DSHW-2009-012658 - 0901a0688013f2ad

BEACON Report No. EM1715
rtcCEIVED
m 0 4 2005
UTAH DIVISION OF
'^|^& HAZARDOUS WASTE
PASSIVE SOIL-GAS SURVEY
ATK THIOKOL PROPULSION
CORINNE, UT
Prepared for
ATK Thiokol, Inc.
PO Box 707 MS T12A
Brigham City, UT 84302
by
flCON
ENVIRONMENTAL
SERVICES, INC.
Beacon Environmental Services, Inc.
323 Williams Street
Suite D
Bel Air, MD 21014
November 10, 2004
Applying Results from Soil-Gas Surveys
The utility of soil-gas surveys is directly proportional to their accuracy in reflecting and
representing changes in the subsurface concentrations of source compounds. Passive soil-gas
survey results are the mass collected from the vapor-phase emanating from the source. The
vapor-phase is merely a fractional trace of the source, so, as a matter of convenience, the units
used in reporting detection values from passive soil-gas surveys are smaller than those employed
for source-compound concentrations.
The critical fact is that, whatever the relative concentrations of source and associated soil gas.
best results are realized when the ratio of soil-gas measurements to actual subsurface
concentrations remains as close to constant as the real world permits. It is the reliability and
consistency of this ratio, not the particular units of mass {e.g., nanograms) that determine
usefulness. Thus, BEACON emphasizes the necessity of conducting — at minimum — follow-
on intrusive sampling at one or two points that show relatively high soil-gas measurements to
obtain corresponding concentrations of soil and groundwater contaminants. These correspondent
values furnish the basis for approximating the required ratio. Once that ratio is established, it can
be used in conjunction with the soil-gas measurements (regardless of the units adopted) to
estimate subsurface contaminant concentrations across the survey field. It is important to keep in
mind, however, that specific conditions at individual sample points, including soil porosity and
permeability, depth to contamination, and perched ground water, can have significant impact on
soil-gas measurements at those locations.
When passive soil-gas surveys are handled in this way, the data provide information that can
yield substantial savings in drilling costs and in time. They furnish, among other things, a
checklist of compounds expected at each survey location and help to determine how and where
drilling budgets can most effectively be spent.
BEACON Report Number: EM1715
Passive Soil-Gas Survey
ATK Thiokol Propulsion
Corinne, UT
This Passive Soil-Gas Survey Report has been prepared for ATK Thiokol, Inc. (ATK) by Beacon
Environmental Services, Inc. (BEACON) in accordance with the terms of Purchase Order No. M5FB031,
dated August 13, 2004. BEACON'S principal technical contact at ATK for this project has been Mr. John
Holladay. Passive soil-gas samples were collected following the protocols of the EMFLUX® Passive
Soil-Gas Sampling System.
In this survey, passive soil-gas samples were deployed in separate areas on the Thiokol Propulsion Site.
The following field sample designations were assigned for each of the areas: SWMU 551 (M551-01A
through M551-24A), Site M-39 (M39-01 through M39-11), and Plant 3 (M212-01 through M2I2-08).
Eleven samples were also collected outside of these areas, designated M207-01, M207-02, DRAIN-01,
DRAIN-02, DRAIN-03, FB-01, FB-02, FB-03, FB-04, M2I4-01, and M214-02.
1. Objectives
Soil-gas samples were collected to determine the presence, identity, and relative strength of
targeted contaminants in soil and/or ground water at the ATK Thiokol Propulsion site. Survey
results will be used to identify source areas and delineate the lateral extent of contamination.
2. Target Compounds
This survey targeted the 15 compounds listed in Attachment 1, which supplies the resulting
laboratory data in nanograms (ng) of specific compound per cartridge. Table 1 provides the data
for those compounds detected at one or more locations.
3. Survey Description
No. of Field Sample Points (SWMU 551): 24
No. of Field Sample Points (Plant 3): 8
No. of Field Sample Points (Site M-39): 11
No. of Field Sample Points (Other Areas): 11
No. of Trip Blanks: _1
Total No. of Samples: 57
Field sample locations for SWMU 551 and Plant 3 are shown on Figures 1-1 and 2-1.
Note: No compounds were identified on the samples collected at Site M-39 or the samples
collected outside of the three areas. At the request of ATK, no maps were provided
showing those sample locations.
f ( ( ( ( ( I ( I ( f ( { \ ( { I I I f ( I I / (
M151
OLD DRUM
STORAGE AREA
M311
PM4
./^f
^O ^O
MSS'
MSS'
19A MSS1-20A MS81-21A M881-22A MSS1-2M MSS'
A A • •
ISA MSSt-14A MSS1-1SA MS51-1SA MS61-1TA MS6'<-ieA
A A A A
-OTA MSSI-OtA MtSI-OM MSSMOA HSS1-11A M88'I-12A
A A A A
-01A MSS1-02A MSS1.03A MSS14MA MSS1.0SA MSS14WA
.•I : rr
lEACON
,ENVIRONMENTAL
in WW.IIM <ilmt. MM. D. Bri Air. MUlin4.
