DSHW-1997-001304 - 0901a0688013a82e

DEFENSE AND LAUNCH VEHICLES DIVISION
P.O. BOX 689
BRIGHAM CITY, UT 84302.0689
80l-863-35n
SPACE-DEFENSE-FASTENING SYSTEMS
^^1^
^/S 2 7 1997
.... w/• OdS'(^'=;
Division of Solidi Hazardous Waste
t-tati Department of Environmental Quality
THIOKOL CORPORATION
SEMI-ANNUAL RFI PROGRESS REPORT
1 September 1996 -1 March 1997
«
DEFENSE AND LAUNCH VEHICLES DIVISION WWtf^^JtfSfSl^
P.O. BOX 689
BRIGHAM CITY, UT 84302-0689 AEROSPACE & INDUSTRIAl TECHNOIOGIES
801-863-3511
20 February 1997
W300-FY97-ST037
Dennis R. Downs, Executive Secretary
Utah Solid and Hazardous Waste Control Board
288 North 1460 West
PO Box 144880
Salt Lake City, Utah 84114-4880
Dear Mr. Downs:
ATTENTION: Jeff Vandell
SUBJECT: Semi-Annual RFI Progress Report
As required by Section VII.H of Thiokol Corporation's Post Closure Permit, the
following semi-annual RFI progress report is submitted for your review. The
reporting period covered by this report Is 1 September 1996 -1 March 1997.
Notification of three newly identified SWMUs Is included along with laboratory data
and/or Solid Waste Management Unit Assessment Plans for the respective units.
If you have any questions in this matter, please contact me at [phone], or
Frank Walker at [phone].
Sincerely,
J. R. Whimpey, Manager
Environmental Services
JRW/afw
c: Don Ostler, Director, Division of Water Quality
Notification of Newly-Identified Solid Waste Management Units
As required by section VII.E. of Module Vll ofthe Post-Closure Permit issued to
Thiokol Corporation by the Utah Solid and Hazardous Waste Control Board, Thiokol
Corporation hereby serves notice ofthe identification of three additional Solid
Waste Management Units for inclusion on the list of SWMUs.
The newly-identified units are as follows:
SWMU #665, Subsurface Wastewater Discharge from Building M-53;
SWMU #666, Drywell at Building M-56;
SWMU #667, Septic Drainfield for Building 1-5
DESCRIPTION OF NEW UNITS
SWMU #665, Subsurface Wastewater Discharge from Building
M-53;
During site excavation for an addition to building M-53, a buried drain line was
discovered which appeared to discharge to the subsurface. The line was traced to
a floor drain inside M-53. The drain also collects run-off water from roof drains atop
M-53. A Solid Waste Management Unit Assessment Plan and a proposal to cap
the residual contamination at the site with a concrete pad is included.
SWMU #666, Drywell at Building M-56-,
A shallow drywell was discovered on the south side of building M-56. The drywell
historically has collected wastewater from building floor drains. The building is used
for propellant development, mix, and weigh-up. Samples were collect upon
discovery to characterize the site. This site was inadvertently omitted from the
previous notification of new SWMUs. Laboratory data collected to date from this
site is included and will be evaluated in the RFI process to determine the need for
further action.
SWMU #667, Septic Drainfield for Building 1-5
Building 1-5 is an Ordnance Development facility located in the Manufacturing Area.
The facility septic tank and drainfield was identified as having received industrial
wastewater. The septic tank contents have been removed and the tank cleaned
and filled. An investigation plan to evaluate any contamination to the drainfield has
been prepared and is attached.
ENVIRONMENTAL LAB WORK REQUEST
L
P^" THIOKOL ENVIRONMENTAL LABORATORV LWR No. EI1227
Login No.
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REPORT RESULTS TO:
HELEN WARD. VIS 301
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REMARKS
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FOR LABORATORV USE ONLV i DATF. (OMI'I.ETEI) DATE REPORTED
•
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Requested
Tuesday, July 30, 1996
TESTED FOR Ttiiokol: DLV
Environmental Monitoring
Helen Ward M/S 301
Thiokol Corp.UT 84322
Frank Walker
Project: Solid Waste Mgmt Invest.
Login Number L408
Lab Number Client Number
Test Requested Description
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
• EJrigham City, UT 84302-0707
801-863-5445
800-863-8080
L408-1 M-56 DRYWELL SURFACE
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846. 6010 Ag ICP Metals Analysis (RCRA)
SW-846, 6010 Al ICP Metals Analysis (RCRA)
SW-846,6010 Ba ICP Metals Analysis (RCRA)
SW-846, 6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846. 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846. 7740 GFAA Selenium Analysis (RCRA)
SW-846. 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846, 6010 Al ICP Metals Analysis (RCRA)
SW-846,6010 Ba ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846, 6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7740 GFAA Selenium Analysis (RCRA)
SOP 302
SOP 420
SOP 420
Perchlorate - lon Chromatography
HPLC Analysis HMX and RDX
HPLC Analysis for NG
Received
Matrix
Collect Date/Time
06/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soii
Soil
Soil
Soil
Soil
Soil
Soil
Soii
Soil
Soil
Soil
Soil
Soil
06/16/96 14:05
L408-2
SW-846.
L408-3
SOP 302
SOP 420
SOP 420
L408-4
M-56 DRYWELL SURFACE
3260 Volatile Organics
M-56 DRYWELL SURFACE
Perchlorate - lon Chromatography
HPLC Analysis HMX and RDX
HPLC Analysis for NG
M-56 DRYX/VELL 2 FT.
06/19/96
Soil
06/19/96
Soil
Soil
Soil
06/19/96
06/16/96 14:05
06/16/96 14:05
06/16/96 14:10
L408-5 M-56 DRYWELL 2 FT.
SW-846, 8260 Volatile Organics
L408-6 M-56 DRYWELL 2 FT.
06/19/96
Soil
06/19/96
06/16/96 14:10
06/16/96 14:10
Page 1 of 6
Work Order Comments
Lead results for L408-1 show evidence of nonhomogeneity. The actual concentration for lead
^^ may be twice the reported concentration.
y Certified By Date
This is to certify that the following samples were analyzed using good laboratory' practices to shotv
the folowing results:
o
Page 2 of 6
Listing of Results by Sample
a
1 Sample
1 Sample
CAS
Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
ID: M-56 DRYWELL SURFACE
Test Parameter
ICP/GFAA METALS DIGESTION
ALUMINUM
BARIUM
CADMIUM
CHROMIUM
LEAD
SILVER
ARSENIC
MERCURY
SELENIUM
ID: M-56 DRYWELL SURFACE
Test Parameter
1,1,1.2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBEN2ENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
Result
8880
73.8
1.32
19.7
36.3
U
7.4
0.03
U
Result
u
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Units
ug/kg
3.9 JB ug/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Det.
Limit
1.6
0.06
0.13
0.32
1.6
0.19
0.9
0.01
1.3
Det.
Limit
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
Lab ID: L40£;-1 Collect Date:
Rep. Dil.
Limit Factor Method
7.99
0.32
0.64
1.6
7.99
0.96
2.6
0.03
4.4
SW-846, 3050
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846.6010
1 SW-846,6010
1 SW-846, 7060
1 SW-846, 7471A
1 SW-846, 7740
06/16/96 14:05
Analvst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
CRS
CRS
Lab ID: L408-2 Collect Date:
Rep. Dil.
Limit Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 '
10
10
10
10
10
10 1
10 1
10
10 1
10 1
10 1
10 1
10 1
10 1
1 SW-846,8260
1 SW-846,8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
06/25/96 13
06/28/96 11
06/28/96 11
06/28/96 11
06/28/96 11
06/28/96 11
06/28/96 11
07/23/96 19
07/25/96 09
07/23/96 15
00
10
10
10
10
10
10
39
59
13
06/16/96 14:05
Analyst Test Date
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
_ MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
06/25/96 12:13
06/25/95 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12;13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25,'96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/95 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
05/25/96 12:13
05/25/96 12:13
Page 3 of 6
o
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
U
U
U
U
U
U
u
u
u
u
0.74 J
U
U
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
06/25/96 12:13
[sample ID: M-56 DRYWELL SURFACE Lab ID: L40a-3 Collect Date: 06/16/96 14:05
Det.
1 Sample
1 Sample
CAS
Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
Test Parameter
PERCHLORATE
HMX
NG
ID: M-56 DRYWELL 2 FT.
Test Parameter
ICP/GFAA METALS DIGESTION
ALUMINUM
BARIUM
CADMIUM
CHROMIUM
LEAD
SILVER
ARSENIC
MERCURY
SELENIUM
ID: M-56 DRYWELL 2 FT.
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2.3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4.TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOR08ENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
Result
u
6.8
U
Result
10500
53.4
14.4
1090
837
U
9.7
1.7
1.2
Result
u
970
U
5.4 J
1.8 J
1.2 J
U
U
U
U
U
U
U
U
0.59 J
U
U
U
u
u
u
u
u
u
u
u
u
u
0.56 J
U
U
U
Units
ug'g
ug/g
ug/g
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Limit
2.9
0.5
0.5
Det.
Limit
1.46
0.06
0.12
0.29
1.46
0.18
0.8
0.01
1.2
Det.
Limit
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
Limit
15
1.5
1.5
Lab ID:
Rep.
Limit
7.29
0.29
0.58
1.46
7.29
0.88
2.3
0.03
4
Lab ID:
Rep.
Limit
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Factor Method
1
1
1
SOP 302
SOP 420
SOP 420
Analyst Test Date
KEN
KMS
KMS
L408-4 Collect Date:
Dil.
Factor Method
1
1
1
1
1
1
1
1
1
SW-846, 3050
SW-846,6010
SW-846. 6010
SW-846,6010
SW-846,6010
SW-846. 6010
SW-846. 6010
SW-846, 7060
SW-846. 7471A
SW-846, 7740
07/22/96 12:12
06/25/96 16:00
06/25/96 15:00
36/16/96 14:10
Analvst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
CRS
CRS
L40&-5 Collect Date:
Dil.
Factor Method
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
05/25/96 13.00
06/28/96 11:25
06/28/96 11:25
06/28/96 11:25
06/28/96 11:25
06/28/96 11:25
05/28/96 11:25
07/23/96 20:06
07/25/96 10:03
07/23/96 15:31
36/16/96 14:10
Analyst Test Date
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12.50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
Page 4 of 6
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1.3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: M-56 DRYWELL 2 FT.
Test Parameter
PERCHLORATE
HMX
NG
U
U
U
U
u
6.4 J
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
0.77 J
U
u
89
u
u
Result
'9
1.7
U
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
3
0.5
0.5
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
15
1.5
1.5
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
06/25/96 12:50
L40i3-6 Collect Date: 06/16/96 14:10
Dil.
Factor Method
1
1
1
SOP 302
SOP 420
SOP 420
Analyst
KEN
KMS
KMS
Test Date
07/22/96 12:21
06/25/96 16:00
06/25/96 15:00
•
Page 5 of 6
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected
but was below the detection limit.
B This flag is used when ah analyte is found in the blank as well as the sample
Det. Limit Method Detection Limit (approximately three times the signal noise level)
Rep. Limit Reporting Limit is normally the value of the lowest standard run with the
analysis. The value is approximately 5 to 10 times the Method Detection Limit.
Dil. Factor Dilution Factor - The prepared sample was diluted by this factor because the
sample was too concentrated or due to other interferences in the sample matrix.
Any dilution factor causes an appropriate increase in the method detection limit
and reporting limit.
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This
flag is used either when estimating a concentration for tentatively identified compounds or
when the data indicated the presence of a compound that meets the identification criteria
but the result is less than the specified reporting limit (e.g. 3 J with a reporting iimit of 10)
Page 6 of 6
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Requested
Tuesday, August 27,1996
TESTED FOR Thiokol: DLV
Environmental Monitoring
Helen Ward M/S 301
Thiokol Corp,UT 84322
Frank Walker
Project: Solid Waste Mgmt Invest.
Login Number L478
Lab Number Client Number
Test Requested Description
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
F'.O. Box 707 M/S 245
EJrigham City, UT 84302-0707
801-863-5445
800-863-8080
IReceived
Matrix
Collect Date/Time
L478-1 M-56 DRYWELL 2 FT. 08/05/96 06/16/96 14:10
SW-846, 1311
SW-846, 3010
SW-846, 6010
SW-846,6010
SW-846,6010
SW-846, 7470A
TCLP Extraction
ICP Metals Digestion
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Soil
TCLP Extr
TCLP Extr
TCLP Extr
TCLP Extr
TCLP Extr
Work Order Comments
This sample was originally submitted on work order L408 (L408-4). A request was made to add
TCLP analysis on 1 Aug. 1996 by Frank Walker.
/I
/^^ Certified By Date Certified By
This is to certify that the following samples were analyzed using good laboratory practices to show
the folowing results:
o
Page 1 of 3
Listing of Results by Sample
Sample ID: M-56 DRYWELL 2 FT. Lab ID: L478-1 Collect Date: 06/16/96 14:10
suit
67
12
136
Units
ug/l
ug/l
ug/l
Det.
Limit
2
5
25
Rep.
Limit
10
25
125
Dil.
Fact:
1
1
1
or Method
SW-846, 1311
SW-846, 3010
SW-846,6010
SW-846, 6010
SW-846, 6010
Analyst
KWB
KWB
KWB
KWB
KWB
Test Date
08/15/96 14:00
08/20/96 13:30
08/21/96 13:38
08/21/96 13:38
08/21/96 13:38
Test Parameter
TCLP EXTRACTION
ICP METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
MERCURY U ug/l 0.2 0.5 1 SW-846, 7470A KEN 08/15/96 10:57
Page 2 of 3
Data Reporting Qualifiers
U indicates compound was analyzed for and was not detected, or the compound was detected
but was below the detection limit.
B This flag is used when an analyte is found in the blank as well as the sample
Det. Limit Method Detection Limit (approximately three times the signal noise level)
Rep. Limit Reporting Limit is normally the value of the lowest standard run with the
analysis. The value is approximately 5 to 10 times the Method Detection Limit.
Dil. Factor Dilution Factor - The prepared sample was diluted by this factor because the
sample was too concentrated or due to other interferences in the sample matrix.
Any dilution factor causes an appropriate increase in the method detection limit
and reporting limit.
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This
flag is used either when estimating a concentration for tentatively identified compounds or
when the data indicated the presence of a compound that meets the identification criteria
but the result is less than the specified reporting limit (e.g. 3 J with a reporting limit of 10)
Page 3 of 3
#
o
PROPOSAL FOR SWMU #665 AT BUILDING M-53
CURRENT CONDITIONS
During site excavation for an addition to building M-53, a buried drain line was
intercepted which appeared to discharge to the subsurface. The line was traced to
a floor drain inside M-53. The drain also collects run-off water from roof drains atop
M-53.
PAST AND PRESENT OPERATIONS
Building M-53 is located in the Manufacturing Area at Thiokol's Promontory Facility.
The building was constructed in the early 60's as a Propellant and Material
Development Laboratory. The portion ofthe building associated with the newly
discovered discharge has been a metallography lab for studying the structure and
properties of metals. The area is currently used for heat treating metal and also
houses some machine shop operations.
SITE CHARACTERIZATION
Soil samples were collected on 11 November 1997 to characterize the newly
identified site. A sample was collected from surface soil at the assumed point of
discharge. A two foot depth sample was also collected from the same point. Two
additional samples were collected 25 feet down gradient at the same depths. The
samples were taken to Thiokol's Environmental Laborator/ for metals, volatile
organics and semi-volatile organic analysis.
The laboratory results indicate that metals concentrations are generally within
background ranges for soils at Thiokol's facility. Some volatile organic analytes
were detected but qualified by the laboratory that the reported value was an
estimated value and less that the specified reporting limit (PQL). Some analytes
were also qualified as found in the laboratory blank. In all cases, concentrations
found in the blank were also less than the specified reporting limit. Two of the
samples had phthlate esters present. EPA considers phthlate esters to be common
laboratory contaminants\ No other semi-volatile organics were reported as
detected. The laboratory did report the presence of "peaks" on the chromatograms
indicating the presence of additional organic compounds (TICs). The TICs were
identified as PCBs.
Additional samples were collected on 18 November 1997 to verify the presence of
PCBs. These samples along with the sample containing the highest concentration
from the sampling conducted on 11 November 1997 was sent to the laboratory for
analysis. EPA Test Method SW-846 8080 was requested. Results indicate the
presence of PCBs ranging from 0.76 ppm to 14.8 ppm.
The source ofthe PCB contamination has not been Identified at this time. There is
o ^ Risk Assessment Guidance for Superfund Volume I Human Health Evaluation
Manual (Part A): USEPA, EPA/540/1-89/002
o
no PCB contaminated electrical equipment at this location.
PCBs are regulated by EPA under TSCA, unless the PCB waste also meets the
definition of RCRA hazardous waste. Material containing less than 50 ppm PCBs
are essentially unregulated by TSCA. However, RCRA has proposed an action
level In the Subpart S Rule, and EPA Region III has calculated and published a
risk-based concentration for PCBs.
The action level under the proposed Subpart S Rule is 0.09 mg/kg, and the Region
III Risk-Base Concentration for soil ingestion In a residential scenario is 0.083
mg/kg. These two cleanup levels were considered when evaluating the
remediation options for the site. Thiokol initiated a voluntary cleanup action to
remove the contaminated soil and prepare the site for the proposed construction.
Approximately 15 yd^ of contaminated soil was removed for offsite disposal.
Verification samples collected following the excavation revealed remaining
contamination at less than 5 ppm.
The building expansion planned for M-53 involves extending the existing concrete
pad out from the building (south) approximately 43 feet to accommodate placement
of a new chiller unit and jib crane as well as storage space. The attached drawing,
M53SWMU, shows relevant information to this proposal.
Geology
M-53 Is located on a the western flank of the Blue Springs Hills. This is a horst and
graben block fault system with two major fault trends: north 15 degrees east, and
east-west. The Blue Springs Hills at this location consists of Paleozoic carbonate
units covered with a thin veneer of Quaternary alluvium. The valley is filled with
Tertiary and Quaternary sediments which include older fluvial and lacustrine
sediments, alluvial fan deposits. Lake Bonneville sediments, and recent alluvium.
M-53 is sited on the gentle slope of a moderately large alluvial fan. Sediments
consist of unconsolidated gravels, sands, and clays of colluvial (debris flow), fluvial,
and alluvial depositional environments.
Hvdroloqy
Thiokol geology is complex, and the subsurface hydrology reflects this. Two
general hydrogeologic units are recognized at or adjacent to the M-53 facility: the
valley-fill and bedrock. The environments of deposition and diagenesis of each of
these units results in significant differences in the ability to store and transmit
ground water. Porosity and its influence on permeability is the most signiflcant
difference between the valley-fill and bedrock units. The porosity ofthe valley-fill is
generally interstifial porosity, while the bedrock porosity is generally secondary
(fractures).
Within the valley-fill, ground water occurs In unconfined conditions. The valley-fill
sediments consist of sands and gravels Interbedded with silts and clays. Generally,
the coarser materials are found along the margins ofthe valley and as basal
sediments above the bedrock. The silts and clays act as confining units
interbedded within the coarser materials. Within consolidated sediments, ground
•
water occurs in fault zones, fracture zones, and solution cavities in the limestones.
Upper and Lower Bounds of Aquifers
The upper and lower bounds ofthe uppermost perched aquifer is defined in the
following sections. The upper bound ofthe regional aquifer is Illustrated on Figure
3.4.1. The lower boundary ofthe regional aquifer is more difficult to delineate. The
regional aquifer is found in unconsolidated alluvial material within the Blue Springs
Valley, and in fractured bedrock along the flanks ofthe range. The unconsolidated
material consists primarily of interbedded (intertongued) sands, gravels, silts and
clays. There does not appear to be a distinct low permeability barrier beneath the
enfire site, although disconfinuous zones are ubiquitous. The thickness ofthe
aquifer is unknown but it is expected to be greater than 500 feet. All of the wells
installed to-date have been drilled to less than the bottom ofthe aquifer. The
deepest wells drilled into the saturated zone are Thiokol exploratory water wells
TCC8 and TCC8A, completed in 1960 and 1962 west of U. S. Air Force Plant 78.
Well TCC 8A was drilled 610 feet deep, penetrating 460 feet of saturated material.
Perched Water System
The perched water system at M-136 is located upgradient ofthe M-53 facility, and
is not a factor in this risk assessment.
Regional Water System
The regional water system is found at elevation 4275' MSL, approximately 200 feet
below ground level.
Ground Water Flow Directions
Static water levels are recorded semiannually from all monitoring wells.
Piezometric surface is illustrated on Figure 3.4.1. These are based upon water
levels compiled in November 1996.
Regional Ground Water Flow Direcfions
North of M-53, groundwater appears to pool behind the hydrogeologic constriction
at Engineering Mountain and flow east and then southward around the constriction
through fractures, solution channels, and fault breccia in the adjacent carbonate
rocks. Groundwater flows south-southwest through fractures and solution channels
on the western flank ofthe Blue Springs Hills to the coarse sediments ofthe alluvial
fan beneath M-53. Water moves predominately southward beneath M-53, and
reenters fractured carbonate bedrock on the southern edge ofthe alluvial fan. This
ground water flow pattern has not varied signiflcantiy during the time period that
Thiokol Corporation has monitored static water levels.
0
Transmissivity, Conductivity and Storativity Estimates
Hydraulic properties for wells adjacent to the M-186 area were submitted to the
Utah DSHW as Appendix K of the M-136 Buming Area Groundwater Monitoring
Program 1992 Interim Report.
Legal Description of Site
The center of the site is located approximately N. 41 39' 40", W. 112 26' 00" in
Section 29, TIIN, R5W, SLBM.
Historical Land Use and Ownership
Thiokol's Northern Utah-based Operations are located in Box Elder County, Utah,
approximately thirty miles northwest of Brigham City. The thirty-square-mile
plantsite is remote from any major population center and is also reasonably isolated
from ranches located at varying distances from the area boundaries. The plantsite
is composed of four major areas in which manufacturing and testing activities take
place: Administration and Manufacturing Areas, UDLV (Formerly Air Force Plant
78), Test Area, and the High-Performance Propellant Development Area.
Thiokol Corp. owns and operates all four areas. All areas are contiguous, and
waste disposal is managed by one organization.
Thiokol purchased the property and began operations in 1956. Prior to that time,
the plantsite was used principally for cattle grazing. No commercial crops (other
than open range) are grown on Thiokol property. Approximately 800 acres of
irrigated crops are grown south and west of Thiokol on the east flank of the
Promontory Mountains. Water for irrigafion is obtained from Promontory Mountain
sources.
Climate
Currently, Thiokol has a 10-meter meteorological tower and instruments to measure
and record air temperature, barometric pressure, relative humidity, solar radiation,
precipitation, vertical and horizontal wind speed and direcfion.
The climate ofthe Great Salt Lake Basin is largely dominated by the Sierra Nevada
Mountains, 500 mi. to the west and the Rocky Mountains, 300 mi. to the east. The
Sierras and other mountain ranges forming the west coast chain modify the
character of winter storms which move across the Great Salt Lake Basin. Most of
the moist Pacific air which brings winter precipitation to the basin must move across
these mountain barriers with consequent loss of moisture. This partially accounts
for the aridity ofthe Salt Lake Basin. The Rocky Mountains to the east also have a
marked moderating influence on the climate ofthe Salt Lake Basin. The mountains
prevent the weshward penetrafion of all but exceptionally strong masses of cold
continental air.
The Salt Lake Valley is frequently under the influence of the Great Basin high-
pressure area with its characteristic light winds and clear weather. The circulation
and terrain features favor the development of unusual vertical wind structures in the
valleys, in which the increase of wind speed with height is much less than that
observed in open, well-ventilated regions. This effect is most pronounced in the
summer months, when Salt Lake City shows a nearly constant mean wind in the
first 3,000 ft above the surface. Winds aloft dictate a mean east-southeasterly flow
over the area every month of the year.
The Thiokol plantsite is classifled as semiarid, with an average annual total
precipitafion of 14.88 inches at the Thiokol meteorology stafion. During the winter
months, the average total snov\rfall amounts to 24 inches. Precipitafion typically
occurs on 95 days out ofthe year (includes trace precipitation). During the year, it
would be expected that 35 percent of the days would be clear, 30 percent of the
days would be partly cloudy, 34 percent would be cloudy, and fog would be
expected to occur about 1 percent of the time.
Locally, temperatures in the Blue Creek Valley are strongly affected by the Great
Salt Lake. Because of Its high salt content, the lake does not freeze, allowing it to
act as a heat sink through the year. This influence tends to lengthen the growing
season, lower summer temperatures, and raise winter temperatures (URM, 1985).
December, January, February, July, and August contribute the least rain during the
year.
Background Levels of Constituents
A summary of laboratory results for background levels of inorganic constituents
reported during Thiokol's RFI is found in the following Table.
ANALYTE
Cadmium
Chromium
Copper
Lead
Nickel
Silver
Zinc
Arsenic
Mercury
Selenium
Beryllium
Barium
MINIMUM
0.1
13.4
0.1
1.5
9.47
0.1
32.7
6.5
0.011
0.1
0.5
109
MAXIMUM
0.95
38.6
11.5
32.5
29.1
12.8
74.4
16.3
0.035
2.7
1.06
141
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
0
Potentiallv Exposed Populations
The Thiokol facilities are located in a remote area of eastern Box Elder County,
Utah. Box Elder County occupies an area of 5,640 square miles. A 1980
populafion of 33,212 represents a population density of about six individuals per
square mile. The populafion ofthe rural areas ofthe county (less than 2,500
population) is about 14,000. Family groups living in the area of Thiokol can be
classified into (1) ranchers and farmers, and (2) externally employed heads of
o
o
households who commute from long distances. There are no schools, hospitals, or
churches in the area ofthe plant. There are no inhabited buildings or ranch houses
within one mile ofthe M-381 facility.
Future land use is not expected to present a greater risk to human health than
present use because of the remote location, and the lack of nearby population
centers, potable water sources, and infrastructure. If the present industrial land use
changes, it will likely return to open-range grazing and nonirrigated farming and
ranching. Residential land use is not considered a reasonable probability for future
land use.
Current and future Thiokol workers are considered the rnost likely population which
might be exposed to contaminants at M-53.
OTHER SWMUs AT M-53 <-->
SWMU # 260 is a building discharge consisting of wastewater from sinks, BAC
cooling and boiler condensate. This SWMU is in close proximity to the newly
identifled site, but has been determined to be independent^. The discharge was
formerly to a drywell. The drywell was removed in the SO's at which time the
discharge pipe was extended north to a drainage channel. In 1995 the discharge
was connected to the wastewater collection system for treatment at Thiokol's
domestic wastewater treatment facility.
The drainage channel was sampled in March 1994 as part of Thiokol's RFI.
Volatile organics, semi-volatile organics, cadmium, mercui7, and pH analysis were
requested. All volatile organics detected were qualifled by the lab as below the
quantification limit and/or also found in the laboratory blank. The laboratory was
unable to analyze the surface samples for semi-volatiles due to recent asphalt
paving activity which rendered the samples unusable. Samples collected from the
two foot depth revealed the presence of phthalate esters which were also found in
the blank.
In the fall of 1996, the locafion ofthe removed drywell was scaled from facility
drawings and the site sampled. Samples were collected at five and 10 foot depths.
Metals concentrations were within background ranges and organics detected were
all qualified as below the reporting limit (PQL). The laboratory data is included as
part ofthis report.
PROPOSED CORRECTIVE ACTION FOR THE SITE
Thiokol proposes to expand the planned concrete pad further south (beyond 43
feet) and then transition down to a formed concrete drainage channel, transitioning
back to the level ofthe existing asphalt road as shown on the accompanying
drawing.
^ Laboratory Analytical Data from sampling event dated 12 Nov 96 lists the site as
SWMU #260 due to the close proximity of the sites, and that the new site had not
yet been designated.
9
Extending the concrete to cap the residual contamination in the area would
essentailly eliminate the potential exposure; thus, mininni2:ing risk by:
• eliminafing access of individuals to currently contaminated media, and
• prevenfing currently uncontaminated media from becoming contaminated
in the future due to contaminate transport
With the exposure pathway removed, the level of risk present at the site would
meet the risk exposure criterion of R315-101.
ENVIRONMENTAL LAB WORK REQUEST Li^^/
4 THIOKOL ENVIRONMENTAL LABORATORY LWR No. El 1304
Login No.
A AF ll'/iUciZ-52 fo
COST CENTER
L^Z4-C
WORKORDER
/ 2 A/cv re
ORCAMZ.VTION
/:./) ^'rj/]n-<^^,^/rJ^
MAILSTOP REPORT RESU LTS TO:
HELEN WARD, MS 301
/
b^
i
SAMPLE
pr 0fVi\ Sw
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IS' TIAG^J Ii-
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TYPE
G
l/
y
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i/^
y
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ix
t/
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c
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SAMPLE INFORMATION
LOCATION
MSS
II
If
//
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TIME
/^S6)
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TEST
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AhSh,Ai,d<^,B^, cdXr, Cu
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REMARKS
,^,l>>,Si,/}^,Z>, ^.P-
CHAIN OF CUSTODY
RELINQIII.SIIEDBV
^ /4^£i^^^
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DATE
//'/^•fi^
TIME
/o:is'^
RECErV'ED B^
/f//^/^//..,..^
DATE
- //'/:i.'-9^
TIME
//'T<r
4 D.VTF. KniPl.ETED
FOR LABORATORY USE ONLY
DATE REPORTED
#
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Requested
Monaay, November 18, 1996
TESTED FOR Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp.UT 84322
Frank Walker
Project: Solid Waste Mgmt Invest.
Login Number L661
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
E3righam City, UT 84302-0707
{101-863-5445
800-863-8080
o
Lab Number Client Number
Test Requested
L661-1 #260 PT
sw 846, 9045
SW-846, 3050
SW-846, 3550
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846. 6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471A
SW-846, 7740
1^-846.'8260- --^
SW-846, 8270
Description
. DIS. SURF. M-53
pH Electrode Measurement
ICP/GFAA Metals Digestion
Sonication Extraction
Ag ICP Metals Analysis (RCRA)
Al
Ba
Be
Cd
Cr
Cu
Ni
Pb
Sb
Zn
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Selenium Analysis (RCRA)
^l^^iiatiSlCggariics^ ^
Semi-Volatile Organics
Received Collect Date/Time
Matrix
11/12/96 11/11/96 16:50
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
0
Pagel of 13
L661-2 #260 PT. DIS. 2 FT. M-53 11/12/96 11/11/96 17:05
o
SW 846, 9045 pH Electrode Measurement
SW-846, 3050 ICP/GFAA Metats Digestion
SW-846, 3550 Sonication Extraction
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846. 6010 Al ICP Metals Analysis (RCRA)
SW-846,6010 Ba ICP Metals Analysis (RCRA)
SW-846, 6010 Be ICP Metals Analysis (RCRA)
SW-846. 6010 Cd ICP Metals Analysis (RCRA)
SW-846, 6010 Cr ICP Metals Analysis (RCRA)
SW-846, 6010 Cu ICP Metals Analysis (RCRA)
SW-846, 6010 Ni ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 6010 Sb ICP Metals Analysis (RCRA)
SW-846, 6010 Zn ICP Metals Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7740 GF/VA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
SW-846, 8270 Semi-Volatile Organics
L661-3 #260,25' DN GD SUR. M-53
SW 846, 9045
SW-846, 3050
SW-846, 3550
SW-846,6010
SW-846. 6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846. 6010
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471A
SW-846. 7740
SW-846, 8260
SW-846, 8270
pH Electrode Measurement
ICP/GFAA Metals Digestion
Sonication Extraction
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Ni ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Sb ICP Metals Analysis (RCRA)
Zn ICP Metals Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Selenium Analysis (RCRA)
Volatile Organics
Semi-Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soii
Soil
Soil
Soil
Soil
Soil
Soil
11/12/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
11/11/96 17:15
o
Page 2 of 13
L661-4 #260,25' DN GD 2Fr. M-53 11/12/96 11/11/96 17:30
#
SW 846, 9045 pH Electrode Measurement
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846, 3550 Sonication Extraction
SW-846. 6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Al ICP Metals Analysis (RCRA)
SW-846. 6010 Ba ICP Metals Analysis (RCRA)
SW-846. 6010 Be ICP Metals Analysis (RCRA)
SW-846, 6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Cu ICP Metals Analysis (RCRA)
SW-846,6010 Ni ICP Metals Analysis (RCRA)
SW-846, 6010 Pb ICP Metals Analysis (RCRA)
SW-846,6010 Sb ICP Metals Analysis (RCRA)
SW-846,6010 Zn ICP Metals Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846. 7740 GFAA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
SW-846, 8270 Semi-Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
o
Worl< Order Comments
8270 Semivolatile extracts for samples L661-1, L661-3, and 1.661-4 were dark and oily.
Sample L661-1 showed PCB's present at approximatly 14,200ug/kg (see attached list of
Tentatively Identified Compounds (TICs) for individual PCB and estimated concentrations).
No PCB's were detected in samples L661-2. L661-3, and L661-4.
c-^l^l U^-6v-w^
<•' Certified By
I'//'^/1L
Date
This is to certify that the following samples were analyzed using good laboratory practices to show
the folowing results:
o
Page 3 of 13
0
#
9
O
sample ID: #260 PT. DIS. SURF *r
Listing of Results by Sample 6^'
y vo ,u ^I'l"^
M-53 Lab ID: L661-1 Collect Date: 11/11/96 16:50
Test Parameter
PH
ICP/GFAA METALS DIGESTION
SONICATION EXTRACTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
SELENIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
!^Ul ,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
jl,1-DICHLOROETHENE
ll, 1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2.4-TRIMETHYLBEN2ENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1.4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
IIBROMOFORM
BROMOMETHANE
jr-iCAi^eON TETRACHLORIDE
jkCHLOROBENZENE
p! ^CHLOROETHANE
KCHLOROFORM
^CHLOROMETHANE
•f5ciS-1,2-DICHLOROETHENE
10061-01-5'i.;CIS-1,3-DICHLOROPROPENE
' JlpiBROMOCHLOROMETHANE
tjJDIBROMOMETHANE
^DICHLORODIFLUOROMETHANE
['ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
•ftl
Result
7.71
13300
U
99
0.6
0.6
24
17
U
17
U
99
7
0.3
1.7
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
1.3 J
u
u
1.4 J
u
u
u
1.3 J
u
Units
ug/g
ug/g
ug/g
ug/g
ug'g
U9'9
ug'g
ug'g
ug'g
ug'g
ug'g
ug'g
ug'g
ug/g
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug'kg
ug'kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
1.1 JB ug/kg
U
U
U
1.2 J
U
U
U
U
U
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
Det.
Limit
1.6
3.3
0.07
0.1
0.1
0.3
0.1
1.6
0.7
0.2
0.3
0.9
0.01
1.3
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
Rep.
Limit
8.1
16
0.3
0.7
0.7
1.6
0.7
8.1
3.3
0.98
1.3
2.6
0.03
4.4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Dill.
Facior Method
SW 846, 9045
SW-846, 3050
SW-846, 3550
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846. 6010
SW-846. 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471A
SW-846, 7740
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst.
MTB
KWB
SDM
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
KEN
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
PUIMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Test Date
11/15/96 14:45
11/14/96 10:00
11/14/96 00:00
11/14/96 14:18
11/14/96 14:18
11/14/96 14:18
11/14/96 14:18
11/14/96 14:18
11/14/9614:18
11/14/96 14:18
11/14/96 14:18
11/14/96 14:18
11/14/96 14:18
11/14/96 14:18
11/14/96 15:38
11/15/96 14:16
11/14/96 17:38
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11.10
Page 4 of 13
m
(I
#
108-38-3 ffS!
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6 f
135-98-8.
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
4 1 il
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
'I-'NAPHTHALENE
il
i
•^ r
k
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
ll^'^OLUENE
1 ':lfRANS-1,2-DICHLOROETHENE
10061-02-6 a JTRANS-1,3-DICHLOROPROPENE
79-01-6 E| ITRICHLOROETHENE
75-69-4 ^TRICHLOROFLUOROMETHANE
75-01-4 HIVINYL CHLORIDE
120-82-1 1,2,4-TRICHLOROBENZENE
95-50-1 1,2-DICHLOROBENZENE
541-73-1 1,3-DICHLOROBENZENE
106-46-7 1,4-DICHLOROBENZENE
95-95-4 2,4,5-TRICHLOROPHENOL
88-06-2 2,4,6-TRICHLOROPHENOL
120-83-2 2,4-DICHLOROPHENOL
105-67-9 2,4-DIMETHYLPHENOL
51-28-5 2,4-DINITROPHENOL
121-14-2 2,4-DINITROTOLUENE
606-20-2 2.6-DINITROTOLUENE
91-58-7 2-CHLORONAPHTHALENE
95-57-8 2-CHLOROPHENOL
91-57-6 2-METHYLNAPHTHALENE
95-48-7 2-METHYLPHENOL
88-74-4 2-NITROANILINE
88-75-5 2-NITROPHENOL
56-55-3 3,3'-DICHLOROBENZIDlNE
99-09-2 3-NITROANILINE
534-52-1 4,6-DINITRO-2-METHYLPHENOL
101 -55-3 4-BROMOPHENYL-PHENYLETHER
59-50-7 4-CHLORO-3-METHYLPHENOL
106-47-8 4-CHLOROANILINE
7005-72-3 4-CHLOROPHENYL-PHENYLETHER
106-44-5 4-METHYLPHENOL
100-01-06 4-NITROANILINE
100-02-7 4-NITROPHENOL
83-32-9 ACENAPHTHENE
208-96-8 ACENAPHTHYLENE
120-12-7 ANTHRACENE
S6-5S-3 BENZO(A)ANTHRACENE
50-32-8 BENZO(A)PYRENE
205-99-2 BENZO(B)FLUORANTHENE
191-24-2 BENZO(G,H,l)PERYLENE
207-08-9 BENZO(K)FLUORANTHENE
111-91-1 BIS(2-CHLOROETHOXY)METHANE
111-44-4 BIS(2-CHLOROETHYL)ETHER
108-60-1 BIS(2-CHLOROISOPROPYL)ETHER
117-81-7 BIS(2-ETHYLHEXYL)PHTHALATE
85-68-7 BUTYLBENZYLPHTHALATE
120-12-7 CARBAZOLE
218-01-9 CHRYSENE
84-74-2 DI-N-BUTYLPHTHALATE
117-84-0 DI-N-OCTYLPHTHALATE
53-70-3 D;BCNZ(A,H)ANTHRACENE
132-64-9 DIBENZOFURAN
84-66-2 UIETHYLPHTHALATE
131-11-3 DIMETHYLPHTHALATE
206-44-0 FLUORANTHENE
86-73-7 FLUORENE
118-74-1 HEXACHLOROBENZENE
87-68-3 HEXACHLOROBUTADIENE
77-47^ HEXACHLOROCYCLOPENTADIENE
67-72-1 HEXACHLOROETHANE
U
U
U
U
U
U
U
U
U
U
1.3 J
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
114 J
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
"9'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug'kg
ug'kg
ug/kg
ug'kg
ug'kg
ug'kg
ug/kg
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
63
63
63
147
133
90
90
SO
1400
190
63
63
110
73
77
50
120
333
80
800
63
100
60
140
133
120
80
63
117
63
260
83
167
137
160
177
190
190
83
83
333
83
83
83
83
100
63
S3
73
63
63
30
200
53
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
333
333
333
333
333
333
333
333
1670
333
333
333
333
333
333
1670
333
667
1670
1670
333
667
667
333
333
1670
1670
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846, 8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846.8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW.846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846.8270
1 SW-846.8270
1 SW.846.8270
1 SW.846,8270
1 SW.846.8270
1 SW.846,8270
MMR
MMR
M/iR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
tJMR
MMR
MMR
NflMR
MMR
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/96 11:10
11/14/9611:10
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11'14/96 19:08
11/14/96 19:08
11/14/9619:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/9619:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
Page 5 Of 13
<»
n
193-39-5
78-59-1
621-64-7
86-30-6
91-20-3
98-95-3
87-86-5
85-01-8
108-95-2
129-00-0
INDENO(1 ,2,3-CD)PYRENE
ISOPHORONE
N-NITROSO-DI-N-PROPYLAMINE
N-NITROSODIPHENYLAMINE
NAPHTHALENE
NITROBENZENE
PENTACHLOROPHENOL
PHENANTHRENE
PHENOL
PYRENE
[ Sample ID: #260 PT. DIS. 2 FT. ^1 "^"^^
630-20-6ff
71-55-6 ;:,
79-34-5 A
79.00-5 \
75-34-3 t
75-35-4 l|
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7 '.
590-20-7 ;
78-93-3
95-49-8 .
591-78-6 '
106-43-4 '
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2 1
74-83-9 1
56-23-5 i
108-90-7 1
75.00-3
67-66-3
74-87.3 L
Test Parameter
PH
ICP/GFAA METALS DIGESTION
SONICATION EXTRACTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
SFI FNIUM
^ 1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,I-DICHLOROETHANE
1.1-DICHLOROETHENE
1,1.DICHLOROPROPENE
1,2,3.TRICHLOROBENZENE
, 1.2,3.TRICHLOROPROPANE
- 1,2,4-TRICHLOROBENZENE
•1,2,4-TRIMETHYLBENZENE
". 1,2-DIBROMO-3-CHLOROPROPAN
\ 1,2-DIBROMOETHANE
11,2-DICHLOROBENZENE
H, 1,2-DICHLOROETHANE
U 1,2-DICHLOROPROPANE
11,3,5-TRIMETHYLBENZENE
j| 1,3-DICHLOROBENZENE
\ 1,3-DICHLOROPROPANE
\ 1,4-DICHLOROBENZENE
i 2,2-DICHLOROPROPANE
2-BUTANONE
|2-CHLOROTOLUENE
12-HEXANONE
\ 4-CHLOROTOLUENE
1 4-ISOPROPYLTOLUENE
1 4-METHYL-2-PENTANONE
1 ACETONE
1 BENZENE
1 BROMOBrNZENE
1 BROMOCHLOROMETHANE
\ BROM JDICHLOROMETHANE
|i BROMOFORM
jifBROMOMETHANE
i|cARBON TETRACHLORIDE
ICHLOROBENZENE
^CHLOROETHANE
fcHLOROFORM
'i.CHLOROMETKMNE
U
U
U
U
U
U
U
U
U
U
Result
7.65
12900
U
87
0.6
0.9
19
9.2
U
13
U
48
6.6
0.03
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
1
u
u
1.1
u
u
u
u
u
1.1
u
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
Units
ug'g
ug'g
ug'g
ug'g
ug'g
ug'g
ug'g
ug'g
ug'g
ug'g
ug'g
ug'g
ug'g
ug'g
ug'kg
ug'kg
ug'kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug'kg
ug'kg
ug'kg
J ug'kg
ug'kg
ug/kg
J ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
JB ug/kg
ug/kg
123
73
400
63
53
47
120
180
50
63
Det.
Limit
1.5
3.1
0.06
0.1
0.1
0.3
0.1
1.5
0.6
0.2
0.2
0.9
0.01
1.2
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
333
333
333
333
333
333
1670
333
333
333
Lab ID:
Rep.
Limit
7.7
15
0.3
0.6
0.6
1.5
0.6
7.7
3.1
0.9
1.2
2.5
0.03
4.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
1
1
1
1
1
1
1
1
1
1
SW.846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
11/14/96 19:08
L661 -2 Collect Date: 11 /11 /96 17:05
Dil.
Facnpr Method
1 SW 846, 9045
SW.846, 3050
SW.846, 3550
SW.846, 6010
SW.846, 6010
SW.846, 6010
SW.846, 6010
SW.846, 6010
SW.846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW.846, 7471A
SW.846, 7740
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846. 8260
SW.846. 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW-846, 8260
SW.846. 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW.846, 8260
SW.846, 8260
SW.846. 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
MTB
KWB
SDM
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
KEN
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
mm
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Test Date
11/15/96 14:45
11/14/96 10:00
11/14/96 00:00
11/14/96 14:21
11/14/96 14:21
11/14/96 14:21
11/14/96 14:21
11/14/96 14:21
11/14/96 14:21
11/14/96 14:21
11/14/96 14:21
11/14/96 14:21
11/14/96 14:21
11/14/96 14:21
11/14/96 15:47
11/15/96 14:26
11/14/96 17:47
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
=age6 of 13
•
o
156-59.4 itt CIS.1,2.DICHLOROETHENE
10061.01^j CIS-1,3-DICHLOROPROPENE
f DIBROMOCHLOROMETHANE
'li DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
•EIHEXACHLOROBUTADIENE
i-^jlSOPROPYLBENZENE
r,i M,P-XYLENE
ft-?
