DSHW-2002-004247 - 0901a0688013dd96

ATK
ALUANT TECHSYSTEMS
12 September 2002
8200-CY03:ST070
Mr. Deimis R. Downs, Executive Secretary
State ofUtah
Department of Environmental Quality
Division of Solid and Hazardous Waste
288 N. 1460 W.
P.O. Box 144880
SaU Lake City, Utah 84114-4880
Dear Mr. Downs
ATTENTION: Jeff Vandell
Thiokol Propulsion Corp.
P.O. Box 707
Brigham City, UT 84302-0707
Tel [phone]
Fax [phone]
rtEi i^Eb
SEP 1 7 2002
lOA of Solid & Hazardous
h nenartmpnt nf FnvlrnnmenMI Ouali'
Division df SoUd i Hazardous Waste
Subject: Semi-Aimual RFI Progress Report
As required by Section VIIH of Thiokol Corporation's Post Closure Permit, the following semi-
aimual RFI progress report is submitted for your review. The reporting period covered by this
report is 1 March 2002 -1 September2002.
Included is a work plan for passive soil gas survey for three SWMUs 625, 202, and 551.
Ifyou have any questions regarding this report, please direct them to Paul Hancock at (435) 863-
3344.
Sincerely
Susan Jew, ^Director
Environmental Services
c: Don Ostler, Director, Division of Water Quahty
SEMI-ANNUAL RFI PROGRESS REPORT
1 March 2002 -1 September 2002
1. Description and estimation of tlie percentage of the RCRA Facilities
Investigation completed;
Three potential Solid Waste Management Units within the T-75 facility were
investigated. These are old test holes where thermal safety studies were
conducted approximately 20-25 years ago. The holes were approximately 2- 3
feet in diameter and one foot deep. To the best of our knowledge only one test
was conducted at the three sites using a then new potential oxidizer hydrazinium
diperchlorate. Due to the instability ofthe material, gradual increases in
temperature were tested. One ofthe tests detonated therefore fiirther tests were
cancelled and the material and equipment were removed fi-om all sites. It was not
believed that any waste was left or any hazardous constituents remained. To
confirm this information the three test holes were sampled for constituents of
concem, volatile organics, explosive constituents, and total metals. Prior to
sampling, small shaped charges of pentalite were used to fire the holes to assure
safety with minimal displacement ofthe soil. No indications of an additional
energetic release were seen.
2. Summaries of all findings;
The raw analytical data from all sampling activities during the reporting period
for T-75 are included as an attachment. No hazardous constituents were detected
above backgroimd levels with detection limits far below any risk-based levels.
Thiokol believes that this confirms the indication that they would not be Solid
Waste Management Units.
3. Summaries ofall changes made in the RCRA Facility Investigation during
the reporting period;
Additional investigations of three solid waste management units #625, 202, and
551 using passive soil gas surveys are proposed. The purpose ofthe survey is to
determine that sources of groundwater contamination plumes. The Work Plan is
included with this report. Thiokol requests approval ofthe Work Plan so that
work can commence prior to freezing weather.
4. Summaries of all contact with representatives of the local community, public
interest groups or State Government during the reporting period:
Correspondence regarding RFI activities has been limited to the Division of Solid
and Hazardous Waste, the Division of Water quality, the U.S. Fish and Wildlife
and the Department of Natural Resources.
5. Summaries of aii problems or potential problems encountered during the
reporting period;
There were no significant problems encoimtered during the reporting period.
6. Actions taken to rectify problems
Thiokol continues to review all available information and pursue all avenues
to resolve any uncertainty associated with the solid waste management imits.
Changes in personnel during the reporting period;
There were no persormel changes. The existing environmental staff will
continue to conduct the sampling when possible. Contractors will be used
when specialized equipment is required.
Projected work for the next reporting period;
Efforts for the next reporting period will focus on investigating additional
solid waste management units, primarily the passive soil gas survey and report
preparation for these projects.
9. Copies of daily reports, inspection reports, laboratory and monitoring
data.
The raw analytical data and field notes from all sampling activities are
included as an attachment.
Additional
Investigation of SWMUs #625, 202, 551
Passive Soil Gas Survey
Work Plan
September 2002
ATK Thiokol Propulsion
RFI Work Plans
September 2002
1.0 SAMPLING OBJECTIVE
Passive soil gas vapor sampling using passive soil gas modules are to be used to provide
indications of sources of groundwater contamination potentially from old Solid Waste
Management sites. These units have demonstrated effectiveness at other locations for
determining subsurface areas impacted by VOCs and old disposal areas.
2.0 SITE LOCATIONS
The passive soil gas samplers will be used at three SoHd Waste Management Units. These
units are suspected of being contamination sources for VOCs currently found in the ground water
at Thiokol.
. i't^ -: l- 'i^^ -""'^•^ v]/' 7 :M' ^
625
202
551
Old Septic Tank drain fields A, B, and C, located across
fi-om the Space administration area. These units were
sample previously as part ofthe RFI. Results indicated
that no hazardous substances were above background or
risk based levels.
Old propellant buming ground at Plant III. This site was
sampled previously as part if the RFI. No contamination
above background levels was found. Recommendation of
no fiirther action.
Old drum storage area at building M-l87 This site was
sampled previously as part ofthe RFI. Results showed
trace amounts of two solvents, but far below risk based
levels. Recommendation of no further action.
3.0 BACKGROUND INFORMATION
Previous soil sampling at the three Solid Waste Management Units 622, 551, 202 have
not indicated any significant contamination. A copy ofthe RFI for each of these units is
attached in Appendix A. However, groundwater contamination pattems indicate that the
source ofthe contamination may be from previous disposal practices at these sites.
Thiokol is seeking to identify the sources ofthe groundwater contamination plume at
these locations with the use of passive soil gas modules.
ATK Thiokol Propulsion
RFI Work Plans
September 2002
3.1 Module Description
A typical passive soil gas module consists of several passive sorbent collection devises
(sorbers). A typical sorber is 15 to 25 millimeters (mm) long, with a 3 mm inside
diameter (ID), and contains 40 milligrams (mg) of a granular adsorbent material.
Adsorbents used are typically polymeric and carbonaceous resins chosen for their affinity
for a broad range of VOCs and SVOCs with minimal uptake of water vapor. The units
have a retrieval cord which is fashioned with a loop. Both the rettieval cord and sorbant
container are constructed solely ofa chemically inert, hydrophobic, microporous
membrane (expanded polytetrafluoroethylene, ePTFE). The loop is used as a means of
tying the module to a string for installation and retrieval. Attachment 1 shows a typical
module.
VOC and SVOC vapors penetrate the module freely and collect on the adsorbent
material.
3.2 Use and Limitations of Data
Data from the Passive soil gas modules generally are intended to indicate potential site
contamination. Data from the passive soil gas modules are of definitive quahty. They are
considered to provide definitive evidence ofthe presence or absence of contamination.
Passive soil gas module data identify soil gas mass levels present in the vapor phase.
Vapors are subject to a variety of attenuation factors during migration away from the
source and concentration in the module. Thus, mass levels reported from the module will
often be less than concenfrations reported in soil and groundwater matrix data. (Passive
soil gas module data are not reported in concentration units: they are reported in mass
units.) The long time frame for Passive soil gas module sampling should allow an
equilibrium measurement of soil gas concentrations and provides fiilly acceptable
sensitivity based upon EPA demonsfration project results. In most instances, the Passive
soil gas module soil gas masses reported on the modules correlate favorably with
concentrations reported in the soil, active soil gas or groundwater (e.g., where soil gas
levels are reported at greater levels relative to other sampled locations on the site, matrix
data should reveal the same pattem, and vice versa). However, due to a variety of factors,
a perfect comparison between matrix data and soil gas levels can rarely be achieved.
Soil gas signals reported by this method cannot be directly attributed to soil-adsorbed,
groundwater, and/or free-product contamination. The soil gas signal reported from each
module can evolve from all of these sources. Differentiation between soil and
groundwater contamination can only be achieved with prior knowledge of the site history
(i.e., the site is known to have groundwater contamination only).
ATK Thiokol Propulsion
RFI Work Plans
September 2002
4.0 SAMPLING STRATEGY
4.1 Sampling Protocol
Approximately 100 samples will be collected using Passive soil gas module cartridges.
48 will be collected at the old drain fields (SWMU 625), 25 at the old propellant bum
ground (SWMU 202) and 24 at the old dmm storage area (SWMU 551). Grids will be
measured and each site and passive soil gas module cartridges will be installed at each
grid intersect. Drawings ofthe sites with the grid layout are in Attachment 2.
The sorber module consists of a porous tube, which is sealed at one end. Contained in
the tube is the granular sorbent with a unique identification tag for each sample. The
sorber module will be placed at the locations described above to a depth of not less than 2
feet using the procedures described in section 6 . The module will remain in place
approximately 2 weeks , allowing sufficient time for potential contaminants to diffuse
into the sorbent material. Modules are then collected by field personnel, put into
specially prepared impermeable containers and shipped under strict chain of custody to
the laboratory. The analysis ofthe modules requires the technology ofthe associated
laboratory for the best results. The list of analytes is a modified short list of SW-846
Method 8260 volatile compounds.
