DSHW-1996-002474 - 0901a0688013e4f7

HAND DELIVERED
DIVISION OF SOLID &
HAZARDOUS WASTE
AM P^
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THIOKOL CORPORATION I %Wl>ir>b
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SEMI-ANNUAL RFI PROGRESS REPORT
1 SEPTEMBER 1995 - 1 Miarch 1996
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m SEMI-ANNUAL RFI PROGRESS REPORT
1 SEPTEMBER 1995 - 1 MARCH 1!J96
1. Description and estimation of the percentage of the RCRA Facility Investigation
completed;
To date, soils at the following SWMUs have been sampled:
M-19A Photographic Processing Discharge, SWMU 553;
E-517-W Surface Discharge, SWMU 282;
M-576-N Surface Discharge, SWMU 271;
M-514 Surface Discharge, SWMU 618;
S-501 Surface Discharge, SWMU 266;
M-640 Surface Discharge, SWMU 381;
M-641 Surface Discharge, SWMU 264;
M-585-N Surface Discharge, SWMU 273;
M-606 Surface Discharge, SWMU 527;
M-628 Surface Discharge, SWMU 528;
M-593 Surface Discharge, SWMU 274;
M-636-SW Surface Discharge, SWMU 367;
M-570 Surface Discharge, SWMU 285;
M-197 Surface Discharge, SWMU 483;
M-197-BP Surface Discharge, SWMU 360;
M-702 Surface Discharge, SWMU 620;
A-9 Surface Discharge, SWMU 267;
A-2 Surface Discharge, SWMU 560;
M-66 Surface Discharge, SWMU 432;
M-72 Surface Discharge, SWMU 263;
M-67 Surface Discharge, SWMUs 261 and 433;
M-14N and M-14S Surface Discharges, SWMUs 257 and 270;
M-53-BP Surface Discharge, SWMU 260;
M-53-E Surface Discharge, SWMU 259;
M-33-B and M-33-C Surface Discharges, SWMDs 258 and 413;
M-39 Surface Discharge, SWMU 425;
Combined Surface Discharge for M-8, M-9, M-10, M-52, and M-179-N,
SWMUs 268, 611, 269, 409, 472, and 255;
M-57 Surface Discharge, SWMU 615;
M-55-W Surface Discharge, SWMU 621;
M-9 Strand Burner Exhaust Discharge, SWMU 652;
M-40 Surface Discharge, SWMU 642;
M-205 Surface Discharge, SWMU 286;
T-21-D Surface Discharge, SWMU 559;
T-6-A Surface Discharge, SWMU 287;
Old Drum Storage Area East of M 203, SWl^^IU 203;
M-114 Surface Discharge, SWMU 426;
M-227 Hydrofluoric Acid Treatment Unit, S>VT^U 192;
•
M-9-NE Surface Discharge, SWMU 651;
M-186 Industrial Waste Landflll, SWMU 212;
M-136 Old Waste Oil Disposal Pit, SWMU 208;
M-187 Old Drum Storage Area, SWMU 551;
T-l Photographic Processing Drainfleld, SWA'IU 648;
A-2 Photographic Processing Drainfleld, SWMU 191;
I-IO-NE Subsurface Discharge, SWMU 645;
I-IO-SE Subsurface Discharge, SWMU 436;
I-IO-S Subsurface Discharge, SWMU 234;
T-111 Subsurface Discharge, SWMU 355;
T-24A Surface Discharge, SWMU 401;
M-2 Laundry Drainfleld C, SWMU 627;
M-19A Drywell, SWMU 444;
M-39 Subsurface Discharge, SWMU 425;
T-51A Surface Discharge, SWMU 402;
M-2 Laundry Drainfleld B, SWMU 626;
M-19A Strand Burner Exhaust Discharge, SVV^IU 650;
M-585 Strand Burner Exhaust Discharge, S\^^[U 649;
Historic Burning Ground NE of M-243, SWMU 202;
M-2 Laundry Drainfleld A, SWMU 465;
Old Burning Grounds at M-136, SWMU 243;^ n d '^< AA [ '^U
M-193-S Septic Drainfleld, SWMU 638;'^ :>cf ^ '^ " '^^''•-"^ '' ^^
M-193-N Septic Drainfleld, SWMU 632;*^
M-191 Septic Drainfield, SWMU 631;-^
M-338 Subsurface Discharge, SWMU 608;i^
Domestic Wastewater Drainfields A, B and C, SWMU 625 ;i—
M-348 Subsurface Discharge, SWMU 395; ^
M-72 Septic Drainfield, SWMU 630;-^
M-71 Septic Drainfield, SWMU 646; ^
M-19A Septic Drainfield, SWMU 628; ^^
Removed Sump at M-622, SWMU 316;»-V
M-117 Subsurface Discharge, SWMU 254; and
T-14A Subsurface Discharge, SWMU 493.t---
These sites represent approximately 83 percent of the SWMUs in Phase I of the
RFI.
The final closure report including Certification of Closure for the following sites
is expected to be submitted concurrently >vith this progress report:
M-39 Photographic Waste Discharge Site, SWl^lU 290;
M-114 Photographic Waste Discharge Site, SWMUs 23 and 426; and
M-636 Photographic Waste Discharge Site, SWMU 24
M-508 Photographic Waste Discharge Site, SWMUs 20 and 423
9
2. Summaries of all findings;
The raw analytical data for the reporting period is included with this report.
This data will be compared to standards considered to be protective of health
and the environment as outlined in Section 8.0 of the Data Collection Quality
Assurance Plan. Volume Two, Thiokol RCRA Facility Investigation Work Plans.
3. Summaries of all changes made in the RCRA Facility Investigation during the
reporting period;
There were no changes made to the approved Work plans of the RFI. Work
plans for three newly identified sites are included with this report for the
Division's review and approval.
4. Summaries of all contact with representatives of the local community, public
interest groups or State Government during the reporting period;
Correspondence regarding RFI activities has been limited to the Division of
Solid and Hazardous Waste and the Division of Wateir Quality.
5. Summaries of all problems or potential problems encountered during the
reporting period;
While conducting preparations to sample the site designated as Old Buming
Grounds West of M-174, SWMU No. 195, personnel having knowledge of historic
operations of that area indicated that the actual burn ground was not in the
area shown on the work plan map. Instead, the bumi area appears to have
been located just north of M-47. The two buildings are located reasonably close
to one another and access to both is by the same road. A non-hazardous debris
disposal area has been identified in the approximate area of the alleged bum
ground. This may have contributed to the confusion regarding the location of
the burn area.
6. Actions being taken to rectify problems;
The location of the burn area is actively being researched by revievring available
documents and interviewing of former and current employiees. In the event that
the location is different from the current work plan, Thiokol will submit a
modified work plan prior to initiating sampling activities.
7. Changes in personnel during the reporting period;
There has been no change in coordination and project management for the RFI
during the reporting period. The current environmental staff will continue to
conduct the sampling when possible. Contractors vnll be used when specialized
equipment is required.
8. Projected work for the next reporting period;
Investigation activities will focus on the remaining sites having approved work
plans. Nearly all the remaining sites have some level of uncertainty associated
with them in terms of exact location, site accessability, or safety concerns.
9. Copies of daily reports, inspection reports, laboratory and monitoring data.
Copies of the daily logs and laboratory data received during the reporting
period are included with this report.
M-40 Magnesium Grinding Area
Investigation Plan
SWMU No. 655
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Thiokol Corporation
RFI Work plans, Vol. 4
20 February 1996
1.0 SAMPLING OBJECTIVE
Soil samples collected at this site during Phase I of tlie RFI will be analyzed for
verification of the presence of hazardous waste or hazardous waste constituents indicating
a release from the SWMU.
2.0 SITE LOCATION
Son samples will be taken from the soil adjacent to the concrete pad on the east side of
building M-40.
3.0 BACKGROUND INFORMATION
Magnesium fines escaping from the cyclones accumulated on a concrete pad on the east
side of the building. The accumulation of fines created a safety hazard. Historically,
buildiag operators would periodically sweep the dust and fines from the pad onto the
surface of the soil east of the building. This investigation plan has been prepared as a part
of Thiokol's RFI to verify the nature and extent of any contamination due to this practice.
4.0 SAMPLING RATIONALE
The constituent of concem for this site is magnesium- The magnesium fmes are suspected
of being potentially reactive when finely ground. There are no other known or suspected
constituents for this site.
5.0 SAMPLING STRATEGY
The area of concem for this site is very small. Two locations will be chosen with surface
and 2 foot samples collected at each location.
6.0 BACKGROUND
Extensive soil sampling of the Thiokol faciUty has established a data base for naturally
occurring inorganic constituents. This data base consists of background samples used in
the closure of various RCRA facilities at Thiokol. Additional background samples will
be collected throughout the RFI. The analytical results of iiie backgroimd samples taken
during Phase I sampling will be added to this data base to provide site specific data.
Analytical data obtained from investigation activities at thij; site will be compared to this
data base for determination of contamination above background and/or health based risk
levels.
Thiokol Corporation
RFI Work plans, Vol. 4
20 February 1996
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7.0 SAMPLING EQUIPMENT
1. Stainless steel hand auger, scoop and/or spatula
2. Certified clean sample bottles
3. Distilled water
4. Tape measure
5. Alconox soap wash
6. Tap water
7. Wash bucket
8. Cleaning brush
9. Rubber gloves
10. Lab labels and custody seals
11. Cooler and ice
8.0 SAMPLING TECHNIQUE
NOTE: For personal safety and to prevent cross contamination, use new rubber gloves
at each sample point when handling samples and sampling equipment.
Procedure for Using Stainless Steel Hand Auger
1. Clean soU auger in a 5 gallon bucket containing soapy water, rinse auger with tap
water, and then final rinse with distilled (deionized) waiter. The soapy water and tap
water shall be replaced after each use to assure good cleaning and to minimize
cross-contamination.
2. Clear any trash and debris away from sampUng points to preclude entry into sample.
3. Using auger and tape measure, obtain the desired depth.
4. Once desired depth is obtained, remove auger and any loose sods.
5. Using a cleaned stainless steel spatula, remove a poition of soU from the bottom of
the auger.
6. FiU a sample container with soU from the auger.
7. Clean spatula between each sampling point. Wash with detergent water, foUowed
by a distilled water rinse.
NOTE: Containerize all wash jmd rinse water for hazardous waste analysis to
determine final disposition.
8. The samples wiU be identified as foUows with the depth noted after each assigned
Thiokol Corporation
RFI Work plans, Vol. 4
20 February 1996
sample number:
•
• For example, the sample taken at the surface from buUding M-40 would be
labeled as SWMU 655, surface.
9. Repeat above steps for each sample.
9.0 SAMPLE DOCUMENTATION
The foUowing information must be recorded in the Field Book:
Date and time of sampling
Sampler's name and signature
Location of samples including depth
Type, number, sample number, and seals used on sample bottles
Weather
Texture and color of samples
Any other pertinent information
10.0 ANALYTICAL PARAMETERS
The soil samples wUl be analyzed by a State certified lab on for the foUowing
constituents:
PARAMETER MEITIOD
Magnesium 6010
11.0 SAMPLE ACCOUNTABILITY AND CUSTODY
Follow procedures specified in the Waste Analysis Plan, Appendix 02.D of Thiokol
Corporation Hazardous Waste Permit Application. November 1991. These procedures are
also contained in the Data CoUection QuaUty Assurance PLm in Volume Two of the RFI
Work plans. Requirements for sample custody and custody seals are discussed in these
documents.
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M-15A Drywell
Investigation Plan
SWMU No. 662
•
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Thiokol Corporation
RFI Work Plans, Vol. 4
20 February 1996
1.0 SAMPLING OBJECTIVE
SoU samples coUected at this site during Phase I of the RI^ wiU be analyzed for
verification of the presence of hazardous waste or hazardous waste constituents
indicating a release from the SWMU.
2.0 SITE LOCATION
Samples wiU be taken from an abandoned dryweU adjaccEit to buUding M-15A. See
Figure 662-1 for site location.
3.0 BACKGROUND INFORMATION
This unit consists of an abandoned dry weU which forme;rly received waste flows from
the compressor buUding designated as M-l5A. There is no visible evidence at the
ground surface of the location of the dryweU; therefore, it wUl be necessary to conduct
some initial site reconnaissance to define the area for soU sampling activities.
4.0 SAMPLING RATIONALE
The contaminant deposition expected at this clryweU is a smaU, shaUow, localized area
with contamination primarUy on the surface. The dryweU is expected to be a covered
bottomless structure with only the discharge itself as the hiydrauUc driver for vertical
movement. The constituents of concem for this site are metals and volatUe organics.
5.0 SAMPLING STRATEGY
The dryweU wUl be investigated by obtaining a sample from the material in the bottom
and at a depth of 2 feet below the first sampling point using a stainless steel hand
auger.
DupUcate and QA/QC samples wiU be coUected according to the frequencies outlined
in Section 3.2 of the RFI Phase I Data CoUection QuaUty Assurance Plan. The
foUowing chart summarizes the recommended frequency for these samples.
SAMPLE TYPE PROPOSED FREQUENCY
DupUcate 5% or 1 per site, which ever is greater
Rinse Field Blanks 5% or 1 per site, which ever is greater
Spikes 1 % of the totail RFI samples
ABANDONED
2'0 SUMP
ADAMnr\Mrn HDAIM nn n
MUAAINUVi'lNLL/ UIXnilN I ILLL/
Thiokol Corporation
RFI Work Plans, Vol. 4
20 February 1996
6.0 BACKGROUND
Background samples have been coUected in areas known or beUeved to be free of
contamination within the Manufacturing and Administraticin Area. These background
samples were coUected at corresponding depths to obtain s;amples in similar strata to
those taken in the area of concem.
Extensive soil sampling of the Thiokol faciUty has establisihed a data base for naturaUy
occurring inorganic constituents. This data base consists of backgroimd samples used
in the closure of various RCRA faciUties at Thiokol. Tlie analytical results of the
background samples taken during Phase I sampling wiU be added to this data base to
provide site specific data. Analytical data obtained from investigation activities at this
site wUl be compared to this data base for determination of contamination above
background levels.
7.0 SAMPLING EQUIPMENT
#
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
Stainless steel soU auger
Field book
Certified clean sample bottles
DistUled water
Measuring tape
Alconox soap wash
Tap water
Wash buckets
Cleaning brush
Rubber gloves
T ,ab labels and seals
Cooler and ice
Stainless steel spatula
Shovel
8.0 SAMPLING TECHNIQUE
NOTE: For personal safety and to prevent cross contamination, use new rubber gloves
at each sample point when handling samples <ind sampUng equipment.
8.1 Procedure for Using Stainless Steel Hand Auger
1. Clean soil auger in a 5 gaUon bucket containing soapy water, rinse auger with
tap water, and then final rinse with distilled (deionized) water. The soapy water
and tap water shaU be replaced after each use to assure good cleaning and
#
Thiokol Corporation
RFI Work Plans, Vol. 4
20 February 1996
minimize cross-contamination.
2. Clear any trash and debris away from sampling points to preclude entry into
sample.
3. Using auger and tape measure, obtain the desired depth.
4. Once desired depth is obtained, remove auger and imy loose soUs.
5. Using a cleaned stainless steel spatula, remove a portion of soU from the
bottom of the auger.
6. FUl a sample container with soil from the auger.
7. Clean spatula between each sampling point. Wa:sh with detergent water,
foUowed by a distUled water rinse.
NOTE: Containerize aU wash and rinse waiter for future analysis for
hazardous constituents.
8. The samples wiU be identified as foUows with the depth noted after each
assigned sample number:
• The sample taken from boring #1 at the 2 foot level would be labeled as
SWMU 662, #1 @ 2'.
9. Repeat above steps for each sample.
9.0 SAMPLE DOCUMENTATION
The foUowing information must be recorded m the Field B^ook:
Date and time of sampling
Sampler's name and signature
Location of samples including depth
Type, number, sample number, and seals used on simiple bottles
Weather
Texture and color of samples
Any other pertinent information
Thiokol Corporation
RFI Work Plans, Vol. 4
20 February 1996
10.0 ANALYTICAL PARAMETERS
The soil samples wiU be analyzed by a State certified lab on for the foUowing
constituents:
PARAMETER METHOD
RCRA Metals (Panel) 6010
VolatUe Organics 8260
11.0 SAMPLE ACCOUNTABILITY AND CUSTODY
FoUow procedures specified in the Waste Analysis Plan, Appendix 02.D of Thiokol
Corporation Hazardous Waste Permit Application. November 1991. These procedures
are also contained in the Data CoUection Quality Assurance Plan in Volume Two of
the RFI Work Plans. Requirements for sample custody amd custody seals are discussed
in these documents.
^
Septic Drainfields Receiving Industrial Wastewater
investigation Plan
SWMU Nos. 663 and 664
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Thiokol Corporation
RFI Work Plans, Vol. 4
20 Febniary 1996
1.0 SAMPLING OBJECTIVE
Samples collected at these sites during Phase I of the RFI wUl be analyzed for
verification of the presence of hazardous waste or hazardous waste constituents
indicating a release from the SWMUs.
2.0 SITE LOCATION
Samples wUl be taken from the individual buUding drainfields. Refer to FaciUty
Engineering Drawings for additional detaU of each site.
Buildings discharging industrial wastewater to septic systems which are to be sampled
under this plan, and the corresponding soUd v/aste management unit numbers are as
follows:
BtlLDING
M-15A
T-10
-SWMU^NO..'.^ii^-v^
663
664
3.0 BACKGROUND INFORMATION
These sites are septic drainfields which have received industrial wastewater flows
having constituents potentiaUy exceeding relevant regulatory, health and risk based
standards.
4.0 SAMPLING RATIONALE
The constituents of concem for these sites are those which in previous wastewater
sampling have exceeded relevant regulatory, health and risk based standards. These
constituents are listed for the respective buUdings in Section 10.0 of this plan. Phase I
sampling will focus on verification of these constituents in the soU.
The constituents of concem for the septic systems covered by this plan were chosen
after a review of existing sampling data. The discharges have been sampled previously
for parameters regulated by the Utah Water Quality Act.
5.0 SAMPLING STRATEGY
m These sites are considered small locaUzed areas with the source of contamination at
some depth in the soil profile. A stratified random design wUl be implemented for
Phase I sampling at each site. The drainfield sites wUl be divided into grids consisting
of squares each 5 ft by 5 ft. The intersection of the grids wiU be numbered and
ABANDONED
2'0 SUMP
APAMnnMcn HDAIM nn n
r^Ljr^i-iLj\.ji-n_iy Lji\rMi-t i iL_L.Ly
BLDG. M-15 ^v^
85^-1
0 BLDG. 1-10
Thiokol Corporation
RFI Work Plans, Vol. 4
20 February 1996
sample locations chosen using a Random Numbers Table or a random number
generator. Four locations wiU be chosen wiUi samples taken from the 5 and 10 foot
depths at each location. The actual location of the sample; sites will not be chosen
untU the day of sampling.
Samples from each septic tank were previously coUected <md analyzed, the results of
which were used in identifying constituents of concem foi: the drainfields. No
additional samples wUl be coUected from the septic tanJlcs.
SWMU Nos. 663 and 664 wiU be grouped together as on(5 site for determining the
number of dupUcate and QA/QC samples. The foUowmg chart summarizes the
recommended frequency for these samples.
SAMPLE TYPE PROPOSED FREOUENCY
Duplicate 5% or 1 per site, which ever is greater
Rinse Field Blanks 5 % or 1 per site, which ever is greater
Spikes 1 % of the total RFI samples
6.0 BACKGROUND
Background samples have been coUected in areas known or beUeved to be free of
contamination within the Manufacturing and Administration Area for use in comparing
concentrations. These background samples were coUected at corresponding depths to
obtain samples in similar strata to those taken in the areas of concem.
Extensive soU sampling of the Thiokol faciUty has establi£;hed a data base for naturaUy
occurring inorganic constituents. This data base consists of background samples used
in the closure of various RCRA facUities at Thiokol. The analytical results of the
backgroimd samples taken during Phase I sampling wUl b(; added to this data base to
provide site specific data. Analytical data obtained from investigation activities at this
site wiU be compared to this data base for determination of contamination above
background levels.
7.0 SAMPLING EQUIPMENT
1. New split-spoon sampler
2. Field book
3. Certified clean sample bottles
4. DistUled water
5. Tape measure
6. Alconox soap wash
7. Tap water
8. Steam cleaner or wash buckets
Thiokol Corporation
RFI Work Plans, Voi. 4
20 February 1996
JH
9. Cleaning brush
10. Rubber gloves
11. Lab labels and seals
12. Cooler and ice
13. Stainless steel spatula
14. Shovel
15. Steam cleaned auger rig and tooUng
8.0 SAMPLING TECHNIQUE
NOTE: For personal safety and to prevent cross contamination, use new rubber gloves
at each sample point when handling samples and sampUng equipment.
1. Using a cleaned spUt-spoon and auger rig, retrieve a continuous soU sample
down to the prescribed depth. Samples wiU be collected at 5 and 10 foot
depths and placed into sample bottles. This wiU be accomplished as foUows:
A) CarefuUy spUt open spoon
B) Measure core to find the required sample depths
C) Using cleaned stainless steel spatula, remove a portion of soil at the
required depth to fiU the sample bottle(s).
D) Seal sample bottle Ud with seal, note sample: location and depth on
sample bottle label, and place in cooler containing ice.
E) Note soU Uthology in log book
F) Scrape the remaining soil out of spoon and leave in same area as sample
point.
2. After sample has been taken at the depliis noted above, decontaminate the spUt
spoon, spatula, and any associated equipment as foUows.
A) Steam clean with Alconox soap or scrub witb brush in wash basin or
bucket containing Alconox soap and water.
B) Rinse with tap water (Do not reuse tap water)
C) Give final rinse with deionized water
NOTE: Containerize all wash and rinse wat(jr for hazardous waste
analysis to detemiine proper disposition.
3. The samples wUl be identified as foUows with the depth noted after each
#
Thiokol Corporation
RFI Work Plans, Voi. 4
20 February 1996
assigned sample humber:
• The sample taken from grid #12 at the 5 foot level would be labeled as
SWMU 663, #12 @ 5'.
9.0 SAMPLE DOCUMENTATION
The foUowing information must be recorded in the Field Book:
Date and time of sampUng
Sampler's name and signature
Location of samples including depth
Type, number, sample number, and seals used on sample bottles
Weather
Texture and color of samples
Any other pertinent information
10.0 ANALYTICAL PARAMETERS
The soU samples wUl be analyzed by a State certified lab on for the foUowing constituents:
BUILDING
M-15A
MO
SWMU NO:
663
664
PARAMETERS
RCRA Metals (Panel)
VolatUe Organics
RCRA Metals (Panel)
Volatile Orpanif^'^
SW-846 MFTHODS
(UNLESS
OTHERWISE
INDICATED)
6010
8260
6010
87,60
11.0 SAMPLE ACCOUNTABILITY AND CUSTODY
Follow procedures specified in the Waste Analysis Plan,, Appendix 02.D of Thiokol Corporation
Hazardous Waste Permit Application. November 1991. Tiiese procedures are also contained in
the Data Collection Quality Assurance Plan m Volume Two of the RFI Work plans.
Requirements for sample custody and custody seals are disicussed in these documents.
125
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Thiokol Corporation RCRA Faciiity Investigation
W0#: 1B940 LWR*: ^//d^
STTE: Old Burning Groimds at M-136 .^
DESCRIPTION: SWMU #243; Grid # O . 2 ft
PARAMETERS
VolatUe Organics
METHOD
8240
l-jakf- 'Brau^n-
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DATE: //^9^/^'-* TIME: A^-^^ /.SAMPI.F.R=
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: £'1/04^
SfTE: Old Buming Grounds at M-136
DESCRIPTION: SWMU #243; Grid # 3 , 2 ft
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PARAMETERS
Cd, Cr, Ag, Pb
Mercury
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
DATE: // ^Af3'^ TIME: /f^/sAMPLER: /4/=^
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Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: ^f/C^O
SITE: Old Buming Grounds at M-136
DESCRIPTION: SWMU #243; Grid # ^ , S ft
PARAMETERS METHOD
Volatile Organics 8240
DATE: ll%<pt 'T^ TIME: /^5 ^ SAMPLER: /4<^^
Thiokol Corporation RCRA FacUity InvestigaUon
WO#: IB940 LWR#. ^(/Q^
SITE: Old Burning Grounds at M-136
DESCRIPTION: SWMU #243; Grid # _JS.. 5 ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb 6010
Mercury 7470
HMX HPLC
Nitroglycerin HPLC
DATE: /I^CfiM ^ TIME: /4^Xi> SAMPLER: /4A0
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Thiokol Corporation RCRA Facility InvestigaUon
WO#:1B940 LWR#: ^(10^
SITE: Old Buming Grounds at M-136 _
DESCRIPTION: SWMU #243; Grid # O^2 ft — •
PARAMETERS ^^THOD Q
VolatUe Organics ^240
DATE : f/%</:it9T TIME: /$~^0 SAMPLER: Af^
12'
JSSO-Thiokol Corporation RCRA Facility Investigation
WO#: 1B940 LWR#: £'//O^0
SITE: Old Buming Grounds at M-136
DESCRIPTION: SWMU #243; Grid # 3^—^l ft
PARAMETERS
Cd, Cr, Ag, Pb
Mercury
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
DATE: //"^Cfit^i TIME: /S~S^ SAMPLER: '^r/W
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W0#: 1B940 .LWR#: E^ 11040
SITE: Old Burning Groimds at M-136 ^
DESCRIPTION: SWMU #243; Grid # oZ-rS ft
PARAMETERS
VolatUe Organics
METHOD
8240
-^a^ e/i ft
DATE: // '>tf>r9^ TIME: /5^Z. SAMPLER: Af^^
Thiokol Corporation RCRA FacUity InvesUgation
W0#: 1B940 LWR#: S'll04{)
SITE: Old Buming Grounds at M-136
DESCRIPTION: SWMU #243; Grid # _2_2r5 ft
PARAMETERS
Cd, Cr, Ag, Pb
Mercian
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
DATE: // 5^/?r5!r^ TIME: /J^2- SAMPLER: /f/x^J
1(^00 'Burn (Sro,jL/}d^ ^/"tf: pr<^/)arm t ^
•/^ J^u CIL.
,;,iar-h.^l.ab»^
128
It ^p-h'ir .
Thiokol CorporaUon RCRA Facility Investigation
WO#: 1B940 LWR#; ^//^^.n
SITE: Old Buraing Grounds at M-136 '
DESCRIPTION: SWMU #243; Grid # SZ^, 2 ft
PARAMETERS METHOD
VolaUle Organics 8240
DATE: /Z 'iC/!r^r' TIME: 7"^^ SAMPLER: A^
Thiokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR*:
SITE: Old Buming Grounds at M-136 _
DESCRIPTION: SWI^rV #243; Grid # 6, Z^ 2 ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb 6010
Mercury 1\1^
HMX HPLC
Nitroglycerin HPLC
DATE: /Z^Y/Jfyr TIME: 7i ^ SAMPLER: -^vJ
SITE: Old Buming Grounds at M-136
DESCRIPTION: SWMU #243; Grid # S~Z.,S ft
PARAMETERS METHOD
Volatile Organics 8240
DXTE-./ZS^/^iy^ TIME: ^<? ^ SAMPLER: i^T^
V^fi/ tUrd
f V^i/cL
.-1^ ^ T^'co/Corporation RCRA Facility Investigation *T2 J^ " "7 I
(^t/C^ W0#: IB940 LWR#: 1= (iO^fi P^ - Z-1
tmimwt~-( ffc* 'i*..' li m ^^ *m m i »W--
'J
1 9C
^Z7_
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: £ll(j<i^
SrrE: Old Buming Grounds at M-136
DESCRIPTION: SWMU #243; Grid # S_2~, 5 ft
PARAMETERS
Cd, Cr, Ag, Pb
Mercury
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
DATE: l2,'H/>r*if^ TV^E-.^O^ SAMPLER: ^TU,/
Thiokol Corporation RCRA FacUity InvesUgation
W0#: 1B940 LWR#: £ll04<J
SITE: Old Buming Groimds at M-136 —
DESCRIPTION: SWMU #243; Grid # /^ 2 ft
PARAMETERS
VolatUe Organics
METHOD
8240
#
HKTZ:IZ^fit*ir^ TIME: 827 SAMPLER:
;— «
77110^0/ Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: £///../
SITE: Old Buming Grounds at M-136 , ' '
DESCRIPTION: SWMU #243; Grid # /^ ^ 2 ft
fJ
PARAMETERS
Cd, Cr, Ag, Pb
Mercury
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
DATE:/ZW^^5^ ™1E: "621 SAMPLER: fJ
, ^ Thiokol Corporation RCRA FacUity Investigation
.OV^(iJ__ W0#: 1B940 LWR#: S//C)^
SITE: Old Buming Grounds at M-136 .^j
DESCRIPTION: SWMU #243; Grid # fy- . 5 ft
PARAMETERS
VolatUe Organics
METHOD
8240
KC^^m.
Liq/it ^rdu//i
•^if.^/^
--4
—r
m DATE: /Z ^l^t ^^ '"'^- ^"^^ SAMPLER: pl^
> .. --'•-•'• - •-- • • —I '..,1^ I J ..»-.«:- ^»wV .»^-.>
130
Thiokol Corporation RCRA FacUity InvestigaUon
WO#: 1B940 LWR#: £/{C'^
iQ^^H^ _ STE: Old Buming Grounds at M-136
DESCRIPTION: SWMU #243; Grid # T^- . 5 ft
" PARAMETERS METHOD
Cd, Cr, Ag, Pb 6010
Mercury 7470
HMX HPLC
Nitroglycerin HPLC
DATE: ^"2- ylff'^yf TIME: S^d^ SAMPLER: /~L*^
3JO_ Thiokol CorporaUon RCRA FacUity InvesUgaUon
W0#: IB940 LWR#: S/ZOi^
STTE: Old Buming Grounds at M-136 ,-/^ -p,- ' /?
DESCRIPTION: SWMU #243; Grid # /y, 2 ft PC " /O
PARAMETERS METHOD
VolatUe Organics 8240
>//^ 'Clci.
DATE:/ZVtr/>/'*?/'' TIME: '7/'^' SAMPLER: /^<-X-^
77iw*o/ Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/flOfC
SITE: Old Burning Grounds at M-136 —
DESCRIPTION: S\\'MU #243; Grid # /y . 2 ft
PARAMETERS ^IETHOD
Cd, Cr, Ag, Pb «>10
Mercurv "^^"^^
HMX HPLC
Nitroglycerin HPLC
DATE: /2'YCifili^ TIME: ^ ^0 SAMPLER: F^
O 7 Z -> ra/oAo/Corporation RCRA FacUity Investigation o^ 'Z. 2,~]
W0#: 1B940 LWR#: ^//O^O ——
SITE: Old Buming Grounds at M-136
DESCRIPTION: SWMU #243; Grid # // . 5 ft ;
PARAMETERS METHOD ^ ''^J~
VolatUe Organics 8240
DATE: / Z- ^Z*/" ^X^ TIME: 9^1) SAMPLER: puJ
•" *- " ''• '-'•''•.•• -» —'-- —.-'- -^•^-^ - - •-••- i-.^.1 _ -'•
Thiokol Corporation RCRA FacUity Investigation., 1 '-^ l
W0#: 1B940 LWR#: £H04^ -L«JJ-
IZJL
LWR#: C//i
SITE: Old Buming Grounds at M-136 . n
DESCRffTION: SWMU #243; Grid # //, 5 ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb 6010
Mercury 7470
HMX HPLC
Nitroglycerin HPLC
DATE: /Z^Cpf^i TIME: ?^3 S^IMPLER: fu-^
Thiokol Corporation RCRA FacUity Investigation
if^ 7 <^ W0#: 1B940 LWR#: £7/^^ lir - 1^
1^ ^^ SITE: Old Buming Grounds at M-136 , ©-^- ^—j-
DESCRIPTION: SWMU #243; Grid # lOyrl ft
PARAMETERS METHOD S '/-/r Cj
VolatUe Organics 8240
DATE: /Z^^r^/\ TIME: /O'lS^ S^MPLEV.•. f^' )
DATE : IZ^/it'l'i' TIME: I f^l Q SAMPLER: •^^'
•f^^
Thiokol Corporation RCRA Facility Investigation
SITE: Old Binning Grounds at M-136 .
DESCRIPTION: S\VMU #243; Grid # lOy, S ft RCl ^ 1"^
tU^-Oa^
"1-i
1
Thiokol Corporation RCRA FacUitv Investigation ,
W0#: 1B940 LWR#: ^///Ti^ i"
SITE: Old Buming Grounds at M-136 ^-^"^ t
DESCRUmON: SWMU #243; Grid # /C^. 2 ft "
PARAMETERS METHOD
Cd, Cr, Ag, Pb 6010 ^^-
Mercury -J^-JQ ]
HMX HPLC •*"
Nitroglycerin HPLC
DATE: /^ X^/^f/' TIME: /^ 2 i'^ SAMPLER: F>-*- -f"
PARAMETERS METHOD
1
VolatUe Organics 8240 <r ..t
I >« >>tl «»» " *«l
132
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^((0^0
SITE: Old Buming Groimds at M-136 . -
DESCRIPTION: SWMU #243; Grid # JOH^, S ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb 6010
Mercury 7470
HMX HPLC
Nitroglycerin HPLC
DATE: JZ ^jOt^ ^ TIME: ^^Jt) SAMPLER: ''TO
' Thiokol Corporation RCRA FacUity InvestigaUon jT
//)Si^ W0#: 1B940 LWR#: S//04O g^ ^ J^
~*^ STTE: Old Buming Grounds at M-136 . ^
DESCRIPTION: SWMU #243; Grid # I'LO. 2 ft
DATE:/^<V^;^f 5 TIME:/g571) SAMPLER: puj
PARAMETERS METHOD CJOLUiaM '^1 l'l"
VolatUe Organics 8240 'M
Thiokol Corporation RCRA FacUity InvesUgaUon
W0#: 1B940 LWR#: ^//OiO
SITE: Old Buming Grounds at M-136
DESCRIPTION: S\VMU #243; Grid # /Zo, 2 ft
PARAMETERS METHOD
Cd, Cr, Ag, Ph Mto
Mercurv 7470
HMX HPLC
Nitroglycerin HPLC
DATC: /^ \x^F f ^ TIME: /O^"^ SAMPLER: ^^
WO#: 1B940
SITE: OJd Buming Grounds at M-136
DESCRIPTION: SWMU #243; Grid # 2JAJ_, 5 R
PARAMETERS ^^^^^^
VolatUe Organics
•'^^ ~'°:.'ir""""°""S°'?>^ —3-^j^/7-
cW%K i>,it-
%
DATC :/-t 5cfir'i^ TIME: /^ i^^ SAMPLER: f^
fc^ i I f •.if* . ^U</1,.AV. ..1. •^. L^ .
m
:
"
re*, C.n»r.*" «CRA f*-'S'S^Sk W0#; 1B940 LWK#. OllVt^
SFTC: Old Burning Grounds at M-136
DESCRIPTION: SWMU #243; Grid # 7JLL' ^ "
133
PARAMETCRS
Cd, Cr, Ag. Pb
Mercury
HMX
NUroglycerin
METHOD
6010
7470
HPLC
HPLC
DATC: /7,S^/^fr TIME: /^rj^SAMPLER: ^^
Thiokol Corporation RCRA FacUity Investigation
IjiO W0#: 1B940 LWR#: £7/£>^>
SITE: Old Buming Grounds at M-136 ^^^
DESCRIPTION: S\\'MU #243; Grid # /g^ ft
PARAMETERS
Volatile Organics
METHOD
8240
BC ^ 2^
-5111- U/ifA
:50M/ -QmjttJ—. I ^-
•
-- UIJL
DATC: /^S^Z-f^^ TIME: A/O SAMPLER: ,ii>>^
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR*, ^/C>425
SFTE: Old Buraing Grounds at M-136 ^^
DESCRIPTION: SWMU #243; Grid # JSh 1 ft
PARAMETERS
Cd, Cr, Ag, Pb
Mercurv
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
DATC: /Z^/^.r TIME: ///^ SAMPLER: f^^
/ens
Thiokol CorporaUon RCRA FaciUty Investigation
W0#: 1B940 Lwk#: CT/J^^^
STTE: Old Buming Grounds at M-136
DESCRIPTION: S\VMU #243; Grid # /5S^ 5 ft
PARAMETERS
VolatUe Organics
METHOD
8240
ZC ' ll
•I DATC: IZ. S<pt H'^ TIME: //20 SAMPLER: r'"^
134
.... .^ WL . ...^ . .-.-»—~.-.-.^-»-i-t.:..A»y»^ i«i « .,'. 'aL t^»fV .liW' *iti
Thiokol Corporation RCRA FacUity Investigation
j^T'jr^^r^.^ii^/'.i'
/,.;,--) WO#:1B940 LWR#:^//^^
// ^t-/ SFTE: Old Buming Grounds at M-136
DESCRIPTION: SWMU #243; Grid # /S^ S ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb 6010
Mercury 7470
HMX HPLC
Nitroglycerin HPLC
DATC:/l^»'f5- TIME: J/ ZO SAMPLER: f^
,. _ Thiokol CorporaUon RCRA FacUity Investigation . 1/3 L WO#:1B940 LWR#: C^tlO^O gC — J 3
SITC: Old Buming Grounds at M-136 _
DESCRIPTION: S\\'MU #243; Grid # I "7J,! ft
METHOD Cu PARAMETCRS Mt^l^O" O/UJ / S///
VolaUle Organics 8240
_DATC: / ^ 'ycfi TJf TIME: SAMPLER: /^^^
f
Thiokol Corporation RCRA FacUity Investigation
W0#: IB940 LWR#: £://^>^"
SITC: Old Buraing Grounds at M-136 _
DESCRIPTION: S\A'MU #243; Grid # l7/,l ft
PARAMETCRS METHOD
Cd, Cr, Ag, Pb 6010
Mercury 7470
HMX HPLC
Nitroglycerin HPLC
DATC: /Z 'yCfit'7f^ TIME: SAMPLER: f^^
: ^-,
Thiokol Corporation RCRA FacUity Investigation
WO#:1B940 LWR#: J^//^^ \\40 SITCi Old Burning Grounds at M-136 ^^ TLi ~ \ ^T
•^^-^ DESCRIPTION: SWMU #243; Grid # XiT" ^ "^^ f^^^ '-^
PARAMETERS IVIETHOD
VolatUe Organics 8^40
DATC : /t S^r ?i TIME: //^^ SAMPLER: f^
-/..^^ m Thiokol Corporation RCRA FacUity Inve^atimi^
W0#: 1B940 LWR#: S/lt^f^
SITE: Old Burning Grounds at M-136
135
:•
DESCRIPTION: SWMU #243; Grid #
PARAMETERS
Cd, Cr, Ag, Pb
Mercury
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
DATE: /^ '>^T fS~hME: II4Z> SAMPLER: F*-^
_/Msi \rt^iC /^r Zuticfi O.M <:/&COT\
iSn Af QrJ ^ITL
m
-
Thiokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#: ^/lO^fO
STTC: Old Buming Grounds at M-136 . __
DESCRIPTION: SWMU #243; Grid # 0(ca 2 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC: /Z^rC4(ll^ J TIME: I2Z<^ SAMPLER: '^^
I
Thiokol Corporation RCRA Facilitv InvestigaUon
W0#: 1B940 LWR#: ^//04^
SITC: Old Burning Grounds at M-136
DESCRIPTION: SWMU #243; Grid # fSl^l ft
PARAMETERS
Cd. Cr, Ag, Pb
Mercury
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
-liA.TE:^Z%'C/>l~9S-TTME:I^ZO SAMPLER: /^J
r-y 7 C^ Thiokol Corporation RCRA FacUity Investigation
l^^2__ W0#: 1B940 LWR#: £7/04-0
SITE: Old Buming Grounds at M-136
DESCRIPTION: S\NTVai #243; Grid # IS~U, 5 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
Bc^ 7
-•>il-k, chu
Rr-f
^i/H, Ck 't^-
-DATC: TIME: /^Xi "SAMPLER: /""^U
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: ^//040
SUE: Old Buming Grounds at M-136 '-T^
_ DESCRIPTION: SWMU #243; Grid # /S~C» S ft
PARAMETCRS METHOD
Cd, Cr, Ag, Pb 6010
Mercury 7470
HMX HPLC
Nitroglycerin HPLC
DATC: I'f. ^^f ^T^TTME: /i35r~SAMPLER: ^*-^
Thiokol Corporation RCRA FacUitv InvesUgaUon
1367 W0#: 1B940 LWR#: E/fO^-O V^C ~ Zl
^ SITC: Old Buming Grounds at M-136 ^ ^— ^
DESCRIPTION: SWMU #243; Grid # "ZO-^l ft
PARAMETCRS METHOD
VolatUe Organics 8240
S)lki C-ia-u
DATC: /^Syrf3 TIME: /3S'I SAMPLER: /"t^
Tluokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: £^//C40
SITC: Old Buming Grounds at M-136 _ ^""^ r
DESCRIPTION: SAATVIU #243; DUP. Grid # OC^ , ZihHt " —
PARAMETCRS METHOD
VolatUe Organics 8240
DATC: lZ\(^t^f TIME: /^T/ SAMPLER: rW
Thiokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: ti/lO^O
STTE: Old Buming Grounds at M-136 ^
DESCRIPTION: SWMU #243; Grid # 20\ , 2 ft
PARAMETCRS METHOD
-_ Cd, Cr, Ag, Pb 6010
Mercun 7470
HMX HPLC
Nitroglycerin HPLC
DATC: ^Zhfit^y TIME: 13^/ SAMPLER: /-Uj
-•-/>_!
JML
Thiokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: (Tl/dfO
SITC: Old Buming Grounds at M-136 .
DESCRIPTION: SWMU #243; Grid # 2cS_, 5 ft
1 ."jrr
^£_^/^Z,.
PARAMETCRS
VolatUe Organics
METHOD
8240
-DATC:/ZV^^^ TIME:W':=551^ S*^«'"=•»• ^~'->'
77.ioko/ Corporation RCRA FacUity ^^'^'ff)^..
WO#:1B940 V^WI.CllM-^
STTE: Old Bi
DESCRIPTION
PARAMETCRS
^^l/y Cla.J.
SrrE: Old Buming Grounds at M-136 ^^
nPSCRIPTION: SWMU #243; Grid # _UJ3- = "
METHOD
6010
7470
HPLC
HPLC
Cd, Cr, Ag, Pb
Mercury
HMX
Nitroglycerin
l:IZ'nPl'^<^ TlME:,err SAMPLER: H^_ DATC:
/4_lk
Thiokol CorporaUon RCRA FaciUty Investigation
W0#: 1B940 LWR#: SllCH-0
STTE: Old Buming Grounds at M-136 . ^
DESCRIPTION: SWMU #243; Grid # //fc?2 ft Rr = -L
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC: (Z'>C0 fS" TIME: l^-'Z^^yO SAMPLER: /'^^
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^jO^O
SITC: Old Buming Grounds at M-136
DESCRIPTION: SWMU #243; Grid # jJlhfl ft
PARAMETCRS
Cd, Cr, Ag, Pb
Mercury
HMX
NUroglycerin
METHOD
6010
7470
HPLC
HPLC
• i DATC: IZ^k^tf^ TIME: l^l'^ SAMPLER: F^
. ...- .^_.»^J.« .:.^L^Jr^Jk. r^.^^^- ••, H..>.7l^^:^iL.»iI^^
138
Thiokol Corporation RCRA FacUity InvesUgation
WO*: 1B940 LWR#: Si'/^O
.J ^-^ srrE: Old Buming Grounds at M-136 ._ "Q/^ >— //
/T'O-i DESCRIPTION: SWMU #243; Grid # '(*='. S ft PC, ~: LiSL
PARAMETCRS METHOD
VolatUe Organics 8240 ^ kLbf^^M^
DATC: / 2 Upt^^ TIME: !45'S^ SAMPLER: Fi<-^
I
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:
srrE: Old Buraing Grounds at M-136 ^
DESCRIPTION: SWMU #243; Grid # /?>, 5 ft
PARAMETERS METHOD
Cd, Cr, Ag, Pb 6010
Mercury 7470
HMX HPLC
Nitroglycerin HPLC
DATC: /Z^Af/^ TIME: I4Z<> SAMPLER: P^ ^^
•nmkol CorporaUon RCRA FacUitv Investigation
WO#:1B940 LWR#: ^^ _ - ,
SITC: Old Buming Grounds at M-136 S<— - Z4
DESCRIPTION: SWMU #243; Grid # /fe. 2 ft ^
^^MJVffiTCRS METHOD —p, 7~;i^T7~
Volatile Organics 5340
DATC: I6r^f>r<^^ .^„
77„o*oi Corporation RCRA FaciUty Investigation
W0#: 1B940 ^WKff^
SITC: Old Bmning Grounds at M-13b >X/ ^ ft
DESCRiniON: SW^a] #243: Grid # i£U. ^
.x^^c METHOD PARAMETCRS
6010 Cd, Cr, Ag, Pb .^^.^^
Mercun ^pLC
HMX HPLC
Nitroglycerin
lj±.
:.>WuU.'V'*r-.J>--.
m
.15-4^
•
Thiokol CorporaUon RCRA FacUity Investigation
W0#: 1B940 LWR#:
SITE: Old Buming Grounds at M-136 j^^
DESCRIPTION: SWMU #243; Grid # f^H». 5 ft
PARAMETERS
VolatUe Organics
METHOD
8240
DATC: IZ ^t f j'^TIME: /^44- SAMPI.F.R: , iPf ^
Thiokol CorporaUon RCRA FacUity InvesUgation
WO#: 1B940 LWR*:
SITE: Old Buming Grounds at M-136
DESCRIPTION: SWMU #243; Grid # _Z±*» 5 "
PARAMETERS
Cd. Cr, Ag, Pb
Mercury
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
DATC: /7.S^,.rf^J-^TIME: /5^^ SAMPLER: F^.^
Thiokol Corporation RCRA FacUitv InvestigaU»,„
W0#: IB940 LWR#:
SITC: Old Buming Grounds at M-136
DESCRIPTION: SWMU #243; DUP. Grid # /4b
PARAMETC.RS
tT n
Cd. Cr, Ag, Pb
Mercury
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
Hl'LC
DATC: /l^pf f(^ TIME: /f 4^ SAMPLER: f^
139
^C- /Cr
:5/l/i. dia t^j^
I boo "Burn GtVuitd Of^cro/ffy*^ l^/vrM^d us h)
Siiut cfou.>A ,30 -Hiat 7^^^ Ccufd l^arn
140
C 7/0
073L _
:. Mor ^<:^
/ i/JJ/rU >-M0- '"> •'-••' - 'Sr /c
C'^J ^ ,y<^, M'dC: ^L-J,/ir( ,-^ ^A 2
Thiokol Corporation RCRA FaciUtv Investigation
W0#: 1B940 LWR#: ^//C'4 Z
SITC: Old Burning Grounds at M-136 ~P C ~/ 7
DESCRIPTION: SWMU #243: Grid # /^f 2 ft *^-^ ^-l—l— DESCRIPTION: SWMU #243; Grid # /ff2 ft
PARAMETCRS METHOD
VolatUe Organics 8240
DATC: ll^t'y'i TIME: 7 ?0 SAMPLER: FoJ
Thiokol Corporation RCRA Facility Investigation
WO#; 1B940 LWR#: ^/fC<f-1^
SITC: Old Burning Grounds at M-136
DESCRIPTION: SNVMU #243; Grid # l^f , 2 ft
PARAMETCRS METHOD
Cd, Cr, Ag, Pb 6010
Mercury 7470
HMX HPLC
Nitroglycerin HPLC
DATC: / 2 S y r '^f TIME: "7 IC SAMPLER: f-<-*^'
Thiokol Corporation RCRA FacUity Investigation
W0#: IB940 LWR#: ^ IjC^AZ.
STTE: Old Burning Grounds at M-136
ci^ f
. .^ . 3111:.: vjia curaing vjrounos ai .M-IJU ^ _y —j
0 l-H! DESCRIPTION: SWMU #243; Grid # /y^. 5 ft \iO_ —j /
PARAMETCRS METHOD
VolatUe Organics 8240
140
Thiokol Corporation RCRA FacUity Investigation
W0#: IB940 LWR#; d/lO'^'L
SITE: Old Buraing Grounds at M-136 . .
DESCRIPTION: S\\'MU #243; Grid # J^fli = ft
PARAMETCRS METHOD
Cd. Cr, Ag, Pb 6010
.Mercun 7470
HMX HPLC
Nitroglycerin HPLC
DATC: / 3 S-^-" '^ *7 J^ TIME: T'^C' SAMPLER: fiJ^
a
%
141
oe3f
Thiokol CorporaUon RCRA FacUity Investigation
W0#: 1B940 LWR#: ^//dT^Z
STTE: Old Buming Grounds at M-136
DESCRIPTION: SWMU #243; Grid # /fC, 2 ft
gc=- 1^
PARAMETCRS
VolatUe Organics
METHOD
8240
-5 ilh, 5^^-
DATC:/jrj^rfr TIME: 63 f SAMPLER: >^^'
. 1
r
r
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: c://^^'^
STTE: Old Buming Grounds at M-136
DESCRIPTION: SWMU #243; Grid # /f6. 2 ft
PARAMETCRS METHOD
Cd, Cr, Ag, Pb
Mercury
HMX
Nitroglycerin
6010
7470
HPLC
HPLC
DATC: ly^'yifif ^5 TIME: ^3^ SAMPLER: P-t*^
oe^_ Thiokol Corporation RCRA FacUity InvesUgation
W0#.- 1B940 LWR#: 0tC^C.
STTC: Old Buming Grounds at M-136 Q.
DESCRIPTION: SWMU #243; Grid # I fWs ft
EC- /Z
PARAMETCRS
Volatile Organics
METHOD
8240
DATC: /7 5i^/'9S^'TUitE: €^40 SAMPLER: Fc-^
Thiokol CorporaUon RCRA FacUity Investigation
W0#: 1B940 LWR#: £'/f^'Z..
SITC: Old Buming Grounds at M-136 ,^ .
DESCRIPTION: S\\'MU #243; Grid # /7US ft
PARAMETCRS
Cd, Cr, Ag, Pb
Mercun-
HMX
Nitroglycerin
DATC:/7Wt'7J^ TIME:
METHOD
6010
7470
HPLC
HPLC
a'^fO SAMPLER: 7"
142
n9oo P^MhlisL/t^ ^</ ^U- M-/9.^ 'SOUHK Y)ri}jrtU^/c/
-Nf-
ili VanJimi ^ SO. 7/4
II
-fc^
t ^^ 1 ^ P^R
l/)3c> Ar M'l^S -5 Col/ecfyy o r/tt^ bJaAK
% ^ O. -"CiLiFh. ^Ji .Zn, B^, Tf.
Thiokol Corporation RCRA Facility Investigation
WO#: 1B940 Lwii#: C'flO^Z.^
SITC: M-193-S Septic Drainfield .
DESCRIPTION: SWMU #638; Grid # j? ;5 ft
iC^il
PARAMETCRS
As, Cd, Cr, Cu, Pb, Ni. Zn
Mercurv
METHOD
6010
7470
Moisi
•So/ti ^_a //_
DATC: j^ %Z,fit9f TIME: 1041 SAMPLER-
Thiokol Corporation RCRA FacUity Investigation
WO#:1B940 LWR#: £7^C>^'^
SITC: M-193-S Septic Drainfield C~ - r
DESCRIPTION: SWMU #638; Grid # _^;= "
cr..}
PARAMETERS
Volatile Organics
1,4-Dichlorobenzene
METHOD
8240
8270
DATC: /S S^t "ir TIME-- M'^ ^A-MPLER: r«J
_^ . .t.. '
143
Thiokol Corporation RCRA FacUity InvesUgation
WO#: 1B940 LWR#: £7/^42
/ACI^ SFTC: M-193-S Septic Drainfleld
^^•-J-> DESCRHTION: SWMU #638; Grid # 5^; 10 ft ——
PARAMETCRS METHOD C>^ ~ ^
Volatile Organics 8240
1,4-Dichiorobenzene 8270 ^O/lc/. 5^//-
r
M^
- J>ATC: lI'Hfif ^r TI^JE: /CTS- SAMPLER: f.^
Thiokol Corporation RCRA Facility Investieation
WO#: IB940 LWR#: kf/D^t.
SITE: M-193-S Septic Drainfield
DESCRIPTION: S\VMU #638; Grid # _5^;10 ft
PARAMETCRS METHOD
As, Cd, Cr, Cu, Pb, Ni. Zn 6010
Mercury 7470
DATC: /B^fi;^^^ TIME: /DS"^ SAMPLER: >^-^
//-^ , TWoifco/Corporation RCRA FacUity Investigation 72/^ — >t
1^ i'O W0#: 1B940 LWR#: £f l04L P* ^ " T
SITE: M-193-S Septic Drainfield -
DESCRIPTION: SWMU #638; Grid # -^l ;5 ft
PARAMETCRS METHOD
As. Cd, Cr, Cu, Pb. Ni, Zn 6010
Mercuiy 7470
DATC: 15 ^JOT ff TIME: // ZO SAMPLER: F't^ il
\
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/0*ihZ.
STTE: M-193-S Septic Drainfield ^
DESCRIPTION: SWMU #638; Grid # ^/ ;5 ft
PARAMETERS METHOD
Volatile Organics 8240
1,4-Dichlorobenzene 8270
DATC: /3 '^tpr 9S^ TIME: // 20 SAMPLER: /'*"
I ^ A<^>JU^» •r..\- .i^/l^*V.l.J'»^| ^^'^r'^.f^.-U^/A:
144
Thiokol Corporation RCRA Facility Investigation
WO#: IB940 LWR#: £"(/£>< Z-
STTE: M-193-S Septic Drainfleld
DESCRIPTION: SWMU #638; Grid # ^4/ ;10 ft
//i5. PARAMETCRS
As, Cd. Cr, Cu, Pb, Ni. Zn
Mercury
METHOD
6010
7470
TiKTE: 13 ycprf S^ '^^^- ^^-33 SAMPLER: puJ
Thiokol Corpofation RCRA FacUity Investigation
W0#: 1B940 LWR#: c'//04^
SITC: M-193-S Septic Drainfield .
DESCRIPTION: SWMU #638; Grid # _fr/;U ft
PARAMETCRS
Volatile Orgamcs
1,4-Dichlorobenzene
METHOD
8240
8270
.E-^_f_i^
EJIC.OU/J /crc a
_Qrau<^l_Jkf__
Mc/fC£iJr^<lM^
DATC:/3C<^y^ fr' TIME: //33 SAMPLER: ru^
lis? 3rdaK fo^ Lun cly
Thiokol Corporation RCRA Facilitv Investigation
W0#: 1B940 Lwk#: ^//C^ t-
SITC: M-193-S Septic Drainfield
DESCRIPTION: SWMU #638; Grid # 00> ,S ft
PARAMETERS
As. Cd, Cr, Cu, Pb, Ni, Zn
Mercury
METHOD
6010
7470
SCJF^A
}lkru.jEjU. .'5ojiA_
jm_\f_
\>KTE:/^5i^ ^^^TIME: /^-Tf SAMPLER: /^
W0#: 1B940 LWR#: ^//04Z-.
STTE: .M-193-S Septic Drainfield
DESCRIPTION: SNVTVIU #638; Grid # 5^5 ft
PARAMETCRS
Volatile Organics
1,4-Dichlorobenzene
METHOD
8240
8270
DATC: /35«?r"?*5 ^TL\IE: /ZT*^ SAMPLER: /^O^
Thiokol Corporation RCRA Facility In\cstigation
145
r r t 1210
WO#: 1B940 LWR#: /5"//^)^C
SFTE: M-193-S Septic Drainfield
DESCRIPTION: SWMU #638; Grid # w>C^,10 ft
PARAMETERS
As, Cd, Cr, Cu, Pb. Ni, Zn
Mercury
METHOD
6010
7470
DATC: /5 ><^rf r~TIME: /^/^ SAMPLER: /T^^
Thiokol Corporation RCRA FacUity InvesUgation
W0#: 1B940 LWR#
SITC: M-193-S Septic Drainfield
DESCRIPTION: SWMU #638; Grid # ^Z>,Vi ft
^//o^-^
PARAMETCRS
Volatile Organics
1,4-Dichlorobenzene
METHOD
8240
8270
3C^^
/<^ru f.
hn mj/i
ti^.
Za^c^
JMILL
-
-V
m DATC: /J Sc^f 9 J^'TIME: /J/^ SAMPLER: /=i^J
Thiokol Corporation RCRA Facility Investigation
Thiokol CorporaUon RCRA FacUity Investigation
W0#: 1B9^ c LWR#: £//<Df Z_
Srre:/^VrJ-SeDtic Drainfleld
DESCRHTTON: SWMU #£lZ», Grid # ^7^, lOtt 2^/4ceJ^
PARAMETCRS
Volatile Organics
1.4-Dichlorobenzene
METHOD
8240
8270
DATC: / 5 Py)r5 JXTIME: /5/<^ SAMPLER: /^-U
/S3o
\VO#:1B940 LWR#: ^//^^ 2.
SFTE: M-193-S Septic Drainfield
DESCRIPTION: S\\'MU #638; Grid # //;5 ft
PARA.METCRS
As. Cd. Cr, Cu. Pb, Ni. Zn
Meicury
METHOD
6010
7470
DATC: /3 ^r^r^TTSfE: /SZO SAMPLER: /^U
Thiokol Corporation RCRA FacUity Investigation
-Be- L
Ikm-Jt M<_
/mWi
i.
-I 1
1
-• * -'-••• ' "* 1>«..
146 f-z/o^z^^ W0#: 1B940 LWR#
SFFE: M-193-S Septic Drainfield
DESCRIPTION: SWMU #638; Grid # _7^;5 ft
PARAMETCRS
Volatile Organics
1,4-Dichlorobenzene
METHOD
8240
8270
DATC:yJ?0^,^ ^^^'TIME: IS JO SAMPLER: fH/
134c
Thiokol Corporation RCRA FaciUtv Investigation
W0#: 1B940 LWR#: cT/'/d^^-
STTE: M-193-S Septic Drainfield
DESCRIPTION: SWMU #638; Grid # _7^;10 ft
BC^
PARAMETCRS
As, Cd. Cr, Cu. Pb. Ni. Zn
Mercury
METHOD
6010
7470
DATC: /5 Sir/37^'r3 TIME: /J*^0 SAMPLER: /x*J
Thiokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#: ^//O^Z-
STTE: M-193-S Septic Drainfield
DESCRIPTION: SWMU #638; Grid # Y1,10 ft
PARAMETCRS
Volatile Organics
1.4-Dichlorobenzene
METHOD
8240
8270
DATC: / 3 Scl/^rf r~ TIME: /3^0 SAMPLER:/HLJ
/:34-'r Alod/fif foU'/'fS-il :^u)AiJ ^ L3z^
% 4^1 ^6 \-m
-^
n5
_&iA>ivL_ik^ 6, e(. ,ze
v^-1^-^ -^' -"-i- ^' ->T I aitr- —••- ;-*-—^'
t t
Thiokol CorporaUon RCRA FacUity Investigation
\JL,<: W0#: 1B940 LWR#: £'/l04'Z,
STTE: M-193-N Septic Drainfield ^^
DESCRIPTION: SWMU #632; Grid # Q ;5 ft
PARAMETERS
As, Cd. Cr. Cu, Pb, Ni, Zn
Mercury
METHOD
6010
7470
147
5C^7
MOisi d/i
^
/4^g
DATC: l^^ycpr^^ TIME: /^/SSAMPLER: r^^'
Thiokol CorporaUon RCRA FacUitv Investigation
W0#: 1B940 LWR#: £il04-?__
SITC: M-193-N Septic Drainfield ^«
DESCRIPTION: SWMU #632; Grid # _S ;10 ft
PARAMETERS
As, Cd, Cr, Cu, Pb, Ni, Zn
Mercury
METHOD
6010
7470
-^^^(^
^lik. Ch
^^
DATC: / 5 5«y3rf j*^ TIME: /^2&> SAJWPLER: f—X.J
I^OJj Dc/f0^.rr-J TSo^p/r's CA//<i/^Jtr/ -Ai M-S^^ ^a/^^U>y
Tluokol CorporaUon RCRA FacUity Investigation
W0#: 1B940 LWR#: EI(04H-
S.;5ft
SITC: M-193-N Septic Drainfield
DESCRIPTION: SWMU #632; Grid #
PARAMETERS
As. Cd. Cr, Cu, Pb. Ni. Zn
Mercury
METHOD
6010
7470
DATC: /^ 5«:/i»^?J TIME: /!D4^' SAAIPLER: ''
JC^^
-SilHi Cld i^a^
-f
,-. 1 T«t»«^r<t '"rr'VfTv^'i^i. Jt^
148
^ SS^^'n'^r""""" '^^'^ ^"''"'^ InvestigaUon
WO#. 1B940 LWR#. ^/^^^jo,
/<<^— srrE: M-193-N Septic Drainfield '
^~. DESCRIPTION: SWMU #632; Grid # 28-10 ft
PARAMETFRS
As, Cd. Cr, Cu. Pb. Ni. Zn
Mercury
METHOD
6010
7470
DATC:/5'S^^fj-^V5i-r^,,MPLER: ^^
-J^
%
Ik'Od "^j/HMLr/rian C'f^iij /^.Ft- ^/-/t ^y edifUc^ r
ti
lots' -C'fl in^.rfii^ Cr^i^ ^'^f'^ "\ '^^ ./-/'/^.^
Thiokol Corporation RCRA FacUity InvesUgation j>
WO#: 1B940 LWR#: ^ll04^ii
STTE: M-193-N Septic Drainfield ^ '^
DESCRIPTION: SWMU #632; Grid # Qj^ ft
PARAMETCRS
As, Cd. Cr, Cu, Pb. Ni. Zn
Mercury
METHOD
6010
7470
jgc^e
^ilf^ c, t^Mc^
DATC.: /-f %Cfit^r^ TIME: /C'^'T^ SAMPLER: PoJ
ltr, ^"''"'' Corporation RCRA FacUity InvestigaUon
J_tIO__ WO#:1B940 LWR#: ^NQ^^^
SFTC: M-193-N Septic Drainfleld ^
DESCRIPTION: SWMU #632; Grid # 5^blO ft
PARAMETFR«;
As. Cd. Cr. Cu. Pb. Ni. Zn
Mercurv
METHOD
6010
7470
Sl I fy Cl&ti iPtf!
^^. ?/9/?fg /1/u. so/U
DATC: /4 ^f-f(~^rE: l((0 SAMPLER , f^
'i.-.. _. _.
:
mokol Corporafion RCRA FacUity Investigation
\V0#: 1B940 LWR#- B7/04^
/lth SFFE: M-193-N Septic Drainfield
I DESCRIPTION: SWMU #632; Grid # /O^H
PARAMETF.RS METHOD
I As, Cd, Cr, Cu, Pb. Ni, Zn
_i Mercury 6010
7470
149
'^C ^ 5"
^f'lf^ Ck^
7 DATC: /f ^^ y_p TIME: I lth SAMPLER: P^
I ^f3 Thiokol Corporation RCRA FacUitv Investigation
•—^^^ W0#: 1B940 " LWR#: ^//£>f^
STTE: M-193-N Septic Drainfield ^^
DESCRIPTION: SWMU #632; Grid # /OSyiQ ft
PARAMETCRS
As. Cd, Cr, Cu, Pb, Ni, Zn
Mercury
METHOD
6010
7470
D.\TC: l4-^jfir9r~ TIME: //S^ SAMPLER:/^^
^
1
-X-
i
r
u
Mg "B/M/hUrMOJl CrCjjJ /^A /i>^ hf^a /c
7-zf A-i- n'l'll e^/ahii^fr^
3^--^T^
•gA"'p<^iO' ^sWABce.^
I V
I 160 h^B!
Z^.LP6,^2. 4.1
... I ...->- ^ .^,. ,.f « .. ^ i .J.^. =.!,».,. \
150
/30(^
-Thiokol CorporaUon RCRA FacUity InvesUgation
W0#: IB940 LWR#: E'Ud'f'^
STTE: M-191 Septic Drainfield
DESCRIPTION: SWMU #631; Grid # ^"6 ; 5 ft
PARAMETER.^
Beryllium
Cadmiuni
Thallium
Mercury
METHOD
6010
6010
6010
7470
BC^JL.
^(IfOtAcl ^^j
'5>a/fc/
DATC: /^ 5t^;^y/— •VTME:/'S0>O SAMPLER: fU
I ^0 f Thiokol Corporation RCRA FacUity Investigation
' -^ I WO#:1B940 LWR#: £11044
SITE: M-191 Septic Drainfield _^.
DESCRIPTION: SWMU #631; Grid # _^:^;10 ft
PARAMETCRS
Betyllium
Cadmium
Thallium
Mercury
METHOD
6010
6010
6010
7470
DATC: /^SV^rf i'^ TXm.:/3<^f SAMPLER: /TUJ
Thiokol CorporaUon RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: ^//C44
STTE: M-191 Septic Drainfield
DESCRIPTION: SWMU #631; Grid # ^3 ^ ^
PARAMETCRS
Beryllium
Cadmium
Thallium
Mereury
METHOD
6010
6010
6010
7470
gr.' 7
^'ancif -Sil'-I
EC- ^
Siih
DATC: l4^t<Tl TIME:/^3^ SAMPLER:
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: S//d4^
STTE: M-191 Septic Drainfield - _
DESCRIPTION: SWMU #631; Grid # T '^lO ft
PARAMETCRS
Beryllium
Cadmium
Thallium
Mercury
METHOD
6010
6010
6010
7470
Sc- 6
%an(L
DATC: 14 hpt ^S ^lE: / ^4/ SAAffLER^ fiO
••Vi)
*-''-y--^-- -V.ti'* T -I- t, a----"*^ -• ...^ .a'!'-. -''..-• .>- .•..••-,,
Thiokol Corporation RCRA Facility Investieation
/34/ ^^°*- •?940 LWR#: '^//C^^
' SFFE:/fl-/?<Septic Drainfield :StVJUO -**^Z, S I
DESCRIPTION: SWMU #_4?/_; Grid #43.;^^ ft l:>Uphaafl
PARAMETCRS
•^ Be. Cd
Mercury
METHOD
kTl. 3P»r 6010
7470
151
DATC: Af Scf? ^ f J TIME: / 3^ / SAMPLER: /"T.^
/35"6> C^l/eo/tJ J<!/H<k. BJGA/^ ^j(6^ifx<^ Jece^ o/^
7Sfilii—5p£iiL '2aMf/tr f-
Uj^, ^ /09^^i L,(^R. eoc4<l
He, Cd, 7/ , Hp
'?//3tSiar/>ra.4 /7?Xe^tU /e^/r- £m Sr<ri^ ^
/fe^ 7*10*0/ Corporation RCRA FacUitv Investigation
W0#: 1B940 LWR#: ^//04^
SITC: M-191 Sepfic Drainfield
DESCRIPTION: SWMU #631; Grid # 6S- 5 ft
PARAMETC.RS
Beryllium
Cadmium
Thallium
Mercury
METHOD
6010
6010
6010
7470
•^c
^
3,//-
DATC: f^ ^^r ff TIME: /-fZI^SAMPLER: f^'
152
I4^h
Thiokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: £/l04^
STTE: M-191 Septic Drainfield ^
DESCRIPTION: SWMU #631; Grid # _^;10 ft
PARAMETCRS
Beryllium
Cadmium
Thallium
Mercury
METHOD
6010
6010
6010
7470
DATC: Ij^tif^ TIME: /45^ SAMPLER: ft^
Thiokol Corporation RCRA FacUitv Investigation
U.'S'l^ WO#: 1B940 LWR#: ^ //^>ff
SFFE: M-191 Septic Drainfield _.
DESCRIPTION: SWMU #631; Grid tt &Z^S ft
PARAMETCRS
Beryllium
Cadmium
Thallium
Mercury
METHOD
6010
6010
6010
7470
EC - /
3/// ^/?c/ A>-^ 3
DATC: H S^ y-fj"lTME: /^^'Z- SAMPLER: /^^
/r/5
Thiokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 Lwk#: ^/fC^^
STTE: M-191 Septic Drainfleld ^
DESCRIPTION: SWMU #631; Grid # C?2|10 ft
PARAMETCRS
Beryllium
Cadmium
Thallium
Mercury
METHOD
6010
6010
6010
7470
B,C--C
7^±AS^.
DATC: '*' ^\' ""/*> TIME: f "^ J3 SAMPLER: /^
-«,f>^ .ikJ. ,,tlt, ti.' .nJ-^t^m<..r.-rm^ m'^^.,„.,e,^^.,la .
153
J
i
T
#
i
5e.pf /^ /f^6:
^/tt_^o^/iko-^OyjA :^M -^ Mojl
I I -
Thiokol Corporation RCRA FacUity Invesligation
WO#: 1B940 LWR#: £//04B
STTE: Old Buming Grounds at M-136 ' S^i ^
DESCRIPTION: SWMU #243; Grid # 14 . 2 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
-DATC: f-Z^'^r' TIME: So4, &VMPLER: J^<"'
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: tZf/04^
SFFE: Old Buming Grounds at M-136-S/W*!//
DESCRIPTION: SWMU #243; Grid # /^ , 2 ft
PARAMETCRS
Cd, Cr, Ag, Pb
Mercury
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
DATC:f-/g-fr TIME: Sb^ SAMPLER: >C-.«^
BC^ ^U
'S/lt, Crave./
Ond 5tf/i^
St*",'J;".?""""*" ^^^ ^'"^"^'y tovestipation W0#: 1B940 LWR#: ff/7c4£
STTE: Old Buming Grounds at M-136 - ^A*a.l4
DESCRIPTION: SWMU #243; Grid # /•f7sii
PARAMETER*;
VolatUe Organics
METHOD
8240
TZC - /4
Sl/l/.Q/a t
•
DATC: ^/g-fr TIME:^8/4 SAMPLER: fJ
154
Thiokol Corporation RCRA FaciUty Investigation
WO#: 1B940 LWR#: £'/ta4Q
SITC: Old Buming Grounds at M-136 -5/*ui//
DESCRIPTION: SWMU #243; Grid # /4 , S ft
PARAMETCRS METHOD
Cd, Cr, Ag, Pb 6010
Mercury 7470
HMX HPLC
Nitroglycerin HPLC
DATC: f-/6'f^ TlSfE:d8/4 SAMPLER: /V>
•samdlc /rvt*\. ^ •*^/4 ^ ft fiAeZ <oZc£.(yy,
Voc MJ-hxIs . a Ac/ ^xp/o^/udr anal't'i/.r-
O^.^Q, ^t-U/hJi/ff/*, ffe Sa/>Y>lc ^^*l3Z-2/S. J^acjtls W//Z
/f<g'/ a//a**J P^rtcA-4:A<m £>/ 156/7/ -sPoOK T^z^uc^
drilkrj /4> 6>/l'/rMA*- J/I/A'M. <M c/r^/i. AJJif^t-r 3aA4^Jr
Cen /fC Ca//t,c/cJ. //ho/r^ /JVe /Z^c/ M0<^^
^ fi£.i^ /^>03^(m afiproviA(aL/'f ZO^ /ti -/^
/)0/) 7 Thiokol Corporation RCRA FaciUty Investigation
^T^*^- W0#: 1B940 LWR#: ^77(546
SFTC: Old Buming Grounds at M-136 - OM»tf iB ^ -^ 2 7
DESCRIPTION: SWMU #243; Grid # 3Z-, 2 ft -—^
PARAMETERS METHOD
VolatUe Organics 8240
DATC: f-/8-'?r' TIME; ^^0 Z_SAMPLER: ^^
Tiiiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: £y/04&
STTE: Old Buming Grounds at M-136 - SA**//
DESCRIPTION: SWMU #243; Grid # 7Z-, 2 ft
PARAMETCRS METHOD
Cd, Cr, Ag, Pb 6010
Mercun' 7470
HMX HPLC
Nitroglycerin HPLC
DATC: f./S-fr TIME: ^^i5 ^^ SAMPLER: /^«-»
C/ouof 5///-m
155
Thiokol CorporaUon RCRA FacUitv Investigation
W0#: 1B940 LWR#: ^//0^2>
— SITE: Old Buming Grounds at M-136 - "S-^*'"''
O'f^f DESCRIPTION: SWMU #243; Grid # ? 2-. 5 ft
PARAMETFRS
VolatUe Organics
METHOD
8240
S/// i^/?o/
/?/U Sd/!,/
DATE: 9-/e- 9 r TIME: OfOf SAMPLER: Fi,J
Thiokol Corporation RCRA FacUitv Investigation
W0#: 1B940 LWR#: e.//£>f'&
STTE: Old Buming Grounds at M-136 - ^M* '(
DESCRIPTION: SWMU #243; Grid # 3 2_, s ft
PARAMETCRS
Cd. Cr, Ag, Pb
Mercury
HMX
Nitroglycerin
DATC: f'/d~i^
METHOD
6010
7470
HPLC
HPLC
TIME •.oii>f SAMPLER: /vJ
9Zo Cr(FLL' cfr, /f/j^o/C
^S7 5<!rt/-,n// £f.i/> ^!v_ a.j
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: £7/^ 4€
SITE: Old Buraing Grounds at M-136 - S/uait
DESCRIPTION: SWMU #243; Grid # ^'t , 2 ft
r^= 33
PARAMETERS
VolatUe Organics
METHOD
8240
S//-^
•
...^. 9-/f^'9f TIME: /OCT'^ SAMPLER: ^-^^
Thiokol Corporation RCRA FacUitv Investigatioji
W0#: 1B940 LWR#: enO<fZ.
