DSHW-2005-002640 - 0901a0688013e042

HAND DELIVERED
DEC 1 li 2005
SOLID & HAZARDOUS WASTE
RESULTS OF POST-EXCAVATION SAMPLING
AT M-39 AND M-636
ATK THIOKOL, INC.
Promontory, Utah
Revised
October 2005
Prepared by ——- —^
EARTHFAX ENGINEERING, INC. ^1^^
Engineers/Scientists i^^^A
Midvale, Utah ^"^I^
www.earthfax.com CSiVVt\iSiX.
ATK Thiokol, Inc. . Results of M-39 and M-636 Sampling
Promontory, Utah October 2005
TABLE OF CONTENTS
Section Paqe
CHAPTER 1 -INTRODUCTION 1
CHAPTER 2 - HUMAN-HEALTH AND ECOLOGICAL RISK 2
2.1 SOIL TO GROUNDWATER MIGRATION PATHWAY 2
2.2 HUMAN-HEALTH RISK 3
2.3 ECOLOGICAL RISK 4
CHAPTER 3 - RESULTS AND DISCUSSION 6
3.1 SAMPLING AND ANALYSIS METHODS 6
3.2 ANALYTICAL RESULTS 6
3.2.1 M-39 6
3.2.2 M-636 .7
3.2.3 Potential for Migration to Groundwater 8
3.2.4 Quality Assurance Samples 8
CHAPTER4 - POST-CLOSURE PLANS 13
CHAPTER 3 - REFERENCES 14
EarthFax Engineering, Inc.
ATK Thiokol, Inc. Results of M-39 and M-636 Sampling
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LIST OF TABLES
Table Paqe
2-1. Human Health Remediation Goals for the M-39 and M-636 Sites 5
2-2. Ecological Soil Screening Levels for Cadmium 5
3-1. Results of M-39 Soil Chemical Analyses 10
3-2. Results of M-636 Soil Analyses 11
3-3. Results of Duplicate Sample Analyses 12
LIST OF APPENDICES
A - Results of Soil Chemical Analyses
B - Field Notes
C - Results of Soil Gas Analyses
LIST OF PLATES
3-1. M-39 Soil Sample Locations
3-2. M-636 Soil Sample Locations
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ATK Thiokol, Inc. Results of M-39 and M-636 Sampling
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RESULTS OF POST-EXCAVATION SAMPLING
AT M-39 AND M-363
CHAPTER 1
INTRODUCTION
Between 1962 and 1982, ATK Thiokol, Inc. ("Thiokol," formerly Thiokol Corporation)
discharged X-ray film development wastewater into shallow ditches adjacent to buiidings M-39
and M-636 at their Promontory, Utah facility. Impacted soil at these sites were subsequently
sampled, excavated, and disposed of off site in 1995. Following the collection of confirmatory
samples, additional soil was excavated in specific areas to meet remediation goals (Thiokol,
1996).
The Utah Department of Environmental Quality, Division of Solid and Hazardous Waste
("the Division") reviewed the data collected from the sites, following re-excavation, and
recommended additional sampling to determine ifthe site met the requirements of R315-101.
Thiokol agreed with these recommendations and submitted a sampling and analysis plan to the
Division (EarthFax Engineering, 2003). This plan was subsequently approved by the Division.
The purpose of this current document is to:
• Present the results of the final confirmatory sampling at M-39 and M-636,
• Discuss human-health and ecological risk associated with residual contamination at the
sites, and
• Discuss the potential for migration of metals contamination from soil to groundwater at
the sites.
A discussion of human-health and ecological risk is presented in Chapter 2, together with an
evaluation of the potential for residual metals contamination at the sites to migrate from the soil
to groundwater. This is followed by the results of sample analyses in Chapter 3 and a
discussion of post-closure plans in Chapter 4. References cited herein are listed in Chapter 5.
1 EarthFax Engineering, Inc.
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Promontory, Utah October 2005
CHAPTER 2
HUMAN-HEALTH AND ECOLOGICAL RISK
2.1 SOIL TO GROUNDWATER MIGRATION PATHWAY
The project sampling and analysis plan (EarthFax Engineering, 2003) identified
cadmium, perchlorate, and silver as the inorganic contaminants of potential concern. Three
methods of analysis were presented in that plan to show that no significant potential exists for
residual metals contamination at M-39 and M-636 to leach from soil to groundwater. These
approaches are summarized as follows:
1. A water balance evaluation was conducted in accordance with methods outlined by
Thornthwaite and Mather (1957), as modified by the U.S. Environmental Protection
Agency (1975). Results ofthis evaluation indicated that no significant potential exists for
water to percolate from the sites below a depth of 5 feet under normal conditions. As a
point of reference, the depth to groundwater at M-39 and M-636 is approximately 215
feet and 76 feet, respectively (Sergent, Hauskins & Beckwith, 1988). The lack of deep
percolation predicted by this evaluation is due to the moisture deficit created by the high
annual potential evapotranspiration relative tothe annual precipitation.
2. Investigations conducted by Utah State University (1992a; 1992b) indicated that 1 inch
of precipitation could infiltrate 0.89 foot into the soil at M-39 and up to 3.2 feet into the
soil at M-636. Assuming no runoff or evapotranspiration from a precipitation event, 11.2
and 3.1 inches of water would be required to infiltrate 10 feet into the soil at M-39 and M-
636, respectively. As indicated in the sampling and analysis plan, an individual
precipitation event with a return period of about 2,500 years (probability of occurrence of
4x10"^) would be required to produce the rainfall necessary to infiltrate 10 feet into the
soil at M-636, while an event with a significantly larger return period (and
correspondingly lower probability) would be required to produce the rainfall necessary to
infiltrate 10 feet into the soil at M-39. Alternatively, the amount of water required to
infiltrate 10 feet into the soil is equivalent to five back-to-back 100-year, 6-hour storms at
M-39 and two back-to-back 10-year, 6-hour storms at M-636. The probability of these
storms occurring in the same year is 10'^° and 10'^, respectively. However, these storms
would need to occur in immediate succession to avoid evapotranspiration between
rainfall events, and all ofthe precipitation would need to remain on site, with no runoff.
Furthermore, even under these unlikely scenarios, water would only percolate 10 feet
into the ground, not to the water table. Thus, deep percolation of water and potential
contaminants from M-39 and M-636 to groundwater is extremely unlikely.
3. Pre-remediation data reported by Utah State University (1992a; 1992b) indicated that
concentrations of silver and cadmium at M-39 and M-636 tend to decrease substantially
with depth. At M-39, only 6 of 32 sample locations contained silver concentrations in
excess of 200 mg/kg at a depth of 1 to 2 feet and nearly all samples collected at these
EarthFax Engineering, Inc.
ATK Thiokol, Inc. Results of M-39 and M-636 Sampling
Promontory, Utah October 2005
shallow depths contained silver concentrations that were less than 10% of the value at
the surface. No pre-remediation cadmium concentrations exceeded the remediation
goal at M-39. At M-636, samples were collected at depths up to 13 feet. None of the
deep samples at this location contained silver or cadmium concentrations that exceeded
the remediation goal. In fact, only one sample collected at 12 to 13 feet contained even
detectable silver (MDL = 6.4 mg/kg) and only two samples collected below 11 feet
contained detectable cadmium (MDL =1.1 mg/kg). Hence, even under the driving force
of active wastewater discharges, contaminants were adsorbed to the soil far short of the
groundwater surface, thus further verifying that leaching to groundwater is not a viable
pathway for exposure to potential contaminants from the M-39 and M-636 sites.
In addition to these evaluations that were previously presented to the Division (see
EarthFax Engineering, 2003), the Division independently evaluated the potential for residual
metal contamination to migrate from soil to groundwater at the sites. The results ofthe
Division's evaluation, which concluded that no significant soil-to-groundwater migration potential
exists, are presented in Section 3.2.3 ofthis report. Based on the conclusions drawn from these
multiple evaluations, the soil-to-groundwater migration is not considered a viable pathway for
this assessment.
2.2 HUMAN-HEALTH RISK
Preliminary remediation goals were developed in the project sampling and analysis plan
(EarthFax Engineering, 2003). As indicated in Sections 2.1.2 and 2.1.3 of that document, that
evaluation included an analysis ofthe following exposure pathways, under industrial and
residential land-use scenarios, as appropriate, based on the conceptual site model:
• Inhalation of contaminated fugitive dust
• Dermal contact with contaminated soil or water
• Direct ingestion of contaminated soil
• Ingestion of contaminated produce, beef, or milk grown or produced on site.
Remediation goals calculated in accordance with that human-health risk assessment are
repeated in Table 2-1. As a point of comparison, the values in Table 2-1 are at or below those
developed by the U.S. Environmental Protection Agency, Region IX (Smucker, 2004).
3 EarthFax Engineering, Inc.
ATK Thiokol, Inc. Results of M-39 and M-636 Sampling
Promontory, Utah October 2005
2.3 ECOLOGICAL RISK
Ecological soil screening levels for cadmium have been developed by the U.S.
Environmental Protection Agency (2005), as listed in Table 2-2. Past experience at the sites
has indicated that very dry conditions exist in the upper foot of soil, resulting in minimal if any
populations of soil invertebrates and insects. Hence, neither this ecological component nor the
avian or mammalian ground insectivores that would otherwise feed thereon will be considered
further in this screening analysis. Ofthe remaining biological types included in Table 2-2, the
most restrictive soil screening level is 28 mg/kg for avian herbivores, using doves as the
surrogate (U.S. Environmental Protection Agency, 2005). This value is slightly higher than the
human-health screening value for cadmium under a residential land-use scenario and less than
the associated value under an industrial land-use scenario (see Table 2-1).
Only limited data are available concerning appropriate ecological soil screening levels
for perchlorate and silver. The most comprehensive summary of perchlorate ecological risk is a
recent external review draft published by the U.S. Environmental Protection Agency (2002) with
the notation that it has not been formally released by EPA and should not be cited or quoted.
This document contained preliminary soil screening values for terrestrial plants and soil
invertebrates, but no other ecological components. Given the preliminary nature and limited
breadth of the data, too much uncertainty is associated with the ecological soil screening values
for perchlorate to rely on those values. Hence, potential perchlorate risks to the local ecology
will not be considered further in this assessment.
EPA is currently in the process of developing ecological soil screening levels for silver
(see http://www.epa.qov/superfund/proqrams/risk/ecorisk/ecossl.htm); however, neither that
review nor any other comprehensive evaluation has been published to provide ecological soil
screening values for silver with an acceptable degree of uncertainty. Hence, potential silver
risks to the local ecology will not be considered further in this assessment.
EarthFax Engineering, Inc.
ATK Thiokol, Inc.
Promontory, Utah
Results of M-39 and M-636 Sampling
October 2005
TABLE 2-1
Human Health Remediation Goals for the M-39 and M-636 Sites'^'
Contaminant
Cadmium
Perchlorate
Silver
Residential
PRG (mg/kg)
24
7.8
390
Critical Exposure
Ingestion - produce
Ingestion - soil
Ingestion-soil
Industrial |
PRG (mg/kg)
130
100
4,900
Critical Exposure
Cumulative - soil
Ingestion - soil
Cumulative - soil
(a) From EarthFax Engineering (2003)
TABLE 2-2
Ecological Soil Screening Levels for Cadmium
Contaminant
Cadmium
Cadmium
Cadmium
Cadmium
Cadmium
Cadmium
Cadmium
Cadmium
Species/Type
Terrestrial plants
Soil invertebrates
Avian herbivore
Avian ground insectivore
Avian carnivore
Mammalian herbivore
Mammalian ground insectivore
Mammalian carnivore
Concentration
(mg/kg)
32
140
28(3)
0.77
630
73
0.36
84
Reference
US EPA, 2005
US EPA, 2005
US EPA, 2005
US EPA, 2005
US EPA, 2005
US EPA, 2005
US EPA, 2005
US EPA, 2005
*^' Critical pathway (see Section 2.3)
EarthFax Engineering, Inc.
ATK Thiokol, Inc. Results of M-39 and M-636 Sampling
Promontory, Utah October 2005
CHAPTER 3
RESULTS AND DISCUSSION
3.1 SAMPLING AND ANALYSIS METHODS
All soil sampling was performed in accordance with the approved plan (EarthFax
Engineering, 2003). This included the following activities:
Establishment of sampling grids over each site.
Collection of three individual soil subsamples from within each grid.
Combining the three individual subsamples to create one composite soil sample from the
grid area.
Analysis of all soil samples for cadmium, perchlorate, and silver. These analyses were
performed by the Thiokol environmental laboratory.
In addition to the collection of soil samples, soil-gas data were collected at M-39 to
assess whether volatile organic compounds detected in an adjacent monitoring well originate
from M-39 or from an upgradient source elsewhere at the facility. These data were obtained
using passive soil-gas collectors, as outlined in Section 3.2 ofthe approved work plan. The
collectors were analyzed in accordance with EPA Method 8260B by Beacon Environmental
Services, Inc, (Bel Air, Maryland).
3.2 ANALYTICAL RESULTS
3.2.1 M-39
Composite soil samples were collected from the eight grids at M-39 noted on Plate 3-1,
as required by the Sampling and Analysis Plan. Results of analyses of those samples are
provided in Appendix A and summarized in Table 3-1. Field notes associated with sample
collection are provided in Appendix B. No sample at M-39 contained a concentration of the
analytes of concern (cadmium, perchlorate, or silver) that exceeded the Preliminary
Remediation Goals ("PRGs"), assuming either a residential or industrial land-use scenario, or
6 EarthFax Engineering, Inc.
ATK Thiokol, Inc. | Results of M-39 and M-636 Sampling
Promontory, Utah ' October 2005
that exceeded the Ecological Soil Screening Levels ("Eco-SSLs") for the site. Hence, the
requirements of R315-3-1.1 (e)(5) and (6) have be|en met for M-39 under the current industrial
and potential future residential land-use scenarios.
Soil-gas data were obtained from the 11 locations at M-39 noted on Plate 3-1. These
data, which are presented in Appendix C, indicate that no volatile organic compounds were
detected in the shallow soil at M-39. Based on the data obtained from the soil and soil-gas
sampling, it is concluded that past excavation efforts were sufficient to remove the impacted soil
at M-39. Hence, it is recommended that Thi
removal, in accordance with R315-101-6(c).
3.2.2 M-636
at M-39. Hence, it is recommended that Thiokol petition the Division for closure of M-39 by
Composite soil samples were collected from the 41 grids at M-636 as noted on Plate 3-
2. Results of analyses of those samples are provided in Appendix A and summarized in Table
3-2. The associated field notes are included in Appendix B. Concentrations of cadmium and
perchlorate at this site were all less than the residential and industrial PRGs and the Eco-SSLs,
where available. Concentrations of silver exceeded the residential PRG, but were less than the
industrial PRG, at 14 ofthe 41 locations (see Plate 3-2).
The requirements of R315-3-1.1(e)(5) and (6) have been met at M-636 under the current
industrial land-use scenario. Based on this conclusion, it is recommended that Thiokol petition
the Division for closure of M-636 by removal, in accordance with R315-101-6(c). Since the risk
associated with a residential land-use scenario exceeds the criteria of R315-101 at some
locations within M-636, unrestricted closure of the site may not be appropriate. Thus, it is
recommended that deed notations be included in jthe petition for site closure once the site has
i been surveyed.
EarthFax Engineering, Inc.
ATK Thiokol, Inc. Results of M-39 and M-636 Sampling
Promontory, Utah October 2005
3.2.3 Potential for Migration to Groundwater
In a comment letter to Thiokol dated September 13, 2005, the Division noted that the
EPA Region 9 default soil screening values for migration to groundwater are 8.0 mg/kg and 34
I mg/kg for cadmium and silver, respectively (see Smucker, 2004). With average cadmium
concentrations of 2.3 and 2.9 mg/kg at M-39 and M-636, respectively, no significant potential
exists for this contaminant to migrate to groundwater from soil at these sites. However, with
average silver concentrations of 116 and 325 mg/kg at M-39 and M-636, respectively, the
Division evaluated the potential for silver to migrate from the soil to groundwater at the sites.
Their evaluation was based on the EPA Region 9 tap-water PRG of 0.18 mg/L for silver
(Smucker, 2004), a dilution attenuation factor of 2p, and an estimate distribution coefficient (Ko)
of 110 L/kg (see U.S. Environmental Protection Agency [1996], based on a soil pH of 8.0, which
is reasonable for the limestone-derived soils ofthe site). Using these values, the Division
calculated a soil screening value of 396 mg/kg for migration to groundwater (i.e., 0.18 mg/L x 20
x 110 L/kg). Given an average silver concentration measured in the soil at M-636 of 325 mg/kg,
it is again concluded that no substantial potential exists foi
due to leaching from soil that remains at M-39 and M-636.
3.2.4 Quality Assurance Samples
it is again concluded that no substantial potential exists for groundwater contamination to occur
No cadmium, perchlorate, or silver was detected in any trip blank, equipment blank, or
field blank. Results of analyses of blind duplicate samples are summarized in Table 3-3. This
evaluation was made using the relative percent difference ("RPD") as a measure of precision
Blind duplicate and other quality-assurance samp
4.1.2 ofthe approved sampling and analysis plan
es were collected in accordance with Section
(EarthFax Engineering, 2003).
A meaningful RPD could not be calculated for the perchlorate data since no
concentrations exceeded the detection limit. With the exception of one low-concentration
sample and its duplicate where the RPD was 25.0% (i.e., sample M636-16 and duplicate M636-
47), all cadmium data exhibited an RPD of less th'an 20%. Hence, the cadmium data are
considered sufficiently accurate that they can be accepted without qualification.
8 EarthFax Engineering, Inc.
ATK Thiokol, Inc. Results of M-39 and M-636 Sampling
Promontory, Utah October 2005
I
Several of the duplicate silver analyses exceeded an RPD of 20%. The laboratory
I
reviewed their data and found no irregularities. Filirthermore, all duplicate sample results are
less than the PRGs proposed for the site. Therefore, the silver data are considered sufficiently
accurate that they can be accepted with qualification.
Results of laboratory quality assurance analyses are provided in Appendix A. Except in
those cases where spike values were too low for the sample matrix or because of higher than
expected concentrations in the initial sample, matrix spike analyses were within the limits
prescribed by the laboratory QA/QC plan. As noted previously, duplicate recoveries in the case
of perchlorate were meaningless due to the non-detection of perchlorate in the samples.
As indicated in Section 3.2.1, no volatile organic compounds ("VOCs") were detected in
the shallow soil at M-39. Furthermore, no VOCs were detected in the trip blanks and field
blanks associated with soil-gas sampling. The data are, therefore, considered sufficiently
I
accurate that they can be accepted without qualification.
All planned samples were collected and a
data set is considered 100% complete.
I sample results are usable. Therefore, the
EarthFax Engineering, Inc.
ATK Thiokol, Inc.
Promontory, Utah
Results of M-39 and M-636 Sampling
October 2005
TABLE 3-1
Results of M-39 Soil Chemical Analyses
Sample
Number
Residential PRG'"'
Industrial PRG'^'
Ecological SSL'"'
M39-9-04-01
M39-9-04-02
M39-9-04-03
M39-9-04-04
M39-9-04-05
M39-9-04-Q6
M39-9-04-07
M39-9-04-08
Goncentration (mg/kg) |
Cadmium'
24 1
130 1
28
1.79
3.21 I
11.1 1
0.9 J 1
0.4 J 1
0.4 J i
0.4 J
<0.2 1
Perchlorate
7.8
100
~
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.4
<0.1
Silver |
390
4,900
~
140
189
232
131
47.1
34.4
109
49.4
'^' Human-health preliminary remediation goal from Table 2-1
^"^ Critical ecological soil screen le\l/el from Table 2-2 (see Section 2.3 of text)
10 EarthFax Engineering, Inc.
ATK Thiokol, Inc.
Promontory, Utah
Results of M-39 and M-636 Sampling
October 2005
TABLE 3-2
Results of M-636i Soil Analyses
Sample
Number
Residential PRG*^'
Industrial PRG*^'
Ecoioqical SSL^"'
M636-9-04-01
M636-9-04-02
M636-9-04-03
M636-9-04-04
M636-9-04-05
M636-9-04-06
M636-9-04-07
M636-9-04-08
M636-9-04-09
M636-9-04-10
M636-9-04-11
M636-9-04-12
M636-9-04-13
M636-9-04-14
M636-9-04-15
M636-9-04-16
M636-9-04-17
M636-9-04-18
M636-9-04-19
M636-9-04-20
M636-9-04-21
M636-9-04-22
M636-9-04-23
M636-9-04-24
M636-9-04-25
M636-9-04-26
M636-9-04-27
M636-9-04-28
M636-9-04-29
M636-9-04-30
M636-9-04-31
M636-9-04-32
M636-9-04-33
M636-9-04-34
M636-9-04-35
M636-9-04-36
M636-9-04-37
M636-9-04-38
M636-9-04-39
M636-9-04-40
M636-9-04-41
Concentration (mg/kg) ||
Cadmium 1
24 1
130 1
28 1
1.64 1
1.8 1
1.78 1
2.23 1
0.9 J i
0.9 J 1
2.89
2.02 1
3.58 1
0.6 J 1
5.03 1
4.29 [
1.32
0.8 J 1
1.23 1
0.9 J 1
1.68 1
1.9 [
2.87
3.83
2.1 i
1.74 1
1.48 1
6.33 !
5.81
4.55 1
5.36 i
5.31 1
4.41 1
5.83 1
6.09
10.9 1
5.9
5.28
1.1 J
1.57 !
2.21
l.OJ 1
0.4 J 1
0.6 J 1
<0.2 i
Perchlorate
7.8
100
~
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
Silver
390
4,900
~
23.2
31
15.2
128
•sk^::^s396m- -v
•Mm^l^5T5UP^A^
386
71.1
148
•s:-mv655SP?f i..:.:
45.1
29.9
18.4
46.7
';'VA,iji;.90ir.?t^i'ft
1.46
135
46
121
'^^m49omm:m 119
117
87.7
•M-MM&^^''r<'.":
338
K-sjSs';ii769fei;i#:m';
msmaam^^v:.;:. •.'.^imesm::-^:-:
>:-;::;;:ii;473a&S'v;:
;;i::;:S890ii?i\>K
iiS#?-i3^380?fe;'-y;^i
•:'/^smGm-€m^
..' .V-696": •
284
172
218
93.8
15.3
20.7
37
0.46 J
'°' Preliminary remediation goal from EarthFax Engineering (2003). Note: Shaded cells
exceed residential (but not industrial) PRG.
*"' Critical ecological soil screen level from Table 2-2 (see Section 2.3 of text)
11 EarthFax Engineering, Inc.
tV)
2-
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3"
(D
3"
«P
3" o
TABLE 3-3
Results of Duplicate Sample Analyses
Sample Number'^'
Initial Dup.
Cadmium
Initial Dup. RPD*"'
Perchlorate
Initial Dup. RPD""
Silver
Initial Dup. RPD""
;i':i«aiiiia^»l^^ll^^Hl^^ilfilii»
M39-02
M39-05
M39-10
M39-09
3.21
0.4
3.64
<0.2
-12.6
(c)
<0.1
<0.1
<0.1
<0.1
(c)
(c)
189
47.1
384
32.3
-68.1
37.3
M636-03
M636-04
M636-13
M636-16
M636-23
M636-30
M636-33
M636^2
M636-46
M636-43
M636-47
M636-44
M636-48
M636^5
1.78
2.23
1.32
0.9
1.48
5.83
5.90
1.60
1.93
1.48
0.7
1.71
5.18
5.51
10.7
14.4
-11.4
25.0
-14.4
11.8
6.8
<0.1
<0.1
<0.1
<0.1
<0.1
<Q.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
(c)
(c)
(c)
(c)
(c)
(c)
(c)
15.2
128
18.4
1.46
87.7
890
696
13.6
160
21.5
488
82.8
455
63.5
~"1171~
-22.2
-15.5
-198.8
5.7
64.7
166.6
(^' For brevity, all sample numbers in this table have omitted the interior numbers "9-04"
"'* Relative percent difference (%)
"^' Not calculated due to non-detectable concentration in at least one of the samples
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ATK Thiokol, Inc.
Promontory, Utah
Results of M-39 and M-636 Sampling
October 2005
CHAPTER 4
POST-CLOSURE PLANS
As noted in Section 3.2 of the approved sampling and analysis plan (EarthFax
Engineering, 2003), trichloroethene, 1,1,1-trichloroethane, and 1,1-dichloroethene have been
detected in a groundwater monitoring well located adjacent to the M-39 site. The soil-gas data
discussed in Section 3.2.1 indicate that no volatile organic compounds exist in the shallow soil
at M-39. Hence, the groundwater contamination beneath that site originates from an upgradient
location. The issue of groundwater contamination at M-39 will be addressed as part of site-wide
groundwater management.
Thiokol currently has a Land-Use Tracking Plan in place to address the long-term
management of soil at M-636. Under this plan, future soil excavation and land-use changes at
M-636, if any, are monitored to ensure that site use remains compatible with industrial closure.
As part of the SWMU management plan, Thiokol Facilities Engineering uses a site master plan
and map with all SWMU locations clearly defined. Prior to any digging or soil movement, this
master plan is reviewed to assure that no SWMUs are located in the area that will be disturbed.
In addition, the M-636 site deed will be amended to indicate long-term use restrictions. A Utah-
licensed surveyor recently surveyed the site and will provide the coordinates. A copy of the
amended deed will be provided to the Division once that process is completed.
13 EarthFax Engineering, Inc.
ATK Thiokol, Inc. Results of M-39 and M-636 Sampling
Promontory, Utah October 2005
CHAPTER 5
1
REFERENCES
EarthFax Engineering, Inc. 2003. Sampling and Analysis Plan to Evaluate Areas of Potential
Soil Contamination at M-39 and M-636. Project report prepared for ATK Thiokol
Propulsion. Midvale, Utah.
Sergent, Hauskins & Beckwith. 1988. Report for Geohydrologic Investigation, Photographic
Waste Sites, Morton Thiokol Inc., Box Elder County, Utah. Project report prepared for
Morton Thiokol Inc., Wasatch Operations. | Salt Lake City, Utah.
Smucker, S. 2004. Preliminary Remediation Goals (PRG) Table. U.S. Environmental
Protection Agency, Region 9. San Francisco, California. Available on the Internet at
www.epa.gov/reqion09/waste/sfund/prq/in'dex.htm.
Thiokol Corporation. 1996. Closure of Photographic Waste Discharge Sites at M-39, M-114, M-
508, and M-636: Results of Investigative Phase. Report submitted to the Utah Solid and
Hazardous Waste Control Board. Brigham City, Utah.
Thornthwaite, CW. and J.R Mather. 1957. Instructions and Tables for Computing Potential
Evapotranspiration and the Water Balance. Publications in Climatology. Vo. 10, No. 3,
pp. 185-311.
U.S. Environmental Protection Agency. 1975. Use of the Water Balance Method for Predicting
Leachate Generation from Solid Waste Disposal Sites. Report No. EPA/530/SW-168.
Office of Solid Waste Management Programs. Washington, D.C.
U.S. Environmental Protection Agency. 1996. Soil Screening Guidance: Technical Background
Document. EPA/540/R95/128. Office of Solid Waste and Emergency Response.
Washington, D.C.
U.S. Environmental Protection Agency. 2002. Perchlorate Environmental Contamination:
Toxicological Review and Risk Characterization - External Review Draft. NCEA-1-0503.
Office of Research and Development. Washington, D.C.
U.S. Environmental Protection Agency. 2005. Ecological Soil Screening Levels for Cadmium -
Interim Final. OSWER Directive 9285.7-65. Office of Solid Waste and Emergency
Response. Washington, D.C.
Utah State University. 1992a. Final Report for Spils Study of Space Operations Facilities (M-
39, M-114) Photographic Developer Waste Discharge Sites. Project report prepared for
Thiokol Corporation. Logan, Utah.
Utah State University. 1992b. Final Report for Soils Study of Air Force Plant 78 (M-508, M-
636) Photographic Developer Waste Discharge Sites. Project report prepared for
Thiokol Corporation. Logan, Utah.
14 EarthFax Engineering, Inc.
ATK Thiokol, Inc.
Promontory, Utah
Results of M-39 and M-636 Sampling
October 2005
APPENDIXA
Results of Soil Chemical Analyses
EarthFax Engineering, Inc.
M-39 soil analytical results
gliSBfSAMRlMiCS
0409020-01
0409020-02
0409020-03
0409020-04
0409020-05
0409020-06
0409020-07
0409020-08
0409020-09
0409046-73
0409020-11
0409020-12
0409020-10
0409046-01
0409046-02
0409046-03
0409046-04
0409046-05
0409046-06
0409046-07
0409046-08
0409046-09
0409046-73
0409046-11
0409046-12
0409046-10
0409020-01
0409020-02
0409020-03
0409020-04
0409020-05
0409020-06
0409020-07
0409020-08
0409020-09
0409046-73
0409020-11
0409020-12
0409020-10
liSl^lENJ^^SSiMRllESiei
M39-9-04-01
M39-9-04-02
M39-9-04-03
M39-9-04-04
M39-9-04-05
M39-9-04-06
M39-9-04-07
M39-9-04-08
M39-9-04-09
M39-9-04-10
M39-9-04EB
M39-9-04FB
M39-9-04TB
M39-9-04-01
M39-9-04-02
M39-9-04-03
M39-9-04-04
M39-9-04-05
M39-9-04-06
M39-9-04-07
M39-9-04-08
M39-9-04-09
M39-9-04-10
M39-9-04EB
M39-9-04FB
M39-9-04TB
M39-9-04-01
M39-9-04-02
M39-9-04-03
M39-9-04-04
M39-9-04-05
M39-9-04-06
M39-9-04-07
M39-9-04-08
M39-9-04-09
M39-9-04-10
M39-9-04EB
M39-9-04FB
M39-9-04TB
@jrESt^|^NAl5'rSnE?MMES
60 IOB
6010B
601 OB
601 OB
6010B
60 IOB
6010B
601 OB
601 OB
60108
601 OB
601 OB
601 OB
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
6010B
601 OB
601 OB
60 IOB
601 OB
6010B
6010B
601 OB
601 OB
601 OB
60 IOB
601 OB
6010B
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
i^NAli^TE
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
iRESilDiSl
1.79
3.21
11.1
0.9 J
0.4 J
0.4 J
0.4 J
U
u
3.64
U
U
U
U
U
U
U
U
U
<EQL
U
U
U
U
U
U
140
189
232
131
47:1
34.4
109
49.4
32.3
384
U
U
U
Mmi
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g_j
ug/g
ug/g^
ug/L
ug/L
ug/L
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
ug/L
ug/L
ug/L
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/L
ug/L
ug/L
imii
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
3.7
3.7
3.7
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
1
1
1
0.22
0.22
0.22
0.22
0.22
0.22
0.22
0.22
0.22
0.22
2.2
2.2
2.2
IEW
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
12.2
12.2
12.2
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
4
4
4
0.73
0.73
0.73
0.73
0.73
0.73
0.73
0.73
0.73
0.73
7.26
7.26
7.26
PJillTilO.N.is
10
10
10
^N/5;ilMSIS?DpIE^
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/13/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/13/2004
10/20/2004
10/20/2004
10/20/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/13/2004
10/06/2004
10/06/2004
10/06/2004
fSAMRilEDSDpE?
