DSHW-2011-003529 - 0901a06880208beb

February 28,2011
8200-FY11-071 HAND DELIVERED
Mr. Scott T. Anderson, Executive Secretary 2 8 2011
State of Utah Department of Environmental Quality
Division of Solid and Hazardous Waste gouo &^HAZARDOUS°WASTE
195N.1950W. 7/)// r)nc^A^
P.O. Box 144880 ' • ^^^^
Salt Lake City, Utah 84114-4880
Subject: Submittal of M-136 LTTA Post-closure Permit Semi-Annual Report
Promontory Facility, EPA ID #UTD009081357
Dear Mr. Anderson,
Enclosed is the submittal ofthe M-136 Liquid Thermal Treatment Area (LTTA) Post-Closure Permit
Semi-Annual Report. The post-closure permit for the M-136 LTA, Sections IV.E.2 and IV.E.3
require semi-annual reports detailing results of sample analyses including concentration of
hazardous constituents and a summary of QA/QC data, measurements of static water levels, and total
well depths of wells completed in unconsolidated materials.
If you have any questions regarding this information, please contact Allen Lee at 801-251-5688.
I certify under penalty of law that this document and all attachments were prepared under my
direction or supervision in accordance with a system designed to assure that qualified personnel
properly gather and evaluate the information submitted. Based on my inquiry ofthe person or
persons who manage the system, or those persons directly responsible for gathering the information,
the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the
possibility of fine and imprisonment for knowing violations.
Sincerely,
David P. Gosen, P.E., Director
Envirormiental Services
HAND DELIVERED
FEB 2 8 2011
UTAH DIVISION OF
SOLID & HAZARDOUS VVASTE
M-136 LTTA ^^11.005^4-
POST-CLOSURE PERMIT
2010 FALL SEMI-ANNUAL REPORT
ATK
ATK LAUNCH SYSTEMS Inc.
Promontory Facility
Box Elder County, Utah
EPA ID# UTD009081357
Febmary 2011
Preface
This IS a semi-annual report submitted to the Utah Division of Solid and
Hazardous Waste to comply with requirements of the M-136 LTTA Post-Closure
Permit It contains data and information compiled dunng the second half of 2011
concerning the M-136 Burning Area and LTTA groundwater This report is meant
to be read in conjunction with the previously submitted intenm and semiannual
reports, and Post-Closure Permit Application
This report is organized into one volume containing text, figures, and appendices
A, B,C and D
III P a g e
Table of Contents
Preface ii
Table of Contents in
Plates, Tables, and Appendicies iv
1 0 Ground Water Sampling 1
1 1 Introduction 1
1 2 Analytical Results of Ground Water Sampling 1
2 0 Static Water Levels and Well Depths 3
3 0 Hazardous Plume Charactenstics 14
31 Trichloroethene 14
3 2 1,1,1-Tnchloroethane 14
3 3 1,1-Dichloroethene 15
3 4 1,1-Dichloroethane 16
3 5 1,1 Dichloroethane 16
3 6 Perchlorate 16
3 7 Cis-1,2-Dichloroethane 16
4 0 Corrective Action Program Effectiveness 18
III I P a g e
Plates, Tables, and Appendices
Plates are located in Appendix D
PLATE 1
PLATE 1
PLATE 2
PLATE 3
PLATE 4
PLATE 5
PLATE 6
PLATE?
Potentiometric Map and Flow Lines (Sheet 1 of 2)
Potentiometric Map and Flow Lines (Sheet 2 of 2)
1,1-Dichloroethane (DCA) Isoconcentration Map
1,1-Dichloroethene (DCE) Isoconcentration Map
1,1,1-Tnchloroethane (TCA) Isoconcentration Map
Tnchloroethene (TCE) Isoconcentration Map
Perchlorate Isoconcentration Map
Chloroform Isoconcentration Map
TABLE 1 Fall 2010 Water Levels 3
TABLE 2 Depths of Wells Completed in Unconsolidated Material (Fall 08) 8
TABLE 3 Summary of Representative Hydraulic Conductivities 9
Appendicies are located following text
APPENDIX A
APPENDIX B
APPENDIX C
APPENDIX D
Analytical Data - Volatiies
Analytical Data - Perchlorate, HMX, and RDX
Raw Analytical Data
Plates
IV I P a g e
Promontory Post-Closure Permit
Fall 2010 Semi-Annual Report
Section 1 0
Ground Water Sampling
1 1 INTRODUCTION
In September 1992, Thiokol Corporation received a post-closure permit for the
M-136 Liquid Thennal Treatment Area (LTTA) Sections V F 3 and V F 4 of the
permit requires submittal of a semiannual report detailing results of sample
analyses including concentration of hazardous constituents and a summary of
QA/QC data, measurements of static water levels, and total well depth estimates
The Fall 2010 sampling effort consisted of nineteen Wells and four Spnngs The
nineteen wells sampled were selected from previous compliance wells and wells
near penmeter sources The selected wells and spnngs help in the ongoing
evaluation of plume boundaries at the facility
Wells and Spnngs sampled were C-6, C-7, C-8, D-5, D-6, E-2, E-5, E-6, F-4, G-
3, H-6, H-8, J-2, J-5, J-6, J-7, J-8, LF-2, LF-3, Fish Spnng, Horse Spnng, Pipe
Spnng and Shotgun Spnng All samples were analyzed for VOCs and
Perchlorate No sample was collected from C-6 due to problems with the bladder
pump QA/QC samples were collected from Wells C-7 and C-8
1 2 ANALYTICAL RESULTS OF GROUND WATER SAMPLING
A complete summary of the ground water analytical results, by constituent, are
located in Appendices A, B, and C These Appendices list individual parameters
for each well by constituents, sample number, well number, replicate, aliquot,
date, results, and Estimated Quantification Limits or detection limits Also
included in the summary are the data for the field blanks Appendix C contains
the laboratory reports containing the analytical data and QA/QC for ground water
samples
Samples were collected, preserved, and transported according to the approved
Sampling Plan of the Permit Attachment 4 Samples were analyzed according to
USEPA approved methods All major peaks greater than 25% of the peak height
of the closest internal standard are identified to the extent analytically possible,
using the most current NBS library Two sets of field blanks, Tnp Blanks and
replicates were collected, which represent at a minimum, 10% of the total
samples The laboratory provided method blanks, spikes, and duplicates, and
results are located in Appendix C Qualifiers as defined by the EPA Contract Lab
Program were used where applicable (organic analyses)
The results reported from the Lab on QA/QC samples detected trace amounts of
chlorobenzene and chloroform in samples (TB-002-Tnp Blank at 0 2 ppb, and
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Fall 2010 Semi-Annual Report
FB-002-Field Blank at 0 3) This is most likely from laboratory contamination
(instrument cleaning) Analytical results are summanzed in the tables of
Appendix A and B Raw analytical data can be found in Appendix C and
isoconcentration maps of contaminants of concern can be found in Appendix D
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Section 2.0
Static Water Levels and Well Depths
2 1 STATIC WATER LEVELS
Static water levels for all monitoring wells were measured and recorded dunng
the fall of 2010 The water level measurements collected dunng the second
semi-annual sampling event can be found in Table 1 As shown in Table 1, 57
monitonng wells showed a decrease from Spnng 2010 to Fall 2010, 44 wells had
an increase from the previous year, and 8 wells were not evaluated dunng this
event H-2 was not found in due to snow, BC wells due to artesian pressure and
the presence of vegetable oil on the water table at well A-1 Water levels have
increased by as much as 1 50 feet at well X-5 and declined by as much as 1 82
feet at well G-6 from the spnng of 2010
The decrease in water levels overall at the Promontory facility can be attnbuted
to continuing drought conditions in the west over the past several years Static
water levels (SWLs) of groundwater monitonng wells (taken in the fall of 2010)
are recorded in Table 1 Additionally, Table 2 contains a list of monitonng wells
that are completed in unconsolidated material at the Promontory Facility and the
associated measured depth of each well A 2010 potentiometnc surface map of
the facility can be found in Appendix D
2 2 HYDRAULIC CONDUCTIVITIES
The hydraulic conductivity for each well was determined from well data collected
from ATK reports as well as slug testing conducted dunng the groundwater flow
and contaminant transport modeling effort (December 2005) The measured
hydraulic conductivity values for the wells are summarized in Table 3 Measured
hydraulic conductivity ranges from 0 05 to 775 ft/day These data were used to
obtain an initial distnbution of hydraulic conductivity values, which were modified
dunng calibration of the model Areas of higher hydraulic conductivity are
typically found where faults and/or fracture zones acts as major conduits of
groundwater flow and contaminant migration
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TABLE 1 - ATK LAUNCH SYSTEMS PROMONTORY
FALL 2010 WATER LEVELS
Elevation 2010 Spnng 2010 Fall
Well of top Depth to SWL SWL NET
No Date of casing Water Elevation Elevation CHANGE
A-1 12/13/2010 29-Aug-12 oil/no wl NA NA NA
A-2 12/13/2010 12-Dec-12 172 09 4558 40 4558 69 -0 29
A-3 12/13/2010 14-NOV-12 104 19 4598 52 4598 69 -0 17
A-5 12/13/2010 22-Aug-12 327 12 4291 42 4290 66 0 76
A-6 12/13/2010 8-Apr-12 190 11 4291 94 4292 09 -0 15
A-7 12/13/2010 28-Mar-12 178 01 4293 14 4292 89 0 25
A-8 12/13/2010 12-Apr-12 193 41 4293 19 4293 34 -0 15
A-9 12/13/2010 5-May-12 216 47 4293 33 4292 96 0 37
A-10 12/13/2010 23-Jan-13 214 18 4558 25 4558 36 -0 11
B-1 12/13/2010 31-Jul-12 304 00 4292 22 4291 95 0 27
B-2S 12/13/2010 25-Apr-12 207 51 4291 80 4292 00 -0 20
B-21 12/13/2010 25-Apr-12 207 46 4291 85 4292 02 -0 17
B-2D 12/13/2010 25-Apr-12 208 00 4291 31 4291 15 0 16
B-3 12/14/2010 14-Aug-12 319 06 4291 69 4292 05 -0 36
B-4 12/14/2010 3-May-12 216 65 4290 64 4290 99 -0 35
B-5 12/14/2010 15-Feb-12 153 92 4275 17 4275 38 -0 21
B-6 12/14/2010 15-Dec-ll 99 27 4267 75 4267 01 0 74
B-7 12/14/2010 18-Nov-ll 72 60 4267 56 4267 96 -0 40
B-8 12/14/2010 11-Dec-11 87 39 4276 33 4276 23 0 10
B-9 12/14/2010 9-NOV-12 135 82 4561 97 4561 19 0 78
B-10 12/14/2010 22-Sep-12 88 07 4560 99 4559 73 1 26
C-1 12/14/2010 19-May-12 233 33 4290 40 4289 95 0 45
C-2 12/14/2010 19-Jul-12 294 26 4290 30 4290 16 0 14
C-3 12/14/2010 25-Aug-12 330 64 4290 98 4291 24 -0 26
C-4 12/14/2010 26-NOV-12 237 59 4477 09 4476 71 0 38
C-5 12/14/2010 5-Mar-12 155 18 4293 29 4293 15 0 14
C-6 12/13/2010 23-May-12 234 58 4292 44 4292 82 -0 38
C-7 12/13/2010 27-Dec-11 88 25 4291 48 4291 67 -0 19
C-8 12/13/2010 31-Jan-12 121 59 4292 53 4292 84 -0 31
D-1 12/14/2010 8-N0V-I2 138 44 4558 49 4558 53 -0 04
D-2 12/14/2010 9-Aug-12 313 28 4291 80 4291 43 0 37
D-3 12/14/2010 18-Jun-12 259 99 4293 88 4294 06 -0 18
D-4 12/01/2010 18-May-12 228 91 4293 44 4293 25 0 19
D-5 12/01/2010 20-May-12 231 75 4292 51 4292 35 0 16
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TABLE 1 - ATK LAUNCH SYSTEMS PROMONTORY
FALL 2010 WATER LEVELS
Elevation 2010 Spnng 2010 Fall
Well
No Date
of top
of casing
Depth to
Water
SWL
Elevation
SWL
Elevation
NET
CHANGE
D-6 08/23/2010 29-Jun-12 272 95 4291 21 4291 28 -0 07
E-1 12/15/2010 29-Dec-ll 102 70 4278 36 4278 48 -0 12
E-2 12/01/2010 20-Dec-11 101 12 4271 20 4271 37 -0 17
E-3 10/07/2010 23-Dec-l 1 108 70 4266 98 4267 05 -0 07
E-4 10/07/2010 8-Dec-ll 94 30 4265 86 4265 94 -0 08
E-5 10/07/2010 4344 55 80 27 4264 28 4264 33 -0 05
E-6 10/07/2010 10-Nov-ll 68 03 4263 98 4264 04 -0 06
E-7 10/07/2010 15-Dec-ll 98 30 4268 81 4267 69 1 12
E-8 10/07/2010 19-Mar-12 194 74 4267 32 4267 46 -0 14
E-9 10/07/2010 21-Apr-12 202 93 4292 45 4292 77 -0 32
E-10 12/15/2010 12-Jan-13 471 30 4289 91 4290 17 -0 26
EW-6 12/21/2010 13-Nov-ll 68 57 4266 68 4267 08 -0 40
F-1 12/15/2010 26-Dec-ll 87 89 4290 30 4290 61 -0 31
F-2S 12/15/2010 30-Dec-ll 103 94 4278 41 4278 53 -0 12
F-21 12/15/2010 30-Dec-ll 104 00 4278 35 4278 50 -0 15
F-2D 12/15/2010 30-Dec-l 1 92 27 4290 08 4290 00 0 08
F-3 12/15/2010 10-Dec-ll 83 63 4279 16 4279 44 -0 28
F-4 12/13/2010 23-Feb-12 169 58 4267 56 4267 76 -0 20
F-5 12/15/2010 15-Dec-ll 99 77 4267 46 4267 67 -0 21
G-1 10/07/2010 30-Nov-ll 84 47 4267 84 4268 06 -0 22
G-2 10/07/2010 2-Nov-ll 58 33 4266 30 4266 42 -0 12
G-3 10/07/2010 14-Sep-ll 12 10 4263 79 4263 79 0 00
G-4 12/28/2010 8-Nov-l 1 66 97 4263 97 4263 96 0 01
G-5 12/28/2010 8-Jan-12 130 74 4260 48 4260 20 0 28
G-6 12/28/2010 4325 83 68 19 4257 64 4259 46 -1 82
G-7 12/28/2010 3-Jan-12 127 56 4258 79 4258 74 0 05
G-8 12/28/2010 3-Apr-12 219 23 4258 58 4258 15 0 43
H-1 12/21/2010 3-Oct-ll 29 43 4265 31 4265 46 -0 15
H-2 12/3/2010 15-Oct-ll NA NA 4265 96 NA
H-3 12/21/2010 5-Nov-ll 61 36 4266 62 4266 84 -0 22
H-4 12/21/2010 2-Dec-ll 87 25 4267 41 4267 66 -0 25
H-5 12/21/2010 9-Oct-ll 35 06 4265 09 4265 24 -0 15
H-6 12/03/2010 17-Oct-ll 44 34 4264 34 4264 52 -0 18
H-7 12/21/2010 28-Dec-11 112 54 4268 08 4268 40 -0 32
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Fall 2010 Semi-Annual Report
TABLE 1 - ATK LAUNCH SYSTEMS PROMONTORY
FALL 2010 WATER LEVELS
Elevation 2010 Fall 2010 Spnng
Well of top Depth to SWL SWL NET
No Date of casing Water Elevation Elevation CHANGE
H-8 12/03/2010 4386 17 106 05 4280 12 4280 44 -0 32
H-9 12/21/2010 29-Aug-l 1 1 60 4257 67 4257 02 0 65
H-10 12/21/2010 16-Aug-ll 3 50 4242 77 4242 08 0 69
J-1 12/27/2010 4455 00 120 87 4334 13 4333 86 0 27
J-2 12/01/2010 1-Oct-12 344 51 4314 07 4313 70 0 37
J-3 12/13/2010 25-Jul-12 123 52 4467 19 4467 11 0 08
J-4 12/13/2010 25-Jun-12 287 87 4272 30 4272 31 -0 01
J-5 10/12/2010 17-Oct-ll 49 70 4258 95 4258 83 0 12
J-6 10/12/2010 4321 70 63 27 4258 43 28-Aug-11 0 12
J-7 10/07/2010 5-Mar-12 114 83 4334 13 11-Nov-ll 0 80
J-8 10/12/2010 8-Mar-]2 11851 4333 02 IO-Nov-11 0 67
J-9 10/12/2010 13-Mar-13 530 96 4290 93 30-Sep-11 -0 32
LF-1 12/27/2010 7-Feb-12 120 75 4300 96 4299 91 1 05
LF-2 10/07/2010 20-Feb-12 129 47 4305 30 13-0ct-11 0 51
LF-3 12/21/2010 4419 92 120 49 4299 43 8-0ct-11 -0 24
LF-4 12/21/2010 lO-Mar-12 152 95 4300 12 9-0ct-11 -0 23
M39-
B1 12/03/21010 4-Sep-12 214 80 4417 08 3-Feb-12 -0 44
M114-
B1 12/03/21010 25-Jun-12 162 12 4398 02 4398 30 -0 28
M508-
B1 12/27/2010 8-May-12 160 68 4351 40 29-Nov-l 1 0 07
M508-
1 12/27/2010 2-May-12 156 50 4350 18 29-Nov-l 1 -0 88
M508-
2 12/27/2010 lO-May-12 165 52 4348 89 27-Nov-l 1 -1 05
M508-
3 12/27/2010 2-May-12 154 75 4351 62 29-Nov-l 1 0 01
M508-
4 12/27/2010 7-May-12 159 62 4352 37 30-NOV-11 0 08
M636-
B1 12/03/21010 29-Sep-12 76 95 4579 96 14-JUI-12 0 19
P-1 12/27/2010 14-Jun-12 203 07 4346 25 24-Nov-l 1 0 18
P-2 12/27/2010 4-Jun-12 137 76 4401 45 4401 37 0 08
P-5 12/27/2010 24-Apr-12 122 88 4375 29 23-Dec-11 -0 14
P-6 12/27/2010 5-Jun-12 88 02 4452 91 9-Mar-12 0 13
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TABLE 1 - ATK LAUNCH SYSTEMS PROMONTORY
FALL 2010 WATER LEVELS
Elevation 2010 Fall 2010 Spnng
Well of top Depth to SWL SWL NET
No Date of casing Water Elevation Elevation CHANGE
P-7 12/27/2010 25-May-12 79 80 4449 72 6-Mar-12 -0 16
P-8 12/27/2010 13-May-12 160 87 4356 93 4-Dec-11 0 25
P-9 12/27/2010 26-May-12 177 38 4353 32 3-Dec-11 -1 76
T-1 12/21/2010 13-Dec-ll 98 24 4267 59 6-Sep-11 -0 22
T-2 12/21/2010 26-Jul-12 300 85 4290 77 4291 54 -0 77
X-4 12/13/2010 4861 35 607 10 4254 25 23-Aug-11 0 35
X-5 12/13/2010 4491 31 236 60 4254 71 4253 21 1 50
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Total
TABLE 2
Fall 2008
Depth of Monitonng Wells Completed in Unconsolidated Material
Well Total
Depth
Well Total Depth Well Total Depth
A-7 243 15 G-1 97 59 H-5 47 83
B-5 177 77 G-2 98 95 H-6 52 90
B-6 125 56 G-3 26 48 H-8 149 52
B-7 97 38 G-4 76 21 H-9 11 97
B-8 112 68 BC-1 64 41 H-10 28 05
C-7 108 36 BC-2 44 49 J-1 144 08
E-1 126 31 BC-3 34 39 J-3 146 43
E-2 120 12 BC-4 76 45 EW-6 206 46
E-4 131 84 BC-5 39 47 M508-1 202 87
E-5 120 36 BC-6 38 40 M508-2 199 30
E-8 225 84 LF-1 136 12 M508-3 202 32
E-9 232 09 LF-2 152 63 M508-4 200 54
F-1 106 32 LF-3 147 65 M508-B1 181 58
F-2A 150 48 P-1 256 71 TCC1 214 05
F-2B 217 05 P-2 178 30
F-2C 318 91 P-5 125 55
F-3 107 48 H-4 102 28
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TABLE 3
SUMMARY OF REPRESENTATIVE HYDRAULIC CONDUCTIVITIES
Well No
Hydraulic
Conductivity
(ft/day)
Hydraulic
Conductivity
Range (ft/day)
A-1 730
A-2 27 23-31
A-3 54 42-75
A-4 410 350-470
A-5 190 120-260
A-6 360 310-410
A-8 775 650-900
A-9 145 120-170
A-10 15 13-17
B-1 33 26-41
B-3 2 73 2-3 4
B-4 39 82 35 28-44 35
B-5 0 75 0 3-1 1
B-6 470
B-7 4 85 4 2-5 5
B-8 3 11
B-9 26
C-1 52 37-70
C-2 510
C-3 30 5 26-35
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TABLE 3 (Continued)
SUMMARY OF REPRESENTATIVE HYDRAULIC CONDUCTIVITIES
Well No
Hydraulic
Conductivity
(ft/day)
Hydraulic
Conductivity
Range (ft/day)
C-4 560 470-650
C-5 43
C-6 18 15-30
C-7 250 210-290
C-8 3 45 1-5 9
D-1 54
D-2 552 5 445-660
D-3 2 93
D-4 0 55
D-5 0 26
D-6 92 4
E-1 39 2 36 2-42 2
E-2 89 55 87 0-92 1
E-3 114 05 100 9-127 2
E-4 14 45 13 0-15 9
E-5 23 15 22 2-24 1
E-6 4 95 4 9-5 0
E-7 0 55 0 5-0 6
E-8 109 10 7-11 1
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TABLE 3 (Continued)
SUMMARY OF REPRESENTATIVE HYDRAULIC CONDUCTIVITIES
Well No
Hydraulic
Conductivity
(ft/day)
Hydraulic
Conductivity
Range (ft/day)
E-9 05
E-10 30 7 30 2-31 2
F-1 16 37 16 13-16 60
F-2A 2 31 2 20-2 41
F-2B 2 07 1 68-2 46
F-2C 0 07 0 052-0 087
F-3 3 73 3 67-3 79
F-4 63 73 62 15-65 30
G-1 16 69 16 26-17 12
G-2 41 38 38 61-44 14
G-3 2 05 1 91-2 18
G-4 40 58 37 96-43 19
G-5 29 43 27 62-31 23
G-6 62 76 57 82-68 44
G-7 7 01 6 85-7 16
G-8 0 34
BC-2 12
BC-3 10
BC-4 1
BC-5 92
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TABLE 3 (Continued)
SUMMARY OF REPRESENTATIVE HYDRAULIC CONDUCTIVITIES
Well No
Hydraulic
Conductivity
(ft/mm)
Hydraulic
Conductivity
Range (ft/day)
BC-6 9
LF-1 4 66 3 08-6 23
LF-2 1 6
LF-3 5 07 4 80-5 33
LF-4 21 25
P-1 03
P-2 17 16-18
P-3 63 5 62-65
P-5 6
P-6 24
P-7 37 5 29-46
P-8 38
P-9 32
H-1 0 66 0 62-0 69
H-2 1 38 1 29-1 46
H-3 4 17
H-4 298 73 269 86-327 60
H-5 6 78 5 21-8 35
H-6 1 41
H-7 55 43 54 79-56 07
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TABLE 3 (Continued)
SUMMARY OF REPRESENTATIVE HYDRAULIC CONDUCTIVITIES
Well No
Hydraulic
Conductivity
(ft/day)
Hydraulic
Conductivity
Range (ft/day)
H-8 1 39
H-9 0 11
H-10 0 05
J-1 04 0 34-0 46
J-3 0 05
J-4 10 36 5 14-15 58
J-5 311 69 203 76-419 62
J-6 149 4 138 66-160 13
J-7 0 11 0 06-0 15
J-8 0 11 0 06-0 15
J-9 0 029
EW-1 7
EW-6 108 66
X-4 11 5
X-5 1 32
M-508-1 56 5 45-5 75
M-508-2 3 15
M-508-3 34 3 38-3 42
M-508-4 3 29 2 74-3 83
M-508-B1 0 45 0 45-0 46
TCC-2 09 0 46-1 33
(a) The hydraulic conductivity range identifies the results of all testing of the
well I e the results of a slug and bail test conducted at the same time
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Fall 2010 Semi-Annual Report
Section 3.0
Hazardous Plume Charactenstics
Hazardous plumes at M-136 histoncally have consisted of six volatile organic
compounds (other volatile constituents are occasionally found at very low levels
in one or more wells) These constituents are tnchloroethene (TCE), 1,1,1-
tnchloroethane (TCA), 1,1-dichloroethene (DCE), 1,1-dichloroethane (DCA),
chloroform, and cis-1,2-dichloroethene In addition to the VOCs, perchlorate is
also a contaminant of concern at the facility These plumes are descnbed below
and illustrated in Figures 3 1 through 3 6 of the Fall 2009 Semi-Annual Report
that was previously submitted to the Division Isoconcentration maps of
constituents DCA, DCE, perchlorate, TCA, and TCE can be found in Appendix D
Isoconcentration maps were generated with data from 2009, 2010, and 2011 No
map was prepared for cis-1,2,dichloroethene because no significant change was
noted from 2009 to 2010
31 TRICHLOROETHENE
The TCE contamination at the facility consists of four major parts a major plume
south and east of the M-136 burning grounds, a small plume in the perched
aquifer centered at well D-1, a plume associated with well B-6 beneath the
Administration/ Manufactunng area and, a small plume north and west of the
Administration area In addition, several small plumes are located at the
northernmost manufactunng area (previously the U S A F Plant 78), and the
ATK Launch Systems sanitary landfill
The major plume onginates in the M-136 Burning Ground source area, and has
migrated south and south-southwest with values above 5 mg/l beyond the ATK
Launch Systems property boundary At the Administration/Manufactunng areas,
additional sources (likely buned dram fields) of tnchloroethene have raised mean
values in the ground water at wells B-6 and G-2, and E-1 This plume extends
beneath adjacent agricultural lands to an unused irngation well EW-6 EW-6 has
seen a significant reduction in the amount of TCE that was once detected
(concentrations have dropped from 299 ug/L to 34 1 ug/L) Eight monitonng wells
have been constructed on Mr Adams property to monitor contaminant migration
Low levels of TCE have been identified in a few of these wells, but none of the
wells have been above the MCL of 5 ug/L
The plume in the northern manufactunng area appears to have onginated from
laboratory wastes associated with a lab located in building E-519 The plume
has migrated southwest From P-8 to M508-4 Two years ago the level at M508-4
was at 6200 and last year dropped to 2350 ug/L The plume has moved further
west to M508-3 was at 5810 ug/L, in 2009 Additional groundwater monitor wells
14| Page February 20 1 0
Promontory Post-Closure Permit
Fall 2010 Semi-Annual Report
have been installed downgradient of J-1 to determine the area and extent of the
plume There does appear to be some natural attenuation of this plume
Monitonng Well J-4 located by M-114, has identified a plume that had
approximately 7000 ug/l TCE In the Fall of 2006 this amount rose to 9000 ug/l
and in the spnng of 2007, to 11,700 ug/l, and finally to 14,400 ug/L dunng the Fall
of 2007 Since then, the levels of TCE have significantly dropped to the 3000 to
4000 ug/L range Passive Soil Gas sampling was used to determine if the TCE
was coming from the canyon east of the well No TCE was detected In 2009, a
new well, J-9 was installed to determine if the TCE contamination was moving
East from J-4 Analytical data reported from samples collected from J-9, have
shown non-detects for TCE, which demonstrates that the TCE contamination in
the J-4 area is being monitored by down gradient wells
In September 2007, 8000 gallons of Vegetable oil was injected in A-1, near the
M-136 burning grounds to evaluate enhanced anaerobic bioremediation of
perchlorate and solvent contaminated groundwater Significant reductions of TCE
were observed in well A-1 Concentrations of TCE went from 1,210 to 6 6 ug/L
Reductions have also been noted in some of the wells near A-1 Monitonng is
ongoing at the downgradient wells
3 2 1,1,1 -TRICHLOROETHANE
The 1,1,1-tnchloroethane in ground water can be found in two pnmary plumes
The largest plume is centered on the southeast border of the burning grounds
The highest levels (1090 mg/l) of contamination are in wells C-3 and A-5 A
second large plume at well B-5 has almost disappeared in the last decade with
concentrations reducing from approximately 15,000 mg/l in 1990 to 266 mg/l in
2002 to 48 ug/L in 2008 The 1,1,1-tnchloroethane plume has naturally degraded
to DCE and then to mostly nonhazardous constituents The source of this plume
IS uncertain, but a spill in 1984 at the M-52 degreaser of approximately 1,000
gallons of 1,1,1-tnchloroethane seems to be the likely source
There has been a noted decrease in TCA in the Burning grounds as part of the
Bioremediation project A-1 reduced from 128 ug/L to ND Well A-5 has reduced
from 5000 to 1020 ug/L dunng 2009 Monitonng will be ongoing as this project
continues
3 3 1,1-DICHLOROETHENE
1,1-Dichloroethene is a breakdown product of 1,1,1-tnchloroethane, and is found
in the TCA plumes There are two known 1,1-dichloroethene plumes, one
15 I Page February 20 10
Promontory Post-Closure Permit
Fall 2010 Semi-Annual Report
beneath the burning area which extends south of the Administration Building and
another very minor plume at well P-6
3 4 1,1-DICHLOROETHANE
Small plumes of 1,1-dichloroethane are centered at wells A-5,C-3, B-5, G-2 and
EW-6
3 5 CHLOROFORM
A chloroform plume is located beneath the M-136 Burning Grounds, and small
plumes are centered at wells F-1, B-5 and extend south of the Administration
area Reductions in the M-136-Burning Grounds have been noted, A-5 dropped
from 700 ug/L to 473 ug/L dunng 2008 and 2009 Monitoring well EW6 went from
1 5 ug/L to ND
3 6 PERCHLORATE
Perchlorate plumes are monitored at the facility because of regulatory oversight,
and concerns expressed by UDSHW and USEPA Region VIII as part of the ATK
Launch Systems CME Small plumes are found in monitonng wells which access
perched aquifers to the east of plant The major plume extends beneath pnor
disposal areas in the burning grounds, the perchlorate gnnd building M-174, the
washout building M-115, and the drainfield west of the Administration area
Concentrations of 200,000 and 135,000 ug/L were detected within the burning
grounds plume dunng the fall of 2010 at wells D-4 and D-5, respectively
Concentrations at G-2 were up from 49,400 ug/L in 2008 to 52,100 ug/L in 2010
in the plume west of the administration area
A major source of perchlorate found in Pipe Spnng on the southwest plant
boundary may be histoncal disposal of washout waters from Minuteman
production It is possible that these wastes have migrated southward in perched
zones to this spnng ATK has constructed monitonng wells in this area to
evaluate this potential Of note is a substantial fluctuation in perchlorate in Pipe
Spnng, from approximately a high 440 mg/l to a recent concentration of 311 ug/l
Reductions have been observed at the Burning grounds resulting most likely
from the vegetable oil remediation
3 7 CIS-1,2-DICHLOROETHENE
Cis-1,2-dichloroethene plumes are located beneath pnor disposal areas at wells,
F-1, G-2 and the burning grounds. Well D-3 in the Burning Grounds was
16 I Page February 20 10
Promontory Post-Closure Permit
Fall 2010 Semi-Annual Report
detected at a concentration of 157,000 ug/L in 2008 Cis-1,2-dichloroethene is a
biological reductive dehalogenation breakdown product of chloroethenes (TCE)
and IS definitive evidence of natural attenuation by anaerobic bacteria The
significant increases at A-6 are likely due to the bioremediation Project at M-136
Significant reductions have been noted in EW-6 well on the Adams property It
went from 69 ug/l tol 3 ug/L and has continued to drop to a recent concentration
of 11 ug/L in 2009
17 I Page February 20 10
Promontory Post-Closure Permit
Fall 2010 Semi-Annual Report
Section 4.0
Corrective Action Program Effectiveness
In December 1992, ATK (then Thiokol) submitted the M-136 Liquid Thermal
Treatment Area Corrective Action Plan which describes the installation of wells
on the southern plant boundary These wells are used for corrective action
monitonng (to demonstrate the effectiveness of the corrective action program),
and to initiate active treatment strategies, if required
Concentration levels of hazardous constituents in groundwater monitonng wells
in source areas have generally diminished since disposal practices ceased in fall
1988 Well A-4 reported 47,000 mg/l TCA and 21,000 mg/l TCE in October 1988
and has dropped to approximately 2,780 mg/l TCA and 5,735 mg/l TCE
Similarly, well A-5 declined from 39,000 mg/l TCA and 2,300 mg/l TCE to
approximately 1,330 mg/l TCA and 1,020 mg/l TCE in spnng 2005 and further to
962 ug/l and 2080 ug/l TCE in fall 2008 A large TCA plume at well B-5 has
mostly disappeared in the last decade from approximately 15,000 mg/l in 1990 to
48 ug/L in 2008 The source of this plume is uncertain, but a spill in 1984 at the
M-52 degreaser of approximately 1,000 gallons of 1,1,1-tnchloroethane may
have contnbuted to it
Concentration levels in many wells and contaminated spnngs downgradient of
source areas have been relatively stable and have been trending down This may
indicate attenuation and degradation of constituents is approximately equal to
migration from source areas Well E-5 reported 25 mg/l TCE in October 2002,
only slightly greater than 10 mg/l TCE reported in spnng 1996 Well E-6 reported
77 mg/l TCE in October 2002, which is up from 31 mg/l reported in December
1990, but only slightly above 72 mg/l reported in June 1993, it is currently at 37
ug/L Well E-9 has been an exception to this general decline and reported levels
of TCE
Sampling of an old, unused agncultural well (EW-6) on Ray Adams property
revealed that TCE and breakdown products and perchlorate have migrated
farther off-plant than previously believed Eight additional monitonng wells have
been constructed on Mr Adams property and two wells downgradient of
contaminated spnngs to evaluate the extent of migration off plant The sampling
of these wells indicates contamination is predominantly moving southeast in
fractured carbonates, and only very slowly migrating to the south and west
Cis-1,2-dichloroethene is a biological reductive-dehalogenation breakdown
product of chloroethenes (TCE) and is definitive evidence of natural attenuation
by anaerobic bactena Cis-1,2-dichloroethene has been reported previously, in
18 I Page February 20 10
Promontory Post-Closure Permit
Fall 2010 Semi-Annual Report
plumes located at wells B-6, G-2, and F-1 These plumes have substantially
diminished as the cis-1,2-dichloroethene is (presumably) converted to ethenes
In September 2007, a pilot test was conducted at the Burning Grounds to
evaluate enhanced anaerobic bioremediation of Perchlorate and solvent-
contaminated groundwater 8000 gallons of soybean oil along with sodium
bromide (used as a tracer) was injected into well A-1 at the burning grounds
Sampling of local wells is ongoing to determine the effectiveness of the
treatment Significant reductions in perchlorate and TCE have been observed in
some of the downgradient wells
19 I Page February 20 10
APPENDIX A
ANALYTICAL DATA - VOLATILES
This appendix is oiganized as follows
CONSTITLE\T - Paiametei being analyzed foi
LOCATION
LAB
SAMPLE DATE
CONC
EQL
UNIT -
LAB SAMPLE ID
DILUTION
Well Numbei oi Spiing Number
1, 3 = outside laboiatory, 4 = ATK Launch Systems
Date sample was taken
Concenti£tion_leyel of^ojistitu^^
Method reporting limit estabhshed by EPA for
a given analytical method
Unit of measure
Unique sample ID number issued by the Lab
Dilution of sample
L^iSAMPLED_DATE j CCg^L|^UiT| ,UVB_SAiy!BiiJ | pilu|jpn
1,2 TETRACHLOROETHANE
1,2-TETRACHLOROETHANE
1,2-TETRACHLOROETHANE
1,2-TETRACHLOROETHANE
1,2-TETRACHLCIROETHANE
1-TRICHLOROETHANE
1-TRICHLOROETHANE
1-TRlCHLOROETHANE
1-TRICHLOROETHANE
l-TRICHLOROETHANE
I-TRICHLOR6ETHANE
1-TRICHLOROETHANE
l-TRIOHLbRqETHANE
1-TRICHLOROETHANE
1-TRlCHLOROETHANE
1-TRICHLOROETHANE
l-TRICHLOROETHANE
1-TRICHLOROETHANE
1-TRICHLOROETHANE
1-TRICHLOROETHANE
l-TRICHLOROETHANE
l-TRICHLOROETHANE
1-TRICHLOROETHANE
l-TRICHLOROETHANE
1-TRICHLOROETHAINE
I-TRICHIOROETHANE
l-TRICHLOROiTHANE
l-TRICHLOROETHANE
l^RICHLOROETHAN^ _
l-TRICHLOROETHANE
1-TRICHLOROETHANE
l-TRICHLOROETHANE
1-TRjCHLOROETHANE
l-TRICHLOROETHANE
2,2-TETRACHLOROETHANE
2,2-TETRACHLOROETHANE
2,2-TETRACHLOROETHANE
2,2-TETRACHLOROETHANE
2,2-TETRACHLOROETHANE
2,2-TETRACHLOROETHANE
2,2-TETRACHLORBETHANE
2,2-TETRACHLOROETHANE
2,2-TETRACHLOROETHANE
2,2-TETRACHLOROETHANE
2,2-TETRACHILOROETHANE
2,2-TETRACHLOROEFHANE
2,2-TETRACHLOROETHANE
2,2-TETRACHLOROETHANE
2,2-TETRACHLORBETHANE
2,2-TETRACHLOROETHANE
2,2-TETRACHLOROETHANE
2,2-TETRACHLOROETHANE
2,2-TETRACHLOROETHANE
2,2-TETRACHL6ROETHANE
lD-6 ^
,Fish Spring
Horse Spring
Pipe Spring
Shotgun Spring
^C-7
iC-7A
X-8
^C-8A _
!D-4
I D-5
I D-6
I E-2
I E-6
I F-4
iFB-l
|FB-2
I Fish Spring
jG-3
_^H-6
j Horse Spring
i-2
-I -
U-5 U-6
J-7
'|LF-2_Z/.