SITC: Old Buming Grounds at M-136 - "^^e-11
DESCRIPTION: SWMU #243; Grid # S'f 2 ft
PARAMETFR«;
Cd, Cr, Ag, Pb
Mercun-
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
DATC: 9-/6 '9r- TIME: /OO^C SAMI'LER: /-< /-UJ
<1 ..\-.-^ >•.'-.' . >
156 Thiokol CorporaUon RCRA FaciUty Investigation
W0#: 1B940 LWR#: £/tC4t,
STTE: Old Buming Grounds at M-136 - 5rJi^l^
DESCRIPTION: SWMU #243; Grid # S~/ , 5 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
Be ^ If
An/ '3a/tc/
DATC: ^-/^-^S' TIME; : lO/-> SAMPLER : /^-^
Thiokol Corporation RCRA FacUitv InvestigaUon
W0#: 1B940 L\VR#: C"//<:> <fi
SFTC: Old Buming Grounds at M-136 -S/Uc //
DESCRIPTION: SWMU #243; Grid # J7 . 5 ft
PARAMETCRS
Cd, Cr, Ag, Pb
Mercun'
ICVDC
Nitroglycerin
DATC: 9-/3''? i^
METHOD
6010
7470
HPLC
HPLC
TIME •./or SAMPLER: ^L.'
.v -, .*, Thiokol Corporation RCRA FacUitv Investigation
lt>2tj^ W0#: 1B940 LWR#: ^'tOi^
SITC: Old Buming Grounds at M-136 ~^A^<'
DESCRIPTION: SWMU #243; Grid # 4^ , 2 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
SC^/Z
DATC: ^-/d-ff TTSTE: /D3'^ SAMPLER: /^^
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^//C'4&-
STTE: Old Buming Grounds at M-136 . .
DESCRIPTION: SVNTMU #243; DUP. Grid # /^UP , %-Tt
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC: ^-/B 'f f TIME : /O?'^ SAMPLER: /^C«--'
157
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR*: £:it04^
STTE: Old Buming Grounds at M-136 -^^^''
DESCRIPTION: SWMU #243; Grid # 4"^ . 2 ft
PARAMETCRS
I Cd, Cr, Ag, Pb
-j Mercury
i HMX
-^ NUroglycerin
METHOD
6010
7470
HPLC
HPLC
DATC : ^-/g-*?^ TIME: /d? J ^AMPLER: F^^
If Thiokol Corporation RCRA FacUitv Investigation
/^7 W0#: 1B940 LWR#: ^//O^t
irJlA ^^^^'- ^^^ Bummg Grounds at M-136 - SAW<J '^
JUn^L DESCRIPTION: SWMU #243; Grid # -44-, 5 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
-gc^//
S//'^ OtJ
f^^ Sen J
%•
%
m D\TE:^-/0-^<r TIME.: I040 SAMPLER:/^
Tldokol CorporaUon RCRA FacUity Investigation
W0#; 1B940 LWR#: ^//^»
SFTE: Old Buming Grounds at M-136 -S/K^ "
DESCRIPTION: SWMU #243; Grid # ^4--, 5 It
PARAMETCRS
Cd, Cr. Ag, Pb
Mercury
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
DATC: 9'IB. ••^'7- TX^TE: lOZ/L> SAMPLER: /''<''
Thiokol Corporation RCRA Facilitv Investigation
, - ^^ • W0#: 1B940 LWR#: ^/fC>4^
/'-'-^ / SITC: Old Burning Grounds at M-136- £>yttf</f
DESCRIPTION: S\\'MU #243; Grid # S2 , 2 ft
PARAMETC.RS
VolatUe Organics
METHOD
8240
L - 7X
UA^
DATC: 9'/^-'7<' TIME: /^ 5^ SAMPLER: /^CO
1 ^^
Thiokol Corporation RCRA FacUity Investigation
WO#:1B940 LWR#: ^ff04e
STTE: Old Buming Grounds at M-136 •-^'''*^''
DESCRIPTION: SWMU #243; Grid # _tl3< ^ '» ^
PARAMETCRS METHOV
Cd, Cr, Ag, Pb
Mercury
HMX
Nitroglycerin
6010
7470
HPLC
HPLC
DATC: fVg-fi' TIME:/^r^ SAMPLER: ^^
DESCRIPTION: SWMU #243
METHOD
VolaUle Organics
DATC: J-^^^S TIME: //// SAMPLER: ^^-^
7*10*0/ Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^//i>4S'
STTE: Old Buming Grounds at M-136 ~ SMC:^'
DESCRIPTION: SWMU #243; Grid # 1^-3, S ft
PARAMETCRS METHOD
Cd, Cr, Ag, Pb 6010
Mercury 7470
HMX HPLC
Nitroglycerin HPLC
DATC: . 9'/S'-*7"S TIME: //// SAMPLER: AiLx-'
SITC: Old Burning Grounds at M-136 '^^^"/^
DESCRIPTION: S^^'MU ««; Grid # _T3 2 "
PARAMETCRS ^ESIOD
DATC •9'/B-9^ TIME: /IZf SAMPLER: ^^
STTE: Old Buming Grounds at M-136 '^Hf^^
TvircrniTrnON- SWMU #243; Grid # Z>->_, 5 «
Silt GAC! PARAMETCRS
8240 /,;^ 'SQ/CI
—-— Thiokol corporation RCRA ^^^^fff^^ -jrT^ —-
•LA ^llf- !jJ:ff\
-^nri^- /a'A.e
VolatUe Organics i)fO\'d/
-'J
159
Thiokol Corporation RCRA FacUity InvesUgation
WO#: 1B940 LWR#: ^11 i-<^
STTE: Old Buming Grounds at M-136 ^^"^ "
DESCRIPTION: SWMU #243; Grid # Tf-, 2 ft
PARAMETCRS
Cd, Cr, Ag, Pb
Mercury
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
DATC: 9-^/6-^'^ TIME: //Z 9 SAMPLER: ,C^_
11^^ Thiokol Corporation RCRA FacUity Investigation
\^OIt: IB940 LWR#: e^Z/C-^-^
SITE: Old Buming Grounds at M-136 l^iui. if
DESCRIPTION: SN^TVIU #243; Grid # ^4-,5ft T-/'- /3
#
PARAMETERS
VolatUe Organics
METHOD
8240
Ti\TE: 'y-Z't ''94 TIME: //JB SAMPLER: /^.<_/
Thiokol Corporation RCRA Tacilit\ Investigation
WO#: 1B940 ' LWR#: E//C4S-
STTE: Old Buming Grounds at M-136 - tiA<^ ^'
DESCRIPTION: SWMU #243; Grid # f«f , 5 ft
PARAMETCRS METHOD
Cd, Cr, Ag, Pb
Mercury
HMX
Nitroglycerin
6010
7470
HPLC
HPLC
DATC: 9-/^-?^ TIME: //JS SAMPLER: ^f^^'
, „ ..„„ HCRA FacUitv Investigation
-^ 77.10*0/Corporation RCRA l-acm^ ^^j^^^
'"^ l7/-Z WO#: 1B940 \ , , <„^^,, I
^^-^^^^^ SITC: Old Burning Grounds at M-136 ^
DESCRHTION: S^^'MU «43; Grid # ^^, -
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC: q-ie -^ r^TIME: /^^ ^ SAMPLER: F^
Silf 0/icL
%c^rlcL
:5]lf
-i
rt
— 4
1
I
J
-~* • - »•»* -•*^--.»^». •• ••• .t... ..- i, .afn m 'i,^ » •.V •^.-.^.1^*,^-!., ,,.---:.i.'.^.'-"-«-f:-«>-.<rv-...- ••^•--•..- .
160
,7..o*o/ corporation RCRA FacUUyJnvgig-tion
WO#: 1B940 LW#^ •T^IZTI
SITC: Old Buming Gromids at M-136 '.>^^
r>i7<:rRiPnON: SWMU #243; Gnd # _Z£J.. 2 " DESCRUmON: SWMU
PARAMETCRS
Cd, Cr, Ag, Pb
Mercury
HMX
NUroglycerin
METHOD
6010
7470
HPLC
HPLC
DATC: 9-It -fr TIME: / Zg Z^ SAMPLER: : F^
m^ Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: er>>^^^'
SITE: Old Buming Grounds at M-136 - SMc I (
DESCRIPTION: SWMU #243; Grid # ^/'l , 5 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC : 9-/S-^F TIME: /2/'f SAMPLER: p-U^
^C - U
^t/i 0^.^
fiyu. 'S^-'ld
/fifil S'ctML
6rc,\ftj. if
Thiokol Corporation RCRA FacUity InvesUgation
W0#: 1B940 LWR#: ^Jl^^f^
SFTC: Old Buming Grounds at M-136 - 5"'^"=' ' <
DESCRIPTION: SWMU #243; Grid # /^V , 5 ft
PARAMETCRS METHOD
Cd, Cr, Ag, Pb
Mercury
HMX
Nitroglycerin
6010
7470
HPLC
HPLC
DATC: 9-l^-^<7^ TIME: IZZ^ SAMPLER: A-^
Z-l< l^rfalC hi' Luncl^^
z^A/t^ nr Booic-
/S ^/).T /9 9i^
/3^^ A^ 5-/>^ ^^ //-/5CP ;^a;/^t; ^-z^? £IIAMU±
1530
-MSS -•-,•' iij;:^ ^-. . ^ v;y_ >^w^>/«>iy ^.±:^ S2Mpj
'n.,-»i,«i rn—wtrotinn HCRA FacUitv Investieation U
S-Z
Thiokol CorporaUon RCRA FacUity InvesUgation
W0#: 1B940 LWR#; ^//O^Q
SITE: Old Buming Grounds at M-136 ~^SAtaff
9Z^1 ft DESCRIPTION: SWMU #243; Grid i
PARAMETCRS
VolatUe Organics
_Z^2
METHOD
8240
gc~ 3X
^ilf bJiti:
^d/m /an
_^A^^.. r-
, f-/0 ^f TIME: /J50 SAMPLER: F ^^ DATC
771/0*0/ Corporation RCRA FacUity In^esU^""?^^
W0#: 1B940 LWR#: ^^^
STTE: Old Buming Grounds at M-136 ^J^"''
DESCRIPTION: SWMU #243; Grid # _Zc^ 2 ft
m
PARAMETERS
Cd, Cr. Ag, Pb
Mercury
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
I64C
DATC: 9-/8-9^ TIME: /T^;^ SAMPLER:
77iio*o; CorporaUon RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/fQ/f^
STTE: Old Buming Grounds at M-136 jS*** ' '
DESCRIPTION: SWMU #243; Grid # J Z^ S ft
F^
3c^ 1_
PARAMETERS
VolatUe Organics
METHOD
8240
DATC : ^-/^-fi^ TIME: /3^^ SAMPLER: Z^U^
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £-//04'2—
SITC: Old Burning Grounds at M-136 ^^^'
DESCRIPTION: SWMU #243; Grid # vZ. S ft
PARAMETERS
Cd. Cr, Ag, Pb
Mercury
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
DATC: '^'/^^•?^ TIME: l34C SAMPLER: AJ
Thiokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: ^ //04-2'
SITC: Old Buming Grounds at M-136 - -^"^ •'/ ^
DESCRIPTION: SWMU #243; DUP. Grid # v'l., ^
PARAMETCRS METHOD
Cd, Cr, Ag, Pb
Mercury
HMX
Nitroglycerin
6010
7470
HPLC
HPLC
DATC: I'li;^^^ TIME: /3^C' SAMPLER: ^{/J
13^ 2L 7*10*0/ CorporaUon RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: £'/l04t
STTE: Old Buming Grounds at M-136 •S/*^'^'
DESCRIPTION: S\\'MU #243; Grid # _Jf^, 2 ft
PARAMETERS
VolatUe Organics
METHOD
8240
Sc - -^r^ ll
ZZoi^f ^ilf
Uj.!tl\ .:z,on^-
u Vc
DATC: 9-/€'-'9\ TIME: is^7 SAMPLER .:F^
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^//Cfy
STTE: Old Burning Grounds at M-136 .5/5< ^-^-i
DESCRIPTION: SWMU #243; Grid # VC-, 2 ft
PARAMETERS
Cd. Cr. Ag, Pb
Mercury
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
l4l^
DATC: /--/6'^/^ TVSTE: /35" 7 SAMPLER: ^ ^^
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: &/c4-B
STTE: Old Buming Grounds at M-136 %'r.A.a-C\
DESCRIPTION: S\\'MU #243; Grid # QC-, S ft
PARAMETCRS
VolatUe Organics
METHOD
8240
3c_^_K^
n'lti-,}- ^,-)h
^/^-^s iH^
Thiokol Corporation RCRA FacUity Investigation
LWR#: tl'^'r<--W0#: 1B940 '.i-SITC: Old Burning Grounds at M-136 "^'^'^
DESCRIPTION: SWMU #243; Grid # _xA' » f«
PARAMETCRS
Cd, Cr, Ag, Pb
Mercury
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
f^
::
%•
I44Z) ZMMOTIAA CooiV _on JonaK. Sc?M/ylcs Co//cehl
und A/ CuJ\Z eiid4h -i^tun ^ /A-^S. Z^a/^rcLj^
is 21 &f(€^/rrt^ ._b.a C^roiLnJ :50m/?/cS 'Sou.ft^ of M-:^!-
^-
Thiokol Corporation RCRA FaciUty InvesUgaUon
W0#: 1B940 Lwik#:
SITE: Buming Ground Area
DESCRIPTION: Strategic RFI Background; Surface
PARAMETCRS
VolatUe Organics
METHOD
jS-e-^.»-_
-.^~
S//V- g/fo
SA\all—^f^'^<- ^
m
DKTE: ^-/Q -^-^ TIME:/Sr27 SAMPU:R: F^'
Thiokol CorporaUon RCRA FacUity Investigation
W0#: 1B940 LWR#:
SITC: Buming Ground Area
DESCRIPTION: Strategic RFI Background; Surface
PARAMETCRS METHOD
Cd, Cr, Ag, Pb, As, Ba, Se, Sb Be, Ti, Ni, Zn 6010
Mercury 7470
Cyanide 9010
HMX HPLC
Nitroglycerin HPLC
pH 9045
Sulfate 9036\9038
_DATC:7-/e"f S~ TIME:/S2 7 SAMPLER: fu^
^'iV
Tluokol Corporation RCRA FacUity InvestigaUon
T W0#: 1B940 LWR#:
- SITC: Buming Ground Area
DESCRIPTION: Strategic RFI Background; 2 ft
PARAMETERS
VolatUe Organics
METHOD
8240
3C^^J
jSiJr a/i6
7SM4lJ—QrdLi/Ci
DATC: 9-/&-'7*^ TDIE: /^^O SAMPLER: F^
Thiokol CorporaUon RCRA Facility InvestigaUon
W0#: 1B940 LWR#:
SITC: Buming Groimd Area
DESCRIPTION: Strategic RFI Background; 2 ft
PARAMETCRS METHOD
Cd, Cr, Ag, Pb, As, Ba, Se, Sb Be, Ti, Ni, Zn 6010
Mercury 7470
Cyanide 9010
MVK HPLC
Nitroglycerin HPLC
pH 9045
Sulfate _ 9036\9038
DATC: Y'/6i~'?i TXS\E: /^^O SAMPLER: FLJ
jS-41
Thiokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#:
SITC: Burning Groimd Area
DESCRIPTION: Strategic RH Background; 5 ft
PARAMETCRS
VolatUe Orgaiucs
5-^^; l/o^
METHOD
8240
'6Z70
Kc ' ZZ-
DATC: ^-/g>-*?S^ TIME: /5^0 SAMPLER: F^
Thiokol CorporaUon RCRA FacUity InvestigaUon
W0#: 1B940 LWR#:
SITE: Buming Groimd Area
DESCRIPTION: Strategic RH Background; 5 ft
PARAMETCRS METHOD
Cd, Cr, Ag, Pb, As, Ba, Se, Sb Be, Ti, Ni, Zn 6010
Mercury 7470
Cyanide 9010
HMX HPLC
Nitroglycerin HPLC
pH 9045
Sulfate ^ 9036\9038 rr j
DATC: T-/^-5'3 TIME: /5^C> SAMPLER: /''^
/00(i Bum (£,ou,J -io ~Burn
/lolkc/ /^; /vO ^'^
-Zl^M rcL lc (c Op c rolji
A T^^tZccU<:::7
320 '^/m/'^r/ifi^/i OeLO__0/l c:^'/c ^/c/ <^//%^ o/>^^'ajL^
A/^pt-J)/i .J.%J^:-^ - .
/VY '^A' 1/6/ik. UJH I 601/ec/- ^OfvflC^ frsnn
^r_^iC—f/k/-^' r/ef /^S from /^cU dnlkJ acjiaCcJ'
h Cm hn
B^-Q i-MU-
Thiokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: ^//,i?S"0
SITC: Buming Ground Area
DESCRIPTION: Strategic RFI Background; 10 ft
PARAMETCRS
VolatUe Organics
"Staiu—1/<3 A--
:s.C-L_a
S/// dP/''<d
J^/<^ _v$^^^.'^_
DATC: ^P'l^-f S^ TIME: ^^*^ SAMPLER: /=W
niDOHJl
Thiokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: £^//OSO
SITC: Buming Groimd Area
DESCRIPTION: Strategic RFI Background; ILO ft.
PARAMETERS
Semi VolatUes
METHOD
8270
9C'V_
_DATC: ^-/f-'7> TIME: 03^-' SAMPLER: Fu.'
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £//0S~O
SITE: Buming Ground Area
DESCRIPTION: Strategic RH Background; 10 ft
PARAMETCRS METHOD
Cd, Cr, Ag, Pb, As, Ba, Se, Sb Be, Ti, Ni, Zn 6010
Mercury 7470
Cyanide SK)10
HMX HPLC
Nitroglycerin HPLC
pH 9045
Sulfate ^ .. r^ 9036\9038
.DATC: y'/9-9y TmE:S<rcJ SAMPLER: F<^
Thiokol Corporation RCRA FacUity InvesUgation
W0#: 1B940 LWR#: O^/fCS'u
SITE: Buming Groimd Area
DESCRIPTION: Strategic KFI Background; 15 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
3C- /(^„
Z,tu Sci/tJ
.. "f'/^-'ir nATP. -J'f'-r-'?) TIME: *?CJ SAMPLER:
Thiokol CorporaUon RCRA FacUitv Investigation
WO#:1B940 Lwk#: £)TrZ^
SITE: Buming Groimd Area
DESCRIPTION: Strategic RH Background; IS ft.
PARAMETCRS METHOD
Semi VolatUes 5270
ft tA-^
_DATC.: <?_/<?_ ^f— TTii«.. Or^A _ ^ )
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: (^((O^STJ
SITC: Buming Groimd Area
DESCRUmON: Strategic RH Background; 15 ft
PARAMETCRS METHOD
Cd, Cr, Ag, Pb, As, Ba, Se, Sb Be, Ti, Ni, Zn 6010
Mercury 7470
Cyanide 9010
HMX HPLC
Nitroglycerin HPLC
PH 9045
Sulfate 2p36\9038 __ ,
DATC: 9'/7'l\ TIME: f^ d/ SAMPLER: /^U
9iZ-
Thiokol Corporation RCRA FacUitv InvesUgation
W0#: 1B940 LWR#: C/ZOTQ
SITC: Buming Ground Area
DESCRIPTION: Strategic RFI Background; Surface
PARAMETCRS
Semi VolatUes
METHOD
8270
'^U
TIME: DATC: 9-/9-91^
Thiokol CorporaUon RCRA FacUitv InvestigaUon
WO#:1B940 Lwk#: ^//^"Tc^
SITC: Buming Ground Area
DESCRHTION: Strategic RFI Backgromid; 2 ft.
y/^ SAMPLER:Vct/
PARAMETC.RS
Semi VolatUes
METHOD
8270
'^3.
' ^'/c ^ri^lc
armhsr] / u ^
of O/if/ /lA/ JQ /U//^ I*" '^' i^
DATC: 5?^/^, ^^ TIME: <?^i
Thiokol Corporation RCRA FacUitv Investigation
WO#: 1B940 LWR#: £^//CS^
SITE: Buming Ground Area
DESCRIPTION: Strategic RFI Background; 5 ft.
SAMPLER: /^i—^
PARAMETCRS
Semi VolatUes
METHOD
8270
DATC: J-/9-9r' TIME: ?ZP SAMPLER: F^
J05C _Jz.^u,pmrJ C/eo/icd _.^^c/ _.o.i--s,Az__ Of- JA-Z'^e
Thiokol Corporation RCRA FacUitv Investigation
W0#: 1B940 LWR#: £'105''^
SITC: M-338 Subsurface Discharge,
DESCRIPTION: SWMU #608; ^^/^Pepth
PARAMETCRS
Antimonv
Arsenic
Chromium
Lead
Sulfate
pH
DATC: 9'/9'9r
METHOD
6010
6010
6010
6010
300
9045
TIME: /OS^ i Fuj
Bc^Uj __
Sif JO irk
_Jj/lL _^/Jci
_jr
Jr
i/Z3
Thiokol CorporaUon RCRA Facility InvestigaUon
W0#: 1B940 LWR#: £'//0S~O
SITC: M-338 Subsurface Discharge
DESCRIPTION: SWMU #608; ]Q f^yCts. zc^&
PARAMETCRS
Antimony
Arsenic
Chroinium
Lead
Sulfate
pH
DAi-E: 9-I9-9T
METHOD
6010
6010
6010
6010
300
9045
Sfli ^ /M^ SG^U
TIME: lll2 SAMPLER: F^
ISeo.^, .^4>/»^/l^a^.ms^iv/ZA ^/As_ z:^.
>^Z- .Z^~^6 7 - SaJcAf _/s.
Zlac//H^ ZaZp CA^^:Jz /^. /U'34e acc<i:5s zvMZ /;^f T
Z^fc^
^-z^?-fr~
OlI^Z^mMUAi^jt —CFeto a_L. M-/^/^ i^:^Z:d)irt ^ZZi>K< ^
to__Caf_ tf^gyuj 'f^fiacc Eaac/s o/tc/ (SrouMc/'i /irriAJOs
/^^«g^r a/i.J UJ Zcch- yyax^ Sa/uJ)Zfh^, pa/A.fr
C>8i7_77Sc6__Uffi _oycK. (gr/^ ?f5" rs^u.i/uu
7D.AfL
OB ^7
Thiokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: E:ilOi^'2..
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # JT . 5 ft 75c.^JL
PARAMETERS
VolatUe Organics
METHOD
8260 TjQncl - d I'u,
- DATE: 'f'2C'9r TIME: 'C:J4 7 SAMPLER: /^c
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: ^7/^ 5" 2-
SITC: Domestic Wastewater Drainfieliis A. B, and C
DESCRIPTION: SWMU #625; Grid # S*^, 5 ft
PARAMETERS METHOD
Bis(2-ethylhexyl)phthalate
Nitrobenzene
8270
8270
DATC: f-Zc'^^ TIME: 'C'^ 7 SAMPLER: /^i-
8
/.; ;> ^.^•::r^7^^t^^k^^^-
Thiokol CorporaUon RCRA FacUity InvesUgaUon
W0#: IB940 LWR#: d.-'/CS'^
STTE: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # O , 5 ft
PARAMETCRS
B, Cd, CT, Ag, Pb
Mercury
METHOD
6010
7470
DATC: 7-A"'7'''r^ TIME: &'VA'7 SAMPLER: >C,
Thiokol CorporaUon RCRA FaciUtv InvestigaUon
W0#: 1B940 Lwiw: ^//C ^" ^
SITC: DomesUc Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # TT , 10 ft
Se — 7
PARAMETCRS
VolatUe Organics
METHOD
8260
DATE: 9'^''7^ -mA-E: BS& SAMPLER: F'-^
Thiokol Corporation RCRA FacUitv Investigation .,
W0#: 1B940 LWR#: £^^^ ^ ^
SITE: Domestic Wastewater Drainfields A, B,_and C
DESCRIPTION: SWMU #625; Grid # .-^ , 10 ft
73/11-(f^^ci':^!- )
-• •—
PARAMETERS METHOD •
Bis(2-ethyUiexyl)phthalate
Nitrobenzene
8270
8270
-DATC: 9'ZC-^T' TIME: &5'Pj SAMPLER: /""-O
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £//C5Z-
SFTC: Domestic Wastewater Drainfields A,_B, and C
DESCRIPTION: SWMU #625; Grid # -^ , 10 ft
PARAMETCRS
B, Cd, Cr, Ag, Pb
Mercurv
METHOD
6010
7470
, r»«Ti7. 9'2i'-9*r^ TTvnr. ^< ?o (SAMPI FRr F'L
Thiokol Corporation RCRA FacUitv Investigation
W0#: 1B940 LWR#: £://^T 2-
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRimON: SWMU #625; Rmse Blank Grid # __V , _yUt
PARAMETFRg
VolatUe Organics
METHOD
8260
DATE: Zc -'yi TIME: 9/^- SAMPLER: /^^^
Thiokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: ^//o<^Z-
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Rinse Blank Grid # D
PARAMETCRS
B, Cd, Cr, Ag, Pb
Mercurv
METHOD
6010
7470
9
/OW
DATC: S^'2c;-'^J' TIME: 9/L- SAMPLER: Fi^^
Thiokol CorporaUon RCRA FacUity Investigation
W0#: 1B940 LWR#: ^y/^i 2_
SITE: DomesUc Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; D«*S«M # 5^ , /O ft
/?in\e A?/^^ /<^
PARAMETCRS METHOD ""
Bis(2-ethyUiexyl)phthalate
Nitrobenzene
8270
8270
CL-
DATE: 9-i,c.^ -v r-TIME: 9rc. SAMPLER: r^^
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: ^/^CSiZ.
SITC: Domestic Wastewater Drainfields A, B. and C
DESCRIPTION: SWMU #625; Grid # 73,, S ft
PARAMETCRS
VolatUe Organics
METHOD
8260
DATC: 9'Zc-'rr , 9zo
ZC -- 1^
/hCi^'f' ^'ff' CJ,-t/\
TIME: 7 ^i-^ SAMPLER: F^
Thiokol Corporation RCRA Facility Investigation
WO#: 1B940 LWRj»: ^//jJ6' 2.
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # 7?, 5 ft
PARAMETCRS METHOD
f. rC< • C.'/\ 'J cind
-f irdc'^/
Bis(2-ethyUiexyl)phthalate
Nitrobenzene
8270
8270
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: C^/^S'^
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # 7/?, 5 ft
PARA.METCRS METHOD
B, Cd, Cr, Ag, Pb
Mercm-v
6010
7470
DATC: Q-?-Zc--9^ TIME : 9Z0 SAMPLER: r^:
10
J7^177^.
Tiiiokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: ^llOh^
SITC: Domestic Wastewater Dramfields A, B, and C
DESCRIPTION: SWMU #625; Grid # 77 , 10 ft
PARAMETCRS
^'olalUe Organics
METHOD
8260
-DATC: 9-2C''l7^ TIME: 9 Jf
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: .^//^S"Z.
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # / 7, 10 ft
SAMPLER: V^c-J
PARAMETCRS METHOD
7B.C7E1^...
fiAx ^ond
i^/Jj^^j? 'ifUll
al^jT ^Ji/i.
Bis(2-ethyUiexyI)phthalate
Nitrobenzene
8270
8270
DATE: ^-2t--5>'j TIME: ' -^ / SAMPLER: /^uj
Thiokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#: £-//0^2-
SITE: Domestic Wastewater Drainfields A. B, and C
DESCRIPTION: SWMU #625; Grid # 7r> , 10 ft
PARAMETCRS
B. Cd. Cr, Ag, Pb
Mercurv
METHOD
6010
7470
IIO
DATC: f'Zo-'/i TIME: / •-) / SAMPLER: F^
Thiokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: ^f/CS"1.
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: S\VMU #625; Grid # 7S , 5 ft
Be - /-z^
PARAMETCRS
VolatUe Organics
METHOD
8260
S///_ Jrj
'i^Pc-9x^ /C^t^l 1 . CAK«DI CD. {^ L*-'
Thiokol Corporation RCRA FacUitv Investigation i—^
W0#: 1B940 L\VR#: ^ // C T^^'S2.
STTE: Domestic Wastewater Drainfields A, JB^ and C
DESCRIPTION: SWMU #625; Grid # _7i_, 5 ft
PARAMETCRS METHOD
Bis(2-ethyUiexyl)phthalate
Nitrobenzene
8270
8270
DATC: ^-Zo-^'i TLME: IOC \ 7 SAMPLER: Fi^
• \ •/
•
Thiokol Corporation RCRA FacUity Investigation 1 1
W0#: 1B940 LWR(/: £//0^Z.
STTE: DomesUc Wastewater Drainfields A. B, and C
DESCRIPTION: SWMU #625; Grid # 7ST5 ft
PARAMETCRS METHOD
B, Cd, Cr, Ag, Pb 6010
Mercury 7470
— DATC: 9'ZO-9r TIME: Z^'/'"^SAMPLER: y^*
Thiokol Corporation RCRA Facility Investigation
A; J 5- W0#: 1B940 LWR#: £-//^.:S'2_ JZ^- zT //
STTE: Domestic Wastewater Drainfields A, B, and C ——
DESCRIPTION: SWMU #625; Grid # _ZSTi0 ft
PARAMETCRS METHOD ^ / // ^7F.d-
VolatUe Organics 8260 fy/UL J^.'^/'PL-
I
#
DATE: •^-ZL-^'^ TTME: /^^ J ^-S^iMPLER: /^ ^^
Thiokol Corporation RCRA Facility InvestigaUon
W0#: 1B940 LWR#: <£7/(0S""2-
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: S^VMU #625; Grid # 7^, 10 ft
PARAMETERS METHOD
Bis(2-ethyUiexyl)phthalate 8270
Nitrobenzene 8270
DATC: 9-Z<-- ' *?*? TIME: //? ? <r~ SAMPT FP- yC', _
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £//CSr2-
SITE: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: S>VMU #625; Grid # _7S"', 10 ft
PARAMETERS
B, Cd, Cr, Ag, Pb
Mercurv
MF:THOD
6010
7470
DATF. 9'7r-^<^ TIME: /^M'S SAMPLER: /=l<y'
Thiokol Corporation RCRA FacUitv Investigation
//2^, WO#: 1B940 LWR#: ^OC-S'1. O Q_ " Fi
SITC: Domestic Wastewater Drainfields A, B, and C .^—_.^ —
DESCRIPTION: SWMU #625; Grid # _2E:» 5 ft
PARAMETCRS MI:TH0D /l^t i^ '^i/f
VolatUe Organics 8260
DATEi^-^'f r'^ ^ miE^ _//2^_ SAMPLER: Fi^
Thiokol Corporation RCRA FacUity InvesUgation
W0#: 1B940 LWR#: £.IIOi
SITE: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; DUP Grid #^8 . _
PARAMETCRS
VolatUe Organics
METHOD
8260
DATC: 9'ZO-9r^ TIME: iize^ SAMPLER: FJ
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: <£'//<?S'Z—
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # 3&, 5 ft
PARAMETCRS METHOD
Bis(2-etbyUiexyl)phthalate
Nitrobenzene
8270
8270
DATC: ^-ZO-*fi TIME: J/Z^ SAMPLER: /c^
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWRJC: ^'/£^~
SITE: Domestic Wastewater Drainfields A. B. and C
DESCRIPTION: SWMU #625; Grid # .3R, 5 ft
PARAMETERS METHOD
M
B, Cd, Cr, Ag, Pb
Mercurv
6010
7470
l~2tO'9^ TIME: //-Z^ SAMPI FB- /^io DATC:
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: /T/Z^S'^-
SITE: Domestic Wastewater Drainfieliis A, B, and C
DESCRIPTION: SWMU #625; Grid # 3S . 10 ft
PARAMETCRS METHOD
Sc- io
VolatUe Organics 8260
DATE: 9-ZO''7S^ TIME: //4C SAMPLER: F^
Thiokol CorporaUon RCRA FacUity Investigation
W0#: 1B940 LWR#: £'//CS' Z.
SITC: Domestic Wastewater Drainfields A. B, and C
DESCRIPTION: SWMU #625; Grid # _^S> 10 ft
PARAMETCRS METHOD
Bis(2-ethyUiexyl)phthalate
Nitrobenzene
8270
8270
DATE:
0^^^7r:-^^7-'-
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^//^>irz.
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # 3^, 10 ft
13
PARAMETCRS
B, Cd, Cr, Ag, Pb
Mercury
METHOD
6010
7470
LlJSZ
.DATC: f-22 'fy TIME: //<2/J SAMPi FR.
Thiokol Corporation RCRA FacUity InvesUgation
W0#: 1B940 LWR#: S/tCiTZ.^
STTE: Domestic Wastewater Drainfields A, B, and C
DESCRffTION: SWMU #625; Grid # J^, , 5 ft
^J
-BC ^ C
^/t and hfu. Sg/tc/
PARAMETCRS
VolatUe Organics
METHOD
8260
DATC: 9 -10-'9S TIME/Vi SAMPLER: F^J
Tluokol Corporation RCRA FacUitv InvesUgation
W0#: 1B940 LWR#: <EV/d>S~2.
SITE: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMV #625; Grid # J^. s ft
PARAMETCRS
Bis(2-etbylhexyl)phthalate
Nitrobenzene
METHOD
8270
8270
DATE: l-ZO'9'!^ TTMC /.^/C ,..
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^IIOT'^-
SITE: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # J?U. 5 ft
PARAMETCRS
B. Cd, Cr, Ag, Pb
Mercurv
METHOD
6010
7470
4,^^^9<^ /?/f CAK mt I7n.
•
Thiokol Corporation RCRA FaciUty InvestigaUon
WO#: 1B940 LWR#: &/0rZ
^3 I <7^ SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # JCa , 10 ft
PARAMETCRS METHOD
VolatUe Organics 8260
'h^ - n
._._.. i5iii._^jii.
/it\ci Silt
DATE: f-Zo -f^j" TIME: JZ>Z^' SAMPLER: /=-u.J
14
•...-SMrm^^l:
Thiokol Corporation RCRA FacUitv InvestigaUon
WO#: 1B940 LWR#: £//0'S'Z.
STTE: DomesUc Wastewater Dramfields A, B, and C
DESCRHTION: SWMU #625; Grid # 2 (c. . 10 ft
PARAMETERS METHOD
Bis(2-ethyUiexyl)phthalate
Nitrobenzene
8270
8270
DATE: f'ZCyT TIME: ^'^C :^ CikotcD.
Thiokol CorporaUon RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/O'S'Z
SFTC: Domestic Wastewater Dramfields A, B, and C
DESCRIPTION: SWMU #625; Grid # J^. 10 ft
PARAMETERS
B. Cd, Cr, Ag, Pb
Merciu-v
METHOD
6010
7470
DATC: ^-^—ff^TIME: /^/^ SAMPLER: /W
Thiokol Corporation RCRA Facility Investigatioii
WO#: 1B940 LWR#: n/Z^'-S"^
SFTC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; DUP Grid # ?4J , /C) ft
PARAMETERS METHOD
Bis(2-cthyUiexyl)phthalate
Nitrobenzene
8270
8270
'S^L
DATC : 'r-ZC -9 f^ TIME: /^:Z SAMPLER -Ft u^
Thiokol Corporation RCRA FaciUty Investigation
r, • W0#: 1B940 LWR#: BUOS^Z
SFTC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # /6J , 5 ft
PARAMETCRS
VolatUe Organics
METHOD
8260
he = Zo
E/./u.__7S(±i}ji_
Qild S///-
-Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 L\VR#: £Z//OS'Z.
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # /09, 5 ft
c A xroi CD. /^t^
PARAMETCRS METHOD
Bis(2-ethyUiexyl)phthalate
Nitrobenzene
8270
8270
DATC: 9- ZO^fS^ TIME: I3S'0 SAMPLER:
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £//C£'2.
STTE: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # /39_, 5 ft
15
PARAMETCRS
B, Cd, Cr, Ag, Pb
Mercurv
METHOD
6010
7470
DATC: ^-Z0^9r~ TIME: /3S0 S/UVIPLER:
7:ftio*o/ CorporaUon RCRA FacUitv Investigation
W0#: 1B940 LWR#: &/O^Z.
t* tU
I•40'^ SFTC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # ZSf. 10 ft
PARAMETCRS
VolatUe Organics
B.CJL^J4'_
5/// a/:d
J^^^M
DATC: f-2e>'9<' TIMF- id.fi^T' SA VfOI CD. X^,.)
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: ^/(O^Z-
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # ^Bf, 10 ft
PARAMETCRS MIETHOD
Bis(2-ethyUie.vyl)phthalate
Nitrobenzene
8270
8270
DATE: 9'7j)-^<r TIME: l4t^ SAMPIFR;
Thiokol Corporation RCRA Facility Invesligation
W0#: 1B940 LWR#: £//CS"Z.
SITE: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # /Bt, 10 ft
fuJ
PARAMETERS METHOD
B, Cd, Cr, Ag, Pb
Mercurv
6010
7470
TIME: 14/)^ SMIPLER: >-/.-
lit'/.
DATF- 9-Za -9<i
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/CS'Z
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRHTION: SWMU #625; Grid # /4-7, s ft
PARAMETCRS
VolatUe Organics
METHOD
8260
BH ' r fi
JiOs/lu^//y_
^_S'c^-yL._st //__
DATE: 9-1.0 >r TIME: Mry SAMPLER: /^.-
16 77uo*o/ Corporation RCRA FacUity Investigation
W0#: IB940 LWR#: i^/'C'TZ,
SITE: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # /47. 5 ft
PARAMETCRS METHOD
Bis(2-ethyUiexyl)phthalate
Nitrobenzene
8270
8270
9- l,j ' 9< TIME: /4t 9 SAMPLER: l^"^ DATC:
Thiokol CorporaUon RCRA FaciUty Investigation
W0#: 1B940 LWR#: £llO "S Z.
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SVVMU #625; Grid # /f 7, 5 ft
PARAMETCRS
B, Cd, Cr, Ag, Pb
Mercurv
METHOD
6010
7470
JFS"/
T^KVL: ^'Z<^'9r TIME: I4-Z9 SAMPLER: A
Thiokol Corporation RCRA Facility Investigation
-"•^^ -won-. 1B940 Lwk#: EllO'it.
STTE: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # 141 . 10 ft
PARAMETCRS
VolatUe Organics
METHOD
8260
^LllJXZ^'^ .
DATC: ^'U^9<7 TIME: /f?9 SAMPLER: rL u^
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £11052.
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # /-f7.10 ft
PARAMETCRS METHOD
Bis(2-ethyUiexyl)phthalate
Nitrobenzene
8270
8270
-DATC: 9'2^''9r~ TIME: /45,^ SAMPLER: ,^^C'
Thiokol Corporarion RCRA Facility Investigation
W0#: 1B940 LWR#: f//(?.S"Z^
SITC: DomesUc Wastewater Dramfields A, B, and C
DESCRIPTION: SWMU #625; Grid # /-f 7 ' ^0 ft
PARAMETCRS METHOD
B, Cd, Cr, Ag, Pb
Mercurv
6010
7470
• i-v
Vi
}7i'i/>7i^/cS fl^l/iy^tf'c/ /7 /i/-t:^2 /ohc'^i.i D f,
'lix Q<ilL/.rl B-]ai- iV \)cs.--^<h\c {u<i AfV cLelvdci
Ona MCvg-S0.ft^^2 p(g^ iJiaK\ /.\c>\Ar..H- "^'-^ LU b:«-_
-B)
rt_
XtLi^ JlA, ^ L. •htA<^ T -V^ CiW.
'g^^>.\,^pVU^^ t;t^
te^
q-i-T- QC
g nd l.k'tti»t\ •^^
Thiokol CorporaUon RCRA Facility Investigation
W0#: 1B940 Lmttl: ^//C S /
SITE: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # -4-f', , 5 ft EL -: ^._.
PARAMETCRS
VolatUe Organics
METHOD
8260
^/// - A iili I
.J)ATC: / -z<r-vr TIME: f^^^ SAMPLER: ri..^^
Thiokol CorporaUon RCRA Facility Investigation
WO#: 1B940 LWR#: <t /'^C '^'^
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRUnON: SWMU #625; Grid # 4^., 5 ft
PARAMETCRS METHOD
Bi$(2-ethyUiexyl)phthalate
Nitrobenzene
8270
8270
-DATC: /''Zs -^ r^ TIME: L.^-L SAMPLER: fw^
Thiokol Corporation RCRA FacUitv Investigation
W0#: 1B940 LWR#: .<£//t.S '/
STTE: DomesUc Wastewater Drainfields A. B, and C
DESCRHTION: SWMU #625; Grid # ^^ , 5 ft
PARAMETCRS
B, Cd, Cr, Ag, Pb
Mercury
AfETHOD
6010
7470
y-7c-<^rr ^zZ. SAMPLER- ^ yi.<^
18
e:>^
.K-:-^W^m
-Thiokol Corporation RCRA FaciUty Investigation
WO#: IB940 LWR#: £//Cj''/
STTE: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # 4f: . 10 ft t>C'/L
PARAMETCRS
VolatUe Organics
METHOD
8260 JlLtS/. '^'1/
Jk/lcJ 4 u^ -^fiJic/
DATC: /-I -'-f^ TIME: SAMPLER: f^
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: EllC^'i
STTE: Domestic Wastewater Dramfields A, B, and C
DESCRIPTION: SWMU #625; Grid # -ffc, 10 ft
PARAMETCRS METHOD
Bis(2-ethyUiexyl)phthalate 8270
Nitrobenzene 8270
DATC: T'l^''7':> -TTSTEC"'j S SAMPLER:
Thiokol Corporation RCRA Facilitv Investigation
W0#: 1B940 L\VR#: c"//^ J'/
STTC: DomesUc Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # ^fc, 10 ft
PARAMETCRS METHOD
B, Cd, Cr, Ag, Pb 6010
Mercurv 7470
^1 L.i^
DATC: / ' r ^ 5 TIME:. SAMPLER: /-
- Thiokol Corporation RCRA FacUity InvestigaUon
j<^ VtOH: 1B940 LWR#: dry/Cli >'
SITE: DomesUc Wastewater Dramfields A^ B, and C
DESCRIPTION: SVVTVIU #625; Grid # cr'r , 5 ft
PARAMETCRS
VolatUe Organics
METHOD
8260
.3^-.17.
Ly/.'d ...^.'^^.iZ-
77iio*o/ Corporation RCRA FacUity Investigation^^
W0#: 1B940 LWR#: iZ'^^^-^ ^
SITC: Domestic Wastewater Dramfields A. B, and C
DESCRIPTION: SWMU #625; Grid # jtsl' 5 ^
PARAMETCRS METHOD
Bis(2-ethyUiexyl)phthalate
Nitrobenzene
8270
8270
Thiokol Corporation RCRA Facility InvesUgation
W0#: 1B940 . LWR#: ^//dy
SITE: DomesUc Wastewater Dramfields A^Bj and C
DESCRIPTION: SWMU #625; Grid # _^2, 5 ft
19
PARAMETCRS
B. Cd, Cr, Ag, Pb
Mercury
METHOD
6010
7470
/OO'
DATC: V'-/S "TC TIME: Y/^ .SAMPLER: /I'^^^.y'
Thiokol Corporation RCRA FacUity Investigation
W0#: IB940 LWR#: ^ir'y/'c. ^V
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # _F^, 10 ft
PARAMETCRS METHOD
VolatUe Organics 8260
:g.4._£_^__
^'^'U 'TXI/id __
/•
DATC: / '/>-?-• ^C TIME : /Coc SAMPLER: rc
Thiokol Corporation RCRA FaciUty InvestigaUon
W0#: 1B940 LWR#: ^i=//<i: j"^'
SFFE: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # /T^^-. 10 ft
METHOD PARAMETERS
Bis(2-ethyUiexyl)phthalate
Nitrobenzene
8270
8270
DATE: V - 7 \' •'^ ^ TIME: /I'i/J Si^AlPLER: F <-<y
Thiokol Corporation RCRA FacUity InvesUgation
W0#: 1B940 LWR#: ^^T/yC^'^
SITE: Domestic Wastewater Drainfields A. B. and C
DESCRIPTION: SWMU #625; Grid # p-7 , 10 ft
PARAMETCRS METHOD
B, Cd, Cr, Ag, Pb
Mercurv
6010
7470
//'{i-
DATC: '^- Z r r PTIME: /C'/IO SAMPLER:
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £//£ ^'^
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # /2*?, 5 ft DC /^
PARAMETCRS
VolatUe Orgamcs
METHOD
8260
'30/'d ^rVid ^?pLr^ f
DATE: 9-Z T ' ''7 C TIME: /^H-O SAMPLER: /"u--'
</<^ .:.., '!;.-7-<^jimmy>^
20 Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^^/L.-<ry-
STTE: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid tl /Z^, 5 ft
PARAMETCRS METHOD
Bis(2-ethyUiexyl)phthalate
Nitrobenzene 8270
8270
- y-jr-^r DATE: T-JY-rS TIME: //;</.'
Thiokol CorporaUon RCRA FacUity Investigation
W0#: 1B940 LWR#: ^//O'i.'T
SITC: DomesUc Wastewater Dramfields A, B, and C
DESCRIPTION: SWMU #625; Grid # /Zh. 5 ft
CA Il4^nT trr*. /^,.
- -
/C'J^
I
PARAMETCRS
B, Cd, Cr, Ag, Pb
Mercury
METHOD
6010
7470
DATC: 9-zr'^<r' TIME: /CfC SAMPLER: r^
Thiokol CorporaUon RCRA FacUitv Investigation
WO#; 1B940 LWR#: j£//C- \'^
STTE: DomesUc Wastewater Drainfields A, B, and C
DESCRIPTION: S\VMU #625; Grid # ZZ±L< 10 ft
__BC '_Z:^
PARAMETCRS
VolatUe Organics
METHOD
8260
.^F^""^/... J/Fc/ 72t]rJ_^
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 L\VR#: C-//CS>^
SITC: Domestic Wastewater Dramfields A. B. and C
DESCRIPTION: SWMU #625; Grid # /^fc', 10 ft
C. J
PARAMETCRS
Bis(2-etbyUiexyl)phthalate
NUrobenzene
.METHOD
8270
8270
DATF.: 'f'Z'^-^C T..\IE: /^i C SAAffLER:
Thiokol Corporation RCRA Facilit)' Investigation
W0#: 1B940 LV^TJ*: B/'C'^^
SFTC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: S\VMU #625; Grid # jZYJ , 10 ft
H^
PARA.METERS
B, Cd, Cr, Ag, Pb
Mercurv
METHOD
6010
7470
HH
Thiokol CorporaUon RCRA FacUity Investigation
W0#: 1B940 LWR#: ^//OS^
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # _lt^, 5 ft
21
n<-' g
PARAMETCRS
VolatUe Organics
METHOD
8260 MZlF^t :s,Z:Z
DATF. 9-z<r^r TIME: /IZ4-SAMPLER: /^Z>-^
Thiokol Corporation RCRA FacUitv InvesUgaUon
W0#: 1B940 LWR#: i^/f^T^
STTE: Domestic Wastewater Drainfields A, B^and C
DESCRIPTION: SWMU #625; Grid # IZS , 5 ft
PARAMETERS METHOD
Bis(2-ethyUiexyl)phthalate
Nitrobenzene 8270
8270
-DATC: 9-2S -9C TIME: 7/Z^ SAMPLER: /X-
Tldokol Corporation RCRA FacUitv Investigation
W0#: 1B940 LWR#: ^f{C T^
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRHTION: SWMU #625; Grid # / Z^S ft
PARAMETCRS METHOD
B, Cd, Cr, Ag, Pb 6010
Mercury 7479
DATC: ^.2 --TIME: IIZ 4 SA^^>LER: j:.
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: ^./fCS^
jj "1 e— SITC: Domestic Wastewater Drainfields A, Bjjnd C
-^ DESCRIPTION: SWTVIU #625; Grid tt /ZS , 10 ft
PARAMETCRS
VolatUe Organics
METHOD
8260
3cj^J7U
S/-/- /{/V/X ^^"HL
C/^ tin d z>c: n J "f
-fl
M,
1.
DATE: '"/"/'>"'• /"S TTME: //3"^ SAMPI FR- /L<-^
Thiokol Corporation RCRA F-cUity InvestigaUon ,^
W0#: 1B940 LWR#: i^/fC^'l
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWAIU #625; Grid # /2<."^10 ft
PARAMETCRS METHOD
Bis(2-ethyUiexyl)phthalate
Nitrobenzene
8270
8270
^'- 1(7 DATC: ' IS •^/5^TI> TIME: / /3S SAMPLER : f^
22
'- f:
Thiokol Corporation RCRA Facility Investigation
W0#: IB940 LWR#: ^//C><:'9
STTE: Domestic Wastewater DraiiUlelds A, B, and C
DESCRIPTION: SWMU #625; Grid tt /LS , 10 ft
PARAMETCRS
B, Cd, Cr, Ag, Pb
Mercury
METHOD
6010
7470
DATC: 9-1^^1^ TIME: //5.5^ SAMPLER: Pu^
Thiokol Corporation RCRA FaciUtv Investigation
WO#: 1B940 LWR#: B/'/'Sf
SFTC: DomesUc Wastewater Drainfields A. B, and C
DESCRIPTION: SWMU #625; Grid # Z/f, 5 ft
JBc.HL_^J-__
PARAMETCRS
VolatUe Organics
METHOD
8260
nA-TF- 7'F^ ^ f- i TTMF- //.T<^ SAMPt FU-
Thiokol Corporation RCRA Facilitv Investigation
WO#: 1B940 LWR#: ^//C'S*/
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # 2/9 , 5 ft
/L
—
—
—
3^
._
PARAMETCRS METHOD
Bis(2-ethyUiexyl)phthalate
NUrobenzene
8270
8270
DATF- 9' 7. r-9 F TTMF-// <C<1
Thiokol Corporation RCRA FacUitv Investigation
W0#: 1B940 LWR#: £'//C^/
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRHTION: SWMU #625; Grid # 2^/ /*, 5 ft
SAMPT FR-F-^
PARAMETCRS
B, Cd, Cr, Ag, Pb
Mercun
METHOD
6010
7470
\U •L
_ HATF-9'. T^'^7' TT\fF-// Tci-SA\fPIFR ./>
Thiokol Corporation RCRA FacUitv Investigation
W0#: 1B940 L\VR#: S//C>S9
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: S\\AIU #625: Grid # Z/'j • 10 ft
PARAMETCRS
VolatUe Organics
METHOD
8260
'^-2T'9r
. Bc^.J2^. -__
Thiokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#: ^//^'S^
SITC: Domestic Wastewater Draiiifields A, B, and C 23
DESCRIPTION: SWMV #625; Grid # _^ V^, 10 ft
PARAMETCRS
Bis(2-ethyUiexyl)phthalate
Nitrobenzene
METHOD
8270
8270
-DATC: 9-2'^'-'^! 7~ TIME: A "^ *^ SAMPLER: /'(>-'''
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: £7/^^
STTE: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # 2''^/, 10 ft
PARAMETERS
B, Cd, Cr, Ag, Pb
Mercury
METTIOD
6010
7470
J)ATC: FZS --9<^ TIME: IZC> '^ SAMPLER:
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: i^Z/CJ^/
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; DUP Grid # Z/'/ , /Q ft
Fu^
PARAMETCRS
VolatUe Orgaiucs
METHOD
8260
. DATE: / " 2 S - 9 F" TIME: / "ZO e_SAM:PLER: FL 'Ls,-/
LZ/c ld>rii:\^. A. Ounc U
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: E/fOS^"
SITE: Domestic Wastewater Drainfields K, B, and C
DESCRHTION: SWMU #625; Grid # ^C C 5 ft
PARAMETERS
VolatUe Orgaiucs
METHOD
8260
5^^ /
(a?
nvu 'Sand Q/(.d
^il4
_DATC: 5-:v-^s' TIME: /XFy SAMPLER: ^
i
24 Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#; £//0'C9
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # ^cY,, 5 ft
PARAMETCRS METHOD
'pi^^m^^i}\
Bis(2-ethyUiexyl)phthalate
Nitrobenzene
8270
8270
rvAxc. Q. r><::-Q< TTME: /3 1?5''''SAMPLER:
Thiokol Corporation RCRA FacUitv InvestigaUon
W0#: 1B940 LWR#: cl/OS'y
SITC: DomesUc Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # 2£k.' 5 ft
PARAMETCRS
B, Cd, Cr, Ag, Pb
Mercurv
METHOD
6010
7470
DATC •: 7-- 7.S ' ^lc7 TIME: /JjT SANCLER: f"^
I7^^c /C/: f< Slo/I <3, iJii (lyc Ard /^-//^^-^.c^ ::so/up///,-<^ <rF'_
ZLh ._ji^c^ [gh I5
Thiokol Corporation RCRA FacUitv InvesUgation
W0#: IB940 LWR#: ^//CSZ.
STTE: Domestic Wastewater Drainfields A, B, and C
DESCRHTION: SWMU #625; Rinse Blank Grid # ^><^ , 6 ft
PARAMETCRS
B, Cd, Cr, Ag, Pb
Mercun'
METHOD
6010
7470
DATC: ,'^1'1^-9 7 .^^. 13 fc SAMPLER: FiF
'S94C ^^^ cz//^-^/
177/^fyc F/Ci/L
)Ci;Vc he^/i^
^'L-r-^iF / 5 <^' A
•
I7>S-F
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: ^1 Ic^
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # 20 U 10 ft
PARAMETERS
VolatUe Organics
METHOD
8260
DATE : 'f't^'K' TIME: IBS-F, SAMPLER: FJ
Thiokol CorporaUon RCRA FaciUty Investigation
W0#: 1B940 LWR#: ^HCFf
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # 2.0i^ , 10 ft
PARAMETCRS
Bis(2-etbylhexyl)phthalate
Nitrobenzene
METHOD
8270
8270
DATC: ^'"^ is-'^ir TIME: /jTr.
25
Be- 7
CjlM--Uni7L,
of Ufp<: r
itfi'<^i ^ f
/o'' '^0/u.p lx,_
SAMPLER: r..j
Thiokol Corporation RCRA FacUity Invesligation
W0#: 1B940 LWR#: ^HL'^Tf
SITE: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # :^'C , 10 ft
•
PARAMETERS
B, Cd, Cr, Ag, Pb
Mercury
METHOD
6010
7470
_pATC: ']'VS'H'^ TIME: /JST^SAMDPLER: ^^
l/LjP' Thiokol Corporation RCRA FaciUty Investigation
ITIJ- W0#: IB940 LWR#: l^//CTf
SITE: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # 9u., S ft
3C_^JF.
PARAMETCRS
VolatUe Organics
METTIOD
8260
DATE: 9-7^-9^^ TTMF. /4JD
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: £71(^^9
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # 9ia . 5 ft
C A K4DT cn. AL
PARAMETCRS METHOD
Bis(2-ethyUiexyl)phthalate
Nitrobenzene
8270
8270
DATE: 9- -i-r- 97 TIME: /^lO SAMPLER: fU
26 Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: /f=//i? S^9
SITC: Domestic Wastewater Drainfields A, B. and C
DESCRIPTION: SWMU #625; DUP Grid # 96. 5ft
PARAMETCRS METHOD
Bis(2-ethyUiexyl)phthalate
Nitrobenzene
8270
8270
DATE: 7-/'7-fS TIME : 14^0 SAMPLER: Tc
Thiokol Corporation RCRA Facility Investigation
WO#: 1B940 LWR#: £//OS9
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # _£^, 5 ft
PARAMETCRS
B, Cd, Cr, Ag, Pb
Mercurv
METHOD
6010
7470
DATC: '7'zr-9r TIME: J4/0 SAMPLER:
l^X .Jkidi'.auhjL -AF^ l/lcl\ ....^c^<Z£>f>^ rJ___a_ __py_/L/fc/ii.
J^ci^ /"^^ ro /in^-j ^.i^r^'^/tik.<c/^^.^/2/yip/c s if.
.F^F^'^"^^.
.^^6.^^_
J0O ^/n*/tu/y/^at dreuy .J/acL -/>i^ .^/^^Z^z.^i^aut^Atut'/
li^ l7)M/ui__^__Sr7j__JI_FC, •tf
(Cif-
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: ^//^Jf^(fZ-.
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # 9L: , 10 ft
PARAMETCRS
VolatUe Organics
DATE: 9-z^'9r TIME:
METHOD
8260
SAMPLER: /^^
..?6-_._;. z^
F/:^_, C)di^cl
0f-/C^^'^r /e,rc/
•
-Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^£y/<3-S=^ 0
STTE: DomesUc Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # ?6.10 ft
•2^ 27
PARAMETCRS METHOD
Bis(2-ethylhexyl)phthalate
Nitrobenzene
8270
8270
f'Z^-fr /s~/<^ SAMPLER: DATE: /'^-^ ^ ' y TIME:
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: £^//OCr'Z-
SITC: Domestic Wastewater Drainfields A. B, and C
DESCRIPTION: SWMU #625; DUP Grid # ^ , /^ ft
>^..0
PARAMETCRS
Bis(2-ethyUiexyl)phthalate
Nitrobenzene
METHOD
8270
8270
-DATE: 9''Z/i3 — ^F' TIME: /S/O SAMPLER:
Thiokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: ^//C P^ C» 2_
SITC: Domestic Wastewater Drainfieliis A, B, and C
DESCRIPTION: S\VMU #625; Grid # 9^, 10 ft
FZy
PARAMETCRS
B, Cd, Cr, Ag, Pb
Mercurv
METHOD
6010
7470
DATC : 9-Z^^ fr'-rmF.. /.S /^ SA\.n>TFD. F^
Thiokol Corporation RCRA FacUity Investigation ^
I r-2 <r' W0#: 1B940 LWR#: ^//CCZ
/ -^ -^ _— SITE: Domestic Wastewater Drainfields A, B, and C if- . S ft
— ;/1
DESCRIPTION: SWMU #625; Grid #
PARAMETERS
VolatUe Organics
METHOD
8260
^///- ^-//z:v
f 'MiZU-
C,^ 7 <r: .- ™„. ,^5^ CAA«PI FD-r. (..^
Thiokol Corporation RCRA FaciUty Investigation
WOiC: 1B940 LWR#: £'//Ci' 'Z
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # /4- , 5 ft
PARAMETCRS METHOD
Bis(2-ethyUiexyl)phthalate
Nitrobenzene
8270
8270
(T? DATE: j-2L- l^ TIME: / ^JT": SAMPLER: Fi^
ligation
f^WR#: i^//CG 2^
r^ewater Drainfields A, B, and C
HPTION: SWMU #625; Grid # /^ , 5 ft
PARAMETERS
B, Cd, Cr, Ag, Pb
Mercun'
METHOD
6010
7470
._DATC: 9-26 -ff TIME: /^ -^ J SAMPI.FR
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWRjf: (^//C ^ Z.~~
SITE: DomesUc Wastewater Drainfields A, B, and C
DESCRHTION: SWMU #625; DUP Grid # /^ , 5 ft
FuJ
PARAMETCRS
B, Cd, Cr, Ag, Pb
Mercurv
METHOD
6010
7470
— DATC: 9-ZL -ft^ TIME: 1^3 T SAMPLER: F^
Thiokol CorporaUon RCRA FaciUty Investigation
'^77^^ W0#: 1B940 LWR#: ^jlC 6 Z-
FFJJ SFTC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625: Grid # /•4- ,
PARAMETERS
VolatUe Organics
, 10 ft
METHOD
8260
'Bc^F^
ZuLi^f -^ilf
_DATE: ^-2U ' 9i TLME: ih.4-F SAMPLER: Z^ij^
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^UCC' L^
SITE: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # /4- , 10 ft
PARAMETERS METHOD
Bis(2-ethyUiexyl)phthalate
Nitrobenzene
8270
8270
H-IU-^C ,nATF. 7'/../^;"VC. TIMF
Thiokol Corporation RCRA FacUir.- Investigation
W0#: 1B940 LWR#: C-l ii'iii Z-
SITC: Domestic Wastewater Drainfields A, B, and C
DESCRIPTION: SWMU #625; Grid # 14- , 10 ft
/ ^74 "! S A MPI FR - F^
PARAMETCRS
B. Cd. Cr, Ag, Pb
Mercurv
Jf
METHOD
6010
7470
DATC: 9-Zu 9] TIME: /^F SAMPLER: f^
29
U-L.
7 27- 9<>'
jLimiJujjJiMlL CirtK. di/ii'/ Ot rAiilCl T/ry/!y\rr
iZi^ /7 Z4-/Z>0 TV. t^kc(n\ dlrun 4 7rTL pF'cIS (J/I-J CJCV.-^.J^ ^/rlu'i^n ^r.-.rk: 1^ A-S4i /z
. ClJi^Jlucl UIJCC^I ULU. k d^^t-.-t'il
MF777 7£±MA CLL^^- drj^<JdL-^ Zizldl 5/v/^<c -^J- Z9\'
Thiokol Corporation RCRA FacUity Investigation
^ , W0#: 1B940 LWR#: d/ICi^.'Z
I. ^ f C SITE: M-348 Subsurface Discharge
DESCRIPTION: SWMU #395; rt-d Depth
u p^vc
PARAMETCRS
Antimony
Arsenic
Chromium
Lead
Sulfate
pH
DATC: V • 2 7-9r TIME:
METHOD
6010
6010
6010
6010
300
9045
F9C i
Thiokol CorporaUon RCRA FacUity InvesUgation
W0#: 1B940 LWR#: ^///^ Z-
STTE: M-348 Subsurface Discbarge
DESCRIPTION: SWMU #395; 71' Depth
PARAMETCRS
Antimony
Arsenic
Chromium
Lead
Sulfate
pH
METHOD
6010
6010
6010
6010
300
9045
DATC: 9-Z7-9r TIME : FS'O SA^O»LER: FuZ
RL,-- iZ.
^Z)/l I (7,./1J i^tjUJi I
^c- 5" JS
j£i^—c/^
^7j
7PJILI /ic r ru/]/i/.^^, yy i^er^ ouxi/l -
iruH-
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Bk'/i ICs CZl Id c /dd 4ti ei'^t F^/JL c/gcc,^ //;fi<L_^ ^ ,
[pcidL /LJ^ 'jf^ ^-CLL-^OA<P-ICA Z^ - Vo A'J>
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#:
SITC: M-72 Septic Drainfield
DESCRIPTION: S\\'MU #630; Rinse Blank Grid # X.
PARAMETCRS .METHOD
.-JCLU
As, Be, Cd, Cr, Cu,
Pb, Ni. Tl, Zn 6010
n " DATC: ^-^7-97 TIME: //-S'S'" SXMPLEK: Ac>
30
_//^3
Thiokol Corporation RCRA FacUitv Investigation
W0#: 1B940 LWR#: EllOf^ 2.
SITC: M-72 Septic Drainfield
DESCRHTION: SWMU #630; Grid # 3 I , S ft
PARAMETCRS
VolatUe Organics
METHOD
8260
DATC: 'j-Zl'^f TIME: IIC 3 SAMPLER: FuJ
Thiokol CorporaUon RCRA FacUitv Investigation
W0#: 1B940 LWR#: £llC t2-
SITE: .M-72 Septic Drainfield
DESCRHTION: SWMU #630; Grid # "Vl , 5 ft
PARAMETCRS
As, Be, Cd, Cr, Cu,
Pb, Ni, TT, Zn
METHOD
6010
Be - dc
^-Tf-_Zz^/-
/
•
-diyait LUFFS.
^aZicl Ond
rci',.^1.
DATC: 9-2 7-•^i^ TIME: 1103 SAAn>LER: /=U_.
dd-Ti' . FUtiiCi' reffx^ji fc. 0/di.'once. b<:r/coo FF_ ^ ^^'^~
±o_a JjZU u^^Z7CZti.m C/pprcxMQJcJ^. 5_ F^^J^^^j^c
/)/ r'-l y/ -7/ Zl.r... CU,r^r...-. CLi -^ iA. IL^
CMC/ZTJ:
ibtA 0^5^.
c/^^JZl
L<i.»: _^r^c/.._^_2j:-
7^/0*0/ Corporation RCRA FacUitv InvestigaUon
W0#: 1B940 LWR#: £-(10 t 7
SITC: M-72 Septic Drainfield
DESCRIPTION: S\\'MU #630; Grid # Z7, 5 ft
PARAMETCRS
VolatUe Organics
METHOD
8260
DATC: FZ7'9^ TIMF.: / ZJ C
Thiokol Corporation RCRA FacUitv Investigation
W0#: 1B940 LWR#: ^//CG Z.
SITE: M-72 Septic Drainfield
DESCRHTION: S\\^IU #630; Grid # 27 , 5 ft
SAMPI FD . F^
PARAMETCRS
As, Be. Cd, Cr, Cu,
Pb, Ni, Tl. Zn
METHOD
6010
DATC, : 9-Z7-9r TIME: / • SAAffLER:
Thiokol Corporation RCRA FaciUty Investigation
WO*: 1B940 LWR#; ^//0(pZ^
SITC: M-72 Septic Drainfield
/ 1777\ DESCRIPTION: SWMU #630; Grid # Z'Z- 10 ft
PARAMETERS
VolatUe Organics
METHOD
8260
DATC: 7 ' Z 7- 9F TIME: /Z'Zi 3 SAMPLER: F^Z
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: p^t/QOfZ-
STTE: M-72 Septic Drainfield
DESCRIPTION: SWMU #630; Grid # 'Zf, 10 ft
PARAMETERS
As, Be, Cd, Cr, Cu,
Pb, Ni, Tl, Zn
METHOD
6010
31
•RC - /oo/iF' .
l^inj fdrd Q6mc
Sc?iid O/I J
-9^
0 /
FJIFJ.1 LUjdk-
Fed FI4oM^<)-—
C0/C/ifl(y>
DATC: i-21 '9F TIME: / 2 ? J SAMPLER: /^L
lM^_^.CF.j571_^ff<L^^on._J.MAcA-JS,r^C^
Thiokol CorporaUon RCRA FacUitv InvesUgaUon
W0#: 1B940 LWR#:
_/J3 2S. STTE: M-72 Septic Drainfield
DESCRIPTION: S\VMU #630; Grid #
PARAMETCRS
VolatUe Organics
3 .5 ft
METHOD
8260
7?<i- ^^
^/ff z/L/,rk
fi^iJL San £
DATE : 9' ZT'9'^ TIME: /!-> J SAMPLER: F^l-U
Thiokol CorporaUon RCRA FacUitv Investigation
W0#: 1B940 LWR#: ^//(^X^'Z-.
SITC: M-72 Septic Drainfield
DESCRIPTION: S\\'MU #630; Grid # 3 . 6 ft "D UT*
PARA.METCRS
Volatile Organics
METHOD
8260
DATE: 9-Z1-7 T TIME: /llF SAMPLER: F^.^
3C 32 J»o*o/Conxiration RCRA FacUJy^lnvestigation
SITC: M-72 Septic Drainfield
DESCRIPTION: SWMU #630; Grid # _3 , 5 f,
As. Be, Cd, Cr, Cu,
Pb. Ni, TI, Zn 6010
DATC: 9- z 7-FF-,
mt
TIME: /-3rS> SAMPLER.
77i/o*o/ Corporation RCRA FacUitv Investigation
W0#: 1B940 LWR#: ^//^.^,p
SFTC: M-72 Septic Drainfield
DESCRHTION: SWMU #630; Grid # 3 10 ft
J^ J
PARAMETCRS
VolatUe Organics
METHOD
8260
;: 9-Z7-^« DATC: V-ZZ-^'C—TIME: 14/]^^ SA^fP, FR.
Thiokol Corporation RCRA FacUitv Investigation
W0#: 1B940 L\VR#: <^//^: £; 2_
SITC: M-72 Septic Dramfield
DESCRIPTION: SWMU #630; Grid # _3_. 10 ft
FU
PARA.METCRS
As, Be, Cd, Cr, Cu,
Pb, Ni, TT, Zn
METHOD
6010
DATC: 9-Z7-97— TRIE: /^g SAAn>LER: /S-
-_ Thiokol Corporation RCRA FacUitv Investigation
l^-^'l W0#: 1B940 L\VR#: EJ/OC:Z'
--'- '- SITC: .M-72 Septic Drainfield
DESCRIPTION: SWAIL' #630; Grid # 3^ 5 ft
PARA.METCRS
VolatUe Organics
.METHOD
8260
l/L-r 7
p.-rr-. O. W C.< n*-'
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 L\VR#: ^//<^6 2-
SITC: M-72 Septic Dramfield ^^
DESCRIPTION: S^^•ML' #630; Grid # t) , 5 ft
•%c-
F'cd
Find
/zzz/A
5/// n--^
3c
^ttC^
luFix
-(I
'cf C/uci
'\ //
Zl/7d O/nod/
FF zd Upp€r
/e^d/
PARAMETCRS
As, Be, Cd, Cr, Cu.
