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Home My WebLink AboutDSHW-2008-002061 - 0901a0688013d589REGESVED APR 2 3 2008 uian UIVISlUN OF SOLID & HAZARDOUS WASTE RESULTS OF THE HYDRASLEEVE DISCRETE INTERVAL NO-PURGE SAMPLER EVALUATION ATK Launch Systems Promontory Facility Promontory, Utah February 2008 Revised April 2008 EarthFax EarthFax Engineering, Inc. Engineers / Scientists www.earthfax.com •i: ?iTK Launch Systems » . HydraSleeve® Results Report Promontory, ,Utah revised April'2008 JOUS ' ! .•* '^ t'•' ',' 11 fl .'"• C / r • t • . ,. , , '-..-.•^Vv ::,UUn>-i!\\<-2,-i J--, ijii'j; TABLE OF CONTENTS 1.0 INTRODUCTION 1 2.0 HYDRASLEEVE® TECHNOLOGY 2 2.1 BACKGROUND :....; 2 2.2 GROUNDWATER SAMPLING AND WELL SELECTION 3 2.3 FIELD MEASUREMENTS • 5 2.4 ANALYTICAL METHODS 5 2.5 QA/QC SAMPLE COLLECTION 5 2.5.1 Trip Blanks 5 2.5.2 Field Blanks 6 2.5.3 Equipment Blanks 6 2.5.4 Field Duplicate Samples 6 3.0 SAMPLING RESULTS AND COMPARISON 7 3.1 DATA PRESENTATION 7 3.2 SAMPLING RESULTS COMPARISON 7 3.3 CONVENTIONAL STATISTICAL ANALYSES 8 3.3.1 Data Distribution.: 8 3.3.2 Wilcoxon Matched-Pairs Signed Ranks Test 9 3.3.3 Sign Test: -. , 10 3.3.4 Linear Regression 10 3.3.5 Median RPD 12 3.3.6 Qualitative Assessment 13 3.4 QUALITY ASSURANCE/QUALITY CONTROL 13 4.0 CONCLUSIONS 15 5.0 REFERENCES 16 ATK Launch Systems Promontory, Utah HydraSleeve® Resiilts Report revised April 2008 TABLE OF CONTENTS (continued) TABLES Table 1 Table 2 Table 3 Table 4 Tables Monitoring Well Information , Field Parameters/ HydraSleeve® Samples Statistical Summary for HydraSleeve® Sampler Statistical Summary for Metals Statistical Summary for VOCs FIGURES Figurel Site Location Map Figure 2 Monitoring Wells Sampled During Study APPENDICIES Appendix A Test for Normality Appendix B Linear Regression Plots Appendix C Laboratory Analytical Data 111 ATK Launch Systems HydraSleeve® Results Report Promontory, Utah revised April 2008 RESULTS OF THE THE HYDRASLEEVE® DISCRETE INTERVAL NO-PURGE SAMPLER EVALUATION 1.0 INTRODUCTION ATK Launch Systems evaluated the efficacy ofthe HydraSleeve® discrete interval no-purge sampler for use in their groundwater monitoring program. To accomplish this objective, the HydraSleeve® was utilized along with the conventional sampling 3-volume purge method for the spring 2007 sampling event at the ATK Promontory, Utah facility (figure 1). This report provides a description of activities for the HydraSleeve® demonstration. A review of the HydraSleeve® technology, well selection criteria, and outline of the field activities are presented in Chapter 2. Chapter 3 presents a discussion of statistical comparison, data evaluation, and QA/QC results from this demonstration. Chapter 4 presents conclusions and references can be found in Chapter 5. ATK Launch Systems HydraSleeve® Results Report Promontory, Utah revised April 2008 2.0 HYDRASLEEVE® TECHNOLOGY 2.1 BACKGROUND The HydraSleeve® sampler (US patents #6,481,300 and #6,837,120), manufactured by Geolnsight (www.hydrasleeve.com), is designed to collect a representative groundwater sample for analyses of most physical and chemical parameters without purging the well. It collects a water sample from a defined interval within the well screen without mixing fluid from other intervals. Physically, it is a section of lay-flat polyethylene tubing, sealed at the bottom end, and built with a polyethylene reed-valve at the top end. The empty sampler is weighted at the bottom, attached to a line, and then lowered to a predetermined depth within the well screen. It is typically left in the well for a period of time to allow the well to re-equilibrate following sampler deployment. Once the well has re-equilibrated, the sampler can be activated for sample collection. Prior to activation, the sampler remains in a collapsed (i.e., empty) state and therefore takes up minimal space within the well. To activate, the sampler is pulled up a distance equal to 1 to 2 times the sampler length (2.5 to 5 feet for a 30-inch-long sampler). As the sampler rises through the water column, the reed valve opens, allowing the sampler to "core" the water column through which it is being raised. Once full, the reed valve closes, which prohibits any more water from entering the sampler. An altemate approach to activating the sampler is to raise and lower it multiple times over a distance equal to the sampler length. However, this approach is less attractive because the raising and lowering of the sampler can result in increased agitation ofthe water in the well and higher turbidity levels in the sample. ATK Launch Systems HydraSleeve® Results Report Promontory, Utah revised April 2008 The 24- to 30-inch-long sampler can be purchased in either 1.5- or 2.5-inch diameter models; the 30-inch sampler has volumes of 1,000 mL and 2,500 mL for these diameters, respectively. Previous studies by the United States Army Corps of Engineers for the former McClellan Air Force Base, Califomia focused on the demonstration of several sampling methods (diffusion, HydraSleeve®, low-purge, etc.). Once collected, the data were screened using the Shapiro-Wilk's W test to determine distribution. The appropriate statistical test method was then applied to the data to determine comparability ofthe data. From a performance perspective, the HydraSleeve® method produced results that were most similar to the results obtained from the conventional sampling method (three- volume purge). The study also found that the HydraSleeve® was substantially less expensive than conventional methods (Parsons 2005). 2.2 GROUNDWATER SAMPLING AND WELL SELECTION Conventional sampling at ATK that is part of regularly scheduled sampling is performed using a 3-volume purge technique. This method involves removing a large volume of water (three to five well-casing volumes) from the well over a short period of time. The objective ofthis method is to remove all stagnant water present within the well casing, as well as groundwater present in the surrounding well filter pack. Theoretically, by removing this water quickly, the "stagnant" water that resided in the well and filter pack will be replaced with "fresh" groundwater from the surrounding formation with minimal mixing. The "fresh" groundwater that is then sampled is considered to be representative of the local groundwater. Rapid drawdown of the water level in a well is not uncommon, and wells are often purged dry using this method. Prior to purging, each well was sampled using a HydraSleeve® sampler. A new HydraSleeve® was lowered, allowed to settle for approximately 24 hours, and removed from each well in accordance with the manufacture's recommendations. The pH, ATK Launch Systems HydraSleeve® Results Report Promontory, Utah revised April 2008 temperature, and specific conductance of the HydraSleeve® sample were determined and the well was then sampled conventionally utilizing the 3-volume purge method. A submersible pump (i.e., Grundfos RediFlo2®) was then used to perform- conventional purging and sampling at each of the wells. The pump intake was positioned at the midpoint of the saturated portion of the well screen and the well was purged of 3- volumes of water. Field parameters were monitored during purging and included temperature, pH, and specific conductance. Once the field parameters had stabilized and 3-volumes of water had been purged from the well (described in the Groundwater Sampling and Analysis Plan (SAP) for Post Closure Permit [ATK, 2005a]), the sample was collected directly from the pump discharge as specified in the SAP (ATK, 2005). A total of 16 wells (H and J series wells) were sampled at ATK's Promontory Facility as part ofthis demonstration, with two samples collected from each well (one HydraSleeve® sample and one conventional sample). These wells represent various depths, contaminant concentrations, and hydraulic conductivities. The selected wells range in depths from 25 feet to 165 feet. Hydraulic conductivities in these wells range from 0.11 ft/day to 311.69 ft/day. Concentrations of perchlorate range from less than the method detection limit MDL to 1490 ug/L and TCE concentrations from less than the (MDL) to 456 ug/L. Table 1 is a summary of the wells sampled along with construction details, contaminant concentrations, and hydraulic conductivities of each well (if known). Figure 2 shows the location of each ofthe selected wells. Originally 19 wells were proposed for inclusion in this study. Three wells were dropped from the sampling plan due to having dedicated systems installed at great depths. Wells J-2 and J-4 are over 300 feet deep and would require a well service contractor to remove the dedicated systems. Likewise, well M39-BI is completed with a dedicated system at a depth of near 240'. ATK Launch Systems HydraSleeve® Results Report Promontory, Utah revised April 2008 2.3 FIELD MEASUREMENTS The depth to water was measured in each well prior to sampling. The HydraSleeve® was then installed and left hanging in the well at least 24 hours prior to sampling to allow the well to reach equilibrium. The well was then sampled with the HydraSleeve® from the center of the screened interval or saturated interval if the static water level was below the top ofthe screened interval. Measurements of traditional well stabilization parameters were made during conventional sampling. These parameters included groundwater temperature, pH, and specific conductance (see Table 2). These measurements along with the total volume purged, the time spent purging, and the average pump rate for each well were summarized and recorded in a field notebook. 2.4 ANALYTICAL METHODS All samples were analyzed for volatile organic compounds ("VOCs") by EPA Method 8260, perchlorate by EPA 314, and metals by EPA Method 6010. All analyses were performed by the ATK Environmental Laboratory in accordance with their Laboratory Quality Assurance Plan (ATK, 2005b). 2.5 QA/QC SAMPLE COLLECTION Quality Assurance/Quality Control (QA/QC) samples were collected as part of this evaluation, including trip blanks, equipment blanks, field blanks, and blind duplicates. The purpose of these samples and the methods of their collection are outlined below. , 2.5.1 Trip Blanks A trip blank is a saraple of distilled and/or deionized, organic-free water preserved with hydrochloric acid provided in three VOC bottles. Trip blanks were prepared only for the analysis of VOCs and were subjected to the same handling as the other samples. Trip blanks serve to identify contamination from sample containers or ATK Launch Systems ": HydraSleeve® Results Report Promontory, Utah ' revised April 2008 transportation and storage procedures. One trip blank was submitted for every 20 wells sampled (i.e., one trip blank as part of this demonstration). 2.5.2 Field Blanks Field blanks consisted of empty, clean sample containers filled with the distilled or deionized water used for equipment blanks. The field blank container was sealed and carried through the same handling, shipping, and analytical procedures as the primary sample. The purpose of field blanks is to verify that the environment was free of contaminants during sampling. A field blank was collected at a frequency of 1 for every 10 wells sampled (i.e., two field blanks total for this project). 2.5.3 Equipment Blanks Equipment blanks were collected and analyzed to determine if contamination was being introduced into samples by the sampling equipment. One equipment blank was collected for each 10 field samples. The HydraSleeve® equipment blanks were collected- by first filling a new HydraSleeve® with distilled water. The water was then removed from the HydraSleeve®, placed in the appropriate sample bottles, and analyzed for the constiments sampled in groundwater. 2.5.4 Field Duplicate Samples . Field duplicate and regular samples were collected simultaneously, from the same sample interval, and treated in an identical manner during storage, transportation, and analysis. Field duplicate samples were collected at a frequency of 1 for each 10 samples. ATK Launch Systems HydraSleeve® Results Report Promontory, Utah revised April 2008 3.0 SAMPLING RESULTS AND COMPARISON 3.1 DATA PRESENTATION Field measurements collected during sampling activities can be found in Table 2. Laboratory analytical results are included in the appendices ofthis report. 3.2 SAMPLING RESULTS COMPARISON For this report, the data were evaluated by comparing the HydraSleeve® data with the conventional 3-volume purge method using conventional statistical methods. These methods were applied with the objective of identifying general trends or tendencies present in the data sets. Overall conclusions related to sampler performance were made based on these statistics. The analytical data set was subdivided into the following categories for comparison purposes: 1. All data combined 2. All Metals a. Barium b. Chromium c. Lead d. Manganese e. Zinc 3. All VOCs a. TCE b. Toluene 4. Perchlorate The 3-volume to HydraSleeve® comparison was performed for each of the analytical groups and subgroups listed above, resulting in a total of 11 dataset "comparisons. The quantitative evaluation processes described in Section 3.3 were applied to each of these 11 comparison instances. The results of these quantitative comparisons were then considered using a qualitative review to derive final conclusions about each specific comparison. ATK Launch Systems HydraSleeve® Results Report Promontory, Utah revised April 2008 Prior to applying the statistical analysis tools, the datasets used for comparison were evaluated by the criteria listed below. • Instances where both results being compared were not detected (e.g., zinc was not detected in either the 3-volume purge or the HydraSleeve® samples) were not evaluated further. • For instances where a result was not detected (ND) at the method detection limit (MDL) using one sampling method, and the corresponding result using the other sampling method was a detected value, a value of one-half of the MDL was used for the ND measurement in the statistical analyses. 3.3 CONVENTIONAL STATISTICAL ANALYSES The distribution of the data was evaluated in order select the most appropriate statistical methods to apply to the data. Conventional statistical methods were then selected and used to evaluate the data sets that were being compared. 3.3.1 Data Distribution Each of the data sets was tested for normality in order to determine whether parametric or non-parametric statistical tests were appropriate for the data analysis. The Shapiro-Wilk's W test and the Lilliefors test were used to determine data distribution. Several groupings of data were evaluated for normality as described below. Initially, data sets for both of the sampling methods were tested for each of the different compound groupings (all data combined, metals only, VOCs, etc.). Since the difference between two sampling methods was the end-use ofthe data for comparison purposes, the Shapiro-Wilk's W test was applied to the populations of differences between two sampling methods being compared. As an example of this variance of normality testing, (e.g., all Barium concentrations at well J-l at the same sample depth using the 3-volume purge and HydraSleeve® sampling methods), the difference between those two concentrations was calculated. After the differences were ATK Launch Systems HydraSleeve® Results Report Promontory, Utah revised April 2008 calculated fpr all possible comparisons of analytical resuhs obtained using those two sampling methods, the Shapiro-Wilk's W test or the Lilliefors test was then applied to that population (e.g., 3-volume versus HydraSleeve® for VOCs only). The Shapiro- Wilk's W test was used for data sets where N<50 and the Lilliefors test where N>50. The results of all normality tests are included in Appendix A. Tests for normality failed (i.e., data sets are not normally distributed) for all of the data subsets evaluated. The overall lack of normally-distributed data sets supports the use of nonparametric statistical tools as described below. 3.3.2 Wilcoxon Matched-Pairs Signed Ranks Test The Wilcoxon Matched-Pairs Signed Ranks Test (Wilcoxon test) was applied to determine if two dependent variables (e.g., 3-volume and HydraSleeve® analytical results) represent two different populations. The Wilcoxon test is a nonparametric procedure used in hypothesis testing when one or more ofthe assumptions of the students paired ttest (e.g., normal population distributions) are violated. The Wilcoxon test determines if the median ofthe differences between the pairs of data (e.g., the 3-Volume measurement and the HydraSleeve® measurement for a given'well [ D9 ]) is equal to zero. If a significant difference is obtained, it indicates that there is a high likelihood that the two data sets represent different populations. A test statistic (the Wilcoxon T statistic) is calculated and associated with a p- value (and corresponding confidence level). For example, a Wilcoxon T statistic that resulted in a p-value of 0.03 would correspond to a confidence level of 97 percent that the two samples represent two different populations. Table 3 includes summaries of the results of the Wilcoxon test analyses. Values presented in this table are the confidence level (i.e., 1 minus the p-value) that the two sampling methods represent different populations. For this analysis, if the confidence was ATK Launch Systems HydraSleeve® Results Report Promontory, Utah revised April 2008 greater than 90 percent, the two populations were deemed to be different at a statistically significant level. 3.3.3 Sign Test The sign test is a nonparametric altemative to the smdents paired t-test for dependent samples. The test is applicable to situations where the investigator has two measures (e.g., under two conditions) for each subject and wants to establish whether or not the two measurements (or conditions) are different. The only assumption required by this test is that the underlying distribution ofthe variable of interest is continuous; no assumptions about the nature or shape of the underlying distribution are required. The test simply computes the number of times (across subjects) that the value of the first variable (A) is larger than that of the second variable (B). Under the null hypothesis, which states that the two variables are not different from each other, this is expected to be the case about 50 percent of the time. Based on the number of observed cases where A is greater than B, a p-value and associated confidence level can be calculated for the data set. Table 3 includes summaries of the results of the sign test analyses. Values presented in this table are the confidence that the two sampling methods represent different populations. For this analysis, if the confidence was greater than or equal to 90 percent, the two populations were deemed to be different at a statistically significant level. The results of the sign test also indicate the percentage of times that non-equal values are greater than or less than the comparative set of values (i.e., the percent of times that values in population A were greater than values in population B). 3.3.4 Linear Regression In addition to the traditional statistical tools discussed previously, two other quantitative tools were used to compare the various combinations of data sets. The results for each sampling method were plotted against the corresponding results for the other sampling method using X-Y scatter plots. Best-fit linear trend lines were then fitted to 10 ATK Launch Systems HydraSleeve® Results Report Promontory, Utah revised April 2008 these data sets, and the slope and goodness-of-fit (R2) value for each line was calculated. Best-fit linear trend lines were fitted to each of the subgroups of compounds/analytes listed in Section 3.2. These plots are included in Appendix B. Slopes that are close to 1 suggest that the average correlation between the sampling method's being compared approaches a 1 to 1 ratio, whereas higher or lower slopes suggest that one sampling method is more likely to result in higher or lower concentrations than the other method. Likewise, the closer the R2 value is to 1, the better the fit of the data to the trend line, and the lower the degree of scatter of data about the best-fit linear trend line. Table 3 includes summaries of the slope and R2 values for each of the figures discussed above. The following criteria were used to determine if sample sets were similar or not. • If the slope was between 0.90 and 1.10, the two sets of sampling results were deemed to be similar. • If the slope was equal to or greater than 1.10, the sampling device represented on the Y-axis of the plot was deemed to be more likely to retum a higher-magnitude result than the sampling device represented on the X-axis. • If the slope was equal to or less than 0.90, the sampling device represented on the X-axis of the plot was deemed to be more likely to remm a higher-magnitude result than the samphng device represented on the Y-axis. Similarly, the following guidelines were applied to the R2 values: • If the R2 value was greater than or equal to 0.90, the degree of scatter ofthe data relative to the best-fit linear trend line was deemed to be low; therefore the observation made based on the slope was considered more meaningful. • If the R2 value was less than 0.90, the degree of scatter of the data relafive to the best-fit linear trend line was deemed to be significant; therefore the observation made based on the slope was considered less meaningfiil. The threshold values described above were selected somewhat arbitrarily but similar to previous studies comparing sampling methods (Parsons 2005), and were also ATK Launch Systems HydraSleeve® Results Report Promontory, Utah revised April 2008 based on a qualitative review of the data. The guidelines established for R2 values were used primarily in the qualitative evaluation. 3.3.5 Median RPD An additional quantitative analysis tool applied to the data sets is referred to as the median relative percent difference (RPD). The first step in this analysis was to calculate the RPD of each data pair using the following equation: RPD= 100*[(A-B)/{(A+B)/2}] Where: A = Result from sampling method A; and B = Result from sampling method B. A positive RPD indicates that the result from sampling method A is higher than the result from sampling method B, while a negafive RPD indicates the opposite. RPDs close to zero generally indicate that results from both sampling methods were similar. Once all the RPDs were calculated, the median of the RPDs for each data comparison group was calculated by ranking the RPD values from lowest to highest and choosing the middle value of the ranked set of calculated RPDs. If the number of RPD values was even, then the median was selected as the mean RPD of the middle two values. This median RPD was then used as an indicator of the comparability of the two sampling methods for each compound/analyte subset. A positive value for the median RPD would indicate that sampling method A results were more frequently higher than sampling method B results (the reverse is true for negative values). Additionally, the closer the median RPD is to zero, the more likely the two sampling methods retumed similar results (essentially, for every time sampling method A was greater than sampling method B, there were an equal number of times where sampling method B was greater than sampling method A). Conversely, if the median RPD is much greater than or less than zero, the more likely one sampling method was to remm results that were significantly greater than the other method. For this analysis, a median RPD value between 10 and -10 was considered to indicate that both sampling methods retumed 12 ATK Launch Systems HydraSleeve® Results Report Promontory, Utah revised April 2008 similar concentrations. As with the guideline values described for the linear regression analysis, these values were selected somewhat arbitrarily, but also were based on a qualitative review of the data. Table 3 includes a summary of the results of the median RPD analysis. 3.3.6 Qualitative Assessment Each of the statistical analyses described above was applied all of the possible comparison combinations. Ofthe 16 possible comparison combinations, 8 (50 percent) had sufficiently small populations (i.e., fewer than 5 data pairs) that the results of the stafisfical analyses are not considered to be particularly meaningful. Of the remaining 8 combinations, all 8 instances where both the conventional statisfical and other quantitative comparison tests resulted in consistent observations. If the results of each of the four quantitative comparisons were consistent for a particular comparison (as shown in Tables 3 through 5 by having consistency of all four comparative test results), the resulting observation was validated and deemed correct without fiirther review. For those instances where the results of the four quantitative analyses varied, the results of the two populations being compared were scmtinized qualitatively, and a general conclusion regarding the comparison was made. 3.4 QUALITY ASSURANCE/QUALITY CONTROL In accordance with the Work Plan (EarthFax, 2006) and as described in Secfion 2.5, QA/QC samples were collected during this sampling event. These samples included field duplicate, equipment blank, trip blank, and field blank samples. During the HydraSleeve® comparison sampling, three equipment blanks (EB) were collected. Two samples were collected on May 9"^, 2007 and one sample was collected on May ll'^ 2007. A small amount of toluene (1.1 ug/l) was detected in the 13 ATK Launch Systems HydraSleeve® Results Report Promontory, Utah revised April 2008 sample collected on May 11*. No other constituents were found. Addifionally, two field blanks (FB) were collected on May 9'\ 2007 and May lO"", 2007. No contaminants were found in the FB samples, which is an indication that ambient conditions during sampling did not affect the samples. Four trip blanks were collected during this evaluation. No contaminafion was reported for any of the constiments from the TBs. As indicated above, two duplicate samples were collected with the HydraSleeve sampler. Three additional duplicate samples were collected from the 3-volume purge samples as part of the 2"'' Quarter groundwater sampling event. HydraSleeve duplicate samples were collected at well H-3 and at well H-4. Perchlorate concentrations in well H-4 were comparable between the HydraSleeve method at 41.4 and the duplicate HydraSleeve sample at 36.9 ug/L. Well H- 3, H-3-HS, and H-3-HSD also showed results that were comparable. Results of all sampling including the QA/QC results can be found in Appendix C. 14 ATK Launch Systems HydraSleeve® Results Report Promontory, Utah revised April 2008 4.0 CONCLUSIONS The purpose of this endeavor was to evaluate the efficacy of the HydraSleeve® discrete interval no-purge sampler for use in ATK's groundwater monitoring program. The current sampling program utilizes both dedicated and non-dedicated pumping systems to collect groundwater samples for submission to the onsite analytical laboratory. These pumping systems can be expensive, time consuming, and produce contaminated groundwater for disposal. The appeal of the HydraSleeve® sampler is that the cost is minimal and the time required to collect a representative sample is greatly reduced when compared to conventional sampling methods. , Based on the statistical analyses previously mentioned, the HydraSleeve® sampler typically produced results that were similar to or more conservative (i.e., higher concentration) than the 3-volume purge method currently employed by ATK. 15 ATK Launch Systems HydraSleeve® Results Report Promontory, Utah revised April 2008 5.0 REFERENCES ATK, 2005a. ATK Thiokol Inc. May 2005. Groundwater Sampling and Analysis Plan for ^^ Post-Closure Permit. Revision 5. Promontory, Utah. ATK, 2005b. ATK Thiokol Propulsion. March 2005. Post-Closure Permit Quality Assurance Project Plan (QAPP). Appendix 4. Promontory, Utah. Parsons. 2005. Results Report for the Demonstration of No-Purge Groundwater Sampling Devices at Former McClellan Air Force Base, Cahfomia. Denver, Colorado. U.S. Environmental Protection Agency. 2000. Guidance for Data Quality Assessment. Practical Methods for Data Analysis. EPA QA/G-9. Office of Environmental Information. Washington D.C. U.S. Environmental Protection Agency. 2006. Data Quality Assessment: Statistical Methods for Practitioners. Washington D.C. 16 ATK Launch Systems HydraSleeve® Results Report Promontory, Utah revised April 2008 TABLES i « i i i i i ATK Launch Systems Promontory, Utah Revised April 2008 HydraSleeve® Resuhs Report Febmary 2008 TABLE 1. MONITORING WELL INFORMATION Well Identification H-1 H-2 H-3 H-4 H-5 H-6 H-7 H-8 H-9 H-10 J-l J-3 J-5 . J-6 J-7 J-8 Constmcfion Material PVC PVC PVC PVC PVC PVC PVC PVC PVC PVC PVC PVC PVC PVC PVC PVC Casing Diameter (in) 4 4 4 4 4 4 4 4 2 2 4 4 , 4 4 . 4 4 Screened Interval (ft) 38-48 54-64 75 - 85 92.5 - 102.5 39.5-49.5 46.5 - 56.5 120- 130 132-142 10-25 20-30 139- 149 139-149 66-76 86 -96 135-145 155-165 Well Depth (ft) 48 64 85 102.5 49.5 56.5 130 142 25 30 155 150 77 • 97 145 165 Perchlorate ^^' Concentration (ug/L) U 11.9 U 41.4, 14.5 U . U u u u 1490 U 13.7 11.5 593 U TCE ^" Concentration (ug/L) U U u . 2j , U 5j U U u u 456 U 3.9j l-5j 24.7 U Hydraulic Conductivity (ft/day) 0,66 1.38 4.17 . 298.73 6.78 1.41 55.43 0.39 O.ll 0.05 0.4 0.5 311.69 149.4 0.11 0.11 (a) Samples collected with the HydraSleeve during 2007 ATK Launch Systems Inc. Promontory, Utah HydraSleeve Results Report February 2008 Table 2 Field Parameters/HydraSleeve Samples Well ID J-1 J-3 J-5 J-6 J-7 J-8 H-1 H-2 H-3 H-4 H-4D H-6 H-5 H-7 H-8 H-9 H-10 Date 4/24/2007 4/23/2007 5/8/2007 5/7/2007 4/24/2007 4/24/2007 5/9/2007 5/10/2007 5/10/2007 5/11/2007 5/11/2007 5/8/2007 5/9/2007 5/15/2007 5/15/2007 5/17/2007 5/17/2007 Time 1200 1437 1245 1335 1406 958 1346 1040 . 1040 1410 1040 1202 1303 1009 1112 pH (pH units) 8.11 Conductivity (mohs/cm) 3.85 NOT MEASURED 7.11 7.96 7.64 4.447 3.706 3.727 NOT MEASURED 7.39 6.97 7.35 7.05 7.3 7.31 7.56 7.31 7.58 7.25 7.65 6.334 8.687 11.34 7.381 8.527 6.347 5.506 7.166 6.142 10.55 20.42 Temperature (°C) 14.6 18.9 19.6 14.8 16.4 17.3 19.7 18.5 20.2 21.6 18.5 19.2 21.5 12.5 15.2 ATK Launch Systems Promontory, Utah HydraSleeve Results Report February 2008 Table 3. Statistical Summary for HydraSleeve Sampler ATK Launch Systems, Promontory UT. Sampler A Sampler B All Data 3-Volume HydraSleeve All Metals 3-Volume HydraSleeve All VOCs 3-Volume HydraSleeve Perchlorate 3-Volume HydraSleeve Number of Comparisons 95 . 69 19 7 Number of Instances Where Sampler A>B 45 39 5 2 Number of Instances Where Sampler A<B 47 29 12 5 Number of Instances Where Sampler A = B 3 1 2 0 Statistical Tests Sign ^^' Wilcoxon ^"' 8% (51%) 30% 72% (43%) 69% 86% (71%) 78% 55% (71%) 92% Quantitative Comparitive Tests Median X-Y Scatter RPD *'' Slope (R2) ^^ 0.0 1.16(0.96) 3.4 1.25 (0.96) -13.3 1.07 (0.99) -2.0 1.0 (1.02) Comparison Sampler A Sampler B 3-Volume = HydraSleeve 3-Volume = HydraSleeve 3-Volume < HydraSleeve 3-Volume < HydraSleeve "' First value is the confidence that the popuiations are statlsticaily different. Values between 90 and 100 indicate that the two populations being corppared are statistically different. Value in parentheses indicates the percentage of times Sampler B concentration was greater than Sampler A concentration "'' Value is the confidence that the populations are statistically different. Values between 90 and 100 indicate that the two populations being compared are statistically different. <'=' RPD=Relative Percent Difference. A positive value indicates that the concentration in Sampler A was typically greater thatn the concentration in Sampler B. A negative value indicates that the concentration in Sampler B was typically greater than the concentration in Sampler A. A value between rIO and 10 indicate that the two populations are similar. '"' Slopes between 0.90 and 1.10 indicate the popuiations are similar. Slopes less than 0.90 indicate that the concentration in Sampler A was typically greater than the concentration in Sampler B. Slopes greater than 1.10 indicate that the concentration in Sampler 8 was typically greater than the concentration in Sampler A. R2 values less than 0.90 indicate a greater degree of scatter and a lower confidence that the value is meaningful. R2 values greater than 1.10 indicate a lower degree of scatter and a higher confidence that the value is meaningful. ATK Launch Systems Promontory, Utah HdryaSleeve Results Report February 2008 Barium 3-Vol Hydras /l.r 95.8 175 . 75.7 66.1 66.2 64 67.2 44.1 70 42.9 45.6 150 210 91.7 93 282 274 98.3 95.8 195 181 131 133 81.9 80.2 113 90 194 166 313 308 Sampler Sampler A>B AB 8 Table 4. Statistical Summary for Metals ATK Launch Systems, Promontory UT . Hydras 19 5 15 13 5 17 5 19 324 5 15 Sampler A"' W+ = 50.50 N = 11,p<= 88% W-= 15.50 0.123 Sign Test'"' 23% RPD <'' SLOPE'"' (27%) 86.95 1.65i0.93) Lead 3-Vol Hydras 10 29 21 10 31 29 38 38 30 29 28 27 32 27 38 35 Sampler Sampler A>B ' A<B 6 1 Wilcoxon '•" W+ = 21, W- = 7 N = 7, p <= 0.2969 70% Sign Test'"' 88% (14%) . RPD<'' 5.15 [SLOPE "" 0.47 (0.27) Manganese 3-Vol Hydras 49.2 64.9 636 1070 0.5 24.4 4.6 38.5 18.1 121 71.4 79.3 1700 2150 17.3 10.5 19.7 10.8 53.2 64.9 60.4 24.8 128 116 1.6 7.39 157 33.3 554 503 475 435 Sampler Sampler A>B AB AB A-' . Not Enough Data Sign Test'"' 0% (0%) Not Enough Data Zinc 3-Vol 23 103 " 14 17 22 39 22 5 5 35 49 29 21 43 Sampler A>B 10 HydraS 21 5 11 5 21 34 24 12 21 27 16 5 5 55.4 Sampler A<B 4 Wilcoxon '•" W+ = 77, W N = 14, p<= 86% = 28 0.1353 Sign Test"" || 82% RPD(O) (29%) 18.8 SLOPE *'" 0.01 (0.003]|| ''"' Vaiue is the confidence that the populations are statistically different. Values between 90 and 100 indicate that the two populations being compared are statistically different. '"' First value is the confidence that the populations are statistically different. Values between 90 and 100 indicate that the two populations being compared are statistically different. Value in parentheses indicates the percentage of times Sampler B concentration was greater than Sampler A concentration ATK Launch Systems Promontory, Utah HdryaSleeve Results Report February 2008 '"' RPD=Relative Percent Difference. A positive value indicates that the concentration in Sampler A was typically greater thatn the concentration in Sampler B. A negative value indicates that the concentration in Sampler B was typically greater than the concentration in Sampler A. A value between-10 and 10 indicate that the two populations are similar. '"' Slopes between 0.90 and 1.10 indicate the populations are similar. Slopes less than 0.90 indicate that the concentration in Sampler A was typically greater than the concentration in Sampler B. Slopes greater than 1.10 Indicate that the concentration in Sampler 8 was typically greater than the concentration in Sampler A. R2 values less than 0.90 indicate a greater degree of scatter and a lower confidence that the value is meaningful. ATK Launch Systems Promontory, Utah HydraSleeve Results Report February 2008 Table 5. Statistical Summary for VOCs ATK Launch Systems, Promontory UT TCE Well J-1 J-3 J-5 J-6 J-7 H-6 TCE 3-Vol . HydraS 426 456 4 0.355 3.6 3.9 1.5 1.5 16.2 24.7 5 5 Sampler Sampler A>B A<B 1 3 2= Wilcoxon '•" W-l- = 2, W- = 8 N=4, p<=0.375 63% Sign Test'"' 38% (75%) RPD "=' -3.4 SLOPE *° 1.07 (0.99) Toluene 3-Vol HydraS 1 0.105 0.105 3.5 0.7 1.8 0.105 1.1 0.75 1.1 0.8 1.6 0.9 1.9 0.105 0.9 1 0.7 2.1 2.4 Sampler Sampler A>B AB A Not Enough Data Sign Test ^°' . 0% . (0%) . TCA 3-Vol HydraS 23.3 22.1 Sampler Sampler A>B A Not Enough Data Sign Test*"' 0% (0%) > Xylenes 3-Vol 0.8 .^ Sampler A>B 0 HydraS 1.8 Sampler A<B 1 Wilcoxon *^' Not Enough Data Sign 0% Test"". (100%) '"' Value is the confidence that the populations are statistically different. Values between 90 and 100 indicate that the two populations being compared are statistically different. '*' First value is the confidence that the populations are statistically different. Values between 90 and 100 indicate that the two populations being compared are statistically different. Value in parentheses indicates the percentage of times Sampler B concentration was greater than Sampler A concentration i"^' RPD=Relative Percent Difference. A positive value indicates that the concentration in Sampler A was typically greater thatn the concentration in Sampler B.' A negative value indicates that the concentration in Sampler B was typically greater than the concentration in Sampler A. A value between -10 and 10 indicate that the two populations are similar. Slopes between 0.90 and 1.10 indicate the populations are similar. Slopes less than 0.90 indicate that the concentration in Sampler A was typically greater than the concentration in Sampler B. Slopes greater than 1.10 indicate that the concentration in Sampler B was typically greater than the concentration in Sampler A. R2 values less than 0.90 Indicate a greater degree of scatter and a lower confidence that the value Is meaningful. R2 values greater than 1.10 indicate a lower degree of scatter and a higher confidence that the value is meaningful. w ATK Launch Systems Promontory, Utah HydraSleeve Results Report April 2008 Table 6. Statistical Summary for Perchlorate ATK Launch Systems, Promontory UT Well l.D. J-1 J-5 J-6 J-7 H-2 H-4 H-5 Sampler A 3-Volume Results (ug/L) 1460 10.9 12.8 589 10.6 41.5 12.2 Sampler A>B 2 Wilcoxon *^' W-H = 3.5 N=7 W- = 24.5 p<= 0.078, 92% Sampler B HydraSleeve Results (ug/L) 1490 13.7 11.5 593 11.9 41.4 14.5 Sampler A (71%) 1 -2.0 J 1.0(1.02)1 ' ' Value is the confidence that the populations are statistically different. Values between 90 and 100 indicate that the two populations being compared are statistically different. '^' First value Is the confidence that the populations are statistically different. Values between 90 and 100 indicate that the two populations being compared are statistically different. Value in parentheses indicates the percentage of times Sampler B conc. was greater than Sampler A conc. '"' RPD=Relative Percent Difference. A positive value indicates that the concentration in Sampler A was typically greater thatn the concentration in Sampler B. A negative value indicates that the concentration in Sampler B was typically greater than fhe concentration in Sampler A. A value between -10 and 10 indicate that the two populations are similar. '"'' Slopes between 0.90 and 1.10 indicate the populations are similar. Slopes less than 0.90 indicate that the concentration in Sampler A was typically greater than the concentration in Sampler B. Slopes greater than 1.10 indicate that the concentration in Sampler B was typically greater than the concentration in Sampler A. R2 values less than 0,90 indicate a greater degree of scatter and a lower confidence that the value is meaningful. R2 values greater than 1.10 indicate a lower degree of scatter and a higher confidence that the value is meaningful. ATK Launch Systems HydraSleeve® Results Report Promontory, Utah revised April 2008 FIGURES [~^] Bear Lake Miles 0 10 20 30 FIGURE 1. SITE LOCATION MAP «f',l ' --w Xf ^*.V i 1 1 ! \ 1 J-8, ' - ^ J-- , .'!, ' ' / •l'l. I '--.f "I ^. t-.il •i ! i I; H-7 r" ' ':^r^'KJ:i. •-:^./^^fl^"i s^ ^ ^Iv -:?;?-:••: „l... _.-fV-^ H-3 t; ^,v ,^ . ..i .. . ; .. 'H-2 ^-- 4- :?-Vl i ^-i ^X-k:i^^:- • „.,„.. /r-> .. .... :-.-i.i .•....'- -....:|...-...;.. .. 1 !— , . '..l:'-:^:; i23r^;<- r"-...<:••; -- 2li •••" .. 2:. .J. ?r:.-.; j r 1 • v: ,—,....^...|_. ||^.;?--^^"jk«r;.l;:,|, • :x - 1^*^-^ •• ..„Lis;i' -•>. .-i,.^ ^•^i" ™r*^ ..-•-<fr-^:: H-10 LEGEND 9 MONITORING WELL EVALUATED WITH THE HYDRASLEEVE H-9 fM • • FIGURE 2. MONITORING WELLS SAMPLED DURING STUDY ATK Launch Systems HydraSleeve® Results Report Promontory, Utah revised April 2008 APPENDIX A TEST FOR NORMALITY EARTHFAX ENGINEERING, INC. ENGINEERS / SCIENTISTS PROJECT I^ZZ't.^ COMPllTFn /*-*^ O ruFr.tern _ PAGE— _ DATE _ _ DATE _ / OF / 'Darrc 5>r-& /0> SO - AU- tAi^rA. Az-t_ MeT/H-5 CKrOAUU.**A. LcfWO /V\.AiOCvA:*^e.5cr SiucJtnZ AL.U V^C PA-TTV T2LG- i A: l/i'efZrS Te^r - ShA.p'ie> -uJiiicTi^r K3 AJrtLAA.»Vt_ AJor AJoe*t/^.#4-C_ '^^ (PS l(p n ^ iu> z 9~ W 1^ s IO I I I 7 OATT*.- VO G^at^^ou AJcrrS)i3Cxj«»+t DATiV TO e'i'A^.c*A-Te5 J /JOT e-Oco-t^A fl n /Uja'VO » •fc.t^ Sd.=. 69.34. 57«^=.O.fc5^ Sl^^.rtjvt/t; ce*? <l^/65.5-V-. 0.867 MSA^ - 3.^5 sa =• 43.7 Slo/x.^o.9i6, ff r-nsr - Mevtoo lL7-(p SA-;Z8.iW Sl«fe_^0.%*?/ StV^iiaoLJ-as^T Cu <ro.s-) =.o.-7foz. 1 • ATK Launch Systems HydraSleeve® Results Report Promontory, Utah revised April 2008 APPENDIX B LINEAR REGRESSION PLOTS All Data ATK Launch Systems 2500 2000 c n C a> u c o o > 0) ® 500 (0 (0 •o v=1.1584x-9.2268* R^ = 0.961^--^^^ • ^^ ^^^^ w -^^^ • 0 r^^i^ • 1 200 400 1 600 1 800 1 1000 1 1 1 1200 1400 1600 18 1500 1000 -500 3-Volume Purge Concentration (ug/L) All Metals 2500 ^ 2000 3^ O 1500 ra 4-> C o c 1000 o o 0) > ii 500 (0 ra y=1.2509x-17.884^ R^ = 0.958^,^'— • ^^y^^"^ ^^^^ 0 rr^:^ 200 <• x"'^ • 1 400 1 600 1 800 1 1000 1 1200 1 1 . 1400 1600 18 -500 3-Vol Purge Concentration (ug/L) All VOC'S ATK Launch Systems 500 450 400 y = :1.0686x +0.1544 R' = 0.9993/ ^^ ^^ ^^ ^^ ^^ ^^ ^^ wf- 1 \ 1 1 ' 1 1 1 1 -J "3) _3_ C _o S u c O o o (0 2 •o > X 350 300 250 200 150 100 50 0 50 100 150 200 250 3-Vol Purge Concentration (ug/L) 300 350 400 450 Perchlorate 1600 1400 D> 3 C o ra t-*•• c o o c o o o 5: 0) o if) ra •o >* 120U 1000 800 fiOO 400 200 0 y = 1.0188X-•0.1559 /^ ^/ ^^^ ^^ /^ ^^ -^. ^ 1 .—1 1 ^—1 1 200 400 600 800 1000 3-Vol Purge Concentration (ug/L) 1200 1400 1600 BARIUM 350 300 • y = u.sBJbx + 11 .t)U 1 , R^ = 0.