DSHW-2002-006054 - 0901a06880156af6

ATK
ALLiANTTECHSYSTEMS
September 20, 2002
8200-FY03-077
Dennis R. Downs
Division of Solid and Hazardous Waste
288 North 1460 West
P. O. Box 144880
Salt Lake City, Utah 84114-4880
Thiokol Propulsion Corp.
P.O. Box 707
Brigham City, UT 84302-0707
Tel [phone]
Fax [phone]
HAND DELIVERED
SEP 2 3 2002
Utah Division of Solid
. and Hazardous Waste
Subject: Response to September 3, 2002 letter regarding Compliance bvaluation "
and Operation and Maintenance Inspections (Promontory, EPA ID #
UTD009081357)
Dear Mr. Downs:
This letter is in response to your September 3'^^ letter addressing concerns observed
during the DEQ's June and July inspecfions of ATK Thiokol Propulsion's Promontory
Facility. Each issue addressed in your letter is repeated in regular text below, with
Thiokol's response in italics.
1. The Division is concerned that hazardous constituents may be released to the
environment from operations conducted at the M-136 Bum Grounds. There are
two areas in particular where it appears that hazardous constituents could be
released to the ground. The first area is the trench where the third stage
Minuteman motors are burned, and the second is the area where the gravel-filled
bum trays are located. The trench is a concern since the motors are bumed
directly on the ground, and the area around the gravel-filled bum trays is a
concern since it is evident that material that has fallen off of the tray during or
after a bum is left on the ground.
Does Thiokol have procedures in place to periodically analyze the soil in the bum
trench or the area next to the bum trays to determine if hazardous constituents are
accumulating? The Division strongly recommends Thiokol have procedures to
periodically assess the condition ofthe bum grounds. Appropriate procedures to
address this issue will be included as permit conditions upon permit issuance.
We agree that the permit that is currently being revised is the appropriate place
to address these procedures. Thiokol utilizes a Zone of Engineering Control
(ZOEC) concept to assess the condition ofthe buming grounds. The ZOEC is
described in the Subpart X permit submittal. This is to compare soil sampling
results to risk based concentrations such as the Region 9 PRG tables. (PRGs are
intended to protect direct human exposures to the soil, but are not protective of
groundwater. Included in this response are a copy ofthe results from a recent
ZOEC sampling event as well as a previous one for comparison, also, data from
in and around the gravel filled "Alliant" tray. In one example, we treated
Autoliv formulations that are high in cobalt and copper. We saw an upward
trending of a total metal analysis in an area around the tray and have since
stopped accepting these formulations. Other than these, we have not seen an
increase in hazardous constituents that would be a concern.
Associated with our concems about the release of hazardous constituents at M-
136 is the observation that perchlorate concentrations in groundwater appear to be
increasing. Monitoring data for wells adjacent to the bum grounds (wells A-4, A-
5, C-1 and A-8) indicate that perchlorate concentrations have increased
considerably since 1995 (see enclosed chart). Does Thiokol have an explanation
for the increasing perchlorate concentrations that have been observed in these
wells?
Rising perchlorate values in the cited wells are a function of past disposal
practices rather than current disposal activities. The source area for the
perchlorate in these wells was a LTTA located near well A-6. Since disposal
practices ceased in 1988, perchlorate levels have significantly declined as
contaminated groundwater has migrated down gradient from A-6 towards wells
A-4, A-5, C-1, and A-8. See the enclosed chart modified with data from A-6. It is
expected that these paired trends will continue in the future
2. The Post-Bum Cleanup and Tray Maintenance instmcfions for the M-l36 Bum
Grounds indicate that the bum trays are to be inspected for holes in the bottom of
the tray, weld cracks, side wall height, whether the trays are sitting on the ground
or not, and other conditions that might render the tray unusable. It appears that a
record of these inspection items is not maintained. Apparently the only record
kept of tray inspecfions is the "satisfactory", "unsatisfactory" or "needs
improvement" rating that appears on the Daily Waste Propellant Log. In addition,
the specific tray isn't even identified - only the Bum Stafion is recorded in the
log. The inspection items from the Process Instmctions should be included on a
checklist for the specific tray that is being inspected.
As a result ofthe State's Compliance Inspection, we are revising our Bum
Grounds procedures and inspection program to align more closely with the
State's expectations of a good management practices. Specifically, we will
modify our procedures to require tray cleaning as soon as safety allows, which is
generally the next day. End ofthe work week bums will be cleaned up the next
business day. However, any derived from trays, if not cleaned the next day, will
be covered and labeled until the tray contents can be removed and packaged for
hazardous waste disposal.
It also appears that a record of when the bum trays are cleaned out is not kept.
The Division expects bum trays will be cleaned out as soon after a bum as safety
allows. The date the trays are cleaned out and the disposition of the ash and
debris removed from the trays should be recorded. These issues need to be
addressed as a permit for the bum grounds is pursued by Thiokol.
Thiokol is currently inspecting the bum trays and recording the results on the
Daily Waste Propellant Log. Each tray is tied to a unique bum station within the
Bum Grounds. We will now number all bum trays and modify our bum record to
record all tray inspection results, tray numbers and station locations, trays not
passing inspection and removed from service, as well as all other information we
are currently tracking. All inspection results, dates, etc. will be recorded in an
electronic format which will be available for inspection by the State. We believe
these changes will address the concems you expressed in your letter.
At the M-225 Bum Grounds, it was observed that ash and debris had not been
cleaned out of the bum trays, including the "derived from" tray, since the last
bum was conducted five days prior to the inspection. The "derived from" tray is
reserved for buming reactive hazardous waste that also has a listed hazardous
waste code attached to it. Thiokol has been managing the debris that is removed
from this tray after a bum as hazardous waste and the tray is supposed to be kept
covered when not in use. At the time of the inspection, the debris in the tray
apparently included partially bumed hazardous waste, and the tray was not
covered.
M-225 has managed their reactive waste under a separate system from M-136 in
the past. We will now implement the same waste tracking and management
system at both M-136 and M-225. Implementation ofthis program at M-225
should help to correct the concems the State has at this facility.
The inspection of the M-225 Bum Grounds revealed a few problems with its
management: the trays were not cleaned out as soon after a bum as safety
allowed; partially bumed hazardous waste was not separated from ash for re-
buming; and "derived from" waste was left uncovered in the bum tray. In
addifion, it appears that records for the Bum Grounds, as discussed in issue
number two above, are not kept at M-225.
With regards to separation of hazardous waste for re-buming, ATK Thiokol has
never used this practice. Handling of partially bumed items/propellant adds
unnecessary risk to operators. If a waste requires re-buming, additional donor is
added to the tray without handling the partially bumed material, then re-bumed.
The tray you mentioned contained propellant ash from buming propellant
contaminated with acetone. The portion you suggested that was not fully bumed,
was fully reacted and was not intended to be re-bumed. Although the ash no
longer carried an F003 code because ofthe F003 exemption, it was a poor
management practice, and should have been covered. Under the revised
management procedures that will be implemented for M-225, these problems
should be corrected in the future.
Outside the machine shop at building E-517, the inspectors questioned Thiokol
personnel about three dmms that were labeled as non-hazardous waste. The
dmms contained metal machining coolant sludge that had been removed from a
bulk tank which supplied coolant for a number of machines. The non-hazardous
characterization of the waste was based on process knowledge only.
Based on the concern that heavy metals may be in the coolant sludge, the
inspectors requested Thiokol perform a laboratory analysis. The resulting
analysis indicated that metals were not a concern, however, the analysis did
identify the presence of organics. The coolant sludge is now being managed as a
hazardous waste. In order to ensure proper waste characterization and
management, the Division recommends Thiokol assess any other waste streams
that have been characterized as non-hazardous based solely on process
knowledge.
Upon receipt ofthe analytical results for the E-517 machining coolant sludge
drums, we proceeded to investigate where these trace levels of solvent could have
come from. All operators interviewed said that they had not used any ofthe
identified solvents in the past several years. Our best guess is that it may have
been trapped in the sump sludge for several years from a floor wax stripper.
Although we do not believe this material is a hazardous waste, we will handle it
as a hazardous waste as a precaution. We will also closely review all non-
hazardous waste streams, and analyze all waste which could have a potential for
containing hazardous constituents.
5. The containment sump in the floor of the 90-day hazardous waste storage dock at
the M-68 paint shop was approximately one-half full of water at the time of the
inspection. Is there a procedure in place for the removal of water from
containment sumps? The Division recommends that accumulated water be
promptly removed from sumps so that the full capacity of the sump is available in
the event of a release and so that releases of waste can be detected by observing
the sump.
All of our TSDFs have requirements in place to pump out sumps within 72 hours
or sooner if it is a threat to human health or the environment. However, other
sumps like the one at M-68, do not have a specific requirements for pumping. We
will modify GM 3.1 (Disposal Instructions for Waste Materials) to include a
requirement to promptly remove any accumulation of rain water from these
containment sumps.
6. Thiokol has warning signs posted at the entrance to the M-l86 Hazardous Waste
Storage facility as required; however, there isn't a sign on the stmcture itself that
designates the area as hazardous waste storage. In addition, there are no signs in
the storage area that designate bays by compatibility group. It seems feasible that
someone unfamiliar with the operations at the storage facility could place
containers of waste in the wrong place. The Division suggests that Thiokol posts
one or two signs on the stmcture at M-l86 to designate it £is hazardous waste
storage. It is also suggested that movable signs are made that can be used to
designate bays by compatibility group.
We will install an additional sign on building M-l86 as recommended by the
State. With regards to unfamiliar operators placing incompatible waste in the
same bay, we do not believe this is an issue for our situation. M-l 86 is a secured
area, and no waste is moved into or out ofthis site without one of the four trained
operators present. With the exception of lab packs, very few incompatibles are
ever stored in these bays, which makes it very easy to manage. Therefore, we do
not believe identification of each bay by compatibility group is necessary.
In regard to the O&M Inspection, the results of the well condition assessment are
summarized in the enclosed table. A few problems were identified as a result of the
inspection. These problems are discussed below.
1. The well apron for well A-7 has major cracks in it that could compromise the
surface seal if it is not repaired. The Division recommends that the apron for this
well be repaired.
The A-7 well apron will be repaired/ replaced this Fall as recommended.
2. The padlocks on wells F-5 and T-l could not be opened at the time of the
inspection. It is recommended that the padlocks be replaced if they can't be
fixed.
The two padlocks will be repaired or replaced this Fall as recommended.
3. Thiokol notified the Division of the status of well A-4 prior to the inspection. It is
understood that an accident occurred while Thiokol was repairing the well that
caused hardware to become lodged inside the well. Apparently, attempts to solve
the problem were unsuccessful.
Well A-4 has historically been one of the most contaminated wells at Thiokol.
Since it provides a data point for one of the most contaminated zones of the
regional aquifer, it is an important well to maintain. Monitoring data from well
A-4 will become important in the future when evaluating the degradation of
contaminants. In addition, it is an important well for monitoring groundwater
while the M-136 Bum Grounds are in operafion. It is requested that Thiokol
report to the Division options for recovering well A-4 so it can be returned to
operating status.
Options include:
1. Abandon the well with no replacement. Well A-5 is nearby, and
completed in same aquifer with similar contamination levels.
2. Abandon the well and installing new well nearby.
3. Attempt to refurbish well by:
A. Remove pump and associated piping (attempted but low
probability of success).
B. Remove piping and force old pump to the bottom ofthe
well.
C. Fish and remove PVC well casing, clean original boring,
and replace well casing
D. Use cable tool rig to pulverize casing, pump, tubing,
bentonite annular material, and clean original boring.
Replace well casing.
We would like to meet with the State to discuss these options and choose an acceptable
solution.
ATK Thiokol will work diligently to correct and address all issues idenfified by the State.
We appreciate the State's cooperation and efforts to work together with ATK Thiokol to
improved our environmental management practices. If you have any question, or need
clarificafion on any issues, I can be reached at [phone], or contact Gene Curtis at
[phone].
Sincerely,
S. E. Jew, Director
Environmental Services
Date
S95
F95
S96
F96
S97
F97
S98
F98
S99
F99
SOO
FOO
SOI
FOI
S02
A-4
NS
700
690
800
500
900
<200
1800
3100
2000
1600
1500
003
008
OOS
A-5
2270
2720
2700
3400
2700
2800
2600
2800
3200
2500
2300
3100
3700
3790
4180
C-1
<100
<100
330
500
500
1700
2700
6500
7200
4400
6000
7800
7300
6430
5790
A-8
NS
3680
NS
NS
NS
NS
NS
NS
NS
17000
13000
NS
19000
18500
NS
A-6
27130
27000
25750
34666
23000
23250
27250
27250
29440
25000
19000
22000
21000
17000
15000
Perchlorate Trend Near M-136 (Wells A-4, A-5, C-1 & A-8)
40000
35000
30000
® 15000 0.
10000
5000
|||^t.lUl<ll I bill
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•t ll'"
'J ,1
•I'Wiij-'ii
Z ^*5i^"*;^. ,4 U.-.. ^^-t'-V
S95 F95 S96 F96 S97 F97 S98 F98 S99 F99 SOO FOO SOI FOI S02
Sampling Event
-•-Well A^
-•-Well A-5
A Well C-1
-•-Well A-8
-«-Well A-6
ENVIRONMENTAL LAB WORK REQUEST
™ THIOKOL ENMRONMENTAL LABORATORY LWR No. E11901
Login No.
iavcl W<-wicoc ^
OKG.\NIZATIO.N
EXTENSION
MAILSTOE'
COST CENTER
^•7V0
WORK ORDER DATE
REPORT RESULTS TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE
' /
• ?
3.
4.
5.
6.
7.
8.
9.
10.
1 1..
12.
DATE
f'2l-oo
<^-Zi-o^
TYPE
G
X
X
c
LOCATION
i^-^t^UM^ (^5'1\
TIME
/S7^y
l^'OO
TEST REMARKS
CHAIN OF CUSTODY
RELINQUISHED BY
^\^\/iU^
DATE TIME ECE RECEIVED BY DATE TIME
t/r€A ^~7r-oo /^:^^ ^:^^^^^^'(^-:2^'^ //••
FOR LABORATORY USE 0>fLY
DATE COMPLETED DATE REPORTED Sjr.NATURZ
CERTIFICATE OF ANALYSIS
Listing of sample Information and Testing Requested
Friday, November 10, 2000
TESTED FOR Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp, UT 84322
Gene Curtis
Project: Misc. Environmental Testing
Login Number L3506
Lab No Client Number
Test Requested Description
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-3732
800-863-8080
Received CollectDate/Time
Matrix
L3506-1 1 -M-136 ALIANT TRAY ASH 09/25/00 09/21/00 15:54
SW-846
SW-846
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SOP 420
SOP 302
7740
7471A
7060
6010
6010
6010
6010
6010
3810
3050
I L3506-2 2 - EAST OF TRAY
GFAA Selenium Analysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Head Space Screen GC/MS
ICP/GFAA Metals Digestion
HPLC Analysis HMX
Perchlorate - lon Chromatography
Waste
Waste
Waste
Waste
Waste
Waste
Waste
Waste
Waste
Waste
Waste
Waste
GROUND ASH BY TRAY 09/25/00 09/21/00 15:54
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SOP 420
SOP 302
7740
7471A
7060
6010
6010
6010
6010
6010
3810
3050
GFAA Selenium Analysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Head Space Screen GC/MS
ICP/GFAA Metals Digestion
HPLC Analysis HMX
Perchlorate - lon Chromatography
Waste
Waste
Waste
Waste
Waste
Waste
Waste
Waste
Waste
Waste
Waste
Waste
Comments:
L3506-1; L3506-2
For GC/MS results see attached memo.
L3506 Hg: Recovery of MS and MSD low due to the presence of a negative matrix interference present in
the sample. All other QC acceptable. Data accepted.
L3506 As: Recovery of MS and MSD high due to the presence of a positive matrix interference present in
the sample. All other QC acceptable. Data accepted.
L3506 Ag and Pb: Recovery of the matrix spikes showed a negative interference for these elements.
Close examination of the results showed an overcorrection from the lEC's based on the high
concentration of aluminum. Samples were diluted 1:10 and rerun for these elements with acceptable
results that are reported herein, but with an increase in the MDL for these elements.