METHYLENE CHLORIDE
^.BUTYLBENZENE
igN-PROPYLBENZENE
I^INAPHTHALENE
Ip-XYLENE
j:SEC-BUTYLBENZENE
ifSTYRENE
l' IJITERT-BUTYLBENZENE
'ijTETRACHLOROETHENE
gOLUENE
_j|i]|TRANS.1,2.DICHLOROETHENE
10061.02-6 !;'.TRANS.1,3-DICHLOROPROPENE
79.01.6 IJTRICHLOROETHENE
75.69.4 jwjrRICHLOROFLUOROMETHANE
75.01.4 ^.VINYL CHLORIDE
120-82-1 1,2,4-TRICHLOROBENZENE
95-50-1 1,2-DICHLOROBENZENE
541-73-1 1,3-DICHLOROBENZENE
106-46-7 1,4-DICHLOROBENZENE
95-95-4 2,4,5-TRICHLOROPHENOL
88-06-2 2,4,6-TRICHLOROPHENOL
120-83-2 2,4-DICHLOROPHENOL
105-67-9 2,4-DIMETHYLPHENOL
51-28-5 2,4-DINITROPHENOL
121-14-2 2,4-DINITROTOLUENE
606-20-2 2,6-DINITROTOLUENE
91-58-7 2-CHLORONAPHTHALENE
95-57-8 2-CHLOROPHENOL
91-57-6 2-METHYLNAPHTHALENE
95-48-7 2-METHYLPHENOL
88-74-4 2-NITROANILINE
88-75-5 2-NITROPHENOL
56-55-3 3,3'-DICHLOROBENZIDINE
99-09-2 3-NITROANILINE
534-52.1 4,6.DINITR0.2.METHYLPHENOL
101.55.3 4-BROMOPHENYL-PHENYLETHER
59-50-7 4-CHLORO-3-METHYLPHENOL
106-47-8 4.CHLOROANILINE
7005-72-3 4-CHLOROPHENYL-PHENYLETHER
106-44-5 4.METHYLPHENOL
100-01-06 4-NITROANILINE
100-02-7 4-NITROPHENOL
83-32-9 ACENAPHTHENE
208-96-8 ACENAPHTHYLENE
120-12-7 ANTHRACENE
56-55-3 BENZO(A)ANTHRACENE
50-32-8 BENZO(A)PYRENE
205-99-2 BENZO(B)FLUORANTHENE
191-24-2 BEN;:O(G,H,I)PERYLENE
207-08-9 BENZO(K)FLUORANTHENE
111-91-1 BI.S(2-CHLOROETHOXY)METHANE
111-44-4 r.lS(2-CHLOROETHYL)ETHER
108-60-1 B1S(2-CHL0R01S0PR0PYL)ETHER
117-81-7 BIS(2-ETHYLHEXYL)PHTHALATE
85-68-7 BUTYLBENZYLPHTHALATE
120-12-7 CARBAZOIL
218-01-9 CHRYSPNE
84-74-2 DI-N-nU fYLPHTHALATE
117-84-0 DI-N-OCTYLPHTHALATE
53-70-3 DIBENZ'.A,H)ANTHRACENE
132-64-9 DIBENZOFURAN
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug'kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug'kg
ug'kg
ug'kg
ug/kg
ug'kg
ug'kg
ug/kg
ug'kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
63
63
53
147
133
90
90
90
1400
190
63
63
110
73
77
50
120
333
80
800
63
1l}0
60
140
133
120
80
63
117
63
260
83
167
137
160
177
190
190
83
83
333
83
83
83
83
100
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
333 1
333
333
333
333 1
333
333
333
1670
333
333
333
333
333
333
1670
333
667
1670
1670
333
667
667
333
333
1670
1670
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
SW-846, 8260
SW-846, 8260
SW.846. 8260
SW-846, 8260
SW'S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
SW-846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW-846. 8260
SW.846. 8260
SW.846, 8260
SW.846. 8260
SW-846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846. 8260
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW.846, 8270
I SW.846.8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846. 8270
SW.846, 8270
1 SW.846,8270
1 SW.846,8270
1 SW.846,8270
1 SW.846, 8270
1 SW-846.8270
1 SW.846,8270
1 SW.846,8270
1 SW.846,8270
1 SW.846,8270
1 SW.846,8270
1 SW-846,8270
1 SW.846,8270
1 SW.846,8270
1 SW.846,8270
1 SW.846,8270
1 SW.846,8270
1 SW.846,8270
1 SW.8<5,8270
1 SW.846,8270
1 SW.846,8270
1 SW.8A6,8270
1 SW.846,8270
1 SV/.S46,8270
1 SW-846,8270
1 SW.846,8270
1 SW.846,8270
1 SW.846.8270
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/96 11:46
11/14/9611:46
11/14/96 11:46
11/14/96 11:46
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17.36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17.36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
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11/14/96 17.36
11/14/96 17:36
Page 7 of 13
•
9
#
84-66-2 tDIETHYLPHTHALATE
131-11-3 DIMETHYLPHTHALATE
206-44-0 FLUORANTHENE
86-73-7 FLUORENE /"
118-74-1 HEXACHLOROBENZENE
87-68-3 HEXACHLOROBUTADIENE
77-47-4 HEXACHLOROCYCLOPENTADIENE
67-72-1 HEXACHLOROETHANE
193-39-5 INDENO(1,2,3-CD)PYRENE
78-59-1 ISOPHORONE
621-64.7 N.NITROSO.DI.N.PROPYLAMINE
86.30-6 N-NITROSODIPHENYLAMINE
91-20-3 NAPHTHALENE
98-95-3 NITROBENZENE
87-86.5 PENTACHLOROPHENOL
8501.8 PHENANTHRENE
108-95.2 PHENOL
129.00.0 PYRENE
1 Sample ID: #260,25' DN GD SUR.^- "^ M.53
Test Parameter
PH
ICP/GFAA METALS DIGESTION
SONICATION EXTRACTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
SELENIUM
630.20.6 Ml ,1,1,2-TETRACHLOROETHANE
71.55.6 w|l,1,1.TRICHLOROETHANE
79.34.5 1
79-00.5 1
75.34-3 1
75-35-4 i
11.1,2.2.TETRACHLOROETHANE
11,1,2-TRICHLOROETHANE
11,1-DICHLOROETHANE
IMI, 1-DICHLOROETHENE
563-58-6 ill,1-DICHLOROPROPENE
87-61-6 l| ,1,2,3.TRICHLOROBEN2ENE
96.18-4
120-82.1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
, ,1,2,3-TRICHLOROPROPANE
: 1,2,4-TRICHLOROBENZENE
• J,2,4-TRIMETHYLBENZENE
jl ,2-DIBROMO-3-CHLOROPROPAN
iil ,2-DIBROMOETHANE
;i1,2.DICHLOROBENZENE
||l ,2-DICHLOROETHANE
W ,2-DICHLOROPROPANE
f i^ ,3,S-TRIMETHYLBENZENE
•|l ,3-DICHLOROBENZENE
j'S 1,3-DICHLOROPROPANE
ttl ,4-DICHLOR DBENZENE
:'i2,2-DICHLOROPROPANE
II2-BUTANONE
I'SZ-CHLOROl OLUENE
591-78-6 f}.||2-HEXAh'ONE
106-43-4
99.87.6
108.10.1
67.64-1
71-43.2
108.86.1
74.97.5 I
ffl4-CHLOROTOLUENE
'! 4-;SOPROPYLTOLUENE
iiji 4-METHYL-2-PENTANONE
Sj ACETONE
1 BENZENE
I'BROMOBENZENE
-CJBROMOCHLOROMETHANE
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
Result
7.8
9690
U
78
0.4
0.5
21
16
U
15
13
122
5.9
0.3
2.2
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
U
u
u
u
u
u
u
u
u
u
1.2 J
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug'g
ug/g
ug/g
ug/g
ug'g
ug'g
ug/g
ug/g
ug'g
ug'g
ug/g
ug'g
ug/g
ug/g
ug/kg
ug/kg
ug'kg
ug'kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug'kg
ug/kg
63
53
73
63
63
30
200
53
123
73
400
63
53
47
120
180
50
63
Det.
Limit
1.6
3.3
0.07
0.1
0.1
0.3
0.1
1.6
0.7
0.2
0.3
0.9
0.01
1.3
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
333
333
333
333
333
333
333
333
333
333
333
333
333
333
1670
333
333
333
Lab ID:
Rep.
Limit
8.2
16
0.3
0.7
0.7
1.6
0.7
8.2
3.3
0.99
1.3
2.6
0.02
4.5
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
1 SW.846,8270
-1 SW.846,8270
1 SW.846,8270
-1 SW.846,8270
1 SW.846,8270
•1 SW.846,8270
•1 SW.846,8270
•1 SW.846,8270
1 SW.846,8270
•1 SW.846,8270
'1 SW.846,8270
-1 SW-846,8270
1 SW.846,8270
•' SW.846,8270
•1 SW.846,8270
•I SW.846,8270
1 SW.846,8270
1 SW.846,8270
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
L66I.3 Collect Date:
Diii.
Fac:tor Method
•1 SW 846, 9045
SW.846, 3050
SW.846, 3550
1 SW.846,6010
1 SW.846,6010
1 SW.846,6010
1 SW.846,6010
•1 SW.846,6010
1 SW-846,6010
1 SW.846,6010
1 SW.846,6010
1 SW.846,6010
1 SW.846,6010
•I SW.846,6010
1 SW-846,7060
1 SW.846, 7471A
1 SW-846, 7740
1 SW.846,8260
1 SW.S46,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
•1 SW.846,8260
•1 SW-846, 8260
1 SW.846,8260
•1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846.8260
1 SW.846.8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846.8260
1 SW.846,8260
1 SW.846,8260
1 SW.846.8260
1 SW.846,8260
1 SW-846,8260
Analyst
MTB
KWB
SDM
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
KEN
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
11/14/96 17:36
1/11/96 17:15
Test Date
11/15/96 14:45
11/14/96 10:00
11/14/96 00:00
11/14/96 14:36
11/14/96 14:36
11/14/96 14:36
11/14/96 14:36
11/14/96 14:36
11/14/96 14:36
11/14/96 14:36
11/14/96 14:36
11/14/96 14:36
11/14/96 14:36
11/14/96 14:36
11/14/96 16:14
11/15/96 14:30
11/15/96 08:28
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
Pages of 13
#
#
75-27-4 f
75-25-2 ''.[
74-83-9 ..j
56-23.5 1
108-90-7f
75-00-3 1
67-66-3 1:
74-87-3 :
156-59-4j
10061-01-!
124-48-1 _
74-95-3
75-71-8 •
100-41-4! '<
87-68-3 K
98.82.8 H
108-38-3
75-09-2
104-51-8 '
103-65-1 j
91-20-3 ''
95-47-6 !
135-98-8 '
100-42-5
98.06.6
127.18-4
108-88-3
156-60-5
?l BROMODICHLOROMh 1 HANE
i BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
' CHLOROETHANE
CHLOROFORM
1, CHLOROMETHANE
; CIS-1,2-DICHLOROETHENE
5I CIS.1,3.DICHLOROPROPENE
f DIBROMOCHLOROMETHANE
i DIBROMOMETHANE
1 DICHLORODIFLUOROMETHANE
1 ETHYLBENZENE
1 HEXACHLOROBUTADIENE
1 ISOPROPYLBENZENE
W M.P.XYLENE
•m METHYLENE CHLORIDE
\ N.BUTYLBENZENE
•" N.PROPYLBENZENE
l| NAPHTHALENE
•ilcXYLENE
;|SEC-BUTYLBENZENE
^ISTYRENE
:VERT.BUTYLBENZENE
ISTETRACHLOROETHENE
•IJTOLUENE
i^TRANS-1,2.DICHLOROETHENE
10061-02-6|TRANS-1,3-D1CHLOROPROPENE
79-01-6 (IIJjTRICHLOROETHENE
75-69-4 ||LTRICHLOROFLUOROMETHANE
75-01-4 ^VINYL CHLORIDE
120.82-1 1,2,4.TRICHL0R0BENZENE
95.50.1 1,2-DICHLOROBENZENE
541-73.1 1,3.DICHLOROBENZENE
106-»6.7 1,4.DICHLOROBENZENE
95.95-4 2,4,5.TRICHLOROPHENOL
88.06.2 2,4,6-TRICHLOROPHENOL
120.83-2 2,4.DICHLOROPHENOL
105.67.9 2,4-DIMETHYLPHENOL
51.28.5 2,4.DlNITROPHENOL
121.14.2 2,4-DINITROTOLUENE
606.20.2 2,6.DINITROTOLUENE
91.58-7 2-CHLORONAPHTHALENE
95.57.8 2-CHLOROPHENOL
91.57.6 2.METHYLNAPHTHALENE
9S-»8-7 2.METHYLPHENOL
88.74-4 2.NITROANILINE
88.75-5 2-NITROPHENOL
56-55-3 3,3'-DICHLOROBENZIDINE
99-09-2 3.NITROANILINE
534-52-1 4,6-DlNITRO-2.METHYLPHENOL
101.55.3 4.BROMOPHENYL.PHENYLETHER
59.50.7 4.CHLORO.3.METHYLPHENOL
106-47-8 4.CHLOROANILINE
7005.72.3 4.CHLOROPHENYL.PHENYLETHER
IO6.44.5 4.METHYLPHENOL
100.01.06 4.NITROANILINE
100-02.7 4-NITROPHENOL
83-32-9 ACENAPHTHENE
208-96-8 ACENAPHTHYLENE
120-12-7 ANTHRACENE
56-55-3 BENZO(A)ANTHRACENE
50-32-8 BENZO(A)PYRENE
205-99-2 BENZO(B)FLUORANTHENE
191-24.2 BENZO(G,H,l)PERYLENE
207.08-9 BENZO(K)FLUORANTHENE
111-91-1 BIS(2-CHLOROETHOXY)METHANE
111-44-4 BIS(2-CHLOROETHYL)ETHER
108-60-1 BIS(2.CHLOROISOPROPYL)ETHER
1.9 J
U
U
U
2.1 J
U
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1 JB ug/kg
U
U
U
1.7 J
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
1.7 J
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
•J
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug'kg
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
63
63
63
147
133
90
90
90
1400
190
63
63
110
73
77
50
120
333
80
800
63
100
60
140
133
120
80
63
117
63
260
83
167
137
160
177
190
190
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
333
333
333
333
333
333
333
333
1670
333
333
333
333
333
333
1670
333
667
1670
1670
333
667
667
333
333
1670
1670
333
333
333
333
333
333
333
333
333
333
333
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.S46,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW-846,8260
1 SW.846.8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW-«46,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846.8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846,8260
1 SW.846, 8270
1 SW.846,8270
1 SW-846,8270
1 SW.846.8270
1 SW.846,8270
1 SW.846,8270
1 SW.846,8270
1 SW.846.8270
1 SW.846,8270
1 SW.846,8270
1 SW.846.8270
1 SW.846,8270
1 SW.846,8270
1 SW.846,8270
1 SW.846. 8270
1 SW-846,8270
1 SW.846,8270
1 SW.846,8270
1 SW.846,8270
1 SW.846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846.8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW.846,8270
1 SW.846.8270
1 SW-846,8270
1 SW.846.8270
1 SW.846.8270
1 SW.846.8270
1 SW.846,8270
1 SW.846,8270
1 SW-846,8270
1 SW.846,8270
1 SW.846,8270
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
- JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 12:21
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
=age9 of 13
•
9
9
117.81.7 BIS(2-ETHYLHEXYL)PHTHALATE
85-68-7 BUTYLBENZYLPHTHALATE
120-12-7 CARBAZOLE
218-01.9 CHRYSENE
84.74-2 DI.N.BUTYLPHTHALATE
117-84.0 DI.N.OCTYLPHTHALATE
53.70-3 DIBENZ(A,H)ANTHRACENE
132.64.9 DIBENZOFURAN
84-66-2 DIETHYLPHTHALATE
131-11-3 DIMETHYLPHTHALATE
206-44-0 FLUORANTHENE
86-73-7 FLUORENE
118-74-1 HEXACHLOROBENZENE
87-68-3 HEXACHLOROBUTADIENE
77-47-4 HEXACHLOROCYCLOPENTADIENE
67.72-1 HEXACHLOROETHANE
193-39-5 INDENO(1,2,3-CD)PYRENE
78-59-1 ISOPHORONE
621-64-7 N-NITROSO-DI-N-PROPYLAMINE
86-30-6 N-NITROSODIPHENYLAMINE
91-20-3 NAPHTHALENE
98-95-3 NITROBENZENE
87-86-5 PENTACHLOROPHENOL
85.01-8 PHENANTHRENE
108.95-2 PHENOL
129-00-0 PYRENE
1 Sample ID: #260,25' DN GD 2FT. ^ 'j M-53
Test Parameter
PH
ICP/GFAA METALS DIGESTION
SONICATION EXTRACTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
SELENIUM
630-20-6
71-55.6
79.34.5
79.00.5
75.34.3
75-35-4
563-58-6
87-61-6
96-18-4
120-82.1
95.63.6
96.12.8
IO6.93-4
95.50-1
107-06-2
78-87-5
108-67-8
541-73-1
•4
f
1
1
1
!
ti
t
It
^t \i
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1.2,3-TRICHLOROBENZENE
1,2,3-TRICHLORdPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETKANE
1,2-DICHLOROBENZENE
1,2-DICHLOP JETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
142-28-9 ||j!jl,?.DICHLOROPROPANE
106-46-7
590-20-7
78-93-3
|11,4-DICHLOROBENZENE
1) 2,2-DICHLOROPROPANE
>l'S2.BUTANONE
95-49-8 y^2-CHLOROT0LUENE
i>1580 '
W»139 J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
Result
7.7
14700
U
110
0.6
0.1
19
9.7
U
13
U
46
7.1
U
2
u
1.4 J
U
U
U
U
U
U
U
u
u
u
U
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug'kg
ug'kg
ug'kg
ug/kg
ug'kg
ug'kg
ug'kg
ug'kg
ug'kg
ug'kg
ug'kg
ug'kg
ug'kg
ug'kg
ug'kg
Units
ug'g
ug'g
ug'g
ug'g
ug/g
ug'g
ug/g
ug/g
ug'g
ug'g
ug'g
ug/g
ug/g
ug'g
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug/kg
ug'kg
ug/kg
ug/kg
ug'kg
83
83
333
83
83
83
83
100
63
53
73
63
63
30
200
S3
123
73
400
63
S3
47
120
180
50
63
Det.
Limit
1.6
3.1
0.06
0.1
0.1
0.3
0.1
1.6
0.6
0.2
0.3
0.9
0.01
1.3
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
1670
333
333
333
Lab ID:
Rep.
Limit
7.8
16
0.3
0.6
0.6
1.6
0.6
7.8
3.1
0.9
1.3
2.5
0.04
4.3
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
SW-846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.S46, 8270
SW.846. 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW-846, 8270
SW.846. 8270
SW.846, 8270
SW.846. 8270
SW.846, 8270
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
L661-4 Collect Date:
Dill.
Factor Method
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
SW 846, 9045
SW.846, 3050
SW.846, 3550
SW.846, 6010
SW.846, 6010
SW.846, 6010
SW.846. 6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846. 6010
SW-846. 6010
SW-846,6010
SW-846,6010
SW-846, 7060
SW-846, 7471A
SW.846. 7740
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
Analyst
MTB
KWB
SDM
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
KEN
CRS
MMR
vnviR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
11/14/96 19:53
1/11/96 17:30
Test Date
11/15/96 14:45
11/14/96 10:00
11/14/96 00:00
11/14/96 14:39
11/14/96 14:39
11/14/96 14:39
11/14/96 14:39
11/14/96 14:39
11/14/96 14:39
11/14/96 14:39
11/14/96 14:39
11/14/96 14:39
11/14/96 14:39
11/14/96 14:39
11/14/96 16:23
11/15/96 14:35
11/15/96 08:37
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
Page 10 of 13
#
o
o
2-HEXANONE
4-CHLOROTOLUENE
4.ISOPROPYLTOLUENE
4.METHYL.2.PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
74-87-3 ,;f CHLOROMETHANE
156.59-4 ^Ic'S.1,2-DICHLOROETHENE
10061-01-5':|ciS-1,3-DICHLOROPROPENE
124-48-1 ^DIBROMOCHLOROMETHANE
»fDIBROMOMETHANE
IMDICHLORODIFLUOROMETHANE
JjETHYLBENZENE
HEXACHLOROBUTADIENE
j ,1; ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N.PROPYLBENZENE
NAPHTHALENE
CXYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS.1.2.D1CHLOROETHENE
TRANS.1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
(VINYL CHLORIDE
1,2,4.TRICHLOROBENZENE
1,2.DICHLOROBENZENE
1,3.DICHLOROBENZENE
1.4.DICHLOROBENZENE
2,4,5.TRICHLOROPHENOL
2,4,6.TRICHLOROPHENOL
2,4-DICHLOROPHENOL
2,4.DIMETHYLPHENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
2-METHYLNAPHTHALENE
2-METHYLPHENOL
2-NITROANILINE
2-NITROPHENOL
3,3'-DICHLOROBENZIDINE
3-NITROANILINE
4,6-DINITRO-2-METHYLPHENOL
4-BROMOPHENYL-PHENYLETHER
4-CHLORO.3.METHYLPHENOL
4-CHLOROANILINE
4-CHLOROPHENYL-PHENYLETHER
4-METHYLPHENOL
4-NITROANIUNE
4-NITROPHENOL
ACENAPHTHENE
ACENAPHTHYLENE
ANTHRACENE
108-88-3 p
156-60-5 v'>i
10061-02
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1 JB ug/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug/kg
ug/kg
ug'kg
ug'kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug'kg
ug/kg
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
63
63
63
147
133
90
90
90
1400
190
S3
S3
110
73
77
50
120
333
80
800
63
100
60
140
133
120
80
63
117
63
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
333
333
333
333
333
333
333
333
1670
333
333
333
333
333
333
1670
333
667
1670
1670
333
667
667
333
333
1670
1670
333
333
333
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW-846, 8260
SW-846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.S46, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
SW.846, 8260
t SW.846,8260
t SW.846,8260
1 SW.846,8260
t SW.846.8260
I SW.846,8260
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846. 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846. 8270
SW-846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
1 SW-«46,8270
1 SW.846.8270
1 SW.846,8270
1 SW.846,8270
1 SW.846,8270
1 SW.846.8270
1 SW.846,8270
1 SW-«46,8270
1 SW.846,8270
1 SW.846,8270
1 SW.846,8270
1 SW.846,8270
1 SW.846,8270
1 SW.846,8270
1 SW.846,8270
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
AfflUIR
MMR
MMR
MMR
MMR
MMR
hfl\/IR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12.57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 12:57
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/9618:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
Pagell of 13
m
#
55.55.3 BENZO(A)ANTHRACENE
50.32.8 BENZO(A)PYRENE
205-99.2 BENZO(B)FLUORANTHENE
191-24.2 BENZO(G,H,l)PERYLENE
207.O8.9 BENZO(K)FLUORANTHENE
111.91.1 BIS(2<:HL0R0ETH0XY)METHANE
111-44-4 BIS(2.CHL0R0ETHYL)ETHER
108.60.1 BIS(2-CHLOROISOPROPYL)ETHER
117-81-7 BIS(2-ETHYLHEXYL)PHTHALATE
85-68-7 ; BUTYLBENZYLPHTHALATE
120-12-7 CARBAZOLE
218-01-9 CHRYSENE
84-74-2 DI-N-BUTYLPHTHALATE
117-84-0 DI-N-OCTYLPHTHALATE
53-70-3 DIBENZ(A,H)ANTHRACENE
132-64-9 DIBENZOFURAN
84-66-2 DIETHYLPHTHALATE
131-11-3 DIMETHYLPHTHALATE
206-44-0 FLUORANTHENE
86-73-7 FLUORENE
118-74-1 HEXACHLOROBENZENE
87-68-3 HEXACHLOROBUTADIENE
77-47-4 HEXACHLOROCYCLOPENTADIENE
67-72-1 HEXACHLOROETHANE
193-39-5 INDENO(1,2,3-CD)PYRENE
78-59-1 ISOPHORONE
621-64-7 N-NITROSO-DI-N-PROPYLAMINE
86-30-6 N-NITROSODIPHENYLAMINE
91-20-3 NAPHTHALENE
98-95-3 NITROBENZENE
87-86-5 PENTACHLOROPHENOL
85-01-8 PHENANTHRENE
108-95-2 PHENOL
129-00-0 PYRENE
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug'kg
ug/kg
ug/kg
ug'kg
260
83
167
137
160
177
190
190
83
83
333
83
83
83
83
100
63
53
73
63
63
30
200
53
123
73
400
63
53
47
120
180
50
63
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
1670
333
333
333
SW.846, 8270
SW-846, 8270
SW.846, 8270
SW.846, 8270
SW-846. 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW-846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW-846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846, 8270
SW.846. 8270
SW.846, 8270
SW.846, 8270
SW-846, 8270
SW.846, 8270
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
11'14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
11/14/96 18:22
#
Page 12 of 13
#
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected
but was below the detection limit, i
B This flag is used when an analyte is found in the blank as well as the sample
Det. Limit Method Detection Limit (approximately three times the signal noise level)
Rep. Limit Reporting Limit is nonmally the value of the lowest standard run with the
analysis. The value is approximately 5 to 10 times the Method Detection Limit.
Dil. Factor Dilution Factor - The prepared sample was diluted by this factor because the
sample was too concentrated or due to other interferences in the sample matnx.
Any diiution factor causes an appropriate increase in the method detection limit
and reporling limit.
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This
flag is used either when estimating a concentration for tentatively identified compounds or
when the data indicated the presence of a compound that meets the identification criteria
but the result is less than the specified reporting limit (e.g, 3 J with a reporting limit of 10)
^
9
Page 13 of 13
#
Tentatively Identified Compound Report
Sample
Method
Library
R.T.
21.19
21.60
22.36
22.44
22.76
22.87
22.97
23.27
23.37
23.52
23.57
23.78
23.86
24.01
24.04
24.45
24.52
24.54
24.70
25.00
25.05
25.16
25.55
26.04
26.39
: L661-1
: SW846, 8270
: NBS75K.L
Est. Conc
586 J ug/kg
165 J ug/kg
228 J ug/kg
823 J ug/kg
371 J ug/kg
1910 Jug/kg
541 J ug/kg
397 J ug/kg
758 J ug/kg
134 Jug/kg
1510 Jug/kg
345 J ug/kg
247 J ug/kg
889 J ug/kg
1040 Jug/kg
793 J ug/kg
467 J ug/kg
397 J ug/kg
235 J ug/kg
1267 J ug/kg
152 J ug/kg
137 Jug/kg
377 J ug/kg
240 J ug/kg
184 J ug/kg
979 J ug/kg
7,730 J ug/kg
5,280 J ug/kg
184 J ug/kg
14,200 J ug/kg
•A*******«>*****AA**A***********i**^**********^^^^^A
Tentative ID
1,1'-Biphenyl, 2,2',3,4-tetrachloro
1,1'-Biphenyl, 2,2',5,6-Tetrachloro
1,1'-Biphenyl, 2,3',5,5'-tetrachlor
1,1'-Biphenyl, 2,2',4,5,5'-pentachloro
1,1'-Biphenyl, 2,2',3',4,5-Pentachioro
1,1'-Biphenyl, 2,3,3',4',6-pentachloro
1,1'-Biphenyl, 2,3,3',4,4'-pentachloro
1,1'-Biphenyl, 2,2',4,4',6-Pentachloro
1,1'-Biphenyl, 2,3,3',4,4'-pentachloro
1,1'-Biphenyl, 2,3',4,4',5,5'-hexachloro
1,1'-Biphenyl, 2,3',4,4',5-pentachloro
1,1'-Biphenyl, 2,2',3,3',4,4'-hexachloro
1,1'-Biphenyl, 2,2',3,4',5',6-hexachloro
1,1'-Biphenyl, hexachloro-
1,1'-Biphenyl, 2,3',4,4',5-pentachloro
1,1'-Biphenyl, 2,3,3',4,4',5-hexachloro
1,1'-Biphenyl,2,2',3,3',5,5'-Hexachloro
1,1'-Biphenyl, 2,3,4,5,6-pentachloro
1,1'-Biphenyl, hexachloro-
1,1'-Biphenyl, hexachloro-
1,1'-Biphenyl, 3,3',4,4',5,5'-hexachloro
1,r-Biphenyl, 2,2',3,3',4,6'-hexachloro
1,1'-Biphenyl, 2,3,3',4,5,6-hexachtoro
1,1'-Biphenyl, 3,3',4,4',5,5'-hexachloro
1,1'-Biphenyl, 2,3,3',4,4',5,5'-heptachloro
Total Tetrachloro-1,1 '-Biphenyl's
Total Pentachloro-1,1 '-Biphenyl's
Total Hexachloro-1,1'-Biphenyl's
Total Heptachloro-1,1 '-Biphenyl's
Total Poly Chlorinated Biphenyl's
CAS# Qual
052663-59-9
041464-41-9
041464-42-0
037680-73-2
041464-51-1
038380-03-9
032598-14^
039485-83-1
032598-14^
052663-72-6
031508-00-6
038380-07-3
038380-04-0
026601-64-9
031508-00-6
038380-08-4
035694-04-3
018259-05-7
026601-64-9
026601-64-9
032774-16-6
038380-05-1
041411-62-5
032774-16-6
039635-31-9
99
99
99
99
99
99
99
99
99
99
99
99
99
99
99
99
99
95
99
99
99
99
99
99
99
#
ENVIRONMENTAL LAB WORK REQUEST
L0--7^
*
™ THIOKOL ENVIRONMENTAL LABORATORY LWR No. El 1308
Login No. /_f^ 7t
f^ fU/'LiLL^ 6.^:YC'
COST CENTER WORKORDER
/ m^ A'A-'^'U/i-
ORCANIZATION
.iwr
MAILSTOP REPORT RESULTS TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
a
SAMPLE
7/-I; 3 /
v.; -:/ ^
"•' M -^ / 3
^Ai^S3-^
s
ll'
11
i:
D.\TE
/'< /i-.--
/9Vcu
?€yC/^
TYPE
G
>
y
y
^
^.^
c
'
-
LOCATION
A/-S ]
AL- TT
//i^\^
L-''TJ/y >.''^ <-.
M'S^2
^-/r'
TIME
/44S'
./^-•^V-
;>iV"r
^ii?
/yif-<r
TEST
^l'/3
/^^c./l
/'^: rb
•pc/Z
•p<^- 3
.^ >
REMARKS
••-^Vci ^.l-ilV-'
A/Wt/f<^^
CHAIN OF CUSTODY
RELIN(:»l ISIIF.D B^
A.-irc^./->L_
DATE
/i^/M-'^(,-
TIME
/<rc'<i;
RECEIVED BS
//^/#..^
(/1' i;^ I't- /
DATE
^/^'A^^^^
TIME
/^;^iP'
«l
FOR LABORATORY USE ONLY
UArF<()\IPl.ETEI) DATE REPORTED SIGNATI RE
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Requested
Thursday, December 12, 1996
TESTED FOR Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp.UT 84322
Frank Walker
Project: Solid Waste Mgmt Invest.
Login Number L678
Lab Number Client Number
Test Requested Description
ANALYZED BV Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-5445
800-863-8080
Received Collect Date/Time
Matrix
SW846,
SW.846,
8080
3550
Organochlorine Pestlcides/PCBs
Sonication Extraction
Soil
Soil
L678.1 M-53.1
SW 846. 8080
SW.846. 3550
L678.2 M.53.2
SW 846, 8080
SW.846, 3550
L678-3 M-53-3
SW 846, 8080
SW-846. 3550
Organochlorine Pesticides/PCBs
Sonication Extraction
Organochlonne Pesticides/PCBs
Sonication Extraction
Organochlorine Pesticides/PCBs
Sonication Extraction
L678-4 #260 PT OF DIS SUR.
SW 846. 8080
SW-846, 3550
L678-5 M-53-4
SW 846, 8080
SW-846. 3550
Organochlorine Pesticides/PCBs
Sonication Extraction
Organochlonne Pesticides/PCBs
Sonication Extraction
L678-6 T-75 DUMP SITE
11/18/96
Soil
Soil
11/18/96
Soil
Soil
11/18/96
Soil
Soil
11/12/96
Soil
Soil
11/19/96
Soil
Soil
11/20/96
11/18/96 14:45
11/18/96 14:50
11/18/96 14:55
11/11/96 16:50
11/19/96 08:27
11/20/96 13:00
''•C-
Certified By Date
This is to certify that the following samples were analyzed using good laboratory practices to show
the folowing results:
Page 1 of 5
Listing of Results by Sample
1 Sample ID: M-53-1
Test Parameter
4,4'-DDD
4,4'-DDE
4,4'-DDT
ALDRIN
ALPHA-BHC
AROCLOR 1016
AROCLOR 1221
AROCLOR 1232
AROCLOR 1242
AROCLOR 1248
AROCLOR 1254
AROCLOR 1260
BETA-BHC
CHLORDANE
DELTA-BHC
DIELDRIN
ENDOSULFAN 1
ENDOSULFAN II
ENDOSULFAN SULFATE
ENDRIN
ENDRIN ALDEHYDE
ENDRIN KETONE
GAMMA-BHC
HEPTACHLOR
HEPTACHLOR EPOXIDE
METHOXYCHLOR
TOXAPHENE
SONICATION EXTRACTION
1 Sample ID: M-53-2
Test Parameter
4,4'-DDD
4,4'-DDE
4.4'-DDT
ALDRIN
ALPHA-BHC
AROCLOR 1016
AROCLOR 1221
AROCLOR 1232
AROCLOR 1242
AROCLOR 1248
AROCLOR 1254
AROCLOR 1260
BETA-BHC
CHLORDANE
DELTA-BHC
DIELDRIN
ENDOSULFAN 1
ENDOSULFAN II
ENDOSULFAN SULFATE
ENDRIN
ENDRIN ALDEHYDE
ENDRIN KETONE
GAMMA-BHC
HEPTACHLOR
HEPTACHLOR EPOXIDE
METHOXYCHLOR
TOXAPHENE
SONICATION EXTRACTION
Result
u
u
u
u
u
u
U
U
u
u
1.18
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Result
u
U
u
u
u
u
u
u
u
u
1.59
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Det.
Limit
0.033
0.016
0.033
0.016
0.016
0.03
0.03
0.03
0.03
0.03
0.03
0.03
0.016
0.033
0.033
0.016
0.05
0.016
0.16
0.05
0.067
0.033
0.016
0.016
0.33
0.67
0.67
Det.
Limit
0.033
0.016
0.033
0.016
0.016
0.03
0.03
0.03
0.03
0.03
0.03
0.03
0.016
0.033
0.033
0.016
0.05
0.016
0.16
0.05
0.067
0.033
0.016
0.016
0.33
0.67
0.67
Lab ID:
Rep.
Limit
0.1
0.05
0.1
0.05
0.05
0.09
0.09
0.09
0.09
0.09
0.09
0.09
0.05
0.1
0.1
0.05
0.1
0.05
0.5
0.1
0.2
0.1
0.05
0.05
1
2
2
Lab ID:
Rep.
Limit
0.1
0.05
0.1
0.05
0.05
0.09
0.09
0.09
0.09
0.09
0.09
0.09
0.05
0.1
0.1
0.05
0.1
0.05
0.5
0.1
0.2
0.1
0.05
0.05
1
2
2
L678-
DiL
Collect Date: 11/18/96 14:45
Factor Method
11)
11)
11)
10
10
10
11)
10
11)
11)
11)
10
11)
10
11)
11)
10
10
10
10
10
10
10
10
10
10
10
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846. 8080
SW 846, 8080
SW 846. 8080
SW 846, 8080
SW 846. 8080
SW 846. 8080
SW 846. 8080
SW 846. 8080
SW 846. 8080
SW 846. 8080
SW 846, 8080
SW 846. 8080
SW 846, 8080
SW 846, 8080
SW 846. 8080
SW 846. 8080
SW 846, 8080
SW 846, 8080
SW 846. 8080
SW 846, 8080
SW 846. 8080
SW 846, 8080
SW-846, 3550
Analvst
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
SDM
L678-2 Collect Date:
Dil.
Factor Method
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW 846, 8080
SW 846. 8080
SW 846, 8080
SW 846, 8080
SW 846. 8080
SW 846. 8080
SW 846, 8080
SW 846, 8080
sw 846. 8080
SW 846. 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW-846, 3550
Analvsl
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
SDM
Test Date
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/21/96 09:05
11/19/96 00:00
1/18/96 14:50
Test Date
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/21/96 10:36
11/19/96 00:00
Page 2 of 5
Sample ID: M-53-3 Lab ID: L678-3 Collect Date: 11/18/96 14:55
•
Test Parameter
4,4'.DDD
4,4'.DDE
4,4'-DDT
ALDRIN
ALPHA-BHC
AROCLOR 1016
AROCLOR 1221
AROCLOR 1232
AROCLOR 1242
AROCLOR 1248
AROCLOR 1254
AROCLOR 1260
BETA-BHC
CHLORDANE
DELTA-BHC
DIELDRIN
ENDOSULFAN 1
ENDOSULFAN II
ENDOSULFAN SULFATE
ENDRIN
ENDRIN ALDEHYDE
ENDRIN KETONE
GAMMA.BHC
HEPTACHLOR
HEPTACHLOR EPOXIDE
METHOXYCHLOR
TOXAPHENE
SONICATION EXTRACTION
Result
U
u
u
u
u
u
u
u
u
u
0.764
u
u
u
U
U
U
U
u
U
U
u
u
u
u
u
u
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Det.
Limit
0.033
0.016
0.033
0.016
0.016
0.03
0.03
0.03
0.03
0.03
0.03
0.03
0.016
0.033
0.033
0.016
0.05
0.016
0.16
0.05
0.067
0.033
0.016
0.016
0.33
0.67
0.67
Rep.
Limit
0.1
0.05
0.1
0.05
0.05
0.09
0.09
0.09
0.09
0.09
0.09
0.09
0.05
0.1
0.1
0.05
0.1
0.05
OS
0.1
0.2
0.1
0.05
0.05
1
2
2
DiL
Factor Method
10
11}
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ID
10
ID
ID
ID
ID
10
10
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846. 8080
SW 846. 8080
SW 846. 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846. 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846. 8080
SW 846, 8080
SW 846. 8080
SW 846. 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846. 8080
SW.846, 3550
Analyst
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
SDM
Test Date
11/21/96 11:18
11/21/96 11:18
11/21/96 11:18
11/21/96 11:18
11/21/96 1V18
11/21/96 11:18
11/21/96 11:18
11/21/95 11:18
11/21/96 11:18
11/21/96 11:18
11/21/96 11:18
11/21/95 11:18
11/21/95 11:18
11/21/96 11:18
11/21/96 11:18
11/21/96 11:18
11/21/96 11:18
11/21/96 11:18
11/21/96 11:18
11/21/96 1118
11/21/96 11:18
11/21/96 11:18
11/21/96 11:18
11/21/96 11:18
11/21/96 11:18
11/21/96 11:18
11/21/96 11:18
11/19/96 00:00
Sample ID: #260 PT OF DIS SUR
Test Parameter
4,4-.DDD
4,4'.DDE
4,4'.DDT
ALDRIN
ALPHA.BHC
AROCLOR 1016
AROCLOR 1221
AROCLOR 1232
AROCLOR 1242
AROCLOR 1248
AROCLOR 1254
AROCLOR 1260
BETA-BHC
CHLORDANE
DELTA-BHC
DIELDRIN
ENDOSULFAN I
ENDOSULFAN II
ENDOSULFAN SULFATE
ENDRIN
ENDRIN ALDEHYDE
ENDRIN KETONE
GAMMA-BHC
HEPTACHLOR
HEPTACHLOR EPOXIDE
METHOXYCHLOR
TOXAPHENE
SONICATION EXTRACTION
•
Sample ID: M-53-4
Test Parameter
4,4'-DDD
4,4'.DDE
Lab ID: L678.4 Collect Date: 11/11/96 16:50
Result Units
U mg/kg
U
U
U
U
U
U
U
U
U
14.8
U
U
U
U
U
u
u
u
u
u
u
u
u
u
U
u
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Det.
Limit
0.033
0.016
0.033
0.016
0.016
0.03
0.03
0.03
0.03
0.03
0.03
0.03
0.016
0.033
0.033
0.016
0.05
0.016
0.16
0.05
0.067
0.033
0.016
0.016
0.33
0.67
0.67
Rep.
Limit
0.1
0.05
0.1
0.05
0.05
0.09
0.09
0.09
0.09
0.09
0.09
0.09
0.05
0.1
0.1
0.05
0.1
0.05
OS
0.1
0.2
0.1
0.05
0.05
1
2
2
Dill.
Factor
100
100
100
100
100
100
100
100
100
100
100
1IX)
100
100
100
100
100
100
100
100
100
100
100
100
100
IDO
IDO
Method
sw 846. 8080
SW 846, 8080
SW 846, 8080
SW 846. 8080
SW 846, 8080
SW 846. 8080
SW 846, 8080
SW 846. 8080
SW 846. 8080
SW 846, 8080
SW 846. 8080
SW 846, 8080
SW 846, 8080
SW 846. 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846. 8080
SW 846. 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846. 8080
SW.846, 3550
Analyst
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
SDM
Test Date
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/21/96 12:04
11/19/96 00:00
Lab ID: L678.5 Collect Date: 11/19/96 08:27
Det. Rep.
Result Units Limit Limit
U mg/kg 0.033 0.1
U mg/kg 0.016 0.05
Dil.
Factor Method
-.0 sw 846, 8080
'0 SW 846, 8080
Analyst Test Date
BLW 11/21/96 12:45
BLW 11/21/96 12:45
Page 3 of 5
0
9
4,4'-DDT
ALDRIN
ALPHA-BHC
AROCLOR 1016
AROCLOR 1221
AROCLOR 1232
AROCLOR 1242
AROCLOR 1248
AROCLOR 1254
AROCLOR 1260
BETA-BHC
CHLORDANE
DELTA-BHC
DIELDRIN
ENDOSULFAN 1
ENDOSULFAN II
ENDOSULFAN SULFATE
ENDRIN
ENDRIN ALDEHYDE
ENDRIN KETONE
GAMMA-BHC
HEPTACHLOR
HEPTACHLOR EPOXIDE
METHOXYCHLOR
TOXAPHENE
SONICATION EXTRACTION
1 Sample ID: T-75 DUMP SITE
Test Parameter
4,4'-DDD
4,4'-DDE
4.4'-DDT
ALDRIN
ALPHA-BHC
AROCLOR 1016
AROCLOR 1221
AROCLOR 1232
AROCLOR 1242
AROCLOR 1248
AROCLOR 1254
AROCLOR 1260
BETA-BHC
CHLORDANE
DELTA-BHC
DIELDRIN
ENDOSULFAN 1
ENDOSULFAN II
ENDOSULFAN SULFATE
ENDRIN
ENDRIN ALDEHYDE
ENDRIN KETONE
GAMMA-BHC
HEPTACHLOR
HEPTACHLOR EPOXIDE
METHOXYCHLOR
TOXAPHENE
SONICATION EXTRACTION
U
U
U
U
u
u
u
u
1.41
u
u
u
U
u
u
u
u
u
u
u
u
u
u
u
u
Result
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
0.033
0.016
0.016
0.03
0.03
0.03
0.03
0.03
0.03
0.03
0.016
0.033
0.033
0.016
0.05
0.016
0.16
O.OS
0.067
0.033
0.016
0.016
0.33
0.67
0.67
Det.
Limit
0.033
0.016
0.033
0.016
0.016
0.03
0.03
0.03
0.03
0.03
0.03
0.03
0.016
0.033
0.033
0.016
0.05
0.016
0.16
0.05
0.067
0.033
0.016
0.016
0.33
0.67
0.67
0.1
0.05
0.05
0.09
0.09
0.09
0.09
0.09
0.09
0.09
O.OS
0.1
0.1
0.05
0.1
0.05
0.5
0.1
0.2
0.1
0.05
0.05
1
2
2
Lab ID:
Rep.
Limit
0.1
0.05
0.1
0.05
0.05
0.09
0.09
0.09
0.09
0.09
0.09
0.09
0.05
0.1
0.1
0.05
0.1
0.05
0.5
0.1
0.2
0.1
0.05
0.05
1
2
2
10
10
10'
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
11)
10
10
10
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846. 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846. 8080
SW 846. 8080
SW 846. 8080
SW 846, 8080
SW.846, 3550
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
SDM
L678.6 Collect Date:
Dil.
Factor Method
1
1
1
1
1
'\
1
•j
•i
•1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846. 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846. 8080
SW 846. 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW-846. 3550
Analys
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
SDM
11/21/96 12:45
11/21/96 12:45
11/21/96 12:45
11/21/96 12:45
11/21/96 12:45
11/21/96 12:45
11/21/96 12:45
11/21/96 12:45
11/21/96 12:45
11/21/96 12:45
11/21/95 12:45
11/21/96 12:45
11/21/96 12:45
11/21/96 12:45
11/21/96 12:45
11/21/96 12:45
11/21/96 12:45
11/21/96 12:45
11/21/96 12:45
11/21/96 12:45
11/21/96 12:45
11/21/95 12:45
11/21/96 12:45
11/21/96 12:45
11/21/96 12:45
11/19/96 00:00
1/20/96 13:00
Test Date
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03.00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/21/96 03:00
11/20/96 00:00
Page 4 of 5
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, orthe compound was detected
but was below the detection limit.
B This flag is used when an analyte is found in the blank as well as the sample
Det. Limit Method Detection Limit (approximately three times the signal noise level)
Rep. Limit Reporting Limit is normally the value ofthe lowest standard run with the
analysis. The value is approximately 5 to 10 times the Method Detection Limit.
Dil. Factor Dilution Factor - The prepared sample was diluted by this factor because the
sample was too concentrated or due to other interferences in the sample matrix.
Any dilution factor causes an appropriate increase in the method detection limit
and reporting limit.
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This
flag is used either when estimating a concentration for tentatively identified compounds or
when the data indicated the presence of a compound that meets the identification criteria
but the result is less than the specified reporting limit (e.g. 3 J with a reporting limit of 10)
•
Page 5 of 5
ENVIRONMENTAL LAB WORK REQUEST fl^-
fl: ™ THIOKOL ENVIRONMENTAL LABORATORY LWR No. E11327
Login No.
r&r^'/y^cr^'-rf
ORGANIZATION /^
EXTENSION COST CENTER WORKORDER
/-zT-fy
MAILSTOP
1 «3/
REPORT RESULTS TO:
HELEN WARD, MS 301
.SAMPLE
/ 77/^^5/
7^/?^^/
/77^^JJ2
4
'M65-^f^'\
^MSZ-gJAN-Z
/UvJ-iJU4w-a
%
'
10
II
12
DATE
/V-f?
v
(/
/-3-yi
/'
i3 ^^
TVTE
C
;^
1 /
^r
K
X
K
c
SAMPLE INFORMATION
LOCATION
/97-Cf/
1 /
I r
M-S3>
M-^l>
M-si
TIME
mill—Bim
UPt'.lPO
11
»^
TEST
/&/S
^/
//
V^e*
V^ih
>c?^
REMARKS
CHAIN OF CUSTODY
RELINQUISHED BY DATE TIME RECEIVED BY
^^i^ ".r-v^ A^fy /9'y > ^ 'u^^
DATE
i-gr-^ '•-r
TIME
jjti^L
FOR LABORATORY USE ONLY
m
DATE COMPLETED DATE REPORTED SIGNATURE
•
CERTIFICATE OF ANALYSIS
Listing of sample information and Testing Requested
Thursday, January 30,1997
TESTED FOR Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp, UT 84322
Kevin Thackeray
Project: Misc. Environmentai Testing
Login Number L756
Lab No Client Number
Test Requested
I L756-1
Description
ANALYZED B Thiokol Environmental Laboratory
Thiokol corporation
P O Box 707 M/S 245
Brigham eity.UT 84302-0707
801-863^3732
800-863-8080
Received CollectDate/Time
Matrix
1776031. M-81 01/08/97 I:JU/08^7 09:00
sw 846, 8080 Analysis for PCBs in Oil Oil
L756-2 7013381. M-81 01/08/97 1JU^"°^^°^^°°
SW 846. 8080 Analysis for PCBs in Oil
L756-3 1776032, M-SI 01/08/97
SW 846, 8080 Analysis for PCBs in Oil
L756-4 M53-8JAN-1 01/08/97
SW 846, 8080 Organochlorine Pesticides/PCBs
/08/97 09:00
/08/97 00:00
L756-5 M53-8JAN-2
SW 846, 8080 Organochlorine Pesticides/PCBs
01/08/97 ::^W^7 00;pO
soil
L756-6 M53.8JAN-BG3 01/08/97 1/08/97 00:00
SW 846, 8080 Organochlorine Pesticides/PCBs aoil
Certified By "^^^^
T/7/S certifies that the following samples were analyzeci using good laboratoiy practiced fo »"'''*'"'® following results:
rM-
•
Page 1 of 4
Listing of Results by Sample
JBampI elD: 1776031, M-ei Lab ID: L75&-1 Collect Date: 01/08/97 09:00
Test Parameter
AROCLOR 1016
AROCLOR 1221
AROCLOR 1232
AROCLOR 1242
AROCLOR 1248
AROCLOR 1254
AROCLOR 1260
lample ID: 7013381, M-SI
Test Parameter
AROCLOR 1016
AROCLOR 1221
AROCLOR 1232
AROCLOR 1242
AROCLOR 1248
AROCLOR 1254
AROCLOR 1260
Result
u
u u
u
u
u
u
Result
u
u
u
u
u
u
u
Units
mgrtcg
mgrtig
mgrttg
mg/kg
mgrtig
mgrtcg
mgrtcg
Units
mg/kg
mgrtcg
mgrtcg
mg/kg
mgrtcg
mgrtcg
mgrtcg
Limtt
.204
.415
.202
.106
.091
.17
.385
1
Oet
.204
.415
.202
106
091
.17
.365
Umit Fattor
.612
1.25
.606
.318
.273
.51
1.01
Lab ID:
Rep.
.612
1.25
.606
.318
.273
.51
1.01
L756-2
DII.
JEactor
Method
sw 846, 8080
SW 846, 8080
sw 846,8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
Analvst
BLW
BLW
BLW
BLW
BLW
BLW
BLW
Collect Date: 01
Method
SW 846.8080
SW 846.8080
SW 846,8080
SW 846, 8080
SW 846, 8080
SW 846.8080
SW 846, 8080
Analyst
BLW
BLW
BLW
BLW
BLW
BLW
BLW
Test Date
01/17/97 04*1
01/17/97 04O1
01/17/97 04<M
01/17/97 04t)1
01/17/97 04fl1
01/17/97 04*1
01/17/9704*1
/08/97 09:00 |
Test Date
01/17/97 04:42
01/17/97 04:42
01/17/9704:42
01/17/9704:42
01/17/9704:42
01/17/97 04:42
01/17/9704:42
luampl lie 10: 1776032. M.81 Lab ID: L756-3 Collect Date: 01/08/97 09:00
Test Parameter
AROCLOR 1016
AROCLOR 1221
AROCLOR 1232
AROCLOR 1242
AROCLOR 1248
AROCLOR 1254
AROCLOR 1260
Result
u
u
u
u
u
u
u
Units
mg/kg
mgrtcg
mgrtcg
mgrtcg
mgrtcg
mgrtcg
mg/kg
Limit
.204
.415
.202
.106
.091
.17
.365
Limit
.612
1.25
.606
.318
.273
.51
1.01
JEactor Method
SW 846, 8080
SW 846, 8080
SW 846,6080
SW 846. 8080
SW 848, 8080
SW 846, 8080
SW 846, 8080
Analvst
BLW
BLW
BLW
BLW
BLW
BLW
BLW
Test Date
01/17/97 0523
01/17/97 0523
01/17/970523
01/17/970523
01/17/970523
01/17/97 0523
01/17/9705-23
JHumplelD: M53-8JAN-1
Test Parameter
4,4-.ODD
4,4'^3DE
4,4'.0DT
ALORIN
ALPHA-BHC
AROCLOR 1016
AROCLOR 1221
AROCLOR 1232
AROCLOR 1242
AROCLOR 1248
AROCLOR 1254
/VROCLOR 1260
BETA.BHC
CHLORDANE
OELTA-«HC
DIELDRIN
ENDOSULFAN I
ENDOSULFAN II
ENDOSULFAN SULFATE
ENORIN
ENDRIN ALDEHYDE
ENDRIN KETONE
GAMMA.BHC
HEPTACHLOR
HEPTACHLOR EPOXIDE
METHOXYCHLOR
TOXAPHENE
Lab ID: L756.4 Collect Date: 01/08/97 00:00
Result Units
U
u
u
u
u
u
u
u
u
u
3.47
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
mgrtcg
mg/kg
mgrtcg
mgrtcg
mgrtcg
mgrtcg
mg/kg
mgrtcg
mgrtcg
mg/kg
mgrtcg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mgrtcg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Det Rep. Oil.
