DSHW-2017-003423 - 0901a068806e9cc8

Orbital ATK
April 19, 2017
8200-FY17-019
Div of Waste Management
and Radiation Control
APR 2 0 2017
Scott T. Anderson, Director DS^V/-£017-00 3 4-23
Department of Environmental Quality
Division of Waste Management and Radiation Control
ATTN: Jeff Vandel
P.O. Box 144880
195 North 1950 West
Salt Lake City, Utah 84114-4880
RE: Sampling Results Report and Proposed Corrective Action Solid Waste Management
Unit # 553, ATK Launch Systems Inc. - Promontory Facility, EPA ID# UTD009081357
Dear Mr. Anderson,
In an August 6, 2016 letter from your office (DSHW-2016-012110), a sampling and analysis
plan was approved to conduct additional sampling at SWMU #553. Included with this letter is
a report on the results of that investigation and a proposed corrective action plan.
If you have questions, or need additional information, please contact Paul Hancock at (435)
863-3344.
Sincerely,
Environmental Services
Orbital ATK, Inc. • P.O. Box 707 Brigham City, Utah 84321 • (801 )250-5911
DSU'W'Zon-OOa»4-Z3
rbitalATK
Div of Waste Management
and Radiation Control
APR 2 0 2017
Sampling Results Report and Proposed
Corrective Action for
Solid Waste Management Unit 553
Promontory Facility
Prepared for:
Utah Department of Environmental Quality
Division of Waste Management and Radiation Control
Prepared by:
ATK Launch Systems Inc.
UTD009081357
April 2017
Orbital ATK
SAMPLING RESULTS REPORT
Solid Waste Management Unit 553 Resample
Promontory Facility ATK Launch Systems
TABLE OF CONTENTS
1.0 INTRODUCTION...................................................................................................................................2
1.1 Background................................................................................................................................. 2
2.0 FIELD SAMPLING ACTIVITY AND CHANGES .....................................................................2
3.0 SAMPLING RESULTS...........................................................................................................................3
4.0 PROPOSED CORRECTIVE ACTION..............................................................................................6
4.1 Corrective Action Process.......................................................................................................... 7
4.2 Confirmation Sampling and Analysis...................................................................................7
4.3 Decontamination Procedures...................................................................................................7
4.4 Sampling Handling and Custody...........................................................................................8
4.6 Quality Control Samples...........................................................................................................8
4.6.1 Field Quality Control Samples................................ ................................................8
4.6.2 Laboratory Quality Control Samples......................................................................8
4.7 Data Management.......................................................................................................................9
5.0 DATA VALIDATION AND USABILITY.......................................................................................9
5.1 Data Review, Verification, and Validation...........................................................................9
FIGURES
FIGURE 1 SWMU #553 Soil Sample Results
FIGURE 2 SWMU #553 Characterization of 50’ Location
FIGURE 3 SWMU #553 Proposed Excavation Areas
ATTACHMENTS
Attachment A
Attachment B
Attachment C
Analytical Data Sheets
XRF Readings
Field Notes
1
Orbital ATI Solid Waste Management Unit 553 Resample
Promontory Facility ATK Launch Systems
SAMPLING RESULTS REPORT
1.0 INTRODUCTION
A Sampling and Analysis Plan (SAP) was developed in response to a request by the Utah
Division of Waste Management and Radiation Control (the Division) to resample a Solid Waste
Management Unit (SWMU) designated as #553. This is a historic photographic fixer discharge
area at the Promontory ATK Launch System Inc. (ATK) facility. The Division approved the
plan in an August 6, 2016 letter. The sampling was conducted on September 16, 2016 with
Division representative Jeff Vandel at the site.
1.1 BACKGROUND
The building called M-19A at the ATK facility was historically used to develop X-ray
photographs from the X-ray of solid rocket motors such as Minute Man. The spent photographic
fixer solution was discharged to a dry well which could overflow through a pipe into a stonn
drainage channel designated as SWMU #553.
In October 1993 the storm drainage channel was sampled using a Division approved plan as part
of the site RFI program. A report of the investigation was included in Thiokol Propulsion RCRA
Facility Investigation Source and Contamination Characterization Phase 1 SWMUs , August
2000 (2000 RFI report). This sampling is supplemental to information contained in the 2000 RFI
report. Although the 2000 RFI report showed constituent values that were below risk based
levels, the sampling indicated an increasing trend in silver concentrations with distance from the
discharge site. The new sampling included greater distances from the discharge point and
greater depths. Additional details can be found in the May 2016 SAP.
2.0 FIELD SAMPLING ACTIVITIES AND CHANGES
The sampling within the stream channel was completed at the depths and locations specified in
the SAP. However, on the day of sampling, it was noted that a visual difference was seen in the
soil along the west bank of the drainage stream at the first sampling point called the 50 foot
location. This difference was characterized by a dark coloration band. Using the hand held
Orbital ATL Solid Waste Management Unit 553 Resample
Promontory Facility ATK Launch Systems
SAMPLING RESULTS REPORT
XRF it was determined that this narrow zone of soil was highest in silver and chromium values.
With Jeff Vandel’s approval, investigation of the stream bank was included with the SAP. An
additional deviation from the SAP at the request of Jeff Vandel was the inclusion of Cr (VI)
analysis of samples that indicated high chromium content when using the XRF. There were two
sampling sites, the 50 ft. and 250 ft. where the XRF indicated high levels for the constituents of
concern. Both of these were along the west bank and associated with the distinctive dark color
band. Other sites along the bank were tested with the XRF and none were found that indicated
higher concentrations, nor were there any visual indications of the darker soil. Due to this
expanded investigation, many XRF readings were taken beyond what was noted in the field
book, therefore the location of some readings in the XRF files are approximate.
Based on the results of the initial sampling more samples were later collected in the two areas
along the bank that indicated higher metals values, specifically for Cr (VI). This sampling
helped to better define the extent of the higher values. These sample results are also included in
this report.
(VI) was found at concentrations that would exceed the residential RSLs. These higher Cr (VI)
values were found at two locations along the west bank of the drainage channel previously
described, at the 50 foot and at 250 feet. The 50 foot West Bank location had the highest values
for all constituents. The higher Cr (VI) values correlated to higher total chromium levels as
would be expected. The duplicate sample to “250”, called “250A”, was very comparable
indicating good laboratory reproducibility. The background samples matched other 2000 RFI
related background soil levels for metals with the exception of a higher value for silver. Figure 2
shows the sample results of the additional sampling conducted on the west bank at the 50 foot
location. This shows that the high Cr (VI) levels are primarily limited to a narrow band
approximately I foot wide and approximately 9 feet in length covered with approximately 2-3
feet of soil overburden. Closer examination of the darker band of soil shows that it appears to
contain ash with burnt twigs and grass. The other Cr (VI) samples in the location were less than
3.0 SAMPLE RESULTS
Figure 1 shows the sample results of both the initial and follow-up sampling events. Only Cr
Orbital ATK
SAMPLING RESULTS REPORT
Solid Waste Management Unit 553 Resample
Promontory Facility ATK Launch Systems
background. At the 250 - 300 foot west bank location the darker band of soil was also visible
although less pronounced, and the Cr (VI) value was lower at 2.6 ppm. The TCLP sample
collected at the 50 foot west bank location with the highest total cadmium, chromium and silver
analytical values were found to be far below TCLP hazardous waste levels. Comparison of the
field XRF data with the actual laboratory analytical results showed that in this situation the XRF
was only qualitative or an indicator of the actual values for the constituents of concern due to
possible interferences or calibration problems. The analytical data sheets are included in
Attachment A. A copy of the excel file with the XRF readings for silver chromium and
cadmium is in Attachment B. A copy of the field notes is found in Attachment C.
