DSHW-1998-001899 - 0901a0688013a792

PROPULSION GROUP
P.O. BOX 707
BRIGHAM CITY, UT 84302-0707
801.863-3511
THtOKOL
AEROSPACE & INDUSTRIAL TECHNOLOGIES
12 March 1998
8740-FY98-ST067
Scott Anderson, Hazardous Waste Branch Manager
Division of Solid and Hazardous Waste
Department of Environmental Quality
P.O.Box 144880
Salt Lake City, Utah 84114-4880
m] 7 mz
•Jfa/. Department Of Environmental Quiy
Dear Mr. Anderson
Subject: Application for Permit Modification of Thiokol's Corrective Action Management
Unit (CAMU), UTD009081357
Thiokol requests a Class 1 permit modification to amend disposal options of treated soils from
our Corrective Action Management Unit (CAMU). In July 1996, Thiokol submitted a request
to the Utah Division of Solid and Hazardous Waste to modify its Post-Closure Permit to
designate two Solid Waste Management Units (#425 and # 367) and a nearby treatment area
as a Corrective Action Management Unit (CAMU). CAMU designation was granted on 11
July 1997. The requested plan outlined the removal of soils contaminated with silver and
cadmium to risk based levels, and the treatment of soils with slaked lime to eliminate the
hazardous waste characteristic for cadmium. The plan indicated that "ifa recycling facility
willing to accept contaminated soils can be identified, precious metals in soils which are
excavated as part ofthis CAMU plan will be reclaimed" (Section 2.8 RECYCLE OF
METALS, p.6). Unfortimately, in the period between request submittal and the CAMU
approval, Barrick Mercur Gold Mines, Inc., Thiokol's planned reclamation facility ceased
their mining process and notified Thiokol that they will no longer accept our soils. Thiokol
has contacted other mines / mills in northem Utah, westem Nevada and southem Idaho, but
has been unable to identify another facility willing to accept our soils.
Thiokol proposes, following treatment as outlined in the CAMU plan, to dispose ofthe
nonhazardous soils as solid waste in our permitted, onsite, solid waste landflll. The proposed
landflll location is illustrated on Figure 1. The actual disposal area, including the depth ofthe
soil top and bottom will be submitted to the DSHW at the conclusion ofthe project, as part of
the CAMU report. An estimated 300 cubic yards of treated soil will be disposed in the
landfill. A sampling plan for the treated soils which will be sampled for toxicity characteristic
prior to disposal, is attached as Appendix 1. If any ofthe soils exhibit the toxicity
characteristic following treatment, the soil will be retreated with additional water and/or lime.
Approximately 30 days after retreatment, the soils will again be sampled for the toxicity
characteristic. This process will be repeated until the waste no longer exhibits a characteristic
Application for Permit Modification of
Thiokors Corrective Action Management Unit
12 March 1998 Page 2
of toxicity. If the soils cannot be rendered nonhazardous, they will be handled and disposed
of as hazardous waste.
Thiokol also proposes to include as part ofthe CAMU, SWMU # 444, a dry well from
building M-19A, which processed and disposed of photographic waste streams. The soils
from the drywell contain wastes similar in nature to the CiAMU sites, with no significant
quantities of volatile organic compounds (VOC). The laboratory report for volatile organics
and selected metals in soils fi-om #444 are enclosed with this request.
If you have questions or need additional information, please call John Holladay at 863-6895.
Sincerely
J. D. Thompson, Director
Environmental, Fire & Security
Enclosures: Corrective Action Management Unit Sampling Plan
Laboratory report (volatile organics) for M-i9A drywell (#444)
Laboratory report (selected metals) for M-19A drywell (#444)
Figure 1: Landfill, M-336 CAMU Soil Placement
THIOKOL
CORRECTIVE ACTION MANAGEMENT UNIT
SAMPLING PLAN
1.0 Thiokol Corrective Action Management Unit (CAMU)
The Utah Division of Solid and Hazardous Waste has designated two Solid Waste
Management Units (#425 and # 367) and a nearby treatment area as a Corrective Action
Management Unit (CAMU). SWMU #444 may also be included in the CAMU if approved by
the DSHW. The CAMU plan outlined the removal of soils contaminated with silver and
cadmiiun to risk based levels, and the treatment of soils with slaked lime to eliminate the
hazardous waste characteristic for cadmium. This Sampling plan will be used for verification
sampling ofthe excavated soils.