!LF-3
Pipe Spring
Shotgun Spring
TB-1
TB-2 ~
C-7'"
;C-7A _
•c-8
4 J)8/23/2010
4 10/05/2010
4 10/05/2010
'4 10/05/2010
4 10/05/2010
4 12/13/2010
4 12/13/2010
4 12/13/2010
4 '12/13/2010
J4 12/01/2010
T4 12/01/2010
•4 ^08/23/2010
4_ I2/OI/2OIO
(4 10/07/2010
I4 ;10/07/2010
4 [12/13/2010
4 :12/13/2010
I4 jl2/2i/20lO
s4 TlO/05/2010
14 (10/07/2010
^4 ,12/03/2010
i4 [12/03/2010
j4 [10/05/2010
j4 ; 12/01/2010
10/12/2010
10/12/2010
10/07/2010
10/12/2010
10/07/2010
C-8A
'D-4
'D-5
'D-6
E-2
iE-5
I E-6
,F-4
FB-i
^FB-2
• Fish Spring
G-3
H-6
H-8
iHorse Spring
,J-5
ui
u
u
^1
u'l
ui
u'
u'
2 IJi
5 9Ji
324
U'
0 6ji
ui
u,
u
ui
ul
u
1 Ij'
10; Ug/L
10
10
12/21/2010
10/05/2010
:10/05/2010
12/13/2010
12/21/2010
12/13/2010
;12/13/2010
[12/13/2010
12/13/2010
^12/01/2010
[12/01/2010
'08/23/2OIO
12/01/2010
10/07/2010
10/07/2010
12/13/2010
12/13/2010
12/21/2010
10/05/2010
10/07/2010
12/03/2010
12/03/2010
10/05/2010
II2/OI/2OIO
^10/12/2010
ug/L
ug/L
10-ug/L
JOTug/L
.10'ug/L
10'ug/l
10 s ug/L
lOlug/L
T6^ug/L
10'ug/L
10-ug/L
10 ug/L
10 ug/L
10 ug/L
10iug/L
10 i ug/L
"io'ug/L
10;ug/L
lOJug/L
10[ug/L^
10,Ug/L
10:ug/L
10 ug/L
10:Ug/L
lojug/L
loiug/L
lOJug/L
0 4J 10|ug/L
U^
u'f
10^ ug/L
10'ug/L
U; 10 Ug/L
„Uu.
y,.
u[
IF
u
u
u
u'
u
u.
u^
u^
u
U;
ui
u(
u
u
u
1008028-01
1010002-01
1010002-02
1010002-03
1010002-04
1012015-06
1012015-07
1012015-02
1012015-03
1012003-01
1012003-02
1008028-01
1012003-03
1010005-03
1010005-04
1012015-01
1012015-04
1012027-02
1010002-01
1010005-05
1012009-01
1012009-02
1010002-02
1012003-04
1010012-01
1010012-02
1010005-01
1010012-03
1010005-02
1012027-01
1010002-03
1010002-04
1012015-05
10 ug/L
io ug/L
10 ug/L
10'ug/L
10[ug/L
lolug/L
loiug/L
ibTug/L
10 ug/L
10
10
ug/L
10 ug/L
10 ug/L
101ug/L
10 ug/L
10 ug/L
10 ug/L
10;ug/L
10[ug/L
10Iug/L
10=ug/L
10120^7-03
1012015-06
1012015-07
10120^-02
1012015^03
1012003-01
[1012003-02
1008028-01
1012003-03
1010005-03
1010005-04
1012015-01
1012015-04
1012027-02
1010002-01
1010005-05
1012009-01
1012009-02
1010002-02
1012003-04
1010012-01
II J. 4.:„-,^IIJU|NT,.^^,l.
1,1,2,2 JETRACHLOROETHANE^^
1,1,2,2 TETRACHLOROETHANE
1,1,2,2 TETRACHLOROETHANE"
1,1,2,2-TETRACHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2,2 TETRACHLOROETHANE
1,1,2,2-TETRACH LO ROETH AN E
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
I,I,2-TRICHL6ROETHANE
1,1,2-TRICHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1,2-TRICHLORbETHANE
1,1,2-TRICHLOROETHANE
1,1,2-TRICHLOROETHANE
l,y-TRICHLOROFirHANE _
%1,2-TRICHLORbETHANE
1,1,2-TRICHLOROETHANE
1,1,2-TRICHLOROETHANE
I, 1,2-TRICHLOROIETHANE
[1,1,2-TRICHLOROETHANE
[l,£2-TRICHL0R0ETHANE
II, l,2-TRICHL0R0ETHANE
'1,1^-TRICHLOROETHANE
'1,1,2-TRICHLOROETHANE
I,I,2-TRICHLOR6ETHANE
•• 1,1,2-TRICHL_0R0ETHANE
: l,l,2-TRICHL6RbETHANE""
i. WEf , f d^ffMAMPISD EiATE 1 CONC EQiruNlr l-tAt.SAMPLEnb*! blfutjon^
:J-6 10/12/2010 u ig'ugA 1010012-02 i 1
J 7 ' '4 10/07/2010 u i?ug/r 1010005 01 \ 1
J 8 4 10/12/2010 u 10 ug/L 1010012-03 ' 1
LF-2 4 10/07/2010 u 10; ug/L 1010005-02 [ 1
I LF-3 '4 12/21/2010 u 10; Ug/L 1012027-01 \ 1
: Pipe Spring '4 10/05/2010 u 10'ug/L 1010002-03 ' 1
Shotgun Spring i4 10/05/2010 u 10 Ug/L 1010002-04 ^ 1
TB-1 4 12/13/2010 u 10 ug/L 1012015-05 1
lTB-2 4 12/21/2010 u 101Ug/L 1012027-03 1
'c-7 4 12/13/2010 u 10^ Ug/L 1012015-06 ~\ 1
C 7A 4 12/13/2010 u 10 Ug/L 1012015-07 1
C-8 4 12/13/2010 u 10 ug/L 1012015-02 1
C-8A 4 12/13/2010 u 10 ug/L 1012015-03 1
'D-4 'A 12/01/2010 u 101ug/L 1012003-01 ; 1
|D-5 12/01/2010 u lOjug/L 1012003-02 i 1
'D-6 A 08/23/2010 17 9 loIug/L 1008028-01 ^ 1
iE-2 A 12/01/2010 U 101ug/L 1012003-03 [ 1
'E-5 A 10/07/2010 U 4010005-03 ! i
fE-6 |4 10/07/2010 U 10 ug/L 1010005-04 1
F-4 A 12/13/2010 U 10 ug/L 1012015-01 1
FB-1 !4 12/13/2010 u 10 ug/L 1012015-04 1
FB-2 ,4 12/21/2010 u "1012627-02 1
Fish Spring 4 10/05/2010 u 10 ug/L 1010002-01 1
G-3 A 10/07/2010 u 10 ug/L 1010005-05 1
jH-6 A 12/03/2010 U 10 Ug/L 1012009-01 1
'|H-8"' ,4 12/03/2010 U 10 ug/L ; 1012009-02 1
Horse Spring 4 10/05/2010 U 10 ug/L 1010002-02 1
J-2 J4 12/01/2010 U 10 ug/L 1012003-04 1
J-5 ..^
4
10/12/2010 U 10 ug/L '1010012-01 [ 1
J-6 ..^
4 10/12/2010 u " lo'ug/L 1010012-02 \ 1
J-7 ^4 10/07/2010 u "To ug/L 1010005-01 1
,J-8 10/12/2010 u 10 ug/L 1010012-03 1
LF-2 A 10/07/2010 u JLO'ug/Lj 1010005-02 1
LF-3
Pipe Spring
A 12/21/2010 u 10 ug/L 1012027-01 1 LF-3
Pipe Spring [4 .... 10/05/2010 u 10:ug/L 1010002-03 1
Shotgun Spring f
4 10/05/2010 u 101ug/L ; 1010002-04 1
^TB;1 '4
""•'4 "
12/13/2010 u 10|Lig/L 1012015-05 1
ITB^2 "
'4
""•'4 " 12/21/2010 u '1012027-03 "1 1
'C-7 '4 12/13/2010 u 10]ug/L 1012015-06 j 1
ic 7A 4 12/13/2010 u 10'ug/L 1012015-07 1
lC-8 4 12/13/2010 ul 10 f Ug/L 1012015-02 1
|C-8A 4 12/13/2010 U^ 10 Ug/L •1012015-03 1
jD-4 '4 12/01/2010 U 101ug/L 1012003-01 1 1
D-5 4 12/01/2010 U 10^ug/L 1012003-02 1
D-6 ^4 08/23/2010 3 8 J 10 ug/L 11008028-01 1
E-2 i4 12/01/2010 U' 10 ug/L ! 1012003-03 1
E-5 l4 10/07/2010 U 101ug/L 1010005-03 i 1
[E-6 '4 10/07/2010 U 10'Ug/L 1010005-04 \ 1
IF-4 4 12/13/2010 U 10 ug/L 1012015-01 1
!FB-1 4 12/13/2010 U 10^ug/L 1012015-04 1
FB-2 4 12/21/2010 U 10 ug/L 1012027-02 1
Fish Spring 4 10/05/2010 U 10 ug/L ,1010002-01 1
jG-3 A 10/07/2010 U 10 ug/L [1010005-05 1
H 6 4 12/03/2010 U 10!ug/L [1012009-01 1
I, 1,2-TRICHLOROETHANE
[l,l,2-TRIC_HL6ROEfHANE
II, 1,2-TRICHLORO ETHAN E
'1,1,2-TRiaHILOROETHANE
1,1,2-TRicHLORbETHANE
1,1-DICHLORbETHANE
1,1-DICHLOROETHANE
1,1-DICHLORbETHANE
[1,1-DICHLORbETHANE
'1,1-DICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHAlNE
'1,1-DICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHANE
'1,1-DICHLOROETHANE
^1,1-DICHLOROETHANE
'1,1-DICHLOROETHANE
'1,1-DICHLOROETHANE
1,1-DICHLORbETHANE
g4.,pf^'w£ti^""|-'i:xBi'
10 Ug/L
10'Ug/L
10 ug/L
10 ug/L
10Iug/L
1-DICHLOROETHANE
1-DICHLOROETHANE
1-DICHLOROETHANE
1-DICHLOROETHANE
1-DICHLOROETHANE
1-DICHLOROETHANE
1-DICHLOROETHANE
1-DICHLbROETHANE
1-DICHLOROETHANE'
1-DICHLOROETHANE
1-DICHLOROETHANE
l-DICHLOROETHANE
1-piCHLOROETHENE
1-DICHLOROETHENE
1-DICHLOROETHENE
l-DJCTLOFlbEfHi
1-DICHLOROETHENE
1-DICHLOROETHENE
1-DICHLOROETHENE
l-DigjlLOROETHE^
1-blCHLOROETHENE
1-DICHLOROETHENE
1-DICHLOROETHENE
l-DICHLORbETHENE
1-DICHLbROETHENE
l-DICHLOROETHENE
1-DICHLOROETHENE
1-DICHLOROETHENE
1-DICHLOROETHENE
1-blCHLOROETHENE
1-DICHLOROETHENE
l-DICHLblRbETHENE
l-DICHLOFt^OETHENE
l-DICHLOROETHENE
1-DICHLOROETHENE
1-DICHLOROETHENE
1-DICHLOROETHENE
l-DICHLOROETHENE
1-DICHLbROETHENE
1-DICHLOROETHENE
1-DICHLOROETHENE
1-DICHLOROPROPENE
1-DICHLOROPROPENE
l-DICHLOROPROPENE^^
l-blCHLOROPROPENE
1-DICHLOROPROPENE
2,3-TRICHLOROBENZENE
2,3-TRICHLORbBENZENE
2,3-TRICHLOROBENZENE
2,3-TRICHLOROBENZENE
2,3-TRICHLOROBENZENE
2,3-TRICHLOROPROPANE
2,3-TRICHLORbPRbPANE
H-8_
Horse Spring
J-2
J-5_
J-6
J 7 "
J-8
LF-2
LF-3
Pipe Spring
;Shotgun Spring
•TB-1
TB-2
C-7™
C-7A
C-8
'C-8A
D-4
ID-S"
!D-6
E-5
E-6"
F-4
FB-f
FB-2""
Fish Spring
G-3
H-e"
H-8
Horse Spring
J-2
J-5
LAB SAMPLEDlDATC
4 12/03/2010
10/05/2010
12/01/2010
10/12/2010
1^12/2010
10/07/2010
10/12/2010
10/07/2010
12/21/2010
10/05/2010
10/05/2010
12/13/2010
12/21/2010
12/13/2010
12/13/2010
12/13/2010
12/13/2010
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u
u
u[
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u
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u
u
Ul
u^
u
Ui
^tliiNrrflj^
10 ug/L JLOlOO^-05
10 ug/L i 1012009-01 i
10 ug/L 1012009-02 '
10 ug/L 1010002-02
10 ug/L 1012003-04
10 ug/L 1010012-01
10 ug/L 4010012-02
10 ug/L '1010005-01
10 ug/L 1010012 03
10 ug/L 4010005-02
10 ug/L 1012027-01
10 ug/L 1010002-03
10 ug/L 1010002-04
10 ug/L 1012015-05
10 ug/L 1012027 03
JIO ug/L 4012015-06
10 ug/L 11012015-07
10^ug/L_ 1012015-02
10 ug/L 1012015-03
10 ug/L 1012003-01
10 ug/L ;1012003j;p2
1008028-01
, 1012003-03
1010005-03
ug/L_ 1010005-04
ug/L 1012015-oi
10: ug/L 1012015-04
10,ug/L 1012027-02
To'ug/L "i6i66o2-6r
10 Ug/L 40i0005-05
lOug/L 1012009-01
10 = ug/L [1012009-02
"lOiUg/Lj 1010002-02I
10 ug/L 1012003-04
10 ug/L 4010012-01
'1010012-02
1010005-01
1010012-03
1010005-02
1012027-01
10i6002-63
10 ug/L
10 ug/L
10 ug/L
10
10
1010002-04
ug/L
ug/L
lO'ug/L
10iug/L
10 ug/L
10 ug/L
lO'ug/L
iOi.yg/L..
iiOug/L
10 ug/L
10|ug/L
1? ug/L
loTug/L
10 ug/L '1012015-02"
1012015-03
1012003-oT
1012003-02
1008028-01
,1012003-03
1010005-03
1010005-04
1012015-05
4012027-03
'1012015-^
[i012015-07
J:.04ug/L„„
lOjUg/L
lOjug/L
10\ug/L
lOjug/L
10 ug/l
10 ug/l
F-4 4
'FB-1 4
FB-2 4
'Fish Spring 4
G-3 4
;H-6 4
H-8 4
^Horse Spring 4
'J-2 ••I4
J-5 4
iJ-6 4
!j-7 4
J-8 4
LF-2 '4
LF-3 A
Pipe Spring [4
llS^plQEfim^
Ul 10 ug/L
' 10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
101ug/L
1;
1
1
1
1
1
1
1
i
1
1
1
1
1
1
i[
li
1'
1
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ll
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1
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li
1
1
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1
1
1-
1
1
ll
1
1
1
1
1
ll
1
1
1
BROMOMETHANE
BROMOMETHANE
BROMOMETHANE
BROMOMETHANE
BROMOMETHANE ^
BROMOMETHANE
BROMOMETHANE
BROMOMJETHANE
BROMOMETHANE
BROMOMETHANE
BROMOMETHANE
BROMOMETHANE
JBROMOMEJHANE
BROMOMETHANE
BROMOMETHANE
BROMOMETHANE
BROMOMETHANE^
BROMOMETHANE
BROMOMETHANE
CARBON DISULFIDE
CARBON DISULFIDE
CARBON DISULFIDE
CARBON DISULFIDE
CARBONJDISULFIDL
CARBON DISULFIDE
CARBON DISULFIDE
CARBON DISULFIDE
CARBON DISULFIDE
CARBON DISULFIDE
CARBON DISULFIDL
CARBON DISULFIDE
CARBON DISULFIDE
CARBON DISULFIDE
CARBON DISULFIDE
CARBONDISULFIDE
CARBON DJSULFIDE
bAJRBq^N DISl^^
CARBON DISULFIDE
CARBbN DISULFIDE
CARBON DISULFIDE
CARBON DISULFIDE
iCARBON bjSlAFIDL
CARBON DISULFIDE
CARBON DISULFIDE
CARBON
CARBON
CARBON
CARBON
CARBON
CARBON
CARBON
CARBON
CARBON
DJSULFIDjL
mSULFIDL
DISULFIDE
DISULFIDE
TETRACHLORIDE
TETRACHLORIDE
TETRACHLORIDE
TETRACHLORIDE
TETRACHLORIDE
12/13/2010
12/13/2010
12/21/2010
10/05/2010
10/07/2010
12/03/2010
12/03/2010
10/05/2010
"i2'/01/20i6"
10/12/2010
10/12/2010
10/07/2010
10/12/2010
^Shotgun Springy
(TB-i
TB-2
C-7
C 7A
C-8
C-8A
D-4
D-5
D-6
:E-2
E-5
.iE-6
F-4
,FB-1
'FB-2
• Fish Spring
10/07/2010
12/21/2010"
10/05/2010
10/05/2010
i2/i3/20l6
12/2i/2010
12/13/2010
12/1372016
12/13/2010
12/13/2010
12/01/2010
12/01/2010
08/23/2010
12/01/2010
10/07/2010
10/07/2010
127l3/20id
12/13/2010
12/21/2016
10/05/2010
CARBON TETRACHLORIDE
G-3
H-6
'H-8
Horse Spring
J-2
J-5
JI-6
7-7"71
J-8
LF-2
LF-3
Pipe Spring
Shotgun Spnng
|TB-1
'TB-2
_iC-7
I C-7 A 7
jC-8
^C-8A
!D-4 •• _1
"•D-5™
10/07/2010
112/03/2010
42/03/2010
[10/05/2010
[12/01/2010
[10/12/2010
116/12/2010
io/ci7/26io"
l6/12/20i0™
10/07/2010
12/21/2010
10/05/2010
10/05/2010
12/13/2010
12/21/2010
.12/13/2010™
12/13/2010
12/13/2010
12/13/2010
,12/01/2010
Ul
u
Ul
u
u7
u
u,
•-i
u
u
Ui
i
u
u
u
u
u
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10
10
: 12/01/2010
u
u
u
u
u
u
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JJ
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u.
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ul
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u[
u
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u"
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u( UI u u 2J>i,^ 3 6 j'
ug/L
ug/L
10 ug/L
10,ug/L
10iug/L
lOiUg/L
lOjug/L
lolug/L
10 ug/L
10|Ug/L"
10,ug/L
10)ug/L
"i61ug/L
ug/L 10
10
ffe;SA*Ji1PLE*i#-
1012015 01 _
1012015-04
1012027 02
1010002-01
1010005-05
1012009-01
1012009-02
1010002-02
1012003-04
1010012-01
4010012-02
i 1010005-01
Wiq012-03 _
4610065-62
4012027-01
1010002-03
1010002-04
4012015^5
1012027-03
1012015-06 _
1012015-07 _
1012015-02
1012015-03
1012003^01
1612603-62
i6o8628-oi
ug/L
10;Ug/L
16•ug/L
10 ug/L
lolug/L
10[ug/L
lojug/L'
io Ug/L'
ug/L
ug/L
ug/L
1012003-03
1010005-03
10
10
10
1010005-04
1012015-01
1012015-04
1012027-02
1610602-01
101ug/L
10 ug/L
10iu.g/L
10 ug/L
10 ug/L
10 ug/L
.lOiygA^
10 ug/L
10 ug/L
10 Ug7L
10 ug/L
lOiug/L
"16 jug/L
10 ug/L
10 ug/L
10;ug/L
10 ug/L
1010005-05
1012609-01
1012009-02
l6l0002b2
1012663-64
1010012-01
4010012-02
1016665-01™
iqi6oi™2-ci3
1010005-02
1012027-01
1610002-03
1010002-04
1012015-05
1012027-03
1012615-06
1012015-07
1012015-02
1012015-03
1012003rm^
1612003-02
CARBON TETRACHLORIDE
CARBON TETRACHLORIDE
CARBON TETRACHLORIDE
CARBON TETRACHLORIDE
CARBON TETRACHLORIDE
CARBON TET"R"ACH"LORIDE™
CARBON TETRACHLORIDE
CARBON TETRACHLORIDE
CARBON TETRACHLORIDE
CARB"O N™TETRA"CH LO RI DE™
CARBON TETRACHLORIDE
CARBON TETRACHLORIDE
:CAIRB0N TETRACHLORIDE
CARBON TETRACHLORIDE
CARBON TETRACHLORIDE
CARBON TETRACHLORIDE
jCARBON TETRACHLORIDE
CARBqiM TETRACHLORIDE
CARBON TETFIACHLbRIDE"
CARBON TETRACHLORIDE^
CARBON TETRACHLORIDE 7
CARBON TETRACHLORIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROBENZENE
CHLOROBENZENE
CHLOROBENZENE
CHLOROBENZENE
CHJ.OROBLNZENE7
CHLbROBENZENE
CHLbROBENZENE
CHLOROBENZENE
CHLOROBENZENE
CHLOROBENZENE
CHLOROBENZENE
bHLqROBENZENE
,CHLbROBENZENIEl"
iCHLORbBENZENE^
bHLOROBENZENE
CHJLqROBENZENE
CHLOROBENZENE ^ 7
CHLOROBENZENE
CHLOROBENZENE
CHLOROBENZENE
CHiqRbBENZENE" 71
CHLORbBENZENE
CHLOROBENZENE
CHLOROBENZENE
CHLOROBENZENE
CHLOROBENZENE
CHLOROBENZENE
CHLOROBENZENE
CHLbROETHANE^
CHLOROETHANE
AlfcLLTi
D 6
E-2
E 5
E 6
|F-4
'FB-1
FB-2
Fish Spnng
H-6
H-8
Horse Spring
J-2
'J-5
J-6
J-7
J-8
.iLF:2 _
LF-3
iPipe Spring
Shotgun Spring
TB-1
,TB-2
b-7
C-7A
C-8
C-8A
D-4
D-5
b-6
E-2
E-5
L6 _ _
F-4
FB-1
FB-2
Fish Spring
jH-6
(H-8
J Horse Spnng
i-2
i'J-5
J-6
ij-7
;j"-"8""
^F-27
(LF 3
Pipe Spring
Shotgun Spring
TB-1
^TB-2
.C-7
7c-7A
LAB SAMPLED DME
4 08/23/2010
,12/01/2010
10/07/2010 "
10/07/2010
12/13/2010
12/13/2010
12/21/2010
10/05/2010
10/07/2010
I12/O3/2OIO
i12/03/2010
10/05/2010
12/01/2010
,10/12/2010
[10/12/2010
'10/07/2010
16/12/2010
10/07/2010
,42/21/2010
10/05/2010
'10/05/2010
[12/13/2010
14
•4 •
(4-
4
4
,4
4
4
14
'4
[4
4
4
4
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Jiii I4
4
A
(4
4
4
4
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4"
(4
[4
•4
4
12/21/2010
12/13/2010
42713/2010
12/13/2010
12/13/2010
12/01/2010
42/01/2010
'08/23/2010
il2/oi/2010
i10/07/2010
10/07/2010
"112/13/2010"
'i2/13/2010
42/21/2010
[10/65/2010
10/07/2010"
42/03/2010
12/03/2010
T6/05/2010
12/0J/2010
10/12/2010
:10/12/2010
]l0/07/2010
To/12/2016
10/07/2010
12/21/2010
10/05/2010
16/05/2010
42/13/2010
42/21/2010
i12/13/2010
"[i2/13/2010
CONG
351
Ul
u^i
u.
u
u
UJ u
u
u
u
ui
u,
u™f
u
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lO'ug/L^ 1008028-01
_i6'ug/L 1012003-03
10|ug/L 11016005-03
loiug/L 1010005-04
" 10 ug/L lOlJoiS-Ol
io ug/L 1012015-04
lOjug/L 1012027-02
lOjug/L 11010002-01
10'ug/L 1610005-05
ID^
10 ug/L
10 ug/L
lOjug/L
10 ug/L
10|ug/L
10 ug/L
loIug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug7L
10 ug/L
10'ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10
16
1012009-01
1012009-02
1010002-02
1012003-04
4010012-01
1010012-02
1010005-01
1010012 03™
1010005-02™
101202 T'-Ol
1010002-03
1010002-04
1012015-05
l6i2027-03
1012015-06
1012015-07
1012015-02
1012015-03
1012003-01
1012003-02
ug/L 4008028-01
U^
u'
04J^
U
Ui
0 3J
03J
U
Ui
0 2Ji
U
04J(
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u
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Ug/L
10] Ug/L
io ug/L
10 ug/L
T0(ug/L
10 ug/L
.10 ug/L
1.0 ug/L
10'ug/L
10 ug/L
10^ug/L
10 ug/L
4012003-03
4010005-03
1010665-04
1012015-61
1012015-04
1012027-02^
ioi6oo2-6i^
1010005-05
10
10
1012009-01
1012009-02
1016002-02
1012003-64
ug/L
ug/L
10 Uf/L
10 ug/L
10^ ug/L
10 ug/L
10 ug/L
loiug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
,1010012-01
1010012-02
1010005-01
1016012-03
,1010005-02
1012027-01
1010002-03
1010002-04
1012015-05
1012027-03
1012015-06
1012015-07
Dilution I
1
1
1
1
1
1
1
1
1
1
1
1:
li
"1
1
1
1:
1
1
1
1
1
1,
1
Ij
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1
1
1
1,
1
ij
1
1
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1
1
1
1
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1
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1
1
1
1
li
1,
1
1
E^^^l^^Nsi^i[i^r~"[^^
12/13/2010
12/13/2010
12/01/2010
12/01/2010
08/23/2010
12/61/2610
10/07/2010
10/07/2010
12/13/2010
12/13/2010
12/21/2010
10/05/2010
10/07/2010
12/03/2010
12/03/2010
10/05/2010
.10 ug/L
10 ug/L
10 Ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10.ug/L
CHLOROETHANE
CHLOROETHANE
CHLOROETHANE
CHLOROETHANE
CHLOROETHANE
CHLOROETHANE
iCHLOROETHANE
CHLqROETHANE
CHLOROETHANE
CHLOROETHAIsiE
CHLOROETHANE
CHLOROETHANE
CHIXDROETHANE
CHLOROETHANE
iCHLOROETHANE
CHLOROETHANE
CHLOROETH
CHLqRbjJHANE
CHLOROETHANE™
CHLOROETHANE
CHLO^EJHANE
CHLbROETHANE
CHLOROETHANE
CHLOROETHANE
CHLORbETHANE
CHLOROETHAJNIE
CHLOROETHANE
CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORM'
CHLOROFORM
OHj^ROFORM^
CHLOROFORM
; CHLOROFORM
CHLOROFORM
"CHLOROFOFIM
CHLbRbpORM^^
CHLOROFORM
iCHLOROFORM
'CHLOROFORiyL
'CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORM^
CHLqROFORMl
CHLOROFORM
CHLOROFORM_
CHLbfiOFORIvi
CHLORbpORM
CHLbROFORM
CHLOROFORM
CHLOROPbRM^
CHLORbFORM
C-8
C-8A
iD-4
D-5
D-6
E-2
I E-5
|E-6
F-4
[FB-l _
iFB-2
Fish Spnng
ql3
I H-6
^H-8
Horse Spring
•>2" "7_'
iJ:5 „ _11
J-6
'J.:.7
\]-8
'LF-2
LF-3
Pipe Spring
Shotgun Spring
TB4
TB-2
C-7
C-7A _
C-8
C-8A
D-4
D^S _
0-6"' '™"'
E-2
E-5 __™
E-6 "7„7
F.4
FB-1
FB-2
4
[4
|4
.J4
I4
4
I4"
j4...
i4
^v..^.^..^
|4
,4
[4
4
A
A
A
I4
A-
4
I4
i4
-t A
A
j4
4
'A
A
12/01/2010
10/12/2010
10/12/2016
10/07/2010
10/12/2010
'10/67/2010
[12/21/2010
40/05/2010
40/05/2010
,12/13/2"6lO
T2/2I/2OIO
12/13/2010
42/13/2610
il2/13/2010
[l2/13/20ib
'12/01/2010
s12/61/2010
Fisji Spring
G-3
iH-6
[H-8
Horse Spnng
J-2
|j-5
ij-6
J-7
j"-8
LF-2
I LF-3
Pipe Spring
Shotgun Spring
4
4
I4
4
A
A
4
4
4
08/23/2010
12/61/2010
10/07/2010
10/07/2610
12/13/2010
12/13/2016
12/21/2010
10/05/2010
i6707/2010
12/03/20i0
12/03/2010
10/05/2010
12/01/2610
'10/12/2010
10/12/2010
JO/07/2010
10/12/2010"
10/07/2010
;i2/21/2010
iio/05/2010
10/05/2010
U
U
U
U|
u t-u
Ui
u
U'™
U
U;
Ui
U
u
ui
u'
U;
ul
u?
u
10IUg/L
10'ug/L
10 ug/L
10 ug/L
lOjug/L,
10 ug/Ll
10(ug/L
idug/L
10"ug/7
lOlug/L
10 ug/L
lojug/L
10!ug/L
79 3
Uj ^
7 5 J
t"
3 9.JL.