MSS1-20A PASSIVE SOIL-GAS SAMPLE LOCATION
200
Figure I-l
Passive Soil-Gas Survey
Sample Locations
SWMU 551
Thiokol Propulsion Site
Corinne, UT
{,(({(( I (('(''' ^ I ( ( ( I I ( < f ( ! , , ( f ( ( ( ( ^ ' I •: ( I
-^^W^'
A
M212-07
M212-08
A
M212-«1
M212-02 r' -!:••• ijo.ru
r I:(,.!:• I.-.••_
A
M212-03
A
M212-06
^ PASSIVE SOIL-GAS SAMPLE LOCATION
M212-02
A
M212-04
NOT TO SCALE
SEACON
.ENVIRONMENTAL
y 1^!^i^MM^.^•l•!M•
.11.1 WUBam NirM, Siriu TX IM Air, MD 21tl-l, mUTB-HlO
M212-05
Figure 2-1
Passive Soil-Gas Survey
Sample Locations
Plant3, BIdg. 212
Thiokol Propulsion Site
Corinne, UT
BEACON ENVIRONMENTAL SERVICES, INC.
Passive Soil-Gas Survey
.\'TK Tliiokol Propulsion
Coiinne. UT
4. Field Work
ATK was provided a Field Kit with the equipment needed to conduct a 54-point passive soil-gas
survey. Samplers were deployed on September 21 and 22, 2004, and were retrieved on October
5, 2004. Attachment 2 desciibes the field procedures used. Individual deployment and retrieval
times will be found in the Field Deployment Report (Attachment 3).
Analysis and Reporting Dates
BEACON'S laboratory received 57 samples for analysis on October 8, 2004.
Adsorbent cartridges from the passive samplers were thermally desorbed, then analyzed
using gas chromatography/mass spectrometry (GC/MS) equipment, in accordance with
EPA Method 8260B (Modified), as described in Attachment 4. BEACON's laboratory
analyzed each cartridge for the targeted compounds.
BEACON'S laboratory completed the analysis on October 14, 2004. Following a
laboratory review, results were provided to ATK on October 15. 2004.
• On November 5, 2004, ATK authorized BEACON to issue the final report.
Report Notes and Quality Assurance/Quality Control Factors
Table 1 provides survey results in nanograms per cartridge by sample-point number and
compound name. The quantitation levels represent values above which quantitative
laboratory results can be achieved within specified limits of precision and with a high
degree of confidence. The quantitation level for each compound, therefore, provides a
reliable basis for comparing the relative strength of any detection of that compound.
Data Compatibility. It is important to note that when sample locations are covered with
or near the edge of an artificial surface {e.g., asphalt or concrete), sample measurements
are often distorted (increased) significantly. Such distortion can be attributed to the fact
that gas rising from sources beneath impermeable caps tends to reach equilibrium
underneath the cap. Thus, a reading taken below or near an impermeable surface is
much higher than it would be in the absence of such a cap.
The Chain-of-Custody form, which was shipped with the samples for this survey, is
supplied as Attachment 5.
Laboratory QA/QC procedures included standards, surrogates, and blanks appropriate
to EPA Method 8260 (Modified). Field work, analyses, and reporting were done in
accordance with BEACON's Quality Assurance Program Plan.
BEACON ENVIRONMENTAL SERVICES, INC.
Passive Soil-Gas Survey
ATK Thiokol Propulsion
Corinne. UT
QA/QC Contaminant Corrections. Following EPA guidelines, laboratory data is not
cortected for method blank or trip blank sample contamination values; any
contamination detected on QA/QC samples is reported in Attachment 1.
Laboratory method blanks are run each day with project samples to identify
contamination present in the laboratory. If contamination is detected on a method blank,
measurements of identical compounds on samples analyzed the same day are considered
to be suspect and are flagged in the laboratory report. The laboratory method blanks
analyzed in connection with the present samples revealed no contamination.
The trip blank is a sampling cartridge prepared, transported, and analyzed with other
samples but intentionally not exposed. Any target compounds identified on the trip
blanks are reported in the laboratory data. The analysis of the trip blanks (labeled Trip-
1, Trip-2, and Trip-3 in Attachment 1) reported none of the targeted compounds,
indicating that the survey site itself is the source of detected contamination.
Survey findings are relative exclusively to this project and should not routinely be
compared with results of other BEACON Surveys. To establisli a relationship between
reported soil-gas measurements and actual subsurface contaminant concentrations,
which will indicate those detections representing significant subsurface contamination,
BEACON recommends the guidelines on the inside front cover of this report.
No compounds were identified at Site M-39, therefore, no compound distribution maps
were provided for that area. At the request of ATK, the following compound distribution
maps have been provided for SWMU 551 and Plant 3.
SWMU 551
Figure 1-2 — Tetrachloroethene
Figure 1-3 — Trichloroethene
Figure 1-4 — 1,1,1-Trichloroethane
Plant 3
Figure 2-2 — Trichloroethene
Figure 2-3 — 1,1,1-Trichloroethane
BEACON ENVIRONMENTAL SERVICES, INC.