Page 1 of 4
Certified By ^^~y9U^^ {1^ /pyf^. 3^0^
Max N. Coates, QC Officer Date
Tinis certifies that ttie following samples were analyzed using good laboratory practices to show the following results:
Page 2 of 4
Listing of Results by Sample
SampI elD: 1 -M-136 ALIANT TRAY ASH LablD:L3506-1 Collect Date: 09/21/00 15:54
Test Parameter
SELENIUM
MERCURY
ARSENIC
BARIUM
CADMIUM
CHROMIUM
LEAD
SILVER
HEAD SPACE SCREEN GC/MS
ICP/GFAA METAIS DIGESTION
HMX
PERCHLORATE
Result
4.6
U
91
1.3
11
U
U
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
MDL EQL
1.1
.02
.97
.05
.1
.3
13
1.6
3.6
.05
3.2
.3
.5
1.3
67
Dil.
Factor
20
1
20
1
1
1
10
10
1
1
1
1
Method
SW-846, 7740
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3810
SW-846, 3050
SOP 420
SOP 302
Analyst
CWS
CWS
CWS
LVD
LVD
LVD
LVD
LVD
MKR
LVD
KMS
CWS
Test Date
10/30/00 16:20
10/19/00 09:56
10/30/00 13:55
10/31/00 11:31
10/31/00 11:31
10/31/00 11:31
11/03/00 14:49
11/03/0014:49
10/05/00 12:00
10/27/00 12:00
09/27/00 07:56
10/06/0012:33
IsamplelD: 2-EAST OF TRAY GROUND ASH BY TRAY Lab ID:L3506-2 Collect Date: 09/21/00 15:54 |
Test Parameter
SELENIUM
MERCURY
ARSENIC
BARIUM
CADMIUM
CHROMIUM
LEAD
SILVER
HEAD SPACE SCREEN GC/MS
ICP/GFAA METALS DIGESTION
HMX
PERCHLORATE
Result Units
Dil.
MDL EQL Factor
7.2
U
12
42
.2
12
U
U
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
1
.01
.9
.05
.1
.3
13
1.5
.5
.2
3.5
.04
3.1
.3
.5
1.3
63
7.6
20
1
20
1
1
1
10
10
1
1
1
1
Method
SW-846, 7740
SW-846, 7471A
SW-846, 7060
SW-846, 8010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3810
SW-846, 3050
SOP 420
SOP 302
Analyst
CWS
CWS
CWS
LVD
LVD
LVD
LVD
LVD
MKR
LVD
KMS
CWS
Test Date
10/30/00
10/19/00
10/30/00
10/31/00
10/31/00
10/31/00
11/03/00
11/03/00
10/05/00
10/27/00
09/27/00
10/06/00
16:27
10:00
14:02
11:37
11:37
11:37
14:52
14:52
12:00
12:00
08:27
13:02
Page 3 of 4
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected but was
below the MDL.
B Gas Chromatography and Mass Spectral Data Flag. This flag is used when an analyte is found in
the blank as well as the sample
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This flag is used
either when estimating a concentration for tentatively identified compounds or when the data
indicated the presence of a compound that meets the identification criteria but the result is less than
the EQL (e.g. 3 J with an EQL of 10)
MDL Method Detection Limit: The minimum concentration of a substance that can be confidently
measured and reported. The laboratory has demonstrated that the MDL can be achieved in a
laboratory reagent blank, but does not guarentee it can be achieved in all sample matrices.
The MDL is approximately three times the signal noise level.
EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many
analytes the EQL is selected as the value of the lowest standard in the calibration curve.
Dil. Factor Dilution Factor: The prepared smple was diluted by this factor because the sample was too
concentrated or due to other interferences in the sample matrix. Any dilution factor causes
an appropriate increase in the MDL and EQL.
Page 4 of 4
PROPULSION GROUP OoTHtOKOL
SCIENCE AND ENGINEERING AEROSPACE . INDUSTRIAL TECHNOLOGIES
P. 0. Box 707, M/S 245
Brigham City, UT 84302-0707
801 -863-3511
LWR-FY00-D1382
5 October, 2000
FROM: Kelly Richardson
LWR: El 1901
WO: 1B909
SUBJECT: Ash Samples From Alliant Tray/Ground (L3506-1 & 2)
Two samples of ash were submitted for GC/MS headspace analysis of volatile organic compounds.
One sample of ash was from the tray (L3506-1) and one from the ground on the east side of the tray
(L3506-2).
Approximately one gram of each sample was transferred into a 10-ml headspace vial and heated at
110°C for approximately twenty minutes. After heating, a 250-^il aliquot of the headspace gas was taken
and direct injected into the GC/MS.
No volatile.organic compounds were detected in either sample.
If you have any questions regarding this analysis I can be reached at extension 3216.
Kelly Richardson
Spectrochemical Analysis
DEC 05 '00 07:42AM TC PiNflLYTICftL LAB P.2/4
ooTinoiiroE PROPULSION GROUP
scieNce AND ENGiNEEniNG *e«o»Ace&.NousTWALTreHNOLo««
P.O. 80X707, MfiS 245
Srlgriain City, UT i430M707
^LWn-FY00-D1382
5 October. 2000
FROM: Kelly Hiohardson
LWR: El 1901
WO: 1B909
SUBJECT: Ash Samples From Alliant Tray/Ground (L3506-1 & 2)
Two samples of ash were submitted for GC/MS analysis of HMX. One sample of ash was from the tray
(13506*1) and one from the ground on the east side of the tray (L3506-2).
Approximately one gram of each sample was transferred into a 10-ml headspace vial and heated at
110*C for appro)(imately twenty minutes. After heating, a 260•^l aliquot of the headspace gas was taken
and direct injected into the GC/MS.
No HMX was detected in either sample.
if you have any questions regarding this analysis I can be reached at extension 3216.
Kelly Richardson
Spectrochemical Analysis
DEC 05 '00 07:42AM TC ANALYTICAL LAB P. 3/4
File : C:\HPCHEMM\DATA\L3506-1.D
Operator : mkr
Acquired ; 4 Occ 3000 2:43 pm using AccsMethod HEAD5FCE
Inscruin«nt : 2-HP71
Sample Name: Ash. From Tray
Misc Info : L3506-1
Vial dumber: 3
Abundance
1.1«+07-
1.05»+07-
16407
9500000-
9000000-
B500000-
8000000-
7500000-
7000000-
6500000-
6000000'
5500000
5000000
4500000
4000000
3500000'
3000000
2500000
2000000^
1600000'
1000000;
500000'
0-
rime->
Mr
Water
, 1.00 2.09 ?-90 'IrQP ?-09
TIC:L3506-1.0
-
1' 1 1 1 1 1 11 1 1 • 1 1 1 1 ' 1 1 1 1 1 1 1 1 1 1 11 1 1 1 1 1 1 I 1 1 1 1 1 i 1 1 1 1 1 1 1 1 < 1 1 1 1 1 i 1 1 I I 1 1 1 1 1
6.00 7.00 6.00 9.00 10.00 11.00 12.00 13.00 U.OO 15.00 16.00 17.00 18.00
_J
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ENVIRONMENTAL LAB WORK REQUEST
'° THIOKOL ENVIRONMENTAL LABORATORY LWR No.
Login No.
E11999
DM: .
3?<y^
COSr CENTEH WORK OKDEH
IBIO'I H ?o-o/
OkGANlZA.T10N
St/VVjtVonMQ.</v7kj^-3g/
RliPOHT RESULI S TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE
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REMARKS
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CHAIN OF CUSTODY
RELINQUISHED BY
''^^Sv'ty(jA£6tyi^
DATE
"^^20-01
TIME
/a: /(
RECEIVED BY
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DATE
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FOR LABORATORY USE ONLY
iMIEt-OMl'LKTEl) DATE REI'OUTF.D SIGNATURE
CERTIFICATE OF ANALYSIS
Listing of sample Information and Testing Requested
Wednesday, September 26, 2001
TESTED FOR ATK Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp, UT 84322
Paul Hancock
Project: Misc. Environmental Testing
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-3732
800-863-8080
Login Number L4449
Lab No Client Number
Test Requested
Received
Description
CollectDate/Time
l\/latrix
I L4449-1 M-136 10-4 08/20/01 08/16/01 13:46
6010
6010
Tfiiol<ol SOP 30
SW-846, 8260
SW-846, 7471A
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,
SW-846,
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 420
Metals Analysis by Flame AE
Volatile Organics
CV Mercury Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Cd ICP Metais Analysis (RCRA)
Ba ICP Metais Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Mo iCP Metals Analysis (RCRA)
Sb iCP Metals Analysis (RCRA)
Pb iCP Metals Analysis (RCRA)
Se iCP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Co ICP Metals Analysis (RCRA)
iCP/GFAA Metals Digestion
HPLC Analysis HMX
HPLC Analysis for NG
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
I L4449-2 M-136 67-3 08/20/01 08/16/01 15:00
TIniokol SOP 30
SW-846, 8260
SW-846, 7471A
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 420
Metals Analysis by Flame AE
Volatile Organics
CV Mercury Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Cd iCP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Mo ICP Metals Analysis (RCRA)
Sb ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Co ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
HPLC Analysis HMX
HPLC Analysis for NG
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
^as:e 1 of 29
L4449-3 M-136 71-9 08/20/01 08/16/01 15:27
Tfiiokol SOP 30
SW-846, 8260
SW-846, 7471A
SW-846, 6010
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 420
6010
6010
6010
,6010
6010
6010
,6010
Metals Analysis by Flame AE
Volatile Organics
CV Mercury Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Mo ICP Metals Analysis (RCRA)
Sb ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Co ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
HPLC Analysis HMX
HPLC Analysis for NG
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L4449-4 M-136 50-3 08/20/01 08/16/01 15:38
Thiokol SOP 30
SW-846, 8260
SW-846, 7471A
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 420
Metals Analysis by Flame AE
Volatile Organics
CV Mercury Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Mo ICP Metals Analysis (RCRA)
Sb ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Co ICP Metals Analysis (RCRA)
ICP/GF/\A Metals Digestion
HPLC Analysis HMX
HPLC Analysis for NG
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L4449-5 M-136 98-3 08/20/01 08/16/01 15:53
Thiokol SOP 30
SW-846, 8260
SW-846, 7471A
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 420
Metals Analysis by Flame AE
Volatile Organics
CV Mercury Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Mo ICP Metals Analysis (RCRA)
Sb ICP Mstals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Co ICP Metals Analysis (RCRA)
ICP/GF/^ Metals Digestion
HPLC Analysis HMX
HPLC Analysis for NG
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L4449-6 M-136 21-2 08/20/01 08/16/01 16:03
Thiokol SOP 30
SW-846, 8260
SW-846, 7471A
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 420
Metals Analysis by Flame AE
Volatile Organics
CV Mercury Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Mo ICP Metals Analysis (RCRA)
Sb ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Co ICP Metals Analysis (RCRA)
ICP/GFAA Metals D:ges1ion
HPLC Analysis HMX
HPLC Analysis for NG
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soi!
Soil
Soil
1129
L4449-7 M-13619-5 08/20/01 08/20/01 09:52
Thiokol SOP 30
SW-846, 8260
SW-846, 7471A
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 420
Metals Analysis by Flame AE
Volatile Organics
CV Mercury Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Mo ICP Metals Analysis (RCRA)
Sb ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Co ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
HPLC Analysis HMX
HPLC Analysis for NG
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L4449-8 M-136 33-7 08/20/01 08/20/01 10:04
Thiokol SOP 30
SW-846, 8260
SW-846, 7471A
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 420
Metals Analysis by Flame AE
Volatile Organics
CV Mercury Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Mo ICP Metals Analysis (RCRA)
Sb ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Co ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
HPLC Analysis HMX
HPLC Analysis for NG
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L4449-9 M-136 DISPERSION 08/20/01 08/20/01 10:23
Thiokol SOP 30
SW-846, 8260
SW-846, 7471A
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 420
Metals Analysis by Flame AE
Volatile Organics
CV Mercury Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Mo ICP Metals Analysis (RCRA)
Sb ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Co ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
HPLC Analysis HMX
HPLC Analysis for NG
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L4449-10 M-136 BKG 08/20/01 08/20/01 10:35
Thiokol SOP 30
SW-846, 8260
SW-846, 7471A
SW-846, 6010
SW-846, 6010
SW-e46, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 60 iO
SW-846, 3050
SOP 420
SOP 420
Metals Analysis by Flame AE
Volatile Organics
CV Mercury Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Mo ICP Metals Analysis (RCRA)
Sb ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Co ICP MptqIs Analyt,is (HCRA)
ICP/G: AA Metals DiOf-stion
HPi C Analysis HMX
HPl C A-ilyslsforNG
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Pige 3u; 29
L4449-11 M-136 55-8
Thiokol SOP 30
SW-846, 8260
SW-846, 7471A
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-845, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 420
L4449-12 M-136 75-8
Metals Analysis by Flame AE
Volatile Organics
CV Mercury Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Mo ICP Metals Analysis (RCRA)
Sb ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Co ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
HPLC Analysis HMX
HPLC Analysis for NG
08/20/01 08/16/01 15:10
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
08/20/01 08/16/01 15:30
Thiokol SOP 30 Metals Analysis by Flame AE Soil
SW-846,8260 Volatile Organics Soil
SW-846, 7471A CV Mercury Analysis (RCRA) Soil
SW-846,6010 Ag ICP Metals Analysis (RCRA) Soil
SW-846, 6010 Ba ICP Metals Analysis (RCRA) Soil
SW-846, 6010 Co ICP Metals Analysis (RCRA) Soil
SW-846,6010 Mo ICP Metals Analysis (RCRA) Soil
SW-846, 6010 Pb ICP Metals Analysis (RCRA) Soil
SW-846,6010 Se ICP Metals Analysis (RCRA) Soil
SW-846, 6010 Sb ICP Metals Analysis (RCRA) Soil
SW-846, 6010 Cu ICP Metals Analysis (RCRA) Soil
SW-846, 6010 Cr ICP Metals Analysis (RCRA) Soil
SW-846,6010 Cd ICP Metals Analysis (RCRA) Soil
SW-846,3050 ICP/GFAA Metals Digestion Soil
SOP 420 HPLC Analysis HMX Soil
SOP 420 HPLC Analysis for NG Soil
Comments:
L4449 Hg: Recovery for MS and MSD sliglntly low due to the presence of a negative matrix interference
present in the sample. All other QC acceptaiale.
L4449 Metals 6010: The results for these samples show that they are nonhomogeneous. There also
appears to be slight interferences (negative) for lead which would likely require GFAA analysis to resolve.
Interferences for molybdenum (positive) and silver (negative) were resolved
L4449 Cs: The samples were analyzed by ICP-MS. Post digestion spikes were used. All QC acceptable.
Data accepted.
Certified By W o-*---^
QC Coordinatol-(j Date
This certifies that the following samples were analyzed using good laboratory practices to show the following results:
Z"=?-5&PT-2»® I
Page A . f :-l9
Listing of Results by Sample
1 Sample IC
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61 -6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541 -73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71 -8
100-41-4
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01 -4
: M-136 10-4
Test Parameter
CESIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBHOMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-GHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METH YL-2-PENTANON E
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENECHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ANTIMONY
BARIUM •
CADMIUM
f: :ROMIUM
COBALT
COPPER
ResMit
27.35
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u u u u u u
u u u u u u u 11
u u
u u u u
u u u u u u u 3.8
u
u u
u u u
u u
u u u u u u u u u u u u u u u u
u u 33
65
.7
12
721
910
Units MDL
ug/g .:
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g .0
ug/g 2.
iig/g .0
ug/g
ug/g
ug/g
ug/g
Lab ID: L4449-1 Collect Date: 08/16/01 13:46 |
Dil.
EQL Factor Method
1 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 •
10
10
10 -
10
10
10
10
10
50
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
1 10
1 10
1 10
10
10
1 10
10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 .04
6 13
5 3
1 .Ij
3 1 •;
1 '^
1 .U
Thiokol SOP 30
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 7471A
1 SW-846,6010
1 SW-846,6010
1 SW-846, 6010
1 SW-846, 6010
,SW-B46, 6010
1 ,SW-846, 6010
Analyst
CWS
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
LVD
LVD
LVD
LVD
LVD
LVD
Page
Test Date
09/25/01 12:00
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
08/28/01 17:50
09/10/01 13:03
09/17/01 13:35
09/17/01 13:35
09/17/01 13:35
r:9/17.'01 13:35
09/17/01 13:35
09/17/01 n?5
5 Of 29
LEAD
MOLYBDENUM
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
HMX
NITROGLYCERIN
U
7
U
U
U
U
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
1.3
.2
3.1
.2
.5
.5
6.5
.8
16
.8
.5
.5
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 420
LVD
LVD
LVD
LVD
LVD
KMS
KMS
09/17/01 13:35
09/17/01 13:35
09/17/01 13:35
09/17/01 13:35
09/14/01 12:00
08/31/01 12:13
08/31/01 12:13
'age 6 of 29
1 Sample IC
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591 -78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71 -43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01 -4
: M-136 67-3
Test Parameter
CESIUM
1,1,1,2-1 b 1 RACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-1 k 1 RACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DiCHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-Di CHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M, P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
IblRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ANTIMONY
BARIUM
CADMIUM
P' RC'.'IUM
Cf-BALF
Cf PPER
LEAD
MOI .BDENUM
Result
3.03
U
U
U
U
u
u
u
u
u
u
u u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u u
u
u
u
u
u
u
u u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
.016
u
98
.35
13
8.1
i3
1.7
U
Units MDL
ug/g .:
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg
ug/kg
ug/kg
ug/kg 1
ug/kg 1
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg 1
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g .0
ug/g 2.
ug/g .0
ug/g 0
ug/g
ug/g .0
ug/g 0
ug,'g 1
ug/;j
Lab ID: L4449-2 Collect Date: 08/16/01 15:00 |
Dil.
