DSHW-2003-004219 - 0901a0688013faf3

JOK
ALLIANT TECHSYSTEMS^
Aliiant Aerospace Company
P.O. Box 98
Magna, UT 84044-1
Tel [phone]
May 8,2003
Dennis R. Downs, Director
Department of Environmental Quality
Division of Solid and Hazardous Waste
288 North 1460 West
P.O. Box 144880
Salt Lake City, Utah
84114-4880
HAND DELIVERED
MAY I 3 2003
Utah Division of Solid
pnd Hozordni is Waste
RE: ATK Thiokol Propulsion QA/QC Split Sample Results
EPA ID # UTD001705029, Bacchus Works
Dear Mr. Downs,
The purpose of this letter is to report the analytical results on QA/QC spUt samples tiiat were prepared
on ApnJ 8, 2003 and submitted to the ATK Thiokol Promontory Laboratory for testing. The QA/QC
samples were prepared by Environmental Resource Associates of Colorado and submitted to the State
Laboraiory and the ATK Thiokol Promontory Laboratory under the direction of the Utah Division of
Solid and Hazardous Waste.
The table below contains the results from the ATK Thiokol Promontory Laboratory,
copies of the individual analysis reports are attached.
ATK Thiokol Promontory Results
Additionally,
Sample
Nimiber
Site 101
Site 102
Site 103
Site 104
Site 105
CL04*
(ppb)
<4
16
135
No Sample
No Sample
DCE*
(ppb)
No Sample
No Sample
No Sample
4.4J
105
DCA*
(ppb)
No Sample
No Sample
No Sample
4.9J
99
Freon 113
(ppb)
No Sample
No Sample
No Sample
51
427
TCA*
(ppb)
No Sample
No Sample
No Sample
<5
101
TCE*
(ppb)
No Sample
No Sample
No Sample
93
4.6J
*CL04: Perchlorate, DCE: 1,1-Dichloroethene, DCA: l,2-Dicliloroethane,TCA: 1,1,1-Trichloroethane,
TCE: Trichloroethene
If you have any questions or need additional information conceming this issue, please contact
Allen Lee at 251-5688.
Sincerely,
^
Paul Hancock, Manager
Environmental Remediation
PJM\ABL
CERTIFICATE OF ANALYSIS
Listing of sampie information and Testing Requested
Friday, April 25, 2003
TESTED FOR ATK Thiokol: Bacchus
Environmental Compliance M/S M7H7
P. O. Box 98
Magna, UT 84044-0098
Alien Lee
Project: Lab Anal - Rem - Groundwater
Login Number L6496
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-3732
800-863-8080
Lab No Client Number
Test Requested
1 L6496-1 SITE 101
EPA 314.0
L6496-2 SITE 102
EPA 314.0
1 L6496-3 SITE 103
Description
MAGNA
Perchlorate - lon Chromatography
MAGNA
Perchlorate - lon Chromatography
MAGNA
Received CollectDate/Time
Matrix
04/10/03 04/08/0310:00 1
Water
04/10/03 04/08/03 10:15
Water
04/10/03 04/08/03 11:00
EPA 314.0 Perchlorate - lon Chromatography Water
Certified ified By ^o-^^
Date QC Coordinator
This certifies tliat the following samples were analyzed using good laboratory practices to show the following results:
Page 1 of 3
[
Listing of Results by Sample
SamplelD: SITE 101 MAGNA Lab ID: L6496-1 Collect Date: 04/08/03 10:00
Test Parameter
PERCHLORATE
I Sample ID: SITE 102
Dil.
Result Units MDL EQL Factor Method Analyst Test Date
U ug/l 1 4 1 EPA 314.0 CWS 04/18/03 14:31
MAGNA Lab ID: L6496-2 Collect Date: 04/08/03 10:15
Test Parameter
PERCHLORATE
G
DII.
Result Units MDL EQL Factor Method Analyst Test Date
16 ug/l 1 4 1 EPA 3140 CWS 04/18/0314:43
SamplelD: SITE 103 MAGNA Lab ID: L64g6-3 Collect Date: 04/08/03 11:00
Twt Parsmeter
PERCHLORATE
DII.