Pb, Ni, Tl, Zn
METHOD
6010
DATC •- 9'27- f^^^TIME: /4"2^ SAMPLER: fuy
wm
•
77iio*o/ Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^//(^z (^ 2-
SITC: M-72 Septic DrainfieW ^
DESCRIPTION: SWMU #630; Grid # f> , ~i ft
PARAMETCRS
As, Be, Cd, Cr, Cu,
Pb, Ni, Tl, Zn
METHOD
6010
DuP
33
mi
DATC : f'Z7-9r TIME •.mi SAMPLER: FuJ
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: c'lOi^Z.
SITC: M-72 Septic Drainfield ^^-
DESCRIPTION: S\\'MU #630; Grid # 5 , 10 ft
PARAMETCRS
VolatUe Organics
METHOD
8260
3C__^_.
HATF- ^- 2 7-'^7<r TIME: I44X^ SAMPLER: f'
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: F^JOh'Z—
SITC: M-72 Septic Drainfield
DESCRIPTION: SWMU #630; Grid # ^ ,10 ft
PARAMETCRS
As, Be, Cd, Cr, Cu,
Pb, Ni, TT, Zn
METHOD
6010
DATC : J-ZZ-f^ TIME: /FTC SAMPLER: F^"^
FTP/I lp k S c/cr // t^V r^ rl -fr-. Zd - F^ /o/j^.-'ci^r:
'E^:j.cju<z.d ^y lyrA^ii filh" A(- 71 /z\^-- er
ddd7tZs .-^-/a/d
^.MA ~/) /^L Cli hnu^c d ^Di^i'c -hL^\ i ferl_t^<___olc^_
•
•z*:^>,*/<:^if:^m
34
IIH^ ^/7 5tF nit. AF.7d.pjiF^S.
~ IIZF
.^.XleCi}:-_Cld._^
Hy. Osii v_ .^Iri ^ Jii_3..(
Thiokol Corporation RCRA FacUity Investigation
W0#: IB940 LWR#: £V/<f6 3
SFTC: M-71 Septic Drainfield
DESCRIPTION: SWMU #646; Grid # 3 j , S ft
PARAMETCRS
VolatUe Organics
METHOD
8260
FiiLf/UU 9^^4Zc^
.(.2Fl___F^:///aciJlf
3CF_..(^_ .
._ZZiCj'^F.-...c/arK
^^•S^F: ..c7/?J Q/oi.
DATC: 9-Ze-97^ TIME: .//zv SAMPT FR-
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: S//Z)i^3
STTE: M-71 Septic Dramfield
DESCRIPTION: S\\'MU #646; Grid # 3 \ , 5 ft
PARAMETERS
Be
Mercun'
pH
METHOD
6010
7470
FL^
DATC: 9-Zfi-9S TIME://<^S SAMPLER: Fi^
Thiokol Corporation RCRA FacUitv Investigation
,,-, . WO#: 1B940 LWR#: a/fC(^Z
IJ ^^ SFTC: M-71 Septic Drainfield
DESCRIPTION: SWMU #646; Grid # 1 I , 10 ft
" r-<1
PARAMETCRS
VolatUe Organics
METHOD
8260
o"v.// FFiJ..
_<^-'rcVi ._n'CjF
—-- (J- --
DATC: .9-Ze •97~ TTSXE: 11 3 S^SANffLER: F^
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^'//^'^J
SITC: M-71 Septic Drainfield
DESCRIPTION: SW^K: tt(A(,; Grid # 3 / , 10 ft
PARAMETCRS
Be
Mercun-
pH
METHOD
6010
7470
DATC: 9-Zi::-9\ TIME: i I Z'd SAMPLER:
•
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: <5//^'6j
^ SFFE: M-71 Septic Drainfield s3-c,! -£0
IjSTi DESCRIPTION: S^VMU #646; Grid # ^frS fl
PARAMETERS
VolatUe Organics
DATC: 9'ie '^'J'
METHOD
8260
TIME: IIFF SAMPI F.R: /--''
Thiokol CorporaUon RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: £//^/-> ^
STTE: M-71 Septic Drainfield
DESCRIPTION: SWMU #646; Grid # 3? , 5 ft
PARAMETCRS
Be
Mercurv
pH
METHOD
6010
7470
DATF.: . 7~2-^- / J TTMF- , ,// .^ ^ CAMPI FP.
Thiokol Corporation RCRA FaciUty Investigation
- r rT' W0#: 1B940 LWR#: E//C- 0 J
^^..J... SITC: M-71 Septic Drainfield
DESCRIPTION: S\niU #646; Grid # 3/ . 10 ft ^
PARAMETCRS
VolatUe Organics
METHOD
8260
^ Xi\TE:9'Z€>'i F TTS^: / ZO\ SAVtPl.F.H- F\J
77uo*o/ Corporation RCRA Facility InvestigaUon
W0#: IB940 LWR#: Izl/C l^2>
SITE: M-71 Septic Drainfield _
DESCRIPTION: S>A'MU #646; Grid # J>J . 10 ft
PARAMETCRS
Be
Mercurv
— pH
METHOD
6010
7470
li\TE:9'Z'7^-9S TlME:lZO:> SAMPLER: f"^'
35
Ec^ e
bl'fi.uA 3i|f-
J3<-3__Z(
miLic.^iZd...
A F v^^g-r FcpF\
F:^.F5Cf/l[plC to
at A[^^ .//cMv
^LiJ/iT^^- ^'^.^ IX.
%
. J2;>^c/s ci/:J___jF':ou/iF F<^p^cFc.cJ 7fe„ Ff /< I'L to
^__7^:::/K_ _Fp^SJ) Z/rouJic/. . F^xF . .FC'.uf>/jiiq .. p^/t<A .. -
__/:/l/riXxI u J- -d1'i04____:F<-^ .. -fl-^,<cF>y _.J\aS_cl_JdaF--.-
^..^OFcl...:f/<^>Fbrc -4i--^ ......^.CZlnntj....3<^/.pciF FZT^, /JI
36
)rj/>o/y)mc F-4>
aJ-
— I44F
JT^Zl^iJJjJl/k.
'Sci/:pZ(cl
FZFo/y; FJtZ'/^j/?^ rJ'A ^^'o,p/i^r?<Z
Jj:iJc7^ J^ Jj/ MCzSJ z ^__ . '£^
d/i'S/fc OZ FF/Z^l ^/^Ac 7)ro/Afir-/c/ F>cuFrc
Z'^F.
Thiokol CorporaUon RCRA FaciUtv Investigation
W0#: 1B940 LWR#:
SFTC: M-19A SepUc Drainfield
DESCRIPTION: SWMU #628; Grid IZ-rS, ft
PARAMETCRS
Cadinium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
Bc^ ^7
T^and Q/jd Qfci.
JTZLO
DATC: 9'Z^F F' TIME: /fC^^^SAMPLER:
Thiokol CorporaUon RCRA FacUity InvesUgaUon
W0#: 1B940 LWR#:
SITC: M-19A Septic Drainfleld ^
DESCRIPTION: SWMU #628; Grid /^<10 ft
FK^J L'utiiiKp^ -/TC/II
PARAMETCRS
Cadmium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
/lolc ' a rc
__jqrMclcJ^^aiauiLi
Fj/nF/c/ti^ F<L^^£^
Zi'j^ cJroi n frJcF
3c^^^FZ/^-CZC^
DATC: 9'-'cZ^FT~ TIME: /5"/<^^ SAMPLER: F^
JS^.O.___Fd^_pcf,<^c-^\.^ASC£jAatLUcF h-< TTW rjcUj, ,.
Arid/ Zt^ ^ rc^frFcur^ltA .un '^cuLcc_d^_Mr_f'^^^j^'Vj^y-
Tid.-^ LL'£^f^.J^.^J.
't (••
37
/r
-.F-/'. -7
•/ f
^'•^ Vt rJ •-,• 46 J^ ^ ."r ( •••^//
Lvj/rc/rfu.' <///S<: iS/:'id<-^ F'/c^ rc ^./jjFc/-, LL -^
:^>UJJii/J. 'F FFd d. Id I
Thiokol Corporation RCRA FacUitv Investigation
W0#: 1B940 LWR#: £//OL>C'
SITE: M-71 Septic Drainfield
DESCRIPTION: SWMU #646; Rmse Blank Grid # • , ft
PARAMETCRS
Be/tlj, CO 7\<j, h>lo
Mercurv
pH
METHOD
6010
7470
DATC: ZC-Z-y ^ TIME:i'^iV.' SM.TPLEK: F^lcy
-Thiokol Corporation RCRA Facility InvestigaUon
W0#: 1B940 LWR#: CT//0/:>/
SITC: M-71 Septic Drainfield ' ^ O
DESCRIPTION: S\\'MU #646; Grid # /^f, 5 ft
PARAMETCRS
VolatUe Organics
METHOD
8260
^ :c
•o..' //(J uilc/ (^yj./f
DATC :lFZ'VF TIME; t^3S-SAMPLER: FLJ
Tiiiokol Corporation RCRA FaciUty InvestigaUon
W0#: 1B940 LWR#: £,//OLC
SITC: M-71 Septic Drainfield .
DESCRIPTION: S^\'MU #646; Grid # 'Cl , 5 ft
PARAMETCRS METHOD
Be
Mercurv
pH
6010
7470
'••r^
/^-2'vr
DATC: / ^3^ '•tF^'.^lME: FJTS" SAMT'IFR-Ft^
.. .^ 77i/o*o/Corporation RCRA FacUity Investigation
!) "^ .. _ W0#: 1B940 LWR#: ElICO L'
SITC: M-71 Septic Drainfield
- DESCRIPTION: S^VMU #646; Grid # IOi , 10 ft
PARAMETCRS
VolatUe Organics
METHOD
8260
Zc.,.^_5l3.
•}±JL tl. ! "j • ;d
DATC : ^/C C- 9 ^-^ TIME: ^^^^ SAMPLER: Fc^
38 Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: £^//ChO
SITC: M-71 Septic Drainfield
DESCRIPTION: SWMU #646; Grid # J_C_I, 10 ft
PARAMETCRS METHOD
Be
Mercurv
pH
6010
7470
•FL
DATC: /^ 2-9 I TIME:<^5 *5 SAMPLER: F*-
Thiokol CorporaUon RCRA FacUitv Investigation
\V0#: 1B940 LWR#: C/f^LC
SITC: M-71 Septic Drainfield
DESCRIPTION: S\VMU #646; Grid # ^OC. 5 ft
PARAMETCRS
Volatile Organics
METHOD
8260
..FC ^_4r _
iJJ)ti\ -d'/j.v/.S'//^
DATC: /O'i-'^S TVSTT.: VFt SAU
Thiokol Corporation RCRA FacUity Investigation
WO*: 1B940 LWR#: C-r/^OC--^
SITC: M-71 Septic Drainfield
DESCRIPTION: S\\'MU #646; Grid # /OJj, 5 ft
.F UL^
PARAMETCRS METHOD
Be
Mercun
pH
6010
7470
F^
DATC: ZO ' 0-^Z\ TIME: 7 ZC SA\n»I FH-
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: /^//^^'*-•
SITC: M-71 SepUc Dramfield ^^
DESCRIPTION: SWMU #646; Grid # /6G, 10 ft
F<^
PARAMETERS
VolatUe Organics
METHOD
8260 777c4^ . '^'Ih
//J"7.^/' 'Z/, CAA fPI FP' FuO
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: t-llCUO
SITC: .M-71 Septic Drainfield
DESCRIPTION: SWAIU #646; Grid It JP L . lO »
PARAMETCRS
Volatile Organics
METHOD
8260
'17) UP
.DATC : iO'l-ZF^ TIME: ^^0 SA>n'LER: rUJ
•
-Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: j^/OO^O
SITC: M-71 Septic Drainfield
DESCRIPTION: SWMU #646; Grid # /OL', 10 ft
39
PARAMETERS
Be
Mercurv
pH
METTIOD
6010
7470
MK-TE-./O'ZF'F' TIME: Z^^ SAMPLER: F^
^^^ ' ' d ^9 Ah 19/^ ^U^y/U^ii Z.'ZFJ ^
Thiokol Corporation RCRA FacUitv InvesUgation
W0#: 1B940 LWR#: /^//6'0 Ir
SFTC: M-19A Septic Drainfield
DESCRIPTION: SWMU #628; Grid 2-' ^ f'
_SF^^/0O
PARAMETERS
Cadmium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
33cfL^anJ._^/iu/c
JlZJ
-ZV TIME: //d'r^ SAAIPLER: F(-<.J
estigation
/ . 10 ft
_ DATC: /6 -I
Thiokol Corporation RCRA FacUitv InvesUgation
W0#: 1B940 LWR# ~
SITC: M-19A Septic Drainfield
DESCRIPTION: SWMU #628; Grid
y
Bc^fo
PARAMETCRS
Catlmium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
d^c>cj7i_a/fd
ZC ''^''^^ TIME: Z/27 SAMPLER: FF^' _DATC:
77i/o*o/ Corporation RCRA FacUitv Investigation
WO*' 1B940 LWR#: ^//00(^
STTE: M-I9A Septic Drainfield
DESCRIPTION: SWAIU #628; DUP Grid Q /^
PARA.METCRS
Catlmium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
DATC: /^';',.^-^7' TIME: //;7 7 SANffLER: FuJ
iJ
-ti'^
. «•.« J k^'.fc«A.-aZj**« • — -fln -''^'"^
40
llf7L
Thiokol Corporation RCRA FacUity Investigation
WO#: IB940 LWR#:
SITC: M-19A Septic Drainfield
DESCRIPTION: SWMU #6 F^C^ -?.'^
PARAMETCI
pH
METHOD
6010
6010
6010
6010
9045
7F:j/:Fo/7r/0{rui >^ T
dZIF
1340
.J4c>^.
DATC: /O 'Z' ZF TIME: //_5Y^AMPLER: PLJU
Thiokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: ^//^O L
SITE: M-19A Septic Drainfield Fd:> 1/ r
DESCRHTION: SWMU #628; Grid / / , yf^ 2? /z X^
SC
PARAMETCRS
Cadmium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
IQQ _
.FJ^oolZ_f__^m,Mf_
DATC: Z<^ - 2-9^-] TFVfF- 72///
Thiokol Corporation RCRA FacUity Investigation
W0#: IB940 LWR#: 5.1 10IfiLf
STTE: M-19A Septic Drainfield
DESCRIPTION: S\\'MU #628; Grid ^Q .. 5 ft
KKXKm CO. r,)
j4<faM ZS^zJr.^_lFZd
-SC.=F34
PARAMETCRS
Cadmium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
-//JVC ^tld-^FTOrzii.
Ti\TE://?-Z'f<r ™IE= I^C SAMPLER: F^
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 L^VR#: t-^ICO^
SITC: M-19A Septic Drainfield
DESCRIPTION: S^^'MU #628; Grid 2 6>. 10 ft
PARAMETCRS
Cadmium
Chromium
Silver
Lead
pH
METHOD
6010
6010
6010
6010
9045
O/i
iDO
zaueL
tc/c^
DATC :/^-2'fr'TIME: /4{) ^ SA-NffLER: F^
xftii'^*-^'- /" <-
-~ /cT/S" ^th
or AA m afi Z>i'<^/' nr,^ 0>f 0>id drjL u/^if
5U//1>I // -^-.g^^ ^
l-y'^'T •? honing', UJa.r& Otioi,fi/n^ m ttu ^i-M af n 'ULCIL ^^sy- hoZe. Flh^^aho/zo/t&uJ- . .
JlZ^s / 7<^ ^ ^^(Z/npiZii ZJ//2^ ^^F/J/Z^^J-J
^7^_j?^/i -iOfc^ 2^: aLej2^JlZ2s^Jz/frLjO}^
acLJ^ ZJFZZU. F^/?^u/ r^A-'Mj ^r/j/jr.r.^¥
J2^Z>..F7^<^ eJFC zan^ z7lt/Ft:rrpp/tiqK _ /jnfz^
a j^
Z)/}cl /Z j<L 0 i^4Uc?l^ ' ^a^ /JJ^i^rt
//.^. I n/is F/uini,
-_ I'SSX Thiokol CorporaUon RCRA Facility Investigation
W0#; IB940 LWR#:
SITC: M-117 Subsurface Discharge
DESCRIPTION: SWMU #254; ^F ^P*^
PARAMETCRS
Antimony
Sulfate
pH
METHOD
6010
300
9045
roci:^. IZ
DATC: /0'Z-^S~ TIME: /^'S'/SAMI'LER: Z-ld
dlicrafioKS Aa/HZ fi, tu ^ho^
"f^'Odd 3
•
^^^^ f .—•— _—. -_
4t> /ef/ Cinia 9t> F-S . ~pau^Cf L/Kji ol/ slyixc/igy^
F^<K/^//9> ^ T-f 5'A. ^^^uyctl FliZJ^ji^t^ _Jjl-*^^
/ocm U/AicA. UUi/l /Ibf o/Zoo-^ t/yg. ol aucj / y/<
06^.
^t-<y<-'
S/^-V _d(/<-' cdy^v^cli o^f T-/4 SujA^Q-a^^
Thiokol CorporaUon RCRA FacUity InvestigaUon
W0#: IB940 LWR#: £-///;£, 7
SFTC: T-I4A Subsurface Discharge '
DESCRIPTION: SWMU #493;<i*^ Depth
"-^
F:,C- /7
PARAMETCRS
Antimony
Arsenic
Chromium
Lead
Sulfate
pH
METHOD
6010
6010
6010
6010
300
9045
Q-i7l^'F Gnd cc.e-:^^
I5u/Ic/ F
DATC: lc -J- 7 7~ TIME: 0 S"6 SAMPLER: FuJ -A
FF •-{y-\ IMV<?
i.C<^"
.F'^h^F.-^..-J Fl:x.^..c.^.[ ^c:<(_i^__i(LK ^.__S.f_^J< i. 2_<.rv^. Jiv«^
i-a*^s \-.F i'^ iil Fi^r. -s t Ul^^,|}^'_ ^ ._.;,t'i\.i-.k
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: i-J/O L 7
SITE: T-14A Subsurface Discharge
DESCRIPTION: SWMU #493;
PARAMETCRS
Antimony
Arsenic
Chromium
Uad
Sulfate
pH
-)i Depth
METHOD
6010
6010
6010
6010
300
9045
DATC: / L •7\' TIME: 9/^ SAMPLER: t'-^
.50-
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: El 1067
SFTC: South of M-153
DESCRIPTION: Manufacturing Area Background; Surface
PARAMETERS
VolatUe Organics
METHOD
8260
,_J5.'
.7^717
DATE: 10/3/95 TIME : iCck'' SAMPLER: f^J
•
77iio*o/ Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: El 1067
SITC: South of M-1S3
DESCRIPTION: Manufacturing Area Background; Surface
43
PARAMETERS
Semi-VolatUe Organics
METHOD
8270
DATC: 10/3/95
10 io
%
TIME: /OOo SAMPr.FR-Fi.^
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: El 1067
DESCRIPTION: Manufacturing Area Background; Surface
PARAMETERS METHOD
pH 9045
Cd, Cr, Ag, Pb, Be, Cu, Sb, Se, As 6010
Ni, B, Zn, Tl, Mn 6010
Mercury 7470
HMX HPLC
Nitroglycerin HPLC
Perchlorates IC
Cyanide 9010
Sulfate 300
-DATC: 10/3/95 TIME: fOC O SAMPLER:
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: El 1067
SFTC: South of M-153
DESCRIPTION: Manufacturing Area Background; 2 ft.
-A-'
PARAMETCRS
VolatUe Organics
METHOD
8260
?F7
^>l-l
' ^f
— cJ r^^
0
DATC: 10/3/95 TIME; : IClO SAMPLER: /IV
Thiokol CorporaUon RCRA FacUity InvesUgation
W0#: 1B940 LWR#: El 1067
STTE: South of M-153
DESCRIPTION: Manufacturing Area Background; 2 ft.
PARAMETERS
Semi-VolatUe Organics
METHOD
8270
OATT.: 10/^/95 TIME: UK-'
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: El 1067
DESCRIPTION: Manufacturing Area Background; 2 ft
SAMPLER: Fd
PARAMETERS
pH
Cd, Cr, Ag, Pb, Be, Cu, Sb, Se, As
Ni, B, Zn, TI, Mn
Mercury
HMX
Nitroglycerin
Perchlorates
Cyanide
Sulfate
DATC: 10/3/95 TIME:
METHOD
9045
6010
6010
7470
HPLC
HPLC
IC
9010
300
/O i 0 SAMPLER: f-L^
44
ID ZC
Thiokol Corporation RCRA FacUity Investigation
WO#: IB940 LWR#: El 1067
SFFE: South of M-153
DESCRIPTION: Manufacturing Area Background; 5 ft.
PARAMETCRS
VolatUe Organics
METHOD
8260
:EC ^ /F7-
5)/y
i^^:
TIMF.: JOZO .SAMPI.FR: F\/-J -DATC: 10/3/95
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: El 1067
STTC: South of M-1S3
DESCRIPTION: Manufacturing Area Background; 5 ft.
PARAMETERS
Semi-VolatUe Organics
METHOD
8270
TIME: //>7.0 SAMPI FR- Px^ -DATC: 10/3/95
7^io*o/ Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: E11067
DESCRIPTION: Manufacturing Area Background; 5 ft.
PARAMETCRS
pH
Cd, Cr, Ag, Pb, Be, Cu, Sb, Se, As
Ni, B, Zn, TT, Mn
Mercury
HMX
Nitroglycerin
Perchlorates
Cyanide
Sulfate
-DATC: 10/3/95
Tiiiokol CorporaUon RCRA FacUity Investigation
W0#: 1B940 LWR#: El 1067
SFTE: South of M-153
DESCRIPTION: Manufacturing Area Background; 10 ft.
METHOD
9045
6010
6010
7470
HPLC
HPLC
IC
9010
300
TIME: I0'2C' SAMPLER: /l^
PARAMETCRS
VolatUe Organics
METHOD
82<UI_
M£cliu n-^.. h.rc^n-::'!..
s. -'F.
_DATC: 10/3/95 TIME: /Z>OC' SANffLER:
-Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: £11067
SITC: South of M-153
DESCRIPTION: Manufacturing Area Backgroimd; 10 ft.
r^^
PARAMETERS
Semi-VolatUe Organics
METHOD
8270
DATC: 10/3/95 TIME: /0 7)C SAMPLER: FF
SAMPLER:
_ 1144-.^
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: El 1067
DESCRIPTION: Manufacturing Area Background; 10 ft.
PARAMETCRS METHOD
. pH 9045
Cd, Cr, Ag, Pb, Be, Cu, Sb, Se, As 6010
Ni, B, Zn, Tl, Mn 6010
Mercury 7470
HMX HPLC
Nitroglycerin HPLC
Perchlorates IC
Cyanide 9010
Sulfate 300
_DATF.: 10/:</95 TTME: /D lO
Thiokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#:E11067
DESCRIPTION: Manufacturing Area Background; DUP 10 ft.
PARAMETCRS METHOD
pH 9045
Cd, Cr, Ag, Pb, Be, Cu, Sb, Se. As 6010
Ni. B. Zn. TT. Mn 6010
Mercury 7470
HMX HPLC
Nitroglycerin HPLC
Perchlorates IC
Cyanide 9010
Sulfate 300
DATC: 10/3/95 TIME: lOlO SAMPLER:
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: E11067
SFTC: South of M-153
DESCRIPTION: Manufacturing Area Background; IS ft.
45
F^-o
Fd
TBc ^id.
m PARAMETERS
VolatUe Orgaiucs
METHOD
8260
-5J//
DATC: 10/3/95 TIME: 1/4^ SANffLER:
Thiokol CorporaUon RCRA FaciUty Investigation
W0#: IB940 LWR#: El 1067
SFTC: South of M-153
DESCRIPTION: Manufacturing Area Background; 15 ft.
A'^J
PARAMETCRS
Semi-VolatUe Organics
METHOD
8270
DATE: 10/3/95 TIME: /D44 SAMPLER:
Thiokol Corporation RCRA Facility InvesUgaUon
W0#: 1B940 LWR#:E11067
DESCRIPTION: Manufacturing Area Background; IS ft.
Fu/
PARAMETCRS
pH
__ Cd, Cr, Ag, Pb, Be,
Ni, B, Zn, Tl, Mn
— Mercurv
HMX
NUroglycerin
Perchlorates
Cvanide
Sulfate
DATC: 10/3/95
Cu, Sb, Se, As
TIME:
METHOD
9045
6010
6010
7470
HPLC
HPLC
IC
9010
300
/044- i
F-±ZLi^x
46
.d^//?^d^ f/i:on CLFF /C'/A pZo/'.Z /ZF ZZ-OF
tk
IftVlLV f -"
47
ISOO
.Z2>-/:?aZ—Z'Z9S7
at /tZ'C^SIo Z:o ^t<s- Sg«=</ Cy(^s-^
"^"nj/l/l A/mr/iitJjl/l/}-^,/^ .^7) AU^ ^Z" ,"Vi
_^Za5urc
^p/a/i., ///>prax//tia7^Z^ SD Z^s a/ s^cJ ^g^
/IQ/ld sp reader. ^
JzcooJca x£^^v^r-jtZic_c//^i/u/'ZKd^i!7ir(:a.-—-^4^^t^
/^ Corhp/cJe, aZ "T^/S Z)/7C
'^cn.
5 /_-_^e r_^_^,f_ci
•
P0S.O__ 7ZF]-g/k.CrAr/^ 3//£ ZrFM./^a7foi^ ZlZ /U-ZZ4. Z^
^KFo..(7c^im- .^acfA Aas____b<f_^_d^_Jj^//ccZ__a/^^
-07i/f</.._7Ah ^/Zc r<^sirr^J Zz> /A Zir/^/ziJ^ .ra/r^ur.
-Se^d^ Ftp/iroK/yna^/^ :5' /^s ^F ^zrr^'^AcA
'Jc.
11-14- 9F . .
iSoo Zh ZZ'IfZZ do S3/nplc S^// /^/J6uj/no (^)/co.iAi/if»^ ^
For mmtr lAoJ of S^r^p T- S8 B. %; w-G/i COA-
IK^Icll \—'i'—\
#f fSC
14'
at
^
EKcfWArep Age^?
Thiokol Corporation RCRA FaciUtv Investigation
W0#: 1B940 Lwik#: tf"//// /'
SITC: Sump Removal at M-622
DESCRIPTION: SWMU #316; LocaUon # / ; Su/^. deep
PARAMETCRS
Cd, Cr, Ag, Pb
Hg
Ng, HMX
Perchlorates
Nitrate
METHOD
6010
7470
HPLC
IC
DATC: //~/4-9S^ TIME: ^3^^ SAMPLER: Af^i^
Thiokol CorporaUon RCRA FacUity InvesUgation
W0#: 1B940 LWR#: £///l{
SITC: Sump Removal at M-622
DESCRIPTION: SWMU #316; LocaUon # / ; Sw^ft. deep
PARAMETERS METHOD
VOA 8260
DATC: 11^14-99^ TIME: /3CO SAMPLER: /^/"-^
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: £"/////
SITC: Sump Removal at M-622
DESCRIPTION: STWMU #316; LocaUon # / ; / ft. deep
PARAMETCRS METHOD
Cd, Cr, Ag, Pb
Hg
Ng, HMX
Perchlorates
Nitrate
6010
7470
HPLC
IC
DATC: 11-1^-9 f TIME: ''3/G SAMPLER: >^/=C_)
49
Thiokol CorporaUon RCRA FaciUty Investigation
W0#: 1B940 LWR#: £7////
SFTC: Sump Removal at M-622
DESCRHTION: SWMU #316; Location #__/_; _j^ ft. deep
PARAMETCRS
VOA
METHOD
8260
DATC: l(-/4-'fS TIME: /J/^J SAMPLER: i4i=C:>
Thiokol Corporation RCRA FacUitv Investigation
W0#: 1B940 LWR#: <f7////
SITC: Sump Removal at M-622
DESCRHTION: SWMU #316; LocaUon #_Z^;3aQl. deep
PARAMETCRS METHOD
VOA 8260
DATC: lh/<^-9S^ TIME: Z^?/J^ SAAH-LER: AJ^U^
Thiokol Corporation RCRA FaciUty InvestigaUon
W0#: 1B940 LWR#: £y////
SITE: Sump Removal at M-622
DESCRIPTION: SWMU #316; UcaUon # Z ; ^^t. deep
PARAMETERS
Cd, Cr, Ag, Pb
Hg
Ng, HMX
Perchlorates
Nitrate
METHOD
6010
7470
HPLC
IC
DATC: /r- ^fS^ TUVffi-^ /J/J" SAMPLER: jy=i<.I
Thiokol Corporation RCRA FaciUty InvesUgation
W0#: 1B940 LWR#: £//1//
SITE: Sump Removal at M-622 ._ .
DESCRIPTION: SWMU #316; Location #_^_; _/_ ft. deep
PARAMETERS
Cd, Cr, Ag, Pb
Hg
Ng, HMX
Perchlorates
Nitrate
METHOD
6010
7470
HPLC
IC
DATC: ll-/4-9F^ TTSTE: nZ^ SAMPLER: AF^
m
77iio*o/ Corporation RCRA FacUity InvMtigation
WO#:1B940 LWR#: £/JlH
STTE: Sump Removal at M-622
DESCRIPTION: SWMU #316; Location # /^ ; _/_ ft. deep
PARAMETCRS
VOA
METHOD
8260
DATC; . I{-14"9^ TIME: I3ZO, SAMPLER: AF-^
Thiokol CorporaUon RCRA FacUity Investigation
W0#: 1B940 LWR#: £//// /
SITC: Sump Removal at M-622
DESCRIPTION: SWMU #316; LocaUon # ; ft- deep
PARAMETCRS
Unified SoU Classification
METHOD
7 -'•'
i
DATC: /I-/4-9F TIME: /3ZO SAMPLER: At^"^
•l.FDdc 9S^
13/D Ai Ad'^f io troadoQs^t Co^^Ad^ou/uiaC
,_^^<£r <^jCCa.iZ^-fccL Oil-^0-- Z>£ 'S/ZO'f/
Flodji/iiiL-/i(m • ^Ci(MM<fd_„ OifiprcKfntafrl'i' ^/Ai.. i
J>f^ /^ccd.
F
Sf^Z<^~ l^oodti y Srct^r.d^,
.^^FU-
u
-
i.L>rviA:.. /•»•»• » J
ENVIRONMENTAL LAB WORK REQUEST (j^^ 91) -U fi
™^ THIOKOL ENVraONMENTAL LABORATORY LWRNo. El 1040
_^^ /
AF U)a^^
EXTENSION COST CENTER
UJ340
WORKORDER
18940 lt^fit9C
ORCANrZATION
B/lQirO ^^9r
MAIL STOP
3o/£
REPORT RESin.TS TO:
KELEN WARD, MS 301
SAMPLE INFORMATION
\.
/
SAMPLE
•Zfi-
7 f^-h
3 t^dH^
SPr
s-l=t
7 A-
^ CU^2^
WCleldS-Z-
2_ fi-
ll Gdt4T2-
<7f'r
p. Cd.HS Z.
DATE
9-ll-f9
ll
II
II
fl
fl
II
»1
f'/z-yr
^-an-
il
, 1
TYPE
G
- ^
y
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LOCATION
/l^-iSO ^fio
If
If
fl
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11
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n
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TIME
047
mi
14^-^
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dor'
'dcF
TIST
z/>c - ez4o
QI,CoAs,Pk^Co/o /Iq,
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Cd.O.,A^,fih, H-^ , Hxi
Cci,Cr,ZU.p6, H9, -dAi
lAoc.
C</,Cf,Z^.Ph,ld\,hh^>
\Zoc
cd Cr 4^ 1% Hcj FMK
\Zoc
CZl, Cr^ At,, PL, dq HHZ
REMARKS
//AiK, /JG
X ,A)&
<f /UG
' . X/<3
/JG
ZIG
CHAIN OF CUSTODY
RELINQUISHED BY
JaJozJi^
DATE
iZ ^i 97
TIME
' I4-FZ>
RECEIVED BY
^ YAC/AZF/^-iitiF"
DATE
f^/7^9^
TIME
/^^5
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED SIGNATURE
ENVIRONMENTAL LAB WORK REQUEST
™^ THIOKOL ENVIRONMENTAL LABORATORY
FROM:
ORGANIZATION
EXTENSION
MAIL STOP
LWRNo.
COST CENTER WORK ORDER
E11040
DATE
REPORT RESin,TS TO:
HELEN WARD, MS 301
/
V
•/
^
/
\
/
N
/
N
/
\
SAMPLE
-ZPT
^-Gd4 7U
<-/=f-
y^d 4-19
7 f^ ^ /^**-i9
7f^
1 Qd*/--/e4/^
^n&i-if^lo4
^^•CJ^IOi
DATE
/^Syvfr
tl
K
fl
H
\(
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H
i\
'1
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//
TYPE
G
• •
*-^
ly
i^
t/
l/
x/
V
y
y/
y
A
C
SAMPLE INFORMATION
LOCATION
Si^MU-if Z4^
AJ~I?L
l(
/(
il
'1
l(
l{
/I
/(
1'
'1
/'
TIME
^ezy
OSZl
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^/o
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923
^23
/oir
loiF
TEST
Vcc
Cd,Cr,A^.Py,ikM^%, A/i
uoc^
cd, Cr, A^, /^O, /h. HHA, ^
VoG.
CA.Cr /U fio fl^? //At/
\IOC^
REMARKS
r
fG
.K)&
CdCr A*i f'h /A flif^y^ NG
MOL.
Cd Cf Ao f>h ^o ^
dtL
CJ Cr A> flo /^ //-6
JC XIC:.
^ XJfeS
CHAIN OF CUSTODY
RELINQUISHED BY DATE TIME RECEIVED BY
a=
DATE TtME
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED SIGNATURE
ENVIRONMENTAL LAB WORK REQIHEST
# THIOKOL ENVIRONMENTAL LABORATORY LWR No. E11040
'&^^
EXTENSION COST CENTER WORK ORDER
ORGANIZATION REPORT RESULTS TO:
HELEN WARD, MS 301
t
,/
\
/
\
<
0
\
/ \l
SAMPLE
\, ed ^ iic>
•• Gd-a^lto
' Gd4^tio
= ^^ /«»
•pff.
^ ^U ISO 7 A<-
' <^* 'P'u
» 6W# /so
^od^r7S_
'^Gd^/lf
'^ Oj 4 /7f
DATE
litM
i{
ll
II
u
K
i(
1 •
K
II
K
1 <
TYPE
G
- y
y
^
y
ly
ly
y
y
sy
L/
\r
1/
C
2
SAMPLE INFORMATION
LOCATION
^iM/\\ 0 41/^3
AA'iZi^
l(
i(
'(
'(
'(
>l
II
II
1^
'\
n
TIME
m^c^
ID^O
lOi^Si
TliST
yoc^
CJ Cf A ^i. ^-f m
J u
ll^G
REMARKS
X fjG
/O^'Ci Cf Ac Ph fi^ /^/AX //G
IHIO
mo
Ilto
nto
AoG.
Cd Cr A Fl, ^4 FMx A/G
, 1 ^
CA Cr A Fy> ;^7 ///«X ^G
•J J
\JOG
aC/ /U ^b /i^ /.^AOC /Us
\ZOG
Cd Cr A*s F/o //^ /IAX //<S
CHAIN OF CUSTODY
RELINQUISHED BY DATE TIME RECEIVED BY DATE TIME
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED
ENVIRONMENTAL LAB WORK REQUEST
THIOKOL ENVIRONMENTAL LABORATORY
COST CENTER
LWR No. E11040
WORK OROER DATE ?^
ORGANIZATION MAIL STOP REPORT RESULTS TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS
Q^i^-zFt 942^7 5uH(U 4^Z43
/
Gd-^ISZr?f^ /I It
I3ZL VoG
I52L. ClCr.A^^PU UJ l4K^Air.
(^•^I^OSft If i7 If I33F Voe
^F^^£: fl \y ll
'&/^Z6^-ii^- n
B3£ CJ Cr A^ H Hf I/UK ^\G
y If IJ£L Moe.
Af n d^
'GdMoZk^l 'n y If i3£L Du? \l0G
XeidtZ^^tk ll y
*&z^2cs-^ri
/^i/Zo^-6-ft
If IF
ll v
F iiS-/ CA C^ Ac| Tb t4^ ^hJ^ uc-
// I^iQ_ VOG
mo. CA Cr f^>^ ^ }?f^J^t Ki&
Gd-tf-I7(^-ZF,- fl y K I4z:u ^DC^
/^"^njrZ^ft i( y It lilk. CAc^ hc^ Pb Hg JMlK /Jg*
bd^ncrm i^ y fi \fOG
CM m-5 ft // ^
CHAIN OF CUSTODY
RELINQUISHED BY DATE TIME RECEIVED BY DATE TIME
FOR LABORATORY USE ONLY
TE COMPLETED DATE REPORTED SIGNATURE
October 18, 1995 CERTIFICATE OF AINALYSIS
RESUI.TS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward MIS 301
Thiokol Corp. Ut 84322
A.F. WALKER
EXT 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Oty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order )i^ 9509020 Sample and Test Code Identifiaition
Lab ID:
OIA
Sample ID:
GD #3, 2 FT. M-136
Test Codes and Names
Lab ID:
02A
Sample ID:
GD #3, 5 FT. M-136
Lab ID:
03A
Sample ID:
GD #32, 2 FT. M-136
Lab ID:
04A
Sample ID:
GD #32, 5 FT. M-136
Lab ID:
05A
Sample ID:
GD #52, 2 FT. M-136
Lab ID:
06A
Sample ID:
GD #52, 5 FT. M-136
HMX
NO
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8260S
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Orgamcs
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8260S
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NO
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8260S
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8260S
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB A£2
AG AE2
HG CV2
8260S
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A Method
SOP 420
SOP 420
SW-846, 3050
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,8260A
Method
,6010
,6010
,6010
,6010
7471
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A Method
SOP 420
SOP 420
SW-846, 3050
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,8260A
Method
,6010
,6010
, 6010
,6010
,7471
HMX HMX SOP 420
Page#:lof ^'^
Work Order jj^ 9509020 Sample and Test Code Identification
Lab ID:
06A
Sample ID:
GD #52, 5 FT. M-136
Test Codes and Names
Lab ID:
07A
Sample ID:
GD #74, 2 FT. M-136
Lab ID:
08A
Sample ID:
GD #74, 5 FT. M-136
Lab ID:
09A
Sample ID:
GD #19, 2 FT. M-136
Lab ID:
lOA
Sample ID:
GD #19, 5 FT. M-136
Lab ID:
llA
Sample ID:
GD #104, 2 FT. M-136
Lab ID:
12A
Sample ID:
GD #104, 5 FT. M-136
NG
3050
CD AE2
CR~AE2
PB~AE2
AG AE2
HG CV2
8260S
Nitroglycerine
Acid Digestion
Cadmium Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NG
3050
CD AE2
CR~AE2
PB AE2
AG AE2
HG~CV2
8260S
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chroinium
Lead
Silver
Mftrcuiy
Volatile Organics'
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB~AE2
AG AE2
HG~CV2
82603
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NO
3050
CD AE2
CR~AE2
PB~AE2
AG AE2
HG~CV2
8266s
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercuiy
Volatile Organics
Test Codes and Names
HMX
NO
3050
CD AE2
CR~AE2
PB~AE2
Ad"AE2
HG~CV2
8260S
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NO
3050
CD AE2
CR~AE2
PB~AE2
AG~AE2
HG CV2
8260S
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NO
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG~CV2
8260S
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Method
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Page #:2
Work Order <i 9509020
•#^^
Sample ID:
GD #120, 2 FT. M-136
UbID:
14A
Sample ID:
GD #120, 5 FT. M-136
Lab ID:
T3A—
Sample ID:
GD #150, 2 FT. M-136
Lab ID:
16A
Sample ID:
GD #150, 5 FT. M-136
Lab ID:
17A
Sample ID:
GD #179, 2 FT. M-136
UbID:
ISA
Sample ID:
GD #179, 5 FT. M-136
Lab ID:
19A
Sample ID:
GD #156, 2 FT. M-136
Sample and Test Code Identification
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8260s
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
826DS
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8260s
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HO CV2
8260s
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercuiy
Volatile Organics
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8260s
HMX
Nitroglycerine
Acid Digestion
Cadinium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NO
3050
CD AE2
CR AE2
PB AE2
AG AE2
HO CV2
8260s
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chroinium
lejid
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
7471
Page #:3
Work Order # 9509020 Sample and Test Code Identification
Lab ID:
~T5A
Lab ID:
"IOA
Sample ID:
GD #156, 2 FT. M-136
Sample ID:
GD #156, 5 FT. M-136
Test Codes and Names
Lab ID:
~2TA
:>amp
3D«(
lelD:
GD #205, 2 FT. M-136
Lab ID:
~SA
Sample ID:
GD jR05, 5 FT. M-136
Lab ID:
~23A
lelD:
OD #176, 2 FT. M-136
Lab ID:
24A
Sample ID:
GD #176, 5 FT. M-136
Lab ID:
^5A—
Sample ID:
GD «05, 2 FT. M-136 DUP.
8260S Volatile Organics
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8260s
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chroinium
Lead
Silver
Mercury
Volatile Orgamcs
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8260s
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AO AE2
HG CV2
8260s
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chronuum
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AO AE2
HG CV2
8260s
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NG
3050
CD AE2
CR~AE2
PB AE2
AG AE2
HG CV2
8260s
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercuiy
Volatile Organics
Test Codes and Names
8260S Volatile Organics
Comments
'I^^^
,6010
,6010
,6010
,6010
Method
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A Method
SOP 420
SOP 420
SW-846, 3050
SW-846,
SW-846,
SW-846,
SW-846,
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
8^-846, 6010
SW-846, 6010
SW-84«, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SW-846,8260A
Certried By
•
Page #:4
•
This is to certify that the following samples Were analyzed using good laboratory practices
to show the following results.
ample ID: GD #3, 2 FT. M-136 Lab ID: 9509020-OlA Collected: 09/11/95 14:47:00
SST
a
Ltroglycerlne
::ld Digestion
idmlum
iromium
3ad
Liver
arcury
olatile Organics
anzene
romobenzene
roEd^^l orome thane
roi^|Hchl or ome theme
romoform
romomethane
-butylbenzene
ec-butylbenzene
ert-butylbenzene
arbon tetrachloride
hlorobenzene
hloroethane
:hloroform
:hlorome thane
.-chlorotoluene
-chlorotoluene
libromochlorometheine
.,2 - dibromo-3 -chloropropan
,2-dibromoethane
ibromome theine
ichlorodifluoromethane
,1-dichloroethane
,2-dichloroethane
,1-dichloroethene
is-1,2-dichloroethene
rans-1,2-dichloroethene
,2-dichloropropane
,3-dichloropropane
, 2 -dichloropropcine
,1-dichloropropene
:is-1,3-dichloropropene
rans-l,3-dichloropropene
, 2.^j^hlorobenzene
, 3 fl^Bhlorobenzene
RESULT
U
u
09/15/95
0.16
19.6
U
U
U
U
u
u u u
u u
u u u 1.1 J
u 1.7 BJ
U
U
u u
u
u
u u u
u u u u u u
u u
u
u u u
DNITS
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
. ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.500
0.500
0.1
0.3
1.5
0.2
0.013
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZiED
09/19/95
09/19/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
09/26/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95'
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-845,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
Page #: 5
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #3, 2 FT. M-136 Lab ID: 9509020-OlA CoUected: 09/11/95 14:47:00
TEST
Volatile Organics
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2- tetrachloroe thcine
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
tri chlorof luorome theuie
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-buteuione
4 -methyl - 2 -pentcuione
2-hexcLnone
fluorobenzene
chlorobenzene-d5
1,4 -di chlorobenzene-d4
RESDLT
U
U
u D
U
11 B
U
U
U
U
U
U
1.1 J
U
U
9.4 BJ
U
U
U
U
U
U
U
U
U
2.4 BJ
U
U
U
858913
610275
228426
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
LO
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organica 8260S
Surrogate
dibromofluoromethane
1,2-dichloroethane-d4
toluene-d8
bromof1uorobenzene
%Recovery
98.7
102
102
106
METHOD/CAS#
SW-846,8260A
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6 ^^
108-67-8 ^^
75-01-4 ^P^
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Racovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #3, 5 FT. M-136 Lab ID: 9509020-02A CoUected: 09/11/95 14:56:00
TEST RESULT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMX O MG/KG O.SOO 09/19/95 KMS SOP 420
Page #: 6
October 18, 1995 10:02
Sample ID: GD #3, 5 FT. M-136
CERTIFICATE OF ANiU^YSIS
< RESULTS BY SAMPLE
•i^' Lab ID: 9509020-02A CoUected: 09/11/95 14:56:00
TEST
Kitroglycerine
Acid Digestion
Cadmitun
Chromiiun
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodichloromethane
bromoform
^l^jomome thane
IHbuty Ibenz ene
^rec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3-chloropropan
1,2-dibromoethane
dibromomethane
di chlorodi fluoromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2 -dichloropropcine
1,1-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
^hylbenzene
M^achlorobutadiene
RESDLT
U
09/15/95
0.52
21.6
4.83
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.4 BJ
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u u u
u u
u u
u
u
u
DNITS
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.500
0.1
0.3
1.6
0.2
0.015
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/19/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
09/26/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
KMS
KWB
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
Page #: 7
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #3, 5 FT. M-136 Lab ID: 9509020-02A CoUected: 09/11/95 14:56:00
TEST
Volatile Organics
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1, 2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluorometheme
1,2,3- trichloropropcine
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene- d5
1,4-dichlorobenzene- d4
RESDLT
U
u 10 B
U
U
U
U
U
U
u u u 6.7 BJ
U
tJ
U
U
U
U
U
U
U
2.5 BJ
D
U
U
888951
631324
243048
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluoromethane
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
%Recovery
96.1
101
102
104
METHOD/CAS#
SW-846,8260A
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6 ^^
108-38-3 ^^
67-64-1 ^W
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Racovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #32, 2 FT. M-136 Lab ID: 9509020-03A CoUected: 09/11/95 15:30:00
TEST RESDLT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMZ
Nitroglycerine
U MG/KG 0.500 09/19/95 KMS SOP 420
U MG/KG 0.500 09/19/95 KMS SOP 420
Page #: 8
Dctober 18, 1995 10:02
ample ID: GD #32, 2 FT. M-136
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9509020-03A CoUected: 09/11/95 15:30:00
EST RESDLT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
:!id Digestion
admliun
tiromlum
aad
ilver
ercury
olatile Organics
enzene
romobenzene
romochlorome thane
romodichloromethane
romoform
romome theine
-butylbenzene
ec^M|:ylbenzene
er^Httylbenzene
•arbon tetrachloride
hlorobenzene
:hloroe thane
:hloroform
:hlorome thane
-chlorotoluene
-chlorotoluene
libromochloromethane
L,2 -dibromo-3-chloropropan
L,2-dibromoethane
iibromomethane
iichlorodifluoromethane
L,1-dichloroethame
L,2-dichloroethane
'., 1 - di chl or oe thene
:is-1,2-dichloroethene
:rans-1,2-dichloroethene
.,2 -dichloropropane
.,3-dichloropropane
!,2-dichloropropane
.,1-dichloropropene
:is-l,3-dichloropropene
irans-1,3-dichloropropene
.,2-dichlorobenzene
.,3-dichlorobenzene
L,4-dichlorobenzene
ethylbenzene
lexachlorobutadiene
Lsong^y Ibenzene
I - il^^opyltoluene
09/15/95
0.42
19.8
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
1.9 BJ
U
U
U
U
U
U
U
u u u u u u
u
u u u u u
u .
u u u u u
u
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg ,
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.1
0.3
1.6
0.2
0.013
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/15/95
09/19/95
09/19/95
^9/19/95
09/19/95
09/26/95
09/25/SI5
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
KWB
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA.
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
Page #: 9
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #32, 2 FT. M-136 Lab ID: 9509020-03A CoUected: 09/11/95 15:30:00
TEST
Volatile Organics
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,l-trichloroethane
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butomone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4 -di chlorobenzene-d4
RESDLT
8.9 BJ
U
U
U
U
U
U
U
U
U
10 B
3.9
U
U
U
U
U
U
U
U
u
BJ
U
U
U
836124
571826
187362
Surrogate
Surrogate
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
ID
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA.
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
/Recovery Data For Volatile Organics 8260S
dibromofluoromethane
1,2-dichloroetheme-d4
toluene-d8
bromofluorobenzene
%Racovary
99.2
97.8
105
116
METHOD/CAS#
SW-846,8260A
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1 ^^
78-93-3 ^B
108-10-1 ^^
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #32, 5 FT. M-136 Lab ID: 9509020-04A CoUected: 09/11/95 15:42:00
TEST RESXTLT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMZ
Ni troglycerine
Acid Digestion
u
u
09/15/95
MG/KG
MG/KG
DATE
0.500
0.500
09/19/95
09/19/95
09/15/95
KMS
KMS
KWB
SOP 420
SOP 420
SW-846, 3050
Page ft: 10
October 18, 1995 10:02
Sample ID: GD #32, 5 FT. M-136
CERTIFICATE OF AI^J^U^YSIS
' RESULTS BY SAMPLE
Lab ID: 9509020-04A CoUected: 09/11/95 15:42:00
TEST
Cadmitun
Chromiiun
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodichloromethane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
^^^bon tetrachloride
^^^orobenzene
^BR oroe theme
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3 -chloropropan
1,2-dibromoetheme
dibromome theme
dichlorodifluoromethane
1,1-di chloroethane
1,2-dichloroethcme
1,1-dichloroethene
cis-1,2-dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropeme
2,2-dichloropropeme
1,1-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
i^kithalene
RESDLT
u
20.2
U
U
U
U
U
U
U
U
U
U
u u
u 1.6 J
U
1.3 BJ
U
U
U
1.2 J
U
U
U
U
u
u u
u u u D
U
U
U
u u u u u
u u
u 4.7 BJ
U
DNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
1.6
0.2
0.014
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/19/95
09/19/95
09/19/95
09/19/95
09/26/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
Page#: 11
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #32, 5 FT. M-136 Lab ID: 9509020-04A CoUected: 09/11/95 15:42:00
TEST
Volatile Organics
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroethane
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESDLT
8.0
4.7
U
U
U
U
U
U
U
O
BJ
U
U
U
U
U
U
U
U
U
BJ
U
U
U
956729
691896
266045
Surrogate
Surrogate
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
/Recovery Data For Volatile Organics 8260S
dibromofluoromethane
1,2-dichloroethcme-d4
toluene-d8
bromofluorobenzene
%Racovery
97.1
99.2
100
105
METHOD/CAS#
SW-846,8260A
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1 ^^
591-78-6 ^^
INTSTDl ^W
1NTSTD2
INTSTD3
Recovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #52, 2 FT. M-136 Lab ID: 9509020-05A CoUected: 09/12/95 07:45:00
TEST RESDLT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMZ
Kltroglycerlne
Acid Digestion
Cadmium
u
u
09/15/95
0.25
MG/KG
MG/KG
DATE
ug/g
0.500
0.500
0.1
09/19/95
09/19/95
09/15/95
09/19/95
KMS
KMS
KWB
LVD
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
Page #: 12
October 18, 1995 10:02
Sample ID: GD #52, 2 FT. M-136
CERTIFICATE OF AN^O^YSIS
^ RESULTS BY SAMPI.E
Lab ID: 9509020-05A CoUected: 09/12/95 07:45:00
TEST
Chromiiun
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodi chloromethane
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
^al oroe thane
J^^oroform
^^H orome theme
~2- chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3-chloropropan
1,2-dibromoetheme
dibromomethcme
dichlorodifluoromethane
1,1-dichloroethane
1,2 -di chloroetheme
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropane
2,2-dichloropropeme
1,1-dichloropropene
cis-1,3 -dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachl orobut adi ene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
l^^trene
RESULT
14.8
5.27
U
0.03
U
U
U
a
U
U
u u u u 1.3 J
U
1.9 BJ
U
U
U
1.3 J
U
U
U
U
U
U
U
U
U
u D
U
. u U
U
U
U
u u u u
u 5.3 BJ
U
U
U
DNITS
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.3
1.5
0.2
0.01,4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/19/95
09/19/95
09/19/95
09/26/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA.
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
Page #: 13
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #52, 2 FT. M-136 Lab ID: 9509020-05A CoUected: 09/12/95 07:45:00
TEST
Volatile Organics
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tet rachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m, p-xylene
acetone
2-butcmone
4 -methyl - 2 -pentemone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESDLT
U
U
u 1.1 J
u
u 1.8 BJ
U
U
U
U
U
U
U
U
U
3.9 BJ
U
U
U
962566
670345
245730
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorometheme
1,2-di chl oroe theme - d4
toluene-d8
bromofluorobenzene
%Recovary
97.2
101
103
110
METHOD/CAS#
SW-846,8260A
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl ^^
INTSTD2 ^A
INTSTD3 ^^
Racovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #52, 5 FT. M-136 Lab ID: 9509020-06A CoUected: 09/12/95 08:05:00
TEST RESDLT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMZ
Ni troglycerlne
Acid Digestion
Cadmium
Chromium
u
u
09/15/95
U
18.3
MG/KG
MG/KG
DATE
ug/g
ug/g
0
0
.500
.500
0.1
0.3
09/19/95
09/19/95
09/15/95
09/19/95
09/19/95
KMS
KMS
KWB
LVD
LVD
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
Page #: 14
October 18, 1995 10:02
Sample ID: GD #52, 5 FT. M-136
CERTIFICATE OF AN/kLYSIS
^ RESULTS BY SAMPLE
Lab ID: 9509020-06A CoUected: 09/12/95 08:05:00
TEST
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodi chlorome thane
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorometheme
Jl^chlorotoluene
^^Hhlorotoluene
^bromochloromethane
1,2-dibromo-3-chloropropem
1,2-dibromoetheme
dibromomethcme
dichlorodifluorometheme
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2 -dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropeme
2,2-dichloropropane
1,1-dichloropropene
cis-1,3 -dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
J^L,2,2-tetrachloroethane
RESDLT
u
u
u
u u
u
u u
u u u u u u u 2.2 BJ
U
U
U
U
U
U
U
U
u u u u u u u u
u
u
u u u u u
u u
u 4.4 BJ
U
U
U
U
u
DNITS
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
1.6
0.2
0.015
Id
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANJ^LYZED
09/19/95
09/19/95
09/26/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
Page #: 15
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #52, 5 FT. M-136 Lab ID: 9509020-06A CoUected: 09/12/95 08:05:00
TEST
Volatile Organics
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4 -methyl - 2 -pentcuione
2 -hexemone
fluorobenzene
chlorobenzene-d5
1,4 -di chlorobenzene-d4
RESDLT
U
U
u u
u
u u
u
u
u u u u u 3.3 BJ
U
U
U
928557
664841
259191
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluoromethane
1 ,2-dichloroe theme-d4
toluene-d8
bromofluorobenzene
%Recovery
97.1
99.6
100
104
METHOD/CAS#
SW-846,8260A
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3 ^^
w
Recovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #74, 2 FT. M-136 Lab ID: 9509020-07A CoUected: 09/12/95 08:27:00
TEST RESULT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMZ
Nltroglycerlne
Acid Digestion
Cadmiiun
Chromiiun
Lead
u
u
09/15/95
U
13.5
U
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
0
0
.500
-500
0.1
0.3
1.6
09/19/95
09/19/95
09/15/95
09/19/95
09/19/95
09/19/95
KMS
KMS
KWB
LVD
LVD
LVD
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
Page #: 16
October 18, 1995 10:02
•
Sample ID: GD #74, 2 FT. M-136
CERTIFICATE OF A>f^J.YSIS
RESULTS BY SAMPLE
Lab ID: 9509020-07A CoUected: 09/12/95 08:27:00
TEST
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodichloromethane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
yW|romochlorome thane
I^B-dibromo-3-chloropropem
^^ - dibromoe theme
dibromomethane
dichlorodifluoromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropane
2,2-dichloropropane
1,1-dichloropropene
cis-1,3 -dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachl orobut adi ene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
^^^uene
ABL 3 - trichlorobenzene
RESDLT
U
0.03
U
U
U
U
u u u
u
u u
u u 37
U
U
U
U
U
U
U
u u u u u u u
u u u u u u u u u D
u u
u u u u u u u u u
DNITS
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.2
0.015
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANJILYZED
09/19/95
09/26/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
Page #: 17
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #74, 2 FT. M-136 Lab ID: 9509020-07A CoUected: 09/12/95 08:27:00
TEST
Volatile Organics
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-but6mone
4 -methyl - 2 -pentemone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESDLT
U
U
U
U
U
U
U
U
U
U
U
U
U
u tr 1002072
531263
126749
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorometheme
1 ,2-dichloroetheme-d4
toluene-d8
bromofluorobenzene
%Recovary
94.5
90.4
118
122
METHOD/CAS#
SW-846,8260A
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits ^^^
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #74, 5 FT. M-136 Lab ID: 9509020-08A CoUected: 09/12/95 08:46:00
TEST RESDLT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMZ
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
u
' u
09/15/95
0.77
17.3
2.00
U
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
0
0
.500
.500
0.1
0.3
1.5
0.2
09/19/95
09/19/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
KMS
KMS
KWB
LVD
LVD
LVD
LVD
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Page #: 18
October 18, 1995 10:02 CERTIFICATE OF AN^^LLYSIS
:i RESULTS BY SAMPLE
Sample ID: GD #74, 5 FT. M-136 Lab ED: 9509020-08A CoUected: 09/12/95 08:46:00
TEST RESULT DNITS DETECTION ANJILYZED BY
LIMIT
METHOD/CAS#
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chloromethane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenz ene
chloroetheme
chloroform
chlorome thane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropan
1^2' dibromoe theme
^^^ omome theme
^PJHilorodifluoromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-l,2-dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropeme
2,2-dichloropropane
1,1-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
kl-trichloroetheme
U ug/g
u
u
u u
u u u
u u u u u 55
u u u ..
u u u u u. u
u u
u u
u u • u
u V
u u u
u
u
u u
u
u u u u u u u u u u .9 J
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
115
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 '
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/26/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/:J5/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/;J5/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/::5/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
Page #: 19
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #74, 5 FT. M-136 Lab ID: 9509020-08A CoUected: 09/12/95 08:46:00
TEST
Volatile Organics
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentemone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4 -di chlorobenzene-d4
RESDLT
U
U
u u
u u u
u u u u
u u 652857
331655
105535
Surrogate
Surrogate
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
!/Recovery Data For Volatile Organics 8260S
dibromofluoromethane
1 ,2 -di chloroetheme-d4
toluene-d8
bromofluorobenz sne
%Recovery
85.8
78.0
119
105
METHOD/CAS#
SW-846,8260A
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits _
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
^ V
Sample ID: GD #19, 2 FT. M-136 Lab ID: 9509020-09A CoUected: 09/12/95 09:10:00
TEST RESDLT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMZ
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
u
u
09/15/95
0.25
18.9
U
U
U
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
0
0
0
.500
.500
0.1
0.3
1.6
0.2
.013
09/19/95
09/19/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
09/26/95
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
Page #: 20
October 18, 1995 10:02
•
Sample ID: GD #19, 2 FT. M-136
CERTIFICATE OF AT^^d^YSIS
RESULTS BY SAMPLE
Lab ID: 9509020-09A CoUected: 09/12/95 09:10:00
TEST
Volatile Organics
benzene
bromobenzene
bromoch1orome theme
bromodichloromethane
bromoform
bromome thane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3 -chloropropem
1,2-dibromoethane
dibromomethane
i^chl orodifl uorome thane
m^^ - di chl oroe theme
^^E-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropane
2,2-dichloropropeme
1,1-dichloropropene
cis-1,3 -dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 - isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,l-trichloroethane
1,1,2 -trichloroethane
d^kphloroe thene
RESDLT
U
U
u u
u u u
u u u u u 31
u u u u u u u u u u u u u D
u u u u u u u u
u u u u u u u u u u u u
u u 5.2 J
u
u
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
AN.IVLYZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
Page #: 21
October 18, 1995 10:02
miple ID: GD #19, 2 FT. M-136
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9509020-09A CoUected: 09/12/95 09:10:00
EST
}latile Organics
.-ichlorof luorome theme
.2,3-trichloropropane
.2,4-trimethylbenzene
.3,5-trimethylbenzene
Lnyl chloride
-xylene
,p-xylene
retone
-butemone
-methyl - 2 -pentemone
-hexemone
Luorobenzene
llorobenzene-d5
,4-dichlorobenzene-d4
RESULT
D
U
U
U
U
U
U
U
u u u 727149
352428
95187
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluoromethane
1 ,2 -di chloroethane-d4
toluene-d8
bromofluorobenzene
%Recovery
86.2
79.6
125
113
METHOD/CAS#
SW-846,8260A
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125 i \
ample ID: GD #19, 5 FT. M-136 Lab ID: 9509020-lOA CoUected: 09/12/95 09:23:00
EST
MZ
1troglycerine
cid Digestion
admium
hromlum
aad
ilvar
ercury
olatile Organics
enzene
RESDLT
U
U
09/15/95
0.75
17.7
3.11
U
U
U
DNITS
MG/KG
MG/KG
DATB
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
DETECTION
LIMIT
0.500
0.500
0.1
0.3
1.5
0.2
0.015
10
ANALYZED
09/19/95
09/19/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
09/26/95
09/25/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
METHOD/CAS#
SOP
SOP
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
71-43-2
420
420
3050
6010
6010
6010
6010
7471
8260A
d
Page #: 22
October 18, 1995 10:02
Sample ID: GD #19, 5 FT. M-136
CERTIFICATE OF ANCLLYSIS
RESULTS BY SAMPLE
Lab ID: 9509020-lOA CoUected: 09/12/95 09:23:00
TEST RESDLT DNITS DETECTION ANi^YZED BY
LIMIT
METHOD/CAS#
Volatile Organics
bromobenzene
bromochloromethane
bromodi chlorome theme
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3-chloropropem
1,2-dibromoethane
dibromometheme
dichlorodifluoromethane
1^1-dichloroethane
^•|-dichloroe theme
^^•-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropeme
2,2-dichloropropane
1,1-dichloropropene
cis-1, 3-dichloropropene
trans-l,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroetheme
trichloroethene
Lchlorofluorome thane
#
u
u u u u
u u u
u u u 14
u u u u u u u u o u u u u u u u u u u u u u u u u u . u
u u u u u u u u u 6.3 J
u u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/:25/95
09/;J5/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
Page #: 23
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #19, 5 FT. M-136 Lab ID: 9509020-lOA CoUected: 09/12/95 09:23:00
TEST
Volatile Organics
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentanone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESDLT
u
u u u u
u u u
u u 698024
404892
122028
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
MMR
MMR
wm MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatila Organics 8260S
Surrogate
dibromofluorometheme
1 ,2 -dichloroetheme-d4
toluene-d8
bromofluorobenzene
%Racovery
84.0
78.1
115
110
METHOD/CAS#
SW-846,8260A
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Iilmlts
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125 ^^^
Sample ID: GD #104, 2 FT. M-136 Lab ID: 9509020-11A CoUected: 09/12/95 10:25:00
TEST
HMZ
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
RESDLT
U
u
09/15/95
0.73
17.9
2.70
U
U
U
U
UNITS
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
DETECTION
LIMIT
0.500
0.500
0.1
0.3
1.7
0.2
0.014
10
10
ANALYZED
09/19/95
09/19/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
09/26/95
09/25/95
09/25/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
METHOD/CAS#
SOP
SOP
SW-846
SW-846
SW-846
SW-846,
SW-846,
SW-846,
SW-846,
71-43-2
108-86-
420
420
3050
6010
6010
6010
6010
7471
8260A
Page #: 24
October 18, 1995 10:02
Sample ID: GD #104, 2 FT. M-136
CERTIFICATE OF AN^LLYSIS
RESULTS BY SAMPLiE k-i,
Lab ID: 9509020-11A CoUected: 09/12/95 10:25:00
TEST
Volatile Organics
bromochloromethane
bromodichlorometheme
bromoform
bromome thane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropan
1,2-dibromoethane
dibromomethane
dichlorodifluorometheme
1,1-dichloroethane
^ll^ -dichloroe theme
J^B - di chl oroe thene
TIR -1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropane
1,1-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n -propylbenzene
styrene
1,1,1,2- tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroetheme
trichloroethene
trichlorofluorometheme
j^^, 3 - trichloropropane
RESULT
u
u u u u u u u u u 55
U
U
U
"u U
U
U
u u u u u u u
u
u u u
u u u u
u
u u
u D
u D
U
u u u
u
u u 4.6 J
U
U
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANJ^YZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-4G-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
Page #: 25
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #104, 2 FT. M-136 Lab ID: 9509020-llA CoUected: 09/12/95 10:25:00
TEST
Volatila Organics
RESULT
1,2,4-trimethylbenzene U
1,3,5-trimethylbenzene U
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4 -di chlorobenz ene-<
U
u u
u u u u 401677
226153
34 77919
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
ID
10
10
ANALYZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromof luorome thauie
1,2-dichloroetheme-d4
toluene-d8
bromofluorobenzene
%Racovery
82.3
77.9
117
104
METHOD/CAS#
SW-846, 8260A
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #104, 5 FT. M-136 Lab ID: 9509020-12A CoUected: 09/12/95 10:30:00
TEST
HMZ
Ni troglycerlne
Acid Digestion
Cadmium
Chromium
Lead
Silvar
Mercury
Volatila Organics
benzene
bromobenzene
bromochloromethane
RESULT
U
u
09/15/95
0.24
19.5
2.58
U
U
U
u
u
UNITS
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.500
0.500
0.1
0.3
1.5
0.2
0.015
10
10
10
ANALYZED
09/19/95
09/19/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
09/26/95
09/25/95
09/25/95
09/25/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
METHOD/CAS#
SOP
SOP
SW-846,
SW-846,
SW-846,
SW-846,
SW-84 6,
SW-846,
SW-846,
71-43-2
108-86-
74-97-5
420
420
3050
6010
6010
6010
6010
7471
8260A
1
Page #: 26
October 18, 1995 10:02
Sample ID: GD #104, 5 FT. M-136
CERTIFICATE OF AT^^ILYSIS
RESULTS BY SAMPLE
Lab ID: 9509020-12A CoUected: 09/12/95 10:30:00
TEST
Volatila Organics
bromodichloromethane
bromoform
bromomethane
n-butyIbenz ene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropem
1,2-dibromoethane
dibromometheme
dichlorodifluorometheme
1,1-dichloroetheme
1,2-dichloroetheme
^1^1 - dichloroethene
J^B -1,2- dichloroethene
^^Rms -1,2-dichloroethene
.1,2-dichloropropame
1,3-dichloropropame
2,2-dichloropropame
1,1-dichloropropene
cis-1,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroethane
trichloroethene
trichlorofluorometheme
3^2,3-trichloropropane
jfft|,4 -trimethylbenzene
RESULT
U
u u u u u u u
u 38
u u u u u
u u u u u u u u u
u u
u
u u u u u V
u u
u u u
u u
u u u u
u
u 3.2 J
u u u .
u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ilNALYZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6-
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
Page #: 27
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #104, 5 FT. M-136 Lab ID: 9509020-12A CoUected: 09/12/95 10:30:00
TEST
Volatila Organics
RESULT
1,3,5-trimethylbenzene U
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butcmone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-
U
U
o u
u u
u 579909
305775
d4 99473
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
ANALYZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
Surrogate/Recovery Data For Volatile Organic
Surrogate
dibromofluoromethane
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
%Racovary
72.9 Q
69.2 Q
125
108
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
3 8260S
METHOD/CAS#
SW-846,8260A
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #120, 2 FT. M-136 Lab ID: 9509020-13A CoUected: 09/12/95 10:50:00
TEST
HMZ
Ni troglycerlne
Acid Digestion
Cadmium
Chromiiun
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodichloromethane
RESULT
U
u
09/15/95
0.41
19.7
U
a
U
u
u u
u
UNITS
MG/KG
M3/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.500
0.500
0.1
0.3
1.5
0.2
0.013
10
10
10
10
ANALYZED
09/19/95
09/19/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
09/26/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
METHOD/CAS#
SOP
SOP
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
71-43-2
108-86-
74-97-5
75-27-4
420
420
3050
6010
6010
6010
6010
7471
8260A
L
^^
Page #: 28
October 18, 1995 10:02
Sample ID: GD #120, 2 FT. M-136
CERTIFICATB: OF AIV^^LYSIS
RESULTS BY SAMPLE;
Lab ID: 9509020-13A CoUected: 09/12/95 10:50:00
TEST RESULT UNITS DETECTION JI^'ALYZED BY
LIMIT
METHOD/CAS#
Volatila Organics
bromoform
bromome thane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropan
1,2-dibromoethane
dibromomethane
dichlorodifluorometheme
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
^^s -1,2- dichloroethene
fl^nms -1,2-dichloroethene
^B^ -dichloropropeme
1,3-dichloropropane
2,2-dichloropropane
1,1-dichloropropene
cis-1,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,5-trimethylbenzene
u
u u u u u u u 13
U
u
u
u
u u u u u
u
u u u
u u a u u u u u u u u u u u u u
u u u
u u u u J
u
u u
u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
SW-846,8260A
10 09/25/95 MMR 75-25-2
10 09/25/95 MMR 74-83-9
10 09/25/95 MMR 104-51-8
10 09/25/95 MMR 135-98-8
10 09/25/95 MMR 98-06-6
10 09/25/95 MMR 56-23-5
10 09/25/95 MMR 108-90-7
10 09/25/95 MMR 75-00-3
10 09/25/95 MMR 67-66-3
10 09/25/95 MMR 74-87-3
10 09/25/95 MMR 95-49-8
10 09/25/95 MMR 106-43-4
10 09/25/95 MMR 124-48-1
10 09/25/95 MMR 96-12-8
10 09/25/95 MMR 106-93-4
10 09/25/95 MMR 74-95-3
10 09/25/95 MMR 75-71-8
10 09/25/95 MMR 75-34-3
10 09/25/95 MMR 107-06-2
10 09/25/95 MMR 75-35-4
10 09/25/95 MMR 156-59-4
10 09/25/95 MMR 156-60-5
10 09/25/95 MMR 78-87-5
10 09/25/95 MMR 142-28-9
10 09/25/95 MMR 590-20-7
10 09/25/95 MMR 563-58-6
10 09/25/95 MMR 10061-01-5
10 09/25/95 MMR 10061-02-6
10 09/25/95 MMR 95-50-1
10 09/25/95 MMR 541-73-1
10 09/25/95 MMR 106-46-7
10 09/25/95 MMR 100-41-4
10 09/25/95 MMR 87-68-3
10 • 09/25/95 MMR 98-82-8
10 09/25/95 MMR 99-87-6
10 09/25/95 MMR 75-09-2
10 09/25/95 MMR 91-20-3
10 09/25/95 MMR 103-65-1
10 09/25/95 MMR 100-42-5
10 09/25/95 MMR 630-20-6
10 09/25/95 MMR 79-34-5
10 09/25/95 MMR 127-18-4
10 09/25/95 MMR 108-88-3
10 09/25/95 MMR 87-61-6
10 09/25/95 MMR 120-82-1
10 09/25/95 MMR 71-55-6
10 09/25/95 MMR 79-00-5
10 09/25/95 MMR 79-01-6
10 09/25/95 MMR 75-69-4
10 09/25/95 MMR 96-18-4
10 09/25/95 MMR 95-63-6
10 09/25/95 MMR 108-67-8
Page #: 29
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #120, 2 FT. M-136 Lab ID: 9509020-13A CoUected: 09/12/95 10:50:00
TEST
Volatile Organics
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentanone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-
RESULT
U
U
u u u
u
u 413377
253077
d4 85851
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
IJO
ANALYZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatila Organics 8260S
Surrogate
dibromofluoromethane
1,2-dichloroethane-d4
toluene-d8
bromof1uorobenzene
%Recovary
79.7
75.6
116
109
METHOD/CAS#
SW-846,8260A
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #120, 5 FT. M-136 Lab ID: 9509020-14A CoUected: 09/12/95 10:55:00
TEST
HMZ
Nltroglycerlne
Acid Digestion
Cadmium
Chromium
Lead
Silvar
Marcury
Volatila Organics
benzene
bromobenzene
bromochlorometheme
bromodichloromethane
bromoform
RESULT
U
U
09/15/95
0.26
19.4
U
U
0.01
U
U
U
U
U
UNITS
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0
0
0
.500
.500
0.1
0.3
1.6
0.2
.010
10
10
10
10
10
ANALYZED
09/19/95
09/19/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
09/26/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SOP '
SOP '
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
71-43-2
108-86-]
74-97-5
75-27-4
75-25-2
120
120
3050
6010
6010
6010
6010
7471
8260A
^^
Page #: 30
October 18, 1995 10:02
Sample ID: GD #120, 5 FT. M-136
CERTIFICATE OF AN^O^YSIS
RESULTS BY SAMPLE
Lab ID: 9509020-14A CoUected: 09/12/95 10:55:00
TEST
Volatile Organics
bromomethane
n-butyIbenz ene
sec-butyIbenz ene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo- 3 -chloropropan
1,2-dibromoethane
dibromometheme
di chlorodi fluorome theme
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-l,2-dichloroethene
^yrans-1,2-dichloroethene
^Be -dichloropropeme
^B^ - dichloropropane
2,2-dichloropropeme
1,1-dichloropropene
cis-l,3-dichloropropene
trans-1,3-dichloropropene
1,2 -di chlorobenz ene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadi ene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethane
te trachloroe thene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroetheme
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
i^ftnyl chloride
RESULT
U
u u u u u u 8 J
u u u u u
u u u u u u u u u
u
u
u u u
u u u u
u u u u
u u u u u u
u
o u 6 J
u u u u u
u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
iVNALYZED
09/25/95
.09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
Page #: 31
October 18, 1995 10:02
Sample ID: GD #120, 5 FT. M-136
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9509020-14A CoUected: 09/12/95 10:55:00
TEST
Volatile Organics
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentanone
2 - hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-
RESULT
U
u u u
u u 572806
319752
d4 106326
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
ANALYZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
Surrogate/Recovery Data For Volatila Organic
Surrogate
dibromof luorcxne theme
1,2 -dichloroetheme-d4
toluene-d8
bromofluorobenzene
%Racovery
75.5
75.4
122
108
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
a 8260S
METHOD/CAS#
SW-846,8260A
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #150, 2 FT. M-136 Lab ED: 9509020-15A CoUected: 09/12/95 11:10:00
TEST
HMZ
Nl troglycerlne
Acid Digestion
Cadmiiun
Chromiiun
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodi chlorome theme
bromoform
bromometheme
RESULT
o
u
09/15/95
U
19.8
U
U
U
U
U
U
U
U
U
UNITS
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0
0
0
.500
.500
0.1
0.3
1.6
0.2
.017
10
10
10
10
10
10
ANALYZED
09/19/95
09/19/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
09/26/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SOP '
SOP '
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
71-43-2
120
120
3050
6010
6010
6010
6010
7471
8260A
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9 j0|k
Page #: 32
October 18, 1995 10:02
'^l
Sample ID: GD #150, 2 FT. M-136
CERTIFICATE OF A?H[^d.YSIS
RESULTS BY SAMPLE
Lab ID: 9509020-15A CoUected: 09/12/95 11:10:00
TEST
Volatila Organics
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
ch1oromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropan
1,2-dibromoethane
dibromomethane
di chlorodi fluoromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trems-1,2-dichloroethene
^^-dichloropropane
^B|-di chloropropane
^^P^-di chl oropropane
1,1-dichloropropene
cis-l,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
j^^lene
RESULT
U
u u u u
u 20
u
u
u u
u u u "u u u u u
u u u u . u
u u u u u u
u u
u
u u
u 0
u . u
u u u u 7 J
u u u
u
u u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
J!LN.I^YZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
Page #: 33
October 18, 1995 10:02
Sample ID: GD #150, 2 FT. M-136
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9509020-15A CoUected: 09/12/95 11:10:00
TEST
Volatila Organics
m,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-
RESULT
U
u
u
u
u 492396
269430
d4 74167
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
-
ANALYZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatila Organics 8260S
Surrogate
dibromofluoromethane
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
%Recovary
76.1
75.9
122
116
METHOD/CAS#
SW-846,8260A
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #150, 5 FT. M-136 Lab ID: 9509020-16A CoUected: 09/12/95 11:20:00
TEST
HMZ
Ni troglycerlne
Acid Digestion
Cadmium
Chromium
Lead
Silvar
Marcury
Volatila Organics
benzene
bromobenzene
bromochloromethane
bromodi chlorome theme
bromoform
bromomethane
•n-butylbenzene
RESULT
U
u
09/15/95
0.34
19.1
2.06
U
U
U
U
U
U
U
U
U
UNITS
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0
0
0
.500
.500
0.1 •
0.3
1.6
0.2
016
10
10
10
10
10
10
10
ANALYZED
09/19/95
09/19/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
09/26/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SOP 420
SOP 420
SW-846,
SW-84 6,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,(
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
3050
6010
6010
6010
6010
7471
3260A
^K
Page #: 34
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #150, 5 FT. M-136 Lab ED: 9509020-16A CoUected: 09/12/95 11:20:00
TEST
Volatile Organics
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3-chloropropan
1,2-dibromoethane
dibromomethane
dichlorodifluorometheme
1,1-dichloroetheme
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2-dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropane
^^ -dichloropropeme
1^^ - di chloropropane
*|^PI - di chl oropropene
cis-1, 3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4-i sopropyltoluene
methylene chloricle
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
^^1^-xylene
RESULT
u u u u u 5 J
U
U
U
U
U
u u u u
u u u u u u u u u u u u u u u u
u u u u
u u u u u u u 5 J
u u u u
u u u u
u
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Al^ALYZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/:>5/95
09/25/95
09/25/95
09/:>5/95
09/25/95
09/25/95
09/25/95
09/:25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
Page #: 35
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #150, 5 FT. M-136 Lab ID: 9509020-16A CoUected: 09/12/95 11:20:00
TEST
Volatila Organics
acetone
2-butemone
4-methyl-2-pentanone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
u u
u u 448985
270848
87961
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
ANALYZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Surrogate/Recovery Data For Volatila Organics 8260S
Surrogate
dibromofluorometheme
1,2-dichloroetheme-d4
toluene-d8
bromofluorobenzene
%Racovery
78.7
80.2
117
106
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Sample ID: GD #179, 2 FT. M-136 Lab ID: 9509020-17A
TEST RESULT UNITS DETECTION ANALYZED
LIMIT
BY
CoUected: 09/12/95
METHOD/CAsi^P
HMZ
Ni troglycerlne
Acid Digestion
Cadmium
Chromium
Lead
Silvar
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chlorometheme
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
U
U
09/15/95
0.
