DSHW-1997-002921 - 0901a06880158473

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AU6 2 9 1997
TfflOKOL CORPORATION ,,,Jl::^,:,^,„,,,
Utah Department of Environmental Quality
SEMI-ANNUAL RFI PROGRESS REPORT
I March 1997 - 1 September 1997
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SEMI-ANNUAL RFI PROGRESS RIi:PORT
1 SEPTEMBER 1996 -1 MARCH 1997
1. Description and estimation of the percentage of the RCl^ Facility Investigation
completed;
To date, soils at the following SWMUs have been sampled:
M-19A Photographic Processing Discharge, SWMU 553;
E-517-W Surface Discharge, SWMU 282;
M-576-N Surface Discharge, SWMU 271;
M-514 Surface Discharge, SWMU 618;
S-501 Surface Discharge, SWMU 266;
M-640 Surface Discharge, SWMU 381;
M-641 Surface Discharge, SWMU 264;
M-585-N Surface Discharge, SWMU 273;
M-606 Surface Discharge, SWMU 527;
M-628 Surface Discharge, SWMU 528;
M-593 Surface Discharge, SWMU 274;
M-636-SW Surface Discharge, SWMU 367;
M-570 Surface Discharge, SWMU 285;
M-197 Surface Discharge, SWMU 483;
M-197-BP Surface Discharge, SWMU 360;
M-702 Surface Discharge, SWMU 620;
A-9 Surface Discharge, SWMU 267;
A-2 Surface Discharge, SWMU 560;
M-66 Surface Discharge, SWMU 432;
M-72 Surface Discharge, SWMU 263;
M-67 Surface Discharge, SWMUs 261 and 433;
M-14N and M-14S Surface Discharges, SWMUs 257 and 270;
M-53-BP Surface Discharge, SWMU 260;
M-53-E Surface Discharge, SWMU 259;
M-33-B and M-33-C Surface Discharges, SWMUs 258 and 413;
M-39 Surface Discharge, SWMU 425;
Combined Surface Discharge for M-8, M-9, M-10, M-52, and M-179-N,
SWMUs 268, 611, 269, 409, 472, and 255;
M-57 Surface Discharge, SWMU 615;
M-55-W Surface Discharge, SWMU 621;
M-9 Strand Burner Exhaust Discharge, SWMU 652;
M-40 Surface Discharge, SWMU 642;
M-205 Surface Discharge, SWMU 286;
T-21-D Surface Discharge, SWMU 559;
T-6-A Surface Discharge, SWMU 287;
Old Dmm Storage Area East of M-203, SWMU 203;
M-114 Surface Discharge, SWMU 426;
M-227 Hydrofluoric Acid Treatment Unit, SWMU 192;
M-9-NE Surface Discharge, SWMU 651;
M-186 Industrial Waste Landfill, SWMU 212;
M-136 Old Waste Oil Disposal Pit, SWMU 208;
M-187 Old Drum Storage Area, SWMU 551;
T-l Photographic Processing Drainfield, SWMU 648;
A-2 Photographic Processing Drainfield, SWMU 191;
I-IO-NE Subsurface Discharge, SWMU 645;
I-IO-SE Subsurface Discharge, SWMU 436;
I-IO-S Subsurface Discharge, SWMU 234;
T-l 11 Subsurface Discharge, SWMU 355;
T-24A Surface Discharge, SWMU 401;
M-2 Laundry Drainfield C, SWMU 627;
M-19A Dry well, SWMU 444;
M-39 Subsurface Discharge, SWMU 425;
T-51A Surface Discharge, SWMU 402;
M-2 Laundry Drainfield B, SWMU 626;
M-19A Strand Burner Exhaust Discharge, SWMU 650;
M-585 Strand Burner Exhaust Discharge, SWMU 649;
Historic Burning Ground NE of M-243, SWMU 202;
M-2 Laundry Drainfield A, SWMU 465;
Old Burning Grounds at M-136, SWMU 243;
M-193-S Septic Drainfield, SWMU 638;
M-193-N Septic Drainfield, SWMU 632;
M-191 Septic Drainfield, SWMU 631;
M-338 Subsurface Discharge, SWMU 608;
Domestic Wastewater Drainfields A, B and C, SWMU 625;
M-348 Subsurface Discharge, SWMU 395;
M-72 Septic Drainfield, SWMU 630;
M-71 Sepdc Drainfield, SWMU 646;
M-19A Septic Drainfield, SWMU 628;
Removed Sump at M-622, SWMU 316;
M-117 Subsurface Discharge, SWMU 254;
T-14A Subsurface Discharge, SWMU 493;
T-3 Subsurface Discharge, SWMU 446;
M-53-MH Subsurface Discharge, SWMU 228;
Old Burning Ground West of M-174, SWMU 195;
Old Burning Ground East of M-303, SWMU 233;
I-IO Septic Drainfield, SWMU 664;
M-15 A Septic Drainfield, SWMU 663;
M-15A Dry well, SWMU 662;
M-137A Removed Waste Oil Storage Tank, SWMU 616;
M-53-BP Removed Dry well and Surface Discharge, SWMU 616;
T-35 Beryllium Test Area, SWMU 201;
T-35 Beryllium Waste Disposal Area, SWMU 200;
M-40 Magnesium Grinding Area, SWMU-655;w^ . . I ^^^ ^ ,i iq.y
T-53A Subsurface Building Discharge, SWMU 3531\^ /l/li^-/<A 1 / ^ ^ij? t. 7 /
T-015A Subsurface Building Discharge, SWMU 397,^
T-053 Sump, SWMU 497;*^
1-5 Septic Drainfield, SWMU 667^^ ,
M-85 Deactivated Sump, SWMU 139!^
M-83 Removed Sump, SWMU 457*^.
E-502 Removed Sump, SWMU 177!^ y ^^
M-34 Old Perchloric Acid Sump, SWMU 196, 23%;
M-126 Removed North Sump, SWMU 162; and
M-126 Removed Middle Sump, SWMU 16^^
These sites represent approximately 98 percent of the SWMUs in Phase I of the RFI.
At the time of this report, Thiokol has a contractor on site providing support to the
investigafion ofthe following sites.
DESCRIPTION
SUBSURFACE BUILDING DISCHARGE
ABANDONED DRYWELL (POSSIBLY REMOVED)
BUILDING DISCHARGE
SOUTH WEST ABANDONED DRYWELL
SOUTH EAST ABANDONED DRYWELL
During the reporting period, Thiokol has initiated closure or interim measures at
several SWMU sites. A brief discussion of actions taken to date at these sites follows.
Closure activity has begun at the M-225 Buming Ground, SWMU 19, to investigate
several of the old burning sites at the facility. The investigative phase of the closure
will be followed by cleanup measures as necessary. Closure of these sites is following
the approved closure procedures found in Closure Plan for Old Open Burning Sites at
the M-225 OB/OD Facility. Analytical results from the sampling phase of closure was
not available at the time of this report. This data will be included in the report
summarizing the results ofthe investigafive phase.
Interim measures are being taken at two SWMU sites, SWMUs 665 and 234. As
outlined in the previous semi-annual report, interim measures were required at these
sites to accommodate modifications to the buildings.
On 12 June 1997, the drywell and adjacent soils at SWMU 234 were excavated to a
depth of seven feet. All contaminated soil and waste residues removed from the site
were staged on plastic sheeting near the point of excavation.
SWMU
354
609
622
640
643
BUILDING
T-097A
M-009NE
M-364
M-009SW
M-009SE
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Two verification soil samples were collected following the initial excavation and
analyzed for RCRA metals and volatile organics. One sample (L1024-1) was collected
from the location of the center of the drywell at a depth of 7 - 7.5 feet. The sample was
light brown to tan colored soil consisting of very dense silt and clay. It was noted that
when the excavator encountered this layer it was difficult to penetrate and was initially
thought to be a concrete slab. The second sample (L1024-3) was collected
approximately four feet west of the first and at the same depth. The sample was in
coarser and darker soils.
The analytical results of verification samples did not indicate the presence of any
volatile organics and the inorganic results were compared with soil background levels.
Concentrations of metals were found to be above background levels necessitating
further excavation. On 15 July 1997, additional soil was removed from the site and a
verification sample collected. Laboratory results indicate that all parameters are now at
or below respective background levels.
A composite sample of excavated soil staged at the site was collected and sent for
TCLP analysis to determine proper disposal options.
At the time of preparation of this report, Thiokol is reviewing disposal options for the
soil excavated at the site. Thiokol will review the results ofthe analytical data and
dispose of the soil properly. Final disposition of the material will be reported in a Final
Interim Measures Report.
Interim measures at SWMU 665 are nearing completion. The concrete pad which will
cap the low concentration of residual contamination at SM^MU 665 is approximately
90% constmcted. These interim measures will continue to follow the approved plan
Proposal For SWMU #665 at Building M-53. Thiokol will notify the Division upon
completion of the concrete pad as requested in the approval letter.
Thiokol has begun preliminary preparations for corrective action for two additional
SWMUs, SWMU 367 and 425, which will involve the remediation of contaminated
soils from these sites in a Corrective Action Management Unit.
2. Summaries of all findings;
The available raw analytical data from all sampling activities during the reporting
period and any data from the previous reporting period which was not available at the
time of reporting is included.
3. Summaries of all changes made in the RCRA Facility Investigation during the
reporting period;
Thiokol initiated interim measures for SWMUs #665 and 234 during the reporting
period. Approval to institute interim measures was received from the Division of Solid
•
and Hazardous Waste on 30 April 1997, and the post-closure permit has been modified
to allow for the incorporation of voluntary cleanup actions, or interim measures into the
permit.
Thiokol received approval for designation of a Corrective Action Management Unit for
the remediation of soils at Solid Waste Management Units 367 and 425 from the
Division of Solid and Hazardous Waste on July 11, 1997. Module VII of the Post-
Closure Permit has been modified to add a new condition to allow for the incorporation
of voluntary cleanup actions, or interim measures. Corrective action at these sites will
be conducted in accordance with the terms and conditions of the permit modification.
4. Summaries of all contact with representatives of the local community, public
interest groups or State Government during the reporting period;
Correspondence regarding RFI activities has been limited to the Division of Solid and
Hazardous Waste and the Division of Water Quality.
5. Summaries of all problems or potential problems encountered during the reporting
period;
There were no significant problems encountered during the reporting period. As
discussed in previous reports, nearly all the remaining sites have some level of
uncertainty associated with them in terms of exact location, site accessibility, or safety
concems. Considerable effort has been made during the reporting period to resolve this
uncertainty.
6. Actions being taken to rectify problems;
Thiokol is reviewing all available information and interviewing personnel in a effort to
resolve the uncertainty associated whh the remaining sites.
7. Changes in personnel during the reporting period;
The existing enviromnental staffwill continue to conduct the sampling when possible.
Contractors will be used when specialized equipment is required.
8. Projected work for the next reporting period;
Efforts for the next reporting period will focus on completing the investigation for the
remaining sites, completing closure for the M-225 Burning Area, completion of
interim measures at SWMUs 665 and 234, and report preparation for these projects.
9. Copies of daily reports, inspection reports, laboratory and monitoring data.
The raw analytical data from all sampling activities during the reporting period and any
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data from the previous reporting period which was not available at the time of reporting
is included.
I 125
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WO#:1B940 LWR#: £rOff
SITE: T-53A Drywell _
DESCRIPTION: SWMU 353; Depth ^ ^1-
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PARAMETERS
RCRA Metals
plus Sb, Sulfate and pH
DATE:
METHOD
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Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR#: £il7Sj-
SITE: T-53A Drywell ,^
DESCRIPTION: SWMU 353; Depth 5 l-h
PARAMETERS METHOD
Volatile Organics 8260
DATE: ^/^TTIME: I^ ^^ SAMPLER: '^^'-
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WO#:1B940 LWR #: S/fjS'f
SITE: T-53A Drywell ' 6 fr
DESCRIPTION: SWMU 353; 6fi4^^
PARAMETERS
RCRA Metals
plus Sb, Sulfate and pH
METHOD
60 KD
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Thiokol Corporation RCRA Facility Investigation
WO#:1B940 L\NR#: e//JC4
SITE: T-53A Drywell ' Sf/-~
DESCRIPTION: SWMU 353; Go4^>^— , !Crrr~
PARAMETERS
Volatile Organics
METHOD
8260
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Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR#: ^//J5~S
SITE: Magnesium Grinding Area
DESCRIPTION: SWMU 655; Site #1 Surface
PARAMETERS METHOD
As, Ba, Cd, Cr, Pb, Hg, Se, Ag, Mg
DATE: ^^/fJME: /f70 SAMPLER: /ffvj
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #: ^// J SB
SITE: Magnesium Grinding Area
DESCRIPTION: SWMU 655; Site #2, Surface
PARAMETERS METHOD
As, Ba, Cd, Cr, Pb, Hg, Se, Ag, Mg
DATE:^/f 7TIME: /'^^-T'SAMPLER A ^"^
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WO#:1B940 LWR #: <^//J srB
SITE: Magnesium Grinding Area
DESCRIPTION: SWMU 655; Site #1, 2 ft
PARAMETERS METHOD
As, Ba, Cd, Cr, Pb, Hg, Se, Ag, Mg
DATE: ^^/f 7TIME: /f J^ SAMPLER: Af^^^
7/7/o/(o/Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: tT^lZnl
SITE: Magnesium Grinding Area
DESCRIPTION: SWMU 655;.Site #2, 2 ft
PARAMETERS METHOD
As, Ba, Cd, Cr, Pb, Hg, Se, Ag, Mg
DATE: %/,irmE: WTIAMPLER: ^ F"^
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WO#:1B940 LWR#:
SITE: 1-5 Septic System
DESCRIPTION: SWMU 667; Grid # / : 5 ft
PARAMETER.^
Volatile Organics
METHOD
8260
DATE: ^//^ TIME: f/^ SAMPLER: AFU^
Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR#:
SITE: 1-5 Septic System .
DESCRIPTION: SWMU 667; Grid # / : 5 ft
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PARAMETERS
RCRA Metals
METHOD
6010, 7470/7471
DATE: 57^7 TIME: ^^ SAMPLER: /^FUJ
Mm. Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR#:
SITE: 1-5 Septic System /
DESCRIPTION: SWMU 667; Grid #. .; 10 ft
PARAMETERS
Volatile Organics
METHOD
8260
DATE: S/^^TIME: ^/gSAMPLER: /^fiiAJ
Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR#:
SITE: 1-5 Septic System
DESCRIPTION: SWMU 667; Grid # [_, 10 ft
PARAMETERS
RCRA Metals
METHOD
6010, 7470/7471
DATE: S^^ TIME: J^ SAMPLER . f
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WO#:1B940 LWR#:
SITE: 1-5 Septic System ^
DESCRIPTION: SWMU 667; Grid # ^^5 ft
PARAMETERS
Volatile Organics
METHOD
8260
DATE:^/^ TIME: ^SlTsAMPLER: A^^
Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR#:
SITE: 1-5 Septic System
DESCRIPTION: SWMU 667; Grid # _2--r5 ft
PARAMETERS
RCRA Metals
METHOD
6010, 7470/7471
DATE:^/.-TIME: ^^'SAMPLER: A^^
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W0#: 1B940 LWR#:
SITE: 1-5 Septic System
DESCRIPTION: SWMU 667; Grid # "Z-HO ft
METHOD PARAMETERS
Volatile Organics
DATE: ^f TIME: ^^^AMPLER: A ^
8260
Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR#:
SITE: 1-5 Septic System
DESCRIPTION: SWMU 667; Grid # ^<TD ft
PARAMETERS
RCRA Metals
METHOD
6010, 7470/7471
DATE: t/.^ TIME: /^2..SAMPLER /^ fW
2Z^ 2^
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Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR#:
SITE: 1-5 Septic System
DESCRIPTION: SWMU 667; Grid # 3 ; 5 ft
PARAMETERS
Volatile Organics
METHOD
8260
DATE:^f TIME: /6td SAMPLER: A^^
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Thiokol Corporation RCFLA Facility Investigation
WO#:1B940 LWR#:
SITE: 1-5 Septic System
DESCRIPTION: SWMU 667; Grid # >A ; 5 ft
PARAMETERS
RCRA Metals
METHOD
6010, 7470/7471
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W0#: 1B940 LWR#:
DATE: 5^ TIME: /St^ SAMPLER: fi^fU
SITE: 1-5 Septic System
DESCRIPTION: SWMU 667; Grid # J> ; 10 ft
PARAMETERS
Volatile Organics
METHOD
8260
DATE: y/f TIME: /03^kUPLER: AP^
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W0#: 1B940 LWR#:
SITE: 1-5 Septic System
DESCRIPTION: SWMU 667; Grid # 3 ; 10 ft
PARAMETERS
RCRA Metals
METHOD
6010, 7470/7471
DATE:^f a TIME: /^J 2.§AMPLER /^P%J
M^
r/7/o/co/Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:
SITE: 1-5 Septic System .