§399^^ • * ^x^^ ^^ \y^ • >^ ^ • • -- -• -•. 1 -• 1 1 1 i 250 3 'C ,o ra c 200 0) o c o ^ 150 0) > W 100 ra X 50 0 50 100 150 200 250 3-Vol Purge Concentration (ug/L) 300 350 CHROMIUM 350 300 y = 1.6505x-32.469 R^ = 0.93 3 C o 4-1 ra ii *j c o u c o o ^ > o 0) ra •o >» 250 200 150 100 50 .• • 100 150 200 -50 2(i0 3-Vol Purge Concentration (ug/L) LEAD 40 35 3, 30 c • g ra 25 4-1 C o c 20 o o 0) (0 2 10 > z 0 • • ^^r- y = 0.465x +14.748 • ^^-^^ ) \ - 1— 1 1 1 1 ' 10" 15 20 25 3-Vol Purge Concentration (ug/L) 30 35 40 2500 1 ^ 2000 - 3" "o) 0 1500 n 2 +j • c • 0 c 1000 0 > 0 i> 500 - (/) ra •0 > ( -500 - MANGANESE y=1.2664x-15.209 R^ = 0.9634,^^ • ^^,1^*''^ ) 200 400 600 800 ' 1000 1200 3-Vol Purge Concentration (ug/L) s 1400 1600 18 00 ZINC 60 J 50 c .2 40 4-1 ra I. +rf c 0) c 30 o O 0) > o o 20 V) ra k. •o > ^ 10 , • • • ' • • • • • • !••• — ' • • r- • [ v = 0.0096x +18.449 R" = 0.0003 1 ••• I 0 20 40 60 80 3-Vol Purge Concentration (ug/L) 100 120 TCE 500 450 d 400 3^ ^ 350 o 2 300 c o C 250 o o ©200 0) 4) to 150 ffi im •o >» 100 50 y = 1.0696X +0.5697 R = 0.9996/ ^^ ^^ ^^ ^^ ^^ ^ ^^ >^ 50 100 150 200 250 300 3-Vol Purge Concentration (ug/L) 350 400 450 TOLUENE • • • • • •• • y = 0.0219x +1.4939 R^ = 0.0002 • . 1 1 1 1 3.5 3- ^ c o '"§ 2.5 c g 2 o o 0) > 0) V) ra im •a z 1.5 0.5 0.5 1 1.5 3-Vol Purge Concentration (ug/L) 2.5 ATK Launch Systems HydraSleeve® Results'Report Promontory, Utah revised April 2008 APPENDIX C LABORATORY ANALYTICAL DATA CERTIFICATE OF ANALYSIS Listing of Sample Infornnation and Testing Requested Wednesday, May 16, 2007 TESTED FOR: ATK Thiokol: DLV Environmental Monitoring MS 301 Thiokol Corp, UT 84322 ANALYZED BY: ATK Thiokol Propulsion Environmental Laboratory P.O. Box 707, M/S 245 Brigham City, UT 84302-0707 435-863-3732 435-863-8080 Contact Name: Project: Sample Delivery Group: Dave Covington Ground Water Testing - DLV 0705012 Page 1 of 9 Sample Delivery Group: 0705012 Sample No. Client No. Test Requested EPA 314.0 SW-846, 3010A SW-846, 6010B (Water) SW-846, 7470A SW-846, 8260B (Water) Sample Description Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Received Collect Date/Time Matrix ' 0705012-01 2164-Trip Blank SW-846, 82608 (Water) 0705012-02 2165-J.BHS Volatile Organic Analysis 05/07/07 4/25/2007 10:21:26 Water 05/07/07 4/25/2007 13:51:26 Water Water Water Water Water 0705012-03 2166-J-8 05/07/07 4/25/2007 14:33:26 EPA 314.0 SW-846! 3010A SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water Certified By: ' W. Scott Fraser, Quality Assurance Officer 05/16/2007 Date Ttiis certifies ttiat ttie following data meets the requirements of thie National Erivironmenfal Laboratory Accreditation Program (NELAP) unless ottierwise annotated: Page 2 of 9 Listing of Results by Sampie Sample Delivery Group: 0705012 Client Sample ID: 2164-Trip Blank Sample Description: • ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705012-01 DateSampled: 04/25/07 10:21 CAS Number i Tesf Method: 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1. 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1^ 106-46-7 75-71-8 • 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 Test Parameter SW-846, 8260B (Water) Volatile Org ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZEhJE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1.2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE . 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-111 RACHLOROETHANE Result Units u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L. ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . ug/L ug/L ug/L DL 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 . 0.16 0.2 0.13 0.27 0,16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 Dilu EQL Fac 100 1 10 1 10 1 10 1 10 1 10 • 1 10 1 10 1 10 10 1 10 1 10 .10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 . ' 10' 10 10 10 10 10 10 10 10 10' 10 10 io' •10 10 10 10 10 10 • 10 10 10 10 • 10 lon tor Analvst LSH LSH LSH LSH LSH LSH LSH LSH :. LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 . LSH 1 LSH 1 " LSH 1 LSH 1 LSH 1 . LSH Test Date 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07- 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 • 05/08/07 05/08/07 05/08/07 05/08/07 .05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 • 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 Page 3 of 9 Listing of Results by Sample Sample Delivery Group: 0705012 Client Sampla ID: 2164 - Trip Blank Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705012-01 DateSampled: 04/25/07 10:21 CAS Number Test Parameter Result Test Metliod: ' SW-846, 82608 (Water) Volatile Organic Analysis 127-18-4 TETRACHLOROETHENE 108-88-3 TOLUENE 87-61-6 1,2,3-TRICHLOROBENZENE 120-82-1 1,2,4-TRICHLOROBENZENE 71-55-6 1,1,1-TRICHLOROETHANE . 79-00-5 1,1,2-TRICHLOROETHANE 79-01-6 TRICHLOROETHENE 75-69-4 TRICHLOROFLUOROMETHANE 96-18-4 1,2.3-TRICHLOROPROPANE 95-63-6 1,2,4-TRIMETHYLBENZENE 108-67-8 1,3,5-TRIMETHYLBENZENE 108-05-4 VINYLACETATE 75-01-4 VINYLCHLORIDE 1330-20-7 m!p-XYLENE 95-47-6 o-XYLENE 460-00-4 BROMOFLUOROBENZENE 1868-53-7 DIBROMOFLUOROMETHANE 17060-07-0 1,2-DICHLOROETHANE-D4 2037-26-5 TOLUENE-DB Units sis U U U U U u u u u u u u . u u u 105 103 107 98.4 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 .0.29 0.13 0.3 1.6 0.18 EQL 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 Diluti Fac sr Analvst Test Date ... LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 , 05/08/07 05/08/07 05/08/07 05/08/07 • 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 Client Sample ID: 2165-J-8 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705012-02 Date Sampled: 04/25/07 13:51 CAS Number "TestMeiltod: 014797-73-0 fast Metliod: Test Meihod: Test Parameter EPA 314.0 PERCHLORATE SW-846, iOlOA " ' 3010A ACID DIGESTION Result Units Perctilorate - lon Chromatograptiy U ug/L Metals Digestion 05/08/2007 10:30 MDL Dilution EQL Factor Analvst Test Date KEN MTB 05/15/07 05/08/07 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 Test Metliod: 7439-97-6 TestMethod; 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 SW-846, 6010B (Water) ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC SW-846, 74T0A MERCURY SIV-S46, 8260B flVater) Volatile Organic Analysis ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE Metals Analysis by ICP - 6010 U 45.6 U 13. J' U 79.3 U U 34. J ug/L- ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Mercury Analysis 20 2 1 10 20 1 1 30 10 100 10 5 50 100, 5 5 150 50 MTB MTB MTB MTB MTB MTB MTB MTB MTB 05/09/07 05/09/07 05/09/07 05/09/07 05/09/07 05/09/07 05/09/07 05/09/07 05/09/07 U ug/L 0.3 TCP 05/11/07 U u u u u ug/L ug/L ug/L ug/L ug/L 30 0.22 0.31 0.19 0.37 100 10 10 10 10 LSH LSH LSH LSH LSH Page 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 4 of 9 Listing of Results by Sample Sample Delivery Group: 0705012 Client Sample ID: 2165-J-8 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705012-02 DateSampled: 04/25/07 13:51 Dilution CAS Number ; TestMethod; • 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 .106-43-4 124-48-1 96-12-8 . 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 . 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 • 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 Tost Parameter Result SW-846, 8260B (Water) Volatile Organic Analysir BROMOFORM BROMOMETHANE 2-BUtANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUEKIE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE • ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENECHLORIDE 4-METHYL-2-PENTANONE -, NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1.2.3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE • :i,1,1-TRICHLOROETHANE U U U U U U U U U U U U U u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L- ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L • ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 0.42 0.57 1.11 0.3 0.16 0.2. 0.13 0.27 0.16 0.35 1.71 0.3. 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 . 0.16 0.16 0.34 0.16 0.24 • 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 . 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 EQL Fac 10 1 10 1 10 1 • 10 1 10 1 10 • 1 10 1 10 1 - 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 10 10 10 10 10 10 10 ' 10 10 10 10 10 10 10 10 10 10 10 IO- IO 10 10 10 10 10 10 10 10 10 10 10 10 IO- IO tor Analvst LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 1 LSH 1 LSH 1 LSH 1 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 1 LSH 1 LSH LSH 1 LSH 1 LSH Test Date • 05/08/07 • 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07, 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 - 0'5/08/07 05/08/07 05/08/07 ' 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 .05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 Page 5 of 9 Listing of Results by Sample Sample Delivery Group: 0705012 Client Sample ID: 2165-J-8 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705012-02 Date Sampled: 04/25/07 13:51 Dilution CAS Number testMethod2 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-0S4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter Result SW-846, 8260B (Water) Volatile Organic Analysis 1,1,2-TRICHLOROETHANE U TRICHLOROETHENE U TRICHLOROFLUOROMETHANE U 1,2,3-TRICHLOROPROPANE U 1,2,4-TRIMETHYLBENZENE U 1,3,5-TRIMETHYLBENZENE U VINYLACETATE U VINYL CHLORIDE U m.p-XYLENE U o-XYLENE U BROMOFLUOROBENZENE 106 DIBROMOFLUOROMETHANE 104 1,2-DICHLOROETHANE-D4 105 TOLUENE-D8 98.2 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDLr "• T'.' T 0.25 , 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 . EQL 10 10 10 10 10 10 10 10 10 10 Factor 'Z..Z. Analyst 'I... Ill LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date j 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 . 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 Client Sample ID: 2166-J-8 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705012-03 Date Sampled: 04/25/07 14:33 CAS Number "' YestMethodr 014797-73-0 , test Metttod: Test Parameter Ef>A314.d PERCHLORATE SW-846, 3010A Result , Units Perchlorate - Ion Chromatography MDL Dilution EQL Factor Analvst Test Date U ug/L Metals Digestion 05/08/2007 10:30 TestMethod: 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 TestMethod: 7439-97-6 TestMethod: 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 3010A ACID DIGESTION SW-846, 6010B (Water) Metais Analysjs by ICP - 6010 ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC KEN MTB 05/15/07 05/08/07 u 42.9 U 33. J U 71.4 U U 39. J ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L .,_,..„ 20 2 1 10 20 1 1 30 10 '...\.17f 100 10 5 50 100 5 5 150 50 11,...' l'.'l_.'^'" MTB MTB MTB MTB MTB MTB MTB MTB MTB .; ......J 05/09/07 05/09/07 05/09/07 05/09/07 05/09/07 05/09/07 05/09/07 05/09/07 05/09/07 SW-846, 74T0A MERCURY SW-846, 8266B (Water) Mercury Analysis U ug/L 0.3 Volatile Organic Analysis TCP 05/11/07 ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 30 0.22 0.31 0.19 0.37 0.42 0.57 i.ir 0.3 0.16 100 10 10 10 10 10 10 10 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/08/07 - 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 Page 6 of 9 Listing of Results by Sample Sample Delivery Group: 0705012 Client Sample ID: 2166-J-8 Sample Description': ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705012-03 DateSampled: 04/25/07 14:33 CAS Number ; TesiMeWod: 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 • 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100^1-4 591-78-6 87-68-3 98-82-8 99-87-6 • 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 Test Parameter " SiV-M6, 82iS0B (Water) Volaie Organic TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE . CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER , CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE . 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE 1,1,2-fRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE . 1,2,4-TRIMETHYLBENZENE Result ; Analysis U U U U U u u u u. u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug'L ug/L ug/L ug/L ug/L ug/L ' ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81. 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 o:i6 . 0.25 0.71 0.25 0.33 0.19 Dilui [L Fac .... . 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 ' 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 ion lor Analvst LSH LSH LSH LSH LSH LSH LSH LSH LSH . LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 1 LSH 1 . LSH 1 LSH 1 LSH 1 LSH t LSH 1 LSH 1 LSH Test Date : i 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 Page 7 of 9 Listing of Results by Sample Sample Delivery Group: 0705012 Client Sample ID: 2166-J-8 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705012-03 Date Sampled: 04/25/07 14:33 CAS Number Test Method; 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter Result SW-846, 8260B (Water) Volatile Organic Analysis 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m.p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 TOLUENE-D8 U u u u u 104 104 105 97.9 Units ug/L ug/L ug/L ug/L ug/L % % % % ek 1 0.29 0.13 • 0.3 1.6 0.18 EQL 10 10 10 10 10 Dilution Factor "••••""•^•- Analvst LSH LSH LSH LSH LSH LSH - LSH LSH LSH Test Date 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 Page 8 of 9 Data Reporting Qualifiers U Indicates that ttie analyte was not detected, or the analyte was detected but was below the MDL. B This flag is used when an analyte Is found in the blank as well as the sample. Indicates an extimated value. This flag is used either when estimating a concentration for tentatively identified compounds or when the data indicated the presence of a compound that meets the identification criteria but the result Is less than the EQL (e.g. 3 J with an EQL of 10). MDL Method Detection Limit: The minimum concentration of a substance that can be confidently measured and reported. The laboratory has demonstrated that the MDL can be achieved In a laboratory reagent blank, but does not guarantee It can be achieved in ail sample matrices. EQL Estimated Quantitation Limit: The EQL generally Is 5 to 10 times the MDL. For many analytes the EQL is selected as the value of the lowest standard In the caiibration cun/e. Dilution Dilution Factor: The prepared sample was diluted by this factor because the Factor sample was too concentrated or due to other Interferences in the sample matrix. Any dilution factor causes a corresponding increase in the MDL and EQL. Page 9 of 9 ATK Launch Systems Group Environmental Laboratory OVPS-Qi^ Client Name:. . no coaler Q Hand delTvered, sami Sample Receipt Checklist SDG No. ^7c^2^i)r^ Carrier: Q Hand delivered, no coaler Carrier Number: sample(s) taken out at receiving counter ///? Cooler Information: Cooler Nuinber/ID ^<Ji UJkA-U^ Condition ot Shipping Container: Cooler Sealed (taped): Cuslody Seals Present: Coolant: State ot Coolant; p^ood •Yes QYes Qlntact aice QFrozen QFair lo •Broken •Blue Ice i)^< QNot Applicable •Not Applicable •Not Applicable •Damaged (explain). Thermometer ID: 4l^Lit}*f Reading;_5__°C Packing Description: lone •Partially Frozen CF:; Seal Number: Other: •Melted Corrected Temp:_ Temp Blank Included: QYes QNo Chain-0(-Custody Information: COC Present: z' ,^^,/.>r M^^^ COC Nliimhar/sV K. /Z VW C. COC signed (relinquished and received): Jyes COC or LW I agrees with sample labels: f^i as •No •No •No Other: •Not Applicable •Not Applicable NotB.'!- Sample Information: Samples included in cooler: 07 oS^r^L^ t Custody Seals Present: Sample containers intact: Samples in proper containers: Sufficient sampte volume: •Yes •Intact ^es ^es f^n Other All samples received in hold time: jHe^ Water - VOA's have zero headspace: BPre-presarved with HCI: Notes: •Broken Seal Number(s). •No Notes: •No •No •No ^es QNo •Not Applicable •Pre-preserved with NaaSad: •Non-Preserved: )^es QAdjusted (see comments below) QNot Applicable • NaOH = ZnAC /NaOH = Water - pH acceptable upon receipt: HNO, =. _HjSO, = _HCL = Water - pH adjusted: (mfg. & Lot No.) HNOj, HzSO,. NajSOA Notes: _NaOH . ZnAC. _HCI Other SOP-102Form A 0705012 ENVIRONMENTAL LAB WORK REQUEST TO TfflOKOL ENVIRONMENTAL LABORATORY FROM: Dave Covington ORGANIZATION: . Environmental Services EXTENSION: 3898 MAILSTOP; 301 COST CENTER: 8200 LWR No. E12742 Login No. WORKORDER: 988P LS333 GW DATE: 05/07/07 REPORT RESULTS TO: HELEN RAVSTEN, MS 301 SAMPLE INFORMATION SAMPLE /. 2164 2165 2166 DATE 4-25-07 4-25-07 4-25-07 TYPE G C LOCATION Trip Blank J-8HS J-8 TIME 10:21 13:51 14:33 TEST VOA (Method 8260) Perchlorate, Metals, (Method 6010), Voc's (Method 8260) '- . REMARKS ||;iftS;hi;V^,sn, • CHAIN OF CUSTODY RELINQUISHED BY DATE TIME RECEIVED BY DATE TIME ^^y^^y ^'Ir^ y<V/&^ s- 7'Or ^€3^ FOR LABORATORY USE ONLY DATE COMPLETED DATE REPORTED 1 i^=^^i^=a= jl SIGNATURE CERTIFICATE OF ANALYSIS Listing of Sarnple Information and Testing Requested Tuesday, May 22, 2007 TESTED FOR: ATK Thiokol: DLV Environmental Monitoring MS 301 Thiokol Gorp, UT 84322 ANALYZED BY: ATK Thiokol Propulsion Environmental Laboratory P.O. Box 707, M/S 245 Brigham City, UT 84302-0707 435-863-3732 435-863-8080 Contact Name: Project: Sample Delivery Group: Dave Covington Ground Water Testing - DLV 0705015 Pagel of 16 Sample Delivery Group: 0705015 Sample No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 0705015-01 2167-J-6 HS 05/08/07 5/7/2007 12:33:04 EPA 314.0 SW-846, 301 OA SW-846, 6010B (Water) SW-846, 7470A SW-846, 82606 (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705015-02 2168-J-6 05/08/07 5/7/2007 13:13:04 EPA 314.0 SW-846, 301 OA SW-846, 6010B (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705015-03 2169-J-6 D 05/08/07 5/7/2007 13:13:04 EPA 314.0 SW-846, 30IOA SW-846, 6010B (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705015-04 2170-FB 05/08/07 5/7/2007 13:30:04 EPA 314.0 SW-846, 301 OA SW-846, 6010B (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705015-05 2171 -EB 05/08/07 5/7/2007 12:37:04 EPA 314.0 SW-846, 3010A SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705015-06 2172-J-5 HS 05/08/07 5/7/2007 14:40:04 EPA 314.0 SW-846, 301 OA SW-846, 601 OB (Water) SW-846, 7470A Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Water Water Water Water Page 2 Of 16 Sample Delivery Group: 0705015 Sample No. Client No. Test Requested 0705015-06 2172-J-5 HS SW-846, 8260B (Water) Sample Description Volatile Organic Analysis Received Collect Date/Time Matrix 05/08/07 5/7/200714:40:04 Water Certified By: W. Scott Fraser, Quality Assurance Officer 05/22/2007 Date Ttiis certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation Program (NELAP) unless otherwise annotated: Page 3 of 16 Listing of Results by Sample Sample Delivery Group: 0705015 Client Sample ID: 2167 - J-6 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample 10: 0705015-01 DateSampled: 05/07/07 12:33 CAS Number • fesiUetiiod2 014797-73-0 TestMethod: TestMethod: ^ "" 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 fesi Metfiod; 7439-97-6 Test Meiiiod: 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 Test Parameter 'EPAHATf 'f PERCHLORATE SliV-'846,'3dldA' 3010A ACID DIGESTION Result Units Perchlorate - lon Chromatography 11.5 ug/L Metals Digestion MDL 05/09/2007 09:00 SW-846, 6010B (Water) ARSENIC BARIUrvl CADH^IUIUI CHROtVllUM LEAD MANGANESE SILVER TIN ZINC 'SW-846,'7470A MERCURY "'SW-846, 826dB (Water) Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE u 67.2 u u U 38.5 3.6 J 39. J U ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L U ug/L u U U u u u u u u u u u u u u u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Dilution EQL Factor Analvst Test Date JMM 05/18/07 MTB 05/09/07 20 2 1 10 20 ' 1 1 30 10 0.3 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 100 10 5 50 100 5 5 150 50 1 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 MTB MTB MTB MTB liflTB MTB MTB MTB MTB TCP LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/15/07 05/15/07 05/15/07 05/15/07' 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/11/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 Page 4 of 16 Listing of Results by Sample Sample Delivery Group: 0705015 Client Sample ID: 2167-J-6 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705015-01 Date Sampled: 05/07/07 12:33 CAS Number Test Parameter festMediod:f ' SW-846, 8260B CWater) ' Volatile Organic A^lysis 156-59-4 CIS-1,2-DICHLOROETHENE 156-60-5 TRANS-1,2-DICHLOROETHENE 78-87-5 1,2-DICHLOROPROPANE 142-28-9 1,3-DICHLOROPROPANE 563-58-6 1,1-DICHLOROPROPENE 10061-01-5 CIS-1,3-DICHLOROPROPENE 10061-02-6 TRANS-1,3-DICHLOROPROPENE 590-20-7 2,2-DICHLOROPROPANE 100-41-4 ETHYLBENZENE 591-78-6 2-HEXANONE ' 87-68-3 HEXACHLOROBUTADIENE 98-82-8 ISOPROPYLBENZENE 99-87-6 4-ISOPROPYLTOLUENE 75-09-2 METHYLENE CHLORIDE 108-10-1 4-METHYL-2-PENTANONE 91-20-3 NAPHTHALENE 103-65-1 N-PROPYLBENZENE 100-42-5 STYRENE 630-20-6 1,1,1,2-TETRACHLOROETHAN E 79-34-5 1,1,2,2-TETRACHLOROETHANE 127-18-4 TETRACHLOROETHENE 108-88-3 TOLUENE 87-61-6 1,2,3-TRICHLOROBENZENE' 120-82-1 1,2,4-TRICHLOROBENZENE 71-55-6 1,1,1-TRICHLOROETHANE 79-00-5 1,1,2-TRICHLOROETHANE 79-01-6 TRICHLOROETHENE 75-69-4 TRICHLOROFLUOROMETHANE 96-18-4 1,2,3-TRICHLOROPROPANE 95-63-6 1.2,4-TRIMETHYLBENZENE 108-67-8 1,3,5-TRIMETHYLBENZENE 108-05-4 VINYLACETATE 75-01-4 VINYLCHLORIDE 1330-20-7 m.p-XYLENE 95-47-6 o-XYLENE 460-00-4 BROMOFLUOROBENZENE 1868-53-7 DIBROMOFLUOROMETHANE 17060-07-0 1,2-DICHLOROETHANE-D4 2037-26-5 TOLUENE-D8 Result sis U U U U U U U u u u u u u u u u u u u u u 1.8 J u u . u u 1.5J u u u u u u u u 108 102 106 99.2 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L • ug/L ug/L ug/L ug/L ug/L • ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % . % % % MDL. 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 O.IS"" 0.17 0.25 0.65 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Dilution EQL Factor Analvst 10' 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH'^ 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 . LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH Test Date 05/08/07 • 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 . 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 Client Sample ID: 2168-J-6 Sample Description: ATK-DLV - Groundwater Spring 2007. Laboratory Sample ID: 0705015-02 DateSampled: 05/07/07 13:13 CAS Number TestMeOiod: 014797-73-0 test Method: Test Parameter WASIW "• • PERCHLORATE SW-846^ 30iOA 3010A ACID DIGESTION Result Units Perchlorate - lon Chromatography 12.8 ug/L Metals Digestion 05/09/2007 09:00 MDL Dilution EQL Factor Analvst Test Date JMM MTB 05/18/07 05/09/07 Page 5 Of 16 Listing of Results by Sample Sample Delivery Group: 0705015 Client Sample ID: 2168-J-6 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705015-02 Date Sampled: 05/07/07 13:13 CAS Number Test Methodic 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 TesfMet/iod; 7439-97-6 Yesr Metfiod; 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 • 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 . 142-28-9 563-58-6 10061-01-5 Test Parameter SW-846,'6010BC^ter) ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC SW-846, 7470A Result Units Metals Anaiysis by ICP - 6^10 MDL Dilution EQL Factor Analvst Test Date u 64 U U U 4.6 J U U 17. J Mercury Analysis MERCURY SIV-846, 8i26i9B (Water) Volatile Organic Analysis ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE U U U U U U U U U U U U U U U U U U U U U u U u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L U ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 20 2 1. 10 20 1 1 30 10 0.3 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 100 10 5- 50 100 5 5 150 50 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 .10 10 10 10 10 10 10 10 10 10 10 10 10 MTB MTB MTB. MTB MTB MTB MTB MTB MTB 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 TCP 05/11/07 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 Page 6 Of 16 Listing of Results by Sample Sample Delivery Group: 0705015 Client Sample ID: 2168 - J-6 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705015-02 DateSampled: 05/07/07 13:13 CAS Number • Yesr Metfiod;" 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter 'SW-846,~8260B'(Water) Volaie Organic TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m.p-XYLENE . o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 T0LUENE-D8 Result Analysis U U U u u u u u u u u u u u u 0.7 J u u u u 1.5 J U U u u u u u u 103 106 103 99.4 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71, 0.25 - 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Dilu EQL Fac 10 1 10 1 10 1 10 1 10 1 10 . 1 10 1 10 1 10 . 1 10 1 10 1 10- 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 ion lor Analvst LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 .05/08/07 05/08/07 Client Sample 10: 2169-J-6 D Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705015-03 Date Sampled: 05/07/07 13:13 CAS Number ; Yesr Metfiod; 014797-73-0 ; test Metiiod: ^ TesiMetiiod2 7440-38-2 . 7440-39-3 7440-43-9 7440-47-3 Test Parameter Result EPA 314.0 Perchlorate - lon Chromatography PERCHLORATE 13.8 SW-846,30iOA __ Metals Digestion ___ 3010A ACID DIGESTION 05/09/2007 09:00 SW.S46, 6010B (Water) Metals Analysis by ICP - 6010 ARSENIC U BARIUM 64.6 CADMIUM •' U CHROMIUM U Units M ug/L - • • • - • • ug/L ug/L ug/L ug/L Dilution EQL Factor Analvst Test Date JMM 05/18/07 MTB 05/09/07 20 2 1 10 100 10 5 50 1 1 1 1 MTB MTB MTB MTB 05/15/07 05/15/07 05/15/07 05/15/07 Page 7 of 16 Listing of Results by Sample Sample Delivery Group: 0705015 Client Sample ID: 2169-J-6 D Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705015-03 Date Sampled: 05/07/07 13:13 CAS Number " TestHleiiiodF 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 YestMetfiod; 7439-97-6 Test'Method:" 67-64-1 ' 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 Test Parameter SW-846, ediOBftVai^rj LEAD MANGANESE SILVER TIN ZINC Result Metals Analysis by ICP- 6010~ U 5.39 U 31. J 14. J Units -— ug/L ug/L ug/L • ug/L ug/L MDL • ...."•••••'•' 20 1 1 30 10 EQL 100 5 5 150 50 Dilution Factor Analvst Test Date SIV-846, 7470A MERCURY SIV-846, MMB/VVarer)' Mercury Analysis Volatile Organic Analysis U ug/L ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1 -DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 0.3 30 0.22 0.31 0.19 0.37 0.42 • 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 ' 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 '•••'• •••' 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 ! 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 MTB MTB MTB MTB MTB 05/15/07 05/15/07 .05/15/07 05/15/07 05/15/07 TCP 05/11/07 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/08/07 05/08/07 .. 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 Page 8 of 16 Listing of Results by Sample Sample Delivery Group: 0705015 Client Sample ID: 2169 - J-6 D Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705015-03 Date Sampled: 05/07/07 13:13 CAS Number TestMethod: 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95^63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter SW-846, 8260B (Water) Volatile Organ HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2.4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYLCHLORIDE m,p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DlCHLOROETHANE-D4 TOLUENE-D8 Result ic Analysis U U U u u u u u u u u u u u u u u u u u u. u u u u 103 104 106 99.7 Units ug/L ug/L ug/L ug/L • ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Dilution |L Factor Analvst 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 —- 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH Test Date 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 ' 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 Client Sample ID: 2170 - FB Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705015-04 DateSampled: 05/07/07 13:30 CAS Number " Yesr Mer/iio'd;"' 014797-73-0 Tesr Metfiod; TestMethod: 7440-38-2 7440-39-3 7440--43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 Test Parameter EPA 314.0 PERCHLORATE SW-846, 3010A 3010A ACID DIGESTION SW-846, 6010B (Water) ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN Result Perctilorate - lon Chromatography U Metals Digestion 05/09/2007 09:00 Metals Analysis by ICP-6010 U U U U U U U U Units • ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL Dilution EQL Factor Analvst Test Date JMM MTB 05/18/07 05/09/07 20 2 1 10 20 1 1 30 100 10 . 5 50 100 5 5 150 MTB MTB MTB MTB MTB MTB MTB MTB 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 Page 9 of 16 Listing of Results by Sample Sample Delivery Group: 0705015 Client Sample ID: 2170-FB Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705015-04 Date Sampled: 05/07/07 13:30 CAS Number 21esiMeiiiod~ 7440-66-6 TestMethod: 7439-97-6 JestMetfio'd:'' 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 . 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43^ 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 Test Parameter S^-846, 60408 (Water) ZINC Result tk^etals Analysis by ICP - 6010 Units MDL U ug/L Mercury Analysis SW-846, 7470A MERCURY SW-846, 8260B (Water) "" "volaliie Organic Analysis ACETONE BENZENE BROMOCHLOROMETHANE BROMOOICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLORbMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1 -DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 10 U ug/L 0.3 Dilution EQL Factor Analvst Test Date 50 u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 • 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 . 0.15 0.18- 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 MTB 05/15/07 TCP LSH LSH LSH LSH LSH , LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH. LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH : LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/11/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 . 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 • 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 Page 10 of 16 Listing of Results by Sample Sample Delivery Group: 0705015 Client Sample ID: 2170 - FB Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705015-04 Date Sampled: 05/07/07 13:30 CAS Number [ YesTMetfiodT _ 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69^ . 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 , 95-47-6 460-00^ 1868-53-7 17060-07-0 2037-26-5 Test Parameter SIV-846, 8260flJVVarer; Volatile Organic 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1 -TRICHLOROETHANE 1,1,2-TRlCHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m,p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 T0LUENE-D8 Result Analysis U U U U U U U U U U U U U u u u u u u u u 106 103 104 100 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 ' 0.33 0.19 0.29 0.13 0.3 1.6 0.18 EQL 10 • 10 10 10 10 . 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 Diluti Fac on :or Analvst Test Date • -• - LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH - -•—••I 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 Client Sample ID: 2171 - EB Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705015-05 DateSampled: 05/07/07 12:37 Dilution CAS Number : TestMethod: 014797-73-0 r TestMethod: r resrMetfiodT J 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 TestMethod: 7439-97-6 Test Parameter EPA 314.0 PERCHLORATE SW-846, 3dl6A 3010A ACID DIGESTION • SW-84:6,J0m (Water) ' ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC SW-B46, 7470A MERCURY Perchlorate - lon Metals Digestion 1 Chrom Result atography 5.39 05/09/2007 09:00 Metais Analysis by ic'p - 6010 " Mercury Analysis U U U U u u u u u u Units ug/L . . .„ ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 1 • 20 2 1 10 20 1 1 30 10 0.3 EQL 4 100 10 5 50 100 5 5 150 50 1 Factor 1 1 1 1 1 1 1 1. 1 1 1 1 Analyst JMM MTB MTB MTB MTB MTB MTB MTB MTB " MTB MTB TCP Test Date „ . i 05/18/07 05/09/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/11/07 Page 11 of 16 Listing of Results by Sample Sample Delivery Group: 0705015 Client Sample ID: 2171-EB Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705015-05 DateSampled: 05/07/07 12:37 CAS Number : TestMeOiod: _ 67-64-1 71-43-2 . 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51:8 . 135-98-8 98-06-6 75-15-0 56-23-5 . 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 .106-43^ 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 . 103-65-1 100-42-5 . 630-20-6 79-34-5 Test Parameter "SW-ai'e, 8266B~(Water) Voiatile Organk; ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE . CARBON DISULFIDE CARBON IblRACHLORIDE . CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOR9TOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLpROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE Result Analysis U U U U U u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L DL 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 Dilu EQL Fac 100 1 10 1 10- 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 10 1 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 id 10 10 10 10 10 . 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 lon tor Analvst LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH LSH LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH Test Date •'— '— • • -y 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 Page 12 of 16 Listing of Results by Sample Sample Delivery Group: 0705015 Client Sample ID: 2171-EB Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705015-05 DateSampled: 05/07/07 12:37 CAS Number I TestMeiiiod2' 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18^ 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter SW-846, 8260B (Water) Volatile Organic TETRACHLOROETHENE . TOLUENE 1.2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1; 1 -TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m.p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 TOLUENE-D8 Result Analysis U U U U U U U U U U U U U U U 108 103 105 101 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0'.3 1.6 0.18 Dilution EQL Factor Analvst Test Date 10 10 10 10 • 10 10 10 10 10 10 10 10 10 10 10 . .. LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 1 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 • 05/08/07 05/08/07 Client Sample ID: 2172-J-5 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705015-06 Date Sampled: 05/07/07 14:40 CAS Number : YesrMetfiod; 014797-73-0 : re'sr Metfiod: Test Parameter EPA 314.0 "_ PERCHLORATE "SW-846, ioioiT' f 3010A ACID DIGESTION Result Units Perchlorate - lon Chromatography 13.7 Metals Digestion 05/09/2007 09:00 MDL Dilution EQL Factor Analvst Test Date ug/L JMM MTB 05/18/07 05/09/07 Test Method: SW-846, 6010B (Water) Metals Analysis by ICP - 6010 7440-38-2 7440-39-3 7440^3-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 TesrMer/iod; 7439-97-6 lest Metiiod:' 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC ''SW-846,'"7476A f MERCURY Sm46, 8260B (Water) u 66.2 U U U 24.4 1.3J 32. J 14. J ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Mercury Analysis Volatile Organic Analysis U ug/L ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE U U U u u ug/L ug/L ug/L ug/L ug/L 20 2 1 10 20 1 1 30 10 0.3 30 0.22 . 0.31 0.19 0.37 100 10 5 50 100 5 5 . 150 50 ^ 1 100 10 10 lo 10 1 1 1 1 • 1 •1 1 1 1 1 1 1 1 1 1 MTB MTB MTB MTB MTB MTB MTB MTB MTB TCP LSH LSH LSH LSH LSH 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/11/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 Page 13 of 16 Listing of Results by Sample Sample Delivery Group: 0705015 Client Sample ID: 2172-J-5 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705015-06 Date Sampled: 05/07/07 14:40 Dilution CAS Number I TesWethod2 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 . 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 54i;73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-12-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 - 120-82-1 71-55-6 Test Parameter SW-846, 8260S (Water) "" VolaWe Organic BROMOFORM BROMOMETHANE 2-BUTANONE. N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBONDISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2.2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUErJE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE Result Analysis U U U U U U U U U u u u u u u u u u u u u u u u u u u u u u u Ll u u u u u u u u u u u u u u u 3.5 J u u u Units "••"••." ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L - ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 EQL Factor Analvst " • 10 • 1 10 1 10 1 10 1 10 1 'lo 10 10 10 10 10 10 10 10 10 10 10. 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10, . 10 10 10 10 10 10 10 10 10 10 10 10 • 10 10 10 •-• • LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 1 LSH 1 LSH 1 .. LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 ' LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH Test Date - • —1 • _^^ . J 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 • 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 Page Uof 16 Listing of Results by Sample Sample Delivery Group: 0705015 Client Sample ID: 2172-J-5 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705015-06 DateSampled: 05/07/07 14:40 CAS Number rest Metfiod;" 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter ~ SIV-846, 82608 (WaM f VolatileOrganic 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m,p-XYLENE O-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 TOLUENE-D8 Result Analysis U 3.9 J U U U U U , U 1.8 J U 105 104 106 99.3 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL EQL Diluti Fac - -""• 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 -••• 10 10 10 10 10 10 10 10 10 10 :gr Analvst Test Date LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH J 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 05/08/07 Page 15 of 16 Data Reporting Qualifiers U indicates ttiat the analyte was not detected, or ttie analyte was detected but was below the MDL. B This flag is used when an analyte is found in the blanl< as well as the sample. Indicates an extimated value. This flag is used either when estimating a concentration for tentatively identified compounds or when the data indicated the presence of a compound that meets the identification criteria but the result is less than the EQL (e.g. 3 J with an EQL of 10). MDL Method Detection Limit: The minimum concentration of a substance that can be confidently measured and reported. The laboratory has demonstrated that the MDL can be achieved in a laboratory reagent blanl<, but does not guarantee it can be achieved in all sample matrices. EQL Estimated Quantitation Limit: The EQL.generaiiy is 5 to 10 times the MDL. For many analytes the EQL is selected as the value of the lowest standard in the calibration curve. Diiution Dilution Factor: The prepared sample was diluted by this factor because the Factor sample was too concentrated or due to other interferences in the sample matrix. Any dilution factor causes a corresponding increase in the MDL and EQL. Page 16 of 16 ATK Launch Systems Group Environmentar Laboratory O^OSOAS Client Name: Sample Receipt Checklist SOG No. fP7pS~0i^ Carrier: Q Hand delivered, no cooler Carrier Number:^ 7^ Q HandTOlivered, sample(s) taken out at receiving counter Cooler Information: Cooler Number/ID: l^iujl^ ^ \A) ibu{-<g^ Condition of Shipping Container: Cooler Sealed (taped): Custody Seals Present: Coolant: State of Coolant: Thermometer \D^/.^W5>T-' Packing Description: ^ood QYes QYes Qlntact Qlce UFrozen ^Reading:. QFair QNot Applicable ja^o , - QNot Applicable ^0 QNot Applicable QBroken QBlue Ica ^one QPanially Frozen QMelted // °C CF: QDamaged (explain). Seal Number: Other: Corrected Temp: Temp Blank Included: QYes QNo Chain-Of-Custody Information; COC Present: ^ —JTrf^ COC Number(s)^Lf£jL3L3 COC signed (relinquished and received): COC or LWI agrees with sample labels: X"> ^No •No •No Other: QNot Applicable QNot Applicable . Notes:. Sample information: Samples includad in cooler: OTOSO^ Custody Seals Present: Sample containers intact: Samples in proper containers: Sufficient sample volume: All samples received in hold time: Water - VOA's have zero headspace: J^re-preserved with HCI: Notes: ' d(jo Other •Broken Seal Number(s). QNo Notes: QNo QNo •No ^es QNo QNot Applicable Pre-preserved with NajSjOa: QNon-Preserved: Waler -pH acceptable upon receipt: ^Jv^* HNO, = ^ L^ HjS04 = •Adjusted (see comirwnts below) QNot Applicable NaOH = _ZnAC /NaOH = HCL = Water - pH adjusted: (mfg. & Lot No.) HNOj H2SO.. NajSOjOj : other _ Notes: _NaOH. _ZnAC HCL SOP-102FormA 0705015 ENVIRONMENTAL LAB WORK REQUEST TO THIOKOL ENVIRONMENTAL LABORATORY FROM: • Dave Covington ORGANIZATION: Environmental Services EXTENSION 3898 MAIL STOP: 301 LWRNO.E12743 Logiii No. COST CENTER: 8200 WORK ORDER: 9.88P LS333 GW DATE? 05/08/07 REPORT RESULTS TO: HELEN RAVSTEN, MS 301 • SAMPLE INFORMATION SAMPLE 2167 2168 2169 2170 2171 2172 DATE 5-7-07 5-7-07 5-7-07 5-7-07 5-7-07 5-7-07 TYPE G C LOCATION J-6HS J-6 J-6D FB EB J-5 HS TIME 12:33 13:13 13:13 13:30 13:37 14:40 TEST Perchlorate, Metals, (Method 6010), Voc's (Method 8260) Perchlorate, Metals, (Method 6010), Voc's (Method 8260) i. " tv K (. •» REMARKS |^„:«k^g:kksn. |g;ifeS;h^A'g,sn, tv •t !«. ^ . . . . CHAIN OF CUSTODY RELINQUISHED BV z^^<: f^ DATE S''-^^e>-? TIME ^/.'