DSHW-2012-011780 - 0901a0688032d6ad

HAZARDOUS WASTE INSPECTION REPORT
Division of
Solid and Hazardous Waste
DEC 1 2 2012
MI - omzo
Dates of Inspection:
Facility:
Facility Contact:
Notification:
Applicable Regulations:
Type of Inspection:
Participants:
Time of Arrival:
Time of Departure:
Report Prepared by:
September 25th, 26th and 27th, 2012
ATK Launch Systems Inc. - Promontory
P.O. Box 707
Brigham City, UT 84302-0707
George Gooch, Manager
Environmental Services
[phone]
UTD009081357 Generator, TSD
RCRA Permit, UAC R315
CEI
Jeff Vandel, Inspection Leader, DSHW
Hao Zhu, DSHW
George Gooch, ATK
Blair Palmer, ATK
Randy Fullmer, ATK
Susan Knapp, ATK Internal Auditor
25 September 2012: 8:55 AM
26 September 2012: 9:05 AM
25 September 2012: 4:00 PM
26 September 2012: 3:30 PM
Jeff Vandel
Facilitv Description
ATK Chemical Corporation first began operations at the ATK Launch Systems - Promontory
(ATK) facility in 1956. ATK and its predecessors have been primarily involved in the research,
testing and production of rocket motor propellants. The manufacturing processes at ATK -
Promontory include the preparation and mixing of high-energy ingredients, casting and curing of
the propellant formulations, assembly of rocket motor segments (or military flares), and quality
control testing of finished products. These activities have included the production and testing of
motors for the Space Shuttle, the wash-out and reloading of Minuteman ICBMs, and many other
projects for the Department ofDefense (DOD).
1
The ATK facility is a 20,000 acre site that is remotely located in Box Elder County,
approximately 30 miles northwest of Brigham City, Utah. The closest inhabitants to the facility
live approximately one mile to the west of the administration area on a cattle ranch.
The ATK plant is divided into four major areas designated as: Defense and Launch Vehicle
(DLV), Administrative and Manufacturing Area (or Space), Test Area, and High Performance
Propellant Development Area (or Plant III). There are approximately 675 buildings located on
the four areas that comprise the ATK plant.
Currently, ATK's primary activities consist of: military flare production; work on the next
generation of the Space Launch System, 5 segment solid rocket motor called "Liberty";
restoration of stages one and two of Minuteman motors; destruction of third stage Minuteman
motors by open burning; rocket motor casing work for Castor, GEM 40 and GEM 60 motors and
production work on Trident D-5 motor nozzles.
Waste Stream Management
ATK generates, treats, and stores characteristic and listed hazardous wastes as defined by R315-
2 of the Rules as a result of its manufacturing and demilitarization activities. ATK has RCRA
Part B permits for hazardous waste storage, and post-closure care. In addition, ATK treats
reactive (and/or ignitable) hazardous wastes at the facility primarily by open burning, although
wastes are also occasionally treated by open detonation. These treatment activities are conducted
at two separate sites at the facility. These OB/OD sites are designated as M-136, which is
located north ofthe Administration and Manufacturing Areas and M-225, which is located in the
southeast area of the facility at Plant III. A permit module containing conditions for open
burning and open detonation - "Thermal Treatment of Energetic Wastes" - was added to the
Hazardous Waste Storage Permit on September 30, 2010.
There are six permitted storage areas at the ATK facility: M-186, M-705S, E-501, S-633, M-603
and M-47. ATK is also permitted to store solid reactive waste received from off-site at the
M-136 Burn Grounds for up to 14 days. In addition, ATK is permitted to treat waste hydrazine
at building T-29B by dilution in accordance with Module V of ATK's Storage Permit. Dilution
of waste hydrazine with water is a DOT requirement for shipping this highly volatile material
off-site to a waste disposal facility. This inspection report covers these hazardous waste
management activities at the Promontory facility.
Inspection
Credentials, Purpose and Scope
The ATK - Promontory inspection was scheduled in early September 2012. The Bear River
Health Department was notified of the inspection and was invited to participate. The inspection
was initiated on the morning of September 25th and concluded on the afternoon of September
26th, 2012. It was stated at the beginning ofthe inspection that it was being conducted to
evaluate ATK's compliance with its RCRA permits and the Hazardous Waste Management
2
Rules (the Rules). The scope of the inspection, and an approximate schedule, was then discussed
with ATK personnel. Prior to the inspection, it was decided to focus on the following areas:
M-136 and M-225 Open Burning Grounds - inspect the site, condition of burn trays,
condition of containers (if any) and the operating record.
M-l 86 and M-705S Hazardous Waste Storage - inspect the site, condition of containers,
sumps, operating record for inspections.
X-ray Photograph Sites - inspect one or more of these sites to be determined in the field.
Machine Shop - inspect the site, waste management practices and 90-day waste dock.
Inspect main sources of reactive hazardous waste. Look for potential for reducing
"contaminated debris" that is sent to the burn grounds for open burning.
Inspect sources of rags, debris, flammable liquids and sludge that are generated from the
"painting/coating" operations at the facility.
T29B Hydrazine Treatment facility - inspect the site, look at records.
Waste Analysis records for reactive hazardous wastes generated on and off-site. Also
treatment effectiveness records for burn ground ash and residue.
Inspect the burn ground operating record for notation of clearing index, wind speed, etc. as
required by Condition IV.C.3.e.
Manifests - look at a number of manifests for wastes received and wastes shipped.
In addition to discussing the scope of the inspection, ATK personnel were asked some questions
that were prepared prior to the inspection to get current information on hazardous waste issues at
the facility. These questions and the notes taken while they were discussed are included with the
Pre-inspection Checklist in Appendix A.
M-225 Burn Grounds
The M-225 Burn Grounds are located at Plant III. Access to Plant III is controlled and the Burn
Grounds are enclosed by a fence with a locked gate. Open Burning at M-225 is conducted much
less frequently and at lower quantities than at M-136. Only hazardous wastes that are generated
from development projects at Plant III are burned at M-225.
Reactive, hazardous waste is brought to the M-225 Burn Grounds from the 90-day waste docks
located at Plant III. The 90-day clock begins once the waste is placed at the dock and ends once
the waste is burned at M-225. The day after the waste is burned, it is inspected to see if it was
burned completely. If it was, it is placed into a roll-off container and then is taken to the solid
waste landfill located at the M-l 36 Burn Grounds. If the burn was not complete, based on the
visual inspection, it is burned again. If the waste stream that is burned has a listed waste code
associated with it, it is burned separately and the ash is placed in a container and is shipped off-
site as hazardous waste.
The burn trays are either covered or turned upside down when not in use. Inspection records for
the M-225 Burn Grounds for the months April through July, 2012 have been inspected and are
attached to this report in Appendix B. Activity at Plant III has substantially decreased in recent
3
years, so the Burn Grounds are used much less frequently. During the inspection, the burn
ground area and burn pans were clean and in good condition.
M-136 Burn Grounds
The vast majority of reactive hazardous wastes that are open-burned at ATK are burned at the
M-136 Burn Grounds. Module IV - Thermal Treatment of Energetic Wastes was added to the
ATK Storage Permit on September 30, 2010. This Module contains conditions for the
management of both burn grounds. Open burning is typically conducted once or twice each
week at M-136 when the clearing index is 500 or greater. During the winter months, the clearing
index is commonly below 500 and burns are conducted less frequently. Like at M-225, the
quantity of waste that is burned at M-l 36 has decreased significantly in recent years.
The Burn Grounds are located within ATK's secured area, and entry into the Burn Grounds is
further controlled by a gate at the access road. The Bum Grounds are equipped with video
cameras, an alarm system, and a bunker from which burn events are monitored and controlled.
Open burning is mainly conducted in steel pans or trays. A variety of containers are used to hold
the hazardous waste (reactive and/or ignitable waste) that is burned in the pans. These containers
include super sacks, plastic bags, slids, and cardboard boxes and drums.
During the inspection, the remains of 300 pound, D-5 motor segments were observed at Burn
Station 14. The motor segments were burned the previous day. ATK maintains a waste tracking
system that utilizes bar codes that are attached to waste containers. The tracking information is
kept in an Access database. A printout of some of the information that is kept in the database is
included with this report in Appendix C. The record for the treatment of the D-5 motor segments
that were observed during the inspection is shown at the bottom of the printout.
Permit Condition IV.C.3.e. requires that ATK record in the operating record the temperature,
wind speed, wind direction, sky conditions and clearing index each time an open burn is
conducted at the facility. Prior to the inspection, it was decided to check to see that these
meteorological conditions are being recorded as required. As can be seen in the record included
in Appendix C, ATK is recording these conditions and appears to be in compliance with this
requirement.
During the inspection, Burn Stations 13, 7 and 6 were also observed. At station 13, ATK uses
"clamshell trays." These are metal boxes with vented lids where smaller, potentially propulsive
waste items (e.g. igniters) are burned. "Super sack" containers of solid propellant that had been
washed out of AMRAAM air to air missiles were observed in burn trays at Burn Station 7 during
the inspection. The containers had an accumulation start date of 9/24/2012, so they had been
placed in the trays the day before the inspection. "Slid" containers shipped up from the ATK
Bacchus facility are burned at Burn Station 6. The burn trays at this station are filled with gravel
to protect the tray. The trays at Burn Station 6 were empty during the inspection.
ATK burns whole rocket motor segments (e.g. Third Stage, Minuteman III motors) at Burn
Station 14. Some motors are split open prior to burning with linear charges. Others, such as the
V
4
Minuteman III, are treated by removing the nozzles and then burning the motor aft end up. If the
burn is determined to be complete, the residue and ash remaining after the burn is collected and
then placed into the on-site solid waste landfill.
Run-on of precipitation at M-136 is controlled by drainage ditches that direct surface water flow
around the burn grounds. These drainage ditches were inspected earlier in 2012 and appear that
they would drain surface water around the burn grounds. Run-off is also controlled by drainage
ditches although storm water flow generally just seeps into the ground, as it has not been
observed in ditches downhill of the burn grounds. The Division is currently reviewing a Storm
Water Management Plan that ATK has submitted to our office in accordance with the Thermal
Treatment of Energetic Wastes permit module.
During the inspection, analytical results of ash from past open burning events at M-136 were
requested. ATK provided laboratory reports for ash samples that were collected in March, 2012,
May 2010, May, 2003 and June 2003. All of these ash samples were analyzed for perchlorate
except the 2012 samples were analyzed for perchlorate and NG, HMX and RDX.