DESCRIPTION: SWMU 667; Grid # ^ ; 5 ft
PARAMETERS
Volatile Organics
METHOD
8260
DATE: ^It^ TIME: /anr^AMPLER: 'j^'^^
r/7/o/co/Corporation RCRA Facility Invejstigation
WO#:1B940 LWR #:
SITE: 1-5 Septic System M
DESCRIPTION: SWMU 667; Grid # ^ ; 5 ft
PARAMETERS
RCRA Metals
•METHOD
6010, 7470/7471
DATE : 5|^^ TIME: /^y^AMPLER: ^^
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Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR#:
SITE: 1-5 Septic System
DESCRIPTION: SWMU 667; Grid # 4- : 10 ft
•PARAMETERS METHOD
Volatile Organics 8260.
DATE: Jf^TME: f//fl^SAMPLER: A^^^
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Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR #:
SITE: 1-5 Septic System
DESCRIPTION: SWMU 667; Grid # "C ; 10 ft
PARAMETERS METHOD
RCRA Metals 6010, 7470/7471
DATE:?j;- TIME: //iO ^SAMPLER /{fpuj
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Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR#:
SITE: M-85 Deactivated Sump
DESCRIPTION: SWMU 139; Grid # f ; 5 ft
lt-^
PARAMETERS
Volatile Organics
METHOD Z/!'/ 1
8260
DATE:Sy/y TIME: //"f^ifeAMPLER: AFJU
I '
Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR #: a ^n
SITE: M-85 Deactivated Sump
DESCRIPTION: SWMU 139; Grid #_/; 5 ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Be 6010
Mercury 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
DATE: ^ TIME:/^ SAMPLER: A^FuJ
T-i
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r/i/o/co/Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:
SITE: M-85 Deactivated Sump
DESCRIPTION: SWMU 139; Grid # / : 10 ft
PARAMETERS
Volatile Organics
METHOD
8260
DATE:^7^TIME: /^^O SAMPLER: >^fFO
SITE: M-85 Deactivated Sump
DESCRIPTION: SWMU 139; Grid # / ; io ft
^^^^fl^ MEIHOD
Cd, Cr, Ag, Pb, Be goTo
•^^'^^^ 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
DATE: ¥/r TIME: /2:^0 SAMPLER AfHj
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JJA}^ T/i/o/co/Corporation RCRA Facility Investigation
WO#:1B940 LWR #:
SITE: M-85 Deactivated Sump
DESCRIPTION: SWMU 139; Grid # '^-T-6 ft
PARAMETERS
Volatile Organics
METHOD
8260
DATE: ^9 TIME: /^/i SAMF>LER: ^ftAJ
r/i/o/co/Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:
SITE: M-85 Deactivated Sump
DESCRIPTION: SWMU 139; Grid # __?ri-5 ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Be 6010
Mercury 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
DATE:§^/f TIME: /Z//TAMPLER: A^^
ENVIRONMENTAL LAB woRii REQUEST
139
r/7/o/co/Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:
12>^ SITE: M-85 Deactivated Sump
DESCRIPTION: SWMU 139; Grid # 2-HO ft
d /^O
PARAMETERS
Volatile Organics
METHOD
8260
Aied/HH^ ho 'P'-^
•^
DATE: J/f TIME: /ZJO SAMPLER: AP^
//f- ^/jd S^ £.=&.
rdc^ v
-<i-
X^^^rsSo^""^"," """^ ^^°''*y investigation
SITE: M-85 Deactivated Sump
DESCRIPTION: SWMU 139; Grid #_^^o ft
Mercury 7A-7nr,
HMX, RDX. Perchlorates, NG, Nitrate
DATE: YjfTmE: /^^Q SAMPLER: J^f'^
l'i€~0 ft A/I-^S fp S&n^p/c . ri^/pinudd ^i</K.fi
Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR#:
SITE: M-83 Removed Sump
DESCRIPTION: SWMU 457; Grid #_/ ; 5 ft
j^
Sl
M-e'^
«^
3o' 'ns*
1 r^
PARAMETERS
Volatile Organics
METHOD 2/5 i_
8260
DATE: ^i^TIME: 1^0 SAMPLER: Af^^
• f
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:
SITE: M-83 Removed Sump
DESCRIPTION: SWMU 457; Grid # _] ; 5 ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Be 6010
Mercury 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
DATE:f/f^ TIME: I400 SAMPLER: A^%*J
^^ /£!_
A(C dl ua\ a rg j.'e [S.
U *<^<^ <:7(^fxv( •f^
i"
' ' ^^1
i' ^H
•" ^^M
• ^^1
irj" ^^M
pH
&V^^I i ^M
'ii-m fel
'J .f-.
»••• ---"
v^.r' •• K
-••. T'-
_ ..••.•
..-
.^ .-•.""
1 rJ-
:i-
/4I^
/f^&
SITE: M-83 Removed Sump
DESCRIPTION: SWMU 457; Grid #__[_; 10 ft
^^^SAMIIESS METHOD
Volatile Organics 8260
DATE:?//tTIME: /^(f/^SAMPLER: M'^
Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR#:
SITE: M-83 Removed Sump ,
DESCRIPTION: SWMU 457; Grid #_\ ; 10 ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Be 6010
Mercury 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
DATE: ^9 TIME: /^4g^-6AMPLER AFv^
Th/o/co/Corporation RCRA Facility Investigation
WO#:1B940 LWR#: ^
SITE: M-83 Removed Sump ^
DESCRIPTION: SWMU 457; Grid # ^-r^ft
PARAMETERS
Volatile Organics
METHOD
82.60
DATE:^<?'TIME: /^gg^SAMPLER: /'^'W
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:
SITE: M-83 Removed Sump
DESCRIPTION: SWMU 457; Grid # ^-r5 ft;
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Be 6010
Mercury 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
DATE: ^7f TIME: /fZ&SAMPLER: Af^*^
£i ^rou'}/^ V^
d ^miie-U C/rd ^
W^7^ Jntv-f^
•Sx^A^f
&//^y-2 ^
Aild/gyn ^/7nci
red ii\.
ENVIRONMENTAL LAB WOIRK REQUEST
.///
141
rj?/o/f6/Corporation RCRA Facility Investigation
WO#:1B940 LWR#:
SITE: M-83 Removed Sump
DESCRIPTION: SWMU 457; Grid # 2<1Q ft
PARAMETFPS
Volatile Organics
-J9M.
METHOD ^/^Jph IO<.h fl^^^
8260 "^/i^ ~ ^(X^-t^
DATE:^//f TIME: ^J^ SAMPLER: /(fyd
r/7/o/fo/Corporation RCRA Facility Investigation
WO#:1B940 LWR #:
SITE: M-83 Removed Sump ,_
DESCRIPTION: SWMU 457; Grid# ^"-rTO ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Be 6010
Mercury 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
)rociC <3/\.d ^and
f- •' --••"
fc-;
A^^•l/ 7'^'o'fo/Corporation RCRA Facili^y Investigation
-^^ WO#:1B940 LWR#;
SITE: E-502 Removed Sump
DESCRIPTION: SWMU 177; Grid # ^; 5 ft
PARAMETERS METHOD
8260 Volatile Organics
DATE:^2*TIME: i"Z"UAMPLER: AP
Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR#:
SITE: E-502 Removed Sump .
DESCRIPTION: SWMU 177; Grid # . \ .J 5 ft
PARAMETERS METHO.Q
Cd, Cr, Ag, Pb, Be 6010
Mercury 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
DATE: S^/z«riME: <^^^SAMPLER: Af«^
1^
;!!+ uj\n'<^
JAAA tu il'^ ^ya-^^
^V.VCikinfc^t |UC^K<^Tit^«
4*
WW
'#
&
iHi^
r/7/o/co/ Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:
SITE: E-502 Removed Sump
DESCRIPTION: SWMU 177; Grid # L_; 10 ft
PARAMETER5y
Volatile Organics
METHOD
8260
DATE:y/toTIME: 9?c) SAMPLER: >^f:^
T/j/o/co/Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:
SITE: E-502 Removed Sump
DESCRIPTION: SWMU 177; Grid # {_; 10 ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Be 6010
Mercury 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
DATE: Sjf-XO TIME: *??» SAMPLER y^piO
M^d:^
TceX Q>Yn o^) -
wmsmm mm
ENVIRONMENTAL LAB WORK REQUEST
• Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR#:
SITE: E-502 Removed Sump ^
DESCRIPTION: SWMU 177; Grid# ^.yfl
PARAMETERS
Volatile Organics
METHOD
8260
Thiokol Corporation RCRA Facility Investigation
— • W0#: 1B940 LWR#:
SITE: E-502 Removed Sump ^
DESCRIPTION: SWMU 177; Grid # ^^T5 ft
DATE: ^-^ TIME: 9^ SAMPLER: A^
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Be 6010
Mercury 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
DATE: ^«>riME: ^SISsAMPLER: /^^tjd
143
w^
hrdUJ/^//(^d ''SJ//
-^ms o-f OKfdallr^. \
^dn^ ^/
^
:i ^
Thiokol Corporation RCRA Facility Investigat
W0#; 1B940 LWR#:
. SITE: E-502 Removed Sump
DESCRIPTION: SWMU 177; Grid #
PARAMETERS
Volatile Organics 8260
ion
;.i0ft
MglHQD
DATE: ifuXmE: /Q 0 7sAMPLER: ^^p^
Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR #:
SITE: E-502 Removed Sump
DESCRIPTION: SWMU 177; Grid #_JZ-i-10 ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Be 6010
Mercury 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
DATE: yZJ^lME: /(^ *J SAMPLER A^ u->
^A/6
Mediiuu kr/^un^
^dt-
dec f^- fi-S4 ^ 3ait\ft<^ ^fd ^^roh/cyii Ar,d'S^^^u) a'^^d% ;^
(V • ...-,
<*".--.
r .--
If' ,.--•"
'3 -•'••••'"'
%-r.
i
r/j/o/co/Corporation RCRA Facility Investigation
W0#; 1B940 LWR#:
SITE: M-34 Old Perchloric Acid Sump /
DESCRIPTION: SWMU 196, 236; Grid # / ; 5 fl;
PARAMETERS
Volatile Organics
METHOD
8260
DATE: f/^oTIME: ///> SAMPLER: /^l*->
\
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:
SITE: M-34 Old Perchloric Acid Sump
DESCRIPTION: SWMU 196, 236; Grid; l# / ;5ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Be 6010
Mercury 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
DATE.9/t^ TIME: ///ST^SAMPLER: AF^
^( ' 189^
/<-3f Stu«»u#/9(.
^io/f7 mr
DA
m^
ENVIRONMENTAL LAB WORK REQUEST
Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR#:
SITE: M-34 Old Perchloric Acid Sump /
DESCRIPTION: SWMU 196, 236; Grid #__/_; 10 ft
PARAMETERS
Volatile Organics
METHOD
8260
DATE: ^jf^lME: ''-''^^ SAMPLER: AF*^
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:
SITE: M-34 Old Perchloric Acid Sump /
DESCRIPTION: SWMU 196, 236; Grid # [_, 10 ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Be 6010
Mercury 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
DATE: f/tOTIME: //^^ SAMPLER Jip^ut^J
/U|-3f 5WMU^/9h
4iPw
145
f\^ll?^l?<'
Iiokf-
l-f- Si/H
frCjrYt^yed n^cK^
af QppraK fC^.
~~M^.
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:
SITE: M-34 Old Perchloric Acid Sump ^
DESCRIPTION: SWMU 196, 236; Grid # _^_, 5 ft
4I4J4
PARAMETERS
Volatile Organics
METHOD
"^{[r iy\ii> '^\vec.^2.
8260
K DATE:S^cyriME: //^S SAMPLER: fif^
it\c! Qit£ A vVgL<
5c^^vd
1
146
SITE: M-34 Old Perchloric Acid Sump
DESCRIPTION: SWMU 196, 236; Grid# 2.--5 ft
EA^JMEIgBS sflETHOD
Cd, Cr, Ag, Pb, Be eoTo
UM^'^r^v 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
DATE:^COTIME: //^/IAMPLER: >4<=UJ
/•/ • .
'Sf: ZO Ar-iO
..'•••
:.'^-'.
•r.
..•«f
U
.•iV
T/7/oto/ Corporation RCRA Facility Investigation
WO#:1B940 LWR#:
SITE: M-34 Old Perchloric Acid Sump
DESCRIPTION: SWMU 196, 236; Grid #_±=r-10 ft
PARAMETERS
Volatile Organics
lUIETHOD
8260
DATE: ^0 TIME: /A^3r^AMPLER: M^^^
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:
SITE: M-34 Old Perchloric Acid Sump
DESCRIPTION: SWMU 196, 236; Grid # ^-JI.O ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Be 6010
Mercury 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
DATE: ^fech-IME: //rr-gAMPLER: Afi^
7/e//?
147
?^
S^fzo /rrc^ Af^^
/32s^ ^1- fA'/?(.. 7d_ Co/fc^i- Sa,t--^ja/cs tQoriA ff'j^nucd
A^rtix <^ncJ ^^iJdlc Sim^f^
lll^
Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR#:
SITE: M-126 North Removed Sump ,
DESCRIPTION: SWMU 162; Grid # / ; 5 ft
PARAMETERS
Volatile Organics
METHOD
8260
L DATE:^^* TIME: /? JC»SAMPLER: -f^lhj^
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:
SITE: M-126 North Removed Sump
DESCRIPTION: SWMU 162; Grid # I : 5 ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Be 6010
Mercury lAir^HAl^
HMX, RDX, Perchlorates, NG, Nitrate
DATE
'^4va
^< TIME: iZlt^ AMPLER: >^FuJ)
Wof °B9^4"'° w!^." ^^^ '^^'"^y '"-^^'9-^-
SITE: M-126 North Removed Sump
DESCRIPTION: SWMU 162; Grid# / ; io ft
- PARAMETERS
Volatile Organics
METHOD
8260
DATE: ^JxA TIME: /i«^AMPLER: ^^P^
i/d/^o
A'lAI'S-h Med/.rr,-. <:ryi^
-^^f-4 rm/^ I
10 n 71
L
^^
'' I
r,.-.'-
^ •K
4
148
Jim.