23
35
.7
U
U
U
U
U
U
u u u u
u
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.500
0.500
0.1
0.3
1.6
0.2
0.016
10
10
10
10
10
10
10
10
09/19/95
09/19/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
09/26/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
Page #: 36
October 18, 1995 10:02
Sample ID: GD #179, 2 FT. M-136
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9509020-17A CoUected: 09/12/95
TEST
Volatile Organics
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropem
1,2-dibromoetheme
dibromometheme
dichlorodifluorometheme
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1, 2-dichloroethene
trans-l,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropeme
2_, 2 -dichloropropeme
1^^ - di chloropropene
^^^-1,3-dichloropropene
'trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
jafttone
RESULT
U
U
u u 49
U
u u u u
u u
u u
u
u u
u u u u u u u u u u
u u u u u
u u u
u u u u u u 5 J
u u u u
u u u u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
lb 10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANJLLYZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
Page #: 37
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #179, 2 FT. M-136 Lab ID: 9509020-I7A CoUected: 09/12/95
TEST
Volatila Organics
2-butanone
4-methyl-2-pentanone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-
RESULT
U
u
u 406533
229271
d4 77310
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
ANALYZED BY
09/25/95 MMR
09/25/95 MMR
09/25/95 MMR
09/25/95 MMR
09/25/95 MMR
09/25/95 MMR
Surrogate/Recovery Data For Volatila Organics 8260S
Surrogate
dibromofluoromethane
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
%Recovary
78.7
76.2
119
106
METHOD/CAS#
SW-846,8260A
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
1NTSTD3
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Sample ID: GD #179, 5 FT. M-136 Lab ID: 9509020-18A CoUected: 09/12/95 11:40:00
TEST
HMZ
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Marcury
Volatila Organics
benzene
bromobenzene
bromochloromethane
bromodi chloromethane
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
RESULT
U
u
09/15/95
0.25
22.3
U
U
U
U
U
U
U
U
U
U
U
U
UNITS
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0
0
0
.500
.500
0.1
0.3
1.5
0.2
.016
10
10
10
10
10
10
10
10
10
ANALYZED
09/19/95
09/19/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
09/26/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS 4t^ V
SOP 420
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6 ^^^
Page #: 38
October 18, 1995 10:02 CERTIFICATE OF A?^^lLYSIS
RESULTS BY SAMPLE
Sample ID: GD #179, 5 FT. M-136 Lab ID: 9509020-18A CoUected: 09/12/95 11:40:00
TEST
Volatile Organics
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo- 3 -chloropropem
1,2-dibromoethane
dibromomethane
dichlorodifluorometheme
1,1-dichloroetheme
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropeme
2,2-dichloropropane
1,1-dichloropropene
^ba -1,3- dichloropropene
^^Pns -1, 3 - di chloropropene
r; 2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
i sopropylbenzene
4-isopropyltoluene
methylene chloride
naphthalene
n-propyIbenz ene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m, p-xylene
acetone
^butanone
RESULT
u u u 74
U
U
U
U
u u u u u
u u u u u u .
u u u u u u u u u u
u u u
u u u u u u u u 4 J
u u u
u
u u u u u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
. ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 .
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
J!LNJIU^YZED
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
Page #: 39
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #179, 5 FT. M-136 Lab ID: 9509020-18A CoUected: 09/12/95 11:40:00
TEST
Volatile Organics
4-methyl-2-pentemone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-
RESULT
U
u 380397
225324
d4 84340
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
ANALYZED BY
09/25/95 MMR
09/25/95 MMR
09/25/95 MMR
09/25/95 MMR
09/25/95 MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorometheme
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
^Recovery
78.4
78.8
115
97.3
METHOD/CAS#
SW-846,8260A
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Sample ID: GD #156, 2 FT. M-136 Lab ID: 9509020-19A CoUected: 09/12/95 13:26:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMZ
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chloromethane
bromoform
bromome theme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
,carbon tetrachloride
u
D
09/15/95
0.34
23.5
U
U
U
U
U
D
U
U
U
U
U
U
U
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.500
0.500
0.1
0.3
1.6
0.2
0.014
10
10
10
10
10
10
10
10
10
10
09/19/95
09/19/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
09/26/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
Page #: 40
October 18, 1995 10:02
Sample ID: GD #156, 2 FT. M-136
CERTIFICATE OF AI^JiiLLYSIS
RESULTS BY SAMPLE
Lab ID: 9509020-19A CoUected: 09/12/95 13:26:00
TEST RESULT UNITS DETECTION JJNJU.YZED BY
LIMIT
METHOD/CAS#
Volatila Organics
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3 -chloropropem
1,2-dibromoetheme
dibromomethcme
dichlorodifluoromethane
1,1-dichloroetheme
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2 -dichloropropane
1,3-dichloropropane
2,2-dichloropropeme
1,1-dichloropropene
cis-1, 3 -dichloropropene
^Buis -1,3- dichloropropene
^^B-dichlorobenzene
^^ -dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
u
u
u
u u
u u u
u u u
u u u u u u u u u u u u u u u u u u u
u u
u u u
u
u u
u 15
u
u u
u u u u u u u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
Page #: 41
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #156, 2 FT. M-136 Lab ID: 9509020-19A CoUected: 09/12/95 13:26:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene
U
691158
357635
•d4 87991
Surrogate/Re
Surrogate
ug/Kg
ug/Kg
ug/Kg
ug/Kg
covery Data
dibromofluorometheme
1,2 -di chloroetheme-d4
toluene-d8
bromofluorobenzene
SW-846,8260A
10 09/25/95 MMR 591-78-6
09/25/95 MMR INTSTDl
09/25/95 MMR INTSTD2
09/25/95 MMR INTSTD3
For Volatile Organics 8260S
%Recovary Recovery Limits
77.8 75.0 TO 125
78.9 75.0 TO 125
125 75.0 TO 125
125 75.0 TO 125
Sample ID: GD #156, 5 FT. M-136 Lab ID: 9509020-20A CoUected: 09/12/95 13:35:00
TEST
HMZ
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silvar
Marcury
Volatila Organics
benzene
bromobenzene
bromochlorometheme
bromodi chloromethane
bromoform
bromome theme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
RESDLT
D
U
09/15/95
U
21.4
U
D
D
D
U
U
U
U
U
U
U
U
U
U
UNITS
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0
0
0
.500
.500
0.1
0.3
1.6
0.2
.014
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/19/95
09/19/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
09/26/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
^^
SOP 420 ^^
SOP 420
SW-846,
SW-846,
SW-846,
SW-84e,
SW-846,
SW-846,
3050
6010
6010
6010
6010
7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2 '
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7 —
Page #: 42
October 18, 1995 10:02
•
Sample ID: GD #156, 5 FT. M-136
CERTIFIC:ATE OF AP^f^^lLYSIS
RESULTS BY SAMPLE
Lab ID: 9509020-20A CoUected: 09/12/95 13:35:00
TEST RESULT UNITS DETECTION il^JIkLYZED BY
LIMIT
METHOD/CAS#
Volatila Organics
chloroetheme
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3-chloropropem
1,2-dibromoetheme
dibromomethane
dichlorodifluorometheme
1,1-dichloroetheme
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2-dichloroethene
trans-l,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropeme
2,2-dichloropropane
1,1-dichloropropene
cis-1,3-dichloropropene
trems-1,3-dichloropropene
^^2 -dichlorobenzene
I^^P -dichlorobenzene
^^4 -dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2- tetrachloroe theine
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1, l-trichloroethane
1,1,2-trichloroetheme
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentemone
^hexemone
•
u
u u u u u u u
u u u
u u u
u u
u u u
u u u
u u
u
u u u
u u u u u u u u u u 8 J
• u
u u u u u o u u u u
u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
Page #: 43
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #156, 5 FT. M-136 Lab ID: 9509020-20A CoUected: 09/12/95 13:35:00
TEST RESXTLT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
fluorobenzene
chlorobenzene-d5 1,4-dichlorobenzene-d4
584032 ug/Kg
290573 ug/Kg
68185 ug/Kg
Surrogate/Recovery Data
Surrogate
dibromofluoromethane
1,2-dichloroetheme-d4
toluene-d8
bromofluorobenzene
SW-846,8260A
09/25/95 MMR INTSTDl
09/25/95 MMR INTSTD2
09/25/95 MMR INTSTD3
For Volatila Organics 8260S
%Recovary Recovery Limits
78.8 75.0 TO 125
75.4 75.0 TO 125
125 75.0 TO 125
123 75.0 TO 125
Sample ID: GD #205, 2 FT. M-136 Lab ID: 9509020-21A CoUected: 09/12/95 13:51:00
TEST
HMZ
Nltroglycarine
Acid Digestion
Cadmium
Chromium
Lead
Silvar
Marcury
Volatila Organics
benzene
bromobenzene
bromochlorome theme
bromodi chloromethane
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
RESULT
U
u
09/15/95
U
18.6
2.25
U
U
U
U
U
U
U
U
U
U
U
U
U
U
UNITS
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0
0
0
.500
.500
0.1
0.3
1.6
0.2
.013
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/19/95
09/19/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SOP 420 ^^
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3 ^^^
Page #: 44
October 18, 1995 10:02 CERTIFIC:ATE OF AJ^^^LLYSIS
RESULTS BY SAMPLE
Sample ID: GD #205, 2 FT. M-136 Lab ID: 9509020-21A CoUected: 09/12/95 13:51:00
TEST RESULT UNITS DETECTION J!^J\LYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3-chloropropem
1,2-dibromoetheme
dibromomethane
di chlorodi f1uorome theme
1,1-dichloroetheme
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2 -dichloropropane
1,3-dichloropropane
2,2-dichloropropane
1,1-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
/^ki -dichlorobenzene
^^^B - di chl orobenz ene
^ffnylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl- 2-pentanone
2-hexanone
f^orobenzene §
u
u u u u u u u
u u u u u u u
o u u u u u u u u u u u u
u u
u u
u u u
u u 12 B
u u u
u u u u u u u u u u 989084
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
ID
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
Page #: 45
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #205, 2 FT. M-136 Lab ID: 9509020-21A CoUected: 09/12/95 13:51:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
chlorobenzene-d5
1,4-dichlorobenzene-d4
428079 ug/Kg
102455 ug/Kg
Surrogate/Recovery Data
Surrogate
dibromofluorometheme
1,2 -di chloroetheme-d4
toluene-d8
bromofluorobenz ene
SW-846,8260A
09/26/95 MMR INTSTD2
09/26/95 MMR INTSTD3
For Volatila
%Racovary
78.5
77.6
122
115
Organics 8260S
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Sample ID: GD #205, 5 FT. M-136 Lab ID: 9509020-22A CoUected: 09/12/95 14:00:00
TEST
HMZ
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Laad
Silver
Marcury
Volatila Organics
benzene
bromobenzene
bromochlorometheme
bromodi chloromethane
bromoform
bromomethane
n-butylbenz ene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chlorofonn
RESULT
U
u
09/15/95
0.26
21.1
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
tJNITS
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.500
0.500
0.1
0.3
1.6
0.2
0.014
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/19/95
09/19/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SOP 420
SOP 420 ^
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
^ 1
^
Page #: 46
October 18, 1995 10:02
•
Sample ID: GD #205, 5 FT. M-136
CERTIFICATE OF ANALYSIS
RESUI.TS BY SAMPLE
Lab D): 9509020-22A CoUected: 09/12/95 14:00:00
TEST RESULT UNITS DETECTION ANfJJiYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3-chloropropan
1,2-dibromoetheme
dibromomethane
dichlorodifluoromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1, 2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropeme
2,2-dichloropropeme
1,1-dichloropropene
cis-1,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
^^-dichlorobenzene
^^w^lbenzene
iHcachlorobutadiene
isopropylbenzene
4-isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2, 3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroethane
trichloroethene
trichlorofluorometheme
1,2,3 -tri chloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m, p-xylene
acetone
2 -butanone
4-methyl-2-pentanone
2-hexanone
fluorobenz ene
chlorobenzene-dS
u
u
u u u u
u u u u
u
u u
u
u u
u u
u u u u
u u
u u
u
u u u u u o u
u u 12 B
u u u u u u u u u u u u
u 848782
411254
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3-
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
Page tt: 47
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #205, 5 FT. M-136 Lab ID: 9509020-22A CoUected: 09/12/95 14:00:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatila Organics
1,4 -dichlorobenzene-d4 100058 ug/Kg
Surrogat e/Recove ry
Surrogate
dibromofluoromethane
1,2-dichloroetheme-d4
toluene-d8
bromofluorobenzene
SW-846,8260A
09/26/95 MMR INTSTD3
Data For Volatila
%Recovery
81.0
82.2
125
120
Organics 8260S
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Sample ID: GD #176, 2 FT. M-136 Lab ID: 9509020-23A CoUected: 09/12/95 14:26:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMZ
Nltroglycerlne
Acid Digestion
Cadmium
Chromium
Laad
Silvar
Mercury
Volatila Organics
benzene
bromobenzene
bromochlorometheme
bromodichlorometheme
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
u
u
09/15/95
0.41
23.2
U
U
D
U
' U
U
U
U
U
U
D
U
U
U
U
U
U
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.500
0.500
0.1
0.3
1.5
0.2
0.016
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/19/95
09/19/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
Page tt: 48
October 18, 1995 10:02
f
nple ample ID: GD #176, 2 FT. M-136
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9509020-23A CoUected: 09/12/95 14:26:00
EST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
olatile Organics
-chlorotoluene
-chlorotoluene
ibromochlorometheme
,2 -dibromo- 3 -chloropropem
,2-dibromoetheme
ibromometheme
ichlorodifluorome thane
,1-dichloroethane
,2 -dichloroethane
,1-dichloroethene
LS-1,2-dichloroethene
rans-l,2-dichloroethene
,2-dichloropropeme
, 3-dichloropropeme
,2 -dichloropropane
,l-dichloropropene
is-1,3-dichloropropene
rans-1,3-dichloropropene
,2-dichlorobenzene
,3-dichlorobenzene
,4-dichlorobenzene
th^^^nzene
ex^^Borobutadiene
sopfBpy Ibenz ene
- isopropyltoluene
ethylene chloride
aphthalene
-propylbenzene
tyrene
,1,1,2-tetrachloroethane
,1,2,2-tetrachloroethane
etrachloroethene
oluene
,2,3-trichlorobenzene
,2,4-trichlorobenzene
,1,1-trichloroethane
,1,2-trichloroetheme
richloroethene
richlorofluorometheme
,2,3-trichloropropane
,2,4-trimethylbenzene
,3,5-trimethylbenzene
inyl chloride
-xylene
,p-xylene
ketone
-butanone
-methyl- 2-pentemone
-hexemone
luorobenzene
nicrobenzene-d5
,4 -di chlorobenzene-d4
u
u u u u u u u u u u u u
u u
u u
u
u u
u u
u
u u
u
u u u u u u u u u 15 B
u u u u u
u
u u
u 3.4 J
u
u u 673551
358877
107789
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/9S
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Page tt: 49
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
iample ID: GD #176, 2 FT. M-136 Lab ID: 9509020-23A CoUected: 09/12/95 14:26:00
•EST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
olatile Organics
Surrogate
dibromof1uorome theme
1,2-dichloroe thane-d4
toluene-d8
bromofluorobenzene
For Volatile
%Recovary
81.2
86.9
118
112
SW-846,8260A
Organics 8260S
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
iample ID: GD #176, 5 FT. M-136 Lab ID: 9509020-24A CoUected: 09/12/95 14:37:00
'EST
MZ
ltroglycerlne
cid Digestion
admliun
hromlum
ead
ilver
darcury
/olatile Organics
oenzene
aromobenzene
iromochlorometheme
romodichlorometheme
romoform
romometheme
-butylbenzene
ec-butylbenzene
ert-butylbenzene
arbon tetrachloride
hlorobenzene
hloroethane
hloroform
hloromethane
-chlorotoluene
-chlorotoluene
RESULT
u
u
09/15/95
0.25
20.9
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u u
UNITS
KK3/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.500
0.500
0.1
0.3
1.6
0.2
0.016
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/19/95
09/19/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SOP 420
SOP 420
SW-846, 3050 i
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
Page tt: 50
October 18, 1995 10:02 CERTIFICATE OF ANi^J^YSIS
RESUILTS BY SAMPLE
Sample ID: GD #176, 5 FT. M-136 Lab ED: 9509020-24A •- CoUected: 09/12/95 14:37:00
TEST
Volatile Organics
dibromochlorome thane
1,2-dibromo-3 -chloropropan
1,2-dibromoethane
dibromomethane
dichlorodifluorometheme
1,1-dichloroethane
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropane
2,2-dichloropropane
1,1-dichloropropene
cis-l,3-dichloropropene
trems-1, 3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
^^propylbenzene
^^isopropyltoluene
^JRhylene chloride
naphthalene
h-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
te trachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2 -butanone
4-methyl-2-pentemone
2 -hexanone
fluorobenzene
chlorobenzene- d5
1,4-dichlorobenzene - d4
RESULT
U
u u u u u u u u u u
u u
u u u
u u u u u u
u 15 B
u
u u u u u D
u u 16 B
U
U
U
U
U
u u u u 8.6 J
U
U
U
675031
328774
90779
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANiLLYZED
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/:J6/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Page #: 51
October 18, 1995 10:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #176, 5 FT. M-136 Lab ID: 9509020-24A CoUected: 09/12/95 14:37:00
'EST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
olatile Organics
Surrogate/Recovery Data For Volatile Organics 8260S
SW-846,8260A
Surrogate %Recovary
dibromofluorometheme 79.4
1,2-dichloroethane-d4 86.4
toluene-d8 126 Q
bromofluorobenzene 105
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Iample ID: GD #205, 2 FT. M-136 DUP. Lab ID: 9509020-25A CoUected: 09/12/95 13:51:00
•EST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
olatile Organics
enzene
romobenzene
romochloromethane
romodi chlorome thane
romoform
romome t heme
-butylbenzene
ec-butylbenzene
ert-butylbenzene
arbon tetrachloride
hlorobenzene
hloroethane
hloroform
-hloromethane
:-chlorotoluene
:-chlorotoluene
libromochlorometheme
.,2 -dibromo-3 -chloropropem
.,2 -dibromoetheme
Iibromomethane
ichlorodifluorometheme
,1-dichloroetheme
,2-dichloroetheme
,1-dichloroethene
is-1,2-dichloroethene
rems-1,2-dichloroethene
,2-dichloropropeme
,3-dichloropropane
,2 -dichloropropeme
,l-dichloropropene
i s-1,3 -dichloropropene
rans-l,3-dichloropropene
,2-dichlorobenzene
,3-dichlorobenzene
u u u u u u u u u u u u u u
u D
u
u
u
u
u u u u u u u u u u u u
u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
Page tt: 52
October 18, 1995 10:02 CERTIFICATE OF ANi^JLYSIS
RESUILTS BY SAMPLE
Sample ID: GD #205, 2 FT. M-136 DUP. Lab ED: 9509020-25A CoUected: 09/12/95 13:51:00
TEST
Volatila Organics
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
RESULT
u u u u u 3.4 BJ
U
U
U
1,1,1,2-tetrachloroethane U
1,1,2,2-tetrachloroethane U
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
Jm&,5 -trimethylbenzene
^1^1 chloride
^^^lene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentemone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4 -dichlorobenzene-d4
U
U
U
U
16 B
U
U
U
U
U
U
U
U
U
U
U
U
U
373524
212937
82188
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Dai:
Surrogate
dibromofluoromethane
1, 2 -di chloroethane-d4
toluene-d8 .
bromofluorobenzene
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANiLLYZED
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
:a For Volatile Organics 8260S
%Racovary
79.9
88.8
114
92.4
METHOD/CAS#
SW-846,8260A
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Page tt: 53
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J * Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1, IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits. If surrogate recoveries are out
of limits, any values reported are for indication only.
ENVIRONMENTAL LAB WORK REIQUEST 9^7-^
TfflOKOL ENVIRONMENTAL LABORATORY LWR No. E11042
^^- /).F /{Z^ZA^. /-
EXTENSION
4F3'^/P
COST CENTER
-MZl^l
WORK ORDER
ifff40
DATE
/y s^rff~
ORGANIZATION
dkz^
REPORT RESin.T!i TO:
HELEN WARD, MS 301
SAMPLE DEFORMATION
SAMPLE
Oi ^ 14/^
DATE
f-//'fr '^
TYPE LOCATION TIME
tsj(
TEST
\Zoc
REMARKS
t/
y
Cdit-/4<i,. Z7.fr hMl ' y ll FJI Cd, Or,Appl'J /j? ////// AJC
\yf^d^/'fO 9^Z-iF ^ /I ^94± VoC-
i-tZ'ii ,-' i/ ll IJH. Cd,Cr,A^,Pb,lZj, HAd/{,AZG
^< yGdl//4/^
1'/Z'1S y ,'94± Ci^Cr, A^., /% H^. ^AiZ. A/(Z^
L/'^
&df^/9^ ±ir9r ^ // 73SL J/OL
M
6J-4- Iff
J±CL li y d 'JIO Ci/Ctr^A^, P/», //a ,F/(X. Af^
(Zd^ili
<rr
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'^^dif- I9u
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<l y If m± Od,Ct, 4^. Z^, d^, FA(A Afo7>
Ui
'-Odtf /9(f // V n 640 \}oc
^n ^-"^^Z ,1 ./ ll iW Cd, Cr,,A<j, Ph, H^^ Hm^ A/o
RELINQUISHED BY
JajMlL.
DATE
IZ ^i-?r
CHAIN OF CUSTODfY /
TIME
I^Oc>
RECEJVED BY
Z/Z/F/JT,,...^
DATE
- ^vr-fr
TIME
/9^/J.
€ FOR LABORATORY USE ONLY
ATE COMPLETED OATE REPORTED SIGNATURE
ENVIRONMENTAL LAB WORK REQUEST
THIOKOL ENVIRONMENTAL LABORATORY
woaxoasiK
OBOAMZAITON UVOBT ROULTS TOI
HELEN WARD, MS 301
SAMFLE INFORMATION
SAMPLE OATE TVPE ux:AnoN TIME 'nsrf BmASXS
*l-(i-«fr'^
i /U-/93-S
ViA^ 7.kL*y.\<\.
/idn-sT''^^ lblc> VOL
fl y If /olo 4Q^^
•y^ia^lj
V
11 y
v\
/' /o2D As,Cc<,Cr,Ci^ ,M,,Ui,l»v
• Rc . Ti •'
/( 2M1
%
•bCs ; l^-'D\ck\oco\»u
a-Li iL£L
i«^ /< iMl As,C<Jl,Cr,CvK .>l.)U>, gn. rf|
l( y It lors' HbG 1/4^ 'QicAloro/k.iiyit,
/nft /( tr' F /OS^ A^,cd,Cr,Cu, H,/>',2n Hk.
V
yi
/( /( nzo t/OC ', 1,4' pi^A/oraAcx
II cy /I
._^
mo A^.Cd^Cr. Cu,Ph,Ui i^n, f^
"" Cd-*/-4t /of/ 11 fl H35 VOO. /f4 Dic/i/cri>/^.„
"-&
/«<-
ioft y' 11
Gd 4t^SO
_5jfFt
11^5 ^s. C4,Cr, Cu^ Ph,hF, g^ ,/U-
l( H IZTf iZoG /^4^'VfcA/6foht^i^i^
(7 /$di^S^ /< / / fZ^ 4s, Cd, Cr, Cu, Vi., A/7^ '^^r^
CHAIN OF CUSTODY
RFIiNQUISHESBY DATE TIME RECEIVED BV DATE TIME
FOR LABORATORY USE ONLY
DAIE OOMimB) DAIBUFOBnO HGNATUBS
ENVIRONMENTAL J:AB WORK REQUEST ^Fd jd F 9 a
"• THIOKOL ENVmONMFNTAL LABORATORY
l|F.OM.
OaCAMZAnON
KmNBON
MUL trap
COCT cvms
eiio^z^ P<if<3
wououss IMIS
•Bwr RBaa.li rai
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMFLE
1. Gd ^S'O
//>FF
Do^P /off'
DATE
i'lS'^r *"
TVPE
y
LOCATION
M'/9^'^
V
TIME TEST
nio
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iZOG If4' 7?/<t/iZ/yroZu/i^j^
REMARKS
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Gd^ S
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A^.Cd.Cr. Cu^Pb,h/F: r/>. l-l-^
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A.Cd. Cr. Cu. Fb,Al/,
ll y /U-I9I-A/
I4'I^'A<>, Cd, Cr, Cu, Ph, ^1,
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CHAIN OF CUSTODY
- RKI JNQUISHED BY DATE TIME RECETVIESBY DATE
'
TIME
DATE O0N<n.Em)
FOR LABORiiLTORY USE ONLY
DA18 RETOKnO aCNATUU
October 18, 1995 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward MIS 301
Thiokol Corp, Ut 84322
A.F. WALKER
EXT 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs MIS 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Orders 9509029
Lab ID:
OIA
Sample ID:
GD #146, 2 FT.
Sample and Test Code Identification
Test Codes and Names
Lab ID:
02A
Sample ID:
GD#146, 5 FT.
UbID:
03 A
Sample ID:
GD #146, 5 FT. DUPLICATE
UbID:
04A
Sample ID:
GD #199, 2 FT.
UbID:
~O5A
Sample ID:
GD #199 TFT.
UbID:
06A
Sample ID:
GD #196, 2 FT.
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG A£2
HO CV2
8260S
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NO
3050
CU AE2
CR AE2
PB AE2
AO AE2
HG CV2
8260S
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8260s
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8260s
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Or;ganica
Test Codes and Names
HMX
NG
HMX
Nitroglycerine
Page tt:l of
Method
SOP 420
sop 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
S-W-i46,S260A Method
SOP 420
SOP 420
/7
Work Orderly 9509029 Sample and T<?st Code Identification
Sample ID:
GD #196, 2 FT.
UbID: Sample ID:
07A GD #196, 5 FT.
UbID:
08A
Sample ID:
M-l93^ RINSE BLANK
UbID:
09A
Sample ID:
GD#5, 5FT.
UbID:
lOA
Sample ID:
GD #5, 10 FT.
UbID:
llA
Sample ID:
GD#41,5Fr.
UbID:
12A
Sample ID:
GD#41, IOFT.
•
Test Codes and Names
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8260s
Ai:id Digestion
Cadmium
Cliromium
L(!ad
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB"AE2
AG AE2
HG CV2
8260s
HIVDC
Nitroglycerine
Ai;id Digestion
Cadmium
Cliromium
U-id
Silver
Mercury
Volatile Organics
Test Codes and Names
3010
AS AE2
BE AE2
CD""AE2
CR AE2
CU AE2
PB AE2
NI AE2
TL AE2
ZN AE2
HG CV3
8260
Acid Digestion
Al-senic
B<:ryllium
Ciidmium
Chromium
Copper
Lead
Nickel
Tliallium
Zinc
Mercury
Volatile Organics
Test Codes and Names
3050
CD AE2
CR AE2
CU AE2
PB'AE2
NI AE2
ZN AE2
AS GF2
H0~CV2
8260S
Acid Digestion
Ciidmium
Chromium
Copper
Lead
Nickel
Zinc
Aisenic
M'srcury
Volatile Organics
Test Codes and Names
3050
CD AE2
CR AE2
CU~AE2
PB AE2
NI AE2
ZfTAEZ
AS"GF2
HO CV2
8260s
Acid Digestion
Cedmium
Chromium
Ccipper
L.id
Nickel
Zinc
Aisenic
Mercury
Volatile Organics
Test Codes and Names
3050
CD AE2
CR AE2
CU AE2
PB AE2
NI AE2
ZtT AE2
AS GF2
HG CV2
8260s
Acid Digestion
Ct dmium
Ctiromium
Copper
Lead
Nickel
Zi:iic
Aisenic
Mcsrcury
Volatile Organics
Test Codes and Names
3050
CD AE2
CR AE2
CU AE2
Acid Digestion
Cadmium
Ctiromium
Ccipper
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SW-846, 3010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7470
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
Page #:2
Work Order # 9509029 Sample and Test Code Identification
UbID:
12A
UbID:
13A
Sample ID:
GDiMl, IOFT.
Sample ID:
GD i»0, 5 FT.
Test Codes and Names
UbID:
14A
Sample ID:
GD #50, 10 FT.
Lab ID:
ISA
UbID:
16A
Sample ID:
OD gX, 10 FT. DUPLICATE
Sample ID:
GD#71,5 FT.
Ub ID:
17A
le ID:
GD#71, IOFT.
UbID:
18A
Sample ID:
GD #8, 5 FT.
UbID:
19A
Sample ID:
OD #8, 10 FT.
PB AE2
NI AE2
ZN AE2
AS GF2
HG CV2
8260s
Lead
Nickel
Zinc
Arsenic
Mercury
Volatile Oiganics
Test Codes and Names
3050
CD AE2
CR AE2
CU AE2
PB AE2
NI AE2
ZN AE2
AS GF2
HG CV2
8260s
Acid Digestion
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Mercury
Volatile Organics
Test Codes and Names
3050
CD_AE2
CR_AE2
CU_AE2
PB_AE2
NI_AE2
ZN_AE2
AS_GF2
HG_CV2
8260S
Acid Digestion
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Mercuiy
Volatile Organics
Test Codes and Names
8260S Volatile Organics
Test Codes and Names
3050
CD AE2
CR AE2
CU AE2
PB AE2
NI AE2
ZN AE2
AS GF2
HG CV2
8260s
Acid Digestion
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Mercury
Volatile Organics
Test Codes and Names
3050
CD AE2 CR AE2
CU AE2
PB AE2 NI AE2
ZN AE2
AS QF2
HG CV2
8260S
Acid Digestion
Cadmium Chromium
Copper
Lead Nickel
Zinc
Arsenic
Mercury
Volatile Organics
Test Codes and Names
3050
CD AE2
CR AE2
CU AE2
PB AE2
NI AE2
ZN AE2
AS GF2
HG CV2
Acid Digestion
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Mercury
Test Codes and Names
3050
CD AE2
CR AE2
CU AE2
Acid Digestion
Cadmium
Chromium
Copper
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846,8260A Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846,8260A Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846,8260A
Method
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846,8260A Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471 Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
Page #:3
Worit Order # 9509029 Sample and Test Code Identification
^ Sample ID:
GD#8i IOFT. Test Codes and Names Method
PB AE2
NI AE2
ZN AE2
AS GF2
HG CV2
Lead
Nickel
Zinc
Arseni<:
Mercuiy
Comments
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
Certified By
Page #:4
This is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: GD #146, 2 FT. Lab ID: 9509029-OlA CoUected: 09/12/95 15:31:00
TEST
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochlorometheuie
bromodi ch1oromethane
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chl oroe thauie
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo- 3 -chloropropem
1,2-dibromoethane
dibromome theme
dichlorodifluoromethane
1,1-dichloroe thane
1,2-dichloroethame
1,1-dichloroethene
cis-1,2-di chloroethene
trams-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropame
1,l-dichloropropene
cis-1,3-dichloropropene
trams-l,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
RESULT
U
u
09/15/95
U
20.4
U
U
0.01
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u u u u
u u u u u
u
u u u u u u
DNITS
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.500
0.500
0.1
0.3
1.6
0.2
0.013
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/21/95
09/21/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
10/10/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5 ^^
75-27-4 ^B
75-25-2 ^P
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1 ^^
Page tt: 5
October 18, 1995 10:44
Sample ID: GD #146, 2 FT.
CERTIFICATE OF A^[AJLYSIS
RESU1.TS BY SAMPLE
Lab ID: 9509029-OlA CoUected: 09/12/95 15:31:00
TEST
Volatile Organics
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2- trichloroe thaine
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
jn^, 5 - trimethylbenzene
flA^l chloride
amylene
m, p-xylene
acetone
2-butamone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESDLT
U
u u u u 16 B
U
U
U
U
U
U
U
u
u 11 B
U
U
U
U
U
U
u u u 7.8 J
U
U
U
589813
293529
82946
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Dal:
Surrogate
dibromofluoromethane
1,2-dichloroethame-d4
toluene-d8
bromofluorobenzene
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
AN^kLYZED
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/:26/95
09/26/95
09/26/95
09/26/95
09/:26/95
09/26/95
09/26/95
09/26/95
09/;26/95
09/;J6/95
09/:J6/95
09/:>6/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
:a For Voiatilo Orgamics 8260S
%Recovery
75.7
80.6
124
111
METHOD/CAS#
SW-846,8260A
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #146, 5 FT. Lab H): 9509029-02A CoUected: 09/12/95 15:44:00
TEST RESDLT DNITS DETECTION A1S7ALYZED BY
LIHIT
METHOD/CAS#
HMX U MG/KG 0.500 09/:21/95 KMS SOP 420
Page tt: 6
October 18, 1995 10:44 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #146, 5 FT. Lab ID: 9509029-02A CoUected: 09/12/95 15:44:00
TEST
Nltroglycerlne
Acid Digestion
Cadmiiom
Chromium
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethame
bromodi chloromethame
bromoform
bromomethame
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethame
chloroform
chloromethame
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3-chloropropam
1,2-dibromoethane
dibromomethane
dichlorodifluoromethane
1,1-dichloroethame
1,2-dichloroethane
1,1 - di chl oroe thene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
RESDLT
U
09/15/95
U
22.7
U
U
U
-
U
u
u u u u u
u u u u u u u u D
D
U
U
U
U
U
u u u u u
u
u u u u u u
u u u
DNITS
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.500
0.1
0.3
1.6
0.2
0.014
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/21/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
10/10/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01
10061-02-
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
^^ 0
•5
-6
^^
Page tt: 7
October 18, 1995 10:44
Sample ID: GD #146, 5 FT.
CERTIFIC:ATE OF AN^fd^VSIS
RESULTS BY SAMPLE
Lab ID: 9509029-02A CoUected: 09/12/95 15:44:00
TEST
Volatile Organics
i sopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethame
1,1,2,2-tetrachloroethame
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropame
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
l^^p-xylene
VHetone
2-butanone
4-methyl-2-pentanone
2 -hexanone
fluorobenzene
chlorobenzene-d5
1,4 -di chlorobenzene-d4
RESDLT
U
U
13 B
U
U
U
U
U
U
U
0
U
13 B
U
U
U
U
U
U
U
U
U
U
U
U
U
808192
368123
88808
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluoromethane
1,2-• dichloroethane-d4
toluene-d8
bron lofluorobenze ne
%Recovery
76.6
77.5
122
113
METHOD/CAS#
SW-846,8260A
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Iilmlts
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #146, 5 FT. DUPLICATE Lab ID: 9509029-03A CoUected: 09/12/95 15:44:00
TEST RESDLT DNITS DETECTION JVNALYZED BY
LIMIT
METHOD/CAS#
HMX
Nltroglycerlne
U MG/KG 0.500 09/21/95 KMS
U MG/KG 0.500 09/21/95 KMS
SOP 420
SOP 420
Page tt: 8
October 18, 1995 10:44 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #146, 5 FT. DUPLICATE Lab ID: 9509029-03A CoUected: 09/12/95 15:44:00
TEST RESULT ITNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
09/15/95
0.24
20.8
U
U
0.02
DATE.
ug/g
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.6
0.2
0.013
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
10/10/95
KWB
LVD
LVD
LVD
LVD
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
7471
Sample ID: GD #199, 2 FT. Lab ID: 9509029-04A CoUected: 09/13/95 07:30:00
TEST
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodichloromethame
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
RESULT
U
u
09/15/95
U
21.8
U
U
O
U
U
U
U
U
u u
u
u
u
u
u
u
UNITS
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0
0
0
.500
.500
0.1
0.3
1.5
0.2
.013
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/21/95
09/21/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
10/10/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SOP 420 ^^
SOP 420 ^^
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3 ^^
Page tt: 9
October 18, 1995 10:44
Sample ID: GD #199, 2 FT.
CERTIFIC:ATE OF AT^^^^ILYSIS
RESUILTS BY SAMPLE
Lab ID: 9509029-04A CoUected: 09/13/95 07:30:00
TEST
Volatile Organics
chloromethame
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethame
1,2-dibromo-3 -chloropropan
1,2-dibromoetheme
dibromomethane
dichlorodifluoromethame
1,1-dichloroetheme
1,2-dichloroethame
1,1-dichloroethene
cis-1,2-dichloroethene
t rans-1,2 -di chloroethene
1,2-dichloropropane
1,3-dichloropropame
2,2-dichloropropame
1,l-dichloropropene
cis-1,3 -dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
^^ -dichlorobenzene
^^^ - di chl orobenz ene
H^^ylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethame
1,1,2,2-tetrachloroethane
tet rachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethame
1,1,2-trichloroethame
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
jg|k)robenzene - d5
RESDLT
U
u
u u u
u u u a u
u u
u
. u
u
u
u
u
u D
u
u
u
u
a
D
15 B
u u
u
u
u
u u u
u 16 B
U
U
n
u
u
u
u
u
u 4.8 J
u
u
u 780307
334199
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
IJO
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
;U(TJ^YZED
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/:26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/;26/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
Page tt: 10
October 18, 1995 10:44 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #199, 2 FT. Lab ID: 9509029-04A CoUected: 09/13/95 07:30:00
TEST RESDLT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
1,4 -di chlorobenzene-d4 73954 ug/Kg 09/26/95 MMR
SW-846,8260A
INTSTD3
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate %Recovery
dibromofluoromethane 76.4
l,2-dichloroethane-d4 80.6
toluene-d8 125
bromofluorobenzene 122
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Sample ID: GD #199, 5 FT. Lab ID: 9509029-05A CoUected: 09/13/95 07:40:00
TEST RESDLT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMX
Nl troglycerlne
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chloromethame
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethame
chloroform
chloromethane
u
u
09/15/95
U
24.8
U
U
U
U
U
U
U
U
U
U
U
U
U
O
U
U
U
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.500
0.500
0.1
0.3
1.6
0.2
0.014
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/21/95
09/21/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
10/10/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
Page#: 11
October 18, 1995 10:44
Sample ID: GD #199, 5 FT.
CERTIFICATE OF ANi^J^YSIS
RESULTS BY SAMPLE
Lab EC): 9509029-05A CoUected: 09/13/95 07:40:00
TEST RESDLT DNITS DETECTION ANJLLYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
2-chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3 -chloropropam
1,2-dibromoethane
dibromomethane
dichlorodifluoromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropame
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis'l,3-dichloropropene
trams-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4'dichlorobenzene
•
ylbenzene
pichlorobutadiene
propylbenzene
4 - isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethame
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butamone
4-methyl-2-pentanone
2-hexemone
fluorobenzene
chlorobenzene-d5
1 „^- di chlorobenzene-d4 1 -A.-d
u
u u u u u u u
u u u u u u u u u u u u u u u u
u 14 B
u
u u
u
u
u
u u u 13 B
U
u
u u u u u u u 3.9 J
u
u
u 699793
353085
106822
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/ Kg
ug/ Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/:26/95
0£>/;26/95
09/:>-6/95
09/26/95
09/26/95
09/:26/95
09/:J6/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/:!6/95
09/26/95
09/:>.6/95
09/26/95
09/26/95
09/26/95
09/26/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Page tf: 12
October 18, 1995 10:44 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #199, 5 FT. Lab ID: 9509029-05A CoUected: 09/13/95 07:40:00
TEST RESDLT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Surrogate
dibromofluoromethane
1,2-dichloroethame-d4
toluene-d8
bromofluorobenzene
For Volatile
%Recovery
76.3
82.7
123
102-
SW-846,8260A
Organics 8260S
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Sample ID: GD #196, 2 FT. Lab ID: 9509029-06A CoUected: 09/13/95 08:34:00
TEST
HHX
Nltroglycerlne
Acid Digestion
Cadmium
Chromiiun
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethame
bromodi chloromethame
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chlorome thame
2 -chlorotoluene
4 -chlorotoluene
RESULT
u
u
09/15/95
0.17
22.3
U
U
U
U
U
U
* U
U
U
u
u
u
u
u
u
u
u
u
u
UNITS
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.500
0.500
0.1
0.3
1.6
0.2
0.013
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/21/95
09/21/95
09/15/95
09/19/95
09/19/95
09/19/95
09/19/95
10/10/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SOP 420
SOP 420
SW-846, 3050 ^^
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4 ^_^
Page tt: 13
October 18, 1995 10:44
Sample ID: GD #196, 2 FT.
CERTI] i'lc ATE OF A^fi^kLYSIS
RISUILTS BY SAMPLE
Lab ED: 9509029-06A CoUected: 09/13/95 08:34:00
TEST
Volatile Organics
dibromochloromethane
1,2-dibromo-3 -chloropropam
1,2-dibromoetheme
dibromomethane
dichlorodifluoromethame
1,1-di chloroethane
1,2-dichloroethame
1,1-dichloroethene
cis-1,2-di chloroe thene
trans -1,2-dichloroethene
1,2-dichloropropane
1,3- dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis-1,3 -dichloropropene
trams-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
jMujropylbenzene
^^Bopropyltoluene
^Khylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m, p-xylene
acetone
2-butanone
4 -methyl - 2 -pentamone
2-hexamone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
U
u u u u u u u u u u
u u
u u u
u u u u
u u
u 19 B
u u u u u u u u u 7.8 BJ
u u u u
u u u u u
u u
u
u 430748
256028
87598
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug.'Kg
ug.'Kg
ug/Kg
ug/Kg
ug,'Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug, Kg
ug, Kg
ug/Kg
ug/Kg
ug, Kg
ug/Kg
ug. Kg
ug/ Kg
ug/Kg
ug/Kg
ug/ Kg
ug/ Kg
ug/ Kg
ug/ Kg
ug/Kg
ug/ Kg
ug/Kg
ug/ Kg
ug/ Kg
ug/ Kg
ug/Kg
ug/ Kg
ug/ Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANJU^YZED
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/:26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/:>6/95
09/26/95
09/26/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Page tt: 14
October 18, 1995 10:44 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #196, 2 FT. Lab ID: 9509029-06A CoUected: 09/13/95 08:34:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics SW-846,8260A
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate %Recovary
dibromofluoromethame 81.0
1,2-dichloroethane-d4 87.9
toluene-d8 113
bromofluorobenzene 99.9
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Sample ID: GD #196, 5 FT. Lab ID: 9509029-07A CoUected: 09/13/95 08:40:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HHX
Nltroglycerlne
Acid Digestion
Cadmium
Chromium
Laad
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethame
bromodichloromethame
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethame
chloroform
chloromethane
2 -chlorotoluene
4-chlorotoluene
u
u
09/20/95
0.17
16.6
2.10
U
0.01
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.500
0.500
0.1
0.3
1.7
0.2
0.013
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/21/95
09/21/95
09/20/95
09/21/95
09/21/95
09/21/95
09/21/95
10/10/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
Page tt: 15
October 18, 1995 10:44
Sample ID: GD #196, 5 FT.
CERTIHCATE OF A^fAJL YSIS
RISUL,TS BY SAMPLE
LibDI): 9509029-07A CoUected: 09/13/95 08:40:00
TEST
Volatile Organics
dibromochlorometheme
1,2-dibromo-3 -chloropropan
1,2-dibromoetheme
dibromometheme
di chlorodi fluoromethame
1,1-dichloroethame
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trams-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropeme
1,l-dichloropropene
cis-1,3-dichloropropene
trems-1,3 -dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
^^propylbenzene
1^^opropyl toluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethame
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,l-trichloroethane.
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentemone
2-hexamone
fluorobenzene
chlorobenzene- d5
1,4-dichlorobenzene-d4
RESULT
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
15 B
u
u
u
u
u
u
u
u
u
12 B
U
u
u
u
u
u
u
u
u
u
u
u
u
728204
374272
112049
UN3TS
ug
ug.
ug.
ug.
ug.
ug.
ug.
ug
ug.
ug,
ug.
ug.
ug.
ug,
ug,
ug.
ug,
ug.
ug.
ug.
ug.
ug.
ug,
ug,
ug,
ug.
ug.
ug.
ug.
ug.
ug.
ug.
ug.
ug.
ug.
ug.
ug.
ug,
ug,
ug,
ug,
ug,
ug.
ug.
ug
ug,
ug.
ug
ug
ug.
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
AN;ILYZED
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Page tt: 16
October 18, 1995 10:44 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #196, 5 FT. Lab ID: 9509029-07A CoUected: 09/13/95 08:40:00
TEST RESULT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Surrogate
dibromofluorometheme
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
For Volatile
%Recovery
76.8
83.9
119
108
SW-846,8260A
Organics 8260S
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Sample ID: M-193-S RINSE BLANK Lab ID: 9509029-08A CoUected: 09/13/95 10:30:00
TEST
Acid Digestion
Arsenic
Beryllium
Cadmium
Chromium
Copper
Lead
Nickel
Thallium
Zinc
Mercury
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodichlorometheme
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
RESDLT
09/22/95
U
U
U
U
10.8
U
U
U
113
U
U
U
U
U
U
u
u
u
u
u
DNITS
DATE
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
0
0
0
0
0
0
0
0
0
0
0
50
2
2
5
2
25
10
50
4
.15
.20
.20
.20
.30
.10
.40
.20
.20
.20
.30
ANALYZED
09/22/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/25/95
09/27/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
BY
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3010
6010
6010 ^^
6010
6010
6010
6010
6010
6010
6010
7470
SW-846,8260A
71-43-2
108-86-1
74-97-5-
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5 ^^
Page tt: 17
October 18, 1995 10:44 CERTIFICATE OF AN^iLYSIS
RISULTS BY SAMPLE
Sample ID: M-193-S RINSE BLANK Lab ID: 9509029-08A CoUected: 09/13/95 10:30:00
TEST
Volatile Organics
chlorobenzene
chloroethane
chloroform
chloromethame
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3-chloropropam
1,2-dibromoetheme
dibromome thane
dichlorodifluoromethame
1,1-dichloroethame
1,2-dichloroethane
1,1-dichloroethene
cis-1,2 -dichloroethene
trems-1, 2-dichloroethene
1,2-dichloropropane
1,3-dichloropropeme
2,2-dichloropropame
1,l-dichloropropene
cis-1,3 -dichloropropene
j^^ns-1, 3-dichloropropene
^^^-dichlorobenzene
^^ -dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethame
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
^^|ethyl - 2 -pentemone
RESDLT
U
U
u u u
u u
u
u u
u
u u u u u u u u u u D
u u u u
u u
u u u
u u u u
u u
u
u ' D
u 1.8
u u
u u u u u
u u
u
DNJTS
uc;/L
uc;/L
uc:/L
uc;/L
uc/L
uc:/L
UC'/L
uc:/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
uc/L
UC
UC
UC
UC
UC
UC
UC
UC
UC
UC
UC
/L
/L
/L
/L
/L
/L
/L
/L
/L
/L
/L
uc/L
UC /L
DETECTION
LIMIT
0.20
0.40
0.40
0.60
0.20
0.20
0.30
0.20
0.20
0.20
0.20
0.10
0.20
0.60
0.20
0.20
0.20
0.20
0.20
0.20
0.20
0.20
0.10
0.20
0.20
0.30
0.20
0.20
0.20
0.30
0.20
0.20
0.20
0.20
0.30
0.90
0.30
0.20
0.20
0.20
0.20
0.30
0.30
0.20
0.20
0.20
0.40
0.20
0.20
10
10
10
ANJUiYZED
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8260A
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
Page#: 18
October 18, 1995 10:44 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-193-S RINSE BLANK Lab ID: 9509029-08A CoUected: 09/13/95 10:30:00
TEST
Volatile Orgainlcs
2-hexamone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene•
RESDLT
u 1124446
717759
•d4 278103
DNITS
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
10
ANALYZED BY
09/19/95 JMA
09/19/95 JMA
09/19/95 JMA
09/19/95 JMA
Surrogate/Recovery Data For Volatile Organics 8260
Surrogate
dibromof1uoromethane
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
%Recovery
101
105
96.2
105
METHOD/CAS#
SW-846,8260A
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
80.0 TO 120
80.0 TO 120
80.0 TO 120
80.0 TO 120
Sample ID: GD #5, 5 FT. Lab ID: 9509029-09A CoUected: 09/13/95 10:43:00
TEST
Add Digestion
Cadmium
Chromium
Copper
Lead
Nickal
Zinc
Arsenic
Mercury
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodi chlorometheme
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
RESDLT
09/20/95
U
8.41
5.25
U
7.29
32.6
5.1
U
U
U
U
U
U
U
U
a U
DNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
0.1
1.6
0.64 .
0.3
1.9
0.014
10
10
10
10
10
10
10
10
10
ANALYZED
09/20/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
10/05/95
10/10/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
KWB
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
^^
3050 ^pr
6010
6010
6010
6010
6010
6010
7060
7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6 —
Page tt: 19
October 18, 1995 10:44 CERTIFICATE OF ANM.YSIS
RES ULI S BY SAMPLE
M e ID: GD #5, 5 FT. Lab ID: 9509029-09A CoUected: 09/13/95 10:43:00
TEST
Volatile Organics
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3-chloropropem
1,2-dibromoetheme
iibromome theme
ii chlorodifluoromethame
1,1-dichloroethame
.,2-dichloroethane
.,1-dichloroethene
:is-1,2 -dichloroethene
:rems-1,2-dichloroethene
., 2-dichloropropane
,3-dichloropropame
,2-dichloropropeme
,l-dichloropropene
is-1,3-dichloropropene
rans-l,3 -di chloropropene
, 2 ^^khlorobenzene
, 3 VHilorobenzene
,4-dichlorobenzene
thyIbenzene
axachlorobutadiene
sopropylbenzene
-isopropyltoluene
3thylene chloride
iphthalene
- propyIbenzene
•.yrene
1,1,2-tetrachloroethane
1,2,2-tetrachloroethane
1 trachloroethene
iluene
2,3-trichlorobenzene
2,4-trichlorobenzene
1,1-trichloroethane
1,2 -trichloroethane
ichloroethene
ichlorofluoromethane
2,3-trichloropropeme
2,4-trimethylbenzene
5,5-trimethylbenzene
lyl chloride
cyl ene
(-xylene
itone
lutanone
RESDLT
u
u u u u u u u u u u a u u u u u u
u
u
u u D
u a u D
u u
u 7.3 BJ
U
U
D
V
U
U
U
U
D
8.7 BJ
D
U
U
U
U
U
U
U
U
3.8 J
U
DNITi;
ug/Kc,
ug/Kc
ug/Kc
ug/Kc
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
- ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/&5
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/915
09/26/913
09/26/95
09/26/9!>
09/26/95
09/26/95
09/26/9Ei
09/26/95
09/26/95.
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,82G0A
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
Rge#:20
October 18, 1995 10:44 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #5, 5 FT. Lab ID: 9509029-09A CoUected: 09/13/95 10:43:00
TEST
Volatile Organics
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-dS
1,4-dichlorobenzene-
RESULT
U
u 834981
439889
d4 144246
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
ANALYZED BY
09/26/95 MMR
09/26/95 MMR
09/26/95 MMR
09/26/95 MMR
09/26/95 MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluoromethame
1,2-dichloroethame-d4
toluene-d8
bromofluorobenzene
%Recovery
84.1
88.8
115
101
METHOD/CAS#
SW-846,8260A
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Sample ID: GD #5, 10 FT. Lab ID: 9509029-lOA CoUected: 09/13/95 10:55:00
TEST
Acid Digestion
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chloromethane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
RESDLT
09/20/95
0.15
9.77
6.49
U
7.53
29.4
5.8
U
U
u
u
u u
u
u
u
DNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
0.1
1.5
0.59
0.2
1.8
0.011
10
10
10
10
10
10
10
10
ANALYZED
09/20/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
10/05/95
10/10/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
KWB
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
%
3050
6010
6010
6010
6010
6010
6010
7060
7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8 ^
Page tt: 21
October 18, 1995 10:44 CERTIJFIC:ATE OF AP^T/O^YSIS
RiSULTS BY SAMPID
Sample ID: GD #5, 10 FT. lab ID: 9509029-lOA CoUected: 09/13/95 10:55:00
TEST
Volatile Organics
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3 -chloropropam
1,2-dibromoethane
dibromome theme
dichlorodifluorometheme
1,1-dichloroetheme
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2 -dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropame
2j2-dichloropropane
I^H - di chloropropene
'^PP-1,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 - iscjpropyltoluene
methylene chloride
naphthalene
n-propylbenzene
Styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethame
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluorcjme thane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
^Ktone
RESDLT
U
a u u u u u u u u u u u u u u u u u
u
u u
u
u u u u u
u u
u 5.8 BJ
u D
u u u u
u u u 8.7 BJ
U
U
u u
u u u u u 4 J
DN:CTS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
DETECTION
LIMIT
10
10
10
10
10
10
1,0
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
J^.i^YZED
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4.
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
Page tt: 22
October 18, 1995 10:44 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #5, 10 FT. Lab ID: 9509029-lOA CoUected: 09/13/95 10:55:00
TEST RESITLT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
2-butemone
4-methyl-2-pentamone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
a
u u 1015430
473667
134699
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg .
Surrogate/Recovery Data
Surrogate
dibromofluoromethame
1,2 -di chloroetheme-d4
toluene-d8
bromofluorobenzene
10
10
10
09/26/95 MMR
09/26/95 MMR
09/26/95 MMR
09/26/95 MMR
09/26/95 MMR
09/26/95 MMR
For Volatile Organics 8260S
%Recovery
78.9
82.1
125
108
SW-846,8260A
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Sample ID: GD #41, 5 FT Lab ID: 9509029-11A CoUected: 09/13/95 11:20:00
TEST
Acid Digestion
Cadmium
Chrcjmlum
Copper
Lead
Nickal
Zinc
Arsenic
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethame
bromodichloromethane
bromoform
bromometheme
n-butylbenzene
RESXTLT
09/20/95
U
10.6
6.27
U
8.60
31.4
6.4
a
U
U
U
U
U
U
U
DNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
0.1
1.6
0.65
0.3
1.9
0.012
10
10
10
10
10
10
10
ANALYZED
09/20/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
10/05/95
10/10/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
KWB
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS# ^k
SW-846,
. SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
^
3050
6010
6010
6010
6010
6010
6010
7060
7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8 ^^
Page tt: 23
October 18, 1995 10:44 CERTIFICATE OF AN.1LYSIS
R ESlfLTS BY SAMPLE
Sample ID: GD#4l,5FT. ]jihID: 9509029-llA CoUected: 09/13/95 11:20:00
TEST RESDLT DNITS DETECTION JM^ALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chl orome thane
2 - ciiiorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3 -chloropropam
1,2-dibromoetheme
dibromomethane
di chlorodifluoromethane
1,1-dichloroethane
1.2 -dichloroetheme
1,1-dichloroethene
cis-1,2-dichloroethene
trems-l,2-dichloroethene
1,2-dichloropropane
^3 - dichloropropane
-dichloropropame
•dichloropropene
cis-1,3-dichloropropene
transrl,3-dichloropropene
1,2-dichlorobenzene
1.3 -di chlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
i sopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethame
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
xylene
u
u
u u u u u u u u
u u
u u u u u u
u u u u u u u u
u 0
u
u u
u 25 B
u
u ••••
u o u u u u u 13 B
u u
u o
u u u u u
ucr/Kg
uc/Kg
uc;/Kg
uc/Kg
uc/Kg
UC /Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
UC /Kg
UC /Kg
UC /Kg
UC /Kg
uc/Kg
uc/Kg
UC /Kg
uo/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug /Kg
ug'Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 .
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
Page tt: 24
October 18, 1995 10:44 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #41, 5 FT. Lab ID: 9509029-11A CoUected: 09/13/95 11:20:00
TEST RESDLT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
acetone
2-butanone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4 -di chlorobenzene-d4
8.2 J
U
U
U
602805
304687
100119
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
dibromof1uoromethane
1,2 -di chloroethane-d4
toluene-d8
bromofluorobenzt 3ne
10
10
10
10
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
For Volatile Organic
%Recovery
79.7
84.7
119
98.7
MMR
MMR
MMR
MMR
MMR
MMR
MMR
3 8260S
SW-846,8260A
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
75
75.
75.
75.
0
0
0
0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #41, 10 FT.
TEST
Lab ID: 9509029-12A CoUected: 09/13/95 11:33:00
METHOD/CAsi^Pr RESDLT DNITS DETECTION ANALYZED BY
LIMIT
Acid Digestion
Cadmium
Chromium
Copper
Lead
Nickel •
Zinc
Arsenic
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodichloromethane
bromoform
bromometheme
09/20/95
U
11.5
8.50
U
7.91
32.0
5.0
U
U
U
U
U
U
U
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.1
0.3
0.1
1.5
0.61
0.2
1.8
0.013
10
10
10
10
10
10
09/20/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
10/05/95
10/10/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
KWB
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
3050
6010
6010
6010
6010
6010
6010
7060
7471
3260A
Page tt: 25
October 18, 1995 10:44
Sample ID: GD #41, 10 FT.
CERTIFICATE OF ANiULYSIS
RESULTS BY SAMPLE
lab ID: 9509029-12A CoUected: 09/13/95 11:33:00
TEST
Volatile Organics
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethame
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropan
1,2-dibromoetheme
dibromomethane
dichlorodifluoromethame
1,1-dichloroetheme
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2 -dichloroethene
trems-1,2-dichloroethene
L 2-dichloropropane
^B - di chloropropane
^^P -dichloropropane
1,l-dichloropropene
cis-1,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
^•Kylene
RESDLT
U
u
u u u
u u
u u u
u u
u u
u u u
u u u
u u u
u u
u
u u u u u
u
u 8.9 BJ
u
u u u u u u
u u 7.5 BJ
U
U
U
U
u
u
u
u
DNITS
UC /Kg
uc/Kg
UC /Kg
uc/Kg
uc/Kg
UC /Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
UC /Kg
uc/Kg
uc/Kg
uc /Kg
uc/Kg
uc /Kg
uc/Kg
uc /Kg
uc /Kg
uc/Kg
uc /Kg
uc/Kg
uc /Kg
uc/Kg
uc /Kg
uc /Kg
uc /Kg
uc/Kg
uc/Kg
uc/Kg
uc /Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
lb 10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
J^NALYZED
09/26/95
.09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/'26/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
Page tt: 26
October 18, 1995 10:44 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #41, 10 FT. LabID: 9509029-12A CoUected: 09/13/95 11:33:00
TEST RESDLT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
m,p-xylene
acetone
2 -butanone
4 -methyl-2-pentemone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
u
u
u u
u
748068
355038
95995
Surrogate/Re
Surrogate
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
covery Data
dibromofluoromethame
1,2 -di chloroethame-d4
toluene-d8
bromofluorobenz ene
10
10
10
10
10
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
For Volatile Organics 8260S
%Recovery
80.0
77.1
124
107
SW-846,8260A
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
75.
75.
75.
75.
0
0
0
0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #50, 5 FT. LabID: 9509029-13A CoUected: 09/13/95 12:59:00
TEST
Acid Digestion
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chloromethane
bromoform
RESDLT
09/20/95
0.16
9.18
3.90
5.08
7.97
39.1
7.2
U
U
U
U
U
U
DNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
0.1
1.6
0.62
0.2
1.9
0.011
10
10
10
10
10
ANALYZED
09/20/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
10/05/95
10/10/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
KWB
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
MMR
MMR
MMR
MMR
MMR
METHOD/CAS# ^^
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,.
SW-846,
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
3050
6010
6010
6010
6010
6010
6010
7060
7471
3260A
Page tt: 27
October 18, 1995 10:44
y
Sample ID: GD #50, 5 FT.