4 J.
u
u'
u;
u
u;
u
Ui
^ uj
0 6J
... u.,„
u
u^"
u
ui uj
u
.B^/^(yiPligii¥(tDilC(tlon
1012015-02 _ . _
i012015-03
10i2003-01
1012003-02
1008028-01 1
iqi2003-03 ;
1010005-03
1010005-04
1012015-01
1012015-04
10i2027-02
1010002-01 I
1010005-05 i
10 ug/L
10 ug/L
U 10
Ui 10
ug/L
10
10
U
Ui
ui
US
ul
19J'
7 7^10
ug/L
Uj 10 ug/L
ug/L
ug/L
10[ug/L
10'ug/L
10 ug/L
loiug/L
1012009-01
1012009-02
1010002-02
1012002-04
1010012-61
1010012-02
1010005-01
10100121-03
1010005-62
1012027-01
1010002 03
1010002-04
10i2015-65"
1012027-03
1012015-06
i6l2015-07
1012015-02
1012015-03
10112063-01
10
id
ug/L
ug/L
ug/L
10(ug/L
lOiug/L™
lofug/L
10 ug/L
lO'ug/L^
10._ug/L
lolijg/l
ug/L
ug/L
ug/L„
lOjug/L^
l6|ug/L™
10jug/L
10jUg/L
16! ug/L
10|Ug/L™
10:ug/L
10jug/L_
lo1ug/L
10
10
10
1012J03-02
i008028-01
1012003-03
1010005-03
1010005-04
1012015-01
1012015-04
1012027-02
iqwoo2bil
1010665-05
1012009-01
1012009-02
1010002-02
1012003-04
1010012-01
1010012-02
1610005-61
1610012-03
1010005-02
1012027-01
1010002-03
1010002-04
M-
m.-
JENT
CHLOROFORM
CHLOROFORM
CHLOROMETHANE
CHLOROMETHANE
CHLOROMETHANE
CHLOROMETHANE
CHLOROMETHANE
CHLOROMETHANE
CHLOROMETHANE
CHLOROMETHANE^
CHLOROMETHANE
CHLORqMETHANE
CHLOROMETHANE
CHLORbMETHANE
CHLOROMETHANE
CHLOROMETHANE
CHLOROMETHANE
CHLOROMETHANE
CHLOROMETHANE
CHLOROMETHANE
CHLOROMETHANE
CHLOROMETHANE
CHLOROMETHANE
CHLOROMETHANE
CHLOROMETHANE
CHLORbMETHANE
CHLOROMETHANE
CHLOROMETHANE
CHLOROMETHANE^
CHLOROMETHANE
CHLOROMETHANE
CIS-l,2-DICHL0RqETHENE
CIS-ll2-DicHLbRqETHElNE
CIS-1,2-DICH lib Rb ETH E N E
CIS-1,2-DICHL0R0ETHENE
cisTi-DICHLOROETHENE
Cl^l,^DICHILqRqETHENE
CIS-ll2-DlciHLbR0ETHENE
'CIS-1,2-DICHL0R0ETHENE
aS-l,2-DICHJ.0RqETHENE
CIS-ir2-DICHLbR0ETHENE™i
CIS-I,2-DICHLOROJTHEJNE"
CIS-l,2-DICHLbR0ETHENE
CIS-l,2-DICHL0RqETHENE
aS-l,2-JDI£HL^
CIS-l,27DICHLORbETHEJvJE
CIS-1,2-DICHL0R0ETHENE
[aS-l,2-piCHL0R0ETHENE
[CIS-1,2-bicH LO RO ETH E N E
CIS-1,2-DICHL0R0ETHENE
CIS-l,2-DICHLbR0ETHE"NE
CIS-1,2-DICHL0R0ETHENE
CIS-i,2-piCHL0RqETHENE
CIS-l,2-DICHL0RbETHENE
WELL
(TB 1
jTB 2
C 7
'C-7A
C-8
1C8A
I D-4
D-5
I D-6
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••4-
E-5
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in-e '
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iJ-2
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J-2
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^LAB| SAI^PLEgDAJE
4 12/13/2010
12/21/2010
12/13/2010
12/13/2010
12/13/2010
12/13/20i0
12/01/2010
12/01/2010
08/23/2010
12/01/2010
10/07/2010
10/07/2010
12/1372010
12/13/2010
12/21/2010
10/05/2010
10/07/2010
A
A
4
4
4
4
4
4
4
4
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4 '12/13/2010
T 12/01/2010
4 12/01/2010
12/03/2010
12/03/2010
10/05/2010
12/01/2010
10/12/20i0
10/12/2010
10/07/2010
10/71272010
io/07/2010
,12/21/2010
10/05/2010
10/05/2010
12/13/2010"
;12/21/2oio"
12/13/2010
i2/13720l6
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4 12/01/2010
4 40/07/2010
4_To/07/26lO
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4" 12/13/2010
4 (12/21/2010
4 10/05/2010
ld707/2010
12/03/2010
12/03/2010
10/65/2610
4
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10/12/2010
10/12/2010
10/07/2010
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10 ug/L
10 ug/L
16 ug/L
10 ug/L
10 ug/l
10 ug/l
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/J:
16 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
lOjUg/L
10[ug7L
10(ug/L
10jug/L
16" ug/L
10,ug/L
10 ug/L
10 ug/L
10 ug/L
lOiug/L
10,ug/L
10 i ug/L
10(ug/L
10'ug/L
10 ug/L
10 ug/L
10 ug/L
101ug/L
10 ug/L
16!ug/L
10 ug/L
i6 ug/L
10|ug/L
io[ug/L
lo'ug/L
10 ug/L
10,ug/L
10(ug/L
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10(ug/L
10jug/L
To ug/L
10 ug/L
l^B_SAMPLE:
1012015-05
1012027 03
1012015-06
1012015-07
1012015-02
1012015 03
1012003-01
1012003 02
1008028-01
101200J-03
1010005 03
1010005 04
1012015-01
1012015-04
1012027-02
1010002-01
1010005-05
1012009-bi
1012009-02
1010002-02
1012003-04
1010012-01
1010012-02
1010005-01
1010012-03
10i0005-02
1012027-01
1010002-03
1010002-04
10120r5"-05"
1012027'-03
1012015-06
JL012015-07
1012015-02
1012015-03
1012003-01
1012003-q2_
1663628-01
4012003-03
1010005-03
1010005-64
10120JL5-01
1012015-04
1012027-02
1010002-01
1010005-05
1612069-01
1012009-02
1010002-02
1012003-04
1610012-01
1010012-02
1010605-01
1010612-63
JD jDiluJIon I
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CIS-l,2-DICHLqR0ETHENE
CIS-l,2-blCHL0R0ETHENE
CIS-1,2-DICHL0R0ETHENE
CIS-1 2-DICHLOROETHENE
CIST21DICIH|B^
CIS-1,2-DICHL0R0ETHENE
CIS-1,3-DICHL0R0PR0PENE
CIS-1,3-DICHL0R0PR0P^NE
CIS-l,3-DICHL0RbPR0PENE
C[S-1,3-DICHL0R0PR0PENE
CIS-I,3-DICHLORO"P"ROPENE
CIS-1,3-D1CHL0R0PR0PENE
CIS-1,3-DICHL0R0PR0PENE
CIS-l,3-DjCHL0R0PR0PJNE
CIS-1,3-DICHL0R0PR0PENE
CIS-1,3-DICHL0R0PR0PENE
CI?-1,3-DICHL0R0P^PENE
CrS-l,3-"DICHL0RbpR0PENE
CIS-1,3-DICHL0R0PR0PENE
CIS-l,3-DICHL0R0PRbpENE
CIS-l,3bicH ib ROPRbpENE
CIS-1,3-DICHL0R0PR0PENE
CIS-1,3-DICHL0R0PR0PENE
CIS-1,3-DICHL0R0PR0PENE
. CIS-l,3j-DICHL03bPRqPENE
blS4,3-DICHL™0RbPR0™PENE
CIS-1,3-DICHL0R0PR0PENE
l,CIS-l,3-DICHLbR0PRbpENE
CIS-l,3-DICHL0RqPR0PENE
CIIS-I,3-DICHLOROPROP"ENE
CIS-1,3-DICHL0R0PR0PENE
CIS-1,3-DICHL0R0PR0PENE
CIS-l,3-D[CHLqRqPRqPENE
CIS-l,3-DICHLbR0PR0PENE
iCIS-l,3-DICHL0R0PR0PENE
. Dl BROMOCH LOFtOMETTHAN E
Di B RO M OCH Lb ROM ETJH^^
DIBROMOCHLbROMETHANE
DIBROMOCHLOROMETHANE
, DIBROMOCHLOROMETHANE
DIBROMOCHLOROMETHANE
DIBRO M OCH LO RO M ETHAN E
DIBROMOCHLOROMETHANE
DIBROMOCHLOROMETHANE
DIBRBMOCHLOROM ETHANE
DIBROMOCHLOROMETHANE
DIBROMOCHLOROMETHANE
DIBROMOCHLOROMETHANE
DIBROMOCHLOROMETHANE
DIBROMOCHLOROMETHANE
DIBROMOCHLOROMETHANE
DIBROMOCHLOROMETHANE
DIBROMOCHLOROMETHANE
iDIBROMOCHLOROMETHANE
'••~wi'^m." "^ •LABi|FSAMPjED_Cf*TE |ftffi0NC|'¥QL | iWFT tXCSAI#LE_l§f Dillffloh
LF-2 4 10/07/2010 U _^_^10 Ug/L 1010005-02 1
LF-3 4 12/21/2010 U 10(ug/L 1012027-01 1
Pipe Spring 4 10/05/2010 U 10[ug/L 1010002-03 1
Shotgun Spnng 4 10/05/2010 U 10iug/L 1010002-04 1
TB-1 4 12/13/2010 U 10 ug/L 1012015-05 1
TB-2 4 12/21/2010 U 10^u"g/L 1012027-03 1
C-7 4 12/13/2010 U 10.Ug/L 1012015-06 1
C-7A 4 12/13/2010 u lo|ug/L 1012015-07 1
C-8 ^ ; 4 12/13/2010 u 10 ug/L 1012015-02 1
I c-8 A 4 12/13/2010 u 10.ug/l" 1012615-03 1
0^4™"™"™"' 4 12/01/2010 u 16'ug/L 1012003-01 1
D-5 4
...
12/01/2010 u ^10 ug/L 1012003-02 1
D-6 4 08/23/2010 u 10,ug/L 1008028-01 1
E-2 4 12/01/2010 u 10 ug/L 1012003-03 1
E-5 4 10/07/2010 u 10 ug]L 1010005-03 1
E-6 4 10/07/2010 u 10 ug/L 1010005-04 1
F-4 4 JL2/13/2010 u _10 ug/L 1012015-61 1
FB-1 4 12/13/2010 u To ug/L 1012015-04 1
FB-2 4 12/21/2010 u 'iolug/L 1012027-02 1
Fish Spring 4 10/05/2010 u 10 ug/L 1010002-01 1
G-3_^ 44
H-6 ™ '"" A
10/07/2010 u 10 ug/L 1010005-05 1 G-3_^ 44
H-6 ™ '"" A 12/03/2010 u io ug/L 1012009-01 1
H-8 4 12/03/2010 u lOjUg/L 1012009-02 . 1
Horse Spnng 4 10/05/2010 u 10 [ug/L 1010002-02 1
J-2 4 i2/01/2010 u _llO ug/L 1012003-04 _ _ 1
j-s' 4 107l2/26i0 u 10 ug/L 1010012-01™ "" i
J-6 4 10/12/2010 u 10 ug/L 1010012-02 1
J-7 4 10/07/2010 u 10 ug/L 1010005-01 1
J-8 4 10/12/2010 u 10?ug/L 1010012-03 1
LF-2" 4 16/07/2010™ u lOiug/L 1010005-02 • 1
LF-3 4 12/21/2010 u 10:ug/L 1012027-01 1
Pipe Spnng 4 10/05/2010 u lolug/L 1010002-03 1
Shotgun Spring 4 10/05/2010 u -10 ug7L 1010002-04 1
TB-1 4' 12/13/2610 u 10 ug/L 1012015-05 1
TB-2 4 12/21/2010 u 10,ug/L 1012027-03 1
C-7 _ 4 12/13/2010 u! _10'ug/L
Ul 10 Ug/L
1012015-06 1
C-7A 4 12/13/2010
u! _10'ug/L
Ul 10 Ug/L 1012015-07 1
C-B" 4 12/13/2010 Ul lOiUg/L' 1012015-02 1
C-8A 4 12/13/2010 U' 101Ug/L 10i2015-63 1
D-4 4 12/01/2010 U 10 ug/L 1012003-01 1
4 12/01/2010 U io'ug/L 1012663-02 """•71
D-6 4 08/23/2010 U 10 ug/L 1008028-01 1
IE-2 4 12/01/2010 U 10'ug/L 1012003-03 1
E-5 4 10/07/2010 U 10 ug/L 1010005-03 1
E-6^" 4 10/07/2010 U 10 ug/L 1010005-04 i 1
1012015-01 'i " 1 F-4 4 12/13/2010 u 10 ug/L ™
1010005-04 i 1
1012015-01 'i " 1
FB-1 4 12/13/2010 u 10'ug/L 1012015-04 1
FB-2 4 12/21/2010 u 10 ug/L 1012027-02 1
Fish Spring 4 10/05/2010 u _10|ug/L 1010002-01 1
G-3 4 i670772010 u lolug/L 1010005-05 1
H-6 4 12/03/2010 u 10(ug/L 1012009-01 1
H-8 4 12/03/2010 u 10 ug/L 1012009-02 1
Horse Spring 4 10/05/2010 u .10 ug/L 1010002-02 1
J-2' 4 12/01/2010 u 10 ug/L 1012003-04 1
li DIBROMOCHLOROMETHANE
DIBROMOCHLOROMETHANE
DIBROMOCHLOROMETHANE
DIBROMOCHLOROMETHANE
DIBROMOCHLOROMETHANE
DIBROMOCHLOROMETHANE
DIB[ROMOCHLOROMETHANE
DIBROMOCHLOROMETHANE
DIBROMQCHLOROMETHANE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DIBROMOMETHANE
DIBROMbMETHANE
DIBROMOMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
DILnj-ORbDIRbOROMETHANE
DICHLORODIFLUOROMETHANE
DICHLORODIFLUOROMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE _
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE^ _
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE 77 _11
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE
ETHYLBENZENE _
H EXACH LOROBUTADI EN E
HEXACHLOROBUTADIENE
HEXACHLOROBUTADIENE
HEXACH^qROBUTADIENE
HEXACHLOROBUTADIENE
'.tfWEL#
J-5
J-6
J-7
J-8
LF 2
LF-3
Pipe Spring
Shotgun Spring
TB-1
TB-2
D-6
Fish Spring
f Horse Spring
Pipe Spring
Shotgun Spring
D-6
Fish Spring
Horse Spring
Pipe Spring
Shotgun Spring
C-7 _71
;C-7A
ic-8
|c-8A
(D-4
b-5™™"""
•|D-6
'E-2_
E-5
E-6
F-4
^FB-L
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Fish Spnng
G-3
H-6
H-8
Horse Spring
J-2
iJ-5
I J-6 71_
"j-7
,J-8
!LF-2
|LF-3 "7_
Pipe Spring
Shotgun Spnng
TB-1
iTB-27 7.Z
>D-6
Fish Spring
Horse Spring
Pipe Spring
Shotgun Spnng
lll^^Bl SAMPLJP_DATE||
4
4
4
4
4
4
4
4
4
4
4
4
i4
4
4
4
4
4
¥
A
4
[4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
10/12/2010
10/12/2010
10/07/2010
10/12/2010
10/07/2010
12/21/2010
10/05/2010
10/05/2010
12/13/20i0
12/21/2010
08/23/2010
10/05/2010
10/05/2010
10/05/2010
10/05/2010
08/23/2010
10/05/20J.0
10/05/2010
10/05/2010
10/05/2010
12/13/2010
12/13/2010
12/13/2010
12/13/2010
12/01/2010
i27oi72oi6
08/23/2010
12/01/2010
10/07/2010
10/07/2010
12/13/2010
12/13/2010
12721/2010
10/05/2010
16/07/2610
12/03/2010
12/03/2010
10/05/2010
12/01/2010
40/12/2010
[4 10/12/2010
~A'
A
4
J4
'4
i4
j4
A
U
4
'4
4
%
10/07/2010
10/12/2010
40/07/2010
42/21/2010
T6/O5/2OI0"
10/05/2010
12/13/2010
12/21/2010
CONC
U
U^
u'
U
u
u
ul
u"
^U'
u
u
u
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u'
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u'
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u
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™u[
E%lUNIil
10 Ug/L
1.0, ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10'ug/L
10|ug/L
10 ug/L
10(ug/L
io ug/L
10 ug/L
10Iug/L
lOiUg/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
101ug/L
l6'ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10;ug/L
10 ug/L
10iug/L
U
"u'
u
u
"u
Uj
u'
Ui
u
u
u=
10 Ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10
10
08/23/2010
10/05/2010
10/05/2010
10/05/2010
[10/05/2010
U
U
U
u
u
u
ut
u
u.
Ug/L
ug/L
ioiug/L
io'ug/L
10,ug/L
10 ug/L
JO i ug/L
10 ug/L
10 ug/L
lOjUg/L
JLO'ug/L
loTug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
SLABJAMPJ
1010012-01
1010012-02
1010005-01
1010012-03
1010005-02
1012027 01
1010002-03
1010002-04
1012015-05
1012027-03
1008028-01
1010002-01
1010002-02_
1010002-03
1010002-04
1008028-01
1010002-01
4. —
1010002-02
1010002-03
1010002-04
1012015-06
1012015-07
1012015-02
1012015-03
1012003-01
1012003-02
1008028-01
1012003-03
1016605-63
1010005-04
1012015-01
1012015-04
1012027-02
1010002-01
1010005-05
1012009-01
1012009-02
1010002-02
1012003-04
1010012-01
1010012-02
1010005-01
1010012-03
1010005-02
1012027-01
1010002-03
1010002-04
1012015-05
1012027-03
1008028-01
1010002-01
1010002-02
1010002-03^
1010002-04
•.. li-'- CONStlfy^ WELUi?;. LAB SAMPLED_DATE CONCj EQL 1 UNtll LAB_SAMPLE_ID Oilutipn 1
ISOPROPYLBENZENE D 6 4 08/23/2010 u 10 Ug/L 1008028-01 1
ISOPROPYLBENZENE Fish Spring 4 10/05/2010 u 10 Ug/L 1010002-01 1
ISOPROPYLBENZENE Horse Spring 4 10/05/2010 u 10 ug/L 1010002-02 1
ISOPROPYLBENZENE Pipe Spring 4 10/05/2010 u 10 ug/L 1010002-03 1
ISOPROPYLBENZENE Shotgun Spring 4 10/05/2010 u 10 ug/L 1010002-04 1
m,p-XYLENE C-7 4 12/13/2010 u 10 ug/l 1012015-06 1
m,p-XYLENE C-7A 4 12/13/2010 u 10 ug/L 1012015-07 1
m,p-XYLENE C-8 4 12/13/2010 u lo!ug/L 1012015-02 1
m,p-XYLENE C-8A 4 12/13/2010 u lOjug/L 1012015-03 1
m,p-XYLENE D-4 4 12/01/2010 u lOjug/L 1012003-01 1
m,p-XYLENE D-5 4 12/01/2010 u lo'ug/L 1012003-02 1
m,p-XYLENE D-6 4 08/23/2010 u 10 ug/L 1008028-01 1
m,p XYLENE E-2 4 12/01/2010 u 10 ug/L 1012003-03 1
m,p-XYLENE E-5 4 10/07/2010 u 10 ug/L 1010005-03 1
m,p-XYLENE E 6 4 10/07/2010 u 10 ug/L 1010005-04 1
m,p-XYLENE F-4 4 12/13/2010 u 10 ug/L 1012015-01 1
m,p-XYLENE FB-1 4 12/13/2010 u 10 ug/L 1012015-04 1
m,p-XYLENE FB-2 4 12/21/2010 u 10 ug/L 1012627-02 1
m,p-XYLENE Fish Spring 4 10/05/2010 u 10 ug/L 1010002-oi 1
m,p-XYLENE G-3 4 10/07/2010 u 10 ug/L 1010005-05 1
m,p-XYLENE _ H-6 4 12/03/2010 u 10 ug/L 1012009-01 1
• m,p-XYLENE 'H-8 ^ 12/03/2010 u 10 ug/L 1012009-02 1
m,p-XYLENE Horse Spnng 4 10/05/2010 u-10 ug/L 1010002-02 1
,m,p-XYLENE J-2 4 12/01/2010 U' 10 ug/L 1012003-04 1
im,p-XYLENE J-5 4 10/12/2010 u' 10 ug/L 1010012-01 1
im,p-XYLENE J-6 4 10/12/2010 u" 10 ug/L 1010012-02 i
:m,p-XYLENE J-7 4 10/07/2010 u 10 ug/L 1010005-01 1
m,p-XYLENE J-8 4 10/12/2010 u 10 ug/L 1010012-03 I 1
m,p-XYLENE LF-2 4 io/07/2010 u lOlug/L 1010005-02 ' 1
m,p-XYLENE LF-3 4 12/21/2010 u 10 ug/L 1012027-61 1
m,p-XYLENE Pipe Spring 4 10/05/2010 ui 10 ug/L 1010002-03 1
m,p-XYLENE Shotgun Spnng 4 10/05/2010 u 10 ug/L 1010002-04 1
m,p-XYLENE TB-1 (4
TB-2 (4
12/13/2010 u 10^ ug/L 1012015-05 1
m,p-XYLENE
TB-1 (4
TB-2 (4 12/21/2010 u 10 ug/L 1012027-03 1
METHYLENE CHLORIDE C-7 4 12/13/2010 u 10 ug/L 1012015-06 1
METHYLENE CHLORIDE C-7A 4 12/13/2010 u 10 ug/L 1012015-07 [ 1
METHYLENE CHLORIDE C-8 4 12/13/2010 u 10 ug/L 1012015-02 I 1
METHYLENE CHLORIDE C-8A 4 12/13/2010 • u 10 ug/L 1012015-03 • 1
METHYLENE CHLORIDE D-4 4 12/01/2010 Ui 10 ug/L 1012003-01 1
METHYLENE CHLORIDE D-5 4 12/01/2010 u 10 ug/L 1012003-02 1
METHYLENE CHLORIDE D-6 4 08/23/2010 u 10 ug/L IOO8O28-61 " 1
METHYLENE CHLORIDE "E-2 4 "" 12/01/2010 u 10 ug/L i6l2603-03 1
METHYLENE CHLbRIDE E-5 4 10/07/2010 u. 10 ug/L 1010005-03 1
METHYLENE CHLORIDE E-6 4 10/07/2010 u 10 ug/L 1010005-04 1
METHYLENE CHLORIDE F-4 4 12/13/2010 u 10 ug/L 1012015-01 1
METHYLENE CHLORIDE FB-1 4 12/13/2010 i" u 10 ug7L 1012015-04 1 1
, METHYLENE CHLORIDE FB-2 4 12/21/2010 u. 10 ug/L 1012027-02 1
'METHYLENE CHLORIDE Fish Spnng 4 10/05/2010 u 10 ug/L 1010002-01 1
METHYLENE CHLORIDE G-3 4 10/07/2010 u 10 ug/L1 1010005-05 1
METHYLENE CHLORIDE H-6 4 12/03/2010 u 10 ug/L 1012009-01 1
METHYLENE CHLORIDE H-8 4 12/03/2010 u 10,ug/L 1012009-02 1
METHYLENE CHLORIDE Horse Spring 4 10/05/2010 u 10 ug/L 1010002-02 1
METHYLENE CHLORIDE J-2 4 12/01/2010 u 10 ug/L 1012003-04 1
METHYLENE CHLORIDE J-5 4 10/12/2010 u 10 ug/L 1010012-01 1
1 /j. CC»ISTITUENT 1 WEft. 1 LAB 1 SAMPLED_DATE |f CONCj EQL|i3prr f LAB_SAMPLE_ID 1 Dilution
METHYLENE CHLORIDE J-6 4 10/12/2010 U 10 Ug/L 1010012-02 1
METHYLENE CHLORIDE J-7 '4 10/07/2010 U 10 Ug/L 1010005-01 1
METHYLENE CHLORIDE J-8 4 10/12/2010 U 10 Ug/L 1010012 03 1
METHYLENE CHLORIDE .LF-2 4 10/07/2010 U 10 Ug/L 1010005-02 1
METHYLENE CHLORIDE LF-3 4 12/21/2010 U 10 ug/L 1012027-01 1
METHYLENE CHLORIDE Pipe Spring 4 10/05/2010 U 10 ug/L 1010002-03 1
METHYLENE CHLORIDE Shotgun Spring 4 10/05/2010 u 10 ug/L 1010002-04 1
METHYLENE CHLORIDE TB-1 [4 12/13/2010 u 10 ug/L 1012015-05 1
METHYLENE CHLORIDE TB-2 4 12/21/2010 u 10 ug/L 1012027-03 1
NAPHTHALENE D-6 A 08/23/2010 u 10 ug/L 4008028-01 1
NAPHTHALENE Fish Spnng (4 10/05/2010 Uf 10 ug/L i 1010002-01 1
NAPHTHALENE Horse Spring 14 10/05/2010 u' 10 ug/L i 1010002-02 1
NAPHTHALENE • Pipe Spring 4 10/05/2010 u 10 ug/L 1010002-03 1
NAPHTHALENE Shotgun Spnng 4 10/05/2010 u 10 ug/L 1010002-04 1
N-BUTYLBENZENE D-6 •4 08/23/2010 u 10 ug/L 1008028-01 1
N-BUTYLBENZENE Fish Spring A 10/05/2010 u 10 ug/L 1010002-01 1
N-BUTYLBENZENE Horse Spnng A 10/05/2010 u 10 ug/L 1010002-02 1
N-BUTYLBENZENE Pipe Spring A 10/05/2010 u 10iug/L 1010002-03 1
N-BUTYLBENZENE Shotgun Spring 4 10/05/2010 u 10(ug/L 1010002-04 1
N-PROPYLBENZENE D-6 4 08/23/2010 u 10 ug/L 1008028-01 1
N-PROPYLBENZENE Fish Spring 4 10/05/2010 u 10 ug/L 1010002-01 1
N-PROPYLBENZENE Horse Spring 4 10/05/2010 u 10 ug/L ioiooo2-02 1
N-PROPYLBENZENE ^Pipe Spnng 4 10/05/2010 u 10 ug/L 1010002-03 i 1
N-PROPYLBENZENE Shotgun Spring 4 10/05/2010 u 10 ug/L 1010002-04 i 1
0-XYLENE C-7 4 12/13/2010 u[
lojug/L
1012015-06 1
0-XYLENE C-7A" 4 12/13/2010 u lojug/L 1012015-07 1
0-XYLENE C-8 4 12/13/2010 u 10'ug/L 1012015-02 1
0-XYLENE C-8A 4 12/13/2010 u 10 ug/L 1012015-03 1
0-XYLENE D-4 4 12/01/2010 u 101ug/L 1012003-01 1
0-XYLENE "'D-5 4 12/01/2010 u 10 ug/L 1012003-02 i"
0-XYLENE b-6 4 08/23/2010 U; 10 ug/L 1008028-01 1
0-XYLENE E-2 4 12/01/2010 u^ 10 ug/L 1012003-03 1,
0-XYLENE E-5 A 10/07/2010 u 10,ug/L 1010005-03 1
0-XYLENE " E-6 4 10/07/2010 u 10 ug/L 1010005-04 1
0-XYLENE F-4 4 12/13/2010 u 10 ug/L 1012015-01 1
0-XYLENE FB-1 4 12/13/2010 u 10jug/L 1012015-04 1
0-XYLENE FB-2 4 12/21/2010 u 10fug/L 1012027-62 1
0-XYLENE .Fish Spring 4 10/05/2010 u 10 ug/L 1010002-01 1
0-XYLENE G-3 4 10/07/2010 UJ 10 ug/L 1010005-05 1;
0-XYLENE H-6™ 4 12/03/2010 u 10 ug/L 1012009-01 1^
0-XYLENE H-8 4 12/03/2010 u __10 ug/L 1012009-02 i 1
0-XYLENE Horse Spring 4 10/05/2010 u" "™™io|ug/L 1010002-02 1
0-XYLENE iJ-2 (4 12/01/2010 u loTg/L 1012003-04 1
0-XYLENE ts 4 10/12/2010 u 10 ug/L 1010012-01 i 1
0-XYLENE J-6 4 10/12/2010 u lO^ug/L 1010012-02 1
0-XYLENE J-7 4 10/07/2010 u 10'Ug/L 1010005-01 1
0-XYLENE J-8 4 10/12/2010 u 10 ug/L 1010012-03 1
0-XYLENE LF-2 4 10/07/2010 Ul 10 ug/L 1010005-02 li
0-XYLENE • LF-3 4 12/21/2010 U 10.ug/L 1012027-01 1
0-XYLENE Pipe Spring 4 10/05/2010 u^ 10 ug/L 1010002-03 ! 1
0-XYLENE Shotgun Spring 4 10/05/2010 u^ 10 ug/l 1010002-04 1
0-XYLENE TB-1 4 12/13/2010 u 10(ug/L 1012015-05 1
0-XYLENE TB-2 4 12/21/2010 u 10 ug/L 1012027-03 1
SEC-BUTVLBENZENE D-6 4 08/23/2010 u 10 ug/L 1008028-01 1
Dilution ]
1
1
1
1
il
1
1
1
1
1
1
1
1
1
1
li
1
1
1
1
1
1
1
1
1:
1
1
JL|
1
1
1
1
1:
1
1
i|
1
1
1
1
1
_i
_i
1
1^
1
1,
1
1
1
1
IFTT^oNsmiuii^
SEC-BUTTYLBENZENE _
SEC-BUTYLBENZENE
SEC~BUTYLBENZENE
SEC-BUTYLBENZENE
STYRJENE
STYRENE '
STYRENE
STYRENE
STYRENL ™
STYRENE
,STYRENE
iSTYRENE
STYRJNE
S"TYRENE
(STYRENE "
ISTYRENE
STYRENE ^ _
STYVENE
ISTYRENE
ISTYRENE
iSTYRENE
iSTYRENE
[STYRENE
STYRENE
STYRENE
STYRENE
STYRENE
STYRENE
STYRENE
STYRENE™
STYRENE"
STYRENE
STYRENE _
TERT-BUTYLBENZENE™ "™
TERT-BUTYLBENZENE
,TERT-BUTYLBENZENE
TERT-BUTYLBENZENE
TETRACH LO ROETH EN E
TETRACHLO ROETH E NE
i JETRACH LORO ETH EN E
TETRACHLOROETHENE
iTETRACHLOROETHENE
jTETRACHLORqETHENE
TETRiACHlbRbETHENE
TJTRACHLOROETHENE
TETRACHLbRbETHENE
TETRACHLOROETHENE
TETR AC H Lb Rb ETHE N E
TETRACH LO Rb ETH E N E
TiETRACHLOROETHENE
TETRACHLOROETHENE
TETRACH LO RO ETH E N E
TETRACHLOROETHENE
;Fish Spring
Horse Spring
,Pipe Spring
iShotgun Spring
iC-7 ••™ _
C-7A
C-8
C-8A
iD-4
D-5
D-6
E-2
E-5™
E 6
F-4
FB-1
4 iFB-2_^
Fish Spring
iG-3
,H-6
I H-8
'Horse Spnng
(j-2 "••
J-5
fJ-6
T7
T|-8"^ "
4F-2
LF-3 "[
Pipe Spring
Shotgun Spnng
TB-1
TB-2
D-6
4
-A-Fish Spring
Horse Spring
Pipe Spring
Shotgun Spnng
C-7
C-7A
ic-8
jC-8A
••+D-4-
. ,.D:5 .
0-6
1E-5
•E-6
F-4
A
4'
|FB-1
FB-2
J^ish Spring
b-3 "™"
lH-6
•SAMPLED_Di^j|
10/05/2010
io/05/2010
10/05/2010
10/05/2010
12/13/2010
12/13/2010
12/13/2010
12/13/2010
12/01/2016
12/61/2010
08/23/2010
12/01/2010
io/07/2010
10/07/2010
12/13/2010
12/13/2010
12/21/2010
10/05/2010
10/07/2010
12/03/2010
12/03/2010 7^ ™:
10/05/2010 T
12/01/2010
10/12/2016
10/12/20i6
10/07/2010
10/12/2010
10/07/2010
12/21/2010
10/05/2010
10/05/2010
12/13/2010
12721/2016™
08/23/2010™
10/05/2010
10/05/2010
10/05/2010
10/05/2010
12/13/2010
12/13/2010
42/13/20id ™"
fi2/13/2010™
U|
U
U;
u
Ui
u'
U;
ui
u
u
u
u'
u
u
Ul
U
Ui
u
u
u
u
u
u
u
12/01/2010
12/01/2010
08/23/2010
'12/01/2010
"io/07/2010
40/07/2010
12/13/2610
42/13/2010
12/2i/2010
^0/05/2010
40/07/2010
'12/03/2010
Ul
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4 6 Ji
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"EQLfUNIT
10'ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10*ug/L
10 ug/L
10 ug/L
lOiug/L
16 ug/L
10jug/L
lolug/L
10 ug/L
10 ug/L
10Iug/L
10 ug/L
10 ug/L^
10(ug/L
l6lug/L
10 ug/L
101ug/L
10!ug/L
10jug/L
lOiUg/L
l6fug/L
10 ug/L
10(ug/L
lo!ug/L
loiug/L
10 Mg/L
10jug/L
10 ug/L
yg/L
ug/L
10
10
101ug/L
10iug/L
10 ug/L
10,ug/L
10'ug/L
10,ug/L
LABISAMI^E.
1010002-01
i010602-02 "™
1010002-03
1010002-04
1012015-06^
1012015-07
1012015-02
1012015-03
1012003-01
1012003-02
1008028-01
1012003-03
1010005-03
1010005-04
1012015-01
1012015-04
1012627-62™
1010002-01
1010005-05
1012009-01
i012009-02_
1010062-62
1012603-04
1010012-01
1010012-02
1010065-61
4010012-03
1010005-02
1012027-01
10100_02-03_7
10i0002-04
4012015-05_
1012027-03
ID
4008028-01
1010002-01
,1010002-02
11010002-03
i1010002-04
4012015-06
[1012015-07
10\ug/L
lOlug/L
10jug/L
101 ug/L
10 ug/L
lO'Ug/L
lofug/L
10(ug/L
10 ug/L
10 ug/L
loiug/L
lotug/L
10 ug/l
10? ug/L™'
1012015-02
4012015b3
1012003-61
4012003-02
il608028-01
11012003-03
1010005-03™
1010005-04
4012015-01
fidi2015-04
1012027-02
^ 10100^2-OL
"1010005-05^
•1012609-61
CONSTITtStNt-
TETRACHLOROETHENE
TETRACHLOROETHENE
TETRACHLOROETHENE
TETRACHLOROETHENE
TETRACH LO ROETHENL_
TETRACHLOROETHENE
TETRACHLOROETHENE
TETRACHLOROETHENE
TETRACHLOROETHENE
TETRACHLOROETHENE
TETRACHLOROETHENE
TETRACHLOROETHENE
TETRACHLOROETHENE
TOLUENE
TOLUENE
TOLUENE
TOLUENL _
TOLUENE
TOLUENE
TOLUENE
TbujENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
iTOLUENE
TOLUENE _
TOLUENE
TOLUENE
TOLUENE
TOLUENE _
TOLUENE
TOLUENE
TOLUENE
TOLUENE _
TOLUENE
TbLUENE
TOLUENE
TOLUENE™ ^ _
TOLUENE
TRANS4,2-DICHL0RbETHENE
TRANS-L2-DiaHL0R0ETHENE
TRANS-l,2-DICHL0RbETHENE
• TRANS-l,2-DICHL0R0EfHENE
TRANS-l,2-DICHL0RbETHENE
TRANS-l,2-DICHL0RqETHENE
TRANS-i,2-DICHL0R0ETHENE
TRANS-L2-DICHL0RqETHENE
TRANS-1,2-DICHL0R0ETHENE
TRANS-1,2-DICHL0R0ETHENE
iTRANS-l,2-DICHL0R0ETHENE
TRANS-1,2-DICHL0R0ETHENE
|;^^||VELL^: 1 @^^'^S|MPLEff_t)AT^ ^NCf EblL 1 Om fsDilutio§
H-8 4 12/03/2010 u 10 u|/L 101206T02 1
'Horse Spring 4 10/05/2010 u 10 Ug/L 1010002-02 1
[J-2 4 12/01/2010 u 10 Ug/L 1012003-04 1
J-5 4 10/12/2010 u 10 Ug/L 1010012-01 1
J-6 4 10/12/2010 u 10 ug/L 1010012 02 ™ 1
J-7 4 10/07/2010 u 10 ug/L 1016605-01 1
J-8 .4 10/12/2010 u 10 ug/L 1010012-03 1
fLF 2 •4 10/07/2010 u 10 ug/L 1010005-02 1
LF-3 4 12/21/2010 u 10 ug/L 1012027-01 1
IPipe Spring 4 10/05/2016 u 10 ug/L 1010002-03 i [Shotgun Spring 4 10/05/2010 u 10 ug/l 1010002-04 1
TB-l 4 12/13/2010 u 10'ug/L 1012015-05 1
JB-2 4 12/21/2010 u 10 ug/L 1012027-03 1
'C-7 T™ 12/13/2010 u 10 ug/Li 1012015-06 1
C-7A .4 12/13/2010 u 10 ug/L 1612015-07 1
lc-8 (4 12/13/2010 u 10 ug/L 1012015-02 1
u 12/13/2010 u 10<ug/L 1012015-03 1
D-4 4 12/01/2010 u 10 ug/L 1012003-01 1
D-5 4 12/01/2010 u. 10 ug/L 1012003-02 1
D-6 4 08/23/2010 11 ji
.'i
10 ug/L 1008028-01 ....
