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HomeMy WebLinkAboutDSHW-1998-002071 - 0901a0688013bbd9# # PROPUI3iON GROUP W#^tfftJtfVft# P.O. BOX 707 BRIGHAM CITY, UT 84302-0707 AEROSPACE & INDUSTRIAI TECHNOLOGIES 801-863-3511 SEFQ I m^ 31 August 1998 "'-^ °^ ^--nent. Q.,,, 8740-FY98T-098 Dennis R. Downs, Executive Secretary Utah Solid and Hazardous Waste Control Board 288 North 1460 West PO Box 144880 Salt Lake City, Utah 84114-4880 Dear Mr. Downs: ATTENTION: Jeff Vandel SUBJECT: Semi-Annual RFI Progress Report As required by Section VII.H of Thiokol Corporation's Post Closure Permit, the following semi-annual RFI progress report Is submitted for your review. The reporting period covered by this report is 1 March 1998 -1 September 1998. Included is notification of three newly identified SWMUs and corresponding investigation plans, along with a progress summary for Thiokol's Corrective Action Management Unit. Ifyou have any questions in this matter, please contact me at (435) 863-5928, or Frank Walker at (435) 863-5390. Sincerely, J. D. Thompson, Director Environmental, Fire, Medical and Security JDT/afw c: Don Ostler, Director, Division of Water Quality RECEIVED SEP 0 1 1PP8 '?''^'sion Of Solid & Hazardous Waste TfflOKOL CORPORATION ''''"'^''^^^'"^"'°^^"^'^°""'«"fal Quality SEMI-ANNUAL RFI PROGRESS REPORT 1 March 1998-1 September 1998 SEMI-ANNUAL RFI PROGRESS REPORT 1 SEPTEMBER 1997 -1 MARCH 1998 1. Description and estimation of the percentage of the RCRA Facility Investigation completed. To date, soils at the following SWMUs have been sampled: M-19A Photographic Processing Discharge, SWMU 553; E-517-W Surface Discharge, SWMU 282; M-576-N Surface Discharge, SWMU 271; M-514 Surface Discharge, SWMU 618; S-501 Surface Discharge, SWMU 266; M-640 Surface Discharge, SWMU 381; M-641 Surface Discharge, SWMU 264; M-585-N Surface Discharge, SWMU 273; M-606 Surface Discharge, SWMU 527; M-628 Surface Discharge, SWMU 528; M-593 Surface Discharge, SWMU 274; M-636-SW Surface Discharge, SWMU 367; M-570 Surface Discharge, SWMU 285; M-197 Surface Discharge, SWMU 483; M-197-BP Surface Discharge, SWMU 360; M-702 Surface Discharge, SWMU 620; A-9 Surface Discharge, SWMU 267; A-2 Surface Discharge, SWMU 560; M-66 Surface Discharge, SWMU 432; M-72 Surface Discharge, SWMU 263; M-67 Surface Discharge, SWMUs 261 and 433; M-14N and M-14S Surface Discharges, SWMUs 257 and 270; M-53-BP Surface Discharge, SWMU 260; M-53-E Surface Discharge, SWMU 259; M-33-B and M-33-C Surface Discharges, SWMUs 258 and 413; M-39 Surface Discharge, SWMU 425; Combined Surface Discharge for M-8, M-9, M-10, M'52, and M-179-N, SWMUs 268, 611, 269, 409, 472, and 255; M-57 Surface Discharge, SWMU 615; M-55-W Surface Discharge, SWMU 621; M-9 Strand Burner Exhaust Discharge, SWMU 652; M-40 Surface Discharge, SWMU 642; M-205 Surface Discharge, SWMU 286; T-21-D Surface Discharge, SWMU 559; T-6-A Surface Discharge, SWMU 287; Old Drum Storage Area East of M-203, SWMU 203; M-l 14 Surface Discharge, SWMU 426; M-227 Hydrofluoiric Acid Treatment Unit, SWMU 192; M-9-NE Surface Discharge, SWMU 651; M-186 Industrial Waste Landflll, SWMU 212; M-136 Old Waste Oil Disposal Pit, SWMU 208; M-187 Old Drum Storage Area, SWMU 551; T-l Photographic Processing Drainfield, SWMU 648; A-2 Photographic Processing Drainfield, SWMU 191; I-IO-NE Subsurface Discharge, SWMU 645; I-IO-SE Subsurface Discharge, SWMU 436; I-l O-S Subsurface Discharge, SWMU 234; T-l 11 Subsurface Discharge, SWMU 355; T-24A Surface Discharge, SWMU 401; M-2 Laundry Drainfield C, SWMU 627; M-19A Drywell, SWMU 444; M-39 Subsurface Discharge, SWMU 425; T-51A Surface Discharge, SWMU 402; M-2 Laundry Drainfield B, SWMU 626; M-19A Strand Bumer Exhaust Discharge, SWMU 650; M-585 Strand Bumer Exhaust Discharge, SWMU 649; Historic Buming Ground NE of M-243, SWMU 202; M-2 Laundry Dramfield A, SWMU 465; Old Burning Grounds at M-136, SWMU 243; M-193-S Septic Drainfield, SWMU 638; M-193-N