4.2 QA/QC Samples / Data Quality Objectives
The current laboratory limits are presence or absence of the compounds rather than a
defined limit (see section 8 ofthis document for those laboratory limits). Approximately
5% field duplicates will be collected for the Passive soil gas module sampling. The
Passive soil gas module field duplicates will be collected simultaneous with the original
sample. Passive soil gas module duplicates are inherent in the module set-up. Two
sorbers are contained in each module or two single modules will be placed in the same
bore hole. The field personnel will designate the samples to be used as the field duplicate
pair so that second analysis will be performed. Duplicate precision is independent ofthe
bias (accuracy) ofthe analyses and reflects only the degree to which the measurements
agree with one another, not the degree to which they agree with the "true" value ofthe
parameter measured. The precision ofthe Passive soil gas module analysis will be
determined from the modules matrix duplicates. The data validation will use less than
50% RPD limit expressed as follows:
Where:
RPD = relative
Xl, X2 = value of
X,-X2
RPD = (100%)
(X!+X2)/2 percent diflference
sample 1 and sample 2
Approximately 5% trip blanks will be collected for the Passive soil gas module soil gas
samphng. This corresponds to an uninstalled module taken to the field but not placed in
the soil.
ATK Thiokol Propulsion
RFI Work Plans
September 2002
For the Passive soil gas module, frip blank modules will be provided to document
potential exposures that were not part ofthe soil gas signal of interest (i.e., impact during
modules shipment, installation and retrieval, and storage). The trip blanks are identically
manufactured and packaged soil gas modules to those modules placed in the subsurface.
However, the trip blanks remain unopened during all phases ofthe soil gas survey.
Levels reported on the trip blanks may indicate potential impact to modules other than the
contaminant source of interest.
Due to the nature ofthe soil gas modules to be collected, analysis of MSs and MSDs is
not possible for this project. The current laboratory limits are presence or absence ofthe
compounds rather than a defined limit. The results ofthe blank analysis will help to
define accuracy under these limits.
4.3 Background Samples
Three background samples will be collected in areas known or believed to be free of
contamination within the Manufacturing and Administration Area for use in comparing
concentrations
Extensive soil sampling ofthe Thiokol facility has established a data base for naturally
occurring organic constituents. This data base consists of background samples used in
the closure of various RCRA facilities at Thiokol.
5.0 LIST OF FIELD EQUIPMENT
The following table lists all parts and equipment that will be used for this investigation:
Description
Shipping boxes containing individually
numbered passive soil gas collectors
(Modules), including trip blanks
Stainless steel insertion rod, in threaded
sections (for placement of modules in pre-
drilled/driven pilot holes)
Corks with screw eyes attached
Chain of Custody and Installation/Retrieval
Log
Equipment to lay out and mark sample
locations (scaled map, measuring tapes, pin
flags, spray paint)
Disposable gloves and equipment
decontamination supplies
"Little Beaver" gas powered sampling auger
2-inch diameter stem up to 36 inches long
extensions
Tamper-evident seals
Packing Tape
ATK Thiokol Propulsion
RFI Work Plans
September 2002
6.0 MODULE INSTALLATION TECHNIQUE
Passive soil gas module modules will be installed according to the manufacturers specifications
given below. All ofthe Passive soil gas module modules will be installed to not less than 2 feet
sampling depth and left in place for two weeks or as recommended by the manufacturer prior to
module retrieval.
Passive soil gas module installation protocol is given below:
• Always obtain utility clearance before digging or probing.
• It is not recommend installation of modules be within 15 feet of monitoring wells, utility
trenches or other conduits, which may act as a preferential pathway for soil vapor migration.
• Drive/drill narrow pilot hole at desired pre-market location
• Wearing clean gloves, remove module from numbered container and re-seal the jar (this
numbered container should correspond to the numbered module ID tag-please verify this)
• Measure and cut a section of cord that is suitable for the installation.
• Tie one end ofthe cord to the loop in the module, and tie the other end ofthe cord to the
screw-eye in the appropriate size cork
• Place insertion rod into the pre-cut pocket at the base ofthe module and lower it into the
hole. Ifyou encounter resistance remove the module and ream the hole and re-insert the
module
• Once deployed to the desired depth, press the insertion rod against the side or the hole and
twist slightly to release the module. Remove the rod and push any excess cord into the pilot
hole and plug it with the cork.
• Indicate the module number, date, and time of installation and any pertinent comments on the
installation/retrieval log. Write the module serial number on the site map adjacent to the
appropriate map location.
• Clean the tile probe or drill bit and the insertion rod prior to use at the next location. Replace
the gloves as necessary before handling any modules
• Following module installation, the modules selected as trip blanks should be kept in the
sample box provided and stored as described above in "STORAGE" until sample retrieval.
Passive Soil Gas Module Retrieval
• Following the module exposure period (two weeks or as recommended by the manufacmrer)
identify and check each module location in the field using the site map.
• Remove the cork with a penknife or cork screw. Grasp the cord and pull the module from the
ground; verify the module ID number. Cut off and discard the cork and cord. Place the entire
module in its labeled container and tightiy secure the lid.
• Replace the sample container in the box.
ATK Thiokol Propulsion
RFI Work Plans
September 2002
6.1 Passive soil gas module Modules shipping
• Replace the sample container in the box. Where possible, please attempt to keep modules in
numbered sequence to expedite sample check-in and processing.
• Complete the module retrieval date/time on the installation/retrieval log
• Do not use Styrofoam "peanuts" as packing material. Bubble packing is acceptable. Water
ice can be added if desired, but cooling in general is not necessary. If shipping with ice,
please take precautions to keep boxes dry (perhaps shipping in a cooler)
• Retum the samples with paperwork (preferably by ovemight courier).
Holding time is 7 days from collection ofthe passive soil gas module to date of analysis. No
special preservation is required, but it is recommended that samples not be subjected to
extremes of temperature or pressure. If ice is added to the shipping container, care must be
taken that no precipitation enters the modules.
6.2 Passive Soil Gas Module Storage
Passive soil gas module modules are specially cleaned and stored after manufacturing. They
must remain sealed in their vials in the shipping boxes until deployment. DO NOT store them
near potential sources of organic vapors, including petroleum fuels, fiiel exhaust, solvents, or in
areas of new constmction or remodeling where paints, adhesives, foam insulating materials, etc.
may be present.
7.0 SAMPLE DOCUMENTATION
The following information must be recorded in the Field Book:
Date and time of sampling
Sampler's name and signature
Location of samples including depth and corresponding module ID number
Tjqje, number, sample number, and seals used on sample bottles
Weather
Any other pertinent information
ATK Thiokol Propulsion
RFI Work Plans
September 2002
8.0 ANALYTICAL PARAMETERS
The Passive soil gas module modules are required to be analyzed by the manufacturer at their laboratory oi
other approved laboratory. The laboratory uses modified EPA SW-846 Method 8260 for volatile organic
compounds. The sensitivity ofthe Passive soil gas modules for COCs is expected to be quite high. Metho
Detection Limits for Method 8260 analysis in the typical laboratory are as follows:
COC and Typical MDL for Soil Gas Modules
Compound
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,2,4-Trimethylbenzene
1,2-Dichloroben2ene
1,2-Dichloroethane
1,3,5-Trimethylbenzene
1,3-Dichloroben2ene
1,4-Dichlorobenzene
2-Methylnaphthaiene
Acenaphthene
Acenaphthylene
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
cis-1,2-Dichloroethene
Ethylbenzene
Fluorene
m/p-Xylene
Methyl-tert-butylether
Naphthalene
Octane
o-Xylene
Pentadecane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
Trichloroethene
Tridecane
Undecane
Vinyl Chloride
Abbreviation
1112TetCA
111TCA
1122TetCA
112TCA
11 DCA
11 DCE
124TMB
12DCB
12 DCA
135TMB
13DCB
14DCB
2MeNAPH
Acenaphthene
Acenaphthylene
BENZ
CCL4
CIBENZ
CHCL3
C12DCE
ETBENZ
Fluorene
mpXYL
MTBE
NAPH
OCT
oXYL
PENTADEC
PCE
TOL
t12DCE
TCE
TRIDEC
UNDEC
VC
MDL. ua
0.02
0.03
0.02
0.07
0.02
0.06
0.02
0.02
0.01
0.02
0.05
0.02
0.02
0.01
0.01
0.03
0.03
0.01
0.02
0.02
0.02
0.02
0.02
0.48
0.02
0.10
0.02
0.02
0.03
0.03
0.08
0.03
0.02
0.03
0.08
ATK Thiokol Propulsion
RFI Work Plans
September 2002
9.0 SAMPLE ACCOUNTABILITY AND CUSTODY
Follow procedures specified in the in the Data Collection Quality Assurance Plan in Volume Two o
the RFI Work plams. Requirements for sample custody and custody seals are discussed in these
documents.
ATK Thiokol Propulsion
RFI Work Plans
September 2002
Attachment 1
Typical Soil Gas Sorber Description and Installation
G0RE-SORBER® Module
Installation Schematic
KNOT-
STRING
KNOT-
LOOP FOR ATTACHING-
STRING
TAG WITH
UNIQUE SERIAL NUMBER
GRANULAR SORBENT •
BOTTOM END
SEAL
SOIL SURFACE
INSERTION TOOL
POCKET TO RECEIVE
INSERTION TOOL
Creotiv* Tachnologi*
Wortdwids
GORE-SORBER is a registered trademark of W.L. Gore & Associates, Inc.
