DSHW-2009-008865 - 0901a0688013bc6e

ATK
ALLIANT TSCHSYSTEMS
Alliant Aerospace Company
P.O. Box 98
Magna, UT 84044-0098
Tel [phone]
HAND DELIVERED
DEC 5 2002
02^^733.
Utah Division of Solid
and Hazardous Vv'aste
December 4, 2002
Dennis R. Downs, Director
Department of Environmental Quality
Division of Solid and Hazardous Waste
288 North 1460 West
P.O. Box 144880
Salt Lake City, Utah
84114-4880
RE: BW-1 Landflll Area Closure Report Response to Comments
ATK - Thiokol propulsion, Bacchus Works, EPA ID# UTDOO 1705029
Dear Mr. Downs,
This submittal is an addendum to the BW-1 Closure Report Comments ATK submitted to the
Utah Division of Solid and Hazardous Waste (the Division) on November 8, 2002. ATK is
submitting two copies of the response to the BW-1 Closure Report Comments covering the
QA/QC report request. The comments were submitted to ATK by the Utah Division of Solid
and Hazardous Waste (the Division) in a letter dated September 27, 2002.
The QA/QC report that was requested is attached. In addition, through further investigation, a
copy ofthe 1987 Figure 1 (Hercules Bacchus Works Sampling Locations - Soil Gas 1987) from
the Tracer Research Corporation Report was located in archives and is attached.
With the finding of Figure 1, ATK will complete the soil gas comparison requested in the
comments by the Division (Risk Assessment and Source Assessment, Item 3, bullet 2) between
soil gas data collected in 1987 and the soil gas data collected in 2001. The comparison and
update to Chapter 4 of the BW-1 Closure Report will be submitted by February 4, 2003.
Please pull and replace the following pages from the original final closure report for the BW-1
Landfill dated December 2001:
• Table of Contents
• add Figure 1 - Hercules Bacchus Works Sampling Locations - Soil Gas 1987 to Volume 2
Plates
• add Appendix F to Volume 2 - QA/QC Report
If you have any questions or need additional information conceming this issue, please contact
Allen Lee at 251-5688.
Sincerely,
Susan E. Jew, Director
Environmental Services
CLOSURE REPORT FOR THE
BW-1 LANDFILL AREA
Alliant Techsystems inc.
West Valley City, Utah
Prepared by
ALLIANT TECHSYSTEMS INC.
West Valley City, Utah
And
EARTHFAX ENGINEERING, INC.
Midvale, Utah
December13, 2001
Alliant Techsystems Inc, BW-1 Closure Report
Bacchus Works Revised December 5, 2002
TABLE OF CONTENTS
Section Paqe
CHAPTER 1 -INTRODUCTION 1-1
1.1 PURPOSE OF REPORT 1-1
1.2 FACILITY DESCRIPTION 1-1
1.3 REPORT FORMAT 1-3
CHAPTER 2 - BACKGROUND INFORMATION 2-1
2.1 BW-1 HISTORY 2-1
2.2 LOCAL GEOLOGY 2-3
CHAPTER 3 - INVESTIGATION PROCEDURES 3-1
3.1 HEALTH AND SAFETY 3-1
3.2 SOIL-GAS SURVEY 3-1
3.3 CHANGES TO THE CLOSURE PLAN FOR SOIL-GAS SAMPLING 3-2
3.4 DEEP SOIL BORINGS 3-3
3.4.1 Soil Sampiing Procedures 3-3
3.4.2 Sannple Handling Procedures 3-4
3.5 CHANGES TO THE CLOSURE PLAN FOR SOIL BORINGS 3-5
3.6 PROJECT RECORDS 3-5
CHAPTER 4 - RESULTS OF FIELD AND LABORATORY TESTING 4-1
4.1 FIELD MEASUREMENTS 4-1
4.2.1 Soil-Gas Results 4-1
4.2.2 Quality Assurance/Quality Control Results 4-3
Alliant Techsystems Inc. BW-1 Closure Report
Bacchus Works Revised December 5, 2002
TABLE OF CONTENTS (Continued)
Section Paqe
4.3 DEEP SOIL BORINGS 4-15
4.3.1 Boring Locations 4-15
4.3.2 Sample Identification 4-15
4.3.3 Lithologic Logging 4-17
4.3.4 Deep Soil Boring OA/OC 4-18
4.3.5 Deep Soil Boring Results 4-25
4.4 SITE SURVEY 4-33
CHAPTER 5 - CONCLUSIONS AND RECOMMENDATIONS 5-1
CHAPTER 6 - CLOSURE CERTIFICATION 6-1
CHAPTER 7 - REFERENCES 7-1
LIST OF FIGURES
Figure
1-1 COPY OF PUBLIC NOTICE 1-2
2-1 SITE LOCATION MAP 2-2
4-1 DEEP SOIL BORING LOCATIONS 4-16
Alliant Techsystems Inc. BW-1 Closure Report
Bacchus Works Revised December 5, 2002
LIST OF TABLES
Table Paqe
TABLE 4-1 SOIL-GAS FIELD MEASUREMENTS 4-2
TABLE 4-2 SOIL-GAS RESULTS 4-4
TABLE 4-3 TEDLAR BAG STUDY 4-14
TABLE 4-4 SOIL BORING QA/QC TRIP BLANK ANALYSES 4-19
TABLE 4-5 SOIL BORING QA/QC EQUIPMENT BLANK ANALYSES 4-21
TABLE 4-6 SOIL BORING QA/QC FIELD BLANK ANALYSES 4-23
TABLE 4-7 SOIL BORING VOC RESULTS 4-26
TABLE 4-8 SOIL BORING INORGANIC RESULTS 4-34
LIST OF APPENDICES
APPENDIXA RESULTS OF LABORATORY ANALYSES-AIR TOXICS LTD. ANALYTICAL
LABORATORY (VOLUME 1)
APPENDIX B SOIL-GAS CONCENTRATION MAPS (VOLUME 2)
APPENDIX C LITHOLOGIC LOGS AND FIELD DATA SHEETS (VOLUME 2)
APPENDIX D RESULTS OF LABORATORY ANALYSES - THIOKOL ENVIRONMENTAL
LABORATORY (VOLUME 2)
APPENDIX E CONCEPTUAL SITE MODEL FOR THE BW-1 LANDFILL AREA (VOLUME 2)
APPENDIX F LABORATORY QA/QC REPORTS (VOLUME 2)
LIST OF PLATES (VOLUME 2)
PLATE 1 SOIL-GAS SAMPLE LOCATIONS
PLATE 2 SOIL BORING LOCATIONS AND GRAPHICAL LOGS
PLATE 3 BW-1 SURVEY PLAT
FIGURE 1 - HERCULES BACCHUS WORKS SAMPLING LOCATiONS - SOIL GAS 1987
iv
ATK ATK Thiolcol Propulsion Tel; 1 435 863 3511
P.O. Box 707 Fax: [phone]
ALLIANT TECHSYSTEMS^^ Brigliam City, Utah 84302-0707
November 18, 2002
33H0-FY03-M087
TO: A. B. Lee
Environmental Compliance
CC: D. J. Fife, C. D. Falkenberg
FROM: L. R. Lofgreen, QA/QC Coordinator
Analytical Laboratories
SUBJECT: Response to BW-1 Requested Information
As per your E-Mail message of November 11, 2002, the following information is given using the same
numbering sequence in your message. This response refers to Lab Nos.: L4530, L4560, L4584, L4599 and
L4631. A copy of the QC reports with the analysts comments are attached.
• What do the out-of-limit values mean that show in the QC report?
The requirement for data checking and reporting are covered in our QA Plan. Also included is the QC
Data packet checklists this includes the justification for those parameters that did not meet the
laboratory QC goals. This is a common practice that all laboratories use. The limits that were
out-of-tolerance were judged to be acceptable and not affect the results reported.
4 QC sample control limit goals and all qualified (B, J) of analytical results.
* All QC goals are given in the QC reports. Either SW-846 and or the Laboratory Standard Operating
Procedure (SOP) have established these goals. The most restrictive limits of the two are used in
the QC report (see comments attached to the QC report that are provided by the analyst on
justification and reasons for data acceptance for those values outside of the laboratory goals). For
example, the metals analysis Method 6010 allows the LRB and LFB to have values that exceed the
MDL as long as the value is within 2.2 standard deviation of the MDL. Spike recoveries were
extremely high for aluminum. This was due to the concentration of the spiking solution added to
the sample coupled with the fact that the samples have so much aluminum in them. This makes
the spike and spike duplicate results invalid for aluminum. If some of the comments are too brief to
be understood by the reviewer, please call and we can clarify the comment.
"» The data qualifiers (B, J), which are used for GC/MS results are explained in detail at the end of
each Certificate of Analysis. Attached is a copy of this page with this report.
* In reviewing the GC/MS data, it was discovered that LIMS system has left the J and B flag off the
values reported. An annotated report is attached with the proper flags. This appears to have been
an issue with the soils matrix only and will be corrected.
33H0-FY03-M087
Page Two
Indicate problems with calibrations, holding times, temperature of sample, etc.
* It is the policy of the laboratory (QA Plan and or SOP) that each instrument be calibrated before
use. There were no calibration problems as can be seen by the continuing calibration checks and
initial calibration standards shown in the QC reports.
« Holding times are defined by SW-846: Volatiles-14 Days, Metals-6 Months, Nitrate/Nitrite-As soon
as possible. pH as soon as possible. Metals, Nitrate/Nitrite, pH were analyzed as soon as they
could be worked into the testing schedule. There were two Samples L4631-1 and L4631-2 that
were reported one day past the hold time. Both samples were tested within the holding time but
were tested the first time at 14 days. The QC surrogate recovenes were low tor theses two
samples. This is noted in the GC/MS Check sheet, which is attached. The decision was made to
rerun them on the next day. Which put them one day past their hold time. The only analyte
present in both samples was acetone. When compared to the rest of the samples in this set the
values reported are within the scatter of data. Therefore the data was accepted. See attached
GC/MS hold time report.
* The samples were received and logged in according to procedure and refrigerated according to
QA Plan. A copy of the checklist for receipt of samples and the temperature at receipt is attached.
Samples were stored at 4°C after receipt.
• Are all reported results adjusted for dilutions and moisture content?
* All samples were adjusted for dilution.
» A moisture value was made for each sample. These results were submitted to Jon Hermance in
November and December 2001. Copies of those reports are attached.
« The metals values were corrected for moisture in the Certificate of Analysis. The Nitrate/Nitrite and
Volatiles values were not corrected for moisture. The pH values do not need correction.
Please call or have the State of Utah representative call if there are further questions or clarification that is
needed as the data package is reviewed. If the complete data packages are required, they can be copied
and mailed.
Louis R. Lofgreen
ks
Attachments
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected but was
below the MDL.
B Gas Chromatography and Mass Spectral Data Flag. This flag is used when an analyte is found in
the blank as well as the sample
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This flag is used
either when estimating a concentration for tentatively identified compounds or when the data
indicated the presence of a compound that meets the identification criteria but the result is less than
the EQL (e.g. 3 J with an EQL of 10)
MDL Method Detection Limit: The minimum concentration of a substance that can be confidently
measured and reported. The laboratory has demonstrated that the MDL can be achieved in a
laboratory reagent blank, but does not guarentee it can be achieved in ali sample matrices.
The MDL is approximately three times the signal noise level.
EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many
analytes the EQL is selected as the value of the lowest standard in the calibration curve.
Dil. Factor Dilution Factor: The prepared smple was diluted by this factor because the sample was too
concentrated or due to other interferences in the sample matrix. Any dilution factor causes
an appropriate increase in the MDL and EQL.
Page 28of 28
1 Login No
L4530-1
1L4530-2
L4530-3
L4530-4
L4530-5
L4530-6
L4530-7
L4530-8
L4530-9
L4560-1
L4560-2
L4560-4
L4560-5
L4560-6
L4560-7
L4560-8
L4560-9
L4560-10
L4560-11
L4560-12
L4560-13
L4584-1
L4584-2
L4584-3
L4584-4
L4584-5
L4584-6
L4584-7
IL45B4-8
L4584-9
L4584-10
L4584-11 j
L4584-12
L4584-13
|L4599-1
L4599-2
L4599-3
L4599-4
L4599-5
L4531-1
L4531-2
L4531-3
L4531-4
L4531-5
L4531-6
L4531-7
L4531-8
L4531-9
L4531-10
L4531-11
L4531-12
VOLATILE HOLDING TIMES
Required Holding time is 14 days
1 Location
BW-1-TB-1
BW-1-1-0-2
BW-1-1-10-12
BW-1-1-13.3-15
BW-1-1-15-17.7
BW-1-1-20-22
BW-1-1-30-32
BW-1-1-40-41.7
BW-1-1-50-51.7
BW-1-1-66.7-68.3
BW-1-1-70-71.7
BW-1-1-75.76.7
BW-1-2-0-1.7
BW-1-2-10-11.7
BW-1-2-18.3-20
BW-1-2-20-21.7
BW-1-1-60-62
BW-1-1-EB-1
IBW-1-2-31.7.33.3
jBW-1-2-40-41.7
BW-1-1-TB-2
BW-1-2-45-46.7
BW-1-2-FD-1
BW-1-2-50-51.7
BW-1-2-60-61.7
BW-1-2-70-71.7
BW-1-2-EB-2
BW-1-3-0-1.7
BW-1-3-10-11.7
BW-1-3-20-21,7
BW-1-3-30-31.7
BW-1-3-31.7-33
BW-1-3-40-41.7
BW-1-2-TB-3
BW-1-3-50-51.7
BW-1-3-EB-3
1 Date
1 Sampled
9/6/2001
9/6/2001
9/6/2001
9/6/2001
9/6/2001
9/6/2001
9/7/2001
9/7/2001
9/7/2001
9/11/2001
9/11/2001
9/11/2001
9/13/2001
9/13/2001
9/13/2001
9/13/2001
9/10/2001
9/10/2001
9/14/2001
9/14/2001
9/10/2001
9/17/2001
9/17/2001
9/17/2001
9/17/2001
9/18/2001
9/18/2001
9/20/2001
9/20/2001
9/20/2001
9/21/2001
9/21/2001
9/21/2001
9/17/2001
9/24/2001
9/25/2001
BW-1-3-60-61.7 10/1/2001 |
BW-1-3-66.7-68.3
BW-1-3-TB-4
BW-1-4-0-1.7
BW-1-4.10-11.7
BW-1-4-13.3-15
BW-1-4-20-21.7
BW-1-4-30-31.7
BW-1-4-40-41.7
BW-1-4-50-51.7
BW-1-4-58.3-60
BW-1-4-FD-2
BW-1-4-EB-4
BW-1-4-FB-1
3W-1-4-TB-5 1
|L4531-13 1 BW-1-4-23.3-25 )
10/1/2001
9/24/2001
10/2/2001
10/2/2001
10/2/2001
10/2/2001
10/3/2001
10/3/2001
10/3/2001
10/4/2001
10/4/2001
10/4/2001
10/4/2001
10/2/2001
10/3/2001 1
1 Date
1 Analyzed
9/19/2001
9/13/2001
9/13/2001
9/13/2001
9/13/2001
9/13/2001
9/13/2001
9/13/2001
9/13/2001
9/24/2001
9/24/2001
9/24/2001
9/24/2001
9/24/2001
9/24/2001
9/24/2001
9/24/2001
9/20/2001
9/24/2001
9/24/2001
9/20/2001
10/1/2001
10/1/2001
10/1/2001
10/1/2001
10/1/2001
9/28/2001
10/1/2001
10/1/2001
10/2/2001
10/2/2001
10/2/2001
10/2/2001
9/28/2001
10/2/2001
10/3/2001
10/2/2001
10/2/2001
10/3/2001
10/17/2001
10/16/2001
10/17/2001
10/16/2001
10/16/2001
10/16/2001
10/16/2001
10/17/2001
10/17/2001
10/12/2001
10/12/2001
10/13/2001
10/16/2001 1
1 Elapsed 1
1 Days 1
13
7
7
7
7
7
7
7
I "^ 13
13
13
11
' 11
11
11
14
10
10
10
10
14
14
14
14
13
10
11
11
12
11
11
11
11
8
8
1 j
1 1
9
15*
14
15*
14
13
13
13
13
13
8
8
11
13 1
L4531-1 and L4531-3 were run or 10/16/02 but because of low
surrogate recoveries they were rerun on 10/17/02. This is noted on the
volatile check sheet. What was not known at the time was this was
one day passed the hold time. The only analyte reported was acetone
and the values are consistant with the other isamples in the set.
L4631
Login Number_
EPA Method _
SOP Number]
Work Group Number
Arsenic QC Data Package Checklist
L4631
7060
311
WG7700
A complete description of sample and standards preparation is located in the "Standards
Preparation Log" and "Digestion Log"
Standard Soluiton: Standard Concentration
Standard 1
Standard 2
Standard 3
Standard 4
5 ppb
25 ppb
50 ppb
100 pbb
QC Concentration (ppb)
LFB
ICV
QCS
CCV
50.0
50.0
20.0
50.0
Spike Preparation: The preparation of matrix spikes and matrix spike duplicates
is described in the "Digestion Log". Spike Concentration
after final dilution is typically 25 ppb.
Analyst:
Peer review:
Comments:
All QC acceptable
Date: J^ ^f/J)
—-^—yf—
Date: /yt
Package Includes: Autosampler Table L4599
QC Report 2<
Work Group Report 2<
Data Review X
Raw data stored with Login Number L4599
Data package includes data from Login Number(s)
Login Number _
EPA Method _
SOP Number]
Work Group Number_
Arsenic QC Data Package Checklist
L4631
7060
311
WG7675
A complete description of sample and standards preparation is located in the "Standards
Preparation Log" and "Digestion Log"
Standard Soluiton: Standard Concentration QC Concentration (ppb)
Standard 1
Standard 2
Standard 3
Standard 4
5 ppb
25 ppb
50 ppb
100 pbb
LFB
ICV
QCS
CCV
50.0
50.0
20.0
50.0
Spike Preparation: The preparation of matrix spikes and matrix spike duplicates
is described in the "Digestion Log". Spike Concentration
after final dilution is typically 25 ppb.
Analyst:
Peer review:
Comments:
All QC acceptable
Date: ^* ^y^y4->
Date: A^t •U.
Package Includes: Autosampler Table L4560
QC Report 2<
Work Group Report_X
Data Review X
Raw data stored with Login Number L4560
Data package includes data from Login Number(s)
Login Number_
EPA Method _
SOP Number]
Work Group Number
Mercury QC Data Package Checklist
L4631
7471A
316
WG7650
A complete discription of QC, sampie and standards preparation is located in the "Mercury
Analysis Log Book".
Standard Concentration QC Concentration
LFB
ICV
QCS
CCV
Spike Preparation: The preparation of matrix spikes and matrix spike duplicates is described
in the "Mercury Analysis Log Book". Spike concentration after final
dilution is usually 4 ppb Hg.
Standard 1
Standard 2
Standard 3
Standard 4
Standard 5
1 ppb
2 ppb
5 ppb
10 ppb
20 ppb
4 ppb
5 ppb
10.0
5 ppb
Analyst:
Peer review:
Comments:
J^r^^/* Dale: /oAr/"
Date:
Package Includes: Autosampler Table L4599
QC Report 2<
Work Group Report2<
Data Sheet X
Sample Prep Sheet L4599
Raw data stored with Login Number L4599
Data package includes data from Login Number(s)
./
Login Number
EPA Method _
SOP Number"
Work Group Number
Mercury QC Data Package Checklist
L4631
7640A
316
WG7641
A complete discription of QC, sample and standards preparation is located in the "Mercury
Analysis Log Book".
Standard Concentrafion QC Concentration
LFB
ICV
QCS
CCV
Spike Preparation: The preparation of matrix spikes and matrix spike duplicates is described
in the "Mercury Analysis Log Book". Spike concentration after final
dilution is usually 4 ppb Hg.
Standard 1
Standard 2
Standard 3
Standard 4
Standard 5
1 PDb
2 ppb
5 ppb
10 ppb
20 ppb
4 ppb
5 ppb
10.0 ppb
5 ppb
Analyst:
Peer review:
Comments:
All QC acceptable.
Date:
y^lt>S>/l4^?''^'^^'<^—
^'/T/^
Date: //, /•*./»/
Package Includes: Autosampler Table LASII
QC Report X
Work Group Report X
Data Sheet X
Sample Prep Sheet L4572
Raw data stored with Login Number
Data package includes data from Login Number(s)
L4572
Login Number
EPA Method
(A/ork Group Number
Run Number
Standard Solution:
MSTDl
MSTD2
MSTD3
MSTD4
MSTD5
Cal Blank
EPA SW-846
L4631
6010
WG7628
R30908
Log Identification
10/29/2001
10/29/2001
10/29/2001
10/29/2001
10/30/2001
NA
6010 QC Data Package Ctiecklist
QC Solutions: Log Identification
LPC
QC-21
QC-7
QC-7 IOX
QC-Sn
QC-P
10/26/2001
10/19/2001
10/15/2001
10/29/2001
7/10/2001
9/28/2001
Peer reviev^/ by
Analyst: "X^lJ/^^^ - •
0/29, 10/16,8(10/17/01 SIC
LFB >.0 mL of LFS 10/16/01
Matrix Spike lOmLofLFS 10/16/0
QC Samples:! L4595-5, L4599-2,
&L4611-3
Date: ///S^/'Z^t^
Date: >»f^ ->//
Comments: ^^ xc^g^^g^. ^ ^^m.^..^ ^ /Lys^r-
Dilutions: 100 mL Vol. Flasks
Package Includes: Autosampler Table
QC Report-
Work Group Report
Bench Sheet
Data Review
NA
T7 /-
17 ^
:^
Raw data stored with Login Number L4595
Data package includes data for Login Number(s) L4595. L4599, L4611.
L4631,&L4651
Volstiie Organics Data Package Checklist
Sample Logrn No: L^/lf^/'^d.K/p)
Work Group: \A'A^^L>^0
Date RMn:jRjQ£±_acoi
Methcd: H^^
Matrix: IjJoX^
Instrument ID: 3-UP7P^
initial Caiifaraticn LocatJcn: U/ fO /a^Oi^
Run Log
EFs Tune Report
Continuing Calir:raticn: Cuant Repco/Chromatccram
Continuing Calibrsticn Check Report
Reagent Blank; Cuant RsporjChrcrriatcgram '
Sampl6s:Guant Repcr/Chrcmatccram
Samples: TIC Data
Matrix Spike: Guant ReporJCurcmaiccrarn
Mauix Spike Cupiicaie: Cuant RepoPu'Chrcrnatccrarr.
Interna! Standard Area Reccr:
Surccate £ Spike/TZupiicate Recove.^/ Repert
Frec/Exracdcn Leg
Pre£e."/aticn Check
Peer Review »
Nitrate-N QC Data Packs
Login Number L4631
EPA Method 9056.0
SOP Number 341
Work Group Number WG7633
Standard Solution:
Autocall R
Autocal2R
Autocal3R
Autocal4R
Autocal5R
QC Solutions:
ICV
QCS
CCV
Spike Stock Sol.
Spike
Spike Preparation:
Matrix Spike
Matrix Spike Dup.
Analyst: >^^a
Peer review: y^ife/y^
Comments:
All QC acceptable.
Log Identification
CWS-86-489
CWS-86-488
CWS-86-487
CWS-86-486
CWS-86-485
Log Identification
CWS-86-488
Dionex Ref./IO
CWS-86-486
CWS-40-173
mL of Sample
5.00
. 5.00
\^rh ^
ige Checkli
Date:
Date:
st
Concentration (ppm)
Nitrate-N
0.5
2
5
10
20
Concetration (ppm)
Nitrate-N
2
2.26
10
2000
4
uL of Stock
Nitrate-N
10
10
-^>^>^
/^//7//
Package Includes: Autosampler Table
QC Report
Work Group Report
Bench Sheet
Data Review
Raw data stored with Loc
Data package includes data from Login
X
X
X
X
X
lin
Nu
Number
mber(s)
Work Group Summary Report
Quality Control Data
Analysis: PH 9045 Method: SW 846, 9045
Report Date: 15-OCT-Ol
Siunmazry of QC Samples
Sample QC
Niunber Type Description
WG7 621-1 QCS independent Checic Standard
WG7621
QC Measured Values with. Limits
%Recov Limits
99.9 80-120
STiimaary of Spiked Samples
Sample QC Reference Sample
Number Type Number
WG7621-2 DUP L4631-9 9.03
Samples In Workgroup
L4631-1 L4631-2
L4631-7 L4631-8
Spiked Measured Values with Limits
8.99
L4631-4
L4631-9
RPD Limits
0.44 0-20
L4631-5 L4631-6
Analyst:
Peer Review: /\
Date /SO ci- O f
A^l^O (^- (L^i^ Date LSTDC iO)
Volatile Organics Data Package Checklist
Sampie Login No: Lmi^ LWf!^/
Work Group: luf^l^T^
Date Run:/z:f7 - Qc-T o^oi
Methcd:
Matrix:
gz^o
S»orL.
Instrument ID: '^-t^PTZ
llf 0 CT 7^*c I Initiai Calibraticn Location:,
Run Log
SF= Tune Report
Continuing Calicrsticn: Cuant Repcrt/Chromatccram
Continuing CaHbraticn Check Repon
Reagent Elank: Quant ReporjChrcmatcgram '
Samples:Guant Repcn/Chramiatccrarn
Samples: TIC Data
Matrix Spike: Cuant Repcr^Chrcm.atccram
Matrix Spike Duplicate: Cuant Repon/Chrcmatccram
Inte.Tisi Stancard Area Reccn
Surrccate i Spike/'Cupiicate Recover/ Reccr:
Prep/Extra cticn Leg
Preser/aticn Check
Re^r .Review
rf..t,A,ye./^} IS/ cJ-On
<^^t Jsiiel ^
.^^
-£ a/tt-r/^
HJTU^ or^ r? ocr ktl^ S'^.'|b^ k^s^tfa.
CIMAIA IC/N^V. ftyytJJA. Lgfe '^^ ^ .
CERTIFICATE OF ANALYSIS
Listing of sample Information and Testing Requested
Friday, December 7, 2001
TESTED FOR ATK Thiokol: Bacchus
Environmental Compliance M/S M7H7
P. O. Box 98
Magna, UT 84044-0098
Jon Hermance
Project: Lab Anal - Rem - Soil
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-3732
800-863-8080
Login Number L4631
Lab No Ciient Number
Test Requested
L4631-1 BW-1-4-0-1.7
SW-846, 8260
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
L4631-2 BW-1-4-10-11.7
SW-846, 8260
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
L4631-3 BW-1-4-13.3-15
SW-846, 8260
Description
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
A ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb
Se
Be
Ba
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCFIA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al
Ba
Cd
Cr
Pb
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Volatile Organics
Received CollectDate/Time
Matrix
10/11/01 10/02/01 13:00 1
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
10/11/01 10/02/01 14:40
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
10/11/01 10/02/01 15:30
Soil
Page 1 of 28
L4631-4 BW-1-4-20-21.7 10/11/01 10/02/01 16:20
SW
SW'
SW-
SW'
SW-
SW-
SW-
SW-
SW-
sw-
sw-
sw-
sw
sw
SW
•846, 8260
•846, 7471A
846, 7060
•846, 6010
846,6010
846, 6010
-846, 6010
•846,6010
•846, 6010
•846, 6010
•846, 6010
•846, 3050
846, 9056
846, 9056
846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
I L4631-5 BW-1-4-30-31.7 10/11/01 10/03/01 11:50
SW
SW^
SW^
SW-
sw-
sw-
sw-
sw-
sw-
sw-
sw-
sw-
sw
sw
sw
-846, 8260
846, 7471A
846, 7060
•846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 3050
846, 9056
846, 9056
846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Be ICP Melals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L4631-6 BW-1 -4-40-41.7 10/11/01 10/03/01 14:30
SW-
SW-
SW-
SW-
SW^
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW
SW
SW
-846, 8260
-846, 7471A
-846, 7060
•846, 6010
-846, 6010
-846, 6010
-846,6010
•846, 6010
•846, 6010
•846, 6010
•846, 6010
•846, 3050
846, 9056
846, 9056
846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals /Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L4631-7 BW-1-4-50-51.7 10/11/01 10/03/01 16:30
SW
SW
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
sw-
sw-
sw
sw
sw
846, 8260
846, 7471A
846, 7060
846, 6010
846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
•846, 3050
846, 9056
846, 9056
846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
ICP/GF/^ Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Page 2 of 28
L4631-8 BW-1-4-58.3-60 10/11/01 10/04/01 11:00
SW-
SW
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
sw-
sw
sw
sw
846, 8260
-846, 7471A
•846, 7060
846, 6010
-846, 6010
-846,6010
-846, 6010
-846, 6010
-846,6010
-846, 6010
•846, 6010
•846, 3050
846, 9056
846, 9056
846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Be ICP Metals /Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Spll
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L4631-9 BW-1-4-FD-2 10/11/01 10/04/01 12:30
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW
sw
SW
846, 8260
-846, 7471A
-846, 7060
-846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
•846,6010
•846,6010
-846, 3050
846, 9056
846, 9056
846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals /Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L4631-10 BW-1-4-EB-4 10/11/01 10/04/01 12:30
SW-846, 8260
SW-846, 7470A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3010
SW-846, 8260
Volatile Organics Appendix 9
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP Metals Digestion
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
L4631-11 BW-1-4-FB-1
SW-846, 8260
1 L4631-12 BW-1-4-TB-5
SW-846, 8260
L4631-13 BW-1-4-23.3-25
Volatile Organics Appendix 9
Volatile Organics Appendix 9
10/11/01
10/11/01
10/11/01
10/04/01 12:30
Water
10/02/01 09:30
Water
10/03/01 11:05 1
Volatile Organics
Certified
Soil
Date QC Coordinator
This certifies ttiat ttie following samples were anaiyzed using good laboratory practices to stiow ttie following results:
Page 3 of 28
Listing of Results by Sample
1 Sample ID: BW-1-4-0-1.7
630-20-6
71-55-6
79-34-5
79-00-S
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-'I El RACHLOROETHANE
1,1,2-TRICHLOROETH ANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2.3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-THICHL0R0BEN2ENE
1,2,4-TRIMFrHYLBEN2ENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBEN2ENE
1,2-DICHLOnOETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOHOBEN2ENE
1.3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYL VINYL ETHER
2-CHLOflOTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CAHBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
ClS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1.3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
Ss?uit
u
u
u
u
u
.5T
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
.ynjts.
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
5.2 iJ7fe ug/kg
U
U
.7
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
.0147
8.75
14600
140
.8
.5
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L4631-1 Collect Date: 10/02/01 13:00 |
MCk
.6
.6
.9
8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.01
.96
1.4
.05
.1
.1
Oil.
EQL Factor MethPd
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
.04
3.3 2
6.8 1.1
.3 1.1
.5 1.1
.5 1.1
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846.8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, B260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-e46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW.846,8260
1 SW-846, B260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46,8260
I SW-846,8260
SW-846. 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
0 SW-846, 7060
37 SW-846, 6010
37 SW-846, 6010
37 SW-846, 6010
37 SW-846, 6010
Analyst
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR •
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
CWS -
CWS -
MTB 1
MTB
MTB
MTB -
Page
Test Date
10/17/01 12:15
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Q/17/01 12:15
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Q/17/01 12:15
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0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/17/01 12:15
0/22/01 14:17
0/31/01 14:52
0/30/01 14:24
0/30/01 14:24
0/30/01 14:24
0/30/01 14:24
4of28
CHROMIUM
LEAD
SELENIUM
SILVER
ICP/GFAA MET/U.S DIGESTION
NITRATE-N
NITRITE-N
PH
30
12
7.3
U
3.5
.1
8.49
ug/g
ug/g
ug/g
ug/g
mg/(
mg/l
.3
1.4
3.3
.2
.01
.01
1.4
6.8
16
.8
.05
.05
1.137
1.137
1.137
1.137
1
1
1
1
SW-846, 6010
SW.B46, 6010
SW-846, 6010
SW-846, 6010
SW-846. 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
MTB
MTB
CWS
CWS
LDS
10/30/01 14.24
10/30/01 14:24
10/30/01 14:24
10/30/01 14:24
10/24/01 12:00
1Q/16AD1 10:06
10/16/01 10:06
10/1 VOI 09:49
Page 5 of 28
Isample ID: BW-1-4-10-11.7
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-9B-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01 -6
75-69-4
108-05-4
75-01-4
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOHOBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBEN2ENE
1,3-DICHLOROBENZENE
1.3-DICHLOROPROPANE
1,4-DICHL0R0BEN2ENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4.ISOPHOPYLTOLUENE
4-METHYL-2-PENT ANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TEI RACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
u
u
u u
u u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
ynits
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
12316 ug/kg
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u u
4.99
6600
72
4
.5
12
4.9
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L4631-2 Collect Date: 10/02/01 14:40 |
MPL
.6
.6
.9
.8
4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
14
1.8
24
1.1
.5
.6
.5
.8
1
.8
.6
.7
7
.4
.7
.3
.5
.4
1
7
1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
6
.5
.7
4
.5
6
.5
.3
.5
.01
.96
14
.05
.1
.1
.3
1.4
Oil.
EQL Factor Methpd
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
.04
3.3 2
6.8 1.1
.3 1.1
.5 1.1
.5 1.1
1.4 1.1
6.8 1.1
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-e46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-e46,8260
1 SW-846,8260
1 SW-e46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46,8260
1 SW-846,8260
1 SW-B46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
SW-846, 8260
t SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
I SW-846,8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846, 7471A
0 SW-B46,7060
35 SW-846,6010
35 SW-846, 6010
35 SW-846. 6010
35 SW-846, 6010
35 SW-846, 6010
35 SW-B46,6010
Analyst
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB -
Page
Ifist Pate
10/16/0
10/16/0
0/16/0
10/16/0
10/16/0
10/16/0
10/16/0
10/16/0
10/16/0
10/16/0
0/16«
10/16^0
10/16/0
10/16A)
10/16/0
10/16/0
0/16/0
I0/16A3
10/16/0
10/16/0
0/16/0
10/16/0
0/16/0
10/16/0
10/16/0
10/16/0
10/16/0
10/16/0
Q/16/0
10/16/0
10/16A3
10/16/0
0/16/0
0/16/0
0/16/0
10/16/0
10/16/0
0/16/0
0/16/0
0/16/0
0/16/0
0/16AD
0/16/0
10/16/0
0/16A3
0/16/0
0/16A)
0/16A3
0/16/0
on em
0/16/0
0/16/0
0/16/0
0/16/0
10/16/0
0/16/0
0/16/0
0/16/01
0/16/0
0/16/0
10/16/0
0/16/0
0/16/0
0/16/0
0/16/0
0/16/0
0/16/0
0/16/0
0/16/0
0/22/0
10/31/0
0/30/0
0/30/0
0/30/0
0/30/0-
0/30/01
0/30/0-
6of2
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
1 16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
16:24
14:26
15:02
14:27
14:27
14:27
14:27
14:27
14.27
B
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NITRATE-N
NITRITE-N
PH
U
U
U
U
8.94
ug/g
ug/g
mg/l
mg/l
3.3
.2
.01
.01
16
.8
.05
.05
1.135
1.135
1
1
1
1
SW-846. 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
LDS
10/30/01 14:27
10/30/01 14:27
10/24/01 12:00
10/16/01 10:24
10/16/01 10:24
10/15/01 09:49
Page 7 of 28
Isample ID: BW-1-4-13.3-15
CAS
Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-B
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2.4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2.2-DICHLOROPROPANE
2-BLrT ANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOnOETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
ItIRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
Result
u u u u
u u u u
u u u
u u u u
u u u u
u u u
u u
u u
u u 20 e
u
u u u u u
u u u u u u
u u u u u u u u
u u u u
u u
u u u u u u
u u u u u u u u
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
LablD:L4631-3 Collect Date: 10/02/01 15:30 |
MPL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
14
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
6
.6
.5
.7
.4
.5
.6
.5
.3
.5
DM.
