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DSHW-2010-036326 - 0901a068801b5b01
August 4, 2010 8200-FYl 1-032 AOS 0 5 2010 Mr. Scott T. Anderson, Executive Secretary State of Utah Department of Environmental Quality UTAH DIVISION OF Division of Solid and Hazardous Waste SOLID & HAZARDOUS WASTE 195N.1950 W. 2D\D.DZl?)l P.O. Box 144880 Salt Lake City, Utah 84114-4880 Subject: Submittal of M-136 LTTA Post-closure Permit Semi-Annual Report Promontory Facility, EPA ID #UTD009081357 Dear Mr. Anderson, Enclosed is the submittal of the M-136 Liquid Thermal Treatment Area (LTTA) Post-Closure Permit Semi-Annual Report. The post-closure permit for the M-136 LTA, Sections IV.E.2 and IV.E.3 require semi-annual reports detailing results of sample analyses including concentration of hazardous constituents and a summary of QA/QC data, measurements of static water levels, and total well depths of wells completed in unconsolidated materials. If you have any questions regarding this information, please contact Allen Lee at 801-251-5688. I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Sincerely, David P. Gosen, P.E., Director Environmental Services M-136 LTTA POST-CLOSURE PERMIT 2010 SPRING SEMI-ANNUAL REPORT ATK ATK LAUNCH SYSTEMS Inc. Promontory Facility Box Elder County, Utah EPA ID# UTD009081357 August 2010 Promontory Post-Closure Permit Spring 2010 Semi-Annual Report Preface This is a semi-annual report submitted to the Utah Division of Solid and Hazardous Waste to comply with requirements of the M-136 LTTA Post-Closure Permit. It contains data and information compiled during the first half of 2010 concerning the M-136 Burning Area and LTTA groundwater. This report is meant to be read in conjunction with the previously submitted interim and semiannual reports, and Post-Closure Permit Application. This report is organized into one volume: containing text, figures, and appendices A, B, C andD. August 2010 Promontory Post-Closure Permit Spring 2010 Semi-Annual Report Table of Contents Preface ii Table of Contents iii Plates, Tables, and Appendicies iv 1.0 Ground Water Sampling 1 1.1 Introduction 1 1.2 Analytical Results of Ground Water Sampling 1 2.0 Static Water Levels and Well Depths 3 3.0 Hazardous Plume Characteristics 12 3.1 Tri chloro ethene 12 3.2 1,1,1-Trichloroethane 13 3.3 1,1-Dichloro ethene 13 3.4 1,1-Dichloro ethane 13 3.5 1,1 Dichloroethane 14 3.6 Perchlorate 14 3.7 Cis-l,2-Dichloroethane 14 4.0 Corrective Action Program Effectiveness 15 August 2010 Promontory Post-Closure Permit Spring 2010 Semi-Annual Report Plates, Tables, and Appendices Plates are located in Appendix D. PLATE 1 PLATE 1 Potentiometric Map and Flow Lines (Sheet 1 of 2) Potentiometric Map and Flow Lines (Sheet 2 of 2) TABLE 1 Spring 2010 Water Levels 3 TABLE 2 Depths of Wells Completed in UnconsoHdated Material (Fall 2008) 6 TABLE 3 Summary of Representative Hydraulic Conductivities 7 Appendicies are located following text. APPENDIX A APPENDIX B APPENDIX C APPENDIX D Analytical Data - Volatiles Analytical Data - Perchlorate, HMX, and RDX Raw Anal3^ical Data Plates IV August 2010 Section 1.0 Ground Water Sampling 1.1 Introduction In September 1992, Thiokol Corporation received a post-closure permit for the M-136 Liquid Thermal Treatment Area (LTTA). Sections V.F.3 and V.F.4 of the permit requires submittal of a semiannual report detailing results of sample analyses including concentration of hazardous constituents and a summm^y of QA/QC data, measurements of static water levels, and total well depth estimates. The Spring 2010 sampling effort consisted of ten Wells and four Springs. The ten wells sampled were chosen to help fill the data gaps in completing the ongoing groundwater Human Health Risk Assessment process. Wells and Springs sampled were: A-8, B-2D, B-3, B-6, B-10, D-1, D-4, D-5, G-2, LF-1, Connor Spring, Fork Spring, Pipe Spring and Shotgun Spring. All smnples were analyzed for VOC's and Perchlorate. B-3 was also sampled for HMX and RDX. QA/QC samples were collected from Well G-2. 1.2 Analytical Results of Ground Water Sampling A complete summary of the ground water analytical results, by constituent, are located in Appendices A, B, and C. These Appendices list individual par^neters for each well by constituents, sample number, well number, replicate, aliquot, date, results, and Estimated Quantification Limits or detection limits. Also included in the summary are the data for the field blanks. Appendix C contains the laboratory reports containing the analytical data and QA/QC for ground water samples. Samples were collected, preserved, and transported according to the approved Sampling Plan of the Permit Attachment 4. Samples were analyzed according to USEPA approved methods. All major peaks greater than 25% of the peak height of the closest internal standard are identified to the extent ^alytically possible, using the most current NBS library. One set of field blanks. Trip Blanks and replicates were collected, which represent at a minimum, 10% of the total samples. The laboratory provided method blanks, spikes, and duplicates, and results are located in Appendix C. Qualifiers as defined by the EPA Contract Lab Program were used where applicable (organic analyses). The results reported from the Lab on QA/QC samples detected TCE in samples (TP-OOl-Trip Blank at 15 ppb TCE, and FP-OOl-Field Blank at 8.8J TCE). Talking this issue over with Scott Eraser (Quality Assurance Officer of Lab M-53), Scott explained that this was most likely carry over from the previous sample run of G2A (blind dup of G-2) which was 2230 ppb of TCE. Promontory Post-Closure Permit Spring 2010 Semi-Annual Report Section 2.0 Static Water Levels and Well Depths 2.1 STATIC WATER LEVELS Static water levels for all monitoring wells were measured and recorded during the spring of 2010. The water level measurements collected during the first semi-annual sampling event can be found in Table 1. As shown in Table 1, 82 monitoring wells showed a decrease from 2009 to 2010, 24 wells had an increase from the previous year, and 3 wells were not evaluated due to artesian pressure (BC-1 and BC-5) and the presence of vegetable oil on the water table at well A- 1. Water levels have increased by as much as 3.63 feet at well H-10 and declined by as much as 3.58 feet at well D-1 from the fall of 2009. The decrease in water levels overall at the Promontory facility can be attributed to drought conditions in the west over the past several years. Total well depths of groundwater monitoring wells (taken in the Spring of 2010) that were completed in unconsolidated material are recorded in Table 1. Additionally, Table 2 contains a list of monitoring wells that are completed in unconsolidated material at the Promontory Facility and the associated measured depth of each well. 2.2 HYDRAULIC CONDUCTIVITIES The hydraulic conductivity for each well was determined from well data collected from ATK reports as well as slug testing conducted during the groundwater flow and contaminant transport modeling effort (December 2005). The measured hydraulic conductivity values for the wells are summarized in Table 3. Measured hydraulic conductivity ranges from 0.05 to 775 ft/day. These data were used to obtain an initial distribution of hydraulic conductivity values, which were modified during calibration of the model. Areas of higher hydraulic conductivity are typically found where faults and/or fracture zones acts as major conduits of groundwater flow and contaminant migration. 2 I Page August 2010 Promontory Post-Closure Permit Spring 2010 Semi-Annual Report TABLE 1 - ATK LAUNCH SYSTEMS PROMONTORY SPRING 2010 WATER LEVELS Elevation 2010 2009 WeU of top Depth to SWL SWL NET No Date of casing Water Elevation Elevation CHANGE A-1 7/9/2010 4625.03 oil/no wl NA 4291.75 NA A-2 7/13/2010 4730.49 171.80 4558.69 4559.12 -0.43 A-3 7/13/2010 4702.71 104.02 4598.69 4598.98 -0.29 A-5 7/9/2010 4618.54 327.88 4290.66 4291.77 -1.11 A-6 7/13/2010 4482.05 189.96 4292.09 4293.23 -1.14 A-7 7/13/2010 4471.15 178.26 4292.89 4293.42 -0.53 A-8 6/4/2010 4486.6 193.26 4293.34 4293.33 0.01 A-9 7/9/2010 4509.8 216.84 4292.96 4293.34 -0.38 A-10 7/13/2010 4772.43 214.07 4558.36 4559.01 -0.65 B-1 7/13/2010 4596.22 305.22 4291.00 4291.95 -0.95 B-2S 7/13/2010 4499.31 207.31 4292.00 4292.42 -0.42 B-21 7/13/2010 4499.31 207.29 4292.02 4292.47 -0.45 B-2D 6/3/2010 4499.31 208.16 4291.15 4292.44 -1.29 B-3 6/2/2010 4610.75 318.70 4292.05 4293.02 -0.97 B-4 7/8/2010 4507.29 216.30 4290.99 4291.18 -0.19 B-5 7/9/2010 4429.09 153.71 4275.38 4275.84 -0.46 B-6 6/3/2010 4367.02 100.01 4267.01 4268.24 -1.23 B-7 6/18/2010 4340.16 72.20 4267.96 4267.74 0.22 B-8 6/18/2010 4363.72 87.49 4276.23 4276.53 -0.30 B-9 7/13/2010 4697.79 136.60 4561.19 4562.17 -0.98 B-10 6/3/2010 4649.06 89.33 4559.73 4561.10 -1.37 BC-1 6/15/2010 4235.43 artesion NA NA NA BC-2 6/18/2010 4298.37 32.88 4265.49 4265.90 -0.41 BC-3 6/18/2010 4287.33 21.20 4266.13 4266.38 -0.25 BC-4 6/18/2010 4271.86 7.75 4264.11 4264.49 -0.38 BC-5 6/15/2010 4253.96 artesion NA NA NA BC-6 6/18/2010 4271.94 7.54 4264.40 4264.80 -0.40 C-1 7/13/2010 4523.73 233.78 4289.95 4290.36 -0.41 C-2 7/13/2010 4584.56 294.40 4290.16 4290.74 -0.58 C-3 7/13/2010 4621.62 330.38 4291.24 4292.32 -1.08 C-4 7/13/2010 4714.68 237.97 4476.71 4476.83 -0.12 C-5 7/13/2010 4448.47 155.32 4293.15 4293.42 -0.27 3 I Page August 2010 Promontory Post-Closure Permit Spring 2010 Semi-Annual Report TABLE 1 - ATK LAUNCH SYSTEMS PROMONTORY SPRING 2010 WATER LEVELS Elevation 2010 2009 Well of top Depth to SWL SWL NET No Date of casing Water Elevation Elevation CHANGE C-6 7/8/2010 4527.02 234.20 4292.82 4293.35 -0.53 C-7 7/15/2010 4379.73 88.06 4291.67 4292.02 -0.35 C-8 7/9/2010 4414.12 121.28 4292.84 4293.11 -0.27 D-1 6/3/2010 4696.93 138.40 4558.53 4562.11 -3.58 D-2 7/13/2010 4605.08 313.65 4291.43 4292.48 -1.05 D-3 7/9/2010 4553.87 259.81 4294.06 4294.74 -0.68 D-4 6/2/2010 4522.35 229.10 4293.25 4294.61 -1.36 D-5 6/2/2010 4524.26 231.91 4292.35 4293.35 -1.00 D-6 7/13/2010 4564.16 272.88 4291.28 4291.69 -0.41 E-1 7/9/2010 4381.06 102.58 4278.48 4278.85 -0.37 E-2 6/18/2010 4372.32 100.95 4271.37 4271.69 -0.32 E-3 6/18/2010 4375.68 108.63 4267.05 4267.36 -0.31 E-4 7/9/2010 4360.16 94.22 4265.94 4266.26 -0.32 E-5 7/9/2010 4344.55 80.20 4264.35 4264.72 -0.37 E-6 7/9/2010 4332.01 67.97 4264.04 4264.53 -0.49 E-7 6/18/2010 4367.11 99.42 4267.69 4268.09 -0.40 E-8 7/8/2010 4462.06 194.60 4267.46 4267.83 -0.37 E-9 7/8/2010 4495.38 202.61 4292.77 4293.17 -0.40 E-10 7/8/2010 4761.21 471.04 4290.17 4290.48 -0.31 EW-6 6/18/2010 4335.25 68.17 4267.08 4267.42 -0.34 F-1 7/9/2010 4378.19 87.58 4290.61 4290.93 -0.32 F-2S 7/9/2010 4382.35 103.82 4278.53 4279.06 -0.53 F-21 7/9/2010 4382.35 103.85 4278.50 4279.00 -0.50 F-2D 7/9/2010 4382.35 92.35 4290.00 4289.40 0.60 F-3 7/8/2010 4362.79 83.35 4279.44 4279.89 -0.45 F-4 7/8/2010 4437.14 169.38 4267.76 4268.09 -0.33 F-5 6/18/2010 4367.23 99.56 4267.67 4268.27 -0.60 G-1 6/18/2010 4352.31 84.25 4268.06 4268.40 -0.34 G-2 6/3/2010 4324.63 58.21 4266.42 4267.62 -1.20 G-3 6/18/2010 4275.89 12.10 4263.79 4264.25 -0.46 G-4 7/13/2010 4330.94 66.98 4263.96 4264.39 -0.43 G-5 7/13/2010 4391.22 131.02 4260.20 4260.74 -0.54 4 I Page August 2010 Promontory Post-Closure Permit Spring 2010 Semi-Annual Report TABLE 1 - ATK LAUNCH SYSTEMS PROMONTORY SPRING 2010 WATER LEVELS Elevation 2010 2009 Well of top Depth to SWL SWL NET No Date of casing Water Elevation Elevation CHANGE G-6 7/13/2010 4325.83 66.37 4259.46 4259.98 -0.52 G-7 7/13/2010 4386.35 127.61 4258.74 4259.19 -0.45 G-8 7/13/2010 4477.81 219.66 4258.15 4258.62 -0.47 H-1 6/18/2010 4294.74 29.28 4265.46 4265.28 0.18 H-2 6/18/2010 4306.83 40.87 4265.96 4265.88 0.08 H-3 6/18/2010 4327.98 61.14 4266.84 4266.66 0.18 H-4 6/18/2010 4354.66 87.00 4267.66 4267.34 0.32 H-5 6/18/2010 4300.15 34.91 4265.24 4265.08 0.16 H-6 6/18/2010 4308.68 44.16 4264.52 4265.18 -0.66 H-7 6/18/2010 4380.62 112.22 4268.40 4268.11 0.29 H-8 6/18/2010 4386.17 105.73 4280.44 4280.25 0.19 H-9 6/18/2010 4259.27 2.25 4257.02 4256.76 0.26 H-10 6/18/2010 4246.27 4.19 4242.08 4238.45 3.63 J-1 7/6/2010 4455.00 121.14 4333.86 4335.73 -1.87 J-2 7/8/2010 4658.58 344.88 4313.70 4311.53 2.17 J-3 7/8/2010 4590.71 123.60 4467.11 4466.58 0.53 J-4 7/9/2010 4560.17 287.86 4272.31 4272.62 -0.31 J-5 7/15/2010 4308.65 49.82 4258.83 4259.44 -0.61 J-6 7/15/2010 4321.70 63.39 4258.31 4258.84 -0.53 J-7 6/28/2010 4448.96 115.63 4333.33 4334.35 -1.02 J-8 6/28/2010 4451.53 119.18 4332.35 4333.49 -1.14 J-9 7/15/2010 4821.89 530.64 4291.25 4289.87 1.38 LF-1 6/2/2010 4421.71 121.80 4299.91 4301.53 -1.62 LF-2 6/28/2010 4434.77 129.98 4304.79 4305.71 -0.92 LF-3 7/8/2010 4419.92 120.25 4299.67 4299.96 -0.29 LF-4 7/9/2010 4453.07 152.72 4300.35 4300.72 -0.37 M39-B1 7/21/2010 4631.88 214.36 4417.52 4416.61 0.91 I\/I114-B1 7/9/2010 4560.14 161.84 4398.30 4398.84 -0.54 I\/I508-B1 7/8/2010 4512.08 160.75 4351.33 4350.94 0.39 M508-1 7/8/2010 4506.68 155.62 4351.06 4349.88 1.18 M508-2 7/8/2010 4514.41 164.47 4349.94 4349.66 0.28 l\/I508-3 7/8/2010 4506.37 154.76 4351.61 4351.01 0.60 5 I Page August 2010 Promontory Post-Closure Permit Spring 2010 Semi-Annual Report TABLE 1 - ATK LAUNCH SYSTEMS PROMONTORY SPRING 2010 WATER LEVELS Elevation 2010 2009 Well of top Depth to SWL SWL NET No Date of casing Water Elevation Elevation CHANGE l\/1508-4 7/8/2010 4511.99 159.70 4352.29 4351.67 0.62 I\/I636-B1 7/9/2010 4656.91 77.14 4579.77 4580.22 -0.45 P-1 7/8/2010 4549.32 203.25 4346.07 4347.95 -1.88 P-2 7/8/2010 4539.21 137.84 4401.37 4401.39 -0.02 P-5 7/8/2010 4498.17 122.74 4375.43 DRY NA P-6 6/28/2010 4540.93 88.15 4452.78 4455.46 -2.68 P-7 6/28/2010 4529.52 79.64 4449.88 4451.61 -1.73 P-8 7/8/2010 4517.8 161.12 4356.68 4356.11 0.57 P-9 7/8/2010 4530.7 175.62 4355.08 4354.46 0.62 T-1 6/18/2010 4365.83 98.02 4267.81 4268.11 -0.30 T-2 7/13/2010 4591.62 300.08 4291.54 4292.60 -1.06 X-4 7/15/2010 4861.35 607.45 4253.90 4254.19 -0.29 X-5 7/15/2010 4491.31 238.10 4253.21 4253.60 -0.39 6 I Page August 2010 Promontory Post-Closure Permit Spring 2010 Semi-Annual Report TABLE 2 Fall 2008 Total Depth of Monitoring Wells Completed in Unconsolidated Material Well Total Depth Well Total Depth Well Total Depth A-7 243.15 G-1 97.59 H-5 47.83 B-5 177.77 CT-2 98.95 H-6 52.90 B-6 125.56 G-3 26.48 H-8 149.52 B-7 97.38 G-4 76.21 H-9 11.97 B-8 112.68 BC-1 64.41 H-10 28.05 C-7 108.36 BC-2 44.49 J-1 144.08 E-1 126.31 BC-3 34.39 J-3 146.43 E-2 120.12 BC-4 76.45 EW-6 206.46 E-4 131.84 BC-5 39.47 M508-1 202.87 E-5 120.36 BC-6 38.40 M508-2 199.30 E-8 225.84 LF-1 136.12 M508-3 202.32 E-9 232.09 LF-2 152.63 M508-4 200.54 F-1 106.32 LF-3 147.65 M508-B1 181.58 F-2A 150.48 P-1 256.71 TCCl 214.05 F-2B 217.05 P-2 178.30 F-2C 318.91 P-5 125.55 F-3 107.48 H-4 102.28 7 I Page August 2010 Promontory Post-Closure Permit Spring 2010 Semi-Annual Report TABLE 3 SUMMARY OF REPRESENTATIVE HYDRAULIC CONDUCTIVITIES Well No. Hydraulic Conductivity (ft/day) Hydraulic Conductivity Range (ft/day) A-1 730 A-2 27 23-31 A-3 54 42-75 A-4 410 350-470 A-5 190 120-260 A-6 360 310-410 A-8 775 650-900 A-9 145 120-170 A-10 15 13-17 B-1 33 26-41 B-3 2.73 2-3.4 B-4 39.82 35.28-44.35 B-5 0.75 0.3-1.1 B-6 470 B-7 4.85 4.2-5.5 B-8 3.11 B-9 2.6 C-1 52 37-70 C-2 510 C-3 30.5 26-35 8 I Page August 2010 Promontory Post-Closure Permit Spring 2010 Semi-Annual Report TABLE 3 (Continued) SUMMARY OF REPRESENTATIVE HYDRAULIC CONDUCTIVITIES Well No. Hydraulic Conductivity (ft/day) Hydraulic Conductivity Range (ft/day) C-4 560 470-650 C-5 4.3 C-6 18 15-30 C-7 250 210-290 C-8 3.45 1-5.9 D-1 54 D-2 552.5 445-660 D-3 2.93 D-4 0.55 D-5 0.26 D-6 92.4 E-1 39.2 36.2-42.2 E-2 89.55 87.0-92.1 E-3 114.05 100.9-127.2 E-4 14.45 13.0-15.9 E-5 23.15 22.2-24.1 E-6 4.95 4.9-5.0 E-7 0.55 0.5-0.6 E-8 10.9 10.7-11.1 9 I Page August 2010 Promontory Post-Closure Permit Spring 2010 Semi-Annual Report TABLE 3 (Continued) SUMMARY OF REPRESENTATIVE HYDRAULIC CONDUCTIVITIES Well No. Hydraulic Conductivity (ft/day) Hydraulic Conductivity Range (ft/day) E-9 0.5 E-10 30.7 30.2-31.2 F-1 16.37 16.13-16.60 F-2A 2.31 2.20-2.41 F-2B 2.07 1.68-2.46 F-2C 0.07 0.052-0.087 F-3 3.73 3.67-3.79 F-4 63.73 62.15-65.30 G-1 16.69 16.26-17.12 G-2 41.38 38.61-44.14 G-3 2.05 1.91-2.18 G-4 40.58 37.96-43.19 G-5 29.43 27.62-31.23 G-6 62.76 57.82-68.44 G-7 7.01 6.85-7.16 G-8 0.34 BC-2 12 BC-3 10 BC-4 1 BC-5 92 10 I Page August 2010 Promontory Post-Closure Permit Spring 2010 Semi-Annual Report TABLE 3 (Continued) SUMMARY OF REPRESENTATIVE HYDRAULIC CONDUCTIVITIES Well No. Hydraulic Conductivity (ft/min) " Hydraulic Conductivity Range (ft/day) BC-6 9 LF-1 4.66 3.08-6.23 LF-2 1.6 LF-3 5.07 4.80-5.33 LF-4 21.25 P-1 0.3 P-2 17 16-18 P-3 63.5 62-65 P-5 6 P-6 24 P-7 37.5 29-46 P-8 38 P-9 32 H-1 0.66 0.62-0.69 H-2 1.38 1.29-1.46 H-3 4.17 H-4 298.73 269.86-327.60 H-5 6.78 5.21-8.35 H-6 1.41 H-7 55.43 54.79-56.07 11 I Page August 2010 Promontory Post-Closure Permit Spring 2010 Semi-Annual Report TABLE 3 (Continued) SUMMARY OF REPRESENTATIVE HYDRAULIC CONDUCTIVITIES Well No. Hydraulic Conductivity (ft/day) Hydraulic Conductivity Range (ft/day) H-8 1.39 H-9 0.11 H-10 0.05 J-1 0.4 0.34-0.46 J-3 0.05 J-4 10.36 5.14-15.58 J-5 311.69 203.76-419.62 J-6 149.4 138.66-160.13 J-7 0.11 0.06-0.15 J-8 0.11 0.06-0.15 J-9 0.029 EW-1 7 EW-6 108.66 X-4 11.5 X-5 1.32 M-508-1 5.6 5.45-5.75 M-508-2 3.15 M-508-3 3.4 3.38-3.42 M-508-4 3.29 2.74-3.83 M-508-B1 0.45 0.45-0.46 TCC-2 0.9 0.46-1.33 (a) The hydraulic conductivity range identifies the results of all testing of the well i.e. the results of a slug and bail test conducted at the same time. 12 I Page August 2010 Promontory Post-Closure Permit Spring 2010 Semi-Annual Report Section 3.0 Hazardous Plume Characteristics Hazardous plumes at M-136 historically have consisted of six volatile organic compounds (other volatile constituents are occasionally found at very low levels in one or more wells). These constituents are trichloroethene (TCE), 1,1,1-trichloroethane (TCA), 1,1-dichloroethene (DCE), 1,1-dichloroethane (DCA), chloroform, and cis-l,2-dichloroethene. In addition to the VOC's, perchlorate is also a contaminant of concern at the facility. These plumes are described below and illustrated in Figures 3.1 through 3.6 of the Fall 2009 Semi-Annual Report that was previously submitted to the Division. 3.1 TRICHLOROETHENE The TCE contamination at the facility consists of four major parts: a major plume south and east of the M-136 burning grounds, a small plume in the perched aquifer centered at well D-1, a plume associated with well B-6 beneath the Administration/ Manufacturing area and, a small plume north and west of the Administration area. In addition, several small plumes are located at the northernmost manufacturing area (previously the U.S.A.F. Plant 78), and the ATK Launch Systems sanitary landfill. The major plume originates in the M-136 Burning Ground source area, and has migrated south and south-southwest with values above 5 mg/1 beyond the ATK Launch Systems property boundary. At the Administration/Manufacturing areas, additional sources (likely buried drain fields) of trichloro ethene have raised mean values in the ground water at wells B-6 and G-2, and E-1. This plume extends beneath adjacent agricultural lands to an unused irrigation well EW-6. EW-6 has seen a significant reduction in the amount of TCE that was once detected (concentrations have dropped from 299 ug/L to 34.1 ug/L.) Eight monitoring wells have been constructed on Mr. Adams property to monitor contaminant migration. Low levels of TCE have been identified in a few of these wells, but none of the wells have been above the MCE of 5 ug/L. The plume in the northern manufacturing area appears to have originated from laboratory wastes associated with a lab located in building E-519. The plume has migrated southwest From P-8 to M508-4. One year ago the level at M508-4 was at 6200 and now is 2350 ug/L. The plume has moved further west to M508-3 which is now at 5810 ug/L, up from a level of 3170 ug/L. The concentration in J-1 has dropped from 477 ug/L to 310 ug/L in the last 6 months. Additional groundwater monitor wells have been installed downgradient of J-1 to determine the area and extent of the plume. There does appear to be some natural attenuation of this plume. 13 I Page August 2010 Promontory Post-Closure Permit Spring 2010 Semi-Annual Report Monitoring Well J-4 located by M-114, has identified a plume that had approximately 7000 ug/1 TCE. In the Fall of 2006 this amount rose to 9000 ug/1 and in the spring of 2007, to 11,700 ug/1, and finally to 14,400 ug/L during the Fall of 2007. Since then, the levels of TCE have significantly dropped to the 3000 to 4000 ug/L range. Passive Soil Gas sampling was used to determine if the TCE was coming from the canyon east of the well. No TCE was detected. In 2009, a new well, J-9 was installed to determine if the TCE contamination was moving East from J-4. Analytical data reported from samples collected from J-9, have shown non-detects for TCE, which demonstrates that the TCE contamination in the J-4 area is being monitored by down gradient wells. In September 2007, 8000 gallons of Vegetable oil was injected in A-1, near the M-136 burning grounds to evaluate enhanced anaerobic bioremediation of perchlorate and solvent contaminated groundwater. Significant reductions of TCE were observed in well A-1. Concentrations of TCE went from 1,210 to 17 ug/L. Reductions have also been noted in some of the wells near A-1. Monitoring is ongoing at the downgradient wells. 3.2 1,1,1-TRICHLOROETHANE The 1,1,1-tri chloro ethane in ground water can be found in two primary plumes. The largest plume is centered on the southeast border of the burning grounds. The highest levels (1090 mg/1) of contamination are in wells C-3 and A-5. A second large plume at well B-5 has almost disappeared in the last decade with concentrations reducing from approximately 15,000 mg/1 in 1990 to 266 mg/1 in 2002 to 48 ug/L in 2008. The 1,1,1-trichloroethane plume has namrally degraded to DCE and then to mostly nonhazardous constituents. The source of this plume is uncertain, but a spill in 1984 at the M-52 degreaser of approximately 1,000 gallons of 1,1,1- trichloro ethane seems to be the likely source. There has been a noted decrease in TCA in the Burning grounds as part of the Bioremediation project. A-1 has reduced from 128 ug/L to ND. Well A-5 has reduced from 5000 to 1020 ug/L. Monitoring will be ongoing as this project continues. 3.3 1,1-DICHLOROETHENE 1,1-Dichloroethene is a breakdown product of 1,1,1-trichloroethane, and is found in the TCA plumes. There are two known 1,1-dichloroethene plumes, one beneath the burning area which extends south of the Administration Building and another very minor plume at well P-6. 3.4 1,1-DICHLOROETHANE Small plumes of 1,1-dichloroethane are centered at wells A-5,C-3, B-5, G-2 and EW-6. 14 I Page August 2010 Promontory Post-Closure Permit Spring 2010 Semi-Annual Report 3.5 CHLOROFORM A chloroform plume is located beneath the M-136 Burning Grounds, and small plumes are centered at wells F-1, B-5 and extend south of the Administration area. Reductions in the M-136- Buming Grounds have been noted; A-5 dropped from 700 ug/L to 473 ug/L. Monitoring well EW6 went from 1.5 ug/L to ND. 3.6 PERCHLORATE Perchlorate plumes are monitored at the facility because of regulatory oversight, and concerns expressed by UDSHW and USEPA Region VIII as part of the ATK Launch Systems CME. Small plumes are found in monitoring wells which access perched aquifers to the east of plant. The major plume extends beneath prior disposal areas in the burning grounds, the perchlorate grind building M-174, the washout building M-115, and the drainfield west of the Administration area. A major source of perchlorate found in Pipe Spring on the southwest plant boundary may be historical disposal of washout waters from MinuteMan production. It is possible that these wastes have migrated southward in perched zones to this spring. ATK has constructed monitoring wells in this area to evaluate this potential. Of note is a substantial fluctuation in perchlorate in Pipe Spring, from approximately a high 440 mg/1 to a recent concentration of 265 ug/1. Reductions are being observed at the Burning grounds with the Remediation project underway. Significant reductions were noted at EW6, which is on Mr. Adams property, as it went from 4000 ug/1 to 1510 ug/1 and is currently at 2040ug/l. 3.7 CIS-l,2-DICHLOROETHENE Cis-l,2-dichloroethene plumes are located beneath prior disposal areas at wells, F-1, G-2 and the burning grounds. Well D-3 in the Burning Grounds was detected at a concentration of 157,000 ug/L. Cis-l,2-dichloroethene is a biological reductive dehalogenation breakdown product of chloroethenes (TCE) and is definitive evidence of natural attenuation by anaerobic bacteria. The significant increases at A-6 are likely due to the bioremediation Project at M-136. Significant reductions have been noted in EW-6 well on the Adams property. It went from 69 ug/1 to 13 ug/1 and has continued to drop to a recent concentration of 11 ug/L. 15 I Page August 2010 Promontory Post-Closure Permit Spring 2010 Semi-Annual Report Section 4.0 Corrective Action Program Effectiveness In December 1992, ATK (then Thiokol) submitted the M-136 Liquid Thermal Treatment Area Corrective Action Plan which describes the installation of wells on the southern plant boundary. These wells are used for corrective action monitoring (to demonstrate the effectiveness of the corrective action program), and to initiate active treatment strategies, if required. Concentration levels of hazardous constituents in groundwater monitoring wells in source areas have generally diminished since disposal practices ceased in fall 1988. Well A-4 reported 47,000 mg/1 TCA and 21,000 mg/1 TCE in October 1988 and has dropped to approximately 2,780 mg/1 TCA and 5,735 mg/1 TCE. Similarly, well A-5 declined from 39,000 mg/1 TCA and 2,300 mg/1 TCE to approximately 1,330 mg/1 TCA and 1,020 mg/1 TCE in spring 2005 and further to 962 ug/1 and 2080 ug/1 TCE in fall 2008. A large TCA plume at well B-5 has mostly disappeared in the last decade from approximately 15,000 mg/1 in 1990 to 48 ug/L in 2008. The source of this plume is uncertain, but a spill in 1984 at the M-52 degreaser of approximately 1,000 gallons of 1,1,1-trichloroethane may have contributed to it. Concentration levels in many wells and contmninated springs downgradient of source areas have been relatively stable and have been trending down. This may indicate attenuation and degradation of constituents is approximately equal to migration from source areas. Well E-5 reported 25 mg/1 TCE in October 2002, only slightly greater than 10 mg/1 TCE reported in spring 1996. Well E-6 reported 77 mg/1 TCE in October 2002, which is up from 31 mg/1 reported in December 1990, but only slightly above 72 mg/1 reported in June 1993, it is currently at 37 ug/L. Well E-9 has been an exception to this general decline ^d reported levels of TCE. Sampling of an old, unused agricultural well (EW-6) on Ray Adams property revealed that TCE and breakdown products and perchlorate have migrated farther off-plant than previously believed. Eight additional monitoring wells have been constructed on Mr. Adams property and two wells downgradient of contaminated springs to evaluate the extent of migration off plant. The sampling of these wells indicates contamination is predominantly moving southeast in fractured carbonates, and only very slowly migrating to the south and west. Cis-l,2-dichloroethene is a biological reductive-dehalogenation breakdown product of chloroethenes (TCE) and is definitive evidence of natural attenuation by anaerobic bacteria. Cis-l,2-dichloroethene has been reported previously, in plumes located at wells B-6, G-2, and F-1. These plumes have substantially diminished as the cis-1,2- dichloroethene is (presumably) converted to ethenes. Promontory Post-Closure Permit Spring 2010 Semi-Annual Report In September 2007, a pilot test was conducted at the Burning Grounds to evaluate enhanced anaerobic bioremediation of Perchlorate and solvent-contaminated groundwater. 8000 gallons of soybean oil along with sodium bromide (used as a tracer) was injected into well A-1 at the burning grounds. Sampling of local wells is ongoing to determine the effectiveness of the treatment. Significant reductions in perchlorate and TCE have been observed in some of the downgradient wells. APPENDIX A ANALYTICAL DATA - VOLATILES This appendix is organized as follows CONSTITUENT - Parameter being analyzed for LOCATION LAB SAMPLE DATE CONC EQL UNIT LAB SAMPLE ID DILUTION Well Number or Spring Number 1,3 = outside laboratory, 4 = ATK Launch Systems Date sample was taken Concentration level of constituent in sample Method reporting limit established by EPA for a given analytical method Unit of measure Unique sample ID number issued by the Lab Dilution of sample s,J50NSTITUENT LAB SAMPLED DATE cmc EQL mm, 4AB SAMPLE ID Dilution 1112 TETRACHLOROETHANE A 8 4 06/04/2010 0 u 10 Ug/L 100601101 1 1,1 1,2 TETRACHLOROETHANE B 10 4 06/03/2010 0 u 10 ug/L 1006010-02 1 1,1 1 2 TETRACHLOROETHANE B-2D 4 06/03/2010 0 u 10 Ug/L 1006010 03 1 1112 TETRACHLOROETHANE B 3 4 06/02/2010 0 u 500 ug/L 1006009 04 50 1,1 1 2-TETRACHLOROETHANE 8 6 4 06/03/2010 0 u 10 ug/L 1006010 08 1 1112 TETRACHLOROETHANE Connor Spring 4 06/01/2010 0 u 10 Ug/L 1006008 01 1 1,1,1,2 TETRACHLOROETHANE D 1 4 06/03/2010 0 u 10 ug/L 1006010-01 1 1112 TETRACHLOROETHANE D 4 4 06/02/2010 0 u 10 ug/L 1006009 02 1 1,1,1,2-TETRACHLOROETHANE D 5 4 06/02/2010 0 u 100 ug/L 1006009 01 10 1,1 1 2 TETRACHLOROETHANE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 1112 TETRACHLOROETHANE FP 001 4 06/03/2010 0 u 10 ug/L 1006010-07 1 1,1,1 2-TETRACHLOROETHANE G 2 4 06/03/2010 0 u 10 ug/L 1006010-04 1 111 2-TETRACHLOROETHANE G2A 4 06/03/2010 0 u 10 ug/L 1006010 05 1 1,11,2 TETRACHLOROETHANE LF 1 4 06/02/2010 0 u 10 ug/L 1006009-03 1 1,1,1 2 TETRACHLOROETHANE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008-03 1 1,1 1 2-TETRACHLOROETHANE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008 04 1 1,1,1 2 TETRACHLOROETHANE TP 001 4 06/03/2010 0 u 10 ug/L 1006010-06 1 111 TRICHLOROETHANE A8 4 06/04/2010 811 500 ug/L 1006011-01 50 1 1,1 TRICHLOROETHANE B-10 4 06/03/2010 0 u 10 ug/L 1006010 02 1 1,1,1-TRICHLOROETHANE B 2D 4 06/03/2010 621 200 ug/L 1006010-03 20 11,1 TRICHLOROETHANE B 3 4 06/02/2010 500 J 500 ug/L 1006009-04 50 111 TRICHLOROETHANE B 6 4 06/03/2010 140 J 200 ug/L 1006010 08 20 1,1,1 TRICHLOROETHANE Connor Spring 4 06/01/2010 0 U 10 ug/L 1006008-01 1 1 1,1 TRICHLOROETHANE D-1 4 06/03/2010 1400 J 2000 ug/L 1006010-01 200 111 TRICHLOROETHANE D-4 4 06/02/2010 2 IJ 10 ug/L 1006009-02 1 111 TRICHLOROETHANE D 5 4 06/02/2010 0 U 100 ug/L 1006009 01 10 1 1,1 TRICHLOROETHANE Fork Spring 4 06/01/2010 0 U 10 ug/L 1006008-02 1 1,1,1 TRICHLOROETHANE FP 001 4 06/03/2010 0 U 10 ug/L 1006010 07 1 111 TRICHLOROETHANE G-2 4 06/03/2010 170 J 200 ug/L 1006010-04 20 1,1,1-TRICHLOROETHANE G2A 4 06/03/2010 170 J 200 ug/L 1006010-05 20 111 TRICHLOROETHANE LF-1 4 06/02/2010 4 J 10 ug/L 1006009 03 1 1 1,1 TRICHLOROETHANE Pipe Spring 4 06/01/2010 0 U 10 ug/L 1006008 03 1 1,1,1 TRICHLOROETHANE Shot Gun Spring 4 06/01/2010 0 U 10 ug/L 1006008-04 1 1,1,1 TRICHLOROETHANE TP 001 4 06/03/2010 0 U 10 ug/L 1006010-06 1 112 2-TETRACHLOROETHANE A-8 4 06/04/2010 0 U 10 ug/L 1006011-01 1 1,1,2 2 TETRACHLOROETHANE B 10 4 06/03/2010 0 U 10 ug/L 1006010 02 1 112 2 TETRACHLOROETHANE B-2D 4 06/03/2010 0 U 10 ug/L 1006010-03 1 1 1 2,2 TETRACHLOROETHANE B-3 4 06/02/2010 0 U 500 ug/L 1006009-04 50 1,1,2,2-TETRACHLOROETHANE B-6 4 06/03/2010 0 u 10 ug/L 1006010-08 1 112 2-TETRACHLOROETHANE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008-01 1 1,1,2,2 TETRACHLOROETHANE D 1 4 06/03/2010 0 u 10 ug/L 1006010-01 1 1,1,2,2-TETRACHLOROETHANE D-4 4 06/02/2010 0 u 10 ug/L 1006009-02 1 112 2 TETRACHLOROETHANE D-5 4 06/02/2010 0 u 100 ug/L 1006009-01 10 11 2,2 TETRACHLOROETHANE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 1,1,2 2 TETRACHLOROETHANE FP 001 4 06/03/2010 0 u 10 ug/L 1006010 07 1 1,1 2 2 TETRACHLOROETHANE G 2 4 06/03/2010 0 u 10 ug/L 1006010 04 1 112 2 TETRACHLOROETHANE G2A 4 06/03/2010 0 u 10 ug/L 1006010 05 1 112 2 TETRACHLOROETHANE LF 1 4 06/02/2010 0 u 10 ug/L 1006009-03 1 1 1,2 2-TETRACHLOROETHANE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008-03 1 1,1,2 2-TETRACHLOROETHANE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008-04 1 1,1 2 2-TETRACHLOROETHANE TP 001 4 06/03/2010 0 u 10 ug/L 1006010 06 1 112 TRICHLOROETHANE A8 4 06/04/2010 3 7J 10 ug/L 1006011 01 1 112 TRICHLOROETHANE 8 10 4 06/03/2010 0 u 10 ug/L 1006010-02 1 1,1 2 TRICHLOROETHANE B 2D 4 06/03/2010 3 2J 10 ug/L 1006010-03 1 112 TRICHLOROETHANE B 3 4 06/02/2010 0 U 500 ug/L 1006009 04 50 112 TRICHLOROETHANE B 6 4 06/03/2010 0 u 10 ug/L 1006010 08 1 1,1,2-TRICHLOROETHANE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008-01 1 1,1 2 TRICHLOROETHANE D 1 4 06/03/2010 0 u 10 ug/L 1006010 01 1 112 TRICHLOROETHANE D-4 4 06/02/2010 0 u 10 ug/L 1006009 02 1 1,1 2 TRICHLOROETHANE D 5 4 1 06/02/2010 0 u 100 ug/L 1006009-01 10 CONSTITUENT-H' -f^ LOCATION • LAB SAMPLED Djige CONG EQL UNIT mB SfiMPLE ID Dilution! 