Limit I imit Fartnr Method
.033
.016
.033
.016
.016
.03
.03
.03
.03
.03
.03
.03
016
.033
.033
.016
.05
.016
.16
OS
.067
.033
.016
.016
.33
.67
.67
.1
.05
.1
.05
.05
.09
.09
.09
.09
.09
.09
.09
.05
.1
.1
.05
.1
.05
.5
.1
.2
.1
.05
.05
1
2
2
SW846,
SW846,
SW846,
SW846,
SW846,
SW846,
SW846,
SW846,
SW846.
SW846,
SW846,
SW846,
SW846.
SW846,
SW846,
SW846.
SW846,
SW846,
SW846.
SW846.
SW846,
SW846.
SW846,
SW846,
SW846.
SW846,
SW846,
8080
8080
8080
8080
8080
8080
8080
8080
8080
8080
8080
8080
8080
8080
8060
8080
8080
8080
8080
8080
8080
8080
8080
8080
8080
8080
8080
Analyst
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
Test Date
01/16^703:50
01/16S7 03:50
01/16/9703:50
01/16/97 03S0
01/16/97 03:50
01/16/97 03:50
01/16/9703:50
01/16«7 03.-50
01/16^703:50
01/16/97 03:50
01/16/97 0350
01/ie«7 03:50
01/16S7 03:50
01/16/97 03:50
01/109703:50
01/16/97 03:50
01/16/9703:50
01/16/97 03:50
01/1619703:50
01/16/97 03:50
01/16/97 03:50
01/16/97 03:50
01/16^7 03:50
01/16/97 0350
01/16/97 0350
01/16/97 0350
01/16^7 03.50
Page 2 of 4
{sample ID:
1 Sample ID:
M53.8JAN-2
Test Parameter
4,4'.ODD
4,4-.ODE
4,4'.ODT
ALDRIN
ALPHA-flHC
AROCLOR 1016
AROCLOR 1221
AROCLOR 1232
AROCLOR 1242
AROCLOR 1248
AROCLOR 1254
AROCLOR 1260
BETA-BHC
CHLORDANE
DELTA-BHC
DIELDRIN
ENDOSULFAN 1
ENDOSULFAN II
ENDOSULFAN SULFATE
ENORIN
ENORIN ALDEHYDE
ENDRIN KETONE
HEPTACHLOR
HEPTACHLOR EPOXIDE
METHOXYCHLOR
TOXAPHENE
M53.8JAN-BG3
Test parameter
4,4'4DDD
4.44)DE
4,4'J:DT
ALDRIN
ALPHA.BHC
AROCLOR 1016
AROCLOR 1221
AROCLOR 1232
AROCLOR 1242
AROCLOR 1248
AROCLOR 1254
AROCLOR 1260
BETA.BHC
CHLORDANE
DELTA.BHC
DIELDRIN
ENDOSULFAN 1
ENDOSULFAN II
ENDOSULF/VN SULFATE
ENORIN
ENDRIN /UJ5EHYDE
ENDRIN KETONE
GAMMA-BHC
HEPTACHLOR
HEPTACHLOR EPOXIDE
METHOXYCHLOR
TOXAPHENE
Result
u
u
u
u
u
u
u
u
u
u 4.13
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
Result
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u u u
u
u
u
u
u
u u
u
Units
mgrtcg
mgrtcg
mgrtcg
mgrtcg
mg/kg
mgrtcg
mgrtcg
mg/kg
mgrtcg
mg/kg
mg/kg
mg/kg
mgrtcg
mgrtcg
mgrtcg
mg/kg
mg/kg
mg/kg
mg/kg
mgrtcg
mgrtcg
mgrtcg
mgrtcg
mgrtcg
mgrtcg
mgrtcg
mg/kg
Units
mgrtcg
mgrtcg
mgrtcg
mgrtcg
mgrtcg
mgrtcg
mg/kg
mgrtcg
mgrtcg
mg/kg
mgrtcg
mg/kg
mgrtcg
mgrtcg
mgrtcg
mgrtcg
mgrtcg
mg/kg
mgrtcg
mgrtcg
mgrtcg
mgrtcg
mgrtcg
mgrtcg
mg/kg
mgrtcg
mg/kg
Ub ID: L756-5
Oet
Limit
.033
.016
.033
.018
.016
.03
.03
.03
.03
.03
.03
.03
.016
.033
.033
.016
.05
.016
.16
.05
.067
.033
.016
.016
.33
.67
.67
D^
LiflMl
033
016
.033
.016
.016
.03
.03
.03
.03
.03
.03
.03
.016
.033
.033
.016
OS
.016
.16
.05
.067
.033
.016
.016
.33
.67
.67
Rep. Oil,.
LimiL .EnHor
.1
.05
.1
.05
.05
.09
.09
.09
.09
.09
.09
.09
.05
.1
.1
.05
.1
.05
.5
.1
.2
.1
.05
.05
1
2
2
Lab ID:
Rep.
f
L756-6
DiL
.1
.05
.1
.05
OS
.09
.09
.09
.09
.09
.09
.09
.05
.1
.1
.05
.1
.05
.5
.1
.2
.1
.05
.05
1
2
2
Collect Date: 01/08/97 00:00 |
Method
sw 846, 8080
SW 846,8080
SW 846,8080
SW 846, 8080
SW 846, 8080
SW 846.8080
SW 846, 8080
SW 846, 8080
SW 846,8080
SW 846, 8080
SW 846.8080
SW 846, 8080
SW 846. 8080
SW 846,8080
SW 846, 8080
SW 846. 8080
SW 846,8080
SW 846, 8080
SW 846, 8080
SW 846,8080
SW 846.8080
SW 846, 8080
SW 846, 8080
SW 846.8080
SW 846. 8080
SW 846, 8080
SW 846, 8080
Asalyst
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
B.W
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
Test Date
01/16/97 04:30
01/16/97 04.30
01/16/97 04:30
01/16/97 04:30
01/16/97 04:30
01/16«7 04:30
01/16/97 04:30
01/16«7 04:30
01/16/97 04:30
01/16«7 04.30
01/16/97 04:30
01/16fl7 04:30
01/16^7 04.30
01/16^704:30
01/16^7 04:30
01/16S7 04:30
01/16^7 04:30
01/16/97 04:30
01/16«7 04:30
01/16«7 04:30
01/16/97 04.30
01/16«7 04:30
01/16«7 04:30
01/16fl7 04.30
01/16«7 04:30
01/16/97 04:30
01/1647 04:30
Collect Date: 01/08/97 00.00 |
Method
SW 846, 8080
SW 846. 8080
SW 846. 8080
SW 846, 8080
SW 846, 8080
SW 846, 8080
SW 846.8080
SW 846, 8080
SW 846. 8080
SW 846, 8080
SW 846,8080
SW 846, 8080
SW 846,8080
SW 846.8080
SW 846, 8080
SW 846.8080
SW 846. 8080
SW 846. 8080
SW 846.8080
SW 846.8080
SW 846,8080
SW 846. 8080
SW 846.8080
SW 846.8080
SW 846, 8080
SW 846, 8080
SW 846.8080
Ari^lyst
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
Te?tPate
01/16^7 05:11
01/16S7 05:11
01/16/97 05:11
01/1647 05:11
01/1647 05:11
01/1647 05:11
01/1647 05:11
01/1647 05:11
01/1647 05:11
01/1647 05:11
01/1647 05:11
01/1647 05:11
01/1647 05:11
01/1647 05:11
01/1647 05:11
01/1647 05:11
01/16/97 05:11
01/1647 05:11
01/1647 05:11
01/1647 05:11
01/1647 05:11
01/1647 05:11
01/1647 05:11
01/1647 05:11
01/1647 05:11
01/1647 05:11
01/1647 05:11
Page 3 of 4
•
#
•
Data Reporting Qualilfiers
U Indicates compound was analyzed for and was not detected, or th<e compound was detected but was
below the detection limit.
B Gas Chromatography and Mass Spectral Data Flag. This flag is used when an analyte is found in
the blank as well as the sample
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This flag is used
either when estimating a concentration for tentatively identified compounds or when the data
indicated the presence of a compound that meets the identification criteria but the result is less than
the specified reporting limit (e.g. 3 J with a reporting limit of 10)
Det. Limit Method Detection Limit (approximately three times the signal noise level)
Rep. Limit Reporting Limit is normally the value of the lowest standard run writh the analysis. The value
is approximately 5 to 10 times the Method Detection Limit
Dil. Factor Dilution Factor - The prepared sample was diluted by this factor because the sample was
too concentrated or due to other interferences in the sample matrix. Any dilution factor
causes an appropriate increase in the method detection limit and reporting limit
Page 4of 4
1-5 Septic Drainfield
Investigation Plan
SWMU No. 667
«
Thiokol Corporation
RFI Work Plans, Vol. 4
21 February 1997
1.0 SAMPLING OBJECTIVE
Samples collected at this site during Phase I of the RFI will be analyzed for verification
of the presence of hazardous waste or hazardous waste constituents indicating a release
from the SWMU.
2.0 SITE LOCATION
•
Samples will be taken from the building drainfield. Refer to Facility Engineering
Drawings for additional detail for the site.
The building septic system which is to be sampled under this plan, and the
corresponding solid waste management unit is as follows:
1-5
..:Mfsvmv:sm:\\S.
667
3.0 BACKGROUND INFORMATION
This site is a septic drainfield which has been identified as having received industrial
wastewater flows having constituents potentially exceeding relevant regulatory, health
and risk based standards.
4.0 SAMPLING RATIONALE
The constiments of concem for this site are those which in previous wastewater
sampling have exceeded relevant regulatory, health and risk based standards. These
constiments are listed in Section 10.0 of this plan. Phase I sampling will focus on
verification of these constiments in the soil.
The constiments of concem for the septic system covered by this plan were chosen after
a review of existing sampling data. The discharges have been sampled previously for
parameters regulated by the Utah Water Quality Act.
5.0 SAMPLING STRATEGY
A judgmental sampling design will be implemented for Phase I sampling at this site.
Samples will be collected from four locations in the drainfield and at 5 and 10 foot
•
ENVIRDNMENTAL ENGINEERING
CDN I AMlNAl iDN SAMrLiiMG rLAN
rco m SCALE
NDNE
KAVINC ML Rtv.
n
Thiokol Corporation
RFI Work Plans, Vol. 4
21 February 1997
depths. The sampling sites will be selected by identifying iche approximate location of
each lateral distribution line leading from the splitter box, and dividing the length of the
lines by the number of distribution lines. If less than four lateral lines are present, the
fourth sample will be collected from between the distribution lines. One sample will be
collected from each division as close to the distribution line as possible. All dimensions
will be referenced from a permanent physical strucmre. In the event that a selected site
can not be sampled due to an obstruction (road, strucmre, overhead power line, etc.),
the sample will be obtained from the closest available alternate site. All variances to
this plan will be noted in the log book.
Samples from the septic tank were previously collected and analyzed, the results of
which were used in identifying constiments of concem for the drainfield.
Duplicate and QA/QC samples will be collected at the frequency shown in the
following chart.
SAMPLE TYPE PROPOSED FREOUENCY
Duplicate 5% or 1 per site, which ever is greater
Rinse Field Blanks 5% or 1 per site, which ever is greater
Spikes 1 % of the total RFI samples
6.0 BACKGROUND
Background samples have been collected in areas known or believed to be free of
contamination within the Manufacmring and Administration Area for use in comparing
concentrations. These background samples were collected at corresponding depths to
obtain samples in similar strata to those taken in the areas of concern.
Extensive soil sampling of the Thiokol facility has established a data base for namrally
occurring inorganic constiments. This data base consists of background samples used
in the closure of various RCRA facilities at Thiokol. The analytical results of the
background samples taken during Phase I sampling will be added to this data base to
provide site specific data. Analytical data obtained from investigation activities at this
site will be compared to this data base for determination of contamination above
background levels.
7.0 SAMPLING EQUIPMENT
1. New split-spoon sampler
Thiokol Corporation
RFI Work Plans, Vol. 4
21 February 1997
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
Field book
Certified clean sample bottles
Distilled water
Tape measure
Alconox soap wash
Tap water
Steam cleaner or wash buckets
Cleaning brush
Rubber gloves
Lab labels and seals
Cooler and ice
Stainless steel spamla
Shovel
Steam cleaned auger rig and tooling
8.0 SAMPLING TECHNIQUE
NOTE: For personal safety and to prevent cross contamination, use new rubber gloves
at each sample point when handling samples and sampling e;quipment.
1. Using a cleaned split-spoon and auger rig, retrieve a continuous soil sample
down to the prescribed depth. Samples will be collected at 5 and 10 foot depths
and placed into sample bottles. This will be accomplished as follows:
A) Carefully split open spoon
B) Measure core to fmd the required sample depths
C) Using cleaned stainless steel spamla, remove a portion of soil at the
required depth to fill the sample bottle(s).
D) Seal sample bottle lid with seal, note sample location and depth on
sample bottle label, and place in cooler containing ice.
E) Note soil lithology in log book
F) Scrape the remaining soil out of spoon and leave in same area as sample
point.
2. After sample has been taken at the depths noted above, decontaminate the split
spoon, spamla, and any associated equipment as follows.
Thiokol Corporation
RFI Work Plans, Vol. 4
21 February 1997
A) Steam clean with Alconox soap or scrub wiih brush in wash basin or
bucket containing Alconox soap and water.
B) Rinse with tap water (Do not reuse tap water)
C) Give final rinse with deionized water
NOTE: Containerize all wash and rinse water for hazardous waste
analysis to determine proper disposition.
The samples will be identified as follows with the depth noted after each
assigned sample number:
• The sample taken from site #1 at the 5 foot level would be labeled as
SWMU 667, #1 @5'.
9.0 SAMPLE DOCUMENTATION
The following information must be recorded in the Field Book:
Date and time of sampling
Sampler's name and signamre
Location of samples including depth
Type, number, sample number, and seals used on sample bottles
Weather
Texmre and color of samples
Any other pertinent information
10.0 ANALYTICAL PARAMETERS
The soil samples will be analyzed by a State certified lab on for the following constiments:
Thiokol Corporation
RFI Work Plans, Vol. 4
21 February 1997
BUILDING
1-5
SWMU NO:
667
PARAMETERS
RCRA Metals (Panel)
Volatile Organics
SW-846 METHODS
(UNLESS
OTHERWISE
INDICATED)
6010
8260
11.0 SAMPLE ACCOUNTABILITY AND CUSTODY
Follow procedures specified in the Waste Analysis Plan, Appendix 02.D of Thiokol Corporation
Hazardous Waste Permit Application. November 1991. These procedures are also contained in
the Data Collection Quality Assurance Plan in Volume Two of the RFI Work plans.
Requirements for sample custody and custody seals are discussed in these documents.
(»
THIOKOL CORPORATION
SEMI-ANNUAL RFI PROGRESS REPORT
1 September 1996 -1 March 1997
•
SEMI-ANNUAL RFI PROGRESS REPORT
1 SEPTEMBER 1996 -1 MARCH 1997
1. Description and estimation of the percentage of the RCItA Facility Investigation
completed;
To date, soils at the following SWMUs have been sampled:
M-19A Photographic Processing Discharge, SWMU 553;
E-517-W Surface Discharge, SWMU 282;
M-576-N Surface Discharge, SWMU 271;
M-514 Surface Discharge, SWMU 618;
S-501 Surface Discharge, SWMU 266;
M-640 Surface Discharge, SWMU 381;
M-641 Surface Discharge, SWMU 264;
M-585-N Surface Discharge, SWMU 273;
M-606 Surface Discharge, SWMU 527;
M-628 Surface Discharge, SWMU 528;
M-593 Surface Discharge, SWMU 274;
M-636-SW Surface Discharge, SWMU 367;
M-570 Surface Discharge, SWMU 285;
M-197 Surface Discharge, SWMU 483;
M-197-BP Surface Discharge, SWMU 360;
M-702 Surface Discharge, SWMU 620;
A-9 Surface Discharge, SWMU 267;
A-2 Surface Discharge, SWMU 560;
M-66 Surface Discharge, SWMU 432;
M-72 Surface Discharge, SWMU 263;
M-67 Surface Discharge, SWMUs 261 and 433;
M-14N and M-14S Surface Discharges, SWMUs 2:57 and 270;
M-53-BP Surface Discharge, SWMU 260;
M-53-E Surface Discharge, SWMU 259;
M-33-B and M-33-C Surface Discharges, SWMUs 258 and 413;
M-39 Surface Discharge, SWMU 425;
Combined Surface Discharge for M-8, M-9, M-10, M-52, and M-179-N,
SWMUs 268, 611, 269, 409, 472, and 255;
M-57 Surface Discharge, SWMU 615;
M-55-W Surface Discharge, SWMU 621;
M-9 Strand Bumer Exhaust Discharge, SWMU 652;
M-40 Surface Discharge, SWMU 642;
M-205 Surface Discharge, SWMU 286;
T-2 l-D Surface Discharge, SWMU 559;
T-6-A Surface Discharge, SWMU 287;
Old Drum Storage Area East of M-203, SWMU 203;
•
•
M-114 Surface Discharge, SWMU 426;
M-227 Hydrofluoric Acid Treatment Unit, SWMU 192;
M-9-NE Surface Discharge, SWMU 651;
M-186 Industrial Waste Landflll, SWMU 212;
M-136 Old Waste Oil Disposal Pit, SWMU 208;
M-187 Old Drum Storage Area, SWMU 551;
T-l Photographic Processing Drainfield, SWMU 648;
A-2 Photographic Processing Drainfield, SWMU 191;
I-IO-NE Subsurface Discharge, SWMU 645;
I-IO-SE Subsurface Discharge, SWMU 436;
I-IO-S Subsurface Discharge, SWMU 234;
T-l 11 Subsurface Discharge, SWMU 355;
T-24A Surface Discharge, SWMU 401;
M-2 Laundry Drainfield C, SWMU 627;
M-19A Drywell, SWMU 444;
M-39 Subsurface Discharge, SWMU 425;
T-51A Surface Discharge, SWMU 402;
M-2 Laundry Drainfield B, SWMU 626;
M-19A Strand Bumer Exhaust Discharge, SWMU 650;
M-585 Strand Bumer Exhaust Discharge, SWMU 649;
Historic Buming Ground NE of M-243, SWMU 202;
M-2 Laundry Drainfield A, SWMU 465;
Old Buming Grounds at M-136, SWMU 243;
M-193-S Septic Drainfield, SWMU 638;
M-193-N Septic Drainfield, SWMU 632;
M-191 Septic Drainfield, SWMU 631;
M-338 Subsurface Discharge, SWMU 608;
Domestic Wastewater Drainfields A, B and C, SV/MU 625;
M-348 Subsurface Discharge, SWMU 395;
M-72 Septic Drainfield, SWMU 630;
M-71 Septic Drainfield, SWMU 646;
M-19A Septic Drainfield, SWMU 628;
Removed Sump at M-622, SWMU 316;
M-117 Subsurface Discharge, SWMU 254;
T-14A Subsurface Discharge, SWMU 493;
T-3 Subsurface Discharge, SWMU 446;
M-53-MH Subsurface Discharge, SWMU 228;
Old Burning Ground West of M-174, SWMU 195;"^ ^ n 'Q. .. / i^-
Old Burning Ground East of M-303, SWMU 233,*^ ^^P ^' '^ ' W-^<^^ / 7
I-IO Septic Drainfield, SWMU 664;^
M-15A Septic Drainfield, SWMU 663;^
M-15A Drywell, SWMU 662^ ^ ^
M-137A Removed Waste Oil Storage Tank, SWMU 616;^^ ito^
M-53-BP Removed Drywell and Surface^ischarge, SWMUt^t6;
T-35 Beryllium Test Area, SWMU 201*; and
•
T-35 Beryllium Waste Disposal Area, SWMU 200.
#
353
354
397
497
609
622
640
643
655
667
T-053A
T-097A
T-015A
T-053
M-009NE
M-364
M-009SW
M-009SE
M-40
1-5
These sites represent approximately 96 percent of the SWMUs in Phase I of the RFI.
The sites remaining to be sampled in phase I of the RFI are listed below:
SWMU BUILDING DESCRIPTION
SUBSURFACE BUILDING DISCHARGE
SUBSURFACE BUILDING DISCHARGE
SUBSURFACE BUILDING DISCHARGE
SUMP
ABANDONED DRYWELL (POSSIBLY REMOVED)
BUILDING DISCHARGE
SOUTH WEST ABANDONED DRYWELL
SOUTH EAST ABANDONED DRYWELL
MAGNESIUM GRINDING AREA
SEPTIC DRAINFIELD
Summaries of all flndings;
The raw analytical data from all sampling activities during the reporting period and any
data from the previous reporting period which was not available at the time of reporting
is included.
During the reporting period, the following septic tanks associated with identified
SWMUs were opened, the contents removed, and the tank cleaned, inspected and filled:
DESCRIPTION
SEPTIC DRAINFIELD
LAUNDRY SUMP AND DRAINFIELD
SEPTIC DRAINFIELD SYSTEM
SEPTIC DRAINFIELD SYSTEM
SEPTIC DRAINFIELD SYSTEM
SEPTIC DRAINFIELD
SEPTIC DRAINFIELD
SEPTIC DRAINFIELD
Three new SWMUs have been identified during the reporting period. They are as
follows:
SWMU BUILDING DESCRIPTION
SWMU
191
465
626
627
628
629
630
667
BUILDING
A-002
M-002-1
M-002-2
M-002-3
M-019A
M-057
M-072
1-5
665
666
667
M-53
M-56
1-5
Subsurface Wastewater Discharge
Drywell
Septic Drainfield
•
A Solid Waste Management Unit Assessment Plan and/or proposal for corrective action
for each site has been included with this submittal.
3. Summaries of all changes made in the RCRA Facility Investigation during the
reporting period;
There were no changes made to the approved Work plans of the RFI.
4. Summaries of all contact with representatives of the local community, public
interest groups or State Government during the reporting period;
Correspondence regarding RFI activities has been limited to the Division of Solid and
Hazardous Waste and the Division of Water Quality.
5. Summaries of all problems or potential problems encountered during the reporting
period;
There were no significant problems encountered during the reporting period. As
discussed in previous reports, nearly all the remaining sites have some level of
uncertainty associated with them in terms of exact location, site accessibility, or safety
concems. Considerable effort has been made during the reporting period to resolve this
uncertainty.
6. Actions being taken to rectify problems;
Thiokol is reviewing all available information and interviewing personnel in a effort to
resolve the uncertainty associated with the remaining sites.
7. Changes in personnel during the reporting period;
There has been no change in coordination and project management for the RFI during
the reporting period. The current environmental staff will continue to conduct the
sampling when possible. Contractors will be used when ispecialized equipment is
required.
8. Projected work for the next reporting period;
Efforts will then focus on completing the investigation for the remaining sites and data
evaluation and report preparation.
9. Copies of daily reports, inspection reports, laboratory and monitoring data.
The raw analytical data from all sampling activities during the reporting period and any
data from the previous reporting period which was not avaiilable at the time of reporting
is included.
#
ENVIRONMENTAL LAB WORK REQUEST
« ™ THIOKOL ENVIRONMENTAL LABORATORY LWR No. El 1237
Login No.
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ORGANIZATION
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'^Pl (^ HELEN WARD, MS 301
S.AMPLE
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LOCATION
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REM.ARKS
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FOR LABORATORY USE ONL^
DATE COMPLETED DATE REPORTED
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Ftequested
•
#
Monday, September 16, 1996
TESTED FOR Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp,UT 84322
Frank Walker
Project: Solid Waste Mgmt Invest,
Login Number L480
Lab Number Client Number
Test Requested Description
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
301-863-5445
300-863-8080
L480-1 T-3 SURFACE SWMU 446
SW 846, 9045 pH Electrode Measurement
SW 846, 9056 Sulfate /Analysis by IC
SW-846, 3050 ICP/GF/^ Metals Digestion
SW-846, 6010 Pb ICP Metals Analysis (RCRA)
SW-846,6010 Sb ICP Metals Analysis (RCRA)
L480-2 T-3 2 FT. SWMU 446
SW 846, 9045 pH Electrode Measurement
SW 846, 9056 Sulfate Analysis by IC
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 6010 Sb ICP Metals Analysis (RCRA)
L480-3 M-53, MH SURFACE SWMU 228
SW 846, 9045 pH Electrode Measurement
SW-846. 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846, 6010 Cd ICP Metals Analysis (RCRA)
SW-846. 6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Cu ICP Metals Analysis (RCRA)
SW-846. 6010 Pb ICP Metals Analysis (RCRA)
SW-846. 6010 Zn ICP Metals Analysis (RCRA)
SW-646, 7471A CV Mercury Analysis (RCRA)
SW-846. 8260 Volatile Organics
L480-4 M-53, MH 2 FT. SWMU 228
SW 846, 9045 pH Electrode Measurement
SW-846, 3050 ICP/GFAA, Metals Digestion
SW-846, 6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846, 6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Cu ICP Metals Analysis (RCRA)
SW-846, 6010 Pb ICP Metals Analysis (RCRA)
SW-846,6010 Zn ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
Received
Matrix
Collect Date/Time
08/06/96
Soil
Soil
Soil
Soil
Soil
08/06/96
Soil
Soil
Soil
Soil
Soil
08/06/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
08/06/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
08/06/96 07:50
08/06/96 07:56
08/06/96 08:56
08/06/96 09:15
Page 1 of 6
•
Work Order Comments
There is a negative matrix interference for antimony in the rnatrix spike. The matrix spikes for
chromium, silver, and zinc indicate a large degree of nonhomogeneity in the L480-4 sample.
The actual results may be twice those reported.
Certified By Date
777/5 is to certify that the following samples were analyzed using good laboraton' practices to show
the folowing results:
0
•
Page 2 of 6
Listing of Results by Sample
#
1 Sample
1 Sample
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
ID: T-3 SURFACE
Test Parameter
PH
ICP/GFAA METALS DIGESTION
ANTIMONY
LEAD
ID: T-3 2 FT.
Test Parameter
PH
ICP/GFAA METALS DIGESTION
ANTIMONY
LEAD
ID: M-53, MH SURFACE
Test Parameter
PH
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
COPPER
LEAD
SILVER
ZINC
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4.TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBEN2ENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,S-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1.3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENT ANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
SWMU 446
Result
7.64
U
46
SWMU 446
Result
7.7
4.3
29
SWMU 228
Result
7.05
3
1700
210
714
107
2110
170
U
700
6.5 J
U
130
2.7 J
U
U
U
U
65
U
U
230
26
u
110
u
u
53
U
U
U
U
U
17
U
99 B
42
U
U
1.7 J
U
U
3.7 J
130
U
110
U
Units
ug/g
ug/g
Units
ug/g
ug/g
Units
ug/g
ug/g
ug/g
ug/g
ug'g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Det.
Limit
3.2
1.6
Det.
Limit
3.3
1.7
Det.
Umit
01
0 3
01
1.6
0.2
0.3
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
06
Lab ID:
Rep.
Limit
16
7.9
Lab ID:
Rep.
Limit
17
8.3
Lab ID:
Rep.
Limit
0.6
1.6
0.6
8.1
0.97
1.3
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
L480-1 Collect Date:
Dil.
F^aotor Mettiod
1
1
1
SW 846, 9045
SW-846, 3050
SW-846,6010
SW-846,6010
08/06/96 07:50
Analyst Test Date
MTB
KWB
KWB
KWB
L.480-2 Collect Date:
Dil.
Facl:or Method
1
1
1
SW 846, 9045
SW-846. 3050
SW-846. 6010
SW-846,6010
08/14/96 00:00
08/21/96 09:00
09/10/96 14:22
08/23/96 13:21
08/06/96 07:56
Analvst Test Date
MTB
KWB
KWB
KWB
L480-3 Collect Date:
Dil.
Facior Method
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
SW 846, 9045
SW-846, 3050
SW-846. 6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846. 6010
SW-846. 7471A
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
08/14/96 00:00
08/21/96 09:00
08/23/96 13:24
08/23/96 13:24
08/06/96 08:56
Analyst Test Date
MTB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
08/14/96 00:00
08/21/96 09:00
08/23/96 13:27
08/23/96 13:27
08/23/96 13:27
08/23/96 13:27
08/23/96 13:27
08/23/96 13:27
08/29/96 09:24
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/T!r96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13 41
08/13/96 13:41
Pages of6
•
156-59-4 CIS-1,2-DICHLOROETHENE
10061-01-5 CIS-1,3-DlCHLOROPROPENE
124-48-1 DIBROMOCHLOROMETHANE
74-95-3 DIBROMOMETHANE
75-71-8 DICHLORODIFLUOROMETHANE
100-41-4 ETHYLBENZENE
87-68-3 HEXACHLOROBUTADIENE
98-82-8 ISOPROPYLBENZENE
108-38-3 M,P-XYLENE
75-09-2 METHYLENE CHLORIDE
104-51-8 N-BUTYLBENZENE
103-65-1 N-PROPYLBENZENE
91-20-3 NAPHTHALENE
95-47-6 O-XYLENE
135-98-8 SEC-BUTYLBENZENE
100-42-5 STYRENE
98-06-6 TERT-BUTYLBENZENE
127-18-4 TETRACHLOROETHENE
108-88-3 TOLUENE
156-60-5 TRANS-1.2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
79-01-6 TRICHLOROETHENE
75-69-4 TRICHLOROFLUOROMETHANE
75-01-4 VINYL CHLORIDE
72
U
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
9 J ug/kg
1.5 J ug/kg
U ug/kg
340 ug/kg
9.6 JB ug/kg
U ug/kg
13
17
16
12
U
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
2.6 J ug/kg
100 ug/kg
230 ug/kg
4.1 J ug/kg
U ug/kg
66 ug/kg
U ug/kg
U ug/kg
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0,9
0.3
0.2
0.2
0.3
0.3
0.4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
I Sampli e ID: M-53, MH 2 FT. SWMU 228 Lab ID: L48i
Test Parameter
PH
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
COPPER
LEAD
SILVER
ZINC
MERCURY
630-20-6 1,1,1,2-TETRACHLOROETHANE
71-55-6 1,1,1-TRICHLOROETHANE
79-34-5 1,1,2,2-TETRACHLOROETHANE
79-00-5 1,1,2-TRICHLOROETHANE
75-34-3 1,1-DICHLOROETHANE
75-35-4 1,1-DICHLOROETHENE
563-58-6 1,1-DICHLOROPROPENE
87-61-6 1,2,3-TRICHLOROBENZENE
96-18-4 1,2,3-TRICHLOROPROPANE
120-82-1 1.2,4-TRICHLOROBENZENE
95-63-6 1,2,4-TRIMETHYLBENZENE
96-12-8 1,2-DlBROMO-3-CHLOROPROPAN
106-93-4 1,2-DIBROMOETHANE
95-50-1 1,2-DICHLOROBENZENE
107-06-2 1,2-DICHLOROETHANE
78-87-5 1,2-DICHLOROPROPANE
108-67-8 1,3,5-TRIMETHYLBENZENE
541-73-1 1,3-DICHLOROBENZENE
142-28-9 1,3-DICHLOROPROPANE
106-46-7 1,4-DICHLOROBENZENE
590-20-7 2,2-DICHLOROPROPANE
78-93-3 2-BUTANONE
95-49-8 2-CHLOROTOLUENE
591-78-6 2-HEXANONE
106-43-4 4-CHLOROTOLUENE
99-87-6 4-ISOPROPYLTOLUENE
108-10-1 4-METHYL-2-PENTANONE
67-64-1 ACETONE
71-43-2 BENZENE
108-86-1 BROMOBENZENE
74-97-5 BROMOCHLOROMETHANE
75-27-4 BROMODICHLOROMETHANE
75-25-2 BROMOFORM
Result Units
7.39
0.5
170
15
17
4.1
148
1.4
U
7.9 J
U
U
9.3 J
U
U
U
U
u
1.5 J
U
U
25
5.6 J
U
2 J
U
U
7.9 J
U
U
U
U
U
U
U
16 B
5.6 J
U
U
U
U
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Det.
Limit
0.1
0.3
0.1
17
0.2
0.3
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
Rep.
Limit
0.7
1.7
0.7
8.3
0.99
1.3
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Di
Fac
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846.
SW-846.
SW-846,
SW-846,
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8250
MMR
MMR
MMR
N«/IR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/95 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
08/13/96 13:41
0-4 Collect Date: 08/06/96 09:15
tor Method
SW 846, 9045
SW-846, 3050
SW-846. 6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846. 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
Analyst
MTB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Test Date
08/14/96 00:00
08/21/96 09:00
08/23/96 13:30
08/23/96 13:30
08/23/96 13:30
08/23/96 13:30
08/23/96 13:30
08/23/96 13:30
08/29/96 10:25
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/95 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
Page 4 of 6
•
74-83-9 BROMOMETHANE
56-23-5 CARBON TETRACHLORIDE
108-90-7 CHLOROBENZENE
75-00-3 CHLOROETHANE
67-66-3 CHLOROFORM
74-87-3 CHLOROMETHANE
156-59-4 CIS-1,2-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1 DIBROMOCHLOROMETHANE
74-95-3 DIBROMOMETHANE
75-71-8 DICHLORODIFLUOROMETHANE
100-41-4 ETHYLBENZENE
87-68-3 HEXACHLOROBUTADIENE
98-82-8 ISOPROPYLBENZENE
108-38-3 M,P-XYLENE
75-09-2 METHYLENE CHLORIDE
104-51-8 N-BUTYLBENZENE
103-65-1 N-PROPYLBENZENE
91-20-3 NAPHTHALENE
95-47-6 O-XYLENE
135-98-8 SEC-BUTYLBENZENE
100-42-5 STYRENE
98-06-6 TERT-BUTYLBENZENE
127-18-4 TETRACHLOROETHENE
108-88-3 TOLUENE
156-60-5 TRANS-1,2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
79-01-6 TRICHLOROETHENE
75-69-4 TRICHLOROFLUOROMETHANE
75-01-4 VINYL CHLORIDE
u
u
2.9 J
U
U
U
4.9 J
U
U
U
u
u
u
u
5.9 J
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.2 JB ug/kg
U
U
U
U
U
u
u
4.5 J
12
U
U
1.5 J
U
U
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
03
0 3
0.4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14-16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
08/13/96 14:16
Page 5 of 6
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detecied, or the compound was detected
but was below the detection limit.
B This flag is used when an analyte is found in the blank as well as the sample
Det. Limit Method Detection Limit (approximately three times the signal noise level)
Rep. Limit Reporting Limit is normally the value ofthe lowest standard run with the
analysis. The value is approximately 5 to 10 times the Method Detection Limit.
Dil. Factor Dilution Factor - The prepared sample was diluted by this factor because the
sample was too concentrated or due to other interferences in the sample matrix.
Any dilution factor causes an appropriate increase in the method detection limit
and reporting limit.
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This
flag is used either when estimating a concentration for tentatively identified compounds or
when the data indicated the presence of a compound that meets the identification criteria
but the result is less than the specified reporting limit (e.g. 3 J with a reporting limit of 10)
m
m
Page 6 of 6
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Requested
Friday, November 01,1996
TESTED FOR Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp,UT 84322
Frank Walker
Project: Solid Waste Mgmt Invest.
Login Number L539
Lab Number Client Number
Test Requested Description
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-5445
800-863-8080
Ffeceived
Matrix
Collect Date/Time
L539-1 #195GD#15 2FT. N. OF M-301 09/10/96 09/10/96 08:25
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L539-2 #195GD#15 5FT. N. OF M-301 09/10/96 09/10/96 08:35
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GF/^A Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L539-3 #195GD#39 2FT. N. OF M-301 09/10/96 09/10/96 09:00
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Page 1 of 25
L539-4 #195GD#39 5FT. N. OF M-301 09/10/96 09/10/96 09:12
•
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GF/VA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
L539-5 #195GD#86 2FT. N. OF M-301
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
L539-6 #195GD#86 5FT. N. OF M-301
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
L539-7 #195GD#99 2FT. N. OF M-301
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/10/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/10/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/10/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/10/96 09:38
09/10/96 09:46
09/10/96 10:44
•
Page 2 of 25
•
L539-8 #195GD#99 5FT. N. OF M-301 09/10/96 09/10/96 10:51
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L539-9 #195GD#99 5FT. DUP. N. OF M-301
SW-846, 8260 Volatile Organics
L539-10 #195GD#73 2FT. N. OF M-301
09/10/96
Soil
09/10/96
09/10/96 10:51
09/10/96 11:06
L539-11 #195GD#73 5FT. N. OF M-301 09/10/96 09/10/96 11:12
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L539-12 #195GD#178 2FT. N. OF M-301 09/10/96 09/10/96 11:33
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercuiy Analysis (RCRA)
Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Page 3 of 25
L539-13 #195GD#178 5FT. N. OF M-301 09/10/96 09/10/96 11:43
m
•
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
L539-14 #195GD#215 2FT. N. OF M-301
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GF/\A Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
L539-15 #195GD#215 2FTDUP. N. OF M-301
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
L539-16 #195GD#215 5FT. N. OF M-301
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
L539-17 #195GD#269 2FT. N. OF M-301
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/10/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/10/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/10/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/10/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/10/96 11:58
09/10/96 11.58
09/10/96 12:12
09/10/9612:27
Page 4 of 25
L539-18 #195GD#269 5FT. N. OF M-301 09/10/96 09/10/96 12:34
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
tii^KMm.
Certified By
V:^;^
bate
This is to certify that the following samples were analyzed using good laboratory practices to show
the folowing results:
•
Pages of 25
Listing of Results by Sample
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
ID:#195GD#15 2FT. N
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DlBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1.2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUT/VNONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
OF M-301
Result
u
u
04
8.9
U
0.4
0
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Units.
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1 JB ug/kg
U
U
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Det.
Limit
0.5
0.5
0.1
0.3
1.7
0.2
0.02
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
Lab ID:
Rep.
Limit
0.5
0.5
OJ
1.7
8.3
1
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
L5:39-1 Collect Date:
Dil.
Factor Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/10/96 08:25
Analyst Test Date
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/02/96 16:00
10/02/96 16:00
09/18/96 00:00
09/24/96 13:12
09/24/96 13:12
09/24/96 13:12
09/24/96 13:12
09/17/96 12:42
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/9611:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/9611:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/9611:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/9611:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
Page 6 of 25
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #195 GD#15 5 FT. N
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
U
U
U
U
U
U
U
OF M-301
Result
u
u
0.5
11
2.1
U
0
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.1 JB ug/kg
U
U
ug/kg
ug/kg
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
UmU
0.5
0.5
0.1
0.3
1.6
0.2
0.02
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.6
1.6
7.9
0.9
0.05
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
L539-2 Collect Date:
Dil.
Factor Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/11/96 11:15
09/10/96 08:35
Analyst Test Date
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
-MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
HfflVIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/02/96 16:07
10/02/96 16:07
09/18/96 00:00
09/24/96 13:15
09/24/96 13:15
09/24/96 13:15
09/24/96 13:15
09/17/96 12:46
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/9611:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/9611:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/9611:50
09/11/96 11:50
09/11/96 11:50
09/11/9611:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/9611:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
Page 7 of 25
•
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #195 GD#39 2 FT. N
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBEN2ENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
U
U
U
U
U
U
u
u
u
u
u
u
OF M-301
Result
u
u
0.5
12
U
0.4
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.6
0.2
0.02
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.6
1.6
7.8
0.9
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
' SW-846,8260
1 SW-846,8260
1 SW-846,8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
L539-3 Collect Date:
DII.
Factor Method
1 SOP 420
1 SOP 420
SW-846, 3050
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,7471A
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-S46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/11/96 11:50
09/10/96 09:00
Analyst Test Date
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/02/96 16:15
10/02/96 16:15
09/18/96 00.00
09/24/96 13:18
09/24/9613:18
09/24/96 13:18
09/24/96 13:18
09/17/96 12:50
09/11/96 12:25
09/11/96 12.25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/9612:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12.25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/9612:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
Page 8 of 25
•
•
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-O6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
IfcIRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
ID:#195GD#39 5FT. N
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBEN2ENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENT ANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
U
U
1.1
U
U
U
U
U
U
U
U
U
U
U
u
u
u
OF M-301
Result
u
u
u
11
u
0.3
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
JB ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.6
0.2
0.02
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.6
1.6
7.9
0.9
0.05
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
L53g-4 Collect Date:
Dil.
Factor Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/11/9612:25
09/11/9612:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/96 12:25
09/11/9612:25
09/11/96 12:25
09/11/96 12:25
09/11/9612:25
09/11/96 12:25
09/11/96 12:25
09/11/9612:25
09/11/96 12:25
09/11/96 12:25
09/10/96 09:12
Analyst Test Date
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
r^/MR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/02/96 16:22
10/02/96 16:22
09/18/96 00:00
09/24/9613:21
09/24/96 13:21
09/24/96 13:21
09/24/96 13:21
09/17/96 12:54
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/9613:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/9613:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13.00
09/11/96 13:00
09/11/96 13:00
09/11/9613.00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/9613:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/9613:00
09/11/96 13:00
09/11/9613:00
09/11/96 13:00
09/11/96 13:00
Page 9 of 25
#
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-6
10061-02-6
79-01-6
75-69-4
75-01-4
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
ID:#195GD#86 2FT. N
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,S-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
U
U
U
U
U
U
U
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.1 JB ug/kg
U
U
U
U
U
U
u
u
u
u
u
u
u
u
OF M-301
Result
u
u
u
11
u
0.2
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug'g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.6
0.2
0.02
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID: L5:
Rep. D
Limit Fai
0.5
0.5
0.6
1.6
8.1
0.97
0.05
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
;9-5 Collect Date:
1.
tor Method
SOP 420
1 SOP 420
SW-846, 3050
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
I SW-846,6010
1 SW-846,7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analys
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
- MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
I^R
MMR
09/11/9613:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/9613:00
09/11/96 13:00
09/11/9613:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/9613:00
09/11/96 13:00
09/11/9613:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/11/96 13:00
09/10/96 09:381
t Test Date
10/02/95 16:29
10/02/96 16:29
09/18/96 00:00
09/24/96 13:24
09/24/96 13:24
09/24/96 13:24
09/24/96 13:24
09/17/96 12:58
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/9613:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/9613:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
Page 10 of 25
•
#
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #195 GD#86 5 FT. N
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-O6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
OF M-301
Result
u
u
u
13
u
u
0
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.6
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.6
1.6
8.1
0.97
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
WAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
H*/IR
MMR
MMR
MMR
MMR
L53£i-6 Collect Date:
Dil
Factor Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/11/96 13:35
09/11/96 13:35
09/11/96 13.35
09/11/9613:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/9613:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/9613:35
09/11/96 13:35
09/11/9613:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/96 13:35
09/11/9613.35
09/11/96 13:35
09/10/96 09:46
Analyst Test Date
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/02/9616:44
10/02/96 16:44
09/18/96 00:00
09/24/96 13:26
09/24/96 13:26
09/24/96 13:26
09/24/96 13:26
09/17/9613:07
09/11/96 14:10
09/11/96 14:10
09/11/9614:10
09/11/96 14:10
09/11/9614:10
09/11/96 14.10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11796 14:10
09/11/96 14:10
09/11/96 14:10
09/11/9614.10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/9614:10
PageU of25
•
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #195 GD#99 2 FT. N
630-20-6
71-S5-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-1 fc 1KACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.2 JB ug/kg
U
U
U
U
U
U
U
U
U
U
U
U
u
u
OF M-301
Result
u
u
u
14
U
0.2
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.6
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.7
1.6
8.2
0.98
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
L53!9-7 Collect Date:
Dil.
Facitor Method
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
VMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/9614:10
09/11/96 14:10
09/11/9614:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/9614:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
09/11/96 14:10
D9/10/96 10:44
. Test Date
10/02/96 16:51
10/02/96 16:51
09/18/96 00:00
09/24/96 13:41
09/24/96 13:41
09/24/96 13:41
09/24/96 13:41
09/17/96 13:11
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/9614:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/9614:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
Page 12 Of 25
#
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
4-METHYL-2-PENT ANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMfc IHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #195 GD#9g 5 FT. N
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
7S-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.2 JB ug/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
OF M-301
Result
u
u
u
8.6
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.6
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.6
1.6
7.9
0.9
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
ti*/lR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
L539-8 Collect Date:
Dil,
Factor Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
09/11/96 14:45
09/11/9614:45
09/11/96 14:45
09/11/96 14:45
09/11/9614:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14.45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14.45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
09/11/96 14:45
39/10/9610:51
Analyst Test Date
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
^MR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/02/96 16:58
10/02/96 16:58
09/18/96 00:00
09/24/96 13:44
09/24/96 13:44
09/24/96 13:44
09/24/96 13:44
09/17/96 13.15
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15.20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/9615:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15.20
Page 13 of 25
•
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74^3-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #195 GD#g9 SFT. DUP. N
CAS
Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.1 JB ug/kg
U
U
U
U
U
U
U
U
U
U
u
u
u
u
OF M-301
Result
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
tJMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/9615:20
09/11/96 15:20
09/11/9615:20
09/11/9615:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/9615.20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/9615:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/96 15:20
09/11/9615:20
09/11/9615:20
09/11/96 15:20
L53S-g Collect Date: 09/10/96 10:51
Dil.
Fact'Dr Method
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
I^MR
MMR
MMR
. Test Date
09/11/9615.55
09/11/96 15:55
09/11/96 15:55
09/1T796 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/9615:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/9615:55
09/11/9615:55
09/11/96 15:55
09/11/96 15:55
Page 14 of 25
•
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #195 GD#73 2 FT. N
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
OF M-301
Result
u
u
0.2
11
u
0.2
0.04
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.5
0.5
0.1
0.3
1.6
0.2
0.02
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.6
1.6
7.8
0.9
0.05
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
NfflVIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/9615:55
09/11/9615:55
09/11/96 15:55
09/11/9615:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/9615:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/9615:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/9615:55
09/11/9615:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
09/11/96 15:55
L53:3-10 Collect Date: 09/10/96 11:06
Dill.
Facitor Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
Analvsl
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
NflvflR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Test Date
10/02/96 17:06
10/02/96 17:06
09/18/96 00:00
09/24/96 13:46
09/24/96 13:46
09/24/96 13:46
09/24/96 13:46
09/17/96 13:19
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/9616:30
09/11/9616:30
09/11/96 16:30
09/11/96 16:30
09/11/9616:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
Page 15 of 25
•
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74^7-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #195 GD#73 5 FT. N
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1.2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.1 JB ug/kg
U
U
U
U
U
U
U
U
U
U
U
U
u
u
OF M-301
Result
u
u
u
9.4
U
U
0
U
U
U
U
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.6
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.6
1.6
8
0.96
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/9616:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/9616.30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
09/11/96 16:30
L539-11 Collect Date: 09/10/96 11:12
Dil.
Factor Method
1 SOP 420
1 SOP 420
SW-846, 3050
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,7471A
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
Analysi
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Test Date
10/02/96 17:13
10/02/96 17:13
09/18/96 00:00
09/24/96 13:49
09/24/96 13:49
09/24/96 13:49
09/24/96 13:49
09/17/96 13:34
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
Page 16 of 25
n
#
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON 1 b 1RACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #195 GD#178 2 FT. N.