1.1 Soil Sampling
Following the treatment of contaminated soils, samples will be collected and analyzed to
verify that hazardous characteristics (metals) have been removed and the soils are no longer
hazardous. The samples will be analyzed using the Toxic Characteristic Leaching Process
(TCLP). These samples will be collected using a hand auger or scoop at points on a
systematic grid. The soils will be graded to approximately two feet depth on the building
M-572 asphalt surface. Sample locations will be defined by gridding the area of excavation
into 2 ft linear grids. Four samples will be analyzed using TCLP method. Each sample
will consist of a composite of three aliquots, totaling approximately eight ounces of soil.
Each aliquot location will be selected using a digital random number generator. The
samples will be 0-1 foot deep soil cores.
1.2 Sample Collection Methods
The samples will be collected using a stainless steel scoop and hand shovel, or scooped
directly into sampling containers in the following manner:
1) Using a decontaminated stainless steel scoop, or steel shovel, the desired quantity of
soil is collected from the surface ofthe sampling site and consolidated into one
container. Where the soil is loosely consolidated, samples are collected directly into
the sampling containers without use ofa scoop. Containers shall consist of precleaned
8 oz. wide-mouth glass bottles with a Teflon coated seal.
2) Custody seals shall be placed on the bottles, and the samples shall be stored in a cooler
or refrigerator at approximately four degrees Centigrade.
3) The samples will be transported to Thiokol's Environmental Laboratory for analysis.
1.3 Laboratory Analytical Methods
Analyses ofthe soil samples will be performed by a laboratory certified by the State of Utah to
perform the analyses using EPA approved TCLP method. The analytical results and other
relevant data (soil profiles, laboratory QA/QC, actual analytical methods, etc.) will be
organized and included as part of the CAMU Closure Report.
1.4 Quality Assurance
One field blank will be collected and analyzed with the four soil samples. Laboratory
QA/QC will conform to USEPA protocol and standards, and will be included as part of the
CAMU Closure Report.
1.5 Schedule
The soils will be sampled approximately 45 days after all materials from the SWMU's have
been excavated and treated (approximately 15 May 1998). Results should be available
approximately two weeks later, and will be submitted to the DSHW for approval prior to
disposal of treated soils.
ENVIRONMENTAL LAB WORK REQUEST^ ^ r^Q ^/n Cp
TO. TraOKOL ENVIRONMENTAL LABORATORY LWR No. E10633
nOM: /I, F. LUA-LlCef^
ORCANIZAnON ^/Uo/fzd ^^(^11-
BCTDBION
MAIL STOP
WORK ORDER oosTCBnm WORKORDEX •^•I'
REPORT RBULTS TOi
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE
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LOCATION
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TEST RENURKS
d</, Cr, A^ , Ph, Ml' - ^C/O
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CHAIN OF CUSTODY
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-^^\iilttli' iVyV_-9-(C^4 \06r\
RECEIVED BV DATE TIME
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FOR LABORATORY USE ONLY
DATT; ooMPixrn) I>ATE RB>ORTED SIGNATlllE
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Report:
Workorder Comment*?
NITRIC ACID WAS USED FOR THE SILVER EXTRACTIONS ON
SAMPLES OIB, 02B, OSB, AND 04B.
^ >^'<y^
Certified^
I
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•
Page n-.l
This is to certify that the following samples were analyzed using good M>oratory practices
^ to show the foUowing results.
I
Sample ID: M-19A DRYWELL, 1 FT.
KST
dlgbc
Lab ID: 9409009-OlA Collected: 09/15/94 09:30:00
RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
• Id DlgeBtlon
fa dmium
ir omium
Lead
.ckel
Silver
t
Lei
I
10/04/94
2.26
855
366
370
234
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
0.1
0.4
1.8
0.70
0.2
10/04/94
10/06/94
10/06/94
10/06/94
10/06/94
10/06/94
HWB
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
I
|bm] pie ID: M-19A DRYWELL, 3 FT. Lab ID: 9409009-02A Collected: 09/15/94 09:40:00
RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
p:id Digestion
^admium
Siromium
r
Fickel
,lver
I
Pam]
10/04/94
4.73
1510
325
395
253
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.3
0.51
0.2
10/04/94
10/06/94
10/06/94
10/06/94
10/06/94
10/06/94
MWB
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-a46,
SW-846,
3050
6010
6010
6010
6010
6010
.pie ID: M-39 DRYWELL, 1 FT. Lab ID: 9409009-03A CoUected: 09/15/94 10:10:00
r RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Pntisony
^dfflium
'Oir omium
10/04/94
7.34
8.15
75.2
DATE
ug/g
ug/g
ug/g
3.4
0.1
0.3
10/04/94
10/06/94
10/06/94
10/06/94
MWB
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-84G,
3050
6010
6010
6010
I
I
Page #: 3
14:09 btober 19, 1994
fcnple ID: M-39 DRYWELL, 1 FT.