ATK Thiokol Propulsion
RFI Work Plans
September 2002
ATTACHMENT 2
Investigation Maps
OLD DRUM
STORAGE AREA ENVIRONMENTAL
^ERVldE^
OLD DRUM ^TORAdE AREA
AT BLDd. M-l87
^WMU NO. 551
rra m SCALE KAVIHG Hi- P^V.
AIS NOTED!551-lgiWMU
I I I I
ROCKET DISPLAY
SIGN
SEPTIC! DRAINFIELDS
A, B & d
SWMU #625
raw ?=200± 625-l|SwMU
ATK Thiokol Propulsion
RFI Work Plans
September 2002
Appendix A
Copies of RFI Report for SWMU 622, 651 and 202
^
SWMU 202
OLD BURNING AREA NORTHEAST OF M-243
Source Characterization
Unit/Disposal Area Characteristics
This solid waste management unit is the former location of an open buming area northeast of Building M-
243 at Thiokol's High-Performance Propellant Development Area. This unit was operated for a short
period of time for the disposal of test and off-specification propellants by open buming.
The burninig area Is contained within a fenced area measuring approximately 25 ft by 25 ft. tt is estimated
that only about 200 to 300 pounds of waste were burned during the period of operation.
Physical Setting
The High-Performance Propellant Development Area is comprised of soils consisting of a clayey, silt unit
interbedded with minor sand and fine gravel. The thickness of the silt unit is greater than 20 feet. The
gravels are derived from limestone strata of the Pennsylvanian Oquirrh Formation. The gravels consist of
medium to dark gray angular to subangular clasts of limestone and dolomitic limestone. The silt is
calcareous with some clay, sand, and gravel. Clays of the upper interval tend to swell.
The depth to ground water in the vbinity is estimated to be 300 feet. The ground water, based upon the
available data, appears to be restricted to movement along faults and fractures. This is evidenced by Plant
Well No. 3, which was drilled 325 feet into unfractured matenal and was abandoned, as it produced only a
small volume of water.
Subsequently, Plant Well No. 3A was drilled as a replacement to Plant Well No. 3, and was drilled on a
fault having a N85 W trend. This well can produce 190 gpm with five feet of drawdown.
The movement and location of ground water beneath the area known as the High-Perfonmance Propellant
Devek)pment Area has not been well defined. Two wells, TCC3 and TCC3A, were drilled in this area in
1956 and 1962. Detailed discussion on these two wells can be found in RCRA Compliance Plan prepared
for Thiokol by Underground Resource Management, Inc., in August 1985. Well TCC3 was drilled 350 feet
t}elow ground surface and encountered ground water at approximately 300 and 320 feet; static water
levels measured in 1962 showed the water at an elevation of 4260 feet. This well was later abandoned
and has not been used. Well TCC3A is currently being used to supply process water to buildings in the
High-Performance Propellant Development Area. When drilled, this well encountered water at a depth of
317 feet and at 395 feet. The surface elevation of the ground water in 1962 was 285 feet.
Two more wells have been drilled near the M-225 buming grounds. One of these wells was drilled to a
depth of 200 feet, but could not be completed because the fractures in the limestone formations prohibited
further drilling. A second well was completed and ground water encountered at 618 feet. Ground water
appears to flow south and southeast toward the Great Salt Lake
Waste Characteristics
The wastes managed at this site consisted of waste propellant and propellant-contaminated waste.
Thiokol Propulsion RCRA Facility Investigation
Cl Figure 202-2
%
Contamination Characterization
Table 202-1 is a summary of the constituents detected in at least one sample during the investigation for
this site. This table also shows the range of concentrations for each constituent. Minimum concentration
values preceded by a less-than sign (<) indicate the laboratory reported the chemtoal was not detected
and the value shown represents the detection limit. If the laboratory reported a metal undetected in a
sample, but that metal was detected in other samples, the minimum concentration shown is one-half the
reported detection limit.
Also included on Table 202-1 is the 95 percent upper confidence limit (UCLgg). The UCL95 is a value
calculated from the reported laboratory data and represents the value that is equal to or exceeds the true
mean concentration of a chemical at the investigation site. Use of this value as the concentration term
when comparing to background and risk-based screening levels provides reasonable confkJence that the
true site exposure will not be underestimated.
Cl
TABLE 202-1
CONSTITUENT CONCENTRATION RANGE
CONSirrUENT
1,1,1 -TRICHLOROETHANE
2-BUTANONE
ACETONE
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
MINIMUM
CONCENTRATION
(mg/Kg)
0.01
<0.01
0.01
0.05
0.12
10.80
0.75
MAXIMUM
CONCENTRATION
(mg/Kg)
0.03
0.02
0.02
0.42
1.48
18.20
7.08
UCL^
(mg/Kg)
0.02
0.02
0.01
0.47
1.79
15.59
8.79
The laboratory also reported results for chloroform and methylene chloride in low ppb concentration (<10
ug/kg) in at least one sample collected from this site, but the results were qualified as t>eing estimated
values £is they were less than the reporting limit. Because of the qualified data and the very low
concentrations, the results were not considered as positive, and these organics were eliminated from
further consideration. No other organics were detected in any of the samples.
No nitroglycerine, HMX, silver, or mercury were detected in any of the samples from this site above the
method reporting limits.
^
Comparison to Background Concentrations
Table 202-2 is a summary of the corresponding background concentrations for those constituents
detected and summarized in Table 202-1. Included are both the results of background samples taken
from areas at Thiokol believed to be representative of naturally occurring levels of chemicals in the soil
and background concentrations of elements is soils which have been collected in soils of the
counterminous U.S. and analyzed by the U. S. Geological Survey (USGS).
Thiokol Propulsion RCRA Facility Investigation
1,1.1-TricMora«mane Fnquancy Scaairptot
SWMU 202
1.1,1 -TrtchtoroathiM Bmplot by Gioup
SWMU 202
Cl
%
0.024
0.018
0 012
0.006
0.000
24uiiiKifw Fnciuiney SaHwplot
SWMU 202
0.024
0.020
0.01B
0.012
o.oce
0.004
0.000
•
,
,
,
• 1
• 2
c 4
o 8
O 7
• 1 1
• «c
o 7e
D Scaus
o 1i<
0.024
OOIS
0.012
0.006
0.000
a
1 i
Backgnund
Am of Conown
2-Buiwiam BaqMM by Qnup
SWMU 202
CD 25%-78%
o Madian vakm
0.024
0.020
0016
0.012
0.004
0.000
i
:
a
Background
Araa m Concein
CD 25%-75%
• Madlan valua
Figure 202-3a
ri
Cadmium Fraquancy Scanarptot
SWMU 202
0.8
5 8
IC
0.2
0.0
Chtofstorm Fiaquancy
SWMU 202
0.04
0.03
S. 0.02
0 00'—a—o_
^CMnvoinScy^iA
• 1
• 2
o 3
o S
• 1
• 2
> 4 o 5
o 6 O 8
O 9
1.2
0.8
0.4
0.2
0.0
0.03
0.02
Cadmium Boxplol by Qroup
SWMU 202
D
o
Backoreund
AraadConcam
Chlorafonn Bonifcit by Gimp
SWMU 202
zr: MirwAikii
CD 25V75%
o Madian value
Background
Araa ol Cancan
m Min^tax
cm 2SV75%
a Madian value
Figure 202-3c
• «« f
TABLE 202-3
COMPARISON TO BACKGROUND AND RISK- BASED CONCENTRATIONS
CONSTITUENT
1.1.1-
Trichloroethane
Acetone
Beryllium and
compounds
Cadmium and
compounds
Lead
Methyl ethyl
ketone
Total Chromium
(1:6 ratio CrVI:Cr
III)
UCL„
0.02
0.01
0.47
1.79
8.79
0.02
15.59
MAXIMUM REPORTED
RFI CONCENTRATIONS
(mji/Kg)
AREA OF
CONCERN
0.03
0.02
0.42
1.48
7.08
0.02
18.20
THIOKOL
BACKGROUND
0.02
0.04
2.20
1.39
32.50
0.01
38.60
USGS
NATIONAL
BACKGROUND
RANGE'
(mg/Kg)
<1-15
0.01 - 0.7
<10-700
1.0-2000
PRELIMINARY
REMEDIATION'
GOALS mg/Kg)
RESIDENTIAL
768.50
1569.64
154.37
37.00
400.00
7325.38
210.68
INDUSTRIAL
1400.00
6219.62
2241.59
810.00
1000.00
27714.47
448.32
RCRA
CORRECTIVE
ACTION
LEVELS'
(ppmw)
7000.00
8000.00
0.20
40.00
4000.00
400.00
EPA
SOIL
SCREENING
LEVELS
DAF 20
(mg/Kg)
2.00
16.00
63.00
8.00
38.00