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.1 JB ug/kg
U
U
U
u
u
u
u
u
u
u
u
u
u
u
OF M-301
Result
u
u
u
14
U
0.4
0
U
U
U
U
U
U
U
U
U
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.6
0.2
0.02
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.7
1.6
8.2
0.98
0.05
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/9617:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17.05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/9617:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/9617:05
09/11/9617:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
09/11/96 17:05
L539-12 Collect Date: 09/10/96 11:33
Dil.
Factor Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Test Date
10/02/96 17:20
10/02/96 17:20
09/18/96 00:00
09/24/96 14:06
09/24/96 14:06
09/24/96 14:06
09/24/96 14:06
09/17/96 13:38
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
Page 17 Of 25
0
d
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
i08-8&-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
Tfc FRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #195 GD#178 5 FT. N
630-20-6
71-55-6
79-34-5
79-00-5
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
1.7 J
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugfl(g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.2 JB ug/kg
U
U
U
U
U
U
U
U
U
U
U
U
u
u
OF M-301
Result
u
u
0.2
25
U
U
0
U
U
U
U
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.7
0.2
0.01
0.2
0.2
0.3
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.7
1.7
8.3
0.99
0.04
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-&46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
lUWR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/11/96 17:40
09/11/96 17:40
09/11/9617:40
09/11/96 17:40
09/11/9617.40
09/11/96 17:40
09/11/96 17:40
09/11/9617:40
09/11/9617:40
09/11/96 17:40
09/11/9617:40
09/11/96 17:40
09/11/96 17:40
09/11/9617:40
09/11/96 17.40
09/11/9617:40
09/11/96 17:40
09/11/96 17:40
09/11/9617:40
09/11/96 17:40
09/11/9617:40
09/11/9617:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/9617.40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/9617:40
09/11/9617:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
09/11/9617:40
09/11/96 17:40
09/11/96 17:40
09/11/96 17:40
L539-13 Collect Date: 09/10/96 11:43
Dil.
FactiDr Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
Test Date
10/02/96 17:28
10/02/96 17:28
09/18/96 00:00
09/24/96 14:09
09/24/96 14:09
09/24/96 14:09
09/24/96 14:09
09/17/96 13:42
09/11/9618:15
09/11/96 18:15
09/11/96 18:15
09/11/9618:15
Page 18 of 25
•
75-34-3
75-35-4
S63-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #195 GD#215 2 FT. N
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1 JB ug/kg
U
U
U
U
U
U
U
U
U
U
U
U
u
u
OF M-301
Result
u
u
0.1
14
U
0.3
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.6
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.7
1.6
8.2
0.98
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
t SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/9618:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/9618:15
09/11/96 18:15
09/11/9618:15
09/11/96 18:15
09/11/96 18:15
09/11/9618:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/9618.15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/9618:15
09/11/96 18:15
09/11/9618:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
09/11/96 18:15
L539-14 Collect Date: 09/10/96 11:58
Dil.
Factor Method
1 SOP 420
1 SOP 420
SW-846, 3050
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
Analyst
KMS
KMS
KWB
KWB
KWB
KWB
KWB
Test Date
10/02/96 17:35
10/02/96 17:35
09/18/96 00:00
09/24/96 14:12
09/24/96 14:12
09/24/96 14:12
09/24/96 14:12
Page 19 Of 25
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #195 GD#215 2FT DUP. N.
Test Parameter
HMX
NITROGLYCERIN
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.2 JB ug/kg
U
U
U
U
u
u
u
u
u
u
u
u
u
u
OF M-301
Result.
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
KEN
MMR
MMR
MMR
MMR
I^IMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/17/96 13:47
09/11/9618:50
09/11/9618:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/9618:50
09/11/96 18.50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/9618:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/9618.50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/9618:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/9618.50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/9618:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/9618:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
09/11/96 18:50
L539-15 Collect Date: 09/10/96 11:58
Dil.
Facte
1
1
r Method.
SOP 420
SOP 420
Analyst
KMS
KMS
Test Date
10/02/96 17:42
10/02/96 17:42
Page 20 of 25
#
1 Sample
630-20-6
71-55-6
79-34-S
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
ID:#195GD#215 5FT. N
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
0.4
14
U
U
U
OF M-301
Result
u
u
0.6
15
U
U
0
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/g
ug'g
ug/g
ug/g
ug/g
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.2 JB ug/kg
U
U
U
ug/kg
ug/kg
ug/kg
0.1
0.3
1.6
0.2
0.01
Det.
Limit
0.5
0.5
0.1
0.3
1.5
0.2
0.02
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.6
1.6
7.9
0.9
0.04
Lab ID:
Rep.
Limit
0.5
0.5
0.6
1.5
7.6
0.9
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 7471A
KWB
KWB
KWB
KWB
KWB
KEN
L.539-16 Collect Date:
Dil.
Fad: }r Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/18/96 00:00
09/24/96 14:14
09/24/96 14:14
09/24/96 14:14
09/24/96 14:14
09/17/96 13:51
09/10/9612:12
Analyst Test Date
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
-MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/02/96 17:50
10/02/96 17:50
09/18/96 00:00
09/24/96 14:17
09/24/96 14:17
09/24/96 14:17
09/24/96 14:17
09/17/9613:59
09/11/96 19:25
09/11/96 19:25
09/11/9619:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/9619:25
09/11/96 19:25
09/11/96 19:25
09/11/9619:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/9619:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/9619:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
Page 21 of 25
#
#
•
95-47-6 O-XYLENE
135-98-8 SEC-BUTYLBENZENE
100-42-5 STYRENE
98-06-6 TERT-BUTYLBENZENE
127-18-4 TETRACHLOROETHENE
108-88-3 TOLUENE
156-60-5 TRANS-1,2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
79-01-6 TRICHLOROETHENE
75-69-4 TRICHLOROFLUOROMETHANE
75-01-4 VINYL CHLORIDE
U
U
U
U
U
U
U
U
U
U
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
10
10
10
10
10
10
10
10
10
10
10
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
09/11/96 19:25
Sample ID: #195 GD#269 2 FT. N. OF M-301 Lab ID: L539-17 Collect Date: 09/10/96 12:27
Det. Rep.
Test Parameter Result Units Limit Limit
HMX U ug/g 0.5 0.5
NITROGLYCERIN U ug/g 0.5 0.5
ICP/GFAA METALS DIGESTION
CADMIUM 0.5 ug/g 0.1 0.6
CHROMIUM 16 ug/g 0.3 1.6
LEAD 24 ug/g 16 7.8
SILVER U ug/g 0.2 0.9
MERCURY 0.02 ug/g 0.01 0.04
630-20-6 1,1,1,2-TETRACHLOROETHANE U ug/kg 0.2 10
71-55-6 1,1,1-TRICHLOROETHANE U ug/kg 0.2 10
79-34-5 1,1,2,2-TETRACHLOROETHANE U ug/kg 0.3 10
79-00-5 1,1,2-TRICHLOROETHANE U ug/kg 0.2 10
75-34-3 1,1-DICHLOROETHANE U ug/kg 0.1 10
75-35-4 1,1-DICHLOROETHENE U ug/kg 0.6 10
563-58-6 1,1-DICHLOROPROPENE U ug/kg 0.2 10
87-61-6 1,2,3-TRICHLOROBENZENE U ug/kg 0.2 10
96-18-4 1,2,3-TRICHLOROPROPANE U ug/kg 0.2 10
120-82-1 1,2,4-TRICHLOROBENZENE U ug/kg 0.2 10
95-63-6 1,2,4-TRIMETHYLBENZENE U ug/kg 0.2 10
96-12-8 1,2-DIBROMO-3-CHLOROPROPAN U ug/kg 0.2 10
106-93-4 1,2-DIBROMOETHANE U ug/kg 0.2 10
95-50-1 1,2-DICHLOROBENZENE U ug/kg 0.1 10
107-06-2 1,2-DICHLOROETHANE U ug/kg 0.2 10
78-87-5 1,2-DICHLOROPROPANE U ug/kg 0.2 10
108-67-8 1,3,5-TRIMETHYLBENZENE U ug/kg 0.2 10
541-73-1 1,3-DICHLOROBENZENE U ug/kg 0.2 10
142-28-9 1,3-DICHLOROPROPANE U ug/kg 0.2 10
106-46-7 1,4-DICHLOROBENZENE U ug/kg 0.2 10
590-20-7 2,2-DICHLOROPROPANE U ug/kg 0.2 10
78-93-3 2-BUTANONE U ug/kg 10 10
95-49-8 2-CHLOROTOLUENE U ug/kg 0.2 10
591-78-6 2-HEXANONE U ug/kg 10 10
106-43-4 4-CHLOROTOLUENE U ug/kg 0.2 10
99-87-6 4-ISOPROPYLTOLUENE U ug/kg 0.2 10
108-10-1 4-METHYL-2-PENTANONE U ug/kg 10 10
67-64-1 ACETONE 12 B ug/kg 10 10
71-43-2 BENZENE U ug/kg 0.2 10
108-86-1 BROMOBENZENE U ug/kg 0.2 10
74-97-5 BROMOCHLOROMETHANE U ug/kg 0.2 10
75-27-4 BROMODICHLOROMETHANE U ug/kg 0.3 10
75-25-2 BROMOFORM U ug/kg 0.1 10
74-83-9 BROMOMETHANE U ug/kg 0.4 10
56-23-5 CARBON TETRACHLORIDE U ug/kg 0.3 10
108-90-7 CHLOROBENZENE U ug/kg 0.2 10
75-00-3 CHLOROETHANE U ug/kg 0.4 10
67-66-3 CHLOROFORM U ug/kg 0.4 10
74-87-3 CHLOROMETHANE U ug/kg 0.6 10
156-59-4 CIS-1,2-DICHLOROETHENE U ug/kg 0.2 10
10061-01-5 CIS-1,3-DICHLOROPROPENE U ug/kg 0.2 10
124-48-1 DIBROMOCHLOROMETHANE U ug/kg 0.3 10
74-95-3 DIBROMOMETHANE U ug/kg 0.2 10
75-71-8 DICHLORODIFLUOROMETHANE U ug/kg 0.2 10
100-41-4 ETHYLBENZENE 1.8 J ug/kg 0.3 10
87-68-3 HEXACHLOROBUTADIENE U ug/kg 0.2 10
98-82-8 ISOPROPYLBENZENE U ug/kg 0.2 10
Dil.
Fagtor Method Analvst Test Date
SOP 420 KMS 10/02/96 18:04
SOP 420 KMS 10/02/9618:04
SW-846,3050 KWB 09/18/96 00:00
SW-846,6010 KWB 09/24/96 14:31
SW-846,6010 KWB 09/24/96 14:31
SW-846,6010 KWB 09/24/96 14:31
SW-846,6010 KWB 09/24/96 14:31
SW-846,7471A KEN 09/17/9614:03
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846, 8260 MMR 09/11/96 20:00
SW-S46, 8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846, 8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
SW-846, 8260 MMR 09/11/96 20:00
SW-846,8260 MMR 09/11/96 20:00
Page 22 of 25
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
D:#195GD#269 5FT. N
Test Parameter
HMX
NITROGLYCERIN
ICP/GF/iiA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRlCHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
9.1 J ug/kg
1.1 JB ug/kg
U
U
U
4.1 J
U
U
U
U
U
U
U
U
U
U
OF M-301
Result
u
u
0.3
15
3.3
U
0.02
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug'g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.5
0.2
0.02
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.6
1.5
7.5
0.9
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
L539-18 Collect Date:
Diii.
Fac:tor Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
SW-fi46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/11/96 20:00
09/11/96 20.00
09/11/96 20:00
09/11/96 20:00
09/11/96 20:00
09/11/96 20.00
09/11/96 20:00
09/11/96 20:00
09/11/96 20.00
09/11/96 20:00
09/11/96 20:00
09/11/96 20:00
09/11/96 20:00
09/11/96 20:00
09/11/96 20:00
09/11/96 20.00
09/10/96 12:34
Analvst Test Date
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/02/96 18:26
10/02/96 18:26
09/18/96 00:00
09/24/96 14:34
09/24/96 14:34
09/24/96 14:34
09/24/96 14.34
09/17/96 14:08
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
Page 23 of 25
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
U
U
U
U
U
3.1 J
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.1 JB ug/kg
U
U
U
1.4 J
U
U
U
U
U
U
U
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
•\ SW-846,8260
•I SW-846,8260
1 SW-846,8260
11 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
09/11/96 20:35
^
0
Page 24 of 25
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected
but was below the detection limit.
B This flag is used when an analyte is found in the blank as well as the sample
Det. Limit Method Detection Limit (approximately three times the signal noise level)
Rep. Limit Reporting Limit is normally the value of the lowest standard run with the
analysis. The value is approximately 5 to 10 times the Method Detection Limit.
Dil. Factor Dilution Factor - The prepared sample was diluted by this factor because the
sample was too concentrated or due to other interferences in the sample matrix.
Any dilution factor causes an appropriate increase in the method detection limit
and reporting limit.
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This
flag is used either when estimating a concentration for tentatively identified compounds or
when the data indicated the presence of a compound that meets the identification criteria
but the result is less than the specified reporting limit (e.g. 3 J with a reporting limit of 10)
#
^
Page 25 of 25
m CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Flequested
Friday, November 01,1996
m
^
TESTED FOR Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp,UT 84322
Frank Walker
Project: Solid Waste Mgmt Invest.
Login Number L544
Lab Number Client Number
Test Requested Description
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-5445
800-863-8080
L544-1 #233, GD221 2FT. E. OF M-303
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
cv Mercury Analysis (RCRA)
Volatile Organics
L544-2 #233, GD221 SFT. E. OF M-303
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-B46, 6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
L544-3 #233, GD280 2FT. E. OF M-303
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
1CP/GF/\A Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
Received
Matrix
Collect Date/Time
09/11/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/9615:20
09/11/96 15:30
09/11/9614:25
Page 1 of 29
L544-4 #233, GD280 SFT. E. OF M-303 09/11/96 09/11/96 14:48
•
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846, 6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
L544-5 #233, GD340 2FT. E. OF M-303
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
L544-6 #233, GD340 SFT. E. OF M-303
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GF/\A Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
L544-7 #233, GD140 2FT. E. OF M-303
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GF/VA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/96 14:05
09/11/96 14:12
09/11/96 08:40
Page 2 of 29
L544-8 #233, GDI 40 SFT. E. OF M-303 09/11/96 09/11/96 08:50
#
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GF/ivA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
LS44-9 #233, GD112 2FT. E. OF M-303
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
LS44-10 #233, GD112 5FT. E. OF M-303
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GF/VA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
L544-11 #233, GD55 2FT. E. OF M-303
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
1CP/GF/\A Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/96 09:22
09/11/96 09:30
09/11/96 09:55
#
Page 3 of 29
L544-12 #233, GD5S SFT. E. OF M-303 09/11/96 09/11/96 10:02
H
9
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GF/\A Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
LS44-13 #233, GD459 2FT. E. OF M-303
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GF/ivA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
L544-14 #233, GD459 SFT. E. OF M-303
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
L544-15 #233, GD399 2FT. E. OF M-303
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Melals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
LS44-16 #233, GD399 2FT. DUP E. OF M-303
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 6010
SW-846, 7471A
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/96 11:06
09/11/96 11:33
09/11/9611:50
09/11/96 11:50
Page 4 of 29
L544-17 #233, GD399 SFT. E. OF M-303 09/11/96 09/11/96 12:02
•
0
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846, 6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
1CP/GF/\A Metals Digestion
Ag iCP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
L544-18 #233, GD431 2FT. E. OF M-303
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
L544-19 #233, GD431 SFT. E. OF M-303
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
L544-20 #233, GDS12 2FT. E. OF M-303
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/11/96 13:30
09/11/96 13:43
09/11/96 14:02
Page 5 of 29
L544-21 #233, GD512 5FT. E. OF M-303 09/11/96 09/11/9614:20
•
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
HPLC Analysis HMX
HPLC Analysis for NG
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
ii/^h(-
Date
This is to certify that the following samples were analyzed using good laboratory practices to show
the folowing results:
Page 6 of 29
Listing of Results by Sample
•
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
ID: #233, GD221 2FT. E.
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
OF M-303
Result
u
u
0.2
11
u
0.7
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.1 JB ug/kg
U
U
U
U
U
U
U
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Det.
Limit
0.5
0.5
0.1
0.3
1.7
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
Lab ID:
Rep.
Limit
0.5
0.5
0.7
1.7
8.3
1
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
L54.*-1 Collect Date:
Oil.
Factor Method.
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/11/96 15:20
Analyst Test Date
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/10/96 16:43
10/10/96 16:43
09/18/96 00:00
09/24/96 14:37
09/24/96 14:37
09/24/96 14:37
09/24/96 14:37
09/17/96 10:44
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12.58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12.58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/9612:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
Page 7 of 29
#
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59^
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
0: #233, GD221 SFT. E.
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
U
U
U
u
u
u
u
OF M-303
Result
u
u
0.3
11
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.6
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.6
1.6
7.9
0.9
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
L5^l4-2 Collect Date:
Oil.
Factor Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12:58
09/13/96 12.58
09/11/96 15:30
Analvst Test Date
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Hfll/1R
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
luMR
MMR
MMR
10/10/96 17:06
10/10/96 17:06
09/18/96 00:00
09/24/96 14:40
09/24/96 14:40
09/24/96 14:40
09/24/96 14:40
09/17/96 10:48
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/9613:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/9613:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/9613:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
Page 8 of 29
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
ID: #233, GD280 2FT. E.
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROP/VN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
U
U
U
U
U
U
U
U
U
U
U
U
OF M-303
Result
u
u
0.5
16
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ugfltg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.6
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
10
10
10
10
10
10
10
10
10
10
10
10
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Lab ID: L54^)-3 Collect Date:
Rep. Oil.
Liinit Factor Method
0.5
0.5
0.6
1.6
7.8
0.9
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10
10
10
10
10 1
10 1
10
10 1
10 1
10 1
10 1
10.
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10
10 1
1 SOP 420
1 SOP 420
SW-846, 3050
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 • SW-846, 7471A
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/96 13:33
09/13/9613:33
09/13/96 13:33
09/11/9614:25
Analyst Test Date
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
fJMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/10/96 17:14
10/10/96 17:14
09/18/96 00:00
09/24/96 14:43
09/24/96 14:43
09/24/96 14:43
09/24/96 14:43
09/17/96 10:52
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15.27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/9615:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15.27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15.27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
Page 9 of 29
#
#
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06*
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
D: #233, GD280 SFT. E.
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,S-TR1METHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
OF M-303
Result
u
u
0.7
11
3.1
U
0
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug'g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/l(g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.4
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
04
0.4
0.6
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.6
1.4
7
0.8
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
L544-4 Collect Date:
Oil.
Factor Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/12/9615:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/9615:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/12/96 15:27
09/11/96 14:48
Analvst Test Date
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MU1R
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
-MMR
ry«viR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
tJMR
MMR
MMR
MMR
MMR
10/10/96 17:22
10/10/96 17:22
09/26/96 00:00
09/25/96 12:00
09/25/96 12:00
09/25/96 12:00
09/25/9612:00
09/17/96 11:01
09/12/96 16:02
09/12/96 16:02
09/12/96 16.02
09/12/96 16:02
09/12/96 16:02
09/12/96 16.02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/9616:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16.02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
Page 10 of 29
o
#
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
984)6-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
1 fcIRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #233, GD340 2FT.
630-20-6
71-55-6
79-34^5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-S
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-6
108-90-7
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACtIONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
E. OF M-303
Result
u
u
1
13
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.5
0.2
0.02
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.6
1.5
7.5
0.9
0.05
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW.-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
r^R
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
L54'l-5 Collect Date:
Dil.
Facior Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/9616:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16.02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/96 16:02
09/12/9616:02
09/12/96 16:02
39/11/96 14.05
Analyst Test Date
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/10/96 17:30
10/10/96 17:30
09/26/96 00:00
09/25/96 12:03
09/25/96 12:03
09/25/96 12:03
09/25/9612:03
09/17/96 11:05
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16.37
09/12/96 16:37
09/12/9616:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/9616:37
09/12/96 16:37
Pagell of29
•
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156*0-5
10061-02-6
79-01-6
75-69-4
75-01-4
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
0: #233, GD340 SFT. E.
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CAOMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2.4-TRICHLOROBENZENE .
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
U
U
U
U
U
U
u
u
1.2 J
U
U
5.8 J
U
U
U
U
2.2 J
U
U
U
U
U
U
U
U
U
U
OF M-303
Result
u
u
0.9
15
U
0.3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/l(g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.3
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.5
1.3
6.4
0.8
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
IWMR
MMR
N*/IR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
LS4'l-6 Collect Date:
Dil.
Factor Method
SOP 420
SOP 420
SW-846, 3050
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/9616:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/9616:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/12/96 16:37
09/11/9614:12
Analyst Test Date.
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/10/96 17:38
10/10/96 17:38
09/26/96 00:00
09/25/96 12:06
09/25/96 12:06
09/25/96 12:06
09/25/96 12:06
09/17/96 11:09
09/12/96 17:12
09/12/96 17:12
09/12/9617:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/9617:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/9617:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/9617:12
09/12/96 17:12
09/12/9617:12
09/12/96 17:12
09/12/96 17:12
09/12/9617:12
09/12/96 17:12
Page 12 of 29
#
llll
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-6
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #233, GD140 2FT. E.
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1 JB ug/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
OF M-303
Result
u
u
0.9
14
U
U
0.02
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.5
0.5
0.1
0.3
1.5
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.6
1.5
7.4
0.9
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-&46, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-646, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
lt«/IR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
L544-7 Collect Date:
Dil.
Fact; )r Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
09/12/9617:12
09/12/96 17:12
09/12/96 17:12
09/12/9617:12
09/12/96 17:12
09/12/9617:12
09/12/96 17:12
09/12/9617:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/9617:12
09/12/96 17:12
09/12/9617:12
09/12/96 17:12
09/12/9617:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/9617:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
09/12/96 17:12
39/11/96 08:40
Analyst Test Date
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
-WWR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
WWR
MMR
MMR
MMR
MMR
10/10/96 17:45
10/10/96 17:45
09/26/96 00:00
09/25/96 12:09
09/25/96 12:09
09/25/96 12:09
09/25/96 12:09
09/17/9611:13
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/9617:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
Page 13 of 29
108-10-1
67-64-1 •
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74*3-9
56-23-5
108-90-7
75-00-3
67-66-3
74*7-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
ClS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
. TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #233, GDI 40 SFT. E.
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67*
541-73-1
142-28-9
106-46-7
590-20-7
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.1 JB ug/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
OF M-303
Result.
u
u
0.6
17
U
U
0.02
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugfltg
ug/kg
ug/kg
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.4
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit.
0.5
0.5
0.6
1.4
7.1
0.9
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-*46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
LS4'l-8 Collect Date:
Oil,
Factor Method
SOP 420
SOP 420
SW-846,3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 7471A
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/12/96 17:47
09/12/96 17:47
09/12^617:47
09/12/96 17:47
09/12/9617:47
09/12/96 17:47
09/12/96 17:47
09/12/9617:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/9617:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/96 17:47
09/12/9617:47
09/12/96 17:47
09/12/9617:47
09/12/96 17:47
09/12/96 17:47
09/12/9617:47
09/12/96 17:47
09/12/96 17:47
39/11/96 08:50
. Test Date.
10/10/96 17:53
10/10/96 17:53
09/26/96 00:00
09/25/96 12:12
09/25/96 12:12
09/25/96 12:12
09/25/96 12:12
09/17/96 11:18
09/12796 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/9618:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/9618:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
Page 14 Of 29
0
i^
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01*
75-69-4
75-01-4
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #233, GD112 2FT. E
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87*1-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.1 JB ug/kg
U
U
U
U
U
U
u
u
u
u
u
u
u
u
OF M-303
Result
U
u
0.6
16
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/l(g
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.5
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.6
1.5
7.4
0.9
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MAR
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/96 18:22
09/12/9618:22
09/12/96 18:22
L544-9 Collect Date: 09/11 /96 09:22
Dil.
Factor Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Test Date
10/10/96 18:09
10/10/96 18:09
09/26/96 00:00
09/25/9612:26
09/25/96 12:26
09/25/96 12:26
09/25/9612:26
09/17/96 11:26
09/12/9618:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
Page 15 Of 29
0
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78*
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74*3-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98*2*
108-38-3
75-09-2
104-51-8
103*5-1
91-20-3
95-47-6
135-98-8
10(M2-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENT ANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE.
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #233, GD112 SFT.
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61*
96-18-4
120-82-1
95-63-6
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-1 fc rRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugflcg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1 JB ug/kg
U
U
U
U
U
U
U
U
U
U
U
4.2 J
U
U
E. OF M-303
Result
u
u
1.1
18
2.5
U
u
U
U
U
U
U
U
U
U
U
U
U
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/lcg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.5
0.2
0.02
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.6
1.5
7.4
0.9
0.05
10
10
10
10
10
10
10
10
10
10
10
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
-.1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-fi46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW*46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-a46,8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/12/96 18:57
09/12/9618:57
09/12/96 18:57
09/12/96 18:57
09/12/9618:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/9618:57
09/12/9618:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18.57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18.57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/9618:57
09/12/96 18:57
09/12/96 18:57
09/12/9618:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
09/12/96 18:57
L544-10 Collect Date: 09/11 /96 09:30
Dil.
Factor Method
1 SOP 420
1 SOP 420
SW-846, 3050
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,7471A
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
Analyst
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Test Date
10/10/96 18:17
10/10/96 18:17
09/26/96 00:00
09/25/96 12:29
09/25/96 12:29
09/25/96 12:29
09/25/96 12:29
09/17/96 11:30
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/9619:32
09/12/9619:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
Page 16 Of 29
0
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87*
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74*3-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47^
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
ClS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #233, GDSS 2FT. E
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
U
U
U
u
u
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugrttg
ug/kg
ug/kg
ug/kg
1 JB ug/kg
U
U
U
U
U
U
U
U
U
u
u
4.6 J
u
u
OF M-303
Result
u
u
0.98
13
4.6
U
U
U
U
U
U
U
U
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.5
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab 10:
Rep.
Limit
0.5
0.5
0.6
1.5
7.3
0.9
0.04
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-646, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MAR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/12/96 19:32
09/12/9619:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/9619:32
09/12/96 19:32
09/12/96 19:32
09/12/9619:32
09/12/96 19:32
09/12/96 19:32
09/12/9619:32
09/12/96 19:32
09/12/96 19:32
09/12/9619:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/9619:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19.32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/9619:32
09/12/96 19:32
09/12/9619:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/9619:32
09/12/9619:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12/96 19:32
09/12r96 19:32
09/12/96 19:32
09/12/96 19:32
L544-11 Collect Date: 09/11 /96 09:55
Dil.
Factor Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
Test Date
10/10/96 18:25
10/10/96 18:25
09/26/96 00:00
09/25/96 12:31
09/25/96 12:31
09/25/96 12:31
09/25/96 12:31
09/17/96 11:39
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20.07
09/12/96 20.07
Page 17 Of 29
#
#
563-58-6
87*1-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-piCHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #233, GDSS SFT. E.
630-20-6
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1 JB ug/kg
U
U
U
U
u
u
u
u
u
u
u
u
u
u
OF M-303
Result
u
u
1.1
12
2.1
U
U
U
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.5
0.5
0.1
0.3
1.4
0.2
0.01
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.6
1.4
7.2
0.9
0.04
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846.8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20.07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12^6 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20.07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
09/12/96 20:07
L544.12 Collect Date: 09/11 /96 10:02
Dil.
Factor Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
Analyst
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
Test Date
10/10/96 18:32
10/10/96 18:32
09/26/96 00:00
09/25/96 12:34
09/25/96 12:34
09/25/96 12:34
09/25/96 12:34
09/17/9611:43
09/12/96 20:42
Page 18 of 29
m
#
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74*7-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
10O-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #233, GD4S9 2FT. E.
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1 JB ug/kg
u
u
u
u
u
u
u
u
u
u
u
u
u
u
OF M-303
Result
u
u
0.5
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug'g
ug/g
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.5
0.5
0.1
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
Lab ID: L54
Rep. D
Limit Fac
0.5 1
0.5 1
0.6
1 SW-846,8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW*46,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-&46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20.42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
09/12/96 20:42
14-13 Collect Date: 09/11 /96 11:06
1.
toir Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
Analyst
KMS
KMS
KWB
KWB
Test Date
10/10/96 18:40
10/10/96 18:40
09/26/96 00:00
09/25/96 12:37
Page 19 Of 29
#
CHROMIUM
LEAD
SILVER
MERCURY
630-20* 1,1,1,2-TETRACHLOROETHANE
71-55-6 1,1,1-TRICHLOROETHANE
79-34-5 1,1,2,2-TETRACHLOROETHANE
79-00-5 1,1,2-TRICHLOROETHANE
75-34-3 1,1-DICHLOROETHANE
75-35-4 1,1 -DICHLOROETHENE
563-58-6 1,1-DICHLOROPROPENE
87-61* 1,2,3-TRICHLOROBENZENE
96-18-4 1,2,3-TRICHLOROPROPANE
120-82-1 1,2,4-TRICHLOROBENZENE
95-63-6 1,2,4-TRIMETHYLBENZENE
96-12* 1,2-DIBROMO-3-CHLOROPROPAN
106-93-4 1,2-DIBROMOETHANE
95-50-1 1,2-DICHLOROBENZENE
107-06-2 1,2-DICHLOROETHANE
78-87-5 1,2-DICHLOROPROPANE
108-67* 1,3,5-TRIMETHYLBENZENE
541-73-1 1,3-DICHLOROBENZENE
142-28-9 1,3-DICHLOROPROPANE
106-46-7 1,4-DICHLOROBENZENE
590-20-7 2,2-DICHLOROPROPANE
78-93-3 2-BUTANONE
95-49-8 2-CHLOROTOLUENE
591-78-6 2-HEXANONE
106-43-4 4-CHLOROTOLUENE
99-87-6 4-ISOPROPYLTOLUENE
108-10-1 4-METHYL-2-PENTANONE
67-64-1 ACETONE
71-43-2 BENZENE
108-86-1 BROMOBENZENE
74-97-5 BROMOCHLOROMETHANE
75-27-4 BROMODICHLOROMETHANE
75-25-2 BROMOFORM
74-83-9 BROMOMETHANE
56-23-5 CARBON TETRACHLORIDE
108-90-7 CHLOROBENZENE
75-00-3 CHLOROETHANE
67-66-3 CHLOROFORM
74-87-3 CHLOROMETHANE
156-59-4 CIS-1,2-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1 DIBROMOCHLOROMETHANE
74-95-3 DIBROMOMETHANE
75-71-8 DICHLORODIFLUOROMETHANE
100-41-4 ETHYLBENZENE
87-68-3 HEXACHLOROBUTADIENE
98-82-8 ISOPROPYLBENZENE
108-38-3 M,P-XYLENE
75-09-2 METHYLENE CHLORIDE
104-51-8 N-BUTYLBENZENE
103-65-1 N-PROPYLBENZENE
91-20-3 NAPHTHALENE
95-47* O-XYLENE
135-98-8 SEC-BUTYLBENZENE
100-42-5 STYRENE
98-06-6 TERT-BUTYLBENZENE
127-18-4 TETRACHLOROETHENE
108-88-3 TOLUENE
156-60-5 TRANS-1,2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
79-01-6 TRICHLOROETHENE
75-69-4 TRICHLOROFLUOROMETHANE
75-01-4 VINYL CHLORIDE
20
2.7
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
1.8 J
u
u
11
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1 JB ug/kg
U
U
U
4.8 J
U
U
U
U
U
U
U
U
U
U
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.3
1.6
0.2
0.02
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
1.6
8
0.96
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-848, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846.8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/25/96 12:37
09/25/96 12:37
09/25/96 12:37
09/17/9611:51
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21:18
09/12/96 21.18
09/12/96 21:18
09/12/96 21:18
09/12/96 21.18
09/12/96 21:18
Page 20 of 29
Sample ID: #233, GD4S9 SFT. E. OF M-303 Lab ID: LS44-14 Collect Date: 09/11 /96 11:33
H
•
•
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
630-20-6 1,1,1,2-TETRACHLOROETHANE
71-55-6 1,1,1-TRICHLOROETHANE
79-34-5 1,1,2,2-TETRACHLOROETHANE
79-00-5 1,1,2-TRICHLOROETHANE
75-34-3 1,i-DlCHLOROETHANE
75-35-4 1,1-DICHLOROETHENE
563-58-6 1,1 -DICHLOROPROPENE
87-61-6 1,2,3-TRICHLOROBENZENE
96-18-4 1,2,3-TRICHLOROPROPANE
120-82-1 1,2,4-TRICHLOROBENZENE
95-63-6 1,2,4-TRIMETHYLBENZENE
96-12-8 1,2-DIBROMO-3-CHLOROPROPAN
106-93-4 1,2-DIBROMOETHANE
95-50-1 1,2-DICHLOROBENZENE
107-O6-2 1,2-DICHLOROETHANE
78-87-5 1,2-DICHLOROPROPANE
108-67-8 1,3,5-TRIMETHYLBENZENE
541-73-1 1,3-DICHLOROBENZENE
142-28-9 1,3-DICHLOROPROPANE
106-46-7 1,4-DICHLOROBENZENE
590-20-7 2,2-DICHLOROPROPANE
78-93-3 2-BUTANONE
95-49-8 2-CHLOROTOLUENE
591-78* 2-HEXANONE
106-43-4 4-CHLOROTOLUENE
99-87-6 4-ISOPROPYLTOLUENE
108-10-1 4-METHYL-2-PENTANONE
67-64-1 ACETONE
71-43-2 BENZENE
108-86-1 BROMOBENZENE
74-97-S BROMOCHLOROMETHANE
75-27-4 BROMODICHLOROMETHANE
75-25-2 BROMOFORM
74-83-9 BROMOMETHANE
56-23-5 CARBON TETRACHLORIDE,
108-90-7 CHLOROBENZENE
75-00-3 CHLOROETHANE
67-66-3 CHLOROFORM
74-87-3 CHLOROMETHANE
156-59-4 CIS-1,2-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1 DIBROMOCHLOROMETHANE
74-95-3 DIBROMOMETHANE
75-71* DICHLORODIFLUOROMETHANE
100-41-4 ETHYLBEN2:ENE
87-68-3 HEXACHLOROBUTADIENE
98-82-8 ISOPROPYLBENZENE
108-38-3 M,P-XYLENE
75-09-2 METHYLENE CHLORIDE
104-51-8 N-BUTYLBENZENE
103-65-1 N-PROPYLBENZENE
91-20-3 NAPHTHALENE
95-47-6 O-XYLENE
135-98-8 SEC-BUTYLBENZENE
100-42-5 STYRENE
98-06-6 TERT-BUTYLBENZENE
127-18-4 TETRACHLOROETHENE
108-88-3 TOLUENE
Result
u
u
0.7
16
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Units
ug/g
ug/g
ug/g
ug'g
ug'g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugfltg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1 JB ug/kg
U
U
U
U
U
U
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Oet.
Limit
0.5
0.5
0.1
0.3
1.3
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
Rep.
Limit
0.5
0.5
0.5
1.3
6.6
0.8
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
D
Factor _ Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
tJMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MyiR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
Test Date
10/10/96 18:48
10/10/96 18:48
09/26/96 00:00
09/25/96 13:02
09/25/96 13:02
09/25/96 13:02
09/25/96 13:02
09/17/96 11:55
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/9617:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/9617:38
09/13/9617:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/9617:38
09/13/96 17:38
09/13/96 17:38
09/13/9617:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/9617:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/9617:38
09/13/96 17:38
09/13/9617:38
09/13/96 17:38
09/13/9617:38
09/13/9617:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/9617:38
09/13/96 17:38
09/13/9617:38
09/13/9617:38
09/13/96 17:38
09/13/96 17:38
09/13/9617:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/9617:38
Page 21 of 29
ift
0
•
156-60-5
10061-02*
79-01*
75-69-4
75-01-4
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
ID: #233, GD399 2FT. E,
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1.DlCHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMt IHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMb I HANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
U
U
U
U
U
OF M-303
Result
U
u
0.9
9
2.5
0.3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/l(g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.1 JB ug/kg
U
U
U
U
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.5
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.6
1.5
7.7
0.9
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MAR
L544-15 Collect Date:
Dill.
Factor Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846.8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/96 17:38
09/13/9617:38
09/11/9611:50
Analyst Test Date
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
10/10/96 18:56
10/10/96 18:56
09/26/96 00:00
09/25/9613:05
09/25/96 13:05
09/25/96 13:05
09/25/96 13:05
09/17/96 12:00
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/9614:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14.08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14.08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14.08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/9614:08
Page 22 of 29
o
<p
ift
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02*
79-01-6
75-69-4
75-01-4
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #233, GD399 2FT. DUP E
1 Sample
630-20*
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74*3-9
56-23-5
108-90-7
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
ID: #233, GD399 SFT. E.
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMfc I HYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACfclONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
U
U
U
U
U
U
U
U
U
U
OF M-303
Result
u
u
0.6
11
U
0.2
U
OF M-303
Result
u
u
0.8
13
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Units
ug/g
ug'g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.3
0.2
0.01
Det.
Limit
0.5
0.5
0.1
0.3
1.4
0.2
0.02
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.5
1.3
6.4
0.8
0.04
Lab ID:
Rep.
Limit
0.5
0.5
0.6
1.4
6.9
0.8
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
1
1
1
1
1
1
1
1
1
1
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846,8260
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
LS'14-16 Collect Date:
Dil.
Factor Method
1
•I
1
1
1
1
1
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 7471A
09/13/96 14:08
09/13/9614:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/13/96 14.08
09/13/96 14:08
09/13/96 14:08
09/13/96 14:08
09/11/96 11:50
Analyst Test Date
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
L544-17 Collect Date:
Dil.
Factor Method
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846,6010
SW-846,6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
10/10/9619:04
10/10/96 19:04
09/26/96 00:00
09/25/96 13:08
09/25/96 13:08
09/25/96 13:08
09/25/96 13:08
09/17/96 12:04
09/11/96 12:02
Analyst Test Date
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
10/10/96 19:12
10/10/96 19:12
09/26/96 00:00
09/25/96 13:11
09/25/9613:11
09/25/96 13:11
09/25/9613:11
09/17/96 12:08
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/9614:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
Page 23 of 29
n
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
CHLOROETHANE
CHLOROFORM
CHLOROMfc I HANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample 10: #233, GD431 2FT. E.
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
S63-S8-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108*7-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
OF M-303
Result
u
u
0.5
16
2.1
U
0
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.7
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.7
1.7
8.3
0.99
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
LS4-4-18 Collect Date:
Dil.
Factor Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
09/13/96 14:43
39/11/96 13:30
Analyst Test Date
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
-MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
10/11/96 07:11
10/11/96 07:11
09/26/96 00:00
09/25/96 13:14
09/25/96 13:14
09/25/96 13:14
09/25/96 13:14
09/17/96 12:16
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/9615:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/9615:18
09/13/96 15:18
09/13/9615:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/9615:18
Page 24 of 29
ift
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
aXYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #233, GD431 SFT. E.
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE.
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMfc 1 HYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
1.1
u
u
u
u
u
u
u
u
u
u
u
u
u
u
OF M-303
Result
u
u
0.8
11
u
u
0
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
JB ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.3
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.5
1.3
6.7
0.8
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/9615:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/9615:18
09/13/96 15:18
09/13/9615:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
09/13/96 15:18
L544-19 Collect Date: 09/11/96 13:43
Dill.
Factor Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
'SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Test Date
10/11/96 07:35
10/11/96 07:35
09/26/96 00:00
09/25/96 13:28
09/25/96 13:28
09/25/96 13:28
09/25/96 13:28
09/17/96 12:21
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
Page 25 of 29
#
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74*3-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98*6*
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON 1 b 1 RACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample 10: #233, GD512 2FT. E.
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87*1*
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
1.1 JB ug/kg
U
U
U
U
U
U
U
u
u
u
u
u
u
u
OF M-303
Result.
u
u
0.9
15
4.1
u
u
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.5
0.5
0.1
0.3
1.5
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.6
1.5
7.3
0.9
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
•1
1
1
1
T
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
VWR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
LS41-20 Collect Date:
Dil.
Factor Method
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analvsl
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/9615:53
09/13/96 15:53
09/13/96 15:53
09/13/9615:53
09/13/96 15:53
09/13/96 15:53
09/13/9615:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15:53
09/13/96 15.53
09/13/96 15:53
39/11/9614:02
. Test Date.
10/11/96 07:43
10/11/96 07:43
09/26/96 00:00
09/25/96 13:30
09/25/96 13:30
09/25/96 13:30
09/25/96 13:30
09/17/9612.25
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/9616:28
09/13/96 16:28
Page 26 of 29
#
ift
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67*6-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75*9-2
104-51-8
103-65-1
91-20-3
9&47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75*9-4
754)1-4
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE .
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #233, GDS12 SFT. E.
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12*
106-93-4
95-50-1
107-06-2
78-87-5
Test Parameter
HMX
NITROGLYCERIN
ICP/GFAA METALS DIGESTION
CAOMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
OF, M-303
Result
u
u
0.7
22
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
ug'g
ug'g
ug/g
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.5
0.5
0.1
0.3
1.5
0.2
0.01
0.2
0.2
0.3
0.2
0.1
06
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
0.6
1.5
7.4
0.9
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-a46, 8250
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846.8260
SW-84e, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
NMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16.28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16.28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16-.2B
09/13/96 16:28
09/13/96 16:28
09/13/9616:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/9616:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
09/13/96 16:28
L54^l-21 Collect Date: 09/11 /96 14:20
Oil.
Factor Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
.Analvsl
KMS
KMS
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
Test Date
10/11/96 07:50
10/11/96 07:50
09/26/96 00:00
09/25/96 13:33
09/25/96 13:33
09/25/96 13:33
09/25/96 13:33
09/17/96 12:33
09/13/96 17:03
09/13/96 17.03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/9617:03
09/13/96 17:03
09/13/96 17:03
09/13/9617:03
09/13/96 17:03
09/13/96 17:03
09/13/9617:03
09/13/96 17:03
Page 27 of 29
^
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-5»-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98*2-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
794)1-6
75-69-4
75-01-4
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
1.1 JB ug/kg
U
U
U
U
U
U
U
U
u
u
u
u
u
u
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
10
10
10
10
10
10
10
ib
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/13/9617:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/9617:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/9617:03
09/13/96 17:03
09/13/96 17:03
09/13/9617:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/9617:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/9617:03
09/13/9617:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/9617:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
09/13/96 17:03
Page 28 of 29
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected
but was below the detection limit.
B This flag is used when an analyte is found in the blank as well as the sample
Det. Limit Method Detection Limit (approximately three times the signal noise level)
Rep. Limit Reporting Limit is nonmally the value ofthe lowest standard run with the
analysis. The value is approximately 5 to 10 times the Method Detection Limit.
Dil. Factor Dilution Factor - The prepared sample was diluted by this factor because the
sample was too concentrated or due to other interferences in the sample matrix.
Any dilution factor causes an appropriate increase in the method detection limit
and reporting limit.
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This
flag is used either when estimating a concentration for tentatively identified compounds or
when the data indicated the presence of a compound that meets the identification criteria
but the result is less than the specified reporting limit (e.g. 3 J with a reporting limit of 10)
i^
#
Page 29 of 29
0 CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Requested
Friday, November 01,1996
#
TESTED FOR Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp,UT 84322
Frank Walker
Project: Solid Waste Mgmt Invest.
Login Number L545
Lab Number Client Number
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-5445
800-863-8080
Test Requested Description
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Al ICP Metals Analysis (RCRA)
SW-846, 6010 Ba ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846, 6010 Cr ICP Metals Analysis (RCRA)
SW-846, 6010 Cu ICP Metals Analysis (RCRA)
SW-846,6010 Ni ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846,6010 Sb ICP Metals Analysis (RCRA)
SW-846,6010 Zn ICP Metals Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7740 GFAA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
iReceived
Matrix
Collect Date/Time
L545-1
[EPA 200.7]
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 245.1
SOP 420
SOP 420
1-10 RINSE BLANK
SW-846, 8260
L545-2 #664,
ICP Metals Digestion
Ag ICP Metals Analysis (CWA)
Cd ICP Metals Analysis (CWA)
Cr ICP Metals Analysis (CWA)
Pb ICP Metals Analysis (CWA)
CV.Mercury Analysis (CWA)
HPLC Analysis HMX
HPLC Analysis for NG
Volatile Organics
GDI SFT. 1-10
09/12/96
Water
Water
Water
Water
Water
Water
Water
Water
Water
09/12/96
09/12/96 08:20
09/12/96 08:24
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
ift
Page 1 of 30
L545-3 #664, GDI 10FT. -10 09/12/96 09/12/96 08:36
m
9
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Al ICP Metals Analysis (RCRA)
SW-846,6010 Ba ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846, 6010 Cu ICP Metals Analysis (RCRA)
SW-846,6010 Ni ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846,6010 Sb ICP Metals Analysis (RCRA)
SW-846,6010 Zn ICP Metals Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7740 GFAA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
LS4S-4 #664, GD2 SFT. -10
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Al ICP Metals Analysis (RCRA)
SW-846,6010 Ba ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846, 6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Cu ICP Metals Analysis (RCRA)
SW-846,6010 Ni ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846,6010 Sb ICP Metals Analysis (RCRA)
SW-846,6010 Zn ICP Metals Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7740 GFAA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/12/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/12/96 08:56
Page 2 of 30
L545-5 #664, GD210FT. -10 09/12/96 09/12/96 09:08
•
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Al ICP Metals Analysis (RCRA)
SW-846, 6010 Ba ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846, 6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Cu ICP Metals Analysis (RCRA)
SW-846,6010 Nl ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICPMetals Analysis (RCRA)
SW-846,6010 Sb ICP Metals Analysis (RCRA)
SW-846,6010 Zn ICP Metals Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7740 GFAA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
L54S-6 #664, GD3 SFT. 1-10
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Al ICP Metals Analysis (RCRA)
SW-846,6010 Ba ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Cu ICP Metals Analysis (RCRA)
SW-846,6010 Nl ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846,6010 Sb ICP Metals Analysis (RCRA)
SW-846,6010 Zn ICP Metals Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7740 GFAA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/12/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/12/96 09:27
(p
Page 3 of 30
L545-7 #664, GD3 10FT. -10 09/12/96 09/12/96 09:36
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846, 6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Al ICP Metals Analysis (RCRA)
SW-846,6010 Ba ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846, 6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Cu ICP Metals Analysis (RCRA)
SW-846,6010 Ni ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846,6010 Sb ICP Metals Analysis (RCRA)
SW-846,6010 Zn ICP Metals Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7740 GFAA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
L54S-8 #664, GD4 SFT. -10
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Al ICP Metals Analysis (RCRA)
SW-846,6010 Ba ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846, 6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Cu ICP Metals Analysis (RCRA)
SW-846,6010 Nl ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846,6010 Sb ICP Metals Analysis (RCRA)
SW-846,6010 Zn ICP Metals Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7740 GFAA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/12/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/12/96 10:00
Page 4 of 30
L545-9 #664, GD4 10FT. 1-10 09/12/96 09/12/96 10:10
•
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Al ICP Metals Analysis (RCRA)
SW-846,6010 Ba ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Cu ICP Metals Analysis (RCRA)
SW-846,6010 Ni ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846,6010 Sb ICP Metals Analysis (RCRA)
SW-846,6010 Zn ICP Metals Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7740 GFAA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
L545-10 #663, GDI SFT. M-15A
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Al ICP Metals Analysis (RCRA)
SW-846,6010 Ba ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Cu ICP Metals Analysis (RCRA)
SW-846,6010 Ni ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846,6010 Sb ICP Metals Analysis (RCRA)
SW-846,6010 Zn ICP Metals Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7740 GFAA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/12/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/12/96 11:35
Page 5 of 30
L545-11 #663, GDI 10FT. M-15A 09/12/96 09/12/96 11:42
0
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Al ICP Metals Analysis (RCRA)
SW-846,6010 Ba ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Cu ICP Metals Analysis (RCRA)
SW-846,6010 Nl ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846,6010 Sb ICP Metals Analysis (RCRA)
SW-846,6010 Zn ICP Metals Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7740 GFAA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
LS45-12 #663, GD2 SFT. M-15A
SW-846, 3050 ICP/GF/^A Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Al ICP Metals Analysis (RCRA)
SW-846,6010 Ba ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846, 6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Cu ICP Metals Analysis (RCRA)
SW-846,6010 Ni ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846,6010 Sb ICP Metals Analysis (RCRA)
SW-846,6010 Zn ICP Metals Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7740 GFAA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/12/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/12/96 12:04
Page 6 of 30
L54S-13 #663, GD210FT. M-15A 09/12/96 09/12/96 12:12
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Al ICP Metals/Analysis (RCRA)
SW-846,6010 Ba ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846, 6010 Cu ICP Metals Analysis (RCRA)
SW-846,6010 Ni ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846,6010 Sb ICP Metals Analysis (RCRA)
SW-846,6010 Zn ICP Metals Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7740 GFAA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
LS45-14 #663, GD3 SFT. M-15A 09/12/96 09/12/9613:18
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Al ICP Metals Analysis (RCRA)
SW-846,6010 Ba ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846, 6010 Cu ICP Metals Analysis (RCRA)
SW-846,6010 Nl ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846,6010 Sb ICP Metals Analysis (RCRA)
SW-846,6010 Zn ICP Metals Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7740 GFAA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Page 7 of 30
L545-15 #663, GD3 10FT. M-1SA 09/12/96 09/12/9613:23
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846, 6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Al ICP Metals Analysis (RCRA)
SW-846,6010 Ba ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846, 6010 Cu ICP Metals Analysis (RCRA)
SW-846,6010 Ni ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846,6010 Sb ICP Metals Analysis (RCRA)
SW-846,6010 Zn ICP Metals Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7740 GFAA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soii
Soil
Soil
Soil
Soil
Soil
L545-16 #663, GD4 SFT. M-15A 09/12/96 09/12/96 13:47
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Al ICP Metals Analysis (RCRA)
SW-846,6010 Ba ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846, 6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Cu ICP Metals Analysis (RCRA)
SW-846,6010 Nl ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846,6010 Sb ICP Metals Analysis (RCRA)
SW-846,6010 Zn ICP Metals Analysis (RCRA)
SW-846,7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7740 GFAA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Page 8 of 30
L545-17 #663, GD410FT. M-1SA 09/12/96 09/12/96 13:58
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7060
SW-846, 7471A
SW-846, 7740
SW-846, 8260
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Al ICP Metals Analysis (RCRA)
Ba ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Cu ICP Metals Analysis (RCRA)
Ni ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
Sb ICP Metals Analysis (RCRA)
Zn ICP Metals Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Selenium Analysis (RCRA)
Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
•
^--J^rrlj&o/i
Certified By
^k^'^ nj£j± '^7U
Date
This is to certify that the following samples were analyzed using good laboratory practices to show
the folowing results:
Page 9 of 30
Listing of Results by Sarnple
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6 .
