ug/kg
3719 2,4,6-trichl.orophenoI67. ug/kg
4695 2,4,5 -trichtorophenoI
67. ug/kg
3764 2-chtoronaphthalene53. us/ks
4696 2-ni troani L i ne67. u9lk9
3766 dimethyt phthalate33. us/ks
1765 acenaphthytene33. uglkg
4697 l-ni troani Iine67. us/ks
'l '191 acenaphthene33. ugl kg
3750 2,4-dini trophenoI'170. u9/k91192 4'nitrophenot170. ug/ks4698 dibenzofuran33. ug/ks'1193 2,4-dinitrototuene67. u9/k9
4699 2,6-dini trototuene67. u9/k9
3770 diethyl. phthaLate67. uslkg3769 4-chLorophenyt phenyI ether67. uglks
3768 fluorene33. ug/kg
4700 4-ni troani I i ne100. u9/L9
4701 4,6-dini tro-2-nrethylphenot170. ug/ks
LCS LCS LCS
LCS DUP RPD LOU
DUP I.IS
RPD I(S I,ISD RPOBLA}IK
il.0.
N.0.
[.0 .
N.t.
N.C.
N.0.
N.9.
!1.0.
N.D.
N-!.
N.9.
11 15
80 s7
75 36
71 82
l/ 16
8i ?0
gir 39
79 35
7? 75
79 87
7' 31
10 56
973
863
675
876
790
10 85
10 Bl
10 Btl
779
176
966
36 40
71 78
59 65
7t, 80
8? 8e
31 39
79 88
79 87
7t- 30
59 62.
66 72
9
IJ
'10
7
11
10
I
8
10
e
43
81
a1
78
62
B2
82
79
75
BO
77
17 '116
?4 116
22 147
28 123
'i 100
37 14t+
3e 151
60 113
)) tqJ
" 112
3l 145
7 1t3
.tl lq)
1 191
1 132
23 111
39 139
50 158
1 11t+
?5 158
59 121
13 122
1 18i
4689 TCL SU846 Semivotatites/SoiI Batch: 96183S1S026
N.0.
H.0.
[.0.
N.0.
N.D.
N.D.
N.0.
N.D.
N.D.
N.D.
r,l -D.
[.D.
Lan(asier Laboratofies
2425 New Hollanci Prke
PC Box 12425
L3n(is;er. PA I1505-2J:5
7r ;-655-2300 F.r ;'r,;ie.,"j.i i
€)?
"r, '..rrorr, ?o j:ie :.re.:c _ ..lp '^r o.9'4ir:.on oi -,r-hots jad ticc'evtdltoes
(I)Lancaster Laboratories
A The rmo Ana lyti ca I La bo rato ry
QLTALITY CONTROL REPORT
Paqe: 10 of 1 1
LCS LI!.IITS
LOU H I6ii
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LCS l-CS
LCS DUP RPD
itsI.ISO RPD
DUPRPO MS
LLI sample No. 2538086stat 1(18) (6-9") Grab soit Samote
Hercutes: Eacchus Pond
Grouo !,1o. 522259
ilercutes, lncorporated - DE
Sarpl. e Sampl eI.IDL UH I TS
3n? I'ni trosodiphenyIamine
67 - u9/k9
3773 4-brorrcphenyt phenyI ether
1 00 . u9/k93n4 hexachtorobenzene100. us/kg
1194 pentachtorophenot
1 70. ug/kg
3775 phenanth.ene53. u9/k93n6 anthnacene33. ug/kg
47OZ carbazote31. uglks
3777 di-n-butyt phrhalate33. trglkg
3n8 ftuoranthene13. us/ks
1 195 pyrene67. ug/kg
3780 butyt benzyt phthatate67. ug/kg
37A3 3,3' -dichtorobenzidine130. uglkg
3781 benzo (a) anthracene33. ug/ks
3784 bis (2-ethythexyt) phthaLate67. ug/kg
3782 chrysene33. us/kg
37BS di -n-octyt phthatate67. uglkg3786 benzo (b) ftuoranthene67. ug/kg
3787 benzo (k) ftuoranthene130. us/kg
3788 benzo (a) pyrene67. us/ks
3789 indeno (1,2,3-cd) pyrene67. uslks
3790 dibenz (a,h) anthracene67. ug/kg
3791 benzo (9hi) perylene67. uglkg
0111 l.toi sture0.06 % by ct.
BLANK
74 84
81 92
8l 91
7!* 76
7' 33
7t 31
7t, 79
30 90
73 BC
83 9?
36 97
55 58
77 83
93 103
s2 89
81 92
73 80
77 35
7t, 81
22 89
83 91
79 85
/5
BO
82
6J
77
aa
86
77
91
95
68
BO
103
B5
101
80
86
78
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168
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Lancaster Laboralo(et
2425 lJew Hollano Prke
PO tsor 12425
Llrca ji?r PA i76i)5-21:5
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(iI)La ncaster Laboratories
A Thermo Analytical La boratory
QUALITY CCNTROL REPORT
Page: 1': of 11
SURROGAIE LIHITSLO|J H I6H
70 1?1.
LLI sample No. 2538086Stat 1(18) (6-9") 6rab SoiI SampLe
Hercutes: Eacchus Pond
4591 IcL votatites by 8240
4688 TCL SU845 Semivotatites Soit
4689 TCL S|JS/.6 Semivotati tes/Soi L
I; 6roup No. 522f59
i ilercules, !ncorporated - DE
I
I
TRIAL !O
SURRO6AIE SUI.!I.,!ARY
SURNOGATE RECOVERY Z
d4-1 ,z-DcA 91
c9- roluene 94SFB 9i
Phenot -d6 80
l-t lDhenoL a.
?,4 ,o'igP 79
N i t rooz -d5 SB2-Fbionnyl i7
ipten/ Ldl 4 c9
31
74
117
121.
24 113?5 12".
19
aa
i0 lt5
13
120
Lancasier Laboraiories
2425 New Holl;nd Prk€
PC Bct 12 r)\
L.).(.1:'er ci ;aa:-l :
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La ncaster Laboratories
A Thermo Anallrtical Laboratory
CAT
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LLI sample No. ES 2fi8}71Cottected: 6/27/96 ar '11:20 by BR
Suunirted: 6/28/96 Reported: 8/ 6/96Discard: 9/ 6/96
Stat 2(?A) Gcab SoiI Sampte
Hercules: Eacchus Pond
STI2A s0G#: HBP02-01
Account No: C6716
HercuIes. lncorporated - DE
EnvironmenraI AffairsHilmington !E '19894
i P.0.r .let.
!
I
i
r,1E T r,i00
OETECTICIi I.IHIT UNITS
DRY IJEIGHT
::',::i::l1:ll:: l::'.'li. i'ii:i l':'.,: : ":fi':':,! ltE T H00
..:'i:;.i::::,: REIUUTS . OETECTIOH L]HITANALYS I S IIAME
TCL Votati tes by 8240
Thattiur
A I uni nurn
Ant i mony
Bar i um
Bery(t'iun
Cadnri un
Chromi um
Copper
I ron
L ead
Manganese
liickeL
St Iver
Zinc
Arsenic TR
seteniUrIr TR
llercucy
TCL StiB46 S.mivolati tes Soi t
TCL SU846 Semivolati tes/Soi t
I'lo i s ture
AS RECEIVED
4593
1625
1643
164t,
1646
toq I
1619
1651
1 653
165t
1 655
1 658
I06 I
16o6
167?
6935
6936
01 59
4688
4689
01 t1
lq-
8.9
2.2
0.073
0.13
0.47
c.50
3.4
?.4t:- z
n./.6q.n5
r-1 . 4,-io 2s
0.18
0 .028
Joseph Kel. ler
6rent Robi nson
See Page
tig / k9
m9/k9
n9/kg
ms/ kg
n9/kg
nlg/ kg
nrg/ kg
mg/'<c)
m9/ kg
mq/ kg
m9/ i(9
ntg,rkg
m9/ k9
ilgl iq
nrg/ k9
rng/ k9
n9/kg
SL'e Page
See Page
19.
12.
2.9
2.9
0. 099J 0.1,7
0.63
c.67
4.5J 3.2
0.16
u.o I
0. 6c
c. 53
0.31J c.24J 0. c38l
t0.06 7,. oy vr
"Moisturefl represents the Ioss in weight oi rhe sampLe after ovc-n drying at
1C3 - 109 degrees CeLsius.
4)-t
1 CoPY TO HercuIes, lncorporated
1 CoPY T0 ERH - RockT Yountain
0uestionS? Contact your Cticn: Sc.\'Je\ ,lepresentative
a: (7 7) 656.210r,jRachel L. Krearner
1l:21:27 0 0002 23 REP31C 65.00 001164OtJ ASRC9C
RespectfuI ly Submi tred
n6nroaa V. Layilan, Croug LeaJer
ICP l,leiaLs/Lea.hates
rR$lt-d
Lan(arter Ldbo.dtones
2425 l'lew Holland Prke
PO Box 12.125
Ldncasier PA 17505'2d25
71/--6t5-DAA Fax il7 c!r:,>99.e,.,erse ;iie lor E.,it,dnatron oi iymcois ano abbre,/rattons
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Page:
DRY UE I GiIT
i:::::i::i:ii:.:.::rj:::::i:::.:::: IIETHOD
'RESULTS.:',.,:,,. 0ETECT!ON Ll MIT
Account No: 05716
Hercutes, lncorporated - DE
Envi ronmenta I Af fa i rs
Ui lmington DE 19894
(l}Lancaster Laboratories
A Thermo Analytical Laboratory
Subnitted: 6/28/96 Reported: 8/ 6/96Discard: 9/ 6/96
Stat 2(2A) Grab SoiL Sampte
Hercutes: Bacchus Pond
sIT2A SDG#: HBP02-01
CATIIO. AIIALYSIS IIAI.IE
IcL votatj tes by 8240
3431 Chloromethane3415 Bromomethane3136 Vinyt Chtoride3437 chtoroethane3q40 llethytene ChIoride4O7r, Acetone4076 Carbon 0isutfide
1 180 1,1 -Dichtoroethene
3142 1 ,1 -O i ch Loroethane3t,11 Chtoroform3415 1,2-Dichtoroethane4085 2-Butanone3416 1,1,1-Trichtoroethane3447 Cacbon Tetrachtoride409'1 v inyI Acerate3448 BromodichIoromethane
l/.50'1,2-Dichtoropropane
3451* cis-1,3-0ichloropropene1181 Trichtocoethene3152 0ibromochLoromethane3453 1,1,2-TrichLoroethane
1 182 Benzene3151 trans-'1,3-DichIoropropene3456 Bromoform4108 4-ltethyt-2-pentanone/*1O7 2-Hexanone3457 Tetrachtoroethene3149 1,1,2,2-IerrachIoroethane
1 183 To Iuene
1 18/' Ch torobenzene3158 Ethytbenzene1117 Styrene3355 xytene ( totaL )6187 trans-1,2-0ichloroethene6277 cis-1,2'Dich!oroethene
II p.o.I n"l.
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A9 RECE IVEO
ME'I HOO
DETECTICN LtI.IIT UNITS
ugl kg
u9/ kg
ugl k9
ug/kg
u9/ <g
u9l kgrg/\!
ugl <g
'Jglkgu9/ t-g
ugl <9
rgl ig
u9l k9
ugl k9
ug/ t c.
u9/ kg
ugl (g
ug/ <g
u9/ kg
u9/ (g
ugl ks
rs/kg
u_q/ k9
u9/ K9
u9l k9
usr/ kS
u9/ <9
ug/ 1g
ugl kg
u9lks
u9/ (9
u9/kg
u9/ \9
uglkg
'r9/\g
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ouestions? Contact your Ciient
RacheI L. Kreamer
servi ces Repcesen:ai tve
at (7'7) 656-210tr
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Lancaster Ldboratofle5
2425 New Holland Prke
PO 8ox 12425
Lancai:er PA 116A5-iJZS
717-65'5--2i00 F.:r Ii;-65o-.i5,il
Respectfut l-y Submi tted
Iicnei.- $cCia.!n, g.A.
Group LeadL-r, 6Cll':9 \iotat i Ies
See,everse;c:':':.i':tottoec';,-roo,sanoabbrev,alrons 2716 d',* I
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(I)La ncaster Laboratories
A Thermo Analytical Laboratory 3 of 1'l
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t2l6 acr ,o'ro,'., ?a*
Page:
LLI sample No. ES 25380'71Cottected: 6/27/96 at 1'l:20 by BR
subritted: 6/28/96 Reported: 8/ 6/960iscard: 9/ 6/96
Stat Z(2A) Grab Soi I Sampte
Hercutes: Bacchus PondsIT2A SDG#: HBP02-0'l
CATIIO. A}IALYStS HAME
TCL SU846 Semivotatites SoiI
1 185 phenoI3753 bis (2'chtoroethyl.) ether
'1 '! 8c 2 - ch I oropheno I3754 1,3-dichlorobenzene1187 1.4-dichtorobenzene3755 1,2-dichtorobenzene4690 2-methylphenoL
t 69', 2,2'-oxybis (1-chtoropropanel
4692 4-methytphenot1183 N-nitrosodi-n-propytamine3757 hexachtoroethane3758 ni trobenzene3759 i sophorone37!"6 2-ni trophenoI37t-7 2,4-dimethytohenoI3760 bis (2-chtoroethoxy) methane
37..E 2,4-dichtorophenoL1189 1,2,4-trichtorobenzene376i naphthatenei+693 4-chtoroani !ine37oZ hexach Lorobutadi ene1190 4-chtoro-f-methytphenot169t 2-methytnaphrhatene376j hexachlorocyctopentadiene3719 2,4,5-trichtorophenot4695 2,4,5-trichLocophenot3704 2-chIoronaphrhalene4096 2-ni rroani I ine3766 dimerhytphthatate3765 acenachthyLene
] A".ornt tlo: 067]6
I Hercul.es, lncorporated - DE
i Env i rorrnenra t Af fa i rs
: ur l.*i^9ton l€ 1989/.
I
P.0.
Ret.
AS RECEiVED
METHOC
DETECiI9!.1 t_!HIT UfiliS
DRY UEIGHT
::.,:l:.ila:ii:i::i!:iiliti:l:!.,,,lli:i:l'.ii:!l!:.:',: METHoD
::il:,i::,:r::,::::tEF!luII .:ii:l, DErEcr I oN L : H t r
: .:::.i:l::r:::jil::::::,trIiDllrr.::i: 45,
: :::: ::r ::::::.i:: it i:::::!{ r A. ::::ti, 90.
I l':,.i, ..',i..'. tl..tii. .,,i!;.-O:. , i.:i; 49 .
1(
t.!.l,...i. i.,tiit:,t,,,t',,.,.'l...l{,J-...:!i:: 45.
.,,,,.',i.:.,,,.,1,1,i,.r;.,,.,,. 45.. l:' , .,\..)....: 90-:' ... N-.D.. .: 130., :, ,: ::. ' ,,, r' ., .::. 1 ?^
.' . .,....:., ..tt.9. ' 9C.
r ..... i,.,,-i,.,,.,:.,.i.Nir:;,,' r 90.: .,: . : ,: :1, l:::::ll:O:;::::,: 49.
, .l,t,.,.:.l:tl.,. ,t,,.,.llX:,O.. .'l 90.r'.:' ,1 ,,i:,.:,l:,i ,iliDl,:.,',. 90.: -. .t ',,i.: ,,'.:..1,:ll:illitt; 90.
, : , ..i : .t:. t;i'i:.:i ii:...ii.' 1.lli;iD,i.i..ii:: 15 ...u,u... {).
'i, l :,. i:.:,i i.:,,'.,,,',., !i'il{::}':.,1,i:',' 45 .,.,....r.,.,.,',,,.|{..,ar.,.i:, 15.. .;;';... :. , . .. li,, )i' . 130.
. . r,' .'.: .."'li.]:'"'' 90.l :.,.,..'.t.,'.,,,.,f{:,9':,,',,:,, 90'
, : l:,,,, ,:, .:.l, i::,1i,|r,iq:rt,i:,,:i: 45 .: |!1 ::'.::] ],:r|:,^ .,: ))n
t,.'.::,'.,:,,i:::i.i.,.,,,',:,::,!1,1D;',.,i:,.. 90.: ..:.r..jr::f::::ii..::..r:::.|l:tDr:::: 90.: ii:..:N.0... 15,,'..j '..' Y;, .: , 90.,: ::i...: f.l.U.. r{).
'i::::::.:r:.::::r-:.:t:::ll::L}-.:l:::::: 1.5.
33.
07.
J_1 .
i).))-
i:: .
07.
1C,-. .
1!4.
67.
67.
:t
07-
bi.
67.
ji.
ji.
1 C!-r.
67.
6i.
3i-
17i).
67.
67.
5i.
u9lk9
u9/k9
u9/k9
u9l \g
u3l l9
u,j/ <g
19/ <.J
19/ <9
19/'<9
u9/ 39
ug,/ k,q
v9 /'<t)u9/ <9
'rg/ <q
rg/\'J
l.-l / k S',J1/ <g
'rg/'<9
r?/ <c)
ug/(9
L9,/ r g
u-clk9
rg/ <g
ugl <9
u9/k9
':i/'<9rg/'<g
u9lkg
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'Lg / <<.)
ouestions? Contact your
RacheL L. Krearner
CI iena Servr.es Representa:ive
at (7'7) 6':6'2300
MEMBERrffiiE
Lanca5ter Laboratorres
2425 New Holland Prke
PO 8ox 12425
Laccdster. PA 17505'2j i)
711-656-2300 Fax ji, c-ic 16l
RespectfuI ty Submi tted
Chrisrlne !- Ratctif+,
6rouo .eadec, CC/l!S
5ee ie'/efse i l: _ta q{o;ni.tiron,ri !yeb.: r;nc acoreyratrorls
I,LI sample No. Es 2538011
Cottected: 6/27/96 at 11:20 by gR Account llo: 067'16
Hercutes, Incorpocated
Envi ronrnental. Affai rs
uitmington 0E 19894
AS RECEIVED
uE r H00
;iiilliiiiiii8E-iu.gie':iir,:ii DETECT I cH L I r,,r I T uN I Ts
t+ of 11
P.0.
Ret.
DRY UEIGHT
i::::i:.::.::::r::::::i:.i:i.:i:::l:::.:i:r:::::i:.:::::: METHOD
jiii:.:i:ii,.:ii:iiiiREs't Uf s.:,.l:::ii. D E T E C T I ON L I H I T
{i La ncaster Labo rato ries
A Thermo Ana lyti ca I Laboratory Page:3l
tl
]t
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il
DE
suborirted: 6/28196 Reported: 8/ 6196Discard: 9/ 6/96
Stat 2(2A) Grab Soil SarpLe
Hercutes: Eacchus Pond
STT2A SDG#: HBP02.01
CATNO. AIIALYSIS IIAITIE
TcL Su846 Semivotati tes/soi t
4697 3'ni tnoani t ine
1 191 acenaphthene3750 2,4 -dini trophenot
1192 4-ni trophenoI4698 di benzofucan
1 191 2,4-dini trotoluene4699 ?,6-dinitrototuene3n0 diethyt phthatare3769 4-chtorophenyt phenyt ether3768 fluorene4700 4-ni troani I inet701 4,6-dinitro-2-rnethytphenol.3772 N-ni trosodipnenyta(rine3773 4-bromopheny', phenyt ethee377t* hexachtorobenzene'1194 pentachtorophenoI3775 phenanthrene
3776 anthracene1702 carbazoIe3777 di -n-buryt phthaLate3778 f luoranthene
1'195 pycene3780 butyt benzyI phthalate3783 3,3' -dichtocobenzidine3781 b€nzo (a) anthracene3784 bis (2-ethylhexyL ) phthaLate
373? chrysene3785 di -n'octyt phthatate3786 benzo (b) fluoranthene3787 benzo (k) ftuoranthene3788 benzo (a) pyrene3789 indeno (1,2,J-cd) pyrene3790 dibenz (a,h) anthracene3791 benzo (ghi) perytene
67.
35-
170.
171.
o7.
07.
o7.
I ?Lr.
171.
67.
100 .
1nll
170 .
33.
33.i3.
53.
13.
'1i,,1 .
67.
33.
67.
o7.
1i0 .
o/.
67.
67.
u9/ k9
u9/ k9
u9/ kg
uE/(g
ugl <9
ug,/ kg
')g/'!-9Jql kg
ug/ ('l
r:2/ < g
,Jo- / <g
'.rg/'<'tu9/ tg
ug/<g
r9,/ <9
u,)/ <g
u9/'<g
u9/kcJ
ug/'<g
u9/ <9
rgl <9
tJg./ kg
,Jg/ <g
us/k9
u9/K9
u9/ <g
u9/ k9
ug/'<9
u9/ K9
u9/ ''9
ug,/ kg
ug/ k9
u9l k-cr
90.
45.
220.
2?4.
45.
90.
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90.
90.
130 .
2?9.
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Rachet r-. Krearrrer
ctlent serv!ces RePresentatlve
a: (7'7) 656-23C!
7i€Fr
Lancaster Laboratorres
2.125 New Holland Prke
PO 8ox 12425
LJn(aste., PA 1 7605-2J25
7l 7-656-2300 iax: ;l7.o50-2531
Respectfui Ly Submi ttedChrisrine Il. Rarctifi,
Grouo !eade., CCl1.1S
Se:'e,.,erse;:de io. groian;::on oi t'i-oor5 6nd abbrevratrons 1216 Re', lC1l0,/95
I
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(I)La ncaste r Laborato ries
A Thermo Analytical Laboratory
5 of 1'l
Or}
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LLI Sarnple No. ES 2538077Cottected: 06/27/96 ar 1'!:20 by BR
Sutxnitted: 06/28/96
Account Ho: 06716
I xercuLes, incoroorated - DE
I Envi rorunenrar. Affai rs
I Urtmington DE 19894
Stat 2(2A) 6rab SoiI Sampte
Hercutes: Bacchus Pond
STT2A s0G#: HgP02-01
CATI{O ANALYSIS NAME
4593 TCL Votatites by 8240
1625 ThaL t rurn
1643 AIunrirrum
1644 Ant i rnony1640 Sariun'1647 Beryt L itrm1649 CadmiLmr
1 65 1 Chcomi um
1 653 Copper1654 I ron
1 655 Lead
I 658 Manganese
1601 Il ickeL1666 S i Iver1672 Zinc
57Ae SU St"J8/.6 ! CP D I ges t
6535 Arseni c TR
6936 Selenium TR
01 59 llercury5711 SU SU84o Hg Digest
0581 BNA Soi t Extraction
468B TCL SUB46 Serrivotati Ies Soi t4689 TCL Su846 Senrivotati Les/Soi t
01'l 1 Hoisture
!IET HOO
SU-846 82/+08
sll-846 6010A
SU - 846 oC'1 0A
sr/-846 6C't 0A
stJ-846 6410A
su-346 6;1DA
s';-316 6J',t0A
sll-846 601 0A
su-846 5J',rCA
sr-81,6 6,110A
su-846 6!'t CA
SU.BI.6 6!iDA
s|j-346 5ii 0A
srJ-846 501 CA
sr - 846 6C 't 0A
su-s46 3Ct0A
sT - 3/.5 6! 1 0A
s\J-846 6J10A
su-846 7471
^SlJ-846 7/rZ1A Modified
su-846 3550A
su-846 32708
cr ,-ol^ arTao
EPA'160.1 (modi;ied)
ANALYS I S
TRIAL OAIE ANO TIHE
1, 07/02/96 2133
1 07/1i/96 1729') c7/13/96 17291 07/13/96 17?9^, a7/.,3/96 17?9': C7/'.3/96'.7?9'. c7 / 1 _\ /96 17Zq' a7/.3/9. i7?9'' 17/fi/95 172q' c7/13/96 i72C' D7iil/96 i72e. 07/1:/96 17?9', c7 /",3/95 1729'. !7/',3/96 1729', a7 /i1i9o i7Z9
'. 07 / 0z /9o 19 -\!+1 C7i1.3/96 ^.729'. t7 /',i /96 A8+7
1 07/03/96 16481 07i02/q6 1506
1 07/01/96 1930
" 07/04/96 1305', c7/01/96 13C6
1 07/t?/96 15?0
ANALYST
Steven .,i. Lennon
JoIene !!. Schields
iotene H. Schielcs
JoIene Il. Schietos
.loi?ne ll. Schier,crs
..loLene 11. Scnteics
Jo!.ene !t!. Scf,ieLcs
JoLene Nl. Siniet-cs
JoLene !1. Schrelcs
Jolene,rl. Scnier-cs
JoLene I. SchieLcs
Jot.ne !1- Scnielcs
JoLsne ll. Scnir.Lcs
Jol.ene ltl. Schi e!.cs
JoIene !1. Schi etcsDesi R. Caro1.z)
"roiane i!. SchieLCsliina C- HaILer
Net Li S. Markaryan
Frances A. Detrorest
Sherry Lynn 9evLin
Joseph i'l. Ganbler
Josepn ll. Ganbler
lieetay g. Mehta
MEMBEFl
m@?E
Lan(aster Laboratones
2425 Nle,e Holland Pike
PO Box 12425
Lanca5ter PA 17505-2ci-c
717-556-2300 F.rx 7:i 6:!i.rrl
I,AgCRATORY CI{RONf CLF
See ,p..p..; 'ue ier -,c.,.d_.L'n !;57 aijLts aao dDbrevrdtlo.s
ZIL La ncaster Laboratories\ll' A Thermo Analytical Laboratory
LtI sample No. 2538077stat 2(2A) ciab Soi I sampte
Hercutes: Bacchus Pond
I
i croup No. 522ru9
i HercuIes, lncorporated - DE
I
I
QUAL]TY CONTROL REPORT
Page: 6 of
LCS LIMTTS
LOU HIGH
I
'l
t
'l
I
I
I
I
I
t
I
I
Samp I e
HDL
Sampt e
UII I TS
DUP TtSRP! MS MSD RPO
LCS LCS
LCS DUP RPO
4593 TCL Votatites by 82(0
3434 chlocooethanez. ug/ks
3l+35 Bromomethane5. uglkg
3436 Vinyl. Chtoridez- ug/kg
3437 chtoroethane3. u9/ k93440 Methytene chto.ideZ. uS/kS
4071 Acetone7. ug/kS
4076 Carbon Disutfidel. uq/ks
1180 l,'l'DichtoroetheneZ. ug/kg3112 1,1 -Dichtoroethane
1. us/kg
3t 44 Ch I oroform1. uglkg
3t,45 1,2 -0 i ch ioroethane2. uglkg
4085 2-Eutanone7. uslks
3t 46 1, 1,1-Trichtoroethane1. u9/k93447 Carbon Tetrachtoride1. ug/kg4091 vi nyt Acetate3. u9/k9
3448 BromodichLoromethane2. uslkg
3450 1 ,2 -D i ch t oropropane3. ug/ks
3454 cis''l,J'Dichlocopropene1. ug/kg
1181 Trichtoroethene
1 . ug/l.g
3452 D ibromochtoromethane1. uglks3453 1, 1,2'Trichtoroethane2. ug/kg
1 l82 Benzene1. ug/kg
3451 trans-1,3-0ichtocopropene1. ug/kg
B LANK
Batch: E95183lAA
N.D.
[.D .
N.D.
N.D.
90
99
10t-
91
oa
98
100
101
99
78
100
1C1
95
95
92
84
105
100
31
90
9B
98
',07
87
92
96
9?
T
I
I
1 ?7?
1 ?41
1 250
10 254
I zl I
19 150
24 188
I L)5
59 155
51 138
49 155
2? 167
52 162
70 140
19 190
35 155
1 209
1 ?26
71. 157
53 1t9
52 '! 50
37 15',1
17 165
395
295
5 102
1C 89
5vb
11 83
2 103
6 105
495
191
)n os
1 105
3 103
20 105
295
0 101
2 1A2
2 111
396
298
2 ',104
198
102
oo
102
107
99
96
1C2
106
99
9?
93
96
109
90
94
98
93
Lanca5ter Labordtones
2425 New Holland Prke
PO Box 12425
Lanc3;ier PA I 7505-:l:5
717-o56"1i00 F;x ltz-c56'2561 diI5ee.eve.;i :,Oe i,jr ercianal'cn oi ;ynxg,5 ;ag 6![6s'-,r3119n5 2ll5 ::v lC,/10/95
il
I
ouP ilsRPO :'1S MSD RPD
(1)
(2)
I
I
I
I
t
I
I
I
I
t
I
I
I
I
I
I
I
I
(I)Lancaste r Labo ratories
A Thermo Analytical Laboratory
LLI sample No. 2538071Stat 2(2A) Grab Soi L Sampte
Hercutes: Bacchus Pond
Group Io. 522759
liercuIes, :ncorporated - DE
Page: 7 ol :1
LCS LIMITSLOU HICH
45 169
50 12tt
52 140
6t i48
46 157
17 150
37 160
37 162
74 136
30 200
54 156
51 156
50 150
50 165
21 ?99
70 131
?3 177
26 17/+
)4 t4l
57 145
61 142
5i 142
59 135
55 116
50 147
Sampte SampteI{DL UII I TS
5456 Bromoform1. ug/kg
4108 4-Methyt-2-pentanonel. uglks
4107 2-Hexanone3. ug/ks
3457 Tetrachtoroethene
1 . ug/ks
3149 1, 1,2,2-Tetrachtoroethane1. ug/kg
1 1 8l Totuene1. ug/ks
1184 Chlorobenzene
1 . us/ks
3458 EthyLbenzene1. ug/kg
41 17 Styrene1. ug/kg
3355 Xytene (toral.)
'I . u9/196'l87 trans- 1,2-Di ch Ioroethene
z ' us/k-o
6277 cis-1,?-DichIocoethene?. us/kg
1625 That t ium14. mg/kg'1643 Atuminum8.9 mg/ks
1644 Antirnony?.2 mg/ks
1646 Barium2.2 mg/kg
1647 BeryI L iurn0.Ofi mg/kg
'1549 Cadmimr0.13 ms/kg
1651 Chromium0.47 mg/kg
1653 Copper0.50 ng/kg
1654 I ron
3 .4 mg/kg
1655 Lead2.1 mg/ks
1658 Hanganese0.12 ms/ks
1661 Nicket0.46 mg/ks
1666 S i tver
LCS LCS
LCS OUP RPDELAHK
N.D.
r,l.D .
N.D.
N.D.
N.9.
N.D.
N.D.
N.3.
N.D.
N.D.
N.D.
Eatch: 96i345708101
N.D.
Batch: 96'184570B003[.!.
Eatch: 96'1845708C03
N.0.
Batch:9518457C8C03
Batch: 96'1845708!Ci
N.0.
Batch:961845703C03
N.D.
Batch:961345708001ti,r.
Batch: 9618457C8C03
N.C.
Batch:961845703',]C17.2 ) ng/!.i
Eatch:95184570SJ01
N.D.
Batch:961845708:Clti.t.
Batch: 96i845708!Cl
N.D.
Earch:95:8457081CjI.0.0.45 mglks
The resutt for one or
The background nesuIt
?1
(i)
9
0 (,.)
0 (1)
0 (1)
0 (1)
13
0 ('i)
11
(1)
83
91
90
9A
103
96
92
' U:
98
101
89
1645 (2)
95
97
91
38
109
2139 (2)
90
109
91
6
7
12
I
7
1
0
J
7
?
6
I
6
9
2
7
5
7
,1
6
4
5
6
7
93
90
91
115
97
101
97
'108
'101
i05
i01
1n?
96
79
79
100
98
99
102
102
89
94
91
96
o,
both determinations cas tess than ftve tixtesljas more than four tines the spi<e acded.
Lancaster Laboratones
2425 Ne,ru Holland Prke
PC Bcr 12.125
Lincas(er. PA I 760i-24: :;ll-5i6-2i00 Far ?1.;-5;{: I'rl I
{)e
ro/ic/95 ?G;
QUALITY CONTROL REPORT
QUALITY CONTROL REPORT(l)Lancaste r Laboratories Page: I oi
A Thermo Analytical Laboratory
LLI sampl-e No. 25380'7'7
Stat 2(2A) Grab Soi L SampLe
llercutes: Bacchus Pond
I 6roup No. 522139
i Hercutes, lncorporated - DE
I
I
II
:I
I
,l
Sanpt e
TID L
SampI e
UMI TS MS
OUP
RPD tls0
98
92
91
92
IYS
RPD
6
0
1
0
LCS
92
93
6t
79
LCS LCSDUP RPD
LCS LIIIITSLou H l6ir
54 149
49 119
52 1149
26 157
:l
1672 Zinc0.40 ms/kg
6935 Arsenic TRD.?5 mg/ks
6936 Seteniurn TR0,18 ms/kg
0159 Mercury0.028 mg/kg
4688 TCL SU346 Semivolatites SoiI
1 185 phenoI53. us/ks
3753 bis (2-chtoroethy[ ) ether67. u9/k9
1186 2-chtorophenoI33. uslks
3754 1,3'dichlorobenzene
33.ug,/ kg
1187 ,l,4-dichto.obenzene
33. ug/ks3755 1,2-dichtorobenzene13. ug/kg
1690 2-trrethytphenot67. ug/ks
4691 2,2'-oxybis (1'chtoropcopane)
1 00. uslks
1692 4-nrethyIphenoI
100 .ug/ k9
1 188 [-ni trosodi -n'propytamine
67. u9/k9
3757 hexach L oroethane67. ug/kg3758 ni trobenzene
3J.u9l kg
3759 i sophorone67. us/ks
3746 ?'nitrophenoI67. uglkg
37t T 2,4 -d\tnerhytphenot
67. ug/kg
3760 bis (2'chloroethoxy) methane33. us/ks
3748 ?, 4'di chtorophenot33. u9lk9
1189 1,2,4-trichLorobenzene33. ug/ks3761 naphthatene
33.u9/ke
0 (1) 103
0 (1) 91
0 (1) 9?
0 ('l ) 92
72 82
7-\ 81
69 78
75 79
71 73
72 77
69 30
62 70
S/. 97
74 8t,
75 33
77 83
33 92
7L 32
46 57
7i J I
7', 31
77 82
73 77
Iess than five tirnes the l-oo.
5 112
12 158
?3 i3,i
1 172
zo 124
32 1?9
46 123
J6 tOO
s 152
1 230
4q 113
35 130
2', 196
29 152
32 119
33 181
39 135
14 lttl
I
2216 qev ,.rr.rr. {t; I
BLANK
Batch:96i8457080030.80 J mglkS
Batch:961845703C03. N-0.
Eatch: 961845708C03
N.D.
Batch:961845711002
11.0.
Eatch: 96153St-B025
N.D.
N.D .
N.9.
N.D .
N.D.
N.D.
N.D.
N.D.
il.D.
N.0 .
N.D .
N.D.
N.D.
N.9.
N.D.
N.D.
N.D.
N.D.
ri-D-
I
I
I
I
I
I
I
I
I
13
11
12
5
5
6
15
11
1li
1J
'10
1C
9
.,7
11
1l
6
5
76
t)
76
It)
71
62
90
77
BO
78
a7
76
l+1
75
77
78
75
both deterfl inations uas
Lancasler Laboratones
2425 New Holland Prke
PO Box 12425
Lancastet PA 17605-2425
717-656-2300 Fax. [phone]
I
(1) The resutt for one or
See .A.je.5e s.oe 'ot ?,C,liict ca c' ;- mbo.s d.a oocrJ!rdt.o4s
DUP TSRP9 MS I1SD RPO
I
I
t
!
I
I
I
T
I
I
I
t
I
t
I
I
I
T
I
(|)h+mq*.e,r-t"gPgr"*lgries
LLI sampl-e No. 2538077sta( 2(2A) Grab 5oi I Sampte
Hercutes: Bacchus Pond
Sarple Sanote
MDL UNITS
l
I G rouo llo.
iiercutes,
L
522739
! ncorpol.ated
LCS ':CS
LCS DUP RPO
LCS I-II'II TS
LO"J H I CiI
17 115
2!. 1 16
22 117
28 123
1 ]00
J / )tt4
39 151
50 118
5i 143
1 11?
33 145
,]
aa
l9
50
1
25
59
ls
1t-5
191
132
iJ I
139
158
11t-
1<q
1?1
122
131
09
nt, rOr;0.'gS Lfi
L693 4-chtoroani I ine100. ug/kg3762 hexachtorobutadiene67. ug/kg
1 190 4-chIoro-3-methyLphenot67. uglkg
469t, 2-nlethytnaphthaIene33. ug/kg
3763 hexachtorocyc topenradi ene
1 70. uglkg
3749 2,4,6- trichlorophenoI67. us/kg
4695 2,(,5'tri chl.orophenol67. u9,/k9
3764 2-chIoronaphthaIene31. trg/ Lg4696 2-nitroani Iine67. ug/ks3766 dimethyI phthatare33. uslks
3765 acenaphthytene33. us/ks
1697 3-n\troanitine67. us/ks
1 191 acenaphrhene31. us/kg
3750 2,4-dinitrophenot'170. ug/kg
1192 4-nitrophenoL
1 70. us/kg4698 dibenzofuran
33 . u9/ kg
1 1 93 2,4-d i ni troto Iuene67. us/kg
4699 2,6-dinitrotoluene67. ug/ks3770 diethyL phthaIate67. u9/k9
1769 4-chlocophenyt phenyt ether57. uglkg
3768 ftuorene31. ug/kg
4700 4-nitroanitine
1 00. ug/kg
1701 4,6-dini tro-2-methyiphenoI
ELANK
N.D.
N.C.
[.9-
N.D.
N.0 -
[.D.
N.D.
N -0.
N.].
!.0.
N.0.
N.0.
N.D.
N.9.
N.D.
l{.?.
N.D.
N.D.
N-0.
N.9.
N.D.
H.!-
N.9.
1t 15
80 g7
75 86
74 82
17 16
81 90
30 89
79 85
72 78
79 e7
75 81
5
9
1l
'10
7
11
'10
I
B
10
8
4.5
8r
82
78
62
a,
82
79
77
4689 TCL SU345 Senrivotari les/soi L Eatch: 96185s18026
71
'59
t5
32
al
79
7t
59
66
40
7E
65
77
80
89
39
88
87
80
62
72
1C
9
6
a
7
10
10
'10
7
L
9
56
73
63
75
76
on
85
8l
tJ1,
79
76
66
7
1+7
1
Lancas!er Laboratoiles
2425 fle,, Holldnd Prke
PO 3cr I2.125
Ldn(a5iet PA 17605-242!717.!:a-2100 Fat 71i :,.o )ai
QUA:ITY CONTROL REPORT
ug/k9
\ee r_orE,!- t.ae:Or eiplaaA:ioa r)r ,,ioc!5 ;ac 600aevtattons
QUAL]TY CONTROL REPORT(I}La ncaster Laboratories
A Thermo Analytical Laboratory
I Group No. 522739
i Hercutes, lnco!-porated - DE
!
I
Page: 10 of 1 1
LCS LI!IITSLOU H I Gi1
38 147
53 127
1 152
14 176
5t1 120
?7 133
35 133
1 118
)L 1Aa
52 115
1 152
1 262
33 1/.3
I 158
17 168
I 146
2r+ 159
'1 1 161
17 163
,, 171
1 227
' L la
100 101
'l
LLr sample No. 253E077
Stat 2(2A) Grab SoiL Safllpte
HercuIes: Eacchus Pond
Sampte SampleHDL UII I lS
3772 ll-ni trosodiphenytami ne67. uglkg N.D-
3Tn 4-bromophenyl phenyl ether
100. uglkg |1.0.
3774 hexachtorobenzene100. uglkg N.0.
1194 pentachtorophenot
170 - uslks N.D.
3775 phenanthrene35. ug/kg N-D.
3776 anthracene33. us/kg H.9-
470? carbazote33. ug/kg N.D.
3777 di-n-butyI phthaLate13. ul/ls N.9.
3778 ftuoranthene
33 . u9/k9 N .!t -
1 195 pyrene
67 - ug/ks
3780 butyt benzyt Phthatate67. ug/l.g
3783 3,3' -dich!.ocobenzidine
130- ug/kg
3781 benzo (a) anthracene35. ug/kg
378t, bis (2-ethyLhexyt) phthatate
67. ug/kg
3782 chrysene33. us/kg
3785 di -n-octyt phrhaLate
67. ug/kg
3786 benzo (b) ftuoranthene67. ug/k.s
3787 benzo (k) tluoranthene130. ug/ks
f7B8 benzo (a) pyrene67. ug/kg
3789 indeno (1,2,3-cd) pyrene67. us/ks
3790 dibenz (a,h) anthracene67. uslk.g
3791 benzo (ghi ) pecytane
67. uglkg
0111 Moisture0.05 Z by pt.
N.r.
N.D.
N.D.
N.3.
N.0.-
N.0.
il.D.
N.C.
N.D.
N.1.
N.0.
N.D.
N.D.
Batch : 96184C316820001A
I
I
I
I
t
tcs Lcs
I aC nl 'O OOn
DIJP !!S
RPD MS I.ISO F'.PD
7t, 81
81 92
33 94
74 76
75 8i
7t, 31
-qc cc
73 90
5) Yt
85 97
55 58
77 33
93 101
e2 89
ei 92
7i 8C
77 35
t2 g9
z1 91.
79 86
12
:-!
13
2
1C
9
7
11
9
i0
tl
5
7
9
I
13
i0
10
'10
8,
9
B
73
80
B2
63
77
78
B6
77
g1
95
68
80
103
85
103
BO
8o
32
1C0
I
I
I
t
I
I
I
t
t
100
Lancaster Laboratofles
2425 New Holldnd Prke
PO Box l2-125
Lancasiei. PA I 7605-2j25
717-6':o-2100 F;r 71 /'55ri-166 d'; I
il
-r;oi: ;ro abbreyralrons 22 l6 Re! l0il0i95
I
I
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I
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I
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I
I
I
T
(I}La ncaste r Laboratories
A Thermo Analytica I Labo ratory
LLr sample No. 253t01iStat 2(2A) Grab SoiI Sarnpte
Hercutes: Bacchus Pond
4593 TCL volatites by 8240
4688 TCL SU845 Semivotatiles Soit
4689 TCL SU846 Semrvotati Ies/Soi I
6roup llo. 522759liercutes, :nccrporated - 0E
SURR06AIE SUIIT!ARY
SURROGATE RECOVERY %
ci4-1,2-0CA 89C8-tor.uene 91+
!t b li
PhenoL -d6 75
2-Flpheno[ 7^t?,4,5-lBP 90
N i trobz-d5 53
2'Fbiornyl 33Tphenyld]4 ?C
SURROGATE L!XITSLOU HIGH
70 12..
71 121
2/+ 1 li25 1?'19 122
23 120l0 11518 i37
MEMBERreEA
LdncaSter LaboraloneS
2425 Ne,.v lrolland Prke
PO Box l2a2t
Lancasrer PA 1 7605-2425
717-656-2)aO F3x /-17 6ra:adl
QUALITY CONTR.OL REPORT
See .:yerse ;rce 'or ?lDlaaatron of ; imcor; ano 6Sbaevrdtror)5
,t
2216 Rer ,Or-.Orn, ?ti
I
I'l
'l
r
I
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I
I
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I
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.l
I
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il
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il
n
T
I
I
I
T
I
T
I
t
I
I
I
t
I
I
(I)La ncaste r Laboratories
A Thermo Analytical Laboratory
LLI sample No. ES 2538078Cottected: 6/27/96 ar 12:25 by 8R
SuHnitted: 6/28/96 Reported: 8/ 6/96Discard: 9/ 6/96
Stat 3(2C) Grab Soit SanlPte
'Account No: 06716
I HercuLes, Incorpora!ed - DE
I Envi rornrentaL Af fai rs
: i,ti l-mington }E 19894
AS RECE IVED,, ,, r'rElHOD
RESULTS . D€TECTICX LIMTT UNITS
P age:'l of 11
on
Rei..
DRY UE I GHT
.::::::..'.. '.'. ' llETHoo
11,:,1, 1r,,, 1,11tf sul1.s'. :.,r, 0 ET E c I I oN i- I tl I T
Hercutes: Bacchus Pond
ST32C SDG#: HBP02-02
CAINO. ANALYSIS IIAME
4593 TCL VotatiLes by 82401625 Ihattitln1643 Atuninum1614 Antimony1646 Barium1647 Beryt t ium1649 Cadrniun
165 i Ch rorn i urn1653 copper165r, I ron1655 Lead1658 I'langanese1661 NickeL1066 Si Iver167? Zinc6935 Arseni c TR6936 Selenium IR0'159 l.lercury4688 TCL SU846 Semivotatites SoiI4689 TCL SU846 Semivotati Les/Soi L0111 Moisture
'rMoisture'r represents the toss
103 - 105 degrees CeLsius.
t4.
6.9))))
4.173
D.'tl
4.47t.50
! -1.
Lr-'12
i: .4 tL
!'.25
U.IJ
\J .l ao
See Page
m9/k9
mg/k9
orq/kg
n9/k9
mg/ig
m9/ (g
ng/ <g
n9l <g
n9/ (g
rc,J/ <q
m9l is
r'19l <g
n9/ <g
Ing/ i!l
ils/ <!i
m9l (g
See Page
;ee Page
19.
1?.
3.0
c.10
0.'13
0. 54
0.68
1..6
c.'i6
0.62
0.5'1
0.54
c.i4
L). 24
0. 019
in,,reight oi
:7-! 0.C5 73 sy r,:.
Inc:.an3te after oven drying at
3
t,
Respec!fu[ [y Submi tted
R"-lrnona V. I-ayilan, Croup Leaderl!7 letais/Leacheres
C0PY TO Hercutes, Incorpol.ated
CoPY T0 ERH Rocky Mounrain
AITN: Mr. Joseph KeI Lec
ATTI{: Hr. Breni Robinson
t
:::;:l'i]'*.!lHl"' vour c r' ""'"1'i;l ;';'ul:?:I;""'''"
I l1;to'll.3ooo3lrr,rl.loo ASR'IEP
1?6lib s2?r5e
Lanca5ter Labo.atofles
2425 New Holland Prke
PO Bor 12429
Lancaster. PA 1,1 5)5 - 2 !. )5
717 -656-230C Fax 1 1i'i,:t:
I
I
7xEilil tt
))15 ?=.,n,'trrn, ?a j'-.?e'i.'erse side ior erpranarron oi s,rrnSols aro.lbilii.., dlrons
-l
I
(iI)La ncaster Laboratories Paqe:2 of 11 ll
LLr sarnple No. ES 253E078cottected: 6/27/96 at 12:25 by 8R
A Thermo Ana lytical Labo ratory
I
i Account No: 067'16
i Hercutes, lncorporated
I Envi rorsnen:a L Affa i rs
I iji lmington ]E 1989/.
Illil
AS RECEIVED
l"!E T Hoo
ri il,,,i:iliji1tl"1stluJs,:',,ir, DETEc'i I 3N L I r! I T UN I rS
ll
DE
P.0.
ReL.
Suhnitted: 6/28/96 Reported: 81 6/960iscard: 9/ 6/96
Stat 3(2C) Grab Soi t Sampte
Hercutes: Bacchus Pond
ST32C sDG#: HBP02'02
CATNO. AIIALYSI S I{AHE
TcL Votatites by 8240
3431 chtoromethane3/.15 Eronpmethane3436 Vinyt Chl.oride3437 ch!,oroethane3440 l.lerhytene Chtoride4074 Acetone4C76 Carbon Disu[{ide1180'l,l-0ichIoroethene3t12 i.1-Dichtoroethane3114 Ch Ioroiorm
3445'l,2-Dichtoroethane4085 2-Buranone
31t 6 1,'!,'l -Trichtoroethane
3/,17 Carbon Tetrachr-oride409'l Vinyt Acetare31tB Bromodichtoromethane3450 1.?-DichIoropcopane
3451 cis-1,3-Dichtoropropene
'l 181 Trichtoroethene1452 0ibromochLocomethane3453 1,1,2-Trichtoroethane
1 182 Benzene3451 rrans'1,3-Dichtot'opropene1456 Bromofornr/+108 4-l'lethy[-2-pentanone4107 2-He,(anone3457 Tetrachtoroethene3449 1,1.2,2-TetrachIocoethane
1 183 Toluene
1 184 chtorobenzene3458 Ethytbenzene4117 Styrene3355 xylene (toraL )6187 trans-1,2-Dichtoroethene6277 cis-1,2-0ichioroethene
,ll
:i:.::.: i:::::j ::.::: :ll,Dr: :
... :r:::...r-:j.:j..:..i. tr 4..:.::i.:
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)
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ug/'<9
u9/k9
ugl k9
u9/kg
ug/k9
,Jgl ks
ug/kg
ug/ <g
'r9/ <9
,rSl kg
u9/ ks
u9/kg
!9/ <9
u9/ <')
rg/ <qtrl/ k..)
ugl kg
ug/k9
!9/ <9
,Jql k9
usl k!r
19/ ig
ug/ ks
ug/ <g
u9/ Kg
'rg/<g
ug/ <9
uEllg
u9/ kg
r9/kg
L-gl k 9
u9/tg
ug/ <g
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Quest ions? contact your cI ient
Rachet L- Krearner
Serv j ces Representat rve
ar (7'7) 656-23c0
reiH
Lancaster Laborator€s
2425 New Holland Prke
PO 8ox 12425
Ldncdster. PA I i605-2r25
7 I 7-656-2300 Fax 7 I 7-556-253 I
Respec:fu[ [y Subrni tted
i'licnele YcC',;rin, g.A.
Group leader, GC/!'S VoLari les
SEe ie., erSe 5rce ior elolanaton oi ;rmoois ,1nd ;bbrevratrons 12lti Rev i0,/10/95
DE
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(I}La ncaste r Laboratories
A Thermo Analvtical Laboratory
Page: 3 of 11
tl}
::r6 ?E. ,Orr.rr, lO'i
LLI Sample No. ES 2538078Cottected: 6/27/96 at 12:?5 by BR
Subritted: 6/28/96 Reported: 8/ 6/96Discard: 9l 6/96
Stat 3(2c) Grab Soit Sarpte
Hercutes: Bacchus Pond
SI32c SoG#: HBP02-02-
CATIIO. AIIALYSIS IIAME
TCL sU846 Semivotati les Soi t
1185 phenot3753 bis (?-chtoroethy[) ether
1 186 2-chtorophenot375t, 1,3-dichtorobenzene1187 i,4-dichIorobenzene3755 1,2-dichLorobenzene4690 2-methytpneno(4691 2.2'-oxybis (1-chtoropropane)
4692 4-methyLphenot1188 11-ni trosodi -n-propytamine3757 hexach Ioroethane3758 ni trobenzene3759 isophorone3746 2-ni trophenot3717 2,4-dirnethytphenot3760 bis (2-chtonoethoxy) methane3718 2,4-dichIorophenoL1189 1,2,4-trichlorobenzene3761 naphthatene4693 4-chtocoani line3762 hexach Iorobutadi ene
1190 4-chtoro-3-methytphenot
4694 2-methytnaphthatene3763 hexachLorocyctopentadiene3749 2,4,6-rrichLorophenot4695 2,4,5-trichLorophenol3764 Z-chtoronaphthatenei.696 2-nitroanitine3766 dimethyt phthatate3765 acenaphthyIene
I A..ouna tro: 06716
I xercul.es, !ncorporated
I Envr ronnentaL Af fai rs
I ui Lmngron DE '1989/r
I
i
P.0.
Re[ -
AS RECEIVED
IiETHOO
DETECiION LtI.IIT UNIIS
DRY UE] GHT
:ii:::lii:::iili:::i::i:::::i t:ii:i;l]i:;::: ::i:::r:i:: : H ET H00
iii ,,,:l.i;ii.:rir,:tEst!-.I,slill.:.ii DETEc r I 0rl L I M I I
i::,,,i::iit'tiii:t.i.,,,.it,i:: N;qiiii::! 46.
::j:rrril::r:::::i.:....,:ir:N:.:D;:..:r..: 91.
,i:t,,,i.i,iiii',ii:,iit:.i,iji:':li:.:i'!ili0i:.;::1i: 46..:: : ..:l:...j:.,.^..': t.t. ri::'r\.rui..:::r 5u.
!,1. :i:l ,i':l: :. :,' ,i. , :' i i 'i,li'i r D :,:rl,l:.r 46 .
,,;',,'rtiir.i':t.ii!t.:rl:tr:.r.:N.D;:.,,', q6.
,'t,::,tt iti:::,,,: t. ',,,1.,, ,t,,.i. lr,r D'.,.'.:,',' 9'1 .:.r.i:l::::l::..::.],:rt..::N.9r':.:.::' 140,
::,,,, i:'::,::,.,:i.' i.,l:'.,i:.,,t,til : 0,t:'ii.!'l 40.
..j:r::i:ii::::.::::r:'::l:,,: i i:lN I D:.1 :: !. 91 .r:,::.:.'i;:,':':-:':::IN';D:"::' 91'
itl.,:.i,.i:.:l,,rr:.,...r,,,.'':1.,1'1.D.,,t,,,. 46.
:,: i i,iti:;. ii::.:':,:, i',:.i.it:t'::i,.rt., .,D .. ,'.. 9'l .
:. ::':i:t::.i:.:ri:::r::::::.:::.:.:MiD; :::: 91.
,.,:,.,i;,.i.1..,.,.;; ;,,,1.. ;,1i1;,1p ; a;tl,;tit, 9 1 .
. ..'.t,,:.t.i.:i tit,ttrt:i;ltt. ,ii;.:!t.:I 1? ;,t r:,, 46 .
:.,,,,;,i:,,i::':ilil:i,:,:iii.ii:,i,:,il'I,,.};..,.:, 46.
:,.,,.'.i,:':'t t:::.''.',.:',,.:,.t::,tt'' D' ' '. ,: 46 '.,ii,,i:]::,.:.:,,.,,.,.',,,,:,.:..,4t,.[.0.,.',,,, \6.
:i:'...:::..:..:::::.:,:i..),}i!r:.. 110.,:,:'t..tt,,.ii,..,::.,i::,:ii:N:1t,.t,..:,, 91.
, . ,, ':.:: :,:::,[.o,: ,:: 91 ..:, , ,,,1,, ,,:::,\t,^ :,: l,Ii r.ilruj:: . {O.,,,jri.j,l,iii:ri:.,,:,ii::,,iiit,:,q!,;'ri:,,,, Z3O.
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.,,,',,.:,,i,,.'',i',,,1':':,,t'''i'.,ll':O';',,..',. 1.6.
l::::::::::::::::: :,]:l:.'ll:l::i:,|t:]L}--:::]::::i 46.
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u9/:<g
ug/kg
ug,/ <9
u9/kg
!g/ <g
u-ql <g
u9/'<9
t)g/'<g
u9,/ <g
u9l<g
ugl <E
ug/ <9
ug/ Kg
u9l ks
ugl kg
ug/ kg
us/ kg
'.iglkSu9/ kg
u9/ Kg
u9/kg
u9/'r9
u9/'<g
ug/ <9
usl k9
,)g/'<g
'r9/k9u9/ks
uslkg
us/ kg
Ouestrons? Contact your C[!ent
RacheL L. Kreamer
Servrces qepresentatlve
ar (7'7) 656-23A1
Lanca5(er Laboratofle5
2.125 New Holland Prke
PO Box 12425
Ldn(ister PA 17605-2il25
717-656-2i00 Fax [phone]
RespectfuI ly Submi tted
Chrisr!ne iY. Ratctif{, 8.S.
Group l-eader, GC/Mg
see .eve.s€ sroe for €roianai on oi Svmocis dnd dbbrevrdtlons
MEMBEFl
(I)La ncaste r Laboratories
A Thermo Analytical Laboratory
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::::,::,,:::.,::.': : :al/.
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:::,:j:,:,,::,,.,::::,-,, :,:l?,d,,:
. :::'rr.. .:a..r.:.:1,.. .,,j: jBt r' r.: :::: ::ir...: :i::.:i-:U r:
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,,: ,- , .,,,:,,, ,:, .1, |\,
::: j,.::,:,, ,,,:,, k.U.
DRY UE I GTIT
ii:..ii'i;l'::.,i...'.:.::ii.ii.!:!: IIETHOO
SgSU!I$Ii;:r: oETEcT iorl L Ill I T
P age:
Submt tted
Rarcliff, B.S.
GCl M5
l+ of 1l
T
.&l
iiy ro/ jLri 9-< ?a gD
LLI sample No. ES 2538078cotlected: 6/27/96 at 12:25 by BR
I
I Account No: 057'!6j lercutes, !ncorporated - DE
i Environmental. Affai rs
I uitmington DE 19891.
I
suhritted: 6/?8/96 Reported: 8/ 6/960iscard: 9/ 6/96
Stat 3(2C) Grab Soit Sampte
llercuIes: Eacchus Pond
SI32C SDG#: HBP02-02
CATIIO. AIIALYSIS }IAME
TCL SU846 Semivotati tes/soi t
1.697 3-nitroani I ine1191 acenaphthene3750 2,4-dinitrophenot1192 4-ni trophenoI4698 dibenzofuran1'193 2,4-dinitrototuene4099 2,6-dinitrorotuene3770 diethyt phthal.are3769 4-chtorophenyI phenyI ether3768 fluorene4700 4-ni troani t ine4701 4,6-dinitro-2-methytphenol3Tl2 N-nitrosodrphenyLamine3773 4-bromophenyt phenyl ether3771 hexachtorobenzene
1 194 penrach Iorophenot3775 phenanthrene3776 anthracene4702 carbazote3777 di -n-butyt phthatate3778 f tuoeanthene
1 195 pyrene3780 butyt benzyt phthatate3783 3,3' -dichtorobenzidine3781 benzo (a) anthracene
378/+ bis (2'ethylhexyt) phthatate
37AZ chrysene3785 di -n-octyI phthatate
3786 benzo (b) ftuoranthene3787 benzo (k) ftuoranthene3788 benzo (a) pynene3789 indeno (1,2,J-cd) pyrene3790 dibenz (a,h) anthracenq3791 benzo (ghr) perylene
AS RECEIVED
ME T HOD
, ii::::illiii,;:rRE FU-tIq::,.,: .,i D ETEc T I oN L I tr I T url I T s
67:??