Result Units MBL EQL Factor Method Analyst Test Date
135 ug/l 1 4 1 EPA 3140 CWS 04/18/0314:56
Page 2of3
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected
but was below the EQL (Estimated Quantification Limit). The EQL and the RPL (Reporting
Limit) are used in the same manner for this report.
MDL Method Detection Limit: The minimum concentration of a substance that can be confidently
measured and reported. The laboratory has demonstrated that the MDL can be achieved in a
laboratory reagent blank, but does not guarentee it can be achieved in all sample matrices.
The MDL is approximately three times the signal noise level.
EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many
analytes the EQL is selected as the value of the lowest standard in the calibration curve.
Dil. Factor Dilution Factor: The prepared smple was diluted by this factor because the sample was too
concentrated or due to other interferences in the sample matrix. Any dilution factor causes
an appropriate increase in the MDL and EQL.
Page Sof 3
CHAIN OF CUSTODY
ALLIANT TECHSYSTEMS, P.O. BOX 98 MAGNA, UTAH 84404
Collected by: Allen Lee Proiect: Off-sJc [judis.
Contact: Allen Lee CollecUon Location: &ll^tO<^
Telephone: [phone] WorkOrder: 1B391 98BP-1
Turn Around Time:
X'A /^/
.^;/tf /^2.
C/c /oZ
.C/^ /^>Y
<:/<=, /^^^
:;||||iii!i;|||i;;:
/47K'T»iiofcJ
/4rf; ik^JH^l
/4rfc iho^
l4TKlhi^l
i^lKlUiok^)
^Iiiiiiiiiiiii
9l^jfr\lol
B i^^ihi
^iAff\\ol
P^\Af^\\oh
8^^\lol
liSiiili^
iiisiii^i: \o\oO
lO'Ab
//:O0
IWlS'
n:iO
;;l::-?i^itj^ig|;;::|;||
/
/
/
J
3
iiielii'illiiiil-iiiipililil^
••K^iv.;IO:My:s:riii^I;:i.;.y.i:;:i
lipiiBliilSBiSiiiiiis^
ifiiPiiiiiiiiiia^^^^^^^^ wsBm^immKmMmm&
IS§mm&f^BmiMiM0^
:-. •.: • : ::!:.:::::.:.:.:•:.:::.:•::::::•:•;•; :••:..: •':•:... . :::;:::::;:::::,:::::: :•:•:::•:•.';,; ::•;::: :•:•. :•: . :•,;..:.:,!.:\\\\\\\\\\\-:: • •
;>:::•:;;;';::^:;::';:::ii:i-::i :\y;^\:';;::;•;;;•:;:i;:':::';'.:;:;'.:;:.:!;.:j-j^"V[':['•• .'..y::;:;.::;::.:•;•;•;: ;x i/:
y^.-:':.y.::':":i:;;'••••:• ••^-^y.-Vy^:^'':'.;•'::':'::'• • ••••••!•::'•'•:•:•:y^:•:'.:-'::':::::'••:'!!:!:•::::•::•''.:!::'-•::•::::•:••:••:!!!':.!V';:!.:! ••:••• •W.^.V.'•'.".'.': .
-i ^
//)Afi'im\*jk by/y
l^i(XA£HI 0(
1
Received by.
^/z^zf.^^
Dale/Time
i/'/l?'i;-S A/./£?