CSBTIFIGATE OF ANALYSE
V RESULTS BY SAMPLE fP
Lab ID: 9409009-03A CoUected: 09/15/94 U
g0<; RESULT UNITS DETECTION ANALYZED BY
LIMIT
ead
Lver I
Smple ID: M-39 DRYWELL, 3 FT.
246
118
ug/g
ug/g
1.7 10/06/94 LVD
0.2 10/06/94 LVD
METHC
SW-84
SW-84
?b
Lab ID: 9409009-04A CoUected: 09/15/94 1^. ^u.v/v/
1^'
«id Digestion
Etlmony
•dniiun
IhxomiuBi
1-
Silver
1
RESULT
10/04/94
5.99
2.75
26.4
156
43.6
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
DETECTION
LIMIT
2.7
0.1
0.3
1.4
0.2
ANALYZED
10/04/94
10/06/94
10/06/94
10/06/94
10/06/94
10/06/94
BY
MWB
LVD
LVD
LVD
LVD
LVD
METHOD/CAS#
SW-846, 3050
SW-846, 6010
SW'846, 6010
SW'846, 6010
SW-846, 6010
SW-346, 6010
|impi
"ST
iple ID: M-I9A DRYWELL, 1 FT. Lab ID: 9409009-OlB CoUected: 09/15/94 09:30:00
lver I
!>ainple ID: M-19A DRYWELL, 3 FT.
RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
7140 ug/g 0.3 10/12/94 LVD SW-846, 6010
Lab ID: 9409009-02B CoUected: 09/15/94 09:40:00
KST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
I
I
I
I
lver 53500 ug/g 0.3 10/12/94 LVD SW-846, 6010
Page #: 4
»)ctoberl9,1994 14:09 CERTIFICATE-OF ANALlfflS
^ RESULTS BY SAMFLE 10
fcmple ID: M-39 DRYWELL, 1 FT. Lab ID: 9409009-03B CoUected: 09/15/94 10:10:00
rSX RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Silver 255 ug/g 0.3 10/12/94 LVD SW-846, 6010
fcmple ID: M-39 DRYWELL, 3 FT. Lab ID: 9409009-04B CoUected: 09/15/94 10:20:00
TEST RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Liver 114 ug/g 0.3 10/12/94 LVD SW-846, GOlO
I
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I
Page#:5
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ENVIRONMENTAL LAB WORK REQUEST Li>^3
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LWR No. El 1502
Login No. 1
WORK ORDER DATE
REPORT RESULTS TO: / ^ y f /
HELEN WARD, MS 301
SAMPLE INFORMATION
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DATE COMPLETED DATE REPORTED
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ENVIRONMENTAL LAB WORK REQUEST
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OKGANIZATION
EXTENSION
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LWR No. E11502
Login No.
COST CENTER WORKORDER itfe? DATE
REPORT RESULTS TO:
HELEN WARD, MS 301
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CHAIN OF CUSTODY
RELINQUISHED BY DATE TIME RECEIVED BY DATE Tl.ME
DATE COMPLETED
FOR LABORATORY USE ONLY
DATE REPORTED SICMATURE
CERTIFICATE OF ANALYSIS
Listing of sample Infornnation and Testing Requested
Monday, Decemt>er22,1997
TESTED FOR Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp, UT 84322
Frank Walker
Projact: Misc. Environmental Testing
Login Number L1283
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-3732
800-863-8080
Lab No Client Number
Test Requested
1 Ll 283-1 M-19A.01
SW-846, 8260
ILI 283-2 M-39-11-97-01
SW-846, 6010
SW-846, 6010
SW-846, 3050
ILI 283-3 M-39-11-97-02
SW-846, 6010
SW-846,6010
SW-846,3050
ILI 283-4 M^9.11-97-03
SW-846,6010
SW-846, 6010
SW-846, 3050