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
M-636 soil analytical results
giS?;Bfs;s^iiiRi4EgiDj
0409020-13
0409020-14
0409020-15
0409020-16
0409020-17
0409020-18
0409020-19
0409020-20
0409020-21
0409020-22
0409020-23
0409020-24
0409020-25
0409020-26
0409020-27
0409020-28
0409020-29
0409020-30
0409020-31
0409020-32
0409020-33
0409020-34
0409020-35
0409020-36
0409020-37
0409020-38
0409020-39
0409020^0
0409020^1
0409020-42
0409020^3
0409020^4
0409020-45
0409020-46
0409020-47
0409020-48
0409020-49
0409020-50
0409020-51
0409020-52
0409020-53
|i3lilEMiilSAMI2llE3ld)^
M636-9-04-01
M636-9-04-02
M636-9-04-03
M636-9-04-04
M636-9-04-05
M636-9-04-06
M636-9-04-07
M636-9-04-08
M636-9-04-09
M636-9-04-10
M636-9-04-11
M636-9-04-12
M636-9-04-13
M636-9-04-14
M636-9-04-15
M636-9-04-16
M636-9-04-17
M636-9-04-18
M636-9-04-19
M636-9-04-20
M636-9-04-21
M636-9-04-22
M636-9-04-23
M636-9-04-24
M636-9-04-25
M636-9-04-26
M636-9-04-27
M636-9-04-28
M636-9-04-29
M636-9-04-30
M636-9-04-31
M636-9-04-32
M636-9-04-33
M636-9-04-34
M636-9-04-35
M636-9-04-36
M636-9-04-37
M636-9-04-38
M636-9-04-39
M636-9-04-40
M636-9-04^1
I^EglSs
60108
60 IOB
60108
6010B
60108
60 IOB
6010B
6010B
60108
60108
6010B
601 OB
60108
60108
6010B
60108
60108
60108
601 OB
60 IOB
60108
60108
6010B
6010B
60 IOB
60108
6010B
601 OB
60108
60 IOB
60108
601 OB
6010B
60108
60108
60108
60108
601 OB
6010B
60108
60 IOB
iSiiiAli^^IiElilAMEl'
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
ioiM'iv^-itE
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
^d
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
iRESBM
1.64
1.8
1.78
2.23
0.9 J
0.9 J
2.89
2.02
3.58
0.6 J
5.03
4.29
1.32
O.SJ
1.23
0.9 J
1.68
1.9
2.87
3.83
2.1
1.74
1.48
16.33
'5.81
4.55
5.36
5.31
4.41
5.83
6.09
10.9
5.9
5.28
1.1 J
1.57
2.21
1. J
0.4 J
0.6 J
U
sONin?
ug/g
ug/g
ug/g
.ug/g„
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/gH
ug/g
ug/g
ug/g
ug/g
ug/g.
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
(ug/g
ug/g
Wg
ug/g
ug/g
.yg./g_
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
mm 0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
0.18
iEQL^
0.59
0.59
0.59
0.59
6!59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0.59
0,59
SmuiiQNis
•1
i?jo;islAl!sS^Srs2Dli!rE^
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
10/13/2004
gSi9iiweLf^EDiDAqjEfi
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
0409020-54
0409020-55
0409020-56
0409020-57
0409046-70
0409046-71
0409046-72
6469020-59"
0469626-62'
6409026-65 '"
0409020-68
0409020-60
0409020-63
0409020-66
0409020-69
0409020-58
0409020-61
0409020-64
0409020-67
0409046-13
0409046-14
0409046-15
0409046-16
0409046-17
0409046-18
0409046-19
0409046-20
0409046-21
0409046-22
0409046-23
0409046-24
0409046-25
0409046-26
0409046-27
0409046-28
0409046-29
0409046-30
0409046-31
0409046-32
0409046-33
0409046-34
0409046-35 "
0409046-36
0409046-37
M636-9-04^2
M636-9-04-43
M636-9-04^4
M636-9-04-45
M636-9-04^6
M636-9-04-47
M636-9-04-48
'M636-964-E'B1
M636-904-E82
M636-904-EB3
M636-904-EB4
M636-904-FB1
M636-904-FB2
M636-904-FB3
M636-904-FB4
M636-904-TB1
M636-904-TB2
M636-904-TB3
M636-904-TB4
M636-9-04-01
M636-9-04-02
M636-9-04-03
M636-9-04-04
M636-9-04-05
M636-9-04-06
M636-9-04-07
M636-9-04-08
M636-9-04-09
M636-9-04-10
M636-9-04-11
M636-9-04-12
M636-9-04-13
M636-9-04-14
M636-9-04-15
M636-9-04-16
M636-9-04-17
M636-9-04-18
M636-9-04-19
M636-9-04-20
M636-9-04-21
M636-9-04-22
M636-9-04-23
M636-9-04-24
'M636-9-04-25
60108
60108
60108
60108
60 IOB
60108'
6010B
60108
601 OB
6010B
60108
60108
601 OB
60108
60108
601 OB
6010B
60108
60108
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
"E'PA 314.0
EPA 314.0
EPA 314.0
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
CADMIUM
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
Cd
CI04
CI04
CI04
CI04
CIO4
CI04
CI04
CIO4
CI04
CI04
CI04
CI04
CIO4
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
1.6
1.48
1.71
5.51
1.93
0.7 J
5.18
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
U
U
U
U
U
U
U
U
u
u
ug/g
ug/g
ug/g
ug/g
iJ9/g__
ug/g
ug/g
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
0.18
0.18
0.18
0.18
0.18
0.18
0.18
3.7
3.7
" 3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
. 0.59
0.59
0.59
0.59
0.59
0.59
0.59
12.2
12.2
"l'2"2
12.2
12.2
12.2
12.2
12.2
12.2
12.2
12.2
12.2
0.4
0.4
0.4
0.4
0.4
__0.4
"6'-4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
1
1
.1
1
10/13/2004
10/13/2004
10/13/2004
10/13/2004
10/13/2004
10/13/2004
10/13/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
0409046-38
0409046-39
0409046-40
0409046-41
0409046-42
640964'6-4"3""
0409046-44
0409046-45
'0409046-46
0409046-47
0409046-48
10409046-49
0409046-50
0409046-51
0409046-52
0409046-53
0409046-54
0409046-55
0409046-56
0409046-57
0409046-70
0409046-71
0409046--72
0409046-59
0409046-62
0409046-65
0409046-68
0409046-60
0409046-63
0409046-66
0409046-69
0409046-58
0409046-61
0409046-64
0409046-67
0409020-13
0409020-14
0409020-15
0409020-16
0409020-17
0409020-18
0409020-19
0409020-20
0409020-21
M636-9-04-26
M636-9-04-27
M636-9-04-28
M636-9-04-29
M636-9-04-30
M636-9-04-31
M636-9-04-32
M636-9-04-33
M636-9-04-34
M636-9-04-35
M636-9-04-36
M636-9-04-37
M636-9-04-38
M636-9-04-39
M636-9-04-40
M636-9-04-41
M636-9-04-42
M636-9-04-43
M636-9-04-44
M636-9-04^5
M636-9-04-46
M636-9-04-47
M636-9-04-48
M636-904EB1
M636-904EB2
M636-904EB3
M636-904EB4
M636-904FB1
M636-904FB2
M636-904FB3
M636-904FB4
M636-904TB1
M636-904TB2
M636-904TB3
M636-904TB4
M636-9-04-01
M636-9-04-02
M636-9-04-03
M636-9-04-04
M636-9-04-05
M636-9-04-06
M636-9-04-07
M636-9-04-08
M636-9-04-09
EPA 314.0
EPA 314.0
[EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA.314-0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
EPA 314.0
601 OB
6010B
6010B
6010B
601 OB
6010B
eoioB'
6010B
60108
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE "
PERCHLORATE
PERCHLORATE'
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
CI04
CI04
CI04
CI04
CI04
ci64
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
C104
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
CI04
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
U
U
u
U
u
U
U
U
U
u
u
U
u
U
u
u
u
U
U
U
u
u
u
U
U
U
U
u
u
u
u
u
u
u
u
23.2
31
15.2
128
398
575
386
71.1
148
mg/kg
mg/kg
mg/kg
mg/i^g
mg/kg_
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/i^g
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
ug/L
ug/L
lijg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/g
lug/g
ug/g
ug/g„
ug/g
ug/g
ug/g
ug/g
ug/g
0.1
0.1
0.1
0.1
'"'o.l
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
1
1
1
1
1
1
1
1
1
1
1
1
0.22
0.22
0.22
0.22
0,'22
0.22
0.22
0.22
0.22
0.4
0.4
0.4
0.4
0.4
' 6.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
4
4
4
4
4
4
4
4
4
4
4
4
0.73
0.73
0.73
0.73
0,73
0.73
0,73
0,73
0,73
1
\
10
10
10
10
10
10
10
10
10
10
10
10
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/12/2004
10/13/2004
10/13/2004
10/13/2004
10/13/2004
10/13/2004
10/13/2004
10/13/2004
10/13/2004
10/13/2004
10/13/2004
10/13/2004
10/20/2004
10/20/2004
10/20/2004
10/20/2004
10/20/2004
10/20/2004
10/20/2004
10/20/2004
10/20/2004
10/20/2004
10/20/2004
10/20/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
1 09/28/2004
1 09/28/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004 — •
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
0409020-22
"0409020-23
0409020-24
0"469626-'25"~
0409020-26
6469626"-27'
0409020-28
0409020-29
0409020-30
0409020-31
0409020-32
0409020-33
0409020-34
0409020-35
0409020-36
0409020-37
0409020-38
0409020-39
0409020-40
0409020-41
0409020-42
0409020-43
0409020-44
0409020^5
0409020-46
0409020-47
0409020-48
0409020-49
0409020-50
0409020-51
0409020-52
0409020-53
0409020-54
0409020-55
0409020-56
0409020-57
0409046-70
0409046-71
0409046-72
0409020-59
0409020-62
0409020-65
0409020-68
0409020-60
M636-9-04-10
M636-9-04-11
M636-9-04-12
M636-9-04-13
M636-9-04-14
M636-9-04-15
M636-9-04-16
M636-9-04-17
M636-9-04-18
M636-9-04-19
M636-9-04-20
M636-9-04-21
M636-9-04-22
M636-9-04-23
M636-9-04-24
M636-9-04-25
M636-9-04-26
ivi636-9'-04-27
M636-9-04-28
M636-9-04-29
M636-9-04-30
M636-9-04-31
M636-9-04-32
M636-9-04-33
M636-9-04-34
M636-9-04-35
M636-9-04-36
M636-9-04-37
M636-9-04-38
M636-9-04-39
M636-9-04-40
M636-9-04-41
M636-9-04-42
M636-9-04-43
M636-9-04-44
M636-9-04-45
M636-9-04-46
M636-9-04-47
M636-9-04-48
M636-904-EB1
M636-904-EB2
i\/l'636-904-E'B3''
M636-904-EB4
M636-904-FB1
60108
! 60108
6010B
6010B
60108
60108
60108
60108
60108
601 OB
6010B
60108
60108
60108
601 OB
601 OB
6010B
lioioB
601 OB
60108
60108
60108
60108
601 OB
601 OB
601 OB
6010B
60108
6010B
601 OB
60108
60 IOB
60108
60108
60108
60108
60108
60108
60108
6010B
60108
60108
60108
60108
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
^LVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
Ag
Ag
Ag
Ag
Ag. ._ __
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
Ag
655
45.1
29.9
18.4
46,7
901
1.46
135
46
121
905
119
117
87,7
479
338
769
884
853
473
890
1380
704
696
284
172
218
93.8
15,3
20.7
37
0.46 J
13.6
21.5
82,8
63,5
160
488
455
U
U
U
U
U
[ug/g
jug/g
ug/g
ug/g-__
ug/g
ug/g
ug/g
[ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g_
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/L
ug/.L_
ug/L
ug/L
ug/L
0.22
^0.22
0.22
0.22
0.22
0.22
0,22
0,22
0.22
0.22
0.22
0.22
0.22
0.22
0.22
0.22
0.22
0.22
0.22
0.22
0.22
0,22
0.22
0,22
0,22
0.22
0,22
0,22
10,22
0,22
0,22
0,22
0,22
0,22
0.22
0.22
0.22
0.22
0.22
2,2
2.2
2'2
2.2
2,2
0,73
0.73
0.73
0.73
0.73
0,73
0,73
0,73
0,73
0,73
0,73
0,73
0,73
0,73
0,73
0,73
0,73
0,73
0,73
0,73
0,73
0,73
0,73
0,73
0,73
0,73
0,73
0,73
0.73
0,73
0,73
0.73
0,73
0,73
0,73
0,73
0,73
0,73
0.73
7,26
7,26
7,26
7,26
7,26
1
1
1
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
09/28/2004
10/13/2004
10/13/2004
10/13/2004
10/13/2004
10/13/2004
10/13/2004
10/13/2004
10/13/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
1 10/06/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
0'9/14/2064
09/14/2004
09/14/2004
0409020-63
0409020-66
0409020-69
0409020-58
0409020-61
0409020-64
6409026-67
M636-904-FB2
M636-904-F83
M636-904-FB4
IM636-904-TB1
M636-904-TB2
M636-904-fB3'
M636-964-TB4
CQ C
Q C
Q
OO
O
oi
o
o
C0
|
(
0 C
D
60108
6010B
66"IOB' "^
60108
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
SILVER
Ag
Ag
Ag
Ag
Ag
Ag
Ag
U
u
u
u
U
U
U
ug/L
ug/L
ug/L
ug/L
ug/L
u.g/!-l„
ug/L
2,2
2,2
2.2
2.2
2,2
2^2
2,2
7.26
7,26
7,26
7.26
7,26
7'26
7.26
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
10/06/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
09/14/2004
109/14/2004
09/14/2004
GERTIFIGATE OF ANALYSIS
Listihg of Sample Information arid Testing Requested
Monday, October 18, 2004
TESTED FOR: {^TK Thiokol: DLV
Environmental Monitoring
MS, 301
thipkolCorp, Uf 84322
ANALYZEPBY: i^TK Thiokol Propulsion
Ehvironmehtal Laboratory
feo. Box 7(37, M/S 245
Brigham City, UT
84302-0707
435-863-3732
435-863-8080
Contact Name:
Project:
Sample Delivery Group:
John Holladay
UPDES - DLV
0409020
Page 1 of 26
Sample Delivery Group: 0409020
Sample No. Client No.
Test Requested
!•
0409020-01 M 39-9-04-01
Sample Description
Received Collect Date/Time
Matrix
09/15/04 9/14/2004 09:45:00
SW846, 30503:
SW-846. 60103 (Solids)
0409020:.02 M39-9-04-62'
ICP/GFAAMeials DIgeslidn
Metals Analysis by ICP - 6010
Soil
Soil
Og/15/04 9/14/2664-09:50:00
:SW-846,3050B
SW-846, 60106 (Solids)
ICP/GFAA Metals Digestion
Melals Analysis by ICP - 601O
Soil
Soil
0409020-03 M39-9-04-03
SW-846, 3050B;
SW-846, 601 OB (Solids)
0409020-04 M39-9-04-64
IGP/GF/\A Metals Digesiion
Metals Analysis by ICP - 60ib
I
09/15/04 9/14/2004 09:55:00^
Soil
Soil
09/-15/04 9/14/2004 10:00:00
SW-e46, 3050B:
SW-846,:6010B (Solids)
0409020-05 M39-9-04-05
ICP/GFAA Melals Digestion
Metals AnalysIs: by ICP - 6010
Soil
Soil
09/15/04 9/14/2004 10:05:00
SW^46. 3050B :
SW-846, BOlOB (Solids)'
ICP/GFAA Melals Digestion
MelalsAnalysis by ICP - 6010
Soil
Soil
0409020-06 M39-9-04-05 09/15/04 9/14/2004 10:10:00
SW-846. 30508
SW-846, 601 OB (Solids);
0409020-07 M39-9-04-07
liSP/GFAA Melals Digesiion
liletals Anaiysis by iCP - 601O
Soil
Soil
09/15/04 9/14/2004 10:13:00
SW-846, 3050B
SW-846, 6010B;(Solids)
0409020-08 M39-9-04-0a
\CPIGFAA Metals Digestion
Metals Analysis by ICP - 6010
Soil
Soil
09/15/04 9/14/2004 10:15:00
SW-846, 30508
SW-B46, 60108 (Solids)
ICP/GFAA Metals Digestion
Metals Analysis by ICP-6010
Soil
Soil
0409020-09 M39-9-04-:09 09/15/04 9/14/2004 10:05:00
SW-646, 3050B
SW-846. 601 OB (Solids)
0409020-10 M39-9-04TB
iCP/GFAA MetalS: Digestion
Metals Analysis by ICp - 601O
Soil
Soil
09/15/04 9/14/2004 09:30:00
SW-846.:3010A
SW-846, 601 OB (Water)
Meials Digestion
Melals Analysis by ICP - 6010
Water
Water
Page 2 of 26:
Sample Delivery Group: 040902(3
Sample No. Client No.
Test Requested
0405020-11 M39-9-04EB
SW-846, 301 OA:
SW-846, 601 OB (Watei-)
1 0409020-12 M39-9-04FB
SW-846, 30 IOA.
SW-846;:66iOB;(Water)
0409020-13 M636-9-b4-6l
SW-846, 3050B
SW-846. 601 OB (Sbilds)
0409020-14 M636-9-04-02
SW-846. 30508
SW-846, 601 OB (Solids)
0409020-15 M636-9-04-03
SW-846; 30508:
SW-846. 60108 (Sblids):
0409020-16 M636r9-04-04
SW-846i 30508
SW-846; eoiOB (Solids)
0409020-17 M636-9-64-05
SW-846. 3050B
SW-846, 601 OB (Solids)
0409020-18 M636-9-04-06;
•
SW-846; 3050B
SW-846, 601 OB (Solids)
0409020-19 M636-9-04-07
SW-846. 3050B
SW-846, 601 OB (Solids)
0409020-20 M636-9-04-08
SW-846. 30508
SW-846. 601 OB (Solids)
Sample Description
I
Metals: Digestion
Metals-Anaiysis. by ICP - 6010
Metals Digestion
Metals Analysis by !GP - 6010
i
ICP/GF/V\ Metals Digestiori'
Metals Analysis.t5y ICP - 6010
ICP/GF/\A Metals Digestion
Metals Analysis by iCP - 6010
! i
1 •
ICP/GFAA Metais Digestion
Metals Anaiysis by IGP - 6010
ICP/GFAA MetalsDigestion
Metals Analysis by ICP- 6010
i
ICP/GF/SiA Metals Digestion
Metals Analysis by IGP-6010
ICP/GFAA Metals Digestion
Metals Analysis by iCP - 6010
1
i
IGP/GFAA Metals' Digestion
Metals Analysis by ICR- 6010
ICP/GFAA Metals'Digestion
Metals Analysisby ICP r 6010
Received CollectDate/Time
Matrix
09/15/04
Water
Water
09/15/04
Water
Water
09/15/04
Soil
Soil
.69/15/04:
Soli
Soil
09/15/04
Soil
Soil
09/15/04
Soil
Soil
09/15/04
Soil
Soil
09/15/04
Soil
Soil
09/15/04
Soil
Soil
09/15/0-4
Soil
Soil
9/14/2004 09:50:00
9/14/2004 09:50:00
9/14/2004 10:54:00
9/14/2004 10:43:00:
9/14/2004 10:45:00
9/14/200410:50:00:
9/14/200410:54:00
9/14/2004 l'i:00:60
9/14/2004 11:02:00
9/14/2004 11:04:00:
Page 3 of 26
Sample Delivery Group: 0409020
Sample No. Client No.
Test Requested
i 0409020-^21 M636-9-04-69:
i
SW-846, 3050B
SW-846. 601,08 (Solids)
0409020r22 M636-9-04-10
SW-846, 3050B
SW-846, 601 OB (Sblids)
; 0409020-23 M636-9-64-11
SW-846.30508
SW-846, 6010B (Solids)
0409020T24 M636-9-04-12
SW-846,30508
SW-846. 601 OB (Solids)
0409020-25 M636-9-04-13
SW-846,:305pB
SW-846, 60108 (Solids);
1 0409020^26 M636-9-04-14
SW-846, 3050B
SW-846, 60108 (Solids)
0409020-27 M636-9-04-15
SW-846.:3050B
SW-846, 601 OB (Solids)
0409020-28 M636-9-04-16
i • • ••
SW-846. 3050B
SW-845, 601 OB (Solids)
0409020-29 M636-9-04-17
SW-846,:3050B
;SW-846. 601 OB (Solids)
0409020-30 M636-9-04-18
SW-846, 3050B:
SW-846, 601 OB (Solids)
Sample Description
ICP/GFAA Metals Dig
Metals/^nalysis by IGF
3stion
'-6010
iG'p/GFAA;.Metais Digestion
Melals Analysis by IGF' - 6010
ICP/GFM;Metals Digestion
Metals Analysis by ICP - 6010
I
IGP/GFAA Metals Digestion
Melals Analysis by ICP - 6010
IGP/GFAA Metals Digestion
:Metals Analysis;t>y ICP - 6010
,
ICP/GFAA Metais Digestion
Metals Analysis by-ICP - 6010
ICP/GFAA Metals Di^«
Metals Analysis by ICF
1
istion
>-6010
ICP/GFAA Metals Digestion
Metals Anaiysis by ICP-6010
1
1
ICP/GF/VA Metals Dig«
Mislals Analysis by ICF
'stion
>-6010
!
IGP/GFM Metals Digesiion
Metals Analysis by IGP - 6010
Received CollectDate/Time
Matrix
09/15/04
Soil
Soil
09/15/04
Soil
Soil
69/15/04
Soil
Soil
09/15/04
Soil
Sioii
09/15/04
Soil
Soil
09/15/04
Soil
Soil
09/15/04
Soil
Soil
09/15/04
Soil
Soil
09/15/04
Soil
Soil
09/15/04
Soil
Soil
9/14/2004 11:06:00
9/14/2b04'11:08:00
9/14/2004 11:10:00
9/14/2004 11:15:00
9/14/2064 11:17:00
9/14/2004 11:18:00
9/14/200411:22:00
-
9/14/2004 11:26:00
9/14/2004 11:28:00
9/14/2004 11:32:06
Page 4 of 26
Sample Delivery Group: 0409020
Sample No. Client No.
Test Requested
I 0409020-31 M636-9-04-19
SWW6, 3050B;
SVV-846, 60108 (Solids)
6469020-32 M636-9-04-20
1
SW846. 30508
SW-846, 601 OB (Solids)
0409020-33 M636-9-04-21
SW-846. 3050B
SW-846, ebl.OB (Solids)
i 0409020-34 M536-9-04-22
i
SW-846. 30508
SW-846. 6010B {Solids)
1 0409020-35 M636-9-p4-23
SW-846. 3050B
SW-846. 60ipB;(Solids)
0409020-36 M636-9-04-24
'i
SW-846, 3050B
SW-846, 601 OB (Solids)
0409020-37 M636-9-04r25
SW-846, 3050B
SW-846, 601 OB (Solids)
0409020-38 M636-9-p4-26
SW-846, 3050B
SW-846, 601 OB (Solids)
0469020-39 M636-9-04-27
SW-846, 3050B
SW-846, 60IOB (Solids)
0409020-40 M636-9-04-28
SW-846, 3050B
SW-846, 601 OB (Solids)
Sample Description
ICP/GFAA Metals Digestion
Metais Analysisby IGP-6010
iGP/GFAA Metals Digestiori
Metais Analysis ,by IGP - 6010
1
ICP/GFAA Metals Digestion
iytetals Analysis by ICP - 6010
IGP/GFAA Metals Digestion
;Metals Analysis by IGP - 6010
ICP/GFAA Metals Digestion
Metals Anaiysls:by ICR - 60l0
iCP/GFAA Metals Digestion
Metals Analysis by IGP- 6010
ICP/GF/W Metals Digestiori
Metais Analysis by ICP -:6016
1
IGP/GF/V\ Metals Digestion
Metais Analysis by ICP - 60l6
ICP/GFAA Metais Digestion
Metals Analysis by ICP - 6010
1
1 ICP/GFAA Metals Digestion
Metals Analysis by ICP - eo-iO
Received '
Matr
09/15/04
Soil
Soil
09/15/04
Soil
Soil
09/15/04
Soil
Soil
09/15/04
Soil
Soil
69/15/04
Soli
Soil
09/15/04
Soil
Soil
09/15/04
Soil
Soil
09/15/04
Soil
Soil
09/15/04
Soil
Soil
09/15/04
Soil
Soil
Collect Date/Time
ix
9/14/2004 11:35:00
9/14/200411:37:00
9/14/200411:42:00
9/14/2004 14:40:00
9/14/200414:40:00
9/14/2004 14:45:00
9/14/200414:50:00
9/14/2004 14:55:00
9/14/200415:00:00
9/14/200415:03:00
1
Page :5 Of 26
Sample Delivery Group: 0409020
Sample No. Ciient No,
Test Requested
I 0409020-41 M636-9-04-29
SW-646, 30568
SW-846, 601 OB (Solids)
0409020-42 M636-9-04-3O
i
SW-846, 30508
SVy-846, epiOBiSblids)
0409020-43: M636-9-04-31
1
SW-846,30508
SVV-i3-46,60i OB ^Solids)
( 0409020^44 M6,36-9-b4-32
SW-846, 3P50B
SW-846,:60l6B,(Solids)
: 0409020-45 M636-9-04-33
1
SW-846, 3050B
SW-846, 6010B (Solids)
0409020-46 M636-9-04-34
SW-846. 3050B
SW-846. 601 OB (Solids)
0409020-47 M636-9-64-35
SW-846, 3050B
SW-846, 601 OB (Solids)
0409020-48 M636-9-04-36
SW-846. 3050B
SW-846, 601 OB (Solids)
0409020T49 M636-9-04-37
SW-846, 3050B
SW-846, 60108 (Solids)
0409020-50 M636-9-04-38
SW-846: 3050B
SW-846|6010B (Solids)
Sainple Description
IGP/GFAA Metals Digestion
Metais Analysis by ICP • 6010
iCP/GF/\A Metals Digestion
Metals Analysis by IGP - 6010
IGP/GFAA Metals.Digestion
Metals Anaiysis by IGP-6010
iCP/GFAA'MetalsDigestlon
Metals Analysis by ICP-6010
IGP/GF/\A Metals Digestion
Metals Analysis by IGP - 6010
ICP/GFAA Ivietals Digestion
Metals Anaiysis by IGP-6010
IGF'/GFAA Metals Digestion
Metajs Analysis by idP - 6010
iCP/GFAA Metals Digestion
Melals Analysis by tCP - 6010
ICP/GFAAMetals Digestion
Metals Analysis by iCP- 6010
ICP/GF/VA Metals Digestion
Metals Analysis by ICP - 6010
Received Collect Date/Time
Matrix
09/15/04
Soil
Soil
09/15/04
Soil
Soil
: 09/15/04
-Sbi|:
Soil
09/15/04;
Soil
Soil
09/15/04
Soil
Scili
09/15/04
Soil
Soil
09/15/04
Soil
Soil
09/15/04
Soil
Soil
09/15/04
Soil
:Soil
09/15/04
Soil
Soil
9/14/2004 15:05:00
9/14/2004 15:08:00
9/14/2004 15:13:00
9/14/200415:19:00
9/14/2004 15:21:00
9/14/2004 15:25:00
9/14/12004 15:29:00
9/14/2004 15:33:00 1
9/14/2004 15:35:00
9/14/2004 15:38:00
Page 6 of 26
Sample Delivery Group: 0409020
Sample No. Client No.
Test Requested
1 040902051 M636-9-04-39
SW-B46.3O50B
SW-846, 661 OB (Solids^
0409020-52 M636-9-04-40
SW-iB46, 30508:
SW-846, 60108: (Solids)
0409020-53 M636-9-04^41
i
SW-846, 3050B
SW-846, :601 OiB (Solids)
: 0409020-54 M636-9r04-42
SW.846, 3050B
SW-846, 6010B (Solids)
0409020-55 M636-9-04-43,
SW846. 30508
SW-846, 60108 (Solids)
0409020-56 M636-9-04-44
SW-B46, 305PB
SW-846. 601 OB .(Solids)
0409020-57 M636-9-04-45
SW-84.6. 30508
SW-846, 601 OB (Solids)
0409020-58 M636-904-TB1
.SW-846, 301 OA
SW-846, 60108, (Water)
; 0409020-59 M636-904-EB1
SW-846, 301 OA
SW-846, 6010B (Waler)
0409020-60 M636-904-FB1.
SW-846, 301 OA
SW-846, 60108 (Water)
Sample Description
1
IGP/GFAA Metals Digestion
Metals Analysis by iCP - 6010
IGF'/GFAA Metais'Digestioh
Metals Anaiysis by iCP -6010
1
ICP/GFAA Metais bigestioii
Metais Analysis by. ICP-6010
1
ICP/GFAA Metals Digestion
Metals Analysis by IGP-6010
iCP/GFAA Metals Digestion
Meials Anaiysis^by iQP-eoiO
1
1
ICP/GFAA Melals Digestion
Metals Analysis by ICP - 6010
icP/GF^AA Metals Digestion
Metals Analysis by ICP-6010
Metals Digestion
Metals Analysis by ICP - 6010
Metals Digestion
Metals Analysis by ICR - 6010
Metals Digestion
Metals Analysis by IGP - 6010
Received CollectDate/Time
Matrix
69/15/04 9/14/2004 15:41:00
Soil
Soil
09/15/04 9/14/200415:45:00
Soil
Soil
09/15/04 9/14/2004 15:48:00
Soil
Soil
09/15/04 9/14/200410:45:00
Soil
Soil
09/15/04: 9/I4/20P4; 11:17:00
Soil
I Soil
09/15/04 9/14/2004'14:40:00
Soil
Soil
09/15/04 9/14/2004 15:21:00
Soil
Soli
09/15/04 9/14/2004 14:30:00
Water
Water
09/15/04 9/14/2004 10:41:00
Water
Water
09/15/04 9/14/200410:41:00
Water
Water
Page 7 of 26
Sample Delivery Group:; 0409020
Sample Nb; Client No.
Test Requested
0409020-61 M636-904-tB2
Sample Description
Received: Collect Date/Time
Matrix
09/15/04 9/14/2004 14:30:00
SW-846. 301 OA
SW-846, 601 OB (Waler)
0409020-62 M636-904-EB2
Metals Digestion
Metals Analysis by ICP- 6010
Waler
Water
09/15/04 9/14/2004 11:12:00
SWr846, 3010A
SW-846i 601 OB (Water)
Metais Digestion
ii^etais Analysis by IGP - 6010
Water
Water
0409020-63 M636-904-FB2 09/15/04- 9/14/2004 11:12:00
SW-846, 3010A
SW-846, 60108 (Water)
0409020-64 M636-904-TB3;
Metals Digeslioii
Metals Analysis by ICP - 6010
Water
Water
09/15/04 9/14/2004'14:30:00
SW-846.; 301OA
SW-846.601 OB (Waler)
0409020-65 M636-904-EB3:
MetalsDigestidri ;
Metals Analysis by ICP-6010
Waler
Water
-09/15/04; 9/14/2004 11:48:00
SW-846, 301 OA
SW-846, 6010B (Water)
Melals'Digeslibn
Metals/Analysis by IGP - 6010
Water
Water
0409020-66 M636-904-FB3: 09/15/04 9/14/2004 11:48:00
SW-846. 301OA
SW-846. 6010B (Water)
0409020-67 M636-904-TB4
SW.846. 301 OA
SW-846, 60108 (Water)
0409020-68 M636-904-EB4
SW-846i36lOA
SW-846. 601 OB (Water)
0409020-69 M636-904-FB4
Metais Digestiori
Metajs/l^nalysis by IGP
Metals Digestion {
Metais;Analysis by ICP
Metals Digestion
Metais Analysis by ICP •
6010
6010
•6010
Water
Water
09/15/04 9/14/200414:30:00
Waler
Water
09/15/04 9/14/2004 13:15:00
Water
Water
09/15/04 9/14/2004 13:15:00
SW.846, 301 OA Metals Digestion Water
Page 8 of 26
Sample Delivery Group: 0409020
Sample No. Ciient No.
