DSHW-1993-004238 - 0901a06880157731

HERCULES
Dennis Downs
Director, Department of Environmental Quality
Division of Solid and Hazardous Waste
288 North 1460 West
Salt Lake City, UT 84114-4880
Re: Hazardous Waste Inspection Information Request
Dear Mr. Downs:
Hercules Aerospace Company
Space/Strategic Propulsion
Bacchus Works
Magna, Utah 84044-0098
[phone]
September 29, 1993
DSHW »N
1993.11237
Your recent letter of September 17, 1993 requested information pertaining to the annual
inspection of Hercules' Bacchus Works facility. The inspection this year is focusing on
disposal of Titan IV SRMU forward segment TF009, a task that was accomplished on August
23, 1993. A number of items were requested in order to complete the inspection. Each of
these items is individually addressed below.
Item 1 - Please provide a copy of the hazardous waste manifest which accompanied the
TF009 segment to the UTTR facility.
Response - A copy of the manifest was hand delivered to the Division of Solid and
Hazardous Waste (DSHW) office the week of 27 August 1993. Another copy
is attached to this letter.
Item 2 - Please indicate when TF009 became the property of the U.S. govemment.
Specifically, when was the paper work signed transferring ownership from
Hercules to the U.S. Govemment.
Response - By prior agreement between the various govemment, contractor, and
subcontractor parties, Hercules retained ownership of the segment until
placement of the segment on the Utah Test and Training Range Thermal
Treatment Unit (UTTR TTU) pad. The segment had to be placed to the
satisfaction of the 649 Explosive Ordnance Disposal Squadron (EODS), which
is the Air Force group responsible for placement of the destruct charges.
Except for signatures, all the paperwork pertaining to segment ownership was
filled out prior to disposal. Once the segment was placed, a short signing
ceremony was held on the county road west of the TTU. The 649 EODS was
then notified that the segment belong to the U.S. Govemment and given
direction to proceed with the disposal.
Hazardous Waste Inspection Information Request Page 2
Item 3 - The Hazardous Waste Disposal Plan for TF009 indicates that flexible linear
shape charges were going to be used after the bum to "cut up' the carbon fiber
casing and that the casing will be disposed of at an appropriate industrial waste
facUity. Please provide copies of all manifest or shipping papers used for
disposal of the TF009 casing. Also, indicate how Hercules established that the
casing could be disposed of as solid waste at an industrial facility.
Response - A copy of the hazardous waste manifest used to ship the nonhazardous debris
to USPCI's grassy mountain facility is attached. The debris was shipped as
nonhazardous.
Hercules' knowledge of the Titan SRMU manufacturing process determined
that the only waste code applicable to Titan IV SRMU segment TF009 was
D003 because of the reactive propellant. Treatment of the propellant at the
UTTR TTU and subsequent visual inspection verified that all of the propellant
had been consumed. The residuals no longer had the characteristic of reactivity
and were thus nonhazardous per 40 CFR 261.3(d).
A representative sample collected at the time of disposal confirmed that the
material was indeed nonhazardous (results attached).
Item 4 - Also, if available, please provide photographs of TF009 before unloading, after
unloading, and after disposal.
Response A video tape covering TF009 disposal was hand delivered to the DSHW office
on 16 September 1993 with instructions to place on Bill Wallner's desk.
Additional still photographs taken by the Hercules Photo Department are
included with this letter.
If you have any further questions on this issue, please contact me at 251-3574.
Sincerely,
E. Richard Anderson, Manager
Environmental Engineering and
Hygiene
ERA/CDFalkenberg/
Attachments
Icp6/i^
Please print or type. (Fonn designed for use on elite (12-pitch) typewriter.) Form Appimed. OMB No. 2050-0039. Eitpires 9-30-92
UNIFORM HAZARDOUS
WASTE MANIFEST
1. Generator's US EPA ID No. Manifest
Document No.
U T D 0 0 1 7 0 5 0 2 ^1) 0 1 9 2
2. Pagel
of 1
Information In the shaded areas
Is not required by Federal law.