12 3 TRICHLOROBENZENE B 10 4 06/03/2010 0 u 10 Ug/L 1006010-02 1 12 3 TRICHLOROBENZENE B-2D 4 06/03/2010 0 u 10 Ug/L 1006010-03 1 12 3 TRICHLOROBENZENE B 3 4 06/02/2010 0 u 500 Ug/L 1006009-04 50 1,2,3 TRICHLOROBENZENE 8 6 4 06/03/2010 0 u 10 Ug/L 1006010 08 1 12 3 TRICHLOROBENZENE Connor Spring 4 06/01/2010 0 u 10 Ug/L 1006008 01 1 1 2 3-TRICHLOR08ENZENE D 1 4 06/03/2010 0 u 10 Ug/L 1006010 01 1 12 3 TRICHLOROBENZENE D 4 4 06/02/2010 0 u 10 Ug/L 1006009 02 1 1,2,3-TRICHLOROBENZENE D 5 4 06/02/2010 0 u 100 Ug/L 1006009 01 10 1,2,3-TRlCHLOROBENZENE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 1 2 3-TRICHLOROBENZENE FP 001 4 06/03/2010 0 u 10 ug/L 1006010 07 1 1,2,3-TRICHLOROBENZENE G 2 4 06/03/2010 0 u 10 ug/L 1006010 04 1 12 3 TRICHLOROBENZENE G2A 4 06/03/2010 0 u 10 ug/L 1006010 05 1 1,2,3-TRICHLOROBENZENE LF 1 4 06/02/2010 0 u 10 ug/L 1006009 03 1 1,2,3 TRICHLOROBENZENE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008 03 1 1 2 3-TRICHLOR08ENZENE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008 04 1 12 3 TRICHLOROBENZENE TP-OOl 4 06/03/2010 0 u 10 ug/L 1006010 06 1 12 3 TRICHLOROPROPANE A 8 4 06/04/2010 0 u 10 ug/L 1006011 01 1 1,2,3 TRICHLOROPROPANE B-10 4 06/03/2010 0 u 10 ug/L 1006010 02 1 1,2 3 TRICHLOROPROPANE B-2D 4 06/03/2010 0 u 10 ug/L 1006010 03 1 12 3 TRICHLOROPROPANE B 3 4 06/02/2010 0 u 500 ug/L 1006009 04 50 1 2,3 TRICHLOROPROPANE B-6 4 06/03/2010 0 u 10 ug/L 1006010 08 1 1,2 3 TRICHLOROPROPANE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008 01 1 12 3 TRICHLOROPROPANE D 1 4 06/03/2010 0 u 10 ug/L 1006010 01 1 12 3 TRICHLOROPROPANE D 4 4 06/02/2010 0 u 10 ug/L 1006009 02 1 1,2,3 TRICHLOROPROPANE D 5 4 06/02/2010 0 u 100 ug/L 1006009 01 10 1,2,3 TRICHLOROPROPANE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008-02 1 1,2,3 TRICHLOROPROPANE FP 001 4 06/03/2010 0 u 10 ug/L 1006010-07 1 12 3 TRICHLOROPROPANE G-2 4 06/03/2010 0 u 10 ug/L 1006010-04 1 1,2,3 TRICHLOROPROPANE G2A 4 06/03/2010 0 u 10 ug/L 1006010-05 1 1,2,3 TRICHLOROPROPANE LF 1 4 06/02/2010 0 u 10 ug/L 1006009-03 1 1,2,3-TRICHLOROPROPANE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008-03 1 1,2,3 TRICHLOROPROPANE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008-04 1 1 2,3 TRICHLOROPROPANE TP-OOl 4 06/03/2010 0 u 10 ug/L 1006010 06 1 1,2,4-TRICHLOROBENZENE A 8 4 06/04/2010 0 u 10 ug/L 1006011 01 1 1,2,4-TRICHLOROBENZENE 8-10 4 06/03/2010 0 u 10 ug/L 1006010 02 1 1 2,4-TRICHLOROBENZENE B-2D 4 06/03/2010 0 u 10 ug/L 1006010 03 1 1,2,4 TRICHLOROBENZENE 8 3 4 06/02/2010 0 u 500 ug/L 1006009 04 50 1,2,4 TRICHLOROBENZENE 8 6 4 06/03/2010 0 u 10 ug/L 1006010-08 1 1 2,4-TRICHLOROBENZENE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008-01 1 1,2,4-TRICHLOROBENZENE D 1 4 06/03/2010 0 u 10 ug/L 1006010-01 1 1 2,4-TRICHLOROBENZENE D4 4 06/02/2010 0 u 10 ug/L 1006009 02 1 1,2,4 TRICHLOROBENZENE D 5 4 06/02/2010 0 u 100 ug/L 1006009 01 10 1,2,4 TRICHLOROBENZENE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 1,2,4-TRICHLOROBENZENE FP-OOl 4 06/03/2010 0 u 10 ug/L 1006010-07 1 1 2 4-TRICHLOROBENZENE G-2 4 06/03/2010 0 u 10 ug/L 1006010-04 1 1,2,4-TRICHLOROBENZENE G2A 4 06/03/2010 0 u 10 ug/L 1006010 05 1 1,2,4 TRICHLOROBENZENE LF 1 4 06/02/2010 0 u 10 ug/L 1006009 03 1 1,2,4 TRICHLOROBENZENE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008 03 1 1 2,4-TRICHLOROBENZENE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008 04 1 1,2,4-TRICHLOROBENZENE TP 001 4 06/03/2010 0 u 10 ug/L 1006010 06 1 1,2,4-TRIMETHYLBENZENE A-8 4 06/04/2010 0 u 10 ug/L 100601101 1 1,2,4 TRIMETHYLBENZENE 8-10 4 06/03/2010 0 u 10 ug/L 1006010 02 1 12 4 TRIMETHYLBENZENE B 2D 4 06/03/2010 0 u 10 ug/L 1006010-03 1 12 4 TRIMETHYLBENZENE B-3 4 06/02/2010 0 u 500 ug/L 1006009-04 50 1,2,4 TRIMETHYLBENZENE B-6 4 06/03/2010 0 u 10 ug/L 1006010 08 1 1 24 TRIMETHYLBENZENE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008 01 1 1 24 TRIMETHYLBENZENE D 1 4 06/03/2010 0 u 10 ug/L 1006010-01 1 1,2,4 TRIMETHYLBENZENE D-4 4 06/02/2010 0 u 10 ug/L 1006009 02 1 1 24 TRIMETHYLBENZENE D 5 4 06/02/2010 0 u 100 ug/L 1006009 01 10 124 TRIMETHYLBENZENE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 CONSTITUENT .. L0C;??riON.f LAB SAMPLED DATE CONC EQL UNIT LAB SAMPLE ID: Dilution- 1 2-DICHLOROETHANE B 2D 4 06/03/2010 8 J 10 Ug/L 1006010 03 1 1 2-DICHLOROETHANE B 3 4 06/02/2010 0 U 500 Ug/L 1006009 04 1 2-DICHLOROETHANE B 6 4 06/03/2010 1 7J 10 Ug/L 1006010 08 1 1,2-DICHLOROETHANE Connor Spring 4 06/01/2010 0 U 10 Ug/L 1006008 01 1 1 2-DICHLOROETHANE D-1 4 06/03/2010 0 U 10 Ug/L 1006010-01 1 1 2-DICHLOROETHANE D-4 4 06/02/2010 0 U 10 ug/L 1006009-02 1 1 2-DICHLOROETHANE D-5 4 06/02/2010 0 U 100 ug/L 1006009-01 10 1,2-DICHLOROETHANE Fork Spring 4 06/01/2010 0 U 10 ug/L 1006008-02 1 1 2-DICHLOROETHANE FP-OOl 4 06/03/2010 0 U 10 ug/L 1006010-07 1 1 2-DICHLOROETHANE G 2 4 06/03/2010 28J 10 ug/L 1006010-04 1 1,2-DICHLOROETHANE G2A 4 06/03/2010 28J 10 ug/L 1006010-05 1 1 2 DICHLOROETHANE LF-1 4 06/02/2010 0 U 10 ug/L 1006009-03 1 1,2 DICHLOROETHANE Pipe Spring 4 06/01/2010 0 U 10 ug/L 1006008 03 1 1 2 DICHLOROETHANE Shot Gun Spring 4 06/01/2010 0 U 10 ug/L 1006008 04 1 1 2-DICHLOROETHANE TP-OOl 4 06/03/2010 0 U 10 ug/L 1006010 06 1 1,2-DICHLOROPROPANE A 8 4 06/04/2010 0 U 10 ug/L 1006011 01 1 1 2-DICHLOROPROPANE B 10 4 06/03/2010 0 U 10 ug/L 1006010 02 1 1,2-DICHLOROPROPANE B-2D 4 06/03/2010 0 U 10 ug/L 1006010-03 1 1 2-DICHLOROPROPANE B 3 4 06/02/2010 0 U 500 ug/L 1006009-04 1 2-DICHLOROPROPANE B 6 4 06/03/2010 0 u 10 ug/L 1006010-08 1 1 2 DICHLOROPROPANE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008 01 1 1,2 DICHLOROPROPANE D 1 4 06/03/2010 0 u 10 ug/L 1006010 01 1 1 2 DICHLOROPROPANE D 4 4 06/02/2010 0 u 10 ug/L 1006009 02 1 1 2 DICHLOROPROPANE D 5 4 06/02/2010 0 u 100 ug/L 1006009 01 10 1,2-DICHLOROPROPANE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 1,2-DICHLOROPROPANE FP 001 4 06/03/2010 0 u 10 ug/L 1006010 07 1 1 2-DICHLOROPROPANE G 2 4 06/03/2010 0 u 10 ug/L 1006010-04 1 1 2-DICHLOROPROPANE G2A 4 06/03/2010 0 u 10 ug/L 1006010-05 1 1,2 DICHLOROPROPANE LF 1 4 06/02/2010 0 u 10 ug/L 1006009-03 1 1 2 DICHLOROPROPANE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008-03 1 1,2 DICHLOROPROPANE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008-04 1 1,2 DICHLOROPROPANE TP 001 4 06/03/2010 0 u 10 ug/L 1006010-06 1 1 3,5-TRIMETHYLBENZENE A 8 4 06/04/2010 0 u 10 ug/L 1006011-01 1 1,3,5-TRIMETHYLBENZENE B 10 4 06/03/2010 0 u 10 ug/L 1006010-02 1 1,3,5-TRIMETHYL8ENZENE 8 2D 4 06/03/2010 0 u 10 ug/L 1006010-03 1 1 3 5-TRIMETHYLBENZENE B 3 4 06/02/2010 0 u 500 ug/L 1006009-04 50 1,3,5 TRIMETHYLBENZENE B 6 4 06/03/2010 0 u 10 ug/L 1006010-08 1 1,3,5 TRIMETHYLBENZENE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008-01 1 1 3,5 TRIMETHYLBENZENE D 1 4 06/03/2010 0 u 10 ug/L 1006010-01 1 1,3,5 TRIMETHYLBENZENE D 4 4 06/02/2010 0 u 10 ug/L 1006009 02 1 13 5 TRIMETHYLBENZENE D 5 4 06/02/2010 0 u 100 ug/L 1006009 01 10 1 3,5 TRIMETHYLBENZENE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 1,3,5-TRIMETHYLBENZENE FP 001 4 06/03/2010 0 u 10 ug/L 1006010 07 1 1 3 5-TRIMETHYLBENZENE G 2 4 06/03/2010 0 u 10 ug/L 1006010 04 1 13 5 TRIMETHYLBENZENE G2A 4 06/03/2010 0 u 10 ug/L 1006010-05 1 1,3,5 TRIMETHYLBENZENE LF-1 4 06/02/2010 0 u 10 ug/L 1006009-03 1 1,3,5 TRIMETHYLBENZENE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008-03 1 1,3,5 TRIMETHYLBENZENE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008-04 1 1 3,5 TRIMETHYLBENZENE TP 001 4 06/03/2010 0 u 10 ug/L 1006010 06 1 1,3-DICHLOROBENZENE A 8 4 06/04/2010 0 u 10 ug/L 1006011 01 1 1,3-DICHLOROBENZENE B-10 4 06/03/2010 0 u 10 ug/L 1006010 02 1 1,3-DICHLOROBENZENE B-2D 4 06/03/2010 0 u 10 ug/L 1006010 03 1 1 3-DICHLOROBENZENE 8 3 4 06/02/2010 0 u 500 ug/L 1006009 04 50 1 3-DICHLOROBENZENE B 6 4 06/03/2010 0 u 10 ug/L 1006010 08 1 1,3-DICHLOROBENZENE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008 01 1 1 3-DICHLOROBENZENE D-1 4 06/03/2010 0 u 10 ug/L 1006010-01 1 1 3-DICHLOROBENZENE D-4 4 06/02/2010 0 u 10 ug/L 1006009-02 1 1 3-DICHLOROBENZENE D-5 4 06/02/2010 0 u 100 ug/L 1006009 01 10 1,3-DICHLOROBENZENE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 1 3-DICHLOROBENZENE FP 001 4 06/03/2010 0 u 10 ug/L 1006010 07 1 g} COfeiSTITUENT LOCATION LAB SAMPLED^DAT^ONC EQL UNIT LAB SAMPLE ID £}ilLjtion 2 BUTANONE 8-3 4 06/02/2010 0 U 500 Ug/L 1006009 04 50 2 BUTANONE B 6 4 06/03/2010 0 U 10 Ug/L 1006010 08 1 2-BUTANONE Connor Spring 4 06/01/2010 0 U 10 ug/L 1006008 01 1 2 BUTANONE D 1 4 06/03/2010 0 U 10 Ug/L 1006010-01 1 2 BUTANONE D-4 4 06/02/2010 0 U 10 Ug/L 1006009 02 1 2 BUTANONE D-5 4 06/02/2010 0 U 100 Ug/L 1006009-01 10 2-BUTANONE Fork Spring 4 06/01/2010 0 U 10 Ug/L 1006008-02 1 2 BUTANONE FP-OOl 4 06/03/2010 0 U 10 ug/L 1006010-07 1 2-BUTANONE G 2 4 06/03/2010 0 U 10 ug/L 1006010-04 1 2 BUTANONE G2A 4 06/03/2010 0 U 10 ug/L 1006010-05 1 2 BUTANONE LF 1 4 06/02/2010 0 u 10 ug/L 1006009-03 1 2 BUTANONE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008-03 1 2 BUTANONE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008-04 1 2 BUTANONE TP 001 4 06/03/2010 0 u 10 ug/L 1006010-06 1 2 CHLOROETHYLVINYL ETHER A-8 4 06/04/2010 0 u 10 ug/L 1006011 01 1 2 CHLOROETHYLVINYL ETHER B 10 4 06/03/2010 0 u 10 ug/L 1006010 02 1 2 CHLOROETHYLVINYL ETHER B 2D 4 06/03/2010 0 u 10 ug/L 1006010 03 1 2-CHLOROETHYLVINYL ETHER B 3 4 06/02/2010 0 U 500 ug/L 1006009 04 50 2 CHLOROETHYLVINYL ETHER B 6 4 06/03/2010 0 u 10 ug/L 1006010 08 1 2 CHLOROETHYLVINYL ETHER Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008 01 1 2 CHLOROETHYLVINYL ETHER D-1 4 06/03/2010 0 u 10 ug/L 1006010 01 1 2 CHLOROETHYLVINYL ETHER D 4 4 06/02/2010 0 u 10 ug/L 1006009-02 1 2 CHLOROETHYLVINYL ETHER D 5 4 06/02/2010 0 u 100 ug/L 1006009-01 10 2 CHLOROETHYLVINYL ETHER Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008-02 1 2 CHLOROETHYLVINYL ETHER FP-OOl 4 06/03/2010 0 u 10 ug/L 1006010-07 1 2 CHLOROETHYLVINYL ETHER G 2 4 06/03/2010 0 u 10 ug/L 1006010-04 1 2 CHLOROETHYLVINYL ETHER G2A 4 06/03/2010 0 u 10 ug/L 1006010-05 1 2 CHLOROETHYLVINYL ETHER LF 1 4 06/02/2010 0 u 10 ug/L 1006009-03 1 2 CHLOROETHYLVINYL ETHER Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008 03 1 2 CHLOROETHYLVINYL ETHER Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008-04 1 2 CHLOROETHYLVINYL ETHER TP-OOl 4 06/03/2010 0 u 10 ug/L 1006010-06 1 2 CHLOROTOLUENE A 8 4 06/04/2010 0 u 10 ug/L 1006011-01 1 2 CHLOROTOLUENE B-10 4 06/03/2010 0 u 10 ug/L 1006010-02 1 2 CHLOROTOLUENE B-2D 4 06/03/2010 0 u 10 ug/L 1006010-03 1 2 CHLOROTOLUENE 8-3 4 06/02/2010 0 u 500 ug/L 1006009-04 50 2-CHLOROTOLUENE 8 6 4 06/03/2010 0 u 10 ug/L 1006010-08 1 2-CHLOROTOLUENE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008 01 1 2-CHLOROTOLUENE D-1 4 06/03/2010 0 u 10 ug/L 1006010-01 1 2 CHLOROTOLUENE D-4 4 06/02/2010 0 u 10 ug/L 1006009 02 1 2 CHLOROTOLUENE D 5 4 06/02/2010 0 u 100 ug/L 1006009-01 10 2 CHLOROTOLUENE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008-02 1 2 CHLOROTOLUENE FP-OOl 4 06/03/2010 0 u 10 ug/L 1006010-07 1 2 CHLOROTOLUENE G-2 4 06/03/2010 0 u 10 ug/L 1006010-04 1 2 CHLOROTOLUENE G2A 4 06/03/2010 0 u 10 ug/L 1006010-05 1 2 CHLOROTOLUENE LF-1 4 06/02/2010 0 u 10 ug/L 1006009 03 1 2 CHLOROTOLUENE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008 03 1 2 CHLOROTOLUENE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008 04 1 2 CHLOROTOLUENE TP-OOl 4 06/03/2010 0 u 10 ug/L 1006010 06 1 2 HEXANONE A8 4 06/04/2010 0 u 10 ug/L 1006011 01 1 2 HEXANONE B 10 4 06/03/2010 0 u 10 ug/L 1006010-02 1 2 HEXANONE 8 2D 4 06/03/2010 0 u 10 ug/L 1006010-03 1 2 HEXANONE 8 3 4 06/02/2010 0 u 500 ug/L 1006009-04 50 2 HEXANONE 6 6 4 06/03/2010 0 u 10 ug/L 1006010-08 1 2 HEXANONE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008-01 1 2 HEXANONE D-1 4 06/03/2010 0 u 10 ug/L 1006010-01 1 2 HEXANONE D 4 4 06/02/2010 0 u 10 ug/L 1006009-02 1 2 HEXANONE D 5 4 06/02/2010 0 u 100 ug/L 1006009 01 10 2-HEXANONE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 2 HEXANONE FP 001 4 06/03/2010 0 u 10 ug/L 1006010 07 1 2 HEXANONE G 2 4 06/03/2010 0 u 10 ug/L 1006010 04 1 re(«TITpENT LOCATION C: jlABBfSAMPLED DATE CONC EQy fUNlT-LAB SAMPLE ID Dilution ACETONE 8 6 4 06/03/2010 0 u 10 Ug/L 1006010-08 1 ACETONE Connor Spring 4 06/01/2010 0 u 10 Ug/L 1006008 01 1 ACETONE D 1 4 06/03/2010 0 u 10 Ug/L 1006010 01 1 ACETONE D 4 4 06/02/2010 0 u 10 Ug/L 1006009 02 1 ACETONE D 5 4 06/02/2010 0 u 100 Ug/L 1006009 01 10 ACETONE Fork Spring 4 06/01/2010 0 u 10 Ug/L 1006008 02 1 ACETONE FP 001 4 06/03/2010 0 u 10 ug/L 1006010 07 1 ACETONE G-2 4 06/03/2010 0 u 10 ug/L 1006010 04 1 ACETONE G2A 4 06/03/2010 0 u 10 ug/L 1006010 05 1 ACETONE LF 1 4 06/02/2010 0 u 10 ug/L 1006009 03 1 ACETONE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008 03 1 ACETONE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008 04 1 ACETONE TP 001 4 06/03/2010 0 u 10 ug/L 1006010 06 1 BENZENE A 8 4 06/04/2010 34J 10 ug/L 1006011-01 1 BENZENE B 10 4 06/03/2010 02J 10 ug/L 1006010-02 1 BENZENE 8 2D 4 06/03/2010 1 IJ 10 ug/L 1006010-03 1 BENZENE 8 3 4 06/02/2010 0 u 500 ug/L 1006009-04 50 BENZENE 8 6 4 06/03/2010 06J 10 ug/L 1006010-08 1 BENZENE Connor Spring 4 06/01/2010 0 U 10 ug/L 1006008-01 1 BENZENE D-1 4 06/03/2010 3 6J 10 ug/L 1006010 01 1 BENZENE D-4 4 06/02/2010 0 U 10 ug/L 1006009-02 1 BENZENE D 5 4 06/02/2010 0 U 100 ug/L 1006009 01 10 BENZENE Fork Spring 4 06/01/2010 0 U 10 ug/L 1006008-02 1 BENZENE FP 001 4 06/03/2010 0 U 10 ug/L 1006010 07 1 BENZENE G 2 4 06/03/2010 05J 10 ug/L 1006010 04 1 BENZENE G2A 4 06/03/2010 05J 10 ug/L 1006010 05 1 BENZENE LF 1 4 06/02/2010 0 U 10 ug/L 1006009 03 1 BENZENE Pipe Spring 4 06/01/2010 0 U 10 ug/L 1006008 03 1 BENZENE Shot Gun Spring 4 06/01/2010 0 U 10 ug/L 1006008-04 1 BENZENE TP-OOl 4 06/03/2010 0 U 10 ug/L 1006010-06 1 BROMOBENZENE A-8 4 06/04/2010 0 U 10 ug/L 1006011-01 1 BROMOBENZENE 8-10 4 06/03/2010 0 U 10 ug/L 1006010-02 1 BROMOBENZENE B-2D 4 06/03/2010 0 u 10 ug/L 1006010-03 1 BROMOBENZENE B-3 4 06/02/2010 0 u 500 ug/L 1006009 04 50 BROMOBENZENE B-6 4 06/03/2010 0 u 10 ug/L 1006010 08 1 BROMOBENZENE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008 01 1 BROMOBENZENE D 1 4 06/03/2010 0 u 10 ug/L 1006010 01 1 BROMOBENZENE D-4 4 06/02/2010 0 u 10 ug/L 1006009 02 1 BROMOBENZENE D-5 4 06/02/2010 0 u 100 ug/L 1006009 01 10 BROMOBENZENE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 BROMOBENZENE FP-OOl 4 06/03/2010 0 u 10 ug/L 1006010-07 1 BROMOBENZENE G 2 4 06/03/2010 0 u 10 ug/L 1006010-04 1 BROMOBENZENE G2A 4 06/03/2010 0 u 10 ug/L 1006010 05 1 BROMOBENZENE LF 1 4 06/02/2010 0 u 10 ug/L 1006009 03 1 BROMOBENZENE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008 03 1 BROMOBENZENE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008 04 1 BROMOBENZENE TP 001 4 06/03/2010 0 u 10 ug/L 1006010 06 1 BROMOCHLOROMETHANE A 8 4 06/04/2010 0 u 10 ug/L 1006011 01 1 BROMOCHLOROMETHANE B 10 4 06/03/2010 0 u 10 ug/L 1006010-02 1 BROMOCHLOROMETHANE B-2D 4 06/03/2010 0 u 10 ug/L 1006010-03 1 BROMOCHLOROMETHANE B-3 4 06/02/2010 0 u 500 ug/L 1006009 04 50 BROMOCHLOROMETHANE B 6 4 06/03/2010 0 u 10 ug/L 1006010-08 1 BROMOCHLOROMETHANE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008-01 1 BROMOCHLOROMETHANE D 1 4 06/03/2010 0 u 10 ug/L 1006010 01 1 BROMOCHLOROMETHANE D 4 4 06/02/2010 0 u 10 ug/L 1006009-02 1 BROMOCHLOROMETHANE D 5 4 06/02/2010 0 u 100 ug/L 1006009-01 10 BROMOCHLOROMETHANE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 BROMOCHLOROMETHANE FP 001 4 06/03/2010 0 u 10 ug/L 1006010 07 1 BROMOCHLOROMETHANE G 2 4 06/03/2010 0 u 10 ug/L 1006010 04 1 BROMOCHLOROMETHANE G2A 4 06/03/2010 0 u 10 ug/L 1006010 05 1 CONSTITUENT LOCATION LAB S/VMPLEDOATE CONC EQL UNIT LAB SAMPLE ID mm CARBON DISULFIDE Connor Spring 4 06/01/2010 0 u 10 Ug/L 1006008 01 1 CARBON DISULFIDE D-1 4 06/03/2010 0 u 10 Ug/L 1006010-01 1 CARBON DISULFIDE D 4 4 06/02/2010 0 u 10 Ug/L 1006009 02 1 CARBON DISULFIDE D 5 4 06/02/2010 0 u 100 ug/L 1006009-01 10 CARBON DISULFIDE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 CARBON DISULFIDE FP 001 4 06/03/2010 0 u 10 ug/L 1006010 07 1 CARBON DISULFIDE G 2 4 06/03/2010 0 u 10 ug/L 1006010 04 1 CARBON DISULFIDE G2A 4 06/03/2010 0 u 10 ug/L 1006010 05 1 CARBON DISULFIDE LF 1 4 06/02/2010 0 u 10 ug/L 1006009 03 1 CARBON DISULFIDE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008 03 1 CARBON DISULFIDE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008 04 1 CARBON DISULFIDE TP 001 4 06/03/2010 0 u 10 ug/L 1006010 06 1 CARBON TETRACHLORIDE A 8 4 06/04/2010 6 5J 10 ug/L 1006011 01 1 CARBON TETRACHLORIDE B 10 4 06/03/2010 0 u 10 ug/L 1006010-02 1 CARBON TETRACHLORIDE 8-2 D 4 06/03/2010 45J 10 ug/L 1006010-03 1 CARBON TETRACHLORIDE 8-3 4 06/02/2010 0 U 500 ug/L 1006009-04 50 CARBON TETRACHLORIDE B-6 4 06/03/2010 081 10 ug/L 1006010 08 1 CARBON TETRACHLORIDE Connor Spring 4 06/01/2010 0 U 10 ug/L 1006008 01 1 CARBON TETRACHLORIDE D 1 4 06/03/2010 7 J 10 ug/L 1006010 01 1 CARBON TETRACHLORIDE D-4 4 06/02/2010 2 2 J 10 ug/L 1006009-02 1 CARBON TETRACHLORIDE D 5 4 06/02/2010 0 U 100 ug/L 1006009-01 10 CARBON TETRACHLORIDE Fork Spring 4 06/01/2010 0 U 10 ug/L 1006008 02 1 CARBON TETRACHLORIDE FP 001 4 06/03/2010 0 U 10 ug/L 1006010 07 1 CARBON TETRACHLORIDE G 2 4 06/03/2010 13J 10 ug/L 1006010 04 1 CARBON TETRACHLORIDE G2A 4 06/03/2010 13J 10 ug/L 1006010 05 1 CARBON TETRACHLORIDE LF-1 4 06/02/2010 0 U 10 ug/L 1006009 03 1 CARBON TETRACHLORIDE Pipe Spring 4 06/01/2010 0 U 10 ug/L 1006008-03 1 CARBON TETRACHLORIDE Shot Gun Spring 4 06/01/2010 0 U 10 ug/L 1006008-04 1 CARBON TETRACHLORIDE TP 001 4 06/03/2010 0 U 10 ug/L 1006010 06 1 CHLOROBENZENE A 8 4 06/04/2010 1 J 10 ug/L 1006011 01 1 CHLOROBENZENE 8 10 4 06/03/2010 0 U 10 ug/L 1006010 02 1 CHLOROBENZENE 8 2D 4 06/03/2010 07J 10 ug/L 1006010 03 1 CHLOROBENZENE B 3 4 06/02/2010 0 U 500 ug/L 1006009 04 50 CHLOROBENZENE B-6 4 06/03/2010 0 U 10 ug/L 1006010-08 1 CHLOROBENZENE Connor Spring 4 06/01/2010 0 U 10 ug/L 1006008-01 1 CHLOROBENZENE D 1 4 06/03/2010 02U 10 ug/L 1006010-01 1 CHLOROBENZENE D-4 4 06/02/2010 0 U 10 ug/L 1006009-02 1 CHLOROBENZENE D 5 4 06/02/2010 0 U 100 ug/L 1006009-01 10 CHLOROBENZENE Fork Spring 4 06/01/2010 0 U 10 ug/L 1006008-02 1 CHLOROBENZENE FP-OOl 4 06/03/2010 0 U 10 ug/L 1006010-07 1 CHLOROBENZENE G 2 4 06/03/2010 0 u 10 ug/L 1006010-04 1 CHLOROBENZENE G2A 4 06/03/2010 0 u 10 ug/L 1006010 05 1 CHLOROBENZENE LF 1 4 06/02/2010 0 u 10 ug/L 1006009-03 1 CHLOROBENZENE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008-03 1 CHLOROBENZENE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008 04 1 CHLOROBENZENE TP-OOl 4 06/03/2010 0 u 10 ug/L 1006010 06 1 CHLOROETHANE A8 4 06/04/2010 0 u 10 ug/L 1006011 01 1 CHLOROETHANE 8-10 4 06/03/2010 0 u 10 ug/L 1006010 02 1 CHLOROETHANE 8 2D 4 06/03/2010 0 u 10 ug/L 1006010 03 1 CHLOROETHANE B 3 4 06/02/2010 0 u 500 ug/L 1006009 04 50 CHLOROETHANE B 6 4 06/03/2010 0 u 10 ug/L 1006010 08 1 CHLOROETHANE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008 01 1 CHLOROETHANE D 1 4 06/03/2010 0 u 10 ug/L 1006010-01 1 CHLOROETHANE D 4 4 06/02/2010 0 u 10 ug/L 1006009-02 1 CHLOROETHANE D-5 4 06/02/2010 0 u 100 ug/L 1006009 01 10 CHLOROETHANE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 CHLOROETHANE FP 001 4 06/03/2010 0 u 10 ug/L 1006010 07 1 CHLOROETHANE G 2 4 06/03/2010 0 u 10 ug/L 1006010 04 1 CHLOROETHANE G2A 4 06/03/2010 0 u 10 ug/L 1006010-05 1 CHLOROETHANE LF 1 4 06/02/2010 0 u 10 ug/L 1006009 03 1 i CONSTITUENT LOCATION LAB SAMPLED DATE CONC EQL UNIT LAB SAMPLE ID Dilution CIS 1 3 DICHLOROPROPENE 8 2D 4 06/03/2010 0 u 10 Ug/L 1006010 03 1 CIS 1 3 DICHLOROPROPENE B-3 4 06/02/2010 0 u 500 Ug/L 1006009 04 CIS 1 3-DICHLOROPROPENE 8-6 4 06/03/2010 0 u 10 Ug/L 1006010 08 1 CIS 1,3 DICHLOROPROPENE Connor Spring 4 06/01/2010 0 u 10 Ug/L 1006008 01 1 CIS-1 3-DICHLOROPROPENE D 1 4 06/03/2010 0 u 10 Ug/L 1006010-01 1 CIS-1,3 DICHLOROPROPENE D 4 4 06/02/2010 0 u 10 Ug/L 1006009 02 1 CIS-1 3 DICHLOROPROPENE D 5 4 06/02/2010 0 u 100 Ug/L 1006009 01 CIS-1,3 DICHLOROPROPENE Fork Spring 4 06/01/2010 0 u 10 Ug/L 1006008-02 1 CIS-1 3 DICHLOROPROPENE FP 001 4 06/03/2010 0 u 10 ug/L 1006010 07 1 CIS-1 3-DICHLOROPROPENE G 2 4 06/03/2010 0 u 10 ug/L 1006010 04 1 CIS-1,3-DICHL0R0PR0PENE G2A 4 06/03/2010 0 u 10 ug/L 1006010 05 1 CIS 1 3-DICHLOROPROPENE LF-1 4 06/02/2010 0 u 10 ug/L 1006009 03 1 CIS 1,3 DICHLOROPROPENE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008 03 1 CIS 1,3 DICHLOROPROPENE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008-04 1 CIS-1 3 DICHLOROPROPENE TP 001 4 06/03/2010 0 u 10 ug/L 1006010-06 1 DIBROMOCHLOROMETHANE A 8 4 06/04/2010 0 u 10 ug/L 1006011 01 1 DIBROMOCHLOROMETHANE B-10 4 06/03/2010 0 u 10 ug/L 1006010 02 1 DIBROMOCHLOROMETHANE 8-2D 4 06/03/2010 0 u 10 ug/L 1006010 03 1 DIBROMOCHLOROMETHANE B 3 4 06/02/2010 0 u 500 ug/L 1006009 04 DIBROMOCHLOROMETHANE 8 6 4 06/03/2010 0 u 10 ug/L 1006010 08 1 DIBROMOCHLOROMETHANE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008-01 1 DIBROMOCHLOROMETHANE D 1 4 06/03/2010 0 u 10 ug/L 1006010-01 1 DIBROMOCHLOROMETHANE D 4 4 06/02/2010 0 u 10 ug/L 1006009 02 1 DIBROMOCHLOROMETHANE D 5 4 06/02/2010 0 u 100 ug/L 1006009 01 10 DIBROMOCHLOROMETHANE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 DIBROMOCHLOROMETHANE FP-OOl 4 06/03/2010 0 u 10 ug/L 1006010 07 1 DIBROMOCHLOROMETHANE G-2 4 06/03/2010 0 u 10 ug/L 1006010 04 1 DIBROMOCHLOROMETHANE G2A 4 06/03/2010 0 u 10 ug/L 1006010-05 1 DIBROMOCHLOROMETHANE LF 1 4 06/02/2010 0 u 10 ug/L 1006009-03 1 DIBROMOCHLOROMETHANE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008 03 1 DIBROMOCHLOROMETHANE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008 04 1 DIBROMOCHLOROMETHANE TP-OOl 4 06/03/2010 0 u 10 ug/L 1006010 06 1 DIBROMOMETHANE A 8 4 06/04/2010 0 u 10 ug/L 1006011 01 1 DIBROMOMETHANE 8-10 4 06/03/2010 0 u 10 ug/L 1006010 02 1 DIBROMOMETHANE 8-2D 4 06/03/2010 0 u 10 ug/L 1006010 03 _^ 1 DIBROMOMETHANE B-3 4 06/02/2010 0 u 500 ug/L 1006009 04 50 DIBROMOMETHANE 8-6 4 06/03/2010 0 u 10 ug/L 1006010 08 1 DIBROMOMETHANE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008 01 1 DIBROMOMETHANE D 1 4 06/03/2010 0 u 10 ug/L 1006010 01 1 DIBROMOMETHANE D 4 4 06/02/2010 0 u 10 ug/L 1006009-02 1 DIBROMOMETHANE D 5 4 06/02/2010 0 u 100 ug/L 1006009-01 10 DIBROMOMETHANE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008-02 1 DIBROMOMETHANE FP-OOl 4 06/03/2010 0 u 10 ug/L 1006010 07 1 DIBROMOMETHANE G 2 4 06/03/2010 0 u 10 ug/L 1006010-04 1 DIBROMOMETHANE G2A 4 06/03/2010 0 u 10 ug/L 1006010-05 1 DIBROMOMETHANE LF-1 4 06/02/2010 0 u 10 ug/L 1006009-03 1 DIBROMOMETHANE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008 03 1 DIBROMOMETHANE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008 04 1 DIBROMOMETHANE TP 001 4 06/03/2010 0 u 10 ug/L 1006010 06 1 DICHLORODIFLUOROMETHANE A 8 4 06/04/2010 0 u 10 ug/L 100601101 1 DICHLORODIFLUOROMETHANE 8-10 4 06/03/2010 0 u 10 ug/L 1006010-02 1 DICHLORODIFLUOROMETHANE B 2D 4 06/03/2010 0 u 10 ug/L 1006010-03 1 DICHLORODIFLUOROMETHANE 8 3 4 06/02/2010 0 u 500 ug/L 1006009-04 50 DICHLORODIFLUOROMETHANE B 6 4 06/03/2010 0 u 10 ug/L 1006010 08 1 DICHLORODIFLUOROMETHANE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008-01 1 DICHLORODIFLUOROMETHANE D 1 4 06/03/2010 0 u 10 ug/L 1006010 01 1 DICHLORODIFLUOROMETHANE D 4 4 06/02/2010 0 u 10 ug/L 1006009-02 1 DICHLORODIFLUOROMETHANE D 5 4 06/02/2010 0 u 100 ug/L 1006009 01 10 DICHLORODIFLUOROMETHANE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 DICHLORODIFLUOROMETHANE FP 001 4 06/03/2010 0 u 10 ug/L 1006010 07 1 CONSTIIUENT i . LOfiATiON LAB MMPLBD DATE^ CONC EQL f UNIT LABS/^PLEID Dilution m p XYLENE 8 3 4 06/02/2010 0 U 500 Ug/L 1006009 04 50 m p XYLENE 8 6 4 06/03/2010 0 u 10 Ug/L 1006010 08 1 m p-XYLENE Connor Spring 4 06/01/2010 0 u 10 Ug/L 1006008 01 1 m,p XYLENE D 1 4 06/03/2010 0 u 10 Ug/L 1006010 01 1 m p XYLENE D 4 4 06/02/2010 0 u 10 Ug/L 1006009 02 1 m p XYLENE D 5 4 06/02/2010 0 u 100 Ug/L 1006009 01 10 m p-XYLENE Fork Spring 4 06/01/2010 0 u 10 Ug/L 1006008-02 1 m,p XYLENE FP 001 4 06/03/2010 0 u 10 Ug/L 1006010 07 1 m,p XYLENE G 2 4 06/03/2010 0 u 10 Ug/L 1006010 04 1 m p XYLENE G2A 4 06/03/2010 0 u 10 Ug/L 1006010 05 1 m,p-XYLENE LF 1 4 06/02/2010 0 u 10 ug/L 1006009 03 1 m p XYLENE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008 03 1 m,p XYLENE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008 04 1 m p XYLENE TP 001 4 06/03/2010 0 u 10 ug/L 1006010-06 1 METHYLENE CHLORIDE A 8 4 06/04/2010 0 u 10 ug/L 1006011 01 1 METHYLENE CHLORIDE B 10 4 06/03/2010 0 u 10 ug/L 1006010-02 1 METHYLENE CHLORIDE 8 2D 4 06/03/2010 0 u 10 ug/L 1006010-03 1 METHYLENE CHLORIDE B 3 4 06/02/2010 0 u 500 ug/L 1006009-04 50 METHYLENE CHLORIDE B-6 4 06/03/2010 0 u 10 ug/L 1006010-08 1 METHYLENE CHLORIDE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008-01 1 METHYLENE CHLORIDE D 1 4 06/03/2010 0 u 10 ug/L 1006010 01 1 METHYLENE CHLORIDE D 4 4 06/02/2010 0 u 10 ug/L 1006009 02 1 METHYLENE CHLORIDE D 5 4 06/02/2010 0 u 100 ug/L 1006009 01 10 METHYLENE CHLORIDE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 METHYLENE CHLORIDE FP 001 4 06/03/2010 0 u 10 ug/L 1006010-07 1 METHYLENE CHLORIDE G-2 4 06/03/2010 0 u 10 ug/L 1006010-04 1 METHYLENE CHLORIDE G2A 4 06/03/2010 0 u 10 ug/L 1006010-05 1 METHYLENE CHLORIDE LF-1 4 06/02/2010 0 u 10 ug/L 1006009-03 1 METHYLENE CHLORIDE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008 03 1 METHYLENE CHLORIDE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008 04 1 METHYLENE CHLORIDE TP-OOl 4 06/03/2010 0 u 10 ug/L 1006010 06 1 NAPHTHALENE A8 4 06/04/2010 0 u 10 ug/L 1006011 01 1 NAPHTHALENE 8-10 4 06/03/2010 0 u 10 ug/L 1006010 02 1 NAPHTHALENE 8 2D 4 06/03/2010 0 u 10 ug/L 1006010 03 1 NAPHTHALENE B 3 4 06/02/2010 0 u 500 ug/L 1006009-04 50 NAPHTHALENE 8 6 4 06/03/2010 0 u 10 ug/L 1006010-08 1 NAPHTHALENE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008-01 1 NAPHTHALENE D-1 4 06/03/2010 0 u 10 ug/L 1006010-01 1 NAPHTHALENE D 4 4 06/02/2010 0 u 10 ug/L 1006009-02 1 NAPHTHALENE D 5 4 06/02/2010 0 u 100 ug/L 1006009-01 10 NAPHTHALENE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 NAPHTHALENE FP 001 4 06/03/2010 0 u 10 ug/L 1006010 07 1 NAPHTHALENE G 2 4 06/03/2010 0 u 10 ug/L 1006010 04 1 NAPHTHALENE G2A 4 06/03/2010 0 u 10 ug/L 1006010 05 1 NAPHTHALENE LF-1 4 06/02/2010 0 u 10 ug/L 1006009-03 1 NAPHTHALENE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008 03 1 NAPHTHALENE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008-04 1 NAPHTHALENE TP 001 4 06/03/2010 0 u 10 ug/L 1006010-06 1 N-BUTYLBENZENE A 8 4 06/04/2010 0 u 10 ug/L 1006011-01 1 N-BUTYLBENZENE 8 10 4 06/03/2010 0 u 10 ug/L 1006010-02 1 N-BUTYLBENZENE 8 2D 4 06/03/2010 0 u 10 ug/L 1006010-03 1 N-BUTYLBENZENE B 3 4 06/02/2010 0 u 500 ug/L 1006009-04 50 N-BUTYLBENZENE B 6 4 06/03/2010 0 u 10 ug/L 1006010-08 1 N-BUTYLBENZENE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008 01 1 N-BUT7LBENZENE D 1 4 06/03/2010 0 u 10 ug/L 1006010 01 1 N-BUTYLBENZENE D 4 4 06/02/2010 0 u 10 ug/L 1006009 02 1 N-BUTYLBENZENE D 5 4 06/02/2010 0 u 100 ug/L 1006009 01 10 N-BUTYLBENZENE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 N-BUTYLBENZENE FP 001 4 06/03/2010 0 u 10 ug/L 1006010 07 1 N-BUTYLBENZENE G 2 4 06/03/2010 0 u 10 ug/L 1006010 04 1 : --i- .;*CONSTITUgKi ' -iiOCAllONp £S«LED:mTE CONC; lEQL. *.UIillT LA^SAMPLEID ipilMhorfi STYRENE 8 6 4 06/03/2010 0 u 10 Ug/L 1006010 08 1 STYRENE Connor Spring 4 06/01/2010 0 u 10 Ug/L 1006008 01 1 STYRENE D 1 4 06/03/2010 0 u 10 Ug/L 1006010-01 1 STYRENE D 4 4 06/02/2010 0 u 10 Ug/L 1006009 02 1 STYRENE D 5 4 06/02/2010 0 u 100 Ug/L 1006009-01 10 STYRENE Fork Spring 4 06/01/2010 0 u 10 Ug/L 1006008-02 1 STYRENE FP 001 4 06/03/2010 0 u 10 ug/L 1006010 07 1 STYRENE G-2 4 06/03/2010 0 u 10 ug/L 1006010-04 1 STYRENE G2A 4 06/03/2010 0 u 10 ug/L 1006010 05 1 STYRENE LF-1 4 06/02/2010 0 u 10 ug/L 1006009 03 1 STYRENE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008-03 1 STYRENE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008-04 1 STYRENE TP-OOl 4 06/03/2010 0 u 10 ug/L 1006010 06 1 TERT-BUTYLBENZENE A-8 4 06/04/2010 0 u 10 ug/L 1006011 01 1 TERT-BUTYLBENZENE 8-10 4 06/03/2010 0 u 10 ug/L 1006010-02 1 TERT-BUTYLBENZENE B-2D 4 06/03/2010 0 u 10 ug/L 1006010 03 1 TERT BUTYLBENZENE 8-3 4 06/02/2010 0 u 500 ug/L 1006009 04 50 TERT-BUTYLBENZENE 8 6 4 06/03/2010 0 u 10 ug/L 1006010-08 1 TERT BUTYLBENZENE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008-01 1 TERT BUTYLBENZENE D 1 4 06/03/2010 0 u 10 ug/L 1006010-01 1 TERT BUTYLBENZENE D-4 4 06/02/2010 0 u 10 ug/L 1006009 02 1 TERT-BUTYLBENZENE D-5 4 06/02/2010 0 u 100 ug/L 1006009-01 10 TERT BUTYLBENZENE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008-02 1 TERT BUTYLBENZENE FP 001 4 06/03/2010 0 u 10 ug/L 1006010-07 1 TERT-BUTYLBENZENE G-2 4 06/03/2010 0 u 10 ug/L 1006010 04 1 TERT-BUTYLBENZENE G2A 4 06/03/2010 0 u 10 ug/L 1006010 05 1 TERT-BUTYLBENZENE LF-1 4 06/02/2010 0 u 10 ug/L 1006009-03 1 TERT BUTYLBENZENE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008 03 1 TERT-BUTYLBENZENE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008 04 1 TERT-BUTYLBENZENE TP 001 4 06/03/2010 0 u 10 ug/L 1006010 06 1 TETRACHLOROETHENE A-8 4 06/04/2010 2 8J 10 ug/L 1006011-01 1 TETRACHLOROETHENE B-10 4 06/03/2010 0 u 10 ug/L 1006010-02 1 TETRACHLOROETHENE B-2D 4 06/03/2010 22J 10 ug/L 1006010-03 1 TETRACHLOROETHENE 8-3 4 06/02/2010 0 u 500 ug/L 1006009-04 50 TETRACHLOROETHENE B-6 4 06/03/2010 0 u 10 ug/L 1006010 08 1 TETRACHLOROETHENE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008 01 1 TETRACHLOROETHENE D-1 4 06/03/2010 69J 10 ug/L 1006010-01 1 TETRACHLOROETHENE D-4 4 06/02/2010 0 u 10 ug/L 1006009 02 1 TETRACHLOROETHENE D-5 4 06/02/2010 0 u 100 ug/L 1006009-01 10 TETRACHLOROETHENE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 TETRACHLOROETHENE FP-OOl 4 06/03/2010 0 u 10 ug/L 1006010 07 1 TETRACHLOROETHENE G-2 4 06/03/2010 0 u 10 ug/L 1006010 04 1 TETRACHLOROETHENE G2A 4 06/03/2010 09J 10 ug/L 1006010 05 1 TETRACHLOROETHENE LF-1 4 06/02/2010 0 u 10 ug/L 1006009-03 1 TETRACHLOROETHENE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008-03 1 TETRACHLOROETHENE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008-04 1 TETRACHLOROETHENE TP-OOl 4 06/03/2010 0 u 10 ug/L 1006010-06 1 TOLUENE A 8 4 06/04/2010 0 u 10 ug/L 1006011-01 1 TOLUENE B-10 4 06/03/2010 0 u 10 ug/L 1006010-02 1 TOLUENE B-2D 4 06/03/2010 0 u 10 ug/L 1006010 03 1 TOLUENE 8-3 4 06/02/2010 0 u 500 ug/L 1006009-04 50 TOLUENE 8 6 4 06/03/2010 0 u 10 ug/L 1006010 08 1 TOLUENE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008 01 1 TOLUENE D-1 4 06/03/2010 0 u 10 ug/L 1006010-01 1 TOLUENE D 4 4 06/02/2010 0 u 10 ug/L 1006009 02 1 TOLUENE D 5 4 06/02/2010 0 u 100 ug/L 1006009 01 10 TOLUENE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 TOLUENE FP-OOl 4 06/03/2010 0 u 10 ug/L 1006010-07 1 TOLUENE G 2 4 06/03/2010 0 u 10 ug/L 1006010 04 1 TOLUENE G2A 4 06/03/2010 0 u 10 ug/L 1006010 05 1 • CONSflTUESr"'"' m:--'i LOGmmu % i LA6I SAMflED DATE coNe: ^EQi i^iiiTi rlAB SAMPLEfID Dilution TRICHLOROFLUOROMETHANE Connor Spring 4 06/01/2010 0 u 10 Ug/L 1006008 01 1 TRICHLOROFLUOROMETHANE D 1 4 06/03/2010 0 U 10 ug/L 1006010-01 1 TRICHLOROFLUOROMETHANE D 4 4 06/02/2010 081 10 ug/L 1006009-02 1 TRICHLOROFLUOROMETHANE D 5 4 06/02/2010 0 U 100 ug/L 1006009-01 10 TRICHLOROFLUOROMETHANE Fork Spring 4 06/01/2010 0 U 10 ug/L 1006008-02 1 TRICHLOROFLUOROMETHANE FP 001 4 06/03/2010 0 U 10 ug/L 1006010 07 1 TRICHLOROFLUOROMETHANE G 2 4 06/03/2010 0 u 10 ug/L 1006010-04 1 TRICHLOROFLUOROMETHANE G2A 4 06/03/2010 0 u 10 ug/L 1006010-05 1 TRICHLOROFLUOROMETHANE LF 1 4 06/02/2010 0 u 10 ug/L 1006009-03 1 TRICHLOROFLUOROMETHANE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008-03 1 TRICHLOROFLUOROMETHANE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008-04 1 TRICHLOROFLUOROMETHANE TP 001 4 06/03/2010 0 u 10 ug/L 1006010 06 1 VINYL ACETATE A-8 4 06/04/2010 0 u 50 ug/L 1006011-01 1 VINYL ACETATE 8 10 4 06/03/2010 0 U 50 ug/L 1006010 02 1 VINYL ACETATE B 2D 4 06/03/2010 0 u 50 ug/L 1006010 03 1 VINYL ACETATE B 3 4 06/02/2010 0 u 2500 ug/L 1006009 04 50 VINYL ACETATE 8 6 4 06/03/2010 0 u 50 ug/L 1006010-08 1 VINYL ACETATE Connor Spring 4 06/01/2010 0 u 50 ug/L 1006008 01 1 VINYL ACETATE D 1 4 06/03/2010 0 u 50 ug/L 1006010-01 1 VINYL ACETATE D 4 4 06/02/2010 0 u 50 ug/L 1006009-02 1 VINYL ACETATE D 5 4 06/02/2010 0 u 500 ug/L 1006009-01 10 VINYL ACETATE Fork Spring 4 06/01/2010 0 u 50 ug/L 1006008 02 1 VINYL ACETATE FP-OOl 4 06/03/2010 0 u 50 ug/L 1006010 07 1 VINYL ACETATE G-2 4 06/03/2010 0 u 50 ug/L 1006010-04 1 VINYL ACETATE G2A 4 06/03/2010 0 u 50 ug/L 1006010-05 1 VINYL ACETATE LF 1 4 06/02/2010 0 u 50 ug/L 1006009 03 1 VINYL ACETATE Pipe Spring 4 06/01/2010 0 u 50 ug/L 1006008 03 1 VINYL ACETATE Shot Gun Spring 4 06/01/2010 0 u 50 ug/L 1006008 04 1 VINYL ACETATE TP-OOl 4 06/03/2010 0 u 50 ug/L 1006010-06 1 VINYL CHLORIDE A 8 4 06/04/2010 0 u 10 ug/L 1006011 01 1 VINYL CHLORIDE B 10 4 06/03/2010 0 u 10 ug/L 1006010 02 1 VINYL CHLORIDE 8 2D 4 06/03/2010 0 u 10 ug/L 1006010-03 1 VINYL CHLORIDE 8 3 4 06/02/2010 0 u 500 ug/L 1006009-04 50 VINYL CHLORIDE B-6 4 06/03/2010 0 u 10 ug/L 1006010-08 1 VINYL CHLORIDE Connor Spring 4 06/01/2010 0 u 10 ug/L 1006008-01 1 VINYL CHLORIDE D-1 4 06/03/2010 0 u 10 ug/L 1006010 01 1 VINYL CHLORIDE D 4 4 06/02/2010 0 u 10 ug/L 1006009 02 1 VINYL CHLORIDE D-5 4 06/02/2010 0 u 100 ug/L 1006009-01 10 VINYL CHLORIDE Fork Spring 4 06/01/2010 0 u 10 ug/L 1006008 02 1 VINYL CHLORIDE FP 001 4 06/03/2010 0 u 10 ug/L 1006010 07 1 VINYL CHLORIDE G-2 4 06/03/2010 0 u 10 ug/L 1006010 04 1 VINYL CHLORIDE G2A 4 06/03/2010 0 u 10 ug/L 1006010-05 1 VINYL CHLORIDE LF 1 4 06/02/2010 0 u 10 ug/L 1006009-03 1 VINYL CHLORIDE Pipe Spring 4 06/01/2010 0 u 10 ug/L 1006008-03 1 VINYL CHLORIDE Shot Gun Spring 4 06/01/2010 0 u 10 ug/L 1006008-04 1 VINYL CHLORIDE TP-OOl 4 06/03/2010 0 u 10 ug/L 1006010 06 1 APPENDIX B ANALYTICAL DATA - PERCHLORATE, HMX, RDX, CONDUCTIVITY This appendix is organized as follows CONSTITUENT - Parameter being analyzed for LOCATION LAB SAMPLE DATE CONC EQL UNIT LAB SAMPLE ID DILUTION Well Number or Spring Number 1,3 = outside laboratory, 4 = ATK Launch Systems Date sample was taken Concentration level of constituent in sample Method reporting limit established by EPA for a given analytical method Unit of measure Umque sample ID number issued by the Lab Dilution of sample ^ONSnimENT LO»TION . , LAB SAMPLE DATS liQL mm *AB SAMfLE ID OJjfion PERCHLORATE A-8 4 06/04/2010 8520 400 ug/L 1006011-01 100 PERCHLORATE B-10 4 06/03/2010 4040 200 ug/L 1006010-02 50 PERCHLORATE B-2D 4 06/03/2010 25600 400 ug/L 1006010-03 100 PERCHLORATE B-3 4 06/02/2010 40800 400 ug/L 1006009-04 100 PERCHLORATE B-6 4 06/03/2010 43600 400 ug/L 1006010-08 100 PERCHLORATE Connor Spring 4 06/01/2010 0 U 20 ug/L 1006008-01 5 PERCHLORATE D-1 4 06/03/2010 551 40 ug/L 1006010-01 10 PERCHLORATE D-4 4 06/02/2010 135000 4000 ug/L 1006009-02 1000 PERCHLORATE D-5 4 06/02/2010 200000 4000 ug/L 1006009-01 1000 PERCHLORATE Fork Spring 4 06/01/2010 0 U 4 ug/L 1006008-02 1 PERCHLORATE FP-OOl 4 06/03/2010 0 U 4 ug/L 1006010-07 1 PERCHLORATE G-2 4 06/03/2010 52100 1000 ug/L 1006010-04 250 PERCHLORATE G2A 4 06/03/2010 51900 1000 ug/L 1006010-05 250 PERCHLORATE LF-1 4 06/02/2010 489 40 ug/L 1006009-03 10 PERCHLORATE Pipe Spring 4 06/01/2010 311 40 ug/L 1006008-03 10 PERCHLORATE Shot Gun Spring 4 06/01/2010 75 40 ug/L 1006008-04 10 PERCHLORATE TP-OOl 4 06/03/2010 0 U 4 ug/L 1006010-06 1 RDX B-3 4 06/02/2010 1 94 1 ug/L 1006009-04 1 HMX B-3 4 06/02/2010 2 70 1 ug/L 1006009-04 1 CONDUCTIVITY A-8 4 06/04/2010 1200 1 uS/cm 1006011-01 1 CONDUCTIVITY B-10 4 06/03/2010 1000 1 uS/cm 1006010-02 1 CONDUCTIVITY B-2D 4 06/03/2010 1520 1 uS/cm 1006010-03 1 CONDUCTIVITY B-3 4 06/02/2010 1440 1 uS/cm 1006009-04 1 CONDUCTIVITY B-6 4 06/03/2010 7100 1 uS/cm 1006010-08 1 CONDUCTIVITY Connor Spring 4 06/01/2010 4110 1 uS/cm 1006008-01 1 CONDUCTIVITY D-1 4 06/03/2010 2010 1 uS/cm 1006010-01 1 CONDUCTIVITY D-4 4 06/02/2010 1340 1 uS/cm 1006009-02 1 CONDUCTIVITY D-5 4 06/02/2010 1950 1 uS/cm 1006009-01 1 CONDUCTIVITY Fork Spring 4 06/01/2010 2150 1 uS/cm 1006008-02 1 CONDUCTIVITY FP-OOl 4 06/03/2010 4 54 1 uS/cm 1006010-07 1 CONDUCTIVITY G-2 4 06/03/2010 7780 1 uS/cm 1006010-04 1 CONDUCTIVITY G2A 4 06/03/2010 7810 1 uS/cm 1006010-05 1 CONDUCTIVITY LF-1 4 06/02/2010 8180 1 uS/cm 1006009-03 1 CONDUCTIVITY Pipe Spring 4 06/01/2010 10800 1 uS/cm 1006008-03 1 CONDUCTIVITY Shot Gun Spring 4 06/01/2010 9500 1 uS/cm 1006008-04 1 CONDUCTIVITY TP-OOl 4 06/03/2010 4 04 1 uS/cm 1006010-06 1 1006008 ENVIRONMENTAL LAB WORK REQLEST -0 ATK LALNCH SYSTEMS ENVIROMWEMAL LABORATORY LWR No E13164 Logm No FROM Allen Lee EXTENSION 25688 COST CENTER 8200 WORK ORDER 988P LS333 GW DATE 6/1/2010 ORGANIZATION Environmental Services MAIL STOP 301 REPOR- RESULTS TO HELEN RAVSTEN, MS 301 SAMPLE INFORMATION SAMPLE DATE TYPE LOCATION TIME TEST REMARKS SAMPLE DATE G C LOCATION TIME TEST REMARKS Conner Spring 6/1/10 X Promontory 1200 See Attached Analytical Request Fork Spring 6/1/10 X Promontory 1230 See Attached Analytical Request Pipe Spring 6/1/10 X Promontory 1250 See Attached Analytical Request Shot Gun Spring 6/1/10 X Promontory 1320 See Attached Analytical Request CHAIN OF CUSTODY RELINQUISHED BY DATE TIME RECEIVED BY DATE TIME FOR LABORATORY USE ONLY DATE COMPLETED DATE REPORTED SIGNATURE 988P LS333 GW CERTIFICATE OF ANALYSIS Listing of Sample Information and Testing Requested Wednesday, June 16, 2010 TESTED FOR ATK DLV Environmental Monitoring Thiokol Corp, UT 84322 ANALYZED BY ATK Launch Systems Analytical Chemistry Laboratory P O Box 707, M/S 245 Bngham City, UT 84302-0707 435-863-3732 435-863-8080 Contact Name Project Sample Delivery Group Al Lee Ground Water Testing - DLV 1006008 Page 1 of 12 Prnted 06/16/10 :1 21 Sample Delivery Group 1006008 Sample No Client No Received Collect Date/Time Test Requested Sample Description Matrix 1006008 01 Connor Spring 06/02/10 6/1/2010 12 00 26 EPA 120 1 Conductivity Water EPA 314 0 Perctilorate Ion Chromatography Water SW846 301 OA Metals Digestion Water SW846 601 OB (Water) Metals Analysis by ICP 6010 Water SW846 7470A Mercury Analysis Water SW 846 8260B (Water) Volatile Organic Analysis Water 1006008 02 Fork Spring 06/02/10 6/1/2010 12 30 26 EPA 120 1 Conductivity Water EPA 314 0 Perchlorate Ion Chromatography Water SW846 301 OA Metals Digestion Water SW846 60108 (Water) Metals Analysis by ICP 6010 Water SW846 7470A Mercury Analysis Water SW846 8260B (Water) Volatile Organic Analysis Water 1006008 03 PipeSpnng 06/02/10 6/1/2010 12 50 26 EPA 120 1 Conductivity Water EPA 314 0 Perchlorate Ion Chromatography Water SW846 301 OA Metals Digestion Water SW846 601 OB (Water) Metals Analysis by (CP 6010 Water SW846 7470A Mercury Analysis Water SW 846 8260B (Water) Volatile Organic Analysis Water 1006008 04 Shot Gun Spnng 06/02/10 6/1/2010 13 20 26 EPA 120 1 Conductivity Water EPA 314 0 Perchlorate Ion Chromatography Water SW846 301 OA Metals Digestion Water SW846 601 OB (Water) Metals Analysis by ICP 6010 Water SW846 7470A Mercury Analysis Water Page 2 of 12 Pnnled 06/16/10 11 21 Sample Delivery Group 1006008 Sample No Client No Test Requested 1006008 04 Shot Gun Spring Sample Description Received Collect Date/Time Matrix 06/02/10 6/1/2010 13 20 26 SW846 8260B (Water) Volatile Organic Analysis Wa*er Certified By W Scott Fraser Quality Assurance Officer 06/17/2010 Date This certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation Program (NELAP) unless otherwise annotated Page 3 of 12 Pnn ed 06/16/10 11 21 Listing of Results by Sample Sample Delivery Group 1006008 Client Sample ID Connor Spring Sample Description ATK DLV Groundwater Spring Sampling 2010 Laboratory Sample ID 1006008 01 Date Sampled 06/01/10 12 00 AS Number Dilution AS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date Test Method EPA 1201 Co ductiviy CONDUCTIVITY 4110 uS/cm 0 3 1 JMV 06/11/ 0 Test Method EPA 314 0 Pe ch orate Ion Chronatograpiy 014797 73 0 PERCHLORATE U L.g/L 5 20 5 JMM 06/11/ 0 Tes( Method SW 846 3010A Vietals Diges ion 3010A ACID DIGEST ON 06/07/2010 1 MTB 06/08/10 12 00 00 am Test Method SW 846 6010B (Water) Metals Analysis by ICP 6010 7440 38 2 ARSENIC U ug/L 20 100 J MTB 06/07/10 7440 39 3 BARIUM 70 2 ug/L 2 10 1 MTB 06/07/10 7440 43 9 CADMIUM U ug/L 1 5 1 MTB 06/07/10 7440 47 3 CHROMIUHfl U ug/L 10 50 1 MTB 06/07/10 7440 46 4 COBALT U ug/L 1 5 1 MTB 06/07/10 7439 92 1 LEAD U ug/L 20 100 1 MTB 06/07/10 7439 98 7 MOLYBDENUM U ug/L 1 5 1 MTB 06/07/10 7782 49 2 SELENIUM u ug/L 30 150 1 MTB 06/07/10 7440 22 4 SILVER U ug/L 1 5 1 MTB 06/07/10 Test Method SWS46 7470A Mercury Analysis 7439 97 6 MERCURY U ug/L 0 3 1 1 TCP 06/08/10 Test Method SW 846 82608 (Water) Volatile Organic Analysis 67 64 1 ACETONE u ug/L 5 10 1 QC 06/04/10 71 43 2 BENZENE u ug/L 0 22 10 1 QC 06/04/10 74 97 5 BROMOCHLOROMETHANE u ug/L 0 31 10 1 QC 06/04/10 75 27-4 BROMODICHLOROMETHANE u ug/L 0 19 10 1 QC 06/04/10 108 86 1 BROMOBENZENE u ug/L 0 37 10 1 QC 06/04/10 75 25 2 BROMOFORM u ug/L 0 42 10 1 QC 06/04/10 74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 06/04/10 78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 06/04/10 104 51 8 N BUTYLBENZENE u ug/L 03 10 1 QC 06/04/10 135 98 8 SEC BUTYLBENZENE u ug/L 04 10 1 QC 06/04/10 98 06 6 TERT BUTYLBENZENE u ug/L 0 4 10 1 QC 06/04/10 