CERTIFICATE: OF AI^^yLYSIS
R ESULTS BY SAMPLE
Jab ID: 9509029-13A CoUected: 09/13/95 12:59:00
TEST
Volatile Organics
bromometheme
n-butylbenz ene
sec-butyIbenz ene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3-chloropropan
1,2-dibromoetheme
dibromomethane
di chlorodi fluorometheme
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
^^^ - di chloropropane
^^P-dichloropropane
2,2-dichloropropeme
1,1-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropame
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
^•lyl chloride
RESDLT
U
u u u
u u u u u
u u u u D
u u u u u u u u
u u u u u u u u u u O
u 12 B
u u u . u
u u u u u 11 B
u u u u
u u u
DNITS
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc /Kg
uc/Kg
uc /Kg
uc /Kg
uc/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug /Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug /Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
JWALYZED
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
Page tt: 28
October 18, 1995 10:44 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #50, 5 FT. Lab ID: 9509029-13A CoUected: 09/13/95 12:59:00
TEST
Volatile Organics
o-xylene
m,p-xylene
acetone
2-butamone
4-methyl-2-pentemone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-
RESDLT
U
u 5.6 J
U
U
U
900168
421161
54 134663
Surrogate/Re
Surrogate
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
ANALYZED
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
covery Data For Volatile Organics 8260S
dibromofluorometheme
1,2-dichloroe theme-d4
toluene-d8
bromofluorobenzene
%Recovery
75.1
75.4
124
101
METHOD/CAS#
SW-846,8260A
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #50, 10 FT. LabID: 9509029-14A CoUected: 09/13/95 13:10:00 m
TEST
Acid Dlge
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Mercury
Volatile
benzene
istlon
Organics
bromobenzene
bromochloromethane
bromodichlorometheme
RESDLT
09/20/95
0.26
9.08
6.10
U
7.57
29.9
5.0
U
U
U
U
U
DNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
0.1
1.6
0.66
0.3
2.0
0.014
10
10
10
10
ANALYZED
09/20/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
10/05/95
10/10/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
KWB
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,1
71-43-2
108-86-1
74-97-5
75-27-4
3050
6010
6010
6010
6010
6010
6010
7060
7471
3260A
^^
Page tt: 29
October 18, 1995 10:44 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
^1 le ID: GD #50, 10 FT. La^ID: 9509029-14A CoUected: 09/13/95 13:10:00
TEST
Volatile Organics
bromoform
bromome thane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethame
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo- 3 -chloropropem
1,2-dibromoetheme
dibromomethane
dichlorodifluorome thame
1,1- di chloroethane
1,2-dichloroethame
1,1-dichloroethene
::i s -1,2 - di chl oroethene
:rans-1,2-dichloroethene
L,2-dichloropropane
L, ^^iphl oropropane
!, ^^pbhloropropane
., l^n chl oropropene
:is-1,3 -dichloropropene
rans-1,3-dichloropropene
,2-dichlorobenzene
,3-dichlorobenzene
,4-dichlorobenzene
thylbenzene
exachlorobutadiene
sopropylbenzene
-isopropyltoluene
lethylene chloride
aphthalene
-propylbenzene
tyrene
,1,1,2-tetrachloroethane
,1,2,2-tetrachloroethane
; trachloroe thene
pluene
2,3-trichlorobenzene
2,4-trichlorobenzene
1,l-trichloroethane
1,2-trichloroetheme
•ichloroethene
ichlorofluorometheme
2,3-trichloropropeme
2,4-trimethylbenzene
3,5-trimethylbenzene
RESDLT
u u u u u u u u u u u u u u u u u u u u u u u
u
u D
u u u u
u D
u u u 17 B
u u u u u u u u u 10 B
u D
U
U
U
u
DNITS
ug/J g
ug/F.g
ug/Kg
ug/Kg
ug/Kg
ug/Kj
ug/Kj
ug/Rj
ug/K|j
ug/K:j
ug/K<r
ug/K( r
ug/Kci
ug/Kc
ug/Kc
„ ug/Kc
ug/Kc
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANMJYZRD
09/2(5/95
09/26/95
09/26/95
09/26;/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/9Ei
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
HMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8260A
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
I age #: 30
October 18, 1995 10:44 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #50, 10 FT. LabID: 9509029-14A CoUected: 09/13/95 13:10:00
TEST
Volatile Organics
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene- (
RESDLT
U
U
u 5 J
U
U
U
889823
436624
i4 123344
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
ANALYZED BY
09/26/95 MMR
09/26/95 MMR
09/26/95 MMR
09/26/95 MMR
09/26/95 MMR
09/26/95 MMR
09/26/95 MMR
09/26/95 MMR
09/26/95 MMR
09/26/95 MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorometheme
1,2 -di chloroetheme-d4
toluene-d8
bromofluorobenzene
%Recovery
82.0
84.4
1X9
108
METHOD/CAS#
SW-846,8260A
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Sample ID: GD #50, 10 FT. DUPLICATE Lab ED: 9509029-15A CoUected: 09/13/95 13:10:00
TEST
Volatile Organics
benzene
bromobenzene
bromochloromethame
bromodi chloromethame
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorometheme
2 -chlorotoluene
4 •- chlorotoluene
dibromochloromethane
1,2-dibromo-3-chloropropem
1,2-dibromoetheme
dibromometheme
di chlorodi fluorome theme
1,1-dichloroetheme
•1,2-dichloroethane
RESDLT
U
U
u D
U
U
U
U
U
U
U
u
u
u u u u u
u
u
u
u u
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2 ^^
Page tt: 31
October 18, 1995 10:44
••"•if-
Sample ID: GD #50, 10 FT. DUPLICATE
CERTI]7IC:ATE OF AN/O^YSIS
RJiSULTS BY SAMPLE
LabID: 9509029-15A CoUected: 09/13/95 13:10:00
TEST RESDLT DNITS DETECTION ANJ^YZED BY
LIMIT
METHOD/CAS#
Volatile Organics
1,1- dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropeme
2,2-dichloropropeme
1,l-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4-isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethame
Jt^ 2,2- tetrachloroethame
^B-achl oroe thene
tWuene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentemone
2-hexanone
fluorobenzene
chlorobenzene- d5
1,4 -di chlorobenzene-d4
U
U
U
u
u
u u u u u u
u u u u u 13 B
U
u D
D
U
u
u u u 7.6 BJ
U
U
U
U
U
U
u u u 3.8 J
U
D
U
816753
444220
140447
ug/Kg
ug'Kg
ug/Kg
ug/Kg
ug/Kg
ug'Kg
ug/Kg
ug/Kg
ug/Kg
ug,'Kg
ug/Kg
ug,'Kg
ug/Kg
ug, Kg
ug/Kg
ug/ Kg
ug/ Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/ Kg
ug/Kg
ug/:cg
ug/:Cg
Surrogate/Recovery Data
Surrogate
dibromofluoromethane
1,2 -dichloroethane-d4
toluene -d8
bromofluorobenzene
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/:26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
For Volatile Organics 8260S
%Recovery
81.7
85.2
115
106
SW-846,8260A
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Racovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
]?age tt: 32
October 18, 1995 10:44 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #71, 5 FT. LabID: 9509029-16A CoUected: 09/13/95 13:30:00
TEST
Acid Digestion
CacJmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chlorometheme
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethame
2 -chlorotoluene
4 - chlorotoluene
dibromochlorometheme
1,2-dibromo-3 -chloropropan
1,2-dibromoetheme
dibromome thane
di chlorodi fluorometheme
1,1-di chloroetheme
1,2 -di chloroetheme
1,1-dichloroethene
cis-1,2-dichloroethene
t rems-1,2-dichloroe thene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropeme
1,1-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
RESDLT
09/20/95
U
11.4
5.01
2.57
6.64
38.8
5.8
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
* U
U
u
u
u
u u
u
u u
u
u
u
DNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
0.1
1.5
0.62
0.2
1.8
0.012
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/20/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
10/05/95
10/10/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
KWB
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
6010
7060
7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01
10061-02
A w
-5
^^
Page tt: 33
October 18, 1995 10:44 CERTI FIC:ATE OF AP^^O^YSIS
RESULTS BY SAMPLE
Sample ID: GD#7l,5FT. lab ID: 9509029-16A CoUected: 09/13/95 13:30:00
TEST RESDLT DNCTS DETECTION J^.IILYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
•
, 3 - trichloropropane
,4 -trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexemone
fluorobenzene
chlorc>benzene-d5
1,4 -di chlorobenzene-d4
u
u
u
u u
u u 15 B
U
U
U
U
U
U
u u u 11 B
U
U
u u u
u u u
u
u
u u u 799696
422497
145613
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug'Kg
ug'Kg
ug'Kg
ug/Kg
ug.'Kg
ug.'Kg
Surrogate
dibromofluoromethane
1, 2-di chloroetheme-d'l
toluene-d8
bromofluorobenzene
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
For Volatile Organics 8260S
%Re covery
81.2
79.1
116
99.0
SW-846,8260A
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Page tt: 34
October 18, 1995 10:44 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #71,10 FT. LabID: 9509029-17A CoUected: 09/13/95 13:40:00
TEST
Acid Digestion
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodichloromethane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3 -chloropropan
1,2-dibromoethane
dibromometheme
di chlorodifluorometheme
1,1-dichloroetheme
1,2-dichloroetheme
1,1-dichloroethene
cis-l,2-dicdilproethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis-1,3-dichloropropene
trans-1,3 -dichloropropene
RESDLT
09/20/95
0.17
11.7
7.77
U
9.37
37.2
6.0
U
U
U
U
u u
u u
u u u u u u u u u u u
u u u u u u D
u
u u
u
u u u
DNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
0.1
1.6
0.65
0.3
2.0
0.013
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/20/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
10/05/95
10/10/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
BY
KWB
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
6010
7060
7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01
10061-02
^•^ 9
-5
-6
Page if: 35
October 18, 1995 10:44 CERTIFICATE OF AN;«iLYSIS
R] SUILTS BY SAMPLE
Sample ID: GD #71, 10 FT. LabID: 9509029-17A CoUected: 09/13/95 13:40:00
TEST
Volatile Organics
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4-isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroethane
trichloroethene
^xichlorofluoromethame
^^k,3 -trichloropropame
^^f,4 -trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4 -me thyl-2 -pentanone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESDLT
32
10
6.8
U
U
U
U
U
U
U
B
U
U
u u u
u
u
u u B
u u u u
u u u u u J
u u u 575899
351583
128424
Surrogate
Surrogate
DN}:TS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug /Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANJLLYZED
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
09/26/95
/Recovers Data For Volatile Organic
dibromofluoromethane
1,2-dichloroetheme-dl
toluene-d8
bron lofluorob enze ne
%Recovery
83.7
89.9
112
95.2
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
s 8260S
METHOD/CAS#
SW-846,8260A
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Page #: 36
October 18, 1995 10:44 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #8, 5 FT. LabID: 9509029-18A CoUected: 09/13/95 14:15:00
TEST RESDLT DNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Acid Digestion
CacSffllum
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Mercury
09/20/95
0.17
11.7
7.27
U
8.63
35.0
6.3
U
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
0.1
0.3
0.1
1.6
0.65
0.3
2.0
0.012
09/20/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
10/05/95
10/10/95
KWB
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
6010
7060
7471
Sample ID: GD #8, 10 FT. LabID: 9509029-19A CoUected: 09/13/95 14:28:00
TEST RESDLT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
Chrcsmlum
Copper
Lead
Nickel
Zinc
Arsenic
Mercury
09/20/95
U
9.01
7.39
U
8.37
33.1
5.8
U
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
0.1
0.3
0.1
1.5
0.59
0.2
1.8
0.012
09/20/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
10/05/95
10/10/95
KWB
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,'
3050
6010
6010
6010
6010
6010
6010
7060
7471
Page tt: 37
Data Re]3orting Qualifiers
U Compound was analyzed for bui not detected. Indicates conipound was below detection limit.
J Indicates an estimated value. Tliis flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the idei tification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1.1J with a detection limit of 5.0)
B This flag is used when an analyt'5 is found in the blani: as weU as the sample.
E Estimated value. Result was oui side of the caUbration rainge but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not test(^ for.
Q Surrogate/spike recovery was ou :side of the specified limiits.
ENVIRONMENTAI, LAB WORK REQUEST 'f^J
THIOKOL ENVIRONMENTAL LABORATORY LWR No. E11044
hF K//ft.K6g EX TENSION
<: il^ldL
COST cam-ER WORK ORDER
{yj340 I m4Z) \/4-<ki.f'Z^
ORGANIZATION
RrfU/iX^ouXA€K]rA-t^ 301 (T
REPORT RESULTS TO:
tIELEN WARD, MS 301
^
..•
.-^
-.^
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SAMPLE
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SAMJ'LE IINFORMATION
LOCATION
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TEST REMARKS
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//
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If
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CHA [N OF CUSTODY
RELINQUISHED BY
^^FFJ/sli '/^-'^'—^
DATE 1IME
li^/^S^ l^'l-^ .^--f^^
RECEIVED BY DATE
//5^t^"
TIME
/^H^~
.r^(7%^F^ y/>A> mm. ,^- f-xr-^r F^ZF
FOR LAlJORy^TORY USE ONLY
«
DATE COMPLETED DATE REPORTED SIGNATURE
ENVIRONMENTAL LAB WORK REQUEST
THIOKOL ENVIRONMENTAL LABORATORY
Ai^ uJall/^
OaCAMZATION
BXIBOiaN
•BOBTamiLnTOi
HELENWARD, MS301
SAMPLE INFORMATION
SAMPLE
SAt-
//iff-
/nft-
i.
i.
1.
u
9.
LOL
11.
IL
DATE
f44-fs:
II
fl
ll
TYPE
G
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TIME
I41S-
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(Fl3
TEST
\ 3c, C^' TF F^
II
/(
/'
SEMABKS
A
CHAIN OF CUSTODY
REUNQXJISHES BY DATE TIME RECQVESBY DATE TIME
POR LABORATORY USE ONLY
DAnOOMFLEIB) oimupoRnD nCNATUMK
October 19, 1995 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmeraal Monitoring
TO: Helen Ward M/S 301
Thiokol Corp, Ut 84322
A.F. WALKER
EXT 5390
i^ALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Oty, Ut 84302-0707
/Inalytical Labs M/S 245
/Ittn: Dr. Jotm Terry
Tele: 801-863-2384
Work Order # 9509033 Sample at id Test Code Identif icaition
UbID:
OIA
LabID:
02A
1 )
LabID:
03A
LabID:
04A
LabID:
05A
LabID:
. 06A
)
Sample ID:
GD#28, 5FT. M-193-N
Sample ID:
GD #28, 10 FT. M-193-N
Sample ID:
GD#86, SFT. M-193-N
Sample ID:
GD *86, 10 FT. .M-193-N
Sample ID:
GD #105, SFT. M-193-N
Sample ID:
GD #105, 10 FT. M-193-N
Test Codes and Names
3050
CD AJ2
CR A12
cu A12
PB AI2
NI AE>
ZN A12
AS GF2
HG_C^'2
/vcid Digestion
C^admium
Chromium
C;opper
I.ead
rtickel
7.\nc
/arsenic
Mercury
Test Codes and Names
3050
CD A) 2
CR A12
CU A12
PB AI2
NI AEJ
ZN A12
AS GF2
HG_C^7
hc\A Digestion
C;aditiium
C:h romium
C;opper
I.ead
Nickel
2:inc
j'trsenic
^'Iercuty
Test Codes and Names
3050
CD A12
CR AI2
CU A12
PB AE2
NI AEI
ZN A12
AS Gf 2
HO_CV2
/icid Digestion
Cadmium
C:hromium
Chopper
I.ead
Nickel
2:inc
/irsenic
>4ercury
Test Codes and Names
3050
CD A12
CR A12
CU A12
PB"AI2
NrAEl
ZN A12
AS GF2
HG_C^7
hcM Digestion
Cadmium
Crh romium
cropper
I^d
Nickel
T.ina
/irsenic
Mercury
Test Codes and Names
3050
CD A12
CR AI2
CU A12
PB AE2
NI AEI
ZN A12
AS GF2
HG_CV2
/icid Digestion
C:admium
C:hromium
Chopper
l.ead
Nickel
2:inc
/irsenic
Mercuiy
Test Codes and Names
3050 /icid Digestion
Page #: lof {0
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
Method
SW-846, 3050
Work Orders 9509033
Lab ID: Samnle ID:
06A GD #105, 10 FT. M-193-N
Sample and Test Code Identification
LabID: Sample ID:
07A GD «26, 5 FT. M-191
LabID: Sample ID:
08A GD nt, 10 FT. M-191
LabID: Sample ID:
09A GD #43, 5 FT. M-191
LabID:
IDA
LabID:
UA
Sample ID:
OD #43, IOFT. M-191
Sample ID:
GD #43, 10 FT. DUPLICATE
LabID: Sample TD:
12A RINSE BL/VNK, M-191
LabID: Sample ID:
13A GD#68, 5FT. M-191
LabID: Sample ID:
14A GD #68, 10 FT. M-191
LabID: Sample ID:
"TSA GD #82, 5 FT. M-191
Test Codes and Names
CD_AE2 Cadmium
CR /^E2 Chromium
CU AE2 Copper
PB AE2 Lead
NI AE2 Nickel
ZN" AE2 Zinc
AS GF^ Arsenic
HG_CV2 Mercury
Test Codes and Names
3050 Acid Digestion
BE_AE2 Betyllium
CD AE2 Cadmium
HG CV2 Mercury
TL_GF^ Thallium
Test Codes and Names
3050 Acid Digestion
BE AE2 Beryllium
CD AE2 Cadmium
HG CV2 Mercury
TL_GF2 Thallium
Test Codes and Names
3050 Acid Digestion
BE AE2 Betyllium
CD AE2 Cadmium
HG_CV2 Mercury
TL_GF'2 Thallium
Test Codes and Names
3050 Acid Digestion
BE_AE2 Beryllium
CD KEl Cadmium
HG CV2 Mercury
TL_GF2 Thallium
Test Codes and Names
3050 Acid Digestion
BE_AE2 Beryllium
CD AE2 Cadmium
HO CV2 Mercury
TL_GF2 Thallium
Test Codes and Names
3010 Acid Digestion
BE_A£2 Beryllium
CD AE2 Cadmium
TL AE2 Thallium
Ha_CV3 Mercury
Test Codes and Names
3050 Acid Digestion
BE_AE2 Beryllium
CD /VE2 Cadmium
HO CV2 Mercury
TL_GF2 Thallium
Test Codes and Names
3050 Acid Digestion
BE AE2 Beryllium
CD AE2 Cadmium
H0~CV2 Mercury
TL_GF2 Thallium
Test Codes and Names
3050 Acid Digestion
BE AE2 Beryllium
CD AE2 Cadmium
HG CV2 Mercury
TL_GF^ Thallium
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 7841
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 7841
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 7841
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 7841
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 7841
Method
SW-846, 3010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7470
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 7841
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 7841
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 7841
Page #:2
Work Order # 9509033 Sample and Test Code Identificttion
Sample ID:
GD #82, 10 FT. M-191
Teiit Codes and Names
3050
BE_A)2
CD_Ai2
HG_C/2
TL G)2
.Acid Digestion
iBeiyllium
Cadmium
Mercury
Thallium
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 7841
Comments
^ZfH^C^^H^
Certified By
Page #:3
This is to certify tfiat the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: GD #28, 5 FT. M-193-N Lab ID: 9509033-OlA CoUected: 09/13/95 15:40:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Mercury
09/20/35
U
11.1
7.20
U
10.2
34.9
5.3
U
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
0.1
0.3
O.a
1.5
0.62
0.2
1.9
0.014
09/20/95
09/21/95
09/21/9S
09/21/95
09/21/95
09/21/95
09/21/95
10/05/95
10/10/95
KWB
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
6010
7060
7471
Sample ID: GD #28, 10 FT. M-193-N LabID: 9509033-02A CoUected: 09/13/95 15:55:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Add Digestion
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Mercury
09/20/95
0.43
10.5
7.90
U
9.26
35.6
5.0
U
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
0.1
0.3
0.1
1.7
0.66
0.3
2.0
0.013
09/20/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
10/05/95
10/10/95
KWB
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
6010
7060
7471
Page #: 4
October 19, 1995 11:07 CERTI]?'IC:ATE OF AN>*ILYSIS
RJiSULTS BY SAMPLE
Sample ID: GD #86, 5 FT. M-193-N lab ID: 9509033-03A CoUected: 09/14/95 10:55:00
TEST RESULT UNJ'.TS DETECTION iiN^l^YZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
Chromium
Copper
Lead
Niclcel
Zinc
Arsenic
Mercury
09/20/95
U
12.4
7.24
U
10.4
35.7
5.9
U
DJ.TE
uc/g
uc/g
uc/g
uc/g
uc/g
uc/g
uc/g
uc/g
0.1
0.3
0.1
1.5
0.65
0.3
1.8
0.014
09/20/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
10/05/95
10/10/95
KWB
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
6010
7060
7471
^^ple ID: GD #86, 10 FT. M-193-N ^ibDD: 9509033-04A CoUected: 09/14/95 11:10:00
TEST RESULT UNITS DETECTION ANJIJiYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Mercury
09/20/95
U
7.80
6,94
U
6.13
29.1
4.7
U
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug-'g
ug'g
ug'g
0.1
0.3
0.1
1.5
0.59
0.2
1.8
0.013
09/20/95
09/21/95
09/21/95
09/:21/95
09/21/95
09/:>l/95
09/21/95
10/05/95
10/:L0/95
KWB
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-84 6,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
6010
7060
7471
Page #: 5
October 19, 1995 11:07 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #105, 5 FT. M-193-N LabID: 9509033-05A CoUected: 09/14/95 11:26:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Mercury
09/20/95
U
12.3
7.81
U
8.65
36.3
47.5
U
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
0.1
0.3
0.1
1.7
0.66
0.3
2.0
0.013
09/20/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
10/05/95
10/10/95
KWB
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
6010
7060
7471
Sample ID: GD #105, 10 FT. M-193-N LabID: 9509033-06A CoUected: 09/14/95 11:38:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Mercury
09/20/95
U
12.9
9.93
U
11.8
41.3
7.4
0.02
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
0.1
0.3
0.1
1.6
0.66
0.3
2.0
0.011
09/20/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
09/21/95
10/05/95
10/10/95
KWB
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
6010
7060
7471
Page tt: 6
October 19, 1995 11:07 CERTIFIC:ATE; OF APsf^O^YSIS
RiSULTS BY SAMPLE
Sample ID: GD #26, 5 FT. M-191 lab ID: 9509033-07A CoUected: 09/14/95 13:00:00
TEST RESULT UN::TS DETECTION ;kN.i^YZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Beryllium
Cadmium
Mercury
Thallium
09/20/95
0.75
U
U
0.5
DJiTE
u< [/g
u<f/g
ucr/g
uc/g
0.1
0.1
0.015
2.5
09/20/95
09/21/95
09/21/95
10/10/95
10/17/95
KWB
LVD
LVD
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
7471
7841
Sample ID: GD #26, 10 FT. M-191 Lab ED: 9509033-08A CoUected: 09/14/95 13:09:00
TEST RESULT UNDTS DETECTION ANJ^YZED BY
LIMIT
METHOD/CAS#
Add Digestion
^^ky Ilium
^Cadmium
Mercury
Thallium
09/20/95
0.74
U
U
U
DfTE
uc/g
uc/g
ug/g
ug/g
0.1
0.1
0.014
2.3
09/20/95
09/21/95
09/21/95
10/10/95
10/17/95
KWB
LVD
LVD
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
7471
7841
Sample ID: GD #43, 5 FT. M-191 Lib uy. 9509033-09A CoUected: 09/14/95 13:30:00
TEST RESULT UNITS DETECTION ANJILLYZED BY
LIMIT
METH0D/CAS#
Add Digestion
Beryllium
Cadmium
Mercury
Thallium
09/20/95
0.85
U
0.02
U
DATE
ug/g
ug/g
ug/g
ug/g
0.1
0.1
0.015
2.6
09/20/95
09/21/95
09/21/95
10/10/95
10/17/95
KWB
LVD
LVD
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
7471
7841
Page tt: 7
October 19, 1995 11:07 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #43, 10 FT. M-191 LabID: 9509033-lOA CoUected: 09/14/95 13:41:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Beryllitim
Cadmium
Mercury
Thallium
09/20/95
0.53
U
U
U
DATE
ug/g
ug/g
ug/g
ug/g
0.1
0.1
0.013
2.6
09/20/95
09/21/95
09/21/95
10/10/95
10/17/95
KWB
LVD
LVD
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
7471
7841
Sample ID: GD #43, 10 FT. DUPLICATE LabID: 9509033-llA CoUected: 09/14/95 13:41:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Add Digestion
Beryllium
Cadmium
Mercury
Thallium
09/20/95
0.53
U
U
U
DATE
ug/g
ug/g
ug/g
ug/g
0.1
0.1
0.013
2.6
09/20/95
09/21/95
09/21/95
10/10/95
10/17/95
KWB
LVD
LVD
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846.
3050
6010
6010
7471
7841
Sample ID: RINSE BLANK, M-191 Lab ID: 9509033-12A CoUected: 09/14/95 13:50:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Beryllium
Cadmium
Thallium
Mercury
09/22/95
U
U
U
U
DATE
ug/L
ug/L
ug/L
ug/L
2
2
50
0.15
09/22/95
09/25/95
09/25/95
09/25/95
09/27/95
LVD
LVD
LVD
LVD
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3010
6010
6010
6010
7470
Page #: 8
October 19, 1995 11:07 m
Sample ID: GD #68, 5 FT. M-191
CERTI]7IC:ATE OF AN/ILYSIS
RJiSULTS BY SAMPLE
lab ID: 9509033-13A CoUected: 09/14/95 14:25:00
TEST RESULT UNJ.TS DETECTION AN;MJYZED BY
LIHIT
METH0D/CAS#
Add Digestion
Beryllium
Cadmium
Mercury
Thallium
09/20/95
0.85
U
U
U
DJ.TE
uct/g
uc;/g
uc/g
uc/g
0.1
0.1
0.015
2.5
09/20/95
09/21/95
09/21/95
10/10/95
10/17/95
KWB
LVD
LVD
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
7471
7841
Sample ID: GD #68, 10 FT. M-191 Lab ED: 9509033-14A CoUected: 09/14/95 14:36:00
TEST RESULT UNITS DETECTION ANJ^YZED BY
LIMIT
METHOD/CAS#
Add Digestion
^^^yllium
Cadmium
Mercury
Thallium
09/20/95
0.57
U
U
U
D/TE
uc/g
uc/g
uc/g
uc/g
0.1
0.1
0.013
2.6
09/20/95
09/21/95
09/21/95
10/10/95
10/18/95
KWB
LVD
LVD
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
7471
7841
Sample ID: GD #82, 5 FT. M-191 Lib m: 9509033-15A CoUected: 09/14/95 14:52:00
TEST RESULT UNITS DETECTION ANJLLYZED BY
LIMIT
METHOD/CAS#
Add Digestion
Beryllium
Cadmium
Mercury
Tha 11 liom
09/20/95
0.75
U
U
U
D*rE
ug/g
ug/g
ug/g
ug/g
0.1
0.1
0.011
2.5
09/20/95
09/21/95
09/21/95
10/10/95
10/18/95
KWB
LVD
LVD
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
7471
7841
Page tt: 9
October 19, 1995 11:07 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #82, 10 FT. M-191 LabID: 9509033-16A CoUected: 09/14/95 15:13:00
TEST
Add Digestion
Beryllium
Cadmium
Mercury
Thallium
RESULT
09/20/95
0.81
U
U
U
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
DETECTION
LIMIT
0.1
0.1
0.012
2.6
ANALYZED
09/20/95
09/21/95
09/21/95
10/10/95
10/18/95
BY
KWB
LVD
LVD
CRS
CRS
METHOD/CAS#
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 7841
Page tt: 10
Data Reporting Qualifiers
U Compound was analyzed for but noit detected. Indicates compound was below detection limit.
J Indicates an estimated value. This ilag is used either when estimating a concentration for
tentatively identified compoi inds or when the mass s]jectral data indicated the presence of a
compound that meets the ide ntification criteria but the result is less than the specified
detection limit but greater th in zero. (e. g. l.U with a detection Umit of 5.0)
B This flag is used when an analy te is found in the blank as weU as the sample.
E Estimated value. Result was oitsid; of the caUbration lange but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was nct tested for.
Q Surrogate/spike recovery was o itside of the specified limits.
ENVIRONMENTAL LAB WORK RIEQUEST
^"^fFZ ^
f ^ •- ^
™ THIOKOL ENVIRONMENTAL LABORATORY LWR No. E1I048
FROM:
A F ^aliTiy
ORGANIZATION
Enuirortinin/aJI
EXVENSION
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WORK ORDER
IB940
DATE
9-/e''fF
REPORT RESULTS TO:
HELEN WARD, MS 301
SAMI LE INFORMATION
SAMPLE
Cd.^14 2fr
DATE
9-/0'9i'
TYPE
y
LOCATION TIME
0^0 &
TEST
yoc
REMARKS
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FOR LAI ORATORY USE ONLY
DATE COMPLETED DATE REPORTED
ENVIRONME :NTAL LAB WORK REQUEST
"* iUlOKOL ENVIRONMENTAL LABORATORY >^///)'4A TPQ^Se^ 2
moM, •XTVOiaH
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HELEN WARD, MS 301 |
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CHAIN OF CUSTODY
SEIJNQIJISHESBY DATE TIME RECEIVEl) BY
1 _ ._
DATE TIME
FOR LABORATORY USE ONLY
DATS COMTLEia} DATS MKIKIKU acKAnu w
ENVraONMENTAL, LAB WORK REQUEST
'^ THIOKOL ENVIRONMENTAL LABORATORY
V noMi
OaCAfOZATION
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COST UMIU WOBKOBim DAn
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SAMPLE [NFORMATION
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SEUNQUSHESBY OATE '.IME KECEZVESBY DATE TIME
POR LAI ;ORji.TORY USE ONLY
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HELEN WARD, MS 301
SAMFLE INFORMATION
SAMPLE
1 ^ Cd-^^C
^
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7.
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CHAIN OF CUSTODY
REUNQUSHEI) BY DATE TIME RECOVE!) BY DATE TIME
lUnCOMFLETSD
FOR LABORATORY USE ONLY
DATBRiromD ncKAivu
w
October 18, 1995
m
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
ENT Environmental Monitoring
TO: Helen Ward M/S 301
Thiokol Corp, Ut 84322
A.F. WALKER
EXT 5390
iLNALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham aty. Ut 84302-0707
Analytical Labs M/S 245
Atm: Dr. John Terry
Tele: 801-863-2384
Work Order # 9509035 Sample and Tast (!!ode Identification
LabID:
OIA
Sample ID:
GD #14, 2 FT. M-136
Tesl Codiis and Names
LabID:
02A
Sample ID:
GD#14, 5 ft. M-136
03A
Sample ID:
RINSE BLANK, M-136
LabID:
04A
Sample ID:
OD#32, 2 FT. M-136
LabID:
05A
Sample ID:
GD #32, 5 FT. M-136
LabID:
06A
Sample ID:
GD #51, 2 FT. M-136
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8260S
HMX
N itroglycerine
A ;id Dijgestion
C idmium
C iromium
Liad
Si Iver
}-/, ercur>
V >latile Organics
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8260S
HvlX
Ntroglycerine
A' :id Di);estion
Cndmiuin
Chromium
bad
Si ver
M Jrcury
Vl ilatile Organics
Test Codes and Names
HMX
NG
3010
CD AE2
CR AE2
PB AE2
AG AE2
HG CV3
8260
WtTX.
Ni troglyc:erine
Al id Di{;estion
Ct dmium
Cl romium
Lod
Sil ver
M' srcury
Vl latile iDrganics
Test Codes and Names
HMX
NO
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8260S
HHX
Ni roglycerine
A< Id Digestion
Ct dmium
Cll romium
Lcid
Sil /er
Ml rcuty
Vc latile Organics
Test Coden and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8260S
HIK
Nilroglycerine
Ac id Digestion
Ca Imium
Cil romium
Leid
SiWer
M( rcuty
Vo latile Organics
Test Codeii and Names
Method
SOP 420
SOP 420
SW-846, 3050
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,8260A
Method
.6010
,6010
,6010
,6010
,7471
HMX HMX
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7470
SW-846,8260A Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
Pa.ge#:lof W
Work Orderly 9509035 Sample and Test Code Identification
LabID:
06A
Sample ID:
GD#5T7TFT. M-136
Lab ID:
07A GD nple
#5l7 5 FT. M-136
LabID:
08A
Sample ID:
GD #44, 2 FT. M-136
LabID:
09A
LabID:
lOA
Sample ID:
GD #44, 2 FT. M-136 DUP.
lelD:
GD #44, 5 FT. M-136
Lab ID:
llA
Sample ID:
GD #83, 2 FT. M-136
LabID:
12A
Sample ID:
GD #'83, 5 FT. M-136
LabID:
13A
Sample ID:
GD #94, 2 FT. M-136
Test Codes and Names
NO
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8260S
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8260S
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics '
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8260S
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercuiy
Volatile Organics
Test Codes and Names
8260S Volatile Organics
Test Codes and Names
HMX
NO
3050
CD AE2
CR AE2
PB AE2
Ad'AE2
HG CV2
8260s
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NO
3050
CD AE2
CR AE2
PB AE2
Ad'AE2
Ha"CV2
8260s
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercuiy
Volatile Organics
Test Codes and Names
HMX
NO
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8260s
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercuiy
Volatile Organics
Test Codes and Names
HMX
NQ
3050
CD AE2
CR"AE2
PB AE2
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Method
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
Page #:2
Work Order j}* 9509035 Sample ai id Test Code Identif ictition
0«^ Sample ID:
GD #94, 2 FT. M-136
Test Codes imd Names
LabID: Sample ID:
14A GD #94, 5 FT. M-136
LabID: Sample ID:
GD #101, 2 FT. M-136
LabID:
16A
Sample ID:
GD #101, 5 FT. M-136
>Lab ID:
17A
Sample ID:
GD #92, 2 FT. M-136
LabID:
18A
Sample ID:
GD m, 5 FT. M-136
LabID:
19A
Sample ID:
GD #92, 5 FT. M-136 DUP.
LabID:
20A
Sample ID:
GD #96, 2 FT. M-136
AG AJ-2
HG ca
8260s
Silver
Mercuiy
Volatile Organics
Test Codes and Names
HMX
NG
3050
CD A12
CR A12
PB AI2
AG Ai2
HG C'2
826SS
HMX
Iilitroglycerine
/Vcid Digeslion
Cadmium
Chromium
I.ead
Siilver
Mercuiy
^^olatile Organics
Test Codes and Names
HMX
NG
3050
CD AJ2
CR AI2
PB AE2
AG A12
HG 07
8260s
HMX
Nitroglycerine
/kcid Digestion
Odmium
Ciiromium
I.ead
Silver
Mercury
X'olatile Orgamcs
Tesi: Codes and Names
HMX
NO
3050
CD A12
CR AI2
PB A£l
AO AI2
HO CA2
8260s
HMX
Mitroglycerine
/icid Digestion
Cladmium
Cluomium
Lead
Silver
Mercury
\'olatile Organics
Tesl; Codes and Names
HMX
NG
3050
CD AI2
CR AI2
PB AE!
AG AI2
HG C\2
8260s
FMX
Mitroglycerine
A.cid Digestion
Cadmium
Chromium
Lead
Silver
Mercuiy
V olatile Oi^amcs
Test Codes and Names
HMX
NO
3050
CD A£2
CR AEJ
PB AE: AO AI2
HO C\2
8260s
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
SJver
Mercury
Volatile Organics
Test Codes and Names
HMX
NO
3050
CD AE2
CR AEJ
PB AE:
AO AE2
HG CV2
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
\^[ercury
Test Codes and Names
HMX
NO
3050
CD AEJ
HMX
Nitroglycerine
Acid Digestion
Cadmium
Method
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471 Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
Page tt:3
Work Order # 9509035
LabID: Sample ID:
20A OD j(96, 2 FT. M-136
Sample and Test Code Identification
LabID:
21A
lelD:
OD #96, 5 FT. M-136
Test Codes and Names
CR AE2
PB AE2
AG AE2
HG CV2
8260S
Chromium
Lead
Silver
Mercuiy
Volatile Organics
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AO AE2
HG c:v2
8260S
HMX
Nitroglycerine
Acid Digestion
Cadinium
Chromium
Lead
Silver
Mercuiy
Volatile Organics
Comments
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
^9^
Certified By
Page #:4
i^
This is to certify that tfie following samples were cmalyzed using good laboratory practices
io sfutw tlie folio-wing results.
Sample ID: GD #14, 2 FT. M-136 Lab ED: 9509035-01A CoUected: 09/18/95 08:06:00
TEST
HMX
Nltroglycerlne
Add Digestion
Cadmium
Chromium
Lead
Sliver
Mercury
Volatile Organics
benzene
bromobenzene
J^unochl orome thane
^^Bnodi chl or ome thane
IRRmoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chlorofonn
chloromethame
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropan
1,2-dibromoethane
dibromomethane
di chlorodi fluorome thane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropane
1,1-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
^^-dichlorobenzene
^^^ dichlorobenzene
RESULT
U
U
09/20/95
U
20.9
U
U
0.01
U
U
u
u
u
u
D
U
U
U
U
u
u
u
u. u D
U
U
u
u
u
u
u
u
u
u
D
U
u
u
u D
U
T3N]TS
MCKG
MG'KG
D/TE
uc/g
uc/g
uc/g
uo/g
ug/g
ug 'Kg
ug 'Kg
ug'Kg
ug'Kg
ug'Kg
ug.'Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug,
ug;
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug,
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
ug. Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/ Kg
DETECTION
LIMIT
0.500
0.500
0.1
0.3
1.6
0.2
0.011
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANJU;.YZED
09/22/95
09/22/95
09/20/95
09/21/95
09/21/95
09/21/95
09/21/95
10/10/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
Page tt: 5
October 18, 1995 11:12 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #14, 2 FT. M-136 LabID: 9509035-OlA Collected: 09/18/95 08:06:00
TEST
Volatile Organics
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2- tetrachloroetheuie
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,l-trichloroethane
1,1,2-trichloroetheme
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexcmone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
14B
U
U
U
U
U
U
U
U
U
u
u
u
u 686951
371756
107278
Surrogat
Surrogate
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
e/Recovery Data For Volatile Organics 8260S
dibromofluoromethane
1,2-dichloroetheme-d4
toluene-d8
bromofluorobenzene
%Recovery
82.3
80.2
117
113
METHOD/CAS#
SW-846,8260A
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8 ^^
75-01-4 ^V
95-47-6 ^
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #14, 5 ft. M-136 LabID: 9509035-02A CoUected: 09/18/95 08:14:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMX U MG/KG 0.500 09/22/95 KMS SOP 420
Page tt: 6
Dctober 18, 1995 11:12 CERTIFIC A11E OF ANALYSIS
RESULTS BY SAMPLE
ample ID: GD #14, 5 ft. M-136 LabID: 9509035-02A CoUected: 09/18/95 08:14:00
EST
Ltroglycerlne
::ld Digestion
idmium
.iromium
aad
liver
arcury
3latlle Organics
anzene
romobenzene
romochloromethane
romodi chloromethane
romoform
ronM^ thane
-b^^Bbenzene
ec^Mrcylbenzene
ert-butylbenzene
arbon tetrachloride
hlorobenzene
hloroethane
hloroform
hloromethane
-chlorotoluene
-chlorotoluene
'.ibromochl orome thane
,2-dibromo-3-chloropropcui
,2-dibromoethane
•ibromome theme
iichlorodifluoromethane
,1-dichloroetheme
,2-dichloroethane
,1-dichloroethene
is-1,2 -dichloroethene
rans-1,2-dichloroethene
,2-dichloropropame
,3 -dichloropropane
,2-dichloropropeme
,1-dichloropropene
is-1,3-dichloropropene
rans-1,3-dichloropropene
,2 -di chlorobenzene
,3-dichlorobenzene
,4 -dichlorobenzene
thyUaenzene
ex^^^robutadiene
RESULT
u
09/20/95
U
18.1
U
U
0.01
U
a u u u u u u u u u u u u u u u u
u u
u u u u u u u
u u u u u u u u u u
UNITS
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DEITECTION
LIMIT
0.500
0.1
- 0.3
1.6
0.2
0.012
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANAI.Y:ZED
09/22/95
09/20/95
09/21/95
09/21/95
09/21/95
09/21/95
10/10/95
09/27/95
09/27/95
09/27/«i5
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/S5
09/27/S5
09/27/35
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
BY
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
Page tf: 7
October 18, 1995 11:12 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #14, 5 ft. M-136 LabID: 9509035-02A CoUected: 09/18/95 08:14:00
TEST
Volatile Organics
isopropylbenzene
4 - isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
RESULT
u
u
4.5BJ
U
D
U
1,1,1,2-tetrachloroethame U
1,1,2,2-tetrachloroethame U
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-tri chloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexamone
fluorobenzene
chlorobenzene- d5
1,4 -dichlorobenzene-d4
U
U
U
U
IOB
U
tr
u u u u u u u 4.4J
U
U
U
933725
447481
109739
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
HMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluoromethane
1 ,2 -dichloroethame-d4
toluene-d8
bromofluorobenzene
%Recovery
77.7
72.8 Q
125
118
METHOD/CAS#
SW-846,8260A
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
9S-18-4
95-63-6
108-67-8
75-01-4
95-47-6 ^^
108-38-3 ^B
67-64-1 ^W
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Racovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: RINSE BLANK, M-136 LabID: 9509035-03A CoUected: 09/18/95 08:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMX
Nltroglycerlne
u
u
UG/L
UG/L
500.
500.
09/25/95
09/25/95
KMS
KMS
SOP 420
SOP 420
Page tt: 8
October 18, 1995 11:12
r
ample ID: RINSE BLANK, M-136
CERTIFICATE OF ANALYSIS
RESI LTS BY SAMPLE
Lab iD: 9509035-03A CoUected: 09/18/95 08:20:00
EST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
cld Digestion
admium
hromliim
aad
liver
arcury
olatile Organics
enzene
romobenzene
romochloromethame
romodi chloromethane
romoform
romometheme
-butylbenzene
sc^^tylbenzene
eij^^Kitylbenzene
ar^^ tetrachloride
hlorobenzene
tiloroe thame
hloroform
hlorometheme
-chlorotoluene
-chlorotoluene
ibromochloromethame
,2 -dibromo-3-chloropropem
.,2 -dibromoethane
Iibromomethane
Iichlorodifluorometheme
.,1-dichloroethame
.,2 -di chloroethane
.,1-dichloroethene
is-1,2-dichloroethene
rams-l,2-dichloroethene
,2-dichloropropeme
,3 -dichloropropane
,2-dichloropropeme
,l-dichloropropene
is-1,3-dichloropropene
trams -1,3- dichloropropene
,2-dichlorobenzene
,3-dichlorobenzene
,4-dichlorobenzene
ihylbenzene
2xachlorobutadiene
sopropylbenzene
- i €^^opyl toluene L^B|0
09/22/95
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
DATE
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0,
0
0
0
0
0.
0,
0,
0,
0,
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0,
0.
2
5
25
3
.15
.20
.20
.20
.30
.10
.40
.20
.20
.20
.30
.20
.40
.40
.60
.20
.20
.30
.20
.20
.20
.20
.10
.20
.60
,20
,20
,20
,20
.20
.20
.20
.20
.10
,20
,20
.30
,20
,20
.20
09/22/95
09/25/95
09/25/95
09/25/95
10/05/95
09/27/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/SI5
09/19/515
09/a9/«i5
09/19/SI5
09/19/95
09/19/SI5
09/19/95
09/19/95
09/19/S5
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JHA.
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3010
6010
6010
6010
6010
7470
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-
10061-02-
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
•5
•6
Pa§;e tf: 9
October 18, 1995 11:12 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: RINSE BLANK, M-136 LabID: 9509035-03A CoUected: 09/18/95 08:20:00
TEST
Volatile Organics
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethame
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butamone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
1.6 B
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u u
u 89
6.1 J
u 1.4 J
1118229
706432
263113
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
0.30
0.20
0.20
0.20
0.20
0.30
0.90
0.30
0.20
0.20
0.20
0.20
0.30
0.30
0.20
0.20
0.20
0.40
0.20
0.20
10
10
10
10
ANALYZED
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
09/19/95
Surrogate/Recovery Data For Volatile Organic
Surrogate
dibromofluoromethane
1,2 -di chloroetheme-d4
toluene-d8
bror nofluorobenze ne
%Recovery
99.7
105
98.0
107
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
s 8260
METHOD/CAS#
SW-846,8260A
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1 ^^
78-93-3 ^B
108-10-1 ^W
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
80.0
80.0
80.0
80.0
TO 120
TO 120
TO 120
TO 120
Sample ID: GD #32, 2 FT. M-136 LabID: 9509035-04A CoUected: 09/18/95 09:02:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMX
Nitroglycerine
Acid Digestion
U MG/KG
U MG/KG
09/20/95 DATE
0.500 09/22/95 KMS SOP 420
0.500 09/22/95 KMS SOP 420
09/20/95 KWB SW-846, 3050
Page tt: 10
October 18, 1995 11:12
Sample ID: GD #32, 2 FT. M-136
CERTIFICATE OF ANiU^YSIS
' RESULTS BY SAMPiJ:
l-ablD: 9509035-04A CoUected: 09/18/95 09:02:00
TEST
Cadmixim
Chromium
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodichloromethane
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
^^bon tetrachloride
^^•Lorobenzene
^Wl oroe thane
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3-chloropropem
1,2-dibromoetheme
dibromomethane
dichlorodifluorometheme
1,1-dichloroethane
1,2 -dichloroetheme
1,1-dichloroethene
cis-l,2-dichloroethene
trams-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropame
2,2-dichloropropane
1,l-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
^^^hthal ene
RESULT
U
19.3
2.50
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u u
o
u
u
u
u
u
u
u
u
u
u u
u
u
u u
u
u u
UNETS
u?/g
u3/g
uj/g
uj/g
uj/g
uc/Kg
uc:/Kg
uc/Kg
uc/Kg
uc,7Kg
ucf/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc /Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc /Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
DETECTION
LIMIT
0.1
0.3
1.5
0.2
0.013
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
i^NALYZED
09/21/95
09/21/95
09/21/95
09/21/95
10/10/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
BY
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
Page#: 11
October 18, 1995 11:12 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #32, 2 FT. M-136 LabID: 9509035-04A CoUected: 09/18/95 09:02:00
TEST
Volatile Organics
n-propylbenzene
styrene
1,1,1,2-tetrachloroethame
1,1,2,2-tetrachloroethame
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,l-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4 -methyl - 2 -pentamone
2-hexanone
fluorobenzene
chlorobenzene- d5
1,4-dichlorobenzene-d4
RESULT
u u u U
U
U
U
U
12B
U
U
U
U
U
U
U
u
u
u u u
u 763250
374843
104983
Surrogat
Surrogate
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
e/Recovery Data For Volatile Organics 8260S
dibromofluoromethane
1,2-dichloroethane-d4
toluene-d8
bron lof luoro benze ne
%Recovery
82.2
77.5
123
109
METHOD/CAS#
SW-846,8260A
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1 ^^
591-78-6 ^^
INTSTDl ^^-
INTSTD2
INTSTD3
Recovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #32, 5 FT. M-136 LabID: 9509035-05A CoUected: 09/18/95 09:09:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMX
Nitroglycerine
Acid Digestion
Cadmium
u
u
09/20/95
U
MG/KG
MG/KG
DATE
ug/g
0.500
0.500
0.1
09/22/95
09/22/95
09/20/95
09/21/95
KMS
KMS
KWB
LVD
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
Page tf: 12
October 18, 1995 11:12 CERTI]FIC:ATE OF A?^^LLYSIS
RJiSULTS BY SAMPLE
Sample ID: GD #32, 5 FT. M-136 lab ID: 9509035-05A CoUected: 09/18/95 09:09:00
TEST
Chromium
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenz ene
bromochloromethame
bromodi chlorometheme
bromoform
brcjmome thane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
cW. oroe thame
^^^oroform
^^orome theme
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3 -chloropropan
1,2-dibromoethane
dibromome theme
dichlorodifluorometheme
1,1-di chloroe theme
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans -1,2-dichloroethene
1,2-dichloropropeme
1,3 -dichloropropeme
2,2-dichloropropane
1,l-dichloropropene
cis-1,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4 - di chlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 - isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
^^rene
RESULT
19.6
U
U
U
U
U
U
u
u u
u u u u u u u u u u u u u u u u
u
u u u
u
u u . u
u u u u u u u u
u 4. IB J
u
u
u
UN::TS
u<(/g
uir/g
u<r/g
u<r/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug'Kg
ug/Kg
ug/Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
DETECTION
LIMIT
0.3
1.6
0.2
0.012
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
AN.I^YZED
09/21/95
09/21/95
09/21/95
10/10/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
BY
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
Page tt: 13
October 18, 1995 11:12 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #32, 5 FT. M-136 LabID: 9509035-05A CoUected: 09/18/95 09:09:00
TEST
Volatile Organics
RESULT
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-dS
1,4-dichlorobenzene-d4
U
U
U
U
u u IOB
u u u u
u
u
u u
u 5J
U
U
U
818190
414201
130629
Surrogat
Surrogate
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
e/Recovery Data For Volatile Organics 8260S
dibromof1uoromethane
1 ,2-dichloroetheme-d4
toluene-d8
bromofluorobenz* ane
%Recovery
82.2
81.2
117
104
METHOD/CAS#
SW-846,8260A
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl ^^
INTSTD2 ^B
INTSTD3 ^^
Recovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #51, 2 FT. M-136 Lab ID: 9509035-06A CoUected: 09/18/95 10:06:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMX
Nltroglycerlne
Add Digestion
Cac3mlum
Chromium
u
u
10/05/95
0.85
25.9
MG/KG
MG/KG
DATE
ug/g
ug/g
0
0
.500
.500
0.1
0.3
09/22/95
09/22/95
10/05/95
10/11/95
10/11/95
KMS
KMS
KWB
LVD
LVD
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
Page tt: 14
October 18, 1995 11:12
ample ID: GD #51, 2 FT. M-136
CERTIFICAirE OF ANALYSIS
r^ RESULTS BY SAMPLE
LabID: 9509035-06A CoUected: 09/18/95 10:06:00
EST
aad
liver
arcury
slatlle Organics
anzene
romobenzene
romochloromethane
romodi chlorome thane
romoform
romomethame
-butylbenzene
ac-butylbenzene
art-butylbenzene
arbon tetrachloride
hlorobenzene
hloroethane
hloroform
hloromethane
- (j^j^Brotoluene
- c^^Brotoluene
ib^Ro chlorome thane
,2 -dibromo-3-chloropropan
,2-dibromoethane
ibromomethame
ichlorodifluoromethane
,1-dichloroetheme
,2-dichloroetheme
,1-dichloroethene
jis-1,2-dichloroethene
irans-1,2-dichloroethene
L,2-dichloropropane
L,3-dichloropropame
2,2-dichloropropane
L,1-dichloropropene
::iB-l, 3-dichloropropene
rans-1,3-dichloropropene
,2-dichlorobenzene
,3 -dichlorobenzene
,4-dichlorobenzene
thylbenzene
axachlorobutadi ene
sopropylbenzene
-isopropyltoluene
athylene chloride
aphthalene
-propylbenzene
tyrene
,1,1,2-tetrachloroetheme
,1,j^2-tetrachloroethane
RESULT
u
u
u
u
u u
u
u u u u u u u
u u u
u u u u u u u u u u u u u u u u
u
u u u u u
u u
u 5. IB J
u
u u u u
UNITS
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
1.6
0.2
0.012
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANA]JYZED
10/11/95
10/11/95
10/10/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/:95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/;i5
09/27/95
BY
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
Page tt: 15
October 18, 1995 11:12 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #51, 2 FT. M-136 LabID: 9509035-06A CoUected: 09/18/95 10:06:00
TEST
Volatile Organics
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5 -trimethylbenzene
vinyl chloride
o-xylene
m.p-xylene
acetone
2-butemone
4-methyl-2-pentanone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
7.
U
U
U
U
8BJ
U
U
U
U
U
U
U
U
U
U
U
U
U
488358
325080
120894
Surrogat
Surrogate
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
e/Recovery Data For Volatile Organic
dibromofluoromethane
1 ,2 -dichloroethane-d4
toluene-d8
bromofluorobenzene
%Recovery
84.6
90.9
108
101
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
B 8260S
METHOD/CAS#
SW-846,8260A
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3 jj^
9
Recovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #51, 5 FT. M-136 LabID: 9509035-07A CoUected: 09/18/95 10:12:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMX
Nltroglycerlne
Acid Digestion
Cadmium
Chromium
Lead
U
u
10/05/95
U
23.4
U
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
0
0
.500
.500
0.1
0.3
1.6
09/22/95
09/22/95
10/05/95
10/11/95
10/11/95
10/11/95
KMS
KMS
KWB
LVD
LVD
LVD
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
Page#: 16
October 18, 1995 11:12
ila^ire ,e ID: GD #51, 5 FT. M-136
CERTIFI CATE OF ANALYSIS
. y RESULTS BY SAMPLE
LabID: 9509035-07A CoUected: 09/18/95 10:12:00
TEST
Silver
Mercury
/olatile Organics
oenzene
^romobenzene
bromochloromethame
jromodichloromethame
sromoform
jromomethane
1-butylbenzene
iec-butylbenzene
:ert-butylbenzene
:arbon tetrachloride
ihlorobenzene
:hloroe thame
:hloroform
•hlorome thame
-chlorotoluene
-chlorotoluene
ibromochlorcjme thane
, 2^^romo- 3 - chloropropem
, 2^^^romoethame
ib^Beme thane
i chlorodi fluorome thane
,1-dichloroethane
,2-dichloroethame
,1-dichloroethene
is-1,2-dichloroethene
rans-1,2-dichloroethene
,2 -dichloropropame
,3-dichloropropane
,2-dichloropropane
,1-dichloropropene
is-1,3-dichloropropene
rans-1,3-dichloropropene
,2-dichlorobenzene
,3-dichlorobenzene
4 -dichlorobenzene
-hy Ibenz ene
!xachlorobutadi ene
lopropylbenzene
isopropyltoluene
thylene chloride
phthalene
propylbenzene
yrene
1,1,2-tetrachloroethane
1,2,2-tetrachloroethane
trachloroethene
luene
2,3-trichlorobenzene
RESULT
u
0.01
u u u u u u u u
u
u u u u
u
u u u
u
u u
u
u
u
u
u u
u u
u u u u
u u u u
u u
u u u
u u u u u u u
UNITS
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.2
0.012
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/11/95
10/10/95
09/27/95
09/27/95
,09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/9E-)
09/27/9Ei
09/27/9Ei
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
BY
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
Iage#: 17
October 18, 1995 11:12 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #51, 5 FT. M-136 LabID: 9509035-07A CoUected: 09/18/95 10:12:00
TEST
Volatile Orgamlca
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropame
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
Tl,p-xylene
acetone
2-butcmone
1 -methyl - 2 -pentamone
2-hexemone
fluorobenzene
:hlorobenzene-d5
.,4 -dichlorobenzene-d4
RESULT
u 8.5BJ
u U
U
U
U
U
U
U
U
U
U
U
U
911769
448826
125167
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10 .
10
10
10
10
10
10
10
ANALYZED
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatila Organics 8260S
Surrogate
dibromofluorometheme
1 ,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
ample ID: GD #44, 2 FT.
EST
M-136
RESULT
LabID
UNITS
%Recovery
82.7
82.8
119
110
METHOD/CAS#
SW-846,8260A
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
A
Recovery Limits \
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
: 9509035-08A CoUected: 09/18/95 10:32:00
DETECTION
LIMIT
ANALYZED BY METHOD/CAS#
TL
troglycerlne
id Digestion
imium
romium
id
ver
u
u
/05/95
u
21.5
U
U
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
0
0
.500
.500
0.1
0.3
1.6
0.2
09/22/95
09/22/95
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
KMS
KMS
KWB
LVD
LVD
LVD
LVD
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Page#: 18
October 18, 1995 11:12 CERTI FIC:ATE OF AN^O^YSIS
RESULTS BY SAMPLE
Sample ID: GD #44, 2 FT. M-136 lab ID: 9509035-08A CoUected: 09/18/95 10:32:00
TEST
Mercury
Volatile Organics
benzene
bromobenz ene
bromochloromethane
bromodichlorometheme
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethame
1,2-dibromo-3 -chloropropem
d^ - dibromoetheme
^^P)r omome thame
^jRhlorodif luoromethame
1,1-dichloroethame
1,2-dichloroethame
1,1-dichloroethene
cis-1,2-dichloroethene
trams-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis-l,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3 -di chlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4-isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethame
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1^2,4 -trichlorobenzene
^^, l-trichloroetheme
RESULT
U
U
u u u u u u u u u u u u u u u u D
u u u u u u u u u u u u u
u u u u u u u
u 3.8BJ
u
u u u u . u
u u u 8.5BJ
UN:CTS
u'.j/g
uc /Kg
uc /Kg
uc/Kg
uc/Kg
uc/Kg
uo/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug /Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
DETECTION
LIMIT
0.015
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 -
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ikNALYZED
10/10/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
BY
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
Page tt: 19
October 18, 1995 11:12 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #44, 2 FT. M-136 LabID: 9509035-08A CoUected: 09/18/95 10:32:00
TEST
Volatile Organics
1,1,2-trichloroetheme
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl- 2-pentemone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
U
U
U
U
U
U
U
U
U
U
U
U
U
812614
384026
93649
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorometheme
1 ,2-dichloroetheme-d4
toluene-d8
bromofluorobenzene
%Recovery
82.0
77.4
125
122
METHOD/CAS#
SW-846,8260A
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
^ 9
Sample ID: GD #44, 2 FT. M-136 DUP. LabID: 9509035-09A CoUected: 09/18/95 10:32:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chloromethane
bromoform
bromome thane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethame
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
u
u u u u u u u u
u u u
u u u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
Page ff: 20
October 18, 1995 11:12
•
CERTIFIC ATO OF ANALYSIS
;•,. RESU LTS BY SAMPLE
ample ID: GD #44, 2 FT. M-136 DUP. LabID: 9509035-09A CoUected: 09/18/95 10:32:00
EST RESULT UNITS DETECTION ANAI,YZED BY
LIMIT
METHOD/CAS#
3latlle Organics
,2 -dibromo-3-chloropropem
,2-dibromoethane
ibromomethane
ichlorodifluorometheme
,1-dichloroethane
,2-dichloroethane
,1-dichloroethene
is-1,2-dichloroethene
rems-1,2-dichloroethene
,2-dichloropropane
,3-dichloropropame
,2-dichloropropane
,1-dichloropropene
i s-1,3 -di chloropropene
rans-1,3 -dichloropropene
,2-dichlorobenzene
,3-dichlorobenzene
,4-dichlorobenzene
thylbenzene
exachlorobutadiene
sop^^ylbenzene
- ij^Hopyl toluene
etll^ne chloride
aphthalene
-propylbenzene
tyrene
,1,1,2-tetrachloroetheme
,1,2,2-tetrachloroethane
etrachloroethene
oluene
,2,3-trichlorobenzene
,2,4-trichlorobenzene
,1,1-trichloroethane
,1,2 -trichloroethane
richloroethene
richlorofluoromethane
,2,3-trichloropropame
,2,4-trimethylbenzene
,3,5-trimethylbenzene
inyl chloride
-xylene
,p-xylene
cetone
-butemone
-methyl-2-pentemone
-hexamone
luorobenzene
hlorobenzene-d5
,4-dichlorobenzene-d4
u
u u u u u u u u u u u u u u
u u
u u u u
u 4.7BJ
U
U
U
U
u u u u
u 15B
u u
u u
u u u
u
u u u
u u 685598
336426
85352
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
'09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Pag(i tt: 21
October 18, 1995 11:12 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #44, 2 FT. M-136 DUP. LabID: 9509035-09A CoUected: 09/18/95 10:32:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Surrogate/Recovery
Surrogate
dibromofluoromethane
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
Data For Volatile
%Recovery
78.7
82.0
122
119'
SW-846,8260A
Organics 8260S
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Sample ID: GD #44, 5 FT. M-136 LabID: 9509035-lOA CoUected: 09/18/95 10:40:00
TEST
HMZ
Nitroglycerine
Add Digestion
Cadmliim
Chrcjmlum
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethame
bromodi chloromethame
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
RESULT
U
u
10/05/95
0.27
20.0
u
U
U
u
u D
U
O
U
U
O
U
U
U
u
u
u
u
u
UNITS
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.500
0.500
0.1
0.3
1.5
0.2
0.014
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/22/95
09/22/95
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/10/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SOP 420
SOP 420
SW-846, 3050 ^^
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6 .