SITE: M-126 North Removed Sump .
DESCRIPTION: SWMU 162; Grid #__/__; io ft
EAMBEB5 METHOD
Cd, Cr, Ag, Pb, Be 6010
Mercury 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
DATE: )/zoTIME: /^l^ SAMPLER Af^
M'f^C^ Hoffk (Um&id'>(t»^
Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR #:
SITE: M-126 North Removed Sump —
DESCRIPTION: SWMU 162; Grid #_^rr5 ft
PARAMETERS
Volatile Organics
METHOD
8260
DATE :^^d TIME: /^SAMPLER: A4^
Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR#:
SITE: M-126 North Removed Sump
DESCRIPTION: SWMU 162; Grid#. ^-•5 ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Be 6010
Mercury 7470/'7471
HMX. RDX, Perchlorates, NG, Nitrate
DATE:^2*>TmE:/4^^ SAMPLER: A^^
^yW>
sand /?/i^ Sa^w.
sd/f-
149
^
Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR#:
SITE: M-126 North Removed Sump ^
DESCRIPTION: SWMU 162; Grid # _^; 10 ft
PARAMETERS METHOD
Volatile Organics 8260
DATE: S^ TIME: /^/^ SAMPLER: A=HJ
Ai€d/n,u '^rat^ /
^dHy M /^ ^Md
-^a/tci
T/7/o/co/Corporation RCRA Facility Investigation
WO#:1B940 LWR #:
SITE: M-126 North Removed Sump
DESCRIPTION: SWMU 162; Grid # _2=H 0 ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Be 6010
Mercury 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
DATE:^igK>TIME:/^(^ SAMPLER: AF^
Id^ca/rj^f ff.fcr apprcx.ifn.dh I^^ahcy) ^d ferncucd ifez
-4-K7
Pall AA-I7.L M
T),rK
i/Lin Thiokol Corporation RCRA Facility Investigation
WO#: 1B940 LWR#:
SITE: M-126 Middle Removed Sump
DESCRIPTION: SWMU 163; Grid # / ; 5 ft
l^/lz/l
PARAMETERS
Volatile Organics
METHOD ALfdi[//H^ - h 2^
8260 6'rni.'^f /v/^o^J
%~
r/7/o/co/Corporation RCRA Facility Investigation
WO#:1B940 LWR#:
SITE: M-126 Middle Removed Sump
DESCRIPTION: SWMU 163; Grid# / ; 5 ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Be 6010
Mercury 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
DATE: ^^TIME: /4?0 SAMPLER: Ap^
mef ppm*
.'^
''• ' -•,
150
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:
SITE: M-126 Middle Removed Sump -
DESCRIPTION: SWMU 163; Grid # (_, 10 ft ^/^h/^
PARAMETERS
Volatile Organics
METHOD dUjcL 'mm
8260 (OIHX ^dlr^A/td'^ 14 A/J ^
DATE: R5«?TIME: ]44^ SAMPLER: Ap^
7/7/o/co/Corporation RCRA Facility Investigation
WO#: 1B940 LWR#:
SITE: M-126 Middle Removed Sump
DESCRIPTION: SWMU 163; Grid # (_, 10 ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Be 6010
Mercury 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
DATE: JSZPTIME: /j)S0 SAMPLER A^F^O
j^ '
^i^:^
.'••
•
X-1
-(-.
^d
•^
V:'
.^r-
'i'K
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:
SITE: M-126 Middle Removed Sump
DESCRIPTION: SWMU 163; Grid#__^fift
Mil J^[\'^'^
PARAMETERS
Volatile Organics
METHOD 7:^/i ^ /17/?<^f Mh
8260
DATE:^ifeTIME: /4-^ SAMPLER: ^fhij
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #:
SITE: M-126 Middle Removed Sump -
DESCRIPTION: SWMU 163; Grid #__^5 ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Be 6010
Mercury 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
izZ/ye
A Aid J a. IV. f'
/}mui4 IA}IH\.
^rcd hue^ /md
DATE •^ZPlME: /^CT^ SAMPLER: A^^
•«. .^ ._^
/<c^ Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR #:
SITE: M-126 Middle Removed Sump ^
DESCRIPTION: SWMU 163; Grid# ^^10 ft
151
/^//d// 2^
PARAMETERS METHOD
_ Volatile Organics 8260
DATE: ^O TIME: /fZDd SAMPLER: Arf"^
Thiokol Corporation RCRA Facility Investigation
WO#:1B940 LWR #:
SITE: M-126 Middle Removed Sump ^
DESCRIPTION: SWMU 163; Grid# ^>HOft
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Be 6010
Mercury 7470/7471
HMX, RDX, Perchlorates, NG, Nitrate
DATE:^dTIME: /S2)6sAMPLER: AF^
^Ar ^k) J
^1
I^P
P4 hv Ifl / <)o'"^—\Hj-
n. ^ TV. J
•^ ^\ •' . . J ^
^ff^ ^
Msd^
y/zo J Tti
Thi'!: li Hu 'tlOSf-
T^FI
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../^
• "I I 'n''
./^
152
<?f/ '^^"^
5UU/«U (bl. <^^^ ^^^
1/6A
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5ujiuo iteZ. c;4*^5 lo^^- 6i«(? -
r/lo fT3i^ AfvJ
•^i n/m
<)
Sclrk.f(c' "St^cu •cc/ ^ ^-57f^^' y^ Q^Z^*-fV
^
SfiRPWB^H SPigWlIiWfPJffllWW
153
ZT/ih-^ftik /if f)an[ aroufids -7W<f/7fa '^^f
/Ml
-•-
Tluokol Corporation RCRA Facility Investieation
W0#: 1B940 LWR#:
STTE: T-53 Subsurface Discharge,
DESCRnmON: SWMU #497i&w/pepth iT^
PARAMETFW.S
Volatile Organics
METHOD
82^0
_DATE: tf'Ll TIME: /^S-IAMPLER: >I^MW
TKokol Corporation RCRA Facility Investigation
W0#: 1B940 LWIW:
STTE: T-53 Subsurface Discharm
DESCRIPTION: SWTVIU #497;5P*/Depth :r.A-
PARAMETERS
Cadmium
Copper
Lead
pH
METHOD
<^V%;M3.,^« 6010
iOlO
6010
9045
DATE: tyz/ TIME: /^5-% SAMPLER:
7W<»*o/ Corporation RCRA Facility InvestigaUon
W0#: 1B940 LWR*:
SITE: T-53 Subsurface Discharge ^ •_
DESCRIPTION: SWMU #497;S(«^Depth /O r
PARAMETERS
Volatile Organics
METHOD
DATE: y/Z//f7 TIME: /fl S ^AMPLER: /^^C^^
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR*:
SITE: T-53 Subsurface Discharg^,^, . ^m^
(\S<ia.i\c^ -H^
xO.*'' ^ €,v^
ilh^nJ pii{\iOiy<.
r^cK.
'^vtiujik-^ CdiUckd adp./c.tf
/&/zc/ Zn.
^ m L'^l rd>cyc '^%.,i
^rsn<i? /IrcJna^fl'^d
Cc/^r/^ f "T^
DESCRIPTION: SWMU #497
PARAMETERS
Cadmium
Copper
Lead
pH
^dlTjAjjW^,^.
Depth
METHOD
. 6010
6010
6010
9045
DATE: 9/tf /^ TIME: /^52^SAMPLER: ^pO —
154
r'
i' .^
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LVVTW:
SITE: T-S3 Subsurface Discbare
DESCRIPTION: SWMU #497; (uA ^ Depth ;Wi2.l 5""ff-
PARAMETERS
Volatile Organics
METHOD
DATC: ^^/'/<?7 TIME: /^^^ SAMPLER: Af^
-DOJMvi -f*J7 <S4-«^Z <rf/
J(^//9//^
Sllf- IjJtHx ILL.
izi Icui f-^
RF^
Su)AA.v> 497 <3ii-*t2- |6fr-
VO/V
W^ffr? /(of AO
TUokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:
SITE: T-53 Subsurface Discharge
DESCRIPTION: SWMU #497;^rfTfl)epth I&fepth IO I
PARAMETERS METHOD
Cadmium idri A-S, M« i*^,^^
Copper ' ' J C «>
Lead
pH
DATE:
10
6010
6010
9045
%//<? TIME: m SAMPLER: Af^
iiln/2<
"ddu. f SiJ
fidi!cdu.rtci roci-^
•••••••li
/.?K
155
ftt T-/^/^ f^ Son^ pIfL drH drm^.',d ^ic/uL' 597
'..^^J I ^1 ^ ^^. „i. ( i Nl o:, f _
^
LMTHTIOVT? XOCX\ ^ f^
i3i^ U^A ^..^f^ CoWeA^^
Vtiokol Corporation RCRA Facility Investigation
W0#: IB940 LWR#:
STTE: T-15A Subsurface Discharge /
DESCRIPTION: SWMU #397; 5" Depth
fz/^^
Ccc^v-s<=- ^kStVci
PARAMETERS
Antimony CA ) ^^ t ^% ^ *"
Arsenic
Chromium
Lead
Sulfate
pH
METHOD
6010
6010
6010
6010
300
9045
aH<^ (gvgyc QrdLv.<
r<-^ Colcnu 4-CibStl'OGcl 11^
{}.n^t,v \-e\ic\
DATE T/t,ll?7 TIME: /5/^^ SAMPUEB: ^^
tV2K,v^l •€,
^
J33Q Pnl{fr.ini\ "Sg.vp/^A (^ /O^cJeP-^.. "Sft^ \ ^ro CU r/i^>y c[
-^ I oV/Clugie '•Svlfs r^,vA CU'v^^, ^-?-^ ^
IJOK ^a>o.(>l'^ CQlUri^d
Thiokol Corporation RCRA Facility Investigation
WO#: 1B940 LWR#:
SrTE: T-15A Subsurface Discharge #
DESCRIPTION: SWMU #397; //> Depth
lllUJlT
^^
I
4
PARAMETERS
Antimony
Arsenic
Chromium
Lead
Sulfate
pH
DATE:
METHOD
cAi^.A^jg^S
6010
6010
300
9045
cA CO fcr /^jOtiX
^2//f7 •xrm.-.jSSO SAMPLER: /iFvJ^
Ob<^r^cii (n ^tupi,
ENVIRONMENTAL LAB WORKREQi^EST w^
#
£^ THIOKOL ENVIRONMENTAL LABORATORY LWR No. El 1354
Login No.
/If LLhUdi
EXTENSION COSTCE^fTEI^
UJ3iC'
WOKK ORDER
5'/Ua^ f 7
ORGANIZATION
fn\^ Scic
REPORT RESULTS TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
1 1
SAMPLE
5;v
/(
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5.
6.
7
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10.
11.
12.
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c
LOCATION
T-5ZA
/'
ll
d
TIME
IDlo
/OZO
fOH)
to^o
TEST REMARKS
^CZA Mjkk. f :Sl,,Sa(/^,pd-
VPA - "B-Lbb
S^r ^/'
S^^f ^Z^
•
CHAIN OF CUSTODY
FOR LABORATORY USE ONLY 0^ IA"E COMPLETED DATE REPORTED SIGNATURE
CERTIFICATE OF ANA^LYSIS
Listing of sample Infonnation amd Testing Requested
#
Monday, April 7,1997
TESTED FOR Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp, UT 84322
Franlt Walker
Project: Solid Waste Mgint Invest
Login Number L852
ANALYZED BY Thlokol Environmental Laboratory
lliiokol Corporation
P.O. Box 707 M/S 245
EJrigham City, UT 84302-0707
801-863-3732
£100-863-8080
9
Lab No Client Number
Test Requested
1 L852-1 #353, 3 FT. . T-53A
SW-846, 8260
SW-846, 7471A
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846,3050
SW 846, 9056
SW 846. 9045
1 L852-2 <«.«a S FT.. T-53A
SW-846, 8260
SW-846, 7471A
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-646,6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 3050
SW 846, 9056
sw 846, 9045
Description
Volatile Organics
CV Mercury Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
As ICP Metals Analysis (RCRA)
Cd ICP Metals Anatysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Se ICP Metals Anatysis (RCRA)
Sb ICP Metals Analysis (RCRA,)
Or ICP Metals Anatysis (RCRA)
Ba ICP Metals Anatysis (RCRA,)
ICP/GFAA Metals Digestion
Sulfate Anatysis byte
pH Electrode Measurement
Volatile Organics
CV Mercury Analysis (RCRA)
Ag ICP Metals Anatysis (RCRA)
Sb ICP Metals Anatysis (RCRA)
As ICP Metals Anatysis (RCRA)
Se ICP Metals Anatysis (RCRA)
Ba ICP Metals Analysis (RCR/k)
Or ICP Metals Analysis (RCR/k)
Pb ICP Metals Anatysis (RCR/V)
Cd ICP Metals Analysis (RCR;^)
ICP/GFAA Metals Digestion
Sulfate Analysis by 10
pH Electrode Measurement:
Fleceived ColiectDate/Time
Matrix
03/05/97 03/05/9710:30 1
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
nrMn^m 03/05/9710:40 1
Soil '
Soil ' "- -
Soil -• '•-•' •
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Comments:
L852 6010 ICP Metals: The method used to prepare these samples for analysis results in a negative
matrix interference for Sb. >,
Certified By Date
777/s certifies that the following samples were analyzed using good laborator]/ practices to show the following results:
Page 1 of 4
Listing of Results by Sample
#
•
630-20-6
71-55-6
79-34-5
79O0-5
75<34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79^)1-6
75-69-4
75-01-4
#
#353, 3 FT., T-53A
Test Parameter
1,1. U-TETRACHLOROETHANE
1,1.1-TRICHLOROETHANE
1.1,25-TETRACHLOROETHANE
1.1,2-TOICHLOROETHANE
1.1-DICHLOROETHANE
1.1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
15,4.TRlCHLCROBENZENE
1,2.4-TRlMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-OIBROMOETHANE
1,2-DICHLOROBEN2ENE
1.2-OICHLOROETHANE
1,2-OICHLOROPROPANE
1,3,S.TRII\«ETHYLBENZENE
1 ^DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-OICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
44SOPROPYLTOLUENE
44«THYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TE IRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
OS-1.2-OICHLOROETHENE
CIS-l ,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZFNE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-OICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
HffiRCURY
ANTBIWNY
ARSENIC
BARIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
SULFATE
PH
Result
u
2JB
U
U
U
U
U
U
u u
u u u
u u u
u
u u
u
u
u u
u
u u
u
u u
u
u u
u
u u
u
u u
u
u u
u
u u
u
u u
u u u u
u
u u
u
u u u u
u u
u
u
u
6
u 39
u
43
7
u
u
54
7.88
Units
U9*g
uflrtcg
ug/kg
ug/kg
U9*g
ugAg
ug/kg
ugrttg
ugrtcg
ug/kg
ugrtcg
ugrtcg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ufl/kg
uflrttg
ug/kg
ugrttg
ugftg
U9*8
ug/kg
ug*B
ug/kg
U8*g
ugrttg
ugAg
uglkg
Ufl/kg
U0*8
U9*g
UB*g
ugAa
ugfltg
U9*g
ua*g
ugrtcg
ufl*g
ugrtcg
ug/kg
"8*9
ugrtcg
U9*g
ug/kg
ugftg
ug/ko
UB*g
"8*9
ug/kg
U9*g
U9*8
ugflcg
U8*B
"9*8
"8*8
"0*9
"8*8
"8*8
ug/kg
ug/kg
"8/8
ug/g
ug/g
"8/8
ug/g
"9/8
ug/g
ug/g
ug/g
ug/g
lah ID: L852.1
Det
Limit
.2
2
J
2
.1
.6
2
2
2
2
2
2
2
.1
2
2
2
2
2
2
2
10
2
10
2
2
10
10
.2
.2
.2
.3
.1
4
.3
2
.4
.4
.6
2
2
3
2
2
.3
2
2
2
.3
2
2
2
2
2
2
2
3
.3
2
2
.3
.3
.4
.01
2.7
2.7
.05
.1
.3
1.4
32
2
2.1
Rep. DiL
Limit Factor
10 1
10 1
10 1
10 1
10 1
10 11
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1 .