Test Requested
0409020-69 M636-904-FB4
Sample Description
Received Cpllect Date/Timei
Matrix
09/15/04 9/14/200413:15:00
SW-846, 601 OB (Water) Metals Analysis by ICP - 6010 Water
Certified By: Sionature.Vaiid tp^
W. Scott Fraser, Quality Assurance Officer
10/20/2004
Date
This certifies that the following samptes were analyzetJ using good laboratory practices to show the following results:
Page 9 of 26
Listing of Riesults by Sample
Sample Delivery Group:} 0409020
Client Sample ID; M39-9-D4-01
Sampie Description: ATK-pLV- UPDES Soil testing.
Laboratory Sample ID: 0409020-01
DateSampled: 09/14/04 09:45:
CAS Number Test Pai'arrietBr Resi
TcsiMelHod: SkV-i^S, 305(33 icF/GFAA Metals Digestion
•3050B ACID DIGEstlON
TestMethod: Si/y-SAS, 60103 (Solids) Metais Analysis by iCP - 6010
7440-43^? :CADMIUM
/44br22-4 siLVER
ultj
i;79.
-140
Units
iig/g
ug/g
MDL
,0.18
o;22
EQL
0.594
0.726
Dilution
Facitoir
1
•1
1
Analvst
JMA
MTB
MTB
Tost Dato
09/17^04
•i 0/12/04
10/12/04
CIlBrit Sample ID: M39-9-04-02
Sampio Description: ATK-DLV- IJPpESiSbiiTesting
Latioratory Sampio ID: 0409020-02
Date Sampled: 09/14/04 09:50
CAS Nuriiber Test Parametei' Result Units
rf5^(Afo(/lotf:V SlV-rM6,30SPS " " 1CP/GFM ivi^^tals Di^eViion 7
•3050B:ACID.DIGESTibN
Test Method: SW-846, 60103 (Soildsj Metals Analysis by icp - 6010 [
7440^3-9 CADMIUM
7440-22;4 ;SILVER
Dilution
MDL' EQL: Factor Analvst Test Date
JMA 09/17/04
3.21
.:.:..: 18B
ug/g
ug/g
o;ia
0:22
0.594
0,726
.1
1
MTB
MTB
10/12/04
10/12/04
Clleni;Siampie ID:; M39-9-04-03:
SariiploDescrlptlon: ATK-DLV-tJF>DESSdiiTesting'
Laboratory Sample ID: 0409020-03
Date Sampled: 09/14/04 09:55
CAS Number
Test Method:
TestMethod:
7440-43-9
744b-2i-4
Test Paramatar Result Units
S|Vr846, JoioS ICF/Gi=AA Metais.Digastipn f ~
3050B ACID DIGESTION
SWrB46,Spi6B:(Solids) Metals Anaiysis by ICi=-6010;
CADMIUM lll.i ug/g
Dilution
MDL EQL Factor Analvst Test Date
SILVER 232 ug/g
:0:18
ici;22
0,594 1
0,726 1
JMA
MTB
MTB
09/17/04
10/12/04
10/12/04
Client Sampio ID: M39-9-04r04
Sample Description: ATK-DLy - UPDES Soil Testing
Laboratory Sampio ID: 0409020-04
Date Sampled: 09/14/04 10:00
CAS Number Test Parameter Result Units
TestMethod: SIV-M6,30508 ICP/GFAAMetals Digcistioni
3050B ACID DIGESTION
Tes/Met/ioc<: SW-BtB, BOIOB (SoUds) Melals Analysis by ICP-6010
7440-43-9 CADMIUM
7440-22-4 SILVER;
MDL ISL
Dilution
Factor Analvst Test Date
JMA 09/17/04
0,9 J
131
ug/g
ug/g
0,18
0.22
0.594
P-726
1
1
MTB
MTB
10/12/04
10/12/04
CIlBnt Sampio ID: M39-9-04-05 Laboratory Sample ID: 0409020-05
Date Sampled: 09/14/04 1005
Sample Description; ATK-DLV - UPDES Soil Testing ]
CAS Number TestParameter Result Units
TestMeUiod: SliV-S46,30503 ICP/GFAA Metals Digestion
3050B ACiD DIGESTION
Dilution
MDL EQL Factor Analvst Test Date
JMA. 09/17/04
Page 10 of 26
Listing of Results by Sampie
Sarnple Delivery Group: 0409020
Cllont Sample ID: M39-9-04-05
Sample Description: ATK-DLV - UPDES Soli Testlrig
Laboratory Sample ID: 0409020-05
bate Sampled:; 09/14/04 10:05:
CAS Nuinber Test Parameter Result Units
TestMethod: SWr84e, BOIOB (Solids) Metals Anaiysis by iiiP-ebfoi
MDL
7440-43-9,:
7440.-22-4
CADMIIJM.
SILVER;:
0.4 J ug/g
47.1 ug/g
0,18
6:22
EQL
0.594
0.726
Dilution
Factor Analvst Tost Date
MTB
MTBi
10/12/04
10/12/04
Client Sample ID:; M39-9,-04-p6
SampIoDosbriptlori: AJK-DLV -UPDES-SdiiTestirig
Labdratory Saimple ID: 0409020-06
bate Sarhplod: 69/14/04 10:10
i
CAJS Number Toist Parameter Result Units
TestMethod: SW-846,3()50B ICP/GFAA Metals Digesiion
3050B ACID DIGESTION
TestMethod: SW-84e, BOIOB (Solids) Matals Analysis by iCP-6010 i
7440-43:9 CADMIUM
7440-22^4 SILVER
MDL :;EQL
Dilution
Facitor Analvst Tost Date
JMA 09/17/04
0.4[j
34.4
ug/g
ug/g
0.18
0.22
.;0.594
0.726
1
1
MTB
MTB
10/12/04
10/12/04
Client Sampio ID: M39-9-04-07
SamploDescrlptloii:: ,ATK-DLV - UPDES: Soli Testing
Laboratory Sampio ID: 0409020-07
Date Sampled; 09/14/04 10:13
CAS Number
TestMethod:
TestMethod:
7440-13-9
7440-.22A
Tesit Parameter Result'
SlV-Mfi, 3050^ ICP/GFAA Metals Digestion
3050B:AC|D DiGESTlON:
SIV-fl4e, 601 OB (Solids) Metals Analysis by ICP - 6010
:CADM|UM 0;4J
iSILVER i09
Units
7.'~''
ug/g
uala
Dilution
MDL EQL Factor Analvst Testbate
JMA: 09/17/04
0:18
0.22;
0:594
0.726
1
1
MTB
MTB
10/12/04
10/12/04
Client SamplelD; M39-9-04-08
Samjjle Descrlptidli: ATK-DLV - UPDES'Soil Testing
Laboratory Siample ID:: 0409020-08
Date Sampled: 09/14/04 10:15
CAS Numbor Test Parameter Result: Units
TestMethod: SlrV-846,30508 iCP/GFAA Melals Digestion
3050B ACID DIGESTION
TestMethod: SW-S46,6PiOB'ISqiias) Meiais Analysis by ICP-601 (D 1
7440-43-9 CADMIUM
7440-22-4 SILVER
Dilution MDL EQL Factor Analvst Test Date
JMA. 09/17/04
u
49,4
ug/g
ug/g
0.18
0:22
0:594
0.726
1
1
MTB:
MTB
10/12/04
10/12/04
Client Sample ID: M39-9-04-09
Sample Description: ATK-DLV - LJPDES;Soil Tesling
Laboratory Sample ID: 0409020-09,
Date Sampled: 09/14/04 10:65
CAS Nurnber
Test Method:
TestMethod:
7440-13-9
7440-22-4
Test Paramoter Result
51V-B46, 305^3 :|CP/GF/>,A Metals Digestion
30S0B ACID DIGESTION
SW-B46, BOIOB (Soildsj ; Metals Analysis by ICP - 6010
Units MDL
CADMIUM
SILVER
U ug/g
32.3 ug/g
0.18
0.22
EQL
0.594
0.726
Dilution
Factor Analvst Test Data
JMA
MTB
MTB
09/17/04
10/12/04
10/12/04
Page 11 of 26
Listing of Results by Sample
Sample .Delivery droup: 0409020
Client Sample ID: M39-9-04TB
Sample Dos(:rlptl6n: ATK-DLV - UPDES Soil Testing
Laboratory Sample ID: 0409020-10
Date Samplod: 09/14/04 09:30
CASNumber
TestMethod:'
TestMethod::
7440-43-9;
7440-22-4
Test Parameter
:SW^4«/:30Ja4 • Metals.Digeslioii
3010A ACID DIGESTION:
S}/y-84e, BOIOB (Water): Metals Ariaiysis by ICP - 6010;
1
CADMIUM
SlLVEFt
Rosult Units. MDL EQL
Dilution
Factor Analyst Test Date
MTB 10/04/04
u
u
ug/L
ug/L
3.7
2,2;
'12.21
7,26
1
1
MTB.
MTB
10/06/04
10/06/04
Client Sample ID: M39-9-04EB
Sampio Description: ATK-DLV - UPDES SoilTesting
Laboratory Sampio ID; 0409020-11
DatoSamplod: 09/14/04 09:50
CASNijiriber
feslMetfiod:
TestMethod:
7440-43-9
7440-22-4
Test Parameter
SW-i4S,30idA Metali Diyesiiqn
3010A ACID DIGESTION i
S:W-846, BOIOB (Water) Metals Analysisby ICP-60101
G/yDMIUM'
SILVER
Result Urilts MDL
Dilution
EQL Factor Analvst test Date
MTB 10/04/04
U
u
ug/L
ug/L
3.7
.2:2
12,21
.. 7:26
1
1
MTB
MTB
10/06/04
10/06/04
CHent Sample ID: M39-9-04FB
Sample Description: :ATK-DLy-UPpES,Sq|l Testing;
Laboratory :Sariiple ID: 0409020-12
DateSampled: 09/14/04 09:50
CASNumber Test Parameter Result Units
TestMethod: SW-84$,3dlOA Metais.Digesliqh 1
3010AACipDiGEStlOKl
TestMethod: SW-846, BOioB (Waier) Metals Analysisby ICP-6010
7440-43-9 CADMIUM
7440-22-4 siLVER
MDL
Dilution
EQL Factor Analyst Test Date
U. ug/L
U ug/L
3:7
2.2'
12:21
7.26
1
1
1
MTB
MTB
MTB
10/04/04
10/06/04
10/06/04
Client Sample |D: M636-9-p4-01
Sample Description:, Atk^DLV- UPDES Soil Testing
Laboi-atory Sample ID: 0409020-13
DateSampled: 09/1.4/04 10:54
CAS Number TestParameter Result Units
TestMethod: SVVrS46,30508 ICP/GFAA Metals Digestion i
3050B ACID DIGESTION
tos/Method.' SW-846i 601 OB (Solids) MetalsAnalysisby ICP-6010
7440-43-9 CADMIIJM
7440-22-4 SiLVER^
MDL
Dilution
Factor Analvst Test Date
JMA 09/22/04
1,64
23,2
ug'g
ug/g
:Q:I8
0.22
0:594
0,726
1
1,
MTB
MTB
09/28/04
09/28/04
Client Sample ID: M636r9-04-02
Sample Descriptipn: ATK-DLV-UPDES SoilTesting
Laboratory Sample ID: 0409020-14
Date Sampled: 09/14/04 10:43
I
CAS Number Test Parametor Result Units
TestMethod: SW-846,30S0B ICP/GFAA Melals Digesiion
3b50B AGIO DIGESTION
MDL
Dilution
EQL Factor Analyst Test Date
JMA 09122/04
Page 12 of 26
Listing of Results by Sample
Samjiie Delivery Group: 0409020
CIlentSamplelD: M636-9-04-02
Samplobescrlptlbri: ATK-DLV -.UPDES Soil Testing
Laboratory Sample ID: 0409020-14
Dato Sampled: 09/14/04 10:43
CAS Numbor
TestMethod:
744d-43r9:;
7440-22-4
Test Parameter
'SW-846r66l0B (Solids)
CADMIUM
SILVER
Result Units
Metals Analysis by ICP r 6010:
1.8, ug/g
31 ug/g
MDL
0.18
0.22:
BQL
0.594
0.726
Dllutloiti
Factor Analyst Test Date
MTB
MTB'
09/28/04
09/28/04
Client Sainple ID: M636-9-p4-03
Sample Destiriptlbh: ATK-DLV - UPDES Soij Testing
Laboratory Sample ID: 0409020-15
Date Sampled: 09/14/04 10:45
CAS Number Test Parameter Result Units
Tesi Wethod; 'SIV-846,30508 ICP/GFAA Metals Digestion i
3050B ACID DIGESTION
TestMethod: SW-B4B,601I}B (Solitlsj Metais Analysis by |CP-6010
MDL EQL
Dilution
Factor Analvst Test Date
JMA 09/22/04
7440-43-9 CADMIUM
7440-22-4 SILVER
1.78
15,2
1-.-
Client Sample |D: M636-9-04-04
Sample Doscription: ATK-DLV - UPDES Soii Testing
ug/g
ug/g
0.18
0:22
6.594 1 MTBI 09/28/04
0.726 1 MTB 09/28/04
Laboratory Sample ID: 0409020-16
Dato Samplod: 09/14/04 10:50
CAS Number:
TestMethod;
Test Method:
7440-43-9
7440T22-4
TestParameter Result Units
;-Siy-M5, 30503 ICP/C3FAA Metals bjgesUon
305bB ACID DiGESTlON
SW-34B,:60iOB (Solids) Metals Analysis by icjP - 60Vo;
MDL EQL
Dilution
Facitor Analvst Test Date
CADMIUM
SILVER
••|
2:23 ug/g
128 ug/g
0.18
6.22
0;594
0.726
JMA.
MTB
MTB
09/22/04
09/28/04
09/28/04
CIlentSamplelD: M636-9 04i-05.
Sample Descriptipn: ATK-DLV - UPDES SqilTesling
Laboratory Sample ID: 0409020-17
Date Sampled: 09/14/04 10:54
CAS Number
TestMethod:
Test Mothod:
7440-43-9
7440-22^
Test Piarameter Result Units
SI(V:846, 30503 iCP/GFM-Melals Digeslipn; ;
30508 ACID DIGESTION
Siy-845, 60103 (Solids) Metals Anaiysis by ICP - 601 o'
Dilution
MDL EQL Factor Analvst Test Date
JMA 09/22/04.
CADMIUM
SILVER
0,9 J ug/g
398;. ug/g
0,18:
0,22:
0,594
0.726
MTB
MTB
09/28/04
09/28/04:
CIlentSamplelD: M636-9-r04-06:
Sample Description: ATK:^DLV -.UPDES Soil Testing
Laboratory Sample ID: 0409020-18
Dato Sampled: 09/14/04 11:00
CAS Number
Test Melhod;
TestMethod:
7440-43-9
7440-22-4
Test Parameter Result Units
SIV-846, 30503 ICP/GFAAr»ietals Digestion
;3050& ACID DIGESTION
SIV-846, ediOB (Solids) Melals Analysis byicP - 6010
MDL EQL
Dilution
Factor Analvst Test Date
CADMIUM
SILVER
0,9 J
575
ug/g
ug/g
o;i8
0,22,
0.594
0.725
1 JMA
1 MTB
1 MTB
Page 13 of 26
09/22/04
09/28/04
09/28/04
Listing of Results by Sample
Sample Delivery Group: 0409020
CIlentSamplelD: M636-9-04-07 Laboratory Sample ID: 0409020-19
DateSampled; 09/14/04 11:02
Sampio Description: ATK-DLV r UPDES Soil Testing
CAS Number Test Parariieter Result Units
Test Metiiod: SIV-:M6,:3050B ICP/GF/\A Melals Digestion
30506 ACIDDIGESTIpN
TesfMoihod; SW-846, BOIOB (Solids) Metals Ahaiyslisby ICP-60lb
7440-43-9 CADMIUM
7440-22-4 SILVER
MDL
Dilution
EQL Factor Analvst Tost Date
JMA 09/22/04
2.89
386
ug/g
ug/g
0:18
0.22
6,594
0.725:
1
1
MTB
MTB
09/28/04
09/28/04
Client Sample ID: M636-9-04-08
Sampio Description: ATK-DLV r UPDES SoilTesting
Laboratory SamplelD: 0409020-20
DateSampled: 09/14/04 11:04
CAS Number
test IVfelhod:
: TestMethod:
7440-43-9
7440-22-4
Test Pararrieter
SW-846,J0S0B\ '._ . .. ICP/GF/\A MelalsiDigesUon
3050BACID.blGESTlbN
SW-SjB,6diOBj[Solids) Metals Analysis by ICP - 6010
CADMIUM
SILVER:
Result
'Stion
>-16010
2:02
• 71-jl'
Units
:ug/g
ug/g
MDL
0:18
0,22
EpL
0:594
0,726
Dilution
Factor
1
1
1
Analvst
JMA
...........
MTB
MTB
Test Date
09/22/04
!
09/28/04
09/28/04
CIlentSamplelD: M636-9-04-09
Sample Description: ATi<-DLV - UPDES Soil Testing
Labbratbry Sample ID: 0409020-21
DateSampled: 09/14/0411:06
CAS Number Tost Pararrieter Rgsult- Units
TesiMeOiod: SIV-846,30503 ICP/GFAA Metais Digestion:
3056B ACID DIGESTION
TestMethod: SW-846, BOIOB (Soiids) Melals Ariaiysis by ICP 76010:'
7440-43-9 CADMIUM
7440.22-4 SILVER
MDL
Dilution
EQL Factor Analvst Test Date
JMA 09/22/04
3:58
148
ug/g
ug/g:
0,18
.:0.22
0.594
6.726;
1
1
MTB
MTB
09/28/04
09/28/04
Client Sample ID: M636-9-04-10
Sample Description: ATK-DLV - UPDESSoil Testing
Laboratory Sample ID: 0409020-22
DateSampled: 09/14/04 11:08
CAS Number Test Parariieter Result UhltS:
TestMethod; SW-846,36s()a ICP/GFAA MetalsDigestion
3050B ACiD DIGESTION
TestMelhod: SW-846,.BOiOB (Solids) Melals Ariaiysis by ICP-:60ip ,
7440-43-9 CADMIUM
7440-22-4 SILVER
MDL
Dilution
EQL Factor Analyst Test Date
JMA 09/22/04
0.6J
655;
ug/g
ug/g
0,18
0,22
0.594
6,726'
1
1
MTB
MTB
09/28/04
09/28/04
Client Sample ID: M636-9-04-11
Sample Description; AtK-DLV - UPDES Soil Testing
Laboratory Sample ID: 0409020-23
DateSampled; 09/14/04 11:10
CAS Number Test Parameter Result Units
Tos(Mfl(hot<; SW-846,3Q50B: iCP/GFAAiMetals Digesiion
30S0B:AC1D DiGESTlON
MDL
Dilution
EQL Factor Analyst Test Date
JMA 09/22/04
Page 14 Of 26
Listing flif Resu Its by Sample
iSample DeliyerY Group: 0409020
CIlentSamplelD: M636-9-04-11
Sample Description: ATK-DLV - UPDES Soil Testing
Laboratory Sampie ID: 0409020-23
DateSampled: 09/14/0411:10
CAS Number
TestMethod;
7440-43-9
7440-22-4
Test Parameter
SW-B4E,6010B (Solids)
CADMIUM
;siLVER:
Result
, :Metais Analysis by ICP.- 6010
5,'03
46.1
Units
ug/g
ufl/g
MDL IQL
Dllutibh
Factor Analvst Test Date
0:18
0:22;
0:594 1
6.726 1
MTB
MTB
09/28/04
-09/28/04
Client Sample ID: M636r9'04-12
Sample Descriptiori; ATK-DLV-UPDES Soil Tesling
Laboratory Sample ID: 0409020-24
DateSampled:; p9/i4/04 11:15
CAS Number Test Parameter Result Units
Test MeUiod:: SW-846, 30503 ICP/GFAA Metals DigesUon
3050B A(:ib DIGESTION'
TestMethod: SW-846, BOiOB (Solids) Metals Analysis by icP-6ciiO
744^43-9 CADMIUM
7440-22-4 SILVER;
Dilution
MDL EQL Factor Analvst Test Date
JMA 09/22/04
4.29
29.9
ug'g
ug/g
0:18:
0.22;,:
0,594
0.726
1
1:
MTB
MT,B
09/28/04
09/28/04
Client Sample ID: M636-9-04-13
Sample Description; ATK-DLV-UPDES Soil Testitig
Laboratory Sample ID: 0409020-25
DateSampled: 09/14/04 11:17
CAS Number
Tesf Meihoc/;
Tdsl Method:
7440-43-9
7440-22^
Test Parameter: Result Units
:SlV-846,:i305bS iCP/GFAAMe'tsiisDigesiiion
30508 ACID DIGESTION
SIV-846, 60103 (So//dsJ Matals Analysis by ICP-60lb,
MDL
Dilution
Factor Analvst Test Date
CADMIUM
SILVER
1.32 ug/g
18,4 ug/g
o:i8
0,22
0.594 1
0.726 1
JMA
MTB
MTB
09/22/04
09/28/04
09/28/04
Client Sample ID: M636-9r04-14
Sample Description: ATK-DLV - UPDES Soil Testing
Laboratory Sample ID: 0409020-26
DateSampled: 09/14/0411:18
CAS Number Test Parametar Rosult Units;
TestMethod: SW-84S;^0S0B icp/GFM Metais Di'gestibn' ;
36506/^CipblGESTiON
TestMethod: SW-S46, BOIOB (Solids) Metals Analysis by ICP-eoioj
7440-43-9 • CADMIUM
7440-22-4 SILVER
Dilution .MDL EQL Factor Analvst Test Date
JMA 09/22/04
O.SJ
46[7
ug/g
ug/g
0.18
0.22
0.594
0.726
1
1
MTB
MTB
09/28/04
09/28/04
Client Sample;ib: M635-9-04-15
Sannple Description: ATK-DLV - UPDES Soil Tesling
Laboratory Sample ID:: 0409020-27
Date Sampled: 09/14/04 11:22
CAS Number Test Parameter Rosult Units
TostJUe/hod; SW-846„30SOS ICP/GFAA Metais Digestion :
30S0B ACID/DIGESTION !
Test Methoc/; SW-846, 60103 (Sol/ds) Metals Analysis by ICP-6010'
7440-43-9 CADMIUM
7440-22-1 SILVER
Dilution
MDL EQL Factor Analvst Test Date
JMA 09/22/04
i;23.
901
ug/g
ug/g
o:i8
0,22.
0;594
0,726
1 MTB 09/28/04
1 MTB 09/28/04
Page 15 of 26
Listing of Results by Sample
Sample Delivery Group: 0409020
CIlentSamplelD: M636-9-04-16
Sample Description: ATK'DLV -UPDES Soli Testing
Laboratory Sample ID: 0409020-28
DateSampled: 09/14/04 11:26
CAS Number Test Parameter Result Units
TestMethod: SW-846,3D50B ICP/GFAA Metais Digestion
3050B ACID DiGESTlON
testMethod: SW-846, 6010B (Solids) Metais Analysis by ICF=-60l'o:
7440-43-9 CADMIIJM
7446-122-4 :SILyERv
Dilution
MDL EQL Factor Analvst Test Date
JMA 09/22/04
0.9 J
1.46;
ug/g
:ug/g
0:18
0,22
0:S94
0,726
1
1
MTB
MTB:
09/28/04
09/28/04
CilentSampIo ID: M636-9-64-i7
Sjample Description:: ATK-DLV-UPDES Soil Testing
Laboratory Sample ID; 0409020-29
Date SamiJied:: 09/14/04 11:28
CAS Number Test Parameter' Result Units
test Ma/hoof; SW-846,30503 ICP/GFAAMetals Digestion '
3050B ACID DIGESTION;;
TestMethod: SW-S46, BOIOB (Solids) Metais Analysisby ICP-6016"
MDL
Dilution
Factor Analvst Test Dato
JMA 09/22/04
7446^3-B CAI3MIUM
7440r22-4- SILVEPl;
CIlentSamplelD: M636-9-04-18
Sample Doscription: ATK-DLV - UPDES SbilTesling
CAS Numbor TestParameter
i;6B :ijg/g:
: 13^ ug/g
Result Units
o;i8
6:22
MDL
0:594 1 MTB 69/28/04;
6.726 1 MTB 69/28/04
Laboratory Sample ID;: 6409020-30
Date Sampled: 09/14/04 11:32
Dilution
EQL Factor Analvst Test Date
TestMethod:
Test Mothod:
7440-43-9
7440-22-4
SW-846, 30503 ICP/GFAA Metals Digestion
305QB ACID DIGESTION
SW-846, 60iOB (Solids) Metals Analysis by ICP - 6010
CADMIUM
SILVER
JMA 09/22/04
1.9
46
ug/g^
ug/g
6:18
0:22
0,594
0:726
1
i;
MTB.
MTB
09/28/04
09/28/04
ClientSampie lb: M636-9-04-19
Sample Description: ATK-DLV - UPDES Soil Testing
Laboratory Sampla ID: 0409020-31;
DateSampled: 09/14/04 11:35
CAS Numbor
Test Mothod:
TestMethod:
7440-43-9
7440-22-4
Test Parameter: Result! Units
SW-846, 30508; ICP/GFAA Metals Digesiion '
3050B /iiCID DIGESTION
SW-846, BOIOB (Solids) Metals Analysis by ICP-6010
CADMIUM
SILVER
2,87 ug/g';
121 ug/g;
bL
0:18
0,22
EQL
0,594
0.726;
Dilution
Factor
1
1
1
Analvst
JMA
MTB
MTB
Test Date
09/22/04
09/28/04
09/28/04
CIlentSamplelD:; M636-9T04r2p
Sarnple Description: ATK-DLV - UPDES Soil Testing
Laboratory Sample 10: 0409020-32
DatoSamplod: 09/14/04 11:37
CAS Nurnber Test Parariietor Resultj Units
TestMethod: SW-846,30503 1CP/C3FAAMetais Digesiion
3050B ACiD DIGESTION
MDL EQL
Dilution
Factor Analyst Tost Date
JMA 09/22/04
Page 16 of 26
Listing of Results by Sample
Sample Delivery Group:' 0409020
Client Sample ID: M636-9-04-20
Sample Descriptiori: AJK-DLV - UPDES; Soil Teslirig
Laboratory Sariipla ID: 0409020-32
DateSampled:: 09/14/04:11:37
CAS Number Test Parametei-
Tesf Method: SW-846, 6010B[(Soilds) Metals Anaiysis by ICP- 6610
7440-43^9
7440-22-4:
•CADMIUM:
SILVER-
Result
-6010
3:8:
90S
Uriits
ug/g.-
ug/g
MDL
0,18
6.22
EQL
D.594
6.726
Dilution
Factor
1'
1
Analvst
MTB
•MTB
Test bate
09/28/04
09/28/04
1 Client Sijmple ID: M636-9-p4r2r
SamploDescriptlori: ATK-DLV'- UPDES SoiiTestirig
Laboratory Sainple ID: 0409020-33:
DateSampled: 09/14/0411:42
CASNumber Test Parameter Result
Test Method: SW-846,30503 j6p/C3FAA Melals ciigasiibn
36508 ACID pIGESTIdN
TasfMathoof; SW-846, 6010S fSp/idsJ Metals Analysis by: ICPT 6010 ,
I 7440-43-9; CADMIUM
7440T22-4 SILVER
Units MDL
Dilution
Factor Analvst Test Date
MTB 09/27/04
2,1
119
:ug/g
ug/g
0;18
o;22
0,5941
;0;726.
1
1
MTB
MTB
09/28/04
09/28/04
CIlentSamplelD: M636-g-04-22
Sample Description: ATKrbtv - UPDES Soil Tesling
Laboratory Sample; ID: 0409020-34
Date Sampled: 09/14/04 14:40
CAS Number Test Parameter; Result
Test llfethod;; Si*^846,30503 ;_ ;ICP/C3FAA Metals Djgestion :
3050B ACID DIGESTION
TestMethod; SW-84e, 60108 ('So/ids) f/letajs Analysis layiCP-6010
7440-43-9 CADMIUM
7440-22-4 : SILVER
Units MDL
Dilution
EQL Factor Analyst Test Date
MTB 09/27/04
1,74
117
ug/g
ug/g
0,18
• 0,22:
0,594
0.726;:
1
• 1
MTB
MTB
09/28/04
09/28/04
CIlentSamplelD: M636-9-04-23
SampleDescriptiori: ATK-DLV - UPDESiSoil Testitig
Labdratory SamplelD: 0409020-35
DateSampled: 09/14/04 14:40
CAS Nurriber Test Parameter
reslMei/lod; SW-846,305bS IC'P/GFAA Metais Digestion
3050B ACiD DJCSESTldN
TestMethod: :SW-84B,6DiOB (Solids) Iifletals Analysis by ICP,r 6010.'
7440-43-9
7440-22-4
CADMIUM
SiLVER
Result
.rSOlO!
•t • 1 1.48
6^.7
Units
ug/g
ug/g
MDL
0.18
0,22
EQL
0,594
0.726
Dilution
Factor
1;
i
1
Analvst
MTB
MTB
MTB
Test Dato
10/27/04
09/28/04
09/28/04
CIlentSamplelD: M636-9-04-24
Sample Description: ATK-DLV - UPDES Soil Testing
Laboratory Sample ID: 0409020-36
DateSampled: 09/14/04 14:45
CAS Number
Test Method:
TestMethod:
7440-43-9
7440-22-4
Test Parametor Result
SW-846, 30503 ICP/GFAA Metals Digestion [
3050B ACID piGESTION
SW-S4fi, 60103 (So//ds| Metals Analysisby ICP - 6010
CADMIUM
SILVER
Units MDL
Dilution
EQL Factor Analyst Test Date
MTB 09/27/04
6.33
479
ug/g
ug/g
0,18
0.22
0.594
0.726
1 MTB 09/28/04
1 MTB 09/28/04
Page 17 of 26
Listing of Results by Sample
Sample Delivery Gi-oiip: 0409020
Client Sample iD: M636-9-04-25
Sample Description: ATK-DLV - UPDES Soil Testing
Laboraitbry Sample ID: 0409020-37
DateSampled: 09/14/04 14:50
CAS Number TestParameter Result^ Units
Test Mefhod;. " _SW-846ri05b3 '~^ "iCP/GF/jiAl^etals'Dige'^Uon" ; _2 _
30S0B ACID DIGESTION
Test Method: SW-846, BOIOB (Solids) Metais Anaiysis by IC P - 6010
Dilution
MDL EQL Factor Analvst Test Date
MTB: 09/27/04,
7440-43-9
7440-22-4
CADMIUM
SILVER
5,81
338
ug/g.
uglg
0.18
0,22,
0.594
0726
1
1
MTB
MTB
09/28/04
09/2S/D4
Cllerit Sample ID: M635-9-04-26
SampleDescrlption: ATK-DLV - UPDES Soil Testirig
Laboratory Sample ID: 0409020-38
Date Sanipled; 09/14/04 14:55
CAS Number TestParameter Result.' Units
TestMethod: SW-846,3050B ICP/GFAA Metals Digestion ' !