EQL Factor Method
1 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10 1
10 1
10 -
10
10
10
10 1
50
10
50
10
10
50
10
10
10
1 10
10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
10
10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 .04
3 11
5 .2
9 .5
2 1.1
9 .5
9 5
1 5.6
1 .7
Thiokol SOP 30
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-e46, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 7471A
1 SW-846, 6010
1 SW-846,6010
1 SW-846, 6010
1 ''.W-846, 6010
1 3W-846, 6010
1 SW-816,6'.JiO
1 SW-B^O, 6010
; SW-816, 6010
Analyst
CWS
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
LVD
LVD
LVD
LVD
LVD
LVD
Lvn
LVD
Parjr
Test Date
09/25/01 12:00
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
06/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
03/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
08/28/01 18:23
09/10/01 13:07
09/17/01 13:47
09/17/01 13:47
09/17/01 13:47
09/17/01 13: V
09/1/.-' 13:17
"19/1:. •! 13 ;7
IJ9/1//01 1' !7
09/17/01 1. 17
7c'?.9
SELENIUM
SILVER
ICP/GF/V^ METALS DIGESTION
HMX
NITROGLYCERIN
4.2
U
U
U
ug/g
ug/g
ug/g
ug/g
2.7
.1
.5
.5
14
.7
.5
.5
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 420
LVD
LVD
LVD
KMS
KMS
09/17/01 13:47
09/17/01 13:47
09/14/01 12:00
08/31/01 12:48
08/31/01 12:48
P;ige .129
1 SamplelD
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61 -6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541 -73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
: M-136 71-9
Test Parameter
CESIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-Tb 1 RACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPAN E
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METH YL-2-PENTANON E
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHAN E
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ANTIMONY
BARIUM
CADMIUM
OHRr.WIUM
COBALT
C-OP"ER
LEAL
MOLYvSni ;.' M
Result
2.26
U
U
U
U
U
U
u
u u u u
u u
u u
u u
u u
u u u u u
u u u 8.6
u
u u
u u u
u u u u u
u u
u u u u u u u u
u u u u u u
u u
u u u
u u u u u
u u u 3.9
60
78
^r
,6
:^9
U
U
Units MDL
ug/g .3
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g .0
ug/g 2
ug/g .0
ug/g .0
iig/M
ug/y .0
ug/q .0
ug/g
ug/g
Lab ID: L4449-3 Collect Date: 08/16/01 15:27 |
Dil.
EQL Factor Method
1 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10
10
10
10
50
10
50
10
10
50
10
10
10
10
10
10
10
10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 .04
1 10
4 ,2
8 .4
: 1
8 .4
.4
5.2
.6
Thiokol SOP 30
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-e46,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-B46, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846.8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 7471A
1 SW-846, 6010
1 SW-846, 6010
1 SW-846, 6010
1 .-W 346. 60^0
1 SW-846. 6010
1 SW 846, coin
1 SW-b46, lOlO
1 P,W;"'.6, R010
Analyst
CWS
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
LVD
LVD
LVD
LVD
LVD
LVD
LVD
\.VD
Test Date
09/25/01 12:00
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
08/28/01 18:55
09/10/01 13:12
09/17/01 13:50
09/17/01 13:50
09/17/01 13:50
(..•17/01 13 SO
O'..'17/Ol 13:^0
oy, 17/01 13:50
09/17/01 13:50
09/17/01 13:50
Page 9 of 29
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
HMX
NITROGLYCERIN
u
u
u
u
ug/g
ug/g
ug/g
ug/g
2.5
.1
.5
.5
12
.6
.5
.5
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 420
LVD
LVD
LVD
KMS
KMS
09/17/01 13:50
09/17/01 13:50
09/14/01 12:00
08/31/01 12:57
08/31/01 12:57
Page lOo: 29
1 Sample IC
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41 -4
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01 -4
: M-136 50-3
T^st Parameter
CESIUM
1,1,1,2-1 b rRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOHOETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON IbrRACHLOHIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M, P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ANTIMONY
BARIUM
CADMIUM
CHROMIUM
COBALT
coprcR LEAD
MOLYBDENl;M
Result
1.3
U
U
U
U
U
U
u
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u u
u
u
u
u
u
u
u
u
u u
u
u u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u u
u
u u
u
u
u
u 6.1
.3
1.2
7i:i
70
u
u
Units MDL
ug/g .:
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g .0
ug/g 2.
ug/g .0
ug/g
ug/''
ug/T
ug/g
ug/g 1.
ug/g
Lab ID: L4449-4 Collect Date: 08/16/01 15:38 |
Dil.
EQL Factor Method
1 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10 -
10
10
10
10 1
10 1
10
10
10
10
50
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 .04
5 13
5 .3
1 5
3 1.3
1 5
1 .5
3 6.4
2 .8
Thiokol SOP 30
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-B46, 8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 7471A
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SV/-846, 601C
1 SW-846, 601'.J
1 SW-846, 60 n
1 SW.846, 6010
1 .-W-.146, 6010
Analyst
CWS
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
LVD
LVD
LVD
LVD
LVD
LVL-
LVD
LVD
Page
Test Date
09/25/01 12:00
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
08/28/01 19:28
09/10/01 13:21
09/17/01 13:53
09/17/01 13:53
09/17/01 13:53
09/17.-01 13:53
09/17/01 13:53
09/17/01 13:53
09/17/01 13:53
09/17/01 13:53
11..f29
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
HMX
NITROGLYCERIN
u
u
u
u
ug/g
ug/g
ug/g
ug/g
3.1
.2
.5
.5
15
.8
.5
.5
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 420
LVD 09/17/01 13:53
LVD 09/17/01 13:53
LVD 09/14/01 12:00
KMS 08/31/01 13:06
KMS 08/31/01 13:06
Page 12oi 20
1 Sample IC
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01 -4
: M-136 98-3
Test Parameter
CESIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-1 b rRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENECHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
IblRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ANTIMONY
BARIUM
CADMIUM
CHROMIUM
COBALT
Cnpprq
LEAD
MT^i.YBUrNL'.--
Result
8.85
U
U
U
U
U
U
U
U
U
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
16
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
6.5
77
.51
13
290
717
14
: 3
Units MDL
ug/g .:
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g .0
ug/g 2.
ug/g .0
uq/q
ug/g
ug/g
ug-'g
ug/g 1
.-'j/g
Lab ID: L4449-5 Collect Date: 08/16/01 15:53 |
Dil.
EQL Factor Method
1 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
50 1
10
1 50
10
10
50
10
10
10
1 10
1 10
1 10
1 10
10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 .04
4 12
5 .2
1 .5
2 ^.y
•\ c.
1 .5
2 6
1 .7
Thiokol SOP 30
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
SW-846, 8260
1 SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 7471A
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 GV 84H 6010
1 SW-8.'-6, 60i0
: • W ^ -6, 6^..0
1 .'JW-a46,60'0
1 sw-a-:6, erio
Analyst
CWS
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
LVD
LVD
LVD
L\'D
LVD
LVD
LVD
LVD
l^cige
Test Date.
09/25/01 12:00
06/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
08/28/01 20:01
09/10/01 13:28
09/17/01 13:56
09/17/01 13:56
09/17/01 13:56
09/17/01 13-56
-09/1/,01 13:56
O9./17'01 15.56
09/17.'01 13.56
i;9/i7/ni i^-se
13of 29
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
HMX
NITROGLYCERIN
u
u
u
u
ug/g
ug/g
ug/g
ug/g
2.9
.1
.5
.5
15
.7
.5
.5
SW-846, 6010
SW-e46, 6010
SW-846, 3050
SOP 420
1 SOP 420
LVD 09/17/01 13:56
LVD 09/17/01 13:56
LVD 09/14/01 12:00
KMS 08/31/01 13:14
KMS 08/31/01 13:14
.'aget-lof ?'•
IsamplelD: M-13621-2
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
Test Parameter
CESIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-1 b 1HACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPHOPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ANTIMONY
BARIUM
CADMIUM
CriOMIUM
COBALT
CC-.'PER
LEAD
MOLYBDEr-UM
Result
4.14
U
U
U
U
U
U
U
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
69
.5
2b
152
326
8
8.1
Units MDL
ug/g .:
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g .0
ug/g 2.
ug/g .0
ug'g -0
u5-';i
ug/g .0
ug/g .0
ug/g
ug/g
Lab ID: L4449-6 Collect Date: 08/16/01 16:03 |
Dil.
EQL Factor Method
1 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10
10 1
10
10
10
10
10
50
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
1 10
10
1 10
1 10
1 10
10
10
10
1 10
1 10
1 10
1 10
1 10
1 10
10
10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 .04
1 10
4 .2
8 .4
2 1
a .4
B .4
1 5.2
1 6
Thiokol SOP 30
SW-846, 8260
SW-846, 8260
SW-646, B260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-B46,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 7471A
1 SW-846,6010
1 SW-846, 6010
1 SW-8<16,6010
1 ,=;W-846, fOiO
1 SW 846, 6010
1 SW-845, 6010
1 SW-846, 6010
1 SW-846, 6010
Analyst
CWS
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
LVD
LVD
LVD
' VD
LVD
LVD
LVD
LVC
Page
Test Date
09/25/01 12:00
08/28/01 20:33
08/28/01 20:33
08/26/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
08/28/01 20:33
09/10/01 13:35
09/17/01 13:59
09/17/01 13:59
09/17/01 13:59
01/17/01 13-^0
09/17/.;.) I.'l .9
UJ/17-J1 1? -,9
09/17'01 13 50
J9/IV;0I 13 69
T5of 29
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
HMX
NITROGLYCERIN
u
u
u u
ug/g
ug/g
ug/g
ug/g
2.5
.1
.5
.5
12
.6
.5
.5
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 420
LVD 09/17/01 13:59
LVD 09/17/01 13:59
LVD 09/14/01 12:00
KMS 08/31/01 13:23
KMS 08/31/01 13:23
fag., tGof 29
1 Sample IC
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
: M-136 19-5
Test Parameter
CESIUM
1,1,1,2-1 b 1 HACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON IblHACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DiCHLOROETHENE
CIS-1,3-DICHLOROPROPENE
Dl BROMOCHLOROMETHAN E
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ANTIMONY
BARIUM
CADMIUM
CHROM:UM
CO;":ALI
CO.. 'EH
LEAD
MOLYDiJtWUM
ResMlt
7.81
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u u
u
u
u
u u
u
u
u
u u
u
u u
u
u
u
u
u
u
u u
u
u
u
u 74
2
28
;i50
,420
u 1.3
ynits MDL
ug/g .:
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg 1
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g .0
ug/g 2.
ug/g .0
ug/g
ug/g
ug/g
ug/g
ug/g 1 -
'.'a/&
Lab ID: L4449-7 Collect Date: 08/20/01 09:52 |
DM.
EQL Factor Method
1 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10
10 1
10 1
10
50
10
50 1
10
10
50
10
10
10
10
1 10
10
10
10
10
1 10
10
10
10
10
10
10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 .04
5 12
5 ,2
1 .5
2 1.2
1 .5
1 .5
2 62
1 7
Thiokol SOP 30
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 7471A
1 SW-846, 6010
1 SW-846, 6010
1 SW-846, 6010
1 SW-84R, 6010
1 S'V-84.-, 601..-1
! S\.V-846, 60M
: SW-846, 6010
S'V-846, 6010
Analyst
CWS
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
LVD
LVD
LVD
LVD
LVD
..VD
LVD
LVD
Test Date
09/25/01 12:00
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
06/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21 ;06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21:06
08/28/01 21 ;06
08/28/01 21:06
08/28/01 21:06
09/10/01 13:40
09/17/01 14:02
09/17/01 14:02
09/17/01 14:02
00/17/01 1 -1 02
09/"-/01 :4.02
09/1-701 1102
09, i//01 14:C2
Pl/17,'."i 14;C2
17of2.-9
SELENIUM
SILVER
ICP/GF/iA METALS DIGESTION
HMX
NITROGLYCERIN
U
U
5.44
U
ug/g
ug/g
ug/g
ug/g
3
.1
.5
.5
15
.7
.5
.5
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 420
LVD
LVD
LVD
KMS
KMS
09/17/01 14:02
09/17/01 14:02
09/14/01 12:00
08/31/01 13:32
08/31/01 13:32
Pagn 18uf 29
ISamplelD
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61 -6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541 -73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591 -78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01 -4
: M-136 33-7
Test Parameter
CESIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-THICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENECHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
IblRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ANTIMONY
BARIUM
CADMIUM
CHROMIUM
COGALT
COPPER
LEAD
MCI.V BDENUM
Result
69.95
U
U
U
U
U
U
U
U
U
U
U
u u u u u
u u
u u u u u
u u
u u
u u u u u u u
u u u u u u
u u u u u
u u u u u
u u u
u u u u u u u
u u u u u u u u
u 28
.2
H3
539
lo'^o
u 8
Units MDL
ug/g .:
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg
ug/kg
ug/kg 1
ug/kg 1
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g .0
ug/g
ug/g .0
ug/g
ug.'g
ug/g
u...g
ug/g 1.
'-yg
Lab ID: L4449-8 Collect Date: 08/20/01 10:04 |
Dil.
EQL Factor Method
1 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10
10
10
10
10
50
10
50
10
10
50
10
10
10
10
10
10
10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 .04
3 15
6 .3
1 6
3 1 :3
1 .6
1 .'.>
5 7.5
3 .9
Thiokol SOP 30
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 7471A
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 S •'84.', 5010
1 SW-846, 601U
1 SW846, 601C
1 SW-846, 6010
1 SW 846, 6010
Analyst
CWS
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
LVD
LVD
LVD
L-.'D
LVO
LVD
LVD
LVD
Test Date
09/25/01 12:00
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
08/28/01 21:38
09/10/01 13:50
09/17/01 14:05
09/17/01 14:05
09/17/01 14:05
C9/17/01 ;4:C5
09/17/01 14:05
09/17/01 14:05
09/17/01 14:05
09/17/01 14:05
.9o' 29
SELENIUM
SILVER
ICP/GF/V\ METALS DIGESTION
HMX
NITROGLYCERIN
16
U
4.46
U
ug/g
ug/g
ug/g
ug/g
3.6
.2
.5
.5
18
.9
.5
.5
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 420
LVD
LVD
LVD
KMS
KMS
09/17/01 14:05
09/17/01 14:05
09/14/01 12:00
08/31/01 13:41
08/31/01 13:41
Page ?0of 29
1 Sample ID
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541 -73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
76-69-4
108-05-4
75-01-4
: M-136 DISPERSION
Test Parameter
CESIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOHOPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENECHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ANTIMONY
BARIUM
CADMIUM
c; iRc:-.i. .iM
COBALT
COPPE;^
LEAD
MOLYBOENLIM
Result
3.11
U
U
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u u
u
u
u
u
u
u
u
42
91
1.4
25
20
33
11
2.8
Units MDL
ug/g .3
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g .0
ug/g 2.
ug/g .0
ug/g .0
uo.'g
uy.-j .0
ug/g .0
ug/g
ug/g
Lab ID: L4449-9 Collect Date: 08/20/01 10:23 |
DM.
EQL Factor Method
1 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10
10
50
10 -
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
1 10
10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
2 .05
1 10
4 .2
8 .4
? 1
8 .•!