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 11
10 11
10 '1
10 1
10 1
10 1
10 1
10 1
.04 1
14 1
14 1
J 1
.5 1
1.4 1
6.7 1
16 1
.8 1
11 25
1
Collect
Msatod
SW-846,8260
SW-846.8260
SW-846,8260
SW-846,8260
SW-846,8200
SW-846,8260
SW-846,8260
SW-846.8260
SW-846.826U
SW-846.8260
SW-846,8260
SW-846.8260
SW-846.8260
SW-846,8260
SW-846, 8260
SW-846.8260
SW-846,8760
SW-846,8260
SW-846,8260
SW-846,8260
SW-846.8260
SW-846,8260
SW-846,8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846, 8260
SW-846.8260
SW-846.8260
SW-846,8260
SW-846, 8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-S46.8260
SW-846,8260
SW-846,8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846,8260
SW-846,8260
SW-846. 8260
SW-S46.8260
SW-846.8260
SW-846. tUbU
SW-846.8260
SW-846.8260
SW-846.8260
SW-846. 8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.7471A
SW-846.6010
SW-846,6010
SW-846,6010
SW-846.6010
SW-846.6010
SW-846.6010
SW-846.6010
SW-846,6010
SW-846.3050
SW 846.9056
SW 846.9045
03rtJ5«7 10:30
Analvst Test Date
MMR 03/1QS714J7
lUMR 03/109714:37
MMR 03/10/9714:37
MMR 03/10/9714:37
MMR 03/10/9714:37
MMR 03/10/9714:37
kMR 03/10/9714:37
MriR 03/10/9714:37
MUIR 03/10/9714:37
MMR 03/10^714.37
lyMR 03/10^714:37
MMR 03/10/9714:37
MMR 03/10/9714:37
-MMR - 03/10«7 1437
MMR 03/10/9714:37
MMR 03/10/9714:37
DMR 03/10/9714:37
-•" MMR •03/10«714:37
,'•• MMR 03/103714.37
' "NMR 03/10«714:37
. MMR 03/10/9714:37
. }JMR 03/10/97 14:37
VMR 03/103714:37
MMR 03/103714:37
MMR 03/10/971437
MVIR 03/103714:37
MMR 03/103714:37
MMR - 03/1037 14:37
-NMR 03/103714:37
"NMR ~03/rd37T4:37
MMR 03/103714:37
MMR 03/1037.1437
MMR 03/103714:37
MMR 03/10371437
NMR 03/103714:37
NMR 03/10371437
MMR 03/10371437
MMR 03/10/9714:37
MMR 03/10371437
MMR 03/10371437
MMR 03/10371437
MMR 03/10371437
MMR 03/103714:37
NMR 03/103714:37
NMR 03/103714:37
NMR 03/103714:37
NMR 03/10371437
MMR 03/103714:37
NMR 03/103714:37
- MMR 03/10«714:37
MMR .03/103714:37
MMR 03/10/971437
MMR 03/10371437
MMR 03/103714:37
MMR 03/10371437
MMR 03/103714:37
MMR 03/103714:37
MMR 03/103714:37
MMR 03/10371437
ItMR 03/103714:37
. MMR 03/10371437
NMK 03/103714:37
NMR 03/10371437
KEN 03/193710:59
KWB 03/243713:41
KWB 03/243713:41
KWB 03/243713:41
KWB 03/243713:41
KWB 03/243713:41
KWB 03/243713:41
KWB 03/243713:41
KWB 03/243713:41
KWB 03/1937 00:00
CRS 03/0737 21*6
MtTB 03/183713:30
Page 2 of 4
#
#
1 Sample 10
630-20-6
71-55-6
79-34-5
T&OO-S
7504-3
75-35-4
563-58^
87-61-6
96-18-4
120-82-1
05«3-6
96-12-8
106-93-4
05-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108.90-7
75-00-3
67-66-3
74-87-3
156-59-4
: #353.5 FT.. T-53A
Test Parameter
1.1.12-TETRACHLOROETHANE
1.1.1-TRICHLOROETHANE
1.1.2.2-TETRACHLOROETHANE
1.1.2-TRlCHLOROETHANE
1.1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1.2.3-TRICHLOROBENZENE
1.23-TRICHLOROPROPANE
1.2.4-TRCHLOROBENZENE
1.2.4-TR»^THYLBENZENE
1,2-DIBROMO-W»HLOROPROPAN
1.2-DIBROMOETHANE
1.2-DlCHLOROBENZENE
1.2-DlCHLOROETHANE
1.2-OICHLOROPROPANE
13.5-TRMETHYLBENZENE
1 ^DICHLOROBENZENE
I^OICHLOROPROPANE
1.4-OICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXAh40NE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
•WETHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROD^THANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
as-l .2-OICHLOROETHENE
10061-01-5 aS-13-DX>ILOROPROPENE
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
05-47-8
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
DIBROMOCHLOROMETHANE
DIBROMOtUETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
ItR I-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1.2-DICHLOROETHENE
10061-02-6 TRANS-1.3-DICHLOROPROPENE
7W)1-6
75-69-4
754)1-4
TRICHLOROETHENE
TRK»1LOROFLUOROMETHANE
VINYL OILORIDE
MERCURY
ANTIMONY
ARSENIC
BARIUM
CAOMUM
CHROMUM
LEAD
SELENILHM
SILVER
ICP/GFAA METALS DIGESTION
SULFATE
PH
Result
u
2.7 JB
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u u
u u
u
u u u
u u u
u u
u
u
u u
u u u
u u
u
u u u u
u u u
u u u u
u u u
u
u u
u
u 3.2
u 28
u 19
U
u
u
47
7.92
Vnit«
"8*8
"8*8
ugrtcg
"9*8
"8*8
"8*8
"9*9
"8*8
"8*8
"9*9
"8*8
"9*8
"8*8
"8*8
"8*8
"8*9
"0*8
"8*8
"9*9
ug*g
"8*8
"9*8
"9*9
"8*8
"g/kg
"9*9
"8*8
"9*8
"8*8
UB*8
"8*8
"9*8
"9*8
"8*8
"9*9
"8*8
"9*8
"8*8
"9*8
"9*8
ugflcg
"8*8
"9*8
"8*8
"8*8
"8/1(0
"9*8
"8*9
"9*8
"8*8
"9*9
U9*g
"9*8
ug/kg
"8*9
"8*8
"8*8
"8*8
"8/kg
"gftg
"9*8
"8*9
ug/kg
"9/8
"9/8
U9/9
"0/8
"8/9
"9/8
ug/g
ug/g
ug/g
"8/8
Lab ID: L852-2
Det.
Limit
2
2
3
.2
.1
.0
.2
.2
.2
.2
2
2
2
.1
2
2
2
2
2
2
2
10
.2
10
.2
.2
10
10
.2
.2
.2
3
.1
.4
3
.2
.4
.4
.6
2
2
3
2
2
3
.2
2
2
3
2
2.
2
2
2
2
2
S
3
2
2
3
3
.4
01
:Z.7
2.7
.05
.1
3
13
32
2
2.3
Rep. DIL
Umit Factor
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
.02 1
13 1
13 1
3 li
JS 11
13 -1
6.7 1
16 '1
.8 '1
12 25
1
Collect Date: 03/05/9710:40 |
Mefto<<
SW-846.8260
SW-846,8260
SW-846,8260 .
SW-846.8260
SW-846, 8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846. 8260
SW-846. 8260
SW-846.8260
SW-846.8260
SW-846,8260
SW-846.8260
SW-846,8260
SW-846,8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846,8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846, 8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846. 8260
SW-846.8260
SW-846, 8260
SW-846.8260
SW-846.8260
SW-846. 8260
SW-846.8260
SW-846. 8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-&46.8260
SW-846. 8260
SW-846.8260
SW-846.8260
SW-846, 8260
SW-S46. 8260
SW-846. 8260
SW-846,826U
SW-846, 8260
SW-846,8260
SW-846,8260
SW-846. 8260
SW-846. 8260
SW-846,8260
SW-846.8260
SW-846.8260
SW-846, 8260
SW-846,8260
SW-846.7471A
SW-846,6010
SW-846, 6010
SW-846,6010
SW-846.6010
SW-846.6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,3050
SW 846, 9056
SW 846, 9045
Analyst Test Pate
MMR' 03/103715:12
MMR 03/103715:12
.MMR 03/103715:12
MMR 03/103715:12
MMR 03/1103715:12
MMR 03/103715:12
MIMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
-MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
NMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/1Q3715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
NMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MM^ 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MM^ 03/103715:12
NMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
MMR 03/103715:12
KEN 03/193711.-02
KWB 03/243713:44
KWB 03/243713:44
KWB 03/243713:44
KWB 03/243713:44
KWB 03/243713:44
KWB 03/243713:44
KWB 03^43713:44
KWB 03/243713:44
KWB 03/1937 OOflO
CRS 033737 2123
MTB 03/183713:30
Page 3 of 4
#
•
Data Reporting Qualifiers •«V * ft'*^'•-?
U Indicates compound was analyzed for and was not detected, or the impound was detectied but was
below the detection limit. • .. .v.
B Gas Chromatography and Mass Spectral Data Flag, lliis flag is used when an analyte js foundin, \i
the blank as well as the sample
J Gas Chromatography and Mass Spectral Data Rag. Indicates an eistimated value. This flag is used
either when estimating a concentration for tentatively identified compounds or when the data
indicated the presence of a compound that meets the identification criteria but the result is less than
the specified reporting limit (e.g. 3 J with a reporting limit of 10)
DeL Limit Method Detection Umit (approximately three times the signal noise leveO H;^-^^ C:?:..:^. :-
Rep. Limit Reporting Limit is normally the value of the lowest StandanI mn with the analysis. The .yaliie
isapproximately 5 to 10 times the Method Detection Limit '^
-.,;..: ,;..«ki'& ?:i-:-vrrvj
Dil. Factor Dilution Factor - The prepared sample was diluted by this factor because the sample was ''
too concentrated or due to other interferences in the sample matrix. Any dilution factor' "-•
causes an appropriate increase in the method detection limit and reporting limit" * '* ^^"'^
.*-. . tl -. .1 .y / '.i.
•• fJl-
... , ^
•''••T.--
•.'•-> v.-..
... - '•
•:.^.;-.j(,>|'!
lii-.l.-OJ
...... • w
Page 4 of 4
ENVIRONMENTAL LAB WORK RILQUEST
J^= THIOKOL ENVIRONMENTAL LABORATORY
II FROM: . n Jl ,
II ORGANIZATION
1 £nv/iron/KcnfL^
EXTENSION
MAILSTOP
LWR No. El 1373
Login No. Lies' 1
COSTCENTIil WORKORDER
/E940
DATE
7 Apf 1/^7
REPORT RIS.ULI'S TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE
1-/0 ^^f"
•SlUMM 2ft
TYPE
7/V>7f; y
LOCATION TIME TEST REMARKS
X-io ^ /Ol<
mima
JlCTlA McHils-^
n y 1-10 5 /o\^ lAc/^ -ezho
3 I-l* Hr^tttH tl I'/oS /32>0 ;ggZ4 AUfab^
«^
/• /' y
^<S
c
Cb<-
kA
Cij^-^
yrcrr \Jo.jf\
X-ioS /Zoo V&fir " ^ZC?0
iL yJ^AWgWO , TSC ^^UXW^ —, V-X/r^'
^JLa/ji • i2\ (tilo- r.
:iJ2,dc^LJiu iLflJ. .Eca^ H iirw i.
vtXSL/r G-WTSSL i?.oi<S^ ^^-ni-^A -VroLAJc fL Mi.
CHAIN OF CUSTODY
RELINQUISHED BY
££lt^
DATE
VAfidlji
TIME
/f^g
RECEIVED BY
MQ^^CrfK^rf^A'
DATE
7/?^^/:'^?-
TIME
/^:zo
m DATE COMPLETED
FOR LABORATORY USE ONLY
DATE REPORTED SIGNATURE
• •>'••*-• ;• -s-v-fc..*.'-. "^f^c.^*
CERTIFICATE OF ANM^YSIS
gf-r^i •'-.1't?'.>„
iZ:^-.'
. jv»-. •..it,:?'-,/
Listing of sample information and Testinn Reqiwsted
#
Thursday, Maya. 1997
TESTED FOR Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp, UT 84322
Frank Waiker
Project: Solid Waste Mgmt Inveal
T^.v 1. _j^. ^^•. •-•.. .t--^.':-'-r*^..' •
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City. UT 84302-0707
801-863-3732
800-863-8080
Login Number L905
Lab No Client Number
Test Requested Description
Received CollectDate/Time
^ Matrix
1 L905-1 DRYWELL SWMU 234 Z MOS
SW-846, 7740
SW-846,7471A
SW-846, 7060
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
GFAA Selenium Anatysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Nl ICP Metals Analysis (RCRA)
Sb ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCFtA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCFIA)
ICP/GFAA Metals Oigestton
1 L905-2 DRYWELL SWMU 234 2" 1-10 S
SW-846, 8260 Volatile Organics
1 L905-3 DRYWELL SWMU 234 4' 1-10 S
SW-846.7740
SW-846, 7471A
SW-846,7060
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846,6010
SW-846. 3050
GFAA Selenium Analysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Arsenic Anatysis (RCRA)
Ag ICP Metals Anatysis (RCRA)
Sb ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Ba ICP Metals Anatysis (RCRA)
Cd ICP Metals Analysis (RCI^)
Ni ICP Metals Analysis (RCIR^k)
Cr ICP Metals Analysis (RCIR/V)
ICP/GFAA Metais Olgestkm
IL905-4 DRYWELL SWMU 234 4- MOS
SW-846, 8260
1 L905-5 BACKGROUND MO
SW-846,7740
SW-846, 7471A
SW-846.7060
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-646.6010
SW-846, 6010
SW-846. 6010
SW-846,3050
1 L905-6 BACKGROUND MO
Volatile Organics
MOB
GFAA Selenium Analysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Sb ICP Metals Analysis (RCRA)
Nl ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
ICP/GFAA Metais Digestion
MOB
04AJ7/g7 04/07/9710:15
SOU
Soil
: Soil
Soil
Soil
Soil
SOU
Soil
soil
Soil
Soil
(VW07/97 04/07/9710:15
soil
nimiST 04/07/9713:00
Soy
soil
Soil
soil
SCO
Soil
Soil
Soil
Soil
Soil
Soil
04AJ7/97 04/07/9713:00
Soil
04/09/97 04A}9/g714:30
Soil
Sou
Soil
Sou
Soil
Soil
Soil
Soil
Soil
Sou
Soil
04AJ9/97 04«)9/9714:30
1
1
1
1
1
1
SW-846, 8260 VolatUe Organics Soil
Page 1 of 7
#
comments: • , • ^ -^^li^-f! ,:;./
There was a negative matrix interference for antimony and evidemce of sample nonhomogeneity for Ba,
Cr, Cu, and Pb based on matrix spike results,, The actual results may be 3-5 times greater than those
reported. • •jr:'-.-;.^-'s--.-. ;•: -•i^-:-^-,--:-;-:. --
L905-2 Volatile Organics: Matrix interference was noted on this isaiTiple.