/>'" RECEIVED BY '^{l^6af222i DATE ^-i'Ol TIME O^f^ FOR LABORATORY USE ONLY DATE COMPLETED DATE REPORTED SIGNATURE CERTIFICATE OF ANALYSIS Listing of Sample Information and Testing Requested Monday, June 18, 2007 TESTED FOR: ATK Thiokol: DLV Environmental Monitoring MS 301 Thiokol Corp, UT 84322 ANALYZED BY: ATK Thiokol Propulsion Environmental Laboratory P.O. Box 707, M/S 245 Brigham City, UT 84302-0707 435-863-3732 435-863-8080 Contact Name: Project: Sample Delivery Group: Dave Covington Ground Water Testing - DLV 0705019 Page 1 of 12 Sample Delivery Group: 0705019 Sample No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 0705019-01 2173-J-5 05/09/07 5/8/2007 10:52:26 EPA 314.0 SW-846, 30IOA SW-846, 6010B (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705019-02 2174-J-5 D 05/09/07 5/8/2007 10:52:26 EPA314.0 SW-846, 3010A SW-846, 6010B (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705019-03 2175-H-6 HS 05/09/07 5/8/2007 14:10:26 EPA 314.0 SW-846, 301 OA SW-846, 6010B (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705019-04 2176-H-6 05/09/07 5/8/2007 14:32:26 EPA 314.0 SW-846, 3010A SW-846, 6010B (Water) SW-846, 7470A Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Water Water Water Water Page 2 of 12 Sample Delivery Group: 0705019 Sample No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 0705019-04 2176-H:6 05/09/07 5/8/2007 14:32:26 SW-846, 82608 (Water) Volatile Organic Analysis Water Certified By: W. Scott Fraser, Quality Assurance Officer 06/18/2007 Date This certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation Program (NELAP) unless otherwise annotated: Page 3 of 12 Listing of Results by Sample Sample Delivery Group: 0705019 Client Sample ID: 2173-J-5 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705019-01 DateSampled: 05/08/07 10:52 CAS Number Tesf Metliod:^ 014797-73-0 festMetFod:" Test Parameter lEPA314F'_^f_ PERCHLORATE "sw^m.lbioA 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 "fesTMef/iofli:' 7439-97-6 fesfMeffiodT 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 ' 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 . 75-35-4 301 OA ACID DIGESTION Result Units Perchlorate - lon Chromatography 10.9 ug/L Metals Digestion 05/18/2007 11:00 MDL Dilution EQL Factor Analvst Test Date TeslMethod: SW-846, 6010B (Wafer) Metals Analysis by ICP-JoiO ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC "sw-MlfmA u 66.1 u U u U U U II.J- ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Mercury Analysis MERCURY SW-8462i260B (Water) ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE U ug/L Volatile Organic Analysis 0.3 JMM MTB TCP 05/18/07 05/18/07 20 2 1 10 20 1 1 30 10 100 10 5 50 100 5 5 150 50 MTB MTB MTB MTB MTB MTB MTB MTB MTB _ i 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 05/16/07 U U u u u u u u u u u u u u u u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 Page 4 of 12 Listing of Results by Sample Sample Delivery Group: 0705019 Client Sample ID: 2173-J-5 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705019-01 DateSampled: 05/08/07 10:52 CAS Number ; Testfliethod: ' .156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 ' 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter .^iyM'i%i?.-^?'^.'''!' y^?.°^?^"''^ CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1 -DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-lSOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1 -TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m,p-XYLENE O-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 T0LUENE-D8 Result Analysis U U U U U U U U U u u u u u u u u u u u u u u u u u 3.6 J u u u u u u u u 106 105 105 97.4 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL EQL Oiluti Fac' 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 w Analvst Test Date LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/10/07 . 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 . 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 Client Sample ID: 2174-J-5 D Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705019-02 DateSampled: 05/08/07 10:52 CAS Number : TestMethod: 014797-73-0 ' TestMethod: Test Parameter EPA 314.0 PERCHLORATE SW-846, 3010A • 301 OA ACID DIGESTION Result Units Perchlorate - lon Chromatography 11.8 ug/L Metals Digestion 05/18/2007 11:00 MDL Dilution EQL Factor Analvst Test Date JMM 05/18/07 1 MTB 05/18/07 Page 5 Of 12 Listing of Results by Sample Sample Delivery Group: 0705019 Client Sample ID: 2174-J-5 D Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705019-02 Date Sampled: 05/08/07 10:52 CAS Number test ifethod^ 7440-38-2 7440-39-3 7440-43-9 . 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 TesiMeViod: 7439-97-6 tesiMethod2 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 . 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 . 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 Test Parameter J^Me^SplOBJWater)^ ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC SW-846, 74704 MERCURY Result Metais Analysis by ICP - 6010 Units MDL -6016" u 65.9 U U U u u u 17. J ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L •—~ -;- 20 2 1 10 . 20 . 1 1 30 10 100 10 5 50 100 5 5 150 50 Dilution EQL Factor Analvst Test Date Mercury Analysis SIV-846, 8260B (Water) Volatile Organic Analysis ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE • 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBONDISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE . CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1 -DICHLOROPROPENE • CIS-1,3-DICHLOROPROPENE U ug/L 0.3 u u u u u u u u u u u u u u u u u u u u u u u u u u. u u. u u • u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 , 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 MTB MTB MTB MTB MTB MTB MTB MTB MTB -• • - •• 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 TCP 05/16/07 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Page 6 of 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 . 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 12 Listing of Results by Sample Sample Delivery Group: 0705019 Client Sample ID: 2174 - J-5 D Sample Oescription: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705019-02 DateSampled: 05/08/07 10:52 Diluti CAS Number i TestMethod: 10061-02-6 590-20-7 100-41-4 591-78-6. 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 . 108-67-8 108-05-4 75-01-1 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter ^ SW-846, 8260S (Water) Volatile Organic TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2.-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m,p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1.2-DICHLOROETHANE-D4 TOLUENE-D8 Result Analysis U U U U U U U U U U U U U U U U U u u u 4. J U u U u u u u u 107 103 102 98.8 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 :• 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 EQL Fac 10 1 10 1 10 1 10 . 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 , 1 10 1 10 1 10 1 10 1 -10 1 10 1 10 1 10 1 .10 1 10 1 10 1 10 1 10 1 10 1 10 1 tor Analvst — . LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date 05/10/07 05/10/07 05/10/07 05/10/07 '05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 • 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 . 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 Client Sample ID: 2175-H-6 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: .0705019-03 Date Sampled: 05/08/07 14:10 CAS Number : resfWetfiod; 014797-73-0 TesttJieOiod: Test Parameter EPA 314.0 PERCHLORATE SW-846, 3010A 3010A ACID DIGESTION test Method: 5W-846, 6010B (Water) 7440-38-2 7440-39-3 7440-43-9 7440-47-3 ARSENIC BARIUM CADMIUM CHROMIUM Result Perchlorate - lon Chromatography <EQL Metals Digestion 05/18/2007 11:00 Metals Analysis by ICP - 6010 U 133. U U Units ug/L ug/L ug/L ug/L ug/L MDL Dilution EQL Factor Analvst Test Date JMM MTB 05/18/07 05/18/07 20 2 1 10 100 10 5 50 1 1 1 1 MTB MTB MTB MTB 06/04/07 06/04/07 06/04/07 06/04/07 Page 7 of 12 Listing of Results by Sample Sample Delivery Group: 0705019 Client Sample ID: 2175-H-6 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboi-atory Sample ID: 0705019-03 DateSampled: 05/08/07 14:10 CAS Number : Test Method: ' 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 TestMethod: 7439-97-6 ; Testi^eitiod: 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 Test Parameter SW-846, 60WB (Water) ^Metals Analysis LEAD MANGANESE SILVER TIN ZINC SW-846, 7470/1 : Mercury Analys MERCURY SW-846, 8260B (Water) Volatile Organic ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE . BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBONDISULFIDE CARBON IblRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFbRM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE . 1,2-DICHLOROPROPANE . 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CiS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE Result by rcp"-''601 b'" U 116. U U 16. J s. U Analysis U U U U U u u u u u u u u u u u u u u u , u u u u u u u u u u u u u u u u u u u . u u Units 17!"'! ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L .ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L , ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL EQL Dilui Fad 20 1 1 30 10 100 . 5 5 150 50 0.3 '—•"••-•" 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 . 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 .0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 "-• •. - 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 TO 10 10 10 10 10 10 .10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 ion or Analvst Test Date -"" — MTB MTB MTB MTB MTB • - -• - 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 TCP 05/16/07 .11.:,; LSH LSH LSH LSH , LSH LSH' LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Page 8 of ..11. i 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 12 Listing of Results by Sample Sample Delivery Group: 0705019 Client Sample ID: 2175-H-6 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705019-03 Date Sampled: 05/08/07 14:10 CAS Number Test Parameter Result i' Test Method: SlV-W6, 8260B Ofiaterf Voiatile Organic Analysis 87-68-3 HEXACHLOROBUTADIENE 98-82-8 ISOPROPYLBENZENE 99-87-6 4-ISOPROPYLTOLUENE 75-09-2 METHYLENECHLORIDE 108-10-1 4-METHYL-2-PENT ANONE 91-20-3 NAPHTHALENE 103-65-1 N-PROPYLBENZENE 100-42-5 STYRENE 630-20-6 1,1,1,2-TETRACHLOROETHANE 79-34-5 1,1,2,2-TETRACHLOROETHANE 127-18-4 TETRACHLOROETHENE 108-88-3 TOLUENE 87-61-6 1,2,3-TRICHLOROBENZENE 120-82-1 1,2,4-TRICHLOROBENZENE 71-55-6 1,1,1-TRICHLOROETHANE 79-00-5 1,1,2-TRICHLOROETHANE 79-01-6 TRICHLOROETHENE 75-69-4 TRICHLOROFLUOROMETHANE 96-18-4 1,2,3-TRICHLOROPROPANE 95-63-6 1,2.4-TRlMETHYLBENZENE 108-67-8 1,3,5-TRIMETHYLBENZENE 108-05-4 VINYLACETATE 75-01-4 VINYLCHLORIDE 1330-20-7 m,p-XYLENE 95-47-6 o-XYLENE 460-00-4 BROMOFLUOROBENZENE 1868-53-7 DIBROMOFLUOROMETHANE 17060-07-0 1,2-DICHLOROETHANE-D4 . 2037-26-5 . TOLUENE-D8 Units lis U U U U u u u u u u u 3. J u u U u 5. J u u u u u u u u 105 103 105 100 . ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL EQL Diluti Fad 0.9 , 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 . 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 10 10 10 10 10 10 10 10 10 10 10 10 10 .10 10 10 10 10 10 10 10 10 10 10 10 ac Analvst Test Date LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH , LSH LSH LSH LSH LSH LSH 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 Client Sample ID: 2176 - H-6 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705019-04 DateSampled: 05/08/07 14:32 CAS Number Test Meiiiod: ' 014797-73-0 TestMethod: Test Parameter EPA23i4.i}' '""•' PERCHLORATE SW-846, 30i0A 301 OA ACID DIGESTION Result Units Perchlorate - lon Chromatography < EQL Metals Digestion 05/18/2007 11:00 MDL EQL Dilution Factor Analvst Test Pate ug/L JMM TestMethod: SW-846, 601 OB (Water) Metals Analysis by ICP-6010 MTB 05/18/07 05/18/07 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN U 131. U 33. J U 128. U U ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 20 2 1 10 20 1 1 30 100 10 5 50 100 5 5 150 MTB MTB MTB MTB MTB MTB MTB MTB 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 . 06/04/07 06/04/07 06/04/07 Page 9 of 12 Listing of Results by Sample Sample Delivery Group: 0705019 Client Sample ID: 2176-H-6 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705019-04 DateSampled: 05/08/07 14:32 CAS Number : test Metiiod: 7440-66-6 fest Method;" 7439-97-6 Test MiiOodT 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 •75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 • 74-95-3 •106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 Test Parameter Sy£846, SOm (Water) ZINC 'SW-846, YiiOA Result Metals /Analysis t)y icP -6010 Units 49. J ug/L Mercury Analysis MERCURY ~'SW-846, 82608 (Water) ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBONTETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUErME 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE j 1,2-DICHLOROBEhJZENE 1.3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1 ,'3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE Volatile Organic Analysis U ug/L u u u u . u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 10 . Dilution EQL Factor Analvst Test Date 0.3 50 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 . 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 MTB TCP 06/04/07 05/16/07 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH . LSH LSH LSH LSH • LSH LSH 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 Page 10 of 12 Listing of Results by Sample Sample Delivery Group: 0705019 Client Sample ID: 2176-H-6 Sample Description: ATK-DLV - Groundwater Spring 2007 .. Laboratory Sample ID: 0705019-04 Oate Sampled: 05/08/07 14:32 CAS Number TestMethod: 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-1 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter '~SW-846FS266B'(Waier) """ Volatile oTganic 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2.4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m.p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 T0LUENE-D8 Result Analysis U U U U U U u u u u u u 5. J U U U U u u u u 107 104 102 98.5 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % DL 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Dilui EQL Fac 10 1 10 1 10 1 10 . 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 . 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 ion tor Analvst •-•• LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH, LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date — _. 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 05/10/07 Page 11 of 12 Data Reporting Qualifiers Indicates ttiat tlie analyte was not detected, or tiie analyte was detected but was below the MDL. Ttiis fiag is used wlien an analyte is found in ttie blanl< as well as the sample. Indicates an extimated value. This flag is used either when estimating a concentration for tentatively identified compounds or when the data indicated the presence of a compound that meets the identification criteria but the result is less than the EQL (e.g. 3 J with an EQL of 10). MDL Method Detection Limit: The minimum concentration of a substance that can be confidently measured and reported. The laboratory has demonstrated that the MDL can be achieved in a laboratory reagent blanl<, but does not guarantee it can be achieved in all sample matrices. EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many analytes the EQL is selected as the value ofthe lowest standard in the calibration curve. Dilution Dilution Factor: The prepared sample was diluted by this factor because the Factor sample was too concentrated or due to other interferences in the sample matrix. Any dilution factor causes a corresponding increase in the MDL and EQL. Page 12 of 12 ATK Launch Systems Group Environmental Laboratory - Sample Receipt Checklist y>tUtA(^ dCM tKp ^c>W 0?osP/^ Client Name;. Carrier: Q Hand delivered, no cooler no^el Q Hand^elivered, sample(s) taken out at receiving counter SDG No. Carrier Number: t070e> 019 //^ 0 counter QOamaqed (explain) Seal Numbar: Other: Cooler Information: Cooler Number/ID:_ UlxAJL^4 LO UAJU^ Condition of Shipping Container: Coolar Sealed (taped): Cuslody Seals Present: Coolant: State of Coolant: Thermometer ID: *1^S^ftVf\ Packing Description: ^ood QYes QYes Qlntact •Ice QFrozen Reading: QFair ^0 jSfJo QBroken QBlue ice •Not Applicable •Not Applicable •Not Applicable ^one QPartially Frozen QMe O "C CF: Corrected Temp:, Temp Blank Included: QYes QNo Chaln-Of-Custody Information: COC Present: _ .^.^^m^ ^a COC Nijmber(s>: t. IC' f*t9 COC signed (relinquished and received): COC or LWI agrees with sample labels: •No •No •No Notes:, . Other: •Not Applicable •Nol /Applicable Sample Information: Samples included in cooler: d^yo^yof^ Custody Saals Present: Sample containers intact: Samples in proper containers: Sufficient sample voiuma: All samples received in hold time: •Yes •Intact pees l^'es >P'es Jt^es Water - VOA's have zero headspace: At're-preserved with HCI: Notes: ^0 Other. •Broken Seal Number(sj. •No Notes: •No • •No ' QNo jpe% ONo •Not Applicable Q^re-preserved with Na^SaOs: •Non-Preserved: Water - pH acceptable upon receipt: HNO, = "*• ^^ J^es QAdjusted (see comments below) •Not Applicable _HiSO, = : NaOH = ^ ZnAC /NaOH = _HCL = Water - pH adjusted: (mfg. & Lot No.) HNO, HjSO. NajSOaO, Other. Notes: _NaOH. _ZnAC. HCl SOP-102 Form A 0705019 ENVIRONMENTAL LAB WORK REQUEST TO THIOKOL ENVIRONMENT AJL LABORATORY FROM: Dave Covington ORGANIZATION: Environmental Services EXTENSION: 3898 MAIL STOP: 301 LWR No. El2745 Logiii No. COST CENTER: 8200 . WORK ORDER; 988P LS333 GW DATE: 05/09/07 REPORT RESULTS TO: HELEN RAVSTEN, MS 301 SAMPLE INFORMATION SAMPLE 2173 2174 2175 2176 DATE 5-8-07 5-8-07 5-8-07 5-8-07 TYPE G C LOCATION J-5 J-5D H-6HS H-6 TIME 10:52 10:52 14:10 14:32 TEST Perchlorate, Metals, (Method 6010), Voc's (Method 8260) Perchlorate, Metals, (Method 6010), Voc's (Method 8260) (• (•• i«. i, fl REMARKS PHg'Aisn, |g;ifeS;h^:X'g.sn, t^ •^ •" ' • CHAIN OF CUSTODY RELINQUISHED BV ^ c ^ I J>^- ^t-^ -^ DATE <^'9-^i^ TIME ^l^^ FORLABORATOF DATE COMPLETED RECEIVED BV "rtfJ&itr DATE 5"-f-^7 TIME O'sY^ tY USE ONLY D,\TE RBPORTED SIGNATURE CERTIFICATE OF ANALYSIS Listing of Sample Information and Testing Requested Tuesday, June 05, 2007 TESTED FOR: ATK Thiokol: DLV Environmental Monitoring MS 301 Thiokol Corp, UT 84322 ANALYZED BY: ATK Thiokol Propulsion Environmental Laboratory P.O. Box 707, M/S 245 Brigham City, UT 84302-:0707 435-863-3732 435-863-8080 Contact Name: Project: Sample Delivery Group: Dave Covington Ground Water Testing - DLV 0705026 Page 1 of 18 Sample Delivery Group: 0705026 Sample No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 0705026-01 2177-H-5 HS 05/11/07 5/9/2007 10:30:50 EPA 314.0 SW-846, 3010A SW-846, 6010B (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705026-02 2178-EBHS 05/11/07 5/9/2007 09:00:50 EPA 314.0 SW-846, 301 OA SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) . Perchlorate - lon Chromatography. Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705026-03 2179-FB 05/11/07 5/9/2007 11:07:50 EPA 314.0 SW-846, 301 OA SW-846, 6010B (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Wafer 0705026-04 2180-H-5 05/11/07 5/9/2007 11:17:50 EPA 314.0 SW-846, 3010A SW-846, 6010B (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705026-05 2181 -EB 05/11/07 5/9/2007 11:37:50 EPA 314.0 SW-846, 301 OA SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705026-06 2182-H-1 HS 05/11/07 5/9/2007 14:00:50 EPA 314.0 SW-846, 301 OA SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water Page 2 of 18 Sample Delivery Group: 0705026 Sample No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 0705026-07 2183-H-1 05/11/07 5/9/2007 14:22:50 EPA 314.0 SW-846, 30IOA SW-846, 6010B (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water Certified By: W. Scott Fraser, Quality Assurance Officer 06/05/2007 Date This certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation Program (NELAP) unless otherwise annotated: Page 3 of 18 Listing of Results by Sample Sample Delivery Group: 0705026 Client Sample ID: 2177-H-5 HS '^ Sample Description: ATK-DLV •: Groundwater Spring 2007 Laboratory Sample ID: 0705026-01 DateSampled: 05/09/07 10:30 Dilution CAS Number : resf Method: 014797-73-0 "fesFMetfioS; " : TestMethod: 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 ; TestMethod: 7439-97-6 ; Tesr Meihod; 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 Test Parameter EPA 314.0 _ __Perchlcirate - lon PERCHLORATE SW-846, 3010A Metals Digestion 3010A ACID DIGESTION SIV-846, 6010B (Water) Metals Analysis b ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN • ZINC SW-846, 7470A Mercury Analysis MERCURY SW-846, 82608 (Water) Volatile Organic f ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUEME DIBROMOCHLOROMETHANE 1,2-DISROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE Result Chromatography 14.5 ..^ vv. 05/18/2007 14:00 y ICP-6010 24. J 181 U 324 U 24.8 U U 27. J "•••'• U Analysis U U U U U U U U U U u u u u u u u u u u u u u u u u u u u u u Units ug/L "• ~'""' •• • ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ••" • ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L IMDL 2.5 , -„..^ :,.. .. . 20 2 1 10 20 1 1 30 10 .... v.w.v, .. 0.3 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 EQL Factor Analvst 10 2.5 JMM " ' • • • •" 1 100 10 5 1 50 1 100 . 1 5 5 150 50 ..... .... .......... 1 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 .10 10 10 10 10 10 - — • • MTB MTB MTB MTB MTB MTB MTB MTB MTB MTB '•" •" ; ••-™-- TCP 1 LSH LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH Test Date „ . 05/29/07 ::/::.•; 05/18/07 06/04/07 06/04/07 06/04/07 06/04/07 08/04/07 06/04/07 06/04/07 06/04/07 06/04/07- i 05/16/07 • 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 Page 4 of 18 Listing of Results by Sample Sample Delivery Group: 0705026 Client Sample ID: 2177-H-5 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705026-01 Date Sampled: 05/09/07 10:30 CAS Number i TestMethod: 156-59^ . 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103:65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter SW-846, 8260B (Water) Volatile Organic CIS-1,2-DICHLOROETHENE TRANS-1.2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE ClS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-lSOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1.2,3-TRICHLOROBeNZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE. 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m.p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 TOLUENE-DB Result Analysis U U U U U U U U U U U U U U U U U U U U U 1.9 J u U U U U u u u u u u u u 106 106 108 97.4 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % • % MDL 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Dilu EQL Fac 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 .• 1 10 • 1 10 1 10 1 10. 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 , 1 10 1 10 , 1 ion tor Analvst LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH . LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 . 05/15/07 Client Sample ID: 2178-EBHS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705026-02 Date Sampled: 05/09/07 09:00 CASNumber i TesiMeihod: 014797-73-0 • Tiesf Metfioi/; Test Parameter Result Units EPA 314.0 Perchlorate - lon Chromatography PERCHLORATE U ug/L SW-846, 3010A Metals Digestion 3010A ACID DIGESTION 05/18/2007 14:00 MDL 1 iSk 4 Factor 1. 1 Dilution Factor Analvst Test Date JMM 05/29/07 MTB 05/18/07 Page 5 of 18 Listing of Results by Sample Sample Delivery Group: 0705026 Client Sample ID: 2178-EBHS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705026-02 Date Sampled: 05/09/07 09:00 CAS Number : rest Method.-" 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 : resf Method; 7439-97-6 TestMethod: 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 Test Parameter SW^84626mB0/^aterf ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC SW-846, 7470^ MERCURY SW-8'46, 82608 (Water) Result Metals Analysis by ICP - 6010 U U U U U U U U U Mercury Analysis Volatile Organic Analysis ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLbROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUO,ROMETHANE 1,1-DICHLOROETH.ANE 1,2-DICHLOROETHANE 1.1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL EQL Dilui Fad U ug/L u u u u u u u u u u u u u u u u u u u u u . u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 20 •. 2 1 10 20 1 1 30 10 100 10 5 50 100 5 5 150 50 0.3 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 . 0.15' 6.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 ion ;or Analvst , Test Date MTB MTB MTB MTB MTB MTB MTB MTB . MTB ' i 06/04/07 06/04/07 06/04/07 • 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 TCP 05/16/07 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH. LSH LSH LSH LSH LSH LSH LSH LSH . LSH LSH LSH Page 6 of 05/15/07 05/15/07. 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 18 Listing of Results by Sample Sample Delivery Group: 0705026 Client Sample ID: 2178 - EB HS Sample Description: ATK-DLV - Groundwater Spring 2007 CAS Number . ^g-jjjij-jjfij-j. - 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 . 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter Result SW-846, 8260B (Water) Volatile Organic Analysis TRANS-I ,3-DICHLOROPROPENE U 2,2-DlCHLOROPROPANE U ETHYLBENZENE U 2-HEXANONE U HEXACHLOROBUTADIENE ,U ISOPROPYLBENZENE U 4-ISOPROPYLTOLUENE U METHYLENE CHLORIDE U 4-METHYL-2-PENTANONE U NAPHTHALENE U N-PROPYLBENZENE U STYRENE U 1,1,1,2-TETRACHLOROETHANE U 1,1,2,2-TETRACHLOROETHANE U TETRACHLOROETHENE U TOLUENE 1.6 J 1,2,3-TRICHLOROBENZENE U 1,2,4-TRICHLOROBENZENE U 1,1,1-TRICHLOROETHANE U 1,1,2-TRICHLOROETHANE U TRICHLOROETHENE U TRICHLOROFLUOROMETHANE U 1,2,3-TRICHLOROPROPANE U 1.2,4-TRIMETHYLBENZENE U 1,3,5-TRIMETHYLBENZENE U VINYL ACETATE U VINYL CHLORIDE U m.p-XYLENE U O-XYLENE U BROMOFLUOROBENZENE 105 DIBROMOFLUOROMETHANE 106 1,2-DICHLOROETHANE-D4 104 TOLUENE-D8 98.2 Units ug/L ug/L • ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25.. 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Laboratory Sample ID: 0705026-021 Date Sampled: 05/09/07 09:001 Dilution EQL Factor Analvst .10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH ,10 1 LSH 10 1 LSH 10 1 LSH 10 . 1 LSH 10 . 1 LSH 10 .1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10- 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH Test Date 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 . 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 . 05/15/07 05/15/07 • 05/15/07 05/15/07 05/15/07 05/15/07 Client Sample ID: 2179-FB Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705026-03 Date Sampled: 05/09/07 11:07 CAS Number : Tesf Method; 014797-73-0 : festtleitiod: : reif Method; 7440-38-2 7440-39-3 7440-43-9 .. 7440-47-3 Test Parameter EPA 314.0 PERCHLORATE SW-846, 3016A 3010A ACID DIGESTION yW-8'46,eoio'B]Waier)['''^^ • ARSENIC BARIUM CADMIUM CHROMIUM Result Units Perchlorate - lon Chromatography U ug/L Metals Digestion 05/18/2007 14:00 . Metals Analysis bylc'p - 6010 ' U ug/L U ' ug/L U ug/L U ug/L MDL Dilution EQL Factor Analvst Test Date JMM MTB 05/29/07 05/18/07 20 2 1 10 100 10 5 50 1 1 1 1 MTB MTB MTB MTB 06/04/07 06/04/07 06/04/07 06/04/07 Page 7 of 18 Listing of Results by Sample Sample Delivery Group: 0705026 Client Sample ID: 2179-FB Sample Description: ATK-DLV • Groundwater Spring 2007 Laboratory Sample ID: 0705026-03 Date Sampled: 05/09/07 11:07 Dilution CAS Number : TlBsf Mefhod; ' 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 fesfMef/iod; 7439-97-6 ; Tesf Metfiod; 67-64-1 71-43-2- 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10081-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 Test Parameter Result SW-846, 601 OB (Water) Metals Analysis by ICP-6010 LEAD MANGANESE SILVER TIN ZINC SW-846, 7470A Mercury Analysis MERCURY '''~SW846^826()BfAla^^^^ ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM . BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON IhlKACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETH.ANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1 ,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE U U U U U U U U U U U U U U U U U U U U U U U U u. u u u u u u u u u u u u u u u u u u u u u u Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 20 1 1 30 10 0.3 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 EQL ~'Z' 11 100 5 5 150 50 1 100 10 10 10 10 • 10 10 10 10 10 10 10 10 10 10 10 •10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 Factor i:..'3; Analvst MTB MTB MTB MTB MTB TCP ZZ. LSH LSH LSH LSH LSH LSH LSH LSH LSH - LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date ! 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 - 05/16/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07, 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 Page 8 of 18 Listing of Results by Sample Sample Delivery Group: 0705026 Client Sample ID: 2179-FB Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705026-03 Date Sampled: 05/09/07 11:07 Dilution CAS Number tesi Metiiod: • ' 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18^ 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter 'SW-a46, 82608 (Water) "volatire Organic HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-lSOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANOhJE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1 -TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m,p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 T0LUENE-D8 Result Analysis U U U U U U U U u u u u u u u u u u u u u u u u u 105 106 106 97.5 Units '•••. Zf" ug/L ug/L ug/L ug/L ug/L ug/L , ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL •• 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4:37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 EQL w. -. .. . . . 10 10 10 10 • 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 / Factor 1 - Analvst "":"'f..i' LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date „ . ... ...; 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 .05/15/07 05/15/07 Client Sample ID: 2180-H-5 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705026-04 Date Sampled: 05/09/07 11:17 CAS Number Tesf Method: 014797-73-0 :. Tesf Method ' : TestMethod: 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 Test Parameter Result EPA 314.0 Perchlorate - Ion Chromatography PERCHLORATE 12.2 SW-846, 30ldA Metals Digestion' 3010A ACID DIGESTION 05/18/2007 14:00 SW-846, 60108 (Water) Metals Analysis by ICP - 6010 ARSENIC 32. J BARIUM 195 CADMIUM U CHROMIUM 205 LEAD U MANGANESE 60.4 SILVER U TIN U Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL Dilution EQL Factor Analvst Test Date 2.5 10 2.5 JMM MTB 05/29/07 05/18/07 20 2 1 10 20 1 1 30 100 10 5 50 100 ~ 5 5 150 MTB MTB MTB MTB MTB MTB MTB MTB 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 Page 9 of 18 Listing of Results by Sample Sample Delivery Group: 0705026 Client Sample ID: 2180-H-5 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705026-04 DateSampled: 05/09/07 11:17 CAS Number Test Meiiiod: 7440-66-6 \ test Hiefhod: ' Test Parameter SW-(S4^60iOB(V^tei^^ ZINC • SW-846, 7470A"' 7439-97-6 TestMethodT 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 J 87-68-3 98-82-8 99-87-6 75-09-2 Result Units Metals /Analysis by ICP - 6010 35.J ug/L Mercury Analysis Dilution MDL EQL Factor Analvst Test Date • MERCURY SW-846, 82608 ^fer) ACETONE Volatile Organic Analysis BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLpROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOR08ENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE l:2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-lSOPROPYLTOLUENE METHYLENE CHLORIDE U ug/L u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u . u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 10 0.3 50 30 0.22 0.31 o;i9 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 171 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 . 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 MTB TCP 06/04/07 05/16/07 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH' LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 Page 10 of 18 Listing of Results by Sample Sample Delivery Group: 0705026 Client Sample ID: 2180-H-5 Sample Description: ATK-DLV - Groundwater Spring 2007 CAS Number ; TestMethod: 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18^ 95-63-6 108-67-8 108-05-4 . 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter Result "SW-846; 82608 (Wafer/^" Volatile brganic Anaiysis 4-METHYL-2-PENTANONE . NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m,p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 TOLUENE-D8 — U U U u u u u 0.9 J U U u u u u u u u u u u u 108 107 108 97.3 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % . • % MDL 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Laboratory Sample ID: 0705026-041 DateSampled: 05/09/07 11:171 Dilution EQL Factor Analvst 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH Test Date Z... ,„!, J 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 . ^05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 Client Sample ID: 2181 - EB Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705026-05 Date Sampled: 05/09/07 11:37 Dilution CAS Number Test Mettiod: 014797-73-0 TestMethod: "fesYMethod2 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 2 TesiMeihod: 7439-97-6 Test Parameter EPA 314.0 PERCHLORATE S\ff-846, 3010A 301 OA ACID DIGESTION SW-84i 60108 (yVateO^^^^^^^ ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC SW-846, 7470X MERCURY Perctilorate - lon Metals Digestion Result Chromatography U 05/18/2007 14:00 Metals Analysis by ICP -^6010 Mercury Analysis U U u u u u u u u u Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 1 •-- 20 2 1 10 20 1 1 30 10 0.3 EQL 4 — 100 10 5, 50 100 5 5 150 50 1 Factor Analvst 1 1 1 1 . 1 1 1 1 1 1 1 1 JMM MTB MTB MTB • MTB MTB MTB MTB MTB MTB MTB TCP Test Date 05/29/07 05/18/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 05/16/07 Page 11 of 18 Listing of Results by Sample Sample Delivery Group: 0705026 Client Sample ID: 2181-EB Sample Description: ATK-DLV - Groundwater Spring 2007. Laboratory Sample ID: 0705026-05 Date Sampled: 05/09/07 11:37 CAS Number " TesiMeth6d:__^ 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 . 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 •106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 Test Parameter .,..?^?v?260B (il|fer) ^"^Volatile Org ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE . 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1.2-DIBROMOETHANE 1,2-D|CHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE •1,2-piCHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE ClS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1 ,i2,2-TETRACHLOROETHANE Result ; Analysis Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL Dilution EQL Factor Analvst Test Date 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 ' 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 . 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH • LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 '05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 - 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 Page 12 of 18 Listing of Results by Sample Sample Delivery Group: 0705026 Client Sample ID: 2181 - EB Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705026-05 DateSampled: 05/09/07 11:37 CAS Number , Test Parameter Result : TestMethod: s"W-84VS260B7Wafer/_ Volatile brganic Analysis . 127-18-4 TETRACHLOROETHENE 108-88-3 TOLUENE 87-61-6 1,2,3-TRICHLOROBENZENE 120-82-1 . 1,2,4-TRICHLOROBENZENE 71-55-6 1,1,1-TRICHLOROETHANE 79-00-5 1,1,2-TRICHLOROETHANE 79-01-6 TRICHLOROETHENE 75-69-4 TRICHLOROFLUOROMETHANE 96-18-4 1,2,3-TRICHLOROPROPANE 95-63-6 1,2,4-TRIMETHYLBENZENE 108-67-8 1,3,5-TRIMETHYLBENZENE 108-05-4 VINYLACETATE 75-01-4 VINYLCHLORIDE 1330-20-7 m.p-XYLENE 95-47-6 o-XYLENE 460-00-4 BROMOFLUOROBENZENE 1868-53-7 DIBROMOFLUOROMETHANE 17060-07-0 1,2-DICHLOROETHANE-D4 2037-26-5 TOLUENE-D8 Units sis" U U U U U U u . u u. u u u u u u 106 106 105 98.2 • - • ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL Dilution EQL Factor Analvst Test Date 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 • •• - .. 10 1 10 1 10 1 10 1 10 1 • 10 1 10 1 10 . 1 10 . 1 10 1 10 1 10 1 10 1 .10 1 10 1 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH •••:••• ~ "•] 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 Client Sample ID: 2182-H-1 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705026-06 Date Sampled: 05/09/07 14:00 Dilution CAS Number • TestMethod: 014797-73-0 : TestMethod: \ TestMethod: 7440-38-2 7440-39-3 7440^3-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 . 7440-31-5 7440-66-6 ; 'TeslMethod: 7439-97-6 "''Tesf Method; • 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 Test Parameter Result EPA 314.0 Perchlorate - lon Chromatography PERCHLORATE U SW-846, 30iOA, Metals Digestion 301 OA ACID DIGESTION 05/18/2007 14:00 SW-846, 6010B (Water) Metals Analysis by ICP - 6010 ARSENIC U BARIUM 210 CADMIUM U CHROMIUM U LEAD U MANGANESE 2150 SILVER U TIN U ZINC 24. J SW-846, 7470A Mercury Analysis MERCURY U 'sW-84M260B7wa<er;"''"'Volalile b ACETONE U BENZENE U BROMOCHLOROMETHANE U BROMODICHLOROMETHANE U BROMOBENZENE U Units ._. ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ' ' • •" ug/L ug/L ug/L ug/L ug/L MDL .. ...... 2.5 20 2 1 10 20 1 1 30 10 0.3 .. ......... . 30 0.22 0.31 0.19 "0.37 EQL „. „ 10 Z.Z..Z. 100 10 5 50 •100 5 . 5 150. . 50 ZZZ'Z 1 ......,-v 100 10 10 10 10 Factor ,„„„ ...,.,..,.. 2.5 • Z..:.. 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Analvst .„„..._ JMM MTB MTB MTB MTB MTB MTB MTB MTB MTB MTB i._: _ TCP LSH LSH LSH LSH LSH Test Date . f ••.., 05/29/07 "..ZZZZ 05/18/07 ... ! 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 1 05/16/07 t 05/15/07 05/15/07 . 05/15/07 05/15/07 05/15/07 Page 13 of 18 Listing of Results by Sample Sample Delivery Group: 0705026 Client Sample ID: 2182 - H-1 HS Sample Description: ATK-DLV - Groundwater Spring 2007 CAS Number f Tesf Method; 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 .96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 • 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 Test Parameter Result "~'SW-846, 82608 (Watei)" Vora'tile brgariic Anaiysis BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE " CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVlNYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE . 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE U U U U U U u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u 1.1 J u u u Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 Laboratory Sample ID: 0705026-061 Date Sampled: 05/09/07 14:001 Dilution EQL Factor Analvst 10 .1 LSH 10 1 • LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1' LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 . LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 LSH 10 1 , LSH 10 1 LSH 10 1 LSH 10 1 . .. LSH 10 1 LSH 10 1 LSH 10 . 1 LSH Test Date -• • ••; 05/15/07 05/15/07 . 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 .. 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 . 05/15/07 05/15/07 ' 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 Page 14 of 18 Listing of Results by Sample Sample Delivery Group: 0705026 Client Sample ID: 2182 - H-1 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705026-06 Date Sampled: 05/09/07 14:00 Dilution CAS Number 'Tfes'f Metfiod; 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00^ 1868-53-7 17060-07-0 2037-26-5 Test Parameter ~~SW-84628260B (Wafer) Voiatiie'brganic 1,1,2-TRICH'LOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m,p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 TOLUENE-D8 Result Analysis U U U U U U U U U U 106 106 106 96.9 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 EQL Z" ''Z'. 10 10 10 10 10 10 10 10 10 10 Factor '^Z. z Analvst .: LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date ZZZZl 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 Client Sample ID: 2183-H-1 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705026-07 DateSampled: 05/09/07 14:22 CAS Number i TesTMeiihod;" 014797-73-0 test Meiiiod: TesttAethod: 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 fest Method; 7439-97-6 test Meiiiod: 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 Test Parameter ' EP'niid PERCHLORATE SW-846, 3010A 301 OA ACID DIGEStlON SW-846,6010B (Water) ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC SW-846, 7470A MERCURY SW-846, 8260B (Wafer) ACETONE BENZENE Perchlorate - lon Metals Digestion Metals Analysis b Mercury Analysis Volatile Organic A BROMOCHLbROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE Result Units matography U ug/L MDL 2.5 EQL Dilution Factor Analvst Test Date 10 2.5 05/18/2007 14:00 JMM MTB 05/29/07 05/18/07 u 150 U 21. J U 1700 U U 22. J ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L U ug/L u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 20 2 1 10 20 1 1 30 10 0.3 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 •100 10 5 50 100 5 5 150 50 1 100 10 10 10 10 10 10 10 10 10 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 MTB MTB MTB MTB MTB MTB MTB MTB MTB TCP LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 06/04/07 05/16/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 Page 15 of 18 Listing of Results by Sample Sample Delivery Group: 0705026 Client Sample ID: 2183-H-1 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705026-071 Date Sampled: 05/09/07 14:22 CAS Numbej \fi^fMethod: 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 . 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 . 