Septic Drainfield, SWMU 632; M-191 Septic Drainfield, SWMU 631; M-338 Subsurface Discharge, SWMU 608; Domestic Wastewater Drainfields A, B and C, SWMU 625; M-348 Subsurface Discharge, SWMU 395; M-72 Septic Drainfield, SWMU 630; M-71 Septic Drainfield, SWMU 646; M-19A Septic Drainfield, SWMU 628; Removed Sump at M-622, SWMU 316; M-l 17 Subsurface Discharge, SWMU 254; T-14A Subsurface Discharge, SWMU 493; T-3 Subsurface Discharge, SWMU 446; M-53-MH Subsurface Discharge, SWMU 228; Old Buming Ground West of M-174, SWMU 195; Old Burning Ground East of M-303, SWMU 233; I-IO Septic Drainfield, SWMU 664; M-15A Septic Drainfield, SWMU 663; M-15A Drywell, SWMU 662; M-137A Removed Waste Oil Storage Tank, SWMU 616; M-53-BP Removed Drywell and Surface Discharge, SWMU 616; T-35 Beryllium Test Area, SWMU 201; T-35 Beryllium Waste Disposal Area, SWMU 200; M-40 Magnesiuih Grinding Area, SWMU 655; T-53A Subsurface Building Discharge, SWMU 353; T-015A Subsurface Building Discharge, SWMU 397; T-053 Sump, SWMU 497; 1-5 Septic Drainfield, SWMU 667; M-85 Deactivated Sump, SWMU 139; M-83 Removed Sump, SWMU 457; E-502 Removed Sump, SWMU 177; M-34 Old Perchloric Acid Sump, SWMU 196, 236; M-126 Removed North Sump, SWMU 162; and M-126 Removed Middle Sump, SWMU 163 M-212 Removed North Sump, SWMU 149; M-212 Removed South Sump, SWMU 150; M-227 Hydrofluoric Acid Treatment Unit, SWMU 192; M-345 Old North Drainage Ditch Ponds, SWMU's 320, 321, 322; E-534 Historical Sanitary Sewage Sludge Pond, SWMU 658; M-225 Old Open Buming Sites, SWMU 19; M-14 um tast ^ump, ^WMU 114,^ ^^ n<d' ^D'4 '^^ M-16 Old Sump Location, SWMU 115;»^ ' ^ ^ ^' '^ M-23 Old Sump Location, SWMU 118;*^ M-42 Emergency Containment Sump, SWMU 121; M-57 Spill Containment Sump, SWMU 124;*^ I-IO SE Drywell, SWMU 436K I-IO NE Drywell, SWMU 645,*/ . M-87 Emergency Containment Sump, SWMU 165; M-157 Old Sump Location, SWMU 311,^ North Drainage Ditch, SWMU 230|^ M-58 Drywell; and M-56 Drywell, SWMU 666.*-^ At the time of this report, Thiokol has a contractor on site providing sampling support for investigation activities for several SWMU sites for the RCRA Facility Investigation. In addition, closure activities at the M-225 Burning Ground are nearing completion, and remediation of the SWMUs covered under Thiokol's CAMU designation is progressing. A brief description of these activities follows. Closure of Old Open Buming Sites at M-225 Closure activity is continuing for several of the old open burning trays at the M-225 Burning Ground (SWMU No. 19). Closure is following the approved closure procedures found in Closure Plan for Old Open Burning Sites at the M-225 OB/OD Facility. The sampling phase of the closure is complete, and a risk assessment has been prepared for the residual contamination above background levels. The closure report and risk assessment will be submitted in the very near future. Thiokol's Corrective Action Management Unit Additional contaminated soil has been excavated from the photographic waste discharge sites at M-39, M-19A and M-636. This action was taken after verification samples revealed constituents above the action levels specified in the CAMU plan. All contaminated soil excavated from the photographic sites has been transported to Thiokol's CAMU site at M-571 where they are undergoing treatment to remove any hazardous characteristic. At the time of this report only the site at M-19A had not been remediated to the corrective action levels of the plan. However, laboratory results of verification samples taken following the most recent excavation are not yet available. Thiokol has recently received an unsolicited proposal from a mining company in westem Utah expressing an interest in the contaminated soils from the photographic sites. The mine would reclaim the precious metals from the soil in a batch cyanide leaching plant. This option is contingent upon Thiokol being successful in rendering the soils nonhazardous so they can be managed as solid waste. A copy of the mining company's proposal for the soils is included for the Division's review and consideration. Summaries of all findings; Any available raw analytical data from all sampling activities during the reporting period as well as data from the previous reporting period which was not available at the time of reporting is included. 