Figure 1
SWMU #553, Soil Sample Results
Values in mg/Kg unless noted
4 | P a g e April 20 17
Orbital ATK
SAMPLING RESULTS REPORT
Solid Waste Management Unit 553 Resample
Promontory Facility ATK Launch Systems
Figure 2
SWMU #553
Characterization of 50 ft. Location - West Bank
High Cr (VI) area general
dimensions and new
sampling points values in
ppm. RSIs = Res 0.30,
Ind. 6.3
ST*
• 4'* -iyak*
dm*
l>am? y C ^ * i', / ^ Cr (VI) 0.33 3i
* 1 ft. height
3 ft.------H . •
rm
' » A
mple points
5 | P a g e April 2017
Orbital ATI
SAMPLING RESULTS REPORT
Solid Waste Management Unit 553 Resample
Promontory Facility ATK Launch Systems
4.0 PROPOSED CORRECTIVE ACTION
A proposed corrective action for the high levels of Cr (VI) includes excavation of the narrow soil
band from the two areas. The excavated soil will then be mixed with native soil to reduce the
concentration to levels below the residential Regional Screening Level (RSL) of 0.3 mg/Kg.
This action is allowed since TCLP testing of the highest metal concentrations found at the site
are well below any levels for a hazardous waste designation and mixing is not prohibited. The
two proposed excavation areas are shown in Figure 3.
Figure 3
SWMU 553 Proposed Excavation Areas
Orbital ATi
SAMPLING RESULTS REPORT
Solid Waste Management Unit 553 Resample
Promontory Facility ATK Launch Systems
4.1 CORRECTIVE ACTION PROCESS
The corrective action process would use a backhoe to remove any soil overburden and then
visually remove the higher concentration band of Cr (VI) soil. It is believed that the dark color
characterizing this high level zone of Cr (VI) will be visible as the soil is excavated. Post
excavation confirmation sampling for Cr (VI) will be conducted to assure removal. As the
contaminated soil is removed it will be hauled to the onsite landfill and placed into a steel tray or
a secured location where it will be mixed with clean native soil. Confirmation sampling will be
conducted to assure that the mixing is complete and the soil is below the Cr (VI) RSL value of
0.3 mg/Kg. The soil will then be used as cover or fill.
4.2 CONFIRMATION SAMPLING AND ANALYSIS
Composite samples will be collected from the excavated areas at a depth of two to three inches
using a clean stainless steel scoop. Similarly, when the excavated soil is mixed with clean soil,
composite samples will be collected in the tray at the same depth.
Soil will be placed into a pre-cleaned polyethylene bowl. Plant material, roots, and large rocks
will be manually removed and the sample will be mixed prior to placing into a 4-oz wide-mouth
glass jar with a Teflon® lined lid.
All information collected during the field investigation will be maintained in a field log. Field
documentation will consist of the information provided in the RFI Work Plan QAAP.
The samples will be assigned analysis for Cr (VI) using EPA method 7199. Analysis will be
conducted by ATK Launch Systems Environmental Laboratory at the Promontory facility, a
laboratory certified in the State of Utah.
4.3 DECONTAMINATION PROCEDURES
Prior to and following the collection of each sample, any sampling equipment coming in contact
with the soil will be cleaned with a non-phosphate detergent (e.g., Liquinox®), rinsed with tap
water, and final rinsed with distilled water. Wastewater generated during field decontamination
will be collected and disposed of properly.
7 | P a g e April 20 17
Orbital ATi
SAMPLING RESULTS REPORT
Solid Waste Management Unit 553 Resample
Promontory Facility ATK Launch Systems
4.4 SAMPLE HANDLING AND CUSTODY
Sample containers will consist of glass jars, with Teflon-lined lids. Only decontaminated
stainless steel, polyethylene and/or clean disposable gloves will contact a sample during
placement in a bottle. Disposable gloves will be worn at all times during sample handling to
prevent cross contamination between samples and skin contact with potential contaminants.
Gloves will be disposed of between each sample.
Sample bottles will be placed on ice in waterproof cooler chests for delivery to the analytical
laboratory. Sample labels will be used to identify the samples. These labels will be sufficiently
durable to remain legible when wet and will be marked with indelible ink and affixed to the
sample containers.
A chain-of-custody form will be completed to trace sample possession from the time of
collection through laboratory analysis. One chain-of-custody form will accompany the cooler
container of samples. While the samples are in the custody of the collector, they will not be left
unattended at locations where the samples may be tampered with. The analyses to be performed
will be indicated on the chain-of-custody form, including the quantity and types of containers
that comprise each sample. The shipping container will then be securely closed and delivered to
the analytical laboratory.
All field data will be recorded in a log book. Information to be recorded in the log book will
include the date, time and depth of sample collection, descriptions of the soils encountered at
each sampling location, reasons for field decisions concerning sample intervals, reasons for
departures from prior plans, general observations, etc.
4.5 Field Quality Control Samples
Field QC samples will be analyzed for the same sample constituents as the samples-of-record.
QC samples will consist of collecting field duplicates as a minimum of 10% of the total samples.
4.6 Laboratory Quality Control
Internal laboratory quality control checks will be performed in accordance with the RFI Work
Plan QAPP.
8 | P a g e April 20 17
4.7 DATA MANAGEMENT
Field data will be recorded in a field log book. These data will be maintained in project files for
future reference. Hard copies of laboratory data will be maintained in project files. Electronic
data will be stored indefinitely. Hard-copy data will be maintained for a period of at least 3
years.
yCJ SAMPLING RESULTS REPORT
Orbital ATK/J Solid Waste Management Unit 553 Resample
Promontory Facility ATK Launch Systems
5.0 DATA REVIEW, VERIFICATION, AND VALIDATION
Data review, verification, and validation will occur as outlined in the RFI Work Plan QAPP.
9 | P a g e April 20 17
98CP LS336
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Requested
Monday, November 07, 2016
TESTED FOR:ATK: DLV
Environmental Monitoring
Thiokol Corp, UT 84322
ANALYZED BY:ATK Launch Systems
Analytical Chemistry Laboratory
P.O. Box 707, M/S 245
Brigham City, UT 84302-0707
435-863-3732
435-863-8080
Contact Name:Paul Hancock
Project:Remediation Testing - DLV
Sample Delivery Group:1609015
Page 1 of 7
Printed 11/07/16 1506
Sample Delivery Group: 1609015
Sample No. Client No.