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 Test Parameter SW-a46, 82608 (Water) Volatile Org TERT-BUTYLBENZENE CARBON DISULFIDE CARBON 1 b 1 RACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE ClS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1.3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE • N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2.3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE Result Units ; Analysis u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 Dilut [L Fac 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 ion tor Analvst LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 1 LSH LSH 1 LSH 1 LSH Test Date 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 Page 16 of 18 Listing of Results by Sample Sample Delivery Group: 0705026 Client Sample ID: 2183-H-1 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705026-07 Date Sampled: 05/09/07 14:22 Dilution CAS Number : TestMethod: 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter SW-846, 8260B (Water) Volatile Organic 1,3,5-TRIMETHYLBENZENE . VINYL ACETATE VINYL CHLORIDE m.p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 TOLUENE-D8 Result Analysis U U U u u 106 105 105 99.7 Units ug/L ug/L ug/L ug/L ug/L % % % % . MDL 0.29 0.13 0.3 1.6 0.18 EQL 10 10 10 10 10 Factor Analvst LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 05/15/07 Page 17 of 18 Data Reporting Qualifiers U Indicates thatthe analyte was not detected, or ttie analyte was detected but was below the MDL. B This flag is used when an analyte is found in the blanl< as well as the sample. Indicates an extimated value. This flag is used either when estimating a concentration for tentatively identified compounds or when the data indicated the presence of a compound tliat meets the identification criteria but the result is less than the EQL (e.g. 3 J with an EQL of 10). MDL Method Detection Limit: The minimum concentration of a substance that can be. confidently measured and reported. The laboratory has demonstrated that the MDL can be achieved in a laboratory reagent blanl<, but does not guarantee it can be achieved in all sample matrices. EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many analytes the EQL is selected as the value of the lowest standard in the calibration curve. Dilution Diiution Factor: The prepared sample was diluted by this factor because this Factor sample was too concentrated or due to other interferences in the sample matrix. Any dilution factor causes a corresponding increase in the MDL and EQL. Page 18 of 18 ATK Launch Systems Group Environmental Laboratory (pypTo'LC^ Client Name: oler Q Hand deliverSCf sample(s) t< Sample Receipt Checldist Carrier: Q Hand delivered, no cooler sample(s) taken out at receiving counter SDG No. Carrier Number: (!)'?025rpz.0> A/fH g counter •Damaged (explain) Seal Number: . . .• Olher: Cooler information: Cooler. Numl>er/ID: '^[xAJLJ 1\))\A\-C Condition of Shipping Container: Cooler Sealed (taped): Custody Seals Present: ^^Sood QYes QYes Qlntact Coolant. Qlce State of Coolant: QFrozen Thermometer ID: 1^ f &tS^*f Heading: Packing Description: QFair QNot Applicable fiio QNot Applicable 1^0 QNot Applicable QBroken QBlue Ice ^JVNone 'artlally Frozen QMelted •C CF:__ ^ Corrected Temp:_ Tamp Blank Included: QYes QNo Chaln-OI-Custody Information: t^nain-ui-msioay iniormauon: j^ COC Present: ^ tf r7i// We: COC N[imb«r/st: CIC '/HtA COC signed (relinquished and receivad): COC or LWI agrees with sample labels: Notes:. QNo QNo QNo . Other:. QNot Applicable QNot Applicable Sample Information: Samples included in coolar: fZ?^(P^Cl7.C^ Custody Seals Present: Sampte containers intacl: Samples in proper containers: Sufficient sample volume: All samples received in hold time: QYes Qlntact X^es J^es /^Yes ^es Water - VOA's have zero headspace: Afre-presereed with HCI: Notes: ^o Other. •Broken Seal Number(s). •No . Notes: QNo • QNo QNo p6es QNo QNot Applicable QPre-presen/ed with NajSjOi: QNon-Preserved; Waler - pH acceptable upon receipt: Jt<e% HNOj = ^ U^ H^O. = QAdjusted (sea comments below) QNot /Applicable ' NaOH = ZnAC /NaOH = HCL = Water - pH adjusted: (mfg. & Lot No.) HNOj HjSO,. NajSOjOj Other _ Notes: NaOH. _ZnAC . -HCL SOP-102FormA 0705026 ENVIRONMENTAL LAB WORK REQUEST TO THIOKOL ENVIRONMENTAL LABORATORY FROM: Dave Covington ORGANIZATION: Environmental Services EXTENSION: 3898 MAILSTOP: 301 LWR No. £127-^ Login No. COST CENTER: 8200 WORX ORDER: 988P LS333 GW DATE: 05/09/07 REPORT RESULTS TO: HELEN RAVSTEN, MS 301 SAMPLE INFORMATION SAMPLE . 2177 2178 2179 2180 2181 2182 2183 DATE 5-9-07 5-9-07 5-9-07 5-9-07 5-9-07 5-9-07 5-9-07 TYPE G C LOCATION H-5 HS EB HS FB H-5 EB H-1 HS HI TIME 10:30 9:00 11:07 11:17 11:37 14:00 14:22 • TEST Perchlorate, Metals, (Method 6010), Voc's (Method 8260) Perchlorate, Metals, (Method 6010), Voc's (Method 8260) A " 1.. «' /. ' i^ -i REMARKS ||:ian;hg',X'g,Sn, |g;j^n^:^:X'ist^ c- " iv *l f. i^ " CHAIN OF CUSTODY RELINQUISHEDBY J X s^ ^ DATE >r TIME ^C RECEIVED BY -/<lZ&d^ DATE 5 11-01 TIME ^<€f5' FOR LABORATORY USE ONLY l°"~ DATE REPORTED SIGNATURE CERTIFICATE OF ANALYSIS r . • , '. ^ ' Listing of Sample Information and Testing Requested Friday, June 08, 2007 TESTED FOR: ATK Thiokol: DLV Environmental Monitoring MS 301 Thiokol Corp, UT 84322 ANALYZED BY: ATK Thiokol Propulsion Environmental Laboratory P.O. Box 707, M/S 245 Brigham City, UT 84302-0707 435-863-3732 435-863-8080 Contact Name: Project: Sample Delivery Group: Dave Covington Ground Water Testing - DLV 0705027 Page 1 of 20 Sample Delivery Group: 0705027 Sample No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 0705027-01 2184-HSEB 05/11/07 5/10/2007 09:05:34 EPA 314.0 SW-846, 301 OA SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705027-02 2185-H-2 HS 05/11/07 5/10/2007 09:58:34 EPA 314.0 SW-846, 301 OA SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705027-03 2186-H-2 05/11/07 5/10/2007 10:33:34 EPA 314.0 SW-846, 301 OA SW-846, 6010B (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705027-04 2187-FB 05/11/07 5/10/2007 12:48:34 EPA 314.0 SW-846, 301 OA SW-846, 6010B (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705027-05 2188-EW-6 05/11/07 5/10/2007 12:55:34 EPA 314.0 SW-846, 301 OA SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - Ion Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705027-06 2189-H-3 HS 05/11/07 5/10/2007 13:46:34 EPA 314.0 SW-846, 3010A SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - Ion Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water Page 2 of 20 Sample Delivery Group: 0705027 Sample No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 0705027-07 2190-H-3 HSD EPA 314.0 SW-846, 3010A SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis 0705027-08 2191 -H-3 05/11/07 5/10/2007 13:46:34 Water Water Water Water Water 05/11/07 5/10/2007 14:26:34 EPA 314.0 SW-846, 30IOA SW-846, 6010B (Water) SW-846, 7470A SW-846, 6260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury'Analysis Volatile Organic Analysis Water Water Water Water Water Certified By: W. Scott Fraser, Quality Assurance Officer 06/11/2007 Date This certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation Program (NELAP) unless otherwise annotated: Page 3 of 20 Listing of Results by Sample Sample Delivery Group: 0705027 Client Sample ID: 2184-HSEB Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705027-01 DateSampled: 05/10/07 09:05 CAS Number Tesf Meihod:' 014797-73-0 Test Metfiod; 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 TestMethod: 7439-97-6 Tesf ifethod: ., 67-64-1 71-43-2 • 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 ' 75-35-4 Test Parameter EPA 314.0 PERCHLORATE SW-846, idiOA " 3010A ACID DIGESTION Result Units Perchlorate - lon Chromatography U ug/L Metals Digestion 05/18/2007 14.00 TestMethod: SW-846, 60108 (Water) Metals Analysis by ICP-6010 ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC SIV-846; 7470A Mercury Analysis MERCURY SlV-846, 826d8 (yi/aterj Volatile Organic Analysis ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE ' CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DiBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZeNE 1,3-DICHLOROBENZeNE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE U ; ug/L U ug/L U U U U U U U ug/L ug/L ug/L ug/L ug/L' ug/L ug/L U ug/L u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug'L ug/L IVIDL 0.3 Dilution EQL Factor Analvst Test Date JMM MTB TCP 05/29/07 05/18/07 20 2 1 10 20 1 1 30 10 -"• 100 10 5 50 100 5 5 150 50 ...". ..I'. MTB MTB MTB MTB MTB MTB MTB MTB MTB 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 . v.. •• 05/16/07 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25. 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 100 10 10 10 10 10 . 10. 10 10 10 10 10 10 10 • 10 10 10 10 10 10 10 10 10 10 10 10 10 • 10 10 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH . LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 Page 4 of 20 Listing of Results by Sample Sample Delivery Group: 0705027 - Client Sample ID: 2184-HSEB Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705027-01 DateSampled: 05/10/07 09:05 CAS Numbei' TestMethod: 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-r 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96^18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 . 17060-07-0 2037-26-5 Test Parameter 5^-846, 8260S (Water) Result Volatile Organic Analysis CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE . 1,2,4-TRICHLORbBEN2ENE 1,1,1 -TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-tRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m.p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-b4 TOLUENE-b8 Units MDL sis U U u u u u u u u u u u u ,u u u u u u u u 1.1 J u u u u u u u u u u u u u 107 105 106 94.1 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . ug/L • ug/L ug/L ug/L ug/L • ug/L ug/L ug/L • ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 • 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Dilution EQL Factor Analvst Test Date 10 10 10 10 10' 10 10 10 10 10 10 10 10 10 10 10 10 ,10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 Client Sample ID: 2185-H-2 HS Sample Oescription: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705027-02 Date; Sampled: 05/10/07 09:58 CAS Number ' rest Metfiod: 014797-73-0 tesf Method: Test Parameter EPA 314.0 PERCHLORATE SW-846, 3010A 3010A ACID DIGESTION Result Units Perchlorate - lon Chronnatography , 11.9 ug/L Metals Digestion 05/18/2007 14:00 MDL 2.5 Dilution EQL Factor Analvst Test Date 10 2.5 JMM 05/29/07 MTB 05/18/07 Page 5 of 20 Listing of Results by Sample Sample Delivery Group: 0705027 Client Sample ID: 2185-H-2 HS Sample Description: ATK-DLV - Groundwater Spring 2007 CAS Number ' TestMethod: 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 .TestMethod: 7439-97-6 TestMethod: 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 . 75-25-2 74-83-9 78-93-3 104-51-8 • 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 ^106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 .10061-01-5 Test Parameter Result SkV^846, 60108 (Water) Metals"/\nalysis by icp"-6010 ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE . SILVER TIN ZINC SW-846, 7470A Mercury Analysis MERCURY SW-846, 8260B (Water) Volatile Organic Anaiysis • ACETONE BENZENE BROMOCHLOROI\flETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE . 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBEN2ENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE U 93 U 17. J 29. J 10.5 U U U U U U U U U U u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L-' ug/L ug/L ug/L ug/L , ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 20 2 1 10 20 1 1 30 10 0.3 30 0.22 0.31 0.19 0.37 0.42 0.57 1.1.1 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 ' 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 Laboratory SamplelD: E9L 100 10 5 50 100 5 5 150 50 1 100 10 10 10' 10 10 10 10 1.0 i'p • '10 10 10 10 10 10. 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 0705027-021 Date Sampled: 05/10/07 09:58 Dilution Factor Analvst 1 MTB 1 MTB 1 MTB 1 MTB 1 MTB 1 MTB 1 MTB 1 MTB 1 MTB 1 TCP 1. LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 . LSH 1 LSH 1 LSH 1 LSH 1 LSH •1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH '1 LSH 1 LSH 1 LSH i , LSH i LSH 1 , LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1' LSH 1 LSH 1 . LSH 1 LSH 1 LSH 1 LSH Test Date. 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 : 05/16/07 •- '• 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 . 05/22/07 05/22/07 05/22/07 05/22/07 .05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 Page 6 Of 20 Listing of Results by Sample Sample Delivery Group: 0705027 Client Sample ID: 2185 - H-2 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705027-02 Date Sampled: 05/10/07 09:58 CAS Number TesiMeihod: 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter SIV-846, 82608 (Water) Result Volatile Organic Analysis TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1.2.2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRlCHLOROBENZEt^E 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE . TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYLACETATE VINYL CHLORIDE m.p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 TOLUENE-D8 Units sis U U U U U U U U U U u u u u u 1.1 J u u u u u u u u u • u u u u 106 107 107 96.4 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Dilution EQL Factor Analvst Test Date 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH , LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH . LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 ' 05/22/07 . 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 Client Sample ID: 2186 - H-2 Sampie Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705027-03 DateSampled: 05/10/07 10:33 CAS Number TestMethod: 014797-73-0 TestMef/iod; Test Parameter ' EPA 314.0 _ PERCHLORATE sw-m,3mA 3010A ACID DIGESTION Test Method: SW-846," 60^08 (Water)" 7440-38-2 7440-39-3 7440-43-9 7440-47-3 ARSENIC BARIUM CADMIUM CHROMIUM Result Perchlorate - lon Chromatography Metals Digestion Metals Analysis by 10.6 05/18/2007 14:00 ICP-6010 U 91.7 U 49. J Units ug/L ug/L ug/L ug/L ug/L MDL 2.5 Dilution EQL Factor Analvst Test Date 10 2.5 JMM MTB 05/29/07 05/18/07 20 . 2 1 10 100 10 5 50 1 1 1 1 MTB MTB MTB MTB 06/05/07 06/05/07 06/05/07 06/05/07 Page 7 Of 20 Listing of Results by Sample Sample Delivery Group: 0705027 Client Sample ID: 2186 :Hr2 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705027-03 DateSampled: 05/10/07 10:33 CAS Number ; tesf Meihod: 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6. testi/eiiiod: 7439-97-6 Test Metiiod: 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 . . 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15TO 56-23-5 108-90-7 75-00-3 • 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 Test Parameter "siV-84'6, 60*08 flVater; LEAD MANGANESE SILVER TIN ZINC SIV-846, 747M Result Metals Analysis by ICP - 6010 31. J 17.3 U U U Units ug/L ug/L ug/L ug/L ug/L . MDL 20 1 1 30 10 EQL 100 , 5 5 150 50 Diluti Faci Mercury Analysis MEFiCURY SIV-846, 82608 (Water) ACETONE BENZENE BROMOCHLOROMETHANE . BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE . CARBONTETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-0 ICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLPROETHANE 1,1-DICHLOROETHENE ClS-1,2-DICHLOROETHENE TRANS-1,2-DICHLORPETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE . ETHYLBENZENE 2-HEXANONE Volatile Organic Analysis U ug/L u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 0.3 30 0.22 0.31 0.19 0.37 . 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18, 0.9 0.16 0.7 100 10 10 10 • 10 10 10 10 10 10 •10 • 10 10 • 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 sr Analvst • Test Date • •• MTB .; MTB MTB MTB MTB ,^ , V.J 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 TCP 05/16/07 LSH LSH LSH . LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH . LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 . 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 Page 8 of 20 Listing of Results by Sample Sample Delivery Group: 0705027 Client Sample ID: 2186 - H-2 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705027-03 DateSampled: 05/10/07 10:33 CAS Number : TestMethod: 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00^ 1868-53-7 17060-07-0 2037-26-5 Test Parameter SIV-846, 82608 (Water) Volatile Or HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENECHLORIDE 4-METHYL-2-PENT ANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1.1 -TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYL8ENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m,p-XYLENE O-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 TOLUENE-D8 Result Units u u u u u u u u u u u u u u u u u u u u u u u u u 108 107 106 95.2 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 '10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 Diluti Fad on or Analvst Test Date LSH. LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 Client Sample ID: 2187-FB Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705027-04 DateSampled: 05/10/07 12:48 CAS Number ; TestMethod: 014797-73-0 tes't'iileihod': 'test Method: 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 Test Parameter FPTS'U'O PERCHLORATE SW-846, ioTOA 301 OA ACID DICE SIV-846, 60108 (Wah ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN Result Units Perchlorate - lon Chromatography U ug/L Metals Digestion MDL - Dilution EQL Factor Analvst Test Date 05/18/2007 14:00 JMM MTB 05/29/07 05/18/07 Metals Analysis by ICP - 6010 u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 20 2 1 10 20 1 1 30 100 10 5 50 100 5 5 150 MTB MTB MTB MTB MTB MTB MTB MTB 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 Page 9 of 20 Listing of Results by Sample Sample Delivery Group: 0705027 Client Sample ID: 2187-FB Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratoiy Sample ID: 0705027-04 DateSampled: 05/10/07 12:48 CAS Number •'TestMetiiod: ' 7440-66-6 TesfHethodr 7439-97-6 TesililethodT' • 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75:25-2 74-83-9 78-93-3 104-51-8 '135-98-8 98-06-6 75-15-0 • 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 Test Parameter Result Units " SW-M676dl0fli (Wafer)" ^'"M^ ZINC • U ug/L 'SW-846, 7470/2 " •^rcuT^Anaiysi's MDL Dilution EQL Factor Analvst Test Date MERCURY SW-846, 82608 (Water) Volatile Organic Analysis ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE ' CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1 ;2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLORbBENZENE DICHLORODIFLUOROMETHANE i;i-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE U ug/L is U U U U u u u u u u u . u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 10 • 0.3 50 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 • 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 . 10 10 10 10 10 10 10 10 10 MTB 106/05/07 TCP 05/16/07 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH. LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH • LSH LSH LSH , LSH LSH 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 Page 10 of 20 Listing of Results by Sample Sample Delivery Group: 0705027 Client Sample ID: 2187-FB Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705027-04 Date Sampled: 05/10/07 12:48 CAS Number Test Parameter Result TestMetfiod.' "SW-846, 82608 (Water) Voiatile Organic Analysis 108-10-1 4-METHYL-2-PENTANONE 91-20-3 tgAPHTHALENE 103-65-1 N-PROPYLBENZENE 100-42-5 STYRENE 630-20-6 1,1,1,2-TETRACHLOROETHANE 79-34-5 1,1,2,2-TETRACHLOROETHANE 127-18-4 TETRACHLOROETHENE 108-88-3 TOLUENE 87-61-6 1,2,3-TRICHLOROBENZENE 120-82-1 1,2,4-TRICHLOROBENZENE 71-55-6 1,1,1-TRICHLOROETHANE 79-00-5 1,1,2-TRICHLOROETHANE 79-01-6 TRICHLOROETHENE 75-69-4 TRICHLOROFLUOROMETHANE 96-18-4 1,2,3-TRICHLOROPROPANE 95-63-6 1,2,4-TRIMETHYLBENZEN E 108-67-8 1,3,5-TRIMETHYLBENZENE 108-05-4 VINYLACETATE 75-01-4 VINYL CHLORIDE 1330-20-7 m.p-XYLENE 95-47-6 o-XYLENE 460-00-4 BROMOFLUOROBENZENE 1868-53-7 DIBROMOFLUOROMETHANE 17060-07-0 1.2-DICHLOROETHANE-D4 2037-26-5 TOLUENE-D8 Units sis U U U U U U U U U u u u u u u u u u u • U' u 106 104 103 95.2 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Dilution EQL Factor Analvst Test Date 10 10 10 10 10 10 10 10 10 10 10 10 IO- IO 10 10 10 10 10 10 10 LSH LSH LSH LSH LSH LSH' LSH LSH LSH LSH t LSH LSH LSH . LSH LSH 1 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 Client Sample ID: 2188-EW-6 Sample.Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705027-05 DateSampled: 05/10/07 12:55 CAS Number i TestMethod: 014797-73-0 TestMethod: i "tesiO/letiiod': 7440-38-2 7440-39-3 7440^3-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 test Metfiod: 7439-97-6 Test Parameter JEPA3i4.df PERCHLORATE SW-846, 3010A 3010A ACID DIGESTION SW«^M6J!0i(M/lViiter)^ ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC SIV-846, 7470>1 MERCURY Perchlorate - lon Metals Digestion Result Chromatography 4610 05/18/2007 14:00 Metals Analysis by ICP - 6010 Mercury Analysis U 23.7 U U 20. J 141 U U 86.6 U Units ug/L - ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL Dilution EQL Factor Analvst Test Date 20 JMM 05/29/07 MTB 05/18/07 20 2 1 10 20 1 • 1 30 10 100 10 5 50 100 5 5 150 50 MTB MTB MTB MTB MTB MTB MTB MTB MTB 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 0.3 TCP 05/16/07 Page 11 of 20 Listing of Results by Sample Sample Delivery Group: 0705027 Client Sample ID: 2188 - EW-6 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705027-05 DateSampled: 05/10/07 12:55 CAS Number : T^sif Metfiod: 67-64-1 71,43-2 74-97-5 75-27-4 108-86-1 . 75-25-2 74-83-9 78-93-3 104-61-8 135-98-8 98-06-6 75-15-0 •, 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 . 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 • 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 Test Parameter SlV-¥46, 82608 (Wafer) Volatile Organic ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBONDISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBRbMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE .. 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE Result Analysis U U U U U U U U U U U U U U U U 2.1 J U U U U U U U " U U U u 6.4 J U 61.7 39.1 U U • U U U U U u u u u u u u u u u u u Units ug/L ug/L ug/L ug/L ug/L ug/L • ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL Diiu EQL Fad 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 '• 0.25 0.15 5.86 5.62 5.88 0.66 • 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 100 10 10 10 10 10 10 10 10 io 10 10 10 10 10 10 10 10 10 10 10 • 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 . 10 10 10 10 10 10 10 10 10 10 ion or Analvst Test Date LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH - - . 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 Page 12 of 20 Listing of Results by Sample Sample Delivery Group: 0705027 Client Sample ID: 2188-EW-6 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705027-05 DateSampled: 05/10/07 12:55 CAS Number TestMethod: 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 106-05-4 75-01-4 .1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter Result " SW-846, 82(508 (Wafer) Volatiie Organic Analysis " TETFJACHLOROETHENE . TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYLCHLORIDE m.p-XYLENE O-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 T0LUENE-D8 U U U U U U 263 U U U U U U U U 109 108 105 94.9 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % Bk 0.28 • 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 iSL 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 Dilution Factor ,., ^..^ Analyst LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 Client Sample ID: 2189-H-3 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705027-06 DateSampled: 05/10/07 13:46 Dilution CAS Number TestMethod: 014797-73-0 tesfMeiiiod2 i TestMethod: 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 Test Parameter EPA 314.0 PERCHLORATE ' SiV-846, iOJM 3010A ACID DIGESTION SIV-846, 60108 (Wafer) ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC ....— — — Perchlorate -lon Metals Digestion - Result Chromatography U """"•"• •• "'"-'••'• •"" —. • 05/18/2007 14:00 Metals Analysis by ICP - 6010 - . . U 274 U U 38. J 10.8 U U 12. J • .- - .. Units ug/L .... ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L , MDL 5 '- "~- — 20 2 1 10 20 1 1 30 10 .•,.s^^ .„ EQL 20 100 10 5 50 100 5 5 150 50 . ............ Factor 5 — - 1 , 1 ,....-. . v.v. •:. Analyst JMM " • MTB MTB MTB MTB MTB MTB MTB MTB MTB MTB ^ . .^ Test Date • . 05/29/07 ! 05/18/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 „... . .. . .„ TestMethod: 7439-97-6 fesf Metfiod; 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 SW-846, 7470A MERCURY 'sw2846,'i260B (Water) Mercury Analysis Volatile Organic Analysis U ug/L 0.3 TCP 05/16/07 ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE u u u u u ug/L ug/L ug/L ug/L ug/L ...,„...,.. ... 30 0.22 0.31 0.19 0.37 100 10 10 10 10 ;• "z z •".. zz LSH LSH LSH LSH LSH 05/22/07 05/22/07 05/22/07 '. 05/22/07 05/22/07 Page 13 of 20 Listing of Results by Sample Sample Delivery Group: 0705027 Client Sample ID: 2189-H-3 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705027-06 DateSampled: 05/10/07 13:46 CAS Number ; resfMe"tfio"d; 75-25-2 74-83-9 78-93-3 104-51-8. 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 . 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 '100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 ' 71-55-6 Test Parameter Result """siV-Me, 82608 (Water) Volatile Organic Analysis" BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER ' CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2.2-DICHLOROPROPANE ETHYLBENZENE 2-HEXAN0NE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE • 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE U U U U U U U U U U U U U U U U u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u 1.1 J u u u Units HI ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53- 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 Dilution EQL Factor Analvst Test Date 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10. 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 .10 10 10 10 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 , 05/22/07 . •. 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 ' 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 Page 14 of 20 Listing of Results by Sample Sample Delivery Group: 0705027 Client Sample ID: 2189 - H-3 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratary Sample ID: 0705027-06 Date Sampled: 05/10/07 13:46 CAS Number Test Parameter Result tesVMef/iod: SW-846]^ 82608 (Wafer) ^ Voratjie^rgar^^nalysis 79-00-5 1,1,2-TRICHLOROETHANE 79-01-6 TRICHLOROETHENE 75-69-4 TRICHLOROFLUOROMETHANE 96-18-4 1,2,3-TRICHLOROPROPANE 95-63-6 1,2,4-TRIMETHYLBENZENE 108-67-8 1,3,5-TRIMETHYLBENZENE 108-05-4 VINYLACETATE 75-01-4 VINYLCHLORIDE 1330-20-7 m.p-XYLENE 95-47-6 o-XYLENE 460-00-4 BROMOFLUOROBENZENE 1868-53-7 DIBROMOFLUOROMETHANE 17060-07-0 1,2-DICHLOROETHANE-D4 2037-26-5 TOLUENE-D8 Units sis U U U U U U U U u u 105 108 107 94.5 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 EQk Diluti Faci 10 10 10 10 10 10 10 10 10 10 ion or Analvst Test Date - -••• LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 • 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 Client Sample ID: 2190-H-3 HSD Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705027-07 DateSampled: 05/10/07 13:46 CAS Number ri^sf Metiiod: " 014797-73-0 ; test Method: TestMethod: 7440-38-2 7440-39-3 . 7440-43-9 7440-47-3 7439-92-1 , 7439-96-5 7440-22-4 7440-31-5 7440-66-6 i' tesfiiteiiiod2' 7439-97-6 i test Method: 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 Test Parameter EPA 314.0 PERCHLORATE SW-846, JOIO/l 3010A ACID DIGESTION SW-846, 60108 (Water) f ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC '•jiV^84^'74704 •;•""•'. ZZ MERCURY SW-846, 82608 (Water) ACETONE BENZENE Perchlorate - lon Metals Digestion Metals Analysis b • Mercury Analysis Result Chromatography U 05/18/2007 14:00 y ICP-6010 U 272 U U 41. J 11.5 U u U ;;•"••• T" 1 • u Volatile Organic Analysis BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE u u u u u u u u u u Units ug/L ..... ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L '''."".•. ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL Dilution EQL Factor Analvst Test Date 20 JMM MTB 05/29/07 05/18/07 I."Z' 20 2 1 10 20 1 1 30 10 ZZZ: 100 10 5 50 100 5 5 150 50 . zzzz^ MTB MTB MTB MTB MTB MTB MTB MTB MTB ; 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 0.3 TCP 05/16/07 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 100 10 10 10 10 10 10 • 10 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 . 05/22/07 05/22/07 05/22/07 Page 15 of 20 Listing of Results by Sample Sample Delivery Group: 0705027 Client Sample ID: 2190-H-3 HSD Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705027-07 DateSampled: 05/10/07 13:46 CAS Number : TestMethod: 98-06-6 75-15-0. 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 . 124-48-1 96-12-8 . 74-95-3 106-93-4 95-S0-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-68-6 10061-01-5 10061-02-6 590-20-7 100-41^ 591-78-6, 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 Test Parameter SW-846, 82608 (Water) Volatile Organic An TERT-BUTYLBENZENE CARBONDISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORJVI CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE • 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TFiANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE • HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE . 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1 -TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE Result alysis U u. U U U U U • U U U U U U U U U U U U U u u u u u u u u u , • u u u u u u u u u u u u u 1.5 J u u u u u • u u u Units ... ..... ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . ug/L ug/L ug/L ug/L MDL Dilution EQL Factor Analvst Test Date 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88, 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 -; 0.33 0.19 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 — - LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 Page 16 of 20 Listing of Results by Sample Sample Delivery Group: 0705027 Client Sample ID: 2190 - H-3 HSD Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705027-07 DateSampled: 05/10/07 13:46 Dilution CASNumber ;_ Tesf Method; 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 .• 17060-07-0 2037-26-5 Test Parameter Result SW-846, 82608 (Wafer) Volatile Organic Analysis . 1,3,5-TRIMETHYLBENZENE U VINYL ACETATE U VINYLCHLORIDE U m.p-XYLENE U o-XYLENE U BROMOFLUOROBENZENE 106 DIBROMOFLUOROMETHANE 109 1,2-DICHLOROETHANE-D4 106 TOLUENE-D8 97.5 Units ug/L ug/L • ug/L ug/L ug/L % % % % MDL ^...'..•.vl... 0.29 0.13 0.3 1.6 0.18 EQL 10 10 10 10 10 Factor zzzz^^z Analvst Z:Z.' H LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date .ZZZ.^ZZZZ 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 Client Sample ID: 2191 - H-3 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705027-08 DateSampled: 05/10/07 14:26 CAS Number :" tiesf iWeithoci: 014797-73-0 fesf Metfiod; Test Parameter EPA 314.0 Result Units Perchlorate - lon Chromatography MDL Dilution EQL Factor Analvst Test Date PERCHLORATE SW-846, SdiOA 301 OA ACID DIGESTION : TestMethod: SW-846, 60108 (Water) 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 . 7439-96-5 7440-22-4 7440-31-5 7440-66-6 Tesfiiliethod: 7439-97-6 Tesf Mef/iod; 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 . 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC SW-846, 7470>» MERCURY 's'W-'84M260B"(M^fer/ Metals Digestion U 05/18/2007 Metals Analysis by ICP Mercury Analysis 14:00 eofo U 282 U 15. J 38. J 19.7 U U U ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . 5 20 2 1 10 20 1 1 30 10 20 100 10 5 50 . 100 5 5 150 50 5 1 JMM MTB MTB MTB MTB MTB MTB MTB MTB MTB MTB 05/29/07 ••",".'.'• ZZ 05/18/07 ZZ"' 06/05/07 06/05/07 06/05/07 06/05/07 06/05/07 • 06/05/07 06/05/07 06/05/07 06/05/07 U ug/L 0.3 TCP 05/16/07 Volatile Organic Analysis ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE U u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 Page 17 of 20 Listing of Results by Sample Sample Delivery Group: 0705027 Client Sample ID: 2191-H-3 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705027-08 DateSampled: 05/10/07 14:26 CAS Number Test Parameter Result : tesf MeUiod: SW-8'K2S260B~(Water)_ ^yo'^'i'^JJ^anic Analysis 110-75-8 2-CHLOROETHYLVINYL ETHER 67-66-3 • CHLOROFORM 74-87-3 CHLOROMETHANE 95-49-8 2-CHLOROTOLUENE 106-43-4 4-CHLOROTOLUENE 124-48-1 DIBROMOCHLOROMETHANE 96-12-8 1,2-DIBROMO-3-CHLOROPROPANE 74-95-3 DIBROMOMETHANE 106-93-4 1,2-DIBROMOETHANE 95-50-1 1,2-DICHLOROBENZENE 541-73-1 1,3-DICHLOROBENZENE 106-46-7 1,4-DICHLOROBENZENE 75-71-8 DICHLORODIFLUOROMETHANE 75-34-3 1,1-DICHLOROETHANE 107-06-2 1,2-DICHLOROETHANE 75-35-4 1,1-DICHLOROETHENE 156-59-4 CIS-1,2-DICHLOROETHENE 156-60-5 TRANS-1,2-DICHLOROETHENE 78-87-6 1,2-DICHLOROPROPANE 142-28-9 1,3-DICHLOROPROPANE 563-58-6 1,1-DICHLOROPROPENE 10061-01-6 CIS-1,3-DICHLOROPROPENE 10061 -02-6 TFJANS-1,3-DICHLOROPROPENE 590-20-7 2,2-DICHLOROPROPANE 100-41^ ETHYLBENZENE 591-78-6 2-HEXANONE 87-68-3 HEXACHLOROBUTADIENE 98-82-8 ISOPROPYLBENZENE 99-87-6 4-ISOPROPYLTOLUENE 75-09-2 METHYLENECHLORIDE 108-10-1 4-METHYL-2-PENTANONE 91-20-3 NAPHTHALENE 103-65-1 N-PROPYLBENZENE 100-42-5 STYRENE 630-20-6 1,1,1,2-TETRACHLOROETHANE 79-34-5 1,1,2,2-TETRACHLOROETHANE 127-18-4 TETFIACHLOROETHENE 108-88-3 TOLUENE 87-61-6 1,2,3-TRICHLOROBENZENE 120-82-1 1,2,4-TRICHLOROBENZENE 71-55-6 1,1,1-TRICHLOROETHANE 79-00-5 1,1,2-TRICHLOROETHANE 79-01-6 TRICHLOROETHENE 75-69-4 TRICHLOROFLUOROMETHANE 96-18-4 1,2,3-TRICHLOROPROPANE 95-63-6 1,2,4-TRIMETHYLBENZENE 108-67-8 1,3,5-TRIMETHYLBENZENE 108-05-4 VINYLACETATE 75-01-4 VINYLCHLORIDE 1330-20-7 m,p-XYLENE 95-47-6 o-XYLENE Units sis U U U u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L •ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 . 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Dilut [L Fac . 10 1 10 1 10 1 10 . 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 • 1 10 1 10 1 10 1 10 1 10 . 1 10 1 10 1 10 . 1 10 1 10 1 10 1 10 1 10 1 10 1 10 10 10 10 1 10 10 1 10 1 10 1 10 1 10 1 '10 10 1 10 10 10 10 10 10 10 10 10 10 10 ion tor Analvst .......... . . . LSH . LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH ' LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date 05/22/07 05/22/07 05/22/07 . 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 . 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 • 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 05/22/07 •05/22/07 Page 18 of 20 Listing of Results by Sample Sample Delivery Group: 0705027 Client Sample ID: 2191 - H-3 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705027-08 Date Sampled: 05/10/07 14:26 CAS Number i TestMethod: 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter SW^mfl2!mfWate2f vitotiieO^ianic BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 T0LUENE-D8 Result Analysis 107 108 109 95.7 Units % % % % MDL Dilution EQL Factor Analvst Test Date LSH LSH LSH LSH 05/22/07 05/22/07 05/22/07 05/22/07 Page 19 of 20 Data Reporting Qualifiers U Indicates thiat the analyte was not detected, or the analyte was detected but was below the MDL. B This flag is used when an analyte is found in the blank as well as the sample. Indicates an extimated value. This flag is used either when estimating a concentration for tentatively identified compounds or when the data indicated the presence of a compound that meets the identification criteria but the result is less than the EQL (e.g. 3 J with an EQL of 10). MDL Method Detection Limit: The minimum concentration of a substance that can be confidently measured and reported. The laboratory has demonstrated that the MDL can be achieved in a laboratory reagent blank, but does not guarantee it can be achieved in all sample matrices. EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many analytes the EQL is selected as the value of the lowest standard in the calibration curve. Dilution Dilution Factor: The prepared sample was diluted by this factor because the Factor sample was too concentrated or due to other interferences in the sample matrix. Any dilution factor causes a corresponding increase in the MDL and EQL. Page 20 of 20 ATK Launch Systems Group Environmental Laboratory Client H.n..firflCLfiMxdi ^^ft^^ Z>l.V^ ojpso^y Sample Receipt Checklist Carrier: Q Hand delivered, no cooler Q Hand dsMvered, sample(s) taken out at receiving counter SDG No. Carrier Number: 1070^0X7 MA B counter QDamaged (explain) Seal Number: Other: Cooler Information: Cooler Number/ID: ^fMuOkiht^ Condition ol Shipping Container: Cooler Sealed (taped): Custody Seals Present: Coolant State of Coolant: ThermomelerlD: *i ^^^it'f Ji^ood UYes QYes Qlntact Qlce QFrozen y Reading:. QFair ^0 J*o QBroken QBlue Ice rr QNot Applicable QNot Applicable QNot Applicable Jfk\one ally Frozen QMe -C CF; Corrected Temp:_ Temp Blank Included: QYes QNo Packing Description: Chaln-Of-Custody Inlormation: COC Present: *» ..< -9>/<« P(^^ COC NumtiBr/sl: h /fc- /W f ' COC signed (relinquished and received): JiC<os COC or LWI agrees with sample labels: Si^e% QNo QNo QNo Other: QNot Applicable QNot /Applicable Notes: Sample information: Samples included in cooler: /j? 7/^.5-^^ 7 Custody Seals Present: QYes Qlntact Sample containers intact: f(!^^ Samples in proper containers: : ^es Sufficient sample volume: JV ^^ All samples received in hold time: J^os Water - VOA's tiave zero headspace: ^J^re-presen/ed with HCI; Notes; ^ x>° other. QBroken Seal Number(s). QNo Notes: QNo QNo : QNo VATes QNo QNot />ipplicable QPre-preserved with NajSzOj! , QNon-Preserved: Water - pH acceptable upon receipt: jl^es QAdjusted (see comments below) QNot Applicable HNOj = ^L^ HjSO. = NaOH = '^ ZnAC /NaOH = _HCL =. Water - pH adjusted: (mfg. & Lot No.) HNO3 _____HzS04 NajSOjOj ^Other, Notes: _NaOH _ZnAC _HCI_ SOP-102Form A 0705027 ENVIRONMENTAL LAB WORK REQUEST TO TfflOKOL ENVIRONMENTAL LABORATORY FROM: Dave Covington ORGANIZATION; Environmental Services EXTENSION; 3898 MAILSTOP: 301 LWRNO.E12747 Login No. II COST CENTER; 8200 WORKORDER: 988P LS333 GW DATE; 05/10/07 REPORT RESULTS TO; HELEN RAVSTKN, MS 301 SAMPLE INFORMATION SAMPLE 2184 2185 2186 .2187 2188 2189 2190 2191 DATE 5-10-07 5-10-07 5-10-07 5-10-07 5-10-07 5-10-07 5-10-07 5-10-07 TYPE G C LOCATION HSEB H-2HS H-2 FB EW-6 H-3HS H-3 HSD H-3 TIME 9:05 9:58 10:33 12:48 12:55 13:46 13:46 14:26 TEST , Perchlorate, Metals, (Method 6010), Voc's (Method 8260) Perchlorate, Metals, (Method 6010), Voc's (Method 8260) REMARKS §'Tag:h^;Xisn, |g:ifeS;i?^,X'g,sn, CHAIN OF CUSTODY RELINQUISHED BV DATE TIME RECEIVED BV DATE TIME z 5^-//'^>'7 tuc f'iho7 0%l6? FOR LABORATORY USE ONLY f 1 DATE COMPLETED DATE REPORTED SIGNATURE CERTIFICATE OF ANALYSIS Listing of Sample Information and Testing Requested Friday, June 29, 2007 TESTED FOR: ATK Thiokol: DLV Environmental Monitoring MS 301 , Thiokol Corp, UT 84322 ANALYZED BY: ATK Thiokol Propulsion Environmental Laboratory P.O. Box 707, M/S 245 Brigham City, UT 84302-0707 435-863-3732 435-863-8080 Contact Name: Project: Sample Delivery Group: Dave Covington Ground Water Testing - DLV 0705029 Page 1 of 9 Sample Delivery Group: 0705029 Sample No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 0705029-01 2192-H-4 HS 05/15/07 5/11/2007 10:40:46 EPA 314.0 SW-846, 30IOA SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705029-02 2193-H-4 HSD 05/15/07 5/11/2007 10:40:46 EPA 314.0 SW-846, 301 OA SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705029-03 2194 - H-4 05/15/07 5/11/2007 11:24:46 EPA 314.0 SW-846, 301 OA SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water Certified By: W. Scott Fraser, Quality Assurance Officer 06/29/2007 Date This certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation Program (NELAP) unless otherwise annotated: Page 2 of 9 Listing of Results by Sample Sample Delivery Group: 0705029 Client Sample ID: 2192 - H-4 HS Sample Description:. ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705029-01 Date Sampled: 05/11/07 10:40 CAS Number test Method: 014797-73-0 ; TestMethod: TestMethod: 7440-38-2 7440-39-3 7440-43-9 7440^7-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 reVtiWethod: 7439-97-6 Test Metfiod; 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106^3-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 Test Parameter EPA 3i4^d _ PERCHLORATE '~SW-846,3010A' Result Units Perchlorate - lon Chromatography 41.4 ug/L Metals Digestion 3010A ACID DIGESTION 05/19/2007 09:00 SW-846, 601 OB (Water) ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC 'SW-m,7470A ' " MERCURY SW-84628260B (Water) Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1.2-DICHLOROETHANE 1,1-DICHLOROETHENE U 95.8 U 19. J 29. J 64.9 U U 21. J ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L U ug/L u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 2.5 0.3 Dilution EQL Factor Analvst Test Date 10 2.5 JMM TCP 06/05/07 20 2 1 10 20 1 1 30 10 100 10 5 50 100 5 5 150 50 1 1 1 1 1 1 1 1 1 1 MTB MTB MTB MTB MTB MTB MTB MTB MTB MTB . 05/19/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 05/21/07 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 . 10 10 10 10 10 10 10 10 10 10 10 10 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Page 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 . 