3. Summaries of all changes made in the RCRA Facility Investigation during the reporting period. Thiokol has identified three new solid waste management units to be included in the Facility Investigation. A brief description of the unit's follows and an investigation workplan are included. SWMU No.: 669 Two historical "drying ponds" west of building M-13 received overflow wastewater from the process sump at the north west end of the building. The overflow traveled via a concrete ditch to the ponds where the water percolated and evaporated. Building M- 13 has been used as a grinding facility for ammonium perchlorate since its construction in the early 60's. The ponds were removed many years ago but a portion of the concrete trench is still visible. Other than the trench, no other visible physical evidence oftheir location remains at the site. SWMU No.: 670 Building M-16 also had two historical "drying ponds" believed to be similar in constmction and function to those at Building M-13. Operations at M-16 include several processes in the manufacturing of tactical motors. Again, these ponds were removed many years ago with no remaining visible evidence of their location. SWMU No.: 671 This unit is a drywell located east of building M-58. The building is currently used only for storage of propellant materials and equipment, but has historically been used as a propellant development oven. This drywell will be added to the investigation workplan for other dry wells submitted previously, and the sampling strategy outlined in that plan will be followed during assessment and sampling. Investigation workplans for these newly identified SWMUs is included with this report. 4. Summaries of all contact with representatives of the local community, public interest groups or State Gk)vernment during the reporting period; Correspondence regarding RFI activities has been limited to the Division of Solid and Hazardous Waste and the Division of Water Quality. 5. Summaries of all problems or potential problems encountered during the reporting period. There were no significant problems encountered during the reporting period. 6. Actions being taken to rectify problems; Thiokol continues to review all available information and pursue all avenues to resolve any uncertainty associated with the solid waste management units. 7. Changes in personnel during the reporting period. The existing environmental staff will continue to conduct the sampling when possible. Interstate Drilling of Midvale, Utah, is providing the equipment and operators to assist Thiokol personnel in collecting environmental samples. 8. Projected work for the next reporting period. Efforts for the next reporting period will focus on investigating additional solid waste management units, completing and submitting the closure plan for the M-225 Burning Area, completion of remediation of the sites in the CAMU, and report preparation for these projects. 9. Copies of daily reports, inspection reports, laboratory and monitoring data. Available analytical data from all sampling activities and any data from the previous reporting period, which was not available at the time of reporting, is included. M-13 Drying Ponds Investigation Plan SWMU No. 669 Thiokol Corporation RFI Work Plans, Vol. 4 21 February 1997 1.0 SAMPLING OBJECTIVE Samples collected at this site during Phase I of the RFI will be analyzed for verification ofthe presence ofhazardous waste or hazardous waste constituents indicating a release from the SWMU. 2.0 SITE LOCATION The building and the corresponding solid waste management unit to be sampled under this plan is as follows: M-13 IrSWMpN®;?!