' EPA Region 9 Preliminary Remediation Qoals (11/1/1999) ' EPA Region III Risk-Based Concentrattons (October 22,1997)
^ EPA proposed RCRA Corrective Action Rule (55 FR 30798. July 27,1990) * USGS Background Concentrations of Elements In Soils (1984)
Thiokol Propulsion RCRA Facility lnvestlgatk)n
CASE SELECTION CONDITIONS:
Include if:
vl ='1,1,1-TR'
RIABLES:
5; GROUP -9999
2: NEWRESUL -9999
STAT. Kruskal-Wallis ANOVA by Ranks (202stat.sta)
NONPAR Independent (grouping) variable: GROUP
__ STATS Kruskal-Wallis test: H (1, N= 51) = 16.16669 p =.0001
Depend.: Valid Sum of
NEWRESUL Code N Ranks
"" Group 1 1 42 945.0000
Group 2 2 9 381.0000
^ data fiie: 202stat.sta [ 410 cases with 6 variables ]
CASE SELECTION CONDITIONS:
Include If:
vl='2-Butano'
VARIABLES:
5: GROUP -9999
2: NEWRESUL -9999
01
STAT. Kruskal-Wallis ANOVA by Ranks (202stat.sta)
NONPAR Independent (grouping) variable: GROUP
STATS Kaiskal-Wallis test: H (1, N= 51) = 34.59423 p =.0000
Depend.: Valid Sum of
NEWRESUL Code N Ranks
Group 1 1 42 927.0000
Group 2 2 9 399.0000
data file: 202stat.sta [ 410 cases with 6 variables ]
CASE SELECTION CONDITIONS:
Include if:
v1='acetone'
VARIABLES:
- 5: GROUP -9999
2: NEWRESUL -9999
STAT. Kruskal-Wallis ANOVA by Ranks (202stat.sta)
ONPAR Independent (grouping) variable: GROUP
TATS Knjskal-Wallis test: H (1, N= 51) = 13.01973 p =.0003
Depend.: Valid Sum of
NEWRESUL Code N Ranks
STAT. Kruskal-Wallis ANOVA by Ranks (202stat.sta)
NONPAR Independent (grouping) variable: GROUP
STATS Kruskal-Wallis test: H (1, N= 51) = .0050764 p =.9432
AP i^p epend.: Valid Sum of
EWRESUL Code N Ranks
Group 1 1 42 1094.000
Group 2 2 9 232.000
data file: 202stat.sta [ 410 cases with 6 variables ]
CASE SELECTION CONDITIONS:
Include if:
vl ='chromium'
VARIABLES:
5: GROUP -9999
'- 2: NEWRESUL -9999
STAT. Kruskal-Wallis ANOVA by Ranks (202stat.sta)
NONPAR Independent (grouping) variable: GROUP
STATS Kmskal-Wallis test: H (1. N= 54) = 11.41311 p =.0007
Depend.: Valid Sum of
NEWRESUL Code N Ranks
"T^G Group 1 1 45 1383.000
roup 2 2 9 102.000
^ data file: 202stat.sta [ 410 cases with 6 variables ]
CASE SELECTION CONDITIONS:
.. Include if:
vis'lead'
VARIABLES:
5: GROUP -9999
2: NEWRESUL -9999
STAT. Kmskal-Wallis ANOVA by Ranks (202stat.sta)
NONPAR Independent (grouping) variable: GROUP
STATS Kmskal-Wallis test: H (1, N= 49) = .1566830 p =.6922
Depend.: Valid Sum of
NEWRESUL Code N Ranks
Group 1 1 40 1015.000
Group 2 2 9 210.000
m SWMU 551
OLD DRUM STORAGE AREA AT M-187
Source Characterization
Unit/Disposal Area Characteristics
SWMU 551 is designated as the location of a former storage area for empty drums. The storage area was
designated as M-187 located in Thiokol's Administration and Manufacturing Area (See Figures 551-1 and
551-2).
The site was used as storage for empty drums to be returned back to vendors or non-returnable drums to
be sold to drum recyclers or otherwise disposed.
The operational dates for this site are unknown. However, its use is estimated to have begun
approximately 10 to 15 years prior to when the drum storage yard was moved to M-136, which occurred in
1986.
This site was not intended for management of waste materials. The empty drums likely contained some
residual product as evidence of spilled materials is visible on the surface of the soil.
Physical Setting
This site is located on the western flank of the Blue Springs Hills. This is a horst and graben block fault
system with two major fault trends: north 15 degrees east and east-west. The Blue Springs Hills at this
location consists of Paleozoic carbonate units covered with a thin veneer of Quaternary alluvium. The
valley is filled with Tertiary and Quaternary sediments which include older fluvial and lacustrine sediments,
alluvial fan deposits. Lake Bonneville sediments, and recent alluvium. M-187 is sited on the gentle slope of
a moderately large alluvial fan. Sediments consist of unconsolidated gravels, sands, and clays of colluvial
(debris flow), fluvial, and alluvial depositional environments.
Within the valley-fill, ground water occurs in unconfined conditions. The valley-fill sediments consist of
sands and gravels interbedded with silts and clays. Generally, the coarser materials are found along the
margins of the valley and as basal sediments above the bedrock. The silts and clays act as confining units
interbedded within the coarser materials. Within consolidated sediments, ground water occurs in fault
zones and solution cavities in the limestones.
The regional aquifer is found in unconsolidated alluvial material within the Blue Springs Valley and in
fractured bedrock along the flanks of the range. There does not appear to be a distinct low permeability
barrier t)eneath the entire site, although discontinuous zones are ubiquitous. The thickness of the aquifer
is unknown but it is expected to be greater than 500 feet. All of the wells installed to date have been drilled
to less than the bottom of the aquifer. The deepest wells drilled into the saturated zone are Thiokol
exploratory water wells TCC8 and TCC8A, completed in 1960 and 1962, west of UDLV. Well TCC8A was
drilled 610 feet deep, penetrating 460 feet of saturated material.
This site is located approximately 800 feet north of monitoring well B-5 and approximately 1000 feet
southwest of well B-4. Wells B-4 and B-5 were installed in 1989 to a depth of 237 feet and 176 feet
respectively. The depth to ground water was 215.87 feet in well B-4 and 153.48 feet in well B-5 when
measured in November 1999. Ground water movement appears to be from well B-4 towards well B-5
which is a southwesteriy direction.
Thiokol Propulsion RCRA Facility Investigation
m
g^jj^i:i*- ^.v'
Figure 551-2
Contamination Characterization
Table 551-1 is a summary of the constituents detected in at least one sample during the investigation for
this site. This table also shows the range of concentrations for each constituent. Minimum concentration
values preceded by a less-than sign (<) indicate the laboratory reported the chemical was not detected
and the value shown represents the detection limit. If the laboratory reported a metal undetected in a
sample, but that metal was detected in other samples, the minimum concentration shown is one-half the
reported detection limit.
Also included on Table 551-1 is the 95 percent upper confidence limit (UCL95). The UCL95 is a value
calculated from the reported laboratory data and represents the value that is equal to or exceeds the true
mean concentration of a chemical at the investigation site. Use of this value as the concentration term
when comparing to background and risk-based screening levels provides reasonable confidence that the
true site exposure will not be underestimated.
TABLE 551-1
CONSTITUENT CONCENTRATION RANGE
t
CONSTITUENT
1.1.1-
TRICHLOROb IHANE
2-BUTANONE
2-HEXANONE
ACETONE
CADMIUM
CHROMIUM
LEAD
MERCURY
METHYLENE
CHLORIDE
SILVER
MINIMUM
CONCENTRATION
(mg/Kg)
<0.010
<0.010
<0.010
<0.010
0.05
12.40
7.70
0.01
<0.010
0.10
MAXIMUM
CONCENTRATION
(mg/Kg)
0.06
0.04
0.03
0.07
0.83
21.80
63.90
0.07
0.04
3.50
UCL ,5
(mg/Kg)
0.02
0.02
0.01
0.02
0.43
18.00
22.54
0.05
0.01
0.49
The laboratory also reported results for trichloroethene, 1,1,1-dichloroethene, and 4-methyl-2-pentanone
in low ppb concentrations (<10 ug/kg) in at least one sample collected from this site, but the results were
all qualified as being estimated values as they were less than the reporting limit. The results for many of
these chemicals were also qualified as being found in the laboratory blank. Because of these data
qualifiers and the very low concentrations, the results were not considered as positive results and these
organics were eliminated from further consideration.
The samples were also analyzed for perchlorate, but the laboratory reported the result for all samples as
undetected.