Test Requested Sample Description
Received Collect Date/Time
Matrix
1609015-01 553 50 - E bank 09/17/16 09/15/2016 09.35 0
SW-846 Method 7199 Cr (VI) Metals Analysis by 1C Soil
SW-846. 1311 TCLP Extraction Soil
SW-846, 3010A Metals Digestion TCLP Extraction
SW-846, 3050B ICP/GFAA Metals Digestion Soil
SW-846, 3060A Alkaline Digestion for Hexavalent Chromium Soil
SW-846, 6010C (Solids)Metals Analysis by ICP - 6010C Soil
SW-846, 6010C (Water)Metals Analysis by ICP - 601 OC TCLP Extraction
1609015-02 553 150- 1 -2 09/17/16 09/15/2016 10 12 0
SW-846, 3050B ICP/GFAA Metals Digestion Soil
SW-846, 6010C (Solids)Metals Analysis by ICP - 6010C Soil
1609015-03 553 250 - E bank 09/17/16 09/15/2016 11:00:0i
SW-846, 3050B ICP/GFAA Metals Digestion Soil
SW-846, 601OC (Solids)Metals Analysis by ICP - 6010C Soil
1609015-04 553 250A - E bank 09/17/16 09/15/2016 11.00:0i
SW-846, 3050B ICP/GFAA Metals Digestion Soil
SW-846, 601 OC (Solids)Metals Analysis by ICP - 6010C Soil
1609015-05 553 Background 09/17/16 09/15/2016 11-05:0i
SW-846 Method 7199 Cr (VI) Metals Analysis by IC Soil
SW-846, 3050B ICP/GFAA Metals Digestion Soil
SW-846, 3060A Alkaline Digestion for Hexavalent Chromium Soil
SW-846, 601 OC (Solids)Metals Analysis by ICP - 601 OC Soil
1609015-06 553 300 - Surface 09/17/16 09/15/2016 12 45.0
SW-846, 3050B ICP/GFAA Metals Digestion Soil
SW-846, 60IOC (Solids)Metals Analysis by ICP - 601 OC Soil
1609015-07 553 350 - 25 - 3 09/17/16 09/15/2016 13:15:0
SW-846 Method 7199 Cr (VI) Metals Analysis by IC Soil
SW-846, 3050B ICP/GFAA Metals Digestion Soil
SW-846, 3060A Alkaline Digestion for Hexavalent Chromium Soil
SW-846, 601 OC (Solids)Metals Analysis by ICP - 6010C Soil
1609015-08 553 500 -1 09/17/16 09/15/2016 13 50:0
SW-846, 3050B ICP/GFAA Metals Digestion So11
SW-846, 6010C (Solids) Metals Analysis by ICR - 6010C So11
Page 2 of 7
Printed- 11/07/1615.06
Sample Delivery Group: 1609015
Sample No. Client No.Received Collect Date/Time
Test Requested Sample Description Matrix
1609015-09 553 300 - 3 NW bank 09/17/16 09/15/2016 14:40 0
SW-846, 3050B ICP/GFAA Metals Digestion Soil
SW-846, 6010C (Solids)Metals Analysis by ICP - 6010C Soil
Certified By: W 11/07/2016
W. Scott Fraser, Quality Assurance Officer Date
This certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation
Program (NELAP) unless otherwise annotated:
Page 3 of 7
Printed. 11/07/16 1506
Listing of Results by Sample
Sample Delivery Group: 1609015
Client Sample ID: 553 50 - E bank
Sample Description: ATK-DLV - SWMU553
Laboratory Sample ID: 1609015-01
Date Sampled: 09/15/16 09.35
Dilution
CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date
| Test Method:SW-846 Method 7199 Cr (VI) Metals Analysis by 1C 1
18540-29-9 CHROMIUM HEXAVALENT 22800.ug/kg 80 400 1 CRS 10/20/16
| Test Method:SW-846, 1311 TCLP Extraction |
1311 EXTRACTION 10/03/2016 1 MTB 10/03/16
\ Test Method:SW-846,3010A Metals Digestion 1
3010A ACID DIGESTION 10/04/2016 1 MTB 10/04/16
| Test Method:SW-846, 3050B ICP/GFAA Metals Digestion |
3050B ACID DIGESTION DATE 09/28/2016 1 MTB 09/28/16
| Test Method:SW-846, 3060A Alkaline Digestion for Hexavalent Chromium
3060A ALKALINE DIGESTION DATE 10/13/2016 1 MTB 10/13/16
| Test Method:SW-846, 6010C (Solids)Metals Analysis by ICP-6010C |
7440-43-9 CADMIUM 59 2 ug/g 0.1 0.5 1 MTB 09/30/16
7440-47-3 CHROMIUM 926 ug/g 1 5 1 MTB 09/30/16
7440-22-4 SILVER 195 ug/g 0.1 0.5 1 MTB 09/30/16
| Test Method:SW-846, 6010C (Water)Metals Analysis by ICP - 6010C |
7440-43-9 CADMIUM 670 ug/L 1 5 1 MTB 10/05/16
7440-47-3 CHROMIUM 124.ug/L 10 50 1 MTB 10/05/16
7440-22-4 SILVER 98.9 ug/L 1 5 1 MTB 10/05/16
Client Sample ID: 553 150- 1 -2 Laboratory Sample ID:1609015-02
Date Sampled: 09/15/1610.12
Sample Description: ATK-DLV - SWMU553
Dilution
CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date
| Test Method:SW-846,3050B ICP/GFAA Metals Digestion 1
3050B ACID DIGESTION DATE 09/28/2016 1 MTB 09/28/16
| Test Method:SW-846, 6010C (Solids)Metals Analysis by ICP - 6010C |
7440-43-9 CADMIUM 1 7 ug/g 0 1 0.5 1 MTB 09/30/16
7440-47-3 CHROMIUM 108 ug/g 1 5 1 MTB 09/30/16
7440-22-4 SILVER 183 ug/g 0 1 0 5 1 MTB 09/30/16
Client Sample ID: 553 250 - E bank Laboratory Sample ID:1609015-03
Date Sampled: 09/15/16 11 00
Sample Description: ATK-DLV - SWMU553
Dilution
CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date
| Test Method:SW-846, 3050B ICP/GFAA Metals Digestion |
3050B ACID DIGESTION DATE 09/28/2016 1 MTB 09/28/16
| Test Method:SW-846, 6010C (Solids)Metals Analysis by ICP - 6010C I
7440-43-9 CADMIUM 0.7 ug/g 0 1 0 5 1 MTB 09/30/16
7440-47-3 CHROMIUM 78 5 ug/g i 5 1 MTB 09/30/16
7440-22-4 SILVER 204 ug/g 0.1 0.5 1 MTB 09/30/16
Page 4 of 7
Printed- 11/07/1615.06
Listing of Results by Sample
Sample Delivery Group: 1609015
Client Sample ID:553 250A - E bank Laboratory Sample ID:1609015-04
Sample Description:ATK-DLV - SWMU553
Date Sampled:09/15/16 11 00
Dilution
CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date
Test Method: SW-846,3050B____________ICP/GFAA Metals Digestion
3050B ACID DIGESTION DATE 09/28/2016 1 MTB 09/28/16
| Test Method:SW-846, 6010C (Solids)Metals Analysis by ICP-6010C |
7440-43-9 CADMIUM 06 ug/g 0 1 0.5 1 MTB 09/30/16
7440-47-3 CHROMIUM 80.6 ug/g 1 5 1 MTB 09/30/16
7440-22-4 SILVER 207. ug/g 0.1 0.5 1 MTB 09/30/16
Client Sample ID: 553 Background Laboratory Sample ID:1609015-05
Sample Description: ATK-DLV - SWMU553
Date Sampled: 09/15/16 11.05