-*::! 669 Samples will be taken from the area of the historical drying ponds. No visable physical evidence remains to indicate the location of the ponds. Building personnel and facility maps will be utilized to approximate the location. See Drawing MP-D-22/1. 3.0 BACKGROUND INFORMATION This unit consisted of two historical "drying ponds" west of building M-13 that received overflow wastewater from the process sump at the north west end of the building. The overflow traveled via a concrete ditch to the ponds where the water percolated and evaporated. Building M-13 has been used as a grinding facility for ammonium perchlorate since its constmction in the early 60's. The ponds were removed many years ago and there is no visible physical evidence of their location. 4.0 SAMPLING RATIONALE The constituents of concem for this site are metals, volatile organics, and explosives. Phase I sampling will focus oh verification ofthese constituents in the soil. 5.0 SAMPLING STRATEGY The location of the two "drying ponds" has been graded and revegetated making it necessary to approximate the location by referring to facility drawings, aerial photographs and interviews with building personnel. • Thiokol Corporation RFI Work Plans, Vol. 4 21 February 1997 The site of each pond will be divided into 5' x 5' grids. The intersection of the grids will be numbered and sample locations chosen using a random number generator or table. The actual sampling grids will be chosen the day of the sampling. Two grids from each pond will be chosen and samples taken from 2, 5 and ten foot depths. Duplicate and QA/QC samples will be collected at the frequency shown in the following chart. SAMPLE TYPE PROPOSED FREQUENCY Duplicate 5% or 1 per site, which ever is greater Rinse Field Blanks 5% or 1 per site, which ever is greater Spikes 1% of the total RFI samples 6.0 BACKGROUND Background samples have been collected in areas known or believed to be free of contamination within the Manufacmring and Administration Area for use in comparing concentrations. These background samples were collected at corresponding depths to obtain samples in similar strata to those taken in the areas of concern. Extensive soil sampling of the Thiokol facility has established a data base for naturally occurring inorganic constituents. This data base consists of background samples used in the closure of various RCRA facilities at Thiokol. The analytical results of the background samples taken during Phase I sampling will be added to this data base to provide site specific data. Analytical data obtained from investigation activities at this site will be compared to this data base for determination of contamination above background levels. 7.0 SAMPLING EQUIPMENT 1. New split-spoon sampler 2. Field book 3. Certified clean sample bottles 4. Distilled water 5. Tape measure 6. Alconox soap wash 7. Tap water 8. Steam cleaner or wash buckets Thiokol Corporation RFI Work Plans, Vol. 4 21 February 1997 9. Cleaning bmsh 10. Rubber gloves 11. Lab labels and seals 12. Cooler and ice 13. Stainless steel spawla 14. Shovel 15. Steam cleaned auger rig and tooling 8.0 SAMPLING TECHNIQUE NOTE: For personal safety and to prevent cross contamination, use new mbber gloves at each sample point when handling samples and sampling equipment. 1. Using a cleaned split-spoon and auger rig, retrieve a continuous soil sample down to the prescribed depth. Samples will be collected at 2, 5 and 10 foot depths and placed into sample bottles. This will be accomplished as follows: A) Carefully split open spoon B) Measure core to find the required sample depths C) Using cleaned stainless steel spatula, remove a portion of soil at the required depth to fill the sample bottle(s). D) Seal sample bottle lid with seal, note sample location and depth on sample bottle label, and place in cooler containing ice. E) Note soil lithology in log book F) Scrape the remaining soil out of spoon and leave in same area as sample point. 