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4 ^^
Page tf: 22
October 18, 1995 11:12 CERTIFICATE OF ANiU^YSIS
RESULTS BY SAMPLE
Sample ID: GD #44, 5 FT. M-136 lab ID: 9509035-lOA CoUected: 09/18/95 10:40:00
TEST RESULT UNITS DETECTION J^NALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
dibromochlorometheme
1,2-dibromo-3-chloropropan
1,2-dibromoethane
dibromometheme
dichlorodifluoromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trams-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropane
1,1-dichloropropene
cis-1,3 -dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
l^cachl orobutadi ene
^^^propylbenzene
^B^ Bopropyl toluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene -v'
trichlorofluorometheme
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4 -me thyl-2 -pentanone
2-hexanone
fluorobenzene
chlorobenzene- d5
1,4-dichlorobenzene-d4
u
u u u
u u u u u u u u u u u
u u
u
u u
u
u u
u u
u u u u u u u
u 13B
u
u u u . u
u
u u u 3.2 J
u u u 708758
329882
103514
uc/Kg
uc/Kg
uc/Kg
uc /Kg
uc/Kg
uc /Kg
uc/Kg
uc /Kg
uc/Kg
uc/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug /Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug/Kg
ug/Kg
ug.'Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug'Kg
ug 'Kg
ug'Kg
ug. 'Kg
10
10
10
10
10
10
ID
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Page tt: 23
October 18, 1995 11:12 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #44, 5 FT. M-136 LabID: 9509035-lOA CoUected: 09/18/95 10:40:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Surrogate/Re covery
Surrogate
dibromofluoromethane
1,2-dichloroetheme-d4
toluene-d8
bromofluorobenzene
Data For Volatile
%Recovery
74.2 Q
75.2
125
104 ,
SW-846,8260A
Organics 8260S
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Sample ID: GD #83, 2 FT. M-136 LabID: 9509035-llA CoUected: 09/18/95 10:59:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMZ
Nltroglycerlne
Acid Digestion
Cadmium
Chromium
Lead
Silver
Hercury
Volatile Organics
benzene
bromobenzene
bromochloromethame
bromodichlorometheme
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethame
2 -chlorotoluene
4 -chlorotoluene
u
u
10/05/95
0.27
20.6
U
U
U
U
U
u u u u
u
u u u u u
u u u u
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.500
0.500
0.1
0.3
1.5
0.2
0.014
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/22/95
09/22/95
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/10/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
Page ff: IA
October 18, 1995 11:12
Sample ID: GD #83, 2 FT. M-136
CERTIFICATE OF AIV^yLYSIS
R EStLTS BY SAMPLE
Ub][D: 9509035-llA CoUected: 09/18/95 10:59:00
TEST RESULT UNITS DETECTION :RLNALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
dibromochloromethane
1,2-dibromo-3-chloropropem
1,2-dibromoethane
dibromometheme
dichlorodifluoromethane
1,1-dichloroetheme
1,2-dichloroethane
1,1-di chloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropame
1,3-dichloropropane
2,2-dichloropropame
1,l-dichloropropene
cis-l,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
^^cachl orobutadi ene
^Hspropylbenzene
"^^i sopropyl toluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethame
1,1,2,2-tetrachloroethame
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentemone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
u
u u
u u u
u u
u u u
u u
u
u u
u u u u u u u 4. IB J
u u u u u u u
u u
17B
u
u u u
u u
u
u u
u
u u
u 771708
347936
85104
uff/Kg
u<[/Kg
U(r/Kg
un/Kg
u<(/Kg
u<r/Kg
u<r/Kg
u(r/Kg
u(r/Kg
u(f/Kg
u<[/Kg
u<r/Kg
U([/Kg
u<r/Kg
u<r/Kg
u<[/Kg
u<r/Kg
u<r/Kg
u<r/Kg
u<r/Kg
u<r/Kg
U(r/Kg
u<r/Kg
u<r/Kg
u<r/Kg
u<r/Kg
u(f/Kg
u<r/Kg
u<f/Kg
u<f/Kg
u<f/Kg
u<[/Kg
u< r/Kg
u< r/Kg
u(F/Kg
u< r/Kg
u<r/Kg
uir/Kg
u([/Kg
u<r/Kg
u([/Kg
u<[/Kg
u<r/Kg
u<r/Kg
U(r/Kg
u<r/Kg
u<r/Kg
u<r/Kg
u((/Kg
U(r/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Page tt: 25
October 18, 1995 11:12 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #83, 2 FT. M-136 LabID: 9509035-llA CoUected: 09/18/95 10:59:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Surrogate
dibromofluoromethame
1,2-dichloroethame-d4
toluene-d8
bromofluorobenzene
For Volatile
%Recovery
81.7
81.2
125
120'
SW-846,8260A
Organics 8260S
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Sample ID: GD #83, 5 FT. M-136 LabID: 9509035-12A CoUected: 09/18/95 11:11:00
TEST
HMZ
Nltroglycerlne
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercuzy
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodichloromethane
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
.4 - chlorotoluene
RESULT
u
u
10/05/95
1.26
21.9
u
U
U
u u u u u u u
u u u u u u u u u
TJNITS
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0
0
0
.500
.500
0.1
0.3
1.6
0.2
.014
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/22/95
09/22/95
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/10/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SOP 420
SOP 420
SW-846, 3050 ^^
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4 ^^
Page tf: 26
)ctober 18, 1995 11:12
miple ID: GD #83, 5 FT. M-136
CERTIFICAIE OF ANAI.YSIS
RESULTS BY SAMPLE
LabliD: 9509035-12A CoUected: 09/18/95 11:11:00
SST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
3C^P>>
• is^prc
ilatlle Organics
-bromochloromethane
2 -dibromo-3 -chloropropan
2-dibromoetheme
.bromometheme
. chlorodi fluoromethane
1-dichloroethame
2-dichloroethane
1-dichloroethene
-s-1,2 -dichloroethene
rams -1,2-dichloroethene
2-dichloropropane
3-dichloropropame
.2-dichloropropeme
,1-dichloropropene
Ls-1,3-dichloropropene
rans-l,3-dichloropropene
,2-dichlorobenzene
,3-dichlorobenzene
,4-dichlorobenzene
thylbenzene
Lorobutadiene
|>ylbenzene
Tropyltoluene
athylene chloride
aphthalene
-propylbenzene
tyrene
,1,1,2-tetrachloroethame
,1,2,2-tetrachloroethane
etrachloroethene
loluene
.,2,3-trichlorobenzene
.,2,4-trichlorobenzene
.,1,1-trichloroetheme
-,1,2-trichloroethane
;richloroethene
;ri chlorofluorome thane
,2,3-trichloropropane
,2,4-trimethylbenzene
,3,5-trimethylbenzene
inyl chloride
-xylene
,p-xylene
cetone
-butanone
-methyl-2-pentemone
-hexanone
luorobenzene
hlorobenzene-d5
,4 -dichlorobenzene-d4
u
u u u u u u u u u u u
u u u
u u u u u u u u u u
u
u u u u u u u 12B
u u u O
u u u u u 3. 7 J
u u u 911165
416715
119094
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
-09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
09/27/
95
95
95
95
95
95
95
95
95
95
95
95
95
95
95
95
95
95
95
95
95
95
95
95
95
95
95
95
95
95
515
95
515
£»5
95
95
95
95
95
95
95
95
95
95
95
95
95
95
95
95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR:
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
•6
-5
-6
-4
-4
-6
71-55-
79-00-
79-01-
75-69-
96-18-
95-63-
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Page #: 27
October 18, 1995 11:12 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #83, 5 FT. M-136 LabID: 9509035-12A CoUected: 09/18/95 11:11:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Surrogate
dibromofluoromethane
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
For Voiatilo
%Recovery
79.5
81.0
124
110
SW-846,8260A
Organics 8260S
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Sample ID: GD #94, 2 FT. M-136 LabID: 9509035-13A CoUected: 09/18/95 11:29:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMZ
Nltroglycerlne
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodi chloromethane
bromofonn
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
.4 - chlorotoluene
u
u
10/05/95
0.56
20.9
U
U
U
U
U
. u
U
U
U
U
U
U
U
U
U
U
U
U
U
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.500
0.500
0.1
0.3
1.6
0.2
0.011
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/22/95
09/22/95
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/10/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
Page tf: 28
October 18, 1995 11:12
#
ample ID: GD #94, 2 FT. M-136
CERTIFIC AIE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9509035-13A CoUected: 09/18/95 11:29:00
EST RESXTLT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
3latlle Organics
ibromochlorometheme
,2 -dibromo-3-chloropropan
,2-dibromoethane
I ibromometheme
ichlorodifluorometheme
,1-dichloroetheme
,2-dichloroethane
I,1-dichloroethene
is-1,2-dichloroethene
rems-1,2-dichloroethene
,2-dichloropropane
I,3-dichloropropame
,2 -dichloropropeme
,l-dichloropropene
is-1,3 -dichloropropene
rans-1,3-dichloropropene
, 2-dichlorobenzene
, 3-dichlorobenzene
,4-dichlorobenzene
thylbenzene
exachlorobutadiene
son^Kylbenzene
- illBbpyltoluene
ethylene chloride
aphthalene
-propylbenzene
tyrene
,1,1,2-tetrachloroethame
,1,2,2-tetrachloroethane
e t rachloroethene
oluene
,2,3-trichlorobenzene
,2,4-trichlorobenzene
,1,1-trichloroetheme
,1,2-trichloroetheme
richloroethene
richlorofluorometheme
,2,3-trichloropropane
,2,4-trimethylbenzene
,3,5-trimethylbenzene
inyl chloride
-xylene
,p-xylene
cetone
-butanone
-methyl- 2-pentemone
-hexanone
luorobenzene
nicrobenzene-d5
,4 -dichlorobenzene-d4
u
u u
u u u u u u u u u u u u O
u u u u u u u u u
u u
u u u u u u 14B
u u u u u u u u u u u u u 818977
385383
108276
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
D9/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
09/27/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Page tt: 29
October 18, 1995 11:12 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
sample ID: GD #94, 2 FT. M-136 LabID: 9509035-13A CoUected: 09/18/95 11:29:00
CEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
'olatile Organics SW-846,8260A
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate %Recovery
dibromofluoromethane 78.5
1,2-dichloroetheme-d4 77.5
toluene-d8 125
bromofluorobenzene 113
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Iample ID: GD #94, 5 FT. M-136 LabID: 9509035-14A CoUected: 09/18/95 10:38:00
•EST
MX
ltroglycerlne
eid Digestion
admium
bromlum
sad
ilver
ercury
olatile Organics
enzene
rc^mobenzene
rcamochlorome thane
romodi chloromethame
romoform
romome thame
•butylbenzene
JC-butylbenzene
jrt-butylbenzene
irbon tetrachloride
ilorobenzene
iloroe thame
iloroform
ll orome theme
chlorotoluene
chlorotoluene
RESULT
u
u
10/05/95
0.18
22.3
U
U
U
U
U
U
U
u u u
u u
u u
u u
u u u
UNITS
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0
0
0
.500
.500
0.1
0.3
1.6
0.2
.015
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/22/95
09/22/95
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/10/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SOP 420
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050 (
6010
6010
6010
6010
7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
Page tt: 30
October 18, 1995 11:12 CERTIFICATE OF AI"«^^U.YSIS
RESULTS BY SAMPLE
Sample ID: GD #94, 5 FT. M-136 l^blD: 9509035-14A CoUected: 09/18/95 10:38:00
TEST RESULT UNITS DETECTION J^NALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
dibromochloromethane
1,2-dibromo-3-chloropropan
1,2-dibromoethane
dibromomethane
di chlorodi fluoromethame
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2 -dichloropropane
1,3-dichloropropane
2,2-dichloropropeme
1,l-dichloropropene
cis-1,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
J|ucachlorobutadiene
^^^propy Ibenz ene
^^isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane '
1,1,2-trichloroethane
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene- d5
1,4-dichlorobenzene-d4
u
u u
u u
u u u
u u u u u u u u u u u
u u u u 4.9BJ
U
U
U
u u u u
u
u 2 IB
U
u u
u
o u
u u u u u u u 682429
326545
100088
uc /Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc /Kg
uc /Kg
uc /Kg
uc /Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug'Kg
ug'Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Page#: 31
October 18, 1995 11:12 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #94, 5 FT. M-136 Lab ID: 9509035-14A CoUected: 09/18/95 10:38:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Surrogate
dibromofluorometheme
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
Por Volatile
%Recovery
80.1
78.3
121
104
SW-846,8260A
Organics 8260S
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Sample ID: GD #101, 2 FT. M-136 Lab ID: 9509035-15A CoUected: 09/18/95 12:02:00
TEST
HMZ
Ni troglycerlne
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chlorcjme thane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
RESULT
u
u
10/05/95
U
23.9
U
U
0.02
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
U
UNITS
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.500
0.500
0.1
0.3
1.5
0.2
0.013
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/22/95
09/22/95
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/10/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SOP 420
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050 ^P
6010
6010
6010
6010
7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4 ^
Page ft: 32
October 18, 1995 11:12
ample ID: GD #101, 2 FT. M-136
CERTIFIC lAirE OF ANALYSIS
RESU LTS BY SAMPLE
LabID: 9509035-15A CoUected: 09/18/95 12:02:00
EST RESULT UNITS DIITECTION ANAI,YZED BY
LIMIT
METHOD/CAS#
olatile Organics
ibromochloromethame
,2-dibromo-3-chloropropem
,2 -dibromoethane
ibromomethane
i ch1orodi fluoromethane
,1-di chloroe theme
,2 -di chloroe thane
,1-dichloroethene
is-1,2 -dichloroethene
rans-l,2-dichloroethene
,2 -dichloropropeme
,3-dichloropropane
,2-dichloropropeme
,l-dichloropropene
is-1,3-dichloropropene
rems-1,3-dichloropropene
,2-dichlorobenzene
,3-dichlorobenzene
,4-dichlorobenzene
thylbenzene
axachlorobutadiene
30|^|y Ibenzene
- il^Hopyltoluene
atn^rene chloride
aphthalene
-propylbenzene
zyrene
,1,1,2-tetrachloroetheme
,1,2,2-tetrachloroethane
etrachloroethene
oluene
,2,3-trichlorobenzene
,2,4-trichlorobenzene
,1,1-trichloroethane
,1,2-trichloroetheme
richloroethene
richlorofluorometheme
,2,3-trichloropropane
. 2,4-trimethylbenzene
.3,5 -trimethylbenzene
Lnyl chloride
-xylene
p-xylene
:etone
•butemone
•methyl-2-pentanone
hexanone
.uorobenzene
ilorobenzene-d5
4-di chlorobenzene-d4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u 3.8BJ
U
U
U
U
U
U
U
U
U
IOB
U
u u u
u u '
u u u u u u
u 796245
372843
98443
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/&5
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Page; tt: 33
October 18, 1995 11:12 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #ioi, 2 FT. M-136 LabID: 9509035-15A CoUected: 09/18/95 12:02:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Surrogate/Recovery
Surrogate
dibromofluoromethane
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
Data For Volatile
%Recovery
81.5
79.8
123
114
SW-846,8260A
Organics 826OS
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Sample ID: GD #101, 5 FT. M-136 LabID: 9509035-16A CoUected; 09/18/95 12:14:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMZ
Nltroglycerlne
Acid Digestion
Cadmium
Chromium
Lead
Silver
Marcury
Volatile Organics
benzene
bromobenzene
bromochloromethame
bromodi chlorometheme
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
u
u
10/05/95
1.14
21.8
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.500
0.500
0.1
0.3
1.6
0.2
0.012
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/22/95
09/22/95
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/10/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
Page tf: 34
Dctober 18, 1995 11:12
ample ID: GD #101, 5 FT. M-136
CERTIFIC A11E OF ANAI.YSIS
RESULTS BY SAMPLE
Lab ED: 9509035-16A CoUected: 09/18/95 12:14:00
EST
olatile Organics
ibromochloromethame
,2 -dibromo-3 -chloropropan
,2-dibromoethane
ibromomethane
L chlorodi fluorometheme
,1-dichloroethane
,2-dichloroethame
,1-dichloroethene
is-1,2 -dichloroethene
rans-1,2-dichloroethene
,2-dichloropropeme
,3-dichloropropeme
,2-dichloropropane
,l-dichloropropene
is -1,3-dichloropropene
rans-1,3-dichloropropene
,2-dichlorobenzene
,3-dichlorobenzene
,4-dichlorobenzene
thylbenzene
axachlorobutadiene
30Q^^/lbenzene
- ii^^Popyltoluene
athylene chloride
aphthalene
-propylbenzene
cyrene
,1,1,2-tetrachloroethane
,1,2,2-tetrachloroethane
atrachloroethene
oluene
,2,3-trichlorobenzene
,2,4-trichlorobenzene
,1,1-trichloroetheme
,1,2-trichloroethane
richloroethene
richlorofluoromethane
,2,3-trichloropropame
,2,4-trimethylbenzene
,3,5-trimethylbenzene
Lnyl chloride
-xylene
,p-xylene
retone
-butanone
-methyl-2-pentanone
-hexanone
Luorobenzene
ilorobenzene-d5
4 -dichlorobenzene-d4
RESULT
u u
u u
u
u u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
4.9BJ
U
U
U
U
U
u u
u
u 123
U
U
U
U
U
u
u
u
u
u
u
u
u 498111
269871
88590
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/28/95
09/28/95
09/28/S5
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/915
09/28/915
09/28/95
09/28/915
09/28/95
09/28/95
09/28/95
09/28/9r>
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/9Ei
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
. 103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Page tt: 35
October 18, 1995 11:12 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #101, 5 FT. M-136 LabID: 9509035-16A CoUected: 09/18/95 12:14:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics SW-846,8260A
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate %Recovery
dibromof1uoromethane 79.2
1,2-dichloroethane-d4 82.2
toluene-d8 114
bromofluorobenzene 104
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Sample ID: GD #92, 2 FT. M-136 LabID: 9509035-17A CoUected: 09/18/95 13:30:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMZ
Nltroglycerlne
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethame
bromodi chloromethane
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
.4 - chlorotoluene
u
u
10/05/95
U
21.6
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u u u u u
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.500
0.500
0.1
0.3
1.6
0.2
0.013
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/22/95
09/22/95
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/10/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
0.9/28/95
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
Page tt: 36
October 18, 1995 11:12
Sj^Pe ID: GD #92, 2 FT. M-136
CERTIF [CATE OF ANAILYSIS
REJ ULTS BY SAMPLE
LaMD: 9509035-17A CoUected: 09/18/95 13:30:00
TEST
Volatile Organics
dibromochlorometheme
1,2-dibromo-3 -chloropropan
1,2-dibromoetheme
dibromomethane
dichlorodifluorometheme
1,1-dichloroethane
1,2-dichloroetheme
1,1-dichloroethene
=is-1,2-dichloroethene
trans -1,2-dichloroethene
L,2-dichloropropane
L,3-dichloropropeme
1,2-dichloropropeme
.,l-dichloropropene
:is-1,3-dichloropropene
:rans-1,3-dichloropropene
.,2-dichlorobenzene
.,3-dichlorobenzene
.,4-dichlorobenzene
^thylbenzene
exachlorobutadi ene
sopropylbenzene
-isopropyltoluene
etJ^Kne chloride
ap^HLlene
-propylbenzene
tyrene
,1,1,2-tetrachloroethane
,1,2,2-tetrachloroetheme
atrachloroethene
oluene
,2,3-trichlorobenzene
,2,4-trichlorobenzene
,1,1-trichloroethane
,1,2-trichloroetheme
-ichloroethene
.'ichlorof luorome theme
2,3-trichloropropane
2,4-trimethylbenzene
3,5-trimethylbenzene
nyl chloride
xylene
p-xylene
etone
butanone
•nethyl - 2 -pentanone
nexanone
aorobenzene
lorobenzene-d5
t-dichlorobenzene-d4
RESULT
U
U
u u
u u u u u u u u u u u u u u u u u u
u 4.3BJ
U
U
U
u u
u u u
u 8.6BJ
u
u
u
u
u u u u u 3.9J
U
U
U
617796
304126
90463
UNITS
ug/Rj
ug/K,j
ug/K(.r
ug/K<r
ug/Kc f
ug/Kc •
ug/Kc
ug/Kc
ug/Kc
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
, 09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/915
09/28/9!;
09/28/95
09/28/9;-)
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Piige^': 37
October 18, 1995 11:12 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #92, 2 FT. M-136 LabID: 9509035-17A CoUected: 09/18/95 13:30:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Surrogate
dibromofluorometheme
1,2-dichloroethame-d4
toluene-d8
bromofluorobenzene
For Volatile
%Recovery
78.1
80.6
117
110
SW-846,8260A
Organics 8260S
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
Sample ID: GD #92, 5 FT. M-136 LabID: 9509035-18A CoUected: 09/18/95 13:40:00
TEST
HMZ
Nltroglycerlne
Add Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethame
bromodi chloromethane
bromoform
bromome theme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
ch1orometheme
2-chlorotoluene
4-chlorotoluene
RESULT
u
u
10/05/95
0.19
24.7
U
U
U
U
U
U
' U
U
U
U
U
U
U
U
U
U
U
U
U
UNITS
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0
0
0
.500
.500
0.1
0.3
1.7
0.2
.014
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/22/95
09/22/95
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/10/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SOP 420
SOP 420
SW-846, 3050 ^B
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4 ^^
Page tt: 38
October 18, 1995 11:12
Sample ID: GD #92, 5 FT. M-136
CERTIFICATE OF AN^U^YSIS
REStT^TS BY SAMPLE
lab ID: 9509035-18A CoUected: 09/18/95 13:40:00
TEST
Volatile Organics
dibromochloromethane
1,2-dibromo-3-chloropropem
1,2-dibromoethane
dibromomethane
di chlorodi fluorometheme
1,1-dichloroe thane
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropeme
1,3 -dichloropropane
2,2-dichloropropeme
1,l-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2 -di chlorobenzene
1,3 -di chlorobenz ene
1,4-dichlorobenzene
ethylbenzene
lexachlorobutadiene
^^Bpropylbenzene
^Bl sopropy 1 toluene
. methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl- 2-pentanone
2 -hexanone
fluorobenzene
chlorobenzene-d5
1,4 -di chlorobenz ene-d4
RESULT
U
U
u u u u u u u u u
u u u
u u u
u u u
u u
u 4.3BJ
U
U
U
u u
u u u u 15B
u
u u U
U
U
u u u u u u u 772313
384416
105837
UNETS
uc
uc
uc
uc
uc
uc
uc
/Kg
/Kg
/Kg
/Kg
/Kg
/Kg
/Kg
uc /Kg
uc /Kg
uc/Kg
uc/Kg
uc /Kg
uc /Kg
uc /Kg
uc /Kg
uc/Kg
uc /Kg
uc/Kg
uc /Kg
uc /Kg
uc/Kg
uc/Kg
uc /Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug /Kg
DETECTION
LIMIT
10
10
10
10
10
10
lfl
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 •
10
10
10
10
10
10
10
10
10
10
10
10
10
J^NALYZED
09,/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Page tf: 39
October 18, 1995 11:12 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #92, 5 FT. M-136 LabID: 9509035-18A CoUected: 09/18/95 13:40:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Surrogate/Recovery
Surrogate
dibromofluoromethane
1,2- di chloroetheme-d4
toluene-d8
bromof1uorobenzene
Data For Volatile
%Recovery
83.2
82.7
120
115
SW-846,8260A
Organics 8260S
Recovery Limits
75.0 TO 125
75.0 TO 125
75.0 TO 125
75.0 TO 125
iample ID: GD #92, 5 FT. M-136 DUP. LabID: 9509035-19A CoUected: 09/18/95 13:40:00
•EST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
MX
ltroglycerlne
cld Digestion
admium
hromlum
sad
ilvar
iercury
o
u
0/05/95
U
24.6
U
u
u
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
0
0
0
.500
.500
0.1
0.3
1.6
0.2
.011
09/22/95
09/22/95
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/10/95
KMS
KMS
KWB
LVD
LVD
LVD
LVD
CRS
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
'ample ID: GD #96, 2 FT. M-136 LabID: 9509035-20A CoUected: 09/18/95 13:57:00
SST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
. troglycerlne
lid Digestion
dmium
u
u
10/05/95
1.14
MG/KG
MG/KG
DATE
ug/g
0.500
0.500
0.1
09/22/95
09/22/95
10/05/95
10/11/95
KMS
KMS
KWB
LVD
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
Page tt: 40
October 18, 1995 11:12 m
Sample ID: GD #96, 2 FT. M-136
CERTIFICATE OF ANiO^YSIS
RESULTS BY SAMPLE
lab ID: 9509035-20A CoUected: 09/18/95 13:57:00
TEST
Chromium
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodi chlorome thane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
^^|orof orm
VHorome thane
2~- chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3-chloropropam
1,2-dibromoetheme
dibromometheme
dichlorodifluoromethane
1,1-dichloroetheme
1,2-dichloroetheme
1,1-dichloroethene
cis-l, 2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis-1,3 -dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4-isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
^^rene
RESULT
22.1
u
U
0.01
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u u
u u
u
u u
u u
u
u
u
u
u
u
u
u
u
u
u
u 5.6BJ
u
u
u
UNITS
u'.j/g
u'.j/g
u'.r/g
u'.r/g
uc /Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.3
1.6
0.2
0.0098
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
J^ALYZED
10/11/95
10/11/95
10/11/95
10/10/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
BY
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
Page tt: 41
October 18, 1995 11:12 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #96, 2 FT. M-136 LabID: 9509035-20A CoUected: 09/18/95 13:57:00
TEST
Volatile Organics
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethame
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butcmone
4-methyl-2-pentamone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
U
U
U
U
U
U
15B
U
U
U
u u
u u o
u
u u
u
u 1068486
600667
195105
Surrogat
Surrogate
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
I'o 10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
e/Recovery Data For Volatile Organics 8260S
dibromofluoromethane
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
%Recovery
92.9
96.7
107
107
METHOD/CAS#
SW-846,8260A
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2 ^^
INTSTD3 ^V
Recovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Sample ID: GD #96, 5 FT. M-136 LabID: 9509035-21A CoUected: 09/18/95 14:22:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMX
Nltroglycerlne
Acid Digestion
Cadmium
Chromium
u
u
10/05/95
u
19.9
MG/KG
MG/KG
DATE
ug/g
ug/g
0
0
.500
.500
0.1
0.3
09/22/95
09/22/95
10/05/95
10/11/95
10/11/95
KMS
KMS
KWB
LVD
LVD
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
Page tf: Al
October 18, 1995 11:12
•
Sample ID: GD #96, 5 FT. M-136
CERT] FKGATE OF ANALYSIS
I ESULTS BY SAMPLE
LabID: 9509035-21A CoUected: 09/18/95 14:22:00
TEST
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodichloromethane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorometheme
^^Kchlorotoluene
^Bchlorotoluene
^^bromochl orome theme
1,2-dibromo-3-chloropropem
1,2-dibromoetheme
dibromometheme
dichlorodifluoromethame
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropeme
2,2-dichloropropame
1,l-dichloropropene
cis-1,3-dichloropropene
trans -1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
RESULT
u
u
0.02
u U
U
U
U
U
u u u u u u u u u u u u
u u u u u u u u u u u
u u u
' u u u u
u u
u 8.9BJ
u
u u u u
TO ITS
^g/g
vg/g
vg/g
uij/Kg
U|j/Kg
u;j/Kg
uj/Kg
u:j/Kg
U'.r/Kg
u'.r/Kg
U'.r/Kg
uir/Kg
uir/Kg
Ul r/Kg
uir/Kg
u< r/Kg
u< r/Kg
u< r/Kg
Ul r/Kg
u<r/Kg
u< r/Kg
u(f/Kg
uu/Kg
uc i/Kg
uc[/Kg
uc:/Kg
uc ;/Kg
uc/Kg
uc/Kg
uc /Kg
uc/Kg
UC /Kg
uc /Kg
uc /Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc /Kg
uc /Kg
uc/Kg
uc /Kg
uc /Kg
uc /Kg
uc/Kg
uc/Kg
uc/Kg
ug/Kg
DETECTION
LIMIT
1.6
0.2
0.013
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/11/95
.10/11/95
10/10/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09,/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
BY
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
# Page ff: 43
October 18, 1995 11:12 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #96, 5 FT. M-136 Lab ID: 9509035-21A CoUected: 09/18/95 14:22:00
TEST
Volatile Organics
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropame
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
U
u
u u
18B
U
U
U
U
U
U
u
u u
3.9 J
U
U
U
452001
287049
109402
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorometheme
1 ,2 -dichloroetheme-d4
toluene-d8
bromofluorobenzene
%Racovery
82.0
88.8
107
98.5
METHOD/CAS#
SW-846,8260A
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
•
Racovery Limits
75.0
75.0
75.0
75.0
TO 125
TO 125
TO 125
TO 125
Page tt: AA
Dati I Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compoimds or when the mass spectral data indicated the presence of a
compound that meets the idt ntification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. l.U with a detection limit of 5.0)
B This flag is used when an analj te is found in the blank as weU as the sample.
E Estimated value. Result was oi itside of the caUbration irange but within the linear
range of the instrument.
BDL Indicates an analyte which was belcw the detection Umits for the test.
NA Not appUcable.
NT Indicates that an analyte was nc t tested for.
Q Surrogate/spike recovery was o utside of the specified Umits. If surrogate recoveries are out
of Umits, any values reported ane for indication only.
•
ENVIRONMENTAL LAB WORK RJEQUEST
THIOKOL ENVIRONMENTAL LABORATORY LWR No. E11050
AP UJal^ y F390
COST CENTKR
du3^o
WORK ORDER
/^7Z40
DATE ^,—
%19-^C
ORGANIZATION f/li/'ro/mt/i^ MA LSTOF'
7^01 €
REPORT RESULTS TO:
HELEN WARD, MS 301
SAM] 'LE INFORMATION
SAMPLE
TT^S.
DATE
9'iff'9i
TYPE
V
LOCATION
/i/4=iO
TIME
/Tt7
TEST
iz^c- eziaO
REMARKS
±l^'d_ II ^/^ Sf/Jtf IZO/I '^Z70
H^, <^m('47). Hm/^. , Al<i'> ' " -
/yi' //
4 "RticXj/irtiuni "LdSZiF. ll iSTL Itjl, (g-llgf -M-((L-)
::2 £r_ %ie^' / u r^d_ izoc- e2.c^o
/I fvf'fy' y 9U ^r)f' -\Zff4' 6-2-70
It
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II t/T^F ^ // 9Z7 ^rri' f/oA
fl ±mF. y u
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JSM. :^^j£dL
'^^ckf^cir^d^' n i^o_ \ZoA
ll 1/ F S^o 'yfrrti IZQA
fl II / t3^0 ^di ^^ 3
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/ /T' II
li-
li.
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II If
11 ^
y
1/
y CpAlNOl^^STODY ^^^' "^ Z>
RELINQUISHED BY
.~Q p//^F'^
DATE
?'/?-?r
TME
/FoO
RECEIVED BY
.AFcFAMc/i^-i jh^
DATE
"/-/f' 9F
TIME
/F^^
FOR LAI lOR^iTORY USE ONLY
«
DATE COMPLETED DATE REPORTED
ENVIRONMENTAL LAB WORK REQUEST fc Jf
THIOKOL ENVIRONMENTAL LABORATORY
raoMi
OBGAMUIION
KsmaioN
MAO. nor
B//OSO fQf^ Z^
BOOBT aaWLTl TOl
HELEN WARD, MS 301
F
7
SAMPLE
6-/^\
3- SnJ/iK\} HtoC
3.
«.
3.
i.
7.
i.
9.
la
IL
a
DATC
9-/Ur
9d<f^i
tm
a
i/
y
c
SAMPLE INFORMATION
LOCATION
M'Sse
M'33'b
17ME
lOSf
fin
TEST SEMABKS
:5i>, As, Cr, Ph ^^F^lc , pit
f f
Jl m
CHAIN OF CUSTODY
KEUNQUISHESBY DATE
=^=^=9^=:^^
TIME SECETVESBY DATE TIME
FOR LABORATORY USE ONLY
DATCCOMnens OAniiEroRnD aCNATUU
November 6, 1995 CERTIf ICATE OF ANALYSIS
RESUI,TS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward M/S 301
Thiokol Corp, Ut 84322
A.F. WALKER
EXT 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Oty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. Jofin Terry
Tele: 801-863-2384
Work Orderly 9509039 Sample at id Test Code Identifiicattion
LabID:
OIA
Sample ID:
BACKGROUND SURFACE M-136
Test Codes and Names
LabID:
02A
LabID:
03A
Sample ID:
BACKGROUND SURFACE M-136
Sample ID:
BACKGROUND 2 FT. M-136
LabID:
04A
LabID:
~O5A
Sample ID: na !Ki BACKGROUND 2 FT. M-136
Sample ID:
BACKGROUND 5 FT. M-136
PH
TI GF
HMX
NO
3050
SB AE2
BA AI2
BE M2
CD A12
CR AI2
PB AE2
NI AEi
AO AJ2
TL Ml
ZN A12
AS GFJ
HG 0 7
SE"GF;
CN Al(2
soflc 8260S
pH
Tiunium
HMX
Nitroglycerine
/Lcid Digestion
jiuitimony
Itarium
Etetyllium
Cradmium
Chromium
l«ad
Mickel
Silver
Thallium
2;inc
.^iTsenie
Mercury
Selenium
Ibul Cyanide
Sulfate
\'olatile Organica
Test: Codes and Names
8270S Semi-Volatile Organics
Tesl: Codes and Names
PH
TI GFI
HSiX
NO
3050
SB AE:
BA AE2 BE AE>
CD AI2
CR AE2
PB AEI
NI AE
AO AI2
TL AEI
ZN A£2
AS GE; HG C\2
SE GF
CN A12
S04IC2
8260S
pH
TiUnium
FMX
Mitroglycerine
i^.cid Digestiion
Ajitimony
Barium Beiyllium
Cadmium
Chromium
Lead
Nickel
Silver
Thallium
Zinc
Arsenic
Mercury
Sslenium
Total Cyanide
Siilfate
Volatile Organics
Test Codes and Names
8270S Sismi-Volatile Organics
Test Codes and Names
PH
TI_GF1
HMX
NG
pH
TiUnium
HMX
Nitroglycerine
Method
EPA 150.1
EPA 283.2
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 9012
SW-846, 9056
SW-846,8260A
Method
SW-846, 8270
Method
EPA 150.1
EPA 283.2
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-84«, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 9012
SW-846, 9056
SW-846,8260A Method
SW-846, 8270
Method
EPA 150.1
EPA 283.2
SOP 420
SOP 420
Page tt:l of p-- <-/
Work Order # 9509039 Sample and Test Code Identification
LabID:
""O3A
Sample ID:
2Kl
Test Codes and Names
BACKGROUND 5 FT. M-136
LabID:
06A
LabID:
07A
Sample ID:
BACKGROUND 5 FT. M-136
Sample ID:
BACKGROUND 10 FT. M-136
Lab ID:
08A
Sample ID:
BACKGROUND 15 FT. M-136
LabID:
09A
Sample ID:
M-338 5 FT. SWMU #608
3050
SB AE2
BA AE2
BE AE2
CD AE2
CR AE2
PB AE2
NI AE2
AO AE2
TL AE2
ZN AE2
AS GF2
HG CV2
SE OF2
CN"AU2
S04IC2
8260S
Acid Digestion
Antimony
Barium
Beiyllium
Cadmium
Chromium
Lead
Nickel
Silver
Thallium
Zinc
Arsenic
Mercuiy
Selenium
Total Cyanide
Sulfate
Volatile Organics
Test Codes and Names
8270S Semi-Volatile Organics
Test Codes and Names
PH pH
TI_GF1 Titanium
HMX HMX
NO Nitroglycerine
3050 Acid Digestion
SB_AE2 Antimony
BA_AE2 Barium
BE_A£2 Beryllium
CD_AE2 Cadmium
CR_AE2 Chromium
PB_AE2 Lead
NI_AE2 Nickel
AG_AE2 SUver
TL_AE2 Thallium
ZN_AE2 Zinc
AS_GF2 Arsenic
HG_CV2 Mercury
SE OF2 Selenium
82T0S Semi-Volatile Organics
CN AU2 Total Cyanide
S04iC2 Sulfate
8260S Volatile Organics
Test Codes and Names
PH
TI QFl
HMX
NO
3050
SB AE2
BA AE2
BE AE2
CD AE2
CR AE2
PB AE2
NI AE2
AG AE2
TL AE2
ZN AE2
AS GF2
HG CV2
SE'GF2
8270S
CN AU2
S041C2
8260S
pH
Titanium
HMX
Nitroglycerine
Acid Digestion
Antimony
Barium
Beryllium
Cadmium
Chromium
Lead
Nickel
Silver
Thallium
Zinc
Arsenic
Mercury
Selenium
Semi-Volatile Organics
Toul Cyanide
Sulfate
Volatile Organics
Test Codes and Names
PH
3050
SB_AE2
CR AE2
pH
Acid Digestion
Antimony
Chromium
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 9012
SW-846, 9056
SW-846,8260A Method
SW-846, 8270
Method
EPA 150.1
EPA 283.2
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8270
SW-846, 9012
SW-846, 9056
SW-846,8260A Method
EPA 150.1
EPA 283.2
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8270
SW-846, 9012
SW-846, 9056
SW-846,8260A Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
Page #:2
Work Orders 9509039 Sample a ad Test Code Identifictttion
J.jib ID:
|09A
W
LabID:
lOA
Sample ID:
M-338, 5 FT. SWMU #608
Sample ID:
M-338, 10 FT. SWMU #608
Test Codes and Names
PB A12 l>ad
AS G12 .Vrsenic
SO^IC I Sulfate
Test Codes and Names
PH pH
3050 Acid Digestion
SB_AI 2 /Vntimony
CR A)2 (iromium
PB AI 2 l^d
AS G12 jVrsenic
SO?IC 1 Slulfate
Comments
Method
SW-846, 6010
SW-846, 7060
SW-846, 9056
Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 9056
Workorder: NOTE FOR METHOE < 8270: The mtemal standard solution used for
these samples appeared to be sUghtly degraded, this resulted
in low surrogate recov( ries
^^3l^i'^i^4^*V^
Certified By
Page tt:3
This is to certify tfiat tlie following samples were analyzed using good laboratory practices
to sfiow tfie following results.
Sample ID: BACKGROUND SURFACE M-136 Lab ID: 9509039-OlA CoUected: 09/18/95 15:27:00
TEST
pH
Titanitun
HMZ
Ni troglycerlne
Acid Digestion
Antimony
Barium
Beryllium
Cadmium
Chromium
Lead
Nickel
Silver
Thallium
Zinc
Arsenic
Mercxiry
Selenium
Total Cyanide
Sulfate
Volatile Organics
benzene
bromobenzene
bromochloroinetheine
bromodi chlorome theuie
bromoform
bromomethane
n-butylbenzene
RESDLT
7.59
459.5
U
U
10/05/95
U
131
0.75
U
15.8
U
11.5
O
U
48.0
8.4
0.02
U
U
11
U
U
U
D
U
U
U
DNITS
pH Unit
ug/L
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
5.2
0.500
o.5ao
3.2
0.06
0.1
0.1
0.3
1.6
0.62
0.2
3.2
0.2
1.9
0.012
1.5
0.15
1
10
10
10
10
10
10
10
ANALYZED
09/22/95
10/24/95
09/21/95
09/21/95
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/17/95
10/10/95
10/16/95
09/27/95
09/29/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
BY
AA
CRS
KMS
KMS
KWB
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
KEN
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
EPA 150.1
EPA 283.2
SOP 420
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
3050
6010
6010
6010
6010
6010
6010 ^A
6010
6010
6010
6010
7060
7471
7740
9012
9056
3260A
_
Page tt: A
November 6, 1995 08:45 CERTI FICATE OF ANiO^YSIS
RESULTS BY SAMPLE
Sample ID: BACKGROUND SURFACE M-136 lab ID: 9509039-OlA CoUected: 09/18/95 15:27:00
TEST
Volatile Organics
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropan
1,2-dibromoetheme
dibromomethane
dichlorodifluoromethane
1,1-dichloroetheme
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-l,2-dichloroethene
1,2-dichloropropane
^L3 -dichloropropane
^^H -dichloropropeme
^^ - dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
^^D-xylene
RESULT
u
u
u u u
u u u u u
u u u
u u u u u u u u u u u
u u u u u
u u
u . u u u
u u u
u D
u u 22B
u u u u
u u u u u
UNITS
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc /Kg
uc/Kg
uc /Kg
uc /Kg
uc /Kg
uc /Kg
uc /Kg
uc /Kg
uc /Kg
uc /Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc /Kg
uc/Kg
uc /Kg
uc /Kg
uc/Kg
uc/Kg
uo/Kg
uc/Kg
uc/Kg
uo/Kg
uc/Kg
uo/Kg
U9/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
J\NALYZED
09/28/95
.09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
Page tf: 5
November 6, 1995 08:45 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: BACKGROUND SURFACE M-136 LabID: 9509039-OlA CoUected: 09/18/95 15:27:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
acetone
2-butanone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
u
u u
u 492664
214542
70259
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
dibromofluorometheme
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
10
10
10
10
,
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
For Volatila Organics 8260S
%Recovery
75.9
75.5
125
96.7
SW-846,8260A
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.
53
85.
80.
4
3
6
6
TO 112
TO 121
TO 143
TO 130
Sample ID: BACKGROUND SURFACE M-136 Lab ID: 9509039-02A CoUected: 09/19/95 09:12:00
TEST
Semi-Volatile Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroetheme
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)metheme
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4-chloroemiline
hexachlorobutadiene
4 -rhioro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
RESULT
U
U
u u D
U
U
U
U
U
U
u u
u u u u u u u u u
u
u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS# fl^
SW-846, 8270
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3.
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4 ^^
Page tf: 6
November 6, 1995 08:45 CERTIFICATE OF A]^.^YSIS
j RESULTS BY SAMPLE
Sample ID: BACKGROUND SURFACE M-136 )^bID: 9509039-02A CoUected: 09/19/95 09:12:00
TEST
Seml-Volatlle Organics
2 -chloronaphthalene
2-nitroaniline
dimethylphthalate
acenaphthylene
3-nitroaniline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofurem
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroemiline
4,6-dinitro-2-methylphenol
n-nitrosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenanthrene
.^^thracene
Hv n - butylphthalate
fluoremthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3 -cd)pyrene
dibenz(a,h) emthracene
benzo (g,h, Dperylene
RESULT
u u u
u u u
u
u
u u
u
u
u
u u
u
u
u
u u
u
u 949.0
D
U
U
U
U
U
U
U
u
u u
• u
u
u
UNITS
u([/Kg
utf/Kg
ucf/Kg
ucr/Kg
uci/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc /Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc /Kg
uc /Kg
uc/Kg
uc/Kg
uc /Kg
uc /Kg
uc/Kg
uc/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery lata
Surrogate
2 -fluorophenol
phenol -d5
nitrobenzene-d5
2 -fluorobiphenyl
2,4,6-
terphe
tribromophenol
nyl-dl4
DETECTION
LIMIT
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 827OS
%R«covery
14.28
19.71
17.40
26.17
39.87
58.88
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
Page tf: 7
November 6, 1995 08:45 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: BACKGROUND 2 FT. M-136 LabID: 9509039-03A CoUected: 09/18/95 15:40:00
TEST
PH
Titanium
HMX
Ni troglycerlne
Acid Digestion
Antimony
Barixim
Beryllium
Cadmium
Chromium
Lead
Nickel
Silver
Thallium
Zinc
Arsenic
Mercury
Selenium
Total Cyani<ls
Sulfate
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chlorometheme
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
RESULT
7.80
386.0
U
U
10/05/95
7.22
135
0.61
U
13.4
U
9.47
U
U
32.7
9.8
U
U
U
15
U
U
U
D
U
U
U
U
UNITS
pH Unit
ug/L
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
5.3
0.500
0.500
3.3
0.07
0.1
0.1
0.3
1.7
0.67
0.2
3.3
0.3
2.0
0.013
1.6
0.15
1
10
10
10
10
10
10
10
10
ANALYZED
09/22/95
.10/24/95
09/21/95
09/21/95
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/17/95
10/10/95
10/16/95
09/27/95
09/29/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
BY
AA
CRS
KMS
KMS
KWB
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
KEN
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
EPA 150.1
EPA 283.2
SOP 420
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
3050
6010
6010
6010
6010
6010
6010 d^k
6010
6010
6010
6010
7060
7471
7740
9012
9056
3260A
^^^^^
Page tt: 8
November 6, 1995 08:45 CERTI FICATE OF ANiVLYSIS
RESULTS BY SAMPLE
Sample ID: BACKGROUND 2 FT. M-136 l^blD: 9509039-03A CoUected: 09/18/95 15:40:00
TEST
Volatile Organics
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3-chloropropan
1,2-dibromoetheme
dibromometheme
dichlorodifluorometheme
1,1-dichloroetheme
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropane
2,2-dichloropropane
^^ba. - dichloropropene
^HB -1,3- dichloropropene
^rans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4-isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroetheme
t e t rachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
^cstone
RESULT
U
U
u u
u
u u
u
u u
u u u u u u u u u
u
u
u u
u u u
u
u u u
u 3.7BJ
u u u u u
u
u u u 12B
U
U
u u
u
u u u
u u
UNETS
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc /Kg
uc /Kg
uc /Kg
uc /Kg
uc /Kg
uc /Kg
uc/Kg
uc/Kg
uc /Kg
uc /Kg
uc /Kg
uc/Kg
uo/Kg
uo/Kg
uc/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
I'O
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
J^ALYZED
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
Page #: 9
November 6, 1995 08:45 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: BACKGROUND 2 FT. M-136 LabID: 9509039-03A CoUected: 09/18/95 15:40:00
TEST
Volatile Organics
2 -butanone
4-methyl-2-pentanone
2 - hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene- (
RESULT
u
u
u 549782
292115
14 89892
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
ANALYZED BY
09/28/95 MMR
09/28/95 MMR
09/28/95 MMR
09/28/95 MMR
09/28/95 MMR
09/28/95 MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluoromethane
1,2 -dichloroetheme-d4
toluene-d8
bromof1uorobenzene
%Recovery
83.1
87.0
114
108
METHOD/CAS#
SW-846,82eOA
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4 TO 112
53.3 TO 121
85.6 TO 143
80.6 TO 130
Sample ID: BACKGROUND 2 FT. M-136 LabID: 9509039-04A CoUected: 09/19/95 09:21:00
TEST
Semi-Volatile Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethcme
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4 -chloroani1ine
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachloroc:yclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
RESULT
U
u
u
u
u u u
u
u
u
u
u
u
u
u
u u
u u
u
u u
u
u
. u
u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
BY
JMA
JMA
JMA
JMA
JM;V
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS # ^^
SW-846, 8270
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7 ^^
Page tt: 10
November 6, 1995 08:45
•
CERTIFICATE OF AN^SXYSIS
RESULTS BY SAMPLE
Sample ID: BACKGROUND 2 FT. M-136 lab ID: 9509039-04A CoUected: 09/19/95 09:21:00
TEST
Semi-Volatile Organics
2-nitroaniline
dimethylphthalate
acenaphthylene
3-nitroemiline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofurem
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenyl(
fluorene
4-nitroemiline
ether
4,6-dinitro-2-methylphenol
n-nitrosodiphenylamine
4 -bromophenyl-phenyle'
hexachlorobenzene
pentachlorophenol
phenanthrene
^Ithracene
.^^k- n - butylphthal ate
^Ruoranthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
ther
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoremthene
benzo(a)pyrene
indeno(1,2,3 -cd)pyrene
dibenz(a,h) emthracene
benzo(g,h, Dperylene
RESULT
91.3
U
U
U
U
U
U
U
U
U
U
U
U
u u u u
u u u u u J
u u
u
u
u u
u u u
u u
u u
u
UNCTS
uc /Kg
uc /Kg
uc /Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc /Kg
uc/Kg
uc/Kg
uc /Kg
uc /Kg
uc/Kg
uc /Kg
uc/Kg
uc /Kg
uc /Kg
uc/Kg
uc/Kg
uc/Kg
uo/Kg
uc/Kg
Surrogate/Recovery rata
Surrogate
2 -fluorophenol
phenol -d5
nitrobenzene -d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
DETECTION
LIMIT
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
JVNALYZKD
10/18/95
.10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270S
%Recovery
17.41
19.17
19.2 Q
21.63
38.21
69.52
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
Page#: 11
November 6, 1995 08:45 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: BACKGROUND 5 FT. M-136 LabID: 9509039-05A CoUected: 09/18/95 15:48:00
TEST
pH
rltanlum
ms.
iltroglycerlne
icid Digestion
mtimony
tarlum
1 erylliuffl
' admium
hromlum
ead
ickel
Liver
lalllum
lnc
:senlc
jrcury
1 lenium
ital Cyanide
Ifate
latile Organics
izene
Dmobenzene
imochloromethane
jmodichloromethame
jmoform
jmomethane
)utyIbenzene
:-butylbenzene
RESULT
7.95
400.3
U
U
10/05/95
4.29
141
0.63
U
14.6
U
11.6
U
D
36.5
8.4
0.01
U
U
25.8
U
u
u
u
u u
u
• u
UNITS
pH Unit
ug/L
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
5.2
0.500
0.500
3.2
0.06
0.1
0.1
0.3
1.6
0.65
0.2
3.2
0.3
1.9
0.012
1.6
0.15
1
10
10
10
10
10
10
10
10
ANALYZED
09/22/95
10/24/95
09/21/95
09/21/95
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/17/95
10/10/95
10/16/95
09/27/95
09/29/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
BY
AA
CRS
KMS
KMS
KWB
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD .
LVD
CRS
CRS
CRS
KEN
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
EPA 150.1
EPA 283.2
SOP 420
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
3050
6010
6010
6010
6010
6010
6010 ,
6010
6010
6010
6010
7060
7471
7740
9012
9056
3260A
Page tt: 12
November 6, 1995 08:45 CERTIFICATE: OF AI^^^YSIS
R ESULTS BY SAMPLE
Sample ID: BACKGROUND 5 FT. M-136 lab ID: 9509039-05A CoUected: 09/18/95 15:48:00
TEST
Volatile Organics
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3-chloropropan
1,2-dibromoethane
dibromometheme
di chlorodifluorometheme
1,1-dichloroetheme
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3 -di chloropropeme
2,2-dichloropropeme
^^k - dichloropropene
^^B -1,3- dichloropropene
xrans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
afietone
RESULT
U
U
u u u u u u u u u u . u
u u
u u
u u
u u u u u u u u D
u u
u 3.3BJ
U
D
U
U
D
U
D
U
U
4.7BJ
U
U
U
U
U
U
U
U
U
5.5J
UNCTS
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc /Kg
uc/Kg
uc /Kg
uc/Kg
uo/Kg
uc/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug'Kg
ug'Kg
ug'Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
JVNALYZED
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
Page tt: 13
November 6, 1995 08:45 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: BACKGROUND 5 FT. M-136 LabID: 9509039-05A CoUected: 09/18/95 15:48:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
2-butemone
4-methyl-2-pentemone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
u
u
u 448539
234820
78952
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
dibromofluoromethane
1,2-dichloroetheme-d4
toluene-d8
bromofluorobenzene
10
10
10
09/28/95 MMR
09/28/95 MMR
09/28/95 MMR
09/28/95 MMR
09/28/95 MMR
09/28/95 MMR
For Volatile Organics 8260S
%Recovery
83
85
.3
.0
112
96 .9
SW-846,8260A
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4 TO 112
53.3 TO 121
85.6 TO 143
80.6 TO 130
Sample DO: BACKGROUND 5 FT. M-136 Lab ID: 9509039-06A CoUected: 09/19/95 09:27:00
TEST
Seml-Volatlle Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4 -chloroani1ine
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachl oroc:ycl opentadi ene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
RESULT
U
u
u u u u u
u u
u u
u u
u u u u
u u
u u
u u u u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS# ^^
SW-846, 8270
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7 ^^
Page tf: 14
November 6, 1995 08:45 CERTIl^'ICATE OF A?^^lLYSIS
R] iSULTS BY SAMPLE
Sample ID: BACKGROUND 5 FT. M-136 lab ID: 9509039-06A CoUected: 09/19/95 09:27:00
TEST
Semi-Volatile Organics
2-nitroaniline
dimethylphthalate
acenaphthylene
3-nitroaniline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofurem
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroemiline
4,6-dinitro-2-methylphenol
n-nitrosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenemthrene
emthracene
^^n - butyIphthalate
^Horemthene
pyrene
butylbenzylphthalate
benzo(a) emthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octyIphthalate
benzo(b)fluoremthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h)anthracene
benzo (g,h, Dperylene
RESULT
U
U
u u u
u u u
u u u
u u u
u u u u u
u u 656.0
U
U
u
u u u D
U
U
U
U
U
u
u
UNJ:TS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug/Kg
ug'Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -fluorophenol
phenol -d5
nitrobenzene-d5
2 -fluorobiphenyl
2,4,6-
terphe
tribromophenol
nyl-dl4
DETECTION
LIMIT
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANJLLYZED
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Siaml-Volatile Organics 8270S
%R6covery
22.29
24.08
22.10
25.11
37.75
66.65
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
Page tt: 15
November 6, 1995 08:45 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ED: BACKGROUND 10 FT. M-136 Lab ID: 9509039-07A CoUected: 09/19/95 08:50:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
pH
Titanium
HMZ
Nltroglycerlne
Acid Digestion
Antimony
Barium
Beryllium
Cadmium
Chromium
Lead
Nickel
Silver
Thallium
Zinc
Arsenic
Mercury
Selenium
Seml-Volatlle Organics
phenol
bis (2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propyleunine
hexachloroethane
nitrobenzene
8.02
371.0
U
U
10/05/95
4.28
109
0.56
U
14.3
U
11.4
U
U
33.0
8.3
U
U
U
U
U
u
u
u
u
u D
U
U
U
pH Unit
ug/L
MG/KG
MG/KG .
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
5.2
0.500
0.500
3.3
0.07
0.1
0.1
0.3
1.6
0.65
0.2
3.3
0.3
2.0
0.011
1.6
330
330
330
330
330
330
330
330
330
330
330
330
09/22/95
10/24/95
09/21/95
09/21/95
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/17/95
10/10/95
10/16/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
AA
CRS
KMS
KMS
KWB
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
EPA 150.1
EPA 283.2
SOP 420
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-84e,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1-
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
3050
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
7060
7471
7740
8270
Page tt: 16
November 6, 1995 08:45 CERTIFICATE OF AN^U^YSIS
RESULTS BY SAMPLE
Sample ID: BACKGROUND 10 FT. M-136 ]-abID: 9509039-07A CoUected: 09/19/95 08:50:00
TEST
Semi-Volatile Organics
isophorone
2-nitrophenol
2,4-dimethylphenol
bis (2-chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4-chlorocmiline
hexachlorobutadiene
4-chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2-chloronaphthalene
2-nitroemiline
dimethylphthalate
acenaphthylene
3 - ni t roani 1 ine
acenaphthene
^^4 -dinitrophenol
^^nitrophenol
^j^Ptenzofurem
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroemiline
4,6-dinitro-2-methylphenol
n-nitrosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenanthrene
anthracene
di-n-butylphthalate
fluoremthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoremthene
benzo(k)fluoremthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h) emthracene
benzo (g,h, Dperylene
RESULT
U
u u
u u u u
u u u
u
u u u u u u u u u
u u u u u u
u
u u D
u
u u u u u 101 J
u . u
u u D
u u u u u u u u
u
UNETS
uc:/Kg
uc/Kg
uc/Kg
uc:/Kg
uc/Kg
uc/Kg
uc/Kg
uc /Kg
uc/Kg
uc /Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc /Kg
uc /Kg
uc /Kg
uc /Kg
uc /Kg
uc/Kg
uc /Kg
uc/Kg
uc/Kg
uc /Kg
uc /Kg
uc /Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc /Kg
uc /Kg
uc /Kg
uc /Kg
uc/Kg
uc/Kg
uo/Kg
uo/Kg
DETECTION
LIMIT
330
330
330
330
330
330
33.0
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
2WALYZED
11/01/95
.11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
Page tf: 17
November 6, 1995 08:45 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: BACKGROUND 10 FT. M-136 Lab ID: 9509039-07A CoUected: 09/19/95 08:50:00
TEST
Semi-Volatile Organics
RESULT
Surrogate
UNITS
/Recovery Data
Surrogate
2 -fluorophenol
phenol -d5
nitrobenzene-d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl
Total Cyanide
Sulfate
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodi chlorometheme
bromoform
bromcxne theme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorcjmethane
2 -chlorotoluene
4 -chlorotoluene
dibrcimochloromethane
1,2-dibromo-3 -chloropropan
1,2-dibromoethane
dibromometheme
dichlorodifluoromethane
1,1-di chloroethane
1,2-dichloroethane
1,1-di chloroethene
cis-1,2-dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropeme
2,2-dichloropropeme
1,1-dichloropropene
cis-1,3 -dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
-dl4
u
24.7
u u U
U
U
U
U
U
U
U
U
U
u u u u u u u u u u u
u
u
u u
u
u u u u u u u u
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
ANALYZED BY METHOD/CAS#
SW-846,
For Semi-Volatile Organics 8270S
%Recovery
61
53
44
58
74
.08
.36
.65
.7.2
.16
114.8
0 .15
1
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
09/27/95
09/29/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
KEN
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,
SW-846,
8270
9012
9056
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-
10061-02-
95-50-1
541-73-1
106-46-7
100-41-4
^ w
5
6
^^^
Page ff: 18
November 6, 1995 08:45 CERTI FICATE OF AN^O^YSIS
RESULTS BY SAMPLE
Sample ID: BACKGROUND 10 FT. M-136 lab ID: 9509039-07A CoUected: 09/19/95 08:50:00
TEST
Volatile Organics
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroetheme
te t rachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
^^Kylene
I^H-xylene
'^rcetone
2-butemone
4-methyl-2-pentemone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4 -di chlorobenzene-d4
RESULT
U
U
U
U
u u u u u
u
u u
u 17B
U
U
U
U
u u u u
u 6. 8 J
u U
U
521370
260757
96017
UNCTS
uc /Kg
uc /Kg
uc /Kg
uc/Kg
uc/Kg
uc/Kg
ug/Kg
uo/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recoverv- Data For Volatile Organics 8260S
Surrogate
dibromofluorometheme
1,2-• di chl oroe thane - d I
toluene-d8
bromofluorobenzene
^Recovery
74.8
75.5
115
94.9
METHOD/CAS#
SW-846,8260A
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Racovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Sample ID: BACKGROUND 15 FT. M-136 Lab ID: 9509039-08A CoUected: 09/19/95 09:00:00
TEST RESULT UN]TS DETECTION ANJILYZED BY
LIMIT
METHOD/CAS#
pH
Titanium
8.38 pH anit
490.1 uc/L
09/22/95 AA EPA 150.1
4.7 10/24/95 CRS EPA 283.2
Page #: 19
November 6, 1995 08:45 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: BACKGROUND 15 FT. M-136 Lab ID: 9509039-08A CoUected: 09/19/95 09:00:00
TEST
HMZ
Nltroglycerine
Acid Digestion
Antimony
Barium
Beryllium
Chromium
Lead
Nickel
Silver
Thallium
Zinc
Arsenic
Mercury
Selenium
Semi-Volatile Organics
phenol
bis (2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis{2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propyleunine
hexachloroetheme
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)metheme
^,4 -dichlorophenol
RESULT
U
U
10/05/95
U
138
0.80
U
16.5
U
11.4
U
U
40.0
6.2
0.01
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
UNITS
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.500
0.500
3.0
0.06
0.1
0.1
0.3
1.5
0.59
0.2
3.0
0.2
1.8
0.013
1.4
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
09/21/95
09/21/95
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/17/95
10/10/95
10/16/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
BY
KMS
KMS
KWB
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SOP 420
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
3050
6010
6010
6010
6010
6010
GOlO
6010
6010 ^^
6010
6010
7060
7471
7740
8270
^^
Page tt: 20
November 6, 1995 08:45
#
CERTD^'ICATE OF ANi^LLYSIS
R)!SULTS BY SAMPLE
Sample ID: BACKGROUND 15 FT. M-136 lab ID: 9509039-08A CoUected: 09/19/95 09:00:00
TEST
Semi-Volatile Organics
1,2,4-trichlorobenzene
naphthalene
4-chloroemiline
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachl oroc:y cl opentadi ene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2-chloronaphthalene
2 - ni troemi 1 ine
dimethylphthalate
acenaphthylene
3-nitroaniline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofurem
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
^•^lorophenyl -phenylether
^^Hbrene
^kitroaniline
4,6-dinitro-2-methylphenol
n-nitrosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenanthrene
emthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoremthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h) anthracene
benzo(g,h,i)perylene
RESULT
U
U
u u u u u u u u u u u u u
u
u u u u u D
u u u u u u u
u u 922.0
U
u u u u u
u u u u u
u u u
UN::TS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug'Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug,'Kg
ug/Kg
ug/Kg
ug/Kg
ug; Kg
ug, Kg
ug/Kg
ug/ Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANi\LYZED
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
Surrogate/Recovery Data For Seml-Volatlle Organics 8270S
Surrogate
2 -fluorophenol
%Recovery
29.75
Recovery Limits
25 TO 121
Page tf: 21
November 6, 1995 08:45 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: BACKGROUND 15 FT. M-136 Lab ID: 9509039-08A CoUected: 09/19/95 09:00:00
TEST
Seml-Volatlle Organics
Total Cyanide
Sulfate
Volatile Organics
benzene
brcamobenzene
bromochloromethane
bromodi chlorometheme
bromoform
brc^mome tihane
n-butylbenzene
sec-butylbenzene
te rt-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
phenol
RESULT
-d5
nitrobenzene-d5
2 -fluorobiphenyl
2,4,6-
UNITS
tribromcjphenol
terphenyl-dl4
1,2-dibromo-3 -chloropropan
1,2-dibromoetheme
dibromome thane
dichlorodif luorcjmetheme
1,1 - di chloroetheme
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2-dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2 -dichlorcjprcjpane
1,1-dichloropropene
cis-1,3-dichloropropene
trems -1,3- dicdiloroprcspene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 - iscjpropyl toluene
methylene chloride
u
24.3
u u u
u U
O
U
U
U
U
U
U
U
U
u
u D
U
U
U
U
U
U
u u u u
. u u
u u
u u u u u u u
u 3.4BJ
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
31
32
33
42
67
0
.63
.63
.85
.48
.37
.15
1
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
24
23
30
19
18
09/27/95
09/29/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
BY
TO 113
TO 120
TO 115
TO 122
TO 137
KEN
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
SW-846, 9012
SW-846, 9056
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5 ^^
108-90-7 ^m
75-00-3 ^^
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
Page tt: 22
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
A Ie ID: BACKGROUND 15 FT. M-136 Lsb ID: 9509039-08A CoUected: 09/19/95 09:00:00
TEST
Volatile Organics
naphthalene
n-propylbenzene
styrene
RESULT
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2, 3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl czhloride
o-xylene
m,p-xylene
acetone
2 -butanone
4-methyl- 2-pentanone
2^^xanone
^^^fobenzene
c)i^R:obenzene - d5
1,4- dic:hlorobenzene - d4
4.
u
U
U
U
U
U
U
U
U
163
U
u
u
u
u
D
u
D
u ,4 J
U
U
U
645876
348203
123621
Surrogat
Surrogate
UNI'.:S
ug/ Cg
ug/ Cg
ug/:Cg
ug/lCg
ug/)Cg
ug/.'Cg
ug/)Cg
ug/JCg
ug/):g
ug/):g
ug/]:g
ug/Kg
ug/l :g
ug/l :g
ug/] :g
ug/l :g
ug/l ;g
ug/I ;g
ug/I g
ug/?g
ug/Fg
ug/Fg
ug/Fg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10 -
10
10
10
10
10
10
10
10
10
10
10
10
10
10
AUrAICiYZED
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/23/95
09/2.3/95
09/23/95
09/23/95
09/2S/95
09/28/95
09/28/95
09/28/95
09/213/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/2&/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
e/Recovery Oata For Volatile Oiganics 8260S
dibromofluoromethane
1 ,2 -dichloroethane-d4
toluene-d8
bromofluorobenzene
^Recovery
86.1
84.5
109
95.6
METHOD/CAS#
SW-846,8260A
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 13 0
Sample ID: M-338, 5 FT. SWMU #608 Lab ID: 9509039-09A CoUected: 09/19/95 10:59:00
TEST RESULT UNIT;; DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
pH
Acid Digestion
Antimony
Chromium
8.15
10/05/95
5.73
14.1
pH Un::t
DATE
ug/g
ug/g
3.3
0.3
09/22/95
10/05/95
10/11/95
10/11/95
AA
KWB
LVD
LVD
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
Page t. 23
November 6, 1995 08:45 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-338, 5 FT. SWMU #608 LabID: 9509039-09A CoUected: 09/19/95 10:59:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Lead
Arsenic
Sulfate
U ug/g
31.7 ug/g
27.8 ug/g
1.6 10/11/95 LVD
2.0 10/17/95 CRS
1 09/29/95 CRS
SW-846, 6010
SW-846, 7060
SW-846, 9056
Sample ID: M-338, 10 FT. SWMU #608 LabID: 9509039-lOA CoUected: 09/19/95 11:13:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
pH
Add Digestion
Antimony
Chromium
Lead
Arsenic
Sulfate
8.32
10/05/95
7.17
12.5
U
13.5
49.9
pH Dnit
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
3.2
0.3
1.6
1.9
1
09/22/95
10/05/95
10/11/95
10/11/95
10/11/95
10/17/95
09/29/95
AA
KWB
LVD
LVD
LVD
CRS
CRS
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 9056
Page ff: 24
Dati I Reporting Qualifiers
U Compound was analyzed for bi it not detected. Indicates compound was below detection limit.
J Indicates an estimated value. Oliis flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the id( ntiilcation criteria but ttie result is less than the specified
detection limit but greater than zero. (e.g. l.U with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was 01 itside of the caUbration irange but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection Umits for the test.
NA Not appUcable.
NT Indicates that an analyte was nc t tested for.
Q Surrogate/spike recovery was 0 utside of the specified liinits. If surrogate recoveries are out
of limits, any values reported a le for indication only.
m ENVIRONMEN rAL LAB WORK RE(^UEST
THIOKOL ENVIRONMENTAL LABORATORY LWR No. E11052
A F UdALf/:ei^ EX- :ENSION COST CENTI!R WORK ORDER
9^^.o'^^
ORGANIZATION
£-/ny,ror^Ujf/'. y 3oi€
REPORT RESULTS TO:
HELEN WARD, MS 301
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ENVIRONMENTAL LAB WORK REQUEST
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SAMPLE INFORMATION
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November 3, 1995
•
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward MIS 301
Thiokol Corp, Ut 84322
A.F. WALKER
EXT 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
/Inalytical Labs MIS 245
Atm: Dr. Jofm Terry
Tele: 801-863-2384
Work Orderly 9509043 Sample ai id Test Code Identifilcaition
LabID:
OIA
Sample ID:
GD /«, 5 FT. 11625
Test Codes and Names
LabID:
02A
Sample ID:
GD #5, 10 FT. #625
'LabID:
03A
Sample ID:
RINSE BLANK imS
LabID:
04A
Sample ID:
GD m, 5 FT. #625
UbID:
"OSA
Sample ID:
GD i«73, 10 FT. #625
LabID:
06A
Sample ID:
GD#75, 5FT. #625
3050
B AE2
CD A)2
CR A12
PB AI2
AG A)L2
HG C''2
8270s
8260S
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
3050
B AE2
CD A] 2
CR A12
PB AI2
AG A12
HG c-n. 8275s 8260S
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
3010
B AE2
CD A] 2
CR AI2
PB A£2
AG A] 2
HG C^'3
8260
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Orgamcs
Test Codes and Names
3050
B AE2 CD A] 2
CR AI2
PB AE2
AO A12
HG 0^7
8270s
8260S
Acid Digestion
Boron Cadmium
Chromium
Lead
Silver
Mercuiy
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
3050
B AE2
CD A] 2
CR AI2
PB A£2
AG A] 2
HG 0 7
8270s 8260S
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
6010
6010
6010
6010
3050
B AE2
Acid Digestion
Boron
Method
SW-846, 3050
SW-846, 6010
SW-846,
SW-846,
SW-846,
SW-846,
SW-846, 7471
SW-846, 8270
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A
Method
SW-846, 3010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7470
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
Page#:lof ^(^
Work Order <» 9509043 Sample and Test Code Identification
LabID:
06A
Sample ID:
GD #75, 5 FT. #625
LabID:
07A
Sample ID:
GD ins, 10 FT. #625
LabID:
'"08A
Sample ID:
GD m, 5 FT. #625
UbID:
09A
UbID:
lOA
Sample ID:
OD «8, 5 FT. #625 DUP.
Sample ID:
OD #36, 5 FT. #625
UbID:
UA
lelD:
GD ifi6, 10 FT. #625
UbID:
12A
UbID:
13A
Sample ID:
GD#36, IOFT. #625 DUP.
Sample ID:
GD #189, 5 FT. #625
UbID:
14A
Sample ID:
GD #189, 10 FT. #625
Tftst Codes and Names
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8270s
8260S
Cadnuum
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
3050
B AE2
CD A£2
CR AE2
PB AE2
AG"AE2
HG CV2
8270s
8260S
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
3050
B AE2
CD AE2
CR AE2
PB AE2
AG"AE2
HG CV2
8270s 8260S
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
Volatile Oroanics
Test Codes and Names
8260S Volatile Orgaiucs
Test Codes and Names
3050
B AE2
CD AE2
CR"AE2
PB AE2
AG AE2
HO CV2
8270s
8260S
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
3050
B AE2
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8270s
8260S
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
8270S Semi-Volatile Organics
Test Codes and Names
3050
B AE2
CD AE2
CR AE2
PB AE2
AG AE2
HO CV2
8270S
8260S
Acid Digestion
Boron
Cadnuum
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
3050
B AE2
CD AE2
Acid Digestion
Boron
Cadmium
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A
Method
SW-846, 3050
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A
Method
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A
Method
SW-846, 8270
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
Page tt:2
Work Order A< 9509043 Sample ai id Test Code Identif ictttion
UbID:
I5A
Sample ID:
GD#189, IOFT. #625
Test Codes and Names
Sample ID:
GD #147, 5 FT. #625
UbID:
16A
Sample ID:
GD #147, 10 FT. #625
Ub ID:
"HA
Sample ID:
GD #38, 10 FT. #625
CR A] 2
PB AI2
AO A.12
HO C/2
8270S
8260S
Chromium
Lead
Silver
Mercury
Semi-Volatile Oiganics
Volatile Organics
Test Codes and Names
3050
B AE2
CD A] 2
CR A12
PB A£2
AG A12
HG C"2
8270S
8260S
Acid Digeslion
Boron
Cadmium
Chromium
Lead
Silver
Mercuiy
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
3050
B AE2
CD A12
CR AI2
PB AEJ
AG'A12
HG"C^2
8270S
8260S
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercuiy
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
3050
B AE2
CD AI2
CR AE2
PB AEI
AG AI2
HG C\2
8270S
8260S
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercuiy
Semi-Volatile Organics
Volatile Organics
Cnmmeints
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,8260A
Method
,6010
,6010
,7471
8270
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A
Workorder: NOTE FOR METHOD 8270: The intemal standard solution used for
these samples appeared to be slightly degraded, this resulted
in low surrogate recoveries.
Report: There is evidence of a s light negative matrix interference for
lead and silver.
Certified By
Page #:3
This is to certify tliat tfie following samples were analyzed using good laboratory practices
to sfiow the following results.
Sample ID: GD #5, 5 FT. #625 Lab ID: 9509043-OlA Collected: 09/20/95 08:47:00
TEST
Add Digestion
Boron
Cadinium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
phenol
bis (2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis (2-chloroethoxy)metheuie
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4 -chloroaniline
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroaniline
dimethylphthalate
acenaphthylene
3-nitroaniline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dinitrotoluene
RESULT
10/05/95
6.00
0.36
21.6
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u u
u u u u u u u
u u u
u u u u
DNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.4
0.1
0.3
1.5
0.2
0.015
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
. 330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
ANALYZED
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/10/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
BY
KVfB
LVD
LVD
LVD
LVD
LVD
CRS
JMA
<THA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
3050
6010
6010
6010
6010
6010
7471
8270
A V
^^
Page tt: A
November 3, 1995 13:36
Sample ID: GD #5, 5 FT. #625
CERTIFICATE OF AN^O^YSIS
RESULTS BY SAMPLE
lab ID: 9509043-01A Collected: 09/20/95 08:47:00
TEST
Semi-Volatile Organics
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenyl (
fluorene
4-nitroaniline
2 ther
4,6-dinitro-2-methylphenol
n-nitrosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenanthrene
anthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
^l^zo (b) fluoranthene
^^^zo (k) fluoranthene
^^izo (a) pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h) amthracene
benzo(g,h,i)perylene
Volatile Organics
benzene
bromobenzene
bromochl orome theUie
bromodi chloromethane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
RESULT
387
U
U
U
U
U
U
U
U
U
U
U
U
.3
U
D
U
U
U
U
U
U
U
u
u u u u
UNCTS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery rata
Surrogate
2 -fluorophenol
phenol -d5
nitrobenzene -d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
U
U
U
U
U
U
D
U
U
U
u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
AN.IILYZED
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270S
%Recovery
25.01
25.61
25.55
25.29
33.76
63.95
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
Page tt: 5
November 3, 1995 13:36 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #5, 5 FT. #625 Lab ID: 9509043-OlA Collected: 09/20/95 08:47:00
TEST
Volatile Organics
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo- 3 -chloropropan
1,2-dibromoethane
dibromomethane
dichlorodifluoromethane
1.1-dichloroetheme
1.2 -dichloroethcuie
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2 -di chloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropane
1,1-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl- 2-pentanone
2-hexanone
fluorobenzene
RESULT
U
U
u u u u
u u u u
u
u
u u
u u
u u
u u u u u u u u u u o u u u u u u u u 5.0 J
u » u D
u
u u u u u u u u
u 763343
tJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1 ^^^
106-46-7 flB
100-41-4 ^^
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
Page tt: 6
November 3, 1995 13:36 CERTIFICATE OF ANiU^YSIS
*' RESULTS BY SAMPLE
Sample ID: GD #5, 5 FT. #625 i i' «• '• lab ID: 9509043-OlA CoUected: 09/20/95 08:47:00
TEST
Volatile Organics
chlorobenzene-d5
1,4-dichlorobenzene•
RESULT UNCTS
422638 uc/Kg
-d4 151858 uc/Kg
DETECTION ANALYZED BY METHOD/CAS#
LIMIT
SW-846,8260A
10/03/95 MMR INTSTD2
10/03/95 MMR INTSTD3
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluoromethane
1,2 -di chloroetheme-c 4
toluene-da
bromofluorobenzene
%Recovery Recovery Limits
83.3 58.4 TO 112
76.3 53.3 TO 121
124 85.6 TO 143
110 80.6 TO 130
Sample ID: GD #5, 10 FT. #625 lab ID: 9509043-02A CoUected: 09/20/95 08:58:00
TEST
Acid Digestion
^Kon
Cadmium
Chromium
Lead
Silver
Mercury
Seml-Volatlle Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
RESULT
10/05/95
5.
0.
13
75
28
l.l
U
U
u
u u u u u u u
u u u u u
u u u
UN::TS
DATE
Ui[/g
u<r/g
utr/g
uc[/g
uct/g
uct/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug''Kg
ug'Kg
ug'Kg
DETECTION
LIMIT
0.4
0.1
0.3
1.6
0.2
0.014 .
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
AN.I^YZED
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/10/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
BY
KWB
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
3050
6010
6010
6010
6010
6010
7471
8270
Page tf: 7
November 3, 1995 13:36 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #5, 10 FT. #625 Lab ID: 9509043-02A CoUected: 09/20/95 08:58:00
TEST
Seml-Volatlle Organics
bis(2-chloroethoxy)metheme
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4 - chloroeuiiline
hexachlorobutadi ene
4-chloro-3-methylphenol
2-methylnaphthalene
hexachloroc:yclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroaniline
dimethylphthalate
acenaphthylene
3-nitroaniline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofurem
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4 - ni troani1ine
4,6- dinitro-2-methylphenol
n - nitrosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenanthrene
emthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis (2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3 -cd)pyrene
dibenz(a,h) emthracene
benzo (g,h, Dperylene
RESULT
U
u u u u u u u o u u u u u D
D
U
U
U
U
u u u
u D
U
U
U
u
u u
u
u u
u u
u u u u u u u u u u
u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2 ^^
84-66-2 flB
7005-72-3 ^^
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
Page tt: 8
November 3, 1995 13:36 CERTIJP'ICATE OF ANCLLYSIS
RiSULTS BY SAMPLE
Sample ID: GD #5, 10 FT. #625 lab ID: 9509043-02A CoUected: 09/20/95 08:58:00
TEST
Semi-Volatile Organics
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chloromethane
bromoform
bromome thame
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
i^|or obenz ene
^I^Boroe thane
chlorofonn
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
RESULT UN;:TS
Surrogate/Recovery Iata
Surrogate
2-fluorophenol
phenol -d5
nitrobenzene-d5
2-fluorobd
2,4,6-
iphenyl
tribromophenol
terphenyl•
1,2-dibromo-3-chloropropan
1,2-dibromoetheme
dibromomethane
di chl orodi f luor ome thane
1,1-di chloroethane
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis-1,3-dichloropropene
trans -1,3 -dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4-isopropyltoluene
methylene chloride
•dl4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u u u u u u u u u
u u u
u u a
u u u u u
u
u u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug'Kg
ug'Kg
ug/Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug 'Kg
ug/Kg
ug'Kg
ug'Kg
ug'Kg
ug'Kg
ug/Kg
ug/Kg
ug'Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
AN^M^YZED BY METHOD/CAS#
SW-846, 8270
For Semi-Volatile Organics 827OS
%Recovery
39.47
37.13
39.70
40.74
40.72
64.13
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
Page tt: 9
November 3, 1995 13:36 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #5, 10 FT. #625 Lab ID: 9509043-02A CoUected: 09/20/95 08:58:00
TEST
Volatile Organics
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethame
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroethane
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
5
U
U
U
U
U
u u
u u .6J
U
u
u u u u u u u u u u
u 549695
324799
132062
Surrogate
Surrogate
/Rec
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
::overy Data For Volatile Organics 8260S
dibromofluorometheme
1,2-dichloroetheme-d4
toluene-d8
bromofluorobenzene
%Recovery
83.0
83.5
121
109
METHOD/CAS#
SW-846,8260A
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1 ^^.
591-78-6 flB'
INTSTDl ^^
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Sample ID: RINSE BLANK #625 LabID: 9509043-03A CoUected: 09/20/95 09:16:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Boron
Cadmium
Chromium
09/22/95
28
U
U
DATE
ug/L
ug/L
ug/L
6
2
5
09/22/95
09/25/95
09/25/95
09/25/95
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
3010
6010
6010
6010
Page tt: 10
November 3, 1995 13:36
fliiiple ID: RINSE BLANK #625
CERTIFICATE OF AN^O^YSIS
RSSULTS BY SAMPLE
lab ID: 9509043-03A CoUected: 09/20/95 09:16:00
TEST RESULT UNJITS DETECTION ANilLYZED BY
LIMIT
METHOD/CAS#
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodichlorometheme
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorome theme
2 -chlorotoluene
4-chlorotoluene
komochlorome thane
Fdibromo-3 -chloropropem
l'r2 - dibromoetheme
dibromomethane
di chlorodi fluorometheme
1,1-di chloroetheme
1,2-dichloroethane
1,1-di chloroethene
cis-l,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis-l,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethame
u
u
u
u
u u u u
u
u
u D
u
u u 3.6
u u u u u
u u u
u u
u u u
u u u u
u
u u V
u a u u a u u
u
u
u
u
uc/L
uc/L
ug/L
ug/L
ug/L
ug'L
ug'L
ug/L
ug/L
ug/L
ug/L
ug,'L
ug/L
ug/L
ug/L
ug;L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/Ci
ug/C
ug/L
ug/j
ug/j
ug/j
ug/zj
ug/:.
ug/;..
ug/3.
ug/].
ug/].
ug/],
ug/Ii
ug/I.
ug/L
ug/I
ug/I
ug/I
ug/l
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
25
3
0.15
0.20
0.20
0.20
0.30
0.10
0.40
0.20
0.20
0.20
0.30
0.20
0.40
0.40
0.60
0.20
0.20
0.30
0.20
0.20
0.20
0.20
0.10
0.20
0.60
0.20
0.20
0.20
0.20
0.20
0.20
0.20
0.20
0.10
0.20
0.20
0.30
0.20
0.20
0.20
0.30
0.20
0.20
0.20
0.20
0.30
09/25/95
10/05/95
09/27/95
09/28/95
09/28/95
09/:J8/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/23/95
09/23/95
09/28/95
09/'28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/2£l/95
09/2£l/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 6010
SW-846, 6010
SW-846, 7470
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
Page#: 11
November 3, 1995 13:36
Sample D): RINSE BLANK #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9509043-03A CoUected: 09/20/95 09:16:00
TEST
Volatile Organics
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentemone
2 -hexanone
fluorobenzene
chlorobenzene-d5
1,4 -dichlorobenzene-d4
RESULT
U
U
u
u u
u
u u
u V
u u u
u 40
3.9 J
U
1.0 J
719164
533290
233254
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
0.90
0.30
0.20
0.20
0.20
0.20
0.30
0.30
0.20
0.20
0.20
0.40
0.20
0.20
10
10
10
10
ANALYZED
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
09/28/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8260
Sxirrogate
dibromofluoromethane
1 ,2 -dichloroethane-d4
toluene-d8
bromof1uorobenzene
%Recovery
98.7
108
99.2
104
METHOD/CAS#
SW-846,8260A
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
•
Recovery Limits
80.0
80.0
80.0
80.0
TO 120
TO 120
TO 120
TO 120
Sample ID: GD #73, 5 FT. #625 LabID: 9509043-04A CoUected: 09/20/95 09:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Boron
Cadmium
Chromiua
Lead
Silver
10/05/95
2.23
0.56
18.7
U
11.8
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
0.4
0.1
0.3
1.6
0.2
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
KWB
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
Page tt: 12
November 3, 1995 13:36
f
nple ample ID: GD #73, 5 FT. #625
CERTIFIC ATE OF ANA1.YSIS
RiSULTS BY SAMPLE
LabID: 9509043-04A CoUected: 09/20/95 09:20:00
EST
arcury
ami-Volatile Organics
tienol
is(2-chloroethyl)ether
-chlorophenol
,3-dichlorobenzene
,4 -dichlorobenzene
,2-dichlorobenzene
-methylphenol
is(2-chloroisopropyl)ethe
-methyIpheno1
-nitroso-di-n-propyleimine
axachloroethane
itrobenzene
sophorone
-nitrophenol
,4 -dimethylphenol
is(2-chloroethoxy)methane
,4-dichlorophenol
,2,4-trichlorobenzene
aphthalene
-ch^^oaniline
sxl^Bor obut adi ene
-cflf^^o-3-methylphenol
-methylnaphthalene
exachlorocyclopentadiene
,4,6-trichlorophenol
,4,5-trichlorophenol
-chloronaphthalene
-nitroemiline
imethylphthalate
cenaphthylene
-nitroemiline
cenaphthene
,4-dinitrophenol
-nitrophenol
ibenzofursm
,6-dinitrotoluene
,4-dinitrotoluene
iethyIphthalate
-chlorophenyl-phenylether
luorene
-nitroemiline
,6-dinitro-2-methylphenol
-nitrosodiphenylamine
-bromophenyl-phenylether
axachlorobenzene
2ntachlorophenol
lenanthrene
Ithracene
L ^n-butyIphthalate
Luoremthene
RESULT
0.03
U
U
U
U
U
U
U
u u
u u u u
u
u u
u u u
u u
u
u u u u u u u o u u
u u u u u u u u u u
u u u u
u u 564
u
UNITS
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.015
330
330
330
330
- 330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
ANAI.Y:ZED
10/10/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/915
10/18/915
10/18/9:5
10/18/95
10/18/915
10/18/95
10/18/915
10/18/915
10/18/915
10/18/915
10/18/95
10/18/95
BY
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 7471
SW-846, 8270
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
Page tt: 13
November 3, 1995 13:36 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #73, 5 FT. #625 LabID: 9509043-04A CoUected: 09/20/95 09:20:00
TEST
Seml-Volatlle Organics
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoremthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h) emthracene
benzo(g,h,i)perylene
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodi chloromethane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
RESULT
Surrogate
U
U
U
U
U
O
U
U
U
U
U
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
/Recovery Data
Surrogate
2 -fluorophenol
phenol -d5
nitrobenzene-d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl
1,2-dibromo-3 -chloropropem
1,2-dibromoethane
dibromometheme
di chlorodi fluorometheme
1,1-dichloroetheme
1,2-dichloroethane
1,1-dichloroethene
cis-l,2-dichloroethene j
trans-1,2-dichloroethene
•dl4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u u
u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
BY
JM;^
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Seml-Volatlle Organics 8270S
%Recovery
28.09
26.91
27.37
29.52
40.92
63.65
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
mm MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
— A
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
Page#: 14
November 3, 1995 13:36 CERTIFICATE OF AN/O^YSIS
RESULTS BY SAMPLE
Sample ID: GD #73, 5 FT. #625 lab ID: 9509043-04A CoUected: 09/20/95 09:20:00
TEST
Volatile Organics
1,2-dichloropropane
1,3-dichloropropeme
2,2-dichloropropeme
1,1-dichloropropene
cis-1,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
^^^, 3 - trichlorobenzene
i^B, 4 - trichlorobenzene
51^, 1 - trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2 - hexemone
fluorobenzene
chlorobenzene-d5
1,4 -di chlorobenzene-d4
RESULT
3
U
U
U
O
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u u
u
u .8J
O
u u u u u u D
U
u u D
U
568483
361959
136253
Surrogate
Surrogate
UN:CTS
uc/Kg
uc/Kg
uc/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug'Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
AN.IVLYZED
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MJ^IR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
s/Recover;' Data For Volatile Organics 8260S
di bromofluorometheme
1,2-dichloroethane-dl
toluene-d8
bromofluorobenzene
%Recovery
83.4
82.5
118
112
METHOD/CAS#
SW-846,8260A
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Page tt: 15
November 3, 1995 13:36 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #73, 10 FT. #625 Lab ID: 9509043-05A CoUected: 09/20/95 09:39:00
TEST
Acid Digestion
Boron
Cadmium
Chromitiffl
Lead
Silver
Mercury
Seml-Volatlle Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroetheme
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)metheme
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4 -chloroemi1ine
hexachlorobutadiene
4-chloro-3-methylphenol
2-methylnaphthalene
hexachloroc:yclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroaniline
dimethylphthalate
acenaphthylene
3-nitroemiline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofurem
2,6-dinitrotoluene
2,4-dinitrotoluene
RESULT
10/05/95
3.99
U
10.1
U
U
U
U
U
U
U
u u u u
u u u u u u u u u u u u u u
u u • u
u u u u u u u
u u u u
u
UNITS
DATK
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.3
0.1
0.3
1.4
0.2
0.014
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
ANALYZED
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/25/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
BY
KWB
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMR.