8 .4
1 5.2
1 F
Thiokol SOP 30
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 7471A
1 SW-846, 6010
1 SW-846, 6010
1 SW-846, 6010
1 SV.'84G, r>01f
1 SV---84C, 6010
1 SW 846, 6010
! SW-846, 6010
1 ?.:'•' ':"•. snir;
Analyst
CWS
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
LVD
LVD
LVD
L^'D
L>'D
LVD
LVD
LVD
Test Date
09/25/01 12:00
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22.11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/26/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
08/28/01 22:11
09/10/01 13:54
09/17/01 1408
09/17/01 1408
09/17/01 14:08
09/: 7/01 1408
09/17/01 14:08
09/^7/01 14i;;6
09/17/01 14:C8
09/17/01 14:08
P.ge2iof 29
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
HMX
NITROGLYCERIN
u
u
u
u
ug/g
ug/g
ug/g
ug/g
2.5
.1
.5
.5
13
.6
.5
.5
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
1 SOP 420
LVD 09/17/01 14:08
LVD 09/17/01 14:08
LVD 09/14/01 12:00
KMS 08/31/01 13:50
KMS 08/31/01 13:50
P^;- 22 t ?.":
1 Sample IC
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
: M-136 BKG
Test Parameter
CESIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-1 b 1 HACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ANTIMONY
BARIUM
CADMIUM
CHRCIIUM
COBALT
COI':'ER
LEAD
MOL'^BDENUM
Besyit
3.61
U
U
u u u u u u
u u
u u u
u u
u u
u u
u u u u u
u u
u u u u u
u u u
u u u u u u u
u u u
u u u u u
u u u
u u u u u
u u u
u u
u u u
u u
u 4.2
119
1
?.'•
12
ir.
10
u
Units MDL
ug/g .:
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g .0
ug/g 3.
ug/g .0
ug/g
•g/g
•g/g
'-a/g
ug/g 1.
ug/g
LablD:L4449-10 Collect Date: 08/20/01 10:35 |
Dil.
EQL Factor Method
1 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10
10 -
50
10
50
10
10
50
10
10
10
10
10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 .04
1 15
6 .3
1 .6
3 ' -^
1 6
1 .6
5 7.7
2 .9
Thiokol SOP 30
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 7471A
1 SW-B46, 6010
1 SW-846, 6010
1 SW-846,6010
•_',v-p;6, "010
1 SWo46, .010
SW.346, :.010
1 SWd46, 6010
1 SV-/ )46, i.QIC
Analyst
CWS
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
LVD
LVD
LVD
LVD
LVD
1 VD
LVD
LVD
Test Date
09/25/01 12:00
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
Oa/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
08/28/01 22:43
09/10/01 13:59
09/17/01 14:11
09/17/01 14:11
09/17/01 14:11
09/" ^.'O: 14:11
09,'-7/01 14.11
09/://01 14:11
09/17/01 14:11
09/17/01 14:11
r.jge23oi29
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
HMX
NITROGLYCERIN
u
u
u
u
ug/g
ug/g
ug/g
ug/g
3.7
.2
.5
.5
18
.9
.5
.5
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 420
LVD
LVD
LVD
KMS
KMS
09/17/01 14:11
09/17/01 14:11
09/14/01 12:00
08/31/01 13:58
08/31/01 13:58
PaQ'?2 lof 29
IsamplelD
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71 -8
100-41-4
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91-20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
: M-136 55-8
Test Parameter
CESIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON IbTRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENECHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ANTIMONY
BARIUM
CADMIUM
C;:ROMIUM
C-3BALT
LOPPCR
LEAD
MOLYBDr•^lU^.1
Result
4.56
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u u u u
u u u
u u
u u u
u u
u u u
u u
u u
u u u
u u
u u u
u u u
u u u
u u u u u
u u
u u u u u u
u u
u u u u 3.6
86
1.2
:-A
,11
2y
10
u
Units MDL
ug/g .3
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg
ug/kg
ug/kg
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g .0
ug/g 3.
ug/g .Ol
ug/g
ug.'n
ug/l.
ug/y
ug/g 1.
ug/g
LablD:L4449-11 Collect Date: 08/16/01 15:10 |
Dil.
EQj. Factor Method
1 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10
10
10
50
10
50
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
1 10
1 10
1 10
1 10
10
10
10
1 10
1 10
1 10
1 10
1 .04
1 15
B .3
1 1
1
1
5 7
?
6
5
H
6
B
Thiokol SOP 30
SW-846,
SW-846,
SW-846,
SW-B46,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
SW-846, 8260
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
8260
8260
8260
8260
8260
SW-846, 8260
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
1 SW-846
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
1 SW-846,8260
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
8260
8260
8260
8260
8260
8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW-846
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
1 SW-846,8260
1 SW-846,8260
1 SW-846
1 SW-846
8260
8260
1 SW-846,8260
1 SW-846
1 SW-846
1 SW-846
8260
8260
8260
1 SW-846,8260
1 SW-846,8260
1 SW-846 8260
1 SW-846,8260
1 SW-846
1 SW-846
1 SW-846
1 SW-846
1 SW :i6
1 .SW .246
; SV-..-846
1 SW-846
1 S'V-846
7471A
6010
6010
6010
S010
6010
6010
6010
60 :0
Analyst
CWS
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
LVD
LVD
LVD
LVD
i VD
1 \ID
. VD
1 VD
Test Date
09/25/01 12:00
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/0123:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
08/28/01 23:15
09/10/01 14:03
09/17/01 14:29
09/17/01 14:29
09/17/01 14:29
09/17/01 14:''9
09/17/01 14' 9
09/17/1,1 K 9
09/17/01 1" i
09/17/01 ' 9
l-..go:15of 29
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
HMX
NITROGLYCERIN
u
u
u u
ug/g
ug/g
ug/g
ug/g
37
.2
.5
.5
18
.9
.5
.5
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 420
LVD
LVD
LVD
KMS
KMS
09/17/01 14:29
09/17/01 14:29
09/14/01 12:00
08/31/01 14:07
08/31/01 1407
P....g(^26c-f 2P
{Sample IC
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
107-02-8
107-13-1
71 -43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71 -8
100-41-4
87-68-3
98-82-8
1330-20-7
75-09-2
104-51-8
103-65-1
91 -20-3
1330-20-7
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
: M-136 75-8
lest Parameter
CESIUM
1,1,1,2-1 b 1 HACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-1 b 1 HACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOHOPROPANE
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
ACROLEIN
ACRYLONITRILE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON DISULFIDE
CARBON Ibl HACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
Tb1RACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL ACETATE
VINYL CHLORIDE
MERCURY
ANTIMONY
BARIUM
CADMIUM
CMRCMi: -A
CCBALT
Cl.'PPEU
LEAD
MOLYBPENL'M
Result
20.16
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
18
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
5.8
86
.8
23
35
73
U
U
Units MDL
ug/g .C
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg 1
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/g .0
ug/g 2
ug/g .0
ug/g
utj.'g
ug-'g
ug..g
ug/g 1
ug-'Q
LablD:L4449-12 Collect Date: 08/16/01 15:30 |
DM.
EQL Factor Method
1 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10
10
10
50
10
50
10
10
50
10
10
10
10
10
10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 10
1 .04
6 13
5 .3
1 .5
3 1.3
'. .5
.5
:i 6.5
?. .8
Thiokol SOP 30
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 7471A
1 SW-846,6010
1 SW-846, 6010
1 SW-846, 6010
1 SV-.-84C 6010
1 .r/-'-^, 6C10
1 bW-846, 6010
1 SW-846, 6010
1 ;'.W-84G, 6010
Analyst
CWS
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
LSH
CWS
LVD
LVD
LVD
I.VD
•/r
• '/!•
i.7C
. 1/
Test Date
09/25/01 12:00
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
08/28/01 23:48
09/10/01 14:08
09/17/01 14:40
09/17/01 14:40
09/17/01 14:40
. . .//Ol i,':40
• - n^ i-Mo
O:-. 01 1'i:40
Oa/:-01 14:40
09/1/01 14:40
Page 27of 29
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
HMX
NITROGLYCERIN
u u
u u
ug/g
ug/g
ug/g
ug/g
3.1
.2
.5
.5
16
.8
.5
.5
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 420
LVD
LVD
LVD
KMS
KMS
09/17/01 14:40
09/17/01 14:40
09/14/01 12:00
08/31/01 14:16
08/31/01 14:16
Page 28 of 29
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected but was
below the MDL.
B Gas Chromatography and Mass Spectral Data Flag. This flag is used when an analyte is found in
the blank as well as the sample
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This flag is used
either when estimating a concentration for tentatively identified compounds or when the data
indicated the presence of a compound that meets the identification criteria but the result is less than
the EQL (e.g. 3 J with an EQL of 10)
MDL Method Detection Limit: The minimum concentration of a substance that can be confidently
measured and reported. The laboratory has demonstrated that the MDL can be achieved in a
laboratory reagent blank, but does not guarentee it can be achieved in all sample matrices.
The MDL is approximately three times the signal noise level.
EQL Estimated Quantitation Limit: The EQL generally is 5 to 10 times the MDL. For many
analytes the EQL is selected as the value of the lowest standard in the calibration curve.
Dil. Factor Dilution Factor: The prepared smple was diluted by this factor because the sample was too
concentrated or due to other interferences in the sample matrix. Any dilution factor causes
an appropriate increase in the MDL and EQL.
Papu29.;f23
V\Ar-V^^ Soiv^pl^^ (L^\c\
ENVIRONMENTAL LAB WORK REQUEST
''* . u
fi-
'M^'
'. '\-
I
'-'••;
• '.
.;
™= THIOKOL ENVIRONMENTAL LABORATORY
WtOM!
ORGANIZATION
SAMPLE
1 ZDtfC 7<9-5-
^TpS^^^^'ip
'• -ioec 9^-1
'\^^Jk>-^
',25?^z. ^f-/
*" ^^G:. ^-f
'\2i>^^l 7-:^
'Z^£V: 34-7
"'^^i^S'O'l
'"^^^?
^(>«. /&^3-2-
12.
DATE
f9MAK
/(
/(
/I
/I
/\
fi
f(
/r
n
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COSTCINTUl
LWR No.
Login No.
WORKORDER
El1365
DATE
RIFORTRISULTSTO: 11
HELEN WARD, MS 301 ||
SAMPLE INFORMATION
LOCATION
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TIME
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TEST REMARKS
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CHAIN OF CUSTODY
RELINQUISHED BY
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DATE
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TIME
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RECEIVED BY
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DATE
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TIME
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FOR LABORATORY USE ONLY
II DATE COMPLETED DATE REPORTED SIGNATURE 1
m
CERTIFICATE OF ANALYSIS
Listing of sample Infonmation and Testing Requested
Thursday, May 8,1997
TESTED FOR Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokoi Corp, UT 84322
Helen Ravsten
ANALYZED BY Thiokol Environmental Lat)oratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-3732
800-863-8080
Login Number L879
Lab No Client Number
Test Requested Description
Received CollectDate/Time
Matrix
IL879-1 ZOEC 70-5. M-136
Thiokol SOP 30
SW-846, 8260
SW-846. 7740
SW-846, 7481
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW.846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 302
IL879-2 ZOEC 42-6. M-136
Metals Analysis by Flame AE
Volatile Organics
GFAA Selenium Analysis (RCRA)
GFAA Molydbenum Analysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Co ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Cr ICP Melals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
HPLC Analysis HMX
Perctilorate - lon Chromatography
03«V97 03/19«713:33 1
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
9?/29/97 9?/l9/97l3;4l I
Thiol<ol SOP 30
SW-846, 8260
SW-846, 7740
SW-846, 7481
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 302
Metals Analysis by Flame AE
Volatile Organics
GFAA Selenium Analysis (RCRA)
GFAA Molydbenum Analysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Cd ICP Melals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Co ICP MetalsAnalysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
HPLC Analysis HMX
Perchlorate - lon Chromatography
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Page 1 of 19
[
''>fm:''m^W^'^'''^?^^^ ^^
L87&3 ZOFC 96-1 M-136 03/20«7 03/19/9713:20
Thiokol SOP 30
SW-846, 8260
SW-846, 7740
SW-846,7481
SW-846, 7471A
SW.e46, 7060
SW.846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 302
Metals Analysis by Ffaune AE^i J«
Volatile Organics ^ --#''i^''< ^. -•
GFAA Selenium Analysis (RCRA)
GFAA Molydbenum Analysis (RCRA)
CV Mercury Analysis (RCRA) .
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Co ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
HPLC Analysis HMX
Perchlorate - lon Chromatography
Sou
Soil
Soil
Son
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L879-4 ZOEC 30-6. M-136 03^0/97 03/19/97 13:49
Thiokol SOP 30
SW-846, 8260
SW-846, 7740
SW-846, 7481
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 302
Metals Analysis by Flame AE
Volatile Organics
GFAA Selenium Analysis (RCRA)
GFAA Molydbenum Analysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metais Analysis (RCRA)
Co ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestkm
HPLC Analysis HMX
Perchlorate - lon Chromatography
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L879-5 ZOEC 29-1. M-136 jssmL 03/19/97 13.53
Thiokol SOP 30
SW-846, 8260
SW-846, 7740
SW-846, 7481
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 3050
SOP 420
SOP 302
Metals Analysis by Flame AE
Volatile Organics
GFAA Selenium Analysis (RCRA)
GFAA Molydbenum Analysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Co ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Matals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
HPLC Analysis HMX
Perchlorate - lon Chromatography
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Page 2 of 19
-m ^*.^, $: ^3>:' :^^^
I L879-6 ZOEC 8-4. M-lJe" 03/20/97 03/19/9713:59
Thfokol SOP 30
SW-846, 8260
SW-846, 7740
SW-846, 7481
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 302
Metais Analysis by Ftame AE
Volatile Organics
GF/VA Selenium Analysis (RCRA)
GFAA Molydbenum Analysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Arsenk: Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Co ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
HPLC Analysis HMX
Perchlorate - lon Chromatography
Son
Soil
Soil
Soil
Soil
Soil
Soil
Soli
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
I L879-7 ZOEC 7-5. M-136 03/20/97 03/19/9714:05
Thiokoi SOP 30
SW-846, 8260
SW-846, 7740
SW-846, 7481
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 302
IL87^ ZOEC 34-7. M-136"
Metals Analysis by Flame AE
Volatile Organics
GFAA Selenium Analysis (RCRA)
GFAA Molydbenum Analysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Co ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
HPLC Analysis HMX
Perchlorate - lon Chromatography
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
03/20/97 03/19/9714:15
Thiokol SOP 30
SW-846, 8260
SW-846, 7740
SW-846, 7481
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 302
Metals Analysis by Flame AE
Volatile Organics
GFAA Selenium Analysis (RCRA)
GFAA Molydbenum Analysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Co ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
HPLC Analysis HMX
Perchlorate - lon Chromatography
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Page 3 of 19
I L879.^ ZOEC 50-7. M-136
Thiokol SOP 30
SW-846, 8260
SW-84e, 7740
SW-846,7481
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 302
I L879-10 ZOEC 88-9. M-136
Thiokol SOP 30
SW-846, 8260
SW-846,7740
SW-846, 7481
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 302
Metals Analysis by Ftame AE
Volatile Organics
GFAA Selenium Analysis (RCRA)
GFAA Molydbenum Analysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metais Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Co ICP Metais Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Cr ICP Metais Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
ICP/GFAA Metals DIgestkin
HPLC Analysis HMX
Perchlorate - lon Chromatography
03/20/97 03/19/97 14.26
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soli
Soil
Soil
Soil
Soil
Soil
03/20/97 03/19/9714:37
Metals Analysis by Flame AE
Volatile Organics
GFAA Selenium Analysis (RCRA)
GFAA Molydbenum Analysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Co ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
HPLC Analysis HMX
Perchlorate - lon Chromatography
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L879-11 70EC 106.3-2. M-136 03/20/97 03/19/9714:46
TWokol SOP 30
SW-846, 8260
SW-846, 7740
SW-846, 7481
SW-846, 7471A
SW-846,7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 302
Melals Analysis by Flame AE
Volatile Organics
GFAA Selenium Analysis (RCRA)
GFAA Molydbenum Analysis (RCRA)
CV Mercury Analysis (RCRA)
GF/kA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Co ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
HPLC Analysis HMX
Perchlorate - lon Chromatography
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soli
Soil
Soil
Soil
Soli
Soil
Soil
Page 4 of 19
• '-^ru-. J-if^- ,'"^/.-
1 L879.12 DISPERSION AREA
Thiokol SOP 30
SW-846, 8260
SW-846, 7740
SW-846, 7481
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 302
03«)/97 03/19«714:53
Metals Analysis by Flame AE *; , ,
Volatile Organics
GFAA Selenium Analysis (RCRA)
GFAA Molydbenum Analysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Co ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cu ICP Metais Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
ICP/GFAA Metais Digestion
HPLC Analysis HMX
Perchlorate - lon Chromatography
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
SoH
Soil
Soli
Soil
Soil
Soil
Soil
Soil
Comments:
There was evidence of sample nonhomogeneity for barium arium. /?