170.
17C .3i.
67.
67.
67.il.
100 .
'170.
67.
'100 .
1 rl,1
'l7c .
i3.
JJ.
67.
67.
150 .
33.
67.
33.
67.
67.
1i0 .
67.
67.
o7.
67.
us/ (9
u9/ (g
egl'{cJ
us/kg
uglk9
,J9/kS
,t9/ <9
ugl Kg
ugl kg
ug/ks,
u9/kg
ugl k9
.-gl {9
u9l kg
u9/ <9
u9l k9
u9li9
u9/ <9
u9lkg
ug/k9
u9l Kg
ug/ <g
u9/ks
u9/ks
us/ k9
uql (g
u9/ kg
ug/kg
,rg/ Kg
ug/k9
,rgl k 9
ug/ ks
usl <9
u9/ k9
.:::..i:,:l:,,,:,::l;:;,,!(:,,D1'i i,. 91'
.riii,,i.'::.'itii'li;,D,:,,,: 46.
i::::::::::i:.::ii:ii: tI; C l].: ':,: 23 0 .
' i.i'ri...il.'ii.D:.,':,'i 23C.
:::'i:t.:i,,i1'lNID:ii",, 16.
. ... r... trrq, A t.
,r:,:i:,i:',ir:,:.:iii$,),,,,,:: 91.
,,,:.i.::it:.r':,,,}l,o-., , .91.ol
:::::i::.!::j:r::::::li.l9a': 46.
l:ii.,'i:!,,i'i.:1,...,',l,li). l:, 140.'.i'i.':i:'. * tr "'. )an
,,,,,,,.,. ,,,,,,,M.,.,, Y l.
' ,rr,ii:,;i::;,:,ill,,.o.',,,,,, tco.
..' .',1.,:,.i,ii:.',i'i,.l{;D r,i," 1 /r 0 .
i:.::.::ifii:]:i::rt::,::::ll;:D ::::: 230.:. '. r.:.)i,D:. 46.
.i,,,,.,j1,,:,.i,ll.,:,i,,:,.:,l'l.D.,'' 46.
.:.,:,,,.:,,'i.,:,,i::.],j,]:,i.1{',,9,.:,,,: 46.
.. . tl..:.....,..'..t.l.,l.t'.'t:,ll i,O .' ',:,, 46 '
,il, :i...iil;:i.i.i.,'...,!ilN. D .. :i: t,6.
. lii!, :,,i ii'ti:.,::iiili,:., tr..D , i',i:.. r 91 .
i i.:.: :ti :l.;,l.: :.liii:.i:,ii,:i: l{'"} i l:], :'.i 9 1 .
.:,i:,.t,i:,:t:.,:i:,1iii:,iliirt:;D,i:.1 180.
.: .,.' ,:.i ,: 1tt0 - _,
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::l:::,:,:::i,::,,r':;!.:.:.:::,'::::::N',9t.::'r:: 180.
,,,. ..,,,..,,,,,,, t;.r. . :] .:. , ::,:, .,1{.0. yl.
...,,,1,,.......,..,,,,,,,.,,,::'l+.0,.., 91'
.... i ..: .-. r. q Q.j
ouest r ons? Contact
RacheI L- Kre3mer
your Ctien: Services Representativeat (717) 65o-2100
RespectfuI iychrist:ne Y.
Group Leader,
MEMBEFI
faEFiI
Lancaster Laboratofle5
2425 New Holland Prke
PO 8ox 12425
Lan(asrer PA \7 6A5-1t25
7 17 -636-2300 Fax: 7 I 7-656-258 l
I
5ee reverse Srde for expldn.ltron of tymbois J.o doorevratlons
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&&&
(I)La ncaste r Laboratories
A Thermo Analytical Laboratory
MET HCD
su-845 82408
su-816 6010A
stJ-8(5 6l'r0A
su-846 60 tcA
su-846 6010A
su- 946 6C't 0A
sU-346 6Cl0r\
SH - 346 oJ: LrA
S!,- 84i o'.1i 0A
sr,-846 6.'1!A
cr,-C/! rlr,l^
S',j-346 611'lCAcrr-Ol^ l-11n^
Sll-3/.6 oli0A
SU-446 o,i,lr',
S'J-E4o ii5DA
srJ-846 60',]0A
su-8+6 0ii lA
su-846 7471
^Sl.J-846 7(71A l''odrf ied
su-346 1550A
su-846 82708
sH-816 82708
EPA ]60.1 (rrodif reC)
AIIALYS I S
TR I AL oATE ANO I II'IE
1 07/02/96 2220
', 07/13/96 1.734' 07/13/96 1774' 07/'13/96 ''734^ 07/1-:/96 1734': A7/^,3/96 1T3t+1. D7 /',3/96 ifi4', 07/'11/ci6 1Ti\' a7/13/96 173t,' a7/1i/95 173t
' o7/1i/96 1734' 07 /.3 /96 '1734': a7/"t3/crb 1734' 07!,i/96 i734' a7/i1/93'.71t' a7!Q2/96 1ei4' f;7/',3/96.,73L' 07/',7/s6 s852
1 07/03/96 1610', 07/0?/96 1505
1 07/01/96 1930. 07/0!,/96 1357i 07/04/95 1357
1 07/A?/96 152C
LABOFATORY CHR.ONICLE
Page: 5 of 1'l
AIIATYST
Steven J. Lennon
Jotene rl. Schietds
Jotene t'j. Schier.cis
Jolene Y. Schiel.ds
Jol.ene H. SchieLcs
JoIene ,!. Sch ielCs
JotenL. l!. Schietos
Jotene Y. Schre',ds
.ioLene ltl. SchieLds
Jol.ene I. Scnier-cs
Jote.e I. Schields
Jolene i!. SchieLcs
Jotane 1\1. SchieLcs
JoLene !!- SchieLcis
..loLene ll. S.tietcs
Desi R. CarDZza
JoLene M. SchieLds
Nina C. HatLer
llel.Li S. llackaryan
FTances A. DefioIest
Sherry Lynn DevIin
Joseph H. GambLer
Joseph Fl. Gambter
NeeLay 8. Mehta
LLI Samp1e No. ES 2538078Cottecred: A6/27/96 ar 12:25 by BR
SuUni rted: 06/?8/96
Account {o: c6716
Heecules, Inccrporated
Envi ronmental, Affa i rs
U1 I,mington DE 19894
DE
Stat l(zc) Grab Soi t Sample
Hercutes: Bacchus Pond
STIZC S0G#: HBP02-02
CATIIO AIIALYSIS IIAHE
4593 TCL VotatiLes by 8240
1625 ThaI L ium
1 643 A turni num
1641 Antimony1646 Bariun
1647 8eryl. t ium
1649 Cadmiurn
1651 Chromiu:rn
1653 copper
1654 l.on
1 655 Lead
1 558 Manganese
1651 N i cket
1666 si tver
1672 Zinc
5708 sU SU846 ICP oigest
6935 Arseni c TR
6936 Setenium TR
0159 ltlercury
5711 sU SU846 Hg Digest
0381 8NA soi I Extraction/.688 TCL su846 Senlivolati Ies Soi Lr.6&9 TCL sU346 semivotati Les/Soi L
0111 Moisture
refir
Lancasler Laboratories
2425 Ne,ry Holland Prke
PO 0or 12425
Lrnc.:ter PA 17605-2-
717.5i6-2100 Far :::
,\}-
l2r6 Re.; r0/j0,95 L;:+e e:<,le: Je ,.....-;o-;'|qr gi 3,mbo: anc joo,eTral'ons
(iI)Lancaster Laboratories
QIJALITY CONTROL REPORT
Page: 6 of
A The rmo An a lyti ca I La bo rato ry T
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RPO
LLI sample No. 2538078Stat 3(2c) Grab SoiI Samp(e
Hercutesr Bacchus Pond
Group tlo. 5227J9
Hercules, lncorporated - DE
Sampt e
rttDL
Sampt e
UNITS
OUP
RPO ils l!s9
US
RPO LCS
LCS
DUP
LCS LIiIITSr_ou H I6H
4593 TCL Votatites by 8240
3434 ChloromethaneZ. ug/kg
3435 Eroflomethanel- uglkg
3436 vinyt Chtoride2. ug/kS
3437 chtoroethane3. ug/kg
3440 ilethyIene Chtoride2. ug/kgl,O7l, Acetone7. us/kg
1076 Carbon D'isutfide
5 ' ug/k'g
1180 1,'l -Dichtoroethene
Z- ug/kg
344? 1,1'DichIoroerhane1. us/kg
3441 ChIoroform1. us/ks
3t 45 1,2-0ichtoroethane?' ug/kg
4085 2-Butanone7. ug/kS
3446 1,1,1-TrichLoroethane1. ug/kg
3447 Carbon TetrachLoride1, ug./kg
4091 Vinyt Acetare3. trg/kg3448 Bronrodichtonomethane?. ug/ks
3450 1,2-Dichtoropropane3. us/ks315t cis-1,3'Dichtoropropene
1 - uglkg
1181 TrichIoroethene1. ug/kg
3452 DibromochIoromethane1. ug/kg
3453 1,'1,2-TrichtoroethaneZ. ug/ks
1 1 82 Benzene1. u9/k9
1451 trans'1,3'Dichtoropropene
1 . ug/kg
B LA}IK
gatch: E96!831AA
[.0.
N.0.
N.9.
N.D.
[.D.
N.D.
il.c,
N.D .
N.D.
N.D.
N.D .
N.9.
N -9.
N.0.
N.D.
N.0.
N.0.
N.D.
N.D-
il.0.
N.0.
[.0.
N.0.
99
'!34
91
1t2
es
1n,
107
99
95
93
1C2
1Ur
99
92
95
96
1C9
90
9t,
96
93
e7
98
10e
10i
?9
:00
101
95
95
9?
.05
10c
81
9C
98
98
1. A7
87
92
v6
92
395
295
5 102
1C 89
396
11 83
2 103
6 105
495
295
1 91
20 95
1 105
3 103
20 105
295
0 10'1
2 102
2 111
396
298
2 104
198
1 27?
1 241
1 250
10 2s4
1 ?21
19 150
2r, 183
1 233
59 155
51 138
19 155
22 167
52 162
70 140
19 ',190
3s 155
1 289
1 225
71 157
53 149
52 150
37 151
17 183
MEMBEFlrRm
Lancaster Laboratories
2425 New Holland Pike
PO 8ox 12425
Lancaster. PA 17 605-2425
7 17 -656- 23OA Fdx: 7 1 7-656-2631 d1I
I
Sae re,.er:a ::s 1l'a\c i, ,ii 1'r c jycjoiS and aobrevralrons 2.:16 .lev 101-iC/95
7ot
DUP JIIS LCS LCS LCSRPO MS IISO RPD LCS DUP RPD LOU
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(I)hilt,,1s^t,r,#,?,0.r,*gr,"Pag e:11
LLI sample No. 2538078Stat 3(2C) Grab Soit Sarnpl.e
Hercutes: Bacchus Pond
Sarpte SamoteI'IDL UII I TS
3456 Eromoform1. ug/kg
4108 4-t'{erhyt -2-penranone
3. ug/kg4107 2-Hexanone3. ug/ kg
3457 Tet.achl.oroethene1. uglkg
3t,49 1,1,2,2-Ietrachtoroethane
1 - ug/kg
1 183 Totuene
1 - ug/kg
1 184 Chtorobenzene1. ug/ks
3458 Ethytbenzene1. us/kg
4'l 17 Styrene1. ug/kg
3355 xytene (toraL)
1. ug/kg
6187 trans- 1,2-0ichloroethene2. ug/ kg6277 cis-1,2-DichLoroethene?. ugl kg
1625 That L ium11. mg/ks
1643 Atuminun8.9 mg/ks
1644 nntimony2.2 mg/kg
1646 Barium?.2 mg/kg
1647 Eeryttiun0.0-,3 m9/k9
1649 Cadmium
0. ll ms/kg
1651 Chromiw0.47 mg/kg
1653 Copper
0 - 50 m9lk9
1654 I ron
BLA}IK
N.D.
li -9.
N.D.
N.9.
N.D.
N.9.
N.D.
N.D.
N.D.
N.9.
N.D.
N.9.
Batch:961845708C01
N.9.
Batch:9618457C8C31
N.D.
Batch: 96'1845708C03
N.D.
Batch: 96i845708.t03
N.D.
Batch:961845703C01
N.0.
Eatch:961845708!03
N.0.
Eatch:96i845708C0i
N.0.
Batch : 961 845703!01
N.9.
6atch: 96':845708!037.2 J ns/t,?
Batch: 95'1845 203403
Barch: 961845708301
Eatch: 95'18457C3!01
Batch: 95i845708!r0l
ti.0.
?1
(1)
9
0 (1)
0 ('l )
0 ('l)
0 (1)
'13
0 (1)
11
0 (1)
('l)
five times
added -
88
98
'101
115
'100
195
96
'107
99
':25
'1 C1.
105
93
10)7
92
105
96
128
119
2t,52
96
1 1(,
97
1AZ
the Loo
B5
91
90
1i0
9(1
101
96
1C3
98
10'1
89
16t 5 (2)
95
97
91
33
131
109
2139 (2)
90
109
91
97
6
12
1
7
1
0
7
2
6
t,
6
9
2
5
7
1
6
4
7
5
6
7
45
50
64
16
17
5t
37
30
54
5/+
50
50
zt
70
23
?6
57
61.
53
69
55
50
93
90
91
115
97
101
97
108
101
'106
101
102
95
79
79
100
98
99
1C2
102
B9
9t*
94
96
LIHTTS
It I 6't{
169
124
140
148
157
150
160
162
136
200
156
156
150
155
299
131
177
171
1 t,1
145
14?
14?
135
146
1655 Lead
2.4
1658 lt'langanese
mg/kg
ms/ks
0.12 mg/kg
0 .46 mslks
0.45 ng/kg
(1) Ihe result for one or both deterninations(2) The background resutt las more than four
thao
spi ke
Lancaster Laboratories
2425 New Holldnd Prke
PO 8ox 12425
Lancaste( PA I 7605-2425
717-656-2i00 Fax 7 I i-65r.15S ;
,t
,orrorr, ?aE
QI-TALITY CONTROL REPORT
No. 522739les, lncorporated - 0E
See reve'se s'ce 1o' :,o ar;i:or oi t,,ncol1 anq dobrevtatlons 22 I6 Re';
(I}Lancaster Laboratories
A Thermo Analytical La boratory
QUAL]TY CONTROL REPORT
Page: 3of 11
I es
9Z
93
87
79
!-CS LCS LIHTTS
RPD LOU IIIGH
77
76
73
76
76
74
71
62
90
77
80
/o
87
76
/.1
75
77
78
75
5 112
12 158
23 13t+
1 172
20 12t+
32 129
46 123
36 166
5 152
'1 230
40 113
35 180
21 196
29 182
3? 119
33 184
JY IJ)
4t1 142
21 113
f,l
frl
:il
rl
:l
',ll
rt
h
I
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I
LLI sample No. 253807Estat 3(2C) Grab SoiL sarnpte
Hercutes: Eacchus Pond
Group No. 522739
flercutas, lncoroorated - D€
Sanpte Samp[eMDL UII I TS
167? Zlnc
SLANK
Batch:9618457080030.80 J m€./kg
Eatch:961845708003
N.D.
Batch:961845708C05
N.D.
satch:961845711002
N.9.
mg/ks
ms/k9
mg/ks
ms/k9
0 (1)
0 (1)
0 (1)
0 ('l )
MS
108
9'r
9?
92
MSD
98
9?
94
9Z
!1S
RPD
6
0
,l
0
149
11.9
157
LCS
DUP
DUP
RPD
0.40
6935 Arsenic TRn2<
6936 sel.enium TR
0.18
0159 l,tercury
0 .028
19
5Z
26
4688 TcL su846 Senrivotati tes Soi t Eatch: 96iB3Sl-8026
1 185 pheno(
33. us,i ks
3753 bis (2-chIocoechy[ ) ether67. ug./kg
1186 2-chl.oroprrenot33. ugl ks375t 1,3-dichIorooenzene33. ug/kg
11a7 1,4-dichtorocenzene33. ug/kg3755 1,2-dichtorooenzene
31.u9/kg
1690 2-methytpheno(
67.ug/kg
4691 2,2''oxybis (1 -chtoropcopane)
100 . us./ k9
4692 4-rethytphenoI't00 .ug/k9
1'188 N-ni trosocii -n-propytamine
67. ug/kg
5757 hexach Loroethane
67. ug/i:g
3758 ni trobenzene33. us/ks
3759 i sophorone
67.ug/kg
5745 2-ni trophenoL
67.ug/kg
3717 2,4' dinethyIphenoI
67.uglke
3760 bis (2-chIoroethoxy) merhane33. us/ks
3748 2,4-dichtorophenoI31. ug/kg
1189 1,2,4-trichLorobenzene33. ug/ks
1761 naph that ene33. uslks
(1) The result for one or both deteflninations Has Iess than five !imes
Lancaster Laboratofles
2425 New Holland Prke
PO Box 12425
Lancastel PA 17 605-2a25
717-656-2300 Fax [phone]
7? 32
7 -\ 8!,
69 7&
75 79
71 7e
72 77
69 3C
6? 70
84 97
74 81
75 83
a7 a?
8l 92
71 82
48 57
73 81
71 81
77 32
I) | |
rhe 100.
1j
'1 1
1-)
5
5
6
15
11
14
13
'!0
7
10
9
17
11
1l
6
5
I
I
T
I
IMEMElERtmm5ee teverse ;:o: ;or :ipranairon cr :,.aoo15 afo dob.evrairons
/'?
2:16 Re'. rOr;OrSS ?C#
LCS LCS
LCS DUP RPD
DUP li,!S
RPO IlS HSD RPD
T
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(I)Lancaster Labo ratories
QIJALITY CONTROL REPORT
Page: 9 of 11A Thermo Analytical Labo ratory
LLI sampfe No. 2538078Stat 3(2C) Grab soiI Sampte
tlercutes: Bacchus Pond
, 6roup xo. 522I59
I Hercutes. incorporated
l
Sarpte SampteMDL UII I TS
4693 4-chIoroani t ine100. ug/kg
3762 hexachlorobutadiene67. us/ks
1190 /+-chLoro-3-methyiphenoI
67. ug/kg
1694 2-methytnaphthatene33. uglkq
3763 hexach Iorocyc topentadi ene
1 70. usl k9
3719 2,4,6-trichtorophenoI67. ug/kg
4695 2,4, 5-tri ch LorophenoI67. uglkg
3764 2 - ch l.oronaphrhaL ene33. ug/kg4696 2-nitroani Iine67. uglkg
1766 diflrethyl. phthalate33. uglkg
3765 acenaphthytene
l3 . u-a/ k9
4697 3-ni troani I ine67. ug/kg1191 acenaphthene33. ug/kg3750 2,(-dinitrophenoI
1 70. uS/kg
1 192 4-ni trophenoI
170 - ug/?.g4698 dibenzofuran33. ug/ks
1 191 2,1'dint troroIuene67. us/ke
4699 2,6-dini trototuene67. us/ke3r/0 diethyt ph(hatate57. uglkg
3769 4-chtoropheny( phenyI ether67. ug/kg3768 f Iuocene33. uglkS4700 4-nitroanitine
1 00. ug/kg(701 4,6-dinitro-2-rEthytphenoI170. u9/k9
BLAN(
N.9.
N.D .
!,1.9 .
I.D.
x.D.
N.3.
N.D.
l,l.t.
N.t.
ll.9 .
N.D.
!.c.
N -C.
N.D.
N.3.
l(.9.
N.l'.
N.D.
N.D.
N.9.
N.9.
N.D.
1t+ 15
80 87
75 86
71 5?
17 16
81 9C
g0 s9
7? 78
79 87
75 3]
36 4C
71 78
59 55
71 77
7\ 80
B'r 39
79 88
79 87
71 B0
59 62
66 72
5
9
IJ
10
7
1'l
1C
o
I
10
I
1.3
B1
82
62
82
B2
79
75
3C
77
LCS L ll'l!TS
'.OU H I GH
17 116
2t- 1t6
22 147
2A 123
'i 100
5i 144
39 15'1
60 118
51 143
1 112
33 145
7 143
47 145
1 191
'1 132
28 131
39 139
50 158
1 114
25 '158
59 121
38 12?
1 181
4689 TCL SU846 Semivolati les/Soi t Baicl: 95'l83Sr-80?6
10
9
B
6
e
7
'0
'10
1C
7
t,
9
56
73
6l
76
90
B5
B]
81
79
76
Lan(aster Laboratorres
2425 New Holland Prke
PO 8ox 12425
Ldncasler PA 17605-2d:5
7 I 7-655'21C0 tax 1 11'6,'6' 253'.
,t.?.j
MEMBEFt
See iele.se srde for ecotar;i.on oi 5ymboi5 a.c aoorevratrons r 0i l0/95
1t
(l}La ncaste r Laboratories Pa_oe: 10 of ilA Thermo Ana lytica I La bo ratory
LLI sample No. 2538078
Stat 3(2c) Grab soi t Sampte
Hercules: Bacchus Pond
Sanpt e Sarnpt eMDL UN I TS BLANK
3772 N'nitrosodiphenytanrine
67 . us/ks ll.9 -
3773 4-bt'omophenyI phenyI ether100. ue/ks N.D.
3774 hexachtorobenzene100. us/kg N.D.
1194 pentachtorophenoI170. ug/kg N.D.
3775 phenanthrene33. ug/k.s N.0.
3n6 anthracene
33 . ug./kg N .0 .
4702 carbazote33. ug/kg N.r.
3777 di'n'butyI phthatate
33. uslkg N.?.3Tl8 f Iuoranthene53. ug/kg N .D .
1 1 95 pyrene
67 . ug/kg N.3.
3780 butyt benzyL phthatate
67 . ug/ks N.l.
3783 3,3t'dichtorobenzidine130. ug/ks N.l.
3781 benzo (a) anthracene33. ug/ks N.D.
378t, bi s (2-ethythexy[ ) phthaIate
67. us/kg fl.D.
3782 chcysene33. ug/kg 1.1.9.
37BS d'i -n-oc!yt phthaIate
67 . u9/k9 ll.D.
3786 benzo (b) fIuoranthene67. us/kg N.D.
J7B7 benzo (k) fIuoranthene130. ug/kg N.9.
J788 benzo (a) pyrene
67 . ug/ks N.D.
3789 indeno ( 1,2,3-cd) pyrene
67 - uglke N.0.
3790 dibenz (a,h) anthracene
67 . ugtkg N.0 -
3791 benzo (9hi) pecytene67. us/ks N.D.
0111 l.loisture0.06 % by ut.
!
I Group No. 522739
I Hefcutes, lncorporated - 0E
I
i
LCS LCsLCS DUP RPO
DUP iISRPD MS MSD RPD
"lljl
,il
1l
Batch: 96184C3!632CC03A
ll
iI
I
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t
I
t
,l
I
12 73
i3 80
13 82
26i
1C 77
977
-1 't 86
977
10 91
12 95
568
780
9 101
885
13 103
lC B0
'10 86
'10 73
382
9Bi
s75
'1 00 10c 0
74 84
31 92
83 9t,
74 76
75 33
7t, 79
8C 9C
73 80
3i 9?
85 97
55 58
77 83
93 103
82 89
8] 92
73 80
77 85
7t 81
83 91
79 86
tcs Llr'rt TsLoq H [ 6it
38 117
53 127
1 152
14 176
5/4 120
ZI IJJ
J) JJJ
1 118
26 137
52 115
1 152
1 ?52
JJ l.{J
I 158
17 163
4 lr{O
24 r59
11 151
17 163
1 171
1 227
1 219
100 1c1
reii-il
Lancaster Laborato.res
2425 New Hoiland Prke
PO 8ox 12.125
Ldnc.rsrer. PA I 751'5-2J:5
717-656-21C0 Fax [phone]
,t
,orrorr, ?ai
QI-IA],TTY CONTROL REFORT
See re,/-o:;e lrd€ icr exOia,raiion oi ri-oois ind aobrevraltods
I
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(|)L?[t*s^tgtB,?,r.r.*lgr'.t
LLI sample No. 2538078Star 3(2c) Grab Soit Sarnpte
Hercutes: Sacchus Pond
4591 TCL Votatites by 8240
4688 TCL SU846 Semivotatites Soit
4639 TCL SU846 SemivoIati Les/Soi t
i Group tlo. 522IJ9
i Heccutes. lncorporateC - DE
i
SURROGATE SUMI'!ARY
TRIAL IO STRROGATE RECOVERY Z
c4-1 ,2-0cA 89
c8 - to L uene 936EB 83
Phenol -d6 692-F'.phenol 072,4,6-rE? 57
N i trobz-Cs 792-Fbipnnyt ill
Tph eny I d,14 'J7
Lancrster Laborato0es
2425 New Holland Pike
PO Box 12425
Lancrster. PA 17605-2!).t
117-656-2340 Fdx 717-r-!o l5d
11
a2.
,0,.'Orn, ?a*
SURROGATE L IMI ISLOW H I GII
70 12181 1 't7
74 121
24 11125 12^,',9 12?
23 r205C 1i5
o iJ,
QUALITY CONTROL REPORT
MEMBEFI
seP 'e!e.te !,qe 'cr erptin;t,;i;rhol,, ,t:c: aLore,tai oo:
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La ncaster Labo ratories
A Thermo Analytical Laboratory(I)
CAI
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LLI sample No. ES 2538079CoLtected: 6/?7/96 at 12:25 by 8R
Suunitted: 6/28/96 Reported: el 6/960iscard: 9/ 6/96
Stat 3(2C) (14-18") G.ab SoiI Sampte
Hercutes: Bacchus Pond
32C11 SDG#: HBP02'03
] e..ount llo: 06716
I HercuLes, lncorporated - 9EI Fnvi romentaI Atf a i rs
I uitrineton oE 1989/.
I
I
lvlr. Joseph Ke!.'.er
Mr. Brenf Robinson
Page:
Re::pectful ty Submi tted
Railona V. Laynnn, Grou9 I-eader
ICP liera ls,/Leachates
1 of 11
P .0.
4593
16?5
1643
1641
1646
l04r
I 64v
1651
I O)J
165/,
l6))
1 658
too I
1666
1 A7a
6935
6936
0159
4588
4689
01'11
ANALysrs [AflE ]:iliniiii.li:,:jtiitJl-Isi:r,r':.i:i: ,rtrlilli'r,r,T uNITS
TCL Votatites by 8240 See Pa-oeIhattiun ::::i::t::::::i.i:::.,.::... tt.-D: 13. m9/k9Aluninur ii:::!:i:i!,it::illi6,l$0: .t!,' 8.7 ng/<gAntimbny :.,:j::.:i::i::i:i:l: U.D. 2.1 m9lk9
gar ium ::iiti1:iit,,,,i:i,,,,,, .., 45 r, ? .1 mg/kg
Beryt t i urn ::,i.::ii:::::t:t::: , t.,. 0.e s ,, 0.071 mg/kgCadrnium :.:.::ii:i;:ll:i:i,i::i,,:r.i:0-a8 : J C.13 mg/kgChromiLm ,.,,,,::,,:,,:.:::,: 14.o 0.15 mg/<gCopper iil';i:':.li ,::il.:: ,', ll5."q: C,13 xrg/(g
Lead :,:jj:.:: i:,.: 10,3 2.3 ng/".gManganege il::'iii:li:i.lil:l::i:i :r: It I - i ., .12 x9/ ksNicket li:ii:li,i',.rlilrjrll , 7,7 : C.t 1 nrg/ks
Si tver :t,',,.,,,,,.:'.,..,!:. i,l.l, ' 11.43 mgrkgZinc ,ilitji:,t,,,:l,:,:i,.. i 39.5 L'.i3 ;ng/'<g
Arsenic TR iii:i.:;:,,,i:.11i,,. ,.4,1 f;.21 ng/kg
setenim rR li::l:l:;:'::ii:;l:':ll':l" o't'r . I 0' 17 ;n-o/kgI'iercury :::i::::::;r;:::::ji::::,:: r:..0r,:j2 J C.028 ng/'tg
TCL SU846 Semivotatites Soil See Page
TCt SU8/r6 Semivotaai les/Soi L S!.e Pace
3
L
AS RECEIVED
"l,loisruref represents the Ioss in *ei9ht of the >ampLe after oven drying ar103 '105 degrees Cetsius.
DRY UEIGHT
laliii:i:r:..llfE$u!Ll,,lr' .': orr ecr t ox t- t u t r
.:.:::::i:.j:::..::r'::::.:::.::::illID'j: 17.
i::,::.:.,,i.:,':,:3it,1iq;liiit.i.ri;:,tt;i I1.: .. : ,, :N.0... 2.7,,:'.:::,:j:.:,>/:J: , :,:. ?.7
'.,,..,. ... 'i. ,,O.,Sg ... 0.090. .. : : ::,. 0rl;5 ': J 0.16, :,,.. i:,1':i,::,t,.i,i6;a,, ,,: O.S7
:::i:.11.:,,:l,i:.:i,19-,8r:.:,::,.::.! 0.61'.. ."?.,72O... . 4.2
.i'r.ii.:,,,,.l.::.,,i,.i:l5ii ,,.,...'. 2.9: ,.,..;',,.;,.:.,1?.3 , 0.i5
'liit:,i.,,i.i!,.t':ti:,i;,qi.B,,':.,,,,i.,,,.i. 0.56
....,.tii::ttiil,'t,.it'iilt,.:i.,}l|:rD-,,t. 0.55. j:i :.:' ::,:::50:.:: :::: 0.1,9,,,:.,:::,::,:, " . ,,'.':.... "iij:l'r.r'.(:' U.Jl. , ..1, .. .,1., ,:p...5a.....,. .t O.Zz
:t.:.r:::.:i::1::.;..:r:i.:::::.rr|,]r:0/+1:;ri::J 0.036
1 CoPY T0 tlercutes, Incorporated
1 CoPY T0 ERI'I ' Rocky I'lounla rn
Questions? contact your cLient seTv:ces Reocesentatire
RacheL ,-. Kreaner
15:13:27 D 0002 23 REP 1?6L36 522739310 25.00 0c 1 1 2(00 AsRo00
Lan(a5(er Laboratorre5
2425 New Holland Prke
PO 8ox 12425
LJn(ast€r PA i] 60\-11,.
7l;-656-:lCC Fdr 711-55b-rt-: l
t9i-*
MEMBEFl
):= :",iala ! iI? :a;i a,c t)'.t a'
LLI sample No. ES 2538079
cottected: 6/27/96 at 12:25 by BR
Suunitted: 6/28/96 Reported: 8/ 6/960iscard: 9/ b/96
Stat 3(2C) (14-18r') Grab SoiI Sampte
Heacutes: Eacchus Pond
32C14 S0G#: ltBP02-03
CATNO. ANALYSIS IIAME
IcL sU846 Semi vo I at i t eslso i t
4697 5-ni troani I ine
'1 19'l acenaph thene3750 2,4-dinitnophenoI1192 (-nitrophenoI
4698 di benzofuran1193 2,4-dinitrototuene/+599 2,6-dinitrotoIuene3770 di ethyt phthalate3769 4-chlocopirenyI phenyI ether3768 f Iuorene4700 4-ni troani I ine
4701 4,6-dinitro'2-methytphenot3772 N'nitrosodiphenytamine3771 4-bromophenyI Phenyt ether377/. hexachtot'obenzene1194 penEachtoroDhenoI
3775 phenanthrene
3776 anthracenel,7OZ carbazote3777 di -n'buryt phthatate
3778 f Iuoranthene
1 195 pyrene3780 butyt benzyl phthalate
3783 3,3'-di ch Lorobenzidi ne
3781 benzo (a) anthracene
37A4 bis (2'erhythexyt) phthal.ate
3782 chrysene3785 di -n-octyl. phthatate
3786 benzo (b) ftuoranthenei787 benzo (k) fiuoranthene1788 benzo (a) PYrene3789 indeno (1,2,5-cd) pyrene
3790 Cibenz (a,h) anthracene3791 benzo (gni) perytene
ouest i ons? Contact
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A Thermo Analytical Laboratory
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your Ctient Services RePt.esen:ative
ar (7'7) 656-2300
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2425 New Holland Prke
PO Bor 12415
LJnc.,siet PA 1;505-lc2ijt7.056_2jCC :ar -. / .15-:5ili
Respectfut Iy Submi tted
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- - :i j l-tcoi5 jnc ;clre.lato.:
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(iI)Lancaste r Laboratories
A Thermo Analytical Laboratory
METHOO
su-846 82408
5U-846 6010A
su-846 6t10A
5u-846 6C10A
su-846 6C10A
su-846 6010A
SU- B/to 6! 10A
su-846 5C10A
su-346 61't0A
S''J - 84 5 bl 'l 0A
SIJ - 3.16 6,11 CA
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su-546 ll5CA!l'ec6 5r) I 0A
SU- 84o 6.1 1 0A
su-346 7171A
SU-846 7i71A l'1odi f i ed
stJ-846 3550A
su-345 BZ70B
su-846 E270a
tPA lOU.l (mocltleC)
A}.IALYS I S
TRIAL DATE AND T I!'1E
1 07/0?/96 2330
1 07/13/96 17191 07/11/96 17!,9
'. 07/13/96 17t+91 07 /13/96 17t 91 07/i3/96 1719', A7 / 13/96 "t71,9
^. 07/13/96 17!9
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1 07/t3/96 16',31, n7/t?/96 1506
" c7/01/96 1930i 07/05/95 1?271 c7/15/96 1?27
1 07/A2/96 1524
I,ABORATORY CHRONICLE
Page: 5 of 11
ANAI. Y S T
Ctark A. Dougherty
Jolene I'1. Schietds
JoIene lil. SchieLcs
JoI ane I'l- Sch i eLos
JoLene tl. SchielCs
Joi.ene !!. scrietcs
ioIene i!- ScnieLcis
Joiene !1. 9chielcs
JoLsne ll. Scriej.cs
..ioLene !!. Schi ir.cs
"lotene fi. 9crieLcs
,,lol.L-ne )1. Scr i L'lcs
ioLane !1. Schietcs
Joi,ene l:- Scr ic-!.cs
,.ioLene itl- Scniclds
Desi R. Carozz.:
.,,o1-ane ltl. Sin ietds
Nina C. Nal.i.er
NeLLi S. 14arkaryan
Frances A. Dernorest
Sherry Lynn Devtin
.loseph i\1. Ganrbter
Joseoh !1. c.]mbIer
HeeIay 6. Mehta
LLr sample No. Es 2538079Cotlected: C6/?7/96 at 12:25 by ER
suhritted: 06/28/96
, Account llo: 067'6
i ttercuLes, :nc3roorated
Envi rortrrental Affai rs
: si lmington OE '19394,
IStat f(2C) (14-'18") Grab SoiL SampIe
tlercutes: Bacchus Pond
32C14 SDG#: HBP02-03
CATNO AI{ALYSIS IIAME
t593 TCL vol.atites by 8240
1625 thattiun1613 Atuminunr
1614 Antirnony1646 Earirnr1647 Beryt t iun1649 Cadmitfn'1551 Chcomiwr'1653 Cooper
1654 I ron1655 Leaci
1658 Manganese1061 ll i cke L
-1660 SiLver1672 I i nc
5708 sU SlJ846 IgP Digest
69J5 Arseni c TR
693t' setenium TR
01 59 t'lercury57ll Su Sk'846 Hg oigest
0381 BNA Soi I Extracti on
4688 lCL 518/.6 Semivot6ti les Soi L
4e,89 TCL su846 SemivoIati tes/soi t
0111 lloisture
Lanca5tei Laboratoi?s
2425 New Hollano Prke
PO 8ox 12J25
Lan(alter PA \ ;-40->- t :.)':
717-c55-2iCC F.i\ -' .-ia :'ra l
MEMBEFl
2215 .
(l}Lancaste r Laborato ries
A Thermo Analytical Laboratory
QUALITY CONTROL REPORT
Pa9 e:'1 1
LCS LIIIITSLOU H t GiI
1 272
1 2t,1
'1 250
10 254
1 221
19 150
?t+ 188
59 155
51 1lB
49 155
22 167
52 162
70 140
19 190
35 155
1 2C9
1 225
7" 157
53 1,i9
52 150
37 151
17 i83
il
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LLI sample No. 2538079Stat 3(2C) (14-19") G.ab Soit Sampte
Nercutes: Bacchus Pond
I Group No. 522IJ9
i Hercul.es. Incocoorated - oE
i
i
I
Sa[pt e
ItDL
Samp I e
UNITS
DUP HSRP' MS I.ISD RPD
LCS LCSLCS OUP RPO
4593 rCL Votatites by 82(0
3434 Ch Ioromethane2. ug/ks
3435 Eroflromethane3. ug/kg
3436 vinyt ChtorideZ. uglkg
3437 Chtocoethane3. ug/ks
3/+10 l.tethytene Chtoride?- ug/kg
1074 Acetone7. uglkg
4076 Carbon Disutfide3. ug/kg
'i 'l B0 I , 1 -0 i ch toroethBne2. uslkg3142 1,1-Dichtoroethane
'1 . us/ks
3411 Chtoroform1. ug/kg
3115 1,2-0ichtoroethaneZ. us/ks
4085 2-Butanone7. us/kg
3/.1,6 'l ,1, 1- Tri ch t oroethane1. ug/ks
3447 Cacbon Tetrachloride1. uglkg
4091 Vinyt Acetate' 3. uglkg
3448 Bromodichtoromethane
2 ' ug/ks
3450 1,2'0ichtorooropanel. u9/ kq
3t 5t, c i s'1,3'D i ch loropropene1. us/ks
1181 Trichtoroethene1. ug/kg
3452 Dibromoch Loromethane1. ug/ks3453 1, 1,2-Trichtoroethane2. ug/kg
'l 162 Benzene
'I . u9/k.9
3451 trans-'1, J-Dichtoropropene'l ' ug/[g
B tANK
Eatch: E961831AA
N.D.
N.9.
N.D.
N.0.
N.0.
N.!.
N.D .
N.9.
N.D.
N.9-
[.0.
r,l.D.
N .0.
il.0.
N.0.
N.D.
N.D.
N .0.
N-9.
N.9.
N.C.
N.D.
N.9.
395
?95
5 102
10 89
3C6
41 Aa
2 ',O3
6 '105
495
295
191
20 95
1 105
j 103
20 105
295
0 101
2 ',02
2 111
196
298
2 101
198
90 87
99 98
1A4 100
91 101
102 99
g8 78
1cz 10c
107 lCt
99 95
96 95
93 92
102 81
106 105
104 .. 00
99 81
92 9C
98 98
96 93
1C9 107
90 87
9L 92
98 96
g-2, 92
Lancaster Laboratorles
2425 New l-loiland Prke
PO Box 12425
LJncasier PA I 7505-::::5
7r7-656-210a i* | ii -556-253 ie'. ll'li l-: {t; I
I
MEMBEFl
5ee 'e,.,erse 5,ue.or:'c:anziron oi !7-c.i,! ;ec abbre'laiion;
LCS LCS LCS
LCS DUP RP9 LOU
93
90
91
1 _15
97
't 01
97
'r08
101
106
101
'l 02
96
79
79
100
93
99
1n,
102
B9
91.
9L
96
98
DUP :IS
RPD HS MSD RPO
I
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(I)Lancaster Laboratories
A Thermo Ana lytica I La bo ratory
QUAIITY CONTROL REPORT
LIMITS
H!GH
45 169
50 1?1
52 140
54 148
46 157
t7 150
37 160
37 162
74 136
30 200
51 156
54 156
50 150
50 165
21 ?99
7D 131
23 1Tl
?6 174
54 141
57 145
61 1t42
53 ltz
6e 135
5 5 1t,6
50 147
,:
17ol
LLr sample No. 2538019Stat 3(2C) ('14-18") Grab SoiI Sampte
Hercutes: Bacchus Pond
Ij Grouo llo. 5227J9
i.lercuIes. lncoroorated' DE
I
i
i
1. ug/kg N.D. 88 33
4108 4-t!ethyt'2'pentanone3. rrg/ks ll.D. 98 91
4107 2-Hexanone3. ug/kg N.D. 101 9c
f457 Tetrachtoroerhene1. u9/k9 ll.D. 115 110
341,9 1, 1,2,2-Tetrachtoroerhane
1 . ug/kg N.0. 100 9t
1 I8f fotuene
1 . ug/Y.g Il.D. 105 103
1 184 Chtorobenzene
1 . ug,/kS N.D. 96 96
3458 Ethytbenzene1- ug/kg N.D. 1C7 '.1t,
4117 styrene
'1 . uglkg ri.D. 99 92
3355 Xytene (to(aL )1. u9/k9 N.9. ic5 103
61e7 trans-1,2-DichIoroethene2. u9lk9 N.C. ir:4 98
6277 cis-1,?-CichLoroethene2. ug/k.g N.D. 1C5 :01
1625 Thal.tium Satch:951845708JC311. m9/k9 N.9. ( 1 ) 91 39
16/+i Atuminun Batch: 9518457080C38-7 mg/kg N.9. ?1. 2C27 1515 (2)
1644 Antimony Batch: 961845708C03?.1 mg/kg ri.D. ( -" ) 92 95
1646 Barium Batch: 961945708i01
2.1 mg/kg 1i.3. 9 1C5 97
1647 Beryt t itrn Batcn: 96184570B0030.071 rng,rkg N.9. 0 (1) 96 91
1649 Cadmiurn Eatch: 961845708C030.13 ms/kg r1.9. 0 (1) 93 38
1651 chronrium Eatch: 961845708C03
0.15 mg/kg |i.D. o (i) 128 1Jl
'1653 Copper Batch: 9618457080010.48 ms/kg N.0. 0 (1) I'19 1C9
1654 lron Batch: 96184570B3013.3 mg/ks 7.2 J mglkq 13 ?t152 2'39 (2)
'1555 Lead Barch: 961345708.1012.3 m9/k9 N.o. o (' ) 96 90
1658 Hanganese Batch: 951845708101
0.12 mg/kg N.D. 'l 1 115 1C9
16C,1 il i cker. Batcir: 961845703C030.44 mg/kq ll.D. 0 (:) 97 9'1
i666 Si lver Batch: 951845708C010.(3 rng/ks N.!. (:) 102 97
(1) Ihe result for one or both deternrinations las Iess than five times the l-oC-
(2) Ihe background resutt Has more than four tinres the spi(L'added.
sample SampieMOL UN ! TS
3456 Bromoforn
BLANK
Lancaster Labordtofles
2425 New Holland Pike
PO Bor 12125
L.rnrd!Ie,. :A i;605-2425
717-b50-2100 Fcr 717-o:o-lc.j l
6
7
12
4
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3
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il
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Page: 8 o{A Thermo Ana lytica I La boratory
LLI sample No. 25380'79Stat 5(2C) (14-18") crab SoiI Sampte
Hercutes: Bacchus Pond
I
i croup lto.
I Hercutes,
I
I
I
5?2739
!ncocporated - DE
SamPl. e
I.(DL
1672 Zinc
0 .38
6935 Arsenic TR
0.24
5936 SeLenium TR
0.17
0159 l{ercury
0.028
Sampte
UHI TS
m9./k9
mg/ ks
m9/k9
mg/kg
0 (1) 108
0 (1) 91
0 ('!) 92
0 (1) 92
LCS LII!ITSLOU HIGH
54 149
49 149
52 119
26 157
BLA}IK
Batch:96i8457080030.80 J rE/kS
Eatch:961845708C03[.0.
Eatch:9618/.57080C5
N.D.
satch:961845711002
r-.9.
t4sD
98
92
94
92
!ts
RPO
5
0
'I
0
92
93
87
79
4688 1c!- SU346 Senrivolati tes Soi I Batch: 96'i83513026
1 185 phenot
33. ug/kg
3753 bis (?-chloroethyt) ether
67. u9lk9
1186 2-chlorophenoL33. ugl k 93751 1,3-dichLorocenzenei3. ugl k9
1187 1,4-dichtorobenzene33. ug/kg
3755 1,2-di ch Iorobenzene33. us/kg
4690 2-nrethyLphenoI67. us/ks4691 2,2' -oxybis (1 -chtoropropane)
1 00. ug/ kg
4692 4-rnethytphenoL100. ug/ks
'l l88 N-nitrosodi -n-pcopytamine
67.u9l ks
3757 hexachLocoethane
67.uglkg
3758 ni trobenzene33. u9/ks3759 i sophorone
67.ug /kg3716 2-ni trophL.noI
67.u9/ks
3747 ?,4'dtnethyIphenot
67.us/k9
3760 bis (2-chtoroethoxy) methane33. ug/ks
3748 2,4-dichtorophenor.
us/ k9
1189 1,2,4-trichLorobenzene
33.uglk g
3761 naphrhalene
13.
(1) The resutt
u9/l(9
for one oc both determinations uas Iess
72 82
7t B(
5? 73
7-\ 79
74 73
1a
69 80
62 70
34 97
7t, 84
7t 83
77 B3
33 92
7L 32
(3 57
i _'\ 1l
71 31
77 82
73 77
than five times the 100.
5 112
12 158
23 134
1 172
20 124
i2 129
16 123
36 166
5 152
1 230
t0 113
35 130
21. ',195
29 182
32 119
33 18/*
5e 135
44 14?
lI IJJ
tlD
))li 7: ,.r,.,'n, ?43
'ti
11
12
5
5
6
t)
11
14
IJ
'!0
7
10
9
ll
77
76
t5
lo
71
71
62
90
77
6t
76
11
75
77
75
Lancaste. Laboratones
2425 llelv Holland Prke
PO Bc.( 12.125
Ld.(:1i.r. PA I 7605'21:5
7l i -a!;;-l?00 F;r.717-r!o-263 i
QI-IALITY CONTR.OL REPOR.T
>Ee.e,.,e.:i ::.)t ali_iFa. a--ac i,li:ai .tccra:la'l)r
I
I
I (l}Lancaster Laboratories
A Thermo Analytical Laboratory
QUALTTY CONTROL REPORT
Page: 9 of 'l 1
LIIIITS
HIGH
LCS LCS LCS
LCs DUP RPD LOU
DUP I'IS
RPD MS !.(SD RPO
I
,l
il
it
lt
il
rI
Sanpte SampteMDL UII ! TS
4693 4-chlonoani I ine100. us/kg
3762 hexachtoroburadiene67. uglkg
1 190 4-chtoro-3'methytphenoI
67 - ug/ks
1694 2-methytnaphthaIene33. ug/kg
3763 hexachtorocyctopentadiene170. us/ks
3749 2,4,6-trichtorophenot67. trglkg
1595 2,4,5-trichLorophenoL67. us/kg
3761 2-chIoronaPhth3Lene33. us/k-g
l+696 Z-ni troani L i ne
67 - ug/le
3766 dimethyt phthal.aEe
33. us./kg
3765 acenaphthytene31. ug/kg
4697 3-ni troani t i ne67. ug/kg
1191 acenaphthene33. ugl ks
3750 2,4'dini trophenot
1 70. ugl ks
1192 4-nitrophenoI170. us/ks
1695 dibenzofuran33. ug/kg
1 191 2,4-dini trototuene67. uglks
4699 2,6-dini tr.ototuene67. u9/k9
3770 diethyL phthatate67. uglkg
3769 4-chLorophenyt phenyI ethec
67. ug/kg3768 f Iuorenel3. us/ks
4700 4-ni troani I ine'100. us/ks
4701 lr,6-dini tro-2-methytphenoL170. uS/kg
LLI sample No. 2538079Stat 3(2C) ('14'18") Grab Soi t sarnpte
Hercutes: Eacchus Pond
I
I
r Croup xo. 52229
I Hercutes, !ncorporated - DE
I
1/, 15
an aa
7., 86
7L O'
17 ro
3't 90
3C 39
79 85
l a /5
79 87
75 81
36 4C
71 78
59 55
73 77
71 30
82 59
81 39
79 37
qo (,
BLAilT
N.0.
N.9.
H.D.
[.c.
N.D.
N.9.
N.D.
N.9.
fi.0.
N.D.
N .0.
N.9.
N.).
N.D.
N.3.
N.!.
N.9.
N.9.
N.9.
il.0.
N.0.
ii.D.
|l 9.
5
9
IJ
'10
7
't 'l
i0
B
8
10
8
43
81
32
78
6?
82
79
75
17 116
2t+ 116
2Z 117
23 123
1 100
37 144
39 15'l
60 '.l ',!8
5i 113
1 11?
33 145
/r lqi
47 145
'1 191
1 132
23 131
39 139
5r-1 158
?5 158
59 121
36 12?
't 18't
,l
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4589 TC!- SU846 SenrivoLati tes/Soi I Satch: 96i83S18026
10
9
I
6
8
7
10
10
i0
7
t-
I
56
63
75
76
90
l,]l
o/
79
76
6b
Lancaster Laboratones
2425 New Holland Prke
PO Box 12425
Lancasier P3 1i605-il
7li-i156-2100 !ar r I
MEMBEFl
.)e?i,':.,):|-.-.-,.-.,...',,,.,..-',.l'.|
.z
,rrrrt ?aJ
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A Thermo Analytical Laboratory
LLI sample No. ES 2538097
cottected: 06/27196 at 12:45 bY BR
suhnitted: 06128/96
(D Lancaster Laboratories
I"ABORATORY CHRONICTE
Page: 6 of 1?
Jotene M. Schietds
JoIene I't. Schietds
Jotene l.l. SchieIds
Jotene i!. Schietds
Jotene {. Schietds
Jotene M. Schietds
JoLene I'1. Schietds
Jotene iv. schietds
JoIene i'1. schietds
Jotene it!. SchieLcis
Jotene 11. Schietds
Jotene Y. SchieLds
JoIene il. Schiel.ds
Jotene M. Schields
Desi R. Carozza
Jotene M- Schietds
Nina c. llaU.er
Nel.ti S. F.ackaryan
Frances A.oemorest
sherry Lynn Devtin
Joseph l'1. Gambler
Joseph M. Gambter
Neelay B. flehta
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i Hercutes, Incorporated ' DE
I Envi ronmentat Af f ai rs
! u'i trin.lton cE '19894t-
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Stat 4(4A) Grab SoiI SamPte
Hercutes: Eacchus Pond
sT44A SDG#: l{8P02-18
CAT[0 AIIALYSI S llA]lE
4593 TCL Votatil.es bY 8240
1629 ThattiLm1643 Atuoinun
1644 AntinonY
1646 Bariun
1647 Beryttiun
1549 Cadmiur
1651 Chromium
1653 Copper
165t, I ron
1655 Lead
1558 llanganese1661 tlickeI1666 S i I'ver
167? Ziac
5708 SU Su846 ICP Disest
6935 Arsenic TR
6936 Seteniun TR
0159 Hercury
5711 su SU8/'6 Hg Digest
0381 BNA soi I Extraction
4688 TCL SU845 SemivoLatites SoiI
4689 TCL SU8/+5 Semivotati Les/soi I
0111 iloi sture
I,IETHOO
su-846 82408
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6C10A
su-845 60',!0A
su-846 60i0A
su-846 6010A
su-846 5C10A
su-8,46 6C10A
su-846 6010A
su-846 6010A
su-346 6C10A
su-846 50',I0A
su-816 6J10A
su-846 3050A
su-845 6ClDA
su-846 6010A
su-845 7471A
5U-E46 7471A llodified
su-846 3550A
su-816 82708
srJ-846 BZ70B
EPA '160.3 (modi f ied)
AIIALYS IS
TRIAL DATE AII9 TIfiE AIIALYST
1 07103/96 1226 Rick S. Rodsers $il1
tlr
I
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07/13/96 1908
07/13/96 1908
07/13/96 1908
07/13/96 1908
07/13/96 1908
07/11/96 1913
07/13/96 1908
07/13/96 1903
c7/13/96 1e03
07/13/96 1908
07/13/96 1908
07/1,3/96 1908
07/13/96 1908
a7/13/96 1908
07/0?/96 193/+g7/,.3/95 1908
07/17/96 1015
07/03/96 1701
07/0?/96 1506
07/01/96 1930
07/05/96 2102
07/05/96 2102
07/0?/96 15?A
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2425 Ne,, Holland Prke
c1.66r r1.125
L3n(a ;ier PA ll aO5-24,-.5
7 I 7-656-2 3OO F ;t. 7 1 i'536-263 |
MEMBER
.ce,.' I0/lCi !15
t{s
I"ISD RPO
3
2
5
10
3
11
2
5
4
2
,1
20
1
3
20
2
0
2
2
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2
1
DUPRPD I'IS
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(I}Lancaste r Laboratories 127of
A Thermo Analytical Laboratory
LLI sample No. 2538097
Stat 4(4A) Grab Soit SampIe
Hercutes: Bacchus Pond
6roup tJo. 522739
Hercutes, !ncorporated - DE
sanp I e
I.IDL
Sarnpt e
UNIIS
LCS LCS
LCS DUP RPO
LCS LII'llTS
LOIJ HI6i]
4593 TcL votati les by 8210
3434 ChtoromethaneZ. ug/kg
3435 Bromomethane3. uglkg
3436 Vinyt Chtoride?- ug/kg
3437 chtocoethane3. us/kg
3440 MethyIene chtot^ideZ. uglkg
4074 Acetone7. ug/kg
4076 Carbon Disutiidel. ug/ks'1180 1,1-DichIoroetheneZ. ug/kg
344? 1,1 -Dichtoroethane
1. ug/kg
3414 Chtoroform1. ug/kg3445 1,2'0ichlocoethaneZ. ug/kg4085 2-Butanone7. ug/kg
3146 1,1 ,1'Trich Ioroethane
1 . uglkg
3447 Carbon Tetrachtonide1. ug/ks
1091 vinyI Aceta(e3. us/kg
3448 Eromodichtoromethane2. uglkg
5450 1,2-DichLoropropane3. ug/ks
3451 cis-1,3-DichtoroProPene1. ug/kg
1181 TrichIoroethene
'l . ug/ks
5452 DibromochIoromethane1. us/ks
3153 1, 1,2-TrichLoroethane2. uslks
11BZ Benzene
1 ' ug/ks
3451 trans-1, J'oichloroProPene1. ug/kg
BLANK
Batch: E96'1831A8
N.0.
ll.D.
N.D.
N.0.
?. J u9/\2
N.D.
N.9.
N.0.
N.9.
iI.0.
N.D.
il.0.
N.0.
N.D.
N.0.
11.9.
N.D.
N.0.
H.D.
tl.D.
N .D.
N -!.
90 87
99 98
104 1 00
9'1 101
1C2 99
88 78
13? 1 00
1A7 101
99 95
96 95
93 92
102 8/t
106 'r 05
104 100
99 81
9? 90
98 98
96 98
109 107
90 87
94 92
98 96
93 92
1 ?72
1 ?41
1 ?s0
10 254
1 221
19 150
24 188
I Zt5
59 155
51 138
49 155
22 167
sz 16?.
70 140
19 190
15 155
1 209
1 226
71 157
53 149
5? ',150
37 151
17 181
95
95
'102
89
96
oo
103
105
95
95
91
95
't 05
101
105
95
101
102
11'l
96
98
104
98
Lancas{er Latroralo.res
2425 New Holldnd Ptke
PC 8o:( l2:125
Lan(a5:er, PA 11 645-2,!25
7l7-556'2100 rat. 11 t- -116-)i1:See.:ver:e t 1: -t' :(ciand: c-- :o ; anc lcari..,ratt(]ns 2216 Re,,"rr.',, {'P
QUALTTY CONTROL REPORT
{i La ncaster Laboratories Paqe: 8 of 12
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A Thermo A,nalytical Laboratory
LLI sample No. 2538097Stat 4(4A) Grab Soit Sampte
Hercutes: Bacchus Pond
DUP
RPO
522739
Incorporated - 0E
l.rsD
t'ts
RPO LCS
LCS LCS LCSDUP RPD LOTJ
LIIIIITS
IiIGH
Sarpte SarptetlDL U[ I TS
3456 Eroooform1. us/ks
4108 4-ltethyt -2-pentanone
3. us/kg
4107 2'Hexanone3. uglkg
3457 Tetrachtoroethene1. us/kg3449 1,1,2.2-I etrachIoroethane1. uglkg
1183 Totuene1. uS/kg
1'184 chtorobenzene1. us/ks
3458 Ethytbenzene1. uslks
4l 17 styrene1. ug/kg
3355 xyLene (tota[)
1. ug/kg6l87 trans-1,2-0ichtoroethenez- uglkg6?77 cis-1,2-DichIoroethene2. us/kg
BLANK
N.D .
r,t.D .
il.D.
r{.0.
N.D .
[.0.
N.D.
|1.D.
N .0.
N.D.
[_D.
N.D.
Batch:961845708C03
N.D .
Batch:961845708003
N .D.
Batch:951845708003[.0.
Batch:961845708003
N.0.
Eatch : 96 1 845708003
N.0.
Batch:961845708003[.0.
Batch:96'1845708003
N.D.
Eatch:961845708005
N.D.
Batch:96'18457080037.2 J mg/kg
Batch:961845708003
N.D.
Batch:96'1345708003
N.D.
Barch:961845708003
N.D.
Batch;961845708003[.0.
88 83
98 91
101 90
115 110
100 91
105 103
96 96
107 104
99 92
105 103
104 98
105 101
(1) 93 89
21 Z0Z7 1645 (2)
(1) 92 9s
9 105 97
0 (1) 96 91
0 (1) 93 88
0 (1) 123 .131
0 (1) 119 109
13 ?t52 ?139 (2)
0 (1) 96 90
11 116 109
0 ('r) 97 91
(1) 102 97
6
7
12
4
7
1
0
3
7
?
6
11
6
9
?