SOSOBACID DIGESTION
TestMethod: SW-S46-6diOB (Solids) MetalsAnalysisby ICP-ebio
MDL EQL-
Dilution
Factor Analvst Tost Date
MTB 09/27/04
7440-43-9 CADMIUM
7440-22-4' SILVER
Client SamplelD: M636-9-04-27
Sample Description: ATK-DLV - UPDES Soil Testing
CASNumber TestParameter
4.55 ug/g
:, 769 iig/g.; :
Result Units
0,18
0;22
MDL
e:594 1 MTB 09/28/04
6,726 i MTB 09/28/04
Laboratory Sample ID: 0409020:39;
Date Samplod: 09/14/04 15:00
Dilution
EQL Factor Analvst Testbate
TestMethod:
TestMethod:
7440-43-9'
7440-22-4
SW-846,30503 ICP/GF/iiA Metals Digestion
3050B ACID DIGESTION
SW-S46,1501103/So«ds) Melals Analysis by iCF'- 6010
CADMIUM
• SILVER '• , ,
MTB 69/27/04
10
5,36
884
ug/g-
ug/g
6.18
0:22
6:594^
0,726
"I:
1
MTB
MTB
09/28/04
69/28/04
CIlentSamplelD; M636-9-04-:28
Sample Description: ATK-DLV - UPDES Soil Tesling
l.abpratory Sample ID: 0409020-40
DateSampled: 09/14/04 15:03
CAS Number
Test Metbod:
TestMethod:
7440-43-9
7440-22T4
Test Parameter {Result- Units
SW-846,30508 ilCp/GFAA Metals Digestiori ,
3650B ACip'DIGESTiON
SW-S46, 601 OB (Solids) Metais Analysis by ICP-6010 i
MDL EQL
Dilution
Factor Analvst Test Date
CADMIUM
SILVER
5:31 ug/g
853 ug/g
0.18
0,22
0,594 1
0,726 1
MTB
MTB
MTB
09/27/04
09/28/04
09/28/04
Cliont Sample ID: M636-9-04-29
Sample Description: ATK-DLV -- UPDES Soi| Testing
Laboratory Sample ID: 0409020^41
DateSampled: 09/14/04;15',05
CAS Number Test Parameter Result I Units;
TestMelhod: SW846, 30503 icP/GF/V^ Metals Digestion
3050B ACID DIGESTION
MDL EQL
Dilution
Factor Analyst Test Date
MTB 09/27/04
Page 18 of 26
Listing of Results by Sample
Sample Delivery Group; 0409020
Client SamplelD: M636-9-04-2g
Sample Descriptipn: AtK-DLV - UPDES StpilTesling
Laboratory SamplelD: 0409020-41
DateSampled: 09/14/04 15:05
CAS Ntimber TestParameter Result Urilts
test Methoci; SW-84Bi BOIOB (Solids) MeiaisAnalysis by ICP-6010
Dilution
MDL EQL Factbr Arialvst TestPate
7440-13-9
7440-22-4
CADMIUM
SILVER
• -6010|
4.41
473
:Ug/g
ug/g
6.18
6.22
;e.594
0.726
1
1
MTB
MTB
09/28/04
09/28/04
CIlentSamplelD: Mi636-9-04-30
Sample Description:; ATKrDLV - UPDES Soil Teslirig
Laboratiary Sample ID: 0409020-42
DateSampled: 09/14/04 15:08
CAS Number
TestMethod;
TestMethod:
7440^3-9
7440-22-^4
Test Parameter Result: Units
SW-84S,3050B ' " rCf?7GFAA"MetJs_bige^^^^ "
3050BA(3ib DIGESTION 1
SW-846, BOIOB (Solids) li)leUlsAnaiysisbylCP-66lO | '
Dilution
MDL EQL Factor Analvst TestPate
CADMIUM
SILVER'
5:83 ug/g
890: ug/g
0:i8
0.22
0.594 1
0.726 1
MTB
MTB
MTB
09/27/04
09/28/04
09/28/04
Client Sample ID: M636r9-04-31
Sample boscrlpt|on:: ATK-DLV - Uf'DES Soil testirig
Laboratory Sample ID: 0409020-43
Date Siampled: 09/14/04 15:13
•I
CAS Number Test Parameter Result Urilts
TesfMefhod: iSW846,30508 itP/GFAA Metals DigesUon
3050B ACiD DIGESTION
TestMelhod: SW-846, WiOB (SoBdsj luletals-Analysls by ICP - 6010
7440-43-9: CXDMIUM;
7440-22-4 SILVER
Dilution
MDL EQL Factor Analvst Test Dale
MTB 09/27/04
6;09
1380
ug/g.
>jg/e;
6:18
:P^?2
6.594:
e;726:
r
• i;
MTB
MTB
09/28/04
09/28/04
Client Sample ID: M636-9-04^32
Sample Description: ATK-DLV - UPDES Soli Testing
Laboratory Sample ID: 0409020-44
DateSampled; 09/14/04 15:19
CAS Number
Tos/Mofhod;
Tesf Method:
7440-43-9
7440-22-4
Test Paramoter Rosulti Units
'SW-S46, 30503 iCP/dPAA Metals Digestion
30508 ACiD DIGESTION
SW-846, eiOiOB (Solids) " 'MeiaisAnalysis by ICR-^010
Dilution
MDL EQL Factoi^ Analvst Test Date
MTB 09/27/04
'|-CADMIUM
SILVER
10;9
704
ug/g
ug/g
0,18
6.22
0,594;
0.726
1
1
MTB
MTB
09/28/04
09/28/04
CIlentSamplelD: M636-9-D4-33
Sariiple Description; ATK-DLV-UPDES Soil Testing
Laboratory Sample ID: 0409020-45
DateSampled: 09/14/04 15:21
CAS Number
TestMethod:
Tost Method:
7440-43-9
7440-22-4
Test Parameter Result Units
SW-e46, 30503 ICP/GFAA Metals Digestion '
;3050B ACID DIGESTION
SW-845, 60103 (Solids) Metals Analysis by ICP - 6010 i
CADMIUM
SILVER
Dilution
MDL EQL Factor Analvst Test Date
MTB 09/27/04
5.9
696
ug/g
ug/g
0.18
0,22
0.594
0.726
1 MTB 09/28/04
1 MTB 09/28/04
Page 19 of 26
Listihg of Results by Sample
Sample Delivery Group: 0409020
Client SamplelD: M636-9-04-34
Saniple Description:: AtK-DLV - UPDES SoilTesting
Laboratoty Sample |D: 0409020-46
DateSampled: 09/14/04 15:25;
CAS Number
Test Mofhod;'
Test Parameter
•SW^W6,3^
30506 ACID DIGESTioi»i
Result Units
iCP/GF/V!k Metals pigestion
Dilution
MDL EQL Factor Analvst Test Date
MTB 09/27/04
TestMelhod: SW-i46, 601 OB (Solids) MBtaisAnaiyslsbyiCP-SOlb
7440-43-9
7440-22-4
CADMIUM
SILVER;
5,28
284
ug/g
ug/g
0,18
0.22
10.594
0:726
1
1
MTB
MTB
09/28/04
09/28/04
Client Sample ID: M636-9-04-35
Sample Descriptipn:; ATK-DLV - UPDES SbilTesiing
Laboriatory Sample ID: 0409020-47
Dato Sampled: 09/14/0415:29
CAS Number Test Parameter
TestMefhoc/; SW-S46,30508 ICP/GFAA Metals Digestion
30508 ACID biGESTION
TesilMethod: SW-846, 601 OB (Solids) Metals Analysis by ICP -6010
7440-43-9 CADMIUM
7440-22-4: SiLVER
Result
stion
-6010
1..1J
172
Units
ug/g
ug/g
MDL
0.18
0:22
EQL
o:S94
0.726
Dilution
Factor
1
1
1
Analvst
MTB
MTB
MTBi
Test'Datie
09/27/04
09/28/04
:09/28/04
CIlentSamplelD: M636-9-b4-36
Sample Descrlptibn: ATK-DLV-UPDES SoilTesting i
Labdratory Sample ID: 0409020-48
Date Sampled: 09/14/0415:33
CAS Number
resfMef/ibd;
TestMethod:
7440-43-9
7440-22-4
TestParameter Result Units
SW-846,^3d^B _ ' li:P/6F/UMelalsbigestion
;3050B ACID DIGESTION
SW-846iBDibB (Solids) Metais Analysis by ICP-6010
CADMIUM
SILVER
1.57
218
ug/g
ug/g
DL
0:18
0.22
EpL
0.594
0.726
Dilution
Factor
1
1
1
Analvst
MTB
MTB
MTB
Test Date
09/27/04
09/28/04
09/28/04
CIlentSamplelD: M636-9-04.37
Sampie Description: ATK-DLV - UPDES Soil Testing
Laboratory Sampio ID; 0409020-49
DateSampled; 09/14/04 15:35
CAS Number
TestMethod:
TestMethod:
7440-4379'
7440-22-4
Test Parameter Result Units
SW-84S,365dB ICP/GFAA Metais Digestion
3050B ACID DIGESTION
SW-846, 60103 (Solids) Melals Analysis by ICP - (3010
MDL
CADMIUM
SILVER
2.21
93.8
ug/g
ug/g
o;i8
0.22
EQL
0:594
0,725
Dilution
Factor Analyst Test Date
MTB
MTB.
MTB
09/27/04
09/28/04
09/28/04
Client Sample ID: M636-9r04-38
Sample Doscription: ATK-DLV - UPDES Soil Testing
Laboratory Sample IP: 0409020-50
Date Sariiplod: 09/14/04 15:38
CAS Number Test Parameter Result Units
Test Metiiod: SW-846,30503 1CP/GF/^A Metals Digestion '
3050B ACID DiGESTlON
MDL
Dilution
Factor Analvst Test Date
MTB 09/27/04
Page 20 Of 26
Listing of Results by Sample
Sample Delivery Group: 0409020
Client Samplb ID: M636r9r04-38
Sample Description: ATK-DLV - UPDES Soil testing;
Laboratory Sample:ip: 0409020-50
bate Sampled: 09/14/04 15:38
CAS Number
TesfMefhod;:
7446^3-9
7440-22:4
Test Paratneter
SW-84i BOIOB (Soildsj
CADMIUM
SILVER
Result I Units
Metals-Analysis by ICP-6010 |
I.J
15,3;
ug/g
ug/g
MDL
0,18
0.22
Dilution
EQL Factor Analvst test Date
0,594
0:726
MTB
MTB
09/28/04
09/28/04
ClientSampie ID: M636-9-04-39;
SiamploDesci-lption: ATK-DLV- Ui^iDES Soil Testing
Laboratory Sample ID: 0409020-51
DateSampled: 09/14/04 15:41
CAS Nuinber -TestParameter Result Units
Test Meihod: :SW-846,;30SOB ICP/GFAA Melafs Digestion
30506 ACID DIGESTION
tesiMethod; SW-'846760l'0B (Solids) '7^iaisA^aly^is;bylC(»-^oio 1
7440^43-9 CADMIUM
7440-22-4 SILVER
MDL
Dilution
EQL Factor Analvst Test Date
MTB 09/27/04
o,4;j
26,7
ug/Q
ug/g
0.18
0.22
6:594
0,726
• -
1
1
MTB
MTB
09/26/04
09/28/04
CIlentSamplelD: M636-9-04.-40
Sampip Descriptipn: ATK-DLV - UPDES Soil Testing
LaiJbratoiy Sample ID: 0409020-52
Date Sampled: 09'14/04 15:45
CAS Number TestParameter Result Units
resf Meihod;: SW-^846,30503 ICP/GFAA Metals Digestion ,
;3050B ACID DIGESTION
Tesf Malhod; SW.846, 60108 (So/idij MetalsAnalysisby ICP-60101
7440-43-9 CADMIUM
7440:22-4 SILVER
MDL
Dilution
EQL Factor Analvsit Test Data
MTB 09/27/04
0,6iJ
;37
ug/g
:U8/g
0.18
0.22
0:594
0:726
1
1
MTB
MTB
09/28/04
09/28/04
Cliont Sample IP: M636-9-04-41
Sample Descriptipn: ATK-DLV - UPDESSoil Testing
Laboratory Sample ID: 0409020-53
Date Sampled: 09/14/04 15:48
CAS Number TestParameter
TesiMethod: SWrSiB, 3050B ICP/GFAA Metols Digestion
3050B ACID DIGESTION
TestMethod: SW-846, 60103 fSoffds} Metais Analysis byiCP-6016,
7446.43-9 CADMIUM
7440-22-4 SILVER
Result
1-6016,
ju
0.46 J
Units.
ug/g
ug/g
MDL
"
0,18
0,22
EpL
0:594
0,726
Dilution:
Factor
:1,
1
1
Analyst
MTB
MTB
MTB
Test Date
69/28/04
10/13/04
10/13/04
CIlentSamplelD: M636-9-04-42
Sample Description: ATK-DLV - UPDES Soil Testing
Laboralory Sample ID: 0409020-54
DateSampled: 09/14/04 10:45
CAS Number
TesfMefhocf;
TesfMefhod;
7440^3-9
7440-22-4
Test Parariioter Result Units
SW-846, 305(16 iCP/dpAA Metals digesiion
3050B ACID DIGESTION
SW-S46, 60103 (Solids) Metals Analysis by ICi° - 6010-
MDL
CADMIUM,
SILVER
1.6 ug/g
13.6 ug/g
0,18
0.22
EQL
0.594
0;726
Dilution
Factor Analvst Test Date
MTB
MTB
MTB
03/28/04
10/13/04
10/13/04
Page 21 of 26
Listing of Results by Sample
Sample Delivery Group: 0409020
Client Sample lb: M636-9-04-43
Sample bescriptipn: Atk-OLv - UPDES:S6il testing
Laboratory Sample ID: 0409020-55
DateSampled: 09/14/04 11:17
CAS Number
test Method-
Test/iiefhod:
7446r43-i9
7440-22-4
Test Parameter Result
:SW-846,30503 ICP/GFAA Metals Digestion
3050B ACID DIGESTION
SW-846, i;oi()B:(fSol/ds) "li/letais Ariaiysis by ICP - 6010
Units MDL
Dilution
EQL Factor Analvst Test Date
CADMIUM
SILVER
1.48
21.5
ug/g
ug/g
0.18
0.22
0.594
0.726
MTB
MTB
MTB
09/28/64:
10/13/04
10/13/04
Client Sami)le iD: M636-9r04-44
Sample Doscription: ATK-DLV - UPDES Soil Tesling
Laboratory Sample ID: 0409020-56
DateSampled: 09/14/04 14:40
CAS Nlumber Test Parameter Result Units
Test Meihod: SW-846,3050i ICP/GFAA Metals Digesiion
3050B ACID DIGESTION
Tesf Metfiod: SW-846,WiOB (Soiids) MetalsAnalysisby ICP-66l0
7440-43-9 CAblUllUM
7440-22-4- SILVER
.MDL
Dilution
Factor Analvst Test Date
MTB 09/28/04
1,71
82:8
ug/g
ug/g
0:18
0.22
0:594
6:726-'
1
1
MTB
MTB
16/13/04
10/13/04
Clldrit Sample ID: M636-9.-04-45
Sample Description: ATK-DLV - UPDES Soil Testirig
Laboratory Sample ID: 0409020-57
Date Sampled; 09/14/04 15:21
CAS Number
Tos ("Meth oci:
TesfMefhod;
7440^3-9
7440-2i-4:
Test Parametar Rosult
SW-846,305(13 ICP/GFAA Metais Digestion
36568 ACID DIGESTION
SW-84B, BOIOB (Solids) Metals/kiialysis by ICP-6010
CADMIUM 5.51
SILVER . :63.5
Units
•_...
ug/g
ug/g
MDL
Dilution
EQL Factor Analyst Test Date
MTB 09/28/04
•0-18
'6:22
6:594 1
6.726: 1
MTB
MTB
10/13/04
10/13/04
CllentSariiplelD: M636-904-TB1
Sampie Description: ATK-DLV - UPDES Soil Testing
Laboratory Sampio ID: 0409020-58
DateSampled: 09/14/04 14:30
CAS Number
Tosf Method;
Test Method:
7440-43-9
7440-22-4:
Test: Parameter
SW-846,301PA MetalsDigestion
3010A ACID DIGESTION
SW-846, 6016B (Water) Melals Analysis by ICP - 6010
CADMIUM;
SILVER
Result Urilts MDL
Dilution
EQL Factor Analvst Test Date
:U ug/L
'U ug/L
3.7
2.2
12.21
7.26
MTB
MTB
MTB
10/04/04
10/06/04
10/06/04
ClioritSampielD: M636-904-EB1
Sartiple Description: ATK-DLV - UPDES SoilTesting
Laboratory Sarriple ID: 0409020-59
DateSampled: 09/14/04 10:41
CAS Number Test Parariieter
TeslMcilliod; SW-846,30JOA MetalsDigestion
30iOA ACID DIGESTION
Resultl Units MDL EQL
Dilution
Factor Analvst Test bate
MTB 10/04/04
Page 22 of 26
Listing of Results] by Sample
Sample Delivery Group: 0409020
Client SamplelD: M636:904-EB1
Sample Description: ATK-DLV - UPDES Soil Testing ^
Laboratory Sample ID: 0409020-59
Date Sampled: 09/14/04 10:41
CAS Number
TestMethod:
7440-43-9
7440-22-4
Test Parariieter
SW-B46,6Q10B (Water)
CADMIUM
SILVER
Result
Metals Analysis by \CP~ 60t0
U
U
Units
ug/L
ug/L
MDL
3:7
2.2
Dilution
EQL Factor Analvst Test Pate
12.21
7.26
MTB
MTB
16/06/04
10/06/04
Client Sample ID: M636-904-FB1
Sample Description: ATK-DLV - UPDESSoil testirig
Laboratory Sample ID: 0409020-60
Date Sampled: 09/14/04 10:41
CAS Number
TesfMefhod;
TestMethod:
7440.-43:9,
7440-22:4
TestParameter
SW-84B,3010A 'i^elals Digestiori^
3pipA AC|D DIGESTION
SW-846,60108 (Water; Metala Anaiysis by ICP - 6010
CADMIUM
SILVEIR:
Restilt Units MDL
Dilution
EQL Factor Analvst Test Date
MTB •10/04/04
u
u
ug/L
ug/L
3:7
2:2
12:21
7.26;
1.
1
MTB
MTB
10/06/04
10/06/04
Client Sample ID:; M636-904-TB2:
Sample bescripitlon: ATK-DLV - UPDES Soil Testing
Laboratory Sample ID: 0409020-61
Date Sampled: 09/14/04 14:30
CAS Numbor
Test Method:
TestMethod:
7440-43-9
7440-22-4
Tost Parariieter
SW-84B,3010A Mstals Digestion
3010A ACIDDIGESTION
SW-84S, 6010B (Water) Melals Analysisby ICP - 6010
CADMIUM
SILVER
Result Units MDL
Dilution
EQL Factor Analvst Test Date
MTB 10/04/04
u
i!>
ug/L
•ug/L
3.7
2.2:
12.21
7.26
1
1
MTB.
MTB
10/06/04
10/06/04
CIlentSamplelD: M636-904-EB2
Sample Dbscriptlpn: ATK-DLV- UPIDESSbil;Testing;
Laboratory Sampio ID: 0409020-62
DateSampled: 09/14/04 11:12
CAS Number Test Parameter
TestMethod: SW-846,30iOA MetalsDigestion
3010A ACID DKBESTION;
TestMethod: SW-B46, BOIOB (Water) Metals Anoiyiis by iCP-6010
7440-43-9 CADMIUM
7440-22-4 SILVER
Result'
-6010
• • •
U
u
units
ug/L
ug/L
MDL
3.7
2:2
EQL
12,21
7,26
Dilution
Factor
1
1
1
Analvst
MTB
MTB
MTB
Test bate
10/04/04
10/06/04
10/06/04
Client Sample ID; M636-904-FB2
Sample Description: ATK-DLV - UPDES Soil Tesling
l.aboratory Sampla IP: 0409020-63
Date Sampled: 09/14/04 11:12
CAS Nuriiber
Tesfiifefhod;
Test Mtsihdd:
7440-43-9
7440-22-4
Tost Parameter
SW-646, 30)04 ; Metais Digestion
3010A ACID DIGESTION
SW-846, 60103 fWa(er) Metals Ariaiysis by ICP-6O1O
CADMIUM
SILVER
Result Units MDL
Dilution
• EQL Factor Analvst Test Date
U ug/L
U ug/L
3,7
2,2
12,21
7:26
1
1
1
MTB
MTB
MTB
Page 23 of 26
10/04/04
10/06/04
10/0S/04
Listirig of Results by Sample
Satiiple Delivery Group: 0409020
Client Sample ID: M636-904-TB3
Sample Description: ATK-DLV - UPDES ;Soil Testing
Laboratory Sannple ID; 0409020-64
DateSampled:: 09/14/0414:30
CAS Number Test Parameter Result Units
: Tost Method: SW-846,3010A MetalsDigestion
3010A ACID DiGESTlON
TestMethod:. SW-846, 601 OB (Water) MetalsAnalysisby ICP-6010
7440-43-9 CADMIUM
7440-22-4 SILVER
Dilution
MDI, EQL Factor Analvst Test Date
U ug/L
U ug/L
3.7
2:2
12:21
7:26
1
1
1
MTB
MTB
MTB
-10/04/04
'10/06/04
10/05/04
Client Saniple ID: M636-^904-EB3
Sample Description: ATK-DLV-UPDESiSoil TesUng
Laboratoiy Sample ID: 0409020-65
DateSampled: 09/14/04 11:48
CAS Number Test Parameter
Tesf/ifefhDd; SW-84B,3010A MetalsDigestion
;3010A ACID;DiGEStl6i>l
TestMethod: .SWr84B, BOi OB (Water) MetalsAnalysisby ICP - 6010;
7440-43-9; CADMIUM
7440-22-4 SILVER
Result Units
Dilution
MDL EQL Factor Analyst Test Dato
MTB 10/04/04
u u
ug/L
ug/L
3:7
:2:2
12.21
7.26
1
1
MTB:
MTB
10/06/04
10/06/04
ClientSampielb: M636:904-FB3
Sampte Descrlptibn: ATK-DLV - UPDES Soil testing
Laboratory SamplelD: 0409020-66
Date Sampled;: 09/14/04 11:48
CAS Numbor
test Method:
TestMethod:
7440-43-9
7440-22-4
Test Parameter
SW-846,3010A ;Meials Digestion
SpiOA ACID DIGEStiON:
SW-SA6,6010B (Water) Metals Analysis by ICP-6010
CADMIUM
SILVER
Ftesult Units
Dilution
MDL EQL Factor Analyst: Test Date
MTB 10/04/04
u 6.
ug/L
ug/L
37
2:2
12.21
7,26
1
1
MTB
MTB
10/06/04
10/06/04
ClientSampie ID: M636-904-tB4
Sampio Description: ATK-DLV- UPDES Soil tesling
Laboratory Sample ID: 0409020-67
Date Sampled: 09/14/04 14:30
CAS Number TestParameter
TesfMefhod; SW-i46,3010A MetalsDigestion
30l0AACIDDIGESfl6N
Test iWefhod; SW-846, 60108 (IVater) ;Metals Analysis tjy ICP - 6010
7440-43-9 CADMIUM
7440-22-4 SILVER
Result
-6010
u
-1
Units.
ug/L
ug/L
MDL
3:7
2.2
EQL
12.21
,7,26
Dilution
Factor
1
1
1
Analyst
MTB
MTB
MTB
TcJst Date
10/04/04
10/06/04
10/06/04
CIlentSamplelD: M636Tg04-EB4
Sample Description: ATK-DLV - UPDES Sciil Testing
Laboratory Sampio ID; 0409020-66
DateSampled: 09/14/04 13:15
CAS Number TestParameter
TestMethod: SW-846,3010A Metais Cligesiion
3010A ACiD DIGESTION
Res Uit I Units MDL
Dilution
Factor Analvst Test Date
MTB 10/04/04
Page 24 of 26
Listing of Results by Sample
Sarnple Delivery Group: 0409020
Client Sample lb: lyl636-904-EB4
Sample Descrlptioh: ATK-DLV - UPOESSoilTestirig
Laboratory Sample ID: 0409020-68
Date Sampled: 09/14/04 13:15
CAS Number
TesfMefhod;
7440-43-9
7440-22-4
Test Parameter
SW:84I6, 60103/Walor;
CADMIUM
SILVER
Result
Metais Analysiis by ICP- 60,10
iu^-
jU
Urilts
ug/L
ug/L
Dilution
MDL EQL Factor Analyst Test Date
3.7:
2:2
12:21
:7;26
MTB
MTB
10/06/04
10/06/64
Client Sample ID: M636-904-FB4
Sampio Descriptipn: ;ATK-IDLy;- Ut^DES Soil Testirig
Laboratory Saniple ID: 0409020-69
bate Sampled: 09/14/04 13:15
CAS Number: Test Parameter
TestMethod: Siiii-846,36ibA: Metals Digestion
3016A ACID piGESTION
Test Mefhoii: JSW-846, 6010B (Wafer) Metals Analysis by ICP - 60i6
7440-43-9: CADMIUM:
7440-22-4 SILVER
Result Units MDL
Dilution
EQL Factor Analvst Test Date
MTB 10/04/04
IU
iU
ug/L
ug/l.
37
2.2
12.21
7:26
1.
1
MTB
MTB
10/05/04
10/06/04
Page 25 of 26
Data Reporting Qualifiers
U Iridicates that the:ana|yte was riot detected, or tlie analyte was detected but
was beloyy the iWDL.
B This flag is used vvheh an analyle is found In the blank as well as the sampie.
J Iridicates ^n esfimated value. This flag is used either when estimating a
cdhcentration for; tentatively identified compounds di' when the data; indicated
the:presence ofa (ibrnpound that itieets the ideritification criteria but the
result is less than the EdL (e.g. ;3 J with an EQL of 10).
MDL Metiiod Detection Limit; The;minimum:concentratibn of a substance that can be
confidently measured and repprted. j The laboratory-lias derrionstrated that the
MDL can be achieved in a laboratory reagentblank, but does not guarantee it
cari be achieved'in all sample matricies.
EQL Estiriiated Quantitation Liniit: The EQL generally isS to iO times the; MDL. For
many analytes the EQL.is selecteida's'the value ofthe lowest standard in the:
calibration curve;
Diiution Dilultion Factor: the prepared sample was diluted by this:factor because the
Factor sample was too concentrated or due Ito other int^rferericies in the sample matrix,
Any dilution factor causes a corresponding increase, in the MDL and EQL.
Page 26 of 26
CERTIFICATE OF ANALYSIS
Listing of Sarnple InfoTOation and Testing Requested
Thursday, October 2i, 2004
TESTED FOR: ATK Thiokol: DLV
Environmental Monitoring
MS 301
thiokol Corp, UT 84322
ANALYZEDBY: ATK Thiokol Propulsion
Environmental Laboratory
P.O. Box 707, M/S 245
Brigham Gity, UT
84302-0707
435-863-3732
435-863-8080
Contact Name:
Project:
Sample Delivery Group:
John Holladay
: UPDES-DLV
0409046
Page 1 of22
Sample peiivery Group: 0469046:
Sample No. Client No.
Test Requested
0409046-01 M39-9-04-01
Sample Desciiiption
Received Collect Date/Time
IVIatrix
09/29/04 9/14/2004 09:45:00
EPA314,0
0409046-02 M39-9-04-02
EPA 314.0
: 0409046-03 M39,:9-p4-03
- Periihidrate - Ion Chromatography
Perchlorate - lori Chromatography
Soil
•09/29/04 9/14/2004 09:50:00
Soil
09/29/04 9/14/2004 09:55:00
EPA 314.0 Perchlorate - Ion Chromatography Soil
0409046-04 M39-9-04-04
EPA 314,0
0409046-05 M39-9-04-05
I
Perchlorate - |on Chromatography
09/29/04 9/14/2004 10:00:00
Soil
09/29/04 9/14/2004 10:05:00
EPA 314:0 Perciliorate - lon Chromalography Soil
i 0409046-06 M39-9-04-06
EPA314.b
0409046-07 M39-9-04-07
Perchlorale-ion Chromatography
09/29/04 9/14/200410; 10:00
Soil
09/29/04 9/14/2004 10:13:00
EPA 314,0
0409046-08 M39-9-04-08
EPA 314.0
0409046-09 M39-9-04-09
Pei'chlorat'e - lon Chromatography
Pisrchlorate;- Ion Chromatography
Soil
09/29/04 9/14/2004 10:15:00:
Soil
09/29/04 9/14/2004 10:05:00
EPA3U:0 Perchl6rale;r lon Chrbmatbgraphy; Soil
0409046-10 M39-9-04TB
EPA 314.0
0409046-11 M39-9-04EB
Perchlorate - ion Chromatography
09/29/04 9/14/2004 09:30;00
Water
09/29/04 9/14/200409:50:00
EPA'314,0 Perchlorate - lon Chromatography Water
0409046-12 M39-9-04FB
EPA 314,0
0409046-13 M636-9-04-01
ERA314.0.
09/29/04 9/14/2004 09:50:00
'Perchlorate - lon Chrornatography Water
09/29/04 9/14/2004 10:54:04
Perchlorate - Ion Chromalography Soii
Page 2 of 22
Sample Delivery Group: 0409046
Sample No. Client No.
Test Requested
j 0409046-14 ivi636-9-04-02:
Sariiple Description
Received CollectDate/Time
Matrix
09/29/04 9/14/2004 10:43:04
I
EPA 314.0 Perchlorale - Ion Chroriiatography Soil
0409046-15 M636-9-04-03 09/29/04 9/14/2004 10:45:04 I
EPA314.0 Perc;hlorate - Ion Chromatpgrapiiy Soil
0409046-16 M636-9-04-04 09/29/04 9/14/2004 10:50:04
EPA 314,0 Perchlorale - Ion Chromatography Soil
0409046-17 M6?6:9-04-05
EPA 314.0
0409046-18 M636-9-04-06
Perchiorate - ion Chromalography
-09/29/04 9/14/200410:54:04
Soil
.09/29/04 9/14/2004 11:00:04'
EPA 314.0 Pefciilbrate - Ion Chrdniatography Soii
0409046^19 M636=:9-04-07
EPA314:0
0409046-20 M636::9-04-08,
Perchlorale-Ton Chromatography
09/29/04 9/14/2004 11:02:04
Soil
09/29/04 9/14/2004 11:04:04:
EPA314,0
0409046-21 M636-9-04.P9
Perchlorate,- Ion Chromatography
1
So
09/29/04
1
9/14/2004 11:06:04
EPA 314,0
0409046-22 M636-9-04-10
Perchlorate - lon Chromalography Soil
09/29/04 9/14/2004 11:08:04
EPA314,0 Perciilprale - lon Chromalography Soil
0409046-23 M636-9-04-11 09/29/04 9/14/200411:10:04
EPA 314.0
0409046-24 M636-9-04-12
Perchlorale - lon Chromatography Soil
09/29/04 9/14/2004 11:15:04
EPA314,0
EPA314.0
0409046-25 M636-9-04-14
Perchlorale - Ion Chromatography Soii
0409046-25 M636-9-04-13
I
Perchlorate - lon Chrornatography
09/29/04 9/14/2004 11:17:04
Soil
09/29/04 9/14/2004 11:18:04
EPA 314,0 Perchlorate -Ion Chromatography Soil
Page 3 of 22
Sample Delivery Group: 0409046
Sample No. Cllerit No.
TestRequested Sampie Description
0409046T27 M636-9-04-15
Received Collect Date/Time
Matrix
09/29/04 9/14/2004 11:22:04
EPA 314.0 Perchlorate - lon Chroriiatography Soil
0409046-28 M636-9-04-16:
EPA 314.0
0409046-29 M636-9-04-17
Perchlorate - ion Chromalography
09/29/04 9/14/2004 11:26:04
Soil
09/29/04 9/14/2004 11:28:04
EPA 314.0 Perchlorale - ion Chromatography Soil
0409046-30 M636-9-04-18 I
EPA 314.0
I 0409046-31 M636-9-04-19
Perciliorate-Ion Chromalography
09/29/04 9/14/2004 11:32:04
Soil
09/29/04 9/14/2004 11:35:04
EPA314:0 Perchlorate T lon Chromalography Soil
0409046-32 M636-9-04-20 09/29/04 9/14/2004 11:37:04
EPA314;0
! 0409045-33 M636.9-04-2T
Perchlorate-Ion Chromatography Soil
09/29/04 9/14/200411:42:04
EPA314;0 Perchlorale - Ion Chromatography Soil
0409046-34 M636-9-04-22
EPA 314,0
0409046-35; M636-9-04-23
Rerchlorate - Ion Chromatography
09/29/04 9/14/2004 14:40:04
Soil
09/29/04 9/14/2004-14:40:04
EPA314,0 Perchlorale - Ion Chromatography Soil
0409046-36 M636-9-04-24
EPA314,0 Percfi|brate - lon Chromatography
09/29/04 9/14/2004 14:45:04
Soil
0409046-37 M636-9-04-25 09/29/04 9/14/2004 14:50:04
EPA 314,0 Peirchlorate - Ion Chromatography Soil
0409046-38 M636-9-04-26 09/29/04 9/14/2004 14:55:04 I
EPA314,0
0409046-39 M636-9-04-27
Perciliorate - lon Chromatography
_J
Soil
09/29/04 9/14/2004 15:00:04
EPA 314.0 Perchlorate - Ion Chromatography Soil
Page 4 of22
Sample Delivery Group: 0409046
Sample No. Client No.