Thiokol Propulsion RCRA Facility Investigation
1,1,1-Trichloroetnane Frequency Scanerplot
SWMU 551
1,1,1-Trichloroethane Boxplot by Group
SWMU 551
"I
0 06
0.05
004
0.03
0 02
001
"
•
• .
o
Stttttt^tt
. o
O
O
o o
1 case
2caaes
3 cases
4 cases
5 cases
7 cases
0.06
0.05
E
r 003
0.02
0 01
D
Background
Area of Concem
m; Min-Max
CD 25%-75%
0 Madian value
2-Butanone Frequerrcy Scanerplot
SWMU 551
2-Butanone Boxptot by Group
SWMU 551
£ 0.02
001
^ttttttgtt
1 case
2 cases
3-4 cases
5-6case«
7 cases
6-9 case*
>9 cases
0.04
E
0.02
001
0.00
Background
Area ol Concern
HI Min-Max
CD 25%-75%
• Median value
Figure 551 -3a
>
10
08
I 0.6
0.0
Cadmium Frequency Scatlsrplol
SWMU 551
5 t t t t t
^ c\j in (^ o m
t t
gaSgggg8B8
• 1 case
° 2 cases
° 3 cases
o 4 cases
o 5 cases
0.8
06
02
Cadmium Boxplot by Group
SWMU 551
a
Background
Area of Concem
zn Min-Max
CD 25%-75%
• Median value
m
Chromium Frequency Scatterplot
SWMU 551
§tttttt§t 5 li. t w I* "?
gs g s ^ ig gy 1 case
2c
30
18
Chromium Boxplot by Group
SWMU 551
Figure 551 -3c
a
•
Background
Area ol Concem
3Z Min-Max
cm 25%-75%
u Median value
m
-^
Methylene Chloride Frequency Scatterplot
SWMU 551
0.035
0.030
O.QEO
I 0.015
0.010
O.OOS
gttttttgtt
gsgg^igg^^
1 case
° 2 cases
o 4 cases
o 5 cases
o Ceases
O 8 cases
Methylene Chloride Boxplol by Qroup
SWMU 551
0035
0.010
0.005
Badtgrtxjhd
Area of CorKern
in Min-Max
cm 25%-75%
o Median value
12
= 6
iB
Silver Frequency Scatterplot
SWMU 551
ft " " ' Q 9 , B a Q_
g; N ITI .f> o
g s g g i i g' g y
1 case
° 4 cases
° 5 cases
o 6 cases
o 7 cases
Silver Boxplot by Group
SWMU 551
Background
Area of Concem
HI Min-Max
CD 25%-75%
• Median value
Figure 551-3e
# iwf #
TABLE 551-3
COMPARISON TO BACKGROUND AND RISK- BASED CONCENTRATIONS
CONSTITUENT
2-HEXANONE
Acetone
1.1.1-
Trichloroethane
Lead
Silver and
compounds
Cadmium and
compounds
Total Chromium
(1:6 ratio CrVhCr
III)
Mercury and
compounds
UCL,5
0.01
0.02
0.02
22.54
0.49
0.43
18.00
0.02
MAXIMUM REPORTED
RFI CONCENTRATIONS
(mg/Kg)
AREA OF
CONCERN
0.03
0.07
0.06
63.90
3.50
0.83
21.80
0.07
THIOKOL
BACKGROUND
0.00
0.04
0.02
32.50
12.80
1.39
38.60
0.04
USGS
NATIONAL
BACKGROUND
RANGE'
(mg/Kg)
<10-700
0.01 - 0.7
1.0-2000
<0.01 - 4.6
PREUMINARY
REMEDIATION'
GOALS (mg/Kg)
RESIDENTIAL
1569.64
768.50
400.00
391.07
37.00
210.68
23.46
INDUSTRIAL
6219.62
1400.00
1000.00
10219.79
810.00
448.32
613.20
RCRA
CORRECTIVE
ACTION
LEVELS'
(ppmw)
8000.00
7000.00
200.00
40.00
400.00
20.00
EPA
SOIL
SCREENING
LEVELS
DAF 20
(mg/Kg)
16.00
2.00
34.00
8.00
38.00
Thiokol Propulsion RCRA Facility Investigation
This site may pose a slight increased risk due to surface levels of lead and volatile organics. However, the
concentrations for all of these COPC do not exceed the EPA's Preliminary Remediation Goal for residential
exposure.
Recommendations for Additional Work
Based on the findings of the investigation conducted at this site during the RFI, Thiokol believes there is no
further action needed for this site.
3
Thiokol Propulsion RCRA Facility Investigation
Group 1 1 42 1260.000
Group 2 2 19 631.000
ata fiie: 551stat.sta [ 603 cases with 6 variables ]
CASE SELECTION CONDITIONS:
Include if:
v1 ='acetone'
VARIABLES:
5: GROUP -9999
2: NEWRESUL -9999
STAT. Kruskal-Wallis ANOVA by Ranks (551stat.sta)
NONPAR Independent (grouping) variable: GROUP
STATS Kruskal-Wallis test: H (1, N= 61) = .0710280 p =.7898
Depend.: Valid Sum of
NEWRESUL Code N Ranks
Group 1 1 42 1316.500
Group 2 2 19 574.500
data file: 551stat.sta [ 603 cases with 6 variables ]
ra CASE SELECTION CONDITIONS:
nclude if:
v1='cadmium'
VARIABLES:
^ 5: GROUP -9999
2: NEWRESUL -9999
STAT. Kruskal-Wallis ANOVA by Ranks (551 stat.sta)
NONPAR Independent (grouping) variable: GROUP
^ STATS Kruskal-Wallis test: H (1, N= 64) = 1.216566 p =.2700
Depend.: Valid Sum of
NEWRESUL Code N Ranks
~ Group 1 1 45 1536.000
Group 2 2 19 544.000
-" data file: 551 stat.sta [ 603 cases with 6 variables ]
CASE SELECTION CONDITIONS:
Include if:
vl ='chromium'
^. ARIABLES:
5: GROUP -9999
2: NEWRESUL -9999
"- VARIABLES:
5: GROUP -9999
>2: NEWRESUL -9999
STAT. Kruskal-Wallis ANOVA by Ranks (551 stat.sta)
NONPAR Independent (grouping) variable: GROUP
STATS Kruskal-Wallis test: H (1, N= 56) = .0493678 p =.8242
Depend.:
NEWRESUL Code
Valid
N
Sum of
Ranks
Group 1
Group 2
1
2
37
19
data file: 551 stat.sta [ 603 cases with 6 variables ]
CASE SELECTION CONDITIONS:
Include if:
v1='silver'
VARIABLES:
5: GROUP -9999
2: NEWRESUL -9999
1064.000
532.000
^
STAT.
NONPAR
STATS
Depend.:
NEWRESUL
Kruskal-Wallis ANOVA by Ranks (551 stat.sta)
Independent (grouping) variable: GROUP
Kruskal-Wallis test: H (1, N= 59) = .6337014 p =.4260
Code
Valid
N
Sum of
Ranks
Group 1
Group 2
1
2
40
19
1240.000
530.000
— data file: 551 stat.sta [ 603 cases with 6 variables ]
-%
SWMU 625
SEPTIC DRAINFIELDS A, B, and C
Source Characterization
Unit/Disposal Area Characteristics
This solid waste management unit is identified as the septic drainfield system for a large portion of
Thiokol's Administration and Manufacturing Area (See Figures 625-1 and 625-2). The drainfield is located
southwest of the rocket display across State Highway 83.
Drainfield A was used during the period of 1975 -1995, drainfield B from 1982 -1995, and drainfield C
from 1987 -1995. In 1995, the drainfields were abandoned when septic and industrial wastes were
collected and piped to a new wastewater treatment plant.
Hydrogeologic Characteristics
This site is located on the western flank of the Blue Springs Hills. This is a horst and graben block fault
system with two major fault trends: north 15 degrees east and east-west. The Blue Springs Hills at this
location consists of Paleozoic carbonate units covered with a thin veneer of Quaternary alluvium. The
valley is filled with Tertiary and Quatemary sediments which include older fluvial and lacustrine sediments,
alluvial fan deposits. Lake Bonneville sediments, and recent alluvium. The disposal area is sited on the
gentle slope of a moderately large alluvial fan. Sediments consist of unconsolidated gravels, sands, and
clays of colluvial (debris flow), fluvial, and alluvial depositional environments.
Within the valley-fill, ground water occurs in unconfined conditions. The valley-fill sediments consist of
sands and gravels interbedded with silts and clays. Generally, the coarser materials are found along the
margins of the valley and as basal sediments above the bedrock. The silts and clays act as confining units
interbedded within the coarser materials. Within consolidated sediments, ground water occurs in fault
zones and solution cavities in the limestones.
The regional aquifer is found in unconsolidated alluvial material with the Blue Springs Valley and in
fractured bedrock along the flanks of the range. There does not appear to be a distinct low pemneability
barrier beneath the entire site, although discontinuous zones are ubiquitous. The thickness of the aquifer
is unknown but it is expected to be greater than 500 feet. All of the wells installed to date have been drilled
to less than the bottom of the aquifer. The deepest wells drilled Into the saturated zone are Thiokol
exploratory water wells TCC8 and TCC8A, completed in 1960 and 1962, west of UDLV. Well TCC8A was
drilled 610 feet deep, penetrating 460 feet of saturated material.
This site is located approximately 800 feet south of monitoring well E-2,1000 feet east of well G-1, and
200 feet west of wells E-7, F-5, and B-6. Depth to ground water on June 30, 1999, was measured as
100.58' in E-2, 83.56' in G-1, and 98.80' in B-6.
Ground water movement appears to be from north to south at this site.
Waste Characteristics
The wastes managed at this unit were predominantly domestic waste with some industrial wastewater.
Thiokol Propulsion RCRA Facility Investigation
Ii Figure 625-2
-•
M
Also included on Table 625-1 is the 95 percent upper confidence limit (UCL gg). The UCL gg is a value
calculated from the reported laboratory data and represents the value that is equal to or exceeds the true
mean concentration of a chemical at the investigation site 95 percent of the time. Use of this value as the
concentration term when comparing to background and risk-based screening levels provides reasonable
confidence that the true site exposure will not be underestimated.