Passive Sail-Gas Survey
ATK Tliiokol Propulsion
Corinne, UT
The following Attachments are included:
-1 - Laboratory Report
-2- Field Procedures
-3- Field Deployment Report
-4- Laboratory Procedures
-5- Chain-of-Custody Form
EMI715
BEACON ENVIRONMENTAL SERVICES, INC.
Passive Soil-Gas Survey
ATK Thiokol Propulsion
Corinne, LIT
Table 1
Beacon Environmental Services, Inc.
323 Williams Street, Suite D
Bel Air, MD 21014
Passive Soil-Gas Data
Analysis by EPA Method 8260B (Modified)
Client Sample ED:
Project Number:
Lab File ID:
Received Date:
Analysis Date:
Analysis Time:
Units:
COMPOUNDS
Chloroform
1,1,1 -Trichloroethane
Trichloroethene
Tetrachloroethene
Client Sample ID:
Project Number:
Lab File ID:
Received Date:
Analysis Date:
Analysis Time:
Units:
COMPOUNDS
Chloroform
1,1,1 -Trichloroethane
Trichloroethene
Tetrachloroethene
Meth_Blk
EMI715
40I0I213
Trip-l
EM1715
40I0I2I4
10/8/2004
M39-01
EM1715
40I0I215
10/8/2004
M39-02
EM17I5
40101216
10/8/2004
10/12/2004 10/12/2004 10/12/2004 10/12/2004
18:11
ng/trap
<25
<25
<25
<25
M39-05
EM1715
4010I2I9
10/8/2004
18:42
ng/trap
<25
<25
<25
<25
M39-06
EM1715
40101220
10/8/2004
19:13
ng/trap
<25
<25
<25
<25
M39-07
EM1715
40101221
10/8/2004
19:44
ng/trap
<25
<25
<25
<25
M39-08
EM1715
40101222
10/8/2004
M39-03
EM1715
40101217
10/8/2004
10/12/2004
20:15
ng/trap
<25
<25
<25
<25
M39-09
EM1715
40101223
10/8/2004
M39-04
EM17I5
40101218
10/8/2004
10/12/2004
20:46
ng/trap
<25
<25
<25
<25
M39-10
EM1715
40101224
10/8/2004
10/12/2004 10/12/2004 10/12/2004 10/12/2004 10/12/2004 10/12/2004
21:17
ng/trap
<25
<25
<25
<25
21:48
ng/trap
<25
<25
<25
<25
22:19
ng/trap
<25
<25
<25
<25
22:50
ng/trap
<25
<25
<25
<25
23:21
ng/trap
<25
<25
<25
<25
23:51
ng/trap
<25
<25
<25
<25
Results in nanograms (ng).
J = Estimated value below reported quantitation level. B = Detected in method blank.
BEACON ENVIRONMENTAL SERVICES, INC.
Passive Soil-Gas Survey
ATK Thiokol Propulsion
Corinne, UT
Table 1
(continued)
Beacon Environmental Services, Inc.
323 Williams Street, Suite D
Bel Air, MD 21014
Passive Soil-Gas Data
Analysis by EPA Method 8260B (Modified)
Client Sample ID:
Project Number:
Lab File ED:
Received Date:
Analysis Date:
Analysis Time:
Units:
COMPOUNDS
Chloroform
1,1,1-Trichloroethane
Trichloroethene
Tetrachloroethene
Client Sample ID:
Project Number:
Lab File ID:
Received Date:
Analysis Date:
Analysis Time:
Units:
COMPOUNDS
Chloroform
1,1,1 -Trichloroethane
Trichloroethene
Tetrachloroethene
M39-11
EM1715
40101225
10/8/2004
10/13/2004
0:22
ng/trap
<25
<25
<25
<25
FB-01
EM1715
40101226
10/8/2004
10/13/2004
0:53
ng/trap
<25
<25
<25
<25
FB-02
EM1715
40101227
10/8/2004
10/13/2004
1:24
ng/trap
<25
<25
<25
<25
FB-03
EM1715
40101228
10/8/2004
10/13/2004
1:55
ng/trap
<25
<25
<25
<25
FB-04
EM1715
40101229
10/8/2004
10/13/2004
2:26
ng/trap
<25
<25
<25
<25
M551-01A M551-02A M551-03A M551-04A M551-05A
EM1715
40101231
10/8/2004
10/13/2004
3:28
ng/trap
<25
771
6,458
<25
EM17I5
40101232
10/8/2004
10/13/2004
3:59
ng/trap
<25
300
1,268
<25
EMI7I5
40101233
10/8/2004
10/13/2004
4:30
ng/trap
<25
491
1,181
<25
EM1715
40101234
10/8/2004
10/13/2004
5:01
ng/trap
<25
27
43
<25
EM1715
40101235
10/8/2004
10/13/2004
5:32
ng/trap
<25
336
764
26
Trip-2
EM1715
40101230
10/8/2004
10/13/2004
2:57
ng/trap
<25
<25
<25
<25
M551-06A
EM1715
40101236
10/8/2004
10/13/2004
6:03
ng/trap
<25
847
1,088
82
Results in nanograms (ng).
J = Estimated value below reported quantitation level. B = Detected in method blank.