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 3 Of 9 Listing of Results by Sample Sample Delivery Group: 0705029 Client Sample ID: 2192-H-4 HS Sample Oescription: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705029-01 Date Sampled: 05/11/07 10:40 CAS Number Tesftilethodl 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter SW-846, 8260B (Water) Volatile C CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE . 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1.2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m.p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 T0LUENE-D8 Result Units u u u u u u u u u u u u u u u u u u u u u 'l.6J u u u u u u u u u u u u u 106 109 107 95.5 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Dilution EQL Factor Analvst Test Date 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH • LSH LSH LSH LSH LSH LSH LSH • ' •• 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 05/23/07 Client Sample ID: 2193-H-4 HSD Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705029-02 Date Sampled: 05/11/07 10:40 CAS Number • tesfMethodi' 014797-73-0 : TestMethod: . Test Parameter "EPA 31 i'o '""""" PERCHLORATE Result Units SW-846, 3010A 3010A ACID DIGESTION Perchlorate - lon Metals Digestion Chromatography 36.9 05/19/2007 09:00 ug/L MDL 2.5 Dilution EQL Factor Analvst Test Date 10 2.5 JMM 06/05/07 MTB 05/19/07 Page 4 of 9 Listing of Results by Sample Sample Delivery Group: 0705029 Client Sample ID: 2193 vH-4 HSD Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705029-02 Date Sampled: 05/11/07 10:40 CAS Number tesi Method: 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 Test Metfiod: 7439-97-6 TestMethod: 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59^ 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 Test Parameter SW-846, VdTOB (Waierf ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC SW-846, 747dA MERCURY SW-846, 8260B (Water) Result Metais Analysis by ICP - 6010 U 95.8 U U 31. J 122 U U . 11. J Mercury Analysis Volatile Organic Analysis ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBRqMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL Dilution EQL Factor Analvst Test Date U ug/L 20 2 1 10 20 1 1 30 10 0.3 100 10 5 50 100 5 5 150 50 MTB MTB MTB MTB MTB MTB MTB MTB MTB TCP 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 05/21/07 u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 .5.86 5.62 . 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 100 10 10 10 10 10 10 10 10 10 lo 10 10 10 10 10 10 10 10 10 10 10' 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH . LSH LSH LSH LSH LSH LSH ' LSH LSH 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 . 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 • 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 Page 5 of 9 Listing of Results by Sample Sample Delivery Group: 0705029 Client Sample ID: 2193-H-4 HSD Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705029-02 Date Sampled: 05/11/07 10:40 CAS Number i TestMethod: 10061-02-6 590-20-7 100-41-4 . 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 ' 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter SIV-846, 82608 (Water) Volatile Organic . TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOFiOPROPANE ETHYLBENZENE . 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE . TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1 -TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m,p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 TOLUENE-D8 Result Analysis U U U U U U U U U U U U U U u 2.2 J U U U U U U u u u u u u u 108 95.9 99.3 109 Units .-.-.- ug/L ug/L ug/L . ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 . 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 . 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Dilut EQL Fac 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 ion tor Analvst , .. „ LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date .......— ; 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 ' 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 Client Sample ID: 2194 - H-4 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705029-03 DateSampled: 05/11/07 11:24 Dilution CAS Number testMeiiiod: 014797-73-0 ; TesfMefftod; ; TesfWeihod: ~ 7440-38-2 7440-39-3 7440-43-9 7440-47-3 Test Parameter EPA 314.0 PERCHLORATE SW-846, 3010A 3010A ACID DIGESTION ''sW-M6,6mB(Wa^0 Z ARSENIC BARIUM CADMIUM CHROMIUM Result Perchlorate - lon Chromatography 41.5 Metals Digestion 05/19/2007 09:00 Metals Analysis by ICP - 6010 U 98.3 U 24. J Units .„_ ..„ ug/L ZZ."'~Z ug/L ug/L ug/L ug/L MDL ZZ.ZZZ 2.5 ; ZZ..ZZZ 20 2 1 10 EQL 10 100 10 5 50 Factor ••:.•• •„•,..•. ••,•,., 2.5 1 ZZ.ZZZ 1 1 1 1 Analyst JMM MTB ZZZZZZ^ MTB MTB MTB MTB Test Date •.::;.;! 06/05/07 05/19/07 "" ' 06/06/07 06/06/07 06/06/07 06/06/07 Page 6 of 9 Listing of Results by Sample Sample Delivery Group: 0705029 Client Sample ID: 2194 - H-4 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705029-03 DateSampled: 05/11/07 11:24 CAS Number ' TestMethod: 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 I ' TestMethod: 7439-97-6 Test Mettiod: 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 ' 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93^ 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 Test Parameter SW-m, 60108 (Water) LEAD MANGANESE SILVER TIN ZINC Result Metals Analysis by ICP - 6010 30. J 53.2 U U u Units ug/L ug/L ug/L ug/L ug/L MDL Dilution EQL Factor Analvst Test Date SIV-846, 7470A MERCURY SW-846, 82608 (Water) Mercury Analysis Volatile Organic Analysis ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE • DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE U ug/L u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 20 1 1 30 10 100 5 5 150 50 0.3 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 MTB MTB MTB MTB MTB TCP 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 05/21/07 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH •LSH LSH LSH LSH 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 . 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 Page 7 of 9 Listing of Results by Sample Sample Delivery Group: 0705029 Client Sample ID: 2194-H-4 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705029-03 Date Sampled: 05/11 /07 11:24 Diiution CAS Number : TestMeOiodr 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108r88-3 87-61-6 120-82-1 71-55-6 79-00-5 " 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter SW-846, 8260B (Water) VolaTile Organic HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLbROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1 -TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m,p-XYL£NE O-XYLENE .BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 TOLUENE-D8 Result Analysis U U U U u u u u u u u u u u u u 2. J u u u u u u u . u 113 94.7 98.1 110 Units ug/L • ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % • % % MDL 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 EQL Fac 10 1 10 1 10 1 10 1 10 1 • 10 1 10 1 10 1 10 1 10 1 10 1 10 1 .10 . 1 1.0 1 • 10 . 1 10 1 10 1 10 1 10 1 10 1 10 1 10 10 10 10 tor Analvst LSH LSH LSH • LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH" . LSH LSH LSH LSH LSH LSH LSH LSH Test bate . -, 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 , 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 05/24/07 Page 8 of 9 Data Reporting Qualifiers U Indicates ttiat the analyte was not detected, or the analyte was detected but was below the MDL. B This flag is used when an analyte is found in the blanlc as well as the sample. Indicates an extimated value. This flag is used either when estimating a concentration for tentatively identified compounds or when the data indicated the presence of a compound that meets the identification criteria but the result is less than the EQL (e.g. 3 J with an EQL of 10). MDL Method Detection Limit: The minimum concentration of a substance that can be confidently measured and reported. The laboratory has demonstrated that the MDL can be achieved in a laboratory reagent blank, but does not guarantee it can be achieved in all sample matrices. EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many analytes the EQL is selected as the value ofthe lowest standard in the calibration curve. Diiution Dilution Factor: The prepared sample was diluted by this factor because the Factor sample was too concentrated or due to other interferences in the sample matrix. Any dilution factor causes a corresponding increase in the MDL and EQL. Page 9 of 9 ATK Launch Systems Group Environmental Laboratory Sample Receipt Checklist Iz^fiv^ COD lui.^ l-ix*^ (Py^S'iPzf Client Name:. SNo. 070*rO^^ Carrier: Q Hand delivered, no cooler Carrier Number:. Q Hand delivered, sample(s) laken out at receiving counter _KA Cooler Information y^^c/ k\jOW\<^ Cooler Number/ID:. Condition of Shipping Container. Cooler Sealed (taped): Custody Seals Present: Coolant: State ol Coolant: _. Thermometer \0-.UiSfv*^^ Heading:. Packing Description: ^l^ood QYes QYes Qlntact Qlce •Frozen •Fair ;^o J^o •Broken •Blue Ice ji(iaT\e QP^ially Frozen ."C CF: •Not Applicabla QNot Applicable QNot Applicabla QDamaged (explain). Seal Number: Other: QMelted Correcled Temp:. Temp Blank Included: QYes QNo. Chain-Of-Custody Information: COC Present: «- , <- 'j.i & COC Himbml^s) f;. I/ /If fi COC signed (relinquished and receivad): COC or LWI agrees with sample labels: ^e •No •No •No Other: •Not /Applicable QNot Applicable Sample Information: Samples included in cooler: cpypsip ;?^ Custody Seals Present: Sample containers intact: Samples in proper coniainers; Sufficient sample volume: All samples received in hold time: •Yes Qlntact iCfes Sf^es <*^Yes Xes /ttto •Bra •No QNo QNo QNo Water - VOA's have zero headspace: JSfre-presarved w/ith HCl: Notes: Other. •Broken Seal Number(s). Notes: res QNo QNot Applicable F're-preserved with NajSjOj •Non-Preserved: Jfies •Adjusted (see comments below) QNot Applicable Water - pH acceptable upon receipt: HNO, _H;SO. _NaOH = _ZnAC /NaOH =. _HCL = Water • pH adjusted; (mfg. & Lot No.) HNOj HzSO,. NajSOiO, Other _ Notes: _NaOH. _ZnAC. _HCI SOP-102Fomi A 0705029 ENVIRONMENTAL LAB WORK REQUEST TO THIOKOL ENVIRONIVIENTAL LABORATORY FROM: Dave Covington ORGANIZATION: Environmental Services EXTENSION: 3898 MAILSTOP: 301 LWRNO.E12748 Login No. COST CENTER 8200 WORKORDER: 988P LS333 GW DATE. 05/11/07 REPORT RESULTS TO: HELEN RAVSTEN, MS 301 SAMPLE INFORMATION SAMPLE 2192 2193 2194 DATE 5-11-07 5-11-07 5-11-07 TYPE G C LOCATION H-4HS H-4 HSD H-4 TIME 10:40 10:40 11:24 TEST Perchlorate, Metals, (Method 6010), Voc's (Method 8260) Perchlorate, Metals, (Method 6010), Voc's (Method 8260) 1 REMARKS g;j»S:hi;X'g,sn, ||:iSs:ki;Xisrt, CHAIN OF CUSTODY RELINQUISHED BV DATE TIME RECEIVED BV /(Iy^6ll6> 9-fS- DATE TIME :A2^ ^^-/-s-^7 /^;^7 •07 N^7 FOR LABORATORY USE ONLY > DATE COMPLETED DATE REPORTED SIGNATURE CERTIFICATE OF ANALYSIS Listing of Sample Information and Testing Requested Friday, June 29, 2007 TESTED FOR: ATK Thiokol: DLV Environmental Monitoring MS 301 Thiokol Gorp, UT 84322 ANALYZED BY: ATK Thiokol Propulsion Environmental Laboratory P.O. Box 707, M/S 245 Brigham City, UT 84302-0707 435-863-3732 435-863-8080 Contact Name: Project: Sample Delivery Group: Dave Covington Ground Water Testing - DLV 0705030 Page 1 of 14 Sample Delivery Group: 0705030 Sample No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 0705030-01 2195 - H-7 HS 05/15/07 5/16/2007 08:40:31 EPA 314.0 SW-846, 3010A SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705030-02 2196-H-7 EPA 314.0 SW-846, 3010A SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) 0705030-03 2197-H-7 EB 05/15/07 5/16/2007 08:42:31 Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 05/15/07 5/16/2007 08:42:31 EPA 314.0 SW-846, 301 OA SW-846, 6010B (Water) SW-846, 7470A SW-846, 8260B (Water) 0705030-04 2198 - H-8 HS EPA 314.0 SW-846, 301 O.A SW-846, 60IOB (Water) SW-846, 7470A SW-846, 8260B (Water) 0705030-05 2199-H-8 Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 05/15/07 5/16/2007 08:42:31 Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 05/15/07 5/16/2007 08:42:31 EPA 314.0 SW-846, 301 OA SW-846, 60100 (Water) SW-846, 7470A Perchloi-ate - ion Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Water Water Water Water Page 2 of 14 V Sample Delivery Group: 0705030 Sample No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 0705030-05 2199-H-8 05/15/07 5/16/2007 08:42:31 SW-846, 8260B (Water) Volatile Organic Analysis Water Certified By: W. Scott Fraser, Quality Assurance Officer 06/29/2007 Date This certifies that the following data meets the requirements ofthe National Environmental Laboratory Accreditation Program (NELAP) unless otherwise annotated: Page 3 of 14 Listing of Results by Sample Sample Delivery Group: 0705030 Client Sample ID: 2195-H-7 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705030-01 DateSampled: 05/16/07 08:40 CAS Number : TestMethod: 014797-73-0 i Test Metiiod: Test Parameter M^V^-L^ZZ... PERCHLORATE "SliV-M67301CI/l Result Units Perchlorate - lon Chromatography U ug/L Metals Digestion 3010A ACID DIGESTION TestMeOiod: 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 test if^od: 7439-97-6 Test Metiiod: 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1. 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 SW-846, 60108 (Water) ARSENIC BARIUIVl CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC Sm46,7470A MERCURY SW-84628260B (Water) Mercury Analysis Volatile Organic Analysis ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE MDL 2.5 Dilution EQL Factor Analvst Test Date 05/19/2007 09:00 Metals Analysis by ICP - 6010 U ug/L 80.2 ug/L . U ug/L U ug/L 27.J ug/L 7.39 ug/L U ug/L U ug/L U ug/L U ug/L 0.3 10 2.5 JMM TCP 06/05/07 20 2 1 10 20 1 1 30 10 100 • 10 5 50 100 5 5 150 50 1 MTB MTB MTB MTB MTB MTB MTB MTB MTB MTB 05/19/07 06/06/07 . 06/06/07 06/06/07 06/06/07 • 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 05/21/07 u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L . ug/L ug/L Og/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 30 0.22 0.31 0.19 0.37 0.42 0.57 . 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH • LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 . 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 Page 4 of 14 Listing of Results by Sample Sample Delivery Group: 0705030 Client Sample ID: 2195-H-7 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705030-01 DateSampled: 05/16/07 08:40 Dilution CAS Number \ test Method: 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter SIV-846, «260fi (Water) Volatile Organic CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1 -TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE • 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m.p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 TOLUENE-D8 Result Analysis U U U U u u u u u • u u u u u u u u u u u u u u u u u u u u u u u u u u 108 102 112 98.4 Units —• ug/L ug/L ug/L ug/L ug/L ug/L ug/L • ug/L ug/L ug/L ug/L ug/L • ug/L ug/L ug/L ug/L ug/L ug/L ug/L • ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 EQL —'•—- 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 Factor Analvst • -" "- LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH . LSH LSH LSH • LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date •*•" •••••- 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 . 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 05/29/07 Client Sample ID: 2196 - H-7 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705030-02 DateSampled: 05/16/07 08:42 CAS Number ''~test"Meih'odr 014797-73-0 : TestMethod: Test Parameter '"EPA'Sl/F'ff'ff PERCHLORATE SW-846, ididA 301 OA ACID DIGESTION Result Units Perchlorate - lon Chromatography U ug/L Metals Digestion 05/19/2007 09:00 MDL 2.5 EQL . .............. 10 Dilution Factor Analvst Test Date 2.5 JMM 06/05/07 MTB 05/19/07 Page 5 of 14 Listing of Results by Sample Sample Delivery Group: 0705030 Client Sample ID: 2196-H-7 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705030-02 Date Sampled: 05/16/07 08:42 CAS Number testMeiiiod: 7440-38-2 7440-39-3 7440-43-9 , 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 test Mettiod: Test Parameter '~ SW-846, 60108 (Water) ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC SW-846, 7470A Result Metals'Analysis by ICP - ioio" U 81.9 U U 28. J 1.6 J U U 29. J Mercury Analysis Units ^.^^.•'.^:.. ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 7439-97-6 TestMethod: MERCURY SW-846, 82608 (Water) Volatile Organic Analysis 67-64-1 71-43-2 74-97-5 . 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93^ 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 . 142-28-9 563-58-6 10061-01-5 ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE , 1,1-OlCHLOROETHENE ^ CIS-1,2-DICHLOROETHENE TRANS-1,2-OICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1 -DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE U ug/L U u u u u u . u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 0.3 Dilution EQL Factor Analvst Test Date _ ^ 20 2 1 10 20 1 1 30 10 100 . 10 5 50 100 5 5 150 50 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 MTB MTB MTB • MTB MTB MTB MTB MTB MTB 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 . 06/06/07 06/06/07 06/06/07 TCP 05/21/07 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 Page 6 of 14 Listing of Results by Sample Sample Delivery Group: 0705030 Client Sample ID: 2196-H-7 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705030-02 DateSampled: 05/16/07 08:42 CAS Number Test Parameter 2 test Meiiiod: _^ SW-846, 82608 (Water) Volatile Organic Analysis 10061-02-6 TRANS-1,3-DICHLOROPROPENE 590-20-7 2,2-DICHLOROPROPANE 100-41-4 . ETHYLBENZENE 591-78-6 2-HEXANONE 87-68-3 HEXACHLOROBUTADIENE 98-82-8 ISOPROPYLBENZENE 99-87-6 4-ISOPROPYLTOLUENE .,, 75-09-2 METHYLENE CHLORIDE 108-10-1 4-METHYL-2-PENTANONE 91-20-3 NAPHTHALENE 103-65-1 N-PROPYLBENZENE 100-42-5 STYRENE 630-20-6 1,1,1,2-TETRACHLOROETHANE 79-34-5 1,1,2,2-TETFJACHLOROETHANE 127-18-4 TETRACHLOROETHENE 108-88-3 TOLUENE 87-61-6 1,2,3-TRICHLOROBENZENE 120-82-1 1,2,4-TRICHLOROBENZENE 71-55-6 1,1,1-TRICHLOROETHANE " 79-00-5 1,1,2-TRICHLOROETHANE 79-01-6 TRICHLOROETHENE 75-69-4 TRICHLOROFLUOROMETHANE 96-18-4 1,2,3-TRICHLOROPROPANE 95-63-6 1,2,4-TRIMETHYLBENZENE 108-67-8 1,3,5-TRIMETHYLBENZENE 108-05-4 VINYLACETATE 75-01^ VINYLCHLORIDE 1330-20-7 m.p-XYLENE 95-47-6 o-XYLENE 460-00-4 BROMOFLUOROBENZENE 1868-53-7 DIBROMOFLUOROMETHANE 17060-07-0 1,2-DICHLOROETHANE-D4 2037-26-5 T0LUENE-D8 Result sis U U U U U u u u u u u u u u u u u u u u u u u u u u u u u 109 99.3 98.8 100 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 EQL 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10. Dilut Fact — ion or Analvst ••-• LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date 05/30/07 05/30/07 05/30/07 05/30/07 • 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 Client Sample ID: 2197 - H-7 EB Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705030-03 DateSampled: 05/16/07 08:42 CAS Number \ tfsfMettiod: 014797-73-0 \ tesfMetiiod2 Test Parameter "EPA3i'4.0 • PERCHLORATE l:Mtg4M0i;M 301 OA ACID DIGESTION Test Mettiod: SW-846, 6010B (Water) 7440-38-2 7440-39-3 7440-43-9 7440-47-3 ARSENIC BARIUM CADMIUM CHROMIUM Result Units Perchlorate - lon Chromatography U ug/L . Metals Digestion 05/12/2007 • 09:00 Metals Analysis by ICP - 6010 U ug/L U ug/L U ug/L U ug/L M Dilution EQL Factor Analvst Test Date 2.5 10 2.5 JMM MTB 06/05/07 05/12/07 20 2 1 10 100 10 5 50 1 1 1 1 MTB MTB MTB MTB ""! 06/06/07 06/06/07 06/06/07 06/06/07 Page 7 Of 14 Listing of Results by Sample Sample Delivery Group: 0705030 Client Sample ID: 2197 - H-7 EB Sampie Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705030-03 DateSampled: 05/16/07 08:42 CAS Number Test Method; 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 Test Metfiod:- 7439-97-6 Test Metfiod: 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 • 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124,-48-1 96-12-a 74-95-3 106-93-4 95-50-1 •. 541-73-1 106-46-7 . 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 AOO-At-4 591-78-6 Test Parameter SW-846, 60108 (Water) Metals Anaiysis b LEAD MANGANESE SILVER TIN ZINC SW-846,7470A Mercury Analysis MERCURY SyV-846, 8260B (Water) Volatile Organic f ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMEJHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-0/8ROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMEtHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENIENE 2-HEXANONE Result Units U ug/L U ug/L U ug/L U ug/L U ug/L MDL Diluti Faci U ug/L u u u u u u u u u u u u u u u .u u u u u u u u u u- u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug)L ug/L 20 •.• 1 1 30 • 10 • 100 5 5 150 50 0.3 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 . 0.9 O.ie 0.7 , 100 10 10 10 10 10 10 10 10 10 . 10 10 10 10 .10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 . 10 10 10 10 10 10 •\o 10 gr Analvst Test Date MTB MTB MTB MTB MTB TCP LSH LSH LSH . LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH . LSH LSH Page 8 of - • 06/06/07 . 06/06/07 06/06/07 06/06/07 06/06/07 05/21/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 . 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 - 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 OSCiOfOT 05/30/07 14 Listing of Results by Sample Sample Delivery Group: 0705030 Client Sample ID: 2197-H-7 EB Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705030-03 DateSampled: 05/16/07 08:42 CAS Number TesfMef/iod; 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108:67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter SIV-846, 8260B (Water) Result Volatile Organic Analysis HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENECHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYLCHLORIDE m,p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 TOLUENE-D8 Units Dilution MDL EQL Factor Analvst Test Date u u u u u u u u u u u 0.7 J u u u u u u u u u u u u u 108 96.5 105 98.8 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 . 0.85 .• 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0,33 0.19 0.29 0.13 0.3 1.6 0.18 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 . 10 10 10 10 10 , 1 - —•• LSH LSH LSH LSH LSH LSH . LSH LSH LSH LSH LSH LSH' LSH LSH LSH . LSH LSH. LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/30/07 05/30/07 . 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 . 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 • 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 Client Sample ID: 2198-H-8 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705030-04 DateSampled: 05/16/07 08:42 CAS Number : Test Metiiod: 014797-73-0 2 TestMeOiod: '' TestMeOiod: 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 ' 7439-96-5 7440-22-4 7440-31-5 Test Parameter EPA 314.0 • PERCHLORATE SW-846, 301 OA 3010A ACID DIGESTION SW.846, 6010B (Water) ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN' Result Perchlorate - lon Chromatography U. Metals Digestion 05/19/2007 09:00 Metals Analysis by ICP - 6010 U 90 U 15. J 27. J 33.3 U U Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 2.5 Dilution EQL Factor Analvst Test Date 10 2.5 JMM MTB 06/05/07 05/19/07 20 2. 1 10 20 1 1 30 100 10 5 50 100 5 5- 150 MTB MTB MTB MTB MTB MTB MTB. , MTB 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 Page 9 of 14 Listing of Results by Sample Sample Delivery Group: 0705030 Client Sample ID: 2198 - H-8 HS Sample Description: ATI<-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705030-04 DateSampled: 05/16/07 08:42 CAS Number testMeihod2 7440-66-6 Testilettiod: 7439-97-6 : TestMettioil: 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 . 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59^ 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 Test Parameter SIV-846, 60J0B (Water; Metals Ana ZINC SW-846, 74704 Mercury Ar MERCURY SW-846, 8260B (Water) Volatile Ore ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM' BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVlNYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBEN2ENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1 -DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE Result Units U ug/L MDL Oiluti EQL Fac U ug/L. U U U U U U U U U U U U u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . 10 0.3 50 30 • 0.22 0.31 0.19 ; 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0:3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 100 10 .10 10 10 10 10 10 10 10 10 10 10 10 10 10 . 10 10 10 10 10 10 10 10 . 10 10' 10 10 10 10 10 10 10 10 10 10 10 10 10 10 • 10 10 10 10 10 gr Analvst Test Date MTB TCP 06/06/07 05/21/07 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH , LSH LSH LSH . LSH LSH LSH LSH LSH LSH LSH LSH • 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 . 05/30/07 05/30/07 05/30/07 05/30/07 • 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 Page 10 of 14 Listing of Results by Sample Sample Delivery Group: 0705030 Client Sample ID: 2198 - H-8 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705030-04 DateSampled: 05/16/07 08:42 CASNumber : TesfMeOiodf 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 . 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 . 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter Result SW-846','8260B (Wate'ir) Volatile brganic Analysis 4-METHYL-2-PENTANONE NAPHTHALENE N-PFiOPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1 -TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m,p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 TOLUENE-D8 U U U U U U U 0.9 J U u u u u u u u u u u u u 110 97.7 102 ior Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Diluti EQL Fad 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 lOi on ;or Analvst Test Date LSH LSH LSH LSH LSH LSH. LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH . LSH LSH LSH 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 Client Sample ID: 2199-H-8 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705030-05 DateSampled: 05/16/07 08:42 CAS Number TestMethod: 014797-73-0 TestMeOiod: TestMethod: 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 fest Metfiod; 7439-97-6 Test Parameter Ef>A314.0 PERCHLORATE SW-846, 30iOA 3010A ACID DIGESTION SW-846, 60108 (Water) ARSENIC BARIUM CADMIUM CHROMIUM LEAD • MANGANESE SILVER TIN ZINC SW-846,747dA MERCURY Result Perchlorate - lon Chromatography U Metals Digestion 05/19/2007 09:00 Metals Analysis by ICP - 6010 U 113 . U 29. J 32. J 157 U U 21. J Mercury Analysis U Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL Dilution EQL Factor Analvst Test Date 2.5 10 2.5 JMM MTB 06/05/07 05/19/07 20 2 1 10 20 1 1 30 10 100 10 5 50 100 5 5 150 50 MTB MTB MTB MTB MTB MTB MTB- MTB • MTB 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 0.3 TCP • 05/21/07 Page 11 of 14 Listing of Results by Sample Sample Delivery Group: 0705030 Client Sample ID: 2199-H-8 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705030-05 DateSampled: 05/16/07 08:42 CAS Number Test Metfiod; 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 • 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 • 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 . 103-65-1 100-42-5 630-20-6 79-34-5 Test Parameter SW-846, 8260B(Watefj" Volatile Organic ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE. . BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETFiACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLORbPROPANE 1,3-DlCHLOROPRbPANE 1,1-DICHLOROPROPENE ClS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-lSOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1.2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE Result Analysis U U U U . U U U . U u u u' u . u u u u u u u u u u u u u u u u u u u u u u u u u u u • u u u u u u u u u u u u Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L rUg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L u'g/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL Dilution EQL Factor Analvst Test Date 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3' 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 ' 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 •LSH LSH LSH LSH LSH , LSH LSH • LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 Page 12 of 14 Listing of Results by Sample Sample Delivery Group: 0705030 Client Sample ID: 2199 - H-8 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705030-05 DateSampled: 05/16/07 08:42 CAS Number TesiMettiod2 . 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 ., 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 . 460-00-4 1868-53-7 .17060-07-0 2037-26-5 Test Parameter "SW-846, 82608 (Water) Volatile Organic .. TETRACHLOROETHENE TOLUEhJE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE . 1.1,2-TRICHLOROETHANE TRICHLOROETHENE . TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m.p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 TOL'UENE-D8 Result Analysis U U U U U U U u , U u u u u u u 108 99.6 110 98.6 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Dilut EQL Fac •^•• 10 1 10 1 • 10 1 • 10 • 1 10 1 10 1 • 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 • 1 ion tor Analvst ..... . LSH • LSH LSH LSH LSH ' LSH • LSH . LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date 05/30/07 05/30/07 • 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 Page 13 of 14 Data Reporting Qualifiers U Indicates tttat tlie analyte was not detected, or ttie analyte was detected but was below the IVIDL. B Ttiis flag is used wlien an analyte is found in ttie blank as well as the sample. Indicates an extimated value. This flag is used either when estimating a concentration for tentatively identified compounds or when the data indicated the presence of a compound that,meets the identification criteria but the result is less than the EQL (e.g. 3 J with an EQL of 10). IVIDL Method Detection Limit: The minimum concentration of a substance that can be confidently measured and reported. The laboratory has demonstrated that the MDL can be achieved in a laboratory reagent blanlc, but does not guarantee it can be achieved in all sample matrices. EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many analytes the EQL is selected as the value of the lowest standard in the calibration curve. Dilution Dilution Factor: The prepared sample was diluted by this factor because the Factor sample was too concentrated or due to other interferences in the sample matrix. Any dilution factor causes a corresponding increase in the MDL and EQL. Page 14 of 14 0705^0^0 ATK Launch Systems Group Environmental Laboratory Sample Receipt Checklist eliv( Client Name: Carrier: % OJJ'C LO\/\t^<,^-t>^ SDQ No. ig>7vyo-i^ Carrier Number:_ • Hand delivered, no cooler Q Hand deTivered, sample(s) taken out at receiving counter JiA_ Cooler Information: Cooler Number/ID: k/i/cg> k iO^iU^ Condition of Shipping Container- Cooler Sealed (taped): Cuslody Seals Present: Coolant: State of Coolant: Thermomeler ID: If I ^H Tfl'i^ Readii bGood QYes QYes Qlntact Qlce QFrozeri mg: QFair ^0 Xlo QBroken QBlue Ice ^l^one QPartially Frozen \S^ °C CF: QNot Applicable QNot Applicable QNot Applicable QDamaged (explain). Seal Number: Other: QMelted Corrected Temp:. _°C Temp Blank Included: QYes QNo Packing Oescription: jLtce^v^ ^^fCt. 'Crt^r^^PitXtf Chain-Of-Custody Information: COC Present: /^ IJ^ rte^/) J^^^ cnr. NL;mber/fil/*y / X V> 1/ ^ ' , COC signed (relinquished and received): ^e% COC or LWI agrees with sample labels: jC'es QNo QNo QNo Other:. QNot Applicable QNot Applicable NntBS- Sample Information: Samples ir^cluded in cooler: Ol 0^01.0 •...-.• • • • Custody Seals Present: Sample containers intact: Samples in proper containers: Sufficient sample volume: All samples received in hold time: Water - VOAs have zero headspace: jaPre-preserved with HCl: Notes: QYes Qlntact J^es »^es- l^es jH^-es ;a»|o QBro QNo QNo QNo QNo Other. QBroken Seal Number(s). Notes: Ji(fes QNo QPre-preserved with NajSjO,: QNot Applicable QNon-Preserved: Water - pH acceptable upon receipt: HNO3 Wi/es QAdjusted (see comments below) QNot Applicable .HzSO. = NaOH = ZnAC /NaOH = -HCL =. Water - pH adjusted; (mfQ. & Lot No.) HNOj ; H2SO.. NajSOiOj : Other _ Notes; _NaOH. _ZnAC. _HCI_ SOP-102Form A 0705030 ENVIRONMENTAL LAB WORK REQUEST TO THIOKOL ENVIRONMENTAL LABORATORY FROM: Dave Covington ORGAtflZATION: Environmental Services EXTENSION: 3898 MAILSTOP: . 301 LWRNO.E12750 Login No. II COST CENTER; 8200 WORK ORDER; 988P LS333 GW DATE: 05/15/07 • . REPORT RESULTS TO HELEN RAVSTEN, MS 301 SAMPLE 2195 2196 2197 2198 2199 • DATE 5-15-07 5-15-07 5-15-07 5-15-07 5-15-07 TYPE G c SAMPLE INFORMATION LOCATION H-7 HS H-7 H-7 EB H-8 HS H-8 TIME 11:58 12:23 12:31 13:02 13:38 TEST Perchlorate, Metals, (Method 6010), Voc's (Method 8260) Perchlorate, Metals, (Method 6010), Voc's (Method 8260) ,1 <^ -t^ IV ,» •- REMARKS f*k^g;kisn. |g:i8^'klX'g.sn, ,^^r^ < l- A <* CHAIN OF CUSTODY RELINQUISHED BV • • r- ^ ^ y AS?-^ i,-,--^ ^^^ DATE ^~ Y^'Z^y FOR TIME /^.•3 7 LABORATOF RECEIVED BY V'/^/W' LY USE ONLY DATE j^^/r-o? TIME f</27 DATE COMPLETED DATE REPORTED SIGNATURE CERTIFICATE OF ANALYSIS Listing of Sample Information and Testing Requested Friday, May 04, 2007 TESTED FOR: ATK Thiokol: DLV Environmental Monitoring MS 301 Thiokol Corp, UT 84322 ANALYZED BY: ATK Thiokol Propulsion Environmental Laboratory P.O. Box 707, M/S 245 Brigham City, UT 84302-0707 435-863-3732 435-863-8080 Contact Name: Project: Sample Delivery Group: Dave Covington Ground Water Testing - DLV 0704033 Page 1 of 15 Sample Delivery Group: 0704033 Sample No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 0704033-01 2153-Trip Blank SW-846, 8260B (Water) 0704033-02 2154-J-2 EPA 314.0 SW-846, 3010A SW-846, 6010B (Water) SW-846, 7470A SW-846, 8260B (Water) 0704033-03 2155-J-2D EPA 314.0 SW-846, 301 OA SW-846, 6010B (Water) SW-846, 7470A SW-846, 8260B (Water) 0704033-04 2156-J-3HS EPA 314.0 SW-846, 30IOA SW-846, 601 oB (Water) SW-846, 7470A SW-846, 8260B (Water) 0704033-05 2157-J-3 EPA 314.0 SW-846, 3010A SW-846, 6010B (Water) ' SW-846, 7470A SW-846, 8260B (Water) 0704033-06 2158-J-4 EPA 314.0 SW-846, 3010A SW-846, 60100 (Water) SW-846, 7470A Volatile Organic Analysis Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis , Volatile Organic Arialysis Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis ^ Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis 04/24/07 4/23/2007 10:30:58 ! Water 04/24/07 4/23/2007 11:27:58 Water Water Water Water Water 04/24/07 4/23/2007 11:27:58 Water Water Water Water Water 04/24/07 4/23/2007 12:35:58 ! Water Water Waler Water Water 04/24/07 4/23/2007 13:15:58 Water Water Water Water Water 04/24/07 4/23/2007 13:55:58 Water Water Water Water Page 2 of 15 Sample Delivery Group: 0704033 Sample No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 0704033-06 2158-J-4 04/24/07 4/23/2007 13:55:58 SW-846, 8260B (Water) Volatile Organic Analysis Water Certified By: W. Scott Fraser, Quality Assurance Officer 05/04/2007 Date This certifies that the following data meets the requirements of the National Environmental Laboratory Accreditation Program (NELAP) unless otherwise annotated: '. Page 3 of 15 Listing of Results by Sample Sample Delivery Group: 0704033 Client Sample 10: 2153-Trip Blank Sample Description: ATK-DLV - Grounciwater Spring 2007 Laboratory Sample ID: 0704033-01 DateSampled: 04/23/07 10:30 Dilution CAS Number : tesfifeOiod: 67-64-1 71-43-2 74-97-5 75-27-4- 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 7S-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95T49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 •106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 •91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 Test Parameter SW-846, 82608 (Water) Volatile Organic ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE . DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE •1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE . 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1.3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE . Result Analysis U U U U U U U U U U U U u u u u u u u u u u u u Ll u u u u u u u u u u u u u u u . u u u u. u u u • u u u u Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ' ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L. ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4, 0.15 0.17 0.25 0.85 EQL Fac 100 1 10 1 10 1 10 1 10 1 10 • 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 .1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 .10- 1 10 1 10 1 .10 1 10 1 .10 1 10 1 10 1 10 1 10 1 tor Analvst LSH LSH LSH LSH . LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH . • LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 •04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 , 04/26/07 04/26/07 04/26/07 • 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 Page 4 of 15 Listing of Results by Sample Sample Delivery Group: 0704033 Client Sample ID: 2153 - Trip Blank Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0704033-01 Date Sampled: 04/23/07 10:30 CASNumber testMeaiod2 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 . 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 ,108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter SW-84IS,826dB'(Water) Volatile Organic TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1 -TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYLCHLORIDE m,p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 TOLUENE-D8 Result Analysis U U u u u u u u u u u u u u u 106 102 102 98.3 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Dilution EQL Factor Analvst 10 10 10 10 10 10 10 . 10 10 10 10 10 10 10 • 10 ••••~~ 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 ' LSH: 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 . LSH 1 LSH 1 LSH 1 LSH 1 • LSH 1 LSH . Test Date 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 • 04/26/07 Client Sample ID: 2154 - J-2 Sample Desdription: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0704033-02 DateSampled: .04/23/07 11:27 CAS Number 2 test Meihod: 014797-73-0 "test Method: Test Parameter Result Units EPA 314.0 Perchlorate - Ion Chromatography PERCHLORATE 203 ug/L SW-846,3010A Metals Digestion MDL Dilution EQL Factor Analvst Test Date KEN 04/30/07 3010A ACID DIGESTION TestMethod: 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 tesf Method: 7439-97-6 TesiMeOiodY 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 SW-846, 60108 (Water) ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC SW-846, 747dA MERCURY SW-846, 8260B (Water) ACETONE BENZENE BROMOCHLOROMETHANE . BROMODICHLOROMETHANE BROMOBENZENE 05/01/2007 12:00 by ICP-6010 U 130 U 38. J U • 218 U U 69.5 ug/L ug/L ug/L ug/L ug/L ug/L ug/L • ug/L ug/L Mercury Analysis Volatile Organic Analysis U ug/L u u u u u ug/L ug/L ug/L ug/L ug/L 20 2 1 10 20 1 1 30 10 0.3 30 0.22 0.31 0.19 0.37 100 10 5 50 100 5 5 150 50 1 100 10 -.: 10 10 10- . 1 1 1 1 1 1 1 1 1 1 1 1 • 1 1 1 1 ••"•-• MTB MTB MTB MTB MTB MTB MTB MTB MTB' MTB TCP • LSH . LSH LSH LSH LSH 05/01/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 04/26/07 04/26/07 04/26/07 04/26/07 ' 04/26/07 04/26/07 Page 5 of 15 Listing of Results by Sample Sample Delivery Group: 0704033 Client Sample ID: 2154 - J-2 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sampfe (D: 0704033-02 DateSampled: 04/23/07 11:27 CAS Number TestMethod:" 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 • 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 -590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100^2-5 630-20-6 79-34-5 127-18-4 108-88-3 67-61-6 120-82-1 71-55-6 Test Parameter Result SW-846,"8260B (Water) Volatile Organic Analysis BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,'3-DICHLOROPROPANE 1,1-DICHLOROPROPENE "y CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2.2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORjDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE U U U U U U U U U U U U U U U U U U u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L og/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 0.42 0.57 1.11 6.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 Dilut [L Fac 10 1 10 1 10 . 1 10 . 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 . 1 10 1 -10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 . • 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 . 1 10 1 10 1 10 1 10 • 1 10 1 10 1 10 1 ion tor Analvst LSH' LSH LSH • LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH • LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 • 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 . 04/26/07 04/26/07 04/26/07 Page 6 of 15 Listing of Results by Sample Sample Delivery Group: 0704033 Client Sample ID: 2154 - J-2 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0704033-02 Date Sampled: 04/23/07 11:27 Dilution CAS Number Test Metiiod: 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 ; 108-67-8 108-05-1 75-01-4 1330-20-7 95-47-6 • 460-00-4 . 1868-53-7 17060-07-0 2037-26-5 Test Parameter . SlV-g46, 8260B (Water) Volatile Organic 1 ;i ,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYLCHLORIDE m,p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 T0LUENE-D8 Result Analysis U U U U u u u u Ll u 107 101 102 100 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 EQL Factor Analvst 10 10 10 •••10 .• 10 10 10 10 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH 1 LSH 1 . LSH 1 LSH 1 LSH LSH Test Date 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 Client Sample ID: 2155-J-2D Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0704033-03 Date Sanipled: 04/23/07 11 ;27 CAS Number [ TesiMeihod2 014797-73-0 TestMethod: Test Parameter EPA314.0~ "" PERCHLORATE SW-846, 3010A 301 OA ACID DIGESTION Test Method: SW-84e, SOIOB (Water) 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 . 