1 E-2 4 J^Ol/2010 10 ug/L 1012003-03 1
,E-5 4 10/07/2010 10 ug/L 1010005-03 ... ~i
j4 10/07/2010 u 10.ug/L 1010005-04 1
F-4 4 12/13/2010 u lolug/L 1012015-01 1
FB-1 4 12/13/2010 . . Uj lOiug/L 1012015-04 1
FB-2 4 12/21/2010 u' 10,ug/L 1012027-02 1
Fish Spring 4 10/05/2010 uj"" 10 ug/L 1010002-01 1
G-3 4 10/07/2010 u 10 ug/L 1010005-05 1
H-6 4 12/03/2010 u 10; ug/L 1012009-01 1
H-8 4 12/03/2010 u 10 ug/L 1012009-02 1
Horse Spnng j4 10/05/2010 u. 10(ug/L 1010002-02 1
J-2 '4 12/01/2010 u 10 ug/L 1012003-04 1
J-5 15 10/12/2010 U; 101ug/L 1010012-01 1
J-6 '4 10/12/2010 '"™u*' 10 ug/L 10106i2-62 1
J-7 4 10/07/2010 u 10 ug/L 1010005-01 1
J-8 4 10/12/2010 u 10 ug/L 1010012-03 1
LF-2 4 10/07/2016 u 10;ug/L 1010065-02 1
LF-3 4 12/21/2010" ' u 10!ug/L 1012027-01 1
Pipe Spring (4 10/05/2010 u loJug/L 1010002-03 1
Shotgun Spring 4 10/05/2010 u' 10iug/L 1010002-04 1
TB-1 14 12/13/2010 yj.....
U'
lOiug/L 1012015-05 1
TB-2 4 "i2/2i/2oio
yj.....
U' 10,ug/L 1012027-03 1
C-7 4 12/13/2010 u 10[ug/L 1012015-06 1
C-7A 4 12/13/2010 u' 10 ug/L 1012015-07 1
C-8 4 12/13/2010 Ul
••'"" u^"^
10 ug/L 1012015-02 1
C-8A 4 i2/13/26lO
Ul
••'"" u^"^ 10 ug/L 1012015-03 1
D-4 :4 12/01/2010 u lOiUg/L 1012003-01 1
D-5 4 12/01/2010 u 10iug/L 1012003-02 1
D-6 14 08/23/2010 uJ 10*ug/L 1008028-01 1
E-2 4 12/01/2010 u 10-ug/L 1012003-03 1
E-5 4 10/07/2010 ul 10'ug/L 1010005-03 i
E-6 4 10/07/2010 u' 10 ug/L 1010005-04 1
F-4 4 12/13/2010 u' 10 ug/L 1012015-01 1
FB-1 4 12/13/2010 u. 10 ug/L ioi2015-04 1
I i I CONSTITUENT
TRANS-1,2-DICHL0R0ETHENE
TRANS-1,
TRANS-1,
TRANS-1
TRANS-1,
TRANS 1
TRANS-1
TRANS-1
TRANS-1
TRANS-1
TRANS-l
TRANS-1
TRANS4,
TRANS-1
TRANS-1
TRANS-1
TRANS-jL
TRANS-l,
TRANS-l[
TRANS-1,
TRANS-1,
fRANS4,
TRANS-1,
TRANS-1
T^ANS-1
TRANS-1
TRANS-i
TRANS-1
TRANS4
TRANS-l^
TRANS-1
TRANS-1
TRANS-i
TRANS-i
TRANS-1
TRANS-1
TRANS-1,
TRANS-l
TRANS-1,
TRANS-1,
TRANS-1,
TRANS-l
TRANS-1,
TRANS-1,
TRANS-i
TRANS-1
2-DICHLOROETHENE
2-DICHLOROETHENE
2-DICHLOROETHENE
2-DICHLOROETHENE
2-DICHLOROETHENE
2-DICHLOROETHENE
2-DICHLOROETHENE
2-DICHLOROETHENE
2-DICHLOROETHENE
2-DicHLORbETHENE
2-DICHLOROETHENE
2-DlCHLOROETHENE
2-DICHLORbETHENE
2-DICHLOROETHENE
2-DICHLOROETHENE
2- DJCHLOROETHENE
3- DICHLORbPROPENE
3-DICHLOROPROPENE
3-DICHLOROPROPENE
3-DICHLOROPROPJNE
3-DICHLORbPROPENE
3-DICHLOROPROPENE
3 DICHLOROPROPENE
3-DICHLOROPROPENE
3-DICHLOROPROPENE
3-DICHLOROPROPENE
3-DICHLOROPROPENE
3-DICHLOROPROPiENE
3-bicHLOiFloiPRbPENE
3-DICHLOROPROPENE
3-DICHLOROPROPENE
3-DICHLOROPROPEJNE
3-DicHLORbPROPENE
3-DICHLOROPROPENE
3-DICHLOROPRbPENE
3 - DJICH LO R OflRO/E N E_
3-blCHLOROPROPENE
3-DicHLOROPROPENE
3-DICHLORqPROPENE
3-DICHLOROPROPENE
3-DICHLOROPROPENE
3-DICHL0R"bPR0PENE
3-DICHLOROPROPENE
3-DICHLORbPROPENE
3-DICHLOROPROPENE
TRICHLOROETHENE ""
TRICHLOROETHENE
TRICHJ^ROrmENE _
TRICHLOROETHENE
[TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
•^-'; W.p.L^
:FB-2
Fish Spring
.G-3
'H-6
H-8
Horse Spring
iJ-2
J-5_
£-6
J-7
J-8
LF-2
LF-3 " 7_ _7
Pipe Spnng
Shotgun Spring
TB-1
TB-2
C-7
C-7A
C-8
C-8A 7
D-4
D-5
D-6
E-2 71
E-5
E-6
F-4
FB-1
I LAB]
4
4
4
4
4
4
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4
4
4
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A
4
4
4
14
. S£^f> LE^D_DAT|
12/21/2010
10/05/2010
10/07/2oio
12/03/2010
12/03/2010
10/65/2010
12/01/2010
10/12/2010
16/12/2610
10/07/2010
40/12/2010
10/07/2010
12/21/2010
10/05/2010
,10/05/26io
[12/13/2010
42/21/2010
12/13/2010
4 42/13/2010
4 12/13/2010
4 _ 12/i3/20i0
4 ~" 12/01/2010
12/01/2010
I FB-2
Fish Spnng
IG-3 i
H^6 1 ^71
'H-8
Horse Spnng
•^i-2_ •
J-5
08/23/2010
42/OI/2OI0I
"io/07/2bio
10/07/2010
'12/13/2010
12/13/2010
12/21/2010
10/05/2010
16/07/2010
12703/2610
J-6
J-7
J-8
LF-2
LF-3
Pipe Spring
Shotgun Spring
ITB-I
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iC-7
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ic-8 _7_
b-8A
D-4
D-5
D-6
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4
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u
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42/03/2010
10/05/2010
12/01/2010
10/12/20lio7
io/i2/2oio
40/07/2010
'10/12/2010
10/01/2010
li/'iijioio
10/05/2010
10/05/2016
12/13/2010
12/21/2010
12/13/2010
12/13/2010
12/L3/20l6
12/13/2010
12/01/2010
12/01/2010
08/23/2010
12/01/2010
Uf
U.
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EQI.|UN1T|
io ug/L
10 Ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
10 ug/L
"10 ug7L
10[ug/L
10[ug/L
lOjug/L
io ug/L
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101ug/L
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[l012027-CI3_
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1012015-02
4612015-03
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10jug/L
101ug/L
idug/L
10 ug/L
10,ug/L
10'ug/L
10 ug/L
i6 ug/L
10 ug/L
10 ug/L
10,ug/L
™'ia"ug/L
10 ug/L
10'ug/L
101 ug/L
10 Ug/L
10 ug/L
10 ug/L
1012003-01
11012003-02
1608O28-OI
4012003-03
10
16
ug/JL
ug/L
10 ug/L
10 [ug/L
lojug/L
10 ug/L™'
10;ug/L
lo'ug/L
10 ug/L
10 ug/L
To ug/L
100
106
1010005-03
,1010005-04
1012015-61
1012015-04
1012027-02
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1010005-05
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1012009-02
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ug/L
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TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENJ
TRICHLOROETHENE
TRICHLOPbETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
TRICHLOROFLUORbMETHANE
TRICHLOROFLUOROMETHANE
TR IC H LO RO F LU 0 ROM ETHANE
TRICHLOROFLubROMETHANE
TRICHLOROFLUOROMETHANE
TRICHLOROFLUOROMETHANE
TRICHLOROFLUOROMETHANE
TRICHLOROFLUOROMETHANE ^
TRICHLOROFLUOROMETHANE
TRICHLOROFLUOROMETHANL
TRICHLOROaUOROMETHANE
TRICHLOROFLUOROMETHANE^
TRICHLbROFLubROMETHANE
TRICHLOROFLUOROMETHANE
TRICHLOROFLUOROMETHANE _
TRICHLOROFLUOROMETHANE
TR IC H LO RO F LU O RO M ETH A N E " "
TRICHLOROFLUOROMETHANE
TRI£H LO RbF Lub Rbivi ET H AN E'
TRICHLOROFLUOROMETHANE _
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TRICHLORqFLUqROMETHANL
TRICHLbFtqFLUORbMETHANE
TRICHLOROFLUOROMETHANL^
TRICHLOROFLUOROMETHANE
TRICHLOROFLUOROMETHANE
TRICH LO RO F LU ORO M ETH AN E
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL ACETATE
VINYL ACETATE
VINYL ACETATE
|Sp ^iwEi^T
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lE-6
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FB-2
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iH-6
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iJ-2
!J-5
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J-8
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C-7
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D-5
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^i|P^l|^ii-^EDj@ATE ||G0N6|!EQL-|p)NrP
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C-7A
C-8
C 8A
4-^
•4
10/07/2010
io/07/2010
12/13/2010
12/13/2010
12/21/2010
10/05/2010
10/07/2010
12/03/2010
12/03/2010
10/05/2010
12/01/2010
10/12/2010
10/12/2010
,10/07/2010
[10/12/2010
10/07/2010
12/21/2010
10/05/2010
'i0/05/2010
12/13/2010
il2i/21/2Q10
12/13/2010
12/13/2010
12/13/2010
12/13/2616
12/01/2016
i2/01/2010
J08/23/2010
12/01/2010
'10/07/2010
"io/07/2010
12/13/2010
12/13/20107
i2/21/2010
10/05/2010
10/07/2010
12/03/2010
12/0372010
10/05/2010
12/01/2010
10/12/2610™
10/12/2010
16/67/2016
10/12/2010
i6/™07/20l6
12/21/2010
40 9
28 1
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10/05/2010
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12/21/2010"
12/13/2010
, 12/13/2010
[12713/2016
12/13/2010
Ui
U.
u'
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10 ug/L
10 ug/L
10 ug/L
10.ug/l
10'ug/L
10 ug/L
10 ug/L
10 f ug/L
10 ug/L
10 ug/L
10 ug/L
lOjUg/L
lOjug/L
lofug/L
10 ug/L
10,ug/L
"10 ug/L
lOiug/L
10'ug/L
10|ug/L
10 ug/L
10'Ug/L
10'ug7L
10|ug/L
lOlug/L
lojug/L
101ug/L
lOjug/L
l6Tg/L
Ug/L 10
B1AB_^MPLE_
1010005-03
1010065-04
1012015-01
1012015-04
1012027-02
1010002-01
1010005-05
1012009-01
1012009-02
1010002-02
1012003 04
,1010012-01
1010012-62
1010005-01
1010012-03
1010005-02
ii6l2027'-6l
4010002-03
1010002-04
4012015-05
1012027-03
1012015-06
1012015-07
4012015-02
'1012015-03
1012003-oi 7
i 1012003-02
1008028-01
1012003-03
1010005-03
ug/L
ug/L.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
10
10
10
10
16
10
10
10
10 Ug/L
10,ug/L
lO^Lig/L
10[ug/L
10*ug/L
10|ug/L
lOjug/L
l6fug/L
10jug/L
10iug/L
" 16] ug/L™
10 ug/L
50 ug/L
50,ug/L
50i.ug/L
501 ug/L
1010005-04
1012015-OL
ilj6l[2015-64
[1012027-02
1010062-01
[1010005-05
[1612069-01
[1012609-02
1010002-02
1012003-04_
1010012-01
1010012-02"
1010005-01
1010012-03
1010005-02
1012027-01
1010002-63
1010002-04
1012615-65
1012027-03
1012015-06
10120J.5-07
1012015-02
10120i5-03
.ID I ^Dilution I
1
1
1
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I iMsi SAMPLED DATE
4 12/01/2010
12/01/2010
O8/23/261O
12/01/2010
10/6772010
10/07/2010
12/13/2010
12/13/2010
12/21/2010
10/05/2010 ™
10/07/2010
12/03/2010
'12/O3/2OJLO
™io/05/20l6
i12/01/2010
'10/12/2010
10/12/2610
f QL |ipiT|i^|^(^|LE^ip
50 ug/L 1012003-01
50 ug/L 1012003-02
50fug/L 1008028-01
50iUg/L _1012q03-03
50 ug/L 1010005-03
50,ug/L Toio6o5-04
50 ug/L 1012015-01
50jug/L 4012015-04
5o!"ug7L ,1012027^2
50 ug/L 'ioi6o02-01
50 ug/L 1010005-05
50 ug/L '1012009-01
4012009-02
1010002-62
,1012003-04
50 ug/L *1010012-01
50:ug/L 4010012-02
50'ug/L T1O16665-61
50 ug/L T1OIOOI2-O3
50[ug/L 1010005-02^
50'ug/Lj 1012027-01
50 ug/L 1010002-03
50jug/L 4010602-04
50'ug/L [1012015-05
50 ug/L 1012027-03
lOiug/L 1012015-06
10-ug/L '
DilutitJig
1 VINYL
VINYL
VINYL
VINYL
iVINYL
VINYL
VINYL
VINYL
VINYL
VINYL
VINYL
VINYL
[VINYL
VINYL
VINYL
IVINYL
[VINYL
VINYL
VINYL
VINYL
VINYL
VINYL
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[VINYL
'VINYL
^VINYL
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(VINYL
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, CfNSTITUENT-
ACETATE
ACETATE
ACETATE
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ACETATE
ACETATE
ACETATE
ACETATE
ACETATE
ACETATE
ACETATE
ACETATE
ACETATE
ACETATE
ACETATE
ACETATE
ACETATE
ACETATE
ACETATE
ACETATE
ACETATE
ACETI^TE
ACETATE
ACETATE
ACETATE
CHLOmDE
CHLORIDE
CHLOR[DE
CHLqRIDE
CHLORIDE
VINYL
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iyiNYL
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lyiNYL
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' VINYL
VINYL
VINYL
VINYL
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CHLORIDE
CHLORIDE
CHLbRIDE
CHLORIDE
CHLbRiDE
CHLORIDE
CHLO_RIDE
CHLORIDE
CHLORIDE
CHLORIDE
CHLORIDE
CHLORIDE
CHLORIDE
CHLORIDE™
CHLORIDE
CHLORIDE
CHLORIDE
CHLORIDE
CHLORIDE
CHLORIDE
CHLORIDE
CHLORIDE
CHLORIDE
CHLORIDE
D-4
D-5
b-6
lE-2
E 5
E-6
iF-4
IFB-I
FB-2
|Fish Spnng
G-3
H-6
H-87
Horse Spring
J-2
J-5
,J-6"
J-7
J-8
LF-2
LF-3
Pipe Spnng
(shotgun Spnng
TB-1
TB-2
C-7
C-7A
C-8
C-8A
D-4
D-5
D-6
E-5
E-6
F-4
FB-1
IFB-2
Fish Spring
G-3
H-6 71
H-8~
Horse Spring
J-2
J-5^
J-6
J-7
J-8
LF-2
LF-3
Pipe Spring
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TB-1 _
TB-2
4_
4
,4
4
|4
•4
(4
4
[4
'4
A
4_
"4
4
4
4 _
4 i10/07/2010
[4 40/12/2010
4 10/07/2010
4 ^2/21/2010
4 40705/20i0™
I410/05/2010
4 ,12/13/2010
14 _h2/21/2010
4 12/13/2loio
4 12/13/2010
12/13/2010
14^ 12/13/2010
[47 12/01/2010
4 12/61/2010
,4 08/23/2010
"4 .12/01/2010
4_ J10/07/2010
4 7lO/07/20l6
14 ; 12/13/2010
47112/13/2610
,4 12/21/2010
'A 10/05/2010
U 10/01/2010
42/03/2010 4
4
.4
A
A
4
'4
4
.!4
4
.[4
(4
4
4
(12/03/2010
10/05/2010
42/01/2016
10/12/2010
10/12/2010
10/07/2010
40/12/2010
10/01/2010
12/21/2010
io/05/2010
10/05/2010
12/13/2616
I12/21/2OIO™
mm.
u
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Ug/L
Ug/L
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50 Ug/L
50 ug/L
50 ug/L
lO.ug/L
10'ug/L
10
1012015-07
1012015-02
10
10
1012015-03
,10i2"003-01 ug/L ____
ug/L 10i2603-02
ug/L jl008028-01
10:ug/L 71012603^3
101 ug/L |l010005-03
10'ug/L 4010005-04
10[Ug/L '1012015-01
lOjug/L 1012015-04^
10 ug/L 'i012627-02
10 ug/L 1010002-01
10 ug/L ]l010005-65
lok^L Toizoog-of
10 ug/L7l0i2009-02
10 j ug/L i 1010002-02
10 ug/L 1012003-04
10[ug/L jl010012-0L
10 ug/L il0100i2-02
10! ug/L T0IOOO5-OI
10 ug/L 1010012-03
10[ug/L 4010005-02
i6jug/L [1612027-01
10;ug/L '1010002-03
lOiug/L 1010002-04
lO'ug/L 1012015-05
10 ug/L 1012027-03
APPENDIX B
ANALYTICAL DATA - PERCHLOFLATE
1 his appendix is oiganized as follo\^s
CONSTITUEN T
LOCATION
LAB
SAMPLE DATE
CONC
EQL
UNIT
LAB SAMPLE ID
DILUTION
Paiametei being analyzed foi
WeU Numbei oi Spnng Numbei
1 3 = outside laboiatoiy 4 = ATK Launch Systems
Date sample was taken
Concentration leygLoLconstituent-in-sample,
Method reporting limit established by EPA for
a given analytical method
Unit of measure
Unique sample ID number issued by the Lab
Dilution of sample
miw LAB t 'ID • P©ilu*tioh'
PERCHLORATE C-7 4 12/13/2010 102
PERCHLORATE C-7A 4 12/13/2010 97
PERCHLORATE c-s" 4 12/13/2010 7 i
PERCHLORATE C-8A 4 12/13/2010 7
PERCHLORATE D-4 4 12/01/2010 130000
PERCHLORATE D-5 4 12/bl/2blb 168000
PERCHLORATE D-e" A 08/23/2010 73400
PERCHLORATE ' E-2 4 12/01/2010 1 U
PERCHLORATE ]
PERCHLORAfE ^
E-5 4 10/07/2010 57 PERCHLORATE ]
PERCHLORAfE ^ E1"6 4 10/07/2010 51
PERCHLORATE " F-4 ~i4" 12/13/2010 184
PERCHLORATE FB-1 4 12/13/2010 U
PERCHLORATE |^FB-2
PERCHLORATE (Fish Spring
4 12/21/2010 U PERCHLORATE |^FB-2
PERCHLORATE (Fish Spring 14 10/05/2010 U
PERCHLORATE G-3 T 10/07/2010 J u'
PERCHLORATE H-6 4 12/03/2010 u
PERCHLORATE H-8 A 12/03/2010 u
PERCHLORATE Horse Spring 4 10/05/2010 u
PERCHLORATE J-2 ,4
•...
12/01/2010 223
PERCHLORATE J-5 4 10/12/2010 " 23'(^
, ... Jr. .„).. PERCHLORATE J-6 " *4 10/12/2010 12
PERCHLORATE J-7 [4 10/07/2010 618
PERCHLORATE J-8 4 10/12/2010
PERCHLORATE LF-2 4 10/07/2010 U
PERCHLORATE LF-3 4 JL2/21/2010
PERCHLORATE Pipe Spring (4 10/05/2010 265
IIERCHLORATE Shotgun Spring t4" 10/05/2010 92
PERCHLORATE TB-1 14 12/13/2010 U
PERCHLORATE TB-2 14 12/21/2010
20 ug/L
20 ug/L
4 ug/L
4000bjg/L
4000 uj^L.
4000 ug/L
40 ug/L
40 ug/L
20 ug/L
4 ug/L
4 ug/L
4 ug/L
40 ug/L
40 ug/L
201ug/L
20[ug/L
40'ug/L
'2b[ug/L
4'ug/L
4 ug/L
4qiug/L
ug/T
40 ug/L
4
40 ug/L
40iug/L
4.ug/L
4 ug/L
1012015-06 5
1012015-07 5
11012015-02 1
1012015-03 \
1012003-01 1 1006
1012003-02" 1000
'i008028-01 .... 1000,
1012003-03 lol
1010005-03 10
i1010005-04 5
1012015-01 1
1012015-04 1
1012027-02 1
11010002-01 10
' 1010005-05 10;
1012009-01 5'
1012009-02
1010002-02 1
1012003-04 5
lbl0012-01 l[
1010012-02 1,
1010005-01 Tq^
1010012-03 ll
1010005-02 lOi
1012027-01
-„-,-,-li
ioiobo2-03 10
1010002-04 lOi
1012015-05 1''
1012027-03 [j[
Promontory Post-Closure Permit
Fall 2010 Semi-Annual Report
APPENDIX C
ANALYTICAL DATA SHEETS
1008028
ENVIRONMENTAL LAB WORK REQUEST
™ ATK E>fVIRONMENTAL LABORATORY LWRNo
Login No
E13190
FROM EXTINSION COST CSNTIR WORKORDER DAT!
ORCANliATION MAILSTOr REPORT RESULTS TO
HELEN RAVSTEN, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS SAMPLE DATE
G c
LOCATION TIME TEST REMARKS
y ISIS
2
J
3
4
5
6
7
9
10
n
t
12
CHAIN OF CUSTODY
RELINQUISHED BY DATE TIME RECErVED BY DATE TIME
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED
988P LS333 GW
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Requested
Friday, September 10, 2010
TESTED FOR ATK DLV
Environmental Monitoring
Thiokol Corp, UT 84322
ANALYZED BY ATK Launch Systems
Analytical Chemistry Laboratory
P O Box 707, M/S 245
Bngham City, UT 84302-0707
435-863-3732
435-863-8080
Contact Name:
Project
Sample Delivery Group.
Al Lee
Ground Water Testing - DLV
1008028
Page 1 of 5
Pnnted 09/10/10 11 18
Sample Delivery Group 1008028
Sample No Client No
Test Requested
1008028 01 D 6
Sample Description
Received Collect Date/Time
Matrix
08/27/10 8/23/2010 15 15 13
EPA 314 0
SW-846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
Certified By 09/10/2010
W Scott Fraser, Quality Assurance Officer Date
r/i/s certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation
Program (NELAP) unless otherwise annotated
Page 2 of 5
Pnnted 09/10/10 1118
Listing of Results by Sample
Sample Delivery Group 1008028
Client Sample 10 0 6
Sample Description ATK DLV Ground Water Fall 2010
Laboratory Sample ID 1008028 01
Date Sampled 08/23/10 15 15
Dilution
CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date
Test Method EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE 73400 ug/L 1000 4000 1000 JMM 09/02/10
Test Method SIV 846, 8260S (Water) Volatile Organic Analysis
67 64 1 ACETONE 72 J ug/L 5 10 1 QC 08/30/10
71-43 2 BENZENE 0 8 J ug/L 0 22 10 1 QC 08/30/10
74 97 5 BROMOCHLOROMETHANE U ug/L 0 31 10 1 QC 08/30/10
75 27-4 BROMODICHLOROMETHANE 0 8 J ug/L 0 19 10 1 QC 08/30/10
108 86 1 BROMOBENZENE U ug/L 0 37 10 1 QC 08/30/10
75 25 2 BROMOFORM U ug/L 0 42 10 1 QC 08/30/10
74 83 9 BROMOMETHANE U ug/L 0 57 10 1 QC 08/30/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 08/30/10
104 51 8 N BUTYLBENZENE u ug/L 0 3 10 1 QC 08/30/10
135 98 8 SEC BUTYLBENZENE u ug/L 0 4 10 1 QC 08/30/10
98 06 6 TERT BUTYLBENZENE u ug/L 04 10 1 QC 08/30/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 08/30/10
56 23 5 CARBON TETRACHLORIDE 3 5 J ug/L 0 27 10 1 QC 08/30/10
108 90 7 CHLOROBENZENE 06 J ug/L 0 16 10 1 QC 08/30/10
75 00 3 CHLOROETHANE U ug/L 0 35 10 1 QC 08/30/10
110 75 8 2 CHLOROETHYLVINYL ETHER U ug/L 1 71 10 1 QC 08/30/10
67 66 3 CHLOROFORM 79 3 ug/L 0 3 10 1 QC 08/30/10
74 87 3 CHLOROMETHANE U ug/L 0 81 10 1 QC 08/30/10
95 49-8 2 CHLOROTOLUENE u ug/L 0 24 10 1 QC 08/30/10
106^3 4 4 CHLOROTOLUENE u ug/L 0 15 10 1 QC 08/30/10
124-48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 08/30/10
96 12 8 1 2 DIBROMO 3 CHLOROPROPANE u ug/L 0 35 10 1 QC 08/30/10
74 95 3 DIBROMOMETHANE u ug/L 0 25 10 1 QC 08/30/10
106 93 4 1 2 DIBROMOETHANE u ug/L 0 15 10 1 QC 08/30/10
95 50 1 1 2 DICHLOROBENZENE u ug/L 5 86 10 1 QC 08/30/10
541 73 1 1 3 DICHLOROBENZENE u ug/L 5 62 10 1 QC 08/30/10
106-46-7 1 4 DICHLOROBENZENE u ug/L 5 88 10 1 QC 08/30/10
75 71 8 DICHLORODIFLUOROMETHANE u ug/L 0 66 10 1 QC 08/30/10
75 34 3 1 1 DICHLOROETHANE 3 8 J ug/L 0 49 10 1 QC 08/30/10
107 06 2 1 2 DICHLOROETHANE 22 1 ug/L 0 29 10 1 QC 08/30/10
75 35 4 1 1 DICHLOROETHENE 59 ug/L 0 16 10 1 QC 08/30/10
156 59 4 CIS-1 2 DICHLOROETHENE 13 6 ug/L 0 16 10 1 QC 08/30/10
156-60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 QC 08/30/10
78 87 5 1 2 DICHLOROPROPANE U ug/L 0 16 10 1 QC 08/30/10
142 28 9 1 3 DICHLOROPROPANE U ug/L 0 24 10 1 QC 08/30/10
563 58 6 1 1 DICHLOROPROPENE U ug/L 0 17 10 1 QC 08/30/10
10061 01 5 CIS 1 3 DICHLOROPROPENE U ug/L 04 10 1 QC 08/30/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE U ug/L 04 10 1 QC 08/30/10
590 20 7 2 2 DICHLOROPROPANE U ug/L 09 10 1 QC 08/30/10
100-41 4 ETHYLBENZENE U ug/L 0 16 10 1 QC 08/30/10
591 78 6 2 HEXANONE U ug/L 07 10 1 QC 08/30/10
87 68 3 HEXACHLOROBUTADIENE U ug/L 0 9 10 1 QC 08/30/10
98 82 8 ISOPROPYLBEtvlZENE U ug/L 0 58 10 1 QC 08/30/10
99 87 6 4 ISOPROPYLTOLUENE u ug/L 0 24 10 1 QC 08/30/10
75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 08/30/10
108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 08/30/10
91 20 3 NAPHTHALENE u ug/L 4 10 1 QC 08/30/10
103-65 1 N PROPYLBENZENE u ug/L 0 5 10 1 QC 08/30/10
Pnnted
Page 3 of 5
09/10/10 11 18
Listing of Results by Sample
Sample Delivery Group 1008028
Client Sample ID D 6 Laboratory Sample ID 1008028 01
Sample Description ATK DLV Ground Water Fail 2010
Date Sampled 08/23/10 15 15
CAS Number Test Parameter Result Units MDL
Dilution
EQL Factor Analyst Test Date
TesfMef/iod SW 846, 8260S (Water) Volatile Organic Analysis
MDL
100 42 5 STYRENE U ug/L 0 3 10 1 QC 08/30/10
630 20 6 1112 TETRACHLOROETHANE U ug/L 0 25 10 1 QC 08/30/1 0
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 08/30/10
127 18-4 TETRACHLOROETHENE 4 6 J ug/L 0 4 10 1 QC 08/30/1 0
108 88 3 TOLUENE 1 1 J ug/L 0 5 10 1 QC 08/30/10
87 61-6 1 2 3 TRICHLOROBENZENE U ug/L 0 23 10 1 QC 08/30/10
120 82 1 1 2 4 TRICHLOROBENZENE U ug/L 4 37 10 1 QC 08/30/10
71 55 6 1 1 1 TRICHLOROETHANE 324 ug/L 0 16 10 1 QC 08/30/10
79 00 5 1 1 2 TRICHLOROETHANE 17 9 ug/L 0 25 10 1 QC 08/30/10
79 01 6 TRICHLOROETHENE 830 ug/L 7 100 10 QC 08/30/10
75 69-4 TRICHLOROFLUOROMETHANE 0 6 J ug/L 0 3 10 1 QC 08/30/10
96 18 4 1 2 3 TRICHLOROPROPANE U ug/L 0 33 10 1 QC 08/30/10
95 63 6 1 2 4-TRIMETHYLBENZENE U ug/L 0 19 10 1 QC 08/30/10
108 67 8 1 3 5 TRIMETHYLBENZENE U ug/L 0 29 10 1 QC 08/30/10
108 05 4 VINYL ACETATE U ug/L 20 50 1 QC 08/30/10
75 01 4 VINYL CHLORIDE u ug/L 03 10 1 QC 08/30/10
1330 20 7 m p XYLENE u ug/L 0 6 10 1 QC 08/30/10
95^7 6 0 XYLENE u ug/L 0 3 10 1 QC 08/30/10
460 00 4 BROMOFLUOROBENZENE 95 % 1 QC 08/30/10
1868 53 7 DIBROMOFLUOROMETHANE 92 % 1 QC 08/30/10
17060 07 0 1 2 DICHLOROETHANE D4 101 % 1 QC 08/30/10
2037 26 5 TOLUENE D8 97 % 1 QC 08/30/10
Pnnted
Page 4 of 5
09/10/10 11 18
Data Reporting Qualifiers
indicates that the analyte concentration is less than the MDL
This flag is used when an analyte is found in the blank as well as the sample
Indicates an extimated value This flag is used either when estimating a concentration
for tentatively identified compounds or when the data indicated the presence of a
compound that meets the identification critena but the result is less than the
EQL (eg 3 J with an EQL of 10)
MDL Method Detection Limit The minimum concentration of a substance that can be
confidently measured and reported The laboratory has demonstrated that the
MDL can be achieved in a laboratory reagent blank, but does not guarantee it
can be achieved in all sample matnces
EQL Estimated Quantitation Limit The EQL generally is 5 to 10 times the MDL For
many analytes the EQL is selected as the value of the lowest standard in the
calibration curve
Dilution Dilution Factor The prepared sample was diluted by this factor because the
Factor sample was too concentrated or due to other interferences in the sample matrix
Any dilution factor causes a corresponding increase in the MDL and EQL
Page 5 of 5
Pnnted 09/10/10 1118
ATK Launch Systems
Environmental Laboratory
Client Name
Sample Receipt Checklist
SDG No
Gamer Garner Number
XHand delivered no cooler • Hand delivered sample(s) taken out at receiving counter
l/902>OZb
Cooler Information
Cooler Number/ID
Condition of Shipping Container
Cooler Sealed (taped)
Custody Seals Present
•Good
DYes
•Yes
• Intact
Coolant nice
State of Coolant OFrozen
Thermometer ID /"i ^7iSfi Reading.
Packing Descnptlon
•Fair
•No
•No
•Broken
•Blue Ice •None
•Partially Frozen
9 C CF
j^ot Applicable
^^iNot Applicable
€(^ot Applicable
•Damaged (explain).
Seal Number ,
Other
•Melted
Cor'ected Temp _ Temp Blank Included DYes DNo
Chain-Of-Custody information
COC Present ^ . «
COC Nuinber(s) t li I nC/
COC signed (relinquished and received)
COC or LWi agrees witt) sample labels
•No
•No
•No
Other
•Not Applicable
•Not Applicable
Notes
Sample Information
Samples included In cooler
Custody Seals Present
Sample containers intact
Samples in proper containers
Sufficient sample volume
All samples received in hold time
•Yes
•Intact
^es
;j||Yes
iCi'es
Water - VOA s have zero headspace
P^re-preserved with HCl
Notes
^o
•Broken
•No
•No
•No
•No
jWes
Other
Seal Number(s).
Notes
• No
•Pre-preserved with NajSjOj
•Not Applicable
•Non-Preserved
Water - pH acceptable upon receipt DYes DAdjusted (see comments below) ^^ot Applicable
HNOj = H2SO4 = NaOH = ZnAC /NaOH •= HCL =
Water-pH adjusted (mfg & Lot No)
HNO3 HjSOi,
NajSOjOj Other,
Notes
NaOH ZnAC HCl
SOP-102 Form A C>&/^?//0
ENVIRONMENTAL LAB WORK REQUEST
^° ATK ENVIRONMENTAL LABORATORY LWRNo
Login No
E13201
FROM EXTENSION COST CENTER
8zoo
WORK ORDER DATE
ORGANIZATION MAIL STOP
3ol
REPORT RESULTS TO
HELEN RAVSTEN, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REIVIARKS SAMPLE DATE
G c
LOCATION TIME TEST REIVIARKS
f^iSln )JOt-Sz^o^ Ci-oH - VH O
fieffe-K /zstr I'L CX, u <^
Y-mo u ^( <i
X li^rov^y^\i:><'f\ /3Z0
5
6
7
8
9
10
II
12
CHAIN OF CUSTODY
^^J^^QUISHJ^D BY DATE TIME RECEIVED BY DATE TIME
l/fMiAAP/A.