CERTIFICATE OF ANALYSIS
Listing of sample Information and Testing Requested
Thursday, April 24, 2003
TESTED FOR ATK Thiokol: Bacchus
Environmental Compliance M/S M7H7
P. O. Box 98
Magna, UT 84044-0098
Allen Lee
Project: Lab Anal - Rem - Groundwater
Login Number L6497
Lab No Client Number
Test Requested Description
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-3732
800-863-8080
Received CollectDate/Time
Matrix
IL6497-1 SITE 104
SW-846, 8260
1 L6497-2 SITE 105
MAGNA
Volatile Organics Appendix 9
MAGNA
04/10/03
04/10/03
04/08/03 11:15
Water
04/08/03 11.30 1
SW-846, 6260 Volatile Organics Appendix 9
Certified I tified BvVJv^
Water
QC Coordinator I (\ Date
This certifies that the following samples were analyzed using good laboratory practices to show the following results:
-22-Af R-?.C)0^
Page 1 of 6
Listing of Results by Sample
1 Sample ID: SITE 104 MAGNA
CAS
Number
630-20.6
71-55-6
79-34-S
79-00-5
75-34-3
75-3S-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
71-36-3
590-20-7
78-93-3
110-75-8
95-49-8
591-78-6
78-83-1
79-46-9
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
107-05-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
126-99-8
156-59-4
10061-01-5
108-94-1
124-48-1
74-95-3
75-71-8
141-78-6
60-29-7
97-63-2
100-41-4
76-13-1
87-68-3
67-63-0
98-82-8
1330-20-7
126-98-7
74-88-4
80-62-6
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
107-12-0
110-86-1
135-98-8
100-42-5
Twt Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1.1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1.2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
1-BUTANOL
2,2-DICHLOflOPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
2-METHYL-1-PR0PAN0L
2-NITROPROPANE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
ALLYL CHLORIDE
BENZENE
BR0M0BEN7FNE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CHLOROPRENE
CIS-1.2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
CYCLOHEXANONE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYL ACETATE
ETHYL ETHER
ETHYL METHACRYLATE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYL ALCOHOL
ISOPROPYLBENZENE
M.P-XYLENE
METHACRYLONITRILE
METHYL IODIDE
METHYL METHACRYLATE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
PROPIONITRILE
PYRIDINE
SEC-BUTYLBENZENE
STYRENE
Result
U
u u
u u 44J
U
U
U
u
u u
u u 4.9J
u U
U
U
U
U
U
u u u u u
u u u u u u u u u u
u u
u u
u u u
u u
u u u u
u u u u u
u u u 51
u u u u
u u
u u u u u u
u u
u u
Units
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ugf)
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
Lab ID: L6497-1 Collect Date: 04/08/03 11:15 |
MDL
.3
.2
.9
.3
.5
.2
.2
.2
.3
.5
.2
.4
.2
.3
.3
.2
.3
.2
.2
.1
5.2
.9
1.1
1.7
.2
.7
5.3
.99
.2
.2
.5
1.1
47
.9
.5
.2
.4
.3
.2
.4
.6
.1
.3
.2
.4
.3
.8
.9
.2
.4
1.6
.2
.3
.7
.6
.2
.2
.2
.2
.6
3
.2
.3
.4
.2
.5
.8
.3
.2
.3
.2
.4
25
.2
.2
Oil.
£QL Fac
5
5
5 1
5
5
5
10 1
10 1
5
10 1
10
10
5
10 1
5 1
5
10
10 1
10
10
52 1
10
100 1
17 1
10 1
50 1
53 1
9.9 1
10 1
10 1
50 1
100 1
5 1
5 1
100 1
5 1
10 1
10 1
5 1
5 1
10 1
5 1
5 1
5 1
10 1
5 1
10 1
5 1
10 1
5 1
16 1
5 1
5 1
5 1
6.3 1
2 1
5 1
5 1
1.5 1
10 1
30 1
10 1
5 1
5 1
5 1
5 1
10 1
10 1
10 1
10 1
5 1
5 1
249 1
10 1
5 1
tor Method
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-84e, 8260
SW-846. 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
Page
Test Date
04/16/0315:18
04/16/0315:18
04/16/03 15:18
04/16«)3 15:18
04/16/0315:18
04/16/03 15:18
04/16/0315:18
04/16/0315:18
04/16/0315:18
04/16/0315:18
04/16/0315:18
04/16/0315:18
04/15/0315:18
04/16/0315:18
04/16/03 15:18
04/16/0315:18
04/16/03 15:18
04/16/0315:18
04/16/0315:18
04/16/0315:18
04/16/0315:18
04/16/0315:18
04/16/0315:18