£QL Factor Method'
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10
10
10
10
10
10
10
10
10 1
10
10 1
10 1
10 1
10 1
10 1
10
10 1
10 1
10 1
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 S'W-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-646, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-646, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
lest Pate
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17A)1 13:25
0/17/01 13:25
10/17/01 13:25
10/17/01 13:25
10/17/01 13:25
10/17/01 13:25
10/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
10/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
0/17/01 13:25
Page 8 of 28
Isample IP: BW-1-4-20-21.7
630-20-6
71 -55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-5B-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-B
106-93-4
95-50-1
107-06-2
78-87-5
106-67-B
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-£
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
Twt Parametex
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOHOETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBEN2ENE
1,2,4-TRIMETHYLBENZENE
1,2-DlBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVlNYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-lSOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULRDE
CAHBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
u
2.5 T
U
U
U
ST
U
U
U
U
U
U
u
u u
u u u u u
u
u u u u u u u
ynits
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
S.ej-,B,ugMg
u
u u u
u u u u u
u u
u u u u u
u u u
u u
u u
u u u
u u u u u
u u u u u u u u u u 3.42
6910
67
.28
.38
12
43
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug*g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L4631-4 Collect Date: 10/02/01 16:20 |
MDL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
5
.5
.7
1.2
.6
.7
6
.6
.5
.7
4
.5
.6
.5
.3
.5
.01
.7
.98
.04
.08
.08
.2
.98
Pll.
EQL Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
.04 1
2.3 2
4.9 1.1
.2 1.1
.4 1.1
.4 1.1
.98 1.1
4.9 1.1
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-e46,8260
1 SW-846,8260
1 SW.846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW.846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
0 SW-846,7060
39 SW-e46, 6010
39 SW-846, 6010
39 SW-846, 6010
39 SW-846, 6010
39 SW-846,6010
39 SW-a46, 6010
&naly^
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR 1
MKR 1
MKR
MKR 1
MKR -
MKR -
CWS 1
CWS 1
MTB 1
MTB 1
MTB 1
MTB 1
MTB 1
MTB 1
Page
Test Date
10/16/01 17:35
10/16/01 17:35
10/16/01 17:35
10/16/01 17:35
10/16/01 17:35
10/16/01 17:35
10/16/01 17:35
10/16/01 17:35
10/16/01 17:35
10/16/01 17:35
10/16/01 17:35
10/16/01 17:35
10/16/01 17:35
10/16/01 17:35
yo/^m^ i7:35
10/16/01 17:35
1Q/16«1 17:35
10/16/01 17:35
0/16/01 17:35
0/16rtD1 17:35
0/16/01 17:35
10/16/01 17:35
0/16/01 17:35
10/16/01 17:35
10/16«)1 17:35
10/16/01 17:35
10/16/01 17:35
1Q/I6rt)1 17:35
10/16/01 17:35
1Q/16W1 17.35
0/16/01 17:35
0/16/D1 17:35
0/16mi 17:35
0/16/01 17:35
10/16/01 17:35
10/16/01 17:35
0/16/01 17:35
0/16/01 17:35
0/16/01 17:35
10/16/01 17:35
0/16/01 17:35
10/16/01 17:35
ttVia/OI 17:35
0/16/01 17:35
0/16/01 17:35
0/16/01 17:35
0/16/01 17:35
10/16/01 17:35
0/16/01 17:35
0/16/01 17:35
0/16/01 17:35
0/16rt)1 17:35
0/16/01 17:35
0/16/01 17:35
0/16/01 17:35
0/16/01 17:35
0/16/01 17:35
0/16/01 17:35
0/16/01 17:35
0/16/01 17:35
0/16/01 17:35
0/16/01 17:35
0/16/01 17:35
0/16/01 17:35
0/16/01 17:35
0/16/01 17:35
0/16/01 17:35
0/16/01 17:35
0/16/01 17:35
0/22/01 14:28
0/31/01 15:12
0/30/01 14:30
0/30/01 14:30
0/30/01 14:30
0/30/01 14:30
0/30/01 14:30
0/30/01 14:30
9 Of 28
SELENIUM
SILVER
(CP/GFAA METALS DIGESTION
NITRATE-N
NITRITE-N
PH
U
U
.037
U
9.38
ug/g
ug/g
mg/l
mg/l
2.3
.1
.01
.01
12
.6
.05
.05
1.139
1.139
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW B46, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
LDS
10/30/01 14:30
10/30/01 14:30
10/24AD1 12:00
10/16/01 10:41
10/16/01 10:41
10/15/01 09:49
Pagel Oof 28
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43^
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
D: BW-1-4-30-31.7
Test Parameter
1.1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOHOETHANE
1,1,2,2-TETRACHLOROETH AN E
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-THIMETHYLBENZENE
1,2-DIBHOMO-3-CHLOROPROPANE
1,2-DIBHOMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-lSOPROPYLTOLUENE
4-METHYL-2-PENTAN0NE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1
74-95-3
75-71-8
-100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPHOPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
C/ADMIUM
CHROMIUM
LEAD
Result
u
U
U
U
u u
u u u
u u
u u
u u
u u
u u
u u
u u u
u u u u 34 e
u u
u u u u
u u u u u u
u u u u
u u u u u u u
u u u u u
u u u u u u u u
u u u u u 4.36
8640
79
.4
.7
14
5.6
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L4631-5 Collect Date: 10/03/01 11:50 |
MDL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.01
.9
1.3
.05
.1
.1
.3
1.3
Dil.
EQL Factor Method •
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
.04 1
3.1 2
6.5 1.1
.3 1.1
.5 1.1
.5 1.1
1.3 1.1
6.5 1.1
1 SW.846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46,8260
1 SW.846,8260
1 SW-846,8260
1 SW-e46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-e46, 8260
I SW-846,8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW-846, B260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 6260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
0 SW.846, 7060
48 SW.846,6010
48 SW-846, 6010
48 SW-846, 6010
48 SW-846, 6010
48 SW-846,6010
48 SW-846, 6010
Anajyst
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR -
MKR
MKR
MKR 1
MKR 1
MKR 1
MKR 1
MKR 1
MKR 1
MKR 1
MKR 1
MKR 1
MKR 1
MKR 1
CWS 1
CWS 1
MTB 1
MTB 1
MTB 1
MTB 1
MTB 1
MTB -
Page 1
Test Date
10/16/01 18:10
10/16/01 18:10
10/16/01 18-10
10/16/01 18:10
10/16/01 18:10
10/16/01 18:10
10/16/01 18:10
10/16/01 18:10
10/16/01 18:10
10/16/01 18:10
10/16/01 18:10
10/16/01 18:10
10/16«)1 18:10
10/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
10/16/01 18:10
10/16/01 18:10
0/16/01 18:10
0/16/01 18:10
10/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
10/16/01 18:10
10/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
10/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/16/01 18:10
0/22/01 14:33
0/31/01 15-43
0/30/01 14:34
0/30/01 14:34
0/30/01 14:34
0/30/01 14:34
0/30/01 14:34
0/30/01 14:34
lof 28
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NlTRATE-N
NITRITE-N
PH
U
U
.063
U
9.27
ug/g
ug/g
mg/l
mg/l
3.1
.2
.01
.01
16
.8
.05
OS
1.148
1.148
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-B46, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
LDS
10/30/01 14:34
10/30/01 14:34
10/24/01 12:00
10/16/01 10:59
10/16/01 10:59
10/15/01 09:49
Page 12 Of 28
1 Sample ID: BW-1-4-40-41.7
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
7B-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-£
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
Test Parametgr
1.1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOHOETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOHOPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1.2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1.3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1.3-DlCHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPHOPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
i CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BLTTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENe
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
U
U
u
U
U
u
U
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
9i3,e"9/kg
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u u
u
u u
u
u
u
u u
u
u
u
u
u
u u
u
u
u
u u
u
u
u
5.33
7240
380
.3
.6
16
6
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L4631-6
MDL
.6
.6
9
.8
4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
11
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.01
.96
1.4
.05
.1
.1
.3
1.4
EQL
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
.04
3.3
6.8
.3
.5
.5
1.4
6.8
Oil.
Factor
20
1.134
1.134
1.134
1.134
1.134
1.134
Collect Date: 10/03/01 14:30 1
Method
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-B46, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, B260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-B46,6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Analyst
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
Test Date
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16rt)1 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18 46
10/16/01 18:46
10/16/01 1846
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/15/01 18:46
10/16/01 18:46
10/16/01 18.46
10/16/01 18:46
10/16/01 18.46
1Q/16rt)1 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
lO/ierai 18:46
10/16/01 18-46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16A)1 18:46
in/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/15/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/16/01 18:46
10/22/01 14:40
10/31/01 15:53
10/30/01 14:37
10/30/01 14:37
10/30/01 14:37
10/30/01 14:37
10/30/01 14:37
10/30/01 14:37
Page 13 of 28
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NITRATE-N
NITRITE-N
PH
U
.3
.046
U
9.19
ug/g
ug/g
mg/l
mg/l
3.3
.2
.01
.01
16
.8
.05
.05
1.134
1.134
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
LDS
10/30/01 14:37
10/30/01 14:37
10/24/01 12:00
10/16/01 11:16
10/16/01 11:16
10/15/01 09:49
Page 14 Of 28
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-56-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
7B-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27^
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
ID: BW-1-4-50-51.7
Test Parameter
1 1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1 1-DICHLOROPROPENE
1 2,3-TRICHLOROBENZENE
1,2,3-THICHLOROPROPANE
1,2,4-THICHLOHOBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPHOPANE
1 [2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-THIMETHYLBENZENE
1,3-DICHLOROBEN2ENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOflOTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENT ANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TE 1HACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
10061-01 -5 CIS-1,3-DICHLOROPROPENE
124-48-1
74-95-3
75-71-6
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
H EXACHLOHOBUTADIEN E
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
8.9 T,8 ug/kg
u '
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
3.07
9440
167
.4
.4
15
3.9
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L4631-7
MPL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.01
.9
1.3
.05
.1
.1
.3
1.3
EQL
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
.04
3.2
6.7 1
.3 1
.5 1
.5 1
1.3 1
6.7 1
Dil.
Factor
20
138
138
138
138
138
138
Collect Date: 10/03/01 16:30 |
_ Method
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Analyst
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR 1
MKR 1
MKR 1
MKR 1
MKR 1
MKR 1
MKR 1
MKR 1
MKR 1
MKR 1
CWS 1
CWS 1
MTB 1
MTB 1
MTB 1
MTB 1
MTB 1
MTB 1
Pagel
Igst Date
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19.21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16«)1 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16rtl1 19:21
10/16rtl1 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/16/01 19:21
10/15/01 19:21
10/15/01 19:21
10/16/01 19:21
0/16/01 19:21
0/16/01 19:21
0/16/01 19:21
10/16/01 19:21
10/16/01 19:21
O/16/01 19:21
0/16/01 19:21
o/^m^ i9;2i
0/16/01 19:21
0/16/01 19:21
0/16/01 19:21
Q/16/01 19:21
0/16/01 19:21
0/16/01 19:21
0/16/01 19:21
0/16/01 19:21
0/16/01 19:21
0/16/01 19:21
0/16/01 19:21
0/16/01 19:21
0/16/01 19:21
0/16/01 19:21
0/15«)1 19:21
0/16/01 19:21
0/16/01 19:21
0/15/01 19:21
0/16/01 19:21
0/16/01 19:21
0/22/01 14:44
0/31/01 16:03
0/30/01 14:55
0/30/01 14:55
0/30/01 14:55
0/30/01 14:55
0/30/01 14:55
0/30/01 14:55
5of28
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NITRATE-N
NITRITE-N
PH
U
U
.1
U
9.14
ug/g
ug/g
mg/l
mg/l
3.2
.2
.01
.01
16
.8
.05
.05
1.138
1.138
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
LDS
10/30/01 14:55
10/30/01 14:55
10/24/01 12:00
10/16/01 12:09
10/16/01 12:09
10/15/01 09:49
PagelSof 28
1 Sample ID; BW-1-4-58.3-60
630-20-6
71-55-6
79-34-5
79-00-6
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-£
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
Test Parameter
1,1,1,2-TETHACHLOROETHANE
1,1,1-TRICHLOROETHANE
1.1,2.2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2.4-TRICHLOROBENZENE
1,2,4-TRIMETHYLB ENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOHOBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2.2-DlCHLOROPROPANE
2-BUTANONE
2-CHLOHOETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4.METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOHOBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
79-01-6
75-69-4
108-05-4
75-01-4
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYUIUM
CADMIUM
CHROMIUM
LEAD
Result
U
U
U
u u u
u u
21
u u u u
u u
u u
u u u u u u u
u u u u
11B
u u
u u
u u
u 2.8 T
u u u u
u u u u
u u u
u u
u u
u u u
u u
u u u u u u u u
u u u
u .0341
5.45
6460
270
.3
.5
10
8.1
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug-'g
ug/g
ug/g
ug/g
LablD:L4631-8
MDL
.6
.6
,9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
24
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
1
.5
.5
.5
.5
1.3
.5
5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.01
.9
1.3
.05
.1
.1
.3
1.3
Dil.
EQL Factor
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
50 1
10 1
10 1
50 1
10 1
10 1
50 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
.04 1
3.1 20
6.6 1.136
.3 1.136
.5 1.136
.5 1.136
1.3 1.136
6.6 1.136
Collect Date: 10/04/01 11:00 |
Methoii •
SW-846, 82 50
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-646, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-B46, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8250
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
SW-846. 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Analyst
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
Twt Date
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/D1 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16.21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16.21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/17/01 16.21
10/17/01 16:21
10/17/01 16:21
10/17/01 16:21
10/22/01 14:54
10/31/01 16:13
10/30/01 14:58
10/30/01 14:58
ia'30/01 14:58
10/30/01 14:58
10/30/01 14:58
10/30/01 14:58
Page 17 of 28
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NITHATE-N
NITRITE-N
PH
U
U
49
U
8.97
ug/g
ug/g
mg/l
mg/l
31
2
.01
.01
16
.8
.06
.05
1.136
1 136
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
LDS
10/30/01 14:58
10/30/01 14:58
10/24/01 12:00
10/16.'0l 12:26
10/16/01 12:26
10/15/01 0949
Paoftio-"
1 Sample ID: BW-1-4-FD-2
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541 -73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-£
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
Test Parameter
1,1,1,2-TETHACHLOROETHANE
1,1.1-TRICHLOROETHANE
1.1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1.1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4.METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON ItrRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
u
u u u u u
u u
u u
u u u u u u
u u
u u u u u
u u u u u u u u u
u u u u u
u u u u u
u u u u u
u u
u u u u
u u u u u u
u u u u u
u u u u u .0238
5.22
6430
208
.3
.6
11
6.3
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L4631-9 Collect Date: 10/04/01 12:30 |
MDL
.6
.6
9
.8
4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
24
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.01
1.4
2
.08
.2
.2
.4
2
Oil.
EQL Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
.04 1
4.8 2
10 1.1
.4 1.1
.8 1.1
.8 1.1
2 1.1
10 1.1
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846. 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-B46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, B260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
0 SW-846,7060
34 SW-846, 6010
34 SW-846,6010
34 SW-846,6010
34 SW-846,6010
34 SW-846,6010
34 SW-846,6010
Analyst
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR -
MKR
MKR
MKR
MKR
MKR
MKR
MKR -
MKR -
MKR
MKR -
CWS 1
CWS -
MTB -
MTB 1
MTB 1
MTB 1
MTB -
MTB
Page 1
Test Pate
10/17/01
10/17/01
10/17/01
10/17/01
10/17/01
10/17/01
0/17/01
10/17/01
10/17/01
0/17/01
0/17/01
0/17/01
10/17/01
10/17/01
10/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
10/17/01
10/17/01
10/17/01
10/17/01
10/17/01
10/17/01
10/17/01
10/17/01
10/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
10/17/01
10/17/01
10/17/01
0/17/01
0/17/01
10/17/01
0/17/01
10/17/01
10/17/01
0/17/D1
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/17/01
0/22/01
0/31/01
0^0/01
0/30/01
0/30/01
0/30/01
0/30/01
0/30/01
9 Of 28
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16:56
16.56
16:56
16:56
16:56
16:56
14:56
16:23
15:02
15:02
15:02
15:02
15:02
15:02
> *•
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NITRATE-N
NITRITE-N
PH
48
U
.51
U
9.03
ug/g
ug/g
mg/l
mg/l
48
.2
.01
.01
24
1.2
.05
.05
1.134
1.134
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-646, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
LDS
10/30/01 15:02
10/30/01 15:02
10/24/01 12:00
10/16/01 12:44
10/16/01 1244
10/15/01 09 49
Page 20 Of 28
1 Sample ID: BW-1-4-EB-4
CAS
Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-B
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
71-36-3
590-20-7
78-93-3
110-75-B
95-49-8
591-78-6
78-63-1
79-46-9
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
107-05-1
71-43-2
108-S6-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
126-99-8
156-59-4
10061-01-5
108-94-1
124-48-1
74-95-3
75-71-8
141-78-6
60-29-7
97-63-2
100-41-4
76-13-1
87-68-3
67-63-0
98-82-8
1330-20-7
126-98-7
74-8&4
80-62-6
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
107-12-0
110-86-1
135-98-8
100-42-5
98-06-6
127-18-4
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPHOPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1.2,4-TRICHLOROBENZENE
1.2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPHOPANE
1.2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
1-BUTANOL
2,2-DICHLOROPHOPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
2-METHYL-1-PROPANOL
2-NITROPROPANE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4.METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
ALLYL CHLORIDE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CHLOROPRENE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
CYCLOHEXANONE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYL ACETATE
ETHYL ETHER
ETHYL METHACRYLATE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYL ALCOHOL
ISOPROPYLBENZENE
M,P-XYLENE
METHACRYLONITRILE
METHYL IODIDE
METHYL METHACRYLATE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
PROPIONITRILE
PYRIDINE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
Result
u
u
u
u
u
u
u
u u
u
u
u u
u
u
u
u
u
u
u u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u u
u
u
u
u
u
u u
u
u
u
u
u
unit?
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
ug/l
ug/!
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/I
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ugfl
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
LablD:L4631-10 Collect Date: 10/04/01 12:30 j
MDL
1
1
1
1
1
1
10
10
1
10
10
10
1
10
1
1
10
10
10
10
18
10
20
.6
10
10
2.1
.9
10
10
10
20
1
1
20
1
10
10
1
1
2
1
1
1
2
1
2
1
10
1
17
1
1
1
1.6
.9
1
1
.5
10
17
10
1
1
1
1
10
10
10
10
1
1
25
10
1
10
1
Dfl.
EQL Factor Method '
5
5
5
5
5
5
10
10
5
10
10
10
5
10
5
5
10
10
10
10
184
10
100
6.4
10
50
21
9.2
10
10
50
100
5
5
100
5
10
10
5
5
10
5
5
5
10
5
10
5
10
5
173
5
5
5
16
9.1
5
5
5.3 1
10 1
174 1
10 1
5 1
5 1
5 1
5 1
10 1
10 1
10 1
10 1
5 1
5 1
249 1
10 1
5 1
10 1
5 1
1 SW-846,8260
1 SW-846, B260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-646,8260
1 SW-646,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-646,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-e46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, B260
SW-846, 8260
SW-846, 8260
SW-fl46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
Analyst
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR 1
MKR •
MKH 1
MKR 1
MKR 1
MKR 1
MKR 1
MKH 1
MKR 1
MKR 1
MKH 1
MKH 1
MKH 1
MKH 1
MKR 1
MKH 1
MKH 1
MKR 1
MKR 1
Page 2
Test Pate
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12rt)1 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 2315
10/12/01 23:15
10/12/01 23:15
10/12/Dl 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
0/12/Ql 23:15
10/12/01 23:15
10/12/01 23:15
a/12/01 23:15
10/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
10/12/01 23:15
0/12/01 23:15
0/12/01 23:15
t0/ia/Dl 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12A)1 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
0/12/01 23:15
lof 28
108-8B-3
156-60-5
10061-02-6
110-57-6
79-01-6
75-69-4
108-05-4
75-01-4
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRANS-1,4-DlCHLORO-2-BLrrEN
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ICP METALS DIGESTION
U
U
U
U
3.7
U
U
U
.5
U
295
U
U
48
U
U
U
U
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
10
1
1
1
2
.2
1.5
25
1
2
2
5
25
60
3
5
5
5
10
5
5
5
10
.7
4.3
125
5
10
10
25
125
300
15
1 SW-B46,8260
1 SW-846,8260
SW-B46, 8260
SW-B46, B260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
SW-846, 7470A
SW-846, 7060
SW-846, 6010
SW-B46, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-B46, 6010
SW-846, 3010
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
CWS
CWS
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/12/01 23:15
10/18/01 14:47
10/26/01 15:00
10/30/01 12:22
10/30/01 12:22
10/30/01 12:22
10/30/01 12:22
10/30/01 12:22
10/30rt)1 12:22
10/30/01 12:22
10/30/01 12:22
10/25/01 12:00
Page 22 Of 28
. V
Isample ID: BW-1-4-FB-1
CAS
Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-5B-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
71-36-3
590-20-7
78-93-3
110-75-8
95-49-B
591-78-6
78-83-1
79-46-9
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
107-05-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
126-99-8
156-59-4
10061-01-5
108-94-1
12448-1
74-95-3
75-71-8
141-78-6
60-29-7
97-63-2
100-41-4
76-13-1
87-6B-3
67-63-0
96-82-6
1330-20-7
126-98-7
74-88-4
80-62-6
75-09-2
104-51-B
103-65-1
91-20-3
1330-20-7
107-12-0
110-86-1
135-98-8
100-42-5
98-06-6
127-18-4
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHyLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
1-BUTANOL
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
2-METH YL-1 -PROPANOL
2-NITROPROPANE
4-CHLOROTOLUENE
4.ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
ALLYL CHLORIDE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CHLOROPRENE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
CYCLOHEXANONE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLOHODIFLUOHOMa-HANE
ETHYL ACETATE
ETHYL ETHER
ETHYL METHACRYLATE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIEN E
ISOPROPYL ALCOHOL
ISOPROPYLBENZENE
M,P-XYLENE
METHACRYLONITRILE
METHYL IODIDE
METHYL METHACRYLATE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
PROPIONITRILE
PYRIDINE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
Result
U
u
U
u u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u u
u
u
u
u
u
u
u
u
u u
u
u
u
u u
u u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
Units
ug/l
ug/l
ug/i
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/I
ug/l
LablD:L4631-11 Collect Date: 10/04/01 12:30 |
MDL
1
1
1
1
1
1
10
10
1
10
10
10
1
10
1
1
10
10
10
10
18
10
20
.6
10
10
2.1
.9
10
10
10
20
1
1
20
1
10
10
1
1
2
1
1
1
2
1
2
1
10
1
17
1
1
1
1.6
.9
1
1
.5
10
17
10
1
1
1
1
10
10
10
10
1
1
25
10
1
10
1
DiL
EQL Factor Method
5
5
5
5
5
5
10
10
5
10
10
10
5
10
5
5
10
10
10
10
184
10
100
6.4
10
50
21
9.2
10
10
50
100
5
5
100
5
10
10
5
5
10
5
5
5
10
5
10
5
10
5
173
5
5
5
16 1
9.1
5
5
5.3 1
10 1
174 1
10 1
5 1
5 1
5 1
5 1
10 1
10 1
10 1
10 1
5 1
5 1
249 1
10 1
5 1
10 1
5 1
1 SW-646,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46,8260
1 SW-B46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46, 8260
1 SW-B46,8260
1 SW-846,8260
1 SW-846, 8260
I SW-846,8260
SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKH
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKH
MKH
MKR
MKR
MKR
MKR
IfiSt Date
10/12/01 23:50
10/12/01 23.50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12A)1 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/0123:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12A)1 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12A)1 23:50
10/12/01 23:50
10/12/0123:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
Page 23 Of 28
10B-88-3 TOLUENE
156-60-5 TRANS-1,2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
110-57-6 TRANS-1,4-DICHLORO-2-BUTEN
79-01-6 TRICHLOROETHENE
75-69-4 TRICHLOROFLUOROMETHANE
108-05-4 VINYL ACETATE
75-01 -4 VINYL CHLORIDE
u
u u u 1.1
u u u
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
10
1
1
1
2
5
5
5
10
5
5
5
10
SW-B46, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKR
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
10/12/01 23:50
Page 24of 28
1 Sample
CAS
Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
71-36-3
590-20-7
7B-93-3
110-75-8
95-49-8
591-78-6
78-83-1
79-46-9
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
107-05-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
126-99-8
156-59-4
10061-01-5
108-94-1
124^-1
74-95-3
75-71-8
141-78-6
60-29-7
97-63-2
100-41-4
76-13-1
87-68-3
67-63-0
98-B2-B
1330-20-7
126-98-7
74-88-4
80-62-6
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
107-12-0
110-86-1
135-98-8
100-42-5
98-06-6
127-1 B-4
D: BW-1-4-TB-5
Test Parameter
1,1,1,2-TETRACHLOROETH AN E
1,1,1 -TRICHLOROETHANE
1,1,2,2-1 h 1 RACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1.2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
1-BUTANOL
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
2-METH YL-1-PROPANOL
2-NITROPROPANE
4-CHLOROTOLUENE
4-ISOPHOPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
ALLYL CHLORIDE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON IhrRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CHLOROPRENE
CIS-1,2-DICHLOROETHENE
CIS-1.3-DICHLOROPROPENE
CYCLOHEXANONE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYL ACETATE
ETHYL ETHER
ETHYL METHACRYLATE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYL ALCOHOL
ISOPROPYLBENZENE
M,P-XYLENE
METHACRYLONITRILE
METHYL IODIDE
METHYL METHACRYLATE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
PROPIONITRILE
PYRIDINE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
I'ETHACHLOROETHENE
Result
U
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u u
u
u
u
u u u
u
Units.
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
LablD:L4631-12 Collect Date: 10/02/01 09:30 j
MDL
1
1
1
1
1
1
10
10
1
10
10
10
1
10
1
1
10
10
10
10
18
10
20
.6
10
10
2.1
.9
10
10
10
20
1
1
20
1
10
10
1
1
2
1
1
1
2
1
2
1
10
1
17
1
1
1
1.6
.9
1
1
.5
10
17
10
1
1
1
1
10
10
10
10
1
1
25
10
1
10
1
Dil.
EQL Factor Methpd <
5
5
5
5
5
5
10
10
5
10
10
10
5
10
5
5
10
10
10
10
184
10
100
6.4
10
50
21
9.2
10
10
50
100
5
5
100
5
10
10
5
5
10
5
5
5
10
5
10
5
10
5
173
5
5
5
16
9.1
5
5
5.3 1
10 1
174 1
10 1
5 1
5 1
5 1
5 1
10 1
10 1
10 1
10 1
5 1
5 1
249 1
10 1
5 1
10 1
5 1
1 SW-846,8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, B260
1 SW-B46, B260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
1 SW-846,8260
SW-84e, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, B260
SW-B46, 8260
SW-B46, 8260
SW-846, 8260
SW-846, B260
SW-846, 8260
SW-B46, 8260
Analyst
MKR
MKR
MKR
MKH
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR 1
MKR -
MKR -
MKR -
MKR
MKH
MKH -
MKH
MKR 1
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR -
MKR
MKR 1
MKR -
MKR
MKR
MKR 1
MKR 1
MKR
MKR
MKR
MKR 1
MKR 1
MKR 1
MKR 1
MKR 1
MKR -
MKR 1
MKR 1
Page 2
Test Date
0/13/01 12:24
10/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
10/13/01 12:24
10/13/01 12:24
10/13/01 12:24
10/13/01 12:24
0/13/01 12:24
10/13/01 12:24
10/13/01 12:24
0/13/01 12:24
0/13/01 12:24
10/13/01 12:24
10/13/01 12:24
10/13/01 12:24
0/13rt)1 12:24
10/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
10/13/01 12:24
10/13/01 12:24
10/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13rt)l 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
0/13/01 12:24
5of28
10B-B8-3 TOLUENE
156-60-5 TRANS-1,2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
110-57-6 TRANS-1,4-DICHLORO-2-BUTEN
79-01-6 TRICHLOROETHENE
75-69-4 TRICHLOROFLUOROMETHANE
108-05-4 VINYL ACETATE
75-01-4 VINYL CHLORIDE
U
u u
u u
u u
u
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
10
1
1
1
2
5
5
5
10
5
5
5
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
10/13/01 12:24
10/13/01 12:24
10/13/01 12:24
10/13/01 12:24
10/13/01 12:24
10/13/01 12:24
10/13/01 12:24
10/13/01 12:24
Page 26 of 28
IsamplelD: BW-1-4-23.3-25
CAS
Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-1 B-4
120-B2-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-2B-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
10B-B6-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-11TRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOHOBENZENE
1,2,4-TRIMETHYLBENZENE
1,2.DIBROMO-3-CHLOROPHOPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBEN2ENE
2,2-DICHLOROPROPANE
2-BUTANONE
2.CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULRDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHAN E
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
Result
u
u u
u u
u u u u u u
u u u
u u
u u
u u
u u
u u u u u
u Ufi
u u u u u u u u u u
u u u u u u u u u u
u u u u u
u u u u u u u u
u u u u u
u u
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
LablD:L4631-13 ' Collect Date: 10/03/0111:05 |
MDU
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
DM.
EQL Factor Method'
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846. 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-646,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-e46.8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-646, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-646, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analvst
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKH
MKH
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR -
MKH '
Te.st Date
10/16/0121:07
10/16/0121:07
0/16/0121:07
10/16/0121:07
10/16/0121:07
10/16/01 21:07
10/16/01 21:07
10/16/01 21:07
10/16/01 21:07
0/16/01 21:07
0/16/01 21:07
0/16/01 21:07
10/16/01 21:07
10/16/01 21:07
10/15/01 21:07
10/16/01 21:07
0/16/01 21:07
0/16/0121:07
10/16/0121:07
10/16/0121:07
10/16/0121:07
10/16/0121:07
10/16/0121:07
0/16/01 21:07
0/16/01 21:07
0/16A)1 21:07
10/16/01 21:07
10/16/01 21:07
10/16/01 21:07
10/16/01 21:07
0/15/0121:07
10/16/0121:07
10/16/0121:07
10/16/0121:07
10/16/0121:07
10/16/0121:07
10/16/0121:07
10/16/0121:07
0/16/0121:07
0/16/0121:07
0/16/01 21:07
0/16/01 21:07
10/16rt)1 21:07
10/16/01 21:07
0/16rt)1 21:07
0/16/01 21:07
0/16/01 21:07
10/16/01 21:07
10/15/01 21:07
10/16/0121:07
10/16/01 21.-07
0/15/0121:07
0/15/01 21:07
0/16/0121:07
0/16/0121:07
0/16/01 21:07
0/16/01 21:07
0/16/01 21:07
0/16/01 21:07
0/16/01 21:07
0/16/01 21:07
0/16/01 21:07
0/16/01 21:07
0/16rt)1 21:07
0/16/01 21:07
0/16/01 21:07
0/16/01 21:07
0/16/01 21:07
0/16/01 21:07
Page 27 Of 28
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected but was
below the MDL.
B Gas Chromatography and Mass Spectral Data Flag. This flag is used when an analyte is found in
the blank as well as the sample
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This flag is used
either when estimating a concentration tor tentatively identified compounds or when the data
indicated the presence of a compound that meets the identification criteria but the result is less than
the EQL (e.g. 3 J with an EQL of 10)
MDL Method Detection Limit: The minimum concentration of a substance that can be confidently
measured and reported. The laboratory has demonstrated that the MDL can be achieved in a
laboratory reagent blank, but does not guarentee it can be achieved in all sample matrices.
The MDL is approximately three times the signal noise levei.
EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many
analytes the EQL is selected cis the value of the lowest standard in the calibration curve.
Dil. Factor Dilution Factor: The prepared smple was diluted by this factor because the sampie was too
concentrated or due to other interferences in the sample matrix. Any dilution factor causes
an appropriate increase in the MDL and EQL.
Page 28 of 28
SCIENCE AND ENGINEERING THtaKOL
Control of Environmentai Samples
Document No.
SOP-102
Effective Date
14 July 98
Issue
5
Page
3 Of 4
Sample Receipt Checklist
LWR/PO No: /_ (/ U 3/
Receipt Date: /^ » ^^^ - tP /
Received by: //(/^S
LabID: /. f/^ 3/ :<yes No
Samples for Compiiance Testing
Chairs of Custody (COC)
If No, was a COC initiated at receipt?
7^ Custody Seal on Shipping Container
Custody Seals on Sample Containers
-P^ Samples Accompanied by Airtiill or Bill of Laden
Samples Property Labeled
If No, explain:
Are sample quantities adequate for required testing? -z^
If No, explain:
17-Are samples in appropriate containers?
If No, explain:
Are samples within holding times? 1^
If No, explain:
Are all sample containers assigned unique laboratory numbers? HA.
If no, assign unique numbers
Temperature of sample at time of receipt: HtCCljHX^/l^ (^cro/'*^^ *^//c^ Y0*'^'^V*C
pHLog
Sample ID: k-
Initial pH:
Final pH:
-^ 7^
ATK
ALLIANT TECHSYSTEMS
LWR-FY01 -D1609
5 November 2001
TO:
CC:
FROM:
LWR:
WO:
J. Hermance
F. E. Bares and L. Lof gren
L. V. Dearden
L4599 and L4631
M1101
Thiokol Propulsion
P.O. Box 707
Brigham City, Utah 84302-0707 USA
Tel: [phone]
Fax: [phone]
SUBJECT: Soil Moisture
Results for the soil moisture content are given below in tabular form. Samples were tested using the
ASTM Method: D2216-98 - Standard Test Method for Laboratory Determination of Water(Moisture)
Content of Soil and Rock by Mass.
Sample
Percent
Moisture
L4599-1
L4599-3
L4631-
L4631-
L4631-
L4631-
L4631-
L4631-
L4831-8
L4631-9
-1
-2
-4
-5
-6
-7
11.4
11.6
12.0
11.9
12.2
12.9
11.8
12.1
11.9
11.8
If you have any questions feel free to contact us at ext. 2744.
M, T. Burnett
L. V. Dearden
Chemical and Physical Analysis
L4599
Login Number_
EPA Method _
SOP Number"
Work Group Number
Arsenic QC Data Package Checklist
L4599
7060
311
WG7700
A complete description of sample and standards preparation is located in the "Standards
Preparation Log" and "Digestion Log"
Standard Soluiton: Standard Concentration QC Concentration (ppb)
Standard 1
Standard 2
Standard 3
Standard 4
5 ppb
25 ppb
50 ppb
100 pbb
LFB
ICV
QCS
CCV
50.0
50.0
20.0
50.0
Spike Preparation: The preparation of matrix spikes and matrix spike duplicates
is described in the "Digestion Log", Spike Concentration
after final dilution is typically 25 ppb.