L905-4 Volatile Organics: Miscelaneous hydrocartions typical of gasoline and/or deisel fuel were
detected in this sample. * >7
<:CX^-)fl./Z/^ r-/e/n
X Certified By Date
This ceitmes that the foUowing samples were analyzed using good laboratory' practices to show the following results:
«
#
Page 2 of 7
•^-f'*9C't
Usting of ResiLillter by Sarnple"
#
1 Sample ID: DRVWELL SWMU 234 Z MOS
Test Parameter
SELENIUM
MERCURY
ARSENIC
ANTIMONY
BARIUM
CADMIUM
CHROMIUM
LEAD
NICKEL
SILVER
CP/GFAA METALS DIGESTION
Result
U
11
5.8
U
461
IJ
22
36
17
2
Units
ug/g
us/fl
"9/8
"9/8
"8/8
ug/g
ug/g
ug/g
"8/8
ug/g
•»# Lnb ID:
Det. rRop.
Umit Limit
.»C-^-3-2 .01 .03
S 32
24 12
.OS 2
X8 .5
2 12
12 5.0
5 2.4
.1 .7
VBOS-\
CO.
Factor
* ' '^ Collect Dote: 04A)7/9710:15 |
.;vr- •
^etiHHl
: SW-846.7740
'' SW.848. 7471A
; SW-846.7060
SW-846.6010
SW-846.6010
SW-846.6010
SW-846.6010
SW-846.6010
SW'446,6010
SW-846.6010
SW-846.3050
, •••
-Analyst
CRS
KEN
CRS
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
lBtPat«
053237 1625
04/103711:46
05323711:49
04/1137 14:49
04/113714:49
04/113714:49
04/113714:49
04/113714:49
04/113714:49
04/1137 14:49
043937 00.-00
«
•
Page 3 of 7
I.«^l^^-^"*:^*t^-~^
I Sample ID: DRYWELL SWMU 234 Z l-10S^ .*4W li:iBbiD:L9(l5-2 Collect Date; 04/07/9710:1 sl
Tyf Parameter R»«uH Upjtt
^Det..'>)R.p.
Limit Limit
DB. V
Factor M*<tiod ?Aiwty«t Test Date
#
630-20-6
71-55-6
7»-34-6
7»«0-5
75^4-3
75-35^
56:»-S8-6
87-61-6
96-18-4
120-82-1
9S«3-€
06-12-8
106-93-4
95-50-1
107-06-2
78-87-S
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
7»«3.3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
7WXK3
67-66-3
74-87-3
158-59-4
1.1.12-TETRACHU3ROETHANE
1,1.1-TRICHLOROETHANE
1,122-TETHACHU)ROETHANE
1.12-TPICHLOROETHANE
1,1-DICHLOROETHANE
1.1-niCHLOROETHENE
1,1-OICHLOROPROPENE
123-TRK>ILOROBENZENE
1 2.3-TRK:HLOROPROPANE
12.4-TRICHLOROBENZENE
1 2.4-TRIMETHYLBENZENE
12-D1BROMO-3-CHLOROPROPAN
12-D(BROMtOETHANE
12-DICHLOROBENZENE
12-OICHLOROETHANE
1,2-OICHLOROPROPANE
13.5-TRBMETHYLBENZENE
1 ,U3ICHLOROBENZENE
1 ^^DICHLOROPROPANE
1.4-DK»1LOROBENZENE
22-DlCHLOROPROPANE
2-BUTANONg
2-CHLOROTOLUENE
2-HEXANONE
401LOROTOLUENE
4-4SOPROPYLTOLUENE
44METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODK>1LOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
aS-1.2-OICHLOROETHENE
10061-01-5 aS-l 3-OICHLOROPROPENE
124-48-1
74-95-3
75-71-8
10O41-4
87-68-3
98-82-8
108-38-3
TS-OQ-Z
104-51-8
103-65-1
91-20-3
96-47-6
135-98-8
10O-42-5
98064
127-184
108-88-3
15&«05
OIBROMOCHLOROtWETHANE
DIBROMOMETHANE
DK>ILORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYIENE
METHYLENE CHLORIOE
N-BUTYLBENZENE
N-PROPV13ENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
IbRT-BUTYlBENZENE
TETRACHLOROETHENE
TOLUENE
TKANS-12-DICHLOROETHENE
10061-02-6 TRANS-1.3-OICHLOROPROPENE
79-01-6
75-69-4
75^)1-4
TRrcHLOROETHENE
TRICHLOROaUOROMETHANE
VINYLCHLORIDE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u u u u u u u u u u u u
u
u u u
u u u u u u
u
u
u
u u u u
u u
u
u
u
u
u
u
u
u
u
"9*8
"0*9
"9*8
"tl*8
"»*8
u»*B
m*8
^^*8
m*s ualkg
"0*0
"9*8
ug/kg
ug/kg
"9*0
ug/kg
"9*0
ugAs
"0*8
"9*0
ugAis
"B/IC8
ug/kg
UB*g
ug/kg
ug/kg
ugAcg
ug/kg
ug«g
ug/kg
ug/kg
uo«g
ug/kg
"0*9
uo*a
ug/kg
ug/kg
ug/kg
"9*8
ug/kg
ug/kg
ugftg
ug/kg
"8*8
ugftg
ug/kg
ug/kg
ugrtcg
ug/kg
ug/kg
ug/kg
"0*0
"0*9
ug*g
ug/kg
ug/kg
ug/kg
"9*8
u8/k8
ug/kg
ug/kg
uglkg
uo*g
,...2
• .2 •
- .a-
2
.1-
6
2
2
. 2
'2
2
2
2
.1
2
2
2
• 2
2
2
2
10
2
10
2.
2
10
10
2
2
2
3
.1
.4
3
2
.4
.4
i!
2
2
3
2
2
3
2
2
2
3
.2
.2
2
2
2
2
2
,9
3
2
2
3
3
.4
?*10 "
^10
#-10
10
''10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-446.
SW-846,
SW-846,
SW-846,
SW-846.
SW-846.
SW-846.
SW-646.
SW-846.
SW-846.
SW-e46.
SW-846,
SW-846.
SW-846.
SW-846,
SW-846.
SW-846.
SW-848,
SW-846.
•SW.848,
SW-446,
SW-846.
SW-846.
SW-846.
SW-846,
SW-846.
SW-846,
SW-846,
SW-846
SW-846
SW-846
SW-646
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-«46
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-84fl
SW-846
SW-84e
SW-&4e
SW-84e
sw-a4«
SW-84C
SW-84(
SW-84(
SW-84(
SW-84(
SW-84(
SW-844
SW-841
SW-841
SW-841
SW-841
SW-841
060
1280
B260 :
B260
fl260
8260
B260
B260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
,8260
.8260
,8260
,8260
,8260
,8260
,8260
.8260
.8260
,8260
.8260
.8260
1.8260
.8260
1,8760
),8260
S.B260
S.8260
1.8260
}.8260
;.8260
9.8260
9,8260
S,8260
5.8260
L MMR
-'.' MMR
iwMR
MMR
'MMR
' MQMR
'MMR
:-MMR
PMWK
MMIC
MMR
MMR
PWnll
MMR
MMR
RAnK
MMR
MMR
MMR
' , - MMR
' NMR
MMR
MMR
MMR
PWnK
MMR
MMR
wnrmK
MMR
RflvIK
PWnn
MMR
MMn
MMR
MMR
MMR
MMR
MMR
MMR
MMR
HAnn
MMR
HWnK
MMR
NMR
PreWIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
fjfjtn
NMR
PWnlC
HraWn
RranR
lUMR
MMR
RranH
MMR
HwwH
04393716:57
0439371657
0430371657
043937 1657
04A)9371657
0439371657
043937 1657
04AJ937 1657
043937 16.57
043937 1657
0AI0aiB7 1657
043937 1657
043937 1657
0439371657
043937 1657
04/00371657
043937 1657
04A»371657
0439371657
043937 1657
043937 16.57
043937 16:57
043937 16:57
04393716:57
04393716.57
043937 1657
043937 1657
04/0937 1657
043937 16:57
043937 16.57
04393716:57
043937 16:57
043937 16.57
043937 1657
043937 16.57
043937 1657
0439371657
043937 1657
043937 16:57
043037 16:57
043937 16:57
043937 1657
04/0937 1657
043937 1657
043937 16:57
04393716:57
043937 16:57
043937 1657
043037 1657
043937 16.57
04na«71«57
043937 16:57
043937 1657
043937 16:57
043937 16.57
043937 1657
043937 1657
043937 1657
0439371657
04A)937 16:57
043937 16:57
0439371657
043937 1657
1 Sample ID: DRYWELL SWMU 234 4' MOS LablD:lJ905-3 Collect Date: 04/07/9713.00
T?st parameter
SELENIUM
MERCURY
ARSENIC
ANTMONY
BARIUM
CADMIUM
CHROMIUM
LEAD
NICKEL
SILVER
ICP/GFAA METALS DIGESTION
Result
U
.4
11
U
162
.8
24
16
14
U
Units
U9/B
ug/g
"8/8
"8/8
"0/8
"8/8
ug/g
U8/8
ug/g
"8/9
CteL
Limit
12
.01
12
3
.196
.1
3
115
.6
2
Rep.
Limit
4
.04
4
IS
3
.6
,1-5
7.4
3
.9
DIIL
Factor Methocf
SW-84a.7740
SW-846. 7471A
SW-846,7060
SW-B46.e010
SW-846.6010
SW-846.6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846.3050
Analyst
CRS
KEN
CRS
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
Page
Test Date
0S32371634
04/10371154
0632371158
04/11371452
04/11371452
04/11371452
04/113714:52
04/113714.52
04/113714:52
04/1137 14:52
04393700:00
4of7
•
^
1 Sample ID
630-20-6
71-55-6
79-34-6
79O0-5
75-34-3
ra-35-4
563-58-6
87-61-6
96-18-4
120«2-1
05-63-6
06-12.«
106-93-4
05-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
500-20-7
78-93-3
95-49-8
591-78-6
106-43-4
9M7-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-S
56-23-5
108-90-7
75-003
67-66-3
74-87-3
156-59-4
J V
: DRYWELL SWMU 234 4' MOS
Tg^ Parameter
1,1.12-TETRACHLOROETHANE
1.1.1-TRICHLOROETHANE
1.122-TETRACHLOROETHANE
1.12-TRICHLOROETHANE
1.1-DICHLOROETHANE
1 .I-DICHLOROETHENE
1.1-DICHLOROPROPENE
123-TRK»<L0R08£NZENE
123-TRICHLOROPROPANE
12.4-TRICHLOROBENZENE
12,4-TRMETHYLBENZfcNE
12-OIBROhK>-3-Cm.OROPROPAN
12-DIBROMOETHANE
12-DICHLOROBENZENE
12-OICHLOROETHANE
12-OlCHLOROPROPANE
13.5-TRIMETHYLBENZENE
1343ICHLOROBENZENE
13^5ICHLOROPROPANE
1.4-DICHLOROBENZENE
22-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
44SOPROPYLTOLUENE
44(1ETHYL-2-PEMTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CtS-12-DICHLOROETHENE
lOOei-OI-S CIS-13-DICHLOROPROPENE
124-18-1
74-95-3
75-71-8
100-41-4
87-683
98-82-8
108-.T8-3
75^19-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60^
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DtCHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYIRFNZENE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-12-OICHLOROETHENE
10061-02-6 TRANS-1.3,45ICHLOROPROPENE
70^)1-6
75-69-4
75-01-4
TRICHLOROETHENE
TRICHLOROFLUOROftCTHANE
VINYLCHLORIDE
Result
u
13J
U
U
U
U
U
U
U
u u
u
u u
u
u u
u u u
u
11
u
u
u u
u 41B
15J
U
U
U
U
U
U
u
u u
u
u u
u
u u u
u
u 3.6 J
U
U
U
u 3.8 J
U
U
U
U
2J
u U
2.SJ
U
U
Units
"9*8
ug/kg
"9*8
"g/kg
"0*8
"9*8
"9*9
ug/kg
"8*8
"9*8
ug/kg
ug/kg
ug/kg
"8*8
"8*8
ug/kg
"8*9
"0*8
"g/kg
"0*9
ug/kg
ug/kg
"g*8
ugftg
ug/kg
ug/kg
"9*8
"8*8
"8*8
"B/kg
ug/hg
ugfltg
UB*g
"8*8
"9*8
"0*8
"8*8
"8*8
ug/kg
ugAcg
ug/kg
ug/kg
U9*g
ug/kg
ug/kg
ug/kg
U9*g
U9*g
U9*B
ugflcg
ug/kg
ugflcg
ugflcg
"8*8
"gflcg
ugflcg
ugflcg
ug/kg
"S/kg
ugfliB
ugAcg
ug/kg
ugflcg
^m s^^lS^
LablD:L906-4
DeL
Limit
2.
2
3
2
.11
.« 2
'2.
2.
2
2
2
2
.1
2
2
2
2
2
2
2
10
2
10
2
2
10
10
2
2
2.
3
.1
.4
3
2
.4
.4
.6
2
2
3
2
2
.3
2
2
2
3
2
.2
2
2
2
2
2
.9
3
2
2
3
3
.4
Rep. "-DIL
LimK Facte*
; 10 V
10 1
10 -':• 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
i^iii^^^^^-^-. • •••r
Trvj>v>7<f coflgrtpate; 04A?7/9713.-00 |
-^^•^TSV^^"^*
r Metlwd ''
.«rSW.846.8280
-,SW446.8260
*• SW-846.8260
SW-846.8260
SW-846,8260
' SW-846.8260
SW-846.8260
SW446.8260
SW-846,8260
SW-846.8260
SW-846.8260
SW-846,8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-84e.8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846, 8260
SW-846,8260
SW-846,8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846,8260
SW-846.8260
SW-846,8260
SW-846.8260
SW-846.8260
SW-846,8260
SW-S46,8260
SW-846,8260
SW-846.8260
SW-846.8260
SW-846,8260
SW-846.8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846,8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-a46. 8260
SW-846.8260
SW-846,8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
8W-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
,,rajVj;.-;- -
'-Analyst
-•. RffiniC
'-'d- MMR
MMR
. RffnTi
RWW^
MMR
NMR
.• MMR
iAJR
NMR
MMR
MMR
MMR
NMR
NMR
RWnr\
HWAK
MMR
-•' HWnK
MMR
MMR
RW"R
RWlr\
MMR
RAran
RvMK
'MMR
MMR
MMR
Mw^
MMR
MMR
MMR
BWWA
MMK
MMR
MnW\
MMR
RWnK
kMJO
MMR
RmMR
HffVIK
RffVIn
RrWlr\
MMR
IffMK
• MWIK
MMR
MMR
MMn
HWnR
MMR
fimwm\
RttnR
mvm
mvm
MMR
BrlwK
RBMK
Test Date
0439»71734
04/09371734
0439371734
0438371734
0439371734
0439371734
04393717:34
0439371734
0439371734
0439371734
0439371734
0439371734
0430371734
0439371734
0430371734
0439371734
0439371734
0430371734
0439371734
0439371734
043937 17-34
0439371734
0439371734
0439371734
043937 17:34
0439371734
04393717:34
0439371734
0439371734
0439371734
0439371734
0439371734
043937 17:34
0439371734
0439371734
0439371734
0439371734
043937 17:34
04393717:34
043937 17:34
04A)9371734
04A)9371734
04/09371734
0439371734
04393717:34
0439371734
0439371734
0439371734
0439371734
04/09371734
04/DaS7 17:34
043937 17:34
043937 17:34
043937 17:34
0430371734
0439371734
0439371734
0439371734
0439371734
0439371734
04A)0371734
0439371734
0439371734
ISample ID: BACKGROUND MO MOB Lab ID: Lg05-!3 Collect Date: 04^)9/9714:30
Test Pararneter
SELENIUM
MERCURY
ARSENIC
ANTIMONY
BARIUM
CADMIUM
CHROMIUM
LEAD
NICKEL
SILVER
ICP/GFAA METALS DIGESTION
Result
0
.02
11
U
122
.6
17
4.1
14
2
Units
ug/g
ug/g
"9/8
"9/8
ug/g
"9/8
ug/g
"8/8
ug/g
ug/g
D^
Limit
,9
.01
.9
23
.05
.(» 2
12
.5
.1
Rep.