7
5
1
6
4
7
5
6
93
90
9l
115
97
101
97
108
'101
105
101
10?
96
79
79
't 00
98
99
102
102
B9
94
94
96
98
45 169
50 1?4
52 140
61 '148
16 157
47 150
37 160
37 16?
7+ 136
50 200
54 156
54 156
50 150
s0 165
21 299
70 131
23 1n
z6 I 14
54 111
57 145
61 142
53 142
69 135
55 1t6
50 147
'1625 Thal.tium
14.
1643 Atuminun
m9/ks
9.0 mg/kg
1644 Antimony2.2 ms/ke'1646 BariunZ.Z mg/kg
1647 EerytLium0.074 mS/kg
1649 Cadmiun0.13 ms/kg
1651 Chrmim0.47 mg/kg
1653 Copper0.50 mg/ks
1654 Iron3.4 mg/kg
1655 LeadZ-4 ms/kg
1658 lianganese0.12 mg/ks
1651 Nickel.0.46 ng/kg
1665 Si tver0.15 re/ks
(1) The result for one or- both determinations vas less than five times the L00.(2) The background result Has more than four times the spike added.
Lancaster Laboratones
2425 l'lew Hotland Prke
PC Box 12425
Lancdsier. PA I 7505-2425
717-b55-2100 Fax [phone]xmil ci,c.es itt I
.l
QUALITY CONTROL REPORT
IiGrous llo-
i Hercutes,
I
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I
5ee :g..3.i; SiJe'Oa :Yoiaad',./. ci',t- :',., nna tO0'e'.,rdi,Cn:2216 Re.
LCS LCSLCS OUP RPD
6
5
DUP l.lsRPD MS I.,ISD RPO
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(iI)Lancaster Laboratories
A Thermo Analytica I Laboratory
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II Grouo l,lo. 5222J9
I ne.cutes. !ncoroorated - DE
I
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Page: 9 of 12
LCS LIMITSLOU lll G'rl
51 149
49 119
5? 119
?6 157
5 112
12 158
Z) IJ4
1 172
20 124
3? 129
46 123
36 166
5 ]52
1 230
10 113
35 180
?1 196
29 182
3? 119
33 184
39 115
4l+ 1t z
21 115
LLI sanple No. 2538091Stat 4(4A) Grab Soit Sa.rpte
Hercutes: Eacchus Pond
4688 TCL SU846 SemivoLatites SoiI Batch: 96183St8026
Sanpl e SaflpteIitDL UNITS
1672 Zinc0.40 ng/kg
5935 Arsenic TR0.25 ms/kg
5936 SeLenit.IIl TR0.18 m9/k9
0159 lleccury0.028 ms/ks
1 185 phenot53. ug/kg3753 bis (2-chtonoethyL) ether67. u9lk9
1186 2-chtorophenoI33. ug/kg
3754 1,5-dichtorobenzene53. ug/kg
1187 1,4-dichtorobenzene.33. ug/ks
3755 1,2-dichtorobenzene33. uglkg
4690 2-methytphenot67. ul/kg
4691 2,2' -oxybis (l -chtorop.opane)
100. ug/kg
4692 4-methytphenoI
100 .'.tslkg1188 it-ni trosodi -n-propytamine
67. us/ks
3757 hexacht oroethane67. uglkg
5758 ni trobenzene33. uslkg5759 i sophorone67. us/kg
3746 2-nitrophenot67. ug/kg
37 47 ?, 4' dinethytphenoI67. us/kg
3760 bis (2-chtocoethoxy) methane33. us/kg3748 ?,4-dich.torophenol31. uS/kg
1 189 1,2,4- tIich tor-obenzene3J. ug/kg
3761 naphthatene33. us/kg
ELANK
Eatch:9618457080C30.80 J ms/kg
Batch: 961845708i03
it/.D.
Batch: 961845708003
N.0.
Barch: 9618457'1 1 002
ll.D.
0 (1) 108
0 (1) 9',1
0 (1) 92
0 (1) 92
98
9Z
91
92
7? 82
69 73
75 79
74 7A
7? 77
59 80
62 70
84 97
74 84
75 8l
77 83
83 92
7t 82
48 57
73 81
71 81
77 82
73 77
6
0
1
0
IJ
11
12
5
q
6
15
11
13
'10
7
'10
9
17
il
13
92
93
79
T.D.
N.9.
N.C-
[-D-
Lancaster Laboratorres
2d25 ilew Holland Prke
PC 3ox 12.125
L3ncasrir. oA \ 7 605 -2,12t
7ll'6i5-2100 iav 7fi 45a i':21
r'9.
, . ,,rrnr., la #
76
73
76
76
71
62
90
80
78
76
41
75
78
75
(1) The resutt for one or both determinations cas Less than five times the 100-
QUATITY CONTROL REPORT
5ee re,.,er;e :roe ior Exoianal q" 'r ', tdtboL and nocra', r.ltrorrj
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(iI}La ncaste r Laborato ries Page: 10 of 1?
A Thermo Analytical Laboratory
ilLLI Sample No. 2538097Stat 4(4A) Grab Soi I Sampte
llercutes: Bacchus Pond
Group no. 522239
Hercutes, lncorporated - DE II
SanpLe SafpteI.IDL U}I I TS
4693 4-chtoroanitine100. uglkg
3762 hexachlorobutadi ene67. uglkg
1190 4-chtoco-3-methytphenoI67. ug/kg
4694 2-methytnaphthatene33. uglks
3763 hexachtorocyctopentadi ene
170.uglkg3749 2.4,6-tcichl.orophenoL67. ug/ks
4695 2,4,5-trichLorophenoI67. ug/ks
3764 2-chtoconaphthateneJ3. us/kg4696 2-nitroanitine67. ug/kg
3765 dimethyt phthatate33. us/ks3765 acenaphthytene33. us/ks
4697 3-ni troani I ine
67 - us/ks
1 191 acenaphthene33. ug/kg
3750 2,4-dini trophenoI170. us/kg
1192 4-nitrophenoI170. uslkg
4698 di benzofuran33. ug/ks
1 193 2,4-dini trototuene67. ug/kg
4699 2,6'dini trotoLuene67. ug/kg3n0 diethyt phthaLate67. uglkg
3769 4-chtorophenyI phenyt ether67. ug/ks
3768 ftuorene33. us/kg
4700 4-nitroani Iine
100.ug/Lg
4701 4,6-dini tro-2-methytphenoI
ug/kg
DUP
RP9
f{s
RPD
5
9
LCS
DUP
LCS
RPO
LCS LII',IITSLOU HIGH
17 116
Zt 116
2? 117
28 123
1 100
37 144
39 151
60 118
53 143
1 11?
33 145
7 113
4t t4)
1 ',191
1 132
?a 121
39 139
50 158
1 114
25 158
59 121
38 122
'I 181
BLAIIK
N .0.
[-D.
N.D.
N.9 .
N.D.
[.9.
N.D.
N.D.
N.9.
N.D.
N.D.
N .0.
N.D.
N.C .
N.D.
N.r.
N.?.
N.C.
N.D.
ll.D.
N.Et .
N.D.
N.0.
14 15
80 87
75 86
74 3?
17 ,16
81 90
80 89
79 85
72 78
79 87
36 40
71 78
59 65
73 77
74 80
82 89
31 89
79 33
79 87
74 80
59 62
66 7?
1l
10
7
'1 I
10
8
I
10
o
LCS
43
B1
82
6?
q)
82
79
t>
80
77
L
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4689 TCL SU846 SemivolatiIes/Soit Batch: 96'183S1S026
10
9
8
6
7
1C
'10
'10
4
9
56
73
63
76
90
85
83
84
79
76
66
MEMBEFlyrcIil
Lanca5ler Laboraroiles
2425 flela Hoiland Prke
PO Box 12{2S
Liocasiel PA 17505 242;
7l /'556-2loLl Fa 111 -c16-2631
,%'5ry
QUA],ITY CONTROL REPORT
170.
^oef, .i 2 .ar,'i j at t):';:l;6 Rer' lCilC,95
T
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(iI)Lancaster Laboratories
A Thermo Analytical Laboratory
LLI sample No. 2538097Stat 4(4A) crab Soi I SanpLe
Hercules: Bacchus Pond
I
I
I Group ilo.
I Hercules,
l
I
5?2739
!ncorporated - 08
Safiple SampleI,IDL UN I TS
3772 [-ni trosodiphenytami ne67. us/kg
3773 4-brorcphenyL phenyt ether100. us/kg3n4 hexach t orobenzene100. uslkg
1194 pentachtorophenot170. uglkg
3775 phenanthrene33. ug/kg376 anthracene33. us/ks
47OZ cacbazole33. ug/ks3n7 di-n-butyL phthatate33. us/kg3778 fIuoranthene33. ug/ks
1 195 pyrene67. ug/ks3780 butyt benzyL phthalate67. uglkg
3783 3,3t -dichtorobenzidine
150. ug/kg
3781 benzo (a) anthracenell. uslks3781 bis (2-ethyl.hexy[) phrhatare67. ug/kg
3782 chrysene33. ug/kg
1785 di -n-octyt phthaLare67. uglkg
3786 benzo (b) ftuoranthene67. ug/kg3787 benzo (k) ftuocanthene
1f 0. ug./kS
3788 benzo (a) pyrene67. uslks
3789 indeno (1,2,3-cd) pyrene67. us/ks3799 dibenz (a,h) anthracene67. us/ks
3791 benzo (ghi) penytene67. ug/kg
01 'l 1 lloisture0.06 7. by ur.
LCS LCS
LCS DUP RPD
DUP HSRPD I'IS I.ISD RPO
tCS LIMITS
LOU HI6H
't1
17
t5
80
82
63
77
77
86
77
91
95
68
80
103
85
101
BO
7A
82
6J
t>
10c 100 0
9
10
12
7
9
8
1l
10
'10
10
I
9
8
74
s2
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ELANK
N.0.
N.D.
N.0.
N.0.
N.D.
N.9.
N.9.
t{.0_
[-D.
N.D.
N.D.
N.9.
N.9.
N.0.
l.9.
N.D.
N.C.
N.D.
81
85
74
75
71
80
t)
a?
86
55
77
93
82
81
7i
77
51.
92
94
t6
8l
81
79
90
80
92
58
6J
r03
B9
9?
80
o<
B1
39
91
86
12
13
tl
z
'10
9
'1 1
]B
53
1
14
54
27
l5
1
.L
5Z
1
33
q
17
4
147
1?7
152
176
120
IJJ
t5J
118
137
115
152
262
I4J
158
168
146
159
163
171
227
?19
101
Batch: 961840116320001A
ffigi-f,
Lancaster Laboratofles
2425 New Holland Prke
Pa Bot 12'.25
LJ.aastp. pa
"'iei5-242',1 11 -5t5-23AC Fet i-l,i -c>c-26i.
Q:TALITY CONTROL REPORT
5a: ':. e.se ). lo cr i\Dr4a J ':,rrrar$ dtP
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(l}Lancaster Laboratories 'rz12 of
A Thermo Analytical Laboratory
LLI sample No. 253809'1stat 4(4A) Grab Soit Sampte
Herculesi Bacchus Pond
4593 TcL votatites by 8240
4688 TCL SU845 Semivotatites soit
4689 TcL SU846 Semivotati r.es/Soi I
SURROGATE SUMI'IARY
SURROGATE RECOVER
d4-1,2-DCA 90
i3- toluene 95sr8 37
Phenot -d6 84Z-Fl.phenot S'l
?,t1 ,5'f BP 1DS
lli trobz-ds 97
Z-Fbiphnyt 85Tphenytdl4 80
I
I Group No.
I nercutes,
I
I
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5??739
Incorporated - DE
SURROGATE
LCU
70
aa
71
2l+
25
19
23
l0
t6
LII'IITS
H I6H
ttl
117
121
113
121
12?
120
115
137
ll
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rl
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Lanca5ter Laboratofle5
2425 l'.le,N Holland Prke
PC Ecr ll-12S
Ld-.;;l.r PA r7605-2425
71;-556-2300 Fax | \,^.'c56'2631
il
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QLTALITY CONTROL REPORT
MEMBEFl
lee .eye.se srde ior ? 49,a.al on oI ; /noois and Jbb.evrairons 1 0/lcl95
.I COPY TO
1 COPY TO
CAT
r{0.
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(I)La ncaster Laboratories
A Thermo Analytical Laboratory
LLr sample No. ES 2538085Cottecred: 6/27/96 ar 10:35 by BR
Subritted: 6/28/96 Reporred: 8/ 6/96Discard: 9/ 6/96
Stat 1(18) Grab SoiI Sanpte
Hercutes: Bacchus PondSI11B SDG#: HBP02-06
i Account !{o: 05716
I Hercutes, Incorporated - DE
] Envi r-onmenta L Affa i rsI f iLminqton cE ]989/+
AS RECEIVED
::::.:::i:::::il;;1:::::r::::::f::': - l"tETllOD
.,r,i;i::.il'i.ll:::,$!lrf s,:,:t::. DETEcII oll L IM I T UN I rs
P.0.
Rel. -
Page:
DRY UEIGHT
4593
1625
1643
164t+
1646
1647
1649
165 1
1 651
t6)4
1555
1 658
lbo I
1666
1672
6935
6936
0r 59
4688
4689
011 1
13.
3.7
)1
t. t
c .07'l
0.13
c-45
Lr .4t
1.32.i
0.4t,
0.{50.i8
D.:4
c.0?5
See Page
n9/kg
n9/ <9
mglkg
ng/kg
mg/kg
flrlr/ kg
nq/k tm9/.i!
Blg/ <9
rng/'(9
ng/ <tJ
irg/ <!
fitg/k9
m9/ <g
m9,/ k E
ln9./ <'J
m9,'<9
See Page
See Paqe
ANALYSIS IIAME
TCL Votati Les by 8240
Thal.tiun
A Ir.uni nurn
Ant i fllony
Bar i um
Beryttiun
Cadniun
Ch romi w
Copper
I ron
Lead
ilanganese
N i ckel.
Si Ivec
Zrnc
Arsenic TR
Seteoiun TR
ftercury
TCL SU846 Semivolati Les Soi t
TCL SlJ8,46 Semivotati tes/Soi L
Moi sture
"Hoisture" represents the Ioss
103 - 105 degrees Cetsius.
:.r:lrli',1.:::,,ii.REStlLIS',,,.':
METHOD
DETECIION LIIIIT
11.
2.7
2.7
0. 090
0.16
0.57
0.51
4.1
2.9
0. 15
0. 55
0.s5
c.49
0.30
0.2?
0. 035
3
1:::.r:-:tt-i:-i\:::,: - :: :- . -,?1. t
in ueight o{ rhe sampLe after
C.C6 i by rt-
oven drying at
flercutes, Incorporated
ERM - Rocky Hountain
ouest ions? Contact your CL i enr
Rachel L. Kream.-r
l5:22:15 D 0002 ?t REP310 25.00 0r.j1121,CC ASRC|C
Lan(a5ter Laboratofles
M E M B E R 2425l\lewHoilandPrke
ATTN: l'1r. Joseph Ket Ler
ATTH: I'lr. Erent Robinson
Servi ces Representati veat (7'7) 650-2309
1 25416 5??7i,)
RespectfuL l.y Subni tred
Ran:ona V. Layfilan, 6roup Leader
! CP iYeaalrs/Leachates
?A e.! 12 rzt
Lan(a!,er. ri i ; bajS _2J,1 _::1i-ar;-zic) Fax -r. ::,; -';ii
tt?.i)ce .evPrse :rde ior t. pld-3i oa :; : rmoois anrl abCrevraiio^j
(I)La ncaste r Laboratories
A Thermo Analytical Laboratory
2538085by BR
8/ 6/96
!
i Account tlo: 06716
i tercul,es. :nccrporated - oE
I Envi romentaL Atia irs
I ui tri ng,on DE i9894
I
Page:
DRY UEIGHT
.t,i::.,ii'ii:i;,ii::.:ij,il,,:,'.;l'r.,.i,,,',lr;.:,,., HETH00
::ir::::.j:i:ii:ii;:REEAl is,ii i.,i: D E I E c T I 0N L I H I T
.,.,'.t,.',',,'.,'.N'; 0:i:.i,.'i:
:li',::.'t::l:,::,i li, o.,:l:.'i:,'::,,:, r' ^,,,.::
:.1;::r:i: :.: :: :N . D:.j:.i:::::,:,:],,}.}.
LLI Sampl-e No. EScoItected: 6/27/96 at 10:35
Subfli tted: 6/28/96 Reported:Discard: 9/ 6/96
Stat 1(18) Grab Soi t Sampte
Hercules: Bacchus PondsI11B SDG#: HBP02-06
CATNO. ANALYSIS IIAME
TcL voLatites by 8240
3434 Ch toromethane3435 B.omomethane3436 Vinyt Chl.oride3L37 Ch I oroethane5440 llethytene Chtoride4A71 Acerone4076 Carbon 0isutfide1180 1,1-0ichtoroerhene341? '1 ,'l -0ichtoroethane
3t,44 Chtoroform
3t,15'1,2-Dichtoroethane/.085 2-Eutanone34+6 1 ,1 ,1 - trichLoroethane34/,7 Carbon Tetrachtoride4091 Vinyt Acerate
311+8 Bromodi ch Ioromethane3450 1,2-DichLocopropane3151 cis-'1,3-0ichtoropropene1181 Trichtoroethene3452 Dibrornochloronrethane3153 1,1,2-TrichLoroethane
1 182 Benzene3451 tcans-1,3-0ichIoropropene3456 Brornofocnr4108 4-l'lethyt-2-penranone4107 2-Hexanone3457 Tetrachtoroethene34t-? 1,1,2,2-Terrachtoroethane
I tdJ totuene
'l 184 Ch Iorobenzene3458 EthyIbenzenel+117 styrene3355 xytene ( tota[ )618T trans - I ,2'D i ch toroethene6277 cis-1,2-DichLoroethene
P.0.
Ret -
1l
]l
]l
AS RECEIVED
::::::;::::i:j::f:i-!ii::::::r:::i:::i::::.:j.::: METIiOD
iliil;:'#I.EF, lJttqrl:.::::: DETEcT I 0x L I r't I T uN I rs
j::i:::'.:r:': ::.. :.: "fl 'u. :
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::::l:::::::::,1:i:,::,i:i::,i::r::::::.i:'ll _ t. :'r'i :ii:'::r'::':ii::::r i, : -
::::l::iit:'l,liili:::::.i::::;:.:,:i',.:ll. D,. :.,
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,1:::,:if:jl'i:::l,,;:'':,:::j'l!.t. l'
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u9/ <9
u9/ <g
u9/ <g
u9/ ig,
u9l *9
19/ <9
rgl <')
'.rgl <g
't9/ <g
ug/ kg
\r9/ <'.a
rg/ <g'jq/'<g
ug/\9
'.i91 <!i
'tg/ <g
u9,/ <9
ug/'(g
u!/ <g
u9l<g
rg/'<9
,Jg/ks
ugl <9
u9/ t9
ug/ <g
ug/<g
u9/'<cJ
uc)/ <<J
ugl <g
u9l k:n
ug/ <9
ug/<9
u9/<9
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::::,.::: )i::0 I
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: :::.:i::::,:::.1::r:, :: ' M i.O.
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Questions? cont.rcr your Ctien: Services Reprcsentarive
Rachel !. Kreanrer a"- (7^7) 6ib-Z1ltJ
Lancaster Labora(ofles
2425 New Hoiland Prke
PO 8ox 12125
Lancas:er PA 17605-2ar-5
7 I 7-555-2-r00 Fax: : i ;';-:6-:56 I
tl'
',,r0,r, ?tJ
RespectfuL Iy submi tred
Michele McCtal-in, B.A.
Group ,eaCer, GC/FS Vol.ati tes
SCe ,?,..r.:: : :e 't. i,: ;.a!,Cn Oi:ymi;r; trid aobreridtioi: -rl
MEMBER
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LLI Sample No. ES
Co[ [ected: 6/27/96 at 10:35
suunitred: 6/28/96 Reported:Discard: 9/ 6/96
Stat 1(18) Grab SoiI Sampte
Hercutes: Eacchus PondSIIlB SOG#: HBP02-06
CAII{O. AHALYSIS IIAME
TCL Su846 Semivotati Les Soi t
1 185 phenoL3753 bis (2-chtoroethyt) ether'1186 2-chtorophenot375!" 1,J-dichtorobenzene1187 1,4-dichIorobenzene3755 1,2-dichIorobenzene4090 2'methylphenoI4691 2.2'-oxybis (1-chIoropropane)469? 4'methytphenoI1183 tl-nitrosodi -n-propyIamine
3757 herachtoroethanE3758 ni trobenzene3759 i sophorone37t-6 2-ni trophenoI37t7 2,1-dimethy!.phenoL3760 bis (2-chtoroethoxy) merhanei718 2,4-dichtorophenoL
1'189 1,2.4'trichIocobenzene3761 naphthatene4693 4-ch(oroani I ine3762 hexachlorobutadiene'1190 4-chtoro-3-methytphenoI469t* 2-methytnaphrhatene3763 hexachtorocyctopenradiene3719 2,4,6-trichiorophenoI1695 2,4,5-rrichr.oroohenoI376!1 2-chtoronaphthatene1696 2-ni tnoani t i ne3766 dimerhyt phrhatate3765 acenaphthylene
I Accoun! llo: 06716
i ttercuIes, Inco.porated - DE
I Envi rorrnentat Af fa r rs
ItJr Lrnincron DE '19891+
I
AS RECEIVED
METHOO
RrSULIS DETECTI0!i LII',llT UlllIS
ORY IJE I G}IT
irr::i:rj::..:::it::r::i:r.::: METH00
,l'iFESULIS',,:',, DETECTICN Lf HtT
I of 1!
1?.
84.
42.
42.q?.
4?.
84.
130.
130 .
84;
84.
42.
8l+.
12.
12.
4?.
42.
130.
84.
42.,1n
84.
8/. .
4?.
o+.
42.
4?.
P.0.
Ret .
M;0 ..'
N: D.
l{.c.,
H. D.
l{: ?,,
H.LI-,
M,r.'
lt . r;.
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67.
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57.3i.
67.
07.
c7.
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?:
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5;.
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17C.
67.
07.
67.
i3.
u9/ k9
u9/k9
ug/ <9
u9/k9
tJg/ <g
u9/ kg
,tg/ <g
u9/ (g
u9/ <g
!9/ <9
\9/ <e
:q/ (s
u9l i9
u3l (g
ug/ <g
r9l.i9
ug/ r9
19/ <ti
!9/ <g
usl i9
u9l k9
!9/ <c)
ug/ <<J
u9 / <<J
r3l k9
r9/ <!
')g/ lg
)9/ <g
t)9/ <ci
'J9/'<9
Ouestions? Contact
RacheI L. Kreamer
your CL ient Services Repcesen:ative
at (7"7) 6i6-2300
Resoec:fuI Ly Subrni tted
chcistine M. Rarctiff,
crouD leader, 6ClMS
. )a :.--aa.. r,:.j iaiJre._,1ai,.ta!
B.S
Ldncdster Laboratories
2425 New Holland Pike
PO 8ox 12425
Ldn(aster. Pa l75il5'ld:i
717'696-llCC iar 7ll ri:i'l:i
(l)Lancaster Laboratories
A Thermo Analytical Laboratory
2538085
by 8R
8/ 6/96
MEMBEFl
-i-- r a i,,
t'!D-
,",t.rr, ?a,J
3l
(l)Lancaster Laboratories Paq e:4 0t tlA Thermo Analytical Laboratory
LLI sampl-e No. ES 2538085Cottected: 6/27/96 at 10:35 by 8R
Subrnitted: 6128/96 Reported: 8/ 6/96Discard: 9l 6196
stat 1(18) Grab Soi t Sampte
llercutes: Sacchus Pond
ST1 1B SoG#: HBP02-06
CATI.IO, AIIALYSIS NAI.IE
TcL Su846 Semivolati Les/Soi t
4697 3-ni troani I i ne
.1 191 acenaphthene3750 2,4-dinitroohenot1192 4-nitrophenol-4698 di benzofuran'1193 2,4-dinitroroluene4699 2,6-dinirrotol.uene3770 diethyt phrhatate
3769 4-chtorophenyt phenyt ether
3768 ftuorene1700 4-ni troani t ine4701 4,5-dinitro-2'rnethyIphenot3772 N-ni trosodipheny'.antine37Ti 4'bromophenyt phenyL ether3T7r- hexach I orobenzene1194 pentach!.oropheno!3775 phenanthrene
3776 anthracene4702 carbazote3777 di -n-butyt phrhaIate3778 f Iuoranthene
'i 195 pyrene3780 butyt benzyl phthatate3783 3.3' -dichlorobenzidine
37A1 benzo (a) anthracene37?!, bis (2-ethythexyt) phthatate3782 chrysene3785 di -n-ocryt phthatate
37eb benzo (b) {Luoranthene3787 benzo (k) fiuoranthene3733 benzo (a) pyrene3789 indeno (1,2,3-cd) py.ene3790 dibenz (a,h) anthracene
3791 benzo (ghi ) peryLene
I
I A..ounr No: 06716
i xercutes, tncocporated ' DE
i Envi rorrnentai Affa i cs
I uilminoton cE i9694t-
I
AS RECEIVED
METIIOO
DETECilori !_tlilT UilrS
DRY UEIGHT
i,i'..,ti::::.::ili::::.:j,iti:,r,::.r::ii'if:.:..'::i; METHoD
ii.:i:::i:iir.illEsULl:::,l.,i DEIEcI I 0N L I ir I I
on
Re[.
i:rit:::::i:::ii::-::s.:,:.:i:.: :::: :.:.:::
::i!:::!:::::liii:: :.:.DlrIirjT (a.j :
67.
17C.
17'-1.
31 .
b7.
67.
07.
67.
1C0.
170.
67.
1C0 .'rc0.
-i-i,
ii.za
o,.
67.
llc.
:.3.
67.
67.
lf,L' .
o7.
07-
67.
u9/Kg
u9/ <9
u9/ i9
u9/ <g
u9/ks
ugl (g
u9/ <g
ugl (9
!9/ <9
u9/ ks
ug,i kg
ue,t <')
ug,/ <g
uglkg
ugl (9
uglis
uEl (9
tJ,J/ <g
'J9./ <g
ugl ig
u9/ (9
ug/'<g
u9/'<9
ug/ <9
u9/ (9
ug/ (g
u9/ k<)
u,r/ <g
ugl (9
u9/ kg
u]/ ig
'!9/ <g
ug/ k ri
u9/ <')
,',, 84.
t41.," 210.,, ,1n
',, 42.
" 84.i. 84,', e1.
fr.,:.,:,'. 4?.,,,i 110..: zrn
:;, 130.,:', 130 .
:,:';; 42',,: 12.
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l.::1 42.:i o,
:,:., 1 70.. ., 41.
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, AJ
f,';i 84 ':,.::: 170.,)1,:,,, 94,
oc.'' Bl+.,,..'. 84 .
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ouest i ons? Contact
RacheI l-. Kreamer
your Ct ient Services Represen!arive
at [phone]
Respec,: f uL r-y Submi t tedChristlne 14. Ratctiir,
c.oup'-eader, 6clli5
!, r9o!., dac ;::.? /lalrcas
Lancasler Laboratories
2425 tlew Holland Prke
PO Bor I 2a25
Lancairar PA 17605-:J:5
717-555-1100 Far il;-556-1631 ':i I
I
See iev€rse t,Ce :Or erp,.la;i a_ :22 15 Rev 10./-1O95
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&&&
tlercules: Sacchus PondSI118 SDG#: tl8P02-116
CATNO ANALYSIS IIAME
4593 TCL Vol.a(i Les by 8240
1625 Thaltim16/.3 Atunrintln
1644 Antlmony
1 6q6 Bae i unr
16117 Eeryttium
1 649 Cadoi um165'l Chronri unr
1 65i Copper'1654 I ron
1 55 5 Lead
1653 l.langanese
1661 Nickel
1666 S i Lver1.672 Z i nc
5703 StJ SU846 ICP Digest69i5 A.seni c TR6936 SeIenlum TR
0i 59 t'lercury
571 'l SU 511846 I.l9 D isest
0381 0NA Soi t Extracrion
4683 TCL SUB4o Senri votati Ies Soi I4689 TCL SU546 Senri votat i tes/So i L
01 I1 I'roisture
!lETHOO
su-846 82408
su-846 6010A
stJ-845 631 0A
su-846 6J10A
su-846 6C1 0A
su - 8/16 6t 't 0A
su-846 6C10A
su-846 6010A
S',,1-84o 6010A
s'J-845 6310A
su-346 6C 1 0A
su-8/.5 6J'r CA
:lu-346 6liCA
sr,J - 346 6t 't 0A
c!r-D/a !ila,
s,J-346 3050A
s'J-846 6Ci0A
su-345 6!10A
su-846 7(71A
59-846 747]A Modi f i ed
Su-845 3550A
s'J-846 82708
su-316 8270s
EPA 160.1 (modified)
ANALYS I S
IR I AL DATE AX!' 1 tME
1. 07/03/96 05?l
. 07/1,3/96 1759', 07 /':\/95 17591 D7/",3/9r. 17'"9. a7/..3i96 1759': 07/13/96 1759', 07/',-:i9o 17591 07/13/9b 1759I A7/13/95 17591 07/"3/95 1759' 07/i3/9o 1759^ D7/13/9o 1759' a7/'3i96 i75;^, 07/1.3/9b',7tt-1 D7/1,:/r5 1759'\. c7 / c?is' 1934"t 07 / 1 _1/56 1759' C7/1,7/95 991.1
. c7/133/96 16251 07/q?/96 15C6
1. 07/01/96 193t)1 07/45/95 lt'C': 07/05/95 1,t:'.0
i 07/02/96 152A
I,ABORATORY CHRONTCLE
Page: 5 of 1'l
ANALY ST
Ctark A. Dougherty
Jolene il. Schie!.cis
JoLene M. SchieLcs
JoLene f!. SchieLis
JoLene I. Scnielcis
iol.ene l'!. Schietcs
JoLene 11. S.iiel.cs
JoLene !1. Schie'.cs
JoLene tl. ScSieLcs
JoL;ne il- SchieLds
Joi.ene M. Sc;riel.cs
JoIene I'1. Schielcis
Jol-ene !!. Schielcs
..io ! r.ne i'l . Sc:r i e i. ds
iciene 1!. Schle!.cs
Desi it. Caroz:a
Jor.ene lt. ScnietCs
Nina a. Ha!.Ler
I'leLLi S, Farkaryan
FTances A. Demorest
Sherry Lynn DevLin
,ioseph I. oambter
Josep|l l,1.6ambLer
Ieel.ay B. lilehta
(iI)La ncaste r Laboratories
A Thermo Analytical Laboratory
LLI sample No. ES 2538085Cottected: 06/27t96 ar '10:35 by BR
Subnri tted: 06/?8/96
Stat 1(18) 6rab Soi t Sampte
Account No:36716
ilercuLes, I ncorporated
Envi ronment.r L Affa i rs
lJi tmington CE 19894
LancaSter Laborato,reS
2425 Nerv Holland Prke
PO Bor 12a25
Lancasier PA I :r:C5.lll5
717-656-2i011 Ser 7ll ii6 lt:
o'
22lo Rev ,0/iC/95 ?e;- cct) n- c jcc'eYrd!lonq
(l)La ncaste r Laborato ries
A Thermo Analytical Laboratory
Q'JALITY CONTRCL REPORT
Page: 6 of
LCS LII'I!TS
LOU HIGH
il
,]l
trl
1l
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il
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LLI sample No. 2538035
Stat 1(lB) Grab SoiI Sample
Ilercutes: Bacchus Pond
Gfoup !lo. 52269
Hercutes, Incorporated
Samp t e
IID L
SampLe
UNITS
DUP MS
RP9 MS HSD RPD
LCS LCs
LCS DUP RPD
/i591 TCL votatites by 8240
3431 Chtorornethane2. ug/kg
3435 Bromomethane3. ug/kg
3436 Vinyt chl.oride2- u9/k93437 Ch Ioroethane3. ug/kg
3440 Methytene Chtoride7. ug/ks
LO74 Acetone7. u!/ks
4076 Carbon DisuL;ide3. us/kg
1180 1,1 -Dichlocoethene
2. ug/Y.g
3l+42 l, 1 -0ichtoroethane1. ug/kg
3414 ChIoroform'I . ug./kg
34t+5 1,2'DichIoroethaneZ. ug/kg
4085 2-Eutanone7. us/kg
3146'1,1, 1-Trichtoroethane1. ug/kg3447 Carbon Tetrachloride
'l . ug/kg
4091 Vinyl Acetate3. ug/kg3448 Bromodichtoromethane2. us/ks3450 1,2-0 i ch (orc,pcopane
3. u9/'L93454 cis'1,3-Dichtoroprooene1. ug/kg'1181 TrichIocoethene1. ug/kg
3t 5? Dibromochloromethane1. us/kg
3153 1,1,2-TrichLoroethane2. ug/kg
1 182 Eenzene
1 - uslkg
1451 trans-1,3-DichloroproPene1. uglkg
BLANK
Batch: E961Bl1AB
N.0.
N.D.
N.9.
N.D.
?. J uglke
N.!-
!,1.9.
N.!.
N.D.
N.3.
N.D.
N.9.
N.D.
N.D.
N.D.
N.0.
x.0.
N.D.
N.D.
N.0.
N..1.
N.9.
N.r.
90
99
91
10?
S3
132
i07
99
96
93
102
105
'104
99
92
93
96
109
90
9t
c)Z
93
87
98
100
101
99
78
100
:01
95
95
92
g11
105
't 0c
al
90
98
98
107
92
96
92
395
295
5 102
10 89
396
11 88
2 10:
6 105
455
295
191
?a 95
1 105
3 103
20 105
295
0 101
z 102
2 111
396
298
2 10t,
1 93,
9B
a,..Orr, ?a *
1
1
1,
10
1
'19
24
59
51
19
22
70
19
35
I
1
7',
53
37
17
?72
250
254
z?1
150
id5
?33
155
138
155
167
16?
140
190
t))
2no
))a
157
149
150
151
181
Lancaster Laboratortes
2425 Ne,A Holland Prke
PO Bor l2J:5
L-ioc;sie, it !r-605-2125
; i7-55o--1i00 ;ar ll i-65ij-2b8 I 1:Ot 1 1a.: .tooi:n.r,dt:ort5
t!'l-,J
LCS I-CSI.CS DUP RPO
DUP !:S
RPD I'IS MSD RP9
(1)
(z)
I
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(I}Lancaster Laboratories
A Thermo Analytical Laboratory
QLIAIITY CONTROL REPORT
't 'l
LCS LII'IITSI-OIJ H I GI
LLI sample No. 2538C85stat 1( 18) 6cab Soi I Sampte
Hercutes: Bacchus Pond
Group No. 52269llercules, lncct'porJ(ed - DE
Sampte sanpleMDL UN I TS
3456 Bromoform
'1 . ug/ kg
4108 (-t'tethyt -2-pentanone
3. us/ks
4107 2-Hexanone3. ug/ks
3457 Tetrachtoroethene1. uglkg
3t t+9 1,1,2,2-tetrachLoroethane
'l . ug/kg
1 1 83 ToIuene
1 - ug/ks
1 1 B1 Ch I orobenzene
'1 . ug/kS
3458 Erhytbenzene
1 - ue/kg
4117 Styr^ene1. uglkS
3355 xytene ( total )1. ug/kS
6187 trans-1,2'Dichtoroethene2- us/kg
6277 cis-1,2-D ichLoroethene2. ug/kg
1625 Ihat L iun11. ms/ks
1643 A[uminm8.7 mg/ks
1644 Ant imony?.1 mg/kg
1646 Barium?.1 mg/ks
1647 BeryItim0-071 ns/ks
1649 CaCmiunrtl.13 mg/kg
1651 Chromrum0.45 ms/ ks
1653 Cooper0.48 me/ks
1654 I ron
3. I mg/ kg
1655 Lead
2 .3 m9/ k9
1658 Manganese0.12 mg/kg
1661 N i ckel0.t,1 nlq/kg
1666 Silver0./.3 rrsl!.g
BLANK
N.0.
H.0.
N-0.
N.D.
N.D.
N.9.
N.D.
N.0.
N"D.
N.D.
N.D.
Batch:95'184570B00i
N-0.
Eatch:961345708!Cl
il.0.
Batch:95'1845708!03
N.D.Batch: 961845708C03
ri.D.
Batch:96'1845708C03
N.9.
Eatch:961845703!01
N.D.
Barch:9613457011C0i
N.D.
Batch: 951845703003
Batch:96',]8457C80017.2 J mS/kS
Satch:9o1345708.10i
N.9.
Batch: 96'18457083C1
N.0.
Batch: 96184570810i\.0.
Earch:961845708i03
N -0 -
83
98
'1 01
115
100
't 05
96
107
99
105
'1C4
'105
(1) 93
21 2s27
(1) 92
9 105
0 (1) 96
0 (1)
0 ('1 ) 123
0 (i) 119
! I a/ (,
0 (1) 96
]',] ',r16
0 (1) E7
(1 ) 1D2
83
90
': 10
9t,
101
96
104
9?
133
98
101
39
16/,5 (2)
95
97
9'l
FA
11',
'09
2.39 (2)
9C
109
9l
97
6
7
1.2
I
7
0
3
7
Z
6
4
6
9
z
7
5
7
1
6
t,
7
5
6
7
93
9C
91.
i '15
97
1 0'1
97
103
i01
1C6
101
102
96
79
100
98
99
102
102
B9
91,
9/,
96
9g
145
50
5?
64
46
17
37
5t
30
51-
50
50
?1
70
26
54
57
ol
53
69
55
50
'169
't40
tco
157
150
160
l6t
200
i)o
t)6
'150
165
299
111
111
112
112
ti)
116
1 /.7
The resutt for one or both determinations
The baclground resull !as more than for-:r'
Lancasier Laboratones
2425 Ne,n Holland Prke
PO Bor 12d:5
the 100.
3l
Sanp t e
MDL
Sampte
ulrlTs
LCS
LCS DUP
92
93
aa
79
76
76
74
TI
62
90
77
80
76
4t
t>
77
LCS LIIIITS
LOU HIGH
Il
il
ll
il
il
il
ll
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I
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(I)La ncaster Laboratories
QTJALITY CONTROL REPORT
Pa-oe: 8 of 1'lA Thermo Analytical Laboratory
LLr sample No. 2538085
Stat 1(18) Grab Soit SanpLe
Hercutes: Eacchus Pond
Group No. 522139
tlercutes, !ncorporated DE
OUPRPO MS TISD
LCS
RPD
MS
RPO
6
0
167? Zinc0.38 mg/kg
6935 Acsenic TR0.24 mg/kg
6936 Setenitm TR0.17 mg/kS
0159 llercury0.028 mg/ks
t;688 TCL SU846 Semivotari tes Soi I
.1 185 phenot
33. u9lk9
3753 bis (2-chtonoerhyt ) ether67. us/ks
1 186 2-chlorophenot33. uglkg
3754 .l,3'dichtorobenzene
33. ug/kg
1187 1,4-dichtorobenzene33. ug/ks
3755'1,2-dichIorobenzene13. us/ks4690 2-methytphenoI67. u9lk9
1691 2,2''oxybis (1 -chtoropropane)
1 00. uglkg
4692 4-rtethyipheno(
1 00. ug/ks
'l 188 [-ni trosodi -n-propytami ne67. u9lk9
3757 hexach t oroethane67. ug/kg
3758 ni trobenzene31. ug/kg
3759 i sophorone67. ug/ks
3746 2-nitrophenot67. us/ks
3747 2,1' dinethytphenoI67. u9lk9
3760 bis (2-chLoroethoxy) tnerhane33. ug/kg
3718 2,L-dichtocophenoI13. ug/ks1189 1,2,4-trichtorobenzene33. uglkg
3761 naphthatene
u9/ k9
BLAN K
Batch:96'18457080030.80 J mS/kS
Barch: 961845708?03
N.D.
Batch:961845708003
N.D.
Eatch: 96184571 1002
N.0.
Batch:9618fSr-8025
0 (1) 108
0 (1) 91
0 (1) 92
0 (1) 92
98
9Z
94
92
54
49
5Z
26
149
149
149
157
5 11?
12 158
23 134
1 172
32 129
46 123
36 165
5 152
1 230
t0 113
35 180
21 196
29 18?
32 119
33 18L
39 135
14 1t?
2., 133
Ihe resutt for one or both detertnina!ions
72 82
75 84
69 78
75 79
a/ 10
72 77
69 80
6? 70
8t, S7
74 84
75 83
77 83
3l 9?
74 82
/+8 57
T3 81
71 81
77 82
71 77
Has less than five tinles rhe LOQ.
N.9.
[.D.
N.D.
N.D.
N.D.
fl.0.
N.D.
N.D.
u:D'
N.D.
[.0.
N.D.
N.D.
N.0.
N.D.
N.0.
N.r.
N.9.
N.3.
13
11
1l
5
5
6
15
11
tq
13
10
7
10
9
17
11
IJ
6
5
Lancaster Laboratofles
2425 Ne,, Holland Pike
PO Scx 12425
Lae.asiel PA 17 6A5 -}!.Zt
;li-656-2100 Fax 717-.i55-2631 -
tt
.... ,nr,O,'ra ?t O'ree..?€.)i ide fC.:(r ii-rt.o^,)i 5yrreC:s uel: lo1r"y,61,a^t
I
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75
(1)
I
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(I)Lancaster Laboratories
A Thermo Analytical Laboratory
QUALITY CONTROL REPORT
Page: 9of 11
LLI sample No. 2538085Stat 1(1B) Grab Soi t Sampte
Hercutes: Bacchus Pond
I Grouo Ho. 5227J9
I nercutes, lncorporated
I
l
Sampte SampteI1DL UN I IS
4693 4-chtoroani tine100. ug/kg
376? hexachlorobutadiene67. uglkg
1 190 4-chIoro-3-nrethytphenot67. ug/ks
469t, 2-nrcthytnaphrhatene33. ug/ks
3763 hexach Iorocyclopentadiene170. us/kg
3749 2,4,6-trichtorophenol67. ug/kg
4695 2,4,5-trichIorophenoI67. ug/kg
3764 2-chtoronaphthatene33. ugl ksL696 2-ni troani t i ne67. u9lk9
3766 dinethyL phthalate33. ug/kg
3765 acenaphthytene33. us,/ks
t 697 3-ni troani I i ne67. u9/k9
1 191 acenaphthene33. ug/ k9
3750 ?,4-dioi rrophenoI170. u9/k91192 4-ni trophenot170. ug/ks
4698 di benzofuran33. ug/kg
'l 193 2,4-dini trototuene67. us/kg
4699 2,6- di ni trototuene67. us/kg
3n0 diethyt phrhatate
67. ug/ks
5769 4-chlorophenyI phenyt ether67. ug/kg3768 f Iuorene13. ug/kg
4700 4-nitroani t ine
100 . ug./ks4701 4,6-di ni tro-2-methytphenoI
1 70 . us/kg
DUP !SRPD HS MSD RPD
LCS LCS
LCS DUP RPD
LCS LIHITS
LOU HIGH
17 116
2L 116
?2 147
28 1?3
1 100
37 144
39 151
60 118
53 143
1 11?
33 14s
7 143
47 145
1 191
1 132
28 131
39 139
50 158
1 114
?5 158
59 1?1
38 1ZZ
1 181
B LA}IK
N .0.
[.0 .
N.D.
N.D.
N.D.
n.!,
N.D.
N.D.
N.9.
N -9.
N.0.
[.0.
N.3.
N.D.
N.0.
N.D -
N.D.
N.0.
N.D.
N.).
N.0.
N.9.
N.D.
11 15
80 87
75 86
at. a)
17 16
31 9C
3C 89
79 85
7? 78
79 87
75 81
4
9
36 10
71 78
59 55
73 77
74 30
&2 89
31 89
79 88
79 87
7t 80
59 6?
66 7?
5
9
13
10
7
11
10
8
a
1C
I
43
B1
a)
78
6?
82
32
79
75
80
77
4689 TCL SU8/t6 Seflrivotati les/Soi t Batch: 96183S18026
10
9
I
6
8
7
10
10
10
7
56
T3
63
7q
76
90
85
83
B4
79
76
66
Lancaster Laboratores
2425 New Hollanci Prk€
PO Bor 12,125
La.(a5ier PA lTqC!-:1.'
;17-655,:loc .. i :r: .r.r.r .5il
Q9,
,nrta'r, ia -i!ee,e','erle 5to: ic)r :rc,;naI'or cI nr2r!::.. c aoore',rciiiD.
MEMBER
(I}La ncaste r Laborato ries
A Thermo Analytical Laboratory
QUALITY CONTROL REPORT
Page: 10 of 11
LCS LII'IITS
LOU HIGiI
38 147
53 127
1 152
14 176
5t+ 120
27 133
3s 133
1 1t3
26 137
52 115
'1 152
1 262.
33 143
8 158
17 168
4 116
24 159
'l 1 163
17 161
1 171
1 227
1 ?19
'100 101
ll
1l
rt
ll
1l
It
II
LLI sanple No. 2538085Stat 1(18) Grab Soit Sarnpte
Hercutes: Bacchus Pond
I
i
I
I Group llo. 522239
i tlercutes, lncorporated - DE
I
I
i
Safipte SampteIiIDL UII I TS
3772 ll-nitrosodiphenytami ne67. uglks
3773 4-brornphenyt phenyt ether
1 00. ug/kg3774 hexachtorobenzene'100. uglkg
1194 pentachtorophenoI170. ug/kg
3775 phenanthrene33. uglks
3776 anthracene33. ug/kg
47OZ carbazote33. ug/kg3777 di-n-butyt phthaIate
33- uglkg
3778 fIuoranthene33. us/ks
1195 pyrene
67 - u9/k9
3780 butyt benzyI phrhaLate67. uglk.g
3783 3,3' -di chtorobenzidine130. u9/k9
3781 benzo (a) anthracene33. u9/k9
3784 bis (2-ethythexyt) phthatate
67. us/kg
37AZ chrysene33. us/ks
3785 di -n-octyt phthatate67. ug/kg
3786 benzo (b) ftuocanthene67. ug/ks3787 benzo (k) ftuoranthene110. u9lk9
3788 benzo (a) pyrene67. ug/ks
3789 indeno (1,2,3-cd) pyrene
67. ug/kg
3790 dibenz (a,h) anthracene67. uglkg
3791 benzo (9hi) perytene67. us/kg0l1l Moisture0.06 % by tt.
BLANK
[-D.
N.9.
ll-D-
N.D.
N.D.
lt.D.
I.D.
N.9.
!{.0.
N.D.
ll.D.
N.D.
N.D .
il.9.
N.9 .
N.D .
N.D.
N.0.
N.D.
N.9.
N.D.
N.D.
Batch : 961840116820003A
LCs LCSLCS DUP RPD
OUP MS
RPD l'1S l.lSD RPD
81
o2
74
7t,
71
T5
6J
e6
55
77
93
82
81
7i
77
7t,
82
oz
79
E4
92
91
76
83
31
90
80
92
97
58
83
103
89
92
80
81
89
91
11
I
10
12
5
7
9
I
13
10
10
10
9
8
il
;
l1
rl
'r
T
,l
I
,l
T3
82
63
77
77
7B
B6
77
91
95
68
80
85
103
80
1A
8l
75
100 100 0
1?
13
13
z
10
9
7
Lancaster Laboratones
2425 New Holiand Prke
PO Bcr :1125
LJnCi\iE, PA | /',, --- j - L:
7lr-656-:i00 = j : -.'.aa-ilat,':: Iii 6 'e : i:1 )At )l
11
I
I
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LLI sample No. 2538085Stat 'l(18) Grab Soit SampLe
Hercutes: Bacchus Pond
4593 TCL Votatites by 8240
4688 TCL SU846 SemivotatiLes SoiI
4689 ICL SU846 Semivotatites/Soi L
Hercutes, Incorporated - DE
QUALITY CONTROL REPORT
SURROGAIE LIITIIIS
LOU H I GII
70 1?1
8,1
21
Lancaster Labo ratoriesA Thermo Analytical Laboratory
TRIAL ID
Lancdster Laboratorres
2,125 I'le'{ Hollano Prke
2O Box 12.129
Laocdsi?.. PA I | 6A5-2. :"')
t- 1 ,- -'.',6-))CA Fil '- 1:t' .
SUR ROGATE
SURR OGATE
d4-1,2-DCA
d3- to L uene
5t u
Pheno I -d6
2-FIphenot
2,4,6-fs?
Nitrobz-d5
2-Fbipnnyt
ipheny'ld l4
SUMTAR Y
RECOVERY Z
ao
vq
90
81
77
96
s7
78
67
?5 12119 12?
23 120
13
ot
,,r,,,, ?aJ
Group llo. 522f59
; -'Cc.; inO iOilrF,,rnlrlni
HI
3l
1l
1l
1l
Il
ll
il
il
It
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La ncaster Laborato ries
A division of Thermo Analvtical lnc.(I)
CAI
[o-
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4593
1625
1643
1644
1646
1647
1649
1651
1653
1654
1655
1558
1661
1666
1672
6935
6936
01 59
4688
4689
0111
LLI sanple No. ES 2538096Cotlected: 6/?6/96 at 13:05 by BR
suunitted: 6128/96 Reported: 8/ 9/96Discard: 9/ 9/96
Cu-4 Disc. crab SoiL Sarple
Hercutes: Bacchus Pond
S4DIS SDG#: HBP02-17
Account llo: 06716
Hercutes, Incorporated - 0E
Envi ronrnentaI Af fairs
lJitmington DE 19894
Page:
P.O.
Re[.
Respectfut ty subni tted
Ramona V. Layman. Group Leader
ICP lletats/Leachates
lof 12
,e
221. Qe,,, 5/0r c. ?a J
AIIALYSIS }IAI.IE
TCL votatiLes by 8240
That t iun
A luuni nun
Ant i mony
Bar i un
BeryI t iun
Cadri um
Chromi um
Copper
I ron
Lead
llanganese
lIickeL
Si Iver
Zinc
Arsenic TR
Seteniurn TR
llercury
TcL StJ846 Semivotatiles Soit
TCL SU845 Semivotati tes/Soi t
llo i sture
1 CoPY T0 Hercutes, Incorporated
1 CoPY T0 ERl.l - Rocky llountain
14.
9.0
2.2))
0.074
0.13
0.47
0 .50
3.4
?.4
0 -12
0.46
0 .45
3.8
0.?5
0.18
0 .028
ATTN: Hr. Joseph Ketter
ATTN: Mr. Brent Robinson
AS RECEIVED
rf:r::::::t::*:.:.;.:i:::.:.:.:i.:r:.:.:i:.:::: IIETH@
iii11i:r.:;. iBEsrstslri;::! DETECT I on t Inr T ux I Ts
DRY UEIGIIT
;iiiiliiiiiililii:,:r::Xiliiiill!':ii:ilil METHoo
iiliiilliiil,iljB.q.-*J,,$=ry: ji#DETECTr0NLrr.rrr
20.
13.
3.1
3.1
0.'t0
0. 18
0.66
0.70
4.7
3.4
0.17
o.64
0.63
5.t,
0.35
o.2s
0.039
See Page
rF,/ks
rn9/k9
nrg/kg
nrll/k9
m9/kg
ms/ks
mg/k9
m9/k9
nE,/k9
mg/kg
mg/kg
rr€/k9
rE/kg
f,E/kg
m9/kg
ms/kg
m9/k9
See Page
See Page
4
5
.i:ia-a.l!rii!t:' : : - : & - 4 0,06 7. by tJt.rrl,loisturel represents the toss in reight of the samp[e after oven drying at
103 - 105 deqrees Cetsius.
questions? Contact your Ctient Services Representative
Rachet L. Kreamer at [phone]
09:24:29 D 0002 23 REP 126136 52?739055 70.20 00087095 ASR000
Lrncisie'Labc'elofle!
2425 Ne'x Holland Prke
PO Bor 12125
Ldr:(f, Ie.,a 1 ;6C5 -:i25
71 7';!56-2lt)0 F.\ 7 I l.6qo-r"5a ir .:\.erSe Si!:i: ;^. -tf ';-:,,rn,-.i :'7-rCis a.q,tbO.c,jr.Iroa5
=T
'l
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Page:2ot 1?
Suuni tted:
D i scard:
Reported: 8/ 91966/28/969/ 9/96
CU-4 Disc. Grab Soi L Sanpl,e
Hercutes: Bacchus Pords4DIS SDG#: HBP02-17
CAT[O. AIIALYSI S IIAIiIE
TCL Votatil.es by 8240
3434
3435
3436
3437
3440
4074
4076
I 180
1442
3444
3445
4085
3446
3447
4091
3448
3450
3451
1 181
3452
3453
11A2
345 1
3456
41 08
4107
3457
3449
1183
1 184
3458
4117
3355
6187
62T7
3.
4.
3.
4.
3.
10.
4.
3.
1.
3-
10.
1.
1.
4.
3.
4.
1.
'I .
1.
3.
1.
'1.
'I .
4.
4.
1.
l.
t.
1.
1.
t.
t.
1
Ch Iorornethane
Bromomthane
Vinyt Chtoride
Ch Ioroethane
lilethytene Ch toride
Acetone
Cacbon 0isutfide
1,1 -Dichloroethene
1,1 -Dichtocoethane
Ch I oroform
1.2-Dichtoroethane
2 -Butanone
1, 1, 1 -Tri ch Loroethane
Carbon Tetrachtoridevinyt Acetate
Brornodi ch t orornethane
1,2-Dichtoropropane
ci s - 1, 3-D i ch toroprop€ne
T ri ch Ioroethene
D i bromoch Iorornethane
1, 1,2-Trichtoroethane
Benzene
trans- 1,3-D i ch Ioropropene
Bromoform
4-ilethyt -2-pentanone
2 - flexanone
Tet rach I oroethene
1 ,1 ,?,2-Ierrach Ioroethane
To I uene
Ch I orobenzene
Ethytbenzene
Styrene
Xytene (tota[ )
trans- 1, 2-D i ch loroethene
ci s-1,2-Dichtocoethene
Questions? Contact youc Ctient Services Representative
Rachet L. Kreamer at [phone]
Ldncas!er Laboratofles
2.125 i.1e,ru Ho land P,r:
I-'C Bo\ l2-125
Lnn.;i!er PA I 7605-: l:5
717-656-:j00 F)1 11i-.e. aal1
tR)'d-t
(iI)Lancaster Laboratories
A division of Thermo Analytical lnc.
LLI sample No. ES 2538096Cottected: 6/26/96 at 13:05 by BR
AS RECEIVED
;':*i::1:::r:ji:::riiil:::ii:::r:::::::::::::::::lj: llETH00
niiiiii:ini:,il8f#tlli:i,r.r: oerEcr t or L IitI T un I Ts
us/ks
u9/ks
u9/k9
us/ks
us/ks
ug/ks
uglk9
ug/kg
uglkg
ug/kg
ug/kg
ug/kg
us/k9
uglks
u9/ks
u9/k9
ug/kg
ug/kg
us/kg
uglkg
u9/k9
us/kg
uglkg
ug/kg
u9lk9
us/ks
uglkg
ug/kg
ug/kg
uglkg
uglkg
uglkg
uglks
u9lkg
ug/kg
Account llo: 06716
Hercutes, Incorporated - DE
Envi rofinentat Affai rs
l.li l.rington DE 19894
P.O.
Ret.
Respectfut Iy Sutxni tted
l.tichete llcctarin, 8.A.
Group Leader, GC/llS Votatites
DRY UEIGIIT
1i1i:rl:i:ii:irri::l::i:::::+1:ji:::ir:i::ii:::: l,lETHoo
ii*i:::'.:::#i8#*.H{,fjiiiiii DETEcT I oil L I n r I
22't ?ev j.'0I ,4.
A division of Thermo Analytical lnc.
LLI sample No. ES 2538096
Co[tected: 6/?6/96 at 13:05 by BR
suhritted: 6/28196 Reported: 8/ 9/96
Discard: 9/ 9/96
CU-4 Disc. Grab Soit Sarpte
llercutes: Bacchus Pord
S4DIS SDG#: l{8P02'17
Account llo: 06716
Hercutes, lncorporated ' DE
EnviroflrEntat Affairs
uitmington DE 19894
Page: 3 of 1?
P.0.
Re[.
Respectf ut ty Subri tted
tljcheie I'lcCtarin, B.A.
croup Leader, GC./HS Votatites
(l)La ncaste r Laborato ries
=l
=l
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I,r
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CAT[0. AI{ALYSIS ttA!,{E
TcL votatites by 8240
AS RECEIVED
..:4.:i:L.i:+rr:rln'i:i.rr:ir':i:i:::::::::::::: METI|OD
,:rulili;i*#J$;Xii DETEcT roN LIt'tlT utrrrs
ORY UEIGHT::i:i:rrr::::1::::liilj:::ii:i:iji;*:i:i:r:ii llETHoo
iillillii:':,'::nflEdirEIEii:ii1:i oerrcr t ot{ l- I t{ t r
l,lethytene chtoride Has detected in the method btank at an estimated
concentration of 2. ug/kg. The btank vatue xas not subtracted from the
anatyticaI resutt.
questions? Contact your Ctient
Rachel L. Kreamer
Servi ces Representativeat (717) 656'2100
LSncJSte: LJOcra:o.rF!
2;125 1.1e.! Hoil.nd P,(?
PO Eox i2a25
Lancasie.. 9A 1 i 6a', - ).:i',
7l7-656'21C0 c i^ 1:1 -c|o'24?l
oB
2216 :". 5.ir .c la i
,I
MEMBEFI
2- e,,1-p :,t:? ':: .,a )...t.,.^ -ir'_'Cr''; .laC ab3'e. a' 9r'S
CAT
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(I)Hr,t3rlgt-L*,-0,[?}g.rJ.s 4of 1?