Analyst:
Peer review:
Comments:
All QC acceptable
!> Date: ^/X/y ^/
Date:
Package Includes: Autosampler Table X
QC Report 2<_
Work Group Report X
Data Review X
Raw data stored with Login Number
Data package includes data from Login Number(s) L4599
L4631
Login N umber _
EPA Method _
SOP Number^
Work Group Number
Arsenic QC Data Package Checklist
L4599
7060
311
WG7675
A complete description of sample and standards preparation is located in the "Standards
Preparation Log" and "Digestion Log"
Standard Soluiton: Standard Concentration QC Concentration (ppb)
Standard 1
Standard 2
Standard 3
Standard 4
5 ppb
25 ppb
50 ppb
100 pbb
LFB
ICV
QCS
CCV
50.0
50.0
20.0
50.0
Spike Preparation:
Analyst:
Peer review:
Comments:
All QC acceptable
The preparation of matrix spikes and matrix spike duplicates
is described in the "Digestion Log". Spike Concentration
after final dilution is typically 25 ppb.
Date:
Date:
^J/VJ
Package Includes: Autosampler Table L4560
QC Report 2<
Work Group Report 2<
Data Review X
Raw data stored with Login Number L4560
Data package includes data from Login Number(s)
/
Login Number _
EPA Method _
SOP Number'
Work Group Number_
Mercury QC Data Package Checklist
L4599
7471A
316
WG7650
A complete discription of QC, sample and standards preparation is located in the "Mercury
Analysis Log Book".
Standard Concentration QC Concentration
LFB
ICV
QCS
CCV
Spike Preparation: The preparation of matrix spikes and matrix spike duplicates is descnbed
in the "Mercury Analysis Log Book". Spike concentration after final
dilution is usually 4 ppb Hg.
Standard 1
Standard 2
Standard 3
Standard 4
Standard 5
1 ppb
2 ppb
5 ppb
10 ppb
20 ppb
4 ppb
5 ppb
10.0
5 ppb
Analyst:
Peer review:
Date:
Date: yy/-xya/
Comments:
Package Includes: Autosampler Table 2£.
QC Report 2<_
Work Group Report X
Data Sheet 2<_
Sample Prep Sheet X
Raw data stored with Login Number
Data package includes data from Login Number(s) L4599
L4631
Login Number_
EPA Method _
SOP Number^
Work Group Number
Mercury QC Data Package Checklist
L4599
7470A
316
WG7601
A complete discription of QC, sample and standards preparation is located in the "Mercury
Analysis Log Book".
Standard Concentration QC Concentration
Standard 1
Standard 2
Standard 3
Standard 4
Standard 5
1 ppb
2 ppb
5 ppb
10 ppb
20 ppb
LFB
ICV
QCS
CCV
4 ppb
5 ppb
10.0 ppb
5 ppb
Spike Preparation: The preparation of matrix spikes and matrix spike duplicates is described
in the "Mercury Analysis Log Book". Spike concentration after final
dilution is usefally 4 ppb Hg.
Analyst:
Peer review:
Comments:
All QC acceptable.
J^ yt>r Date: ^V/oA?
Date: // kA,
Package Includes: Autosampler Table L4602
QC Report 2<
Work Group Report 2<
Data Sheet X
Sample Prep Sheet L4602
Raw data stored with Login Number
Data package includes data from Login Number(s)
L4602
EPA SW-846 6010 QC Data Package Checklist
Login Number
EPA Method _
lA/ork Group Nunnber
Run Number
Standard Solution:
MSTDl
MSTD2
MSTD3
MSTD4
MSTD5
Cal Blank
L4599
6010
WC76a8 ^6 li^S
-R30900 ' £_3o f/i
Log Identification
10/29/2001
10/29/2001
10/29/2001
10/29/2001
10/30/2001
NA
QC Solutions: Log Identification
LPC
QC-21
QC-7
QC-7 IOX
QC-Sn
QC-P
10/26/2001
10/19/2001
10/15/2001
10/29/2001
7/10/2001
9/38/2001
SIC
LFB
Matrix Spike
QC Samples:
0/29, 10/16,&10/17/01
LOmLof LFS 10/16/01
'.OmLof LFS 10/16/01
L4595-5, L4599-2,
&L4611-3
Analyst:
Peer review by:
Comments
Date: /•/<- /"i^^
Date: /'M'^n
^^H^.
gjujii, <7.Z)t.
«<•*
/^^^tiyi*>^ ^-i^^ ^>->^ '••'^^ ^
VL9Sf1
Package Includes: Autosampler Table
QC Report
Work Group Report
Bench Sheet
Data Review
NA.
AS ^i,fC^/
g
^
^aJ^ ^pC Mil ^t^
Raw data stored with Login Number L4595
Data package includes data for Login Number(s) L4595, L4599, L4611,
L4631,&L4651
^
Login Number
EPA Method
SOP Number
Work Group Number
Standard Solution:
QC
Spik€
Spike F
^
Matrix
Analyst:
Peer review:.
Comments:
All QC acceptable.
Nitrite-N QC Data Package Checklist
L4599
300.0
341
WG7596
Autocall R
Autocal2R
AutocalSR
AutocaWR
AutocalSR
:; Solutions:
ICV
CCV
} Stock Sol.
Spike
'reparation:
latrix Spike
Spike Dup.
^/^
Log Identification
CWS-86-489
CWS-86-488
CWS-86-487
CWS-86-486
CWS-86-485
Log Identification
CWS-86-488
CWS-86-486
CWS-40-176
mL of Sample
5.00
5.00
^^
dt^^^>'^^^——
Date:
Date:
Concentration (ppm)
Nitrite-N
0.5
2
5
10
20
Concetration (ppm)
Nitrite-N
2
10
2000
4
uL of Stock
Nitrite-N
10
10
Package Includes: Autosampler Table
QC Report
Work Group Report
Bench Sheet ;
Data Review \
Raw data stored with Login Number
Data package includes data from Login Number(s)
X
X
Work Group Summary Report
Quality Con-trol Data
Analysis: PH 9045 Method: SW 846, 9045
Report Date: 02-OCT-Ol
Summary of QC Samples
Sample QP
Ntimber Type Description
WG7554 -1 QCS Independent Check Standard
WG7554
QC Measured Values with Limits
%Recov Limits
101 80-120
Summary of Spiked Samples
Sample QC Reference Sample
Nnmher Type Number
WG7554-2 DUP L4599-3 9.09
Samples In Workgroup
L4599-1 L4599-3
9.03
Spiked Measured Values with Limits
RPD Limits
0.66 0-20
Date (;:s~acf^sx^
Date C^'Z-^U-^f
VOLATILE ORGANICS
DATA PACKAGE REFERANCE
Sampie Login No. L ^^^^
Date Run O'L QCX^'1J^{ WorkGroup [jj (j. -ft-^Lff
The data pack is filed with sample number [^ ^'?^^^ -/ . / z.
VoistJle Organics Data Package Checklist
Sample Login No: Lnc^^q
Work Group: <oer7«^^«;
Dats Run: C^^irT IJJMK
Method:,
Matrix:
^IhO
ii-'/VTgg
Instrument ID: \iiPlZ
pg seP is^i IniiicI Calibraticn Locaiicn:
Run Log
BF5 Tune Report
Continuing Calibrsticn: Quant Rcport/Chromatccram
Ccntinuing Caiibraticn Check Report
Reagent Blank: Cuant ReporjChrcmatcgram '
Samcles:Guant Repcn/Chrcm.aiccram
Samples: TiC Data
Matrix Spike: Guant Repcn/Chrcma:ccra.m
Matrix Spike Cupiicais: Guam RepoPL/Chrcmatccram
Inte.T.al Stancard Area Reccr;
Surccate h. Scik£.''Cuciic3te Recove.'"/ r.^zzr..
.^rec/Extracticn Leg
rrese."/a"ncn Chec:<
Peer Review
Work Group Summary Report
Quality Control Data
Analysis: PH 9045 Method: SW 846, 9045
Report Date: 02-OCT-OI
Siumaaify of QC Samples
Sample QC
Number Type Description
WG7554-1 QCS Independent Check Standard
WG7554
QC Measured Values with Limits
%Recov Limits
101 80-120
Summary of Spiked Samples
Sample QC Reference Sample
Type Number Number
WG7554-2 DUP L4599-3 9.09 9.03
Spiked Measured Values with Limits
RPD Limits
0.66 0-20
Samples In Workgroup
L4599-1 L4599-3
Ana
Peer Review:
Date ($32-^;g^"^^y
-Date cr2.^cJ-^/
CERTIFICATE OF ANALYSIS
Listing of sample Information and Testing Requested
Friday, December 7, 2001
TESTED FOR ATK Thiokol: Bacchus
Environmental Compliance M/S M7H7
P. O. Box 98
Magna, UT 84044-0098
Jon Hermance
Project: Lab Anal - Rem - Soil
Login Number L4599
Lab No Client Number
Test Requested Description
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-3732
800-863-8080
Received CollectDate/Time
Matrix
1 L4599-1 BW-1-3-50-51.7
SW-846, 8260
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
1 L4599-2 BW-1-3-EB-3
SW-846, 8260
SW-846, 7470A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3010
1 L4599-3 BW-1-3-60-61.7
SW-846, 8260
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
1 L4599-4 BW-1-3-66.7-68.3
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Volatile Organics Appendix 9
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
ICP Metals Digestion
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
10/02/01 09/24/01 11:50
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
10/02/01 09/25/01 08:30
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
10/02/01 10/01/01 11:00
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
10/02/01 10/01/01 14:40
1
1
SW-846, 8260 Volatile Organics Soil
Page lof 12
L4599-5 BW-1-3-TB-4 10/02/01 09/24/01 08:40
SW-846, 8260 Volatile Organics /Appendix 9 Water
Comments:
L4599-1 6010 Metals: There was evidence of a slight matrix interference for Cd, Cr, Pb, Se, and Ag for
this matrix.
Certified By ^cw^ N CHC^V^ 7- OH^- 7P01
QC Coordinator 'A Date
Ttiis certifies ttiat ttie following samples were analyzed using good laboratory practices to stiow the following results:
Page 2 of 12
Listing of Results by Sample
1 Sample ID: BW-1-3-50-51.7
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-1
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-O2-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-9O-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
155-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
Test Parameter
1,1.1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBEN2ENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBEN2ENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1.2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPBOPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPBOPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOHOTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
Result
u
u
u u u u u u
u u u u
u u u u
u u
u u u
u u
u u u
u u
ynits
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
9.6TU6 ug/kg
u u u u
u u u u u
u u u u u u u u
u u u u u u u
u u u
u u u
u u u u u
u u u u
u u 4.63
8840
117
.5
.5
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L4599-1 Collect Date: 09/24/01 11:50 |
MDL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.01
.9
13
.05
.1
.1
Dll.
EQL Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
.04
3.1 2
6.4 1.1
.3 1.1
.5 11
.5 1.1
1 SW-846, 8260
1 SW-846
1 SW-846
1 SW-846
1 SW-e46
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-B46
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-B46
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-B46
1 SW-846
1 SW-e46
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
: SW-846
t SW-846
1 SW-846
1 SW-846
SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
0 SW-846
29 SW-846
29 SW-846
29 SW-846
29 SW-846
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
6260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
7471A
7060
6010
6010
6010
6010
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
CWS
MTB
MTB
MTB
MTB
Page
Test Pat«
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
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10/02/01 18:02
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10/02/01 18:02
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10/02AD1 18:02
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10/02/01 18 02
10/02/01 18:02
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10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02rt)1 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10«)2/01 18:02
10flD2/01 18.02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10A)2/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10^2/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/02/01 18:02
10/22/01 14:07
10/31/01 13:57
10/30/01 14:10
10/30/01 14:10
10/30/01 14:10
10/30/01 14:10
3of 12
i>'^ I^-.^'i^%^'^^
C?:^ S^-^s., .^
0 i^g' .3
9. <-/ -^0.7 -^ IS ,'^2S •Sk,^
1 ^r'V'*^ ^
1 Sample ID: BW-1-3-EB-3
CAS
Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-1
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
71-36-3
590-20-7
78-93-3
110-75-8
95-49-8
591-78-6
78-83-1
79-46-9
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
107-05-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
126-99-8
156-59-4
10061-01-5
108-94-1
124-48-1
74-95-3
75-71-8
141-78-6
60-29-7
97-63-2
100-41-4
76-13-1
87-68-3
67-63^)
98-82-8
1330-20-7
126-96-7
74-88-4
80-62-6
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
107-12-0
110-86-1
135-98-8
100-42-5
98-06-6
127-18-4
Tflst Parameter
1,1 1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETHACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
1-BUTANOL
2,2-DICHLOHOPROPANE
2-BUT ANONE
2-CHLOHOETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
2-METH YL-1-PROPANOL
2-NITROPROPANE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
ALLYL CHLORIDE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CHLOROPRENE
CIS-1.2-DICHLOROETHENE
CIS-1.3-DICHLOROPROPENE
CYCLOHEXANONE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYL ACETATE
ETHYL ETHER
ETHYL METHACRYLATE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYL ALCOHOL
ISOPROPYLBENZENE
M.P-XYLENE
METHACRYLONITRILE
METHYL IODIDE
METHYL METHACRYLATE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
PROPIONITRILE
PYRIDINE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
Result
U
u
u
U
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u u
u
u u
u
u
u
u
u
u u
u
u
u
u
u u
u
u
u
u
u
1.2 XT-
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u u
u
u
u
u
u
Units
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
Lab ID: L4599-2 Collect Date: 09/25/01 08:30 |
MPL
1
1
1
1
1
1
10
10
1
10
10
10
1
10
1
1
10
10
10
10
18
10
20
.6
10
10
21
9
10
10
10
20
1
1
20
1
10
10
1
1
2
1
1
1
2
1
2
1
10
1
17
1
1
1
1.6
.9
1
1
.5
10
17
10
1
1
1
1
10
10
10
10
1
1
25
10
1
10
1
Dll.
IQL Factor MgUifid
5
5
5
5
5
5
10
10
5
10
10
10
5
10
5
5
10
10
10
10
184
10
100
64
10
50
21
9.2
10
10
50
100
5
5
100
5
10
10
5
5
10
5
5
5
10
5
10
5
10
5
173
5 1
5 1
5
16 1
9.1 1
5 1
5 1
5.3 1
10 1
174 1
10 1
5 1
5 1
5 1
5 1
10 1
10 1
10 1
10 1
5 1
5 1
249 1
10 1
5 1
10 1
5 1
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 6260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-B46, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analjal
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
Page
Test Date
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10rt)3/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03rt)1 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
5of12
108-88-3
156-60-5
10061-02-6
110-57-6
79-01-6
75-69-4
108-05-4
75-01-4
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRANS-1,4-DICHLORO-2-BUTEN
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ICP METALS DIGESTION
U
U
u
u u u u u u u 54
1.6
U
5.7
U
27
U
U
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
1
1
1
10
1
1
1
2
.2
1.5
25
1
2
2
5
25
60
3
5
5
5
10
5
5
5
10
.7
4.3
125
5
10
10
25
125 ^
300
15 -
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
SW-846, 7470A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3010
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
CWS
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/03/01 17:09
10/10/01 12:07
10/26/01 14:49
10/30/01 12:42
10/30/01 12:42
10/30/01 12.42
10/30/01 12:42
10/30/01 12:42
10/30/01 12:42
10/30/01 12:42
10/30/01 12:42
10/25^1 12:00
Page 6 of 12
1 Sample
630-20-6
71-55-6
79-34-5
79-00-S
75-34-3
75-35-1
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-13-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
ID: BW-1-3-60-61.7
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1.1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1.1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOHOPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1.2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-lSOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1.2-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-18-1
74-95-3
75-71-8
100-11-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-12-5
98-06-6
127-18-1
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u u
u
u
u
u
Units.
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/Kg
ug/kg
ug/kg
ug/kg
ug/kg
8.83-ftug/kg
u
u
u
u u
u
u
u
u
u
u u
u
u u
u
u
u
u u
u
u u
u u
u
u
u
u u
u
u
u
u u
u u u u
u
u
5.54
6140
321
.3
.3
11
7.2
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L4599-3
MDL
.6
6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
6
.5
8
1
8
6
.7
.7
4
.7
.3
.5
.4
1
.7
1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
6
6
.5
.7
4
5
.6
.5
.3
.5
01
1
14
06
.1
.1
.3
1.4
Oil.
EQL Factor
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
50 1
10 1
10 1
50 1
10 1
10 1
50 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
.04 1
34 20
7.1 1.131
.3 1.131
.6 1.131
.6 1.131
1.4 1.131
7.1 1.131
Collect Date: 10/01/01 11:00 |
Methpd
SW-846. 8260
SW-B46, 8260
SW-846, 8260
SW-846. 8260
SW-B46. 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 6260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-B46. 8260
SW-B46. 8260
SW-846. 8260
SW-846, 8260
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
Page
Test Date
10/02/01 18:36
10/02/01 18.36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18.36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10«)2/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10rt)2/01 18:36
10i«2/01 18:36
10/02/01 18:36
10/02AD1 18:36
10/02/01 18:36
10/02«)1 18:36
10/02A)1 18:36
10/02^)1 18:36
10/02/01 18:36
10/02/01 18:36
10rt)2/01 18:36
10rt32/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02rt31 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02A31 18:36
10/02A31 18:36
10/02A)1 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/02/01 18:36
10/22/01 14:10
10/31/01 14-41
10/30/01 14:20
10/30/01 14:20
10/30/01 14:20
10/30/01 14:20
10/30/01 14:20
10/30/01 14:20
7of 12
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NITRATE-N
NITHITE-N
PH
u U
.083
U
9.09
ug/g
ug/g
mg/l
mg/l
3.4
.2
.01
.01
17
.8
.05
.05
1.131
1.131
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
CMF
10/30/01 14:20
10/30/01 14:20
10/24/01 12:00
10/09/01 13:11
10/09/01 13:11
10/02/01 12:00
Page 8 of 12
jSamplelD: BW-1-3-66.7-68.3 Lab ID: L4599-4 Collect Date: 10/01/0114:40
CAS
Number Test Parameter
630-20-6 1,1,1,2-TETRACHLOROETHANE
71-55-6 1,1,1-TRICHLOROETHANE
79-34-5 1,1,2,2-TETRACHLOROETHANE
79-00-5 1,1,2-TRICHLOROETHANE
75-34-3 1,1-DICHLOROETHANE
75-35-4 1,1-DICHLOROETHENE
563-58-6 1,1-DICHLOROPROPENE
87-61-6 1,2,3-TRICHLOROBENZENE
96-18-4 1,2.3-TRICHLOROPROPANE
120-82-1 1,2,4-THICHLOROBEN2ENE
95-63-6 1,2,4-TRIMETHYLBENZENE
96-12-8 1,2-DIBROMO-3-CHLOROPROPANE
106-93-1 1,2-DIBROMOETHANE
95-50-1 1,2-DICHLOROBENZENE
107-06-2 1,2-DICHLOROETHANE
78-87-S 1,2-DICHLOROPROPANE
108-67-8 1,3,5-TRIMETHYLBENZENE
541-73-1 1,3-DICHLOROBENZENE
142-28-9 1,3-DICHLOROPROPANE
106-46-7 1,4-DICHLOROBENZENE
590-20-7 2,2-DICHLOROPROPANE
78-93-3 2-SUTANONE
110-57-8 2-CHLOROETHYLVINYL ETHER
95-49-8 2-CHLOHOTOLUENE
591-78-6 2-HEXANONE
106-43-4 4-CHLOROTOLUENE
99-87-6 4-ISOPROPYLTOLUENE
108-10-1 4-METHYL-2-PENTANONE
67-64-1 ACETONE
107-02-8 ACROLEIN
107-13-1 ACRYLONITRILE
71-43-2 BENZENE
108-86-1 BROMOBENZENE
74-97-5 BROMOCHLOROMETHANE
75-27-4 BROMODICHLOROMETHANE
75-25-2 BROMOFORM
74-83-9 BROMOMETHANE
75-15-0 CARBON DISULFIDE
56-23-5 CARBON TETRACHLORIDE
108-90-7 CHLOROBENZENE
75-00-3 CHLOROETHANE
67-66-3 CHLOROFORM
74-87-3 CHLOROMETHANE
156-59-4 ClS-1,2-DICHLOROETHENE
10061-01-5 ClS-1.3-DICHLOROPROPENE
124-48-1 DIBROMOCHLOROMETHANE
74-95-3 DIBROMOMETHANE
75-71-8 DICHLORODIFLUOROMETHANE
100-11-1 ETHYLBENZENE
76-13-1 FREON 113
87-68-3 HEXACHLOROBUTADIENE
98-82-8 ISOPROPYLBENZENE
1330-20-7 M.P-XYLENE
75-09-2 METHYLENE CHLORIDE
104-51-8 N-BUTYLBENZENE
103-65-1 N-PROPYLBENZENE
91-20-3 NAPHTHALENE
1330-20-7 O-XYLENE
135-98-8 SEC-BUTYLBENZENE
100-42-5 STYRENE
98-06-6 TERT-BUTYLBENZENE
127-18-4 TETRACHLOROETHENE
108-88-3 TOLUENE
156-60-5 TRANS-1,2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOnOPROPENE
79-01-6 TRICHLOROETHENE
75-69-4 TRICHLOROFLUOROMETHANE
108-05-4 VINYL ACETATE
75-01-1 VINYL CHLORIDE
Result
u
Units
ug/kg
2.9 1* ug/kg
u U
u
.5
U
U
U
U
U
u
u u u u u
u u
u u
u u u u u
u u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
4.3X6-ug/kg
U
U
U
U
U
u u
u U
u
u u .7
U
u u u u
u u u u u
u 1.3-0-
u u u
u u u
u u u u u
1.5 T
u u u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
u9/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
MPI-
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
24
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
6
.6
.5
.7
.4
.5
6
.5
.3
.5
Di .
EQL Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10 -
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10
10
10
10
10
10
10
10
10
1 SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-&46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-e46, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
Test Date
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02A)1 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10rtD2/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02A31 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02A)1 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
10/02/01 19:09
Page 9 of 12
Isample ID: BW-1-3-TB-4
CAS
Numbei
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-16-7
71-36-3
590-20-7
78-93-3
110-75-8
95-49-8
591-78-6
78-83-1
79-46-9
106-43-1
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
107-05-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
126-99-8
156-59-4
10061-01-5
108-94-1
124-48-1
74-95-3
75-71-8
141-78-6
60-29-7
97-63-2
100-41-4
76-13-1
87-68-3
67-63-0
98-82-8
1330-20-7
126-98-7
74-88-4
80-62-6
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
107-12-0
110-86-1
135-98-8
tOO-12-5
98-06-6
127-18-4
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOHOBENZENE
1,2.3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1.3.5-TRlMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
1-BUTANOL
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
2-METHYL-1 -PROPANOL
2-NITROPROPANE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
ALLYL CHLORIDE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CHLOROPRENE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
CYCLOHEXANONE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYL ACETATE
ETHYL ETHER
ETHYL METHACRYLATE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYL ALCOHOL
ISOPROPYLBENZENE
M,P-XYLENE
METHACRYLONITRILE
METHYL IODIDE
METHYL METHACRYLATE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
PROPIONITRILE
PYRIDINE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
ResMit
u
U
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u u
u
u
u
u u
u
u u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Unit?
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/7
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
Lab ID; L4599-5 Collect Date: 09/24/01 08:40 |
MDL
1
1
1
1
1
1
10
10
1
10
10
10
1
10
1
1
10
10
10
10
18
10
20
.6
10
10
2.1
.9
10
10
10
20
1
1
20
1
10
10
1
1
2
1
1
1
2
1
2
1
10
1
17
1
1
1
1.6
.9
1
1
.5
10
17
10
1
1
1
1
10
10
10
10
1
1
25
10
1
10
1
Dil.
EQL Factor Method.
5
5
5
5
5
5
10
10
5
10
10
10
5
10
5
5
10
10
10
10
184
10
100
6 4
10
50
21
9.2
10
10
50
100
5
5
100
S
10
10
5
5
10
5
5
5
10
5
10
5
10
5 1
173
5 1
5
5 1
16 1
9.1 1
5 1
5 1
5.3 1
10 1
174 1
10 1
5 1
5 1
6 1
5 1
10 1
10 1
10 1
10 1
5 1
5 1
249 1
10 1
5 1
10 1
5 1
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846.8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46, 8260
1 SW-846,8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846.8260
I SW-846,8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-84€, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 6260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
lest Pate
10/03(101 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03rt)1 17:42
10/03/01 17:42
10/03«)1 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03«1 17:42
10/03fl1 17:42
10/03«)1 17:42
10103m 17:42
10/03(01 17:42
10/03/01 17:42
10/03/01 17:42
10/03«)1 17:42
10/03rt)1 17:42
10/03rt31 17:42
10/03/01 17:42
10/03roi 17:42
10/03rt)1 17:42
10rt)3/01 17:42
10/03/01 17:42
10«)3rt)1 17:42
1QrtJ3rt)1 17:42
10/03rt)1 17:42
10/03rt31 17:42
lOraroi 17:42
lO/Oarai 17:42
10/03rai 17:42
10/03rt)1 17:42
10/03«)1 17:42
10/03A)1 17:42
lOJQSm 17:42
10/03rt)1 17:42
10/03/01 17:42
10KX3K)1 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10rt)3mi 17:42
1Q/03rai 17:42
10/03rtl1 17:42
10/03rt)1 17:42
10/03/01 17:42
10/03/01 17.42
10rt)3/01 17:42
10/D3A31 17:42
10/03/01 17:42
10/03/01 17 42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03«)1 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
Pagel Oof 12
108-88-3 TOLUENE
156-60-5 TRANS-1,2-DICHLOROETHENE
10061 -02-6 TRANS-1,3-DICHLOROPROPENE
110-57-6 TRANS-1,4-DICHLORO-2-BUTEN
79-01-6 TRICHLOROETHENE
75-69-4 TRICHLOROFLUOROMETHANE
108-05-4 VINYL ACETATE
75-01-4 VINYL CHLORIDE
U
u U
U
U
u u u
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
10
1
1
1
2
5
5
5
10
5
5
5
10
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-845, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
10/03/01 17:42
PageUof 12
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected but was
below the MDL.
B Gas Chromatography and Mass Spectral Data Flag. This flag is used when an analyte is found in
the blank as well as the sample
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This flag is used
either when estimating a concentration for tentatively identified compounds or when the data
indicated the presence of a compound that meets the identification criteria but the result is less than
the EQL (e.g. 3 J with an EQL of 10)
MDL Method Detection Limit: The minimum concentration of a substance that can be confidently
measured and reported. The laboratory has demonstrated that the MDL can be achieved in a
laboratory reagent blank, but does not guarentee it can be achieved in all sample matrices.
The MDL is approximately three times the signal noise level.
EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many
analytes the EQL is selected as the value of the lowest standard in the calibration curve.
Dil. Factor Dilution Factor: The prepared smple was diluted by this factor because the sample was too
concentrated or due to other interferences in the sample matrix. Any dilution factor causes
an appropriate increase in the MDL and EQL.
Page12of 12
THIOKOL Corporation
THIOKOL ENVIRONIVIENTAL LABORATORY
INVOICE
TEJiJ— Customer Purchase Order No Invoice Date
08-NOV-01
Voucher No Invoice No
BILL TO:
Alliant Techsystems
ATK Thiokol: Bacchus
Environmental Compliance M/S M7H'.
P. O. Box 98
Magna, UT 84044-0098
SEND PAYIMENT TO:
Thiokol Corporation
Space Operations
Attn: General Accounting, M/S T12
P.O. Box 707
Brigham City, UT 84302-0707
Login No: L45g9
Sample ID (Client ID):
L4599-1(BW-1-3-50-51.7),
L4599-5(BW-1-3-TB-4),
Received Date 02-OCT-OI
L4599-2(BW-1-3-EB-3), L4599-3(BW-1-3-60-61.7), L4599-4(BW-1-3-66.7-68.3),
Qty
3
2
2
2
2
2
1
Matrix
Soil
Soil
Soii
Soil
Soil
Water
Water
Anaiysis
8260
METALS -ATK SOIL
NITRATE 9056 (IC)
NITRITE 9056 (IC)
PH 9045
8260IX
MET-ATK 3010
Description
Volatile Organics
ATK Soil testing metals
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Volatile Organics Appendix 9
METALS FOR H20 (ATK SOILS)
5 Samples: 14 Analyses;
Unit Price Total Price
175.00
0.00
25.00
25.00
15.00
175.00
0.00
Total Amount Due:
$525.00
$0.00
$50.00
$50.00
$30.00
$350.00
$0.00
$1,005.00
Thank vou for vour business
Page 1 of 1
y
•/
/ SCIENCE AND ENGINEERING THtOKCOL
Control of Environmental Samples
Document No. [
SOP-102 1
Effective Date
14 July 98
Issue
5
Page
3 of 4
Sample Receipt Checlclist
LWR/PO No: /. ^S^ ^
Receipt Date: ^ ' OCT - Of
Received by: /^(/O B
LabID: /. ^jT^^
Samples for Compliance Testing
Chain of Custody (COC)
If No, was a COC initiated at receipt?
Custody Seal on Shipping Container
Custody Seals on Sample Containers
Samples Accompanied by Airbill or Bill of Laden
Samples Properly Labeled
.•:^ W-^v;^^tesi^^-^-l^^
/
y^
K
'fii;>':;teN6"^^r-:- • ;
>^ X 1
X
If No, explain:
Are sample quantities adequate for required testing? X
If No, explain: |
Are samples in appropriate containers? )\
If No, explain:
Are samples within holding times? X
If No, explain:
Are all sample containers assigned unique laboratory numbers? v/i
If no, assign unique numbers j
Temperature of sample at time of receipt: il-cce^/'y-ee^ /V/ ccrz?/<^ i^/,ic . 7>*-5^' '^tt
pH Log 1
SamplelD:
Inttial pH:
Final pH:
2
< Z-
ATK
ALLIANT TECHSYSTEMS
LWR-FY01 -D1609
5 November 2001
TO:
CC:
FROM:
LWR:
WO:
J. Hermance
F. E. Bares and L. Lofgren
L. V. Dearden
L4599 and L4631
M1101
Thiokol Propulsion
P.O. Box 707
Brigham City, Utah 84302-0707 USA
Tel: [phone]
Fax: [phone]
SUBJECT: Soil Moisture
Results for the soil moisture content are given below in tabular form. Samples were tested using the
ASTM Method: D2216-98 - Standard Test Method for Laboratory Determination of Water(Moisture)
Content of Soil and Rock by Mass.
Sample
Percent
Moisture
L4599-1
L4599-3
L4631-1
L4631-
L4631-
L4631-
L4631-
L4631-
L4631-8
L4631-9
-2
-4
-5
-6
-7
11.4
11.6
12.0
11.9
12.2
12.9
11.8
12.1
11.9
11.8
If you have any questions feel free to contact us at ext. 2744.
M. T. Burnett
L. V. Dearden
Chemical and Physical Analysis
L4584
VOLATILE ORGANICS
DATA PACKAGE REFERANCE
Sample Login No. L^S^Y
Date Run ^ Sf/ 'U^i Work Group JUJ^ 7S^ I
The data pack is filed with sample number LHS^f%
Login Number
EPA Method
SOP Number
Work Group Number
Arsenic QC Data Package Checklist
L4584
7060
A complete descnption of samrM -i x ., ^ .• • , ^ • x.. ..o. _• ^ Dr-,r,oK.,+ „ 1 ^o," .,„rj 'T.; ^Pl© and stanOards preparation is located in the "Standards Preparation Log and Digestion Loa"
Standard Soluiton; Standard Concentration
Standard i
Standard 2
Standard 3
Standard 4
5 ppb
25 ppb
50 ppb
100 pbb
QC Concentration (ppb)
LFB
ICV
QCS
CCV
50.0
50.0
20.0
50.0
Spike Preparation: The preparation of matrix spikes and matrix spike duplicates
is described in the "Digestion Log". Spike Concentration
after final dilution is typically 25 ppb.
Analyst:
Peer review:
Comments:
All QC acceptable
Package Includes:
Date: .A/''
Date: ^<^^'^/o(
Autosampler Table L4560
QC Report 2<
Work Group Report _X
Data Review X
Data package Raw data stored with Login Number L4560
includes data from Login Number(s)
Login Number_
EPA Method _
SOP Number^
Work Group Number
Mercury QC Data Package Checklist
L4584
7470A
316
WG7601
A complete discription of QC, sample and standards preparation is located in the "Mercury
Analysis Log Book".
Standard Concentration QC Concentration
Standard 1
Standard 2
Standard 3
Standard 4
Standard 5
1 ppb
2 ppb
5 ppb
10 ppb
20 ppb
LFB
ICV
QCS
CCV
4 ppb
5 ppb
10.0 ppb
5 ppb
Spike Preparation: The preparation of matnx spikes and matrix spike duplicates is described
in the "Mercury Analysis Log Book". Spike concentration after final
dilution is vsu6lly 4 ppb Hg.
Analyst:
Peer review:
Comments:
All QC acceptable.
lilution IS usj^lly 4 ppb I
Date:
Date:
/^//»/t/
Z"^. yr^Af
Package Includes: Autosampler Table L4602
QC Report 2<
Work Group Report 2<
Data Sheet X
Sample Prep Sheet L4602
Raw data stored with Login Number
Data package includes data from Login Number(s)
L4602
Login Number
EPA Method _
SOP Number^
Work Group Number
Arsenic QC Data Package Checklist
L4584
7060
311
WG7542
A complete description of sample and standards preparation is located in the "Standards
Preparation Log" and "Digestion Log"
Standard Soluiton: Standard Concentration QC Concentration (ppb)
Standard 1
Standard 2
Standard 3
Standard 4
5 ppb
25 ppb
50 ppb
100 pbb
LFB
ic_y
QCS
ccy^J
50.0
50.0
20.0
50.0
Spike Preparation: The preparation of matrix spikes and matrix spike duplicates
is described in the "Digestion Log". Spike Concentration
after final dilution is typically 25 ppb.
Analyst:
Peer review:
Comments:
All QC acceptable
Package Includes: Autosampler Table L4530
QC Report _X
Work Group Report 2<
Data Review X
Raw data stored with Login Number L4530.
Data package includes data from Login Number(s) ._
/ y
Login Number
EPA Method _
SOP Number'
Work Group Number
Mercury QC Data Package Checklist
L4584
7471A
316
WG7559
A complete discription of QC, sample and standards preparation is located in the "Mercury
Analysis Log Book".
Standard Concentration QC Concentration
LFB
ICV
QCS
CCV
Spike Preparation: The preparation of matrix spikes and matrix spike duplicates is described
in the "Mercury Analysis Log Book". Spike concentration after final
dilution is usually 4 ppb Hg.
Standard 1
Standard 2
Standard 3
Standard 4
Standard 5
1 ppb
2 ppb
5 ppb
10 ppb
20 ppb
4 ppb
5 ppb
10.0
5 ppb
Analyst:
Peer review:
Comments:
All QC acceptable.
t^ Date:
Date:
^"M
/o/rTAr
Package Includes: Autosampler Table L4530
QC Reportjc
Work Group Report _)<
Data Sheet x
Sample Prep Sheet L4530
Raw data stored with Login Number L4530
Data package includes data from Login Number(s)
EPA SW-846 6010 QC Data Package Checklist
" Login Number_
EPA Method _
lA/ork Group Number_
Run Number _
Standard Solution:
fvlSTDl
MSTD2
MSTD3
MSTD4
MSTD5
Cal Blank
L4584
6010
WG7527
R30741
Log Identification
9/25/2001
9/24/2001
9/25/2001
9/24/2001
9/25/2001
NA
QC Solutions: Log Identification
LPC
QC-21
QC-7
QC-7 IOX
QC-Sn
QC-P
9/25/2001
9/25/2001
8/30/2001
9/20/2001
7/10/2001
8/21/2001
Analyst:
Peer review by:
SIC
LFB
Matrix Spike
QC Samples:
Date:
Date:
9/19 & 9/25/2001
2.0 mL of LFS 9/13/01
4.0 mL of LFS 9/13/01
L4530-2, L4560-9,
&L4584-10
/^/z^/
/o/i/^/
Comments: ^
t ^ AXi)t^fiiit4a
^ g»xt.«»w«y S' /,</ S^^
Dilutions: 100 mL Vol. Rasks
Package Includes: Autosampler Table
QC Report
Work Group Report
Bench Sheet
Data Review
NA^
T^
Raw data stored with Login Number L4530
Data package includes data for Login Number(s) L4530, L4560, & L4584
Volatile Organics Data Package CheckJist
Ssmple Logfn No: L "i^^
Work Group:_lAiik2^itL
Date Run: Ol QrT?^!
