DSHW-2006-005755 - 0901a06880157096

Launch Systems Group
P.O. Box 707
Brigham City, UT 84302
www.atk.com
6 October 2006
8200-FY06-057
Mr. Dennis R. Downs, Executive Secretary
State of Utah
Department of Environmental Quality
Division of Solid and Hazardous Waste
288 N. 1460 W.
P.O. Box 144880
Salt Lake City, Utah 84114-4880
Dear Mr. Downs
ATTENTION: Jeff Vandel
Subject: Semi-Annual RFI Progress Report
0(^.0 330 f
OCT 1 1 2008
SOLID & HAZARDOUS WASTE
As required by Section VllH of Thiokol Corporation's Post Closure Permit, the following semi-annual RFI
progress report is submitted for your review. The reporting period covered by this report is 1 March 2006 - 1
September 2006.
This report contains details on two new SWMU's and the pilot lest for perchlorate in soil biotreatment.
If you have any questions regarding this report, please direct them to Paul Hancock at [phone].
Sincerely
David P. Gosen, P.E., Director
Environmental Services
c: Walter L. Baker, Director, Division of Water Quality
SEMI-ANNUAL RFI PROGRESS REPORT
1 March 2006 -1 September 2006
ATK Thiokol Promontory Facility
1. Description and estimation of the percentage of the RCRA Facilities
Investigation completed
Two new sites are being added to the SWMU list, these are two septic tank drain
fields in the Plant 3 facility, SWMU #678, M-201 septic tank drain field and
SWMU #679, M-205 septic tank drain field. The addition of these new SWMUs
is a result of increasing contamination levels in the water supply well in Plant 3
Well 3A. As described in previous correspondence with the DSHW,
Trichloroethylene (TCE) and perchlorate have been detected in the well. The
well is not a drinking water source and signs are posted that it is not to be used for
dinking water. Both of the drain fields are domestic systems only with two hand
washing sinks, and two showers and toilets connected to M-201 and two toilets
and hand washing sinks being connected to M-205. ATK is developing a
treatment system to address the contamination which will be detailed in a
forthcoming letter.
Pilot test for Treatment of Perchlorate Contaminated Soils.
As described in the September 2005 RFI semiannual report, a perchlorate in soil
treatment pilot test was started. This soil was the result of the cleanup of
perchlorate spills including SWMU 677. The DSHW approved the test plan
entitled Work Plan For a Con-ective-Measure Pilot Test to Evaluate Ex-Situ
Remediation of Perchlorate-Contaminated Soil, September 2005. The bio-piles
have not appeared to have gone anaerobic at this point as perchlorate degradation
has been minimal. ATK has been investigating the mixing of additional simple
sugar electron donors into the piles to enhance the biologic action and drive the
piles anaerobic. More details will be provided to the Division prior to addition of
the new amendment.
2. Summaries of all fmdings
The Septic tanks for M-201 and M-205 were sampled and the results are attached.
These results indicate that perchlorate is degraded in the septic tanks in addition
to some TCE degradation.
A risk assessment was performed for human health exposures to TCE and
perchlorate under the water use exposure scenarios at Plant 3. The results of the
risk assessment demonstrate that the current levels are protective of human heath.
A copy of the risk assessment is attached.
3. Summaries of all changes made in the RCRA Facility Investigation during
the reporting period
The ongoing implementation of the perchlorate contaminated soil treatment pilot
test. Two additional SWMU's, #678 and #679 were added to the SWMU list.
4. Summaries of all contact with representatives of the local community, public
interest groups or State Government during the reporting period
Correspondence regarding RFI activities has been limited to the Division of Solid
and Hazardous Waste and the Division of Water quality.
5. Summaries of all problems or potential problems encountered during the
reporting period
There were no significant problems encountered during the reporting period.
6. Actions taken to rectify problems
Thiokol continues to review all available information and pursue all avenues
to resolve any uncertainty associated with the solid waste management units.
7. Changes in personnel during the reporting period
There are no changes in personnel. The existing environmental staff will continue
to conduct the sampling when possible. Contractors will be used when
specialized equipment is required.
8. Projected work for the next reporting period
Efforts for the next reporting period will focus on receiving approval for
voluntary corrective measures, investigating additional solid waste management
units, and report preparation. The perchlorate contaminated soil bio-remediation
pilot test will be ongoing through the next reporting period.