135-98-8
100-42-5
98-06-6
ID: 1-10 RINSE BLANK
Test Parameter
ICP METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
HMX
NITROGLYCERIN
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANbNE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON Tfc I RACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
Result
3.5
U
U
1.9
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
58
U
14
U
U
U
200
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
Units
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1.1 JBug/l
U
U
U
U
U
U
U
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ugfl
Oet.
Limit
1
2.5
13
1.5
0.2
100
100
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
Lab ID:
Rep.
Limit
5
13
63
7.5
0.5
100
100
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
LS^^I Collect Date:
Oil.
Factor Method
[EPA 200.7]
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 245.1
SOP 420
SOP 420
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/12/96 08:20
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KEN
KMS
KMS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/20/96 11:00
09/23/96 15:02
09/23/96 15:02
09/23/96 15:02
09/23/9615:02
09/19/96 13:45
10/11/96 09:37
10/11/96 09:37
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/9617:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/9617:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/9617:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/9617:41
09/23/9617:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/9617:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/9617:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/9617:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/9617:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
Page 10 of 30
127-18-4
108-88-3
156-60-5
10061-02-6
79-01*
75-69-4
75-01-4
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #664, GDI SFT. 1-10
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
Test Parameter
ICP/GFAA METALS DIGESTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
SELENIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1.2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBEh4ZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
U
U
U
U
U
U
U
Result
11200
2.4
81
0.5
0.7
15
6.4
2.3
13
0.1
37
8.3
U
1.5
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
1.2
2.4
0.05
0.1
0.1
0.2
0.1
1.2
0.5
0.1
0.2
0.7
0.01
0.97
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
10
10
10
10
10
10
10
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Lab ID: LS4S-2 Collect Date:
Rep. Dil.
Limit Factor Method
6
12
0.2
0.5
0.5
1.2
0.5
6
2.4
0.7
0.97
1.9
0.04
3.3
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
SW-846, 3050
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,7060
1 SW-846,7471A
1 SW-846,7740
1 SW-846,8260
i SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/96 17:41
09/23/9617:41
09/23/96 17:41
09/12/96 08:24
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
KEN
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
I^R
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
09/26/96 00:00
09/25/96 13:36
09/25/96 13:36
09/25/96 13:36
09/25/96 13:36
09/25/96 13:36
09/25/96 13:36
09/25/96 13:36
09/25/96 13:36
09/25/96 13:36
09/25/96 13:36
09/25/96 13:36
10/18/96 11:10
09/19/96 09:10
10/21/96 15:20
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/9618:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/9618:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/9618:13
09/13/9618:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
Pagell of30
•
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02*
79-01-6
75-69-4
75-01-4
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
IO:#664, GDI 10FT. MO
Test Parameter
ICP/GFAA METALS DIGESTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
SELENIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2.2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-lSOPROPYLTOLUENE
4JI/IETHYL-2-PENTANONE
ACfclONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
U
u
u
u
Result
13000
u
97
0.8
0.9
15
9.8
4.3
15
U
46
5.9
0.02
1.4
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug'g
ug'g
ug'g
ug/g
ug/g
ug/g
ug/g
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
1.4
2.7
0.05
0.1
0.1
0.3
0.1
1.4
0.5
0.2
0.2
0.8
0.01
1.1
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
6.8
14
0.3
0.5
0.5
1.4
0.5
6.8
2.7
0.8
1.1
2.2
0.04
3.7
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
LS45-3 Collect Date:
Dil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 7060
SW-846, 7471A
SW-846, 7740
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/9618:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/13/96 18:13
09/12/96 08:36
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
KEN
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
- MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
09/26/96 00:00
09/25/96 13:39
09/25/96 13:39
09/25/9613:39
09/25/96 13:39
09/25/96 13:39
09/25/96 13:39
09/25/96 13:39
09/25/96 13:39
09/25/96 13:39
09/25/96 13:39
09/25/96 13:39
10/18/96 11:17
09/19/96 09:14
10/21/96 15:28
09/13/96 18:48
09/13/9618:48
09/13/96 18:48
09/13/9618:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/9618:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
Page 12 of 30
75-25-2
74*3-9
56-23-5
108-90-7
75-00-3
67-66-3
74*7-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47*
135-98-8
100-42-5
98-06-6
127-18-4
108*8-3
156-60-5
10061-02*
79-01-6
75-69-4
75-01-4
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
ClS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #664, GD2 SFT. 1-10
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-67-5
108-67-8
541-73-1
142-28-9
106-46-7
Test Parameter
ICP/GFAA METALS DIGESTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
SELENIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETH/^NE .
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
1.5 JBugAg
U
U
U
U
U
U
U
u
u
u
u
u
u
u
Result
11100
u
71
0.6
0.4
19
6.2
U
16
u
42
8.9
0
3.1
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug'g
ug'g
ug/g
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
1.5
3.1
0.06
0.1
0.1
0.3
0.1
1.5
0.6
0.2
0.2
0.9
0.01
1.2
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
7.7
15
0.3
0.6
0.6
1.5
0.6
7.7
3.1
0.9
1.2
2.5
0.04
4.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
LS45-4 Collect Date:
Dill.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 7060
SW-846, 7471A
SW-846, 7740
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
Analvsl
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
KEN
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/9618:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/9618:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/9618:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/96 18:48
09/13/9618:48
39/12/96 08:56
Test Date
10/03/96 13:00
10/08/96 14:18
10/08/96 14:18
10/08/96 14:18
10/08/96 14:18
10/08/96 14:18
10/08/96 14:18
10/08/96 14:18
10/08/96 14:18
10/08/96 14:18
10/08/96 14:18
10/08/96 14:18
10/18/9611:30
09/19/96 09:19
10/21/96 15:36
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/9619:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
Page 13 of 30
•
590-20-7
78-93-3
96-19-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-S
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67*6-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01*
75-69-4
75-01-4
2,2-DICHLOROPROP/VNE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
ClS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #664, GD2 10FT. 1-10
630-20-6
71-55*
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
Test Parameter
ICP/GFAA METALS DIGESTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
SELENIUM
1,1,1,2-TETRACHLOROETHANE
1 ,t ,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Result
10900
u
102
0.6
0.3
14
5.8
U
10
u
33
4.6
0.01
1.6
U
U
U
U
U
U
U
U
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
04
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
1.6
3.2
0.06
0.1
0.1
0.3
0.1
1.6
0.6
0.2
0.3
0.9
0.01
1.3
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
8.1
16
0.3
0.6
0.6
1.6
0.6
8.1
3.2
0.97
1.3
2.6
0.02
4.4
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
hMR
MMR
MMR
MMR
MMR
09/13^6 19:23
09/13/96 19:23
09/13/96 19:23
09/13/9619:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19.23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19.23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/96 19:23
09/13/9619:23
09/13/96 19:23
09/13/96 19:23
L54S-S Collect Date: 09/12/96 09:081
Dil.
Factor Method
SW-846, 3050
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 7060
SW-846, 7471A
SW-846, 7740
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
KEN
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
; Test Date
10/03/96 13:00
10/08/96 14:21
10/08/96 14:21
10/08/96 14:21
10/08/96 14:21
10/08/96 14:21
10/08/96 14:21
10/08/96 14:21
10/08/96 14:21
10/08/96 14:21
10/08/96 14:21
10/08/96 14:21
10/18/96 11:43
09/19/96 09:27
10/23/96 08:47
09/13/96 19:58
Q9n3'96 19.58
09/13/9619:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
Page 14 of 30
e
^
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107r06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01*
75-69-4
75-01-4
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMfc 1 HANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #664, GD3 SFT. 1-10
Test Parameter
ICP/GFAA METALS DIGESTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
1.6 J
U
U
U
u
u
u
u
u
u
u
u
u
u
u
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
1.1 JB ugAg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Result
13500
U
98
0.7
0.4
18
11
U
13
U
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
1.4
2.8
0.06
0.1
0.1
0.3
0.1
1.4
0.6
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
6.9
14
0.3
0.6
0.6
1.4
0.6
6.9
2.8
0.8
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
- MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/13/96 19:58
09/13/96 19:58
09/13/9619:58
09/13/9619:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/9619:58
09/13/9619:58
09/13/96 19:58
09/13/9619:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
09/13/96 19:58
LS4j;-6 Collect Date: 09/12/96 09:27
Oil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Analyst
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
Test Date
10/03/96 13:00
10/08/96 14:24
10/08/96 14:24
10/08/96 14:24
10/08/9614:24
10/08/96 14:24
10/08/96 14:24
10/08/96 14:24
10/08/96 14:24
10/08/96 14:24
10/08/96 14:24
Page 15 of 30
(p
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108*7-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06*
127-18-4
108*8-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
ZINC
ARSENIC
MERCURY
SELENIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE .
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
57
6.1
0
2.6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/g
ug/g
ug/g
ug/g
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.7 JB ug/kg
U
U
U
U
U
U
U
U
U
U
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
0.2
0.8
0.01
1.1
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
1.1
2.2
0.04
3.7
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-S46, 6010
SW-846, 7060
SW-846, 7471A
SW-846, 7740
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
KWB
CRS
KEN
CRS
MAR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
rwg^R
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
IVWR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/08/96 14:24
10/18/96 11:56
09/19/96 09:36
10/23/96 08:55
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/t3/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
09/13/96 20:33
Page 16 of 30
•
1 Sample
630-20*
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82*
108-38-3
75-09-2
104-51-8
103-65-1
ID:#664, GD3 10FT. 1-10
Test Parameter
ICP/GFAA METALS DIGESTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
SELENIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
Result
16100
U
100
0.8
0.2
20
8.1
U
12
U
42
5.5
0
1.8
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
1.2 JB ugAg
U
U
ug/kg
ug/kg
Det.
Limit
1.4
2.8
0.06
0.1
0.1
0.3
0.1
1.4
0.6
0.2
0.2
0.8
0.01
1.1
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
Lab ID:
Rep.
Limit
7
14
0.3
0.6
0.6
1.4
0.6
7
2.8
0.8
1.1
2.2
0.03
3.8
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
L&45-7 Collect Date:
Oil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471A
SW-846, 7740
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/12/96 09:36
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
KEN
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/03/96 13:00
10/08/96 14:27
10/08/96 14:27
10/08/96 14:27
10/08/96 14:27
10/08/96 14:27
10/08/96 14:27
10/08/96 14:27
10/08/96 14:27
10/08/96 14:27
10/08/96 14:27
10/08/96 14:27
10/18/96 12:09
09/19/96 09:40
10/23/96 09:00
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
Page 17 of 30
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-«
79-01-6
75-69-4
75-01-4
[sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-6
108-90-7
75-00-3
67-66-3
74-87-3
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
ID: #664, GD4 SFT. 1-10
Test Parameter
ICP/GFAA METALS DIGESTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
SELENIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE .
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
.1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
U
U
U
U
U
U
U
U
U
u
u
u
Result
13800
U
103
0.7
0.1
18
7.2
U
12
U
38
5.7
U
2.9
U
U
U
U
U
U
U
U
U
U
u
u
u
u
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug'g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
1.7
3.3
0.07
0.1
0.1
0.3
0.1
1.7
0.7
0.2
0.3
0.9
0.01
1.3
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
10
ib
10
10
10
10
10
10
10
10
10
10
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
'I SW-846,8260
-1 SW-846,8260
-;. SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
Lab ID: LS45-8 Collect Date:
Rep. Dil.
Limit Factor Method
8.3
17
0.3
0.7
0.7
1.7
0.7
8.3
3.3
1
1.3
2.7
0.04
4.5
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
SW-846, 3050
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,7060
1 SW-846,7471A
1 SW-846,7740
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/13/96 21:07
09/12/96 10:00
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
KEN
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/03/96 13:00
10/08/96 14:29
10/08/96 14:29
10/08/96 14:29
10/08/96 14:29
10/08/96 14:29
10/08/96 14:29
10/08/96 14:29
10/08/96 14:29
10/08/96 14:29
10/08/96 14:29
10/08/96 14:29
10/18/96 12:16
09/19/96 09:44
10/23/96 09:11
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
Page 18 of 30
•
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
,100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47*
135-98-8
10O-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18^
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
0:#664, GD410FT. 1-10
Test Parameter
ICP/GFAA METALS DIGESTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
SELENIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
U
U
u
u
u
u
u
u
u
1.1
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Result
17300
u
120
0.9
0.5
21
8.6
U
13
U
45
6.3
0.01
1.8
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
JB ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
1.5
3
0.06
0.1
0.1
0.3
0.1
1.5
0.6
0.2
0.2
0.8
0.01
1.2
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
7.5
15
0.3
0.6
0.6
1.5
0.6
7.5
3
0.9
1.2
2.4
0.03
4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
LS45-9 Collect Date:
OiL
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471A
SW-846, 7740
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21.42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
09/13/96 21:42
39/12/9610:10
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
KEN
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
10/03/96 13:00
10/08/96 14:43
10/08/96 14:43
10/08/9614:43
10/08/96 14:43
10/08/96 14:43
10/08/96 14:43
10/08/96 14:43
10/08/96 14:43
10/08/96 14:43
10/08/96 14:43
10/08/96 14:43
10/18/96 12:44
09/19/96 09:52
10/23/96 09:29
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13796 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
Page 19 of 30
•
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-231-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06*
127-18-4
108*8-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DlCHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #663, GDI SFT.
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
Test Parameter
ICP/GFAA METALS DIGESTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
SELENIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
1.3 JB ug/kg
U
U
U
U
U
U
U
U
u
u
u
u
u
u
M-15A
Result
12100
U
96
0.7
0.3
16
8.4
U
13
U
43
7
0.2
2.1
U
U
U
1.8 J
U
U
U
U
U
U
U
U
U
U
1.9 J
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
1.5
3
0.06
0.1
0.1
0.3
0.1
1.5
0.6
0.2
0.2
0.9
0.01
1.2
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Umjt
7.6
15
0.3
0.6
0.6
1.5
0*
7.6
3
0.9
1.2
2.4
0.04
4.1
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
09/13/96 22:17
L54I5-10 Collect Date: 09/12/96 11:35
Oil.
Facitor Method
SW-846, 3050
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 7060
SW-846, 7471A
SW-846, 7740
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
KEN
CRS
MMR
MMR
MMR
MAR
MMR
MAR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
Test Date
10/03/96 13:00
10/08/96 14:46
10/08/96 14:46
10/08/96 14:46
10/08/96 14:46
10/08/96 14:46
10/08/96 14:46
10/08/96 14:46
10/08/96 14:46
10/08/96 14:46
10/08/96 14:46
10/08/96 14:46
10/18/9612:56
09/19/96 09:57
10/23/96 09:42
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
Page 20 of 30
#
78-87-5
108*7*
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108*6-1
74-97-5
75-27-4
75-25-2
74*3-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98*
100-42-5
98-06-6
127-18-4
108-88-3
156*0-5
10061-02-6
79-01-6
75-69-4
75-01-4
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 SamplelD: #663, GDI 10FT.
630-20-6
71-55-6
79-34-5
Test Parameter
ICP/GFAA METALS DIGESTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
SELENIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
U
U
U
U
U
U
U
U
U
U
U
U
U
2.3 J
U
U
4 J
U
U
U
3.9 J
U
U
U
U
U
4 J
U
u
1.3 J
U
u
u
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
1.4 JB ug/kg
u
U
U
U
U
U
U
U
2 J
U
U
U
U
U
M-1SA
Result
12800
U
97
0.7
O.S
17
8.2
U
13
U
44
5
0
2.2
U
U
U
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
1.5
3
0.06
0.1
0.1
0.3
0.1
1.5
0.6
0.2
0.2
0.9
0.01
1.2
0.2
0.2
0.3
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
7.6
15
0.3
0.6
0.6
1.5
0.6
7.6
3
0.9
1.2
2.4
0.04
4.1
10
10
10
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
t S\/y-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
•1 SW-846,8260
1 SW-846,8260
•1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 * SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
M^R
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/24/96 15:00
09/24/96 15.00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/9615:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/9615:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/9615:00
09/24/96 15:00
09/24/96 15:00
09/24/9615:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/9615:00
09/24/96 15:00
09/24/9615:00
09/24/96 15:00
09/24/96 15:00
09/24/9615:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/96 15:00
09/24/9615:00
09/24/96 15:00
LS4&-11 Collect Date: 09/12/96 11:42
Oil.
Factor Method
SW-846, 3050
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,7060
1 SW-846,7471A
1 SW-846,7740
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
Analyst
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
KEN
CRS
MMR
MMR
MMR
Test Date
10/03/96 13:00
10/08/96 14:49
10/08/96 14:49
10/08/96 14:49
10/08/96 14:49
10/08/96 14:49
10/08/96 14:49
10/08/96 14:49
10/08/96 14:49
10/08/96 14:49
10/08/96 14:49
10/08/96 14:49
10/18/96 13:04
09/19/96 10:03
10/23/96 09:50
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
Page 21 of 30
#
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108*7-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #663, GD2 SFT. M-1SA
Test Parameter
ICP/GFAA METALS DIGESTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
1.3 JB ugAg
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Result
12900
u
110
0.7
0.1
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
1.7
3.3
0.07
0.1
0.1
10
10
ib
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
Lab ID: L54
Rep. Oi
Limit Fac
8.3 1
17 1
0.3 1
0.7 1
0.7 1
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
t SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
I SW-846,8260
1 SW-846,8260
1 SW-S46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/9615:35
09/24/96 15:35
09/24/9615:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
09/24/96 15:35
ii-12 Collect Date: 09/12/96 12:04
1.
tor Method
SW-846, 3050
SW-846, 6010
SW-846,6010
SW-846,6010
SW-846, 6010
SW-846, 6010
Analyst
KWB
KWB
KWB
KWB
KWB
KWB
Test Date
10/03/96 13:00
10/08/96 14:52
10/08/9614:52
10/08/96 14:52
10/08/96 14:52
10/08/96 14:52
Page 22 of 30
#
0
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
SELENIUM
630-20-6 1,1,1,2-TETRACHLOROETHANE
71-55* 1,1,1-TRICHLOROETHANE
79-34-5 1,1,2,2-TETRACHLOROETHANE
79-00-5 1,1,2-TRICHLOROETHANE
75-34-3 1,1-DICHLOROETHANE
75-35-4 1,1-DICHLOROETHENE
563-58-6 1,1-DICHLOROPROPENE
87-61-6 1,2,3-TRICHLOROBENZENE
96-18-4 1,2,3-TRICHLOROPROPANE
120-82-1 1,2,4-TRICHLOROBENZENE
95-63-6 1,2,4-TRIMETHYLBENZENE
96-12-8 1,2-DIBROMO-3-CHLOROPROPAN
106-93-4 1,2-DIBROMOETHANE
95-50-1 1,2-DICHLOROBENZENE
107-06-2 1,2-DICHLOROETHANE
78-87-5 1,2-DICHLOROPROPANE
108-67* 1,3,5-TRIMETHYLBENZENE
541 -73-1 1,3-DICHLOROBENZENE
142-28-9 1,3-DICHLOROPROPANE
106-46-7 1,4-DICHLOROBENZENE
590-20-7 2,2-DICHLOROPROPANE
78-93-3 2-BUTANONE
95-49-8 2-CHLOROTOLUENE
591-78-6 2-HEXANONE
106-43-4 4-CHLOROTOLUENE
99-87-6 4-ISOPROPYLTOLUENE
108-10-1 4-METHYL-2-PENTANONE
67-64-1 ACETONE
71-43-2 BENZENE
108-86-1 BROMOBENZENE
74-97-5 BROMOCHLOROMETHANE
75-27-4 BROMODICHLOROMETHANE
75-25-2 BROMOFORM
74-83-9 BROMOMETHANE
56-23-5 CARBON TETRACHLORIDE
108-90-7 CHLOROBENZENE
75-00-3 CHLOROETHANE
67-66-3 CHLOROFORM
74-87-3 CHLOROMETHANE
156-59-4 CIS-1,2-DICHLOROETHENE
IOOei-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1 DIBROMOCHLOROMETHANE
74-95-3 DIBROMOMETHANE
75-71-8 DICHLORODIFLUOROMETHANE
100-41-4 ETHYLBENZENE
87-68-3 HEXACHLOROBUTADIENE
98*2-8 ISOPROPYLBENZENE
108-38-3 M,P-XYLENE
75-09-2 METHYLENE CHLORIDE
104-51-8 N-BUTYLBENZENE
103-65-1 N-PROPYLBENZENE
91-20-3 NAPHTHALENE
95-47-6 O-XYLENE
135-98-8 SEC-BUTYLBENZENE
100-42-5 STYRENE
98-06-6 TERT-BUTYLBENZENE
127-18-4 TETRACHLOROETHENE
108-88-3 TOLUENE
156-60-5 TRANS-1,2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
79-01-6 TRICHLOROETHENE
16
8.7
U
13
U
43
5.3
0.01
2.4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
1.3 JB ugAg
U
U
U
U
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
0.3
0.1
1.7
0.7
0.2
0.3
0.9
0.01
1.3
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
1.7
0.7
8.3
3.3
1
1.3
2.7
0.03
4.5
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,7060
1 SW-846, 7471A
1 SW-846,7740
t SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW*46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
KWB
KWB
KWB
KWB
KWB
KWB
CRS
KEN
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
10/08/9614:52
10/08/96 14:52
10/08/96 14:52
10/08/96 14:52
10/08/96 14:52
10/08/96 14:52
10/18/96 13:16
09/19/96 10:07
10/23/9611:01
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/9616:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16:10
09/24/96 16;10
09/24/96 16:10
Page 23 of 30
75-69-4
75-01-4
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
ug/kg
ug/kg
0.3
0.4
10
10
SW-846, 8260
SW-846, 8260
MMR
MMR
09/24/96 16:10
09/24/96 16:10
II sample ID: #663, GD2 10FT. M-1SA Lab ID: L5'15-13 Collect Date: 09/12/96 12:12
Test Parameter Result Units
ICP/GFAA METALS DIGESTION
ALUMINUM 15500 ug/g
ANTIMONY U ug/g
BARIUM 111 ug/g
BERYLLIUM 0.7 ug/g
CAOMIUM 0.2 ug/g
CHROMIUM 21 ug/g
COPPER 7.7 ug/g
LEAD U ug/g
NICKEL 14 ug/g
SILVER U ug/g
ZINC 42 ug/g
ARSENIC 5.5 ug/g
MERCURY 0.01 ug/g
SELENIUM 2.2 ug/g
630-20-6 1,1,1,2-TETRACHLOROETHANE U ug/kg
71-55-6 1,1,1-TRICHLOROETHANE U ug/kg
79-34-5 1,1,2,2-TETRACHLOROETHANE U ugAg
79-00-5 1,1,2-TRICHLOROETHANE U ug/kg
75-34-3 1,1-DICHLOROETHANE U ug/kg
75-35-4 1,1-DICHLOROETHENE U ug/kg
563-58* 1,1-DICHLOROPROPENE U ugAg
87-61-6 1,2,3-TRICHLOROBENZENE U ug/kg
96-18-4 1,2,3-TRICHLOROPROPANE U ugAg
120-82-1 1,2,4-TRICHLOROBENZENE U ugAg
95-63-6 1,2,4-TRIMETHYLBENZENE U ugAg
96-12-8 1,2-DIBROMO-3-CHLOROPROPAN U ug/kg
106-93-4 1,2-DIBROMOETHANE U ugAg
95-50-1 1,2-DICHLOROBENZENE U ugAg
107-06-2 1,2-DICHLOROETHANE U ugAg
78*7-5 1,2-DICHLOROPROPANE U ug/kg
108-67-8 1,3,5-TRIMETHYLBENZENE U ug/kg
541-73-1 1,3-DICHLOROBENZENE U ug/kg
142-28-9 1,3-DICHLOROPROPANE U ug/kg
106-45-7 1,4-DICHLOROBENZENE U ug/kg
590-20-7 2,2-DICHLOROPROPANE U ug/kg
78-93-3 2-BUTANONE U ug/kg
95-49-8 2-CHLOROTOLUENE U ug/kg
591-78-6 2-HEXANONE U ug/kg
106-43-4 4-CHLOROTOLUENE U ug/kg
99-87-6 4-ISOPROPYLTOLUENE U ug/kg
108-10-1 4-METHYL-2-PENTANONE U ug/kg
67-64-1 ACETONE U ugAg
71-43-2 BENZENE U ugAg
108-86-1 BROMOBENZENE U ugAg
74-97-5 BROMOCHLOROMETHANE U ugAg
75-27-4 BROMODICHLOROMETHANE U ugAg
75-25-2 BROMOFORM U ug/l(g
74-83-9 BROMOMETHANE U ug/kg
56-23-5 CARBON TETRACHLORIDE U ugAg
108-90-7 CHLOROBENZENE U ug/kg
75-00-3 CHLOROETHANE U ug/kg
67-66-3 CHLOROFORM U ugAg
74-87-3 CHLOROMETHANE U ug/kg
156-59-4 CIS-1,2-DICHLOROETHENE U ug/kg
10061-01-5 CIS-1,3-DICHLOROPROPENE U ugAg
124-48-1 DIBROMOCHLOROMETHANE U ug/kg
74-95-3 DIBROMOMETHANE U ug/kg
75-71-8 DICHLORODIFLUOROMETHANE U ug/kg
100-41-4 ETHYLBENZENE U ugAg
87-68-3 HEXACHLOROBUTADIENE U ugAg
98*2-8 ISOPROPYLBENZENE U ugAg
108-38-3 M,P-XYLENE U ug/kg
75-09-2 METHYLENE CHLORIDE 1.2 JB ug/kg
Oet. Rep. Oil.
Limit Limit Factor Method Analyst Test Date
SW-846,3050 KWB 10/03/96 13:00
1.4 6.8 1 SW-846,6010 KWB 10/08/96 14:55
2.7 14 -I SW-846,6010 KWB 10/08/96 14:55
0.05 0.3 1 SW-846,6010 KWB 10/08/96 14:55
0.1 0.5 1 SW-846,6010 KWB 10/08/96 14:55
0.1 0.5 11 SW-846,6010 KWB 10/08/96 14:55
0.3 1.4 1 SW-846,6010 KWB 10/08/96 14:55
0.1 0.5 1 SW-846,6010 KWB 10/08/96 14:55
1.4 6.8 1 SW-846,6010 KWB 10/08/96 14:55
0.5 2.7 1 SW-846,6010 KWB 10/08/9614:55
0.2 0.8 1 SW-846,6010 KWB 10/08/9614:55
0.2 1.1 1 SW-846,6010 KWB 10/08/96 14:55
0.8 2.2 1 SW-846,7060 CRS 10/18/96 13:23
0.01 0.02 1 SW-846,7471A KEN 09/19/96 10:16
1.1 3.7 1 SW-846,7740 CRS 10/23/96 11:09
0.2 10 1 SW-846,8260 MMR 09/24/96 16:45
0.2 10 1 SW-846,8260 MMR 09/24/9616:45
0.3 10 1 SW-846,8260 MMR 09/24/96 16:45
0.2 10 1 SW-846,8260 MMR 09/24/96 16:45
0.1 10 1 SW-846,8260 MMR 09/24/9616:45
0.6 10 1 SW-846,8260 MMR 09/24/96 16:45
0.2 10 1 SW-846,8260 MAR 09/24/9616:45
0.2 10 1 SW-846,8260 MMR 09/24/9616:45
0.2 10 1 SW-846,8260 MMR 09/24/9616:45
0.2 10 1 SW-846,8260 MMR 09/24/96 16:45
0.2 10 1 SW-846,8260 MMR 09/24/96 16:45
0.2 10 1 SW-846,8260 MMR 09/24/96 16:45
0.2 10 1 SW-846,8260 MMR 09/24/9616:45
0.1 10 1 SW-846,8260 MMR 09/24/96 16:45
0.2 10 1 SW-846,8260 MMR 09/24/9616:45
0.2 10 1 SW-846,8260 MMR 09/24/9616:45
0.2 10 1 SW-846,8260 MMR 09/24/96 16:45
0.2 10 1 SW-846,8260 MMR 09/24/9616:45
0.2 10 1 SW-846,8260 MMR 09/24/96 16:45
0.2 10 1 SW-846,8260 MMR 09/24/96 16:45
0.2 10 1 SW-846,8260 MMR 09/24/96 16:45
10 10 1 SW-846,8260 MMR 09/24/96 16:45
0.2 10 1 SW-846,8260 MAR 09/24/9616:45
10 10 1 SW-846,8260 MMR 09/24/96 16:45
0.2 10 1 SW-846,8260 MMR 09/24/96 16:45
0.2 10 1 SW-846,8260 MMR 09/24/96 16:45
10 10 1 SW-846,8260 MMR 09/24/96 16:45
10 10 1 SW-846,8260 MMR 09/24/96 16:45
0.2 10 1 SW-846,8260 MMR 09/24/96 16:45
0.2 10 1 SW-846,8260 MMR 09/24/9616:45
0.2 10 1 SW-846,8260 MMR 09/24/96 16:45
0.3 10 1 SW-846,8260 MMR 09/24/9616:45
0.1 10 1 SW-846,8260 MMR 09/24/96 16:45
0.4 10 1 SW-846,8260 MMR 09/24/96 16:45
0.3 10 1 SW-846,8260 MMR 09/24/9616:45
0.2 10 1 SW-846,8260 MMR 09/24/96 16:45
0.4 10 1 SW-846,8260 MAR 09/24/96 16:45
0.4 10 1 SW-846,8260 MMR 09/24/96 16:45
0.6 10 1 SW-846,8260 MMR 09/24/9616:45
0.2 10 1 SW-846,8260 MMR 09/24/96 16:45
0.2 10 1 SW-846,8260 MMR 09/24/96 16:45
0.3 10 1 SW-846,8260 MMR 09/24/9616:45
0.2 10 1 SW-846,8260 MMR 09/24/96 16:45
0.2 10 1 SW-846,8260 MMR 09/24/96 16:45
0.3 10 1 SW-846,8260 MMR 09/24/96 16:45
0.2 10 1 SW-846,8260 MAR 09/24/9616:45
0.2 10 1 SW-846,8260 MMR 09/24/9616:45
0.2 10 1 SW-846,8260 MMR 09/24/96 16:45
0.3 10 1 SW-846,8260 MMR 09/24/96 16:45
Page 24 of 30
m
#
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06*
127-18-4
108-88-3
156-60-5
10061-02-e
79-01-6
75-69-4
75-01-4
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
10: #663, GD3 SFT.
Test Parameter
ICP/GFAA METALS DIGESTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
SELENIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
M-15A
Result
16500
U
130
0.8
0.5
22
8.6
U
14
U
44
5.8
U
1.4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
1.6
3.2
0.06
0.1
0.1
0.3
0.1
1.6
0.6
0.2
0.3
0.9
0.01
1.3
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
7.9
16
0.3
0.6
0.6
1.6
0.6
7.9
3.2
0.9
1.3
2.5
0.03
4.3
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MAR
L&<IS-14 Collect Date:
Dil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471A
SW-846, 7740
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/24/96 16:45
09/24/9616:45
09/24/96 16:45
09/24/9616:45
09/24/96 16:45
09/24/96 16:45
09/24/96 16:45
09/24/96 16:45
09/24/96 16:45
09/24/96 16:45
09/24/96 16:45
09/24/96 16:45
09/24/96 16:45
09/24/96 16:45
09/12/9613:18
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
KEN
CRS
MMR
MMR
I^AVIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
N«VIR
MMR
MMR
MMR
MAR
MMR
MAR
MMR
MMR
10/03/96 13:00
10/08/96 15:17
10/08/96 15:17
10/08/9615:17
10/08/96 15:17
10/08/96 15:17
10/08/96 15:17
10/08/96 15:17
10/08/96 15:17
10/08/9615:17
10/08/96 15:17
10/08/96 15:17
10/18/96 13:40
09/19/96 10:20
10/23/96 11:17
09/24/96 17:19
09/24/9617:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/9617:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/9617:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/9617:19
09/24/96 17:19
09/24/96 17:19
09/24/9617:19
09/24/96 17:19
09/24/9617:19
09/24/96 17:19
09/24/96 17:19
Page 25 of 30
#
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82*
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6 .
135-98*
100-42-5
98*6-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75*1-4
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #663, GD3 10FT. M-
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
Test Parameter
ICP/GFAA METALS DIGESTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
SELENIUM
1,1.1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
U
U
U
U
U
U
U
U
U
U
U
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
1.1 JB ug/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
15A
Result
13800
U
118
0.7
0.3
18
8.7
U
14
U
42
7.6
U
1.9
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
Units.
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
1.6
3.2
0.06
0.1
0.1
0.3
0.1
1.6
0.6
0.2
0.3
0.9
0.01
1.3
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
7.9
16
0.3
0.6
0.6
1.6
0*
7.9
3.2
0.95
1.3
2.5
0.04
4.3
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
LS4!5-1S Collect Date:
Oil.
Facior Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471A
SW-846, 7740
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/9617:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/9617:19
09/24/96 17:19
09/24/96 17:19
09/24/9617:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/24/96 17:19
09/12/96 13:23
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
KEN
CRS
- MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
N«^R
MMR
MMR
MMR
MMR
MMR
10/03/96 13.00
10/08/96 15:20
10/08/96 15:20
10/08/96 15:20
10/08/9615:20
10/08/96 15:20
10/08/9615:20
10/08/96 15:20
10/08/96 15:20
10/08/96 15:20
10/08/9615:20
10/08/96 15:20
10/18/9613:48
09/19/96 10:24
10/23/96 11:25
09/24/96 17:54
09/24/96 17:54
09/24/9617:54
09/24/96 17.54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/9617:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/9617:54
09/24/9617:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/9617.54
09/24/96 17:54
09/24/96 17:54
Page 26 of 30
il
•
#
99*7-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
76-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108*8-3
156-60-5
10061-02-6
79-01-6
75*9-4
75-01-4
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #663, GD4SFT.
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58*
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
Test Parameter
ICP/GFAA METALS DIGESTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
SELENIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
U
U
U
U
U
U
U
U
u
u
u
. u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.4 JB ug/kg
U
U
U
U
u
U
U
U
U
U
U
U
U
U
M-15A
Result
13300
U
102
0.7
0.4
18
8
U
15
U
49
7.2
0.03
1.9
U
U
U
U
U
U
U
u
u
u
u
u
u
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
1.6
3.2
0.06
0.1
0.1
0.3
0.1
1.6
0.6
0.2
0.3
0.9
0.01
1.3
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
10
id
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
8
16
0.3
06
0.6
1.6
0.6
8
3.2
0.96
1.3
2.6
0.04
4.4
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
L54£l-16 Collect Date:
Oil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471A
SW-846, 7740
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analysi
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
KEN
CRS
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/9617:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/9617:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/9617:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/2*96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/96 17:54
09/24/9617:54
39/12/96 13:47
Test Date
10/03/96 13:00
10/08/96 15:23
10/08/96 15:23
10/08/96 15:23
10/08/96 15:23
10/08/96 15:23
10/08/96 15:23
10/08/96 15:23
10/08/96 15:23
10/08/96 15:23
10/08/96 15:23
10/08/96 15:23
10/18/96 14:10
09/19/96 10:28
10/23/96 11:32
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
Page 27 of 30
#
95-50-1
107-06-2
78-87-5
108*7-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-9O-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98*6-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #663, GD4 10FT.
630-20-6
Test Parameter
ICP/GFAA METALS DIGESTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
SELENIUM
1,1,1,2-TETRACHLOROETHANE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
1.4 JB ugAg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
M-15A
Result
20700
U
133
0.98
0.5
24
11
U
17
U
53
6.2
U
2.5
U
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
1.5
3
0.06
0.1
0.1
0.3
0.1
1.5
0.6
0.2
0.2
0.8
0.02
1.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
7.5
15
0.3
0.6
0.6
1.5
0.6
7.5
3
0.9
1.2
2.4
0.04
4
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MAR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/9618:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/9618:29
09/24/9618:29
09/24/9618:29
09/24/9618:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
09/24/96 18:29
L545-17 Collect Date: 09/12/96 13:58
Dil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471A
SW-846, 7740
SW-846, 8260
Analyst
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
KEN
CRS
MMR
Test Date
10/03/96 13:00
10/08/96 15:26
10/08/96 15:26
10/08/96 15:26
10/08/96 15:26
10/08/96 15:26
10/08/96 15:26
10/08/96 15:26
10/08/96 15:26
10/08/96 15:26
10/08/96 15:26
10/08/96 15:26
10/18/96 14:17
09/19/96 10:32
10/23/96 11:45
09/24/96 19:04
Page 28 of 30
o
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-O6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-5&-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DlBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-lSOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug'kg
ug'kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
1.3 JB ug/kg
U
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
1 SW-846,8260
1 . SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
•1 SW-846,8260
•1 SW-846,8260
11 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-S46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
VS^R
MMR
MMR
MMR
MMR
MAR
MAR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
-MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/24/9619:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/9619:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/9619:04
09/24/9619:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/9619:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
09/24/96 19:04
#
Page 29 of 30
•
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected
but was below the detection limit.
B This flag is used when an analyte is found in the blank as well as the sample
Det. Limit Method Detection Limit (approximately three times the signal noise level)
Rep. Limit Reporting Limit is normally the value ofthe lowest standard run with the
analysis. The value is approximately 5 to 10 times the Method Detection Limit.
Dil. Factor Dilution Factor - The prepared sample was diluted by this factor because the
sample was too concentrated or due to other interferences in the sample matrix.
Any dilution factor causes an appropriate increase in the method detection limit
and reporting limit.
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This
flag is used either when estimating a concentration for tentatively identified compounds or
when the data indicated the presence of a compound that meets the identification criteria
but the result is less than the specified reporting limit (e.g. 3 J with a reporting limit of 10)
#
Page 30 of 30
9 CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Flequested
Friday, November 01,1996
TESTED FOR Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp,UT 84322
Frank Walker
Project: Solid Waste Mgmt Invest.
Login Number L560
Lab Number Client Number
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
301-863-5445
300-863-8080
Test Requested Description
LS60-1 T-35 RINSE BLANK
[EPA 200.7] ICP Metals Digestion
EPA 200.7 Ag ICP Metals Analysis (CWA)
EPA 200.7 Be ICP Metals Analysis (CWA)
EPA 200.7 Cd ICP Metals Analysis (CWA)
EPA 200.7 Cr ICP Metals Analysis (CWA)
EPA 200.7 Pb ICP Metals Analysis (CWA)
EPA 245.1 CV Mercury Analysis (CWA)
SW-846, 8260 Volatile Organics
L560-2 #201, GD3 SFT. T-35
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
L560-3 #201,GD310FT. T-3S
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846, 6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
Received
Matrix
Collect Date/Time
09/19/96
Water
Water
Water
Water
Water
Water
Water
Water
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/17/9610:05
09/17/96 10:08
09/17/96 10:20
•
Page 1 of 30
LS60-4 #201,GD14 7FT. T-35 09/19/96 09/17/96 11:01
#
SW-846, 3050 ICP/GFAiA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846, 6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
LS60-S #201, GDI 41 OFT. T-35
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-546, 6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
LS60-6 #201, GD7 SFT. T-3S
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
LS60-7 #201,GD7 10FT. T-3S
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846, 6010 Ag ICP Melals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846, 6010 Cd ICP Metals Analysis (RCRA)
SW-846, 6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
L560-8 #201, GD11 SFT. T-35
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846, 6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/17/96 11:22
09/17/9614:22
09/17/96 14:52
09/17/96 15:20
Page 2 of 30
L560-9 #201, GD11 SFT. DUP. T-3S 09/19/96 09/17/96 15:20
•
#
SW-846, 3050 ICP/GFAiA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
L560-10 #201, GD11 10FT. T-3S
SW-846, 3050 ICP/GFAiA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
L560-11 #201, GD9 SFT. T-35
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846, 6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
L560-12 #201,GD910FT. T-3S
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846, 6010 Cd ICP Metals Analysis (RCRA)
SW-846, 6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
LS60-13 #201, GDI 7.5FT: T-3S
SW-846, 30S0 ICP/GFAAMetals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846, 6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/17/96 15:40
09/18/96 09:07
09/18/96 09:20
09/18/96 09:51
Page 3 of 30
L560-14 #201, GDI 10FT. T-35 09/19/96 09/18/9610:22
#
#
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
L560-1S #200, GDIS SFT. T-35
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
L560-16 #200, GD1510FT. T-35
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
LS60-17 #200, GD20 SFT. T-35
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-646, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
L560-18 #200, GD20 10FT. T-3S
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846, 6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/18/9612:59
09/18/9613:11
09/18/9613:40
09/18/9613:53
Page 4 of 30
il
L560-19 #200, GD12 5FT. T-3S 09/19/96 09/18/96 14:10
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
Ag
Be
Cd
Cr
Pb
ICP/GFAA Metals Digestion
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
L560-22 #200, GD6 SFT. T-35
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
LS60-23 #200, GD6 10FT. T-35
SW-846, 3050
SW-846,6010
SW-846, 6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
ICP/GF/VA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Cd ICP Metals Analysis (RCRA)
Cr ICP Metals Analysis (RCRA)
Pb ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
LS60-20 #200, GDI2 SFT. DUP. T-35
SW-846, 8260 Volatile Organics
L560-21 #200, GD1210FT. T-3S
09/19/96
Soil
09/19/96
09/18/96 14:10
09/18/96 14:34
09/18/96 15:00
09/18/96 15:20
Work Order Comments
There is a slight matrix interference for beryllium, chromium, and lead as exhibited in the
matrix spike results.
<^.u.1. .CP
Certified By
iikt /
Date
%
This is to certif that the following samples were analyzed using good laboratory practices to show
the folowing results:
Page 5 of 30
Listing of Results by Sample
m
m
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61*
96-18-4
120-82-1
95*3-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108*6-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
10: T-35 RINSE BLANK
Test Parameter
ICP METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
Result.
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
. u
u
u
u
39
u
10
u
u
u
130
u
u
u
u
0.9 J
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Units.
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/I
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1.1 JBug/l
U
U
U
u
u
u
u
u
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
Det.
Limit.
1
1
2.5
13
1.5
0.2
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
Lab ID: L56()-1 Collect Date:
Rep. Dil.
Limit Factor Method
5
5
13
63
7.5
0.5
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
[EPA 200.7]
1 EPA 200.7
1 EPA 200.7
1 EPA 200.7
1 EPA 200.7
1 EPA 200.7
1 EPA 245.1
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-&46, 8260
09/17/96 10:05
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/07/96 10:00
10/05/96 09:55
10/05/96 09:55
10/05/96 09:55
10/05/96 09:55
10/05/96 09:55
09/19/96 13:51
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/9618:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/9618:16
09/23/96 18:16
09/23/96 18:16
09/23/9618:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/9618:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/9618:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/9618:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/9618:16
Page 6 of 30
m
•
108-88-3 TOLUENE
156-60-5 TRANS-1,2-DICHLOROETHENE
10O61-O2-6 TRANS-1,3-DICHLOROPROPENE
79-01* TRICHLOROETHENE
75*9-4 TRICHLOROFLUOROMETHANE
75-01-4 VINYL CHLORIDE
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
0.3
0.2
0.2
0.3
0.3
0.4
10
10
10
10
10
10
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
8260
8260
8260
8260
8260
8260
MMR
MMR
MMR
MMR
MMR
MMR
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/96 18:16
09/23/9618:16
0 SamplelD: #201, GD3SFT. T-3S Lab ID: L560-2 Collect Date: 09/17/96 10:08
Det. Rep.