Method: )?'?<> V
Matrix: 'jQil
Instnjment ID: '^.f^fyi.
VJ(r 7^^i^ Initial Calibration Loeatien:
Run Log
EFs Tune Report
Continuing Calibraticn: Quant Report/Ci'.romatccram
Continuing Calibraticn Check Report
Reagent Elanlc Guant Rspoa/Chrcmatcgram '
Samples:Quant Repcr/Chromatccram
Samples: TIC Daia
Matrix Spike; Quant Rspon/Chrcmaiccra.m
Matrix Spike Duplicate: Cuant Reporj'Chrcmatccrcrr;
Inte.Tiai Standard Area .Report
Surrccate i Spike/'Cupiicate Recover/ .Rsccrt
Frep/Exracticn Leg
Preser^/aticn C^S:Ck
Peer Review
File Name | Initial | ijiwmm m c^ii
cn n^f<o(-z\
U'O'JSy/-'/ 1
/•J'/
7..S/
(S^
iiBMaahb is^/
XiOhl'^l z,\ LW
See Run Leg I (^y'
(Xi^
(OGIS^/-^ I /X'V'
ueE.
Nitrate-N QC Data Packc
Login Number L4584
EPA Method 9056.0
SOP Number 341
Work Group Number WG7534
Standard Solution: Log Identification
Autocall R
Autocal2R
Autocal3R
AutocaWR
Autocal5R
QC Solutions:
ICV
QCS
CCV
Spike Stock Sol.
Spike
Spike Preparation:
Matrix Spike
Matrix Spike Dup.
Analyst: ,^^^
Peer review: /{^u<^
Comments:
All QC acceptable.
CWS-86-489
CWS-86-488
CWS-86-487
CWS-86-486
CWS-86-485
Log Identification
CWS-86-488
Dionex Ref./10
CWS-86-486
CWS-40-173
mL of Sample
5.00
5.00
ige Checklist
Date:
Date:
Concentration (ppm)
Nitrate-N
0.5
2
5
10
20
Concetration (ppm)
Nitrate-N
2
2.26
10
2000
4
uL of Stock
Nitrate-N
10
10
Package Includes:
RE
Data package inc
Autosampler Table
QC Report
Work Group Report
Bench Sheet
Data Review
iw data stored with Loc
•ludes data from Login
X
X
X
X
X
in
Nu
Number
mber(s)
Work Group Summary Report
Quality Control Data
''^-^alysis: PH 9045 Method: SW 846, 9045
Report Date: 26-SEP-Ol 'WG7528
Summaxy of QC Samples
Sample QC
Ntimber Type Description
WG7528-1 QCS Independent Check Standard
QC Measured Values with Limits
%Recov Limits
100.1 80-120
Summary of Spiked Sasrples
Sample QC Reference Sampl«
Type Number Number
WG7528-2 DUP L4584-12 8.699
Samples In Workgroup
L4584-2 L4584-3
L4584-8 L4584-9
Spiked Measured Values with Limits
8.709
L4584-4
L4584-10
RPD Limits
0.11 0-20
L4584-5
L4584-12
L4584-7
Analyst: '<^.fM^
Peer Review: i/^'^'^^'Y^
Date ^ 2StP ^
Date 2.^S<'y^ ^/
'4
CERTIFICATE OF ANALYSIS
Listing of sample Information and Testing Requested
Friday, December 7, 2001
TESTED FOR ATK Thiokol: Bacchus
Environmental Compliance M/S M7H7
P. O. Box 98
Magna, UT 84044-0098
Jon Hermance
Project: Lab Anal - Rem - Soil
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, LIT 84302-0707
801-863-3732
800-863-8080
Login Nunnber L4584
Lab No Client Number
Test Requested
Received
Description
CollectDate/Time
Matrix
1 L4584-1 BW-1-2-45-46.7
SW-846, 8260
1 L4584-2 BW-1-2-FD-1
Volatile Organics
09/25/01
09/25/01
09/17/01 10:30 1
Soil
09/17/01 11:45 1
SW
SW.
SW
SW-
SW
SW
SW
SW-
SW-
SW-
SW-
SW-
sw
SW
SW
-846, 8260
846, 7471A
-846, 7060
846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
•846, 6010
•846, 3050
846, 9056
846, 9056
846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L4584-3 BW-1-2-50-51.7 09/25/01 09/17/01 12:15
SW-
SW
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW
sw
SW
846, 8260
-846, 7471A
-846, 7060
•846, 6010
•846, 6010
•846,6010
-846, 6010
-846, 6010
846, 6010
846, 6010
-846, 6010
-846, 3050
846, 9056
846, 9056
846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Page 1 of 29
4 L4584-4 BW-1-2-60-61.7 09/25/01 09/17/01 16:20
SW
SW
SW
SW
SW
SW
SW
3W
SW-
SW
SW-
SW-
SW
SW
SW
846, 8260
846, 7471A
-846, 7060
-846, 6010
846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
•846, 6010
•846, 3050
846, 9056
846, 9056
846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Ba ICP Metals /^alysis (RCRA)
ICP/GF/VA Metals Digestion
Nitrate Analysis by IC
Nitrite Anaiysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L4584-5 BW-1-2-70-71.7 09/25/01 09/18/01 11:40
SW^
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
sw
sw
sw
'846, 8260
•846, 7471A
•846, 7060
•846, 6010
•846, 6010
•846, 6010
•846, 6010
•846, 6010
•846, 6010
•846, 6010
•846,6010
•846, 3050
846, 9056
846, 9056
846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GF/\A Arsenic Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
ICP Metals /Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Ag
Be
Cd
Ba
Al
Pb
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soii
Soil
Soil
Soil
Soil
Soil
L4584-6 BW-1-2-EB-2 09/25/01 09/18/01 14:00
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
846, 8260
846, 7470A
846, 7060
846, 6010
846, 6010
846, 6010
846, 6010
846, 6010
846, 6010
846, 6010
846, 6010
846, 3010
Volatile Organics Appendix 9
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Pb ICP Metals /Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
ICP Metals Digestion
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
L45B4-7 BW-1-3-0-1.7 09/25/01 09/20/01 10:30
SW
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-sw sw
sw
-846, 8260
-846, 7471A
-846, 7060
-846, 6010
-846,6010
-846,6010
-846, 6010
-846, 6010
-846, 6010
-846,6010
•846, 6010
•846, 3050
846, 9056
846, 9056
846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Al ICP Metals /^alysis (RCRA)
Be ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Page 2 of 29
I L4584-8 BW-1-3-10-11.7 09/25/01 09/20/01 11:50
SW
SW^
SW^
SW^
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW
SW
SW
846, 8260
-846, 7471A
-846, 7060
-846, 6010
-846, 6010
-846,6010
-846,6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
•846, 3050
846, 9056
846, 9056
846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH ElectrcxJe Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soii
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L4584-9 BW-1-3-20-21.7 09/25/01 09/20/01 15:10
SW
SW-
SW
SW
SW
SW
SW
SW-
SW
SW-
SW-
SW-
SW
SW
SW
846, 8260
846, 7471A
846, 7060
-846,6010
-846,6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 3050
846, 9056
846, 9056
846, 9045
I L4584-10 BW-1-3-30-31.7
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/25/01 09/21/01 09:40
SW-846, 8260
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
IL4584-11 BW-1-3-31.7-33
SW-846, 8260
IL4584-12 BW-1-3-40-41.7
Volatile Organics
09/25/01
09/25/01
09/21/01 10:40
Soil
09/21/01 12:15
SW-846, 8260
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GF/VA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals /^alysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soii
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Page 3 of 29
L4584-13 BW-1-2-TB-3 09/25/01 09/17/01 09:00
SW-846, 8260 Volatile Organics Appendix 9 Water
Comments:
L4584 Method 6010 Metals: A slight negative matrix interference was obsen/ed for Ba, Cd, Cr, Pb and Se
for one of the samples in this set.
Certified By Qa>*i^ K ^^^TO'^^^-. 7-C^^Z^Z<^ {
QC Coordinator'[J Date
This certifies that the following samples were analyzed using good laboratory practices to show the following results:
Page 4of29
Listing of Results by Sample
1 sample ID: BW-i -2-45-46.7
CAS
Number
630-20-6
71 -55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-t
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-67-6
108-10-1
67-64-1
107-02-8
107-13-1
71JI3-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
lest Psramster
1,1,1,2-1 bTR ACHLOROETH ANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-THICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRlCHLOROBEN2ENE
1.2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBEN2ENE
1,3-DICHLOHOPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-lSOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON IbTRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOBOETHENE
10061-01-5 CIS-1,3-DlCHLOBOPROPENE
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
9B-B2-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPHOPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRI CHLOROFLUOROMETH ANE
VINYL ACETATE
VINYL CHLORIDE
Result
U
U
u u u u u u u u u u
u u u
u u u u u u
u u u u u
u u 13 ft,
u u u u
u u u u u u u u
u u u u u
u u
u u u u u u u u u u
u u u u u
u u u u u u
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ugAig
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Lab ID: L4584-1 Collect Date: 09/17/01 10:30 |
WPL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
Dil.
EOL Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50 •
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10 1
10
10
10
10
10
10 •
10 1
10 1
10 1
10 •>
10 -
10 1
10 1
10 1
10
10 1
10 1
10 1
10 1
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46.8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
I SW-846,8260
1 SW-846,8260
1 SW-846,8260
I SW-846,8260
1 SW-B46,8260
I SW-846,8260
1 SW-846,8260
1 SW-846,8260
I SW-846,8260
1 SW-846, 8260
I SW-B46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,6260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-»46,8260
1 SW-846,8260
I SW-846,8260
I SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
! SW-846,8260
SW-846, 8260
SW-B46, 8260
1 SW-846,8260
1 SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
Test Daje
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15.24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01'01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15.24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15.24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
10/01/01 15:24
Page 5 of 29
1 Sample ID: BW-1-2-FD-1
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-O2-8
107-13-1
71-43-2
10B-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75O0-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
last P^rsrppter
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2.3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-THIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPHOPANE
1.2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOHOBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PHOPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
rETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
U
U
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u u
u
u
u
u
u
.Units
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
6.11, !f\ug/kg
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u .7
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
1 82
13400
157
.8
.5
12
49
ug'kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Lab ID: L4584-2 Collect Date: 09/17/01 11:45 |
MPL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
14
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.01
.8
13
.05
.1
.1
.3
1.3
Dil.
EQL Factor Method.
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10 1
50
10
10
50
10 1
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
.04 1
2.8 2
6.3 1.2
.3 1.2
.5 1.2
.5 1.2
13 1.2
6.3 1.2
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 6260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
3 SW-846, 7060
13 SW-846, 6010
13 SW-846,6010
13 SW-846,6010
13 SW-e46,6010
13 SW-846, 6010
13 SW-846, 6010
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
Page
Test Date
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10A31/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/01/01 15:57
10/03/01 11:58
09/28/01 13:18
09/27/01 13:25
09/27/01 13:25
09/27/01 13:25
09/27/01 13:25
09/27/01 13:25
09/27/01 13:25
6of29
SELENIUM
SILVER
ICP/GF/WMET/y.S DIGESTION
NITRATE-N
NITRITE-N
PH
U
U
1.7
U
8.416
ug/g
ug/g
mg/l
mg/l
3
.2
.01
.01
15
.8
.05
.05
1.213
1.213
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
CMF
09/27/01 13:25
09/27/01 13:25
09/26/01 12:00
09/27/01 13:27
09/27/01 13:27
09/26/01 12:00
Page 7of 29
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
10S-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
ID: BW-1-2-50-51.7
Test Parameter
1,1,1,2-TETHACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOHOETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBEN2ENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1.2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROaENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
ThIHACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1.3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
u
.8"3-
u u
u u u u u u
u u u
u u u u
u u u u u
u u
u u u u
Units
ug/kg
• ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
7-5TjSu9/kg
u u
u u u
u u u u u
u u u u u
u u u u u u u u
u u u u u
u u u u u
u u u u
u u u u 1.94
15500
161
.8
u 14
2.5
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug'g
Lab ID: L4584-3 Collect Date: 09/17/01 12:15 |
MPL
.6
.6
.9
.8
.4
.5
6
.99
1.3
6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
6
1 4
18
24
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
4
.7
.3
.5
.4
1
.7
1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.01
.9
1.3
.05
.1
.1
.3
1.3
DiL
SQL Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
.04 1
3 2
67 1.2
.3 1.2
.5 1.2
.5 1.2
1.3 1.2
6.7 1.2
1 SW-846.8260
1 SW-846,8260
1 SW-e46,8260
1 SW-846. 8260
1 SW-846, 8260
1 SW-846.8260
1 SW-846.8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-B46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-e46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 7471A
3 SW-846, 7060
14 SW-846,6010
14 SW-846, 6010
14 SW-846, 6010
14 SW-846, 6010
14 SW-846, 6010
14 SW-846, 6010
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
Page
TestDste
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16.31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/01/01 16:31
10/03/01 12:02
09/28/01 13:28
09/27/01 13:28
09/27/01 13:28
09/27/01 13:28
09/27/01 13:28
09/27/01 13:28
09/27/01 13:28
8 of 29
SELENIUM
SILVER
ICP/GF/W METALS DIGESTION
NITRATE-N
NITRITE-N
PH
U
U
1 7
U
8.45
ug/g
ug'g
mg'l
mg/l
3.2
.2
.01
.01
16
.8
.05
.05
1.214
1.214
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
CMF
09/27/01 13:28
09/27/01 13:28
09/26/01 12:00
09/27/01 13:45
09/27/01 13:45
09/26/01 12:00
Page 9 of 29
1 Sample 1
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-e
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
ID: BW-1-2-60-61.7
Test Parameter
1.1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-Tt 1 RACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1.2,4-TRIMETHYLBEN2ENE
1.2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBEN2ENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2.DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-lSOPROPYLTOLUENE
4-METHYL-2-PENTAN0NE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON Tb 1 HACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
10061 -01 -5 CIS-1,3-DlCHLOROPROPENE
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-06-4
75-01-4
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOHOBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
u
u
u
u
u
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.7 •J" ug/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
11 B
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
.8 1
u
u
u
u
1.83
18000
173
.9
.5
19
2
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L4584-4 Collect Date: 09/17/01 16:20 |
MDL
.6
.6
.9
8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.01
.9
1.4
.05
.1
.1
.3
1.4
Dil.
EQL Factor Mjethfiri
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10 1
10
10 1
10
10
10
10
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
.04 1
3 2(
6.8 1.2
.3 1.2,
.5 1.2
.5 1.2
1.4 1.2
6.8 1.2.
1 SW-e46.8260
1 SW-846.8260
1 SW-846.8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846.8260
I SW-846,8260
1 SW-B46,8260
1 SW-846,8260
1 SW-B46,8260
1 SW-846,8260
1 SW-B46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,6260
1 SW-B46,8260
1 SW-B46,8260
1 SW-846,8260
1 SW-B46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
D SW-846,7060
21 SW-846,6010
21 SW-846, 6010
21 SW-846, 6010
21 SW-846,6010
21 SW-846, 6010
21 SW-e46, 6010
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
Test Pate
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
IQ'01/01 17:04
10/01/01 17:04
IO'01/OI 17:04
lO'OI/OI 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
lO'OI/OI 17:04
10/01/01 17:04
10«)1/01 17:04
10/01/01 17:04
10/01/01 17:04
1Qrt)1/01 17:04
10/01/01 17:04
IQ'01/01 17:04
1(V01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
IQ'01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/01/01 17:04
10/03/01 12:07
09/28/01 13:35
09/27/01 13:31
09/27/01 13:31
09/27/01 13:31
09/27/01 13:31
09/27/01 13:31
09/27/01 13:31
Pagel Oof 29
SELENIUM
SILVER
ICP/GF/W METALS DIGESTION
NITRATE-N
NITRITE-N
PH
U
U
1.3
U
8.484
ug/g
ug/g
mg/I
mg/l
3.3
.2
.01
.01
16
.8
.05
.05
1.221
1.221
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-e46, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
CMF
09/27/01 13:31
09/27/01 13:31
09/26/01 12:00
09/27/01 14:02
09/27/01 14:02
09/26rt)1 12:00
Page 11 of 29
Isample ID: BW-1-2-70-71.7
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
641-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-6B-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01 -6
75-69-4
108-05-4
75-01-4
Test Paramctgr
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1.1,2-THICHLOHOETHANE
1.1-DICHLOROETHANE
1.1-DICHLOROETHENE
1.1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPHOPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CAHBON DISULFIDE
CAHBON 1 b 1 HACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPHOPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
u
a.g'X
u
u
u .8
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug'kg
ug'kg
ug/kg
ug'kg
ug'kg
ug/kg
ug/kg
9.7 Tft ug/kg
u •"
u
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
•ST
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
2.506
18200
156
.96
u
20
4.8
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug'kg
ug'kg
ug'kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Lab ID: L4584-5 Collect Date: 09/18/0111:40 |
MPL
.6
.6
9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
4
.7
.3
.5
4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.01
.9
1.4
.06
1
.1
.3
14
Dil.
EQL Factor Meth9<J
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10 1
10 1
10
10 1
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
.04 1
3.1 2
7.1 1.2
.3 1.2
.6 1.2
.6 1.2
1.4 1.2
7.1 1.2
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-B46, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
I SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-646. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
0 SW-846, 7060
53 SW-846, 6010
53 SW-846, 6010
53 SW-846, 6010
53 SW-846,6010
53 SW-846,6010
53 SW-846, 6010
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
lesLPste
10/01/01 17:37
IQ'01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10rt)1/01 17:37
lO'OI/OI 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
IQ'01/01 17:37
10/01/01 17:37
10/01/01 17.37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/01/01 17:37
IQ'01/01 17:37
10/01/01 17:37
10/01/01 17:37
10/03/01 12:17
09/28/01 13:55
09/27/01 13:34
09/27/01 13:34
09/27/01 13:34
09/27/01 13:34
09/27/01 13:34
09/27/01 13:34
Page 12 Of 29
SELENIUM
SILVER
ICP/GF/^A METALS DIGESTION
NITHATE-N
NITRITE-N
PH
5.5
U
.55
U
8.52
ug/g
ug'g
mg/l
mg/l
34
.2
.01
.01
17
.9
.05
.05
1.253
1.253
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
CMF
09/27/01 13:34
09/27/01 13:34
09/26/01 12:00
09/27/01 14:20
09/27/01 14:20
09/26/01 12:00
Page 13 Of 29
Isample ID: BW-1.2-EB-2
CAS
Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
71-36-3
590-20-7
78-93-3
110-75-8
95-49-8
591-78-6
78-83-1
79-46-9
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
107-05-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
126-99-8
156-59-4
10061-01-5
108-94-1
124-48-1
74-95-3
75-71-8
141-78-6
60-29-7
97-63-2
100-41-4
76-13-1
87-68-3
67-63-0
98-82-8
1330-20-7
126-98-7
74-88-4
80-62-6
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
107-12-0
110-86-1
135-98-8
10O-42-5
98-06-6
127-18-4
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1.2-TRICHLOROETHANE
1.1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBEN2ENE
1,2,3-TRICHLOROPROPANE
1,2,4-THICHLOROBEN2ENE
1,2,4-THIMETHYLBENZENE
1,2-DIBHOMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOHOBENZENE
1-BUTANOL
2.2-DICHLOROPROPANE
2-BUTANONE
2-CHLOBOETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
2-METHYL-1-PROPANOL
2-NITROPROPANE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
ALLYL CHLORIDE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CHLOROPRENE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOHOPROPENE
CYCLOHEXANONE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYL ACETATE
ETHYL ETHER
ETHYL METHACRYLATE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYL ALCOHOL
ISOPROPYLBENZENE
M.P-XYLENE
METHACRYLONITRILE
METHYL IODIDE
METHYL METHACRYLATE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
PROPIONITRILE
PYRIDINE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
1 b1RACHLOROETHENE
Result
u
u u
u u
u u u
u u u u u u
u u
u u u u u u u u u u
u u
u u u u u
u u u u u u u u
u u u u 6.6
u u u u u
u u u 5.1,7-
u u u u
u u u u u
u u 57
u
u u u
u u u
u u u
Units
ug/l
ug/l
ug/l
ug/l
ug/(
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/(
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
LablD:L4584-6 Collect Date: 09/18/01 14.00 I
MDL
1
1
1
1
1
1
10
10
1
10
10
10
1
10
1
1
10
10
10
10
18
10
20
.6
10
10
2.1
.9
10
10
10
20
1
1
20
1
10
10
1
1
2
1
1
1
2
1
2
1
10
1
17
1
1
1
1.6
.9
1
1
.5
10
17
10
1
1
1
1
10
10
10
10
1
1
25
10
1
10
1
DIL
EQL Factor Method
5
5
5
5
5
5
10
10
5
10
10
10
5
10
5
5
10
10
10
10
184
10
100
64
10
50
21
9.2
10
10
50
100
5
5
100
5
10
10
5
5
10
5
5
5
10
5
10
5
10
5
173
5
5
5
16
9.1
5
5
5.3
10
174 1
10 1
5 1
5 1
5 1
5 1
10 1
10 1
10 1
10 1
5 1
5 1
249 1
10 1
5 1
10 1
5 1
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846.8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
Analyst
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
lest D^te
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28K)1 19
09/281^01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28«1 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28rt)1 19
09/28/01 19
09/28rt)1 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28rt)1 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
Og/ZBfOI 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28^1 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
09/28/01 19
Page 14 Of 29
18
IB
IB
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
IB
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
18
IB
18
18
18
te
18
18
18
18
IB
18
18
18
18
108-88-3
156-60-5
10061-02-6
110-57-6
79-01-6
75-69-4
108-05-4
75-01-4
TOLUENE
TRANS-1,2-DICHLOROETHENE
THANS-1,3-DICHLOROPROPENE
TRANS-1,4-DICHLORO-2-BUTEN
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ICP METALS DIGESTION
U
u u u u u u u
u u
u u u 8.5
U
U
U
U
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
10
1
1
1
2
.2
1.5
25
1
2
2
6
25
60
3
5
5
5
10
5
5
5
10
.7
43
125
5
10
10
25 -
125
300
15 1
1 SW-846,8260
1 SW-846.8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7470A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3010
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
CWS
CWS
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
09/28/01 19:18
09/28/01 19:18
09/28/01 19:18
09/28/01 19:18
09/28/01 19:18
09/28/01 19:18
09/28/01 19:18
09/28/01 19:18
10/10/01 11:11
10/26/01 14:42
09/28/01 15:11
09/28rtD1 15:11
09/28/01 15:11
09/28/01 15:11
09/28/01 15:11
09/28/01 15:11
09/28/01 15:11
09/28/01 15:11
09/26/01 12:00
Page 15 of 29
I Sampie ID: BW-1-3-0-1.7 Lab ID: L4584-7 Collect Date: 09/20/01 10:30
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
Test Parameter
1,1,1,2-TETRACHLOHOETHANE
1,1,1-TRICHLOROETHANE
1,1,2.2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPHOPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON 1 b rRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
ClS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1.2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
u
u u
u u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u u
u
u u
u
u
25 g,
u u
u u
u
u
u
u
u
u
u u
u
u u
u
u
u
u
u
u
u
u
u
u
u u
u
u u
u
u u
u
u
u
u
u
u
u
.0202
6.92
16100
150
.76
.63
21
12
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
MPL
.6
.6
.9
.8
.4
.5
.6
99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.02
8
1.2
.05
.1
.1
.2
1.2
Dil.
EQL Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10 1
10 1
10
10
10
10
10
10 1
10
10
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
04 1
2.8 2
6.2 1.0
.2 1.0
.5 1.0
.5 1.0
1.2 1.0
6.2 1.0
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46, 8260
1 SW-B46, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-B46, 8260
SW-B46, 8260
SW-B46, 8260
SW-B46, 8260
SW-B46, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
0 SW-846. 7060
65 SW-846,6010
65 SW-846, 6010
65 SW-846, 6010
65 SW-846, 6010
65 SW-846, 6010
65 SW-846, 6010
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
Ifi.st Date
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 1B:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18-11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/01/01 18:11
10/03/01 12:23
09/28/01 14:05
09/27/01 13:37
09/27/01 13:37
09/27/01 13:37
09/27/01 13:37
09/27/01 13:37
09/27/01 13:37
PagelSof 29
SFI FNIUM
SILVER
ICP/GFAA METALS DIGESTION
NITRATE-N
NITRITE-N
PH
U
U
3.7
.11
8.296
ug/g
ug'g
mg/l
mg/l
3
.1
.01
.01
15
.7
.05
.05
1.065
1.065
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846. 9045
MTB
MTB
MTB
CWS
CWS
CMF
09/27/01 13:37
09/27/01 13:37
09/26/01 12:00
09/27/01 14:37
09/27/01 14:37
09/26/01 12:00
Page 17 of 29
{sample ID: BW-1-3-10-11.7
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91 -20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
Test Parameter
1,1,1,2-TETRACHLOHOETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPHOPEN E
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-THICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPHOPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
U
u
u
u
u
u u u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
11 B. u^
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u u
u u
u
u u
u
u
u 2.31
7120
68
.33
.73
11
5.8
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug'kg
ug/kg
ug'kg
ug'kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug'kg
ug/kg
ug'kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ugrtcg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Lab ID: L4584-8 Collect Date: 09/20/01 11:50 |
MDL
.6
.6
9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.01
.9
1.2
.05
.1
.1
.2
1.2
Oil.
ggL Factor Method.
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
.04 1
3.2 2
6.1 1.0
.2 1.0
.5 1.0
.5 1.0
1.2 1.0
6.1 1.0
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846.8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-S46,8260
SW-846, 8260
I SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46. 8260
SW-B46, 7471A
0 SW-846, 7060
49 SW-846, 6010
49 SW-846, 6010
49 SW-846, 6010
49 SW-846, 6010
49 SW-846, 6010
49 SW-846,6010
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
lest P9te
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 1844
10/01/01 18:44
10/01/01 18 44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18.44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 1844
10/01/01 18:44
10/01/01 18 44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10A31/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/01/01 18:44
10/03/01 12:31
09/28/01 14:12
09/27/01 13:40
09/27/01 13:40
09/27/01 13:40
09/27/01 13:40
09/27/01 13:40
09/27/01 13:40
Page 18 of 29
3
U ug/g
PH "•'' 'S/g ^f ,5 ^.9
~ ^"' "•' if I gs
•'«-«.9a<s Civs MS"«7
IsamplelD: BW-1-3-20-21.7
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
Ifist Parameter
1,1,1.2-TETRACHLOROETHANE
1.1,1-TRlCHLOROETHANE
1,1,2,2.TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOHOPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DieROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DlCHLOHOBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1.3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2.2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOHOTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPHOPYLTOLUENE
4-METHYL-2-PENT ANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARSON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOHOBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIOE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
u
u
u
u
u
u
u
u
u
u u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
5-9;i,&ug/kg
u
u
u
u
u
u
u u
u
u
u
u
u
u
u u
u
u u
u
u
u
u
u
u
u
u
u u
u
u u
u
u
u
u
u
u
u
u u
3.7
6730
98
.3
U
16
7.9
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug'g
Lab ID: L4584-9 Collect Date: 09/20/01 15:10 |
MPL
6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
4
.5
6
.5
.3
.5
.01
.98
1.3
.05
.1
.1
.3
1.3
Dll.
5QL Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10 1
10
10
10
10
10 1
10 1
10 1
10
10 1
10 1
10
10 1
10 1
10 1
10 1
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
.04 1
3.3 2
6.5 1.0
.3 1.0
.5 1.0
.5 1.0
1.3 1.0
6.5 1.0
1 SW-846,8260
1 SW-846.8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
I SW-846,8260
SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
I SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, B260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 7471A
0 SW-846, 7060
57 SW-846, 6010
57 SW-846, 6010
57 SW-846,6010
57 SW-846, 6010
57 SW-846, 6010
57 SW-846, 6010
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
Testpste
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15.49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
IO'02/OI 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10rt)2/01 15:49
10/02/01 15:49
10/02/01 15:49
10rt32A)1 15:49
10/02/01 15:49
10/02/01 15:49
10rt)2/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02AD1 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/02/01 15:49
10/03/01 12:36
09/28/01 14:19
09/27/01 13:43
09/27/01 13:43
09/27/01 13:43
09/27/01 13:43
09/27/01 13:43
09/27/01 13:43
Page 20 Of 29
UTB 09/27/01 13:43
.fi 1057 SW-846,6010 ^J|» 09/27/0113:43
,, uo/Q 31 'I QS SW-e46,6010 W™ /Q^ ^2:00
fS"--^*''™ - S S S ; |K:S CM. «««"-
NlTRATE-N U
NlTRlTE-N 8,776
PH
page 21 Of 29
IsamplelD: BW-1-3-30-31.7
630-20-6
71 -55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-67-3
156-59^
10061-01-£
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
Test Psrsmeter
1,1,1,2-TETHACHLOROETHANE
1.1,1 -TRICHLOROETHANE
1,1,2,2-TETHACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1.2,4-TRICHLOHOBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOHOPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPHOPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOHOETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CAHBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHHOMIUM
LEAD
Result
U
u u
u u
u u u u u
u u u u
u u u
u u
u u
u u u u u
u u
12 g
u u
u u u u u
u u u u u
u u u
u u u u u
u u u
u u
u u u
u u
u u u u u u
u u u
u u 1 46
10900
86
.52
.15
15
11
units
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug'g
LablD:L4584-10 Collect Date: 09/21/01 09:40 j
MDL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
24
11
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.01
7
11
.04
09
.09
.2
1.1
Dil.
EQL Factor Mfittlfid
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
.04 1
24 2
5.5 1.2
.2 1.2
.4 1.2
.4 1.2
1.1 1.2
5.5 1.2
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
3 SW-846, 7060
18 SW-846, 6010
18 SW-846. 6010
18 SW-846, 6010
18 SW-846, 6010
18 SW-846, 6010
18 SW-846, 6010
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
Test Date
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16.22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
IO'02/OI 16:22
10/02A)1 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
1Q/02AD1 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10'02A)1 16:22
10/02/01 16:22
10/02/01 16:22
10/D2AD1 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/02/01 16:22
10/03/01 12 45
09/28/01 14:29
09/27/01 14:00
09/27/01 14:00
09/27/01 14:00
09/27/01 14:00
09/27/01 14:00
09/27/01 14:00
Page 22 of 29
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NITRATE-N
NITRITE-N
PH
3.6
U
1.5
U
8.678
ug/g
ug/g
mg/l
mg/l
2.6
.1
.01
.01
13
.7
.05
.05
1.218
1.218
1
1
1
1
SW-B46, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
CMF
09/27/01 14:00
09/27/01 14:00
09/26/01 12:00
09/27/01 16:37
09/27/01 16:37
09/26/01 12:00
Page 23 of 29
• h
IsamplelD: BW-1-3-31.7-33 LablD:L4584-11 Collect Date: 09/21/01 10:40
CAS
Number Test Parameter
630-20-6 1,1,1,2-TETHACHLOHOETH ANE
71-55-6 1,1,1-TRICHLOROETHANE
79-34-5 1,1,2,2-TETRACHLOROETHANE
79-00-5 1,1,2-THICHLOHOETHANE
75-34-3 1.1 -DICHLOROETHANE
75-35-4 1,1-DICHLOROETHENE
563-58-6 1,1-DICHLOROPROPENE
87-61-6 1,2,3-TRICHLOROBENZENE
96-18-4 1,2,3-TRICHLOROPROPANE
120-82-1 1,2,4-TRICHLOROBENZENE
95-63-6 1,2,4-TRIMETHYLBENZENE
96-12-8 1,2-DIBROMO-3-CHLOROPROPANE
106-93-4 1,2-DIBROMOETHANE
95-50-1 1.2-DICHLOROBENZENE
107-06-2 1,2-DICHLOROETHANE
78-87-5 1,2-DlCHLOHOPROPANE
106-67-8 1,3,5-TRIMETHYLBENZENE
541 -73-1 1,3-DICHLOROBENZENE
142-28-9 1,3-DICHLOROPROPANE
106-46-7 1,4-DICHLOROBENZENE
590-20-7 2,2-DICHLOROPROPANE
78-93-3 2-BUTANONE
110-57-8 2-CHLOROETHYLVINYL ETHER
95-49-8 2-CHLOROTOLUENE
591-78-6 2-HEXANONE
106-43-4 4-CHLOROTOLUENE
99-87-6 4-ISOPROPYLTOLUENE
108-10-1 4-METHYL-2-PENTANONE
67-64-1 ACETONE
107-02-8 ACROLEIN
107-13-1 ACRYLONITRILE
71-43-2 BENZENE
108-86-1 BROMOBENZENE
74-97-5 BROMOCHLOROMETHANE
75-27-4 BROMODICHLOROMETHANE
75-25-2 BROMOFORM
74-83-9 BROMOMETHANE
75-15-0 CARBON DISULFIDE
56-23-5 CARBON TETRACHLORIDE
108-90-7 CHLOROBENZENE
75-00-3 CHLOROETHANE
67-66-3 CHLOROFORM
74-87-3 CHLOROMETHANE
156-59-4 CIS-1,2-DICHLOROETHENE
10061 -01 -5 CIS-1,3-DICHLOROPROPENE
124-48-1 DIBROMOCHLOROMETHANE
74-95-3 DIBROMOMETHANE
75-71-8 DICHLORODIFLUOROMETHANE
100-41-4 ETHYLBENZENE
76-13-1 FREON 113
87-68-3 HEXACHLOROBUTADIENE
98-82-8 ISOPROPYLBENZENE
1330-20-7 M,P-XYLENE
75-09-2 METHYLENE CHLORIDE
104-51-8 N-BUTYLBENZENE
103-65-1 N-PROPYLBENZENE
91-20-3 NAPHTHALENE
1330-20-7 O-XYLENE
135-98-8 SEC-BUTYLBENZENE
100-42-5 STYRENE
98-06-6 TERT-BUTYLBENZENE
127-18-4 TETRACHLOROETHENE
108-88-3 TOLUENE
156-60-5 THANS-1,2-DICHLOROETHENE
10061 -02-6 TRANS-1,3-DICHLOROPROPENE
79-01-6 TRICHLOROETHENE
75-69-4 TRICHLOROFLUOROMETHANE
108-05-4 VINYL ACETATE
75-01-4 VINYL CHLORIDE
Result
U
Units
ug/kg
1.7-X ug/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
14^
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugrtcg
ug'kg
ug'kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
MPL
.6
6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
24
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
DiL
EQL Factor Methgtf.
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46,8260
1 SW-B46,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
Analvst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
Test Pate
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02'DI 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
1Q/02A31 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02^1 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02AD1 16:55
10/02/01 16:55
10/02/01 16:55
IO'02/OI 16:55
10/02/01 16:55
IO/02'OI 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02A)1 16:55
10/02A31 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
10/02/01 16:55
Page 24 Of 29
« •*
1 Sample ID: BW-1 -3-40-41.7
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-O6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
7B-93-3
110-57-8
95-49-6
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-;
124^8-1
74-95-3
75-71-8
10O-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
96-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
Isst Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOHOETHANE
1,1,2-TRICHLOHOETHANE
1.1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOHOBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBHOMOETHANE
1,2-DICHLOROBEN2ENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBEN2ENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBEN2ENE
2,2-DICHLOROPROPANE
2-BLrrANONE
2-CHLOHOETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
ClS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u u
u
19^
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
.0266
2.54
12200
155
.48
.42
16
3.6
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug'kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L4584-12 Collect Date: 09/21/01 12:15 |
MDL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
14
1.8
2.4
1.1
.5
.6
.5
.6
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.01
.9
1.2
05
.1
.1
.2
1.2
Dil.