3. Generator's Name and Mailing .Address Uerculea Incorporated
P.O. Box 93, M/S X3J1
Hagna^Jtah 840«A Generator's Phone ( 801 ) 250-5911 (ATTIT Mike Parker)
A. State Manifest Document Number
B; State Generatof's ID; •: j ? > 3
Transporter 1 Company Name
D.S.G.W. Ogden S.P.
6. US EPA ID Number
|C A n0069132 0 6
C. State Transporter's ID ,1031
D. Transportef's Phone(K>0} '767-3846
Transporter 2 Company Name
Savase Industries
7.
9. Designated Facility Name and Site Address
Utah Test and Training Range
Oasis, Utah
8. US EPA ID Number
ID.T.D.9.3.3.0.6.7.3.1
E. State Transporter's 10
F. Transportei'sPhone(801) 973-9638
10. US EPA ID Number G. State FacHity's 10.
lu TO 5 7.0 0 9 0 0 0 1
H. Facility's Phone
(801) 777^1524
11. us DOT Description (Including Proper Shipping Name, Hazard Class and ID Number) 12. Containers
No. Type
13. Total Ouantity
14. Unit Wt/Vol
::•-• -I.'-.--: Ol.. Waste No,
X
RQ Waste Rocket Motor, 1.3C, UrI0186, ?<1 II
(tX)03) (Titan IV SRMU Forward Segoent TF009) 001 CTP 0 0 0 6 S D003
J. Additional Descriptions for Materials Listed Above
' a. : Ccntt'alns Alusilnuai Powder, AitBiioniuB Pisrchlorate
K. Handling Codes for Wastes Listed Above
•::::.r:a.-^DS?:;- .•:'•- ••
15. Special Handling Instructions and Additional Information ^^ ... . . .... , *
3ote: Shipping weight includes 7,500 pound clevis ring that will retum to the factory
after shlpoent. In case of accident evacuate and block area. I^merseni^ Response Contact: •flo.TrMlts!ft In corpora r^dy Gary TJioniriwen (^0!) ^.'Sn-S?!! 16. GENERATOR'S CERTIFICATION: I hereby declare tttat ttie contents of this consignment are fully and accurately described above by
proper shipping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highway
according to applicable international and national government regulations.
If I am a large quantity generator. I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be
economically practicable and that_ I have, selected-the practicable method of treatment, storage, or disposal cun^ently available to me which minimizes the present and
future threat to human health and the environment: OR, if I am a small quantity generator, I have made a good faith effort to minimize my waste generation and select
the t}est waste management mettiod that is available to me and that I can afford.
Printed/Typed Name Signature Month Day Year
II Ml-I 17. Transporter! Acknowledgement of Receipt of Materials
Printed/Typed Name _ Signature-Month Day Year
18. Transporter 2 Acknowledgement of Receipt of Materials
Printed/Typed Name Signature. Month Day Year
IIIIII
19. Discrepancy Indication Space
20. Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted in Item 19.
Printed/Typed Name Signature Month Day Year
M II II
style F15 REV-6 Printed by Labelmaster, An American Labalmark Co., Ghbago, IL 60646 [phone] EPA Form 8700-22 (Rev. 9-88) Prevkxjs ediiioos ar« obsi.lme
k PHMTEI) CN RECYCtfi) PAPER
f USING SOVBEAN N( PWITEI WIIH
SOY INK GENERATOR COPY
Please print or type. (Form designed for use on elite (12-pitch) typewriter.) fivm AppiXKed. OMB Ata 2050-0039. Bcpires 9-30-92
UNIFORM HAZARDOUS
WASTE MANIFEST
1. Generator's US EPA ID No. Manifest
Document No. II T D 0 0 1 7 0 5 0 2 910 0 2 0 a 1 . . . .
2. Page 1
of 1
Information in the shaded areas
is not required by Federal law.