LLI sanple No. ES 2538096Cottected: 6/26/96 at 13:05 by BR
Subnitted: 6128/96 Reported: 8/ 9/96Discard: 9/ 9/96
CU-4 Disc. Grab SoiI Sarpte
Hercutes: Bacchus Pond
S4DIS SDG#: HBP02-17
AI{ALYSIS IIAI,IE
TcL sU846 Semivotatites SoiI
Account !Io: 06716
Hercutes, Incorporated - DE
Envi ronrnentat Af f ai rs
uitmingron DE 19894
AS RECETVED
I,IETHOO
OETECTIOII LII.ITT UI{IIS
DRY IJEIGIIT
iiiillliiii:j,,.,*lila,.:,.i:xillililiiii,i.rii rlETHoD
iiiiiiiiiiiiii8,Efl.t*1F,..:1 oETEcr I 0r L I rtr I T
1.7 .
93.
47.
47-
47.
47.
93.
140.
140.
93.
93.
47.
93.
93.
93.
47.
47.
47.
47.
140.
93.
93.
47.
230.
93.
93.
47.
93.
47.
47.
1 185
3753
1 186
3754
1187
3755
4690
4691
4692
1 188
3757
3758
3759
3746
3747
3760
3748
1 189
1761
4693
376?
1 190
4694
3763
3749
4695
3764
4696
3766
3765
pheno Ibis (2-chtoroethyl) ethec
2-ch IocophenoI
1,3-dichtorobenzene
1,4-dichtorobenzene
1,2-di chtorobenzene
2-methyl.pheno L
2, 2' -oxybi s ( 1 -ch to.opropane)
4 -methytphenot
t{ - ni trosodi -n-propyt ami ne
hexach Ioroethane
ni trobenzene
i sophorone
2-ni trophenoL
2,4-di methyt phenoIbis (2-chtocoethoxy) methane
2,4-di ch I orophenol
1, 2, 4- trichtocobenzene
naph tha t ene
4-chtoroani t ine
hexach Iorobutadi ene
4- ch I oro-3 -methytphenot
2-methytnaph tha I ene
hexach Iorocyc Iopentadi ene
2, 4, 6- t r i ch I orophenol
2,4,5 - tri ch torophenot
2-ch Ioronaphtha I ene
2-ni troani L inedimethyt phthatate
acenaph thyt ene
33.
67.
33.
33.
33.
33.
67.
'100 .
100 .
67.
67.
33.
67.
67.
67.
33.
33.
33.
33.
'100 .
67.
67.
33.
170.
67.
67-
33.
67.
33.
33.
ug/k9
ug/kg
ug/kg
ug/ks
uglkg
ug/kg
u9/k9
u9/ kg
ug/ks
ug/k9
ug/kg
ug/ks
ug/kg
uglkg
us/k9
u9/k9
ug/kg
u9/kg
uglkg
ug/kg
uglkg
ug/kg
uglkg
uglkg
u9/ks
us/k9
ug/kg
u9/ks
ug/kg
uslks
ouestions? contact your CIient
RacheI L. Kreamer
Servi ces Representati veat (7'17) 656-?300
RespectfuI ty Su8ni tted
Chcistine lt. Ratctiff, B.S,
Group Leader, GC/MSLaricdster r-abo.dione!
2,125 Ne,/r' Foiiarrc Pr'l,e
PC 30^ 12.115
Li.cagiel DA 1 7,rr)5-lc: :
717-.556-2j30 Fat t-1t--i;l )r:,3
g'?)
22tL 1e't 5to1!91 ?t J
MEMBER
(iI}La ncaste r Laboratories Page: 5 of 1?
=T
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A division of Thermo Analytical lnc.
LLI sample No. ES 2538096cottected: 6/?6196 at 13:05 by BR P.0.
Rel..
submitted: 6/28/96 Reported: 8/ 9196Discacd: 9/ 9/96
cU-4 Disc. Grab SoiI Sarple
Hercutes: Bacchus Pond
S4DIS SDG#: tl8P02-17
CAT[0. AilALYSIS [Al'rE
TCL sU846 Semivotatites/Soit
4697 3-nitroani Iine1191 acenaphthene3750 2,4'dinitrophenoI1192 4-nitrophenoI4698 dibenzofuran1193 2;4-dinitrototuene4699 2,6-dinitrototuene
3T7O diethyt phthatate
3769 4-chlorophenyL phenyl. ether376€ fluorene4700 4-nitroani tine
4701 4,6-dinitro'2-methYtPhenot3Tn il-nitrosodiphenytamine3773 4-brorrcphenyt phenyl ether
3Tf4 hexachIorobenzene1194 pentachtorophenoI3775 phenanthrene
3776 anthracene47O? carbazote3TTl di'n'butyt phthatate3Tl8 ftuoranthene1195 pyrene3780 butyt benzyt phthatate
3783 3,3'-dichtorobenzidine3781 benzo (a) anthracene3784 bis (2-ethythexyt) Phthatate3782 chrysene3785 di-n-octyt Phthatate3786 benzo (b) fluoranthene3787 benzo (k) fluoranthene3788 benzo (a) pyrene
3789 indeno (1,2,3'cd) PYrene3790 dibenz (a,h) anthracene3791 benzo (ghi) PerYtene
Account llo: 06716
Hercutes, Incorporated - 0E
EnviroffEntaI Affairs
iJitminqton DE 19894
AS RECEIVED
IIETHOO
iiriiiiili.:.i,+:!f,E$lsr5:llliii DETEcT I otl L I !t I T ull I TS
DRY tJE I GHI
!jti::ii1:ti.,1.nii!tli:,:ia!:.::;..i.:;:l;,.i1; ttlETHOo
tijr,iiiiiiii$Ftr$lr#j* DETECT r 0N L r H r T
91.
47.
?30.
230.
47.
93.
93.
93.
93.
47.
140.
230.
93.
'140.
140.
?30.
47.
47.
l+7 .
47.
47.
93.
93.
190.
47.
93.
47.
93.
93.
190.
93.
93.
93.
93-
67-
53.
170.
170.
33-
67.
67-
67.
67.
33-
100 .
170.
67.
100.
100.
'170 .
33-
33.
33.J 33.
33-
67.
67.
130.
33.
67.
33.
67.
67-
130 .ot-, 67.
67.
6t-
us/k9
ug/k9
u9/kg
us/ks
ug/k9
uglkg
us/kg
uglkg
ug/kg
uglkg
us/kg
uglkg
uglkg
uglk9
u9/k9
uglkg
uglkg
ug/kg
uglk9
uglkg
us/ks
uglkg
us/kg
us/kg
uglkg
us/ks
uslkg
ug/kg
ug/kg
uglkg
uglkg
uglkg
uglk9
ug/ks
Questions? Contact your Ctient
Rachet L. Kreamer
Servi ces Representativeat (717) 656'2300
l_Jn(JSIe. l-attorn!3fl ?S
2425 lle'd Hoildno Prke
PO Box 12125
Ldncasier. PA l;6i5-l 125
;17-656-2lCC Fax r' 17 -615-2€,31
Respectf uI ty Subri tted
christine H. Ratciiff, B.S.
croup Leader, GC/lls
:ee re'/er!e 5rC€'l: lro -jn3:roa i :.-ac s Jnd dc:'':. a::c.5 22ld ?e! 510r '9^
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&&&
(iI}Lancaster Laboratories
I"ABORATORY CHRONICTE
Page: 6 of 1?A division of Thermo Analytical tnc.
LLI sample No. ES 2538096cottected: 06/?6/96 at 13:05 by BR
SuEnitted: 06128/96
Account llo: 06716
Hercutes, Incorporated - DE
EnvirormentaI Affairs
Uitminston DE 19894
CU-4 Disc. Grab Soi I Sanpl.e
Hercutes: Sacchus PondS40lS SDG#: HBP02-17
CATr{o A!{ALYSIS NAilE
4593 TCL Votatites by 8240
1625 ThatLiun
1643 Al,uminun
1644 Antirbny1646 Bariun1647 Beryl.tiun
1649 Cadmiun
1651 chromiun
1653 copper
1654 Iron
1655 Lead1658 tlanganese1661 ll i cket
1666 Si tver
1672 Zinc
570E SL, SU845 ICP Digest
6955 Arsenic TR6936 Sel.eniusn TR
0159 Mercury
5711 SU SU845 Hg Digest
0381 BilA soiI Extraction
4688 TCL SU846 Semivol.atites Soit
4689 TCL SU846 Semivotatites/SoiI
0111 lloisture
l,'tETH00
su-845 82408
su-846 5010A
srJ-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
srJ-846 6010A
su-846 6010A
sr,-846 6010A
srl-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 60'l0A
su-846 30504
srJ-846 6010A
su-846 5010A
su-816 7471A
St,-846 7471A Modified
su-846 3550A
su-846 82708
su-846 82708
EPA 160.3 (modified)
AIIALYS I S
TRIAL DATE AXD TII.IE
1 07/03/96 1154
AIIALYST
Rick S. Rodgers
Jotene i{. Schietds
Jotene lil. SchieIds
Jotene il. Schietds
Jotene l,l. Schietds
Jolene l,l. Schields
Jotene l,t- Schiel.ds
Jotene M. SchieLds
Jotene l,l. Schietds
Jotene !1. Schietds
Jotene I',l. Schietds
Jotene l,l. Schietds
Jotene ll. Schietds
Jotene ll. Schietds
Nina C. llatter
Desi R. Carozza
Desi R. carozza
Jotene ll. Schietds
Nina C. Hatter
lletti S. llarkaryan
Frances A. De,mrest
sherry Lynn oevtin
Joseph I't. Garbler
Joseph !,l. Ganrbter
[eetay B. Hehta
1
1
1
1
1
1
1
1
1
1
1
1
1
1
'I
2
07/13/96 1903
07/13/96 1e03
07/13/96 1903
07/13/96 1903
07/13/96 1903
07/13t96 1903
07t13/96 1903
07/13/96 1903
07/13/96 1903
07/13t96 1903
07/13/96 1903
07/13/96 1903
07/13/96 1903
08/08/96 1353
07/02/96 1934
07/31t96 1940
07/13/96 1903
07/17/96 1011
07/03/96 1654
07/0?/96 1506
07/01/96 1930
07/05/96 2011
07/05/96 2011
07/02/e6 1520
Lanca5!er Laboratorre:
2425 i.le',r Hoiianc Prxe
PC Bcr i2-i25
Lanc.rr:et PA'.1 445- i.i)a
711-b55-1100 Fa:< 11t'-,:>,, )c?.'9r^ ?.#
MEMEtER
5ee .e,,e.s-" I :e _ir e(cr,rndt r^ c't;-cot: ani il)t.e..,,;lrorr5 -r2'a i,-i iC
QUALITY CONTROL REPORT I
"i
Group [o. 52289
llercutes, Incorporated - 0E
Page: 7 ol 12
LCS LII,IITSLOU 1I I GH
*,I
,l
:l
saflpte
HDL
Samp t e
UII I TS
DUP I,IS LCS LCSRPO IIS I{SD RPO LCS OUP RPD
(|)Lru,n#:Igt,,Lgb-o,[?lP#*
LLr saurple No. 2538096
CU-4 Disc. Grab Soit Sarpte
Hercutes: Bacchus Pond
4593 TcL Votatites by 8240
3434 ChIorornethane
2.us/ks
3435 BrooEnrethane3. us/ks
3436 Vinyt Chtoridez- ug/kg
3437 Ch(oroethane3. ug/kg
3440 ilethytene Chloridez- uglks
4074 Acetone
7 - us/kg
4075 Carbon Disutfide3. us/kg
1160 1,1 -Dichtoroethene?. ug/kg
344? 1,1-Dichtoroethane1. ug/kg
5444 Chtot-oform
1 - us/kg
3445 1,2-Dichtoroethane2- ug/kg
4085 2-Butanone7. uglkg
34t 6 1,1, 1-Trichtoroethane1. w/ks3447 carbon Tetrachtoride1. ug/kg
4091 vinyl Acetate
3.uglk9
3448 Bromodichtororpthane2. uS/kg
3450 1,2'DichIoroproPane3. uslkg
3454 cis-1,3-DichtocoProPene1. uglkg
1181 Trichloroethene1. us/kg
3452 Dibromochtoromethane1. ug/ks
3453 1, 1,2-Trichioroethane?. us/ks
1 182 Benzene1. u9/k9
3451 trans-1,3-0ichtoroproPene
1 ' ug/ks
Batch: E961831A8
l'1. D.
ll.D .
T.D.
|t.D.
2. J us/kg
lt.D.
N .D.
lt.D .
It.D.
[.0.
|l.D .
l't.0.
ll.D .
H. D.
H.D.
N.D.
lt ,0.
[.0.
|1. D.
N.D.
It.D.
[.D.
r{ .0,
90 87
99 98
104 100
91 101
102 99
88 78
102 100
107 101
99 95
96 95
93 92
102 U
106 105
104 100
99 61
92 90
98 96
96 98
109 107
90 87
94 92
98 96
93 9?
395
295
5 102
10 89
396
11 88
2 103
6 105
495
?95
191
20 95
I 105
3 103
20 105
?95
0 101
2 10?
? 111
396
298
2 'lo4
198
1 ?72
'l 241
1 250
'10 ?54
1 221
19 150
24 188
1 ?33
59 155
51 138
49 155
?2 167
52 162
70 140
19 190
35 155
1 ?Oe
1 2?6
71 157
53 149
5? 150
37 151
17 183
I
I
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MEMBER
%@ril
Lan(J!ter Labor;loret
2425 Ne'r'/ Hoiland Prk€
PC 3ox 12425
rancasi4( PA I 7605-1r25
7l7-656-2 300 F tx'1 11 -556-2i81,
I
Qe.,5'0' c6 di I
I
22 !a
LCS
DUP
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(iI}La ncaste r Laboratories
QUALITY CONTROL REPORT
Page: 8 of 12A division of Thermo Analytical lnc.
LLr sample No. 2538096
C1,t-4 Disc. Grab Soi I Sanpte
llercules: Bacchus Pond
Group llo. 522759
Hercutes, lncorporated - DE
Sarpte SanpteII{DL UII I TS
3456 Bromoform1. ug/kg
4108 4-ltethyt -2-pentanone
3. ug/kg
4107 2'Hexanone3. ug/kg
3457 Tetrachtoroethene1. ug/ks
3449 1, 1,2,2-TetrachIoroethane1. uglkg
1183 Totuene1. us/kg
1'184 Chtorobenzene1. uglkg
3458 Ethyibenzene1. uglkg
41 17 Styrene1. ug/ks
3355 xytene (totat)
1. u9/k9
6187 trans-1,2-0ichtoroethene2- us/kg62V cls-1,2'Dichtoroethene
BLAIIK
x-D.
H.D ,
It.D .
t{.0 .
lr .0.
ll.D .
[.0.
[ .0.
N.D .
I.D.
[.D.
[.0 .
Batch:961845708003
r,l.D.
Batch:961845708003
[.0 .
Batch:961845708001
[ .0.
Batch:961845708003
It.D .
Eatch: 961845708003[.D.
Batch: 961845708001
I,l.D.
Batch:961845708001
N.D.
Batch:951845708003
[.D.
Eatch: 9618457080037.2 J m9/k9
Batch: 961845708003
N.0.
Batch:961845708001
It.0.
Batch: 961845708003
N.D.
Eatch:961845708003
N.D .
DUPRPo ilS I'|SD
88 83
98 91
101 90
115 1 t0
100 9t1
105 103
96 96
107 104
99 92
105 103
104 98
105 101
(1) 93 89
21 2027 1645 (Z)
(1) 92 95
9 105 97
0(1) 96 91
0 (1) 93 88
0 (1 ) 128 131
0 (1) 119 109
13 2452 2139 (2)
0 (1) 96 90
11 116 109
0 (1) 97 91
(1) 102 97
LCS LIHITS
LOU HIGH
45 169
50 124
5? 140
Ut 148
46 157
47 150
37 160
37 162
74 136
30 ?00
54 156
54 156
50 150
50 165
21 299
70 131
?3 1Tl
26 174
54 141
57 145
61 142
53 14?
69 135
55 146
50 1t+7
HSRPD LCS
693
790
12 91
4 115
797
1 101
097
3 ]oE
7 101
2 106
6 101
4 10?
696
979
279
7 100
598
799
1 102
6 102
489
794
594
696
798
LCS
RPO
?.
1625 Thattiun
14.
1643 Atuminun
uglk9
mg/ks
9.0 ng/kg
1644 Antimony?.2 mg/kg
1646 BariunZ.? rglkg
1647 Beryttitrn0.074 mg/kg
1649 Cadmiun0.13 mg/kg
165'l Chromiuun0.47 ms/ks
1653 Copper0.50 ms/ks
1654 lron3.1, m9.i k9
1655 Lead2.4 tr€/kg
1658 llanganese0.12 m9/k9
1661 ilicke(0.46 m9lks
1666 Si tver
0 .45 trt9/kg
(l) the resutt for one or(2) The background resu(t
both determinations uas Iess than five times the LOa.
rras more than four times the spike added.
LarraaSler t-acoratofl e5
2425 Nevt rci dnc Prit
?O 0o^ l2:::
L,inads:er il !'6:5-:42!
7l7-556'2301) ?ar .'1:--t't ).i 2216 riev s,'7cr a. dt#
I
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76
7i
76
76
74
71
62
90
n
80
78
87
76
41
75
77
78
7S
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Page: 9 of
Group ilo. 5227j9
Hercutes, lncorporated - DE
Sarpte
}ID L
1672 zin.c
Sanpt e
UI{ I TS
DUP IiIS LCS LCS
RPD IiIS I,ISD RPO LCS DUP RPO
LCS L II.II TSLorJ fl I GH
54 149
49 149
52 149
26 157
5 112
1? 1s8
23 134
1 172
?o 1?4
3? 129
46 123
56 166
5 152
1 230
40 113
35 180
21 196
29 182
32 119
JJ IOq
39 135
44 142
21 133
3.8 trE/ks
6935 Arsenic TR0.25 trtg/kg
6936 Seteniun TR
0- 18 m9/ks
0159 Mercury0.028 trt9/kg
0 (1) 102
0 (1) 91
0 (1) 92
0 (1) 92
107
9?
94
9?
3
0
1
0
13
11
12
5
5
6
15
11
14
13
'10
7
10
9
17
11
13
6
5
95
93
87
79
4688 TcL SU846 Semivotatiles SoiI Batch: 96183St8026
1185 phenol33. u9lk9
3753 bis (2-chtoroethyt) ether67. uglks
1186 2-chtorophenot33. us/ks
3754 1,3-dichtocobenzene33- ug/kg
1187 1,4-dichtorobenzene33. ug/ks
3755'1,2-dichtorobenzene33. uglkg
4690 2-rcthytphenot67. u9/k9
4691 2,2'-oxybis (1'chtoropcopane)100. u9lk9
4692 4-nEthytphenot100. ug/ks
1 188 N-ni trosodi -n'p.opytamine67. uslks
3757 hexachlocoethane67. u9lk9
3758 ni trobenzene33. us/kg
3759 isophocone
67.u9/ k9
3746 2'ni trophenol.67. uglkg
5747 2,4'dinethytphenot67. ug/ks
3760 bis (2-chtoroethoxy) rnethane33. uglkg
3748 2,4'dichtorophenot33. uglkg
1 189 1,2,4- tr i ch Iorobenzene33. us/kg
3761 naphthatene
33.
LancJsie, LiSoratcr9!:
2425 Ne,! Holland Pr\.
PC Bo\ l2ii25
l-3.(drie,. PA i 76J5.:325
?r 7-655-2100 Fdv ;l;-6-<o-203 l
72 82
758/-
69 78
75 79
74 78
72 77
69 80
6? 70
8/ 97
7484
75 83
T7 83
83 92
74 82
48 57
73 81
71 81
T7 8?
T3n
(1) The resutt for one oc both determinations Has tess than five times the L00-
lPa +e.sa::,.1e toi 9{:
QUALITY CONTROL REPORT
(I)hgn:r:lglLgng,IrlP#o
LLI Saruple No. 2538096
cU-4 0isc. Grab Soit Sarpte
Hercutes: Bacchus Pond
ELAIIK
Eatch:9621357080050.86 J m€/ks
satch:961845708003
II.D.
Batch: 961845708003
[.D.Batch: 961845711002
[.D.
:^ I !icoF,.jrai,oa<
g?_
?e, 5.'. .J ?a J
DUP I,IS LCS LCS LCSRPO IiIS HSD RPD LCS DUP RPO LOU
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(I)Lancaster Laboratories Page: 10 of 12A division of Thermo Analytical lnc.
Sarpte Saflple}tOL UII I IS
4593 4-chloroani Iine100. us/ks
3762 hexachtorobutadiene67. us/kg
1 190 4-chtoro-3-methytphenol.67. u9/k9
4694 ?-nethytnaphthatene33. ug/ks3763 hexachIorocyctopentadiene
us/k93749 2,4,6- trichtorophenol67. ug/kg
4695 2,4,5- ttichtocophenot67. ug/kg
3764 ?- chLoronaphthatene13. ug/kg
4696 2-ni troani t ine67. us/ks
3766 dimethyt phthatate33. ug/kg
3765 acenaphthytene33. us/ks
4697 3-nitroanitine67. uslks
1 191 acenaphthene33. uS/kS
3750 2,4-dini trophenoI170. ug/ks
1192 4-nitrophenot170. ug/kg
4698 dibenzofuran31. ug/ks
1 193 2,4-dinitrototuene67. uslkg
4699 ?,6'dinitrototuene67. uglks320 di ethyt phthatate67. u9lk9
3759 4-chtorophenyI pheny( ether
67 - uglkg
3768 ftuorene33. uglkg
4700 4-nitroani tine
'100 . us/ks
4701 4,6-di ni tro' 2'methytphenot170. us/kg
LLI sample No. 2538096
CU-4 Disc. Grab SoiI Sarpte
llercutes: Bacchus Pond
Group llo. 522739
Hercutes, Incorporated - 0E
14 15
80 87
75 86
74 8?
17 16
81 90
80 89
79 85
TZ 78
79 87
75 81
36 40
71 78
59 65
T3 77
74 80
82 89
81 89
79 88
79 87
74 80
59 62
66 7?
BLAIIK
[.D.
it.D.
It.D,
it.D .
il.D .
il.0.
[.0 .
[.0 .
I.D .
It.D.
[.D.
5
9
13
10
'11
10
6
8
10
8
43
81
82
78
62
82
82
79
75
80
77
LII,IITS
flIGlt
17 '.116
24 116
2? 147
28 123
1 100
37 144
39 151
60 118
53 143
1 112
33 145
7 143
47 145
1 191
1 132
?8 131
39 139
50 158
1 114
25 158
59 121
38 12?
t 181
4689 TcL SU845 Semivotatites/SoiI Batch: 96185518026
[ .0.
I.D.
ti.D.
il.0.
[.0.
[.0.
N.D.
t't -0 .
t{.D .
il .0.
[.0.
lt.D.
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Lanca5ter Laocratofies
2425 Ne.r Hoilano Fr(e
PC tscx i2125
Lancasler PA I 7605-:425
717-656-2100 Fax ;17-.i5o-2aa
QUALITY CONTROL REPORT
MEMBER
5ee :e'/erse s,c? :ai 3.(c ind:ron ol j /- oors 6ad rbbrel.,iaitcns ?2ld 2"\' 5i0l
4)e,ae.:^ tflE
(iI)Lancaster Laboratories
QUALITY CONTROL REPORT
Page: 11 of
'11
1l
rI
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A division of Thermo Analytical lnc.
Sanpte Sampte}IDL UI{ITS
57?"2 ll'ni trosodiphenytamine
6t-w/ks37R 4-bromophenyl phenyt ether'100. ug/ks
3774 hexachtorobenzene'100. uglkg
1194 pentachIorophenot170. ur,/kg3TR phenanthrene
53. uglkg
3776 anthracene33- ug/kg
4702 carbazote33. uslks3Tn di-n-butyt phthatate
33. uglks3 78 fluoranthene33. uglkg
1195 pyrene
67. uslkg
3780 butyt benzyt phthatate
67. ug/ks
5783 3,3r -dichtorobenzidine
uslk9
3781 benzo (a) anthracene53. uglkg
3784 bis (2-ethythexyt) Phthalate67. ug/ks
5782 chrysene33. uglkg
3785 di-n-octyt phthatate
67. us/kgf786 benzo (b) ftuocanthene67. ug/kg
3787 benzo (k) ftuoranthene130. ug/kg
3788 benzo (a) pyrene67. uslks
3789 indeno (1,2,1-cd) Pyrene67. ug/kg
3790 dibenz (a,h) anthracene67. uglkg
3791 benzo (9hi) PerYtene67. ug/kg
0111 l,loisture0.06 % by ur.
ELAIIK
[.0.
u.o .
lt.D.
lil.D .
ll.D .
il .D.
[.D .
it.D.
r,l.D.
l{.0 .
!l.D .
N.D .
N.D.
t{.0 .
il.0.
il.0.
ll.D.
l{.0.
[.0 .
|t.D.
l{.0.
ll.D .
Batch : 961 8403'.I 6820003A
LLI sanple No. 2538096
CU-4 0isc. crab Soit Sarnpte
Hercutes: Bacchus Pond
Group l,lo. 5227j9
Hercutes, Incorporated ' DE
748/.
81 92
83 94
74 76
75 83
74 81
74 79
80 90
T3 80
83 9?
86 97
55 58
n83
93 103
E2 89
81 9?
T3 80
T7 85
74 8r
8? 8e
83 91
79 86
ouP ils Lcs LcsRPD IIS iISD RPO LCS DUP RPD
lcs LIlillTsTSJ HIGH
38 147
53 127
1 152
14 176
,4 120
27 133
35 133
1 I18
26 137
5? 115
1 152
1 ?62
33 14s
8 158
17 168
4 146
?4 159
11 163
17 163
1 171
1 227
1 Z',lg
100 101
12
13
13
?
10
9
7
11
9
10
1Z
5
9
8
13
10
10
10
73
80
8?
63
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78
86
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95
66
80
103
85
103
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86
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MEMElEFlreiiE
Lancaster LabDr.lrories
2425 lJe,r'/ Holland Prke
PO Box 12d25
LJrtJster. tA I 7505-id25
71 ;-655-2100 F,rx 7ll-5-<o-l6El
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a: ; -t:r1 ibCre.,,rd'r,tn<1216 Qev 5;0L'45
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LLI sample No. 2538096
CU-4 Disc. Grab Soit Sarpte
Hercutes: Bacchus Pord
Group l{o. 522759
Hercutes, lncorporated - 0E
Page: 12 ol
SURROGATE LII.IITSLOU HIGH
70 1?1
81
74
24 11325 12119 12?
?3 12030 11518 137
(I)La ncaste r Laboratories
A division of Thermo Analytical inc.
SURROGATE SUIII.IARY
TRIAL ID SURROGATE RECOVERY Z
4593 TCL Votatites by 8240 d4-1,2-DcA 93d8-totuene 100BFB 92
4688 TCL SU846 Seflivol.atites SoiL Phenot-d6 812-Fl.phenot 74?,4,6-rBP 89
4689 TCL SU846 Seilivo(atites/Soi| tlitrobz-d5 95Z-Fbiphnyt 84Tphenytdl4 82
117
1?1
Lan(a5ie. LiboratcrLes
2425 Ne', Hoildnc Prre
PC 9or 12,125
!irc3si3.. oA l 16i5'2.125'i 11. 456- 23OA i ax j 11 -6>o - 26?,
QUALITY CONTROL REPORT
iee revor'r: j::::e i9'1,2;c1'2' ''-.a :. i'1 ZOI:= ,.a:.O^'S
oB.
2:'5 ?e, 5/Ol :6 ?t J
Lancaster Laboratories
A Thermo Analytical Laboratory I
I253808 l
by BR
Page:
DRY UE ! GilT
LLI Samp1e No. ES
col tected: 6/27/96 at 09:05
Suhnitted: 6/28/96 Repocted: 8/ 6/96Discard: 9/ 6196
CU-4 JtJo Hatrix Spike Gcab Soit Sampte
Hercules: Bacchus Pond
S4JU0 SDG#: HgP02'0/+MS
i Account llo: 06716
I Hercul.es, Incorpocated - DE
i Envi rorrnental. Afra i rs
i Ui Imingron DE '19894
I
P.0.
Rel..
ll
CAT
N0.AIIALYSIS UAIitE
TCL vo(atites by 8240
Thattiun
Atuminum
Anr i fitony
Bar i um
Beryttiun
Cadrni un
Chromi m
Copper
I ron
Laad
I'langanese
N i cket
S i Iver
Zinc
Arsenic TR
Sel.eniun TR
!lercury
ICL Pesticides in Sol.ids
TcL 59846 Semivotati tes Soi L
TCL Su846 Semivotati Les/Soi I
Moisture
AS RECEIVED
:.:::.rt*:i::i*ii;:t::::'-:::.:.::t:::.:i:1t-::.:..-:l:t METHOD
'.'"'r'rii'i:[E5utrS.,,,,,.::., 0ETEI-l' I 0N t Ill I r ull I Ts
See Page1t,. mg/kg3.8 ,rg/kg2.2 mg/kg2.2 mg/kg0.tJfi m9/ks0.]i m9/k90.46 m9/kg0.49 ng/<9i.l mg/ (g
2./. fl_q/kg,.12 m9/i9C.45 ns/ksC.4/. mg/ig0.i9 m-ol<g
0 .25 ng,'<g
0. i8 ms/<q
0.' 28 rng/<9
See Page
See Page
See 2age
0.06 li by Ht.
IIETHOO
OETECTIOII LIIIIT
18.
11.
)d
2.8
0. 094
o .17
0 .60
0.64
1.3
J. I
0. 15
0.59
0.57
0. 51
0.32
0.23
0. 037
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16?5
1613
1614
1616
1617
1649
165 1
'16s3
lO>.r
1655
1658
ioo r
1666
1672
6935
6936
01 591a)<
4688
4689
01 18
3
4
5
1 COPY IO
1 COPY TO
Hercutes, IncorporatedERH Rocky Mountain
ouestions? Contact your Ctient
RacheI L. Krearner
14:06:57 D 0002 23 REP
310 25.00 00137200 AsR000
ATTN: Hr. Joseph Kel',er
ATTH: I'tr- Brent Robinson
Services Representat iveat [phone]
126436 522739
Respectfut Iy Submi tted
RanDna V. LayilEn, Group Leader
ICP i'leta Is/Leachates
MEMBEFI
,AKMI
Lancaster Laboratories
2425 New Holland Prke
PO Box 12425
Lancaster PA 1'l 605'2425
717-656'23C0 F;x 717'655-253t
at
2216 Rer ,Orrorn, ?ai5ee reverie i,ce icr e\oiaaa: c. f: :;aooi5 an! abf,aevralrons
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?of 14
Sutrnitted: 6/28/960iscard: 9/ 6196
CU-4 JUD ilatrix Spike Grab Soit
Hercutes: Bacchus Pond
54JUD SDG#: HBP02-04t!S
AIIALYS t S IIAI'IE
TCL Votatites by 8240
8/ 6/96
Samp I e
Account llo: 06716
HercuIes, Incorporated - DE
Envi ronnuntaI Affa i rs
Ui [mington DE 1989/.
RE CE I VED
::::: I'|ETHoo
'.., OETECTICN LIHIT UNIIS
DRY UE I GHT
:l:::li:l::.4.!;:.:::::.: ::tt::: :: :::: ::::::..:::jj:::::r::::: jjj.6r crr I I a
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,21 -21..
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,:,',9S;,,,
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,,,,19-
,, .20 "
.:21 -:41
u9/ <9
!q/"9
u.l/ i9
u9/ <g
u /k9
ug/ <9
u9/ <9
u9/ k9
ug/ <9
\)g/ <g
!9/'<g
re/ <9
ug,/l(9
rr9l <g
ug/ <9
ugl i9
u9/ <s
r9/ <9
ug/ t9
u9l19
ug/ <g
ug/ ks
u9/ <3
u9/ <9
ugl(9
u9/ <g
u9i <.9
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tilET H00
DETECT ION
3.
4.
3.
1.
1
9.
4.
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l.
1.
3.
9.
1.
4.
1
4.
1.
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1.
3.
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1.
1.
1,
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3435
3t 36
3437
3440
4074
4076
1 180
344?
34t-4
3445
4085
3416
3447
4091
3t 18
34 50
3451
1 181
3452
3153
1 182
34 51
3156
4103
4107
3457
34t 9
1 183
1184
3458t 117
33s5
6',I87
6277
Ch Ionomethane
Eromomethane
VinyL Chl.oride
ch Ioroethane
l'tethytene Chtoride
Acetone
Carbon 0isutfide'l,l-0ichtoroethene
1,1 -Dichtoroethane
Ch Ioroform
1,2-0ichtoroethane
2 - Butanone
'1, 1, 1 -Tri chtoroethane
Carbon TetrachtorideVinyl Acetate
Bromodi ch I ocomethane
1,2-Dichtoropropane
ci s - 1,3 -D i ch !.oropropene
Tri ch I oroethene
Dibromochtoromethane
'1 , 1 .2-Trich toroethane
Benzene
tnans- 1,3-D i ch Iocopropene
B romofornr
4 -llethyt -2 -pentanone
2 - tlexanone
T etrach I ocoethene
1,1 ,2,2 -Tetrach Ioroethane
To t uene
ch Iorobenzene
E thytbenzene
S tyrene
Xytene (totat )
trans-1, 2-D i ch Ioroethene
ci s- 1, 2-Di chtoroethene
ouestions? Contact your Ct ient
Rachet L. Kreamer
Services Representative
at ( 7r 7) 656-2300
j rli:ll1i1:::ili li:,j;?Z;:rt:,:.::::::. :, ......:Z>:.:.t
26,
L). -
.:)':t'::::.:' 26;
{t2-
24.
Respecrfut l.y Submi tted
Hichele McCLarin, B.A.
croup l-eader, GC/|'1S Volat i Les
'!.
MEMBER
TXEm
Lancaster Ldboratofles
2425 New Holland Prke
PC Box 12425
Lancaster PA 17605-2d2',
717-656-2300 Fax't i: -z:,:,orror$ dtJ
(I}Lancaster Laboratories
A Thermo Analytical Laboratory
LLI sample No. ES 2538081Cottected: 6/?7/96 at 09:05 by BR
(,ei i.e':e .je ic' :,1.-"'a'.-a' oi ly-boi5d.o acbrevrdtrons
(l)Lancaste r Laboratories
A Thermo Analytical Laboratory
Page: 3 ol 14
DRY UEIGHT
i';ij:!:rli,itiiti:ii!:i:ii.i:!,i:.!iiaiir.:ii:!:i:i; ilETHOD
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LLI sampJ-e No. ES 253E081cottected: 6/?7/96 at 09:05 by BR
suBtritred: 6/28/96 Reported: 8/ 6/960iscard: 9/ 6/96
Account No: 05716
Hercutes, Incorporated - DE
Envi ronmentai Affai rs
Uitmington 9E 19894
CU-4 JUo Mat.ix Spike Grab SoiI Sampte
Hercutes: Eacchus Pond
54JUD S0G#: HBP02-04ils
CATIIO. AIIALYSIS UAIIE
IcL Pesticides in Sotids
1981 Atpha BHC
1982 Eera BHC1983 Det ta BHC1213 Ganma BHC ' Lindane1219 HeptachIor12?0 Al.drin'1984 Heptachtor- Epoxide'1989 Endosutfan i
1222 0ietdrin1985 D0E1?23 Endr- in1990 Endosutfan ! I1986 DoD1991 Endosutfan sutfate1221 oDT3017 Endrin Ketone1859 Methoxychtor3025 ALpha chtordane3026 6amna Ch Iordane1988 Toxaphene
1992 Endrin Atdehyde1995 PcB-10161994 PC8-12211995 PCB-1?321996 PCB-12421997 PCB-12181998 PCB-12541999 PCB-1260
AS RECEIVED
I.IET HOD
iii:riiiitl:::j:irtf:SutiF,:ii:i DEIEcT I 0r'l L tr'! I T uN I Ts
6.
9.
1C.
5.
4C.
':.
1 ,000 .'10 .
30.
30.
50.
50.
/+C .ic.i0.
rigl k9
us/ lg
u9l (9
ug/ <g
u9l kg
ug/ <g
us/k9
us/ kq
ugl (g
ug/ kg
ug/ i(S
ugl (g
ug/<9
u9/ <9
u9/<g
uslkg
ug/<g
u9/<9!g/ <g
!q/ <g
u9lks
usl kg
ug/ <9
ugl ig
ugl <9
u9/ <g
Ng/\9
':9/ <9
Ouestions? Contact youc Ctient Services Representative
RacheL L. Kreamer at [phone]
istr'fi
Lan(aster Laboratones
2425 New Holland Prke
PO Box 12425
Lrncasrer PA I 7605-2,125
7l7'556'2100 F;x 7f i -6\6')531
T
,artrr$ d3 I'
Respectfu( [y Submitted
..jenifec E. Hess, B.S.
Group !eader Pesti cicies/PCBs
5ee revgl5g 516E'_',1;;..itlon ct ;.-cols and aooia/,airons 2216
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(D La ncaste r Labo ratories Page: 4 of 11A Thermo Analytical Laboratory
LLI sample No. ES 2538081Cottected: 6/27/96 at 09:05 by BR i Account tlo: 06716i Hercutes, tncorporated - DE
I Envi rormentat Afiairs
I Uitmington DE 19894
AS RECEIVED
HETH00
DETECT!O}I LIMIT U}IITS
P.0.
Re[.Subnitred: 6/?8/96 Reported: B/ 6/96Discard: 9/ 6/96
Cu-4 JUD ilatrix Spike Grab SoiI SampLe
Hercutes: Eacchus Pond
S4JUD SDG#: HgP02-04HS
CAT}IO. A',IALYSIS IIAME
TCL SU846 Semivotatites Soit
1 185 phenol3753 bis (2-chtoroethyt) ether
1 185 2-ch t orophenoI3754 1,J-dichl.orobenzene1187 1,4-dichtorobenzene
3755'1,2-dichtorobenzene4690 2-methytphenolL691 2,2'-oxybis ('1-chioropropane)1692 4-rethytphenoL1188 I-nitrosodi-n-propytamine3757 hexachtoroethane3758 ni tcobenzene3759 isophorone
37t 6 2-ni trophenot3747 2,4-dimethytphenoI3760 bis (2-chtoroethoxy) methane37t+8 2,4-dichIorophenoI'1189 1,2,4-trichtorobenzene3761 naphthalene4693 4-chtoroani t ine3762 hexachtor-obutadiene
1 190 4-ch Ioro-3-rnethytphenot4691 2-methytnaphrhatene3763 hexachIorocycIopentadiene3749 2,4,6-trichtorophenoI4695 2,4,5-trichl.orophenoI3761, 2-chtoronaphthatene4696 2-ni troani t i ne3766 dimethyt phrhatate3765 acenaphthytene
ouestrons? Contact your Ctrent
RacheI L. Kreamer
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100.
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DRY 9EIGHT
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u9/ k9
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Lancaster Labo(atones
2425 New Holland Prke
PO Box 12425
Lancastel PA I 7605-2425
t- 1l -656-2340 Fax 7 l7 ir55 i i6
Respectfut ly submi rted
Ch.istine l'.l. Ratcl.jff ,
6.oup !eader, cC/t'1S
See -e;erse:rce'c,r e!olao:: ar t' 5ynrbois,tod abbreyattons
B.S.
,]}
22 16 Re,. ,Orr'r$ lai
(I)La ncaster Laborato ries
DRY UEIGHT
j:r:r::ii:,r:!:::::*ijr:ili:::::i:::::i:,::: METHOo
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87.
87.
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A Thermo Analytical Laboratory
LLr sample No. Es 2538081Cottected: 6/27/96 at 09:05 by BR
Suboritted: 6/?8/96 Reported: 8/ 6/96Discard: 9/ 6/96
CU-4 JUD lilatrix Spike 6rab SoiL Samp[e
tlercutes: Bacchus Pond
s4JU0 SOG#: HBP02-041,1s
CAT}IO. AIIALYSIS }IAI.IE
ICL SU846 Semivotati Ies/Soi I
4697 3-ni troani t ine
1 191 acenaphthene3750 2,4-dinitrophenol1192 4-nitrophenot4698 dibenzofuran1193 2,(-dinitrototuene
t 699 2,6-dini trotoIuene3770 diethyt phthatare3769 4-chtorophenyI phenyI ether3768 ftuorene4700 4-ni troani t ine4701 4,6-dini tro-2-methyLphenoL3nZ N-ni trosodiphenytarnine3773 4-bromophenyt phenyI ether3774 hexachtorobenzene1194 pentachtorophenot3775 phenanthrene3776 anthracene470? carbazote3777 di -n-butyt phthatate3 78 ftuoranthene
1 195 pyrene3780 butyl benzyl phthatate
3783 3.3' -dichtorobenzidine3781 benzo (a) anthracene3784 bis (2-ethythexyt) phthatate
3782 chrysene3785 di -n-octyt phthaIare3735 benzo (b) f(uoranthene3787 benzo (k) ftuoranthene3788 benzo (a) pyrene3739 indeno (1,2,3-cd) pyrene
3790 dibenz (a,h) anrhracene3791 benzo (ghi) perytene
AS RECE IVED
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130 .
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67.i3.
67.
67.
110.
67.
67.
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u9/kg
u9/k9
ug/k9
u9/ks
ugl kg
ug/ (g
u9/ kg
u9/kg
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u9/ kg
ug/k9
ug/k9
uSl;(9
u9/ kg
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ug/ kg
u9/ks
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ug/ <9
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RacheI L- Kreaflter
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Chris!rne l!. Ratctiff ,
G.oup Leader, GC,/,'!S
See reverse trCe :or etpldr 3iron cl ;ymbois and abore./rattonsE6m
Lancaster Laboratofle5
2425 New Holldnd Prke
PO Box 12425
Lancaster PA 17 605 - 2425
717-656-2 100 Frx: 717-655'2681
B.S
22 l6 ,le'. l0/l0i9t
&&&
LLr sample No. ES 2538081Cottected: 06/?7/96 at 09:05 by BR
suhni rted: 06/28/96
CtJ-4 JUD Matrix Spike Grab Soit Sampte
Hercutes: Bacchus Pond
54JUD SDG#: HBP02-04Ms
CATMO AIIALYSI S IIAI{E
4593 TCL VoLatites by 8240
16?5 Thattium
1 543 A Iumi num
1641 AnriR)ny
1646 Bariun'1647 BeryLtium1649 Cadmiun
1 55 1 Chcomi um
1 653 Copper165/, I ron
1 655 Lead
1658 Manganese1651 tlickeL'1656 Silver
167? Zinc
5708 SU SU8/+6 IcP Digest
6915 Arsenic TR
6936 Setenium TR
0'159 l,tercury
5711 SU SU846 Hs 0igest
TRIAL
1
,]
1
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1
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Lancaster Laboratoftes
2425 New Holland Prke
PO Box 12425
Lancasrer PA I 7 60', -2: i',
7l7-655-2100 Fet. '4" 61i:
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(I}hgmq*r,rts,?gr.*Pries
0819 Sot id Sampte Pest icide Extract SU-846 3550A1?25 TcL Pesticides in SoL ids su-846 BC81
I 0381 eNA soil Extraction su-846 3i50AI 4688 TCL 5!846 SemivolatiLes SoiL SU-846 827084689 TCL SU8/+6 SemivoIati tes/Soi I Su-E46 32708
0l'18 Ittoisture
I'IET HOD
su-816 82408
su-846 6010A
su-846 6C10A
su-846 6010A
su-846 6010A
su-846 6C10A
su-846 601 0A
sr.r-846 6010A
su-34o 60iCA
srJ-846 6C1 0A
su-8/,6 5010A
su-846 6010A
su-846 6C10A
su-816 6a1CA
crr-o/ ! (11rn^
su-346 3050A
su-346 6110A
su-346 6Ji0A
SU-846 717i A
SU-845 7.171A l'1oCi i i ed
EPA 160-l (moCr ; i ed)
Account llo: 06716
HercuLes, lncorporated
Envi .orvnenta I Afia i rs!i Imington DE ]9894
ANALYS I S
OATE AIIO TIHE
07/03/96 051.0
07/13/96 17i4
07/13/96 171107/i3/96 171./-07/i3/96 17',r.
07/',3/96 17i107t1\/96 17"1
07/13/96 17.,407/ii/96 17',4
07/13/96 17^t4
07 / 13/96 17' 4
07/13/96'.,7',4
07/13/96 1714
17/i3/96 17"107/1i/9t, 17',4
07 /c?/c6 ,,931
D7/1.3/96 17'/-
c7/17i96 C33/*
a7/03/96 161,7
27/02/e6 15D6
07/01/96 1400
07/iE/96 C5Z7
07/01/96 1930
57/04/96 1121
07/a4/96 1123
07!12/96 1524
AIIALYS T
Ctark A. Dougherty
Jotene 11. SchieLds
JoIene M. Schietcs
JoLene M. Schiel.ds
Jo[:ne tl. SchieLds
JoIene i{. SchieLCs
JoLene I!. SchieLis
Jotene iit. Schiel.ds
Jotene I. Schietds
Jolene ll. SchieLds
Jotene M. SchieLos
JoIene tl. SchieLcis
Jo(ene f'l. SchieLis
Joiene I. SchieIos
JoIene I. Schietos
Desi R- carozza
Jotene ltl. SchieLds
tlina C. HatLer
NeLLi S. Markaryan
Frances A. De:norest
liattheH U- Kofroth
MicheLe 0. Mack
Shenry Lynn Devtin
Joseph I. Gambler
Josepn lt. GamDIer
tteelay B. I'lehta
Page: 6 of 14
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I,ABORATORY CHRONICLE
(I}h?[tn*,.,',]?,?g,'.919r*'
LLI sample No. 2538081
CU-4 JUD Matrix Spike Grab Soit Sampte
Hercutes: Bacchus Pond
Samp t e
I.IDL
Sanp I e
UIlTS
I GrouP No. 522739
j ttercuLes, :ncorporated ' cE
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OUP
RP9
90 g7
99 98
r04 10c
91 101
102 99
88 78
10? 100
':07 i 01
99 95
96 95
93 92
102 84
106 I05
104 100
99 81
92 90
93 98
96 98
109 107
90 87
94 92
93 96
93 92
QUALITY CONTROL REPORT
Page: 7 of 1l+
LCS LII'IITS
LOU H IGH
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LCS
RPD
LCS
DUPLCS
HS
RPOI.ISDMS
4593'fCL votatiles by 8240
3434 ch t oromethane?' ug/kg
3135 Eromomethane3. uglkg
3436 Vinyt Chtoride2. uslks
34J7 Ch I oroethane3. ug/kg
3440 Hethytene Chtoride2- us/ks
4071 Acetone7. ug/kg
4076 Carbon 0isutJide3. uslks'I180'1,1-Dichloeoethene
Z. ug/kg3442 1,1 -Dichtoroethane1. uglkg3t'11 Chtoroform1. uglkg
3445 1 .2 -D i ch toroethaneZ. ug/kg
4085 2-Eutanone7. ug/kg
3446 1,1, 1-TcichLoroethane
'I . ug/kg
1447 Carbon TetrachLoride1. ug/kg
4091 Vinyl Acetate3. ug,/ks
3448 Bromod i ch I oromethane?. us/ks
3450 1,2-Dichtoropropane3. ug/ks
3454 cis-1,1'Dichtoropropene1. ug/kg
1181 Trichtoroethene1. us/kg
3452 DibromochIoromethane1. ug/kg
3t 53 1, 1,2'Trichloroethane2. ug/ks
1 1 82 Benzene1. uglkg
3451 trans'1,J-Dich!.ot'opropene
ugl k9
BLANK
Batch: E961 831A8
il.0.
N.0.
N.D-
l.D.
J ug/kg
Lancaster Laboratones
2425 New Holland Prke
PO Box 12.125
Ldncaste( PA i75O;-2t25
717-655-2300 irr 7:,--d:6-1681
i ?72
1 241
1 250
'10 254
1 Z?1
19 150
?4 188
1 ?33
59 155
51 138
t+9 155
22 167
52 162
70 140
19 190
35 155
1 209
1 226
71 157
53 1149
52 150
37 151
17 183
a!)
2 7 I ; oe.., ,Orr.rr, ?a #
j95
295
5 102
10 89
396
11 88
2 103
6 105
495
295
191
20 95
1 105
3 '103
20 105
?95
0 '101
2 1.02
2 111
396
298
z 104
198
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(|)h+ffiq*ff.19?s'"*gI'.s
LLI Sample No. 2538081
CU-4 JUo natrix Spike Grab SoiL sampl.e
Hefcutes: Eacchus Pond
Group tlo. 522239
Hercutes, lncorporated - DE
Page: I of 1t
LCS LI14ITS
LOU HIGH
45 169
50 124
5? 140
64 148
16 157
47 150
37 150
37 162
74 136
30 200
54 156
51. 156
50 150
50 155
21 299
70 131
23 177
26 174
54 141
57 145
61 142
53 142
6e 135
55 146
50 1t7
Sa{Tpt e Sampl eiIDL UIIITS
3455 Eromo{orm
LCS LCS
LCS DUP RPD
DUP MSRFD MS TISD RPO
1 . ug/kg N.D. 38 834108 4-Methyt -2-pentanone
3. ug,/ks N.D. 98 91
4 107 2-Hexanone3. ug/kg N.0- 101 903457 TetrachLoroethene1. uglkg il .9- 't 15 110
3t149 1, 1,2,2-Tetrachtoroethane
1 . u9/k9 N.). :00 91
1 183 ToIuene1. uslks N.D. tC5 101
1 1 B/. Ch L orobenzene
1 . uglkg N.!. 96 963458 Ethytbenzene
1 . us/ks N.9. 107 1 04
41 17 Styrene
1 . u9/k9 {.0. 99 92
1355 Xytene (totaL)1. us/ks N.D. 105 103
6187 trans-1,2-0ichIoroethene?. us/kg N .9 . 1 0/. 986277 cis' 1,?-D ichloroethene2. us/kg N.o. 'lo5 101
1625 Thal.tiun Barch:961845708!Cl1t+. m9/k9 N.D. ( 1 ) 93 89
1643 Atuminum Batch: 96',18457083038.8 ms/ke N.D. 21 20?7 1645 (2)
1644 Antimony Batch: 9618457083032.2 mg/kg N.D. (1) 92 95
1646 Barium Batch: 961845703!012.2 mg/ks N.D. 9 105 97
1647 Beryt t iurn Batch: 96'18457080050.08 mg/ks N.D. 0 (1) 96 91'1649 Cadmiun Batch: 9518457083010.13 ms/ks N.D. 0 (1) 93 88
]651 Chromiunr Batch: 961845703C030.46 mg/ks ri-D. 0 (1) 123 1jl
1653 Copper Eatch: 961845708C030.49 m9/k9 N.9. 0 (1) 119 109
1654 lcon Batch: 961845708,:033.1 ms/ks 7.2 J mE/kg 13 2452 2139 (2)
1655 Lead Barch: 961845708iC3?.tt mg/kg N.D. 0 (1) 96 90
1658 Hanganese gatch: 961845708C030.12 m9/k9 N.0. 11 116 109'1661 N icket Barch: 9618457083030.45 mg/ks I.0. 0 (1) 97 91
1666 S i tver Batch: 9618457083010.41 me/ks u.D. (1) 102 97
(1) Ihe result for one or both determinations vas Iess than five times the 100.(2) The backgrouM resutt ras more than four times the spike added.
693
790
12 91
4 115
797
't 10'l
097
I 108
7 101
? ;06
6 101
4 102
696
979
279
7 100
598
799
1 102
6 102
t, 89
794
594
696
798
iFHTi
Lancaster Laboratofle5
2425 Ne,! Holland Plk€
PO Box 12425
Lancasle( PA 17605-2425
717-656-:100 tar: 7l 7-65o'268 1
tt_
,or,orr, ?ai
QUALITY CONTROL REPORT
See reve'se sroe for ?ra a.ai:o. of Symbols and abbrevratrons 2216 Rev
I(l)La ncaste r Laborato ries
QUALITY CONTROL REPORT
Page: 9 of 14
A Thermo Ana lytica I La boratory 'l
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LLI sample No. 2538081
CIJ-4 JUD t'tarrix Spike Grab Soi L Sarpte
Hercu(es: Bacchus Pond
Group |,1o. 522I39
Hercules, !ncorporated - DE
Sanpte Sampl.eI{DL UH I IS
1672 Zinc0.19 ng/kg
5935 Arsenic tn0.25 mg/kg
6956 Seteniun TR0.18 ms/ks
0159 llercury0.028 m9/ks
LCS LCSLCS DUP RPO
DUP IlSRPD MS FSO RPO
LCS LIiYITSLOU HIGH
54 149
19 149
52 1t9
?6 157
BLAIJ(
Eatch : 96'l 8457080030.80 J mS/kS
Eatch:961845708C05
N.D.
Batch:961845708003
|1.D.
Batch:96'!845711002
N.0.
Batch:96'1830103A
11.0.
N.9.
N.D.
N.D.
N.D.
N -0.
N.D.
N.0.
N.D.
N.D.
N.D.
N.0.
ll -D.
N.D.
[.9.
N.D.
N.0.
N.0.
N.D.
0 (1)
0 (1)
0 (1)
0 (1)
108
91
92
9Z
98
92
91
92
92
9J
87
79
6
0
1
0
1??5 lcL Pesticides in Sotids
l9Bl Atpha BHC5. us/kg
1982 Beta 8Hc5. ug/ks1983 0etta BHC1. ug/kg
1218 Gamla BllC - Lindane
'l . uglks'1219 Heptachtor1. us/kq
1220 Atdrin1. ug/kg
1984 lleptachtoc Epoxide3. u9/k9
1989 Endosutfan I4. u9/k9
1 222 Di etdr i n4. uglks
1985 D0E
'I . ug/kg
1?23 Endrin6. ug/kg
1990 Endosutfan I I9. ug/ks't986 DDo3. u9/k9
1991 EndosuI fan SLr( fate10. ug/ks
1?21 DoT1. us/kg
30'17 Endrin Ketone5. us/ks
1859 ltethoxych I or40. ug/ k9
3025 Atpha chtordane4. ug/kg3025 Ganrna Chtordane1. ug/ks
69 85
76 89
73 89
7) qq
71 86
77 92
74 38
79 95
79 94
e7 105
77 93
8? 95
84 101
69 78
79 97
47 57
81 95
T3 89
?1
l6
'19
20
19
19
10
18
17
1B
19
15
18
1Z
?0
19
15
2A
t6
a1
85
76
70
85
81
89
98
93
9t,
a:
90
58
81
65 127
50 137
67 '120
T3 120
69 120
67 120
60 120
60 120
79 120
72 120
68 126
62 120
72 123
6? 1?0
61 121
75 125
57 1t1
75 125
75 1?5
(1) The resutt for one or both determinations vas Less than five times the 100.
Lancaster Laboratofles
2425 New Holland Pike
PO Box 12425
Lancaster PA 17605-2.125
717-556'2100 Fax 717'55c-2631r&rn d:l
I
5ee.everse..iCe tr; ototac,a'a^ :: ;,rools anc ii;'e,rratroni 22 l6 Ae'/ iC/lOi-o>
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Ilcroup tto. 52239
I ttercutes, tncorporated - OE
j
Sample ganpte
HDL UNITS
l9BB Toxaphene1,000. uslks
1992 Endrin Atdehyde10. uslks
1993 PCB-101610. us/ks
1994 PCS-122130. u9,/k9
1995 PCB-123250. ug/kg
1996 ?cs-1?4?50. us/ks
1997 PCB-124840. us/ks'1998 PcB - 125430. ug/ks
1999 PCB- 126010. trgl ks
DUP IlS
RPO M9 MSO RPD
LCS LCS
LCS DUP RPO
LCS LIMITS
LOIJ H I GH
57 123
4688 TCL SU846 Semivolati Les soi t Batch: 9o183S!9C26
1 1 85 phenoI13. us/kg
3753 bis (2-chloroethy[) ether67. ug/ks1186 2-chtorophenoI33. uglks3751 1,3'dichtorobenzene13. us/kg
1187 1,4-dichtorobenzene33. uglks
3755 1,2'di ch Iorobenzene33. us/kg
1650 2-methyLphenoI67. u9lk9l+691 2,2' -oxybrs ( l -chtoroprooane)
100 . us/k.s469? 4-methytphenoL100. uglks1'l88 N-ni trosodi -n-pcopytamine
67. us/ks
3757 hexach t oroethane67. ug/ks
3758 ni trobenzene33. ug/ks3759 i sophocone67. uslks
3746 2-ni tropheno!.67. ug/kS
N.D.
N.0.
N.D.
N.D.
N.D.
N.D.
N.D.
N.0.
N.D.
N.D.
N.D.
r1 .0.
N.D.
N-0.
5 112
12 158
23 134
1 172
20 124
32 129
46 123
36 166
5 152
1 210
4A 113
35 180
2i 196
29 182
13 77
11 76
12 7i
576
576
674
t) / I
11 1)
14 90
t) I I
'10 B0
778
10 87
9 7t)
72 32
75 54
69 78
75 79
7t, 78
7? 77
69 80
62 70
Bt, 97
7t, 8t
75 8i
/ / 5J
33 e2
Lan(aster Laboratofie5
2425 New Holldnd PrkE
PO Box 12425
Lancasier PA 17505-2r::
717-656-2300 f a\ 7', ).;)\a-2i31
(I}La ncaste r Laboratories
A Thermo Analytical Laboratory
LLI sample No. 2538081
CU-4 JUO Matrix Spike Crab Soi I Sampie
Hercutes: Bacchus Pond
gLANK
N.D.
N.D.
N.D.
r,J.0.
ll.D.
N.0.
N.D.
N.D.
N.D.
15
QIJAI,ITY CONTROL REPORT
Page: 10 of 11
a,
'nr-.0,,r,
?ait' l' ;;-co,: J': icc.e,.,t.riroa!