Test Requested
0409046-40 M636-9-04-28
Sample Description
Received Collect Date/Time
Matrix
09/29/04 9/14/200415:03:04
EPA 314:0 Perchjprate - lon Chromatography Soil
0409046-41 M636-9-04-29 09/29/04 9/14/2004 15:05:04
EPA 314,0
0409046-42 M636-9-04-30
Perc;hlorate- Ion Chromalography Soil
09/29/04 9/14/2004 15:08:04
EPA 314.0 Perchlorale - Ion Chromatography Soil
0409045-43 M636-9-04-31 09/29/04 9/14/200415:13:04
EPA 314.0
I 0409046-44 M636-9-04-32
Perchlorate - lon Chromatogi-aphy Soil
09/29/04 9/14/2004 15:19:04
EPA 314,0 Perchlorate-loh Chromalography Soil
0409046-45 M636-9-04-33 09/29/04 9/14/2004 15:21:04
EPA 314,0 Perchlorate • lon Chrbmatbgraphy
0409046-46 M636-9-04-34
Soil
09/29/04 9/14/2004 15:25:04
EPA 314.0 ;Pei;chlorate- Ion Chroriiatography Soil
0409046-47 M636-9-04-35 09/29/04 9/14/2004 15:29:04
EPA 314,0 Perchlorate - Ion Chromalography
0409046-48 M636-9-04-36
;Sdil
09/29/04 9/14/2004 15:33:04
EPA:314.0 Perchlorate - Ion Chromatography Soil
0409046-49 M636-9-04-37
EPA 314:0 Perchlorate - Ion'Chromatography
0409046-50 M636-9-04-38
09/29/04 9/14/2004 15:35:04
Soil
09/29/04 9/14/200415:38:04
EPA 314,0 Perchlorale - lon Chromatography
0409046r51 M636-9-04-39
Soil
09/29/04 9/14/2004 15:41:04
EPA 314,0
0409046-52 M636-9-04-40
Perchlorale - ion Chromatography Soil
09/29/04 9/14/2004 15:45:04
•
EPA 314.0 Perchlorate - lon Chromalography Soil
Page 5 of 22
Sample Delivery Group: 0409046;
Sample No. Client No.
Test Requested Sample Description
Received Collect Date/Time
Matrix
0409046-53 iyi636-9-04-41 09/29/04 9/14/200415:48:04
EPA 314.0 Perchlorale - Ion Chromalography Soil
0409046.54 M636-9-04-42 09/29/04 9/14/200410:45:04
EPA 314:0 Perchlorate - lon Chromatography Soil
0409046-55 M636-9-04-43 09/29/04 9/14/2004 11:17:04
EPA 314,0 Perchlorale - Ion Chromatography Soil
1 0409046-56- M636-9-04-44
EPA314.0 Perchlorate - lon Chrornalbgraphy
09/29/04 9/14/200414:40:04
Soil
0409046-57 M636-9-04-45 09/29/04 9/14/200415:21:04
EPA 314.0 Perchlorate - Ion Chrpmatpgraphy Soil
0409046-58 M636-904TB1 09/29/04 9/14/200414:30:04
EPA314;D Perchlorate - lon Chrornatography Water
0409046-59 M636-9Q4EB1 09/29/04 9/14/2004 10:41:04
EPA314.0 Perchlorate - lon Chromatography Water
0409046-60 M636-904FB1
EPA314.d
0409046-61 M636-904TB2
09/29/04 9/14/2004 10:41:04
Perchlorale - lon Chrornatography Waler
I
EPA314.0 Perchlorale - Ion Ctirornatography
09/29/04 9/14/200414:30:04
Water
0409046-62 M636-904EB2
EPA 314-0 Perchlorate - Ion Chromatography
09/29/04 9/14/2004 11:12:04 I
Water
0409046-63 M636-904FB2 09/29/04 9/14/2004 11:12:04
EPA 314.0
0403046-64 M636-904TB3
EPA314,0
0409046.65 M636-904EB3
Perchlorate r lon Chromatography Waler
Perchlorate - lon Chromalography
09/29/04 9/14/200414:30:04
Waler
09/29/04 9/14/2004 11:48:04
EPA 314.0 Perchlorate - lon Chromatography Water
Page 6 of 22
Sample Delivery Group: 0409046
Sampie No. Client No.
Test Requestied;
, 0409046-66 M636-904FB3
Sample Desicription
Received Collect Date/Time
Matrix
09/29/04 9/14/2004 11:48:04
EPA3T4:0 I 'Peri::hlorate - lon Chromatography Waler
0409046-67 M636-904TB4 09/29/04 9/14/2004 14:30:04
EPA314.0
0409046-68 M636-904EB4
Perchlorate - lon Chromatography Waler
09/29/04 9/14/2004 13:15:04
EPA 314,0 Perchlorale - lon Chromatography Water
0409046-69 M636-904FB4
EPA 314,0
0409046-70 M636-9-04-46
Perchlorate - lon Chromalography
09/29/04 9/14/2004 13:15:04
Water
09/29/04 9/14/2004 10:50:04
EPA,314.0
SW-846, 3050B
SW-846. 601 OB (Solids)
0409046-71 M636-9-04-47
Perchlorate - Ion Chromalography.
ICP/GFAA Metals Digestion
Metals Analysis by ICP -6010
Soil
Soil
Soil
09/29/04 9/14/2004 11:26:04
EPA;314,0
SW-846,3050B
SW-846.-60ipB (Solids)
0409046-72 M636-9-04-48
Perchlorate- Ion Chromatography
ICP/GFAAMetals DigestiiDn
Metals Analysis by ICP - 6010
Soil
Soii
Soil
09/29/04 9/14/2004 15:08:04
EPA314.0
SW-846, 3050B
SW-846. 601 OB (Sol|ds)
Perchlorate-Ion Chromatography •
ICP/GFAA Metals Digestion
Metals Analysis by ICP -60lb
Soil
Soil
Soil
0409046-73 M39-9-04-10 09/29/04 9/14/2004 09:50:04
EPA314:0
;SW-846, 3050B;
Perchlorate -ibh Chromatography
ICP/GF/\A Metals Digestion
Soil
Soii
Page 7 of 22
Sample Delivery Group: 0409046
Sample Nb. Client No.
TestRequested
0409046-73 M 39^9-04-10
I
Sample Description
Received Cpllect Date/Time
Matrix
09/29/04 9/14/2004 09:50:04
SW-846, 601 OB (Solids) Metals Anaiysis by iCP • 601O Soil
Cornments: I
Samples were submill^d'iriltially for metals ariaiysis without perchlorate testing, F'erchibrate analysis was requested al a
later data by this time tiie walersamples Had been acid fixed. [The acid fixed caused the samples to have ahjgh back
ground conductivity and a 10 foid cJilution was required to bring the bac:kground conductivity down to acceptable levels for
perchlorale testing.
Certified By: sionaiinuvow liMA ip^ 10/22/2004
W. Scott Fraser, Quality Assurance Officer Date
This certifies that tlie following samples were analyzed using good laboralory practices to show (he following i-esults:
Page 8 of 22
Listing of Results by Sampie
Sample Delivery Group: 0409046
Client Samjpie ID: M39-9-04-;oi
Sample Description: ATK-DLV - UPDES Spjl Testirig
Laboratory Sample ID: 0409046-01
Date Sampled: 09/14/04 09:45
CAS Number Test Parametor
TesfMefhod; EPA 314.0
PERCHLORATE-
Result Units
Perchlorate -Ion Chromatography
U mg/kg
MDL
0.1
Dilution
E(3L Factor Analvst Tost Date
0.4 JJH 10/06/04
ClientSampIo iD: M39-9-b4-02
Sample Description: ATK-DLV- UPDES Soil Testing
Laboratory Sample ID: 0409046-02
Date Sampled: 09/14/04 09:50
CAS Numbor Test Parameter
TesfMefhod; EPA 314.0
PERCHLORATE:
Result Urilts MDL
Dilution
EQL Factor Analvst Test Date
Perctilorate - Ion Chramalograpliy
U, mg/kg; 0;1 ;6.4 JJH 10/05/04
CIlentSamplelD: M39-9-04-03
Sample Description: ATK-DLV - UPDES Soil Testing
Laboratory Sample ID: 0409046-03
Date Sampled: 09/14/04 09:55
CAS Numbor Test PariametBr
TestMethod: EPA314J)
PERCHLORATE
Result Urilts
Perchlorale- Ion (JHromatography
U mg/kg
MDL
0.1'
Dilution;
EQL Factor Analyst Test Date
0,4 JJH 10/05/04
Client Sahfipio ID: M3g-9^04r04
Sampio Description: ATK-DLV - UPDES Soil Testing:
Laboratory Sample ID: 0409046-04
Data Sampled: 09/14/04 10:00
CAS Number Test Paramoter Result Units
Tesl Mefhocf; EPA 314.0 Perctilorate - lon Chromaiograptiy
PERCHLORATE lu mg/kg
MDL
0.1
Dilution
EQL Factor Analvst Test Date
0.4 JJH 10/06/04
Client Sample ID: M39-9-04-,05
Sampie Description: ATK-DLV- UPDES Soil Teslirig
Laboriatory Sample ID: 0409046-05
bate Sampled: 09/14/04 10:05
CAS Numbor Test Parameter Result Urilts MDL
Tesf/Mefhod; EPA314.0 Perchiorate r ion Chromaiograptiy
PERCHL6R/\TE-,- IU mg/kg 0.1
Dilution
EQL Factor Analvst Test Date
0.4 JJH 10/06/04
Client Sample ID: W39-9-O4-06
Sample Description: /\T1<-DLV - UPDE^ Soil Testing
Laboratory Sample ID: 0409046-06
bate Samplod: 09/14/04 10:10
CAS Numbor Test Parametor
TestMelhod: EPA 314.0
PERCHLORATE
Result Uriits
Perchlorale - Ion Chromatography
I U mg/kg
MDL
Dilution
EQL Factor Analvst Test Date
0.4 JJH 10/06/04
Page 9 of 22
Listing of Results by Sample
Sample delivery Group:! 0409046
Client Sample ID: iyi39-.9-04-07
Sample Description: ATK-DLV - UPDES Soil Testirig
Laboratory Sampio ID: 0409046-07
DateSampled: 09/14/04 10:13
CAS Number
TestMethod:
Test Parameter:
EPA 314:0
PERCHLORATE
Result i Units
Perehlorate - lon Chromatography
.. ... < EQL nig/kg
MDL
0.1
Dilution
EQL Factor Analvst Testbate
0.4 JJH 10/06/04
CIlentSamplelD: M39-9-04-08
Sample Doscription: ATK-DLV - UPDES Soil Tesling
Laboratory Sample ID: 0409046-08
Date Sampled: 09/14/04 10:15
CAS Nuriiber TestParameter
TesfMefhod; EPA 314:0
PERCHLORATE
Resultj Units MDL
Perdilorale- loh Chromatograpliy
iJ. mg/kg 6-1
Dllutiori
EQL Factoi' Analvst Test Date
.6:4 1 JJH 10/66/04
CIlentSamplelD: M39-9-04.O9
Sample Ddscriptiori: ATK-DLV - UPDES Soil Testirig:
Laboratory Sample ID: 0409046-09
DateSampled: 09/14/04 10:05
CAS Number TestParameter
Tesl Melhod; EPA3i4.0:
PERCHLORATE
Result Units
Perchlorate - |qn Chrorriatpgraphy
U mg/kg
MDL
0.1
Dilution
EQL Factor Analvst Test Date:
0.4 JJH 10/06/04
Clierit Sample/ID: M39-9r04TB
Sampio Descriijtioh: : ATK-Dl-V - UPDES Soil Testing
LaboratorySaniplB ID: 0409046-10
Date Sampled: 09/14/04 09:30
CAS Number Test Parametor Result Units
Test Method: EPA 314.0 Perchiorate - ion Chromatography
PERCHLORATE U ug/L
MDL
-10
Dilution
EQL Factor Analvst Test Date
40 10 JJH 10/20/04
Client Sample ID: M39-9-04EB
Sample Descriplion: ATK-DLV - UPDES Spil Testing
Laboratory Sample ID: 0409046-11
DateSiampled: 09/14/04 09:50
I
CAS Number TestParameter Result Units MDL.
Tesf Method: EPA 314.0 Perchiorate - ion Chromatography
PERCHLORATE |u ug/L 10
pilution
EQL Factor Analvst Test Date
46 10 JJH 16/20/04
CIlentSamplelD: M39^9-04FB
Sample Description; ATK-DLV - UPDES Soil Tesling.
Laboratory Sampio ID: 0409046-12
DateSampled: 09/14/04 09:50
CAS Numbor Test Paramoter
Tesf Mefhod; EPA 314.0
PERCHLORATE
Result Units MDL
Perchlorate - lon Chromaiograptiy
U ug/L 10
Dilution
EQL Factor Analvst Test Date
40 10 JJH 10/20/04
Page 10 of 22
Listing of Results by Sample
Sample Delivery Group:| 0409046
Client-Sample ID: M536-9-04-01
Sample Doscription: ATK-DLV - UPDESiSoil Testing
Laboratory Sample ID; 0409046.13
Date Sampled: 09/14/04 10:54
CAS Number Test Parameter
TeitMeihod: EPASU.O
PERCHLORATE
Result Units
Perchlorale -lon Chromatography
IJ mg/kg
MDL
0.1
Dilution
EQL Factor Analvst Test Date
6:4 JJH 10/06/04
Client Sample ID: M636-9-p4-02
Sample Description: ATK-DLV - UPDES Soil Testing
Laboratory SamiJie ID: 0409046-14
Date Sanipled: 09/14/04 10:43
CAS Number TestParameter
Tesf Mofhod; £P4 314.0
PERCHLORATE
Result Urilts
Perchlorate - Ion Cliromatography
•••'•" i "
U mg/kg
MDL
0:1
Dllutibh
EQL Factor Analyst Test Date
0.4 JJH 10/06/04
Client Sample ID: M636-9-04.03
SampleBescriptlon:: ATK-DLV -UPDESSoil Testirig
Laboratory Sample ID: 0409046-15
bate;Sampldd: 09/14/04 10:45
I
CAS Number Test Parameter Result Units MDL
TestlHefiibd;; EPA3i4,0: Perchlorate - lon Chrbmatograptiy
• • • I' PERCHLORATE U mg/kg 0.1
Dilution
EQL Factbr Analvst TestPate
0.4 JJH 10/06/04
CIlentSamplelD; M53&-9-04-O4
Sample Description: ATK^DLV - OPDES Soil testing
Laboratory Sampie ID: 0409046-16;
Dato Sampled:^ :b9/14/04 10:50
CAS Number Test Parameter
TestMethod: EPA 314.0
PERCHLOR/^TE
Result Units
Pen^hlorate - Ion Chrdnitatography
IU rhg/kg
MDL
0:1
Dilution
EQL Factor Analvst Test Date
0:4 JJH 10/05/04
Client Sample ID: M636-9-b4-05
Sample Description:: ATK-DLV - UPDES Soil Testing
Laboriatbry Sampio ID: 0409046-17
Date Sampled: 09/14/04 10:54
CASNumber
TesfMefhod;
Tesit Parameter
EFA 314.0
PERCHLOI^ATE
Result. Units MDL
Perchlorale - lon Chromaiograptiy
IU. mg/kg 0.1
Dilution
EQL Factor Analvst Test. Dato
0.4 JJH 10/06/04
Client Sample ID: M636-9-04-06
Sampieboscrlptlon: ATK-DLV - UPDESSoil Testing
Laboratory Sample ID: 0409046-18
Date Samplod: 09/14/04 11:00
CAS Number TestParameter
Test Method: EPA 314.0
PERCHLORATE
Result Units
• • I'
Perchlorate- lon Chromatography
U mgJkg
MDL
0:1
Dilution
Factor Analyst Test Date
0.4 JJH 10/06/04
Page 11 of 22
Listing of Results by Sample
Sample Delivery ;Grpup: 0409046
Client SamiJle ID: M636-9r04-07
Sample Description: ATK.DLV - UPDES Soil Testing
Laboratory Sample ID: 0409046-19
DateSampled: 09/14/04 11:02
CAS Numbor Test Rarameter Result Units
TesfMefhod; EPA 314.0 Perchlorate-Ion Chromatography
• "• ••:••••••• •• [
PERCHLORATE U mg/kg'
MDL
0:1
Dilution
EQL Factor Analvst Test Date
0.4 1 JJH 10/06/04
CIlentSamplelD: M636-9-04-08
Sample Description: ATK-DLV -UPIDES Soil Testirig
Laboratory Sample ID: 0409046-20:
DateSampled: 09/14/04 11:04
CAS Nunniber Tost Parameter
TesfMefiiod; EPA3U.6
PERCHLORATE
Result Units
Perciliorate • ion Chromatography
U nig/kg
MDL
0.1
IQL
Dilution
Factor Analvst Test Date
0,4 JJH 10/06/04
Client Sampie lb; iyi636-9-04-b9
Sample Description: ATK-DLV - UPDES Soil Testing
Laboratory Sample ID: 0409046-21
Date iSarnpled: 09/14/64 11:06
CAS Number Test Parameter
TestMethod: EPA'SIIO
PERCHLORATE
Result Urilts
I,
Dilution
EQL Factor Analvst Tost Date
Perchlorate • Ion Chromatography
U mg/kg o:i 6.4: JJH 10/05/04
Client Samjjle |D: M636-9-04-10
Sample Descriptiori: ATK-DLV ^ UPDES Spil Testing
Laljpratory Sample ID: 0409046-22
DateSampled: 09/14/04 11:08
I
CAS Number Test Parameter
TesfMefhod; EPA 314.0
PERCHLORATE
Result Units
Perchlorate-ibh Chromatography
U ;mg/kg
MDL
6:1
Dilution
EQL Factor Analvst Test Date
6.4 JJH 10/05/04
Client Sample ID: M636-g-04-11
Sample Descriptipn: ATI<-DLV - UPDES Soil Tesling
Laboratory SamplelD: 0409046-23
DateSampled: 09/14/0411:10
CAS Number Test Parametor
TestMethod: EPA3i4^0
PERCHLORATE
Result^ Units MDL EQL
Perchlorate-loh Chrornatography
IJ mg/kfl 6;i 0.1
Dilution
Factor Analvst Test Date
JJH 10/06/04
CIlentSamplelD: M636-9-04-12
Satnple Description: .ATK-DLV- Ul=DES Soil Testing
Laboratory Sample ID: 0409046-24
Date Sampled: 09/14/04 11:15
CAS Number Test Pararrieter
Tesf Method; EPA 314.()
PERCHLORATE
Result Units MDL
Perchlorale - Ion Cliromatography
U mg/kg 0;i
Dilution
EQL Factor Analvst Test Date
0.4. JJH 10/06/04
Page 12 Of 22
Lifting of Results by Sample
Sample Delivery Group: 0409046
Client Sample ID: M636-9-p4-13
Sample Description: ATK;^DLV - UPDES: Soii Testing :
Laboratory Sample ID: 0409046-25
DateSampled: 09/14/04 11:17
CASNiJmber Test Parameter Result Units MDL
TesfMethooi; EPA3U.0 Perchlorate-Ion Chromalography
PERCHLORATE | U nig/kg 0.1
Dilution
EQL Factor Analvst Tost Date
0.4 JJH 16/66/04
CIlentSamplelD: M636-9-04-14
Sariiple Description: ATK-DLV -:UPDES Soli Testing
Laboratory Sample ID: 0409046-26
DateSampled:' 09/14/04 11:18
CAS Number Tost Parameter
TesfMclhotf: EPA314.q
PERCHLORATE
Result Units
Perchlorata;- IpnChrorhalogtaphy-
I U nig/kg
MDL
:o.l
Dilution
EQL Factor Analvst Test Date
0.4 JJH 10/06/04
Cllerit Sampio ID:: M636-9-04-i5
Sampio Description: ATK-DLV - UPDES Soil Testirig
Laboratory Sample JD: 0409046-27
DateSampled: 09/14/04 11:22
CAS Number Test Parameter
TestMethod: EPA 314.0
PERCHLORATE
Result Units:
Perehlorate - Ion Chromatography
U mg/kg
MDL
0:1
Dilution
EQL Factor Analvst Test Date
04 JJH 10/06/04
Client Sample ID: M636-g-04-16
Saniple Description: ATK-DLV - UPDES Soil Testing
Labbratoiy Sampio ID: 0409046-28
Dato Sampled: 09/14/04 11:26
CAS Number Test Parariieter
TestMelhod: EPA 314:6
PERCHLORATE
Result Urilts
Perchlorate - Ion Chromatography
U mg/kg
MDL
Dilutlori
EQL Factor Analyst Test Date
0:4 JJH 10/06/04
Client Sample ID: M636:9-04-17
Sample Description: ATK-DLV - UPDES Soil Testing
Laboratory SamplelD: 0409046-29
Date-Sampled: 09/14/0411:28
CAS Number Test Parameter
Test Metiiod: EPA 314.0
PERCHLORATE
Result Units
Perchlorale - Ion Chromalography
I U mg/i(g
MDL
0,1
Dilution
EQL Factor Analyst Test Date
0.4 JJH 10/06/04
CIlentSamplelD: M636-9-04-i8
Sariiple Description: ATK-DLV - UPDES Soli tesling
Laboratory Sampio ID: 0409046-30
Date Sampled: 09/14/04 11:32
CAS Number Test Parameter Result Units MDL
TestMethod: EPA 314.0 Perctilorate - lon Chromatography
PERCHLORATE U mg/kg 0,1
Dilution
EQL Factor Analvst Test Date
10/12/04
Page 13 of 22
Listing of Results by Sample
Sample Delivery Group: 0409046
Client Sample iD: M636-9-04-19
Sampio Doscription; ATK-DLV -UPDES Soil Testing
Laboratory Sample ID; 0409046-31
Date Sampled: 09/14/04 11:35
CAS Nurriber TestiPararnater
TesfMefhod; EPA 314.0
PERfcHLORATE
Result Units
Perchiorate - lon Ctiromatography;
U mg/kg
MDL
0,1
Dilution
EQL Factor Analvst Test Dato
0.4; JJH '10/12/04
ClientSariiplelD: M636-9-04-2P
Sample Description: ATK-DLV - UPDES Soil Tesling
Laboratory Sampio ID: 0409046-32
DateSampled: 09/14/04 11:37
CAS Number Tost Parameter
TesfMefhod; EPA 314:0
PERCHLORATE
Result Units MDL
Perchlorale - lon Chrpmalograptiy
ll mg/kg ;0,1,
Dilution
EQL Factor Analvst Test Dato
0,4 JJH 10/12/04
Client Saniple ID: M636-9-04-21
Sample Description: ATK-DLV - UPDES Soil tesling
Laboratory Sample ID: 0409046-33
DateSampled; 09/14/04 11:42
CAS Number Test Parameter
Test fiJethod: EPA 314.0
PERCHLORATE
Result Units
Perchlorate - ion Chromalography
U mg/kg
MDL
Dilution
EQL : Factbr Analvst Test Date
0.4 JJH 10/12/04
Client Sample ID: M636-9-04-22:
Sampie Description: ATi<-DLV - UPDES Soil testing
Laboratory Sample ID: 0409046-34
Date Sampilod: 09/14/04 14:40
CAS Numbor Test Parametor Result Units MDL
TestMethod: EPA 314.0 Perchlorate-Ion Ctiromatography
PERCHLORATE |u mg/kg 6.1
Dilution
EQL Factor Analvst Test Date
0.4 JJH 10/12/64
Client Sample ip: M636-9-04-23
Sample Description: ATK-DLV - UPDES Soil Tesling
Laboratory Sample ID: 0409046-35
Dato Sampled: 09/14/04 14:40
CAS Number Test Rarameter Result Units
TesiMethod: EPA 314.0 Perchlorate - Ion Chromqlography
PERCHLORATE: |u mg/kg
MDL
0.1
Dilution
EQL Factor Analyst Test Date
0.4 JJH 10/12/04
Client Sample ID: M636-9-04-24:
Sample Descriptiori: ATK-DLV - UPDES Soil Testing
Laboratory Sampio ID: 0409046-36
Date Sannplad: 09/14/04 14:45
CAS Number Test Parameter
TosI Method; EPA 314.0
PERCHLORATE
Result Units
Perctilorate - lon Chromatography
U mg/kg
MDL
Dilution
EQL Factor Analvst Test Date
0.4 JJH 10/12/04
Page 14 of 22
Listing of Results by Sample
Sample Delivery Group: 0409046
Client Sample ID: M636-9T04-25:
Sample Descriptioii: ATK-DLV - UPDES Soil Tesling
Laboratory Sample ID: 0409046-37
Date Sampled: 09/14/04 14:50
CAS tslumber TestParameter Result Urilts MDL
TesfMefhod; EPA3U.0 Perchlorate-ion Chrornatography:
PERCHLORATE U mg/kg 0.1
Dilution
EQL Factoi' Arialvst Test Date
6:4 JJH 10/12/04
CIlentSamplelD: M636-9-04-26
Sample Description: Ati<-DLV- UPDES SdiiTeisting
Laboratory Sample ID: 0409046-38
DateSampled: 09/14/0414:55
CASNumber TestParameter
Tesf/lfofhod; EPA314.0
PERCHLORATE
Result Units
Perchlorate- lon Chroniatography
U mg/kg
MDL
0.1.
Dilution
EQL Factor Analvst Test Date
0.4 JJH 10/12/04
Client SamiJIo ID: M636-9-04r27-
Sample Deiscription: AtK-DLV - UPDES Sbil Testirig
Laboratory Sample ID; 0409046-39
Date Sampled: 09/14/04:15:00
CAS Number
Test Method:
Tost Parameter
EPA 314.0
PEF?CHLORATE
Result Units
:Perchlorate - lon Chrornatography
U mg/kg
MDL
0.1
Dilution
EQL Factor Analvst Tost Date
:0:4 JJH 10/12/04
CIlentSamplelD: :M636-9-04-28
SampleDescrlptibri: Ajk^pLV - UPDES Soil Tesling
Laboratory Sampio ID: 0409046-40
Date Samplod: 09/14/04 15:03
CAS Number TestParameter Result Units
TestMethod: EPA3Ui) Perchiprate - ion cfirorriatbgraphy
;PERCHL0RATE U mg/kg;
MDL
0.1
IQL:
o:4
Dilution
Factor Analyst Test Date,
JJH 10/12/04
Client SamplelD: M636-9-04-29,
Sample bescriptibn: ATK-DLV - UPDES Soil Tesling
Laboratory Sample ID: 0409046-41
Date Sampled: 09/14/04 15:05
CAS Numbor Test Parameter Result Units MDL E(3L
TestMethod: EPA 314.0. Perchlorate-lon Chromatography
PERCHLORATE, U mg/kg 0,1 0:4
Dllutlan
Factor Analvst Test Date
JJH, 10/12/04
Cliont Sample IDi M636-9-04-30
Sample Description; ATK.DLV,- UPDES Soil Tesling
i Laboratory Sample ID: 0409046-42
DateSiampled: 09/14/04 15:08
CAS Numbor
Tesf Method:
Test Paramoter
EPA:314:0
PERCHLORATE
Result Units MDL
Perchlorate - ion Chrornatography
U mg/kg 0:i
Dilution
EQL Factor Analvst Test Date
0.4 1 JJH 10/12/04
Page 15 of 22
Listing of Results' by Sample
Sample Delivery Group: 0409046
Client Sample ID: M636-9-04-31
Sample.Description: ATK-DLV - UPDES SpilTeslIng
Laboratory Sample ID: 0409046-43
Date Sampled: 09/14/04 15:13
CAS Number test Parameter
TesiMefhod; EPA3U.0
PERi^HLORATE
Result I Units
Perchlorate-lon Chromatography
U mg/kg
MDL
0.1
Dilution
EQL :Factor Analvst Test Date
6,4 ; JJH 10/12/04
ClientSampie ID: (iA636-9-04-32
SampleDescrlption: ATK-DLV-UPDESSoilTesling
Laboratory Sample ID: 0409046-44
Date Samplod; 69/14/04;l5:l9
CAS Number Test Parametor
TestMeOiqd: EPA 314.6
PERCHLORATE
Result I Units
••••'!•• Perchlorale .-Ion Chromatography
U mg/kg
MDL
Dilution
EQL Factor Analvst Test Date
JJH 10/12/04
CIlentSamplelD: M636-g-04-33
Sample Descriptiori: ATK-DLV - UF'pES Soil Testing
Laboratory Sample ID: 0409046-45
DateSampled: 09/14/04 15:21
CAS Number Test Parameter
Tesf Afefhdd; EPA314.0
PERCHLORATE'
Result- Units
Pei;chlorale - Ion Chromatography
U mg/kg
MDL
0.1
Dilution
EQL: Factor Analyst Test Date
0.4 JJH 10/12/04
Client Sampie ID: M636-9-04-34
Sample bescription: ATK-DLV - UPDES Soil Testing
Laboratory Sample ID:; 0409046-46
DateSampled: 09/14/04 15:25
CAS Number Test Parameter
Tesf Mofhod;; EPA 314.0
PERCHLORATE
Result- Units
Perchiorate i lon Chromatography
U mg/kg
MDL
6;i
Dilutlori
EQL Factor Arialvst Test Date
0,4 JJH; 16/12/04
CIlentSamplelD: M636-9rb4-35
Sample pescription: ATK-DLV - UPDESSoil Testing
Laboratory Sample ID: 0409046-47
DateSampled: 09/14/04 15:29
CAS Ntjrriber Tost Parameter Result Units
Test Method: EPA 314.0 Perchlorate - Ion Chromatography
"I •'
PERCHLORATE U mg/kg
MDL
6:1
Dilution
EQL Factor Analvst Test Date
0,4 1 JJH 10/12/04
Client Sample ID: M636-9-04-36
Sample Descjriptipn: ATK-DLV - UpDES Soil Testing I
Labpraitory Sampio ID; 0409046-48
DateSampled: 09/14/04 15:33
CAS Number
TesfMefhod;
Test Parameter
EPA 314.0
PERCHLORATE
Result Units
Perchlorate - ion Chromatography
U mg/kg
MDL
0,1
Dilution
EQL Facitor Analvst Test Date
0,4 JJH 10/12/04
Page 16 of 22
Listing of Resultsj by Sample
;Sample Delivery Group: 0409046
ClientSampie ID: M636:9-p4-37
SamplePesci-iptldn: ATK-DLV-UPpEiS'Soil tesling
Laboratory Sample ID: 0409046-49
bate Sampled; : 09/14/04 15:35
CAS Number Test Parameter
TesfMefhod; EPA 314.0
PERCHLORATE
Result Units
perctilorate - Ion Chromatography
Ui mg/kg
MDL
0,1
Dilution
EQL Factor Analvst Tost Date
0,4 1 JJH 10/12/04
Client Sample ID: M636-9rb4-38
Sample Description: ATI<-DLV - UPDES;Soil Tiaslipg
Laboratory Sample ID; 0409046-50
DateSampled: 09/14/04 15:38
CAS Number TestParameter
TesfMeihocf; EPA 314.0:
PERCHLORATE
Result Units MDL
Perchlorale-.Ion Chromatography
U mg/Kg 0,1
Dilution
EQL Factor Analvst: Test Date
JJH 10/13/04
CllontSample ID; M636-9-04-:39
Sample Dascriptlon: Atk-DLV'- UPDES Sbil Tesiing
Laboratory Sample ID: 0409046-51
Date Sampled; 09/14/04 15:41
CASNumber Test Pariameter,
TesfMefhod;; EPA 314,0:
PERCHLORATE-
Resulti Units MDL
• !'•
Dilution
Factor Analyst Test Date
Perchlorale-lohChrorhatography;
U riig/kg 0,1 0,4 JJH 10/13/04
Client Sample ID; M636-9-04-40
Sample Description:: ATK-DLV - UPDES SpirTestlng
Laboratory Sample ID: 0409046-52
Date Sampled: 09/14/04 15:45
CAS Number Test Parameter
TesfMefhod; EPA 314.0
PERCHLORATE
Result Units
Perciliorate - Ion Chromatography
•• ••!