Perchlorate was detected in the 2012 ash sample at 4.48 mg/kg and HMX was detected at 0.43
mg/kg. Perchlorate was not detected in the ash samples that were collected in 2010 and 2003.
Copies of these analytical reports are included with this report in Appendix D. These
concentrations of perchlorate and HMX in the 2012 ash sample do not make the material
hazardous (the waste was deactivated), however, the disposal of potentially contaminated ash in
the on-site solid waste landfill is a concern. The Division is currently investigating perchlorate
contamination at the area and in groundwater. ATK's practice of disposing burn ground ash and
residue in the on-site landfill will be a part of this investigation.
M-186 Hazardous Waste Storage Area
The M-l 86 hazardous waste storage area is the primary, permitted storage facility at ATK.
Access to the facility is controlled by the gate at the entrance to the M-136 Burn Grounds. An
additional fence surrounds the storage area, and appropriate signs are posted on the fence at the
entrance and other locations. The facility is enclosed on three sides and has a roof. The floor is
sealed concrete, and is sloped towards collection sumps.
The inspection of the storage area included an examination of the containers, hazardous waste
labels, the eyewash and shower stations, fire extinguishers, sumps, and grounds. A copy ofthe
contingency plan is kept at the facility.
ATK also receives hazardous waste from off-site ATK facilities for storage and/or accumulation
prior to shipping the waste off-site for treatment and disposal. These ATK facilities include
Space Systems, Case Refurbishment Center (CRC), Composite Structures and Bacchus.
Hazardous wastes that are not treated at ATK Promontory are stored at the M-l 86 storage
facility until they are shipped off-site for treatment and disposal. No problems were observed
during the inspection. The storage area appears to be well managed. Inspections of the area are
conducted daily and the sumps are inspected by guards on weekends.
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M-705S Hazardous Waste Storage
Building M-705S is one of the permitted hazardous waste storage facilities. This storage facility
is relatively small and is used for storing hazardous waste, accumulating small quantities of
hazardous waste for packaging in drums and compacting rags contaminated with hazardous
waste. Containers were covered and properly labeled. Inspection records for the facility were
reviewed in the building. The storage facility appears to be well managed. No problems were
observed.
M-24 Propellant Mix Building and M-300 Propellant Casting Building
At the beginning of the inspection, the propellant mix building (M-24) was identified by ATK as
one of the larger sources of reactive hazardous waste. Some reactive hazardous waste is also
generated at the propellant casting building (M-300). Based on information provided by ATK
personnel, ATK has put processes in place to reduce the amount of contaminated waste (e.g.
gloves contaminated with propellant) that is generated from these manufacturing activities and
sent to the burn grounds for open burning. According to ATK this type of waste has been
reduced in the last ten years from approximately 1,200 pounds per rocket motor segment to about
400 pounds.
The propellant-contaminated waste that is currently generated at these buildings consists of:
cotton and rubber gloves, rags, scrapers, pink poly material, and craft paper. Excess and scrap
propellant, that is sent to the burn grounds, is also generated at these buildings.
Hazardous wastes generated here are managed by using satellite accumulation containers -
which are emptied daily when operations are conducted, and 90-day "waste docks" which are
located outside of the buildings. ATK is currently using a non-hazardous, citrus-based solvent
for cleaning metal parts and tools with rags.
E-517 Machine Shop
A large machine shop is located in the E-517 building complex. In addition to machining metal
parts, the nozzles for Trident D5 missiles are assembled and painted in this building. Work is
also done in the shop on the Castor, GEM 40 and GEM 60 projects. The bulk ofthe hazardous
waste that is generated in the building is waste rags contaminated with methyl ethyl ketone
(MEK, waste code D035). There are many satellite accumulation containers in the area. These
containers are ten gallon metal cans with flip-top lids. The cans are labeled "Waste Flammable
Solids." Every night these cans are emptied into drums that are kept outside the building in a 90-
day accumulation area. This area, referred to as a 90-day hazardous waste dock, is an enclosed
shed with a locked door and drums are kept on containing pallets.
ATK assigns employees to be "Waste Dock Coordinators." These employees are responsible for
the management of hazardous wastes that are generated in their area and accumulated at their
local 90-day waste dock. The coordinator for building E-517 is Dan Loomis. The training
record for this employee was requested. Based on the record, it appears that ATK is in
6
compliance with the Personnel Training requirements (Permit Section II.H.) of the Hazardous
Waste Storage Permit.
M-16 Flare Casting Building
The production of military flares has become a major part of ATK's business in recent years.
The flare casting building was visited during the inspection. Reactive hazardous waste (flare
propellant) and propellant-contaminated waste is generated at the building. This waste stream
includes "grain caps" which are plastic caps that are pushed into the propellant at the top of the
flare before it is cast, gloves, rags and rumple cloth. Based on our discussion of the generation
of these propellant-contaminated wastes during the inspection, it appears that ATK is making an
effort to minimize them.
T-29B Hydrazine Dilution
In recent years, the generation of waste hydrazine at ATK has significantly declined. In addition,
ATK has started filtering used hydrazine after static tests instead of disposing of all of it. This
practice of recycling the used hydrazine has been working, but ATK occasionally still dilutes
waste hydrazine and ships it off-site for disposal. The hydrazine dilution building was inactive at
the time ofthe inspection and was not inspected.
Hazardous Waste Storage Facilities E-501, S-633, M-603 and M-47
These hazardous waste storage facilities were not in use at the time of the inspection and
therefore were not inspected.
Operating Record
Records observed during the inspection, or taken with us for later observation, included:
personnel training records, inspection records, hazardous waste manifests, burn ground records,
the 2011 Biennial Report and waste analysis records.
Two areas of concern were identified through the inspection of these records. These issues are
addressed below.
Compliance Status
R315-2 General Requirements
2- 6 Requirements for Recyclable Materials - OK
R315-3 Application and Permit Procedures for Hazardous Waste Treatment, Storage, and
Disposal Facilities
3- 1 General Information - OK
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3-2 Permit Application - OK
3-3 Permit Conditions - OK
3-4 Changes to Permit - OK
3-5 Expiration and Continuation of Permits - OK
3-6 Special Forms of Permits - OK
3-7 Interim Status - OK
R315-5 Hazardous Waste Generator Requirements
5-1 Purpose, Scope and Applicability - OK
5-2 The Manifest - OK
5-3 Pre-Transport Requirements
3.34 Accumulation Time - OK
5-4 Recordkeeping and Reporting - OK
R315-8 Hazardous Waste Treatment, Storage, and Disposal Facility Requirements
8-1 Purpose, Scope and Applicability
8-2 General Facility Standards
2.1 Applicability - The regulations in this section apply to ATK
2.2 Identification Number - OK
2.3 Required Notices - OK
2.4 General Waste Analysis - OK
2.5 Security - OK
2.6 General Inspection Requirements - OK
2.7 Personnel Training - OK
2.8 General Requirements for Ignitable, Reactive, or Incompatible Wastes - OK
R315-8-3 Preparedness and Prevention
3.1 Applicability - The regulations in this section apply to ATK
3.2 Design and Operation of Facility - OK
3.3 Required Equipment - OK
3.4 Testing and Maintenance of Equipment - OK
3.5 Access to Communications or Alarm System - OK
3.6 Required Aisle Space - OK
3.7 Arrangements with Local Authorities - OK
8
R315-8-4 Contingency Plan and Emergency Procedures
4.1 Applicability - The regulations in this section apply to ATK
4.2 Purpose and Implementation of Contingency Plan - OK
4.3 Content of Contingency Plan - OK
4.4 Copies of Contingency Plan - OK
4.5 Amendment of Contingency Plan - OK
4.6 Emergency Coordinator - OK
4.7 Emergency Procedures - OK
R315-8-5 Manifest System, Recordkeeping, and Reporting
5.1 Applicability - The regulations in this section apply to ATK
5.2 Use of Manifest System - OK
5.3 Operating Record - OK
5.4 Manifest Discrepancies - OK
5.5 Availability, Retention, and Disposition of Records - OK
5.6 Biennial Report - A mistake was observed in the Biennial Report. ATK indicated
on two GM Forms for the generation of reactive hazardous waste, that the waste was
shipped off-site instead of being managed on-site by open burning. ATK has been made
aware of the mistake and will correct it in their record.
5.7 Unmanifested Waste Report - NA
5.8 Additional Reports - OK
R315-8-7 Closure and Post-Closure - OK
R315-8-8 Financial Requirements - Not reviewed during this inspection
R315-8-9 Use and Management of Containers
9.1 Applicability - The regulations in this section apply to ATK
9.2 Condition of Containers - OK
9.3 Compatibility of Waste with Containers - OK
9.4 Management of Containers - OK
9.5 Inspections - OK
9.6 Containment - OK
9.7 Special Requirements for Ignitable or Reactive Waste - OK
9.8 Special Requirements for Incompatible Wastes - OK
9.9 Closure - NA
9.10 Air Emission Standards - OK
R315-8-16 Miscellaneous Units - ATK disposes of ash and residue that have been judged to be
deactivated by open burning in an on-site, solid waste landfill. Analytical results of an ash
sample collected in March of 2012 indicate the presence of perchlorate at 4.48 mg/kg and HMX
at 0.43 mg/kg. These concentrations of perchlorate and HMX do not make the material
hazardous (the waste was deactivated), however, the disposal of potentially contaminated ash in
the on-site solid waste landfill is a concern. The Division is currently investigating perchlorate
9
contamination at the area and in groundwater. ATK's practice of disposing burn ground ash and
residue in the on-site landfill will be a part of this investigation.
R315-13-1 Land Disposal Restrictions - OK
Hazardous Waste Storage Permit
ATK appears to be in compliance with the currently applicable conditions of Modules I through
Module V and the associated Attachments of the Hazardous Waste Storage Permit.
Date
10
APPENDIX A
Pre-Inspection Checklist
Facility: ATK Launch Systems Inc.
Promontory Facility
EPAID#: UTD009081357
Address: ATK Launch Systems Inc.