(I)Lancaster Laboratories
QUALITY CONTROL REPORT
Page: 'l '1 of '14
A Thermo Analytical Laboratory I'l
I
IiIS LCS LCS
I.|SO RPD LCS DUP RPO
DUPRP9 MS
LLr sample No. 253808i
CU-4 JUD l,latrix Spike Grab Soi t Sarpte
tlercutes: Sacchus Pond
I Group No.
: Hercutes,
i
52?739
Inco.porated - DE
Sampte SampteMDL UII I TS
3747 ?,4 -dinethyLphenoL
67. ug/kg
3760 bis (2-chtoroethoxy) methane31. uglks
3718 ?,4-dichtorophenoI33. uslks
1189 1,2,4-trich torobenzene33. ug/kg
3761 naphthatene33. ug/kgt693 4-chtoroanitine100. uslks
3762 hexachIorobutadiene67. u9/Y.9
1 190 4'chtoro-3-methytphenoI67. ug/k.g
1694 2-fllethytnaphthatene33. ug/kg
3763 hexachtorocyctopentadi ene
1 70. u9/ k9
371? Z,t,6-ltichtorophenol67. ug/kg
4695 2,4, 5-trichiorophenoI67. uq/ks
3764 2-chIoronaphthatene33. ug/ks4696 2-ni troani t ine67. ug/ks
3760 dirEthyt phthatate33. uslkg
3765 acenaphthytene33. uelks
BLAIIK
N.D.
r,1.0.
N.D.
[.0.
N.D.
N.D.
N.9.
N.D.
N.C.
N.D.
I.D.
N-0.
N.0.
N.D.
N.9.
N.D.
13 57
73 81
71 81
77 82
73 77
1/, 15
3C 87
75 86
L io
31 9C
80 8e
79 85
72 7e
79 87
17
'11
13
6
5
5
9
i3
10
7
11
10
8
I
10
a
75
78
t>
43
82
1A
62
82
oz
79
75
80
77
73
6l
75
to
90
B5
LCS LII,IITS
LO\J H t G:1
3? 119
33 184
3e 135
44 112
21 133
17 116
2t+ 116
?2 1/.7
?8 1?3
1 100
37 144
39 151
60 118
)J I4J
1 112
33 145
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1
1
28
39
50
4689 TcL su845 seflivotati Ies/soi I Batch: 96'183s18026
1697 3-ni troani I ine67. uglkg'1191 acenaphthene33. us/ks
3750 2,4-dini trophenot170. u9/1.9
119? 4-ni trophenoL
1 70. us/ks
4698 di benzofuran31. us/kg
1193 2,4-dinitrototuene67. ug/kg
t 699 ?,6'dini trototuene67. ug/ks
MEMBEFlrffil-il
1,5 40
I to
59 65
73 77
7r, 80
s2 89
81 89
'10
9
8
6
8
7
10
113
145
191
132
131
139
153
Lan(a5ter Laboratofle5
2425 New Holland Prke
PO Box 12425
Lancastel PA i] 6A5-2t25
717'656-2100 Fax 7l 7-556-2681
I
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Group l,lo. 5222J9
Hercutes, Inco.porated - DE
QI-IALITY CONTROL REPORT
Page: '12 of 14
LCS LIIt,IITS
LOU HIGH
DUP MSRPD MS MSD RPD
LCS LCSLCS DUP RPO
sarpt e Sanpl. eMDt UII I TS
3770 diethyl. phthatate67. ug/kg5769 (-chtorophenyt phenyt ether67. uglkg
3768 ftuorene33. us/ks
4700 4-ni troani L ine100. ug/kg1701 4,6-dini tro-2-methytphenot170. u9lk93772 N-ni trosodiphenytaarine67. us/ks3Ii-J 4-bromophenyL phenyt erher
1 00. u9/ ks
3774 hexachtorobenzene100. u9/k9119q pentachto.ophenot170. u9lk9
3775 phenanthrene31. us/ksJ776 anthracene13. u9/ k91702 carbazote33. ug/ke3n7 di-n-butyI phthat6te33. u9/k9
3778 ftuoranthene13. ug/ k9
1 195 pyrene67. uslkg
3780 butyl. benzyI phthatate67. u9/k9
3783 3,3' -dichtorobenzidine130. u9/k9
3781 benzo (a) anthracene31. u9lk9
3781 bis (2-ethyLhexy[) phrhaLate67. us,/ks
3782 chrysene31. uslkg3785 di -n-octyI phrhatate67. uglks3786 benzo (b) ftuoranthene67. u9/k93787 benzo (k) fLuoranthene'130. uslks
37BB benzo (a) pyrene67. us/kg
37Bq indeno (1,2,3-cd) pyeene67. us/ks
083
084
779
476
966
?73
i80
lB2
263
077
977
185
977
0 9l
295
568
780
9 103
885
I 103
080
086
078
882
79 88
79 87
74 80
59 62
66 72
7t, 84
81 9?
81 9r.
7t, 76
75 83
7t, 79
3C 90
73 80
BJ 92
e6 97
55 58
77 83
93 101
32 39
81 92
7i 80
77 85
7t 81
82 89
1
25
59
?n
,1
33
5l
'1
11
27
35
,]
25
52
1
1
33
8
17
4
2l+
11
17
1
114
158
121
12?
18',!
147
1?7
15?
176
120
113
1',I8
137
115
152
262
1\3
158
168
146
159
loJ
163
tt I
Lancaster Laboratofie5
2425 New Holland Prke
PO 8ox 12425
Ldn.asie. PA I7605-2+ll
717-656-2100 Far 7'i-aja :rij
,t|.#
(I)Lancaster Labo ratories
A Thermo Analytica I La boratory
LLI sample No. 2538081
CU-4 JUo llatrix Spike Gcab Soit Saspl.e
Hercutes: Bacchus Pond
ELANK
[.0.
N.D.
N.D.
N.D.
N.9.
il.0.
N.D.
N.D.
N.0.
N.D.
N-1.
N.D.
N.9.
N.9 .
N.0.
N.9.
N.9.
N.0.
lt.D.
N.0.
N.9.
N.C.
N.0.
N.D.
N.9.
Se: 'e ie'r: :,q: ror e:o,jn;;,on ol ;7:;rbor; and abbrevratron5 22 I 6 le,. l0,i 10/95
LLI sample No. 2538081
CH-4 JUD ilatrix Spike Grab SoiI Sample
Hercules: Eacchus Pond
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Group llo. 522259
tlercutes, lncorporated - DE
Page:
LCS LCSI-Cs DUP RPO
B]
75
Sarpte SampleIITDL UNITS
3790 dibenz (a,h) anthracene67. us/kg
3791 benzo (ghi) PerYtene67. ug/kg
01 18 Moi sture0.06 Z by Ht.
BLANK
[.D .
N-D.
Batch : 961840316820003A
Lancaster Laboratorles
2425 New Holland Prke
PO 8ox 12d25
Ldncasie( PA I 7605-2425
717-656-2i00 Fax [phone] I
9
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83 91
79 36
LCS Llt'!trs
LO\J H ! GiI
1 ?27
1 219
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QUALITY CONTROL REPORT
- aa)r ind -ica:a,.lairons
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LLf sample No. 2538081CU-4 JUo Hatrix Spike Crab SoiI Sampte
Hercutes: Eacchus pond
1225 IcL pesticides in sol.ids
4593 TCL Votatites by 82q0
4688 TCL SU846 Semivotatites Soi t
4689 TCL SU846 Semivol.ati Les/Soi L
Group No. 522139
Hercutes, lncorporated - DE
QI-TALTTY CONTROL REPORT
SURROGATE LII{ITSLOU HIGH
La ncaster Laboratories
\Il1lm o An a I yt i ca I La bo rato ry
I
TRIAL ID
Lancaster Laboratofles
2425 New Holland Prke
PO 8ox 12425
Lancaster. PA I 7505-2125
717 -6t6-23AA Far 717-o1:-l6d
SURRO6ATE
SURROGAIE
TCX
DCB
d|+-1,2-,cA
d3-totuene
BTB
PhenoL -d6
2-FtphenoL
?,4,o-aBP
Nitrobz-d5
2-tbiphnyL
TDrreny ldl4
SUMHAR Y
RECOVERY Z
63
5J
89
102
9?
65
52
77
lt
1L
3l
50
50
70
ol
74
24
25,.9
23
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120
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121
117
121
113
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122
120
115
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MEMBER
see.:'/erse ;rcje for e,o,;r,il oe oi \ tr,;a,; j:c abore,.,tattons Rer
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Rel.
Pagel 'I of 1?
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11.
2.6
2.6
0. 088
0. i6
0. 56
0.60
4- t
?.9
0. 14
0.55
0. 54
0.4E
0.30n)1
0. 035
4593
1625
1643
164t
16t 6
1647
1649
1651
lo)5
l6)4
1655
'1658
t6b I
1666
1672
6935
6936
01 59
4688
t+689
0111
AS RECEIVED
itlt:::.1:.rji::tl::,t-1.i...1 ,:::::1.::.:::.::i:::::::.:r:.: lt E T tl 00
liiiriliiIifiE,f!,ltilg:Ijr;1, DETECT I 0N L I M I r uN I rs
see Page
13 . rng/kg8.6 ng/'Kg2-1 mS/kS2-1 mg/kEC.070 m9/kg
0. '12 ng/kg
0.4 5 ng/!.g
C .48 n9/ <g3.2 ng/(g2.3 mg/(g
0. 1 1 ms/kg0.44 m9/k90./,3 ms/k9C.l3 ms/ke
0.?t, tt19/'<g
0. 1 7 ng/'r.g
Ll , 328 ng/ Kg
See Fage
See Prge
i:i:,::i,':::::i::ii:i::',20:.2:. :,j:.:' 0.06 il by rt.
in',.reight of the sampte after oven drying at
DRY IJEIGHT,.,,:,:,:,,,,::::,:i:1::,:,'::::r,:::,,,,,:,:,,,1:,, HFTHoD
iir:::.iiiii:rii,.8gsu,clq;:*i. oere cr t ol u I r I rANALYSIS IIAITE
TCL Votatites by 8240
Thattitrn
A Iurni nun
Ant innny
8ar i um
Becyt L i trn
Cadni un
Chromi un
Copper
I ron
Lead
Flanganese
l{ickeI
S i tver
ztnc
Arsenic TR
SeIeniurn TR
Mercury
TCL 51J846 Semivotatites SoiI'tCL SU846 Semivotati tes/Soi t
Hoi sture
"lloisturetr aepresents the Ioss
103 - 105 degrees Cetsius.
.,,,,,5,, t,,;;,.,,,.,,,
i.'i:i:::rt,liri0'i i:li :;t
.i. j.t.,:!:;::,lilr., Oi:::,i::::,
ATTN: Hr. Joseph KeLLer
ATiN: Mr. Bnent Robinson
Services Represen!ativeat (7i7) 656-2300126i,36 522739
Lancas(er Laboratofles
2425 llerv Holland P:ke
PO Box 12425
Lancasier. PA 17 6A5' 2424
717-656'2i00 Fax il7-b':5-2561
Respec:fuL Ly Submi tted
Ramona V. Layman, 6roup Leader
ICP Metats/Leachates
i?I
I
(I)h+ffiq*s#,s?s'"*tsr'*
LLI sample No. ES 2538098Cottected: 6127/96 at 12:45 by sR
SuHnitted: 6/?8/96 RePorted: 8/ 7/960iscard: 9/ 7/96
Stat 4(44) (6-10") Gcab SoiL Sarnpte
Hercutes: Eacchus Pond44A6- S0Gf: ll8P02-'19
Hercutes, lncorporated
ERH ' Rocky Hountain
ouestions? Contact your CIienr
Rachel L. Krea,nef
03:46:51 D 0002 23 REP310 25.00 001',t2100 ASR000
Account No: 067'16
Hercutes, lnccrporated - DE
j Envirorrnental. Affairs
I Uitmington DE 1989/+
MEMBEFt
5ee reve.se sicie ior erplanai,o. of s/ftrbols a.o aobre, iiion5 22:6 R:,r t0/10/95
P.0.
Ret.
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LLI sanple No. ES 2538098
col,tected: 6/?7/96 at 12:45 bY 8R
suEnitted: 6/?8t96 RePorted: 8/ 7/96
0iscard: 9/ 7/96
stat 4(4A) (6'10() Grab Soit Sanpte
Hercutes: Bacchus Pord
14A6- SoG#: HBP02'19
CAT}IO. AIIALYSIS IIATIE
TCL Votati Les bY 8240
343t+ Chtoromethane
3435 Brornomethane3436 Vinyt Chl.oride
3437 Chtoroethane3440 !.lethyIene ChIoride4074 Acetone4076 Carbon Disutfide1180 1,1-Dichtoroethene3412 1,,l'0ichIoroelhane3t,41 chtorofocrn
3445'1,2-Dichtoroethane4085 2-Butanone3116 1,1,'1-Trichtoroethane
3417 carbon TetrachIoriCe
4091 Vinyt Acetate
3418 Brornodichtoromethane
3450'1,2'0ichtoroProPane345t1 cis-1,1-0ichtoroProPene1181 Trichtoroethene
3452 DibromochIoromethane3453 1,1,2'Tr-ichl'oroethane
1 1 82 Benzene3451 trans'1,3-DichIoroProPene3456 Bromoform4108 4-Methyt-2'Pentanone
1107 2-Hexanone3457 Tetrachtoroethene
3449 1,1,2,2-Tetrachloroethane
1 183 Toluene
1 184 Ch(orobenzene3458 EthYtbenzene1.117 Styrene3355 xytene (totat)
6187 trans-1,2-DichIol.oethene
6Zn cis-1,?-0ichtoroethene
Tt
I eccount No: 06716 I
I xeccutes, Incorporated - 0E I
I Envirorrnentat Affaics Ii tJrtmi^gton DE 19894 |lltr
RECE I VED
TIETHOO
r::,' DETECTf0H LIl.lIT UlllTS
ORY UEIGHT
:ii::i::::i.:.:::r:::i:i.:::::.:::.il::j::::r:;::::':ii: llETHoD
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ancaster Laboratories
A Thermo AnalYtical La boratory
Page:
Respect:f ut ly S,Jbmi tted
Hichele i!cCtarln, g.A.
Group :eader, Gg/li9 VoLatj Ies
2ol 12
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us/k9
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u9l k9
ug/ kg
u9/kg
u9/ k9
usl ks
u9l k9
ug/(g
ug/kg
ug/ kg
u9/k9
u9lis
u9/ f9
ug/ i(9
us/kg
uglkg
'rg/'r9u9/k9
u9/ <s
u9/kg
u9/ kg
us/kg
ugl kg
u9/ k9
u9/\9
ug/kg
u9lkg
ug/ <9
u9/ ks
ugl l{g
u9/ kS
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ouestions? contacr Your cr' len':
Rachet L. Krealner
SeTvj ces Representat I ve
at ( 71 7) 655-2iC0
Lancasler Laboratorles
2425 Nle,^ Holland Prke
PO Bo1 12125
Ldncasier PA 17605-21:l
717-6:6-21C0 Fax 7l:'::c -li:31
MEMBER
see re..,erse 5roe ioa eroldnallon ci;vmbors "c iollrellalroni
Lancaster Laboratories
Aihermo Analrtical Laboratory
P age:3of 12
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LLI samPle No- ES 2538098
coite"t.a, '6/27/96 at '12:45 bY BR
Suhritted: 6t28/96 Reported: 8/ 7/96
Discard: 9/ 7196
I
I Account llo: 06716
i Hercutes, lncorPorated ' DE
I Envi rornrentaI Af fairs
i uit.ingto.t DE 19894
P.0.
Ret.
5ss1 ((4A) (6-1Oil) Grab SoiI Sampte
Hercules: Bacchus Pond
44A6' SDG#: HBP02-19
CATNO. ANALYSIS }IAI'IE
TcL votati tes bY 8240
Benzene uas detected
concentration of 1'
anatYticat resutt'
AS RECEIVED
rii*iirlln!-$:tj.tff ,,,,1i1[io "'' T u]r I Ts
in the method bl'ank at an estimated
,t)*n.- ir'," ulrni vatue pas not subtracted from the
ORY UEIGHT
:.ir.::ir,.::,,,,.:'::,:.:. llETHOO
':ir,pEgUt1g,r,.: DETECTI0N LIlllT
Ouest ions? Contact
Rachet'.. Krealner
vour Ct ient services Representatlve
at [phone]
Lancaster Laboratorres
2425 New Hoiland Prke
PO Box 12425
t ancastel PA , ,'6n5-2t25
717-655-210C iax 717-55o-1631
ResPectfuI LY Submi tted
Miche!'e McClarin' 6'A'
GcouP -eader' Gc/HS Votati tes
See ie'.'e.5e ilde icr ?1ci'ir'lio' ci ''1"'"i)r! 'lec i3or9/rat'oa' 7::5 ;:' rl_ 9i d'1
T
MEMBEFI
I
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t
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(I)Lancaster Laboratories
IIETHOD
DETECIICN LIIi,!IT UIJI TS
u9/k9
!s/ <g
ug/\9
u9lks
ug/\9
u9,/ kg
uE/k9
ug/ <g
!9/'<g
uglk9
ugltg
uglkg
2e/ <gu!/is
u9/<g
u9/ <g
ug/ <9
!9/ <e
')g/ <g
qg/kg
ug/\c:
u9/k9
us/<g
!9/k9
u9/kg
u9/kg
ug/r9
u9/k9ug/\9
u9lk9
Respect f uI Ly Submi ttedChristine Y. RatcLiff,
Group l-eaCer, CC/MS
t
,.-OOr5 arrO ;a3r:Ylal'Oni
4ol 12
42.
84.
1?.
42.
42.
12.u.'110.
110.
84.
84.
1?.
84.
84.
4?.t2.
4?.
4?.'E0.
84.
84.
42.
210.u.u.
4?.
84.
12.
Page:A Thermo Analytical Laboratory
LLr sample No. Es 2538098cott*ted: 6/?7196 at 12:15 by BR
suutritted: 6/28t96 Reportedl 8/ 7/960iscard: 9/ 7/96
Stat 4(4A) (6-10,,) Grab SoiI SatrpLe
Hercu(es: Bacchus Pond4446- SDG#: HBP02- t9
CATItO, AIIALYSIS llAIitE :.,::,.
fCL SU846 Smivotati les SoiI
Account tlo:057'15
AS RECEIVED
P. O.
Rel..
ORY UEIGHT
ii'ri:li:,t:it':li:it,.::,t..,.,.it,,,:.it. :,,..1.,.i,' lilEltloo
i..iiliti.iilt,:.j:,ir,:.8qSUtIE:l :.:r: DETECT IOH L I Mt T
1 185
3753
1 186
3751
11A7
3755
4690
469?
1 188
3757
3758
1759
3716
3760
3718
1 189
3761
4693
376?
1 190
4691
3763
3749
4695
3764
t 6c6
3766
3765
phenoL
bis (2-chLoroethy[) ether
2-chLorophenoL
1,J-dichIorobenzene
1,4-dichtorobenzene
1,2-dichlorobenzene
2 - methy I pheno L
2,2' -oxybi s ( 1 -chtoeopropane)
4-methytphenol.
N -ni trosodi -n- propyt ami ne
hexach Loroethane
ni trobenzene
i sophorone
2-ni trophenoI
2,4 -d i methy t pheno ibis (2-chLoroethoxy) merhane
2,4-dichLorophenoL
1,2,4-tri ch Lorobenzene
naphthr Lene
4-chLoroani I ine
hexach Iorobutadi ene
4 " ch L oro - f -!rethyL pheno L
2 -rnerhy t naph !ha I ene
hexach Iorocyc I opentadi ene
2,4,6- trichlorophenoI
2,4, 5- trich LorophenoL
2 - ch I oronaph tha I ene
2-ni troani I inedimethyt phrhatate
acenaph thy I ene
Questrons? Contact your
RacheI L. Kreaner
irf.ESutIsi
67.
31.
15.
31.
j-1-
o7.
r00.
l0!'.
67.
ji.
67.
07.
07-t3.ji.
il.
10c.
67.
67.3i.
170 .
67.
67.ji.
67.
t5 -
CL ient Services Repaesentar!ve
at (7'.7) 656-23CC
Lanca5ler lJoo.aloil,o!
M E M B g g 2425Ne,ruFlcLlanoP,[eK-li-l ;,1i;#i*j,;:, i,',, ;,u,n.,,
,!}.?.Jsee reve.3i j rii :':{arana-:_l: l5 E,-. lC/lC 95
I
I
I(iI)Lancaster Laboratories
Re[.
5of 12
u.
42.
210.
1?.
81.u.
42.
IJU.
210.
130.
210.
12.
1?.
42.
12.
42.
81.
1 70.
1?.
84.
42.
8/..
oq.
170.
84.
B/..
Page:
ORY IJEICHT
i;i:i:il:::li:i:;:i:ii.rii:!r:i;::: METHOo
",RESUIIS'].i;i:
DETECTION LIMII
'lA Thermo Analytical Laboratory
LLI sanple No. Es 2538098
cottecred: 6/27/96 ar 12:45 by 8R
Subnitted: 6/?8/96 Repoetdz 81 7/96
oiscard: 9/ 7!96
stat 4(4A) (6-10x) Grab Soit SampLe
Hercutes: Bacchus Pond
44A6- s0G#: HBP02-19
CATllo. AHALYSI S llAr'l€
TCL s1J846 sffiivotati Ies/soi I
4697 5-nitroanitine1191 acmaphthene3750 2,4'dinitrophenot1'192 4-ni trophenoL4698 dibenzofuran
1193 2,4-dinitrotoIuene4699 ?,6-din'itrorotuene3770 diethyl. phthaLate
3769 4'chtorophenyl phenyI ether
3763 f Iuorene4700 4-ni troani I ine
4701 4,6'dinitro-2-methytphenoL377? {-ni !rosodiphenytamine3773 4-bromophenyL phenyI ether3771 hexachtorobenzene119/* pentachtorophenol3n5 phenanthrene
3776 anthracene
47OZ carbazote3Tn di -n-butyl. phthatate
3778 ftuoranthene
1 195 pyrene
3780 butyl benzy[ phtha[ate
3783 3,3' -dichIorobenzidine
378l benzo (a) anthracene
37:c/- bis (2-ethyLhexyt) phthal.ate
37aZ chrysene3785 di -n-octYL phthatate
3786 benzo (b) ftuoranthene3787 benzo (k) iLuocanthene
3788 benzo (a) pyrene
3789 indeno (1,2,5-cd) pyrene
3790 dibenz (a,h) anthracene
3791 benzo (ghi) perytene
I
l Account tlo: 06716
I Hercul,es, lncorporated - oE
I Envi romrentat Af fai rs
luit*'^g.on oE l9B9/.
i
I
I
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t
I
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I
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I
I
A9 RECEIVEO
:.::::j::.:::::t::i::::::ri:li:::::.,: ::: :.::: l'tEIHoO
:;::,:i::':l:li':ii'tEsuET.8,:',|::..i DETECT I Or.l L I t! I I utl I Is
: illii ii i:it::i:i:ri ::ll :'.:riiil rI . 0 j
::: :-::..r i.r:tl .::':: :: . iI.0.
:t::l:l::t ;:ti:ri:: :1:i::;: :i |l:D
t!,: :t.,,,i:j:.,,,,:f t:':; fl :D:,
:,:: . ti:::.rr:..::t ; :.it I.iD.
... tt. -- : .J:i!t.,1ii::tit:,,'lf: g.,t'
: t't:tir. :...u:q
,.1 1... . x.o ' :' '
"1;',;'ZOO.,.,',,,,.r:;:::::., l[;P;:]i
... 1:li:j::.:,i..ll-9. r:
t:',:i.iit;i:,:ttU.g. ::
il:i:,t,:, ':t:N:;Ot
1';' ,,11 -2..r; ',
. :,, ,t:: :tu,;:g. .t,',..,.ll,D:'
67.
31.'170 .
17n
67.
57.
67.
07-
13.
100 .
1'/C.
b7.
100 .
100.
3i.
iJ.
51.ll.
67.iri.
67.
15.
67.
150 .
67.
67.
67.
67.
u9/kg
uglk9
ug/ks
u9/kg
u9lk9
ug/k9
ug/tg
ugl <9
'ra/kgu9/k9
u9/kg
!9/\9
rg / <.)
ug/(g
u9/(9
u9/k9lg/kg
ug/kg
,J9/ <g
ug/k9!9/ls
ug/ \.J
u9/kg
ug/19
ug/lg
uq/ kg
trg,/ Kg
u9/kg
uslkg
ug/k9
u9/k9
us/k9
ug/ ks
uglk9
Ouestions? Contact your ctient Services Rep.esentalive
Rachel L. Krearrcr at (7'7) 656-230c
Lancasler !aboralones
2425 Ne,r'/ Hoiiand Prke
PC Box t2:12-c
L;nclsr.a PA ,, t-515-2e21
;1 ;-656-2100 ?ar 7 17'656-253
RespectfuL l-y Submi ttedchristine !- Pa!clifi,
Croup l-ead!.f, 6CIES
ie:.ayerre lc+ t:'-.O;.toltc'o; i.-a': ) ':' c aoc'? a1 ::ta
,l}
..', ,- ,n,t,.,r. ?ap
I
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MEMgER
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&&6.
(I}Lancaste r Laborato ries
)RY CHRONfCLE
Page: 6 of 12
LLI Sample No.cottected: 06127/96 at
A Thermo Analytical Laboratory
ES 2538098'12:45 by BR
I
I Account lo: 067t6
r tiercuLes, lncorporated - DE
i EnviromentaL Afiairs
I tJiLmington D€ 19894
IStat 4(4A) (6-10',) Grab SoiI Sampte
Hercutes: Bacchus Pond44A6- SoG#: HBP0?- l9
CATIIO AIIALYSIS XAME
4593 TCL VoLatites by 8?40 07/01/96 0517 C(ark A. Dougherty
IIEI HOO
su-846 82/+08
su-846 6010A
slJ-846 6010A
su-8(6 6010A
sw-846 6010A
sr.J-346 6310A
su- 346 ,5i 10A
su-846 6010A
su-346 6C10A
su-9(6 6C10A
su-346 6C10A
s!.J-316 6C10A
SII - 84o 641 0A
sH-846 o010A
ss-816 6110A
5tJ-8/r6 l!50A
su-816 60'10A
s.J-3r,6 6i't0A
su-846 7(71A
5u-lll,6 71,7'lA l'1odi f i ed
su-946 1550A
slJ-346 827C8
su-346 B?708
EPA '160.1 (moCi fied)
16?5
1 613
1641
1616
toq/
1 649
'I 651
I O)J
165/.
1 655
1 658
1 661
1 666
1672
5708
6915
6916
That t iw
Atwinm
Ant ircnyBariu
Beryl. I i um
Cadmi ul
Chrmi w
Copper
I ron
Lead
llanganese
N ickel.
Si Iver
Zinc
su su846 tCP Diqest
Arsenic TR
Seleniw IR
AXALYS I S
OAIE AIID
07 /13/96
07 /13/96
07 / 13 /96
07 / 13/96
07 /13/96
D7 / 13 /96
07 / 1a /96
07 1'.31q5
s7 /.:3/96
07 / "3/9607/ "3/96q7 / 13 /96
a7 /13/96
07 / 13/96
c7 /0?/96
07 / 13/96
a7/17 /96
ANAI.YST
19'13
1913
191 lr91l
19' l'19,3
!9r3
19'..1't9'3
19^,!
1911
i 9-13
1913
1911
193/.
1913
1 020
Jotene M. Schietds
Jotene it. Schiel.ds
Jotene lil. Schiel.cis
Jol.ene i'l. Schietds
Jotene M. SchieLis
Jot ene lil. Sch i elos
Jotene tl- schieLcis
Jotene i(. Schietcs
Joiene t1- SchieLCs
Jolene M. SchieLcs
Jolene t!. schieLis
Jotene !'.l. Schier,ds
Jolene F!. Schielcis
JoIene !!- SchieLis
0esi R. Carozza
Joi.ene l{. SchieLds
tlina C. Lrauer
t
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0'159 llercury
5711 SU SlJ846 H9 oigesr
0381 BNA Soit Extraction4688 TCL SU846 Sffiivotati Les Soi I4689 TCL sU846 SemivoIati Les/Soi t
01 'l 1 llo isture
07/03/96 1703 NeLLi S. llarkaryanq7/C2/96 1506 Frances A. Demorest
07/01/96 1C3O Sherry Lynn Devtin
07/05/96 2154 Joseoh I'1. Gaf,bIerD7/05/96 ?15/+ Joseph lq. SambLer
07/0?/96 152A leeIay 8. Mehta
Ldncaster Laboralor et
M E M B E g 2d25NevrroliarcP,,ef6ill ii;ii#i:i:''::,i,'1,,,,u,,
D,
,r," *", ,n.,Ur, [3
TABORATORY
tee fe,rerse tde rr rrarartailon of ;r-cr;r: ;^o 6cc'et,ratror\i
I
I
I
T,LI sanple No. 2538098
Stat 4(4A) (6-10") 6rab Soit Saapl.e
Hercutes: Eacchus Pond
I
I
; Group xo. 522759
I Hercutes, :ncorporated - DE
I
II
I
Page: 7 of 12
LCS LII'IITSLOU HI GiI
(iI)La ncaster Laborator:ies
A Thermo Analytical Laboratory
Sanpl, e
MDL
Satrlpl.e
UHITS
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LCS LCSLCS DUP RPD
DUP lils
RPD MS I'1SD RPOELAXK
Batch: E96'l831AC4595 TCL Votatites by 9240
5414 ChLocmethane?. uglkg
3455 BrqMethane5. us/ks
5436 vinyt chtoride?. us/kg
3437 chtoroethanel. ug/kg
3440 ttethytene chLoride?. ug/kg
4074 Acetone7. us/kg4076 Carbon Disul.;ide5. ug/ks
1'180 1,'l-0ichLoroethene2. ug/ks3442 I , 'l -D i ch toroethane1. uslkg
f444 Ch Ioroform1. uglks
3445'1,2'0ichtocoethane2. uglkg
4085 2-Butanone7. uglks
5446'1,1, 1-TrichIoroethane1. uglkg3447 carbon TetrachLoride1. uslkg4091 V'inyl Acetate
5. ug/kg3448 SrmodichIororethaneZ. ug/ks
1450 1,2-Dichtoropropane3. u9lk9
3454 cis-1,3'DichLo.oProPene1. ug./kg
1181 Trichloroethene1. uglks
5452 Dibrorcchtoromethane1. ug/kg
3153 1,1,2-Trichtoroethane?. uq/kg
1 1 B? Benzene
'1 ' ug/kg3451 trans-1,J-Dichtoropropene1. us/kg
N.D .
N.9.
N.D.
N.0.
'l . J uglkl
N.9 -
90 87
99 98
104 100
91 101
1C2 99
88 78
1 C2 ',l00
107 101
99 95
96 95
93 92
102 R4
'106 'i 05
104 1 D0
99 81
9? 9C
99 98
96 93
1C9 1.97
90 87
9t, 9?
98 96
91 9?
395
295
s t02
10 89
196
11 88
? 103
6 105
495
295
'1 91
20 s5
1 105
I 103
20 105
295
0 101
2 102
2 111
396
298
? i01
r98
1 ?T?
t zql
1. ?50
10 ?51
1 ?21
19 150
?1 188
1 ?13
59 155
s1 118
19 155
22 167
s? 162
70 110
19 190
35 155
1 2C9
1 ??6
7i 157
53 119
5? 150
37 151
17 183
Lancasler Laboratone5
M E M B E R 2425NewHollandPrke
7ffii-n iii'#i:1i':::;iir.,u,u.,,:i I
t
I
QLiALITY CONTROL REPORT
5ee':.r:rie ;roe :c' :tcrandlon ci s,r::9,: rnrl iiicr:.r(ii.cn -r0,,95
l-cs
RPD
83
o1
I
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(I)La ncaste r Laboratories
A Thermo Analytical Laboratory
r GrouD !,io.
I Hercutes,
I
I
i
5z?Ti9
:ncorporated - DE
Page: 8 of 1?
LCS LII'ItISLOU HIGH
LLr sample No. 2538098Stat 4(4A) (6-10'.) Grab SoiI SanpLe
Hercutes: Bacchus Pond
Sarpt e
MDL
1
6
I
I
I
I
I
I
3456 Eromoform1. us/ks4108 4-Hethyt -2-pentanone3. uslkg
4107 2-Hexanone3. ug/ks3457 Tetrachtoroerhene1. uglks3119 1,'|'.2,2-Ietrachtoroethane1. uglkg1185 ToLuene
'| - uglks
1 184 Chtorobenzene1. us/kg3458 Ethytbenzene
1 ' us/kg
41 17 Sryrenel. uglksJ555 Xytene (torat)
'l ' uglkg6187 trans-'1,?-0ichLo.oethene?' sg/'<g6?77 cis-1,2-Dichtoroerhene2. ug/kg
1625 ThaLtiu11. m9/k9
1643 Atwinum8.6 mg/kg
1644 Anr ircny2.1 ms/kg
1646 Sariq2.1 mg/ks
1647 Eeryt t im0.070 ms/kg'1649 Cadm'iw0.12 mg/ks
1651 Chrmim0.45 ms/ks
165J Coppec0.48 mg/kg
1654 Iron3.2 m9/k9
1655 Lead?.3 mg/kg
'1658 l.{anganese
0.1 1 ms/ks
1661 lr icket0.14 m9/k9
1666 Si Lver0.13 ms/ks
I.9 -
N.O-
N.0-
il-D.
N.D.
|i .).
N-).
N.0-
N.).
N.3.
Eatch: 961845708003
N .D.
Earch: c6i845708003
Batch: 961845708CC3
ti.D.
Satch: 961845708003I.0.
Eatch:961845708C03
N-9.
Sarch: 961845708e01
N.5.
Batch:9613/+5708C01ti.c.
Batch: 90'1845708t03
N.D.gatct: 9o'i8457oBOtil7.2 J mg/ks
Batch:961845708.101
ti.D.
Barcir:9618457C8301
ti _r.
Eatch: 961845706a03
N.D.
Eatch: 96i345708101
li.D-
MS
95
101 90
115 110
'100 91
105 :03
96 9i,
105 1 0l
1C4 9e
'r 05 101
(1) 93 89
?1 ?2?7 1545 <2)
(1) 9? 95
9 'lc5 97
c (1) 96 91
0 ('1 ) 91 38
0 (-1 ) 128 1ll
0 (1) 'l 19 109
11 2452 2139 (2)
0 (1) 96 9C
11 116 109
0 (1) 97 91
(1) 142 97
6
7
12
4
7
1
0
l
7
2
6
4
6
I
?
7
5
7
7
5
6
7
45
50
q2
61
16
t7
37
37
74
30
5t+
50
50
21
70
23
?5
51
)/
61
69
55
50
169
'124
140
148
157
'150
160
't62
136
200
156
156
150
165
299
13i
177
174
141
115
14?
112
115
146
LCSLCS OUP
9l
90
91
't15
97
101
97
108
101
105
lnl
103
96
79
79
100
98
9C
10?
10?
89
94
94
96
98
(1) The resuLt for one or both dererminations cas tess than five times the LOo.(2) The background resu[t ras more than four times the spike added.
I rFffiii;'uii*11,'',..
I
,',"16 Rev,Orr.,'r, d'3
I
QLTALITY . CONTROL REPORT
(I)Lancaster Laboratories Page:9of 1?
I
I
I
IA Thermo Analytical Laboratory
LLr sample No. 2538098stat 4(4A) (6-1otr) Grab soit sampl.e
NercuIes: Eacchus Pond
lcroup ilo.
Hercu I es,
52?739
lncorporated ' DE I
tSatrple safipLer,rDL Ulll IS
1672 zinc0.38 ms/ks
5935 Arsenic TR0.?4 mg/ks
6936 Setenim TRq.17 mg/kg
0159 flercury0.028 ms/ks
SLAIIK
Satch:9618457080050.80 J mglkggatch:951845708U03
[. D.
Batch:961845708003
x.D.
Batch: 96184571 1C02
N .0.
DUPRPD MS I{SO
72
75
ov
77
7t,
72
69
g/.
74
75
77
7r.
t5
71
n
73
98
92
91
92
32
84
78
7q
80
70
97
34
85
83
9?
32
57
B1
81
s?
77
ils
RPO
6
0
1
0
13
11
i2
5
5
6
15
11
14
IJ
'1C
7
1C
9
11
1l
6
5
92
87
79
77
76
t3
76
76
71
71
62
90
BO
73
87
76
75
77
78
75
LCS LCS LCS LIMITSLCS DUP RPO LOU HIG'd
0 (1) 108
0 ('1 ) 91
0 (1) 9?
0 (1) 92
51 149
19 149
s? 149
26 157
5 112
1? ',158
?3 174
1 172
20 124
32 1?9
46 1?3
J6 rOO
5 152
'l 230
40 113
35 180
2', 196
29 182
3? 119
3l '184
19 115
t,4 11?
2', 133
I
I
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t
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t
4688 TcL sU846 smivotatites soiI Batch:9618]sLB026
1 185 phenol.33. us,/ks5751 bis (2-chtoroethyt) ether
67. us/kg
I 186 2-ch t orophenot
13. uglks5754 1,1-dichtorobenzene33. ug/kg
1187 1,4-dichtorobenzenell. us/kg3755 1,2-dichtorobenzenell. ug/ks
4690 2-rethyIphenoL67. uslko
4691 Z,?' -oxyhis (1'chtoroProPane)
1 00. us/ks
469? 4'nethyl.phenol.
100.us/ks
11BB N-nitrosodi -n-proPytamine
67. ug/kg3757 hexach Ioroethane67. us,/ks
3758 ni trobenzene35. uS/kg3759 i sophorone67. uslks
5746 2'ni trophenoL67. us/ks
3747 2,1-d\nerhytphenol67. us/kg
1760 bis (2-chtoroethoxy) methanell. ug/kg
3748 2,4-dichtorophenot33. ug/ks'l'189 1,?,4-trichLorobenzene35. uglkg
5761 naphthatene13. ug/kg
N.0 .
I.D.
Lancasler Laboratoaet
M E M B g g 2d25Ne'rHollandPtke
7rcm i:;Lrji',ij':::,i,'i,u .u,,
(1) The resuLt for one or both de(erminations pas Iess than five tines the L00-
d1 I
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QUAIITY CONTROL REPORT
S.e .e.?,5e S,d€ ;or -:1o,a. ar'ta a: t.!ill6 .ie; lCll0i95
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(I)hemq*..,'*"gPg:*lgri.'
LLr sample No. 2538098Stat 4(4A) (6-10,') Grab SoiL Sampte
Hercutes: gacchus pond
QUATITY CONTROL REPORT
Pase: 10 of 12
j 6roup No. 522259i ttercutes, lncorporated - DE
I Satrpte SanpLeilDL UtitTs
4693 (-chl.onoanitine
100. uglkg
3762 hexach Iorobr:tadi ene
67 . ug,/kg
I 190 4-chl.oeo-f -methyLphenot57. u9lk9
4694 2-oEthyl.naphrhalenell. ug/ks
3763 hexachLorocycLop€nradiene110. uglks371.9 2,1,6- rrichLoroohenoL67. us./kg4695 2,4,5 - tr ichtorophenot
67 . ug,/kgJ764 2-chtoronaphrhaLene53. us/t:s4696 2-ni troani t i ne67. us/kg
3766 dimrhyt phthaLate33. ue/ks5765 acenaphthyIene33. us/kg
4697 3-nitroanitine67. us/kg
1 1 91 acenaphthene13, ug/k g
3750 2,4-dini trophenoL170. uglkg
119? 4-nitrophenot
ug/k94698 dibenzofuranll. us/kg
1 l91 2,4-dini rrorotuene67. ug/ks4699 2,5-dini rrototuene67. us,/ks
1770 diethyt phth3t ate67. u9./k93769 4-chtorophenyI phenyt ether67. uglksJ768 f I uorene33. uglkg4700 4-ni troani t i ne100. us,/kg4701 4,6-dini tro-Z-methyl.phenot
170.us,/ks
MS
RPO
LCSLCS ouP
43
82
7B
6?
B2
82
79
75
6U
56
73
63
75
76
9C
B5
B]
BL
79
76
66
LCS LCS LIHTTSRPO LOIJ HICH
80
7-\
71
17
31
e0
79
36
71
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4689 TCt SU845 SmivoLac i tes/Soi L Barch: 961BlS,-8026
N-3.
N.0.
N-9-
N -9.
li-0.
N.D.
N-0.
N.D.
N.D.
N_l-
N.0.
N.D-
N -9 -
N.!-
N.l.
N.!_
!.1.
15
87
86
'16
90
39
35
78
37
81
40
78
65
77
8C
S9
89
3B
87
s0
62
7?
5
9
13
10
7
11
10
8
10
5
10
9
8
6
I
7
10
10
1C
7
1
9
17
21
2?
23
1
37
39
60
55
179
75
59
n
7t
79
79
7/.
59
66
116
116
117
123
100
111
151
118
141
112
115
7 143
47 145
1 191
1 13?
?8 131
l9 119
50 r58
1 114
25 153
5e 121
IA 11)
1 181
Ldn(;5i:r LJoof:ic( e,
2d2-q Ne,to Ho 1...1 P,k.,
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Lancasler Labora(oile5
M E M B E R 2425NewHollandPrkerl6in hiffi ,:::;r.,u,u,.,,
Batch: 96'1840516320001A
II
iGroup No. 52?7--(9
i Hercul,es, lncorporated - oE
I
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71 84
81 9?
83 91
74 76
75 8l
74 79
80 90
73 80
e3 92
e5 97
55 58
77 83
93 r0l
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8] 9?
fi80
77 85
s2 89
83 91
79 86
QUALITY CONTROL REPORT
LLI sample No. 2538098
Stat 4(44) (6-10'r) Grab soil. Sampl.e
Hercutes: Bacchus Pond
LCS
LCS OUP
13 80
'll e?
263
'10 77
977
11 86
977
10 91
1.2 95
568
730
9 101
885
11 103
10 B0
10 86
10 7A
882
933
875
100 100
Page: 1t of 1Z
LCS LCS LIr,4tTS
RPD LOU H[Gi{
J6 t\t
53 127
1 152
11 176
54 120
27 113
5s 133
1 118
26 137
5? 115
1 1t2
1. ?62
33 143
8 158
17 ',168
1 146
21 159
'l'r 153
17 163
', 171
1 227
1 ?1e
0 100 101
satrpte SanpleMDL UII I TS
5772 {'ni trosodiphenylamine67. uglks
37"15 4-brmphenyt phenyl ether100. us/kg
324 hexachtorobenzene'100. us/ks
1194 pentachIorophenol
170. uglkg
3275 phenanthrene33. ug/kgfZ6 anthracene35. uslkg
4702 carbazote13. uglks3777 di -n'butyl. phrhaIate
55. us/kg3r78 ftuoranthene13. uglkg
l l95 pyrene67. ug/kg
3780 butyt benzyl Phtha[3te67. us/ks
3783 3,3' -dichLorobenzidine
130. uq/ks
3781 benzo (a) anthracene33. us/kg
01 11 lioi sture0.06 Z by ut
HS
RPDBLAXK
r,1.0 .
I.D.
N.0 .
H.D .
N .C.
N_9.
I.9.
N-9.
N .9.
N.D.
N.0 -
I.0 .
N.D.
3784 bis (2-ethythexyt) phthatate
67. us/k.g N.0.
3782 chrysene15. ug/ks t/ .D.
5785 di'n-octyl phthaLate
67 . uglkg rJ.D.
3786 benzo (b, fIuoranthene
67. us/kg tl.D.
3787 bmzo (k) fLuoranthene130. ug/kg N .D.
3788 benzo (a) pycene
67 . ug,/kg N.D.
3789 indeno (1,2,3'cd) pyrene
67 . uslks N -D -
3790 dibenz (a,h) anthracene67. uslkg N.D.
3791 benzo (ghi) Pery(ene
67 . uglkg N.D.
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(I)La ncaste r Laborato ries
A Thermo Analytical Laboratory
LLr sarnple No. 2538098Stat /.(4A) (6-'10',) 6rab Soit SarJoLe
Hercules: gacchus Pord
4593 IcL votatites by 8240
4688 ICL sU846 Senivota(ites Soi t
4589 ICL Str846 Semivotati Ies/Soi L
t,
I Group llo. 522IJ9 :i Heccul,es, lncorporated - OE i,lrl
SURROGAIE SUIttHARY
S'JRROGATE RECOVERY i
d4- I,?-DCA 95
cg - to l.uene t5Bt8 9n
Phenol. -d6 75z-FLphenoL 572,4,6-rBP 77
Ni trobz-ds 3lz-Fbiphnyt it,Iphenytcii4 58
SAIRROGATE LIiIITSLCU HIGH
70 12..81 1177t 1?',
24 11325 12.19 12?
23 120i0 11513 137
LancaSter Laborator et
M E M B E R 2425NewHollandP'ke7Xm ;1ffi '::: ;f,'i,u,u,,,orro,'r,'l}
QUAIfTY CONTRCL REPORT
See reve.ie srde for erpldnai on oi 5"-coli anc abbre r ;: afs
(iI)Lancaster Laboratories Page:1of 14
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A Thermo Analytical Laboratory
LLr sanple No. EL 2531997
col.tected: 6/27196 ar 08:25 by BR
suBni tted: 6/2El96 Reportedz 8/ 1/960iscard: 8/ 9196
sed.,/Equip Rinse Grab lJater sanpte
HercuIes: Bacchus Pond
SE0ER SD6#: tlBP0lEB*
I A".ount tio: 06716
i ttercutes, !ncorporated - oE
i Envi romenta r Af ia i rs
I tli tmington :E :9894
AS RECEIVED
P.0.
CAIIIO. AIIALYSIS IIAHE
45C? TcL votatites by 8240 - Uater'172? That t im1713 Atwinun
17t+4 Anr i rcny
1716 Eariu1747 Seryt t iu17tg Cadmim
1751 chrmium1753 copper1i54 I ron1755 Lead1758 llanganese1,761 NicreI1756 Si Iver177? Z i nc7035 Aesenic TR
?A36 seLeniur TR0?59 i!ercury0937 TCL Pesticides in Uaters4678 TcL su846 ssrivolati Ies/uatersL679 TCL sUB46 Smivotati Ies/Uaters
1 COPY
1 CCPY
I,IET HOO
DETECTIC]I L!I.iIT U}{ITS.ri:.,ri;.r,;lii45s1r!Is ..: :
"::i i.:.:.:..i.rri'.":.:i .r .'
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See Page
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IO HercuIes, lncoroorated
ERr4 - Rocky l{ountain
ATTH: tir. Joseph l(el Ier
AlTr,l: Yr. Brenr Rabinson
ouestions? Contact you. CI ienr Services Repres..ntarive
RacheI L. Kceaflcr a: (i:7) 65o'8ce
03:22:29 D 0(rr2 15 REP 12ar,-a$ 52?727310 55_00 DC130700 ASRtln
RespectfuL Ly subfi,i tred
Rarcna V. Laynan, 0roup Leader
!CP !{etals/Le3.iatcsLancaster LdboratoileS
M E M B E R 2425NewHollanoPrkeTKfiI i:;1fu,*':::;i,,iuu,u.,iif
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(iI)Lancaster Laboratories Page: 2 of 14A Thermo Analytical Laboratory
LLI Sample No. EL ?53i997Cottecled: 6/?7/96 at 0B:25 by sR
Suunitted: 6/?8/96 Reportedl 8/ 1/960iscard: a/ 9196
Sed.,/Equip Rinse crab lJater sampte
Hercutes: Eacchus Pord
S€DER SDG#: HBP0IEBr
CAT
TCL Votatil.es by 8240 - Uater
1258 Ch t ororethanei?57 Brorcmethane3192 Vinyt ChLorioe1494 Chtoeoethanei497 lilethytene Chl.oride3198 Acetone3499 Cafbon 0isutlide3500 i,1'Cichtoroerherle :
3501 l,'!-0rcnl.oroerhane1503 Ch L oroform1504 1,2'Dichl.oroerhane
0i16 a-Butanone1505 :, I, l -Trichloroethane
5506 Carbon IetrachtoriCei507 YinyL Acetatr3508 6ronDdi ch Loromerhane1509 i,2'CichLo.opropane3516 cis''l,l.DrchLoroo.opene3511 Trichtoroethene3512 oibromochloronerhane :
3515 Eenzene ..1510 rrans-1,J-0ichIoropropene35'!3 Erorcform
3521. 4-IethyL-Z-pentanone
1520 2-Hexanonel5?3 Tctrachloroethene
15?l 1,1,2,2-Tet.achLoroerhane
35?1 ToIuene3525 Cntorobenzene3526 E thyI benzene35?3 sryrene15?9 xytene (totaL)
5780 trans-1,2-Dichtoroethene l6268 cis-1,2-0ichi.oroethene
i Account No: 05716
I Hercutes, !ncgrporated - 0ElEnviromnrai. Af iarrs
i ui Lmington rE '19894
AS RECEIVED
14EI HOD
11ggli(1gl!,.11 DETECilfT- L!HlT UNIIS
P.O.
Ret.
Resoec tf uL !.y Submi ttedYicreIc- ycctarin, B,A.
Group -eaCer, GC/r9 Votatites
.rL;0;
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ouestions? Cont3cr you" C1. ienlRaciel L- Kreatner
Servl ces Represen:ai r ve
at (717) 6)5-2130
Lancaster Laboraiorier
2425 New Hoilrnc Prkc
PO Box 12J25
Ldncast€. Pl I 1505-:{.25
717-656-2100 F.x 7)t 6t6 1621
D,
*", ,nr,O,nt ?a,$lee':. :r:e lce r:' :, c, ara\ton oi 3' t- ools and ;oorevrdlrons
(I)Lancaster Laboratories
'11
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LLf sample llo. EL 2531991cot[ec!ed: 5/27/96 at 08:25 by 8R
sutfnirted: 6/28/96 Reported: 8/ 1/96Discard: A/ 9/96
sed./Equip Rinse Grab uater sampte
HercuIes: Eacchus Pond
SEDER S0G#: HBPo1E8*
: Account xo: 057!6
I Hercutes, lncorporated - DE'€nvirorenral. Af+airs
, ,,ti lmingron 9g '19994
A Thermo Analytical Laboratory
Page: 3 of 14
all
7)16 ReY ,OrrOrn, laJ
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CATNO. ANALYSIS IIAI'(E
TCL Pesticides in lJaters
1600
1601
1601
1602
1604
1605
1606
1616
1610
i607
16',I1
16r5
'1603
1617
1609
09t3
1Bo0
1i6 1
136216il
1618
15'19
1620
loJ !
16??
1623
1624
16?6
AS RECE!VED... llETlloo
.t::::: l|:, ::t,:'i:lliESUqISil ::t,t, oETEC'I I 0x L I tl t I Utl I IS
at (7'7) 656-2i00
Ouestions? Contact your CLient Services Repfesen!ative
RacheI L- K.earner
Respectf uI r-y submi tted.leniier E. lless, B.S.
croup Leader Pesticides/PCBsLanca5ler Laboratofles
M E M B E R 2425NewHoilandPrke
7I6m i}ffi '::: ;ii,u,u,u,,sel 'e,. e'se s Ji icr prcrdni: c^ 1i i/-ao ) d'd ;bo,e,rdt o15
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(I)h+nm*stLg?g'"*gr,"Page: J of 1zr
LLr Sample No. EL 2531991Cottecred: 6/27196 at 0E:?5 by 0R
Suhnitted: 6/?3/96 Rcportedr g/ t/960iscard: 8/ 9/96
Sed-,/Equip Rinse Grab Uater Sarnpte
l{ercutes: Eacchus pond
SEDER SDG#: ttBPo'lEB*
CAIilo. AHALYSIS [AtitE
ICL SU846 Semivolati Iesluatefs
3913 phenoL3867 bis (2-chl.oroerhyl.) ether3874 2-chl.orophenoL3383 1,3-dichl.orobenzenel3B4 1,(-clichtorocenzene
3882 !.2-dichLorobenzene
4630 2-rnethyIphenol.1081 2,2,oxybis ( l.chtoropropanel . lt,t32 4-methylphenot
391 5 N -ni rrosodi -n-propytami nel9O? he.\achtoroernane
39 !0 nr rrobenzene1tA4 i sophorone3911 2-nitrophenor.3590 2,4-dimerhyLphenol.i866 bis (2-chIoroethoxy) merhane3SE5 2,1,-dichLorophenot39?1':,2,4-rrichLorobenzene3906 n6ph thi I ene5871 4-cnLoroaniLlne3900 hexachloroburadiene .387? 4-chLoro-f-rethyl.phenot :.3905 2-ftethytnaphrhal.ene3901 hexachIorocyclopentadiene
1?Z? 2,4,5-tricrl.orophenoL3ill5 2-chtoronaohrhatenej';07 2-ni troani L r nei391 dimethyLphthatate3353 acenaphthytene
Ii Account llor 05716 P. O.
PeL.HercuLes, lnccrporated - DEEnviromcnr:i, AffairsUiImington !E :9894
AS RECEIVEO, XETHOO
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Services Repnesental ivear (7'7) 656-21C0
Ldncatler LaoorJioftes
M E M B E R 2425NewHoll.rndPkc
TXTit i:;iffi 'r,;: t,'l7,u,o.,
RespectfuL Ly Su5mi tteCclrfis::ne'.1. Ratclifi, B-S.
Cfoup l_eadc., ccl1,!9
Seerever5esroe'ori.cdralono::.-co'sandabbre,/r6lons 2216 Rev,Orror95 d3
A Thermo Analytical Laboratory
LLr sample No. EL 2531997Cotlected: 6/27/96 at 08:25 by BR
subnitted: 6/28/96 Reparted: 8/ 1/96oiscard: 8/ 9/96
sed./Equip Rinse 6rab Uater Sanple
Hercules: Eacchus Pond
SEDER S06f: HBP01€8"
CAT ::i::i::::i::tt:::i:tit:;UO. ANALYSIS tlAl4E :.:'::.:r:
f CL SU846 Semivolat i tes/tJaters
A9 RECEIVE)
tE'StjiIS;ii, DETE:Tl:N r_lF! l' UllllS
gage: 5 of 14
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P.O.
1908
3e57
3895
391?
5394iqos
1e,87
3875
3898
3909
4683
1914
3869
3399
391 6
i859
/+b84
3880
3897
l9i9
1870
3e85
3M0
3853
3876
le96
1861
3S52
lB54
39C3
335l
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ciibenzofuran ..,.i.t:,::.:'.:;;: ::.1,:' [,.i..,' :. ':g/'"
2,1-dini trototuene rli'ti:::::'iii1.::::l ::.,:.1:::|{.1...: i- 'r9/1-
a,6-dinitrotol.uene l.::l:::i::.'::.: 1. u.!.: :. !'-rli
diethyl. Phlh3Late :l:il;i:llir::,i:::l :i: :N:-]..:: l. 't)/'.4-chtorophenyl phenyL elher i::i.,.li.:.,1:,;:i::::;::.:.r:i ,rt;11.; !. !g/ I
f tuorene :i:t:t:i::,1:i;::t::.:::rt:: .:li.D. ?. t9/t-
4-nitroaniline ,!!"1':'ii:::i'ill:,i.1!: ':,Vii': i q. ':9/t-4,6-diniro-z-inethylehenoL .:;,t,t:t:,iil::ir;:;,l;it.: r:i.:. -1i. :9/l
r{-nilrosodipheny|anine :r.::'.i:il,,iil;,ii:li.iii,..,1r.,}...: t. !9/:
4'bromophenyl- phenyi elher 'r.i:i!":r,:i:i:l::'lii'1,,;:1fl.it' t'. ug/t'
hexachtorobenzene .,::ii'; ,',:i:l l.i::,::: U.?. " 2- !9/ i
pen t ac h I or ooneno t , i:,]:il:,t::.,'::i l!''iii!:.;i.'rl;. f :. , :' ? - !9,/ L
anthracene !i.it::!i,",i:ij;:i.ii:::l :,til,). ,1 :. us/l
carbazote :r::l;:il1::i:it.jijij:::r'::::,ir:t''..: 2. !q/l
di -n-butyt Dhthatate :':,tiiiili,i:iiiiii:.,::i",i:fi':'!.: ':9/t-
f luoranthene ';:'.1::lii:::;::i:i'. ,r:',: :,:i;::*: ' :: :' ug/ t'
pyrene :.:::i,;:rlii:tiil:l::r:}I.il: :. ue/'i
buryt benzyt phthatate li:ll:!l:.:illi::;l: i:::i ,i,\r,r. : L. usl',
3,3'-dichLorobenzidine ::i,:i:iiitt:::,i:li ::L:::..,1.r. I t. ug/i
benzo (a) anthraccne :iit,tli:,,i;ii::i:tt;li i::l:i :ilt.r... 2- uslr
bis (2-ethy(hexyt) phthalate ,l'':!': .1r.,':,:,,.i l:i:.:':ft::;. t'. !9/'.
chrysene l:i;!.;,'.,, :1;,'1,'! "1, ';v.a' r 2. 'Lg/ |
di-n-octyt Phthalate '.!liir;;:,,11:,i:li'i:ll':r:l:I.r' I l'- u9/!.
benzo (b) f luoranthene :i1::i::i;liri:;::,::":'i:l |J-!', t'- u1/t'
benzo (i) ftuoranthene l.:1,;ii:l:rl':.iri:'.li'::!'li,:'r,, !,. u9/'.
benzo (a) pyrene , '::': :': i,l"ir. I'1.r." t . us/.
indeno (1,?,3-cd) pyrene ::;: r:::', r!.:;': ll;f .r 4. !9/ 'dibenz (a,h) anthTacene ::,:l; :'i . ',\.:. (. rg,/'.
benzo (ghi) perylene l,:..'::,1 ..',r':..ll.l-' a- ug/'.
oue to insufficient sanpLe, the quantitatif,nr.inrits for the C:/!'1S
senrivotati Ie coupounCs pere ralsec-
ouestions? Contact youl Ctient Services Recresenritlve
Rachel -. Krilaner ar (7'7) 656-?io'-l
Lan(a5ter Laoo.atofie5
M E M B E R 2425NewHollandPrke7Xm i;.h1i;'::: ;ili,u,u,,
Respecriul ly Submi tted
christine \1. Ratcli f 1.