75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 06/04/10 56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 06/04/10 108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 QC 06/04/10 75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 06/04/10 110 75 8 2 CHLOROETHYLVINYL ETHER u ug/L 1 71 10 1 QC 06/04/10 67 66 3 CHLOROFORM u ug/L 0 3 10 1 QC 06/04/10 74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 06/04/10 95-49 8 2 CHLOROTOLUENE u ug/L 0 24 10 1 QC 06/04/10 106 43 4 4 CHLOROTOLUENE u ug/L 0 5 10 1 QC 06/04/10 124-48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 06/04/10 96 12 8 1 2 DIBROMO 3 CHLOROPROPANIE u ug/L 0 35 0 1 QC 06/04/10 74 95 3 DIBROMOMETHANE u ug/L 0 25 10 1 QC 06/04/10 106 93 4 1 2 DIBROMOETHANE u L.g/L 5 10 QC 06/04/10 95 50 1 1 2 DICHLOROBENZEWE u ug/L 5 86 " GO 06/04/10 S-tl 73 1 1 3 DICHLOROBENZENE u ug/L 5 62 0 1 QC oe/o'i/io 06 46 7 1 4 D ChLOROBENZENE L -g/L 5 88 1C 1 QC 06/04/10 75 71 8 DICH^QRODIF.JOROVETHANE u ug/L C 66 c QC 06/04/10 Page 4 of 12 Printed 06/16/10 11 21 Listing of Results by Sample Sample Delivery Group 1006008 Client Sample ID Conno Spring Laboratory Sample ID 1006008 01 Sample Description ATK DLV Groundwater Spnng Sampling 2010 Date Sampled 06/01/10 12 00 CAS Number Test Parameter Result Units IVIDL Dilution EQL Factor Analyst Test Date res( Method SW 846 8260B (Water) Volatile Organic Analysis IVIDL 75 34 3 1 DiCHLOROE'hAME u ugL 0 49 10 1 QC 06/04/10 107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 QC 06/04/10 75 35-4 1 1 DICHLOROE'HENE u ug/L 0 16 10 1 QC 06/04/10 156 59 4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 06/04/10 156 60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 QC 06/04/10 78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 06/04/10 142 28 9 1 3 DICHLOROPROPANE u ug/L 0 24 10 1 QC 06/04/10 563 58 6 1 1 DICHLOROPROPENE u ug/L 0 17 0 1 QC 05/04/10 10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 06/04/10 10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 0 4 10 1 QC 06/04/10 590 20 7 2 2 DICHLOROPROPANE u ug/L 0 9 10 1 QC 06/04/10 100-41-4 ETHYLBENZENE u ug/L 0 16 10 1 QC 06/04/10 591 78 6 2 HEXANONE u ug/L 0 7 10 1 QC 06/04/10 87 68 3 HEXACHLOROBUTADIENE u ug/L 0 9 10 1 QC 06/04/10 98 82 8 ISOPROPYLBENZENE u ug/L 0 58 10 1 QC 06/04/10 99 87-6 4 ISOPROPYLTOLUENE u ug/L 0 24 10 1 QC 06/04/10 75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 06/04/10 108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 06/04/10 91 20 3 NAPHTHALENE u ug/L 4 10 1 QC 06/04/10 103 65 1 N PROPYLBENZENE u ug/L 0 5 10 1 QC 06/04/10 100-42 5 STYRENE u ug/L 0 3 10 1 QC 06/04/10 630 20 6 1112 TETRACHLOROETHANE u ug/L 0 25 10 1 QC 06/04/10 79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 06/04/10 127 18-4 TETRACHLOROETHENE u ug/L 04 10 1 QC 06/04/10 108 88 3 TOLUENE u ug/L 05 10 1 QC 06/04/10 87-61-6 1 2 3 TRICHLOROBENZENE u ug/L 0 23 10 1 QC 06/04/10 120 82 1 1 2 4 TRICHLOROBENZENE u ug/L 4 37 10 1 QC 06/04/10 71 55-6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 06/04/10 79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 06/04/10 79 01-6 TRICHLOROETHENE u ug/L 07 10 1 QC 06/04/10 75 69^ TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 06/04/10 96 18-4 1 2 3 TRICHLOROPROPANE u ug/L 0 33 10 1 QC 06/04/10 95 63-6 1 2 4 TRIMETHYLBENZENE u ug/L 0 19 10 1 QC 06/04/10 108-67 8 1 3 5 TRIMETHYLBENZENE u ug/L 0 29 10 1 QC 06/04/10 108 05 4 VINYL ACETATE u ug/L 20 50 1 QC 06/04/10 75 01-4 VINYL CHLORIDE u ug/L 03 10 1 QC 06/04/10 1330 20 7 m p XYLENE u ug/L 06 10 1 QC 06/04/10 95-47 6 oXYLENE u ug/L 0 3 10 1 QC 06/04/10 460 00 4 BROMOFLUOROBENZENE 96 3 V 1 QC 06/04/10 1868 53 7 DIBROMOFLUOROMETHANE 103 / 1 QC 06/04/10 17060 07 0 1 2 DICHLOROETHANE D4 107 "/ 1 QC 06/04/10 2037 26 5 TOLUENE D8 98 /o 1 QC OS/04/10 Client Sample ID Fork Spnng Laboratory Sample ID 1006008 02 Sample Description ATK DLV Groundwater Spring Sampling 2010 Date Sampled 06/01/10 12 30 CAS Number Test Parameter Result Units MDL Dilution EQL Factor Analyst Test Date Test Method EPA 120 1 Cora c ivi'y CONDJCTIVITY 2 5C JS/CP-G 3 1 1 JVV 06 1 '10 Page 5 of 12 Pnntsd 06/16/10 1121 Listing of Results by Sample Sample Delivery Group 1006008 Client Sample ID Fork Spring Sample Description ATK DLV Groundwater Spring Sampling 2010 Laboratory Sample ID 1006008 02 Date Sampled 06/01/10 12 30 CAS Number Test Parameter Result Units IVIDL Dilution EQL Factor Analyst Test Date Test Method EPA 314 0 Perchlorate Ion Chromatography 014797 73 0 PERCHLORATE U ug/L 1 4 JMV 06/11/10 Test Method SWi46 3010A We'.als Digestion 3C10A ACID DIGESTION 06/07/2010 MTB 06/08/10 12 00 00 am Test Method SW 846 601 OB (Water) Metals Analysis by ICP 6010 7440 38 2 ARSENIC U ug/L 20 100 1 MTB 06/07/10 7440 39 3 BARIUM 57 5 ug/L 2 10 1 MTB 06/07/10 7440 43 9 CADMIUM U ug/L 1 5 1 MTB 06/07/10 7440 47 3 CHROMIUM U ug/L 10 50 1 MTB 06/07/10 7440 48 4 COBALT U ug/L 1 5 1 MTB 06/07/10 7439 92 1 LEAD U ug/L 20 100 1 MTB 06/07/10 7439 98 7 MOLYBDENUM U ug/L 1 5 1 MTB 06/07/10 7782 49 2 SELENIUM u ug/L 30 150 1 MTB 06/07/10 7440 22 4 SILVER u ug/L 1 5 1 MTB 06/07/10 Test Method SW 846 7470A Mercury Analysis 7439 97 6 MERCURY u ug/L 0 3 1 1 TCP 06/08/10 Test Method SW 846 8260B (Water) Volatile Organic Analysis 67-64 1 ACETONE u ug/L 5 10 1 QC 06/04/10 71 43 2 BENZENE u ug/L 0 22 10 1 QC 06/04/10 74 97 5 BROMOCHLOROMETHANE u ug/L 0 31 10 1 QC 06/04/10 75 27-4 BROMODICHLOROMETHANE u ug/L 0 19 10 1 QC 06/04/10 108 86 1 BROMOBENZENE u ug/L 0 37 10 1 QC 06/04/10 75 25 2 BROMOFORM u ug/L 0 42 10 1 QC 06/04/10 74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 06/04/10 78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 06/04/10 104 51 8 N BUTYLBENZENE u ug/L 0 3 10 1 QC 06/04/10 135 98 8 SEC BUTYLBENZENE u ug/L 04 10 1 QC 06/04/10 98 06 6 TERT BUTYLBENZENE u ug/L 0 4 10 1 QC 06/04/10 75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 06/04/10 56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 06/04/10 108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 QC 06/04/10 75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 06/04/10 110 75 8 2 CHLOROETHYLVINYL ETHER u ug/L 1 71 10 1 QC 06/04/10 67 66 3 CHLOROFORM u ug/L 0 3 10 1 QC 06/04/10 74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 06/04/10 95-49 8 2 CHLOROTOLUENE u ug/L 0 24 10 1 QC 06/04/10 106 43 4 4 CHLOROTOLUENE J ug/L 0 15 10 1 QC 06/04/10 124-48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 05/04/10 96 12 8 1 2 DIBROMO 3 CHLOROPROPANE u tg/L 0 35 10 1 QC 06/04/10 74 95 3 DIBROMOMETHANE u ug/L 0 25 10 1 QC 06/04/10 106 93 4 1 2 DIBROMOETHANE L ug/L 0 15 10 QC 06/04/10 95 50 1 1 2 DlCHLOROBENZENE u ug/L 5 86 10 QC 06/04/ 0 541 73 1 1 3 DlCHLOROBENZENE J ug/L 5 62 10 QC 06/04/10 06 46 7 1 4 DICHLOROBE\ZENE u Lg/L 5 88 10 QC 06/04/10 75 71 8 DIC-LORODIFLJOROMETHANE -g/' C 66 10 QC 06/04/1 „ 75 34 3 i DICHLOROETHANE L 9'-0 49 u QC 06/04/1C 107 06 2 2 D C-J OROE'^HANE u JS -0 29 1C QC 05/04/ 0 75 35 4 1 DiC-'LOROETnENE jg/. C 6 10 QC 06/04/-'0 Page 6 of 12 Pnnted 06/16/10 1121 Listing of Results by Sample Sample Delivery Group 1006008 Client Sample ID Fork Spring Laboratory Sample ID 1006008 02 Date Sampled 06/01/10 12 30 Sample Description ATK DLV Groundwa er Spring Sampling 2010 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date Test Method SW 846 8260B (Water) Volati'e Orgs nic Analys s 156 59 4 CIS 1 2 DICHLOROETHENE U ug/L 0 16 0 QC 06/04/10 156 so 5 TRANS 1 2 DICHLOROETHENE U ug/L " 34 10 QC 06/04/10 78 87 5 1 2 DICHLOROPROPANE U ug/L 0 16 10 QC 06/04/10 142 28 9 1 3 DICHLOROPRQOANE U ug/L 0 24 10 QC 06/04/10 563 58 6 1 1 DICHLOROPROPENE U ug/L 0 17 10 QC 06/04/10 10061 01 5 CIS 1 3 DICHLOROPROPENE u jg/L 0 4 10 QC 06/04/10 10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 0 4 10 1 QC 06/04/10 590 20 7 2 2 DICHLOROPROPANE u g/L 0 9 10 1 QC 06/04/ 0 100-41 4 ETHYLBENZENE u ug/L 0 16 10 1 QC 06/04/10 591 78 S 2 HEXANONE u ug/L 0 7 10 1 QC 06/04/10 87 68 3 HEXACHLOROBUTADIENE u ug/L 0 9 10 1 QC 06/04/10 98 82 8 ISOPROPYLBENZENE u ug/L 0 58 10 1 QC 06/04/10 99 87 6 4 ISOPROPYLTOLUENE u ug/L 0 24 10 1 QC 06/04/10 75 09 2 METHYLENE CHLORIDE U ug/L 08 10 1 QC 06/04/10 108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 06/04/10 91 20 3 NAPHTHALENE u ug/L 4 10 1 QC 06/04/10 103 65 1 N PROPYLBENZENE u ug/L 0 5 10 1 QC 06/04/10 100-42 5 STYRENE u ug/L 0 3 10 1 QC 06/04/10 630 20 6 1112 TETRACHLOROETHANE u ug/L 0 25 10 1 QC 06/04/10 79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 06/04/10 127 18 4 TETRACHLOROETHENE u ug/L 0 4 10 1 QC 06/04/10 108 88 3 TOLUENE u ug/L 0 5 10 1 QC 06/04/10 87 61 6 1 2 3 TRICHLOROBENZENE u ug/L 0 23 10 1 QC 06/04/10 120 82 1 1 2 4 TRICHLOROBENZENE u ug/L 4 37 10 1 QC 06/04/10 71 55 6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 06/04/10 79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 06/04/10 79 01-6 TRICHLOROETHENE u ug/L 07 10 1 QC 06/04/10 75-69 4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 06/04/10 96 18-4 1 2 3 TRICHLOROPROPANE u ug/L 0 33 10 1 QC 06/04/10 95-63 6 1 2 4 TRIMETHYLBENZENE u ug/L 0 19 10 1 QC 06/04/10 108-67 8 1 3 5 TRIMETHYLBENZENE u ug/L 0 29 10 1 QC 06/04/10 108 05 4 VINYL ACETATE u ug/L 20 50 1 QC 06/04/10 75 01-4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 06/04/10 1330 20 7 mp XYLENE u ug/L 06 10 1 QC 06/04/10 95-47 6 o-XYLENE u ug/L 0 3 10 1 QC 06/04/10 460-00 4 BROMOFLUOROBENZENE 97 5 / 1 QC 06/04/-'0 1868 53 7 DIBROMOFLUOROMETHANE 102 / 1 QC 06/04/ 0 17060 07 0 1 2 DICHLOROETHANE D4 105 V 1 QC 06/04/10 2037 26 5 TOLUENE D8 96 6 / 1 QC 06/04/10 Client Sample ID Pipe Spnng Laboratory Sample ID 1006008 03 Date Sampled 06/01/10 12 50 Sample Description ATK DLV Groundwater Spnng Sampling 2010 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date Test Method EPA 120 1 Corduc ivity CONDUCTIVrY 10800 jS/cm o 3 1 1 VM 06/11/10 Test Method EPA 314 0 Perc'-iorae 10 ChrOTiatog aphy 014797 73 0 PERCHLORATE 3 1 ^5 10 4 VM 06/11/10 Page 7 of 12 Pnrted 06/16/10 1121 Listing of Results by Sample Sample Delivery Group 1006008 Client Sample ID Pioe Spnng Sample Description ATK DLV Groundwater Spring Sampling 2010 Laboratory Sample ID 1006008 03 Date Sampled 06/01/10 i2 50 CAS Number Test Method 7440 38 2 7440 39 3 7440 43 9 7440 47 3 7440 48 4 7439 92 1 7439 98 7 7782 49 2 7440 22 4 Test Method 7439 97 6 Tesf Method Test Parameter SW846 3010A 30 OA ACID DIGESTION Metals Digestion Result Units 06/07/2010 12 00 00 am MDL Dilution Factor Analyst Test Date TestMethod SW 846 6010B (Water) Meta;s Analysis by ICP 6010 ARSENIC BARIUM CADMIUM CHROMIUM COBALT LEAD MOLYBDENUM SELENIUM SILVER SIV846 7470A MERCURY SW846 8260B (Water) U 69 1 U U U U u u u Mercury Analysis Volatile Organic Analysis ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 20 2 1 .0 1 20 1 30 1 100 10 5 50 5 100 5 150 5 67 64 1 ACETONE U ug/L 5 10 1 QC 06/04/10 71 43 2 BENZENE U ug/L 0 22 10 1 QC 06/04/10 74 97 5 BROMOCHLOROMETHANE U ug/L 0 31 10 1 QC 06/04/10 75 27-4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 06/04/10 108 86 1 BROMOBENZENE U ug/L 0 37 10 1 QC 06/04/10 75 25 2 BROMOFORM U ug/L 0 42 10 1 QC 06/04/10 74 83 9 BROMOMETHANE U ug/L 0 57 10 1 QC 06/04/10 78 93 3 2 BUTANONE U ug/L 1 11 10 1 QC 06/04/10 104 51 8 N BUTYLBENZENE U ug/L 0 3 10 1 QC 06/04/10 135 98 8 SEC BUTYLBENZENE U ug/L 04 10 1 QC 06/04/10 98 06 6 TERT BUTYLBENZENE U ug/L 0 4 10 1 QC 06/04/10 75 15 0 CARBON DISULFIDE U ug/L 0 13 10 1 QC 06/04/10 56 23 5 CARBON TETRACHLORIDE U ug/L 0 27 10 1 QC 06/04/10 108 90 7 CHLOROBENZENE U ug/L 0 16 10 1 QC 06/04/10 75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 06/04/10 110 75 8 2 CHLOROETHYLVINYL ETHER u ug/L 1 71 10 1 QC 06/04/10 67-«6 3 CHLOROFORM u ug/L 0 3 10 1 QC 06/04/10 74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 06/04/10 95-49 8 2 CHLOROTOLUENE u ug/L 0 24 10 1 QC 06/04/10 106 43 4 4 CHLOROTOLUENE u ug/L 0 15 10 1 QC 06/04/10 124 48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 06/04/10 96 12 8 1 2 DIBROMO 3 CHLOROPROPANE u ug/L 0 35 10 1 QC 06/04/10 74 95 3 DIBROMOMETHANE u ug/L 0 25 10 1 QC 06/04/10 106 93 4 1 2 DIBROMOETHANE u ug/L 0 15 10 1 QC 06/04/10 95 50 1 1 2 DlCHLOROBENZENE u ug/L 5 86 10 1 QC 06/04/10 541 73 1 1 3 DlCHLOROBENZENE u ug/L 5 62 10 1 QC 06/04/10 106-46 7 1 4 DlCHLOROBENZENE u ug/L 5 88 10 1 QC 06/04/10 75 71 8 DICHLORODIFLUOROMETHANE u ug/L 0 66 0 1 QC 06/04/10 75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 -10 -1 QC 06/04/1 0 107 06 2 1 2 DICHLOROETHANE L ug/L 0 29 "0 1 QC 06/04/10 75 35 4 1 DICHLOROETHENE L Lg/L 0 6 0 QC 06/04/lO 166 59 4 CIS 1 2 DICHLOROETHENE U .g/-0 16 c QC 06/04/ 0 56 60 5 TRANS 1 2 DICriLOROE-hEKE J ug'-0 34 10 QC 06/04/lO 78 87 5 1 2 DICHLOROPRO=ANE J ug/-0 16 10 QC 06/04/10 Page 8 of 12 MT3 MTB MTB WTB MTB MTB MTB MTB MTB MTB TCP 06/08/10 06/07/10 06/07/10 06/07/10 06/07/10 06/07/10 06/07/10 06/07/10 06/07/10 06/07/10 06/08/10 Printed 06/16/10 11 21 Listing of Results by Sample Sample Delivery Group 1006008 Client Sample ID Pipe Spring Laboratory Sample ID 1006008 03 Sample Descript ion ATK Di_V Groundwater Spnng Sampling 2010 Date Sampled 06/01/10 12 50 CAS Number Test Parameter Result Units MDL Dilution EQL Factor Analyst Test Date Test Method SW 846 82606 (Water) Volatile Organic Analysis 142 28 9 1 3 D CHLOROPROPANE U ug/L 0 24 10 QC 06/C4/1 0 563 58 6 1 DICHLOROPROPENE U g/-0 17 10 1 QC 06/04/10 10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 0 4 10 1 QC 06/04/10 10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 06/04/10 590 20 7 2 2 DICHLOROPROPANE u jg/L 0 9 10 1 QC 06/04/10 100 41 4 ETHYLBENZENE U jg/^ 0 6 10 1 QC 06/04/10 591 78 6 2 HEXANONE u ug/L 0 7 10 1 QC 06/04/10 87 68 3 HEXACHLOROBUTADIENE u ug/L 0 9 10 1 QC 06/04/1 0 98 82 8 ISOPROPYLBENZENE u ug/L 0 58 10 1 QC 06/04/10 99 87 6 4 ISOPROPYLTOLUENE u ug/L 0 24 10 1 QC 06/04/10 75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 06/04/10 108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 06/04/10 91 20 3 NAPHTHALENE u ug/L 4 10 1 QC 06/04/10 103 65 1 N PROPYLBENZENE u ug/L 0 5 10 1 QC 06/04/10 100-42 5 STYRENE u ug/L 0 3 10 1 QC 06/04/10 630 20 6 1112 TETRACHLOROETHANE u ug/L 0 25 10 1 QC 06/04/10 79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 06/04/10 127 18 4 TETRACHLOROETHENE u ug/L 04 10 1 QC 08/04/10 108 88 3 TOLUENE u ug/L 0 5 10 1 QC 06/04/10 87 61 6 1 2 3 TRICHLOROBENZENE u ug/L 0 23 10 1 QC 06/04/10 120 82 1 1 2 4 TRICHLOROBENZENE u ug/L 4 37 10 1 QC 06/04/10 71 55 6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 06/04/10 79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 06/04/10 79 01 6 TRICHLOROETHENE 62 J ug/L 07 10 1 QC 06/04/10 75 69 4 TRICHLOROFLUOROMETHANE u ug/L 03 10 1 QC 06/04/10 96 18-4 1 2 3 TRICHLOROPROPANE u ug/L 0 33 10 1 QC 06/04/10 95 63-6 1 2 4 TRIMETHYLBENZENE u ug/L 0 19 10 1 QC 06/04/10 108-67 8 1 3 5 TRIMETHYLBENZENE u ug/L 0 29 10 1 QC 06/04/10 108 05 4 VINYL ACETATE u ug/L 20 50 1 QC 06/04/10 75 01-4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 06/04/10 1330 20 7 m p XYLENE u ug/L 06 10 1 QC 06/04/10 95-47 6 0 XYLENE u ug/L 0 3 10 1 QC 06/04/10 460 00 4 BROMOFLUOROBENZENE 97 9 % 1 QC 06/04/10 1868 53 7 DIBROMOFLUOROMETHANE 105 /o 1 QC 06/04/10 17060 07 0 1 2 DICHLOROETHANE D4 111 % 1 QC 06/04/10 2037 26 5 TOLUENE D8 96 3 / QC 06/04/10 Client Sample ID Shot Gun Spnng Laboratory Sample ID 1006008 04 Sample Description ATK DLV Groundwater Spnng Sampling 2010 Date Sampled 06/01/10 13 20 CAS Number Test Parameter Result Units MDL Dilution EQL Factor Analyst Test Date Test Method EPA 1201 Conductivity CONDUCTIVITY 9500 uS/cm 0 3 1 1 JMM 06/11/10 Test Method EPA 314 0 Perchlorate ion Chroma ography 0 4797 73 0 PERCHLORATE 75 g/L 10 40 10 MM 06/11/10 Test Method SW846 3010A We a.s Digestior 3010A ACID DIGESTION 06/07'20i0 i2 00 CO am MTB 06/08/10 Page 9 of 12 Pnnted 06/16/10 1121 Listing of Results by Sample Sample Delivery Group 1006008 Client Sample ID Shot Gun Spnng Sample Description ATK DLV Groundwater Spnng SampI ng 2010 Laboratory Sample ID 1006008 04 Date Sampled 06/01/10 13 20 CAS Number Test Method 7440 38 2 7440 39 3 7440 43 9 7440 47 3 7440 48 4 7439 92 1 7439 98 7 7782 49 2 7440 22 4 Test Method 7439 97 6 Test Method Test Parameter SW846 6010B (Water) ARSENIC BARIUM CADMIUM CHROMIUM COBALT LEAD MOLYBDENUM SELENiJM SILVER SW846 7470A MERCURY SW846 8260B (Water) Result Me'als Analysis by ICP 6010 U 80 6 U u u u u u u Units ug/L ug/L ugL ug/L ug L ug/L ug/L ug/L ug/L Mercury Analysis Volatile Organic Analysis U ug/L MDL 20 2 1 20 1 30 1 0 3 Dilution EQL Factor Analyst Test Date 100 10 5 50 5 00 5 150 5 67 64 1 ACETONE U ug/L 5 10 1 QC 06/04/ 0 71-43 2 BENZENE U ug/L 0 22 10 1 QC 06/04/10 74 97 5 BROMOCHLOROMETHANE u ug/L 0 31 10 1 QC 06/04/10 75 27-4 BROMODICHLOROMETHANE u ug/L 0 19 10 1 QC 06/04/10 108 85 1 BROMOBENZENE u ug/L 0 37 10 1 QC 06/04/10 75 26 2 BROMOFORM u ug/L 0 42 10 1 QC 06/04/10 74 83 9 BROMOMETHANE L ug/L 0 57 10 1 QC 06/04/10 78 93 3 2 BUTANONE U ug/L 1 11 10 1 QC 06/04/10 104 51 8 N BUTYLBENZENE U ug/L 03 10 1 QC 06/04/10 135 98 8 SEC BUTYLBENZENE U ug/L 0 4 10 1 QC 06/04/10 98 06 6 TERT BUTYLBENZENE u ug/L 04 10 1 QC 06/04/10 75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 06/04/10 56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 06/04/10 108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 QC 06/04/10 75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 06/04/10 110 75 8 2 CHLOROETHYLVINYL ETHER u ug/L 1 71 10 1 QC 06/04/10 67 66 3 CHLOROFORM u ug/L 0 3 10 1 QC 06/04/10 74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 06/04/10 95-49 8 2 CHLOROTOLUENE u ug/L 0 24 10 1 QC 06/04/10 106-43 4 4 CHLOROTOLUENE u ug/L 0 15 10 1 QC 06/04/10 124-48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 06/04/10 96 12 8 1 2 DIBROMO 3 CHLOROPROPANE u ug/L 0 35 10 1 QC 06/04/10 74 95 3 DIBROMOMETHANE u ug/L 0 25 10 1 QC 06/04/10 106 93-4 1 2 OIBROMOETHANE u ug/L 0 15 10 1 QC 06/04/10 95 50 1 1 2 DlCHLOROBENZENE u ug/L 5 86 10 1 QC 06/04/10 541 73 1 1 3 DlCHLOROBENZENE u ug/L 5 62 10 1 QC 06/04/1 0 i06 46 7 1 4 DlCHLOROBENZENE u ug/L 5 88 10 1 QC 06/04/10 75 71 8 DICHLORODIFLUOROMETHANE u ug/L 0 66 10 1 QC 06/04/10 75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 06/04/10 107 06 2 1 2 DICHLOROETHANE L ug/L 0 29 10 1 QC 06/04/10 75 35 4 1 1 DICHLOROETHENE u ug/^ 0 16 10 1 QC 06/04/10 156 59 4 C'S 1 2 DICHLOROETHENE u ug/L 0 16 0 1 QC 06 04/ 0 56 60 5 TRANS 1 2 DICHLOROETHENE J g'L C 34 10 QC 06(04/10 78 87 5 1 2 DICHLOROPROPANE L ug/^ 0 6 0 1 QC 05 04'-!0 142 28 9 1 3 DICHLOROPROPANE u jg L 0 24 10 1 QC 05/04/ 0 563 58 6 1 D CHLOROPRQPENE J g/L C 7 10 QC C6'04 -!0 10061 Oi 5 C'S 1 3 D CHLORQPROPENE u ug/-0 4 lO 1 06'C4/ 0 MTB MTB MTB MTB MTB MTB MTB MTB MTB TCP 06/07/IC 06/07/10 06/07/10 06/07/10 06/07/1C 06/07/10 06/07/10 06/07/ 0 06/07/10 06/08/1 0 Page 10 of 12 Pnnted 06/16/10 11 21 Listing of Results by Sample Sample Delivery Group 1006008 Client Sample ID Shot Gun Spnng Laboratory Sample ID 1006008 04 Sample Description ATK DLV Groundwater Spnng Sampling 2010 Date Sampled 06/01/10 13 20 CAS Number Test Parameter Result Units MDL Dilution EQL Factor Analyst Test Date Test Method SW 846 8260B (Water) Volatile 0 game Ana ysis 10061 02 6 TRANS 1 3 DICHLOROPROPENE U ug/_ 0 4 10 1 QC 06/04/10 590 20 7 2 2 DICHLOROPROPANE U ug L 0 9 10 1 QC 06/04/10 100 41 4 ETHYLBENZENE u ug/L 0 16 10 1 QC 06/C4/10 591 78 6 2 HEXANONE u ug/L 0 7 10 1 QC 06/04/10 87 68 3 HEXACHLOROBUTADIENE U g/L 0 9 10 1 QC 06/04/lO 98 82 8 ISOPROPYLBENZENE U ug/L 0 58 10 1 QC 06/04/10 99 87 6 4 ISOPROPYLTOLUENE u ug/L 0 24 10 1 QC 06/04/10 75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 06/04/ 0 108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 QC 06/04/10 91 20 3 NAPHTHALENE u ug/L 4 10 1 QC 06/04/10 103 65 1 N PROPYLBENZENE u ug/L 0 5 10 1 QC 06/04/10 100-42 5 STYRENE u ug/L 0 3 10 1 QC 06/04/10 630 20 6 1112 TETRACHLOROETHANE u ug/L 0 25 10 1 QC 06/04/10 79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 06/04/10 127 18 4 TETRACHLOROETHENE u ug/L 0 4 10 1 QC 06/04/10 108 88 3 TOLUENE u ug/L 0 5 10 1 QC 06/04/10 87 61 6 1 2 3 TRICHLOROBENZENE u ug/L 0 23 10 1 QC 06/04/10 120 82 1 1 2 4 TRICHLOROBENZENE u ug/L 4 37 10 1 QC 06/04/10 71 55 6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 05/04/10 79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 06/04/10 79 01 6 TRICHLOROETHENE 5 1 J ug/L 07 10 1 QC 06/04/10 75 69 4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 06/04/10 96 18-4 1 2 3 TRICHLOROPROPANE u ug/L 0 33 10 1 QC 06/04/10 95 63 6 1 2 4 TRIMETHYLBENZENE u ug/L 0 19 10 1 QC 06/04/10 108 67 8 1 3 5 TRIMETHYLBENZENE u ug/L 0 29 10 1 QC 06/04/10 108 05 4 VINYL ACETATE u ug/L 20 50 1 QC 06/04/10 75 01-4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 06/04/10 1330 20 7 mp XYLENE u ug/L 0 6 10 1 QC 06/04/10 95-47 6 o-XYLENE u ug/L 0 3 10 1 QC 06/04/10 460 00 4 BROMOFLUOROBENZENE 97 9 % 1 QC 06/04/10 1868 53 7 DIBROMOFLUOROMETHANE 104 / 1 QC 06/04/10 17060 07 0 1 2 DICHLOROETHANE D4 110 y 1 QC 06/04/10 2037 26 5 TOLUENE D8 97 4 % 1 QC 06/04/10 Page 11 of 12 Pnrted 06/16/10 1121 Data Reporting Qualifiers Indicates that the analyte concentration is less than the MDL This flag is used when an analyte is found in the blank as well as the sample Indicates an extimated value This flag is used either when estimating a concentration for tentatively identified compounds or when the data indicated the presence of a compound that meets the identification criteria but the result is less than the EQL (e g 3 J with an EQL of 10) MDL Method Detection Limit The minimum concentration of a substance that can be confidently measured and reported The laboratory has demonstrated that the MDL can be achieved in a laboratory reagent blank but does not guarantee it can be achieved in all sample matrices EQL Estimated Quantitation Limit The EQL generally is 5 to 10 times the MDL For many analytes the EQL is selected as the value of the lowest standard in the calibration curve Dilution Dilution Factor The prepared sample was diluted by this factor because the Factor sample was too concentrated or due to other interferences in the sample matrix Any dilution factor causes a corresponding increase in the MDL and EQL Page 12 of 12 Pnnted 06/16/10 11 21 ATK Launch Systems Environmental Laboratory Sample Receipt Checklist Client Name SDC So Camer Z Hand del verea no cooier CaTe Njnber 3 hard deltvered samp e(5) aKcnoL at receivirg ccLn er Cooler Information Cooler Number/ID Coid'tion of Stiipping Coitainer Cooler Sealed (taped) custody Seals Present Coolant State of Coolan ZYes •Yes • Intact jrair •Broken •Blue Ice zNone •Frozen partially Frozen CF • NO App cable • No Appii.^ble • NotAppioali'e .Damaged (expain, _ Seal N-mber , Otner Thermometer ID SIMJ^SO Reading V C Packing Descnption • Vie ed Con-eced Temp _ Temp Blank Included _Yes Ctialn-Of-Custody Information coo Present r- ,n i , COO Number(3) •g /•? / 6»5" No'es. COC signed (relinquished and received) p^es COC or LWI agrees with sample labels R/es •No CNo • No other •Not Applicable DNot Applicable Sample Information Samples included in cooler custody Seals Present Sample containers Intact Samples in proper containers Suffiaent sample volume All samples received In hold time •Yes •Intact iSfe% AYes 4Ves iVes water - VOA s have zero headspace pi^re-preserved with HOI Notes •Broken CNo •No DNo ONo other Seal Number(s). Notes jrt'es •No CNot Applicable Qpre-presecved with l>ta2S20] ONon Preserved water - pH acceptable upon receipt HN0j = . •Adjusted (see comments below) GNot/Applicable _HjS04 = NaOH = ZnAC /NaOH = HCL water pH adjusted (mfg & Lot No) HNOj HjSO,. NajSOA Other _ Notes NaOH 2nAC HCI SOP 102 Form A o(/l(n^//(? 2010 Spring GW Sampling 1006008 SAMPLE NUMBER Sf^i'i^'^ ATK Launch Systems, Inc Promontory, UTAH (801) 251-5688 DATE SAMPLER ANALYTICAL LABORATORY ATK Environmental Laboratory M53 Bottle NurtLber No of Containers Fid Preservative/ Treatment Requested Analysis 11 3 4 degrees C Acidified 2 mL HCL VOA, Appendix 9 Method 82 60 4T 1 5 mL HN03 As, Ba, Cd, Cr, Pb, Kg, Se, Ag Mo, Co EPA Method 6 010 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314 0 2010 Spring GW Sampling ATK Launch Systems, Inc Promontory, UTAH (801) 251-5688 SAMPLE NUMBER Spfl^ DATE ^// SAMPLER U^?:!^'^fJ^y^^ 1006008 ANALYTICAL LABORATORY ATK Environmental Laboratory M53 Bottle Number No of Containers Fid Preservative/ Treatment Requested Analysis 11 3 4 degrees C Acidified 2 mL HCL VOA, Appendix 9 Method 8260 4T 1 5 mL HN03 As, Ba, Cd, Cr, Pb, Hg, Se, Ag Mo, Co EPA Method 6010 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314 0 2 010 Spring GW Sampling 1006008 SAMPLE NUMBER ATK Launch Systems, Inc Promontory, UTAH (801) 251-5688 SAMPLER DATE ^////^ ANALYTICAL LABORATORY ATK Environmental Laboratory M53 Bottle No of Preservative/ Number Containers Fid Treatment Recjuested Analysis 11 4 degrees C Acidified 2 mL HCL VOA, Appendix 9 Method 8260 4T 5 mL HN03 As, Ba, Cd, Cr, Pb, Hg, Se, Ag Mo, Co EPA Method 6010 4 degrees C Perchlorate, Conductivity EPA Method 314 0 2010 Spring GW Sampling ATK Lavinch Systems, Inc Promontory, UTAH , , (801) 251-5688 SAMPLE NUMBER .^(/•(w?^ DATE <^/( /l£> SAMPLER 1006008 ANALYTICAL LABORATORY ATK Environmental Laboratory MS3 Bottle Number No of Containers Fid Preservative/ Treatment Requested Analysis 11 3 4 degrees C Acidified 2 mL HCL VOA, Appendix 9 Method 8260 4T 1 5 mL HN03 As, Ba, Cd, Cr, Pb, Hg, Se, Ag Mo, Co EPA Method 6010 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314 0 1006009 ENVIRONMENTAL LAB WORK REQUEST ^° ATK ENVIRONMENTAL LABORATORY ' LWR \o E13166 ' Logm No FROM EXTENSION COST CENTER WORK ORDER DATE ORGAMZATION ^UILST0P REPORT RESLLTS TO HELEN RAVSTEN MS 301 SAMPLE INFORMATION SAMPLE DATE TYPE LOCATION TIME TEST REMARKS SAMPLE DATE G c LOCATION TIME TEST REMARKS I / X If f( n 'f 3 LF- / X ^' ,t tr If ^ g-s X u f( n " 5 6 7 8 9 10 11 1 CHAIN OF CUSTODY RELpC^^^^ED BY DATE TIME RECEIVED BY DATE TIME A5 //£> FOR LABORATORY LSE ONLY DATE COMPLETED DATE REPORTED 988P LS333 GW CERTIFICATE OF ANALYSIS Listing of Sample Information and Testing Requested Wednesday, June 16, 2010 TESTED FOR ATK DLV Environmental Monitonng Thiokol Corp, UT 84322 ANALYZED BY ATK Launch Systems Analytical Chemistry Laboratory P O Box 707, M/S 245 Bngham City, UT 84302-0707 435-863-3732 435-863-8080 Contact Name Project Sample Delivery Group Al Lee Ground Water Testing - DLV 1006009 Page 1 of 11 Pnnted 06/16/10 11 23 Sample Delivery Group 1006009 Sample No Client No Test Requested 1006009 01 D5 Sample Description Received Collect Date/Time Matrix 06/03/10 6/2/2010 14 40 59 EPA 120 1 EPA 314 0 SW 846 8260B (Water) 1006009 02 D4 Conductivity Perctilorate Ion Chronatograpny Volatile Organic Analysis Water Water Water 06/03/10 6/2/2010 15 20 59 EPA 120 1 EPA 314 0 SW 846 8260B (Water) 1006009 03 LF 1 Conductivity Perchlora'e Ion Chromatography Volatile Organic Analysis Water Water Water 06/03/10 6/2/2010 16 30 59 EPA 120 1 EPA 314 0 SW 846 8260B (Water) i 1006009 04 B3 Conductivity Perchlorate Ion Chromatography Volatile Organic Analysis Water Water Water 06/03/10 6/2/2010 17 30 59 EPA 120 1 EPA 314 0 SW 846 8260B (Water) SW846 8330A Conductivity Perchlorate Ion Chromatography Volatile Organic Analysis Explosives Extraction Water Water Water Water Page 2 of 11 Pnnted 06/? 6/? 0 ) 1 23 Sample Delivery Group 1006009 Sample No Client No Test Requested 1006009 04 B3 Sample Description Received Collect Date/Time Matrix 06/03/10 6/2/2010 17 30 59 SW 846 8330A Moa (Water) Explosives Analysis Water Certified By W Scott Fraser Quality Assurance Officer 06/17/2010 Date This certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation Program (NELAP) unless othenMise annotated Page 3 of 11 Pnn'ed 06/16/10 11 23 Listing of Results by Sample Sample Delivery Group 1006009 Ghent Sample ID D5 Sample Description ATK DLV G oundwater Spnng 20 lO Laboratory Sample ID 1006009 01 Date Sampled 06/02/10 14 40 AS Number Dilution AS Number Test Parameter Result Units MDL Factor Analvst Test Date Test Method EPA 1201 Cora ^ivty CONDUCTIViTY 1950 uS/CT 0 3 1 1 JWM 06/14/10 TestMethod EPA 314 0 Pe chlorate Ion Chromatography 014797 73 0 PERCHLORATE 200000 ug/L 1000 4C0C lOOO JVM 06/ 5/10 Test Method SW846 8260B (Water) Volatile Organic Analysis 67 64 1 ACETONE U ug/L SO -00 10 QC 06/04/10 71-43 2 BENZENE J ug/L 2 2 100 10 QC 06/04/10 74 97 5 BROMOCHLOROMETHANE U ug/L 3 1 100 10 QC 06/04/10 75 27 4 BROMODiCHLOROMETriANE U ug/L 1 9 100 10 QC 06/04/1 0 108 86 1 BROMOBENZENE U ug/L 3 7 100 10 QC 06/04/10 75 25 2 BROMOFORM U ug/L 4 2 100 10 QC 06/04/10 74 83 9 BROMOMETHANE U ug/L 5 7 100 10 QC 06/04/10 78 93 3 2 BUTANONE U ug/L 11 1 100 10 QC 06/04/10 104 51 8 N BUTYLBENZENE U ug/L 3 100 10 QC 06/04/10 135 98 8 SEC BUTYLBENZENE U ug/L 4 100 10 QC 06/04/10 98 06 6 TERT BUTYLBENZENE U ug/L 4 100 10 QC 06/04/1 0 75 15 0 CARBON DISULFIDE u ug/L 1 3 100 10 QC 06/04/1 0 56 23 5 CARBON TETRACHLORIDE U ug/L 2 7 100 10 QC 06/04/10 108 90 7 CHLOROBENZENE U ug/L 1 6 100 10 QC 06/04/10 75 00 3 CHLOROETHANE u ug/L 3 5 100 10 QC 06/04/10 110 75 8 2 CHLOROETHYLVINYL ETHER U ug/L 17 1 ]00 10 QC 06/04/10 67 66 3 CHLOROFORM U ug/L 3 100 10 QC 06/04/10 74 87 3 CHLOROMETHANE U ug/L 8 1 100 10 QC 06/04/10 95-49 8 2 CHLOROTOLUENE u ug/L 24 100 10 QC 06/04/10 106 43 4 4 CHLOROTOLUENE u ug/L 1 5 100 10 QC 06/04/10 124-48 1 DIBROMOCHLOROMETHANE u ug/L 1 8 100 10 QC 06/04/10 96 12 8 1 2 DIBROMO 3 CHLOROPROPANE u ug/L 3 5 100 10 QC 06/04/10 74 95 3 DIBROMOMETHANE u ug/L 2 5 100 10 QC 06/04/10 106 93 4 1 2 DIBROMOETHANE u ug/L 1 5 100 10 QC 06/04/10 95 50 1 1 2 DlCHLOROBENZENE u ug/L 58 6 100 10 QC 06/04/10 541 73 1 1 3 DlCHLOROBENZENE u ug/L 56 2 100 10 QC 06/04/10 106-46 7 1 4 DlCHLOROBENZENE u ug/L 58 8 100 10 QC 05/04/10 75 71 8 DICHLORODIFLUOROMETHANE u ug/L 66 100 10 QC 06/04/10 75 34 3 1 1 DICHLOROETHANE u ug/L 4 9 100 10 QC 06/04/10 107 06 2 1 2 DICHLOROETHANE u ug/L 2 9 100 10 QC 06/04/10 75 35-4 1 1 DICHLOROETHENE 6 2 J ug/L 1 6 100 10 QC 06/04/10 156 59 4 CIS 1 2 DICHLOROETHENE u ug/L 1 6 100 10 QC 06/04/10 156 60 5 TRANS 1 2 DICHLOROETHENE u ug/L 3 4 100 10 QC 06/04/10 78 87 5 1 2 DICHLOROPROPANE u ug/L 1 6 100 10 QC 06/04/10 142 28 9 1 3 DICHLOROPROPANE u ug/L 2 4 100 10 QC 06/04/10 563 58 6 1 1 DICHLOROPROPENE u ug/L 1 7 100 10 QC 06/04/10 10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 4 100 10 QC 05/04/10 10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 4 100 lO QC 06/04/10 590 20 7 2 2 DICHLOROPROPANE u ug/L 9 10C 10 QC 06/04/10 100 41 4 ETHYLBENZENE u ug/L 1 6 100 10 QC 06/04/10 591 78 6 2 HEXANONE J ug/L 7 100 10 QC 06/04/1 0 87 68 3 HEXACHLOROBUTADIENE u jg/L 9 ^00 10 QC 06/04/10 98 82 8 ISOPROPYLBENZENE u -g/L 5 8 00 G QC 06/04/10 99 87 6 4 SOPROi^^LTO-v^ESE L ug/L 2 4 1 CO 0 QC 06/04/1C 75 C9 2 ViE"rHVLENE CH ORIDE u ugU 8 IOC 0 QC 06/04/10 Page 4 of 11 Printed 06/16/10 1123 Listing of Results by Sample Sample Delivery Group 1006009 Client Sample ID D5 Sample Description ATK DLV Groundwater Spring 2010 Laboratory Sample ID Date Sampled 1006009 01 06/02/10 14 40 CAS Number Test Parameter Result Units MDL EQL Dilution Factor Analvst Test Date Test Method SW 846 8260S (Water) Voia iie 0 gar c Analys s 108 10 1 4 METHYL 2 PENTANONE U ug/L 5 3 00 10 QC 06/04/10 91 20 3 NAP-THALENE u ug/L 40 100 0 QC 06/04/10 103 65 1 N PROPYLBENZENE L ug/L 5 100 10 QC 06/04/10 100 42 5 STYRENE L jg/L 3 100 10 QC 06/04/ 0 630 20 6 1112 TETRACHLOROETHANE J ug/L 2 5 ;00 10 QC 06/04/10 79 34 5 112 2 TETRACHLOROE"^HANE u ug/L 8 5 100 10 QC 05/04/10 127 18 4 TETRACHLOROETHENE u ug/L 4 100 10 QC 06/04 10 108 88 3 TOLUENE u ug/L 5 100 10 QC 06/04/10 87 61 6 1 2 3 TRICHLOROBENZENE u ug/L 2 3 100 10 QC 06/04/10 120 82 1 2 4 TRICHLOROBENZENE u ug/L 43 7 100 10 QC 06/04/10 71 55 6 1 1 TRICHLOROETHANE u ug/L 1 6 100 10 QC 06/04/10 79 00 5 1 1 2 TRICHLOROETHANE u ug/L 2 5 100 10 QC 06/04/10 79 01 6 TRICHLOROETHENE 340 ug/L 7 100 10 QC 06/04/10 75 69 4 TRICHLOROFLUOROMETHANE U ug/L 3 100 10 QC 06/04/10 96 18-4 1 2 3 TRICHLOROPROPANE U ug/L 3 3 100 10 QC 06/04/10 95 63 6 1 2 4 TRIMETHYLBENZENE U ug/L 1 9 100 10 QC 06/04/10 108 67 8 1 3 5 TRIMETHYLBENZENE U ug/L 2 9 100 10 QC 06/04/10 108 05 4 VINYL ACETATE U ug/L 200 500 10 QC 06/04/10 75 01-4 VINYL CHLORIDE u ug/L 3 100 10 QC 06/04/10 1330 20 7 m p XYLENE u ug/L 6 100 10 QC 06/04/10 95-47 6 0 XYLENE u ug/L 3 100 10 QC 06/04/10 460 00 4 BROMOFLUOROBENZENE 93 7 V 10 QC 06/04/10 1868 53 7 DIBROMOFLUOROMETHANE 105 / 10 QC 05/04/10 17060 07 0 1 2 DICHLOROETHANE D4 110 / 10 QC 06/04/10 2037 26 5 TOLUENE D8 95 2 / 10 QC 06/04/10 Client Sample ID D4 Laboratory Sample ID 1006009 02 Sample Description ATK DLV Groundv^ater Spnng 2010 Date Sampled 06/02/10 15 20 CAS Number Test Parameter Result Units MDL EQL Dilution Factor Analyst Test Date Test Method EPA 120 1 Conductivity CONDUCTIVITY 1340 uS/cm 0 3 1 1 JMM 05/14/10 Test Method EPA 314 0 Perchlorate Ion Chromatography 014797 73 0 PERCHLORATE 135000 ug/L 1000 4000 1000 JMM 06/15/10 Test Method SW 846 8260B (Water) Volatile Organic Analysis 67 64 1 ACETONE U ug/L 5 10 1 QC 06/04/10 71-43 2 BENZENE U ug/L 0 22 10 1 QC 06/04/10 74 97 5 BROMOCHLOROMETHANE U ug/L 0 31 10 1 QC 06/04/10 75 27 4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 06/04/10 ,08 86 1 BROMOBENZENE U ug/L 0 37 10 1 QC 06/04/10 75 25 2 BROMOFORM U ug/i. 0 42 10 1 QC 06/04/10 74 83 9 BROMOMETHANE U ug'L 0 57 10 1 QC 06/04/10 78 93 3 2 BUTANONE U ug/L 1 -10 QC 06 04 0 104 5 8 N BUTYLBENZENE u ug/-0 3 10 1 QC 06/04 10 135 98 8 SEC BUTYLBENZENE J -g ^ 0 4 10 QC 06/04/10 98 06 6 TER^ 3U~v_BENZENE J ug/^ 0 4 0 QC 06 04 C 75 C CARBON DISULFIDE U ug L 0 13 0 1 QC C6'04/10 Page 5 of 11 Pnn(ed 06/16/10 1123 Listing of Results by Sample Sample Delivery Group 1006009 Client Sample ID D4 Sample Description ATK DLV Groundvi/ater Spring 2010 Laboratory Sample 10 Date Sampled 1006009 02 06/02/10 15 20 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analvst Test Date TestMethod SW 846 8260B (Water) Vola ile 0 g jnic Aralys'.s 56 23 5 CARBON TETRACHLORIDE 22 jg -0 27 10 QC 06/04/1C 108 90 7 Ch.OROBENZENE U ug/L 0 6 10 QC 06/04/10 75 00 3 CHLOROETHANE U ug L 0 35 10 1 QC 06/04/10 110 75 8 2 CHLOROETHYLV NYL ETHER J ug/L 1 71 10 1 QC 06/04/10 67 66 3 Ch.OROtQRM 1 7 J ug/L 0 3 10 QC 06/04/10 74 87 3 CHLOROMETHANE U ug/L 0 81 10 1 QC 05/04/10 95-49 8 2 CHLOROTOLUENE U ugli-0 24 10 1 QC 06/04/10 106 43 4 4 CHLOROTOLUENE U ug/L 0 15 10 QC 06/04/10 124 48 1 DIBROMOCHLOROMETHANE U ug/L 0 18 10 1 QC 06/04/10 96 12 8 1 2 DIBROMO 3 CHLOROPROPANE U ug/L 0 35 10 1 QC 06/04/10 74 95 3 DIBROMOMETHANE U ug/L C 26 10 QC 06/04/10 106 93 4 1 2 DIBROMOETHANE u ug/L 0 15 10 1 QC 06/04/10 95 50 1 1 2 DlCHLOROBENZENE u ug/L 5 86 10 1 QC 06/04/10 541 73 1 1 3 DlCHLOROBENZENE u ug/L 5 62 10 1 QC 06/04/10 106 46 7 1 4 DlCHLOROBENZENE u ug/L 5 88 10 1 QC 06/04/10 75 71 8 DICHLORODIFLUOROMETHANE u ug/L 0 66 10 1 QC 06/04/10 75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 06/04/10 107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 06/04/10 75 35 4 1 1 DICHLOROETHENE 11 4 ug/L 0 16 10 1 QC 06/04/10 156 59 4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 06/04/10 156 60 5 TRANS 1 2 DICHLOROETHENE u ugL 0 34 10 1 QC 06/04/10 78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 06/04/10 142 28 9 1 3 DICHLOROPROPANE u ug/L 0 24 10 1 QC 06/04/10 563 58 6 1 1 DICHLOROPROPENE u ug/L 0 17 10 1 QC 06/04/10 10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 0 4 10 1 QC 06/04/10 10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 06/04/10 590 20 7 2 2 DICHLOROPROPANE u ug/L 0 9 10 1 QC 06/04/10 100-41 4 ETHYLBENZENE u ug/L 0 16 10 1 QC 05/04/10 591 78 6 2 HEXANONE u ug/L 07 10 1 QC 06/04/10 67-68 3 HEXACHLOROBUTADIENE u ug/L 0 9 10 1 QC 06/04/10 98 82 8 ISOPROPYLBENZENE u ug/L 0 58 10 1 QC 06/04/10 99 87 6 4 ISOPROPYLTOLUENE u ug/L 0 24 10 1 QC 06/04/10 75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 05/04/10 108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 06/04/10 91 20 3 NAPHTHALENE u ug/L 4 10 1 QC 05/04/10 103 65 1 N PROPYLBENZENE u ug/L 0 5 10 1 QC 05/04/10 100-42 5 STYRENE u ug/L 0 3 10 1 QC 06/04/10 630 20 6 1112 TETRACHLOROETHANE u ug/L 0 25 10 1 QC 05/04/10 79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 06/04/10 127 18-4 TETRACHLOROETHENE u ug/L 04 10 1 QC 06/04/10 108 88 3 TOLUENE u ug/L 0 5 10 1 QC 06/04/10 87 61 6 1 2 3 TRICHLOROBENZENE u ug/L 0 23 10 1 QC 05/04/10 120 82 1 1 2 4 TRICHLOROBENZENE u ug/L 4 37 10 1 QC 06/04/10 71 55 6 1 1 1 TRICHLOROETHANE 2 1 J ug/L 0 16 10 QC 06/04/10 79 0" 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 06/04/10 79 0 5 TRICHLOROE-'HENE 40 8 g/L 0 7 10 1 QC 05/04/10 75 69 4 TRICHLOROFLLOROMETHANE 0 8 ' ug/L 0 3 0 QC 06/04/10 96 16 4 1 2 3 "RiCHLOROPROPANE u ug/-0 33 0 1 QC 06 04 1 0 95 63 6 1 2 4 'RlWiETl-'^LBENZENE J -g 1-u IS 1.. 