04/16/0315:18
04/16rt)3 15:18
04/16/03 15:18
04/16A33 15:18
04/16/03 15:18
04^16/0315:18
04/16/0315:18
04/16/0315:18
04/16/0315:18
04/16/0315:18
04/16/0315:18
04/16rt53 15:18
04/16/0315:18
04/16W3 15:18
04/16/0315:18
04/1 &03 15:18
04/16/0315:18
04^16/0315:18
04/16/0315:18
04/16/03 15:18
04/16rt)3 15:18
04/16/0315:18
04/16rt)3 15:18
04/16/0315:18
04/16rt)3 15:18
04/16/0315:18
04^16A33 15:18
04/16/0315:18
04/16/0315:18
04/16/0315:18
04/16'03 15:18
04/16/0315:18
04/16rt)3 15:18
04/16/0315:18
04AiaO3 15:18
04/16/0315:18
04/16/0315:18
04/16«)3 15:18
04/16/0315:18
04/16/0315:18
04/1 SrtO 15:18
04/18/0315:18
04/16rt)3 15:18
04/16/0315:18
04/16AD3 15:18
04/16/03 15:18
04/16/0315:18
04/16/0315:18
04/16/0315:18
04/16/0315:18
04/16/0315:18
04/16/0315:18
2of6
98-06-6 TERT-BUTYLBENZENE
127-18-4 TETRACHLOROETHENE
108-88-3 TOLUENE
156-W-5 TRANS-1.2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
110-57-6 TRANS-1,4-DICHLORO-2-BUTEN
79-01-6 TRICHLOROETHENE
75-69-4 TRICHLOROFLUOROMETHANE
108-05-4 VINYL ACETATE
75-01-4 VINYL CHLORIDE
u
u u u u
u 93
U
U
U
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
.2
.3
.2
.3
.2
.7
.7
.3
1.3
.3
10
5
5
5
5
10
5
5
5
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-a46. 8260
SW-846, 8260
SW-846, 8260
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
04/16/0315:18
04/16/0315:18
04/16/0315:18
04/ieW)3 15:18
04/16/0315:18
04/16/0315:18
04/16/0315:18
04/16/0315:18
04/16*315:18
04/16/0315:18
Page 3of 6
1 Sample ID: SITE 105 MAGNA
CAS
Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
71-36-3
590-20-7
78-93-3
110-75-8
95-49-8
591-78-6
78-83-1
79-46-9
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
107-05-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
126-99-8
156-59-4
10061-01-5
108-94-1
124-48-1
74-95-3
75-71-8
141-78-6
60-29-7
97-63-2
100-41-4
76-13-1
87-68-3
67-63-0
98-82-8
1330-20-7
126-98-7
74-88-4
80^2-6
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
107-12-0
110-86-1
135-98-8
100-42-5
98-06-6
127-18-4
Ifist Psrsmetfic
1.1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1.1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1.2,3-TRICHLOROBENZENE
1.2.3-TRICHLOROPROPANE
1.2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1.2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1.3.5-TRIMETHYLBEN2ENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
1-BUTANOL
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
2-METHYL-1-PROPANOL
2-NITROPROPANE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTAN0NE
ACETONE
ACROLEIN
ACRYLONITRILE
ALLYL CHLORIDE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CHLOROPRENE
CIS-1.2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
CYCLOHEXANONE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYL ACETATE
ETHYL ETHER
ETHYL METHACRYLATE
ETHYLBENZENE
FREON 113
HEXACHLOROBUTADIENE
ISOPROPYL ALCOHOL
ISOPROPYLBENZENE
M.P-XYLENE
METHACRYLONITRILE
METHYL IODIDE
METHYL METHACRYLATE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
PROPIONITRILE
PYRIDINE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
Result
u
101
u u
u 105
U
U
U
u
u u u
u 99
U
U
u u u u u
u u u u u u u
u u u u u
u u u u u
u u u u u u u
u u u u u
u u u u u
u u 427
u u
u u
u u u
u u u u u
u u
u u u u
Unit§.
ugfl-
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/I
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
LablD:L6497-2 Collect Date: 04/08/03 11:30 |
MDU
.3
.2
.9
.3
.5
.2
.2
.2
.3
.5
.2
.4
.2
.3
.3
.2
.3
.2
.2
.1
5.2
.9
1.1
1.7
.2
.7
5.3
.99
.2
.2
.5
1.1
47
.9
.5
.2
.4
.3
.2
.4
.6
.1
.3
.2
.4
.3
.8
.9
.2
.4
1.6
.2
.3
.7
.6
.2
.2
.2
.6
.6
3
.2
.3
.4
.2
.5
.8
.3
.2
.3
.2
.4
25
.2
.2
.2
.3
DII.