2. After sample has been taken at the depths noted above, decontaminate the split spoon, spatula, and any associated equipment as follows. A) Steam clean with Alconox soap or scmb with bmsh in wash basin or bucket containing Alconox soap and water. B) Rinse with tap water (Do not reuse tap water) C) Give final rinse with deionized water Thiokol Corporation RFI Work Plans, Vol. 4 21 February 1997 NOTE: Containerize all wash and rinse water for hazardous waste analysis to determine proper disposition. The samples will be identified as follows with the depth noted after each assigned sample number: • The sample taken from site #1 at the 5 foot level would be labeled as SWMU669, #1@5'. 9.0 SAMPLE DOCUMENTATION The following information must be recorded in the Field Book: Date and time of sampling Sampler's name and signature Location of samples including depth Type, number, sample number, and seals used on sample bottles Weather Texture and color of samples Any other pertinent information 10.0 ANALYTICAL PARAMETERS The soil samples will be analyzed by a State certified lab for the following constiments: BUILDING M-13 SWMUNO: 669 PARAM h'/l'ERS Metals (Panel) Volatile Organics HMX, RDX, Perchlorate, NG, Nitrate, Chloride SW-846 METHODS (UNLESS OTHERWISE INDICATED) 6010 8260 HPLC Thiokol Corporation RFI Work Plans, Vol. 4 21 February 1997 11.0 SAMPLE ACCOUNTABILITY AND CUSTODY Follow procedures specified in the Waste Analysis Plan, Appendix 02.D of Thiokol Corporation Hazardous Waste Permit Application, November 1991. These procedures are also contained in the Data Collection Quality Assurance Plan in Volume Two of the RFI Work plans. Requirements for sample custody and custody seals are discussed in these documents. » Thiokol Corporation RFI Work Plans, Vol. 4 21 February 1997 PLOT PLAN 10 40 ^SSm fCALC IM FECT m.> M ] KfTtC « 1 1 i •1 ,^r.-- ^.-.-:jlpi'"'^ EQUIPMENT , muHAnc tno LH/M •MOU CMt REFERENCE DRAWINGS rAOina eo'ii AKMTICIWM IIH-4-1 TN.U »• a • irl-i Tnlw I-t »ll...| TM«i; »•« LEGEND »-*Am VUVtl _T-..Mt HVMANTI —•—M|Ufl«ll UNU —•—IIIAM LMI —M-OMO. ntuM CHEMICAL CORPORATION WUATCH OIVrtlON M-16 Drying Ponds Investigation Plan I SWMU No. 670 f ~\ iii;i^:,„.jiii£iiA^'^a^.' .««iif-':'-*. Thiokol Corporation RFI Work Plans, Vol. 4 21 February 1997 1.0 SAMPLING OBJECTFVE Samples collected at this site during Phase I of the RFI will be analyzed for verification of the presence of hazardous waste or hazardous waste constituents indicating a release from the SWMU. 2.0 SITE LOCATION The building and the corresponding solid waste management unit to be sampled under this plan is as follows: •\|BUIM)n<G% M-16 670 Samples will be taken from the area of the historical drying ponds. No visible physical evidence remains to indicate the location of the ponds. Building personnel and facility maps will be utilized to approximate the location. See Drawing MP-D-26/1. x 3.0 BACKGROUND INFORMATION This unit consisted of two historical "drying ponds" west of building M-16 that received overflow wastewater from the process sump at the north west end of the building. The overflow traveled via a concrete ditch to the ponds where the water percolated and evaporated. Building M-16 has been used for several processes in the manufacmring of tactical motors since its constmction in the early 60's. The ponds were removed many years ago and there is no visible physical evidence of their location. 