ILI 283-5 M-39-11-97-04
SW-846, 6010
SW-846,6010
SW-846, 3050
IL1283^ M-39-11-97-05
SW-846, 6010
SW-846,6010
SW.846,3050
IL1283-7 M-39-11-97.06
SW-a46, 6010
SW-846, 6010
SW-846, 3050
iL1283-8 M-39-11-97-07
Descrtption
Volatile Organics
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Ag ICP Metais Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals DIgesUon
Ag ICP Metals Analysis (RCRA)
Cd ICP Metais Analysis (RCRA)
ICP/GFAA Metals DigesUon
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Received
11/10/97
11/10/97
11/10/97
11/10/97
11/10/97
11/10/97
11/10/97
11/10/97
CollectDate/Time
Matrix
11/06/9711:15 1
Soil
11/06/9710:48 I
Soil
Soil
Son
11/06/9710:49 1
Soil
Soil
Soil
11/06/9710:51 1
Soil
Soil
Soil
11/06/9710:52 1
Soil
Soli
Soil
11/06/9710:53 1
Soil
Soil
Soil
11/06/97 10.54 1
Soil
Son
Soil
11/06/9710:55 1
SW-846, 6010
SW.846, 6010
SW-846,3050
SW-846,6010
SW-846,6010
SW-846, 3050
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Soil
Son
Soil
IL1283-9 M-39-11-97-08
SW-846, 6010
SW-846, 6010
SW-846,3050
ILI283-10 M-39-11-97-09
SW-846, 6010
SW-846, 6010
SW-846,3050
lL1283.11 M^9-1147-10
Ag ICP Melals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
11/10/97
11/10/97
11/10/97
11/06/97 10:56
Soil
Sou
Soil
11/06«7 10:57
Soil
Soil
Soil
11/06/97 10:fiR
1
1
1 Soil
Soil
Soli
i I Paae 1 of 7
Ll 283-12 M-636-11-97-01 ii/ff^ 117TO/97 11/10/97 09:34
SW-846,6010
SW-&46,6010
SW-846,3050
Ag ICP Metals Analysts (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
SW-846,6010
SW-846,6010
SW-846, 3050
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Soil
Soil
Soil
IL1283-13 M-636-11-97-02
SW-846, 6010
SW'846, 6010
SW-846,3050
IL1283-14 M-636-11-97-03
SW-846, 6010
SW-846,6010
SW-846,3050
IL1283-15 M-636-11-97-04
SW-846,6010
SW-846,6010
SW-846, 3050
IL1283-16 M-636-11-97-05
SW-846, 6010
. SW-846,6010
SW-846,3050
IL12B3-17 M-636-11-97-06
SW-846,6010
SW-846,6010
SW-846, 3050
ILI 283-18 M-636-11-97-07
SW-846, 6010
SW-846, 6010
SW-846, 3050
1 Ll 283-19 M.636-11 -97-08
SW.846,6010
SW-846,6010
SW-846, 3050
ILI 283-20 M.636-11-97-09
SW-846, 6010
SW-846,6010
SW-846,3050
kl283-21 M.636-11-97-10
SW-846,6010
SW-«46,6010
SW.846,3050
ILI 283.22 M.636.11-97.11
SW.e46, 6010
SW.846, 6010
SW.846, 3050
IL1283.23 M-636-11-97.12
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metais Analysis (RCRA)
ICP/GFAA Metals DigesUon
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP M^ls Analysis (RCRA)
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals DigesUon
11/10/97
11/10/97
11/10/97
11/10/97
11M0/97
11/10/97
11/10/97
11/10/97
11/10/97
11/10/97
11/10/97
11/10/97 09.37
Soil
Soil
Soil
11/10/97 09:40
Soil
Soil
Soil
11/10/97 09:49
Soil
Soil
Soil
11/10/97 09:51
Soil
Soil
Sou
11/10/97 09-.53
Soil
Soil
Soil
11/10/97 09:56
Soil
Soil
Soil
11/10/97 09.58
Soil
Soil
Soil
11/10/9710:00
Soil
Soil
Soil
11/10/9710:02
Soil
Soil
Soil
11/10/9710:03
Soil
Soil
Son
11/10/9710:05
1
1
1 Soil
Soil
Soil
Certified By S^v^ nZf-^^?