1 QC 05'04' C 08 67 8 1 3 5 TRSVETHVLBENZENE 9 L u 29 0 QC C6/04'10 Page 6 of 11 Pnnted 06/16/10 11 23 Listing of Results by Sample Sample Delivery Group 1006009 Client Sample ID D4 Sample Description ATK DLV Groundv/ater Spnng 2010 Laboratory Sample ID 1006009 02 Date Sampled 06/02/10 15 20 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date Test Method SW 846 82608 (Water) Vola i e Crga ic A alysis 108 05 4 VINYL ACETA'E U ug/L 20 50 1 QC 06/04/10 75 01 4 ViNYL CHLORIDE U ug/L 0 3 0 1 QC 06/04/10 1330 20 7 n p XYLENE U ug/L 0 6 10 1 QC 06/04/' 0 95 47 6 0 XYLENE U ug/-0 3 10 QC 06/04/10 450 00 4 BROMOFLUOROBENZENE 99 / QC 06/04/1 0 1868 53 7 DIBROMOFLUOROMETHANE 101 V 1 QC 06/04/10 17060 07 0 1 2 DICHLOROETHANE D4 105 / 1 QC 06/04/10 2037 26 5 TOLUENE D8 95 3 / 1 QC 06/04/10 Client Sample ID LF 1 Sample Description ATK DLV Groundwater Spring 2010 Laboratory Sample ID 1006009 03 Date Sampled 06/02/10 16 30 Dilution AS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date Test Method EPA 120 1 Conductivity CONDUCTIVITY 8180 uS/cm 0 3 1 1 JMM 06/14/10 Test Method EPA 314 0 Perchlorate Ion Chromatography 014797 73 0 PERCHLORATE 489 ug/L 10 40 10 JMM 06/15/10 TestMethod SW 846 8260B (Water) Volatile Organic Analysis 67 54 1 ACETONE U ug/L 5 10 1 QC 06/04/1 0 71-43 2 BENZENE U ug/L 0 22 10 1 QC 06/04/1 0 74 97 5 BROMOCHLOROMETHANE U ug/L 0 31 10 1 QC 05/04/10 75 27-4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 06/04/10 108 85 1 BROMOBENZENE U ug/L 0 37 10 1 QC 06/04/10 75 25 2 BROMOFORM U ug/L 0 42 10 1 QC 06/04/10 74 83 9 BROMOMETHANE U ug/L 0 57 10 1 QC 06/04/10 78 93 3 2 BUTANONE U ug/L 1 11 10 1 QC 06/04/10 104 51 8 N BUTYLBENZENE U ug/L 0 3 10 1 QC 06/04/10 135 98 8 SEC BUTYLBENZENE U ug/L 04 10 1 QC 06/04/10 98 06 6 TERT BUTYLBENZENE U ug/L 04 10 1 QC 06/04/10 75 15 0 CARBON DISULFIDE U ug/L 0 13 10 1 QC 06/04/10 56 23 5 CARBON TETRACHLORIDE U ug/L 0 27 10 1 QC 06/04/10 108 90 7 CHLOROBENZENE U ug/L 0 16 10 1 QC 06/04/10 75 00 3 CHLOROETHANE U ug/L 0 35 10 1 QC 06/04/10 110 75 8 2 CHLOROETHYLVINYL ETHER U ug/L 1 7 10 1 QC 06/04/10 67 66 3 CHLOROFORM U ug/L 0 3 10 1 QC 06/04/10 74 87 3 CHLOROMETHANE U ug/L 0 81 10 1 QC 06/04/10 95 49 8 2 CHLOROTOLUENE U ug/L 0 24 10 1 QC 06/04/10 106 43-4 4 CHLOROTOLUENE U ug/L 0 15 10 1 QC 05/04/10 124-48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 06/04/10 96 12 8 1 2 DIBROMO 3 CHLOROPROPANE u ug/L 0 35 10 1 QC 06/04/10 74 95 3 DIBROMOMETHANE J ug/L 0 25 10 1 QC 06/04/10 06 93 4 1 2 DIBROMOETHANE u ug/L 0 5 10 1 06/04/10 95 50 1 1 2 DiCH OROBENZENE u ug/L 5 86 10 1 QC 06/04 10 541 73 1 3 DlCHLOROBENZENE L ug/L 5 62 10 QC 05/04/10 06 46 7 1 4 DlCHLOROBENZENE -g/-5 88 c QC 06/04/1 u 75 7 8 D CHLOROD'-^JOROVEThANE S 0 66 QC C6/04/1C 75 34 3 DiC-J^CROE^HANE J .g/ 0 49 '0 1 QC 05/04/ 0 Page 7 of 11 Pnrted 06/16/10 11 23 Listing of Results by Sample Sample Delivery Group 1006009 Client Sample ID LF 1 Sample Description ATK DLV Grounawater Spnng 2010 Laboratory Sample ID Date Sampled 1006009 03 06/02/10 16 30 Dilution CAS Number Test Parameter Result Units MDL Factor Analvst Test Date Tes( Method SW 846 8260B (Water) Vola ile 0 game Analysis 107 06 2 1 2 DlCHLOROE''HANE U ug/L 0 29 10 QC 06/04/10 75 35 4 , 1 DICHLOROETHENE 05J jg/L " 6 0 1 QC 06/04/10 156 59 4 CIS 1 2 DICHLOROETHENE U ug/L 0 16 10 1 QC 05/04/10 156 60 5 TRANS 1 2 DICHLOROETHENE U ug/L 0 34 10 1 QC 06/04/10 78 87 5 2 DICHLOROPROPANE L ug/ 0 16 10 1 QC 06/04/10 142 28 9 3 DICHLOROPROPANE U ug/L 0 24 10 1 QC 06/04/10 563 58 6 1 1 DICHLOROPROPENE U ug/L 0 17 10 1 QC 06/04/10 10051 01 5 CIS 1 3 DICHLOROPROPENE U ug/L 04 10 1 QC 06/04/10 10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 06/04/10 590 20 7 2 2 DICHLOROPROPANE u ug/L 0 9 10 1 QC 06/04/10 100-41 4 ETHYLBENZENE u ug/L 0 16 10 1 QC 06/04/10 591 78 5 2 HEXANONE u ug/L 0 7 10 1 QC 06/04/10 87 58 3 HEXACHLOROBUTADIENE u ug/L 09 10 1 QC 06/04/10 98 82 8 ISOPROPYLBENZENE u ug/L 0 58 10 1 QC 06/04/10 99 87 5 4 ISOPROPYLTOLUENE u ug/L 0 24 10 1 QC 06/04/10 75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 06/04/10 108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 06/04/10 91 20 3 NAPHTHALENE u ug/L 4 10 1 QC 06/04/10 103 65 1 N PROPYLBENZENE u ug/L 0 5 10 1 QC 06/04/10 100 42 5 STYRENE u ug/L 0 3 10 1 QC 06/04/10 630 20 5 1112 TETRACHLOROETHANE u ug/L 0 25 10 1 QC 06/04/10 79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 06/04/10 127 18 4 TETRACHLOROETHENE u ug/L 04 10 1 QC 06/04/10 108 88 3 TOLUENE u ug/L 0 5 10 1 QC 06/04/10 87 61 6 1 2 3 TRICHLOROBENZENE u ug/L 0 23 10 1 QC 05/04/10 120 82 1 1 2 4 TRICHLOROBENZENE u ug/L 4 37 10 1 QC 06/04/10 71 55 5 1 1 1 TRICHLOROETHANE 4 J ug/L 0 16 10 1 QC 06/04/10 79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 06/04/10 79 01-6 TRICHLOROETHENE 34 2 ug/L 07 10 1 QC 06/04/10 75 69-4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 06/04/10 96 18-4 1 2 3 TRICHLOROPROPANE u ug/L 0 33 10 1 QC 05/04/10 95 63-5 1 2 4 TRIMETHYLBENZENE u ug/L 0 19 10 1 QC 06/04/10 108 67 8 1 3 5 TRIMETHYLBENZENE u ug/L 0 29 10 1 QC 06/04/10 108 05-4 VINYL ACETATE u ug/L 20 50 1 QC 06/04/10 75 01-4 VINYL CHLORIDE u ug/L 03 10 1 QC 05/04/10 1330 20 7 mp XYLENE u ug/L 06 10 1 QC 06/04/10 95-47 5 0 XYLENE u ug/L 0 3 10 1 QC 06/04/10 450 00 4 BROMOFLUOROBENZENE 95 8 / 1 QC 05/04/10 1868 53 7 DIBROMOFLUOROMETHANE 101 '/ 1 QC 06/04/10 17050 07 0 1 2 DICHLOROETHANE D4 109 V 1 QC 05/04/10 2037 26 5 TOLUENE D8 95 8 /„ 1 QC 06/04/10 Ghent Sample ID B3 Laboratory Sample ID 1006009 04 Sample Description ATK DLV Groundv^fater Spnng 2010 Date Sampled 06/02/10 17 30 CAS Number Test Parameter Result Units MDL EQL Dilution Factor Analvst Test Date Test Method EPA 120 1 Corduc vi y CONDJCTIV'TV 1440 uS/cn „ 3 1 1 MM 06/14/10 Page 8 of 11 Pnnted 06/16/10 1123 Listing of Results by Sample Sample Delivery Group 1006009 Client Sample ID 8 3 Sample Description ATK DLV Groundvi/ater Spring 2010 Laboratory Sample ID 1006009 04 Date Sampled 06/02/10 17 30 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date Test Method EPA 314 0 Perchlora e Ion Chronatog aohy 0 4797 73 0 =ERCHLGRATE 4080" ug/L 00 400 100 vv 06/15/10 Tesf Method SW 846 82608 (Water) Vola'ile Organ c Analysis 67 64 1 ACETONE U ug 250 500 50 QC 06/04/10 71 43 2 BENZENE U ug 1 500 50 QC 06/04/1 0 74 97 5 BROMOCHLOROMETHANE u ug/L 15 5 500 53 QC 06/04/10 75 27 4 BROMODICHLOROMETHANE J ug'L 9 5 500 50 QC 06/04/10 108 86 1 BROMOBENZENE u ug/L 18 5 500 50 QC 06/04/10 75 25 2 BROMOFORM u ug/L 2 500 50 QC 06/04/10 74 83 9 BROMOMETHANE u ug/L 28 5 500 50 QC 06/04/10 78 93 3 2 BUTANONE u ug/L 55 5 500 50 QC 06/04/10 104 51 8 N BUTYLBENZENE u ug/L 15 500 50 QC 06/04/10 135 98 8 SEC BUTYLBENZENE u ug/L 20 500 50 QC 06/04/10 98 05 6 TERT BUTYLBENZENE u ug/L 20 500 50 QC 06/04/10 75 15 0 CARBON DISULFIDE u ug/L 6 5 500 50 QC 06/04/10 56 23 5 CARBON TETRACHLORIDE u ug/L 13 5 500 50 QC 06/04/10 108 90 7 CHLOROBENZENE u ug/L 8 500 50 QC 06/04/10 75 00 3 CHLOROETHANE u ug/L 17 5 500 50 QC 06/04/10 110 75 8 2 CHLOROETHYLVINYL ETHER u ug/L 85 5 500 50 QC 05/04/10 57 66 3 CHLOROFORM u ug/L 15 500 50 QC 05/04/10 74 87 3 CHLOROMETHANE u ug/L 40 5 500 50 QC 05/04/10 95-49 8 2 CHLOROTOLUENE u ug/L 12 500 50 QC 06/04/10 106-43 4 4 CHLOROTOLUENE u ug/L 7 5 500 50 QC 06/04/10 124 48 1 DIBROMOCHLOROMETHANE u ug/L 9 500 50 QC 06/04/10 96 12 8 1 2 DIBROMO 3 CHLOROPROPANE u ug/L 17 5 500 50 QC 06/04/10 74 95 3 DIBROMOMETHANE u ug/L 12 5 500 50 QC 05/04/10 106 93 4 1 2 DIBROMOETHANE u ug/L 7 5 500 50 QC 06/04/10 95 50 1 1 2 DlCHLOROBENZENE u ug/L 293 500 50 QC 06/04/10 541 73 1 1 3 DlCHLOROBENZENE u ug/L 281 500 50 QC 05/04/10 106 46 7 1 4 DlCHLOROBENZENE u ug/L 294 500 50 QC 06/04/10 75 71 8 DICHLORODIFLUOROMETHANE u ug/L 33 500 50 QC 06/04/10 75 34 3 1 1 DICHLOROETHANE u ug/L 24 5 500 50 QC 06/04/10 107 05 2 1 2 DICHLOROETHANE u ug/L 14 5 500 50 QC 06/04/10 75 35-4 1 1 DICHLOROETHENE 500 ug/L 8 500 50 QC 06/04/10 156 59 4 CIS 1 2 DICHLOROETHENE u ug/L 8 500 50 QC 06/04/10 156 60 5 TRANS 1 2 DICHLOROETHENE u ug/L 17 500 50 QC 05/04/10 78 87 5 1 2 DICHLOROPROPANE u ug/L 8 500 50 QC 05/04/10 142 28 9 1 3 DICHLOROPROPANE u ug/L 12 500 50 QC 06/04/10 563 58 6 1 1 DICHLOROPROPENE u ug/L 8 5 500 50 QC 06/04/10 10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 20 500 50 QC 06/04/10 10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 20 500 50 QC 06/04/10 590 20 7 2 2 DICHLOROPROPANE u ug/L 45 500 50 QC 06/04/10 100-41 4 ETHYLBENZENE u ug/L 8 500 50 QC 05/04/10 591 78 6 2 HEXANONE u ug/L 35 500 50 QC 06/04/10 87 68 3 HEXACHLOROBUTADIENE u jg/i-45 500 50 QC 05/04/10 98 82 8 ISOPROPYL-BENZENE u ug/L 29 500 50 QC 05/04/10 99 87 5 4 ISOPROPYLTOLUENE u ug/L 12 50" 5C QC 06/04/10 75 09 2 METHYLENE CHLORIDE u ug/L 40 500 50 QC 05 04 '0 1C8 10 1 4 METHYL 2 OENTANCNE -g/ 26 5 500 to QC 06'C4/ 0 9 20 3 NAPrTnALENE J ug' 20 500 53 QC 06'C4/ u 03 65 1 N PROPv.BENZENE L ug/i-25 500 5.. QC 06/04 10 Page 9 of 11 Pnnted 06/16/ Oil 23 Listing of Results by Sample Sample Delivery Group 1006009 Client Sample ID B3 Sample Description ATK DLV Groundvi/ater Spnng 2010 Laboratory Sample ID Date Sampled 1006009 04 06/02/10 17 30 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date Tesf Method SW 846 8260fi (Water) Volati e Organ c Analysis ICO 42 5 STYRENE U ug/L 15 500 50 QC 06/04/lO 630 2^ 6 1 1 2 TETRACHLOROETHANE u jg/L 12 5 500 50 QC 06/04/10 79 34 5 112 2 TE^RACHLOROE-^HANE u ug/L 42 5 500 50 QC 06/04/ 0 27 18 4 TETRACHLOROETHENE u ug/L 20 500 50 QC 06/04/10 108 8B 3 TOLUENE J ug/L 25 500 50 QC 06/04/ 0 87 61 6 1 2 3 TRICHLOROBENZENE u jg/L 11 5 500 50 QC 06/04/10 120 82 1 1 2 4 TRICHLOROBENZENE u ug/L 218 5 500 50 QC 06/04/10 71 55 5 1 1 1 TRICHLOROETHANE 500 J ug/L 8 500 50 QC 06/04/10 79 00 5 1 1 2 TRICHLOROETHANE U ug/L 12 5 500 50 QC 06/04/10 79 01 6 TRICHLOROETHENE 3270 ug/L 35 500 50 QC 06/04/10 75 69 4 TRICHLOROFLUOROMETHANE U ug/L 15 500 50 QC 06/04/10 96 18 4 1 2 3 TRICHLOROPROPANE U ug/L 16 5 500 50 QC 06/04/10 95 53 6 1 2 4 TRIMETHYLBENZENE U ug/L 9 5 500 50 QC 06/04/10 108 67 8 1 3 5 TRIMETHYLBENZENE U ug/L 14 5 500 50 QC 06/04/10 108 05 4 VINYL ACETATE U ug/L 1000 2500 50 QC 05/04/10 75 01 4 VINYL CHLORIDE U ug/L 15 500 50 QC 05/04/10 1330 20 7 mp XYLENE U ug/L 30 500 50 QC 06/04/10 95 47 5 0 XYLENE U ug/L 15 500 50 QC 06/04/10 460 00 4 BROMOFLUOROBENZENE 93 5 /o 50 QC 06/04/10 1868 53 7 DIBROMOFLUOROMETHANE 104 / 50 QC 06/04/10 17060 07 0 1 2 DICHLOROETHANE D4 109 / 50 QC 06/04/10 2037 26 5 TOLUENE D8 96 7 V 50 QC 06/04/10 Tesf Method 5^846 8330^ Explosives Extraction DATE COMPLETED 06/09/2010 1 JNB 06/09/10 00 00 Test Method SIV846 8330/) Mod (Wafer; Explosives Analysis 2591 41 0 HMX 2 70 ug/L 0 3 1 1 JNB 06/10/10 121 82 4 RDX 1 94 ug/L 0 3 1 1 JNB 06/10/10 99 08 1 3 NITROTOLUENE 99 2 / 1 JNB 06/10/10 Page 10 of 11 Prnted 06/16/10 11 23 Data Reporting Qualifiers Indicates that the analyte concentration is less than the MDL This flag is used when an analyte is found in the blank as well as the sample Indicates an extimated value This flag is used either when estimating a concentration for tentatively identified compounds or when the data indicated the presence of a compound that meets the identification criteria but the result is less than the EQL (e g 3 J with an EQL of 10) MDL Method Detection Limit The minimum concentration of a substance that can be confidently measured and reported The laboratory has demonstrated that the MDL can be achieved in a laboratory reagent blank but does not guarantee it can be achieved in all sample matnces EQL Estimated Quantitation Limit The EQL generally is 5 to 10 times the MDL For many analytes the EQL is selected as the value of the lowest standard m the calibration curve Dilution Dilution Factor The prepared sample was diluted by this factor because the Factor sample was too concentrated or due to other interferences in the sample matnx Any dilution factor causes a corresponding increase in the MDL and EQL Page 11 of 11 Pnnted 06/16/10 1123 ATK Launch Systems Environmental Laboratory Sample Receipt Checklist C lent Name 10(^X^00^ SDG No Carr er ; Hard delivered no cooler Car ler Numoer • Hand delivered sample(s) taken out at ece vi g counter Cooler Information , Cooler Number/ID _^ood ives rYes _ Intact >ce ^Frozen Thermometer ID Reading _ Packing Description Condi lor of Shipping Con ainer Coole Sealed (aped) Custody Sea's Present Coolant State 0 Coolant -Fair -Broken IBIue Ice ;:None -Pa'tially Frozen Jfi C C'=_ -Not App icable ;Not Applicab e ZNot Applicable -Damagea (exp a i) _ Seal Nurrbe Ohe "Melted Corrected Temp _ Temp Blank ncluded ^Yes Chain Of Custody Information COC Present ^ , , , 3(fe COC Number{s) »*fe> COC signed (relinquished and rece ved) Jfy'e: COC or LWI agrees with sample labels j!ile Notes :NO JNo •No Olher DNot Applicable :Not Applicable Sample Information Samples included in cooler Custody Seals Present Sample containers intact Samples In proper con ainers Sufficient sample volume All samples received in hold time LYes GIntact Xres ^es ^es Water - VOA s have zero headspace p(f re-preserved with HCI Notes Other •Broken Seai Number(s)_ "No Notes •No CNo L.NO ^es DNo '"Not Applicable CPre preserved with NajSjOj •Non Preserved Water - pH acceptable upon receipt CYes rAdjusted (see commen s below) jj^o' Applicable HNOj = HjSO = NaOH = ZnAC /NaOH = HCL = . Water pH adjusted (mfg & Lot No) HNOj HjSO, NajSOjOj Other. Notes NaOH ZnAC HCI SOP 102 Form A 2 010 Spring GW Sampling 1006009 SAMPLE NUMBER ATK Launch Systems, Inc Promontory, UTAH (801) 251-5688 DATE SAMPLER ANALYTICAL LABORATORY ATK Environmental Laboratory MS3 Bottle Number No of Containers Fid Preservative/ Treatment Requested Analysis 11 3 4 degrees C VOA, Appendix 9 Acidified Method 8260 2 mL HCL 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314 0 2 010 Spring GW Sampling 1006009 ATK Launch Systems, Inc Promontory, UTAH (801) 251-5688 SAMPLE NUMBER DATE SAMPLER ANALYTICAL LABORATORY ATK Environmental Laboratory M53 Bottle No of Preservative/ Nuii±)er Containers Fid Treatment Requested Analysis 11 4 degrees C Acidified 2 mL HCL VOA, Appendix 9 Method 8260 4 degrees C Perchlorate, Conductivity EPA Method 314 0 2 010 Spring GW Sampling ATK Launch Systems, Inc Promontory, UTAH (801) 251-5688 SAMPLE NUMBER Lf^l DATE ^I^LjlO SAMPLER 1006009 ANALYTICAL LABORATORY ATK Environmental Laboratory M53 Bottle Number No of Containers Fid Preservative/ Treatment Requested Analysis 11 3 4 degrees C VOA, Appendix 9 Acidified Method 8260 2 mL HCL 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314 0 2 010 Spring GW Sampling ATK Launch Systems, Inc Promontory, UTAH (801) 251-5688 SAMPLE NUMBER E^-^ DATE ^ ^d([0 SAMPLER 1006009 ANALYTICAL LABORATORY ATK Environmental Laboratory MS3 Bottle Number No of Containers Fid Preservative/ Treatment Requested Analysis 11 3 4 degrees C Acidified 2 mL HCL VOA, Appendix 9 Method 8260 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314 0 i 1 ENVIRONMENTAL LAB WORK REQUEST 1006010 ™ ATK ENVIRONMENTAL LABORATORY LWR No Logm No E13167 FROM EXTENSION COST CENTER WORK ORBER DATE ORO/IMZATIOV MAIL STOP REPORT RESULTS TO HELEN RAVSTEN, MS 301 SAMPLE INFORMATION SAMPLE DATE TYPE LOCATION TIME TEST REMARKS SAMPLE DATE G C LOCATION TIME TEST REMARKS • D-f See, ^'^cUt^ ai*>L-fi£^ l^aices. ^ ^-10 . J 11 ft (( \zso a (c * 6-2-IHOO (( a (I u ^( .1 r( IHIO n „ r( -J (( a (X (( f< (( 9 10 11 12 CHAIN OF CUSTODY DATE TIME RECEIVED BY DATE TIME i I FOR LABORATORY USE ONLY DATE COMPLETED DATE REPORTED 988P ^S333 GW CERTIFICATE OF ANALYSIS Listing of Sample Information and Testing Requested Wednesday, June 16 2010 TESTED FOR ATK DLV Environmental Monitonng Thiokol Corp, UT 84322 ANALYZED BY ATK Launch Systems Analytical Chemistry Laboratory P O Box 707, M/S 245 Bngham City, UT 84302-0707 435-863-3732 435-863-8080 Contact Name Project Sample Delivery Group Al Lee Ground Water Testing - DLV 1006010 Page 1 of 18 Pnnted 06/16/10 125 Sample Delivery Group 1006010 Sample No Client No Received Collect Date/Time Test Requested Sample Description Matrix 1006010 01 D1 06/03/10 6/3/2010 11 00 00 EPA 120 1 EPA 314 0 SW846 8260B (Water) Conductivity Perctilorate Ion Chrorratography Volatile Organic Analysis Water Water Water 1006010 02 BIO 06/03/10 6/3/2010 11 55 00 EPA 120 1 EPA 314 0 SW846 8260B (Water) Conductivity Perctilorate Ion Chromatography Volatile Organic Analysis Water Water Water '1006010 03 B2D 06/03/10 6/3/2010 12 50 00 | 1 EPA 120 1 EPA 314 0 SW 846 8260B (Water) Conductivity Perchlorate Ion Chromatography Volatile Organic Analysis Water Water Water ,1006010 04 G2 06/03/10 6/3/2010 14 00 00 | i EPA 120 1 EPA 314 0 SW846 8260B (Water) Conductivity Perchlorate Ion Chromatography Volatile Organic Analysis Water Water Water '1006010 05 G2A 06/03/10 6/3/2010 14 05 00 i EPA 120 1 EPA 314 0 SW846 8260B (Water) Conductivity Perchlorate Ion Chromatography Volatile Organic Analysis Water Water Water 1006010 06 TP 001 06/03/10 6/3/2010 14 10 00 1 EPA 120 1 EPA 314 0 SW846 8260B (Water) Conductivity Perchlorate Ion Chromatography Volatile Organic Analysis Water Water Water 'l 006010 07 FP001 06/03/10 6/3/2010 14 15 00 EPA 120 1 EPA 314 0 SW 846 8260B (Water) Conductivity Perchlorate Ion Chromatography Volatile Organic Analysis Water Water Water '1006010 08 B6 06/03/10 6/3/2010 14 45 00 ' EPA 120 1 EPA 314 0 Conductivity Perchlorate Ion Chromatography Water Water Page 2 of 18 Pnnted 06/16/10 1125 Sample Delivery Group 1006010 Sample No Client No Test Requested 1006010 08 B6 Sample Description Received Collect Date/Time Matrix 06/03/10 6/3/2010 14 45 00 SW 846 8260B (Water) Volatile Organic Analysis Water Certified By W Scott Fraser Quality Assurance Officer 06/17/2010 Date This certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation Program (NELAP) unless otherwise annotated Page 3 of 18 Pnnted 06/16/10 11 25 Listing of Results by Sample Sample Delivery Group 1006010 Ghent Sample ID D 1 Sample Description ATK DLV Groundv\/ater Spnng 2010 Laboratory Sample ID Date Sampled 1006010 01 06/03/10 11 00 AS Number Test Parameter Result Units MDL EQL Dilution Factor Analvst Test Date Tesf Method EPA 1201 Co djctivly CONDUCTIVITY 2010 uS/cn C 3 1 1 JMM 06/14/10 Test Method EPA 314 0 Percnio ate lor Cnroma ography 014797 73 0 PERCHLORATE 551 jg/L 10 40 10 JMM 06/15/10 Test Method SIV 846 8260S (Water) Vola ile Organic Analys s 67 64 1 ACETONE U ug/L 5 10 1 QC 06/08/1 0 71 43 2 BENZENE 3 6 J ug/L 0 22 10 1 QC 06/08/10 74 97 5 BROMOCHLOROMETHANE U ug/L 0 31 10 1 QC 06/08/10 75 27-4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 06/08/10 108 86 1 BROMOBENZENE U ug/L 0 37 10 1 QC 06/08/10 75 25 2 BROMOFORM U ug/L 0 42 10 1 QC 06/08/10 74 83 9 BROMOMETHANE U ug/L 0 57 10 1 QC 06/08/10 78 93 3 2 BUTANONE U ug/L 1 11 10 1 QC 06/08/1 0 104 51 8 N BUTYLBENZENE U ug/L 0 3 10 1 QC 06/08/1 0 135 98 8 SEC BUTYLBENZENE u ug/L 04 10 1 QC 06/08/10 98 06 6 TERT BUTYLBENZENE U ug/L 0 4 10 1 QC 06/08/10 75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 06/08/10 56 23 5 CARBON TETRACHLORIDE 7 J ug/L 0 27 10 1 QC 06/08/10 108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 QC 06/08/10 75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 06/08/10 110 75 8 2 CHLOROETHYLVINYL ETHER u ug/L 1 71 10 1 QC 06/08/10 67 66 3 CHLOROFORM 27 3 ug/L 0 3 10 1 QC 06/08/10 74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 06/08/10 95-49 8 2 CHLOROTOLUENE U ug/L 0 24 10 1 QC 06/08/10 106-43 4 4 CHLOROTOLUENE U ug/L 0 15 10 1 QC 06/08/10 124-48 1 DIBROMOCHLOROMETHANE U ug/L 0 18 10 1 QC 06/08/10 96 12 8 1 2 DIBROMO 3 CHLOROPROPANE U ug/L 0 35 10 1 QC 06/08/10 74 95 3 DIBROMOMETHANE U ug/L 0 25 10 1 QC 06/08/10 106 93-4 1 2 DIBROMOETHANE U ug/L 0 15 10 1 QC 06/08/10 95 50 1 1 2 DlCHLOROBENZENE U ug/L 5 86 10 1 QC 06/08/10 541 73 1 1 3 DlCHLOROBENZENE U ug/L 5 62 10 1 QC 06/08/10 106-46 7 1 4 DlCHLOROBENZENE U ug/L 5 88 10 1 QC 06/08/10 75 71 8 DICHLORODIFLUOROMETHANE U ug/L 0 66 10 1 QC 06/08/10 75 34 3 1 1 DICHLOROETHANE 18 9 ug/L 0 49 10 1 QC 06/08/10 107 06 2 1 2 DICHLOROETHANE U ug/L 0 29 10 1 QC 06/08/10 75 35 4 1 1 DICHLOROETHENE 787 ug/L 0 16 10 1 QC 06/08/10 155 59 4 CIS 1 2 DICHLOROETHENE U ug/L 0 16 10 1 QC 06/08/10 156 60 5 TRANS 1 2 DICHLOROETHENE 0 3 J ug/L 0 34 10 1 QC 06/08/10 78 87 5 1 2 DICHLOROPROPANE U ug/L 0 16 10 1 QC 06/08/10 142 28 9 1 3 DICHLOROPROPANE U ug/L 0 24 10 1 QC 06/08/10 563 58 6 1 1 DICHLOROPROPENE U ug/L 0 17 10 1 QC 06/08/10 10061 01 5 CIS 1 3 DICHLOROPROPENE U ug/L 04 10 1 QC 06/08/10 10061 02 6 TRANS 1 3 DICHLOROPROPENE U ug/L 04 10 1 QC 06/08/10 590 20 7 2 2 DICHLOROPROPANE U ug/L 0 9 Q 1 QC 06/08/10 100-41 4 ETHYLBENZENE U ug/L 0 16 10 1 QC 06/08/10 591 78 6 2"EXANONE U ug/L 0 7 10 1 QC 06/08/10 87 68 3 rEXACHLOROBUTAD ENE L ug/L 0 9 10 QC 06/08/10 98 82 8 ISOPROPYLBENZENE L ug/L 0 58 10 QC 05/08/10 99 87 6 4 ISOPRCPV^TCLLESE U ug/-0 24 10 QC 05/08/10 75 09 2 VE"hV ENE C-JLOR'DE U jg L C 8 10 1 QC 05/08/, C Page 4 of 18 Pnnted 06/16/10 11 25 Listing of Results by Sample Sample Delivery Group 1006010 Client Sample ID D 1 Laboratory Sample ID 1006010 01 Sample Description ATK DLV Groundwater Spring 2010 Date Sampled 06/03/10 11 00 CAS Number Test Parameter Result Units MDL Dilution Factor Analyst Test Date Tesf Method SIV 846 82606 (Water) Volat 'e Organic Analysis 108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 05/08/10 91 20 3 NAPHTHALENE u ug/L 4 10 1 QC 06/08/10 103 65 \ PROPYLBENZENE u ug/L 0 5 10 1 QC 05/08/lO 100 42 5 STYRENE J ug/L 0 3 10 1 QC 06/08/10 630 20 6 1112 TETRACHLOROETHANE u ug/L 0 25 10 1 QC 06/08/10 79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 06/08/10 127 18 4 TETRACHLOROETHENE 6 9 J ug/L 04 10 1 QC 06/08/10 108 88 3 TOLUENE u ug/L 0 5 10 1 QC 05/08/10 87 61 5 1 2 3 TRICHLOROBENZENE u ug/L 0 23 10 1 QC 06/08/10 120 82 1 1 2 4 TRICHLOROBENZENE u ug/L 4 37 10 1 QC 06/08/10 71 55 6 1 1 TRICHLOROETHANE 1400 J ug/L 32 2000 200 QC 06/08/10 79 00 5 1 1 2 TRICHLOROETHANE U ug/L 0 25 10 1 QC 06/08/10 79 01 6 TRICHLOROETHENE 9850 ug/L 140 2000 200 QC 06/08/10 7S 69^ TRICHLOROFLUOROMETHANE U ug/L 0 3 10 1 QC 06/08/10 96 18-4 1 2 3 TRICHLOROPROPANE U ug/L 0 33 10 1 QC 06/08/10 9S 63 6 1 2 4 TRIMETHYLBENZENE U ug/L 0 19 10 1 QC 06/08/10 106 67 8 1 3 5 TRIMETHYLBENZENE U ug/L 0 29 10 1 QC 06/08/10 108 05 4 VINYL ACETATE U ug/L 20 50 1 QC 06/08/10 75 01-4 VINYL CHLORIDE U ug/L 0 3 10 1 QC 06/08/10 1330 20 7 m p XYLENE U ug/L 0 6 10 1 QC 06/08/10 9S-47 6 0 XYLENE U ug/L 0 3 10 1 QC 06/08/10 460 00 4 BROMOFLUOROBENZENE 95 6 / 1 QC 06/08/10 1868 53 7 DIBROMOFLUOROMETHANE 103 / 1 QC 06/08/10 17060 07 0 1 2 DICHLOROETHANE D4 108 "/ 1 QC 06/08/10 2037 26 5 TOLUENE D8 98 % QC 06/08/10 Client Sample ID B 10 Laboratory Sample ID 1006010 02 Sample Description ATK DLV Groundwater Spnng 2010 Date Sampled 06/03/10 11 55 CAS Number Test Parameter Result Units MDL EQL Dilution Factor Analvst Test Date TesfMef/iod EPA 120 1 Conductivity CONDUCTIVITY 1000 uS/cm 0 3 1 1 JMM 06/14/10 TestMethod EPA3140 Perchlorate Ion Chromatography 014797 73 0 PERCHLORATE 4040 ug/L 50 200 50 JMM 06/15/10 Tesf Method SW 846 8260B (Water) Volatile Organic Analysis 67 64 1 ACETONE U ug/L 5 10 1 QC 06/08/10 71 43 2 BENZENE 02 J ug/L 0 22 10 1 QC 06/08/10 74 97 5 BROMOCHLOROMETHANE u ug/L 0 31 10 1 QC 06/08/10 75 27-4 BROMODICHLOROMETHANE u ug/L 0 19 10 1 QC 06/08/10 108 86 1 BROMOBENZENE u ug/L 0 37 10 QC 06/08/10 75 25 2 BROMOFORM u ug/L 0 42 10 1 QC 05/08/10 74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 06/08/lO 78 93 3 2 BUTANONE J ug/L 1 11 10 1 QC 05/08/10 104 51 8 N BUTYLBENZENE u ug/L 0 3 c QC 06/08 10 135 98 8 SEC BUTYLBENZENE u ug/L 0 4 10 1 QC 06/08 10 98 05 5 TERT BUTYLBENZENE J ug L 0 4 10 1 QC 06/08/10 75 15 0 CARBON DISULFIDE u ug' 0 13 10 1 QC 06/08/iC Page 5 of 18 Pnnted 06/16/10 11 25 Listing of Results by Sample Sample Delivery Group 1006010 Ghent Sample ID BIO Sample Descnption ATK DLV Groundwater Spring 2010 Laboratory Sample ID Date Sampled 1006010 02 06/03/10 11 55 CAS Number Tesf Method Test Parameter SW846 8260B (Water) Result Units Volat leOrga ic Analyses MDL Dilution EQL Factor Analvst Test Date 55 23 5 CARBON TETRACH' ORIDE U ug/L 0 27 0 1 QC 06/08/10 108 90 7 CHLOROBENZENE U ug/L 0 16 10 1 QC 06/08/10 75 00 3 CHLOROETHANE U jg/L 0 35 10 1 QC 06/08/10 110 75 8 2 CHLOROETHYLVINYL ETHER U ug/L 1 71 10 1 QC 06/08/10 67 66 3 CHLOROFORM J ug/L 0 3 10 1 QC 06/08/10 74 87 3 CHLOROMETHANE J ug/L 0 81 10 1 QC 06/08/10 95^9 8 2 CHLOROTOLUENE u ug/L 0 24 10 1 QC 06/08/10 105-43 4 4 CHLOROTOLUENE u ug/L 0 15 10 1 QC 06/08/10 124 48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 06/08/10 96 12 8 1 2 DIBROMO 3 CHLOROPROPANE u ug/L 0 35 10 1 QC 06/08/10 74 95 3 DIBROMOMETHANE u ug/L 0 25 10 1 QC 06/08/1 0 106 93 4 1 2 DIBROMOETHANE u ug/L 0 15 10 1 QC 06/08/10 95 50 1 1 2 DlCHLOROBENZENE u ug/L 5 85 10 1 QC 06/08/10 541 73 1 1 3 DlCHLOROBENZENE u ug/L 5 62 10 1 QC 05/08/10 106-46 7 1 4 DlCHLOROBENZENE u ug/L 5 88 10 1 QC 06/08/10 75 71 8 DICHLORODIFLUOROMETHANE u ug/L 0 56 10 1 QC 06/08/10 75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 06/08/10 107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 06/08/10 75 35-4 1 1 DICHLOROETHENE 2 1 J ug/L 0 16 10 1 QC 06/08/10 156 59 4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 06/08/10 156 60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 lO 1 QC 05/08/10 78 87 5 1 2 DICHLOROPROPANE u ug/L 0 15 10 1 QC 06/08/10 142 28 9 1 3 DICHLOROPROPANE u ug/L 0 24 10 1 QC 06/08/10 563 58 6 1 1 DICHLOROPROPENE u ug/L 0 17 10 1 QC 06/08/10 10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 06/08/10 10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 0 4 10 1 QC 06/08/10 590 20 7 2 2 DICHLOROPROPANE u ug/L 09 10 1 QC 06/08/10 100-41 4 ETHYLBENZENE u ug/L 0 16 10 1 QC 06/08/10 591 78 6 2 HEXANONE u ug/L 07 10 1 QC 06/08/10 87 68 3 HEXACHLOROBUTADIENE u ug/L 0 9 10 1 QC 06/08/10 98 82 8 ISOPROPYLBENZENE u ug/L 0 58 10 1 QC 06/08/10 99 87-6 4 ISOPROPYLTOLUENE u ug/L 0 24 10 1 QC 06/08/10 75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 06/08/10 108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 06/08/10 91 20 3 NAPHTHALENE u ug/L 4 10 1 QC 06/08/10 103 65 1 N PROPYLBENZENE u ug/L 0 5 10 1 QC 05/08/10 100-42 5 STYRENE u ug/L 0 3 10 1 QC 06/08/10 630 20 6 1112 TETRACHLOROETHANE u ug/L 0 25 10 1 QC 06/08/10 79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 05/08/10 127 18 4 TETRACHLOROETHENE u ug/L 04 10 1 QC 06/08/10 108 88 3 TOLUENE u ug/L 0 5 10 1 QC 05/08/10 87 61 6 1 2 3 TRICHLOROBENZENE u ug/L 0 23 0 1 QC 06/08/10 120 82 1 1 2 4 -TRICHLOROBENZENE u ug/L 4 37 10 1 QC 05/08/10 71 55 6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 06/08/10 79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 06/08/10 79 01 6 'RICHLOROETHENE 40 2 ug/L 07 10 1 QC 05/08/10 75 69 4 TRICHLOROFLUOROMETHANE u g/L 0 3 10 QC 06/08/10 96 ,8 4 1 2 3 ""R CHLOROPROPANE J ug/L ^ 33 QC 06/08/10 95 63 6 2 4 TRiME~HYL3ENZENE u ug/L 0 19 0 GC 05/08/ 0 08 67 8 i 3 5 "TRIMET-'Y^BENZENE u ug/L 0 29 10 1 QC 05/08/10 Page 6 of 18 Pnnted 06/16/10 11 25 Listing of Results by Sample Sample Delivery Group 1006010 Ghent Sample ID B 10 Sample Description ATK DLV Groundwa er Spnng 2010 Laboratory Sample ID Date Sampled 1006010 02 06/03/10 ' 1 55 GAS Number Test Parameter Result Units MDL EQL Dilution Factor Analvst Test Date Tesf Method SIV 846 82606 (Water) Voiat e 0 gan c Analysis 108 06 4 VINYL ACETATE L ug/L 20 50 -1 QC 05/08/10 75 01 4 VINYL CHLORIDE U ug/L 0 3 10 1 QC 06/08/ 0 1330 20 7 m p XYLENE U ug/L 0 5 10 1 QC 05/08/10 95-47 6 0 XYLENE u ug/L 0 3 10 1 QC C6/08/10 460 00 4 BROMOFLUOROBENZENE 93 8 / 1 QC 06/08/10 1868 53 7 DIBROMOFLUOROMETHANE 106 / 1 QC 06/08/10 17060 07 0 2 DICHLOROETHANE D4 110 / 1 QC 05/08/10 2037 26 5 TOLUENE 08 96 5 / QC 06/08/10 Ghent Sample ID B 2D Laboratory Sample ID 1006010 03 Sample Description ATK DLV Groundwater Spnng 2010 Date Sampled 06/03/10 12 50 CAS Number Test Parameter Result Units MDL EQL Dilution Factor Analvst Test Date Tesf Method EPA 120 1 Conductivity CONDUCTIVITY 1520 uS/cm 0 3 1 1 JMM 06/14/10 Test Method EPA3140 Perchlorate Ion Chromatography 014797 73 0 PERCHLORATE 25600 ug/L 100 400 100 JMM 06/15/10 Tesf Method SIV 846 8260B (Water) Volatile Organic Analysis 57-64 1 ACETONE U ug/L 5 10 1 QC 06/08/10 71-43 2 BENZENE 1 1 J ug/L 0 22 10 1 QC 06/08/10 74 97 5 BROMOCHLOROMETHANE U ug/L 0 31 10 1 QC 06/08/10 75 27-4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 05/08/10 108 86 1 BROMOBENZENE U ug/L 0 37 10 1 QC 06/08/10 75 25 2 BROMOFORM U ug/L 0 42 10 1 QC 06/08/10 74 83 9 BROMOMETHANE U ug/L 0 57 10 1 QC 06/08/10 78 93 3 2 BUTANONE U ug/L 1 11 10 1 QC 06/08/10 104 51 8 N BUTYLBENZENE U ug/L 0 3 10 1 QC 06/08/10 135 98 8 SEC BUTYLBENZENE U ug/L 04 10 1 QC 05/08/10 98 06 6 TERT BUTYLBENZENE U ug/L 04 10 1 QC 06/08/10 75 15 0 CARBON DISULFIDE U ug/L 0 13 10 1 QC 05/08/10 56 23 5 CARBON TETRACHLORIDE 4 5 J ug/L 0 27 10 1 QC 06/08/10 108 90 7 CHLOROBENZENE 0 7 J ug/L 0 16 10 1 QC 06/08/10 75 00 3 CHLOROETHANE U ug/L 0 35 10 1 QC 06/08/10 110 75 8 2 CHLOROETHYLVINYL ETHER U ug/L 1 71 .0 1 QC 06/08/10 57-65 3 CHLOROFORM 89 8 ug/L 0 3 10 1 QC 05/08/10 74 87 3 CHLOROMETHANE U ug/L 0 81 10 1 QC 06/08/10 95 49 8 2 CHLOROTOLUENE U ug/L 0 24 10 1 QC 06/08/10 105-43 4 4 CHLOROTOLUENE U ug/L 0 15 10 1 QC 05/08/10 124-48 DIBROMOCHLOROMETHANE U ug/L 0 18 10 1 QC 06/08/10 96 12 8 1 2 DIBROMO 3 CHLOROPROPANE U ug/L 0 35 10 1 QC 05/08/10 74 95 3 DIBROMOMETHANE U ug/-0 25 10 1 QC 06/08/10 106 93 4 1 2 DIBROMOETHANE U ug/L 0 15 10 1 QC 06/08/10 95 50 1 2 DlCHLOROBENZENE b ug'L 5 86 10 1 QC 05/08/10 541 73 3 DlCHLOROBENZENE U ug/L 5 62 lO 1 QC 06/08/10 -05 45 7 4 DlCHLOROBENZENE J ug L 5 88 10 QC 06/08/10 75 71 8 DICHLORODi'LJOROMETHANE J g/L 0 56 10 QC 06 08 -0 75 34 3 1 1 D CHLOROETHANE 38 9 ug/. 0 49 10 1 QC 06/38/ 0 Page 7 of 18 Pnnted 06/16/10 1125 Listing of Results by Sample Sample Delivery Group 1006010 Ghent Sample ID B 2D Sample Description ATK DLV G'-ouidwater Spring 20 rO Laboratory Sample ID Date Sampled 1006010 03 06/03/10 12 50 CAS Number Test Parameter Result Units MDL EQL Dilution Factor Analvst Test Date Tesf Method SIV 846 82606 (Water) Volatile Organic Analys s 107 06 2 1 2 DICHLOROETHANE 8 J ug/L 0 29 10 QC 06/08/10 75 35 4 1 1 0'CHLOROE~-iENE 444 ug/L 3 2 200 20 GC 06/08/10 155 59 4 CIS 1 2 DICHLOROE'^HENE 20 9 ug/L 0 15 10 1 QC 06/08/10 156 50 5 TRANS 1 2 DICHLOROETHENE U jg/L 0 34 10 1 QC 06/08/10 78 87 5 1 2 DICHLOROPROPANE u ug/L 0 15 0 QC 06/08/1 0 142 28 9 1 3 DICHLOROPROPANE u ug/-0 24 10 1 QC 06/08/10 563 58 6 1 DICHLOROPROPENE u ug/L 0 17 10 1 QC 06/08/10 10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 06/08/10 10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 06/08/10 590 20 7 2 2 DICHLOROPROPANE u ug/L 0 9 10 1 QC 06/08/10 100 41 4 ETHYLBENZENE u ug/L 0 15 10 1 QC 05/08/10 591 78 6 2 HEXANONE u ug/L 07 10 1 QC 05/08/10 87 58 3 HEXACHLOROBUTADIENE u ug/L 0 9 10 1 QC 06/08/10 98 82 8 ISOPROPYLBENZENE u ug/L 0 58 10 1 QC 06/08/10 99 87 6 4 ISOPROPYLTOLUENE u ug/L 0 24 10 1 QC 06/08/10 75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 06/08/10 108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 06/08/10 91 20 3 NAPHTHALENE u ug/L 4 10 1 QC 06/08/10 103 55 1 N PROPYLBENZENE u ug/L 0 5 10 1 QC 06/08/10 100 42 5 STYRENE u ug/L 0 3 10 1 QC 05/08/10 530 20 6 1112 TETRACHLOROETHANE u ug/L 0 25 10 1 QC 06/08/10 79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 06/08/10 127 18 4 TETRACHLOROETHENE 22J ug/L 04 10 1 QC 05/08/10 108 88 3 TOLUENE U ug/L 0 5 10 1 QC 06/08/10 87 51 6 1 2 3 TRICHLOROBENZENE u ug/L 0 23 10 1 QC 06/08/10 120 82 1 1 2 4 TRICHLOROBENZENE u ug/L 4 37 10 1 QC 05/08/10 71 55 6 1 1 1 TRICHLOROETHANE 621 ug/L 3 2 200 QC 06/08/10 79 00 5 1 1 2 TRICHLOROETHANE 32J ug/L 0 25 10 1 QC 06/08/10 79 01 6 TRICHLOROETHENE 3190 ug/L 14 200 20 QC 05/08/10 75 59-4 TRICHLOROFLUOROMETHANE U ug/L 0 3 10 1 QC 06/08/10 96 18-4 1 2 3 TRICHLOROPROPANE U ug/L 0 33 10 1 QC 06/08/10 95-63 6 1 2 4 TRIMETHYLBENZENE U ug/L 0 19 10 1 QC 05/08/10 108 67 8 1 3 5 TRIMETHYLBENZENE U ug/L 0 29 10 1 QC 06/08/10 108 05 4 VINYL ACETATE U ug/L 20 50 1 QC 06/08/10 75 01-1 VINYL CHLORIDE U ug/L 03 10 1 QC 05/08/10 1330 20 7 m p XYLENE U ug/L 06 10 1 QC 06/08/10 95-47 6 0 XYLENE U ug/L 0 3 10 1 QC 05/08/10 460 00 4 BROMOFLUOROBENZENE 93 6 V 1 QC 05/08/10 1868 53 7 DIBROMOFLUOROMETHANE 105 / 1 QC 06/08/10 17060 07 0 1 2 DICHLOROETHANE D4 108 / 1 QC 05/08/10 2037 26 5 TOLUENE D8 97 3 V QC 06/08/10 Ghent Sample ID G2 Laboratory Sample ID 1006010 04 Sample Description ATK DLV Groundwater Spnng 2010 Date Sampled 06/03/10 14 00 GAS Number Test Parameter Result Units MDL EQL Dilution Factor Analvst Test Date Tesf Method EPA 1201 Condoctivty CONDUCTIVITY 7780 S c-^ 0 3 1 MV 05/14/10 Page 8 of 18 Pnnted 06/16/10 1125 Listing of Results by Sample Sample Delivery Group 1006010 Ghent Sample ID G2 Sample Description ATK DLV Groundwater Spnng 2010 Laboratory Sample ID 1006010 04 Date Sam pled 06/03/10 14 00 Dilution AS Number Test Parameter Result Units MDL EQL Factor Analvst Test Date Tesf Method EPA 314 0 i^erchloate Ion Chror-a ograohy 014797 73 0 PERCHLORA'^E 52100 ug/L 250 lOOO 250 JMM 06/15/10 TestMethod SW 846 82606 (Water) Volatile Org: nic Analysis 57 64 1 ACETONE U ug/L 5 0 1 QC 06/08/10 71 43 2 BENZENE 05J ug/L 0 22 10 1 QC 06/08/10 74 97 5 BROMOCHLOROMETHANE J ug/L 0 31 10 1 QC 06/08/10 75 27-4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 06/08/10 108 86 1 BROMOBENZENE U ug/L 0 37 10 1 QC 06/08/10 75 25 2 BROMOFORM U ug/L 0 42 10 1 QC 06/08/10 74 83 9 BROMOMETHANE u ug/L 0 57 10 1 QC 06/08/10 78 93 3 2 BUTANONE u ug/L 1 11 10 1 QC 06/08/10 104 51 8 N BUTYLBENZENE L ug/L 0 3 10 1 QC 06/08/10 135 98 8 SEC BUTYLBENZENE U ug/L 04 10 1 QC 06/08/10 98 06 6 TERT BUTYLBENZENE U ug/L 04 10 1 QC 06/08/10 75 15 0 CARBON DISULFIDE U ug/L 0 13 10 1 QC 05/08/10 56 23 5 CARBON TETRACHLORIDE 1 3 J ug/L 0 27 10 1 QC 06/08/10 108 90 7 CHLOROBENZENE U ug/L 0 16 10 QC 06/08/10 75 00 3 CHLOROETHANE U ug/L 0 35 10 1 QC 06/08/10 110 75 8 2 CHLOROETHYLVINYL ETHER U ug/L 1 71 10 1 QC 06/08/10 67 66 3 CHLOROFORM 32 ug/L 03 10 1 QC 06/08/10 74 87 3 CHLOROMETHANE U ug/L 0 81 10 1 QC 06/08/10 95 49 8 2 CHLOROTOLUENE U ug/L 0 24 10 1 QC 06/08/10 106-43 4 4 CHLOROTOLUENE U ug/L 0 15 10 1 QC 06/08/10 124-48 1 DIBROMOCHLOROMETHANE U ug/L 0 18 10 1 QC 06/08/10 96 12 8 1 2 DIBROMO-3 CHLOROPROPANE U ug/L 0 35 10 1 QC 06/08/10 74 95 3 DIBROMOMETHANE U ug/L 0 25 10 1 QC 06/08/10 106 93 4 1 2 DIBROMOETHANE U ug/L 0 15 10 1 QC 06/08/10 95 50 1 1 2 DlCHLOROBENZENE U ug/L 5 86 10 1 QC 06/08/10 541 73 1 1 3 DlCHLOROBENZENE u ug/L 5 62 10 1 QC 06/08/10 106-46 7 1 4 DlCHLOROBENZENE u ug/L 5 88 10 1 QC 06/08/10 76 71 8 DICHLORODIFLUOROMETHANE u ug/L 0 56 10 1 QC 06/08/10 76 34 3 1 1 DICHLOROETHANE 12 8 ug/L 0 49 10 1 QC 06/08/10 107 06 2 1 2 DICHLOROETHANE 28J ug/L 0 29 10 1 QC 06/08/10 75 35^ 1 1 DICHLOROETHENE 270 ug/L 3 2 200 QC 05/08/10 156 59-4 CIS 1 2 DICHLOROETHENE 40 4 ug/L 0 16 10 1 QC 06/08/10 156-60 5 TRANS 1 2 DICHLOROETHENE U ug/L 0 34 10 1 QC 06/08/10 78 87 5 1 2 DICHLOROPROPANE U ug/L 0 16 10 1 QC 06/08/10 142 28 9 1 3 DICHLOROPROPANE U ug/L 0 24 10 1 QC 06/08/10 563 58 6 1 1 DICHLOROPROPENE U ug/L 0 17 10 1 QC 06/08/10 10061 01 5 CIS 1 3 DICHLOROPROPENE U ug/L 04 10 1 QC 06/08/10 10061 02 6 TRANS 1 3 DICHLOROPROPENE U ug/L 04 10 1 QC 06/08/10 590 20 7 2 2 DICHLOROPROPANE U ug/L 0 9 10 1 QC 06/08/10 100 41-4 ETHYLBENZENE u ug/L 0 16 10 1 QC 06/08/10 591 78 6 2 HEXANONE u ug/L 0 7 10 1 QC 05/08/10 87 68 3 HEXACHLOROBUTADIENE J jg/L 0 9 10 1 QC 06/08/10 98 82 8 ISOPROPYLBENZENE J ug/L 0 58 10 1 QC 06/08/10 99 87 6 4 ISOPROPYLTOLUENE ug/L C 24 lO QC 06/08/10 75 09 2 METHYLENE ChLOR DE u ug/L 0 8 10 1 QC 06/08/10 08 10 1 4 VETHYL 2 PENTANONE g L 0 53 10 1 QC 06/08/10 91 20 3 NAPr-ThA ENE L ug/ 4 10 QC 06/08/10 ,03 65 1 N PROPYLBENZENE L .g/' 0 5 10 1 QC 06/08/10 Page 9 of 18 Pnnted 06/16/10 11 25 Listing of Results by Sample Sample Delivery Group 1006010 Ghent Sample ID G2 Sample Description ATK DLV Groundwater Spring 2010 Laboratory Sample ID Date Sampled 1006010 04 06/03/10 14 00 GAS Number Tesf Method Test Parameter SIV 846 82606 flVaferj Result Vola 1 e Organic Analysis Units MDL Dilution EQL Factor Analvst Test Date 00 42 5 STYRENE U ug/L 0 3 QC 06/08/10 630 20 6 2 TETRACHLOROETHANE L ugL 0 25 0 1 QC 05/08/1 0 79 34 5 1 2 2 TETRACHLOROETHANE J ug/L 0 85 10 1 QC 06/08/1 0 127 18 4 TETRACHLOROETHENE U ug/L 0 4 10 1 QC 06/08/10 108 88 3 TOLUENE U ug/L 0 5 10 1 QC 06/08/10 87 51 5 2 3 TRICHLOROBENZENE u ug/L 0 23 10 1 QC 06/08/10 120 82 1 1 2 4 TRICHLOROBENZENE J ug/L 4 37 10 QC 05/08/10 71 55 6 1 1 TRICHLOROETHANE 170 J ug/L 3 2 200 20 QC 05/08/10 79 00 5 1 1 2 TRICHLOROETHANE 1 9 J ug/L 0 25 10 1 QC 06/08/10 79 01 6 TRICHLOROETHENE 2060 ug/L 14 200 20 QC 06/08/10 75-69 4 TRICHLOROFLUOROMETHANE U ug/L 0 3 10 1 QC 06/08/10 95 18 4 1 2 3 TRICHLOROPROPANE U ug/L 0 33 10 1 QC 06/08/10 95 63 6 1 2 4 TRIMETHYLBENZENE U ug/L 0 19 10 1 QC 06/08/10 108 57 8 1 3 5 TRIMETHYLBENZENE U ug/L 0 29 10 1 QC 06/08/10 108 05 4 VINYL ACETATE U ug/L 20 50 1 QC 06/08/10 75 01-4 VINYL CHLORIDE U ug/L 0 3 10 1 QC 05/08/10 1330 20 7 m p XYLENE U ug/L 0 6 10 1 QC 06/08/10 95-47 6 0 XYLENE U ug/L 0 3 10 1 QC 06/08/10 450 00 4 BROMOFLUOROBENZENE 93 9 / 1 QC 06/08/10 1868 53 7 DIBROMOFLUOROMETHANE 104 / 1 QC 06/08/10 17060 07 0 1 2 DICHLOROETHANE D4 108 / 1 QC 06/08/10 2037 25 5 TOLUENE D8 95 6 /o 1 QC 06/08/10 Ghent Sample ID G2A Sample Description ATK DLV Groundwater Spnng 2010 Laboratory Sample ID 1006010 05 Date Sampled 06/03/10 14 05 Dilution AS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TesfMef/iod EPA 120 1 Conductivity CONDUCTIVITY 7810 uS/cm 0 3 1 1 JMM 06/14/10 TesfMef/iod EPA 314 0 Perchlorate Ion Chromatography 014797 73 0 PERCHLORATE 51900 ug/L 250 1000 250 JMM 06/15/10 Tesf Method SIV 846 82606 (Water) Volatile Organic Analysis 67 54 1 ACETONE U ug/L 5 10 1 QC 06/08/10 71-43 2 BENZENE 0 5 J ug/L 0 22 10 1 QC 06/08/10 74 97 