Promontory Facility
P.O. Box 707
Brigham City, UT 84302-0707
Type of Inspection: Compliance Evaluation Inspection (CEI)
Date of Inspection: September 25 & 26, 2012
Team Leader: Jeff Vandel
Team Members: Hao Zhu
Pre-Inspection Conference
Date: TM.tCiZ Time: H-jO Q*A
Inspection Scope:
M-136 and M-225 Open Burning Grounds - inspect the site, condition of burn trays, operating record
for inspections
M-l 86 and M-705S Hazardous Waste Storage - inspect the site, condition of containers, sumps,
operating record for inspections
X-ray Photograph Sites - inspect one or more of these sites to be determined in the field
Machine Shop - inspect the site, waste management
Inspect main sources of reactive hazardous waste if able. Look for potential for reducing
"contaminated debris" that is sent to bum grounds
Inspect sources of rags, debris, flammable liquids and sludge that are generated from
"painting/coating" operations at the facility
T29B Hydrazine Treatment facility - inspect the site, look at records
Waste Analysis records for reactive hazardous wastes generated on and off-site. Also treatment
effectiveness records for burn ground ash and residue
Inspect the burn ground operating record for notation of clearing index, wind speed, etc. as required by
Condition IV.C.3.e.
Manifests - look at a number of manifests for wastes received and wastes shipped
Safety Equipment: PPE
Inspection Notification: {indicate the contact and the date and time of contact)
Facility: George Gooch. ATK Launch Systems - Promontory, August 29, 2012
Local Health Department: Clayne Shakespeare Bear River Health Dep't., September 20, 2012
Team Leader:
o
Supervisor:
4
ATK Launch Systems Inc. - Promontory
2012 RCRA Compliance Evaluation Inspection
General Information
1. Describe the primary activities that are currently being conducted at the Promontory
facility?
Production (GEM, D-5, other motors, flares or energetics?):
f |a U <s - ^-U U - /d) M( fi-fr^ y,j f'/c Ai T K "fU^L
Demilitarization (Minuteman?): , ... i r
t-^l1 tv\&L.Ln*JL jHt^ l>"e/V>4 WCVK V
is - -j i ^ v-** - ,
' 1 1 f ijo-YVK or 7h'rc(
2. What hazardous wastes does T^ritrkrri currently accept from off-site for treatment
(hazardous wastewater, waste propellant, etc.)? •
3. What are the main sources ofthe reactive hazardous waste that is burned at M-l 36
(look at Burn Ground records to determine what the main sources are - would like to
inspect these areas)?
S^S
4. What are the main sources of the hazardous waste that is burned at M-225?
5. What X-ray Photograph facilities are currently operating?
Cjc.^ -Ic c\t^;U,\ - prides 7/kt:V iAC-l Jt{VVCK4zd fo
6. Are the remains of hazardous wastes that are received from off-site and open-burned
at Promontory disposed of in the on-site, solid waste landfill? Are any of these
wastes managed separately due to the presence of listed constituents? (Show "cradle
to grave" documentation for a waste shipment received from off-site)
Un4-f;f o^^k. @LU~I^' %r,U wciAa'ji
7. The generation of D003 (reactive hazardous waste) that is treated at the burn grounds
does not appear to be shown in the 2011 Biennial Report. What was the quantity of
this waste stream that was generated for the reporting period?
8. Based on the 2011 Biennial Report, 21,077 pounds of "rags and debris" were
generated from "painting/coating" operations at the facility. What are these operations
(would like to inspect)? ^ ^ ^ ^ ^ 5LU{/
In addition, 9,025 pounds of "flammable liquids with sludge" were also generated
from "painting/coating" operations. Are these wastes generated from the same
activities as above? If not, where are they generated?
vie-I U^CN1
APPENDIX B
M-225(S-635/WORK AREA READINESS CHECKLIST
Inspections musFWcompleted at least once per calendar week when the area is not in use and within 24 hours of a storm event.
DAILY
ITEM S / N / U / (N/A)
SUN MON TUES WED THUR FRI SAT
-
COMMENTS / CORRECTIVE ACTIONS/DATE CORRECTED
MOTORS/CONTAINERS CLOSED, NO
SPILLS/ LEAKS, PROPERLY LABELED2 y
WASTE MATERIALS IN ASSIGNED PLACE
BURN TRAYS: HOLES, WATER LEVEL,
DETERIORATION2,3'"
ROADWAYS/OTHER SURFACES1 /
LOADING/UNLOADING AREAS1
OATE i
WEEKLY
ITEM S / N / U / (N/A) COMMENTS / CORRECTIVE ACTIONS DATE / INITIALS
FENCES AND SIGNS IN GOOD REPAIR
GATES, LOCKS, AND ROAD BARRICADES
EROSION
ITEM S / N / U / (N/A) COMMENTS / CORRECTIVE ACTIONS DATE / INITIALS
BUNKER: INTERIOR, GOOD CONDITION
TELEPHONE/RADIO OPERATIONAL
FIRE EXTINGUISHER PRESENT/FUNCTIONAL
MEDICAL BOX
ITEM
OFFS
S / N / U / (N/A)
* ASTE
COMMENTS / CORRECTIVE ACTIONS DATE / INITIALS
IN COMPLIANCE WITH NEW ARRIVAL/RAINFALL EVENT CHECKS
WASTE STREAM CONSISTENT W/MANIFEST & PROFILE
STORAGE LOCATION/NUMBER OF ITEMS
S SATISFACTORY NO CORRECTIVE ACTION REQUIRED
N NEEDS IMPROVEMENT PROMPT ATTENTION REQUIRED: NO STOP OF OPERATIONS AND/OR EQUIPMENT USAGE. COMMENTS REQUIRED
U UNSATISFACTORY IMMEDIATE CORRECTIVE ACTION: STOP OPERATIONS / USE OF EQUIPMENT UNTIL FIXED. COMMENTS REQUIRED
N/A NOT APPLICABLE EQUIPMENT WILL NOT BE USED THIS SHIFT
1 - Daily when in use (i.e. when loading or unloading operations occur at the facility).
2 - Inspect upon arrival, then each calendar week
3 - Inspect after each storm event. * A storm event is defined as more than one inch of precipitation in a one-hour period.
• Not required during inspection of S-633.
FORM FQA-0373 (REV 10-10)
AREA READINESS CHECKLIST
Inspections must be completed at least once per calendar week when the area is not in use and within 24 hours of a storm event.
DAILY
ITEM S / N / U / (N/A)
SUN MON TUES WED THUR FRI SAT COMMENTS / CORRECTIVE ACTIONS/DATE CORRECTED
MOTORS/CONTAINERS CLOSED, NO
SPILLS/ LEAKS, PROPERLY LABELED2
WASTE MATERIALS IN ASSIGNED PLACE 1/
BURN TRAYS: HOLES, WATER LEVEL,
DETERIORATION2'3''
ROADWAYS/OTHER SURFACES1
LOADING/UNLOADING AREAS1
YTE / INITIALS
If 1 m 0.
ITEM S/N/U / (N/A) COMMENTS / CORRECTIVE ACTIONS DATE / INITIALS
FENCES AND SIGNS IN GOOD REPAIR
GATES, LOCKS, AND ROAD BARRICADES
EROSION
1 ITEM S / N / U / (N/A) COMMENTS / CORRECTIVE ACTIONS DATE / INITIALS
BUNKER: INTERIOR, GOOD CONDITION
TELEPHONE/RADIO OPERATIONAL
FIRE EXTINGUISHER PRESENT/FUNCTIONAL
MEDICAL BOX
OFFS , ASTE
ITEM S / N / U / (N/A) COMMENTS / CORRECTIVE ACTIONS DATE / INITIALS
IN COMPLIANCE WITH NEW ARRIVAL/RAINFALL EVENT CHECKS
WASTE STREAM CONSISTENT W/MANIFEST & PROFILE
STORAGE LOCATION/NUMBER OF ITEMS
SATISFACTORY NO CORRECTIVE ACTION REQUIRED
NEEDS IMPROVEMENT PROMPT ATTENTION REQUIRED: NO STOP OF OPERATIONS AND/OR EQUIPMENT USAGE. COMMENTS REQUIRED
UNSATISFACTORY IMMEDIATE CORRECTIVE ACTION: STOP OPERATIONS / USE OF EQUIPMENT UNTIL FIXED. COMMENTS REQUIRED
N/A NOT APPLICABLE EQUIPMENT WILL NOT BE USED THIS SHIFT
1 - Daily when in use (i.e. when loading or unloading operations occur at the facility).
2 - Inspect upon arrival, then each calendar week
3 - Inspect after each storm event. * A storm event is defined as more than one inch of precipitation in a one-hour period.
• Not required during inspection of S-633.
FORM FQA-0373 (REV 10-10)
M-136/V-225^-63^WORK AREA READINESS CHECKLIST
InspectionsTnust Decompieted at least once per calendar week when the area is not in use and within 24 hours of a storm event.
ITEM S / N / U / (N/A)
SUN MON TUES WED THUR FRI SAT COMMENTS / CORRECTIVE ACTIONS/DATE CORRECTED
MOTORS/CONTAINERS CLOSED, NO
SPILLS/ LEAKS, PROPERLY LABELED2 y H
WASTE MATERIALS IN ASSIGNED PLACE \y
BURN TRAYS: HOLES, WATER LEVEL,
DETERIORATION2'3'" y \y
ROADWAYS/OTHER SURFACES1 y y y
LOADING/UNLOADING AREAS1 y
DATE / INITIALS fa ^ 5f alt i
WEEKLY
ITEM S IHI UI (N/A) COMMENTS / CORRECTIVE ACTIONS DATE / INITIALS
FENCES AND SIGNS IN GOOD REPAIR
GATES, LOCKS, AND ROAD BARRICADES
EROSION'
ITEM
j L»^f
S / N / U / (N/A) COMMENTS / CORRECTIVE ACTIONS DATE / INITIALS
BUNKER: INTERIOR, GOOD CONDITION
TELEPHONE/RADIO OPERATIONAL
FIRE EXTINGUISHER PRESENT/FUNCTIONAL
MEDICAL BOX
OFFS TE WASTE
ITEM S / N / U / (N/A) COMMENTS / CORRECTIVE ACTIONS DATE / INITIALS
IN COMPLIANCE WITH NEW ARRIVAL/RAINFALL EVENT CHECKS
WASTE STREAM CONSISTENT W/MANIFEST & PROFILE
STORAGE LOCATION/NUMBER OF ITEMS
SATISFACTORY NO CORRECTIVE ACTION REQUIRED
NEEDS IMPROVEMENT PROMPT ATTENTION REQUIRED: NO STOP OF OPERATIONS AND/OR EQUIPMENT USAGE. COMMENTS REQUIRED
UNSATISFACTORY IMMEDIATE CORRECTIVE ACTION: STOP OPERATIONS / USE OF EQUIPMENT UNTIL FIXED. COMMENTS REQUIRED
N/A NOT APPLICABLE EQUIPMENT WILL NOT BE USED THIS SHIFT
1 - Daily when in use (i.e. when loading or unloading operations occur at the facility).