FOR LABORATORY USE ONLY
DATE COMrLETED DATE REPORTED SIGNATURE
988P LS333 GW
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testmg Requested
Monday, October 18, 2010
TESTED FOR ATK DLV
Environmental Monitonng
Thiokol Corp, UT 84322
ANALYZED BY: ATK Launch Systems
Analytical Chemistry Laboratory
P O Box 707, M/S 245
Bngham City, UT 84302-0707
435-863-3732
435-863-8080
Contact Name
Project:
Sample Delivery Group.
Al Lee
Ground Water Testing - DLV
1010002
Page 1 of 10
Pnnted 10/18/10 1101
Sample Delivery Group 1010002
Sample No Client No Received Collect Date/Time
Test Requested Sample Description Matrix
1010002 01 Fish Spring 10/05/10 10/5/2010 12 45 00
EPA 314 0
SW-846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
1010002-02 Horse Spring 10/05/10 10/5/2010 12 55 00
EPA 314 0
SW846 8260B (Water)
Perchlorate - Ion Chromatography
Volatile Organic Analysis
Water
Water
1010002-03 Pipe Spring 10/05/10 10/5/2010 13 10 00
EPA 314 0
SW846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
1010002 04 Shotgun Spnng 10/05/10 10/5/2010 13 20 00
EPA 314 0
SW-846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
Certified By ^ 10/18/2010
W Scott Fraser, Quality Assurance Officer Date
This certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation
Program (NELAP) unless otherwise annotated
Page 2 of 10
Pnnted 10/18/101101
Listing of Results by Sample
Sample Delivery Group 1010002
Client Sample ID Fish Spnng Laboratory Sample ID 1010002 01
Date Sampled 10/05/10 12 45
Sample Description
Dilution
CAS Number Test Parameter Result Units MDL EQL Factor Analvst Test Date
Test Method EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE U ug/L 10 40 10 JMM 10/12/10
Test Method SW 846, S260B (Water) Volatile Organic Analysis
67 64 1 ACETONE U ug/L 5 10 1 PCI 10/07/10
71 43 2 BENZENE U ug/L 0 22 10 1 PCI 10/07/10
74 97 5 BROMOCHLOROMETHANE U ug/L 0 31 10 1 PCI 10/07/10
75 27 4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 PCI 10/07/10
108 86 1 BROMOBENZENE U ug/L 0 37 10 1 PCI 10/07/10
75 25 2 BROMOFORM u ug/L 0 42 10 1 PCI 10/07/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 PCI 10/07/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 PCI 10/07/10
104 51 8 N BUTYLBENZENE u ug/L 0 3 10 1 PCI 10/07/10
135 98 8 SEC BUTYLBENZENE u ug/L 0 4 10 1 PCI 10/07/10
98 06 6 TERT BUTYLBENZENE u ug/L 04 10 1 PCI 10/07/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 PCI 10/07/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 PCI 10/07/10
108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 PCI 10/07/10
75 00 3 CHLOROETHANE u ug/L 0 35 10 1 PCI 10/07/10
110 75 8 2 CHLOROETHYLVINYL ETHER u ug/L 1 71 10 1 PCI 10/07/10
67 66 3 CHLOROFORM u ug/L 0 3 10 1 PCI 10/07/10
74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 PCI 10/07/10
95 49 8 2 CHLOROTOLUENE u ug/L 0 24 10 1 PCI 10/07/10
106-43-4 4 CHLOROTOLUENE u ug/L 0 15 10 1 PCI 10/07/10
124-48-1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 PCI 10/07/10
96 12 8 1 2 DIBROMO 3 CHLOROPROPANE u ug/L 0 35 10 1 PCI 10/07/10
74 95 3 DIBROMOMETHANE u ug/L 0 25 10 1 PCI 10/07/10
106 93-4 1 2 DIBROMOETHANE u ug/L 0 15 10 1 PCI 10/07/10
95 50 1 1 2 DICHLOROBENZENE u ug/L 5 86 10 1 PCI 10/07/10
541 73 1 1 3 DICHLOROBENZENE u ug/L 5 62 10 1 PCI 10/07/10
106-46 7 1 4-DlCHLOROBENZENE u ug/L 5 88 10 1 PCI 10/07/10
75 71 8 DICHLORODIFLUOROMETHANE u ug/L 0 66 10 1 PCI 10/07/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 PCI 10/07/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 PCI 10/07/10
75 35-4 1 1 DICHLOROETHENE u ug/L 0 16 10 1 PCI 10/07/10
156 59-4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 PCI 10/07/10
156-60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 PCI 10/07/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 PCI 10/07/10
142 28 9 1 3 DICHLOROPROPANE u ug/L 0 24 10 1 PCI 10/07/10
563 58-6 1 1-DICHLOROPROPENE u ug/L 0 17 10 1 PCI 10/07/10
10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 PCI 10/07/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 PCI 10/07/10
590 20 7 2 2 DICHLOROPROPANE u ug/L 0 9 10 1 PCI 10/07/10
100-41 4 ETHYLBENZENE u ug/L 0 16 10 1 PCI 10/07/10
591 78 6 2 HEXANONE u ug/L 0 7 10 1 PCI 10/07/10
87 68 3 HEXACHLOROBUTADIENE u ug/L 0 9 10 1 PCI 10/07/10
98 82 8 ISOPROPYLBENZENE u ug/L 0 58 10 1 PCI 10/07/10
99 87 6 4 ISOPROPYLTOLUENE u ug/L 0 24 10 1 PCI 10/07/10
75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 PCI 10/07/10
108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 PCI 10/07/10
91 20 3 NAPHTHALENE u ug/L 4 10 1 PCI 10/07/10
103-65 1 N-PROPYLBENZENE u ug/L 0 5 10 1 PCI 10/07/10
Page 3 of 10
Pnnted 10/18/10 1101
Listing of Results by Sample
Sample Delivery Group 1010002
Ghent Sample ID Fish Spring Laboratory Sample ID 1010002-01
Sample Description
DateSampled 10/05/10 1245
CAS Number Test Parameter Result Units MDL
Dilution
EQL Factor Analvst Test Date
Test Method SW 846, 82606 (Water) Volatile Organic Analysis
MDL
100-42 5 STYRENE u ug/L 0 3 10 1 PCI 10/07/10
630 20 6 1112 TETRACHLOROETHANE u ug/L 0 25 10 1 PCI 10/07/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 PCI 10/07/10
127 18 4 TETRACHLOROETHENE u ug/L 04 10 1 PCI 10/07/10
108 88 3 TOLUENE u ug/L 0 5 10 1 PCI 10/07/10
87 61 6 1 2 3 TRICHLOROBENZENE u ug/L 0 23 10 1 PCI 10/07/10
120 82 1 1 2 4 TRICHLOROBENZENE u ug/L 4 37 10 1 PCI 10/07/10
71 55 6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 PCI 10/07/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 PCI 10/07/10
79 01 6 TRICHLOROETHENE u ug/L 0 7 10 1 PCI 10/07/10
75 69 4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 PCI 10/07/10
96 18-4 1 2 3 TRICHLOROPROPANE u ug/L 0 33 10 1 PCI 10/07/10
95 63 6 1 2 4 TRIMETHYLBENZENE u ug/L 0 19 10 1 PCI 10/07/10
108 67 8 1 3 5 TRIMETHYLBENZENE u ug/L 0 29 10 1 PCI 10/07/10
108 05 4 VINYL ACETATE u ug/L 20 50 1 PCI 10/07/10
75 01-4 VINYL CHLORIDE u ug/L 0 3 10 1 PCI 10/07/10
1330 20 7 nn p XYLENE u ug/L 0 6 10 1 PCI 10/07/10
95-47 6 0 XYLENE u ug/L 0 3 10 1 PCI 10/07/10
460 00 4 BROMOFLUOROBENZENE 108 % 1 PCI 10/07/10
1868 53 7 DIBROMOFLUOROMETHANE 98 6 % 1 PCI 10/07/10
17060 07 0 1 2 DICHLOROETHANE D4 104 % 1 PCI 10/07/10
2037 26 5 TOLUENE D8 97 1 % 1 PCI 10/07/10
Ghent Sample ID Horse Spring Laboratory Sample ID 1010002-02
Sample Description
Date Sampled 10/05/10 12 55
Dilution
GAS Number Test Parameter Result Units MDL EQL Factor Analvst Test Date
Test Method EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE U ug/L 10 40 10 JMM 10/12/10
Test Method SW846, S260B (Water) Volatile Organic Analysis
67 64 1 ACETONE U ug/L 5 10 1 PCI 10/07/10
71 43 2 BENZENE U ug/L 0 22 10 1 PCI 10/07/10
74 97 5 BROMOCHLOROMETHANE U ug/L 0 31 10 1 PCI 10/07/10
75 27-4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 PCI 10/07/10
108 86 1 BROMOBENZENE U ug/L 0 37 10 1 PCI 10/07/10
75 25 2 BROMOFORM U ug/L 0 42 10 1 PCI 10/07/10
74 83 9 BROMOMETHANE U ug/L 0 57 10 1 PCI 10/07/10
78 93 3 2 BUTANONE U ug/L 1 11 10 1 PCI 10/07/10
104 51 8 N BUTYLBENZENE U ug/L 0 3 10 1 PCI 10/07/10
135 98 8 SEC BUTYLBENZENE U ug/L 04 10 1 PCI 10/07/10
98 06 6 TERT BUTYLBENZENE U ug/L 04 10 1 PCI 10/07/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 PCI 10/07/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 PCI 10/07/10
108 90 7 CHLOROBENZENE 04J ug/L 0 16 10 1 PCI 10/07/10
75 00 3 CHLOROETHANE u ug/L 0 35 10 1 PCI 10/07/10
110 75-8 2 CHLOROETHYLVINYL ETHER u ug/L 1 71 10 1 PCI 10/07/10
67 66 3 CHLOROFORM u ug/L 0 3 10 1 PCI 10/07/10
74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 PCI 10/07/10
Page 4 of 10
Pnnted 10/18/10 1101
Listing of Results by Sample
Sample Delivery Group 1010002
Client Sample ID Horse Spnng Laboratory Sample ID 1010002 02
DateSampled 10/05/10 12 55
Sample Description
Dilution
GAS Number Test Parameter Result Units MDL EQL Factor Analvst Test Date
Tesf Method SIV 846, 82606 (Water) Volatile Organic Analysis
95-49 8 2 CHLOROTOLUENE u ug/L 0 24 10 1 PCI 10/07/10
106 43 4 4 CHLOROTOLUENE U ug/L 0 15 10 1 PCI 10/07/10
124-48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 PCI 10/07/10
96 12 8 1 2 DIBROMO 3 CHLOROPROPANE u ug/L 0 35 10 1 PCI 10/07/10
74 95 3 DIBROMOMETHANE u ug/L 0 25 10 1 PCI 10/07/10
106 93 4 1 2 DIBROMOETHANE u ug/L 0 15 10 1 PCI 10/07/10
95 50 1 1 2 DICHLOROBENZENE u ug/L 5 86 10 1 PCI 10/07/10
541 73 1 1 3 DICHLOROBENZENE u ug/L 5 62 10 1 PCI 10/07/10
106 46 7 1 4 DICHLOROBENZENE u ug/L 5 88 10 1 PCI 10/07/10
75 71 8 DICHLORODIFLUOROMETHANE u ug/L 0 66 10 1 PCI 10/07/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 PCI 10/07/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 PCI 10/07/10
75 35-4 1 1-DICHLOROETHENE u ug/L 0 16 10 1 PCI 10/07/10
156 59 4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 PCI 10/07/10
156-60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 PCI 10/07/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 PCI 10/07/10
142 28 9 1 3 DICHLOROPROPANE u ug/L 0 24 10 1 PCI 10/07/10
563 58 6 1 1-DICHLOROPROPENE u ug/L 0 17 10 1 PCI 10/07/10
10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 PCI 10/07/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 PCI 10/07/10
590 20 7 2 2 DICHLOROPROPANE u ug/L 09 10 1 PCI 10/07/10
100-41 4 ETHYLBENZENE u ug/L 0 16 10 1 PCI 10/07/10
591 78 6 2-HEXANONE u ug/L 07 10 1 PCI 10/07/10
87 68 3 HEXACHLOROBUTADIENE u ug/L 09 10 1 PCI 10/07/10
98 82 8 ISOPROPYLBENZENE u ug/L 0 58 10 1 PCI 10/07/10
99 87 6 4 ISOPROPYLTOLUENE u ug/L 0 24 10 1 PCI 10/07/10
75 09 2 METHYLENE CHLORIDE u ug/L 08 10 1 PCI 10/07/10
108 10 1 4 METHYL 2-PENTANONE u ug/L 0 53 10 1 PCI 10/07/10
91 20 3 NAPHTHALENE u ug/L 4 10 1 PCI 10/07/10
103 65 1 N PROPYLBENZENE u ug/L 05 10 1 PCI 10/07/10
100-42 5 STYRENE u ug/L 03 10 1 PCI 10/07/10
630 20 6 1112 TETRACHLOROETHANE u ug/L 0 25 10 1 PCI 10/07/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 PCI 10/07/10
127 18 4 TETRACHLOROETHENE u ug/L 04 10 1 PCI 10/07/10
108 88 3 TOLUENE u ug/L 0 5 10 1 PCI 10/07/10
87-61 6 1 2 3 TRICHLOROBENZENE u ug/L 0 23 10 1 PCI 10/07/10
120 82 1 1 2 4 TRICHLOROBENZENE u ug/L 4 37 10 1 PCI 10/07/10
71 55 6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 PCI 10/07/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 PCI 10/07/10
79 01-6 TRICHLOROETHENE 08J ug/L 07 10 1 PCI 10/07/10
75 69-4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 PCI 10/07/10
96 18-4 1 2 3 TRICHLOROPROPANE u ug/L 0 33 10 1 PCI 10/07/10
95-63-6 1 2 4 TRIMETHYLBENZENE u ug/L 0 19 10 1 PCI 10/07/10
108 67 8 1 3 5 TRIMETHYLBENZENE u ug/L 0 29 10 1 PCI 10/07/10
108 05 4 VINYL ACETATE u ug/L 20 50 1 PCI 10/07/10
75 01-4 VINYL CHLORIDE u ug/L 0 3 10 1 PCI 10/07/10
1330 20 7 mp XYLENE u ug/L 06 10 1 PCI 10/07/10
95-47 6 0 XYLENE u ug/L 0 3 10 1 PCI 10/07/10
460 00 4 BROMOFLUOROBENZENE 106 % 1 PCI 10/07/10
1868 53 7 DIBROMOFLUOROMETHANE 99 4 % 1 PCI 10/07/10
Page 5 of 10
Pnnted 10/18/10 1101
Listing of Results by Sample
Sample Delivery Group 1010002
Ghent Sample ID Horse Spnng
Sample Description
Laboratory Sample ID 1010002 02
Date Sampled 10/05/10 12 55
Dilution
GAS Number Test Parameter Result Units MDL EQL Factor Analvst Test Date
Tesf Method SW 846, 82606 (Water) Volatile Organic Analysis
17060 07 0 1 2 DICHLOROETHANE D4 105 % 1 PCI 10/07/10
2037 26 5 TOLUENE D8 96 7 % 1 PCI 10/07/10
Ghent Sample ID Pipe Spnng
Sample Description
Laboratory Sample ID 1010002 03
DateSampled 10/05/10 13 10
Dilution
GAS Number Test Parameter Result Units MDL IQk Factor Analvst Test Date
Test Method EPA 314 0 Perchlorate Ion Chromatography
014797 73-0 PERCHLORATE 265 ug/L 10 40 10 JMM 10/12/10
Tesf Method SIV 846, 8260S (Water) Volatile Organic Analysis
67 64 1 ACETONE U ug/L 5 10 1 PCI 10/07/10
71-43 2 BENZENE U ug/L 0 22 10 1 PCI 10/07/10
74 97 5 BROMOCHLOROMETHANE u ug/L 0 31 10 1 PCI 10/07/10
75 27-4 BROMODICHLOROMETHANE u ug/L 0 19 10 1 PCI 10/07/10
108 86 1 BROMOBENZENE u ug/L 0 37 10 1 PCI 10/07/10
75 25 2 BROMOFORM u ug/L 0 42 10 1 PCI 10/07/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 PCI 10/07/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 PCI 10/07/10
104 51 8 N BUTYLBENZENE u ug/L 0 3 10 1 PCI 10/07/10
135 98 8 SEC BUTYLBENZENE u ug/L 0 4 10 1 PCI 10/07/10
98 06-6 TERT BUTYLBENZENE u ug/L 04 10 1 PCI 10/07/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 PCI 10/07/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 PCI 10/07/10
108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 PCI 10/07/10
75 00 3 CHLOROETHANE u ug/L 0 35 10 1 PCI 10/07/10
110 75 8 2 CHLOROETHYLVINYL ETHER u ug/L 1 71 10 1 PCI 10/07/10
67-66 3 CHLOROFORM u ug/L 03 10 1 PCI 10/07/10
74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 PCI 10/07/10
95-49 8 2 CHLOROTOLUENE u ug/L 0 24 10 1 PCI 10/07/10
106-43 4 4 CHLOROTOLUENE u ug/L 0 15 10 1 PCI 10/07/10
124-48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 PCI 10/07/10
96 12 8 1 2 DIBROMO 3 CHLOROPROPANE u ug/L 0 35 10 1 PCI 10/07/10
74 95 3 DIBROMOMETHANE u ug/L 0 25 10 1 PCI 10/07/10
106 93-4 1 2 DIBROMOETHANE u ug/L 0 15 10 1 PCI 10/07/10
95 50 1 1 2 DICHLOROBENZENE u ug/L 5 86 10 1 PCI 10/07/10
541 73 1 1 3 DICHLOROBENZENE u ug/L 5 62 10 1 PCI 10/07/10
106 46 7 1 4 DICHLOROBENZENE u ug/L 5 88 10 1 PCI 10/07/10
76 71 8 DICHLORODIFLUOROMETHANE u ug/L 0 66 10 1 PCI 10/07/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 PCI 10/07/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 PCI 10/07/10
75 35-4 1 1 DICHLOROETHENE u ug/L 0 16 10 1 PCI 10/07/10
156 59 4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 PCI 10/07/10
156 60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 PCI 10/07/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 PCI 10/07/10
142 28 9 1 3 DICHLOROPROPANE u ug/L 0 24 10 1 PCI 10/07/10
563 58 6 1 1 DICHLOROPROPENE u ug/L 0 17 10 1 PCI 10/07/10
10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 PCI 10/07/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 0 4 10 1 PCI 10/07/10
Page 6 Of 10
Pnnted 10/18/10 1101
Listing of Results by Sample
Sample Delivery Group 1010002
Ghent Sample ID Pipe Spnng Laboratory Sample ID 1010002 03
Sample Description
Date Sampled 10/05/10 13 10
GAS Number Test Parameter Result Units MDL EQL
Dilution
Factor Analvst Test Date
Tesf Method SIV 846, 82606 (Water) Volatile Organic Analysis
MDL EQL
590 20 7 2 2 DICHLOROPROPANE U ug/L 0 9 10 1 PCI 10/07/10
100 41 4 ETHYLBENZENE U ug/L 0 16 10 1 PCI 10/07/10
591 78-6 2 HEXANONE U ug/L 07 10 1 PCI 10/07/10
87 68 3 HEXACHLOROBUTADIENE U ug/L 0 9 10 1 PCI 10/07/10
98 82 8 ISOPROPYLBENZENE U ug/L 0 58 10 1 PCI 10/07/10
99 87 6 4 ISOPROPYLTOLUENE U ug/L 0 24 10 1 PCI 10/07/10
75 09 2 METHYLENE CHLORIDE U ug/L 0 8 10 1 PCI 10/07/10
108 10 1 4 METHYL 2 PENTANONE U ug/L 0 53 10 1 PCI 10/07/10
91 20 3 NAPHTHALENE U ug/L 4 10 1 PCI 10/07/10
103 65 1 N PROPYLBENZENE u ug/L 0 5 10 1 PCI 10/07/10
100-42 5 STYRENE u ug/L 0 3 10 1 PCI 10/07/10
630 20 6 1112 TETRACHLOROETHANE u ug/L 0 25 10 1 PCI 10/07/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 PCI 10/07/10
127 18 4 TETRACHLOROETHENE u ug/L 04 10 1 PCI 10/07/10
108 88 3 TOLUENE u ug/L 05 10 1 PCI 10/07/10
87-61-6 1 2 3-TRICHLOROBENZENE u ug/L 0 23 10 1 PCI 10/07/10
120 82 1 1 2 4 TRICHLOROBENZENE u ug/L 4 37 10 1 PCI 10/07/10
71 55 6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 PCI 10/07/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 PCI 10/07/10
79 01 6 TRICHLOROETHENE 5 3 J ug/L 07 10 1 PCI 10/07/10
75 69-4 TRICHLOROFLUOROMETHANE U ug/L 0 3 10 1 PCI 10/07/10
96 18-4 1 2 3 TRICHLOROPROPANE U ug/L 0 33 10 1 PCI 10/07/10
95 63 6 1 2 4 TRIMETHYLBENZENE U ug/L 0 19 10 1 PCI 10/07/10
108 67 8 1 3 5 TRIMETHYLBENZENE U ug/L 0 29 10 1 PCI 10/07/10
108 05-4 VINYL ACETATE U ug/L 20 50 1 PCI 10/07/10
75 01-4 VINYL CHLORIDE u ug/L 03 10 1 PCI 10/07/10
1330 20 7 m p XYLENE u ug/L 06 10 1 PCI 10/07/10
95-47 6 0 XYLENE u ug/L 0 3 10 1 PCI 10/07/10
460 00-4 BROMOFLUOROBENZENE 107 % 1 PCI 10/07/10
1868 53 7 DIBROMOFLUOROMETHANE 99 6 % 1 PCI 10/07/10
17060 07 0 1 2 DICHLOROETHANE D4 107 % 1 PCI 10/07/10
2037 26 5 TOLUENE D8 96 3 % 1 PCI 10/07/10
Ghent Sample ID Shotgun Spnng Laboratory Sample ID 1010002 04
Sample Description
Date Sampled 10/05/10 13 20
CAS Number Test Parameter Result Units MDL EQL
Dilution
Factor Analvst Test Date
Test Method EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE 92 ug/L 10 40 10 JMM 10/12/10
TesfMef/iod SW 846, S260B (Water) Volatale Organic Analysis
67 64 1 ACETONE U ug/L 5 10 1 PCI 10/07/10
71-43 2 BENZENE U ug/L 0 22 10 1 PCI 10/07/10
74 97 5 BROMOCHLOROMETHANE U ug/L 0 31 10 1 PCI 10/07/10
75 27-4 BROMODICHLOROMETHANE u ug/L 0 19 10 1 PCI 10/07/10
108 86 1 BROMOBENZENE u ug/L 0 37 10 1 PCI 10/07/10
75 25 2 BROMOFORM u ug/L 0 42 10 1 PCI 10/07/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 PCI 10/07/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 PCI 10/07/10
Page 7 of 10
Pnnted 10/18/10 1101
Listing of Results by Sample
Sample Delivery Group 1010002
Ghent Sample ID Shotgun Spnng
Sample Description
Laboratory Sample ID
Date Sampled
1010002 04
10/05/10 13 20
GAS Number
Tesf Mefhod
104 51 8
135 98 8
98 06-6
75 15 0
56 23 5
108 90 7
75 00 3
110 75 8
67 66 3
74 87 3
95-49 8
106-43 4
124 48 1
96 12 8
74 95 3
106 93 4
95 50 1
541 73 1
106-46 7
75 71 8
75 34 3
107 06 2
75 35-4
156 59-4
156 60 5
78 87 5
142 28 9
563 58 6
10061 01 5
10061 02 6
590 20 7
100-41 4
591 78 6
87 68 3
98 82 8
99 87-6
75 09 2
108 10 1
91 20 3
103 65 1
100-42 5
630 20 6
79 34 5
127 18 4
108 88 3
87 61-6
120 82 1
71 55 6
79 00 5
79 01 6
Test Parameter
SW 846, 82606 (Wafer;
Result
Volatile Organic Analysis
Units
N BUTYLBENZENE
SEC BUTYLBENZENE
TERT BUTYLBENZENE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
2 CHLOROETHYLVINYL ETHER
CHLOROFORM
CHLOROMETHANE
2 CHLOROTOLUENE
4 CHLOROTOLUENE
DIBROMOCHLOROMETHANE
1 2 DIBROMO 3 CHLOROPROPANE
DIBROMOMETHANE
1 2 DIBROMOETHANE
1 2 DICHLOROBENZENE
1 3 DICHLOROBENZENE
1 4 DICHLOROBENZENE
DICHLORODIFLUOROMETHANE
1 1 DICHLOROETHANE
1 2 DICHLOROETHANE
1 1 DICHLOROETHENE
CIS-1 2 DICHLOROETHENE
TRANS 1 2 DICHLOROETHENE
1 2 DICHLOROPROPANE
1 3 DICHLOROPROPANE
1 1 DICHLOROPROPENE
CIS 1 3 DICHLOROPROPENE
TRANS 1 3 DICHLOROPROPENE
2 2 DICHLOROPROPANE
ETHYLBENZENE
2 HEXANONE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
4 ISOPROPYLTOLUENE
METHYLENE CHLORIDE
4 METHYL 2 PENTANONE
NAPHTHALENE
N PROPYLBENZENE
STYRENE
1112 TETRACHLOROETHANE
112 2 TETRACHLOROETHANE
TETRAC HLOROETHENE
TOLUENE
1 2 3 TRICHLOROBENZENE
1 2 4 TRICHLOROBENZENE
1 1 1 TRICHLOROETHANE
1 1 2 TRICHLOROETHANE
TRICHLOROETHENE
U
U
U
U
U
0 4 J
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
J 5 9
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
MDL
03
0 4
0 4
0 13
0 27
0 16
0 35
1 71
0 3
0 81
0 24
0 15
0 18
0 35
0 25
0 15
5 86
5 62
5 88
0 66
0 49
0 29
0 16
0 16
0 34
0 16
0 24
0 17
04
04
0 9
0 16
07
0 9
0 58
0 24
0 8
0 53
4
0 5
0 3
0 25
0 85
04
0 5
0 23
4 37
0 16
0 25
0 7
Dilution
EQL Factor Analvst Test Date
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
PCI 10/07/10
Page 8 of 10
Pnnted 10/18/10 1101
Listing of Results by Sample
Sample Delivery Group 1010002
Client Sample ID Shotgun Spnng Laboratory Sample ID 1010002 04
Sample Description
Date Sampled 10/05/10 13 20
CAS Number Test Parameter Result Units MDL
Dilution
EQL Factor Analvst Test Date
Tesf Method SW 846, 82606 (Wafer) Volatile Organic Analysis
75 69-4 TRICHLOROFLUOROMETHANE U ug/L 0 3 10 1 PCI 10/07/10
96 18 4 1 2 3 TRICHLOROPROPANE U ug/L 0 33 10 1 PCI 10/07/10
95 63-6 1 2 4 TRIMETHYLBENZENE u ug/L 0 19 10 1 PCI 10/07/10
108 67 8 1 3 5 TRIMETHYLBENZENE u ug/L 0 29 10 1 PCI 10/07/10
108 05 4 VINYL ACETATE u ug/L 20 50 1 PCI 10/07/10
75 01 4 VINYL CHLORIDE u ug/L 0 3 10 1 PCI 10/07/10
1330 20 7 m p XYLENE u ug/L 06 10 1 PCI 10/07/10
95-47-6 0-XYLENE u ug/L 0 3 10 1 PCI 10/07/10
460 00 4 BROMOFLUOROBENZENE 111 % 1 PCI 10/07/10
1868 53 7 DIBROMOFLUOROMETHANE 98 8 % 1 PCI 10/07/10
17060 07 0 1 2 DICHLOROETHANE D4 104 % 1 PCI 10/07/10
2037 26 5 TOLUENE D8 99 3 % 1 PCI 10/07/10
Page 9 Of 10
Pnnted 10/18/10 1101
Data Reporting Qualifiers
U Indicates that the analyte concentration is less than the MDL
B This flag is used when an analyte is found in the blank as well as the sample
indicates an extimated value This flag is used either when estimating a concentration
for tentatively identified compounds or when the data indicated the presence of a
compound that meets the identification criteria but the result is less than the
EQL (e g 3 J with an EQL of 10)
MDL Method Detection Limit The minimum concentration of a substance that can be
confidently measured and reported The laboratory has demonstrated that the
MDL can be achieved in a laboratory reagent blank, but does not guarantee it
can be achieved in all sample matnces
EQL Estimated Quantitation Limit The EQL generally is 5 to 10 times the MDL For
many analytes the EQL is selected as the value of the lowest standard in the
calibration curve
Dilution Dilution Factor The prepared sample was diluted by this factor because the
Factor sample was too concentrated or due to other interferences in the sample matrix
Any dilution factor causes a corresponding increase in the MDL and EQL
Page 10 of 10
Pnnted 10/18/10 1101
ATK Launch Systems
Environmental Laboratory
Client Name _
Sample Receipt Checklist
SDG No
Carrier
C Hand delivered no cooler
Gamer Number
Hand delivered sample{s) taken out at receiving counter
{OlOOOT^
Cooler Information
Cooler Number/ID
Condition of Shipping Container ^fGood
Cooler Sealed (taped) DYes
Custody Seals Present DYes
•Intact
Coolant Clce
State of Caolanl • Frozen
Thermometer ID Reading _
Packing Description
•Fair
•No
•No
C Broken
• Blue Ice ONone
•Partially Frozen
3^ C CF •
•Not Applicable
J^/I^Q^ Applicable
^l^t Applicable
•Damaged (explain)
Seal Number
Other
•Melted
Corrected Temp "^"^'C Temp Blank Included DYes
Chain Of Custody Information
COC Present tl\1.tnl JS^es
COC Number(s) 11 gZ-P' .
COC signed (relinquished and received) ^^s
COC or LWI agrees with sample labels >Yes
Other .
CNo
• No
•Not Applicable
•Not Applicable
Sample Information
Samples included in cooler fv^A ^pri*^,\it>f^e $f>fim. ?}f>£.f^yij , ^o4-jU(/\ ^/7Vt^
Custody Seals Present
Sample containers Intact
Samples in proper containers
Sufficient sample volume
All samples received in hold time
DYes
•Intact
j?^s
pYes
yies
Water - VOAs have zero headspace
^re-preserved with HCl
Notes
Other
Seal Number(E).
Notes
gpffo
•Broken
•No
•No
•No
•No
•Yes fi/do • Not Applicable
• Pre-preserved with Na2S20] •NorvPreserved
Water - pH acceptable upon receipt DYes OAdjustad (see comments below) Bflol Applicable
HNO3 = HjSO^ = NaOH = ZnAC /NaOH = HCL =
Water pH adjusted (mfg & Lot No )
HNOj HjSO. .
NajSOzOs Other _
Notes
NaOH ZnAC HCl
SOP-102Form A
ENVIRONMENTAL LAB WORK REQUEST
1010005
™ ATK ENVIRONMENTAL LABORATORY LWR No
Login No
E13202
FROM
/il/cv\ Lcc
EXTENSION COST CENTER WORK ORDER ^^3?