CAS Number Test Parameter Result Units MDL EQL
Dilution
Factor Analyst Test Date
| Test Method:SW-846 Method 7199 Cr(VI) Metals Analysis by 1C |
18540-29-9 CHROMIUM HEXAVALENT 110. J ug/kg 80 400 1 CRS 10/20/16
| Test Method:SW-846, 3050B ICP/GFAA Metals Digestion [
3050B ACID DIGESTION DATE 09/28/2016 1 MTB 09/28/16
| Test Method:SW-846, 3060A Alkaline Digestion for Hexavalent Chromium |
3060A ALKALINE DIGESTION DATE 10/13/2016 1 MTB 10/13/16
| Test Method:SW-846 6010C (Solids) Metals Analysis by ICP-6010C |
7440-43-9 CADMIUM 0.3 J ug/g 0 1 0.5 1 MTB 09/30/16
7440-47-3 CHROMIUM 15.ug/g 1 5 1 MTB 09/30/16
7440-22-4 SILVER 32.2 ug/g 0.1 0 5 1 MTB 09/30/16
Client Sample ID: 553 300 - Surface Laboratory Sample ID: 1609015-06
Date Sampled: 09/15/16 12 45
Sample Description: ATK-DLV - SWMU553
CAS Number Test Parameter Result Units MDL EQL
Dilution
Factor Analyst Test Date
| Test Method:SW-846 3050B ICP/GFAA Metals Digestion |
3050B ACID DIGESTION DATE 09/28/2016 1 MTB 09/28/16
| Test Method:SW-846, 6010C (Solids)Metals Analysis bylCP-6010C |
7440-43-9 CADMIUM 02 J ug/g 0.1 0.5 1 MTB 09/30/16
7440-47-3 CHROMIUM 13.3 ug/g 1 5 1 MTB 09/30/16
7440-22-4 SILVER 91 8 ug/g 0.1 0.5 1 MTB 09/30/16
Client Sample ID: 553 350-25-3 Laboratory Sample ID:1609015-07
Sample Description: ATK-DLV - SWMU553
Date Sampled: 09/15/161315
CAS Number Test Parameter Result Units MDL
Dilution
EQL Factor Analyst Test Date
| Test Method:SW-846 Method 7199 Cr (VI) Metals Analysis by 1C 1
18540-29-9 CHROMIUM HEXAVALENT 170. J ug/kg 80 400 1 CRS 10/20/16
Page 5 of 7
Printed- 11/07/1615.06
Listing of Results by Sample
Sample Delivery Group: 1609015
Client Sample ID: 553 350-25-3 Laboratory Sample ID:1609015-07
Sample Description: ATK-DLV - SWMU553
Date Sampled: 09/15/16 13:15
CAS Number Test Parameter Result Units MDL EQL
Dilution
Factor Analyst Test Date
| Test Method:SW-846, 3050B ICP/GFAA Metals Digestion
3050B ACID DIGESTION DATE 09/28/2016 1 MTB 09/28/16
| Test Method:SW-846, 3060A Alkaline Digestion for Hexavalent Chromium |
3060A ALKALINE DIGESTION DATE 10/13/2016 1 MTB 10/13/16
| Test Method:SW-846, 6010C (Solids) Metals Analysis by ICP - 6010C |
7440-43-9 CADMIUM 0.6 ug/g 0.1 0 5 1 MTB 09/30/16
7440-47-3 CHROMIUM 10 5 ug/g 1 5 1 MTB 09/30/16
7440-22-4 SILVER 41 3 ug/g 0.1 0.5 1 MTB 09/30/16
Client Sample ID: 553 500-1 Laboratory Sample ID:1609015-08
Sample Description: ATK-DLV - SWMU553
Date Sampled: 09/15/16 13 50
CAS Number Test Parameter Result Units MDL EQL
Dilution
Factor Analyst Test Date
| Test Method:SW-846, 3050B ICP/GFAA Metals Digestion |
3050B ACID DIGESTION DATE 09/28/2016 1 MTB 09/28/16
| Test Method:SW-846, 6010C (Solids) Metals Analysis by ICP - 6010C |
7440-43-9 CADMIUM 0.3 J ug/g 0 1 0.5 1 MTB 09/30/16
7440-47-3 CHROMIUM 12.3 ug/g 1 5 1 MTB 09/30/16
7440-22-4 SILVER 64.6 ug/g 0 1 0 5 1 MTB 09/30/16
Client Sample ID: 553 300 - 3 NW bank Laboratory Sample ID:1609015-09
Sample Description: ATK-DLV - SWMU553
Date Sampled: 09/15/16 14 40
CAS Number Test Parameter Result Units MDL EQL
Dilution
Factor Analyst Test Date
| Test Method:SW-846, 3050B ICP/GFAA Metals Digestion I
3050B ACID DIGESTION DATE 09/28/2016 1 MTB 09/28/16
| Test Method:SW-846, 6010C (Solids) Metals Analysis by ICP - 6010C |
7440-43-9 CADMIUM 0 9 ug/g 0 1 0.5 1 MTB 09/30/16
7440-47-3 CHROMIUM 45.6 ug/g 1 5 1 MTB 09/30/16
7440-22-4 SILVER 207 ug/g 0 1 0.5 1 MTB 09/30/16
Page 6 of 7
11/07/16 15.06Printed
Data Reporting Qualifiers
U Indicates that the analyte concentration is less than the MDL.
B This flag is used when an analyte is found in the blank as well as the sample.
J Indicates an extimated value. This flag is used either when estimating a concentration
for tentatively identified compounds or when the data indicated the presence of a
compound that meets the identification criteria but the result is less than the
EQL (e.g. 3 J with an EQL of 10).
MDL Method Detection Limit: The minimum concentration of a substance that can be
confidently measured and reported. The laboratory has demonstrated that the
MDL can be achieved in a laboratory reagent blank, but does not guarantee it
can be achieved in all sample matrices.
EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For
many analytes the EQL is selected as the value of the lowest standard in the
calibration curve.
Dilution Dilution Factor: The prepared sample was diluted by this factor because the
Factor sample was too concentrated or due to other interferences in the sample matrix.
Any dilution factor causes a corresponding increase in the MDL and EQL.
Page 7 of 7
Printed. 11/07/16 1506
ATK Space Systems Group
Environmental Laboratory
Client Name:.
CarDen
Hand delivered,
—STf tKV
elivered, no cooler AfHai
Sample Receipt Checklist
SDG No iioqoig'Date:.
Carrier Number
ind delivered, samplers) taken out at receiving counter
Initials;
Cooler Infoimation:
Cooler Number/ID;_____
Condition of Shipping Container
Cooler Sealed (taped):
Custody Seals Present:
'iUACph'
alnar UGood r.Falr
Coolant:
State of Coolant:
Thermometer ID:
Packing Description:
r.Yes
GFalr
UNo
'L
LNot Applicable
GNot Applicable
□Damaged (explain)
: Yes □Not Applicable
'Intact 3 Broken Seal Number
utce uSIuelce riNone Other
r Frozen ‘^Partially Frozen "Melted
Reading:.^"CF:Corrected Temp:_"C Temp Blank Included: ‘.Yes No
Chaln-Of-Custody Information:
COC PresentCOC Numberfs)' C \3 IOM
COC signed (relinquished and received).