U mg/kg
MDL
0.1
Dilution
EQL, Factor Analvst Test Date
0,4 -JJH 10/13/04
Cllont Sample ID: M636-9-04-41
Sariipie Description: ATK-DLV - UPDES Soil Testing
Labdratiory Sample ID: 0409046-53
Date Sampled: 09/14/04 15:48
CAS Number Test Parameter
TestMethod: EPA 314.0
PERCHLORATE
Result Units
Perchlorale - lon Chromatography
[ ,
jU mg/kg
MDL
0.1
Dilution
EQL Factor Analvst Test Date
0.4 JJH 10/13/04
ClientSampie ID: M636-9-04r42
SampleDescrlption: ATK-DLV- UPDES Soil Testing
Laboratory Sample ID: 0409046-54
DateSampled: 09/14/0410:45
CAS Numbor Tost Parameter
TesfMefhod; EPA 314.0
PERCHLORATE
^ Result Units
I • Perchlorate - Ipn Chromatography
' U mg/kg
MDL
0.1
Dilution
EQL Factor Analvst Test Date
0,4 JJH 10/13/04
Page 17 of 22
Listing pf Results by Sample
Sample Delivery Group: 0409046
CIlentSamplelD: M636-9-04-43
Sampio Description: ATK-DLV - UPDES;Spi| Testing
Laboratory Sample ID: 0409046-55
DateSampled: 09/14/0411:17
CAS Number Test Parameter
rcsfMef/iocf; EPA 314.0
PEfSCHLORATE
Result Units
Perchlorate-ion Chromatography
-U nig/kg
MDL
0„1:
Dilution
EQL Factor Analyst Test Date
0.4^ JJH 10/13/04
Client Sample lb: M636r9-b4-44;
Sample Description: ATK-DLV - UPDESSoil testing
Laboratory Sample ID: 0409046-56
•ate Sampled: 09/14/04 14:40
CAS Nuriiber TestParameter
Toif Mefhod; iPA3U.6
PERCHLORATE
Result Units
Perchlorate -Ion Ctiromatography
U mg/kg
MDL
0.1
Dllutioh
EQL Factor Analyst Test Date
6,4 JJH 10/13/04
ClientSampie ID: M636-9-04-45
Sample Descriptiori: ATK-DLV - UPDES Soli Testing
Laboratory Sample ID: 0409046-57
Date Samplisd: 09/14/04 15:21
CAS Numbor TestParameter Result Units MDL
Test Mefhod; EPA 314:0 Perchlorate - lon Chromaiograptiy
PERGHLPRATE til mg/kg p.i:
Dilution
EQL Factor Analvst Test Dato
0.4 JJH •10/13/04
Client Samplb ID: M636-904TB1
Sample Description: AT1<-DLV - UPDES Soil Testing
Laboratory Sampio ib: 0409046-58
Date Sampled: 09/14/04 14:30
CAS Number Test Parameter
TesfMefhod: EPA 314.0
PERCHLORATE
Result Units
Perchlorate - Ion Chromatography
U ug/L
MDt EQL
Dilution
Factor Analvst Test Dato
40 10 JJH 10/20/04
Client Sample ID: M636-904EBi
Sample Description: ATK-DLV - UPDES Soil Teslirig
Laboratory Sample ID; 0409046-59
DatoSamplod: 09/14/04 10:41
CASNuniber Test Parameter Result Units MDL
Tesf Mefhdcf; EPA 314.0 Reriiihiorate - iori Chromatography
PERCHLORATE' ij ug/L 10
Dilution
EQL Factor Analvst Test Date
40 '10 JJH 10/20/04
Client Sample ID: M636-904FB1
SampleDescrlption: ATK-OLV - UPDES Soil tesling
Laboratory SamplelD: 0409046.60
DateSampled: 09/14/0410:41
CAS Nurriber Tost Parameter
TesfMefhod; EPA 314^0
PERCHLORATE
Result Units MDL
Perchlorale - lon Chromotography
U ug/L 10
Dilution
EQL Factor Analvst Test Date
10 JJH 10/20/04
Page 18 of 22
Listing of Results by Sample
Sample Delivery Group: 0409046
Client Sample ID; M636-904TB2
Sampio Description: ATK-DLV - UPDES Soil Testing
Laboratory Sample ID: 0409046-61
Date Sampled; • 09/14/04 14:30
CAS Number Test Parariieter Result , Units
Tesl Melhod: EPA 314,0 Perchlorate - lon Chromaiograptiy
PERCHLORATE Ul ug/L
MDL
Dilution
EQL Factor Analvst TestPate
10 46 10 JJH 10/20/04
Client SamplelD: M636-904EB2
Sample Description: AtK-DLV T UPDES Soil testing
Laboratory Sample ID: 0409046-62
DateSampled: 09/14/04:11:12
CAS Nuriiber Test Parametor
fcslMetiiad: EPA 314.0
PERCHLORATE
Result Units MDL
Perchlorate - Ion Chromatography
• U ug/L 10
Dilution
EQL i^actor Analvst Test Date
40 10 JJH 10/20/04
Client Sampio iD: M636-904FB2
Sample Descriptiori: ATK-DLV -UPDES Soil Testing
Laboratory Sample ID: 0409046-63
DateSampled: 09/14/04 11:12
CAS Number Test Parameter Rosult Units MDL
TestMethod: EPA 314.0 Perchlorale - ion Chrornatography
PERCHLORATE: U ug/L 10
Dilution
EQL Factor Analvst Tost Dato
40 •10 JJH 10/20/04
Client Sample ID: M636-9b4TB3
Sample Description: ATK-DLV - UPDES Soil Tesiing
Laboratory Sample ID: 0409046-64
DateSampled: 09/14/04 14:30
CAS Number
TesiMefhod;
Test Parameter
EPA 314.6
PERCHLORATE
Result Units MDL
Perchlorate - Ion Ctirbmalography
U ug/L
Dilution
EQL Factor Analyst Test Date
10 40 10 JJH 10/20/04
Client Sample ID; M636-904EB3
Sample Description: ATK-DLV - UPDES Soil tesling
Laboratory Sample ID: 0409046-65
DateSampled: 09/14/04 11:48
CAS Number Test Parameter Result Units
Tesl fliiefhod; EPA. 314.0 Perchlorate - Ion Chromatography
PERCHLORATE U; ug/L
MDL
lp:
Dilution
EQL Factor Arialvst Test Date
40 10 JJH 10/20/04
Client Sample ID: M636-904FB3::
Sample.Description: ATK-DLV-UPDES Soil Testing
Laboratory Sampio ID; 0409046'66
DateSampled: 09/14/04 11:48
CAS Number Test Parameter
TestMelhod: EPA 314.0
PERCHLORATE
Result Units MDL
Perchlorate - Ion Ctiromatography
U ug/L 10
Dilution
EQL Factor Analvst Test Date
40 10 JJH 10/20/04
Page 19 Of 22
Listing of Results by Sample
Sarnple Delivery Group: 0409046
CIlentSamplelD: M636-9b4TB4
Sample Doscription: ATK-DLV - UPDES Soil Tesling
Laboratory Sample ID: 0409046-67
DateSampled: 09/14/04 14:30
CAS Number Test Parameter
TesfMefhod; EPA 314.0
PERCHLORATE
Result' Units
Perchlorate - Ion Chromatography
•U, ug/L
MDL
10
Dilution
EQL Factor Analvst Test D^tB:
40 10 JJH' 10/20/04
CIlentSamplelD: M636-904EB4;
Sariiple Description: ATK-DLV - UPDES Soil Testing
Laboratory Sample ID: 0409046-68
Date Sampled: 09/14/04 13:15
CAS Number Tost Parameter
TestMelhod: EPA 314.0
PERCHLORATE
Result Urilts MDL
• • • I Perctilorate - Ion Chromatography
U ug/L 10
Dilutlori '
EQL Factor Analvst Test Date
40 10 JJH '10/20/04
Client Sample;|p: M636-904FB4
Sample Description: ATK-DLV - UPDESSoil Testing
Laboratory Sample ID: 0409046-69
Diite Samplod: 09/14/04 13:15
CAS NLimber' Test Pararrieter
TesfMefhocf; EPA314.0
PERCHLORATE
Result Units
Perchlorate T Ion Chfomatpgraphy
U ug/L
MDL
Dilution
EQL Factor Analvst Test Dato
40 -10 JJH 10/20/04
Client Sample ID: M636-9-04-46
Sample:Descrii3tioii: ATK-DLV -;U(=^pES;'Soil Testing;
Laboratory Sample ID: 0409045-70
Date Sambied: 09/14/0410:50
CAS Number
Tesl Mofhod;
Tesf Method:
Test Method:
7440^3-9
7440-22-4
Test Parameter
EPA 314.0
PERCHLORATE
5^-846, 3050B
30,508 ACID DIGESTIOf^
SM/-846, eOlOBYSofjds)
CADMIUM
SILVER
Result
Perchlorate - Ion Chromalography
:0
ICP/GFAA Metals Digestion
Metals Analysis by ICP - 6016
1:93
160
Units
mg/kg
ug/g
ug/g
MDL
0.1
0,18
0,22
EQL
0,4
0,594
0.726
Dilution
EQL Factor Analvst Test Date
JJH
MTB
10/13/04
09/28/04
1 MTB 10/13/01
i MTB 10/13/04
Client Sample ID: M636-9-04-47
Sample Description: ATK-DLV - UPDES Soil Testirig
Laboratory Sampio ID: 0409046-71
bate Sampled; 09/14/04 11:26
CAS Number
TesfMefhod;
Tasf/Hethod;
Tesf Mefhod;
7440-43-9
7446-22-4
test Parameter
EPA 314.0
PERCHLORATE
Siy-846, 3050B
3050B ACID DIGESTION
SW-S46, 60*08 fSoi/ds)
CADMIUM
SILVER
Result Units
Perchlorate - lon Chromatography
U mg/kg
ICP/GFAA Metals Digesiion
Motals Anaiysis by ICP - 6010
0,7 J ug/g
488 ug/q
MbL
0,1
Dilution
EQL Factbr Analvst Test Date
JJH
MTB
10/13/04
09/28/04
0,18
0:22
0,594
0.726
1
•1
MTB
MTB
10/13/04
10/13/04
Page 20 of 22
Listihg of Results by Sample
Sarriple Delivery Grciup: 0409046
CIlentSamplelD; M636-9-04-48
SamploDescrlptlon: ATK-DLV -UPDES Spii Testing
Laboratory Sample ID: 0409046-72
DateSampled: 09/14/04 15:08
CAS Number
TesfMefhod;
TesfMefhod;
TesfMefhod:
•7440-43-?:
7440-22-4
Test Paramoter
EPA 314.6
PERCHLORATE
SlV-^846,3050B
• 3050B ACio biGEStiON
SW-846. 60m (Solids):
CADMIUM
SILVER
Result Units
:Perchlprate - Ion Chromalography
U mg/kg
:iCP/GFAA,Mi5tals Digestion
Metals Analysis by ICP r;6010
5;1B ug/g
455 ug/g
MDL
0,1
Dilution
-EQL Factbr Analyst Test Date
0:4 JJH 10/13/04
MTB 09/28/04
0;18
0,22
0.594
0.726
1
1
MTB
MTB
10/13/04
10/13/04
CIlentSamplelD: M39-9-04;l0
Sample Description: ATk-DLV•: UPDES Soil Testing
Laboratory Sample ID: 0409046-73
DateSampled: 09/14/04 09:50
CAS Number
TosfMpfhod;:
TestMethod:
Test Method:
7440-43-9
7440-22^
Test ParariiBtej- ReJBUlt: Units
EPA 314.0 Perchiorate - Ion Chrornatography
;PERCHLORATE
SW-846. 30508 Icp/GFAAMelals Digestioh
3050a ACID DiCJEStlON
SW-846, BOIOB (Sdlids) Metals Analysis by ICP - 6010
CADMIUM
SILVER
U mg/kg
MDL
0:1
Dilution
EQL Factor Arialvst Test Date
• 0.4 JJH
MTB
10/13/04
09/28/04
3.64
384
ug/g
ug/g
0.18
0.22
0.594
0,726
1
1
MTB
MTB
10/13/04
10/13/04
Page 21 of 22
Data Reporting Qualifiers
U indicates tliat the analyte was not detected, of the analyte was detected but
was below the MDL.:
B This flag is used when an analyte is fqtjnd in the blank as well as the sample.
J Indicates an estimated vajue. This flag is usisd either wheri estimating a
concentratipn;fortentatively identified compounds or vyhen the data indicated
the presertce of a compound that meets the identification criteria but the
resultis less than the EQL (e,g. 3 J with ah EQL of 10).
MDL Metiiod Detection Liniit: The m.inimuiti concentration of a substance that can be
confidently-rrieasuredand reported. |The laboratory has, demonstrated that the
MDL can be achieved iri a labbratbry, reagent blank, but does hot guarantee it
can be achieved in all sample, matrices.
EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL, For
many analytes the:EQL is selected asthe value ofthe; lowest standard in the
calibration curve;
Diluiion Dilution Factor The prepared sample was diluted by this facitor because the
Factor sample was toqconcentrated or due to other interferences in the sample matrix.
Any dilutionJfactor causes a corresponding increase in.the MDL and EQL.
Page 22 of 22
ATK THIOKOL
PROPULSION
15-Oct-04
Quality Control Aliquot
Aliquot Reference Ailquot Date Tested
Quality Control Report
Department: Metals Analysis
WSd409-099
6010BMetals_S
Test Parameter Measured Value
Recovery RPD
(•/.Recov) Limits (RPD) Limits
Aliquots on Worksheet
0409020-33A1
0409620-34A1
0409020-35A1
0409020-36A1
04e9e26-37A1
0409020-38A1
6409620-3gA1
0409620-40A1
0409020-41A1
0409020-42A1
ICP QCS19 Metals
MT0409-106
ICP QCS07 Metals
MT64e9-ie7
(MSD) Matrix Spike Duplicate
MT0409-114 MT0409-113
(MS) Matrix Spike
MT0409-113 0409020-33A1
9tt8rt)4 13:31
9fl!8/0413:40
9/28/0413:43
9/2870413:47
g/2BA)4 13:50
9/28/04 13:53
9/28/0413:57
9«8rt)414:00
9/28/0414:03
9/28/0414:07
9/28/0413:08
9/28/04 13:09
9«8i/0413:37
9/28/0413:34
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CAOMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
. SILVER
(LRB) Laboratory Reagent Blank
MTO469-110 9/28/0413:19 CADMIUM
SILVER
(LFBD) Laboratory Fortified Blank Duplicate
MT0409-112 MT0409-111 9/28/04 13:25 CADMIUM
SILVER
(LFB) Laboratory Fortified Blank
MT0409-111 9/28/0413:22 CADMIUM
SiLVER
(ICV) Initial Calibration Verification
MT6469-108 9/28/0413:13 CADMIUM
SILVER
(CCV) Continuing Calibration Verification
MT0409-115 9/28/0414:10 CADMIUM
SILVER
(CALB) Calibration Blank
MT0409-109 9/28/0413:16 CADMIUM
SILVER
MT0409-116 9/28/0414:13 CADMIUM
2.1 ug/g
119 ug/g
1.74 ug/g
117 ug/g
1.48 ug/g
87.7 ug/g
6.33 ug/g
479 ug/g
5.81 ug/g
338 ug/g
4.55 ug/g
769 ug/g
5.36 ug/g
884 ug/g
5.31 ug/g
853 ug/g
4.41 ug/g
473 ug/g
5.83 ug/g
890 ug/g
980 ug/g
497 ug/g
38 ug/g
122 ug/g
37.9 ug/g
121 ug/g
6.3 J ug/g
U ug/g
382 ug/g
140 ug/g
374 ug/g
137 ug/g
1950 ug/g
246 ug/g
1940 ug/g
245 ug/g
U ug/g
U ug/g
U ug/g
98.0
99.3
90.6
16.9 •
95-105
95-105
70-130
70-130
.311
.832
0-25
0-25
Spike value too lov/ for sample matrix.
90
10.1 *
70 • 130
70-130
Spike value too lev/ for sample matrix.
95.4
93.1
93.6
91.6
97.4
98.4
96.8
97.9
<6.18
<0.22
70-130
76-130
70-130
70-136
96-110
90-110
90-110
90-110
<0.18
<6.22
<0.18
MDL
MDL
1.9
1.S8
MDL
MDL
MDL
0-25
6-25
Page 1 ot 2
DDnDMi'^ll^r^M Quality Control Report
PROPULSION Department: MelalsAnalysis
15-Oct-04 WS6409-099
Quality Control Aliquot 6010B MetalS_S Recovery RPD
Ailquot Reference Aliquot Date Tested Test Parameter Measured Value (%Recov) umlts (RPD) Limits
(CALB) Calibration Blank
MT0409-116 9/28/0414:13 SILVER 0.41Jug/g <0.22 MDL
Analyst Review:
Peer Review:
Page 2 of 2
DDnDm^!l^r?M Quality Control Report
PROPULSION Department: Metals Analysis
15-Oct-04 WS0409-100
Quality Control Aliquot 601 OB MetalS_S Recovery RPD
Aliquot Reference Aliquot Date Tested TestParameter Measured Value (%Recov) Limits (RPD) Limits
Aliquots on Worksheet
0409020-43A1 9/28/0414:47 CADMIUM
SILVER
0409026-44A1 9/28/0414:57 CADMIUM
SILVER
0409026-45A1 9/28/0415:00 CADMIUM
SILVER
0409020-46A1 9/28/0415:03 CADMIUM
SILVER
0409620-47A1 9/28/0415:07 CADMIUM
SILVER
0409020-48A1 9/28/0415:10 CADMIUM
SILVER
0409020-49A1 9/28/0415:13 CADMIUM
SILVER
6409020-50A1 9/28/0415:17 CADMIUM
SILVER
6409620-51A1 9/28/0415:19 CADMIUM
SILVER
0409020-52A1 9/28/0415:22 CADMIUM
SILVER
ICP QCS19 Metals
MT0409-117 9/28/0414:22 CADMIUM 969 ug/g 96.9 95-105
ICP QCS07 Metals
MT0409-11B 9/28/0414:25 SILVER 491 ug/g 98.2 95-105
(MSD) Matrix Spike Duplicate
MT0409-125 MT0409-124 CADMIUM 42.8 ug/g 183* 70-130 3.49 0-25
Higti concentrations of Cd and Ag. Spike values low compared to the Cd & Ag concentration in ttie sampie.
SILVER 1300 ug/g 996* 70-130 10.4 0-25
Higti concentrations of Cd and Ag. Spike values low compared to the Cd & Ag concentration in the sample.
(MS) Matrix Spike
MT0409-124 0409020-43A1 9/28/0414:53 CADMIUM 41.3 ug/g 89.1 70-136
SILVER 1440 ug/g 454* 70-130
High concentrations of Cd and Ag. Spike values low compared to the Cd & Ag concentration in the sample.
(LRB) Laboratory Reagent Blank
MT0409-121 9/28/0414:35 CADMIUM 0.2 J ug/g
SILVER U ug/g
(LFBD) Laboratory Fortified Blank Duplicate
MT0409-123 MT0409-122 9/28/0414:41 CADMIUM 369 ug/g
SILVER 136 ug/g
(LFB) Laboratory Fortified Blank
MT0409-122 9/28/0414:38 CADMIUM 373 ug/g
SILVER 137 ug/g
(ICV) Initial Calibration Verification
MT0409-119 9/28/0414:29 CADMIUM 1940 ug/g
SILVER 245 ug/g
(CCV) Continuing Calibration Verification
MT0409-126 9/28/0415:25 CADMIUM 1930 ug/g
SILVER 244 ug/g
(CALB) Calibration Blank
MT0409-120 9/28/0414:31 CADMIUM U ug/g
SILVER U ug/g
MT0409-127 9/28/0415:28 CADMIUM U ug/g <0.18 MDL
6.09
1380
10.9
704
5.9
696
5.28
284
I.U
172
1.57
218
2.21
93.8
I.J
15.3
0.4 J
20.7
0.6 J
37
969
491
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
92.2
90.9
93.2
91.2
96.7
97.9
96.7
97.6
<0.18
<0.22
70-130
70-130
70-130
70-136
90-110
90-110
90-110
90-116
<6.18
<:6.22
MOL
MDL
1.11
.364
MDL
MDL
0-25
0-25
Page 1 of 2
DDH Jnl^^nllr Quality Control Report
PROPULSION Department: Metals Analysis
15-Oct-04 WS0409-100
Quality Control Aliquot 6010B MetalS_S Recovery RPD
Ailquot Reference Ailquot Date Tested TestParameter Measured Value (%Recov) Limits (RPD) Limits
(CALB) Calibration Blank
MT0409-127 9/28/0415:28 SILVER U ug/g <0.22 MDL
Analyst Review: ^^' P- C>t^ ^1-^ /^ " '^'- ^^
Peer Review:
Page 2 of 2
ATK THIOKOL
PROPULSION
06-Oct-04
Quality Control Aliquot
Aliquot Reference Aliquot Date Tested
Quality Control Report
Department: Metals Analysis
WS0410-009
601 OBI Metals.
Test Parameter
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
_w
Measured Value
U
U
U
U
U
u
U
u
u
u
u u u u u u
u
u
u
u
u
u
u
u u
u
u u
u u
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug'L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Recovery RPD
(•/.Recov) Limits (RPD) Limits
Aliquots on Worksheet
0409020-10A1
0409020-1 IAI
0409020-12A1
0409020-58A1
0409026-59A1
0409020-60A1
0409020-61 Al
0409626-62A1
0409020-63A1
0409020-64A1
0409020-65A1
6409020-S6A1
0409020-67A1
0409020-68A1
0409020-69A1
ICP QCS19 Metals
MT0410-1
ICP QCS07 Metals
MT0410-2
(MSD) Matrix Spike Duplicate
MT0410-9 MT0410-8
MT0410-13 MT0410-12
(MS) Matrix Spike
MT0410-8 040902O-10A1
MT0410-12 0409020-65A1
(LRB) Laboratory Reagent Blank
MT0410-5
(LFBD) Laboratory Fortified Blank Duplicate
MT0410-7 MT0410-6
(LFB) Laboratory Fortified Blank
MT0410-6
(ICV) Initial Calibration Verification
MT0410-3
(CCV) Continuing Calibration Verification
MT0410-10
MT0410-14
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
1000 ug/L
489 ug/L
100
97.8
204 ug/L
73.5 ug/L
202 ug/L
73.1 ugrt.
202 ug/L
73.1 ug/L
203 ug/L
73 ug/L
U ug/L
U ugfl.
201 ug/L
72.7 ugA.
202 ug/L
72.6 ugfl.
1980 ug/L
246 ug/L
1920 ugfl.
241 ug/L
1920 ugfl.
241 ug/L
102
97.8
101
97.2
101
97.1
101
97.1
101
97.0
101
96.9
99.0
98.5
95.9
96.5
95.9
96.5
.591
.628
.593
.6958
<3.7 MDL
<2.2 MDL
.248
.138
Page 1 ot 2
ATK THIOKOL
PROPULSION
06-Oct-04
Quality Control Aliquot
Aliquot Reference Aliquot Date Tested
Quality Controi Report
Department: Metals Analysis
WS0410-009
6010B Metals_W
Test Parameter
V
Measured Value
U ugfl.
U ugfl.
U ugfl.
U ugfl.
U ugfl.
U ugfl.
Recovery
(•/oRecov) Limits
<3.7
<2.2
<3.7
<2.2
<3.7
<2.2
RPD
(RPD)
MDL
MDL
MDL
MDL
MDL
MDL
Limits
(CALB) Calibration Blank
MT0410-4
MT0410-11
MT0410-15
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
Analyst Review:
Peer Review:
^>r;.^ .iS^-^-^:^ /o-C~t)^
S^tKtg? /^- 7-0<f
Page 2 of 2
ATK THIOKOL
PROPULSION
15-Oct-04
Quality Control Aliquot
Aliquot Reference Ailquot Date Tested
Quality Control Report
Department: Metals Analysis
WSd409-063
601 OB Metals S
Test Parameter Measured Value
3.21
189
11.1
232
0.9 J
131
0.4 J
47.1
0.4 J
34.4
0.4 J
109
U
49.4
U
32.3
1.79
140
1010
497
32.7
60.8
32
59.2
U
U
19
7.1
19.1
7.09
19S0
247
1860
236
U
U
U
U
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Recovery RPD
(•/.Recov) Limits (RPD) Limits
Aliquots on Worksheet
0409020-02A1 10/12/0414:47
04090204)3A1 10/12/0414:50
0469020-04A1 10/12/6414:53
0409020-05A1 10/12/04 14:59
0409020-06A1 10/12/0415:09
0409020-07 Al 10/12/0415:12
0409020-08A1 10/12/0415:15
0409020-09A1 1 Q/12/0415:18
0409020-01A1 10/12AM 14:45
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CAOMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
ICP QCS19 Metals
MT0409-62
ICP QCS07 Metats
MT0409-63
(MSD) Matrix Spike Duplicate
MT0409-70 MT0409-69
10/12/0414:23 CADMIUM
10/12/0414:25 SILVER
10/12/0415:04 CADMIUM
SILVER
(MS) Matrix Spike
MT0409-69 0409020-05A1 10/12/0415:01
(LRB) Laboratory Reagent Blank
MT0409-66 10/12/0414:37
(LFBD) Laboratory Fortified Blank Duplicate
MT0409-68 MT0409-67 10/12/04 14:42
(LFB) Laboratory Fortified Blank
MT0409-67 10/12/0414:40
(ICV) Initial Calibration Verification
MT0409-64 10/12/04 14:29
(CCV) Continuing Calibration Verification
MT0409-71 10/12/0415:29
(CALB) Calibration Blank
MT0409-65 10/12/0414:34
MT0409-72 10/12/0415:26
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CAOMIUM
SILVER
101
99.4
81.2
92.2
81.5
83.1
95.1
94.6
95.7
94.5
97.9
98.8
93.2
94.4
95 -105
95-105
70-130
70-130
70-130
70-130
<0.18
<0.22
70-130
70 -130
70-130
76-130
90-110
90-110
90-110
90-110
<0.18
<0.22
<0.1B
<0.22
2.19
2.79
MDL
MDL
.62
.17
MDL
MDL
MDL
MDL
0-
0-
0-
0-
-25
-25
•25
•25
Analyst Review: ^->^.^, s/S^-^v^^-^^ /g^-/jr-oy
Peer Review: /^ -/s--^Y
Page 1 of 1
ATK THIOKOL
PROPULSION
15-Oct-04
Quality Control Aliquot
Aliquot Reference Ailquot
Aliquots on Worksheet
0409020-20A1
0409020-21 Al
0409020-22A1
0409020-23A1
0409020-24A1
04D9020-25A1
0409020-26A1
0409020-27A1
0409020-28A1
0409020-29A1
ICP QCS19 Metals
MT0409-84
ICP QCS07 Metals
MT0409-85
Date Tested
9/28/0411:56
9«a/04 12:04
9/28/04 12:07
9/28/0412:11
9/28/04 12:14
9/28/04 12:16
9/28/04 12:19
9/28/0412:22
9/28/04 12:25
9/28/04 12:28
9«8/04 11:27
9/28/0411:34
Quality Control Report
Department: Metals Analysis
WS0409-081
601 OB Metals.
Test Parameter
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
S
Measured Value
2.02
71.1
3.58
148
0.6 J
655
5.03
45.1
4.29
29.9
1.32
18.4
0.8 J
46.7
1.23
901
0.9 J
1.46
1.68
135
985
506
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Recovery
(•/oRecov)
98.5
101
RPD
Umits (RPD) Limits
95-105
95-105
(MSD) Matrix Spike Duplicate
MT0409-92 MT0409-91
(MS) Matrix Spike
MT0409-91 0409020-20A1
9/26/0412:01 CADMIUM
SILVER
9/28/0411:58 CADMIUM
SILVER
(LRB) Laboratory Reagent Blank
MT0409-a8 9/28/0411:43 CADMIUM
SILVER
(LFBD) Laboratory Fortified Blank Duplicate
MT0409-90 MT6409-89 9/28/04 11:50 CADMIUM
SILVER
(LFB) Laboratory Fortified Blank
MT0409-89 9/28/0411:47 CADMIUM
SILVER
(ICV) Initial Calibration Verification
MT0409-86 9/28/0411:37 CADMIUM
SILVER
(CCV) Continuing Calibration Verification
MT0409-93 9/28/0412:31 CADMIUM
SILVER
(CALB) Calibration Blank
MT0409-87 9/28/0411:40 CADMIUM
SILVER
MT0409-94 9/28/0412:34 CADMIUM
40.2 ug/g 191 *
Non-homogeneous soil
129 ug/g 767 *
Non-homogeneous soil
39.9 ug/g 190 *
Non-homogeneous soii
139 ug/g 903 *
Non-homogeneous soil
100
98.6
70-130 .679 0-25
sample. Data accepted.
70-130 7.61 0-25
sample. Data accepted.
70-130
sample. Data accepted.
70-130
sample. Data accepted.
0.3 J
0.25 J
401
148
405
148
1980
250
1900
241
U
0.28 J
0.2 J
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
MDL
MDL
.942
.355
101
99.0
98.8
100
95.2
96.4
<0.1B
<6.22
70-130
70-130
70-130
70-130
90-110
90-110
90-110
90-110
<0.18 MDL
<0.22 MDL
<0.18 MDL
0-25
0-25
Page 1 of 2
DDnDuI^li^r^M Quality Control Report
PROPULSION Department: Metals Analysis
15-Oct-04 WS0409-081
Quality Control Aliquot 6010^ MetalS_S Recovery RPD
Aliquot Reference Aliquot Date Tested Test Parameter Measured Value (%Recov) Limits (RPD) Limits
(CALB) Calibration Blank
MT0409-94 9/28/0412:34 SILVER 0.24 J ug/g <0.22 MDL
Peer Review:
Page 2 of 2
ATK THIOKOL
PROPULSION
15-Oct-04
Quality Control Aliquot
Quality Control Report
Department: Metals Analysis
WS0409-080
601 OB Metals S
Aliquot Reference Aliquot
Aliquots on Worksheet
0409020-13A1
0409020-14A1
0409020-15A1
0409020-16 Al
0409020-17A1
0409O2O-18A1
0469026-19A1
0409020-30A1
0409020-31A1
0469020-32A1
ICP QCS19 Metals
MT0469-73
ICP QCS07 Metals
MT6469-74
(MSD) Matrix Spike Duplicate
MT0409-81 MT0409-80
(MS) Matrix Spike
MT0409-80 0409020-13A1
Date Tested
9/28/04 09:44
9/28/04 09:52
3/28/04 09:55
9/28/04 09:58
snam 10:01
9/28/04 10:04
9/28/04 10:08
9/28/0410:11
9/28/0410:14
9/28/0410:17
9/2BA>4 09:19
9/28/04 09:22
9/28/04 09:49
9/28/04 09:47
(LRB) Laboratory Reagent Blank
MT0409-77 9/28/04 09:32
Test Parameter
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
(LFBD) Laboratory Fortified Blank Duplicate
MT0409-79 MT0409-78 a/28/04 09:38
(LFB) Laboratory Fortified Blank
MT0409-78 9/28/04 09:35
(ICV) Initial Calibration Verification
MT0409-75 9/28/04 09:26
(CCV) Continuing Calibration Verification
MT0409-82
(CALB) Calibration Blank
MT0409-76
MT6469-83
9/28/0410:20
9/28/04 09:29
9/28/0410:23
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
SILVER
CADMIUM
Measured Value
1.64
23.2
1.8
31
1.78
15.2
2.23
128
0.9 J
398
0.9 J
575
2.89
386
1.9
46
2.87
121
3.83
905
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Recovery RPD
(%Recov) Limits (RPD) Limits
979 ug/g 97.9 95-105
499 ug/g 99.7 95-105
38.9 ug/g 98.4 70-130 3.73 0-25
42.9 ug/g 139* 70-130 1.24 0-25
Non-homogeneous soil sample. Data accepted.