9. Copies of daily reports, inspection reports, laboratory and monitoring data
Results of the analysis of the M-205 and M-201 septic tank samples and the Well
3A water use Human Health Risk Assessment report are included as an
attachment.
M-201 and M-205 Septic Tank Sampling Results
3S
Thursday, April 06, 2006
CERTIFiCATI
>ample
TESTED FOR: ATK Thiokol: DLV
Environmental Monitoring
Thiokol Corp, UT 84322
ANALYZED BY: ATK Thiokol Propulsion
Environmental Laboratory
P.O. Box 707, IVl/S 245
Brigham City, UT
84302-0707
435-863-3732
435-863-8080
Contact Name:
Project:
Sample Delivery Group:
Dave Covington
Misc. Environmental Testing - DLV
0603035
Page 1 of 7
ENVIRONMENTAL LAB WORK REQUEST fiQ.0'b<^'^'5
TO THIOKOL ENVIRONMENTAL LABORATORY
Dave Covington
ORGANIZATION:
Environmental Services
nXTENSION:
3898
MAIL STOP.
301
-—'—^— 1
LWR No, E12621
Login No.
COSTCE.NTER:
8200
WOKK ORDER:
984P-LS333
DATi;:
3-30-06
RP.PORTRKSULTSTO.
HELEN RAVSTEN, MS 301
SAMPLE INFORMATION
SAMPLE
1
2
9.
10.
DATK
3-30-06
3-30-06
TYl'L
G
X
C
LOCATION
M-201 Septic
tank
M-205 Septic
tank
TIME
4^736
TKST
VOCs CLO4
VOCs CLO4
RE.MARKS
CHAIN OF CUSTODY
lUiLINQUISHKU ItY
/ ^-^^>>^
"^
OATE
J-^-^^
TIME
/^.'^r
KECEIVED BY
y/iji,^
DATE TIME
lY^/^
'=. ==^r: 1
FOR LABORATORY USE ONLY
DATE COMl'LEIED DATB REPORTHI) SIGNATUKH
Sample Delivery Group: 0603035
Sample No. Client No.
Test Requested
! 0603035-01 M-201 Septic Tank
EPA 314.0
SW-846, 8260B (Water)
; 0603035-02 1^-205 Septic Tank
EPA 314.0
SW-846, 8260B (Water)
Certified By; Signature valid '
Sample Description
Perchlorate - Ion Chromalography
Volatile Organics Appendix 9
Perchlorate - Ion Chromatography
Volatile Organics Appendix 9
%M'^j^
Received Collect Date/Time
Matrix
03/30/06 3/30/2006 13:20:19 j
Water
Water
03/30/06 3/30/2006 13:35:51
1
Water
Water
04/07/2006
W. Scott Fraser, Quality Assurance Officer Date
This certifies that ihe following data meets the requirements of the National Environmental Laboratory Accreditation
Program (NELAP) unless otherwise annotated:
Page 2 of 7
Listing of Results by Sample
Sample Delivery Group: 0603035
Client Sample ID: M-201 Septic Tank
Sample Description: ATK-DLV - Septic Tank Samples
Laboratory Sample ID: 0603035-01
Date Sampled: 03/30/06 13:20
CAS Number
• Test Metiiod:
014797-73-0
: Test Method:
67-64-1
107-02-8
107-13-1
107-05-1
71-43-2
108-86-1
7'l-y7-5
75-27-4
75-25-2
74-83-9
71-36-3
78-93-3
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
126-99-8
95-49-8
100-43-4
108-94-1
9G-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-34-3
107-06-2
75-35-4
156-59-4
75-71-8
78-37-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
141-78-6
100-41-4
60-29-7
97-63-2
76-13-1
Test Parameter
EPA 314.0 "perchlorate - Ion'
PERCHLORATE
SW.846, 8260B (Water) VolatileOrganics
ACETONE
ACROLEIt^J
ACI^YLONITRILE
ALLYL CHLORIDE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
1-BUTANOL
2-BUTANONE
SEC-BUTYLBENZENE
TERT-BUTYLBENZENE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
2-CHLOROETHYLVINYL ETHER
CHLOROFORM
CHIOROMETHANE
CHLOROPRENE {2-CHL0R0-1,3-BUTADII