EQL Factor Methotj
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10
10
.04
3 2
6.1 1.1
.2 1.1
.5 1.1
.5 1.1
1.2 1.1
6.1 1.1
1 SW-846,8260
1 SW-B46,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,6260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW.846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 6260
1 SW-B46, 8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 6260
t SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-845, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 6260
SW-846, 7471A
0 SW-846, 7060
06 SW-846,6010
06 SW-846,6010
06 SW-846,6010
06 SW-846, 6010
06 SW-846,6010
06 SW-846,6010
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
lest P9te
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
ID'02'01 17:29
1OA32/01 17:29
10/02/01 17:29
10102/01 17.29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02«1 17:29
10/02/01 17:29
10rt52AD1 17:29
10/02^)1 17:29
10/02/01 17.29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10A52A31 17:29
10/02/01 17:29
10/02/01 17:29
10/02^1 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10102101 17:29
10/02/01 17:29
10I02J01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10m2/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10A)2/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/02/01 17:29
10/03/01 12:52
09/28/01 15:06
09/27/01 14:09
09/27/01 14:09
09/27/01 14:09
09/27/01 14:09
09/27/01 14:09
09/27/01 14:09
Page 25 Of 29
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NITRATE-N
NITRITE-N
PH
U
U
.67
U
8.699
ug'g
ug'g
mg'l
mg/l
2.9
.1
.01
.01
15
.7
.05
.05
1.106
1.106
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
CMF
09/27/01 1409
09/27/01 14:09
09/26/01 12:00
09/27/01 16:55
09/27/01 16:55
09/26/01 12:00
Page 26 Of 29
i Sample
CAS
Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
71-36-3
590-20-7
78-93-3
110-75-8
95-49-8
591-78-6
78-83-1
79-46-9
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
107-05-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
126-99-8
156-59-4
10061-01-E
108-94-1
124-48-1
74-95-3
75-71-8
141-78-6
60-29-7
97-63-2
100-41-4
76-13-1
87-6B-3
67-63-0
98-82-8
1330-20-7
126-98-7
74-88-4
80-62-6
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
107-12-0
110-86-1
135-98-8
100-42-5
98-06-6
127-16-4
D: BW-1-2-TB-3
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOHOETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPHOPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOHOETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOHOBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
1-BUTANOL
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
2-METHYL-1 -PROPANOL
2-NlTROPROPANE
4-CHLOHOTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
ALLYL CHLORIDE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CHLOROPRENE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
CYCLOHEXANONE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYL ACETATE
ETHYL ETHEH
ETHYL METHACRYLATE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYL ALCOHOL
ISOPROPYLBENZENE
M,P-XYLENE
METHACRYLONITRILE
METHYL IODIDE
METHYL METHACRYLATE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
PROPIONITRILE
PYRIDINE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
Result
u
u
u
u
u u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
1.37-
u ^ u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u u
u
10
u
u
u
u
u
u
u
u
u
u
Units
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
ug/l
ug/l
ug/l
ug/l
LablD:L4584-13 Collect Date: 09/17/01 09:00 |
MOL
1
1
1
1
1
1
10
10
1
10
10
10
1
10
1
1
10
10
10
10
18
10
20
.6
10
10
2.1
.9
10
10
10
20
1
1
20
1
10
10
1
1
2
1
1
1
2
1
2
1
10
1
17
1
1
1
1.6
.9
1
1
.5
10
17
10
1
1
1
1
10
10
10
10
1
1
25
10
1
10
1
Dil.
EQL Factor Methoci •
5
5
5
5
5
5
10
10
5
10
10
10
5
10
5
5
10
10
10
10
184
10
100
64
10
50
21
9.2
10
10
50
100
5
5
100
5
10
10
5
5
10
5
5
5
10
5
10
5
10
5 1
173
5 '
5
5
16 1
9.1 1
5 1
5 1
5.3 1
10 1
174 1
10 1
5 1
5 1
5 1
5 1
10 1
10 1
10 1
10 1
5 1
5 1
249 1
10 1
5 1
10 1
5 1
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846. 8260
1 SW-846,8260
1 SW-B46.8260
1 SW-846,8260
1 SW-846,8260
1 SW-646,8260
1 SW-846,8260
1 SW-846.8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-646,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-e46, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 6260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 6260
SW-846, 8260
SW-846, 8260
SW-846, 6260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-a46, 8260
Analyst
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
IfiSt Date
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28AD1 19:50
09/26/01 19:50
09/28/01 19:50
09/2a'01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/26/01 19:50
09/26/01 19:50
09/28rtl1 19:50
09/28A)1 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/26/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28rt31 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28^)1 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/26/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
Page 27 Of 29
« >-
108-88-3 TOLUENE
156-60-5 TRANS-1,2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
110-57-6 TRANS-1,4-DICHLOHO-2-BUTEN
79-01-6 TRICHLOROETHENE
75-69-4 TRICHLOROFLUOROMETHANE
108-05-4 VINYL ACETATE
75-01-4 VINYL CHLORIDE
u
u
u u
u u
u u
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
0
1
1
1
2
5
5
5
10
5
5
5
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
09/28/01 19:50
Page 28 Of 29
•«•- •«
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected but was
below the MDL.
B Gas Chromatography and Mass Spectral Data Flag. This flag is used when an analyte is found in
the blank as well as the sample
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This flag is used
either when estimating a concentration for tentatively identified compounds or when the data
indicated the presence of a compound that meets the identification critena but the result is less than
the EQL (e.g. 3 J with an EQL of 10)
MDL Method Detection Limit: The minimum concentration of a substance that can be confidently
measured and reported. The laboratory has demonstrated that the MDL can be achieved in a
laboratory reagent blank, but does not guarentee it can be achieved in all sample matrices.
The MDL is approximately three times the signal noise level.
EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many
analytes the EQL is selected as the value of the lowest standard in the calibration curve.
Dil. Factor Dilution Factor: The prepared smple was diluted by this factor because the sample was too
concentrated or due to other interferences in the sample matrix. Any dilution factor causes
an appropriate increase in the MDL and EQL.
Page 29 of 29
/ SCIENCE AND ENGINEERING THMOHSOL
Control ot Environmental Samptes
[Jocumant No.
SOP-102
Eflectiv* Date
14 July 98
Issue
5
Page
3 of 4
LWfVPONo: / ^S ^'Y
Sample Receipt Checklist
ReceiptPate: ZS- ^Cpt. - 200]
Received by: K U<J B
^'P- Lu£'o(/
Samples for Compliance Testing
v^*^-$?fes^^i| ^*o
Chain of Custody (COC) )<
If No, was a COC initiated at receipt?
Custody Seal on Shipping Container X
Custody Seals on Sample Containers X
Samples Accompanied by Aittiiil or Bill of Laden
Samples Properiy Labeled
If No, explain:
Are sample quantities adequate for required testing? X
If No, explain:
Are samples in appropriate containers? K
If No, explain:
Are samples within holding times?
If No, explain:
Are all sample containers assigned unique laboratory numbers? NI\
If no. assign unique numbers
Temperature of sample at time of receipt:
SamptelD:
(IfCe.^ t/^^ /Vi C07> ]^^ uj/ice . T^t*^ '^ Y'C-
pHLog
mitial pH:
Final pH:
ATK
ALLIANT TECHSYSTEMS^
LWR-FY01-D1668
19 November 2001
TO:
CC:
FROM:
LWR:
WO:
J. Hermance
F. E. Bares and L. Lofgren
L. V. Dearden
L4584
M1101
Thiokol Propulsion
P.O. Box 707
Brigham City, Utah 64302-0707 USA
Tel: [phone]
Fax: [phone]
SUBJECT: Soil Moisture Content
Results for the soil moisture content are given below in tabular form. Samples were tested using the
ASTM Method: D2216-98 - Standard Test Method for Laboratory Determination of Water(Moisture)
Content of Soil and Rock by Mass. Testing was performed on September 26, 2001.
Sample
Percent
Moisture
L4$84-2
L4584-3
L4584-4
L4584-5
L4584-7
L4584-8
L4584-9
L4584-10
L4584-12
17.6
17.7
18.1
20.2
6.13
4.62
5.39
17.9
9.62
If you have any questions feel free to contact us at ext. 2744.
M. T. Burnett
L. V. Dearden
Chemical and Physical Analysis
L4560
Volatile Organics Data .^acksge Checklist
Sampie Logfn No:__Lj££fc£_
Work Group: /< nV l^i^
Date Run:?^Sfc^ 2Q<ii
Methcd: ^,7t,Q<^
Matrix: ^ c n.
instrument \D:2L±IL1
Initial Calibraticn Location: ^-V^^o
Run Leg
EFB Tune Repcr
Continuing Calibrsticn: Cuant Repcru'Chromatccrcm
Continuing Caiibraticn Check Report
Resce.nt Elank: Cuant RsporjChrcmatcgram '
Sampies:Guant Repcr/Chromatccram
Samples: TiC Data
Matrix Spike: Cuant .RsccryChrcmatccra.Ti
Matrix Spike Duplicate: Cuant .RecorL/Chrcmaiccram
In-e.Tial Standarc Area Reccr:
Surrccate & Scike/'CuciicaTe Recover/ .Reccr;
rrep/Exiracticn L:c
Fresep/aticn Check
Peer Review
LOvy 79<f'f
fTTO^aay^
^(r'^S/'i'-'T-
See Run Leg
^^^^^i^S
tt'^7<^//-^
Kji. -?c, it,- y
(^
uy
64/
iM
^
/J^
!>/{
L^4
Login Number
EPA Method
SOP Number"
Work Group Number
Arsenic QC Data Package Checklist
L4560
7060
311
WG7675
A complete description of sample and standards preparation is located in the "Standards
Preparation Log" and "Digestion Log"
Standard Soluiton: Standard Concentration QC Concentration (ppb)
Standard 1
Standard 2
Standard 3
Standard 4
5 ppb
25 ppb
50 ppb
100 pbb
LFB
ICV
QCS
CCV
50.0
50.0
20.0
50.0
Spike Preparation: The preparation of matrix spikes and matrix spike duplicates
is described in the "Digestion Log". Spike Concentration
atter final dilution is typically 25 ppb.
Analyst:
Peer review:
Comments:
All QC acceptable
Date: ^^^. ^^>/^^
Date: /* ^r-r/^r
Package Includes: Autosampler Table X_
QC Report 2<_
Work Group Report X
Data Review X
Raw data stored with Login Number
Data package includes data from Login Number(s) L4560
L4584
L4599
L4631
Login Number
EPA Method _
SOP Number"
Work Group Number
Mercury QC Data Package Checklist
L4560
7470A
316
WG7601
A complete discription of QC, sample and standards preparation is located in the "Mercury
Analysis Log Book".
Standard Concentrafion QC Concentration
LFB
ICV
QCS
CCV
Spike Preparation: The preparation of matrix spikes and matrix spike duplicates is described
in the "Mercury Analysis Log Book". Spike concentration after final
dilution is usually 4 ppb Hg.
Standard 1
Standard 2
Standard 3
Standard 4
Standard 5
1 ppb
2 ppb
5 ppb
10 ppb
20 ppb
4 ppb
5 ppb
10.0 ppb
5 ppb
Analyst:
Peer review:
Comments:
All QC acceptable.
Date:
Date: ^/s.^/*/
Package Includes: Autosampler Table L4602
QC Report 2<
Work Group Report _X
Data Sheet X
Sample Prep Sheet L4602
Raw data stored with Login Number _
Data package includes data from Login Number(s)
L4602
Login Number
EPA Method _
SOP Number'
Work Group Number
Arsenic QC Data Package Checklist
L4560
7060
311
WG7542
A complete description of sample and standards preparation is located in the "Standards
Preparation Log" and "Digestion Log"
Standard Soluiton: Standard Concentration
Standard 1
Standard 2
Standard 3
Standard 4
5 ppb
25 ppb
50 ppb
100 pbb
QC Concentration (ppb)
LFB
ICV
QCS
CCV
50.0
50.0
20.0
50.0
Spike Preparation:
Analyst:
Peer review:
Comments:
All QC acceptable
The preparation of matrix spikes and matrix spike duplicates
is described in the "Digestion Log". Spike Concentration
after final dilution is typically 25 ppb.
^^^^ Date: y^^^/of
—* "r-
Date: ^/z.f/*f
Package Includes: Autosampler Table L4530
QC Report 2<
Work Group Report 2<
Data Review X
Raw data stored with Login Number L4530
Data package includes data from Login Number(s)
Login Number
EPA Method
SOP Number'
Work Group Number
Mercury QC Data Package Checklist
L4560
7471A
316
WG7559
A complete discription of QC, sample and standards preparation is located in the "Mercury
Analysis Log Book".
Standard Concentration QC Concentration
Standard 1
Standard 2
Standard 3
Standard 4
Standard 5
1 ppb
2 ppb
5 ppb
10 ppb
20 ppb
4 ppb
5 ppb
10.0
5 ppb
LFB
ICV
QCS
CCV
Spike Preparation: The preparation of matrix spikes and matrix spike duplicates is described
in the "Mercury Analysis Log Book". Spike concentration after final
dilution is usti^lly 4 ppb Hg.
Analyst:
Peer review:
Comments:
All QC acceptable.
Date: /*/ys)
Date: /a /TT/or
Package Includes: Autosampler Table L4530
QC Report_x
Work Group Report _x
Data Sheet x
Sample Prep Sheet L4530
Raw data stored with Login Number L4530
Data package includes data from Login Number(s)
EPA SW-846 6010 QC Data Package Checklist
Login Number
EPA Mettiod
uVork Group Number
Run Number
Standard Solution:
MSTDl
MSTD2
MSTD3
MSTD4
MSTD5
Cal Blank
QC Solutions:
LPC
QC-21
QC-7
QC-7 IOX
QC-Sn
QC-P
Analyst: .
Peer review by:
Comments: ^
oiu /i/ 1
Dilutions:
Package Includes:
Data pac
L4560
6010
WG7524
R30744
Log Identification
9/25/2001
9/24/2001
9/25/2001
9/24/2001
9/25/2001
NA
Log Identification
9/25/2001
9/25/2001
9/27/2001
9/27/2001
7/10/2001
9/28/2001
SIC
LFB
Matrix Spike
QC Samples:
Date:
Date:
' kJkZ/i' ,^^/u^f^
9/19 & 9/25/2001
2.0 mL of LFS 9/13/01
4.0 mL of LFS 9/13/01
L4540-1 & L4584-6
5^ '/^•^^
100 mL Vol. Flasks
Autosampler Table _
QC Report "
Work Group Report _
Bench Sheet
Data Review
Raw data stored
likage includes data
Hf\y
^
y \y.
/
with Login Number L4540
for Login Number(s) L4540, L4542, L4560,
L4562, & L4584
Login Number
EPA Method
lA/ork Group Number
Run Number
Standard Solution:
MSTDl
MSTD2
MSTD3
MSTD4
MSTD5
Cal Blank
EPA SW-846
L4560
6010
WG7527
R30741
Log Identification
9/25/2001
9/24/2001
9/25/2001
9/24/2001
9/25/2001
NA
6010 QC Data Package Checkli
QC Solutions: Log Identification
LPC
QC-21
QC-7
QC-7 IOX
QC-Sn
QC-P
9/25/2001
9/25/2001
8/30/2001
9/20/2001
7/10/2001
8/21/2001
Analyst:
Peer review by: /^ijiSf
.:2?i//2g..^—
-a^CL.
SIC
LFB
Matrix Spike
QC Samples:
Date:
Date:
9/19 & 9/25/2001
2.0 mL of LFS 9/13/01
4.0 mL of LFS 9/13/01
L4530-2, L4560-9,
&L4584-10
/-/5/^
/^/^/^/^
Comments:
'¥
Dilutions: 100 mL Vol. Flasks
Package Includes: Autosampler Table
QC Report
Work Group Report
Bench Sheet
Data Review
NA
TT
^
~7 ^
Raw data stored with Login Number L4530
Dota package includes data for Login Number(s) L4530. L4560, & L4584
Login Number _
EPA Method _
SOPNumber_
Work Group Number _
Standard Solution:
Nitrite-N QC Data Package Checklist
L4560
9056.0
341
WG7517
Log Identification Concentration (ppm)
Nitrite-N
Autocall R
Autocal2R
Autocal3R
AutocaWR
AutocalSR
CWS-86-489
CWS-86-488
CWS-86-487
CWS-86-486
CWS-86-485
0.5
10
20
QC Solutions: Log Identification Concetration (ppm)
Nitrite-N
CWS-86-488
CWS-86-486
CWS-40-176
ICV
CCV
Spike Stock Sol.
Spike
Spike Preparation: mL of Sample
10
2000
uL of Stock
Nitrite-N
Matrix Spike
Matrix Spike Dup
Analyst:
Peer review:
Comments:
All QC acceptable.
10
10
Package Includes: Autosampler Table
QC Report^
WorkGroup Report^
Bench Sheet^
Data Review X
Raw data stored with Login Number
Data package includes data from Login Number(s)
Work Group Summary Report
Quality Control Data
Analysis: PH 9045 Method: SW 846, 9045
Report Date: 19-SEP-Ol
Summary of QC Samples
Sample QC
Nijmber TyP® Descript.ion
WG7 4 7 4 -1 QCS Independent Check Standard
WG7474
QC Measured Values with Limits
%ReGOV Iiimi ts
100.3 80-120
Summary of Spiked Samples
Sample QC Reference Sample
Number
WG7474-2
Type Number
DUP L4560-12
Samples In Workgroup
L4560-3 L4560-5
L4560-11 L4560-12
Spiked Measured Values with Limits
8.41
L4560-6
RPD
1.06
Limits
0-20
L4560-8 L4560-9
Analyst
Pee
DdLt: /9S^o/
r Revie^TT/^^/^^ ^^ 0/4^ Date f 1 ^Jc^^J
Volatile Organics Data Package Checklist
Sample Login No: L ^^hO
V^ork Group: u ir-r l^'Y
Date Run:>(S£.-P 20^1
Methcd: ,??fcO c;
Maoix: S.ofC
Irstrume.nt ID:Ji_j££l2?
Initial Calibration Location: L.^^o
Run Leg
EFB Tune Report
Continuing Calibration: Quant Repcn/Chromatocram
Ccntinuing Cafibraticn Check Report
Reagent Elank: Guant ReporjChrcmatcgram '
Samcles:Guant Repcrt/Chrcmatccram
Samples: TIC Data
Matrix Scike; Cuant RepcryChrcmatcgram
Matrix Scike Duplicate: Guar: .=v=poru'Chrcrr,atccrarr,
Inie.Tial Standarc Area Reccr
Surccate i Spike.''CuciicaTe Recover/ Reccr
,=r£p/Ex:racticn Leg
rreser/aticn Check
Peer Review
^crr.—.er..i:
r^yt^
CERTIFICATE OF ANALYSIS
Listing of sample information and Testing Requested
Friday, December 7, 2001
TESTED FOR ATK Thiokol: Bacchus
Environmental Compliance M/S M7H7
P. O. Box 98
Magna, UT 84044-0098
Jon IHermance
Project: Lab Anal - Rem - Soil
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-3732
800-863-8080
Login Number L4560
Lab No Client Number
Test Requested
L4560-1 BW-1-1-66.7-68.3
SW-846, 8260
1 L4560-2 BW-1-1-70-71.7
SW-846, 8260
1 L4560-3 BW-1-1-71.7-73.3
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
1 L4560-4 BW-1-1-75-76.7
SW-846, 8260
L4560-5 BW-1-2-0-1.7
SW-846, 8260
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
Description
Volatile Organics
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Volatile Organics
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Received CollectDate/Time
09/18/01
09/18/01
09/18/01
09/18/01
09/18/01
Matrix
09/11/01 14:00
Soil
09/11/01 14:50
Soil
09/11/01 12:00 1
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/01 14:40
Soil
09/13/01 11:15
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Page 1 of 25
L4560-6 BW-1-2-10-11.7 09/18/01 09/13/01 14:00
SW'
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW
SW
SW
•846, 8260
•846, 7471A
846, 7060
•846, 6010
-846, 6010
-846, 6010
-846, 6010
•846, 6010
•846, 6010
•846, 6010
•846, 6010
•846, 3050
846, 9056
846, 9056
846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
1 L4560-7 BW-1-2-18.3-20
SW-846, 8260
1 L4560-8 BW-1-2-20-21.7
Volatile Organics
09/18/01
09/18/01
09/13/01 15:00
Soil
09/13/01 15:15 1
SW-
sw-
sw-
sw-
sw-
sw
sw-
sw-
sw-
sw-
sw-
sw-
sw
sw
sw
-846, 8260
-846, 7471A
-846, 7060
-846, 6010
•846, 6010
•846,6010
•846, 6010
•846, 6010
•846, 6010
'846, 6010
•846, 6010
•846, 3050
846, 9056
846, 9056
846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GF/^ Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L4560-9 BW-1-1-60-62 09/18/01 09/10/01 16:10
SW
SW
SW
SW
SW
SW
SW-
SW-
SW-
SW-
SW-
SW-
sw
sw
sw
-846, 8260
-846, 7471A
-846, 7060
-846,6010
-846, 6010
•846, 6010
•846, 6010
•846, 6010
•846, 6010
•846, 6010
•846, 6010
-846, 3050
846, 9056
846, 9056
846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L4560-10 BW-1-1-EB-1 09/18/01 09/10/01 12:05
SW-846, 8260
SW-846, 7470A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-e46, 6010
SW-846, 3010
Volatile Organics Appendix 9
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
ICP Metals Digestion
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Page 2 of 25
L4560-11 BW-1-2-31.7-33.3 09/16/01 09/14/01 10:50
SW-846, 8260
SW-846, 7471A
SW-846, 7060
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW 846,
SW 846,
SW 846,
6010
,6010
6010
6010
6010
,6010
,6010
,6010
3050
,9056
9056
,9045
I L4560-12 BW-1-2-40-41.7
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/18/01 09/14/01 13:00
SW-846, 8260
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Cr ICP Metals /Vnalysis (RCRA)
Pb ICP Metals /Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
I L4560-13 BW-1-1-TB-2 09/18/01 09/10/01 11:00
SW-846, 8260 Volatile Organics Appendix 9 Water
Comments:
L4560 Method 6010 Metals: A slight negative matrix interference was observed for Ba, Cd, Cr, Pb, and
Se for one of the samples in this set.
Certified By CM,**^
OC Coordinator
This certifies that the following samples were analyzed using good laboratory practices to show the foltowing results:
Date
Page 3of 25
Listing of Results by Sample
IsamplelD: BW-1-1-66.7-68.3
CAS
Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
Test Parameter
1,1.1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1.2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1.1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRiCHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPHOPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2.2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DiCHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DI CHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
Result
U
U
u U
u
u u u
u u
u u
u u
u u
u u u u u u u u
u u u u
ynits
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
6.9x»^ug/kg
u u
u u u
u u u u u u
u u
u u u u u
u u
u u u
u u u u u
u u u u u u
u u u u u u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
LablD:L4560-1 Collect Date: 09/11/01 14:00 |
MDL
.6
.6
.9
.8
4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
Dll.
EQL Factor McthQ^I
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
1 SW-846,8260
1 SW-846. 8260
1 SW-846. 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-e46,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
t SW-846,8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
t SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-646, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Test Djitg
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
09/24/01 14 43
09/24/01 14:43
09/24/01 14:43
09/24/01 14:43
Page 4 of 25
IsamplelD: BW-1-1-70-71.7
CAS
Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75O0-3
67-66-3
74-87-3
156-59^
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1.2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1.2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BLrrANONE
2-CHLOROETHYLVINyL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
Result
U
u
U
u u u u
u u u u u u u
u u u u u
u u
u u u u u
u u
17fi
u u u u
u u u
u u u
u u
u u
u u u u u u u u u u u
u u u u u
u u
u u u
u u u u u
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
LablD:L4560-2 Collect Date: 09/11/01 14:50 |
MDL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
Oil.
EQL Factor Mpthod
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 -
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10 1
10 1
10 1
10 1
10
10 1
10 1
10
10 1
10
10
10
10 -
10
10
10
10
10
10
10 1
10 1
10
10 1
10 1
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
1 SW-846,8260
1 SW-846, 8260
1 SW-B46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
t SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, B260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
AnpiYst
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Test Dste
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24A)1 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24«1 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
09/24/01 15:16
Page 5 of 25
IsamplelD: BW-1-1-71.7-73.3
IfiSt Parameter
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NITRATE-N
NITRITE-N
PH
Result
U
3.34
8540
100
.4
U
16
6
U
U
U
U
9.07
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
mg/l
mg/l
Lab ID: U4560-3
MDL
.01
.98
1.3
.05
.1
.1
.3
1.3
3.2
.2
.01
.01
IQL
.04
3.3
6.6
.3
.5
.5
1.3
6.6
16
.8
.05
.05
DII.
Factor
1
20
1.077
1.077
1.077
1.077
1.077
1.077
1.077
1.077
1
1
1
1
Collect Date: 09/11/01 12:00 |
Method
SW-846, 7471A
SW-846, 7060
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
Analyst
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
MTB
MTB
MTB
CWS
CWS
LDS
I^t Date
10/03/01 10:40
09/28/01 11:54
09/27/01 12:43
09/27/01 12:43
09/27/01 12:43
09/27/01 12:43
09/27/01 12:43
09/27/01 12:43
09/27/01 12:43
09/27/01 12:43
09/26/01 12:00
09/21/01 09:57
09/21/01 09:57
09/18/01 14:24
Page 6of 25
IsamplelD: BW-1-1-75-76.7
CAS
Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
96-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
Test Parameter
1,1,1.2-TETRACHLOBOETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-1 fc 1HACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRlCHLOROPFIOPANE
1,2,4-TRICHLOROBENZENE
1,2.4-TRlMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1.2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRlMETH YLBENZENE
1.3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENT ANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULRDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BLTTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
Result
u
u
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
226
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug*g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
LablD;L4560-4 Collect Date: 09/11/Dl 14:40 1
MpL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
Oil.
EQL Factor Methotf.
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10
10
10 1
10
10 1
10
10
10 1
10 1
10 ••
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
1 SW-846, 8260
1 SW-e46,8260
1 SW-846, 3260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-e46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
1 SW-B46,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Test pate
09/24/01 15:48
09/24/01 15 48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15-48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24)01 15:48
09/24^)1 15:48
09/24/01 15:48
09/24/01 15:48
09/24rt)1 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24A31 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24^)1 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24A)1 15:48
09/24«)1 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
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09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
09/24/01 15:48
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09/24/01 15:48
Page Zof 25
SamplelD: BW-1-2-0-1.7 Lab 10: L4560-5 Collect Date: 09/13/01 11:15
Test Parameter
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
1.1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2.4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOHOETHANE
1,2-DICHLOROPROPANE
1.3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULRDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1
74-95-3
75-71-B
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Bssmt
u
.7
U
U
U
U
U
U
u
u u
u u u u u
u u u u u
u u
u u
u u
u 276
u u u
u u u u u u u u u
u u u u u u u u
u u u u u
u u u u u
u u u u u u u u u u .387
6.89
13900
130
.7
.5
22
9.6
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
MDL
6
6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
4
.5
.6
.5
.3
.5
.01
.96
1.3
.05
.1
.1
.3
1.3
Dil.
EQL Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
04 1
3.3 2
6.5 1.0
.3 1.0
.5 1.0
.5 1.0
1.3 1.0
6.5 1.0
1 SW-846. 8260
1 SW-846. 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846.8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-e46,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-e46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-646, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
D SW-846, 7060
76 SW-846,6010
76 SW-846,6010
76 SW-846,6010
76 SW-846,6010
76 SW-846.6010
76 SW-846, 6010
Analyst
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
Page
lest Pate
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 1620
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
09/24/01 16:20
10/03/01 10:44
09/28/01 12:05
09/27/01 12:46
09/27/01 12:46
09/27/01 12:46
09/27/01 12:46
09/27/01 12:46
09/27/01 12:46
Bof 25
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NITRATE-N
NITRITE-N
PH
7.2
U
1.3
.13
8.32
ug/g
ug/g
mg/l
mg/l
3.1
.2
.01
.01
16
.8
.05
.05
1.076
1.076
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW B46, 9045
MTB
MTB
MTB
CWS
CWS
LDS
09/27/01 12:46
09/27/01 12:46
09/26/01 12:00
09/21/01 10:15
09/21/01 10:15
09/18/01 14:24
Page 9 of 25
IsamplelD: BW-1-2-10-11.7
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-B
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
Test Parameter
1 1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1.1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1.DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2.3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1.2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMErHYLBENZENE
1,3-DICHLOROBENZENE
1.3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2.2-DlCHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENT ANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-18-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01 -6
75-69-4
108-05-4
75-01 -4
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZEN E
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
U
u
U
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
7.3:j-e,ug/kg
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u u
u
u
u
u u
u
u
.178
946
11800
113
.62
48
17
17
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug'g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L4560-6
MDL
.6
.6
9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.01
.8
1.1
05
.09
.09
.2
11
Dll.
EQL Factor
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
50 1
10 1
10 1
50 1
10 1
10 1
50 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
.04 1
2.8 20
5.7 1.121
.2 1.121
.5 1.121
.5 1.121
1.1 1.121
5.7 1.121
Collect Date: 09/13/01 14:00 |
Method.
SW.846, 8260
SW-846. 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, B260
SW-B46, 8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW.B46, 8260
SW-B46, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846. 8260
SW-846, 7471A
SW-846. 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-e46, 6010
SW-846, 6010
SW-846, 6010
Analyst
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
Test Date
09/24/01 16:52
09/24A)1 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24A)1 16:52
09/24/01 16:52
09/24/01 16:52
09/24A)l 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
09/24/01 16:52
10/03/01 10:57
09/28/01 12:11
09/27/01 12:49
09/27/01 12:49
09/27/01 12:49
09/27/01 12:49
09/27/01 12:49
09/27/01 12:49
Page 10 of 25
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NITRATE-N
NITRITE-N
PH
3.6
U
6.5
U
8.3
ug/g
ug/g
mg/l
mg/l
2.7
.1
.01
.01
14
.7
.05
.05
1.121
1.121
1
1
1
1
SW-846. 6010
SW-K46, 6010
SW-?46. 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
LDS
09/27/01 12:49
09/27/01 12:49
09/26/01 12:00
09/21/01 10:32
09/21/01 10:32
09/18/01 14:24
Page 11 of 25
IsamplelD: BW-1-2-18.3-20
CAS
Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
Test Parameter
1,1.1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TE 1 HACHLOROETHANE
1,1.2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1.2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULRDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TEIHACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
Result
U
u u
u u u
u u u
u u u u
u u u u u u u
u u u u u u u u
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
9.5-g-,G. ug/kg
u u u
u u u
u u u
u u u
u u u
u u u u u
u u
u u u
u u
u u u
u u
u u u
u u u u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Lab ID: L4560-7 Collect Date: 09/13/01 15:00 |
MDL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
Dil.
EQL Factor Mgthod
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-B46, 8260
SW-B46, 8260
SW-B46, 8260
SW-B46, 8260
SW-B46, 8260
SW-B46, 8260
SW-B46, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-B46, 8260
SW-B46, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Test Date
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24rt)1 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24mi 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24A)1 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24A)1 17:24
09/24AD1 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
09/24/01 17:24
Page 12 Of 25
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-B2-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
D: BW-1-2-20-21.7
T?5t Pprjmeter
1.1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1.2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1.2,3-TRICHLOROPROPANE
1.2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DlBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPHOPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULRDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZEN E
1t1RACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
u
u u u u u
u u
u u
u u u u u
u u
u u
u u u u u
u u u
u 12 B
u u u u u u u
u u u
u u u
u u u u u
u u u u u
u u
u u u
u u
u u u
u u
u u u u u u 1.84
12700
105
.5
.6
14
8.1
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Lab ID: L4560-8 Collect Date: 09/13/01 15:15 |
MDL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
24
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.01
.9
1 4
.05
.1
.1
.3
1.4
Dil.
EQL Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10 1
10
10
10
10
10
.04
3.2 2
6.7 1.1
.3 1.1
.5 1.1
.5 1.1
1 4 1.1
67 1.1
1 SW-846,8260
1 SW-B46, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-646,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,6260
1 SW-846, 8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-B46,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW;846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
SW-846, 8260
1 SW-846, B260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
0 SW-846,7060
48 SW-846, 6010
48 SW-846, 6010
48 SW-846, 6010
48 SW-B46. 6010
48 SW-846, 6010
48 SW-a46,6010
Analyst
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
Test Date.
09/24/01 17:57
09/24/01 17:57
09/24/01 17.57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24^)1 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24A)1 17:57
09/24A)1 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
09/24/01 17:57
10/03/01 11:00
09/28/01 12:18
09/27/01 12:52
09/27/01 12:52
09/27/01 12:52
09/27/01 12:52
09/27/01 12:52
09/27/01 12:52
Page 13 Of 25
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NITRATE-N
NITRITE-N
PH
U
U
9.2
U
8.51
ug/g
ug/g
mg/l
mg/l
3.2
.2
.01
.01
16
.8
.05
.05
1.148
1.148
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
LDS
09/27/01 12:52
09/27/01 12:52
09/26/01 12:00
09/21/01 10:50
09/21/01 10:50
09/18/01 14:24
Page 14 Of 25
IsamplelD: BW-M-60-62
630-20-6
71-55-6
79-34-5
79-00-S
75-34-3
75-35-4
563-5B-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-B
541-73-1
142-28-9
106-46-7
590-20-7
76-93-3
110-57-8
95-49-8
591-78-6
106-43-*
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
Test Parameter
1,1,1.2-TETRACHLOROETHANE
1.1.1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1.2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBEN2ENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULRDE
CAHBON TEIRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-6
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODI FLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
ltlHACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-T ,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
13 e
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
5.08
14000
113
.6
.2
14
6.7
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
U9'g
Lab ID: L4560-9 Collect Date: 09/10/01 16:10 |
MDL
.6
.6
.9
.6
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
24
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
5
.7
1.2
.6
.7
.6
6
.5
.7
.4
.5
.6
.5
.3
.5
.01
.9
1.4
.05
.1
.1
.3
1.4
Oil.