BEACON ENVIRONMENTAL SERVICES, INC.
Passive Soil-Gas Survey
.ATK Thiokol Propulsion
Corinne, UT
Table 1
(continued)
Beacon Environmental Services, Inc.
323 Williams Street, Suite D
Bel Air, MD 21014
Passive Soil-Gas Data
Analysis by EPA Method 8260B (Modified)
Client Sample ID:
Project Number:
Lab File ID:
Received Date:
Analysis Date:
Analysis Time:
Units:
COMPOUNDS
Chloroform
1,1,1 -Trichloroethane
Trichloroethene
Tetrachloroethene
Client Sample ID:
Project Number:
Lab File ID;
Received Date:
Analysis Date:
Analysis Time:
Units:
COMPOUNDS
Chloroform
1,1,1 -Trichloroethane
Trichloroethene
Tetrachloroethene
M551-07A M551-08A M551-09A M551-10A M551-11A M551-12A |
EM1715
40101237
10/8/2004
EM1715
40101238
10/8/2004
EM1715
40101239
10/8/2004
EM1715
40101240
10/8/2004
EM1715
40101241
10/8/2004
10/13/2004 10/13/2004 10/13/2004 10/13/2004 10/13/2004
6:34
ng/trap
<25
53
39
<25
7:05
ng/trap
<25
1,362
2,754
53
7:36
ng/trap
<25
314
653
<25
8:07
ng/trap
<25
804
3,097
<25
8:38
ng/trap
<25
504
1,872
<25
M551-13A M551-14A M551-15A M551-16A M551-17A
EM1715
40101243
10/8/2004
10/13/2004
9:39
ng/trap
<25
41
121
<25
EM1715
40101244
10/8/2004
EM1715
40101245
10/8/2004
10/13/2004 10/13/2004
10:10
ng/trap
<25
131
942
<25
10:41
ng/trap
<25
209
645
<25
EM1715
40101246
10/8/2004
10/13/2004
11:12
ng/trap
<25
42
<25
<25
EM1715
40101247
10/8/2004
10/13/2004
11:43
ng/trap
<25
41
25
<25
EMI715
40101242
10/8/2004
10/13/2004
9:09
ng/trap
<25
129
616
<25
M551-18A
EM1715
40101248
10/8/2004
10/13/2004
12:14
ng/trap
<25
<25
<25
<25
Results in nanograms (ng).
J = Estimated value below reported quantitation level. B = Detected in method blank.
BEACON ENVIRONMENTAL SERVICES, INC.
Passive Soil-Gas Sui'vey
ATK Thiokol Propulsion
Corinne, UT
Table 1
(continued)
Beacon Environmental Services, Inc.
323 Williams Street, Suite D
Bel Air, MD 21014
Passive Soil-Gas Data
Analysis by EPA Method 8260B (Modified)
Client Sample ED:
F*roject Number:
Lab File ID:
Received Date:
Analysis Date:
Analysis Time:
Units:
COMPOUNDS
Chloroform
1,1,1 -Trichloroethane
Trichloroethene
Tetrachloroethene
Client Sample ID:
Project Number:
Lab File ID:
Received Date:
Analysis Date:
Analysis Time:
Units:
COMPOUNDS
Chloroform
1,1,1 -Trichloroethane
Trichloroethene
Tetrachloroethene
M551-19A M551-20A M551-21A M551-22A M551-23A M551-24A |
EM1715
40101249
10/8/2004
EM1715
40101250
10/8/2004
EM1715
40101251
10/8/2004
EM1715
40101252
10/8/2004
10/13/2004 10/13/2004 10/13/2004 10/13/2004
12:45
ng/trap
<25
<25
<25
<25
13:16
ng/trap
<25
121
117
<25
13:47
ng/trap
<25
36
<25
<25
DRAIN-01 DRAIN-02 DRAIN-03
EM1715
40101255
10/8/2004
EM1715
40101256
10/8/2004
EM1715
40101257
10/8/2004
14:18
ng/trap
<25
903
659
<25
Meth_Blk
EM1715
40101303
EM1715
40101253
10/8/2004
10/13/2004
14:48
ng/trap
<25
127
247
<25
Trip-3
EM1715
40101304
10/8/2004
EM1715
40101254
10/8/2004
10/13/2004
15:19
ng/trap
33
403
950
<25
M212-01
EM1715
40101305
10/8/2004
10/13/2004 10/13/2004 10/13/2004 10/13/2004 10/13/2004 10/13/2004
15:50
ng/trap
<25
<25
<25
<25
16:21
ng/trap
<25
<25
<25
<25
16:52
ng/trap
<25
<25
<25
<25
18:25
ng/trap
<25
<25
<25
<25
18:56
ng/trap
<25
<25
<25
<25
19:27
ng/trap
<25
<25
94
<25
Results in nanograms (ng).
J = Estimated value below reported quantitation level. B - Detected in method blank.
BEACON ENVIRONMENTAL SERVICES, INC.
Passive Soil-Gas Survey
•ATK Thiokol Propulsion
Corinne. LIT
Table 1
(continued)
Beacon Environmental Services, Inc.