COC or LWI agrees with sample labels:
•JNo Other________
rJNo UNot Applicable
.INo GNot Applicable
Sample Information:
Samples included In cooler qUVa A<xCT °
Custody Seals Present:i Yes Jo Other
"Intact Broken Seal Numberfst
Sample containers intact "'No Notes:
Samples in proper containers:□No
Sufficient sample volume:/■'bs GNo
AH samples received in hold time:‘Xes .INo
Water-VOA's have zero headspace: 'Yes GNo ivNot Applicable
Pre-preserved with HCl: Pro-preserved with NajSzOj' ' Non-Preserved:
Notes:
Water - pH acceptable upon receipt:□Yes □Adjusted (see comments below)5Wot Applicable
HNO- =HsSO. =NaOH =ZnAC /NaOH =HCL =
Water - pH adjusted: (mfg. & Lot No.)
\
fi
HNO.HaSO.NaOH ZnAC HCl l'
Na^SOXh Other
t
I)
SOP-102 Form A
ENVIRONMENTAL LAB WORK REQUEST
to: ORBITAL ATK ENVIRONMENTAL LABORATORY LWR No. E13704
Login No.
FROM;
rRu i
EXTENSION:COST CENTER:
8200
WORK ORDER:
3HffjO.03.3300.0000
DATE:
Mj/zolb
ORGANIZATION:1 ENVIRO•NMENTAL SERVICES
MAIL STOP-
301
REPORT RESULTS Tfl
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS
G c
1/isf fa Y
St/o mu stt<;TWaje S.<ivesr Chrot^iw^
fitdMtWM , C r~ (vlS LOW
€or- Crfvl)
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2.t>U? £L€£^TfDM
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rn/I V\Aiu.WA
H/fcUb X /^;ho
Cad^iuW'-,
£kvE>WAl'U\*-\
10.
11.
12.
13.
CHAIN OF CUSTODY
RELINQUISHED BY RECEIVED BY DATE TIME
Ha/ 1/Vn/m 0M5
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED SIGNATURE
98CP LS336
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Requested
Wednesday, December 14, 2016
TESTED FOR: ATK: DLV
Environmental Monitoring
Thiokol Corp, UT 84322
ANALYZED BY: ATK Launch Systems
Analytical Chemistry Laboratory
P.O. Box 707, M/S 245
Brigham City, UT 84302-0707
435-863-3732
435-863-8080
Contact Name:
Project-
Sample Delivery Group:
Paul Hancock
Remediation Testing - DLV
1611012
Printed.
Page 1 of 6
12/14/16 16.35
Sample Delivery Group: 1611012
Sample No. Client No. Received Collect Date/Time
Test Requested Sample Description Matrix
1611012-01 #150’H2 11/11/16 11/11/2016 10 55:0(
SW-846 Method 7199 Cr (VI) Metals Analysis by 1C Soil
SW-846, 3050B ICP/GFAA Metals Digestion Soil
SW-846, 3060A Alkaline Digestion for Hexavalent Chromium Soil
SW-846, 6010C (Solids)Metals Analysis by ICP - 6010C Soil
1611012-02 #2 50' H2 11/11/16 11/11/2016 11 05:0(
SW-846 Method 7199 Cr (VI) Metals Analysis by 1C Soil
SW-846, 3050B ICP/GFAA Metals Digestion Soil
SW-846, 3060A Alkaline Digestion for Hexavalent Chromium Soil
SW-846, 6010C (Solids)Metals Analysis by ICP - 6010C Soil
1611012-03 #3 50' H2 11/11/16 11/11/2016 11:10:0(
SW-846 Method 7199 Cr (VI) Metals Analysis by 1C Soil
SW-846, 3050B ICP/GFAA Metals Digestion Soil
SW-846, 3060A Alkaline Digestion for Hexavalent Chromium Soil
SW-846, 6010C (Solids)Metals Analysis by ICP - 6010C Soil
1611012-04 #4 50'H2 11/11/16 11/11/2016 11:16:0C
SW-846 Method 7199 Cr (VI) Metals Analysis by IC Soil
SW-846, 30SOB ICP/GFAA Metals Digestion Soil
SW-846, 3060A Alkaline Digestion for Hexavalent Chromium Soil
SW-846, 6010C (Solids)Metals Analysis by ICP - 6010C Soil
1611012-05 #5 50' H2 11/11/16 11/11/2016 11:21:0(
SW-846 Method 7199 Cr (VI) Metals Analysis by IC Soil
SW-846, 3050B ICP/GFAA Metals Digestion Soil
SW-846, 3060A Alkaline Digestion for Hexavalent Chromium Soil
SW-846, 6010C (Solids)Metals Analysis by ICP - 6010C Soil
1611012-06 #6 50'H2 11/11/16 11/11/2016 11:35.0(
SW-846 Method 7199 Cr (VI) Metals Analysis by IC Soil
SW-846, 3050B ICP/GFAA Metals Digestion Soil
SW-846, 3060A Alkaline Digestion for Hexavalent Chromium Soil
Page 2 of 6
12/14/16 16.35Printed'
Sample Delivery Group: 1611012
Sample No. Client No.
Test Requested Sample Description
Received Collect Date/Time
Matrix
1611012-06 #6 50' H2 11/11/16 11/11/2016 11 35 0(
SW-846, 6010C (Solids) Metals Analysis by ICR - 6010C Soil
___________
W. Scott Fraser, Quality Assurance Officer
12/14/2016
Date
This certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation
Program (NELAP) unless otherwise annotated:
Page 3 of 6
Printed- 12/14/16 16 35
Listing of Results by Sample
Sample Delivery Group: 1611012
Client Sample ID: #1 50' H2 Laboratory Sample ID:1611012-01
Sample Description: ATK-DLV - SWMU 553
Date Sampled: 11/11/16 10:55
CAS Number Test Parameter Result Units MDL EQL
Dilution
Factor Analyst Test Date
| Test Method:SW-846 Method 7199 Cr(VI) Metals Analysis by 1C |
18540-29-9 CHROMIUM HEXAVALENT 1710.ug/kg 80 400 1 MTB 11/28/16
| Test Method:SW-846. 3050B ICP/GFAA Metals Digestion |
3050B ACID DIGESTION DATE 12/05/2016 1 MTB 12/05/16
| Test Method:SW-846, 3060A Alkaline Digestion for Hexavalent Chromium |
3060A ALKALINE DIGESTION DATE 11/21/2016 1 MTB 11/21/16
| Test Method:SW-846, 6010C (Solids) Metals Analysis by ICR - 6010C |
7440-47-3 CHROMIUM 39.8 ug/g 1 5 1 MTB 12/06/16
Client Sample ID: #2 50' H2 Laboratory Sample ID:1611012-02
Sample Description: ATK-DLV - SWMU 553
Date Sampled: 11/11/16 11 05
CAS Number Test Parameter Result Units MDL EQL
Dilution
Factor Analyst Test Date
| Test Method:SW-846 Method 7199 Cr(VI) Metals Analysis by 1C |
18540-29-9 CHROMIUM HEXAVALENT 16900.ug/kg 80 400 1 MTB 11/28/16
| Test Method:SW-846, 3050B ICP/GFAA Metals Digestion I
3050B ACID DIGESTION DATE 12/05/2016 1 MTB 12/05/16
| Test Method:SW-846, 3060A Alkaline Digestion for Hexavalent Chromium ]
3060A ALKALINE DIGESTION DATE 11/21/2016 1 MTB 11/21/16
| Test Method:SW-846, 6010C (Solids) Metals Analysis by ICP - 6010C |
7440-47-3 CHROMIUM 671.ug/g 1 5 1 MTB 12/06/16
Client Sample ID: #3 50' H2 Laboratory Sample ID:1611012-03
Sample Description: ATK-DLV - SWMU 553