<7 Certified Bv Date ^^ Certified By
77J/S certifies that the following samples were analyzed using good laboratory practices to show the following results:
Page 5 of 19
Listing of Results by Sample
IsamplelD
630-20-6
71-55-6
79-34-5
7frO0-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-48-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75^XK3
67-66-3
74-87-3
156-59-4
: ZOEC 70-5, M-136
Test Parameter
CESIUM
1,1,1,2-TETRACHLORGETHANE
1,1,1-TRICHLORaETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1.1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1.2-DIBROMOETHANE
1,2-OICHLOROBENZENE
1,2-D(CHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1.3-DICHLOROPROPANE
1,4-DICMLOROBENZENE
2,2-DICMLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZFNE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1
74-96-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-8
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYl BFNZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZFNE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUPTLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1.2-DICHLOROETHENE
10061-02-6 TRAh4S-1,3-DICHLOROPROPENE
79-01-6
75-69-4
75-01-4
TRICHLOROETHENE
TRICHLOROFLUOROME! HANE
VINYL CHLORIDE
SELENIUM
MOLYBDENUM
MERCURY
ARSENIC
ALUMINUM
BARIUM
CADMIUM
CHROMIUM
COBALT
COPPER
LEAD
SILVER
ICP/GFAA METALS DIGESTION
HMX
Result
259
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u u u u
u u
u u u u u u u
u u
u u u u u
u u
u u
u u
u u
u u
u u
u u u
u u u
u u
u 1.8
5.2
.01
9.2
30000
91
.7
30
7.3
28
U
U
U
Units
ug/g
ug/kg
ug/kg
ugrtcg
ugfltg
ugrttg
ugAg
ugfltg
ugfltg
ug/kg
ugflig
ugrttg
ugrttg
ugrttg
ugrttg
ugfltg
ugrttg
ugrttg
ugfltg
ugfltg
ugrttg
ugrttg
ugrttg
ugrttg
ugfltg
ugrttg
ugfltg
ugfltg
ug/kg
ugrttg
ugrttg
ugrttg
ugrtcg
ugflcg
ugrttg
ugrttg
ugfltg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugfltg
ugflcg
ugflcg
ugrtcg
ugflcg
ugrttg
ugrttg
ugrttg
ugrttg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugfltg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L879-1 Collect Date: 03/19/9713:33 |
Det
UmH
87
i
.2
.3
2
.1
.8
i
...2
.2
.2
.2
.2
.2
.1
.2
.2
2
.2
.2
.2
2
10
2
10
2
.2
10
10
.2
.2
2
.3
.1
.4
.3
.2
.4
.4
.6
.2
2
.3
.2
2
3
2
2
2
.3
2
2
2
2
2
2
2
.9
.3
.2
2
.3
.3
.4
1.1
2
.01
1.1
1.5
.06
.1
.3
.1
.1
1.5
.2
.5
Rep. Dil.
Limit. Factor M>ttl94
223 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10
10 1
10 1
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
3.8
1.1
.02
3.8
7.3
.3
.6
1.5
.6
.6
7.3
.9
.5
Thiokol SOP 30
SW-846,8260
SW-846.8260
SW-846. 8260
SW-S46. 8260
SW-S46.8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846.8260
SW-846. 8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846. 8260
SW-846.8260
SW-846. 8260
SW-&46.8260
SW-846. 8260
SW-846. 8260
SW-846,8260
SW-846, 8260
SW-646, 8260
SW-84e, 8260
SW-846.8260
SW-846.8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846.8260
1 SW-846.8260
1 SW-846.8260
1 SW-846.8260
t SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846.8260
1 SW-84e. 8260
1 SW-846.8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846.8260
1 SW.846.7740
1 SW.846.7481
1 SW-846,7471A
1 SW.846,7060
1 SW.846,6010
1 SW.846,6010
1 SW.846,6010
1 SW.846,8010
1 SW.846,6010
1 SW.846.6010
1 SW.846.6010
1 SW.846.6010
1 SW.846.3050
1 SOP 420
Analyst
CRS
MMR
MMR
MMR
nflnR
MMR
MMR
MMR
ttMMO
lUMR
MMR
MMR
MMR
MMR
MMR
IWKAR
MMR
MMR
MMR
MMR
MMR
MMR
IMMR
HMR
MMR
UMD mviiT
M/IR
MMR
IvmnR
MJIR
KMR
MMR
MMR
M/IR
MMR
MUIR
nwnn
MMR
Mm
MMR
MUIR
MMR
MMR
MMR
^MR
MMR
MMR
MMR
MUIR
MUIR
MMR
MMR
IWlUlK
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
IMMR
BflViR
CRS
CRS
KEN
CRS
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KMS
IfiStDate
06/06ra7 11:38
03/24fl7 12:22
03/24/97 12:22
03/24«7 12:22
oanAiar 1222
03/24/97 12:22
03/24/97 12:22
03/24/97 12:22
03/24/97 12:22
oaaAmy 12:22
03«4«7 12:22
03/24/97 12:22
03«4/97 12:22
03/24ffl7 12:22
03/24/97 12:22
03«4«7 12:22
03/24/97 1222
03/24«712:22
03/24/97 12:22
03/24/97 12:22
03/24/97 12:22
03/24/97 12:22
03/24/97 12:22
03/24/97 1222
03/24«7 12:22
03/24/97 12:22
03/24/97 12:22
03/24«7 12:22
03Q4/97 12:22
03/24/97 12:22
03/24/97 12:22
0304/97 12:22
03/24/97 12:22
03/24/9712:22
03/24/97 12:22
03/24/97 12:22
03/24/97 1222
03«4/97 12:22
03/24/97 12:22
03/24/9712:22
03/24«7 12:22
03/24«7 12:22
03/24/97 1222
03«4«7 1222
03/24/97 12:22
03«4/97 1222
03a4«7 1222
03/24/97 12:22
03^4/9712:22
03«4«7 1222
03/24/97 12:22
03/24«7 12:22
03«4/97 12:22
03/24/97 1222
03^4/97 1222
03/24«7 12:22
03/24/97 1222
03«4«7 1222
03/24/97 12:22
03«4/97 12:22
03/24/97 12:22
03/24/97 1222
03/24/971222
03/24/971222
05«)2fl714:01
05rt)5«7 10:52
04/10/97 10:49
05rt)1/97 16:14
04/11/9713:18
04/11/9713:18
04/11/9713:18
04/11/9713:18
04/11/9713:18
04/11/9713:18
04/11/9713:18
04/11/9713:18
04/09^7 00.00
03/27/97 12:59
Page 6 of 19
PERCHLORATE U ug/g 1.4 7.2 1 SOP 302 CRS 04/24/9712:42
Page 7 of 19
^*f»
1 Sample ID;
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
: ZOEC 42-6, M-136
Test Parameter
CESIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRK>tLOROETHANE
1,1,22-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
12,4-TRICHLOROBENZENE
12,4-TRIMETHYLBENZENE
12-DIBROMO-3-CHLOROPROPAN
12-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
22-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROIMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
t-> 79-01-6
75-69-4
75-01-4
l/0»/>("»
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
SELENIUM
MOLYBDENUM -JsO^-'-
MERCURY •L:>fj
ARSENIC .'.:....
ALUMINUM 79,,t"C.>;,v^
BARIUM 5,s , -'' 11^
CADMIUM ^'^ ' ''*•
CHROMIUM 7 0,-00 ;|.'.'
COBALT ^n^r,f„
COPPER X}V~ ff nr,
1 LEAD
? ^Ci^SILVER
ff»>
X<^oa
ICP/GFAA METALS DIGESTION
HMX
PERCHLORATE
Result
135
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u u
u u u
u u u u
u u
u u u u u u u u
u u u
u u u
u u u
u u u u u u u u u
u 12J
u u 0
4.2
.02
9.5
20200
108
.8
22
9.4
29
U
U
56.5
3.7
Units
ug/g
ugrttg
ugrtcg
ugrttg
ug/kg
ug/kg
ugflcg
ugflcg
ugflcg
ugflcg
ugflcg
ugrtcg
ug/kg
ugrtcg
ugrtcg
ugflcg
ug/kg
ugflcg
ugflcg
ugflcg
ugflcg
ugrttg
ug/kg
ugrttg
ugfltg
ugflcg
ugflcg
ugflcg
ugflcg
ugrtcg
ugrtcg
ugflcg
ugrttg
ugfltg
ugflcg
ug/kg
ugflcg
ugflcg
ugflcg
ugrtcg
ug/kg
ugrtcg
ugrtcg
ugflcg
ugrttg
ugrttg
ug/kg
ugrttg
ugrttg
ug/kg
ugflcg
ugflcg
ugrtcg
ugrtcg
ugrtcg
ugrttg
ugrttg
ugrttg
ugrttg
ugrtcg
ugflcg
ugflcg
ugrtcg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Ub ID: L879-2
Det
Limit
95
2
2
.3
.2
.1
.6
.2
2
.2
2
2
2
.2
.1
.2
.2
2
2
2
2
.2
10
.2
10
2
2
10
10
2
.2
2
.3
.1
.4
.3
2
.4
.4
.6
.2
.2
.3
.2
.2
.3
2
2
2
.3
2
.2
.2
.2
.2
.2
2
.9
.3
2
.2
.3
.3
.4
1.6
2
.02
1.6
2
.08
2
.4
2
2
2
.2
.5
1.5
Rep.
Limit
317
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
5.4
1.6
.05
5.4
9.9
.4
.8
2
.8
.8
9.9
12
.5
7.3
Dil.
Factor
Collect Dote: 03/19/9713:41 |
Method
Tliinknl SOP 30
SW-846,8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-848,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846.8260
SW-846.8260
SW-846,8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846,8260
SW-846.8260
SW-846,8260
SW-846,8260
SW-846, 7740
SW-846, 7481
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 302
Analyst
CRS
MMR
MMR
I^AriR
MMR
MMR
Mm
iVlnR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
IvIvIR
MMR
MMR
MMR
MMR
RAnR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
IvlSriR
MMR
MW1R
NWIR
MMR
MMR
MMR
IravIR
MMR
MMR
MMR
MMR
IVnIR
MMR
MMR
MMR
MMR
MMR
RreVlR
IVIVIR
IVIVIR
MMR
MMR
MMR
MMR
wIVIR
MMR
CRS
CRS
KEN
CRS
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KMS
CRS
Test pate
05/06/9711:38
03/24/97 12:56
03/24/97 12:56
03«4«7 12:56
03^4/97 12:56
03/24/97 12:56
03/24/97 12:56
03/24/97 12:56
03/24/97 12:56
03/24/97 12:56
03/24/97 12:56
03/24/97 12:56
03/24/97 1256
03«4/97 12:56
03/24/9712:56
03/24/97 12:56
Q3I2AB7 12:56
03«4/97 12:56
03/24/97 12:56
03/24/97 12:56
03/24/9712:56
03/24/9712:56
03/24/97 12:56
03/24«7 12:56
03/24/97 12:56
03/24/97 12:56
03/24/97 12:56
03/24/97 12:56
03«4«7 12:56
03/24/97 12:56
03/24/97 12:56
03/24/97 12:56
03«4«7 12:56
03/24/97 12:56
03^4/97 12:56
03/24/97 12:56
03/24/9712:56
03/24/9712:56
03/24/97 12:56
03/24/97 12:56
03/24/97 12:56
03/24/97 12:56
03/24/97 12:56
03/24/97 12:56
03/24/97 12:56
03/24/97 12:56
03/24/9712:56
03/24/9712:56
03/24/97 12:56
03/24/97 12:56
03/24/97 12:56
03/24/97 12:56
03^4/97 12:56
03^4/97 12:56
03/24/97 12:56
03/24/9712:56
03/24/97 12:56
03/24/97 12:56
03/24/97 12:56
03/24/97 12:56
03^4/97 12:56
03/24/97 12:56
03/24/9712:56
03/24/97 12:56
05/02/9714:11
05/05/9711:02
04/10«7 10:54
05^1/97 16:23
04/11/97 13:21
04/11/97 13:21
04/11/97 1321
04/11/97 1321
04/11/9713:21
04/11/971321
04/11/971321
04/11/971321
04/09/97 00:00
03/28/97 07:36
04/24/97 12:50
Page 8 of 19
:- J
IsamplelO
63O-20-6
71-65-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
. 74-87-3
156-59-4
ZOEC 96-1, M-136
IsHEaiameter
CESIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2.TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
12,3-TRICHLOROBENZENE
1.2,3-TRICHLOROPROPANE
12.4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBeNZENE
1,2-DIBROMO-3-CHLOROPROPAN
12-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
12-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1.2-DICHLOROETHENE
10061 -01 -5 CIS-1,3-DICHLOROPROPENE
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75439-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBEN7FNE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
79-01-6
75-69-4
75-01-4
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
SELENIUM
MOLYBDENUM
MERCURY
ARSENIC
ALUMINUM
BARIUM
CADMIUM
CHROMIUM
COBALT
COPPER
LEAD
SILVER
K:P/GFAA METALS DIGESTION
HMX
PERCHLORATE
Result
192
U
U
u
u u
u u u u u u
u u u u u u u
u u
u u
u u
u u u
u u
u u u u u u u
u u u u
u u
u u
u u
u u
u u
u u u u u u
u u
u u
u u
u 0
3.1
.02
6.5
la-mn
66
.1
16
6.9
51
7.8
u
u
u
Unit?.
ug/g
ugrtcg
ugrtcg
ug/kg
ugfltg
ugflcg
ugflcg
ugrttg
ugrttg
ugrttg
ugrttg
ugrtcg
ugflcg
ugrtcg
ugflcg
ugflcg
ugrttg
ugrttg
ugrtig
ugrttg
ugrttg
ugrttg
ugflcg
ugrtcg
ugflcg
ugfltg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ug/kg
ugrttg
ugflcg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugflcg
ugflcg
ugflcg
ugflcg
ugflcg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugflcg
ugflcg
ugflcg
ugflcg
ugflcg
ugrttg
ugrttg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Lab ID: L879-3
Dot
Limit
81
2
.2
.3
2
.1
.6
2
.2
.2
2
2
2
2
.1
2
2
2
2
2
2
2
10
2
10
2
2
10
10
2
.2
.2
.3
.1
.4
.3
2
.4
.4
.6
2
2
.3
2
2
.3
2
2
2
.3
2
2
2
2
2
2
2
.9
.3
.2
.2
.3
.3
.4
1.3
2
.01
1.3
1.7
.07
.1
.3
.1
.1
1.7
2
.5
1.5
Rep.