3. Generator's Name and Mailing Address Hercules Incorporated
P.O. Box 98, M/S X3J1
Magna Utah 84044
4. Generator's Phone( 301 )250-59II (Attn; Mike Parker)
A. State Manifest Oocurnent Number.
B. State Generator's ID :';;
5. Transporter 1 Company Name ^ Triad Transporters Inc. hz Bf |PA ID Number 7 9 1 C. -State Transportef's ID
D. Transporter's Phoned 800^32 4-1139
7. Transporter 2 Company Name 8. US EPA ID Number E. State Transportef's ID:
F. Transporter's Phone. •.
9. Designated Facility Name and Site Address
CS. Pollution Control Inc,
7 Hi lU 3 Hi K, Kxlt 41 on 180
Grassy Mtn. Facility, Clive Ut
10. us EPA ID Number G. State Facilit/s ID
IIITD991301748
H. -Facility's Phone
(8Q1): 595 3900
11. us DOT Description (Including Proper Shipping Name, Hazard Class and ID Number) 12. Containers
No. Type
13. Total
Quantity
14. Unit Wt/Vol
• A.:: Waste No.
Waste Rocket Mctor Debris, Non Hazardous
IJon Regulated
/& S<?o
0 01 ic M L-2 ::0 0 TJR
d. t;-.,u:,!,'
J. Additional Descriptions for Materials Listed Above :
; fteight in Box 13 is^^^^^e^^
K. Handling Codes foi' Wastes Listed Atiove
:-_,.::...:.-j^-^-•;.•...•,-:.-• ;v;.;.^7f..v:-:
15. Special Handling Instructions and Additional Information
Reference Acceptance Number GM91-1500
Load NuHber it&Sm H% ^HS
16. GENERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by
proper shipping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highway
according to applk:able international and national government regulations.
If I am a large quantity generator. I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be
economically practicable and that I have selected the practicable method of treatment.; storage.^or disposal currently available to me which minimizes ttte present and
futurejhreat to human health and the environment:.OR. if I am a small quantity generator, I have made a good faith effort to minimize my waste generation and select
thVbest waste management mettiod that is available to me and that I can afford.
Printed/Typed Name Signature
...Jr-;
Month Day Year
17. Transporter 1 Acknowledgemehf of Receiptof Materials
, Rrinted/Typed-Name Signature - •-;• Month Day Year
18. Transporter 2 Acknowledgement of Receipt of Materials / t
Printed/Tyjjed Name Signature Month Day Year
IIIIII
19. Discrepancy Indication Space
20. Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted In Item 19.
Printod/Tyfjed Name Signature Month Day Year
I I I I I I
style PIS REV-6 Printed by Labelfnaster, An American Latwlmaik Co., Chicago, IL 60646 [phone] EPA Form 8700-22 (Rev. 9-88) Previcxis sditnns are obsolete.