ORCANIZATION MAIL STOP REPORT RESULTS TO
HELEN RAVSTEN, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS SAMPLE DATE
G c
LOCATION TIME TEST REMARKS
Y
X /rr^»yk>t\/vft^ \\^
/
J K « <•> n
;f U (( If t(
^ ^-J ll 11 ll V
6
7
S
9
10
11
12
CHAIN OF CUSTODY
R)tC^UISHEDB« DATE TIME RECEIVED BY DATE TIME
/Sso
FOR LABORATORY USE ONLY
DATE COMPLETED DATE KEFORTED SIGNATURE
988P LS333 GW
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Requested
Monday, October 18, 2010
TESTED FOR ATK DLV
Environmental Monitonng
Thiokol Corp, UT 84322
ANALYZED BY ATK Launch Systems
Analytical Chemistry Laboratory
P O Box 707, M/S 245
Bngham City, UT 84302-0707
435-863-3732
435-863-8080
Contact Name
Project-
Sample Delivery Group
Al Lee
Ground Water Testing - DLV
1010005
Page 1 of 9
Pnnted 10/18/10 1101
Sample Delivery Group 1010005
Sample No Client No Received Collect Date/Time
Test Requested Sample Description Matrix
1010005 01 J7 10/07/10 10/7/2010 11 15 00
EPA 314 0
SW846 8260B (Water)
Perchlorate Ion Ctiromatography
Volatile Organic Analysis
Water
Water
1010005 02 I-F2 10/07/10 10/7/2010 11 50 00
EPA 314 0
SW846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
1010005 03 E5 10/07/10 10/7/2010 12 40 00
EPA 314 0
SW 846 8280B (Water)
Perchlorate - Ion Chromatography
Volatile Organic Analysis
Water
Water
1010005 04 E6 10/07/10 10/7/2010 13 00 00
EPA 314 0
SW846 82608 (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Wafer
1010005 05 G-3 10/07/10 10/7/2010 13 40 00
EPA 314 0 Perchlorate Ion Chromatography Water
Page 2 of 9
Pnnted 10/18/10 1101
Sample Delivery Group 1010005
Sample No Client No
Test Requested Sample Description
Received Collect Date/Time
Matrix
1010005-05 G 3 10/07/10 10/7/2010 13 40 00
SW 846 8260B (Water) Volatile Organic Analysis Water
Certified By 10/18/2010
W Scott Fraser, Quality Assurance Officer Date
This certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation
Program (NELAP) unless otherwise annotated
Page 3 of 9
Pnnted 10/18/101101
Listing of Results by Sample
Sample Delivery Group 1010005
Client Sarnple ID J 7 Laboratory Sample ID 1010005 01
DateSampled 10/07/10 1115
Sample Description
Dilution
CAS Number Test Parameter Result Units MDL Factor Analvst Test Date
Tesf Method EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE 518 ug/L 10 40 10 JMM 10/12/10
Test Method SIV 846 8260S (Wafer; Volatile Organic Analysis
67-64 1 ACETONE U ug/L 5 10 1 QC 10/11/10
107 02 8 ACROLEIN U ug/L 6 10 1 QC 10/11/10
71-43 2 BENZENE u ug/L 0 22 10 1 QC 10/11/10
75 27 4 BROMODICHLOROMETHANE u ug/L 0 19 10 1 QC 10/11/10
75 25 2 BROMOFORM u ug/L 0 42 10 1 QC 10/11/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 10/11/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 10/11/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 10/11/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 10/11/10
108 90 7 CHLOROBENZENE 0 3 J ug/L 0 16 10 1 QC 10/11/10
75-00-3 CHLOROETHANE U ug/L 0 35 10 1 QC 10/11/10
67 66 3 CHLOROFORM U ug/L 0 3 10 1 QC 10/11/10
74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 10/11/10
124 48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 10/11/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 10/11/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 10/11/10
75 35-4 1 1 DICHLOROETHENE 57 J ug/L 0 16 10 1 QC 10/11/10
156 59 4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 10/11/10
156-60 5 TRANS 1 2 DICHLOROETHENE U ug/L 0 34 10 1 QC 10/11/10
78 87 5 1 2 DICHLOROPROPANE U ug/L 0 16 10 1 QC 10/11/10
10061 01 5 CIS 1 3-DICHLOROPROPENE U ug/L 04 10 1 QC 10/11/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE U ug/L 04 10 1 QC 10/11/10
100-41 4 ETHYLBENZENE U ug/L 0 16 10 1 QC 10/11/10
591-78 6 2 HEXANONE U ug/L 07 10 1 QC 10/11/10
75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 10/11/10
108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 10/11/10
100-42 5 STYRENE u ug/L 0 3 10 1 QC 10/11/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 10/11/10
127-18 4 TETRACHLOROETHENE u ug/L 04 10 1 QC 10/11/10
108 88 3 TOLUENE u ug/L 0 5 10 1 QC 10/11/10
71 55 6 1 1 1-TRICHLOROETHANE 35J ug/L 0 16 10 1 QC 10/11/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 10/11/10
79 01 6 TRICHLOROETHENE 40 4 ug/L 07 10 1 QC 10/11/10
75-69-4 TRICHLOROFLUOROMETHANE U ug/L 0 3 10 1 QC 10/11/10
108 05 4 VINYL ACETATE U ug/L 20 50 1 QC 10/11/10
75 01-4 VINYL CHLORIDE U ug/L 0 3 10 1 QC 10/11/10
1330 20 7 m p XYLENE u ug/L 06 10 1 QC 10/11/10
95-47 6 0 XYLENE u ug/L 0 3 10 1 QC 10/11/10
17060 07 0 1 2 DICHLOROETHANE D4 105 % 1 QC 10/11/10
460 00 4 BROMOFLUOROBENZENE 103 % 1 QC 10/11/10
2037 26 5 TOLUENE D8 97 2 % 1 QC 10/11/10
1868 53 7 DIBROMOFLUOROMETHANE 101 % 1 QC 10/11/10
Pnnted
Page 4 of 9
)0/J8/10 11 01
Listing of Results by Sample
Sample Delivery Group 1010005
Client Sample ID LF 2
Sample Description
Laboratory Sample ID 1010005 02
Date Sampled 10/07/10 11 50
AS Number Test Parameter Result Units MDL EQL
Dilution
Factor Analvst Test Date
Tesf Method EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE U ug/L 10 40 10 JMM 10/12/10
Tesf Method SIV 846, 82606 (Water) Volatile Organic Analysis
67-64 1 ACETONE U ug/L 5 10 1 QC 10/11/10
107 02 8 ACROLEIN U ug/L 6 10 1 QC 10/11/10
71 43 2 BENZENE U ug/L 0 22 10 1 QC 10/11/10
75 27 4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 10/11/10
75-25 2 BROMOFORM u ug/L 0 42 10 1 QC 10/11/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 10/11/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 10/11/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 10/11/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 10/11/10
108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 QC 10/11/10
75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 10/11/10
67 66 3 CHLOROFORM u ug/L 0 3 10 1 QC 10/11/10
74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 10/11/10
124^8 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 10/11/10
75 34 3 1 1 DICHLOROETHANE 1 6 J ug/L 0 49 10 1 QC 10/11/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 10/11/10
75 35 4 1 1 DICHLOROETHENE u ug/L 0 16 10 1 QC 10/11/10
156-59 4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 10/11/10
156 60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 QC 10/11/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 10/11/10
10061-01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 10/11/10
10061-02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 10/11/10
100-41-4 ETHYLBENZENE u ug/L 0 16 10 1 QC 10/11/10
591 78-6 2 HEXANONE u ug/L 07 10 1 QC 10/11/10
75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 10/11/10
108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 10/11/10
100-42 5 STYRENE u ug/L 0 3 10 1 QC 10/11/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 10/11/10
127 18-4 TETRACHLOROETHENE u ug/L 04 10 1 QC 10/11/10
108 88 3 TOLUENE u ug/L 0 5 10 1 QC 10/11/10
71-55 6 1 1 1 TRICHLOROETHANE 11J ug/L 0 16 10 1 QC 10/11/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 10/11/10
79 01 6 TRICHLOROETHENE u ug/L 07 10 1 QC 10/11/10
75 69-4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 10/11/10
108 05^ VINYL ACETATE u ug/L 20 50 1 QC 10/11/10
75 01 4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 10/11/10
1330 20 7 m p XYLENE u ug/L 06 10 1 QC 10/11/10
95^7 6 0 XYLENE u ug/L 0 3 10 1 QC 10/11/10
17060 07 0 1 2 DICHLOROETHANE D4 105 % 1 QC 10/11/10
460 00 4 BROMOFLUOROBENZENE 102 % 1 QC 10/11/10
2037 26 5 TOLUENE D8 97 1 % 1 QC 10/11/10
1868 53 7 DIBROMOFLUOROMETHANE 100 % 1 QC 10/11/10
Pnnted
Page 5 of 9
10/18/10 11 01
Listing of Results by Sample
Sample Delivery Group 1010005
Client Sample ID E5 Laboratory Sample ID 1010005 03
DateSampled 10/07/10 1240
Sample Description
Dilution
CAS Number Test Parameter Result Units MDL EQL Factor Analvst Test Date
TesfMef/iod EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE 57 ug/L 10 40 10 JMM 10/12/10
Tesf Method SIV 846, 8260B (Water) Volatile Organic Analysis
67 64 1 ACETONE U ug/L 5 10 1 QC 10/11/10
107 02 8 ACROLEIN U ug/L 6 10 1 QC 10/11/10
71-43 2 BENZENE U ug/L 0 22 10 1 QC 10/11/10
75 27 4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 10/11/10
75 25 2 BROMOFORM u ug/L 0 42 10 1 QC 10/11/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 10/11/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 10/11/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 10/11/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 10/11/10
108-90 7 CHLOROBENZENE u ug/L 0 16 10 1 QC 10/11/10
75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 10/11/10
67-66 3 CHLOROFORM 75J ug/L 0 3 10 1 QC 10/11/10
74-87 3 CHLOROMETHANE U ug/L 0 81 10 1 QC 10/11/10
124-48 1 DIBROMOCHLOROMETHANE U ug/L 0 18 10 1 QC 10/11/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 10/11/10
107 06-2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 10/11/10
75 35 4 1 1 DICHLOROETHENE u ug/L 0 16 10 1 QC 10/11/10
156 59 4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 10/11/10
156-60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 QC 10/11/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 10/11/10
10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 10/11/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 0 4 10 1 QC 10/11/10
100-41 4 ETHYLBENZENE u ug/L 0 16 10 1 QC 10/11/10
591 78 6 2 HEXANONE u ug/L 0 7 10 1 QC 10/11/10
75-09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 10/11/10
108 10 1 4 METHYL 2-PENTANONE u ug/L 0 53 10 1 QC 10/11/10
100-42 5 STYRENE u ug/L 0 3 10 1 QC 10/11/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 10/11/10
127 18-4 TETRACHLOROETHENE u ug/L 04 10 1 QC 10/11/10
108 88 3 TOLUENE u ug/L 0 5 10 1 QC 10/11/10
71-55-6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 10/11/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 10/11/10
79 01 6 TRICHLOROETHENE 40 9 ug/L 07 10 1 QC 10/11/10
75 69 4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 10/11/10
108 05 4 VINYL ACETATE u ug/L 20 50 1 QC 10/11/10
75 01-4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 10/11/10
1330 20 7 m p XYLENE u ug/L 0 6 10 1 QC 10/11/10
95-47-6 0 XYLENE u ug/L 0 3 10 1 QC 10/11/10
17060 07 0 1 2 DICHLOROETHANE D4 106 % 1 QC 10/11/10
460 00-4 BROMOFLUOROBENZENE 100 % 1 QC 10/11/10
2037 26 5 TOLUENE D8 96 7 % 1 QC 10/11/10
1868-53 7 DIBROMOFLUOROMETHANE 97 2 % 1 QC 10/11/10
Pnnted
Page 6 of 9
10/18/10 11 01
Listing of Results by Sample
Sample Delivery Group 1010005
Client Sample ID E6 Laboratory Sample ID 1010005 04
Date Sampled 10/07/10 13 00
Sample Description
Dilution
CAS Number Test Parameter Result Units MDL Factor Analvst Test Date
Tesf Method EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE 51 ug/L 5 20 5 JMM 10/12/10
Tesf Method SIV 846, 8260S (Wafer; Volatile Organic Analysis
67 64 1 ACETONE U ug/L 5 10 1 QC 10/11/10
107 02 8 ACROLEIN U ug/L 6 10 1 QC 10/11/10
71-43 2 BENZENE U ug/L 0 22 10 1 QC 10/11/10
75 27 4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 10/11/10
75 25 2 BROMOFORM U ug/L 0 42 10 1 QC 10/11/10
74 83 9 BROMOMETHANE U ug/L 0 57 10 1 QC 10/11/10
78 93 3 2 BUTANONE U ug/L 1 11 10 1 QC 10/11/10
75 15 0 CARBON DISULFIDE 04 J ug/L 0 13 10 1 QC 10/11/10
56 23 5 CARBON TETRACHLORIDE U ug/L 0 27 10 1 QC 10/11/10
108 90 7 CHLOROBENZENE 03 J ug/L 0 16 10 1 QC 10/11/10
75 00 3 CHLOROETHANE U ug/L 0 35 10 1 QC 10/11/10
67-66-3 CHLOROFORM 3 9 J ug/L 0 3 10 1 QC 10/11/10
74 87 3 CHLOROMETHANE U ug/L 0 81 10 1 QC 10/11/10
124-48 1 DIBROMOCHLOROMETHANE U ug/L 0 18 10 1 QC 10/11/10
75 34 3 1 1 DICHLOROETHANE U ug/L 0 49 10 1 QC 10/11/10
107 06 2 1 2 DICHLOROETHANE U ug/L 0 29 10 1 QC 10/11/10
75 35-4 1 1 DICHLOROETHENE 2 3 J ug/L 0 16 10 1 QC 10/11/10
156 59-4 CIS 1 2 DICHLOROETHENE U ug/L 0 16 10 1 QC 10/11/10
156 60-5 TRANS 1 2 DICHLOROETHENE U ug/L 0 34 10 1 QC 10/11/10
78 87 5 1 2 DICHLOROPROPANE U ug/L 0 16 10 1 QC 10/11/10
10061 01 5 CIS 1 3 DICHLOROPROPENE U ug/L 04 10 1 QC 10/11/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE U ug/L 04 10 1 QC 10/11/10
100^1 4 ETHYLBENZENE U ug/L 0 16 10 1 QC 10/11/10
591 78 6 2 HEXANONE U ug/L 0 7 10 1 QC 10/11/10
75 09 2 METHYLENE CHLORIDE U ug/L 0 8 10 1 QC 10/11/10
108 10 1 4 METHYL 2 PENTANONE U ug/L 0 53 10 1 QC 10/11/10
100-42 5 STYRENE U ug/L 0 3 10 1 QC 10/11/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 10/11/10
127 18 4 TETRACHLOROETHENE u ug/L 04 10 1 QC 10/11/10
108 88 3 TOLUENE u ug/L 0 5 10 1 QC 10/11/10
71 55 6 1 1 1-TRICHLOROETHANE 06 J ug/L 0 16 10 1 QC 10/11/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 10/11/10
79 01 6 TRICHLOROETHENE 28 1 ug/L 07 10 1 QC 10/11/10
75-69-4 TRICHLOROFLUOROMETHANE U ug/L 0 3 10 1 QC 10/11/10
108 05 4 VINYL ACETATE U ug/L 20 50 1 QC 10/11/10
75 01-4 VINYL CHLORIDE U ug/L 0 3 10 1 QC 10/11/10
1330 20 7 m p XYLENE U ug/L 06 10 1 QC 10/11/10
95-47-6 0 XYLENE U ug/L 0 3 10 1 QC 10/11/10
17060 07 0 1 2 DICHLOROETHANE D4 107 % 1 QC 10/11/10
460 00-4 BROMOFLUOROBENZENE 103 % 1 QC 10/11/10
2037 26 5 TOLUENE D8 99 3 % 1 QC 10/11/10
1868 53-7 DIBROMOFLUOROMETHANE 102 % 1 QC 10/11/10
Pnnted
Page 7 of 9
10/18/10 11 01
Listing of Results by Sample
Sample Delivery Group 1010005
Client Sample ID G 3 Laboratory Sample ID 1010005 05
Date Sampled 10/07/10 13 40
Sample Description
Dilution
CAS Number Test Parameter Result Units MDL EQL Factor Analvst Test Date
Tesf Method EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE U ug/L 10 40 10 JMM 10/12/10
Tesf Method SIV 846, 8260B (Wafer; Volatile Organic Analysis
67 64 1 ACETONE U ug/L 5 10 1 QC 10/11/10
107 02 8 ACROLEIN U ug/L 6 10 1 QC 10/11/10
71^3-2 BENZENE U ug/L 0 22 10 1 QC 10/11/10
75 27-4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 10/11/10
75 25 2 BROMOFORM U ug/L 0 42 10 1 QC 10/11/10
74 83 9 BROMOMETHANE U ug/L 0 57 10 1 QC 10/11/10
78 93 3 2 BUTANONE U ug/L 1 11 10 1 QC 10/11/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 10/11/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 10/11/10
108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 QC 10/11/10
75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 10/11/10
67 66 3 CHLOROFORM u ug/L 0 3 10 1 QC 10/11/10
74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 10/11/10
124^8 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 10/11/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 10/11/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 10/11/10
75 35-4 1 1 DICHLOROETHENE u ug/L 0 16 10 1 QC 10/11/10
156-59 4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 10/11/10
156 60 5 TRANS 1 2-DICHLOROETHENE u ug/L 0 34 10 1 QC 10/11/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 10/11/10
10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 10/11/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 10/11/10
100 41 4 ETHYLBENZENE u ug/L 0 16 10 1 QC 10/11/10
591 78 6 2 HEXANONE u ug/L 0 7 10 1 QC 10/11/10
75 09-2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 10/11/10
108 10 1 4 METHYL 2-PENTANONE u ug/L 0 53 10 1 QC 10/11/10
100-42 5 STYRENE u ug/L 0 3 10 1 QC 10/11/10
79 34-5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 10/11/10
127 18-4 TETRACHLOROETHENE u ug/L 0 4 10 1 QC 10/11/10
108 88 3 TOLUENE u ug/L 0 5 10 1 QC 10/11/10
71 55 6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 10/11/10
79 00-5 1 1 2-TRICHLOROETHANE u ug/L 0 25 10 1 QC 10/11/10
79 01 6 TRICHLOROETHENE u ug/L 0 7 10 1 QC 10/11/10
75 69-4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 10/11/10
108 05 4 VINYL ACETATE u ug/L 20 50 1 QC 10/11/10
75 01-4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 10/11/10
1330 20 7 m p XYLENE u ug/L 06 10 1 QC 10/11/10
95 47 6 0 XYLENE u ug/L 0 3 10 1 QC 10/11/10
17060 07 0 1 2 DICHLOROETHANE D4 103 % 1 QC 10/11/10
460 00 4 BROMOFLUOROBENZENE 103 % 1 QC 10/11/10
2037 26 5 TOLUENE D8 97 2 % 1 QC 10/11/10
1868 53 7 DIBROMOFLUOROMETHANE 102 % 1 QC 10/11/10
Pnnted
Page 8 of 9
10/18/10 11 01
Data Reporting Qualifiers
U Indicates that the analyte concentration is less than the MDL
B This flag is used when an analyte is found in the blank as well as the sample
Indicates an extimated value This flag is used either when estimating a concentration
for tentatively identified compounds or when the data indicated the presence of a
compound that meets the identification criteria but the result is less than the
EQL (e g 3 J with an EQL of 10)
MDL Method Detection Limit The minimum concentration of a substance that can be
confidently measured and reported The laboratory has demonstrated that the
MDL can be achieved in a laboratory reagent blank, but does not guarantee it
can be achieved in all sample matnces
EQL Estimated Quantitation Limit The EQL generally is 5 to 10 times the MDL For
many analytes the EQL is selected as the value of the lowest standard in the
calibration curve
Dilution Dilution Factor The prepared sample was diluted by this factor because the
Factor sample was too concentrated or due to other interferences in the sample matnx
Any dilution factor causes a corresponding increase in the MDL and EQL
Page 9 of 9
Pnnted 10/18/10 1101
ATK Launch Systems
Environmental Laboratory
Client Name Ou/
Garner
Sample Receipt Checklist
SDG No
Camer Number
• Hand delivered no cooler jyftand delivered sample(5) taken out at receiving counter
Cooler Information
Cooler Number/ID
Condition of Shipping Container
Cooler Sealed (taped)
Custody Seals Present
Coolant
state of Coolant
Thermometer ID
Packing Description
p6ood
•Yes
•Yes
• Intact
•Ice
^pf^ozen
Reading _
•Fair
•No
• No
•Broken
^^ue Ice DNone
•Partially Frozen
S. C CF "
•Not Applicable
^^ficH Applicable
^ot Applicable
•Damaged (explain) _
Seal Number
Other
•Melted
Corrected Temp r Temp Blank Included DYes ^No
Chaln-Of-Custody Information
COC Present »- ft -»^i ^BYes
COC Number(s) tll^*'01-—" ^
COC signed (relinquished and received) jXyes
COC or LWI agrees with sample labels ^es
Notes
•No
•No
•No
Other
•Not Applicable
•Not Applicable
Sample Information
Samples included in cooler
Custody Seals Present
Sample containers intact
Samples in proper containers
Sufficient sample volume
All samples received In hold time
•Yes
•Intact
pYes
JZl^es
jaYes
Water - VO/U have zero headspace
ZPre-preserved with HCl
Notes
other
•Broken Seal Number(s) _
•No Notes
•No
• No
•No
•No
•Pre-preserved with Na^SjOs
•Not Applicable
DNon-Preserved
Water - pH acceptable upon receipt •Yes DAdjusted (see comments below) ,0flot Applicable
HNO3 = H2SO4 = NaOH = ZnAC /NaOH = HCL =
Water pH adjusted (mfg & Lot No)
HNO3 HzSOi.
NajSOjOj other _
Notes
NaOH _ZnAC HCl
SOP-102 Form A
ENVIRONMENTAL LAB WORK REQUEST
1010012
" ATK ENVIRONMENTAL LABORATORY LWR No
Login No
E13205
FROM CXTZNSION COST CENTER WORKORDER
usss3e-i<di
PATI
0Rf;ANlZAT10N MAIL STOP
SOI
REPORT RESULTS TO
HELEN RAVSTEN, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS SAMPLE DATE
G c
LOCATION TIME TEST REMARKS
1 y,s K I^Hs^
/
J
% Jt LC tu
4
5
6
7
8
9
10
11
12
CHAIN OF CUSTODY
R^^/^IS^D^ DATE TIME RECEIVED BY DATE TIME
/^M/2 lof IS./10 /^^
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED
988P LS333 G\N
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Requested
Monday, November 08, 2010
TESTED FOR ATK DLV
Environmental Monitonng
Thiokol Corp, UT 84322
ANALYZED BY-ATK Launch Systems
Analytical Chemistry Laboratory
P O Box 707, M/S 245
Bngham City, UT 84302-0707
435-863-3732
435-863-8080
Contact Name.
Project.
Sample Delivery Group
Al Lee
Ground Water Testing - DLV
1010012
Page 1 of 6
Pnnted 11/08/10 09 42
Sample Delivery Group 1010012
Sample No Client No Received Collect Date/Time
Test Requested Sample Description Matnx
1010012 01 J5 10/12/10 10/12/2010 13 45 0
EPA 314 0
SW-846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
1010012 02 J6 10/12/10 10/12/2010 13 58 0
EPA 314 0
SW-846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
1010012-03 J 8 10/12/10 10/12/2010 15 47 0
EPA 314 0
SW-846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
Certified By
11/08/2010
W Scott Fraser, Quality Assurance Officer Date
This certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation
Program (NELAP) unless otherwise annotated
Page 2 of 6
Pnnted 11/08/10 09 42
Listing of Results by Sample
Sample Delivery Group 1010012
Client Sample ID J 5 Laboratory Sample ID 1010012 01
Sample Description ATK DLV - Groundwater Fall 2010 DateSampled 10/12/10 1345
CAS Number Test Parameter Result Units MDL
Dilution
EQL Factor Analvst Test Date
Test Method EPA 314 0 Perchlorate Ion Chromatography
MDL
014797 73 0 PERCHLORATE 23 ug/L 1 4 1 JMM 10/19/1C
Test Method SIV 846 8260B (Water) Volatile Organic Analysis
67 64 1 ACETONE U ug/L 5 10 1 QC 10/14/10
107 02 8 ACROLEIN U ug/L 6 10 1 QC 10/14/10
71-43 2 BENZENE U ug/L 0 22 10 1 QC 10/14/10
75 27 4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 10/14/10
75 25 2 BROMOFORM U ug/L 0 42 10 1 QC 10/14/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 10/14/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 10/14/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 10/14/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 10/14/10
108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 QC 10/14/10
75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 10/14/10
67 66 3 CHLOROFORM 0 6 J ug/L 0 3 10 1 QC 10/14/10
74 87 3 CHLOROMETHANE U ug/L 0 81 10 1 QC 10/14/10
124^8 1 DIBROMOCHLOROMETHANE U ug/L 0 18 10 1 QC 10/14/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 10/14/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 10/14/10
75 35 4 1 1 DICHLOROETHENE u ug/L 0 16 10 1 QC 10/14/10
156 59 4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 10/14/10
156 60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 QC 10/14/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 10/14/10
10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 10/14/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 10/14/10
100-41-4 ETHYLBENZENE u ug/L 0 16 10 1 QC 10/14/10
591 78-6 2 HEXANONE u ug/L 07 10 1 QC 10/14/10
75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 10/14/10
108-10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 10/14/10
100-42 5 STYRENE u ug/L 0 3 10 1 QC 10/14/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 10/14/10
127-16-4 TETRACHLOROETHENE u ug/L 04 10 1 QC 10/14/10
108 88 3 TOLUENE u ug/L 0 5 10 1 QC 10/14/10
71 55 6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 10/14/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 10/14/10
79 01-6 TRICHLOROETHENE 34 J ug/L 07 10 1 QC 10/14/10
75 69-4 TRICHLOROFLUOROMETHANE u ug/L 03 10 1 QC 10/14/10
108 05-4 VINYL ACETATE u ug/L 20 50 1 QC 10/14/10
75 01-4 VINYL CHLORIDE u ug/L 03 10 1 QC 10/14/10
1330 20 7 m p XYLENE u ug/L 06 10 1 QC 10/14/10
95-47 6 0 XYLENE u ug/L 0 3 10 1 QC 10/14/10
17060 07 0 1 2 DICHLOROETHANE D4 101 % 1 QC 10/14/10
460 00 4 BROMOFLUOROBENZENE 103 % 1 QC 10/14/10
2037 26 5 TOLUENE D8 93 4 % 1 QC 10/14/10
1868 53 7 DIBROMOFLUOROMETHANE 97 5 % 1 QC 10/14/10
Pnnted
Page 3 of 6
11/08/10 09 42
Listing of Results by Sample
Sample Delivery Group 1010012
Client Sample ID J6 Laboratory Sample ID 1010012 02
Sample Description ATK DLV Groundwater Fall 2010
Date Sampled 10/12/10 13 58
CAS Number Test Parameter Result Units MDL
Dilution
EQL Factor Analvst Test Date
Test Method EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE 12 ug/L 1 4 1 JMM 10/19/10
Test Method SW 846, 8260B (Water) Volatile Organic Analysis
67 64 1 ACETONE U ug/L 5 10 1 QC 10/14/10
107 02 8 ACROLEIN U ug/L 6 10 1 QC 10/14/10
71-43 2 BENZENE U ug/L 0 22 10 1 QC 10/14/10
75 27 4 BROMODICHLOROMETHANE u ug/L 0 19 10 1 QC 10/14/10
75 25 2 BROMOFORM u ug/L 0 42 10 1 QC 10/14/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 10/14/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 10/14/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 10/14/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 10/14/10
108 90 7 CHLOROBENZENE 0 3 J ug/L 0 16 10 1 QC 10/14/10
75-00 3 CHLOROETHANE U ug/L 0 35 10 1 QC 10/14/10
67 66 3 CHLOROFORM U ug/L 0 3 10 1 QC 10/14/10
74 87 3 CHLOROMETHANE U ug/L 0 81 10 1 QC 10/14/10
124-48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 10/14/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 10/14/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 10/14/10
75 35-4 1 1 DICHLOROETHENE u ug/L 0 16 10 1 QC 10/14/10
156 59^ CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 10/14/10
156-60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 QC 10/14/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 10/14/10
10061-01 5 CIS-1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 10/14/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 10/14/10
100-41 4 ETHYLBENZENE u ug/L 0 16 10 1 QC 10/14/10
591 78-6 2 HEXANONE u ug/L 07 10 1 QC 10/14/10
75 09 2 METHYLENE CHLORIDE u ug/L 08 10 1 QC 10/14/10
108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 10/14/10
100-42 5 STYRENE u ug/L 0 3 10 1 QC 10/14/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 10/14/10
127 18-4 TETRACHLOROETHENE u ug/L 04 10 1 QC 10/14/10
108 88 3 TOLUENE u ug/L 05 10 1 QC 10/14/10
71 55-6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 10/14/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 10/14/10
79 01 6 TRICHLOROETHENE u ug/L 07 10 1 QC 10/14/10
75 69-4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 10/14/10
108 05 4 VINYL ACETATE u ug/L 20 50 1 QC 10/14/10
75 01-4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 10/14/10
1330 20-7 m p XYLENE u ug/L 06 10 1 QC 10/14/10
95^7 6 0 XYLENE u ug/L 0 3 10 1 QC 10/14/10
17060 07-0 1 2 DICHL0R0ETHANE-D4 100 % 1 QC 10/14/10
460 00 4 BROMOFLUOROBENZENE 103 % 1 QC 10/14/10
2037 26 5 TOLUENE D8 94 2 % 1 QC 10/14/10
1868 53 7 DIBROMOFLUOROMETHANE 96 % 1 QC 10/14/10
Pnnted
Page 4 of 6
11/08/10 09 42
Listing of Results by Sample
Sample Delivery Group 1010012
Client Sample ID J8 Laboratory Sample ID 1010012 03
Sample Description ATK DLV Groundwater Fall 2010
DateSampled 10/12/10 15 47
CAS Number Test Parameter Result Units MDL
Dilution
EQL Factor Analvst Test Date
Test Method EPA 314 0 Perchlorate Ion Chromatography
MDL
014797 73 0 PERCHLORATE U ug/L 1 4 1 JMM 10/19/10
Test Method SW 846 82606 flVaferJ Volatile Organic Analysis
67 64 1 ACETONE U ug/L 5 10 1 QC 10/14/10
107 02 8 ACROLEIN U ug/L 6 10 1 QC 10/14/10
71-43 2 BENZENE U ug/L 0 22 10 1 QC 10/14/10
75 27 4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 10/14/10
75 25 2 BROMOFORM U ug/L 0 42 10 1 QC 10/14/10
74 83 9 BROMOMETHANE U ug/L 0 57 10 1 QC 10/14/10
78 93 3 2 BUTANONE U ug/L 1 11 10 1 QC 10/14/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 10/14/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 10/14/10
108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 QC 10/14/10
75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 10/14/10
67 66 3 CHLOROFORM u ug/L 0 3 10 1 QC 10/14/10
74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 10/14/10
124-48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 10/14/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 10/14/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 10/14/10
75 35-4 1 1 DICHLOROETHENE u ug/L 0 16 10 1 QC 10/14/10
156 59 4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 10/14/10
156 60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 QC 10/14/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 10/14/10
10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 10/14/10
10061-02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 10/14/10
100 41-4 ETHYLBENZENE u ug/L 0 16 10 1 QC 10/14/10
591 78 6 2 HEXANONE u ug/L 0 7 10 1 QC 10/14/10
75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 10/14/10
108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 10/14/10
100-42 5 STYRENE u ug/L 0 3 10 1 QC 10/14/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 10/14/10
127 18-4 TETRACHLOROETHENE u ug/L 04 10 1 QC 10/14/10
108-88 3 TOLUENE u ug/L 05 10 1 QC 10/14/10
71 55 6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 10/14/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 10/14/10
79 01 6 TRICHLOROETHENE u ug/L 0 7 10 1 QC 10/14/10
75 69-4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 10/14/10
108 05-4 VINYL ACETATE u ug/L 20 50 1 QC 10/14/10
75 01 4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 10/14/10
1330 20 7 m p XYLENE u ug/L 06 10 1 QC 10/14/10
95 47 6 0 XYLENE u ug/L 0 3 10 1 QC 10/14/10
17060 07 0 1 2 DICHLOROETHANE D4 101 % 1 QC 10/14/10
460 00 4 BROMOFLUOROBENZENE 103 % 1 QC 10/14/10
2037 26 5 TOLUENE D8 95 1 % 1 QC 10/14/10
1868 53 7 DIBROMOFLUOROMETHANE 99 1 % 1 QC 10/14/10
Pnnted
Page 5 of 6
11/08/10 09 42
Data Reporting Qualifiers
Indicates that the analyte concentration is less than the MDL
This flag is used when an analyte is found in the blank as well as the sample
Indicates an extimated value This flag is used either when estimating a concentration
for tentatively identified compounds or when the data indicated the presence of a
compound that meets the identification critena but the result is less than the
EQL (e g 3 J with an EQL of 10)
MDL Method Detection Limit The minimum concentration of a substance that can be
confidently measured and reported The laboratory has demonstrated that the
MDL can be achieved in a laboratory reagent blank, but does not guarantee it
can be achieved in all sample matnces
EQL Estimated Quantitation Limit The EQL generally is 5 to 10 times the MDL For
many analytes the EQL is selected as the value of the lowest standard in the
calibration curve
Dilution Dilution Factor The prepared sample was diluted by this factor because the
Factor sample was too concentrated or due to other interferences in the sample matrix
Any dilution factor causes a corresponding increase in the MDL and EQL
Page 6 of 6
Pnnted 11/08/10 09 42
ATK Launch Systems
Environmental Laboratory
Client Name
Sample Receipt Checklist
SDG No
Camer _ Gamer Number
• Hand delivered no cooler y|Hand delivered sample(s) taken out at receiving counter
Cooler Information
Cooler Number/IO.
CoTAdrtton of Shipping Container
Cooler Sealed (taped)
Custody Seals Present
Coolant
state of Coolant
Thermometer ID
Packing Descnption
fe^ood
•Yes
•Yes
•Intact
•Ice
^JfTozen
Reading,
•Fair
OI<to
•Not Applicable
•Not Applicable
•Not Applicable
•Damaged (explain).
•Broken
p^e Ice GNone
•Partially Frozen
_4_C CF. :
Seal Number
Other
•Melted
Corrected Temp _ Temp Blank Included dYes DNo
Notes
Chain-Of Custody Information
COC Present _. ,0 7-,
COCNumbeits)_t/P*CO ^
COC signed (relinquuhed and received) ISYK^
COC or LWI agrees with sample labels icPi'es
•No
•No
•No
Other
•Not Applicable
•Not Applicable
Sample Information
Samples included in cooler
Custody Seals Present
Sample containers intact.