C.ouo l-eeC!r, GC/l4S
lEa reverre:rde io' srcianalon oi iymools 6nd abbrer16!on5
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(D Lancaste r Laboratories Page i 6of 14A Thermo Analytical Laboratory
LLI Sample No. FL ?53-7991CotIected: C6/?7/96 ar 08:?5 by Gt
Subflitted: 06/28/96
Sed./Equip Rinse crab Uater sampl.e
'Account |lo: C67'6
i iiercuIes, !ncf,roora!eC - 0E
Environn[ntel Afiairs
, liini^gton !E iglJqz,
HercuIes: Bacchus Pond
S€DER S0G#: HBP0lES*
CATNO AIIALYSIS XAME
4592 IcL r./otarites by 9240 - Uater
1722 Thattiurn1741 Al.uminm
1 744 Anr ircny
1 746 Bar i ur1747 Beryl. lim1749 Cadmiw
1 75 1 Chrorni un
1 753 Copper
i 754 I ron
1 755 Lead
1758 ltianganese1751 I'l icket1766 sil.ver
177? ztnc1818 UU SU846 ICP Digesr (lot rec)7015 Arsenic TR70J6 Seleniun lR
0259 l,lercury57ll uu srJ846 H9 oigesr
0817 Uater Sanpte Pest. Extraction09J7 TCL Pesticides in uaters
0811 8XA Uatef Exrraction1679 lCL SU8(6 Searivotati Ies/l,Jatersc679 TCL 9!8(6 Sffiivol.arir-es/parers
ANAI.YS I9TR!AL DAIE AND TIHE
, t)7/03/96 03t,_\
1 07/15/95 A3??., 07t:5/96 A3??i 07/:5/96 032?1 C7/15/9o C32'r'1 07,t15/96 C3??. 07/15/96 A32?1. C7/,,5/96 A3Z2', D7/1-</96 0i??", 7711.5/96 0i2?'. 07/..5/C5 C3??1 !7/15/96 C32j1 1.7 taa tot, l1).
' .'?/1< /(1A \lt,1 a:./i 5,/9, 012?: 17,r.1/Cl. lrr)
i ai,/15/95 ci?z', c7/15/96 C3??
' !7!43/96 185C1 !i!12/9o ?',2?
., 07/01./96 133C
' !7/A6/96 065e
1 07/C?/q6 C9i0
" t7/13/96 C9i4": iz/D3/96 !9'.1
AIIAI. YST
Susan A. l{cMahon
Donna R. Sackett
Donna R. Sackert
0onna R. Sackerr
CLrnnn R. Sacke:r
0onna R. Sackett
0onna R- Sackert
Conna R. sackett
Donqa R. Sackert
!onna R. Sackerr
oonna R. Sacke:t
0onna R. Sackettgonna R. Sackerr
0onna lt. Saciel!
fonna R. S.rckert
Christine il. Conlin
!onna R. Sackett
Conna :i. Sacke:t
Iel.ti S. l,,larkaryan!e'rli S. !arkaryan
l,laccie A. NataIe
Do!!l.as C. Seitz
l'lari a A. Davenporr
Stephanie I'1. Shenk
Sre)hanie l'!. Shenk
iYETHOD
slJ-346 3?408
su-346 6010A
SU-346 5.r10A
su-346 6at,_1A
SIJ-94o 6ilOA
SU-3r,o 6ll0A
Sl|-316 6!10A
su-846 6J'ltA
s\.J-3c6 5al0,i
S'J-946 orllCi
su - 346 60',rCA
s\r-3(6 6lloA
lll - E4o 5;r 1 aA
s',i-3t,5 6JlCA
Slj-94d ]iCi^
S!,-g1o c- l0A
s';-946 6llrlA
su-846 7L,7lA
SJ- 3(5 7i70A
sq-846 3;'108
sL'-3.i6 lil0B
s,r-?(6 It:713
su-3(6 8?7!3
LancaS(er L;ooraior e3
M E M B 6 g 24251'1e'rHolar:oF,<e
7lk-flil f;ii,,;",n,t:: ti,,;..,...:3
LABORATOP,Y CHF.ONICLE
Se: rererre srde for eic;^j_ a. of symbol5 ano abbrerratroas 2216 ae,. l0/J0/95
LLr sample No. 2531991
sed./Equip Rinse Grab lJater SifilpLe
HercuIes: Sacchus Pord
crouo No- 5?i727i.erc!tes, :ncorirrated fE
Pa-oe: 7 ot
LCS LII',IITSLOU H ! Gil
(iI)Lancaster Laboratories
A Thermo Analytical Laboratory
it
ll
T
il
T
L
I
T
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RPD
!ls
!!s
sampI e
I'(D L
Satrp! e
uxlts
DLP
RP'
LC9LCS D!?SLAN(
Barch: I9o184'!AA4592 IcL Votatiles by 8240 - uater
'1258 Ch t ormethane3. us/ t
1257 Ermmthane3. us/ t
3492 vinyt Chtoride
?. uo-/ L
3494 Ch Ioroethane3. u9,/ L
3497 tttethy t ene Ch t oc i de
2. u9/ t
3498 Acetone6. us-/ L
3499 Carbon Disutfide3. u9/ l
35C0 1,1-0ichtoroelhene
73 68
83 31
90 52
57 51
tc? 98
67 9l
'i q3 10c
115 109
c5 10e
6t, 97
111 ',! 10
99 1C4
9Z :9:
97 i01
196 105
e7 99
g? 96
1 Cr, 1 01,
9' '02
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l
l0
4
7
3
t
1
41
?
,1
?7
5
?
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c
12
u9./ L
3501 1,1-0rchtoroethaneZ. u9/ t
3503 Chtoroforrn
, . unr,
3504 1,2-0ichtoroethaneZ. uslt0316 2-Butinonel. us/ t
3!,05 1, 1,'l -Trichloroethane
1.
!
t-
1.
l.
u9/ t
1906 carbon Tetrachtoride1. uS/t
3597 VinyL Acerate?' us/[
1503 Ermodichtoromethanel. ug/L
I5D9 1,2-DichtoroproPane
us,/ (
i516 cis- 1,i-Dichlorcpropene'l . us./ [3ii'l TrichLoroe!hene1' ug/L
1512 Dibrcuocirlorotnethane2. u!/l3i1Z 1,1,?'I rlch!.oroethane?' uglt
3515 Benzene
ug/ t5i'10 trans-1,1'Dichtoropropene
u9/ t
Lan(asler Laboratofie5
M E M B E R 2425NewHollandPrke
TIKffi ylii#,i:i;'::: ;r;:,.,,.,d'; I
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QUALITY CONTROL REPOR?
5ee reversi ;t:a:'.'a<oialaia^ li ;/nbo15 aad 6oarevrdlons 22 I5 Rer l0/10/95
LCg LCSLCS DUP QPD
!s
RFD
DL'P
RP9
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LLI sample No. 2537991Sed./Equip Rinse 6rab lJater SafipLe
Hercutes: Bacchus Pond
i
tt, Grouo xo. 5??7?7
i HercuLes, lnrorporated - DE
I
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!s)
7'. 9C
6" 9l
6'Z 95
1C6 'C5
ta vq
: c5 '!5
:!: 'c'l
',a? I f2
: c8 :09
1C4 99
(1) 101 101
174 -77? -7?9 (?)
( -1 ) 1C5 .46
(1) 97 97
(.1 ) 9!, 95
0 (") 78 ?9
0 (r) -?1'. .19',1
174 -151.3 -1!.!_1 (?)
0 (1) 92 93
0 (1) 59 a1
0 ('1 ) 9!. '5(1) 99 'Cl
Page: 8 of '' l,
LCS LIIIITSLO'J H I Gi{
(iI)Lancaste r Laborato ries
A Thermo Analytical Laboratory
SatrpLe SamoteMCL UII I TS
35'!8 Brmform1. ug/t
3521 4-Methyt-?-pentanone5' us/L
5520 2-Hexanone7' ugll
f52? IetrachIoroerhene1. uslt
3521 1, 1,2,2-Tctrachloroethane?' ug/ t3521 ToLueneZ. ugl I
3525 ch I orobenzene1. ug/t15?6 Ethyr.benzene?' ug/t'
3528 Styrene,. ,nr,
3529 xytene (total.),. ,n^
5780 trans-1,2-Dichloroerhene2- uglt
626E cis-1,2-Dichtoroethene2' ug/ t
1722 Thaitiw
174 . us/ t
1741 Atwinm57. uslt
1744 Antircny15. uslt
1746 Baeim2.2 us/l
1747 Beryttim1.3 ug/t
1749 Cadmiw?.7 ug/ t
1751 Chromiw4.3 uS/ t
1751 copper3.8 ugl I
1754 Iron5.9 uglt
gLAI{K
N.9.
Ii-l-
li.).
!i.f.
),J-t-
I1 .f.
Batch:961921843C02r.).
8atc5:96:921849J02Ii.5.
Batch:961921849i02
Barch: 96192'1843-.02
N.0.
Batch: tb19?1848102
0.0C1o J rE,it
Eatch:96192'l:48-1C2
' li.l _
Batcr: 9619213480C2
B6tch: 96192144310?!.!.
Eatcr : 96'9213,',ll!!2
0.C6C7 J ms/t
Batcl.:9ii92181,Sa02
N-D.
Eatch:96192131.3102
\.4 .
Eatcr:95i1218131!?
N.J.
8.1tc:: scl9213.i31f2
1755 Lead
1e.ug/ I
?4
36
/.3
z
0
0
?
1
0
5
4
': 102
24 108
1 !07
1 100
093
197
? to7
9 101
31 111
1 102
I 103
1 1.04
1 '10C
80 120
80 i?o
80 120
80 1?0
80 120
80 120
80 120
80 120
80 120
80 12C
80 120
80 1?0
80 120
'1758 l{aoganese
I ,r, n,l*:, ::1:
1766 si tver1.6 us/ t
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(1) Ihe resutt for one or both delerminations cas (crs than five tin)es the'-O0"(2) The background resutt Has more lhan four tirncs thL'spixe added.
Lanca5ter Laooratones
2425 Ne'.v Hrlla.d P,ke
PO Bo, I2J:5
Ldrlca5!?,. Pl 1 / oa5-242')
717-656-2100 Fr( /17,)5.laBl di
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QUAaITY COITTROL RITPORT
See re,re.s' ! c: ')i irpidna! oi 2i tymooi5 and aboreuat on!l2r6 4e', l0/1085
(I)Lancaster Laboratories Page: 9 of ',4
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LLI sample No. 2531991
Sed./Equip Rinse Grab uater gntrpte
HercuIes: Bacchus Pood
Group llo. 523727
Hercutes, :nco.porateC - DE I
]I
I
Sampte Satrptel'rDL Ulr l TS
1V2 Zlnc12. uslt
7015 Arsenic TR?.7 u9/ t
7056 SeLenium TR
?.7 us/ t
0259 Mercury0.0/-3 us/ t
BLANK
Batch:961921948002
ti .D.
Batcn:96'192184BC02
N.D.
Earch:96'192',!848!0?
N.D.
Batch: 96i3457-1130'lN.!.
Batch: 96'133C005A
0uP
Rp9
0 (1)
0 (1)
0 (1)
r!s,
1C2
79
tts
RPO
LCSLCS DL'P
!-cs Lcs Llt'rI1sR2O LOU H!G!]
80 120
80 120
80 '120
80 120
1n1
i01
79
5
1
103
103
103
9l
9C
10'1
ic!
92
7?
92
B8
90
112
97
95
97
98
9t!
103
9'l
1 I
il
t
0917 ICL Pesricides in Uaters
1600 Atpha BHC0.002 us/ L
1501 Be!a BHc0.008 us/ L
16C3 Detta BHC0-005 u9/t
1602 caflna BHC - Lindane
0. C02 ug/ L
1504 HeptachLor0.005 us/ t1505 Atdrin0.004 u9/t
1606 Heptachtor Epoxide0.001 ug/ I1616 EndotuIfan I0.0Ci us/ |
1610 Dietdrin0.005 u9./t'1607 00E0.005 us/liolt Enortn0-055 us/t'1615 EnclosuI f an I I0.01 ug,/L
16CB DOD
0 .007 u9/ t
16'17 EndosuLfan suLfate
0 .0C7 uS/ l-
1609 D0T0.008 u9/ t
0918 Endrin Ketone0.00/. ug/ t
1850 I'terhoxych !or0.01 u9/ t'1361 Atpha Chto.dane
0.005 us/ [
1362 carnra ChLoedane0.00t u9/ L
85 86
96 I5
97 97
e5 85
75 76
7g 76
23 83
et 9A
119 Ii4
90 91
9e 39
92 q3
9(. 9?
1ti2 '.cz
91 90
e5 86
0
1
0
0
,]
4
0
?
0
0
J
'1
1
0
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?
1
2
0
67 1??
7t+ 1?D
69 126
66 120
54 1?0
4? 120
6!, 120
60 120
66 120
60 120
73 129
67 120
67 121
51 128
71 1?0
76 1?0
57 ',!10
75 1?0
75 120
t
t
I
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t
('l) Ihe resuLt for one or both determinations las Iess rhan;ive tines ih?'.94.I
LnnCaSter LabOratOile5
2425 New Holland Ake
PO Box 12425
Lancasrer PA 17505-2d25
717-555-2100 Far 717'o5o.26al dil
I
I
QUAiITY CONTROL REPORT
MEMBER
5ee rever;e i,ce 'or erolan6l on fi symboi5 dnd 6bbrevralronj 2216 Rev l0/i0,/95
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(I)Lancaster Laboratories
A Thermo Analytical Laboratory
6rouo No. 5?2727He.cuIes, !oco.porated - DE
Page: 10 of ':4
LCS LIr'!tTSLOIJ ITGH
LLI sampLe No. 2531997S*j./Equip Rinse Grab Uarer Safipte
HercuIes: Bacchus Pond
SatrpLe gatrpLe
MDL UX] TS
1613 Toxaphene1. ug/t
1618 Endrin AtCehyde0.01C uglL
1619 PC8-10160.09 us/ tlo20 PcB- 12210.2 ug./ t16?1 PC8 - 1212
0. C9 ug/ t
1 62? PcB - i ?420.05 ug/ t1627 PCg-1?18o.CZ ug/t1621 PcB-',1?540.06 u9./ L'!626 PC8- 1260
0. ,.r7 ug/ t
3f15 phenot?' u9/ t3867 bis (2-chtoroethyL) ether2. u9./ tJ974 ?-chLoropheoot2. us/L3583 1,3'dichtorobenzene2' ug/l5gS1 1,4-dichtorobenzene?, usl t5932 1,2-dichIorobenzene2. usl t(680 2-n:ethytphenol.1- ug/L4681 2,2'oxybis (1-chLoropropane)t,. ug/ |
4c82 4 -merhy L pheno l.1. u9./ ti915 lJ-ni trosodi -n-peopytarni ne1' ug/tii0? hexach t oroethane
4.u9/ ti910 ni trobenzene?' ug/t1iA4 i sophorone2. ug/l
591 1 2-ni trophenol
ug/ L
N-!-
ri-1.
ll.l-
N.!.
N.1.
[.1.
ti.t.
\.D.
N.f .
N.!_
t(.t
Lancat!er Lacor.{ciLe5
M E M B E R 21:SNe',,rcla,,dP,krtkm i:r'i#,::;,=:: ijj1,u,u,,
DUP
NPD
tTc rac
'.CS 'UP RPO
itsI'rs r,,sD RPD
tt659
8 !AXK
[-9.
N.9 .
N-f-
:.i-l-
li.!-
N-l-
li,D _
4678 lCL SU84o Semivor.ati !.es/uaters satcs: 95184tAl025
i9 47
91 91
99 99
79 9?
g! 83
79 ZZ
9' !?
57 63
e3 3l
Ic 1'.\
72 78
97 97
1CC i00
9t 95
311
188
185
568
37C
171
177
?64
07e
4 103
251
091
097
192
5 112
1? 153
t) tJ4
" 17?
20 12t4
i? 1?9
16 166
5 152
I <)U
40 113
35 180
21 196
29 192
QI-IALITY CONTR.OL RSPORT
al}.
221. R€, l0if0l95 t;
Sarple SatrpteitDL UII I TS
3890 2,4-dinrethylphenot2' uslt
3866 bis (2-chtoroethoxy) methane2. ug/ t
3885 2,1-dichtorophenoI4. u9/ t
3921'!,2,4'trichtorobenzene2. u9/ t
3906 naphthateneZ. ug/t
387'1 4-chtoroani t ine4. uq/ t
3900 hexach t orobutadi ene?. ug./ t
187? 4-chLoro-l-rethylphenoI4. u9/ t
3905 2-methytnaphthaLenez' u9'/ |
f901 hexachtorocyctopentadiene6. us/ t
3921 ?,4.6-trichtorochenol.2' u9/''3922 ?,4,5-trichLorophenoIZ. ug./ t39IJ 2-chLoronaphthaIene2. ug/ l.
3907 2-ni troani L i ne?' us/t
3891 dimethyt phthal.ate6' us/t
3858 acenaphthyLene?' us/t
3908 3-ni troani t ine2. us/ll957 acenaphthene
z' u9/ t
3891 2,4'dini trophenot10. uslt
3912 1-ni trophenot10. us/t
3879 dibenzofuran
2. ugl L3894 ?,4-dini trototuene1' ug/t
3895 2,6-dini trototuene?. u9/ |
' Grcup r,lo. 52?727
i fieaautes, Icco.porated ' !E
66 70
90 90
s6 86
79 g1
72 7n
b5 69
91 93
g5 t7
'',: 53
99 37
99 B8
91 e0
97 97
i2 3l
92 9l
e0 8c
93 9l
89 .99
9-\ 96
99 ',rCC
Page: li of '.1
l-cs Lt!it'isr_ou it I G;l
32
33
19
1L
?1
17
2?
2B
1
37
i9
60
5l
1
7 1.t3
t 7 1/,5
1 191
1 1l?
23 1i]
39 119
50 153
(I)La ncaste r Laboratories
A Thermo Analytical Laboratory
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LCS LCSLCS DUP RPO
DUP MSRPo l1S l'{SD RpO
LLr SampLe l.lo. 2531991
Sed./Equip Rinsa Grab Uater Satrpi,e
HercuIes: Bacchus Pond
4579 TCL S!r345 semivotatiIes,/Uaters Eatch: 95184rM026
BLINK
N.0 .
N.0 -
ll .9.
x-c.
N.9 -
N.9 .
N-9.
N.D.
N.' .
[., .
N.0.
N .5.
N.D.
N .0.
N-!_
N.! .
N.9.
N .0.
N.0.
r,1.9 .
N.D .
7
0
0
3
0
2
7
1
1
5
l
'I
1
0
1
?
1
C
10
5
1
,1
1
65
86
B4
70
81
71
15
9'1
8C
41
91
9C
83
95
?5
B6
87
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B5
91
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Lancasler Laboralone5
2d25 New Hoiland Prke
PO Box 12n25
Lancaster. PA 17605-2425
717-656'2100 Fax [phone]
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QJAAITY CO}{TR.CL RE'PORT
MEMBEFl
5e: 'evp.;e t,oe ior :,o,.ndroa oi lynot s 6nd aobr:.. ar oas
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(I)Lancaste r Laboratories Page: 12 ofA Thermo Analytical Laboratory
LLI sample No. 2537991sed./Equip Rinse Grab uater sa[D]-e
Hercules: Bacchus Pond
Group \o. 52:727i!ercJtes, :.cc.Dora!eC - DE
SarpLe SamDteilDL UrllIS
1887 diethyt phrhaIate1' us/t3875 4-chLoropheny( phenyt ether4. us/ t3898 i Iuorene?' us/l
3909 4-ni troani L i ne1' ug/L4683 4,6-dini tro-?-merhytpheno(10. us/l39i4 N-ni trosodiphenyIaflrine1' uglt
3869 4-bromophenyI phenyI ethec4' us/t3899 hexachlorobenzene?' ug/t
3916 pentachLoropnenot2. ugl I3917 phenanthrene?' ug/t
3859 anthraceneZ. ug,/ t
4584 carbazoLe2' us/l5880 di -n-butyL phrhatate2. ug/ t5397 ftuoranthene?. u9/l
39'19 pyrenez' uslt3870 butyt benzyt phthalate1. ug/ L
18,85 3,f ' -dichtorobenzidine1' u'/t
1860 benzo (a) anthracene2' ug/t
3858 bis (2-ethythexyt ) phrhaLate1- uS/ t
38,76 chryseneZ. u9/ (
1396 di -n-octyl phrhaLate1. ug./t
3351 benzo (b) fLuoranthene1' us/L3352 benzo (k) fr.uoranthene4' u9/|1854 ben:o (a) pyrene11- ug/ t390J indeno (1,2,J-cd) pyrene
!-cs
RPO
oUP ItlSRP! ES l,!S9 RPo
59
101
98
86
B1
85
95
90
92
85
B9
9?
B2
77
8,1
10?
90
iD4
B9
94
32
LCS LIMITS
LOIJ H!6H
1 114
z5 158
59 121
38 122
1 181
58 117
53 127
1 15?
11 176
54 120
27 135
40 137
1 118
52 115
'l 15?
1 25?
33 141
I ',158
17 168
t+ 146
21 159
11 163
17 163
1 1714.u9/ t
B l-Alr(
N -9.
N,ri.
N.9.
ri.D.
N.D.
N.!-
N.!.
N.f.
N.9 .
N.D.
N -!.
N.0 .
N.D.
N.C_
N,!.
r,i -D -
N.D.
ri.!.
\'.1.
\.1.
6t, 55
1!l 1C2
1C2 98
95 86
67 bn
:J :C
es 87
gtJ 94
95 ?1
9? 90
99 37
90 8e
91 9'r
s5 30
79 78
35 35
1 !l? 1 0'l
91 91
'1f ! 107
clA 39
9_q 95
e3 8l
75 75
2
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2
2
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2425 New Hclldnd P kP
PO 8or 12d25
Ldn.aste(. PA I 7605.24/5
717-656-2.100 Fa, 717 65o,.lri3i
QI-'IA:ITY CONTROL REPORT
:EF .'.re.9: !ice i-Jr :!aia.atoo oi ivmboll ano abbferlaoons 2215 Rev ,o^or, tlt#
(iI)La ncaste r Laborato ries
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DUP j{s
RPD I4S I.!SD RPD
QUALITY CONTROL F.EPORT
Paqe: 1l of
A Thermo Analytical Laboratory
LLr sampl-e No. 253199i
sed./Equip Rinse 6rab Uater Salrp'.e
Hercutes: Bacchus Pond
I
: croup Io. 522727
i Hercutes, lncorporated - DE
i
;
Satrple silpteM9L UH ! TS
1881 dibenz (a,h) anthracene1. us/ t
3831 benzo (qhi) pe.ytene
1. ug,/ I
6r-ANX
N.9.
Lancaster Laboratoiles
M E M B E R 2425NewHoilandPrkeK-m i:;irJiii,::: ;i,,'u,,,u,,
88 86
74 71
tcs LIr'1tTs!_0u !{ t Gi1
1 227
1 ?19
91
77
,.r,Orr,r$ d?5pE.sre,se roe'or e(olanatron ot iymoo{s and dbbre? dlrons
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(I)Lancaster Laboratories
A Thermo Analytical Laboratory
QUAIITY CONTROL REPORT
Page: 11 of 11
9URNOGATE LIH:TS
LLI sampJ.e No. 2537991
Sed./'Equip Rinse crab uater SampLe
llercutes: Bacchus Pond
0917 ICL Pesticides in lJaters
4592 fCL Vo[atites by 8240 - uarer
4678 TcL Su846 SflrivoIari Ies/Uaters
4679 rCL SU846 Sflrivotati Ies/Ua(ers
Group [o.52?727[iercutes, :cco.poraied - D€
SURRO6ATE SUHI'!ARY
TRIAL :D SURNOGATE RE'CYS9Y Z
rcx 79DCt 9l
Ct+'1,?-OCA lqCc5-to[uene 1]3srB ?'
Z.FLpheno| 56
PhenDL -ci6 35?,t,,6-rBF 31
Ni trobz-ds 81?-Fbiphnyl 7\
Tpheny LCl i 25
Lanca5ter Laborator P!
M E M EI E R 2425 Nerv Hollaod PrkP
7Xm x";:l#l:i; * ii,,,u,u,n,,
60 '120
:c
?1.i0
35
t+3
13
60 1?0
114
't 00
91
12-a
11t,'!10
141
'1}.))',b Ret,Orrorn, ?aPS6e .eyer:e s de :.rr e!o'd.;'rn oi tvmDort and abbrevralLons
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(il)Lancaster hboratories
A Thermo Analytical Laboratory Page:1of ,14
LLI sample No. ES 2538089cotl.ected: 6l?6/96 at 15:00 by 8R
suHnitted: 6/28/96 Reported; 8/ 6/960iscard: 9/ irl96
cU-6 JUD Grab soil sample
Hercutes: Bacchus Pond
s6JU0 soc#: HBP02- 10
CATIIO. AHALYSIS IIAI.iE
4595 TcL Votatites by 8240
16?5 ThaLtim1643 Alwinut1614 Ant imony1646 Bar i um1647 Beryt t im1or9 Cadmiw1651 chromiul1655 copper1654 I ron1655 Lead1658 I'langanese'1661 N icxe[1665 si tver167? Zinc6935 Arsenic TR
6916 Seleniw TR0159 Mercuey1??5 TcL Pesticides in soLids4688 TCL SuB46 Semivotati tes Soi L
4689 TCL SU845 SemivoLari tes,/soi I0111 iYoislure
"Hoisture" represents the Ioss
101 - 105 degrees CeIsius.
i
i Account llo: 06716
r Hercules, lncorporated - 0E
j EnviromenEar Affairs
i Ui tmi ngton !E 19B94
I
AS RECEIVED ORY IJE I GIIT
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DETECIICIJ L!I'(IT UNIIS
See Page
m9/ <9
ng/<9
ng/ <g
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rEl <9
19l (g
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n9,/ < g
r'9; <g
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in weight of the sampte after oven dryin,3 ar
1 COPY
1 COPY
IO Hercutes, lncorporatedIo ERM - Rocky I'lountain
ATTII: Hr. Joseph Ker.ler
ATTf/: Mr- Bren! RDrinson I
ouestions? Cmtact your Client Services Xeoresentative
Rachef L. Kreamer ar. (7'.7) 650-23!0
li;"'li.3ooo8i,rui3o o,*o[i' ..6r';6 t?zr''
IRespc'cif !ri r-y Subrni t t.'C
Ramona V. Layf,tan, Croug '-eaCellCe get!ts/Leachates
::aa':.a',a: alt::r: :.?:i1c_ lt i,,_:a:,t.t.aabb,errai,oni ll 6 ::, 'C,iCl95
Lancaster Laboratore5
2425 New Holland Plle
PO 8or 12r25
L.ilcasier Pl r ;505'2JlS
;17-65b-.::0C ia\'i \ : -a -.6-2;d:l
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(I)Lancaste r Laboratories
LLI sample No. ES 2533089Cot(ected: 6/26/96 at 15:00 by BR
Subfitted: 6/28/96 Repocred. B/ 6/960iscard: 9/ 6196
CtJ-6 JUo Grab SoiI Sampte
Hercutes: Bacchus Pond
S6JU0 SoG#: HBP02- 10
CAIIIO. AHALYS I S IIAI.{E :
TCL VoLatites by 3?40
343t Chtormethane :
5435 Brorpuerhane3/.35 Vinyt ChLoride3437 ChIoroerhane3140 ilethytene Chl.orrde1074 Acetone1076 Carbon OisuLfide1180 1,1-0ichtoroerhene311? 1,1-0ichLoroerhEoe3111 Chtorofo.m3115 1,2-OichLoroethane4CB5 2-Suranone3ir,6 1,1,1-Trichloroerhane
3t,17 Carbon Ie!rachtoride4091 Vinyt lcetar:3148 6roflrodichloronerhane
3/.50'1,2-DichLorop.opane3154 cis-1,1-DichLorop.opene1181 Irichloroerhene
3451 1,1,2-Trichtoroerhane
'l 182 genzene
3156 Bronpform4'108 4-Herhyt -2-pentanone :.1107 ? - Hexanone3i,57 TetrachLoroethene
3449'1,1,?,2.Ierrachtoroethane
': 183 Totuene118/. Chlorobenzene
34 58 E thy L bmzene1117 Styrenell55 Xytene ( rorat )6187 trans-1,2-0ichto.oethene6?77 cis-1,2-Oich'.oroethene
A The rmo Ana I yti ca I La borato ry Page: ? ot 14
DRY I..IE IGHT
t:ji:i.::r:r.r:!ri:rrr .:: .. : llETHoo
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r HercuIes, Incorporated - DElEnvieomentat Affairs
I uit*inston 9E 19894
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A5 RECEIVED
HgYUAA
[r sur-rsr:,:l]i::r, oETEcr r gN L I tit I T rrl I rs
P.O.
Re( -
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Rachet L. Kreaser
Cl ienr Services Represen:ative
at (717) 616-2i0C
: r:,i.ll;0.;
..rr,:ii:i:: fi.:'D .
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Group Leader, 6C,/YS volarj Les
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'Lg/ <9
r9/<9
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tli./ <g
-gl ig
ui / <':'rl/ <9
u9/kg
rg/ (9
ug/ <9
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ug/k9
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2d25 Ne', Horl;/ro P ke
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A Thermo Analytical Laboratory
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Page: 3 ot 14
LLI sample No. Es 2538089cottected: 6126/96 at 15:00 bv BR
Ii Account No: C5716
! tiercutes. !ncorporated - 0E
i Enviromen(aL Affairs
| ,,ti lmington lE !9894
II
AS RECEIVED
Ret -
sutxni tted: 6/28/96 Repotted: 8/ 6/96Discard: 9/ 6196
CU-6 JUo 0rab soit Sampte
Hercutes: Eacchus Pond
S6JU0 SoGf: HBP02-'10
CATllo. AIALYSIS lrA}{E
ICL Pesticides in Sotids
198'l AtPha BHC1982 Beta 8HC1983 Detta 8Hc1218 Gama 8Hc - Lindane121? Heptachtor1220 Al.dcin'1984 Heprachtor Epoxide1989 Endosulfan I12?2 0ietdrin1985 00E1223 Ende i n1990 Endosut fan I I1986 900'1991 Endosutfan Sutfate1??1 00r5017 Endrin Ketone1959 HethoxychIori0?5 ALpha chtordane3026 Ga0na ch[ordane'1988 'foxaphene
1992 Endrio ALdehydei99l PC8-1016'199,i PCB-1221'1995 PCB-1232't996 PCA-1?421997 PC8-1?481998 PCB-1254'1999 PCS - 1260
!,rE'l go9
OETE'T:OX LI!1IT UIIIIS
DRY I.IE I CIIT
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ug/:<g
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ouestions? Contact your Ctient Services Reoresent6rive
Rachel L. Kreaf,Er at (7'7) 656'?3C)
Resgectlu'. ly Submi t!eC
.,'en i ier e. Hes j, 8. S.
G.oup :e3Cer Pesticides/PcgsLanaaster LaboralofleS
M E M g E R 2425NewHollandPrkereFI iliffi,r::,f r?,u,uu,':1 I
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LLI Sample No. ES 2-53E089cotLected: 5/?5/96 ar 15:00 by eR
suuni rred: 6/28/96 Report ed. El 6/96Discard: 9/ 6/96
CU-6 JUo Grab Soit SampLe
Hercutes: Eacchus pond
S6JUD SDG#: HBP02- 10
CATNO. AHALYSIS NAI'IE
TCL SUB46 Smivotari tes SoiL
'l'185 pneno[3n3 bis (2-chtoroerhyt ) erher
1 1 86 2- ch Loropnenol375a l,3.dichtorobenzene1187 1,4-drchLoro5enzene3755 1,2-dichtorooenzene1690 2-methylpnenoL469' 2,?,-oxybis (1-chto.ooropane)
46C2 4-merhyt onenoi
1 188 tJ'nr trosoit -n-propyl.amine3757 hexachloroerhane3758 nitrobenzene3759 i sopnorone57L6 2-nIrrophenoI37t7 2,4-drflreilrytohenol3760 bis (?-chLo.Dcrnoxy) nrethc,ne
37t B 2,4-drch(orop,renoL1189 l,2,4.trichlorobcnzene
3761 naphtnil t ene4693 4-chloroanil.ine3762 hexachIoroDutJdiene1190 4-chloro-3-merh'LpnenoI1694 2-methyl.naphrh3l.ene3763 he^achIorocyctopentadiene3749 2,4,6-rrichlorophenot1695 2,4,5'(.ichLorophenol.3761. 2-chLoronaphrhatene46q6 2-ni tcoanr t tne3766 dimethyt phihaLare77i5 acenaphrhyle.e
Ouestions? Contact
Rachel L. Kreame.
Account lto: C67!6
HL'rcuLes, Incoeporated - 0€Enviromental, AlfairsUiImingron ]E'19894
AS RECEIVEO: .. :)r.:tr ::l:: IETHOO
AESULTS::.:.,.j DEIECTtC,i LIl.t!T UNrTs
P.0.
Ret.
Lan(aslei Lailo jiione5
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yclr CI ient Services ReF.relentatjvea' (7' |) 650-zi:u
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(iI)Lancaster Laboratories
A Thermo Analytical Laboratory
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LLI sanple No. ES 2538089Cottected: 6/26/96 at 15:00 by 9R i Accoun( {o: C5716
I rercul,es, lncorporated - oE
I Envi romrental Affa i rsl',Jilmington ,E 19894
I
I
Page: 5 of 11
1 10.
54.
270.
270.
54.
1 10.
1 10.
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1 10.
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1 10.
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1 10.
110.
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Rel.ISuknitted: 6/?3/96 Reportedt 8/ 6/96Discard: 9/ 6/96
CU-6 JUO Grab SoiL Sampl.e
Hercutes: Eacchus Pond
s6JU0 sDG#: HBP02-10
CATXO. ANALYSIS NAIIE
IcL Su846 strivotati tes/soi L
4697 5-ni troani I ine
1 191 acenaphthenei750 2,4-dinitrophenol1192 4-ni rrophenoI4698 di benzofuran1193 2,4-dinitrototuene/+699 2,6-dinitrotoluene
3770 dielhyt phthaLare
3769 4-chlorophenyt phenyI ether3769 ftuorene4700 4-ni troani L i ne17D1 4,6-dinitro-2-rethytphenol3772 N-nitrosodiphenytamine3773 4-bromophenyi. phenyt ether3774 hexachtorobenzene1194 pentachtorophenot3775 phenanthrene3776 anrhracene470? carbazote37n di -n'butyt phthatare3778 ftuoranthene
1 195 pyrene
3780 butyt benzyL PhthaLate57Bl 3,3' -dichLorobenzidinej7B1 benzo (a) anthracene
378t, bis (2-ethyLhexyl.) phthalate
37AZ chrysene3785 di -n-octyI phthaIate1786 benzo (b) fLuor;nthene
37A7 benzo (k) ftuoranthene3733 benzo (a) pyrene
37E9 indeno (1,2.3-cd) pyrenei790 dibenz (a,h) anthracene
3791 benzo (ghi ) perytene
AS RECEIVEO
r:::::.:::ii::i:iii::rr:::::i:!;:i:tir i:: : i:ti l'l E T HOO
iitiiiii:iii::i:::&qstj. lils :::l:i.: DETEcT ! 0N L t H I I Url I Ts
DRY lJE I GHT
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ouestlons? Contact your Clrent
Rachet L. KrealEr
services Represen:ativeat (7i7) 6i6-23C0
Lancaster Labor;tores
2425 flew Holland Prke
PO 8cr i2dl5
Lanc6siel P4 l;505'2J25
1 1 r- -556 2)C0 .ax i 11 -515-268t
Respec:iuL ty Submi t tedChris!inc !'1- RaicL irf ,
Grouo -eader, 6Cll'lS
;r9 ie,/e.t< : -:e,Or t.a a- j. .,^ f,r i?::a.t I -r.a ii))re,,,:a! ,t-S d=, I
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&&&
LABORATOR.Y CHRONICTE(iI)La ncaste r Laboratories Page: 6 ot 14
LLI Sample No.
Couected: AU26/96 at
Suboritted: 06/28/96
A Thermo Analytical Laboratory
ES 2-53SC89
15:00 by BR
Ij Account No: 06716
I lercul.es, :ncorporared - oE
i Envi romEntai- Af f a i rs
I u, t.ing,o. DE 19894
I
;CU-6 JUo Grab Soi I Saf,pte
Hercutes: Bacchus Pond
S6JU0 SoG#: ll8P02-.l0
CATNO AIIALYSIS XA}IE
4593 ICL VotatiLes by 8240
1625 Thattim'1641 Al.uroinumi644 Antimny1546 Bariur
1647 BeryL l. ium1649 Cadmiw165'l Chromi un
1653 Copper1654 I ron1655 Lead1558 hanganese1661 [ickeL
16o6, Si lver167? Zinc
5708 sU StJ846 ICP 0igest6915 Arsenic TR6936 SeLenium TR
0159 ltercury5711 Su sU846 Hg Digesr
0819 Sotid SampLe Pesticide Extracr1225 lct Pesticides in SoLids
0581 BllA Soi I Extraction/+688 TCL SU846 Smivol.ati tes Soit4689 TCL SU846 Seffivol.ati tes/Soi I
01'l 1 l'{oi sture
FETHOO
su-846 82408
su-846 6010A
slj-846 6C10A
sP-846 6110A
sr.J-346 SC t CA
sr-846 6'llCA
Su - 8q6 6a'l 0A
SU-81.6 601CA
su-346 6 ',t0A
Su - B/.6 6,1 1 0A
StJ-34o 6J1 0A
sr./-346 6,t'tCA
SU - 34o 50'l DA
SlJ-346 6l'lLlIr
s!.r -316 30i0A
sL,-316 6itCA
sr- -846 6111 CA
su-846 7471A
S{.r-846 7471A l4odi fied
su-846 1550A
slJ-346 8C81
su-846 1550A
srr-846 32700
ss-846 82708
EPA 160.1 (modi fied)
AITALYS I S
TRIAL OATE ANO TI!'IE
1 07/05/96 0937
1 07/13/96 18181. A7/1i/96 18.,8', 07/13/96 1e13'' a7l1_a/96 1618't 07/13/96 18181 07/13/96 1g1E1 D7/13/9o 1g'tB', 07/,.3/96 1Ai6'. D7/1,3/96 18',21 C7l1i/9o 18:SI C7/1:/96 il-:e" 07/a=/96 1e^.8' i7/':3/96 18t!
'. x7/'.3ic,. 111.5', a7/02/e6 1934'. c7/t3/96 15"81 07/'.7/95 0931
1 07/03/96 16381 07/A?/96 1506
1 07/01/96'.t1001 07/\8/96 1553
1 07/01/96 1e3C1 07/05/96 17361 07/05/96 1736
1 07/0?/96 152C
ANALYST
R'ick s- Rodgers
JoIene M. Schiel.ds
JoLene !1. Schieids
iotene !l- Schiel.Cs
Jotene \. Schie!cs
Jolene rl. SchieLcs
JoLene N- Sch i€r-ds
JoLene li. Schieios
Jolene $. Schietcs
Jo r.:ne l!. Sch i e lds
Jotene i'l. Sclrietcs
Jotene !!. Schiei.cs
Jo(ene !1. SchjeIcs
.ror. ene ii. Sct i eLas
Jolene l,l. Schie!cs
oesi R. Carozra
Jo(ene it!. Schietcs
i{ina C. HaIr.er
NetLi S. llarkaryan
Frances A. Oemorest
MattheH U. Kofroth
l,,lichel.e D. Mack
sher.y Lynn Devtin
Joseph 14. Ganrbter
Joseoh iil.6ambter
Nee[ay 8. l4ehta
Lanca5ier Labor;lor er
M E M B E R 2425Ne'rHollandPke
7ffiEfig ili:i:,i;,:::'r,;,,,u.. iF.a..,e5e 5;de ;or arl) ;e:: ir,:lr a _1., ar 4 nabte, i. a-., :. 1 .;'.1;iDr?5
JT
(I)Lancaster Laboratories IQT-IALITY CONTROL REPORT
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Page: 7 of 11A Thermo Analytical Laboratory
LLI sample No. 2538089
Cu-6 JUD 6rab SoiI Sampte
Hercutes: Bacchus Pond
IlGroup tto. 52?239
I HercuIes, !ncorporated - D€
i
II
sarpI e
IID L
Sanpl. e
UNITS
LCS LCS
OUP RPD
LCS LIMITS
LOU HIGH
ouP ilsRPD MS I'ISD RPD LCS
4593 TcL VoLatites by 8?40
3454 chLorffithare?. ue/ke
3435 Brmnethane
l ' uglks3416 Vinyt ChLoride
2 ' ug/kg
5437 Ch L oroethane3. ug/kg
3440 ilethytene Chtoride2. u1/kg
4074 Acetone7. uslkg4076 carbon 0isutfide
3. ug,/kg1180 1, 1-0ichloroetheneZ. u-o./kq
3142 1,1-D'ichtoroethane
'l . ug/kg3444 chtorofocm
1 ' us/19
3445 1,?'0ichtoroethane2. u9/k94035 2-Eutanone7. us/ks
3446 1,1, 1-Irichtoroethane1. ug/kg
3447 Cacbon Te!rachto.ide
1 ' ug/ks
4091 vinyt Acetate3. uglks
1448 Ermdichtoromethane2' uglks1450 1,2-DichtoroPropanel. uglks
3454 cis-1,3-DichIoroPropene1. uglkg
1181 Trichtoroethene
1 . ug,/kg
3/*5? o i be omch I orome thanel. us/kg
3451 1,1,2-Trichtoroethane?. uglkg
1 1 82 Benzene1. uglkg
3451 trans-1,J-0ichIoroPropene1. uglks
BLAII(
Eatch: E961831A8
N .9.
N.D.
N.0.
!.0 .
2. J us/kg
90
99
104
91
102
38
,.02
107
99
96
9l
1CZ
1C6
104
99
9?
9B
96
1C9
90
9(.
87
98
100
101
99
1!0
101
95
95
9?
84
105
1CC
81
90
9S
9e
107
g7
9?
96
92
,'
,1
10
19
?(
,1
59
51
4C
??
5?
70
19
35
'l
1
71,
5l
5?
37
17
?72
211
250
?54
2?1
150
188
?13
155
tJ6
155
167
16?
110
19C
155
209
226
157
'I19
150
lcJ
195
?95
5 102
10 89
396
'11 88
2 i03
6 105
195
295
1 9l
20 95
1 105
3 101
20 105
?95
0 101
2 102
2 111
396
?9e
2 101
198
N.D.
H.0.
Lan(asler Laboratofle5
M E M B E R 2425NewHollandPrkeEgiil ir,'lii;;J,il,li,,::,,,,,,,,,.,
93
93
.::, I
I
,f
ae?-u
LCS LCS
LCS DUP RPO
DUP ilsRPO HS I{SD RPO
('l)
(2)
T
T
T
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(I)Lancaster Laboratories
A Thermo ,Analytical Laboratory
QUALTTY CONTR.OL REPORT
Pa_oe: 3 of 14
LLI sample No. 2538089cU-6 JUo Grab SoiI Sanrpte
Hercules: Eacchus Pond
;
i Group tto- 52?759
I Hercutes, lncorporared - 0E
I
I
Sampt e SampteIiIDL UII I IS
J456 Brmf orm1. ug/kg/.'108 4-Hethy[ -?-pentanone
l. uslks
4.]07 2-Hexanone3. ug/kg
l1+57 Ierrachl.oroethene
1 - uglkg3149 1,1,2.?-tetrachloroethane
'I . uglks
1 1 83 IoLuene
1 - ug/kg
'l 1 84 Ch I orobenzene
'1 ' uglkg
3458 Ethyl.benzene1- ug/kg
41 17 Sryrene1. uglkg1355 Xyl,ene (totaL)1. uglkg6187 trans-1,2-Dichloroerhene?. ug/kg
6277 cis-1,2-DichLoroerhene2. uglkC
1625 Thattiw11. ms/ks
1643 Atuminm8.7 mg/kS
164/+ Anrircny2.1 mS/kS
1645 Eariun
2. 1 ms/kg
1647 BeryLLium0.071 mglks
1649 Cadmiw0.11 ms/ks
1651 Chromim0.15 ms/kg
1653 Copper0.48 mS/kS
1654 I ronl.l m9/k9
1655 Lead2.1 m9/k9l6tg i{ang6nese
0. I 2 ns/k.s
1661 NickeL0.14 mg/ks'1666 Silver0.1.J m9/k9
BLANK
N .0.
N.0.
N.0.
N,r.
s.1-
In
N.9.
N -r -
N.3.
N.0.
Eatcir : 96i 845708C03
lY.D-
Barcn: 961345703001
Eatcn: 96'1845708903
N.D.
Batch:96181+5708003
ri.0.Batcr: 961345708C03
N.r.
Batch; 96'1845706001
N -!.
Barch:9613457i,8003
N.0.
Batcn:95'845708C01
N.0-
Barch: 9618457C81017.2 J $g/ K2
Eatch:9518457C3103
N.0.
Eatch:961845708t01
Batcr: 96184570830Jl.!.
Batcr:951845708,401!-9.
88 8l
98 91
101 90
119 1_10
100 9t,
1C5 10i
96 96
1C7 ',aq
99 92
]C5 103
lfiL 98
195 1 0'!
91 39
?127 1.645 (2)
92 95
105 97
96 91
93 88
128 13',1
1t9 109
?(,5? 21.19 (?)
96 90
1 16 109
97 91
lc? e7
rhe 100.
691
790
12 91
1 115
757
1 r01
097
I 108
7 101
2 106
6 101
I 10?
695
979
279
7 100
59e
799
1 ',02
6 10?
/, 89
7 9t1
5 9t,
696
793
LCS LIMITSLO{ H I Gi{
/r5 169
50 1?4
5? 140
64 14A
16 157
47 150
37 160
5( t6Z
71 136
30 200
51 ',t 56
5t 155
50 150
50 165
21 299
70 111
?3 17?
?6 174
54 111
>t t4)
61 1.4?
53 142
59 135
55 116
50 .,/,7
(1)
(1)
9
0 (1)
0 (1)
0 (1)
0 (1)
13
0 (1)
11
0 (1)
('1 )
Ihe resutt for one or both determinations uas tess than five timesIhe background resutt sas more than iolr:'flres the spiie added-
Lancasie. LabaraiJries
2425 lle,r Ho,acd Prte
9C Eo- ') r::
L::{;r:: -'1 -a : '-:
i1,''5:a.- rl, .,.5i:'er..'si, cc rtr :ic :' a' a^,' .''oat-, a' a :::-a.a.tat.)^j l7 l5 le.. lC/li,:15
(l)La ncaster Laborato ries
A Thermo Analytical Laboratory
QUALTTY COI'ITROL RNPORT
Page: 9 of 14
LCS LI''IITSLOU HT6H
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LLI sample No. 2-538089
Cu-5 JUD Grab SoiL Sampte
Hercutes: Eacchus Pond
i
I croup lto. 522159
I liercutc.s. lncorporated - DE
I
I
Sarpte Sa[pl.eHOL U}IITS
1672 Zinc0.58 ms/kg
5955 Arsenic TR0.?4 mg/ks
6936 selenim TR0.17 ms/ks
0159 llercury0.028 mg/kg
SLANK
Batch:9618457080030.80 J m9lk9
Eatch:96',]845708003
N .0.
Eatch:961845708003
N.).
satch:9618457110C2
N,9 .
Batch:96183C101A
N.3 -
N.D.
N .9.
N.D .
N.D.
H.D.
N.9 .
I.C.
{.0.
N.D .
H.9 .
N.D.
N.9.
N.0.
N .0.
N .D.
N.D.
N.0 -
OUP MS LCS LCSRPD MS ISO RPD LCS OUP RPO
0 (1)
0 (1)
0 (1)
0 (1)
't 08
91
9?
98
92
91
92
6q e5
76 99
73 89
70 85
72 88
71 86
77 9?
7t, 88
79 95
79 9t,
87 105
77 ?l
s2 95
a4 r 01
t9 79
79 97
17 57
e1 95
73 89
6
0
1
0
21
16
19
?0
19
'19
18
16
18
17
'18
19
15
12
20
19
15
20
9?
93
79
76
B5
76
7A
78
B5
81
89
B8
98
87
9l
9t,
B3
90
58
B1
81
149
119
149
157
51
49
3?
?6
12?5 TCL Pesticides in soLids
1981 Atpha 8HC5. uslks1982 Beta BHC3. us/kg
1983 Detta BHc
us/ks
65 1?7
50 137
67 120
73 120
69 120
67 1?0
6D 120
6D ',l Z0
79 120
72 120
68 1?6
62 ',120
72 123
62 120
61 1?1
75 125
57 141
75 1?5
75 1?5
1218 cama 8Hc - L indane
't.
'I .
1.
't.
us,/ kq
1219 HeptachLor1. uslkg'1220 Atdr i n1. u9lk91984 Heptachl.or Epoxide5. ug/kg
1989 EndosuLfan I
us./ks
1222 Dietdrin4- us/kgI985 DDE1. uslkg
1Z?3 Endrin6. ug/kg
1990 Endosutfan I I9. ug/kg
1986 D00l. ug/kg1991 EMosul.fan suIfate10. uSlkg
1Z?1 0D1'l . us/ks3017 Endrin Ketone5. u9lk91859 itethoxychLor40. uglkg
3025 Atpha chtordaneI+. us,/ks
3026 6ama chtordane
us/ks
(1) The resutt for ooe or both determinations Has less than five times the Loo
Lanca5ier LdboratoirS
2425 New Hollaf,d Prke
PO Box 12425
Lanca5re[ PA I7605-24:5
717-656-2300 Fax ll;'5to-)531
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(I)Lancaster Laboratories
A Thermo Analytical Laboratory
QUALITY CONTROL REPORT
Page: '10 of 14
LLI sample No. 2538089
CU-6 JUo 6rab SoiL sampl.e
Hercutes: Eacchus Pomi
I Group llo. 52?739
i hercutes, lnaorporated - DE
I
Sarpl.e SampteIIDL UXITS
1988 Toxaphene
1 , 000. uslkg
1992 Endrin ALdehyde10. us/kg
1993 PC8- 101650. ug/ks1991 PCS-12U50. w/ks1995 PCB-121250. uglkg1996 PCB-1U,250. us/ks'1997 PCB - ',l248
40. ug/kg
1998 PC8-125{10. u9lk91999 PC8-126010. us/ks
ELANK
N.9 -
N.D.
N.0.
N.D.
N.0 .
N -C -
N.D.
I{ -0.
N.D.
N,D.
11 .D-
N.D.
N.D.
N.D.
N,D.
ri-D-
N.4,.
N.!.
ti.!.
Lancasler Laoordtor e!
M E M B E R 2425NewHorLafoPikPrffiir ii:ij#,,,1i,,,:,,,;,"
Lcs i-cs
LCS DU2 RPD
DUP MSRPD lTS XSO RPO
123s795159?
LCS LIMITSLos tl I Git
4668 TCL Stl346 SemivoLati l,es Soi t Batch: 95183SLNC?5
1 1 85 phenot33. uS/kg3753 bis (2-chloroethy[) erher67. ug/ks
1186 2'chtoeophenot33. ug/kg3751 1,5-dichtocobenzene33. us/kg'1187 1,4-dichtorobenzene13. ug/ks
1755 l,2.dichtorobenzene51. u9lk94690 2-methytpneno(67. us/ks4691 2,2' -oxybis ('l-chtoropropane)
1 00. ug/kg4692 4.methytphenol
100 ug/ ks
'l 1BB N-ni trosodi -n-propy(amine
67. ug/kgf757 hexachl.oroethane67. us/kg3758 ni trobenzene33. ug/ks5759 i sophorone67. uslks3746 2-ni trophenot67. uq/kq
7? 3?
75 91
69 7E
75 79
74 78
7? 77
69 80
62 7A
u97
75 33
77 8l
7L ?.?
15
11
11
5
5
6
'15
'11
14
1l
'10
7
77
76
73
76
76
71
6?
90
77
BO
87
76
10
9
5 112
1? 153
23 134
1 172
?o 124
3? 1?e
16 123
16 166
5 152
1 210
40 113
15 180
21 196
?9 18?
tR?'.i/rrcoi: ;nd .iobre..,:ailon5 ):-:6 '. lai3O/2,
(I)Lancaster Laboratories
A Thermo Analytical Laboratory
QUAUTY CO!{TROL REPORT
Page; 1-r of 11
LCS DUP
ql
75
77
78
75
43
81
82
7A
6?
B2
8?
79
75
BO
77
56
73
6l
75
76
90
s5
LCS LIMITSLOU HIGH
32 119
53 184
le 115
14 11?
?1. 133
17 116
24 116
?2 147
28 :?3
1 100
37 141
39 151
60 118
1 11?
ll 14s
17 145
1 ',191
1 132
28 131
39 119
50 158
ll
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LLI sample No. 2538089
CU-6 JUD Grab SoiL Sampte
Hercutes: Bacchus Pond
I
!
i 6roup to. 522IJ9
i HercuIes, ]ncorporated ' DE
I
i
18 57
73 81
71 81
77 82
73 77
1t, i5
80 s7
71 32
17 16
31 9C
80 89
79 85
72 78
79 87
75 81
36 40
71 78
59 65
73 77
7/. 30
e? s9
81 eg
JI
1I
ltSa,rpte Safipl.eHDL U! I'TS
5747 2,4-direthytphenot67. us/ks3760 bis (2'chIoroethoxy) rethane33. us/ks
3748 ?,4-dichLorophenot15. us/ks'1189'1,?,4-trichIorobenzene35. us/ks
3761 naphthatene53. ug/ks
4691 4-ch toroani L i ne
100 -ug/ks
3762 hexachtorobutadiene
BLANK
I.0.
I.0 .
lJ .c.
N.0.
N .0.
{.0 .
r,1.0.
[-D.
N.0 -
N.9.
N .0.
N.D .
N.0.
N.D .
N.0.
[.0 .
N-0.
N.D .
lr.0-
N.0.
N.D .
N .0.
N.D .
YS
EPO
17
1.!
.J
6
5
9
13
-10
7
11
10
I
I
10
I
LCS
RPO
DUPRPD MS IiISO
us/ kg
1190 4-chLoro-3-methyIphenoI
67 - ug/kg
4694 2-methytnaphrhaLene33. us/ks
5763 hexachLorocyctooentadiene
]70 - u9,/t:9
3719 ?,4,6. trichtoroohenoI
67 - us/kg
1695 ?,4,5 - lrichLorophenot67. ug/ks3764 2-chLoronaphthaLene33. ug/ks
4696 2-ni troani L ine67. ug./ks
1766 dimethyt phthalate33. u9/ ks3765 acenaphthyIene
JJ.usl kq
4697 3-ni troani t i ne67. u9/k9
1191 acenaphthene51. uslks3750 2,4-dinitrophenoI
170.ug/ ks1'!92 4-nitrophenoL
170 u9l kg
4698 di benzofuran33. uglks
1191 2,4-dinitrototuene67. us/ks4699 2,6-dini trotoLuene
67. ug,/ks
67-
4689 TcL SU846 Semivotati Ieslsoi I Eatch: 96185S18026
10
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(I)Lm*s#.*?s*tg*QI,'IALTTY CCNTROL REPORT
l2 of 14
LLr sample No. 25380E9CIJ-6 JUo c.ab Soit Smp(e
Hercutes: Bacchus Pord
Ii Group Xo. 52229j ilercutes, lncorporated - DE
Safipl.e SanpLerirDL utl s
3770 diethyt phthal.ate67. ug/kg3769 4-chtorophenyl. F,henyL ether67. u9/k93768 fluorene31. uslks
4700 4-nitroani Line100. ug/kg4701 1,6-dinirro.2-methytphenoL
170.ugl ks5772 tl-ni trosodiphenytamine67. us/kg3rrj 4-bromophenyt phenyt ether
1 00. ug/ks374 hexachtocobenzene
100 .u9/ kgl'194 pentachLoropnenoI
170.u9lks
LCSLCS OUP
LCS LIMTTSLOII H I GH
: 114
25 158
59 1?1
3s 12?
1 181
53 127
r '152
1r. 176
,tl 12O
?7 133
35 133
I 118
?6 137
52 115
1 152
1 ?62
li 143
8 158
17 168
4 146
21, 159
tt toJ
17 163
\ 171
LCS
RPO
I
I
N.0.
N.3 .
lr.D.
N.D .
ri,D -
N.D.
N.0.
N.3.
N.C.
N.D.
lr.D .
N.D.
lt-D.
I-0.
N.0.
N.0.
N.D.
N.D.
N.9.
N.!.
il-c.
N.D.
N.9.
79 88
79 87
71 30
59 6?
66 ??
71 31
31 9?