Limit
3.1
.03
3.1
12
2
JS
12
5.8
23
.7
DiL
Fodior Method
SW-846.7740
SW-846.7471A
SW-846. 7060
SW-846.6010
SW-846.6010
SW-846,6010
SW-846, 6010
SW-846,6010
SW-846. 6010
SW-846, 6010
SW-846. 3050
Aqalvst
CRS
KEN
CRS
KWB
KWB
KWB
KWB
KWB.
KWB
KWB
KWB
Page
Test Date
05/02371656
04/103712:41
053237 12:19
04/113715fi7
04/113715^7
04/1137 15S7
04/113715*7
04/1137 15K)7
04/1137 1S.-07
04/1137 15fl7
043937 000)
5of7
4''':-'
•'^:-
*^^T**-^
[SamplelD: BACKGROUND MO MOB Ub ID: L90&<i '"-^^**^ Collect Date: 0W9W714:30 |
•ir.
itt
•
Test Perameter
630-20-6 1,1,1.2-TETRAC»«^}ROETHANE U
71-55-6 1,1,1-TKK>ILOROETHAKE U
70-34-6 1,122-TETRACHLOROETHANE U
7»«W 1,12-TRK>iLOROETHANE U
75-34-3 1,1-OICHLOROETHANE U
76-35-4 1.1.DK>ILOROETHENE U
563-68-6 1,1-DICHLOROPROPENE U
87-61-6 123-TRK>ILOROBENZENE U
06-18-4 12.3-TTOCHLOROPROPANE U
120-82-1 t2.4-TWCHLOROBENZENE U
06-63-6 12.4-TRMETHYLBENZENE U
06-12-8 12-OIBROMO-30COROPROPAN U
106-93-4 12-OIBROMOETHANE U
95-50-1 12-OICHLOROBENZENE U
107-06-2 1,2-DICHLOROETHANE U
78*7-5 12-DICHLOROPROPANE U
108-67-8 135-TRWETHYLBENZENE U
541-73-1 13-DICHLOROBENZENE U
142-28-9 13-OICHLOROPROPANE U
106-46-7 1,4-DK>1LOROBENZENE U
590-20-7 22-OK>1LOROPROPANE U
78-93-3 2-BUTANONE U
95-49-8 2-CHLOROTOLUENE U
991-78-6 2-HEXANONE U
106-43-4 4-CHLOROTOLUENE U
09-87-6 44SOPROPYLTOLUENE U
108-10-1 4-METHYL-2-PENTANONE U
67-64-1 ACETONE U
71-43-2 BENZENE U
108-86-1 BROMOBENZENE U
74-87-5 BROMOCHLOROMETHANE U
75-27-4 BROMODK>ILOROMETHANE U
75-25-2 BROMOFORM U
74-83-9 BROMOMETHANE U
56-23-S CARBONTETRACHLORIDE U
108-90-7 CHLOROBENZENE U
75«>-3 CHLOROETHANE U
67-66-3 CHLOROFORM U
74-87-3 CHLOROMETHANE U
. 156-59-4 aS-12-DICHLOROETHENE U
10061-01-5 aS-13-OICHLOROPROPENE U
124-48-1 OIBRQMOCHLOROMETHANE U
74-95-3 DIBRQMOMETHANE U
75-71-8 DK:HLORODIFLUORaMETHANE U
100-41-4 ETHYLBENZENE U
87-68-3 HEXACHLOROBUTADIENE U
9842-8 ISOPROPYLBENZENE U
108-38-3 M,P-XYLENE U
75-09-2 METHYLENE CHLORIDE U
104-51-8 N-BUTYLBENZENE U
103-65-1 N-PROPYLBENZENE U
91-20J NAPHTHAL£NE U
95-47-6 O-XYLENE U
135-98-8 SEC-BimrLBENZENE U
100-42-5 STYRENE U
08-0fr6 TERT-BUTYLBENZENE U
127-18-4 TETRACHLOROETHENE U
108-88-3 TOLUENE U
156-60-5 TRANS-12-OICHLOROETHENE U
10061-02-6 TRANS-13-DICHLOROPROPENE U
79-01-6 TRICHLOROETHENE U
75-69-4 TRICHLOROFLUOROMETHANE U
75-01-4 VINYLCHLORIDE U
Result Units
"g/i(B
ug/kg
"9*8
ugflcg
"9*g
ugflcg
ugfltg
"8*8
"gflcg
ug*e
"9*8
usflc8
"8/k8
"9*9
ugflcg
"gflcg
"gflcg
ug/kg
ugflcg
ugflcg
ugflcg
DtA. -Rep.
Umtt LImtt
DHL • '^: "T^i^f^^^
ugflcg
ugflcg
ugflcg
ugflcg
ugflcg
ugflcg
ug/kg
ugflcg
"8*8
"S/lc8
ugflcg
uglkg
"g*B
ug/ks
ugflcg
ugflcg
ug/kg
ugflcg
ugflcg
ugflcg
ugflcg
ugflcg
ug/kg
ugflcg
ug/kg
ug/kg
ugflcg
ugflcg
ugflcg
ug/kg
ugflcg
ug/kg
ugflcg
ugflcg
ugflcg
U8/k8
us/kg
"8*8
ugflcg
ugflcg
,2
2
3
.2
.1
.6
.2
,2
2
2
2
2
2
.1
2
2
2
2
2
. 2
2
10
2
10
2
2
10
10
2
2
2
3
.1
.4
3
2
.4
.4
.8
2
2
3
2
2
3
2
2
2
2
2
J!
2
ja a
2
2 3
3
.4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Fe^or Method
ySW-846.8260
r SW-846.8260
^!'SW-846,8260
SW-846.8260
.SW-846.8260
SW-846,8260
SW-846.8260
SW-846.8260
' SW-846.8260
SW-846.8260
.: SW-846.8260
SW.846.8260
' : SW-846.8260
; SW-846.8260
SW-846.8260
SW-846.8260
SW-848.8260
SW-846.8260
SW-846.8260
h SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846,8260
' SW-846,8260
. SW-846.8260
SW-846.8260
SW-846.8260
' SW-846.8260
SW-846.8260
SW-846.8260
SW-846,8260
SW-846.8260
^ SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846,8260
SW-846.8260
SW-846.8260
SW-846.8260
' SW^B46.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-a46, 8260
SW-846.8260
SW.846,8260
SW-846,8260
SW-846,8260
SW-846.8260
SW-846,8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846.8260
SW-846,8260
:^ Analyst
^'' MMR
* MMR
MMR
NMR
MMR
tMJO
MMR
' MMR
MMR
MMR
MMR
Ukn
MMR
|J»LJg7
NUR
MMR
IWAK
MMR
MMR
MMR
MMR
MMR
MMR
043937 18:10
04393718:10
04393718:10 -
04303718:10
043937 18:10
043937 18:10
04393718:10
043937 18:10
043937 18:10
04393718:10
043937 18:10
04393718:10
04/093718:10
043937 18:10
04393718:10
04393718:10
04A)937 18:10
043937 18:10
043937 18:10
043937 18:10
04393718:10
04303718:10
043937 18:10
043937 18:10
043937 18:10
04/093718:10
043937 18:10
04393718:10
04/0937 18:10
043937 18:10
043937 18:10
04393718:10
04393718:10
04393718:10
043937 18:10
04/0937 18:10
04393718:10
04/0937 18:10
04/0937 18:10
043937 18:10
043937 18:10
04/0937 18:10
04303718:10
043937 18:10
043937 18:10
04393718:10
04393718:10
04AB37 18:10
043937 18:10
04393718:10
04A>a«7 18:10
04/0937 18:10
043937 18:10
04/0937 18:10
04A>937 18:10
04393718:10
04393718:10
043937 18:10
04/093718:10
04393718:10
043937 18:10
043937 18:10
04A)937 18:10
Page 6 of 7
•^::^^^ti- '^-^ '• • •^'•^' •'•'i^^^^'^^lH^^^*'*^*****^**^^^
W^Si'd '^'*''' '% ••••DatalRepbrtlffTigQuaimers*
x^ U Indicates compound was analyzed for and was not detected, ortho compound was detected but was
dflk ; below the detection limit. - v^-'' .:w^-'£^-'^';';^.^-il5"i'-=^i^^^
•w '•'^i}•^dd:f^''^d^:::df-':
^J•' B Gas Chromatography and Mass Spectral Data Rag. This flag is used when an analyte is found in
the blank as well as the sample -—'^t;^^ • '%',.:\'%:-"0-:^^.-<:'
J Gas Chromatography and Mass Spectral Data Rag! Indicates ;eiin estimated value. This flag is used
either when estimating a concentration for tentatively identified compounds or when the data
Indicated the presence of a compound that meets the identification criteria but the result Is less than
thespecifledreportinglimit(e.g. 3 J with a reporting limit of 10) -"^''y .'t^f^f^:
DeL Umit Method Detection Limit (approximately three times the si^inal noise leveO
Rep. Limit Reporting Limit is normally the value of the lowest standtird mn with the analysis. The value
is approximately 5 to 10 times the Method Detection Limit *v.i S r^L-A .
Dil. Factor Dilution Factor - The prepared sample was diluted by this: factor because the sample was
too concentrated or due to other interferences in the sample matrix. Any dilution factor
causes an appropriate increase in the method detection limit and reporting limit
;. '••••.•: •^' •' ''- ^'- .-• -^ *^ • "• • s^' • '•'
Page 7of7
ENVIRONMENTAL LAB WORK HKQtEST Uo:i^-
^ THIOKOL ENVIRONMENTAL LABORATORY LWR No. E11411
Login No.
FROM: AF idkpu^ EXTEKSION COSTCENTU WOBXCODDl DATE
/z jo*j ^ 7
ORGANIZATION
5fiy/rd/i t}'\f. nh:d\
MAILSTOP
^0\^
ni(roiiTRUtn.T8'ro:
ISELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE
'/ZJlAA^-/
' IZJO^J'Z
' IZJUf^'3
'• /ZJON"^
s.
•
'• r \.
10.
M.
a
OATE
IZJfNlj
ll
n
i»
TYPE
G
l/
1/
•
U'
c
/
LOCATION
TdO 5 l>>/u^t(l
//
/I
y
TIME
oe^^
II
h
/'
nn
RtHA i^ic-hzls
iroA't,
J^CM McM/^
l/5i'/4's
-
REMARKS
CHAIN OF CUSTODY
RELINQUISHED BY
m
DATE
iiJUAtf7
TIME
/P^D
RECEIVED B)'
^•Hllljnpj
'MJ^ u^z.
DATE
;^/>JL^^ /€(//f
TIME
<i DATECOMPURB
FOR LABORATORY USE ONLY
DATEUPOaTEO SKNATHU
m
CERTIFICAI'E OF ANAI>YSIS
Listing of sample Infomiation and Testing Requested
Monday, July 14,1987
TESTED FOR Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp. UT 84322
Prank Walker
Project: Solid Waste Mgmt InveaL
l-ogin Number L1024
Lab No Client Number
Test Requested Description
^^ALYZEIi BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O, 80x707 M/5 245
Brigham City, UT 84302-0707
801-863-3732
800-863-6080
Received CollectDate/Time
Matrix
•
|L102tl 12JUN.1,
SW.848. 7471A
6W-848, 6010
SW.84e, 6010
sw-84e,60ia
SW-846,6010
SW.646.6010
SW>848,6010
sw.B46,eoio
6W-84S,3050
IL1024-2 12JUN.2.
SW.fi4e, 8260
111024^ i2JUNJ.
SW-84B.7471A
SW.84e,6010
SW.«4e,6010
sw.«4e, SOIO
SW.84e. 6010
SW-848,6010
SW.848, 6010
SW-84e.6010
SW.846,3050
1-10
1.10
MO
IL1024^ 12JUN.4. MO
S DRYWELL
CV Mercuiy Analysis (RCRA.)
Ag ICP Metals Analyaia (RCRA}
As ICP Metals Analysis (RCRA)
BB ICP Metals Analysis (RCRA)
Pb ICP Mstals Aralyas (RCRA)
8s ICP Metals Analysis (RCRA)
cr ICP Metals Analyas (RCRA)
Cd ICP Melals Analysis (RCRA)
ICP/GFAA Mcials Digeetlon
a DRYWELL
Volatile Organics
S DRYWELL
CV Mercury Anatysis (RCRA)
Ag ICP Metab AnalyDls (RCRA)
Ba ICP Metals Analysis (RCRA)
Pb ICP MstslsAnalyiiis (RCRA)
Ss ICP MetalB Analysis (RCRA)
Cr ICP Metals Analyois (RCRA)
Cd ICP Mstals AnalyQis (RCRA)
Aa ICP Metals Analysis (RCRA)
ICP/GFAA Mttato Digestion
S DRYWELL
Ofl/12fl7
(»12/97
1)6/12«7
0a/12«7
08/12/97 08:45
Soli
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
oa/iw97oa;4S
Soil
06^2/97 06:45
Soli
Soil
Soil
Soil
Soil
soli
Soil
Soil
8an
06/12/97 08:45
1
1
1
1 SW.e46,6260 Votabls Organics Soil
Comments:
There was an indication of a slight matrix interference for Ba and Cr. Resutts for As and Se also
experienced interference from the presence of aluminum and Iron respectively.