iOk Fac
5
5
5 1
5
5
5 1
10
10
5
10
10
10 1
5 1
10 1
5 1
5 1
10 1
10
10 1
10 1
52
10 1
100 1
17
10 1
50 1
53 1
9.9 1
10 1
10 1
50 1
100 1
5 1
5 1
100 1
5 1
10 1
10 1
5 1
5 1
10 1
5 1
5 1
5 1
10 1
5 1
10 1
5 1
10 1
5 1
16 1
5 1
5 1
5 1
6.3 1
2 1
5 1
5 1
6 4
10 1
30 1
10 1
5 1
5 1
5 1
5 1
10 1
10 1
10 1
10 1
5 1
5 1
249 1
10 1
5 1
10 1
5 1
tor Method
SW-846. 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846. 8260
SW-846. 8260
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
Page
IS5tDat£
04/16rt33 16:37
04/16W3 16:37
04/16/0316:37
04/16/0316:37
04/16/0316:37
04/16/0316:37
04/16/0316:37
04/16/0316:37
04/16/0316:37
04/16/0316:37
04/16/03 16:37
04/16/03 16:37
04/16/0316:37
04/16/0316:37
04/16/03 16:37
04/16/0316:37
04/16/0316:37
04/16/0316:37
04/16/03 16:37
04/16/03 16:37
04/16/0316:37
04/16/0316:37
04/16/0316:37
04/16/03 16:37
04/16/0316:37
04/16/03 16:37
04/15rt)3 16:37
04/16/03 16:37
04/16/0316:37
04/16A)3 16:37
04/16«)3 16:37
04/15/0316:37
04/16/0316:37
04/16/0316:37
04/16/0316:37
04/16/0316:37
04/16/0316:37
04/16A)3 16:37
04/16/0316:37
04/16/0316:37
04/16/0316:37
04/16/0316:37
04/16/03 16:37
04/16/03 16:37
04/16A)3 16:37
04/16/0316:37
04/1 a«3 16.37
04/16/0316:37
04/16«)3 16:37
04/16/0316:37
04/16/03 16:37
04/16rt)3 16:37
04/16A)3 16:37
04/16/0316:37
04/16rt33 16:37
04/16/0316:37
04^1 &03 16:37
04/16/0316:37
04/16fl53 15:57
04/16/03 16:37
04/16^)316:37
04/16«)3 16:37
04/16/0316:37
04/16«)3 16:37
04/16/0316:37
04/16/0316:37
04/16/0316:37
04/16/0316:37
04/16rt)3 16:37
04/16/0316:37
04/16/0316:37
04/16/0316:37
04/16/0316:37
04/16/0316:37
04/16/0316:37
04/16rt33 16:37
04/16/0316:37
4of6
108-88-3
156-60-5
10061-02-6
110-57-6
79-01-6
75-69-4
108-05-4
7501-4
TOLUENE
TR/U^S-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRANS-1,4-DICHLORO-2-BUTEN
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
U
u u u 4.6J
u U
U
ug/l:
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
.2
.3
.2
.7
.7
.3
1.3
.3
5
5
5
10
5
5
5
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
04/16/0316:37
04/16/0316:37
04/16/03 16.37
04/16/0316:37
04/16A)3 16:37
04/16/0316:37
04/16/0316:37
04/16/03 16:37
Page 5 of 6
Data Reporting Qualifiers
U Indicates compound was analyzed for and was; not detected, or the compound was detected but was
below the MDL.
B Gas Chromatography and Mass Spectral Data Flag. This flag is used when an analyte is found in
the blank as well as the sample
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This flag is used
either when estimating a concentration for tentatively identified compounds or when the data
indicated the presence of a compound that meets the identification criteria but the result is less than
the EQL (e.g. 3 J with an EQL of 10)
MDL Method Detection Limit: The minimum concentration of a substance that can be confidently
measured and reported. The laboratory has demonstrated that the MDL can be achieved in a
laboratory reagent blank, but does not guarentee it can be achieved in all sample matrices.
The MDL is approximately three times the signal noise level.
EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many
analytes the EQL is selected as the value of the lowest standard in the calibration curve.
Dil. Factor Dilution Factor: The prepared sample was diluted by this factor because the sample was
too concentrated or due to other interferences in the sample matrix. Any dilution factor
causes an appropriate increase in the MDL and EQL.