2 - Inspect upon arrival, then each calendar week
3 - Inspect after each storm event. * A storm event is defined as more than one inch of precipitation in a one-hour period.
• Not required during inspection of S-633.
FORM FQA-0373 (REV 10-10)
M^l^/IVl-225/S^635;WORK AREA READINESS CHECKLIST
Inspections must be completed at least once per calendar week when the area is not in use and within 24 hours of a storm event.
DAILY
ITEM
_ MONTHLY
S / N / U / (N/A) COMMENTS / CORRECTIVE ACTIONS zzzzz DATE / INITIALS
BUNKER: INTERIOR, GOOD CONDITION
TELEPHONE/RADIO OPERATIONAL
FIRE EXTINGUISHER PRESENT/FUNCTIONAL
MEDICAL BOX
OFFS TE WASTE
ITEM S / N / U / (N/A) COMMENTS / CORRECTIVE ACTIONS DATE / INITIALS
IN COMPLIANCE WITH NEW ARRIVAL/RAINFALL EVENT CHECKS
WASTE STREAM CONSISTENT W/MANIFEST & PROFILE
STORAGE LOCATION/NUMBER OF ITEMS
SATISFACTORY NO CORRECTIVE ACTION REQUIRED
NEEDS IMPROVEMENT PROMPT ATTENTION REQUIRED: NO STOP OF OPERATIONS AND/OR EQUIPMENT USAGE. COMMENTS REQUIRED
UNSATISFACTORY IMMEDIATE CORRECTIVE ACTION: STOP OPERATIONS / USE OF EQUIPMENT UNTIL FIXED. COMMENTS REQUIRED
N/A NOT APPLICABLE EQUIPMENT WILL NOT BE USED THIS SHIFT
1 - Daily when in use (i.e. when loading or unloading operations occur at the facility).
2 - Inspect upon arrival, then each calendar week
3 - Inspect after each storm event. * A storm event is defined as more than one inch of precipitation in a one-hour period.
• Not required during inspection of S-633.
FORM FQA-0373 (REV 10-10)
M-136{M^25^S-633 WORK AREA READINESS CHECKLIST
Inspections must be completed at least once per calendar week when the area is not in use and within 24 hours of a storm event.
111 S/N/U/(N/A) jT k 1 ITEM SUN MON TUES WED THUR FRI SAT COMMENTS / CORRECTIVE ACTIONS/DATE CORRECTED
MOTORS/CONTAINERS CLOSED. NO
SPILLS/ LEAKS. PROPERLY LABELED2
WASTE MATERIALS IN ASSIGNED PLACE A/ft VIA s BURN TRAYS: HOLES, WATER LEVEL,
DETERIORATION2'3-' 9 5
ROADWAYS/OTHER SURFACES1
s 1
LOADING/UNLOADING AREAS
_ IK
ITEM \ S/N/U/(N/A)
FENCES AND SIGNS IN GOOD REPAIR
GATES, LOCKS, AND ROAD BARRICADES
EROSION-"
wmamm
ITEM
BUNKER: INTERIOR, GOOD CONDITION
TELEPHONE/RADIO OPERATIONAL
FIRE EXTINGUISHER PRESENT/FUNCTIONAL
MEDICAL BOX
_ OFFS
ITEM
IN COMPLIANCE WITH NEW ARRIVAL/RAINFALL EVENT CHECKS
WASTE STREAM CONSISTENT W/MANIFEST & PROFILE
STORAGE LOCATION/NUMBER OF ITEMS
S SATISFACTORY NO CORRECTIVE ACTION REQUIRED
N NEEDS IMPROVEMENT PROMPT ATTENTION REQUIRED: NO STOP OF OPERATIONS AND/OR EQUIPMENT USAGE. COMMENTS REQUIRED
U UNSATISFACTORY IMMEDIATE CORRECTIVE ACTION: STOP OPERATIONS / USE OF EQUIPMENT UNTIL FIXED. COMMENTS REQUIRED
N/A NOT APPLICABLE EQUIPMENT WILL NOT BE USED THIS SHIFT
1 - Daily when in use (i.e. when loading or unloading operations occur at the facility).
2 - Inspect upon arrival, then each calendar week
3 - Inspect after each storm event. * A storm event is defined as more than one inch of precipitation in a one-hour period.
• Not required during inspection of S-633.
FORM FQA-0373 (REV 10-10)
M-136/M-225/S-633 WORK AREA READINESS CHECKLIST
Inspections must be completed at least once per calendar week when the area is not in use and within 24 hours of a storm event.
„:•, :iv,.„:
: • : ITEM SUN
JL
MON
\(J S/N/U/(N/A) .j 13
TUES WED THUR FRI
JLtL
SAT COMMENTS / CORRECTIVE ACTIONS/DATE CORRECTED
MOTORS/CONTAINERS CLOSED, NO
SPILLS/LEAKS, PROPERLY LABELED2 tUk. "/A 6JJL A/ltr
WASTE MATERIALS IN ASSIGNED PLACE A/Ik IL BURN TRAYS: HOLES, WATER LEVEL,
DETERIORATION2-3 -• A//A
ROADWAYS/OTHER SURFACES1 AM WA AL
LOADING/UNLOADING AREAS1 A/ll\ dt A/tf
mm
/M
— 1 88 .Jin
ITEM SlU IV I (N/A) COMMENTS / CORRECTIVE ACTIONS DATE / INITIALS
FENCES AND SIGNS IN GOOD REPAIR
GATES, LOCKS, AND ROAD BARRICADES
EROSION' 2.011. 0
ITEM S / N / U / (N/A) COMMENTS / CORRECTIVE ACTIONS DATE / INITIALS
BUNKER: INTERIOR, GOOD CONDITION
TELEPHONE/RADIO OPERATIONAL
FIRE EXTINGUISHER PRESENT/FUNCTIONAL
3-
MEDICAL BOX
ITEM S / N / U / (N/A) COMMENTS / CORRECTIVE ACTIONS DATE /INITIALS
IN COMPLIANCE WITH NEW ARRIVAL/RAINFALL EVENT CHECKS
WASTE STREAM CONSISTENT W/MANIFEST & PROFILE
STORAGE LOCATION/NUMBER OF ITEMS hi [ A
S SATISFACTORY NO CORRECTIVE ACTION REQUIRED
N NEEDS IMPROVEMENT PROMPT ATTENTION REQUIRED: NO STOP OF OPERATIONS AND/OR EQUIPMENT USAGE. COMMENTS REQUIRED
U UNSATISFACTORY IMMEDIATE CORRECTIVE ACTION: STOP OPERATIONS / USE OF EQUIPMENT UNTIL FIXED. COMMENTS REQUIRED
N/A NOT APPLICABLE EQUIPMENT WILL NOT BE USED THIS SHIFT
1 - Daily when in use (i.e. when loading or unloading operations occur at the facility).
2 - Inspect upon arrival, then each calendar week
3 - Inspect after each storm event. * A storm event is defined as more than one inch of precipitation in a one-hour period.
• Not required during inspection of S-633.
FORM FQA-0373 (REV 10-10)
M-136/M-2257S-633 WORK AREA READINESS CHECKLIST
Inspections must be completed at least once per calendar week when the area is not in use and within 24 hours of a storm event.
ITEM SUN
JL
MON
|-| S/N/U/(N/A) ^
TUES WED THUR FRI SAT COMMENTS / CORRECTIVE ACTIONS/DATE CORRECTED
MOTORS/CONTAINERS CLOSED, NO
SPILLS/ LEAKS, PROPERLY LABELED2 iL At ft
WASTE MATERIALS IN ASSIGNED PLACE odJL Si IA MlL
BURN TRAYS: HOLES, WATER LEVEL,
DETERIORATION2'3'" rV)f\ WA
ROADWAYS/OTHER SURFACES1 LA AJ A
LOADING/UNLOADING AREAS1 V]f\ A/to H>)4;li 44
. :—
/INITIALS
\
" ':«:! IH 1 ITEM S IHI Ml (N/A) COMMENTS / CORRECTIVE ACTIONS DATE / INITIALS
FENCES AND SIGNS IN GOOD REPAIR
GATES, LOCKS, AND ROAD BARRICADES
EROSION
ITEM S/N/U/(N/A) COMMENTS / CORRECTIVE ACTIONS DATE / INITIALS
BUNKER: INTERIOR, GOOD CONDITION
TELEPHONE/RADIO OPERATIONAL
FIRE EXTINGUISHER PRESENT/FUNCTIONAL
MEDICAL BOX A//A
•'•: fyT-'OFES TE'WASTE : • • ;Vr j-'-zU. t-V
ITEM S / N / U / (N/A) COMMENTS / CORRECTIVE ACTIONS DATE /INITIALS
IN COMPLIANCE WITH NEW ARRIVAL/RAINFALL EVENT CHECKS sJ/A
WASTE STREAM CONSISTENT W/MANIFEST & PROFILE
STORAGE LOCATION/NUMBER OF ITEMS f>/A
S SATISFACTORY NO CORRECTIVE ACTION REQUIRED
N NEEDS IMPROVEMENT PROMPT ATTENTION REQUIRED: NO STOP OF OPERATIONS AND/OR EQUIPMENT USAGE. COMMENTS REQUIRED
U UNSATISFACTORY IMMEDIATE CORRECTIVE ACTION: STOP OPERATIONS / USE OF EQUIPMENT UNTIL FIXED. COMMENTS REQUIRED
N/A NOT APPLICABLE EQUIPMENT WILL NOT BE USED THIS SHIFT
1 - Daily when in use (i.e. when loading or unloading operations occur at the facility).
2 - Inspect upon arrival, then each calendar week
3 - Inspect after each storm event. * A storm event is defined as more than one inch of precipitation in a one-hour period.
• Not required during inspection of S-633.
FORM FQA-0373 (REV 10-10)
M-136/M-225/S-633 WORK AREA READINESS CHECKLIST
• -
Inspections must be completed at least once per calendar week when the area is not in use and within 24 hours of a storm event.