323 Williams Street, Suite D
Bel Air, MD 21014
Passive Soil-Gas Data
Analysis by EPA Method 8260B (Modified)
Client Sample ID:
Project Number:
Lab File ID:
Received Date:
Analysis Date:
Analysis Time:
Units:
COMPOUNDS
Chloroform
1,1,1-Trichloroethane
Trichloroethene
Tetrachloroethene
Client Sample ID:
Project Number:
Lab File ID:
Received Date:
Analysis Date:
Analysis Time:
Units:
COMPOUNDS
Chloroform
1,1,1 -Trichloroethane
Trichloroethene
Tetrachloroethene
M212-02
EM1715
40101306
10/8/2004
M212-03
EM1715
40101307
10/8/2004
M212-04
EM1715
40101308
10/8/2004
M212-05
EM1715
40101309
10/8/2004
10/13/2004 10/13/2004 10/13/2004 10/13/2004
19:58
ng/trap
<25
<25
179
<25
M212-08
EM1715
40101312
10/8/2004
20:29
ng/trap
<25
<25
431
<25
M207-01
EM1715
40101313
10/8/2004
21:00
ng/trap
<25
<25
231
<25
M207-02
EM1715
40101314
10/8/2004
21:31
ng/trap
<25
<25
26
<25
M214-01
EM1715
40101315
10/8/2004
M212-06
EM1715
40101310
10/8/2004
10/13/2004
22:02
ng/trap
<25
47
111
<25
M214-02
EM1715
40101316
10/8/2004
10/13/2004 10/13/2004 10/14/2004 10/14/2004 10/14/2004
23:04
ng/trap
<25
25
617
<25
23:35
ng/trap
<25
<25
<25
<25
0:06
ng/trap
<25
<25
<25
<25
0:37
ng/trap
<25
<25
<25
<25
1:08
ng/trap
<25
<25
<25
<25
M212-07
EM1715
40101311
10/8/2004
10/13/2004
22:33
ng/trap
<25
<25
30
<25
Results in nanograms (ng).
J = Estimated value below reported quantitation level. B = Detected in method blank.
( ( ( ( ( ( { ( t I I I ,,•(/(•.(('
MI51
OLD DRUM
•^.TORAGE AREA
M31
PM41
A '/r ^o ^io
MSS' -1»A MSS1-20A MS81-21A MSS1-22A MSS1-23A MSS
MSS'
53
ik A A A A
MSB' -07A HSS14M MS61-08A MSSI-IQA MSS1-11A MSS'
-24A
A A A A
,13A MSS1-14A MSS1-1SA MSS1-1SA MSS1-17A MSS'
26
A A A A
MSSl-OIA MSS142A MSS1.03A MSS1.04A MSS1-0SA MSS'
18A
12A
8|2
L
-OSA
100
90
80
70
60
50
40
30
20
10
Color Scale
(nanograms)
L SEACON
(ENVIRONMENTAL
Uraron Pro^rft Da. f-Mni\ OrteWr JOVJ
Scale in Feet
100 200
82 TETRACHLOROETHENE (nanograms)
^ PASSIVE SOIL-GAS SAMPLE LOCATION
MSS1-2<IA
Figure 1-2
Passive Soil-Gas Survey
Tetrachloroethene
SWMU 551
Thiokol Propulsion Site
Corinne, UT
( I I i (
M15
M3-
A '/r ^o
PM4H
'^0117
MSS'
i;:i
MSS'
39
659
-,A—
247
'19A MSS1-20A MSS1-21A MSS1-22A MSS1-23A MSS'
950
24A
942 645 25 A A A A
13A MSS1.14A MBS1-1SA MSS1-16A MS61-17A MSS
2,754 653 3,097 1,872
• • • •
MS8'l47A MSSI-OSA MSS14>M M»1-10A MSSLIIA MSS'
ISA
616
6:
MSI
'12A
1,268 1.181 43 764 1,088 A A A A
MBS102A MSS14)3A MSS1.04A MSS1.0SA MSti-06A
7,000
6,500
6,000
5,500
5,000
4,500
4,000
3,500
3,000
2.500
2,000
1,500
1,000
500
L-'o
Color Scale
(nanograms)
OLD DRUM
:^ rORAGfr, AREA
E BEACON
lENVIRONMENTAL
Scale in Feet
100
39 TRICHLOROETHENE (nanograms)
A PASSIVE SOIL-GAS SAMPLE LOCATION MS61-20A
200
J:J WHIiiiB .SinM, Sun* 1). bri :Ur. Ml> 11014. Mt-«7«-Wi0
Figure 1-3
Passive Soil-Gas Survey
Trichloroethene
SWMU 551
Thiokol Propulsion Site
Corinne, UT
M15
^:.>LD DRUM
^^TORAGE AREA
M3
PM411
A/>, /^-o '^O,.