TABLE 625-1
CONSTITUENT CONCENTRATION RANGE
^
CONSTITUENT
BIS(2-
ETHYLHEXYL)PHTHALATE
BORON
CADMIUM
CHLOROFORM
CHROMIUM
DI-N-BUTYLPHTHALATE
LEAD
MERCURY
SILVER
BARIUM
COPPER
ZINC
MINIMUM
CONCENTRATION
(mg/Kg)
<0.33
0.20
0.05
<0.01
10.10
<0.33
0.70
0.004
0.10
21.40
3.28
19.6
MAXIMUM
CONCENTRATION
(mg/Kg)
0.70
14.20
0.98
0.02
52.90
0.56
15.80
0.75
166.00
176.00
53.00
149.00
UCLK
(mg/Kg)
0.21
9.68
0.42
0.01
17.91
0.20
1.22
0.02
1.21
136.47
14.27
57.43
The laboratory also reported results for methylene chloride, acetone, and 1,1,1-trichloroethane in low ppb
concentrations (<10 ug/kg) and diethylphthalate also at low ppb (<330 ug/Kg) in at least one sample
collected from this site. However, the results were all qualified as t>eing estimated values as they were
less than the reporting limit. Many of these chemicals were also qualified as being found in the laboratory
blank. With the exception of 1,1,1 -trichloroethane. all of these organics are considered by EPA to t>e
common lat>oratory contaminants. Because of these data qualifiers and the very low concentrations, the
results were not considered as positive results and the chemicals were eliminated from further
consideration.
Comparison to Baclcground Concentrations
Table 625-2 is a summary of the corresponding background concentrations for those constituents
detected and summarized in Table 625-1. Included are both the results of background samples taken
from areas at Thiokol t)elieved to be representative of naturally occurring levels of chemicals in the soil
Thiokol Propulsion RCRA Facility Investigation
Zinc Frequency Scatterplot
SWMU 625
Zinc Boxplot t>y Group
SWMU 625
140
120
100
S eo
Re
s
u
l
t
2
40
20
. : ; • •
j
trt-t-i-i-Ki-t-i-->LLLi.Li.L>Li.U.lJ.U. yjCMin(DOino»no
g^^^g^i^H Background
Area ol Concem
1 Min-Max
: I 25%-75%
o Median value
Silver Frequency Scalterplol
SWMU 625
Silver Boxplol by Group
SWMU 625
#
(9 o in p in o
1 case
' 4casas
o 5c
o 14c
o 15 cases
Figure 625-3a
1 .,
Background
Area of CorKern
m Min-Max
CD 25')i-75%
• Median value
Dl-N-Butylphthalate Frequency Scatterplot
SWMU 625
Dl-N-Butylphthalate Boxplot by Group
SWMU 625
g"»Sggg8g
^ case
o 3 cases
'•- J case?
o 5 cases
o 6 cases
1 0
OB
0.6
04
0.2
...
V^ 1
Background
Area ol Concern
Min-Max
CD 25';o-75'i=
o Median value
Copper Frequency Scanerplot
SWMU 625
Copper Boxplot by Group
SWMU 825
%
1 case
BG-SUB BG-5FT BG-10FT A0C-5FT ° 2 cases
8G-2FT BG-6FT BG-1 SFT AOC-10FT ° 3 cases
60
50
30
Figure 625-3c
D
I — I
Background
Area ol Concern
in *«n-Max
CH 25%-75%
• Median value
m
Cadmium Frequency Scatterplot
SWMU 625
^ttttttct
gSiJS^^g8^
1 case
° 2 cases
° 3 cases
o 5 cases
o 11 cases
^ 0.8
06
Cadmium Boxplol by Group
SWMU 625
...
D
Background
Area of Concem
I Min-Max
CD 25%-75%
• Median value
Boron Frequency Scanerplot
SWMU 625
Boron BOKplot by Group
SWMU 625
28
24
20
^ 16
t
IE 12
8
4
,
•
• ,
•
1
1
! '
28
of 12
a
D
BG-SUR BG-5FT BG-10FT AOC-SFT
BG-2FT BG-6FT BG-1SFT AOC-10FT " ' ^aae
Background
Area ol CorKern
^ Min-Max
CD 25%-r5%
• Median value
m Figure 625-3e
Comparison to Risk-Based Levels
Table 625-3 is a tabular comparison of the maximum concentration levels and the calculated 95 percent
upper confidence limit (UCL 95) for the constituents of concern to the respective maximum Thiokol
background level, USGS background levels. Preliminary Remediation Goals. RCRA Corrective Action
Levels, and EPA Soil Screening Levels.
The PRG values shown in Table 625-3 are chemical concentrations that correspond to fixed levels of risk
(i.e., either a one-in-one-million [10*] cancer risk, or a noncarcinogenic hazard quotient of 1).
The RCRA Corrective Action Levels represent proposed values which, if found in the environment in
excess of this level, could trigger the need for further analysis.
Soil Screening Levels (SSL) are concentrations of contaminants in soil that are designed to be protective
of exposures in a residential setting. The SSL represent the concentration of a contaminant, which if
present at a site at or below this concentration, would be considered protective of ground water. The
values shown were developed using a dilution attenuation factor (DAF) of 20 to account for natural
processes that reduce contaminant concentrations In the subsurface.
There were no cases where either the maximum area of concem concentration or the calculated UCL ^
value exceeded the risk-based concentrations.
Qppglusipns
The investigation conducted at this site does not indicate the presence of chemicals which are significantly
atjove Thiokol background levels or which exceed risk-beised standards.
This site does not appear to pose any risk to human health or the environment.
Recommendations for Additional Work
Based on the findings of the investigation conducted during the RFI, Thiokol believes no further action is
needed for this site.
m Thiokol Propulskjn RCRA Facility Investigation
# #
TABLE 625-3
COMPARISON TO BACKGROUND AND RISK- BASED CONCENTRATIONS
CONSTITUENT
Total Chromium
(1:6 ratio CrVI:Cr
III)
Zinc
UCL„
17.91
57.43
MAXIMUM REPORTED
RFI CONCENTRATIONS
(mg/Kg)
AREA OF
CONCERN
52.90
149.00
THIOKOL
BACKGROUND
38.60
89.00
USGS
NATIONAL
BACKGROUND
RANGE'
(mg/Kg)
1.0-2000
<5 - 2900
PRELIMINARY
REMEDIATION'
GOALS mg/Kg)
RESIDENTIAL
210.68
23463.19
INDUSTRIAL
448.32
RCRA
CORRECTIVE
ACTION
LEVELS'
(ppmw)
400.00
EPA
SOIL
SCREENING
LEVELS
DAF 20
(mg/Kg)
38.00
12000.00
' EPA Region 9 Preliminary Remediation Goals (11/1/1999)
^ EPA proposed RCRA Corrective Action Rule (55 FR 30798, July 27,1990)
^ EPA Region III Risk-Based Concentrations (October 22,1997)
* USGS Background Concentrations of Elements in Soils (1984)
Thiokol Propulsion RCRA Facility Investigation
Depend.:
VAR2
Group 1
Group 2
Code
1
2
Valid
N
38
31
Sum of
Ranks
1554.000
861.000
data file: 625stat.STA [ 761 cases with 6 variables ]
CASE SELECTION CONDITIONS:
Include if:
v1='lead'
VARIABLES:
5: VAR5
2: VAR2
-9999
-9999
STAT.
NONPAR
STATS
Depend.:
VAR2
Group 1
Group 2
Kruskal-Wallis ANOVA by Ranks (625stat.sta)
Independent (grouping) variable: VAR5
Kruskal-Wallis test: H ( 1, N= 70) = 13.29941 p =.0003
Code
1
2
Valid
N
39
31
Sum of
Ranks
1675.500
809.500
—^data file: 625stat.STA [ 761 cases with 6 variables ]
CASE SELECTION CONDITIONS:
Include if:
v1='DI-N-BUT'
VARIABLES:
5: VAR5
2: VAR2
STAT.
NONPAR
STATS
Depend.:
VAR2
Group 1
Group 2
-9999
-9999
Kruskal-Wallis ANOVA by Ranks (625stat.sta)
Independent (grouping) variable: VAR5
Kruskal-Wallis test: H (1, N= 65) = .3997892 p =.5272
Code
1
2
Valid
N
32
33
Sum of
Ranks
1010.500
1134.500
"* data file: 625stat.STA [ 761 cases with 6 variables ]
CASE SELECTION CONDITIONS:
Include if:
v1='copper'
VARIABLES:
5: VAR5
2: VAR2
-9999
-9999
vl ='cadmium'
VARIABLES:
5: VAR5 -9999
12: VAR2 -9999
STAT.
NONPAR
STATS
Depend.:
VAR2
Kruskal-Wallis ANOVA by Ranks (625stat.sta)
Independent (grouping) variable: VAR5
Kruskal-Wallis test: H (1, N= 75) = 1.856299 p =.1731
Code
Valid
N
Sum of
Ranks
Group 1
Group 2
1
2
44
31
1794.500
1055.500
data file: 625stat.STA [ 761 cases with 6 variables ]
CASE SELECTION CONDITIONS:
Include if:
v1='boron'
VARIABLES:
5: VAR5 -9999
2: VAR2 -9999
kSTAT.
'NONPAR
STATS
Dcpci'id..