- -,^fe* . ' - DAILY - . -3MP>^V> -V -
_ OFF
ITEM S / N / U / (N/A) COMMENTS / CORRECTIVE ACTIONS DATE / INITIALS
IN COMPLIANCE WITH NEW ARRIVAL/RAINFALL EVENT CHECKS ft 31* 41l2 WASTE STREAM CONSISTENT W/MANIFEST & PROFILE
STORAGE LOCATION/NUMBER OF ITEMS
S SATISFACTORY NO CORRECTIVE ACTION REQUIRED
N NEEDS IMPROVEMENT PROMPT ATTENTION REQUIRED: NO STOP OF OPERATIONS AND/OR EQUIPMENT USAGE. COMMENTS REQUIRED
U UNSATISFACTORY IMMEDIATE CORRECTIVE ACTION: STOP OPERATIONS / USE OF EQUIPMENT UNTIL FIXED. COMMENTS REQUIRED
N/A NOT APPLICABLE EQUIPMENT WILL NOT BE USED THIS SHIFT
1 - Daily when in use (i.e. when loading or unloading operations occur at the facility).
2 - Inspect upon arrival, then each calendar week
3 - Inspect after each storm event. * A storm event is defined as more than one inch of precipitation in a one-hour period.
• Not required during inspection of S-633.
FORM FQA-0373 (REV 10-10)
APPENDIX C
Log Date Burn Grounds
—
Building# Station Profile
ri— •
Material Description Burn Date _—_|
Burn time Wind Speed
9/14/2012 M136 M101 13 PR22 Aluminized HTPB class 1.3 propellants - isocyanate cured, no nitramines
9/14/2012 M136 M015 13 PR68 Suspect group C Class 1.1D
9/14/2012 M136 M009 13 PR38 Suspect Group A Class 1.3
9/14/2012 M136 M087 13 PR44 Development Matl - R&D Lab use only. Suspect Group D Class 1.1D
9/14/2012 M136 M009 13 PR41 Suspect group C Class 1.1
9/14/2012 M136 M009 13 PR41 Suspect group C Class 1.1
9/14/2012 M136 1010 13 PR22 Aluminized HTPB class 1.3 propellants - isocyanate cured, no nitramines
9/14/2012 M136 M056 13 PR22 Aluminized HTPB class 1.3 propellants - isocyanate cured, no nitramines
9/14/2012 M136 1010 13 PR44 Russian DDT Pipes containing known and developmental materials
9/14/2012 M136 M323 13 PR41 Suspect group C Class 1.1
9/14/2012 M136 1010 13 PR44 Russian DDT Pipes containing known and developmental materials
9/14/2012 M136 1005 13 PR45 Developmental articles expected to be Group E Class 1.3
9/14/2012 M136 M053 13 PR44 Development Matl - R&D Lab use only. Suspect Group D Class 1.ID
9/14/2012 M136 M323 13 PR38 Suspect Group A Class 1.3
9/14/2012 M136 M053 13 PR30 NG based cross linked double base propellants with nitramines, D-5 or equiv.
9/14/2012 M136 M057 13 PR12 Aluminized HTPB with nitramines & isocyantes
9/14/2012 M136 M043 13 PR19 Aluminized HB, HC or HA polymer - propellant
9/12/2012 M136 M115 7 PR19 Minuteman stage 1 Propellant TP-H1011
9/14/2012 M136 M057 13 PR38 Suspect Group A Class 1.3
9/11/2012 M136 M115 7 PR23 AMRAAM Washout Material
9/11/2012 M136 M115 7 PR23 AMRAAM Washout Material
9/11/2012 M136 M115 10 PR23 AMRAAM Washout Material
9/12/2012 M136 M115 7 PR23 AMRAAM Washout Material
9/12/2012 M136 M115 7 PR23 AMRAAM Washout Material
9/12/2012 M136 M115 10 PR23 AMRAAM Washout Material
9/11/2012 M136 M016 10 PR13 LUU-19 and M278 B/B INFRARED ILLUMINATE
9/14/2012 M136 M043 13 PR76 IHPRPT Propellant,TP-N1043
9/11/2012 M136 1020 10 PR11 Boron Potassium Nitrate (BKN03)
9/14/2012 M136 M043 13 PR22 Aluminized HTPB class 1.3 propellants - isocyanate cured, no nitramines
9/14/2012 M136 M087 13 PR68 Suspect group C Class 1.ID
9/14/2012 M136 1010 13 PR48 Primary Explosives (no lead or water reactives)
9/14/2012 M136 M009 13 PR76 IHPRPT Propellant,TP-N1043
9/14/2012 M136 M323 13 PR39 Suspect group C Class 1.1C
9/14/2012 M136 M323 13 PR39 Suspect group C Class 1.1C
9/14/2012 M136 M323 13 PR38 Suspect Group A Class 1.3
9/14/2012 M136 M323 13 PR38 Suspect Group A Class 1.3
9/14/2012 M136 M087 13 PR30 NG based cross linked double base propellants with nitramines, D-5 or equiv.
9/14/2012 M136 M323 13 PR38 Suspect Group A Class 1.3
9/14/2012 M136 M009 13 PR38 Suspect Group A Class 1.3
9/11/2012 M136 M115 10 PR23 AMRAAM Washout Material
9/14/2012 M136 M057 13 PR22 Aluminized HTPB class 1.3 propellants - isocyanate cured, no nitramines
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
Log Oaje
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/12/2012
9/14/2012
9/11/2012
9/11/2012
9/11/2012
9/12/2012
9/12/2012
9/12/2012
9/11/2012
9/14/2012
9/11/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/11/2012
9/14/2012
Wind Direction
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
Temperature
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
Sky Conditions
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clearing Index Date Cleaned Non Haz Ash Derived From Ash Note Delay Delay Clean
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
Burn Grounds | Buildings | Station | Profile | Material Description
9/14/2012 M136 M057 13 PR19 Aluminized HB, HC or HA polymer - propellant
9/14/2012 M136 M057 13 PR76 IHPRPT Propellant,TP-N1043
9/14/2012 M136 M057 13 PR22 Aluminized HTPB class 1.3 propellants - isocyanate cured, no nitramines
9/11/2012 M136 M115 7 PR23 AMRAAM Washout Material
9/14/2012 M136 1005 13 PR19 Minuteman III Stage IPropellant TP-H1011
9/14/2012 M136 M009 13 PR44 Development Matl - R&D Lab use only. Suspect Group D Class 1.1D
9/14/2012 M136 M087 13 PR30 NG based cross linked double base propellants with nitramines, D-5 or equiv.
9/14/2012 M136 M053 13 PR33 Nitroguanidine (NQ)
9/14/2012 M136 M043 13 PR19 PropellantTP-H1148
9/12/2012 M136 M027 10 PR19 PropellantTP-H1148
9/14/2012 M136 M009 13 PR22 Aluminized HTPB class 1.3 propellants - isocyanate cured, no nitramines
9/12/2012 M136 M320 7 PR19 PropellantTP-H1148
9/12/2012 M136 M320 7 PR19 PropellantTP-H1148
9/11/2012 M136 M115 10 PR23 AMRAAM Washout Material
9/12/2012 M136 M11S 10 PR23 AMRAAM Washout Material
9/14/2012 M136 M323 13 PR38 Suspect Group A Class 1.3
9/14/2012 M136 M043 13 PR30 NG based cross linked double base propellants with nitramines, D-5 or equiv.