MSS'
41
i
MSS'
53 804 504 1,362 314
• A
MSS'i-OTA MS814eA MSS1-0M MSSMOA MBS1-11A MS6'
T
i
MSS'
^Oi21
A-
36
-A-
903
—Ar-
127
—A^ 1»A MSS1-20A MSS1.21A MSS1-22A MS51-23A MSS'
42
403
.24A
131 209 42 41 A A A A
13A MSS1-14A MSS1-1SA MSS1-1BA MSS1-17A MSS' -ISA
1?9
12A
27 336 8-17 300 491 A A
.01A MSS1.02A MSS1.03A MS51-(MA MSS1.0SA MSS'I^OSA
r' 1,500
1,400
-1,300
-1,200
[-1,100
1,000
900
800
700
600
! 1-500
400
300
200
100
L... ! 0
Color Scale
(nanograms)
) WMUiii. siiTTi, 'Mil U. IM Mr, KW lltU, HO^Tt-WlA
llrariMi Vn^trt N#. EMI^IS, OrMbtr MWJ
Scale in Feet
100 200
36 1,1,1 -TRICHLOROETHANE (nanograms)
^ PASSIVE SOIL-GAS SAMPLE LOCATION
MSS1-20A
Figure 1-4
Passive Soil-Gas Survey
1,1,1-Trichloroethane
SWMU 551
Thiokol Propulsion Site
Corinne, UT
EMFLUX PASSIVE SOIL-GAS SURVEY
FIELD DEPLOYMENT REPORT
FIELD
SAMPLE ID
/M GSl- lU
M<=^'^h\lA
^S5f'l?fi
MS^l-m
/M56-1 - l^A
MS5\ -2//\
M55/ - Z2A
MS€l-ti/^
/^SSi'l'^f^
Date Emplaced
1\S\^nD^
Time Emplaced
/4-'(>^
/^•27
/4.'?/
;4;55
K:5c>
/4:Z5
/^iz-?
/f.7>r
/4:/D
Date Retrieved
^oorzQsf
Time Retrieved
/^:24
f4v^7
(4:^^
lA:3o
t&:3t
/4'53
;^i3^
(^:35
Hi 3^
1 : ^^^^^==^ ===
FIELD NOTES
(e.g., asphalt/concrete covering, description of sample location, cartridge/vial condition)
^BEACON;
I" , ENVIRONMENTAL!
Page of
{ I
EMFLUX PASSIVE SOIL-GAS SURVEY
FIELD DEPLOYMENT REPORT
Beacon Project No.:
Site Name:
Project Information
Site Location:
EM1715
Thiokol Propulsion — Plant 3
Corinne, UT
SEACON
ENVIRONMENTAL
SERVICES, INC,
Client Information |
Company Name:
Office Location:
Samples Collected By:
ATK Thiokol, Inc
Corinne, UT
313 Williami Strm. Suite D. Bel Air, MD 21014.8OO-S7a.UI0
FIELD
SAMPLE ID
Uz/z-c?/
AiZ\1 ^OZ
A) 2-17-^3
M%[l'(A
A)^^^-o^
Mza^ofo
Atin-o-y
Nziz-oS
A1707- 0)
yif 207-02
p<2/)/M-o/
D£AIKI'D2
VMttJ-OJ
F^ -01
fO-o-^
Date Emplaced
aZ^PffToH
Time Emplaced
/e:5i
10:47
/o-^is
ID-^^
10.'^i
10:^7
/0:5'e
/d.fS
ir-fO
;/./^
(I.SS
IZ-co
iZiOS
13-3^
i'3-31
Date Retrieved
05 OCT o4
Time Retrieved
^S"bS
iS.o 6
l§:oh
t^'Ol
IS.' 0%
/r;o«
/^'O'?
l^i(0
l^-l(:>
1^17
n'^'-Ao
D8M2-
c>?-t1
0^^
f}%-ii^
..—-"• 1
FIELD NOTES
{e.g., asphalt/concrete covering, description of sample location, sampling hole depth,
cartridge/vial condition)
1==^
Page of
/ ( 1 ( ( (• ' I f ( I I
I (
EMFLUX PASSIVE SOIL-GAS SURVEY
FIELD DEPLOYMENT REPORT
FIELD
SAMPLE ID
^^-03
ffi>- 0^
l\f[\\A' 0^
M^t^-o^
Date Emplaced
ifi-^fX^cA-
Time Emplaced
13-3'?
Ig-.-fl/
r
UM5
ll:H
Date Retrieved
0^(>CT 04
1
Time Retrieved
(?? : Z^
0% :lS
/rz-f
/c.-z--^
•,=-• • : ...ir. ::•
FIELD NOTES
(e.g., asphalt/concrete covering, description of sample location, cartridge/vial condition)
— —-- "• •—•— - -• •- =•=- • -^ •• =~=^ =^ : =—• •- = — . ~
^EEACON
\F .ENVIRONMENTAL!