Date Sampled: 11/11/16 11:10
CAS Number Test Parameter Result Units MDL EQL
Dilution
Factor Analyst Test Date
| Test Method:SW-846 Method 7199 Cr (VI) Metals Analysis by 1C
18540-29-9 CHROMIUM HEXAVALENT 180. J ug/kg 80 400 1 MTB 11/28/16
| Test Method:SW-846, 3050B ICP/GFAA Metals Digestion |
3050B ACID DIGESTION DATE 12/05/2016 1 MTB 12/05/16
| Test Method:SW-846, 3060A Alkaline Digestion for Hexavalent Chromium
3060A ALKALINE DIGESTION DATE 11/21/2016 1 MTB 11/21/16
| Test Method:SW-846, 6010C (Solids) Metals Analysis by ICP - 6010C |
7440-47-3 CHROMIUM 13.1 ug/g 1 5 1 MTB 12/06/16
Page 4 of 6
Printed. 12/14/161635
Listing of Results by Sample
Sample Delivery Group: 1611012
Client Sample ID: #4 50'H2 Laboratory Sample ID:1611012-04
Sample Description: ATK-DLV - SWMU 553
Date Sampled: 11/11/16 11:16
CAS Number Test Parameter Result Units MDL EQL
Dilution
Factor Analyst Test Date
| Test Method:SW-846 Method 7199 Or (VI) Metals Analysis by 1C |
18540-29-9 CHROMIUM HEXAVALENT 688.ug/kg 80 400 1 MTB 11/28/16
| Test Method:SW-846, 3050B ICP/GFAA Metals Digestion |
3050B ACID DIGESTION DATE 12/05/2016 1 MTB 12/05/16
| Test Method:SW-846, 3060A Alkaline Digestion for Hexavalent Chromium |
3060A ALKALINE DIGESTION DATE 11/21/2016 1 MTB 11/21/16
| Test Method:SW-846, 6010C (Solids) Metals Analysis by ICP - 6010C |
7440-47-3 CHROMIUM 13.2 ug/g 1 5 1 MTB 12/06/16
Client Sample ID: #5 50' H2 Laboratory Sample ID:1611012-05
Sample Description: ATK-DLV - SWMU 553
Date Sampled: 11/11/16 11.21
CAS Number Test Parameter Result Units MDL EQL
Dilution
Factor Analyst Test Date
| Test Method:SW-846 Method 7199 Cr (VI) Metals Analysis by 1C |
18540-29-9 CHROMIUM HEXAVALENT 330.ug/kg 62 310 0.78 MTB 11/28/16
| Test Method:SW-846, 3050B ICP/GFAA Metals Digestion
3050B ACID DIGESTION DATE 12/05/2016 1 MTB 12/05/16
\ Test Method:SW-846, 3060A Alkaline Digestion lor Hexavalent Chromium
3060A ALKALINE DIGESTION DATE 11/21/2016 1 MTB 11/21/16
| Test Method:SW-846, 6010C (Solids) Metals Analysis by ICP - 6010C |
7440-47-3 CHROMIUM 13 ug/g 1 5 1 MTB 12/06/16
Client Sample ID: #6 50'H2 Laboratory Sample ID:1611012-06
Sample Description: ATK-DLV - SWMU 553
Date Sampled: 11/11/16 11.35
CAS Number Test Parameter Result Units MDL EQL
Dilution
Factor Analyst Test Date
| Test Method:SW-846 Method 7199 Cr(VI) Metals Analysis by 1C __________I
18540-29-9 CHROMIUM HEXAVALENT 140. J ug/kg 80 400 1 MTB 11/28/16
| Test Method:SW-846, 3050B ICP/GFAA Metals Digestion |
3050B ACID DIGESTION DATE 12/05/2016 1 MTB 12/05/16
| Test Method:SW-846, 3060A Alkaline Digestion for Hexavalent Chromium |
3060A ALKALINE DIGESTION DATE 11/21/2016 1 MTB 11/21/16
| Test Method:SW-846, 6010C (Solids) Metals Analysis by ICP - 6010C [
7440-47-3 CHROMIUM 14.4 ug/g 1 5 1 MTB 12/06/16
Page 5 of 6
Printed. 12/14/16 16 35
Data Reporting Qualifiers
U Indicates that the analyte concentration is less than the MDL
B This flag is used when an analyte is found in the blank as well as the sample.
J Indicates an extimated value. This flag is used either when estimating a concentration
for tentatively identified compounds or when the data indicated the presence of a
compound that meets the identification criteria but the result is less than the
EQL (e.g. 3 J with an EQL of 10).
MDL Method Detection Limit: The minimum concentration of a substance that can be
confidently measured and reported. The laboratory has demonstrated that the
MDL can be achieved in a laboratory reagent blank, but does not guarantee it
can be achieved in all sample matrices.
EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For
many analytes the EQL is selected as the value of the lowest standard in the
calibration curve.
Dilution Dilution Factor: The prepared sample was diluted by this factor because the
Factor sample was too concentrated or due to other interferences in the sample matrix.
Any dilution factor causes a corresponding increase in the MDL and EQL.
Printed’
Page 6 of 6
12/14/16 16.35
ATK Space Systems Group
Environmental Laboratory
Client Name:
..... IWi: -DlV
fa, J Hampd-.
Sample Receipt Checklist
______ SDG No. __________
(o W ol Z-
Carrier.Hand delivered, no cooler
_j___________________________________ Carriar Number_
/Hand delivered, sample(s) taken out at receiving counter_______
Date: UM/1 (*
Initials- •tL
Cooler Information:
Cooler Number/ID:
Condition of Shipping Container:f?Good rFair 1'iNot Applicable □Damaaed fexplain)
Cooler Sealed (taped)::.Yes '.’No Applicable
Custody Seals Present .-■Yes '’No C^tot Applicable
rjlntact jBiuken Seal Number:
Coolant f-iloe JBIue Ice i:None Other
State of Coolant: ^>Frozen
Thermometer ID: Readina
iPartially Frozen T MeKed
*4 “C CF:Corrected Temo: °C Temp Blank Included: "Yes No
Packing Description:
Chain-Of-Custody Information:COC Present “/res 1N0 Other.________
COC Numbers):___________^________
COC signed (relinquished and received): ares ONo I :Not ApplicableCOC or LWi agrees with sample labels: ^es :.:No HNot Applicable
Notes:__________________________________________________________________
Sample Information:
Samples included in cooler:y-4^
Custody Seals Present CYes •irfo Other
Illntact .: Broken Seal Humberts)
Sample containers intact r.No Notes:
Samples in proper containers:«Ves : iNo
Sufficient sample volume Vfes ;:No
All samples received in hold time:>^es :No
Water- VOA's have zero headspace- :Yes QNo a^ot Applicable
Pre-preservedwithHCI: rPre-preservedwithNajSjO,: : Non-Preserved:
Water - pH acceptable upon receipt:
HNO* =
TYes
H^O,=
Adjusted (see comments below)
NaOH «=
sfJot Applicable
ZnAC fNaOH =HCL =
Water - pH adjusted: (mfg. & Lot No.)