Certified By i^ 2L
James M, Anderson, QC Officer ' Dite
This certifies that th9 following samplea were analysed using good laboratory practices to show the following results:
m
Page 1 of 4
Listing of Results by Sample
IsanwIelO: 12JUN-1,M0 S DRYWELL
{sample IE
630-204
7i.«s.e
79J4.8
7040.9
7S.84.3
764S-4
9S3.5ft«
<74i-e
96-18-4
120.82.1
984M
06.12.8
10&43-4
SS-SO-I
107-06-2
71-87.8
10»^-8
S41-7S-1
142-28-9
106^«-7
990-:0>7
7843.3
96-404
991-784
106-43-4
99474
108-10-1
67-64-1
71.43'2
lOB-se-i
74-S74
75-27-4
75-25-2
74-83-9
S6-23-S
10840-7
7S-0M
6748-3
74474
18B49.4
Test Parameter
MERCURY
ARSENIC
BARIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ICPf3FM METALS OnESTION
Result
.00372
li
74
.7
IS
U
U
U
: 12JUN.2,|.10 S DRYWELL
Test Parameter
1,1.1.2.TETRACMLOROETHANE
1,1 .l-TRCHLOROETHANB
1.122.TCTRACHIJ0R0ETHANE
1,12-TRICHLOROETHANE
1,1-aCHLOROETHANE
1,1«ieHLOR0ETHENE
1.1-OICHLOROPROPENE
U^TRtCHLOROBENZENE
1,2,».TRKHLOROPROPANE
12/4-THICHLOROBEN2ENE
U/4-TRIMeTHYLeENZENE
1.2-aiBROMO-3-CHLORaPROPAN
1,2-DieROMOETHANE
1,2.DtCHLOR0BENZENe
12-DICHLOROETHANE
12-OCHLOROPNOPANE
1 ^^TRIMETHYLBENZENE
1,3.DICHLjOROBENZENe
1,S-DICHLOROPHOPANE
1,4-OICHLOROBENZeNE
2,2-DICHLOROPROPANE
2-8UTAN0NE
J<!HLOROT0LUENE
2-HEXANONB
^CHLOROTOLUENE
4-)SOPfiOPYLTOLUENE
4*eTHYL-2-PEMTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOPORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROrORM
CHLOROMETHANE
CI5-12-OICHLOROETHENe
10061-01-6 CIS-l ^DICHLOROPROPENE
124-48.1
744S4
75-714
ioa-4m
87-684
88424
108484
7S-09-2
104414
103.65-1
91-204
05-474
19548.6
100-124
98454
127-18-4
108.884
195404
WBROMOCHLOROMETHANE
DIBROMOMETHANE
DlCHLORODtPLUOROMETHANE
ETHYLBENZENE
HEXACHLOROeUTAOIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYUENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC4UTYLBeNZENE
STYRENE
TCRT4UTYLBENZENE
TTTRACHLOROETHENE
TOLUENE
TRANS-U-nCHLOROeTHENE
10061424 -mAr4S-1,S4})CHL0R0PROPENE
7M14
764&4
7541.4
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
WNYLCHLORBE
Result
U
u u u
u u u u u
u u u u u u u u u u
u u
u u
u u
u u 2.7JB
u u u u u u u u u
u u u
u u u u u u
u u u u
u u
u u u u u
u u
u
u u
u
^HIMH
UnHs
"9/!>
"9/9
ugfg
US/8
U9/3
119/g
ug/g
ug/g
isn't*
vglkg
ug/l«B
ug/Kg
us/Kg
uglkg
uglkg
UQiTcg
UBAQ
ugn^
uglkg
U9/lq
uglkg
us/hs
ug/l«
uglkg
ugl^
uglkg
uglkg
uglkg
"tUfl
uglkg
ug/ks
ufl/kg
uglkg
ugne
u^ftg
uglkg
"oma
"9*9
uglkg
ug/kg
uglkg
U9rt«
ug4«
uglkg
uglkg
wglkg
uglkg
Ligncs
ug/kg
ug/ka
uglkg
uglkg
ug/kg
uglkg
uglkg
uglkg
uglkg
ug/kg
ugAg
uglkg
uglkg
uglkg
la/kg
ugAg
"9*9
ug/ks
U0*g
"9*9
U9*9
ugfltg
U9*9
uglkg
LablD;L102<M Collect Date; 06/123708:46 I
Det.
LMt
.001
3.3
M
.1
.3
1.B
3.S
.2
nep. DII
Umit FBI
.004 1
IS 1
.3 1
.6 1
1.6 1
8 1
19 1
M 1
LablD:Lin
Det
Umit
.2
2
3
2
.1
.8
2
2
2
2
2
1
2
,1
1
2
2
.Sl
2
.2
2
10
2
10-
.3
2
10
10
.2
2
A
.3
.1
,4
.,1
2
A
A
.6
.2
.2
.3
.2
.2
.3
2
2
.2
.3
.2
2
.2
.2
2
.2
2
,9
3
2
.2
.3
A
,4
Rep. DII
Umit Fe
10
10
10
10 1
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 •
10
10
10
10 '
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
aw Mattwd
fiW44S, 7471A
SW-846,6010
8W448,8010
SW446,6010
8W446,e010
SW-848,6010
8W44e,eoio
SW446.6010
SW-S46,80S0
Analyst
KEN
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
Test DM*
07/07/9710;15
08/20/8714:35
Oe/20/971439
06«af971495
06/20A714:35
08aO«7143S
0«20ffl714:35
Q6mi«71435
OS/18«7 00:00
4-21 Colled Date: 06/12/9708:46 1
t
rtor Mftfiod
8W-S46,82S0
CW44e,8200
SW-e46,8260
SW-846, 8360
8W446.a2e0
SW-848,8260
SW448,B2eO
8W-846,e280
6W44a,8260
6w-846.e2eo
sw.e46,a2eo
8W446,8260
SW-849,8280
8W446,82eO
SW-840,83S0
9W446,B2B0
SW-84e,82S0
fiW44S,82e0
SW-848,8260
«W.84e,8200
SW-84S,82eO
1 ew-846,62ao
8W446,6260
sw44a,e260
1 8W446,e260
1 8W-84e,8360
1 9W-84a,B380
1 8W-846,a280
1 8W44e,8260
1 SW-84a,82eD
1 8W446,82S0
1 ew-84e,82«0
1 sw-84e,82eo
1 5W-84S.82eo
1 SW-646,8200
1 8W-84S,8260
1 SW446,82e0
1 8W-846,<260
1 aW-646,B2eO
1 SW-848,8260
1 8W-S46,82ea
1 SW-84V,62eO
1 SW445,B2eD
1 8W446,82e0
1 6W-84e,8250
1 SW-S46,626a
1 SW44e,8260
1 8W448,8260
1 SW-848,6280
1 SW448,e260
1 sw-»4e,a26o
1 6W-648,8260
1 SW-846.6260
1 8W44e.62eo
1 8W44e,6260
1 SW-e46,8280
11 8W-«46,826D
1 &W-84e, 8260
•\ SW446,828D
1 SW44e.8260
1 8W-84S, 6260
1 SW-846,8280
\ 8W-64S,B2eO
Analyst
•MR
MMR
WInR
MWR
MMR
MMR
MMR
MMR
MiyR
MMR
MMR
NMU
MMR
MPnK
IWnK
MUR
PW»W
MMP
IVPRN
WlWrV
MMR
MVIR
RvVK
nWnR
MMR
RWnK
NInR
WWW
v/W^K
MMR
VntnR
MMR
MMR
Rffwcl
MMR
HWFIR
MMR
Mwn
MMR
NMX
Mffi
nwWK
MMR
iWWR
MMR
MMR
IVPnrf
MMR
MMR
nflMn
nWnR
My^%
RnMR
WWIR
MMR
ImflR
MMR
MMn
HWflN
MMR
MMK
MM^
Test Date
e«fl7/9719*9
06/17/97 16-.S9
08/17/971859
06/17/0716*9
0»17/9718:59
06/17/97 16:S9
08/17/0716:58
08^7/971659
08/17/9716£9
08/17/9716:59
06/17/97 16:99
06^7/9716:59
06/17/9716M
oan7/5716:99
08/17/9716:59
0»17/97 16:59
06/17/97 18:»
oen7/9718:58
06/17/97 ie«9
06/17S7 16:98
06/17/971S£9
06/17/971659
06/17/07 16:58
oen7/97ie£8
06/17/9716:58
06/17/97IB-W
06/17/9716£9
06/17/971659
08/17/3716dS
06/17/971S;S9
06/17/9716.99
06/17/871859
0eM7/871659
oamiai ie«9 00/17/97 ie:S9
06/17/07 1859
08fl7/971658
08/17/9716*9
08M7/97 16;SB
06/17/97 ie£9
06/17/971859
06^7/9718:59
06f17«f718S9
06/17/97 1859
06/17/971659
05/17/971659
08/17/9718.69
06/17/8719:99
0en7/971659
06/17/971659
OSmm 1659
0»17/97 1659
08/17/9716:59
OS/17/97 1659
08^7/97 1659
06rt7/97 1659
06/17/971659
08rt7/97 1659
06/17/9718:59
06/17/9716.-99
0an7/971859
Oert7/971859
oaniisi 1659
! 2of4
#
•
#
1 Sample ID
{sample 10
630-304
71-654
79-344
79404
76444
7545-4
563.954
87414
96-16-4
12042-1
95434
06-124
10&43-4
9540-1
107-(»3
78474
108474
541-73-1
142-284
106-48-7
59040-7
78-934
8S-494
Cai-784
iae-4s-«
89474
10B-10.1
67.64-1
71-43-2
108-86-1
74-974
75-274
7S.2S.3
74434
Se-234
10840-7
7S-00-3
67-664
74474
16649-4
: l2JUN-a, 1-10 S DRYWELL
MERCURY
ARSENIC
BARIUM
CADMIUM
CHROMIUM
LEAD
SELENIUM
SILVER
ICP/GPAA METALS 0IQE8TI0N
Result
.037
30
182
4,8
14
18
U
3
i: 12JUN-4,M0 S DRYWELL
Test Parameter
1,1.1,3-TETRACHUOROFrHANE
1,1,1-TRICHLOROeTHANE
1.1 ^,^TETRACHL0ROETHANE
1.1.2-TRICHLOROETHANE
1.1-OlCHLOROETHANE
1,1-DICHLOROeTHENE
l.l-WCHLOROPROPeNE
1,2>TRICHLOR0BENZENE
1Z4-TRICHLOR0BENZENE
1,2.4-TRMeTHYLBENZENe
1 .g OIHROMO 3JJ-ILOftQPBOPAM 1 )fc^»*lHI^%»BW*^^^^^T»^»*F^^^ IW« ^'"
U-DIBRQMOETHANE
U-OICHLOROBENZENE
1,2-OICHLOROETHANE
1,2.0ICHLOR0PR0PANE
1 ^.e-TRIMETHYLBENZENB
1>0ICHL0R0BENZENE
I^DKHLOROPROPANE
1/4-OICHLOROBENZENE
2,3-OICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-eKLOROTOLUENE
44SOPROPYLTOLUeNE
4-METHYL.2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMOOICHLOROMETHANE
6ROMOPORM
BROMOMETHANE
CARBON TETKACn.ORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1 .Z-OtCHLOROETHENE
10061-014 CIS-1 ,>-OK:HL0RaPROPENE
124-48-1
74-854
78-714
10041-4
87484
98-82-6
108484
7549-2
104414
10345-1
91-204
95-474
135484
100-424
96464
127-18-1
1084V3
156404
OIBROMOCHLORODCTNANE
DIBROMOMETHANE
nCHLOROOIPLUOROMETHANE
BTHYLBENZENE
HEXACHLOROeUTAOIENE
ISOPROPYLBENZENE
M,P-XYIENE
METHYLENE CHLORIDE
N-BUrflfiENZENE
N4»R0PYLBENZENE
NAPHTHALENE
OOCYLENE
SEC-BUTYLBENZENE
STYRENE
TERT4UTYLBEN2ENE
TETRACHLOROETHENE
TOLUENE
TRANS-1 j-0)CHLOROETHENE
10061-024 TRANS-IAOttHLOROPROPENE
78414
7649-4
7941-4
TRICHLOROETHENE
TRJCHLOROFLUOROMETHANE
VINYLCHLORIDE
Result
u
u u u u u
u u
u u u
u
u u u u u u u u
u u u u u u u
u u u
u u u u
u u u u u u u
u u
u
u u
u u u u
u u
u u u u u u u u
u u
u
Mpits
U9/S
"9/9
uglg
uglg
ug/fl
ug/S
Ug/S
uglg
UnHs
ug/ks
ug/kg
"9^8
ug/iq
U9*g
ugAig
ug/kg
Ufl/kg
ug/ltg
us*g
uglkg
ugl*g
ug/kg
uglkg
"9*9
uglkg
Ufl/kg
ug/hg
"g/hg
uglkg
U9*S
"9/l«9
ug/kg
Ufl/kg
ugAg
ug/kg
uo*a
"9*9
ug/kg
Ufl/kg
u9«e
ug/kg
uglka
ii»ks
uglkg
itg/kg
ug/kg
tt9*8
ug/kg
ug/kg
ugAig
ugAg
ug/kg
"9*9
uglkg
U0*a
uglkg
us/ks
"9*9
uglkg
US/kg
"9*8
ug4Q
ug/kg
ug/kg
uglkg
uglkg
U0*9
U9*9
ugfl^
u9*g
uglkg
uglkg
Lab ID: Ll 024-3 Collect Date: 08/12ffl7 06:45 j
Det
Umit
.002
3,1
M
.1
A
1.6
3.7
2
IRep. Dil •
Limit Faelpr Mrth«»<
.005
IS
3
.6
1.6
7.7
18
.9
1 SW446,7471A
1 9W-84e,6010
1 SW448.e010
1 8W446,6010
1 8W-846,6010
1 8W446,801D
1 9W-84e,6010
1 SW-848.6010
1 SW-846,3060
Analyst
KEN
KWB
KWB
KWB
KWB
MNB
KWB
KWB
KWB
Tertpale
07/07/0710:19
06/20/971450
06/20^71450
08COW71450
osnoigj 14.50
0800/97 14.50
0600/971450
0600071450
06/18*7 00.00
UblD:L102'M Collect Date: 06/12/97 08:46 1
Det
Umit
.3
.2
.3
.2
.1
.6
.2
,2
3
,2
.2
.2
2
.1
2
.2
2
2
2
2
2
10
2
10
.2
.2
10
10
2
2
2
.3
.1
.d
.3
.2
,4
A
£
2
2
3
2
,2
.3
.2
.2
2
3
2
2
.2
,2
.2
.2
2
,9
.9
.2
2
.3
.3
A
Rep. Dl
Limit Fa
10
10
10
10
10
10
10
10
10
10
10
Ifl
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ID
10
10
10
10
10
10
10
10
10
10
10
10
.
ctot. Method
1 6W446,8280
1 9W446,8260
1 sw-64s,e2eo
1 SW.846,8260
1 8W-846,e260
1 SW-B4e, 8260
1 SW44e,B260
1 SW-846,8260
1. SW.B4e,B260
1 SW-846,8280
1 SW-84e,8260
1 SW-846,e260
1 SW446.82eO
t SW-646,8260
1 8W-S48,8260
1 8W448,8260
1 SW-S4e,826D
1 SW446,B2eO
1 SW446,82eO
1 SW-846,8260
1 8W44e, 8260
1 sw-a48,B2eo
1 SW-846,8260
1 8W-846,8260
1 SW446,e2e0
1 8W-846,8260
1 8W-846,8260
1 SW-84a,B260
1 SW-848,8280
1 SW-846, B260
1 SW44«,82eO
1 aW-S4«,8260
1 fiW-846,82eo
1 SW-A46,8260
1 SW-84e, B260
1 SW44e,82eo
1 9W-84e.8260
1 8W-846.B2eo
1 8W-B4e.6260
1 SW446,82eO
1 SW-84e. 8260
1 SW446,8280
1 8W448.neO
1 SW446,8260
1 8W-846,8260
1 SW-84e,8260
1 8W446,e2e0
1 8W-84e, 8260
1 SW.84S,82«0
1 SW-S46.8280
1 SW446.8260
1 SW-84e,8260
1 8W-84e,8260
1 SW-846. B260
1 8W446,8260
1 SW-846,8260
1 6W.846.82S0
1 8W.84e,8260
1 SW.848.8260
1 SW.848.8260
ll 8W-84e, 8260
'1 SW448,B2eO
1 SW-848,8260
frnly«t
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
WMR
nWnR
MMR
TWBR
MMR
MUft
wlViK
Mmnn
MMR
MMR
MMR
MMR
MRtt%
WIVIK
BwVW
MMR
MMR
MMR
r/9n%
MMR
rRMR
WPffX
MMR
IMMR
MMR
Mem
BWTR
RnMR
MMR
MMR
MMR
mm
MMR
WW\
n^W
RWnR
MWl
WwnR
MMR
^/^iw%
MMR
MMR
MMR
RwMR
MMR
MMR
IffnR
wlMR
RwnR
MMR
WPnR
MMR
MMR
MM^
Test Date
08/17/97 17:33
06/17/97 1733
06/17/97 17:33
06/17/9717:33
06^7/971733
06/17/97 1733
06/17/971733
06^7/971733
0«tt7/S7 I7fl3
06/17/97 1733
06n 7/9717:33
06rtT/9717:33
06/17/97 17.33
06/17/971733
06/17/971733
06/17/97 1733
06/17/97 17.33
06/17/97 1733
061^7/971733
06/17/971733
oan 7/971733
oen7/97i7a3
08rt7/9717'33
06^7/871733
06/17/971733
06/17/87 17:38
oamiai 1733
06/17/97 1733
06/17/97 1733
OSn 7^71733
06/17/971733
06/17/871733
08^7/9717:33
06/17/871733
08/17/87 17.-33
06/17/871733
08rt7/9717:39
OenT/87 1733
08/17/971733
06n7/971733
06/17/87 17:33
Oan7/87 1733
06/17/971735
06/17/971733
06^7/971733
06^7/9717:83
08/l7A97ir33
06/17/971738
0e/17«7 1733
06/17/19717.33
06/17/97 1733
08/17/9717:33
06/17/97 17.33
06/17/9717:33
06n7/971733
06/17/97 17:33
08^7/97 17:33
06/17/97 1733
0e«7/871733
08/17(97 1733
oemigr 1733
06fl7/9T 17:33
06/17/9717:33
— -> -J >
Data Reporting Qualifieirs
u indicates compound was analyzed for and was not detected, or the compound was detected but v/as
below the detection limit.