Page of
, MJlr n. IM Av. KU):i*
Attachment 4
LABORATORY PROCEDURES
FOR PASSIVE SOIL-GAS SAMPLES
Following are laboratory procedures used with BEACON Passive Soil-Gas Surveys, a screening
technology for expedited site investigation. After exposure, adsorbent cartridges from the passive
samplers are analyzed using U.S. EPA Method 8260B as described in the Solid Waste Manual (SW-846),
a capillary gas chromatographic/mass spectrometric method, modified to accommodate high temperature
thermal desorption of the adsorbent cartridges. This procedure is summarized as follows:
A. The adsorbent cartridges are loaded with internal standards and surrogates prior to loading the
autosampler with the cartridges. The loaded cartridges are purged in a helium flow. Then the
cartridges are thermally desorbed in a helium flow onto a focusing trap. Any analytes in the
helium stream are adsorbed onto a focusing trap.
B. Following trap focusing, the trap is thermally desorbed onto a DB-VRX 60m, 0.25 mm ID, 1.40
micron filament thickness capillary column.
C. The GC/MS is scanned between 35 and 270 Atomic Mass Units (AMU) at 3.12 scans per second.
D. BFB tuning criteria and the initial five-point calibration procedures are those stated in method
SW846-8260B. System performance and calibration check criteria are met prior to analysis of
samples. A laboratory method blank is analyzed after the daily standard to determine that the
system is contaminant-free.
E. The instrumentation used for these analyses includes:
Agilent 6890-5973 Gas Chromatograph/Mass Spectrometer;
• Markes Unity thermal desorber;
Markes UltrA autosampler; and
Markes Mass Flow Controller Module.
Attachment 5
Chain-of-Custody Form
I f
CHAIN-OF-CUSTODY
EMFLUX PASSIVE SOIL-GAS SAMPLES
Project Information
Beacon Project No.:
Site Name:
Site Location:
Analytical Method:
Target Compounds:
EM1715
Thiokol Propulsion — Site M-39
Corinne, UT
EMFLUX EPA Method 8260B
ABEAOON
k \ENVIRONMENTAL
^n SERVICES. INC.
3D Williami SirM. Suite D. Bel Air. ,M0 21014. SOO-ITt-SSIO
Client Information
Company Name:
Office Location:
Samples Submitted By:
Contact Phone No.:
ATK Thiokol, Inc.
Corinne, UT
Beacon Project No. EM1715 Target Compound List
Field Sample ID Lab Sample ID
(for lab use only)
Comments
(only necessary if problem or discrepancy)
Condition of sample or vial Date Time Initial
Trip-1 im Tri^-l
/*i^?-oi 1^1^ /V\^1-o| ^/. /S:^l 'Mt-
M-^'\-0^ Llli. AAM-ol. (S'.y
M ,s^ - 03 1^19 Mll-Di /S-'^3 J^ Rl5 MYro± /r^ -4C^
ms M'^'t-oS fs-^s <^CH
MZ^- Oi, I71S MVljiOt^ /^•'4t^ 'Jc^
MTPl'On nil M^l-o-^ IS!^1 J^ M^'f- 0<S l^lf _M15i^ JSf^L_ JOL.
M-^Cj ^ o^ n\^ M'i'i-o'^ /^"f^ -JCti-
/M.^q'/o ITI5 MM'to tS'.So GJAt
yyyi^i'ix \^\^ MVi-W JSj^L <ki^
FB -o\ l>is Ffe-») Qgi-t? ^M-
Fd-QT-illL Fft-oZ Df-'Z.I rKM^
-^e-D3 1^1? P6-03 Mll±_ MM
f^-o^i illL F6-0M .cXiis: Aoit-
IjpN Shipment of Field Kit to Site — Custody Seal # 00357970 Intact?
ReUifqufebed by; Date/Time
^AT/O/ MtP^ />/-.
Courier y Received by: Date/Time
7^^
ntact? (V) N" Shipment of Field Kit to Laboratory — Custody Seal # ^Q 3^7971
cennquisneQ Dy; Date/Time
10 In lo^
Courier
/^cX eceivc Date/Time jJate/ Hm
09V<^
Page / of /
CHAIN-OF-CUSTODY
EMFLUX PASSIVE SOIL-GAS SAMPLES
Pro
Beacon Project No.:
Site Name:
Site Location:
Analytical Method:
Target Compounds:
ect Information
EM1715
Thiokol Propulsion — Plant 3
Corinne, UT
EMFLUX EPA Method 8260B
ABEAeON
> \ENVIRONMENTAL
^n SERVICES. INC.
3D Willi.mi Street. Suite D. Bel Air. MD 21014.800-878.5510
Client Information
Company Name:
Office Location:
Samples Submitted By:
Contact Phone No.:
ATK Thiokol, Inc.