HNO,H^O,NaOH 2nAC HCf
NflnSOnO,Other
Notes:
SOP-102 Form A
ENVIRONMENTAL LAB WORK REQUEST
I TO: ATK LAUNCH SYSTEMS ENVIRONMENTAL LABORATORY LWR No.Login No.
FROM:
Paul Hancock
EXTENSION:
3344
COST CENTER
8200
Project SL Task #.
3HR30.03.33
00.0000
DATE- //
Nov-4-0^2016
ORGANIZATION:
| ENVIRONMENTAL SERVICES
MAIL STOP.
301
REPORT RESULTS TO:
Paul Hancock
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS
G c
Ll/n/ib y Cr, Cr (VI)
2.
((
u/n h b
r
X //l OS’Cr, Cr (VI)
e 1 f '
n! till (*X &3So //z //.’ to Cr, Cr (VI)
fl 4 SlAjWA M f t
/»/*//1 y tte So Hz,Hi Ho Cr, Cr (VI)
5.kli'lh ■x Hz l/:?(Cl-, ^
II 6. StDlW-H t *
ii/ nl XT U& So H'Z~irzs’(fir. (T. /\/1N
8.
’
■ 0.
11.
CHAIN OF CUSTODY
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED SIGNATURE
98CP LS336
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Requested
Wednesday, December 14, 2016
TESTED FOR:ATK: DLV
Environmental Monitoring
Thiokol Corp, UT 84322
ANALYZED BY:ATK Launch Systems
Analytical Chemistry Laboratory
P.O. Box 707, M/S 245
Brigham City, UT 84302-0707
435-863-3732
435-863-8080
Contact Name:Paul Hancock
Project:Remediation Testing - DLV
Sample Delivery Group:1611015
Page 1 of 4
Printed' 12/14/1616:39
Sample Delivery Group: 1611015
Sample No. Client No.Received Collect Date/Time
Test Requested Sample Description Matrix
1611015-01 250 A resample 11/17/16 11/17/2016 13 40:0i
SW-846 Method 7199 Cr (VI) Metals Analysis by IC Soil
SW-846, 3050B ICP/GFAA Metals Digestion Soil
SW-846, 3060A Alkaline Digestion for Hexavalent Chromium Soil
SW-846, 6010C (Solids)Metals Analysis by ICP - 6010C Soil
Certified By:
W. Scott Fraser, Quality Assurance Officer
12/14/2016
Date
This certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation
Program (NELAP) unless otherwise annotated:
Page 2 of 4
Printed: 12/14/16 1639
Listing of Results by Sample
Sample Delivery Group: 1611015
Client Sample ID:250 A resample Laboratory Sample ID: 1611015-01
Sample Description:ATK-DLV - SWMU 553
Date Sampled: 11/17/16 13.40
Dilution
CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date
| Test Method:SW-846 Method 7199 Cr (VI) Metals Analysis by 1C 1
18540-29-9 CHROMIUM HEXAVALENT 2830 ug/kg 80 400 1 MTB 11/28/16
| Test Method:SW-846, 3050B ICP/GFAA Metals Digestion |
3050B ACID DIGESTION DATE 11/29/2016 1 MTB 11/29/16
| Test Method:SW-846 3060A Alkaline Digestion for Hexavalent Chromium |
3060A ALKALINE DIGESTION DATE 11/21/2016 i MTB 11/21/16
| Test Method:SW-846 6010C (Solids)Metals Analysis by ICP-6010C |
7440-47-3 CHROMIUM 153.ug/g 1 5 1 MTB 11/30/16
Page 3 of 4
12/14/16 16.39Printed-
Data Reporting Qualifiers
U Indicates that the analyte concentration is less than the MDL.
B This flag is used when an analyte is found in the blank as well as the sample.
J Indicates an extimated value. This flag is used either when estimating a concentration
for tentatively identified compounds or when the data indicated the presence of a
compound that meets the identification criteria but the result is less than the
EQL (e.g. 3 J with an EQL of 10).
MDL Method Detection Limit: The minimum concentration of a substance that can be
confidently measured and reported. The laboratory has demonstrated that the
MDL can be achieved in a laboratory reagent blank, but does not guarantee it
can be achieved in all sample matrices.
EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For
many analytes the EQL is selected as the value of the lowest standard in the
calibration curve.
Dilution Dilution Factor: The prepared sample was diluted by this factor because the
Factor sample was too concentrated or due to other interferences in the sample matrix.
Any dilution factor causes a corresponding increase in the MDL and EQL.
Printed
Page 4 of 4
12/14/16 16:39
ATK Space Systems Group
Environmental Laboratory
&
Client Name:_
Carrier,
. Hand delivered, no cooler_______n Hand delivered, samples) taken out at receiving counter
Sample Receipt Checklist
______ SDGNo. ___________[U ll 0 l1?Date.
Carrier Number,Initials:■ m
Cooler Infbrmatioi
Cooler Number/ID:
Condition of Shipping Container
Cooler Sealed (taped):
Custody Seals Present:
Coolant
State of Coolant:
"fedUlir__
kintalner UGood 'Fair
::Yes
r'Yes
rjlntact
Ulce
'Frozen
rFpir
WoNo
'-’No
j Broken
[■‘Blue Ice ('Nona
«Mrtially Frozen
rj Not Applicable
T-Not Applicable
□Not Applicable
□Damaged (explain).
Seal Number _
Other_______
□Melted
Thermometer ID: ■\laP\3fe6ftS' Reading: [6»& "C CF:_
Packing Description.
Corrected Temp:,"C Temp Blank Included: : Yes No
COC Present:
COO NumbertsV y
□No Other
COC signed (relinquished and received)-
COC or LWI agrees with sample labels:4z □ No
.'□No
□Not Applicable
□ Not Applicable
Notes:
Sample Information:
Samples included in cooler tL
Custody Seals Present:
Sample containers Intact:
Samples In proper containers.
Sufficient sample volume:
All samples received in hold time: tfes
Water- VGA's have zero headspace:
. Pre-preserued with MCI:
Notes:
□Yes Other
□Intact 'JBroRen Seal Numberfs)tt^ss "‘No Notes:
Wes LINO
\ftfs JNo
"No
.Yes
□No ^ot Applicable
rPre-preserved with NajSjO.:Non-Preserved:
Water - pH acceptable upon receipt ' i Yes
HNOj =HjSO. =
-Adjusted (see comments below)
_____________NaOH =__________
lot Applicable
_ZnAC /NaOH =_HCL =
Water - pH adjusted: (mfg. & Lot No.)
HNOsH2SO<_NaOH _ZnAC_HCI,
NajSOjOj
Notes:
Other
SOP-102 Form A
^Cb- jkllol'S
ENVIRONMENTAL LAB WORK REQUEST
to: ATK LAUNCH SYSTEMS ENVIRONMENTAL LABORATORY LWR No.
Login No.
FROM;
Paul Hancock
EXTENSION:
3344
COST CENTER;
8200
Project & last it:
3HR30.03.33
00.0000
DATE:
Nov. 17,2016
ORGANIZATION.