2-CHLOROTOLUENE
4-CHLOROTOLUENE
CYCLOHEXANONE
1,2-DIBROMO-3-CHLOROPROPANE
DIBROMOCHLOROMETHANE
1,2-DIBROMOETHANE
DIBROMOMETHANE
1,2-DICHLOROBENZENE
1 ,3-D;CHLOROBENZENE
1,4-DICHLOROBENZENE
1,1-DICHLOROETHANE
1,2-DICHLOROETHANE
1,1-DICHLOROETHENE
CIS-1,2-DICHLOROETHENE
DICHLORODIFLUOROMETHANE
1,2-DICHLOROPROPANE
1,3-DICHLOROPROPANE
2,Z-DICHL0R0PR0PANE
1,1-DICHLOROPROPENE
CIS-1,3-DICHLOROPROPENE
TRANS-1,3-DICHLOROPROPENE
ETHYL ACETATE
ETHYLBENZENE
ETHYL ETHER
ETHYL METHACRYLATE
1,1,2-TRICHLORO-1,2,2-TRIFLUOROETH/
Result
Chromalography
U
Appendix 9
U
U
U
U
U
U
u
u
u
u
u
16.5
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
24.8
u
u
u
u
55.0
U
U
U
U
U
U
u
u
u
u
u
u
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
MDL
...—........ .
1
30
4.65
16
0.5
0.22
0.37
0.31
0.19
0.42
0.57
5.2
1.11
0.16
0.2
0.13
0.27
0.16
0.35
1.71
0.3
0.81
0.9
0.24
0.15
1.56
0.35
0.18
0.15
0.25
5.86
5.62
5.88
0.49
0.29
0.16
0.16
0.66
0.16
0.24
0.9
0.17
0.4
0.18
0.03
0.16
0.2
0.19
1
Dilu
EQL Fac
•-"-' - •••
4
100
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 A
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
tion
:for Analyst
- -- • ~ —
1 CA
1 LSH
1 LSH
1 LSH
1 LSH
1 LSH
1 LSH
1 LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
Test Date
-• —
04/04/06
1
04/03/06
04/03/05
04/03/06
04/03/06
0-1/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/05
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/05
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/05
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
Page 3 of 7
Listing of Results by Sample
Sample Delivery Group: 0603035
j Client Sample ID: M-201 Septic Tank
Sample Descr
CAS Number
Test Method:
87-68-3
591-78-6
67-63-0
98-82-8
108-10-1
78-83-1
79-46-9
99-87-6
126-98-7
74-88-4
80-62-6
75-09-2
104-51-8
103-65-1
91-20-3
107-12-0
100-42-5
156-60-5
110-57-6
108-88-3
630-20-6
79-34-5
127-18-4
87-61-6
120-82-1
79-00-5
79-01-6
71-55-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
95-47-6
460-00-4
1868-53-7
17060-07-0
2037-26-5
ption: ATK-DLV - Septic Tank Samples
Test Parameter
SW-846, 8260B (Water) Volatile Organics
HEXACHLOROBUTADIENE
2-HEXANONE
ISOPROPYL ALCOHOL
ISOPROPYLBENZENE
4-METHYL-2-PENTANONE
2-METHYL-1-PR0PAN0L (ISOSUTYL ALC
2-NITROPROPANE
4-ISOPROPYLTOLUENE
METHACRYLOt^lTRILE
METHYL IODIDE
METHYL METHACRYLATE
METHYLENE CHLORIDE
N-BUTYLDENZENE
N-PROPYLBENZENE
NAPHTHALENE
PROPIONITRILE
STYRENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,4-DICHLORO-2-BUTENE
TOLUENE
1,1,1,2-TETRACHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE
1,2,3-TRICHLOROBENZENE
1,2,4-TRICHLOROBENZENE
1,1,2-TRICHLOROETHANE
TRICHLOROETHENE
1,1,1-TRICHLOROETHANE
TRICHLOROFLUOROMETHANE
1,2,3-TRICHLOROPROPANE
1,2,4-TRIMETHYLBENZENE
1,3,5-TRIMETHYLBENZENE
VINYL ACETATE
VINYL CHLORIDE
m,p-XYLENE
o-XYLENE
BROMOFLUOROBENZENE
DIBROMOFLUOROMETHANE
1,2-DICHLOROETHANE-D4
T0LUENE-D8
Result
Appendix 9
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
2.2 J
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
101
100
101
99.1
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