Janifes M. Anderson. QC Officer Date
Jt\i% certifies ttiat tfie following samples were analyzed using good laboratory practices to stiow ttie following results:
Page 2of7
Listing of Results by Samp iple
1 Sample ID:
CAS
Numtier
630-20-6
71.5M
79-34.5
7M(^
75-344
75-35.4
563-564
87-414
06.1M
12M2-1
95-6»4
96-12-8
106-93-4
9540-1
107-06-2
78474
106474
541.73.1
142-284
106-46-7
590-20-7
78-934
95-494
591-784
106-434
99474
108-10-1
67-64-1
71-43.2
10846-1
74-974
75-274
75-25-2
74-834
56-234
108-90-7
75404
67464
74474
156-594
M-19A-01
Testpqrflm»t«r
1.1,1,2-TETRACHLOROETHANE
1.1.1-TRICHLOROETHANE
1.1,2>TETRACHLOROETHANE
1.1 i-TRICHLOROETHANE
1,1-OlCHLOROETHANE
1.1-OICHLOROETHENE
1,1-OlCHLOROPROPENE
1,2.3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2.4-TRICHLOROBENZENE
1.2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
U-OIBROMOETHANE
1,2-DICHLOROBENZENE
1 ^DICHLOROETHANE
U-DICHLOROPROPANE
1,3.5-TRIMETHYLBENZENE
1,3.DICHLOROBENZENE
I.3.DICHLOROPROPANE
1,4.0ICHLOROBENZENE
2,2-DICHLOROPROPANE
2.BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4<:HLOROTOLUENE
4.ISOPROPYLTOLUENE
4.METHYL-2^»ENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
ClS-1,2.DICHL0R0ETHENE
10061414 CtS-1,3.DlCHLOROPROPENE
124-48-1
74-954
75-714
10041-4
87-684
9S-82-4
108-384
7549-2
104414
103-65-1
91-204
95-474
135-984
100424
98464
127-184
108-884
156404
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
tSOPROPVLBEtCENE
M,P.XYLENE
METHYLENE CHLORIOE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHniALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-OlCHLOROETHENE
10061-024 TRANS-1,3.DICHLOROPROPENE
79414
75-694
75414
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE.
VINYL CHLORDE
1 Sample ID: M^l 1-97-01
TestparaiTietei
CADMIUM
SILVER
ICP/GFAA METALS DIGESTION
Result
u
1.1JB
U
U
U
U
U
U
U
U
U
U
U
u U
U
U
u u
u
u u
u
u u
u
u
u
u u
u u
u
u u
u
u
u u
u
u u
u
u
u u u
u u
u
u u
u
u u u
u u u u
Unite
ugfliB
ug/kg
U9fl<8
ug/kg
ugflig
ugftg
ugrtiQ
ug/kg
ugntg
ugAg
ugAg
ugAg
ugrtio
ugftg
ugAig
ugrttg
ugflig
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
22JB ug/kg
U
u
Result
228
284
ug/kg
ugAg
Unite
ug/g
ug/g
Lab ID: L1263.1
Det Rep. OIL
Unnit 1
2
2
.3
2
.1
.6
2
2
2
2
2
2
2
.1
2
2
2
2
2
2
2
10
.2
10
.2
2
10
10
2
2
2
.3
.1
.4
.3
2
.4
.4
.6
.2
2
.3
2
2
.3
.2
2
2
.3
.2
.2
2
2
2
2
2
a
.3
2
2
.3
.3
.4
Limit Factor
16
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
•10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Collect Date: 11/06/9711:15 (
Method
SW-a46,8260
SW-646,6260
SW-846.8260
SW-446,8260
SW-846, 8260
SW-846,8260
SW-846,8260
SW-846.8260
SW-846.8260
SW-846,8260
SW-846,8260
SW-846.8260
SW-846.8260
SW-646.8260
SW-846,8260
SW-446,8260
SW446.B260
SW-846, 8260
SW-846,8260
SW-846,8260
SW-84e,8260
SW448,8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-646. 8260
SW-446.8260
SW-846.8260
SW44e. 8260
SW446. 8260
SW-846.8280
SW-846.8260
SW-848.S2eO
SW-846,8260
SW-846,8260
SW-646.8260
SW-646.8260
SW-446.8260
SW-846.8260
SW-846.8260
SW446,8260
SW446, 8260
SW-848,8260
SW-846.8260
SW446.8260
SW-846.8260
SW-44S. 8200
SW-446,8260
SW-S46.8260
SW-846.8260
SW-&46. 8260
SW-846,8260
SW-848,8260
SW-846, 8260
sw-84e,62eo
SW-846.8260
SW-646.8260
SW-646.8260
SW-646. 8260
SW-446.8260
SW446.8260
SW446.8260
SW-846,8260
Ana'yit
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
JY
LablD:L12B3.2 Collect Date:
DeL
Limit
.1
.2
Rep.