Page 6of6
CHAIN OF CUSTODY
ALLIANT TECHSYSTEMS, P.O. BOX 98 MAGNA, UTAH 84404
CoUected by: Allen Lee Project: Off'S,-/^, Ivcjl^
Contact: Allen Lee Collection Location: /H/^tO 1^
Telephone: [phone] WorkOrder: 1B391 98BP-1
Turn Around Time:.
^;h /^/
^:-fc /^2.
C/c /^3
.c/^ /^¥
c-4, /t^iS'
/47T<'ni^
/4m Kiiofo/
/4TK VuoKki
^TKTMi=>l
i^TKTUcI^)
iiiiliiiil
WmSSS
^l^nlol
/3 i^ilol
^lAfr\\ol
^\Afr\lo^
8^(Y\lol
:||;f|liiiii;i-
\D\00
10'lb
//:00
ii: /i'
//.•iO
|:|||pMii|tiy.|
•:::;Pf#i:;iS::n-:
/
/
/
^
3
|:i||.;ii:;iti|;:;.;.j^
xfmiB> i^mm
m^^^BiUB^SmBmKi
mKBBSBBlSli^ml^
l^iBi^iiiiiiiililH^^
mSmms8mmmmsmmls^mU
§Mitm :ii^Mki$Mi§m^iMMSM^
:::y:\r:-^y-:.::y.y-y:::\::'-'-^ • ••• ;:--::';'^:":":o.::.: :.:.:i:.:i::i::-:':-.-:-i-:-io:o:::::::::::::":':;::': v:^:A:\:y<y:^^-:: y'::::^.-:::^:: yyy\y\ , .
•••:•••;; ;•;:•;:; ;:;•; ;;;;•;;;;!•••::: ;•.•:;•::•::•;; i ;•;.:•;•;:::;•;:•; ;•:•:•:•:•;•:•;:;•:: ;:;:;:;x:.; ;•; ;•; y\y: ••:•:•::•:;:; ^m^^^ ••;;:•::::: :•:::;•;•;•;:::;:;:;:::;.:;.;;;;-;; i \-- ::::•:;;;;; ;•:.:;•:
;.;-i;-;-; ;••••;•;•;•;•:;;;;J;-;;:; •;•;•;•;i:i;;!;•;;i;;;;i;;;;;;• ;;;.v-i;;;:;:;•;;•;•;•;;:;;;•;;•!:•;;IJJB^^^ ;;:.;;•;;;;•; •;:?:i;;i;;y
^f KV; •:•::•:•:::•:•. •:•.•.• •.•^.' '••!:::::•••:• •iiii':-:'. '•. •!;•;•;;;;;; ;•.••; ••;.;:;;?;•;•;;•; i ;•; ;;;;:;• •;; J ••:;:••;;;•:;!;•;: ;.;BH: " v^.: ••••••; •.•; ;•;; ;•;•;;;.;;.;; :;•• ;iSB.v.: :•;•;;;:;;:
:;|:i??:!i-.;y?::!.;;l||:.;;;:^
• •:,:•;:;':;';•;.:•:;:•: ,: •••:;• •:'::•.:::::':.;•;:':• • •.•::•::::•:::::::::,.•.•:•::•.•.•:•:•.:•:•:::::':::':::::'.:':::::':::•:•:•::• :•:;:•;..,:;: •.::::::.; •
!•::•: :!••:•:•:•:••:::':;; ::.!;!•!• :•;•••••: WiSmimmSmMu^
:: •! ::;:;i:-;;: i-'-^ii • ••••••••;:;:;•; H?;^:-;;;;:: ;••;:•; :•:•::••;•••;;;!:; ;^^ ;•;•; :.v;.::: ;••••:••••;; ;•;•::;:::; ;''^^.- '• '• ^^-^ !•; r^^-^; ^^^- ^-^y] '•• • • •:.::::: y\\.\ '.'.'.••.
"^^M S W- '• WS M i- WM ^ '^ ^y M W!^ W ^^^^ M;;; M ^ \ W ^^^: i '^-MM E'. i-;:
7 '? 1 /j/JUuism h^jj
0UJPi a
Received by:
'l^'/tJ E^CtC^
Date/Time |
i/'/(;'i^-s u/;/(p 1