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
3050
6010
6010
6010
6010
6010
7471
8270
A W
^^
Page tt: 16
November 3, 1995 13:36
Sample ID: GD #73, 10 FT. #625
CERTIHCATE OF AN^^LLYSIS
Rl SULTS BY SAMPLE
LabID: 9509043-05A CoUected: 09/20/95 09:39:00
TEST RESULT UN]TS DETECTION ANJ^YZED BY
LIMIT
METHOD/CAS#
Semi-Volatile Organics
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroemiline
4,6-dinitro-2-methylphenol
n - ni trosodiphenyleimine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenanthrene
anthracene
di -n-butylphthalate
fluoremthene
pyrene
butylbenzylphthalate
benzo(a) emthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoremthene
IMDZO(k)fluoranthene
I^KO (a) pyrene
^iroeno(1,2,3 -cd)pyrene
dibenz(a,h)anthracene
benzo(g,h,i)perylene
SW-846, 8270
U ug/Kg 330 10/18/95 JMA 84-66-2
U ug/Kg 330 10/18/95 JMA 7005-72-3
U ug/Kg 330 10/18/95 JMA 86-73-7
U ug/Kg 660 10/18/95 JMA 100-01-06
U ug/Kg 330 10/18/95 JMA 534-52-1
U ug/Kg 330 10/18/95 JMA 86-30-6
U ug'Kg . 330 10/18/95 JMA 101-55-3
U ug'Kg 330 10/18/95 JMA 118-74-1
U ug'Kg 1700 10/18/95 JMA 87-86-5
U ug'Kg 330 10/18/95 JMA 85-01-8
U ug'Kg 330 10/18/95 JMA 120-12-7
U ug/Kg 330 10/18/95 JMA 84-74-2
U ug/Kg 330 10/18/95 JMA 206-44-0
U ug/Kg 330 10/18/95 JMA 129-00-0
U ug/Kg 330 10/18/95 JMA 85-68-7
U ug/Kg 330 10/18/95 JMA 56-55-3
U ug/'Kg 330 10/18/95 JMA 91-94-1
U ug/'Kg 330 10/18/95 JMA 117-81-7
U ug;'Kg 330 10/18/95 JMA 218-01-9
U ug/Kg 330 10/18/95 JMA 117-84-0
U ug/Kg 330 10/18/95 JMA 205-99-2
U ug/Kg 330 10/18/95 JMA 207-08-9
U ug/Kg 330 10/18/95 JMA 50-32-8
U ug/Kg 330 10/18/95 JMA 193-39-5
U ug/Kg 330 10/18/95 JMA 53-70-3
U ug/Kg 330 10/18/95 JMA 191-24-2
Surrogate/Recovery Data For Seml-Volatlle Organics 8270S
Surrogate
2 -fluorophenol
phenol-d5
nitrobenzene-d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
%Recovery
42.68
39.77
42 .17
41.22
42.44
65.51
Recovery Limits
25 TO 121
24 TO 113
23 TO 120
30 TO 115
19 TO 122
18 TO 137
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodi chlorometheme
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
U
U
U
U
U
U
U
U
U
U
U
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
SW-846,8260A
10 10/03/95 MMR 71-43-2
10 10/03/95 MMR 108-86-1
10 10/03/95 MMR 74-97-5
10 10/03/95 MMR 75-27-4
10 10/03/95 MMR 75-25-2
10 10/03/95 MMR 74-83-9
10 10/03/95 MMR 104-51-8
10 10/03/95 MMR 135-98-8
10 10/03/95 MMR 98-06-6
10 10/03/95 MMR 56-23-5
10 10/03/95 MMR 108-90-7
10 10/03/95 MMR 75-00-3
10 10/03/95 MMR 67-66-3
Page tt: 17
November 3, 1995 13:36
Sample ID: GD #73, 10 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9509043-05A CoUected: 09/20/95 09:39:00
•
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorcsme thane
1,2-dibromo-3 -chloropropem
1,2-dibromoetheme
dibromomethane
di chlorodi fluoromethane
1,1-dichloroethane
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2-dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropane
2,2-dichloropropeme
1,l-dichloropropene
cis-l,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
i sopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroetheme
t e t rachl oroe thene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butcmone
4-methyl-2-pentanone
2-hexemone
fluorobenzene
chlorobenzene-d5
u
u u u u u u u u u u u u u u u
u u u u
u u u u u
u
u u u
u a u
u u u
u 5.1 J
u u u u u u u u u
u
u
u u 499411
320905
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846,8260A
10/03/95 MMR 74-87-3
10/03/95 MMR 95-49-8
10/03/95 MMR 106-43-4
10/03/95 MMR 124-48-1
10/03/95 MMR 96-12-8
10/03/95 MMR 106-93-4
10/03/95 MMR 74-95-3
10/03/95 MMR 75-71-8
10/03/95 MMR 75-34-3
10/03/95 MMR 107-06-2
10/03/95 MMR 75-35-4
10/03/95 MMR 156-59-4
10/03/95 MMR 156-60-5
10/03/95 MMR 78-87-5
10/03/95 MMR 142-28-9
10/03/95 MMR 590-20-7
10/03/95 MMR 563-58-6
10/03/95 MMR 10061-01-5
10/03/95 MMR 10061-02-6
10/03/95 MMR 95-50-1
10/03/95 MMR 541-73-1
10/03/95 MMR 106-46-7
10/03/95 MMR 100-41-4
10/03/95 MMR 87-68-3
10/03/95 MMR 98-82-8
10/03/95 MMR 99-87-6
10/03/95 MMR 75-09-2
10/03/95 MMR 91-20-3
10/03/95 MMR 103-65-1
10/03/95 MMR 100-42-5
10/03/95 MMR 630-20-6
10/03/95 MMR 79-34-5
10/03/95 MMR 127-18-4
10/03/95 MMR 108-88-3
10/03/95 MMR 87-61-6
10/03/95 MMR 120-82-1
10/03/95 MMR 71-55-6
10/03/95 MMR 79-00-5
10/03/95 MMR 79-01-6
10/03/95 MMR 75-69-4
10/03/95 MMR 96-18-4
10/03/95 MMR 95-63-6
10/03/95 MMR 108-67-8
10/03/95 MMR 75-01-4
10/03/95 MMR 95-47-6
10/03/95 MMR 108-38-3
10/03/95 MMR 67-64-1
10/03/95 MMR 78-93-3
10/03/95 MMR 108-10-1
10/03/95 MMR 591-78-6
10/03/95 MMR INTSTDl
10/03/95 MMR INTSTD2
Page tf: 18 o
November 3, 1995 13:36 CERTIFICATE OF AN^LLYSIS
^ RliSULTS BY SAMPLE
•!• •?••••
Sample ID: GD #73, 10 FT. #625 lab ID: 9509043-05A CoUected: 09/20/95 09:39:00
TEST RESXTLT UNJiTS DETECTION ANJ^YZED BY
LIMIT
METHOD/CAS#
Volatile Organics
1,4 -dichlorobenzene-d4 150521 ug/Kg
Surrogate
dibromofluorome thane
1,2-dichloroethane-dI
toluene-d8
bromofluorobenzene
SW-846,8260A
10/03/95 MMR INTSTD3
For Volatile
%Recovery
88.0
91.6
114
101
Organics 8260S
Recovery Limits
58.4 TO 112
53.3 TO 121
85.6 TO 143
80.6 TO 130
Sample ID: GD #75, 5 FT. #625 LabID: 9509043-06A CoUected: 09/20/95 10:02:00
TEST
Acid Digestion
i^con
Cadmium
Chromium
Lead
Silver
Mercury
Seml-Volatlle Organics
phenol
bis(2-chloroethyl)ether
2-chlorophenol
1,3 -dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroetheme
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)metheme
RESULT
10/05/95
5.67
U
19.9
U
U
U
U
U
D
U
U
U
U
U
U
U
D
U
U
U
U
U
UN3TS
DiTE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug,
ug,
ug,
ug,
ug;
ug.
ug,
ug,
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
Kg
DETECTION
LIMIT
0.4
0.1
0.3
1.6
0.2
0.014
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANikLYZED
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/25/95
10/
10/
10/
10/
10/
10/
10/
10/
10/
10/
10/
10/
10/
10/
10/
10/
18/95
L8/95
18/95
18/95
18/95
18/95
18/95
L8/95
18/95
18/95
18/95
18/95
18/95
L8/95
L8/95
L8/95
BY
KWB
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
3050
6010
6010
6010
6010
6010
7471
8270
Page tt: 19
'Iovember3, 1995 13:36
imple ID: GD #75, 5 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9509043-06A CoUected: 09/20/95 10:02:00
SST
uni-Volatile Organics
4-dichlorophenol
2,4-trichlorobenzene
iphthalene
-chloroaniline
jxachlorobutadiene
-chloro-3-methylphenol
-methylnaphthalene
3xachloroc:yclopentadiene
,4,6-trichlorophenol
.4,5-trichlorophenol
-chloronaphthalene
-nitroemiline
Imethylphthalate
:enaphthylene
-nitroaniline
:enaphthene
,4 -dinitrophenol
-nitrophenol
Lbenzofuran
,6-dinitrotoluene
,4-dinitrotoluene
iethyIphthalate
-chlorophenyl-phenylether
Luorene
-nitroaniline
,6-dinitro-2-methylphenol
-nitrosodiphenylamine
-bromophenyl-phenylether
axachlorobenzene
antachlorophenol
tienemthrene
jithracene
d-n-butylphthalate
luoranthene
yrene
lutylbenzyIphthalate
lenzo (a) emthracene
,3'-dichlorobenzidine
is(2-ethylhexyl)phthalate
hrysene
i-n-octylphthalate
enzo(b)fluoranthene
enzo(k)fluoranthene
enzo(a)pyrene
ndeno(1,2,3 -cd)pyrene
ibenz(a,h)anthracene
2nzo(g,h, Dperylene
RESULT
U
u
u
u u o
u
u
u
u
u
a u
u
u
u
u
U
u D
0
u
u
u u u
u
u
u u
u u
346
u u
u
u
u
u
u u
u u
u
u
u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
. 330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
Page tt: 20 •
November 3, 1995 13:36 CERTIJ^ICATE OF AN^LLYSIS
RiSULTS BY SAMPLE.
Sample ID: GD #75, 5 FT. #625 lab ID: 9509043-06A CoUected: 09/20/95 10:02:00
TEST
Semi-Volatile Organics
Volatile Organics
benzene
bromobenzene
bromochlorome thane
bromodi chloromethane
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
^^^orobenzene
^^^oroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
RESULT
Surrogate
UNJTS
/Recovery Data
Surrogate
2 -fluorophenol
phenol -d5
nitrobenzene-d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl •
1,2-dibromo-3-chloropropan
1,2-dibromoethane
dibromometheme
dichlorodif1uorometheme
1,1-dichloroetheme
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropeme
2,2-dichloropropeme
1,l-dichloropropene
cis-1,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
•dl4
U
U
U
U
U
U
U
U
U
U
u
u
u u
u
u u
u
u u
u
u u u
u
u
u
. u
u
u
u
u
u
u
u
u
u u
u
u
ug/Kg
ug/Kg
ug.'Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug.'Kg
ug/'Kg
ug;'Kg
ug,'Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/ Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
ANi^LYZED BY METHOD/CAS#
SW-846, 8270
For Semi-Volatile Organics 8270S
%Recovery
32
33
36
35
41
61
.81
.17
.05
.81
.86
.92
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
• Page tt: 21
November 3, 1995 13:36 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #75, 5 FT. #625 Lab ID: 9509043-06A CoUected: 09/20/95 10:02:00
TEST
Volatile Organics
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentemone
2 -hexanone
fluorobenzene
chlorobenzene-d5
l,4-dichlorobenzene-d4
RESULT
5
U
U
U
U
U
U
u u u .9J
U
U
U
U
U
U
U
U
u u u D
U
529135
304526
125845
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorometheme
1,2-dichloroethane-d4
toluene-d8
bromof1uorobenzene
%Recovery
82.8
83.5
123
102 •
METHOD/CAS#
SW-846,8260A
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1 ^^
591-78-6 ^B
INTSTDl ^^
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Sample ID: GD #75, 10 FT. #625 Lab ID: 9509043-07A CoUected: 09/20/95 10:35:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Boron
Cadmium
Chromium
10/05/95
4.67
U
11.4
DATE
ug/g
ug/g
ug/g
0.4
0.1
0.3
10/05/95
10/11/95
10/11/95
10/11/95
KWB
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
Page tt: 22 •
November 3, 1995 13:36
Sample ID: GD #75, 10 FT. #625
CERTIFICATE OF AI^J^^LYSIS
RESULTS BY SAMPLE
Jab ID: 9509043-07A CoUected: 09/20/95 10:35:00
TEST
Lead
Silver
Mercury
Seml-Volatlle Organics
phenol
bis(2-chloroethyl)ether
2-chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroe theme
nitrobenzene
isophorone
2-nitrophenol
^^4 - dimethylphenol
^^B (2 - chloroethoxy) metheme
^^^ -dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4 -chloroani1ine
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroemiline
dimethylphthalate
acenaphthylene
3-nitroemiline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofurem
2,6-dinitrotoluene
2,4-dinitrotoluene
di e thyIphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroemiline
4,6-dinitro-2-methyIphenol
n-ni trosodiphenylamine
4 -bromopheny1-phenylether
hexachlorobenzene
RESULT
u
u
u
u u
u
u u
u
u
u u u u u u
u u u u u u
u u u
u u u u u u u
u u u
u u u u u
u u u u u u
u u
UNETS
uj/g
uj/g
uj/g
uc
uc
uc
uc
uc
uc
uc
uc
uc
uc
uc
uc
uc
uc
uc
uc
uc
uc
uc
uc
/Kg
/Kg
/Kg
/Kg
/Kg
/Kg
/Kg
/Kg
/Kg
/Kg
/Kg
/Kg
/Kg
/Kg
/Kg
/Kg
/Kg
/Kg
/Kg
/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc/Kg
uc /Kg
uo/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug /Kg
DETECTION
LIMIT
1.6
0.2
0.011
33,0
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
i\NALYZED
10/11/95
10/11/95
10/25/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
BY
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JHA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
• Page tt: 23
November 3, 1995 13:36
Sample ID: GD #75, 10 FT. #625
CERTIFICATE OF ANALYSIS
RESUI.TS BY SAMPLE
LabH): 9509043-07A CoUected: 09/20/95 10:35:00
TEST
Semi-Volatile Organics
pentachlorophenol
phenemthrene
emthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a) emthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthaiate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3 -cd)pyrene
dibenz(a,h) emthracene
benzo(g,h,i)perylene
Volatile Organics
benzene
bromobenz ene
bromochlorometheme
bromodi chloromethane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorometheme
2-chlorotoluene
4-chlorotoluene
dibromochloromethane
RESULT
U
U
U
U
U
U
U
u u u
u u u u u D
u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2-fluorophenol
phenol -ds nitrobenzene -d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
1,2 -dibromo-3 -chloropropem
1,2-dibromoetheme
dibromometheme
dichlorodifluorometheme
u u a
u u u u
u
u
u u
u
u u u u u u u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270S
%Recovery
34.37
34.57
33.95
33.01
39.35
62.81
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits ^^
25
24
23
30
19
18
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
V
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
Page tf: 24
November 3, 1995 13:36 CERTIFICATE OF ATM^O^YSIS
I , RESULTS BY SAMPLE
Sample ID: GD #75, 10 FT. #625 Lab ID: 9509043-07A CoUected: 09/20/95 10:35:00
TEST
Volatile Organics
1,1-dichloroetheme
1,2-dichloroe theme
1,1-dichloroethene
cis-1,2-dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis-l,3-dichloropropene
trans -1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
jl^rene
•H| ,1,2- tetrachloroetheme
^W ,2,2- tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentanone
2-hexemone
fluorobenzene
chlorobenzene-dS
1,4 -dichlorobenzene-d4
RESULT
U
U
u
u u
u
u u u
u u u u u u u u
u u u
u u u u u u
u
u u
u
u u
u u
u u u u 5.0 J
u u
u 214790
74265
24052
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
iOTALYZED
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
laSR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorome thane
1,2-dichloroethane-d4
%Recovery
64.7
41.5 Q
METHOD/CAS#
SW-846,8260A
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
TO 112
TO 121
Page tt: 25
November 3, 1995 13:36 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #75, 10 FT. #625 Lab ID: 9509043-07A CoUected: 09/20/95 10:35:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
toluene-d8
bromofluorobenzene
164 Q
105
85.6 TO 143
80.6 TO 130
SW-846,8260A
Sample ID: GD #38, 5 FT. #625 LabID: 9509043-08A CoUected: 09/20/95 11:28:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Seml-Volatlle Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis (2-chloroethoxy)metheme
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4 -chloroani1ine
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachloroc:yclopentadiene
10/05/95
6.54
U
19.7
U
U
U
U
U
U
U
U
U
u
u
u u
u ' u
u u u u u u u u u u 0
D
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.4
0.1
0.3
1.6
0.2
0.012
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/25/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
KWB
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
Page ff: 26 •
November 3, 1995 13:36 CERTIFICATE OF ANi^LYSIS
. RESULTS BY SAMPLE
Sample ID: GD #38, 5 FT. #625 LabID: 9509043-08A CoUected: 09/20/95 11:28:00
TEST
Seml-Volatlle Organics
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroemiline
dimethylphthalate
acenaphthylene
3-nitroemiline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofurem
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroaniline ~
4,6-dinitro-2-methyIphenol
n-nitrosodiphenylamine
4 -bromophenyl-phenylether
hexachlorobenzene
^^vitachlorophenol
fl^^nemthrene
emthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3 -cd)pyrene
dibenz(a,h)anthracene
benzo(g,h, Dperylene
RESULT
218
•
Surrogate/Re
Surrogate
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
u u
u
u
u u
D
u
u u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
icovery Data
2 -fluorophenol
phenol -d5
nitrobenzene -d5
2 -fluorobiphenyl
2,4,6-
terphe
tribromophenol
nyl-dl4
DETECTION
LIMIT
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
J^NALYZED
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
10/18/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Seml-Volatlle Organics 8270S
%Recovery
37.67
35.55
36.65
35.79
40.92
61.26
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
• Page tt: 11
November 3, 1995 13:36 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #38, 5 FT. #625 LabID: 9509043-08A CoUected: 09/20/95 11:28:00
TEST
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodi chlorometheme
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropan
1,2-dibromoetheme
dibromometheme
di chlorodi fluorometheme
1,1-di chloroetheme
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropeme
2,2-dichloropropane
1,1 -dichlorcjpropene
cis-1,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propyIbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroetheme
trichloroethene
RESULT
U
u
u
u
u
u
u
u u
u u
u
u
u
u u
u u u u
u
u
u
u
u
u
u
u
u u
u u u u u
u
u u
u
u
u
u
u
u u
u
u
u u
3.4J
u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
BY
MMR
MMR
MMR
MMR
MMR
jmR
MMR
MMR
MMR
MMR
MMR
. MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3 j^^
107-06-2 ^B
75-35-4 ^^
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
Page tt: 28 •
November 3, 1995 13:36
•
Sample ID: GD #38, 5 FT. #625
CERTIFICATE OF ANi^kLYSIS
RESULTS BY SAMPLE
LabID: 9509043-08A CoUected: 09/20/95 11:28:00
TEST
Volatile Organics
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
U
u
u u u u u u u u
u 516519
298359
118513
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
AN.\LYZED
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
Surrogate/Recovery Data For Volatile Organlci
Surrogate
dibromofluoromethane
1,2-dichloroetheme-d4
toluene-d8
1^^ bromofluorobenzene
%Recovery
87.2
87.4
120
109
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
9 8260S
METHOD/CAS#
SW-846,8260A
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD 2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Sample ID: GD #38, 5 FT. #625 DUP. LabID: 9509043-09A CoUected: 09/20/95 11:28:00
TEST
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodichloromethane
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3-chloropropem
1^-dibromoethane
RESULT
U
u u u D
U
U
U
U
U
U
U
u u u u u u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANiiLYZED
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
Page tt: 29
November 3, 1995 13:36 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #38, 5 FT. #625 DUP. LabID: 9509043-09A CoUected: 09/20/95 11:28:00
TEST
Volatile Organics
dibromometheme
dichlorodifluorometheme
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-di chloroethene
trans-1,2-dichloroethene
1,2 -dicrhloropropeme
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis-1,3 -dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
t r i chloroethene
trichlorofluorometheme
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
u u u u u
u u u
u u
u
u u
u u u
u u
u
u
u u
u u u u u u u u 6. 7 J
u
u u
u
u n u u u u u u
u 428195
243960
96272
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3 ^^
103-65-1 ^B
100-42-5 ^W
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Page tt: 30
November 3, 1995 13:36 CERTIFICATE OF APs[^lLYSIS
RESULTS BY SAMPLE
Sample ID: GD #38, 5 FT. #625 DUP. LabID: 9509043-09A CoUected: 09/20/95 11:28:00
TEST RESULT UNITS DETECTION AN.IkLYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Surrogate/Recovery-
Surrogate
dibromofluoromethane
1,2 -dichloroetheme-d4
toluene-d8
bromofluorobenzene
Data For Volatile
%Reoovery
83.5
85.6
118
108
SW-846,8260A
Organics 8260S
Recovery Limits
58.4 TO 112
53.3 TO 121
85.6 TO 143
80.6 TO 130
Sample ID: GD #36, 5 FT. #625 LabID: 9509043-lOA CoUected: 09/20/95 13:15:00
TEST
Acid Digestion
Boron
A^^dmlum
Chromium
Lead
Silver
Mercury
Semi-Volatile Organica
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethcme
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)metheme
2,4-dichlorophenol
1,2,4-trichlorobenzene
^iphthalene
RESULT
10/05/95
6.
0.
24
61
38
r.5
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
U
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.4
0.1
0.3
1.6
0.2
0.014
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
AN.ilLYZED
10/05/95
10/11/95
10/11/95
10/11/95
10/11/95
10/11/95
10/25/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
BY
KWB
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
Page tt: 31
November 3, 1995 13:36 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #36, 5 FT. #625 LabID: 9509043-lOA CoUected: 09/20/95 13:15:00
TEST RESULT
Seml-Volatlle Organics
4-chloroemiline
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachloroc:yclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroemiline
dimethylphthalate
acenaphthylene
3-nitroaniline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofurem
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4 -ni troani1ine
4,6-dinitro-2-methyIphenol
n-ni trosodipheny1amine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenemthrene
anthracene
di-n-butylphthalate
fluoremthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoremthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3 -cd)pyrene
dibenz(a,h) emthracene
benzo (g,h, Dperylene
Surrogate/Re
Surrogate
U
U
U
U
U
u u u u u
u u u u u u u u u u
u u u u u u u u u u u u u D
u u
a
u u u
u u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
covery Data
2-fluorophenol
phenol-d5
nitrobenzene -d5
DETECTION
LIMIT
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330 •
330
330
330
330
330
330
330
330
330
ANALYZED
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06 £^
534-52-1 flB
86-30-6 ^^
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Seml-Volatlle Organics 8270S
%Recovery
24.27
22.52
24.31
Recovery Limits
25
24
23
TO 121
TO 113
TO 120
Page tf: 32 •
November 3, 1995 13:36
Sample ID: GD #36, 5 FT. #625
CERTIFICATE OF AI^ikLYSIS
RESULTS BY SAMPLE
•, f,. LabID: 9509043-lOA CoUected: 09/20/95 13:15:00
TEST RESULT UNITS DETECTION J^ALYZED BY
LIMIT
METHOD/CAS#
Semi-Volatile Organics
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodichlorometheme
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
^^bromochlorometheme
fl^P -dibromo-3 -chloropropem
i!^ - dibromoetheme
dibromomethane
dichlorodifluorometheme
1,1-dichloroetheme
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2 -dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis-1,3 -dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
t^^uene
U
U
U
U
U
U
U
U
D
U
U
D
U
U
U
U
U
U
U
U
u u u u u u u
u
u
u
u u u u u u
u u
u u u u u u u u u
ug/Kg
ug/Kg -
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
26.25
36.77
61.74
10
10
lb
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
30
19
18
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
Page tt: 33
November 3, 1995 13:36 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #36, 5 FT. #625 LabID: 9509043-lOA CoUected: 09/20/95 13:15:00
TEST
Volatile Organics
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentemone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4 -di chlorobenzene-d4
RESULT
U
U
5.0 J
U
U
U
U
U
a
u
u
u u
u
u
u 554161
305278
112604
Surrogate/Re<
Surrogate
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
covery Data For Volatile Organics 8260S
dibromofluorometheme
1 ,2 -dichloroethane-d4
toluene-d8
bromofluorobenzene
%Recovery
85.0
83.3
124
107
METHOD/CAS#
SW-846,8260A
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
^
Recovery Limits ^^F
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Sample ID: GD #36, 10 FT. #625 LabID: 9509043-11A CoUected: 09/20/95 13:25:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
10/10/95
5.31
U
12.5
U
U
U
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
0.4
0.1
0.3
1.6
0.2
0.0092
10/10/95
10/13/95
10/13/95
10/13/95
10/13/95
10/13/95
10/25/95
SJM
LVD
LVD
LVD
LVD
LVD
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
7471
Page tt: 34 •
November 3, 1995 13:36
Sample ID: GD #36, 10 FT. #625
CERTIFICATE OF AN^^YSIS
RESULTS BY SAMPLE
LabID: 9509043-llA CoUected: 09/20/95 13:25:00
TEST RESULT UNITS DETECTION i^NALYZED BY
LIMIT
METHOD/CAS#
Seml-Volatlle Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethcme
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)metheme
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4-chloroemiline
hexachlorobutadiene
^^chloro-3 -methylphenol
fl^fliethylnaphthalene
^^ficachlorocjyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroemiline
dimethylphthalate
acenaphthylene
3-nitroemiline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dini trotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroaniline
4,6-dinitro-2-methylphenol
n-nitrosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenanthrene
anthracene
di-n-butylphthalate
f luoremthene
pyrene
butyIbenzyIphthalate
u D
U
U
O
u u u u u
u u u u u u u u u u u. u u
u u u
u u u u u D
u u
u D
u
u
u
u u
u u u u u u u 172 J
u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg -
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
SW-846, 8270
10/19/95 JMA 108-95-2
10/19/95 JMA 111-44-4
10/19/95 JMA 95-57-8
10/19/95 JMA 541-73-1
10/19/95 JMA 106-46-7
10/19/95 JMA 95-50-1
10/19/95 JMA 95-48-7
10/19/95 JMA 108-60-1
10/19/95 JMA 106-44-5
10/19/95 JMA 621-64-7
10/19/95 JMA 67-72-1
10/19/95 JMA 98-95-3
10/19/95 JMA 78-59-1
10/19/95 JMA 88-75-5
10/19/95 JMA 105-67-9
10/19/95 JMA 111-91-1
10/19/95 JMA 120-83-2
10/19/95 JMA 120-82-1
10/19/95 JMA 91-20-3
10/19/95 JMA 106-47-8
10/19/95 JMA 87-68-3
10/19/95 JMA 59-50-7
10/19/95 JMA 91-57-6
10/19/95 JMA 77-47-4
10/19/95 JMA 88-06-2
10/19/95 JMA 95-95-4
10/19/95 JMA 91-58-7
10/19/95 JMA 88-74-4
10/19/95 JMA 131-11-3
10/19/95 JMA 208-96-8
10/19/95 JMA 99-09-2
10/19/95 JMA 83-32-9
10/19/95 JMA 51-28-5
10/19/95 JMA 100-02-7
10/19/95 JMA 132-64-9
10/19/95 JMA 606-20-2
10/19/95 JMA 121-14-2
10/19/95 JMA 84-66-2
10/19/95 JMA 7005-72-3
10/19/95 JMA 86-73-7
10/19/95 JMA 100-01-06
10/19/95 JMA 534-52-1
10/19/95 JMA 86-30-6
10/19/95 JMA 101-55-3
10/19/95 JMA 118-74-1
10/19/95 JMA 87-86-5
10/19/95 JMA 85-01-8
10/19/95 JMA 120-12-7
10/19/95 JMA 84-74-2
10/19/95 JMA 206-44-0
10/19/95 JMA 129-00-0
10/19/95 JMA 85-68-7
Page tt: 35
November 3, 1995 13:36
Sample ID: GD #36, 10 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9509043-llA CoUected: 09/20/95 13:25:00
TEST
Seml-Volatlle Organics
benzo(a) emthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoremthene
benzo(k)fluoremthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h)anthracene
benzo(g,h,i)perylene
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chloromethane
bromoform
bromcjme theme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
RESULT
U
U
u u u
u u u
u
u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -fluorophenol
phenol -d5
nitrobenzene -d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
1,2-dibromo-3 -chloropropem
1,2-dibromoetheme
dibromometheme
di chlorodifluorometheme
1,1-dichloroethane
1,2 -di chloroetheme
1,1-dichloroethene
cis-1,2 -dichloroethene !
t rans-1,2 -di chloroethene
1,2-dichloropropeme
1,3-dichloropropeme
.
u u u
u
u
u
n
u u u u u
u
u u
u u u u
u u u
u
u
u u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270S
%Recovery
26.48
27.65
27.49
27.90
36.35
57.49
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
IMMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
A SW-846, 8260A ^^
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
Page tt: 36
>a!i^] le ID: GD #36, 10 FT. #625
CERTIFICATE OF ANAI.YSIS
RESULTS BY SAMPLE
LabID: 9509043-llA CoUected: 09/20/95 13:25:00
TEST
Volatile Organics
2,2-dichloropropane
1,l-dichloropropene
cis-1,3 -dichloropropene
trans-1,3 -di chloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4 -diczhlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene cliloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3 -tri chlorobenz ene
1,2,4-trichlorobenzene
1,1,l-trichloroethane
1 j^jl^ - tric:hloroe theme
tjIBloroe thene
tnlRlorof luorometheme
1,2,3- tric:hloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl- 2-pentanone
2 -hexanone
fluorobenzene
chlorobenz ene-d5
1,4 -di chlorobenzene-d4
RESULT
5
5,
U
U
U
U
U
U
U
U
U
n
u
u D
u D
U
U
U
U
U
u
.6J
U
D
U
U
U
U
D
U
U
.4J
U
D
U
400261
226308
98872
Surrogate
Surrogate
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10 -
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANAI.YZED
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/02./95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
(/Recovery Data For Volatile Organics 8260S
dibromofluoromethane
1,2-di chloroethane-d4
toluene-d8
bromofluorobenzene
%Recovery
74.7
72.5
125
100
METHOD/CAS#
SW-846,8260A
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Page #: 37
November 3, 1995 13:36 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #36, 10 FT. #625 DUP. LabID: 9509043-12A CoUected: 09/20/95 13:25:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Semi-Volatile Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis (2-chloroisopr(3pyl) ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
iscjphorone
2 -nitrcjphenol
2,4-dimethylphenol
bis(2-chloroethoxy)metheme
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4 -chloroemiline
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6- tric:hlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroaniline
dimethylphthalate
acenaphthylene
3-nitroaniline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofurem
2,6-dinitrotoluene
2,4-dinitrotoluene
di e thyIphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroemiline
4,6-dinitro-2-methylphenol
n-ni trosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenemthrene
anthracene
di-n-butylphthalate
fluorem thene
pyrene
butylbenzylphthalate
u u u u u u u u u u u u u u
u u
u u
u u
u u
u
u
u u
u u
u
u u u u D
u u u u u u D
u u u u
u u
u u u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8270
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
Page tt: 38 9
November 3, 1995 13:36
•
CERTIFICATE OF Al^^^LYSIS
1' RESULTS BY SAMPILEI
Sample ED: GD #36, 10 FT. #625 DUP. Lab ID: 9509043-12A CoUected: 09/20/95 13:25:00
TEST REStJLT
Semi-Volatile Organics
benzo(a) emthracene U
3,3'-dichlorobenzidine U
bis(2-ethylhexyl)phthalate U
chrysene U
di-n-octylphthalate U
benzo(b)fluoremthene D
benzo(k)fluoremthene U
benzo(a)pyrene U
indeno(1,2,3-cd)pyrene U
dibenz(a,h) emthracene U
benzo (g,h, Dperylene U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -fluorophenol
phenol-d5
nitrobenzene-d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
DETECTION
LIMIT
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Seml-Volatlle Organics 8270S
%Recovery
38.48
35.91
37.26
35.85
36.33
55.71
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
Sample ID: GD #189, 5 FT. #625 LabID: 9509043-13A CoUected: 09/20/95 13:50:00
TEST
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Seml-Volatlle Organics
phenol
bis(2 -chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
RESULT
10/10/95
1.
0.
IE
91
37
i.3
U
U
U
U
U
U
U
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.4
0.1
0.3
1.5
0.2
0.014
330
330
330
330
J^ALYZED
10/10/95
10/13/95
10/13/95
10/13/95
10/13/95
10/13/95
10/25/95
10/19/95
10/19/95
10/19/95
10/19/95
BY
SJM
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
541-73-1
3050
6010
6010
6010
6010
6010
7471
8270
Page tt: 39
November 3, 1995 13:36 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #189, 5 FT. #625 Lab ID: 9509043-13A CoUected: 09/20/95 13:50:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Seml-Volatlle Organics
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propyleunine
hexachloroetheme
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4 -chloroani1ine
hexachlorobutadiene
4-chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroemiline
dimethylphthalate
acenaphthylene
3 - ni troemi 1 ine
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofurem
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroaniline
4,6-dinitro-2-methylphenol
n-ni trosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenemthrene
anthracene
di-n-butylphthalate
fluoremthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis (2-ethylhexyl)phthalate
chrysene
u
u u u u
u
u u
u u u
u
u u u u u u
u u
u u u
u u u u D
u u u u u u u
u u u u u u n u
u
u D
u u u u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8270
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
Page tf: 40
November 3, 1995 13:36 CERTIFICATE OF ANALYSIS
, RESULTS BY SAMPLE
Sample ID: GD #189, 5 FT. #625 LabID: 9509043-13A CoUected: 09/20/95 13:50:00
TEST
Semi-Volatile Organics
di-n-octylphthalate
benzo(b)fluoremthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h)anthracene
benzo(g,h,i)perylene
RESULT
u
u
u
u
u
u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2-•fluorophenol
phenol -d5
nitrobenzene
2-
2,
-d5
•fluorobiphenyl
,4,6-tribromophenol
terphenyl-dl4
Volatile Organics
benzene
^Juromobenzene
fl^nmochlorome theme
Mromodi chl orome thane
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3 -chloropropem
1,2-dibromoetheme
dibromome theme
dichlorodifluorcjme thane
1,1-dichloroethane
1,2 -di chloroe theme
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropane
2,2-dichloropropeme
1,l-dichloropropene
cis-1,3-dichloropropene
!
trans-1,3-dichloropropene
«
U
U
u
u
u u u u u u u n u U
D
u u u u u u u u u u D
u
u u u
u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
.MiFALYZED
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Seml-Volatlle Organics 8270S
%Recovery
39.68
36.51
38.76
36.01
35.73
55.13
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
Page tt: 41
November 3, 1995 13:36 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #189, 5 FT. #625 LabID: 9509043-13A CoUected: 09/20/95 13:50:00
TEST
Volatile Organics
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
RESULT
u u u u u u u u
u u
u 1,1,1,2-tetrachloroetheme U
1,1,2,2-tetrachloroetheme D
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroethane
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentemone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
u
u u
u 4.1 J
u u u u
u u u u
u D
u
u u 402570
240499
106920
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
msR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorometheme
] .,2 -di chloroetheme-d4
toluene-d8
bromofluorobenzene
%Recovery
80.7
77.5
120
101
METHOD/CAS#
SW-846,8260A
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4 ^^
95-63-6 ^B
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Page tt: Al
November 3, 1995 13:36
Sample ID: GD #189,10 FT. #625
CERTIFICATE OF AN^kLYSIS
RESULTS BY SAMPLE
LabID: 9509043-14A CoUected: 09/20/95 14:05:00
TEST RESULT UNITS DETECTION AN.\LYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
^2-dichlorobenzene
^Bte thy Iphenol
^101 (2-chloroisopropyl) ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroetheme
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4-chloroaniline
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocryclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroemiline
dimethylphthalate
acenaphthylene
3-nitroaniline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofurem
2,6-dinitrotoluene
^1^- dinitrotoluene
10/10/95
7.62
0.39
10.8
0
U
U
U
U
U
U
U
U
U
U
U
U
n
u
u
u
D
u
u u u
u
u
u
u
u
u u
u
u u
u
u u
u
u
u
u
u
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.4
0.1
0.3
1.6
0.2
0.012
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
10/10/95
10/13/95
10/13/95
10/13/95
10/13/95
10/13/95
10/25/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
SJM
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
3050
6010
6010
6010
6010
6010
7471
8270
Page tt: 43
November 3, 1995 13:36
Sample ID: GD #189,10 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9509043-14A CoUected: 09/20/95 14:05:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Seml-Volatlle Organics
diethylphthalate U ug/Kg 330 10/19/95 JMA
4-chlorophenyl-phenylether U ug/Kg 330 10/19/95 JMA
fluorene U ug/Kg 330 10/19/95 JMA
4-nitroaniline U ug/Kg 660 10/19/95 JMA
4,6-dinitro-2-methylphenol U ug/Kg 330 10/19/95 JMA
n-nitrosodiphenylamine U ug/Kg 330 10/19/95 JMA
4-bromophenyl-phenylether U ug/Kg 330 10/19/95 JMA
hexachlorobenzene U ug/Kg 330 10/19/95 JMA
pentachlorophenol U ug/Kg 1700 10/19/95 JMA
phenanthrene U ug/Kg 330 10/19/95 JMA
anthracene U ug/Kg 330 10/19/95 JMA
di-n-butylphthalate 103 J ug/Kg 330 10/19/95 JMA
fluoranthene U ug/Kg 330 10/19/95 JMA
pyrene U ug/Kg 330 10/19/95 JMA
butylbenzylphthalate U ug/Kg 330 10/19/95 JMA
benzo(a)anthracene U ug/Kg 330 10/19/95 JMA
3,3'-dichlorobenzidine U ug/Kg 330 10/19/95 JMA
bis(2-ethylhexyl)phthalate U ug/Kg 330 10/19/95 JMA
chrysene U ug/Kg 330 10/19/95 JMA
di-n-octylphthalate U ug/Kg 330 10/19/95 JMA
benzo(b)fluoranthene U ug/Kg 330 10/19/95 JMA
benzo(k)fluoranthene U ug/Kg 330 10/19/95 JMA
benzo(a)pyrene U ug/Kg 330 10/19/95 JMA
indeno(1,2,3 -cd)pyrene U ug/Kg 330 10/19/95 JMA
dibenz(a,h)anthracene U ug/Kg 330 10/19/95 JMA
benzo(g,h, Dperylene U ug/Kg 330 10/19/95 JMA
SW-846, 8270
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
•9
•0
•2
•9
218-01-
117-84-
205-99-
207-08-
50-32-8
193-39-5
53-70-3
191-24-2
Surrogate/Recovery Data For Semi-Volatile Organics 8270S
Surrogate %Recovery
2-fluorophenol 24.96
phenol-d5 25.20
ni trobenzene-d5 23.97
2-fluorobiphenyl 24.23
2,4,6-tribromophenol 32.76
terphenyl-dl4 54.27
Recovery Limits
25 TO 121
24 TO 113
23 TO 120
30 TO 115
19 TO 122
18 TO 137
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chlorometheme
bromoform
bromome theme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
U
D
U
U
U
U
U
U
U
U
U
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
SW-846,8260A
10/03/95 MMR 71-43-2
10/03/95 MMR 108-86-1
10/03/95 MMR 74-97-5
10/03/95 MMR 75-27-4
10/03/95 MMR 75-25-2
10/03/95 MMR 74-83-9
10/03/95 MMR 104-51-8
10/03/95 MMR 135-98-8
10/03/95 MMR 98-06-6
10/03/95 MMR 56-23-5
10/03/95 MMR 108-90-7
10/03/95 MMR 75-00-3
10/03/95 MMR 67-66-3
Page if: AA
>Iovember 3, 1995 13:36
, ample ID: GD #189, 10 FT. #625
CERTIFICATE OF ANAL.YSIS
.^ RESULTS BY SAMPLE
LabID: 9509043-14A CoUected: 09/20/95 14:05:00
EST
3latile Organics
1 ilorometheme
-chlorotoluene
1 -chlorotoluene
ibromochlorometheme
' ,2 -dibromo- 3 -chloropropem
,2-dibromoetheme
Ibromome theme
, ichlorodifluorometheme
|,1-dichloroethane
,2-dichloroethane
,1-dichloroethene
LS-l>2-dichloroethene
rans-1,2-dichloroethene
,2-dichloropropane
,3-dichloropropane
,2 -dichloropropeme
,l-dichloropropene
is-1,3-dichloropropene
rans-1,3-dichloropropene
,2-dichlorobenzene
,3-dichlorobenzene
, 4-gUchlorobenzene
th'jIBnzene
2X^M orobutadi ene
sopropylbenzene
-isopropyltoluene
athylene chloride
aphthalene
-propylbenzene
tyrene
,1,1,2-tetrachloroethane
,1,2,2-tetrachloroetheme
etrachloroethene
oluene
,2,3-trichlorobenzene
,2,4-trichlorobenzene
,1,1-trichloroethane
,1,2-trichloroetheme
richloroethene
richlorofluoromethane
,2,3- trichlorcspropeme
,2,4-trimethylbenzene
,3,5-trimethylbenzene
inyl chloride
-xylene
,p-xylene
cetone
-butanone
-methyl-2-pentanone
-hexemone
luorobenzene
tilorobenzene - d5
RESULT
U
u u u u
u u o u u u u u u
u u u u u u u u u
u u u u u u u u D
u a u u 4.2J
o u u o
u u u u u u u u u 498731
289037
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALY2'.ED
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2 orob€
Page tt: 45
November 3, 1995 13:36
Sample ID: GD #189, 10 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9509043-14A CoUected: 09/20/95 14:05:00
^
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
1,4 -di chlorobenzene -d4 116588 ug/Kg
Surrogate/Recovery
Surrogate
dibromofluoromethane
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
SW-846,8260A
10/03/95 MMR INTSTD3
Data For Volatile
%Recovery
81.5
72.9
121
106
Organics 8260S
Recovery Limits
58.4 TO 112
53.3 TO 121
85.6 TO 143
80.6 TO 130
Sample ID: GD #147, 5 FT. #625 Lab ID: 9509043-15A CoUected: 09/20/95 14:29:00
TEST
Acid Digestion
Boron
Cadmium
Chromiuni
Lead
Silver
Mercury
Seml-Volatlle Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)metheme
RESULT
10/10/95
4.80
0.56
12.4
U
U
U
V
U
U
• O
U
U
U
U
U
U
U
u u
u u
u
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.4
0.1
0.3
1.6
0.2
0.014
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
10/10/95
10/13/95
10/13/95
10/13/95
10/13/95
10/13/95
10/25/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
BY
SJM
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846.
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
3050
6010 ^B
6010
6010
6010
6010
7471
8270
Page #: 46 o
November 3, 1995 13:36 CERTIFICATE OF AN^U^YSIS
RESULTS BY SAMPLE
Sample ID: GD #147, 5 FT. #625 Lab ID: 9509043-15A CoUected: 09/20/95 14:29:00
TEST
Semi-Volatile Organics
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4-chloroemiline
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroemiline
dimethylphthalate
acenaphthylene
3-nitroemiline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofurem
2,6-dinitrotoluene
2,4-dinitrotoluene
j^e thy Iphthalate
flBehlorophenyl -phenylether
^Wuorene
4-nitroaniline
4,6-dinitro-2-methylphenol
n-nitrosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenemthrene
emthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoremthene
benzo(k)fluoremthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h)anthracene
benzo(g,h, Dperylene
RESULT
u
u u
u u
u u u u u u u u
u u u u u u u u u u u u u u
u u u a u u u u D
u u u
u
u u u u
u D
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
Page tt: Al
November 3, 1995 13:36
Sample ID: GD #147, 5 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9509043-15A CoUected: 09/20/95 14:29:00
TEST
Seml-Volatlle Organics
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodichlorometheme
bromoform
bromome thane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetracdiloride
chlorobenzene
chloroetheme
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
RESULT UNITS
Surrogate/Recovery Data
Surrogate
2-fluorophenol
phenol -d5
nitrobenzene -d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
1,2-dibromo-3 -chloropropem
1,2-dibromoethane
dibromometheme
dichlorodifluoromethane
1,1-dichloroetheme
1,2-dichloroethane
1,1-dichloroethene
cis-1,27dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropeme
2,2-dichloropropeme
1,1-dichloropropene
cis-1,3 -dichloropropene
trans-1,3-dichloroprop
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
i sopropylbenzene
4 -isopropyltoluene
methylene chloride
)ene
U
U
U
U
U
U
U
U
U
U
U
u u u u u u u
u u u u u D
u u u
u u u u
u u u u u
u u
u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
ANALYZED BY METHOD/CAS#
SW-846, 8270
For Semi-Volatile Organics 8270S
%Recovery
14
14
14
16
28
49
.11
.92
2 Q
7 Q
.13
.76
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5 ^^
108-90-7 ^B
75-00-3 ^^
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
Page ft: 48
November 3, 1995 13:36
#
Sample ID: GD #147, 5 FT. #625
CERTIFICATE OF A^J^^LLYSIS
RESULTS BY SAMPLE
Lab ID: 9509043-15A CoUected: 09/20/95 14:29:00
TEST
Volatile Organics
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
^^cethyl - 2 -pentanone
IBIexemone
Iffuorobenzene
chlorobenzene-d5
1,4-dichlorobenzene- d4
RESULT
4
U
U
U
u u
u u
u u .9J
U
u u u
u u
u u
u
u u u u 344302
203853
94558
Surrogate
Surrogate
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANJLLYZED
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
i/Recovery Data For Volatile Organics 8260S
dibromofluorometheme
1,2-dichloroetheme-d4
toluene-dS
bromofluorobenz* sne
%Recovery
72.8
71.7
124
99.2
METHOD/CAS#
SW-846,8260A
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 13 0
Sample ID: GD #147, 10 FT. #625 LabID: 9509043-16A CoUected: 09/20/95 14:39:00
TEST RESULT UNITS DETECTION ANJLLYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Boron
Cadmium
Chrc omitiffl
10/10/95
4.40
0.39
10.2
DATE
ug/g
ug/g
ug/g
0.4
0.1
0.3
10/10/95
10/13/95
10/13/95
10/13/95
SJM
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
Page ft: 49
November 3, 1995 13:36
Sample ID: GD #147, 10 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9509043-16A CoUected: 09/20/95 14:39:00
•
TEST
Lead
Silver
Meroury
Seml-Volatlle Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroe thcLne
nitrobenzene isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4-chloroeuiiline
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocryclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2-chloronaphthalene
2-nitroaniline
dimethylphthalate
acenaphthylene
3-nitroaniline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofurem
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4-chlorophenyl-phenylether
fluorene
4-nitroemiline
4, 6-dinitro-2-methyIphenol
n-nitrosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
RESULT
U
D
0.01
U
U
U
U
U
U
U
U
u
u u
u u
u u
u u u u u u u
u
u D
u u u u
u u u
u u
u u
u
u u u u u u
u u
UNITS
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
1.6
0.2
0.012
310
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
ANALYZED
10/13/95
10/13/95
10/25/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
BY
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
iJMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9 ^^
111-91-1 flB
120-83-2 ^IW
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
Page tt: 50
November 3, 1995 13:36
Sample ID: GD #147, 10 FT. #625
CERTIFICATE OF ANi^iLYSIS
. RESULTS BY SAMPLE
Lab ID: 9509043-16A CoUected: 09/20/95 14:39:00
TEST RESULT UNITS DETECTION ANJ^YZED BY
LIMIT
METHOD/CAS#
Seni-Volatile Organics
pentachlorophenol
phenanthrene
anthracene
di-n-butylphthalate
fluoremthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis (2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h)anthracene
benzo(g,h,i)perylene
m
w
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chlorometheme
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorometheme
2 -chlorotoluene
4 - cJhlorotoluene
dibromochlorometheme
56
U
u
u BJ
U
U
O
U
U
u
u
u
u o
u
u u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2-fluc
phenol
(rophenol
,-d5
nitrobenzene !-d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terpheny1-dl4
1,2-dibromo-3-chloropropan
1,2-dibromoetheme
dibromometheme
di chlorodi fluorome thane
»
U
u u u u
a u
u
u
u u
u
u
a
u
u
u
u
u u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8270
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270S
%Recovery
105.6
93.52
78.86
83.23
85.76
133.7
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
Page tt: 51
November 3, 1995 13:36 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #147, 10 FT. #625 LabID: 9509043-16A CoUected: 09/20/95 14:39:00
TEST
Volatile Orgabics
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2 -dichloroethene
t rans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropeme
1,1-dichloropropene
cis-1,3 -dichloropropene
trems-1,3 -dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isoprcjpylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroetheme
te t rachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
t ri chloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentanone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
u
u u u
u u u u u u u u D
u u u u u u u u u u u u D
u u 5.4J
U
U
U
U
U
u u
u
u u u u u 469262
294766
124376
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorometheme
1,2-dichloroetheme-d4
%Recovery
85.7
80.8
METHOD/CAS#
SW-846,8260A
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5 J^
630-20-6 IB
79-34-5 ^^
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
TO 112
TO 121
Page tt: 52
November 3, 1995 13:36
Sample ID: GD #147, 10 FT. #625
CERTIFICATE OF AN^U^YSIS
RESULTS BY SAMPLE
Lab ID: 9509043-16A CoUected: 09/20/95 14:39:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/(^AS#
Volatile Organics
toluene-d8
bromofluorobenzene
115
104
85.6 TO 143
80.6 TO 130
SW-846,8260A
Sample ID: GD #38, 10 FT. #625 LabID: 9509043-17A CoUected: 09/20/95 11:40:00
TEST
Acid Digestion
Boron
Cadmium
Chromium
Laad
^Rver
Mercury
Seni-Volatile Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroetheme
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)metheme
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4 -chloroani1ine
hexachlorobutadi ene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
RESULT
10/10/95
3.35
U
11.9
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u u
u
u
u
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.4
0.1
0.3
1.6
0.2
0.013
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
J^ALYZED
10/10/95
10/13/95
10/13/95
10/13/95
10/13/95
10/13/95
10/25/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
BY
SJM
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
Page tt: 53
November 3, 1995 13:36
Sample ID: GD #38, 10 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9509043-17A CoUected: 09/20/95 11:40:00
9
TEST
Seni-Volatile Organics
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroemiline
dimethylphthalate
acenaphthylene
3-nitroemiline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroaniline
4,6-dinitro-2-methylphenol
n - hi t rosodiphenyleunine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenanthrene
anthracene
di-n-butylphthalate
fluoremthene
pyrene
butylbenzylphthalate
benzo(a) emthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoremthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h)anthracene
benzo(g,h, Dperylene
RESULT
U
u u u u
u u u
u u u
u
u u
u u a U
u u u D
u
u 24 BJ
U
U
U
D
U
U
U
U
U
U
U
U
D
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -fluorophenol
phenol -d5
nitrobenzene-d5
2 -fluorobiphenyl
2,4,6-
terphe
tribromophenol
nyl-dl4
DETECTION
LIMIT
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA.
JMA
JMA
JMA
iJMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5 ^^
85-01-8 ^B
120-12-7 ^^
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Seml-Volatlle Organics 8270S
%Recovery
39.00
39.16
29.86
42.81
82.96
132.8
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
Page tf: 54
\
O
November 3, 1995 13:36 CERTIFICATE OF AT^^O^YSIS
RESULTS BY SAMPLE
Sample ID: GD #38, 10 FT. #625 LabID: 9509043-17A CoUected: 09/20/95 11:40:00
TEST
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodichlorometheme
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropem
1,2-dibromoetheme
dibromomethane
di chlorodi f1uoromethane
^^^ - dichloroe theme
^^fl -dichloroe theme
^^1-dichloroethene
cis-l,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis-1,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
RESULT
U
U
u u u u u u V
u u u u
u u u u u u u u u u u u u u
u u u u D
u u u u
a u
u u u u D
u u u
u u u 5.2J
u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
J^ALYZED
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
Page #: 55
November 3, 1995 13:36 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #38,10 FT. #625 LabID: 9509043-17A CoUected: 09/20/95 11:40:00
TEST
Volatile Organics
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentemone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4 -di chlorobenzene-d4
RESULT
U
U
D
U
U
U
U
3.5 J
U
U
U
515605
302939
119894
Surrogate/Recc
Surrogate
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
lb
10
10
10
ANALYZED
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
10/03/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
)very Data For Volatile Organics 8260S
dibromofluorometheme
1 ,2 -dichloroethane-d4
toluene-d8
bromofluorobenzene
%Recovery
81.8
76.5
121
105
METHOD/CAS#
SW-846,8260A
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
A^ IB
Page #: 56 a
#
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identiiied compounds or when the mass sj^ectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1. IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration i-ange but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits. If surrogate recoveries are out
of limits, any values reported are for indication only.
ENVIRONMENTAL LAB WORK REQUEST m-<7^9'/^^'/-
THIOKOL ENVIRONMENTAL LABORATORY LWR No. E1I059
A ^ IUALICC ^ ~>
EXTENSION
6.3'/C
COST CENTER
U'3 40
WORK ORDER
iBf4o
.TE , ^
ORGANIZATION NUILSTOP
B/<^'Uif2X> 3o/c
Ri;PORT RESULTS TO:
HELEN WARD, MS 301
\
/
\
/
\
\
SAMPLE
1. C4-d4-<tt
^-rFr
ll
ll
4 t<y^ ^^
iC ft
,/
ll
7. (c-7l -i'r- t^y
5 I-V
• '
'• If
10. C-rl // i'V
/FT
//
//
DATE
l^'/m
h
II
11
1.'
ll
i
••
TYPE
G
ly
y
F
y
y
• i^
i/
y
y
/
1/
/
c
^
SAMPLE INFORMATION
LOCATION
C5^'/Wf d-Fls"
II
, 1
/'
/ /
/ /
)
/
1
1 1
/
/
TIME
^'^
tl
II
Fo<
tF"^
ff.C
9/<
ll
r/
lODO
ll
ll
TEST
dec- fuc
/Jihzhdn-7/F
8, Cd Cr, 1^, l^b , H^
- S^d ^/
-vc ^/
Sy^ ^ S
Fc-^ ^'
<^r FZ^
Fee //•}
^cr ^1
<./y r^2..
Txir ^^
REMARKS
CHAIN OF CUSTODY
RELINQUISHED BY DATE TIME RECEIVED BY DATE TIME
9^z<r'f\ /<^r .^m^^d T i'Z^- 9F zy/'cF
FOR LABORATORY USE ONLY
U^EC COMPLETED DATE REPORTED
ENVIRONMENTAL LAB WORK REQUEST 9^ 'ZF'Fi/-
«
TinOKOL ENVIRONMENTAL LABORATORY LWR No. n 2L^ S/ZOS'i'
EXTE7JS10N cosTCHnni
00^46
WORK ORDER
yB94^
DATE
ORGANIZATION MAILSTOP
30/F
REPORT RESULTS TO:
HELEN WARD, MS 301
y
/
1
\
\
1 1
\
/
1
\
d
7
\
SAMPLE
5/V
//
//
/LFT
/I
l<
' Cd ^ /zs-
II
, 1
'" Cd d I2T
/D ff
"•
12-
DATE
/'ZS^\
\
TYPE
G
- y
/
y
y
y
y
i/
y
y
y
iZ
F
c
/
SAMPLE INFORMATION
LOCATION
Sto/i^u -4 l^i_-^
i
1
TIME
1040
:l
II
MTO
'I
/>
lltd-
/I
II
//
>i
TEST
iZc'C' 771 ^^
AJ 1 hr u/ly tl-U1^
B, Cd.Cr^A^. ^^,
^^ ^/
%^rF7.
-^r */--^
-^<;edl
'^r -4 2.
sv^ -a 3
^rc 4 f
^r^i^2.
^^4 1
REMARKS
rii'-Fc/'c
//^
1 1
CHAIN OF CUSTODY
Rn,INQUISHEDBY DATE TIME RECEIVED BY DATE TIME
FOR LABORATORY USE ONLY
DATC COMPLETE) DATE REPORTED 1
ENVIRONMENTAL LAB WORK REQUEST ^f/f/^r^
•
TinOKOL ENVIRONMENTAL LABORATORY LWR No. ^/^j5-^
iPSS^ COSTCaWTOl WORK ORDER
9-^r-f^
ORGANIZATION REPORT RESULTS TO:
HELEN WARD, MS 301
,/
/
^ \
F
w
*
\
/
•7
SAMPIX
i\
>i
//ift-
ll
6.
//
' »• &/ ^ Ztf t
9.
//
10.
1/
'RlK<<r. 'Elan
11
fl
DATE
(
9'Z^-4.-
' /i
/
i
t
I
TYPE
3 C
y
\
i
SAMPLE INFORMATION
LOCATION
^LO/HU-H^I^ZF
/
TIME
ll^d
• If
ll
l20t
IFhF
1
IZ4^
tl
TEST
Zc^^- 3Z(y^
"SisZ v.'i-rk^i Av>cj| Ijpiif-Mi
/jjtr/>f)fi\.'y(ij
REMARKS
ur.
•B>,C'^iCr,A^. Ph, Mh
< •)' ' f
'S^tr -id. Z
T^,r ^ 3
:S3^^ ;^/ pl*/
-^^ ^/
-^^ y^^
-S^^ ^3
Fn:.^ 4-1
^c^-^l^
^ii/}^
Cz. 'Bct:ti.s ,
\
// //
CHAIN OF CUSTODY
i^^ 4^3
REUNQUISHED BY DATE TIME RECETVia) BY DATE TIME
4
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED SICNATVRE
ENVIRONMENTAL LAB WORK REQUEST ^fl9F£jF
TinOKOL ENVIRONMENTAL LAOORATORY
EXTENSION
57^0
COSTCaWTUt
\AJ3i-h
LWR No. £/IO^
WORK OROOl
Zr7>94o
i
9-2FFr
ORGANIZATION
JoilZ
RIPORT RESULTS TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS
'^-zr^r' 'Sijotv,!/ **" I^Z^ /j^-r llo A - <^zc,o
fl n 'I -fl AJlh-ahr.yi'ji^^f
la^
/I
^ 4f(.
5fit
il S, CA, Cr,\,f>F d^
/ l( y dM. %t:e-4i
ll y II -^cc^Z-
II II y II %c^^l
II p/> ^ -P-9L->C
CHAIN OF CUSTODY
RHJNQUISIIEDBY DATE TIME RECEIVED BY DATE TIME
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTS) SICNATVRE
November 3, 1995
m
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward MIS 301
Thiokol Corp, Ut 84322
A.F. WALKER
EXT 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs MIS 245
Attn: Dr. Jofm Terry
Tele: 801-863-2384
WorkOrder)}' 9509054
Sample ID:
Sample and Test Code Identifiattion
LabID:
OIA GD
nple lU:
#48, 5 FT. #625
LabID:
02A
Sample ID:
GD #48, 10 FT. #625
LabID:
03A
Sample ID:
GD #89, 5 FT. #625
LabID:
04A
Sample ID:
OD #89, 10 FT. #625
LabID:
05A
Sample ID;
GD #128, 5 FT. #625
LabID:
06A
Sample ID:
GD #'l28, 10 FT. #625
Test Codes and Names
3050
B AE2
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8270s
8260S
Acid Digestion ,
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
Volatile Oivanics
Test Codes and Names
3050
B AE2
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
827i5S
8260S
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
3050
B AE2
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
827DS
8260S
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercuiy
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
3050
B AE2
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
827DS
8260S
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
3050
B AE2
CD AE2
CR AE2
PB AE2
AO AE2
HG CV2
8270s
8260S
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
3050 Acid Digestion
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A Method
SW-846, 3050
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A Method
SW-846. 3050
SW-846, 6010
SW-846. 6010
SW-846. 6010
SW-846. 6010
SW-846. 6010
SW-846, 7471
SW-846, 8270
SW-846.8260A Method
SW-846. 3050
Page tt:l of
Work Orders 9509054 Sample and Test Code Identification
LabID:
06A
Sample ID:
GD #128. 10 FT. #625
Test Codes and Names
LabID:
07A
Sample ID:
GD #125, 5 FT. #625
Lab ID:
08A
Sample ID: mpl GD #125, 10 FT. #625
LabID:
09A
Sample ID:
GD #219, 5 FT. #625
LabID:
lOA
Sample ID:
GD #219, 10 FT. #625
UbID:
UA
Lab ID:
12A
Sample ID:
GD #219. 10 FT. #625 DUP.
Sample ID:
GD «06. 5 FT. #625
Lab ID:
13A
B AE2
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
827DS
8260S
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Otganics
Volatile Organics
Test Codes and Names
3050
B AE2 CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8270s
8260S
Acid Digestion
Boron Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
3050
B AE2
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8270s
8260S
Acid Digestion
Boron Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
3050
B AE2
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
827DS
8260S
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercuiy
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
3050 Acid Digestion
B_AE2 Boron
CD_AE2 Cadmium
CR_AE2 Chromium
PB_AE2 Lead
AO_AE2 Silver
HG CV2 Mercuiy
8270s Semi-Volatile Oi^ganics
8260S Volatile Organics
Test Codes and Names
8260S Volatile Organics
Test Codes and Names
Sample ID:
GD mt, 5 Ft. RINSE BLANK
3050
B AE2
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8270S
8260S
Acid Digestion
Boron
Cadmium
Chroinium
Lead
Silver
Mercury
Semi-Volatile Oiganics
Volatile Oiganics
Test Codes and Names
3010
B AE2
CD AE2
CR AE2
PB AE2
AG AE2
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Method
SW-846. 6010
SW-846. 6010
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846. 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846.8260A
Method
SW-846. 3050
SW-846. 6010
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846. 7471
SW-846. 8270
SW-846.8260A
Method
SW-846, 3050
SW-846, 6010
SW-846. 6010
SW-846. 6010
SW-846. 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846.8260A
Method
SW-846.8260A
Method
SW-846. 3050
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846.8260A Method
SW-846. 3010
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010 o
Page #:2
WorkOrder/}' 9509054 Sample and Test Code Identilfication
•
LabID: Sample ID:
13A GD #206, 5 FT. RINSE BLANK
LabID:
14A
Sample ID:
OD #206, 10 FT. #625
LabID:
•"HA
Sample ID:
OD #96, 5 FT. #625
LabID:
16A
Sample ID:
GD #96, 5 FT. #625 DUP.
Test Codes and Names
HG_CV3 Mercury
8270 Semi-Volatile Organics
8260 Volatile Oi;ganics
Test Codes and Names
3050
B AE2
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8270S
8260S
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
3050
B AE2
CD AE2
CR A£2
PB AE2
AG AE2
HO CV2
8270S
8260S
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercuiy
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
8270S Semi-Volatile Organics
Comments
Method
SW-846, 7470
SW-846, 8270
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A Method
,3050
.6010
,6010
.6010
,6010
,6010
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846, 7471
SW-846, 8270
SW-846,8260A
Method
SW-846, 8270
Report: There is evidence of a slight negative matrix interference for
lead and silver.
^QZ. 5^^^^^-W^
Certified By
•
Page #:3
This is to certify tfiat tfie following samples were analyzed using good laboratory practices
to sfiow tfie following results.
Sample ID: GD #48, 5 FT. #625 Lab ID: 9509054-OlA Collected: 09/25/95 08:40:00
TEST
Add Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Seml-Volatlle Organics
phenol
bis(2-chloroethyl)ether
2-chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis (2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethcme
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2 -chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4 -chloroani1ine
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroaniline
dimethylphthalate
acenaphthylene
3-nitroaniline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
^,6-dinitrotoluene
RESULT
10/10/95
6.39
U
19.4
U
U
0.02
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u u u u u
u u u u u u u
u u u
u u u u
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.4
0.1
0.3
1.6
0.2
0.014
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
ANALYZED
10/10/95
10/13/95
10/13/95
10/13/95
10/13/95
10/13/95
10/25/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
BY
SJM
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JHA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METEOD/CAS#
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1 ^^
95-48-7 ^B
108-60-1 ^^
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2 ^^
Page ff: A o
Novembers, 1995 13:54
Sample ID: GD #48, 5 FT. #625
CERTIFICATE OF A>[AJLYSIS
RESULTS BY SAMPLE
Lab ID: 9509054-OlA CoUected: 09/25/95 08:40:00
TEST RESULT UNITS DETECTION ANikLYZED BY
LIMIT
METHOD/CAS#
Seml-Volatlle Organics
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4 -nitroeuiiline
4,6-dinitro-2-methylphenol
n-ni trosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenanthrene
anthracene
di-n-butylphthalate
fluorauithene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
i^^zo (b) fluoranthene
U^pizo (k) fluoranthene
cenzo(a)pyrene
indeno(1,2,3 -cd)pyrene
dibenz(a,h)anthracene
benzo (g,h, Dperylene
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodi chlorometheme
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
U
u u u u u u u u u u u u u u
u
u u u
u u u u
u u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -fluorophenol
phenol-dS
nitrobenzene -d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
*
u u u u
u
u
u u u u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8270
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270S
%Recovery
71.64
76.32
73.35
78.62
87.00
126.5
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
Page #: 5
November 3, 1995 13:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #48, 5 FT. #625 Lab ID: 9509054-OlA CoUected: 09/25/95 08:40:00
TEST REST7LT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3-chloropropan
1,2-dibromoethane
dibromome thane
di chlorodifluoromethsme
1,1-dichloroetheme
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
i sopropylbenzene
4 - isoprcipyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroetheme
trichloroethene
t r i chlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentemone
2-hexemone
fluorobenzene
u
u u
u
u u u u
u u u u u u u u
u u u u u u u u u u u
u u
u u
u u u u u u 5.5 J
u u u u u u u
u
u u u u u 774897
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
, MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
Page tt: 6
Novembers, 1995 13:54 CERTIFICATE OF AN^O^YSIS
RESULTS BY SAMPLE
Sample ID: GD #48, 5 FT. #625 Lab ID: 9509054-OlA CoUected: 09/25/95 08:40:00
TEST RESULT UNITS DETECTION ;kN.I^YZEO BY
LIMIT
METHOD/CAS#
Volatile Organics
chlorobenzene-d5
1,4-dichlorobenzene •
368791 ug/Kg
•d4 134412 ug/Kg
Surrogate/Recovery Data
Surrogate
dibromofluoromethane
1,2-dichloroetheme-d4
toluene-d8
bromofluorobenzene
SW-846,8260A
10/06/95 MMR INTSTD2
10/06/95 MMR INTSTD3
For Volatile Organics 8260S
%Recovery Recovery Limits
85.4 58.4 TO 112
76.7 53.3 TO 121
119 85.6 TO 143
107 80.6 TO 130
Sample ID: GD #48, 10 FT. #625 Lab ID: 9509054-02A CoUected: 09/25/95 08:55:00
TEST RESULT UNITS DETECTION ANJIILYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
ron
Cadmi\jm
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4 -dimethylphenol
#
10/10/95
7.77
U
10.9
U
U
D
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.4
0.1
0.3
1.7
0.2
0.011
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
10/10/95
10/13/95
10/13/95
10/13/95
10/13/95
10/13/95
10/25/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
SJM
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
3050
6010
6010
6010
6010
6010
7471
8270
Page tf: 1
Sample ID: GD #48, 10 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9509054-02A CoUected: 09/25/95 08:55:00
TEST »
Semi-Volatile Organics
bis(2-chloroethoxy)methane
2,4 -di rhlorophenol
1,2,4-trichlorobenzene
naphthalene
4 -chloroaniline
hexachlorobutadi ene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroaniline
dime thyIphthalate
acenaphthylene
3-nitroaniline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4-chlorophenyl-phenylether
fluorene
4-nitroaniline
4,6-dinitro-2-me thyIphenol
n-nitrosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenemthrene
anthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h)anthracene
benzo (g,h, Dperylene
RESULT
U
u
u u
u u u
u u u u u u u
u
u n D
o D
u
n u
u u u u u u
u u u u 62 J
u u
u
u u u
u u u u
u n u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3 M
86-73-7 W
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
Page #: 8
Novembers, 1995 13:54
Sample ID: GD #48, 10 FT. #625
CERTIFICATE OF ANiU^YSIS
i, ' RESULTS BY SAMPLE
Lab ID: 9509054-02A CoUected: 09/25/95 08:55:00
TEST
Semi-Volatile Organics
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chlorometheme
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
^jorobenzene
^Horoe thane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
RESULT UNITS
Surrogate/Recovery Data
Surrogate
2-fluorophenol
phenol -d5
nitrobenzene -d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terpheny1-dl4
1,2-dibromo-3-chloropropem
1,2-dibromoetheme
dibromome thane
dichlorodifluorometheme
1,1-dichloroe thane
1,2-dichloroethane
1,1-di chloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
U
U
U
U
U
U
U
U
U
u u u
u u a u u 0
u u u 0
u u D
D
U
u u u u u u u u u
u u
u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
J^ALYZED BY METHOD/CAS#
SW-846, 8270
For Semi-Volatile Organics 827OS
%Recovery
50
54
51
58
86
.40
.96
.30
.6,4
.00
128.8
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
• Page tt: 9
Sample ID: GD #48, 10 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9509054-02A CoUected: 09/25/95 08:55:00
TEST
Volatile Organics
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4 -di chlorobenzene-d4
RESULT
3
U
n U
U
U
U
U
U
u . IJ
n
u
u
u
u u u
u
u D
D
U
U
775742
391236
151003
Surrogate
Surrogate
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10 .