MDL
0.9
0.7
3
0.58
0.53
5.33
0.99
0.24
0.39
0.21
0.49
0.77
0.3
0.15
4
0.39
0.17
0.34
0.65
0.21
0.25
0.85
0.28
0.23
4.37
0.25
0.71
0.16
0.25
0.33
0.19
0.29
0.13
0.3
1.6
0.18
Laboratory Sample ID: 0603035-01
Dafe Sampled: 03/30/06 13:20
Dilution
EQL Factor Analyst
• " ••• -
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
10 1 LSH
1 LSH
1 LSH
1 LSH
1 LSH
Test Date
—— ... 1
04/03/05
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/05
04/03/05
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/05
04/03/05
04/03/06
04/03/06
04/03/06
04/03/05
04/03/05
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
Client Sample ID: M-205 Septic Tank
Sample Description: ATK-DLV - Septic Tank Samples
Laboratory Sample ID: 0603035-02
Date Sampled: 03/30/06 13:35
CAS Number
: fes( Method:
014797-73-0
Test Parameter
'WA 314.6'~_
PERCHLORATE
Result Units
Perchlorate - Ion Chromalography
U ug/L
MDL EQL
Dilution
Factor Analyst Test Date
CA 04/04/05
Page 4 of 7
Listing of Results by Sample
Sample Delivery Group: 0603035
Client Sample ID: M-205 Septic Tank
Sample Description; ATK-DLV - Septic Tank Samples
Laboratory Sample ID: 0603035-02
Date Sampled: 03/30/06 13:35
CAS Number
r Test Method:
67-64-1
107-02-8
107-13-1
107-05-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
71-36-3
78-93-3
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
126-99-8
95-49-8
106-43-4
108-94-1
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
105-46-7
75-34-3
107-06-2
75-35-4
156-59-4
75-71-a
78-87-5
142-28-9
590-20-7
563-58-0
10061-01-5
10061-02-6
141-78-5
100-41-4
60-29-7
97-63-2
76-13-1
87-68-3
591-78-6
67-63-0
Test Parameter
SW-846, 8260B (Water) Volatile Organics
ACETONE
ACROLEIN
ACRYLONITRILE
ALLYL CHLORIDE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
1-BUTANOL
2-BUTANONE
SEC-BUTYLBENZENE
TERT-BUTYLBENZENE
CARBON DISULFIDE
CARBON Tt 1KACHLORIDE
CHLOROBENZENE
CHLOROETHANE
2-CHLOROETHYLVINYL ETHER
CHLOROFORM
CHLOROMETHANE
CHLOROPRENE (2-CHL0R0-1,3-BUTADII
2-CHLOROTOLUENE
4-CHLOROTOLUENE
CYCLOHEXANONE
1,2-DIBROMO-3-CHLOROPROPANE
DIBROMOCHLOROMETHANE
I,2-D:BROMOETHANE
DIBROMOMETHANE
1 ,2-D:CHLOROBENZENE
1 ,3-D;CHLOROBENZENE
I,4-D;CHLOROBENZENE
1,1 -DICHLOROETHANE
1,2-DICHLOROETHANE
1,1-DICHLOROETHENE
CIS-1,2-DICHLOROETHENE
DICHLORODIFLUOROMETHANE
1.2-DICHLOROPROPANE
1 ,3-D;CHLOROPROPANE
2.2-DICHLOROPROPANE
1,1-DICHLOROPROPENE
CIS-1 ,3-D:CHLOROPROPENE
TRANS-1 ,3-DICHLOROPROPENE
ETHYL ACETATE
ETHYLBENZENE
ETHYL ETHER
ETHYL METHACRYLATE
1,1,2-TRICHL0R0-1,2,2-TRlFLUOROETH/
HEXACHLOROBUTADIENE
2-HEXANONE
ISOPROPYL ALCOHOL
Result
Appendix 9
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
0]=
30
4.65
16
0.5
0.22
0.37
0.31
0.19
0.42
0.57
5.2
1.11
0.16
0.2
0.13
0.27
0.16
0.35
1.71
0.3
0.81
0.9
0.24
0.15
1.56
0.35
0.18
0.15
0.25
5.86
5.62
5.88
0.49
0.29
0.16
0.16
0.66
0.16
0.24
0.9
0.17
0.4
0.18
0.63
0.16
0.2
0.19
1
0.9
0.7
3
Dilu
EQL Fac
100
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10
10 1
10 1
10
10
10 1
10 1
10 1
10
10 1
10 1
10
10
10
10
10 1
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
tion
tor Analyst
..