B Gas Chromatography and Mass Spectral Data Flag. This flag is usee! when an analyte Is found in
the blank as well as the sample
J Gas Chromatography and Mass Spectral Oata Rag. Indicates an eslimated value. This flag Is used
either when estimating a concentration for tentatively identified compounds or when the data
indicated the presence of a compound that meets the Identification criteria but the result is less than
the specified reporting limit (e.g, 3 J with a reporting limit of 10)
Oet. Umtt Method Detection Limit (approximately three times the signal noise level)
Rep. Limit Reporting Limit Is nonnnally the value ofthe loi/vest standard mn with the analysis. The value
is approximately 5 to 10 times the Method Detection Umit
Dil. Factor Dilution Factor - The prepared sample v/as diluted by this factor because the sample was
too concentrated or due to other interferences in the sample matrix. Any dilution factor
causes an appropriate Increase in the method detection limit and reporting limit
ENVIRONMENTAL LAB WORK REQtrEST Lfp'?^
iP= THIOKOL ENVIRONMENTAL LABORATORY LWR No. El 1430
Login No.
/4P (jU/ViXeg^ S270
COST CENTER -g -TUf WORKORDER
/SJ(LI 'ir ORGANIZATION
^yiro/^/Mnfay "^74
REPORT RESULTS TO:
HELEN WARD, MS 301
i
SAMPLE
^-/^-/SJu/f
0
1 f 10.
"
12.
DATE
/rJu{^
0
TYPE
G
\y
C
SAMPLE INFORMATION
LOCATION TIME
J.-ZO'^dr^L/Clf
ll
TEST
J^CJZA Mihds.
REMARKS
CHAIN OF CUSTODY
RELINQUISHED BV
<^B^/Ji(M^
DATE
7-/<r^9-y
TIME
//^r
RECEIVEiD IIY
/., -a 71
DATE
\a^ "7*
^-/r- 9-y
TIME
/drr
FOR LABORATORY USE ONLY
#
DATE COMPLETED DATE REPORTED SIGNATURE
CERTIFICATE OF ANALYSIS
Usting of sample Infomiation and Testing Dlequested
Thursdsy, July 31,1997
TESTED FOR Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp, UT 84322
Frank Waiker
Project: SoHd Waste Mgmt Invest
Login Number L1075
Lab No Client Number
Test Requested
I Ll 075-1
Description
.\NALYZEB MY Thiokoi Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-3732
800-863-8080
Received CollectDate/Time
Matrix
t-10-15 JULY 1-10 DRYWELL 07/15/97 07/15/9713:00
SW-846.7471A
SW-846, 6010
SW-846. 6010
SW-846. 6010
SW-846. 6010
SW-846. 6010
SW-846, 6010
SW-846. 6010
SW-846. 6010
SW-846. 3050
CV Mercury Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
As ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA,)
Se ICP Metals Analysis (RCRA>)
Pb ICP Metals Analysis (RCRA)
Cr ICP Metals Analyais (RCRA)
Ba ICP Metals Analyais (RCRA)
ICP/GFAA Metals Digestion
Sou
Soil
Soil
Soil
Soil
Soil
Sou
Soil
Soil
Soil
tified By ^^d^sU^U^- /^2!JLA'^^:^ r/F/97
pSaxnps M. Anderson, QC Officer Date
Certified
This certifies that the following samples were analyzed using good laboratory practices to show the following results:
Page 1 of 3
Usting of Results by Sample
\^^ ID: 1-10-15 JULY HO DRYWELL Lob ID: Ll 075-1 Collect Date: 07/15/9713.-00n
Test Parameter
MERCURY
^^XMMNxMM
ARSENK:
BARHJM
CHROMIUM
LEAD
SELENIUM
StVER
ICP/GFAA METALS DIGESTION
fififlilt
.024
6460
U
107
U
11
U
U
U
IMf
uglg
uglg
"o/g
"D'O
uglg
uglg
uglg
ug/g
uglg
Det
Lknit
.009
1.4
23
.(«
.1
3
1.4
33
2
Rep.
Limit
.03
6S
14
3
.6
1.4
6.9
17
.8
Dil.
Factor Mtthfid
SW-846.7471A
SW-846.6010
SW-846.6010
SW-846.6010
SW-846,6010
SW-846,6010
SW-846.6010
SW-846.6010
SW-846.6010
SW446.3050
Afialvrt
KEN
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
TCftDiltfi
mi2Am 10.41
07/25*712:15
07/25«712:15
07/25*7 12:15
07/25*712:15
07/25*7 12:15
07/25*7 12:15
07/25*7 12:15
07/25*7 12:15
07/23*711*0
0
#
Page 2of3
#
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the icompound was detected but was
below the detection limit.
B Gas Chromatography and Mass Spectral Data Rag. ITiis flag is used when an analyte is found in
the blank as well as the sample
J Gas Chromatography and Mass Spectral Data Rag. Indicates an estimated value. This flag is used
either when estimating a concentration for tentatively identified compounds or when the data
indicated the presence of a compound that meets the identification criteria but the result is less than
the specified reporting limit (e.g. 3 J with a reporting limit of 10)
Det. Limit Method Detection Limit (approximately three times the signal noise leveO
Rep. Umit Reporting Umit is noimally the value ofthe lowest standard run with the analysis. The value
is approximately 5 to 10 times the Method Detection Umit
Dil. Factor Dilution Factor - The prepared sample was diluted by this factor because the sample was
too concentrated or due to other interferences in the sample matrix. Any dilution factor
causes an appropriate increase in the method detection limit and reporting limit
Page 3 of 3
ENVIRONMENTAL LAU WORK REQUEST
iro. THIOKOL ENVIRONMENTAL LABORATORV
FROM: .
ff UJa}^
ORGANIZATION
fnu
t.\-: .;N>iioN
M.VII.STOP
30/^
LWR No.
Login No.
COST CENTER WORKORDER
/E940
E11358
DATE
3>/f 7
REPORT RESULTS TO:
H ELEN WARD, MS 301
i
SAMPLE
1 SUJUO (flSS-
2 svjL\u («s-<r
-=;.+, tl7_ <;o2.
5.
6.
7.
1"
1.
10.
11
li
DATE
Vio/'ry
n
li
11
TYPE
G
)/
y
y
i/
c
SAMPLE INFORMATION
LOCATION
/W'fO
AX'lo
M'4o
AA-^0
TI.ME
l^yo
i^-ii
I'l^^r
/H'd
TEST
A^:^^xdXr,Ph,H^,%
/'
n
ll
REMARKS
--^,A^..Mc^
CHAIN OF CUSTODY
RELINQUISHED BY
^ iM/i.-
DATE
^liih 7
/
TIME
/ln(}
RECEIVED BY
KAU rf!liilli.L.<XJV
-~t
DATE
^li'ln
1
TIME
dre
«
DATE COMPLETED
FOR LABORy«LTORV USE ONLY
DATE REPORTED SIGNATURE
CERTIFICATE OF ANALYSIS
Listing of sample Information and Testing Requested
#
Friday, April 4, 1997
TESTED FOR Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp, UT 84322
Frank Walker
Project: Solid Waste Mgmt Invest.
Login Number L861
Lab No Client Number
Test Requested Description
ANAJLYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-3732
800-863-8080
Received CollectDate/Time
Matrix
L861-1 SWMU 655. SITE #1 SUR
SW-846, 7471A
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
CV Mercury Analysis (RCRA)
Ag ICP Metals Anatysis (RCRA)
As ICP Metals Anatysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Mg ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
L861-2 SWMU 655, SITE #1 2
SW-846, 7471A
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
CV Mercury Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Ba ICP Metals Anatysis (RCI^)
Mg ICP Metals Analysis (RCRA)
Se ICP Metals Analysis (RCRA)
Pb ICP Metals Anatysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
As ICP Metals Analysis (RCRA)
ICP/GF/VA Metals Digestion
L861-3 SWMU 655. SITE #2SUR
SW-846, 7471A
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
CV Mercury Analysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Mg ICP Metals Analysis (RCRA)
Se ICP Metals Anatysis (RCRA)
Pb ICP Metals Anatysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
As ICP Metals Anatysis (RCRA)
Ba ICP Metals Analysis (RCRA)
ICP/GFAA Metals Digestion
L861-4 SWMU 655, SITE #2 2
^
SW-846, 7471A
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
CV Mercury Anatysis (RCRA)
Ag ICP Metals Analysis (RCRA)
Se ICP Metals Anatysis (RCRA)
Pb ICP Metals Analysis (RCRA)
As ICP Metals Anatysis (RCR/\)
Ba ICP Metals Anatysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Mg ICP Metals Anatysis (RCRA)
Cd ICP Metals Analysis (RCRA)
ICP/GF/^A Metals Digestion
03/11/97 03/10/9714:30
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
03/11/97 03/10/9714:37
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
03/11/97 03/10/97 14:35
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
03/11/97 03/10/97 14:45
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Page 1 of 4
// Ceitified By Date
This certifies that the foiiowing samples were analyzed using good laborator,/ practices to show the following results:
m
•
Page 2 of 4
Listing of Results by Sample
[SamplelD: SWMU 655, SITE#1 SUR LablD:L861-1 Collect Date: 03/10/9714:30
#
Test Parameter
MERCURY
ARSENIC
BARIUM
CADMIUM
CHROMIUM
LEAD
MAGNESIUM
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
Result
u
u
88
1.1
14
3
105000
u 2.5
Units
"9/g
"9/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Det.
Umit
.01
3.1
.06
.1
.3
1.6
3
3.7
.2
Rep.
Umit
.04
16
.3
.6
1.6
7.8
15
19
.9
DII.
Factor
50
Method
SW-846, 7471A
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-a46,6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
Analvst
KEN
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
Test Date
03/19/9711:06
03/24/97 13:47
03/24/97 13:47
03/24/97 13:47
03/24/97 13:47
03«4/97 13:47
03«7/97 12:06
03/24/97 13:47
03/24/97 13:47
03/19/97 00:00
[Sample ID: SWMU 655, SITE #1 2 LablD:L861-2 Collect Date: 03/10/97 14:37
Test Parameter
MERCURY
ARSENIC
BARIUM
CADMIUM
CHROMIUM
LEAD
MAGNESIUM
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
Result
.03
U
106
U
18
U
11900
U
U
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Limit
.01
3
.06
.1
.3
1.5
3
3.6
.2
Umit
.03
15
.3
.6
1.5
7.5
15
18
.9
Factor
50
Method
SW-846, 7471A
SW-S46, 6010
SW-846, 6010
SW-846, 6010
SW446, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
Analvst
KEN
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
Test Date
03/19/9711:19
03/24/97 14:02
03/24/97 14:02
03/24*7 14:02
03/24/97 14:02
03/24/97 14:02
03/27*7 12:09
03«4/97 14:02
03«4/97 14:02
03/19/97 00:00
I Sample ID: SWMU 655, SITE #2SUR LablD:L&61-3 Collect Date: 03/10/97 14:35
•
Test Parameter
MERCURY
ARSENIC
BARIUM
CADMIUM
CHROMIUM
LEAD
MAGNESIUM
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
Result
.01
u
85
1.1
19
u
47600
U
.4
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Limit
.01
3
.06
.1
.3
1.5
3
3.6
2
Limit
.02
15
.3
.6
1.5
7.5
15
18
.9
Factor
5Ci
Method
SW-846, 7471A
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 3050
Analyst
KEN
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
Test Date
03/19/9711:22
03/24/97 14:05
03«4/97 14.05
03«4*7 14:05
03«4*7 14:05
03«4/97 14:05
03/27/97 12:12
03/24/97 14:05
03/24/97 14:05
03/19/97 00:00
I Sample ID: SWMU 655, SITE #2 2 LablD:L8614 Collect Date: 03/10/9714:45
Test Parameter
MERCURY
ARSENIC
BARIUM
CADMIUM
CHROMIUM
LEAD
MAGNESIUM
SELENIUM
SILVER
ICP/GFAA METALS DIGESTION
Result
.02
U
143
U
21
U
10500
U
.5
Units
ug/g
ug/g
ug/B
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Limit
.01
3.1
oe;
.1
.3
1.6
3.1
3.8
.2
Limit
.04
16
.3
.6
1.6
7.9
16
19
.9
Factoi
60
r Method
SW-846, 7471A
SW-846,6010
SW-S46, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846,6010
SW-846, 6010
SW-846, 3050
Analvst
KEN
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
Test Date
03/19*711:26
03/24*7 14:08
03«4/97 14:08
03/24«7 14:08
03/24/97 14:08
03/24/9714:08
03/27/97 12:15
03/24/97 14:08
03/24/97 14:08
03/19/97 00:00
Page 3 of 4
#
#
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected but was
below the detection limit.
B Gas Chromatography and Mass Spectral Data Flag. This flag is used when an anaiyte is found in
the blank as well as the sample
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This flag is used
either when estimating a concentration for tentatively identified compounds or when the data
indicated the presence of a compound that meets the identification criteria but the result is less than
the specified reporting limit (e.g. 3 J with a reporting limit of 10)
Det. Limit Method Detection Limit (approximately three times the sicinal noise level)
Rep. Limit Reporting Limit is normally the value ofthe lowest standard run with the analysis. The value
is approximately 5 to 10 times the Method Detection Limit
Dil. Factor Dilution Factor - The prepared sample was diluted by this factor because the sample was
too concentrated or due to other interferences in the sample matrix. Any dilution factor
causes an appropriate increase in the method detection limit and reporting limit
Page 4 of 4