9/14/2012 M136 1005 13 PR07 Nitrate ester based lacquers (binder premix)
9/12/2012 M136 M115 10 PR23 AMRAAM Washout Material
9/14/2012 M136 1005 13 PR07 Nitrate ester based lacquers (binder premix)
9/14/2012 M136 1005 13 PR45 Developmental articles expected to be Group E Class 1.3
9/14/2012 M136 M053 13 PR44 Development Matl - R&D Lab use only. Suspect Group D Class 1.1D
9/14/2012 M136 M015 13 PR68 Suspect group C Class 1.1D
9/14/2012 M136 1005 13 PR45 Developmental articles expected to be Group E Class 1.3
9/14/2012 M136 1005 13 PR22 Aluminized HTPB class 1.3 propellants - isocyanate cured, no nitramines
9/14/2012 M136 T075 13 PR20 Detonation cord, linear shaped charge, or mild detonation fuse - lead sheathed
9/14/2012 M136 M323 13 PR38 Suspect Group A Class 1.3
9/11/2012 M136 M024 10 PR19 PropellantTP-H1148
9/14/2012 M136 1005 13 PR42 Suspect Group C Class 1.3
9/14/2012 M136 1005 13 PR45 Developmental materials expected to be Group E Class 1.3
9/14/2012 M136 M059 13 PR46 Reactive metal powders
9/13/2012 M136 M689 14 PR31 Minuteman II Stage 3 Rocket Motor
9/14/2012 M136 1005 13 PR68 Suspect group C Class 1.1D
9/14/2012 M136 M323 13 PR44 Development Matl - R&D Lab use only. Suspect Group D Class 1.1D
9/14/2012 M136 M053 13 PR72 R&D Lab Reactive Materials with Lead Content - Suspected Group 1.1 C, Class
9/14/2012 M136 S575 13 PR64 R&D Lab developed reactive with high metal content, Group E 1.3
9/14/2012 M136 M087 13 PR44 Development Matl - R&D Lab use only. Suspect Group D Class 1.ID
9/14/2012 M136 M043 13 PR19 Aluminized HB, HC or HA polymer - propellant
9/14/2012 M136 M057 13 PR12 Aluminized HTPB with nitramines & isocyantes
9/14/2012 M136 M057 13 PR19 Aluminized HB, HC or HA polymer - propellant
9/14/2012 M136 M009 13 PR22 Aluminized HTPB class 1.3 propellants - isocyanate cured, no nitramines
Burn Date
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
Burn time
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
Wind Speed
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/11/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/12/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/12/2012 SE 80 Clear 680
9/12/2012 SE 80 Clear 680
9/11/2012 SE 80 Clear 680
9/12/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/12/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/11/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/13/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
9/14/2012 SE 80 Clear 680
T 1
Date Cleaned
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012'
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
Non Haz Ash
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136IWT
M136 IWT
M136 IWT
M136 IWT
M136IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136IWT
M136 IWT
M136 IWT
M136 IWT
M136IWT
M136 IWT
M136IWT
M136 IWT
M136 IWT
M136IWT
M136 IWT
M136 IWT
M136 IWT
M136IWT
Derived From Ash
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
tlote Delay
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
Delay Clean
log Date
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/12/2012
9/14/2012
9/12/2012
9/12/2012
9/14/2012
9/14/2012
9/14/2012
9/12/2012
9/12/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/11/2012
9/14/2012
9/14/2012
9/14/2012
9/12/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/19/2012
9/18/2012
9/18/2012
9/18/2012
9/18/2012
9/19/2012
9/18/2012
Burn Grounds
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
M136
Building#
M087
M053
M053
M043
M627
M057
M705
M705
M323
M087
T075
M115
M115
M053
T024
M087
T075
T075
T075
M025
M043
M087
T024
M115
T024
1010
1010
M323
M323
T024
1010
1010
1010
T075
M115
M300
M016
M300
IVI 300
M115
T021
it.i(k): ?mi Material Dew ,
13 PR22 Castor 120 Propellant TP-H1246
13 PR44 Development Matl - R&D Lab use only. Suspect Group D Class 1.ID
13 PR44 Development Matl-R&D Lab use only. Suspect Group D Class 1.ID
13 PR13 LUU-19 and M278B/B INFRARED ILLUMINATE
10 PR19 Minuteman III Stage IPropellantTP-HlOll
13 PR38 Suspect Group A Class 1.3
7 PR74 M-705 T-1 Sump Sludge
10 PR19 AP contaminated filter socks
13 PR38 Suspect Group A Class 1.3
13 PR44 Development Matl - R&D Lab use only. Suspect Group D Class 1.1D
13 PR44 Development Matl - R&D Lab use only. Suspect Group D Class 1.1D
10 PR23 AMRAAM Washout Material
10 PR23 AMRAAM Washout Material
13 PR23 AMRAAM Washout Material
10 PR22 KEI Stage I igniter/Gem 40 igniter
13 PR76 IHPRPT Propellant,TP-N1043
13 PR20 Detonation Cord-HMX or RDX filled
13 PR68 Suspect group C Class 1.1D
13 PR20 Linear Shaped Charge with Aluminum or Copper Jacket
10 PR19 PropellantTP-H1148
13 PR76 IHPRPT Propellant,TP-N1043
13 PR76 IHPRPT Propellant,TP-N1043
13 PR22 Aluminized HTPB class 1.3 propellants - isocyanate cured, no nitramines
10 PR23 AMRAAM Washout Material
13 PR49 Primary Explosives (with lead, no water reactives)
13 PR30 M795 Impulse Cartridges
13 PR11 LUU and 2.75" Flare Igniters (full or partially assembled)
13 PR23 Low smoke class 1.3 propellants without nitramines
13 PR11 Igniter - Pyrotechnic
13 PR49 Primary Explosives (with lead, no water reactives)
13 PR44 Russian DDT Pipes containing known and developmental materials
13 PR44 Russian DDT Pipes containing known and developmental materials
13 PR49 Detonator, MK 59 MOD 0 PN 652220
13 PR30 M796 Impulse Cartridges
10 PR23 AMRAAM Washout Material
10 PR19 PropellantTP-H1148
10 PR13 LUU-19 and M278 B/B INFRARED ILLUMINATE
10 PR19 PropellantTP-H1148
10 PR19 PropellantTP-H1148
10 PR23 AMRAAM Washout Material
10 PR28 M257 or LUU2 Flaresffull or Partial)
Burn Date
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
Burn time
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
9:50
10:30
10:30
10:30
10:30
10:30
10:30
10:30
10:30
10:30
10:30
10:00
10:00
10:00
10:00
10:00
10:00
10:00
Wind Speed
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
5
5
5
5
5
5
5
Log Date
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/12/2012
9/14/2012
9/12/2012
9/12/2012
9/14/2012
9/14/2012
9/14/2012
9/12/2012
9/12/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/14/2012
9/11/2012
9/14/2012
9/14/2012
9/14/2012
9/12/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/19/2012
9/18/2012
9/18/2012
9/18/2012
9/18/2012
9/19/2012
9/18/2012
Wind Direction
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
Temperature
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
80
54
54
54
54
54
54
54
54
54
54
62
62
62
62
62
62
62
Sky Conditions
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Partly Cloudy
Partly Cloudy
Partly Cloudy
Partly Cloudy
Partly Cloudy
Partly Cloudy
Partly Cloudy
Partly Cloudy
Partly Cloudy
Partly Cloudy
Clear
Clear
Clear
Clear
Clear
Clear
Clear
~ "
Clearing Index
680
680
680
680
680
680
680
680
680
680
680
680
680
680
680
680
680
680
680
680
680
680
680
680
860
860
860
860
860
860
860
860
860
860
699
699
699
699
699
699
699
Date Cleaned
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/15/2012
9/17/2012
9/17/2012
9/17/2012
9/17/2012
9/17/2012
9/17/2012
9/17/2012
9/17/2012
9/17/2012
9/17/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
Non Haz Ash
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
Derived From Ash
None
None
None
None
None
None
Off-Site Disposal
Off-Site Disposal
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
Off-Site Disposal
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
Note Delay
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
FALSE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
Delay Clean
Bulk Propel
Bulk Propel
Bulk Propel
Bulk Propel
Bulk Propel
Bulk Propel
Bulk Propel
Bulk Propel
Bulk Propel
Bulk Propel
lant 13
lant 13
lant 13
lant 13
lant 13
lant 13
lant 13
lant 13
lant 13
lant 13
Hot/Smoldering 7,10
Hot/Smoldering 7,10
Hot/Smoldering 7,10
Hot/Smoldering 7,10
Hot/Smoldering 7,10
Hot/Smoldering 7,10
Hot/Smoldering 7,10
Log Date j Burn Grounds | Building** | Station | Profile | Material Description
9/15/2012 M136 M136 7 PR23 AMRAAM Washout Material
9/18/2012 M136 M016 10 PR13 LUU-19 and M278 B/B INFRARED ILLUMINATE
9/19/2012 M136 M115 10 PR23 AMRAAM Washout Material
9/19/2012 M136 M115 10 PR23 AMRAAM Washout Material
9/19/2012 M136 M627 10 PR19 Minuteman III Stage IPropellant TP-H1011
9/18/2012 M136 M300 10 PR19 PropellantTP-H1148
9/19/2012 M136 M115 10 PR23 AMRAAM Washout Material
9/21/2012 M136 1020 10 PR11 Boron Potassium Nitrate (BKN03)
9/19/2012 M136 M115 10 PR23 AMRAAM Washout Material
9/19/2012 M136 M115 10 PR23 AMRAAM Washout Material
9/19/2012 M136 M11S 10 PR23 AMRAAM Washout Material
9/19/2012 M136 M115 10 PR23 AMRAAM Washout Material
9/19/2012 M136 M115 10 PR23 AMRAAM Washout Material
9/18/2012 M136 M016 10 PR13 LUU-19 and M278 B/B INFRARED ILLUMINATE
9/18/2012 M136 M016 10 PR13 LUU-19 and M278 B/B INFRARED ILLUMINATE
9/19/2012 M136 M115 10 PR23 AMRAAM Washout Material
9/18/2012 M136 M300 10 PR19 PropellantTP-H1148
9/19/2012 M136 M115 10 PR23 AMRAAM Washout Material
9/19/2012 M136 M027 10 PR19 PropellantTP-H1148
9/21/2012 M136 M627 10 PR19 Minuteman III Stage IPropellant TP-H1011
9/19/2012 M136 M627 10 PR19 Minuteman III Stage IPropellant TP-H1011
9/19/2012 M136 1020 10 PR11 Boron Potassium Nitrate (BKN03)
9/19/2012 M136 1020 10 PR11 Boron Potassium Nitrate (BKN03)
9/19/2012 M136 M115 10 PR19 Minuteman stage 1 Propellant TP-H1011
9/21/2012 M136 M627 10 PR19 Minuteman III Stage IPropellant TP-H1011
9/19/2012 M136 M115 10 PR19 Minuteman stage 1 Propellant TP-H1011
9/21/2012 M136 M115 10 PR19 Minuteman stage 1 Propellant TP-H1011
9/21/2012 M136 M115 10 PR19 Minuteman stage 1 Propellant TP-H1011
9/21/2012 M136 M325 10 PR19 PropellantTP-H1148
9/15/2012 M136 M136 7 PR23 AMRAAM Washout Material
9/19/2012 M136 M027 10 PR19 PropellantTP-H1148
9/21/2012 M136 M016 10 PR13 LUU-19 and M278 B/B INFRARED ILLUMINATE
9/21/2012 M136 M115 10 PR19 Minuteman stage 1 Propellant TP-H1011
9/15/2012 M136 M136 7 PR23 AMRAAM Washout Material
9/21/2012 M136 M115 10 PR19 Minuteman stage 1 Propellant TP-H1011
9/19/2012 M136 M115 10 PR23 AMRAAM Washout Material
9/21/2012 M136 M115 10 PR19 Minuteman stage 1 Propellant TP-H1011
9/21/2012 M136 M115 10 PR19 Minuteman stage 1 Propellant TP-H1011
9/21/2012 M136 M016 10 PR13 LUU-19 and M278 B/B INFRARED ILLUMINATE
9/21/2012 M136 M048 10 PR17 Aircmm Flare/Decoy Propellant TP-H1255
9/21/2012 M136 M115 10 PR19 Minuteman stage 1 Propellant TP-H1011
Burn Date
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
9/22/2012
Burn time
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
10:00
Wind Speed
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
Log Date
9/15/2012
9/18/2012
9/19/2012
9/19/2012
9/19/2012
9/18/2012
9/19/2012
9/21/2012
9/19/2012
9/19/2012
9/19/2012
9/19/2012
9/19/2012
9/18/2012
9/18/2012
9/19/2012
9/18/2012
9/19/2012
9/19/2012
9/21/2012
9/19/2012
9/19/2012
9/19/2012
9/19/2012
9/21/2012
9/19/2012
9/21/2012
9/21/2012
9/21/2012
9/15/2012
9/19/2012
9/21/2012
9/21/2012
9/15/2012
9/21/2012
9/19/2012
9/21/2012
9/21/2012
9/21/2012
9/21/2012
9/21/2012
Wind Directiof|i
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
SE
Temperature
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
62
Sky Conditions
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clear
Clearing Index
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
699
Date Cleaned
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
9/24/2012
Non Haz Ash
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
M136 IWT
Derived From Ash
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
None
Note Delay
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
TRUE
Delay Clean
Hot/Smolderi
Hot/Smolderi
Hot/Smolderi
Hot/Smolderi
Hot/Smolderi
Hot/Smolderi
Hot/Smolder
Hot/Smolderi
Hot/Smolder
Hot/Smolderi
Hot/Smolder
Hot/Smolder
Hot/Smolder
Hot/Smolder
Hot/Smolderi
Hot/Smolder
Hot/Smolderi
Hot/Smolderi
Hot/Smolderi
Hot/Smolderi
Hot/Smolder
Hot/Smolderi
Hot/Smolderi
Hot/Smolderi
Hot/Smolderi
Hot/Smolderi
Hot/Smolder
Hot/Smolderi
Hot/Smolderi
Hot/Smolderi
Hot/Smolderi
Hot/Smolderi
Hot/Smolderi
Hot/Smolder
Hot/Smolder
Hot/Smolder
Hot/Smolderi
Hot/Smolder
Hot/Smolder
Hot/Smolderi
Hot/Smolder
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
ng 7,10
Log Date
9/21/2012
9/24/2012
9/24/2012
Burn Grounds I Building# Station Profile Material Description
M136 M115 10 PR19 Minuteman stage 1 Propellant TP-H1011
M136 AT 14 PR30 "300 pound" motors cast with double base propellant
M136 AT 14 PR30 "300 pound" motors cast with double base propellant
Burn Date j Burn time j Wind Sf
9/22/2012 10:00 5
9/24/2012 16:00 0
9/24/2012 16:00 0
Log Date | Wind Direction | Temperature | Sky Conditions | Clearing Index | Date Cleaned Non Haz Ash | Derived From Ash [ Note Delay j Delay Clean
9/21/2012 SE 62 Clear 699 9/24/2012 M136 IWT None TRUE Hot/Smoldering 7,10
9/24/2012 E 66 Partly Cloudy 780 9/25/2012 M136 IWT None FALSE
9/24/2012 E 66 Partly Cloudy 780 9/25/2012 M136 IWT None FALSE
APPENDIX D
1203017
ENVIRONMENTAL LAB WORK REQUEST
TO ATK ENVIRONMENTAL LABORATORY LWRNo.E J3 33S5'
Login No.