Test Parameter Result Units Limit Limit
ICP/GFAA METALS DIGESTION
BERYLLIUM 41 ug/g 0.1 0.6
CADMIUM 0.9 ug/g 0.1 0.6
CHROMIUM 19 ug/g 0.3 1.5
LEAD U ug/g 1.5 7.4
SILVER U ug/g 0.2 0.9
MERCURY 0.03 ug/g 0.02 0.05
630-20-6 1,1,1,2-TETRACHLOROETHANE U ug/kg 0.2 10
71-55-6 1,1,1-TRICHLOROETHANE U ug/kg 0.2 10
79-34-5 1,1,2,2-TETRACHLOROETHANE U ug/kg 0.3 10
79-00-5 1,1,2-TRICHLOROETHANE U ug/kg 0.2 10
75-34-3 1,1-DICHLOROETHANE U ug/kg 0.1 10
75-35-4 1,1-DICHLOROETHENE U ug/kg 0.6 10
563-58-6 1,1-DICHLOROPROPENE , U ug/kg 0.2 10
87-61-6 1,2,3-TRICHLOROBENZENE U ug/kg 0.2 10
96-18-4 1,2,3-TRICHLOROPROPANE U ugAg 0.2 10
120-82-1 1,2,4-TRICHLOROBENZENE U ugAg 0.2 10
95-63-6 1,2,4-TRIMETHYLBENZENE U ug/kg 0.2 10
96-12-8 1,2-DlBROMO-3-CHLOROPROPAN U ugAg 0.2 10
106-93-4 1,2-DIBROMOETHANE U ugAg 0.2 10
95-50-1 1,2-DICHLOROBENZENE U ugAg 0.1 10
107-06-2 1,2-DICHLOROETHANE U ug/kg 0.2 10
78-87-5 1,2-DICHLOROPROPANE U ug/kg 0.2 10
108-67-8 1,3,5-TRIMETHYLBENZENE U ugAg 0.2 10
541-73-1 1,3-DICHLOROBENZENE U ugAg 0.2 10
142-28-9 1,3-DICHLOROPROPANE U ugAg 0.2 10
106-46-7 1,4-DICHLOROBENZENE U ugAg 0.2 10
590-20-7 2,2-DICHLOROPROPANE U ugAg 0.2 10
78-93-3 2-BUTANONE U ugAg 10 10
95-49-8 2-CHLOROTOLUENE U ugAg 0.2 10
591-78-6 2-HEXANONE U ug/kg 10 10
106-43-4 4-CHLOROTOLUENE U ugAg 0.2 10
99-87-6 4-ISOPROPYLTOLUENE U ug/kg 0.2 10
108-10-1 4-METHYL-2-PENTANONE U ug/kg 10 10
67-64-1 ACETONE U ug/kg 10 10
71-43-2 BENZENE U ug/kg 0.2 10
108-86-1 BROMOBENZENE U ugAg 0.2 10
74-97-5 BROMOCHLOROMETHANE U ug/kg 0.2 10
75-27-4 BROMODICHLOROMETHANE U ugAg 0.3 10
75-25-2 BROMOFORM U ugAg 0.1 10
74-83-9 BROMOMETHANE U ugAg 0.4 10
56-23-5 CARBON TETRACHLORIDE U ugAg 0.3 10
108-90-7 CHLOROBENZENE U ug/kg 0.2 10
75-00-3 CHLOROETHANE U ug/kg 0.4 10
67-66-3 CHLOROFORM U ug/kg 0.4 10
74-87-3 CHLOROMETHANE U ug/kg 06 10
156-59-4 CIS-1,2-DICHLOROETHENE U ug/kg 0.2 10
10061-01-5 ClS-1,3-DICHLOROPROPENE U ug/kg 0.2 10
124-48-1 DIBROMOCHLOROMETHANE U ug/kg 0.3 10
74-95-3 DIBROMOMETHANE U ugAg 0.2 10
75-71-8 DICHLORODIFLUOROMETHANE U ugAg 0.2 10
100-41-4 ETHYLBENZENE U ugAg 0.3 10
87-68-3 HEXACHLOROBUTADIENE U ug/kg 0.2 10
98-82-8 ISOPROPYLBENZENE U ugAg 0.2 10
108-38-3 M,P-XYLENE U ug/kg 0.2 10
75-09-2 METHYLENE CHLORIDE 1.2 JBugAg 0.3 10
104-51-8 N-BUTYLBENZENE U ug/kg 0.2 10
103-65-1 N-PROPYLBENZENE U ug/kg 0.2 10
91-20-3 NAPHTHALENE U ug/kg 0.2 10
95-47-6 O-XYLENE U ug/kg 0.2 10
Oil.
Factor Method Analvst Test Date
SW-846,3050 KWB 10/10/96 09:30
1 SW-846,6010 KWB 10/10/9612:18
1 SW-846,6010 KWB 10/10/96 12:18
1 SW-846,6010 KWB 10/10/96 12:18
1 SW-846,6010 KWB 10/10/96 12:18
1 SW-846,6010 KWB 10/10/96 12:18
1 SW-846,7471A CRS 10/17/96 09:00
1 SW-846,8260 MMR 09/25/9613:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/9613.58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/9613:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/9613:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MAR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/9613:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MAR 09/25/9613:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13.58
1 SW-846,8260 MAR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/9613:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MAR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/9613:58
1 SW-846,8260 MMR 09/25/9613:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MAR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
1 3W-846,8260 MMR 09/25/96 13:58
1 SW-846,8260 MMR 09/25/96 13:58
Page 7 of 30
135-98-8
100-42-5
98-06-6
127-18-4
108*8-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
[Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108*6-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE .
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
O:#201,GD3 10FT. T-35
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4JUIETHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
U
U
U
U
U
U
U
U
U
U
Result
0.3
0.4
14
U
U
0.04
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.1
0.1
0.3
1.5
0.2
0.02
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.6
0.6
1-5
7.5
0.9
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
L56i)-3 Collect Date:
Dil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-646, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-646, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/25/96 13:58
09/25/96 13:58
09/25/96 13:58
09/25/96 13:58
09/25/96 13:58
09/25/96 13:58
09/25/96 13:58
09/25/96 13:58
09/25/96 13:58
09/25/9613:58
09/17/9610:20
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
10/10/96 09:30
10/10/96 12:20
10/10/96 12:20
10/10/96 12:20
10/10/96 12:20
10/10/96 12:20
10/17/96 09:04
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
Page 8 of 30
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156*0-5
10061-02-6
79-01-6
75-69-4
75-01-4
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
j Sample 10: #201, GD14 7FT. T-35
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58*
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE,
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DlBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Result
0.4
0.2
14
U
U
0.02
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.1
0.1
0.3
1*
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.6
0.6
1.6
8
0.96
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
M^R
MMR
MAR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
L560-4 Collect Date:
Dil.
Facitor Method
SW-846, 3050
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/96 14:33
09/25/9614:33
09/25/96 14:33
09/25/96 14:33
09/17/96 11:01
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Ml/IR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MAR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
10/10/96 09:30
10/10/96 12:23
10/10/96 12:23
10/10/96 12:23
10/10/9612:23
10/10/96 12:23
10/17/96 09:15
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/9615:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/9615:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/9615:08
09/25/96 15:08
09/25/96 15:08
09/25/9615:08
Page 9 of 30
87-68-3
98-82-8
108-38-3
75-09-2
104-51*
103-65-1
91-20-3
95-47-6
135-98*
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78*
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
0: #201, GDI 41 OFT. T-35
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMb I HYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
U
U
U
ug/kg
ug/kg
ug/kg
1.4 JB ug/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
u
Result
0.3
0.5
13
U
U
0.01
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
Units
ug'g
ug/g
ug/g
ug/g
ug'g
ug/g
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Umit
0.1
0.1
0.3
1.6
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.6
0.6
1.6
7.9
0.95
0.03
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
L560-5 Collect Date:
Dil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15.08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/25/96 15:08
09/17/96 11:22
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
- MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/10/96 09:30
10/10/96 12:46
10/10/96 12:46
10/10/96 12:46
10/10/96 12:46
10/10/96 12:46
10/17/96 09:19
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/9615:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
Page 10 of 30
124-48-1
74-95-3
75-71*
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98*
100-42-5
98-06-6
127-18-4
108-88-3
• 156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
D:#201,GD7SFT. T-35
Test Parameter
ICP/GFAAMETALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Result
15
0.7
16
U
U
0.02
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.1
0.1
0.3
1.6
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.6
0.6
1.6
7.8
0.9
0.03
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
•SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
L560-6 Collect Date:
Dil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/9615:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
09/25/96 15:43
39/17/9614:22
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MAR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/10/96 09:30
10/10/96 12:49
10/10/96 12:49
10/10/96 12:49
10/10/96 12:49
10/10/96 12:49
10/17/96 09:23
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/9616:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
Page 11 of 30
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
10042-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #201, GD7 10FT. T-35
630-20-6
71-55-6
79-34-5
794)0-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78*
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
U
U
U
U
U
U
U
U
U
U
U
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
2.2 JB ug/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Result
6.7
0.96
15
2.1
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.1
0.1
0.3
1.5
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab 10:
Rep.
Limit
0.6
0.6
1.5
7.6
0.9
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
. SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
L560-7 Collect Date:
Oil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
09/25/96 16:18
39/17/9614:52
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MMR
MMR
MMR
IWMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
10/10/96 09:30
10/10/96 12:52
10/10/96 12:52
10/10/96 12:52
10/10/96 12:52
10/10/96 12:52
10/17/96 09:27
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
Page 12 Of 30
#
74-83-9
56-23-5
108-90-7
754)0-3
67*6-3
74*7-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82*
108-38-3
754)9-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
984)6-6
127-18-4
108-88-3
156-60-5
10061-02-6
794)1-6
75-69-4
754)1-4
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #201, GD11 SFT. T-35
630-20-6
71-55-6
79-34-5
794)0-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120*2-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78*
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DiBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
1.8 JB ugAg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Result
0.3
0.4
11
U
U
0.1
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.1
0.1
0.3
1.5
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.6
0.6
1.5
7.6
0.9
0.03
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/9616:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
09/25/96 16:52
L56()-8 Collect Date: 09/17/96 15:20
Dil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-S46, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MAR
MMR
- MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
H*/IR
MMR
MMR
Hffl^R
MMR
MAR
MAR
MMR
MMR
MMR
MMR
Test Date
10/10/96 09:30
10/10/9612:55
10/10/96 12:55
10/10/96 12:55
10/10/96 12:55
10/10/96 12:55
10/17/96 09:31
09/25/96 17:27
09/25/96 17:27
09/25/9617:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/9617:27
09/25/9617:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/9617:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/9617:27
09/25/96 17:27
09/25/9617:27
Page 13 of 30
^
108-86-1 BROMOBENZENE
74-97-5 BROMOCHLOROMETHANE
75-27-4 BROMODICHLOROMETHANE
75-25-2 BROMOFORM
74-83-9 BROMOMETHANE
56-23-5 CARBON TETRACHLORIDE
108-90-7 CHLOROBENZENE
754)0-3 CHLOROETHANE
67-66-3 CHLOROFORM
74-87-3 CHLOROMETHANE
156-59-4 CIS-1,2-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1 DIBROMOCHLOROMETHANE
74-95-3 DIBROMOMETHANE
75-71-8 DICHLORODIFLUOROMETHANE
100-41-4 ETHYLBENZENE
87-68-3 HEXACHLOROBUTADIENE
98-82-8 ISOPROPYLBENZENE
108-38-3 M,P-XYLENE
75-09-2 METHYLENE CHLORIDE
104-51 -8 N-BUTYLBENZENE
103-66-1 N-PROPYLBENZENE
91-20-3 NAPHTHALENE
95-47-6 O-XYLENE
135-98-8 SEC-BUTYLBENZENE
100-42-5 STYRENE
98456-6 TERT-BUTYLBENZENE
127-18-4 TETRACHLOROETHENE
108-88-3 TOLUENE
156-60-5 TRANS-1,2-DICHLOROETHENE
100614)2-6 TRANS-1,3-DICHLOROPROPENE
794)1-6 TRICHLOROETHENE
75-69-4 TRICHLOROFLUOROMETHANE
75-01-4 VINYL CHLORIDE
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MAR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/96 17:27
09/25/9617:27
09/25/96 17:27
09/25/96 17:27
09/25/9617:27
09/25/96 17:27
09/25/9617:27
09/25/96 17:27
09/25/96 17:27
09/25/9617:27
09/25/96 17:27
09/25/96 17:27
09/25/9617:27
09/25/96 17:27
09/25/96 17:27
09/25/9617:27
09/25/96 17:27
09/25/9617:27
09/25/96 17:27
09/25/96 17:27
09/25/9617:27
09/25/9617:27
09/25/96 17:27
09/25/9617:27
Sample ID: #201, GD11 SFT. DUP. T-3S Lab ID: L560-9 Collect Date: 09/17/96 15:20
Oet.
Test Parameter.
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1 Sample ID: #201, GD11 10FT. T-35
630-20-6
71-55-6
79-34-5
794X)-6
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-6
106-93-4
95-50-1
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
Result
0.3
0.7
12
U
. U
0.04
Result
0.5
0.2
12
U
U
0
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
Limit
0.1
0.1
0.3
1.5
0.2
0.01
Det.
Limit
0.1
0.1
0.3
1.3
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
Limit
0.6
0.6
1.5
7.5
0.9
0.04
Lab ID:
Rep.
Limit
0.5
0.5
1.3
6.6
0.8
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Fact'
1
1
1
1
1
1
>r Method.
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
Analyst
KWB
KWB
KWB
KWB
KWB
KWB
CRS
Test Date
10/10/96 09:30
10/10/9612:57
10/10/96 12:57
10/10/96 12:57
10/10/96 12:57
10/10/96 12:57
10/17/96 09:39
L560-10 Collect Date: 09/17/96 15:40
Dil.
Factor Method
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MAR
MMR
MMR
MAR
Test Date
10/10/96 09:30
10/10/96 13:11
10/10/96 13:11
10/10/9613:11
10/10/96 13:11
10/10/96 13:11
10/17/96 09:46
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/9618:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
Page 14 of 30
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74*7-3
156-59-4
100614)1-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98*6*
127-18-4
108*8-3
156-60-5
10061-02-6
794)1-6
75-69-4
754)1-4
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
24:HLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #201, GD9 SFT." T-3S
630-20-6
71-55-6
79-34-5
794)0-5
75-34-3
75-35-4
563-58-6 '
87-61-6
96-18-4
120-82-1
Test Parameter
ICP/GFAAMETALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
. u
u
u
u
u
u
u
u
u
u
u
u
Result
0.7
0.2
16
U
u
0.03
U
U
U
U
u
u
u
u
u
u
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
Units
ug'g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.1
0.1
0.3
1.6
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.7
0.7
1.6
8.2
0.98
0.03
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/9618:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/9618:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
09/25/96 18:02
LS&3-11 Collect Date: 09/18/96 09:07
Oil.
Factor Method
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
Test Date
10/10/96 09:30
10/10/96 13:14
10/10/96 13:14
10/10/96 13:14
10/10/96 13:14
10/10/96 13:14
10/17/96 09:50
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/9618:37
09/25/96 18:37
09/25/96 18:37
Page 15 of 30
m
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
754)0-3
67-66-3
74-87-3
156-59-4
100614)1-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
754)9-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
984)6-6
127-18-4
108-88-3
156-60-5
100614)2-6
79-01-6
75-69-4
754)1-4
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON 1 fc 1 RACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE .
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #201, GD9 10FT. T-35
630-20*
71-55-6
79-34-5
794)0-5
75-34-3
75-35-4
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
1.3 JBugAg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Result
0.3
0.5
11
U
U
U
U
U
U
U
U
U
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.1
0.1
0.3
1.5
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0*
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
06
0.6
1.5
7.4
0.9
0.03
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MAR
MMR
MMR
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/9618:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
09/25/96 18:37
L560-12 Collect Date: 09/18/96 09:20
Dil.
Facte r Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-S46, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MAR
MMR
MMR
MMR
Test Date
10/10/96 09:30
10/10/96 13:17
10/10/96 13:17
10/10/96 13:17
10/10/96 13:17
10/10/96 13:17
10/17/96 09:54
09/25/96 19:12
09/25/9619:12
09/25/96 19:12
09/25/9619:12
09/25/96 19:12
09/25/96 19:12
Page 16 of 30
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12*
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-»3-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
100614)1-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
984)6-6
127-18-4
108-88-3
156-60-5
100614)2-6
79-01-6
75-69-4
75-01-4
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #201, GDI 7.5FT. T-35
630-20-6
71-55-6
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Result
0.1
0.6
22
u
u
0.02
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/lcg
ugAg
ugAg
ugAg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ug/kg
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.1
0.1
0.3
1.6
0.2
0.02
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10
10
10
10
10
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
Lab ID: LS6
Rep. 0
Limit Fac
0.6 1
0.6 1
1.6 1
8 1
0.96 1
0.05 1
10 1
10 1
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
t SW-846,8260
1 SW-846,8260
1 SW-846,8260
I SW-846,8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MAR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MAR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/9619:12
09/25/96 19:12
09/25/96 19:12
09/25/9619:12
09/25/96 19:12
09/25/9619:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/9619:12
09/25/9619:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/9619:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/9619:12
09/25/96 19:12
09/25/9619:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/9619:12
09/25/9619:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/2Sr96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
09/25/96 19:12
0-13 Collect Date: 09/18/96 09:51
1.
-tor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
Analyst
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
Test Date
10/10/96 09:30
10/10/96 13:47
10/10/96 13:47
10/10/96 13:47
10/10/96 13:47
10/10/96 13:47
10/17/9610:02
09/25/96 19:47
09/25/96 19:47
Page 17 of 30
•
79-34-5
794)0-5
75-34-3
75-35-4
563-58*
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74*3-9
56-23-5
108-90-7
754)0-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98*2-8
108-38-3
754)9-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98*
100-42-5
984)6-6
127-18-4
108-88-3
156-60-5
100614)2-6
79-01-6
75-69-4
75-01-4
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DlBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
24:HLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOME 1 HANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-)CYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #201, GDI 10FT. T-35
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
1.7 JB ugAg
U
U
U
U
U
U
U
U
U
U
u
u
u
u
Result
0.1
0.5
25
U
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
04
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.1
0.1
0.3
1.6
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.6
0.6
1.6
7.7
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/9619:47
09/25/96 19:47
09/25/9619:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/9619:47
09/25/9619:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/9619:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/9619:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
09/25/96 19:47
LS60-14 Collect Date: 09/18/96 10:22
Oil.
Facte
1
1
1
1
r Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW*46,6010
SW-846, 6010
Analyst
KWB
KWB
KWB
KWB
KWB
Test Date
10/14/96 00:00
10/15/96 13:56
10/15/96 13:56
10/15/96 13:56
10/15/96 13:56
Page 18 of 30
630-20-6
71-55-6
79-34-5
794K)-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78*7-5
108*7-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97*
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
754)0-3
67-66-3
74-87-3
156-59-4
100614)1-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
754)9-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
984)6-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01*
75-69-4
754)1-4
SILVER
MERCURY
1,1,1,2-1 fc 1 KACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
44\4ETHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #200, GDIS SFT. T-35
Test Parameter
ICP/GFAA METALS DIGESTION
0.2
0.02
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
-u
u
u
u
u
u
Result
ug/g
ug/g
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/lcg
ugAg
Units
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.9
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
KWB
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/15/96 13:56
10/17/96 10:06
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
09/25/96 20:22
L560-15 Collect Date: 09/18/96 12:59
Oil.
F.3ctor Method
SW-846, 3050
Analvsl
KWB
Test Date
10/14/96 00:00
Page 19 of 30
#
630-20-6
71-55-6
79-34-5
794)0-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78-87-5
108*7*
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106^3-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
754)0-3
67-66-3
74-87-3
156-59-4
100614)1-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
754)9-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
984)6-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-11T RACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DlBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
0.6
0.2
17
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.3 JB ug/kg
U
U
U
U
U
U
U
U
U
U
U
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.1
0.1
0.3
1*
0.2
0.02
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
0.6
0.^
1.6
8
0.96
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/15/96 13:59
10/15/96 13:59
10/15/96 13:59
10/15/9613:59
10/15/96 13:59
10/17/96 10:10
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
09/25/96 20:56
Page 20 of 30
1 Sample
630-20-6
71-55-6
79-34-5
794)0-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78*7*
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
100614)1-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
754)9-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
ID: #200, GDI 51 OFT. T-3S
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DlBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
24:HLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
Result
1.9
0.2
22
U
U
0.3
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
. u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
1.1 JB ugAg
U
U
U
U
U
U
U
u
u
u
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
Det.
Limit
0.1
0.1
0.3
1.5
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
Lab ID:
Rep.
Limit
0.6
0.6
1.5
7.4
0.9
0.03
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
LS60-16 Collect Date:
Dil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/18/9613:11
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MVIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/14/96 00:00
10/15/96 14.02
10/15/96 14:02
10/15/96 14:02
10/15/96 14:02
10/15/96 14:02
10/17/96 10:14
09/26/96 11:01
09/26/9611:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/9611:01
09/26/96 11:01
09/26/9611:01
09/26/96 11:01
09/26/96 11:01
09/26/9611:01
09/26/96 11.01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/9611:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/9611:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/9611:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/9611:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/9611:01
09/26/96 11:01
09/26/96 11.01
09/26/9611:01
09/26/96 11:01
09/26/96 11:01
09/26/9611:01
09/26/96 11:01
Page 21 of 30
100614)2-6 TRANS-1,3-DICHLOROPROPENE
794)1-6 TRICHLOROETHENE
75-69-4 TRICHLOROFLUOROMETHANE
754)1-4 VINYL CHLORIDE
U ug/kg
U ugAg
U ugAg
U ugAg
0.2
0.3
0.3
0.4
10
ib
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
09/26/96 11:01
09/26/96 11:01
09/26/96 11:01
09/26/96 11.01
Sample ID: #200, GD20 SFT. T-35 Lab ID: L560-17 Collect Date: 09/18/96 13:40
•
Oet. Rep.
Test Parameter Result Units Limit Limit
ICP/GFAA METALS DIGESTION
BERYLLIUM 0.6 ug/g 0.1 0.6
CADMIUM 0.2 ug/g 0.1 0.6
CHROMIUM 16 ug/g 0.3 1.6
LEAD U ug/g 1.6 8
SILVER U ug/g 0.2 0.95
MERCURY 0.03 ug/g 0.01 0.04
630-20-6 1,1,1,2-TETRACHLOROETHANE U ug/kg 0.2 10
71-55-6 1,1,1-TRICHLOROETHANE U ugAg 0.2 10
79-34-5 1,1,2,2-TETRACHLOROETHANE U ug/kg 0.3 10
794X)-5 1,1,2-TRICHLOROETHANE U ug/kg 0.2 10
75-34-3 1,1-DICHLOROETHANE U ug/kg 0.1 10
75-35-4 1,1-DICHLOROETHENE U ug/kg 0.6 10
563-58-6 1,1-DICHLOROPROPENE U ug/kg 0.2 10
87-61-6 1,2,3-TRICHLOROBENZENE U ug/kg 0.2 10
96-18-4 1,2,3-TRICHLOROPROPANE U ug/kg 0.2 10
120-82-1 1,2,4-TRICHLOROBENZENE U ug/kg 0.2 10
95-63* 1,2,4-TRIMETHYLBENZENE U ug/kg 0.2 10
96-12-8 1,2-DIBROMO-3-CHLOROPROPAN U ug/kg 0.2 10
106-93-4 1,2-DIBROMOETHANE U ug/kg 0.2 10
95-50-1 1,2-DICHLOROBENZENE U ug/kg 0.1 10
1074)6-2 1,2-DICHLOROETHANE U ugAg 0.2 10
78-87-5 1,2-DICHLOROPROPANE U ugAg 0.2 10
108*7-8 1,3,5-TRIMETHYLBENZENE U ugAg 0.2 10
541-73-1 1,3-DICHLOROBENZENE U ugAg 0.2 10
142-28-9 1,3-DICHLOROPROPANE U ug/kg 0.2 10
106-46-7 1,4-DICHLOROBENZENE U ugAg 0.2 10
590-20-7 2,2-DICHLOROPROPANE U ugAg 0.2 10
78-93-3 2-BUTANONE U ugAg 10 10
95-49* 2-CHLOROTOLUENE U ugAg 0.2 10
591-78-6 2-HEXANONE U ug/kg 10 10
106-43-4 4-CHLOROTOLUENE U ug/kg 0.2 10
99-87-6 4-ISOPROPYLTOLUENE U ug/kg 0.2 10
108-10-1 4-METHYL-2-PENTANONE U ugAg 10 10
67-64-1 ACETONE U ugAg 10 10
71-43-2 BENZENE U ug/kg 0.2 10
108-86-1 BROMOBENZENE U ug/kg 0.2 10
74-97-5 BROMOCHLOROMETHANE U ug/kg 0.2 10
75-27-4 BROMODICHLOROMETHANE U ug/kg 0.3 10
75-25-2 BROMOFORM U ug/kg 0.1 10
74-83-9 BROMOMETHANE U ug/kg 0.4 10
56-23-5 CARBON TETRACHLORIDE U ugAg 0.3 10
108-90-7 CHLOROBENZENE U ug/kg 0.2 10
754)0-3 CHLOROETHANE U ug/kg 0.4 10
67-66-3 CHLOROFORM U ug/kg 0.4 10
74-87-3 CHLOROMETHANE U ugAg 0.6 10
156-59-4 CIS-1,2-DICHLOROETHENE U ug/kg 0.2 10
10061-01-5 CIS-1,3-DICHLOROPROPENE U ug/kg 0.2 10
124-48-1 DIBROMOCHLOROMETHANE U ug/kg 0.3 10
74-95-3 DIBROMOMETHANE U ug/kg 0.2 10
75-71-8 DICHLORODIFLUOROMETHANE U ug/kg 0.2 10
100-41-4 ETHYLBENZENE U ug/kg 0.3 10
87-68-3 HEXACHLOROBUTADIENE U ugAg 0.2 10
98-82-8 ISOPROPYLBENZENE U ug/kg 0.2 10
108-38-3 M,P-XYLENE U ug/kg 0.2 10
754)9-2 METHYLENE CHLORIDE U ug/kg 0.3 10
104-51-8 N-BUTYLBENZENE U ugAg 0.2 10
103-65-1 N-PROPYLBENZENE U ug/kg 0.2 10
91-20-3 NAPHTHALENE U ugAg 0.2 10
95-47-6 O-XYLENE U ug/kg 0.2 10
135-98-8 SEC-BUTYLBENZENE U ug/kg 0.2 10
100-42-5 STYRENE U ug/kg 0.2 10
Oil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Test Date
10/14/96 00:00
10/15/96 14:05
10/15/96 14:05
10/15/96 14:05
10/15/96 14:05
10/15/96 14:05
10/17/9610:18
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/9611:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/9611:36
09/26/9611:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/9611:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/9611:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/9611:36
09/26/96 11:36
09/26/9611:36
09/26/9611:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/9611:36
09/26/96 11:36
09/26/9611:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/9611:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/9611:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/9611:36
09/26/96 11:36
09/26/9611:36
Page 22 of 30
98-06-6
127-18-4
108-88-3
156*0-5
100614)2-6
794)1*
75*9-4
75431-4
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #200, GD201 OFT. T-35
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-9O-7
754)0-3
67-66-3
74-87-3
156-59-4
10061-01-5
124^8-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
754)9-2
104-51-8
103-65-1
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DlBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
U
U
U
U
U
U
U
U
Result
0.3
0.6
17
U
U
0.02
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug'g
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
1.4 JB ugAg
U
U
ugAg
ug/kg
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.1
0.1
0.3
1.6
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
10
10
10
10 .
10
10
10
10
Lab ID:
Rep.
Limit
06
0.6
1.6
8
0.95
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
L560-18 Collect Date:
Oil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/26/9611:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/96 11:36
09/26/9611:36
09/26/96 11:36
09/26/96 11:36
09/18/9613:53
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/14/96 00:00
10/15/96 14:08
10/15/96 14:08
10/15/96 14:08
10/15/96 14:08
10/15/96 14:08
10/17/96 10:25
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/9612:11
09/26/9612:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/9612:11
09/26/96 12:11
09/26/96 12:11
09/26/9612:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/9612:11
09/26/96 12:11
09/26/9612:11
09/26/96 12:11
09/26/9612:11
09/26/9612:11
09/26/96 12:11
09/26/96 12:11
09/26/9612:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/9612:11
09/26/96 12:11
09/26/9612:11
09/26/9612:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
Page 23 of 30
m
91-20-3
95-47-6
135-98-8
100-42-5
984)6-6
127-18-4
108*8-3
156-60-5
10061-02-6
794)1-6
75-69-4
754)1-4
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87*
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
0: #200, GDI2 SFT. T-35
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
U
U
U
U
U
U
U
U
U
U
U
U
Result
0.3
0.8
17
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.1
0.1
0.3
1.7
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.7
0.7
1.7
8.3
0.99
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
1.560-19 Collect Date:
Dill.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/26/9612:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/26/9612:11
09/26/96 12:11
09/26/96 12:11
09/26/96 12:11
09/18/96 14:10
Analyst Test Date.
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
-MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/14/96 00:00
10/15/96 14:11
10/15/96 14:11
10/15/9614:11
10/15/96 14:11
10/15/96 14:11
10/17/9610:29
09/26/96 12:46
09/26/96 12:46
09/26/9612:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/9612:46
09/26/96 12:46
09/26/96 12:46
09/26/9612:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/9612:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/9612:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
Page 24 of 30
n
108-38-3
754)9-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-6
98-06-6
127-18-4
108-88-3
156-60-5
100614)2-6
794)1-6
75-69-4
754)1-4
1 Sample
CAS
Numbei
630-20-6
71-55-6
79-34-5
794)0-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
754)0-3
67-66-3
74-87-3
156-59-4
100614)1-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
754)9-2
104-51-8
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
D: #200, GD12 SFT. DUP. T-3S
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
ClS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
U ugAg
3.5 JB ugAg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Result
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
U
u
u
u
u
u
u
u
4.3 J
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
3.3 JE
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
Units
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
LS60-20 Collect Date:
Dill.
Factor Method
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/96 12:46
09/26/9612:46
09/26/96 12:46
09/18/96 14:10
Analyst Test Date
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
lulMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/9613:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/9613:21
09/26/96 13:21
09/26/96 13:21
09/26/9613:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/9613:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/9613:21
09/26/96 13:21
Page 25 of 30
•
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
984)6*
127-18-4
108-88-3
156-60-5
100614)2-6
794)1-6
75-69-4
754)1-4
1 Sample
630-20-6
71-55-6
79-34-5
794)0-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
100614)1*
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
0: #200, GDI 21 OFT. T-35
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DlBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
U
U
U
U
U
U
U
U
U
U
U
U
u
Result
u
0.5
16
U
U
0.02
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/lcg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.1
0.1
0.3
1.6
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.6
0.6
1.6
7.9
0.9
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
L560-21 Collect Date:
Oil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/9613:21
09/26/9613:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/26/96 13:21
09/18/9614:34
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/14/96 00:00
10/15/96 14:25
10/15/96 14:25
10/15/96 14:25
10/15/96 14:25
10/15/96 14:25
10/17/96 10:33
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/9613:56
09/26/96 13:56
09/26/96 13:56
09/26/9613:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/9613:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/9613:56
09/26/96 13:56
09/26/96 13:56
09/26/9613:56
09/26/96 13:56
09/26/9613:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/9613.56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/9613:56
09/26/96 13:56
09/26/96 13:56
Page 26 of 30
•
#
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
984)6-6
127-18-4
108-88-3
156*0-5
100614)2-6
794)1-6
75-69-4
754)1-4
1 Sample
630-20-6
71-55-6
79-34-5
794)0-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
754X)-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETH/WJE
VINYL CHLORIDE
D: #200, GD6 SFT. T-3S
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE .
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE .
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
24:HLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
U
u
ug/kg
ug/kg
3.3 JB ug/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Result
0.2
U
24
U
U
0.03
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.1
0.1
0.3
1.4
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
0.5
1.4
6.8
0.8
0.03
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
L56I3-22 Collect Date:
Dill.
Facior Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/26/9613:56
09/26/9613:56
09/26/9613:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/9613:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/26/96 13:56
09/18/96 15:00
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
M^R
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Ml/IR
MMR
MUIR
MMR
MMR
MMR
- MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
M^^R
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MUIR
MMR
10/14/96 00:00
10/15/96 14:28
10/15/96 14:28
10/15/96 14:28
10/15/96 14:28
10/15/96 14:28
10/17/9611:49
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/9614:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
Page 27 of 30
•
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
754)9-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
984)6-6
127-18-4
108-88-3
156-60-5
100614)2*
79*1*
75-69-4
754)1-4
1 Sample
630-20-6
71-55-6
79-34-5
794X)-5
75-34-3
75-35-4
563-58*
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
754X)-3
67-66-3
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
ID:#200, GD6 10FT. T-3S
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DlBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
U
U
U
u
u
u
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
6.9 JB ugAg
U
U
U
U
U
U
u
u
u
u
u
u
u
u
Result
0.1
0.6
18
U
U
0.03
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.1
0.1
0.3
1.5
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.6
0.6
1.5
7.6
0.9
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
LS60-23 Collect Date:
Dil.
Facitor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
09/26/96 14:30
39/18/96 15:20
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MUIR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/14/96 00:00
10/15/96 14:30
10/15/96 14:30
10/15/96 14:30
10/15/96 14:30
10/15/96 14:30
10/17/96 11:57
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/9615:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/9615:05
09/26/96 15:05
09/2B796 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/9615:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
Page 28 of 30
•
74*7-3
156-59-4
100614)1-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
754)9-2
104-51-8
103-65-1
91-20-3
9S47-6
135-98-8
100-42-5
984)6-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
U
U
U
U
U
U
U
U
U
U
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
7.2 JB ugAg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/26/96 15:05
09/26/9615:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
09/26/96 15:05
Page 29 of 30
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected
but was below the detection limit.
B This flag is used when an analyte is found in the blank as well as the sample
Det. Limit Method Detection Limit (approximately three times the signal noise level)
Rep. Limit Reporting Limit is normally the value of the lowest standard run with the
analysis. The value is approximately 5 to 10 times the Method Detection Limit.
Dil. Factor Dilution Factor - The prepared sample was diluted by this factor because the
sample was too concentrated or due to other interferences in the sample matrix.
Any dilution factor causes an appropriate increase in the method detection limit
and reporting limit.
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This
flag is used either when estimating a concentration for tentatively identified compounds or
when the data indicated the presence of a compound that meets the identification criteria
but the result is less than the specified reporting limit (e.g. 3 J with a reporting limit of 10)
Page 30 of 30
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Fiequested
Friday, November 08,1996
TESTED FOR Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp,UT 84322
Frank Walker
Project: Solid Waste Mgmt Invest.
Login Number L553
Lab Number Client Number
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-5445
800-863-8080
Test Requested Description
Received
Matrix
Collect Date/Time
L553-1 #662
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-a46, 6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7060
SW-846, 7471A
SW-846, 7740
SW-846, 8260
L553-2 #662,
GD1 SFT. M-15A DRYWELL
ICP/GFAA Metals Digestion
Ag ICP Melals Analysis (RCRA)
Al
Ba
Be
Cd
Cr
Cu
Nl
Pb
Sb
Zn
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Melals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Selenium Analysis (RCRA)
Volatile Organics
GDI 5FT. DUP. M-15A DRYWELL
09/16/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/16/96
09/16/96 15:07
09/16/96 15:07
SW-846, 8260 Volatile Organics Soil
Page 1 of 21
#
1 LSS3-3 #662
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7060
SW-846, 7471A
SW-846, 7740
SW-846, 8260
1 L5S3-4 #616
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
1 L5S3-S #616,
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
L553-6 #616,
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
LS53-7 #616,
SW-846, 3050
SW-846, 6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
GD1 10FT. M-1 SA DRYWELL
ICP/GFAA Metals Digestion
Ag ICP Metals Analysis (RCRA)
Al
Ba
Be
Cd
Cr
Cu
Ni
Pb
Sb
Zn
ICP Melals Analysis (RCRA)
ICP Melals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Melals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Melals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Selenium Analysis (RCRA)
Volatile Organics
GD910FT. M-137B
Cd
Cr
Pb
ICP/GFAA Metals Digestion
ICP Metals Analysis (RCRA)
ICP Melals Analysis (RCRA)
ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
GD91SFT. M-137B
Cd
Cr
Pb
ICP/GFAA Metals Digestion
ICP Metals Analysis (RCRA)
ICP Melals Analysis (RCRA)
ICP Melals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
GDI 6 10FT. M-137B
Cd
Cr
Pb
ICP/GFAA Metals Digestion
ICP Melals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Melals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
GDI 61 SFT. . M-137B
Cd
Cr
Pb
ICP/GFAA Metals Digestion
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
09/16/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/16/96
Soil
Soil
Soil
Soil
Soil
Soil
09/16/96
Soil
Soil
Soil
Soil
Soil
Soil
09/16/96
Soil
Soil
Soil
Soil
Soil
Soil
09/16/96
Soil
Soil
Soil
Soil
Soil
Soil
09/16/96 15:15
09/16/96 09:32
09/16/96 09:42
09/16/96 10:13
09/16/96 10:27 |
Page 2 of 21
L5S3-8 #616, GDI 41 OFT. M-137B 09/16/96 09/16/96 10:56
•
•
•
SW-846, 3050 ICP/GFAA Melals Digestion
SW-846,6010 Cd ICP Melals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Melals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
L553-9 #616, GD1415FT. M-137B
SW-846, 3050 ICP/GFAA Melals Digestion
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Melals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
LS53-10 #616, GD210FT. M-137B
SW-846, 3050 ICP/GFA>A Melals Digestion
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Melals Analysis (RCRA)
SW-846, 7471A CVMercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
L553-11 #616, GD210FT. DUP. M-137B
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846, 6010 Cd ICP Melals Analysis (RCRA)
SW-846,6010 Cr ICP Melals Analysis (RCRA)
SW-846,6010 Pb ICPMetals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
LSS3-12 #616, GD215FT. M-137B
SW-846, 3050 ICP/GFAA Melals Digestion
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
L553-13 #260, SFT. M-S3-BP
SW 846, 9045 pH Electrode Measurement
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
SW-846, 8270 Semi-Volatile Organics
L5S3-14 #260, 10FT. M-53-BP
SW 846, 9045 pH Electrode Measurement
SW-846, 3050 ICP/GFAA Melals Digestion
SW-846, 6010 Cd ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
SW-846, 8270 Semi-Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
09/16/96
Soil
Soil
Soil
Soil
Soil
Soil
09/16/96
Soil
Soil
Soil
Soil
Soil
Soil
09/16/96
Soil
Soil
Soil
Soil
Soil
09/16/96
Soil
Soil
Soil
Soil
Soil
Soil
09/16/96
Soil
Soil
Soil
Soil
Soil
Soil
09/16/96
Soil
Soil
Soil
Soil
Soil
Soil
09/16/9611.04
09/16/96 11:40
09/16/96 11:40
09/16/96 11:52
09/16/96 13:45
09/16/96 13:57
Page 3 of 21
y Certified By Date
This is to certify that the following samples were analyzed using good laboratory practices to show
the folowing results:
Page 4 of 21
Listing of Results by Sample
#
•
1 Sample ID: #662, GD1 SFT.
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
Test Parameter
ICP/GFAA METALS DIGESTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
SELENIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DlBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE ,
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
ClS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROME 1 HANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
M-1 S/\ DRYWELL
Result
13900
U
98
0.7
0.3
19
8.6
U
15
U
60
130
0.02
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
Oet.
Limit
1.3
26
0.05
0.1
0.1
0.3
0.1
1.3
0.5
0.2
0.2
0.7
0.01
1
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
Lab lb:
Rep.
Limit
6.4
13
0.3
0.5
0.5
1.3
0.5
6.4
2.6
0.8
1
2
0.04
3.5
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
1.553-1 Collect Date:
Oil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471A
SW-846, 7740
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-&46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/16/9615:07
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
KEN
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/03/96 13:00
10/08/96 15:29
10/08/96 15.29
10/08/96 15:29
10/08/96 15:29
10/08/96 15:29
10/08/96 15:29
10/08/96 15:29
10/08/96 15:29
10/08/96 15:29
10/08/96 15:29
10/08/96 15:29
10/18/96 14:32
09/19/96 10:45
10/23/96 11:53
09/24/96 19:39
09/24/96 19:39
09/24/9619:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/9619:39
09/24/9619:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/9619:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
Page 5 of 21
•
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
984)6-6
127-18-4
108-88-3
156-60-5
100614)2-6
79-01-6
75-69-4
75-01-4
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #662, GDI SFT. DUP.
CAS
Number
630-20-6
71-55-6
79-34-5
794)0-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78*
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
Test Parameter
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1.2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
U
U
U
U
U
U
U
U
U
U
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
M-1 SA DRYWELL
Result
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Units
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
1.2 JB ugAg
U
U
U
ugAg
ugAg
ugAg
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit.
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MUIR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
L55;5-2 Collect Date:
Oil.
Factor Method
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW*46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/24/96 19:39
09/16/9615:07
Analvst Test Date
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MUIR
MMR
MMR
MMR
MMR
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
Page 6 of 21
•
95-47-6
135-98-8
100-42-5
98*6-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
10: #662, GDI 10FT.
Test Parameter
ICP/GFAA METALS DIGESTION
ALUMINUM
ANTIMONY
BARIUM
BERYLLIUM
CAOMIUM
CHROMIUM
COPPER
LEAD
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
SELENIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENT ANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
U
U
U
U
U
U
U
U
U
U
U
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
M-1 SA DRYWELL
Result
18900
U
134
0.9
0.4
22
9.8
U
15
U
50
59
0.02
1.5
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Units
ug/g
ug'g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
1.4
2.8
0.06
0.1
0.1
0.3
0.1
1.4
0.6
0.2
0.2
0.8
0.01
1.1
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
7
14
0.3
0.6
0.6
1.4
0.6
7
2.8
0.8
1.1
2.2
0.04
3.8
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MUIR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
LSS3-3 Collect Date:
Dit.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-S46, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471A
SW-846, 7740
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-*46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/24/96 20:14
09/16/9615:15
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
KEN
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/03/96 13:00
10/08/9615:32
10/08/96 15.32
10/08/96 15:32
10/08/96 15:32
10/08/96 15:32
10/08/96 15:32
10/08/96 15:32
10/08/96 15:32
10/08/96 15:32
10/08/96 15:32
10/08/96 15:32
10/18/96 14:40
09/19/96 10:49
10/23/96 12:00
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20.49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20.49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
Page 7 of 21
100614)1-5
124-48-1
74-95-3
76-71-8
100-41-4
87-68-3
98-82-8
108-38-3
764)9-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98*
100-42-5
984)6-6
127-18-4
108-88-3
156-60-5
100614)2-6
794)1*
75-69-4
754)1-4
1 Sample 1
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58*
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
ltlRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
0:#616, GD910FT.
Test Parameter
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
.1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
U
U
U
U
U
U
U
U
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
1.4 JB ug/kg
U
U
U
U
U
U
1.1 J
16
U
U
U
26
U
U
M-137B
Result
0.3
14
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Umjt
0.1
0.3
1.4
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
1.4
6.8
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
L55:}-4 Collect Date: i
Dil.
Factor Method
SW-846, 3050
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20:49
09/24/96 20.49
09/24/96 20:49
09/24/96 20:49
09/16/96 09:32]
Analyst Test Date
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
-PUIMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
10/03/96 13:00
10/08/96 15:46
10/08/96 15:46
10/08/96 15:46
09/19/96 10:53
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21.23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
Pages of 21
74-87-3
156-59-4
100614)1-5
124-48-1
74-95-3
75-71-8
100-41-4
87*8-3
98-82-8
108-38-3
754)9-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
754)1-4
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
D:#616, GD915FT.
Test Parameter
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
M-137B
Result
0.4
12
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
Units.
ug/g
ug/g
ug/g
ug/g
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.1
0.3
1.3
0.02
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Umjt
0.5
1.3
6.6
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
L553-5 Collect Date:
Oil.
Factor Method.
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
.SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analys
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
09/24/96 21:23
39/16/96 09:42
. Test Date.
10/03/96 13:00
10/08/96 15:49
10/08/96 15:49
10/08/96 15:49
09/19/96 10:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
Page 9 of 21
754X)-3
67-66-3
74-87-3
156-59-4
100614)1-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
754)9-2
104-51-8
103-6S-1
91-20-3
95-47-6
135-98-8
100-42-5
984)6-6
127-18-4
108-88-3
156-60-5
100614)2-6
794)1-6
75-69-4
75-01-4
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMfc 1 HANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #616, GDI 6 10FT.
630-20-6
71-55-6
79-34-5
794)0-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78*7-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108*6-1
74-97-5
75-27-4
75-25-2
74-83-9
Test Parameter
ICP/(3FAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DlCHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DlBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
U
U
U
U
U
U
U
U
U
U
U
U
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug'kg
ug/kg
ug/kg
ug/kg
1.1 JB ug/kg
U
U
U
U
U
U
U
1.2 J
U
U
U
U
U
U
M-137B
Result
0.3
21
U
U
U
U
U
U
U
U
U
u
u
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.1
0.3
1.4
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.6
1.4
7.1
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
•1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
•I SW-846,8260
1 SW-846,8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
L5£i3-6 Collect Date:
Oil.
Factor Method
SW-846, 3050
1 SW-846,6010
1 SW-846,6010
1 SW-846,6010
1 SW-846,7471A
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
09/24/96 21:58
09/24/96 21.58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21.58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21-.58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24)96 21.58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/24/96 21:58
09/16/96 10:13
Analyst Test Date
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MV1R
MUIR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
10/03/96 13:00
10/08/96 15:51
10/08/9615:51
10/08/96 15:51
09/19/96 11:06
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
Page 10 Of 21
m
•
•
56-23-5
108-90-7
754X)-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75439-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
984)6-6
127-18-4
108-88-3
156-60-5
100614)2*
794)1-6
75-69-4
75-01-4
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #616, GDI 6 1 SFT.
630-20-6
71-55-6
79-34-5
794)0-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78*
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
Test Parameter
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1.1.2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
M-137B
Result
0.3
13
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.07
0.2
0.8
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.3
0.8
4.2
0.03
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MUIR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
LSS3-7 Collect Date:
Oil..
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
09/24/96 22:33
39/16/96 10:27
Analyst Test Date
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
-MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
10/03/9613:00
10/08/96 15:54
10/08/96 15:54
10/08/9615:54
09/19/96 11:10
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23.08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
Pagell of21
m
75-25-2
74-83-9
56-23-5
108-90-7
754X)-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47*
135-98-8
100-42-5
984)6-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
754)1-4
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DiBROMOCHLOROMfc 1 HANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
0: #616, GDI 41 OFT.
Test Parameter
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
1.3 JB ug/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
M-137B
Result
0.6
21
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
U
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.1
0.3
1.6
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.6
1.6
8
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MV1R
MMR
L55:5-8 Collect Date:
Oil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MUIR
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
09/24/96 23:08
39/16/96 10:56
. Test Date
10/10/96 09:30
10/10/96 11:43
10/10/96 11:43
10/10/96 11:43
09/19/9611:19
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/2TO6 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
Page 12 Of 21
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
100614)1-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82*
108-38-3
754)9-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
75-01-4
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87*1-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87*
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78*
10&43-4
99-87-6
108-10-1
67-64-1
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
0:#616, GD141SFT.
Test Parameter
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLpROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
24;HLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
U
U
u
u
u
u
u
1J
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
1.4 JBugAg
U
U
U
U
U
U
U
U
U
U
U
u
u
u
M-137B
Result
0.7
16
3.9
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/lcg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.1
0.3
1.5
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.6
1.5
7.7
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-&46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
L.55:3-9 Collect Date:
Oil.
Facior Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
09/24/96 23:43
39/16/96 11:04
Analyst Test Date
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/10/96 09:30
10/10/96 11:46
10/10/96 11:46
10/10/9611:46
09/19/96 11:23
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/9612:18
09/25/96 12:18
Page 13 of 21
•
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
754X)-3
67-66-3
74-87-3
156-59-4
100614)1-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
9S47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
100614)2-6
79-01-6
75-69-4
754)1-4
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
ClS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #616, GD21 OFT.
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
Test Parameter
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
24:HLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
M-137B
Result
0.3
3.7
U
0.01
u
68
U
U
1.4 J
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/lcg
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.1
0.3
1.3
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.5
1.3
6.7
0.03
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/9612:18
09/25/96 12:18
09/25/96 12:18
09/25/9612:18
09/25/96 12:18
09/25/96 12:18
09/25/9612:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/9612:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/9612:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
09/25/96 12:18
L55;)-10 Collect Date: 09/16/96 11 ;40
Dil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Test Date
10/10/96 09:30
10/10/96 11:48
10/10/96 11:48
10/10/96 11:48
09/19/96 11:31
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/9611:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/9611:39
09/25/96 11:39
Page 14 of 21
•
•
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74*3-9
56-23-5
108-90-7
754)0-3
67*6-3
74-87-3
156-59-4
100614)1-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104*1-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
984)6-6
127-18-4
108-88-3
156-60-5
10061-02-6
794)1-6
75-69-4
75-01-4
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #616, GD2 10FT. DUP.
Test Parameter
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM .
LEAD
MERCURY
1 Sample ID: #616, GD2 1 SFT.
630-20-6
71-55-6
79-34-5
794)0-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
Test Parameter
ICP/GFAA METALS DIGESTION
CADMIUM
CHROMIUM
LEAD
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
U
U
U
U
U
U
U
U
U
U
U
2 J
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
2 JB ugAg
U
U
U
U
U
U
U
140
U
U
U
23
U
u
M-137B
Result
0.4
6.8
U
U
M-1378
Result
0.6
9.4
3.8
0.02
U
210
U
U
3.3 J
U
U
U
U
U
U
U
U
U
u
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
Units
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/lcg
ugAg
ugAg
ug/kg
ugAg
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.1
0.3
1.5
0.01
Det.
Limit
0.1
0.3
1.6
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.6
1.5
7.6
0.04
Lab ID:
Rep.