4.0 SAMPLING RATIONALE The constituents of concern for this site are metals, volatile organics, and explosives. Phase I sampling will focus on verification of these constiments in the soil. • 5.0 SAMPLING STRATEGY The location ofthe two "drying ponds" has been graded and revegetated making it necessary to approximate the location by referring to facility drawings, aerial Thiokol Corporation RFI Work Plans, Vol. 4 21 February 1997 photographs and interviews with building personnel. The site of each pond will be divided into 5' x 5' grids. The intersection of the grids will be numbered and sample locations chosen using a random number generator or table. The actual sampling grid will be chosen the day of the sampling. Two grids from each pond will be chosen and samples taken from 2, 5 and ten foot depths. Duplicate and QA/QC samples will be collected at the frequency shown in the following chart. SAMPLE TYPE PROPOSED FREOUENCY Duplicate 5% or 1 per site, which ever is greater Rinse Field Blanks 5% or 1 per site, which ever is greater Spikes 1 % of the total RFI samples 6.0 BACKGROUND Background samples have been collected in areas known or believed to be free of contamination within the Manufacmring and Administration Area for use in comparing concentrations. These background samples were collected at corresponding depths to obtain samples in similar strata to those taken in the areas of concern. Extensive soil sampling of the Thiokol facility has established a data base for namrally occurring inorganic constituents. This data base consists of background samples used in the closure of various RCRA facilities at Thiokol. The analytical results of the background samples taken during Phase I sampling will be added to this data base to provide site specific data. Analytical data obtained from investigation activities at this site will be compared to this data base for determination of contamination above background levels. 7.0 SAMPLING EQUIPMENT 1. 2. 3. 4. 5. 6. 7. New split-spoon sampler Field book Certified clean sample bottles Distilled water Tape measure Alconox soap wash Tap water Thiokol Corporation RFI Work Plans, Vol. 4 21 February 1997 8. Steam cleaner or wash buckets 9. Cleaning bmsh 10. Rubber gloves 11. Lab labels and seals 12. Cooler and ice 13. Stainless steel spamla 14. Shovel 15. Steam cleaned auger rig and tooling 8.0 SAMPLING TECHNIQUE NOTE: For personal safety and to prevent cross contamination, use new mbber gloves at each sample point when handling samples and sampling equipment. 1. Using a cleaned split-spoon and auger rig, retrieve a continuous soil sample down to the prescribed depth. Samples will be collected at 2, 5 and 10 foot depths and placed into sample bottles. This will be accomplished as follows: A) Carefiilly split open spoon B) Measure core to find the required sample depths C) Using cleaned stainless steel spatula, remove a portion of soil at the required depth to fill the sample bottle(s). D) Seal sample bottle lid with seal, note sample location and depth on sample bottle label, and place in cooler containing ice. E) Note soil lithology in log book F) Scrape the remaining soil out of spoon and leave in same area as sample point. 2. After sample has been taken at the depths noted above, decontaminate the split spoon, spatula, and any associated equipment as follows. A) Steam clean with Alconox soap or scmb with bmsh in wash basin or bucket containing Alconox soap and water. B) Rinse with tap water (Do not reuse tap water) C) Give final rinse with deionized water Thiokol Corporation Rn Work Plans, Vol. 4 21 February 1997 NOTE: Containerize all wash and rinse water for hazardous waste analysis td determine proper disposition. The samples will be identified as follows with the depth noted after each assigned sample number: • The sample taken from site #1 at the 5 foot level would be labeled as SWMU670, #1@5'. 