5 BROMOCHLOROMETHANE U ug/L 0 31 10 1 QC 06/08/10 75 27-4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 06/08/10 108 86 1 BROMOBENZENE J ug/L 0 37 10 1 QC 06/08/10 75 25 2 BROMQi^ORM U ug/L 0 42 10 1 QC 06/08/10 74 83 9 BROMOMETHANE U ug/L 0 57 10 QC 06/08/10 78 93 3 2 BU"rANONE U ug/L 1 11 10 1 QC 06/08/10 104 51 8 N BUTYLBENZENE U ug/L 0 3 10 1 QC 06/08/10 135 98 8 SEC BU"^YLBENZENE U g/L 0 4 10 1 QC 05/08/10 98 06 6 'ERT BUTYLBENZENE U ug/L 0 4 10 QC 06/08/10 75 15 0 CARBON D SUL- DE ug L 0 i3 0 QC 06/08/10 56 23 5 CARBON TETRACHLORIDE 1 3 J ug/-0 27 c 1 QC 05/08 10 108 90 7 CHLOROBENZENE U g/L 0 6 10 1 QC 05/08' 0 75 CO 3 CHLORGE'HANE L ug L 0 35 lO QC 06/08/ 0 Page 10 of 18 Pnnted 06/16/ 0 11 25 Listing of Results by Sample Sample Delivery Group 1006010 Client Sample ID G2A Sample Descnption ATK DLV Groundwater Spring 2010 Laboratory Sample ID 10060 0 05 Date Sampled 06/03/10 14 05 CAS Number Test Parameter Result Units MDL EQL Tesf Method SW 846 82606 (Water) Vola ile Organ c A-IE ysis 110 75 8 2 CHLOROE~HVLVINYL ETHER L g/L 1 71 0 67 65 3 CHLOROFORM 31 4 ug/L 0 3 ,0 74 87 3 CHLOROMETHANE U ug/L 0 81 10 95-49 8 2 CHLOROTOLUENE U ug/L 0 24 10 105-43 4 4 CHLOROTOLUENE U ug/L 0 15 10 124 48 1 D BROMOCHLOROMETHANE U ug/L 0 18 10 95 12 8 1 2 DIBROMO 3 CHLOROPROPANE U ug/L 0 35 10 74 95 3 DIBROMOMETHANE U ug/L 0 25 10 106 93 4 1 2 DIBROMOETHANE u ug/L 0 15 10 95 50 1 1 2 DlCHLOROBENZENE u ug/L 5 85 10 541 73 1 1 3 DlCHLOROBENZENE u ug/L 5 62 10 106 45 7 1 4 DlCHLOROBENZENE u ug/L 5 88 10 75 71 8 DICHLORODIFLUOROMETHANE u ug/L 0 66 10 75 34 3 1 1 DICHLOROETHANE 12 7 ug/L 0 49 10 107 06 2 1 2 DICHLOROETHANE 28 J ug/L 0 29 10 75 35-4 1 1 DICHLOROETHENE 264 ug/L 3 2 200 156 59 4 CIS 1 2 DICHLOROETHENE 40 6 ug/L 0 16 10 156 60 5 TRANS 1 2 DICHLOROETHENE U ug/L 0 34 10 78 87 S 1 2 DICHLOROPROPANE U ug/L 0 16 10 142 28 9 1 3 DICHLOROPROPANE U ug/L 0 24 10 563 58 6 1 1 DICHLOROPROPENE U ug/L 0 17 10 10061 01 5 CIS 1 3 DICHLOROPROPENE U ug/L 04 10 10061 02 6 TRANS 1 3 DICHLOROPROPENE U ug/L 04 10 590 20 7 2 2 DICHLOROPROPANE U ug/L 09 10 100-41 4 ETHYLBENZENE U ug/L 0 16 10 591 78 6 2 HEXANONE U ug/L 07 10 87-68 3 HEXACHLOROBUTADIENE U ug/L 09 10 98 82 8 ISOPROPYLBENZENE U ug/L 0 58 10 99 87 6 4 ISOPROPYLTOLUENE U ug/L 0 24 10 75 09 2 METHYLENE CHLORIDE U ug/L 08 10 108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 91 20 3 NAPHTHALENE u ug/L 4 10 103 65 1 N PROPYLBENZENE u ug/L 0 5 10 100-42 5 STYRENE u ug/L 03 10 630 20 6 1112 TETRACHLOROETHANE u ug/L 0 25 10 79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 127 18 4 TETRACHLOROETHENE 09 J ug/L 0 4 10 108 88 3 TOLUENE U ug/L 0 5 10 87 61-6 1 2 3 TRICHLOROBENZENE U ug/L 0 23 10 120 82 1 1 2 4 TRICHLOROBENZENE U ug/L 4 37 10 71 55 6 1 1 1 TRICHLOROETHANE 170 J ug/L 32 200 79 00 5 1 1 2 TRICHLOROETHANE 1 7 J ug/L 0 25 10 79 01 5 TRICHLOROETHENE 2230 ug/L 14 200 75 59 4 TRICHLOROFLUOROMETHANE U ug/L 0 3 10 96 18-4 2 3 TRICHLOROPROPANE U ug/L 0 33 0 95 63 5 2 4 TRIMETHYLBENZENE U ug/ 0 19 10 108 67 8 3 5 TRIMETHYLBENZENE U ug/L 0 29 10 08 05 4 ViNY ACETATE L ug/L 20 50 75 01 4 VNv CHLORIDE L g/' 0 3 0 330 20 7 m p XYLENE U 06 10 Dilution Factor Analvst Test Date 20 20 20 QC 05/08/10 QC 05/08/10 QC 06/06/ 0 QC 05/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/ 0 QC 06/08/1 0 QC 06/08/10 QC 06/08/1 0 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 05/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 05/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 06/08/10 QC 05/08/10 QC 06/08/10 QC 05/08/1 0 QC 05/08/ 0 QC 06/08/ 0 QC 06/08/ 0 QC 05/08/10 Page 11 of 18 Pnnted 06/16/10 11 25 Listing of Results by Sample Sample Delivery Group 1006010 Client Sample ID G2A Sample Description ATK DLV Groundwater Sonng 2010 Laboratory Sample ID 1006010 05 Date Sampled 06/03/10 14 05 GAS Number Tesf Method 95 47 6 460 00 4 1868 53 7 17050 07 0 2037 26 5 Test Parameter SW 846 82606 (Water) Result Voia'ile Organic Analysis 0 XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1 2 DICHLOROETHANE D4 TOLUENE D8 U 98 4 105 108 96 3 Units ug/L / / / /o MDL Dilution Factor Analvst Test Date 10 QC QC QC QC QC 05/08/10 06/08/10 06/08/10 05/08/10 06/08/10 Ghent Sample ID TP 001 Sample Description ATK DLV Groundwater Spnng 2010 Laboratory Sample ID 1006010 06 Date Sampled 06/03/10 14 10 CAS Number Test Parameter Result Units MDL EQL Dilution Factor Analvst Test Date Tesf Method EPA 120 1 Conductivity CONDUCTIVITY 4 04 uS/cm 0 3 1 1 JMM 05/14/10 Test Method EPA 314 0 Perchlorate Ion Chromatography 014797 73 0 PERCHLORATE U ug/L 1 4 1 JMM 06/15/10 Tesf Method SIV 846 82608 CIVafer; Volatile Organic Analysis 67 64 1 ACETONE U ug/L 5 10 1 QC 06/08/10 71-43 2 BENZENE U ug/L 0 22 10 1 QC 06/08/10 74 97 5 BROMOCHLOROMETHANE U ug/L 0 31 10 1 QC 06/08/10 75 27-4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 06/08/10 108 86 1 BROMOBENZENE U ug/L 0 37 10 1 QC 06/08/10 75 25 2 BROMOFORM U ug/L 0 42 10 1 QC 06/08/10 74 83 9 BROMOMETHANE U ug/L 0 57 10 1 QC 06/08/10 78 93 3 2 BUTANONE U ug/L 1 11 10 1 QC 06/08/10 104 51 8 N BUTYLBENZENE U ug/L 03 10 1 QC 05/08/10 135 98 8 SEC BUTYLBENZENE U ug/L 0 4 10 1 QC 05/08/10 98 06 6 TERT BUTYLBENZENE U ug/L 04 10 1 QC 06/08/10 75 15 0 CARBON DISULFIDE U ug/L 0 13 10 1 QC 06/08/10 56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 06/08/10 108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 QC 06/08/10 75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 06/08/10 110 75 8 2 CHLOROETHYLVINYL ETHER u ug/L 1 71 10 1 QC 06/08/10 67 66 3 CHLOROFORM u ug/L 0 3 10 1 QC 06/08/10 74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 06/08/10 95-49 8 2 CHLOROTOLUENE u ug/L 0 24 10 1 QC 06/08/10 106-43 4 4 CHLOROTOLUENE u ug/L 0 15 10 1 QC 06/08/10 124-48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 06/08/10 96 12 8 1 2 DIBROMO-3 CHLOROPROPANE u ug/L 0 35 10 1 QC 05/08/10 74 95 3 DIBROMOMETHANE u ug/L 0 25 10 1 QC 06/08/10 106 93 4 1 2 DIBROMOETHANE u ug/L 0 15 10 1 QC 06/08/10 95 50 1 1 2 DlCHLOROBENZENE u ug/L 5 86 10 1 QC 06/08/10 541 73 1 1 3 DlCHLOROBENZENE u ug/L 5 62 10 1 QC 06/08/10 106-46 7 4 DlCHLOROBENZENE J ug/L 5 88 10 1 QC 06/08/10 75 71 8 D CHLORODIFLUOROMETHANE u ug/L 0 56 10 1 QC 06/08/10 75 34 3 1 1 D CHLOROETHANE L ug/L 0 49 0 1 QC 06/08/10 107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 05/08/10 75 35 4 1 , DICHLOROETHENE J g/L 0 15 10 1 QC 06/08/10 156 59 4 ClS 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 06 08/10 Page 12 of 18 Pnnted 06/ 6/1O 11 25 Listing of Results by Sample Sample Delivery Group 1006010 Client Sample ID TP 001 Sample Description ATK DLV Groundwater Spring 2010 Laboratory Sample ID 1006010 06 Date Sampled 06/03/10 14 10 GAS Number Test Parameter Result Units MDL EQL Dilution Factor Analvst Test Date Tesf Method SIV 846 82606 flVafer^ Vola ile Organic Analysis 56 60 5 ""RANS 1 2 D-CHLOROETHENE u ug/L 0 34 0 1 QC 05/08/10 78 87 6 1 2 D CHLOROPROPANE u ug/L 0 16 10 QC 06/08/10 142 28 9 3 DICHLOROPROPANE u -g/L 0 24 10 1 QC 05/08/10 563 58 5 1 1 DICHLOROPROPENE u g'L 0 17 10 1 QC 06/08/10 0061 01 5 CIS 1 3 DICHLOROPROPENE u ug'L 0 4 10 1 QC 06/08/10 10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 05/08/10 590 20 7 2 2 DICHLOROPROPANE u ug/L 0 9 10 1 QC 06/08/10 100-41 4 ETHYLBENZENE u ug/L 0 16 10 1 QC 06/08/10 591 78 6 2 HEXANONE u ug/L 07 10 1 QC 06/08/10 87 68 3 HEXACHLOROBUTADIENE u ug/L 0 9 10 1 QC 06/08/10 98 82 8 ISOPROPYLBENZENE u ug/L 0 58 10 1 QC 06/08/10 99 87 5 4 ISOPROPYLTOLUENE u ug/L 0 24 10 1 QC 05/08/10 75 09 2 METHYLENE CHLORIDE u ug/L 0 8 10 1 QC 06/08/10 108 10 1 4 METHYL 2 PENTANONE u ug/L 0 53 10 1 QC 06/08/10 91 20 3 NAPHTHALENE u ug/L 4 10 1 QC 06/08/10 103 55 1 N PROPYLBENZENE u ug/L 0 5 10 1 QC 06/08/10 100 42 5 STYRENE u ug/L 0 3 10 1 QC 06/08/10 630 20 6 1112 TETRACHLOROETHANE u ug/L 0 25 10 1 QC 06/08/10 79 34 5 112 2 TETRACHLOROETHANE u ug/L 0 85 10 1 QC 06/08/10 127 18 4 TETRACHLOROETHENE u ug/L 0 4 10 1 QC 06/08/10 108 88 3 TOLUENE u ug/L 0 5 10 1 QC 06/08/10 87 61 5 1 2 3 TRICHLOROBENZENE u ug/L 0 23 10 1 QC 06/08/10 120 82 1 1 2 4 TRICHLOROBENZENE u ug/L 4 37 10 1 QC 06/08/10 71 55-6 1 1 1 TRICHLOROETHANE u ug/L 0 16 10 1 QC 06/08/10 79 00 5 1 1 2 TRICHLOROETHANE u ug/L 0 25 10 1 QC 06/08/10 79 01 6 TRICHLOROETHENE 15 ug/L 07 10 1 QC 06/08/10 75 69-4 TRICHLOROFLUOROMETHANE u ug/L 0 3 10 1 QC 06/08/10 96 18-4 1 2 3 TRICHLOROPROPANE u ug/L 0 33 10 1 QC 06/08/10 95 63 6 1 2 4 TRIMETHYLBENZENE u ug/L 0 19 10 1 QC 06/08/10 108 67 8 1 3 5 TRIMETHYLBENZENE u ug/L 0 29 10 1 QC 06/08/10 108 05 4 VINYL ACETATE u ug/L 20 50 1 QC 06/08/10 75 01-4 VINYL CHLORIDE u ug/L 0 3 10 1 QC 06/08/10 1330 20 7 mp XYLENE u ug/L 06 10 1 QC 06/08/10 95-47-6 0 XYLENE u ug/L 0 3 10 1 QC 06/08/10 460 00 4 BROMOFLUOROBENZENE 92 9 / 1 QC 06/08/10 1868 53 7 DIBROMOFLUOROMETHANE 101 /o 1 QC 06/08/10 17060 07 0 1 2 DICHLOROETHANE D4 108 /o 1 QC 06/08/10 2037 26 5 TOLUENE D8 96 3 / 1 QC 06/08/10 Ghent Sample ID FP 001 Laboratory Sample ID 1006010 07 Sample Description ATK DLV Groundwater Spring 2010 Date Sampled 06/03/10 14 15 CAS Number Test Parameter Result Units MDL EQL Dilution Factor Analvst Test Date Tesf Method EPA 120 1 Conductivity CONDUCTIvrv 4 54 uS cn" 0 3 1 JVV 05/ 4/i0 Test Method EPA 314 0 Pe ch orate lo" Crroratograo'' y 0 4797 73 0 PERCHLORATE J ug'L 4 .,5/15/'C Page 13 of 18 United 06/16/10 1125 Listing of Results by Sample Sample Delivery Group 1006010 Ghent Sample ID FP 001 Sample Description ATK DLV Groundwater Spnng 2010 Laboratory Sample ID 1006010 07 Date Sampled 06/03/10 14 15 GAS Number Tesf Method Test Parameter SIV 846 82606 (Water) Result Units Volatile Organic Analysis MDL Dilution EQL Factor Analvst Test Date 67 64 1 ACETONE U ug/L 5 10 1 QC 06/08/10 71 43 2 BENZENE U ug/L 0 22 10 1 QC 05/08/ 0 74 97 5 BROMOCHLOROMETHANE U jg/L 0 31 10 1 QC 06/08/10 75 27 4 BROMODICHLOROMETHANE u ug/ 0 19 10 1 QC 06/08/10 108 86 1 BROMOBENZENE U ug/L 0 37 10 1 QC 06/08/10 75 25 2 BROMOFORM U ug/L 0 42 10 1 QC 06/08/10 74 83 9 BROMOMETHANE U ug/L 0 57 10 1 QC 05/08/10 78 93 3 2 BUTANONE J ugL 1 11 10 1 QC 06/08/10 104 51 8 N BUTYLBENZENE u ug/L 0 3 10 1 QC 06/08/10 135 98 8 SEC BUTYLBENZENE u ug/L 04 10 1 QC 06/08/10 98 06 6 TERT BUTYLBENZENE u ug L 0 4 10 1 QC 06/08/10 75 15 0 CARBON DISULFIDE u ug/L 0 13 10 1 QC 06/08/10 56 23 5 CARBON TETRACHLORIDE u ug/L 0 27 10 1 QC 06/08/10 108 90 7 CHLOROBENZENE u ug/L 0 16 10 1 QC 06/08/10 75 00 3 CHLOROETHANE u ug/L 0 35 10 1 QC 06/08/10 110 75 8 2 CHLOROETHYLVINYL ETHER u ug/L 1 71 10 1 QC 06/08/10 67 66 3 CHLOROFORM u ug/L 0 3 10 1 QC 06/08/10 74 87 3 CHLOROMETHANE u ug/L 0 81 10 1 QC 06/08/10 95-49 8 2 CHLOROTOLUENE u ug/L 0 24 10 1 QC 06/08/10 106-43 4 4 CHLOROTOLUENE u ug/L 0 15 10 1 QC 06/08/10 124 48 1 DIBROMOCHLOROMETHANE u ug/L 0 18 10 1 QC 05/08/10 95 12 8 1 2 DIBROMO 3 CHLOROPROPANE u ug/L 0 35 10 1 QC 06/08/10 74 95 3 DIBROMOMETHANE u ug/L 0 25 10 1 QC 06/08/10 106 93 4 1 2 DIBROMOETHANE u ug/L 0 15 10 1 QC 06/08/10 95 50 1 1 2 DlCHLOROBENZENE u ug/L 5 86 10 1 QC 06/08/10 541 73 1 1 3 DlCHLOROBENZENE u ug/L 5 62 10 1 QC 06/08/10 106-46 7 1 4 DlCHLOROBENZENE u ug/L 5 88 10 1 QC 06/08/10 75 71 8 DICHLORODIFLUOROMETHANE u ug/L 0 66 10 1 QC 06/08/10 75 34 3 1 1 DICHLOROETHANE u ug/L 0 49 10 1 QC 06/08/10 107 06 2 1 2 DICHLOROETHANE u ug/L 0 29 10 1 QC 06/08/10 75 35-4 1 1 DICHLOROETHENE u ug/L 0 16 10 1 QC 06/08/10 156 59 4 CIS 1 2 DICHLOROETHENE u ug/L 0 16 10 1 QC 05/08/10 156-60 5 TRANS 1 2 DICHLOROETHENE u ug/L 0 34 10 1 QC 05/08/10 78 87 5 1 2 DICHLOROPROPANE u ug/L 0 16 10 1 QC 06/08/10 142 28 9 1 3 DICHLOROPROPANE u ug/L 0 24 10 1 QC 06/08/10 563 58 6 1 1 DICHLOROPROPENE u ug/L 0 17 10 1 QC 06/08/10 10061 01 5 CIS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 06/08/10 10061 02 6 TRANS 1 3 DICHLOROPROPENE u ug/L 04 10 1 QC 06/08/10 590 20 7 2 2 DICHLOROPROPANE u ug/L 0 9 10 1 QC 06/08/10 100 41 4 ETHYLBENZENE u ug/L 0 16 10 1 QC 06/08/10 591 76 6 2 HEXANONE u ug/L 07 10 1 QC 06/08/10 87 68 3 HEXACHLOROBUTADIENE u ug/L 09 10 1 QC 06/08/10 98 82 8 ISOPROPYLBENZENE u ug/L 0 58 10 1 QC 06/08/10 99 87 6 4 ISOPROPYLTOLUENE u ug/L 0 24 10 1 QC 06/08/10 75 09 2 METHYLENE CHLORIDE u jg/L 0 8 10 1 QC 05/08/10 108 10 1 4 ME'HYL 2 PENTANONE u ug/L 0 53 lO 1 QC 06/08/10 9 20 3 NAPHTHALENE u ug'L 4 10 QC 06/08/10 103 65 1 N PROPYLBENZENE u ug/L 0 5 0 QC 06/08/10 100 42 5 STYRENE u ug/L 0 3 10 1 GC 05/08/1 0 530 20 6 1112 TETRACHLOROETHANE u ug/L 0 25 10 1 QC 05/08/ 0 Page 14 of 18 Pnnted 06/16/10 1125 Listing of Results by Sample Sample Delivery Group 1006010 Ghent Sample ID FP 001 Sample Description ATK DLV Groundwater Spnng 2010 Laboratory Sample ID Date Sampled 1006010 07 06/03/10 14 15 GAS Number Test Parameter Result Units MDL EQL Dilution Factor Analvst Test Date Tesf Method SIV 846 82606 (IVaferj VoiatieOrga •ic Analysis 79 34 5 112 2 TETRACHLOROETHANE L ug/' 0 85 10 1 QC 06/08/10 127 16 4 •^E'TRACHLOROETHENE U ug/L 0 4 10 1 QC 06/08/10 108 88 3 TOLUENE J ug/L 0 5 10 1 QC 06/08/10 87 51 5 1 2 3 TRICHLOROBENZENE J jg/L 0 23 10 1 QC 08/08/ 0 120 82 1 1 2 4 TRICHLOROBENZENE J g/L 4 37 10 QC 06/08/10 71 56 5 1 1 1 TRICHLOROETHANE U 3/L 0 16 10 1 QC 06/08/10 79 00 5 1 1 2 TRICHLOROETHANE U ug/' 0 25 10 1 QC 06/08/10 79 01 6 TRICHLOROETHENE 8 8 o ug/L 0 7 10 1 QC 05/08/10 75 69-4 TRICHLOROFLUOROMETHANE U ug/L 0 3 10 1 QC 06/08/10 96 18 4 1 2 3 TRICHLOROPROPANE u ug/L 0 33 10 1 QC 06/08/10 95 63 5 1 2 4 TRIMETHYLBENZENE u ug/L 0 19 10 1 QC 06/08/10 108 57 8 1 3 5 TRIMETHYLBENZENE u ug/L 0 29 10 1 QC 06/08/10 108 05 4 VINYL ACETATE u ug/L 20 50 1 QC 06/08/10 75 01-4 VINYL CHLORIDE u ug/L 03 10 1 QC 06/08/10 1330 20 7 m p XYLENE u ug/L 06 10 1 QC 06/08/10 95-47 5 0 XYLENE u ug/L 0 3 10 1 QC 06/08/10 460 00 4 BROMOFLUOROBENZENE 96 2 / 1 QC 06/08/10 1868 53 7 DIBROMOFLUOROMETHANE 106 / 1 QC 06/08/10 17060 07 0 1 2 DICHLOROETHANE D4 108 / 1 QC 05/08/10 2037 26 5 TOLUENE D8 98 4 / QC 06/08/10 Ghent Sample ID B6 Laboratory Sample ID 1006010 08 Sample Description ATK DLV Groundwater Spnng 2010 Date Sampled 06/03/10 14 45 GAS Number Test Parameter Result Units MDL EQL Dilution Factor Analvst Test Date TesfMefhod EPA 120 1 Conductivity CONDUCTIVITY 7100 uS/cm 0 3 1 1 JMM 05/14/10 Tesf Method EPA 314 0 Perchlorate Ion Chromatography 014797 73 0 PERCHLORATE 43600 ug/L 100 400 100 JMM 06/15/10 Tesf Method SIV 846 82606 flVafer; Volatile Organic Analysis 57 54 1 ACETONE U ug/L 5 10 1 QC 06/08/10 71-43 2 BENZENE 0 6 J ug/L 0 22 10 1 QC 05/08/10 74 97 5 BROMOCHLOROMETHANE U ug/L 0 31 10 1 QC 06/08/10 75 27 4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 06/08/10 108 86 1 BROMOBENZENE U ug/L 0 37 10 1 QC 06/08/10 75 25 2 BROMOFORM U ug/L 0 42 10 1 QC 06/08/10 74 83 9 BROMOMETHANE U ug/L 0 57 10 1 QC 06/08/10 78 93 3 2 BUTANONE U ug/L 1 11 10 1 QC 06/08/10 104 51 8 N BUTYLBENZENE U ug/L 0 3 10 1 QC 06/08/10 135 98 8 SEC BUTYLBENZENE U ug/L 0 4 0 QC 06/08/10 98 06 6 TERT BUTYLBENZENE U ug/L 04 10 1 QC 06/08/ 0 75 15 0 CARBON DISULFIDE U Lg/L 0 13 10 QC 05/08/11. 56 23 5 CARBON "'•ETRACHLORIDE 08 J ug/-0 27 10 1 QC 05/08/iO 108 90 7 C-^LOROBENZENE U ug/ 0 16 10 1 QC 06/08/10 75 00 3 CH OROETHANE U ug/L 0 35 0 QC 06/08'1C 10 75 8 2 ChLOROEThvLViNY ETHER L ug/L 7 0 QC 06 08/10 67 66 3 Ch 0R0"0RV1 197 ug/L 0 3 10 QC 06/08 0 Page 15 of 18 Pnnted 06/16/10 1 25 Listing of Results by Sample Sample Delivery Group 1006010 Ghent Sample ID B6 Laboratory Sample ID 1006010 08 Sample Description ATK DLV Groundwa'er Sp rg 2010 Date Sampled 06/03/10 14 45 GAS Number Test Parameter Result Units MDL Dilution EQL Factor Analvst Test Date Tesf Method SIV 846 82606 (Water) Vo-ati e Organic Analysis 74 87 3 CHLOROMETHANE J ug/L 0 81 10 GC 06/08/1 0 95 49 8 2 CHLOROTOLUENE U ug/L 0 24 0 1 GC 06/08/10 106 43 4 4 CHLOROTOLUENE L ug/L 0 15 10 1 QC 06/08/10 124 48 1 DIBROMOCHLOROMETHANE U ug/L 0 8 10 QC 06/08/10 96 12 8 1 2 DIBROMO 3 CHLOROPROPANE J Lig/L 0 35 10 1 QC 06/08/10 74 95 3 DIBROMOMETHANE U ug/L 0 25 10 1 QC 06/08/10 106 93 4 1 2 DIBROMOETHANE U ug/L 0 15 lO 1 QC 06/08/1 0 95 50 1 1 2 DlCHLOROBENZENE U ug/L 5 86 10 1 GC 06/08/10 541 73 1 1 3 DlCHLOROBENZENE U ug/L 5 52 10 1 QC 06/08/10 106 46 7 1 4 DlCHLOROBENZENE u ug/L 5 88 10 1 QC 06/08/10 75 71 8 DICHLORODIFLUOROMETHANE u ug/L 0 66 10 1 QC 06/08/10 75 34 3 1 1 DICHLOROETHANE 12 2 ug/L 0 49 10 1 QC 06/08/10 107 06 2 1 2 DICHLOROETHANE 1 7 J ug/L 0 29 10 1 QC 06/08/10 75 35-4 1 1 DICHLOROETHENE 21 7 ug/L 0 16 10 1 QC 06/08/10 156 59 4 CIS 1 2 DICHLOROETHENE 35 4 ug/L 0 16 10 1 QC 06/08/10 156 60 5 TRANS 1 2 DICHLOROETHENE 4 8 J ug/L 0 34 10 1 QC 05/08/10 78 87 5 1 2 DICHLOROPROPANE U ug/L 0 16 10 1 QC 06/08/10 142 28 9 1 3 DICHLOROPROPANE U ug/L 0 24 10 1 QC 06/08/10 563 58 6 1 1 DICHLOROPROPENE U ug/L 0 17 10 1 QC 06/08/10 10061 01 5 CIS 1 3 DICHLOROPROPENE U ug/L 04 10 1 QC 06/08/10 10061 02 6 TRANS 1 3 DICHLOROPROPENE U ug/L 04 10 1 QC 06/08/10 590 20 7 2 2 DICHLOROPROPANE U ug/L 0 9 10 1 QC 06/08/10 100-41 4 ETHYLBENZENE U ug/L 0 16 10 1 QC 06/08/10 591 78 6 2 HEXANONE U ug/L 0 7 10 1 QC 06/08/10 87 68 3 HEXACHLOROBUTADIENE U ug/L 0 9 10 1 QC 06/08/10 98 82 8 ISOPROPYLBENZENE U ug/L 0 58 10 1 QC 06/08/10 99 87 6 4 ISOPROPYLTOLUENE U ug/L 0 24 10 1 QC 06/08/10 75 09 2 METHYLENE CHLORIDE U ug/L 0 8 10 1 QC 06/08/10 108 10 1 4 METHYL 2 PENTANONE U ug/L 0 53 10 1 QC 06/08/10 91 20 3 NAPHTHALENE U ug/L 4 10 1 QC 06/08/10 103-65 1 N PROPYLBENZENE U ug/L 0 5 10 1 QC 05/08/10 100-42 5 STYRENE U ug/L 03 10 1 QC 06/08/10 630 20 6 1112 TETRACHLOROETHANE U ug/L 0 25 10 1 QC 06/08/10 79 34 5 112 2 TETRACHLOROETHANE U ug/L 0 85 10 1 QC 06/08/10 127 18-4 TETRACHLOROETHENE U ug/L 04 10 1 QC 06/08/10 108 88 3 TOLUENE U ug/L 0 5 10 1 QC 06/08/10 87 61 6 1 2 3 TRICHLOROBENZENE U ug/L 0 23 10 1 QC 06/08/10 120 82 1 1 2 4 TRICHLOROBENZENE U ug/L 4 37 10 1 QC 06/08/10 71 55 5 1 1 1 TRICHLOROETHANE 140 J ug/L 3 2 200 20 QC 05/08/10 79 00 5 1 1 2 TRICHLOROETHANE U ug/L 0 25 10 1 QC 06/08/10 79 01 6 TRICHLOROETHENE 2220 ug/L 14 200 20 QC 05/08/10 75 69-4 TRICHLOROFLUOROMETHANE U ug/L 0 3 10 1 QC 06/08/10 96 18 4 1 2 3 TRICHLOROPROPANE U ug/L 0 33 10 1 QC 05/08/10 95 53 6 1 2 4 TRIMETHYLBENZENE U ug/L 0 19 10 1 QC 05/08/10 108 67 8 1 3 5 TRIVETHYLBENZENE U ug/L 0 29 10 1 QC 06/08/10 108 05 4 VINYL ACETATE u LQ/-20 50 1 QC 05/08/ 0 75 01 4 ViNVL CHLORIDE J ug/L 0 3 10 1 QC 06/08/10 1330 20 7 m p XVLENE u ug'L 0 6 10 QC 06/08/10 95 47 5 0 Xv^ENE L ^g 0 3 0 : QC 06/08 10 450 OL 4 BROVOF->.OROBENZENE 95 4 GC 06'08/10 Page 16 of 18 Pnnted 06/16/10 11 ^5 Listing of Results by Sample Sample Delivery Group 1006010 Ghent Sample ID B6 Sample Description ATK DLV Grourdwate Spring 2010 Laboratory Sample ID Date Sampled 1006010 08 06/03/10 14 45 GAS Number Test Method 1868 53 7 17060 07 0 2037 26 5 Test Parameter SIV 846 8260B (Water) Result Vola lie Organic Anaiysis Units MDL Dilution Factor Analvst Test Date DIBROMOFLUOROMET-ANE 1 2 DICHLOROETHANE D4 'OLUENE D8 107 / 113 / 95 8 / QC QC QC 06/08/10 06/08/10 06/08/10 Page 17 of 18 Pnnted 06/16/10 1 25 Data Reporting Qualifiers U Indicates that the analyte concentration is less than the MDL B This flag is used when an analyte is found in the blank as well as the sample Indicates an extimated value This flag is used either when estimating a concentration for tentatively identified compounds or when the data indicated the presence of a compound that meets the identification criteria but the result is less than the EQL (eg 3 J with an EQL of 10) MDL Method Detection Limit The minimum concentration of a substance that can be confidently measured and reported The laboratory has demonstrated that the MDL can be achieved in a laboratory reagent blank but does not guarantee it can be achieved in all sample matrices EQL Estimated Quantitation Limit The EQL generally is 5 to 10 times the MDL For many analytes the EQL is selected as the value of the lowest standard in the calibration curve Dilution Dilution Factor The prepared sample was diluted by this factor because the Factor sample was too concentrated or due to other interferences in the sample matnx Any dilution factor causes a corresponding increase in the MDL and EQL Page 18 of 18 Pnnted 06/16/10 1125 ATK Launch Systems Environmental Laboratory Sample Receipt Checklist Clien Hamifl'Tf<- LiLU^C^ ^(fr^U**^- D LV SDG NO Camer Carrier NuTbe Z Hand delivered no cooler : Hand delivered sample(s) lar<en ou1 a receiving counter Cooler Information , Cooler Number/ID ^ /(MJL ^ IAJ /-t^ 'f—C Condition of Shioping Container Cooler Sealeo (taped) Custody Seals Present ^^^i^ood lYes I In act "Fair >lo ^0 "Broken IBIue Ice ZNone Not App icable Not Applicab e Not Applicable Damaged (expiain). Seal Number , O her Coolant State of Coolant ZFrozen ;3fartially Frozen _Melted Ttiermomete ID Read nq >^ C CF Pack ng Descript on ^/^^ Corrected Temp _ Temp BlanK Included ""Yes :NO Chain-Of Custody Information COC Present r i ^ / / --r COC Number(s) A / Ib/^ f COC signed (relinquished and received) jS^es COC or LWI agrees with san^ple labels ;si'es • No • No • No other • Not Applicable CNot Applicable Sample information Samples Included In cooler Custody Seals Presen Sample containers Intact Samples In proper containers Sufficient sample volume All samples received in hold time HYes •Intact ;SlYes ^fi-es J(^es ;^es Water-VOAs have ze o headspace ^^re-presen/ed with HCI Notes ;S!No •Broken •No rNo JNo • No other Seal Number(s) _ Notes ^es JNo QNot Applicable •Pre preserved with NajSjOj ") Non-Preserved Water-pH acceptable upon receipt "Yes CAdJusted (see comments below) Jiflot Applicable HNO3 = H,SO = NaOH = ZnAC /NaOH = HCL = Water pH adjusted (mfg & Lot No) HNO3 HzSO,. NajSOjOs Other _ Notes NaOH ZnAC HCI SOP 102 Form A 2 010 Spring GW Sampling ATK Launch Systems, Inc Promontory, UTAH (801) 251-5688 SAMPLE NUMBER /)- ( DATE ^ f^(iC> SAMPLER 1006010 ANALYTICAL LABORATORY ATK Environmental Laboratory MS3 Bottle Number No of Containers Fid Preservative/ Treatment Reque'iSted Analysis 11 3 4 degrees C |vOA, Appendix 9 Acidified Method 8260 2 mL HCL 1 9 1 4 degrees C 1 iPerchlorate, Conductivity ,EPA Method 314 0 2010 Spring GW Sampling 1006010 SAMPLE NUMBER lo ATK Launch Systems, Inc Promontory, UTAH (801) 251-5688 DATE Ajik SAMPLER ANALYTICAL LABORATORY ATK Environmental Laboratory M53 Bottle Number No of Containers Fid Preservative/ Treatment Recjue sted Analysis 11 3 4 degrees C Acidified 2 mL HCL VOA, Appendix 9 Method 8260 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314 0 2 010 Spring GW Sampling ATK Launch Systems, Inc Promontory, UTAH (801) 251-5688 SAMPLE NUMBER ^-Zl> DATE ^/^-^/jO SAMPLER 1006010 ANALYTICAL LABORATORY ATK Environmental Laboratory M53 Bottle Number No of Containers Fid Preservative/ Treatment 1 1 Requested Analysis 11 3 4 degrees C Acidified 2 mL HCL |vOA, Appendix 9 Method 8260 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314 0 2 010 Spring GW Sampling ATK Launch Systems, Inc Promontory, UTAH (801) 251-5688 SAMPLE NUMBER 6-Z DATE Q>kll]0 SAMPLER 1006010 ANALYTICAL LABORATORY ATK Environmental Laboratory MSB I Bottle No of Preservative/ Number Containers Fid Treatment Recjueisted Analysis 11 4 degrees C Acidified 2 mL HCL jVOA, Appendix 9 Method 8260 4 degrees C Perchlorate, Conductivity EPA Method 314 0 2010 Spring GW Sampling 1006010 ATK Launch Systems, Inc P romontory, UTAH (801) 251-5688 SAMPLE NUMBER DATE SAMPLER ANALYTICAL LABORATORY ATK Environmental Laboratory M53 Bottle No of Preservative/ Number Containers Fid Treatment Requested Analysis 11 4 degrees C Acidified 2 mL HCL VOA, Appendix 9 Method 8260 4 degrees C Perchlorate, Conductivity EPA Method 314 0 2 010 Spring GW Sampling ATK Launch Systems, Inc Promontory, UTAH (801) 251-5688 SAMPLE NUMBER IP-00( DATE 4rf-^ SAMPLER OA 1006010 ANALYTICAL LABORATORY ATK Environmental Laboratory M53 Bottle Number No of Containers Fid Preservative/ Treatment Recjuested Analysis 11 3 4 degrees C VOA, Appendix 9 Acidified Method 8260 2 mL HCL 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314 0 2 010 Spring GW Sampling 1006010 SAMPLE NUMBER fF-Q:>{ ATK Launch Systems, Inc Promontory, UTAH (801) 251-5688 DATE SAMPLER ANALYTICAL LABORATORY ATK Environmental Laboratory M53 Bottle Number No of Containers Fid Preservative/ Treatment Requested Analysis 11 3 4 degrees C VOA, Appendix 9 Acidified Method 8260 2 mL HCL 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314 0 SAMPLE NUMBER 2 010 Spring GW Sampling ATK Launch Systems, Inc P romont o ry, UTAH (801) 251-5688 DATE STAPLER 1006010 ANALYTICAL LABORATORY ATK Environmental Laboratory MS3 Bottle Number No of Containers Fid Preservative/ Treatment Requested Analysis 11 3 4 degrees C VOA, Appendix 9 Acidified Method 8260 2 mL HCL 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314 0 1006011 ENVIRONMENTAL LAB WORK REQUEST ™ ATK ENVIRONMENTAL LABORATORY LWR No Login iNo E13168 FROM y. 1 EXTE>S10N COST CENTER WORKORDER DATE / / ORGAMZATION ^U(^v\nie*i^<^ Seiroiccs MAIL STOP ^/ REPORT RESLLTS TO HELEN RAVSTEN, MS 301 SAMPLE INFORMATION SAMPLE DATE TYPE LOCATION TIME TEST REMARKS SAMPLE DATE G C LOCATION TIME TEST REMARKS • 2 J 3 4 5 6 7 8 9 10 II 12 CHAIN OF CUSTODY RiluraUISHEDB^ DATE TIME RECEIVED BY DATE TIME ^////^ /YJo [/'tyty'*'-' r- / FOR LABORATORY LSE ONLY DATE COMPI^TED DATE REPORTED 988P LS333 GW CERTIFICATE OF ANALYSIS Listing of Sample Information and Testing Requested Wednesday June 16, 2010 TESTED FOR ATK DLV Environmental Monitoring Thiokol Corp, UT 84322 ANALYZED BY ATK Launch Systems Analytical Chemistry Laboratory P O Box 707, M/S 245 Bngham City, UT 84302-0707 435-863-3732 435-863-8080 Contact Name Project Sample Delivery Group Al Lee Ground Water Testing - DLV 1006011 Page 1 of 5 Prnted 05/16/10 1126 Sample Delivery Group 1006011 Sample No Client No Test Requested 1006011 01 A 8 Sample Description Received Collect Date/Time Matrix 06/04/10 6/4/2010 14 00 4, EPA 120 1 EPA 314 0 SW846 8260B (Water) Conductivity Perchlorate Ion Chromatography Volatile Organic Analysis Water Water Water Certified By W Scott Fraser Quality Assurance Officer 06/17/2010 Date This certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation Program (NELAP) unless otherwise annotated Page 2 of 5 Printed 06/16/10 1126 Listing of Results by Sample Sample Delivery Group 1006011 Client Sample ID A 8 Laboratory Sample ID 1006011 01 Sample Description ATK DLV Groundwater Spring 20 0 Date Sampled 06/04/10 14 00 CAS Number Test Parameter Result Units MDL EQL Dilution Factor Analvst Test Date Test Method EPA 120 1 Conductivity CONDUCTIVITY 1200 uS/cm 0 3 1 1 JVIM 06/14/ 0 Test Method EPA 314 0 Perchlora e Ion Chromatograpny 014797 73 0 PERCHLORATE 8520 uglL. 100 400 100 JMV 06/15/10 Test Method SW 846 8260B (Water) Vola ile Organic Anaiys s 67 6<t 1 ACETONE L ug/L 5 10 1 QC 06/08/10 71 43 2 BENZENE 34 J ug/L 0 22 10 1 QC 06/08/10 74 97 5 BROMOCHLOROMETHANE U ug/L 0 31 10 1 QC 06/08/10 75 27-4 BROMODICHLOROMETHANE U ug/L 0 19 10 1 QC 06/08/10 108 86 1 BROMOBENZENE U ug/L 0 37 10 1 QC 06/08/10 75 25 2 BROMOFORM U ug/L 0 42 10 1 QC 06/08/10 74 83 9 BROMOMETHANE U ug/L 0 57 10 1 QC 06/08/10 78 93 3 2 BUTANONE U ug/L 1 11 10 1 QC 06/08/10 104 51 8 N BUTYLBENZENE U ug/L 0 3 10 1 QC 06/08/10 135 98 8 SEC BUTYLBENZENE U ug/L 04 10 1 QC 06/08/10 98 06 6 TERT BUTYLBENZENE U ug/L 0 4 10 1 QC 06/08/10 75 15 0 CARBON DISULFIDE U ug/L 0 13 10 1 QC 08/08/10 56 23 5 CARBON TETRACHLORIDE 6 5 J ug/L 0 27 10 1 QC 06/08/10 108 90 7 CHLOROBENZENE 1 J ug/L 0 16 10 1 QC 06/08/10 75 00 3 CHLOROETHANE U ug/L 0 35 10 1 QC 06/08/10 110 75 8 2 CHLOROETHYLVINYL ETHER U ug/L 1 71 10 1 QC 06/08/10 67 66 3 CHLOROFORM 142 ug/L 0 3 10 1 QC 06/08/10 74 87 3 CHLOROMETHANE U ug/L 0 81 10 1 QC 06/08/10 95-49 8 2 CHLOROTOLUENE U ug/L 0 24 10 1 QC 06/08/10 106-43 4 4 CHLOROTOLUENE U ug/L 0 15 10 1 QC 06/08/10 124^8 1 DIBROMOCHLOROMETHANE U ug/L 0 18 10 1 QC 06/08/10 96 12 8 1 2 DIBROMO 3 CHLOROPROPANE U ug/L 0 35 10 1 QC 06/08/10 74 95 3 DIBROMOMETHANE U ug/L 0 25 10 1 QC 06/08/10 106 93 4 1 2 DIBROMOETHANE U ug/L 0 15 10 1 QC 06/08/10 95 50 1 1 2 DlCHLOROBENZENE U ug/L 5 86 10 1 QC 06/08/10 541 73 1 1 3 DlCHLOROBENZENE U ug/L 5 62 10 1 QC 06/08/10 106^6 7 1 4 DlCHLOROBENZENE U ug/L 5 88 10 1 QC 06/08/10 75 71 8 DICHLORODIFLUOROMETHANE U ug/L 0 66 10 1 QC 06/08/10 75 34 3 1 1 DICHLOROETHANE 51 ug/L 0 49 10 1 QC 06/08/10 107 06 2 1 2 DICHLOROETHANE 84 J ug/L 0 29 10 1 QC 06/08/10 75 35-4 1 1 DICHLOROETHENE 543 ug/L 8 500 50 QC 06/08/10 156 S9-4 CIS 1 2 DICHLOROETHENE 21 3 ug/L 0 16 10 1 QC 06/08/10 156 60 5 TRANS 1 2 DICHLOROETHENE U ug/L C 34 10 1 QC 06/08/10 78 87 6 1 2 DICHLOROPROPANE U ug/L 0 16 10 1 QC 06/08/10 142 28 9 1 3 DICHLOROPROPANE U ug/L 0 24 10 1 QC 06/08/10 563 58 6 1 1 DICHLOROPROPENE U ug/L 0 17 10 1 QC 06/08/10 10061 01 6 CIS 1 3 DICHLOROPROPENE J ug/L 0 4 10 1 QC 06/08/10 10061 02 6 TRANS 1 3 DICHLOROPROPENE U ug/L 04 10 1 QC 06/08/10 590 20 7 2 2 DICHLOROPROPANE U ug/L 0 9 10 1 QC 06/08/1C 100-41 4 ETHYLBENZENE U -g/L 0 16 0 QC 06/08/10 59 78 6 2 HEXANONE J jg/L 0 7 10 1 QC 06/08/10 87 68 3 HEXACHLOROBUTADIENE U ug/L 0 9 10 1 QC C6/08/10 98 82 8 ISOPRO=VLBE^ZE^E U -g/L 0 58 lO 1 GC 06/08/ 0 99 87 6 4 iSO=ROPY TOLUENE J -g/-0 24 '0 QC 061081 0 75 09 2 VE'HVLt\E CHLOR DE ugL 0 8 10 QC 06'08/10 Page 3 of 5 Pnnted 06/16/10 11 26 Listing of Results by Sample Sample Delivery Group 1006011 Client Sample ID A 8 Sample Description ATK DLV Groundwate Spnng 2010 Laboratory Sample ID Date Sampled 1006011 01 06/04/10 14 00 Dilution Number Test Parameter Result Units MDL EQL Factor Analyst Test Date s( Method SIV 846 82606 (Water) Volatne 0 game Analysis 108 10 4 METHYL 2 PENTANONE L ug/L 0 53 0 QC 06/08/10 91 20 3 NAPHTHALENE U ug/L 4 10 1 QC 06/08/-' 0 103 55 1 N PROPYLBENZENE U ug/L 0 5 10 1 QC 06/08/10 100 42 5 S'YRENE U ug/L 0 3 10 1 QC 06/08/10 630 20 6 1112 TETRACHLOROETHANE U ug/L 0 25 10 QC 06/08/10 79 34 5 1 2 2 TETRACHLOROETHANE U ug/L 0 85 10 1 QC 06/08/10 27 18 4 TETRACHLOROETHENE 2 8 J ug/L 04 10 1 QC 06/08/10 108 88 3 TOLUENE U ug/L 0 5 10 1 QC 06/08/10 87-61 6 1 2 3 TRICHLOROBENZENE U ug/L 0 23 10 1 QC 06/08/10 120 82 1 1 2 4 TRICHLOROBENZENE U ug/L 4 37 10 1 QC 06/08/10 71 55 6 1 1 1 TRICHLOROETHANE 811 ug/L 8 500 QC 06/08/10 79 00 5 1 1 2 TRICHLOROETHANE 37 J ug/L 0 25 10 1 QC 06/08/10 79 01-6 TRICHLOROETHENE 4490 ug/L 35 500 50 QC 06/08/10 75 69-4 TRICHLOROFLUOROMETHANE 1 J ug/L 0 3 10 1 QC 06/08/10 96 18-4 1 2 3 TRICHLOROPROPANE U ug/L 0 33 10 1 QC 06/08/10 95 63 6 1 2 4 TRIMETHYLBENZENE U ug/L 0 19 10 1 QC 06/08/10 108 67 8 1 3 5 TRIMETHYLBENZENE U ug/L 0 29 10 1 QC 06/08/10 108 05 4 VINYL ACETATE U ug/L 20 50 1 QC 06/08/10 75 01-4 VINYL CHLORIDE U ug/L 0 3 10 1 QC 06/08/10 1330 20 7 mp XYLENE U ug/L 0 6 10 1 QC 06/08/10 95-47 6 0 XYLENE U ug/L 0 3 10 1 QC 06/08/10 460 00 4 BROMOFLUOROBENZENE 95 3 / 1 QC 06/08/10 1868 53 7 DIBROMOFLUOROMETHANE 104 /o 1 QC 06/08/10 17060 07 0 1 2 DICHLOROETHANE D4 110 % 1 QC 06/08/10 2037 26 5 TOLUENE D8 97 1 % 1 QC 06/08/10 P tr ed Page 4 of 5 06/16/10 11 26 Data Reporting Qualifiers Indicates that the analyte concentration is less than the MDL This flag is used when an analyte is found in the blank as well as the sample Indicates an extimated value This flag is used either when estimating a concentration for tentatively identified compounds or when the data indicated the presence of a compound that meets the identification criteria but the result is less than the EQL (e g 3 J with an EQL of 10) MDL Method Detection Limit The minimum concentration of a substance that can be confidently measured and reported The laboratory has demonstrated that the MDL can be achieved in a laboratory reagent blank but does not guarantee it can be achieved in all sample matrices EQL Estimated Quantitation Limit The EQL generally is 5 to 10 times the MDL For many analytes the EQL is selected as the value of the lowest standard in the calibration curve Dilution Dilution Factor The prepared sample was diluted by this factor because the Factor sample was too concentrated or due to other interferences in the sample matrix Any dilution factor causes a corresponding increase in the MDL and EQL Page 5 of 5 Pnnted 06/16/10 1126 ATK Launch Systems Environmental Laboratory Sample Receipt Checklist C lent Name SDG ,\o Camer _ ~ Hand delivoreo ro cooler CaTie Number _ Hand de ivered sample(s) tanen o at receiving cour'er Cooler Information Cooler Number/ID Condition of Shipping Container ^Cooo Cooler Sealed (taped) Cus ody Seals Present Coolant State of Coolant CFai -.3roker ZBtue Ice "None Frozen ^Parially Frozen :Yes :Yes Intact Not Applicable Not Applicable NotApp'i able .Damaged (explain). Seal Number . Other Thermome er ID Reading, _ C CF Corrected Temp _ Temp Blank hJuded 3Yes INo Cham Of Custody Information COC Present r ^ I j C- COC Numberfst A/3/ COC signed (relinquished and received) COC or LWI agrees with sample labels ^e Notes -No rNo GNo Othe CNot Applicable ::Not Applicable Sample Infonmation Samples included in cooler Custody Seals Present Sample containers intact Samples in proper containers Stifficient sample volume All samples received In hold time Water - VOA s have zero headspace Ijipre-preserved with HCI Notes ' •Yes • Intact ;SYes ^e^ ifVes ;X*'es ^fJo Oher •Broken Seal Number{s). •No Notes CNo •No CNo JNo jPre preserved with NajSjOj jNot Applicable • Non Preserved Water - pH acceptable upon receipt aYes ^Adjusted (see comments below) ^ot Applicable HNOJ = HjSO, = NaOH = ZnAC /NaOH = HCL = Water pH adjusted (mfg & Lot No) HNO3 HjS04 NajSOjOj Other _ No es NaOH ZnAC HCI SOP 102 Form A SAMPLE NUMBER 2 010 Spring GW Sampling ATK Launch Systems, Inc Promontory, UTAH (801) 251-5688 DATE SAMPLER 1006011 ANALYTICAL LABORATORY ATK Environmental Laboratory M53 Bottle Number No of Containers Fid Preservative/ Treatment Requested Analysis 11 3 4 degrees C VOA, Appendix 9 Acidified Method 8260 2 mL HCL 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314 0 Appendix D 3 2 D C B A D N 507,0 N 506,0 STATE HIGHWAY 83 c B A REV. NO, BY DATE REV. 5A BY DATE REV. NO A BY DRAWN CHECKED ENGINEER SAFETY FACILiTIES USER DRAWN CHECKED ENGINEER SAFETY FACILITIES USER DRAWN DATE CHECKED ENGINEER SAFETY FACILITIES USER REV. NO.. A BY DATE REV. NOy BY DATE REV. NO .V.A A BY DATE DRAWN CHECKED ENGINEER SAFETY FACILfTIES USER DRAWN CHECKED ENGINEER SAFETY FACILTTIES USER DRAWN CHECKED ENGINEER SAFETY FACIUTIES USER REV. NO. BY DATE REV. NOv 'A BY DATE REV. NO A BY DATE DRAWN CHECKED ENGINEER SAFETY FACIUTIES USER DRAWN CHECKED ENGINEER SAFETY FACILITIES USER DRAWN CHECKED ENGINEER SAFETY FACILITIES USER REV. NO.. A BY DATE R^. NO/ A BY DATE REV. NO :V.A A BY DATE DRAWN CHECKED ENGINEER SAFETY FACILTTIES USER DRAWN CHECKED ENGINEER SAFETY FACILITIES USER DRAWN CHECKED ENGINEER SAFETY FACILITIES USER DWG. NO. REFERENCE DRAWINGS DRAWN CHECKED ENGINEER SAFETY FACIUTIES USER MFG. ENGR. imESS ENGR. UnUTIES RRE DEPT. RRE PROT. BY KHB ABL DATE 7/2010 7/2010 ATK ATK Launch Systems Inc. FACILITIES ENGINEERING P.O. Box 707 ms UT40-552 Brigham City, Utah 84302 PLATE 1 SPRING 2010 PDTENTIDMETRIC SURPACE SHEET 1 DF 2 FED NO. SCALE GRID = 1000' DRAWING NO. 2010 PaTENTHMETRICDWG REV. 4 3 SIZE F-42x30 AUTOCAD 4 3 2 D C B A TCC6 -5)l2abc-S 7 H-10 (B-10-5)l2cbb-S HORSE SPRING (A) 4247.5 REV. . "A REV. . "A REV. . "A REV. . "A DWG. NO. REFERENCE DRAWINGS BY DATE M^^TMM ATK Launch Systerns Inc. REV. . "A REV. . "A REV. . "A REV. . "A DWG. NO. REFERENCE DRAWINGS DRAWN KHB 7/2010 M^^TMM ATK Launch Systerns Inc. DRAWN CHECKED ENGINEER SAFETY FACIUTIES USER DRAWN CHECKED ENGINEER SAFETY FACIUTIES USER DRAWN CHECKED ENGINEER SAFETY FACIUTIES USER DRAWN CHECKED ENGINEER SAFETY FACIUTIES USER CHECKED ABL 7/aoio P.O. Box 707 ms UT40-552 BY BY BY BY ENGINEER Brigham City, Utah 84302 DATE DATE DATE DATE SAFETY REV.A "A REV.A REV.A "A REV.A SAFETY REV.A "A REV.A REV.A "A REV.A FACIUTIES h^LA 1 L i REV.A "A REV.A REV.A "A REV.A USER DRAWN CHECKED ENGINEER SAFETY FACIUTIES USER DRAWN CHECKED ENGINEER SAFETY FACIUTIES USER DRAWN CHECKED ENGINEER SAFETY FACIUTIES USER DRAWN CHECKED ENGINEER SAFETY FACIUTIES USER USER SPRING 2010 PDTENTIDMETRIC SURPACE BY BY BY BY MFG. ENGR. SPRING 2010 PDTENTIDMETRIC SURPACE DATE DATE DATE DATE PROCESS ENGR. SPRING 2010 PDTENTIDMETRIC SURPACE ®A REV.A ^A «A UTIUTIES SPRING 2010 PDTENTIDMETRIC SURPACE ®A REV.A ^A «A RRE DEPT. SHEET 2 E F 2 DRAWN CHECKED ENGINEER SAFETY FACIUTIES USER DRAWN CHECKED ENGINEER SAFETY FACIUTIES USER DRAWN CHECKED ENGINEER SAFETY FACIUTIES USER DRAWN CHECKED ENGINEER SAFETY FACIUTIES USER RRE PROT. FEO NO. SCALE DRAWING NO. GRID = 1000' 2010 PDTENTinMETRICDWG REV. BY BY BY BY RRE PROT. FEO NO. SCALE DRAWING NO. GRID = 1000' 2010 PDTENTinMETRICDWG REV. DATE DATE DATE DATE FEO NO. SCALE DRAWING NO. GRID = 1000' 2010 PDTENTinMETRICDWG REV. D C B A 4 3 F-42X30 AUTOCAD 988P LS333 GW CERTIFICATE OF ANALYSIS Listing of Sample Information and Testing Requested Wednesday, June 16, 2010 TESTED FOR: ATK: DLV Environmental Monitoring Thiokol Corp, UT 84322 ANALYZED BY: ATK Launch Systems Analytical Chemistry Laboratory P.O. Box 707, M/S 245 Brigham City, UT 84302-0707 435-863-3732 435-863-8080 Contact Name: Project: Sample Delivery Group: Al Lee Ground Water Testing - DLV 1006008 Page 1 of 12 Printed: 06/16/10 11:21 Sample Delivery Group: 1006008 Sample No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 1006008-01 Connor Spring 06/02/10 6/1/2010 12:00:26 EPA 120.1 EPA 314.0 SW-846. 301 OA SW-846. 601 OB (Water) SW-846. 7470A SW-846. 