EQL Factor Methpd
10
10
10
10
ID
10
10
10
10
10
ID
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10
10
10 1
10
10 1
10
10
10 1
10 1
10 1
10 1
.04 1
31 2
6.8 1.1
.3 1.1
.5 1.1
.5 1.1
1.4 1.1
6.8 11
1 SW-846, 8260
1 SW-846,826Q
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, B260
1 SW-B46,8260
1 SW-B46,8260
1 SW-B46, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-e46, 8260
1 SW-846,8260
1 SW-B46,8260
1 SW-e46, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
I SW-846,8260
SW-846, 8260
SW-846, 8260
1 SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-a46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
0 SW-846. 7060
80 SW-846, 6010
80 SW-846, 6010
80 SW-B46, 6010
80 SW-846, 6010
80 SW-846, 6010
80 SW-846, 6010
Analyst
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
isst Date
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24A)l 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24A31 14:11
09/24/01 14:11
09/24031 14:11
09/24AD1 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/Z4/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24A)l 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
09/24/01 14-11
09/24/01 14:11
09/24/01 14:11
09/24/01 14:11
10/03/01 11:09
09/28/01 12:41
09/27/01 13:10
09/27/01 13:10
09/27/01 13:10
09/27/01 13:10
09/27/01 13:10
09/27/01 13:10
Page 15ot 25
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NITRATE-N
NITRITE-N
PH
5.3
U
41
U
9.08
ug/g
ug/g
mg/l
mg/l
3.3
.2
.01
.01
16
.8
.05
.05
1.180
1.180
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846. 9045
MTB
MTB
MTB
CWS
CWS
LDS
09/27/01 13-10
09/27/01 13:10
09/26/01 12:00
09/21/01 11:07
09/21/01 11:07
09/18/01 14:24
Page 16of 25
IsamplelD: BW-1-1-EB-1
CAS
Number
630-20-6
71 -55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
71-36-3
590-20-7
78-93-3
110-75-8
95-49-8
591-78-6
78-83-1
79-46-9
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
107-05-1
71-43-2
108-66-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
126-99-8
156-59-4
10061-01-5
108-94-1
124-48-1
74-95-3
75-71-8
141-7B-6
60-29-7
97-63-2
100-41-4
76-13-1
87-68-3
67-63-0
98-82-8
1330-20-7
126-98-7
74-88-4
80-62-6
75-09-2
104-51-8
103-65-1
91 -20-3
1330-20-7
107-12-0
110-86-1
135-98-8
100-42-5
98-06-6
127-18-4
Test Parameter
1.1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHAN E
1,1,2,2-T ETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1.2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DlCHLOHOBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
1-BUTANOL
2.2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
2-METH YL-1 -PROPANOL
2-NITROPROPANE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
ALLYL CHLORIDE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON Tb 1 HACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CHLOROPRENE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
CYCLOHEXANONE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYL ACETATE
ETHYL ETHER
ETHYL METHACRYLATE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYL ALCOHOL
ISOPROPYLBENZENE
M.P-XYLENE
METHACRYLONITRILE
METHYL IODIDE
METHYL METHACRYLATE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
PROPIONITRILE
PYRIDINE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
Result
U
u u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
14 &
u
u
u
u
u
u
u
u u
u
u
u
u u
u
u
u
u
u
u
u
u
u u
u
u u
u u
u u u
u u
u
u
u u
u
u
u
u
u
u
u
Unit5
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
LablD:L4560-10 Collect Date: 09/10/01 12:05 |
MDL
.6
.6
.9
.8
.4
.5
6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
18
.6
.6
.6
.6
1.3
2.1
.9
.5
.6
1.4
1.8
2.4
1.1
.5
.5
.6
.5
.8
1
.8
.6
.7
.7
4
.7
.3
.6
.5
.4
17
1
.7
.1
1.6
.9
.7
.5
.5
.5
17
.5
1.3
1
.96
1
.5
.5
.7
1.2
.6
.9
25
.7
.6
.6
.5
Dil.
EQL Factor Method
5
5
5
5
5
5
10
10
5
10
10
10
5
10
5
5
10
10
10
10
184
10
100
64
10
50
21
9.2
10
10
50
100
5
5
100
5
10
10
5
5
10
5
5
5
10
5
10
5
10
5
173
5
5
5
16
9.1
5
5
5.3
10 1
174 1
10 1
5 1
5
5
5 1
10 1
10 1
10 1
10 1
5 1
5 1
249 1
10 1
5 1
10 1
5 1
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-646,8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846.8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
SW-846, 8260
1 SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-646, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
Test pate
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
O9/20rt)1 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20A)1 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20A)1 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
Page 17 Of 25
108-88-3
156-60-5
10061-02-6
110-57-6
79-01-6
75-69-4
108-05-4
75^51-4
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOHOPROPENE
TRANS-1,4-DICHLORO-2-BUTEN
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYUIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ICP METALS DIGESTION
U
U
U
u U
u u u u u 29
14
U
5.1
U
U
U
U
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
.7
.4
.5
.7
.6
.5
.3
.5
.2
1.5
25
1
2
2
5
25
60
3
5
5
5
10
5
5
5
10
7
4.3
125
5
10
10
25
125
300
15
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7470A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3010
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
CWS
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
09/20/01 18:59
10/10/01 11:09
10/26/01 14:36
09/28«)l 15:20
09/28/01 15:20
09/28/01 15:20
09/28/01 15:20
09/28/01 15:20
09/28/01 15.20
09/28/01 15:20
09/28/01 15:20
09/26/01 12:00
Page 18 Of 25
IsamplelD: BW-1-2-31.7-33.3
630-2O-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
S6-23-5
108-90-7
75-00-3
67-66-3
74-B7-3
156-59-4
10061-01-£
124-48-1
74-95-3
75-71-B
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1.1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1.2.3-TRICHLOROBENZENE
1,2.3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DlBHOMO-3-CHLOHOPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOHOPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHEH
2-CHLOHOTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CAHBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
Tt TRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
IOB
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
1.84
8630
100
.37
u
18
3.4
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L4560-11 Collect Date: 09/14/01 10:50 1
MDL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.01
.8
1.2
.05
09
.09
.2
1.2
Dll.
EQL Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10
10
10
10
10 1
10 1
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
.04 1
2.9 2
5.7 IO
.2 1.0
.5 1.0
.5 IO
1.2 1.0
5.7 1.0
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-e46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
t SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-B46,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
0 SW-846,7060
82 SW-846, 6010
82 SW-846,6010
82 SW-846,6010
82 SW-846.6010
82 SW-846. 6010
82 SW-846,6010
Analyst
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
Test D?te
09/24/01 18:29
09/24/01 1B:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 16:29
09/24A)1 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24A)1 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 1B:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
09/24/01 18:29
10/03/01 11:14
09/28/01 13:04
09/27/01 13:19
09/27/01 13:19
09/27/01 13:19
09/27/01 13:19
09/27/01 13:19
09/27/01 13:19
Page 19 Of 25
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NITRATE-N
NITRITE-N
PH
U
U
1.8
U
8.81
ug/g
ug/g
mg/l
mg/I
2.8
.1
.01
.01
14
.7
.05
.05
1.082
1.082
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
LDS
09/27/01 13:19
09/27/01 13:19
09/26/01 12:00
09/21/01 12:00
09/21/01 12:00
09/18/01 14:24
Page 20 Of 25
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-S0-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
D: BW-1-2-40-41.7
Te?t Parameter
1,1.1,2-TETRACHLOROETHANE
1.1,1-TRICHLOROETHANE
1.1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1 -DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1.2,3-TRICHLOROBENZENE
1,2,3-THICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3.CHLOROPROPANE
1,2-DlBROMOErHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHEH
2-CHLOnOTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CAHBON DISULRDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
10061-01-5 ClS-1,3-DICHLOROPROPENE
124-48-1
74-96-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-07-6
75-69-4
108-05-4
75-01-4
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHHOMIUM
LEAD
Result
u
1.9T
u
u
u
.5X
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
10 e.
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u u
u
u u
u
u
u
3.53
16300
16B
.8
.4
17
U
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L4560-12 Collect Date: 09/14/01 13:00 |
MPL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
24
1.1
.5
6
.5
8
1
8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
5
.7
.4
.5
.6
.5
.3
.5
.01
.9
1.4
06
.1
.1
.3
1.4
Dil.
EQL Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
ID
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10
10
10
10 1
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
.04 1
3.2 2
7.1 1.2
.3 1.2
.6 1.2
.6 1.2
1.4 1.2
7.1 1.2
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, B260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,6260
1 SW-846,8260
1 SW-B46, B260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-B46,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
1 SW-846, 8260
SW-846, B260
1 SW-846,8260
1 SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-B46. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, B260
SW-846, B260
SW-846, 7471A
3 SW-846, 7060
16 SW-846, 6010
16 SW-846,6010
16 SW-846, 6010
16 SW-846, 6010
16 SW-846, 6010
16 SW-846, 6010
Analyst
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
Test Date
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24A)1
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24^31
09/24/t)1
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24/01
09/24rt)l
09/2A/01
09/24/01
09/24/01
09/24/01
10/03/01
09/28/01
09/27/01
09/27/01
09/27/01
09/27/01
09/27/01
09/27/01
Page 21 of 25
19.01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19.01
19:01
19:01
19:01
19.01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
19:01
11:56
13:11
13:22
13:22
13:22
13:22
13:22
13:22
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NITRATE-N
NITRITE-N
PH
u
u
9
u
8.5
ug/g
ug/g
mg/I
mg/I
3.4
.2
.01
.01
17
.9
.05
.05
1.216
1.216
1
1
1
1
SW-846, 6010
SW-e46,6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
LDS
09/27/01 13:22
09/27/01 13:22
09/26/01 12:00
09/21/01 12:17
09/21/01 12:17
09/18/01 14:24
Page 22 Of 25
IsamplelD: BW-1-1-TB-2
CAS
Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
71-36-3
590-20-7
78-93-3
110-75-8
95-49-8
591-78-6
78-83-1
79-46-9
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
107-05-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
126-99-8
156-59-4
10061-01-5
108-94-1
124-48-1
74-95-3
75-71-8
141-78-6
60-29-7
97-63-2
100-41-4
76-13-1
87-68-3
67-63-0
98-82-8
1330-20-7
126-98-7
74-88-4
80-62-6
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
107-12-0
110-86-1
135-98-8
100-42-5
98-06-6
127-18-4
lest Paraa>.eter
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2.2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2.3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-THIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBHOMOETHANE
1,2-DICHLOROBENZENE
1.2-DlCHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
1-BUTANOL
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
2-METHYL-l -PROPANOL
2-NITROPROPANE
4-CHLOHOTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
ALLYL CHLORIDE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TEIRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CHLOROPRENE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
CYCLOHEXANONE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYL ACETATE
ETHYL ETHER
ETHYL METHACRYLATE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYL ALCOHOL
ISOPROPYLBENZENE
M,P-XYLENE
METHACRYLONITRILE
METHYL IODIDE
METHYL METHACRYLATE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
PROPIONITRILE
PYRIDINE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
Result
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u u
units
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ugn
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/I
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/I
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
LablD:L4560-13 Collect Date: 09/10/01 11:00 |
MDL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
18
.6
.6
.6
.6
1.3
2.1
.9
.5
.6
14
1.8
2.4
1.1
.5
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.6
.5
.4
17
1
.7
.1
1.6
.9
.7
.5
.5
.5
17
.5
1.3
1
.96
1
.5
.5
.7
1.2
.6
.9
25
.7
.6
.6
.5
Dll.
EQL Factor Method
5
5
5
5
5
5
10
10
5
10
10
10
5
10
5
5
10
10
10
10
184
10
100
6.4
10
50
21
9.2
10
10
50
100
5
5
100
5
10
10
5
5
10
5
5
5
10
5
10
5
10
5
173
5
5
5
16 1
9.1 1
5 1
5 1
5.3 1
10 1
174 1
10 1
5 1
5 1
5 1
5 1
10 1
10 1
10 1
10 1
5 1
5 1
249 1
10 1
5 1
10 1
5 1
1 SW-B46. 8260
1 SW-846, 8260
1 SW-B46, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-B46,8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
Test Date
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20rt)1 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/2a'D1 19:34
09/20/01 19:34
09/20/01 19:34
09/201/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20A)1 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
Page 23 Of 25
108-8B-3 TOLUENE
156-60-5 TRANS-1,2-DICHLOROETHENE
10061 -02-6 TRANS-1,3-DICHLOROPHOPENE
110-57-6 TRANS-1,4-DICHLORO-2-BUTEN
79-01-6 TRICHLOROETHENE
75-69-4 TRICHLOROFLUOROMETHANE
108-05-4 VINYL ACETATE
75-01-4 VINYL CHLORIDE
u
u u u u
u u
u
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
.7
.4
.5
.7
.6
.5
.3
.5
5
5
5
10
5
5
5
10
SW-B46, 8260
SW-846, 8260
1 SW-646,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
09/20/01 19:34
Page 24of 25
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected but was
below the MDL.
B Gas Chromatography and Mass Spectral Data Flag. This flag is used when an analyte is found in
the blank as well as the sample
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This flag is used
either when estimating a concentration for tentatively identified compounds or when the data
indicated the presence of a compound that meets the identification criteria but the result is less than
the EQL (e.g. 3 J with an EQL of 10)
MDL Method Detection Limit: The minimum concentration of a substance that can be confidently
measured and reported. The laboratory has demonstrated that the MDL can be achieved in a
laboratory reagent blank, but does not guarentee it can be achieved in all sample matrices.
The MDL is approximately three times the signal noise level.
EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many
analytes the EQL is selected as the value of the lowest standard in the calibration curve.
Dil. Factor Dilution Factor: The prepared smple was diluted by this factor because the sample was too
concentrated or due to other interferences in the sample matrix. Any dilution factor causes
an appropriate increase in the MDL and EQL.
Page 25 of 25
i!':/ i
•f
<('
SCIENCE AND ENGINEERING
L"/^^^
Control of Environmental Samples
Documant No.
SOP-102 1
EffKtive Dale
14 July 98
Issue
5
Page
3 of 4 1
Sample Receipt Checklist
LWR/PO No: L '/S'Cr O
Receipt Date: 1% '<=>cf -O /
Received by: KIA/S
LabID: L t/f^^) rn^mv^.^ JNO^
Samples for Compliance Testing JL
Chain of Custody (COC) X"
If No, was a COC initiated at receipt?
Custody Seal on Shipping Container X
Custody Seals on Sample Containers X
Samples Accompanied by Airbill or Bill of Laden ?^
Samples Properly Labeled A
If No, explain:
Are sample quantities adequate for required testing? L.
If No, explain:
Are samples in appropriate containers? 21
If No, explain:
Are samples within holding times? iL
If No, explain:
Are all sample containers assigned unique laboratory numbers? ///^
If no, assign unique numbers
Temperature of sample at time of receipt: (ltct'ii^<^ \^ ct^f^^ JAJ/ZC^' 7^»»<j/7 '3;^ V/^
pH Log
SamplelD:
Initial pH:
Final pH:.
< 2
ATK
ALLIANT TECHSYSTEMS
Thiokol Propulsion
P.O. Box 707
Brigham City, Utah 84302-0707 USA
Tel: [phone]
Fax: [phone]
LWR-FY01-D1667
19 November 2001
TO: J. Hermance
CC: F. E. Bares and L. Lofgren
FROM: L. V. Dearden
LWR: L4560
WO: Ml 101
SUBJECT: Soil Moisture Content
Results for the soil moisture content are given below in tabular form. Samples were tested using the
ASTM Method: D2216-98 - Standard Test Method for Laboratory Determination of Water(Moisture)
Content of Soil and Rock by Mass. Testing was performed on September 26, 2001.
Sample
Percent
Moisture
L4560-3
L4560-5
L4560-6
L4560-8
L4560-9
L4560-11
L4560-12
7.11
7.10
10.8
12.9
15.3
7.61
17.8
If you have any questions feel free to contact us at ext. 2744.
M. T. Burnett
L. V. Dearden
Chemical and Physical Analysis
L4530
X
Login Number_
EPA Method _
SOP Number]
Work Group Number
Mercury QC Data Package Checklist
L4530
7471A
316
WG7559
A complete discription of QC, sample and standards preparation is located in the "Mercury
Analysis Log Book".
Standard Concentration QC Concentration
LFB
ICV
QCS
CCV
Spike Preparation: The preparation of matrix spikes and matrix spike duplicates is described
in the "Mercury Analysis Log Book". Spike concentration after final
dilutJon is u^ally 4 ppb Hg.
Standard 1
Standard 2
Standard 3
Standard 4
Standard 5
1 ppb
2 ppb
5 ppb
10 ppb
20 ppb
4 ppb
5 ppb
10.0
5 ppb
Analyst:
Peer review:
Comments:
All QC acceptable.
Date: /> M
Date: /o/9/a/ A//
Package Includes: Autosampler Table _x_
QC Report _x_
Work Group Report _x_
Data Sheet _x_
Sample Prep Sheet x
Raw data stored with Login Number
Data package includes data from Login Number(s) L4530
L4560
L4584
Login Number_
EPA Method,
SOP Number]
Work Group Number
Arsenic QC Data Package Checklist
L4530
7060
311
WG7542
A complete description of sample and standards preparation is located in the "Standards
Preparation Log" and "Digestion Log"
Standard Soluiton: Standard Concentration
Standard 1
Standard 2
Standard 3
Standard 4
5 ppb
25 ppb
50 ppb
100 pbb
QC Concentration (ppb)
LFB
ICV
QCS
CCV
50.0
50.0
20.0
50.0
Spike Preparation:
Analyst:
Peer review:
Comments:
All QC acceptable
The preparation of matrix spikes and matrix spike duplicates
is described in the "Digestion Log". Spike Concentration
after final dilution is typically 25 ppb.
Date: ^^/*//^/ 7*—X J'^
Date: /£>A^/6 f
Package Includes: Autosampler Table X
QC Report 2<.
Work Group Report X
Data Review X
Raw data stored with Login Number
Data package includes data from Login Number(s) L4530
L4560
L4584
Ssmple Loghn No
Work Group: [Jl^imi
Volatile Organics Data Package Checklist
Date Run: /^^^ ^^/
Methcd:
Matrix:
Instrument \D:.?-//P7;L
Initial Calibration Loeatien: l~M^HS
Run Log
EFs Tune Report
Continuing Calibration: Guant RepcrJChromatccram
Continuing Calibraticn Check Report
Reagent Blank: Cuant Recoa/Chrcmatcgram '
Samcles:Guant Repcrt/Chrcmatccram
Samples: TIC Data
Mairix Scike: Quant Repon/Chrcmaiccram
Matrix Spike Duplicate: Cuant RepcrL/Chrcm.atacram
Inte.Tial Stancard .Area Reccr
Surrccate i Scike.Cupiicate Recover/ Rsccr:
,=rec/Extracticn Leg
Preser/aticn Check
Peer .Review
Name | Initial
AM
/ Nitrite-N QC Data Package Checklist
Login Number L4530
EPA Method 300.0
SOP Number 341
Work Group Number WG7478
Standard Solution:
Autocall R
Autocal2R
AutocalSR
AutocaWR
AutocalSR
QC Solutions:
ICV
CCV
Spike Stock Sol.
Spike
Spike Preparation:
Matrix Spike
Matrix Spike Dup.
Analvst: j^<^
Peer review: ^^^l^4«<'
Comments:
All QC acceptable.
Log Identification
CWS-86-489
CWS-86-488
CWS-86-487
CWS-86-486
CWS-86-485
Log Identification
CWS-86-488
CWS-86-486
CWS-40-176
mL of Sample
5.00
5.00
Date:
Date:
i
Concentration (ppm)
Nitrite-N
0.5
2
5
10
20
Concetration (ppm)
Nitrite-N
2
10
2000
4
uL of Stock
Nitrite-N
10
10
'^//<i/^(
Package Includes:
Ra
Data package inc
Autosampler Table _
QC Report]
Work Group Report
Bench Sheet]
Data Review
IW data stored with Loc
ludes data from Login
>
>
>
>
>
in Number
Numbe r(s)
(
(
f \
f
f \
L4520
Login Number _
EPA Method _
i/Vork Group Number _
Run Number
EPA SW-846 6010 QC Data Package Checklist
L4530
6010
WG7527
R30741
Standard Solution:
MSTDl
MSTD2
MSTD3
MSTD4
MSTD5
Cal Blank
Log Identification
9/25/2001
9/24/2001
9/25/2001
9/24/2001
9/25/2001
NA
QC Solutions: Log Identification
LPC
QC-21
QC-7
QC-7 IOX
QC-Sn
QC-P
9/25/2001
9/25/2001
8/30/2001
9/20/2001
7/10/2001
8/21/2001
Analyst:
Peer review by:
Comments
SIC
LFB
Matrix Spike
QC Samples:
Date:
Date:
9/19 & 9/25/2001
2.0 mL of LFS 9/13/01
4.0 mL of LFS 9/13/01
L4530-2, L4560-9,
& L4584-10
M/2/'Z^
/>y4^/
j^ ^ <& r j-^
' nili itinn.<;l^ imm! Vf mL Vol. Flasks
Package Includes: Autosampler Table
QC Report
Work Group Report
Bench Sheet
Data Review
NA
-r
?
Raw data stored with Login Number L4530
Data package includes data for Login Number(s) L4530, L4560, & L4584
Volatile Organics Data Package Checklist
Sample Login No: L'f-f^O
Work Group: UJCrlfT^
Date Run:_L5_2i£L2££J
Methcd: 22ief
Matrix: s-o^V JcA
Instrument ID: ^f^PTV
Initial Caiibraticn Location: L *^^ho
Run Log
EFs Tune Report
Continuing Caiibraticn: Quant Report/Chromatccram
Continuing Calibraticn Check Report
Reagent Elank: Quant Report/Chromatcgram '
SamplesrQuant Repcrt/Chromatccram
Samples: TIC Data
Matrix Spike; Quant Reporo'Chrcmatccram
Matrix Spike Duplicate: Ouant Report/Chrcrratccram
Inre.TisI Standarc Area Rspcn
Surccate & Spike'TDuciicate Recover/ Reccr:
Prep/Exn'acticn Leg
rrese.-^/aticn Check
Peer .Review
at/
JL^i^'^^-ii^r^j^/ jU^^t^i^ZjC:/ ^4^
CERTIFICATE OF ANALYSIS
Listing of sample Information and Testing Requested
Friday, December 7, 2001
TESTED FOR ATK Thiokol: Bacchus
Environmental Compliance M/S M7H7
P. O. Box 98
Magna, UT 84044-0098
Jon Hermance
Project: Lab Anal - Rem - Soil
Login Number L4530
Lab No Ciient Number
Test Requested Description
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-3732
800-863-8080
Received CollectDate/Time
Matrix
sw
SW'
sw
sw
SW'
sw-
sw-
sw-
sw-
sw-
sw-
sw-
sw
sw
SW
-846, 8260
•846, 7471A
-846, 7060
•846, 6010
-846, 6010
•846,6010
•846,6010
•846, 6010
•846, 6010
846,6010
•846,6010
•846, 3050
846, 9056
846, 9056
846, 9045
1 L4530-1 BW-1-TB-1
SW-846, 8260
L4530-2 BW-1-1-0-2
Volatile Organics Appendix 9
09/11/01
09/11/01
09/06/01 08:30
Water
09/06/01 11:15 1
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soii
Soil
Soil
Soil
Soil
I L4530-3 BW-1-1-10-12 09/11/01 09/06/01 13:00
SW
SW
SW
SW
SW-
SW-
SW-
SW-
SW^
SW-
SW-
SW-
SW
SW
SW
-846, 8260
-846, 7471A
-846, 7060
-846, 6010
-846, 6010
•846, 6010
•846, 6010
•846, 6010
•846, 6010
•846, 6010
-846, 6010
-846, 3050
846, 9056
846, 9056
846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
ICP/GF/VA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
1 L4530-4 BW-1-1-13.3-15
SW-846, 8260
L4530-5 BW-1-1-15-17.7
Volatile Organics
09/11/01
09/11/01
09/06/01 15:10 1
Soil
09/06/01 15:21
SW-846, 8260 Volatile Organics Soil
Page 1 of 20
I L4530-6 BW-1-1-20-22 09/11/01 09/06/01 16:40
SW
SW-
SW
SW-
SW-
SW-
SW-
SW-
SW-
sw-
SW-
sw-
SW
sw
SW
-846, 8260
-846, 7471A
-846, 7060
•846, 6010
•846, 6010
•846, 6010
•846, 6010
•846, 6010
•846, 6010
•846,6010
•846, 6010
•846, 3050
846, 9056
846, 9056
846, 9045
I L4530-7 BW-1-1-30-JF
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate /Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/01 09/07/01 10:40
SW
SW-
SW
SW-
SW^
SW-
SW-
SW^
SW^
SW^
SW-
SW-
SW
SW
SW
1-846, 8260
-846, 7471A
-846, 7060
-846, 6010
-846, 6010
•646, 6010
•846,6010
•846, 6010
•846, 6010
•846, 6010
-846, 6010
-846, 3050
846, 9056
846, 9056
846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
I L4530-8 BW-1-1-40-41.7 09/11/01 09/07/01 14:00
SW
SW-
SW-
SW-
SW-
SW-
SW^
SW-
SW-
sw^
sw-
sw-
sw
sw
sw
-846, 8260
-846, 7471A
-846, 7060
•846, 6010
•846, 6010
•846, 6010
•846,6010
•846, 6010
'846, 6010
•846, 6010
-846, 6010
-846, 3050
846, 9056
846, 9056
846, 9045
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals /Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Be ICP Metals /\nalysis (RCRA)
Ba ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soii
I L4530-9 BW-1-1-50-51.7 09/11/01 09/07/01 16:15
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW-
SW
SW-
sw-
sw
sw
sw
•846, 8260
•846, 7471A
•846, 7060
-846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
-846, 6010
•846,6010
•846, 3050
846, 9056
846, 9056
846,9045
Volatile Organics
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Nitrate Analysis by IC
Nitrite Analysis by IC
pH Electrode Measurement
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Comments:
L4530 Method 6010 Metals: A slight negative matrix interference was obsen/ed for Ba, Cd, Cr, Pb, and
Page 2 of 20
Se for one of the samples in this data set.
Results are given based on dry sample weight. Attached is a memo with moisture content of the samples.
QC Coordinator \j
Certified By H'^^'^^^^^ N^^A^'T^ 7- ft&^-2Lfeg>/
Date
This certifies that the following samples were analyzed using good laboratory practices to show the following results:
Page 3 of 20
Listing of Results by Sample
1 Sample ID: BW-l-TB-1
CAS
Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
71-36-3
590-20-7
78-93-3
110-75-8
95-49-8
591-78-6
78-83-1
79-46-9
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
107-05-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
126-99-8
156-59-4
10061-01-5
108-94-1
124-48-1
74-95-3
75-71-8
141-78-6
60-29-7
97-63-2
100-41-4
76-13-1
87-68-3
67-63-0
98-82-8
1330-20-7
126-98-7
74-88-4
80-62-6
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
107-12-0
110-86-1
135-98-8
100-42-5
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1.1,1 -TRICHLOROETHANE
1,1,2,2-TETBACHLOHOETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1.1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOHOETHANE
1,2-DICHLOBOPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOFIOPROPANE
1,4-DICHLOROBENZENE
1-BUTANOL
2.2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
2-METHYL-l -PROPANOL
2-NITROPROPANE
4-CHLOROTOLUENE
4-lSOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
ALLYL CHLORIDE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CAHBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CHLOROPRENE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPHOPENE
CYCLOHEXANONE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYL ACETATE
ETHYL ETHER
ETHYL METHACRYLATE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYL ALCOHOL
ISOPROPYLBENZENE
M.P-XYLENE
METHACRYLONITRILE
METHYL IODIDE
METHYL METHACRYLATE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PHOPYLBENZENE
NAPHTHALENE
O-XYLENE
PROPIONITRILE
PYRIDINE
SEC-BUTYLBENZENE
STYRENE
Result
U
U
u
u
u u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u u
u
u
u
u
u u
u
Units
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/I
ug/l
ug/l
ug/I
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/I
ug/I
ug/I
ug/I
ug/l
ug/I
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/I
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
Lab ID: L4530-1 Collect Oate: 09/06/01 08:30 |
WK
1
1
1
1
1
1
10
10
1
10
10
10
1
10
1
1
10
10
10
10
IB
10
20
.6
10
10
2.1
.9
10
10
10
20
1
1
20
1
10
10
1
1
2
1
1
1
2
1
2
1
10
1
17
1
1
1
1.6
.9
1
1
.5
10
17
10
1
1
1
1
10
10
10
10
1
1
25
10
1
Dil.
Efik Factor MethPd
5
5
5
5
5
5
10
10
5
10
10
10
5
10
5
5
10
10
10
10
184
10
100
6.4
10
50
21
9.2
10
10
50
100
5
5
100
5
10
10
5
5
10
5
5
5
10
5
10
5
10
5
173
5
5
5
16
9.1
5
5
5.3
10 -
174
10 1
5
5 1
5
5
10
10
10
10
5 1
5 1
249 1
10 1
5 1
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846. 8260
1 SW-846. 8260
1 SW-846, 8260
1 SW-846,8250
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-e46,8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
1 SW-846,8260
1 SW-B46,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
SW-846, 8260
1 SW-e46,8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
Ansiysi
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
Page
Test oatfi
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11.01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
09/19/01 11:01
4 Of 20
98-0g-6 TERT-BUTYLBENZENE
127-18-4 TETRACHLOROETHENE
108-88-3 TOLUENE
156-60-5 TRANS-1,2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
110-57-6 TRANS-1,4-0ICHLORO-2-BUTEN
79-01-6 TRICHLOROETHENE
75-69-4 TRICHLOROFLUOROMETHANE
108-05-4 VINYL ACETATE
75-01-4 VINYL CHLORIDE
U
u u u
u u
u u u
u
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
0
2
10
5
5
5
5
10
5
5
5
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
09/19/01 11
09/19/01 11
09/19/01 11
09/19/01 11
09/19/01 11
09/19/01 11
09/19/01 11
09/19/01 11
09/19/01 11
09/19/01 11
01
01
01
01
01
01
01
01
01
01
Page 5 of 20
IsamplelD: BW-1-1-0-2
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61 -6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541 -73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124^^8-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-*
75-01-4
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2.2-TETRACHLOROETHANE
1,1,2-THICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOHOBENZENE
1,2,3-TRICHLOROPROPANE
1,2.4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOHOPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOHOETHANE
1,2-DICHLOHOPROPANE
1,3,5-TRIMErHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOHOTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPHOPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOHOETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
U
u u U
U
u U
U
U
u U
U
U
u
u u u u
u u u u u
u u u
u u loe
u u u u
u u u u u
u u u
u u u
u u
u u u
u u
u u
u u u
u u
u u u u u
u u
u u u
u .031
7.87
19300
149
.9
.7
24
9.6
-Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Lab ID: L4530-2 Collect Date: 09/06/01 11:15 |
MDL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
6
6
6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
6
.7
.6
.6
.5
.7
.4
5
6
.5
.3
5
.01
.99
1.3
.05
.1
.1
.3
1.3
Dil.
equ Factor p/l?thQd
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 '
10
10 ^
10
10
10
10
10
10 1
10 1
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
.04 1
3.4 2
6.6 1.0
.3 1.0
.5 1.0
.5 1.0
1.3 1.0
6.6 1.0
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW.846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46,8260
1 SW-846,8260
) SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
0 SW-846,7060
78 SW-846, 6010
78 SW-846, 6010
78 SW-846, 6010
78 SW-846, 6010
78 SW-846, 6010
78 SW-846,6010
Analyst
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKH
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKR
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
Page
I&st Dat«
09/13/01 16:50
09/13/01 16:50
09/13A31 16:50
09/13A)1 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13rt)1 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13A)1 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13rt)1 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/131/01 16:50
09/13rt)1 16:50
09/13/01 16:50
09/13^1 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
09/13/01 16:50
10/03/01 10:07
09/28/01 10:40
09/27/01 12:20
09/27/01 12:20
09/27/01 12:20
09/27/01 12:20
09/27/01 12:20
09/27/01 12:20
6of20
SFI FNIUM
SILVER
ICP/GFAA METALS DIGESTION
NITRATE-N
NITRITE-N
PH
u u
6.9
U
8.49
ug/g
ug/g
mg/l
mg/l
3.2
.2
.01
.01
16
.8
.05
.05
1.078
1.078
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
LDS
09/27/01 12:20
09/27/01 12:20
09/26/01 12:00
09/18/01 13:56
09/18/01 13:56
09/14/01 07:31
Page 7 of 20
IsamplelD: BW.1-1-10-12
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-61-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05^
75-01-4
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPHOPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DlBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DlCHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DlCHLOHOBENZENE
2,2-DlCHLOROPHOPANE
2-BUTANONE
2-CHLOHOETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTAN0NE
ACETONE
ACROI RIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
ClS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
THANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
R?9yit
u
u
u
u u
u
u u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
9.2"3'je ug/kg
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u u
u
u
u
7.38
7880
73
.4
.2
12
3.9
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/Kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Lab ID: L4530-3 Collect Date: 09/06/01 13.00 |
MPL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
6
7
.5
.6
6
.6
.6
1.3
.5
.6
1 4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.01
.97
1.3
.05
.1
.1
3
1.3
Dil.
iQL Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10
10
10
10 1
10 -
10 •'
.04
3.3 2
6.5 1.0
.3 l.C
.5 1.0
.5 l.C
1.3 1.0
6.5 l.C
SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846. 8260
1 SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
1 SW-846, 8260
SW-B46, 8260
SW-e46, 8260
SW-846, 8260
SW-646, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
0 SW-846,7060
70 SW-846.6010
70 SW-846,6010
70 SW-846,6010
70 SW-846, 6010
70 SW-846,6010
70 SW-846,6010
Analyst
MKH
MKH
MKR
MKR
MKR
MKH
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
Page
Test Date
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/1 SfOI 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13rt)1 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13A31 17:25
09/13A31 17:25
09/13A)1 17:25
09/13/01 17:25
09/13/01 17:25
09/13«)1 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13A31 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
09/13/01 17:25
10/03/01 10:14
09/28/01 11:04
09/27/01 12:29
09/27/01 12:29
09/27/01 12:29
09/27/01 12:29
09/27/01 12:29
09/27/01 12:29
8 Of 20
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NITRATE-N
NITRITE-N
PH
u
u
u u 8.94
ug/g
ug/g
mg/l
mg/l
3.1
.2
.01
.01
16
.8
.05
.05
1.070
1.070
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846. 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
LDS
09/27/01 12:29
09/27/01 12:29
09/26/01 12:00
09/18/01 1413
09/18/01 14:13
09/14/01 07:31
Page 9 of 20
IsamplelD: BW-1-1-13.3-15
CAS
Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
76-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-B7-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59^
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
iBSt Psrqrneter
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TE I HACHLOROETHANE
1,1.2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOHOETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPHOPANE
1,2-DIBROMOETHANE
1,2-DICHLOHOBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,S-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOHOETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOHOTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON Ibl HACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
ClS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOHOETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
Result
U
u u
u
u u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u u
u
u
u
u
u
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
77^ ug/kg
u "^
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Lab ID: L4530-4 Collect Date: 09/06/01 15:10 |
MPL
6
.6
9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
6
.7
.5
.6
.6
.6
.6
1.3
.5
6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
6
.7
.7
4
7
.3
.5
.4
1
7
1
5
.5
.5
.5
1 3
.5
.5
.7
1.2
6
7
.6
.6
.5
7
4
.5
.6
.5
.3
.5
Dl .
EOk Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-a46, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-346, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKH
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKH
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKH
MKR
MKR
MKR
Ifijt Date
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 1759
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
09/13/01 17:59
Page 10 Of 20
IsamplelD: BW-1-1-15-17.7
CAS
Number Test Parameter
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-B7-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-E
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
lOB-05-4
75-01 -4
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-1 b I RACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPHOPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4.ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CAHBON DISULFIDE
CAHBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M, P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
Result
U
U
U
U
U
u u
U
U
u
U
U
U
U
u
U
U
U
u
U
U
u u
u u
u u
UB 12
u u u
u u u u u u u u u u u u u u u u
u u u u
u u u u u u u
u u u u u
u u u
u u
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugiT<g
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Lab ID: L4530-5 Collect Date: 09/06/01 15:21 |
MDL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
Dil.