Limtt
.7
1.1
DIL
Factor Meth94
1
1
1
SW-846, 6010
SW446.6010
SW-846,3050
Test Date
11/17/97 13:00
11/17/97 13.00
11/17/97 13:00
11/17/9713:00
11/17/97 13«)
11/17/97 13.-00
11/17/97 13.-00
11/17/97 13:00
11/17/97 13.00
11/17/97 13«)
11/17/97 13fl0
11/17/9713:00
11/17/97 13:00
11/17/97 13fl0
11/17/9713.00
11/17/9713:00
11/17/97 13:00
11/17/97 13:00
11/17/97 13.00
11/17/9713.00
11/17/97 13:00
11/17/07 13:00
11/17/97 13fl0
11/17/97 13:00
11/17/97 13:00
11/17/0713:00
11/17/97 13:00
11/17/9713.00
11/17/97 13:00
11/17/9713:00
11/17/9713.00
11/17/97 13.00
11/17/97 13:00
11/17/9713:00
11/17/97 13.00
11/17/97 13«)
11/17/9713:00
11/17/9713:00
11/17/97 13:00
11/17/9713:00
11/17/9713:00
11/17/9713:00
11/17/97 13:00
11/17/9713:00
11/17/9713:00
11/17/9713:00
11/17/97 13:00
11/17/9713:00
11/17/9713:00
11/17/9713:00
11/17/97 13.«)
11/17/9713:00
11/17/97 13.-00
11/17/9713:00
11)17/97 13:00
11/17/9713:00
11/17/97 13«)
11/17/9713:00
11/17«7 13:00
11/17/97 13:00
11/17/9713:00
11/17/9713:00
11/17/97 13.-00
11/06«710:48 |
Analyst Test Date
KWB 12/ia«7 09:56
KWB 12/18/97 09:56
LVD 1 12/10«7 00:00
Page 3of7
I Sample ID: M.39.11.97.02 Lab ID: Ll 283.3 Collect Date: 11/06/9710:49
Test Parameter
CADMIUM
SILVER
ICP/GFAA METALS DIGESTION
Result Units
ug/g
ug/g
21
21
DeL
Limit
.1
2
Rep.
Limit
.6
3
Dil.
Factor
1
1
1
Mettiod
SW446,6010
SW446,6010
SW-846.3050
Analyst
KWB
KWB
LVD
Test Date
12/18/97 09:59
12/18/97 09:59
12/10/97 00:00
I Sample ID: M.39-11-97-03 Lab ID: L12834 Collect Date: 11/06/9710:51
Test Parameter
CADMIUM
SILVER
ICP/GFAA METALS DIGESTION
Result Unite
ug/g
ug/g
70
595
DeL
Umlt
.1
2
Rep. DIL
Umlt Factor Method
SW-846,6010
SW-646,6010
SW-646,3050
Analyst Test Date
KWB
KWB
LVD
12/18/97 10:02
12/18/97 10:02
12/10/97 OOM
I Sample ID: M-39-11-97-04 UblD:L128» Collect Date: 11/06/9710:52
Test Parameter
CADMIUM
SILVER
ICP/GFAA METALS DIGESTION
Result Units
4.9 ug/g
242 ug/g
DeL
Limit
.1
2
Rep. DiL
Limit Factor Method
SW448,6010
SW-846,6010
SW-846,3050
Analyst Test Date
KWB 12/18/9710:05
KWB 12/18/9710:05
LVD 12/10/97 00:00
I Sample ID: M.39.11.97.05 Lab ID: Ll 2834 Collect Date: 11/06/9710:53 I
Test Parameter
CADMIUM
SILVER
ICP/GFAA METALS DIGESTION
Result Units
13 ug/g
29 ug/g
DeL
Limtt
.1
2
Rep. DiL
Lirntt Factor
.6
.9
Method
SW446,6010
SW-846.6010
SW.846.3050
Analyst Test Date
KWB 12/18/9710:08
KWB 12/18/9710:08
LVD 12/10^7 00:00
I Sample ID: M-39-11-974)6 Lab ID: L1283.7 Collect Date: 11/06/9710:54 |
Test Parameter
CADMIUM
SILVER
ICP/GFAA METALS DIGESTION
Resutt Unfti
ug/g
ug/g
S3
124
DeL
Limtt
.1
.2
Rep.