7439-96-5 7440-22-4 7440-31-5 7440-66-6, TestMeOiod: 7439-97-6 TestMethod: 67-64-1 71-43-2 . 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC SW-846, 7470A MERCURY Result Perchlorate - Ion Chromatography Metals Digestion 206 05/01/2007 12:00 Metals Analysis by ICP - 6010 1 Mercury Analysis u 115 U 27. J 21. J 155 U U 49. J Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL Dilution EQL Factor Analvst Test Date KEN • 04/30/07 „.. 20 2 ' 1 10 20 1 1 . 30 10 100 10 5 50 100 5 5 150 .50 ... MTB MTB MTB MTB MTB MTB MTB MTB MTB MTB 05/01/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 U ug/L 0.3 TCP 04/26/07 SW-846, 8260B (Water) Volatile Organic Analysis ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE . u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . ug/L 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 100 10 10 . 10 10 • 10 10 10 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 04/26/07 04/26/07 04/26/07 - 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 Page 7 Of 15 Listing of Results by Sample Sample Delivery Group: 0704033 Client Sample ID: 2155-J-2D Sample Oescription: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0704033-03 Date Sampled: 04/23/07 11:27 CAS Number ^'TestMethod: •• 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 Test Parameter SW-846, 8260B (Water) Volatile Organic TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE . DIBROMOMETHANE 1.2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLORpPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-11 IRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE. TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE 1.1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE Result Analysis U U U U U U U u u u u u u u u u u u u u u u u u u u u u u u u u u u. u u u u u u u u u u u u u u u u u Units "•"*"'""•• ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 Dilution EQL Factor Analvst Test Date 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSHj LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 Page 8 of 15 Listing of Results by Sample Sample Delivery Group: 0704033 Client Sample ID: 2155 - J-2D Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0704033-03 Date Sampled: 04/23/07.11:27 Dilution CAS Number TestMeOiod: . 108-67-8 108-05^ 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 . 2037-26-5 Test Parameter SW-846,82608/Water; Volatile 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m,p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 T0LUENE-D8 Result Organic Analysis U U U U U 106 105 106 99.6 Units ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.29 0.13 0.3 1.6 0.18 Ik 10 10 10 10 10 Factor. Analyst LSH LSH- -.LSH LSH LSH LSH LSH LSH LSH Test Date 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 Client Sample ID: 2156-J-3 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: Date Sampled: 0704033-04 04/23/07 12:35 CAS Number : tesi Meiiiod: 014797-73-0 TesfMethod2_ Tesf Mettiod: 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 test Mettiod: 7439-97-6 TesfiiieOiodr 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 Test Parameter Result Units EPA 314.0 Perchlorate - lon Chromatography PERCHLOFIATE < EQL ug/L SW-846, idl OA Metals Digestion MDL EQL Dilution Factor Analvst Test Date KEN 301 OA ACID DIGESTION SW-846, 6i}iOB (Water) Metals Analysis by ICP - 6010 05/01/2007 12:00 MTB ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER : TIN ZINC SW-846, 7470A U 75.7 U U U 1070 U U U ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 20 2 1 10 20 1 1 30 10 100 10 5 50 100 5 5 150 50 MTB MTB MTB MTB MTB MTB MTB MTB MTB Mercury Analysis MERCURY SlV-g4^8260B (^^^^ ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE . BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETFIACHLORIDE CHLOROBENZENE CHLOROETHANE U ug/L 0.3 TCP 04/30/07 05/01/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 04/26/07 Volatile Organic Analysis •u U U u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . ug/L 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 100 10 10 10 10 10 10 10 10 10 10 10 10 - 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 04/26/07 04/26/07 • 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 Page 9 of 15 Listing of Results by Sample Sample Delivery Group: 0704033 Client Sample ID: 2156-J-3 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0704033-04 DateSampled: 04/23/07 12:35 CAS Number rTestMetiiod:[ 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18^ 108-88-3 87-61-6 120-82-1 ^71-55-6 79-00-5 79-01-6 75-69-4 96-18-t 95-63-6 108-67-8 . 108-05-4 75-01-4 1330-20-7 95-47-6 Test Parameter SW-846, 82608 (Water) Volatile Organic 2-CHLOROETHYLVINYL ETHER . CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE IblRACHLOROETHENE TOLUENE 1,2.3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m,p-XYLENE o-XYLENE Result Analysis U U U U U U U U U U U U U U u u u u u. u u u u u u u u u u u- u u u u • M u u u u u u u u u u u u u u u '• u Units ug/L • ug/L ug/L ug/L ug/L ugV ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ,ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L •ug/L ug/L IWIDL 1.71 0.3 0.81 , 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Dilui EQL Fac 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 . 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 ^ 1 10 1 10 1 10 1 10 1 10 . 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 ' 1 10 1 10 1 10 1 10 1 io 1 10 1 10 1 10 1 10 1 10 1 10 1 ion tor Analvst LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date '^ 1 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 * 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 Page 10 of 15 Listing of Results by Sample Sample Delivery Group: 0704033 Client Sample ID: 2156-J-3 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0704033-04 DateSampled: 04/23/07 12:35 CAS Number i TestMethod; 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter SW-846, 82608 (Water) Volatile Organic BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHL0R0ETHANE-D4 TOLUENE-D8 Result Analysis 105 102 101 101 Units % % % % . Dilution MDL EQL Factor Analvst Test Date LSH LSH LSH LSH 04/26/07 04/26/07 04/26/07 04/26/07 Client Sample ID: 2157 - J-3 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID:. 0704033-05 DateSampled: 04/23/07 13:15 CAS Number testMeiiiodr 014797-73-0 r JesflHetiiod: TestMeOiod: 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 Test Method: 7439-97-6 TestMethod: 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 .75-15-0 56-23-5 . 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 Test Parameter 'EPA'fuI """•"' PERCHLORATE 'SW-846,36ldA ~ Result Units Perchlorate - lon Chromatography < EQL ug/L MDL Metals Digestion 3010A ACID DIGESTION SW-846, 60ldB (Water) Metals Analysis by ICP - 6010 05/01/2007 12:00 ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC " SW'-84627~470A "' U 175 . U 52.2 21. J 636 U U 103 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Mercury Analysis MERCURY 'SW-846, 82608 (Water) U ug/L 20 2 1 10 20 1 1 30 10 0.3 Volatile Organic Analysis ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBONTETRACHLORIDE . CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM _ CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE U U U U U U U U U U u u u u u u u u u 'U ug/L ug/L ug/L ug/L ug/L ug/L- ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Dilution EQL Factor Analvst Test Date KEN MTB 04/30/07 .100 10 5 50 100 5 5 150 50 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 100 1 10 1 10 1 10 1 10 1 10 1 10 ,1 10 1 10 1 10. 1 10 1 10 1 . 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 MTB MTB MTB MTB MTB MTB MTB MTB MTB TCP LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/01/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 . 05/02/07 i 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 Page 11 of 15 Listing of Results by Sample Sample Delivery Group: 0704033 Client Sample ID: 2157-J-3 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0704033-05 Date Sampled: 04/23/07 13:15 CAS Number ; tesi liieihod: 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 ';' 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-) 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter "SIV-846,"826dB (Water) ' "Voiatiie Organic DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLbROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-111 RACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1 -TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYLACETATE VINYL CHLORIDE m,p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHL0R0ETHANE-D4 T0LUENE-D8 Result Analysis U U U U U U u u u u u u u u u u u u u u u u u u u u u u u u u u l.J u u u u 4. J u u u u u u u u 106 101 104 100 Units ug/L ug/L ug/L ug/L ug/L ug/L . ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L. ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 .0.15 0.17 0^25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 . 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1-6 0.18 Dilu EQL Fac •-™ "- 10 10 10 10 10 10 10 10 10 10 10 10 10 10 . 10 10 10 10 10 10 10 .10 - 10 10 10 10 10 10 10 1 10 10 10 10 10 10 10 1 10 1 . 10 1 10 1 10 1 10 1 10 1 10 1 10 . 1 10 1 10 1 Uon tor Analvst LSH LSH LSH • LSH LSH • LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH • LSH LSH LSH • LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH . LSH LSH LSH LSH LSH LSH LSH • LSH LSH LSH Test Date ™..™....- 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 - 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 • 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 Page 12 of 15 Listing of Results by Sample Sample Delivery Group: 0704033 Client Sample ID: 2158 - J-4 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0704033-06 DateSampled: 04/23/07 13:55 CAS Number test Metiiod: 014797-73-0 tesfMeOiod:" Test Parameter EPA3U.'0~" ZZ^ PERCHLORATE 'sW846,'3010A~ Result Units Perchlorate - lon Chroriiatography 88.8 ug/L. Metals Digestion MDL TestMeOiod: 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 TestMeOiod:^ 7439-97-6 " teVf'Metfiod: 3010A ACID DIGESTION SW-846, 60108 (Water) ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC JW-_846,7470A f MERCURY SW-M6, 8260S (Wafer) Mercury Analysis U ug/L Volatile Organic Analysis 67-64-1 ACETONE 71-43-2 BENZENE 74-97-5 BROMOCHLOROMETHANE 75-27-4 BROMODICHLOROMETHANE 108-86-1 BROMOBENZENE 75-25-2 BROMOFORM 74-83-9 BROMOMETHANE 78-93-3 2-BUTANONE 104-51-8 N-BUTYLBENZENE 135-98-8 SEC-BUTYLBENZENE 98-06-6 TERT-BUTYLBENZENE 75-15-0 CARBONDISULFIDE 56-23-5 CARBON TETRACHLORIDE 108-90-7 CHLOROBENZENE 75-00-3 CHLOROETHANE 110-75-8 2-CHLpROETHYLVINYL ETHER 67-66-3 CHLOROFORM 74-87-3 CHLOROMETHANE 95-49-8 2-CHLOROTOLUENE 106-43-4 4-CHLOROTOLUENE 124-48-1 DIBROMOCHLOROMETHANE 96-12-8 1,2-DIBROMO-3-CHLOROPROPANE 74-95-3 DIBROMOMETHANE 106-93-4 1,2-DIBROMOETHANE 95-50-1 . 1,2-DICHLOROBENZENE 541-73-1 1,3-DICHLOROBENZENE 106-46-7 1.4-DICHLOROBENZENE 75-71-8 • DICHLORODIFLUOROMETHANE 75-34-3 1,1-DICHLOROETHANE 107t06-2 1,2-DICHLOROETHANE 75-35-4 1,1-DICHLOROETHENE 0.3 Dilution EQL Factor Analvst Test Date 05/01/2007 12:00 ;p-60io U 60.6 U 66.4 33. J 67.4 U U 47. J ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 20 2 1 10 20 1 1 30 10 100 10 5 50 100 5 5 150 50 U u. u U U U U U u u u u u u u u 2.2 J U U U U U U U U u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L - ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 " "• 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 KEN MTB TCP 04/30/07 05/01/07 MTB MTB • MTB MTB MTB MTB MTB MTB MTB 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 04/26/07 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 ' 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 Page 13 of 15 Listing of Results by Sample Sample Delivery Group: ,0704033 Client Sample ID: 2158-J-4 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0704033-06 DateSampled: 04/23/07 13:55 CAS Number Test Parameter testMeiiiod: SW-846, 8260B (Water) Volatile Organic Analysis 156-59-4 CIS-1,2-DICHLOROETHENE 156-60-5 TRANS-1,2-DICHLOROETHENE 78-87-5 1,2-DICHLOROPROPANE 142-28-9 1.3-DICHLOROPROPANE 563-58-6 1,1-DICHLOROPROPENE 10061-01-5 CIS-1,3-DICHLOROPROPENE 10061-02-6 TRANS-1,3-DICHLOROPROPENE 590-20-7 2,2-DICHLOROPROPANE 100-41-4 ETHYLBENZENE 591-78-6 2-HEXANONE 87-68-3 HEXACHLOROBUTADIENE 98-82-8 ISOPROPYLBENZENE 99-87-6 4-ISOPROPYLTOLUENE 75-09-2 METHYLENE CHLORIDE 108-10-1 4-METHYL-2-PENTANONE 91-20-3 NAPHTHALENE 103-65-1 N-PROPYLBENZENE 100-42-5 STYRENE 630-20-6 1,1,1,2-TETRACHLOROETHANE 79-34-5 1,1,2,2-TETRACHLOROETHANE 127-18-4 TETRACHLOROETHENE 108-88-3 TOLUENE 87-61-6 1,2,3-TRICHLOROBENZENE 120-82-1 1,2,4-TRICHLOROBENZENE 71-55-6 1,1,1-TRICHLOROETHANE 79-00-5 1,1,2-TRICHLOROETHANE 79-01-6 TRICHLOROETHENE 75-69-4 TRICHLOROFLUOROMETHANE 96-18-4 1,2,3-TRICHLOROPROPANE 95-63-6 1,2,4-TRIMETHYLBENZENE 108-67-8 1,3,5-TRIMETHYLBENZENE 108-05-4 VINYLACETATE 75-01-4 VINYLCHLORIDE 1330-20-7 m.p-XYLErgE 95-47-6 o-XYLENE 460-00-4 BROMOFLUOROBENZENE . 1868-53-7 DIBROMOFLUOROMETHANE 17060-07-0 1,2-DICHLOROETHANE-D4 2037-26-5 TOLUENE-D8 Result iis 5.3 J U U U U U . .u Ll U U U U U U U Ll U U U u u u u u u u 1.1700 U , • u u u u u u u 106 98.6 102 101 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % • % % % MDL 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 .0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 . 0.29 0.13 0.3 1.6 0.18 Dilu EQL Fac 10 1 10 1 10 1 10 1 10 1 10 1 10' 1 10 . 1 10 ,1 10 1 Id 1 10 . 1 10 1 10 1 10 .1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 . 1 10 , 1 10 1 io 1 10 • 1 10 1 10 1 10 1 10 1 10 • 1 10 1 ion tor Analvst LSH LSH LSH LSH LSH LSH LSH LSH LSH • LSH . LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH -. LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 04/26/07 . 04/26/07 04/26/07 04/26/07 04/26/07 Page 14 of 15 Data Reporting Qualifiers Indicates that the analyte was not detected, or the analyte was detected but was below the MDL. This flag is used when an analyte is found In the blank as well as the sample. Indicates an extimated value. This flag is used either when estimating a concentration for tentatively identified compounds or when the data indicated the presence of a compound that meets the identification criteria but the result is less than the EQL (e.g. 3 J with an EQL of 10). MDL Method Detection Limit: The minimum concentration of a substance that can be confidently measured and reported. The laboratory has demonstrated that the MDL can be achieved in a laboratory reagent blank, but does not guarantee it can be achieved in all sample matrices. EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many analytes the EQL is selected as the value of the lowest standard in the calibration curve. Dilution Dilution Factor: The prepared sample was diluted by this factor because the Factor sample was too concentrated or due to other interferences in the sample matrix. Any dilution factor causes a corresponding increase in the MDL and EQL. Page 15 of 15 ATK Launch Systems Group Environmental Laboratory ^7^Yi^3>3 Client Nanne: I, no cooler Q HamMelivsred, Sample Receipt Ciiecklist SDG No. oio^a-^s Canrror; a Hand delivered, no cooler Carrier Number: _ sample(s) taken out at receiving counter J£B:- Cooler Information: Cooler Number/ID: ^/oU- d iVkAl-U, Condition ol Shipping Containar: Cooler Sealsd (taped): Custody Seals Present. ^QGood QYes QYes Qlntact Coolant: Qlce State of Coolant: QFrozen Thermometer ID: ijl^/ "it-jt/ Reading:^ Packing Description; QFair ^o ^tfjo QBroken QBlue Ice )4None QPanially Frozen 5 -C CF; QNot Applicable QNot Applicable QNot Applicable QDamaged (explain) _ Seal Number: Other: • QMelted Corrected .Temp:_ Temp Blank Included; QYes QNo Ctiain-0(-Custody Information: COC Present: y COC NumberlsV.fc IT. 73 H COC signed (relinquished and received); coc or LWI agrees with sampla labels: Notes;. JrVes ^es QNo QNo QNo Other;. QNot Applicable QNot /Applicable Sample Information: Samples included in coolar: 07^^3 Custody Seals Present; Sample containers intact: Samples in proper containers: Sufficient sample volume; All samples received in hold time; QYes Qlntact ;9Yes pfres jjr-es iXres Water - VOA's have zero headspace; ^re-preserved with HCI: Notes; ' M^ other _ QBroken Seal Number(s) _ QNo Notes; QNo QNo QNo IfVes QNo QNot Applicable QPre-preserved with NajS203; QNon-Preserved; Water - pH acceptable upon receipt: J^es QAdjusted (see comments below) QNot Applicable HNO, s ^ ^ H2SO, = NaOH = ZnAC /NaOH = _HCL = . Water - pH adjusted: (mfg. & Lot No.) HNO3 ^ HjSO,. NajSOjO, Other _ . Notes: _NaOH. _2nAC . -HCL SOP-102Form A 0704033< ENVIRONMENTAL LAB WORK REQUEST TO: THIOKOL ENVIRONMENTAL LABORATORY FROM: Dave Covington ORGANIZATION: Environmental Services EXTENSION: 3898 MAILSTOP: 301 LWR No. E12734 Login No. COST CENTER: 8200 WORKORDER. 988P LS333 GW DATE: 04/23/07 REPORT RESULTS TO: HELEN RAVSTEN, MS 301 SAMPLE INFORMATION SAMPLE 2153 2154 2155 2156 2157 2158 DATE 4-23-07 4-23-07 4-23-07 4-23-07 4-23-07 4-23-07 TYPE G C LOCATION Trip Blank J-2 J-2D J-3HS J-3 J^ TIME 10:30 11:27 11:27 12:35 13:15 13:55 TEST VOA (Method 8260) Perchlorate, Metals, (Method 6010), Voc's (Method 8260) •• • • .; REMARKS |^;i8S:g|Sis,^ CHAIN OF CUSTODY RELINQUISHED BV ^- y> " - DATE r/:^c/~^y TIME ^JSr$~ RECEIVED BY WulkrVk^ DATE /-;?/> ^ ? TIME OfSS^ - FOR LABORATORY USE ONLY 1""™ DATE REPORTED SIGNATURE CERTIFICATE OF ANALYSIS Listing of Sample Information and Testing Requested Friday, June 08, 2007 TESTED FOR: ATK Thiokol: DLV Environmental Monitoring MS301 Thiokol Corp, UT 84322 ANALYZED BY: ATK Thiokol Propulsion Environmental Laboratory P.O. Box 707, M/S 245 Brigham City, UT 84302-0707 435-863-3732 435-863-8080 Contact Name: Project: Sample Delivery Group: Dave Covington Ground Water Testing - DLV 0705034 Page 1 of 14 Sample Delivery Group: 0705034 Sample No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 0705034-01 2200 - H-9 HS 05/18/07 5/17/2007 10:10:05 EPA 314.0 SW-846, 301 OA SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Ctiromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705034-02 2201 - H-9 05/18/07 5/17/2007 10:34:05 EPA 314.0 SW-846, 30IOA SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705034-03 2202-H-10 HS 05/18/07 5/17/2007 11:18:05 EPA 314.0 SW-846, 301 OA SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705034-04 .2203-H-10 05/18/07 5/17/2007 11:44:05 EPA 314.0 SW-846, 301 OA SW-846, 6010B (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - Ion Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0705034-05 2204 - E-3 05/18/07 5/17/2007 14:12:05 EPA 314.0 SW-846, 301 OA SW-846, 6010B (Water) SW-846, 7470A Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Water Water Water Water Page 2 of 14 Sampie Delivery Group: 0705034 Sample No. . Client No. Test Requested Sample Oescription Received Collect Date/Time Matrix 0705034-05 2204 - E-3 SW-846, 8260B (Water) Volatile Organic Analysis 05/18/07 5/17/2007 14:12:05 Water Certified By: W. Scott Fraser, Quality Assurance Officer 06/11/2007 Date This certifies thatthe following data meets the requirements of the National Environmental Laboratory Accreditation Program (NELAP) unless otherwise annotated: Page 3 of 14 Listing of Results by Sample Sample Delivery Group: 0705034 Client Sample ID: 2200 - H-9 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705034-01 Date Sampled: 05/17/07 10:10 CAS Number TestMethod2 . 014797-73-0 Test Mettiod: ^ TestMettiod2 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 i TestMethod:. 7439-97-6 TestMeOiod: 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 ; 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 • 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 Test Parameter EPA 314.0 PERCHLOFtATE SIV.846,30ldA Result Units Perchlorate - lon Chromatography Li ug/L Metals Digestion 3010A ACID DIGESTION SW-846, 60108 (Water) Metals Analysis by ICP - 6010 ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC SIV-846, 7470A 05/19/2007 09:00 ;P-6010 u • 166 U u. 35. J •503 u u 55.4 ug/L ug/L • ug/L ug/L ug/L ug/L ug/L ug/L ug/L MERCURY SW-846, 82608 (Water). Mercury Analysis Volatile Organic Analysis ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE . DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE . 1,1-DICHLOROETHENE U ug/L u u u u u u u u u u u u u u u u u u u u u u u u u u u u . u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Dilution MDL EQL Factor Analvst Test Date 10 0.3 40 10 20 2 1 10 20 1 1 30 10 100 10 • • 5 50 100 5 5 150 50 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 •JMM MTB TCP 06/05/07 05/19/07 MTB MTB MTB MTB MTB MTB MTB MTB MTB 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 • 06/06/07 06/06/07 05/21/07 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH . LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 .05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 • 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 Page 4 of 14 Listing of Results by Sample Sample Delivery Group: 0705034 Client Sample ID: 2200 - H-9 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID; 0705034-01 Date Sampled: 05/17/07 10:10 Dilution CAS Number TestMeOiod: ' 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 . 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 . 103-65-1 100-42-5 • 630-20-6 79-34-5 127-18-4 - 108-88-3 87-61-6 ; 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter Result " SW-846, 8260B (Water) Volatile brganic Analysis CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHL9ROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE . HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1.3,5-TRIMETHYLBENZENE VINYL ACETATE VINYLCHLORIDE m,p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 TOLUENE-D8 U U U U • •: u u u u u u u u u u. u u u u u , u u 0.7 J u u u u u u . u u u u u u • u 107 101 110 98.6 Units ug/L ug/L • ug/L ug/L . ug/L ug/L . ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L :ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . ug/L ug/L ug/L ug/L % .% % % " MDL .0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 . 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0:18 EQL 10 10 10 10 1.0 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 . 10 10 10 10 ,10 10 10 10 10 10 10 Factor Analvst LSH LSH LSH LSH LSH • LSH LSH LSH LSH LSH LSH , LSH •.LSH LSH • LSH LSH LSH LSH LSH LSH LSH LSH, LSH LSH LSH . LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 • 05/30/07 • 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 . . 05/30/07 05/30/07 05/30/07 05/30/07 .05/30/07 •05/30/07 05/30/07 05/30/07 • 05/30/07 05/30/07 05/30/07 05/30/07 Client Sample ID: 2201 - H-9 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705034-02 DateSampled: 05/17/07 10:34 CAS Number TestMeOiod: 014797-73-0 testMeOiod: Test Parameter EPA 314.0 PERCHLORATE SV\/-846,3010A 301 OA ACID DIGESTION Result Units Perchlorate - lon Chromatography U ug/L Metals Digestion 05/19/2007 09:00 MDL Dilution EQL Factor Analvst Test Date 10 40 10 .JMM 06/05/07 • MTB 05/19/07 Page 5 of 14 Listing of Results by Sample Sample Delivery Group: 0705034 Client Sample ID: 2201 - H-9 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705034-02 DateSampled: 05/17/07 10:34 CAS Number i TestMethod: 7440-38-2 7440-39-3 7440-43-9 • 7440-47-3 7439-92-1 . 7439-96-5 •7440-22-4 . 7440-31-5 7440-66-6 test Method: • 7439-97-6 TestMethod: - - . 67-64-1 71-43-2 74-97-5 75-27-4 ' 108-86-1 75-25-2 • 74-83-9 78-93-3 104-51-8. 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-6 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 ,. 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 Test Parameter " SW-846, 6010B (Water) Metals'Ana ARSENIC . BARIUM CADMIUM CHROMIUM LEAD • MANGANESE SILVER TIN ZINC SIV-846, 74704 Mercury An MERCURY SIV.846, 8260S(Wafe;^ 7 Volatile Org ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE • 2'-CHL0R0ETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE . 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE i .2-DICHLOROBENZENE '1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE lil-DICHLOROETHENE • CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE^. 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE Result Units MDL ^^6010 7 U 194 U U 38. J 554 U U 43. J ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 20 2 1. 10 20 1 1 30 10 100. 10 5 50 •100 5 5 150 50 Dilution EQL Factor Analvst Test Date U ug/L u u\ u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . ug/L ug/L ug/L ug/L ug/L ug/L ug/L • ug/L ug/L ug/L ug/L ug/L ug/L 0.3 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 • 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 . 0.24 0.17 0.4 100 10 10 10 10 •10 • 10 10 10 10 10 10 10 10 10 10 • 10 10 10 10 10 10 10 10 10 10 • 10 10 ... • 10 10 10 10 10 10 10 10 10 MTB MTB MTB MTB MTB MTB MTB MTB MTB 06/06/07 06/06/07 . 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 TCP 05/21/07 LSH , LSH LSH LSH LSH LSH LSH ^ LSH LSH. LSH LSH LSH LSH LSH' LSH •• LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH . LSH LSH. LSH LSH 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 • 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 • 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07. 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 Page 6 of 14 Listing of Results by Sample Sample Delivery Group: 0705034 Client Sample ID: 2201 - H-9 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705034-02 Date Sampled: 05/17/07 10:34 Diluti CAS Number ; test Metfiod; 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 • 96-18-4 95-63-6 108-67-8 . 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 .1868-53-7 17060-07-0 2037-26-5 Test Parameter SIV-846, 82608 (Water) Volatile Organic Analy TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE . VINYL ACETATE VINYL CHLORIDE m.p-XYLENE O-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHL0R0ETHANE-D4 TOLUENE-D8 Result sis U U u u u u u u u u u u u u u l.J u u u u u u u u u u u u u 110 100 114 99.5 Units ug/L ug/L ug/L ug/L ug/L ug/L . ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 EQL Fac 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 .•• 10 1 10 1 10 . 1 10 1 ' 10 1 10 1 10 1 10 1 10 • 1 tor Analvst ••^•.- • ••™- LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH • LSH LSH • LSH LSH LSH LSH LSH LSH LSH Test Date 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 . 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 . •• 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 • -05/30/07 05/30/07 . 05/30/07 05/30/07 05/30/07 Client Sample ID; 2202-H-10 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705034-03 DateSampled: 05/17/07 11:18 CAS Number : Tesf Method: 014797-73-0 '' TestMeOiod: TestMeOiod: 7440-38-2 7440-39-3 7440-43-9 7440-47-3 Test Parameter EPA 314.0 PERCHLORATE SW.846, 3010A 3010A ACID DIGESTION SIV-846, 6010B (Water) ARSENIC BARIUM CADMIUM CHROMIUM Result Perchlorate - lonChromatography U Metals Digestion • 05/19/2007 09:00 Metals Analysis by ICP-6010 . U 308 U U Units ug/L ug/L ug/L ug/L ug/L MDL 10 Dilution EQL Factor Analvst Test Date 40 10 JMM MTB 06/05/07 05/19/07 400- 40 20 200 2000 200 100 1000 20 20 20 20 MTB MTB MTB MTB 06/06/07 06/06/07 06/06/07 06/06/07 .Page 7 Of 14 Listing of Results by Sample Sample Delivery Group: 0705034 Client Sample ID: 2202 - H-10 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705034-03 Date Sampled: 05/1.7/07 11:18 CAS Number Test Metiiod: 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 Test Method; 7439-97-6 TesfMettiod: 67-64-1 71-43-2 74-97-5 • 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8. 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 ••' 67-66-3 • 74-87:3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 • 95-50-1 541-73-1 106-46-7 75-71-8 75:34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 • 100-41-4 591-78-6 Test Parameter SW-846, 6010B^ater) LEAD MANGANESE SILVER TIN ZINC SW-846, 74TVA MERCURY SW-846, 82608 (Water) Result Units Meials Analysis by ICP - 6016 Dilution MDL EQL Factor Analvst Test Date Mercury Analysis Volatile Organic Analysis ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVlNYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-piCHLOROETHENE 1 .^-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1; 1 -DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBEf^ZENE 2-HEXANONE U 435 U U U ug/L ug/L ug/L ug/L ug/L U ug/L 400 20 20 600 200 2000 100 100 3000 1000 • 20 20 20 20 20 MTB MTB MTB MTB MTB 06/06/07 ; 06/06/07 06/06/07 06/06/07 06/06/07 0.3 u u u u u u u u u u u. u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 30 0.22 0.31 0.19 0.37 • 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 • 0.81 0.24 0,15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17. 0.4 0.18 0.9 0.16 0.7 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 TCP 05/21/07 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH . LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH • LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 .05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 : 05/30/07 • 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 .05/30/07 05/30/07 Page 8 of 14 Listing of Results by Sample Sample Delivery Group: 0705034 Client Sample ID: 2202-H-10 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705034-03 DateSampled: 05/17/07 11:18 CAS Number Test Parameter Result test Mettiod: SW-846, 82608 (Water) "" Voiatile Organic Analysis 87-68-3 HEXACHLOROBUTADIENE 98-82-8 ISOPROPYLBENZENE 99-87-6 4-ISOPROPYLTOLUENE 75-09-2 METHYLENE CHLORIDE 108-10-1 4-METHYL-2-PENTANONE 91-20-3 NAPHTHALENE 103-65-1 N-PROPYLBENZENE 100-42-5 STYRENE 630-20-6 1,1,1,2-TETRACHLOROETHANE 79-34-5 1,1,2,2-TETRACHLOROETHANE 127-18-4 TETRACHLOROETHENE 108-88-3 TOLUENE 87-61-6 1,2,3-TRICHLOROBENZENE .120-82-1 1,2,4-TRICHLOROBENZENE 71-55-6 1,1.1-TRICHLOROETHANE 79-00-5 1,1,2-TRICHLOROETHANE 79-01-6 , TRICHLOROETHENE 75-69-4 TRICHLOROFLUOROMETHANE 96-18-4 1,2,3-TRICHLOROPROPANE 95-63-6 1,2,4-TRIMETHYLBENZENE 108-67-8 1,3,5.-TRlMETHYLBENZENE 108-05-4 VINYLACETATE 75-01-4 VINYLCHLORIDE 1330-20-7 m.p-XYLENE 95-47-6 o-XYLENE 460-00-4 BROMOFLUOROBENZENE 1868-53-7 DIBROMOFLUOROMETHANE 17060-07-0 1,2-DICHLOROETHANE-D4 2037-26-5 TOLUENE-D8 Units sis U U U U U, u u u u u u . 2.4 J U U ; u u u u u u u u u u u 108 99.7 109 100 ug/L ug/L ug/L ug/L • ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % • % % % MDL 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16' 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Dilution EQL Factor Analvst Test Date 10 10 10 . 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 1.0 10 10 10 10 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH • LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH • 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 . 05/30/07 05/30/07 05/30/07 • 05/30/07 05/30/07 05/30/07 05/30/07 • 05/30/07 05/30/07 . 05/30/07 05/30/07 05/30/07 . 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 Client Sample ID: 2203-H-10 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705034-04 Date Sampled: 05/17/07 11:44 CAS Number TestMeOiod: 014797-73-0 TestMeOiod: TestMeOiod: 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 Test Parameter EPA314.0 • Perchlorate - lon PERCHLORATE SW-846, 3010A Metals Digestion 3010A ACID DIGESTION SW-846, 60108 (Water) Metals Analysis ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN Result Chromatography U 05/19/2007 09:00 jy ICP-6010 U 313 U U U 475 U U Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 10 Dilution EQL Factor Analvst Test Date 40 10 JMM 06/05/07 400. 40 20 200 400 20 20 600 2000 200 100 1000 2000 100 100 3000. 1 20 20 20 20 20 20 20 20 MTB • MTB MTB MTB MTB MTB MTB MTB MTB • 05/19/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 Page 9 of 14 Listing of Results by Sample Sample Delivery Group: 0705034 Client Sample ID: 2203 - H-10 Sarnple Description; ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705034-04 Date Sampled; 05/17/07 11:44 CAS Number Tesf Method: 7440-66-6 TestMethod: 7439-97-6 TestMethod: 67-64-1 71-43-2 74-97-5 75-27^ 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 • 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 •106-43-4 124-48-1 96-12-8 ' 74-95-3 106-93-4 95-50-V 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 • 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 ' 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 Test Parameter "SW-846, eoiOB (Water) ZINC Sm46,74'70A Result Units Metals Analysis by ICP - 6010 U ug/L Mercury Analysis Dilution MDL EQL Factor Analvst Test Date MERCURY SW-846, 8260S (Water) Volatile Organic Analysis ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBONTETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-blBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPRpPENE .TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-lSOPROPYLTOLUENE METHYLENE CHLORIDE U ug/L u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u. u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 200 • 1000 20 MTB 06/06/07 0.3 30 0.22 0.31 0.19 0.37 0.42 • 0.57 , 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 . 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 1 1 100 1 1 10 1 10 'l 10 1 10 1 10 1 10 • 1 10 1 10 10. 10 10 10 10 1 10 10 10 10. 10 . 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 TCP LSH ' LSH LSH . LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH. LSH LSH t LSH 1 LSH LSH LSH 1 LSH' 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH . 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH • 1 • LSH 1 LSH 1 LSH 1 LSH 1 LSH 05/21/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 . 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 Page 10 of 14 Listing of Results by Sample Sample Delivery Group: 0705034 Client Sample ID: . 2203 - H-10 Sample Description; ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705034-04 Date Sampled: 05/17/07 11:44 CASNumber tesiMeOioiir - 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter SW-846, 8260B (Water) Volatile 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE , 1,2,4-TRICHLOROBENZENE 1,1,1 -TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYLACETATE VINYL CHLORIDE m.p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 T0LUENE-D8 Result Units u u u u u u u 2.1 J U U U u u u u u u u u u u 109 100 109 99.8 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Dilution EQL Factor Analvst Test Date 10 10 10 10 10 10 10 10 io 10 10 IO- IO- IO 10 10 10 10 10 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 ' 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 Client Sample ID: 2204 - E-3 Sample Description; ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID; 0705034-05 DateSampled: 05/17/07 14:12 Dilution CAS Number TestMeOiod: 014797-73-0 JesfMetiiod: TestMethod: 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 TestMeOiod: 7439-97-6 Test Parameter EPA 314.0 PERCHLORATE SW-846, 30tO/l 301 OA ACID DIGESTION SW-846, 60108 (Water) ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC SW-846, 7470A MERCURY Result Perchlorate - lon Chromatography Metals Digestion Metals Analysis by Mercury Analysis "l 113 05/12/2007 09:00 ICP-6010 U 89.7 J • U. 962. J U 265 U U U U Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 1 400 40 20 200 400 20 20 600 200 0.3 EQL • 4 2000 200 100 1000 2000 100 100 3000 1000 1 Factor Analyst 1 1 20 20. 20 20 20 20 20 20 20 1 JMM MTB MTB MTB MTB MTB MTB MTB MTB . MTB MTB TCP ' Test Date 06/05/07 05/12/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 06/06/07 . 06/06/07 05/21/07 Pageii of 14 Listing of Results by Sample Sample Delivery Group: 0705034 Client Sample ID: 2204 - E-3 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0705034-05 DateSampled; 05/17/07 14:12 CAS Number Test Parameter tesfMettiod: SW-846, 82608 (Water) Volatile Organic 67-64-1 ACETONE 71-43-2 BENZENE . 74-97-5 BROMOCHLOROMETHANE . 75-27-4 BROMODICHLOROMETHANE 108-86-1 BROMOBENZENE 75-25-2 BROMOFORM 74-83-9 BROMOMETHANE 78-93-3 2-BUTANONE 104-51-8 N-BUTYLBENZENE 135-98-8 SEC-BUTYLBENZENE 98-06-6 TERT-BUTYLBENZENE 75-15-0 CARBON DISULFIDE 56-23-5 CARBONTETRACHLORIDE 108-90-7 CHLOROBENZENE 75-00-3 CHLOROETHANE 110-75-8 2-CHLOROETHYLVINYL ETHER 67-66-3 CHLOROFORM 74-87-3 CHLOROMETHANE • 95-49-8 2-CHLOROTOLUENE 106-43-4 4-CHLOROTOLUENE 124-48-1 DIBROMOCHLOROMETHANE . 96-12-8 1,2-DIBROMO-3-CHLOROPROPANE 74-95-3 DIBROMOMETHANE 106-93-4 1,2-DIBROMOETHANE 95-50-1 1,2-DICHLOROBENZENE 541-73-1 1,3-DICHLOROBENZENE 106-46-7 1,4-DICHLOROBENZENE 75-71-8 DICHLORODIFLUOROMETHANE 75-34-3 1,1-DICHLOROETHANE 107-06-2 1,2-DICHLOROETHANE 75-35-4 1,1-DICHLOROETHENE 156-59-4 CIS-1,2-DICHLOROETHENE 156-60-5 TRANS-1,2-DICHLOROETHENE 78-87-5 1,2-DICHLOROPROPANE 142-28-9 1,3-DICHLOROPROPANE 563-58-6 1,1-DICHLOROPROPENE 10061-01-5 CIS-1,3-DICHLOROPROPENE 10061-02-6 TRANS-1,3-DICHLOROPROPENE 590-20-7 2,2-DICHLOROPROPANE 100-41-4 ETHYLBENZENE 591-78-6 2-HEXANONE 87-68-3 HEXACHLOROBUTADIENE. 98-82-8 ISOPROPYLBENZENE 99-87-6 4-ISOPROPYLTOLUENE 75-09-2 METHYLENECHLORIDE 108-10-1 4-METHYL-2-PENTANONE 91-20-3 NAPHTHALENE 103-65-1 N-PROPYLBENZENE 100-42-5 STYRENE 630-20-6 1,1.1,2-TETRACHLOROETHANE 7 79-34-5 1,1,2,2-TETRACHLOROETHANE Result Analysis U U U U U U U U U U U U U U U U 12.9 U U U U U U U U U U U U u 6.6 J U U U . U U •U U U U U u u u u u u u u . u u Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Dilution MDL EQL Factor Analvst Test Date 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 100 10 10 10 • 10 10 10 10 10 10 .10 10 10" 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10. 10 10 10 10 10 10 10 10 10. 10 10 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH • LSH LSH' LSH LSH LSH LSH LSH LSH LSH • LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH . LSH . LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH • LSH 05/30/07 05/30/07 • 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 • 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 .05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 • 05/30/07 05/30/07 05/30/07 05/30/07 . 05/30/07 05/30/07 05/30/07 05/30/07 • 05/30/07 05/30/07 05/30/07 05/30/07 . 05/30/07 ' 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 Page 12 of 14 . Listing of Results by Sample Sample Delivery Group: 0705034 Client Sample ID: 2204 - E-3 Sample Oescription: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID; 0705034-05 Date Sampled: 05/17/07 14:12 CAS Number Test Parameter Result test MethorJ; SW-846, 8260B (Water) Volatile Organic Analysis 127-18-4 TETRACHLOROETHENE 108-88-3 TOLUENE 87-61-6 1,2,3-TRICHLOROBENZENE 120-82-1 1,2,4-TRICHLORdBENZENE 71:55-6 1,1,1-TRICHLOROETHANE .79-00-5 1,1,2-TRICHLOROETHANE 79-01-6 TRICHLOROETHENE 75-69-4 TRICHLOROFLUOROMETHANE 96-18-4 1,2,3-TRICHLOROPROPANE . 95-63-6 1,2,4-TRIMETHYLBENZENE 108-67-8 1,3,5-TRIMETHYLBENZENE 108-05-4 VINYLACETATE 75-01-4 VINYLCHLORIDE 1330-20-7 m,p-XYLENE 95-47-6 • o-XYLENE 460-00-4 BROMOFLUOROBENZENE 1868-53-7 DIBROMOFLUOROMETHANE 17060-07-0 1,2-DICI-ILPR0ETHANE-D4 2037-26-5 TOLUENE-D8 Units sis U U U u 4.8 J u 63.8 U U U U U U . U U 110 102 109 97.0 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL Dilution EQL Factor Analvst Test Date 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25> 0.33 0.19 0.29 0.13 0.3 1.6 0.18 10 10 10 10 10 10 10 •10 10 10 10 10 10 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 05/30/07 Page 13 of 14 Data Reporting Qualifiers U Indicates that the analyte was not detected, or the analyte was detected but was beiow the MDL. B This flag is used when an anaiyte is found in the blanl< as well as the sample. Indicates an extimated value. This flag is used either when estimating a concentration for tentatively identified compounds or when the data indicated the presence of a compound that meets the identification criteria but the result is iess than the EQL (e.g. 3 J with an EQL of 10). MDL Method Detection Limit: The minimum concentration of a substance that can be confidently measured and reported. The laboratory has demonstrated that the MDL can be achieved in a laboratory reagent blank, but does not guarantee it cari be achieved in all sample matrices. EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many analytes the EQL is selected as the value of the lowest standard in the calibration curve. Dilution Dilution Factor: The prepared sample was diluted by this factor because the Factor sample was too concentrated or due to other interferences in the sample matrix. Any dilution factor causes a corresponding increase in the MDL and EQL. Page Uof 14 ATK Launch Systems Group Environmental Laboratory • Sample Receipt Checklist daliv 0 7(7^ P^ / Client Name:J SDG No.. 07c>S/^^^ Carrier: Q Hand delivered, no cooler Carrier Number:. Q Hand delivered, sample(s) taken out at receiving counter MA. Cooler Information: Cooler Numt>er/ID: ^^^ LOUAJ^ Condition of Shipping Container; Cooler Sealed (taped); Custody Seals Present: Coolant; State of Coolant: Thermometer ID; QYes QYes Qlntact Qlce QFair ^0 QFrozen ll^artia V^/?g(^Readino y ( QNot Applicable ONot Applicable QNot /applicable QBroken . QBlue Ice j^ona artlally Frozen C CF;_ QDamaged (explain). Seal Number; _ Other; QMelted Corrected Temp;. _°C . Temp Blank Included: QYes QNo Packing Description; Chaln-Of-Custody Information: COC Present; <» w^ 7<r'l J<^®^ COC NumberlsV ^ I*' /«• / COC signed (relinquished and received); Ares COC or LWI agrees with sample labels; Jfbes QNo QNo QNo Other; QNot /Vpplicable QNot /Applicable Notes. Sample Information: Samples included in cooler: (PlPSOJc/ '". . • Custody Seals Present; Sample containers intact; Samples in proper containers; Sufficient sample volume; All samples received in hold time; QYes Qlntact ^es jf'es >(5'es ^es ^° QBroken QNo QNo QNo QNo Water - VOA's have zero headspace:. Jlf re-presewed with HCI: Notes; Other; Seal Numl>er(s) _ Notes; • X<e'. QPre-presen/ed vaith NazSjOj; QNo . QNot Applicable QNon-Preserved; Water - pH acceptable upon receipt: pftas QAdjusted (see comments below) QNot Applicable HNOi = ^ C^ HjSO, = __, NaOH = ZnAC /NaOH = _HCL =, Water - pH adjusted: (mfg. & Lot No.) HNOs • ' HjSO,. NajSOiOj : Other _ Notes; _NaOH. _ZnAC . _HCL SOP-102Form A 0705034 ENVIRONMENTAL LAB WORK REQUEST TO TfflOKOL E^fVIRONMENTAL LABORATORY FROM: Dave Covington , ORGANIZATION: Environmental Services EXTENSION: 3898 MAILSTOP: 301 LWRNO.E12751 Logiii No. , COST CENTER: 8200 WORK ORDER: 988P LS333 GW DATE; 05/17/07 REPORT RESLILTS TO: HELEN RAVSTEN, MS 301 SAMPLE INFORMATION SAMPLE 2200 2201 2202 2203 2204 DATE 5-17-07 5-17-07 5-17-07 5-17-07 5-17-07 .. .. TYPE G C LOCATION H-9 HS H-9 H-10 HS H-10 E-3 TIME 10:10 10:34 11:18 11:44 14:12 TEST Perchlorate, Metals, (Method 6010), Voc's (Method 8260) Perchlorate, Metals, (Method 6010), Voc's (Method 8260) REMARKS |g;ian:kg',Xisn, Pikivkisr, • CHAIN OF CUSTODY . »_RELIINQlJJSHEn.BY / y-Xr- y DATE ^yJ'^7 TIME ^f.vr RECEIVED BY yfl;^;t^ DATE . ^-i(.