8260B (Water) Conductivity Perchlorate - Ion Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water Water 1006008-02 Fork Spring 06/02/10 6/1/2010 12:30:26 EPA 120.1 EPA 314.0 SW-846. 301 OA SW-846. 601 OB (Water) SW-846. 7470A SW-846. 8260B (Water) Conductivity Perchlorate - Ion Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water Water 1006008-03 Pipe Spring 06/02/10 6/1/2010 12:50:26 EPA 120.1 EPA 314.0 SW-846. 301 OA SW-846. 601 OB (Water) SW-846. 7470A SW-846. 8260B (Water) Conductivity Perchlorate - Ion Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water Water 1006008-04 Shot Gun Spring 06/02/10 6/1/2010 13:20:26 EPA 120.1 EPA 314.0 SW-846. 301 OA SW-846. 601 OB (Water) SW-846. 7470A Conductivity Perchlorate - Ion Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Water Water Water Water Water Page 2 of 12 Printed: 06/16/10 11:21 Sample Delivery Group: 1006008 Sample No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 1006008-04 Shot Gun Spring 06/02/10 6/1/2010 13:20:26 SW-846. 8260B (Water) Volatile Organic Analysis Water Certified By: 06/17/2010 W. Scott Fraser, Quality Assurance Officer Date This ceiiifies that the following data meets the requirements of the National Environmental Laboratory Accreditation Program (NELAP) unless otherwise annotated: Page 3 of 12 Printed: 06/16/10 11:21 Listing of Results by Sample Sample Delivery Group: 1006008 Client Sample ID: Connor Spring Sample Description: ATK-DLV- Groundwater Spring Sampling 2010 Laboratory Sample ID: 1006008-01 Date Sampled: 06/01/10 12:00 AS Number Test Parameter Result Units MDL EQL Dilution Factor Analyst Test Date TestMe^od: EPA 120.1 Conductivity CONDUCTIVITY 4110 uS/cm 0.3 1 1 JMM 06/11/10 TestMe^od: EPA 314.0 Perchlorate - Ion Chromatography 014797-73-0 PERCHLORATE U ug/L 5 20 5 JMM 06/11/10 TestMe^od: SW-846, 3010A Metals Digestion 3010A ACID DIGESTION 06/07/2010 12:00:00 am 1 MTB 06/08/10 TestMe^od: SlV-846, 6010B (Wafef) Metals Analysis by ICP - 6010 7440-38-2 ARSENIC U ug/L 20 100 1 MTB 06/07/10 7440-39-3 BARIUM 70.2 ug/L 2 10 1 MTB 06/07/10 7440-43-9 CADMIUM U ug/L 1 5 1 MTB 06/07/10 7440-47-3 CHROMIUM U ug/L 10 50 1 MTB 06/07/10 7440-48-4 COBALT U ug/L 1 5 1 MTB 06/07/10 7439-92-1 LEAD U ug/L 20 100 1 MTB 06/07/10 7439-98-7 MOLYBDENUM U ug/L 1 5 1 MTB 06/07/10 7782-49-2 SELENIUM U ug/L 30 150 1 MTB 06/07/10 7440-22-4 SILVER U ug/L 1 5 1 MTB 06/07/10 TestMe^od: SlV-846, 7470A Mercury Analysis 7439-97-6 MERCURY U ug/L 0.3 1 1 TCP 06/08/10 TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 67-64-1 ACETONE U ug/L 5 10 1 OC 06/04/10 71-43-2 BENZENE U ug/L 0.22 10 1 OC 06/04/10 74-97-5 BROMOCHLOROMETHANE U ug/L 0.31 10 1 OC 06/04/10 75-27-4 BROMODICHLOROMETHANE U ug/L 0.19 10 1 OC 06/04/10 108-86-1 BROMOBENZENE U ug/L 0.37 10 1 OC 06/04/10 75-25-2 BROMOFORM U ug/L 0.42 10 1 OC 06/04/10 74-83-9 BROMOMETHANE U ug/L 0.57 10 1 OC 06/04/10 78-93-3 2-BUTANONE U ug/L 1.11 10 1 OC 06/04/10 104-51-8 N-BUTYLBENZENE U ug/L 0.3 10 1 OC 06/04/10 135-98-8 SEC-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/04/10 98-06-6 TERT-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/04/10 75-15-0 CARBON DISULFIDE U ug/L 0.13 10 1 OC 06/04/10 56-23-5 CARBON TETRACHLORIDE U ug/L 0.27 10 1 OC 06/04/10 108-90-7 CHLOROBENZENE U ug/L 0.16 10 1 OC 06/04/10 75-00-3 CHLOROETHANE u ug/L 0.35 10 1 OC 06/04/10 110-75-8 2-CHLOROETHYLVINYL ETHER u ug/L 171 10 1 OC 06/04/10 67-66-3 CHLOROFORM u ug/L 0.3 10 1 OC 06/04/10 74-87-3 CHLOROMETHANE u ug/L 0.81 10 1 OC 06/04/10 95-49-8 2-CHLOROTOLUENE u ug/L 0.24 10 1 OC 06/04/10 106-43-4 4-CHLOROTOLUENE u ug/L 0.15 10 1 OC 06/04/10 124-48-1 DIBROMOCHLOROMETHANE u ug/L 0.18 10 1 OC 06/04/10 96-12-8 1.2-DIBROMO-3-CHLOROPROPANE u ug/L 0.35 10 1 OC 06/04/10 74-95-3 DIBROMOMETHANE u ug/L 0.25 10 1 OC 06/04/10 106-93-4 1.2-DIBROMOETHANE u ug/L 0.15 10 1 OC 06/04/10 95-50-1 1.2-DICHLOROBENZENE u ug/L 5.86 10 1 OC 06/04/10 541-73-1 1.3-DICHLOROBENZENE u ug/L 5.62 10 1 OC 06/04/10 106-46-7 1.4-DICHLOROBENZENE u ug/L 5.88 10 1 OC 06/04/10 75-71-8 DICHLORODIFLUOROMETHANE u ug/L 0.66 10 1 OC 06/04/10 Page 4 Of 12 Printed: 06/16/10 11:21 Listing of Results by Sample Sample Delivery Group: 1006008 Client Sample ID: Connor Spring Laboratory Sample ID: 1006008-01 Date Sampled: 06/01/10 12:00 Sample Description: ATK-DLV- Groundwater Spring Sampling 2010 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 75-34-3 1.1-DICHLOROETHANE u ug/L 0.49 10 1 OC 06/04/10 107-06-2 1.2-DICHLOROETHANE u ug/L 0.29 10 1 OC 06/04/10 75-35-4 1.1-DICHLOROETHENE u ug/L 0.16 10 1 OC 06/04/10 156-59-4 CIS-1.2-DICHLOROETH ENE u ug/L 0.16 10 1 OC 06/04/10 156-60-5 TRANS-1.2-DICHL0R0ETHENE u ug/L 0.34 10 1 OC 06/04/10 78-87-5 1.2-DICHLOROPROPANE u ug/L 0.16 10 1 OC 06/04/10 142-28-9 1.3-DICHLOROPROPANE u ug/L 0.24 10 1 OC 06/04/10 563-58-6 1.1-DICHLOROPROPENE u ug/L 0.17 10 1 OC 06/04/10 10061-01-5 CIS-1.3-DICHLOROPROPENE u ug/L 0.4 10 1 OC 06/04/10 10061-02-6 TRANS-1.3-DICHLOROPROPENE u ug/L 0.4 10 1 OC 06/04/10 590-20-7 2.2-DICHLOROPROPANE u ug/L 0.9 10 1 OC 06/04/10 100-41-4 ETHYLBENZENE u ug/L 0.16 10 1 OC 06/04/10 591-78-6 2-HEXANONE u ug/L 07 10 1 OC 06/04/10 87-68-3 HEXACHLOROBUTADIENE u ug/L 0.9 10 1 OC 06/04/10 98-82-8 ISOPROPYLBENZENE u ug/L 0.58 10 1 OC 06/04/10 99-87-6 4-ISOPROPYLTOLUENE u ug/L 0.24 10 1 OC 06/04/10 75-09-2 METHYLENE CHLORIDE u ug/L 0.8 10 1 OC 06/04/10 108-10-1 4-M ETHYL-2-PEN TAN ONE u ug/L 0.53 10 1 OC 06/04/10 91-20-3 NAPHTHALENE u ug/L 4 10 1 OC 06/04/10 103-65-1 N-PROPYLBENZENE u ug/L 0.5 10 1 OC 06/04/10 100-42-5 STYRENE u ug/L 0.3 10 1 OC 06/04/10 630-20-6 1.1.1.2-TETRACHLOROETHANE u ug/L 0.25 10 1 OC 06/04/10 79-34-5 1.1.2.2-TETRACHLOROETHANE u ug/L 0.85 10 1 OC 06/04/10 127-18-4 TETRACHLOROETHENE u ug/L 0.4 10 1 OC 06/04/10 108-88-3 TOLUENE u ug/L 0.5 10 1 OC 06/04/10 87-61-6 1.2.3-TRICHLOROBENZENE u ug/L 0.23 10 1 OC 06/04/10 120-82-1 1.2.4-TRICHLOROBENZENE u ug/L 4.37 10 1 OC 06/04/10 71-55-6 1.1.1-TRICHLOROETHANE u ug/L 0.16 10 1 OC 06/04/10 79-00-5 1.1.2-TRICHLOROETHANE u ug/L 0.25 10 1 OC 06/04/10 79-01-6 TRICHLOROETHENE u ug/L 07 10 1 OC 06/04/10 75-69-4 TRICHLOROFLUOROMETHANE u ug/L 0.3 10 1 OC 06/04/10 96-18-4 1.2.3-TRICHLOROPROPANE u ug/L 0.33 10 1 OC 06/04/10 95-63-6 1.2.4-TRIM ETHYLBENZENE u ug/L 0.19 10 1 OC 06/04/10 108-67-8 1.3.5-TRIM ETHYLBENZENE u ug/L 0.29 10 1 OC 06/04/10 108-05-4 VINYL ACETATE u ug/L 20 50 1 OC 06/04/10 75-01-4 VINYL CHLORIDE u ug/L 0.3 10 1 OC 06/04/10 1330-20-7 m.p-XYLENE u ug/L 0.6 10 1 OC 06/04/10 95-47-6 o-XYLENE u ug/L 0.3 10 1 OC 06/04/10 460-00-4 BROMOFLUOROBENZENE 96.3 % 1 OC 06/04/10 1868-53-7 DIBROMOFLUOROMETHANE 103 % 1 OC 06/04/10 17060-07-0 1.2-DICHLOROETHANE-D4 107 % 1 OC 06/04/10 2037-26-5 T0LUENE-D8 98 % 1 OC 06/04/10 Client Sample ID: Fork Spring Laboratory Sample ID: 1006008-02 Date Sampled: 06/01/10 12:30 Sample Description: ATK-DLV- Groundwater Spring Sampling 2010 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TestMe^od: EPA 120.1 Conductivity CONDUCTIVITY 2150 uS/cm 0.3 1 1 JMM 06/11/10 Page 5 of 12 Printed: 06/16/10 11:21 Listing of Results by Sample Sample Delivery Group: 1006008 Client Sample ID: Fork Spring Sample Description: ATK-DLV- Groundwater Spring Sampling 2010 Laboratory Sample ID: 1006008-02 Date Sampled: 06/01/10 12:30 AS Number Test Parameter Result Units MDL EQL Dilution Factor Analyst Test Date TestMe^od: EPA 314.0 Perchlorate - Ion Chromatography 014797-73-0 PERCHLORATE u ug/L 1 4 1 JMM 06/11/10 TestMe^od: SW-846, 3010A Metals Digestion 3010A ACID DIGESTION 06/07/2010 12:00:00 am 1 MTB 06/08/10 TestMe^od: SlV-846, 6010B (Wafer) Metals Analysis by ICP - 6010 7440-38-2 ARSENIC U ug/L 20 100 1 MTB 06/07/10 7440-39-3 BARIUM 57.5 ug/L 2 10 1 MTB 06/07/10 7440-43-9 CADMIUM U ug/L 1 5 1 MTB 06/07/10 7440-47-3 CHROMIUM U ug/L 10 50 1 MTB 06/07/10 7440-48-4 COBALT U ug/L 1 5 1 MTB 06/07/10 7439-92-1 LEAD U ug/L 20 100 1 MTB 06/07/10 7439-98-7 MOLYBDENUM U ug/L 1 5 1 MTB 06/07/10 7782-49-2 SELENIUM U ug/L 30 150 1 MTB 06/07/10 7440-22-4 SILVER U ug/L 1 5 1 MTB 06/07/10 TestMe^od: SlV-846, 7470A Mercury Analysis 7439-97-6 MERCURY U ug/L 0.3 1 1 TCP 06/08/10 TestMe^od: SlV-846, 8260B (Water) Volatile Organic Analysis 67-64-1 ACETONE U ug/L 5 10 1 OC 06/04/10 71-43-2 BENZENE U ug/L 0.22 10 1 OC 06/04/10 74-97-5 BROMOCHLOROMETHANE U ug/L 0.31 10 1 OC 06/04/10 75-27-4 BROMODICHLOROMETHANE U ug/L 0.19 10 1 OC 06/04/10 108-86-1 BROMOBENZENE U ug/L 0.37 10 1 OC 06/04/10 75-25-2 BROMOFORM U ug/L 0.42 10 1 OC 06/04/10 74-83-9 BROMOMETHANE U ug/L 0.57 10 1 OC 06/04/10 78-93-3 2-BUTANONE U ug/L 1.11 10 1 OC 06/04/10 104-51-8 N-BUTYLBENZENE U ug/L 0.3 10 1 OC 06/04/10 135-98-8 SEC-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/04/10 98-06-6 TERT-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/04/10 75-15-0 CARBON DISULFIDE U ug/L 0.13 10 1 OC 06/04/10 56-23-5 CARBON TETRACHLORIDE U ug/L 0.27 10 1 OC 06/04/10 108-90-7 CHLOROBENZENE U ug/L 0.16 10 1 OC 06/04/10 75-00-3 CHLOROETHANE U ug/L 0.35 10 1 OC 06/04/10 110-75-8 2-CHLOROETHYLVINYL ETHER U ug/L 171 10 1 OC 06/04/10 67-66-3 CHLOROFORM u ug/L 0.3 10 1 OC 06/04/10 74-87-3 CHLOROMETHANE u ug/L 0.81 10 1 OC 06/04/10 95-49-8 2-CHLOROTOLUENE u ug/L 0.24 10 1 OC 06/04/10 106-43-4 4-CHLOROTOLUENE u ug/L 0.15 10 1 OC 06/04/10 124-48-1 DIBROMOCHLOROMETHANE u ug/L 0.18 10 1 OC 06/04/10 96-12-8 1.2-DIBROMO-3-CHLOROPROPANE u ug/L 0.35 10 1 OC 06/04/10 74-95-3 DIBROMOMETHANE u ug/L 0.25 10 1 OC 06/04/10 106-93-4 1.2-DIBROMOETHANE u ug/L 0.15 10 1 OC 06/04/10 95-50-1 1.2-DICHLOROBENZENE u ug/L 5.86 10 1 OC 06/04/10 541-73-1 1.3-DICHLOROBENZENE u ug/L 5.62 10 1 OC 06/04/10 106-46-7 1.4-DICHLOROBENZENE u ug/L 5.88 10 1 OC 06/04/10 75-71-8 DICHLORODIFLUOROMETHANE u ug/L 0.66 10 1 OC 06/04/10 75-34-3 1.1-DICHLOROETHANE u ug/L 0.49 10 1 OC 06/04/10 107-06-2 1.2-DICHLOROETHANE u ug/L 0.29 10 1 OC 06/04/10 75-35-4 1.1-DICHLOROETHENE u ug/L 0.16 10 1 OC 06/04/10 Page 6 of 12 Printed: 06/16/10 11:21 Listing of Results by Sample Sample Delivery Group: 1006008 Client Sample ID: Fork Spring Laboratory Sample ID: 1006008-02 Date Sampled: 06/01/10 12:30 Sample Description: ATK-DLV- Groundwater Spring Sampling 2010 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TestMe^od: SlV-846, 8260B (Water) Volatile Organic Analysis 156-59-4 CIS-1.2-DICHLOROETH ENE u ug/L 0.16 10 1 OC 06/04/10 156-60-5 TRANS-1.2-DICHLOROETH ENE u ug/L 0.34 10 1 OC 06/04/10 78-87-5 1.2-DICHLOROPROPANE u ug/L 0.16 10 1 OC 06/04/10 142-28-9 1.3-DICHLOROPROPANE u ug/L 0.24 10 1 OC 06/04/10 563-58-6 1.1-DICHLOROPROPENE u ug/L 0.17 10 1 OC 06/04/10 10061-01-5 CIS-1.3-DICHLOROPROPENE u ug/L 0.4 10 1 OC 06/04/10 10061-02-6 TRANS-1.3-DICHLOROPROPENE u ug/L 0.4 10 1 OC 06/04/10 590-20-7 2.2-DICHLOROPROPANE u ug/L 0.9 10 1 OC 06/04/10 100-41-4 ETHYLBENZENE u ug/L 0.16 10 1 OC 06/04/10 591-78-6 2-HEXANONE u ug/L 07 10 1 OC 06/04/10 87-68-3 HEXACHLOROBUTADIENE u ug/L 0.9 10 1 OC 06/04/10 98-82-8 ISOPROPYLBENZENE u ug/L 0.58 10 1 OC 06/04/10 99-87-6 4-ISOPROPYLTOLUENE u ug/L 0.24 10 1 OC 06/04/10 75-09-2 METHYLENE CHLORIDE u ug/L 0.8 10 1 OC 06/04/10 108-10-1 4-M ETHYL-2-PEN TAN ONE u ug/L 0.53 10 1 OC 06/04/10 91-20-3 NAPHTHALENE u ug/L 4 10 1 OC 06/04/10 103-65-1 N-PROPYLBENZENE u ug/L 0.5 10 1 OC 06/04/10 100-42-5 STYRENE u ug/L 0.3 10 1 OC 06/04/10 630-20-6 1.1.1.2-TETRACHLOROETHANE u ug/L 0.25 10 1 OC 06/04/10 79-34-5 1.1.2.2-TETRACHLOROETHANE u ug/L 0.85 10 1 OC 06/04/10 127-18-4 TETRACHLOROETHENE u ug/L 0.4 10 1 OC 06/04/10 108-88-3 TOLUENE u ug/L 0.5 10 1 OC 06/04/10 87-61-6 1.2.3-TRICHLOROBENZENE u ug/L 0.23 10 1 OC 06/04/10 120-82-1 1.2.4-TRICHLOROBENZENE u ug/L 4.37 10 1 OC 06/04/10 71-55-6 1.1.1-TRICHLOROETHANE u ug/L 0.16 10 1 OC 06/04/10 79-00-5 1.1.2-TRICHLOROETHANE u ug/L 0.25 10 1 OC 06/04/10 79-01-6 TRICHLOROETHENE u ug/L 07 10 1 OC 06/04/10 75-69-4 TRICHLOROFLUOROMETHANE u ug/L 0.3 10 1 OC 06/04/10 96-18-4 1.2.3-TRICHLOROPROPANE u ug/L 0.33 10 1 OC 06/04/10 95-63-6 1.2.4-TRIM ETHYLBENZENE u ug/L 0.19 10 1 OC 06/04/10 108-67-8 1.3.5-TRIM ETHYLBENZENE u ug/L 0.29 10 1 OC 06/04/10 108-05-4 VINYL ACETATE u ug/L 20 50 1 OC 06/04/10 75-01-4 VINYL CHLORIDE u ug/L 0.3 10 1 OC 06/04/10 1330-20-7 m.p-XYLENE u ug/L 0.6 10 1 OC 06/04/10 95-47-6 o-XYLENE u ug/L 0.3 10 1 OC 06/04/10 460-00-4 BROMOFLUOROBENZENE 97.5 % 1 OC 06/04/10 1868-53-7 DIBROMOFLUOROMETHANE 102 % 1 OC 06/04/10 17060-07-0 1.2-DICHLOROETHANE-D4 105 % 1 OC 06/04/10 2037-26-5 T0LUENE-D8 96.6 % 1 OC 06/04/10 Client Sample ID: Pipe Spring Laboratory Sample ID: 1006008-03 Date Sampled: 06/01/10 12:50 Sample Description: ATK-DLV- Groundwater Spring Sampling 2010 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TestMe^od: EPA 120.1 Conductivity CONDUCTIVITY 10800 uS/cm 0.3 1 1 JMM 06/11/10 TestMe^od: EPA 314.0 Perchlorate-Ion Chromatography 014797-73-0 PERCHLORATE 311. ug/L 10 40 10 JMM 06/11/10 Page / of 12 Printed: 06/16/10 11:21 Listing of Results by Sample Sample Delivery Group: 1006008 Client Sample ID: Pipe Spring Sample Description: ATK-DLV- Groundwater Spring Sampling 2010 Laboratory Sample ID: 1006008-03 Date Sampled: 06/01/10 12:50 CAS Number Test Parameter TestMe^od: SW-846,3010A Metals Digestion 3010A ACID DIGESTION 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7440-48-4 7439-92-1 7439- 98-7 7782-49-2 7440- 22-4 TestMe^od: 7439-97-6 TestMe^od: Result Units 06/07/2010 12:00:00 am MDL Dilution EQL Factor Analyst Test Date TestMe^od: SW-846, 6010B (Water) Metals Analysis by ICP - 6010 ARSENIC BARIUM CADMIUM CHROMIUM COBALT LEAD MOLYBDENUM SELENIUM SILVER SlV-846, 7470A MERCURY SlV-846, 8260B (Water) U 69.1 U U U U U U U ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 Mercury Analysis Volatile Organic Analysis U ug/1 67-64-1 ACETONE U ug/L 5 10 1 OC 06/04/10 71-43-2 BENZENE U ug/L 0.22 10 1 OC 06/04/10 74-97-5 BROMOCHLOROMETHANE U ug/L 0.31 10 1 OC 06/04/10 75-27-4 BROMODICHLOROMETHANE U ug/L 0.19 10 1 OC 06/04/10 108-86-1 BROMOBENZENE U ug/L 0.37 10 1 OC 06/04/10 75-25-2 BROMOFORM U ug/L 0.42 10 1 OC 06/04/10 74-83-9 BROMOMETHANE U ug/L 0.57 10 1 OC 06/04/10 78-93-3 2-BUTANONE U ug/L 1.11 10 1 OC 06/04/10 104-51-8 N-BUTYLBENZENE U ug/L 0.3 10 1 OC 06/04/10 135-98-8 SEC-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/04/10 98-06-6 TERT-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/04/10 75-15-0 CARBON DISULFIDE U ug/L 0.13 10 1 OC 06/04/10 56-23-5 CARBON TETRACHLORIDE U ug/L 0.27 10 1 OC 06/04/10 108-90-7 CHLOROBENZENE U ug/L 0.16 10 1 OC 06/04/10 75-00-3 CHLOROETHANE U ug/L 0.35 10 1 OC 06/04/10 110-75-8 2-CHLOROETHYLVINYL ETHER U ug/L 171 10 1 OC 06/04/10 67-66-3 CHLOROFORM U ug/L 0.3 10 1 OC 06/04/10 74-87-3 CHLOROMETHANE U ug/L 0.81 10 1 OC 06/04/10 95-49-8 2-CHLOROTOLUENE U ug/L 0.24 10 1 OC 06/04/10 106-43-4 4-CHLOROTOLUENE U ug/L 0.15 10 1 OC 06/04/10 124-48-1 DIBROMOCHLOROMETHANE U ug/L 0.18 10 1 OC 06/04/10 96-12-8 1.2-DIBROMO-3-CHLOROPROPANE U ug/L 0.35 10 1 OC 06/04/10 74-95-3 DIBROMOMETHANE U ug/L 0.25 10 1 OC 06/04/10 106-93-4 1.2-DIBROMOETHANE U ug/L 0.15 10 1 OC 06/04/10 95-50-1 1.2-DICHLOROBENZENE u ug/L 5.86 10 1 OC 06/04/10 541-73-1 1.3-DICHLOROBENZENE u ug/L 5.62 10 1 OC 06/04/10 106-46-7 1.4-DICHLOROBENZENE u ug/L 5.88 10 1 OC 06/04/10 75-71-8 DICHLORODIFLUOROMETHANE u ug/L 0.66 10 1 OC 06/04/10 75-34-3 1.1-DICHLOROETHANE u ug/L 0.49 10 1 OC 06/04/10 107-06-2 1.2-DICHLOROETHANE u ug/L 0.29 10 1 OC 06/04/10 75-35-4 1.1-DICHLOROETHENE u ug/L 0.16 10 1 OC 06/04/10 156-59-4 CIS-1.2-DICHLOROETH ENE u ug/L 0.16 10 1 OC 06/04/10 156-60-5 TRANS-1.2-DICHLOROETH ENE u ug/L 0.34 10 1 OC 06/04/10 78-87-5 1.2-DICHLOROPROPANE u ug/L 0.16 10 1 OC 06/04/10 Page 8 of 12 20 2 1 10 1 20 1 30 1 0.3 100 10 5 50 5 100 5 150 5 MTB MTB MTB MTB MTB MTB MTB MTB MTB MTB TCP 06/08/10 06/07/10 06/07/10 06/07/10 06/07/10 06/07/10 06/07/10 06/07/10 06/07/10 06/07/10 06/08/10 Printed: 06/16/10 11:21 Listing of Results by Sample Sample Delivery Group: 1006008 Client Sample ID: Pipe Spring Laboratory Sample ID: 1006008-03 Date Sampled: 06/01/10 12:50 Sample Description: ATK-DLV- Groundwater Spring Sampling 2010 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TestMe^od: SlV-846, 8260B (Water) Volatile Organic Analysis 142-28-9 1.3-DICHLOROPROPANE u ug/L 0.24 10 1 OC 06/04/10 563-58-6 1.1-DICHLOROPROPENE u ug/L 0.17 10 1 OC 06/04/10 10061-01-5 CIS-1.3-DICHLOROPROPENE u ug/L 0.4 10 1 OC 06/04/10 10061-02-6 TRANS-1.3-DICHLOROPROPENE u ug/L 0.4 10 1 OC 06/04/10 590-20-7 2.2-DICHLOROPROPANE u ug/L 0.9 10 1 OC 06/04/10 100-41-4 ETHYLBENZENE u ug/L 0.16 10 1 OC 06/04/10 591-78-6 2-HEXANONE u ug/L 07 10 1 OC 06/04/10 87-68-3 HEXACHLOROBUTADIENE u ug/L 0.9 10 1 OC 06/04/10 98-82-8 ISOPROPYLBENZENE u ug/L 0.58 10 1 OC 06/04/10 99-87-6 4-ISOPROPYLTOLUENE u ug/L 0.24 10 1 OC 06/04/10 75-09-2 METHYLENE CHLORIDE u ug/L 0.8 10 1 OC 06/04/10 108-10-1 4-M ETHYL-2-PEN TAN ONE u ug/L 0.53 10 1 OC 06/04/10 91-20-3 NAPHTHALENE u ug/L 4 10 1 OC 06/04/10 103-65-1 N-PROPYLBENZENE u ug/L 0.5 10 1 OC 06/04/10 100-42-5 STYRENE u ug/L 0.3 10 1 OC 06/04/10 630-20-6 1.1.1.2-TETRACHLOROETHANE u ug/L 0.25 10 1 OC 06/04/10 79-34-5 1.1.2.2-TETRACHLOROETHANE u ug/L 0.85 10 1 OC 06/04/10 127-18-4 TETRACHLOROETHENE u ug/L 0.4 10 1 OC 06/04/10 108-88-3 TOLUENE u ug/L 0.5 10 1 OC 06/04/10 87-61-6 1.2.3-TRICHLOROBENZENE u ug/L 0.23 10 1 OC 06/04/10 120-82-1 1.2.4-TRICHLOROBENZENE u ug/L 4.37 10 1 OC 06/04/10 71-55-6 1.1.1-TRICHLOROETHANE u ug/L 0.16 10 1 OC 06/04/10 79-00-5 1.1.2-TRICHLOROETHANE u ug/L 0.25 10 1 OC 06/04/10 79-01-6 TRICHLOROETHENE 6.2 J ug/L 07 10 1 OC 06/04/10 75-69-4 TRICHLOROFLUOROMETHANE u ug/L 0.3 10 1 OC 06/04/10 96-18-4 1.2.3-TRICHLOROPROPANE u ug/L 0.33 10 1 OC 06/04/10 95-63-6 1.2.4-TRIM ETHYLBENZENE u ug/L 0.19 10 1 OC 06/04/10 108-67-8 1.3.5-TRIM ETHYLBENZENE u ug/L 0.29 10 1 OC 06/04/10 108-05-4 VINYL ACETATE u ug/L 20 50 1 OC 06/04/10 75-01-4 VINYL CHLORIDE u ug/L 0.3 10 1 OC 06/04/10 1330-20-7 m.p-XYLENE u ug/L 0.6 10 1 OC 06/04/10 95-47-6 o-XYLENE u ug/L 0.3 10 1 OC 06/04/10 460-00-4 BROMOFLUOROBENZENE 97.9 % 1 OC 06/04/10 1868-53-7 DIBROMOFLUOROMETHANE 105 % 1 OC 06/04/10 17060-07-0 1.2-DICHLOROETHANE-D4 111 % 1 OC 06/04/10 2037-26-5 T0LUENE-D8 96.3 % 1 OC 06/04/10 Client Sample ID: Shot Gun Spring Laboratory Sample ID: 1006008-04 Date Sampled: 06/01/10 13:20 Sample Description: ATK-DLV- Groundwater Spring Sampling 2010 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TestMe^od: EPA 120.1 Conductivity CONDUCTIVITY 9500 uS/cm 0.3 1 1 JMM 06/11/10 TestMe^od: EPA 314.0 Perchlorate - Ion Chromatography 014797-73-0 PERCHLORATE 75. ug/L 10 40 10 JMM 06/11/10 TestMe^od: SlV-846, 3010A Metals Digestion 3010A ACID DIGESTION 06/07/2010 1 MTB 06/08/10 12:00:00 am Page 9 of 12 Printed: 06/16/10 11:21 Listing of Results by Sample Sample Delivery Group: 1006008 Client Sample ID: Shot Gun Spring Laboratory Sample ID: 1006008-04 Sample Description: ATK-DLV- Groundwater Spring Sampling 2010 Date Sampled: 06/01/10 13:20 CAS Number Test Parameter Result Units MDL EQL Dilution Factor Analyst Test Date TestMe^od: SlV-846, 6010B (Water) Metals Analysis by ICP -6010 7440-38-2 ARSENIC U ug/L 20 100 1 MTB 06/07/10 7440-39-3 BARIUM 80.6 ug/L 2 10 1 MTB 06/07/10 7440-43-9 CADMIUM U ug/L 1 5 1 MTB 06/07/10 7440-47-3 CHROMIUM U ug/L 10 50 1 MTB 06/07/10 7440-48-4 COBALT U ug/L 1 5 1 MTB 06/07/10 7439-92-1 LEAD U ug/L 20 100 1 MTB 06/07/10 7439-98-7 MOLYBDENUM U ug/L 1 5 1 MTB 06/07/10 7782-49-2 SELENIUM U ug/L 30 150 1 MTB 06/07/10 7440-22-4 SILVER U ug/L 1 5 1 MTB 06/07/10 TestMe^od: SlV-846, 7470A Mercury Analysis 7439-97-6 MERCURY U ug/L 0.3 1 1 TCP 06/08/10 TestMe^od: SlV-846, 8260B (Water) Volatile Organic Analysis 67-64-1 ACETONE U ug/L 5 10 1 OC 06/04/10 71-43-2 BENZENE U ug/L 0.22 10 1 OC 06/04/10 74-97-5 BROMOCHLOROMETHANE U ug/L 0.31 10 1 OC 06/04/10 75-27-4 BROMODICHLOROMETHANE U ug/L 0.19 10 1 OC 06/04/10 108-86-1 BROMOBENZENE U ug/L 0.37 10 1 OC 06/04/10 75-25-2 BROMOFORM U ug/L 0.42 10 1 OC 06/04/10 74-83-9 BROMOMETHANE U ug/L 0.57 10 1 OC 06/04/10 78-93-3 2-BUTANONE U ug/L 1.11 10 1 OC 06/04/10 104-51-8 N-BUTYLBENZENE U ug/L 0.3 10 1 OC 06/04/10 135-98-8 SEC-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/04/10 98-06-6 TERT-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/04/10 75-15-0 CARBON DISULFIDE U ug/L 0.13 10 1 OC 06/04/10 56-23-5 CARBON TETRACHLORIDE U ug/L 0.27 10 1 OC 06/04/10 108-90-7 CHLOROBENZENE U ug/L 0.16 10 1 OC 06/04/10 75-00-3 CHLOROETHANE u ug/L 0.35 10 1 OC 06/04/10 110-75-8 2-CHLOROETHYLVINYL ETHER u ug/L 171 10 1 OC 06/04/10 67-66-3 CHLOROFORM u ug/L 0.3 10 1 OC 06/04/10 74-87-3 CHLOROMETHANE u ug/L 0.81 10 1 OC 06/04/10 95-49-8 2-CHLOROTOLUENE u ug/L 0.24 10 1 OC 06/04/10 106-43-4 4-CHLOROTOLUENE u ug/L 0.15 10 1 OC 06/04/10 124-48-1 DIBROMOCHLOROMETHANE u ug/L 0.18 10 1 OC 06/04/10 96-12-8 1.2-DIBROMO-3-CHLOROPROPANE u ug/L 0.35 10 1 OC 06/04/10 74-95-3 DIBROMOMETHANE u ug/L 0.25 10 1 OC 06/04/10 106-93-4 1.2-DIBROMOETHANE u ug/L 0.15 10 1 OC 06/04/10 95-50-1 1.2-DICHLOROBENZENE u ug/L 5.86 10 1 OC 06/04/10 541-73-1 1.3-DICHLOROBENZENE u ug/L 5.62 10 1 OC 06/04/10 106-46-7 1.4-DICHLOROBENZENE u ug/L 5.88 10 1 OC 06/04/10 75-71-8 DICHLORODIFLUOROMETHANE u ug/L 0.66 10 1 OC 06/04/10 75-34-3 1.1-DICHLOROETHANE u ug/L 0.49 10 1 OC 06/04/10 107-06-2 1.2-DICHLOROETHANE u ug/L 0.29 10 1 OC 06/04/10 75-35-4 1.1-DICHLOROETHENE u ug/L 0.16 10 1 OC 06/04/10 156-59-4 CIS-1.2-DICHLOROETH ENE u ug/L 0.16 10 1 OC 06/04/10 156-60-5 TRANS-1.2-DICHLOROETH ENE u ug/L 0.34 10 1 OC 06/04/10 78-87-5 1.2-DICHLOROPROPANE u ug/L 0.16 10 1 OC 06/04/10 142-28-9 1.3-DICHLOROPROPANE u ug/L 0.24 10 1 OC 06/04/10 563-58-6 1.1-DICHLOROPROPENE u ug/L 0.17 10 1 OC 06/04/10 10061-01-5 CIS-1.3-DICHLOROPROPENE u ug/L 0.4 10 1 OC 06/04/10 Page 10 of 12 Printed: 06/16/10 11:21 Listing of Results by Sample Sample Delivery Group: 1006008 Client Sample ID: Shot Gun Spring Laboratory Sample ID: 1006008-04 Sample Description: ATK-DLV- Groundwater Spring Sampling 2010 Date Sampled: 06/01/10 13:20 CAS Number Test Parameter Result Units MDL Dilution EQL Factor Analyst Test Date TestMe^od: SlV-846, 8260B (Water) Volatile Organic Analysis 10061-02-6 TRANS-1.3-DICHLOROPROPENE u ug/L 0.4 10 1 OC 06/04/10 590-20-7 2.2-DICHLOROPROPANE u ug/L 0.9 10 1 OC 06/04/10 100-41-4 ETHYLBENZENE u ug/L 0.16 10 1 OC 06/04/10 591-78-6 2-HEXANONE u ug/L 07 10 1 OC 06/04/10 87-68-3 HEXACHLOROBUTADIENE u ug/L 0.9 10 1 OC 06/04/10 98-82-8 ISOPROPYLBENZENE u ug/L 0.58 10 1 OC 06/04/10 99-87-6 4-ISOPROPYLTOLUENE u ug/L 0.24 10 1 OC 06/04/10 75-09-2 METHYLENE CHLORIDE u ug/L 0.8 10 1 OC 06/04/10 108-10-1 4-M ETHYL-2-PEN TAN ONE u ug/L 0.53 10 1 OC 06/04/10 91-20-3 NAPHTHALENE u ug/L 4 10 1 OC 06/04/10 103-65-1 N-PROPYLBENZENE u ug/L 0.5 10 1 OC 06/04/10 100-42-5 STYRENE u ug/L 0.3 10 1 OC 06/04/10 630-20-6 1.1.1.2-TETRACHLOROETHANE u ug/L 0.25 10 1 OC 06/04/10 79-34-5 1.1.2.2-TETRACHLOROETHANE u ug/L 0.85 10 1 OC 06/04/10 127-18-4 TETRACHLOROETHENE u ug/L 0.4 10 1 OC 06/04/10 108-88-3 TOLUENE u ug/L 0.5 10 1 OC 06/04/10 87-61-6 1.2.3-TRICHLOROBENZENE u ug/L 0.23 10 1 OC 06/04/10 120-82-1 1.2.4-TRICHLOROBENZENE u ug/L 4.37 10 1 OC 06/04/10 71-55-6 1.1.1-TRICHLOROETHANE u ug/L 0.16 10 1 OC 06/04/10 79-00-5 1.1.2-TRICHLOROETHANE u ug/L 0.25 10 1 OC 06/04/10 79-01-6 TRICHLOROETHENE 5.1 J ug/L 07 10 1 OC 06/04/10 75-69-4 TRICHLOROFLUOROMETHANE u ug/L 0.3 10 1 OC 06/04/10 96-18-4 1.2.3-TRICHLOROPROPANE u ug/L 0.33 10 1 OC 06/04/10 95-63-6 1.2.4-TRIM ETHYLBENZENE u ug/L 0.19 10 1 OC 06/04/10 108-67-8 1.3.5-TRIM ETHYLBENZENE u ug/L 0.29 10 1 OC 06/04/10 108-05-4 VINYL ACETATE u ug/L 20 50 1 OC 06/04/10 75-01-4 VINYL CHLORIDE u ug/L 0.3 10 1 OC 06/04/10 1330-20-7 m.p-XYLENE u ug/L 0.6 10 1 OC 06/04/10 95-47-6 o-XYLENE u ug/L 0.3 10 1 OC 06/04/10 460-00-4 BROMOFLUOROBENZENE 97.9 % 1 OC 06/04/10 1868-53-7 DIBROMOFLUOROMETHANE 104 % 1 OC 06/04/10 17060-07-0 1.2-DICHLOROETHANE-D4 110 % 1 OC 06/04/10 2037-26-5 T0LUENE-D8 97.4 % 1 OC 06/04/10 Page 11 of 12 Printed: 06/16/10 11:21 Data Reporting Qualifiers U Indicates that the analyte concentration is less than the MDL. B This flag is used when an analyte is found in the blank as well as the sample. Indicates an extimated value. This flag is used either when estimating a concentration for tentatively identified compounds or when the data indicated the presence of a compound that meets the identification criteria but the result is less than the EQL (e.g. 3 J with an EQL of 10). MDL Method Detection Limit: The minimum concentration of a substance that can be confidently measured and reported. The laboratory has demonstrated that the MDL can be achieved in a laboratory reagent blank, but does not guarantee it can be achieved in all sample matrices. EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many analytes the EQL is selected as the value of the lowest standard in the calibration cuh/e. Dilution Dilution Factor: The prepared sample was diluted by this factor because the Factor sample was too concentrated or due to other interferences in the sample matrix. Any dilution factor causes a corresponding increase in the MDL and EQL. Page 12 of 12 Printed: 06/16/10 11:21 ATK Launch Systems Environmental Laboratory Client Name: Sample Receipt Checklist • /]rT\C LAuLi^ ^^<^h^< - V SDG No. Camer: • Hand delivered, no cooler Carrier Number: • Hand delivered, sample(s) taken out at receiving counter Cooler information: Cooler Number/ID: Condition of Shipping Container: Cooler Sealed (taped): Custody Seals Present: jj^ood •Yes •Yes •Intact •Fair •Broken •Blue Ice nNone •Not Applicable •Not Applicable •Not Applicable •Damaged (explain). Coolant: State of Coolant: •Frozen partially Frozen Thermometer ID: Reading: / °C CF:_ Seal Number:, Other:__ •Melted Corrected Temp:_ Temp Blank Included: •Yes •No Packing Description: Chain-Of-Custody Information: COC Present: r lO t * COC Numberfs): ^ / 5 / US' COC signed (relinquished and received): COC or LWI agrees with sample labels: pVes •p^es S^es •No •No •No Other: •Not Applicable •Not Applicable Notes: Sample Information: Samples included in cooler: Custody Seals Present: Sample containers intact: Samples in proper containers: Sufficient sample volume: All samples received in hold time: jJtVes Water - VOA's have zero headspace: ;2(Pre-preserved with HCI: Notes: •Yes •Intact ^es 4Ves j2^o •Broken •tslo •No •No •No Other Seal Number(s) _ Notes: (Jrt'es •No •Not Applicable Qpre-preserved with NajSzOs: •Non-Preserved: Water - pH acceptable upon receipt: HNO3 ,H2S04 = ;ayes •Adjusted (see comments below) •Not Applicable NaOH = ^ZnAC /NaOH =. HCL = Water - pH adjusted: (mfg. & Lot No.) HNO3 H2SO4, NazSOzOa Other „ Notes: NaOH_ ZnAC HCI SOP-102 Form A 1006008 ENVIRONMENTAL LAB WORK REQUEST TO ATK LAUNCH SYSTEMS ENVIRONMENTAL LABORATORY LWR No. E13164 Login No. FROM: EXTENSION: COST CENTER: WORK ORDER: DATE: Allen Lee 25688 8200 988P LS333 6/1/2010 GW ORGANIZATION: Environmental Services MAIL STOP: 301 REPORT RESULTS TO: HELEN RAVSTEN, MS 301 SAMPLE INFORMATION SAMPLE DATE TYPE LOCATION TIME TEST REMARKS SAMPLE DATE G C LOCATION TIME TEST REMARKS Conner Spring 6/1/10 X Promontory 1200 See Attached Analytical Request Fork Spring 6/1/10 X Promontory 1230 See Attached Analytical Request Pipe Spring 6/1/10 X Promontory 1250 See Attached Analytical Request Shot Gun Spring 6/1/10 X Promontory 1320 See Attached Analytical Request CHAIN OF CUSTODY RELINQUISHED BY DATE TIME RECEIVED BY DATE TIME FOR LABORATORY USE ONLY DATE COMPLETED DATE REPORTED SIGNATURE SAMPLE NUMBER: Sffi^<^ 2010 Spring GW Sampling ATK Laxanch Systems^ Inc. Promontory-/ UTAH (801) 251-5688 DATE: SAMPLER: 1006008 ANALYTICAL LABORATORY: ATK Environmental Laboratory M53 Bottle Number No. of Containers Fid. Preservative/ Treatment Recjuested Analysis 11 3 4 degrees C Acidified .2 mL HCL VOA, Appendix 9 Method 8260 4T 1 5 mL HN03 As, Ba, Cd, Cr, Pb, Hg, Se, Ag Mo, Co EPA Method 6010 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314.0 SAMPLE NUMBER: SpU^ 2010 Spring GW Sampling ATK Laiinch Systems/ Inc. Promontory, UTAH (801) 251-5688 DATE: /0 SAMPLER: 1006008 ANALYTICAL LABORATORY: ATK Environmental Laboratory M53 Bottle Number No. of Containers Fid. Preservative/ Treatment Requested Analysis 11 3 4 degrees C Acidified .2 mL HCL VOA, Appendix 9 Method 8260 4T 1 5 mL HN03 As, Ba, Cd, Cr, Pb, Hg, Se, Ag Mo, Co EPA Method 6010 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314.0 SAMPLE NUMBER: C^r<M^ 2010 Spring GW Sampling ATK Launch Systems, Inc. Promontory, UTAH (801) 251-5688 DATE SAMPLER: 1006008 ANALYTICAL LABORATORY: ATK Environmental Laboratory MS3 Bottle Number No. of Containers Fid. Preservative/ Treatment Requested Analysis 11 3 4 degrees C Acidified .2 mL HCL VOA, Appendix 9 Method 8260 4T 1 5 mL HN03 As, Ba, Cd, Cr, Pb, Hg, Se, Ag Mo, Co EPA Method 6010 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314.0 2010 Spring GW Sampling ATK Launch Systems, Inc. Promontory, UTAH , , (801) 251-5688 SAMPLE NUMBER: ^K'Wi^ DATE SAMPLER: 1006008 ANALYTICAL LABORATORY: ATK Environmental Laboratory MS3 Bottle Number No. of Containers Fid. Preservative/ Treatment Requested Analysis 11 3 4 degrees C Acidified .2 mL HCL VOA, Appendix 9 Method 8260 4T 1 5 mL HN03 As, Ba, Cd, Cr, Pb, Hg, Se, Ag Mo, Co EPA Method 6010 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314.0 988P LS333 GW CERTIFICATE OF ANALYSIS Listing of Sample Information and Testing Requested Wednesday, June 16, 2010 TESTED FOR: ATK: DLV Environmental Monitoring Thiokol Corp, UT 84322 ANALYZED BY: ATK Launch Systems Analytical Chemistry Laboratory P.O. Box 707, M/S 245 Brigham City, UT 84302-0707 435-863-3732 435-863-8080 Contact Name: Project: Sample Delivery Group: Al Lee Ground Water Testing - DLV 1006009 Page 1 of 11 Printed: 06/16/10 11:23 Sample Delivery Group: 1006009 Sample No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 1006009-01 D-5 06/03/10 6/2/2010 14:40:59 EPA 120.1 EPA 314.0 SW-846. 8260B (Water) Conductivity Perchlorate - Ion Chromatography Volatile Organic Analysis Water Water Water 1006009-02 D-4 06/03/10 6/2/2010 15:20:59 EPA 120.1 EPA 314.0 SW-846. 8260B (Water) Conductivity Perchlorate - Ion Chromatography Volatile Organic Analysis Water Water Water 1006009-03 LF-1 06/03/10 6/2/2010 16:30:59 EPA 120.1 EPA 314.0 SW-846. 8260B (Water) Conductivity Perchlorate - Ion Chromatography Volatile Organic Analysis Water Water Water 1006009-04 B-3 06/03/10 6/2/2010 17:30:59 EPA 120.1 EPA 314.0 SW-846. 8260B (Water) SW-846. 8330A Conductivity Perchlorate - Ion Chromatography Volatile Organic Analysis Explosives Extraction Water Water Water Water Page 2 of 11 Printed: 06/16/10 11:23 Sample Delivery Group: 1006009 Sample No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 1006009-04 B-3 06/03/10 6/2/2010 17:30:59 SW-846. 8330A Mod (Water) Explosives Analysis Water Certified By: 06/17/2010 W. Scott Fraser, Quality Assurance Officer Date This ceiiifies that the following data meets the requirements of the National Environmental Laboratory Accreditation Program (NELAP) unless otherwise annotated: Page 3 of 11 Printed: 06/16/10 11:23 Listing of Results by Sample Sample Delivery Group: 1006009 Client Sample ID: D-5 Sample Description: ATK-DLV - Groundwater Spring 2010 Laboratory Sample ID: 1006009-01 Date Sampled: 06/02/10 14:40 AS Number Test Parameter Result Units MDL EQL Dilution Factor Analvst Test Date TestMe^od: EPA 120.1 Conductivity CONDUCTIVITY 1950 uS/cm 0.3 1 1 JMM 06/14/10 TestMe^od: EPA 314.0 Perchlorate-Ion Chromatography 014797-73-0 PERCHLORATE 200000. ug/L 1000 4000 1000 JMM 06/15/10 TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 67-64-1 ACETONE U ug/L 50 100 10 OC 06/04/10 71-43-2 BENZENE U ug/L 2.2 100 10 OC 06/04/10 74-97-5 BROMOCHLOROMETHANE U ug/L 3.1 100 10 OC 06/04/10 75-27-4 BROMODICHLOROMETHANE U ug/L 1.9 100 10 OC 06/04/10 108-86-1 BROMOBENZENE U ug/L 3.7 100 10 OC 06/04/10 75-25-2 BROMOFORM U ug/L 4.2 100 10 OC 06/04/10 74-83-9 BROMOMETHANE U ug/L 5.7 100 10 OC 06/04/10 78-93-3 2-BUTANONE U ug/L 11.1 100 10 OC 06/04/10 104-51-8 N-BUTYLBENZENE U ug/L 3 100 10 OC 06/04/10 135-98-8 SEC-BUTYLBENZENE U ug/L 4 100 10 OC 06/04/10 98-06-6 TERT-BUTYLBENZENE U ug/L 4 100 10 OC 06/04/10 75-15-0 CARBON DISULFIDE U ug/L 1.3 100 10 OC 06/04/10 56-23-5 CARBON TETRACHLORIDE U ug/L 2.7 100 10 OC 06/04/10 108-90-7 CHLOROBENZENE U ug/L 1.6 100 10 OC 06/04/10 75-00-3 CHLOROETHANE U ug/L 3.5 100 10 OC 06/04/10 110-75-8 2-CHLOROETHYLVINYL ETHER U ug/L 17.1 100 10 OC 06/04/10 67-66-3 CHLOROFORM U ug/L 3 100 10 OC 06/04/10 74-87-3 CHLOROMETHANE U ug/L 8.1 100 10 OC 06/04/10 95-49-8 2-CHLOROTOLUENE U ug/L 2.4 100 10 OC 06/04/10 106-43-4 4-CHLOROTOLUENE U ug/L 1.5 100 10 OC 06/04/10 124-48-1 DIBROMOCHLOROMETHANE U ug/L 1.8 100 10 OC 06/04/10 96-12-8 1.2-DIBROMO-3-CHLOROPROPANE U ug/L 3.5 100 10 OC 06/04/10 74-95-3 DIBROMOMETHANE U ug/L 2.5 100 10 OC 06/04/10 106-93-4 1.2-DIBROMOETHANE u ug/L 1.5 100 10 OC 06/04/10 95-50-1 1.2-DICHLOROBENZENE u ug/L 58.6 100 10 OC 06/04/10 541-73-1 1.3-DICHLOROBENZENE u ug/L 56.2 100 10 OC 06/04/10 106-46-7 1.4-DICHLOROBENZENE u ug/L 58.8 100 10 OC 06/04/10 75-71-8 DICHLORODIFLUOROMETHANE u ug/L 6.6 100 10 OC 06/04/10 75-34-3 1.1-DICHLOROETHANE u ug/L 4.9 100 10 OC 06/04/10 107-06-2 1.2-DICHLOROETHANE u ug/L 2.9 100 10 OC 06/04/10 75-35-4 1.1-DICHLOROETHENE 6.2 J ug/L 1.6 100 10 OC 06/04/10 156-59-4 CIS-1.2-DICHLOROETH ENE U ug/L 1.6 100 10 OC 06/04/10 156-60-5 TRANS-1.2-DICHLOROETH ENE U ug/L 3.4 100 10 OC 06/04/10 78-87-5 1.2-DICHLOROPROPANE U ug/L 1.6 100 10 OC 06/04/10 142-28-9 1.3-DICHLOROPROPANE U ug/L 2.4 100 10 OC 06/04/10 563-58-6 1.1-DICHLOROPROPENE U ug/L 1.7 100 10 OC 06/04/10 10061-01-5 CIS-1.3-DICHLOROPROPENE U ug/L 4 100 10 OC 06/04/10 10061-02-6 TRANS-1.3-DICHLOROPROPENE u ug/L 4 100 10 OC 06/04/10 590-20-7 2.2-DICHLOROPROPANE u ug/L 9 100 10 OC 06/04/10 100-41-4 ETHYLBENZENE u ug/L 1.6 100 10 OC 06/04/10 591-78-6 2-HEXANONE u ug/L 7 100 10 OC 06/04/10 87-68-3 HEXACHLOROBUTADIENE u ug/L 9 100 10 OC 06/04/10 98-82-8 ISOPROPYLBENZENE u ug/L 5.8 100 10 OC 06/04/10 99-87-6 4-ISOPROPYLTOLUENE u ug/L 2.4 100 10 OC 06/04/10 75-09-2 METHYLENE CHLORIDE u ug/L 8 100 10 OC 06/04/10 Page 4 of 11 Printed: 06/16/10 11:23 Listing of Results by Sample Sample Delivery Group: 1006009 Client Sample ID: D-5 Sample Description: ATK-DLV - Groundwater Spring 2010 Laboratory Sample ID: 1006009-01 Date Sampled: 06/02/10 14:40 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analvst Test Date TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 108-10-1 4-M ETHYL-2-PEN TAN ONE U ug/L 5.3 100 10 OC 06/04/10 91-20-3 NAPHTHALENE U ug/L 40 100 10 OC 06/04/10 103-65-1 N-PROPYLBENZENE U ug/L 5 100 10 OC 06/04/10 100-42-5 STYRENE U ug/L 3 100 10 OC 06/04/10 630-20-6 1.1.1.2-TETRACHLOROETHANE U ug/L 2.5 100 10 OC 06/04/10 79-34-5 1.1.2.2-TETRACHLOROETHANE U ug/L 8.5 100 10 OC 06/04/10 127-18-4 TETRACHLOROETHENE U ug/L 4 100 10 OC 06/04/10 108-88-3 TOLUENE U ug/L 5 100 10 OC 06/04/10 87-61-6 1.2.3-TRICHLOROBENZENE U ug/L 2.3 100 10 OC 06/04/10 120-82-1 1.2.4-TRICHLOROBENZENE U ug/L 43.7 100 10 OC 06/04/10 71-55-6 1.1.1-TRICHLOROETHANE U ug/L 1.6 100 10 OC 06/04/10 79-00-5 1.1.2-TRICHLOROETHANE U ug/L 2.5 100 10 OC 06/04/10 79-01-6 TRICHLOROETHENE 340 ug/L 7 100 10 OC 06/04/10 75-69-4 TRICHLOROFLUOROMETHANE U ug/L 3 100 10 OC 06/04/10 96-18-4 1.2.3-TRICHLOROPROPANE U ug/L 3.3 100 10 OC 06/04/10 95-63-6 1.2.4-TRIM ETHYLBENZENE U ug/L 1.9 100 10 OC 06/04/10 108-67-8 1.3.5-TRIM ETHYLBENZENE U ug/L 2.9 100 10 OC 06/04/10 108-05-4 VINYL ACETATE U ug/L 200 500 10 OC 06/04/10 75-01-4 VINYL CHLORIDE U ug/L 3 100 10 OC 06/04/10 1330-20-7 m.p-XYLENE U ug/L 6 100 10 OC 06/04/10 95-47-6 o-XYLENE U ug/L 3 100 10 OC 06/04/10 460-00-4 BROMOFLUOROBENZENE 93.7 % 10 OC 06/04/10 1868-53-7 DIBROMOFLUOROMETHANE 105 % 10 OC 06/04/10 17060-07-0 1.2-DICHLOROETHANE-D4 110 % 10 OC 06/04/10 2037-26-5 T0LUENE-D8 95.2 % 10 OC 06/04/10 Client Sample ID: D-4 Laboratory Sample ID: 1006009-02 Date Sampled: 06/02/10 15:20 Sample Description: ATK-DLV - Groundwater Spring 2010 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analvst Test Date TestMe^od: EPA 120.1 Conductivity CONDUCTIVITY 1340 uS/cm 0.3 1 1 JMM 06/14/10 TestMe^od: EPA 314.0 Perchlorate - Ion Chromatography 014797-73-0 PERCHLORATE 135000. ug/L 1000 4000 1000 JMM 06/15/10 TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 67-64-1 ACETONE U ug/L 5 10 1 OC 06/04/10 71-43-2 BENZENE U ug/L 0.22 10 1 OC 06/04/10 74-97-5 BROMOCHLOROMETHANE U ug/L 0.31 10 1 OC 06/04/10 75-27-4 BROMODICHLOROMETHANE U ug/L 0.19 10 1 OC 06/04/10 108-86-1 BROMOBENZENE U ug/L 0.37 10 1 OC 06/04/10 75-25-2 BROMOFORM U ug/L 0.42 10 1 OC 06/04/10 74-83-9 BROMOMETHANE U ug/L 0.57 10 1 OC 06/04/10 78-93-3 2-BUTANONE U ug/L 1.11 10 1 OC 06/04/10 104-51-8 N-BUTYLBENZENE U ug/L 0.3 10 1 OC 06/04/10 135-98-8 SEC-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/04/10 98-06-6 TERT-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/04/10 75-15-0 CARBON DISULFIDE U ug/L 0.13 10 1 OC 06/04/10 Page 5 of 11 Printed: 06/16/10 11:23 Listing of Results by Sample Sample Delivery Group: 1006009 Client Sample ID: D-4 Laboratory Sample ID: 1006009-02 Sample Description: ATK-DLV - Groundwater Spring 2010 Date Sampled: 06/02/10 15:20 CAS Number Test Parameter Result Units MDL Dilution EQL Factor Analyst Test Date TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 56-23-5 CARBON TETRACHLORIDE 2.2 J ug/L 0.27 10 1 OC 06/04/10 108-90-7 CHLOROBENZENE U ug/L 0.16 10 1 OC 06/04/10 75-00-3 CHLOROETHANE U ug/L 0.35 10 1 OC 06/04/10 110-75-8 