9.0 SAMPLE DOCUMENTATION The following information must be recorded in the Field Book: Date and time of sampling Sampler's name and signamre Location of samples including depth Type, number, sample number, and seals used on sample bottles Weather Texmre and color of samples Any other pertinent information 10.0 ANALYTICAL PARAMETERS The soil samples will be analyzed by a State certified lab for the following constiments: BUILDING M-16 SWMUNO: 670 PARAMETERS Metals (Panel) Volatile Organics HMX, RDX, Perchlorate, NG, Nitrate, Chloride SW-846 METHODS (UNLESS OTHERWISE INDICATED) 6010 8260 HPLC Thiokol Corporation RFI Work Plans, Vol. 4 21 February 1997 11.0 SAMPLE ACCOUNTABILITY AND CUSTODY Follow procedures specified in the Waste Analysis Plan, Appendix 02.D of Thiokol Corporation Hazardous Waste Peimit Application. November 1991. These procedures are also contained in the Data Collection Quality Assurance Plan in Volume Two of the RFI Work plans. Requirements for sample custody and custody seals are discussed in these documents. Thiokol Corporation RFI Work Plans, Vol. 4 21 February 1997 M-W uAmncrumm •UILDINO PLOT PLAM Hug IE 98 04:3Ba Clifton Mining 801-7SG-5454 p-1 To: Bill Moellef Clifton Miring ^B From. Bob Holladay 787-2883 ^P 08/11/98 16:22.00 Page lof 2 Sent by ttie Award Winning Cheyenne BitWre Oifton Mining Company 70 W Canyon Crest Suite D Aipind, Utah 84004 (801) 756-1414 Fax <801) 756-5454 11 August 1998 Thiokol Corporation Attn: Frank WaJker By Fax: 43.S-863'403? Dear Frank: I( has comt to our attention tbat Thiokol has a quantity of silver contaminatBd soil dial has been gathered and stabilized widi hiiit; and i:> ready to be landlllled We would like to propose what may b$ an envjronmentaity preferable alternative. Clifton Mining has recenUy c.oinpleted and placed in operation a small batch cyanide leaching plant (hat we believe would be »utiiblt: for removing die silver from this soil. A brief description of the plant is appended We would propose screening the material at its present location to remove the relxtivef>' uncontaminated rocks larger than 3/8", hauling the fine portion in our trucks to the plant at Cold Hill, Utah, and processing it. Tbe fine din, with silver removed, could then be disposed of with our other tailings, or retumed to 'Ihiokol for disposal. We would need Thiokol to furnish a piece of equipment wirh operator to load the maienal onto tite screen and/or trucks as needed Thiokol would also need to dispose of the rocks left behind and pay any costs associated with returning the fine material to Thiokol, should that be desired. Clil^on Mining would retain (he contained silver as payment. We would expect that Thiokol representatives would visit the Clifton plant to evaluate its suitability, and that Clifton representatives would visit the Thiokol site to xaice samples for analysis before any agreement is finalized. If you have any queshons or need further clarification, contact tne at (435) 753-115? or (801) 376'48?7 or Bill Moeiler or Keith Moeller at the numbers on the letterhead Thanks. Sincerely, '--^^ '/ ••'• ••/' Robert J. Holladay, Vice Presid$«fi (Operations) xuaiici L^ii ' a. Sent by the Award Winning Cheyenne Bitware Clifton Mining Company Gold Hill Leach Plant Clifton Mining Co. has constructed a small plant at its Cactus Mill Site near Gold Hill, Utah. It 18 a batch leach plant capable of processing about five to fifteen tons per day using sodium cyanide or one of several altemate lixiviants to eMract gold and silver from ores m concemrates The plant occupies about 1800 .'iquare feet of a currently unused 5000 square foot building. The equipment area is surrounded by a concrete relaining wail to provide secondary containment of all hqutds u&ed. The plant consists of two leach vessels, one 2400 gallons, thc other 3600 gallons, a slurry pump, thickener, aad 4' x 9' honzontai belt filter. Soluhon from fte filter goes to a 6000 gallon prvg tank, through a Merrill-Crowe unil with a 3' x 3' plate & frame filter to a 5000 gallon barren tank. Power is supplied by either of two diesel powered generators installed for other plants on site Dry ground ore or concentrate is introduced to the leach vessels by front end loader. Hie leached ore is double rinsed with clean water, treated with c.alaum hypochlorite to destroy ony rooidual oyonido, ond vritr th« plant nrad nr filtar