Limit
0.6
1.6
7.8
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
1
1
1
1
1
1
1
-|
1
1
•1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MUIR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/9611:39
09/25/96 11:39
09/25/96 11:39
09/25/9611:39
09/25/9611:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/9611:39
09/25/9611:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/9611:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/9611:39
09/25/9611:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/96 11:39
09/25/9611:39
09/25/96 11.39
09/25/96 11:39
09/25/96 11:39
09/25/9611:39
09/25/96 11:39
LS5:}-11 Collect Date: 09/16/96 11 ;40
Dil.
Factor Method
1
1
1
1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
Analyst
KWB
KWB
KWB
KWB
KEN
Test Date
10/10/96 09:30
10/10/96 11:51
10/10/96 11:51
10/10/96 11:51
09/19/96 11:36
L553-12 Collect Date: 09/16/9611:52
Dil.
Facior Method
1
1
1
1
1,
1
1
1
1
1
1
1
1
1
1
1
1
1
1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
KWB
KWB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
TesTDate
10/10/96 09:30
10/10/96 11:54
10/10/96 11:54
10/10/96 11:54
09/19/96 11:40
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
Page 15 of 21
0
•
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67*4-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
66-23-5
108-90-7
75-00-3
67*6-3
74*7-3
156-59-4
100614)1-5
124-48-1
74-95-3
75-71-8
10041-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
100614)2-6
79-01-6
75-69-4
75-01-4
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
44:HLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #260, SFT.
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
Test Parameter
PH
ICP/GFAA METALS DIGESTION
CADMIUM
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE ,
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
5.5 J
U
U
U
U
U
u
u
u
u
u
u
u
u
u
3.6 J
U
U
U
140
3.1 J
U
U
39
U
U
M-53-BP
Result
7.65
0.7
0.07
U
1.3 J
U
U
U
U
U
U
U
U
U
U
U
U
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/lcg
ugAg
Units
ug/g
ug/g
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.1
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.6
0.03
10
10
10
10
10
10
10
10
10
10
10
10
10
10
1 SW-846,8260
1 SW-846,8260
I SW-846,8260
I SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
•1 SW-846,8260
11 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846, 8260
1 SW-846,8260
1 SW-846,8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/9612:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/9612:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/9612:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/9612:14
09/25/9612:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/9612:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
09/25/96 12:14
L5S3-13 Collect Date: 09/16/96 13:45
Dil.
Factor Method
1 SW 846, 9045
SW-846, 3050
1 SW-846,6010
1 SW-846,7471A
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
Analyst
MTB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Test Date
10/08/96 13:00
10/10/96 09:30
10/10/96 11:57
09/19/96 11:44
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/9612:49
Page 16 of 21
1074)6-2 1,2-DICHLOROETHANE
78-87-5 1,2-DICHLOROPROPANE
108*7-8 1,3,5-TRIMETHYLBENZENE
541-73-1 1,3-DICHLOROBENZENE
142-28-9 1,3-DICHLOROPROPANE
106-46-7 1,4-DICHLOROBENZENE
590-20-7 2,2-DICHLOROPROPANE
78-93-3 2-BUTANONE
95-49-8 2-CHLOROTOLUENE
591-78-6 2-HEXANONE
106-43-4 4-CHLOROTOLUENE
99-87-6 4-ISOPROPYLTOLUENE
108-10-1 4-METHYL-2-PENTANONE
67-64-1 ACETONE
71-43-2 BENZENE
108-86-1 BROMOBENZENE
74-97-5 BROMOCHLOROMETHANE
75-27-4 BROMODICHLOROMETHANE
75-25-2 BROMOFORM
74-83-9 BROMOMETHANE
56-23-5 CARBON TETRACHLORIDE
108-90-7 CHLOROBENZENE
754)0-3 CHLOROETHANE
67-66-3 CHLOROFORM
74-87-3 CHLOROMETHANE
156-59-4 ClS-1,2-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1 DIBROMOCHLOROMETHANE
74-95-3 DIBROMOMETHANE
75-71-8 DICHLORODIFLUOROMETHANE
100-41-4 ETHYLBENZENE
87-68-3 HEXACHLOROBUTADIENE
98-82-8 ISOPROPYLBENZENE
108-38-3 M,P-XYLENE
75-09-2 METHYLENE CHLORIDE
104-51-8 N-BUTYLBENZENE
103-65-1 N-PROPYLBENZENE
91-20-3 NAPHTHALENE
95-47-6 O-XYLENE
135-98-8 SEC-BUTYLBENZENE
100-42-5 STYRENE
984)6* TERT-BUTYLBENZENE
127-18-4 TETRACHLOROETHENE
108-88-3 TOLUENE
156-60-5 TRANS-1,2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
79-01-6 TRICHLOROETHENE
75-69-4 TRICHLOROFLUOROMETHANE
754)1-4 VINYL CHLORIDE
120-82-1 1,2,4-TRICHLOROBENZENE
95-50-1 1,2-DICHLOROBENZENE
541-73-1 1,3-DICHLOROBENZENE
106-46-7 1,4-DICHLOROBENZENE
95-95-4 2,4,5-TRICHLOROPHENOL
88-06-2 2,4,6-TRICHLOROPHENOL
120-83-2 2,4-DICHLOROPHENOL
105-67-9 2,4-DIMETHYLPHENOL
51-28-6 2,4-DINITROPHENOL
121-14-2 2,4-DINITROTOLUENE
606-20-2 2,6-DINITROTOLUENE
91-58-7 2-CHLORONAPHTHALENE
95-57-8 2-CHLOROPHENOL
91-57-6 2-METHYLNAPHTHALENE
95-48-7 2-METHYLPHENOL
88-74-4 2-NITROANILINE
88-75-5 2-NITROPHENOL
56-55-3 3,3'-DICHLOROBENZIDINE
994)9-2 3-NlTROANILINE
534-52-1 4,6-DINITRO-24UlETHYLPHENOL
101-55-3 4-BROMOPHENYL-PHENYLETHER
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
1.4 J
u
u
u
u
u
u
u
u
u
u
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
2.3 JB ugAg
U
U
U
U
U
U
U
1.9 J
U
U
U
1.9 J
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/lcg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
63
63
63
147
133
90
90
90
1400
190
63
63
110
73
77
50
120
333
80
800
63
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
333
333
333
333
333
333
333
333
1670
333
333
333
333
333
333
1670
333
667
1670
1670
333
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SWr846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/25/96 12:49
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/9612:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/9612:29
Page 17 of 21
•
59-50-7
106-47-8
7005-72-3
106-44-5
1004314)6
1004)2-7
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
2074)8-9
111-91-1
111^44-4
108-60-1
117-81-7
85-68-7
120-12-7
2184)1-9
84-74-2
117-844)
53-70-3
132-64-9
84-66-2
131-11-3
206-44*
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
193-39-5
78-59-1
621-64-7
86-30-6
91-20-3
98-95-3
87-86-5
854)1-8
108-95-2
1294X)4)
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87*1-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107436-2
78-87-5
108-67-8
541-73-1
142-28-9
4-CHLORO-3-Mfc 1 HYLPHENOL
4-CHLOROANILINE
4-CHLOROPHENYL-PHENYLETHER
4-METHYLPHENOL
4-NITROANlLINE
4-NITROPHENOL
ACENAPHTHENE
ACENAPHTHYLENE
ANTHRACENE
BENZO(A)ANTHRACENE
BENZO(A)PYRENE
BENZO(B)FLUORANTHENE
BENZO(G,H,l)PERYLENE
BENZO(K)FLUORANTHENE
BIS(24:HL0R0ETH0XY)METHANE
BIS(2-CHLOROETHYL)ETHER
BIS(24:HL0R01S0PR0PYL)ETHER
BIS(2-ETHYLHEXYL)PHTHALATE
BUTYLBENZYLPHTHALATE
CARBAZOLE
CHRYSENE
DI-N-BUTYLPHTHALATE
DI-N-OCTYLPHTHALATE
D1BENZ(A,H)ANTHRACENE
DIBENZOFURAN
DIETHYLPHTHALATE
DIMETHYLPHTHALATE
FLUORANTHENE
FLUORENE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROCYCLOPENTADIENE
HEXACHLOROETHANE
INDENO(1,2,3-CD)PYRENE
ISOPHORONE
N-NITROSO-Dl-N-PROPYLAMINE
N-NITROSODIPHENYLAMINE
NAPHTHALENE
NITROBENZENE
PENTACHLOROPHENOL
PHENANTHRENE
PHENOL
PYRENE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ID: #260, 10FT. M-53-BP
Test Parameter
PH
ICP/GFAA METALS DIGESTION
CADMIUM
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
Result
7.57
0.4
0.3
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
Units
ug/g
ug/g
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
100
60
140
133
120
80
63
117
63
260
83
167
137
160
177
190
190
83
83
333
83
83
83
83
100
63
53
73
63
63
30
200
53
123
73
400
63
53
47
120
180
50
63
Det.
Limit
0.1
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
667
667
333
333
1670
1670
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
1670
333
333
333
Lab 10:
Rep.
Limit
0.6
0.02
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
L55;M4 Collect Date:
Dil.
Facitor Method
SW 846, 9045
SW-846, 3050
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/9612:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/9612:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/96 12:29
09/26/9612:29
09/26/96 12:29
09/26/96 12:29
09/16/9613:57
Analyst Test Date
MTB
KWB
KWB
KEN
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/08/9613:00
10/10/96 09:30
10/10/96 12:15
09/19/96 11:48
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/9613:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/9613:24
09/25/96 13:24
09/25/96 13:24
Page 18 Of 21
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74*3-9
56-23-5
108-90-7
754)0-3
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
984)6*
127-18-4
108-88-3
156-60-5
100614)2-6
794)1-6
75-6»-1
754)1-4
120-82-1
95-50-1
541-73-1
106-46-7
95-95-4
884)6-2
120-83-2
105-67-9
51-28-5
121-14-2
606-20-2
91-58-7
95-57-8
91-57-6
95-48-7
88-74-4
88-75-5
56-55-3
994)9-2
534-52-1
101-55-3
59-50-7
106-47-8
7005-72-3
106-44-5
100-01-06
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M.P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1,2,4-TRICHLOROBENZENE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DICHLOROPHENOL
2,4-DIMETHYLPHENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
2-METHYLNAPHTHALENE
2-METHYLPHENOL
2-NITROANILINE
2-NlTROPHENOL
3,3'-DlCHLOROBENZlDlNE
3-NITROANILINE
4,6-DINITRO-2-METHYLPHENOL
4-BROMOPHENYL-PHENYLETHER
4-CHLORO-3-METHYLPHENOL
4-CHLOROANILINE
4-CHLOROPHENYL-PHENYLETHER
4-METHYLPHENOL
4-NITROANILINE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
3.9 JB ug/kg
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
63
63
63
147
133
90
90
90
1400
190
63
63
110
73
77
50
120
333
80
800
63
100
60
140
133
120
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
333
333
333
333
333
333
333
333
1670
333
333
333
333
333
333
1670
333
667
1670
1670
333
667
667
333
333
1670
11 SW-846,8260
11 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8270
1 SW-846, 8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MUIR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/9613:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/9613:24
09/25/96 13.24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/25/96 13:24
09/26/9613:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/9613:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/9613:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
Page 19 of 21
100-02-7
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
2074)6-9
111-91-1
111-44-4
108*0-1
117-81-7
85-68-7
120-12-7
218-01-9
84-74-2
117-84-0
53-70-3
132-64-9
84-66-2
131-11-3
206-444)
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
193-39-5
78-59-1
621-64-7
86-30-6
91-20-3
98-95-3
87-86-5
85-01-8
108-95-2
129-00-0
4-NITROPHENOL
ACENAPHTHENE
ACENAPHTHYLENE
ANTHRACENE
BENZO(A)ANTHRACENE
BENZO(A)PYRENE
BENZO(B)FLUORANTHENE
BENZO(G,H,l)PERYLENE
BENZO(K)FLUORANTHENE
BIS(2-CHLOROETHOXY)METHANE
BIS(2-CHLOROETHYL)ETHER
BIS(2-CHLOROISOPROPYL)ETHER
BIS(2-ETHYLHEXYL)PHTHALATE
BUTYLBENZYLPHTHALATE
CARBAZOLE
CHRYSENE
DI-N-BUTYLPHTHALATE
Dl-N-OCTYLPHTHALATE
DIBENZ(A,H)ANTHRACENE
DIBENZOFURAN
DIETHYLPHTHALATE
DIMETHYLPHTHALATE
FLUORANTHENE
FLUORENE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROCYCLOPENTADIENE
HEXACHLOROETHANE
INDENO(1,2,3-CD)PYRENE
ISOPHORONE
N-NITROSO-DI-N-PROPYLAMINE
N-NITROSODIPHENYLAMINE
NAPHTHALENE
NITROBENZENE
PENTACHLOROPHENOL
PHENANTHRENE
PHENOL
PYRENE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug'kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
80
63
117
63
260
83
167
137
160
177
190
190
83
83
333
83
83
83
83
100
63
53
73
63
63
30
200
53
123
73
400
63
53
47
120
180
50
63
1670
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
1670
333 1
333
333
SW-846, 8270
\ SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
SW-846, 8270
SW-846, 8270
\ SW*46,6270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-S46, 8270
SW-846, 8270
t SW-846,8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
1 SW-846,8270
1 SW-846,8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
1 SW-846,8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
09/26/96 13:14
09^26/96 13-.14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13.14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/9613:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/9613:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/9613:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
09/26/96 13:14
Page 20 of 21
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected
but was below the detection limit.
B This flag is used when an analyte is found in the blank as well as the sample
Det. Limit Method Detection Limit (approximately three times the signal noise level)
Rep. Limit Reporting Limit is normally the value ofthe lowest standard run with the
analysis. The value is approximately 5 to 10 times the Method Detection Limit.
Dil. Factor Dilution Factor - The prepared sample was diluted by this factor because the
sample was too concentrated or due to other interferences in the sample matrix.
Any dilution factor causes an appropriate increase in the method detection limit
and reporting limit.
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This
flag is used either when estimating a concentration for tentatively identified compounds or
when the data indicated the presence of a compound that meets the identification criteria
but the result is less than the specified reporting limit (e.g. 3 J with a reporting limit of 10)
Page 21 of 21
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing F(equested
Friday, November 01,1996
TESTED FOR Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp,UT 84322
Frank Walker
Project: Solid Waste Mgmt Invest.
Login Number L569
Lab Number Client Number
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
301-863-5445
300-863-8080
Test Requested Description
L569-1 #200, GD001 SFT. T-35
SW-846, 3050 ICP/GFAA Melals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Melals Analysis (RCRA)
SW-846,6010 Cd ICP Melals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Melals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
LS69-2 #200, GD001 10FT. T-35
SW-846, 3050 ICP/GFAA Melals Digestion
SW-846,6010 Ag ICP Melals Analysis (RCRA)
SW-846,6010 Be ICP Melals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Melals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
L569-3 #200, GD002 SFT. T-35
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Melals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Melals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
Received
Matrix
Collect Date/Time
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96 09:24
09/19/96 09:32
09/19/96 10:00
Page 1 of 15
LS69-4 #200, GD00210FT. T-35 09/19/96 09/19/96 10:15
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Melals Analysis (RCRA)
SW-846,6010 Be ICP Melals Analysis (RCRA)
SW-846,6010 Cd ICP Melals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L569-5 #200, GD003 SFT. T-35 09/19/96 09/19/96 10:42
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Melals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
LS69-6 #200, GD00310FT. T-3S 09/19/96 09/19/96 10:57
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Melals Analysis (RCRA)
SW-846,6010 Be ICP Melals Analysis (RCRA)
SW-846, 6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Melals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L569-7 #200, GD004 SFT. T-35 09/19/96 09/19/9611:27
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846,6010 Ag ICP Melals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846,6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CVMercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
L569-8 #200, GD00410FT. T-3S 09/19/96 09/19/96 11:37
SW-846, 3050 ICP/GFAA Melals Digestion
SW-846, 6010 Ag, ICP Metals Analysis (RCRA)
SW-846,6010 Be ICP Metals Analysis (RCRA)
SW-846, 6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr ICP Melals Analysis (RCRA)
SW-846,6010 Pb ICP Metals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Page 2 of 15
•
LS69-9 #200, GDOOS SFT. T-3S 09/19/96 09/19/9611:58
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
1CP/GF/\A Melals Digestion
Ag ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Cd ICP Melals Analysis (RCRA)
Cr ICP Melals Analysis (RCRA)
Pb ICP Melals Analysis (RCRA)
CV Mercury Analysis (RCRA)
Volatile Organics
L569-10 #200, GDOOS 10FT. T-35
SW-846, 3050 ICP/GFAA Melals Digestion
SW-846,6010 Ag ICP Melals Analysis (RCRA)
SW-846,6010 Be ICP Melals Analysis (RCRA)
SW-846, 6010 Cd ICP Metals Analysis (RCRA)
SW-846,6010 Cr IGP Melals Analysis (RCRA)
SW-846,6010 Pb ICP Melals Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 8260 Volatile Organics
L569-11 #200, GDOOS lOFT.DUP T-3S
SW-846, 3050
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7471A
ICP/GFAA Melals Digestion
Ag ICP Metals Analysis (RCRA)
Be ICP Metals Analysis (RCRA)
Cd ICP Melals Analysis (RCRA)
Cr ICP Melals Analysis (RCRA)
Pb ICP Metals.Analysis (RCRA)
CV Mercury Analysis (RCRA)
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96
Soil
Soil
Soil
Soil
Soil
Soil
Soil
09/19/96 12:10
09/19/9612:10
Work Order Comments
There is a slight matrix interference for beryllium, chromium, and lead as exhibited by the
matrix spike results.
Ckvg^?// t-yt/i^
Date /y Certified By
This is to certify that the following samples were analyzed using good laboratory practices to show
the folowing results:
Page 3 of 15
Listing of Results by Sample
1 Sample
630-20-6
71-55-6
79-34-5
794X)-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78*
106-43-4
99*7-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
100614)1-5
124-48-1
74-95-3
75-71-8
100-41-4
87*8-3
98-82-8
108-38-3
754)9-2
104-51*
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
984)6-6
127-18-4
ID: #200, GD001 SFT. T-3S
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
Result
775
6.5
23
U
0.3
0.02
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
24 B
u
u
u
u
u
u
u
u
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
Oet.
Umjt
0.1
0.1
0.3
1.6
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
Lab ID:
Rep.
Limit
0.7
0.7
1*
8.2
0.98
0.03
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
LS69-1 Collect Date:
Oil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/19/96 09:24
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MMR
MMR
MMR
MUIR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
lUIMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/14/96 00:00
10/15/96 14:33
10/15/9614:33
10/15/9614:33
10/15/96 14:33
10/15/96 14:33
10/17/96 12:25
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/9616:14
09/26/96 16:14
09/26/96 16:14
09/26/9616:14
09/26/96 16:14
09/26/96 16:14
09/26/9616:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/9616:14
09/26/9616:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
Page 4 Of 15
•
•
108-88-3
156*0-5
100614)2-6
79-01-6
75-69-4
75-01-4
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #200, GD001 10FT. T-3S
630-20-6
71-55-6
79-34-5
794X)-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95^9-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-4
10061-01*
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75439-2
104-51-8
103-65-1
91-20-3
95-47-6
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DlBROMO-3-CHLOROPROPAN
1,2-DIBROMOETI-IANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
44UIETHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
U
U
U
U
U
U
Result
207
2.1
19
U
U
0.02
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
13 B
u
u
u
u
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/lcg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
0.3
0.2
0.2
0.3
0.3
0.4
Det.
Limit
0.1
0.1
0.3
1.5
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
10
10
10
10
10
10
Lab 10:
Rep.
Limit
0.6
0.6
1.5
7.6
0.9
0.03
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
L56:9-2 Collect Date:
Diii.
Facior Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/26/96 16:14
09/19/96 09:32
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MUIR
MUIR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/14/96 00:00
10/15/96 14:56
10/15/96 14:56
10/15/96 14:56
10/15/96 14:56
10/15/96 14:56
10/17/96 12:29
09/26/96 16:49
09/26/9616:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/9616:49
09/26/96 16:49
09/26/96 16:49
09/26/9616:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/9616:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26796 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/9616:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
Page 5 of 15
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
100614)2-6
79-01-6
75-69-4
75-01-4
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMb 1 HANE
VINYL CHLORIDE
1 Sample ID; #200, GD002 SFT. T-35
630-20*
71-55-6
79-34-5
794)0-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78*
106-43-4
99*7-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74*3-9
56-23-5
108-90-7
754)0-3
67-66-3
74-87-3
156-59-4
100614)1-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
754)9-2
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1 -TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
U
U
U
U
U
U
U
U
U
U
Result
0.7
0.4
15
U
U
0.02
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
16 B
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.1
0.1
0.3
1.6
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0*
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
10
10
ib
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.6
0.6
1.6
7.8
0.9
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MUIR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
L569-3 Collect Date:
Dill.
Facior Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/26/96 16:49
09/19/96 10:00
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
10/14/96 00:00
10/15/9614:58
10/15/9614:58
10/15/96 14:58
10/15/96 14:58
10/15/96 14:58
10/17/9612:33
09/26/9617:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/9617:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/9617:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/9617:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/9617.24
09/26/9617:24
09/26/9617:24
09/26/9617:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/9617:24
Page 6 of 15
•
104-51*
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
984)6-6
127-18-4
108-88-3
156-60-5
100614)2-6
79*1-6
75-69-4
754)1-4
1 Sample
630-20-6
71-55-6
79-34-5
79430-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74*3-9
56-23-5
108-90-7
754X)-3
67-66-3
74-87-3
156-59-4
100614)1-5
124-48-1
74-95-3
75-71-8
100-41-4
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
I0:#200, GD00210FT. T-35
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4OHL0R0T0LUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Result
0.3
0.2
15
U
U
0.02
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.1
0.1
0.3
1.6
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
10
10
10
ib
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.6
0.6
1.6
8
0.96
0.03
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MUIR
MUIR
MMR
MMR
MMR
MMR
MUIR
L569-4 Collect Date:
Dil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/26/9617:24
09/26/96 17:24
09/26/96 17:24
09/26/9617:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/96 17:24
09/26/9617:24
09/26/96 17:24
09/26/9617:24
09/26/9617:24
09/26/96 17:24
09/19/96 10:15
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MUIR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
10/14/96 00:00
10/15/96 15:01
10/15/96 15:01
10/15/96 15:01
10/15/96 15:01
10/15/96 15:01
10/17/96 12:37
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/9617:58
09/26/96 17:58
09/26/9617.58
09/26/96 17:58
09/26/96 17:58
09/26/9617:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/9617:58
09/26/9617:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/9617:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/9617:58
09/26/9617:58
09/26/96 17:58
09/26/9617:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
Page 7 Of 15
87-68-3 .
98*2-8
108-38-3
754)9-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
984)6-6
127-18-4
108-88-3
156-60-5
100614)2-6
794)1-6
7S:-69-4
754)1^
1 Sample
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78*
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
754X)-3
67-66-3
74-87-3
156-59-4
100614)1-5
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
D: #200, GD003 SFT. T-3S
Test Parameter
ICP/GFAAMETALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
24;HLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
U
U
U
25 B
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Result
0.6
U
18
U
U
0.03
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/lcg
ug/lcg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.1
0.1
0.3
1.6
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.6
0.6
1.6
7.9
0.9
0.03
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
L569-5 Collect Date:
Dil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/26/9617:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/9617:58
09/26/96 17:58
09/26/9617:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/96 17:58
09/26/9617:58
09/26/96 17:58
09/26/96 17:58
09/26/9617:58
09/19/96 10:42
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MUIR
MMR
MMR
MUIR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MUIR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/14/96 00:00
10/15/96 15:04
10/15/96 15:04
10/15/96 15:04
10/15/96 15:04
10/15/96 15:04
10/17/9612:45
09/26/96 18:33
09/26/9618:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26796 18:33
09/26/96 18:33
09/26/96 18:33
09/26/9618:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/9618:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
Page 8 of 15
•
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
754)9-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98*
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
100614)2-6
794)1-6
75-69-4
75-01-4
1 Sample
630-20-6
71-55-6
79-34-5
794)0-5
75-34-3
75-35-4
563-58*
87-61-6
96-18-4
120-82-1
95-63-6
96-12*
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
754)0-3
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
IO:#200, GD003 10FT. T-3S
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1 -DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
24:HLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
U
U
U
U
U
U
U
12 B
U
U
U
U
U
U
U
U
U
U
U
u
u
u
Result
0.4
0.6
15
U
U
0.02
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.1
0.1
0.3
1.5
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.6
0.6
1.5
7.7
0.9
0.04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
hIMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MAR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
LS69-6 Collect Date:
Oil.
Facitor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846,6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/26/96 18:33
09/19/9610:57
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MUIR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MUIR
MMR
MUIR
MMR
MMR
MMR
MUIR
MUIR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MUIR
10/14/96 00:00
10/15/96 15:18
10/15/96 15:18
10/15/96 15:18
10/15/9615:18
10/15/96 15:18
10/17/96 12:49
09/26/96 19:08
09/26/96 19:08
09/26/9619:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19.08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/9619:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
Page 9 of 15
67-66-3
74*7-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95^7*
135-98*
100-42*
984)6-6
127-18-4
108-88-3
156-60-5
100614)2-6
794)1-6
75-69-4
754)1-4
1 Sample
630-20-6
71-55-6
79-34-5
794)0-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
1074)6-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
D1BRC3MOCHLOROM ETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
0: #200, GD004 SFT. T-3S
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1 ,2-DIBROMO-34:HLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
24:HLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
U
U
U
U
U
U
U
U
U
U
U
15 B
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Result
0.5
0.2
18
U
U
0.02
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/lcg
ug/lcg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
0.1
0.1
0.3
1.5
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab 10:
Rep.
Limit
0.6
0.6
1.5
7.6
0.9
0.03
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MUIR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
L569-7 Collect Date:
Dil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/9619:08
09/26/96 19:08
09/25/96 19.08
09/26/96 19:08
09/26/96 19:08
09/26/9619:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19.08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
09/26/96 19:08
39/19/9611:27
Analyst Test Date
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
10/14/96 00:00
10/15/96 15:21
10/15/96 15.21
10/15/96 15:21
10/15/96 15:21
10/15/96 15:21
10/17/96 12:56
09/26/9619:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/9619:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/9619:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19.43
09/26/96 19:43
09/26/96 19:43
09/26/9619:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/9619:43
09/26/96 19:43
09/26/96 19:43
Page 10 of 15
74*3-9
56-23-5
108-90-7
75-00-3
67-66-3
74*7-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82*
108-38-3
75-09-2
104-51-8
103-65-1
91-20-3
95-47-6
135-98-8
100-42-5
984)6-6
127-18-4
108-88-3
156-605
100614)2-6
79-01-6
75-69-4
75-01-4
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
ClS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE .
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #200, GD004 10FT. T-3S
63O20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-501
1074)6-2
78-87-5
108*7-8
541-73-1
142-28-9
106-46-7
590-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-101
67-64-1
71-43-2
Test Parameter
ICP/GFAAMETALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-1 b 1 RACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1 ,2-D1BR0M0-34:HL0R0PR0PAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-lSOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
37 B
U
U
U
U
U
U
u
u
u
u
u
u
u
u
Result
0.2
0.4
13
U
U
0
U
U
U
U
U
U
U
U
u
u
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/lcg
ugAg
ugAg
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
Ol
Ol
0.3
1.6
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
Ol
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 1
10 1
10 1
10 1
10 1
Lab ID: L56
Rep. 0
Limit Fac
0.6 1
0.6 1
1.6 1
8.1 1
0.97 1
0.04 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MUIR
MUIR
MMR
MMR
MMR
MUIR
MUIR
MUIR
MMR
MUIR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
9-8 Collect Date:
1.
lor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analysi
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MUIR
MUIR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MUIR
MUIR
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
09/26/96 19:43
39/19/96 11:37
t Test Date
10/14/96 00:00
10/15/96 15:23
10/15/96 15:23
10/15/96 15:23
10/15/96 15:23
10/15/9615:23
10/17/96 13:00
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
Page 11 of 15
108-86-1
74-97-5
75-27-4
75-25-2
74*3-9
56-23-5
108-90-7
75-00-3
67-66-3
74*7-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
754)9-2
104-51-8
103-65-1
91-203
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-605
10061-02-6
79-01-6
75-69-4
754)1-4
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
Mb IHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #200, GDOOS SFT. T-3S
630-20-6
71-55-6
79-34-5
79-005
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-501
107-06-2
78-87-5
108*7-8
541-73-1
142-28-9
106-46-7
590-207
78-93-3
95-49-8
591-78-6
106-43-4
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLORdpROPANE
1,2,4-TRICHLOROBENZENE-
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
15 B
U
U
U
U
U
U
U
U
U
u
u
u
u
u
Result
0.4
0.3
17
U
U
0.03
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/lcg
ugAg
ug/lcg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
0.2
0.2
0.3
Ol
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
Ol
Ol
0.3
1.6
0.2
0.01
0.2
0.2
0.3
0.2
Ol
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.6
0.6
1.6
7.9
0.9
0.03
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
SW-846, 8260
SW.-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
. SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MUIR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
09/26/96 20:18
L569-9 Collect Date: 09/19/96 11:58
Oil.
Factor Method
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MUIR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
. Test Date
10/14/96 00:00
10/15/96 15:26
10/15/96 15:26
10/15/96 15:26
10/15/96 15:26
10/15/96 15:26
10/17/9613:08
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/9615:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/9615:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
Page 12 Of 15
m
99-87-6
108-101
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74*3-9
56-23-5
1Q8-907
754)03
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-203
95^7-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-605
100614)2-6
79*1-6
75-69-4
754)1-4
4-ISOPROPYLTOLUENE
44UIETHYL-2.PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROME rHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #200, GDOOS 10FT. T-35
630206
71-55-6
79-34-5
79-005
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590207
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DlBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
U
U
U
U
U
U
U
U
U
U
U
U
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
4.7 JB ug/kg
U
U
U
U
U
U
U
U
U
U
21 B
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Result
0.3
0.6
13
U
U
0.02
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
0.2
10
10
0.2
0.2
0.2
0.3
Ol
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
02
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Umit
Ol
Ol
0.3
1.6
0.2
0.01
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
Ol
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.6
0.6
1.6
7.9
0.9
O04
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW.S46. 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MUIR
MMR
MMR
MMR
MMR
MUIR
MMR
MUIR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
10/01/96 15:10
LS69-10 Collect Date: 09/19/96 12:10
Oil.
Facitor Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
Analyst
KWB
KWB
KWB
KWB
KWB
KWB
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
Test Date
10/14/96 00:00
10/15/96 15:29
10/15/96 15:29
10/15/96 15:29
10/15/96 15:29
10/15/9615:29
10/17/96 13:12
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/9616:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/9616:25
10/01/96 16.25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
Page 13 of 15
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-101
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74*3-9
56-23-5
108-907
75-003
67-66-3
74-87-3
156-59-4
100614)1-5
124-48-1
74-95-3
75-71*
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-203
95-17-6
135-98*
100-42-5
98-06-6
127-18-4
108-88-3
156*0-5
10061-02-6
79-01-6
75-69-4
754)1-4
2-BUTANONE
24:HLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1 Sample ID: #200, GDOOS 10FT.DUP T-35
Test Parameter
ICP/GFAA METALS DIGESTION
BERYLLIUM
CADMIUM
CHROMIUM
LEAD
SILVER
MERCURY
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
4.7 JB ugAg
U
U
U
U
U
U
U
U
U
U
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
5.7 JB ug/kg
U
U
U
U
U
U
U
U
1.1 J
U
U
U
U
U
Result
0.3
0.6
15
U
U
U
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
Ol
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
Oet.
Limit
Ol
0.1
0.3
1.7
0.2
0.01
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Lab ID:
Rep.
Limit
0.7
0.7
1.7
8.3
1
0.04
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MUIR
MUIR
MMR
MMR
MMR
MMR
MUIR
M^R
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MMR
10/01/96 16:25
10/01/96 16:25
10/01/9616:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16.25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/9616:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/9616:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/9616:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
10/01/96 16:25
L569-11 Collect Date: 09/19/96 12:10
Dil.
Factor Method
SW-846, 3050
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471A
Analyst
KWB
KWB
KWB
KWB
KWB
KWB
CRS
Test Date
10/14/96 00:00
10/15/96 15:32
10/15/96 15:32
10/15/96 15:32
10/15/96 15:32
10/15/96 15:32
10/17/96 13:16
Page 14 of 15
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected
but was below the deteciion limit.
B This flag is used when an analyte is found in the blank as well as the sample
Det. Limit Method Detection Limit (approximately three times the signal noise level)
Rep. Limit Reporting Limit is normally the value of the lowest standard run with the
analysis. The value is approximately 5 to 10 times the Method Detection Limit.
Dil. Factor Dilution Factor - The prepared sample was diluted by this factor because the
sample was too concentrated or due to other interferences in the sample matrix.
Any dilution factor causes an appropriate increase in the method detection limit
and reporting limit.
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This
flag is used either when estimating a concentration for tentatively identified compounds or
when the data indicated the presence of a compound that meets the identification criteria
but the result is less than the specified reporting limit (e.g. 3 J with a reporting limit of 10)
Page 15 of 15
ENVIRONMENTAL LAB WORK REQUEST ^ /
4^ °- THIOKOL EIWIRONMENTAL LABORATORY LWR No. ^f//2<l- 7
Login No. ^^ \S-7<f
^/w^^ Af UA^fey
Bnvtrdt]/hnh/
EXTENSION
5-390
COST CENTER WORKORDER
PORT RESULTS! TO: If ORCANIZATION MAILSTOP
3oie
REPORT RESULTS! TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE
3
DATE TYPE
ly
LOCATION TIME
'T^t i^r
TEST
>^- &ZOO
REMARKS
/ // /f ^ ff I4tir 'r/hj I'^bA -ezjo
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y '/ 1/
7 K i£^ S€t._^^
If ]' f( /470 *^i€:^iH-
CHAIN OF CUSTODY
RELINQUISHED BY
Z^IXl//MJU^
DATE.
^/^sA^
/ /
TIME
^>2r5-
RECETVED BY
-
DATE TIME
FOR LABORATORY USE ONLY
4 DATE COMPLETED DATE REPORTED SIGNATURE
L^7>/
ENVIRONMENTAL LAB WORK REQUEST 7-^ ^
#
™= THIOKOL ENVIRONMENTAL LABORATORY LWR No. ^//Zbl
Login No. ^SV^
1\ f [jj(\Lt^..'^ ^190
COST CENTER WORKORDER DATE '
?--2l'?^
ORGANIZATION MAILSTOP REPORT RESULTS TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
/
^SAMPLE
tAtiCarOutxJ 1,
' l\
' f«
• 'll
' ((
; " ,.
10
II.
12.
DATE
1^7^
t(
'(
f(
'rt n
l(
l<
1
TYPE
G
\y
y
c/
c/
1/
J
if
t/
c
t
•
f
LOCATION
7^^
TIME
/ff«
/f4^ m
IW) mo
(foQ
(90
(W
TEST
i/0/-Y ^9zCro
^A: l/oA -gz7o
REMARKS
IVIMC^ J f5^I\ Cl
3^«r *f-)
-Se:^ -^^Z:
^^^ 14--5
S... ti^
i«S.S,'C,fQT^CA_
CHAIN OF CUSTODY
RELINQUISHED BY DATE TIME RECEIVEDBY DATE TIME
4-
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED SIGNATURE
CERTIFICATE OF ANALYSIS
Listing of Sample Information and Testing Flequested
Tuesday, November OS, 1996
TESTED FOR Thiokol: DLV
Environmental Monitoring
M/S 301
Thiokol Corp,UT 84322
Frank Walker
Project: Solid Waste Mgmt Invest.
Login Number LS74
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-5445
800-863-8080
Lab Number Client Number
Test Requested Description
L574-1 BACKGROUND SURFACE TEST AREA
ASTM D2488-84
SOP 302
SOP 420
SOP 420
SW 846, 9012
SW 846, 9045
SW 846, 9056
SW-846, 3050
SW-846, 3550
SW-846,6010
SW-S46,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846,6010
SW-846, 7060
SW-846, 7471A
SW-846, 7481
SW-846, 7740
SW-846, 8260
SW-846, 8270
Ag
B
Be
Cd
Cr
Cu
Unifled Soil Classlflcation
Perchlorate - lon Chromatography
HPLC Analysis HMX
HPLC Analysis for NG
Cyanide distlllation/colohmetric
pH Electrode Measurement
Sulfate Analysis by IC
ICP/GFAA Metals Digestion
Sonication Extraction
ICP Metels Analysis (RCRA)
ICP Metels Analysis (RCRA)
ICP Metels Analysis (RCRA)
ICP Metels Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metals Analysis (RCRA)
Mn ICP Metals Analysis (RCRA)
Nl
Pb
Sb
.Zn
ICP Metels Analysis (RCRA)
ICP Metals Analysis (RCRA)
ICP Metels Analysis (RCRA)
ICP Metals Analysis (RCRA)
GFAA Arsenic Analysis (RCRA)
CV Mercury Analysis (RCRA)
GFAA Thallium Analysis (RCRA)
GFAA Selenium Analysis (RCRA)
Volatile Organics
Semi-Volatile Organics
Received Coiiect Date/Time
Matrix
09/23/96 09/19/96 14:05
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Page 1 of 19
LS74-2 BACKGROUND 2Fr. TEST AREA 09/23/96 09/19/96 14:14
ASTM D2488-84 UniTied Soil Classlflcation
SOP 302 Perchlorate - lon Chromatography
SOP 420 HPLC Analysis HMX
SOP 420 HPLC Analysis for NG
SW 846, 9012 Cyanide distillation/colorimetric
SW 846, 9045 pH Electrode Measurement
SW 846, 9056 Sulfate Analysis by IC
SW-846, 3050 ICP/GF/VA Metals Digestion
SW-846, 3550 Sonication E)(tractlon
SW-846,6010 Ag ICP Metels Analysis (RCRA)
SW-846, 6010 B ICP Metels Analysis (RCRA)
SW-846,6010 Be ICP Metels Analysis (RCRA)
SW-846,6010 Cd ICP Metels Analysis (RCRA)
SW-846,6010 Cr ICP Metels Analysis (RCRA)
SW-846, 6010 Cu ICP Metels Analysis (RCRA)
SW-846, 6010 Mn ICP Metals Analysis (RCRA)
SW-846,6010 Nl ICP Metels Analysis (RCRA)
SW-846,6010 Pb ICP Metels Analysis (RCRA)
SW-646, 6010 Sb ICP Metels Analysis (RCRA)
SW-846,6010 Zn ICP Metels Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7481 GFAA Tiiallium Analysis (RCRA)
SW-846, 7740 GFAA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
SW-846, 8270 Semi-Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Page 2 of 19
L574-3 BACKGROUND 6FT. TEST AREA 09/23/96 09/19/9614:30
ASTM D2488-84 Unified Soil Classlflcation
SOP 302 Perchlorate - lon Chromatography
SOP 420 HPLC Analysis HMX
SOP 420 HPLC Analysis for NG
SW 846, 9012 Cyanide distillation/colorimetric
SW 846, 9045 pH Electrode Measurement
SW 846, 9056 Sultete Analysis by IC
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846, 3550 Sonication Extraction
SW-846,6010 Ag ICP Metels Analysis (RCRA)
SW-846, 6010 B ICP Metels Analysis (RCRA)
SW-846, 6010 Be ICP Metels Analysis (RCRA)
SW-846, 6010 Cd ICP Metels Analysis (RCRA)
SW-S46, 6010 Cr ICP Metals Analysis (RCRA)
SW-846,6010 Cu ICP Metals Analysis (RCRA)
SW-846, 6010 Mn ICP Metals Analysis (RCRA)
SW-846,6010 Ni ICP Metals Analysis (RCRA)
SW-846,6010 Pb ICP Metels Analysis (RCRA)
SW-S46, 6010 Sb ICP Metals Analysis (RCRA)
SW-846,6010 2n ICP Metels Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7481 GFAiA Thallium Analysis (RCRA)
SW-846, 7740 GFAA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
SW-846, 8270 Semi-Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Page 3 of 19
L574-4 BACKGROUND 10FT. TEST AREA 09/23/96 09/19/9614:40
#
ASTM D2488-84 Unified Soil Classlflcation
SOP 302 Perchlofate • lon Chromatography
SOP 420 HPLC Aiiaiysis HMX
SOP 420 HPLC Analysis for NG
SW 846, 9012 Cyanide distillation/colorimetric
SW 846, 9045 pH Electrode Measurement
SW 846, 9056 Sulfate Analysis by 10
SW-846, 3050 ICP/GFAA Metals Digestion
SW-846, 3550 Sonication Extraction
SW-846,6010 Ag ICP Metels Analysis (RCRA)
SW-846, 6010 B ICP Metels Analysis (RCRA)
SW-846,6010 Be ICP Metels Analysis (RCRA)
SW-846, 6010 Cd ICP Metels Analysis (RCRA)
SW-846,6010 Cr ICP Metels Analysis (RCRA)
SW-846,6010 Cu ICP Metels Analysis (RCRA)
SW-846, 6010 Mn ICP Metels Analysis (RCRA)
SW-846,6010 Ni ICP Metels Analysis (RCRA)
SW-846,6010 Pb ICP Metels Analysis (RCRA)
SW-846,6010 Sb ICP Metals Analysis (RCRA)
SW-846,6010 Zn ICP Metels Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7481 GFAA Thallium Analysis (RCRA)
SW-846, 7740 GFAA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
SW-846, 8270 Semi-Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Page 4 of 19
L574-5 BACKGROUND 15FT. TEST AREA Q9I23IX 09/19/96 15:00
•
ASTM D2488-84 Unified Soil Classlflcation
SOP 302 Perchlorate - lon Chromatography
SOP 420 HPLC Analysis HMX
SOP 420 HPLC Analysis for NG
SW 846, 9012 Cyanide distillation/colorimetric
SW 846, 9045 pH Electrode Measurement
SW 846, 90S6 Sulfate Analysis by IC
SW-846, 3050 ICP/GFM Metals Digestion
SW-846, 3550 Sonication Extraction
SW-846,6010 Ag ICP Metels Analysis (RCRA)
SW-846, 6010 B ICP Metels Analysis (RCRA)
SW-846,6010 Be ICP Metels Analysis (RCRA)
SW-846,6010 Cd ICP Metels Analysis (RCRA)
SW-846,6010 Cr ICP Metals Analysis (RCRA)
SW-846, 6010 Cu ICP Metals Analysis (RCRA)
SW-846, 6010 Mn ICP Metels Analysis (RCRA)
SW-846,6010 Ni ICP Metels Analysis (RCRA)
SW-846,6010 Pb ICP Metels Analysis (RCRA)
SW-846,6010 Sb ICP Metals Analysis (RCRA)
SW-846,6010 Zn ICP Metals Analysis (RCRA)
SW-846, 7060 GFAA Arsenic Analysis (RCRA)
SW-846, 7471A CV Mercury Analysis (RCRA)
SW-846, 7481 GFAA Thallium Analysis (RCRA)
SW-846, 7740 GFAA Selenium Analysis (RCRA)
SW-846, 8260 Volatile Organics
SW-846, 8270 Semi-Volatile Organics
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Page 5 of 19
•
Work Order Comments
(L574-1) Sandy Organic Soil (OL/OH); About 95% fines with a few pebbles and roots. Has
organic odor. A wet, dark brown sample with low plasticity, low toughness, and no dilatancy;
weak to medium reaction with HCI; Hard dry
strength.
(L574-2) Well Graded Gravel with Clay & Sand (GW-GC); About 50% subrounded and 50%
subangular sand particles, with high plasticity, no dilatancy, high toughness. A moist brown
sample which exhibits a strong reaction with HCI; dry strength is very hard and the maximum
particle size is approx. 1-2
inches.
(L574-3) Well Graded Gravel with Silt (GW-GM); A grayish-tan, dry sample with less than 5%
fines. Most particles are subrounded with no dilatancy, low toughness, and nonplastic. Strong
reaction with HCI, very hard dry strength with a max. particle size of approx. 2
inches.
(L574-4) Well Graded Gravel with Clay (GW-GC); A light brov/n to copper, dry, inorganic
sample with approx. 10% fines, max. particle size about 11/2 inches. Particles are subangular
gravel with rapid dilatancy, medium toughness, medium plasticity, and very hard dry
strength.
(L574-5) Pooriy Graded Sand with Silt (SP-SM); A moist, light copper-brown inorganic with
about 90% fines. Three rocks with a diameter of 3/4 inch are present. A pooriy distributed
subrounded gravel with slow dilatancy, low toughness, and nonplastic; Dry strength is low.
'^^^f/u^^'f. U'l^^Oi^^' /l//zM(.-
// Certified By Date
This is to certify that the following samples were analyzed using good laboratory practices to show
the folowing results:
Page 6 of 19
Listing of Results by Sample
•
1 Sample
630-20-6
71-55-6
79-34-5
79-005
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-501
107-06-2
78-87-5
10S-67-8
541-73-1
142-28-9
106-46-7
590-207
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-101
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-907
75-003
67-66-3
74-87-3
156-59-4
ID: BACKGROUND SURFACE
Test Parameter
UNIFIED SOIL CLASSIFICATION
PERCHLORATE
HMX
NITROGLYCERIN
CYANIDE
PH
SULFATE
ICP/GFAA METALS DIGESTION
SONICATION EXTRACTION
ANTIMONY
BERYLLIUM
BORON
CADMIUM
CHROMIUM
COPPER
LEAD
MANGANESE
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
THALUUM
SELENIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1.2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
TEST AREA
Result
u
u
u
0.255
7.82
9.5
U
0.3
7.8
0.4
13
7
U
181
6.3
U
29
7.4
0.02
U
2:2
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
4.9 JB ugAg
U
U
ug/kg
ug/kg
Oet.
Limit
3.8
0.5
0.5
0.149
0.8
3.1
01
0.4
01
0.3
01
1.6
01
0.6
0.2
0.2
0.9
0.01
0.6
1.2
0.2
0.2
0.3
0.2
01
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
01
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
0.4
0.6
0.2
Lab ID: L574-1 Collect Date: 09/19/96 14:05
Rep. Oil.