FROM:
Randy D. Fullmer
EXTENSION:
5277
COST CENTER:
6290
WORK ORDER:
988P/LS333
DATE:-
ORGANIZATION:
ENVIRONMENTAL OPERATION
MAIL STOP: REPORT RESULTS TO:
301B Randy D. Fullmer
SAMPLE
SAMPLE INFORMATION
DATE TYPE LOCATION TIME TEST REMARKS
X M136 013D NG, HMX, RDX, AP Annual Samples
IZ. X M705 07 to Method 8330 Per / Hazardous
C104-Method 314.0 Waste Part B
Permit
Burn Ash
TH90119
Filter Cake
TH901FC
CHAIN OF CUSTODY
RELINQUISHED BY DATE TIME RECEIVED BY DATE TIME
0-!00()
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED SIONATURE
ATK Space Systems Group
Environmental Laboratory
Client Name
Ca/er (U^W) fluU'^~^
j/Hand delivered, no cooler Hand delivered, sample(s) taken out at rece
Sample Receipt Checklist
SDG No.
Carrier Number:,
receiving counter
W9F Initials
Cooler Information:
Cooler Number/ID:
Condition of Shipping Containor:
Cooler Sealed (taped):
Custody Seals Present
Coolant
State of Coolant,
Thermometer ID:
Packing Description.
Good
Yes
Yes
Intact
Ice
Frozen
Reading'.
Fair
No
No
Broken
Blue Ice ytfone
Partially Frozen
5 "C CF:
4X01 Applicable
•^Not Applicable
•rtot Applicable
Damaged (explain).
Seal Number.
Other-
Melted
Corrected Temp: ^ Temp Blank Included. Yes
Chain-Of-Custody Information:
COC Present:
COC Number(s):_
COC signed (relinquished and received):
COC or LWI agrees with sample labels:
Yes
,Yes
Yes
• iNo
•No
•No
Other.
:Not Applicable
: Not Applicable
Sample Information:
Samples included in cooler:
Custody Seals Present:
Sample containers intact:
Samples in proper containers:
Sufficient sample volume:
All samples received in hold time:
Water - VOA's have zero headspace:
1 iPre-preserved with HCl:
Notes:
ilYes
1 ilntact
Ore's
flYes/
ijfes
Other
Seal Numbers) _
Notes:
1IBroken
I INo
I INo
1 INo
ilNo
IlYes
l IPre-preserved with NajSjOy
:iNo WlStAc Applicable
I iNon-Preserved:
Water - pH acceptable upon receipt: 1 lYes1 lAdjusted (see comments below) J^jNot Applicable
HNOj = H2S04 = NaOH = ZnAC /NaOH = HCL =
Water - pH adjusted- (mfg. & Lot No.)
HNOj HjSO,.
Na2S0203 Other _
Notes:
NaOH ZnAC HCl
SOP-102 l-orm A
Data Reporting Qualifiers
U Indicates that the analyte concentration is less than the MDL.
B This flag is used when an analyte is found in the blank as well as the sample.
Indicates an extimated value. This flag is used either when estimating a concentration
for tentatively identified compounds or when the data indicated the presence of a
compound that meets the identification criteria but the result is less than the
EQL (e.g. 3 J with an EQL of 10).
MDL Method Detection Limit: The minimum concentration of a substance that can be
confidently measured and reported. The laboratory has demonstrated that the
MDL can be achieved in a laboratory reagent blank, but does not guarantee it
can be achieved in all sample
matrices.
EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For
many analytes the EQL is selected as the value of the lowest standard in the
calibration curve.
Dilution Dilution Factor: The prepared sample was diluted by this factor because the
Factor sample was too concentrated or due to other interferences in the sample
matrix.
Any dilution factor causes a corresponding increase in the MDL and EQL.
Page 4 of 4
Printed: 05/01/12 07:54
Listing of Results by Sample
Sample Delivery Group: 1203017
Client Sample ID: B4322 - TH90119 - Burn Ash (M136)
Sample Description: ATK-DLV - Annual Waste Characterization - Burn Ash & Filter Cake
Laboratory Sample ID: 1203017-01
Date Sampled: 03/16/12 07:30
CAS Number
Test Method:
014797-73-0
fest Method:
Test Method:
2691-41-0
121-82-4
55-63-0
Test Parameter
EPA 314.0
PERCHLORATE
SW-846,8330A
DATE COMPLETED
Result Units
Perchlorate - lon Chromatography
4.48 mg/kg
Explosives Extraction
03/26/2012
SW-846,8330A Mod (Solids) Explosives Analysis
HMX
RDX
NITROGLYCERIN
0.43 mg/kg
U mg/kg
U mg/kg
MDL
0.1
0.04
0.1
0.06
Dilution
EQL Factor Analyst Test Date
0.4 10
0.2 1
0.2 1
0.2 1
JMM
KMS
04/03/12
03/26/12
KMS 03/27/12
KMS 03/27/12
KMS 03/27/12
99-08-1 3-NITROTOLUENE 15.6 % KMS 03/27/12
Client Sample ID: B4323 - TH901 FC - Filter Cake (M705)
Sample Description: ATK-DLV - Annual Waste Characterization - Burn Ash & Filter Cake
Laboratory Sample ID: 1203017-02
Date Sampled: 03/16/12 07:10
CAS Number
: Test Method:
014797-73-0
Test Method:
2691-41-0
121-82-4
55-63-0
Test Parameter
EPA 314.0
PERCHLORATE
Result Units
Test Method: SW-846,8330A
DATE COMPLETED
Perchlorate - lon Chromatography
U mg/kg
Explosives Extraction
03/26/2012
SW-846,8330A Hod (Solids) Explosives Analysis
HMX
RDX
NITROGLYCERIN
8.36 mg/kg
U mg/kg
U mg/kg
MDL
0.1
0.04
0.1
0.06
Dilution
EQL Factor Analyst Test Date
0.4
0.2
0.2
0.2
10 JMM
KMS
KMS
KMS
KMS
04/03/12
03/26/12
03/27/12
03/27/12
03/27/12
99-08-1 3-NITROTOLUENE 131 % KMS 03/27/12
Page 3 of 4
Printed: 05/01/12 07:54
Sample Delivery Group: 1203017
Sample No. Client No.
Test Requested Sample Description
Received Collect Date/Time
Matrix
1203017-01 B4322 - TH90119 - Burn Ash (M136) 03/20/12 3/16/2012 07:30:00
EPA 314.0
SW-846, 8330A
SW-846, 8330A Mod (Solids)
Perchlorate - lon Chromatography
Explosives Extraction
Explosives Analysis
Waste, Solid
Waste, Solid
Waste, Solid
1203017-02 B4323 - TH901FC - Filter Cake (M705) 03/20/12 3/16/2012 07:10:00
EPA 314.0
SW-846, 8330A
SW-846, 8330A Mod (Solids)
Perchlorate - lon Chromatography
Explosives Extraction
Explosives Analysis
Waste, Solid
Waste, Solid
Waste, Solid
Certified By: 05/01/2012
W. Scott Fraser, Quality Assurance Officer Date
This certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation
Program (NELAP) unless otherwise annotated:
Page 2 of 4
Printed: 05/01/12 07.54
988P LS333
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Requested
Tuesday, May 01, 2012
TESTED FOR: ATK: DLV
Environmental Monitoring
Thiokol Corp, UT 84322
ANALYZED BY: ATK Launch Systems
Analytical Chemistry Laboratory
P.O. Box 707, M/S 245
Brigham City, UT 84302-0707
435-863-3732
435-863-8080
Contact Name: Randy Fullmer
Project:
Sample Delivery Group:
Off Plant Disposal Tests - DLV
1203017
Page 1 of 4
Printed: 05/01/12 07:54
1006004
ENVIRONMENTAL LAB WORK REQUEST
TO ATK LAUNCH SYSTEMS ENVIRONMENTAL LABORATORY LWR No. E13162
Login No.
FROM:
BLAIR PALMER
EXTENSION:
2430
COST CENTER:
8200
Project &Tuk #:
988P/LS333
DATE:
27 May 2010
ORGANIZATION:
ENVIRONMENTAL SERVICES
MAIL STOP: REPORT RESULTS TO:
301 HELEN RAVSTEN
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS
..RSRM
Washout
Ash
Residue
26Mayl0 X M-136 12:45 CIO.