Umit
268
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
4.6
1.3
.04
4.6
8.4
.3
.7
1.7
.7
.7
8.4
1
.5
7.3
DiL
Factor
Collect Date: 03/18/9713:20 |
..
fAVQlVl
Thiokol SOP 30
SW-848,8260
SW-846,8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846, 8260
SW-846,8260
SW-846.8260
SW-846.8260
SW-846. 8260
SW-848,8260
SW-846,8260
SW-846,8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846.8260
SW-846, 8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846. 8260
SW-846.8260
SW-846.8260
SW-848.8260
SW-846, 8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-848.8260
SW-846, 8260
SW-846.8260
SW-846.8260
SW-846, 8260
SW-846,8260
SW-848, 8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 7740
SW-846, 7481
SW-846, 7471A
SW-846, 7060
SW-846,6010
SW-846, 6010
SW-846,6010
SW-846,6010
SW-84e, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 302
Analyst
CRS
MMR
KAnR
MMR
MMR
MMR
lUWflR
MMR
MMR
MMR
MMR
MMR
MMR
MUR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MIMR
MMR
IMMR
MMR
MMR
MMR
MMR
rraVIR
i¥W*ir^
MMR
MMR
WiVIR
MMR
MMR
MMR
MMR
MMR
RAnR
MMR
MMR
MMR
MMR
MMK
AravIR
WIVIR
nffMR
IVlViR
MMR
MMR
RmVIR
CRS
CRS
KEN
CRS
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KMS
CRS
Test Date
05;K)6/97 11:40
0304*7 13:30
03/24/97 13:30
0304/97 13:30
03O4«7 13:30
0304/97 13:30
0304/97 13:30
03O4fl7 13:30
0304/97 13:30
0304/97 13:30
03O4«7 13:30
03O4fl7 13:30
0304/97 13:30
03O4«7 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
03O4«7 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
03O4B7 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
03/24/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
03O4«7 13:30
0304/97 13:30
0304/97 13:30
03O4«7 13:30
0304/97 13:30
0304/97 13:30
03O4«7 13:30
03O4«7 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
03O4«7 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
0304/97 13:30
05^)2/97 14:20
05/05/97 11:18
04/10/9711:02
05«1/97 16:33
04/11/9713:24
04/11/9713:24
04/11/9713:24
04/11/97 13.24
04/11/9713:24
04/11/97 13:24
04/11/97 13:24
04/11/97 1324
04rt)9/97 00:00
0307/97 13:42
0404/97 12:59
Page 9 of 19
r^'":!^*''
IsamplelD
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
. 74-87-3
156-59-4
. ZOEC 3(W, M-136
I»t P«r^met«r
CESIUM
1.1.12-TETRACHLOROETHANE
1.1.1 -TRICHLOROETHANE
1.122-TETRACHLOROETHANE
1.1.2-TRICHLOROETHANE
1.1-DICHLOROETHANE
1.1-DICHLOROETHENE
1.1-DICHLOROPROPENE
1.2,3-TRICHLOROBENZENE
12,3-TRICHLOROPROPANE
12.4-TRICHLOROBENZENE
12.4-TRIMETHYLBENZENE
12-DIBROMO-3-CHLOROPROPAN
1.2-DIBROMOETHANE
12-DICHLOROBENZENE
1.2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBEN7FNE
22-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBEN7FNE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1.2-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
DIBR(3MOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBEr<ZFNE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBEN7FNE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZFNE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1.2-DICHLOROETHENE
10061-02-8 TRANS-1,3-DICHLOROPROPENE
79-01.6
75-69-4
75-01-4
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
SELENIUM
MOLYBDENUM
MERCURY
ARSENIC
ALUMNUM
BARIUM
CADMIUM
CHROMIUM
COBALT
COPPER
LEAD
SILVER
ICP/GFAA METALS DIGESTION
IflMX
PERCHLORATE
Result
205
U
U
U
u u u u u u u u
u u
u u u u
u u u
u u u u
u u u u u
u u u u
u u
u u
u u
u u u
u u u u
u u u u
u u
u u
u u u
u u u 5.6 J
u
u
u 2.8
.02
9.8
21400
147
U
23
6.4
16
U
U
5.34
U
Units
ug/g
ug/kg
ugrttg
ugflcg
ugrtcg
ug/kg
ugrttg
ugrttg
ugrttg
ugrttg
ugfltg
ugflcg
ugrttg
ugrttg
ugrttg
ugrttg
ugfltg
ugrttg
ugrttg
ugrttg
ugfltg
ugrttg
ugrttg
ugfltg
ugflcg
ugrtcg
ugrtcg
ugrttg
ugrttg
ugrttg
ugfltg
ugrttg
ugrttg
ugflcg
ugrttg
ugrttg
ugfltg
ugrttg
ugrttg
ugrttg
ugrtcg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugflcg
ugflcg
ugrtcg
ugrtcg
ugrtcg
ugflcg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugfltg
ugflcg
ugrtcg
ugflcg
ugflcg
ugrttg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L879-4
Det
Umit
77
2
2
.3
2
.1
.6
2
.2
2
2
2
2
2
.1
2
2
2
2
2
2
2
10
2
10
.2
2
10
10
2
2
2
.3
.1
.4
.3
2
.4
.4
.6
2
2
.3
2
2
.3
2
2
2
.3
.2
2
2
2
2
2
2
.9
.3
.2
.2
.3
.3
.4
1.3
2
.01
1.3
1.6
.06
.1
.3
.1
.1
1.6
.2
.5
1.5
Rep. Dil.
Umit Factor
258 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
4.4 1
1.3 1
.04 1
4.4 1
8.1 1
.3 1
.6 1
1.6 1
.6 1
.6 1
8.1 1
.97 1
.5 1
7.4 1
Collect Date: 03/19/9713:49 |
Method
Thkikol SOP 30
SW-846.8260
SW-846.8260
SW-846. 8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-848. 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846. 8260
SW-848. 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-848,8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846. 8260
SW-846, 8260
SW-846. 8260
SW-846.8260
SW-846. 8260
SW-846. 8260
SW-846.8260
SW-846.8260
SW-846.8260
SW.848. 8260
SW-846, 8260
SW-848, 8260
SW-846, 8260
SW-846, 7740
SW-846.7481
SW-846. 7471A
SW-846. 7060
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846,6010
SW-846, 3050
SOP 420
SOP 302
Analyst
CRS
MMR
MMR
RAnR
MMK
MMR
MMR
MMR
NIMR
MMR
RraMR
RraVIR
BmlnR
MMR
MMR
RWnR
MMR
MMR
MMR
MMR
BWrlR
MMR
MMR
MMR
MIUR
MMR
HMR
MMR
RffUIR
MMR
NKnR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
ralVIR
MnA\
MMR
RAVIR
MVIR
MMR
IViVlR
RwWiR
MMR
MMR
NVnR
nWflR
MMR
MV1R
MMR
UMO
fwwnTK MMR
MMR
MMR
IVlnR
UMR
nraVlC
RAVIR
RwVB\
MMR
MMR
CRS
CRS
KEN
CRS
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KMS
CRS
Test Date
06«)6»7 11:42
0304/97 14:05
03O4«7 14:05
0304/97 14:05
0304/97 14:05
0304/97 14K)5
03O4«7 14:05
0304/97 14:05
0304/9714:05
0304/97 14:05
0304/97 14:05
0304/97 14:05
0304/97 14i)5
03O4«7 14:05
0304/97 14:05
0304/97 14:05
0304/97 14:05
03O4«7 14:05
03O4«7 14K)5
0304/97 14:05
0304/97 14:05
03O4«7 14:05
0304/97 14:05
03O4fl7 14:05
03O4«7 14:05
0304/97 14:05
0304/97 14:05
0304/97 14:05
0304/97 14:05
0304/97 14:05
0304*7 14:05
03O4«7 14:05
0304/97 14:05
0304*7 14:05
0304*7 14:05
0304*7 14:05
0304*7 14:05
0304*7 14:05
0304/97 14:05
0304*7 14:05
0304*7 14:05
0304*7 14:05
0304*7 14:05
0304*7 14«5
0304*714:05
0304*7 14:05
0304*7 14:05
0304*714:05
0304/97 14:05
0304*7 14:05
0304*7 14:05
0304*7 14:05
0304*7 14fl5
0304*7 14:05
0304*7 14:05
0304*7 14:05
0304*714:05
0304*7 14:05
0304*7 14:05
0304*7 14:05
0304*7 14K)5
0304*7 14:05
0304*7 14:05
0304*7 14:05
05/02*7 14:36
05*5*711:41
04/10*711:05
05*1*7 16:55
04/11*7 1327
04/11*713:27
04/11*713:27
04/11*713:27
04/11*713:27
04/11*713:27
04/11*713:27
04/11*713:27
04/09*7 00:00
0307*7 13:58
0404*7 13:07
Page 10of 19
[sample ID
630.2O4
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
: ZOEC 29-1, M-136
Ifist PflrfMiista
CESIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1.1-DICHLOROETHANE
1.1-DICHLOROETHENE
1.1-DICHLOROPROPENE
12.3-TRICHLOROBENZENE
12.3-TRICHLOROPROPANE
1.2.4-TRICHLOROBENZENE
1.2.4-TRIMETHYLBENZENE
12-DIBROMK>3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1.3-DICHLOROPROPANE
1.4-DICHLOROBENZENE
22-DK;HLOROPROP/>WE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-12-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBEN7FNE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZFNE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-8UTYI RFNZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
79-01-6
75-69-4
75-01-4
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
SELENIUM
MIOLYBDENUM
MERCURY
ARSENIC
ALUMINUM
BARIUM
CADMIUM
CHROMIUM
COBALT
COPPER
LEAD
SILVER
ICP/GFAA METALS DIGESTION
V«MX
PERCHLORATE
R*«4lt
352
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
1.9
u
21
10600
164
.7
15
5.9
9.7
6
U
U
U
Unit»
ug/g
ug/lqi
ugflcg
ug/kg
ugflcg
ug/kg
ugrtcg
ugflcg
ugrtig
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ug/kg
ugrtcg
ugflcg
ugrtcg
ugrtcg
ugflcg
ugrtcg
ugflcg
ugrtcg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrtcg
ugrtcg
ugflcg
ugflcg
ugflcg
ug/kg
ugrtcg
ugrtcg
ugflcg
ugflcg
ugflcg
ugrttg
ugflcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrttg
ugrttg
ugrttg
ugrtcg
ugflcg
ugrttg
ugrtcg
ugrtcg
ugrtcg
ugflcg
ugflcg
ugrttg
ugrttg
ugrtcg
ugrtcg
ugrtcg
ugrttg
ugrttg
ugrtcg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
•' - • • Y'' '
LablD:L87&-5 Collect Date: 03/19«713:53 |
Det.
Limit
82
.2
.2
.3
2
.1
.6
2
2
2
2
.2
.2
2
.1
2
2
2
2
2
2
2
10
.2
10
2
2
10
10
2
2
2
.3
.1
.4
.3
2
.4
.4
.6
2
.2
.3
.2
.2
.3
.2
2
2
.3
2
2
2
2
2
2
2
.9
.3
.2
.2
.3
.3
.4
1.4
2
.02
1.4
1.7
.07
.1
.3
.1
.1
1.7
2
.5
1.4
Rep. Dil.
Limit Factor Met^94
274 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
47
1.4
.04
4.7
8.6
.3
.7
1.7
.7
.7
8.6
1
.5
7.1
Thtokol SOP 30
SW.846,8260
SW.846.8260
SW.846. 8260
SW-846.8260
SW.446.8260
SW-846.8260
SW-846.8260
SW-846. 8260
SW-846.8260
SW-846. 8260
SW-S46. 8260
SW-846.8260
SW-846. 8260
SW-846. 8260
SW-846.8260
SW-846.8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846.8260
SW-846, 8260
SW-846, 8260
SW-846.8260
SW-846. 8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-848,8260
1 SW..846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
t SW-846,8260
1 SW-846,8260
1 SW-84e, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-848,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846.8260
1 SW-846.8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,7740
1 SW-846,7481
1 SW-846,7471A
1 SW-846,7060
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846.6010
1 SW-846.3050
1 SOP 420
1 SOP 302
Analyst
CRS
MMR
MMR
MMR
MMR
NMR
MMR
MMR
MMR
MMR
t/MR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
nIMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
RWwC
MMR
RraMR
MMR
MMR
MMR
MMR
RWnR
MMR
MMR
MMR
IMnR
MMR
MMR
MMR
MMR
MMR
mvir\
MMR
MMR
MMR
MMR
MMR
nrlwK
MMR
MMR
MMR
MMR
RmMR
RffVlR
MMR
IVIVIR
CRS
CRS
KEN
CRS
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KMS
CRS
Test Date
05*6*7 11:44
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14.39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*714:39
0304*7 14.39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*714:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0aO4*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*714:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304/97 14:39
0304/97 14:39
0304*7 14:39
0304*714:39
0304*714:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14-J9
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*714:39
0304*714:39
0304*714:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
0304*7 14:39
05*2*7 14:46
05/05*711:50
04/10*711:09
05*1*7 17:05
04/11*713:30
04/11*713:30
04/11*713:30
04/11*713:30
04/11*713:30
04/11*713:30
04/11*713:30
04/11*7 13:30
04/09*7 00:00
0307*7 14:07
0404*7 13:15
Page 11 of 19
IsamplelD
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-81-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
9».87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-S
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
754)9-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
10O-42-5
98-06-6
127-18-4
108-88-3
156-60-5
•*
: ZOEC 8-4, M-136
Teft PflPWTWter
CESIUM
1,1,1,2-TETRACHLOROETHANE
1,1 .I-TRK:HLOROETHANE
1.12.2-TETRACHLOROETHANE
1.1.2-TRICHLOROeTHANE
1.1-DICHLOROETHANE
1.1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
12,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROM0.3-CHLOROPROPAN
1.2-DIBROMOETHANE
12-DICHLOROBENZENE
1.2-DICHLOROETHANE
12-DICHLOROPROPANE
1.3.5-TRIMETHYLBENZENE
1.3-DICHLOROBENZENE
1.3-DICHLOROPROPANE
1.4-DICHLOROBENZENE
2.2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4<:HLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMK3BENZENE
BROMOCHLOROMb 1 HANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
aS-1.2-DICHLOROETHENE
1 CIS-1.3-OICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1.2-DICHLOROETHENE
10061-02-6 TRANS-1.3-DICHLOROPROPENE
79-01-6
75-69-4
75-01-4
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
SELENIUM
MOLYBDFNUM
MERCURY
ARSENIC
ALUMNUM
BARIUM
CADMIUM
CHROMUM
COBALT
COPPER
LEAD
SILVER
ICP/GFAA METALS DIGESTION
HMX
PERCHLORATE
ResMit
177
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u 0
12
u
5.3
7400
104
.1
16
1.6
10
U
.2
U
U
^.
Unit?
ug/g
U9*g
ugrttg
ugrttg
ugrttg
ugrttg
ug/kg
ugrtcg
ugflcg
ugrtcg
ug/kg
ugrtcg
ugrtcg
ugflcg
ugrttg
ugrtcg
ugrttg
ugrtcg
ugrttg
ugrttg
ugrttg
ugrttg
ugfltg
ugfltg
ugfltg
ugrtcg
ugrtcg
ugrtcg
ugflcg
ugrttg
ugflcg
ugfltg
ugrtcg
ugrttg
ugrttg
ugrttg
ug/kg
ugrtcg
ugflcg
ugflcg
ugrtcg
ugrtcg
ugflcg
ugflcg
ugflcg
ugflcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugflcg
ugflcg
ugflcg
ugrtcg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
^-^
L
Det
Umit
63
2
.2
.3
.2
.1
.6
.2
2
2
2
2
2
2
.1
.2
.2
2
.2
.2
.2
2
10
2
10
2
2
10
10
2
2
.2
.3
.1
.4
.3
2
.4
.4
.6
2
2
.3
2
2
.3
.2
.2
.2
.3
.2
2
2
2
2
2
2
.9
.3
.2
.2
.3
.3
.4
1.1
.2
.01
1.1
1.3
.05
.1
.3
.1
.1
1.3
2
.5
1.6
*.,• . ...
'• •
.ablD:L879-6 Collect Date: 03/19/9713:59 j
Rep. Dii.