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
Test Date
._ j
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/05
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/05
04/03/05
04/03/05
04/03/05
04/03/06
04/03/05
04/03/05
04/03/05
04/03/06
04/03/06
04/03/05
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
Page 5 of 7
Listing of Results by Sample
Sample Delivery Group: 0603035
Client Sample ID: M-205 Septic Tank
Sample Description: ATK-DLV - Septic Tank Samples
Laboratory Sample ID: 0603035-02
Date Sampled: 03/30/06 13:35
CAS Number
•' Test Meihod:'"
98-82-8
108-10-1
78-83-1
79-45-9
99-87-6
126-98-7
74-88-4
80-52-6
75-09-2
104-51-8
103-65-1
91-20-3
107-12-0
100-42-5
156-60-5
110-57-6
108-88-3
630-20-5
79-34-5
127-18-4
87:61-6
120-82-1
79-00-5
79-01-5
71-55-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
95-47-6
460-00-4
1868-53-7
17060-07-0
2037-26-5
Test Parameter
SW-S46, 82606 (Water) Volatile Organics
ISOPROPYLBENZENE
4-METHYL-2-PeNTANONE
2-METHYL-1-PR0PAN0L (ISOBUTYL ALC
2-NITROPROPANE
4-ISOPROPYLTOLUENE
METHACRYLONITRILE
METHYL IODIDE
METHYL METHACRYLATE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
PROPIONITRILE
STYRENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,4-DICHLORO-2-BUTENE
TOLUENE
1,1,1,2-TETRACHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE
1,2,3-TRICHLOROBENZENE
1,2,4-TRICHLOROBENZENE
1,1,2-TRICHLOROETHANE
TRICHLOROETHENE
1,1.1-TRICHLOROETHANE
TRICHLOROFLUOROMETHANE
1,2,3-TRICHLOROPROPANE
1,2,4-TRIMETHYLBENZENE
1,3,5-TRIMETHYLBENZENE
VINYL ACETATE
VINYL CHLORIDE
m,p-XYLENE
O-XYLENE
BROMOFLUOROBENZENE
DIBROMOFLUOROMETHANE
1,2-DICHLOROETHANE-D4
T0LUENE-D8
Result
Appendix 9
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
6.3 J
u
u
u
u
u
u
u
u
u
101
100
100
99.2
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugfL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
MDL
0.58
0.53
5.33
0.99
0.24
0.39
0.21
0.49
0.77
0.3
0.15
4
0.39
0.17
0.34
0.55
0.21
0.25
0.85
0.28
0.23
4.37
0.25
0.71
0.16
0.25
0.33
0.19
0.29
0.13
0.3
1.6
0.18
Dilu
EQL Fac
•—
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10
10
10
10 1
10 1
10 1
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
tion
tor Analyst
•*"' — "'• • "•
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
Test Date
.. ... „
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/Oe
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/05
04/03/06
04/03/05
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/06
04/03/05
04/03/06
04/03/06
04/03/05
Page 6 Of 7
Data Reporting Qualifiers
Indicates ttiat tlie analyte was not detected, or the anaiyte was detected but
was below the MDL.
This flag Is used when an analyte is found in the blank as well as the sample.
Indicates an extimated value. This flag is used either when estimating a concentration
for tentatively identified compounds or when the data indicated the presence of a
compound that meets the identification criteria but the result is less than the
EQL (e.g, 3 J with an EQL of 10).
MDL Method Detection Limit: The minimum concentration of a substance that can be
confidently measured and reported. The laboratory has demonstrated that the
MDL can be achieved in a laboratory reagent blank, but does not guarantee it
can be achieved in all sample matrices.
EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For
many analytes the EQL is selected as the value of the lowest standard in the
calibration curve.
Dilution Dilution Factor: The prepared sample was diluted by this factor because the
Factor sample was too concentrated or due to other interferences in the sample matrix.
Any dilution factor causes a corresponding increase in the MDL and EQL.
Page 7 of 7