2-CHLOROETHYLVINYL ETHER U ug/L 1.71 10 1 OC 06/04/10 67-66-3 CHLOROFORM 1.7 J ug/L 0.3 10 1 OC 06/04/10 74-87-3 CHLOROMETHANE U ug/L 0.81 10 1 OC 06/04/10 95-49-8 2-CHLOROTOLUENE U ug/L 0.24 10 1 OC 06/04/10 106-43-4 4-CHLOROTOLUENE U ug/L 0.15 10 1 OC 06/04/10 124-48-1 DIBROMOCHLOROMETHANE U ug/L 0.18 10 1 OC 06/04/10 96-12-8 1.2-DIBROMO-3-CHLOROPROPANE U ug/L 0.35 10 1 OC 06/04/10 74-95-3 DIBROMOMETHANE U ug/L 0.25 10 1 OC 06/04/10 106-93-4 1.2-DIBROMOETHANE U ug/L 0.15 10 1 OC 06/04/10 95-50-1 1.2-DICHLOROBENZENE U ug/L 5.86 10 1 OC 06/04/10 541-73-1 1.3-DICHLOROBENZENE U ug/L 5.62 10 1 OC 06/04/10 106-46-7 1.4-DICHLOROBENZENE U ug/L 5.88 10 1 OC 06/04/10 75-71-8 DICHLORODIFLUOROMETHANE U ug/L 0.66 10 1 OC 06/04/10 75-34-3 1.1-DICHLOROETHANE U ug/L 0.49 10 1 OC 06/04/10 107-06-2 1.2-DICHLOROETHANE U ug/L 0.29 10 1 OC 06/04/10 75-35-4 1.1-DICHLOROETHENE 11.4 ug/L 0.16 10 1 OC 06/04/10 156-59-4 CIS-1.2-DICHLOROETH ENE U ug/L 0.16 10 1 OC 06/04/10 156-60-5 TRANS-1.2-DICHLOROETH ENE U ug/L 0.34 10 1 OC 06/04/10 78-87-5 1.2-DICHLOROPROPANE U ug/L 0.16 10 1 OC 06/04/10 142-28-9 1.3-DICHLOROPROPANE U ug/L 0.24 10 1 OC 06/04/10 563-58-6 1.1-DICHLOROPROPENE U ug/L 0.17 10 1 OC 06/04/10 10061-01-5 CIS-1.3-DICHLOROPROPENE U ug/L 0.4 10 1 OC 06/04/10 10061-02-6 TRANS-1.3-DICHLOROPROPENE U ug/L 0.4 10 1 OC 06/04/10 590-20-7 2.2-DICHLOROPROPANE U ug/L 0.9 10 1 OC 06/04/10 100-41-4 ETHYLBENZENE U ug/L 0.16 10 1 OC 06/04/10 591-78-6 2-HEXANONE U ug/L 0.7 10 1 OC 06/04/10 87-68-3 HEXACHLOROBUTADIENE U ug/L 0.9 10 1 OC 06/04/10 98-82-8 ISOPROPYLBENZENE U ug/L 0.58 10 1 OC 06/04/10 99-87-6 4-ISOPROPYLTOLUENE U ug/L 0.24 10 1 OC 06/04/10 75-09-2 METHYLENE CHLORIDE U ug/L 0.8 10 1 OC 06/04/10 108-10-1 4-M ETHYL-2-PEN TAN ONE u ug/L 0.53 10 1 OC 06/04/10 91-20-3 NAPHTHALENE u ug/L 4 10 1 OC 06/04/10 103-65-1 N-PROPYLBENZENE u ug/L 0.5 10 1 OC 06/04/10 100-42-5 STYRENE u ug/L 0.3 10 1 OC 06/04/10 630-20-6 1.1.1.2-TETRACHLOROETHANE u ug/L 0.25 10 1 OC 06/04/10 79-34-5 1.1.2.2-TETRACHLOROETHANE u ug/L 0.85 10 1 OC 06/04/10 127-18-4 TETRACHLOROETHENE u ug/L 0.4 10 1 OC 06/04/10 108-88-3 TOLUENE u ug/L 0.5 10 1 OC 06/04/10 87-61-6 1.2.3-TRICHLOROBENZENE u ug/L 0.23 10 1 OC 06/04/10 120-82-1 1.2.4-TRICHLOROBENZENE u ug/L 4.37 10 1 OC 06/04/10 71-55-6 1.1.1-TRICHLOROETHANE 2.1 J ug/L 0.16 10 1 OC 06/04/10 79-00-5 1.1.2-TRICHLOROETHANE u ug/L 0.25 10 1 OC 06/04/10 79-01-6 TRICHLOROETHENE 40.8 ug/L 0.7 10 1 OC 06/04/10 75-69-4 TRICHLOROFLUOROMETHANE 0.8 J ug/L 0.3 10 1 OC 06/04/10 96-18-4 1.2.3-TRICHLOROPROPANE U ug/L 0.33 10 1 OC 06/04/10 95-63-6 1.2.4-TRIM ETHYLBENZENE U ug/L 0.19 10 1 OC 06/04/10 108-67-8 1.3.5-TRIM ETHYLBENZENE U ug/L 0.29 10 1 OC 06/04/10 Page 6 of 11 Printed: 06/16/10 11:23 Listing of Results by Sample Sample Delivery Group: 1006009 Client Sample ID: D-4 Sample Description: ATK-DLV - Groundwater Spring 2010 Laboratory Sample ID: 1006009-02 Date Sampled: 06/02/10 15:20 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analvst Test Date TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 108-05-4 VINYL ACETATE u ug/L 20 50 1 OC 06/04/10 75-01-4 VINYL CHLORIDE u ug/L 0.3 10 1 OC 06/04/10 1330-20-7 m.p-XYLENE u ug/L 0.6 10 1 OC 06/04/10 95-47-6 o-XYLENE u ug/L 0.3 10 1 OC 06/04/10 460-00-4 BROMOFLUOROBENZENE 99 % 1 OC 06/04/10 1868-53-7 DIBROMOFLUOROMETHANE 101 % 1 OC 06/04/10 17060-07-0 1.2-DICHLOROETHANE-D4 105 % 1 OC 06/04/10 2037-26-5 T0LUENE-D8 96.3 % 1 OC 06/04/10 Client Sample ID: LF-1 Sample Description: ATK-DLV - Groundwater Spring 2010 Laboratory Sample ID: 1006009-03 Date Sampled: 06/02/10 16:30 Dilution CAS Number Test Parameter Result Units MDL EQL TestMe^od: EPA 120.1 Conductivity CONDUCTIVITY 8180 uS/cm 0.3 1 1 JMM 06/14/10 TestMe^od: EPA 314.0 Perchlorate - Ion Chromatography 014797-73-0 PERCHLORATE 489. ug/L 10 40 10 JMM 06/15/10 TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 67-64-1 ACETONE U ug/L 5 10 1 OC 06/04/10 71-43-2 BENZENE U ug/L 0.22 10 1 OC 06/04/10 74-97-5 BROMOCHLOROMETHANE U ug/L 0.31 10 1 OC 06/04/10 75-27-4 BROMODICHLOROMETHANE U ug/L 0.19 10 1 OC 06/04/10 108-86-1 BROMOBENZENE U ug/L 0.37 10 1 OC 06/04/10 75-25-2 BROMOFORM U ug/L 0.42 10 1 OC 06/04/10 74-83-9 BROMOMETHANE U ug/L 0.57 10 1 OC 06/04/10 78-93-3 2-BUTANONE U ug/L 1.11 10 1 OC 06/04/10 104-51-8 N-BUTYLBENZENE U ug/L 0.3 10 1 OC 06/04/10 135-98-8 SEC-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/04/10 98-06-6 TERT-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/04/10 75-15-0 CARBON DISULFIDE U ug/L 0.13 10 1 OC 06/04/10 56-23-5 CARBON TETRACHLORIDE U ug/L 0.27 10 1 OC 06/04/10 108-90-7 CHLOROBENZENE U ug/L 0.16 10 1 OC 06/04/10 75-00-3 CHLOROETHANE U ug/L 0.35 10 1 OC 06/04/10 110-75-8 2-CHLOROETHYLVINYL ETHER U ug/L 1.71 10 1 OC 06/04/10 67-66-3 CHLOROFORM U ug/L 0.3 10 1 OC 06/04/10 74-87-3 CHLOROMETHANE U ug/L 0.81 10 1 OC 06/04/10 95-49-8 2-CHLOROTOLUENE U ug/L 0.24 10 1 OC 06/04/10 106-43-4 4-CHLOROTOLUENE U ug/L 0.15 10 1 OC 06/04/10 124-48-1 DIBROMOCHLOROMETHANE U ug/L 0.18 10 1 OC 06/04/10 96-12-8 1.2-DIBROMO-3-CHLOROPROPANE U ug/L 0.35 10 1 OC 06/04/10 74-95-3 DIBROMOMETHANE U ug/L 0.25 10 1 OC 06/04/10 106-93-4 1.2-DIBROMOETHANE U ug/L 0.15 10 1 OC 06/04/10 95-50-1 1.2-DICHLOROBENZENE U ug/L 5.86 10 1 OC 06/04/10 541-73-1 1.3-DICHLOROBENZENE u ug/L 5.62 10 1 OC 06/04/10 106-46-7 1.4-DICHLOROBENZENE u ug/L 5.88 10 1 OC 06/04/10 75-71-8 DICHLORODIFLUOROMETHANE u ug/L 0.66 10 1 OC 06/04/10 75-34-3 1.1-DICHLOROETHANE u ug/L 0.49 10 1 OC 06/04/10 Page / of 11 Printed: 06/16/10 11:23 Listing of Results by Sample Sample Delivery Group: 1006009 Client Sample ID: LF-1 Laboratory Sample ID: 1006009-03 Date Sampled: 06/02/10 16:30 Sample Description: ATK-DLV - Groundwater Spring 2010 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 107-06-2 1.2-DICHLOROETHANE u ug/L 0.29 10 1 OC 06/04/10 75-35-4 1.1-DICHLOROETHENE 0.5 J ug/L 0.16 10 1 OC 06/04/10 156-59-4 CIS-1.2-DICHLOROETH ENE U ug/L 0.16 10 1 OC 06/04/10 156-60-5 TRANS-1.2-DICHLOROETH ENE U ug/L 0.34 10 1 OC 06/04/10 78-87-5 1.2-DICHLOROPROPANE U ug/L 0.16 10 1 OC 06/04/10 142-28-9 1.3-DICHLOROPROPANE U ug/L 0.24 10 1 OC 06/04/10 563-58-6 1.1-DICHLOROPROPENE U ug/L 0.17 10 1 OC 06/04/10 10061-01-5 CIS-1.3-DICHLOROPROPENE U ug/L 0.4 10 1 OC 06/04/10 10061-02-6 TRANS-1.3-DICHLOROPROPENE u ug/L 0.4 10 1 OC 06/04/10 590-20-7 2.2-DICHLOROPROPANE u ug/L 0.9 10 1 OC 06/04/10 100-41-4 ETHYLBENZENE u ug/L 0.16 10 1 OC 06/04/10 591-78-6 2-HEXANONE u ug/L 0.7 10 1 OC 06/04/10 87-68-3 HEXACHLOROBUTADIENE u ug/L 0.9 10 1 OC 06/04/10 98-82-8 ISOPROPYLBENZENE u ug/L 0.58 10 1 OC 06/04/10 99-87-6 4-ISOPROPYLTOLUENE u ug/L 0.24 10 1 OC 06/04/10 75-09-2 METHYLENE CHLORIDE u ug/L 0.8 10 1 OC 06/04/10 108-10-1 4-M ETHYL-2-PEN TAN ONE u ug/L 0.53 10 1 OC 06/04/10 91-20-3 NAPHTHALENE u ug/L 4 10 1 OC 06/04/10 103-65-1 N-PROPYLBENZENE u ug/L 0.5 10 1 OC 06/04/10 100-42-5 STYRENE u ug/L 0.3 10 1 OC 06/04/10 630-20-6 1.1.1.2-TETRACHLOROETHANE u ug/L 0.25 10 1 OC 06/04/10 79-34-5 1.1.2.2-TETRACHLOROETHANE u ug/L 0.85 10 1 OC 06/04/10 127-18-4 TETRACHLOROETHENE u ug/L 0.4 10 1 OC 06/04/10 108-88-3 TOLUENE u ug/L 0.5 10 1 OC 06/04/10 87-61-6 1.2.3-TRICHLOROBENZENE u ug/L 0.23 10 1 OC 06/04/10 120-82-1 1.2.4-TRICHLOROBENZENE u ug/L 4.37 10 1 OC 06/04/10 71-55-6 1.1.1-TRICHLOROETHANE 4. J ug/L 0.16 10 1 OC 06/04/10 79-00-5 1.1.2-TRICHLOROETHANE u ug/L 0.25 10 1 OC 06/04/10 79-01-6 TRICHLOROETHENE 34.2 ug/L 0.7 10 1 OC 06/04/10 75-69-4 TRICHLOROFLUOROMETHANE U ug/L 0.3 10 1 OC 06/04/10 96-18-4 1.2.3-TRICHLOROPROPANE U ug/L 0.33 10 1 OC 06/04/10 95-63-6 1.2.4-TRIM ETHYLBENZENE U ug/L 0.19 10 1 OC 06/04/10 108-67-8 1.3.5-TRIM ETHYLBENZENE U ug/L 0.29 10 1 OC 06/04/10 108-05-4 VINYL ACETATE U ug/L 20 50 1 OC 06/04/10 75-01-4 VINYL CHLORIDE U ug/L 0.3 10 1 OC 06/04/10 1330-20-7 m.p-XYLENE U ug/L 0.6 10 1 OC 06/04/10 95-47-6 o-XYLENE u ug/L 0.3 10 1 OC 06/04/10 460-00-4 BROMOFLUOROBENZENE 95.8 % 1 OC 06/04/10 1868-53-7 DIBROMOFLUOROMETHANE 101 % 1 OC 06/04/10 17060-07-0 1.2-DICHLOROETHANE-D4 109 % 1 OC 06/04/10 2037-26-5 T0LUENE-D8 95.8 % 1 OC 06/04/10 Client Sample ID: B-3 Laboratory Sample ID: 1006009-04 Date Sampled: 06/02/10 17:30 Sample Description: ATK-DLV - Groundwater Spring 2010 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TestMe^od: EPA 120.1 Conductivity CONDUCTIVITY 1440 uS/cm 0.3 1 1 JMM 06/14/10 Page 8 of 11 Printed: 06/16/10 11:23 Listing of Results by Sample Sample Delivery Group: 1006009 Client Sample ID: B-3 Sample Description: ATK-DLV - Groundwater Spring 2010 Laboratory Sample ID: 1006009-04 Date Sampled: 06/02/10 17:30 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TestMe^od: EPA 314.0 Perchlorate Ion Chromatography 014797-73-0 PERCHLORATE 40800. ug/L 100 400 100 JMM 06/15/10 TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 67-64-1 ACETONE U ug/L 250 500 50 OC 06/04/10 71-43-2 BENZENE U ug/L 11 500 50 OC 06/04/10 74-97-5 BROMOCHLOROMETHANE U ug/L 15.5 500 50 OC 06/04/10 75-27-4 BROMODICHLOROMETHANE U ug/L 9.5 500 50 OC 06/04/10 108-86-1 BROMOBENZENE U ug/L 18.5 500 50 OC 06/04/10 75-25-2 BROMOFORM U ug/L 21 500 50 OC 06/04/10 74-83-9 BROMOMETHANE U ug/L 28.5 500 50 OC 06/04/10 78-93-3 2-BUTANONE U ug/L 55.5 500 50 OC 06/04/10 104-51-8 N-BUTYLBENZENE U ug/L 15 500 50 OC 06/04/10 135-98-8 SEC-BUTYLBENZENE U ug/L 20 500 50 OC 06/04/10 98-06-6 TERT-BUTYLBENZENE U ug/L 20 500 50 OC 06/04/10 75-15-0 CARBON DISULFIDE U ug/L 6.5 500 50 OC 06/04/10 56-23-5 CARBON TETRACHLORIDE U ug/L 13.5 500 50 OC 06/04/10 108-90-7 CHLOROBENZENE U ug/L 8 500 50 OC 06/04/10 75-00-3 CHLOROETHANE U ug/L 17.5 500 50 OC 06/04/10 110-75-8 2-CHLOROETHYLVINYL ETHER U ug/L 85.5 500 50 OC 06/04/10 67-66-3 CHLOROFORM U ug/L 15 500 50 OC 06/04/10 74-87-3 CHLOROMETHANE U ug/L 40.5 500 50 OC 06/04/10 95-49-8 2-CHLOROTOLUENE U ug/L 12 500 50 OC 06/04/10 106-43-4 4-CHLOROTOLUENE U ug/L 7.5 500 50 OC 06/04/10 124-48-1 DIBROMOCHLOROMETHANE U ug/L 9 500 50 OC 06/04/10 96-12-8 1.2-DIBROMO-3-CHLOROPROPANE U ug/L 17.5 500 50 OC 06/04/10 74-95-3 DIBROMOMETHANE U ug/L 12.5 500 50 OC 06/04/10 106-93-4 1.2-DIBROMOETHANE U ug/L 7.5 500 50 OC 06/04/10 95-50-1 1.2-DICHLOROBENZENE u ug/L 293 500 50 OC 06/04/10 541-73-1 1.3-DICHLOROBENZENE u ug/L 281 500 50 OC 06/04/10 106-46-7 1.4-DICHLOROBENZENE u ug/L 294 500 50 OC 06/04/10 75-71-8 DICHLORODIFLUOROMETHANE u ug/L 33 500 50 OC 06/04/10 75-34-3 1.1-DICHLOROETHANE u ug/L 24.5 500 50 OC 06/04/10 107-06-2 1.2-DICHLOROETHANE u ug/L 14.5 500 50 OC 06/04/10 75-35-4 1.1-DICHLOROETHENE 500 ug/L 8 500 50 OC 06/04/10 156-59-4 CIS-1.2-DICHLOROETH ENE U ug/L 8 500 50 OC 06/04/10 156-60-5 TRANS-1.2-DICHLOROETH ENE u ug/L 17 500 50 OC 06/04/10 78-87-5 1.2-DICHLOROPROPANE u ug/L 8 500 50 OC 06/04/10 142-28-9 1.3-DICHLOROPROPANE u ug/L 12 500 50 OC 06/04/10 563-58-6 1.1-DICHLOROPROPENE u ug/L 8.5 500 50 OC 06/04/10 10061-01-5 CIS-1.3-DICHLOROPROPENE u ug/L 20 500 50 OC 06/04/10 10061-02-6 TRANS-1.3-DICHLOROPROPENE u ug/L 20 500 50 OC 06/04/10 590-20-7 2.2-DICHLOROPROPANE u ug/L 45 500 50 OC 06/04/10 100-41-4 ETHYLBENZENE u ug/L 8 500 50 OC 06/04/10 591-78-6 2-HEXANONE u ug/L 35 500 50 OC 06/04/10 87-68-3 HEXACHLOROBUTADIENE u ug/L 45 500 50 OC 06/04/10 98-82-8 ISOPROPYLBENZENE u ug/L 29 500 50 OC 06/04/10 99-87-6 4-ISOPROPYLTOLUENE u ug/L 12 500 50 OC 06/04/10 75-09-2 METHYLENE CHLORIDE u ug/L 40 500 50 OC 06/04/10 108-10-1 4-M ETHYL-2-PEN TAN ONE u ug/L 26.5 500 50 OC 06/04/10 91-20-3 NAPHTHALENE u ug/L 200 500 50 OC 06/04/10 103-65-1 N-PROPYLBENZENE u ug/L 25 500 50 OC 06/04/10 Page 9 of 11 Printed: 06/16/10 11:23 Listing of Results by Sample Sample Delivery Group: 1006009 Client Sample ID: B-3 Sample Description: ATK-DLV - Groundwater Spring 2010 Laboratory Sample ID: 1006009-04 Date Sampled: 06/02/10 17:30 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 100-42-5 STYRENE U ug/L 15 500 50 OC 06/04/10 630-20-6 1.1.1.2-TETRACHLOROETHANE U ug/L 12.5 500 50 OC 06/04/10 79-34-5 1.1.2.2-TETRACHLOROETHANE U ug/L 42.5 500 50 OC 06/04/10 127-18-4 TETRACHLOROETHENE U ug/L 20 500 50 OC 06/04/10 108-88-3 TOLUENE U ug/L 25 500 50 OC 06/04/10 87-61-6 1.2.3-TRICHLOROBENZENE U ug/L 11.5 500 50 OC 06/04/10 120-82-1 1.2.4-TRICHLOROBENZENE U ug/L 218.5 500 50 OC 06/04/10 71-55-6 1.1.1-TRICHLOROETHANE 500. J ug/L 8 500 50 OC 06/04/10 79-00-5 1.1.2-TRICHLOROETHANE U ug/L 12.5 500 50 OC 06/04/10 79-01-6 TRICHLOROETHENE 3270 ug/L 35 500 50 OC 06/04/10 75-69-4 TRICHLOROFLUOROMETHANE U ug/L 15 500 50 OC 06/04/10 96-18-4 1.2.3-TRICHLOROPROPANE U ug/L 16.5 500 50 OC 06/04/10 95-63-6 1.2.4-TRIM ETHYLBENZENE U ug/L 9.5 500 50 OC 06/04/10 108-67-8 1.3.5-TRIM ETHYLBENZENE U ug/L 14.5 500 50 OC 06/04/10 108-05-4 VINYL ACETATE U ug/L 1000 2500 50 OC 06/04/10 75-01-4 VINYL CHLORIDE U ug/L 15 500 50 OC 06/04/10 1330-20-7 m.p-XYLENE U ug/L 30 500 50 OC 06/04/10 95-47-6 o-XYLENE U ug/L 15 500 50 OC 06/04/10 460-00-4 BROMOFLUOROBENZENE 93.5 % 50 OC 06/04/10 1868-53-7 DIBROMOFLUOROMETHANE 104 % 50 OC 06/04/10 17060-07-0 1.2-DICHLOROETHANE-D4 109 % 50 OC 06/04/10 2037-26-5 T0LUENE-D8 96.7 % 50 OC 06/04/10 TestMe^od: SlV-846, 8330A Explosives Extraction DAT ECOMPLETED 06/09/2010 00:00 1 JNB 06/09/10 TestMe^od: SW-846, 8330A Mod(Water) Explosives Analysis 2691-41-0 HMX 2.70 ug/L 0.3 1 1 JNB 06/10/10 121-82-4 RDX 1.94 ug/L 0.3 1 1 JNB 06/10/10 99-08-1 3-NITROTOLUENE 99.2 % 1 JNB 06/10/10 Page 10 of 11 Printed: 06/16/10 11:23 Data Reporting Qualifiers U Indicates that the analyte concentration is less than the MDL. B This flag is used when an analyte is found in the blank as well as the sample. Indicates an extimated value. This flag is used either when estimating a concentration for tentatively identified compounds or when the data indicated the presence of a compound that meets the identification criteria but the result is less than the EQL (e.g. 3 J with an EQL of 10). MDL Method Detection Limit: The minimum concentration of a substance that can be confidently measured and reported. The laboratory has demonstrated that the MDL can be achieved in a laboratory reagent blank, but does not guarantee it can be achieved in all sample matrices. EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many analytes the EQL is selected as the value of the lowest standard in the calibration cuh/e. Dilution Dilution Factor: The prepared sample was diluted by this factor because the Factor sample was too concentrated or due to other interferences in the sample matrix. Any dilution factor causes a corresponding increase in the MDL and EQL. Page 11 of 11 Printed: 06/16/10 11:23 ATK Launch Systems Environmental Laboratory Sample Receipt Checklist ATI/: Liu^c/f 7>iY Client Name:, SDG No. Carrier: n Hand delivered, no cooler Carrier Number: n Hand delivered, sample(s) taken out at receiving counter Cooier Information: Cooler Number/ID: Condition of Shipping Container: Cooler Sealed (taped): Custody Seals Present: Coolant: State of Coolant: Thermometer ID: Packing Description: ^ood • Fair • Not Applicable • Damaged (explain) •Yes 5^0 • Not Applicable •Yes ;^o • Not Applicable • Intact • Broken Seal Number: JSjIce j0 Frozen •Blue Ice •None Other: JSjIce j0 Frozen •Partially Frozen • Melted Reading: CF: Corrected Temp: »C Temp Blank Included: UYes DNo Chain-Of-Custody Information: COC Present: / / ^ Kf©' COC Number(s): F^]^/ (^C^ COC signed (relinquished and received): COC or LWI agrees with sample labels: Notes: • No • No •No Other: •Not Applicable • Not Applicable Sample Information: Samples included in cooler: Custody Seals Present: Sample containers intact: Samples in proper containers: Sufficient sample volume: All samples received in hold time: ^es Water - VOA's have zero headspace: ^re-preserved with HCI: Notes: •Yes • Intact Xfes ^es ^Yes ;^o • No • No • No Other •Broken Seal Number(s) _ •No Notes: ^es •No • Not Applicable •Pre-preserved with Na2S203: • Non-Preserved: Water - pH acceptable upon receipt: UYes nAdjusted (see comments below) ^ot Applicable HNO3 = H2SO4 = NaOH = ZnAC /NaOH = HCL = Water - pH adjusted: (mfg. & Lot No.) HNO3 H2SO4, Na2S0203 Other _ Notes: NaOH _ZnAC. HCI SOP-102 Form A 1006009 ENVIRONMENTAL LAB WORK REQUEST ™= ATK ENVIRONMENTAL LABORATORY LWR No. Login No. E13166 FROM: EXTENSION COST CENTER WORKORDER DATE ORGANIZATION MAIL STOP REPORT RESULTS TO: HELEN RAVSTEN, MS 301 SAMPLE INFORMATION SAMPLE DATE TYPE LOCATION TIME TEST REMARKS SAMPLE DATE G c LOCATION TIME TEST REMARKS tf K f( 'f 3 LF- / X ^' ,1 tf 'f X 5. 6. 7. 8. 9. 10. 11.. 12. CHAIN OF CUSTODY RELp<^J^S]^ED BY DATE TIME RECEIVED BY DATE TIME FOR LABORATORY USE ONLY DATE COMPLETED DATE REPORTED SAMPLE NUMBER 2010 Spring GW Sampling ATK Launch Systems, Inc. Promontory, UTAH (801) 251-5688 : J^-.S' DATE: ^A//^ SAMPLER: 1006009 ANALYTICAL LABORATORY: ATK Environmental Laboratory M53 Bottle Number No. of Containers Fid. Preservative/ Treatment Requested Analysis 11 3 4 degrees C VOA, Appendix 9 Acidified Method 8260 .2 mL HCL 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314.0 SAMPLE NUMBER 2010 Spring GW Sampling ATK Launch Systems, Inc. Promontory, UTAH (801) 251-5688 DATE SAMPLER: 1006009 ANALYTICAL LABORATORY: ATK Environmental Laboratory M53 Bottle Number No. of Containers Fid. Preservative/ Treatment Requested Analysis 11 3 4 degrees C VOA, Appendix 9 Acidified Method 8260 .2 mL HCL 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314.0 2010 Spring GW Sampling ATK Launch Systems, Inc. Promontory, UTAH (801) 251-5688 SAMPLE NUMBER: Lf^l DATE: /^^LjlO SAMPLER: 1006009 ANALYTICAL LABORATORY: ATK Environmental Laboratory M53 Bottle Number No. of Containers Fid. Preservative/ Treatment Requested Analysis 11 3 4 degrees C VOA, Appendix 9 Acidified Method 8260 .2 mL HCL 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314.0 SAMPLE NUMBER: S-3 2010 Spring GW Sampling ATK Launch Systems, Inc. Promontory, UTAH (801) 251-5688 DATE; AM [O SAMPLER: 1006009 ANALYTICAL LABORATORY: ATK Environmental Laboratory MS3 Bottle Number No. of Containers Fid. Preservative/ Treatment Requested Analysis 11 3 4 degrees C Acidified .2 mL HCL VOA, Appendix 9 Method 8260 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314.0 i 1 988P LS333 GW CERTIFICATE OF ANALYSIS Listing of Sample Information and Testing Requested Wednesday, June 16, 2010 TESTED FOR: ATK: DLV Environmental Monitoring Thiokol Corp, UT 84322 ANALYZED BY: ATK Launch Systems Analytical Chemistry Laboratory P.O. Box 707, M/S 245 Brigham City, UT 84302-0707 435-863-3732 435-863-8080 Contact Name: Project: Sample Delivery Group: Al Lee Ground Water Testing - DLV 1006010 Page 1 of 18 Printed: 06/16/10 11:25 Sample Delivery Group: 1006010 Sample No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 1006010-01 D-1 06/03/10 6/3/2010 11:00:00 EPA 120.1 EPA 314.0 SW-846. 8260B (Water) Conductivity Perchlorate - Ion Chromatography Volatile Organic Analysis Water Water Water 1006010-02 B-10 06/03/10 6/3/2010 11:55:00 EPA 120.1 EPA 314.0 SW-846. 8260B (Water) Conductivity Perchlorate - Ion Chromatography Volatile Organic Analysis Water Water Water 1006010-03 B-2D 06/03/10 6/3/2010 12:50:00 EPA 120.1 EPA 314.0 SW-846. 8260B (Water) Conductivity Perchlorate - Ion Chromatography Volatile Organic Analysis Water Water Water 1006010-04 G-2 06/03/10 6/3/2010 14:00:00 EPA 120.1 EPA 314.0 SW-846. 8260B (Water) Conductivity Perchlorate - Ion Chromatography Volatile Organic Analysis Water Water Water 1006010-05 G2A 06/03/10 6/3/2010 14:05:00 EPA 120.1 EPA 314.0 SW-846. 8260B (Water) Conductivity Perchlorate - Ion Chromatography Volatile Organic Analysis Water Water Water 1006010-06 TP-001 06/03/10 6/3/2010 14:10:00 EPA 120.1 EPA 314.0 SW-846. 8260B (Water) Conductivity Perchlorate - Ion Chromatography Volatile Organic Analysis Water Water Water 1006010-07 FP-001 06/03/10 6/3/2010 14:15:00 EPA 120.1 EPA 314.0 SW-846. 8260B (Water) Conductivity Perchlorate - Ion Chromatography Volatile Organic Analysis Water Water Water 1006010-08 B-6 06/03/10 6/3/2010 14:45:00 EPA 120.1 EPA 314.0 Conductivity Perchlorate - Ion Chromatography Water Water Page 2 of 18 Printed: 06/16/10 11:25 Sample Delivery Group: 1006010 Sample No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 1006010-08 B-6 06/03/10 6/3/2010 14:45:00 SW-846. 8260B (Water) Volatile Organic Analysis Water Certified By: 06/17/2010 W. Scott Fraser, Quality Assurance Officer Date This ceiiifies that the following data meets the requirements of the National Environmental Laboratoiy Accreditation Program (NELAP) unless otherwise annotated: Page 3 of 18 Printed: 06/16/10 11:25 Listing of Results by Sample Sample Delivery Group: 1006010 Client Sample ID: D-1 Sample Description: ATK-DLV - Groundwater Spring 2010 Laboratory Sample ID: 1006010-01 Date Sampled: 06/03/10 11:00 CAS Number TestMe^od: TestMe^od: 014797-73-0 TestMe^od: Test Parameter EPA 120.1 CONDUCTIVITY EPA 314.0 PERCHLORATE SW-846, 8260B (Water) Result Units Conductivity 2010 uS/cm Perchlorate - Ion Chromatography 551. ug/L Volatile Organic Analysis MDL 0.3 Dilution EQL Factor Analyst Test Date 10 40 10 JMM JMM 06/14/10 06/15/10 67-64-1 ACETONE U ug/L 5 10 1 OC 06/08/10 71-43-2 BENZENE 3.6 J ug/L 0.22 10 1 OC 06/08/10 74-97-5 BROMOCHLOROMETHANE U ug/L 0.31 10 1 OC 06/08/10 75-27-4 BROMODICHLOROMETHANE U ug/L 0.19 10 1 OC 06/08/10 108-86-1 BROMOBENZENE U ug/L 0.37 10 1 OC 06/08/10 75-25-2 BROMOFORM U ug/L 0.42 10 1 OC 06/08/10 74-83-9 BROMOMETHANE U ug/L 0.57 10 1 OC 06/08/10 78-93-3 2-BUTANONE U ug/L 1.11 10 1 OC 06/08/10 104-51-8 N-BUTYLBENZENE U ug/L 0.3 10 1 OC 06/08/10 135-98-8 SEC-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/08/10 98-06-6 TERT-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/08/10 75-15-0 CARBON DISULFIDE U ug/L 0.13 10 1 OC 06/08/10 56-23-5 CARBON TETRACHLORIDE 7. J ug/L 0.27 10 1 OC 06/08/10 108-90-7 CHLOROBENZENE U ug/L 0.16 10 1 OC 06/08/10 75-00-3 CHLOROETHANE U ug/L 0.35 10 1 OC 06/08/10 110-75-8 2-CHLOROETHYLVINYL ETHER U ug/L 1.71 10 1 OC 06/08/10 67-66-3 CHLOROFORM 27.3 ug/L 0.3 10 1 OC 06/08/10 74-87-3 CHLOROMETHANE U ug/L 0.81 10 1 OC 06/08/10 95-49-8 2-CHLOROTOLUENE U ug/L 0.24 10 1 OC 06/08/10 106-43-4 4-CHLOROTOLUENE U ug/L 0.15 10 1 OC 06/08/10 124-48-1 DIBROMOCHLOROMETHANE U ug/L 0.18 10 1 OC 06/08/10 96-12-8 1.2-DIBROMO-3-CHLOROPROPANE U ug/L 0.35 10 1 OC 06/08/10 74-95-3 DIBROMOMETHANE U ug/L 0.25 10 1 OC 06/08/10 106-93-4 1.2-DIBROMOETHANE U ug/L 0.15 10 1 OC 06/08/10 95-50-1 1.2-DICHLOROBENZENE U ug/L 5.86 10 1 OC 06/08/10 541-73-1 1.3-DICHLOROBENZENE U ug/L 5.62 10 1 OC 06/08/10 106-46-7 1.4-DICHLOROBENZENE U ug/L 5.88 10 1 OC 06/08/10 75-71-8 DICHLORODIFLUOROMETHANE U ug/L 0.66 10 1 OC 06/08/10 75-34-3 1.1-DICHLOROETHANE 18.9 ug/L 0.49 10 1 OC 06/08/10 107-06-2 1.2-DICHLOROETHANE U ug/L 0.29 10 1 OC 06/08/10 75-35-4 1.1-DICHLOROETHENE 787 ug/L 0.16 10 1 OC 06/08/10 156-59-4 CIS-1.2-DICHLOROETH ENE U ug/L 0.16 10 1 OC 06/08/10 156-60-5 TRANS-1.2-DICHLOROETH ENE 0.3 J ug/L 0.34 10 1 OC 06/08/10 78-87-5 1.2-DICHLOROPROPANE U ug/L 0.16 10 1 OC 06/08/10 142-28-9 1.3-DICHLOROPROPANE U ug/L 0.24 10 1 OC 06/08/10 563-58-6 1.1-DICHLOROPROPENE U ug/L 0.17 10 1 OC 06/08/10 10061-01-5 CIS-1.3-DICHLOROPROPENE U ug/L 0.4 10 1 OC 06/08/10 10061-02-6 TRANS-1.3-DICHLOROPROPENE U ug/L 0.4 10 1 OC 06/08/10 590-20-7 2.2-DICHLOROPROPANE U ug/L 0.9 10 1 OC 06/08/10 100-41-4 ETHYLBENZENE U ug/L 0.16 10 1 OC 06/08/10 591-78-6 2-HEXANONE U ug/L 0.7 10 1 OC 06/08/10 87-68-3 HEXACHLOROBUTADIENE U ug/L 0.9 10 1 OC 06/08/10 98-82-8 ISOPROPYLBENZENE U ug/L 0.58 10 1 OC 06/08/10 99-87-6 4-ISOPROPYLTOLUENE U ug/L 0.24 10 1 OC 06/08/10 75-09-2 METHYLENE CHLORIDE U ug/L 0.8 10 1 OC 06/08/10 Page Printed: 06/16/10 11:25 Listing of Results by Sample Sample Delivery Group: 1006010 Client Sample ID: D-1 Laboratory Sample ID: 1006010-01 Date Sampled: 06/03/10 11:00 Sample Description: ATK-DLV - Groundwater Spring 2010 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 108-10-1 4-M ETHYL-2-PEN TAN ONE u ug/L 0.53 10 1 OC 06/08/10 91-20-3 NAPHTHALENE u ug/L 4 10 1 OC 06/08/10 103-65-1 N-PROPYLBENZENE u ug/L 0.5 10 1 OC 06/08/10 100-42-5 STYRENE u ug/L 0.3 10 1 OC 06/08/10 630-20-6 1.1.1.2-TETRACHLOROETHANE u ug/L 0.25 10 1 OC 06/08/10 79-34-5 1.1.2.2-TETRACHLOROETHANE u ug/L 0.85 10 1 OC 06/08/10 127-18-4 TETRACHLOROETHENE 6.9 J ug/L 0.4 10 1 OC 06/08/10 108-88-3 TOLUENE U ug/L 0.5 10 1 OC 06/08/10 87-61-6 1.2.3-TRICHLOROBENZENE U ug/L 0.23 10 1 OC 06/08/10 120-82-1 1.2.4-TRICHLOROBENZENE U ug/L 4.37 10 1 OC 06/08/10 71-55-6 1.1.1-TRICHLOROETHANE 1400. J ug/L 32 2000 200 OC 06/08/10 79-00-5 1.1.2-TRICHLOROETHANE U ug/L 0.25 10 1 OC 06/08/10 79-01-6 TRICHLOROETHENE 9850 ug/L 140 2000 200 OC 06/08/10 75-69-4 TRICHLOROFLUOROMETHANE U ug/L 0.3 10 1 OC 06/08/10 96-18-4 1.2.3-TRICHLOROPROPANE U ug/L 0.33 10 1 OC 06/08/10 95-63-6 1.2.4-TRIM ETHYLBENZENE U ug/L 0.19 10 1 OC 06/08/10 108-67-8 1.3.5-TRIM ETHYLBENZENE U ug/L 0.29 10 1 OC 06/08/10 108-05-4 VINYL ACETATE U ug/L 20 50 1 OC 06/08/10 75-01-4 VINYL CHLORIDE U ug/L 0.3 10 1 OC 06/08/10 1330-20-7 m.p-XYLENE U ug/L 0.6 10 1 OC 06/08/10 95-47-6 o-XYLENE U ug/L 0.3 10 1 OC 06/08/10 460-00-4 BROMOFLUOROBENZENE 95.6 % 1 OC 06/08/10 1868-53-7 DIBROMOFLUOROMETHANE 103 % 1 OC 06/08/10 17060-07-0 1.2-DICHLOROETHANE-D4 108 % 1 OC 06/08/10 2037-26-5 T0LUENE-D8 98 % OC 06/08/10 Client Sample ID: B-10 Laboratory Sample ID: 1006010-02 Date Sampled: 06/03/10 11:55 Sample Description: ATK-DLV - Groundwater Spring 2010 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TestMe^od: EPA 120.1 Conductivity CONDUCTIVITY 1000 uS/cm 0.3 1 1 JMM 06/14/10 TestMe^od: EPA 314.0 Perchlorate - Ion Chromatography 014797-73-0 PERCHLORATE 4040. ug/L 50 200 50 JMM 06/15/10 TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 67-64-1 ACETONE U ug/L 5 10 1 OC 06/08/10 71-43-2 BENZENE 0.2 J ug/L 0.22 10 1 OC 06/08/10 74-97-5 BROMOCHLOROMETHANE U ug/L 0.31 10 1 OC 06/08/10 75-27-4 BROMODICHLOROMETHANE U ug/L 0.19 10 1 OC 06/08/10 108-86-1 BROMOBENZENE U ug/L 0.37 10 1 OC 06/08/10 75-25-2 BROMOFORM U ug/L 0.42 10 1 OC 06/08/10 74-83-9 BROMOMETHANE U ug/L 0.57 10 1 OC 06/08/10 78-93-3 2-BUTANONE U ug/L 1.11 10 1 OC 06/08/10 104-51-8 N-BUTYLBENZENE U ug/L 0.3 10 1 OC 06/08/10 135-98-8 SEC-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/08/10 98-06-6 TERT-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/08/10 75-15-0 CARBON DISULFIDE U ug/L 0.13 10 1 OC 06/08/10 Page 5 of 18 Printed: 06/16/10 11:25 Listing of Results by Sample Sample Delivery Group: 1006010 Client Sample ID: B-10 Laboratory Sample ID: 1006010-02 Sample Description: ATK-DLV - Groundwater Spring 2010 Date Sampled: 06/03/10 11:55 CAS Number Test Parameter Result Units MDL Dilution EQL Factor Analyst Test Date TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 56-23-5 CARBON TETRACHLORIDE U ug/L 0.27 10 1 OC 06/08/10 108-90-7 CHLOROBENZENE U ug/L 0.16 10 1 OC 06/08/10 75-00-3 CHLOROETHANE U ug/L 0.35 10 1 OC 06/08/10 110-75-8 2-CHLOROETHYLVINYL ETHER U ug/L 1.71 10 1 OC 06/08/10 67-66-3 CHLOROFORM U ug/L 0.3 10 1 OC 06/08/10 74-87-3 CHLOROMETHANE U ug/L 0.81 10 1 OC 06/08/10 95-49-8 2-CHLOROTOLUENE U ug/L 0.24 10 1 OC 06/08/10 106-43-4 4-CHLOROTOLUENE U ug/L 0.15 10 1 OC 06/08/10 124-48-1 DIBROMOCHLOROMETHANE U ug/L 0.18 10 1 OC 06/08/10 96-12-8 1.2-DIBROMO-3-CHLOROPROPANE U ug/L 0.35 10 1 OC 06/08/10 74-95-3 DIBROMOMETHANE U ug/L 0.25 10 1 OC 06/08/10 106-93-4 1.2-DIBROMOETHANE U ug/L 0.15 10 1 OC 06/08/10 95-50-1 1.2-DICHLOROBENZENE U ug/L 5.86 10 1 OC 06/08/10 541-73-1 1.3-DICHLOROBENZENE U ug/L 5.62 10 1 OC 06/08/10 106-46-7 1.4-DICHLOROBENZENE U ug/L 5.88 10 1 OC 06/08/10 75-71-8 DICHLORODIFLUOROMETHANE U ug/L 0.66 10 1 OC 06/08/10 75-34-3 1.1-DICHLOROETHANE U ug/L 0.49 10 1 OC 06/08/10 107-06-2 1.2-DICHLOROETHANE U ug/L 0.29 10 1 OC 06/08/10 75-35-4 1.1-DICHLOROETHENE 2.1 J ug/L 0.16 10 1 OC 06/08/10 156-59-4 CIS-1.2-DICHLOROETH ENE U ug/L 0.16 10 1 OC 06/08/10 156-60-5 TRANS-1.2-DICHLOROETH ENE U ug/L 0.34 10 1 OC 06/08/10 78-87-5 1.2-DICHLOROPROPANE U ug/L 0.16 10 1 OC 06/08/10 142-28-9 1.3-DICHLOROPROPANE U ug/L 0.24 10 1 OC 06/08/10 563-58-6 1.1-DICHLOROPROPENE U ug/L 0.17 10 1 OC 06/08/10 10061-01-5 CIS-1.3-DICHLOROPROPENE U ug/L 0.4 10 1 OC 06/08/10 10061-02-6 TRANS-1.3-DICHLOROPROPENE U ug/L 0.4 10 1 OC 06/08/10 590-20-7 2.2-DICHLOROPROPANE U ug/L 0.9 10 1 OC 06/08/10 100-41-4 ETHYLBENZENE U ug/L 0.16 10 1 OC 06/08/10 591-78-6 2-HEXANONE U ug/L 0.7 10 1 OC 06/08/10 87-68-3 HEXACHLOROBUTADIENE U ug/L 0.9 10 1 OC 06/08/10 98-82-8 ISOPROPYLBENZENE U ug/L 0.58 10 1 OC 06/08/10 99-87-6 4-ISOPROPYLTOLUENE u ug/L 0.24 10 1 OC 06/08/10 75-09-2 METHYLENE CHLORIDE u ug/L 0.8 10 1 OC 06/08/10 108-10-1 4-M ETHYL-2-PEN TAN ONE u ug/L 0.53 10 1 OC 06/08/10 91-20-3 NAPHTHALENE u ug/L 4 10 1 OC 06/08/10 103-65-1 N-PROPYLBENZENE u ug/L 0.5 10 1 OC 06/08/10 100-42-5 STYRENE u ug/L 0.3 10 1 OC 06/08/10 630-20-6 1.1.1.2-TETRACHLOROETHANE u ug/L 0.25 10 1 OC 06/08/10 79-34-5 1.1.2.2-TETRACHLOROETHANE u ug/L 0.85 10 1 OC 06/08/10 127-18-4 TETRACHLOROETHENE u ug/L 0.4 10 1 OC 06/08/10 108-88-3 TOLUENE u ug/L 0.5 10 1 OC 06/08/10 87-61-6 1.2.3-TRICHLOROBENZENE u ug/L 0.23 10 1 OC 06/08/10 120-82-1 1.2.4-TRICHLOROBENZENE u ug/L 4.37 10 1 OC 06/08/10 71-55-6 1.1.1-TRICHLOROETHANE u ug/L 0.16 10 1 OC 06/08/10 79-00-5 1.1.2-TRICHLOROETHANE u ug/L 0.25 10 1 OC 06/08/10 79-01-6 TRICHLOROETHENE 40.2 ug/L 0.7 10 1 OC 06/08/10 75-69-4 TRICHLOROFLUOROMETHANE U ug/L 0.3 10 1 OC 06/08/10 96-18-4 1.2.3-TRICHLOROPROPANE U ug/L 0.33 10 1 OC 06/08/10 95-63-6 1.2.4-TRIM ETHYLBENZENE u ug/L 0.19 10 1 OC 06/08/10 108-67-8 1.3.5-TRIM ETHYLBENZENE u ug/L 0.29 10 1 OC 06/08/10 Page 6 of 18 Printed: 06/16/10 11:25 Listing of Results by Sample Sample Delivery Group: 1006010 Client Sample ID: B-10 Sample Description: ATK-DLV - Groundwater Spring 2010 Laboratory Sample ID: 1006010-02 Date Sampled: 06/03/10 11:55 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 108-05-4 VINYL ACETATE u ug/L 20 50 1 OC 06/08/10 75-01-4 VINYL CHLORIDE u ug/L 0.3 10 1 OC 06/08/10 1330-20-7 m.p-XYLENE u ug/L 0.6 10 1 OC 06/08/10 95-47-6 o-XYLENE u ug/L 0.3 10 1 OC 06/08/10 460-00-4 BROMOFLUOROBENZENE 93.8 % 1 OC 06/08/10 1868-53-7 DIBROMOFLUOROMETHANE 106 % 1 OC 06/08/10 17060-07-0 1.2-DICHLOROETHANE-D4 110 % 1 OC 06/08/10 2037-26-5 T0LUENE-D8 96.5 % 1 OC 06/08/10 Client Sample ID: B-2D Laboratory Sample ID: 1006010-03 Date Sampled: 06/03/10 12:50 Sample Description: ATK-DLV - Groundwater Spring 2010 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TestMe^od: EPA 120.1 Conductivity CONDUCTIVITY 1520 uS/cm 0.3 1 1 JMM 06/14/10 TestMe^od: EPA 314.0 Perchlorate - Ion Chromatography 014797-73-0 PERCHLORATE 25600. ug/L 100 400 100 JMM 06/15/10 TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 67-64-1 ACETONE U ug/L 5 10 1 OC 06/08/10 71-43-2 BENZENE 1.1 J ug/L 0.22 10 1 OC 06/08/10 74-97-5 BROMOCHLOROMETHANE U ug/L 0.31 10 1 OC 06/08/10 75-27-4 BROMODICHLOROMETHANE U ug/L 0.19 10 1 OC 06/08/10 108-86-1 BROMOBENZENE U ug/L 0.37 10 1 OC 06/08/10 75-25-2 BROMOFORM U ug/L 0.42 10 1 OC 06/08/10 74-83-9 BROMOMETHANE U ug/L 0.57 10 1 OC 06/08/10 78-93-3 2-BUTANONE U ug/L 1.11 10 1 OC 06/08/10 104-51-8 N-BUTYLBENZENE U ug/L 0.3 10 1 OC 06/08/10 135-98-8 SEC-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/08/10 98-06-6 TERT-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/08/10 75-15-0 CARBON DISULFIDE U ug/L 0.13 10 1 OC 06/08/10 56-23-5 CARBON TETRACHLORIDE 4.5 J ug/L 0.27 10 1 OC 06/08/10 108-90-7 CHLOROBENZENE 0.7 J ug/L 0.16 10 1 OC 06/08/10 75-00-3 CHLOROETHANE U ug/L 0.35 10 1 OC 06/08/10 110-75-8 2-CHLOROETHYLVINYL ETHER U ug/L 1.71 10 1 OC 06/08/10 67-66-3 CHLOROFORM 89.8 ug/L 0.3 10 1 OC 06/08/10 74-87-3 CHLOROMETHANE U ug/L 0.81 10 1 OC 06/08/10 95-49-8 2-CHLOROTOLUENE U ug/L 0.24 10 1 OC 06/08/10 106-43-4 4-CHLOROTOLUENE U ug/L 0.15 10 1 OC 06/08/10 124-48-1 DIBROMOCHLOROMETHANE U ug/L 0.18 10 1 OC 06/08/10 96-12-8 1.2-DIBROMO-3-CHLOROPROPANE U ug/L 0.35 10 1 OC 06/08/10 74-95-3 DIBROMOMETHANE U ug/L 0.25 10 1 OC 06/08/10 106-93-4 1.2-DIBROMOETHANE U ug/L 0.15 10 1 OC 06/08/10 95-50-1 1.2-DICHLOROBENZENE U ug/L 5.86 10 1 OC 06/08/10 541-73-1 1.3-DICHLOROBENZENE U ug/L 5.62 10 1 OC 06/08/10 106-46-7 1.4-DICHLOROBENZENE U ug/L 5.88 10 1 OC 06/08/10 75-71-8 DICHLORODIFLUOROMETHANE U ug/L 0.66 10 1 OC 06/08/10 75-34-3 1.1-DICHLOROETHANE 38.9 ug/L 0.49 10 1 OC 06/08/10 Page / of 18 Printed: 06/16/10 11:25 Listing of Results by Sample Sample Delivery Group: 1006010 Client Sample ID: B-2D Laboratory Sample ID: 1006010-03 Date Sampled: 06/03/10 12:50 Sample Description: ATK-DLV - Groundwater Spring 2010 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 107-06-2 1.2-DICHLOROETHANE 8. J ug/L 0.29 10 1 OC 06/08/10 75-35-4 1.1-DICHLOROETHENE 444 ug/L 3.2 200 20 OC 06/08/10 156-59-4 CIS-1.2-DICHLOROETH ENE 20.9 ug/L 0.16 10 1 OC 06/08/10 156-60-5 TRANS-1.2-DICHLOROETH ENE U ug/L 0.34 10 1 OC 06/08/10 78-87-5 1.2-DICHLOROPROPANE U ug/L 0.16 10 1 OC 06/08/10 142-28-9 1.3-DICHLOROPROPANE U ug/L 0.24 10 1 OC 06/08/10 563-58-6 1.1-DICHLOROPROPENE U ug/L 0.17 10 1 OC 06/08/10 10061-01-5 CIS-1.3-DICHLOROPROPENE U ug/L 0.4 10 1 OC 06/08/10 10061-02-6 TRANS-1.3-DICHLOROPROPENE U ug/L 0.4 10 1 OC 06/08/10 590-20-7 2.2-DICHLOROPROPANE U ug/L 0.9 10 1 OC 06/08/10 100-41-4 ETHYLBENZENE U ug/L 0.16 10 1 OC 06/08/10 591-78-6 2-HEXANONE U ug/L 0.7 10 1 OC 06/08/10 87-68-3 HEXACHLOROBUTADIENE U ug/L 0.9 10 1 OC 06/08/10 98-82-8 ISOPROPYLBENZENE U ug/L 0.58 10 1 OC 06/08/10 99-87-6 4-ISOPROPYLTOLUENE U ug/L 0.24 10 1 OC 06/08/10 75-09-2 METHYLENE CHLORIDE U ug/L 0.8 10 1 OC 06/08/10 108-10-1 4-M ETHYL-2-PEN TAN ONE U ug/L 0.53 10 1 OC 06/08/10 91-20-3 NAPHTHALENE U ug/L 4 10 1 OC 06/08/10 103-65-1 N-PROPYLBENZENE U ug/L 0.5 10 1 OC 06/08/10 100-42-5 STYRENE U ug/L 0.3 10 1 OC 06/08/10 630-20-6 1.1.1.2-TETRACHLOROETHANE U ug/L 0.25 10 1 OC 06/08/10 79-34-5 1.1.2.2-TETRACHLOROETHANE U ug/L 0.85 10 1 OC 06/08/10 127-18-4 TETRACHLOROETHENE 2.2 J ug/L 0.4 10 1 OC 06/08/10 108-88-3 TOLUENE U ug/L 0.5 10 1 OC 06/08/10 87-61-6 1.2.3-TRICHLOROBENZENE U ug/L 0.23 10 1 OC 06/08/10 120-82-1 1.2.4-TRICHLOROBENZENE U ug/L 4.37 10 1 OC 06/08/10 71-55-6 1.1.1-TRICHLOROETHANE 621 ug/L 3.2 200 20 OC 06/08/10 79-00-5 1.1.2-TRICHLOROETHANE 3.2 J ug/L 0.25 10 1 OC 06/08/10 79-01-6 TRICHLOROETHENE 3190 ug/L 14 200 20 OC 06/08/10 75-69-4 TRICHLOROFLUOROMETHANE U ug/L 0.3 10 1 OC 06/08/10 96-18-4 1.2.3-TRICHLOROPROPANE U ug/L 0.33 10 1 OC 06/08/10 95-63-6 1.2.4-TRIM ETHYLBENZENE U ug/L 0.19 10 1 OC 06/08/10 108-67-8 1.3.5-TRIM ETHYLBENZENE U ug/L 0.29 10 1 OC 06/08/10 108-05-4 VINYL ACETATE U ug/L 20 50 1 OC 06/08/10 75-01-4 VINYL CHLORIDE U ug/L 0.3 10 1 OC 06/08/10 1330-20-7 m.p-XYLENE U ug/L 0.6 10 1 OC 06/08/10 95-47-6 o-XYLENE U ug/L 0.3 10 1 OC 06/08/10 460-00-4 BROMOFLUOROBENZENE 93.6 % 1 OC 06/08/10 1868-53-7 DIBROMOFLUOROMETHANE 105 % 1 OC 06/08/10 17060-07-0 1.2-DICHLOROETHANE-D4 108 % 1 OC 06/08/10 2037-26-5 T0LUENE-D8 97.3 % OC 06/08/10 Client Sample ID: G-2 Laboratory Sample ID: 1006010-04 Date Sampled: 06/03/10 14:00 Sample Description: ATK-DLV - Groundwater Spring 2010 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TestMe^od: EPA 120.1 Conductivity CONDUCTIVITY 7780 uS/cm 0.3 1 1 JMM 06/14/10 Page 8 of 18 Printed: 06/16/10 11:25 Listing of Results by Sample Sample Delivery Group: 1006010 Client Sample ID: G-2 Sample Description: ATK-DLV - Groundwater Spring 2010 Laboratory Sample ID: 1006010-04 Date Sampled: 06/03/10 14:00 Dilution CAS Number Test Parameter Result Units MDL EQL TestMe^od: EPA 314.0 Perchlorate Ion Chromatography 014797-73-0 PERCHLORATE 52100. ug/L 250 1000 TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 67-64-1 ACETONE U ug/L 5 10 71-43-2 BENZENE 0.5 J ug/L 0.22 10 74-97-5 BROMOCHLOROMETHANE U ug/L 0.31 10 75-27-4 BROMODICHLOROMETHANE U ug/L 0.19 10 108-86-1 BROMOBENZENE U ug/L 0.37 10 75-25-2 BROMOFORM U ug/L 0.42 10 74-83-9 BROMOMETHANE U ug/L 0.57 10 78-93-3 2-BUTANONE U ug/L 1.11 10 104-51-8 N-BUTYLBENZENE U ug/L 0.3 10 135-98-8 SEC-BUTYLBENZENE U ug/L 0.4 10 98-06-6 TERT-BUTYLBENZENE U ug/L 0.4 10 75-15-0 CARBON DISULFIDE U ug/L 0.13 10 56-23-5 CARBON TETRACHLORIDE 1.3 J ug/L 0.27 10 108-90-7 CHLOROBENZENE U ug/L 0.16 10 75-00-3 CHLOROETHANE U ug/L 0.35 10 110-75-8 2-CHLOROETHYLVINYL ETHER U ug/L 1.71 10 67-66-3 CHLOROFORM 32 ug/L 0.3 10 74-87-3 CHLOROMETHANE U ug/L 0.81 10 95-49-8 2-CHLOROTOLUENE U ug/L 0.24 10 106-43-4 4-CHLOROTOLUENE U ug/L 0.15 10 124-48-1 DIBROMOCHLOROMETHANE U ug/L 0.18 10 96-12-8 1.2-DIBROMO-3-CHLOROPROPANE U ug/L 0.35 10 74-95-3 DIBROMOMETHANE U ug/L 0.25 10 106-93-4 1.2-DIBROMOETHANE U ug/L 0.15 10 95-50-1 1.2-DICHLOROBENZENE U ug/L 5.86 10 541-73-1 1.3-DICHLOROBENZENE U ug/L 5.62 10 106-46-7 1.4-DICHLOROBENZENE U ug/L 5.88 10 75-71-8 DICHLORODIFLUOROMETHANE U ug/L 0.66 10 75-34-3 1.1-DICHLOROETHANE 12.8 ug/L 0.49 10 107-06-2 1.2-DICHLOROETHANE 2.8 J ug/L 0.29 10 75-35-4 1.1-DICHLOROETHENE 270 ug/L 3.2 200 156-59-4 CIS-1.2-DICHLOROETH ENE 40.4 ug/L 0.16 10 156-60-5 TRANS-1.2-DICHLOROETH ENE U ug/L 0.34 10 78-87-5 1.2-DICHLOROPROPANE U ug/L 0.16 10 142-28-9 1.3-DICHLOROPROPANE U ug/L 0.24 10 563-58-6 1.1-DICHLOROPROPENE U ug/L 0.17 10 10061-01-5 CIS-1.3-DICHLOROPROPENE U ug/L 0.4 10 10061-02-6 TRANS-1.3-DICHLOROPROPENE U ug/L 0.4 10 590-20-7 2.2-DICHLOROPROPANE U ug/L 0.9 10 100-41-4 ETHYLBENZENE U ug/L 0.16 10 591-78-6 2-HEXANONE U ug/L 0.7 10 87-68-3 HEXACHLOROBUTADIENE U ug/L 0.9 10 98-82-8 ISOPROPYLBENZENE U ug/L 0.58 10 99-87-6 4-ISOPROPYLTOLUENE U ug/L 0.24 10 75-09-2 METHYLENE CHLORIDE U ug/L 0.8 10 108-10-1 4-M ETHYL-2-PEN