Limit Factor Method
211 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10 1
10 1
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
3.6
1.1
.04
3.6
6.6
.3
.5
1.3
.5
.5
6.6
.8
.5
7.9
Thiokol SOP 30
SW-846,8260
SW-846,8260
SW-848, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846, 8260
SW-846,8260
SW-848,8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.846,8260
SW-848, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-S46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
t SW-846,8260
t SW-846,8260
1 SW-846,8260
1 SW-S46,8260
1 SW-846,8260
t SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846.8260
1 SW-846.8260
1 SW-84e. 8260
1 SW-846.8260
1 SW-846.8260
1 SW-846.8260
1 SW-848.8280
1 SW-846,8260
1 SW'846,8260
1 SW-846,7740
1 SW-846,7481
1 SW-846,7471A
1 SW-846,7060
1 SW-846,6010
1 SW-846.6010
1 SW-846.6010
1 SW-846.6010
1 SW-846.6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,3050
1 SOP 420
1 SOP 302
Anaixst
CRS
MMR
MMR
MMR
tMR
IWMR
RWnK
MMR
MMR
MMR
MMR
MMR
NIVIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
nraVIR
MMR
NIVIR
MMR
MMR
MMR
MMR
r^nR
MMR
nwnR
p/Wnt\
NIVIR
n™MR
MMR
MMR
MMR
MMR
RraVIR
hnMR
MMR
RWrlR
MMR
MMR
MMR
NIMR
NIVIR
MMR
MMR
n™MR
RraVIR
MMR
MMR
MMR
MMR
IVIVIR
MMR
MMR
CRS
CRS
KEN
CRS
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KMS
CRS
Test Date
05/06*711:46
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*715:13
0304*7 15:13
0304*7 15:13
0304*7 15.13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304/97 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304/97 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*7 15:13
0304*715:13
0304*7 15:13
0304/97 15:13
0304*715:13
0304*7 15:13
0304/97 15:13
0304*7 15:13
0304*7 15:13
0304/97 15:13
0304*7 15:13
0304*7 15:13
0304*715:13
0304*7 15:13
0304*715:13
0304*7 15:13
0304*7 15:13
0304*715:13
05/02*7 15:08
05/05/97 12:19
04/10*7 11:13
05/01*7 1727
04/11*714:06
04/11*714.-06
04/11*714^6
04/11*714:06
04/11*714:06
04/11*714.06
04/11*714:06
04/11/9714:06
04/09*7 00:00
0307*7 14:14
0404*7 13:24
Page 12of 19
IsamplelD
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
ZOEC 7-5, M-136
Te?t Pqrameter
CESIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,22-1 fc I RACHLOROETHANE
1.1.2-TRICHLOROETHANE
1.1-DICHLOROETHANE
1.1 -DICHLOROETHENE
1,1-DICHLOROPROPENE
12,3-TRICHLOROBEN2ENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
12.4-TRIMETHYLBEN2ENE
12-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIH«THYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
22-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4^METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-12-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
DIBROMOCHLOROMETH/VNE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZFNE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
79-01-6
75-69-4
75-01-4
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
SELENIUM
MOLYBDENUM
MERCURY
ARSENIC
ALUMINUM
BARIUM
CADMIUM
CHROMIUM
COBALT
COPPER
LEAD
SILVER
ICP/GFAA METALS DIGESTION
HMX
PERCHLORATE
Result
249
U
U
U
U
U
u u u u u u u u
u u
u u u u
u u
u u u u u
u u u u u u u
u u
u u
u u
u u
u u
u u u u
u u u u
u u
u u
u u
u u
u u
u u
0
2.1
u 5.3
13200
142
.2
20
7.1
14
2.7
U
19
U
Unit^
ug/g
ugrttg
ugrttg
ugfltg
ugrttg
ugflcg
ugflcg
ugrtcg
ugrttg
ugrttg
ugrttg
ug/kg
ugflcg
ugflcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrttg
ugrttg
ugrtcg
ug/kg
ugrttg
ugrtcg
ugrtcg
ugrtcg
ug/kg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrttg
ug/kg
ugrttg
ug/kg
ugflcg
ug/kg
ugrtcg
ugrtcg
ug/kg
ugrtcg
ugrtcg
ug/kg
ugrtcg
ug/kg
ug/kg
ugrtcg
ugflcg
ugflcg
ugrtcg
ugrtcg
ugrttg
ugrttg
ugrtcg
ug/kg
ugrtcg
ug/kg
ug/kg
ugrtcg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L879-7 Collect Date: 03/19/9714:05 |
Det.
Limit
63
.2
2
.3
2
.1
.6
.2
2
2
2
2
,2
.2
.1
.2
2
2
2
.2
.2
.2
10
2
10
2
2
10
10
.2
.2
.2
.3
.1
.4
.3
.2
.4
.4
.6
2
2
.3
2
2
.3
.2
.2
.2
.3
2
2
.2
2
2
.2
.2
.9
.3
.2
.2
.3
.3
.4
1.1
.2
.01
1.1
1.3
.05
.1
.3
.1
.1
1.3
2
.5
1.6
Rep. DII.
Umit Factor Method
209 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
3.6
1.1
.04
3.6
6.6
.3
.5
1.3
.5
.5
6.6
.8
.5
7.8
Thiokol SOP 30
SW-846,8260
SW-846,8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-848,8260
SW-e46,8260
SW-846,8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-848,8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846.8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-84e. 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-848,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846.8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,7740
1 SW-846,7481
1 SW-846,7471A
1 SW-846,7060
1 SW-846,6010
1 SW-846.6010
1 SW-846.6010
1 SW-846.6010
1 SW-846.6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,3050
1 SOP 420
1 SOP 302
Analyst
CRS
MMR
ItMR
NWIR
MMR
MMR
AWAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
nW/IR
MMR
MMR
MMR
MMR
MMR
MMR
NInR
MMR
M/IR
MMR
MMR
MMR
MMR
iUiUiR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
IMMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
NIVIR
MMR
MMR
MMR
KMR
CRS
CRS
KEN
CRS
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KMS
CRS
IsstPfte
05*6*7 11:47
0304*7 15:47
0304*7 16:47
0304*7 15:47
0304*7 15:47
0304*7 15:47
0304*7 15:47
0304*7 15:47
0304/97 15.47
0304/97 15:47
0304*7 15:47
0304*7 15:47
0304*7 15:47
0304/97 15:47
0304*7 15:47
0304*7 15:47
0304*7 15:47
0304*7 15:47
0304*7 15:47
0304*7 15:47
03/24*7 15:47
0304/9715:47
0304*7 15:47
0304*7 15:47
0304*7 15:47
0304*7 15:47
0304*7 15:47
0304*7 15:47
0304*7 15:47
03/24*715:47
0304*7 15:47
0304*7 15:47
0304*7 15:47
0304*7 15:47
0304*7 15:47
0304/97 15:47
03/24*715:47
0304*7 15:47
0304*7 15:47
0304*7 15:47
0304*7 15:47
0304/97 15:47
0304*7 15:47
0304*7 15:47
0304/9715:47
03/24/97 15:47
0304*7 15:47
0304*7 15:47
0304*7 15:47
0304/97 15:47
0304*7 15:47
03/24/97 15.47
0304/9715:47
0304*7 15:47
0304*7 15:47
0304*7 15:47
0304/97 15:47
0304/97 15:47
0304*7 15:47
0304*715:47
0304*7 15:47
0304/97 15:47
0304*7 15:47
0304*7 15:47
05*2*7 15:17
05/05/97 12:42
04/10/9711:16
05/01/97 17:42
04/11*714:09
04/11/9714:09
04/11*7 14:09
04/11*714:09
04/11*714:09
04/11*7 14:09
04/11*7 14:09
04/11*714:09
04/09/97 00:00
03/27*7 14:23
0404/97 13:57
Page 13of 19
[^^-
IsamplelD
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
: ZOEC 34-7, M-136
ISSt Par«T»eter
CESIUM
1,1,1.2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
12,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
12-OIBROMOETHANE
12-DICHLOROBENZENE
12-DICHLOROETHANE
12-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBEN7FNE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
10(M2-5
98-06-6
127-18-4
108-88-3
156-60-5
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBEN7FNE
NAPHTHALENE
O-XYLENE
SEC-BUI YLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-12-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
79-01-6
75-69-4
75-01-4
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
SELENIUM
MOLYBDENUM
MERCURY
ARSENIC
ALUMINUM
BARIUM
CADMIUM
CHROMIUM
COBALT
COPPER
LEAD
SILVER
ICP/GFAA MET/U.S DIGESTION
HMX
PERCHLORATE
Result
354
U
U
U
U
U
U
U
U
U
U
U
U
U
u u
u u
u
u u u u u u u
u u u u u
u u
u u u u
u u u
u
u u u u u u u
u u
u u
u u u u u u
u u
u
u u
u 0
2.7
u 7.6
10800
92
.8
15
7.8
20
9
.5
U
U
Units
ug/g
ugrtcg
ugrttg
ugrtcg
ugrtcg
ugrttg
ug/kg
ugrttg
ugrttg
ugrttg
ugflcg
ug/kg
ugrtig
ugrttg
ugrttg
ugrttg
ugfltg
ugrttg
ugrtcg
ugfltg
ugrtcg
ugrtcg
ugrttg
ugrttg
ugrttg
ugflcg
ugflcg
ugflcg
ugflcg
ugflcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrtcg
ug/kg
ugflcg
ugrtcg
ugrtcg
ugflcg
ugrttg
ugrtcg
ugrttg
ugrttg
ugrttg
ugrtcg
ugflcg
ugrtcg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Lab ID: L879-8
DeL
Limit
77
2
2
.3
2
.1
.6
2
2
2
.2
2
2
2
.1
2
2
2
.2
.2
2
2
10
2
10
2
2
10
10
2
2
2
.3
.1
.4
.3
.2
.4
.4
.6
2
2
.3
2
2
.3
2
2
.2
.3
2
2
2
2
2
2
2
.9
.3
.2
2
.3
.3
.4
1.3
2
.01
1.3
1.6
.06
.1
.3
.1
.1
1.6
2
.5
1.6
Rep.
Umit
256
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
4.4
1.3
.04
4.4
8
.3
.6
1.6
.6
.6
8
.96
.5
7.8
Dil.
Factor
Collect Date: 03/19/9714:15 |
Method
Thiokol SOP 30
SW-846,8260
SW-846,8260
SW-848, 8260
SW-846,8260
SW-S46, 8260
SW-84e, 8260
SW-846,8260
SW-84e,8260
SW-846. 8260
SW-848,8260
SW-846, 8260
SW-846,8260
SW-846.8260
SW-846.8260
SW-848. 8260
SW-846. 8260
SW-846, 8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846, 8260
SW-846.8260
SW-846. 8260
SW-846. 8260
SW-846. 8260
SW-848.8260
SW-846, 8260
SW-846.8260
SW-846. 8260
SW-846.8260
SW-846. 8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846,8260
SW-846, 8260
SW-846.8260
SW-846.8260
SW-846. 8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-848.8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846,8260
SW-846, 8260
SW-84C, o260
SW-846, 7740
SW-846, 7481
SW-846, 7471A
SW-846, 7060
SW-846, 6010
SW-846,6010
SW.84e, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 302
Analyst
, CRS
BW^R
MMR
RmnR
MMR
MMR
RAnR
RWnR
NMR
MMR
MMR
wnnn
MMR
MMR
- MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
BflUIR
MMR
IMMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
NIVIR
MMR
nwAn
MMR
MMR
MMR
NIMR
MMR
MMR
NInR
NIVIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
CRS
CRS
KEN
CRS
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KMS
CRS
T^stpate
05*6*711:48
0304*7 16:21
0304*7 1621
0304*7 1621
0304*7 1621
0304*7 1621
0304*7 16:21
0304*7 1621
0304*7 1621
0304*7 1621
0304*7 16:21
0304*7 16:21
0304*7 16:21
0304*7 1621
0304*7 1621
0304*7 1621
0304*7 1621
0304*7 1621
0304/97 16:21
0304*7 16:21
0304/97 16:21
0304*7 1621
0304*7 1621
0304*7 1621
0304*7 1621
0304*7 1621
0304*7 1621
0304*7 16:21
0304*7 16:21
0304*7 16:21
0304*7 1621
0304*7 1621
0304*7 1621
0304*7 1621
0304*7 1621
0304*7 16:21
0304*7 1621
0304*7 1621
0304*7 16:21
0304*7 1621
0304*7 1621
0304*7 1621
0304*7 1621
0304*7 16:21
0304*7 16:21
0304/97 16:21
0304*7 16:21
0304*7 1621
0304*7 1621
0304*7 16:21
0304*7 1621
0304*716:21
0304*7 16:21
0304*7 16:21
0304*7 1621
0304*7 1621
0304*7 1821
0304*7 1621
0304*7 1621
0304*7 16:21
0304*7 16:21
0304*7 16:21
0304*7 16:21
0304*7 1621
05/02*7 15:33
05rt)5*7 12:51
04/10*7 11:24
05*1/97 18:04
04/11*714:12
04/11*714:12
04/11*714:12
04/11*714:12
04/11*714:12
04/11*714:12
04/11*7 14:12
04/11*714:12
04/09*7 00:00
0307*7 14:33
0404*7 14:05
Page 14of 19
\
IsamplelD
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35.-»
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93^
95-49-8
591-78-8
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-e
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75^)9-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
: ZOEC 50-7, M-136
Ifi»t Pflramet*r
CESIUM
1.1.1,2-TETRACHLOROETHANE
1.1.1 -TRICHLOROETHANE
1.12.2-TETRACHLOROETHANE
1.1.2-TRICHLOROETHANE
l.l-DICHLOROETHANE
1.1-DICHLOROETHENE
1,1-DICHLOROPROPENE
12,3-TRICHLOROBENZENE
12,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
12,4-TRIMETHYLBENZENE
1.2-DIBROMO-3-CHLOROPROPAN
12-DIBROMOETHANE
12-DICHLOROBENZENE
1 ,2-DK;HLOROETHANE 1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
) CIS-1.3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1.2-DICHLOROETHENE
10061-02-6 TRANS-1.3-OICHLOROPROPENE
79^)1-6
75-69-4
75-01-4
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
SELENIUM
MOLYBDENUM
MERCURY
ARSENIC
ALUMNUM
BARIUM
CAOMIUM
CHROMIUM
COBALT
COPPER
LEAD
SILVER
ICP/GFAA METALS DIGESTION
HMX
PERCHLORATE
Result
226
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u u
u
u
u u
u
u u
u u
u u
u
u
u
u
u
u
u u
u
u
u
u
u
u 1.7J
u
u
0
1.8
.02
8.3
15900
88
u 19
5.9
147
U
.7
1.17
4.8
Unit?
ug/g
ugrttg
ugflcg
ug/kg
ug/kg
ugrtcg
ugrttg
ugrttg
ugrttg
ug*g
ugrttg
ugrtcg
ugrttg
ugflcg
ugrttg
ugrtcg
ugrtcg
ugrtcg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrtcg
ugfltg
ugrttg
ugrttg
ugrtcg
ugflcg
ugflcg
ugfltg
ugflcg
ugrtig
ugrttg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugflcg
ugflcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrtcg
ugflcg
ugrtcg
ugrtcg
ugrtcg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L879-8 Collect Oate: 03/19/9714:26 |
Det
Limit
78
2
2
.3
2
.1
.8
2
2
2
2
2
2
2
.1
2
2
2
2
2
2
2
10
2
10
2
2
10
10
.2
2
2
.3
.1
.4
.3
2
.4
.4
.6
2
.2
.3
2
2
.3
2
2
2
.3
2
2
2
2
2
2
2
.9
.3
2
2
.3
.3
.4
1.3
2
.02
1.3
1.6
.07
.1
.3
.1
.1
1.6
.2
.5
1.6
Rep. DII
Limit Factor M«UM
261 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10
10
10
10
10
10
10
10
10
10
10
to
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
4.4
1.3
.04
4.4
82
.3
.7
1.6
.7
.7
82
.98
.5
7.9
Thk)holSOP30
SW-848. 8260
SW-846.8260
SW-848.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846. 8260
SW-846. 8260
SW-846.8260
SW-846.8260
SW-846, 8260
SW-846,8260
SW-846,8260
SW-846.8260
SW-846. 8260
SW-846. 8260
SW-846. 8260
SW-846.8260
SW-S46.8260
SW-846,8260
SW-846,8280
SW-846.8260
1 SW-846.8260
SW-846.8260
SW.846. 8260
SW.846, 8260
SW.846,8260
t SW.846,8260
SW-846, 8260
1 SW.846,8260
1 SW.846,8260
1 SW.846.8260
1 SW.846.8260
t SW.846.8260
1 SW.848.8260
1 SW.846.8260
1 SW.«46.8260
1 SW-846.8260
1 SW.846.8260
1 SW.846.8260
1 SW.846.8260
1 SW-846.8260
1 SW-846.8260
1 SW-846.8260
1 SW.846.8260
1 SW.846.8260
1 SW.846.8260
1 SW.846.8260
1 SW.846.8260
1 SW.848.8260
1 SW.846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-84e,8260
1 SW-846,8260
1 SW-846,7740
1 SW-846,7481
1 SW-848,7471A
1 SW-846,7060
1 SW-846,6010
1 SW-848,6010
1 SW-848,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,3050
1 SOP 420
1 SOP 302
Analyst
CRS
MMR
MMR
MMR
MMR
IvIMR
MMR
IVlnR
MMR
MMR
MMR
MMR
nWnfK
MMR
MMR
lUIMR
IvIViR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
IMMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
VMR
MMR
IVIVIR
IVIVIR
NInR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
NInR
MMR
MMR
MMR
MMR
MMR
IVIVIR
IVIVIR
CRS
CRS
KEN
CRS
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KMS
CRS
Test Date
0^06*711:49
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*716:55
0304*7 16:55
0304*7 16:55
0304*716:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304/97 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 1655
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*716:55
0304*7 16:55
0304*7 16:55
0304*716:55
0304*7 16:55
0304*7 16:55
0304/97 16:55
0304*7 16:55
0304/97 1655
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304/97 16:55
0304*716:55
0304/97 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*7 16:55
0304*716:55
05/02*715:42
05*5*7 13:01
04/10*711:28
05/01*7 18:13
04/11*714:15
04/11*714:15
04/11*714:15
04/11*714:15
04/11*7 14:15
04/11*714:15
04/11*714:15
04/11*714:15
04*9*7 00:00
0307*714:41
0404*714:14
Page 15of 19
if'i -lt-»
IsamplelD
630-20-6
71.556
79.34-5
79.00-5
75.34-3
75.35-4
563^8-6
87.61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
7S-0O-3
67-66-3
. 74-87-3
156-59-4
: ZOEC 88-9, M-136
Tjs«t Parflnwter
CESIUM
1,1,12-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1.1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
12.3-TRICHLOROBENZENE
12.3-TRICHLOROPROPANE
12,4-TRICHLOROBENZENE
12.4-TRIMETHYLBENZENE
12-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-OICHLOROBENZENE
12-DICHLOROETHANE
1,2-OICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-OICHLOROPROPANE
1,4-DICHLOROBENZENE
22-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
/ICETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-12-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1
74-95-3
7S-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZfcNE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
79-01-6
75-69-4
75-01-4
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
SELENIUM
MOLYBDENUM
MERCURY
ARSENIC
ALUMNUM
BARIUM
CADMIUM
CHROMUM
COBALT
COPPER
LEAD
SILVER
ICP/GFAA METALS DIGESTION
HMX
PERCHLORATE
Result
222
u
u u
u u
u u
u u , u
u u u u
u u
u u
u u
u u u u
u u u u u
u u u
u u u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u u u 2.9 J
u u u 0
u 5.5
10400
98
u 14
2.9
9
U
.3
U
4.1
Units
ug/g
ugflcg
ug/kg
ug/kg
ug/kg
ug/kg
ugrtcg
ugflcg
ugrtcg
ugrtcg
ugrttg
ugrtig
ugrttg
ugrtig
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugflcg
ugflcg
ugflcg
ugflcg
ugrtcg
ugrtcg
ugflcg
ugflcg
ugrtcg
ug/kg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugflcg
ugflcg
ugrtcg
ugflcg
ugrtcg
ugrtcg
ug/kg
ugrtcg
ugflcg
ugflcg
ugflcg
ugflcg
ugflcg
ugflcg
ugflcg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
LablD:L879-10 Collect Oate: 03/19^714:37 |
Det
Umit
76
2
2
.3
2
.1
.6
2
2
2
2
2
2
2
.1
2
2
2
2
2
2
2
10
2
10
2
.2
10
10
.2
.2
.2
.3
.1
.4
.3
2
.4
.4
.6
.2
2
.3
.2
2
.3
2
2
.2
.3
.2
2
.2
.2
.2
.2
.2
.9
.3
.2
2
.3
.3
.4
1.3
2
.01
1.3
1.6
.06
.1
.3
.1
.1
1.6
2
.5
1.5
Rep. Dil.