EQL Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10
10
10 1
10 '
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-S46, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-B46,8260
1 SW-B46,8260
1 SW-846, B260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
Analyst
MKR
MKR
MKH
MKR
MKR
MKH
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKH
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKH
MKR
MKH
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
Test Date
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13rt)1 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13rt)1 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
09/13/01 18:33
Page 11 of 20
IsamplelD: BW-1-1-20-22
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61 -6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-S
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
Test Parameter
1,1,1,2-TETHACHLOROETHANE
1.1,1 -TRICHLOROETHANE
1,1,2,2-TtI RACHLOROETHANE
1,1,2-TRICHLOROETHANE
1.1-DICHLOROETHANE
1,1-DICHLOHOETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOHOPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPHOPANE
1,4-DICHLOROBENZENE
2,2-DICHLOHOPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENrANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOHOETHENE
10061-01-5 CIS-1,3-DICHLOROPHOPENE
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-OICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
u
u
u
u U
u
u
u
u
u
u
u
u u
u
u
u
u u
u
u
u
u u
u
u
u
u
umts
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
e.e':!'© ug/kg
u u
u
u
u
u
u
u
u u
u
u
u
u u
u u
u
u
u
u
u
u
u u
u
u
u
u u
u
u
u
u
u
u
u u
u
u
u
4.28
7710
62
.3
.5
12
5.4
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/Kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/Kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugrtcg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Lab ID: L4530-6 Collect Oate: 09/06/D1 16:40 |
MPL
.6
6
9
.8
.4
.5
.6
.99
1.3
6
.7
1
8
.7
7
.5
.6
.6
7
.5
.6
.6
6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
6
.5
.3
.5
.01
.98
1.3
.05
.1
.1
.3
1.3
Oil.
IQL Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
.04
3.3 2
6.5 l.C
.3 l.C
.5 l.C
.5 l.C
1.3 l.C
6.5 l.C
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
I SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
0 SW-846,7060
68 SW-846,6010
68 SW-846,6010
)6B SW-846,6010
168 SW-846,6010
)68 SW-846,6010
>68 SW-846, 6010
Analyst
MKH
MKR
MKR
MKH
MKR
MKH
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKH
MKR
MKR
MKH
MKH
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKH
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKR
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
Test Date
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13«)1 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13«1 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13rt]1 19:07
09/13/01 19:07
09/13/01 19:07
09/13A31 19:07
09/13/01 19:07
09/13AD1 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
09/13/01 19:07
10/03/01 10:19
09/28/01 11:10
09/27/01 12:32
09/27/01 12:32
09/27/01 12:32
09/27/01 12:32
09/27/01 12:32
09/27/01 12:32
Page 12 Of 20
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NITHATE-N
NITRITE-N
PH
u u
u u
9.2
ug/g
ug/g
mg/l
mg/I
3.1
.2
.01
.01
16
.8
.05
.05
1.068
1.068
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
LDS
09/27/01 12:32
09/27/01 12:32
09/26/01 12:00
09/18/01 14:31
09/18/01 14:31
09/14/01 07:31
PagelSof 20
IsamplelD: BW-1-1-30-32
630-20-6
71-55-6
79-34-5
79-00-S
75-34-3
75-35-4
563-58-6
87-61-6
96-1 B-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
IfiSt Pjiranieter
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-1 b T RACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1.2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOHOBENZENE
1,2-DICHLOHOETHANE
1,2-DICHLOROPHOPANE
1,3,5-THIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOHOBENZENE
2,2-DICHLOHOPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON 111 HACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOHOETHENE
10061 -01-5 CIS-1,3-DICHLOROPROPENE
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
10061 -02-6 TRANS-1,3-DICHLOROPROPENE
79-01-6
75-69-4
108-05-4
75-01-4
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BEHYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
U
u
u
u
u
u
u
u
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
5.2Xp>>ug/kg
U *
u
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
3.04
7000
85
.3
.3
12
6.3
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L4530-7 Collect Date: 09/07/01 10:40 |
MPU
.6
.6
.9
.8
.4
.5
.6
99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
3
.5
.01
.9
1.3
.05
.1
.1
.3
1.3
Dil.
SQL Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10
10
10
10
10
10 •
.04
3.2 2
6.4 1.0
.3 l.C
.5 l.C
.5 1.0
1.3 1.0
6.4 1.0
1 SW-846,8260
1 SW.846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
t SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
1 SW-846,8260
SW-846, 8260
SW-e46, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-a46. 8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
0 SW-846, 7060
84 SW-846, 6010
84 SW-846, 6010
f84 SW-846, 6010
84 SW-846, 6010
84 SW-846. 6010
84 SW-846, 6010
Analyst
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKH
MKR
MKH
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
IfiSt P9te
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19.41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 1941
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19.41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19.41
09/13/01 19:41
09/13rt)1 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13^1 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19.41
09/13/01 19:41
09/13rt)1 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
09/13/01 19:41
10/03/01 10:26
09/28/01 11:31
09/27/01 12:34
09/27/01 12:34
09/27/01 12:34
09/27/01 12:34
09/27/01 12:34
09/27/01 12:34
Page 14 of 20
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NITRATE-N
NITRITE-N
PH
U
U
7.6
U
9.21
ug/g
ug/g
mg/l
mg/l
3.1
.2
.01
.01
15
.8
.05
.05
1.084
1.084
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
LDS
09/27/01 12:34
09/27/01 12:34
09/26/01 12:00
09/18/01 14:48
09/18/01 14:48
09/14/01 07:31
Page 15 of 20
IsamplelD: BW-1-1-40-41.7
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-B6-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOHOETHANE
1,1,2,2-TETRACHLOROeTH AN E
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1.2,3-TRICHLOROPHOPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TBIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TBIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOHOPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOHOETHENE
10061-02-6 TRANS-1,3-DICHLOHOPROPENE
79-01-6
75-69-4
108-05-4
75-01-4
TRICHLOROETHENE
TRICHLOHOFLUOROMETH AN E
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
u
u u
u
u
u
u u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
6.6-0^
u
u
u u
u
u
u
u u
u
u u
u u
u
u
u
u
u
u
u
u
u u
u
u
u
u u
u u
u
u
u
u
u
u u u
u
.015
4.91
7930
189
.36
U
15
7.4
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
6^ g/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Ub ID: L4530-8 Collect Date: 09/07/01 14:00 |
MDL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
6
7
1
.8
.7
7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.6
.6
1.4
18
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.01
.9
1.2
.05
.1
.1
.2
1.2
Dil.
gQL Factor Methpd
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10
10
10
10
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
.04 1
3.1 2
6.1 1.0
.2 1.0
.5 1.0
.5 1.0
1.2 1.0
6.1 1.0
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-e46,8260
SW-846, 8260
1 SW-846, 8260
SW-846. 8260
SW-e46, 8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, B260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
0 SW-846,7060
67 SW-846, 6010
67 SW-846, 6010
67 SW-846, 6010
67 SW-846,6010
€7 SW-846, 6010
67 SW-846, 6010
Analyst
MKR
MKR
MKR
MKR
MKR
MKH
MKH
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKH
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKH
MKH
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKH
MKR
MKH
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKH
MKH
MKR
MKR
MKR
MKH
MKR
MKR
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
Test Dqte
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20 16
09/13/0120:16
09/13/0120:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/0120:16
09/13AD1 20:16
09/13A31 20:16
09/13AD1 20:16
09/13/0120:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13A)1 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13«1 20:16
09/13«)1 20:16
09/13rt>1 20:16
09/13/01 20:16
09/13/0120:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13rt)1 20:16
09/13rt)1 20:16
09/13rt)1 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13mi 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13A31 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/0120:16
09/13/0120:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/0120:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
09/13/01 20:16
10/03/01 10:31
09/28/01 11:41
09/27/01 12:37
09/27/01 12:37
09/27/01 12:37
09/27/01 12:37
09/27/01 12:37
09/27/01 12:37
Page 16 of 20
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NITRATE-N
NITRITE-N
PH
U
U
7.7
U
1.23
ug/g
ug/g
mg/l
mg/l
3
.1
.01
.01
15
.7
OS
.05
1.067
1.067
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
LDS
09/27/01 12:37
09/27/01 12:37
09/26/01 12:00
09/18/01 15:41
09/18rt)1 15:41
09/14/01 07:31
Page 17of 20
IsamplelD: BW-1-1-50-51.7
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-57-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
S6-23-S
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
76-13-1
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-B
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TE I HACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOHOPROPANE
1,2-DIBROMOETHANE
1.2-DICHLOHOBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOHOPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1.3-DICHLOROPHOPANE
1,4-DICHLOROBBMZENE
2,2-DICHLOHOPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4.CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TtTRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-OICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
Result
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
10 e,
u
u
u
u
u
u
u
u u
u
u
u
u u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
.021
2.55
6680
262
.3
.2
13
5.4
Units
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LabID:L4530-9 Collect Date: 09/07/01 16:15 |
MPL
.6
.6
.9
.8
.4
.5
.6
.99
1.3
.6
.7
1
.B
7
.7
.5
.6
.6
.7
.5
.6
6
.6
.6
1.3
.5
6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.01
.9
1.3
.05
.1
.1
.3
1.3
Oil.
eQL Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
10
10
so
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
.04
3.2 2
6.3 l.C
.3 l.C
.5 l.C
.5 l.C
1.3 l.C
6.3 l.C
SW-846, 8260
1 SW-846, 8260
SW-846, 8260
1 SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-S46, 8260
1 SW-846,8260
I SW-846,8260
1 SW-e46,8260
1 SW-e46,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
1 SW-846,8260
t SW-846,8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
I SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-a46,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
t SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
0 SW-846, 7060
60 SW-846,6010
60 SW-846,6010
160 SW-846, 6010
»60 SW-846,6010
60 SW-846,6010
60 SW-846, 6010
Analyst
MKR
MKR
MKH
MKH
MKH
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKH
MKH
MKR
MKH
MKH
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKH
MKR
MKR
MKR
MKH
MKR
MKH
MKH
MKR
MKH
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKR
MKR
MKH
MKR
MKR
MKR
MKH
MKR
MKR
CWS
CWS
MTB
MTB
MTB
MTB
MTB
MTB
I^t Date
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13A)1 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13rt)1 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13rt)1 20:50
09/13/0120:50
09/13/01 20:50
09/13A)1 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13rt)1 20:50
09/13«)1 20:50
09/13rt)1 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13«)1 20:50
09/13/01 20:50
09/13/01 20:50
09/13rt)1 20:50
09/13A)1 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
09/13«)1 20:50
09/13/01 20:50
09/13/01 20:50
09/13/01 20:50
10/03/01 10:35
09/28/01 11:48
09/27/01 12:40
09/27/01 12:40
09/27/01 12:40
09/27/01 12:40
09/27/01 12:40
09/27/01 12:40
Page 18 Of 20
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
NITRATE-N
NITRITE-N
PH
U
U
6.8
U
9.04
ug/g
ug/g
mg'l
mg/l
3
.2
.01
.01
15
.8
.05
.05
1.060
1.060
1
1
1
1
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 9056
SW 846, 9056
SW 846, 9045
MTB
MTB
MTB
CWS
CWS
LDS
09/27/01 12:40
09/27/01 12:40
09/26/01 12:00
09/18A)1 15:58
09/18/01 15:58
09/14/01 07:31
Page 19 Of 20
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected but was
below the MDL.
B Gas Chromatography and Mass Spectral Data Flag. This tlag is used when an analyte is found in
the blank as well as the sample
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This flag is used
either when estimating a concentration tor tentatively identified compounds or when the data
indicated the presence of a compound that meets the identification criteria but the result is less than
the EQL (e.g. 3 J with an EQL of 10)
MDL Method Detection Limit: The minimum concentration of a substance that can be confidently
measured and reported. The laboratory has demonstrated that the MDL can be achieved in a
laboratory reagent blank, but does not guarentee it can be achieved in all sample matrices.
The MDL is approximately three times the signal noise level.
EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many
analytes the EQL is selected as the value of the lowest standard in the calibration curve.
Dil. Factor Dilution Factor: The prepared smple was diluted by this factor because the sample was too
concentrated or due to other interferences in the sample matrix. Any dilution factor causes
an appropriate increase in the MDL and EQL.
Page 20 of 20
SCIENCE AND ENGINEERING
L "^SlxP
THMuan.
Control of Environmental Samples
Document No.
SOP-102
Effective Date
14 July 98
Issue
5
Page
3 of 4
Sample Receipt Checklist
LWR/PO No: ^ L/^ "J ^
ReceiptPate: //- SspT - P/
Received by; //^[/J B>
LabID: / f/^ 3^ H/te. No
Samples for Compliance Testing X
Chain of Custody (COC) X
If No, was a COC initiated at receipt?
X Custody Seal on Shipping Container
Custody Seals on Sample Containers X
Samples Accompanied by Airbill or Bill of Laden /
Samples Property Labeled
If No, explain:
I 2L
Are sample quantities adequate for required testing? il
If No, explain:
Are samples in appropriate containers? 21
If No, explain:
Are samples within holding times? X
If No, explain:
Are all sample containers assigned unique laboratory numbers? ///)
it no, assign unique numbers
Temperature of sample at time of receipt: R-Cc^t^e/^ t^ £zrt>lzv uo//ce. y"g*^ 'i^ '/'d^
pHLog
SamplelD:
Initial pH:
Final pH:.
M
ATK
ALLIANT TECHSYSTEMS
Thiokol Propulsion
P.O. Box 707
Brigfiam City, Utah 84302-0707 USA
Tel: [phone]
Fax: [phone]
LWR-FY01-D1434
9 October 2001
TO: J. Hermance
CC: F. E. Bares and L. Lofgren
FROM: L. V. Dearden
LWR: L4530
WO: M1101
SUBJECT: Soil Moisture Content
Results for the soil moisture content are given below in tabular form. Samples were tested using the
ASTM Method: D2216-98 - Standard Test Method for Laboratory Determination of Water(Moisture)
Content of Soil and Rock by Mass. Testing was performed on September 26, 2001.
Sample
Percent
Moisture
L4530-2
L4530-3
L4530-6
L4530-7
L4530-8
L4530-9
7.27
6.55
6.38
7.77
6.31
5.65
If you have any questions feel free to contact us at ext. 2744.
M. T. Burnett
L. V. Dearden
Chemical and Physical Analysis
*
«
Thiokol Environmental Laboratory
28-OCT-02
Quality Control Report For Work Order L4560
Samples submitted to the laboratory are assigned a "work order" number with a prefix of 'L' (example L1000)
and each sample is assigned a number which consists of the work order number followed by a dash and a
number (example Ll 000-1). Samples are assigned to "work groups" when the analysts are ready to run a
particular test. Each work group is given a number with a prefix of 'WG' (example WG2100). Quality control
samples that are run with each group of samples are given sample numbers that are the work group number
followed by a dash and number (example WG2100-1). There may be more than one work order number in a
work group. Some of the sample spikes listed in this report may be from a different work order.
This report lists by individual laboratory departments and work groups the quality control samples that were run
with each test requested by this work order. A description of the quality control samples is provided with the
control sample i.e. Continuing Calibration, Initial Calibration Verification, Laboratory Reagent Blank, etc. The
initial calibration of the instruments are not included.
Summary of Work Groups Run witti Workorder
Work Group No. Department
WG7496
WG7514
WG7524
WG7527
WG7474
WG7517
WG7542
WG7559
WG7601
WG7675
(MS) GC/Mass Spectrometry
(MS) GC/Mass Spectrometry
(MT) Metals Analysis
(MT) Metals Analysis
(WT) Wet Lab
(IC) lon Chromatography
(AA) Atomic Absorption
(AA) Atomic Absorption
(AA) Atomic Absorption
(AA) Atomic Absorption
Test
SW-846,
SW-846,
SW-846,
SW-846,
SW 846,
SW846,
SW-846,
SW-846,
SW-846,
SW-846,
8260
8260
6010
6010
9045
9056
7060
7471A
7470A
7060
IVIatrix
Water
Soil
Water
Soil
Soil
Soil
Soil
Soil
Water
Water
Description of Terms
INTSTD Internal Standard
RESP Raw Response from the Instrument
SURR Surrogate
% Recov Percent Recovery from reference value
% Percent Recovery of surrogates from reference value
%RPD Relative Percent Difference between duplicate samples
Limits Laboratory guidelines based on statistical analysis or method requirements
Indicates an out-of-limit value
1 of 20 Pages
Quality Control Report
Department: GC/Mass Spectrometry
2a-ocT-02 WG7496 SW-846, 8260
Sample Description Date Tested Test Parameter Measured Value Recoven/ Limits RPD Limits
WG7496-1 (CC) Continuing Calitiration
Date Tested Test Parameter
20-SEP-01 14:11 INTSTD 1,4-DICHLOROBEN2ENE-D4
INTSTD CHLOROBENZENE-DS
INTSTD FLUOROBENZENE
SURR
SURR
SURR
SURR
1,1,2,2-111 HACHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROPROPANE
BROMOFORM
CHLOROBENZENE
CHLOROFORM
CHLOROMETHANE
ETHYLBENZENE
TOLUENE
VINYL CHLORIDE
1,2-DICHLDROETHANE-D4
BROMOFLUOROBENZENE
DIBROMOaUOROMETHANE
T0LUENE-D8
Measured Value
45 ugfl
46 ug/l
46 ugfl
46 ug/I
47 ug/l
46 ug/l
44 UQ/1
47 ug/l
47 ug/I
48 ug/I
49 ug/I
, Recovery
172613 RESP
371120 RESP
598829 RESP
90.1 %Recov
92.9 %Recov
91.4%R6C0V
92 %Recov
93.9%Recov
95.1%R8C0V
88.5%Recov
93.6%Recov
94.8%Recov
95.8 %Recov
97.9 %Recov
Limits
80 -120
80 -120
BO -120
80 • 120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
86-115
86-118
88-110
2 of 20 Pages
Sample
WG7496-2
Description
(LRB) Latxiralory Reagent Blank
Date Tested Test Parameter Mea
20-SEP-Ol 14:47 INTSTD 1,4-DICHLOROBENZENE-D4
INTSTD CHLOROBENZENE-DS
INTSTD FLUOROBENZENE
1,1,1,2-IErRACHLOROETHANE
1,1.1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBEN2ENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1.3-DICHLOROBENZENE
1,3-OICHLOROPROPANE
1,4-DICHLOROBENZENE
1-BUTANOL
2,2-DICHLOROPROPANE
2-BUTANONE
2-GHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
2-METHYL-l-PROPANOL
2-NITROPROPANE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
AU.YL CHLORIDE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TEIRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CHLOROPRENE
CIS-1.2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
CYCLOHEXANONE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYL ACETATE
ETHYL ETHER
ETHYL METHACRYUTE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYL ALCOHOL
ISOPROPYLBENZENE
M,P-XYLENE
METHACRYLONITRILE
METHYL IODIDE
METHYL METHACRYLATE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
PROPIONITRILE
PYRIDINE
SEC-BLTTYLBENZENE
STYRENE
TERTBUTYLBENZENE
ItlRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRANS-1,4-DICHLORO-2-BUTEN
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
sured Value Recoverv
163759 RESP
368338 RESP
588711 RESP
Uugfl
Uugn
Uugl
Uugfl
Uug/1
Uug/I
Uugl
Uugfl
Uug/I
Uug/I
Uug/I
Uug/I
Uug/I
.lug/l
.2 ug/I
Uug/I
.09 ug/l
.2 ug/l
Uug/I
Uugfl
Uugfl
Uugn
Uug/I
Uugrt
Uug/I
Uugfl
Uugfl
.08 ug/l
Uug/I
Uugfl
Uugfl
1.2 ugi
Uugl
Uugl
Uugfl
.02 ug/l
Uugl
Uug/I
Uug/l
Uugfl
Uug/I
Uug/I
Uug/l
Uug/l
Uug/l
Uug/I
Uugl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uug/I
Uugfl
Uugfl
Uugfl
.05 ugfl
Uugfl
Uugfl
Uugfl
Uugfl
.1 ug/l
Uugfl
Uugfl
Uugfl
.2 ugfl
Uugfl
Uugfl
.8 ug/l
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
.06 ugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Limits
<.55
<.57
<.87
<.78
<.43
<.51
<.62
<.99
<1.27
<.62
< 72
<1
<.78
<.71
<.69
<.48
<.56
<.64
<.73
<.54
< 18.44
<.56
<.63
<.64
<.57
<1.27
<2.09
<.92
<.54
<.55
<1.44
<1.76
<2.41
<1.08
<.49
<.53
<.63
<.51
<.75
<1.01
<.84
<.55
<.73
<.68
<.43
<.73
<.3
<.6
i.52
<.39
i 17.27
<1
<.74
<.ll
<1.56
<.91
<.69
<.52
<.53
<.46
< 17.43
<.51
<1.25
<1.01
<.96
<1.01
<.53
<.52
<.72
<1.24
<.64
<.91
< 24.94
<.65
<.62
<.56
<.51
<.67
<.44
<.51
<.66
<.63
<.54
<.26
<.53
RPD Limit!
3 of 20 Pages
Sample Description
WG7496-3 (MTS) Mettiod Spike
WG7496-4 (MTSD) Method Spike Duplicate
Date Tested Test Parameter
SURR 1,2-DICHLOROETHANE-D4
SURR BROMOFLUOROBENZENE
SURR DIBROMOFLUOROMETHANE
SURR TOLUENE-DB
20-SEP-Ol 15:24 INTSTD 1,4-DICHLOROBENZENE-D4
INTSTD CHLOROBENZENE-DS
INTSTD FLUOROBENZENE
SURR l,2-DICHLOROETHANE-D4
SURR BROMOFLUOROBENZENE
SURR DIBROMOFLUOROMETHANE
SURR T0LUENE-D8
20-SEP-Ol 16:01 INTSTD 1,4-DICHL0R0BENZENE-D4
INTSTD CHLOROBENZENE-DS
INTSTD FLUOROBENZENE
SURR 1,2-DICHLOROETHANE-D4
SURR BROMOFLUOROBENZENE
SURR DIBROMOFLUOROMETHANE
SURR T0LUENE-D8
Measured Value Recoverv LimHs RPD
WG7496-1 (CC) Continuing Calibralion
159791 RESP
367518 RESP
585932 RESP
92.6 ugfl
98.6 ugfl
96.4 ugfl
100.2 ugfl
157899 RESP
367620 RESP
580927 RESP
86'
86
88
86-
86-
88-
•115
•118
•110
•115
•118
•110
Limits
21-SEP-Ol 09:03 INTSTD 1,4-DICHL0ROBENZENE-D4
INTSTD CHLOROBENZENE-DS
INTSTD FLUOROBENZENE
SURR
SURR
SURR
SURR
1,1,2,2-lblKACHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROPROPANE
BROMOFORM
CHLOROBENZENE
CHLOROFORM
CHLOROMETHANE
ETHYLBENZENE
TOLUENE
VINYL CHLORIDE
l,2-DICHLOROETHANE-D4
BROMOFLUOROBENZENE
DIBROMOFLUOROMETHANE
T0LUENE-D8
43 ugfl
46 ugfl
45 ugfl
46 ugfl
45 ugfl
49 ugfl
45 ugfl
48 ugfl
48 ugfl
49 ugfl
49 ugfl
165185 RESP
368587 RESP
606644 RESP
86.7 %Recov
91.8%Recov
89.5 %Recov
92.2 %Recov
90 %Recov
98.1 %Recov
89.4 %Recov
96 %Recov
95.9 %Reccv
98.1 %Recov
98.4 %Recov
80 •
80^
80 •
80 •
80 •
80 •
80^
80 •
80^
80^
80^
86^
86^
88 •
•120
•120
•120
•120
•120
•120
•120
•120
•120
•120
•120
•115
•118
•110
4 of 20 Pages
Sample
WG7496-2
Description
(LRB) Latioratory Reagent Blank
Date Tested Test Parameter Mea
21-SEP-Ol 09:34 INTSTD 1,4-DICHLOROBENZENE-D4
INTSTD CHLOROBENZENE-DS
INTSTD FLUOROBENZENE
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-1 ETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-THIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROP ANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,S-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
1-BUTANOL
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
2-METHYL-1-PR0PAN0L
2-NITROPROPANE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PEMTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
ALLYL CHLORIDE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CHLOROPRENE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
CYCLOHEXANONE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYL ACETATE
ETHYL ETHER
ETHYLMETHACRYLATE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYL ALCOHOL
ISOPROPYLBENZENE
M.P-XYLENE
METHACRYLONITRILE
METHYL IODIDE
METHYL METHACRYLATE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
PROPIONITRILE
PYRIDINE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
IhlHACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHL0ROPROPENE
TRANS-1.4-DICHLORO-2-BUTEN
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
sured Value Recoverv
155584 RESP
366899 RESP
589340 RESP
Uugfl
Uugfl
.07 ugfl
Uugfl
Uugfl
Uugfl
Uugfl
.8 ug/l
Uugfl
.7 ugfl
Uugfl
Uugfl
Uugfl
• lugfl
.2 ug/l
Uugfl
.07 ugfl
.lugfl
Uugfl
.lugfl
Uugfl
Uugfl
Uugfl
Uug/I
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
1.4 ugfl
Uugn
Uu^
Uugfl
.01 ugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
.08 ugfl
Uug/I
.5 ug/l
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
.8 ugfl
Uugfl
Uugfl
1.3 ugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
.05 ugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Limits
<.55
<.57
<.87
<.78
<.43
<.51
<.62
<.99
<1.27
*<.62
<.72
<1
<.78
<.71
<.69
<.48
<.56
<.64
<:.73
<.54
< 18.44
<.56
<.63
<.64
<.57
<1.27
<2.09
<.92
<.54
<.55
<1.44
<1.76
<2.41
<1.08
<.49
<.53
<.63
<.51
<.75
<1.01
<.84
<.55
<.73
<.68
<.43
<.73
<.3
<.6
<.S2
<.39
< 17.27
<1
<.74
<.11
<1.56
<.91
<.69
<.52
<.S3
*<.46
< 17.43
<.51
<1.25
<1.01
<.96
<1.01
*<.53
<.52
<.72
*<1.24
<.64
<.91
< 24.94
<.65
<.62
<.56
<.51
<.67
<.44
<.51
<.66
<.63
<.54
<.26
<.53
RPD Limits
5 Of 20 Pages
Sample Description
WG7496-3 (MTS) Method Spike
WG7496-4 (MTSD) Method Spike Duplicate
Date Tested Test Parameter
SURR l,2-DICHLOROETHANE-D4
SURR BROMOFLUOROBENZENE
SURR DIBROMOFLUOROMETHANE
SURR T0LUENE-D8
21-SEP-Ol 10:07 INTSTD 1,4-DICHL0R0BENZENE-D4
INTSTD CHL0R0BENZENE-D5
INTSTD FLUOROBENZENE
SURR 1,2-DICHLOROETHANE-D4
SURR BROMOFLUOROBENZENE
SURR DIBROMOFLUOROMETHANE
SURR T0LUENE-D8
21-SEP-Ol 10:39 INTSTD 1,4-DICHLOROBENZENE-D4
INTSTD CHLOROBENZENE-DS
INTSTD FLUOROBENZENE
SURR 1,2-DICHLOROETHANE-D4
SURR BROMOFLUOROBENZENE
SURR DIBROMOFLUOROMETHANE
SURR T0LUENE-D8
Measured Value Recoverv Limits RPD Limits
Samples in Work Group WG7496
153895 RESP
365907 RESP
582100 RESP
88.7 ugfl
100.1 ugfl
97.5 ugfl
100 ugfl
154516 RESP
360946 RESP
579049 RESP
86-115
86-118
88-110
86-115
86-116
88-110
L4554-1
L4563-3
L4554-2
L4569-1
L4554-3
L4569-3
L4554-4
L4560-10
L4561-1
L4560-13
L4561-2 L4561-3 L4561-4 L4563-1 L4563-2
6 of 20 Pages
Quality Control Report
Department: GC/Mass Spectrometry
28-OCT-02 WG7514 SW-846, 8260
Sample Description Date Tested Test Parameter Measured Value Recoverv Limits RPD Limits
WG7514-1 (CC) Continuing Calibration
Date Tested Test Parameter
24-SEP-01 10:17 INTSTD 1,4-DICHLOROBENZENE-D4
INTSTD CHLOROBENZENE-DS
INTSTD FLUOROBENZENE
SURR
SURR
SURR
SURR
1,1,2,2-1 b 1 HACHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,2-DICHLOROPROPANE
BROMOFORM
CHLOROBENZENE
CHLOROFORM
CHLOROMETHANE
ETHYLBENZENE
TOLUENE
VINYL CHLORIDE
l,2-DICHLOROETHANE-D4