TAN ONE U ug/L 0.53 10 91-20-3 NAPHTHALENE U ug/L 4 10 103-65-1 N-PROPYLBENZENE U ug/L 0.5 10 20 JMM 06/15/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 OC 06/08/10 Page 9 of 1 Printed: 06/16/10 11:25 Listing of Results by Sample Sample Delivery Group: 1006010 Client Sample ID: G-2 Laboratory Sample ID: 1006010-04 Date Sampled: 06/03/10 14:00 Sample Description: ATK-DLV - Groundwater Spring 2010 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 100-42-5 STYRENE u ug/L 0.3 10 1 OC 06/08/10 630-20-6 1.1.1.2-TETRACHLOROETHANE u ug/L 0.25 10 1 OC 06/08/10 79-34-5 1.1.2.2-TETRACHLOROETHANE u ug/L 0.85 10 1 OC 06/08/10 127-18-4 TETRACHLOROETHENE u ug/L 0.4 10 1 OC 06/08/10 108-88-3 TOLUENE u ug/L 0.5 10 1 OC 06/08/10 87-61-6 1.2.3-TRICHLOROBENZENE u ug/L 0.23 10 1 OC 06/08/10 120-82-1 1.2.4-TRICHLOROBENZENE u ug/L 4.37 10 1 OC 06/08/10 71-55-6 1.1.1-TRICHLOROETHANE 170. J ug/L 3.2 200 20 OC 06/08/10 79-00-5 1.1.2-TRICHLOROETHANE 1.9 J ug/L 0.25 10 1 OC 06/08/10 79-01-6 TRICHLOROETHENE 2060 ug/L 14 200 20 OC 06/08/10 75-69-4 TRICHLOROFLUOROMETHANE U ug/L 0.3 10 1 OC 06/08/10 96-18-4 1.2.3-TRICHLOROPROPANE U ug/L 0.33 10 1 OC 06/08/10 95-63-6 1.2.4-TRIM ETHYLBENZENE U ug/L 0.19 10 1 OC 06/08/10 108-67-8 1.3.5-TRIM ETHYLBENZENE U ug/L 0.29 10 1 OC 06/08/10 108-05-4 VINYL ACETATE U ug/L 20 50 1 OC 06/08/10 75-01-4 VINYL CHLORIDE U ug/L 0.3 10 1 OC 06/08/10 1330-20-7 m.p-XYLENE U ug/L 0.6 10 1 OC 06/08/10 95-47-6 o-XYLENE U ug/L 0.3 10 1 OC 06/08/10 460-00-4 BROMOFLUOROBENZENE 93.9 % 1 OC 06/08/10 1868-53-7 DIBROMOFLUOROMETHANE 104 % 1 OC 06/08/10 17060-07-0 1.2-DICHLOROETHANE-D4 108 % 1 OC 06/08/10 2037-26-5 T0LUENE-D8 96.6 % OC 06/08/10 Client Sample ID: G2A Laboratory Sample ID: 1006010-05 Date Sampled: 06/03/10 14:05 Sample Description: ATK-DLV - Groundwater Spring 2010 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TestMe^od: EPA 120.1 Conductivity CONDUCTIVITY 7810 uS/cm 0.3 1 1 JMM 06/14/10 TestMe^od: EPA 314.0 Perchlorate - Ion Chromatography 014797-73-0 PERCHLORATE 51900. ug/L 250 1000 250 JMM 06/15/10 TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 67-64-1 ACETONE U ug/L 5 10 1 OC 06/08/10 71-43-2 BENZENE 0.5 J ug/L 0.22 10 1 OC 06/08/10 74-97-5 BROMOCHLOROMETHANE U ug/L 0.31 10 1 OC 06/08/10 75-27-4 BROMODICHLOROMETHANE U ug/L 0.19 10 1 OC 06/08/10 108-86-1 BROMOBENZENE U ug/L 0.37 10 1 OC 06/08/10 75-25-2 BROMOFORM U ug/L 0.42 10 1 OC 06/08/10 74-83-9 BROMOMETHANE U ug/L 0.57 10 1 OC 06/08/10 78-93-3 2-BUTANONE U ug/L 1.11 10 1 OC 06/08/10 104-51-8 N-BUTYLBENZENE U ug/L 0.3 10 1 OC 06/08/10 135-98-8 SEC-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/08/10 98-06-6 TERT-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/08/10 75-15-0 CARBON DISULFIDE U ug/L 0.13 10 1 OC 06/08/10 56-23-5 CARBON TETRACHLORIDE 1.3 J ug/L 0.27 10 1 OC 06/08/10 108-90-7 CHLOROBENZENE U ug/L 0.16 10 1 OC 06/08/10 75-00-3 CHLOROETHANE U ug/L 0.35 10 1 OC 06/08/10 Page 10 of 18 Printed: 06/16/10 11:25 Listing of Results by Sample Sample Delivery Group: 1006010 Client Sample ID: G2A Laboratory Sample ID: 1006010-05 Sample Description: ATK-DLV - Groundwater Spring 2010 Date Sampled: 06/03/10 14:05 CAS Number Test Parameter Result Units MDL EQL Dilution Factor Analyst Test Date TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 110-75-8 2-CHLOROETHYLVINYL ETHER U ug/L 1.71 10 1 OC 06/08/10 67-66-3 CHLOROFORM 31.4 ug/L 0.3 10 1 OC 06/08/10 74-87-3 CHLOROMETHANE U ug/L 0.81 10 1 OC 06/08/10 95-49-8 2-CHLOROTOLUENE U ug/L 0.24 10 1 OC 06/08/10 106-43-4 4-CHLOROTOLUENE U ug/L 0.15 10 1 OC 06/08/10 124-48-1 DIBROMOCHLOROMETHANE U ug/L 0.18 10 1 OC 06/08/10 96-12-8 1.2-DIBROMO-3-CHLOROPROPANE U ug/L 0.35 10 1 OC 06/08/10 74-95-3 DIBROMOMETHANE U ug/L 0.25 10 1 OC 06/08/10 106-93-4 1.2-DIBROMOETHANE U ug/L 0.15 10 1 OC 06/08/10 95-50-1 1.2-DICHLOROBENZENE U ug/L 5.86 10 1 OC 06/08/10 541-73-1 1.3-DICHLOROBENZENE U ug/L 5.62 10 1 OC 06/08/10 106-46-7 1.4-DICHLOROBENZENE U ug/L 5.88 10 1 OC 06/08/10 75-71-8 DICHLORODIFLUOROMETHANE U ug/L 0.66 10 1 OC 06/08/10 75-34-3 1.1-DICHLOROETHANE 12.7 ug/L 0.49 10 1 OC 06/08/10 107-06-2 1.2-DICHLOROETHANE 2.8 J ug/L 0.29 10 1 OC 06/08/10 75-35-4 1.1-DICHLOROETHENE 264 ug/L 3.2 200 20 OC 06/08/10 156-59-4 CIS-1.2-DICHLOROETH ENE 40.6 ug/L 0.16 10 1 OC 06/08/10 156-60-5 TRANS-1.2-DICHLOROETH ENE U ug/L 0.34 10 1 OC 06/08/10 78-87-5 1.2-DICHLOROPROPANE U ug/L 0.16 10 1 OC 06/08/10 142-28-9 1.3-DICHLOROPROPANE U ug/L 0.24 10 1 OC 06/08/10 563-58-6 1.1-DICHLOROPROPENE U ug/L 0.17 10 1 OC 06/08/10 10061-01-5 CIS-1.3-DICHLOROPROPENE U ug/L 0.4 10 1 OC 06/08/10 10061-02-6 TRANS-1.3-DICHLOROPROPENE U ug/L 0.4 10 1 OC 06/08/10 590-20-7 2.2-DICHLOROPROPANE U ug/L 0.9 10 1 OC 06/08/10 100-41-4 ETHYLBENZENE U ug/L 0.16 10 1 OC 06/08/10 591-78-6 2-HEXANONE U ug/L 0.7 10 1 OC 06/08/10 87-68-3 HEXACHLOROBUTADIENE U ug/L 0.9 10 1 OC 06/08/10 98-82-8 ISOPROPYLBENZENE U ug/L 0.58 10 1 OC 06/08/10 99-87-6 4-ISOPROPYLTOLUENE U ug/L 0.24 10 1 OC 06/08/10 75-09-2 METHYLENE CHLORIDE U ug/L 0.8 10 1 OC 06/08/10 108-10-1 4-M ETHYL-2-PEN TAN ONE U ug/L 0.53 10 1 OC 06/08/10 91-20-3 NAPHTHALENE U ug/L 4 10 1 OC 06/08/10 103-65-1 N-PROPYLBENZENE U ug/L 0.5 10 1 OC 06/08/10 100-42-5 STYRENE U ug/L 0.3 10 1 OC 06/08/10 630-20-6 1.1.1.2-TETRACHLOROETHANE U ug/L 0.25 10 1 OC 06/08/10 79-34-5 1.1.2.2-TETRACHLOROETHANE U ug/L 0.85 10 1 OC 06/08/10 127-18-4 TETRACHLOROETHENE 0.9 J ug/L 0.4 10 1 OC 06/08/10 108-88-3 TOLUENE U ug/L 0.5 10 1 OC 06/08/10 87-61-6 1.2.3-TRICHLOROBENZENE U ug/L 0.23 10 1 OC 06/08/10 120-82-1 1.2.4-TRICHLOROBENZENE U ug/L 4.37 10 1 OC 06/08/10 71-55-6 1.1.1-TRICHLOROETHANE 170. J ug/L 3.2 200 20 OC 06/08/10 79-00-5 1.1.2-TRICHLOROETHANE 1.7 J ug/L 0.25 10 1 OC 06/08/10 79-01-6 TRICHLOROETHENE 2230 ug/L 14 200 20 OC 06/08/10 75-69-4 TRICHLOROFLUOROMETHANE U ug/L 0.3 10 1 OC 06/08/10 96-18-4 1.2.3-TRICHLOROPROPANE U ug/L 0.33 10 1 OC 06/08/10 95-63-6 1.2.4-TRIM ETHYLBENZENE U ug/L 0.19 10 1 OC 06/08/10 108-67-8 1.3.5-TRIM ETHYLBENZENE U ug/L 0.29 10 1 OC 06/08/10 108-05-4 VINYL ACETATE U ug/L 20 50 1 OC 06/08/10 75-01-4 VINYL CHLORIDE U ug/L 0.3 10 1 OC 06/08/10 1330-20-7 m.p-XYLENE U ug/L 0.6 10 1 OC 06/08/10 Page 11 of 18 Printed: 06/16/10 11:25 Listing of Results by Sample Sample Delivery Group: 1006010 Client Sample ID: G2A Sample Description: ATK-DLV - Groundwater Spring 2010 Laboratory Sample ID: 1006010-05 Date Sampled: 06/03/10 14:05 CAS Number Test Parameter Result Units TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 95-47-6 o-XYLENE U ug/L 460-00-4 BROMOFLUOROBENZENE 98.4 % 1868-53-7 DIBROMOFLUOROMETHANE 105 % 17060-07-0 1.2-DICHLOROETHANE-D4 108 % 2037-26-5 T0LUENE-D8 96.3 % MDL 0.3 EQL 10 Dilution Factor Analyst Test Date OC OC OC OC OC 06/08/10 06/08/10 06/08/10 06/08/10 06/08/10 Client Sample ID: TP-001 Sample Description: ATK-DLV - Groundwater Spring 2010 Laboratory Sample ID: 1006010-06 Date Sampled: 06/03/10 14:10 CAS Number Dilution Test Parameter Result Units MDL EQL TestMe^od: EPA 120.1 Conductivity CONDUCTIVITY 4.04 uS/cm 0.3 1 1 JMM 06/14/10 TestMe^od: EPA 314.0 Perchlorate - Ion Chromatography 014797-73-0 PERCHLORATE U ug/L 1 4 1 JMM 06/15/10 TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 67-64-1 ACETONE U ug/L 5 10 1 OC 06/08/10 71-43-2 BENZENE U ug/L 0.22 10 1 OC 06/08/10 74-97-5 BROMOCHLOROMETHANE U ug/L 0.31 10 1 OC 06/08/10 75-27-4 BROMODICHLOROMETHANE U ug/L 0.19 10 1 OC 06/08/10 108-86-1 BROMOBENZENE U ug/L 0.37 10 1 OC 06/08/10 75-25-2 BROMOFORM U ug/L 0.42 10 1 OC 06/08/10 74-83-9 BROMOMETHANE U ug/L 0.57 10 1 OC 06/08/10 78-93-3 2-BUTANONE U ug/L 1.11 10 1 OC 06/08/10 104-51-8 N-BUTYLBENZENE U ug/L 0.3 10 1 OC 06/08/10 135-98-8 SEC-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/08/10 98-06-6 TERT-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/08/10 75-15-0 CARBON DISULFIDE U ug/L 0.13 10 1 OC 06/08/10 56-23-5 CARBON TETRACHLORIDE U ug/L 0.27 10 1 OC 06/08/10 108-90-7 CHLOROBENZENE U ug/L 0.16 10 1 OC 06/08/10 75-00-3 CHLOROETHANE U ug/L 0.35 10 1 OC 06/08/10 110-75-8 2-CHLOROETHYLVINYL ETHER U ug/L 1.71 10 1 OC 06/08/10 67-66-3 CHLOROFORM U ug/L 0.3 10 1 OC 06/08/10 74-87-3 CHLOROMETHANE U ug/L 0.81 10 1 OC 06/08/10 95-49-8 2-CHLOROTOLUENE U ug/L 0.24 10 1 OC 06/08/10 106-43-4 4-CHLOROTOLUENE U ug/L 0.15 10 1 OC 06/08/10 124-48-1 DIBROMOCHLOROMETHANE U ug/L 0.18 10 1 OC 06/08/10 96-12-8 1.2-DIBROMO-3-CHLOROPROPANE U ug/L 0.35 10 1 OC 06/08/10 74-95-3 DIBROMOMETHANE U ug/L 0.25 10 1 OC 06/08/10 106-93-4 1.2-DIBROMOETHANE u ug/L 0.15 10 1 OC 06/08/10 95-50-1 1.2-DICHLOROBENZENE u ug/L 5.86 10 1 OC 06/08/10 541-73-1 1.3-DICHLOROBENZENE u ug/L 5.62 10 1 OC 06/08/10 106-46-7 1.4-DICHLOROBENZENE u ug/L 5.88 10 1 OC 06/08/10 75-71-8 DICHLORODIFLUOROMETHANE u ug/L 0.66 10 1 OC 06/08/10 75-34-3 1.1-DICHLOROETHANE u ug/L 0.49 10 1 OC 06/08/10 107-06-2 1.2-DICHLOROETHANE u ug/L 0.29 10 1 OC 06/08/10 75-35-4 1.1-DICHLOROETHENE 1. J ug/L 0.16 10 1 OC 06/08/10 156-59-4 CIS-1.2-DICHLOROETH ENE u ug/L 0.16 10 1 OC 06/08/10 Page 12 of 18 Printed: 06/16/10 11:25 Listing of Results by Sample Sample Delivery Group: 1006010 Client Sample ID: TP-001 Laboratory Sample ID: 1006010-06 Date Sampled: 06/03/10 14:10 Sample Description: ATK-DLV - Groundwater Spring 2010 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 156-60-5 TRANS-1.2-DICHLOROETH ENE u ug/L 0.34 10 1 OC 06/08/10 78-87-5 1.2-DICHLOROPROPANE u ug/L 0.16 10 1 OC 06/08/10 142-28-9 1.3-DICHLOROPROPANE u ug/L 0.24 10 1 OC 06/08/10 563-58-6 1.1-DICHLOROPROPENE u ug/L 0.17 10 1 OC 06/08/10 10061-01-5 CIS-1.3-DICHLOROPROPENE u ug/L 0.4 10 1 OC 06/08/10 10061-02-6 TRANS-1.3-DICHLOROPROPENE u ug/L 0.4 10 1 OC 06/08/10 590-20-7 2.2-DICHLOROPROPANE u ug/L 0.9 10 1 OC 06/08/10 100-41-4 ETHYLBENZENE u ug/L 0.16 10 1 OC 06/08/10 591-78-6 2-HEXANONE u ug/L 0.7 10 1 OC 06/08/10 87-68-3 HEXACHLOROBUTADIENE u ug/L 0.9 10 1 OC 06/08/10 98-82-8 ISOPROPYLBENZENE u ug/L 0.58 10 1 OC 06/08/10 99-87-6 4-ISOPROPYLTOLUENE u ug/L 0.24 10 1 OC 06/08/10 75-09-2 METHYLENE CHLORIDE u ug/L 0.8 10 1 OC 06/08/10 108-10-1 4-M ETHYL-2-PEN TAN ONE u ug/L 0.53 10 1 OC 06/08/10 91-20-3 NAPHTHALENE u ug/L 4 10 1 OC 06/08/10 103-65-1 N-PROPYLBENZENE u ug/L 0.5 10 1 OC 06/08/10 100-42-5 STYRENE u ug/L 0.3 10 1 OC 06/08/10 630-20-6 1.1.1.2-TETRACHLOROETHANE u ug/L 0.25 10 1 OC 06/08/10 79-34-5 1.1.2.2-TETRACHLOROETHANE u ug/L 0.85 10 1 OC 06/08/10 127-18-4 TETRACHLOROETHENE u ug/L 0.4 10 1 OC 06/08/10 108-88-3 TOLUENE u ug/L 0.5 10 1 OC 06/08/10 87-61-6 1.2.3-TRICHLOROBENZENE u ug/L 0.23 10 1 OC 06/08/10 120-82-1 1.2.4-TRICHLOROBENZENE u ug/L 4.37 10 1 OC 06/08/10 71-55-6 1.1.1-TRICHLOROETHANE u ug/L 0.16 10 1 OC 06/08/10 79-00-5 1.1.2-TRICHLOROETHANE u ug/L 0.25 10 1 OC 06/08/10 79-01-6 TRICHLOROETHENE 15 ug/L 0.7 10 1 OC 06/08/10 75-69-4 TRICHLOROFLUOROMETHANE u ug/L 0.3 10 1 OC 06/08/10 96-18-4 1.2.3-TRICHLOROPROPANE u ug/L 0.33 10 1 OC 06/08/10 95-63-6 1.2.4-TRIM ETHYLBENZENE u ug/L 0.19 10 1 OC 06/08/10 108-67-8 1.3.5-TRIM ETHYLBENZENE u ug/L 0.29 10 1 OC 06/08/10 108-05-4 VINYL ACETATE u ug/L 20 50 1 OC 06/08/10 75-01-4 VINYL CHLORIDE u ug/L 0.3 10 1 OC 06/08/10 1330-20-7 m.p-XYLENE u ug/L 0.6 10 1 OC 06/08/10 95-47-6 o-XYLENE u ug/L 0.3 10 1 OC 06/08/10 460-00-4 BROMOFLUOROBENZENE 92.9 % 1 OC 06/08/10 1868-53-7 DIBROMOFLUOROMETHANE 101 % 1 OC 06/08/10 17060-07-0 1.2-DICHLOROETHANE-D4 108 % 1 OC 06/08/10 2037-26-5 T0LUENE-D8 96.3 % 1 OC 06/08/10 Client Sample ID: FP-001 Laboratory Sample ID: 1006010-07 Date Sampled: 06/03/10 14:15 Sample Description: ATK-DLV - Groundwater Spring 2010 Dilution CAS Number Test Parameter Result Units MDL EQL Factor Analyst Test Date TestMe^od: EPA 120.1 Conductivity CONDUCTIVITY 4.54 uS/cm 0.3 1 1 JMM 06/14/10 TestMe^od: EPA 314.0 Perchlorate - Ion Chromatography 014797-73-0 PERCHLORATE U ug/L 1 4 1 JMM 06/15/10 Page 13 of 18 Printed: 06/16/10 11:25 Listing of Results by Sample Sample Delivery Group: 1006010 Client Sample ID: FP-001 Laboratory Sample ID: 1006010-07 Sample Description: ATK-DLV - Groundwater Spring 2010 Date Sampled: 06/03/10 14:15 CAS Number Test Parameter Result Units MDL Dilution EQL Factor Analyst Test Date TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 67-64-1 ACETONE U ug/L 5 10 1 OC 06/08/10 71-43-2 BENZENE U ug/L 0.22 10 1 OC 06/08/10 74-97-5 BROMOCHLOROMETHANE U ug/L 0.31 10 1 OC 06/08/10 75-27-4 BROMODICHLOROMETHANE U ug/L 0.19 10 1 OC 06/08/10 108-86-1 BROMOBENZENE U ug/L 0.37 10 1 OC 06/08/10 75-25-2 BROMOFORM U ug/L 0.42 10 1 OC 06/08/10 74-83-9 BROMOMETHANE U ug/L 0.57 10 1 OC 06/08/10 78-93-3 2-BUTANONE U ug/L 1.11 10 1 OC 06/08/10 104-51-8 N-BUTYLBENZENE U ug/L 0.3 10 1 OC 06/08/10 135-98-8 SEC-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/08/10 98-06-6 TERT-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/08/10 75-15-0 CARBON DISULFIDE U ug/L 0.13 10 1 OC 06/08/10 56-23-5 CARBON TETRACHLORIDE U ug/L 0.27 10 1 OC 06/08/10 108-90-7 CHLOROBENZENE U ug/L 0.16 10 1 OC 06/08/10 75-00-3 CHLOROETHANE U ug/L 0.35 10 1 OC 06/08/10 110-75-8 2-CHLOROETHYLVINYL ETHER U ug/L 1.71 10 1 OC 06/08/10 67-66-3 CHLOROFORM U ug/L 0.3 10 1 OC 06/08/10 74-87-3 CHLOROMETHANE U ug/L 0.81 10 1 OC 06/08/10 95-49-8 2-CHLOROTOLUENE U ug/L 0.24 10 1 OC 06/08/10 106-43-4 4-CHLOROTOLUENE U ug/L 0.15 10 1 OC 06/08/10 124-48-1 DIBROMOCHLOROMETHANE U ug/L 0.18 10 1 OC 06/08/10 96-12-8 1.2-DIBROMO-3-CHLOROPROPANE U ug/L 0.35 10 1 OC 06/08/10 74-95-3 DIBROMOMETHANE U ug/L 0.25 10 1 OC 06/08/10 106-93-4 1.2-DIBROMOETHANE U ug/L 0.15 10 1 OC 06/08/10 95-50-1 1.2-DICHLOROBENZENE U ug/L 5.86 10 1 OC 06/08/10 541-73-1 1.3-DICHLOROBENZENE U ug/L 5.62 10 1 OC 06/08/10 106-46-7 1.4-DICHLOROBENZENE u ug/L 5.88 10 1 OC 06/08/10 75-71-8 DICHLORODIFLUOROMETHANE u ug/L 0.66 10 1 OC 06/08/10 75-34-3 1.1-DICHLOROETHANE u ug/L 0.49 10 1 OC 06/08/10 107-06-2 1.2-DICHLOROETHANE u ug/L 0.29 10 1 OC 06/08/10 75-35-4 1.1-DICHLOROETHENE u ug/L 0.16 10 1 OC 06/08/10 156-59-4 CIS-1.2-DICHLOROETH ENE u ug/L 0.16 10 1 OC 06/08/10 156-60-5 TRANS-1.2-DICHLOROETH ENE u ug/L 0.34 10 1 OC 06/08/10 78-87-5 1.2-DICHLOROPROPANE u ug/L 0.16 10 1 OC 06/08/10 142-28-9 1.3-DICHLOROPROPANE u ug/L 0.24 10 1 OC 06/08/10 563-58-6 1.1-DICHLOROPROPENE u ug/L 0.17 10 1 OC 06/08/10 10061-01-5 CIS-1.3-DICHLOROPROPENE u ug/L 0.4 10 1 OC 06/08/10 10061-02-6 TRANS-1.3-DICHLOROPROPENE u ug/L 0.4 10 1 OC 06/08/10 590-20-7 2.2-DICHLOROPROPANE u ug/L 0.9 10 1 OC 06/08/10 100-41-4 ETHYLBENZENE u ug/L 0.16 10 1 OC 06/08/10 591-78-6 2-HEXANONE u ug/L 0.7 10 1 OC 06/08/10 87-68-3 HEXACHLOROBUTADIENE u ug/L 0.9 10 1 OC 06/08/10 98-82-8 ISOPROPYLBENZENE u ug/L 0.58 10 1 OC 06/08/10 99-87-6 4-ISOPROPYLTOLUENE u ug/L 0.24 10 1 OC 06/08/10 75-09-2 METHYLENE CHLORIDE u ug/L 0.8 10 1 OC 06/08/10 108-10-1 4-M ETHYL-2-PEN TAN ONE u ug/L 0.53 10 1 OC 06/08/10 91-20-3 NAPHTHALENE u ug/L 4 10 1 OC 06/08/10 103-65-1 N-PROPYLBENZENE u ug/L 0.5 10 1 OC 06/08/10 100-42-5 STYRENE u ug/L 0.3 10 1 OC 06/08/10 630-20-6 1.1.1.2-TETRACHLOROETHANE u ug/L 0.25 10 1 OC 06/08/10 Page 14 of 18 Printed: 06/16/10 11:25 Listing of Results by Sample Sample Delivery Group: 1006010 Client Sample ID: FP-001 Laboratory Sample ID: 1006010-07 Sample Description: ATK-DLV - Groundwater Spring 2010 Date Sampled: 06/03/10 14:15 CAS Number Test Parameter Result Units MDL Dilution EQL Factor Analyst Test Date TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 79-34-5 1.1.2.2-TETRACHLOROETHANE U ug/L 0.85 10 1 OC 06/08/10 127-18-4 TETRACHLOROETHENE U ug/L 0.4 10 1 OC 06/08/10 108-88-3 TOLUENE U ug/L 0.5 10 1 OC 06/08/10 87-61-6 1.2.3-TRICHLOROBENZENE U ug/L 0.23 10 1 OC 06/08/10 120-82-1 1.2.4-TRICHLOROBENZENE U ug/L 4.37 10 1 OC 06/08/10 71-55-6 1.1.1-TRICHLOROETHANE U ug/L 0.16 10 1 OC 06/08/10 79-00-5 1.1.2-TRICHLOROETHANE U ug/L 0.25 10 1 OC 06/08/10 79-01-6 TRICHLOROETHENE 8.8 J ug/L 0.7 10 1 OC 06/08/10 75-69-4 TRICHLOROFLUOROMETHANE U ug/L 0.3 10 1 OC 06/08/10 96-18-4 1.2.3-TRICHLOROPROPANE U ug/L 0.33 10 1 OC 06/08/10 95-63-6 1.2.4-TRIM ETHYLBENZENE U ug/L 0.19 10 1 OC 06/08/10 108-67-8 1.3.5-TRIM ETHYLBENZENE U ug/L 0.29 10 1 OC 06/08/10 108-05-4 VINYL ACETATE U ug/L 20 50 1 OC 06/08/10 75-01-4 VINYL CHLORIDE U ug/L 0.3 10 1 OC 06/08/10 1330-20-7 m.p-XYLENE U ug/L 0.6 10 1 OC 06/08/10 95-47-6 o-XYLENE U ug/L 0.3 10 1 OC 06/08/10 460-00-4 BROMOFLUOROBENZENE 96.2 % 1 OC 06/08/10 1868-53-7 DIBROMOFLUOROMETHANE 106 % 1 OC 06/08/10 17060-07-0 1.2-DICHLOROETHANE-D4 108 % 1 OC 06/08/10 2037-26-5 T0LUENE-D8 98.4 % 1 OC 06/08/10 Client Sample ID: B-6 Laboratory Sample ID: 1006010-08 Sample Description: ATK-DLV - Groundwater Spring 2010 Date Sampled: 06/03/10 14:45 CAS Number TestMe^od: TestMe^od: 014797-73-0 TestMe^od: Test Parameter EPA 120.1 CONDUCTIVITY EPA 314.0 PERCHLORATE SW-846, 8260B (Water) Result Units MDL EQL Conductivity 7100 uS/cm 0.3 1 Perchlorate - Ion Chromatography 43600. ug/L 100 400 Volatile Organic Analysis Dilution Factor Analyst Test Date 100 JMM JMM 06/14/10 06/15/10 67-64-1 ACETONE U ug/L 5 10 1 OC 06/08/10 71-43-2 BENZENE 0.6 J ug/L 0.22 10 1 OC 06/08/10 74-97-5 BROMOCHLOROMETHANE U ug/L 0.31 10 1 OC 06/08/10 75-27-4 BROMODICHLOROMETHANE U ug/L 0.19 10 1 OC 06/08/10 108-86-1 BROMOBENZENE U ug/L 0.37 10 1 OC 06/08/10 75-25-2 BROMOFORM U ug/L 0.42 10 1 OC 06/08/10 74-83-9 BROMOMETHANE U ug/L 0.57 10 1 OC 06/08/10 78-93-3 2-BUTANONE U ug/L 1.11 10 1 OC 06/08/10 104-51-8 N-BUTYLBENZENE U ug/L 0.3 10 1 OC 06/08/10 135-98-8 SEC-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/08/10 98-06-6 TERT-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/08/10 75-15-0 CARBON DISULFIDE U ug/L 0.13 10 1 OC 06/08/10 56-23-5 CARBON TETRACHLORIDE 0.8 J ug/L 0.27 10 1 OC 06/08/10 108-90-7 CHLOROBENZENE U ug/L 0.16 10 1 OC 06/08/10 75-00-3 CHLOROETHANE U ug/L 0.35 10 1 OC 06/08/10 110-75-8 2-CHLOROETHYLVINYL ETHER U ug/L 1.71 10 1 OC 06/08/10 67-66-3 CHLOROFORM 19.7 ug/L 0.3 10 1 OC 06/08/10 Page 1 Printed: 06/16/10 11:25 Listing of Results by Sample Sample Delivery Group: 1006010 Client Sample ID: B-6 Laboratory Sample ID: 1006010-08 Sample Description: ATK-DLV - Groundwater Spring 2010 Date Sampled: 06/03/10 14:45 CAS Number Test Parameter Result Units MDL EQL Dilution Factor Analyst Test Date TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 74-87-3 CHLOROMETHANE U ug/L 0.81 10 1 OC 06/08/10 95-49-8 2-CHLOROTOLUENE U ug/L 0.24 10 1 OC 06/08/10 106-43-4 4-CHLOROTOLUENE U ug/L 0.15 10 1 OC 06/08/10 124-48-1 DIBROMOCHLOROMETHANE U ug/L 0.18 10 1 OC 06/08/10 96-12-8 1.2-DIBROMO-3-CHLOROPROPANE U ug/L 0.35 10 1 OC 06/08/10 74-95-3 DIBROMOMETHANE U ug/L 0.25 10 1 OC 06/08/10 106-93-4 1.2-DIBROMOETHANE U ug/L 0.15 10 1 OC 06/08/10 95-50-1 1.2-DICHLOROBENZENE U ug/L 5.86 10 1 OC 06/08/10 541-73-1 1.3-DICHLOROBENZENE U ug/L 5.62 10 1 OC 06/08/10 106-46-7 1.4-DICHLOROBENZENE U ug/L 5.88 10 1 OC 06/08/10 75-71-8 DICHLORODIFLUOROMETHANE U ug/L 0.66 10 1 OC 06/08/10 75-34-3 1.1-DICHLOROETHANE 12.2 ug/L 0.49 10 1 OC 06/08/10 107-06-2 1.2-DICHLOROETHANE 1.7 J ug/L 0.29 10 1 OC 06/08/10 75-35-4 1.1-DICHLOROETHENE 21.7 ug/L 0.16 10 1 OC 06/08/10 156-59-4 CIS-1.2-DICHLOROETH ENE 35.4 ug/L 0.16 10 1 OC 06/08/10 156-60-5 TRANS-1.2-DICHLOROETH ENE 4.8 J ug/L 0.34 10 1 OC 06/08/10 78-87-5 1.2-DICHLOROPROPANE U ug/L 0.16 10 1 OC 06/08/10 142-28-9 1.3-DICHLOROPROPANE U ug/L 0.24 10 1 OC 06/08/10 563-58-6 1.1-DICHLOROPROPENE U ug/L 0.17 10 1 OC 06/08/10 10061-01-5 CIS-1.3-DICHLOROPROPENE U ug/L 0.4 10 1 OC 06/08/10 10061-02-6 TRANS-1.3-DICHLOROPROPENE U ug/L 0.4 10 1 OC 06/08/10 590-20-7 2.2-DICHLOROPROPANE U ug/L 0.9 10 1 OC 06/08/10 100-41-4 ETHYLBENZENE U ug/L 0.16 10 1 OC 06/08/10 591-78-6 2-HEXANONE U ug/L 0.7 10 1 OC 06/08/10 87-68-3 HEXACHLOROBUTADIENE U ug/L 0.9 10 1 OC 06/08/10 98-82-8 ISOPROPYLBENZENE U ug/L 0.58 10 1 OC 06/08/10 99-87-6 4-ISOPROPYLTOLUENE U ug/L 0.24 10 1 OC 06/08/10 75-09-2 METHYLENE CHLORIDE U ug/L 0.8 10 1 OC 06/08/10 108-10-1 4-M ETHYL-2-PEN TAN ONE U ug/L 0.53 10 1 OC 06/08/10 91-20-3 NAPHTHALENE U ug/L 4 10 1 OC 06/08/10 103-65-1 N-PROPYLBENZENE U ug/L 0.5 10 1 OC 06/08/10 100-42-5 STYRENE U ug/L 0.3 10 1 OC 06/08/10 630-20-6 1.1.1.2-TETRACHLOROETHANE U ug/L 0.25 10 1 OC 06/08/10 79-34-5 1.1.2.2-TETRACHLOROETHANE U ug/L 0.85 10 1 OC 06/08/10 127-18-4 TETRACHLOROETHENE U ug/L 0.4 10 1 OC 06/08/10 108-88-3 TOLUENE U ug/L 0.5 10 1 OC 06/08/10 87-61-6 1.2.3-TRICHLOROBENZENE U ug/L 0.23 10 1 OC 06/08/10 120-82-1 1.2.4-TRICHLOROBENZENE U ug/L 4.37 10 1 OC 06/08/10 71-55-6 1.1.1-TRICHLOROETHANE 140. J ug/L 3.2 200 20 OC 06/08/10 79-00-5 1.1.2-TRICHLOROETHANE U ug/L 0.25 10 1 OC 06/08/10 79-01-6 TRICHLOROETHENE 2220 ug/L 14 200 20 OC 06/08/10 75-69-4 TRICHLOROFLUOROMETHANE U ug/L 0.3 10 1 OC 06/08/10 96-18-4 1.2.3-TRICHLOROPROPANE U ug/L 0.33 10 1 OC 06/08/10 95-63-6 1.2.4-TRIM ETHYLBENZENE U ug/L 0.19 10 1 OC 06/08/10 108-67-8 1.3.5-TRIM ETHYLBENZENE U ug/L 0.29 10 1 OC 06/08/10 108-05-4 VINYL ACETATE U ug/L 20 50 1 OC 06/08/10 75-01-4 VINYL CHLORIDE U ug/L 0.3 10 1 OC 06/08/10 1330-20-7 m.p-XYLENE U ug/L 0.6 10 1 OC 06/08/10 95-47-6 o-XYLENE U ug/L 0.3 10 1 OC 06/08/10 460-00-4 BROMOFLUOROBENZENE 95.4 % 1 OC 06/08/10 Page 16 of 18 Printed: 06/16/10 11:25 Listing of Results by Sample Sample Delivery Group: 1006010 Client Sample ID: B-6 Sample Description: ATK-DLV - Groundwater Spring 2010 Laboratory Sample ID: Date Sampled: 1006010-08 06/03/10 14:45 CAS Number Test Parameter Result Units MDL EQL Dilution Factor Analyst Test Date TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 1868-53-7 DIBROMOFLUOROMETHANE 107 % 17060-07-0 1.2-DICHLOROETHANE-D4 113 % 2037-26-5 T0LUENE-D8 95.8 % OC OC OC 06/08/10 06/08/10 06/08/10 Page 1 / of 18 Printed: 06/16/10 11:25 Data Reporting Qualifiers U Indicates that the analyte concentration is less than the MDL. B This flag is used when an analyte is found in the blank as well as the sample. Indicates an extimated value. This flag is used either when estimating a concentration for tentatively identified compounds or when the data indicated the presence of a compound that meets the identification criteria but the result is less than the EQL (e.g. 3 J with an EQL of 10). MDL Method Detection Limit: The minimum concentration of a substance that can be confidently measured and reported. The laboratory has demonstrated that the MDL can be achieved in a laboratory reagent blank, but does not guarantee it can be achieved in all sample matrices. EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many analytes the EQL is selected as the value of the lowest standard in the calibration cuh/e. Dilution Dilution Factor: The prepared sample was diluted by this factor because the Factor sample was too concentrated or due to other interferences in the sample matrix. Any dilution factor causes a corresponding increase in the MDL and EQL. Page 18 of 18 Printed: 06/16/10 11:25 ATK Launch Systems Environmental Laboratory Sample Receipt Checklist Client Name: SDG No. Carrier: Carrier Number: • Hand delivered, no cooler • Hand delivered, sample(s) taken out at receiving counter Cooler Information: ^ Cooler Number/ID: ^ /fA^ ^ IAJ • Not Applicable • Not Applicable • Not Applicable •Damaged (explain) _ Condition of Shipping Container: ^[^ood Cooler Sealed (taped): DYes Custody Seals Present: DYes •Intact Coolant: ^ce State of Coolant: • Frozen J^fartially Frozen •Melted Thermometer ID: Reading:, Packing Description: ^^^,1. jW( 4^ •Fair ^0 ^0 •Broken •Blue Ice •None jSpartially Frozen °C CF: Seal Number:. Other: Corrected Temp:_ Temp Blank Included: nYes •No Chain-Of-Custody Information: COC Present: r t ^ / f -7 COC Number(s): k I 3 ( UV COC signed (relinquished and received): COC or LWI agrees with sample labels: '^es Notes: • No • No • No Other: •Not Applicable •Not Applicable Sample Information: Samples included in cooler: 1 C^OO>0/0 Custody Seals Present: nYes •Intact Sample containers intact: ^es Samples in proper containers: ^es Sufficient sample volume: )j^es All samples received in hold time: Water - VOA's have zero headspace: /Spre-preserved with HCI: Notes: j3<tvio Other • Broken Seal Number(s) _ • No Notes: • No • No • No XYes •No •Not Applicable •Pre-preserved with Na2S203: • Non-Preserved: Water - pH acceptable upon receipt: nYes DAdjusted (see comments below) ^ot Applicable HNO3 = H2SO4 = NaOH = ZnAC /NaOH = HCL = Water - pH adjusted: (mfg. & Lot No.) HNO3 H2SO4 Na2S0203 Other _ Notes: _NaOH _ _ZnAC _ _HCL SOP-102 Form A 1006010 ENVIRONMENTAL LAB WORK REQUEST ATK ENVIRONMENTAL LABORATORY ..... LWR No. Login No. E13167 FROM: EXTENSION COST CENTER 6zoa WORK ORDER DATE ORGANIZATION MAIL STOP Jtoi REPORT RESULTS TO: HELEN RAVSTEN, MS 301 SAMPLE INFORMATION SAMPLE DATE TYPE LOCATION TIME TEST REMARKS SAMPLE DATE G C LOCATION TIME TEST REMARKS 6e£^ai(»ckefi(ati^iic^ . J H ft ft ''^ izso a ic ^ IHOO ff a (( u IHOS - T?-co\ n ,r (( (( u « g-6> (( (( ^( 9. 10. 11.. 12. CHAIN OF CUSTODY ^^ft^NQUISHED^Y DATE TIME RECEIVED BY DATE TIME i i FOR LABORATORY USE ONLY DATE COMPLETED DATE REPORTED 2010 Spring GW Samj^ling ATK Laxinch Systems, line. Promontory, UTAJ^I (801) 251-5688i SAMPLE NUMBER: J>- ( DATE: ^/[O SAMPLER: 1006010 ANALYTICAL LABORATORY: ATK Environmental La] Doratory M53 Bottle Number No. of Containers Fid. Preservative/ Treatment Reque sted Analysis 11 3 4 degrees C Acidified .2 mL HCL VOA, Appendix 9 Method 8260 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314.0 SAMPLE NUMBER: 2010 Spring GW Samj^ling ATK Launch Systems,jlnc. Promontory, UTA? (801) 251-5688: DATE SAMPLER: 1006010 ANALYTICAL LABORATORY: ATK Environmental La] Doratory M53 Bottle Number No, of Containers Fid. Pre s ervat ive/ Treatment Reque sted Analysis 11 3 4 degrees C Acidified .2 mL HCL VOA, Appendix 9 Method 8260 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314.0 2010 Spring GW Samplling ATK La\inch Systems, Inc. Promontory, UTAH (801) 251-5688 SAMPLE NUMBER: ^'Zl> DATE: ^/g-S/jP SAMPLER: 1006010 ANALYTICAL LABORATORY: ATK Environmental La] Doratory M53 Bottle Number No. of Containers Fid. Pre s ervat ive/ Treatment Reque sted Analysis 11 3 4 degrees C Acidified ,2 mL HCL VOA, Appendix 9 Method 8260 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314.0 2010 Spring GW Sampling ATK Laxinch Systems, line. Promontory, UTAH (801) 251-5688 SAMPLE NUMBER: ^"Z DATE: jjO SAMPLER; 1006010 ANALYTICAL LABORATORY: ATK Environmental La] Doratory M53 Bottle Number No. of Containers Fid. Preservative/ Treatment Reque sted Analysis 11 3 4 degrees C Acidified ,2 mL HCL VOA, Appendix 9 Method 8260 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314.0 2010 Spring GW Sampling ATK Launch Systems/ Inc, Promontory, UTAH (801) 251-5688 SAMPLE NUMBER: DATE: SAMPLER; 1006010 ANALYTICAL LABORATORY: ATK Environmental Laboratory M53 Bottle Number No. of Containers Fid. Pre s ervat ive/ Treatment Requested Analysis 11 3 4 degrees C VOA, Appendix 9 Acidified Method 8260 .2 mL HCL 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314.0 2010 Spring GW Sampling ATK Launch Systems, Inc. Promontory, UTAH (801) 251-5688 SAMPLE NUMBER: /P-CO( DATE: -Osf^ SAMPLER: OA 1006010 ANALYTICAL LABORATORY: ATK Environmental Laboratory MS3 Bottle Number No. of Containers Fid. Preservative/ Treatment Requested Analysis 11 3 4 degrees C VOA, Appendix 9 Acidified Method 8260 .2 mL HCL 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314.0 2010 Spring GW Sampling ATK Launch Systems, Inc. Promontory, UTAH (801) 251-5688 SAMPLE NUMBER: fp-COi DATE: JS/)0 SAMPLER: 1006010 ANALYTICAL LABORATORY: ATK Environmental Laboratory M53 Bottle Number No. of Containers Fid. Preservative/ Treatment Requested Analysis 11 3 4 degrees C VOA, Appendix 9 Acidified Method 8260 .2 mL HCL 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314.0 2010 Spring GW Sampling ATK Launch Systems, Inc. Promontory, UTAH (801) 251-5688 SAMPLE NUMBER DATE SAMPLER: 1006010 ANALYTICAL LABORATORY: ATK Environmental Laboratory M53 Bottle Number No. of Containers Fid. Preservative/ Treatment Requested Analysis 11 3 4 degrees C VOA, Appendix 9 Acidified Method 8260 ,2 mL HCL 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314.0 988P LS333 GW CERTIFICATE OF ANALYSIS Listing of Sample Information and Testing Requested Wednesday, June 16, 2010 TESTED FOR: ATK: DLV Environmental Monitoring Thiokol Corp, UT 84322 ANALYZED BY: ATK Launch Systems Analytical Chemistry Laboratory P.O. Box 707, M/S 245 Brigham City, UT 84302-0707 435-863-3732 435-863-8080 Contact Name: Project: Sample Delivery Group: Al Lee Ground Water Testing - DLV 1006011 Page 1 of 5 Printed: 06/16/10 11:26 Sample Delivery Group: 1006011 Sample No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 1006011-01 A-8 06/04/10 6/4/2010 14:00:41 EPA 120.1 EPA 314.0 SW-846. 8260B (Water) Conductivity Perchlorate - Ion Chromatography Volatile Organic Analysis Water Water Water Certified By: W. Scott Fraser, Quality Assurance Officer 06/17/2010 Date This ceiiifies that the following data meets the requirements of the National Environmental Laboratoiy Accreditation Program (NELAP) unless otherwise annotated: Page 2 of 5 Printed: 06/16/10 11:26 Listing of Results by Sample Sample Delivery Group: 1006011 Client Sample ID: A-8 Sample Description: ATK-DLV - Groundwater Spring 2010 Laboratory Sample ID: 1006011-01 Date Sampled: 06/04/10 14:00 AS Number Test Parameter Result Units MDL EQL Dilution Factor Analvst Test Date TestMe^od: EPA 120.1 Conductivity CONDUCTIVITY 1200 uS/cm 0.3 1 1 JMM 06/14/10 TestMe^od: EPA 314.0 Perchlorate-Ion Chromatography 014797-73-0 PERCHLORATE 8520. ug/L 100 400 100 JMM 06/15/10 TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 67-64-1 ACETONE U ug/L 5 10 1 OC 06/08/10 71-43-2 BENZENE 3.4 J ug/L 0.22 10 1 OC 06/08/10 74-97-5 BROMOCHLOROMETHANE U ug/L 0.31 10 1 OC 06/08/10 75-27-4 BROMODICHLOROMETHANE U ug/L 0.19 10 1 OC 06/08/10 108-86-1 BROMOBENZENE U ug/L 0.37 10 1 OC 06/08/10 75-25-2 BROMOFORM U ug/L 0.42 10 1 OC 06/08/10 74-83-9 BROMOMETHANE U ug/L 0.57 10 1 OC 06/08/10 78-93-3 2-BUTANONE U ug/L 1.11 10 1 OC 06/08/10 104-51-8 N-BUTYLBENZENE U ug/L 0.3 10 1 OC 06/08/10 135-98-8 SEC-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/08/10 98-06-6 TERT-BUTYLBENZENE U ug/L 0.4 10 1 OC 06/08/10 75-15-0 CARBON DISULFIDE U ug/L 0.13 10 1 OC 06/08/10 56-23-5 CARBON TETRACHLORIDE 6.5 J ug/L 0.27 10 1 OC 06/08/10 108-90-7 CHLOROBENZENE 1. J ug/L 0.16 10 1 OC 06/08/10 75-00-3 CHLOROETHANE U ug/L 0.35 10 1 OC 06/08/10 110-75-8 2-CHLOROETHYLVINYL ETHER U ug/L 1.71 10 1 OC 06/08/10 67-66-3 CHLOROFORM 142 ug/L 0.3 10 1 OC 06/08/10 74-87-3 CHLOROMETHANE U ug/L 0.81 10 1 OC 06/08/10 95-49-8 2-CHLOROTOLUENE U ug/L 0.24 10 1 OC 06/08/10 106-43-4 4-CHLOROTOLUENE U ug/L 0.15 10 1 OC 06/08/10 124-48-1 DIBROMOCHLOROMETHANE U ug/L 0.18 10 1 OC 06/08/10 96-12-8 1.2-DIBROMO-3-CHLOROPROPANE U ug/L 0.35 10 1 OC 06/08/10 74-95-3 DIBROMOMETHANE U ug/L 0.25 10 1 OC 06/08/10 106-93-4 1.2-DIBROMOETHANE U ug/L 0.15 10 1 OC 06/08/10 95-50-1 1.2-DICHLOROBENZENE U ug/L 5.86 10 1 OC 06/08/10 541-73-1 1.3-DICHLOROBENZENE U ug/L 5.62 10 1 OC 06/08/10 106-46-7 1.4-DICHLOROBENZENE U ug/L 5.88 10 1 OC 06/08/10 75-71-8 DICHLORODIFLUOROMETHANE U ug/L 0.66 10 1 OC 06/08/10 75-34-3 1.1-DICHLOROETHANE 51 ug/L 0.49 10 1 OC 06/08/10 107-06-2 1.2-DICHLOROETHANE 8.4 J ug/L 0.29 10 1 OC 06/08/10 75-35-4 1.1-DICHLOROETHENE 543 ug/L 8 500 50 OC 06/08/10 156-59-4 CIS-1.2-DICHLOROETH ENE 21.3 ug/L 0.16 10 1 OC 06/08/10 156-60-5 TRANS-1.2-DICHLOROETH ENE U ug/L 0.34 10 1 OC 06/08/10 78-87-5 1.2-DICHLOROPROPANE U ug/L 0.16 10 1 OC 06/08/10 142-28-9 1.3-DICHLOROPROPANE U ug/L 0.24 10 1 OC 06/08/10 563-58-6 1.1-DICHLOROPROPENE U ug/L 0.17 10 1 OC 06/08/10 10061-01-5 CIS-1.3-DICHLOROPROPENE U ug/L 0.4 10 1 OC 06/08/10 10061-02-6 TRANS-1.3-DICHLOROPROPENE U ug/L 0.4 10 1 OC 06/08/10 590-20-7 2.2-DICHLOROPROPANE U ug/L 0.9 10 1 OC 06/08/10 100-41-4 ETHYLBENZENE U ug/L 0.16 10 1 OC 06/08/10 591-78-6 2-HEXANONE U ug/L 0.7 10 1 OC 06/08/10 87-68-3 HEXACHLOROBUTADIENE U ug/L 0.9 10 1 OC 06/08/10 98-82-8 ISOPROPYLBENZENE U ug/L 0.58 10 1 OC 06/08/10 99-87-6 4-ISOPROPYLTOLUENE U ug/L 0.24 10 1 OC 06/08/10 75-09-2 METHYLENE CHLORIDE U ug/L 0.8 10 1 OC 06/08/10 Page 3 of 5 Printed: 06/16/10 11:26 Listing of Results by Sample Sample Delivery Group: 1006011 Client Sample ID: A-8 Laboratory Sample ID: 1006011-01 Sample Description: ATK-DLV - Groundwater Spring 2010 Date Sampled: 06/04/10 14:00 CAS Number Test Parameter Result Units MDL EQL Dilution Factor Analyst Test Date TestMe^od: SW-846, 8260B (Water) Volatile Organic Analysis 108-10-1 4-M ETHYL-2-PEN TAN ONE U ug/L 0.53 10 1 OC 06/08/10 91-20-3 NAPHTHALENE U ug/L 4 10 1 OC 06/08/10 103-65-1 N-PROPYLBENZENE U ug/L 0.5 10 1 OC 06/08/10 100-42-5 STYRENE U ug/L 0.3 10 1 OC 06/08/10 630-20-6 1.1.1.2-TETRACHLOROETHANE U ug/L 0.25 10 1 OC 06/08/10 79-34-5 1.1.2.2-TETRACHLOROETHANE U ug/L 0.85 10 1 OC 06/08/10 127-18-4 TETRACHLOROETHENE 2.8 J ug/L 0.4 10 1 OC 06/08/10 108-88-3 TOLUENE U ug/L 0.5 10 1 OC 06/08/10 87-61-6 1.2.3-TRICHLOROBENZENE U ug/L 0.23 10 1 OC 06/08/10 120-82-1 1.2.4-TRICHLOROBENZENE U ug/L 4.37 10 1 OC 06/08/10 71-55-6 1.1.1-TRICHLOROETHANE 811 ug/L 8 500 50 OC 06/08/10 79-00-5 1.1.2-TRICHLOROETHANE 3.7 J ug/L 0.25 10 1 OC 06/08/10 79-01-6 TRICHLOROETHENE 4490 ug/L 35 500 50 OC 06/08/10 75-69-4 TRICHLOROFLUOROMETHANE 1. J ug/L 0.3 10 1 OC 06/08/10 96-18-4 1.2.3-TRICHLOROPROPANE U ug/L 0.33 10 1 OC 06/08/10 95-63-6 1.2.4-TRIM ETHYLBENZENE U ug/L 0.19 10 1 OC 06/08/10 108-67-8 1.3.5-TRIM ETHYLBENZENE U ug/L 0.29 10 1 OC 06/08/10 108-05-4 VINYL ACETATE U ug/L 20 50 1 OC 06/08/10 75-01-4 VINYL CHLORIDE U ug/L 0.3 10 1 OC 06/08/10 1330-20-7 m.p-XYLENE U ug/L 0.6 10 1 OC 06/08/10 95-47-6 o-XYLENE U ug/L 0.3 10 1 OC 06/08/10 460-00-4 BROMOFLUOROBENZENE 95.3 % 1 OC 06/08/10 1868-53-7 DIBROMOFLUOROMETHANE 104 % 1 OC 06/08/10 17060-07-0 1.2-DICHLOROETHANE-D4 110 % 1 OC 06/08/10 2037-26-5 T0LUENE-D8 97.1 % 1 OC 06/08/10 Page 4 of 5 Printed: 06/16/10 11:26 Data Reporting Qualifiers U Indicates that the analyte concentration is less than the MDL. B This flag is used when an analyte is found in the blank as well as the sample. Indicates an extimated value. This flag is used either when estimating a concentration for tentatively identified compounds or when the data indicated the presence of a compound that meets the identification criteria but the result is less than the EQL (e.g. 3 J with an EQL of 10). MDL Method Detection Limit: The minimum concentration of a substance that can be confidently measured and reported. The laboratory has demonstrated that the MDL can be achieved in a laboratory reagent blank, but does not guarantee it can be achieved in all sample matrices. EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many analytes the EQL is selected as the value of the lowest standard in the calibration cuh/e. Dilution Dilution Factor: The prepared sample was diluted by this factor because the Factor sample was too concentrated or due to other interferences in the sample matrix. Any dilution factor causes a corresponding increase in the MDL and EQL. Page 5 of 5 Printed: 06/16/10 11:26 ATK Launch Systems Environmental Laboratory Sample Receipt Checklist e:/fn^ LaU^cU ^ef<^lt^$- I^LV SDG NO. Client Name: Carrier: • Hand delivered, no cooler Carrier Number: • Hand delivered, sample(s) taken out at receiving counter •Fair J^No ;^o •Broken •Blue Ice nNone •Not Applicable •Not Applicable •Not Applicable Cooler Information: Cooler Number/ID: Condition of Shipping Container: fcood Cooler Sealed (taped): nYes Custody Seals Present: nYes • Intact Coolant: iS)ce State of Coolant: • Frozen ^Partially Frozen • Melted Thermometer ID: Reading:. »C CF: Packing Description: •Damaged (explain). Seal Number:. Other: Corrected Temp:_ Temp Blank Included: DYes DNo Chain-Of-Custody Information: COC Present: r ^ / j C> COC Number(s): A/3/ COC signed (relinquished and received): COC or LWI agrees with sample labels: Notes: • No •No •No Other: •Not Applicable •Not Applicable Sample Information: Samples included in cooler: Custody Seals Present: Sample containers intact: Samples in proper containers: Sufficient sample volume: All samples received in hold time: Water - VOA's have zero headspace: cS^Pre-preserved with HCI: Notes: ^ •Yes • Intact [)(Yes ;<Yes 5fYes ^es ]JjMo Other •Broken Seal Number(s) _ •No Notes: •No • No • No ;jf^es UNO • Not Applicable [jPre-preserved with Na2S203: •Non-Preserved: Water - pH acceptable upon receipt: •Yes •Adjusted (see comments below) pl(fJot Applicable HNO3 = H2SO4 = NaOH = ZnAC /NaOH = HCL = Water - pH adjusted: (mfg. & Lot No.) HNO3 H2SO4 _ Na2S0203 Other _ Notes: NaOH ZnAC HCI SOP-102 Form A //(? 1006011 ENVIRONMENTAL LAB WORK REQUEST ATK ENVIRONMENTAL LABORATORY LWR No. Login No. E13168 FROM: y EXTENSION COST CENTER WORKORDER DATE / / ORGANIZATION ^ui^v\me*%i^ Seiroic&S MAIL STOP ^/ REPORT RESULTS TO: HELEN RAVSTEN, MS 301 SAMPLE INFORMATION SAMPLE DATE TYPE LOCATION TIME TEST REMARKS SAMPLE DATE G C LOCATION TIME TEST REMARKS 2. J 3. 4. 5. 6. 7. 8. 9. 10. 11.. 12. CHAIN OF CUSTODY J^jIyj^UISHED^ DATE TIME RECEIVED BY DATE TIME /Yso , i FOR LABORATORY USE ONLY DATE COMPLETED DATE REPORTED SAMPLE NUMBER 2010 Spring GW Sampling ATK Launch Systems/ Inc. Promontory, UTAH (801) 251-5688 DATE; SAMPLER: 1006011 ANALYTICAL LABORATORY: ATK Environmental Laboratory M53 Bottle Number No. Of Containers Fid. Preservative/ Treatment Requested Analysis 11 3 4 degrees C VOA, Appendix 9 Acidified Method 8260 .2 mL HCL 9 1 4 degrees C Perchlorate, Conductivity EPA Method 314.0