33 91
7t 76
75 83
71 8]
71 79
e0 90
73 80
93 9?
e6 97
55 58
lt a)
93 103
e2 e9
81 92
73 80
77 35
32 39
'r0 8l
10u
779
176
956
12 73
13 B2
?63
10 77
977
77A
11 86
977
10 91
1? 95
568
780
9 '103
885
13 103
10 B0
'10 e6
lC 73
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3Il5 phenanthrene53. u9lk93776 anthracenell. uglks
4702 carbazote33. u9/kq1777 di -n-butyL phrhatate33. us./kg3778 f Iuoranthene31. ug/ks
1 1 95 pyrene67. uglks3780 butyt benzyt phthalate67. uS/kS5783 5,5, -dichtorobenzidine130. uglkgJ781 benzo (a) anrhracenef3. ug/ks3281 bis (2-erhythexyt ) phrhat ate67. us/ks
378? chrysene13. uglks
5785 di -n-octy( phrhat ate67. u9lk93786 benzo (b) ftuoranrhene67, uglkgJ787 benzo (k) fl.uoranthene'130. ug/kgl78B benzo (a) pyrene67. ug,/kgJ789 indeno (1,2,1-cd) pyrene67. us/ks
Lancaster Labor;tof e't
M E M B E R 2425NewHoL;ndPrteEtIil,=-- ' .,
-
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'-" ,O'r,,rr, ?- i
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Q'JALITY CONTR,OL REPORT
P age:
I
I(I)La ncaster Laboratories
A Th e rmo A; n a lyti ca I La bo rato ry
LLI sample No. 2-538089Cll-6 JUo Grab Soit SampLe
HercuIes: Bacchus Pond
I
I
I Group xo. 52289
I Hercules, Incormrated - DE
I
I
/rIII.tI
itsarpte saflpLe
t(DL ltN I Ts
3790 dibenz (a,h) anthracene
67. us/ks
3791 benzo (9hi) perytene67. ug/kg
0111 l,toisture0.06 Z by ut.
DUPBLAXK RPD
I.0 .
ll.0 .
Barch: 9618405'!6820003A
r1s Lcs Lcs
I4S I'!SD RPO LCS DUP RPD
83 9'r
79 85
985
875
1 00 109
LCS Llr"ilTSLOU IIGH
1 ?27
1. ?19
100 101
tl
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M E M Et E F 2425 Nelv Holland Prke
7rcii-i y}:i::s,::;,,,,i,u,0,,
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LLr sanple No. 2538089Cu-5 JUo Grab SoiI SampLe
Hercutes: Bacchus Pond
'1225 ICL Pesricides in Sotids
4593 ICL VotatiLes by 8240
4688 ICL Su846 Semivotati tes Soi t
4689 ICL Su846 Semivol.ati Les/soi t
SURR06AIE SUHI4ARY
IRIAL ]O SURROGAT5 RECOI/ERY Z
TCx 68DCB 75
d4-1,2-0cA 33
d8- loluene 96Br8 92
Phenot -d6 32?-Fl-ohenoL 772,1,6-!8P 99
{i trobz-cs 37
e - Fb i phny: i9TPhenyLd!4. 7f
QIJAIITY CONTROL REPORT
Pagei 11 ot 11
SURRCGATE LIiI!TS
LOU
50
50
70
74
?t,
25
t9
?3
10
1B
H t6fi
120
120
117
121
1 ',]3
1:z"
1?Z
120
115
137
Lancaste/ labora tor!el
M E M B E R 2425Ne,!HollandPrkeiltili-{ ":?::-':. :.tl
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(iI)La ncaster Laboratories Page: 1 of
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A Thermo Analytical Laboratory
LLr sample No. ES 2538083cottected: 6/27196 at 09:05 by 8R
suutritred: 6/28/96 Reported: 8/ 6/960iscard: 9/ 6/96
cu-4 JUo DupLicate Grab soit sampte
Hercutesl Eacchus Pond
s4JU0 sDG#: HBP02-04DUP
CAT}IO. A}IALYSIS HAME
I
I Account |lo: 06716
I l"rcutes, :ncorporated ' DE
i Envi romenta'r Atfai rs
I t" i tmi ngton cE 19894
AS flECEIVEO
MEIHCO
oETECIi0H L!l{!T U[lTS
DRY VEIGHT
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il1625
1643
1641
1&6
1647
1619
1651
1653
1654
1655
1658
166',]
1666
1672
6955
6916
0159
01 18
0121
mslkg
n9/ <9
mg/ks
mg/kg
nglkg
mg/k9
mg/kg
\9/ <9
n9/ (g
mg/<9
nE/ks
Eg/lg
mg/(g
nE/k9
ms/k9
n9/ ks
trE/ <g
Z by rt.
i1 by !!.
:he
'l?.
2.9
?.9
0.096
0. 17
0.61
0.55
3.1
0. 16
0.60
0. 58
0.32
0. zi
0. c37
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1 CoPY TO ERH Rocky Mountain
ATrN: Mr. Joseph (eli.er
A'I'i-N: Hr. Brent Robinson
Questions? contact your ctient services RePlesentatlve
Raciet L. Xreamer at (7'7) 656-2300
15:19:18 D 0002 23 REP 126t36 52?739
3 1 0 0.00 00000000 AsR000
Respecrful. Iy submi tted
Ranona V. Layman, G.oup LeaCer
ICP l,letaLs/Leach3t.rsLanaaster Laboratoaes
2425 New Holland Ake
PO gox 12425
Lanca5ier PA I r-tiO5-1a25
717-656-23C0 :dx 717-556.:43;nl
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LLI sample No. ES 2-538083cottected: 06/27/96 at 09:05 by BR
SuBtritted: 06/28/96
I o."or . lto: 06716
I HercuLes, lncorporated - DE
I EnvirorenraL Af f a irs
I ui tmington 0E 19894
i
LABOFtr,TORY CI{R,ONICLE
Page: ? ol
ANALYST
Jotme I'1. Schietds
Jotene !. schieLds
Joline i!. SchielcsioIene M. SchieLcs
Jol.ene I. SchieLds
Jor?ne I'1. SchieLcs
JoLene I'1. SchieLcs
JoLene lil. SdhietCs
.iolene ll. SchieLcs
.lolane l'!. ScxieLds
JoIene tl. SchieLcs
JcL.ne l!. Schieios
,.lor.ene:4. Schieiis
-!o I ene ,\1. Sch i e ics
Desi R. Carozza
Jor-ene ft- schietds
Nina C. Hal.ter
lelLi S. !,tarkaryan
Ftances A. Demorest
lleetay B. itehra
NeeLay B. liehta
(iI)Lancaste r Laboratories
A Thermo Analytical LaboratoryI
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Cu-4 JUo Dupl.icate Grab Soil. Saqlte
Hercutes: Sacchus Pond
54JUD S0G#: ll8P02-040UP
CATlr0 AlrALYsls NAfl€
'1625 That t im16q3 ALuminum
1644 Ant ircny
1646 Bar i ur1647 EeryLl.iw
1 649 cadni uil1651 chrnlim1653 copper
1 654 I ron
1655 Lead.1658 t{anganese
1661 rlicket
1666 S i Iver1.67? Zinc
5708 Su SU846 lCP Diqest6935 Arsenic TR
6936 setenim TR
0159 Hercury571I SIJ SlJ846 8g Digest
0118 tloistuce
01?1 iloisture Dupticate
I.4E THCD
su-846 6010A
srJ-846 6010A
su-916 6C10A
su-546 6C10A
sU-81r6 6'J10A
su-846 6Ll10A
SIJ-346 o310A
su-846 6C',r0A
srJ-846 6010A
s',J - 346 6J 1 CA
sil-846 6410A
Su-34o 601CA
su-5(6 6Ci0r1
s';-346 6t1CA
su-8,16 ic50A
su - 846 6,1't 0A
sLJ-31,6 6010A
su-846 7171A
SU-346 717iA ilodiiied
EPA 160.1 (modi fieC)
EPA 16C.1 (mo,iified)
AIIAL YS I STRIAL OATE ANC T!HE
1 07/13/96 17091, A7/13/96 17A9
', 07/13/96 1709'. a7/13/96 17091 C7/13/95 1709
" 07/',3/96 17091 !7/1.1/9;J 17091 A7/1j/95 1it)9'' A7/13/96 ''7C91 Lt7/1i/9tJ 17191 0711i/96 1.7C91, C7/ii/96',7t?
'. C7/1.1/9tJ 17:9". c7/1i/96'.719i 07/02/90',93!1 07/13/9b '.7491 07/17/96 A8i0
" 07/43/96 162?1 07/0?/96 15n6
1 07/0?/96 15?A1 07/C?/96 15?.4
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QL]ALITY CONTROL REPORT
Page: 3 of
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r Hercutes, lncorporated - DE
i
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sanpte SampLeI.IOL UN I TS
1625 Thattim11. m9/k9
1&3 Atminm9.0 m9/k9
1644 Antircny?.2 ms/kq
1646 Sariw?.2 ms/ks
1647 Beryt t im0.C74 ms/ks
1649 Cadmim
0 . 13 ms,/ks
1651 Chrmim0.17 mg/ks
1555 copper0.50 mg/ks
1654 lron3.4 mg/ks
'1655 Lead2.1 ms/kg
1658 l'{anganese0.12 ms/kg
1661 Nicket0.16 m9/k9'1566 Si Lver0.45 mslkg
1672 zinc0.40 mg/kg
5935 Arsenic TR0.25 rng/kg
6936 Sel.enim TR
0. 18 ms/kg
0159 lercury0.028 m9/k9
0.118 Hoisture0.06 % by wt.
0121 Hoisture Dupticate0.06 /. 6y ut.
tcs '-csLCS 9UP RPD
DUP IIS
RPO MS hSD R2D
(1) 95
?1 ZA27
(1) 9?
9 105
0 (1) 96
0 (1) 93
0 (i) 1?3
0 (1) 119
13 2t52
0 (1) q6
11 116
0 ('t) 97
(1) 102
0 (1) 108
0 (1) 91
0 (1) 92
0 (1) 9?
696
979
279
7 10C
598
799
'l 10?
o I ul
189
7 9t,
594
696
798
692
093
137
079
LCS LIMITS
LOU HIGH
50 150
50 165
?1 ?99
70 111
23 177
26 174
5L 141
57 145
61 \t?
)J ICZ
69 135
55 146
50 147
54 149
49 149
5Z 1t*9
26 157
Il
Il
SLAIIK
Batch:961845708005
[.D.
Eatch:961845708C03
N.0.
Satch:961845708003
ll.0 -
Batch: 961845708C03
N.0.
Eatch:96'1845708003I.0.
Batch:961845708003
ti,0.
Eatch: 961845708C03
lr.r.
Batch:96i845708C03
N.D.
Eatch:961845708C037.? J mglkg
Batch:96:845709.03
Batch:96-18{5708303
}J.0.
Eatch:961845708005
N.D .
Batch:961845708003
1.0 .
Eatch:96i8457080030.80 J mglks
Batch:95184:708003
N.D.
Batch:961845708001
N.D .
Eatch:961845711002
N.9.
Eatch : 96184Ci1 6320003A
Eatch : 96'l 84C316320003A
89
1645 (2)
95
97
9-1
38
131
1C9
?139 (?)
90
109
91
97
98
92
91
92
il
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(1) The resutt for one or both determinations pas Iess thon five times the !O0.
(2) The backqround result las more than four times the spi(e adCed.
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Lanca5ter Laboratofles
M E M B E R 2425NewHoilandPIke
7ffiril il:,#i;.,':::.i:;,u,u,,
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LLI sample No. 2538083
CU-4 Juo Duplicate Grab Soit Sampte
Hercutes: Bacchus Pond
)ea,ilje.se t.oe :cr erct6nnlton or tyf:a._. : r-:: :cor:.,lJItoai :.: a qe.,'r'lil0/95
3l
LLI sample No. Es 2533082Cottected: 6/27/96 at 09:05 by 8R
subri tred:
D i scard:
Reported: g/ 6/96
cU-4 JUo flarrix spike oupticate Grab soit Safl'pte
Hercutes: Bacchus Pord
S4JtJo sDo#: HBP02-04MsD
i Account No: 06716
i Hercules, !ncoroorated - D€
i Envi romenrat Af f a irs
i IJi lmington cE 19s94
I
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AS RECEIVED
Page:
P.0-
Ret -
Respectfu( Ly subft'j tted
Rarpna v. l-ayltran. Croup l-eader
!CP l'4eaaLs/Leachates
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1 COPY TO
1 COPY TO
Lancaster Laboratories
A Thermo Analytical Laboratory 1of 14
CATI,IO. ANALYSIS IIAI'{E
4593 TCL voLatites by 8?401625 IhaI t iur1613 AIuninun1611, Ant irrcny1&6 gar ium1647 Beryl.lim164C cadmium1651 chrmiun1653 copper1654 I ron1655 Lead
-1658 Manganese1661 rickeI1qt6 Si Lver1672 Z\nc6935 Arsenic TR6910 se(eniur TR
01 59 llercury1??5 TcL Pesricides in soLids46E8 TcL Su846 Semivo(atil.es SoiI4689 TCL sUB46 semivoIati Les/soi L
0'l 18 Hoi sture
TETHOO
DETECIION L!I.IIT UNITS
See Page
14. mg,/kg8.7 ng/\g?.1 ng/kg2.1 mglkgC.072 ms,/kg0.13 ns/kg0.46 ms/ksC-/.9 mglksi.5 m9/k92.3 nru/kg
11. 1 2 ms/kg' A./.t n9/<9
'-i.4,; ng/kgC.J9 ff.s/ <9
C . ?4 ng,/ <9
0. l7 mg/kg
'-1. C?8 ns/ls
9ee Page
See Page
See Po€e0.06 iL by Ht.
DRY UEIGHT
,:,i i::I ii::i:.i:i;.::'i:,i:, lr::r.::.:::,,:;i:1 !:; llET HoO
:i,;lJ,i ii:.;:ii.i;:Eqsu!I! :, :' :. 0ErEcT I ox L I M I T
:t:ii..ri:i:tr!:i:1::225::::.:::;t:i.t 18.
1:.1,,;,1,,.;t 0 ;:?00:.,.1i. .,1;t,,;r , 1 1 .
:.!iii:,lit,;t:,,:t:;:::::'5qil:::,:l::.liii, 2.8
i.:iiiririiir:::j,:i::i:31t1iil',::;iii:i' 2-B
:iii:::::r:::!;:.i::,i:ri:::6:'6i1iiii::it 0.093
::..::.....,:...:,::.,:..5.-?..,i, 0.16
;:,itt,:,tiii,::i:;i:i::,i::50,"7 ::ti'i:'', 0.59
t::iliii:i,r,tit!l::lr:it,;:t57:5'it:.i:i;.t:,1.. 0.63
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.::::".r:r.,.r:toe-.ti,','!.r': 0.15
;,,,;:1;:;l;::1::i1;,,:i:l;:67;2:::: r: 0.58
:tli:ll:,i:'i:i::ir::,::r6j:1:::1:r,'. 0.57
li' ,.J,::,,i,1:::i'i:::l}0$:, i: i',, ,it,:i: 0 .50
,1.,i;,.::,:,,:.:,?lo;:::l:::::',"' 0.32
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Hercules, lncorpo.ated
ERI'l - Rocky l',lountain
ATTl,l: t'1.- Joseph KeLl.er
ATIN: tir. Brent Robin-son
ouestions? contact your ctient services Representative
RacheL L. Kreamer at (7i7) 65o-2i!'0
14:'17:38 D 0002 23 REP 1?6tii, 5?27i9310 25.00 00137200 AsR000
Lanca5t€i Laoo.alorres
M E M B E R 2425NewlollandP'kP
Y&tH il;!i ;l,i;':::'iii,u,u.,d'I
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A Thermo Ana lytical Laboratory
I,LI sample No. ES 2538082Co[lected: 6/27196 at 09:05 by BR
Suunitted: 6/28t96 Repo?tdz 8/ 6/96Discard: 9/ 6/96
CU-4 JUo Hatrix Spike Dupticate Grab So!l Sanple
Ii Account No: 06715j lercuLes, lncocporared - DEiEnviromnral. Aifairs
luitrinston 0E 19894
I
I
AS RECEIVEO
::i:i.: ",+::ii:.:.r i.:::j l'l ET HOO:nfsrjlfS.::;,.;il DETEcTTON LrHtT uNrTs
? of lt,
P.0.
ReL.
DRY UEIGHT
iiiiilillii'::,,i:ii:i:i',:iitiiiti:i:liiiiit,::i:,i,, HETHOo
iiiiii;i..i!ri:,i.il:i,'iiqsulrls:::ti:.: DETEcTI0N L I rtl T
Quegtrons? Contac! your Client Servjces RepresentativeRachet L. Xre3rner ar (7:7) 656-2lCD
Paqe:
Respe.tfuI Ly slbmi tredIichete l'lcClarin, 8.A.
6roup r-eadr.r, 6C,/MS Vol.ar i les
llercuIes; Bacchus Pond
54JUO SD6#: HSP02-041'!S0
CATNO. AIIALYSIS IJAIIE
TCL Votatites by 8240
3134 ch I ocmthane3435 Brwmerhane3436 VinyL Chl.oride3437 Chto.oethane3410 I'lethytene Chtoride4074 Acetone4A76 carbon 0isuIfide1180 1,1-Oichloroethene3142 1,1-0ichtoroe:hane3141 ChIoroform3145 1,?-0ichIoroethane4085 2-Butanone3446 1.1,1-IrichIoroethane34/.7 Carbon Terrachr-oride4091 Vinyl Acerare3448 EromodichIoromethane3150 1,2-0ichLoropcopane3154 cis- l,l-0ichLoropropene1'181 Tci ch loroethene3152 Dibromochtoromethane3453 1,1,2-TrichLoroethane
1 132 Eenzene1451 trans-1.5-0ichl.oropropene3456 Brmf orm/.108 4-$ethyt-2-pentanone4107 2-Hexanone3157 Terrachtoroethene3119 1,1,2,2-Tetracntoroethane
1 185 To(uene
1 184 Chtorobenzene3458 EthyLbenzene1117 Styrene3355 xytene (totat)6187 trans-1,2-DichIoroethene6277 cis-1,2-0ichLoroethene
.. .tt.: t: :. ii: 1:..::,:::
I::.' :: !:::| 1.1 '..::i:l
:-....'"1 lu-i::-.: -'
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rin :. ,.
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1.
5.
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'1.
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us/ks
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u9li9
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sg/<g
us/ ks
,t9/ <g
u9/ i(S
us/ k9
u-o/kg
us/ kst9/kg
ug/ tg
uglk9
ug/ts
ug/'<9
uql t9
!9/ <9
us./kg
ugl <g
ucJ/19
ur)/ <9
u,) / <.)
u'l/ks
!9 /'<g
Laa(a!ier Ldtorilo.res
2425 lle,a rlo irid Prke
PC Bc, 1l.L;5
:-df.-;ti.. ?n l:,1: 24-l:
,a ,e"e-.,a t:t)e :ot alci:r;i:on q: :,rorl,: j:ao .lobre7r.llicir9 :l l5 Rer iC/10/95
(l)Lancaster Laboratories t
LLI sample No. Es 2538082cottected: 6/27/96 at 09:05 by BR
subritted: 6/?8/96 Repo?ted: 8/ 6/C6oiscard: 9l 6196
I
I Account No: 06716
I leccuLes, Incocporated - DE
i Enviromentat Affairs
I ur lmrnston 9E 19894
I
A Thermo Analytical Laboratory Page: 5 of 14
P .0.
Re(.
DRY UEI6HT
iir;lll;:ii'i:i:i'!l::t:,i:::'i;:ir:!.lri:il'::r:';":', HETHoo
t::rit::::::::i:;i,:i,:r'&E'glJLTS:i i I i: 0E TECT I OI L I M I 1
:;, 6.
,. l.,:-:, ?.
z.r 5.., 5.
.,,, z.
r 10.
i,::' '10.
:'1.::. ?'r::rJ 6.:',, 60.. )-
: . 2,000.:.,,J 1 0.' 40.".: 1o.
;:ti ,:' 60.:r:i 70.
'l:r, 60.:,:::, 40..:'!': lo.
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3.
Cu-4 JUo [atrix spike Dupticate Grab soiL saf,pLe
llercutes: Eacchus Pond
s4JU0 SoG#: hBP02-o4l,lsD
AS RECEIVED
CATIIO. ATIALYSIS IIAME
TCL Pesticides 'in Sotids
1981 Atpha 8Hc1982 Beta BHc1983 oetta BHC'1218 6amm BHC - Lindane1219 Heptach Ior1220 Atdcin1984 Heptachtor Epoxidei989 Endosu[ fan I1222 0iel.drin1985 oDE1??3 Endrin1990 Endosutfan I I1986 DoD1991 EndosuLfan suIfate1?21 DoT3017 Endcin (etone
1859 l{ethoxychtor3025 Atpha chtordane3026 carma chtordane1988 Toxaphene1992 Endrin ALdehyde1993 PC8-10161994 PCS-1?211995 PCB-123?1995 PCS-1?1?1997 PC8- 12181998 PC8-1?541999 PCB-1260
ii 'l -
,: 1., 3.
l. t'.:,. 4.i.,. 1 .
6.. 9.
: to.,, 1.
:: 40':|L
': 1., 1 ,000.ii J '10-
' JU-
l. 3C.:, 50.,ri so.
:.;' 40.
:: , iC.
ouestions? Contact your Client Services Representattve
Rachel L. Krearner at (7'7) 656-2]00
u9lkg
ug/k9!s/i9
us/ ks
us/kg\g/\g
ug/tg!9/ <9
!9./ks
us/ kg
u9/kg
19 /'<g
ug,/kg
ug/ k9
r9l ks
u9/ <9
u9/.<g
ug/ks
u9/kg
ug,/k9
us/ks
u9/kg
u9/kg
u9lkg!9/\S
us/kg
u9/ Kg
uq/ kg
Resoec:fu( ly Subrni tted
Jeniier E. lless, B.S.
Group leader 9esii cides/PCBsLdn(as(er Laboriiores
.2425 i\lelv Hoiia.o Pr(e
PO Eor l2rl5
Lin(Jr:€r ptr I ;a,l;-:12:
:17'd:6 llCC ' j, r:.-'.-':''2;a ,rl
I
li
ipo .eyEr.,r ../!e i.rr rjni;nat on oi t!n50rt ;.c noor?vr.tiio05 l:''. ?e. 'ariC/?5
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(iI}Lancaste r Laboratories
LLI Sample No. ES 253E082Cotlected: 6/?7196 zt 09:05 by 8R
subtritted: 6/28/96 Repoctedt 8/ 6/96oiscard: 9/ 6196
I o..o*, xo: 06716
Hercutes, !nco.porated - 0EEnviromentaI AffairstJltmington DE 19894
A Thermo Analytical Laboratory Page: 4 ot 14
P.0,
Rel..
DRY UE!GHT
lrli::'ii'r1:iii;li'l':'i:j:l'!,,'l:ir'i''::,'i':'',. llETHOo
:r;',',::::,,:,:1,:i..RESULTs,,., 0ETEcI I oil r- ! l,{ I T
CU-4 JUD t{atrix Spike Dupticate Grab Soit
Nercules: Eacchus Pond54JtD S0G#: XBP02-04l.,tSD
CATllo. AlrALYsls IAHE
TCL SU846 Sflivotati tes Soil.
1185 phenol.
3753 bis (2-chLoroethyt) ether
1 186 2-ch L oroF,heno t375t, 1,3-dichtorobenzene1187 l,4.dichloroo€nzene3755 1,2-dichl.orobenzene4690 2-rethyLphencl.469,| 2,2' -oxybis ('l-chr,oropropane)1692 4.methyLphenol.
3757 hexachtoroethane '3758 ni trobenzene :
3759 i sophorone3716 2-ni trophenot3747 2,1-direrhytphenot5760 bis (2-chtoroethoxy) methane37r,8 2,1-dichLorophenot1189 1,2,4-trich[orooenzene .3751 naphthalene ../.o91 4-chIoroani I ine
1190 4-chl.o.o-3-rethyl.phenol.1694 2-methyLnaphthatene3763 hexachtorocycLopentadiene3749 2,4,6.trichLorophenot16C5 2,4,5-trichl.orophenoL3764 2-chLoronaphthaLene4696 2-ni troani I ine3766 dimethyL phrhal.ate3765 acenaphthytene
SampLe
AS RECEIVED
rtEsiJtiI:;
I'rETHO0
DEIECT I ON L I !.I I1 U!{ I TS
I
55.
ot -
JJ.
JJ.
31.3i.
1()A .i00.
67.
67.i::.
67.
07.
67.
33-i3.
100 .
67.
67.
33.
17A.
67.
67.
35.
67.
u9/ks
!g/kg
'J9 /'<9
uq/kg
uglk9
ug/Kg
ra/ <9
15 / <.!
r,l/kS
us/ks19/\9
u9/i9
u9l (9
ls/'<gri/ {g
$/kg19/kg
u9l k9
rg/'<9
uglks
us/ks
ug/<9
u9/kg
ug/is
u9/k9
rg/kg
ug/ig
u9lkg
u'J,/ <9
u9/ks
11.
87.
43.
43.
43.
4i.
87.
1-?0.
110.
13.
(3.
qJ.
45.
13.
220.
87.
87.
43.
87.
13.
43.
i.r,i:ii r;5i,0,:
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'.' 3 ,!i0().'' '.' ;'; a00.
..i::5i;c00.'' .l
ii,3,fC0::::,,i
.:.r::, J,,5ll0;':r:'ri. 3;000 ".:r,',
::1, ti;2rJ0.. ..
:,i:3ij600; ,1.,.,:i 3:;.500, i:
lr,5i;6(0,..
:l::.4'eQc' ' ,
1. j;5t10;', .
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,. ,,ri3ii5q0:..:.
.l;riif,500'.,
,!l.irl:3)500.- ::
':iilj ,l.400.::,:.i:r1ll,:. l::640::::r'
ir,'i:r:;:',':3'isoQ.. .r,
:tirrt:l:1 :.i ii3|,,7.001;,', :
I i I ii:.:ii::.r 5 ;i90:'l.i::
:': : :,:.'r:tir l', 400 :: :':
:,.tiiit,:i'3,r,900: .,'i.r i:i:ill:Jr:80O;::i:
;..',:::l;ri:s;:7go;.',, ,. ,3,400.. .j
:i,.,'' .'J;500:"
ouestions? Contact yo!. Ct ient Services Representatjve
Rachet L. Kreamer at (717) 656-21C0
L6nc65ie' L;co.aiorr9r
M E M B E R 2425N.,!Ho;ndP(E
7Xm-A llrlir;',;: :,.,i,.,,,
Respectful Ly Submi tted
Christine I. Ratclifi, 8.S.
Group Leader, GC,/l4S
)ep .5,.,r : . ce -.,i +rC ar e'. rr Ai rr,b..' a aata .isap';ralton!aa:a,., lt)O/95
Page: 5 ol 14
LLr sample No. ES 2-538082Cottected: 6/27196 at 09:05 by sR
Subni tted: 6/28/96 Reporred: 8/ 6/960iscacd: 9/ 6/96
CE IVED
T,TETHOO
DETECTION LITIT UXITS
P.O.
Ret.
DRY PEIGHT
,il:i':liirl!:i:ii:!;':,:,i,i.r:ii::i::r!:::::i'.:.li;::,:: HETHoD
r,iii:;;,ir,i;l, tesu;1.q,,ri :';r DETEc T I otl L I M t T
87.
43.
2?0.
??0.
43.
s7.or.
87.
13.
110.
??0.
110.
130.
?20.43.t3.
41.
qJ.
43.
170.
43.
t3.
87.
s7.
1 70.
87.
t
t
t
I
T
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I
Cu-4 JUD Iilatrix Spike Dupticate crab Soit Satrpte
ilercutes: Eacchus Pond
54JUD SDG#: HBP02-04lls0
cAr ::,:r:i::,i:;:+r::,ri:i:i:,::::|t0. ANALYSIS xAilE ::i:ilj,ij::l::::ijl:,ft8
ICL SU846 Semivotati tes,/Soi L
4697 3-nitroani I ine1191 acenaphthene3750 2,4'dinitrophenot
i 192 4-ni trophenot4693 di benzofuran1193 2,4-dinitrototuene1699 2,6-dinitrorotuene3770 diethyI phthatate
3769 4-chLorophenyI phenyt ether3768 ftuorene4700 4-ni troani I ine1701 4,6-dinitro-2-methytphenoL3772 N-ni trosodiphenytamine,773 4-beomophenyt phenyl ethe.3771 hexachtorobenzene1194 FEntachtorophenoI3775 phenanrhrene
37-16 anthracene17OZ carbazote3Tn di-n-butyI phthaLate3778 f luoranthene
'l 195 pyrene
3780 butyt benzyl phthatate3783 3,3' -dichLorobenzidine37A1 benzo (a) anthracene3781 bis (2-ethyIhexyt) phthatate3782 chrysene3785 di -n.octyt phthatate
3786 benzo (b) fluoranthene3787 benzo (k) lluoranthene3788 benzo (a) pyrene178C iMeno (1,2,3-cd) pyrene
3790 dibenz (a,h) anthracene3791 benzo (9hi) peryl.ene
67.
JJ.
1 7C.
170.
67-
67.
67.
67.ji.
1Cq.
17C.
l0c.
17C ,
51.
)-\ -
l_1.lt.
67-
o7.
I5U-il.
67.
33.
ir7.
1J11.
67.
67.
57.
67.
u9/k9
:g/k9
19lk9
u9/K9
!9/'<9
t9/ <g
!9/<g
u9 /'< I!i,/tg
!9/ <9li/ks
19 / ?.9
r9/?9
u9 /' j-9
!9/k9
:9/ (9
!9/ (S
'J9/<g
L-9,/ k9
ug/kg
u9/<g
u_o/kg
e9/ <9
u-o/ < I\9/ <9
,J9/ <g
u9/i9
ug/19
u9 /'<g
ug/ <9
ug/rg
u9/tg
u9/ <9
u9/ks
ouestions? Contac! yolr Ctient Servi$es Reoresentetrve
RacheI L. Kreanre. at (7]l) 656-lloC
Respectfut Iy Slbmi ttedChristine r!. Rarc!- i if ,
Group -Lead:r, GC/MSIan(atlei Labcralore9
M E M B E R 2-t25NerlHollandP,KerelE ;ii,,i11ii'',: : ti'u-.u,,,,d'I
I
Helrcutes, !ncormrated - 0EErlviromntaI Affairs
Ui]Lmingron 0€ 19894
9e. :C, il;9!
oY
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&&&
I,ABORATORY CHRONICLE(il)Lancaste r Laboratories Page: 6 ot 14A Thermo Analytical Laboratory
LLI sample No. ES 2-53E082cottected: 06/27/96 at 09:05 by 8R
submitted: 06/28/96
cg-4 JUD flatrix spike Dupticate Grab soit smpLe
Hercutes: Eacchus Pond
s6JUD S0G#: HBP02-04MSD
I Account llo: 06716
I HercuLes, !ncorporated - oE
iEnvirorentaL Affairs
i uiLmington oE 19894
I
I
CATn0 AIALYSI S ]lAH€
4595 1CL Votatites by 8240
1625 Tha(tim'1645 Atminm
16a4 Antircny
1 646 sar i ur
1647 Seryttim1549 cadmim'!651 Chrqtim1651 copper1654 I ron
1 655 Lead
'l 658 Hanganese
1561 Nicket
16o6 Si tver
167? Zinc
5708 Su SU846 ICP 0igest
6935 Arsenic TR
6916 sel.enim TR
0159 llercury5711 Su Su846 Hs oisest
0819 Sol.id Sampte Pesticide Extract
1225 IcL Pesticides in SoLids
0381 EllA Soit Extraction4688 TCL su846 ssnivoLatites soi L
4689 . TCL SU846 Senrivolati Les/soi I
01 18 lloi sture
TET HOO
stJ-8/.6 82408
su-346 6!10A
su-346 6010A
su-846 6010A
s9-3(6 6010A
su-846 6a't0A
su-846 6ClCA
su-346 6C'10A
sr-34o 6llqA
su-845 6,J10A
s;-846 6J',l0A
su-816 5Ct0A
Sr;'34d 6Cl0A
s'H- s1,6 6ClCA
srr- 316 6C',l 0A
s" - 3.o i!5'-lA
S\J-346 oC'l0A
s,l-84,5 6C10A
5U-3/.6 7471A
su-816 747]A uodified
su-81i6 3550A
su-845 8:'gi
su-816 3550A
Sg.E46 B:iOB
s',J-3/r6 82708
EPA 160.j (modified)
AIIALYS I S
TR!AL DATE AND TII'IE
1 07103/96 055C
1 07/13/96 17i91 07/"3/9o 17191 07/13/q6 17191 07/11/96 iTig1 07/13t96 1719, 97/1.1/96 11.9' 07/13/96 17':g1 07/13/96 1719'; A7/13/9iL 17'.91, A7/13/96 171.91 07/'.3/9o 17',91 Ci/13/9b 17..91 07113/96't7'.?1 07/13/96 17',91 07/02t96 19311 07!13/96 17191 D7/"i/96 CA3B
1. 07103/96 16?11 n7/02t96 1506
AIIALYSI
Ctark A. oougherty
JoIene M- Schietds
..'olene tl. Schietis
JoLene M. schieLis
JoLene :,1. Schietcjs
,,io(ene l'1. Schietds
JoIane itl. Schields
JoLene rt. Schietds
Jo I ene M. sch i e!.Cs
iolene I. Schiei-cs
Jotene !1. Schielcs
ioLane i{. SchieLcs
,.i otene !1 . Scir i etds
Jolene !i. SchieLos
JoLene i!. schieids
0esi R. carozza
iotene li!. Sch ieLds
Nina C. HalLer
Ietti S. Harkaryan
Frances A. Demorest
07/01/96 1400 Matthew H. (oJ.oth
07/18/95 A605 MicheLe 0. itack
07/01/96 1930 sherry Lynn Devtin
07/04/96 1?",4 Joseph H. 6ambLer
07/0t,/96 1211 Joseph I'1. 0ambLer
a7/o2/96 152A NeeLay B. itehra
Ldn(6slea LaccIaio. e!
M E M B E R 2425Ne'r:'''rcPke
2. j6 o€,. t,-ri lt..li
QUALTTY CONTROL REPORT
Page: 7 ot
il
"ll
(I}Lancaster
A Thermo
LLr sample No. 2538082
CU-4 JUD llatrix Spike Dupticate Crab Soit SatrFl.e
Hercutes: Bacchus Pond
il
satrple
I.IDL
sanpt euIIts
:I
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DUP
RPO
LCSLCS oUP
LCS tCS L$rrTSRPD LOIJ H I6H
4595 TCL VoLatil,es by 8240
BLANK
Eatch: E961851A8
[.0.
r,l.c .
N.0 .
{.0.
3434 Chlormethane
2. us/kg3435 Eromqnethane3. ug/kg3436 vinyt Chl.oeide?' ug/kg
3437 Chtoroethane3. uslks3440 |tethylene ChLoride?. ug./kg
4074 Acetone
7 ' ug'/kg4076 Carbon 0isutfide5. us,/kg
1180 1,1-Dichtoroethene?. us/Lg
5442 1, l -Dichtocoethane
1. ug/kgJ444 Chtorofonn
1 - us/ks3445 1,2-Dichtoroethane?. uglkg
40E5 Z-Butanone7. ug/ks34tt6 1,1,1-1 t ichIoroethane1. uglkg
5447 Carbon Tetrachtoride1. ug,/kg409'l Vinyt Acetate3. ug/kg3448 BromdichIoromethane?. ug/ks3450 1,?-Dichtoropropane3. uq./ks1454 cis.1,l-Dichtoeoprooene
J uglkg
90 87
99 98
104 100
91 101
'102 99
8S 78
102 10C
147 101
99 95
96 95
93 9?
102 84
106 105
'! c{ !00
99 81
92 90
98 9B
96 98
109 107
90 37
94 9?
98 96
93 9?
3
2
5
10
I
'11
?
6
4
?
20
'1
j
?0
2
0
?
j
2
2
1
95
95
102
B9
96
101
105
95
95
9'1
95
105
103
105
95
101
102
111
96
98
104
98
1 272
1 211
1 250
10 ?54
1 ??1
19 150
?4 188
| 155
59 155
51 138
49 155
?2 167
52 16?
70 110
19 190
55 155
1 209
1 2?6
71 157
53 149
5Z 150
37 15'1
17 18l
ugl kg
1181 Trichtoroethene
1 - ug/kg
3452 Dibrdrcchtoromethane1. ug/kg3451 1, l,2.Trichtc,roethane?. ug/kg
1 1 82 genrene
1.
1.
1.
ug/kg
145'l trans-1,3-0ichl.oropropene
N.! .
N.D.
N.O.
|1.! .
LancaSIer Laooraiones
2a25 IIew Horlano ?rke
PC gox l2a:5
u9/ k9
rFffii.fl i,T
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i'
Grbuo llo.52?7J9
Hei-cutc,s, Incoroorated
rea .ere.!i ide fo. i/cie.iilon j: t/mbi)l5.tio ;ccrcyraircns : r: ar. r1/:aroq
a!?-"
LCS
RPO
DUP
RPO
I
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i croup xo. 522739
i HercuIes, Incorporated - 0E
I
Satrpte Sampl.eIIOL UNITS
1672 Zirc0.19 ms/ks
6935 Arsenic TR0.?4 mg/ks
6936 seteniw TR0.17 ms/ks
0159 llercury0.028 mslks
0 (1) 103
0 (1) 91
0 (1) 9?
0 (1) 92
LCSLCS DUP
g?
93
87
79
76
B2
85
76
7A
85
81
89
98
B7
93
94
90
58
8'l
LCS LIMITSLOU HI6H
51 149
19 1t9
5? 14e
26 157
65 127
50 137
67 120
73 120
6C 120
67 120
60 120
60 120
79 120
7? 120
68 126
62 120
72 123
62 1?O
61 1?1
75 '125
57 11',l
75 125
75 1?5
1??5 lcL Pesticides in sol.ids
1981 Atpha BHC5. ug/ks'1982 Beta BHc5. uglks198f oetta 8fiC
ug/kg
69 85
76 99
73 39
7D 95
7? 33
71 36
77 92
7t, 88
7q 95
79 91
g7 105
77 93
s2 95
8.r 101
69 78
79 97
t+7 57
81 95
73 3C
'12'!8 Gama 8HC - Lindane1. us/kg
1219 Heptachtor'l . ug/kS
1220 Atdrin1. uglks.l984 HeptachLor Epoxidel. us/ks
1989 Endosutfan I4. ug/kg1222 Diel.dr in1. ug/kg
1965 D0E
'1 . uglkg
1223 Endrin6- uglks
1990 Endosut fan I I9. uglkg'1986 DoDl. ug./ks
1991 Endosut fan SuIfate10. ug/kg
12?1 D0r1. us/ks5017 Endcin Ketone5. u9/k91859 tiethoxychIor40. ug/kS
3025 Atpha chtordane4. uqlksJ026 caflma ChIordane
1.
l.u9/ k9
(1) The resutt for one or both determinations las tess than five times the L00.
(I)h+ffiq*stLlPsgsr'"
LLI Sarnple No. 2538082
CU-4 JUo Hatrix Spike oupticate Grab Soit SampLe
llercutes: Bacchus Pond
ELANK
Batch:9518457080010.80 J mg/kg
Batch: 96i845706001
N-9-
Earch:96',l845708001
x.D .
Eatch:961845711C0?
N.D.
Eatch:96'lBl010lA
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.!.
N.9 -
N.9-
N-0.
N.0 -
N.D.
N.D.
N.D.
N.D.
N.D.
N-0.
N.3_
Lanca5ter Laborarorel
2425 Ne\a noiLdnd P i?
PO BLrr l2l:5
LJncdsie. PA I i6,15-:1,1:
717-5;a .:i00 F.r\ : i '):a laA
TSD
98
9?
94
9?
HS
RPD
6
0
1
0
z1
io
19
'19
'19
18
16
18
17
18
'19
15
'18
12
20
19
'15
2!
Q'-IALITY CONTROL REPORT
Page: 9 of 14
:ee ,eve.se !,oe ,tr :.,t.d-;6!An 1; 1,1-r.a:, ,)t J Ji::rf,.,ai c.,;r'r I O/iiii3:
A Thermo Analytica I Laboratory
LLI sarnple No. 2538082
cu-4 JUo Harnix Spike Dupticate crab soiI Sampte
Hercules: Eacchus Pond
QUALITY CONTR,OL REPORT
Page: 10 of
LCS LIl.TTSLOU HI6H
(iI}Lancaste r Laborato ries
ll
il
it
,l
T
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12357
LCS LCS
LCS OUP RPO
95
!s
RPO
'15
DUP
RPD
4688 TCL SU846 Semivotatites Soil Batch: 96i83st8026
SatrpLe Salpl. eI't9L UlllTS
1988 Toxaphene1,000. u9/k9
1992 Endrin Atdehyde10. ug/kg
1993 PCB-101630. us/kg'1994 PC8-122130. ug/kg
1995 PCS-121250. uslkg
1996 PCB-1?4250. ug/ks
1997 PCB-124840. ug/kg
1998 PCB-',I?5410. ug/kg
1999 PCB-126010. us/ks
1 185 phenoL
ll. us/ks
3753 bis (2-chtoroethyt) ether67. uglks
1186 ?-chIorophenoL33. ug/ks
3754 1,5-dichtorobenzene33. us/ks1187 1,4-dichtorobenzene33. ug/ks
f755'1,2-dichtorobenzene33. ug/ks4690 2-methytphenot67. ug/kg
1691 2,?' -oxybis ('l'ch!.oropropane)
100.uglks
469? 4-rcthytphenot
1 00, us/kS
1188 [-ni trosodi -n'propytamine
67. uglkg
J757 hexachtoroethane67. ug/k.s
3758 ni trobenzene31. ug/ks
3759 i sophorone
67. ug/kg
3746 2'ni trophenol67. uslkg
I
i Group xo. 52289
i HercuIes, lncorporated - DE
9?
72 82
7-\ 84
69 7e
7t 79
74 78
7? 77
69 80
62 70
71 84
75 8l
77 8l
83 9?
7t, S?
BLANK
N .D.
N.D.
[.0.
N.0.
N .9.
[.9.
N -0.
I-l-
N .0.
N.9.
N .0.
N.0 .
H.D .
N.9.
N.9.
N.D.
N.0.
N.D .
N.0 -
N.0.
i3
11
12
5
5
6
15
'11
14
1l
10
7
10
g
77
76
T3
76
76
7t
71
90
77
BO
78
76
5 11?
12 158
z5 lJ4
i 17?
?0 124
32 129
46 123
36 166
5 152
1 230
10 1',13
55 180
2\ 196
29 18?
Lancaster LatJoratone5
M E M B E R 2a25NewHollandPrke
freilf'{ i;i;'i,",.t'::: ; t, -0, u, u,
T
d"; t
I
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-^tco,1 a.. I laoie..1;tioe!l.l:6 ':r ;011 l,9i
tlD?o*
DUP l'1SRPD MS tlSD RPO
I
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A Thermo Analytical Laboratory
LLf sample No. 2538082
Cu-/+ JUD Matrix SpiKc Duplicate 6reb Soi L santrLe
HercuIes: Bacchus Pond
QLIALITY CONTROL REPORT
Paqe: 11 of 14
LCS LCS !_CS L lt'l t 1SI.CS OUP RPO LOIJ HIGH
(il}Lancaste r Laboratories
4689 TCL SU846 SsrivoIati Les/Soi I Batch: 9618]S18026
I
: croup xo. 522739
: Hercutes, !ncorporated - OE
I
I
I
18 57
73 31
71 81
77 8?
73 77
1t t5
e0 87
75 86
17 ',16
81 90
80 89
79 85
79 87
75 81
16 1C
71 7e
59 55
71 77
71 8C
9?. 3e
31 39
Satrpte Safi|PLe
lilDL UNITS
3717 ?,a-direthytphenoL67. uslks3760 bis (2-chIoroethoxy) rethane53. u9/k9
3718 2.4-dichloeophenoI33. us/kg
1189 1,2,4-trichIorobenzene53. u9lk9
J76l naphthatene31. ug/kg
4693 4-chLoroani L ine
U9/Y,g
5762 hexachl.orobutadiene67. us./kg1190 4-chIoro-3-methytphenoI67. us/ks
4694 2-methyl.naphthatenell. uglkg
5763 hexachLorocyctopentadiene170. us./kg
3719 2,4,6- ttichLorophenot67. uslkg1695 2,1,5- tcich(orophenot67. ug/kg1764 2-chLoronapnthaIenell. uglkg
4696 ?-nitroani Line
67 . us,/ks
5766 dinrethyL phthaLate33. ug/ v.g
3765 acenaphthytene53. uq/ks
4697 3-nirroani Line67. uglks
1 191 acenaphthene31. ug./l.g
3750 2,4-dinitrophenoL
1 70. ug/r g
1 192 4-ni tropnenoI
t 70.ug/ ks4698 di benzofuran33. ug/kg
'I 195 2,4-dini trorotuene67. ug/kg
1699 2,6-d1ni trotoIuene67. us/kg
ELANK
N.D.
N.C.
N.0.
N-0-
N.D.
N").
N -9.
!,9 -
N-C.
N.D -
[.9.
N -r -
N.9.
N.D.
N.9,
N.f.
N.r.
R_!.
! _D.
17
1'l
13
6
5
5
9
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10
7
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8
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10
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6
3
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75
77
73
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7A
62
82
79
t)
80
77
56
77
63
75
76
90
52 119
35 1e4
3e 135
21 113
17 116
2!1 116
?2 117
?8, -123
1 100
37 111
39 151
60 I'18
1 11?
33 145
17 115
r 191
1 13?
28 131
39 139
50 158
LanCa5ier L;OCralCrLeS
2425 lle,, Hc land P ke
L-lrc;iier. i{ l:ia5 :-il7-o;b.:l:0:,. l.:ee ra.n'.,v , ,, :a ---, . a,.t rotrevral On5 22 l5 ne. ;r/lc,'g-s
(I)Lancaste r Laborato ries
Q'JAL]TY CONTROL REPORT
2a9e; 12 of ',4
it
il
jl
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jl
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A Thermo Analytical Laboratory
LLI sarnple No. 2538082
CU-4 JUD Harrix spike ouplicare crab soit Sanpte
Hercutes: Bacchus Pond
I crouo xo- 5227'J9
I xercul.es, !ncorporated - DE
I
!
Safrpte SaqDLer,roL uil I Ts
5770 diethyt phthatate67. uglks
5769 4-chtorophenyl phenyt ethe.67. us/kg
3768 ftuorene13. u9/k.9
4700 4-nitroanitine100. uglkg
4701 4,6-dinitro-?-methytphenoI
ug/ks
5772 [-ni trosodiphenytaminR67. us/kg
5773 4-brmphenyl phenyI e(her'100. ug/ks
3774 hexachl.oIobenzene
1 00. u9lk9
'l I 94 pentach L orooheno t170. uglkg
5i75 phenanthrene
33. uslks3176 anthracene33. uglks
4702 carbazoIe51. uglkg
3777 di -n-butyt phthatate51. v9/k93778 ftuoranthene11. u9/k9
1 195 pyrene67. uS/kS
3780 butyt benzyt phthaLate67. us/ks
3781 3,3r-dichtorobenzid!ne130. ug/ks
JZB1 benzo (a) anth.acene51. uslkgl7B4 bis (2'ethythexy[) phthaLate
67. us/kg
3782 chrysenell. us/kg
3785 di'n-octyI phthatate
67. ugltgl7B5 benzo (b) fLuoranthene67. uslkg
5787 benzo (k) ftuoranrhene
us/k9
3788 benzo (a) pyrene67. u9/19l7B9 indeno (1,2,i-cd) pyrene
67.u9/ kg
LCS LCSLCS DUP RPO
ouP !'ts
RPO MS I'ISO RPD
10 83
10 84
779
476
966
1? 73
13 S0
11 8?
?63
10 77
977
77A
11 86
977
't0 91
12 95
568
780
9 101
835
13 't 0l
10 3C
1C 86
']0 78
882
LCS LIHITSLOU HIGH
1 111
25 158
59 12',1
38 122
'1 181
l8 117
5t 1?7
1 15?
1/+ 176
5/+ 120
?7 133
35 133
1 i18
26 137
52 1'15
1 15?
1 26?
li 143
I r58
17 163
t 116
?r. 159
11 ',161
17 163
1 171
BLANK
N.D.
N.D.
N.0.
N.0.
N.!.
ri.D.
N.0.
N-! -
N.D.
N.D.
TN
N.0.
N.C.
N.O.
ll _0.
N.D.
N.D .
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N.!.
N .D.
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N.9 .
N,C.
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59
66
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2425 New Hollano P,ke
PO Bor 12.125
lan(d:ter PA,i 6r"',-.-aaa
717 -GaE_2jAa ;:r 7 I 7-5i6_li3
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3790 dibenz (a,h) anthracene67. uq/kg
3791 benzo (ghi) peryime
67. uglks
0118 Moisture0.06 i: by Ht .
B LANK
N .D.
r,1.9 -
Satch : 961 84Cl16e?00C3A
CONTR,OL REPORT
P3qe: 13 of 14
LCS LINITSLOU it t 6t
1 227
1 219
NI!A T.T.nV
(iI)Lancaster Laboratories
A Thermo An a lyti ca I La bo rato ry
LLI sanple No. 25380E:
Cu-1. JUo Hatrix Spike DupLicate 6rab SoiI Samcr.e
Hercutes: Bacchus Pond
!
icroup xo. 522rJ9
, Hercutes, lncorporated - 0E
I
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91
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2425 lle'v HolLand P ii
PO 8ox 12125
Lan(atiei PA I /5a5 lr.!
il7'6i!-:iiLl F;r - r.65:253r
eu?.J
(I}Lancaster Laboratories
I
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LLr sampl-e No. 25380E2
cU-4 JUo l,'tatrix Sprke oupl"icare Grab Soi L Sanrpte
HercuIes: Bacchus Pond
I
I
i Geoup No. 5??739
I teccuLes, lncorporated - DE
i
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4591 rcl votatites by 8240
4688 TcL SU846 Semivotatil.es Soit
4689 TcL sUE46 semivoLati Les/Soi I
SURRO6ATE SUI'i!.!ANY
TRIAL ID SURROGATE
TCX
DCB
ct -1,?-DcA
c8' to I uene
brts
PhenoL -d6
2 - F tphenot
2 ,4 ,6- tB?
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SURROGAIE LIMITS:.ou H I Gll
50 12050 '120
70 121.
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(iI)La ncaste r Laborato ries
Account No: 06716
Hercutes, Incorporated - DE
Envi ronmentaI Affai rs
Ui lmington 0E 19894
Page: 2 of 11
P.0. 000-'106-8811580-uJK
Ret.
rl
3l
1l
:l
A Thermo Analytical Laboratory
,LI sample No. EL 2558160;ottected: 7/31/96 at 12:40 by BC
;uBni tted: 8/ 3/96 Reported: 8/2?/96,iscard: 9/2?/96
P1-ct 113 Conposite tJater Sanpte
lercutes: Bacchus Pond Project No. U69005.0
AS RECEIVED
::::::i::::::::::iii:::i:;::::::::i::::::::::::::::r::::::i:r:: l'lETHoo
:j:r:iiii::;:..::::: ikfsstls.;ii:j: DETECTI0N LItlIT uNITsANALYSIS NAII{E
by 8260 (Hater)
I
,
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:
t
)
,
t
:
tl
)
i
Ii
t
5
Il
II
)
3
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7
3
5
3
0
z
5
Ch t oromethane
Bromomethane
Vinyl. Chtoride
Ch Ioroethane
l.lethytene Chtoride
Acetone
Carbon Disutfide
1,1 -Dichtoroethene
1 ,1 -D i ch Ioroethane
Ch I oroform
1,2-Dichtoroethane
2- Butanone
1, 1, 1 -Tri ch toroethane
Carbon Tetrachtoride
Bromodi ch Ioromethane
1, 1,?,2-T etrach toroethane
1,2-DichIoropropane
t rans- .l,3-D i ch Ioropropene
Trichloroerhene
DibromochIoromethane
1, 1, 2-Tri chtoroethane
Benzene
ci s- 1,5-Di ch Ioropropene
Bromoform
4-ltlethyL -2-pentanone
2 - Hexanone
Tet rach t oroethene
Totuene
Ch Iorobenzene
Ethytbenzene
S tyrene
Xytene (Totat)
t rans - 1 ,2 -D i ch I oroethene
c i s - 1,2-Di chtoroethene
iOi.ii.iii.
iq:i.:rri,:i' t1.. ::::
l:l:!:i:,:ti:$:r.Sli,ii...i
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ii:riiii,,lI ;Bi;,.,: :,i
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;.N,i,f:i'i...lI. Bi;,,i,:,:
tl.tBtlli.r..
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xiro:ii:.;.:.
::::: :::::::::.::rt aiJt ;:::j::
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t0rij,i.i:.
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3.
5.
2.
3.)
6-
3.
1.
2.
1.
2.
3.
1.
1.
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?.
1.
1.
1.
2.)
1.
,1
1.q
7.
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1.
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t.
2.
2.
u€,/ L
us/ t
us/ [
u9/ [
ug/ t
us/ t
usl I
uS,/ L
ugl t
us/ t
ug/ [
u9/ L
ugl t
usl t
ug/ t
usl t
Ug/ I.
us/ t
ug/ L
us/ L
u9/ t
ug/ L
us/ t
usl t
ugl I'
usl t
u9/ t
u9/ t
us/ t
ugl t
u9/ L
u9/ t
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u9/ |
,l
I
,l
,l
,l
:l
;l
.iii:tt lD.i
ii.:..,Iti,D.i
:ii:,l{iD';
Questions? Contact
Rachel L. Kreamer
your Ctient Services Representativeat [phone]
RespectfuI ty Submi tted
HicheIe l.tcCtarin, B.A.
Group Leader, GC/MS Votatites
MEMBEFl
IMEM
Lancaster Laboratofles
2425 New Holland Prke
PO 8ox 12425
Lancaster PA i7 605-2425
7 17 -656-2300 Fax [phone] See reverse srde for e\planatron of symbols and abbreviations 22,6 Rev 1o/30/ssi?:li
I
I La ncaster Laboratories
A Thermo Analytical Laboratory
1""- sample No. EL 2558160. Cottected: 7/31/96 at 12:40 by BC
l:::"::"::.,:x:'::":"'::",::';. u6eo0s o
I AilALYsrs *Ar.{E
rCL SU846 Semivotati Ies/Uaters
] ilIil-.n,".oethyr) ether387t 2-chtorophenol-883 1,3-dichtorobenzeneIl l:i:!lillli3illlil!f,o 2:nrethyt,phenoL
6681
t::904
fr
3886
*:
i87ZI
392?
tr
I
I
I
I
I
I
Questions? Contact your Ctient
RacheI L. Kreamer
AS RECEIVED
I,I E T HOO
i,,:iii:,,iiiii*.E8tjlIS :,:,,,:,i, oETEcr I oll L I r'l I T uN t rs
u9/ I'
u9/ |
u9/ |
usl t
us/ L
u9,/ t
ugl I'
ugl t
ug,/ t
ug,/ t
ugl t
us/ t
u9/ L
u9/ t
u9/ t
u9/ t
ug/ t
ug,/ t
u9/ t
ug/ t
u9/ t
us,/ t
u9/ L
us/ t
ugl t
u9/ L
ugl I
ug./ t
u9/ L
ugl t
Account No:06716
Hercutes, Incorporated - DE
Envi rorrnental. Affai rs
Ui lmington DE 19894
Page: 3 of 11
P.0. 000- 106-881 rJ80-uJK
Ret.
#
Subnitted: 8/ 3/96 Reported: 8/??/96Discard: 9/2?/96
2,2'oxybi s ( 1 -chtoropropane)
4-methytphenoI
N -n i trosodi -n-propyt ami ne
hexach I oroethane
ni trobenzene
i sophorone
2-ni trophenoI
2,4-di nethyLphenotbis (2-chtoroethoxy) methane
2,4 -di ch I oropheno I
1, 2, 4- tri ch Lorobenzene
naph tha t ene
4-chtoroani I ine
hexachtoroh:tadi ene
4 - ch I oro-3 -methy t pheno L
2 -methyt naph tha t ene
hexach Iorocyc topentadi ene
2, 4,6- tri ch I orophenoI
2,4, 5- tri chIorophenot
2 - ch I oronaph tha I ene
2-nitroanitine
dimethyL phthatate
ac enaph t hy t ene
Servr ces Representat i veat [phone]
MEMBEFl7rclir
Lanca5ter Laboratorres
2425 New Holland Prke
PO Box 12425
Lancaster PA 17 605-2425
7 17 -656-2300 F ax. 7 1,- -656-268l,
Respectfut ty Submi tted
Christine M. RatcLiff
Group Leader, GC/MS
5ee re,,,erse srde for explanatron of symbols and abbreviatrons 2216 Rev. l0/10195
I
A Thermo Analytical Laboratory
,LI sample No. EL 2558160lotlected: 7/31/96 at 12:40 by 8C
luHnitted: 8/ 3/96 Reported: 8/22/96)iscard: 9/22196
tPl -GU 113 Cottposi te later Sample
lercutes: Eacchus Pond Project No. U69005.0
Account llo: 06716
Hercutes, Incorporated - DE
Envi rorunentat Affai rs
Uitmington DE 19894
AS RECEIVED
Page: 4,ol 1'l
P.0. 000- 106-881rJ80-uJK
ReL.