Corinne, UT
Beacon Project No. EM 1715 Target Compound List
Field Sample ID Lab Sample ID
(for lab use only)
Comments
(only necessary if problem or discrepancy)
Condition of sample or vial Initial
Trip-2 iliS Tr,«-Z
^ /yt'^si 'OiA ms_ MS^I-oM
/If?.*?/ -P7A IT»9 MS'i\-OlA
yvisGi *03i \^\s M'^^i'oM
M^SJ'OH^ 1^ M'i^i-oHA
l^HS A^^Sl-O^/^ ^S5I 'BSfi
W5 /A^'ii- 0(,/^ AigJ/^pfeA
/nssi -OlA W^ M'i'ii-d^A
M<5$1 -OU ?i^ M5'i\-o'iA
MSSI -D^ih ll-l?" /AS'i\- o'iA
/nifi ^A i^l5" /^55l- IM
MSK/ "ilA m^ .M^'^\-\iA
/wrr/ -1^^ R\S M^^l-llA
M^t-tlfi' ims /^tjsl- \lA
/M<;g/^^/4/^ \1\S M^5\- hA
yVT«)g/-/r/» \^\S M55I- M
ni? M^'^i-K/A /Mgg/ -({.A
m5^l -nfi 1^1^ /V15f>- nA
1^1? /vi'^si- \%A /hsri - irff^ R]? ^55\' nA /*is^/ -^^/i-
Shipment of Field Kit to Site — Custody Seal # 00357970
dby: Date/Time Courier
6/^?/^y
Shipment of Field Kit to Laboratory — Custody Seal U oas^^973 elinquished by
IJHA^/I^
Date/Time ^^ Courier
ny>tx toj^n o^
Page / of 2-
I I I I I ( ( ' f
I { I I ( ( ( <
CHAIN-OF-CUSTODY
EMFLUX PASSIVE SOIL-GAS SAMPLES
Project Information
Beacon Project No.
Site Name:
Site Location:
Analytical Method:
EM1715
Thiokol Propulsion — SWMU 551
Corinne, UT
EMFLUX EPA Method 8260B 323 Williams Sircel. Suite n. Bel \ir. MP 2IIIM. .Illd-'nii-.'SIO
Client Information
Company Name:
Office Location:
Samples Submitted By:
Contact Phone No.:
ATK Thiokol, Inc.
Corinne, UT
Target Compounds: Beacon Project No. EM 1715 Target Compound List
Field Sample ID
w
Lab Sample ID
(for lab use only)
Comments
(only necessary if problem or discrepancy)
Condition of sample or vial Date Time Initial
-Tiip-?Z. ?ffcv>'i}osL Kfc6or<M
A]f$i-^?J2A \1\S /Vl55i-lg/1 MIA cW-
AS^/-^J/» IllS A\S5I-ZM MJ^ .kM-
M9S\ -^2gA_ n-15 -l^M-4€40-
Al^^J^^3^ J-^IS M3& ..^^
MSH^L^ZAL^ |^\^ ./Vl5"5r<- V\A M3th-MAT
MAiihilL [1\S v?(sM/V- o> ]pf2^ M4G-^6ti^
J^«An(-Cf^ 1^19 -pMlAz-P^ 4m4-^ m os'ii' J^
M&hML:LQ±_ R15 Wy^lA/ - 0 3 wnfM i>9^^f kM~
Shipment of Field Kit to Site
Relinquished by:
j/'~'[./t. i-'i-U
— Custody Seal #
Date/Time
y.''-^ ^-^ : /ii-,.. /, .
00357970
Courier
.•'~^'^j"<
Intact? Y N
Received by: Date/Time
Shipment of Field Kit to Laboratory -
Relinquished by:
- Custody Seal #
Date/Time Courier
Intact? Y N
Received bv: Date/Time
Page Z of 2-
(
CHAIN-OF-CUSTODY
EMFLUX PASSIVE SOIL-GAS SAMPLES
Project Information
Beacon Project No.:
Site Name:
Site Location:
Analytical Method:
Target Compounds:
EM1715
Thiokol Propulsion — SWMU 551
Corinne, UT
EMFLUX EPA Method 8260B
ABEAGON
A \ENVIRONMENTAL
1 ^n SERVICES. INC.
323 Williimi Street. Suite D. Bel Air. MD 21014.800-878-S510
Client Information
Company Name:
Office Location:
Samples Submitted By:
Contact Phone No.:
ATK Thiokol, Inc.
Corinne, UT
Beacon Project No. EM1715 Target Compound List
Field Sample ID Lab Sample ID
(for lab use only)
Comments
(only necessary if problem or discrepancy)
Condition of sample or vial Date Time Initial
Trip-3 ms Tfip-S
j^Z4 2. - 0/ lllL /Mill- 01 JS:0 5
MT.IZ'O^' Rl? /Villi-01 tf'Cri'
M2,tz-b-i I^IS /V\Z.ll- ol /.^-•g-6
Jl/|Xf^-o^ 11-15 ./Hill- PH y^ (H
MU^'£><; i>i5 Mm- o? s-'-a MUl. - oi? )l-'5' AAU1- ofe rS-.'^??"
MT.lT'- ol I^IS" MX\X- ^ if-Dl
/f?2<Z -gg i^is" /vtin- o% JllMi-
/i^T-oi^oi n-lf A1Z(?T- -PI I5:jh
AAiol-oZ ITIF M-Lo-\' ol /$•-•/7
/>t2,<4'(?J ^^ir /HUM- o\ /5":&/
./tfZl2-g>2. i^t? /yiliH-Q-L tS'-Z'i
Shipment of Field Kit to Site — Custody Seal # 00357970
ate/Time iMmHSM^ C!ourier Ceived by: Date/Time
Shipment of Field Kit to Laboratory — Custody Seal # OoSs-7?75
Date/Time Courier uate/1 line
Page / of J