1 ENVIRONMENTAL SERVICES
MAIL STOP;
301
REPORT RESULTS TO:
Paul Hancock
SAMPLE INFORMATION
I SAMPLE DATE TYPE LOCATION TIME TEST REMASKS
G C
i. SWMU553 Nov. 17/16 X 250 A resample tl'-p Cr, Cr (VI)
2.
3.
4.
5.
6.
7.
S.
9
10.
(1.
CHAIN OF CUSTODY
RELINQUISHED BY DATE TIME RECEIVED BY DATE TIME
Vrr//b fo!o€>Ufo//6 fe.'Oo
FOR LABORATORY USE ONLY
DATE REPORTEDDATE COMPLETED SIGNATURE
Attachment B
Ag
<LOD
<LOD
<LOD
25062
28536
1171
<LOD
<LOD
195
131
<LOD
10347
69
154
<LOD
82
98
105
166
<LOD
<LOD
cLOD
CLOD
258
189
80
5379
4340
cLOD
5204
475
cLOD
cLOD
cLOD
5487
67
270
343
1929
4394
604
913
299
341
209
247
XRF Readings
SWMU 553 Sept. 15, 2016
Cr Cd Sample Location/ depth
cLOD cLOD 50' / surface
cLOD cLOD 50' / 1-2 ft
cLOD cLOD 50' / 2.5-3 ft
278 cLOD 50 1 / west bank
659 cLOD 50' / west bank
cLOD cLOD 50' / west bank
cLOD cLOD 50 ' / west bank
cLOD cLOD 50 ' / west bank
cLOD cLOD 50' / west bank
cLOD cLOD 50' / west bank
cLOD cLOD 50' / west bank
cLOD cLOD
50' / west bank
cLOD cLOD west bank
cLOD cLOD west bank
cLOD cLOD west bank
cLOD cLOD west bank
cLOD cLOD west bank
cLOD cLOD west bank
cLOD cLOD west bank
cLOD cLOD along west bank
cLOD cLOD along west bank
cLOD CLOD along west bank
cLOD cLOD along west bank
cLOD cLOD 150' / surface
cLOD cLOD 150' /1-2 ft.
cLOD cLOD 150' / 2-5 - 3 ft.
338 cLOD 250 ft/west bank
275 cLOD 250 ft/ west bank
cLOD cLOD 250 ft/west bank
340 cLOD 250 ft / west bank
cLOD cLOD
250 ft/west bank
cLOD cLOD 250' / Surface
cLOD cLOD 250' /1 ft
cLOD cLOD 250' /1-2 ft
cLOD cLOD 250 - 300 ft west bank
cLOD cLOD 250 - 300 ft west bank
cLOD cLOD 250 -300 ft west bank
cLOD cLOD 250 -300 ft west bank
cLOD cLOD 250 - 300 ft west bank
cLOD cLOD 250 - 300 ft west bank
cLOD cLOD 300 ft west bank
cLOD cLOD 300 ft west bank
cLOD cLOD 300 ft west bank
cLOD cLOD 300 ft west bank
cLOD cLOD 300 ft west bank
307 cLOD 300 -350 ft west bank
Date
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
15-Sep-16
Time
9:03:05
9:08:20
9:14:19
9:19:07
9:20:54
9:23:54
9:25:57
9:28:37
9:30:47
9:31:57
9:35:18
9:36:51
9:38:31
9:40:53
9:42:23
9:43:37
9:44:26
9:45:31
9:46:32
9:48:53
9:58:39
10:06:38
10:07:29
10:11:29
10:12:22
10:17:44
10:22:21
10:24:14
10:28:32
10:30:49
10:31:38
10:33:46
10:41:40
10:42:26
10:52:12
10:53:03
10:53:56
10:54:47
10:59:31
11:00:19
11:04:27
11:05:41
11:06:51
11:07:38
11:09:01
11:11:10
Reading
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
* Some locations are approximate
Attachment B XRF Readings
SWMU 553 Sept. 15, 2016
Date Time Reading Ag Cr Cd Sample Location/depth
15-Sep-16 11:12:19 49 <LOD cLOD cLOD 300 - 350 ft west bank
15-Sep-16 11:14:57 50 <LOD cLOD cLOD 300 - 350 ft west bank
15-Sep-16 12:48:19 52 72 cLOD cLOD 300 ft/ surface
15-Sep-16 12:51:24 53 CLOD 1149 53 300 ft / 1 ft
15-Sep-16 12:52:33 54 CLOD 717 cLOD 300 ft / 1.5-2 ft
15-Sep-16 12:53:26 55 CLOD 838 cLOD 300 ft / 2.5-3 ft.
15-Sep-16 12:54:25 56 cLOD 824 cLOD ?
15-Sep-16 12:55:17 57 cLOD 491 cLOD ?
15-Sep-16 12:56:20 58 cLOD 1025 60 ?
15-Sep-16 13:06:01 59 cLOD 362 cLOD 350' / Surface
15-Sep-16 13:06:53 60 cLOD 614 cLOD 350' /1 ft.
15-Sep-16 13:11:48 61 cLOD 620 cLOD 350' / 1.5 - 2 ft.
15-Sep-16 13:13:03 62 cLOD 1027 cLOD 350' / 2-5 - 3 ft.
15-Sep-16 13:18:50 63 cLOD 724 cLOD 350' /4 ft.
15-Sep-16 13:28:41 64 calibrate
15-Sep-16 13:30:31 65 cLOD cLOD cLOD west bank area
15-Sep-16 13:33:24 66 cLOD cLOD cLOD west bank area
15-Sep-16 13:41:03 67 cLOD cLOD cLOD west bank area
15-Sep-16 13:44:05 68 49 cLOD cLOD 500 1 / surface
15-Sep-16 13:45:48 69 99 cLOD cLOD 500’ / 1ft.
15-Sep-16 13:46:49 70 97 cLOD cLOD 500' / 1.5 - 2 ft
15-Sep-16 13:50:41 71 cLOD cLOD cLOD 500 ' / 2.5 - 3 ft.
15-Sep-16 13:53:25 72 cLOD cLOD cLOD Areas along west bank
15-Sep-16 13:54:26 73 cLOD cLOD cLOD Area along west bank
15-Sep-16 14:20:06 75 562 cLOD CLOD 300 ft west bank area
15-Sep-16 14:22:41 76 673 cLOD cLOD 300 ft west bank area
15-Sep-16 14:23:43 77 590 cLOD cLOD 300 ft west bank area
15-Sep-16 14:24:39 78 154 cLOD cLOD 300 ft west bank area
15-Sep-16 14:26:24 79 203 cLOD cLOD 300 ft west bank area
15-Sep-16 14:27:17 80 701 cLOD cLOD 300 ft west bank area
15-Sep-16 14:30:38 81 319 cLOD cLOD 300 ft west bank area
15-Sep-16 14:36:53 82 285 cLOD cLOD 300 ft west bank area
15-Sep-16 14:37:57 83 cLOD cLOD cLOD 300 ft west bank area
15-Sep-16 14:39:27 84 76 cLOD cLOD 300 ft west bank area
15-Sep-16 14:40:26 85 111 cLOD cLOD 300 ft west bank area
15-Sep-16 14:41:31 86 167 cLOD cLOD 300 ft west bank area
* Some locations are approximate
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