Limtt
DIL
Factor
1
1
1
Method
SW446.6010
SW446.6010
SW446.3050
Analyst Test Date
KWB 12/18n710:11
KWB 12/18/9710:11
LVD 12/10/97 00:00
I Sample ID: M.39.11.97.07 Lab ID: Ll 2834 Collect Date: 11/06/9710:55
Test Parameter
CADMIUM
SILVER
ICP/GFAA MET/U.S DIGESTION
ResuU
26
441
Untts
ug/g
ug/g
[)eL
Limtt
.1
2
Rep. DiL
Limtt Factor
.6
.9
Method
SW-846,6010
SW-846, 6010
SW-846,3050
Analyst Test Date
KWB 12/18/9710:14
KWB 12/18/9710:14
LVD 12/10/97 00:00
I Sample ID: M.39.11.97.08 Lab ID: L1283.9 Collect Date: 11/06/9710.56
Test Parameter
CADMIUM
SILVER
ICP/GFAA METALS DIGESTION
Result Untts
1.1 ug/g
ug/g 16
DeL Rep. DiL
Limtt Limtt Factor Method
.1 .5 1 SW-846.6010
.1 .7 1 SW446.6010
1 SW-446,3050
Analyst Test Date
KWB 12/18ffl710:17
KWB 12/18ffl710:17
LVD 12/10^7 00:00
I Sample ID: M.39.11.97.09 LablD:L1283.10 Collect Date: 11/06/9710:57 |
Test Parameter
CADMIUM
SILVER
ICP/GFAA METALS DIGESnON
DeL Rep. DiL
Resmt Untts Umtt Limtt Factor Method
5.5 ug/g .1 J6 1 SW446,6010
IS ug/g .2 .9 1 SW-646,6010
1 SW-846.3050
Analvst Test Date
KWB 12/18/9710:20
KWB 12/18/971020
LVD 12/10/97 00:m
I Sample ID: M-39-11-97-10 Lab ID: Ll 283-11 Collect Date: 11/06/9710:58
Test Parameter
CADMIUM
SILVER
ICP/GFAA METALS DlGESnON
Resqn
45
133
Unit?
ug/g
ufl/B
DeL Rep. DiL
Limtt Limtt Factor Method
.1 .5 1 SW-846,6010
.2 .8 1 SW-846,6010
1 SW-846,3050
Analyst Test Date
KWB 12/18/971023
KWB 12/16/971023
LVD 12/10/97 00:00
si
Page 4 of 7
I Sample ID: M-636-11-97^ Lab ID: Ll 283-12 Collect Date: 11/10/97 09:34 |
Test Parameter
CADMIUM
SILVER
ICP/GFAA METALS DIGESTION
DeL Rep. DiL
Resutt Untts Limtt Limtt Factor Method
70 ug/g .1 .7 1 SW-846,6010
510 ug/g 2 11 SW-846.6010
1 SW-846,3050
Analyst Test Date
KWB 12/18«710:47
KWB 12/18/9710:47
LVD 12/10/97 00:00
I Sample ID: M-636.11-97-02 Lab ID: Ll 283-13 Collect Date: 11/10/97 09:37
Test Parameter
CADMIUM
SILVER
ICP/GFAA METALS DlGESnON
DeL Rep. DiL
Resutt Untts Limtt Limtt Factor Method
2 ug/g .1 .6 1 SW-846,6010
3£ ug/g 2 3 1 SW-846,6010
1 SW-446,3050
Analyst Test Date
KWB 12/18/9710:50
KWB 12/18/9710:50
LVD 12/10/97 00K»
I SamplelD: M-636-11-97-03 Lab ID: L1283-14 Collect Date: 11/10/9709:40
Teat Parameter
CADMIUM
SILVER
ICP/GFAA METALS DIGESTION
BesyH Untts
ug/g
ug/g
.7
5.6
Det Rep. DIL
Umtt Limtt Factor Method
.1 .6 1 SW-846.6010
2 S 1 SW-646,6010
1 SW-846,3050
Analyst Test Date
KWB
KWB
LVD
12/18/97 10:53
12/18/97 10:53
12/10/97 00:00
[Sample ID: M-636-11-97-04 LablD:L1283-15 Collect Date: 11/10/97 09:49 |
Test Parameter
CAOMIUM
SILVER
ICP/GFAA METALS DIGESTION
DeL Rep. DiL
Resutt Untts Umtt Umtt Factor Method
194 ug/g 1.3 6.4 10 SW-846,6010
19600 ug/g IA 9.6 10 SW-846,6010
1 SW-846,3050
Analyst Test Date
KWB 12/18/9710:56
KWB 12/18/9710:56
LVD 12/10/97 00K)0
I Sample ID: M-636-11-97-05 Lab ID: Ll 283-16 Collect Date: 11/10/97 09:51
Test Parameter
CADMIUM
SILVER
ICP/GFAA METALS DIGESTION
Det Rep. DIL
Resutt Untts UnA Limtt Factor Method
48 ug/g .1 M 1 SW446,6010
5350 ug/g 2 -J 1 SW-846,6010
1 SW-446,3050
Analyst Test Date
KWB 12/17/9713:45
KWB 12/17/9713:45
LVD 12/10/97 00:00
I Sample ID; M.636-11-974)6 Ub ID: L1283-17 Collect Date: 11/10/97 09.53
Testparainetw
CADMIUM
SILVER
ICP/GFAA METALSOIGESTION
ResHlt
103
24900
Untts
ug/g
ug/g
Det Rep. DIL
Limtt Limtt Factor Method
13 62 10 SW-846,6010
1.9 9.4 10 SW-846,6010
1 SW-846,3050
Analyst Test Date
KWB 12/17/9713:48
KWB 12/17/9713:48
LVD 12/10/97 00^)0
[SamplelD: M-636-11-97-07 Lab ID: Ll 283-18 Collect Date: 11/10/97 09:56
Test Parameter
CADMIUM
SILVER
ICP/GFAA METALSDIGESnON
Bssijlt Untts
ug/g
ug/g
Det Rep. OIL
Umtt Umlt Factor
11
1050
.1
2 S
Method
SW-846,6010
SW-846,6010
SW-846.3050
Analyst Test Date
KWB 12/17/9713:51
KWB 12/17/9713:51
LVD 12/10/9700:00
[SamplelD: M-636-11-97-08 Lab ID: L1283-19 Collect Date: 11/10/97 09:58
Test Parameter
CADMIUM
SILVER
ICP/GFAA METALS DIGESTION
Det Rep. DO.