Samples in proper containers
Sufficient sample volume
All samples received In hold time
Water—VO A & have zero headspace
pwe-presenred with HCl
Notes
•Yes
•Intact
es(io Other
•Broken Seal Number^s) _
DNo Notes
•No
•No
•No
•No DNot Applicable
•Pre-preserved with NajSjOj •Non Preserved
jrftatA Water - pH acceptable upon receipt QYes QAdjusted (see comments below)
HNO3 = H2SO, = NaOH =
Applicable
ZnAC/NaOH = _HCL =
Water - pH adjusted (mfg & Lot No)
HNO3 HjSO,,
Na,SOiOj ^Other_
Notes
NaOH _ZnAC. HCl
SOP-102 Form A
1012003
ENVIRONMENTAL LAB WORK REQUEST
™ ATK ENVIRONMENTAL LABORATORY LWR No
Login No
E13209
FROM EXTENSION COST CENTER —^———
WORKORDER DATE
ORGANIZATION MAIL STOP REPORT RESULTS TO
HELEN RAVSTEN, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS SAMPLE DATE
G c
LOCATION TIME TEST REMARKS
y /ISO
/ / /zoo II It "
X '/ n f " "
\z\i\li> / fl „ " o "
5
6
7
8
9
10
II
12
CHAIN OF CUSTODY
RELJ^QUISHEDJBV DATE TIME RECEIVED BY DATE TIME
jz/i//a /SVS'
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED
988P LS333 GW
CERTIFICATE OF ANALYSIS
Listing of Sample information and Testing Requested
Friday, January 14, 2011
TESTED FOR ATK DLV
Environmental Monitoring
Thiokol Corp, UT 84322
ANALYZED BY ATK Launch Systems
Analytical Chemistry Laboratory
P O Box 707, M/S 245
Brigham City, UT 84302-0707
435-863-3732
435-863-8080
Contact Name-
Project
Sample Delivery Group
Al Lee
Ground Water Testing - DLV
1012003
Page 1 of 7
Pnnted 01/14/1114 01
Sample Delivery Group 1012003
Sample No Ciient No
Test Requested Sample Description
Received Collect Date/Time
Matrix
1012003 01 D 4 12/01/10 12/1/2010 11 30 00
EPA 3U0
SW 846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
1012003 02 D 5 12/01/10 12/1/2010 12 00 00
EPA 314 0
SW 846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
1012003 03 E 2 12/01/10 12/1/2010 14 30 00
EPA 314 0
SW 846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
1012003 04 J 2 12/01/10 12/1/2010 15 00 00
EPA 314 0
SW846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
Certified By 01/14/2011
W Scott Fraser, Quality Assurance Officer Date
This certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation
Program (NELAP) unless otherwise annotated
Page 2 of 7
Pnnted 01/14/1114 01
Listing of Results by Sample
Sample Delivery Group 1012003
Client Sample ID D4
Sample Description ATK DLV Groundwater Fall 2010
Laboratory Sample ID 1012003 01
DateSampled 12/01/10 11 30
Dilution
CAS Number Test Parameter Result Units MDL EQL Factor Analvst Test Date
Test Method EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE 130000 ug/L 1000 4000 1000 JMM 12/14/10
Tes* Method SIV 846 8260B (Water) Volatile Organic Analysis
67 64 1 ACETONE U ug/L 5 10 1 QC 12/03/10
107 02 8 ACROLEIN U ug/L 6 10 1 QC 12/03/10
71^3 2 BENZENE U ug/L 0 22 10 1 QC 12/03/10
75 27A BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 12/03/10
75 25 2 BROMOFORM U ug/L 0 42 10 1 QC 12/03/10
74 83 9 BROMOMETHANE U ug/L 0 57 10 1 QC 12/03/10
78 93 3 2 BUTANONE U ug/L 1 11 10 1 QC 12/03/10
75 15 0 CARBON DISULFIDE 0 2 J ug/L 0 13 10 1 QC 12/03/10
56 23 S CARBON TETRACHLORIDE 2 5 J ug/L 0 27 10 1 QC 12/03/10
108 90 7 CHLOROBENZENE 04 J ug/L 0 16 10 1 QC 12/03/10
75 00 3 CHLOROETHANE U ug/L 0 35 10 1 QC 12/03/10
67 66 3 CHLOROFORM 1 9 J ug/L 0 3 10 1 QC 12/03/10
74 87 3 CHLOROMETHANE U ug/L 0 81 10 1 QC 12/03/10
124-48 1 DIBROMOCHLOROMETHANE U ug/L 0 18 10 1 QC 12/03/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 12/03/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 12/03/10
75 35 4 1 1 DICHLOROETHENE 12 5 ug/L 0 16 10 1 QC 12/03/10
156 59-4 CIS 1 2 DICHLOROETHENE U ug/L 0 16 10 1 QC 12/03/10
156 60 5 TRANS-1 2 DICHLOROETHENE U ug/L 0 34 10 1 QC 12/03/10
78 87 5 1 2 DICHLOROPROPANE U ug/L 0 16 10 1 QC 12/03/10
10061-01 5 CIS 1 3 DICHLOROPROPENE U ug/L 04 10 1 QC 12/03/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE U ug/L 04 10 1 QC 12/03/10
100-41 4 ETHYLBENZENE U ug/L 0 16 10 1 QC 12/03/10
591 78 6 2 HEXANONE U ug/L 07 10 1 QC 12/03/10
75 09 2 METHYLENE CHLORIDE U ug/L 0 8 10 1 QC 12/03/10
108 10 1 4-METHYL-2 PENTANONE U ug/L 0 53 10 1 QC 12/03/10
100-42 5 STYRENE U ug/L 0 3 10 1 QC 12/03/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 12/03/10
127-18-4 TETRACHLOROETHENE u ug/L 04 10 1 QC 12/03/10
108 88 3 TOLUENE u ug/L 0 5 10 1 QC 12/03/10
71 55 6 1 1 1 TRICHLOROETHANE 2 1 J ug/L 0 16 10 1 QC 12/03/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 12/03/10
79 01 6 TRICHLOROETHENE 55 6 ug/L 07 10 1 QC 12/03/10
75 69-4 TRICHLOROFLUOROMETHANE 0 7 J ug/L 0 3 10 1 QC 12/03/10
108 05-4 VINYL ACETATE U ug/L 20 50 1 QC 12/03/10
75 01-4 VINYL CHLORIDE u ug/L 03 10 1 QC 12/03/10
1330 20 7 m p XYLENE u ug/L 06 10 1 QC 12/03/10
95-47 6 0 XYLENE u ug/L 0 3 10 1 QC 12/03/10
17060 07 0 1 2 DICHLOROETHANE D4 100 % 1 QC 12/03/10
460 00 4 BROMOFLUOROBENZENE 100 % 1 QC 12/03/10
2037 26 5 TOLUENE D8 94 6 % 1 QC 12/03/10
1868 53 7 DIBROMOFLUOROMETHANE 99 1 % 1 QC 12/03/10
Pnnted
Page 3 of 7
01/14/11 14 01
Listing of Results by Sample
Sample Delivery Group 1012003
Client Sample ID D5
Sample Description ATK DLV Groundwater Fall 2010
Laboratory Sample ID 1012003 02
DateSampled 12/01/10 12 00
Dilution
CAS Number Test Parameter Result Units MDL EQL Factor Analvst Test Date
Test Method EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE 168000 ug/L 1000 4000 1000 JMM 12/14/10
fes^ Method SW 846, 82606 (Water) Volatile Organic Analysis
67 64 1 ACETONE U ug/L 5 10 1 QC 12/03/10
107 02 8 ACROLEIN U ug/L 6 10 1 QC 12/03/10
71-43 2 BENZENE OSJ ug/L 0 22 10 1 QC 12/03/10
75 27^ BROMODICHLOROMETHANE u ug/L 0 19 10 1 QC 12/03/10
75 25 2 BROMOFORM u ug/L 0 42 10 1 QC 12/03/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 12/03/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 12/03/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 12/03/10
56 23 5 CARBON TETRACHLORIDE 3 6 J ug/L 0 27 10 1 QC 12/03/10
108 90 7 CHLOROBENZENE 0 4 J ug/L 0 16 10 1 QC 12/03/10
75 00 3 CHLOROETHANE U ug/L 0 35 10 1 QC 12/03/10
67-66 3 CHLOROFORM 7 7 J ug/L 0 3 10 1 QC 12/03/10
74 87 3 CHLOROMETHANE U ug/L 0 81 10 1 QC 12/03/10
124^8 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 12/03/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 12/03/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 12/03/10
75 35A 1 1 DICHLOROETHENE 21 4 ug/L 0 16 10 1 QC 12/03/10
156 59-4 CIS 1 2 DICHLOROETHENE U ug/L 0 16 10 1 QC 12/03/10
156 60 5 TRANS 1 2-DICHLOROETHENE u ug/L 0 34 10 1 QC 12/03/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 12/03/10
10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/03/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/03/10
100-41 4 ETHYLBENZENE u ug/L 0 16 10 1 QC 12/03/10
591 78-6 2 HEXANONE u ug/L 07 10 1 QC 12/03/10
75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 12/03/10
108 10 1 4-METHYL-2-PENTANONE u ug/L 0 53 10 1 QC 12/03/10
100-42 5 STYRENE u ug/L 0 3 10 1 QC 12/03/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 12/03/10
127 18-4 TETRACHLOROETHENE u ug/L 04 10 1 QC 12/03/10
108 88 3 TOLUENE u ug/L 05 10 1 QC 12/03/10
71 55 6 1 1 1 TRICHLOROETHANE 5 9 J ug/L 0 16 10 1 QC 12/03/10
79 00-5 1 1 2 TRICHLOROETHANE U ug/L 0 25 10 1 QC 12/03/10
79 01-6 TRICHLOROETHENE 637 ug/L 7 100 10 QC 12/03/10
75-69 4 TRICHLOROFLUOROMETHANE U ug/L 0 3 10 1 QC 12/03/10
108 05 4 VINYL ACETATE U ug/L 20 50 1 QC 12/03/10
75 01-4 VINYL CHLORIDE U ug/L 0 3 10 1 QC 12/03/10
1330 20 7 m p XYLENE U ug/L 06 10 1 QC 12/03/10
95-47 6 0 XYLENE U ug/L 0 3 10 1 QC 12/03/10
17060 07 0 1 2 DICHLOROETHANE D4 101 % 1 QC 12/03/10
460 00-4 BROMOFLUOROBENZENE 96 % 1 QC 12/03/10
2037 26 5 TOLUENE D8 94 2 % 1 QC 12/03/10
1868 53 7 DIBROMOFLUOROMETHANE 97 7 % 1 QC 12/03/10
Pnnted
Page 4 of 7
01/14/11 14 01
Listing of Results by Sample
Sample Delivery Group 1012003
Client Sample ID E2
Sample Description ATK DLV - Groundwater Fall 2010
Laboratory Sample ID 1012003-03
Date Sampled 12/01/10 14 30
Dilution
CAS Number Test Parameter Result Units MDL EQL Factor Analvst Test Date
Teat Method EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE U ug/L 10 40 10 JMM 12/15/10
Test Method SiiV 846 82608 (Water) Volatile Organic Analysis
67 64 1 ACETONE U ug/L 5 10 1 QC 12/03/10
107 02 8 ACROLEIN U ug/L 6 10 1 QC 12/03/10
71-43 2 BENZENE U ug/L 0 22 10 1 QC 12/03/10
75 27 4 BROMODICHLOROMETHANE u ug/L 0 19 10 1 QC 12/03/10
75 25 2 BROMOFORM u ug/L 0 42 10 1 QC 12/03/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 12/03/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 12/03/10
75-15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 12/03/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 12/03/10
108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 QC 12/03/10
75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 12/03/10
67 66 3 CHLOROFORM u ug/L 0 3 10 1 QC 12/03/10
74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 12/03/10
124-48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 12/03/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 12/03/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 12/03/10
75 35-4 1 1 DICHLOROETHENE u ug/L 0 16 10 1 QC 12/03/10
156 59 4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 12/03/10
156 60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 QC 12/03/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 12/03/10
10061-01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/03/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/03/10
100-41 4 ETHYLBENZENE u ug/L 0 16 10 1 QC 12/03/10
591 78 6 2 HEXANONE u ug/L 07 10 1 QC 12/03/10
75-09 2 METHYLENE CHLORIDE u ug/L 08 10 1 QC 12/03/10
108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 12/03/10
100-42 5 STYRENE u ug/L 0 3 10 1 QC 12/03/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 12/03/10
127 18-4 TETRACHLOROETHENE u ug/L 04 10 1 QC 12/03/10
108 88 3 TOLUENE u ug/L 0 5 10 1 QC 12/03/10
71 55 6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 12/03/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 12/03/10
79 01 6 TRICHLOROETHENE 2 3 J ug/L 07 10 1 QC 12/03/10
75 69 4 TRICHLOROFLUOROMETHANE u ug/L 03 10 1 QC 12/03/10
108 05 4 VINYL ACETATE u ug/L 20 50 1 QC 12/03/10
75 01-4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 12/03/10
1330-20 7 m p XYLENE u ug/L 06 10 1 QC 12/03/10
95-47 6 0 XYLENE u ug/L 0 3 10 1 QC 12/03/10
17060 07 0 1 2 DICHLOROETHANE D4 101 % 1 QC 12/03/10
460 00-4 BROMOFLUOROBENZENE 96 4 % 1 QC 12/03/10
2037 26 5 TOLUENE D8 92 9 % 1 QC 12/03/10
1868 53 7 DIBROMOFLUOROMETHANE 98 7 % 1 QC 12/03/10
Pnnted
Page 5 of 7
01/14/11 14 01
Listing of Results by Sample
Sample Delivery Group 1012003
Client Sample ID J 2 Laboratory Sample ID 1012003 04
Date Sampled 12/01/10 15 00
Sample Description ATK DLV Groundwater Fall 2010
Dilution
CAS Number Test Parameter Result Units MDL EQL Factor Analvst Test Date
Test Method EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE 223 ug/L 5 20 5 JMM 12/15/10
Tesf Method SW 846 8260B (Water) Volatile Organic Analysis
67 64 1 ACETONE U ug/L 5 10 1 QC 12/03/10
107 02 8 ACROLEIN U ug/L 6 10 1 QC 12/03/10
71 43 2 BENZENE U ug/L 0 22 10 1 QC 12/03/10
75 27-4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 12/03/10
75 25 2 BROMOFORM u ug/L 0 42 10 1 QC 12/03/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 12/03/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 12/03/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 12/03/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 12/03/10
108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 QC 12/03/10
75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 12/03/10
67 66 3 CHLOROFORM u ug/L 0 3 10 1 QC 12/03/10
74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 12/03/10
124 48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 12/03/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 12/03/10
107 06-2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 12/03/10
75 35-4 1 1 DICHLOROETHENE u ug/L 0 16 10 1 QC 12/03/10
166 59 4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 12/03/10
156 60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 QC 12/03/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 12/03/10
10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/03/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/03/10
100 41 4 ETHYLBENZENE u ug/L 0 16 10 1 QC 12/03/10
591 78 6 2 HEXANONE u ug/L 0 7 10 1 QC 12/03/10
75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 12/03/10
108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 12/03/10
100-42 5 STYRENE u ug/L 0 3 10 1 QC 12/03/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 12/03/10
127 18-4 TETRACHLOROETHENE u ug/L 0 4 10 1 QC 12/03/10
108 88 3 TOLUENE u ug/L 0 5 10 1 QC 12/03/10
71 55 6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 12/03/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 12/03/10
79 01 6 TRICHLOROETHENE 11J ug/L 0 7 10 1 QC 12/03/10
75 69-4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 12/03/10
108 05 4 VINYL ACETATE u ug/L 20 50 1 QC 12/03/10
75 01 4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 12/03/10
1330 20 7 m p XYLENE u ug/L 0 6 10 1 QC 12/03/10
95-47 6 0 XYLENE u ug/L 0 3 10 1 QC 12/03/10
17060 07 0 1 2 DICHLOROETHANE D4 101 % 1 QC 12/03/10
460 00 4 BROMOFLUOROBENZENE 97 3 % 1 QC 12/03/10
2037 26 5 TOLUENE D8 92 7 % 1 QC 12/03/10
1868 53 7 DIBROMOFLUOROMETHANE 100 % 1 QC 12/03/10
Pnnted
Page 6 of 7
01/14/11 14 01
Data Reporting Qualifiers
indicates that the analyte concentration is less than the MDL
This flag is used when an analyte is found in the blank as well as the sample
Indicates an extimated value This flag is used either when estimating a concentration
for tentatively identified compounds or when the data indicated the presence of a
compound that meets the identification critena but the result is less than the
EQL (eg 3 J with an EQL of 10)
MDL Method Detection Limit The minimum concentration of a substance that can be
confidently measured and reported The laboratory has demonstrated that the
MDL can be achieved in a laboratory reagent blank but does not guarantee it
can be achieved in all sample matnces
EQL Estimated Quantitation Limit The EQL generally is 5 to 10 times the MDL For
many analytes the EQL is selected as the value ofthe lowest standard in the
calibration curve
Dilution Dilution Factor The prepared sample was diluted by this factor because the
Factor sample was too concentrated or due to other interferences in the sample matnx
Any dilution factor causes a corresponding increase in the MDL and EQL
Page 7 of 7
Pnnted 01/14/11 14 01
ATK Launch Systems
Environmental Laboratory
Sample Receipt Checklist
SDG No Client Name
Camer ]kU \J^^ Camer Number
• Hand delivefed no cooler \a^Hand deln/ered sample(s) taken out at receiving coun'er
Cooler Infonnation
Cooler NumbcrflD
Condition cf Shipping Container
Cooler Sealed (taped)
Custody Seals Present
6dood
DYes
•Yes
•Intact
OFair
^0
Coolant
state of Coolant
Themiometer ID
Padang Descnption
tJ^rozen
Reading,
•Not Applicable
QNot Applicable
•Not Applicable
•Broken
•Blue Ice ONone
•Partially FnKcn OMelted
J CF UL.
•Damaged (explain).
Seal Number .
Other
Con-ectedTemp \ 'C Temp Blank Included OYes ON^'
Chaln-Of-Custody Infonnation
COO Present Kx/t^M DNo Other
COC Nuinbej(s) b SOt VtCfa./
COC signed (relinquished and received) 0^ DNo ONot Applicable
COC or LWI agrees with sample labels- ONo DNot/Applicable
Notes
Sample Information
Samples included m cooler
Custody Seals Present DYes
Oln^
Sample oontaners Intact •QNeit
Samples in proper containers-
Suffiaent sample volume
An samples received In hold tone.
Water - VO^V^have zero headspace
IPre-preserved with HCl
Notes
Other
•Broken Seal Number<s).
•No Notes
•No
DNo
•No
•Pre-preserved with NajSsQj.
•Not AppEeable
QNon-Pieserved
Water - pH acceptable upon receipt DYes
HNOi= ^H^0« =
•Adjusted (see comments belov^ \tfNot Applicable
^NaOH" ^ZnAC/NaOH = HCL =
Water-pHadjusted (mfg &Lx)tNo)
HNOs. H^04.
Na^OA ^Other,
Notes
NaOH ZnAC HCl
SOP-102FonnA
1012009
ENVIRONMENTAL LAB WORK REQUEST
" ATK ENVIRONMENTAL LABORATORY LWR No
Login No
E13211
FROMi EXTENSION
^si^e>B
COST CENTER
e>zjao
WORKORDER DATE
/z/s//o
ORGAN1ZATIO^ MAIL STOP REPORT RESULTS TO
HELEN RAVSTEN, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS SAMPLE DATE
G C
LOCATION TIME TEST REMARKS
T
It ft tt tf
3
4
5
6
7
8
9
10
II
12
CHAIN OF CUSTODY
l^UCj^lJ^ISHED ^ DATE TIME RECEIVED BY DATE TIME
////M l^/lf}//6
' / f ^ t
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED
988P LS333 GW
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testmg Requested
Friday, January 14, 2011
TESTED FOR ATK DLV
Environmental Monitoring
Thiokol Corp, UT 84322
ANALYZED BY ATK Launch Systems
Analytical Chemistry Laboratory
P O Box 707, M/S 245
Brigham City, UT 84302-0707
435-863-3732
435-863-8080
Contact Name.
Project
Sample Delivery Group
Al Lee
Ground Water Testing - DLV
1012009
Page 1 of 5
Pnnted 01/14/1114 02
Sample Delivery Group 1012009
Sample No Client No Received Collect Date/Time
Test Requested Sample Description Matrix
1012009 01 H6 12/03/10 12/3/2010 13 40 00
EPA 314 0
SW846 8260B (Water)
Perchlorate Ion Ctiromatography
Volatile Organic Analysis
Water
Water
1012009 02 H 8 12/03/10 12/3/2010 14 30 00
EPA 314 0
SW846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
Certified By 01/14/2011
W Scott Fraser, Quality Assurance Officer Date
This certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation
Program (NELAP) unless otherwise annotated
Page 2 of 5
Pnnted 01/14/11 14 02
Listrng of Results by Sample
Sample Delivery Group 1012009
Client Sample ID H6
Sample Description ATK-DLV Groundwater Fall 2010
Laboratory Sample ID 1012009 01
Date Sampled 12/03/10 13 40
Dilution
CAS Number Test Parameter Result Units MDL EQL Factor Analvst Test Date
Tesf Mefhod EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE U ug/L 5 20 5 JMM 12/15/10
Test Method SIV 846, 82606 (Water) Volatile Organic Analysis
67 64 1 ACETONE U ug/L 5 10 1 QC 12/07/10
107 02 8 ACROLEIN U ug/L 5 10 1 QC 12/07/10
71^3 2 BENZENE u ug/L 0 22 10 1 QC 12/07/10
75 27-4 BROMODICHLOROMETHANE u ug/L 0 19 10 1 QC 12/07/10
75 25 2 BROMOFORM u ug/L 0 42 10 1 QC 12/07/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 12/07/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 12/07/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 12/07/10
S6 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 12/07/10
108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 QC 12/07/10
75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 12/07/10
67 66 3 CHLOROFORM u ug/L 0 3 10 1 QC 12/07/10
74-87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 12/07/10
124 48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 12/07/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 12/07/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 12/07/10
75 35-4 1 1 DICHLOROETHENE 1 8 J ug/L 0 16 10 1 QC 12/07/10
156 59-4 CIS 1 2-DICHLOROETHENE u ug/L 0 16 10 1 QC 12/07/10
1S6-60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 QC 12/07/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 12/07/10
10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/07/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 0 4 10 1 QC 12/07/10
100-41 4 ETHYLBENZENE u ug/L 0 16 10 1 QC 12/07/10
591 78 6 2 HEXANONE u ug/L 07 10 1 QC 12/07/10
75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 12/07/10
108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 12/07/10
100-42 5 STYRENE u ug/L 0 3 10 1 QC 12/07/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 12/07/10
127 18 4 TETRACHLOROETHENE u ug/L 04 10 1 QC 12/07/10
108 88 3 TOLUENE u ug/L 0 5 10 1 QC 12/07/10
71 55-6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 12/07/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 12/07/10
79 01-6 TRICHLOROETHENE 1 5 J ug/L 07 10 1 QC 12/07/10
75 69-4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 12/07/10
108 05 4 VINYL ACETATE u ug/L 20 50 1 QC 12/07/10
75 01-4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 12/07/10
1330 20 7 m p XYLENE u ug/L 0 6 10 1 QC 12/07/10
95-47-6 0 XYLENE u ug/L 0 3 10 1 QC 12/07/10
17060 07 0 1 2 DICHLOROETHANE D4 99 6 % 1 QC 12/07/10
460 00 4 BROMOFLUOROBENZENE 94 9 % 1 QC 12/07/10
2037 26 5 TOLUENE D8 91 9 % 1 QC 12/07/10
1868 53 7 DIBROMOFLUOROMETHANE 98 1 % 1 QC 12/07/10
Pnnted
Page 3 of 5
01/14/11 14 02
Listing of Results by Sample
Sample Delivery Group 1012009
Client Sample ID H 8 Laboratory Sample ID 1012009 02
Date Sampled 12/03/10 14 30
Sample Description ATK DLV Groundwater Fall 2010
Dilution
CAS Number Test Parameter Result Units MDL EQL Factor Analvst Test Date
Tesf Method EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE U ug/L 5 20 5 JMM 12/15/10
Tes< Method SIV 846, 82608 (Water) Volatile Organic Analysis
67 64 1 ACETONE U ug/L 5 10 1 QC 12/07/10
107 02 8 ACROLEIN U ug/L 6 10 1 QC 12/07/10
71 43 2 BENZENE U ug/L 0 22 10 1 QC 12/07/10
75 27 4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 12/07/10
75 25 2 BROMOFORM U ug/L 0 42 10 1 QC 12/07/10
74 83 9 BROMOMETHANE U ug/L 0 57 10 1 QC 12/07/10
78 93 3 2 BUTANONE U ug/L 1 11 10 1 QC 12/07/10
75 15 0 CARBON DISULFIDE U ug/L 0 13 10 1 QC 12/07/10
56 23 5 CARBON TETRACHLORIDE U ug/L 0 27 10 1 QC 12/07/10
108 90 7 CHLOROBENZENE U ug/L 0 16 10 1 QC 12/07/10
75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 12/07/10
67 66 3 CHLOROFORM u ug/L 0 3 10 1 QC 12/07/10
74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 12/07/10
124 48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 12/07/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 12/07/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 12/07/10
75 35-4 1 1 DICHLOROETHENE 06 J ug/L 0 16 10 1 QC 12/07/10
156-59-4 CIS 1 2 DICHLOROETHENE U ug/L 0 16 10 1 QC 12/07/10
156 60 5 TRANS 1 2 DICHLOROETHENE U ug/L 0 34 10 1 QC 12/07/10
78 87 5 1 2 DICHLOROPROPANE U ug/L 0 16 10 1 QC 12/07/10
10061 01 5 CIS 1 3 DICHLOROPROPENE U ug/L 04 10 1 QC 12/07/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/07/10
100-41-4 ETHYLBENZENE u ug/L 0 16 10 1 QC 12/07/10
591 78 6 2 HEXANONE u ug/L 0 7 10 1 QC 12/07/10
75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 12/07/10
108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 12/07/10
100-42 5 STYRENE u ug/L 0 3 10 1 QC 12/07/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 12/07/10
127 18-4 TETRACHLOROETHENE u ug/L 0 4 10 1 QC 12/07/10
108 88 3 TOLUENE u ug/L 0 5 10 1 QC 12/07/10
71 55 6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 12/07/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 12/07/10
79 01 6 TRICHLOROETHENE u ug/L 07 10 1 QC 12/07/10
75 69-4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 12/07/10
108 05-4 VINYL ACETATE u ug/L 20 50 1 QC 12/07/10
75 01 4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 12/07/10
1330 20 7 m p XYLENE u ug/L 06 10 1 QC 12/07/10
95-47 6 0 XYLENE u ug/L 0 3 10 1 QC 12/07/10
17060 07 0 1 2 DICHLOROETHANE D4 99 5 % 1 QC 12/07/10
460 00 4 BROMOFLUOROBENZENE 97 1 % 1 QC 12/07/10
2037 26 5 TOLUENE D8 93 1 % 1 QC 12/07/10
1868 53 7 DIBROMOFLUOROMETHANE 99 4 % 1 QC 12/07/10
Pnnted
Page 4 of 5
01/14/11 14 02
Data Reporting Qualifiers
U Indicates that the analyte concentration is less than the MDL
This flag is used when an analyte is found in the blank as well as the sample
Indicates an extimated value This flag is used either when estimating a concentration
for tentatively identified compounds or when the data indicated the presence of a
compound that meets the identification critena but the result is less than the
EQL (e g 3 J with an EQL of 10)
MDL Method Detection Limit The minimum concentration of a substance that can be
confidently measured and reported The laboratory has demonstrated that the
MDL can be achieved in a laboratory reagent blank, but does not guarantee it
can be achieved in all sample matnces
EQL Estimated Quantitation Limit The EQL generally is 5 to 10 times the MDL For
many analytes the EQL is selected as the value of the lowest standard in the
calibration curve
Dilution Dilution Factor The prepared sample was diluted by this factor because the
Factor sample was too concentrated or due to other interferences in the sample matnx
Any dilution factor causes a corresponding increase in the MDL and EQL
Page 5 of 5
Pnnted 01/14/11 14 02
ATK Launch Systems
Environmental Laboratory
Client Name
Sample Receipt Checklist
SDG No
Camer_
Q Hand delivered no cooler . Camer Nunber
C/Wand delivered sample(s) taken out at receiving counter
I'D {UDtP^
Cooler Information
Cooler NumberJIO
Condition of Shipping Container
Cooler Sealed (taped)
Custody Seals Present
Coolant
State of Coolant „
Thermometer ID t/GlVV^
Packing Description
Cod
•Yes
OYes
•Int^
p^zen
Reading _
DFair
£INo
•Broken
CBlue Ice
^Partially Frozen
•Not Applicaole
ONo' Applicable
•Not Applicable
•Damaged (explain).
jNone
Seal Number _
Other
•Melted
CF Con-ected Temp _ Temp Blank Included OYes V/CJNO
Cham-Of-Custody Infonnation
COC Present f lOO i i
COCNumbef<s)_ELii*d_) /
COC signed (relinquished and received) ^l>fes
COC or LWI agrees with sample labels ffUs
Notes.
ONo
ONo
ONo
Other
•Not Applicable
ONot Applicable
Sample Information
Samples included In cooler ^^<A4^llr^uui^ -v ipUstcU^ j \y-Mov^uvi45 pUjHl^^^U/
Custody Seals Present
Sample comaineis intacL
Samples In proper containers
Sufficient sample volume
All samples received In hold time
•Yes
•In
z
Water - VOA vhave zen headspace
Dfre-presefved with HCl
Notes
ll(io Other
•Broken Seal Numbef<s}_
•No Notes
•No
•No
•No
•No ONot Applicable
•Pref reserved with NaSJ:^ •Non-Preserved
«jNot Water - pH acceptable upon receipt • Yes
HNOjS HjSO< =
•Adjusted (see comments below) iONot Applicable
NaOH= ZnACIHaOH = HCL = _
Water-pH adjusted (mfg & Lot No)
HNOj. H^04,
NajSOjOi Other.