VAR2
Kruskal-Wallis ANOVA by Ranks (625stat.sta)
Independent (grouping) variable: VAR5
Kruskal-Wallis test: H (1, N= 47) = 7.688069 p =.0056
Code
Vaiid
N
Sun-,:'
Ranks
Group 1
Group 2
1
2
16
31
507.5000
620.5000
"" data file: 625stat.STA [ 761 cases with 6 variables ]
CASE SELECTION CONDITIONS:
Include if:
v1='BIS(2-ET'
VARIABLES:
5: VAR5
2: VAR2
-9999
-9999
„ STAT.
NONPAR
STATS
^li
epend.
AR2
Kruskal-Wallis ANOVA by Ranks (625stat.sta)
Independent (grouping) variable: VAR5
Kruskal-Wallis test: H (1, N= 65) = 3.124866 p =.0771
Code
Valid
N
Sum of
Ranks
Group 1
Group 2
1
2
32
33
1144.000
1001.000
%
^J V
,CATE
CRAVE L PIT
175B
Location of Old Test Pits
T-75
I -"7"^ O^ D T-B^T ^ 1 S>/^IAA>C/A;(O-
"~r-7S" (X\r<o>. no^"^"^^ Ui 0-^ ^ o(d -/nrs/ />/1^ 7^>wt/
(Ajeir<- tt5je_ :S' 2o yr^* cuao TSD C(O -HxAD^tJi sU<J.t>c^
c^i^jL. -Hme, /nJo^u»«ijj (X sttuiU a«*oa«f */ f^ i^iA.tUi<up ('Jt'^
C/(ic U;«fel_UioV ctt£.tf^ (X«}aiU . 7o Cw^urt *^K«_ <au^as 6*/<.«Jt_
\
o
/ft(^r(^^
o. O Tes^^r4-«vre&f
-1-
Sorl tcLvcpLi v/r^Aj- CjUiaxJsLil -Qout/i -eacA rcs.-^ 'p'^f OAA.^
OJKX QJM^ZU. A)^ //mX/ ^DXj A'6-^ C/(>y- ^ i/0A^^(2^ YinBTlkLS.
UAA^ -I4«'^^«>t^
ENVIRONMENTAL LAB WORK REQUEST I S^SY
™ THIOKOL ENVIRONMENTAL LABORATORY LWR No. E12112
Login No.
VAIX.^^ i-UA)ga>4-S^H
COST CENTER
%zoo
WORK OMOEK
1^7)'^ 'T^Z-Q-^
ORGANIZATION
]^^iy?Vo>^miU/C^-^
REPORT RESIXIS TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS
T»h <us/ ?»<g X T--/S-m-^^/A^.£S)X.M(r. C/fty ^lili\
/^ Al TiZ^ l(
\\ X 1-75 T^
MOA. fLOSA MBTALS.(ii^/j
Hm, ^K ^t C/tif \\
^i^-^2/kfol tr T-7^ ^^ \)0A^fUM n^c^L^fhi,!) \\
fiiS^i T-75 22SL
1/ 7-7S ^J^s-
^Mx.dPl^M^t.CJi)^
^OA, f^ lheU(hkO
l\ JL ILJS-«&. ^ m,M^,^h
ll
M
^ // T'7g^ 4S5. Vb^ £L£A»fleLk(jbkf^ \\
CHAIN OF CUSTODY
1
RELINQUISHED BY
^iJ /L//ft L^
DATE
7-2?-^2_
TIME
?.'s-^
RECEIVED BY
'^{/^0a^!^
DATE
y-22-p'2
TIME
^.ss~
FOR LABORATORY USE ONLY
DATE COMI'LETED DATE MPORTIi D SI G.N A TURE
CERTIFICATE OF ANALYSIS
Listing of sample Information and Testing Requested
Monday, August 26, 2002
TESTED FOR ATK Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp, UT 84322
Paul Hancock
Project: Misc. Environmental Testing
Login Number L5584
Lab No Client Number
Test Requested Description
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-3732
800-863-8080
Received CoilectDate/Time
Matrix
I L5584-1 PIT 1 WEsf" T-75 07/22/02 07/22/02 09:08
SW-846, 8260
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 8330 Modified
EPA 314.0
Volatile Organics Appendix 9
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metais Analysis (RCRA)
Sb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Explosives Analysis
Perchlorate - lon Chromatography
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
I L5584-2 PIT 2 MID T-75 07/22/02 07/22/02 09:20
SW-846, 8260
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 8330 Modified
EPA 314.0
Volatile Organics Appendix 9
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Pb ICP Metals /^alysis (RCRA)
Sb ICP Metals Analysis (RCRA)
Se ICP Metais Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
ICP/GF/VA Metals Digestion
Explosives Analysis
Perchlorate - lon Chromatography
Soli
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soli
I L5584-3 PIT 3 EAST T-75 07/22/02 07/22/02 09:25
SW-846, 8260
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 8330 Modified
EPA 314.0
Volatile Organics Appendix 9
CV Mercury Analysis (RCRA)
GF/^ Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Sb ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Explosives Analysis
Perchlorate - Ion Chromatography
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Page 1 of 11
L5584-4 SITE B
SW-846, 8260
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SW 846, 8330 Modified
EPA 314.0
T-75
Volatile Organics Appendix 9
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Sb ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Explosives Analysis
Perchlorate • lon Chromatoaraphy
Certified By _C ^ CP^AJLJ
07/22/02
fNxh m
QC Coordinator
07/22/02 09:33
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
i.„
Uji/u^ ^&-/!«&.•
T Date
Ttiis certifies that the following samples were analyzed using good laboratory practices to show the following results:
Page 2 of 11
Listing of Results by Sample
1 Sample ID: PIT 1 WEST T-75
630-20-6
71 -55-6
79-34-5
76-13-1
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-75-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01 -6
75-69-4
108-05-4
75-01 -4
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLORO-1,2,2-
TRIFLUOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DlCHLOHOPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHL0R0PR0PANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOBOPROPANE
1,3.5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOBOPHOPANE
1,4-DICHLOBOBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-lSOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ANTIMONY
CADMIUM
CHROMIUM
LEAD
Result
U
U
U
u
u u
u u
u u
u
u u u u u u u
u u
u u
u u
u u u
u u
u u u
u u u u
u u
u u u u u u u
u u u u u u u
u
u u u 12B
u
u u u u u u
u u u
u u
-037
5.2
3-8
.61
17
U
Vnit?
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Lab ID: L5584-1 Collect Date: 07/22/02 09:08 |
MPL
.6
.6
.9
.5
.8
.4
.5
.6
-99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2-4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
1
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
6
.5
.7
.4
.5
6
.5
.3
.5
.02
1.5
25
.1
.3
1.3
Dll.
EQL Factor Methgd
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
6.4
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10
10 "
10
10
10
10
10 1
10 1
10 1
10
10
10 1
10 1
10 1
.07 1
4.3 2
13 1
.5 1
1.3 1
6.2 1
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-B46,8260
1 SW-846,8260
SW-846, 8260
SW-846, 6260
SW-846, 8260
1 SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
I SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
0 SW-846,7060
SW-B46, 6010
SW-B46, 6010
SW-846, 6010
SW-846, 6010
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
CWS
MTB
MTB
MTB
MTB
Test Date
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/0214:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/0214:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/0214:10
07/23/02 14:10
07/23/0214:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/0214:10
07/23/02 14:10
07/23/02 14:10
07/23/0214:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/0214:10
07/23/0214:10
07/23/02 14:10
07/23/0214:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/0214:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
07/23/02 14:10
08/14/02 10:50
08/08/02 11:19
08/15/02 10:13
08/15/02 10:13
08/15/02 10:13
08/15/02 10:13
Page 3 of 11
2691-41-0
55-63-0
121-82-4
SELENIUM
SILVER
ICP/GF/^A METALS DIGESTION
HMX
NITROGLYCERIN
RDX
PERCHLORATE
U
U
U
U
U
U
ug/g
ug/g
mg/kg
mg/kg
mg/kg
mg/kg
3
.2
.2
.2
.2
.1
15 1
.7 1
.2 1
.2 1
.2 1
.4 10
SW-846, 6010
SW-846, 6010
SW-846. 3050
SW 846, 8330 Modifi
SW 846, 8330 Modifi
SW 846, 8330 Modifi
EPA 314.0
MTB
MTB
MTB
JNB
JNB
JNB
CWS
08/15/02 10:13
08/15/02 1013
08/07/02 12:00
08/21/02 16:59
08/22/02 13:22
08/21/02 16:59
08/07/02 20:66
Page 4 of 11
IsamplelD: PIT 2 MID T-75
630-20-6
71-55-6
79-34-5
76-13-1
79-00-5
75-34-3
75-35-4
563-58-6
67-61 -6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-75-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01 -4
Test Psrsmeter
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-1 b 1 HACHLOROETHANE
1,1,2-TRICHLORO-I,2,2-
TRIFLUOROETHANE
1,1,2-TRI CHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ANTIMONY
CADMIUM
CHROMIUM
LEAD
SELENIUM
Result
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
13B
u
u
u
u
u
u
u
u
u
u
u
u
u
5
u
.7
21
u
u
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Lab ID: L5584-2 Collect Date: 07/22/02 09:20 |
MPL
.6
.6
.9
.5
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1 4
1.8
24
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.02
1.5
2.4
.1
.2
1.2
2.9
Dll.
EQL Factor Meth<?d.