BROMOFLUOROBENZENE
DIBROMOFLUOROMETHANE
T0LUENE-D8
Measured Value
49ugfl(g
47ugfl(g
47ugfl(g
47ugfl<g
53ugfl<g
53ugfl(g
47ugfl(g
46ugfl(g
Slugfl^g
51 ug/kg
47 ug/kg
Recovenr
150038 RESP
348928 RESP
563500 RESP
98.4 %Recov
94.6 %Recov
94.2 %Recov
93.2 %Recov
105%Recov
105%Recov
941 %Recov
92.3%Recov
101.e%Recov
101 %Recov
93.9 %Recov
94.9 %
99.1 %
100.4%
103.3 %
Limits
80 -120
80 -120
80-120
80 -120
80-120
80-120
80-120
80 -120
80-120
80 -120
80-120
7 of 20 Pages
Sample Description
WG7514-2 (LRB) Uboratory Reagent Blank
WG7514-3 (MTS) Method Spike
Reference Sample: WG7514-2
Date Tested Test Parameter Mea
24-SEP-01 10:49 INTSTD 1,4-DICHLOROBENZENED4
INTSTD CHLOROBENZENE-DS
INTSTD FLUOROBENZENE
1,1,1,2-ltmACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-lfclHACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBHOMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1.2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOflOPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
SURR l,2-DICHLOROETHANE-D4
SURR BROMOFLUOROBENZENE
SURR DIBROMOFLUOROMETHANE
SURR T0LUENE-D8
24-SEP-Ol 13:07 INTSTD 1,4-DICHL0R0BENZENE-D4
INTSTD CHLOROBENZENE-DS
INTSTD FLUOROBENZENE
1,1-DICHLOROETHENE
BENZENE
CHLOROBENZENE
TOLUENE
TRICHLOROETHENE
SURR 1,2-DICHLOROETHANED4
SURR BROMOFLUOROBENZENE
SURR DIBROMOFLUOROMETHANE
SURR T0LUENE-D8
sured Value
Uugflcg
Uugflig
Uugfljg
Uugfl<g
Uugflig
Uugflig
Uugflig
.4ugfl<g
Uugflcg
.4ugfl!g
Uugflcg
Uugflcg
Uugflcg
Uugflcg
U ug/kg
U ug/kg
Uugflcg
U ug/kg
U ug/kg
U ug/kg
Uugflcg
U ug/kg
Uugflcg
Uugflcg
Uugflcg
U ug/kg
Uugflcg
U ug/kg
8.5ugflcg
Uugflcg
Uugflcg
.01 ugflcg
Uugflcg
Uugflcg
Uugflcg
Uu^g
Uugflcg
U ug/kg
U ug/kg
U ug/kg
Uugflcg
U ug'kg
Uugflcg
Uu^g
Uugflcg
Uu^g
Uugflcg
Uugflcg
.03 ugflcg
Uugflcg
.6 ugflcg
Uugflcg
.03 uglcg
Uugflcg
Uugflcg
Uugflcg
.4 ugflcg
Uugflcg
Uugflcg
Uugflcg
Uugflcg
Uugflcg
.09 ugflcg
Uugflcg
Uugflcg
Uugflcg
Uugflcg
Uugflcg
Uugflcg
46 ugflcg
47 ugflcg
52 uglcg
50 ugflcg
46 ugflcg
Recoverv
145388 RESP
353394 RESP
552630 RESP
98.8 %
99.9 %
101.1 %
100.1 %
131717 RESP
323998 RESP
514605 RESP
92.9 %Recov
94.5 %Recov
103.5 %Recov
100.2 %Recov
92.5 %Recov
93.9%
102.1 %
96.4 %
100.8%
Limits
<.55
<.S7
<.e7
<.78
<.43
<.51
<.62
<.99
<1.27
<.62
<.72
<1
<.78
<.71
<.69
<.48
<.56
<.64
<.73
<.54
<.56
<.63
<.64
<.57
<1.27
<.54
<.55
<1.44
*<1.76
<2.41
<1.08
<.53
<.63
<.51
<.75
<1.01
<.84
<.55
<.73
<.68
<.43
<.73
<.3
<.52
<.39
<1
<.74
<.11
<.52
<.53
*<.46
<.51
<1.25
<.53
<.52
<.72
<1.24
<.64
<.65
<.62
<.56
<.51
<.67
<.44
<.S1
<.63
<.54
<.26
<.53
80-120
80 -120
80-120
80 -120
80-120
RPD Limits
8 Of 20 Pages
Sample Description Pate Tested Test Parameter Measured Value Recoverv Limits RPD Limits
WG7514-4 (MTSD) Method Spike Duplicate
-.•^ Relerence Sample: WG7514-3
Date Tested Test Parameter
24-SEP-0113:39 INTSTD 1,4-DICHL0R0BENZENE-D4
INTSTD CHLOROBENZENE-DS
INTSTD FLUOROBENZENE
SURR 1,2-DICHLOROETHANE-D4
SURR BROMOFLUOROBENZENE
SURR DIBROMOFLUOROMETHANE
SURR TOLUENE-DB
Measured Value Recoverv Limits
138418 RESP
341738 RESP
538291 RESP
98.8 %
101.5%
98.9 %
99.6 %
Samples in Work Group WG7514
L4560-1 L4560-2 L4560-4 L4560-5 L4560-6 L4560-7 L4560-8 L4560-9 L4560-11 L4560-12
9 Of 20 Pages
28-OCT-02
Sample
Quality Control Report
Department: Metals Anaiysis
W67524 SW-846, 6010
Description
WG7524-12 (OCSI 9) ICP Ind. Check Slandard
WG7524-13 (QCS07) ICP Ind. Check Standard
WG7524-14 (QCS7X10) ICP Ind. Check Standard (HIE 28-SEP-01 14:07
WG7524-15 (QC-P) QC Phosphorus Standard
WG7524-16 (LPC) Laboralory Peitomance C^^eck
WG7524-17 (CALB) Calibration Blank
WG7524-18 (LRB) Laboratory Reagent Blank
WG7524-19 (LFB) Ub Fortified Blank
Reference Sample: WG7524-18
Date Tested
28-SEP-01 14:02
28-SEP-01 14:04
28-SEP-01 14:07
28-SEP-01 14:10
28-SEP-0114:57
28-SEP-01 15:00
28-SEP-Ol 15:02
2B-SEP-01 15:05
Test Parameter
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COPPER
LEAD
MAGNESIUM
NICKEL
SELENIUM
ZINC
BARIUM
SILVER
ALUMINUM
PHOSPHORUS
ALUMINUM
ANTIMONY
BARIUM
BERYLUUM
CADMIUM
CALCIUM
CHROMIUM
COPPER
LEAD
MAGNESIUM
NICKEL
PHOSPHORUS
SELENIUM
SILVER
SODIUM
ZINC
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COPPER
LEAD
MAGNESIUM
NICKEL
PHOSPHORUS
SELENIUM
SILVER
SODIUM
ZINC
ALUMINUM
ANTIMONY
BARIUM
BERYLUUM
CADMIUM
CALCIUM
CHROMIUM
COPPER
LEAD
MAGNESIUM
NICKEL
PHOSPHORUS
SELENIUM
SILVER
SODIUM
ZINC
ALUMINUM
ANTIMONY
BARIUM
BERYLUUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
PHOSPHORUS
SELENIUM
SILVER
ZINC
Measured Value
1005 ugfl
991 ugfl
998 ugfl
988 ugfl
972 u^l
990 ug/l
971 ugfl
lOlSugl
1038ugfl
983 ug'i
508 ugfl
249 ugfl
5049 Uifl
4959 ugfl
4000 ug/l
1940 ugfl
2000 ugfl
2030uflfl
1980ugfl
1990 ugfl
1970 ugfl
1970 ugfl
1950 ugfl
1940 ugfl
2000 ugfl
10400ugfl
2000 ugfl
498 ugfl
20800 u^
1950 ugfl
5.8 ug/l
Uug/l
.7u^
2.5 ugfl
4.3 ugfl
Uugfl
.9 ugfl
Uugl
18 ugfl
1.8 ugfl
Uugfl
16 ugfl
Uugfl
1.1 ugfl
18 ugfl
3.6 ugfl
21 ugfl
15 ugfl
Uugfl
Uugfl
3.4 ugfl
66 ugfl
.7 ugfl
3.7 ugfl
7.1 ugfl
Uugfl
4.4 ugfl
5 ugfl
.2 ugfl
Uugl
384 ugfl
67 ugfl
950 ugfl
445 ugfl
484 ugfl
96 ugfl
184 ugfl
470 ugfl
465 ugi
484 ugfl
485 ugfl
1010ugfl
415ugfl
47 ugfl
585 ugfl
Recoverv
101 %Recov
99 %Recov
100%Recov
99 %Recov
97%Recov
99 ^'oflecov
97 %Recov
102 %Recov
104 %Recov
98 %Recov
102 %Recov
100%Recov
tot %Recov
99 %Recov
100 %Recov
97 %Recov
100 %Recov
101.5%Recov
99 %Recov
99.5 %Recov
98.5 %Recov
98.5 %Recov
97.5 %Recov
97 %Recov
100%Recov
l04%Recov
100 %Recov
99.6 %Recov
104%Recov
97.5 %Recov
92.9 %Recov
86 %Recov
96.8 %Recov
96 %Recov
90.3 %Recov
93.9 %Recov
92.3 %Recov
95.4 %Reeov
96.1 %Recov
100.5 %Recov
83 %Recov
94%Recov
103.7 %Recov
Limits
95-110
95-110
95-110
95-110
95-110
95-110
95-110
95-110
95-110
95-110
95-110
95-110
95-110
95-110
95-105
95-105
95-105
95-105
95-105
95-105
95-105
95-105
95-105
95 -105
95-105
95-105
95-105
95-105
95-105
95-105
<25
<50
<1
*<2
*<2
<10
<5
<2
<25
*<1
<10
<60
<60
<3
*<10
<4
<25
<50
<1
<2
*<2
*<10
<5
*<2
<25
*<1
<10
<60
<60
<3
*<10
*<4
75 -125
75 -125
75-125
75-125
75-125
75-125
75 -125
75-125
75 -125
75 -125
75 -125
75-125
75 -125
RPD Limits
10 Of 20 Pages
Sample Description
WG7524-20 (LFBD) Ub Fortified Blank Duplicate
Relerence Sample: WG7524-18
WG7524-21 (MS) Matnx Spike
Relerence Sample: L4584-6
WG7524-22 (MSD) Matrix Spike Duplicate
Reference Sample: L4584-6
WG7524-16 (LPC) Laboralory Peiloimance Check 2B-SEP-0115:44
WG7524-17 (CALB) Calibralion Blank
WG7524-17 (CALB) Calibration Blank
Date Tested
28-SEP-01 15:08
28-SEP-Ol 15:14
28-SEP-Ol 15:17
2B-SEP-01 15:44
28-SEP-Ol 15:47
02-OCT-OI 14:42
Test Parameter
ALUMINUM
ANTIMONY
BARIUM
BERYU-IUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
PHOSPHORUS
SELENIUM
SILVER
ZINC
ALUMINUM
BARIUM
BERYLUUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
BARIUM
BERYU.IUM
CADMIUM
CHROMIUM
LEAD
SILVER
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COPPER
LEAD
MAGNESIUM
NICKEL
PHOSPHORUS
SELENIUM
SILVER
SODIUM
ZINC
ALUMINUM
ANTIMONY
BARIUM
BERYUJUM
CADMIUM
CALCIUM
CHROMIUM
COPPER
LEAD
MAGNESIUM
NICICEL
PHOSPHORUS
SELENIUM
SILVER
SODIUM
ZINC
ALUMINUM
ANTIMONY
BARIUM
BERYUJUM
CADMIUM
CALCIUM
CHROMIUM
COPPER
LEAD
MAGNESIUM
NICKEL
PHOSPHORUS
SELENIUM
SILVER
SODIUM
ZINC
Measured Value
980 ugfl
465 ugfl
488 ugfl
99 ugfl
186 ugfl
471 ugfl
468 ugfl
485ugfl
490 ugfl
959 ugfl
408 ugfl
47 ugfl
538 ugfl
958 ugfl
483 ugfl
97 ugfl
186 ugfl
465 ugfl
461 u^
556 ugfl
45 ugfl
490 ugfl
100 ugfl
189 ugfl
474 ugfl
473 ugfl
48 ugfl
4000 ugfl
1940 ugfl
2000 ugfl
2040ugfl
2000 ugfl
2010 ugfl
1980 ugfl
1970ugfl
1970 ugfl
1930 ugfl
2010ugfl
10400 ugfl
1910ugfl
502 ugfl
20400 ugfl
1960 ugfl
Uugfl
Uugfl
2.5 ugfl
2.7 ugfl
7.7 ugfl
1.2 ugfl
2.9 ugfl
Uugfl
Uugfl
7 ugfl
Uu^
14 ugfl
Uugfl
1.3 ugfl
30 ugfl
1.5 ugfl
Uugfl
Uugfl
1.7 ugfl
.9 ugfl
Uugfl
Uugfl
Uugfl
2.8 ugfl
6.8 ugfl
1.2 ugfl
2.3 ugfl
Uugfl
SO ugfl
1 ugfl
8.4 ugfl
Uugfl
Recovery
95.9 %Recov
90 %Recov
97.6 %Recov
99 %Recov
91.3%Recov
94.1 %Recov
92.9 %Recov
95.6 %Recov
97.1 %Recov
95.4%Recov
81.6%Recov
94%Recov
94.3%Recov
94.3 %Recov
96.5%Recov
96.9 %Recov
88.7 %Recov
92.9 %Recov
91.5 7oRecov
111.2%Recov
86.8 %Recov
97.9 %Recov
99.9 %Recov
90.2 %Recov
94.7%Recov
93.9 %Recov
92.8 %Recov
100%Recov
97 %Recov
100%Recov
102 %Recov
100 %Recov
100.5 %Recov
99 %Recov
98.5 %Recov
98.5 %Recov
96.5 %Recov
100.5 %flecov
104%Recov
95.5%Recov
100.4 %Recov
102%Recov
98 %Recov
Limits
75-125
75-125
75 -125
75 -125
75-125
75-125
75-125
75 -125
75-125
75-125
75-125
75-125
75 -125
75 -125
75 -125
75 -125
75 -125
75 -125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75 -125
95-105
95-105
95-105
95-105
95-105
95-105
95-105
95-105
95-105
95 -105
95-105
95 -105
95 -105
95 -105
95-105
95-105
<25
<50
*<1
*<2
• <2
<10
<5
<2
<25
*<1
<10
<60
<60
<3
*<10
<4
<25
<50
*<1
<2
<2
*<10
<5
*<2
<25
*<1
<10
<60
<60
<3
<10
<4
RPD
3.2 %RPD
4.5 %RPD
O.B %RPD
3.1 %RPD
1.1 %RPD
0.2 %RPD
0.6 %RPD
0.2 %RPD
1.0%RPD
5.2 %RPD
1.7%RPD
0.0 %RPD
9.5 %RPD
1.4%RPD
3.0 %RPD
1.7%RPD
1.9%RPD
2.6 %RPD
6.7 %RPD
Limits
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
Samples in Woric Group WG7524
— L4542-1 L4542-2 L4542-3 L4542-4 L4542-5 L4562-1 L4584-6 L4560-10
11 Of 20 Pages
28-OCT-02
Sample
Quality Control Report
Department: Metals Analysis
WG7527 SW-846, 6010
Description
V/G7527-1 (QCS19) ICP Ind. Check Standard
WG7527-2 (QCS07) ICP Ind. Check Standard
Date Tested
27-SEP-Ol 11:11
27-SEP-01 11:14
WG7527-3 (QCS7X10) ICP Ind. Check Standard (Hij 27-SEP-Ol 11:17
WG7527-4 (LPC) Uboratory Perfomiance Check 27-SEP-Ol 12:05
WG7527-5 (CALB) Calibration Blank 27-SEP-Ol 12:08
WG7527-6 (LRB) Uboratory Reagent Blank 27-SEP-Ol 12:11
WG7527-7 (LFB) Ub Fortified Blank
Reference Sample: VifG7527-6
27-SEP-Ol 12:14
WG7527-8 (LFBD) Ub Fortilied Blank Duplicate 27-SEP-01 12:17
Reterence Sample: WG7527-6
WG7527-9 (MS) Matrix Spike
Relerence Sample: L4S30-2
WG7527-10 (MSD) Matrix Spike Duplicate
Relerence Sample: L4530-2
27-SEP-Ol 12:23
27-SEP-Ol 12:26
WG7527-4 (LPC) Laboratory Pertormance Check 27-SEP-Ol 12:55
Test Parameter
BERYUIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
BARIUM
SILVER
ALUMINUM
ALUMINUM
BARIUM
BERYLUUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ALUMINUM
BARIUM
BERYLUUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ALUMINUM
BARIUM
BERYUIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ALUMINUM
BARIUM
BERYLUUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ALUMINUM
BARIUM
BERYUIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ALUMINUM
BARIUM
BERYUIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ALUMINUM
BARIUM
BERYLUUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ALUMINUM
BARIUM
BERYLUUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
Measured Value Recoverv Limits
1010 ug/g
996 ug/g
998 ug/g
985 ug/g
1037 ug/g
509 ug/g
252 ug/g
5001 ug/g
4040 ugfl
1990ugfl
2030ugfl
1980ugfl
1990ugfl
1980 ug/l
2010 ugfl
499 ugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uugfl
Uug/I
53 ugfl
Uugfl
22 ugfl
Uugfl
Uugfl
4.9 u^
2 ugfl
1.8 ugfl
72 u^
.8 ugfl
966 ugfl
482 ugfl
95 ugfl
172 u^
463 ugfl
491 ugfl
437 ugfl
46 ugfl
953 ugfl
488 ugfl
95 ugfl
172 ugfl
465 ugfl
464 ugfl
489 ugfl
46 ugfl
17600 ug/g
196 ug/g
11 ug/g
18 ug/g
65 ug/g
55 ug/g
46 ug/g
Uug/g
13900 ug/g
184 ug/g
10 ug/g
17 ug/g
58 ug/g
54 ug/g
45 ug/g
Uug/g
4090 ugfl
1990ugfl
2050ugfl
2050 ugfl
2020 ugfl
2030 ugfl
1990 ugfl
511 ugfl
101 %Recov
100%Recov
100%Recov
99 %Recov
104%Recov
102 %Recov
101 %Recov
100%Recov
101 %Recov
99.5 %Recov
101.5 %Recov
99 %Recov
99.5 %Recov
99 %Recov
100.5 %Recov
99.8 %Recov
105
105
105
105
105
105
105
105
105
105
105
105
105
105
95-105
95-105
<25
<1
<2
<2
<5
<25
<60
<3
<25
<1
<2
*<2
<5
<25
*<60
<3
94.4 %Recov
96.4 %Recov
95 %Recov
83.6 %Recov
92.2 %Recov
97.8 %Recov
72.9%Recov •
90.4 %Recov
93.1 %Recov
97.6 %Recov
95 %Recov
83.6 %Recov
92.6 %Recov
92.4 %Recov
83.3 %Recov
90.4 %Recov
125
125
125
125
125
125
75-125
75 -125
125
125
125
125
125
125
125
125
1503.5 %Recov «75-125
81.6%Recov 75-125
87.2%Recov 75-125
74.6%Recov * 75-125
70.5%Recov * 75-125
78.2%Recov 75-125
79.3%Recov 75-125
0%Recov *75-125
4897.3 %Recov
63.6 %Recov
82 %Recov
73.4 %Recov
61 %Recov
79.8 %Recov
809 %Recov
0 %Recov
102.3%Recov
99.5 %Recov
102.5%Recov
102.5%Recov
101 %Recov
101.5 %Recov
99.5 %Recov
102.2 %Recov
* 75-125
* 75-125
75-125
* 75-125
* 75-125
75 -125
75 -125
* 75 -125
95 -105
95 -105
95 -105
95 -105
95 -105
95 -105
95 -105
95 -105
RPD Limits
14%RPD
1.2%RPD
0.0 %RPD
0.0 %RPD
0.4 %RPD
5.7 %RPD
13.3 %RPD
0.0 %flPD
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
106.0 %RPD
24.8 %RPD
6.1 %RPD
1.6%RPD
144 %RPD
2.0 %RPD
2.0 %RPD
0.0 %RPD
*0
*0
0
0
0
0
0
0
12 of 20 Pages
Sample Description
WG7527-5 (CALB) Calibration Blank
WG7527-6 (LRB) Laboratory Reagent Blank
WG7527-7 (LFB) Ub Fortilied Blank
Relerence Sample: WG7527-6
V^G7527-8 (LFBD) Ub Fortilied Blank Duplk:ate
Relerence Sample: WG7527-6
WG7527-11 (MS) Matrix Spike
Relerence Sample: L4560-9
WG7527-12 (MSO) Matnx Spike Duplicate
Reference Sample: L4560-9
WG7527-4 (LPC) Laboralory Performance Check 27-SEP-Ol 13:46
WG7527-5 (CALB) Calibration Blank
WG7527-6 (LRB) Laboratory Reagent Blank
WG7527-7 (LFB) Lab Fortified Blank
Relerence Sample: WG7527-6
Date Tested
27-SEP-01 12:58
27-SEP-Ol 13:01
27-SEP-Ol 13:04
27-SEP-01 13:07
27-SEP-Ol 13:13
27-SEP-Ol 13:16
27-SEP-Ol 13:46
27-SEP-Ol 13:49
27-SEP-Ol 13:51
27-SEP-Ol 13:54
Test Parameter
ALUMINUM
BARIUM
BERYLUUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ALUMINUM
BARIUM
BERYUIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ALUMINUM
BARIUM
BERYLUUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ALUMINUM
BARIUM
BERYUIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ALUMINUM
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ALUMINUM
BARIUM
BERYLUUM
CADMIUM
CHROMIUM
LEAO
SELENIUM
SILVER
ALUMINUM
BARIUM
BERYLUUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
Measured Value
2.7 ugfl
Uugl
.085 ugfl
2.5 ugfl
Uugfl
Uugfl
46 ugfl
Uugfl
20 ugfl
Uugfl
Uugfl
Uugfl
Uugfl
3.6 ugfl
6.5 ugfl
Uugfl
963 ugfl
482 ugfl
95 ugfl
175 ugfl
460 ugfl
469 ugfl
515 ugfl
45 ugfl
934 ugfl
480 ugfl
95 ugfl
177 ugfl
460 ugfl
455 ugfl
450 ugfl
45 ugfl
15400 ug'g
165 u^g
11 ug/g
19 ug/g
60 ug/g
52 ug/g
50 ug/g
Uug/g
13200 ug/g
165 ug/g
11 ug/g
17 ug/g
58 ug/g
51 ug/g
51 ug/g
Uug/g
4120 ugi
2010ugfl
2080 ugfl
2050 ugfl
2040 ugfl
2050 ugfl
2020 ugi
516 ugfl
1.9 ugfl
Uugfl
.2 ugfl
3.3 ugfl
Uugfl
13ugfl
59 ugfl
Uugfl
18u^
Uugfl
Uugfl
Uugfl
Uugfl
Uugl
33 ugfl
Uugfl
950 u^
479 ugfl
95 ugfl
178 U£^
462 ugfl
441 ugfl
489 ugfl
46 ugfl
Recovery
94.1 %Recov
96.4%Recov
95%Recov
85.1 %Recov
91.6%Recov
93.4%Recov
88.5%Recov
88.4%Recov
91.2%Recov
96 %Recov
95 %Recov
86.1 %Recov
91.6%Recov
90.6 %Recov
75.5 %Recov
88.4 %Recov
1086.3 %Recov
78.8 %Recov
79.2 %Recov
71.9%Recov
70.8%Recov
69.3%Recov
58.4 %Recov
0 %Recov
613.5 %Recov
81 %Recov
81.4%Recov
66%Recov
69.6 %Recov
69.7%Recov
71.8%Recov
0 %Recov
103%Recov
100.5 %Recov
104 %Recov
102.5 %Recov
102%Recov
102.5 %Recov
101 %Recov
103.2 %Recov
92.8 %R8C0V
95.8 %Recov
95 %Reeov
86.6 %Recov
92 %Recov
87.8 %Recov
83.3 %Recov
904 %Recov
Limits
<25
<1
<2
*<2
<5
<25
<60
<3
<25
<1
<2
<2
<5
<25
<60
<3
75-125
75 -125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75 -125
75 -125
75 • 125
• 75-125
75 -125
75 -125
« 75-125
.75-125
*75-125
*75-125
* 75-125
• 75-125
75-125
75-125
• 75-125
• 75-125
• 75 -125
• 75 -125
• 75 -125
95-105
95 -105
95-105
95-105
95-105
95-105
95 -105
95-105
<25
<1
<2
• <2
<5
<25
<60
<3
<25
<1
<2
<2
<5
<25
<60
<3
75 -125
75 -125
75 -125
75-125
75 -125
75 -125
75-125
75 -125
RPD
3.1 %RPD
0.4 %RPD
0.0 %RPD
1.2%RPD
ao %RPD
3.0 %RPD
15.9 %RPD
oo %RPD
55.6 %RPD
2.8 %RPD
2.7 %RPD
8.6 %RPD
1.7%RPD
06 %RPD
4.9 %RPD
0.0 %RPD
Limits
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
• 0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
13 of 20 Pages
Sample Description
WG7527-8 (LFBD) Ub Fortified Blank Duplicate
Relerence Sample: V^G7527-6
WG7527-13 (MS) Matnx Spike
Relerence Sampie: L4584-10
WG7527-14 (MSD) Matrix Spike Duplicate
Reference Sampie: L4584-10
WG7527-4 (LPC) Laboratory Perfomiance Check
WG7527-5 (CALB) Calibration Blank
Samples in Work Group WG7527
L4530-2 L4530-3 L4530-6
L4560-9 L4584-2 L4584-3
L4584-10 L4584-12
Date Tested
27-SEP-Ol 13:57
27-SEP-Ol 14:03
27-SEP-Ol 14:06
27-SEP-Ol 14:12
27-SEP-Ol 14:15
L4530-7
L4584-4
Test Parameter
ALUMINUM
BARIUM
BERYUIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ALUMINUM
BARIUM
BERYUJUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ALUMINUM
BARIUM
BERYUIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ALUMINUM
BARIUM
BERYUIUM
CADMIUM
CHROMIUM
LEAD
SEUENIUM
SILVER
ALUMINUM
BARIUM
BERYLUUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
L45304 L4530-9
L4584-5 L4584-7
Measured Value
929 ugfl
479 ugfl
96 ugfl
176 ugfl
462 ugfl
452 ugfl
502 ugfl
46 ugfl
11000 ug/g
135 ug/g
Uug/g
18 ug/g
59 ug/g
55 ug/g
49 ug/g
Uug/g
11000 ug/g
134 ug'g
Uug/g
18 ug'g
59 ug/g
56 ug'g
48 ug/g
Uug/g
4070 ugfl
2010 ugfl
2070 ugfl
2040 ugfl
2020 ugfl
2020ugfl
2020 ugfl
512 ugfl
5.4 ugfl
Uugfl
.2 ugfl
.8 ugfl
.7 ugfl
5.3 ugfl
13 ugfl
.5 ug/l
L4560-3
L4584-8
Recoverv
90.7%Recov
95.8%Recov
96 %Recov
85.6 %Recov
92 %Recov
90 %Recov
85.9 %Recov
90.4 %Recov
106.5 %Recov
73.7 %Recov
78.4 %Recov
66.8 %Recov
65.8 %Recov
66.5 %Recov
67.9 %Recov
0 %Recov
106.7 %Recov
72.3 %Recov
78.6 %Recov
66.9 %Recov
65.9 %Recov
68.1 %Recov
66.5%Recov
0%Recov
101.8 %Recov
100.5 %Recov
103.5 %Hecov
102%Recov
101 %Recov
101 %Recov
101 %Recov
102.4 %Recov
L4560-5
L4584-9
Limits
75 -125
75 -125
75 -125
75-125
75 -125
75-125
75 -125
75-125
75 -125
• 75-125
75-125
• 75-125
• 75-125
• 75-125
• 75-125
• 75-125
75-125
* 75 -125
75 -125
• 75-125
• 75-125
• 75-125
• 75-125
• 75-125
95-105
95-105
95-105
95-105
95-105
95-105
95-105
95-105
<25
<1
<2
<2
<5
<25
<60
<3
L4560-6
L4560-11
RPD
2.3 %RPD
OO %RPD
1.0 %RPD
1.2%RPD
0.0 %RPD
2.5 %RPD
3.1 %RPD
ao %RPD
0.2 %RPD
1.9 %RPD
0.3 %RPD
0.1 %RPD
0.2 %RPD
2.4 %RPD
2.1 %RPD
0.0 %RPD
Limits
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
0-20
L4560-8
L4560-12
14 Of 20 Pages
Quality Control Report
Department: Wet Lab
28-OCT-02
Sample Description
WG7474-1 (QCS) Independent Check Standard
WG7474-2 (DUP) Duplicate
Reterence Sample: L4560-I2
Samples in Woric Group WG7474
Date Tested
18-SEP-01 14:24
18-SEP-0114:24
W67474 SW 8'
Test Parameter
PH
PH
16, 9045
Measured Value
7.02
8.41
Recoverv Limits
100.3 %Reeov 80-120
RPD
1.1 %RPD
Limits
0-20
L4560-3 L4560-5 L4560^ L4560-8 L4560-9 L4560-11 L4560-12
15 of 20 Pages
28-OCr-02
Sample Description
VI/G7517-1 (ICV) Initial Calibration Verification
WG7517-2 (QCS) Independent Check Standard
WG7517-3 (LRB) Uboratory Reagent Biank
WG7517-4 (LFB) Lab Fortified Blank
Reterence Sample: V1/G7517-3
WG7517-5 (LFBD) Lab Fortified Blank Duplcate
Reterence Sample: WG7517-3
WG7517-6 (MS) Matrix Spike
Relerence Sample: L4560-9
WG7517-7 (MSD) Matrix Spike Duplicate
Relerence Sample: L4560-9
WG7517-8 (CCV) Coritinuing Cal Verificatiori
Samples in Work Group WG7517
Quality Control Report
Department: lon Chromatography
WG7517 sw 846, 9056
Date Tested
21-SEP-Ol 08:30
21-SEP-Ol 08:47
21-SEP-Ol 09:05
21-SEP-Ol 09:22
21-SEP-Ol 09:40
21-SEP-Ol 11:25
21-SEP-Ol 11:42
21-SEP-Ol 12:35
Test Parameter
NITRATE-N
NITRITE-N
NrrRATE-N
NR-RATE-N
NITRITEN
NITRATE-N
NITRITE-N
NITRATE-N
NITRITE-N
NITRATEN
NITRITE-N
NITRATE-N
NITRITE-N
NITRATE-N
NITRITE-N
Measured Value
1.82 mg/l
1.85 mg/l
2.11 mg/l
Umg/1
Umg/I
4.16 mg/l
4.21 mg/l
4.23 mg/l
4.28 mg/l
42.5 mg/l
40.2 mg/l
44.2 mgfl
41.7 mgfl
101 mgfl
101 mgfl
Recovery
91 %Recov
92.5 %Recov
93.4%Recov
104%Recov
105.3 %Recov
105.8 %Recov
107%Recov
105.2 %Recov
100.5 %Recov
109.5%Recov
104.3 %Recov
101 %Recov
101 %Recov
Limits
60 -120
80-120
80 -120
<.01
<.01
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
RPD
1.7%RPD
1.6%RPD
4.0 %RPD
3.7 %RPD
Limits
0-20
0-20
0-20
0-20
L4560-3 L4560-5 L4560-6 L4560-8 L4560-9 L4560-11 L4560-12
16 of 20 Pages
28-OCT-02
Sample
WG7542-1
WG7542-2
WG7542-3
WG7542-4
Description
(ICV) Initial Calibration Verillcation
(QCS) Independent Check Slandard
(LRB) Uboratory Reagent Blank
(U^B) Lab Fortilied Blank
Relerence Sample: WG7542-3
WG7542-5 (LFBD) Ub Fortified Blank Duplicate
Relerence Sample: V^G7542-3
WG7542-6 (MS) Matrix Spike
Relerence Sample: L4530-2
WG7542-7 (MSD) Matrix Spike Duplicate
Relerence Sample: L4530-2
WG7542-12 (CCV) Continuing Cal Verillcation
VI;G7542-12 (CCV) Continuing Cal Verilicalion
WG7542-8 (MS) Matrix Spike
Reference Sample: L4560-9
WG7542-9 (MSD) Matrix Spike Duplicate
Reference Sample: L4560-9
WG7542-12 (CCV) Continuing Cat Verification
WG7542-10 (MS) Matrix Spike
Reference Sample: L4584-10
WG7542-11 (MSD) Matrix Spike Duplicate
Reference Sample: L4584-10
WG7542-12 (CCV) Continuing Cal Verification
WG7542-12 (CCV) Continuing Cal Verificatior
Samples in Work Group WG7542
Quality Control Report
Department: Atomic Absorption
W67542 SW-846, 7060
Date Tested
28-SEP-Ol 09:56
28-SEP-01 10:03
28-SEP-Ol 10:16
28-SEP-Ol 10:23
28-SEP-Ol 10:29
28-SEP-Ol 10:46
28-SEP-Ol 10:53
28-SEP-Ol 11:24
28-SEP-01 12:35
28-SEP-Ol 12:48
28-SEP-Ol 12:54
28-SEP-Ol 13:48
28-SEP-Ol 14:36
28-SEP-Ol 14:42
28-SEP-Ol 14:59
28-SEP-Ol 15:19
Test Parameter
ARSENIC
ARSENIC
ARSENIC
ARSENIC
ARSENIC
ARSENIC
ARSENIC
ARSENIC
ARSENIC
ARSENIC
ARSENIC
ARSENIC
ARSENIC
ARSENIC
ARSENIC
ARSENIC
Measured Value
52 ugfl
21 ugfl
Uugfl
49 ugfl
48 ug/l
61 ug/g
58 ug'g
49 ugfl
48 ugfl
53 ug/g
51 ug/g
49 ugfl
47 ug/g
48 ug/g
47 ugfl
46 ugfl
Recovery
104 %Recov
105 %Recov
98 %Recov
98 %Recov
107%Recov
105.4 %Recov
98 %Recov
96 %Recov
104.1 %Recov
98 %Recov
102.5 %Recov
94 %Recov
92 %Recov
Limits
80-120
80-120
<1.5
80-120
80-120
80 -120
80-120
80-120
80-120
80 -120
103%Recov 80-120
80-120
80 -120
103.2 %Hecov 80-120
80-120
80-120
RPD Limits
2.1 %RPD 0-20
1.5%RPD 0-20
1.1%RPD 0-20
0.7 %RPD 0 • 20
L4530-2
L4560-9
L4584-10
L4530-3
L4584-2
L4584-12
L4S30-6
L4584-3
L4530-7
L4584-4
L4530-8
L4584-5
L4530-9
L4584-7
L4560-3
L4584-8
L4560-5
L4584-9
L4560-6
L4560-11
L4560-8
L4560-12
17 Of 20 Pages
28-OCT-02
Sample Description
WG7559-1 (ICV) Initial Calibration Verifk:atio(i
WG7559-2 (LRB) Laboratoiy Reagent Blank
WG7559-3 (LFB) Ub Fortified Blank
Reterence Sample: WG7S59-2
WG7559-4 (LFBD) Lab Fortilied Blank Duplicate
Reference Sample: WG7559-2
WG7559-5 (QCS) Independent Check Standard
WG7559-10 (CCV) Continuing Cal Verification
WG7559-10 (CCV) Continuing Cal Verification
WG7559-6 (MS) Matrix Spike
Reference Sample: L4560-8
WG7559-7 (MSD) Matrix Spike Duplicate
Relerence Sample: L4560-8
WG7559-10 (CCV) Continuing Cal Venfication
WG7559-1 (ICV) Initial Calibration Verification
VI/G7559-5 (QCS) Independent Check Standard
WG7559-10 (CCV) Continuing Cal Verification
WG7559-B (MS) Matrix Spike
Relererice Sample: L4584-7
VI^G7559-9 (MSD) Matrix Spike Duplicate
Reference Sample: L4584-7
WG7559-10 (CCV) Continuing Cal Verification
WG7559-10 (CCV) Continuing Cal Verificaiion
Samples in Work Group WG7559
L4530-2
L4560-9
L4584-10
L4530-3
L4584-2
L4584-12
L4530-6
L4584-3
Quality Control Report
Department: Atomic Absorption
WG7559 SW-846, 7471A
Date Tested
03OCT-01 09:54
03OCT-01 09:57
03-OCT-01 09:59
03-OCT-01 10:02
03-OCT-01 10:05
03-OCT-01 10:23
03-OCT-01 10:52
03-OCT-01 11:04
03-OCT-01 11:07
03-OCT-01 11:21
03-OCT-Ol 11:45
03-OCT-01 11:48
03-OCT-Ol 12:14
03-OCT-Ol 12:26
03-OCT-Ol 12:28
03-OCT-Ol 12:43
03-OCT-Ol 12:57
L4530-7
L4584-4
Test Parameter
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
Measured Value Recoverv Limits
5.2 ugfl 104 %Recov 80 -120
U ugfl < .24
4.3 ugfl 107.8 %Recov 80-120
4.4 ugfl
Uugfl
5.4 ugi
5.3 ugfl
.47 ug/g
.43 ug/g
5.6 ugfl
5.1 ugfl
10 ugfl
5 ugfl
.43 ug/g
.44 ug/g
5.7 ugfl
5.7 ug/l
110.1 %Recov 80-120
110%Recov 80-120
108%Recov 80-120
106%Recov 80-120
119%Recov 80-120
112.1 %ReCOV 80-120
l12%Recov
102%Recov
100%Recov
100%Recov
106.9 %Recov
80-120
80-120
80-120
80-120
80-120
109.5 %Recov 80-120
U4%Recov 80-120
114%Recov 80-120
RPD Limits
21%RPD 0-20
6.0 %flPD 0-20
2.4 %RPD 0-20
L4530-8
L4584-5
L4530-9
L4584-7
L4560-3
L45B4-8
L4560-5
L4584-9
L4560-6
L4560-11
L4560-8
L4560-12
18 of 20 Pages
28-OCT-02
Sample Description
WG7601 -1 (ICV) Initial Calibration Verification
WG7601-2 (LRB) Uboraloiy Reagent Blank
WG7601 -3 (LFB) Lab Fortilied Blank
Reference Sample: WG7601 -2
WG7601 -4 (LFBD) Ub Fortified Blank Duplcate
Reference Sample: WG7601-2
WG7601 -5 (QCS) Independent Check Standard
WG7601-12 (CCV) Continuing Cal Verification
WG7601-6 (MS) Matrix Spike
Reference Sample: L4584-6
WG7601 -7 (MSD) Matnx Spike Duplicate
Reference Sample: L4584-6
WG7601-12 (CCV) Continuing Cal Verification
WG7601-8 (MS) Matrix Spike
Refererice Sample: L4595-5
WG7601-9 (MSD) Matrix Spike Duplicate
Relerence Sample: L4595-5
WG7601-12 (CCV) Conlinuing Cal Verification
WG7601-10 (MS) Matnx Spike
Reference Sample: L4595-11
WG7601 -11 (MSD) Matrix Spike Duplicate
Reference Sample: L4595-11
WG7601-12 (CCV) Conlinuing Cal VenficaOon
Samples in Work Group WG7601
Date Tested
10-OCT-01 10:21
10-OCT-01 10:24
10-OCT-01 10:26
10-OCT-01 10:29
lOOCT-01 10:32
10-OCT-01 10:52
10-OCT-0111:13
lO-OCT-01 11:16
10-OCT-Ol 11:21
lO-OCT-01 11:35
10-OCT-Ol 11:38
10-OCT-Ol 11:50
10-OCT-Ol 11:59
10-OCT-Ol 12:02
lO-OCT-01 12:19
Quality Control Report
Department: Atomic Absorption
WG7601 SW-846, 7470A
Test Parameter
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
MERCURY
Measured Value
5 ugfl
Uugfl
4u^l
3.9 ugfl
10 ug/l
5.2 ugfl
4.1 ugfl
4 ug/l
5.1 ugfl
3.9 ugfl
4.1 ugfl
5.5 u^
4 ugfl
4.1 ugfl
5.4 ugfl
Recovery
100 %Recov
99.8%Recov
98.6 %flecov
100%Recov
104 %Recov
105.4 %Recov
103.6 %Recov
102%Recov
100.3 %Recov
105%Recov
110%Recov
100%Recov
101.5 %Recov
108 %Recov
Limits
80-120
<.24
80-120
80-120
80 -120
80-120
60 -120
80-120
80-120
80 -120
80-120
80-120
80-120
80-120
80-120
RPD
1.2 %flPD
1.7%RPD
4.6 %RPD
1.5 %RPD
Limits
0-20
0-20
0-20
0-20
L4584-6
L4599-2
L4595-1
L4560-10
L4595-2
L4595-10
L4595-3
L4595-11
L4595-4
L4595-12
L4595-5 L4595-6 L4595-7 L4595-8 L4595-g
19 of 20 Pages
28-OCT-02
Sample
V/G7675-1
WG7675-2
WG7675-3
WG7675-4
Description
(ICV) Inifial Calibration Verification
(QCS) Independent Check Standard
(LRB) Uboratory Reagent Blank
(LFB) Lab Fortified Blank
Refererice Sample: WG7675-3
WG7675-5 (LFBD) Lab Fortilied Blank Duplicate
Refererice Sample: WG7675-3
WG7675-6 (MS) Matrix Spike
Reference Sample: L4631-10
WG7675-8 (CCV) Continuing Cat Veriticaliori
WG7675-7 (MSD) Matrix Spike Duplicate
Reference Sample: L4631-10
WG7675-8 (CCV) Continuing Cal Verification
Samples in Work Group WG7675
Quality Control Report
Department: Atomic Absorption
WG7675 SW-846, 7060
Date Tested
26OCT-01 13:52
26OCT-01 13:59
26-OCT-Ol 14:12
26-OCT-01 14:19
26-OCT-Ol 14:25
26-OCT-01 15:06
26-OCT-Ol 15:26
26-OCT-Ol 15:33
26-OCT-Ol 15:57
Test Parameter
ARSENIC
ARSENIC
ARSENIC
ARSENIC
ARSENIC
ARSENIC
ARSENIC
ARSENIC
ARSENIC
Measured Value Recovery Limits
51 ugfl 102%Recov 80-120
RPD Limits
20 ugfl
.8 ugfl
23 ugfl
23 ugfl
22 ugfl
46 ugfl
22 ugfl
45 ug/l
100%Recov 80-120
<1.5
89.6 %Recov 80 -120
87.4%Recov 80-120
84.5 %Recov 80 -120
92 %Recov 80 -120
85%Recov 80-120
90%Recov 80-120
2.5%RPD 0-20
0.6 %RPD 0-20
L4584-6 L4599-2 L4560-10 L4631-10
20 Of 20 Pages