Notes
NaOH ZnAC HCl
SOP-102 FoimA
1012015
ENVIRONMENTAL LAB WORK REQUEST
''° ATK ENVIRONME^TAL LABORATORY LWR No
Login No
E13216
EXTENSION COST CENTER WORK ORDER DATE
ORCANIZATIOV ^ MAIL STOP REPORT RESULTS TO
HELEN RAVSTEN, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS SAMPLE DATE
G c
LOCATION TIME TEST REMARKS
1 f-c^ izliilio llZC MOC'^Z/^O.CU^-W^ o
X ff /^^ ti f/ fr ^
' c-m I2[,l{t> '/ II /r "
{zjisif X // IH/O t< ff tl '/
h/iiL X 11/S ft ^f t 0
1 t
izliillo /SCO " f, f
' 1
V /ses ff ff fl //f
8
9
10
II
12
CHAIN OF CUSTODY
REIilN?)t;iSHED BY/7 DATE TIME RECEIVED BY DATE TIME
/zltif/i> (
r z c> / /
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED SIGNATURE
988P LS333 GW
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Requested
Friday, January 14, 2011
TESTED FOR ATK DLV
Environmental Monitonng
Thiokol Corp, UT 84322
ANALYZED BY ATK Launch Systems
Analytical Chemistry Laboratory
P O Box 707, M/S 245
Bngham City, UT 84302-0707
435-863-3732
435-863-8080
Contact Name:
Project
Sample Delivery Group
Al Lee
Ground Water Testing - DLV
1012015
Page 1 of 11
Pnnted 01/14/1114 02
Sample Delivery Group 1012015
Sample No Client No Received Collect Date/Time
Test Requested Sample Description Matrix
1012015 01 F4 12/13/10 12/13/2010 13 20 0 1
EPA 314 0
SW 846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
1012015 02 C8 12/13/10 12/13/2010 13 200
EPA 314 0
SW 846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
1012015 03 C SA 12/13/10 12/13/2010 13 20 0
EPA 314 0
SW 846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
1012015 04 FBI 12/13/10 12/13/2010 13 20 0
EPA 314 0
SW 846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
1012015-05 TB-1 12/13/10 12/13/2010 13 20 0
EPA 314 0
SW 846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
1012015-06 C7 12/13/10 12/13/2010 13 200
EPA 314 0
SW846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
1012015-07 C 7A 12/13/10 12/13/2010 13 200
EPA 314 0 Perchlorate Ion Chromatography Water
Page 2 of 11
Pnnted 01/14/11 14 02
Sample Delivery Group 1012015
Sample No Client No
Test Requested Sample Description
Received Collect Date/Time
Matrix
1012015 07 C 7A 12/13/10 12/13/2010 13 20 0
SW846 8260B (Water) Volatile Organic Analysis Water
Certified By 01/14/2011
W Scott Fraser Quality Assurance Officer Date
This certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation
Program (NELAP) unless otherwise annotated
Page 3 of 11
Pnnted 01/14/11 14 02
Listing of Results by Sample
Sample Delivery Group 1012015
Client Sample ID F4 Laboratory Sample ID 1012015 01
Sample Description ATK DLV Goundwater Fall 2010
DateSampled 12/13/10 13 20
CAS Number Test Parameter Result Units MDL
Dilution
EQL Factor Analvst Test Date
Test Method EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE 184 ug/L 1 4 1 JMM 12/16/10
Test Method SW 846, 8260S (Water) Volatile Org anic Analysis
67 64 1 ACETONE U ug/L 5 10 1 QC 12/15/10
107 02 8 ACROLEIN U ug/L 6 10 1 QC 12/15/10
71 43 2 BENZENE u ug/L 0 22 10 1 QC 12/15/10
75 27-4 BROMODICHLOROMETHANE u ug/L 0 19 10 1 QC 12/15/10
75 25 2 BROMOFORM u ug/L 0 42 10 1 QC 12/15/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 12/15/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 12/15/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 12/15/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 12/15/10
108 90 7 CHLOROBENZENE 0 2 J ug/L 0 16 10 1 QC 12/15/10
75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 12/15/10
67 66 3 CHLOROFORM 4 J ug/L 0 3 10 1 QC 12/15/10
74 87 3 CHLOROMETHANE U ug/L 0 81 10 1 QC 12/15/10
124-48 1 DIBROMOCHLOROMETHANE U ug/L 0 18 10 1 QC 12/15/10
75 34 3 1 1 DICHLOROETHANE U ug/L 0 49 10 1 QC 12/15/10
107 06 2 1 2 DICHLOROETHANE U ug/L 0 29 10 1 QC 12/15/10
75 35 4 1 1 DICHLOROETHENE 1 7 J ug/L 0 16 10 1 QC 12/15/10
156-59-4 CIS 1 2 DICHLOROETHENE U ug/L 0 16 10 1 QC 12/15/10
156 60 5 TRANS 1 2 DICHLOROETHENE U ug/L 0 34 10 1 QC 12/15/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 12/15/10
10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/15/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/15/10
100 41 4 ETHYLBENZENE u ug/L 0 16 10 1 QC 12/15/10
591 78 6 2 HEXANONE u ug/L 07 10 1 QC 12/15/10
75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 12/15/10
108 10 1 4 METHYL 2-PENTANONE u ug/L 0 53 10 1 QC 12/15/10
100-42 5 STYRENE u ug/L 0 3 10 1 QC 12/15/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 12/15/10
127 18 4 TETRACHLOROETHENE u ug/L 04 10 1 QC 12/15/10
108 88 3 TOLUENE u ug/L 0 5 10 1 QC 12/15/10
71 55 6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 12/15/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 12/15/10
79 01 6 TRICHLOROETHENE 19 1 ug/L 07 10 1 QC 12/15/10
75-69 4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 12/15/10
108 05 4 VINYL ACETATE u ug/L 20 50 1 QC 12/15/10
75 01 4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 12/15/10
1330 20 7 m p XYLENE u ug/L 0 6 10 1 QC 12/15/10
95-47 6 0 XYLENE u ug/L 03 10 1 QC 12/15/10
17060 07 0 1 2 DICHLOROETHANE D4 97 6 % 1 QC 12/15/10
460 00 4 BROMOFLUOROBENZENE 97 2 % 1 QC 12/15/10
2037 26 5 TOLUENE D8 89 9 % 1 QC 12/15/10
1868 53 7 DIBROMOFLUOROMETHANE 103 % 1 QC 12/15/10
Page 4 of 11
Pnnted 01/14/1114 02
Listing of Results by Sample
Sample Delivery Group 1012015
Client Sample ID C8 Laboratory Sample ID 1012015 02
Sample Description ATK DLV Goundwater Fall 2010
DateSampled 12/13/10 13 20
CAS Number Test Parameter Result Units MDL
Dilution
EQL Factor Analvst Test Date
Test Method EPA 314 0 Perchlorate on Chromatography
014797 73 0 PERCHLORATE 7 ug/L 1 4 1 JMM 12/16/10
Test Mefhod SW 846, 8260B (Water) Volatile Organic Analysis
67 64 1 ACETONE U ug/L 5 10 1 QC 12/15/10
107 02 8 ACROLEIN U ug/L 6 10 1 QC 12/15/10
71 43 2 BENZENE u ug/L 0 22 10 1 QC 12/15/10
75 27 4 BROMODICHLOROMETHANE u ug/L 0 19 10 1 QC 12/15/10
75 25 2 BROMOFORM u ug/L 0 42 10 1 QC 12/15/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 12/15/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 12/15/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 12/15/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 12/15/10
108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 QC 12/15/10
75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 12/15/10
67 66 3 CHLOROFORM u ug/L 0 3 10 1 QC 12/15/10
74-87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 12/15/10
124-48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 12/15/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 12/15/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 12/15/10
75 35 4 1 1 DICHLOROETHENE u ug/L 0 16 10 1 QC 12/15/10
156 59 4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 12/15/10
156 60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 QC 12/15/10
78-87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 12/15/10
10061-01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/15/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/15/10
100-41 4 ETHYLBENZENE u ug/L 0 16 10 1 QC 12/15/10
591 78 5 2 HEXANONE u ug/L 0 7 10 1 QC 12/15/10
75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 12/15/10
108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 12/15/10
100-42 5 STYRENE u ug/L 0 3 10 1 QC 12/15/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 12/15/10
127 18-4 TETRACHLOROETHENE u ug/L 04 10 1 QC 12/16/10
108 88 3 TOLUENE u ug/L 0 5 10 1 QC 12/15/10
71 55-6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 12/15/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 12/15/10
79 01-6 TRICHLOROETHENE u ug/L 07 10 1 QC 12/15/10
75 69-4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 12/15/10
108-05 4 VINYL ACETATE u ug/L 20 50 1 QC 12/15/10
75 01-4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 12/15/10
1330 20 7 m p XYLENE u ug/L 06 10 1 QC 12/15/10
95-47 6 0 XYLENE u ug/L 0 3 10 1 QC 12/15/10
17060-07 0 1 2 DICHLOROETHANE D4 96 8 % 1 QC 12/15/10
460 00 4 BROMOFLUOROBENZENE 98 2 % 1 QC 12/15/10
2037 26 5 TOLUENE D8 90 3 % 1 QC 12/15/10
1868 53 7 DIBROMOFLUOROMETHANE 102 % 1 QC 12/15/10
Page 5 of 11
Pnnted 01/14/1114 02
Listing of Results by Sample
Sample Delivery Group 1012015
Client Sample ID C 8A Laboratory Sample ID 1012015 03
Sample Description ATK DLV Goundwater Fall 2010
Date Sampled 12/13/10 13 20
CAS Number Test Parameter Result Units MDL
Dilution
EQL Factor Analvst Test Date
TestMet/iod EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE 7 ug/L 1 4 1 JMM 12/16/10
Test Method SW 846 8260B (Water) Volatile Org: inic Analysis
67 64 1 ACETONE U ug/L 5 10 1 QC 12/15/10
107 02 8 ACROLEIN U ug/L 6 10 1 QC 12/15/10
71-43 2 BENZENE u ug/L 0 22 10 1 QC 12/15/10
75 27-4 BROMODICHLOROMETHANE u ug/L 0 19 10 1 QC 12/15/10
75 25 2 BROMOFORM u ug/L 0 42 10 1 QC 12/15/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 12/15/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 12/15/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 12/15/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 12/15/10
108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 QC 12/15/10
75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 12/15/10
67 66 3 CHLOROFORM u ug/L 0 3 10 1 QC 12/15/10
74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 12/15/10
124 48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 12/15/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 12/15/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 12/15/10
75 35-4 1 1 DICHLOROETHENE u ug/L 0 16 10 1 QC 12/15/10
156 59 4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 12/15/10
156 60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 QC 12/15/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 12/15/10
10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/15/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/15/10
100 41-4 ETHYLBENZENE u ug/L 0 16 10 1 QC 12/15/10
591 78 6 2 HEXANONE u ug/L 07 10 1 QC 12/15/10
75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 12/15/10
108 10-1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 12/15/10
100-42 5 STYRENE u ug/L 0 3 10 1 QC 12/15/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 12/15/10
127 18 4 TETRACHLOROETHENE u ug/L 04 10 1 QC 12/15/10
108 88 3 TOLUENE u ug/L 0 5 10 1 QC 12/15/10
71 55 6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 12/15/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 12/15/10
79 01 6 TRICHLOROETHENE u ug/L 0 7 10 1 QC 12/15/10
75 69-4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 12/15/10
108 05 4 VINYL ACETATE u ug/L 20 50 1 QC 12/15/10
75 01-4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 12/15/10
1330 20 7 m p XYLENE u ug/L 0 6 10 1 QC 12/15/10
95-47 6 0 XYLENE u ug/L 0 3 10 1 QC 12/15/10
17060 07 0 1 2 DICHLOROETHANE D4 98 4 % 1 QC 12/15/10
460 00 4 BROMOFLUOROBENZENE 95 9 % 1 QC 12/15/10
2037 26 5 TOLUENE D8 90 5 % 1 QC 12/15/10
1868 53 7 DIBROMOFLUOROMETHANE 103 % 1 QC 12/15/10
Page 6 Of 11
Pnnted 01/14/11 14 02
Listing of Results by Sample
Sample Delivery Group 1012015
Client Sample ID FBI Laboratory Sample ID 1012015 04
Sample Description ATK-DLV - Goundwater Fall 2010
DateSampled 12/13/10 13 20
CAS Number Test Parameter Result Units MDL
Dilution
EQL Factor Analvst Test Date
Tesf Method EPA 3140 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE u ug/L 1 4 1 JMM 12/16/10
Tesf Method SW 846 82606 (Water) Volatile Organic Analysis
67 64 1 ACETONE u ug/L 5 10 1 QC 12/15/10
107 02 8 ACROLEIN u ug/L 6 10 1 QC 12/15/10
71 43 2 BENZENE u ug/L 0 22 10 1 QC 12/15/10
75 27-4 BROMODICHLOROMETHANE u ug/L 0 19 10 1 QC 12/15/10
75 25 2 BROMOFORM u ug/L 0 42 10 1 QC 12/15/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 12/15/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 12/15/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 12/15/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 12/15/10
108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 QC 12/15/10
75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 12/15/10
67 66 3 CHLOROFORM u ug/L 0 3 10 1 QC 12/15/10
74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 12/15/10
124 48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 12/15/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 12/15/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 12/15/10
75 35-4 1 1 DICHLOROETHENE u ug/L 0 16 10 1 QC 12/15/10
156 59-4 CIS 1 2-DICHLOROETHENE u ug/L 0 16 10 1 QC 12/15/10
156 60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 QC 12/15/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 12/15/10
10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 0 4 10 1 QC 12/15/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/15/10
100-41-4 ETHYLBENZENE u ug/L 0 16 10 1 QC 12/15/10
591 78 6 2 HEXANONE u ug/L 0 7 10 1 QC 12/15/10
75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 12/15/10
108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 12/15/10
100-42 5 STYRENE u ug/L 03 10 1 QC 12/15/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 12/15/10
127 18-4 TETRACHLOROETHENE u ug/L 04 10 1 QC 12/15/10
108 88 3 TOLUENE u ug/L 0 5 10 1 QC 12/15/10
71 55-6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 12/15/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 12/15/10
79 01-6 TRICHLOROETHENE u ug/L 07 10 1 QC 12/15/10
75 69-4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 12/15/10
108 05 4 VINYL ACETATE u ug/L 20 50 1 QC 12/15/10
75 01-4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 12/15/10
1330 20 7 m p XYLENE u ug/L 06 10 1 QC 12/15/10
95-47-6 0 XYLENE u ug/L 0 3 10 1 QC 12/15/10
17060 07 0 1 2 DICHLOROETHANE D4 97 9 % 1 QC 12/15/10
460 00 4 BROMOFLUOROBENZENE 95 2 % 1 QC 12/15/10
2037 26 5 TOLUENE D8 87 9 % 1 QC 12/15/10
1868 53 7 DIBROMOFLUOROMETHANE 104 % 1 QC 12/15/10
Page 7 of 11
Pnnted 01/14/1114 02
Listing of Results by Sample
Sample Delivery Group 1012015
Client Sample ID TB 1 Laboratory Sample ID 1012015 05
Sample Description ATK DLV Goundwater Fall 2010
DateSampled 12/13/10 13 20
CAS Number Test Parameter Result Units MDL
Dilution
EQL Factor Analvst Test Date
Tesf Method EPA 314 0 Perchlorate Ion Chromatography
MDL
014797 73 0 PERCHLORATE u ug/L 1 4 1 JMM 12/16/10
Test Method SW 846 8260B (Water) Volatile Organic Analysis
67 64 1 ACETONE u ug/L 5 10 1 QC 12/15/10
107 02 8 ACROLEIN u ug/L 6 10 1 QC 12/15/10
71^3 2 BENZENE u ug/L 0 22 10 1 QC 12/15/10
75 27 4 BROMODICHLOROMETHANE u ug/L 0 19 10 1 QC 12/15/10
75 25 2 BROMOFORM u ug/L 0 42 10 1 QC 12/15/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 12/15/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 12/15/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 12/15/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 12/15/10
108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 QC 12/15/10
75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 12/15/10
67 66 3 CHLOROFORM u ug/L 0 3 10 1 QC 12/15/10
74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 12/15/10
124^8 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 12/15/10
75-34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 12/15/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 12/15/10
75 35 4 1 1 DICHLOROETHENE u ug/L 0 16 10 1 QC 12/15/10
156 59 4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 12/15/10
156 60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 QC 12/15/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 12/15/10
10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 0 4 10 1 QC 12/15/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 0 4 10 1 QC 12/15/10
100 41 4 ETHYLBENZENE u ug/L 0 16 10 1 QC 12/15/10
591 78 6 2 HEXANONE u ug/L 07 10 1 QC 12/15/10
75-09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 12/15/10
108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 12/15/10
100^2 5 STYRENE u ug/L 0 3 10 1 QC 12/15/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 12/15/10
127 18 4 TETRACHLOROETHENE u ug/L 04 10 1 QC 12/15/10
108-88 3 TOLUENE u ug/L 05 10 1 QC 12/15/10
71-55 6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 12/15/10
79-00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 12/15/10
79-01 6 TRICHLOROETHENE u ug/L 0 7 10 1 QC 12/15/10
75-69 4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 12/15/10
108 05 4 VINYL ACETATE u ug/L 20 50 1 QC 12/15/10
75 01 4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 12/15/10
1330 20 7 m p XYLENE u ug/L 06 10 1 QC 12/15/10
95 47 6 0 XYLENE u ug/L 0 3 10 1 QC 12/15/10
17060 07 0 1 2 DICHLOROETHANE-D4 98 5 % 1 QC 12/15/10
460 00 4 BROMOFLUOROBENZENE 94 6 % 1 QC 12/15/10
2037 26 5 TOLUENE D8 88 8 % 1 QC 12/15/10
1868 53 7 DIBROMOFLUOROMETHANE 104 % 1 QC 12/15/10
Page 8 of 11
Pnnted 01/14/1114 02
Listing of Results by Sample
Sample Delivery Group 1012015
Client Sample ID C7 Laboratory Sample ID 1012015 06
Date Sampled 12/13/10 13 20
Sample Description ATK DLV Goundwater Fall 2010
Dilution
CAS Number Test Parameter Result Units MDL EQL Factor Analvst Test Date
Tesf Method EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE 102 ug/L 5 20 5 JMM 12/16/10
Tesf Method SIV 846, 8260S (Waferj Volatile Organic Analysis
67 64 1 ACETONE U ug/L 5 10 1 QC 12/15/10
107 02 8 ACROLEIN U ug/L 6 10 1 QC 12/15/10
71-43 2 BENZENE U ug/L 0 22 10 1 QC 12/15/10
75 27 4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 12/15/10
75 25 2 BROMOFORM U ug/L 0 42 10 1 QC 12/15/10
74 83 9 BROMOMETHANE U ug/L 0 57 10 1 QC 12/15/10
78 93 3 2 BUTANONE U ug/L 1 11 10 1 QC 12/15/10
75 15 0 CARBON DISULFIDE U ug/L 0 13 10 1 QC 12/15/10
56 23 5 CARBON TETRACHLORIDE U ug/L 0 27 10 1 QC 12/15/10
108 90 7 CHLOROBENZENE U ug/L 0 16 10 1 QC 12/15/10
75 00 3 CHLOROETHANE U ug/L 0 35 10 1 QC 12/15/10
67 66 3 CHLOROFORM U ug/L 0 3 10 1 QC 12/15/10
74 87 3 CHLOROMETHANE U ug/L 0 81 10 1 QC 12/15/10
124 48 1 DIBROMOCHLOROMETHANE U ug/L 0 18 10 1 QC 12/15/10
75 34 3 1 1 DICHLOROETHANE U ug/L 0 49 10 1 QC 12/15/10
107 06 2 1 2 DICHLOROETHANE U ug/L 0 29 10 1 QC 12/15/10
75 35-4 1 1 DICHLOROETHENE U ug/L 0 16 10 1 QC 12/15/10
156 59 4 CIS 1 2-DICHLOROETHENE U ug/L 0 16 10 1 QC 12/15/10
156 60 5 TRANS 1 2 DICHLOROETHENE U ug/L 0 34 10 1 QC 12/15/10
78 87 5 1 2 DICHLOROPROPANE U ug/L 0 16 10 1 QC 12/15/10
10061 01 5 CIS 1 3 DICHLOROPROPENE U ug/L 0 4 10 1 QC 12/15/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE U ug/L 0 4 10 1 QC 12/15/10
100-41-4 ETHYLBENZENE U ug/L 0 16 10 1 QC 12/15/10
591 78 6 2 HEXANONE u ug/L 0 7 10 1 QC 12/15/10
75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 12/15/10
108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 12/15/10
100 42 5 STYRENE u ug/L 0 3 10 1 QC 12/15/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 12/15/10
127 18 4 TETRACHLOROETHENE u ug/L 0 4 10 1 QC 12/15/10
108 88 3 TOLUENE u ug/L 0 5 10 1 QC 12/15/10
71 55 6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 12/15/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 12/15/10
79 01 6 TRICHLOROETHENE u ug/L 0 7 10 1 QC 12/15/10
75 69 4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 12/15/10
108 05-4 VINYL ACETATE u ug/L 20 50 1 QC 12/15/10
75 01 4 VINYL CHLORIDE u ug/L 03 10 1 QC 12/15/10
1330 20 7 m p XYLENE u ug/L 0 6 10 1 QC 12/15/10
95-47 6 0 XYLENE u ug/L 0 3 10 1 QC 12/15/10
17060 07 0 1 2 DICHLOROETHANE D4 98 2 % 1 QC 12/15/10
460 00 4 BROMOFLUOROBENZENE 93 9 % 1 QC 12/15/10
2037 26 5 TOLUENE D8 89 7 % 1 QC 12/15/10
1868 53 7 DIBROMOFLUOROMETHANE 103 % 1 QC 12/15/10
Page 9 of 11
Pnnted 01/14/1114 02
Listing of Results by Sample
Sample Delivery Group 1012015
Client Sample ID C 7A Laboratory Sample ID 1012015 07
DateSampled 12/13/10 13 20
Sample Description ATK DLV Goundwater Fall 2010
Dilution
CAS Number Test Parameter Result Units MDL EQL Factor Analvst Test Date
Test Method EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE 97 ug/L 5 20 5 JMM 12/16/10
Tesf Method SIV 846, 8260S CWaferj Volatile Organic Analysis
67 64 1 ACETONE U ug/L 5 10 1 QC 12/15/10
107 02 8 ACROLEIN U ug/L 6 10 1 QC 12/15/10
71 43 2 BENZENE U ug/L 0 22 10 1 QC 12/15/10
75 27 4 BROMODICHLOROMETHANE u ug/L 0 19 10 1 QC 12/15/10
75 25 2 BROMOFORM u ug/L 0 42 10 1 QC 12/15/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 12/15/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 12/15/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 12/15/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 12/15/10
108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 QC 12/15/10
75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 12/15/10
67 66 3 CHLOROFORM u ug/L 0 3 10 1 QC 12/15/10
74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 12/15/10
124 48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 12/15/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 12/15/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 12/15/10
75 35 4 1 1 DICHLOROETHENE u ug/L 0 16 10 1 QC 12/15/10
156 59 4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 12/15/10
156 60 5 TRANS-1 2 DICHLOROETHENE u ug/L 0 34 10 1 QC 12/15/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 12/15/10
10061 01 5 CIS 1 3-DICHLOROPROPENE u ug/L 0 4 10 1 QC 12/15/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/15/10
100 41-4 ETHYLBENZENE u ug/L 0 16 10 1 QC 12/15/10
591 78 6 2 HEXANONE u ug/L 0 7 10 1 QC 12/15/10
75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 12/15/10
108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 12/15/10
100^2-5 STYRENE u ug/L 0 3 10 1 QC 12/15/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 12/15/10
127 18 4 TETRACHLOROETHENE u ug/L 04 10 1 QC 12/15/10
108 88 3 TOLUENE u ug/L 0 5 10 1 QC 12/15/10
71 55 6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 12/15/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 12/15/10
79 01 6 TRICHLOROETHENE u ug/L 0 7 10 1 QC 12/15/10
75 69 4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 12/15/10
108 05-4 VINYL ACETATE u ug/L 20 50 1 QC 12/15/10
75 01^ VINYL CHLORIDE u ug/L 0 3 10 1 QC 12/15/10
1330 20 7 mp XYLENE u ug/L 0 6 10 1 QC 12/15/10
95^7 6 0 XYLENE u ug/L 0 3 10 1 QC 12/15/10
17060 07 0 1 2 DICHLOROETHANE D4 97 8 % 1 QC 12/15/10
460 00 4 BROMOFLUOROBENZENE 95 3 % 1 QC 12/15/10
2037 26 5 TOLUENE D8 89 % 1 QC 12/15/10
1868 53 7 DIBROMOFLUOROMETHANE 104 % 1 QC 12/15/10
Page 10 of 11
Pnnted 01/14/1114 02
Data Reporting Qualifiers
Indicates that the analyte concentration is less than the MDL
This flag is used when an analyte is found in the blank as well as the sample
Indicates an extimated value This flag is used either when estimating a concentration
for tentatively identified compounds or when the data indicated the presence of a
compound that meets the identification criteria but the result is less than the
EQL (e g 3 J with an EQL of 10)
MDL Method Detection Limit The minimum concentration of a substance that can be
confidently measured and reported The laboratory has demonstrated that the
MDL can be achieved in a laboratory reagent blank but does not guarantee it
can be achieved in all sample matrices
EQL Estimated Quantitation Limit The EQL generally is 5 to 10 times the MDL For
many analytes the EQL is selected as the value of the lowest standard in the
calibration curve
Dilution Dilution Factor The prepared sample was diluted by this factor because the
Factor sample was too concentrated or due to other interferences in the sample matnx
Any dilution factor causes a corresponding increase in the MDL and EQL
Page 11 of 11
Pnnted 01/14/1114 02
ATK Launch Systems
Environmental Laboratory
Client Name
Sample Receipt Checklist
SDG No
Camer_
• Hand delivered no cooler Camer Number
l>fland delivered sample(s) taken out at receiving counter
Cooler Information
Cooler NumberJIO
Condition of Shipping Container
Cooler Sealed (taped)
Custody Seals Present
Coolant
State of Coolant
Thermometer ID
Packing Descnption
•Yes
•Yes
Qlnteet
OfTOzen
Reading _
DFair •Not Applicable
•Not Applicable
•Not Applicable
•Broken
•Blue Ice ONone
•Partially Frozen DMelted
C CF ~-
DDamaged (explain).
Seal Number.
Other
Connected Temp _ Temp Blank Included OYes
Chain-Of-Custody Informafaon
COC Present ,2^//
COCNumber(s) C
COC signed (relinquished and received)
COC or LWI agrees with sample labels
•No
•No
•No
Notes
Other
•Not Applicable
•Not Ajiplicable
Sample Infonnation
Samples included In cooler
Custody Seals PresenL
Sample container intacL
Samples In proper containers
SufHaent sample volume
All samples received in hold bme'
Water - VO/^»rave zero headspace
ppre-pneserved with HCl
Notes-
OYes
•Intact
z
IQo
•Broken
ONo
•No
ONo
ONo^
Other
Seal Numbet^s) _
Notes
\j^es ONo ONot Applicable
•Pre-preserved with Na2S20]. DNon-Preserved
Bl^otAj Water - pH acceptable upon receipt • Yes
HN03 = H,SO, =
•Adjusted (see comments below) BNot Applicable
NaOH= ^ZnAC/NaOH = HCL =
Water-pH adjusted (mfg & Lot No)
HNO3 ^HjSO^
NajSOjOj Other.
Notes
NaOH. ZnAC HCl
SOP-102 Foim A
1012027
ENVIRONMENTAL LAB WORK REQUEST
™' ATK ENVIRONMENTAL LABORATORY LWR No
Login No
E13219
FROM EXTENSION COST CENTER WORKORDER DATE
ORCAMZATION MAIL STOP
MS
REPORT RESULTS TO
HELEN RAVSTEN, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS SAMPLE DATE
G c
LOCATION TIME TEST REMARKS
/Z'SO l/cc- fj2jCdO, cu^H - sm o A yon
^/F&-^ izlzi/to y /Z)^0 ll It It It
ti 1' ft ll
4
5
6
7
8
9
10
U
12
CHAIN OF CUSTODY
^^el^QUISHED^Y DATE TIME RECEIVED BY DATE TIME
lz/z///o
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED SIGNATURE
988P LS333 GW
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Requested
Friday, January 14, 2011
TESTED FOR ATK DLV
Environmental Monitonng
Thiokol Corp, UT 84322
ANALYZED BY. ATK Launch Systems
Analytical Chemistry Laboratory
P O Box 707, M/S 245
Bngham City, UT 84302-0707
435-863-3732
435-863-8080
Contact Name:
Project.
Sample Delivery Group
Al Lee
Ground Water Testing - DLV
1012027
Page 1 of 6
Pnnted 01/14/1114 02
Sample Delivery Group 1012027
Sample No Client No Received Collect Date/Time
Test Requested Sample Description Matrix
1012027 01 LF3 12/21/10 12/21/2010 10 30 0
EPA 314 0
SW 846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
1012027 02 FB2 12/21/10 12/21/2010 10 40 0
EPA 314 0
SW 846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
1012027 03 TB 2 12/21/10 12/21/2010 10 450
EPA 314 0
SW 846 8260B (Water)
Perchlorate Ion Chromatography
Volatile Organic Analysis
Water
Water
Certified By /( 01/14/2011
W Scott Fraser Quality Assurance Officer Date
This certifies that the following data meets the requirements ofthe National Environmental Laboratory Accreditation
Program (NELAP) unless otherwise annotated
Page 2 of 6
Pnnted 01/14/1114 02
Listing of Results by Sample
Sample Delivery Group 1012027
Client Sample ID LF 3 Laboratory Sample ID 1012027 01
Sample Description ATK DLV Groundwater Fall 2010
Date Sampled 12/21/10 10 30
CAS Number Test Parameter Result Units MDL
Dilution
EQL Factor Analvst Test Date
Test Method EPA 314 0 Perchlorate Ion Chronnatography
014797 73 0 PERCHLORATE u ug/L 1 4 1 PCI 01/05/11
Test Method SIV 846, 8260S (Water) Volatile Organic Analysis
67-64 1 ACETONE u ug/L 5 10 1 QC 12/22/10
107 02 8 ACROLEIN u ug/L 5 10 1 QC 12/22/10
71 43 2 BENZENE u ug/L 0 22 10 1 QC 12/22/10
75 27-4 BROMODICHLOROMETHANE u ug/L 0 19 10 1 QC 12/22/10
75 25 2 BROMOFORM u ug/L 0 42 10 1 QC 12/22/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 12/22/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 12/22/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 12/22/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 12/22/10
108 90 7 CHLOROBENZENE 02 J ug/L 0 16 10 1 QC 12/22/10
75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 12/22/10
67 66 3 CHLOROFORM u ug/L 0 3 10 1 QC 12/22/10
74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 12/22/10
124 48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 12/22/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 12/22/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 12/22/10
75 35-4 1 1 DICHLOROETHENE OSJ ug/L 0 16 10 1 QC 12/22/10
156 59-4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 12/22/10
156 60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 QC 12/22/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 12/22/10
10061 01 5 CIS 1 3-DICHLOROPROPENE u ug/L 04 10 1 QC 12/22/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/22/10
100-41 4 ETHYLBENZENE u ug/L 0 16 10 1 QC 12/22/10
591 78 6 2 HEXANONE u ug/L 0 7 10 1 QC 12/22/10
75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 12/22/10
108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 12/22/10
100-42 5 STYRENE u ug/L 0 3 10 1 QC 12/22/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 12/22/10
127 18 4 TETRACHLOROETHENE u ug/L 04 10 1 QC 12/22/10
108 88 3 TOLUENE u ug/L 0 5 10 1 QC 12/22/10
71 55 6 1 1 1 TRICHLOROETHANE 04 J ug/L 0 16 10 1 QC 12/22/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 12/22/10
79-01-6 TRICHLOROETHENE u ug/L 07 10 1 QC 12/22/10
75 69-4 TRICHLOROFLUOROMETHANE OSJ ug/L 0 3 10 1 QC 12/22/10
108 05 4 VINYL ACETATE u ug/L 20 50 1 QC 12/22/10
75 01 4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 12/22/10
1330 20 7 m p XYLENE u ug/L 06 10 1 QC 12/22/10
95 47 6 o-XYLENE u ug/L 03 10 1 QC 12/22/10
17060 07 0 1 2 DICHLOROETHANE D4 100 % 1 QC 12/22/10
460 00 4 BROMOFLUOROBENZENE 101 % 1 QC 12/22/10
2037 26 5 TOLUENE D8 95 4 % 1 QC 12/22/10
1868 53 7 DIBROMOFLUOROMETHANE 97 5 % 1 QC 12/22/10
Pnnted
Page 3 of 6
01/14/11 14 02
Listing of Results by Sample
Sample Delivery Group 1012027
Ghent Sample ID FB 2 Laboratory Sample ID 1012027 02
Sample Description ATK DLV Groundwater Fall 2010
DateSampled 12/21/10 10 40
CAS Number Test Parameter Result Units MDL
Dilution
EQL Factor Analvst Test Date
Test Method EPA3140 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE u ug/L 1 4 1 PCI 01/05/11
Tesf Method S1V846, 8260B (Water) Volatile Organic Analysis
67 64 1 ACETONE u ug/L 5 10 1 QC 12/22/10
107 02 8 ACROLEIN u ug/L 6 10 1 QC 12/22/10
71 43 2 BENZENE u ug/L 0 22 10 1 QC 12/22/10
75 27 4 BROMODICHLOROMETHANE u ug/L 0 19 10 1 QC 12/22/10
75 25 2 BROMOFORM u ug/L 0 42 10 1 QC 12/22/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 12/22/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 12/22/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 12/22/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 12/22/10
108 90 7 CHLOROBENZENE 0 2 J ug/L 0 16 10 1 QC 12/22/10
75-00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 12/22/10
67 66 3 CHLOROFORM u ug/L 0 3 10 1 QC 12/22/10
74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 12/22/10
124 48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 12/22/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 12/22/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 12/22/10
75 35 4 1 1 DICHLOROETHENE u ug/L 0 16 10 1 QC 12/22/10
156 59 4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 12/22/10
156 60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 QC 12/22/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 12/22/10
10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/22/10
10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/22/10
100-41-4 ETHYLBENZENE u ug/L 0 16 10 1 QC 12/22/10
591 78 6 2 HEXANONE u ug/L 0 7 10 1 QC 12/22/10
75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 12/22/10
108 10 1 4 METHYL-2 PENTANONE u ug/L 0 53 10 1 QC 12/22/10
100-42 5 STYRENE u ug/L 0 3 10 1 QC 12/22/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 12/22/10
127 18 4 TETRACHLOROETHENE u ug/L 04 10 1 QC 12/22/10
108 88 3 TOLUENE u ug/L 0 5 10 1 QC 12/22/10
71 55-6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 12/22/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 12/22/10
79 01 6 TRICHLOROETHENE u ug/L 07 10 1 QC 12/22/10
75 69 4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 12/22/10
108 05 4 VINYL ACETATE u ug/L 20 50 1 QC 12/22/10
75 01-4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 12/22/10
1330 20 7 m p XYLENE u ug/L 06 10 1 QC 12/22/10
95-47-6 0 XYLENE u ug/L 0 3 10 1 QC 12/22/10
17060 07 0 1 2 DICHLOROETHANE D4 100 % 1 QC 12/22/10
460 00 4 BROMOFLUOROBENZENE 102 % 1 QC 12/22/10
2037 26 5 TOLUENE D8 95 2 % 1 QC 12/22/10
1868 53 7 DIBROMOFLUOROMETHANE 99 % 1 QC 12/22/10
Pnnted
Page 4 of 6
01/14/11 14 02
Listing of Results by Sample
Sample Delivery Group 1012027
Client Sample ID TB 2 Laboratory Sample ID 1012027 03
Date Sampled 12/21/10 10 45
Sample Description ATK DLV Groundwater Fall 2010
Date Sampled
Dilution
CAS Number Test Parameter Result Units MDL EQL Factor Analvst Test Date
Test Method EPA 314 0 Perchlorate Ion Chromatography
014797 73 0 PERCHLORATE U ug/L 1 4 1 PCI 01/05/11
Test Method SW 846, 82606 (Water) Volatile Organic Analysis
67 64 1 ACETONE U ug/L 5 10 1 QC 12/22/10
107 02 8 ACROLEIN U ug/L 6 10 1 QC 12/22/10
71-43 2 BENZENE U ug/L 0 22 10 1 QC 12/22/10
75 27-4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 12/22/10
75 25 2 BROMOFORM u ug/L 0 42 10 1 QC 12/22/10
74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 12/22/10
78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 12/22/10
75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 12/22/10
56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 12/22/10
108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 QC 12/22/10
75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 12/22/10
67 66 3 CHLOROFORM 0 3 J ug/L 0 3 10 1 QC 12/22/10
74-87 3 CHLOROMETHANE U ug/L 0 81 10 1 QC 12/22/10
124 48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 12/22/10
75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 12/22/10
107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 12/22/10
75 35-4 1 1 DICHLOROETHENE u ug/L 0 16 10 1 QC 12/22/10
156 59 4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 12/22/10
156 60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 QC 12/22/10
78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 12/22/10
10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/22/10
10061-02-6 TRANS-1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 12/22/10
100-41 4 ETHYLBENZENE u ug/L 0 16 10 1 QC 12/22/10
591 78 6 2 HEXANONE u ug/L 0 7 10 1 QC 12/22/10
75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 12/22/10
108 10 1 4 METHYL 2-PENTANONE u ug/L 0 53 10 1 QC 12/22/10
100-42 5 STYRENE u ug/L 0 3 10 1 QC 12/22/10
79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 12/22/10
127 18 4 TETRACHLOROETHENE u ug/L 0 4 10 1 QC 12/22/10
108 88 3 TOLUENE u ug/L 0 5 10 1 QC 12/22/10
71 55-6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 12/22/10
79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 12/22/10
79 01-6 TRICHLOROETHENE u ug/L 07 10 1 QC 12/22/10
75 69-4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 12/22/10
108 05-4 VINYL ACETATE u ug/L 20 50 1 QC 12/22/10
75 01-4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 12/22/10
1330 20 7 m p XYLENE u ug/L 06 10 1 QC 12/22/10
95-47 6 0 XYLENE u ug/L 0 3 10 1 QC 12/22/10
17060 07 0 1 2 DICHLOROETHANE D4 98 8 % 1 QC 12/22/10
460 00-4 BROMOFLUOROBENZENE 101 % 1 QC 12/22/10
2037 26 5 TOLUENE D8 95 5 % 1 QC 12/22/10
1868 53 7 DIBROMOFLUOROMETHANE 98 8 % 1 QC 12/22/10
Pnnted
Page 5 of 6
01/14/11 14 02
Data Reporting Qualifiers
Indicates that the analyte concentration is less than the MDL
This flag is used when an analyte is found in the blank as well as the sample
Indicates an extimated value This flag is used either when estimating a concentration
for tentatively identified compounds or when the data indicated the presence of a
compound that meets the identification cntena but the result is less than the
EQL (eg 3 J with an EQL of 10)
MDL Method Detection Limit The minimum concentration of a substance that can be
confidently measured and reported The laboratory has demonstrated that the
MDL can be achieved in a laboratory reagent blank but does not guarantee it
can be achieved in all sample matrices
EQL Estimated Quantitation Limit The EQL generally is 5 to 10 times the MDL For
many analytes the EQL is selected as the value of the lowest standard in the
calibration curve
Dilution Dilution Factor The prepared sample was diluted by this factor because the
Factor sample was too concentrated or due to other interferences in the sample matnx
Any dilution factor causes a corresponding increase m the MDL and EQL
Page 6 of 6
Pnnted 01/14/11 14 02
ATK Launch Systems
Environmental Laboratory im
Client Name
Camer
Sample Receipt Ctiecklist
SDG No
Camer Number • Hand delivered ro cooler y^and delivered S3mple(s) taken out at receiving counter
Cooler Information
Cooler Number/ID
Condition of Shipping Container
Cooler Sealed (taped)
Custody Seals Present
(iSood
•Yes
•Yes
Qlntest
Coolant bice
State of Coolant OFrozen
Thermometer 10 Reading _
Packing Descnption
•Fair
JlMo
t^Io'
•Broken
•Blug Ice DNone
BPartially Frozen
_( c CF :
•Not Applicable
•Not Applicable
• Not Applicable
•Damaged (explain) _
Seal Number,
Other
•Melted
Conrected Temp _ Temp Blank Included DYes
Chain-Of-Custody Information
COC Present
COC Number(s).
COC signed (relinquished and received)
COC or LWI agieesvntti sample labels
•No
•No
•No
Other
•Not Applicable
•Not Applicable
Notes
Sample Infomiaiion
Samples induded m cooler
Custody Seals Present
Sample containers intact
Samples m proper containers:
Suffiaent sample volurre
QYes
•Intact
other
All samples received In hold tme. ^es
Water - vOA^Kave zero headspace.
jim«-preseived with HCl
Notes
•Broken Seal Number(s).
•No Notes-
ONo
DNo
•No,
•No ONot Applicable
•Pre-preseived with NajS^Oi. •Non-Preserved
Water- pH acceptable upon receipt IJ|T5 DAdjusted (see comments below) bNot Applicable
HNO3 = HjSO, = NaOH = ^ZnAC /NaOH = . HCL =
Water-pH adjusted (mlg & Lot No)
HNO,_ HiSC.
NajSOjO, .Other.
Notes
NaOH. _ZnAC HCl
SOP-102 Form A
Promontory Post-Closure Permit
Fall 2010 Semi-Annual Report
PLATES
Eartli^x
PROMONTORY FAHUIY ATK LAUNCH SYSTEMS, INC
PROMONTORY FACILITY
PROMONTORY UTAH
PL ATE 2
1,1,-DICHLOROETHANE (DCA)
ISOCONCENTRAHON MAP Eartli^x
PROMONTORY FAHUIY ATK LAUNCH SYSTEMS, INC
PROMONTORY FACILITY
PROMONTORY UTAH
PL ATE 2
1,1,-DICHLOROETHANE (DCA)
ISOCONCENTRAHON MAP Eartli^x ^ ' —TO.™
ATK LAUNCH SYSTEMS, INC
PROMONTORY FACILITY
PROMONTORY UTAH
PL ATE 2
1,1,-DICHLOROETHANE (DCA)
ISOCONCENTRAHON MAP
PROMONTORY FACIUTY ATK LAUNCH SYSTEMS, INC
PROMONTORY. UTAH
PLATE 3
LL-OICHLOROETHENE (DCE)
ISOCONCENTRATION MAP
PROMONTORY FACILITY PLATE 4
1,1,1-TRICHLOROETHANE (TCA)
ISOCONCENTRATION MAP
n PROMONTORY FACIUTY ATK LAUNCH SYSTEMS, INC
PROMONTORY FACIUTY
PLATE 5
TRICHLOROETHENE (TCE)
ISOCONCENTRATION MAP
PROMONTORY FACIUTY ATK LAUNCH SYSTEMS, INC PLAT^ g
PERCHLORATE
ISOCONCENTRATION MAP
EarthFax
PROMONTORY FACIUTl' ATK LAUNCH SYSTEMS, INC
PROMONTORY FAOUTY
PROMONTORY, UTAH
PLATE 7
CHLOROFORM
ISOCONCENTRATION MAP