Resutt Untts Limtt UnJt Factor Method
42
3500
ug/g
ug/g
.1
2
M
s
1
1
1
SW446.6010
SW-846.6010
SW-846.3050
Analvs^ Test Date
KWB 12/17/9713:54
KWB 12/17/9713:54
LVD 12/10^7 00:00
SamplelD: l\4-636-11-97-09 LablD:L1283-20 Collect Date: 11/10/9710:00
Test Parameter
CADMIUM
SILVER
ICP/GFAA METALS DIGESHON
DeL Rep. DU.
Resutt Untts Limtt Umtt Factor Method
499
16400
ug/g
ug/g 1.4
47
7
10
10
1
SW-846,6010
SW-846,6010
SW-846,3050
Analyst Test Date
KWB 12/17/9713:57
KWB 12/17/9713:57
LVD 12/10fl7 00:00
Page 5 of 7
1 Sample ID: M-636-11-97-10
Test Parameter
CAOMIUM
SILVER
ICP/GFAA METALS DIGESTION
1 Sample ID: M436-11-97-11
Test Pflfaineta
CADMIUM
SILVER
ICP/GFAA METALSOIGESTION
1 Sample ID: M-636-11-97-12
Test Parameter
CADMIUM
SILVER
ICP/GFAA METALS DIGESTION
PesHlt
.4
278
Resutt
3.4
2780
Resutt
22
1480
II
I
Untt*
ug/g
ug/g
if
f
Ub ID: L1283-21
Det Rep. DH.
Limtt Limtt Factor
.1 S 1
.1 .7 1
1
UblO:L1283-22
DeL Rep. DU.
Limtt Umtt Factor
.1 S 1
2 A 1
1
UblD: Ll283-23
D«L Rep. DiL
Limtt Limtt Factor
.1 .6 1
2 a 1
1
Collect Date: 11/10/9710:02 i
Method AnalYft Te«tPati»
SW-846,6010 KWB 12/17/9714^)0
SW-846,6010 KWB 12/17/9714:00
SW-846,3050 LVD 12/10/97 OOM
Collect Date: 11/10/8710:03 |
Method Analyst Test Date
SW-846,6010 KWB 12/17/9714OT
SW-846.6010 KWB 12/17/97 14:03
SW-846.3050 LVD 12/10/9700:00
Collect Date: 11/10/9710.05 |
Method Analvst Test Date
SW-846.6010 KWB 12/17/9714:06
SW-846.6010 KWB 12/17/9714:06
SW-846,3050 LVD 12/10*7 00:00
Page Bof 7
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected but was
below the detection limit.
B Gas Chromatography and Mass Spectral Data Flag. This flag is used when an analyte is found in
the blank as well as the sample
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This flag is used
either when estimating a concentration for tentatively identified compounds or when the data
indicated the presence of a compound that meets the identification criteria but the result is less than
the specified reporting limit (e.g. 3 J with a reporting limit of 10)
Det. Limit Method Detection Limtt (approximately three times the signal noise level)
Rep. Limit Reporting Limit is nonmally the value of the lowest standard run vinth the analysis. The value
is approximately 5 to 10 times the Method Detection Limit
Dil. Factor Dilution Factor - The prepared sample was diluted by this factor because the sample was
too concentrated or due to other interferences in the sample matrix. Any dilution factor
causes an appropriate increase in the method detection limit and reporting limit
Page 7of7