-oy TIME O^r - FOR LABORATORY USE ONLY DATE COMPLETED , DATE REPORTED SIGNATtlRE • . •. CERTIFICATE OF ANALYSIS Listing of Sample Information and Testing Requested Friday, May 04, 2007 TESTED FOR: ATK Thiokol: DLV Environmental Monitoring MS 301 Thiokol Corp, UT 84322 ANALYZED BY: ATK Thiokol Propulsion Environmental Laboratory P.O. Box 707, M/S 245 Brigham City, UT 84302-0707 435-863-3732 435-863-8080 Contact Name: Project: Sample Delivery Group: Dave Covington Ground Water Testing - DLV 0704036 Page 1 of 13 Sample Delivery Group: 0704036 Sample No. Client No. Test Requested EPA 314.0 SW-846, 301 OA SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) Sample Description Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Received Collect Date/Time Matrix 0704036-01 ' 2159-Trip Blank SW-846, 8260B (Water) 0704036-02 .2160-J-1 HS Volatile Organic Analysis 04/25/07 4/24/2007 10:30:15 Water 04/25/07 4/24/2007 11:15:15 Water Water Water Water Water 0704036-03 2161-J-1 04/25/07 4/24/2007 11:56:15 EPA 314.0 SW-846, 301 OA SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 MerciJry Analysis Volatile Organic Analysis Water Water Water Water Water 0704036-04 2162-J-7 HS 04/25/07 4/24/2007 13:35:15 EPA 314.0 SW-846, 30IOA SW-846, 601 OB (Water) SW-846, 7470A SW-846, 8260B (Water) Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP - 6010 Mercury Analysis Volatile Organic Analysis Water Water Water Water Water 0704036-05 2163-J-7 04/25/07 4/24/2007 14:21:15 EPA 314.0 SW-846, 301 OA SW-846, 6010B (Water) SW-846, 7470A Perchlorate - lon Chromatography Metals Digestion Metals Analysis by ICP- 6010 Mercury Analysis Water Water Water Water Page 2 of 13 Sample Delivery Group: 0704036 Sampie No. Client No. Test Requested Sample Description Received Collect Date/Time Matrix 0704036-05 2163-J-7 04/25/07 4/24/2007 14:21:15 SW-846, 8260B (Water) Volatile Organic Analysis Water Certified By: W. Scott Fraser, Quality Assurance Officer 05/04/2007 Date This certifies that the following data meets therequirements of the National Environmental Laboratory Accreditation Program (NELAP) unless otherwise annotated: Page 3 of 13 Listing of Results by Sample Sample Delivery Group: 0704036 Client Sample ID: 2159 - Trip Blank Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0704036-01 Date Sampted; 04/24/07 10:30 CAS Number i Test Metiiod: f_ 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43^ 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 .91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 Test Parameter SW-846, S26dB~(Wafer) Volatile Organic ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON 1 b 1 HACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-OIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1 ;4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENECHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE Result Analysis U U U U U U U U U LJ U U U U U U U U u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL iSk Diluti Fad 30 0.22 0.31 0.19 0.37 0.42 . 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 • 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 or Analvst Test Date -•• LSH LSH LSH LSH LSH •LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH \LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH \ 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 . 05/01/07 05/01/07 05/01/07 . 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 Page 4 of 13 Listing of Results by Sample Sample Delivery Group: 0704036 Client Sample ID: 2159-Trip Blank Sample Description; ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0704036-01 DateSampled; 04/24/07 10:30 Dilution CAS Number ^ TestMeOiod: 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter SWJ46, 8260B(Water)_ Volatile Org TETRACHLOROETHENE TOLUENE 1 ;2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1.-TRICHL0R0ETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1.3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m,p-XYLENE O-XYLENE BROMOFLUOROBENZENE . DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 TOLUENE-D8 Result anic Analysis U U U U U U U U U U U U U U U 105 100 103 100 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % ' % MDL 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 . 1.6 0.18 EQL Factor Analvst 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 . LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH Test Date • ••""1 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 Client Sample ID; 2160 - J-1 HS Sample Description; ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID; 0704036-02 DateSampled; 04/24/07 11:15 CAS Number ; TestMeOiod: 014797-73-0 TestMettiodT Test Parameter EPfi^14.0f_ PERCHLORATE SIV-846, iOlM Result Units Perctilorate - lon Ctiromatography 1490 Metals Digestion MDL Dilution EQL Factor Analvst Test Date ug/L 20 3010A ACID DIGESTION • 05/01/2007 12:00 KEN MTB 04/30/07 05/01/07 rest Method: 7440-38-2 7440-39-3 7440-43-9 7440^7-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 . 7440-66-6 test Method: 7439-97-6 TestMethod: 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 SW-846, 60108 (Water) ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC Z,^*S,7470A f MERCURY JSW-M6,82MB(Watef)'^ ACETONE BENZENE Metals Analysis by ICP-6010 U 81.5 U 12. J U 93.7 U U 26. J Mercury Analysis U Volatile Organic Analysis U U BROMOCHLOROMETHANE U BROMODICHLOROMETHANE U BROMOBENZENE U ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L. Z:.:..:ZZ ug/L zzzzz ug/L ug/L ug/L ug/L ug/L 20 2 1 10. 20 1 1 30 10 ZZZ 0.3 zzzzzzz^ 30 0.22 0.31 0.19 0.37 100 10 5 50 100 5 5 150 50 1 zzzz 100 10 10 10 10 • 1 1 1 1 1 1 1 1 1 1 Z.ZZ.:. 1 1 1 1 1 MTB MTB MTB MTB MTB MTB MTB MTB MTB _:;; :i::: TCP LSH LSH LSH LSH LSH 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 04/26/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 Page 5 of 13 Listing of Results by Sample Sample Delivery Group: 0704036 Client Sample ID; 2160 - J-1 HS Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0704036-02 Date Sampled: 04/24/07 11:15 CAS Number • Te'sfMeiiiiJd:" Test Parameter Result Units MDL SIV-846, 8260S (Water; Volatile Organic Analysis 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 • 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTAN0NE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHAN E 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1 -TRICHLOROETH ANE u u u u u u u u u u u u u u u u u u u u u u u u u 43.2 u U u u u u u u u u u u u u u u u u u u u u u u 22.1 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 Dilu |L Fac 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 . 1 10 ' 1 10 1 10 10 10 1 10 1 10 1 10 • 1 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 lon tor Analvst — LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH' LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 .05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 • 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 Page 6 of 13 Listing of Results by Sample Sample Delivery Group: 0704036 Client Sample ID; 2160 - J-1 HS Sample Description; ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID; 0704036-02 DateSampled: 04/24/07 11:15 CAS Number r'TestMethodf"- 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 . 17060-07-0 2037-26-5 Test Parameter Result SiV-846, 82608 (Water) Volatile Organic Analysis 1,1,2-TRICHLOROETHANE U TRICHLOROETHENE 456 TRICHLOROFLUOROMETHANE U 1,2,3-TRICHLOROPROPANE U 1,2,4-TRIMETHYLBENZENE U 1,3,5-TRIMETHYLBENZENE U VINYL ACETATE U VINYL CHLORIDE U m,p-XYLENE. U . o-XYLENE U BROMOFLUOROBENZENE 103 DIBROMOFLUOROMETHANE 102 1,2-DICHLOROETHANE-D4 103 T0LUENE-D8 99.9 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 EQL ' 10 10 10 10 10 10 10 10 10 10 ' Dilution Factor Analvst LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Date ^! 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 .05/01/07 05/01/07 05/01/07 Client Sample ID; 2161 -J-1 Sample Description; ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID; 0704036-03 Date Sampled; 04/24/07 11:56 CAS Number '"tesiMeOio'd:' 014797-73-0 : TestMethod: Test Parameter wniio ~~' Result Units Perchlorate - lon Chromatography MDL PERCHLORATE SW-846, 30ldA 3010A ACID DIGESTION 1460 ug/L EQL 20 Dilution Factor Analvst Test Date KEN 04/30/07 Metals Digestion 05/01/2007 12:00 MTB 05/01/07 Test Mettiod: SW-846, 60108 (Water) Metals Analysis by ICP - 6010 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 TesfMettiod: 7439-97-6 tesf Method: ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC "SW-84627470A ' MERCURY SiW-846, 82608 (Wafer) u 71.7 U 13. J U 49.2 U U 23. J ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Mercury Analysis U ug/L Volatile Organic Analysis 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE U u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 20 2 1 10 , 20 1 1 30 10 0.3 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 100 10 5 50 100 5 5 150 50 1 100 10 10 10 10 10 10 . 10 10 10 1 1 1 1 1 1 1 1 1 1 ' 1 1 1 1 1 1 1 1 1 1 MTB MTB MTB MTB MTB MTB MTB MTB MTB TCP LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 04/26/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 Page 7 of 13 Listing of Results by Sample Sample Delivery Group: 0704036 Client Sample ID; 2161 -J-1 Sample Description; ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID; 0704036-03 Date Sampled; 04/24/07 11:56 CAS Number Test Parameter Result Units MDL EQL Dilut Fad Test Mettiod: 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35^ 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41^ 591-78-6 87-68-3 98-82-8 99-87-6 . 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 ' 79-34-5 127-18^ 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 SW-S46, 82608 (Water) Volatile Organic f TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DlCHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE I'l-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENECHLORIDE 4-METHYL-2-PENTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE U U . U u u u u u u u u u u u u u u u u u 46.1 U U u u u •u u u u u u u u u u u u u u u u u u u 23.3 U 426 U U U ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 10 10 10 10 10 10 10. 10 10 . 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 Ion or Analvst Test Date LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH l^SH LSH LSH Page 8 of 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 ,05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 13 Listing of Results by Sample Saniple Delivery Group: 0704036 Client Sample ID; 2161 .J-l Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0704036-03 Date Sampled: 04/24/07 11:56 CAS Number : TestMeiiiod: 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 460-00^ 1868-53-7 17060-07-0 2037-26-5 Test Parameter SW-84iS, 82608 (Water) Volatiie Organic 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m.p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 TOLUENE-D8 Result Analysis U U U U U 106 101 102 100 Units ug/L ug/L ug/L ug/L ug/L % % % % MDL 0.29 0.13 0.3 1.6 0.18 Dilution EQL Factor Analvst Test Date 10 10 10 10 10 - LSH LSH LSH LSH LSH LSH LSH LSH LSH - • ; 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 Client Sample ID; 2162 - J-7 HS Sample Description; ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID; 0704036-04 Date Sampled; 04/24/07 13:35 CAS Number rest Method: 014797-73-0 tesfMe0iod2 Tesi'Mefiio'd: 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 TestMeOiod: 7439-97-6 '"'Tesi'Me'tho'dr 67-64-1 71-43-2 74-97-5 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 Test Parameter EPA 314.0 "f PERCHLORATE JW-846^010Af _ 3010A ACID DIGESTION ~siV^846r60i'0fl (Wate^ ARSENIC BARIUM CADMIUM CHROMIUM LEAD MANGANESE SILVER TIN ZINC -SW^846,747M Result Units Perchlorate - lon Chromatography 593 ug/L Metals Digestion MDL Dilution EQL Factoi^ Analvst Test Date 20 KEN 04/30/07 05/01/2007 12:00 ;P-6010 U 70 U 15. J U 121 U U 21. J ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MTB 05/01/07 MERCURY S^V-846^8260fl7lVate^) Mercury Analysis Volatile Organic Analysis 20 2 1 10 20 1 1 30 10 100 10 5 -, 50 100 5 5 150 50 MTB MTB MTB MTB MTB . MTB MTB MTB MTB 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 U ug/L 0.3 TCP 04/26/07 ACETONE BENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOBENZENE BROMOFORM BROMOMETHANE 2-BUTANONE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE u u u u u u u u u u u u u u u ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 30 0.22 ' 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 100 10 10 10 10 10 10 10 10 TO 10 10 10 10 10 LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 Page 9 of 13 Listing of Results by Sample Sample Delivery Group: 0704036 Client Sample ID: 2162 - J-7 HS Sample Description; ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID; 0704036-04 DateSampled; 04/24/07 13:35 CAS Number ; tesiyeOiod2 ' 110-75-8 67-66-3 74-87-3 95-49-8 106-43-4 124-48-1 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 108-05-4 75-01-4 1330-20-7 95-47-6 Test Parameter SW-8462ii26dB(Water)' '""voiatilebrganic 2-CHLOROETHYLVINYL ETHER CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PENTANONE • NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1.2.2-TETRACHLOROETHANE TETRACHLOROETHENE . TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE VINYL ACETATE VINYL CHLORIDE m,p-XYLENE O-XYLENE Result Analysis U U U U U U U U U U U U U U U U U U U U U U U U U u u u u u u u u u u u u u u u u u 24.7 U U U u u u u u Units ....... ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . ug/L ug/L ug/L ug/L ug/L' ug/L ug/L ug/L ug/L ug/L MDL 1.71 0.3 0.81 0.24 0.15 0.18 0.35 0.25 0!l5 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 0.15 0.17 0.25 • 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Dilu EQL Fac 10 1 10 1 10 1 10 1 10 1 10 . 1 10 1 . 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 lon tor Analvst LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH. LSH LSH LSH LSH LSH . LSH LSH : LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH . LSH LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH 1 LSH Test Date 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 . 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 Page 10 of 13 Listing of Results by Sample Sample Delivery Group: 0704036 . Client Sample ID; 2162-J-7 HS Sample Description; ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID; 0704036-04 DateSampled: 04/24/07 13:35 CAS Number Test Parameter Result • • Test MeOiod: SW-846, 82608 (Water) Volatile"" On .. 460-00-4 BROMOFLUOROBENZENE 1868-53-7 DIBROMOFLUOROMETHANE 17060-07-0 1,2-DICHLOROETHANE-D4 2037-26-5 TOLUENE-D8 Units MDL Dilution EQL Factor Analvst Test Date Analysis 107 103 104 99.0 ... . % % % % ... 1 1 1 1 •••• LSH LSH LSH LSH - - ' 05/01/07 05/01/07 05/01/07 05/01/07 Client Sample ID: 2163 - J-7 Sample Description: ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0704036-05 Date Sampled; 04/24/07 14:21 Dilution CAS Number '"Test iliiettiod:~'' 014797-73-0 ; 'tesfMeihod: \ TestMeOiod: 7440-38-2 7440-39-3 7440-43-9 7440-47-3 7439-92-1 7439-96-5 7440-22-4 7440-31-5 7440-66-6 Test Mettiod: 7439-97-6 \"TestMeOiod2 67-64-1 71-43-2 74-97-5 • 75-27-4 108-86-1 75-25-2 74-83-9 78-93-3 104-51-8 135-98-8 " 98-06-6 75-15-0 56-23-5 108-90-7 75-00-3 110-75-8 • 67-66-3 74-87-3 95-49-8 106-43-4 Test Parameter Result EPA 314.0 Perchlorate - lon Chromatography PERCHLORATE 589 SIV-846, 3010A Metals Digestion 3010A ACID DIGESTION 05/01/2007 12.00 SIV-846, 60108 (Water) Metals Analysis by ICP - 6010 ARSENIC U BARIUM 44.1 CADMIUM U CHROMIUM 10. J LEAD U MANGANESE 18.1 SILVER U TIN U ZINC 22. J SW-846,7470A' '"• ' MercuryAnalysis MERCURY U SIV-846, 82608 (Water) Volatile Organic Analysis • ACETONE U BENZENE U BROMOCHLOROMETHANE U BROMODICHLOROMETHANE U BROMOBENZENE U BROMOFORM U BROMOMETHANE U 2-BUTANONE . U N-BUTYLBENZENE U . SEC-BUTYLBENZENE U TERT-BUTYLBENZENE U CARBON DISULFIDE U CARBONTETRACHLORIDE U CHLOROBENZENE U CHLOROETHANE U 2-CHLOROETHYLVINYL ETHER U CHLOROFORM U CHLOROMETHANE U 2-CHLOROTOLUENE ; ' U 4-CHLOROTOLUENE U Units I.' ."T" ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ZZZ: ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L • ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL "ZZZ""ZZ. 5 20 2 1 10 20 1 1 30 10 0.3 30 0.22 0.31 0.19 0.37 0.42 0.57 1.11 0.3 0.16 0.2 0.13 0.27 0.16 0.35 1.71 0.3 0.81 0.24 0.15 EQL ZZZ.. 20 100 10 5 50 100 5 5 150 50 1 100 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 Factor zz..zz. 5 1 ".Z Z" Analvst ZZZZ KEN ;;;.;;; MTB MTB MTB MTB MTB MTB MTB MTB MTB MTB TCP LSH LSH LSH LSH . LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH Test Oate - 04/30/07 ; •.: ••;;;;; "; 05/01/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 05/02/07 ; 04/26/07 "•; 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 Page 11 of 13 Listing of Results by Sample Sample Delivery Group: 0704036 Client Sample ID; 2163-J-7 Sample Description; ATK-DLV - Groundwater Spring 2007 Laboratory Sample ID: 0704036-05 Date Sampled; 04/24/07 14:21 CAS Number tesiiiiieiiiod: 124-48-1 _ 96-12-8 74-95-3 106-93-4 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-4 156-60-5 78-87-5 142-28-9 563-58-6 10061-01-5 10061-02-6 590-20'-7 100-41-4 591-78-6 87-68-3 98-82-8 99-87-6 75-09-2 108-10-1 91-20-3 103-65-1 100-42-5 630-20-6 ' 79-34-5 127-18-4 108-88-3 87-61-6 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 96-18-4 95-63-6 108-67-8 106-05-4 75-01-4 1330-20-7 95-47-6 460-00-4 1868-53-7 17060-07-0 2037-26-5 Test Parameter SW-846, 82608 (Water) Volatile Organic DIBROMOCHLOROMETHANE 1,2-DIBROMO-3-CHLOROPROPANE DIBROMOMETHANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,1-DICHLOROPROPENE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE 2,2-DICHLOROPROPANE ETHYLBENZENE 2-HEXANONE HEXACHLOROBUTADIENE ISOPROPYLBENZENE 4-ISOPROPYLTOLUENE METHYLENE CHLORIDE 4-METHYL-2-PeNTANONE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1,1,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2,3-TRICHLOROPROPANE 1,2,4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENe VINYL ACETATE VINYL CHLORIDE m,p-XYLENE o-XYLENE BROMOFLUOROBENZENE DIBROMOFLUOROMETHANE 1,2-DICHLOROETHANE-D4 TOLUENE-D8 Result Analysis U U U U U U U U U u u u u u u u u u u u u u u u u u u u u u u u u u u u u 16.2 u u u u u u u u 106 103 105 100 Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L . ug/L ug/L ug/L ug/L ug/L % % % % MDL. 0.18 0.35 0.25 0.15 5.86 5.62 5.88 0.66 0.49 0.29 0.16 0.16 0.34 0.16 . 0.24 0.17 0.4 0.18 0.9 0.16 0.7 0.9 0.58 0.24 0.77 0.53 4 .0.15 0.17 0.25 0.85 0.28 0.21 0.23 4.37 0.16 0.25 0.71 0.25 0.33 0.19 0.29 0.13 0.3 1.6 0.18 Dllul EQL Fac 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 'l 10 10 10 . 1 10 10 10 10 1 10 1 10 1 • 10 1 10 1 10 1 10 1 10 1 10 1 10 . 1 10 1 10 10 1 10' 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 . 10 1 10 1 10 1 10 1 10 1 ion tor Analyst LSH LSH • LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH LSH ' LSH LSH LSH LSH LSH LSH . LSH LSH LSH LSH LSH LSH LSH LSH • LSH LSH Test Date 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 .05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 • 05/01/07 05/01/07 05/01/07 • 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 05/01/07 Page 12 of 13 Data Reporting Qualifiers U Indicates that the analyte was not detected, or the analyte was detected but was below the MDL. B This flag is used when an analyte is found in the blank as well as the sample. indicates an extimated value. This flag is used either when estimating a concentration for tentatively identified compounds or when the data indicated the presence of a compound that meets the identification criteria but the result is less than the EQL (e.g. 3 J with an EQL of 10). MDL Method Detection Limit: The minimum concentration of a substance that can be confidentiy measured and reported. The laboratory has demonstrated that the MDL can be achieved in a laboratory reagent blank, but does not guarantee it can be achieved in all sample matrices. EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many analytes the EQL is selected as the value of the lowest standard in the calibration curve. Dilution Dilution Factor: The prepared sample was diluted by this factor because the Factor sample was too concentrated or due to other interferences in the sample matrix. Any dilution factor causes a corresponding increase in the MDL and EQL. Page 13 of 13 ATK Launch Systems Group Environmental Laboratory 07C?MO^(^ Client Nn,n. A-X1C LOLUU-ck, ^y ^ leA^>^^ ired, no cooler Q Hand delivered, sample* Sample Receipt Checklist SDQ No. (7t?^H(7'^ (^ Carrier:, Q Hand delivered, no cooler Carrier Number: sample(3) taken out at receiving counter //A Cooler Information; Cooler NumberAD: g-^^ <( IA) luU. Condition of.Shipping Container; Cooler Sealed (taped): Custody Seals Present: Coolant: State of Coolant: Ttiermometer ID: Hly^Mit!9*f Reading:. Packing Oescription: jj^ood QYes DYes Qlntact Qlce QFrozen QFair J^o QBroken QBlue Ice ^one QPartially Frozen V» °C CF: QNot Applicable QNot Applicable QNot Applicable QDamaged (explain). Seal Number: Other: QMelted Corrected Temp;_ Temp Blank Included: QYes QNo Chaln-Of-Custody Informatian: COC Present: ^ Itf rsr-T / i^«s COC Niimhar(s): g- I C> 7 > (» COC signed (relinquistied and received): jt^'es COC or LWI agrees with sample labels: SJ'ss Notes; -. L. QNo QNo QNo Other; QNot Applicable QNot /applicable Sample Information: Samples included in cooler: (^ICP^^^O # Custody Seals Present: Sample containers intact: Samples in proper containers: Sufficieni sample volume: All samples received in hold time: QYes Qlntact JJ^es <Yes X^e. Xes Water - VO/^s have zero tieadspace: JBPre-prosenred with HCl: Other. QBroken Seal Number(s). QNo Notes: QNo QNo • QNo • «; QNo QNot Applicable re-preserved with Na,S,Oj: QNon-Preserved: Water - pH acceptable upon receipt; JfVes QAdjusted (see comments below) QNot Applicable HNOJ = ^ */- HiSO. = NaOH = ZnAC /NaOH = HCL = Water • pH adjusted; (mfg. & Lot No.) HNOj • HjSO.. NaiSOjOj Other _ Notes;-. NaOH. _ZnAC. _HCI_ (8 SOP-102FormA 0704036 ENVIRONMENTAL LAB WORK REQUEST TO THIOKOL ENVIRONMENTAL LABORATORY FROM: Dave Covington ORGANIZATION: I Environmental Services EXTENSION: 3898 MAJL STOP: 301 LWRNO.E12736 Login No. COST CENTER: 8200 WORK ORDER: 988PLS333 GW DATE: 04/24/07 REPORT RESULTS TO: HELEN RAVSTEN, MS 301 SAMPLE INFORMATION SAMPLE 2159 2160 2161 2162 2163 DATE 4-24-07 4-24-07 4-24-07 4-24-07 4-24-07 TYPE G C LOCATION Trip Blank J-IHS J-l J-7 HS J-7. \ TIME 10:30 11:15 11:56 13:35 14:21 TEST VOA (Method 8260) Perchlorate, Metals, (Method 6010), Voc's (Method 8260) REMARKS |8;i«S:k^;X'g,sn, CHAIN OF CUSTODY RELINQUISHED BV £_a^. DATE ^Vsr-^7 TIME P^Sf RECEIVED BY vZhJeui- DATE iZ-^^s-cP'T TIME ^^•?S^ FOR LABORATORY USE ONLY DATE COMPLETED ^ DATE REPORTED SIGNATURE HYDRASLEEVE QA/QC SAMPLE RESULTS EQUIPMENT BLANKS • CONSTITUENT 1,1,1,2-TETRACHLOROETHANE 1,1,1-TRICHLOROETHANE 1,1,2,2-TETRACHLOROETHANE 1,1 .i-TRrCHLbROETHANE 1,1-DICHLOROETHANE 1,1-DICHLOROETHENE 1.1-DICHLOROPROPENE 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROPROPANE 1,2,4-TRICHLOROBENZENE 1,2,4-TRIMETHYLBENZENE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-BUTANONE 2-CHLbRdETHYLviN'i'L ETHER 2-CHLOROTOLUENE 2-HEXANONE 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE 4-METHYL-2-PENTANONE ACETOtJE BENZENE BROMOBENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBONDISULFIDE ' CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHErME CIS-1,3-DICHLOROPROPENE DIBROMOCHLOROMETHANE • DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE m,p-XYLENE METHYLENECHLORIDE NAPHTHALENE N-BUTYLBENZENE N-PR6PYLBENZENE"" '" o-XYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE fEfRACHLOROEfHENE TOLUENE WELL EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS"""" EBHS EBhis EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS - EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EBHS EB'H'S"" EBHS EBHS EB HS EB"HS EBHS EBHS EBHS EBHS EBHS" EBHS SAMPLE NUM 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 _2178 2178 "' 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 '2178 " •""2178"" 2178 2178 2178 2T78 "' 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178 2178~"~ 2178 LAB 4 4 4 4 4 4 "4 4 4 4 4 4 __4_ 4' 4 "'""4"" 4 " "4 4 4 4 4__ "4 4 .4 4 4 4 4 4 _4_ 4' 4 4 4 .' ZZ 4 4 4 4 4 4 4 4 __4.__ 4" 4 4 4 4 4 4 _ 4 Z iZ 4 4 __4___ 4" 4 SAMPLED DATE 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/69/2667 05/09/2007 05/09/2007 . 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 'j_5/09/2007 '"65'/09/2b67 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 "05709/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 CONC U U •U __U _ u" u U U u" • U U U _U u u u u u u u u u u u u u u u u u u u u u ~ fZ.. u u u u u u u u u " u"" u u u iJ"" u u u u u u u 1.6 J EQL 10 10 10 „10 10 10 ^1p_ To" 10 10 10 ^10 _ ib' ' 10 10 10_ 10 10 10 JO '""16"" 10 10 10 10 10 100 10 JO ~"i6 10 10 10 Z 1°.. "'' fo" ' 10 10 10 i"o 10 10 10 10 "10 . 10 10 10 10 10 10 10 "To""" To""" 10 10 _10_ ... ^_. 10 UNIT ug/L ug/L ug/L i!9'L. ug/L ug/L ug/L _ug/L_ ug/L ug/L ug/L ug/L ug/L' ug/L ug/L _ug/L ug/L ug/L ug/L ug/L .,y.g'J:i. ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/J- ys/L ug/L ug/L ug/L ug/L ug/C ug/L ug/L ug/L _ug/L ug/L" ug/L tig/L jjg/L ug/L ug/L ug/L ug/L "ug7L ug/L ug/L Jig"-, ug/L ug/L' LAB SAMPLE ID 0705026-02 0705026-02 0705026-02 0705026-02 ""070502'6-62 0705026-02 0705026-02 0705026-02 0705026-02 0705026-02 0705026-02 0705026-02 JD705026-02 6765626-02" 0705026-02 0705026-02 0705026-02 0705026-02 0705026-02 0705026-02 0705026-02 07059_26;02 "676"56"26-62 0705026-02 0705026-02 • 0705026-02 0705026-02 0705026-02 0765026-02 0705026-02 _0705026-0_2 0705626-0~2 0705026-02 0705026-02 0705026-02 ''6705026;02^ 07'05b26-b2" 0705026-02 0705026-02 0705026-02 ~b"705026-02' 0705026-02 0705026-02 0705026-02 0705026-02. 0705026-02' 0705026-02 0705026-02 0705026-02 ' 0V05O26-62~ 0705026-02 0705026-02 0705026-02_ "6765026^2" 0765626-02' 0705026-02 0705026-02 0705026-02 ""6765626-62" 0705026-02 1 Dilution 1 1 1 1 1 1 • 1 1 _. 1 1 1 1 1 1 1 .. .1 _ _ J "i 1 \ •1 1 1 1 1 1 1 1 1 1 1 1 1 •1 1 ' ZZ.ZJ 1 1 1 J '~-\ 1 1 1 1 '"'""'"'1 1 1 1 'i 1 1 1 i 1 1 1 . 1 1 EB-3 HYDRASLEEVE QA/QC SAMPLE RESULTS EQUIPMENT BLANKS icONSTITUENT h-RANSj^l ,2iiDICHLOROETHENE |tRAN'sT,3iib!c"H'llbRb'p"ROP^^^ TRICHLORbETHENE fRICHLbRbFLUOROMETHANE VINYLACETATE VINYLCHLORIDE 1,1,1,2-TETRACHLOROETHAI>4E 1, l", i-TRICHLbRbETHANE 1,1,2,2-TETRACHLOROETH/\NE 1.1,2-TRICHLORbETHANE ilt'oicS'LOROEfHANE" "' • "'"" ' lil-bicHLbROETHENE 1,1-DICHLOROPROPENE 1,2,3-TRICHLOROBErvlZENE i,2,3-fRiCHLORbPR"bPANE' 1,2,"4-TRICHLO'RbBEI^'ZEN"E'_^ " i,2,4-TRIMETHYrBENZE"l^E "" 1,2-DIBRbMO:3-CHLOROPRbPAt>JE 1,2-DIBRbMbETHANE 1,2;piCHLb'RC«EfgZENE ' "' 1,2;D"lc'HLbRb'ETHAN¥ " '"'_' i ,2i^blCHLOR'bPROPA"NE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DJc"HLbRb_PRbPANE '^f '_ i",4-blCHrbRbB'E"NZE'l^E 2,2-DiCHLbRbPROPANE b-BUTANONE ' 2-CHLOROETHYLVINYL ETHER 2'-CHL'0Rbf0LUE"NE 2-HEXANONE 4-CHLbROTOLUENE 4-lsbPRbF>YLTbLuENE 4-METHYL_-2-p'ENfANbNE '..... A"CET"b"N"E'""" "" BEtMZENE BRqii^OBENZENf ' f f BROMOCHLORbMETHAriilE BROMODICHLbRbMETHAN'E" BRO'MOFO'RM " '"" BROMOMETHANE ' CARBOfij blSULFIDE CAR|[0N TETF^CHLOra CHLbROBENZENE" " ' ' CHLOROETHAtilE CHLbROFORM" CHLbROtul'EfHAiNE CIS':i,''2;picH"LORbETHENE ''f "ZZZ CIS-i,3"-DICHLOROPROP'ENE blBRbMbCHLORblilETHANE blBROMbMETH/SiNE blCtCORqblFLJjbRqME'fHA^^^^^ ETHYLBENZENE " HEXACHLOROBUTADIErME ISOPROPYLBENZENE m,p-XYLENE METHYLENE CHlbRl'DE" "' " "' 1" NAPHTHALENE N-BUTYLBENZEtijE N-PROPYLBENZENE" _ WELL EBHS E'BHS " EB HS EBHS EBHS EB HS 'HS'EB"''" HSEB' HSEB HSEB HSEB HSEB " HSEB HSEB HSEB HSEB" H'S'E'B '" HisEB HSEB H'S EB"'"' HS EB "HSEB' " HS'EB " HSEB" " HSEB"" "HS'E'B""" HS EB HSEB HS EB HSEB HSEB HS EB HS EB HS EB" HSEB HS EB HSEB HSEB ys EB_ HS EEI HSEB HSEB HSEi"_3 HSE"B HS EB HS EB HS EEI HSEB HS EB " HS EB HSEB" 'HS'EB 3 HS'EB' HS EB HSEB HSEB HS'EB HS EB " HSEB HSEEi_ SAMPLE NUM 2178 '"'"2I'78'"" 2178 2lii'8 2178 2178 ••2i84 " 2184 2184 2184 ' "iw" '""2184 "" 2184 2184 2184'7 2184 2184 2184 '2184"" 2184 'i "2184 " Z 2184'.'..'.,'. 2184 2184 2184 2184 i2184 ..2.1.84 " "_"'_2184'3 2184"'" 2184 2184 2184 ""2184 2184 2184 2184 ' .2,184 .1. '2"i84 "' 2184" 2184" _2i843 ""2I84""" " 2184 2J^ 2184 _2184 '"2184' " 2184 2184 2l'84'" 2184 2184 ._2184,„, ""~2i'84'"" 2184 "2184 2184 LAB 4 Z.'^'Z 4" "'4" ..:..4 4 '"'4'" " 4 ' 4-'"' 4 ""4"' ZfZ. zz • 4 _4'_' '"4 " ' "4 "" '*.. . 4 "4" ' .4" 4 •" 4'" A'_ " 4"" 4 .4 4 Z iZ 4 4 "" 4' • 4__ 4 4 4 ZZ... '"4 " '""4"" 4" 4 ' 1 .1"-. "4 4 _" 4" 4 ' '4 .... ^ . 4 " ~ Z' '""4"' zz. " '4 i" 4 ... .^.. 4" 4 4 SAMPLED OATE 05/09/2007 " 05/0'9/2007' 05/09/2007" 05/09/2067 05/09/2007 ^05/09/2007 "657i"q/26q7"' 05/16/2067" 05/10/2007 05/10/2667 ' 65/10/2007"' " 057l"0/2"607 05/10/2007 05/io/2oq-7 057lO/2007 65/10/2607 05/10/2007 05/10/2067 05/16/2007 65/i"6726o7" 05/10/2007 05/10/2007 65/10/2007 "65/16/2667 _ 05/10/2007 "05/10/2007" 05/10/2007 05/i 6/2007 05/io/2qqf " q57i"q/2po7' 65/16/2007 05/10/2007 05/10/2007 _05/10/2"q07" 'o'57i'6'72007"' 65/10/2607 05/10/2007 65/10/2007 " 65/iq/2oo7" q57i'6'/2o67 65/10/2607 "65/10/2067 • "05/10/20"'07' 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 057i6/i2607' "05/10/2067 05/10/2q67 'osnoiidof "65/10/2007" 05716/2607 05/10/2007 65/10/2667 05/10/2007 ""05/10/2007 65/16/2607 _0;5/1CI/2067 COtMC u zz u "u"" u u^ ;... U.." u ...^ "'•"u" u u u u ! Iu "~ u'" u 'u' zz ...iiZ u' IJ u _IJ _ Ci " u u _ u '""u u u u _u___ "~u " u I .....zz u ..yL. u' u u ' u~ u 'u' iJ "u" '" u"' u . ^ zz. u' u u u" u u u JJ EQL 10 io ' 10 io'" ' To T? 'i"6 '"fo " io ^o ""10.1 16 "" '16 " 10 "' 10 Z. ip."" '16 "10 10 16 " '10 "10 10 16 "" "io " " "i'o""" io 10 'i'6 10 16" 16 Z. •'°.„ ""i"66 ib 10 io .Z^o..Z "' 10 "" 16 10 ZJ^... 10" 10 . .10 10 - -„.„... io 16 .... ^.^.... _'"io J' '10'"" ig. ' 10 JO _ '""10 J" ""10 i'6 .1.1°.--. UNIT ug/l. 'ug/ll" ug/L ug/ll "g'L ug/L_ .ug/L '."g"-... ug/L ug/L Jjg/L ,ug/"L_ ug/L .yaZ. ug/L "u"g"/L' "ug'/L ug/L ug/L ug/L 'ug/L ug/L "ug/L ug/L ug/L ug/L". ..."g'L. ug/L Lig./L. ug/L ..yg'-L, ug/L jjg/L ug/L ..yg/L ug'L _ug/L_ . ug/L ug/L ug/L ug/L Tg"/L_ u'g/L ug/L ug/L ug/L ^.u.g'k ug/L ug/L ug/L ...'jg/L-T ug/L ..yg/L. ...."g'L ..".g^L y.g'L ug/L ug/L" ..yg^L... LAB SAMPLE ID q7q5026-q2^ 6705026-02 0705026-62 0705026-02 0765026-02 0705026-62 0765027-qi O7o"5027-6i 0765027-01 "0765027-61 " \ q765b27-bT' " 0705027-01 0705027-6i 0765027-61 0705027ii6l "0765027-61" '0765027-61'" 6705627-01 0765027-61 ''O705027;q"l 0705027-61 0'7b5b27-"6i 0705027-01 ' 6765627-qi 0"76"5"027-6i b765027-"01 0705027-01 0765027-01 0765027-01 _q765627-qi'_ "'0765627-01" 6705627-61 0765027-01 "6765027-01 "'6765627-01" 0705027-01 0705627i-6l 0705027-01 "0705627-61' 0'765'027-bi" 0705027-01 0765027-61 07q5'o27-q"i' 07b'5'027-'6i 0705027-01 b705b27-0i 07O5q27-0J^ 67056'27-6l 0705627-01" 0765027-01 0705027-oi "b7b5"627-6i' b70""5b27-bi 0705027-61 0705027-01 0705027-01 0705027-01 070~5027-oi 0705027-0 i 0705027-01_ Dilution 1 1 ..... 1 1 .„y.. "1 1 " "-' i • 1 _• 1 "" 'i ' 1 1 1 1 1 """"'""' 1 1 •...•.,...•• J 1 "1 '. .• .'1 1 _ ".1 1 "1 1 i 1 1 1 ... 1 2 1.1 " i 'i 1 .ZZ J ,_"! "1 '""" "1 '1 " "1 j "i 1 1 Z.. Z.2 f 1 """ 1 1 1 1 1 i ...1 _ 1 EB-3 HYDRASLEEVE QA/QC SAMPLE RESULTS EQUIPMENT BLANKS CONSTITUENT o-XYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE TRICHLOROFLUOROMETHANE VINYL ACETATE VINYL CHLORIDE WELL HSEB HSEB HSEB HSEB HSEB HSEB HSEB _ H'S'EB"""' HSEB HSEB HSEB HSEB SAMPLE NUM 2184 "2184"" 2184 2184 2184 2184 2184 2184 2184 2184 '""2"i84 " 2184 LAB 4 "4 4 4 4 4 _4_ "4 4 •4""' 4 SAMPLED DATE 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 CONC U _ """u"' u u u 1.1 J y_ """u"" u u u"' u EQL JO '"16 " 10 10 10 10 10 10 10 10 10 UNIT ug/L ug/L ug/L ug/L ug/L ug/L ..ygi.L.. ug7L ug/L jjg/L. ug/L ug/L LAB SAMPLE ID 0705027-01 0705027-01 0705027-01 0705027-01 0705027-01 0705027-01 0705027-01 0705027-01 0705027-01 0705027-01 0705627-0"?' b76'5027-bl Dilution 1 i 1 1 1 1 _ J "'""'• """i 1 1 ' i 1 EB-3 m m m m HYDRASLEEVE QA/QC SAMPLE RESULTS FIELD BLANKS • CONSTITUENT 1,1,1,2-TETF{ACHLOROETHANE i.l.l-TRICHLORbETHANE i,i,2,2lf ETRACHLORbETHANE 1,1,2-TRICHLpRqETHANE i,"l-DICHLORbETHANE 1,1-DICHLOROETHENE i,i-DICHLOROPROPENE 1,2,3-TRiCHLbROBENZENE 1,2,3-TRICHLOROPROPANE 1,2,4-TRICHLOFtqBENZENE T2,4-TRIMETHYLBENZENE CHLOROPROPANE i,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-piCHLqROETHANE i,2-blCHLbROPROPANE 1,3,5-TRiMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE T,4-DICHLbRbBEN'zENE 2,2-blCHLOROPROPANE 2-BUTANONE 2-CHLORbETHYLVINYL ETHER 2-CHLO~R(5TbLUENE 2-'HEXANONE""' 4-CHLORbTbLUENE 4l|SOF>RbPYLfOLUENE" 4lMETHYU2-PENTANqNE ACETbNE777I7"""'Zii'Ii'. ZZ.ZZZ'. BENZEN'E '""7 "Z ZZ' '. BROMOBENZENE BRbMbCHLbRqMETHANE ^ 7i 'BRbMbblCHLbROMETHANE BROMOFORM BROMOMETHANE CARBbN DISULFlbE - CARBON TETRACHLORIDE CH'LORbBENZiENE . CHLORbETHANE"' CHLOROFORM CHLOROMETHANE CIS-1,2-piCHLqRqETHENE cTs-'i ^IpicH'LqROPRbpENE J DiBRbMOCHLbROMETHANE "' DIBROMOMETHANE DICHLbROblFLUbROMETHANE ETHYLBENZENE 'H EiXACHLOROBUTAbl EN E ISOPROPYLBENZENE" m,p-XYLENE METHYLENE CHLORIDE NAF'HTHALENE N-BUTYLBENZENE WELL FB FB" FB FB7... FB"" FB FB FB _ "FB " FB FB FB FB FB"~ FB FB FB FB F'B" FB FB FB" FB F"B 7 FB FB FB FB F.B 'F'B" FB FB FB_ 7" FB " F"B" FB FB FB •' FB7 FB FB FB- FB FB FB FB FB FB'" F.l"i FB FB FB FB'"i SAMPLE* 2170 2170 2170" 'M.i!7P., . .ZZZ "2170" 2170 2170 2170 2170 21 T'O 2170 2170 i 2i'70'7 i2i76 ' "2176 2170 2170 2i76'""' "' 2170 "2176 217'6" 2170 •-2170"" -•2Y70 • • 2170 2170 2170 ^ ""2T76'"" 2i76' • 2176 1 2170 2li70'7 2170 " 2170 2170 2176 ' 2170 2170 ••2{fQ-'" 2170 "21767 21767 - 2ifo 2i'70 "2170 2170 2170 2170"" 2170" 2170 21.7CI____" ""'2170 LAB 4 4" 4 ZZZZ 77.4 ^ """4 "4 • .i,ji7ii 7,4"" •4" ' "4 •4 47'' 47;' • z 4 i4"' 7i. ""4"" "ZZ 4" 4 "4" - „ ..... '"4' '4' 4 iiiil... '".'li'"' 4' 4 '7..1'. "4_ 4" 4 4' 4 " "4"'" 'ZZ± 4" 4 " "4 .... ^ 4 "1" 4 4 " 4 "" ""•4 • 4 4 ....li ZZ SAMPLED DATE 05/07/2007 65/67/2007 65/£7/2067 05/07/2667 05/07/2007 05/07/2007 05/67/2667 65/07/2007 05/07/2007 05/07/2607 oiiomoo? 05/67/2067 65/£7/2007 65/67/"2067 65/07/200'7 65/07/2007 05/67/2067" 65/p7/2007_ 05/07726"67" 05/07/2607 05/07/2007 05/07/2007 _05/67/2J)07 "65/0772667 05/67/2067 65/07/2007 05/07/2667 05/67/2067 '05/67/'2"'067 65/0772667" 05/07/2007 65/07/2067^ 05767/2667" 05/07/2007 05707/2607" 65/07/2007 05/07/2667 6576772667 05/07/2667' 0'5/07/2607" 05/67/2667 05/07/2007 05/07/2007 05/07/2067 05/07/2007 05/07/2667 65/07/2007 (35/07/2007 65/67/2007 05/07/2007 05/07/2007 05/67/2067 6"5'707/2607' CONC U u u u""' u " u " "u u " 'u ' ' "u u"' u u u LJ ' ' 7u "u 1 "u u u ZZZ "u u u u •' u • u u u "Cl' TJ" 7..U.7 u' u"" u u u "u'" u' '"0"" u zzzz 77u7" • "u' u 'u z. zz. u Z" u ..iyi7,ii "u EQL 10 "io 10 " io ""10 10 16 16 "16" IP ' "io io 16 T"6'' io To io 10 10 "io ' 10 •16 "10 ' 16 "' 16 io 16 To "T'6'6" "io 10 7716 . ""io-" 'io 10 10 10 '16 " 16 10" 10 7 1° 7 ipi ' 'io" io 10 10 "16" .'10" 10 " To " To To " UNIT ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ,ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 'ug/L ' ug/L ug/L ug/L ug/L ug/L ug/L .ug/L,. ug/L ug/L "ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug'/L ug/L ug/L ug/L . .yg/L ug/L LAB SAMPLE ID 0705015-04 0705615-04 0705015-04 0705015-04 0705015-04 0705015-04 0705015-04 0705615-04 CI70'56l570'4'' 6705015I04 67050i5l04 0705015-04 _07050X5:P4_ 0705015I64 6'7650i5-04 0705015164 6705615-64 0705015-04 07656'l5-0'4" j6'7650'l'5-64 '67050i5-04 0705015-04 0705015-04 '6705615-04 67056i5-04 0705015-04 6765015-04 070501^-04 76705015I04 "6765615-64 0705015I04 07050i5l04 767056l5;_04 07056j5'-64 "67650"i5-64 0705015-04 6705OI5I04 0705015704 76705015764' '07650T5i^64 6705615-04 0765015-04 6705615-04 07050i5l04 0705015-04 0705015-04 0705015-04 '6765015-04 '67"656l¥-64 6705015-04 0705015104 76765015-04 67050 i^slpT Diiution 1 1 777i7.i ..'iiil .iii.ill ................ 1 1 "'77 i ••". i '1 '1 _77.ii.ii..! 7_,77.i. 1 i "" "i 1 1 "1 '777...i..! ...." 1 1 i 77. ,.7,1 i7ii".ii ..Zii ""i 1 .....Z. 1 "7.7. 1 '"77 7,.i """ ""1 •'""1 __ 1 '^ 1 1 1 "7_.., ,1 7i .... ""T 'MilMi 1 _ J "i FB-1 HYDRASLEEVE QA/QC SAMPLE RESULTS FIELD BLANKS [CONSTITUENT N-PROPV-LBENZENE ._" .. . oi-XYLENE7 Z^L.-Ii-Zi" ZZ.ZZ SEC-BUTY'LBENZENE ' [STYRENE i' TERT-BUTYLBENZENE TETRACHLbRbETHENE TOLUENE" """Z" '7i7 I . Ii T'RANsT'i"2-Dlc"HL"0RbET''HErgE TRANS-1,3-DICHLOROPROPENE TRICHLbROETHENE TRicHLbROFL'uORbM"ETHA"NE VINYLACETATE _ ; _ VINYL CHLbRIDE7 7 7 . „, 1,1 i 1,2lTETRACHLbRbETH ANE i,i,i-TRiCHLbRbETHANE 1,1,2,2-TETI^CHLORqETHANE i,T,'2'TRicHLORqETHANE 7 Z. • 1,i-DICHLbROEfHANE~ T,ilDlCHLbRbETHE"NE" iT-DICHLORbPFtOPENE i,2',3-T'RICHLbRbBE"NZ"E"NE 1,2,3-TRICHLOROPROPANE 1 ,2,4-TRICHLOROBENZE'NE i,"2,4"-TRIMETHYLBENZENE CHLOROPROPANE ii2-blB"RbMbETHANE 1,2-DICHLOROBENZENE i,2-DICHLbF[qETHANE 1,2-'blCHLbRbPR'OPAN"E 1 i3i5lTRiMETHYLBEN2:ENE 7 1,3-"DICHiiiiOROBENZEN'E"' 1 .S-blCHLOROPROPANE i,4-DICHLbRbBENZENE7 2,2lDICHLbRbPRbPAt^E 2-BUTANONE 2-CHLOROETHYLVINYL 'E'THER 2-"CHL0RbTqLUEN| \ 2-HEXANONE 711 4-CHLOROtbLUENE iTsbPRbPYLfbLUENE 4-METHYL-2-PENTANONE ACETqiME BENZENE •" BROMOBENZENE BROMOCHLORqMETHANE BR"bMOblCHLO_RqMETHA^^^^^ I_;,7 BR'bMOFbRM ' " BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLb'RqBiENZEN|7 77i.ZIi i I..i CHLORbETHANE " CHLOROFORM WELL FB FB FB FB" FB' FB FB" FB FB" F|L.„.. ii. FB '" " FB" FB FB " " FB FB_ FB FB FB ' FBIZ ii FB F'B FB FB ""• FB FB " FB FB FB FB 'F'B'"""' FB FB FB FBI FB' F'B" """ FB FBi FB777I FB "FB" FB FB FB FB" "FB ' FB FB FB" FBLIiZ. FB i^B., ,IZ SAMPLE# 2170 "" iiro 2170 2170 7 ..21.'707. "'2170 2176 2170 2T76 _____2170_7.. "2176 "2176 2170 7"""2i79'7..I 2179 2179_ """'2179 2179 _ "2179 2179 2179 _ :"2179 i 2179 2179 2179 " 2i79 '" 2179 2i76 " 2179" 2i79"" 2179 " 2179 2179 2179 "7 217'9 ""2179 2179 2179 2179 2T79 . 2179 ' 2179 2179 2179 " 2179 2179 2179 2179 2179 2179 "" "2179"'' ----- 2i79 LAB 4 ,..„.. 4 4 4 I III" "'74 ""'4 4 ZZ '" 4 """"4 "' 4 ZZ-77.4 _I "Ifl .IfZ"" "4 ii'T" • 4 '"""4 717.471 77.4.7 '4 ~ 4 4 4 "'"4 4 4""" ""4 4 4 4, ' T4 4 "4 4 1 .. 4 4 4 ZZZZZ. "4 "4 "" 4 . ....^..... 4 4__ " ' 4 •4 -" 4 SAMPLED DATE 05/07/2007 65/6772667 05/07/2007 '65/6772067 05/07/2007 "65767/2607 05/07/2007 05/07/2007 65/"o7/2667 05/0ii'/2667 05/07/2007 05/07/2007 '6570772667 " 6'5/69"/2667' 05/69/2007 05/09/2007 7P"5/09/20077 65/09/2007" 65/09/2007 65769/2667 65/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2667 05/09/2007 05/09/2007 65769/2007 "05/09/2007" 05/09/2007 _05709/2067'_ "65/09/2667' 05/6972007 65/69/2067 05/69/2667 "65769/2667' 05/09/2007 05709/2067 05/69/2667 05709/2007_ 65/6'9/2667 05/09/2007 05/69/2067 05/09/2007 05/09/2007 I95/69/26077 "65/69/20'07" 05/69/2007 65/69/2007 05/09/2007^ 05/09/2607 ""65769/2067" 65/097i26o7' CONC U U ' 'u Ll u lii u u ' u' 7y z u" """u""' "u u u u •"70,7 "u u u' " u"'"" u" "Cl" • u u I'iy... " "u" u" "u " "u u ui u iiii yi Z " vZ"" u u '^' u""7 ... ^ i u • u u "'""u "" "u" I. Z...Z u" u" u "u " u' "" u EQL 10 io" io'" ^o io 10 '""io . -...^.. 16" io '.lioIZ "ioZ." 'T9l7i ZoZZ 'To'"' io Ii 19.7. 16 io "-'To"" 10 19 16 i 16 "To"" '7io7'' To 16" 16 w" 10 10 16 16 ^71.07.. "16 "•10 16 .T6'7 16 io6" 16 10 io"'" iijO-Z "To"" 16 10 10 io •' 10 "io • UNIT -ug/L „ ug/L " ug/L " ug/L ug/L ug/L ug/L" ug/L ug/L 7ug/.L . ug/L lygi/Ll ug/L ug/L .yg/L.. ug/L ..liuglL ', yg/L ug/L ug/L " ug/C yg/L ....ug./L... ug/L ug/L ., yglL ug/L ' ug/L ug/L yg/L.! .„..ug/L. ug/L ug/L "ug/L ug/L ' ug/L 'ug/C" ug/L ug/L ug/L, ug/L "ug/L"" ug/L ,. ug./L.. 'Iug/L;', ug/L ug/L ug/L ug/L ug/ll ug/L "•~ug'7L""' ug/L LAB SAMPLE ID 0705015-04 "67656i5-04 0705015-04 '6705015-04 6705615104 67050i5J34 07950T5-^4 "6765615-04' 6765615-64 0705015-04 0705015-04 0705015-04 "67656i5-64 0705026-03 0705026-03 0705026-03 6765626-03 p70562"6l03" "6765026-03 0705026-^3 '670502"6-03' 0765626-63 0705026103 "676502"6'-63 6705026-03 0705026-03 6705626-"03 0705026:03 6765626-63 O765026I03 0705026-03 0~705626-03 '0765026-03 07651026-63 6705026-03 67050261-03 07056'2'6'-63" 0705626-03 6765026-03 0705026163 "0765626I63 076562"6-03 0705026-03 6705026-03 07'6502'6-03 6765026-63 0705026-03 07615026-03 0765026-63 0705026-03 0765626-63 0705026-03 O765026I03 Dilution 1 7Z7'.I.i.i '' 1 '1 1 i i 1 i _'!' ^_7i '" "'"i 1 •" '"'' 1 :...z:,..J 1 '1 I7il ZZ .. ... iZIi" iiiiii..i 1 " 1 Tl 1 1 i, i ' ^ "'•""""' i .. ^ 1 •" 1 . 