PRHTEO ON nECVOHl PAPER
uSHSSoveeANMK P»MIH WITH
SOVINK GENERATOR COPY
ANALYTICAL LABORATORY 6100 8. STRATLER
MURRAY, UTAH 84107
PHONE; [phone]
FAX: [phone]
TO: Hercules
P.O. Box 98
Magna, Utah 84044
SAMPLE ID: Lab #U099075
DATE: 9-23-93
1S30146 Titan Firing D^br/s
CERTIFICATE OF ANALYSIS
TCLP PURGEABLE F-SOLVENTS
Acetone, mg/l
Benzene, mg/1
n-Butyl alcohol, mg/1
Carbon Disulfide, mg/l
Carbon Tetrachloride, mg/l
Chlorobenzene, mg/l
Cyclohexanone, mg/l
1,2-Dichlorobenzene, mg/l
1,4-Dioxane, mg/1
Ethyl acetate, mg/1
Ethyl benzene, mg/l
Ethyl ether, mg/l
Isobutanol, mg/1
Methylene chloride, mg/1
Methyl ethyl ketone, mg/1
Methyl isobutyl ketone, mg/l
Nitrobenzene, mg/l
2-Nitropropane, mg/1
Pyridine, mg/1
Tetrachloroethene, mg/1
Toluene, mg/l
1,1,1-Trichloroethane, mg/l
1,1,2-Trichloroethane, mg/1
1,1,2-Trichlorotrifluoroethane, mg/l
Trichloroethene, mg/l
Trichlorofluoromethane, mg/l
Xylenes, mg/l
DETECTED
<1.0
<.02
<2.0
<.5
<.02
<.02
<2.0
<.l
<1.0
<.2
<.05
<.2
<1.0
<.05
<.5
<.5
<1.0
<.5
<10
<.05
<.l
<.05
<.05
<.5
<.02
<.l
<.05
MDL
1.0
0.02
2.0
0.5
0.02
0.02
2.0
0.1
1.0
0.2
0.05
0.2
1.0
0.05
0.5
0.5
1.0
0.5
10
0.05
0.1
0.05
0.05
0.5
0.02
0.1
0.05
MDL = Minimum Detectable Level
^ ?^^ /^^'
Joel Workman
MTE
ANALYTICAL LABORATORY
6100 S. STRATLER
MURRAY, UTAH 84107
PHONE: [phone]
FAX: [phone]
TO: Hercules
P.O. Box 98
Magna, Utah 84044
DATE: 9-23-93
SAMPLE ID: Lab #U099075
DATE SAMPLED: 9-10-93
DATE SUBMITTED: 9-10-93
1S30146
CERTIFICATE OF ANALYSIS
PARAMETER
TCLP TEST
Antimony as Sb, mg/l
Arsenic as As, mg/1
Barium as Ba, mg/l
Beryllium as Be, mg/1
Cadmium as Cd, mg/l
Chromium as Cr, mg/1
Chromium as Cr (HEX), mg/l
Copper as Su, mg/1
Lead as Pb, mg/l
Manganese as Mn, mg/1
Mercury as Hg, mg/l
Nickel as Ni, mg/1
Potassium as K, mg/1
Selenium as Se, mg/l
Silica as Si, mg/l
Silver as Ag, mg/l
Sodium as Na, mg/1
Titanium as Ti, mg/1
Vanadium as V, mg/1
Zinc as Zn, mg/1
DETECTED
37.0
0.117
6.51
<.01
0.016
0.012
<.02
0.363
<.02
1.04
0.0155
<.01
9.78
<.04
<10
<.01
26.3
<10
<.01
17.4
CpKt
1 • Joel
DATE ANALYZED/METHOD
9-14-93
9-14-93
9-14-93
9-14-93
9-14-93
9-14-93
9-15-93
9-14-93
9-14-93
9-14-93
9-16^-93
9-14-93
9-15-93
9-14-93
9-20-93
9-14-93
9-15-93
9-20-93
9-14-93
9-14-93
WorkiTlan
EPA
EPA
EPA
EPA
EPA
EPA
EPA
EPA
EPA
EPA
EPA
EPA
EPA
EPA
EPA
EPA
EPA
EPA
EPA
EPA
1311/6010
1311/6010
1311/6010
1311/6010
1311/6010
1311/6010
1311/7196
1311/6010
1311/6010
1311/6010
1311/7470
1311/6010
1311/6010
1311/6010
1311/6010
1311/6010
1311/6010
1311/6010
1311/6010
1311/6010
nJ
Ln ANALYTICAL LABORATORY
61 OOS. STRATLER
MURRAY, UTAH 84107
PHONE: [phone]
FAX: [phone]