37.5 ug/g
43.4 ug/g
O.SJ ug/g
U ug/g
395 ug/g
146 ug/g
398 ug/g
146 ug/g
1940 ug/g
246 ug/g
1900 ug/g
240 ug/g
U ug/g
U ug/g
U ug/g
97.9
148*
70-130
70-130
Non-homogeneous soil sample.
98.7
97.2
99.5
97.6
97.0
98.4
94.9
96.1
<0.18
<0.22
76-136
70-136
70-130
70-130
90-110
90-110
90-110
90-110
<0.18
<6.22
<0.18
MDL
MDL
.845
.476
MDL
MDL
MDL
Data
0-25
0-25
Page 1 of 2
DRnDMi^inM" Quality Control Report
PROPULSION Department: Metals Analysis
15-Oct-04 WS0409-080
Quality Control Aliquot 6010B MetalS_S Recovery RPD
Aliquot Reference Aliquot Date Tested TestParameter Measured Value (%Recov) Limits (RPD) Limits
(CALB) Calibration Blank
MT0409-83 9/28/0410:23 SILVER U ug/g <0.22 MDL
Peer Review: -z
Page 2 of 2
ATK THIOKOL
PROPULSION
14-Oct-04
Quality Control Aliquot
Ailquot Reference Aliquot
Aliquots on Worksheet
0409046-01 Al
0409046-02A1
0409046-03A1
0409046-04A1
0409046-05A1
0409046-06A1
0409046-07A1
0409046-08A1
0409046-09A1
0409046-13A1
0409046-14A1
0409046-15A1
0409046-1 BAI
0409046-17A1
0409046-18A1
0409046-19A1
0409046-20A1
0409046-21 Al
0409046-22A1
0409046-23A1
0409046-24A1
0409046-25A1
0409046-26A1
0409046-27A1
0409046-28A1
0409046-29A1
(QCS) Quality Control Sample
100410-37
(MSD) Matrix Spike Duplicate
1C0410-42
1C0410-45
IC0410-41
1C0410-44
(MS) Matrix Spike
1C0410-41
10041044
0409046-08A1
0409046-27A1
Date Tested
10/6/0413:19
1Q/B/D413:35
10/6/04 13:52
10/6/04 14:08
lOrertM 14:25
10/6/0414:41
ICVEiflM 14:58
10/6/0415:14
1Q«n>4 16:20
1Q/6rt)416:37
10/6^416:53
10/6/0417:10
10/6/0417:26
10/6rt)4 17:43
10/6/0418:00
10/6«)4 18:16
10/6«)418:33
10/6/0418:49
10/6rt)419:39
10/6^19:55
10/6/04 20:12
10/6/04 20:28
10/6/04 20:45
10/6/04 21:01
10/6/04 21:51
10/6/04 22:07
10/6/0412:46
IQ/eW 15:47
10/6/04 21:34
1Q/6fl)415:31
10/6/04 21:18
(LRB) Laboratory Reagent Blank
IC0410-3B 10/6/0411:07
Quality Control Report
Department: lon Chromatography
WS0410-033
Perchlorate 314 (IC)_S
Test Parameter
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
(LFBD) Laboratory Fortified Blank Duplicate
IC0410-40 IC0410-39 10/5/04 11:56
(LFB) Laboratory Fortified Blank
IC041O-39 10/6/0411:40
(ICV) Initial Calibration Verification
1C0410-36
IC0410-52
IC0410-54
(DUP) Duplicate Sample
IC0410-55
1C0410-56
IC0410-57
IC0410-58
IC0410-59
lC0410-eO
IC0410-61
IC0410-62
1C0410-63
IC0410-64
IC0410-65
IC0410-66
0409046-01 Al
0409046-02A1
0409046-03A1
0409046-04A1
0409O46-O5A1
0409O46-O6A1
0409046-07A1
0409046-08A1
0409046-09A1
0409O46-13A1
0409046-14A1
0409046-15A1
10^6/0413:02
10/6/0419:22
10/7/04 01:42
10/6/04 22:40
10/6/04 22:57
106/04 23:13
10/6/04 23:30
10/6/04 23:46
10/7/04 00:03
10/7/04 00:19
10/7/04 00:36
10/7/04 00:52
10/7/04 01:09
10/7/04 01:58
10/7/04 02:15
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
Measured Value
U mgflcg
U mg/kg
U mg/kg
U m^g
U mg/kg
U mg/kg
< EQL mg/kg
U mg/kg
U mgflcg
U mg/kg
U mg/kg
U mg/kg
U mg/kg
U mgflcg
U mgflcg
U mg/kg
U mg/kg
U mg/kg
U mg/kg
U mg/kg
U mgflcg
U mg/kg
U mg/kg
U mg/kg
U mg/kg
U mgflcg
48.2 mgflcg
2.4 mgflcg
2.4 mgflcg
2.4 mg/kg
2.4 mgflcg
U mg/kg
22.1 mg/kg
22.3 mgflcg
3.7 mg/kg
3.6 mgflcg
3.6 mgflcg
U mg/kg
U mg/kg
U mg/kg
U mgflcg
Recovery
(•/.Recov)
96.4
93.4
95.8
93.3
96.4
88.4
69.2
91.3
90.5
90.1
Limits
90-110
85-115
85-115
85-115
85-115
<0.1
85-115
85-115
75-125
75-125
75 -125
RPD
(RPD) 1
.0803
.575
MDL
.847
0
0
0
200
High RSD due to values detected below EQL and near
U mg/kg
U mgflcg
< EQL mgflcg
U mg/kg
U mg/kg
0
0
3.13
10
30.9
High RSD due to values detected below EQL and near
U mg/kg
U mg/kg
13.1
200
High RSD due to values detected below EQL and near
U mgflcg 0
Limits
0-25
0-25
0-25
0-25
0-25
0-25
0-25
MDL
0-25
0-25
0-25
0-25
0-25
•MDL
0-25
0-25
•MDL
0-25
Pags 1 of 2
ATK THIOKOL
PROPULSION
14-Oct-04
Quality Control Aliquot
Aliquot Reference Aliquot
(DUP) Duplicate Sample
IC0410-67 0409046-16A1
IC0410-48
IC0410-69
IC0410-70
IC0410-71
IC0410-72
1C0410-73
IC0410-75
IC0410-76
1C0410-77
IC0410-78
IC0410-79
IC041040
1C0410-81
O409O46-17A1
0409046-18A1
0409046-19A1
0409046-20A1
0409046-21A1
0409046-22A1
0409046-23A1
0409046-24A1
0409046-25A1
0409046-26A1
0409046-27A1
0409046-28A1
0409046-29A1
(CCV) Continuing Calibration
1C041043
1C041046
IC0410-49
IC0410-50
IC0410-51
IC0410-53
IC0410-74
Date Tested
10/7/04 02:31
10/7/04 02:48
10/7/04 03:04
10/7/04 03:21
10/7/04 03:37
10/7/04 03:54
10^/04 04:10
10/7/04 04:43
10/7/04 05:00
10/7/04 05:16
10/7/04 05:33
10/7/04 05:50
107/04 06:06
10/7/04 06:23
Verification
1Q/6A)4 16:04
10/6/04 22:24
10/7/04 06:39
10/6/04 10:50
10W/D419:06
10/7/04 01:25
107/0404:27
Quality Control Report
Department: lon Chromatography
WS0410-033
Perchlorate 314 (IC)_S Recovery RPD
Test Parameter
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
Measured Value (%Recov) Limits (RPD)
U mgflcg 200
High RSD due to values detected below EQL and near
U mgflcg 200
High RSD due to values detected below EQL and near
U mgflcg 48.1
High RSD due to values detected below EQL and near
U mgflcg 200
High RSD due to values detected below EQL and near
U mgflcg 12.2
U mg/kg 0
U mgflcg 58.7
Limits
0-25
MDL.
0-25
MDL.
0-25
MDL
0-25
MDL.
0-25
0-25
0-25
High RSD due to values detected below EQL and near MDL.
U mg/kg 200 0-25
High RSD due to values detected below EQL and near
U mgflcg 0
U mg/kg 0
U mg/kg 0
U mg/kg 0
U mgflcg 200
High RSD due to values detected below EQL and near
U mgflcg 56.3
High RSD due to values detected below EQL and near
202. mgflcg 101 85-115
205. mgflcg 102 85-115
205. mgflcg 103 85-115
202. mgflcg 101 85-115
202. mgflcg 101 85-115
204. mgflcg 102 85-115
204. mgflcg 102 85-115
MDL
0-25
0-25
0-25
0-25
0-25
MDL
0-25
MDL
Analyst Review:
Peer Review:
)^ AWQ^
y^^/gy/i"*
Page 2 of 2
ATK THIOKOL
PROPULSION
14-Oct-04
Quality Control Aliquot
Aliquot Reference Aliquot
Aliquots on Worksheet
0409046-30A1
0409046-31 Al
0409046-32A1
0409046-33A1
0409046-34A1
0409046-35A1
0409046-36A1
0409046-37A1
0409046-38A1
0409046-39A1
O4O9O46-40A1
0409046-41 Al
0409046-42A1
0409046-43A1
O409046-44A1
0409046-45A1
0409046-46A1
0409046-47A1
0409046-48A1
0409046-49A1
0409046-50A1
0409046-51A1
0409046-52A1
0409046-53A1
0409046-54A1
0409046-55A1
0409046-56A1
0409046-S7A1
0409046-70A1
0409046-71A1
0409046-72A1
0409046-73A1
(QCS) Quality Control Sample
1C0410-83
(MSD) Matrix Spike Duplicate
1C0410-88 IC0410-87
IC0410-91
IC0410-94
IC0410-90
IC0410-93
(MS) Matrix Spike
IC0410-87 0409046-33A1
1C0410-90
1C0410-93
0409046-4SA1
040904e-73A1
Quality Control Report
Department: lon Chromatography
WS0410-042
Perchlorate 314 (IC).
Date Tested Test Parameter
10/12/0416:48 PERCHLORATE
10/12/0417:04 PERCHLORATE
10/12/0417:21 PERCHLORATE
1Q/12flM 17:37 PERCHLORATE
10/12/0418:27 PERCHLORATE
10n2/D4 18:43 PERCHLORATE
10/12/0419:00 PERCHLORATE
10/12/0419:16 PERCHLORATE
10/12/0419:49 PERCHLORATE
10/12/04 20:06 PERCHLORATE
10/12/04 20:22 PERCHLORATE
10/12/04 20:39 PERCHLORATE
10/12/04 20:55 PERCHLORATE
10/12/04 21:12 PERCHLORATE
10/12/04 21:29 PERCHLORATE
10/12rt)4 21:45 PERCHLORATE
10/12/0423:08 PERCHLORATE
10/12/0423:24 PERCHLORATE
10/12fl)4 23:41 PERCHLORATE
10/12/04 23:57 PERCHLORATE
10^3/04 00:14 PERCHLORATE
10/13/04 00:30 PERCHLORATE
1W13/04 00:47 PERCHLORATE
10/13/04 01:03 PERCHLORATE
10/13/0401:20 PERCHLORATE
10/13/04 01:38 PERCHLORATE
10^3/04 02:09 PERCHLORATE
ItVI 3/04 02:26 PERCHLORATE
10M3/04 02:42 PERCHLORATE
10/13/04 02:59 PERCHLORATE
10/13/04 03:15 PERCHLORATE
10/13/04 03:32 PERCHLORATE
10/12/0416:15 PERCHLORATE
10/12/0418:10 PERCHLORATE
1 Q/12/04 22:18 PERCHLORATE
10/13/64 04:05 PERCHLORATE
.10/12/0417:54 PERCHLORATE
10/12/64 22:02 PERCHLORATE
10/13/04 03:48 PERCHLORATE
(LRB) Laboratory Reagent Blank
IC0410-84 10/12/0414:36 PERCHLORATE
(LFBD) Laboratory Fortified Blank Duplicate
IC0410-86 1C0410-85 10/12/0415:25 PERCHLORATE
(LFB) Laboratory Fortified Blank
IC0410-85 10/12/0415:09 PERCHLORATE
(ICV) Initial Calibration Verification
IC041Ofl2 10/12/0416:31 PERCHLORATE
1C0410-100
IC0410-104
IC0410-127
(DUP) Duplicate Sample
IC0410-102 0409046-30A1
1C0410-103
IC0410-105
1C0410-106
0409046-31 Al
0409046-32A1
0409046-33A1
10/12/04 22:35 PERCHLORATE
10/13/04 05:11 PERCHLORATE
W13J0A 12:32 PERCHLORATE
10/13/04 04:21 PERCHLORATE
10/13/04 04:38 PERCHLORATE
10/13/04 05:27 PERCHLORATE
10/13/04 05:44 PERCHLORATE
_s
Measured Value
U mgflcg
U mgflcg
U mgflcg
U mgflcg
U mg/kg
U mg/kg
U mgflcg
U mgflcg
U mgflcg
U mg/kg
U mgflcg
U mgflcg
U mg/kg
U mg/kg
U mgflcg
U mgflcg
U mg/kg
U mgflcg
U mgflcg
U mgflcg
U mg/kg
U mg/kg
U mg/kg
U mgflcg
U mgflcg
U mgflcg
U mgflcg
U mgflcg
U mgflcg
U mg/kg
U mgflcg
U mgflcg
50.7 mgflcg
2.5 mg/kg
2.6 mg/kg
2.6 mg/kg
2.6 mg/kg
2.6 mgflcg
2.7 mg/kg
U mg/kg
23.4 mg/kg
22.5 mgflcg
3.7 mgflcg
3.7 mg/kg
3.7 mg/kg
4.7 mg/kg
U mgflcg
Recovery
(•/.Recov)
101
101
102
104
102
105
107
93.6
90.0
91.8
92.8
93.0
116
Limits 1
90-110
85-115
85-115
85-115
85-115
85-115
85-115
<0.1
85-115
85-115
75 • 125
75-125
75-125
75 -125
RPD
[RPD) Limits
.99
2.41
3.03
MDL
4
200
High RPD due to values detected below EQL and near
U mgflcg 0
U mg/kg 200
High RPD due to values detected below EQL and near
U mg/kg 0
0-25
0-25
0-25
0-25
0-25
MDL
0-25
0-25
MDL
0-25
Page 1 of 2
ATK THIOKOL
PROPULSION
14-Oct-04
Quality Control Aliquot
Aliquot Reference Aliquot
(DUP) Duplicate Sample
IC0410-107
IC0410-108
IC0410-109
IC0410-110
IC0410-111
ICO410-112
IC0410-113
IC0410-114
IC0410-116
IC0410-117
IC0410-118
IC0410-119
IC0410-120
IC0410-121
IC0410-122
IC0410-123
1C0410-124
IC0410-12S
100410-128
100410-129
ICO41O-130
IC0410-131
IC0410-132
IC0410-133
100410-134
IC0410-135
IC0410-136
IC0410.137
0409046-34A1
0409046-35A1
040fl046-36A1
0409046-37A1
0409046-3BA1
0409046-39A1
0409046-40A1
0409046-41 Al
0409046-42A1
0409046-43A1
0409046-44A1
0409046-45A1
0409046-46A1
0409046-47A1
0409046-48A1
040904e-49A1
0409046-50A1
0409046-51A1
0409046-52A1
0409046-S3A1
0409046-54A1
0409046-55A1
0409046-56A1
0409046-57A1
0409046-70A1
0409046-71 Al
0409046-72A1
0409046-73A1
Date Tested
10^3/04 06:00
10/13fl)4 06:17
IOM 3/04 06:33
ion 3rt)4 07:13
ton 3A>4 07:30
10^3/0407:46
10/13/04 08:03
10/13/04 08:19
10/13/04 09:31
10/13/04 09:47
10/13/0410:04
10/13/0410:20
10/13^416:37
10/13/0410:53
ion 3/0411:10
10/13/0411:26
10/13/0411:43
10/13/0411:59
IOM 3fl)412:49
1W13^413:05
10/13/0413:22
10n3rt)413:38
10/13/0413:55
10/13/0414:11
10/13/0414:28
10/13/0414:44
10/13/0415:01
10/13/0415:17
(CCV) Continuing Calibration Verification
1C0410-49
1C0410-92
IC0410-95
IC0410-98
IC0410-99
IC0410.101
1C0410-115
1C0410-126
10^2/04 19:33
10/12rt)4 22:51
10/13/04 01:53
10/131/0415:34
10/12/0414:19
10/13/04 04:54
10/13/04 08:36
10/13/0412:16
Quality Control Report
Department: lon Chromatography
WS0410-042
Perchlorate 314 (IC)_S
Test Parameter
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
Measured Value
U mgflcg
Recovery
(•/.Recov)
RPD
Limits (RPD)
200
High RPD due to values detected below EQL and near
U mg/kg 0
U mgflcg
U mg/kg
U mg/kg
U mgflcg
<EQL mgflcg
0
0
0
0
200
High RPD due to values detected below EQL and near
U mgflcg 0
U mg/kg 200
High RPD due to values detected below EGL and near
U mg/kg 0
U mgflcg 200
Limits
0-25
MDL
0-25
0-25
0-25
0-25
0-25
0-25
MDL.
0-25
0-25
MDL
0-25
0-25
High RPD due to values detected below EQL and near MDL.
U mgflcg 0 0-25
U mgflcg
U mg/kg
U mgflcg
U mgflcg
0.6 mgflcg
0
0
0
0
200
0-25
0-25
0-25
0-25
0-25
High RPD due to values detected below EQL and near MDL.
U mgflcg 0 0-25
U mgflcg
U mgflcg
U mg/kg
U mg/kg
U mgflcg
U mgflcg
U mgflcg
U mgflcg
U mg/kg
0
0
0
0
0
0
0
0
200
High RPD due to values detected below EQL and neai
U mg/kg 0
213. mgflcg
213. mgflcg
218. mgflcg
223. mg/kg
204. mgflcg
220. mgflcg
223. mgflcg
218. mg/kg
107
107
109
111
102
110
111
109
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
•MDL
0-25
/Analyst Review:
Peer Review:
Page 2 of 2
ATK THIOKOL
PROPULSION
21-Oct-04
Quality Control Aliquot
Aliquot Reference Aliquot
Aliquots on Worksheet
0409046-10A1
0409046-1 IAI
0409046-12A1
0409046-58A1
04O9046-59A1
040904e-60A1
0409046-61 Al
0409046-62A1
0409046-e3A1
0409046-64A1
0409046-65A1
0409046-66A1
0409046-67A1
0409046-6BA1
0409046-69A1
(QCS) Quality Control Sample
IC0410-294
(MSD) Matrix Spike Duplicate
IC0410-300 IC0410-299
(MS) Matrix Spike
IC0410-299 0409046-62A1
Date Tested
^0!20m 17:10
lOffiOW 17:26
10^0/0417:43
1Q«0/04 17:59
10/20/04 18:16
10«0/04 18:32
10/20fl>418:49
10/20/0419:05
10/20/04 20:11
10/20/04 20:28
10«O/04 20:44
10/20/04 21:01
10/20/04 21:17
1Q«0/04 21:34
10«0/04 21:50
lOflOAM 16:37
10fi!0/0419:38
10/20/0419:22
(LRB) Laboratory Reagent Blank
1C0410-295 10/20/0414:58
(LFBD) Laboratory Fortified Blank Duplicate
IC0410-297 100410-296 10^0-04 15:47
(LFB) Laboratory Fortified Biank
1C0410-296 1000/0415:31
(ICV) Initial Calibration Verification
100410-293
IC0410-327
(DUP) Duplicate Sample
1C0410-298
IC041O-301
IC0410-302
IC0410-303
IC0410-305
IC0410-308
IC0410-309
IC0410-310
IC041O-312
1C0410-315
1C0410-316
IC0410-317
IC0410-319
IC0410-322
IC0410J23
0409046-1 OAI
0409046-1 IAI
0409046-12A1
0409046-58A1
040904S-59A1
0409046-60A1
0409048-61A1
0409046-62A1
0409046-63A1
0409046-64A1
0409046-65A1
0409046-66A1
0409046-67A1
0409046-68A1
0409046-69A1
(CCV) Continuing Calibration'
1C0410-304
IC0410-311
IC0410-318
1C0410-325
10/20/0416:53
10/20/04 23:13
10«0/04 22:07
10/20/04 22:23
10/20/04 22:40
10^0/04 23:29
10/20/04 23:46
10/21/04 00:02
10/21/04 00:18
10/21/04 00:35
10/21/04 00:52
10/21/04 01:08
10/21/04 01:25
1001/04 01:41
10/21/04 01:58
10^1/04 02:31
1001/04 02:48
y^erification
1000/0419:55
1000/04 22:56
1001/04 02:15
1001/04 03:04
Quality Control Report
Department: lon Chromatography
WS0410-081
Perchlorate 314 (IC)_W
Test Parameter
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
Measured Value
U
U
U
u u u u u
u
u
u
u
u u u
49.7
251
252
4.22
24.1
23.9
<EQL
ugfl.
ugfl.
ugfl.
ugfl.
ugfl.
ug/L
ug/L
ugfl.
ugfl.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugfl.
ugfl.
ugfl.
ug/L
ug/L
ugfl.
ug/L
< EQL ugfl.
U
U
U
U
U
U
U
U
U
U
U
U
u
u u
211
213
213
214
ugfl.
ug/L
ugfl.
ugfl.
ug/L
ug/L
ug/L
ug/L
ugfl.
ugfl.
ug/L
ug/L
ugfl.
ug/L
ugfl.
ugfl.
ugfl.
ugfl.
ugfl.
Recovery
(•/.Recov)
99.4
100
101
96.5
95.4
92.0
94.0
105
107
106
107
RPD
Limits (RPD)
90-110
85-115
85-115
<1
85-115
85-115
75-125
75 -125
89.1 -118
89.1-118
89.1 -118
89.1-118
.557
MOL
1.07
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Limits
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
Page 1 of 2
DDO JMrcir?M Quality Control Report
PROPULSION Department: lon Chromatography
21-Oc<-04 WS0410-081
Quality Control Aliquot Perchlorate 314 (IC)_W Recovery RPD
Ailquot Reference Aliquot Date Tested TestParameter Measured Value (%Recov) Limits (RPD) Limits
(CCV) Continuing Calibration Verification
IC041O-326 1000/0414:41 PERCHLORATE 206 ugfl. 103 89.1-118
/ 77
/^l^fM Analyst Review:
Peer Review: /<n^'~^^^ /*ALA'^
Page 2 of 2
ATK Thiokol, inc.
Promontory, Utah
Results of M-39 antd M-636 Sampling
October 2005
APPENDIX B
Field Notes
EarthFax Engineering, Inc.
.Mi^"^..Mk.M_3k.. Mov>.(sM.li^A .^^.^.^Al
J>A\/t"„„6?3{/_^r_6T]D.Ai., .„.P/V..y>_. d.A/^^ .:j_..o>f?_^^.. .H^kA:C>^.
/v^.'.'i,^ S^.^^p_L<ri___i_r_?
A)..^. y 3 (o .,<fe/ii.eu:s A .r. 1 / _
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Thiokol Photographic Waste Site Closure
W0#: IB909 LWR#: El
SITE: M-39 _
DESCRIPTION: Surface, M39-9-04^ T/B
PARAMETERS METHOD
CADMIUM, SILVER 6010
Date 9/14/04 Time "^ ! ^-O Sampler X^/il p^A
Thiokol Photographic Waste Site Closure
W0#: 1B909 LWR#: El
SITE: M-39
DESCRIPTION: Surface, M39-9-04-01
PARAMETERS METHOD
CADMIUM, SILVER 6010
Date 9/14/04 Time ^."^r Sampler ^\/^ j Ql^-
3ure wn! ,on P^'^t^g'-aphic Waste Site Closi
WO#:1B909 LWR#: El
SITE: M-39
DESCRIPTION: Suiface, M39-9-04-09
^^^^^^^^ETERS METHOD
CADMIUM, SILVER mdHQU 6010
DateM4/04
i ^Oy^.M^I J^^^^^Km
Mfy
Time^/f'.^ Sampler £>^ j Ql^O
i,:-_-f,L-w»3Hs»*^;r'j:i^-»A^*;.=-CJ-.-*i^-n!
Thiokol Photographic Waste Site Closure
W0#: 1B909 LWR#:E1
SITE: M-39
DESCRIPTION: Surface, M39-9-04-03
PARAMETERS METHOD
CADMIUM, SILVER 6010
'piuf w ^w^/^vsr^^
Date 9/14/04 Time <^^^ Sampler J^ (/^^ , ^
Thiokol Photographic Waste Site Closure
W0#: 1B909 LWR#: El
SITE: M-39
DESCRIPTION: Surface, M39-9-04-04
PARAMETERS METHOD
CADMIUM, SILVER 6010
^^7
Date 9/14/04 Time } Q \ (yt^ Sampler ^^^/Q
Thiokol Photographic Waste Site Closure
W0#: 1B909 LWR#: El
SITE: M-39
DESCRIPTION: Surface, M39-9-04-05
PARAMETERS METHOD
CADMIUM, SILVER 6010
J-O'
^>t:C:^i^/GrmrV^lSL<r'
Date9/14/04 Time \O',0S Sampler n^y Qi^
W0#: 1B909 LWR#: El
SITE: M-39
DESCRIPTION: Surface, M39-9-04-06
PARAMETERS METHOD
CADMIUM, SILVER 6010
.^vu^j^y _;^M-t/arL/
Date 9/14/04 Time/l)'iL) Sampler f'V'Wy' /
"I.-'.r.-J TH.-^j. !.:_ tJ7„„A„ CMi... /-!>,
xntnunpncntj^jiuj I. liiJUlW<WgM!«rpWWl|^BlWWMJB^J^™W^
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. j W0#: 1B909 LWR#: El
i SITE: M-39
j DESCRIPTION: Surface, M39-9-04-07
' PARAMETERS METHOD
I CADMRJM, SILVER 6010
Date 9/14/04 rime /6 '• /? Sampler ^\1 ^ I^ ^C
iiiioKoi rnotograpnic nasre Mie closure
W0#: 1B909 LWR#: El
SITE: M-39
DESCRIPTION: Surface, M39-9-04-08
PARAMETERS METHOD
CADMIUM, SILVER 6010
Stc r <c?/6^,
Date 9/14/04 Tim^/Dr/S" Sampler p,//y/^^^
m
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WO#:lB909 LWR#: El
SITE: M-636
DESCRIPTION: Surface, M636-9-04-0r
PARAMETERS METHOD
CADMIUM, SILVER 6010
m :1
'^
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m
m W^.:'
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Date 9/J 4/04 Time ib'Ah Sampler Pi^
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WOtt: IB909 LWR#: El
SITE: M-636
DESCRIPTION: Surface, M636-9-04-02
PARAMETERS METHOD
CADMIUM, SILVER 6010 ^)LTj ^/tf C
Date 9/14/04 Time |D:43 Sampler fl/M"
VL^ " ""
~I1. - . 1. . 1 T%1. , 4 . :_ ^X7__i_ c;4„ /-'i„.
j inioKui riiuiograpiiii; vvasie oite V.-1USU1C
I WOtt: 1B909 LWRtt: El
I SITE: M-636
I DESCRIPTION: Suiface, M636-9-04-03
1 PARAMETERS METHOD
CADMIUM, SILVER 6010
Date 9/14/04 Time jp; cjtz^ Sampler
Ml m
9m':
Tiiidkoi rh'otogi^apnic vvaste Site Closure
W0#: 1B909 LWRtt: El
SITE: M-636
DESCRIPTION: Suiface, M636-9-04-04
PARAMETERS METHOD
CADMIUM, SILVER 6010
Date 9/14/04 Time (Q: yt> Sampler ^]4
/^ U-r
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Thiokol Photographic Waste Site Closure
WOtt^:J.B909 LWRtt: El
SITE: M-636
DESCRIPTION: Surface, M636-9-04-05
PARAMETERS METHOD
CADMIUM, SILVER 6010
Date 9/14/04 Time \{)-<A Sampler fVI^
0^
$4/14^ ^ (:fMy'l<^^~-~i
•
Thiokol Photographic Waste Site Closure
WOtt: 1B909 LWRtt: El
SITE: M-636
DESCRIPTION: Surface, M636-9-04-06
PARAMETERS METHOD
CADMIUM, SILVER 6010
^L^T' Jj^^^^ f
Date 9/14/04 Time /j ; ^6 Sampler WM
QU^
Thiokol Photographic Waste Site Closure
WOtt: 1B909 LWRtt: El
SITE: M-636
DESCRIPTION: Suiface, M636-9-04-07
PARAMETERS METHOD
CADMIUM, SILVER 6010
^!^J\.<^^y^,.
Date 9/14/04 Time |( -. ol- Sampler f^\^/
Thiokol Photographic Waste Site Closure
W0#: 1B909 LWRtt: El
SITE: M-636
DESCRIPTION: Suiface, M636-9-04-08
PARAMETERS METHOD
CADMIUM, SILVER ^^
Date 9/14/04 Time |f« 04 Sampler ?V(^ -^ - - _-_. ^ v^
Thiokol Photographic Waste Site Closure
WOtt: 1B909 LWRtt: El
SITE: M-636
DESCRIPTION: Suiface, M636-9-04-09
PARAMETERS METHOD
CADMIUM, SILVER 6010
.^ibT
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Date 9/14/04 Time ({''-^if, Sampler f \/V^
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WOtt: 1B909 LWRtt: El
SITE: M-636
DESCRIPTION: Suiface, M636-9-04-10
PARAMETERS METHOD
CADMIUM, SILVER 6010
Date 9/14/04 Time /(:D7 Sampler ^ (_^
Thiokol Photographic Waste Site Closure
WOtt: 1B909 LWRtt: El
SITE: M-636
DESCRIPTION: Suiface, M636-9-04-11
PARAMETERS METHOD
CADMIUM, SILVER 6010
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DESCRIPTION: Surface, M636-9-04-12 ^ "" ^ "
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Thiokol Photographic Waste Site Closure
WOtt: 1B909 LWRtt: El
SITE: M-636
DESCRIPTION: Surface, M636-9-04-13
PARAMETERS METHOD
CADMIUM, SILVER 6010
Date 9/14/04 Time )]; j-^ Sampler f ^^^ ^^
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i WOtt: 1B909 LWRtt: El
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DESCRIPTION: Suiface, M636-9-04-14
PARAMETERS METHOD
: CADMIUM, SILVER 6010
Date 9/14/04 Time /[ : jg- Sampler ^"^ Ijl' y-
i ^/"oAro/ Photographic Waste Site Closure
\ WO#:1B909 LWRtt: El
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i PARAMETERS METHOD
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; SITE: M-636
i DESCRIPTION: Suiface, M636-9-04-I6
I PARAMETERS METHOD
I CADMIUM, SILVER 6010
; Date 9/14/04 Time U'-V^ Sampler f^'pL^
S^ijr i/^y^.3
! Thiokol Photographic Waste Site Closure
i WOtt: 1B909 LWRtt: El
i SITE: M-636
I DESCRIPTION: Surface, M636-9-04-17
! PARAMETERS METHOD
I CADMIUM, SILVER 6010
Date 9/14/04 Time W^'^ Sampler ^^ rsl^
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Thiokol Photographic Waste Site Closure
WO#:1B909 LWRtt: El
SITE: M-636
DESCRIPTION: Suiface, M636-9-04-18
PARAMETERS METHOD
CADMIUM, SILVER 6010
Date 9/14/04 Time l\'t^ Sampler pV l4
c_
5|LT i.&lU\/^.U
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Thiokol Photographic Waste Site Closure
W0#: 1B909 LWRtt: El
SITE: M-636
DESCRIPTION: Surface, M636-9-04-19
PARAMEIERS 7™^
CADMIUM, SILVER 6010
Date 9/14/04 Time H-gcf Sampler ^^
Thiokol Photographic Waste Site Closure
: WOtt: 1B909 LWRtt: Ei
-: SITE: M-636
' DESCRIPTION: Surface, M636-9-04-20
PARAMETERS METHOD
; CADMIUM, SILVER 6010
Date 9/14/04 Time ((;J'? Sampler ''^ r)^,^
Thiokol Photographic Waste Site Closure
WOtt: 1B909 LWRtt: El
SITE: M-636
DESCRIPTION: Suiface, M636-9-04-21
PARAMETERS METHOD
CADMIUM, SILVER 6010
Date 9/14/04 Time (j ^^i Sampler f •/^^T>U6>
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Thiokol Photographic Waste Site Closure
WOtt: 1B909 LWRtt: E),
SITE: M-636 .