1 ' Z.Z ' 7.. ""ii. 1 1 .7,. -Z "1 • 1 "iiiii" 1 . 1 _ .7ili 1 ""' 1 ZZI 1 1 ................J IZi! FB-2 HYDRASLEEVE QA/QC SAMPLE RESULTS FIELD BLANKS 1 CONSTITUENT CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE . DIBROMOCHLOROMETHANE DIBROMbMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE m.p-XYLENE METHYLENE CHLORIDE NAPHTHALENE N-BUTYLBENZENE N-PROPYLBENZENE o-XYLENE SEC-BUTYLBENZENE STY~RErgE TERT-BUTYLBENZENE TETFl/^CHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE TRICHLOROFLUOROMETHANE VINYL ACETATE VINYL CHLORIDE 1,1,1,2-TETRACHLOROETHANE 1,1,1-TRICHLOROETHANE 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICHLOROETHANE 1,1-DICHLOROETHANE 1,1-DICHLOROETHENE 1,1-DICHLOROPROPENE 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROPROPANE 1,2,4-TRICHLOROBENZENE 1,2,4-TRIMETHYLBENZENE CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3"lD'icH"LbROPRbPA"NE 1,4-DICHLOROBENZENE 2.2-DICHLOROPROPANE 2-BUTANONE 2-CHLOROETHYLVINYL ETHER 2-CHLOROTOLUENE 2-HEXANONE 4-CHLOROTOLUENE 4-ISqPROPYLTOLUENE WELL FB FB FB FB FB FB FB FB FB FB FB FB FB FB FB FB FB FB FB FB FB FB FB FB FB F_B ...^......... FB FB FB FB FB FB FB FB FB FB FB FB FB FB FB FB FB F"B FB FB FB FB FB FB FB FB SAMPLE* 2179 2179 2179 2179 "•2179 2179 . 2179 2179 2179 2179 2179 2179 2179 2179 2179 2179 2179 2179 2179 2179 2179 2179 2179 2179 2179 2179 _ 2187"" 2187 2187 2187 2187 2187 2187 2187 2187 2187 2187 2187 2187 2187 2187 2187 . 2187 2187 " "2i87 2187 2187 i2i87" 2187 2187 2187 2187 2187 LAB 4 4 4 4 4"" 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4. 4 4 _ ' "4" 4 4 4 4 4 4 4 4 SAMPLED DATE 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/09/2007 05/10/2007 65/1672007 05/10/2007 65/10/2607 05/10/2007 65/l67'2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 65/10/2607 05/10/2007 05/10/2007 05710/2067 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 CONC . U U U U Ll U U u u u u u u u u u u u u u u u u u u u____ U'" U u . u u u u u u u u u u , u u u u ""'"u""" u u u u u u u u EQL 10 10 10 '10 io 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 UNITJ ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ,iig/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L LAB SAMPLE ID 0705026-03 0705026-03 0705026-03 0705026-03 0705026-03 0705026-03 0705026-03 0705026-03 0705026-03 0705026-03 0705026-03 0705026-03 0705026-03 0705026-03 0705026-03 0705026-03 0705026-63 0705026-03 0705026-03 0705026-03 076i5026"-63 0705026-03 0705626-03 0705026-03 0705026-03 0705026-^3 0765027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-64 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0765627-64 0705027-04 0765027-04 II Dilution || 7. iii...i| 1 1 1 1 - 1 1 1 1 1 1 1 1 1 1 1 .1 1 1 1 1 1 1 1 1 1 "T 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 ...1 _., J 1 1 1 1 1 1 . 1 1 1 FB-3 HYDRASLEEVE QA/QC SAMPLE RESULTS FIELD BLANKS - CONSTITUENT 4-METHYLI2-PENTANONE ACETONE BENZENE BROMOBENZENE BRbMOCHLORbMETHANE BROMODICHLOROMETHANE BROMOFORM BROMO'M'ETHANE CARBON blSULFIDE CARBON TETRACHLORIDE bHLbFtqBE'NZENE CHLbRbETHANE "' CHLOROFORM CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DICHLOROPROPENE biBRbMOCHLORbMEfHA'NE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE ^^ HEXACHLORdBUTAbiENE ISOPROPYLBENZENE m,p-XYLENE METHYLENE CHLORIDE NAPHTHALENE N-BUTYLBENZENE N-PROPYLBENZENE o-XYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TETRACHLOROETHENE TOLUENE TRANST,2-lbiCHLbR0ETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE TRICHLOROFLUOROMETHANE VINYL ACETATE VINYL CHLORIDE WELL FB FB" FB FB FB FB FB_ FB" FB FB FB" "'" "F'B 'FB FB FB FB F'B FB FB FB FB FB FB FB FB FB FB FB FB FB IF'B FB FB FB FB FB FB FB FB SAMPLE* 2187 _ "2187 "~ 2187 2187 2187 2187 2187 2187""' 2187 2187_ _ ' 2i87" '" 2187 2187 2187 2187 2187 . 2187 2187 2187 2187 2187 2187 2187 2187 2187 2187 2187 _ '" ''2i87" "" 2187 2187 2187 2187 "2T87 2187 2187 2187 LAB 4 4 4 4 4 4 __ 4 ""4 4 ._ 4 77 4 "~ "4"" '" "4 4 4 4 4 4 4 4 •4"" 4 4 4 '4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 SAMPLED DATE 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05"/10/2667 05/10/2007 05/10/i2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/10/2007 05/16/2067 05/10/2007 05/10/2007 CONC U____ u'""" u u u u u u"" u u ..Z'uilZ iiZLI '" """u u u u Cl u u u u u u u u u u u u ... ^.... u u u u u u u u EQL _10_ 'T06" 10 . 10 10 10 10 " .10"" 10 10 _ 19 7..i6" 16 10 10 10 10 10 10 19- io"'" 10 10 10 10 10_ ""io""" 10 10 10 10 10 16 10 10 10 10 10 10 UNIT ug/L ug/L ug/L ug/L ug/L ug/L ug/L- ug/L ug/L yg/L,. . jjg/L _ ug/L " ug/C ug/L ug/L ug/L ug/L ug/L ug/L , ug/L "" ug/"L " ug/L. ug/L ug/L ug/L ug/L ug/C" ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L LAB SAMPLE ID 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 070502'7-6"4 0705027-04 ' 0705627-64 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 '6765627I04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04^ "67'0"5027"l04 0705027-04 0705027-04 0705027-0£ '67o562"7'164 0705027-04 0705027-04 0705627-04 0705027-04 0705027-04 0705027-04 0705027-04 0705027-04 Dilution J 1 1 1 1 1 '"" "1 1 1 "77 _.7i '"1 1 1 1 1 1 . 1 1 "i 1 1 1 • 1 1 '' i'i 1 1 -J """ i 1 1 1 1 1 1 1 1 FB-4 HYDRASLEEVE QA/QC SAMPLE RESULTS TRIP BLANKS li icONSTITUENT H ,1,1,2-TETRACHLOROETHANE 1,1,1 -TRICHLORbETHANE i ,i,2,2-f ETRACHLbROEWANE 1,1,2-TRICHLOROETHANE 1,1-DICHLOROETHANE kl-blCHLbROETHENE 1,1-DICHLORbPROPENE i ,2,3-TRICHLbRbBENZEN^^ i,2,3-TRiCHLbROPRbpAbiiE 1.2,4-TRICHLOROBENZENE 1,2,4-TRIMETHYLBENi2ENE CHLOROPROPANE 1,"2-biBR"bM"b"ETHANE 1 ,2~-D~ICHLOROBENZ'ENE' 1,2-blCHLORbEtHANE 1,2-DICHLbRbPROPANE i ,3,5-TRiMETHYLBEN2ENE 1,3-DiCHLORbBEN'ZENE 1,3-DICHLbRbPROPAN'E 1,4-DICHLORbBENZENE 2,2-DICHLORbPROPANE 2-BUTANONE 2-CHLb"RbETHYLViN"YL ETHER 2~-CHLbR0TbLUENE 2-HExi^N0NE 4-CHLOROTOLUENE W-ISOF-ROPYLTOLUENE 4-METHYL-2-PE'NTANbNE U'CETON'E BENZENE BROMOBENZENE BROMbcHLbROMETHANE, BROMODICHLbROMETH/\NE BROM'blFoRM BROMOMETHANE CARBON DISULFIDE CARBOtg TETRACHLORlbE CHLORbBENZENE CHLO'RO'ETHANE" CHLOROFOR'M CHLbROMETHANE cis-1 ,'2-DICHLORbETHENE CIS-1,3-DI(bHLbROPROPENE piBRbMbCHCbROMETHANE DIBROMbME"TH'ANE biCHLORODlFLUOROMETHANE EfHYLBENZE't^"E HEXACHLORbBUTADIENE IsbPRbPYLBENZENE m,p-i>(Y'LENE METHYLENE CHLORIDE NAPHTHALENE N-BUTYLBENZENE N-PROPYLBENZENE | IwELL jTB TB TB TB TB "TB TB TB. T"B' " TB TB TB fi TB TB TB T'B TB T'B TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB • TB TB TB T"B TB TB TB TB T'B TB" TB' 1 1 SAMPLE* 1 2149 2149 2149 i2149 2149 "2"l49 2149 ... .2149 . 1 " '2"14""9 2149 2149 .i2149 2149 2i4~9 2149 12149 2149 i2149 2149 I 2i49 2149 2149 2149 2149 2149 2149 2149 2149 2149 2149 2149 2149 2149 ' 2149 2149 2149 :2149 2149 2149 2149 2149 2149", 2149 2149 21 Tg 2149 2149 2149 2149 2T49 2149 2149 2149 2149 1 1 SAMPLED 1 DATE 1 04/16/2007 047l 6/2007 04/i672667 04/16/2007 04/16/2007 64/i672b07 04/16/2007 64716/2667 04/16/2667 04/16/2007 1 64/16/2067 04/16/2007 b"4i'16/2667 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/i"6/2007" 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/12007 04/16/2007 04/16/20617 04716/2667 04/'l 6/2007 04/li6/2667 04/16/2007 04/16/2007 "64/i6/2667' 04/16/2007 04/16/2067 04/16/2007 04/16/2007 1 [cONC 1 ^ U u 'u u u u ,_.__u_„_ '"u u LJ u u u u u u u u u u u u u u u u u u u u u u u U" u u u u u u u u u u u - 'u u u -U- U u u •Ll 1 1 1 EQL 1 ""^ 10 16 10 10 16 16 r - io ' 10 10 16 10 10 ia 10 16 10 10 1 ""^ 10 '•••10 10 10 10 10 10 10 10 Too 10 10 10 10 • 10 10 10 10 10 10 16 10 10 10 10 10 10 10 10 10 10 10 : io 10 10 1 UNIT •ug/L ug/L ug/L ug/L ug/L ug/L ug/L ...jg/L.,. ' ug/L ug/L . ug/L • ug/L ug/L ug/L ug/L ug/L" ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L- ug/L ug/C. ug/L ug/L 1 ug/L ug/L LAB SAMPLE ID 1 0704030-01 0704030-01 0704030-01 0704030-61 0704030-01 0704030-01 0704030-01 0704030-01 0704o'30-oi 0704030-01 0764630-61 0704030-01 0704030-01 0704030^01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 670'-4630"-01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 67046'36-6i 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 6764036-01 0704030-01 6'i'64636'-6i 0704030-01 0704030-01 Dilution 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 i 1 1 1 1 1 1 1 i i 1 1 1 1 i 1 1 1 1 1 i i 1 1 1 1 i 1 i 1 i| TB-r HYDRASLEEVE QA/QC SAMPLE RESULTS TRIP BLANKS CONSTITUENT o-XYLENE SEC-BUTYLBENZENE STYRENE TERT-_BUTYLBEN"ZENE__ TETRACHLORBETHENE" TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE fFSICHLOROETHENE __ ;i TRiCH'LORbFLubRqMEjrHANE^7 VINYCAC'ETATE • """" VINYL CHLORIDE 1,1,1,2-TETRACHLOROETHANE 1,1,1-TRICHLOROETHANE. 1 il ,2i2-tEfRACHLbROETHAN'E ' 1,1,2-TRICHLOROETHANE 1,1-DICHLOROETHANE 1,1-DICHLOROETHENE. 1,1-DICHLOROPROPENE 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROPROPANE 1,2,4-TRICHLOROBENZENE 1,2,4-TRIMETHYLBENZENE CHLOROPROPANE 1,2-DIBR0M0ETHAtJE_ lif-blCHLbRdBENZENE ' 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-BUTANONE 2-CHLOROETHYLVINYL ETHER 2-CHLOROTOLUENE 2-HEXAN'b'NE 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE 4-METHYL-2-PENTANONE ACETONE BENZE'NE BROMOBENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARB"bN IEIKACHCORIDE CHLOROBENZENE CHLOROETHANE CHLOROFORM CHLOROMETHANE Cls'li",2-blCH[bROETHiENE7 WELL TB TB TB TB TB TB TB TB TEl T'B T'B"" ' TB TB TB TB'Z., T'B""' TB TB TEI TB _ TB" ' TB TB TB TB T'B" •• TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB, TB _ T"B "" TB TB TB TB i^ZZ SAMPLE* 2149 2149 2149 2149 • 2149 2149 2149 2149 2149 214977 "•" 2-i49 '•"• 2149 2153 2153 2"i53" 2153 2153 2153 '""2153 '" 2153 2153 2153 2153 2153 2153 2153 2153 2153 . 2153 2153 2153 "' 2153 2153 2153 2153 2153 2153 2153 2153 2153 2153 2153 2153 2153 2153 2153 2153 2153 2153 2153 2153 2153 2153 SAMPLED DATE 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 04/16/2007 64/167i2667 04/16/2007 04/16/2007 64/16/2007 04/16/2007 04/23/2007 04"/23/"2067 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 "64/12372607" 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 6"4/23/2667 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 CONC U __U ""u"" U U U u u Ll Z.7y.__^ "u U U U __ u "Cl u u u u " "u u u u ; _u_ _ """u " u u u u u u ..u u u u u u u u """u""' u u u u u _ u " 'u " . u u. u u 7_JJ7 " EQL 10 10 10 10 10 10 10 10 10 10 10 10 10 io 10___ ' ' io 10 10 "• 10 10 "io"' 10 10 10 10 10 10 10 10 10 _ 10 ""To' 10 10 10 10 10 10 10 10 _100 "16'"' 10 10 10 10 10 10 10" 10 10 10 __ JO IZlo...'. UNIT ug/L ug/L ug/L ijg/L "ug7C" ug/L ug/L ug/L ug/L ug/C " u"g/L ug/L ug/L .....ug/L ug/L ' "ug/C" ug/L yg/L ug/L ......ug/L. „ ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L, ug/L ug/L ug/L ug/L _.,ug/L_ _ _ug7"L LAB SAMPLE ID 0704030-01 0704030-01 676"4036"6i 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 0704030-01 7^0764636-017 676463'0-6i"' 0704030-01 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 '"'67'64033-6i" 0704033-01 0704033-01 6704033-01 0704033-01 6"7046'33l6i 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 070463"3-01 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 " 07"6403"3loi 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 " O704633-6T'" 0704033-01 0704033-01 0704033-01 0704033-01 J0704033-01 1 DllutionI .., ^ 1 1 1 1 1 1 i .2} "T """1 1 1 J ...... . 1 1 J ""1 1 1 1 . 1 ... 1 1 1 1 _ 1 1 1 1 1 1 1 1 1 1 1 i 1 1 1 . 1 1 _1 ' 1 1 1 1 1 ....... TB-2 HYDRASLEEVE QA/QC SAMPLE RESULTS TRIP BLANKS ir IICONSTITUENT CIS-i,3-DICHLOF!OPROPENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE m,p-XYLENE METHYLENE CHLORIDE NAPHTHALENE N-BUTYLBENZENE N-PROPYLBENZENE o-XYLENE SEC-BUTYLBENZENE STYRENE TERT-BUTYLBENZENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLqROPROPENE TRICHLOROETHENE TRICHLOROFLUOROMETHANE VINYL ACETATE VINYL CHLORIDE 1,1,1,2-TETRACHLOROETHANE 1,1,1-TRICHLOROETHANE 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICHLOROETHANE 1,1-DICHLOROETHANE 1,1-DICHLbROETHENE 1,1-DICHLOROPROPENE 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROPROPANE 1,2,4-TRICHLOROBENZENE 1,2,4-TRIMETHYLBENZENE CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE i ,3-DICHLORbBENZENE" 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-BUTANONE 2-CHLOROETHYLVINYL ETHER 2-CHLOROTOLUENE 2-HEXANONE 4-CHLOROTOLUeNE 4-ISOPROPYLTOLUENE 4-METHYL-2-PENTANONE ACETONE BENZENE WELL TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB SAMPLE* 2153 2153 2153 2153 2153 2153 2153 2153 ^ 2153 2153 2153 2153 2153 2153 2153 2153 2153 2153 2153 2153 2153 2153 2153 2153 2159 2159 2159 2159 , 2159 2159 2159 2159 2159 2159 21597. 2159 2159 2159 2159 ,2159 2159 2159 2159 2159 2159 2159 2159 2159 2159 2159 2159 2159 2159 2159 SAMPLED DATE 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2667 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/23/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2607 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 6"4/2'472667 64/24/2697 CONC U U U U U U U U u u u u u u u u u u u u u u' u u u •u u u u u u u u u u u . u u u u u u u 'Cl u u u u u u u u u ,u. EQL 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 • 16 16 10 10 .10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 100 10 UNIT ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/C ug/L ug/L ug/L ug/L ug/L ....ug^L, . LAB L SAMPLEID 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 •0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 0764633-01 0704033-01 0704033-01 0704033-01 0704033-01 0704033-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 6764'6'36-6l 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 Dilution 11 1 1 "1 1 1 i 1 .1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 TB-3 HYDRASLEEVE QA/QC SAMPLE RESULTS TRIP BLANKS , CONSTITUENT BROMOBENZENE BROMOCHLOROMETHANE BROMppiCHLpROMETHANE^ BROMbFORM " BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE CHLbROFORM" CHLOROMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-DieHL0R"bPRbp"ENE biBROMOCHLbROMEfHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE mip-x'Y"LENE77'" 7"^ Z' l.'l M'ETHYLENXcHLORiDE",.,, ,7 7 NAPHTHACENE'" N-BUTYLBENZENE N-PROPYLBENZENE o-XYLENE SEC'-BUTYL8E'NZ"EN'E' STYRENE TERT-BUTYLBENZENE TETRACHLOROETHENE fOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE TRICHLOROFLUOROMETHANE VINYL ACETATE VINYL CHLORIDE i,iT',2-fETRACHL0RbE"fHANE" 1,1,1 -TRICHLOROETHANE 1,1,2,2-TETRACHLOROETHANE 1,1,2-TRICHLOROETHANE 1,1-DICHLOROETHANE 1,1-DICHLOROETHENE 1,1-DICHLORqPROPENE i,2,3"-"fRicHLbRbBE"NZ'ENE 1,2,3-TRICHLOROPROPANE 1,2,4-TRICHLOROBENZENE 1,2,4-TRIMETHYLBENZENE CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DICHLOROBENZENE 1,2-DICHLOROETHANE 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE 1_,3-DJCHL0RqBENZENE__ _ WELL TB TB TB "" TB '_' T'B"' ' TB TB TB iTB""_ T'B" TB TB TB TB' "' TB TB TB TB fB' TB7_ TB I TB""' TB TB TB TB TB TB TB fB TB TB TB TB TB TB TB TB TB T'B TB 'TB TB TB""" TB TB TB _ TB "' TB TB TB TB fi" TB SAMPLE* 2159 2159 2i59 '" 2159 2159 2159 2159 2159 71 ,2i59 "7 '""'"2i59' 2159 2159 2159 '2T5"9""'' 2159 , 2159 2159 2159 2'i59 '2159'"" 2159 2159 2159 2159 2159 2159 2159 2159 2159 2159 2159 2159 2159 2159 2159 2159 2164 2164 2164 2'i64" 2164 2164 2164 2164 2164 2164 2164 _ i2i"64"""' 2164 2164 2164 2164 2164 2164 SAMPLED DATE 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 04/24/2007 '64725"/2'667 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/20_07 64725/2667' 04/25/2667 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 64/25/2067 CONC U U u_; u u u u ZZy, u u u u u u u u u u u u u u u u u u "u u u u u u u _ u" u u u u u u u u u u u"" u u u u u u_ EQL 10 10 .' "to.. ' "io" 10 10 10 J0_ Z "loZI •"lio " 10 10 10 ZIi? I "io"" 10 10 10 10 16 10_ ""'16' " 10 10 10 10 10 10 10 10 10 10 10 io 10 10 10 10 10 10 10 10 10 10 10 16 10 T"6 10 10 10 10 10 10 UNIT ug/L ug/L u'g/L ~ ug/L ug/C ug/L ug/L ug/L "ug/C ug7C ug/L ug/L ug/L ' u'g7L ""' ug/L '" ug/L ug/L ug/L ug/L ...ug/L...... ug/L ug/L ug/L ug/L • ug/L " 'ug/L '-" ug/L ug/L ug/L ug/C 'ug/L ug/L ug/C ug/L ug/L ug/L "" ug"/L " ug/L ug/L ug/C ug/L ug/L ug/L '•ug7C'"' ug/L ug/L ug/L "ug/C"" ug/L ug/L ug/L ug/L ug/L ug/L _ LAB SAMPLE ID 0704036-01 0704036-01 0704036-01 "6"7"04636-0i 0704036-01 0704036-01 0704036-01 0704036-01 _ 070"4036-6i'" 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 ""6704636-0"i ' 0704036-01 0704036-01 0704036-01 6704636161 0704036-01 0704.036-01 6704636-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 0704036-01 '6704636-61 0704036-01 0704036-01_^ ' 0764036161 0704036-01 0704036-01 0704036-01 " o'765oi2loi" 0705012-01 0705012-01 6705612-61 0705012-01 6"765'6i2-6l 0705012-01 0705012-01 0705012-01 6765612-01 0705012-01 "6705612-61 ' 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 Dilution 1 1 " 1 "" 1 - 1 1 1 1 ... „7 ...ii i 1 1 1 1 I.,ZZ"'' '" "'"1 1 1 1 1 IZ- 1 i 1 1 1 1 '" 1 1 1 1 ""-" 1 1 ___i i 1 1 1 1 1 1 1 1 1 1 • i 1 1 1 T 1 1 1 1 " '1 _i| TB^ HYDRASLEEVE QA/QC SAMPLE RESULTS TRIP BLANKS • - • CONSTITUENT 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2-BUTANONE 2-CHLOROETHYLVINYL ETHER 2-CHLOROTOLUENE 2-HEXANONE 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE 4-METHYL-2-PENTANONE ACETONE BENZENE BROMOBENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON DISULFIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE CHLOROFORM CHCORbMETHANE CIS-1,2-DICHLOROETHENE CIS-1,3-bicHCoRbp"Rb'p'ENE DIBROMOCHLOROMETHANE DIBROMOMETHANE DICHLORODIFLUOROMETHANE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE m.p-XYLENE METHYLENE CHLORIDE NAPHTHALENE N-BUTYLBENZENE N-PROPYLBENZENE CJ-XYLENE SEC-BUTYLBENZiNE"! ""'" STYRENE TERT-BUTYLBENZENE TETRACHLOROETHENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE TRicHLbRbFLubRbMETHANE VINYL ACETATE VINYL CH'LORIDE WELL TB TB TB TB TB TB TB TB TB TB TB TB TB TB TIB ' 1 TB TB TB TB TB fs TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB TB __ T'B""' TB TB TB TB" SAMPLE* 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164 2164' 2164 2164 . 2164 _ 2164__ i''2i6'4""" 2164 2164 2164 2164 ...2164_ "2164'"' 2164 2164 2164 2164 SAMPLED DATE 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 64/25/2007 04/25/2007 04/2572667 04/25/2007 04/25/2007 04/25/2007 "64/2572067- 04/25/2007 04/25/2007 04/25/2007 04/25/2667 04/25/2007 64/2572067 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 04/25/2007 64/25/2667 04/25/2007 64/25/2OO7 04/25/2007 64/25/"2007 ^— CONC U U U U U U U U u u u u u .... -,y... u""" u. u u u u u u u u '~"'u u u u u u u 0 u u u u u "'"'LI u u u u u ,"LJI'""' u ' u u ..... ^....... EQL 10 10 10 10 10 10 10 10 10 10 100 10 10 10 '""16' v 10 10 10 10 10 io 10 10 10 ""16 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 16'"" 16 16 '•' 10 10 UNIT ug/C ug/L ug/L ug/L • ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/C ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L _.. U9/L "ug/C ' ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ' LAB SAMPLE ID 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705612-01 0705012-01 6705012-01 0705012-01 '0705612-61 0705012-01 67056112-61 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 0705012-01 _0705012-01 0705012-01 " 0705012-01 0705012-01 ' 0705012-01 0705012-01 0705012-01 "o7656i"2-oi'" 0705012-01 0705612-61" . O'705012-Oi "oTbsoil-o'i" 1 Dilution i 1 1 1 1 1 1 1 1 1 1 1 1 1 " "i 1 1 1 1 1 ,1 1 1 1 "'"1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 . 1 1 1 1 '1 . 1 1 1 1 TB-5 HYDRASLEEVE QA/QC SAMPLE RESULTS BLIND OUPLICATES CONSTITUENT 1,1,1,2-TETRACHLOROETHANE 1,1,1,2-TETRACHLOROETHANE i,i,i,2-TEfRACH'L6R6'EfHANE 1,1,1,2-TETRACHLOROETHANE 1,1,1-TRICHLOROETHANE 1,1,1-TRICHLOROETHANE 1,1,1-TRICHLOROETHANE 1,1,1 -TRICHLOROETHANE 1,1,2,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE 1,1,2,2-TETRACHLOROETHANE 1,1 ,2TTRICHL0R0ETHANE 1,1,2-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE 1,1-DICHLOROETHANE 1,1-DICHLOROETHANE 1,1-DICHLOROETHANE 1,1-DICHLOROETHANE . 1,1-DICHLOROETHENE 1,1-DICHLOROETHENE 1,1-DICHLOROETHENE 1,1-DICHLOROETHENE 1,1-DICHLOROPROPENE 1,1-DICHLOROPROPENE 1,1-DICHLOROPROPENE 1,1-D'lCHC6R0PRbPEN'E 1,2,3-TRICHLOROBENZENE- 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROBENZENE 1,2,3-TRICHLOROPROPANE 1.2,3-TRICHLOROPROPANE 1,2,3-TRICHLOROPROPANJ 1,2,3-T'RicHL6ROP'ROPANE " 1,2,4-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE ' 1,2,4-TRICHLOROBENZENE 1,2,4-TRII^ETHYLBENZENE 1,2,4-TRIMETHYLBENZENE 1,2,4-TRIMETHYLBENZENE 1,2,4-TRIMETHYLBENZENE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMO-3-CHLOROPROPANE 1,2-DIBROMOETHANE 1,2-DTBROMOETHAtiiE 1,2-DIBROMOETHANE 1,2-DIBROMOETHANE li2-DICHL"0R'6'BE'tJ'zENE 1,2-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1 iis-DICHLORbETH/VNE i ,'2-D'ICHLOROETH Atge 1 ."i-brCHLOROEf'HANE l|l ,2-Dlc'HLbROEf HANE WELL H-3HS H-3 HSD H-4 HS"~ " H-4 HSD H-3HS H-3 HSD H-4"HS H-4 HSD H-3HS H-3 HSD H-4HS H-4 HSD H-3H_S _ H-3HS"D H-4HS H-4 HSD H-3HS_ 1^-37160 H-4HS H-4 HSD H-3HS H-3JHSp_ H-T HS' H-4 HSD H-3HS H-3 HSD H-4HS H-4 HSD H-3HS H-3 HSD HTHS H-4 HSD H-3HS H-3 HSD H-4HS _ HT HSD" H-3HS H-3 HSD H-4HS H-4 HSD H-3HS H-3 HSD HTHS H'-4 HSD H-3HS H-3 HSD H-4HS H-4 HSD H-3HS H-3 HSD H-4HS H-4 HSD tiiis "HS" H-3 HSD H-THS H-4 HSD H"-'3H"S"""" H-3 HSD H-4HS H-4 HSD SAMPLE* 2189 _ 2190 ••"-'-2-192 2193 ""'2189 2190 2192 2193 2189" 2190 2192 2193 .21JL9.,_ "2190"' 2192 '2i93 2189 2190 2192 2193 2189 2190 2192 2193 2189 2190 2192 2193 2189 2190 2192 2193 2189 2190 2192 2193 2189 2190 2192 2193 2l"8"9 2190 2192 i2193 _2J89 "2196 2192 2193 2189 2190 2192 izi 93 2189 2190 2192 2193 2189 2190 2192 2193 LAB 4 4 ""4 .4 _ _ "4 4 '" 4 4 ""4 4 4 4 4 4 4 4 ,-....1. „ """4" 4 4 .4 _i...l ... 4 4 4 4 A""~ 4 4 4 _ _4_ __ .... - 4 4 4 ... ^ .... 4 4 4 4 4 4 4 4 . ..._1.. 4 4 4 4""" 4 4 4 4 .... .^.., . 4 4 4 4 4 SAMPLED DATE 05/10/2007 05/10/2007 "65/11/2607 05/11/2007 05/10/2007 05/10/2007 657i"i7i2667 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 65/11/2667 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 6'57ii/2067 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 j0_5/10/20p7 057il/2067' 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 CONC U U ' U __\i __ "-"u"" u u u u u u u u u u u u u u u u __u__ u u u u u u u u __ u" u u u '""u"'" u u : U u u u u u _u '""u u u u u u u u u '"' u"' U u u U u EQL 10 10 10 ' 10 "• io"" 10 16 10 """16"'" 10 10 10 _ 10_ '"10" 10 10" . 10 10 10 10 10 10 ' "T"o 10 10 "16 10 10 10 10 "i6~ 10 10 10 io . 10' 10 10 10 10 10 10 10 .... TP™.-... ^^„- 10 10 10 16" 10 16 16 10 "10 " 10 io __10 _ ""10"" 10 UNIT ug/L ug/L ug/L ug/L "ug/l" ug/L ug/L ug/L. ug/L ug/L ug/L ug/L ug/L "ug7L" HS/L ug/L _;.ug/L_ "ug'/'C" ug/L ug/L ug/L .. .'ig/.L... ug/L ug/L ug/L ..ug/L . ug/L ug/L ug/L ug/L ug/L ug/L " ... .yg/L... ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/C ug/L ug/L ug/L ug/L" ug/L ug/L ug/L „,"g,/L.. ug'/L ug/L ug/C ug/L ug7C" ug/L LAB SAMPLE ID 0705027-06 0705027-07 0705029-01 0705029-02 '0765027-66 0705027-07 0705029-01 0705029-02 0705027-06 0705027-07 0705029-01 0705029-02 0705027-06 0705027-07 0705029-01 6765629-02 0705027:06 '67656"2'7-07' 0705029-01 0705029-02 0705027-06 0705027-07 6705629-"6i 0705029-02 0705027-06 0705027-07 07"05"629-"6i 0705029-02 0705027-06 0705027-07 0705029-01 0705029-02 0705027-06 0705027-07 0705029-01 "07656'29-0'2 0705027-06 0705027-07 0705029-01 0705029-02 0705027.-06 0705027-07 6765029-01 0705029-02 0705027-06 6705027-07 0705029-01 0705029-02 0705027-06 0705027-07 0705029-01 0705029-02 0705027-06 07£5q27-q7 670562'9-6l 0705029-02 6765027-O6 0705027-07 0705029-01 0705029-02 Dilution 1 1 . 1 1 "i 1 1 1 ' i'" 1 1 1 ^_•• "1 1 i 1 i""'l 1 1 1 1 "" i 1 1 1 1 1 1 1 1 1 1 1 1 ..z. zz. 1 1 1 1 1 1 1 1 . 1 i"'"'" 1 1 „1 1 1 i 1 ... -„,. 1 1. 1 T"'"1 1 . 1 BD-1 HYDRASLEEVE QA/QC SAMPLE RESULTS BLIND OUPLICATES CONSTITUENT 1,2-DICHLOROPROPANE 1,2-piCHlXIROPRqPANE 1 ,21DICHL6R'6"P'R'6"P"AN"E 1,2-DICHLOROPROPANE 1,3,5-TRIMETHYLBENZENE , 1,3,5-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,3-'DiCHLORbBEN"zE"fgE 1,3-DicHLOROPROPANE 1.3-DICHLdRbPR6PAt«JE 1,3-DICHLOROPROPANE 1,3-DICHLOROPROPANE 1,4-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,4-DICHLOROBENZENE 2,2-DICHLOROPROPANE 2,2-DICHLOROPROPANE 2,2-DICHLOROPROPANE 2,2-DICHLOROPROPANE 2-BU"TANI6"NE 2-'BU"fA'N"6NE ' ---— 2-BUTANONE 2-BUTANONE 2-CHLOROETHYLVINYL ETHER 2-CHLOROETHYLVINYL ETHER 2-CHLOROETHYLVINYL ETHER 2-CHLOROETHYLVINYL ETHER 2-CHLOROfOLUENE 2-CHCoRofOLUENE p-'cHTLbRofbLUENE 2-CHLOROTOLUEhjE 2-HEiXAN6"tgE 2-HEXANONE 2-HEXAN'6'NE |2-HEXAtjbNE 4-CHLOROTOLUENE 4-CHLOROTOLUENE 4-CHLOROTOLUENE 4-CHLOROTOLUENE 4-ISOPROPYLTOLUENE 4-ISOPROPYLTOLUENE 4-ISOPROPYLTOLUENE 4-ISOPROPYLTOLUENE 4-METHYL-2-PENTANONE |4-METHYC2-PEf>ilf/^ti|ONE , |4-METHYL-2-PENfAN6fiJE M-l^'EfHYL-2-P"ENTANbNE |ACEf"bNE fcCEfONE kcETONE ACETONE ARSENIC ARSENIC URSENIIC [ARSENIC WELL H-3HS H-_3_HSp_ 'H'T'H'S"!" H-4 HSD H-3HS H-3 HSD H-4HS H-4 HSD H-3HS H-3 HSD H-4HS . H-4 HSD H-3HS H-3 HSD H-4HS H-4 HSD H-3HS H-3 HSD H-4HS H-4 HSD H-3HS H-3 HSD H-4HS H-4 HSD H;3_HS _ "H|i^3 HSD"' H-4HS H-4 HSD H-3HS H-3 HSD H-4HS H-4 HSD H-3HS H-3 HSD H-4HS H-4 HSD H-3HS H-3 HSD H^HS H-4 HSD H-3HS H-3 HSD H-4HS H-4 HSD H-3HS H-3 HSD H-4HS H-4 HSD H-3HS H-3 HSD H-4 HS H^HSD H-3HS H-3 HSD H-4HS H-4 HSD H-3HS H-3 HSD H-4HS H-4 HSO SAMPLE* 2189 2190 2192 2193 2189 2190 2192 2193 2189 .2190 2192 2193 2189 2190 2192 2193 ""• 2189 " 2190 2192 2193 2189 2190 2192 2193 2189 2190 2192 2193 2189 2190 2192 2193 2189 • 2190 2192 2193 2189 2190 2192 2193 2189 2190 2192 2193 2189 2190 2192 2193 2189 2190 2192 2193_ 2i89 2190 2192 2193 2189 2190 2192 2193 LAB 4 4 "" "4 "" 4 4 4 4 4 4 4 4_ 4 4 4 4 4 4 4 4 4 4 4 • 4 _ 4_ _ 4' "" 4 4 4 4 4 4 4 4 4 4 4 4 4 4 • 4 4 4 4 4 4 4 4 4 4 4 __4 ""'4""" 4 • 4 4 • 4 4 4 4 SAMPLED DATE 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 '057ii/2007' 05/10/2007 05/10/2007 05/11/2007 05/11/2007 '05/16/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 "05/'l0/'20"67 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/ii/26'67 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007^ 05/16/2067 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 CONC U U U U U U u u u u 'u'"" u u u u 'u"" u u u u u u u u ' u u u u u u u u u u u u u u u u u u u u u u u u u u _JJ_ .... ^ u u u u u u u EQL 10 ]0 '16 10 10 10 10 10 10 16 10 '""i'o"" 10 10 10 10 "10" 10 10 10 10 10 10 10 10 "i'o"" 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 _.JJD; "Too" ioo 100 ioo 100 100 100 100 UNIT v.ug/L ug/L 'ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ..-"g/L.. ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ...ug'L. ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L .. .yg'L,, ug/L ug/L ug'L ug/L ug/L ug/L ug/L ug/L LAB SAMPLE ID 0705027-06 q705q27-07_ 6705029-6T 0705029-02 0705027-06 0705027-07 0705029-01 0705029-02 0705027-06 0705027-07 07q5029-01_ 0705029-62' 0705027-06 0705027-07 0705029-01 0705029-02 '6705627-66' 0705027-07 0705029-01 0705029-02 0705027-06 0705027-07 0705029-01 0705029-02 0705027-06 0705"o"27i^o"7' 0705029-01 0705029-02 0705027-06 0705027-07 0705029-01 0705029-02 0705027-06 0705027-07 0705029-01 0705029-02 0705027-06 0705027-07 0705029-01 07056'29-02 0705027-06 0705027-07 0705029-01 0705029-02 0705027-06 0705027-07 0705029-01 0705029-02 0705027-06 0705027-07 0705029-01 0705029-02 0705'6"27-66' 6705027-07 0705029-01 0705629-02 0705027-06 0705027-07 0705029-01 0705029-02 Dilution 1 1, ... 1 1 1 1 1 1 1 .1... f" 1 1 „ . l... 1 i" 1 1 1 i 1 - 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 - 1 1 i 1 .. 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 BD-2 HYDRASLEEVE QAJQC SAMPLE RESULTS BLIND DUPLICATES CONSTITUENT BARIUM _ _ BARIUM ' "'""' " BARIUM BARIUM BENZENE BENZENE BENZENE BENZENE BROMOBENZENE BROMOBENZENE BROMOBENZENE BROMOBENZENE BR'0M"0CHL6R0MEfHi^NE" BROMOCHLORbMifH/SvNE BROMOCHLOROMETHANE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMODICHLOROMETHANE BROMODICHLOROMETHANE BROMODIC'HLOR'OMETHANE BROMOFORM BROMOFORM BROMOFORM BROMOFORM BROMO'METhWtgE BROMOMETHANE BROMOMETHANE BROMOMETHANE CADMIUM CADMIUM CADMIUM CADMIUM CARBON DISULFIDE CARBON DISULFIDE CARBON DISULFIDE CARBON DISULFIDE CARBON TETRACHLORIDE CARBON TETRACHLORIDE CARBONTETRACHLORIDE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROBENZENE CHLOROBENZENE CHLOROBENZENE CHLOROETHANE CHLOROETHANE CHLOROETHANE CHLOROETHANE CHLOROFORM CHLOROFORM CHLOROFORM _ CHCOROFORM" " ,"" CHLOROMETHANE CHLOROMEfHANE CHLORbMEfHANE CHLOROMETHANE CHRO'li/IIUM CHROMIUM CHROMIUM [CHROMIUM WELL H-3HS H-SIHSD' H-4HS H-4 HSD H-3HS H-3 HSD H-4HS H-4 HSD niisHS H-3 HSD H-4 "H'S"" H-'4"'H'sb' H-3HS' H-3 HSD H-4JHS_ H-4 HSD H-3HS H-3 HSD 'H-4HS 'H'-4H'SD" H-3HS H-3HSD H-4HS H-4 HSD H-3"HS" H-3 HSD H-4IHS H-4i"HSD' H-3HS H-3 HSD H-4HS H-4 HSD H-3HS H-3 HSD H-4HS H-4 HSD H-3HS H-3 HSD_ 'H-4HS" H-4 HSD H-3HS" H-3 HSD tMHs7_ H-4"HSD" H-3HS H-3 HSD H-4HS H-4 HSD H-3HS H-3 HSD H-4HS H-4 HSD" H-3HS H-3 HSD H-4HS H-4HSD_ 'H-3"HS H-3 HSD H-4HS H-4 HSD SAMPLE* 2189 2190 2192 2193 2189 2J90 2'i92 1" 2193 2189 2190 2192""" 2193__ _ ... ..„^^^ .... 2190 2192 2193 2189 2190 2192 "" 2J_93' ' 2"i89"'" 2190 2192 2193 2189 2190 2i9:2' 2193 2J89 2190 2192 2193 2189 2190 2192 2193 2189 2190 2192 2193 2189 2190 2192"' 2193 2189 2190 2192 2193 ' " 2189 2190 2192_ _ "~ "2193"""" 2189 2190 2192 2193 • 2'i'8"9' 2190 2192 2193 LAB ,- _.i. 1... ""'4" "' . 4 4 4 4 ...... 4 4 4 '7'_4^' 'Z..'*7." ...... ' 4 4 4 4 4 ' '4 ""' "4 4 4 4 '4 """ 4 4 ..... ^4___ 4 4 4 4"""" 4 4 4 J.___ ^ 4'""' 4 4 _ 4 • 7_4_,_7. 4 4 4 4_ _ 4"" 4 4 . 4_ "4"" 4 4 4 4 4 4 4 -1_, , SAMPLED DATE 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 65/10/'2667 05/10/2007 05/11/2007 05/11/2007 '65/io72o6i?'' 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 057ii7'26'07 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 65/11/2007 6"57ii/266'7" 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 65/16/2067 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2667 05/11/2007 05/10/2007 05/10/2007 "o"57i 1/2667 o"5/i 1/2667" 05/10/2007 05/10/2007 65/ii/:2"667 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/1_1/2007 CONC 274 —272"" 95.8 95.8 U U "u""" U u u ....z...... ".'0 "" u u _u "'"u" u u ZLI ^ u " u' u u u "ij" u u '" u u u u u u u u u u u "~"u'"" IJ u" u .... ^-.. u u u u u u u u u u u u _JJ u"" u 19: J _JJ EQL 10 " '16" 10 10 10 10 10 10 10 10 "•"•io" 10 10 io 10 10 10 10 z '" 10' 16"" 10 16 10 " •T6"" 10 16 10 5 "" 5""" 5 5 10 10 10 10 10 10 10 10 10 10 '""'fo 10 10 10 __10_ ""'io"~ 10 10 10 ""16 io'"' 10 •16 10 "•"56" 50 50 50 . UNIT . ..4.g/.L.. "ug/L" ug/L ug/L ug/L ug/L ug/L ug/L "ug/L ug/L _ug/L_ ug/L _ ug/L ug/L ug/L '"~Jg/L"" ug/L ug/L ug/L "'."g^L.7 ug/L ug/L ug/L _ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/C" "g/L . ug/L ug/L ug/L "ug'/L ' ug/L ug/L ug/L u'g7L ug/L ' ug/L ug/L ....Mg/.L_,. ug/L" ug/L ug/L .„i!.g/L... • ug/L """ug/L " ...ug/L... ug/L ug/L "" ug/L • ug/L ug/L ug/L LAB SAMPLE ID 0705027-06 0705027-07 0705029-01 0705029-02 0705027-06 0705027-07 "07'65"o"29"-01 0705029-02 0705027-06 0705027-07 076'502'9-"oi ioi7io75629^62^ 0705027-06" 6705027-07 0705029-01 0705029-02 0705027-06 0705027-07 0705029-6i 0705029-02 '6'76"5027-06 0705027-07 0705029-01 0705029-02 0705027-06 q7q5027-07 6705029-6i "0765029-02 0705027-06 •076502'7ii67 0705029-01 0705029-02 0705027-06 0705027-07 0705029-01 0705029-02 0705027-06 0705027-07 0705029-01 0705029-02 676502!7ii06 0705027-07 0705029-01 670"5029-0"2' 0705027-06 0705027-07 0705029-01 "676"502'9-62" 0705027-06 0705027-07 0705029-01 0765029-0"2" O765627-66 0705027-07 6765029-01 0705029-02 0705027-06 0705027-07 0705029-01 0705029-92 Dilution 1 1 1 1 1 1 i _ 1 'Z7.1777 .'77i".". """"i~ " i 1 .....1 1 1' ••• 177 "i ........... 1 1 _i____ ......... 1 1 i 1 ""• "1 1 1 1 1 1 1 1 1 ._ i, -' •1 1 1. [ 7 i "7. '1 ' 1 1 1 ""- '1 1 1 j____ i"i"i" i 1 1 1 1 1 1 1 1 BD-3 HYDRASLEEVE QA/QC SAMPLE RESULTS BLIND DUPLICATES 1 [IcONSTITUENT 1 CIS-1,2-DICHLbROETHENE CIS-1 ,"2-DICH"CbRbETH"ENE CIS-1,2-DICHLOROETHENE cis-1,2-DICHLbROETHENE CIS-i,3-biCHLOROPROPENE CIS-1,3iiDICHLORbPROPENE CIS-'l is-blCHCbROPROPEhJEi' i " CIs'-iiiJ-'biCHLORbPROP'EI^E' 7 DIBROMOCHLORbMEfHANE DIB'ROMbc'HLbRbMETHANE DIBROMOCHCbROMEfHANE pCBRbMbciiCbRbi^^ETHANE piBR"OMbMETHANE - piBROMOMETHANE blBROMOt/IETHAisiE i; 7„ ' DIB'RCIMOMEf HAI^E pi'CHLbRbDiFLUbROIkilETHANE piCHLbRbDiFLUbROMEfHANE ' DICHLORODIFLUOROMETHANE DICHLbRdDIFLUbROMETHANE ETHYLBEI^ZENE EfHY'CBENZENEi " "i ETHYLBENZENE EfHYLBEt^ZENE" HEXACHLbRbBiijfApiENE "7 HEXACHLbR"6"B'u'fA"D'iE't^"E " HEXACHLOROBUf ADIENE HEXACHLbRbBUT ADIENE ISOPROPYLBENZENE ISqPROPYLBENZENE rsbPROPYLBEtiiz'ENE ISOPROPYLBENZENE CE/vb'i LEAD , LEAD LEAD mip-XYLENE mip-XYLENEi_7 -.i.i ....7 i m','p-XYLENE' m,p-XYLENE MANGANESE MANGANESE MANGANE'SE " " MANGANESE MERCURY MERCURY MERCURY_ i ' ii7,.., ,ii7„„, i7 MERCURY" METHYLENE CHLORIDE METHYLENECHLORIDE METHYLENE CHCORIDE 7 i MEfHYCENEiCHLbRIDE7, [ Z " 7 NAPHTHALErgE """• """ " • NAPHfHALENE NAI'HTHALENE ii i i tvlAPHTHALENE N-BUjS'I.BEt^iZENE7_.i ' ,.,. i. tM-BUTYCBEf^'ZENE N-BUTYLBENZENE ' N-BUTYLBENZENE WELL H-3HS H-3'HSD 'H-4 HS H-4 HSpi H-3HS H-3 HSD H-4i'HS" ' H-4Hsb H-3HS H-3 HSD H-4HS 7 Hl'-i4"HS"b" H-3 HS H-3IHSD H-4HS H-4 inspi" H-3"HS' H-3Hsb H-4IHS HJHSb H-3ii'H^ i H-3"H'sb" H-tHS H-4Hsbi Hi:3HS 7 iH-3"HSb H-4HS" H-4 HSD H-3HS H-3'H"sb' H-4HS H-4 HSD H-3HS" H-3 HSoii 'H-4'tis""" H-4 HSD H-3 HS H-3 HSD in^HsJ, 'H-4 'HS'D HiiSHS H-3 HSD H-4HS 'H^ 'HSD' H-3HS H-3 HSD H-4HS Hiii HSD H-3 HS " H-3 HSD H-4JtS H;"4 HSb HI3 HS""" Hiii3HSb H:4HSi H-4 HSD H-_3 Hs" i H'-"3'HSD H-4HS IJ-4 HSb SAMPLE* 2189 • 2:, go"' _...,„.__^ - 2193 2189 2190 ..... ...^^.. ""2193 2189 .721967" '"2192"" 77,i2i9,3_ ' "2I897 2190" "•" 'iigii"' 7"„i2J9X"'i, '"""2"i89 "" 2190 ii" 2i92"7 "' 2193 .7. 2189","' "'2190 2192 2193 2i89 ' 2190 .ii;2i9i2ii i ii"2i'93ii'i' 2189_ iii"_7ii90_7 2i92~ 2193 "21897" "2190" 2192 2193 2189 7iii2J99__7' 2"i92 2193 2189 '2190 2i92 2193 2189 2190 '2192 . -.7219371 2189 2190 -2192 • 2193 "ii'sg"' 2190 2i927 7i2i93i_ '_2189iii 2190 2192 2193 LAB 4 ZiZi. i. '""4 "'" 4 4 .ii,i'*i ' i '74 ""4 4 ' "'"'4 "Z,i.Z". iii7 ,,4' 4 ..1... 4''" .............. 4 4- ..i.,...'*.i 7 ' '"4, '4 '4"' 7.4 ...Z... . 'i'"' 4 i '4 4 ii..iili" i " "4 4 ' 4 ....J.... 4" 4 4 iiiiilf i .iiiiiif... ii "4" -' ' f4 '4 .i....i 7. """"4" 4 .... 24 : '""4 47 4 4" 1. ... 4" ' 4 _ 4 '. i-li."' "4" • 4 4 SAMPLED DATE 05/10/2007 i65/i'9i/2667 "65'7ii72007 65/11/2607 "05/10/2007 05/10/2007 i957li/209i7^ ''oinviooj 65710/2667 65/10/2667 05/11^2067 "6'57ii/2667 65/10/2607 05/10/2067 65/ii;i2o67 65/11/2607 05/10/2007 05/10/2007 05/11/2007 iqs/i 1/2967 165/19/2607 "6'5/10'/20"07 65/ii/2O07 05/11/2907 i6'5/i67i29'o7 '6'57i6/2667 65/ii/:26o7 657iii/2q97 65/10/2667 '65/16/2607 05/11/2007 65/ii/2007 05/10/2007 65/10/i206'7"' 05/11/2007 05/11/2667 05/10/2007 65/i 0/2667 6"57i 1/2607 05/11/2007 05/10/2007 65/16/2067 057ii726o7 65711/2067 05/10/2007 q5/io/:26o7 65711/2067 057l 1/2007 05/10/2007 65/10/2607 05/'l1/2667 05/11/2967 O"57i6/200"7' 05/10/2007 05/11/2667 05/11/2007 O'S/10/2007 0'57l072007 65/11/2607 05/11/2607 CONC U 17 u i "• u u" uii Ui-'i ... ^ .. "" u u "u"' ilily ' """u " ' "u" _ u ... ^ 17.U • ""'u u 'u "' liiiy,. 77u "1 "u u _7.u "7iiu u u '7i„u u " 7u,„„i '"u"" u "4'li"J" ' 29i'j 31.J "u " "i'u u .1.1.6-8 ii.5 "64.9" 122" u" .... u u „7y.ii u 7u 1 u ily,' "" u u i.y Cl llu' u u u EQL 10 10" 10 10 " 16 " . .^^.. 1 ii617 " 16 16 "io" ZZ. jqil "io" io" 10 ..'io ""'10 io ' 10" il" JO ii 10" 10 .... .^... 7.10 1 10 " "10 10 •16 .1,19 7 ""'16'" 10" l..ip61 ioo' 160 "ili6 "io ""io" 5 '5 ._.. .5.... "5 '"" 1 1 1 11'1 " 1 10 10 10 io " io io 17.10.7 10 "1.10 ... ^^.. io" 10 UNIT "g/.L,. ug/'C' ug/L ug/L ug/L Hg/L., i ug/C" yg/Ci ug/L ug/C ug/L" ililug/C'l ug./L„, ug/L _.ug/L ug/C i....."g/L 1 i....".9',L„,l ug/C ug/L ,.™ug/Li i ug/L ug/L ug/C . "g/L_ ug/C"' ug/L ug/C i..."g/Li. ug/L i "g/L„, ug/L ug/L"' ...ygZC..,, ug/C ug/C iiii.ug/Lii ug/L ug/L • "g/L' ug/L ug/L ."g/Cl " ug/C" ug/L ug/L iig/L ug/C "g'L ug/L ug/Ci " u'g'/C ijjg/L'i ug/L ug/C ug/L ug/C"' ' ug/C .".g/L Hg/L LAB SAMPLE ID 0705027-06 q76'5'6'27-07 "o'765o':29-6i oii'95029-92 0705027-06 0705027-07 6765"6"2"9-6i" 0765029-62 0795027-66 0705027-07 6765629-61 p76"5629;92 07o5O27ii66 0765027-67 0705029-01 'q70'50"29-62 67050'2'7'66 0705027-07 0705029-01 "0765629-02 107q502'-/lci6 i97'9'5927-67' 6705629-Oi 076502"9-62' 070"5027-'66" 0705027-07 0705029-01 67'65029-62 0795627-96 67o'5627i-67 67'05029-6'i 0705029-62 6'70'5627"-66' 679l5027_-97 6765629-61 0705029-02 0705627-66 0765027-67 6765629iio'i 0705029-02 6765627-O6 6i7q"5027-07 076502"9ii6i 0765029-02 6705027-06 0705027-67 '0705'629-gi 6705029ii62 0705027-06 0705027-07 qfosqloloii "6705Q29ilo"2' 07"05027'-66 0705027-67 9705029-91 67'05029-O2 0705027'-'06 0765027-07 0705029-01 0705029-02 Dilution 1 'Zii 1 ""1 iZ"ii77" 1 '1 :.; : 1 1 1 1 .z ii'll'i" iil '1 " 1 '1 i7i7i ,71 ii 1 "1 ..7.1 -., 7,',i,71. l.i 1 1 .711 """"i. 1" 7'1, ,7 lli.. 1 ..iil 1, ZZ:i.i7.1 1 ""1 1 7.71 77 1 1 ll.7, li'l 7-1 .............. 1 i. 'iii' ........ 1 - BD^ HYDRASLEEVE QAyQC SAMPLE RESULTS BLIND DUPLICATES lr "•" [CONSTITUENT ltvi-PRbPYL"BEN"ZEI>il"E . N-PROPYLBENZENE N-PROPYLBENZENE N-PROPYLBENZENE O-XYLENE O-XYLENE O-XYLE"NE " ' "' " O-XYLENE PERCHLORAfE PERCHLORATE PERCHLORATE PERCHLORATE SEC-BUTYLBENZENE SEC-BUTYLBENZENE SEC-BUTYLBENZENE SEC-BUTYLBENZENE SILVER SILVER SILVER SILVER STYRENE STYRENE STYRENE STYRENE TERT-BUTYLBENZENE TERT-BUTYLBENZENE TERT-BUTYLBENZENE TERT-BUTYLBENZENE TETRACHLOROETHENE TETRACHLOROETHENE TETRACHLOROETHENE TETRACHLOROETHENE TIN TIN TIN TIN TOLUENE fOLUENE TOLUENE TOLUENE TRANS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE TRANS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE fRiCHLOROETHENE " " TRICHLOROETHENE TRICHLOROETHENE TRICHLOROETHENE TRICHLOROFLUOROMETHANE .[TRICHLOROFLUOROMETHANE rfRICHLOROFLUOROMETHANE ITRICHLOROFLUOROMETHANE piNYL ACETATE VINYL ACETATE VINYL ACETATE VINYL ACETATE VINYL CHLORIDE K/lKlYL 'C'HLORlbE MNYL CHLOi=!lbE [VINYL-C'H'LORID'E WELL H-3HS H-3 HSD H-4HS H-4 HSD H-3 HS, H-3 HSD H-4HS. H-4 HSD H-3HS H-3 HSD H-4HS Hr4HSD H-3HS tiiis HSD H-4HS H-"4 HSD H-3HS H-3 HSD H-4HS H'-4 HS_D_ H'-3 HS H-3 HSD H-4HS H-4 HSD H-3HS H-3 HSD H-4HS 'H-4 HSD H-3HS H-i3 HSD H-4HS H-4 HSD H-3HS H-3 HSD H-4HS H-4 HSD H-3HS H-3 HSD' H-4HS H-4 HSD H-3HS H-3 HSD H-4HS H-4 HSD H-3HS H-3 HSD H-4 HS H-4 HSD H-3HS H-3 HSD H-4HS 1^-4 HSD ' H-3HS H-3 HSD H-4HS H-4 HSD 'H-3 H'S""" H-3 HSD H-4HS H-4 HSD H-3HS H-3 HSD H-4HS H-4 HSD : SAMPLE* 2189 2190 2192 2193 2189 21?Q__ 2'i"92 2193 2189" 2190 2192 2193 2189 '2196 2192 219:3^_ 2189 " . 2190 :2i92 2193 2189 2190 2192 2"i93 2189 2190 2192 ""2193""' 2189 2190 2192 2193 2189 2190 2192 2193 2189 ' "'2"l96 "~ 2192 2193 2189 2190 2192 '2i93 2189 2190 i2192 2193 2189 2190 2192 '" 2193""" 2189 2190 2192 2193 2189 2190 2192 2193 2189 2190 2192 •"" "2i93"~" LAB 4 4 4 4 4 4 4 4 4 4 .___4 ' 4 '"" 4 4 4 4 4 -•"• 4 "4""' ' 4 4 4 4 4 . 4 4 4 4 4 4 """"4 4 4 4 4 4~" 4 '4'-'- ',••'4—" 4 4 4 4 4 4 4 4 4 4 4 "" 4 4 4 4 4 4 4 ... ..^ 4 4 4 4 ........ SAMPLED DATE 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 O57i6/2607 05/10/2007 05/11/2007 05/11/2007 05/10/2007 65/10/2667 05/11/2007 05/11/2007 05/10/2007. 05/10/2007 o"57ii/"26'o'7 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 0'57-i"0/26"O7 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 6571672067 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 05/10/2007 •65/"l 0/2007" 05/11/2007 05/11/2007 65/id/26'6'i?' 05/10/2007 05/11/2007 05/11/2007 05/10/2007 05/10/2007 05/11/2007 05/11/2007 CONC "u u u u u u u u u u 41.4 36.9 u "u u u u u U __ u^ ""ul"" u u u u • u u u u u u U u u u u 1.1 J- 1.5 J "ii6 J" 2.2 J U u u """u"" u u " 'u u u u u '" "u"" u "'""u""' u u u u' u u u u ""u"".' EQL 10 10 10 10 10 10 16""" 10 "20 20 _ 10_ "' 16' 10 io 10 10 _ ""•5' " 5 5 "' 5 10 10 10 10 10 10 10 10 10 "10 16 •10 150 150 150 •^56" 10 """10 10 10 10 10 10 ""io' • 10 16 10 16 10 10 •""io" ' 10 . ...... 10 10 10 10 10 10 10 10 UNIT ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/ll ug/L .-.yg/L... ug/L ug/L ug/C ug/L ....".g'k... ug/C . ug/L ug/L ug/L ug/L' ug/L ug/L ug/L ug/L ug/L „ug/L ug/ll " ug/L ug/ll 'ug/L' ug/L ug/L ug/L ...ML... ug/C ug/L ._.".g/L.. ug/L ug/L ug/L ug/L ug/L " ug7L"" ug/L ug/L " ug/L ug/L ug/L ug/L „.ug'L 'u'g/L' _.yg/L_.. ug/C ' ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/C" LAB SAMPLE ID 0705027-06 0705027-07 0705029-01 0705029-02 0705027-06 0705027-07 "676'562"9-6"i 0705029-02 6765027-O6 0705027-07 0705029-01 0705029-02 0705027-06 0765627-67 0705029-01 0705029-02 0705027-66 0705027-07 i6765629ii6i 0705029-02 "6765027i-"66 0705027-07 0705029-01 0705029-02 0705027-06 0705027-07 0705029-01 676'5029-0"2" 0705027-06 6-^0"5027-67 "0765b29-"6i 0705029-02 0705027-06 0705027-07 0705029-01 0705029-02 0705027-06 0705b2ii''-'07 67o5629i:oi' 0765029-02 0705027-06 0705027-07 0705029-01 "07650'29ii02' 0705027-06 6765627ii67 0705629-01" 0705029-02 0705027-06 0705027-07 0705029-01 0705029-02 0705027-06 0705027-07 0705029-01 0705029-02 0705027-06 0705027-07 •b76'5'6'29-6'l 0705029-02 0705027-06 0705027-07 0705029-01 0705029-02 Dilution 1 1 1 1 1 1 1 .1. . 5 5 _2.5 2.5!" 1 - '" il 1 1 "i 1 'i • 1 'i •-1 1 1 1 1 1 '""•i " 1 1 1 '-•'- 1- 1 1 1 1 1 ' 1 1 1 1 .... .^. 1 1 '1 1 '1 - 1 1 1 .... 1 1 1 '""'"1" - 1 1 1 1 1"" m m m BD-5 HYDRASLEEVE QA/QC SAMPLE RESULTS BLIND DUPLICATES - CONSTITUENT ZINC ZINC ZINC ZINC WELL H-3HS H-3 HSD H-4HS H-4 HSD SAMPLE* 2189 2190 2192 • 2193 LAB 4 4 4 4 SAMPLED DATE 05/10/2007 05/10/2007, 05/11/2007 05/11/2007 CONC 12. J U 21.J II.J EQL 50 50 50 50 UNIT ug/L ug/L ug/L ug/L LAB SAMPLE ID 0705027-06 0705027-07 0705029-01 0705029-02 Dilution "i 1 1 ' BD-6