Limit Factor Method
ASTM D2488-84
19 25 SOP 302
0.5 1
0.5 1
0.746 1
1
SOP 420
SOP 420
SW 846, 9012
SW 846, 9045
3.8 25 SW 846,9056
16 1
0.6 1
1.9
0.6
1.6
0.6
7.8
0.6
3.1
0.9
1.2
2.5
0.03
2
4.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 3050
SW-846, 3550
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-S46, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471A
SW-846, 7481
SW-846, 7740
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW^6, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-646,8260
1 SW-846,8260
1 SW-S46,8260
1 SW-846,8260
1 SW-846,8260
Analyst
MTB
CRS
KMS
KMS
KEN
MTB
CRS
KWB
SDM
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
CRS
CRS
CRS
MMR
MMR
MMR
MMR
MMR
IvHwiK
MMR
MMR
MUIR
MMR
MMR
MMR
MMR
MUIR
MUIR
MMR
MMR
MMR
MUIR
MUIR
MMR
MUIR
MAR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MUIR
MMR
Test Date
10/21/96 09:00
10/15/9617:54
10/11/96 10:43
10/11/96 10:43
10/03/96 13:00
10/08/96 13:00
10/17/96 15:15
10/18/96 00:00
09/25/96 00:00
10/23/96 13:40
10/23/96 13:40
10/23/9613:40
10/23/96 13:40
10/23/96 13:40
10/23/96 13:40
10/23/96 13:40
10/23/96 13:40
10/23/96 13:40
10/23/96 13:40
10/23/96 13:40
10/23/96 16:51
10/17/96 13.20
10/24/96 10:52
10/23/96 14:07
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17.03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/9617:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/9617:03
10/01/96 17:03
10/01/96 17:03
10/01/9617:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
Page 7 Of 19
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-203
95-47-6
135-98-8
100-42-5
9&06-6
127-18-4
108-88-3
156-605
10061-02-6
79-01-6
75-69-4
75-01-4
120-82-1
95-501
541-73-1
106-46-7
95-95-4
88-06-2
120-83-2
105-67-9
51-28-5
121-14-2
606-202
91-58-7
95-57-8
91-57-6
95-48-7
88-74-4
88-75-5
56-55-3
99-09-2
534-52-1
101-55-3
59-507
106-47-8
7005-72-3
106-44-5
100-01-06
100-02-7
83-32-9
208-96-8
12012-7
56-55-3
5032-8
205-99-2
191-24-2
207-08-9
111-91-1
111-44-4
108-601
117-81-7
85-68-7
12012-7
218-01-9
84-74-2
117-84-0
S3-703
132-64-9
84-66-2
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1,2,4-TRICHLOROBENZENE
1,2-OICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-OlCHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DICHLOROPHENOL
2,4-DIMETHYLPHENOL
2,4-DINITROPHENOL
2,4-DlNlTROTOLUENE
2,6-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
2-METHYLNAPHTHALENE
2-METHYLPHENOL
2-NITROANILINE
2-NITROPHENOL
3,3'-DICHLOROBENZIDINE
3-NITROANILINE
4,6-DINITRO-2-METHYLPHENOL
4-BROMOPHENYL-PHENYLETHER
4-CHLORO-3-METHYLPHENOL
4-CHLOROANIUNE
4-CHLOROPHENYL-PHENYLETHER
4-METHYLPHENOL
4-NITROANILINE
4-NITROPHENOL
ACENAPHTHENE
ACENAPHTHYLENE
ANTHRACENE
BENZO(A)ANTHRACENE
BENZO(A)PYRENE
BENZO(B)FLUORANTHENE
BENZO(G,H,l)PERYLENE
BENZO(K)FLUORANTHENE
BIS(2-CHLOROETHOXY)METHANE
BIS(2-CHLOROETHYL)ETHER
BIS(2-CHLOROISOPROPYL)ETHER
BIS(2-ETHYLHEXYL)PHTHALATE
BUTYLBENZYLPHTHALATE
CARBAZOLE
CHRYSENE
DI-N-BUTYLPHTHALATE
DI-N-OCTYLPHTHALATE
DIBENZ(A,H)ANTHRACENE
DIBENZOFURAN
DIETHYLPHTHALATE
U
U
U
U
U
U
U
U
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
1.4 JB ugAg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
63
63
63
147
133
90
90
90
1400
190
63
63
110
73
77
50
120
333
80
800
63
100
60
140
133
120
80
63
117
63
260
83
167
137
160
177
190
190
83
83
333
83
83
83
83
100
63
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10
10
10
10
10
10
333
333
333
333
333
333
333
333
1670
333
333
333
333
333
333
1670
333
667
1670
1670
333
667
667
333
333
1670
1670
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-S46, 8260
SW-646, 8260
SW-846, 8260
SW-846, 8260
SW-S46,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-646, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-S46, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
1 SW-846,8270
1 SW-846,8270
I SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846.8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
mvin
MMR
MUIR
MUIR
MUIR
MMR
MMR
MUIR
MUIR
MUIR
MAR
MAR
MMR
MUIR
MMR
MUIR
MMR
MUIR
MUIR
MMR
MMR
MUIR
MMR
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/9617:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17.03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/9617:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
10/01/9617:03
10/01/96 17:03
10/01/96 17:03
10/01/96 17:03
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/9616:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:1S
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/9616:15
09/26/96 16:15
09/26^616:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/25/96 16:15
09/26/96 16:15
09/26«6 16:15
09/25/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
Page 8 Of 19
131-11-3
206-44-0
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
193-39-5
78^9-1
621-64-7
86-306
91-203
98-95-3
87-86-5
85-01-8
108-95-2
129-00-0
1 Sample
63O20-6
71-S5-6
79-34-5
79-005
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-501
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590207
78-93-3
95-49-8
591-78-6
106*43-4
DIMETHYLPHTHALATE
FLUORANTHENE
FLUORENE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROCYCLOPENTADIENE
HEXACHLOROETHANE
INDENO(1,2,3-CD)PYRENE
ISOPHORONE
N-NITROSO-DI-N-PROPYLAMINE
N-NITROSODIPHENYLAMINE -
NAPHTHALENE
NITROBENZENE
PENTACHLOROPHENOL
PHENANTHRENE
PHENOL
PYRENE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
ID: BACKGROUND 2FT. TEST AREA
Test Parameter
UNIFIED SOIL CLASSIFICATION
PERCHLORATE
HMX
NITROGLYCERIN
CYANIDE
PH
SULFATE
ICP/GFAA METALS DIGESTION
SONICATION EXTRACTION
ANTIMONY
BERYLLIUM
BORON
CADMIUM
CHROMIUM
COPPER
LEAD
MANGANESE
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
THALLIUM
SELENIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
1,2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3.5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
Result
U
u
u
0157
7.88
7.1
3.3
0.3
8.5
0.4
16
8.4
U
189
8
U
34
6.5
0.02
0.8
1.4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
S3
73
63
63
30
200
53
123
73
400
63
53
47
120
180
50
63
Det.
Limit
4.4
0.5
0.5
015
0.9
3.2
Ol
0.4
0.1
0.3
Ol
1.6
Ol
0.6
0.2
0.3
0.9
0.01
0.7
1.3
0.2
0.2
0.3
0.2
Ol
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
Ol
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
333
333
333
333
333
333
333
333
333
333
333
333
333
1670
333
333
333
Lab ID:
Rep.
Limit
22
0.5
0.5
0.749
4.4
16
0.6
1.9
0.6
1.6
0.6
8.1
0.6
3.2
0.97
1.3
2.6
0.04
2.1
4.4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
09/26/96 16:15
09/26«6 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26/96 16:15
09/26^6 16:15
09/26/96 16:15
LS:r4-2 Collect Date: 09/19/96 14:14
Dil.
Faicrtor Method
::s
1
1
1
1
25
ASTM D2488-84
SOP 302
SOP 420
SOP 420
SW 846, 9012
SW 846, 9045
SW 846, 9056
SW-846, 3050
SW-846, 3550
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471A
SW-846, 7481
SW-846, 7740
SW-&46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-S46, 8260
SW-846,8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
Analyst
MTB
CRS
KMS
KMS
KEN
MTB
CRS
KWB
SDM
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
CRS
CRS
CRS
MUIR
MAR
MUIR
MUIR
MUIR
MMR
MMR
MUIR
MUIR
MMR
MUIR
MUIR
MUIR
MMR
MMR
MMR
MUIR
MUIR
MMR
MUIR
MMR
MUIR
MAR
MUIR
MUIR
Test Date
10/21/96 09:00
10/15/96 18:03
10/11/96 11:07
10/11/96 11:07
10/03/96 13:00
10/08/96 13:00
10/17/96 15:31
10/18/96 00:00
09/25/96 00:00
10/23/9613:54
10/23/96 13:54
10/23/96 13:54
10/23/96 13:54
10/23/96 13:54
10/23/96 13:54
10/23/9613:54
10/23/96 13:54
10/23/9613.54
10/23/96 13:54
10/23/96 13:54
10/23/96 17:15
10/17/96 13:24
10/24/96 11:11
10/23/96 14:29
10/01/96 17:41
10/01/96 17:41
10/01/9617:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/9617:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/9617:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
=age9 of 19
99-87-6 4-lSOPROPYLTOLUENE
108-101 4-METHYL-2-PENTANONE
67-64-1 ACETONE
71-43-2 BENZENE
108-86-1 BROMOBENZENE
74-97-5 BROMOCHLOROMETHANE
75-27-4 BROMODICHLOROMETHANE
75-25-2 BROMOFORM
74-83-9 BROMOMETHANE
56-23-5 CARBON TETRACHLORIDE
108-907 CHLOROBENZENE
75-003 CHLOROETHANE
67-66-3 CHLOROFORM
74-87-3 CHLOROMETHANE
156-59-4 CIS-1,2-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1 DIBROMOCHLOROMETHANE
74-95-3 DIBROMOMETHANE
75-71-8 DICHLORODIFLUOROMETHANE
100-41-4 ETHYLBENZENE
87-68-3 HEXACHLOROBUTADIENE
98-82-8 ISOPROPYLBENZENE
108-38-3 M,P-XYLENE
75-09-2 METHYLENE CHLORIDE
104-51-8 N-BUTYLBENZENE
103-65-1 N-PROPYLBENZENE
91-203 NAPHTHALENE
95-47-6 O-XYLENE
135-98-8 SEC-BUTYLBENZENE
100-42-5 STYRENE
98-06-6 TERT-BUTYLBENZENE
127-18-4 TETRACHLOROETHENE
108-88-3 TOLUENE
1S6-605 TRANS-1.2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
79-01-6 TRICHLOROETHENE
75-69-4 TRICHLOROFLUOROMETHANE
75-01-4 VINYL CHLORIDE
120-82-1 1,2,4-TRICHLOROBENZENE
95-501 1,2-DICHLOROBENZENE
541-73-1 1,3-DICHLOROBENZENE
106-46-7 1,4-DICHLOROBENZENE
95-95-4 2,4,5-TRICHLOROPHENOL
88-06-2 2,4,6-TRICHLOROPHENOL
120-83-2 2,4-DICHLOROPHENOL
105-67-9 2,4-DIMETHYLPHENOL
51-28-5 2,4-DINITROPHENOL
121-14-2 2,4-DINITROTOLUENE
606-202 2,6-DINITROTOLUENE
91-58-7 2-CHLORONAPHTHALENE
95-57-8 2-CHLOROPHENOL
91-57-6 2-METHYLNAPHTHALENE
95-48-7 2-METHYLPHENOL
88-74-4 2-NITROANILINE
88-75-5 2-NITROPHENOL
56-55-3 3,3'-DICHLOROBENZIDINE
99-09-2 3-NITROANILINE
534-52-1 4,6-DINITRO-2-METHYLPHENOL
101-55-3 4-BROMOPHENYL-PHENYLETHER
59-507 4-CHLORO-3-METHYLPHENOL
106-47-8 4-CHLOROANILINE
7005-72-3 4-CHLOROPHENYL-PHENYLETHER
106-44-5 4-METHYLPHENOL
100-01-06 4-NITROANILINE
100-02-7 4-NITROPHENOL
83-32-9 ACENAPHTHENE
208-96-8 ACENAPHTHYLENE
12012-7 ANTHRACENE
56-55-3 BENZO(A)ANTHRACENE
5032-8 BENZO(A)PYRENE
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
4.5 JB ugAg
U
U
U
U
U
U
U
U
U
U
11 B
U
U
U
U
U
U
u
u
2.2 J
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
0.2
10
10
0.2
0.2
0.2
0.3
Ol
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
63
63
63
147
133
90
90
90
1400
190
63
63
110
73
77
50
120
333
80
800
63
100
60
140
133
120
80
63
117
63
260
83
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
333
333
333
333
333
333
333
333
1670
333
333
333
333
333
333
1670
333
667
1670
1670
333
667
667
333
333
1670
1670
333
333
333
333
333
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-S46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
MAR
MMR
MMR
MUIR
MMR
MUIR
MMR
MUIR
MUIR
MMR
MMR
MMR
MMR
MUIR
MUIR
MMR
MMR
MMR
MUIR
MMR
MMR
MMR
MUIR
MUIR
MUIR
MUIR
MMR
MMR
MMR
MMR
Ml^R
MUIR
MUIR
MMR
MMR
MUIR
MMR
MMR
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
10/01/96 17:41
10/01/9617:41
10/01/9617:41
10/01/96 17:41
10/01/96 17:41
10/01/9617:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/9617:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/9617:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
10/01/96 17.41
10/01/96 17:41
10/01/96 17:41
10/01/96 17:41
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/9617:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/9617:01
09/26/96 17:01
09/26/9617:01
09/26/9617:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/9617:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/9617:01
09/26/9617:01
Page 10 of 19
205-99-2
191-24-2
207-08-9
111-91-1
111-44-4
108-601
117-81-7
85-68-7
12012-7
21801-9
84-74-2
117-84-0
53-703
132-64-9
84-66-2
131-11-3
206-44-0
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
193-39-5
78-59-1
621-64-7
86-306
91-203
98-95-3
87-86-5
85-01-8
108-95-2
129-00-0
1 Sample
63O20-6
71-55-6
79-34-5
79-005
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
BENZO(B)FLUORANTHENE
BENZO(G,H,l)PERYLENE
BENZO(K)FLUORANTHENE
BIS(2-CHLOROETHOXY)METHANE
BIS(2-CHLOROETHYL)ETHER
BIS(2-CHLOROISOPROPYL)ETHER
BIS(2-ETHYLHEXYL)PHTHALATE
BUTYLBENZYLPHTHALATE
CARBAZOLE
CHRYSENE
DI-N-BUTYLPHTHALATE
DI-N-OCTYLPHTHALATE
DIBENZ(A,H)ANTHRACENE
DIBENZOFURAN
DIETHYLPHTHAUTE
DIMETHYLPHTHALATE
FLUORANTHENE
FLUORENE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROCYCLOPENTADIENE
HEXACHLOROETHANE
INDENO(1,2,3-CD)PYRENE
ISOPHORONE
N-NITROSO-Dl-N-PROPYLAMINE
N-NITROSODIPHENYLAMINE
NAPHTHALENE
NITROBENZENE
PENTACHLOROPHENOL
PHENANTHRENE
PHENOL
PYRENE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
ID: BACKGROUND 6FT. TEST AREA
Test Parameter
UNIFIED SOIL CLASSIFICATION
PERCHLORATE
HMX
NITROGLYCERIN
CYANIDE
PH
SULFATE
ICP/GFAA METALS DIGESTION
SONICATION EXTRACTION
ANTIMONY
BERYLLIUM
BORON
CADMIUM
CHROMIUM
COPPER
LEAD
MANGANESE
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
THALLIUM
SELENIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1,1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1,2,3-TRICHLOROPROPANE
1,2,4-TRICHLOROBENZENE
Resutt
u
u
u
0.205
8.07
9.2
U
0.3
23.4
Ol
13
5.8
U
120
9.4
0.2
31
9.6
U
07
2.1
U
U
U
U
U
U
U
U
U
U
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
167
137
160
177
190
190
83
83
333
83
83
83
83
100
63
53
73
63
63
30
200
53
123
73
400
63
S3
47
120
180
50
63
Oet.
Limit
3.8
0.5
0.5
0148
0.8
3.3
0.1
0.4
0.1
0.3
01
1.6
0.1
0.7
0.2
0.3
0.9
0.01
07
1.3
0.2
0.2
0.3
0.2
Ol
0.6
0.2
0.2
0.2
0.2
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
1670
333
333
333
UblD:
Rep.
Limit
19
0.5
0.5
0.742
3.8
16
0.7
2
0.7
1.6
0.7
8.2
0.7
3.3
0.98
1.3
2.6
0.04
2.1
4.5
10
10
10
10
10
10
10
10
10
10
1
1
1
1
1
1
1
1
11
11
11
11
11
1!
K
11
11
1
1
•1
1
•1
'1
•\
•\
•1
•1
•\
•1
•1
•I
1
SW-846, 8270
SW-S46, 8270
SW-846, 8270
SW-846,8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846,8270
SW-846, 8270
SW-S46, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
L5:'4-3 Collect Date:
DiL
Fa<rtor Method
25
I
1
1
1
35
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
ASTM D2488-84
SOP 302
SOP 420
SOP 420
SW 846, 9012
SW 846, 9045
SW 846, 9056
SW-846, 3050
SW-846, 3550
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846,6010
SW-S46, 6010
SW-846.6010
SW-846,6010
SW-846, 6010
SW-846,6010
SW-846,6010
SW-846, 7060
SW-846, 7471A
SW-846, 7481
SW-846, 7740
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
09/26/96 17:01
09/26/96 17:01
09/26^6 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/9617.01
09/26/9617:01
09/26/96 17:01
09/26/9617:01
09/26/96 17.01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/96 17:01
09/26/9617:01
09/26/96 17:01
09/26/96 17:01
09/26/9617:01
09/26/96 17:01
09/26/96 17:01
39/19/96 14:30
Analyst Test Date
MTB
CRS
KMS
KMS
KEN
MTB
CRS
KWB
SDM
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
CRS
CRS
CRS
CRS
MMR
MMR
MUIR
MUIR
MUIR
MUIR
MMR
MAR
MUIR
MMR
10/21/96 09:00
10/15/96 18:11
10/11/96 11:15
10/11/96 11:15
10/03^613:00
10/08/96 13:00
10/17/96 15:47
10/18/96 00:00
09/25/96 00:00
10/23/9613:57
10/23/96 13:57
10/23/96 13:57
10/23/96 13:57
10/23«6 13:57
10/23^6 13:57
10/23^6 13:57
10/23^6 13:57
10/23«6 13:57
10/23/96 13:57
10/23/96 13:57
10/23/96 17:23
10/17/96 13:32
10/24/96 11:20
10/23/96 14:34
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
Pagell of 19
95-63-6
96-12-8
106-93-4
95-501
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590207
78-93-3
95-4&-8
591-78-6
106-43-4
99-87-6
108-101
67-64-1
71-43-2
108-86-1
74-97-S
75-27-4
75-25-2
74-83-9
56-23-5
108-907
75-003
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
103-65-1
91-203
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-605
10061-02-6
79-01-6
75-69-4
75-01-4
120-82-1
95-501
541-73-1
106-46-7
95-95-4
88-06-2
120-83-2
105-67-9
51-28-5
121-14-2
606-202
91-58-7
95-57-8
91-57-6
95-48-7
88-74-4
88-75-5
1.2,4-TRIMETHYLBENZENE
1,2-DIBROMO-3-CHLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1,3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON TETRACHLORIDE.
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
CIS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROti«>CHLOROMETHANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1,2,4-TRICHLOROBENZFNE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2.4,6-TRICHLOROPHENOL
2,4-DICHLOROPHENOL
2,4-DIMEfHYLPHENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
2-METHYLNAPHTHALENE
2-METHYLPHENOL
2-NlTROANILINE
2-NITROPHENOL
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
4.9 JB ugAg
u
U
U
U
U
U
U
U
U
U
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
3.7 JB ug/kg
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ug/kg
0.2
0.2
0.2
Ol
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
0.1
0.4
0.3
0.2
0.4
04
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
02
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
63
63
63
147
133
90
90
90
1400
190
63
63
110
73
77
50
120
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10
10
10
10
10
10
10 1
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
333
333
333
333
333
333
333
333
1670
333
333
333
333
333
333
1670
333
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 6260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
SW-846, 8260
SW-846, 8260
1 SW-846,8260
1 SW-S46,8260
1 SW-846,8260
1 SW-846.8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-«46,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8260
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
MulR
MMR
MMR
lUMR
MMR
MMR
MUIR
MMR
MUIR
MUIR
MUIR
MMR
MUIR
MMR
MMR
MMR
MUIR
MUIR
MMR
MUIR
MMR
MUIR
MUIR
MUIR
MUIR
MMR
MMR
MMR
MMR
MUIR
MMR
MMR
MUIR
MUIR
MMR
MUIR
MMR
MUIR
MUIR
MMR
MUIR
MUIR
MMR
MMR
MUIR
MMR
- MUIR
MMR
MMR
MMR
MUIR
MUIR
MAR
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18.18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
10/01/96 18:18
09/26/96 17:46
09/26/96 17:46
09/26/9617:46
09/26/96 17:46
09/26/96 17:46
09/26/96 17:46
09/26/96 17:46
09/26/96 17:46
09/26/9617:46
09/26/96 17:46
09/26/96 17:46
09/26^617:46
09/26/96 17:46
09/26/96 17:46
09/26/96 17:46
09/26/96 17:46
09/26/96 17:46
Page 12 of 19
56-55-3
99-09-2
534-52-1
101-55-3
59-507
106-47-8
7005-72-3
106-44-5
100-01-06
10O02-7
83-32-9
208-96-8
12012-7
56-55-3
5032-8
205-99-2
191-24-2
207-08-9
111-91-1
108*01
117-81-7
85-68-7
12012-7
218-01-9
84-74-2
117-84-0
53-703
132-64-9
8446-2
131-11-3
206-44-0
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
193-39-5
78-59-1
621-64-7
86-306
91-203
98-95-3
87-86-5
85-01-8
108-95-2
129-00-0
3,3'-DICHLOROBENZIDINE
3-NITROANlLINE
4,6-DINITRO-2-METHYLPHENOL
4-BROMOPHENYL-PHENYLETHER
4-CHLORO-3-METHYLPHENOL
4-CHLOROANILINE
4-CHLOROPHENYL-PHENYLETHER
4*IETHYLPHENOL
4-NITROANILINE
4-NrrROPHENOL
ACENAPHTHENE
ACENAPHTHYLENE
ANTHRACENE
BENZO(A)ANTHRACENE
BENZO(A)PYRENE
BENZO(B)FLUORANTHENE
BENZO(G,H,0PERYLENE
BENZO(K)FLUORANTHENE
BIS(2-CHLOROETHOXY)METHANE
BIS(2-CHLOROETHYL)ETHER
BlS(2-CHLOROISOPROPYL)ETHER
BIS(2-ETHYLHEXYL)PHTHALATE
BUTYLBENZYLPHTHALATE
CARBAZOLE
CHRYSENE
DI-N-BUTYLPHTHALATE
DI-N-OCTYLPHTHALATE
DIBENZ(A,H)ANTHRACENE
DIBENZOFURAN
DIETHYLPHTHALATE
DIMETHYLPHTHALATE
FLUORANTHENE
FLUORENE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROCYCLOPENTADIENE
HEXACHLOROETHANE
INDENO(1,2,3-CD)PYRENE
ISOPHORONE
N-NITROSO-DI-N-PROPYLAMINE
N-NITROSODIPHENYLAMINE .
NAPHTHALENE
NITROBENZENE
PENTACHLOROPHENOL
PHENANTHRENE
PHENOL
PYRENE
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
1 SamplelD: BACKGROUND 10FT. TEST AREA
Test Parameter
UNIFIED SOIL CLASSIFICATION
PERCHLORATE
HMX
NITROGLYCERIN
CYANIDE
PH
SULFATE
ICP/GFAA METALS DIGESTION
SONICATION EXTRACTION
ANTIMONY
BERYLLIUM
BORON
CADMIUM
CHROMIUM
COPPER
LEAD
MANGANESE
NICKEL
SILVER
Result
u
u
u
0168
8.07
6.9
U
0.3
10.5
0.9
12
4.8
U
167
6.4
U
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
Units
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
333
80
800
63
100
60
140
133
120
80
63
117
63
260
83
167
137
160
177
190
190
83
83
333
83
83
83
83
100
63
53
73
63
63
30
200
53
123
73
400
63
53
47
120
180
50
63
Det.
Limit
3.9
0.5
0.5
0148
0.8
3.2
Ol
0.4
Ol
0.3
0.1
1.6
Ol
0.6
0.2
667
1670
1670
333
667
667
333
333
1670
1670
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
1670
333
333
333
Lab ID:
Rep.
Limit
19
0.5
0.5
0.742
3.9
16
0.6
2
0.6
1.6
0.6
8.1
0.6
3.2
0.97
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846,8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846,8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846,8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846,8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846. 8270
SW-846, 8270
SW-846, 8270
SW-846. 8270
SW-846, 8270
SW-S46, 8270
SW-«46, 8270
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JWV
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
1.574-4 Collect Date:
Dil.
Factor Method
25
2i5
ASTMD2488-84
SOP 302
SOP 420
SOP 420
SW 846, 9012
SW 846, 9045
SW 846. 9056
SW-846, 3050
SW-846, 3550
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-S46, 6010
SW-846, 6010
SW-846,6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
09/26«6 17:46
09/26«6 17:46
09/26«6 17:46
09/26/96 17:46
09/26/9617:46
09/26/96 17:46
09/26/96 17:46
09/26/96 17:46
09/26/96 17:46
09/25/96 17:46
09/26/96 17:46
09/26/96 17:46
09/26/96 17:46
09/26/9617:46
09/26/96 17:46
09/26/96 17:46
09/26/9617:46
09/26/96 17:46
09/26/96 17:46
09/26«6 17:46
09/26/96 17:46
09/26/9617:46
09/26/96 17:46
09/26/9617:46
09/26/96 17:46
09/26/96 17:46
09/26^617:46
09/26/96 17:46
09/26/9617:46
09/26/9617.46
09/26/96 17:46
09/26^6 17:46
09/26/96 17:46
09/26/96 17:46
09/26/96 17:46
09/26/96 17:46
09/26^617:46
09/26/9617:46
09/26/96 17:46
09/26/96 17:46
09/26/96 17:46
09/26/96 17:46
09/26^617:46
09/26/96 17:46
09/26^617:46
09/26/96 17:46
09/26/96 17:46
09/19/96 14:40
Analyst Test Date
MTB
CRS
KMS
KMS
KEN
MTB
CRS
KWB
SDM
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
KWB
10/21/96 09:00
10/15/96 18:19
10/11/96 11:22
10/11/96 11:22
10/03/96 13:00
10/08^613:00
10/17/96 16:03
10/18/96 00:00
09/25/96 00:00
10/23/96 13:59
10/23^613:59
10/23/96 13:59
10/23/96 13.59
10/23/96 13:59
10/23/96 13:59
10/23/96 13:59
10/23/96 13:59
10/23/96 13:59
10/23/96 13:59
Page 13 Of 19
ZINC
ARSENIC
MERCURY
THALLIUM
SELENIUM
63O20-6 1,1,1,2-TETRACHLOROETHANE
71-55-6 1,1,1-TRICHLOROETHANE
79-34-5 1,1,2,2-TETRACHLOROETHANE
79-005 1,1,2-TRICHLOROETHANE
75-34-3 1,1-DICHLOROETHANE
75-35-4 1,1-DICHLOROETHENE
563-58-6 1,1-DICHLOROPROPENE
87-61-6 1,2,3-TRICHLOROBENZENE
96-18-4 1,2,3-TRICHLOROPROPANE
12082-1 1,2,4-TRICHLOROBENZENE
95-63-6 1,2,4-TRIMETHYLBENZENE
96-12-8 1,2-DIBROMO-3-CHLOROPROPAN
106-93-4 1,2-DIBROMOETHANE
95-501 1,2-DICHLOROBENZENE
107-06-2 1,2-DICHLOROETHANE
78-87-5 1,2-DICHLOROPROPANE
108-67-8 1,3,5-TRIMETHYLBENZENE .
541-73-1 1,3-DICHLOROBENZENE
142-28-9 1,3-DICHLOROPROPANE
106-46-7 1,4-DICHLOROBENZENE
590207 2,2-DICHLOROPROPANE
78-93-3 2-BUTANONE
95-49-8 2-CHLOROTOLUENE
591-78-6 2-HEXANONE
106-43-4 4-CHLOROTOLUENE
99-87-6 4-ISOPROPYLTOLUENE
108-101 4-METHYL-2-PENTANONE
67-64-1 ACETONE
71-43-2 BENZENE
108-86-1 BROMOBENZENE
74-97-5 BROMOCHLOROMETHANE
75-27-4 BROMODICHLOROMETHANE
75-25-2 BROMOFORM
74-83-9 BROMOMETHANE
56-23-5 CARBON TETRACHLORIDE
108-907 CHLOROBENZENE
75-003 CHLOROETHANE
67-66-3 CHLOROFORM
74-67-3 CHLOROMETHANE
156-59-4 CIS-1,2-DICHLOROETHENE
10061-01-5 CIS-1,3-DICHLOROPROPENE
124-48-1 DIBROMOCHLOROMETHANE
74-95-3 DIBROMOMETHANE
75-71-8 DICHLORODIFLUOROMETHANE
100-41-4 ETHYLBENZENE
87-68-3 HEXACHLOROBUTADIENE
98-82-8 ISOPROPYLBENZENE
108-38-3 M,P-XYLENE
75-09-2 METHYLENE CHLORIDE
104-51-8 N-BUTYLBENZENE
103-65-1 N-PROPYLBENZENE
91-203 NAPHTHALENE
95-47-6 O-XYLENE
135-98-8 SEC-BUTYLBENZENE
100-42-5 STYRENE
98-06-6 TERT-BUTYLBENZENE
127-18-4 TETRACHLOROETHENE
108-88-3 TOLUENE
156-605 TRANS-1,2-DICHLOROETHENE
10061-02-6 TRANS-1,3-DICHLOROPROPENE
79-01-6 TRICHLOROETHENE
75-69-4 TRICHLOROFLUOROMETHANE
75-01-4 VINYL CHLORIDE
12082-1 1,2,4-TRICHLOROBENZENE
95-501 1,2-DICHLOROBENZENE
24
6.5
0.04
1
2.7
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
4.7 JB ug/kg
U
U
U
U
U
u
u
u
u
u
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
7.2 JB ugAg
U
U
U
U
U
U
U
U
1.1 J
U
U
U
U
U
u
u
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
0.3
0.9
0.01
07
1.3
0.2
0.2
0.3
0.2
0.1
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
Ol
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
Ol
0.4
03
0.2
0.4
04
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
63
63
1.3
2.6
0.04
2.1
4.4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
333
333
SW-e46, 6010
SW-846, 7060
SW-846, 7471A
SW-846, 7481
SW-846, 7740
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW-646, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846. 8260
SW-846, 8260
SW-846, 8270
SW-846, 8270
KWB
CRS
CRS
CRS
CRS
MUIR
MUIR
MMR
MUIR
MAR
MUIR
MMR
MMR
MMR
MMR
MUIR
MMR
MUIR
MUIR
MUIR
MMR
MUIR
MMR
MUIR
MUIR
MulR
MUIR
MUIR
MUIR
MUIR
MUIR
MUIR
MMR
MUIR
MUIR
MUIR
Mt^R
MUIR
MMR
MMR
MMR
MMR
MMR
MMR
MAR
MMR
MMR
MMR
MMR
MUIR
MUIR
MUIR
MUIR
MUIR
MMR
Ml^R
MUIR
MAR
MMR
MAR
MUIR
MUIR
MUIR
MMR
MMR
MUIR
MUIR
MMR
JMA
JMA
10/23/96 13:59
10/23/96 17:35
10/17/96 13:36
10/24/9611:33
10/23/96 14:46
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/9618:56
10/01/96 18:56
10/01/96 18:56
10/01/9618:56
10/01/96 18:56
10/01/96 18:56
10/01/9618:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:55
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/9618:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/9618:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/9618:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/96 18:56
10/01/9618:56
09/26/96 18:31
09/26/96 18:31
Page 14 of 19
541-73-1
106-46-7
95-95-4
88-06-2
120-83-2
105-67-9
51-28-5
121-14-2
606-202
91-58-7
95-57-8
91-57-6
95-48-7
88-74-4
88-75-5
56-55-3
99-09-2
534-52-1
101-55-3
59-507
106-47-8
7005-72-3
106-44-5
100-01-06
10O02-7
83-32-9
208-96-8
12012-7
56-55-3
5032-8
205-99-2
191-24-2
207-08-9
111-91-1
111-44-4
108-601
117-81-7
85-68-7
12012-7
21801-9
84-74-2
117-84-0
53-703
132-64-9
84-66-2
131-11-3
206-44-0
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
193-39-5
78-59-1
621-64-7
86-306
91-203
98-95-3
87-86-5
85-01-8
108-95-2
129-00-0
1 Sample
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DICHLOROPHENOL
2,4-DIMETHYLPHENOL
2,4-DINn-ROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
2-METHYLNAPHTHALENE
2-METHYLPHENOL
2-NITROANILlNE
2-NlTROPHENOL
3,3'-DlCHLOROBENZIDINE
3-NITROANILINE
4,6-DINITRO-2-METHYLPHENOL
4-BROMOPHENYL-PHENYLETHER
4-CHLORO-3-METHYLPHENOL
4-CHLOROANILINE
4-CHLOROPHENYL-PHENYLETHER
4-METHYLPHENOL
4-NITROANILINE
4-NITROPHENOL
ACENAPHTHENE
ACENAPHTHYLENE
ANTHRACENE
BENZO(A)ANTHRACENE
BENZO(A)PYRENE
BENZO(B)FLUORANTHENE
BENZO(G,H,l)PERYLENE
BENZO(K)FLUORANTHENE
BIS(2-CHLOROETHOXY)Mb I HANE
BIS(2-CHLOROETHYL)ETHER
BIS(2-CHLOROISOPROPYL)ETHER
BIS(2-ETHYLHEXYL)PHTHALATE
BUTYLBENZYLPHTHALATE
CARBAZOLE
CHRYSENE
DI-N-BUTYLPHTHALATE
DI-N-OCTYLPHTHALATE
DIBENZ{A,H)ANTHRACENE
DIBENZOFURAN
DIETHYLPHTHALATE
DIMETHYLPHTHALATE
FLUORANTHENE
FLUORENE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROCYCLOPENTADIENE
HEXACHLOROETHANE
INDENO(1,2,3-CD)PYRENE
ISOPHORONE
N-NITROSO-DI-N-PROPYLAMINE
N-NITROSODIPHENYIAMINE
NAPHTHALENE
NITROBENZENE
PENTACHLOROPHENOL
PHENANTHRENE
PHENOL
PYRENE
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ID: BACKGROUND 1SFT. TEST AREA
Test Parameter
UNIFIED SOIL CLASSIFICATION
PERCHLORATE
HMX
NITROGLYCERIN
Result
u
u
u
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
Units
ug/g
ug/g
ug/g
63
147
133
90
90
90
1400
190
63
63
110
73
77
50
120
333
80
800
63
100
60
140
133
120
80
63
117
63
260
83
167
137
160
177
190
190
83
83
333
83
83
83
83
100
63
53
73
63
63
30
200
53
123
73
400
63
53
47
120
180
50
63
Oet.
Limit
4
0.5
0.5
333
333
333
333
333
333
1670
333
333
333
333
333
333
1670
333
667
1670
1670
333
667
667
333
333
1670
1670
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
1670
333
333
333
Lab ID:
Rep.
Limit
20
0.5
0.5
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846.8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-S46,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW^846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 , SW-846, 8270
1 SW-846,8270
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
- JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
LS74-5 Collect Date:
Oil.
Facior Method
ASTM 02488-84
25 SOP 302
'! SOP 420
'! SOP 420
09/26/96 18:31
09/26^6 18:31
09/26/96 18:31
09/26^6 18:31
09/26/96 18:31
09/26/9618:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26^6 18:31
09/26/96 18:31
09/26«6 18:31
09/26/96 18:31
09/26/96 18:31
09/26/9618:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26^6 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26«6 18:31
09/26/96 18:31
09/26/96 18:31
09/26^618.31
09/26/96 18:31
09/26/96 18:31
09/26/96 18.31
09/26/96 18:31
09/26/96 18:31
09/26/9618:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/26/96 18:31
09/19/9615.00
Analyst Test Date
MTB
CRS
KMS
KMS
10/21/96 09:00
10/15/96 18:28
10/11/96 11:30
10/11/96 11:30
Page 15 of 19
m
63O20-6
71-55-6
79-34-5
79-005
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
96-12-8
106-93-4
95-501
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
590207
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-907
75-003
67-66-3
74-87-3
156-59-4
10061-01-5
124-48-1
74-95-3
75-71-8
100-41-4
87-68-3
98-82-8
108-38-3
75-09-2
104-51-8
CYANIDE
PH
SULFATE
ICP/GFAA METALS DIGESTION
SONICATION EXTRACTION
ANTIMONY
BERYLLIUM
BORON
CADMIUM
CHROMIUM
COPPER
LEAD
MANGANESE
NICKEL
SILVER
ZINC
ARSENIC
MERCURY
THALLIUM
SELENIUM
1,1,1,2-TETRACHLOROETHANE
1,1,1-TRICHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
1,1,2-TRICHLOROETHANE
1,1-DICHLOROETHANE
1.1-DICHLOROETHENE
1,1-DICHLOROPROPENE
1,2,3-TRICHLOROBENZENE
1.2,3-TRICHLOROPROPANE
1.2,4-TRICHLOROBENZENE
1,2,4-TRlMb T HYLBENZENE
1 ,2-DIBROMO-3<:HLOROPROPAN
1,2-DIBROMOETHANE
1,2-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,2-DICHLOROPROPANE
1,3,5-TRIMETHYLBENZENE
1.3-DICHLOROBENZENE
1,3-DICHLOROPROPANE
1,4-DICHLOROBENZENE
2,2-DICHLOROPROPANE
2-BUTANONE
2-CHLOROTOLUENE
2-HEXANONE
4-CHLOROTOLUENE
4-ISOPROPYLTOLUENE
4-METHYL-2-PENTANONE
ACETONE
BENZENE
BROMOBEN7FNE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
CARBON IhlHACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
ClS-1,2-DICHLOROETHENE
CIS-1,3-DICHLOROPROPENE
DIBROMOCHLOROMb 1 hIANE
DIBROMOMETHANE
DICHLORODIFLUOROMETHANE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
M,P-XYLENE
METHYLENE CHLORIDE
N-BUTYLBENZENE
0.182
8.2
19
4.6
2.2
27
0.5
15
10
U
135
8.4
0.6
58
6.2
0.04
1.2
1.9
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
5.6 JB ugAg
U
U
U
U
U
U
U
U
U
U
ug/kg
ugAg
ugAg
ug/kg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
4.5 JB ug/kg
U ugAg
0.15
0.8
3
0.1
0.4
0.1
0.3
0.1
1.5
Ol
0.6
0.2
0.2
0.8
0.01
0.6
1.2
0.2
0.2
0.3
0.2
Ol
0.6
0.2
0.2
0.2
0.2
0.2
0.2
0.2
01
0.2
0.2
0.2
0.2
0.2
0.2
0.2
10
0.2
10
0.2
0.2
10
10
0.2
0.2
0.2
0.3
Ol
0.4
0.3
0.2
0.4
0.4
0.6
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
0.2
0.3
0.2
0.75
4
15
0.6
1.8
0.6
1.5
0.6
7.5
0.6
3
0.9
1.2
2.4
0.04
1.9
4.1
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
1 sw 846,9012 KEN 10/03/96 13:00
1 sw 846,9045 MTB 10/08/9613:00
2!i sw 846,9056 CRS 10/17/96 16:19
SW-S46,3050 KWB 10/18/96 00:00
SW-846,3550 SDM 09/25/96 00.00
1 SW-846,6010 KWB 10/23/96 14:02
1 SW-846,6010 KWB 10/23/96 14:02
1 SW-846,6010 KWB 10/23/9614.02
1 SW-S46,6010 KWB 10/23/9614:02
1 SW-846,6010 KWB 10/23/9614:02
1 SW-846,6010 KWB 10/23/96 14:02
1 SW-846,6010 KWB 10/23/96 14:02
1 SW-846,6010 KWB 10/23/9614:02
1 SW-846,6010 KWB 10/23/96 14:02
1 SW-846,6010 KWB 10/23/9614:02
1 SW-846,6010 KWB 10/23/96 14:02
1 SW-846,7060 CRS 10/23/96 17:43
1 SW-846,7471A CRS 10/17/96 13:40
1 SW-846,7481 CRS 10/24/96 11:41
1 SW-846,7740 CRS 10/23/96 14:54
1 SW-846,8260 MMR 10/02/96 13:42
1 SW-S46,8260 MUIR 10/02/96 13:42
1 SW-846,8260 MMR 10/02/9613:42
1 SW-846,8260 MUIR 10/02/96 13:42
1 SW-846,8260 MUIR 10/02/96 13:42
1 SW-S46,8260 MUIR 10/02/9613:42
1 SW-846,8260 MMR 10/02/9613.42
1 SW-846,8260 MMR 10/02/9613.42
1 SW-846,8260 MUIR 10/02/96 13:42
1 SW-846,8260 MUIR 10/02/96 13:42
1 SW-846,8260 MUIR 10/02/9613:42
1 SW-846,8260 M^R 10/02/96 13:42
1 SW-846,8260 MMR 10/02/96 13:42
1 SW-846,8260 MMR 10/02/96 13:42
1 SW-846,8260 MUIR 10/02/9613:42
1 SW-846,8260 MMR 10/02/96 13:42
1 SW-846,8260 MMR 10/02/96 13:42
1 SW-S46,8260 MUIR 10/02/96 13:42
1 SW-846,8260 MMR 10/02/96 13:42
1 SW-846,8260 MMR 10/02/96 13:42
1 SyV-846,8260 MMR 10/02/96 13:42
1 SW-846,8260 MMR 10/02/96 13:42
1 SW-846,8260 MMR 10/02/9613:42
1 SW-846,8260 MMR 10/02/9613:42
1 SW-846,8260 M^R 10/02/9613:42
1 SW-846,8260 MMR 10/02/96 13.42
1 SW-846, 8260 MUIR 10/02/96 13:42
1 SW-846,8260 MMR 10/02/96 13:42
1 SW-S46,8260 MMR 10/02/9613:42
1 SW-846,8260 MUIR 10/02/96 13:42
1 SW-846,8260 MMR 10/02796 13:42
1 SW-846,8260 MUIR 10/02/96 13:42
1 SW-846,8260 MMR 10/02/96 13:42
1 SW-846,8260 MMR 10/02/96 13:42
1 SW-846,8260 MUIR 10/02/96 13:42
1 SW-846,8260 MMR 10/02/96 13:42
1 SW-846,8260 MUIR 10/02/96 13:42
1 SW-846,8260 MMR 10/02/9613:42
1 SW-846,8260 MMR 10/02/96 13:42
1 SW-846,8260 MMR 10/02/96 13:42
1 SW-846,8260 M^R 10/02/9613:42
1 SW-846,8260 MAR 10/02/96 13:42
1 SW-846,8260 MMR 10/02/96 13:42
1 SW-846,8260 MMR 10/02/96 13:42
1 SW-846,8260 MMR 10/02/9613:42
1 SW-846,8260 MAR 10/02/9613:42
1 SW-846,8260 MUIR 10/02/9613:42
1 SW-846,8260 MMR 10/02/96 13:42
1 SW-846,8260 MUIR 10/02/96 13:42
1 SW-846,8260 MUIR 10/02/96 13:42
Page 16 of 19
•
103-65-1
91-203
95-47-6
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-605
10061-02-6
79-01-6
75-69-4
75-01-4
120-82-1
95-50-1
541-73-1
106-46-7
95-95-4
88-06-2
12083-2
105-67-9
51-28-5
121-14-2
606-202
91-58-7
95-57-8
91-57-6
95-48-7
88-74-4
88-75-5
56-55J
99-09-2
534-52-1
101-55-3
59-507
106-47-8
7005-72-3
106-44-5
100-01-06
100-02-7
83-32-9
208-96-8
12012-7
56-55-3
5032-8
205-99-2
191-24-2
207-08-9
111-91-1
111-44-4
108-601
117-81-7
85-68-7
12012-7
21801-9
84-74-2
117-84-0
53-703
132-64-9
84-66-2
131-11-3
206-44^
86-73-7
118-74-1
87-68-3
77-47-4
67-72-1
193-39-5
78-59-1
621-64-7
N-PROPYLBENZENE
NAPHTHALENE
O-XYLENE
SEC-BUTYLBENZENE
STYRENE
TERT-BUTYLBENZENE
TETRACHLOROETHENE
TOLUENE
TRANS-1,2-DICHLOROETHENE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
VINYL CHLORIDE
1,2,4-TRICHLOROBENZENE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DICHLOROPHENOL
2,4-DIMETHYLPHENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
2-METHYLNAPHTHALENE
2-METHYLPHENOL
2-NlTROANILINE
2-NITROPHENOL
3,3'-DICHLOROBENZIDINE
3-NITROANlLINE
4,6-DINITRO-2-METHYLPHENOL
4-BROMOPHENYL-PHENYLETHER
4-CHLORO-3-METHYLPHENOL
4-CHLOROANILINE
4-CHLOROPHENYL-PHENYLETHER
4-METHYLPHENOL
4-NITROANlLINE
4-NITROPHENOL
ACENAPHTHENE
ACENAPHTHYLENE
ANTHRACENE
BENZO(A)ANTHRACENE
BENZO(A)PYRENE
BENZO(B)FLUORANTHENE
BENZO(G,H,0PERYLENE
BENZO(K)FLUORANTHENE
BIS(2-CHLOROETHOXY)METHANE
BIS(2-CHLOROETHYL)ETHER
BIS(2-CHLOROISOPROPYL)ETHER
BIS(2-ETHYLHEXYL)PHTHALATE
BUTYLBENZYLPHTHALATE
CARBAZOLE
CHRYSENE
DI-N-BUTYLPHTHALATE
DI-N-OCTYLPHTHALATE
DIBENZ(A,H)ANTHRACENE
DIBENZOFURAN
DIETHYLPHTHALATE
DIMETHYLPHTHALATE
FLUORANTHENE
FLUORENE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROCYCLOPENTADIENE
HEXACHLOROETHANE
INDENO(1,2,3-CD)PYRENE
ISOPHORONE
N-NITROSO-DI-N-PROPYLAMINE
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ug/kg
ug/kg
ugAg
0.2
02
0.2
0.2
0.2
0.2
0.9
0.3
0.2
0.2
0.3
0.3
0.4
63
63
63
147
133
90
90
90
1400
190
63
63
110
73
77
SO
120
333
80
800
63
100
60
140
133
120
80
63
117
63
260
83
167
137
160
177
190
190
83
83
333
83
83
83
83
100
63
53
73
63
63
30
200
53
123
73
400
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
333 1
333 1
333 1
333 1
333 1
333
333
333
1670
333
333
333
333
333
333
1670
333
667
1670
1670
333
667
667
333
333
1670
1670
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
SW-846,8260
SW-846,8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-846, 8260
SW-S46, 8260
SW.846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846,8270
SW-846, 8270
SW-846, 8270
SW-S46, 8270
SW-S46, 8270
SW-846, 8270
SW-846, 8270
SW-S46, 6270
SW-846, 8270
SW-S46, 8270
SW-846, 8270
SW-846, 8270
SW-S46, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
1 SW-846,8270
1 SW-846,8270
SW-846, 8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846.8270
1 SW-S46,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-846,8270
1 SW-S46,8270
1 SW-846,8270
MUIR
MAR
MUIR
MMR
MMR
MMR
Ml^R
MUIR
MMR
MMR
MUIR
MMR
MMR
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMPi
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
10/02/96 13:42
10/02/96 13:42
10/02/96 13:42
10/02/96 13:42
10rt)2«6 13:42
10/02^613:42
10/02«6 13:42
10/02^6 13:42
10/02/96 13:42
10/02«6 13:42
10/02^6 13:42
10/02/9613:42
10/02^6 13:42
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26^6 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26^6 19:16
09/26/96 19:16
osaeme i9:i6
09/26/96 19:16
09/26/96 19:16
09/26«6 19:16
09/26/96 19:16
09/26/96 19:16
09/26«6 19:16
09/26/96 19:16
09/26/96 19:16
09/26«6 19:16
09/26/96 19:16
09/26^6 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26^6 19:16
09/26«6 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26«6 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09/26/96 19:16
09126196 19:16
09/26/9619:16
Page 17 of 19
•
86-30-6
91-203
98-95-3
87-86-5
85-01-8
108-95-2
129-00-0
N-NITROSODIPHENYLAMINE
NAPHTHALENE
NITROBENZENE
PENTACHLOROPHENOL
PHENANTHRENE
PHENOL
PYRENE
u
u
u
u
U
U
U
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
ugAg
63
53
47
120
180
50
63
333
333
333
1670
333
333
333
SW-646, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-846, 8270
SW-646, 8270
JMA
JMA
JMA
JMA
JMA
JMA
JMA
09/26/96 19:16
09/26S6 19:16
09/26/96 19:16
09/2656 19:16
09/26/96 19:16
09/26«6 19:16
09/26^6 19:16
Page 18 of 19
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected, or the compound was detected
but was below the detection limit.
B This flag is used when an aiialyte is found in the blank as well as the sample
Det. Limit Method Detection Limit (approximately three times the signal noise level)
Rep. Limit Reporting Limit is nonnally the value ofthe lowest standard run with the
analysis. The value is approximately 5 to 10 times the Method Detection Limit.
Dil. Factor Dilution Factor- The prepared sample was diluted by this factor because the
sample was too concentrated or due to other interferences in the sample matrix.
Any dilution factor causes an appropriate increase in the method detection limit
and reporting limit.
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This
flag is used either when estimating a concentration for teritatively identified compounds or
when the data indicated the presence of a compound that meets the identification criteria
but the result is less than the specified reporting limit (e.g. 3 J with a reporting limit of 10)
Page 19 of 19