DESCRIPTION: Surface, M636-9-04-22
PARAMETERS METHOD
CADMIUM, SILVER 6010
Date 9/14/04 Time /4-'2p SamplerP^ c
pl/[^
Thiokol Photographic Waste Site Closure
WOtt: IB909 LWRtt: El
SITE: M-636
DESCRIPTION: Surface, M636-9-04-23
PARAMETERS METHOD
CADMIUM, SILVER 6010
I Date 9/14/04 Time \s,:^g Sampler '^^^ ^
Thiokol Photographic Waste Site Closure
WOtt: 1B909 LWRtt: El
SITE: M-636
DESCRIPTION: Surface, M636-9-04-24
PARAMETERS METHOD
CADMRJM, SILVER 6010
Date 9/14/04 Time Sampler V v,
; Thiokol Photographic Waste Site Closure
! WOtt: 1B909 LWRtt: El
! SITE: M-636
DESCRIPTION: Suiface, M636-9-04-25
PARAMETERS METHOD
CADMIUM, SILVER 6010
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Thiokol Photographic Waste Site Closure
WOtt: 1B909 LWRtt: El
SITE: M-636
DESCRIPTION: Surface, M636-9-04-26
PARAMETERS METHOD
CADMIUM, SILVER 6010
Date 9/14/04 Time j^'y Sampler P^'^pl/i^
Thiokol Photographic Waste Site Closure
WOtt: 1B909 LWRtt: El
SITE: M-636
DESCRIPTION: Surface, M636-9-04-27
PARAMETERS METHOD
CADMIUM, SILVER 6010
Date 9/14/04 Time j ^Ot Sampler ^^f^y_
Thiokol. Photographic Waste Site Closure
I WOtt: 1B909 " LWRtt: El
I SITE: M-636
: DESCRIPTION: Surface, M636-9-04-28
1 PARAMETERS METHOD
: CADMIUM, SILVER 6010
: Date 9/14/04 Time j^ 03 Sampler J^^^^
Thiokol Photographic Waste Site Closure
WOtt: 1B909 LWRtt: El
SITE: M-636
DESCRIPTION: Surface, M636-9-04-29
PARAMETERS METHOD
CADMIUM, SILVER 6010
Date 9/14/04 Time 1 S" 6 ^ Sampler P^-^
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Thiokol Photographic Waste Site Closure
WOtt: 1B909 LWRtt: El
SITE: M-636
DESCRIPTION: Surface, M636-9-04-30
PARAMETERS METHOD
CADMIUM, SILVER 6010 ^icr^^ i,-L'e^L G%f{
Date 9/14/04 Time \C,Q% Sampler ^^^ ,.^
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Thiokol Photographic Waste Site Closure
WOtt: 1B909 LWRtt: El
SITE: M-636
DESCRIPTION: Surface, M636-9-04-31
PARAMETERS METHOD
CADMRJM, SILVER 6010 vJtz (1 Sl LT 3^
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Date 9/14/04 Time If;f3 Sampler ^ f vH
Thiokol Photographic Waste Site Closure
WOtt: 1B909 LWRtt: El
SITE: M-636
; DESCRIPTION: Suiface, M636-9-04-32 .
PARAMETERS METHOD
CADMIUM, SILVER 6010
Date 9/14/04 Time f^'l^ Sampler P^^,.'
Thiokol Photographic Waste Site Closure
WOtt: 1B909 LWRtt: El
SITE: M-636
DESCRIPTION: Suiface, M636-9-04-33
PARAMETERS METHOD
CADMIUM, SILVER 6010
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Date 9/14/04 Time \<^\ Sampler "'^ -^\(^V
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Thiokol Photographic Waste Site Closure
WOtt: 1B909 LWRtt: El
SITE: M-636
DESCRIPTION: Suiface, M636-9-04-34
PARAMETERS METHOD
CADMIUM, SILVER 6010
Date 9/14/04 Time j'^'Z-'J Sampler ^ a\^W
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r/uo^oZ Photographic Waste Site Closure
WOtt: IB909 LWRtt: El
SITE: M-636
DESCRIPTION: Surface, M636-9-04-35
PARAMETERS METHOD
CADMIUM, SILVER 6010
1
1 Date 9/14/04 Time '5'^°^ Sampler y ^
G^\l'ci $AtJP ivu.\ CLI
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Thiokol Photographic Waste Site Closure
WOtt: 1B909 LWRtt: El
SITE: M-636
i DESCRIPTION: Surface, M636-9-04-36
j PARAMETERS METHOD
! CADMIUM, SILVER 6010
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Date 9/14/04 Time j^ ^ J Sampler > ^y^
y^\\ ^*4*Tf Q.r'Hi^i
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Thiokol Photographic Waste Site Closure
WOtt: 1B909 LWRtt: El
SITE: M-u36
DESCRIPTION: Suiface, M636-9-04-37
PARAMETERS METHOD
CADMIUM, SILVER 6010
Siur i ^wH'T^
- I Date 9/14/04 Time \<^<j Sampler V^p^fi
mfmt.j!m!'XK^i,jt^snv.s,^imiiv.'X'ky£WM!m.^ E^Sf5H§Si»StSffi!?*J'!fiS
[ Thiokol Photographic Waste Site Closure
i W0#: 1B909 LWR#: El
i SITE: M-636
i DESCRIPTION: Surface, M636-9-04-38
j PARAMETERS METHOD
i CADMIUM, SILVER 6010 QfiM^i .(lA 21^^^-
Date 9/14/04 Time K}^ Sampler P^ r>^\f-
Thiokol Photographic Waste Site Closure
WOtt: IB909 LWRtt: El
SITE: M-636
DESCRIPTION: Suiface, M636-9-04-39
PARAMETERS METHOD
CADMIUM, SILVER 6010
X) U ^
Date 9/14/04 Time [(J 41 Sampler ^•J i+
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i Thiokol Photographic Waste Site Closure
i WOtt: 1B909 LWRtt: El
i SITE: M-636
•; DESCRIPTION: Surface, M636-9-04-40
i PARAMETERS METHOD
i CADMIUM, SILVER 6010
^AA
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Date 9/14/04 Time \"S^J Sampler ^ ^s^W
Thiokol Photographic Waste Site Closure
WOtt: 1B909 LWRtt: El
SITE: M-636
DESCRIPTION: Suiface, M636-9-04-41
PARAMETERS METHOD
CADMIUM, SILVER 6010
5:A^
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Date 9/14/04 Time i^-^^ Sampler V^ (^^^p
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ENVIRONMENTAL LAB WORK REQUEST <^y^9^V6'
IfO: THIOKOL ENVIRONMENTAL LABOUATORY
(••KOM:.
JOHN HOLLADAY
ORGi\NIZATtON;
ENViRONMENTAL SERVICES
aXTES'SiON:
6895
NlAlLSToi-;;
301;
LWR No. E12435
Login No.
COSfCENTEK:
8200
KEPORT Rr^SULlTi TO:
WOKK ORDER:
IB907
DATE:
29:Sepl 2004
HELEN RAVSTEN
SAMPLE INFORMATION
SAMPIJi:
i,'M39-9-04-01
i.M39-9-04-Q2;
-3;:M39-9-04-03^
4v:Ni39-9-04-04^
5. M39-9-04-05:
6; M39.9-04-d6
7:M39-9-04-07
\ ^ M39-9-^04.()8
• 9, M39-9-04-09
io:M3:9-9-04TB
i,.M39-9-04EB [
.2M39-9-04EB
.3M636-9-04-1
DATE
14Sep04
I4Sep04,
I4Sep04
:14Sep04
14Sep04
14Sep04
I4Sep04
14Sep04
I4Sep04
I4Sep04 ;
14Sep04
14Sep04
14Sep04 J
TYPE
r^
;
X
>^-.
X
X
X
X
X
x :
X
X
•;x..:
X
.X-..
, LpCAtlQtV
#39:
M-39
MT39
M-39
M-39
M^39
M-59
M-39
M-39
M-39
M-39
M-39
M-636
TtMl?
9:45
9:50
9:55
10:00
10:05
1Q:10
10:13
10:15
10:05
09:30
09:50
09:50
10:54
TEST
Perchlorate
Perchiorate
Perchiorate
Perchlorate
Perchl oraite
Perchlorate
Perchlpfate
Perchl grate
Perchlorate
• - • .*.,••
Perchlorate
Perehlorate
Perchlorate
Perchlorate
REMARK.S
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
\/JaXi^<.
uJ^^iltuc..
lOfdtU^
Soil:
CHAIN OF CUSTODY
RKLINQUlSnED.BY
<Q^cMfU^
DATE
i-lferof
TTVfE
(0- s<^
rUCCEIVEDBY
^fky&iM>
DATE
i-^'y-^Y
TIME
/IPSO
•t FDR LABORATORY USE ONLY
DATECCMI'LLTUD: DATE j^nPORTnp SIGNATURE
ENVIRONMENTAL LAB WORK REQUEST
(P¥P^(P'^&^
Lo: THIOKOL ENVIRONMENTAL LABORATORY
FROM:
JOHN HOLLADAY
ORGANIZATIO.V:
ENViRONMENTAL SER VICES
EXTUNSlbN:
6895
MAILSTOi*;
301
LWRNo.Ei2435
Login No.
COirr CENTER::
8200
REPORr RESULTS Ta:
WOKK.ORDRR:
1B907
6 ATli
29 Sepl 2004
HELEN RAVSTEN
«
SAMPLE;
::»,M636.9-p4-0g
,5.,M636^9-04-03
14 M636-9.04.04
i7,.M636-9-04-05
:,a; M636-9-04-06
,?: M636-9-04-07
20, M636-9-04-Q8
p.. M636-9-O4-09
:i. M636-9-64-I0
25, M636-9-d4-l I
24M636-9-04-12
.3M636-9-04-13
^G,M636-9-04-14
PATK
14Sep04
.14Sep04:
14Sep.p4
;i4Sep04
14Sep04::
l4Sep04
I4Sep:04'^
I4Sep04
i4Sep04
14Sep04
14Sep04 :
14Sep04
14Sep04
TYPE
W&^
'\
X
;X';
;:x.
X
K
X
X
X
:.X.^
X
X
•X^ •
X
SAIMPLE INFORIWATION
LOCATION
M-636
M-636
M-636
M-636:
;M-636:
M-63;6
M-636
M-636:
M-636
'M^636
;M-636
M-636
M-636
TIME
10:43
10:45
1Q:50
10:54
11:00
11:02:
11:04
11:06
11:08
11:10-
11:15
11:17
11:18
TEST
Perchlorate
Perchlorate
Perchlorate
Perch lora:ie
Perchlorate
Perchlorate
Perchlorate
Pei-chlorate
Perchlorate;
Perchlorate
Perchlorate
Pei-chi orate
Perchlorate
Rr.MMlKS
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
CHAIN OF CUSTODY
lilELlNQUlSliEU UY
c^^ \m.dju 1
DATE
•2^^eroA
TliviE
(D:S0
lUXEIVEDUV
^(^c^da^^
• -
DAI'E
^_2f-^^/
TIME
/ P S'O
^
FOR LABORATORY USE ONLY
DATP. COMPLETT-D DA TE KEPORTED
ENVIRONMENTAL LAB WORK REQUEST C>^09P¥h
€ THIOKOL ENVHiONMENTAL LABORATORY LWRN0.EI2435
Login No.
FRO.M:
JOHN HOLLADAY
; EXTENSION:
6895::
COSTrENTER:
8200
WORK ORDER:
1B907 29 Sepl .2004
ORGANIZATION:
ENVIRONMENTAL SERVICES
REPORT RESULTS TO:
301 HELEN RAVSTEN
SAMPLE INFORMATION
SAMPLE
77:,:M63(5-9^04-15
28. M636-9-04-16:
29.M636-9-04-17
JO. M636-9-04-:i8
3i. M636-9-d4-19
31 M636-9-04.2d
:33.M636-9-04-21
^M63^-9-04.22:
35„M636-9-04-23
3«. M636-9-04-24
37 M636-9-04~25
:38M636-9-G4-26
39.M636-9-04-27
DATE
14Sep04
l4Sep04
14Sepd4
14Sep04
14Sep04
l'4Sep04
14Sep04
14Sep04
14Sep04
;14Sepp4
14SepP4
14Sep04
14Sep04
TYPE
j;
••-'
•X
X
X
X
X
X
X
:x.
X
X
X
X
X
LQGATION
M^636
M-636
M-^35
.M^636
M-636
M-636
M-636
M.636
mme
M-636
M-636
M-636
M-636
TIME
11-22
11:26
11:28
11:32
11:35
U:37
ll.;42
14:40
14:40
14:4-5
14:50
14:55
15:00
TEST
Perchloraitei;
Perchlorate
Perchlorate
Perchlorate;
: Perc hi orate;
Perehlorate
Perchlo]-ate
Peithidrate
Perchlorate
Perchlorate
Pei'Chlbratb
Perch Icirate
Perchlorate
lU'AUKKS
Soil
Soil
Soil
Soil
Soil
Soil
•
Soil
Soil
Soil
Soil
Soil
Soil
Soil
CHAIN OF CUSTODY
liELINQUISHEp UY
'ai^^thraAjl
DATE
^%-M
TIME
fc^:^
RECEIVEDBY
l^J >5^fe^
DATE
^-^^-<P^/
•riME
/^ <rzp
\
FOR LABORATORY USE ONLY
ATECO.MPIJ-TRD DATE RUPOIflED
ENVIRONMENTAL LAB WORK REQUEST ovmp¥<^
ko THIOKOL ENVIRONMENTAL LABORATORY
1H0.S1-:
JOHN HOLLADAY
ORGANIZATION:
ENVIRONMENTAL SERVICES
EXTENSION:
6895
MAILSTOP:
301
LWR No. El2435
Login No.
COST CENTER:
8200
REPORT KESULTS TO:
WORKORDER;
1B907
DATE:
29 Sept 2004
HELEN RAVSTEN
SAMPLE
^, M636f9-04-28
4L M636-9-G4-29
:.2,M636-9-04-30
:.3 :M636-9-04-31
.4.:M636^9-04^32 '
4j.:M636-9-04-33 ^
«; M636-9-04-34
|7.vM636r9-d4-35
48 M636-9-d4-36:
49, M636-9-04-37
50 M636-9-04-38
M,M636-9-04-39
5:-M63 6-9-04-40
DATE
14Sep04
14Sep04
14Sepp4
14SepP4
14Sep04
I4Sep04
14Sepp4 "
14Sepd4
l4Sep04
14Sep04
14Sep04
14Sep04
14Sep04
TYPE
^: . ..if:?
X
X
X:
•X.
X
X
X
X.
x;
X
X
X:
X
SAMPLE INFORMATION
LOCATION
M^636
M-636
M-636,-
M-636
M-636
M-636
M-636
M-63:6
M-636
M-636
M.636
M-636:
M-636
TIME
15:03
15:05
15:08
15:13
15:19
15:21
15:25
15:29
15:33
15:35
15:38
15:41
15:45
TEST
•
Perchlorate
Perchlorate
Perchlorate
Perchlorate
Pei-chl orate
Pei-chlorate
Perchlorate
Perchlorate
Perchlorale
Perchlorate
Perchlorate
Perchlorate
Perchlorate
lilCMARKS
-
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
:Soil
Soil
Soil
Soil
Soil
CHAIN OF CUSTODY
lUiLiNQUISIIlip UY
mLctmj.^ J ^
PATE
nSsfiTM
TLME
hyfii
RECEIVEDBY
'y'^'uSa;^
DATE
^'^%oY
TIME
•fO^D
1 FOR LABORATORY USE ONLY
DATE COMPLIED DAIT: Rl-POR:rED SIGNATIIRE
ENVIRONMENTAL LAB WORK REQUEST (P^O'TC) H^e>
^THIPKOL ENVIRONMENTAL LA.BORATORY
FROM;
JOHN HOLLADAY
ORGANIZATIO.N:
EIIVIRONMENTAL SERVICES^
EXTENSION:
6895
MAIL STOP:
301
LWR No. El2435
Login No.
XOSTCiiNTi-R:
8200
REPORT RESUI.-rS TO;
WORK ORDER:
IB9d7
DATU;
29 Sept 2004
HELEN RAVSTEN
SAMPLE INFORMATION
.•SAMPLE
«; M63.6-9-04-41
5+M636^9-0442
33:M636-9-04-43
56. M63:6-9-04-44
37. .M636-9-G4-45
j».M636-9b4TfiJ :
i5:M636-904EBl
^,M636-904EB1
61, M636-904TB2
51 M636-904EB2
63 M636-904FB2
6.M636^904TB3
:65:M636-904EB3
DATE
14Sep04:
l4Sep04
14Sep04
]4Sep04:
14SepD4
l4Sep04
i4Sep04 '•
14SepG4
14SepG4
:i4Sep04
]4Sep04
14Sep04
14Sep04
TYPE;
•X
X
X
.X
X
x:
X'
X
X
:x;
X
•:X?:
:X: .
LQGATION
M-636
M-636
M-636
M-636
'Mi636
M-636
M-636;:
M-636
M-636:
M-636:
M.636
M-636
M-636
TIME
15:48
10:45
11:17
14:40
15:21
m--^o}
10:41
10:41
\H:%0
11:12
11:12
\^:l>o
11:48
TEST
Pei-chlorate:
Perchlorate;
Perchlorate
Perehlorate
Perchlorale
Perchl Gi'ate
perchlorate
Perchl6i-ate
Perchlbrafe
Perchlorate
•
Perchlorate
Piirchl orate
Perchlorate
REMy\RKS
Soil
Soil
Soil
Soil
Soil
IA)-^^
(AA;?^
\A) rvi^y^
VJoJk^
[A) C^yt
w'/v^C-r
W Pj^\rr
VJ/C^
CHAIN OF CUSTODY
RELINQUISHED UY
^[fh^Hri(jfJL^
y 1
DATE
^Sm^
TIME
/^^D
ItECEIVEDBY
y{"u>Aic^
DAIE
^'^9-O'-r
TIME
{Ot>CJ
FOR LABORATORY USE ONLY
=n
DATECO.MPI.r:TED DATE RCrbRTi-D SIGNATURE
o^mo^ c^
ENVIRONMENTAL LAB WORK REQUEST
Oi THIOKOL ENVIRONMENTAL LABORATORY LWR No. E12435
Login No-
PROM:
JOHN HOLLADAY
ORGANIZATION:
ENVIRONMENTAL SERVIGEiS
EXTENSION:
6895
MAILSTOP:
301
COSTCENTER;
8200:
WORKORDER:
1B907
DATIl:
29 Sept 2004
REPORT RESULTS TO:
HELEN RAVSTEN.
SAMPLE INFORMATION
SAMPLE
66, M636-904FB3
67, M636.904TB4
6!iM636-904EB4
69. M636-904FB4
70, M636-9-04-4:6:
71, M636-9-04-47
n. M636-9-04-48
|3. M39-9-04-10
1^.
i>.
70
77;
7ii;
DATE
14Sep04:
l4Sep04.
14Sep04
14Sep04
14Sep04
I4Sep04
14Sep04'
14Sepp4
TYPE
j^
•
X
X
X
X
X
X
X
X
LOGATiON
M-636
M-636
M-636
M-63.6
M-63:6
M-636;
M-636
M-39.
TIME
11::48
i^r^o
13:15
13:15
10:50
11:26
15:08
09:50
TES:r
Perchlorate
Perchlorate
Pei-chloi*ate
Perchlorate
Ag, Cd, EPA601P, Perchlorate
Ag, Cd, EPA601d, Perchlorate
Ag, Gd, EPA60ld, Perchlorate
Ag, Cd, EPA6010, Perchlorate
lUiMAItJCS
WoMyt
\/Ji>M/%
U/'/i-fe
\A) G^:tui
Soil
Soil
Soil
Soil
CHAIN OF CUSTODY
RELINQUISilEIJlJY
lA~CMlJl.e.
'J ''
DATE
^1 S?pfOf
TIME:
it*>rc^
y^ ^ ^
ItECEIVEDBY
v/iA)&^^tm>
DATE
4?_^^..c?f
TIME
/^ ^C>
\
FOR LABORATORY USE ONLY
I ATE COMPLETED UATE REPORTED
ATK Thiokol, Inc. Results of M-39 and M-636 Sampling
Promontory, Utah October 2005
APPENDIX C
Results of Soil Gas Analyses
EarthFax Engineering, Inc.
;Beac6ni&ivir6qm6ntal ServiceS^^
": 353 Williams Str^t, Ste^ D :
Bel Air, MD 21014
Anfiiiysis bj' EPA Method 8260B (Modified)
Cliem Sample ID:
Project Nunibtr:
Lab File ID:
^ieceived DafcY
Analy.si.s Date:
Analysis Time:
Units:,
COMPOUNDS
1 1 r*\•• 1 * "-1—'—J-I l.i-Dichioroemene
ir<'ins-I.2-Dichloroethene •-,
l.I-DichJsDrpelhaijC'
ci.s-1,2-Dichloroelliene;
Chloroform
] ,2-Dichloroeihurje
I.IJ -Trichloroethane .
Carbon Tetrachloride
Trichlorotithene
1 ,L2-TricWoroethane
1,2-Dibromoethano (EDB)
Tetrachloroethene
CWorobenzenc
Bromoform
1,1,2,2-Teiraehli3roeShane
Clten.l 3simpl,e ID:
Project,Number:
:-:iy:-. -LabPileJC):
; y^ :: Received Dale:-
>^rialysis^Dale::
Analysis Time;
UniLs:
COMPOUNDS
1,1 -Dlchjorpethene
trans-1.2rDicHlorocihene
1 ;|^Dichlbroethaiie
cis-1,2-DiGhloroelliGne
Chlorqjferhr; :i
1.2-Dichloroethane'
],.]. 1 -Triclilprocthane
Cyrbon Tetrachloride
Tricliloroethene
l,:i:,2-Triqliibroethaiie
l,2^Dibr6hioethai1e OEDB)
:Tetraeli|prpelhene •'
Chlorobenzehe
Bromofonn
1.1.2,2-Tet:rach)oroeihuiie
MeiH_filk-
,EM[T,715
46iom'3
.' '
10/12/2004
13;11 •
ng/ti-ap
,
!- -,-• •;
-, - •-' <r'5' '.
• '..j.-<l5:,l
• k25( -
<2'5
<25
• <2S,';
<-25:,.-
-<25-;;
• <-2-5- ••
•<25- -
<25
<25-,
<25;
<2'5,
<2'5.
••.. M39:'04-
EML7,13.;'
•. 40;1012L9:-,
• lO/8/2pi34--l
10/1-2/2004 ••
21:17
ng/lrap.
<25 •
<25;:.
<25 •
<25 •
<25,
<25
<25
<25
<25
.•\^5.
.•••<25.
<25
•<25
<25
<25
• Trip,-1
EM 1715
40101214
\0m/2Q04
10/1,2/2004
18:42
ng/trap
•-
-'/• <25
• :'iO • •<25 ,
•'•f- •"<25
'<2-5
<25
<:25
-. • <25-
•f-''- ••<25-
<2-5-
<25
<25
<25
<25.
. <25
- .<25
. M39-.06
,. EM171-5
/:46ror220
-10/8/2004
10/12/2004
21:48
ng/trap
-<25
<25
<25
<25
•r-'S
<2.'i
<25
<25
<2.'i
<25
<25
'•';• <25
<25
<25
<25
M3'9-0'l
•EM1715
40J01215 •
10/8/2004
10/12/2004
19:13
ng/ti'iip
-<25.
•,.,'; • <25' ;
<25- •
<25
<25
<25
<25.
<25,
<25
<25
<25
<25
- <25
<25
<25
M39-07
EM] 715
• 40]p.i'22i •;
10/8/2004
. 10/12/2004
22:19
Tig/irap
<25
<25
<2.5
<25
<25
<25
<25
<25
<2.';
<25
<25
<25
<25
•.; <25
<25
' M39-,02
EM 1.715
,40101216
• 10/8/2004
10/12/2004
19:44
ng/trap
,',' 'M'^25
;:•-•:--^as'
• • ' '•<:25
<25
<25
..' <-25
^ ..", -<25-
f ;•' <25
'--,-<25
<25
<25
<25
<25
<25
<25
-. M39-08
• EM1715
•-'•'40101222
"LO/8/2004
10/12/2004
22:50
ng/trap
-<25
' ' <25
•<25
' <25
<25
<25
<25
<25
• •<25
. ••; . <25
,.;-*<25
• <25
<25
• •<25-
<25
M39-03
EM 1715
40101217
10/8/2004
10/12/2004
-20:15
ng/irap
<25
, <25
<25
<25
<25
<25
<25
<:25
<:25
<25
<-?')
<25
<25
<25
:.<25.
•M39-09
EM;i7'l5
4tlj:frt223
mmimi
10/12/2004
23:2.1
, ng/trap
<25
•• • <25
<25
.<25
.<25.
<25.'
.<25.
<25
. <25
..•••• :<25-
. ••<:25
<25.
.<25
•<?s
<25
M39-04
EMI715
40J01218
10/8/2004
10/12/2004
20:46
ng/trap
<25
<25
<25
<25
<25
<25
<25
<25
<2-5
<25
<25
<25
<25
<25
<25
M39-1G
EM:i:7i;5
-40)01224
10/8/2004
10/12/2004
23:51
ng/trap
. . <23
•-"<2y
<25
<23
<25
<25
<25
<25
<25
<23:
•<:25;
.<2>
<25
<25
<25
Results iii:it;iiiO!:runii (lig): J = Esiimated valuc-belbw repbrlud qiiamitaiion Icviil. B = petecied in inetiind bhmk. Pane 1 of .S
Beacon Environmental Services, Ihc»
323/Williams Street, Ste; D
Bel Air, MD 21014
Analysis by EPA Mefliod 8260B (Modified)
Cliept Sample iD:
Project Nuniber:
Lab File ID:
Received Dale:
: : -Analysis Dale:
Aii:alysis Tirae:
Unils:
COMPOUNDS
1,1-Dichloroetliene
trans-1,2-Dichloroeilicnc
l.l-Dichloroethane
cis-1,2-DJchlorpcthene
Chloroform
1,2-Dichloroetlian'e
1,1,1-TrichloroeUiane
Carbon Tetrachloride.
Trichloroelhene
1,1,2-TrichlGroethane
1,2-Dibromoelhane (EDB)
Tetrachloroothone
Chlorobenzene
Bromoform
1.1,2,2-TeirachlQroclhane
M39-i'l .
EM 1715
40101225
l0/8/2O(M
10/1-3/2004
0:22
ng/irap
<25
<25
<25
<25
<25
<25
<=25
<25 .
<25
<25
<25,
<25
<25
<25
<25
' '. FB-d]
BM1715
40101226
10/8/2004
10/1-3/2004
0:53
ng/trap
<25
<25
<>5
<25
<25
<25
•••.,• <^5
-.^. ' <25
<25
<25
• <25
<25
<25
, <25
<25
FB-()2
EM 1715
40101227 ^
10/8/2004
10/13/2004
1:24
ng/trap
<25 ,
<25
<25,
<25
<25„
•<25'
,, <25 •
<25
<25
<25
<25
<25 ,
<25
, <25
<25
FB-03
.EM1715
. 4t)10l22&
. 10/8/2004
10/13/2004
1:55
ng/trap
<25- ,
<25
•<25
<2-5
<25,
<25
<25
<25
<25-
<25
<25-
<25
<25
<25
<25
; FB-04
EM:I7I:5
40101229
10/8/2004
10/13/2004
2:26
ng/trap
•;<25-.
••;:^<25^:
. . •.• <25-
••" •^^•<25
<25
•'-•<25
. <25;
:•. •'';•:<25•
.• ••.r-<25'
. <25.
••-•' <25-
'.• -<25
- :^-<25
• : <23-
<25
'rrip-2
EMI 715
40101230
irJ/8/2004
10/13/2004
2:57
ng/trai>
<25
<25
•<25-
• <25
<25
<25
<25
<25
<25
<25
<25
<25^
<25
<25
<25
Results in nanograms (tig);, i:-;Esiimated value below reported quanlitatipii level. B - Detected iii meiliod blank. P;\\ic 2 oC .^
PHOTOGRAPHIC WASTE
OUTFALL (ABANDONED)
APPROXIMATE AREA
OF PREVIOUS EXCAVATION
BOUNDARY OF AREA
INVESTIGATED BY U.S.U.
GRID STARTING
POINT
SITE M-39 - "WET" AREA
SITE M-39 -"DRY" AREA
LEGEND
02 GRID NUMBER
(•) SOIL-GAS SAMPLE LOCATION
^^s EarthFax Engineering, Inc.
'^ "^' Engineers/Scientists
^|2^5^ Midvale, Utah
EdrthFdX www.earthfax.com
0' 5'
BASE MAP: DRAWING NO. M39VERI PROVIDED
BY ATK THIOKOL, INC,
DATE BY DATE BY
DRAWN BY: KHB
APPROVED BY: RBW
CHECKED BY: RBW DATE: MARCH 2005
DWG DATA: G:\UC020\THIOKOL PHOTO LABS\
PLATE 3-1,DWG
ATK THIOKOL, INC.
PROMONTORY, UTAH FACILITY
PLATE 3-1
M-39 SOIL SAMPLE LOCATIONS
\
,*•
\
APPROXIMATE EXTENT
PHOTOGRAPHIC WASTE
OUTFALL (ABANDONED)
BOUNDARY OF AREA
INVESTIGATED BY U,S,U
GRID STARTING
POINT
LEGEND
39 GRID NUMBER
GRID WHERE SILVER CONCENTRATION EXCEEDS
RESIDENTIAL PRG BUJ NOJ INDUSTRIAL PRG
(SEE TABLE 2-2)
^^5 EarthFax Engineering, Inc.
'^ "^' Engineers/Scientists
^^ Midvale, Utah
EsrthFdX www.earthfax.com
0' 10'
BASE MAP: DRAWING NO, M636VERI PROVIDED
BY ATK THIOKOL, INC,
Q;
DATE BY DATE BY
DRAWN BY: KHB
APPROVED BY: RBW
CHECKED BY: RBW DATE: MARCH 2005
DWG DATA: G:\UC020\THIOKOL PHOTO LABS\
PLATE 3-2,DWG
ATK THIOKOL, INC.
PROMONTORY, UTAH FACILITY
PLATE 3-2
M-636 SOIL SAMPLE LOCATIONS