mlrii Tum furnii^«s tn •triilahl/' rin site for melting of dore. Process walei is recycled. Sak build up is dealt with by bleeding off small amounts of barren solution as needed for evaporation and solids disposal Cheiriicals used are sodium hydroxide, sodium cyanide, powdered zinc and small amounts of a filter aid. 2'<^ ^TSI'S-SS^-TOB 3UIUIW UO^IJTXD P9E:t'0 8B 2T Sny ENVIRONMENTAL LAB WORK REQUEST iHW ™= THIOKOL ENVraONMENTAL LABORATORY LWR No. E11614 Login No. FROM: ^ik^K l/l//kj:ejz. EXTENSION s^fcp COST CENTER WORK ORDER /gi4c? I r/z^/9^ ORGANIZATION SNUirzo/i}/lJMJrj9C^ MAILSTOP 3o( REPORT RESULTS TO: HELEN WARD, MS 301 SAMPLE INFORMATION SAMPLE 'M-i^3i^-^ 'M-Oi(.-tV 3. 4. 5. 6. L • W 9. 10. ^. 12. DATE f/^'/ff Wiy I'" TYPE G - ly ^ C LOCATION A/^SC^ ^riJH M-^^C ^r.r/4pfc TIME Ofoc^ '^/r TEST REMARKS Cc/, /^^ ^ mr c^s^ //ci^ 9 CHAIN OF CUSTODY RELINQUISHED BY DATE TIME RECEIVED BY DATE TIME 7WU(/(^ ''^-^9' f<?:£>< mc^ 7-Zp-'f9 /<7:^< C FOR LABORATORY USE ONLY COMPLETED DATE REPORTED SIGNATimE CERI'IFICATE OF ANALYSIS Listing of sample information and Testing Requested Wednesday, August 19,1998 TESTED FOR Thiokol: DLV Environmental Monitoring M/S 301 Thiokol Corp, UT 84322 Franl( Wailcer Project: Solid Waste Mgmt Invest Login Number L1734 ANALY2LED BY Thiokol Environmental Laboratorv Thiokol Corporation P.O. Box 707 M/S 245 Brigham City, UT 84302-0707 801-863-3732 800-863-8080 l^bNo Client Number Test Requested ILI 734-1 M^3ft4.GRID#4 SWr846,6010 SW-846, 6010 SW:846,3050 1 Ll 734-2 M-636-28. GRID #28 Description .Ag ICR'Metals Analysis (RCRA) ' Cd^rCP Metals Analysis (RCRA) I.CP/GFAA Metals Digestton • ' *-v Received CollectDate/Time Matrix 07/20/98 07/20/98 09:00 1 Soil Soil Soil 07/20/98 07/20/98 09:15 1 SW-846,6010 SW-846, 6010 SW-846, 3050 Ag ICP Metals Analysis (RCRA) Cd ICP Metals Analysis (RCRA) ICP/GFAA Metals Digestion Certified By Soil Soil Soil Dfate JaiT^s M. Anderson, QC Officer This certifies that tlie following samples were analyzed using good laboratory practices to show the following results: ,.V..'^ *' .- l??i V T- .^w ^..•f .' 'r^ .f .••• ,;-s^,- Ljfcj"«fedt;./a,-HidK' mi^ .:uM.:ii^%-D^no -1 rtf O Listmg of Results by Sample I Sample ID; M-63fr4, GRID #4 l-ab ID: Ll 734-1 Collect Date: 07/20/9809:00 Test Parameter CADMIUM SILVER ICP/GFAA METALS DIGESTION [ Result 3.3 105 Units ug/g Det Umit .09 .1 Rep. Oil. Utnit Factor Method SW-846. 6010 SW.646,6010 SW-846,3050 Analyst Test Date KWB 08/14^811^2 KWB 08/14/9811:02 KWB 08/11/9800:00 Sample ID: M-636-28, GRID i»28 l^b ID: Ll 734-2 Coliect Date: 07/20/98 09:15 Test Parameter CADMIUM SILVER ICP/GFAA METALS DIGESTION Result Units 37 ug/g 10 ug/g Det Limit .1 2 Rep. Dil. Umit Factor Method SW-846,6010 SW-846,6010 SW-846,3050 Analyst Test Date KWB 08/14/9811:05 KWB 08/14/9811:05 KWB 08/11/98 00:00 • Data Reporting Qualifiers U Indicates compound was analyzed for and was not detected, or the compound was detected but was below the detection limit. B Gas Chromatography and Mass Spectral Data Flag. This flag is used whien an analyte is found in the blank as well as the sample J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This flag is used either when estimating a concentration for tentatively identified compounds or when the data indicated the presence of a compound that meets the identification criteria but the result is less than the specified reporting limit (e.g. 3 J with a reporting limit of 10) Det. Limit Method Detection Limit (approximately three times the signal noise level) Rep. Limit Reporting Limit is normally the value of the lowest standard run with the analysis. The value is approximately 5 to 10 times the Method Detection Limit Dil. Factor Dilution Factor - The prepared sample was diluted by this factor because the sample was too concentrated or due to other interferences in the sample matrix. Any dilution factor causes an appropriate increase in the method detection limit and reporting limit