(iI}La ncaste r Laboratories 11
"i1
il
il
I,llr. ANALYSIS }IA}IE
SU846 Semi votat i tes/llaters
3 3-nitroani I ine7 acenaphthene5 2,4'dinitrophenoIZ 4-ni trophenoI7 dibenzofuranL ?,4'dini trototuene5 2,6-dini trototuene7 diethyt phthatate5 4-chtorophenyl phenyt etherI ftuorene? 4-ni troani I ine3 4,6-dinitro-2-methyIphenoI4 N-nitrosodiphenytamine9 4-bromophenyt phenyt ethert hexachtorobenzene6 pentachtorophenoI7 phenanthrene9 anthracene4 carbazote0 di -n-butyl. phthatate7 ftuoranthene9 pyrene0 butyl. benzyI phthal.ate.5 5,3'-dichtorobenzidine0 benzo (a) anthracene8 bis (2-ethythexyt) phthal.ate6 chrysene
'6 di -n-octyl. phthal.ate,1 benzo (b) ftuoranthene,2 benzo (k) ftuoranthene,4 benzo (a) pyrene13 indeno (1 ,?,3-cd) pyrenei1 dibenz (a,h) anthracene,3 benzo (ghi) perytene
!IET HOO
DETECTIOH LII,IIT UNITS
1 ' uglt1' uslt5. uq/t5. uglt
'1 ' ug/t?. uS/ t.1. uglt2. u9/ t?' us/I'1' us/t2' us/t5' us/ t2' us/L2' ugl t
1 ' us/t
1 ' us/t1' uslt
1 ' us/t1' us/t
'l ' uslt
1 ' us/l1. uglt2. uslt2. uS/ L1' uglt?. ug/ L1' ug/t2. ug/t2' uglt2' us/t2' usl I?' usl t2. ug,/ t2. u9/ L
Questions? Contact your Ctient Services Representative
Rachel L. Kreamer at [phone]
I
il
t
t
I
I
I
I
MEMBEFl
,KETT
Lanaaster Laborator{es
2425 New Holland Pike
PO 8ox 12425
Lancaster. PA 17 605-2425
7 17 -656-2300 F ax. 1 1 7 -656 -2 €,8 1
Respectfu[ [y Submi ttedChristine M. Ratctiff
croup Leader, GC/MS
See reverse lide for erplenation of symbols and abbrevratrons.
T
d?I2216 Rev 10/30/95
LABORATORY CHRONTCLE
I
I
(iI}Lancaster Laborato ries
A Thermo Analytical Laboratory
Account No: 06716
Hercutes, Incorporated - DE
Envi ronrnentaI Affai rs
Uitmington DE 19894
08/06/96
08/06/96
o8/06/96
08/06/96
08/06/96
08/06/96
o8/06/96
08/06/96
08/06/96
o8/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/06/96
08/07 /96
0B/06/96
ANAL YS I S
IRIAL DATE AIIO TII.IE ANALYST
1 08/05/96 1801 David A. Hoppman
Page:5 of 11
Tara L. Linvi[[e
Tara L. Linvitlefara L. Linvitte
Tara L. LinviIte
Tara L. Linvitte
Tara L. LinviIte
Tara L. Linvitte
Tara L. Linvitte
Tara L. LinvitIe
Tara L. LinvitIeIara L. Linvitte
Tara L. Linvitl.e
Tara L. Linvitte
Tara L. LinvitteChristine t,l. Contin
Tara L. Linvi Ite
Tara L- LinviIte
Lisa J. Cooke
Hark A. Ratc L i ff
llark A. RatcIiff
,LLI sample No. EL 2558160
ill};.,:,'r',J,'ol^','r'u
at 12:40 bY BC
H:"::"::
":ffi ":"."';:";::'
;"
BPl 15 SOG#:
l;l' AHALY'Ts NA',E
6291
lmt
1744
tliii1751
1753
tliii
1761
riil'
7036
u69005 -0
I'IETHOD
su-846 8260A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
srJ-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
SU-846 6010A
su-846 3005A
su-846 6010A
su-846 6010A
su-846 7470A
su-846 7470A
su-846 35108
su-846 82708
su-846 82708
TCL by 8260 (Harer)
Thatl.ium
A Iuminun
Ant i mony
Bar i um
Beryt I i um
Cadmi un
Chromi un
Copper
I ron
Lead
l.{anganese
N i ckeI
Si Iver
Z inc
lJll StJ846 ICP 0igest (tot rec)
Arsenic TR
Seteniun TR
?307
2307
?307
?307
2307
2307
?307
2307
2307
2307
2307
2307
2307
?307'1330
2307
?307
0?59 l.lercury5713 UIJ SU846 Hg Digest
1658 Net t i S. litarkaryan?122 NeLLi S. Markaryan
0815 BNA l.,ater Extract ion
It*e +:i :r:i: :iltrt::l t::iffi::i:
08/05/96 0730
08/09/96 0540
08/09/96 0540
I
I
I
I
I
I MEMBERKrtr
Lancaster Laboratones
2425 New Holland Prke
PO Box 12425
Lancastet PA 17 605-2425
7 l7-656-2300 F ax.. 7 1l -656-2681 nBaB5 d'PSee reverse srde for explanatron of symbols;nd abbrevrations 2216 Rev
QUALfTY CONTROL REPORT
(I}La ncaster Laboratories Il
il
'll
',1
I
I
MS LCS LCS
MS I.ISO RPD LCS DUP RPO
6of 1'l
LCS LII.tITSLOI' HIGH
I
A Thermo Analytical Laboratory
LLr sample No. 2558160
8P1-GU 113 Corposite Uater Sanpte
Hercutes: Bacchus PonC Pro.iect No. U69005.0
Group No. 527529
Hercutes, Incorporated - 0E
Sarpt e
I'tDL
Sample
UNITS
L by 8260 (Hater)
Ch tonomethane5' ug/t
Sromomethane3. us/t
Vinyt ChIorideZ. us/t
Ch Ioroethane3' ug/t
I{ethytene ChLocide
2. u9/ I'
Acetone6. us,/ L
Carbon Disutfide3. ug/t
1,1-Dichtocoethene
1 - ug/t
1,1-DichtoroethaneZ. ug/t
Ch t oroform1. us/t
1,2-Dichtoroethanez' ug/t
2-Butanone3' uslt
1, 1, 1 - Tri chloroethane
l ' ug/l
Carbon Tetrachtoride
1 ' u,/l
Bromodi ch Iorornethane
1 ' us/l
1, 1,?,?'T elrach Ioroethane2. ugl t
'l ,2-0ichloropropane
'1 ' ug/t
t rans - 1 ,3 -D i ch t ocopropene
1 ' ug/LIri ch Ioroethene
1 ' us/[
D i bcomoch Ioromethane?' us/ t
1, 1, 2'Tri ch Ioroethane?' ug/t
Benzene
1 ' uslt
ci s-'1,3-D i ch Ioropropene
'I ' us/t
ELANK
Eatch: I962181A8
[.0.
N.D.
N.0.
N.0.
H.D.
N.D.
N.D.
N.D.
N.D.
N.D,
N.0.
[ -0.
t{.0.
N.D .
It.D.
N.D.
N.D.
N.D.
N.D.
N.0.
N.D.
N.0.
lil .D.
99
75
85
62
79
108
42
66
82
95
94
116
91
89
92
91
81
85
85
92
8B
80
86
101
95
94
69
89
8B
97
81
93
108
106
99
109
105
103
87
94
9?
100
103
94
92
99
?
24
10
10
13
20
79
?o
12
13
12
16
18
17
11
1
14
I
16
1?
7
14
t4
I
I
I
I
I
I
t
I
t
I
T
MEMBEFlTmri
Lancaster Laboratones
2425 New Holland Prke
PO 8ox 12425
Lancasier PA I 7605-2425
7 17 -656-2300 Fax: [phone] l d?Ii5ee reverse side for explanatlon of symbols and abbrevratrons 2216 Rev. 1O/3O/95
I
I La ncaste r Labo rato ries
,A Thermo Analytical Laboratory
Page: 7 ol 11
1"- sample uo. 2558160
8P1-Gl,J 113 Conposi te Uater Sampl.e
!r,"r"rt"", Bacchus pond project No. U69005.0
ISampte Sarpl.eIiIDL U}I I TS
f,l'*'o'L^
08 4-Methyl.-2-pentanone
l]: '.","*rill09 Tetrachtoroethene1. us/t
l'I,,1"."-::*.1. us/t
i'f'n''*'iiii1. us/t10 Xytene (Totat)
l]i.-".,, jlf l"n, "."",n"""
95 cis-1,2-Dichtoroethene
t*x ;:
57. ug/t
H;", us/r
2.2 us/ L
Ilil-;:
Chromi um
llii. ;:
I ron
ti:".."" ;:
2.9 usl L
li::: us/,
3.6 us/ L
croup No. 527529
Hercutes, Incorporated - DE
DUPRPD I{SBLANK
N.0.
[.0.
N.0.
N.D.
il-D_
N.D.
N.D.
fi,l .D.
11.0.
N.D.
N.D.
Batch:962191848002
N.D.
Satch:962'191848002
0.101 J mg.Zt
Batch:962191848002
il.D.
Batch:962191848002
0.0366 J mg/|.
Eatch:962191848002
N.0.
Batch:962191848002
H.D.
Batch:962191848002
r'1.D.
Batch:962191848002
N.D.
Batch: 96219'1848002
0.0295 J mglt
Batch:962191848002
|t.0.
Satch:962191848002
N.D.
Batch:962191848002
N.D.
Batch:9621918480020.830 ns/L
t{s LCS LCSHSO RPD LCS DUP RPD
LCS LII'IITS
LOU HIGH
80
80
80
80
80
80
80
80
80
80
80
80
80
80
(1)
0 ('1 )
0 (1)
0 (1)
(1)
0 (1)
(1)
0 (1)
0 (1)
(1)
2
0 ('l )
(1)
93 100
118 99
117 98
75 101
79 92
85 99
86 99
83 97
84 99
78 93
81 96
97 98
100 101
108 109
99 100
97 98
96 97
103 104
101 'l 03
100 99
97 97
99 100
98 99
110 110
88 87
the LOo.
18
18
27
15
t4
t4
16
16
18
t/
1
1
1
1
'I
1
'1
1
1
0
1
0
0
0
98
104
'1 06
100
98
97
105
102
104
99
100
101
111
105
120
120
120
120
120
120
120
120
120
120
120
1?0
120
120
jjnc Batch:962191848002lZ. us/ t o.O4t ms/ r. z
rlf r""uta ro. onu or both dererminations Has less than five times
I
MEME!ER7emI
Lancaster Laboratories
2425 New Holland Pike
PO Box 12425
Lancaster PA 1 7605-2425
717-656-2300 Fax:[phone] See reverse srde for explanatron oi symbols and abbre,rrauons d''
QUALITY CONTROL REPORT
2216 Re,r 1O/3O/95
QUALTTY CONTROL REPORT
(iI)Lancaster Laboratories Page:
1
2
2
1
2
1
1
2
0
3
1
1
2
0
3
1
1
0
1
1
I
I
I
I
I
t
I
I
118of
A Thermo A,nalytical Laboratory
LLr sample No. 2558160
8P'l -cU 1'13 Conposite lrater Sampte
Hercutes: Bacchus Pond Project No. U69005.0
Group No.527529
Hercutes, Incorporated ' DE
(1 ) 99 100
0(1) 97 97
0 (1) 95 97
48 47
91 93
92 93
76 78
77 80
80 83
88 90
74 76
90 91
89 9?
67 71
97 100
94 96
1 15 114
67 66
88 9'l
93 9l
79 81
86 87
u77
five times the LOo.
"T
Sampl e Sanpl eiIDL U}I I TS
'senic TR2.7 us./ t
;teniun TR?.7 usl I
!fcury0.43 us,/ t
:L StJ846 Semivotati Ies/Uaters
phenoI
1 ' us/t
bis (2-chtoroethyt) ether1. ug/t
2- ch IorophenoI1. ug/L
1 ,3 -d i ch L orobenzene1. us/L
1,4-dichtorobenzene1. uslt
1 ,2 -di ch torobenzene1. uslt
2-rnethytphenot?. ug/L
2,2'oxybis (1 -chtoropropane)Z. us/ t
4-methytphenoI2' u'/t
il -ni trosodi -n-propyI ami nez' ug/ t
hexach Ioroethane2. us/t
ni trobenzene
'l ' us/t
i sophorone1. us/|.
2-nitrophenotZ. us/ t
2,4-di methytphenot1. u9./[
bi s (2-chtoroethoxy) methane1. ug/t
2, 4 - di ch t oropheno I?' ug/t
1, 2, 4- tri chLorobenzene
1 ' ug/t
naph tha I ene1. u9/1.
4-chtoroani I ineZ. us/t
BLANK
Batch: 96219'1848002
N.0.
Batch:' 962191848002
Itl -D.
Eatch: 962195713001
N.D.
Eatch: 962181JM026
lt.D.
H.D.
N.0 .
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
H.0.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.0.
N.0.
N.D.
DUPRPO t4S
MS LCS LCSIISD RPD LCS DUP RPO
LCS LIMITS
LOU HIGH
80 120
80 120
80 120
0
0
3
101
98
96
2
2
0
3
4
4
2
3
0
3
5
2
?
1
?
3
1
3
1
8
47 48
94 92
94 93
76 76
77 78
80 81
89 90
76 74
91 90
91 88
65 66
99 98
96 94
112 112
71 69
91 90
93 92
78 78
86 86
77 78
5 112
12 158
23 134
1 172
20 124
3? 129
46 tZ5
36 166
5 152
1 230
40 'l 13
55 180
21 196
29 182
3? ',119
33 184
39 135
44 142
21 133
17 116
I
I
t
I
I
,oi3.,es d's I
I
for one or both determinations was tess than
Lancasier Laboratofles
2425 New Holland Pike
PO Box 12425
Lancaster PA 17 605-2425
717-656-2300 Fax' 7 17 -656-?681
MEMBEFI
r1<tE 5ee re'/erse side for explanatron of symbols and abbre'/iations
I
I (I}Lancaster Laborato r ies
A Thermo Analytical Laboratory
9of 11
1"", sample No. 2558160
BPl-ct, 113 Corposite Uater Sampte
!X"r.rt"., Bacchus Pond project No. U69005.0
Group No. 527529
Hercutes. Incorporated - DE
68 69
96 97
84 86
57 61
95 94
97 96
86 BB
92 94
90 84
85 86
62 61
44 46
89 88
104 108
99 102
B7 89
93 93
88 88
89 94
112 1',1 1
89 89
65 65
96 96
84 85
60 59
98 95
98 97
88 87
93 91
84 84
86 86
r08 103
49 47
89 89
107 106
101 97
85 80
95 95
90 90
89 87
1?5 120
90 90
Page:
LCS LIMITS
LOI.' H I GH
1 ?4 116
0 ?? 147
1 28 123
21100
4 37 144
2 39 151
2 60 118
2 53 143
112
145
Ir.*," sanpteI,IDL UIIITS
1 ,,:'*u"n tolotxrtadi ene
i72 4-chtoro-5-methyl.phenot
I i;":::::ii:i.i:,:::".,
"."3' ug/t
l,i:',: i',',i: i i
"
: ":: "
:. :
1 ' us/t
l;i "fi,""::li::"'","
'o1 dimethyt phthatate
l;:'*"*'riii""
-IEL St,846 Semivotati Ies/lJaters
l;;';;;;;";#r;
t\7 acenaphthene
I]i,, .,"'iiii*",
t1? 4-ni trophenoI5- uq/[I di b..rrof ,.,i"rt
,t' i, o.o, n, i?'"1".'*""z' us/ [
I':;I;'ffii":",:"z' u'/t
i';;::::::::11" """'r e'lher
)09 4-nitroanitine
I
ti,
u- o, ", il/olz-**,vt pr,*ot
,14 t{-ni trosodiphenytamine2' u9/[I
BLANK
f .0.
N.D.
N.D.
N.D.
ll .0.
N.D.
N.D.
N.0.
N.D.
N -0.
Batch: 96218tJM026
N.D.
N.D.
N .0.
N.0.
N.D.
N.0.
N.0.
N.D.
N.0.
N.D.
N.0.
N.D.
N.D.
DUPRPD MS
its Lcs LcsI.ISO RPD LCS DUP RPD
70 71
90 91
5853101
9189233
6
1
2
5
1
3
3
?
U
0
s
1
0
07143
1 47 145
5 1 ',191
31132
0 28 131
1 39 139
5 50 158
4 1 ,114
0 ?5 158
0 59 121
3 58 12?
31181
0 38 147
I
I MEMBEFIffiin
Lancaster Laboratofles
2425 New Hollanci Prke
PO Box 12425
Lancastet PA 17 605-2425
717-656-2300 F ax 7 1 t- -555-2681 2216 Rev ro/30/e5 d}!
QUALITY CONTROL REPORT
See reverse srde for explanation of symbols and abbrevratrons
QUALITY CONTROL REPORT(I}Lancaste r Laboratories I
I
I
I
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DUP I.IS LCS LCSRPD I.IS I.ISD RPD LCS DUP RPO
10 of 11
A Thermo Analytical Laboratory
LLI sample No. 2558i60
BPl-GtJ 113 Composire tJater SantPte
HercuIes: Bacchus Pond Project Ho. U69005.0
Group No. 527529
Hercutes, tncorporated - DE
86 85
83 83
42 42
89 88
86 85
92 94
91 91
88 90
97 96
105 104
75 7?
90 90
107 1 06
95 95
110 105
91 88
98 96
86 86
85 BB
87 91
82 87
Sarnple SaoPLeI.IDL UII I TS
4-bromophenyt phenyl etherz' u9/ t
hexach Iorobenzene
1 ' ugll
pentach torophenot1. ug,/L
phenanthrene
1 ' us/t
anth racene
1 ' u'/t
carbazo I e
1 ' u'/L
di -n-butyi phthatate
'1 ' us/t
f Iuoranthene
1 ' u'/L
pyrene
1 ' us/L
butyl benzyI phthatate?' u9/ t
3,3' -di ch torobenzidi ne2. us/L
benzo (a) anthracene
1 ' u,/L
bis (2-ethythexy[ ) phthatate2' u9/ t
chrysene1' us/l'
di -n-octyt phthatate?' u9/ t
benzo (b) fIuoranthene?' u9/ t
benzo (k) fIuoranthene2' us/t
benzo (a) pyrene2. ug/t
indeno (1 ,2,3-cd) pyrene2' us/l
dibenz (a,h) anthracene2. us/ t
benzo (ghi) perylene?. us,/ t
LCS LIMITSLO\.' H I GHBLANK
N.D.
H.D.
N.D.
N.D.
N.D.
N.D.
1. J ug/L
N.D.
N.0.
N.D.
N.0.
N.D.
N.D.
N.D.
N,0.
N.D.
N.D.
N.D.
N.D.
N.D.
N.0.
1
U
0
2
0
3
0
2
1
0
.:
0
0
0
4
J
2
,|
4
4
6
88 BB
85 86
82 75
90 91
88 89
93 9?
93 92
91 90
101 100
104 102
72 72
94 92
110 108
99 97
106 106
90 91
99 99
89 89
9? BB
96 91
91 85
155
01
914
154
127
140
11
126
1s2
lt
01
?33
28
217
04
224
1 11
017
41
61
61
I
I
I
I
I
127
152
176
120
lJ5
137
118
137
115
152
262
t4J
158
168
146
159
IOJ
IOJ
171
227
?19 I
I
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Lancaster Laboratofles
2425 New Holland Prke
PO 8ox 12425
Lanca5ter, PA 17 505-2425
7 17 -656-2300 Fax [phone]
MEMBEFl
5ee re,/e15e srde for exoianatron of svmDols and abbrevratrons 2215 Rev
I
(I)La ncaster Laborato ries
A Thermo Analytical Laboratory
Page: 11 of 11
1"", sampre No. 2558160
8P1-Gu 'l13 Cooposite Uater Sampte
!U"r.ut"., Bacchus Pond project |,lo. U69005.0
I
::
I 4618 rcLSU846 Semivotatiles/uaters
TRIAL ID
I 46tg TcLSr.r846 Semivotati t,es,/rJaters
Group No. 527529
Hercutes, Incorporated - DE
6291 TCL by 8260 (Hater)
SURROGATE SUHI'IARY
SURROGAIE
2'FtphenoI
Phenot -d6
2,4,6-TSP
Nitrobz-d5
2-Fbiphnyt
Tpheny t d1 4
DB FM
'l ,2-DCA-d4d8-totuene
4.BFB
RECOVERY Z
58
39
80
92
a)
81
113
109
94
99
SURROGATE LIIiIITSLOU HIGH
21 10010 9410 123
35 11443 11633 141
86 11880 12088 11086 115
I
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I
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I
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I
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I
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I
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Lancasler Laboralories
2425 New tlolland Pike
PO 8ox 12425
Lancastet ?A 17 605 -2425
7l 7-656-2300 Fax.. 7 11 -65o-2631
QUALTTY CONTROL REPORT
MEMBEFI
\co ro ,-'5p srdc lor e\piandlron a' iymbols and acbrevra(,cns 2216 Rev 10/10,,95 d?
(iI}La ncaster Laborato ries
A Thermo Analytical Laboratory
Lr sample No. EL 2558161
ANALYSIS NAIIE
TCL by 8260 (pater)
Hercutes, lncorpocated
ERI'l - Rocky l.lountain
Cottected: 8/ ?/96 at 14:00 by 8C
l*::::'' 3',r1r1i2
Reported: 8/2?/e6
ff::,"::"-,":::.,':::.":::;".. N. u6e005 0
Quest'ions? Contact your Ctient
RacheI L. Kreamer
03:2?:0? D 0002 4603 169.00 0001 6900 ASR000
Lancaster Laboratofles
2425 New Holland Prke
PC Box 12425
Lancaster. ?A 11 605-2425
717-656-2i00 Fax: [phone]
AS RECEIVED
:::::::::::::::i::::t:::::::::t::::::::l:: :.:: :11:::rl:' M E T H 00
i::::::::::ii::i:ftE$IlLr5,::r]::r DETECT I or'i L I r'r I r uN t r s
See Page
Account No: 06716
Hercutes, Incorporated - DE
EnvironmentaI Affairs
Ui lmington DE 19894
Joseph Ke[ [er
Brent Robinson
RespectfuI Ly Submi tted
Ramona V. Layman, Group Leader
ICP I'letats/Leachates
Sr-,e revl,rse srde for explanatron of symbols and abbrevratrons 2216 Rev ro/ro/e5 d'9
I
6291
T
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ATT[:
ATIH:
t I COPY TO
1 COPY TOI
I
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Servi ces Representat I ve
ar (717) 65o-2300
126/[phone]
MEMBEFl7ffitr
(iI)Lancaster Laborato ries
Account t{o: 067'16
Hercutes, lncorporated - DE
Envi rorrnentaI Affa i rs
tli tmington DE '19894
Page: 2 of
P.0. 000- 1 06-88'l 7380-r,JJK
Ret -
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,A Thermo Analytical Laboratory
,LI Sample No. EL 2558161lottected: 8/ ?/96 at 14:00 by BC
tuHnitted: 8/ 3/96 Reported: 8/22/96)iscard: 9/2?/96
Fiel.d ELank Grab lJater Sampte
ilercutes: Bacchus Pond Project No. U69005,0
I. ANALYSIS NAI',IE
by 8260 (Hater)
5 Ch [oromethane7 Bromomethane5 Vinyt Chtoride8 Chtoroethane'I t{ethytene Chtoride2 Acetone3 Carbon Disutfide0 1,1-Dichtoroethene3 1,1 -Dichtoroethane
6 Chtoroform2 1,?-Otchtoroethane5 2-Butanone8 1,1,1-Trichtoroethane9 Carbon Tetrachtoride6 Brornodichtoromethane1 1,1,2,2-TetrachLoroethane4 1,2-Dichtoropropane6 trans-1,3-0ichloropropene5 Tri ch Ioroethene1 DibromochtoromethaneI 1,1,2-Trichtoroethane1 Benzene7 cis-1,3-Dichtoropropene9 BromoformI 4-ilethyL-2-pentanone9 2-HexanoneL9 Tetrachtoroethenet7 Tot uene3 Chtorobenzene5 Ethytbenzene8 Styrene0 Xytene (Tota[ )t? trans-1,2-Dichlocoethenet5 cis-1,2-0ichtoroethene
AS RECEIVED
l.rETHOo
:i;iij:riii:i:i::i$ggP,.li,f.:5i:i::11 DETECT I 0N L I tr I T uN I Ts
ugl t
us,/ t
us/ t
u9/ t
us/ L
ug/ L
ug,/ L
u9/ |
ug/ t
us/ t
u9/ t
us/ t
us/ |
ug/ L
us/ t
ug,/ L
us/ L
usl t
u9/ L
u9/ L
u9/ t
u9/ I'
us/ t
u9/ I'
us/ [
us/ [
us,/ t
us/ I'
us/ t
ugl t
us/ t
ug,/ L
us/ t
ug/ t
youn Ctient Services Representative
at [phone]
Questions? Contact
Rachet L. Kreamer
Respectfut Ly Submi ttedllichete l.lcCtarin, B.A.
Gr^oup Leader, GC,/MS Votati Ies
MEMBEFl7Xm
Lancaster Laborato(es
2425 New Holland Prke
PO Box 12425
Lancaster, PA 17605-2425
717-656-2300 Fax: [phone] See re./erse srde for explanation of symbols and abbre'rrations 2216 Rev. 1O/3A/95
t
I (iI)La ncaster Laborato ries 3of 6
I"", sample No.
Coltected: 08/0?/96 at
!ru*,..*, os/o3/e6
A Thermo Analytical Laboratory
EL 2558161'14:00 by 8C Account No: 067'16
Hercutes, Incorporated - DE
EnvirormentaL Affairs
Ui lmington DE 19894
Fietd Btank Grab Uater Sampte
Hercules: Bacchus PoM Project ilo. U69005.0
BPFBK SDG#:
I
I
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t
I
CATNO A}IALYSI S NAIIE
6291 TCL by 8260 (Hater)
fiETHOo
su-846 8260A
Lancaster Laborator'es
2425 New Holland Prke
PO Box 12425
Lancaster PA 11 6A5-2425
7 17 -656-23A0 Fax [phone]
ANALYS I S
DATE AND TIt.IE ANALYST
08/05/96 1654 Thomas C. Lehman
,l
I
i
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I
MEMElEFI
TXriE
I.ABORATORY CHRONICLE
I
Se? re',,erse srde for e'c.anatron of svmbols ano aoore'rtaticns
QUALITY CONTROL REPORT(I}lt
'll
il
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DUP MS LCS LCSRPO MS I'ISD RPD LCS DUP RPO
La ncaste r Laborato ries
A Thermo Analytical Laboratory
Lan(aster Laboratofles
2425 Neur Holland Prke
PO 8ox 12425
Lancaster PA 17 605-2425
7 I 7-656-2300 F ax. 7 17 -656-2621
Page: 4 ol
LLI sample No. 2558161
Fiel.d BLank Grab tJater Sampte
Hercutes: Bacchus Pond Project No. U69005.0
SanpI e
UNITS
Group No: 527529
Hercutes, Inconporated - 0E
I
LCS LIMITS
LOIrJ H I GH
L by 8260 (Llater)
BLANK
Batch: I962181A8
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.0.
N.D.
N.D.
N.D.
N.D.
[.0.
N.D.
N.0.
N.D.
N.0.
N.D.
N.D.
N.D.
N.D.
N.D.
Ch Ioromethane3. uS./ L
Bromometh6ne3. ug/t
VinyI Chtoride2. us/t
Ch I oroethane3. us./ t
ilethytene Chtoride2' us/t
Acetone6. us/L
Carbon Disutfide3. uS,/ t
'l ,1-Dichtoroethene1' us/[
1,1-0ichtoroethane2' us/t
Ch I oroform
1 ' us/t,l,2-Dichtoroethane
2' us/t
2- Eutanone5. us,/ [
1, 1, 1 -Trichloroethane
1 ' u'/t
Carbon Tetrachtoride1. ug/t
Bromodichtorofiethane1. uS/|,
1, 1, 2, 2- f "t.achtoroethane2. us,/ t
1,2-Dichtoropropane1. uS,/t
trans- 1, 5'D i ch Iocopropene
1 ' usll
Trichtoroethene
1 ' us/t
Dibromochtoromethane?. ug/L
1, 1, 2-Trichtoroethane2' ug/t
Benzene1. us/t
ci s- 1,3-D i ch Ioropropene1. us/t
99
75
85
62
79
108
42
66
82
95
94
'l '16
91
89
92
91
ot
85
85
92
oo
80
B6
101
95
94
69
89
QA
97
81
93
108
105
99
109
'1 05
103
ol
92
100
103
94
9?
99
2
?4
10
10
IJ
20
79
20
12
IJ
12
16
18
17
11
4
l4
8
16
12
7
14
t4
MEMBEFI
rEHTI See reverse srde for exolanatron oi symoois and abbre,/latrons 22,6 Rev loBa/ss d3 |
I
t Page: 5 of
A Thermo Analytical Laboratory
ILLr sample No. 2558161
ff::,:::",::::..':::.'":::;".. N. u6e005 0
T
(I}La ncaster Labo rato ries
Group No. 5?7529
Hercutes, lncorporated - DE
. - Sampte Sarpte
,J::",.,".,
ulrITs
1. us/t"ii
,:.:::*j:^"**
09 Ietrachtoroethene
[i"'*"':;;:15 Chtorobenzene
'l ' ugll
,frl't'o*ilii1. ug/t
l',:::::, :l!;i::, "."",^"""?' ug/t05 cis-1,2-Dichtoroethene
l' us/t
t
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DUP MS LCS LCS LCSRPD MS I,ISD RPD LCS DUP RPD LOU
LII'IITS
HIGHBLANK
N.D.
N.D.
il.D.
N.D.
1r.0.
N.D.
N.D.
N.D.
N.D.
ll.D.
[.0.
93 100
'l 18 99
1't7 98
75 101
79 92
85 99
86 99
83 97
84 99
78 93
81 96
1
18
18
?7
15
t4
14
16
16
18
MEMBEFl7XmI
Lancaster Laboratofles
2425 New Holland Prke
PO Box 12425
Lancastet PA 17 605-2425
717 -656-2300 Fax: [phone]
QUALITY CONTROL REPORT
See reverse srde for exoianatrofl oi s'/moois and abbre,ratrons 22r6 Rev 1o/3o/s5 dt,
QUALTTY CONTROL REPORT
1T
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88
86
(iI)Page: 6 ofLa ncaster Laboratories
HIGH
118
120
110
115
A Thermo Analytical Laboratory
LLI sample No. 2558161Fietd Btank Grab tJater Sampte
Hercutes: Bacchus Pond Project No. U69005.0
6291 TCL by 8260 (Hater)
Lancaster Laboratofles
2425 New Holland Prke
PO Box 12425
Lancaster PA 17 605-2425
7 17 -656-2300 t ax: 7 17 -656-268 1
I
dltMEMBEFt
t4Km
Group No. 5275?9
Hercutes, Incorporated - DE
2216 Rev l0/10/95See reverse srde for e-\planatron of symbols anci abbre'riatrons
CAT
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Questions? Contact your Ctient Services Representative
Rachel L, Kreamer a\ [phone]
03:19:57 D 0002 4 126436 527529603 49.40 00022090 AsR000
Lancaster Laboratofles
2425 New Holland Prke
PO Box 12425
Lancrtier. PA 17 605-2425
717 -656-2300 Fax 11 ,-.556'2521
Account No: 06716
Hercutes, Incorpocated - DE
Envirormentat Affairs
Uitmington 0E 19894
AS RECEIVED
IlETHOO
OETECTION LII,(IT UNIIS
Respectfu[ [y Submi tted
Ramona V. Layman, Group Leader
ICP lietats/Leachates
LLI sampl-e No. EL 2558159Cottected: 7/30196 ar 08:45 by BC
suunitted: 8/ 3/96Discard: 9/?2196
8/?2/96
BP1-GU 38A Co.rposite Uater Sarpte
Bacchus Pord Project ilo. U69005.0
P.0. 000''106 -881 1380-r,,JK
ReL.
I Ot 5
17??
'1743
..1744
1746
1747
1749
1751
1753
1754
1755
1758
1761't76
177?
705s
7036
0259
AIIALYS I S IIAI.IE
Thatl.iun
Atunintm
Ant i mony
8ar i um
Eeryt I i un
Cadni un
Chromi r.un
Copper
I ron
Lead
lilanganese
Ni ckeI
Si Iver
Zi nc
Arsenic TR
Setenium TR
f{ercury
,,,,.r,, 250.
19;000,
,.a::',,'170
:.,., N.D.
't70.
57.
15.))
t.J
2.7
4.3
3.8
30.
18.
15.
5.4
3.6
12.
2.7
2.7
0.43
u9/ t
u9/ t
usl t
u9/ t
u9/ t
usl t
ugl t
ug/ t
ugl t
u9/ t
u9/ t
u9/ t
us/ t
usl t
ugl t
ugl t
u9/ t
The quantitation timit for mercury nas increaseddue to the nature of the sarpte matrix.
1 CoPY TO Hercutes, Incorporated
1 CoPY TO ERM - Rocky llountain
t:li
;..li
ATTN: l'1r. Joseph Ketler
ATTN; Mr. Brent Robinson
I
I
I
See re,/erse srde Ior expianatron of;ymbol; and abbrevrdtLons 2216 Rev,Orr.r* d'9
&&&
(I}La ncaste r Laboratories
LABORATORY CHRONICLE
Page: 2 o{ 3
=l
A Thermo Analytical Laboratory
i'.
;.'
t-
I.
LLI sample No. EL 2558159Cotlected: 07/30/96 ar 08:45 by BC
suhnitted: 08/03/96
BP'l-GU 38A Corposite Uater Sarpte
Account llo: 06716
Hercutes, Inco.porated - 0E
Environmentat Affairg
Uitmington 0E 19894
t
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Xercutes: Eacchus Pond Project Io.
BP38A SD6#:
CATI'10 AI{ALYSIS llAl'lE
1722 Thattiun
1743 Att.lttinun
1744 Antirony
'l 746 8ar i un'1747 Beryl,Liuun1749 Cadmiun
1751 Chromiun
1753 Copper
1754 lron
1755 Lead
1758 litanganese
1761 llicke(
1766 Si tver
1772 Zinc
1848 tl!,J SU846 ICP Digest (tot rec)7035 Arsenic TR7036 Setenitrn TR
0259 ttercury5713 tlu SU846 H9 Digest
AIIALYS I S
TRIAL OATE A}ID TIIiIE
1 08/06/96 ?3031 08/06/96 ?3031 08/06/96 23031 08/06/96 ?3031 08/06/96 ?3031 08/06/96 ?3031 08/06/96 23031 08/06/96 2303'r 08/09/96 01501 08/06/96 23031 08/09/96 01501 08/06/96 ?3031 08/06/96 23031 08/06/96 23031 08/06/96 13301 08/06/96 23031 08/06/96 2303
1 08/07/96 16551 08/06/96 2122
ANALYST
Tara L. Linvitte
Tara L. Linvi t Le
Tara L. Linvi Lte
Tara L. Linvitte
Tara L. Linvi t Le
Tara L. Linvitte
Taca L. Linvi tte
Tara L. Linvitte
Ju(ie A. Staughenhoupt
Tara L. Linvitl.eJutie A. Staughenhoupt
Tara L. Linvitte
Tara L. Linvitte
Tara L. Linvitte
Christine t'l. Contin
Tara L. Linvitte
Ta.a L. Linvitte
Hett'i S. ilarkaryan
XeLLi S. Markaryan
u69005 .0
l,lETH@
su-846 6010A
su-846 6010A
su-E46 6010A
su-846 6010A
su-846 60'l0A
su-846 5010A
su-846 6010A
se-846 6010A
su-846 6010A
su-846 6010A
su-846 6010A
su-845 60'l0A
su-846 6010A
su-846 6010A
su-846 1005A
su-846 6010A
su-846 6010A
su-846 7470A
su-846 74704
t.-
,!
tl
MEMBEFlrI3rir
LanCaSter LabOratOrteS
2425 New Holldnd Prke
PO 8o\ 12425
Lancdstel PA 11 6A5-2J25
717-656-2300 Fax [phone] ,or,orr, {}5ee reverse:rde for erplanal,on of symbols and 3ilbre',latronj 22l5 Re'.
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(iI)La ncaster Laboratories Page: 3 ofA Thermo Analytical Laboratory
LLI sampLe No. 2558159
SP1-cU 58A Conposite Uater Sarnpte
Heccu(es: Bacchus Pond project [o. U69005.0
:'.' ' ,:: .. Sanple Sarpte
i ,rL ur r TS
;1722 Thal.tiun170. ug/t
.1743 Atuninun57. uglt
.1744 Antiannyi 15. us/t
:1746 Baril.[n| ?.? u9/ t
.1747 Beryt t iuni 1.3 us/t
:1749 Cadmimt. ?.7 u9/ t
.1751 Chromiun: 4.3 ug/ t
11753 Copper; 3.8 u9/ t11754 lroni- 30. ug/ t
1755 Leadi 18. u9/ t
i1758 !{anganesei: 15. us/ t
i.tzet rictet
: 5.4 u9/ t
i1766 Si tver1' ,' 3.6 uslt
1.1772 Zinci tz. us/t
7035 Arsenic TRi 2.7 ug/t
17036 Seteniun TRi ?.7 us/ t
0259 liercury, 0.43 uSlt
BLA}IK
Batch : 9621 9'l 848002
N.D.
Eatch:9621918480020.101 J,nglt
Eatch:962191848002
I.D.
Barch: 962191848002
0.0366 J mglt
Eatch:962191848002
r,t.D.
Batch:962191848002
N.D.
Batch : 962 1 91 848002I.D.
Batch:962191848002
x .0.
Batch: 962191848002
0.0295 J ms,/t
Batch:962191848002
N.D.
Batch:96?191848002
I,r. D .
Batch:962191848002
N.D .
Batch:9621918480020,830 ms/t
Batch : 9621 91 848002
0 -047 rnS/ t
Batch:962191848002
N .0.
Batch: 962191848002
N.0.
Batch:952195713001
N.D.
Lancaster Laboratorres
2425 New Holland Prke
PO Box 12d25
Lancasier PA 17605-242 -\
717-556-2100 Fax 7 17 -a56.2a31
DUP tts LCS LCSRPD IIS I.{SD RPO LCS DUP RPO
LCS LII.IITSLOU }II GH
80 120
80 120
80 1?0
80 120
80 120
80 120
80 120
80 120
80 120
80 1?O
80 120
80 120
80 120
80 120
80 120
80 120
80 120
(1) 97
0 (1) 100
0 (1) 108
0 (1) 99
(1) 97
0 (1) 96
(1) 105
0 ( 1) ]01
0 (l) 100
(1) 97
299
0 (1) 98
(1) 110
288
(1) 99
0 (1) 97
0 (1) 95
98
101
109
100
98
97
104
103
99
97
100
99
110
87
100
97
97
98
104
106
100
98
97
105
102
104
99
100
'101
ltt
105
101
98
96
1
1
1
1
1
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1
1
0
1
0
0
0
0
0
3
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'.(1) The resutt
,-
'i:-:,.
i
.
for one or both determinations Has Iess than five tir$es the LOQ.
rigtr
QUALITY CONTROL REPORT
Group llo. 527529
Hercutes, Incorpocated - 0E
S:e .eve.se ;,;3 :6r s1p';a31 21 ci svmbols dnd dobre,,ralron!2216 Rev.,Orror* d?
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(I)Lancaster Laboratories
A division of Thermo Analytical lnc.
LLI sanple No. EL 2562490cottecred: 8t 9/96 at 16:15 by BR
Subritted: 8/10/96 Reported: g/ L/96
Account t{o: 06716
Hercutes. Incorporated - DE
Envi rorrrentaI Af f ai rsui lmington 0E 19894
Page: 1 o{
P.0. 000- 106-881r399-uJK
Ret.
I0iscard: 10/ 5/96
BP-Z Crab Uater Sarpte
Bacchus Pond
Hercutes - llonthIy SampLingBP-2- SDG#: Htrtsol -07
CATN0. AtlAlYStS llAt'tE
4592 TCL Votatites by 8240 - Uater
CoPY T0 Hercutes. Incorporated
COPY I0 ERH - Rocky Hountain
AS RECEIVED
::..: -::.::: : :.:.:. I{ETHODRE$JIIS',,,r 0ETECTIOtI LII'llT UIITS
See Page
ATTN: Mr. Joseph Ket Ier
ATTN: Mr- Brent Robinson
Servi ces Representat i veat [phone]
1?.6136 528631
Questions? Contact your Ct ient
Rachet L. Kreamer
05:03:21 D 0002 10?78 0.00 00026000 ASR00o
LancJste. L;coralorres
2425 lle,r Hciland Pri(e
PO Box l:1:i
LJn(aster, Pl I ;5C5-14:5
7l7-655.2-i03 Fax j11-6ao 1.64i
Respectfu( [y Submi tted
Ramona V. Layman, Group Leader
I CP liteta I s/LeachatesMEMBEFI
!99 rg,re.se ;rr:e 'or :'!aialdt.tar l: s?nbo 5 nno ;tln'evrai,r)nt
.s9s
??l^ ;?5v i,'01/c "89
(il)La ncaster Laborato ries
Page: 2 ol 6
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A division of Thermo Analytical lnc.
LLI sample No. Et 2562490
Co[ lected: 81 9/96 at 16:]5 by BR
subnitted: 8/10/96 Repocted: 9/ 41960iscard: 10/ 5/96
BP-z Grab tJater Sarnpte
Bacchus Pord
Hercutes - tlonthty SamptingAP'?' SDG#: HHS01-07
Account l{o: 06716
Heccutes, Incorporated - DE
Envi ronrnentat Af fai rs
tlitmington DE 19894
P.o. 000- 106-881r399-uJK
Ret.
CATNO. AIIALYSIS I{AI'IE
TcL votatites by 8240 - lJater
1258 Chtofornethane1257 Bromomethane3t92 Vinyt Chtoride3494 Chtocoethane3497 Hethytene Chtoride3498 Acetone3499 Carbon Disut{ide3500 1,1-0ichtoroethene3501 1,1-Dichtoroethane3503 Chtorofocm3504 1,2-Dichtoroethane0316 2-Butanone
3505'1,1,1-Trichtoroethane3506 Carbon Tetrachtoride3507 Vinyt Acetare3508 Bromodichtororn€thane3509 1,2-0ichloropcopane3516 cis- 1,3-Dichl.oropcopene
351 1 Trichtocoethene351? Dibroopchtoromethane3511 1,1,2-Trichtoroethane3515 Benzene3510 trans-1,3-Dichlocopropene3518 Bromoform3521 /+-llethyt -2-pentanone3520 2-Hexanone35ZZ Tetrachtocoethene3523 1,1,2,2-Tetrachtoroethane35?4 Totuene35?5 Chtocobenzene
35?6 .Ethytbenzene35?8 Styrene3529 xytene (toral)5780 trans-1,2-Dichtoroethene6268 cis-1,2-Dichtoroerhene
i:,ii:,,:,i,1:',,:,,:,1:,N;Dr,:,,
::i,,.::::,:,1i.,,',1,,: ll,.Bli,i
:ii'::, . i'ii::.. :;i::, i:;lf ': P i.i..
:ii;; i ir i;:.:.':i:'i':::i:!!i; ur.'i.:
i: : .., :;ir:,: .:.:.L:r::.l{:Siii:::,::::::::::::::::::'7,::::::,::... l
:,,,,,,,,1,i,:r,,,,,i,,,,,!t,iP.,ri,,,
,....... i,l-. i..,. i.l- l!,i41.'.
ir :::,.::::,,,:::,:'i,,:,i,lliPi,:,:
i:i: r ri:i:::::ii. : :,..::l:r F, .' ..
'i,iiir:,i'i:,,iiiii:ii:,':,,},I:iP:;,,,,
:::::::::::1::.]]!::1:::BaEl::l. , , : : : : . : : : : ,:, : : j: : : :t : : . : : : . : : : ,:, :::::::::1:::::,::::+r::::::,:::, J
,:::,,:::ir:::',:::i:ii :a,!{, I i;, ir
rii.:i :::i!,:.iil::::i;: .ll;iti ii:.:.
,:l ::::::i: l::]:li;:lltl:i$i:l::
:,ii:,iii,i!:ililir,riiiil{iif i::,
.,i:: , lL:ii:.::;.r:r'.i.t:i9t.::.
:.r,i:: i:1;,lii:;,:,il.i:iiifill:i Eil!ii:
'.::;:ir:.I:iiitrir,::!!:9r.ir.rri::'rliii::tii:::i:,ii.:i:lI:. q i:: : i
.ir,i:iir;:ii;ii:riii::,il.(ri f l ::i'r:::,:l:::'i::::i:::::li:,11.:0::::i
,: j.:i::ii:i:r:,:ii;iti.::.{i q i::: I
':: ::.:,:.:r:....i::rii:ltirIi., .r:
:r:i.:r':i.,:i:;::i:....ti.i P r r :::
.:1:'iiiiit:'i:.::i;i:'::ji:l{:;qi..'!l
:..ii.i.:,i:i::ii :ii: .. .t.r I i.:, i.
.i........i:i.:.::r::::::[':et....
.::., i.,..,,ii,,::i:::: i.l!, 0 i . :::
.::.::t:::..t::t::i...::ll.r9i.:it.1::::::j:l | |.:::::; i::l:|l:j D; |:1.
ouestions? Contact your CI ient Services Representative
Rachel L. Kreamer ar (717\ 656-2100
Ldn(tsia. LJborJiole;
2425 New Holland Pri(e
FO Bor 12.125
LSnCaSter. "A i /bu)--f;:
717-656-?100 Fax l' 7-656-2631
AS RECEIVED
::i::::r::i:::,::i:::.:lii:::::;:::i:::; ttlETH00
l:j:i:::ii::i:iE-EsJ!iII;i::li DETEcT I orl t I r,t I T url I TS
ugl t
u9/ t
u9/ t
ug,/ t
ugl t
ugl t
trgl L
ugl t
us/ |
u9/ |
usl t
u9/ t
u9/ t
ugl I
u9/ |
u9/ t
u9/ L
ugl t
u9/ t
u9/ t
ugl t
u9/ t
u9/ t
us/ t
ugl t
u9/ t
u9/ t
u9/ t
ugl t
u9/ t
u9/ t
u9/ t
u9/ t
U9/ L
ugl t
RespectfuI ty Subni tted
MicheIe ltcCtacin, B.A.
Group Leade., GC/ltS VoLatitesffin2215 --e! 5,'Cl;?6 -:-? I
I
tee r9le.re !rde'or :'pr;n.t',cr,:r :lf;5ai! ano ;bbie,.'r.t1ror1;
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(iI)Lancaster Laboratories
I,ABORATORY CHRONICLE
3of 6A division of Thermo Analytical lnc.
LLI sample No. EL 2562490cottected: 08109/96 at 16:15 by BR
Subnitted: 08/10/96
Account ilo: 06716Hercules, Incorporated - 0E
EnvirornEntal Affairs
Uitmington DE 19894
8P-2 6rab Uater Sarlpte
Sacchus Pond
llercutes - l,tonthty Sampt in9BP-2- SOG#: lll'1S01-07
CATIIO ANALYSIS NAI.IE
459? TCL Votati Les by 8240 - tJarer
lrET H00
su-846 82408
AI{ALYS I S
TRIAL OATE AIID TIIIE AIIALYST
1 08/23/96 0934 Thomas c. Lehman
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MEMBEFl
LancJsier Ldboraiorres
2+25 NIe., llorlano P.i€
PO 9ox 12125
Lancasier. PA I 75C5-2rlS
717-656-2100 Fax: 7ll.6l: r58l jCe.e'rerse siCe lor rrO,:ear,cn of;vmboi; arC abcre'/tatlon5
oB,
ieY s/cricc *o'$
LLI Sample No. 2562490
BP-Z Grab Uater Safipte
Bacchus Pond
Hercutes - tlonthty Sarpting
Group l{o. 528631
Hercutes, Incorporated - DE
76 79
8484
82 87
84 82
101 114
93 95
91 99
101 107
103 't05
95 100
94 97
103 108
107 1i3
86 84
97 101
103 106
100 102
94 98
91 93
96 96
98 101
100 104
QUALITY CONTROL REPORT
Page: 4 ot
LCS LII.IITS
LOU I TGH
(iI}La ncaste r Laborato ries
A division of Thermo Analytical lnc.I
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DUP I'{S LCS LCSRPD I,IS IISD RPO LCS DUP RPD
Safipte
I.IDL
Sanpte
UNITS
4592 TCL Votatites by 8240 - lJater Batch: J96235248
1258 Chtoromethane3. ug/t1257 Bromomethane3' us/t
3492 Vinyt Chtocide?. ug,/ t3494 Chtoroethane3. uglt
3497 HethyLene Chtor-ide?' ug/t
3498 Acetone6' ug/t3499 Carbon Disutfide3' ug/t
3500 1,1-Dichloroethene1' us/t3501 1,1-0ichtoroethane?' ugltJ503 Chioroform
1 ' u'/t3504 1,2-Dichtoroethane?' uglt0316 2-Butanone3. uglt3505 1,1,1-Trichtoroethane'I' us/t
3506 Carbon Tetrachtoride1' us/t
5507 Vinyl. Acetate2. ug/t
3508 Eromodichtocomethane1. ug/t3509 1,2-Dichtoropnopane
N.D.
N.D.
N.D .
N.D.
t{.D.
I.D.
[.0 .
ll.D.
N.D.
it.0.
$.0 .
N.D.
N.D.
N.D .
I.D.
[-D.
N.0.
|,1.D.
N.D.
N.D.
H.D.
N.D.
N-0.
11
0
5
3
12
z
3
5
1
6
3
5
5
2
J
3
2
4
?
0
3
4
us/ I3516 cis-1,3-Dichtoropropene
1.us/ t3511 Trichtoroethene
1 ' uglt3512 Dibromochtoromethane?, ug/t
3513 1,1,2-Trichtocoethane2' us/t3515 Eenzene1' uglt
1510 trans'1,3-Dichtoropnopene1. uslt
l-
Lanca5ier Laboratofles
2425 Ne,e Holiand Prke
PO 8ox 12.125
Lancaste.. PA 17505-2.125
7 i ;-556-:100 F a:t i 1,- -655- 253 1
3o+
Qe., 5 0lr?c "q{Y
MEMBEFI
See.everse:rce lo. exp!aloaIrc. of s',,rnbor; and abbre,/raircns
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LLI sample No. 2562490
BP-z Grab Uater Saflpte
Bacchus Pond
llercutes - l,lonthty Sanpt ing
Sarlpte SanpteIiIDL U}I I TS
Bronpform1. ug/t
4-Hethyt -2-pentanone
5 ' uglt
2 - llexanone
7 ' usll
Tet rach I oroethene
1 ' us/t
1, 1,2,2-I etrach toroethane2. us/t
To I uene2. ug/l
Ch t orobenzene1. ug/t
E thy I benzene2' us/t
Styrene1. ug/t
Xytene (totat)
l ' u'lt
trans- 1, 2-0 i ch Ioroethene2. ug/t
ci s-1.2-0i chtoroethene2. uslt
Group lto. 528631
Hercules, Incorporated - DE
QUALITY CONTROL REPORT
LCS
LCS LCS LIMITSRPD LOU IIIGH
(iI}Lancaster Laboratories
A division of Thermo Analytical lnc.
3518
3521
3520
352?
3523
3524
3525
3526
3528
3529
5780
6268
!,ts
87
98
98
91
98
101
97
105
99
105
94
104
l'ts0
90
100
98
95
101
106
100
110
103
107
95
107
lrs
RPO
2
0
4
1
4
1
4
2
1
J
DUP
RPDBLANK
il.D.
t{.0.
[.D.
[.0.
[.0 .
lt.0.
N.D.
I.D.
I.D.
I.D.
I.D.
r.D.
l-3ncdster Labora tofl e5
2425 Ne,^r Hollaeq 9rKe
PC 3ox 12425
Lanc;si.r. PA. 17 6i5 -2!2"
71,1-655-2)A0 Fax 711 olc 261,See ie!?:Se I 4e rCr a (c nrr.t:. .l s!mbors and dobreyralions
$Lancaster Labor:atories
A division of Thermo Analytical lnc.
QUALITY CONTROL REPORT
SURROGATE LII.IITSLOU H I GII
76 11488 11085 115
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LLI sample No. 2562490
BP-2 Grab uater Sampte
Bacchus Pond
hercutes - ttonthty Sampting
4592 ICL votatites by 8240 - trater
Group No. 528631llercutes, Incorporared - DE
SURROGATE SUTII.'ARY
TRIAL ID SURROGATE RECOVERY Z
d4-1,2-DCA 98d8-totuene 1044.BFB 99
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Linc6sier Labordtofie:
?J25 lJe'& Hciraric Prke
PO 8ox 12425
Laqca5iet !A
"
;6At-2:25
717-o56-210C irt 7',1.a56.244
t
MEMBER
iea .e,.n,:€ ,.aa iCt ?- tC a- ;,. o^ Ci ; rr cCr; ;nri :bbreyratrOns
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(l)Lancaster Laboratories
Page:
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LLI sampte No. EL 2562491
cot Iected:
subnitted: 8/10/96 Repocted: 9/ 4/96Discard: 10/ 5/96
Trip Btank Uater Sarp(e
Eacchus Pond
Hercutes - Honthty Sanpting
tll,tSTB SDG#: tlttS0l -08TB*
CATIIO. A}IALYSIS IIAI{E
4592 TCL votatites by 8240 - frater
A division of Thermo Analytical lnc.
Account tlo: 06716
tlercu(es. lncorporated - DE
Envi ronrnentat Af fai rstlitmington DE 19894
AS RECEIVED
:::i::.::::'::::::i::::.:l::::i:::i:lii: ltlETH00
iili:ljli::,ri*ESlItl:;:i:i:, oerecr t ou L I H I T url t Ts
See Page 2
P.0. 000- 106-8817399-UJK
ReL -
lof 6
S]}
:2lt. ?:v 5l0liao +;#
ATT[: Hr.
ATTN : l,lr.
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ICoPY T0 Hercutes, Incorpocated
CoPY T0 ERH - Rocky llountain
Joseph Ketter
Erent Robinson
IQuestions? Contact your Ctient Services Representative
Rachel L. Kreamec at [phone]
3?;oo"t.Booo33o,ul3o or*ooo 126436 s28631
I
Respectfut ty Sulrni tted
Ramona V. Layman, Group Leade.
ICP Metals/Leachates
Lanca5ler Laoorator:e5
2.125 New Holland Prke
PO 3ox 12125
LancJsiel PA 17605-:d25
717-656.2100 Fax J 1 t- -611-2581 I
I
MEMBER
See re,rerse sioe ior ircldni::ci cr irmoci: aed aborel.ralr.t.s
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(I)Lancaster Laboratories
A division of Thermo Analytical lnc.
2562491LLI Sample No. EL
Col tected:
3516 cis-1,3-0ichtoropcopene3511 Trichtoroethene3512 Dibroopchtoromethane35'13 1,1,2-Trichtoroethane3515 Benzene3510 tcans-1,3-Dichtoropropene
Account llo: 06716
Heccutes, Incorporated - DE
Envi rorunentat Affai rs
Uitmington 0E 19894
Page: ? of 6
P.0. 000- 106-8817399-|JJK
Ret.Suhnitted: 8110196 Reported: 9l 4/96Discard: 10/ 5/96
Trip Btank tJater Sampte
Bacchus Pond
Hercutes - l,tonthty Sarpting
lltlsTg SoG#: HilS01-08TBr
CATt{o. AilALYStS [Ar'tE ,i,
TCL Vol.atil.es by 8240 - Uater
1258 Chtorornethane ::.i1257 Bromomethane ::,i319? Vinyt Chtocide :'l.l3494 Ch loroethane :',.3497 Methytene Chtoride ::l3498 Acetone :i3199 Carbon Disul,fide :3500 1,1-Dichtoroethene ,i3501 I,l-Dichtoroethane :i':3503 ChLocofocm ,,35OL 1,2-Dichtoroethane ,,i0315 Z-Butanone ::3505 '1,1,1 -Trichtoroethane i,.
3506 Carbon Tetrachtoride : .3507 Vinyl Acetate ,''3508 Brornodichtocomethane . .3509 1,2-Dichtoropcopane .:.
AS RECEIVED
':,,|...,.:::|'.:.:.:-:.:':',:|:| IttETHoo
ftqEtJll{i:,:,iii 0ETECTlol{ Lll.llT UNITs
3518 Brornoform i:ii3521 4 -ilethyt -z-pentanone .:.:3520 z-Hexanone .,',35?? Tetrachtoroethene .::3523 1,1,2,z-lettachtoroethane ::
35?4 Totuene i,3525 Chtorobenzene ':3526 Ethytbenzene t:;
3523 Styrene '.
3529 xytene (rotat) :5780 trans-1,2-Dichtoroethene ::6?68 cis-1,2-0ichtoroethene .,.
Questions? Contact your CLient
Rachel L- Kreamer
Servt ces Repaesentat i ve
ar [phone]
,;;)r1,0,.r,.,.,,,i[;qi ,.t:i,
,::ttl0,i.,.ij
,,,)1,.0,;, :,r,:z , j.:..:.::,
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Respectfut Ly Suuni tted
l{ichete HcCtarin, B.A.
Group Leader, GC/HS Votati Ies
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MEMBEFI
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(I}Lancaster Laboratories
LABORATORY CHRONICLE
3of 6A division of Thermo Analytical lnc.
LLI Sample No. EL 2562491
Co[ tected:
Submitted: 08t10/96
Accouflt [o: 05716
Hercutes, lncorporated - DE
Envicoilnentat Affairs
lJitmington DE 19894
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CATIIIO ANALYSIS IIAI{E
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ANALYS I STRIAL DATE A}ID TIME AIIALYST
1 08/23/96 1OO9 Thomas C. Lehman t
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Bacchus Pord
llercutes - l,lonthty Sanrpl. in9
Group llo. 528631Hercutes, lncorpocated - OE
QUALITY CONTROL REPORT
Page: 4 of
LCS LII.IITS
LOU HIGH
(iI)La ncaster Laboratories
A division of Thermo Analytical lnc.
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QUALITY CONTROL REPORT
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LLI sanple No. 2562491Trip Btank Uater Sampte
Bacchus Pond
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Group llo. 528631liercutes, Incorporated - DE
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QUALITY CONTROL REPORT
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