UmH Factor M«th94
255 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
4.3
1.3
.04
4.3
8
.3
.6
1.6
.6
.6
8
.96
.5
7.4
Thiokol SOP 30
SW-846,8260
SW-846,8260
SW-846,8260
SW-846,8200
SW-846,8260
SW-846, 8260
SW-846,8200
SW-846,8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846,8260
SW.846,8260
SW-846,8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.846,8260
SW-848, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-848, 8260
SW-846,8260
SW-848, 8260
SW.846, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-848,8260
SW-846, 8260
1 SW-846,8260
t SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
t SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW.«46,8260
1 SW-848,8260
1 SW.846,8260
1 SW.848,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,7740
1 SW-846.7481
1 SW-846,7471A
1 SW-846,7060
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,3050
1 SOP 420
1 SOP 302
Analyst
CRS
MMR
MMR
MMR
nVUiR
MMR
InMR
MMR
MMR
MMR
HWnR
MMR
MMR
MIMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
IWnR
MMR
nWnR
MMR
rtwnn
MMR
MMR
MMR
MMR
MMR
MMR
NInR
MMR
MMR
HnviR
NIViR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
IWnR
MMR
MMR
NInR
WIVw\
MMR
MMR
MIMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
CRS
CRS
KEN
CRS
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KMS
CRS
Test Date
06/06*711:49
0304*7 17:29
0304*7 17:29
0304*7 17:29
0304*7 17:29
0304*7 17:29
0304*7 17:29
0304*7 1729
0304*7 17:29
0304*7 17:29
0304*7 1729
0304*717:29
0304*717:29
0304*717:29
0304*7 17:29
0304*7 17:29
0304*7 17:29
0304*7 17:29
0304*717:29
0304*717:29
0304*717:29
03/24/97 17:29
0304*7 17:29
0304*7 17:29
0304*7 17:29
0304*7 17:29
0304*7 17:29
0304*7 1729
0304*7 1729
0304*7 1729
0304*71729
0304*717:29
0304/9717:29
0304*717:29
0304*7 17:29
0304*7 17:29
0304*7 17:29
0304*7 17:29
0304*7 17:29
03O4/97 17:29
0304*7 17:29
0304*7 17:29
0304*7 17:29
0304*7 17:29
0304*7 17:29
0304*7 17:29
0304*717:29
0304*7 1729
0304*717:29
0304/971729
0304/9717:29
0304/9717:29
0304/9717:29
0304*7 17:29
0304*7 17:29
0304*7 17:29
03/24*7 17:29
0304*7 17:29
0304*717:29
0304*717:29
0304*7 17:29
0304*7 1729
0304*717:29
0304*7 1729
05*2*7 15:51
05*5*7 13:10
04/10*7 11:31
05*1*7 18:23
04(11*7 14:18
04/11*7 14:18
04/11*7 14:18
04/11*714:18
04/11*714:18
04/11*714.18
04/11*714:18
04/11*714:18
04*9*7 00:00
0307/9714:49
0404*7 14:22
Page 16of 19
IsamplelD
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73.1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
: ZOEC 106.3-i M-136
Test Parameter
CESIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1.TRICHLOROETHANE
1,12,2-TET HACHLOROETHANE
1,1,2.TRICHLOROETHANE
1,1-DICHLOROeTHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2.3-TRICHLOROBENZENE
1.2.3-TRICHLOROPROPANE
1.2.4-TRICHLOROBENZENE
1.2.4.TRIMETHYLBENZENE
1.2-DIBROMO-3-CHLOROPROPAN
12-DIBROMOETHANE
1.2-DICHLOROBENZENE
1.2-DICHLOROETHANE
1.2-DICHLOROPROPANE
1.3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1.3-DICHLOROPROPANE
1.4-DICHLOROBENZENE
2.2-OICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BR0M10METHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-12-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETH/VNE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-12-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
79-01-6
75-69-4
75-01-4
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
SELENIUM
MOLYBDENUM
MERCURY
ARSENIC
ALUMNUM
BARIUM
CADMIUM
CHROMIUM
COBALT
COPPER
LEAD
SILVER
ICP/GFAA METALS DIGESTION
HMX
PERCHLORATE
Result
237
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u u
u u u
u u
u u
u u
u u u u
u u u u u
u u u u u
u
u u
u u
u u
u u u u u u 3.1J
u u
u .4
u 5.7
17100
121
.5
fi-
13
U
.2
U
U
Units
ug/g
ugrttg
ugrttg
ugrttg
ugflcg
ugflcg
ugfltg
ugrttg
ugflcg
ugrttg
ugrttg
ugrtcg
ugrttg
ugrtcg
ugrtig
ugrttg
ugrttg
ug/kg
ugrtcg
ugrtcg
ugrtcg
ugrttg
ugfltg
ugrttg
ugrtcg
ugflcg
ugflcg
ugfltg
ugrttg
ugrttg
ugrtig
ugrttg
ugrttg
ugrttg
ugrttg
ug/kg
ugflcg
ugflcg
ugflcg
ugrtcg
ugrtcg
ugflcg
ugflcg
ugflcg
ugflcg
ugflcg
ug/kg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrttg
ugrttg
ugrttg
ugrtcg
ug/kg
ugrtcg
ugrtcg
ugfltg
ug/kg
ugflcg
ugflcg
ugflcg
ugflcg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/fl
ug/fl
ug/g
ug/g
ug/g
ug/g
LablD:L879-11 Collect Date: 03/18/9714:46 |
Det
UmK
43
2
2
.3
.2
.1
.6
2
.2
.2
.2
2
2
2
.1
2
2
2
.2
.2
2
.2
10
.2
10
.2
.2
10
10
2
2
2
.3
.1
.4
.3
.2
.4
.4
.6
2
2
.3
.2
2
.3
2
2
2
.3
2
2
2
2
2
.2
2
.9
.3
2
2
.3
.3
.4
.7
.1
.01
.7
.9
.04
.07
2
.07
.07
.9
.1
.5
1.5
Rep. DII.
Umit Fai
142 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10 1
10 1
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
2.4
.7
.04
2.4
4.5
2
.4
.9
.4
.4
4.5
.5
.5
7.7
* . •
rtor Method
Thkikol SOP 30
SW.846, 8260
SW.846.8260
SW-448.8260
SW-«46.8260
SW.846.8260
SW.846.8260
SW.846, 8260
SW-846,8260
SW-846,8260
SW.846,8260
SW-846,8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846,8260
SW.846, 8260
SW.846,8260
SW.846,8260
SW.846, 8260
SW.846.8260
SW-846.8260
SW-846. 8260
SW-846. 8260
SW-848. 8260
SW-846. 8260
SW-846. 8260
SW.846.8260
SW-846. 8260
i SW-846,8260
SW-846,8260
SW-846, 8260
1 SW-846.8260
1 SW-846.8260
SW-846. 8260
1 SW-846.8260
t SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
t SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846.8260
1 SW-846.8260
1 SW-846.8260
1 SW-846.8260
1 SW-846.8260
1 SW-846.8260
1 SW-846.8260
1 SW-846,8260
1 SW.846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,7740
1 SW-846,7481
1 SW-846,7471A
1 SW-846,7060
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846.6010
1 SW-846.6010
1 SW-846.3050
1 SOP 420
1 SOP 302
Analyst
CRS
MMR
Rw/IR
MMR
MMR
MMR
IVIVIR
MMR
MMR
IVIVIR
NRflR
MMR
nwVIR
MMR
MMR
MMR
BWVIR
MMR
IMMR
lUIMR
MMR
NInR
MMR
MIMR
MMR
MMR
MMR
vnnn
n/IMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
IVIVIR
MMR
MMR
MMR
NIMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
n/nlR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
CRS
CRS
KEN
CRS
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KMS
CRS
Test Date
05*6*711:51
0304*7 18:03
0304*7 18:03
0304*7 18fl3
0304*7 18:03
0304*7 18:03
0304*718:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0»24*7 18:03
0304*7 18K)3
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18K)3
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18K)3
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304/97 18:03
0304/97 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304/97 18:03
0304/97 18:03
0304/97 18:03
0304*7 18:03
0304/97 18:03
0304/97 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*7 18:03
0304*718:03
0304*7 18:03
0304*7 18:03
0304*718:03
05/02*7 16:00
05/05*7 13:20
04/10*7 11:35
05*1*7 18:32
04/11*714:43
04/11*714:43
04/11*714:43
04/11*714:43
04/11*714:43
04/11*714:43
04/11*714:43
04/11*714:43
04*9*7 00:00
0307*7 14:57
0404*7 14:31
Page 17of 19
Sample ID: DISPERSION AREA LablD:L879-12 Collect Date: 03/19/9714:53 |
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
Test Parameter
CESIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHAJ«
1,12.2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
12-DICHLOROETHANE
12-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4<:HLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMfc THANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
79-01-6
75-69-4
75-01-4
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
SELENIUM
MOLYBDENUM
MERCURY
ARSENIC
ALUMINUM
BARIUM
CADMIUM
CHROMIUM
COBALT
COPPER
LEAD
SILVER
ICP/GFAA METALS DIGESTION
HMX
PERCHLORATE
Result
210
U
U
•J
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
.7
.02
4.1
16200
106
.4
23
6.9
13
U
U
.99
U
Units
ug/g
ug/kg
ua'kg
uq/kg
ugflcg
ug/kg
ugrttg
ug/kg
ug/kg
ug/kg
ugrtcg
ugflcg
ugflcg
ugrtcg
ugrtig
ugrtig
ug/kg
ugrtcg
ugrttg
ugrttg
ugrttg
ugrtcg
ug/kg
ugrtcg
ugrtcg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ugrttg
ug/kg
ugrttg
ugfltg
ug/kg
ugrttg
ugrttg
ugrttg
ugfltg
ugrttg
ugrttg
ugrttg
ugrttg
ugrtcg
ugrtcg
ugflcg
ugrtcg
ug/kg
ugrtcg
ugrtcg
ugrtcg
ugrtcg
ugrttg
ugrttg
ug/kg
ug/kg
ugrtcg
ugrtcg
ugflcg
ugflcg
ug/kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Det
Limit
52
2
2
.3
2
.1
.6
.2
.2
.2
2
2
2
2
.1
.2
.2
.2
.2
.2
.2
2
10
2
10
2
.2
10
10
.2
.2
2
.3
.1
.4
.3
2
.4
.4
.6
.2
.2
.3
2
2
.3
2
2
2
.3
.2
.2
.2
.2
.2
.2
2
.9
.3
2
.2
.3
.3
.4
.9
.1
.01
.9
1.1
.04
.09
.2
.09
.09
1.1
.1
.5
1.4
Rep. DII.
Limtt Factor
175 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
3 1
.9 1
.04 1
3 1
5.5 1
.2 1
.4 1
1.1 1
.4 1
.4 1
5.5 1
.7 1
.5 1
7.1 1
Method
Thiokol SOP 30
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846. 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846.8260
SW-846. 8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW'846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46,8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 7740
SW-846, 7481
SW-846, 7471A
SW-846, 7060
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
SOP 420
SOP 302
Analyst
CRS
MMR
MMR
MMR
MMR
IMMR
MAR
MJIR
MMR
MMR
MMR
MMR
MMR
IvIMR
MJK
MMR
MMR
MMR
MMR
MMR
MMR
MMR
^MR
MMR
MMR
MMR
MMR
MMR
MMR
M^R
MIMR
MMR
NMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
IVnIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
NInR
InnR
MJH
CRS
CRS
KEN
CRS
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KMS
CRS
Test Date
05/06*711:53
0304*7 18:37
0304*7 18:37
0304*7 18:37
0304/97 18:37
0304/97 18:37
0304/97 18:37
0304/97 18:37
0304*7 18:37
0304*7 18:37
0304/97 18:37
0304*7 18:37
0304*7 18:37
0304*7 18:37
0304*7 18:37
0304*7 18:37
03/24/97 18:37
03/24/97 18:37
03/24*7 18:37
0304*7 18:37
0304*7 18:37
0304*7 18:37
0304*7 18:37
0304/9718:37
0304*7 18:37
0304/97 18:37
03/24*7 18:37
0304*7 18:37
0304*7 18:37
0304*7 18:37
0304*7 18:37
0304*7 18:37
0304/97 18:37
0304/97 18:37
0304*718:37
0304/97 18:37
0304*7 18:37
0304*7 18:37
0304*7 18:37
0304*7 18:37
0304*7 18:37
0304*7 18:37
0304*7 18:37
0304/97 18:37
0304/9718:37
0304*7 18:37
0304*7 18:37
0304*7 18:37
0304*7 18:37
0304*7 18:37
0304/97 18:37
0304*7 18:37
0304*7 18:37
0304/97 18:37
0304/97 18:37
0304/97 18:37
0304*7 18:37
0304*7 18:37
0304*7 18:37
0304*7 18:37
0304*7 18:37
0304*7 18:37
0304/9718:37
0304*7 18:37
05/02*7 16:09
05/05/97 13:36
04/10/9711:39
05/01*7 18:41
04/11*7 14:46
04/11*714:46
04/11*7 14:46
04/11*7 14:46
04/11*7 14:46
04/11/9714:46
04/11/9714:46
04/11/9714:46
04/09/97 00:00
0307/97 15:05
0404/97 14:39
Page 18of 19
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected but was
below the detection limit.
B Gas Chromatography and Mass Spectral Data Flag. This flag is used when an analyte is found in
the blank as well as the sample
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This flag is used
either when estimating a concentration for tentatively identified compounds or when the data
indicated the presence of a compound that meets the identification criteria but the result is less than
the specified reporting limit (e.g. 3 J with a reporting limit of 10)
Det. Limit Method Detection Limit (approximately three times the signal noise level)
Rep. Limit Reporting Limit is normally the value ofthe lowest standard run with the analysis. The value
is approximately 5 to 10 times the Method Detection Limit
Dil. Factor Dilution Factor - The prepared sample was diluted by this factor because the sample was
too concentrated or due to other interferences in the sample matrix. Any dilution factor
causes an appropriate increase in the method detection limit and reporting limit
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