SAMPLE ID: Lab #U099075 - 1S30146
DATE SAMPLED: 9-10-93 DATE SUBMITTED: 9-10-93
TCLP VOLATILE ORGANIC COMPOUNDS (EPA 8240)
Benzene, mg/1 (D018)
Bromobenzene, mg/l
Bromochloromethane, mg/l
Bromodichloromethane, mg/1
Bromoform, mg/l
Bromomethane, mg/l
n-Butylbenzene, mg/l
sec-Butylbenzene, mg/1
tert-Butylbenzene, mg/1
Carbon tetrachloride, mg/l (D019)
Chlorobenzene, mg/1 (D021)
Chloroethane, mg/1
Chloroform, mg/l (D022)
Chloromethane, mg/1
2-Chlorotoluene, mg/l
4-Chloroto1uene, mg/l
l,2-Dibromo-3-chloropropane, mg/1
1,2-Dibromoethane, mg/1
Dibromochloromethane, mg/1
Dibromomethane, mg/1
1,2-Dichlorobenzene, mg/1
1,3-Dichlorobenzene, mg/1
1,4-Dichlorobenzene, mg/1 (D027)
Dichlorodifluoromethane, mg/l
1,1-Dichloroethane, mg/1
1,2-Dichloroethane, mg/1 (D028)
cis-1,2-Dichloroethene, mg/l
trans-1,2-Dichloroethene, mg/l
1,1-Dichloroethylene, mg/l (D029)
1,2-Dichloropropane, mg/1
1,3-Dichloropropane, mg/1
2,2-Dichloropropane, mg/l
1,1-Dichloropropene, mg/1
cis-1,3-Dichloropropene, mg/l
trans-1,3-Dichloropropene, mg/1
Ethylbenzene, mg/l
DATE ANALYZED: 9-15-93
DETECTED
<.02
<.05
<.05
<.05
<.05
<.05
<.10
<.10
<.10
<.05
<.02
<.05
<.05
<.02
<.10
<.10
<\.Q
<.05
05
05
,10
,10
,10
,05
<.10
<.05
<.05
<.02
<.05
<.05
<.05
<.05
<.05
<.05
<.05
<.05
MDL
0.02
0.05
0.05
0.05
0.05
0.05
0.10
0.10
0.10
0.05
0.02
0.05
0.05
0.02
0.10
0.10
1.0
0.05
0.05
0.05
0.10
0.10
0.10
0.05
0.10
0.05
0.05
0.02
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
MDL = Minimum Detectable Level
-#ti /A
I
Joel Workman.
1—
•—I l— ANALYTICAL LABORATORY
DATE ANALYZED: 9-
DETECTED
<.10
<.10
<.10
<.05
<.10
<.10
<.10
<1.0
<.05
<.05
<.05
<.05
<.10
<.10
<.10
<.05
<.05
<.02
<.10
<.10
<.10
<.10
<.10
<.05
6100 S. STRATLER
MURRAY, UTAH 84107
PHONE: [phone]
FAX: [phone]
•15-93
MDL
0.10
0.10
0.10
0.05
0.10
0.10
0.10
1.0
0.05
0.05
0.05
0.05
0.10
0.10
0.10
0.05
0.05
0.02
0.10
0.10
0.10
0.10
0.10
0.05
SAMPLE ID: Lab #U099075 - 1S30146
DATE SAMPLED: 9-10-93 DATE SUBMITTED: 9-10-93
TCLP VOLATILE ORGANIC COMPOUNDS fEPA 82401
Hexachlorobutadiene, mg/1 (D033)
Isopropyl benzene, mg/1
p-Isopropyltoluene, mg/1
Methylene chloride, mg/l
Methyl ethyl ketone, mg/l (D035)
Naphthalene, mg/l
n-Propylbenzene, mg/l
Pyridine, mg/l (D038)
Styrene, mg/1
1,1,1,2-Tetrachloroethane, mg/l
1,1,2,2-Tetrachloroethane, mg/l
Tetrachloroethene, mg/l (D039)
Toluene, mg/1
1,2,3-Trichlorobenzene, mg/l
1,2,4-Trichlorobenzene, mg/1
1,1,1-Trichloroethane, mg/1
1,1,2-Trichloroethane, mg/l
Trichloroethene, mg/l (D040)
Trichlorofluoromethane, mg/l
1,2,3-Trichloropropane, mg/l
1,2,4-Trimethylbenzene, mg/l
1,3,5-Trimethylbenzene, mg/1