CHAIN OF CUSTODY
RELINQUISHES BY DATE TIME RECEIVED BY DATE TIME
°1'IQ
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED SIGNATURE
ATK Launch Systems
Environmental Laboratory
Sample Receipt Checklist
Client Name: A TK LAt^cit €£f C^UfS „ SDG No.
Carrier:
• Hand delivered, no cooler
Carrier Number
• Hand delivered, sample(s) taken out at receiving counter
Cooler Information:
Cooler Number/ID:
Condition of Shipping Container:
Cooler Sealed (taped):
Custody Seals Present:
Coolant:
State of Coolant:
j^Sood
DYes
•Yes
• Intact
• Ice
frozen
•Fair
.^Broken
JS&lue Ice DNone
•Partially Frozen
CF:
•Not Applicable
•Not Applicable
•Not Applicable
•Damaged (explain).
Seal Number.
Other:
Thermometer ID: Reading: i o °C
Packing Description:
•Melted
Corrected Temp:. Temp Blank Included: ClYes DNo
Chaln-Of-Custody Information:
COC Present: / ^ , ~
COC Numberts): /3 /fr
COC signed (relinquished and received):
COC or LWI agrees with sample labels:
jJVes
"pf/es
jrfes
Notes:
DNo
• No
• No
Other
•Not Applicable
•Not Applicable
Sample Infonnation:
Samples included in cooler:
Custody Seals Present:
Sample containers Intact:
Samples In proper containers:
Sufficient sample volume:
All samples received in hold time:
•Yes
•Intact
^es
jsfres
jtfYes
Xre*
Water - VOA's have zero headspace:
•Pre-preserved with HCl:
Notes:
•Broken
• No
•No
•No
DNo
•Yes
Other
Seal Numbers).
Notes:
DNo
• Pre-preserved with
«No1
Nar&Oj:
lot Applicable
•Non-Preserved:
Water - pH acceptable upon receipt: DYes OAdjusted (see comments below) Oflot Applicable
HNO, = H2S04 = NaOH = ZnAC /NaOH • HCL>
Water - pH adjusted: (mfg. & Lot No.)
HNOj H,SO»
Na2S0203 Other.
Notes:
NaOH ZnAC _HCI_
SOP-102 Form A
988P LS333
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Requested
Friday, June 11, 2010
TESTED FOR: ATK: DLV
Environmental Monitoring
Thiokol Corp, UT 84322
ANALYZED BY: ATK Launch Systems
Analytical Chemistry Laboratory
P.O. Box 707, M/S 245
Brigham City, UT 84302-0707
435-863-3732
435-863-8080
Contact Name: Blair Palmer
Project:
Sample Delivery Group:
Environmental Testing - DLV
1006004
Page 1 of 4
Printed: 06/11/10 10:56
Sample Delivery Group: 1006004
Sample No. Client No. Received Collect Date/Time
Test Requested Sample Description Matrix
1006004-01 RSRM Washout Ash Residue-M-136 06/01/10 5/26/2010 12:45:27
EPA 314.0 Perchlorate - lon Chromatography Waste, Solid
MM* — w~ ^JJ^ 06/11/2010
W. Scott Fraser, Quality Assurance Officer Date
This certifies that the following data meets the requirements ofthe National Environmental Laboratory Accreditation
Program (NELAP) unless otherwise annotated:
Page 2 of 4
Printed: 06/11/10 10:56
Listing of Results by Sample
Sample Delivery Group: 1006004
Client Sample ID: RSRM Washout Ash Residue - M-136
Sample Description: ATK-DLV - RSRM Washout Ash Residue
Laboratory Sample ID: 1006004-01
Date Sampled: 05/26/10 12:45
CAS Number Test Parameter
014797-73-0 PERCHLORATE
Dilution
Result Units MDL EQL Factor Analyst Test Date
Perchlorate - lon Chromatography
< EQL mg/kg 8 200 JMM 06/10/10
Page 3 of 4
Printed: 06/11/10 10:56
Data Reporting Qualifiers
u
B
J
MDL
EQL
Dilution
Factor
Indicates that the analyte concentration is less than the MDL.
This flag is used when an analyte is found in the blank as well as the sample.
Indicates an extimated value. This flag is used either when estimating a concentration
for tentatively identified compounds or when the data indicated the presence of a
compound that meets the identification criteria but the result is less than the
EQL (e.g. 3 J with an EQL of 10).
Method Detection Limit: The minimum concentration of a substance that can be
confidently measured and reported. The laboratory has demonstrated that the
MDL can be achieved in a laboratory reagent blank, but does not guarantee it
can be achieved in all sample matrices.
Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For
many analytes the EQL is selected as the value of the lowest standard in the
calibration curve.
Dilution Factor: The prepared sample was diluted by this factor because the
sample was too concentrated or due to other interferences in the sample matrix.
Any dilution factor causes a corresponding increase in the MDL and EQL.
Page 4 of 4
Printed- 06/11/101056
f
ENVIRONMENTAL LAB WORK REQUEST
THIOKOL ENVIRONMENTAL LABORATORY LWRNo. E12264
Login No.
ORGANIZATION
2>ol
COST CENTER WORK ORDER
7-<7-03
REPORT RESULTS TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS
T^r HLSSL. OSroo
7-J-vi 1/
CHAIN OF CUSTODY
RELINQUISHED BY DATE TIME RECEIVED BY DATE TIME
7 -?-o3
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED
CERTIFICATE OF ANALYSIS
Listing of sample Information and Testing Requested
Wednesday, July 23,2003
TESTED FOR ATK Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp, UT 84322
Gene Curtis
Project: Misc. Environmental Testing
Login Number L6792
Lab No Client Number
Test Requested Description
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-3732
800-863-8080
Received CollectDate/Time
Matrix
I L6792-1 TRAY 41.52.37 /M-136 07/09/03 06724/03 08:00
EPA 314.0
[ Perchlorate • lon Chromatography Waste, Sol
L6792-2 TRAY 54. 32. 29. 33 07/09/03 06/24/03 08:00
EPA 314.0 Waste, Sol Perchlorate - lon Chromatography
Certified
This certifies that the following samples were analyzed using good laboratory practices to show the following results:
QC Coordinator Date
Page 1 of 3
Listing of Results by Sample
I Sample ID: TRAY 41,52,37 (M-136 LablD:L6792-1 Collect Date: 06724/03 08:00
Test Parameter
PERCHLORATE
Dll.
Result Units MDL EQL Factor Method
U mg/kg .1 .4 10 EPA 314.0
Analyst Test Pate
CWS 07/17/0319:05
Collect Date: 06/24/03 08:00 | | Sample ID: TRAY 54, 32, 29, 33 Lab ID:L6792-2
Test Parameter
PERCHLORATE
Dll.
Result Units MDL EQL Factor Method
U mg/kg .1 .4 10 EPA 314.0
Analyst Test Pate
CWS 07/17/0319:20
Page 2of 3
Data Reporting Qualifiers
u
MDL
EQL
Dil. Factor
Indicates compound was analyzed for and was not detected, or the compound was detected
but was below the EQL (Estimated Quantification Limit). The EQL and the RPL (Reporting
Limit) are used in the same manner for this report.
Method Detection Limit: The minimum concentration of a substance that can be confidently
measured and reported. The laboratory has demonstrated that the MDL can be achieved in a
laboratory reagent blank, but does not guarentee it can be achieved in all sample matrices.
The MDL is approximately three times the signal noise level.
Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many
analytes the EQL is selected as the value of the lowest standard in the calibration curve.
Dilution Factor: The prepared smple was diluted by this factor because the sample was too
concentrated or due to other interferences in the sample matrix. Any dilution factor causes
an appropriate increase in the MDL and EQL.
Page 3of3
ENVIRONMENTAL LAB WORK REQUEST
THIOKOL ENVIRONMENTAL LABORATORY LWRNo. E12227
Login No.
(OM. COST CENTER WORKORDER
'01 7-03
ORGANIZATION
ML
REPORT RESULTS TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS
07YO
67 rt
12.
CHAIN OF CUSTODY
RELINQUISHED BY DATE TIME RECEIVED BY DATE TIME
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED
CERTIFICATE OF ANALYSIS
Listing of sample Information and Testing Requested
Monday, May 19, 2003
TESTED FOR ATK Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp, UT 84322
Gene Curtis
Project: Misc. Environmental Testing
Login Number L6565
Lab No Client Number
Test Requested Description
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-3732
800-863-8080
Received CollectDate/Time
Matrix
L6565-1 01 - TRAY # 54 05/07/03 05/07/03 07:40
EPA 314.0 Perchlorate - lon Chromatography Waste, Sol
L6565-2 02 - TRAY # 56 05/07/03 05/07/03 07:43
EPA 314.0 Perchlorate - lon Chromatography
Certified
Waste, Sol
QC Coordinator T \ Date
This certifies that the following samples were analyzed using good laboratory practices to show the following results:
Page 1 of 3
Listing of Results by Sample
Sample ID: 01 - TRAY # 54 Lab ID: L6565-1 Collect Date: 05/07/03 07:40 |
Dll.
Test Parameter Result Units MDL EQL Factor Method Analyst Test Date
PERCHLORATE U mg/kg .1 .4 10 EPA 314.0 CWS 05/15/03 08:30
| Sample ID: 02 - TRAY # 56 Lab ID: L6565-2 Collect Date: 05/07/03 07:43 ]
Dil.
Test Parameter Result Units MDL EQL Factor Method Analyst Test Date
PERCHLORATE U mg/kg .1 .4 10 EPA 314.0 CWS 05/15/03 08:43
Page 2of 3
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected
but was below the EQL (Estimated Quantification Limit). The EQL and the RPL (Reporting
Limit) are used in the same manner for this report.
MDL Method Detection Limit: The minimum concentration of a substance that can be confidently
measured and reported. The laboratory has demonstrated that the MDL can be achieved in a
laboratory reagent blank, but does not guarentee it can be achieved in all sample matrices.
The MDL is approximately three times the signal noise level.
EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many
analytes the EQL is selected as the value of the lowest standard in the calibration curve.
Dil. Factor Dilution Factor: The prepared smple was diluted by this factor because the sample was too
concentrated or due to other interferences in the sample matrix. Any dilution factor causes
an appropriate increase in the MDL and EQL.
Page 3of3