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
6.4
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10 "
10
10
10 1
10
10 •
10 1
10
10 1
10
10
10
10 •
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10
10 1
10 1
10 1
10 1
.07 1
4.2 2
12 1
.5
1.2 1
6.1 1
15 1
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-84e, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
0 SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
CWS
MTB
MTB
MTB
MTB
MTB
Page
Test Djite
07/23/0214:48
07/23/02 14:48
07/23/02 14:48
07/23/021448
07/23/02 14:48
07/23/0214:48
07/23/02 14:48
07/23/02 14:48
07/23/02 14:48
07/23/02 14:48
07/23/02 14:48
07/23/02 14:48
07/23/02 14:48
07/23/0214:48
07/23/02 14:48
07/23/02 14:48
07/23/0214:48
07/23/02 14:48
07/23/02 14:48
07/23/0214:48
07/23/02 14:48
07/23/02 14:48
07/23/0214:48
07/23/0214:48
07/23/0214:48
07/23/0214:48
07/23/02 14:48
07/23/0214:48
07/23/0214:46
07/23/0214:48
07/23/0214:48
07/23/0214:48
07/23/0214:48
07/23/0214:48
07/23/02 14:48
07/23/02 14:48
07/23/02 14:48
07/23/02 14:48
07/23/0214:48
07/23/0214:48
07/23/0214:48
07/23/0214:48
07/23/0214:48
07/23/02 14:48
07/23/02 14:48
07/23/0214:48
07/23/0214:48
07/23/02 14:48
07/23/0214:48
07/23/02 14:48
07/23/0214:48
07/23/0214:48
07/23/02 14:48
07/23/02 14:48
07/23/0214:48
07/23A)2 14:48
07/23/02 14:48
07/23/02 14:48
07/23/02 14:48
07/23/02 14:48
07/23/02 14:48
07/23/02 14:48
07/23/02 14:48
07/23/02 14:48
07/23/02 14:48
07/23/02 14:48
07/23/02 14:48
07/23/02 14:48
07/23/02 14:48
08/14/02 10:54
08/08/02 11:33
08/15/02 10:16
08/15/02 10:16
08/15/02 10:16
08/15/02 10:16
08/15/02 10:16
5of11
2691-41-0
55-63-0
121-82-4
SILVER
ICP/GFAA METALS DIGESTION
HMX
NITROGLYCERIN
RDX
PERCHLORATE
U
U
u U
2
ug/g
mg/kg
mg/kg
mg/kg
mg/kg
.1
.2
.2
.2
.1
.7 1
.2 1
.2 1
.2 1
.4 10
SW-846, 6010
SW-846, 3050
SW 846, 8330 Modifi
SW 846, 8330 Modifi
SW 846, 8330 Modifi
EPA 314.0
MTB
MTB
JNB
JNB
JNB
CWS
08/15/0210:16
08/07/0212:00
08/21/0217:16
08/22/02 13:36
08/21/02 17:16
08/07/02 21:11
Page 6of 11
1 Sample ID: PIT 3 EAST T-75
630-20-6
71-55-6
79-34-5
76-13-1
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541 -73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-75-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
l,1.2-TRICHLORO-1,2,2-
TRIFLUOROETHANE
1,1.2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-OICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,6-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTAN0NE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBLTTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ANTIMONY
CADMIUM
CHROMIUM
LEAD
SELENIUM
Result
u
u u u
u u u u u
u
u u
u u u u u
u u
u u
u u
u u u u u
u u u u u
u
u u u u u
u u u u u
u u u u
u u
u u u
u u
u u
u u
u u u
u u
u u u u u u
5.1
4.6
.51
24
2.3
u
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L5584-3 Collect Date: 07/22/02 09:25 |
MPU
.6
.6
.9
.5
.8
.4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
2.4
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.02
1.4
2.4
.1
.2
1.2
2.9
Dil.
EQL Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
6.4
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
.07
4.1 2
12
.5
1.2
5.9
14
1 SW-846, 8260
SW-846
SW-846
1 SW-846
1 SW-846
1 SW-846
SW-846
SW-846
SW-846
SW-846
1 SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-B46
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
\ SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-B46
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
0 SW-846
SW-846
SW-846
SW-846
SW-e46
SW-846
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
7471A
7060
6010
6010
6010
6010
6010
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
CWS
MTB
MTB
MTB
MTB
MTB
Page
Test Date
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/0215:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/0215:27
07/23/02 15:27
07/23/02 15:27
07/23/0215:27
07/23/0215:27
07/23/0215:27
07/23/02 15:27
07/23/0215:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/0215:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/0215:27
07/23/0215:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23rt)2 15:27
07/23/0215:27
07/23/02 15:27
07/23/02 15:27
07/23/0215:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
07/23/02 15:27
08/14/02 11:04
08/08/02 12:10
08/15/02 10:19
08/15/02 10:19
08/15/02 10:19
08/15/02 10:19
08/15/02 10:19
7of 11
2691 -41 -0
55-63-0
121-82-4
SILVER
ICP/GFAA METALS DIGESTION
HMX
NITROGLYCERIN
RDX
PERCHLORATE
U
U
u u 11
ug/g
mg/kg
mg/kg
mg/kg
mg/kg
.1
.2
.2
.2
.1
.7 1
.2 1
.2 1
.2 1
.4 10
SW-846, 6010
SW-846, 3050
SW 846, 8330 Modifi
SW 846, 8330 Modifi
SW 846, 8330 Modifi
EPA 314.0
MTB
MTB
JNB
JNB
JNB
CWS
08/15/02 10:19
08/07/0212:00
08/21/0217:33
08/22/0213:50
08/21/02 17:33
08/07/02 21:26
Page 8 of 11
IsamplelD: SITES T-75
630-20-6
71-55-6
79-34-5
76-13-1
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
110-75-8
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71 -8
100-41-4
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061 -02-6
79-01 -6
75-69-4
108-06-4
75-01-4
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRI CH LOROETHAN E
1,1,2,2-1 b 1 HACHLOROETHANE
1,1,2-TRICHLORO-l ,2,2-
TRIFLUOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOHOBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROETHYLVINYL ETHER
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ARSENIC
ANTIMONY
CADMIUM
CHROMIUM
LEAD
SELENIUM
Result
u
U
U
U
u
U
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
5.3
28
.55
13
u
u
gtiit%
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Lab ID: L5584-4 Collect Date: 07/22/02 09:33 |
MPL
.6
.6
.9
.5
.8
4
.5
.6
.99
1.3
.6
.7
1
.8
.7
.7
.5
.6
.6
.7
.5
.6
.6
.6
.6
1.3
.5
.6
1.4
1.8
24
1.1
.5
.6
.5
.8
1
.8
.6
.7
.7
.4
.7
.3
.5
.4
1
.7
.1
.5
.5
.5
1.3
.5
.5
.7
1.2
.6
.7
.6
.6
.5
.7
.4
.5
.6
.5
.3
.5
.02
1 4
2.4
.09
.2
1.2
28
Dll.
IQL Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
6.4
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10
10
10
10 1
10 1
10 1
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
.08 1
4.1 2
12 1
.5 1
1.2 1
5.9 1
14 1
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846. 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
SW-846, 8260
1 SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846.8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-e46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7471A
0 SW-846,7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Analyst
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
CWS
MTB
MTB
MTB
MTB
MTB
Test p?te
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/0216:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/0216:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/0216:05
07/23/0216:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/0216:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/0216:05
07/23/0216:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23A)2 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
07/23/02 16:05
08/14/02 11:14
08/08/02 12:20
08/15/02 10:22
08/15/02 10:22
08/15/02 10:22
08/15/02 10:22
08/15/02 10:22
Page 9 of 11
SILVER
ICP/GFAA METALS DIGESTION
2691-41-0 HMX
55-63-0 NITROGLYCERIN
121-82-4 RDX
PERCHLORATE
u
u
u
u
u
ug/g
mg/kg
mg/kg
mg/kg
mg/kg
.1
.2
.2
.2
.1
.7 1
.2 1
.2 1
.2 1
.4 10
SW-846, 6010
SW-846, 3050
SW 846, 8330 Modifi
SW 846, 8330 Modifi
SW 846, 8330 Modifi
EPA 314.0
MTB
MTB
JNB
JNB
JNB
CWS
08/15/0210:22
08/07/02 12:00
08/21/0217:50
08/22/02 14:04
08/21/02 17:50
08/07/02 22:26
Pagel Oof 11
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected but was
below the MDL.
B Gas Chromatography and Mass Spectral Data Flag. This flag is used when an analyte is found in
the blanl< as well as the sample
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This flag is used
either when estimating a concentration for tentatively identified compounds or when the data
indicated the presence of a compound that meets the identification criteria but the result is less than
the EQL (e.g. 3 J with an EQL of 10)
MDL Method Detection Limit: The minimum concentration of a substance that can be confidently
measured and reported. The laboratory has demonstrated that the MDL can be achieved in a
laboratory reagent blank, but does not guarentee it can be achieved in ail sample matrices.
The MDL is approximateiy three times the signal noise levei.
EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many
analytes the EQL is selected as the value of the lowest standard in the calibration curve.
Dil. Factor Dilution Factor: The prepared smple was diluted by this factor because the sample was too
concentrated or due to other interferences in the sample matrix. Any dilution factor causes
an appropriate increase in the MDL and EQL.
Page 11 of 11