Vinyl chloride, mg/1 (D043)
Xylenes, mg/l
MDL = Minimum Detectable Level
i-' Joel Workman ,/
nJ
Ln ANALYTICAL LABORATORY 6100 S. STRATLER
MURRAY. UTAH 84107
PHONE: [phone]
FAX: [phone]
SAMPLE ID: Lab #U099075 - 1S30146
DATE SAMPLED: 9-10-93 DATE SUBMITTED: 9-10-93 DATE ANALYZED: 9-18-93
TCLP SEMI-VOLATILE ORGANICS (EPA 82701
bis(-2-Chloroethyl)ether, mg/1
2-Chlorophenol, mg/1
Phenol, mg/l
1,3-Dichlorobenzene, mg/l
1,4-Dichlorobenzene, mg/l
1,2-Dichlorobenzene, mg/1
2-Methylphenol, mg/1 (D023)
Hexachloroethane, mg/l {D034)
bis(2-Ch1oroisopropy1)ether, mg/1
N-Nitrosodi-n-propylamine, mg/l
3- and 4-Methy1pheno1, mg/l (D025)
Nitrobenzene, mg/l (0036)
Isophorone, mg/1
2-Nitrophenol, mg/1
2,4-Dimethylphenol, mg/l
bis(-2-Ch1oroethoxy)methane, mg/l
2,4-Dichlorophenol, mg/1
1,2,4-Trichlorobenzene, mg/l
Naphthalene, mg/l
Hexachlorobutadiene, mg/1 (D033)
4-Chloro-3-Methy1pheno1, mg/l
2,4,5-Trichlorophenol, mg/l
2,4,6-Trichlorophenol, mg/l (0041)
2-Chloronaphthalene, mg/l
Acenaphthylene, mg/1
Dimethyl phthalate, mg/1
2,6-Dinitrotoluene, mg/l
Acenaphthene, mg/1
2,4-Dinitrophenol, mg/l
2,4-Dinitrotoluene, mg/1 (D030)
4-Nitrophenol, mg/l
DETECTED
<.05
<.05
0.12
<.02
<.05
<.02
<.05
<.02
<.05
<.05
<.05
<.02
<.02
<.05
<.05
<.05
<.05
<.02
<.02
<.02
<.05
<.05
<.05
<.02
<.05
<.02
<.02
<.02
<.5
<.05
<.02
MDL
.05
.05
.02
.02
.05
.02
.05
.02
.05
.05
.05
.02
.02
.05
.05
.05
.05
.02
.02
.02
.05
.05
.05
.02
.05
.02
.02
.02
.5
.05
.02
MDL = Minimum Detectable Level
—• 1=—
L-l I— ANALYTICAL LABORATORY
6100 S. STRATLER
MURRAY, UTAH 84107
PHONE: [phone]
FAX: [phone]
SAMPLE ID: Lab #U099075 - 1S30146
DATE SAMPLED: 9-10-93 DATE SUBMITTED: 9-10-93 DATE ANALYZED: 9-18-93
TCLP SEMI-VOLATILE ORGANICS (EPA 8270)
Fluorene, mg/1
4-Chloropheny1pheny1 ether, mg/1
Diethyl phthalate, mg/l
4,6-Dinitro-2-methylpheno1, mg/l
4-Bromopheny1phenyl ether, mg/l
Hexachlorobenzene, mg/l (D032)
Pentachlorophenol, mg/1 (D037)
Phenanthrene, mg/l
Anthracene, mg/l
Di-n-Butyl phthalate, mg/l
Fluoranthene, mg/1
Pyrene, mg/l
Butylbenzyl phthalate, mg/l
Benzo(a)anthracene, mg/l
Chrysene, mg/l
3,3'-Dich1orobenzidine, mg/1
Bis(2-Ethy1hexyl)phthalate, mg/l
Di-n-octyl phthalate, mg/l
Benzo(b)fluoranthene, mg/l
Benzo(k)fluoranthene, mg/1
Benzo(a)pyrene, mg/1
Indeno(l,2,3-cd)pyrene, mg/l
Dibenzo(a,h)anthracene, mg/l
Benzo(g,h,i)perylene, mg/1
Dibenzofuran, mg/1
DETECTED
<.02
<.05
<.02
<.25
<.02
<.02
<.05
<.05
<.02
<.5
<.02
<.02
<.5
<.l
<.02
<.2
<.02
<.02
<.05
<.02
<.02
<.05
<.02
<.05
<.02
MDL
.02
.05
.02
.25
.02
.02
.05
.05
.02
.5
.02
.02
.5
.1
.02
.2
.02
.02
.05
.02
.02
.05
.02
.05
.02
MDL = Minimum Detectable Level