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
/Recovery Data For Volatile Organics 8260S
dibromofluorome thane
1,2-di chloroe theme-d4
toluene-d8
brom ofluorot )enzene
%Recovery
85.5
74.6
115
103
METHOD/CAS#
SW-846,8260A
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6 ^
im'STDl ^
INTSTD2 ^
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Sample ID: GD #89, 5 FT. #625 LabID: 9509054-03A CoUected: 09/25/95
TEST RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Acid Digestion
Boron
Cadmium
Chromiiiffl
10/10/95
7.17
0.27
16.0
DATE
ug/g
ug/g
ug/g
0.4
0.1
0.3
10/10/95
10/13/95
10/13/95
10/13/95
SJM
LVD
LVD
LVD
SW-846,
SW-846,
SW-346,
SW-846,
3050
6010
6010
6010
Page tt: 10 41
November 3, 1995 13:54 CERTIFICATE OF AN^U^YSIS
RESULTS BY SAMPLE
Sample ID: GD #89, 5 FT. #625 LabID: 9509054-03A CoUected: 09/25/95
TEST
Lead
Silver
Mercury
Semi-Volatile Organics
phenol
bis(2 -chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-prbpylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
^^4 - dimethylphenol
•i^^b (2-chloroethoxy)metheme
^^^ - di chlorophenol
1,2,4-trichlorobenzene
naphthalene
4-chloroaniline
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroaniline
dimethylphthalate
acenaphthylene
3-nitroaniline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroemiline
4,6-dinitro-2-methyIphenol
n-nitrosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
RESULT
u
u
0.01
u u
u
u u u u u
u u u
u u
u
u u u u u
u u
u
u u
u u u u u
u a u
u u u u u u
u u u
u
u u u
UNITS
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
1.5
0.2
0.013
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700 •
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
ANALYZED
10/13/95
10/13/95
10/25/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
BY
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
Page#: 11
November 3, 1995 13:54
Sample ED: GD #89, 5 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9509054-03A CoUected: 09/25/95
TEST
Semi-Volatile Organics
pentachlorophenol
phenemthrene
emthracene
di-n-butylphthalate
fluoremthene
pyrene
butylbenzylphthalate
benzo(a) emthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoremthene
benzo(k)fluoremthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h)anthracene
benzo(g,h, Dperylene
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodi chlorome theme
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorometheme
2 -chlorotoluene
4-chlorotoluene
dibromochloromethane
RESULT
U
U
U
U
a u
u
u u a
u u
u u D
u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -fluorophenol
phenol -d5
nitrobenzene -d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
1,2-dibromo-3 -chloropropem
1,2-dibromoethane
dibromomethane
dichlorodifluorometheme
u u u u u
u u u
u u u u
u
u
u u u u
u
u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270S
%Recovery
70.80
77.12
73.35
82.10
99.60
128.9
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits ii^
25
24
23
30
19
18
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
HMR
MMR
MMR
MMR
MMR
MMR
MMR
^^^'
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
Page tf: 12 •
Novembers, 1995 13:54 CERTIFICATE OF AN^'O.YSIS
RESULTS BY SAMPLE
•
Sample ID: GD #89, 5 FT. #625
TEST
Volatile Organics
1,1-dichloroethane
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropeme
2,2-dichloropropane
1,l-dichloropropene
cis-1,3 -dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
^|to^rene
flH. ,1,2-tetrachloroetheme
^^1,2,2- tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4 -me thyl-2 -pentanone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
' /
RESULT
u u u D
U
D
U
U
U
D
U
U
D
U
U
U
U
U
U
U
U
u u D
U
D
U
U
U
U
U
U
U
U
U
u u u
u u u
u 901635
473208
180045
LabID: 9509054-03A
UNITS DETECTION
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
dibromofluorometheme
1,2-dichloroetheme-d4
LIMIT
10
10
10
10
10
10
10
1-0
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
J^ALYZED
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
CoUected: 09/25/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
For Volatile Organics 8260S
%Recovery
90.2
87.2
METHOD/CAS#
SW-846,8260A
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
TO 112
TO 121
Page #: 13
Novembers, 1995 13:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #89, 5 FT. #625 LabID: 9509054-03A CoUected: 09/25/95
TEST RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Volatile Organics
toluene-d8
bromofluorobenzene
111
106
85.6 TO 143
80.6 TO 130
SW-846,8260A
Sample ID: GD #89, 10 FT. #625 LabID: 9509054-04A CoUected: 09/25/95 10:00:00
TEST
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethcme
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4 - chloroemilijie
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
RESULT
10/10/95
5.19
U
10.2
U
U
U
U
U
U
U
U
U
U
U
U
D
D
U
U
D
U
U
U
U
U
U
O
U
U
U
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.4
0.1
0.3
1.5
0.2
0.010
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
10/10/95
10/13/95
10/13/95
10/13/95
10/13/95
10/13/95
10/25/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
BY
SJM
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6OI0IV
SW-846, 7471
SW-846, 8270
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4 ^
Page#: 14
A le ID: GD #89, 10 FT. #625
CERTIFICATE OF AN^y^YSIS
f RESULTS BY SAMPLE
Lab ID: 9509054-04A CoUected: 09/25/95 10:00:00
TEST
Semi-Volatile Organics
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2-chloronaphthalene
2-nitroaniline
dimethylphthalate
acenaphthylene
3-nitroemiline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dini trotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroaniline
4,6-dinitro-2-methylphenol
n-ni trosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenz ene
pentachlorophenol
^^anthrene
-i^Bracene
^Bn - buty Iph thai at e
fluoranthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octyIphthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h)anthracene
benzo (g,h, Dperylene
RESULT
139
66
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
D
U
n
u
u
u
J
u u
u
u
u J
u u
u D
u u
u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2-flu orophenol
phenol-d5
nitrobenzene
2-flu
2,4,6
terph
-d5
orobiphenyl
-tribromophenol
enyl-dl4
DETECTION
LIMIT
330
330
330
1700
330
330
1700
330
330 .
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANAJiYZED
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/2;i/95
10/23/95
10/23/95
10/23/95
10/23/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
OMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-3
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270S
%Recovery
45.04
47.36
45.03
51.93
90.80
121.7
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 12 0
TO 115
TO 122
TO 137
Page it: 15
November 3, 1995 13:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #89, lo FT. #625 Lab ID: 9509054-04A CoUected: 09/25/95 10:00:00
TBST
Volatile Organics
benzene
bromobenz ene
bromochloromethane
bromodi chloromethane
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3 -chloropropan
1,2-dibromoethane
dibromometheme
di chlorodifluorometheme
1,1-di chloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropeme
2,2 -di chloropropeme
1,1-dichloropropene
cis-1,3-dichloropropene
trems-1,3 -di chloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
RESULT
U
u u u u D
U
U
U
U
u u
u a
u u u u
u u
u
u u D
U
D
D
D
U
U
U
U
U
D
U
U
U
D
n o o D
U
U
u o a u D
u
u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
1-0
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 •
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3 ^^
107-06-2 ^Bl
75-35-4 ^^
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
Page ff: 16 a
November 3, 1995 13:54
Sample ID: GD #89, 10 FT. #625
CERTIFICATE OF AN^O^YSIS
! l ' RESULTS BY SAMPLE
LabID: 9509054-04A CoUected: 09/25/95 10:00:00
TEST
Volatile Organics
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl- 2-pentanone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4 -dichlorobenzene-d4
RESTJLT
U
U
u
u u u
u
u
u u
u 951613
496527
182753
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
1-0
10
10
10
ANALYZED
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorometheme
1,2 -di chloroethane-d4
^^ toluene-d8
^^ bromofluorobenzene
%Recovery
92.3
85.2
112
108
METHOD/CAS#
SW-846,8260A
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Sample ID: GD #128, 5 FT. #625 LabID: 9509054-05A CoUected: 09/25/95 10:40:00
TEST
Acid Digestion
Boron
Cadmium'
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
phenol
bis(2-chloroethyl)
2 -chlorophenol
ether
RESULT
10/10/95
5.
0.
13
76
20
1.0
U
U
U
0
U
U
TJNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.4
0.1
0.3
1.7
0.2
0.0088
330
330
330
ANiUiiYZED
10/10/95
10/13/95
10/13/95
10/13/95
10/13/95
10/13/95
10/25/95
10/23/95
10/23/95
10/23/95
BY
SJM
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
3050
6010
6010
6010
6010
6010
7471
8270
Page ff: 17
November 3, 1995 13:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #128, 5 FT. #625 Lab ID: 9509054-05A CoUected: 09/25/95 10:40:00
TEST
Semi-Volatile Organics
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethcme
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4 -chloroemi1ine
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroaniline
dimethylphthalate
acenaphthylene
3-nitroemiline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroemiline
4,6-dinitro-2-methylphenol
n-ni trosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenemthrene
emthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a) emthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
RESTJLT
U
u u u u
u
u u u u u
u u u
u u
u u u
u
u u
u u u u u u u
u u u u u D
u
u u u a
u u D
u u u u u
u
u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
33-0
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
. 330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
ANALYZED
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2 g^
95-95-4 ^H
91-58-7 ^^
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
Page tt: 18
November 3, 1995 13:54
•
Sample ID: GD #128, 5 FT. #625
CERTIFICATE OF ANiU^YSIS
RESULTS BY SAMPLE
LabID: 9509054-05A CoUected: 09/25/95 10:40:00
TEST
Semi-Volatile Organics
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3 -cd)pyrene
dibenz(a,h) emthracene
benzo (g,h, Dperylene
Volatile Organics
^l^zene
^^nmobenzene
bromochlorometheme
bromodi chlorome theme
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
RESULT
U
U
U
U
U
U
U
D
Surrogate/Re cove
Surrogate
2 -fluorophenol
phenol -d5
nitrobenzene -d5
2 -fluorobiphenyl
2,4,6-
TJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ry Data
tribromophenol
terphenyl-dl4
1,2-dibromo-3-chloropropan
1,2-dibromoetheme
dibromomethane
dichlorodifluoromethane
1,1-dichloroetheme
1,2-dichloroethcme
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropeme
1,l-dichloropropene
cis-1,3-dichloropropene
U
U
U
U
u
u u u u u u
u u u u u u u u u u u
u u
u
u u
u
u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
330
J^ALYZED
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270S
%Recovery
90.76
88.68
85.87
86.83
97.80
122.3
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
Page#: 19
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #128, 5 FT. #625 Lab ID: 9509054-05A CoUected: 09/25/95 10:40:00
TEST RESULT TJNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1- trichloroe thajie
1,1,2-trichloroethane
trichloroethene
tri chlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4 -di chlorobenzene-d4
u
u n u u u u
u
u n u u u u u u u
u 3.1 J
D
u
u u
u u D
u u u u 0
n 947444
432841
142000
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate
dibromofluorometheme
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
10
10
10
10
10
10
10
10
10 .
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
For Volatile Organics 8260S
%Recovery
83.9
71.6
124
111
SW-846,3260A
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-37-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Page #: 20 •
November 3, 1995 13:54
Sample ID: GD #128, 10 FT. #625
CERTIFICATE OF A1V.^YSIS
RESULTS BY SAMPLE;
LabID: 9509054-06A CoUected: 09/25/95 10:50:00
TEST
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
^Bipiethylphenol
^^K (2 - chloroisopropyl) ethe
T-methylphenol
n-nitroso-di-n-propylamine
hexachloroetheme
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)metheme
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4-chloroaniline
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroaniline
dimethylphthalate
acenaphthy1ene
3-nitroaniline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dinitrotoluene
^^4-dinitrotoluene
RESULT
10/10/95
5.54
0.18
10.9
U
D
0.009
U
U
U
U
U
U
U
U
U
U
D
D
D
U
U
U
U
U
u u u
u u u
u u
u
u u
u u u
u u u u
u
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.4
0.1
0.3
1.5
0.2
0.0076
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330 .
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
.I^rALYZED
10/10/95
10/13/95
10/13/95
10/13/95
10/13/95
10/13/95
10/25/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
BY
SJM
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
Page #: 21
Sample ID: GD #128, 10 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9509054-06A CoUected: 09/25/95 10:50:00
TEST
Semi-Volatile Organics
diethylphthalate
4 -chlorophenyl-phenyl
fluorene
4-nitroaniline
ether
4,6-dinitro-2-methylphenol
n-ni trosodipheny1amine
4-bromophenyl-phenyle
hexachlorobenzene
pentachlorophenol
phenanthrene
anthracene
di-n-butylphthalate
fluoremthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
ther
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3 -cd)pyrene
dibenz(a,h)anthracene
benzo(g,h,i)perylene
Volatile Organics
benzene
bromobenzene
bromochlorome theme
bromodi chlorome thane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
RESULT
Surrogate
Surrogati
U
U
U
U
u n
n n u
u u 70 J
u n
u n u u
n u D
u u u u u
TJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
/Recovery Data
3
2-fluorophenol
phenol -d5
nitrobenzene-d5
2-fluorob;
2,4,6-
Lphenyl
tribromophenol
terphenyl -dl4
n U
u .
u u u u
u
u u u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
660
330
330
330
330
1700 -
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8 ^^
193-39-5 O
53-70-3 ^
191-24-2
For Semi-Volatile Organics 8270S
%Recovery
54.96
56.60
58.52
62.10
72.60
125.4
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8250A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
Page #: 22
r November 3, 1995 13:54
Sample ED: GD #128, 10 FT. #625
CERTIFICATE OF AI^^i^iLYSIS
. RESULTS BY SAMPLE
Lab ID: 9509054-06A CoUected: 09/25/95 10:50:00
TEST
Volatile Organics
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3-chloropropan
1,2-dibromoetheme
dibromometheme
dichlorodifluorome theme
1,1-dichloroetheme
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropane
2,2-dichloropropane
1,1-dichloropropene
cis-1,3 -dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
J^A -dichlorobenzene
^^Bylbenzene
^PKachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2, 3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl- 2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
RESTJLT
U
U
u u u
u u u u
u u
u u u u
u u D
u u u u u u u u
u u
u u u u
u u
u u
u u
u u u u u u u u u u u
u 1277378
644290
TJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANJLLYZED
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
Page tt: 23
}
November 3, 1995 13:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #128, 10 FT. #625 LabID: 9509054-06A CoUected: 09/25/95 10:50:00
TEST RESTJLT TJNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
1,4-dichlorobenzene-d4 227208 ug/Kg
Surrogate
dibromofluorometheme
1,2 -di chloroetheme-d4
toluene-d8
bromofluorobenzene
SW-846,8260A
10/06/95 MMR INTSTD3
For Volatile
%Recovery
90.7
84.0
116
110
Organics 8260S
Recovery Limits
58.4 TO 112
53.3 TO 121
85.6 TO 143
80.6 TO 130
Sample ID: GD #125, 5 FT. #625 LabID: 9509054-07A CoUected: 09/25/95 11:24:00
TEST RESTJLT TJNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
phenol
bis(2-chloroethyl)ether
2-chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)metheme
10/10/95
3.13
0.66
18.1
U
U
0.01
U
U
U
U
a
u
u u u u D
U
U
U
u
u
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.4
0.1
0.3
1.6
0.2
0.010
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
10/10/95
10/13/95
10/13/95
10/13/95
10/13/95
10/13/95
10/25/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
SJM
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
3050
6010
6010
6010
6010
6010
7471
8270
Page tt: IA
si^ lie ID: GD #125, 5 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9509054-07A CoUected: 09/25/95 11:24:00
TEST
Semi-Volatile Organics
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4-chloroaniline
hexachlorobutadi ene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2-chloronaphthalene
2-nitroaniline
dime chyIphthalat e
acenaphthylene
3-nicroaniline
. acenaphthene
2,4-dinitrophenol
4-nicrophenol
dibenzofuran
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4j^^lorophenyl -phenylether
f^^pene
4^BK^oemi 1 ine
4", 6-dinitro-2-methylphenol
n-ni trosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenanthrene
anthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h)anthracene
benzo(g,h,i)perylene
RESULT
U
u
u
u 0
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
n
u
u
u
u
u
u
u
n 38 J
u u
u
u
u
u
n
u
n
u
n
u
u
u
UNITS
ug/Kg
-ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
330
330.
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANAlaYZED
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
io/2;;/95
10/23/95
10/22/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
Page #: 25
November 3, 1995 13:54
Sample ID: GD #125, 5 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9509054-07A CoUected: 09/25/95 11:24:00
TEST
Sami-Volatile Organics
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chloromethane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
RESTJLT TJNITS
Surrogate/Recovery Data
Surrogate
2 -fluorophenol
phenol -d5
nitrobenzene
2-fluorobiph
2,4,6-
i-d5
lenyl
tribromophenol
terphenyl-dl4
1,2-dibromo-3-chloropropem
1,2-dibromoethane
dibromometheme
dichlorodifluoromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-l,2-dichloroethene
treuis -1,2- dichloroethene
1,2-dichloropropeme
1,3-dichloropropane
2,2-dichloropropeme
1,l-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
U
U
U
U
U
U
U
U
U
U
D
U
V
U
U
U
U
U
u n u
u u D
u u u
u u o u u V
u u u
u u
u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
ANALYZED BY METHOD/CAS#
SW-846, 8270
For Semi-Volatile Organics 8270S
%Recovery
80
78
77
77
91
.12
.04
.07
.84
.52
128.9
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 •
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5 ^^—^
108-90-7 ^^
75-00-3 ^^
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
Page it: 26 •
SaHp le ID: GD #125, 5 FT. #625
CERTIFICATE OF ANAJLYSIS
RESULTS BY SAMPLE
LabID: 9509054-07'A CoUected: 09/25/95 11:24:00
TEST
Volatile Organics
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethame
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
tri chlorofluorome thane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2 -butanone
4-methyl-2-pentanone
2^Kxemone
i^Hrobenzene
ca^ror obenz ene - d5
1,4-dichlorobenzene-d4
RESULT
U
U
u
u u
a u u u 3.1 J
u n D
u D
u u D
D
U
U
U
a 706224
341730
121897
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10 -
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANAJJYZKD
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/05/95
10/05/95
10/06/95
10/05/95
10/06/95
10/05/95
lO/O'S/95
10/05/95
10/05/95
10/06/95
lO/OS/95
10/06/95
10/05/95
10/06/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8260A
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluoromethane
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
%Recovery
82.7
71.9
117
107
Recovery
58.4 TO
53.3 TO
85.6 TO
80.6 TO
Limits
112
121
143
130
Sample ID: GD #125, 10 FT. #625 LabID: 9509054-08A CoUected: 09/25/95 11:35:00
TEST RESULT UNITS DETECTION ANAIiYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Boron
Cadmium
Chromiiom
10/10/95
3.62
tJ
10.4
DATE
ug/g
ug/g
ug/g
0.4
0.1
0.3
10/10/95
10/13/95
10/13/95
10/13/95
SJM
LVD
LVD
LVD
SW-846,
SW-846,
SW-a46,
SW-846,
3050
6010
6010
6010
Page #: 27
November 3, 1995 13:54
Sample ID: GD #125, 10 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
•
LabID: 9509054-08A CoUected: 09/25/95 11:35:00
TEST
Lead
Silver
Mercury
Semi-Volatile Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4 -chloroemiline
hexachlorobutadiene
4-chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroemiline
dimethylphthalate
acenaphthylene
3-nitroemiline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroemiline
4,6-dinitro-2-methylphenol
n-ni trosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
RESTJLT
U
u
u
u u
u
u u
u
u
u u
u u u u
u u u u u u u u u u u u u u
u u
u u u u D
u u u u
u u u
u u
u
u
TJNITS
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
1.7
0.2
0.014
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
ANALYZED
10/13/95
10/13/95
10/25/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
BY
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9 ^^^
111-91-1 m^
120-83-2 ^tF
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
Page #: 28 #
M le ID: GD #125, 10 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9509054-08A CoUected: 09/25/95 11:35:00
TEST *
Semi-Volatile Organics
pentachlorophenol
phenanthrene
anthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a) emthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoremthene
benzo(k)fluoremthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h)anthracene
benzo (g,h, Dperylene
A V
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodichloromethane
bromoform
bromomechane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorome thane
RESULT
Surrogate
Surrogati
D
n U
60 J
U
U
U
u u u
u u
u u u
u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
/Recovery Data
3
2 -fluorophenol
phenol -dS
nitrobenzene-d5
2-fluorob:
2,4,6-
Lphenyl
tribromophenol
terphenyl •
1,2-dibromo-3-chloropropan
1,2-dibromoetheme
dibromome thane
dichlorodifluoromethane
-dl4
U
U
U
U
D
U
U
U
U
U
U
D
U
u u
u
u
n u u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
1700
330
330
330
330
330
330
330
330 -
330
330
330
330
330
330
330
330
330
• ANAICiYZED
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organica 8270S
%Recovery
42.12
44.24
41.02
46.01
75.20
131.3
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Liaits
25
24
23
30
19
18
10/06/95
10/06/95
10/06/95
lO/OK/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-36-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
Page #: 29
November 3, 1995 13:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #125, 10 FT. #625 LabID: 9509054-08A CoUected: 09/25/95 11:35:00
TEST
Volatile Organics
1,1-dichloroetheme
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropeme
2,2-dichloropropeme
1,l-dichloropropene
cis-1,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentemone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESTJLT
U
u u u a u
u u u u u u u u u u u u u u
u u u u u u u u u u
u u
u u D
u u u u * u u
u 1023173
548046
211998
TJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorometheme
1,2-d ichloroetha ne-d4
%Recovery
90.9
82.1
METHOD/CAS#
SW-846,8260A
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5 ^^
630-20-6 ^B.
79-34-5 ^^
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
TO 112
TO 121
Page tt: 30 a
November 3, 1995 13:54
Sample ID: GD #125, 10 FT. #625
CERTIFICATE OF A1V.^YSIS
RESULTS BY SAMPLE
LabID: 9509054-08A CoUected: 09/25/95 11:35:00
TEST RESULT TJNITS DETECTION il^ALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics toluene-d8
bromofluorobenzene
110
105
85.6 TO 143
80.6 TO 130
SW-846,8260A
Sample ID: GD #219, 5 FT. #625 Lab ED: 9509054-09A CoUected: 09/25/95 11:54:00
TEST
Acid Digestion
Boron
Cadmium
Chromium
Lead
^ft-VBX
Mercury
Semi-Volatile Organics
phenol
bis(2-chloroethyl)ether
2-chlorophenol
1,3-dichlorobenzene
1,4 -di chlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroetheme
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4-chloroaniline
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
RESTJLT
10/10/95
U
0.98
52.9
15.8
166
0.75
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
O
U
U
u
u
TJNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.4
0.1
0.3
1.6
0.2
0.011
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
J^ALYZED
10/10/95
10/13/95
10/13/95
10/13/95
10/13/95
10/13/95
10/25/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
BY
SJM
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50.1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4 nexe
• Page #: 31
Sample ID: GD #219, 5 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9509054-09A CoUected: 09/25/95 11:54:00
TEST •
Semi-Volatile Organics
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2-chloronaphthalene
2-nitroemiline
dimethylphthalate
acenaphthylene
3-nitroaniline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dinitrotoluene
2,4-dinitrotoluene
di e thyIphthaiate
4 -chlorophenyl-phenylether
fluorene
4-nitroaniline
4,6-dinitro-2-methylphenol
n-nitrosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenanthrene
anthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h)anthracene
benzo(g,h,i)perylene
RESTJLT
U
u
u D
U
U
U
n
u
u u
u
D
u
u
u u
u
D
D
D u
u
u 90 J
u
u
u
u u
700
n
u
u D
u
u
u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
2
Surrogate
-fluorophenol
phenol -d5
nitrobenzene-d5
2
2
t
-fluorobiphenyl
,4,6-
srphe
tribromophenol
nyl-dl4
DETECTION
LIMIT
330
330
330
1700
330
330
1700
330
330,
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS #
SW-846, 8270
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8 ^^
120-12-7 ^
84-74-2 ^P
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270S
%Recovery
30.17
42.20
42.05
65.63
68.80
129.3
Recovery Limita
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
Page #: 32 •
pie ID: GD #219, 5 FT. #625
CERTIFICATE OF AN/iJ:.YSIS
RESULTS BY SAMPLE
LabID: 9509054-09A CoUected: 09/25/95 11:54:00
TEST
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chlorome thane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropem
1,2-dibromoethane
dibromome thane
dichlorodifluoromethane
1,1-di chloroe thane
1^- di chl oroe thane
i^^ dichloroe thene
^^1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropeme
1,l-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
RESTJLT
D
U
u u
u u u u u u u u u u n D
u
u
u u
u u D
D
n
u u
u u u D
n D
u n
u u u
u u u
u u D
u u D
n u 3.1 J
u
u
UNITS
ug/Kg
ug/Kg.
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
. ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10,
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
• ANJ^YZED
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,3260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-58-3
98-32-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-13-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
Page #: 33
November 3, 1995 13:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #219, 5 FT. #625 LabID: 9509054-09A CoUected: 09/25/95 11:54:00
TEST
Volatile Organics
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl- 2-pentemone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4 -di chlorobenzene-d4
RESTJLT
u u
u u u
u u
u u u
u 1124991
557181
193582
TJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
ro 10
10
10
ANALYZED
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorometheme
1 ,2 -di chloroethane-d4
toluene-d8
b romofluorobenze ne
%Recovery
91.0
84.6
115
110
METHOD/CAS#
SW-846,8260A
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recoveiry Limita
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130 i^
Sample ID: GD #219, 10 FT. #625 Lab ID: 9509054-IOA CoUected: 09/25/95 12:02:00
TEST
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
RESTJLT
10/10/95
9.23
U
11.9
O
U
0.02
U
U
U
TJNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.4
0.1
0.3
1.6
0.2
0.012
330
330
330
ANALYZED
10/10/95
10/13/95
10/13/95
10/13/95
10/13/95
10/13/95
10/25/95
10/24/95
10/24/95
10/24/95
BY
SJM
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
3050
6010
6010
6010
6010
6010
7471
8270
Page tt: 34
M le ID: GD #219, 10 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLi:
Lab ID: 9509054-lOA CoUected: 09/25/95 12:02:00
TEST •
Semi-Volatile Organics
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2 -di chlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis (2-chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4 -chloroaniline
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2^^5 - trichlorophenol
2^BL oronaphthal ene
2^^t roemi 1 ine
dimethylphthalate
acenaphthy1ene
3-nitroaniline
acenaphthene
2,4-dinitrophenol
4 -nitrophenol
dibenzofurem
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroaniline
4,6-dinitro-2-methylphenol
n-nitrosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenanthrene
anthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
RESULT
U
U
u
u
u
u
u u
u
tr
u
u
u
u
u
u
u
n D
u u
u
u
u
u u
u
D
u
u
u
u
u
u
u u
u u
u
u
u
u
u
u u
50 J
u u
u
u
u
u
TJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
330
330 .
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
AKFAJCYZED
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/2<l/95
10/2^1/95
10/24/95
10/24/95
10/241/95
10/24/95
10/2<:/95
10/24,/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-3
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-3
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-31-7
Page #: 35
November 3, 1995 13:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #219, 10 FT. #625 LabID: 9509054-lOA CoUected: 09/25/95 12:02:00
TEST
Semi-Volatile Organics
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(l,2,3 -cd)pyrene
dibenz(a,h) emthracene
benzo(g,h, Dperylene
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodichloromethane
bromoform
bromometheme
n-butyIbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
RESULT
Surrogate
Surrogati
U
U
U
U
U
U
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
/Recovery Data
B
2 -fluorophenol
phenol -d5
nitrobenzene-d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl
1,2-dibromo- 3 -chloropropan
1,2-dibromoetheme
dibromomethane
dichlorodifluorometheme
1,1-dichloroethane
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2 -dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropane
2,2-dichloropropame
1,1-dichloropropene
cis-1,3-dichloropropene
-dl4
U
U
U
U
u
u u
u u u u u u u u u u u
u
u u
u
u u u u u
u
u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
330
ANALYZED
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270S
%Recovery
69.80
74.76
67.37
73.23
82.92
142.7
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2 ^^
108-86-1 ^B
74-97-5 ^^
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
Page tt: 36
November 3, 1995 13:54
Sample ID: GD #219, 10 FT. #625
CERTIFICATE OF ANiiLYSIS
RESULTS BY SAMPLE
Lab ID: 9509054-lOA CoUected: 09/25/95 12:02:00
TEST
Volatile Organics
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4 -di chlorobenz ene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroetheme
trichloroethene
^^^L chlorof luorome thane
'^^M, 3 -trichloropropeme
^^, 4 - trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4 -methyl - 2 -pentemone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
U
U
U
U
U
U
U
U
U
U
u u u u u u u u u u u u u
u
u u u u u u u u 855002
486511
198777
TJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
lb
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
JI^ALYZED
10/06/95
.10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorome theme
1,2-di chloroetheme-d4
toluene-d8
bromofluorobenzene
^Recovery
92.2
88.8
105
103
METHOD/CAS#
SW-846,8260A
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Page tf: 37
Novembers, 1995 13:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #219, 10 FT. #625 DUP. LabID: 9509054-11A CoUected: 09/25/95 12:02:00
TEST
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chlorometheme
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3 -chloropropan
1,2-dibromoetheme
dibromometheme
dichlorodifluoromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropeme
2,2-dichloropropane
1,l-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
RESTJLT
U
u u u u D
U
U
U
U
u u u u u u u u
u u u u u u u u u
u u u u u u u u u
u D
u u
u u u u u u u u u u
u
u
TJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
1-0
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
•
Page tt: 38 •
November 3, 1995 13:54 CERTIFICATE OF AJ^^^YSIS
RESULTS BY SAMPLE;
Sample ID: GD #219, 10 FT. #625 DUP. LabID: 9509054-11A CoUected: 09/25/95 12:02:00
TEST RESTJLT TJNITS DETECTION .ANfALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl- 2-pentemone
2 -hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
! U
! U
! U
! U
U
U
u
u u
u
u 860484
463150
182729
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
dibromofluorometheme
1,2 -di chloroetheme-d4
toluene-d8
bromofluorobenzene
10
10
10
10
10
10
10
1-0
10
10
10
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
For Volatile Organici
%Recovery
89.5
78.5
110
103
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
B 8260S
SW-846,8260A
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.
53.
85.
80.
4
3
6
6
TO 112
TO 121
TO 143
TO 130
Sample ID: GD #206, 5 FT. #625 LabID: 9509054-12A CoUected: 09/25/95 13:35:00
TEST
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
RESTJLT
10/10/95
8.15
0.48
13.8
U
U
0.01
U
U
U
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.4
0.1
0.3
1.6
0.2
0.011
330
330
330
AN.I^YZED
10/10/95
10/13/95
10/13/95
10/13/95
10/13/95
10/13/95
10/25/95
10/23/95
10/23/95
10/23/95
BY
SJM
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
.108-95-2
111-44-4
95-57-8
3050
6010
6010
6010
6010
6010
7471
8270
Page ff: 39
Sample ED: GD #206, 5 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9509054-12A CoUected: 09/25/95 13:35:00
TEST ,
Semi-Volatile Organics
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethcme
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4 -chloroaniline
hexachlorobutadiene
4-chloro-3-me thyIpheno1
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroaniline
dimethylphthalate
acenaphthylene
3-nitroemiline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dini trotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroemiline
4,6-dinitro-2-methylphenol
n-ni trosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenemthrene
anthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a) emthracene
3,3'-dichlorobenzidine
bis(2-echyIhexyl)phchalace
RESULT
U
u n u u u
u u u u u u D
U
U
u D
U
U
D
D
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u u u
u D
U
U
D
u
u 37 J
U
U
D
U
U
U
TJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
• ANALYZED
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7 ^
88-74-4 ^
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-31-7
Page tt: 40
Novembers, 1995 13:54 CERTIFICATE OF AN^y^YSIS
RESULTS BY SAMPID
Sample ED: GD #206, 5 FT. #625 LabID: 9509054-12A CoUected: 09/25/95 13:35:00
TEST
Semi-Volatile Organics
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h)anthracene
benzo(g,h,i)perylene
Volatile Organics
J|^zene
^^^mobenzene
^IRmochl orome theme
bromodi chlorometheme
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
RESTJLT
U
U
U
U
U
U
U
U
TJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2-fluorophenol
phenol-d5
ni
2-
2,
.trobenzene -d5
fluorobiphenyl
4,6-tribromophenol
terphenyl-dl4
1,2-dibromo-3-chloroprop
1,2-dibromoethane
dibromomethane
dichlorodifluorometheme
1,1-dichloroetheme
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2-dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropeme
2,2-dichloropropeme
1,l-dichloropropene
cis-1,3-dichloropropene
)em
U
O
U
U
U
U
u
u
u
u u
u D
u u
u u
u
u u
u
u
u
u
u
u
u
u
u
u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
33T)
ANALYZED
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270S
%Recovery
51.92
56.32
52.17
61.50
94.96
123.0
10
10
10
10
10
10
10
10
10
10
10
10
10
10 •
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
\
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
Page tt: 41
November 3, 1995 13:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #206, 5 FT. #625 LabID: 9509054-12A CoUected: 09/25/95 13:35:00
TEST
Volatile Organics
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4 -dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroetheme
t e t rachl oroe thene
toluene
1,2,3 -trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane /
1,1,2-trichloroethane •
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentemone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESTJLT
U
u u
u u
u
u
u
u
u
u
u u
u
u
u
u O
u
u
u
u
u
u
u
u
u
u u u
u
u 751153
290727
88053
TJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
ID
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorometheme
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
%Recovery
80.5
71.7
136
115
METHOD/CAS#
SW-846,82eOA
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4 ^
96-18-4 ••
95-63-6 ^^
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Page #: 42
Novembers, 1995 13:54 CERTIFICATE OF AN^U^YSIS
RESULTS BY SAMPLE
Sample ID: GD #206, 5 FT. RINSE BLANK Lab ID: 9509054-13A CoUected: 09/25/95 13:40:00
TEST
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi'Volatile Organics
phenol
bis(2-chloroethyl)ether
2-chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
^^e thy Iphenol
^^(2-chloroisopropyl) ethe
4^methylphenol
n-nitroso-di-n-propyleunine
hexachloroetheme
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis (2-chloroethoxy)metheme
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4 -chloroaniline
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2-chloronaphthalene
2-nitroemiline
dimethylphthalate
acenaphthylene
3-nitroaniline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dinitrotoluene
2^^ dinitrotoluene
RESTJLT
10/10/95
52
3.05
U
U
U
U
U
U
U
U
O
U
U
U
U
. U
u u
u
a u u u U
D
U
U
u
u u u u u u u
u u u
u
u u u
u
TJNITS
DATE
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
6
2
5
25
3
0.15
1.5
5.7
3.3
1.9
4.4
1.9
2.3
5.7
4.0
12
1.6
1.4
2.2
3.6
2.7
5.3
2.7
1.9
1.6
1.8
0.90
3.0
2.2
6.0
2.7
4.0
1.9
1.5
1.6
3.5
2.4
1.9
42
2.4
3.0
1.9
5.7
ANALYZED
10/10/95
10/12/95
10/12/95
10/12/95
10/12/95
10/12/95
10/06/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/;25/95
BY
LVD
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA.
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
3010
6010
6010
6010
6010
6010
7470
8270
Page tt: 43
November 3, 1995 13:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #206, 5 FT. RINSE BLANK Lab ID: 9509054-13A CoUected: 09/25/95 13:40:00
TEST
Semi-Volatile Organics
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroemiline
4,6-dinitro-2-methyIphenol
n-nitrosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenemthrene
emthracene
di-n-butylphthalate
fluoremthene
pyrene
butylbenzylphthalate
benzo(a) emthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoremthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3 -cd)pyrene
dibenz(a,h)anthracene
benzo(g,h, Dperylene
Volatile Organics
benzene
bromobenzene
bromochl or ome thame
bromodi chlorome theme
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
RESTJLT
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
V
16 B
U
U
u
u
a
u
u D
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Surrogate/Recovery Data
Surrogate
2 -fluorophenol
phenol -d5
nitrobenzene-d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
u
u
u
u
6.5
u
u
u
u
u
u
u
8.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
1.9
4.2
1.9
3.6
24
1.9
1.9
1.'9
3.6
5.4
1.9
2.5
2.2
1.9
2.5
7.8
10
2.5
2.5
2.5
5.0
4.8
2.5
3.7
2.5
4.1
ANALYZED
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9 ^^
50-32-8 flB
193-39-5 ^^
53-70-3
191-24-2
Por Semi-Volatile Organics 8270
%Recovery
32.1
22.5
41.3
45.3
71.5
136
0.20
0.20
0.20
0.30
0.10
0.40
0.20
0.20
0.20
0.30
0.20
0.40
0.40
Recovery Limits
21
10
35
43
10
33
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
TO 100
TO 94
TO 114
TO 116
TO 123
TO 141
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
Page #: 44 •
November 3, 1995 13:54 CERTIFICATE OF AP^/O^YSIS
RESULTS BY SAMPLE
Sample ID: GD #206, 5 FT. RINSE BLANK Lab ID: 9509054-lSA CoUected: 09/25/95 13:40:00
TEST RESULT TJNITS DETECTION AN.I^YZED BY
LIMIT
METHOD/CAS#
Volatile Organics
ch1orome thane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3-chloropropan
1,2-dibromoethane
dibromomethane
dichlorodifluoromethane
1,1-dichloroethane
1,2 -di chloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans -1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis-1,3 -dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene IjL - di chl orobenzene
lylbenzene
xachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentanone
2 - hexemone
fluorobenzene
.cUorobenzene - d5 m
u
u u 3.4
U
U
U
U
U
U
U
U
U
U
O
U
U
u u u
u u u u u u 2.6B
U
U
U
U
u u
1.3
U
U
U
U
1.4
• U
U
U
u u u u 170B
23
U
5.2J
816474
613949
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
0.60
0.20
0.20
0.30
0.20
0.20
0.20
0.20
0.10
0.20
0.60
0.20
0.20
0.20
0.20
0.20
0.20
0.20
0.20
0.10
0.20
0.20
0.30
0.20
0.20
0.20
0.30
0.20
0.20
0.20
0.20
0.30
0.90
0.30
0.20
0.20
0.20
0.20
0.30
0.30
0.20
0.20
0.20
0.40
0.20
0.20
10
10
10
10
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
Page ft: 45
November 3, 1995 13:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #206, 5 FT. RINSE BLANK Lab ID: 9509054-13A CoUected: 09/25/95 13:40:00
TEST
Volatile Organics
1,4-dichlorobenzene
RESULT UNITS
-d4 269 797 ug/L
DETECTION ANALYZED BY METHOD/CAS#
LIMIT
SW-846,8260A
10/05/95 MMR INTSTD3
Surrogate/Recovery Data For Volatila Organics 8260
Surrogate
dibromofluoromethane
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
%Recovery Recovery Limits
100 80.0 TO 120
102- 80.0 TO 120
101 80.0 TO 120
103 80.0 TO 120
Sample ID: GD #206, 10 FT. #625 LabID: 9509054-14A CoUected: 09/25/95 13:55:00
TEST RESTJLT TJNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercury
Semi-Volatile Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis{2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)metheme
10/10/95
13.2
U
16.4
U
U
U
U
U
U
U
U
U
U
U
U
U
u u
u
u u u
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.4
0.1
0.3
1.5
0.2
0.011
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
10/10/95
10/13/95
10/13/95
10/13/95
10/13/95
10/13/95
10/25/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
SJM
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
3050
6010
6010
6010
6010
6010
7471
8270
Page tt: 46
pie ID: GD #206, 10 FT. #625
CERTIFICATE OF A>MiLYSIS
RESULTS BY SAMPLE
Lab ID: 9509054-14A CoUected: 09/25/95 13:55:00
TEST •
Semi-Volatile Organics
2,4 -dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4-chloroaniline
hexachlorobutadiene
4-chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroemiline
dimethylphthalate
acenaphthylene
3-nitroaniline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
^^hlorophenyl -phenylether
I^Hsrene
^pitroaniline
4,6-dinitro-2-methylphenol
n-nitrosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenanthrene
anthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h) emthracene
benzo(g,h,i)perylene
RESULT
n
n n
u n
u
u u
u u n u u u
u D
D
D
u n u
u D
u u u D
u u u
u u 63 J
u u u u D
u u u
u D
u
u D
U
TJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
• ANi^YZED
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/:24/95
10/:24/95
10/24/95
10/24/95
10/24/95
10/:',4/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
120-83-2
120-82-1
91-20-3
106-47-3
87-63-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-53-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-3
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-31-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-a
193-39-5
53-70-3
191-24-2
Page #: 47
November 3, 1995 13:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #206, 10 FT. #625 LabID: 9509054-14A CoUected: 09/25/95 13:55:00
TEST
Semi-Volatile Organics
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodi chlorometheme
bromoform
bromome theme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
RESTJLT UNITS
Surrogate/Recovery Data
Surrogate
2 -fluorophenol
phenol -d5
nitrobenzene -d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
1,2-dibromo-3 -chloropropem
1,2-dibromoetheme
dibromomethane
dichlorodifluoromethane
1,1-dichloroetheme
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropeme
1,1-dichloropropene
cis-1,3 -dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
U
U
O
D
U
U
U
u u D
D
U
U
U
u u u u
u u u u
u u
u u u D
u u u
u u u D
u
u u
u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
ANALYZED BY METHOD/CAS#
SW-846, 8270
For Semi-Volatile Organics 8270S
%Recovery
71.08
75.44
66.29
72.34
82.44
127.8
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5 ^^
108-90-7 ^Bl
75-00-3 ^^
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
Page tt: 48
November 3, 1995 13:54
Sample ID: GD #206, 10 FT. #625
CERTIFICATE OF ANiU^YSIS
RESULTS BY SAMPLE
LabID: 9509054-14A CoUected: 09/25/95 13:55:00
TEST
Volatile Organics
naphthalene
n-propylbenzene
styrene
1,1,1,2 -tetrachloroethane
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
^^ethyl - 2 -pentemone
^^Bexanone
^lorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESTJLT
U
U
U
U
U
U
U
U
U
u u
u u u D
U
U
U
U
U
u u u 988340
547912
217391
TJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
ID
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluoromethane
1,2-dichloroetheme-d4
toluene-d8
bron lof luoro) 3enz ene
%Recovery
91.6
82.8
108
102
METHOD/CAS#
SW-846,8260A
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 13 0
Sample ID: GD #96, 5 FT. #625 LabID: 9509054-15A CoUected: 09/25/95 14:10:00
TEST RESTJLT TJNITS DETECTION AN-IOiYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Boron
Cadmium
romium Chro
10/10/95
7.87
0.65
20.0
DATE
ug/g
ug/g
ug/g
0.4
0.1
0.3
10/10/95
10/13/95
10/13/95
10/13/95
SJM
LVD
LVD
LVD
SW-846,.
SW-84 6,
SW-846,
SW-846,
3050
6010
6010
6010
Page tt: 49
November 3, 1995 13:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #96, 5 FT. #625 LabID: 9509054-15A CoUected: 09/25/95 14:10:00
TEST
Lead
Silver
Mercury
Semi-Volatile Organics
phenol
bis(2 -chloroethyl)ether
2-chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)metheme
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4-chloroaniline
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroemiline
dimethylphthalate
acenaphthylene
3-nitroaniline
acenaphthene
2,4 -dini trophenol
4-nitrophenol
dibenzofurem
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroemiline
4,6-dinitro-2-methylphenol
n-ni trosodiphenylamine
4 -bromophenyl-phenylether
hexachlorobenzene
RESTJLT
U
U
u
u
u
u u u u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u o u u u
u u u
' u
u
u
u
u
u
u
u
u u
u
u
u
UNITS
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
1.6
0.2
0.012
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
ANALYZED
10/13/95
10/13/95
10/25/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
BY
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9 ^^
111-91-1 ^B
120-83-2 ^^
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
Page tf: 50 •
November 3, 1995 13:54 CERTIFICATE OF AN^O^YSIS
RESULTS BY SAMPLE
Sample ID: GD #96, 5 FT. #625 LabID: 9509054-15A CoUected: 09/25/95 14:10:00
TEST
Seml-Volatlle Organici
pentachlorophenol
phenemthrene
anthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a) emthracene
B
3,3'-dichlorobenzidine
bis(2 -ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoremthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h)anthracene
benzo(g,h,i)perylene
A w
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodichlorometheme
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
RESULT
U
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -fluorophenol
phenol -d5
nitrobenzene -d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
1,2-dibromo-3 -chloropropan
1,2-dibromoethane
dibromomethane
di chlorodi f1uorometheme
u u u u u D
U
u u
u u u u
u u D
U
U
u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
JkN.ilLYZED
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Siami-Volatile Organics 827OS
%Recovery
48.80
51.36
47.96
51.66
52.32
81.14
10
10
10
10 •
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
Page #: 51
November 3, 1995 13:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #96, 5 FT. #625 LabID: 9509054-15A CoUected: 09/25/95 14:10:00
TEST
Volatile Organics
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropeme
2,2-dichloropropeme
1,1-dichloropropene
cis-1,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroetheme
tet rachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m, p-xylene
acetone
2-butemone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
U
u u u u u
u
u
u u u
u u u u
u u u u D
u u u u u u
u u u u u u u
u
u D
u
u u
u
u
u 952813
428627
137790
TJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
lb
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
10/06/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorometheme
1,2-di chloroetheme-d4
%Recovery
83.9
70.1
METHOD/CAS#
SW-846,8260A
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5 g^
630-20-6 ^m
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
TO 112
TO 121
Page tt: 52
CERTIFICATE OF A^[/^XYSIS
RESULTS BY SAMPLE
#P le ED: GD #96, 5 FT. #625 LabID: 9509054-15A CoUected: 09/25/95 14:10:00
TEST RESULT UNITS DETECTION AN/iLYZED BY
LIMIT
METHOD/CAS#
Volatile Organics toluene-d8
bromofluorobenzene
126
110
85.5 TO 143
80.6 TO 130
SW-846,3260A
Sample ID: GD #96, 5 FT. #625 DUP. LabDD: 9509054-16A CoUected: 09/25/95 14:10:00
TEST
Semi-Volatile Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
^^|chloroethane
^^Bobenzene
^rophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4 -chloroani1ine
hexachlorobutadiene
4 -chloro-3 -methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroaniline
dime thyIphthalate
acenaphthylene
3-nitroemiline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofurem
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
RESULT
U
n
u
n n D
n D
u u u n u u
u u u u D
u n u u u D
U
U
U
U
U
U
u
u
u
n n u 43 J
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
A]:TALYZED
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-33-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
38-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-23-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
Page it: 53
November 3, 1995 13:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #96, 5 FT. #625 DUP. LabID: 9509054-16A CoUected: 09/25/95 14:10:00
TEST
Semi-Volatile Organics
fluorene
4-nitroemiline
4,6-dinitro-2-methylphenol
n-ni trosodiphenyleunine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenanthrene
anthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3 -cd)pyrene
dibenz(a,h) emthracene
benzo(g,h,i)perylene
RESTJLT
D
U
U
U
U
U
a
u u u
u u u u u D
u o
u u D
U
U
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -fluorophenol
phenol -d5
nitrobenzene-d5
2 -fluorobiphenyl
2,4,6-
terphe
tribromophenol
nyl-dl4
DETECTION
LIMIT
330
660
330
330
330
330
1700
33-0
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
10/24/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JHA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5 ^^
53-70-3 mM
191-24-2 ^^
For Semi-Volatile Organics 8270S
%Recovery
93.28
99.60
97.31
101.1
118.2
159.6
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
Page #: 54
•
Data Reporting QualifKjrs
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either v^'hen estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but tlie result is less than the specified
detection limit but greater than zero. (e.g. 1. IJ witli a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instniment.
BDL Indicates an analyte which was below the detection Umiits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified Umits. If surrogate recoveries are out
of limits, any values reported are for indication only.
#
ENVIRONMENTAL LAB WORK RJEC^UEST f'^^f^^;
THIOKOL ENVraONMENTAL LABORATORY LWR No. E11062
A F" /Ua//^z ^2ZC
COST CENTF:R
/M34C
WORK ORDER
9-Z7^9r
ORGANIZATION
/di/iirOAfiun/^
MAIL STOP
10/t:
REPORT RESULIS TO:
HELEN WARD, MS 301
/
/
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TYPE
G
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SAMPLE INFORMATION
LOCATION
^<^/M(/ ^(^z<r'
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TIME
l^/C
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TEST
l/o/J ' '3z<^o
REMARKS
""///^.t^t^'J'^"*'^"^
^c -14 2.
B, Cd.Cr^Aci^Pi. /v:
l/ziA - <8ZipO
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CHAIN OF CUSTODY
RELINQUISHED BY
djjfl/^//^ 4n-irr^o
DATE TIME RECEIVED B^' DATE TIME
Z7///rrrA4^<^'?-y~4^' Z^^^
«
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED
ENVIRONMENTAL LAB WORK REQUEST ^09^^ J
4 TinOKOL ENVraONMENTAL LABORATORY LWRNo. LIIOI^'^
A.f^. IdJ/}//^ ssio
COST csncR
tpzdo :=^^ IB940
ORGANIZATION
g/i[//ro/(MnZad ZOlE
RETORT RESULIS TOi
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMiUlKS
'/'•Z7'W y iU-14^ 0840 Sb, A-i, Ct) pb , ^S^^f^ih-
Pdi
2JL ^-lUi-y I ^6)56 ll
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11 t'zr-fs «/' M-1'^ /o5r<. VOA - 821,0 (, SoirtleS)
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i\ y d fSJ^ ^^<^ •^6"
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// /I ^
CHAIN OF CUSTODY
Rn,INQUISIIEDBY DATE TIME RECEIVED BY DATE TIME
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED SICNATLTIE
ENVIRONMENTAL LAB WORK RE,QUEST ff^f/^J
^- TinOKOL ENVIRONMENTAL LABORAT6RY
i
W FROM:
AF UdQ/lTi/y
ORGANIZATION
EXTBXSION
MAILSTOP
LWR No. ^///)CJ Z^
cosTcairTai WORK ORDER '
9-z7-fr-
RO>ORT RESULIS TOi
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPIX
I/I£L
DATE TYPE
^•Z/9^-
LOCATION TIME TEST RE^LVRKS
/t^-lL 5uiAiU4-^\ti I4t<t> IZoA- 321,0
ll n y ll n A$, ge-. Cd, c<, Cu, n, KJ,, Tl, a^
^£1:. II y 1/ mi ^:^ iZ/
/I ll y /I d ^cc ^^Z-
If y' /' ll 7S^s^^
z^A // y /I mo <^cc^ I
ll y // 1440 ^^^^Z^
CHAIN OF CUSTODY
RELINQUISHED BY DATE TIME RECEIVED BY DATE TIME
FOR LABORATORY USE ONLY
DATE COMPLETED
1
DATE REPORTES SIGNATURE
November 7, 1995 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmemal Monitoring
TO: Helen Ward MIS 301
Thiokol Corp. Ut 84322
A.F. WALKER
EXT 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Oty, Ut 84302-0707
Analytical Labs MIS 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order jjf 9509063
LabID:
OIA
Sample ID:
GD #96, 10 FT. #625
LabID:
02A
Lab ID:
03A
Sample ID:
GD #96, 10 FT. #625 DUP.
Sample ID:
GD #14^ 5 FT. #625
LabID:
04A
Sample ID:
GD #14, 5 FT. #625 DUP.
UbID:
~O5A
Sample ID:
GD #14, 10 FT. #625
Sample and Test Code Identification
Test Codes and Names
LabID:
06A
Sample ID:
SWMU #395 SURFACE, M-348
LabID:
07A
Sample ID:
SWMU #395 2 FT., M-348
3050
B AE2
CD AE2
CR AE2
PB AE2
AG AE2
HO CV2
827DS
8260S
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercuiy
Semi-Volatile Organics
Volatile Organics
Test Codes and Names
8270S Semi-Volatile Organics
Test Codes and Names
3050
B AE2
CD AE2
CR AE2
PB AE2
AG AE2
HG~CV2
8270S
8260S
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercuiy
Semi-Volatile Otganics
Volatile Organics
Test Codes and Names
3050
B AE2
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
Acid Digestion
Boron
Cadnuum
Chromium
Lead
Silver
Mercury
Test Codes and Names
3050
B AE2
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8270s
8260S
Acid Digestion
Boron
Cadmium
Chromium
Lead
Silver
Mercuty
Semi-Volatile Organics
Volatile Oiganics
Test Codes and Names
PH
3050
CR AE2
PB AE2
SB OF2
AS GF2
S04IC2
pH
Acid Digestion
Chromium
Lead
Antimony
Arsenic
Sulfate
Test Codes and Names
PH pH
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-g46, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A Method
SW-846, 8270
Method
SW-846, 3050
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A
Method
SW-846, 3050
SW-g46, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846,8260A Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 7041
SW-846, 7060
SW-846, 9056 Method
EPA 150.1
Page#:lof ^^
Work Order iif 9509063
ibID: .Sample TD:
SWMU #395 #abl]
LabID:
08A
2 FT., M-348
Sample ID:
RINSE BLANK, M-72
LabID:
09A
Sampli
3Dm GD#31,5FT. #630, M-72
LabID:
lOA
Sample ID:
«7, 5 FT. #630, M-72 GD
LabID:
llA
Sample ID:
GD «?, 10 FT. #630, M-72
LabID:
12A
Sample ID:
GD #3, 5 FT. #630, M-72
Sample and Test Code Identificaition
Test Codes and Names
LabID:
13A
Sample ID:
OD«,5FT. #630,M-72 DUP
3050
CR AE2
PB AE2
SB 0F2
AS OF2
SO?IC2
Acid Digestion
Chromium
Lead
Antimony
Arsenic
Sulfate
Test Codes and Names
3010
AS AE2
BE AE2
CD AE2
CR AE2
CU AE2
PB AE2
NI AE2
TL~AE2
ZN AE2
8260
Acid Digestion
Arsenic
Beryllium
Cadinium
Chromium
Copper
Lead
Nickel
Thallium
Zinc
Volatile Organics
Test Codes and Names
3050
BE AE2
CD AE2
CR AE2
CU AE2
PB AE2
NI AE2
Zrr AE2
AS OF2
TL GF2
i26bS
Acid Digestion
Beiyllium
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Thallium
Volatile Organics
Test Codes and Names
3050
BE AE2
CD"AE2
CR AE2
CU AE2
PB~AE2
N1""AE2
ZSr AE2
AS GF2
TL~OF2
82£1>S
Acid Digestion
Beryllium
Cadinium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Thallium
Volatile Organics
Test Codes and Names
3050
BE AE2
CD~AE2
CR AE2
CU AE2
PB AE2
NI"AE2
ZN AE2
AS GF2
TL 0F2
82^
Acid Digestion
Beiyllium
Cadinium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Thallium
Volatile Otganics
Test Codes and Names
3050
BE AE2
CD AE2
CR AE2
CU AE2
PB AE2
NI AE2
ZN"AE2
AS~OF2
TL GF2
826DS
Acid Digestion
Betyllium
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Thallium
Volatile Organics
Test Codes and Names
8260S Volatile Organics
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 7041
SW-846, 7060
SW-846, 9056
Method
SW-846, 3010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-g46, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7841
SW-846,g260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7841
SW-846,8260A Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7841
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-84«, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7841
SW-846,8260A Method
SW-846,8260A
Page tf:2
Work Orderly 9509063 Sample and Test Code Identification
LabID: Sample ID:
14A GD«riOFT. #630, M-72
Test Codes and Names
LabID:
15A
Sample ID:
GD th, 5 FT. #630, M-72
LabID: .Sample TD:
16A GD #5, 5 FT. #630,M-72 DUP
LabID: Sample ID i 17A GD #5, 10 FT. #630, M-72
3050
BE AE2
CD AE2
CR AE2
CU~AE2
PB AE2
NI AE2
ZN AE2
AS GF2
TL GF2
8260S
Acid Digestion
BeryUium
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Thallium
Volatile Oiganics
Test Codes and Names
3050
BE AE2
CD AE2
CR AE2
CU AE2
PB AE2
NI AE2
ZN"AE2
AS GF2
TL GF2
82£DS
Acid Digestion
Beryllium
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Thallium
Volatile Organics
Test Codes and Names
3050
BE AE2
CD AE2
CR'"AE2
CU AE2
PB AE2 NI AE2
Z1^AE2
AS GF2
TL_GF2
Acid Digestion
Beryllium
Cadmium
Chroinium
Copper
Lead Nickel
Zinc
Arsenic
Thallium
Test Codes and Names
3050
BE AE2
CD"AE2
CR AE2
CU"AE2
PB AE2
NI AE2
ZtT AE2
AS GF2
TL GF2
i26bs
Acid Digestion
Beryllium
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Thallium
Volatile Organics
Comments
/UPirC^'^'^
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7841
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7841
SW-846,8260A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7841
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7841
SW-846,8260A
Certried By
Page #:3
o
This is to certify tfiat tfie following samples were analyzed using good laboratory practices
to sfiow the following results.
Sample ID: GD #96, 10 FT. #625 LabID: 9509063-01A CoUected: 09/26/95 15:10:00
TEST
Aclti Digestion
Boron
Cadmium
Chiromlum
Lead
Silver
Mercury
Seml-Volatlle Organics
phenol
bis(2-chloroethyl)ether
2-chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
Jm2-di chlorobenzene
^Methylphenol
^K (2-chloroisopropyl) ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethcme
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4-chloroaniline
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5- trichlorophenol
2 -chloronaphthalene
2-nitroaniline
dimethylphthalate
acenaphthylene
3 -nitrocufiiline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofurem
2j6-dinitrotoluene
RESITLT
10/10/95
4.31
U
12.2
D
U
U
U
U
D
U
U
U
U
D
U
D
U
u u u u D
U
U
U
D
U
U
D
tr
u D
u u u
u u u
u u
u u
TJNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.4
0.1
0-3
1.6
0.2
0.012
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
ANALYZED
10/10/95
10/13/95
10/13/95
10/13/95
10/13/95
10/13/95
10/25/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
BY
SJM
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-84 6,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
3050
6010
6010
6010
6010
6010
7471
8270
# Page tt: A
November 7, 1995 09:50
Sample ID: GD #96, 10 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9509063-01A CoUected: 09/26/95 15:10:00
•
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Seml-Volatlle Organics
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroaniline
4,6-dinitro-2-methylphenol
n-nitrosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenanthrene
anthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
27
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoremthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h) emthracene
benzo(g,h, Dperylene
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chlorometheme
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
U
U
U
U
U
U
U
U
U
u u u BJ
U
u u
u u
u u u u u u u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
usr/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -fluorophenol
phenol-d5
nitrobenzene -dS
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
u u u D
D
U
U
u u
u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8270
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Seml-Volatlle Organics 8270S
%Recovery
67.72
66.36
64.37
68.62
85.48
134.2
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
Page tt: 5
November 7, 1995 09:50
S^ ^mple ID: GD #96, 10 FT. #625
CERTIFICATE OF ANiU^YSIS
RESULTS BY SAMPLE
LabID: 9509063-01A CoUected: 09/26/95 15:10:00
TEST
Volatile Organics
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3 -chloropropan
1,2-dibromoethane
dibromometheme
dichlorodifluorometheme
1,1-dichloroetheme
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2 -dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropeme
2,2-dichloropropeme
1,1-dichloropropene
cis-1,3 -dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
^^ -dichlorobenzene
^Bj -dichlorobenzene
^B^y Ibenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propyIbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroethane
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
RESULT
10
U
u
u
u u
u u u
u
u n
u u u u u u u D
u u u
u
u . u
u 6. 63 J
D
U
D
D
U
u
u
u u
D
U
U
D
U
U
U
U
U
U
U
U
U
U
740687
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
J^ALYZED
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
# Page tt: 6
November 7, 1995 09:50
Sample ID: GD #96, 10 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9509063-OlA CoUected: 09/26/95 15:10:00
#
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
chlorobenzene-d5
1,4-dichlorobenzene-d4
311409
102502
ug/Kg
ug/Kg
SW-846,8260A
10/09/95 MMR INTSTD2
10/09/95 MMR INTSTD3
Surrogate/Recovery Data For Volatile Orgemics 8260S
Surrogate ^Recovery
dibromofluorometheme 84.2
l,2-dichloroetheme-d4 74.6
toluene-d8 125
bromofluorobenzene 110
Racovery Limits
58.4 TO 112
53.3 TO 121
85.6 TO 143
80.6 TO 130
Sample ID: GD #96, 10 FT. #625 DUP. LabID: 9509063-02A CoUected: 09/26/95 15:10:00
TEST
Seml-Volatlle Organics
phenol
bis(2 -chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)metheme
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4-chloroaniline
hexachlorobutadiene
4-chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroaniline
dimethylphthalate
acenaphthy1ene
3-nitroemiline
RESULT
U
u
u u u u u
u
u
u u u
u
u a n u D
u u u u u u
u u
u o u
u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
ANALYZED
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS«
SW-846, 8270
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
\
•
Page tt: 1 ^
November 7, 1995 09:50
•
CERTIFICATE OF AIV^iLYSIS
i , RESULTS BY SAMPLE;
Sample ID: GD #96, 10 FT. #625 DUP. LabID: 9509063-02A CoUected: 09/26/95 15:10:00
TEST RESULT UNITS DETECTION Al^ALYZED BY
LIMIT
METHOD/CAS#
Seml-Volatlle Organics
acenaphthene U ug/Kg 330 11/01/95 JMA
2,4-dinitrophenol U ug/Kg 330 11/01/95 JMA
4-nitrophenol U ug/Kg 1700 11/01/95 JMA
dibenzofuran U ug/Kg 330 11/01/95 JMA
2,6-dinitrotoluene U ug/Kg 330 11/01/95 JMA
2,4-dinitrotoluene U ug/Kg 330 11/01/95 JMA
diethylphthalate U ug/Kg - 330 11/01/95 JMA
4-chlorophenyl-phenylether U ug/Kg 33-0 11/01/95 JMA
fluorene U ug/Kg 330 11/01/95 JMA
4-nitroaniline U ug/Kg 660 11/01/95 JMA
4,6-dinitro-2-methylphenol U ug/Kg 330 11/01/95 JMA
n-nitrosodiphenylamine U ug/Kg 330 11/01/95 JMA
4-bromophenyl-phenylether U ug/Kg 330 11/01/95 JMA
hexachlorobenzene U ug/Kg 330 11/01/95 JMA
pentachlorophenol U ug/Kg 1700 11/01/95 JMA
phenanthrene U ug/Kg 330 11/01/95 JMA
anthracene U ug/Kg 330 11/01/95 JMA
di-n-butylphthalate 18 BJ ug/Kg 330 11/01/95 JMA
fluoremthene U ug/Kg 330 11/01/95 JMA
pyrene U ug/Kg 330 11/01/95 JMA
butylbenzylphthalate U ug/Kg 330 11/01/95 JMA
^Mnzo (a) emthracene U ug/Kg 330 11/01/95 JMA
^^'-dichlorobenzidine U ug/Kg 330 11/01/95 JMA
^ffs (2-ethylhexyl)phthalate U ug/Kg 330 11/01/95 JMA
chrysene U ug/Kg 330 11/01/95 JMA
di-n-octylphthalate U ug/Kg 330 11/01/95 JMA
benzo(b)fluoremthene U ug/Kg 330 11/01/95 JMA
benzo(k)fluoremthene U ug/Kg 330 11/01/95 JMA
benzo(a)pyrene U ug/Kg 330 11/01/95 JMA
indeno(1,2,3-cd)pyrene U ug/Kg 330 11/01/95 JMA
dibenz(a,h)anthracene U ug/Kg 330 11/01/95 JMA
benzo(g,h,i)perylene U ug/Kg 330 11/01/95 JMA
SW-846, 8270
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01
117-84
205-99
207-08
50-32-8
193-39-5
53-70-3
191-24-2
Surrogate/Recovery Data For Seml-Volatlle Organics 8270S
Surrogate %Recovery
2-fluorophenol 74.80
phenol-d5 72.92
nitrobenzene-d5 73.29
2-fluorobiphenyl 73.77
2,4,6-tribromophenol 84.36
terphenyl-dl4 136.6
Recovery Limits
25 TO 121
24 TO 113
23 TO 120
30 TO 115
19 TO 122
18 TO 137
Page tf: 8
November 7, 1995 09:50 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #14,5 FT. #625 Lab ID: 9509063-03A CoUected: 09/26/95 15:35:00
TEST
Add Digestion
Boron
Cadmium
Chromium
Lead
Silver
Merciiry
Seml-Volatlle Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)metheme
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4 -chloroaniline
hexachlorobutadiene
4-chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroaniline
dimethylphthalate
acenaphthylene
3 -ni troemi1ine
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dinitrotoluene
^,4 -dini trotoluene
RESULT
10/10/95
12.4
O
19.9
U
u
u
u
u o u u u u
D
a • u
u u u
u D
u
a u u u u u
u
u u u u u n
u u u
a u u u u
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.4
0.1
0.3
1.6
0.2
0.011
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
ANALYZED
10/10/95
10/16/95
10/16/95
10/16/95
10/16/95
10/16/95
10/25/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
BY
SJM
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-i
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
3050
6010
6010
6010
6010
6010
7471
8270
^ V
^^
Page tt: 9
November 7, 1995 09:50 CERTIFICATE OF AN^iLYSIS
RESULTS BY SAMPLE
Sample ID: GD #14, 5 FT. #625 LabID: 9509063-03A CoUected: 09/26/95 15:35:00
TEST
Seml-Volatlle Organics
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroaniline
4,6-dinitro-2-methylphenol
n-ni trosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenanthrene
emthracene
di-n-butylphthalate
fluoremthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
J^nzo (k) fluoranthene
^^izo (a) pyrene
^BWeno (1,2,3- cd) pyrene
dibenz (a,h) emthracene
benzo(g,h,i)perylene
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodichlorometheme
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
RESULT
46
U
u u u u D
U
U
U
U
U
BJ
U
U
D
U
U
30
U
U
U
a u
u u D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2-fluorophenol
phenol -d5
nitrobenzene-dS
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
n.
u u
u u u D
u u u u u 20
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
JI^ALYZED
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Seml-Volatlle Organics 8270S .
%Racovery
50.28
49.92
47.32
52.08
89.12
129 .8
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
Page tt: 10
November 7, 1995 09:50
Sample ID: GD #14, 5 FT. #625
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9509063-03A CoUected: 09/26/95 15:35:00
•
TEST
Volatile Organics
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3-chloropropan
1,2-dibromoetheme
dibromometheme
dichlorodifluoromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2 -dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropame
2,2-dichloropropeme
1,l-dichloropropene
cis-1,3 -dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachl orobutadi ene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4 -methyl -2 -pentemone
2-hexanone
fluorobenzene
chlorobenzene-d5
RESULT
U
u u u a D
u u u D
u D
u u
u
u u u u D
u u u
u u u 7.6BJ
U
U
U
U
U
U
U
u u u u u
u u
u u D
U
u u u u u 817247
406200
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7 ^^
100-41-4 JA
87-68-3 ^^
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
Page#: II
November 7, 1995 09:50
S^l pie ID: GD #14, 5 FT. #625
CERTIFICATE OF ANiU^YSIS
RESULTS BY SAMPIJE
LabID: 9509063-03A CoUected: 09/26/95 15:35:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
1,4-dichlorobenzene-d4 152740 ug/Kg
Surrogate
dibromofluorometheme
1,2-dichloroetheme-d4
toluene-d8
bromofluorobenzene
lOy
For Volatile
%Recovery
89.4
82.7
116'
106
SW-846,8260A
i'O 9/9 5 MMR INTSTD3
Organics 826OS
Recovery Limits
58.4 TO 112
53.3 TO 121
85.6 TO 143
80.6 TO 130
Sample ID: GD #14, 5 FT. #625 DUP. LabID: 9509063-04A CoUected: 09/26/95 15:35:00
TEST RESULT UNITS DETECTION ANJIkLYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
f ron
dmium
Chromium
Lead
Silver
Marcury
10/10/95
14.2
U
17.7
U
D
0.01
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
0.4
0.1
0.3
1.5
0.2
0.0098
10/10/95
10/16/95
10/16/95
10/16/95
10/16/95
10/16/95
10/25/95
SJM
LVD
LVD
LVD
LVD
LVD
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
7471
Sample ID: GD #14, 10 FT. #625 LabID: 9509063-05A CoUected: 09/26/95 15:45:00
TEST RESULT UNITS DETECTION ANJILYZED BY
LIMIT
METHOD/CAS#
Add Digestion
Boron
Cadmium
Chromiiun
10/10/95
14.0
U
14.0
DATE
ug/g
ug/g
ug/g
0.4
0.1
0.3
10/10/95
10/16/95
10/16/95
10/16/95
SJM
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
Page tt: 12
November 7, 1995 09:50 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #14, 10 FT. #625 LabID: 9509063-05A CoUected: 09/26/95 15:45:00
TEST
Lead
Silver
Mereury
Seal-Volatila Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)metheme
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4-chloroemiline
hexachlorobutadiene
4-chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroemiline
dimethylphthalate
acenaphthylene
3-nitroemiline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dinitrotoluene
2,4-dinitrotoluene
di e thyIphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroaniline
4,6-dinitro-2-methylphenol
n-nitrosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
RESULT
U
u
u
u u u u D
U
U
U
U
u u u u u u u u
u u u u u D
u D
U
U
u n
u u D
u u u D
u u D
u u u
u u u
UNITS
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
1.5
0.2
0.010
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
ANALYZED
10/16/95
10/16/95
10/25/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
BY
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1 ^^
120-83-2 ^B
120-82-1 ^^
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
Page #: 13
November 1, 1995 09:50
Sample ID: GD #14, 10 FT. #625
CERTIFICATE OF AN^^YSIS
r^ RESULTS BY SAMPI.E
Lab ID: 9509063-05A CoUected: 09/26/95 15:45:00
TEST RESITLT UNITS DETECTION AN.M:.YZED BY
LIMIT
METHOD/CAS#
Seml-Volatlle Organics
pentachlorophenol phenanthrene
anthracene di-n-butylphthalate fluoranthene
pyrene
butylbenzylphthalate
benzo(a) emthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoremthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h)anthracene
benzo (g,h, Dperylene
SW-846, 8270
U ug/Kg 1700 11/01/95 JMA 87-86-5
U ug/Kg 330 11/01/95 JMA 85-01-8
U ug/Kg 330 11/01/95 JMA 120-12-7
U ug/Kg 330 11/01/95 JMA 84-74-2
U ug/Kg 330 11/01/95 JMA 206-44-0
D ug/Kg 330 11/01/95 JMA 129-00-0
U ug/Kg 330 11/01/95 JMA 85-68-7
U ug/Kg 330 11/01/95 JMA 56-55-3
U ug/Kg 330 11/01/95 JMA 91-94-1
U ug/Kg 330 11/01/95 JMA 117-81-7
U ug/Kg 330 11/01/95 JMA 218-01-9
U ug/Kg 330 11/01/95 JMA 117-84-0
U ug/Kg 330 11/01/95 JMA 205-99-2
a ug/Kg 330 11/01/95 JMA 207-08-9
U ug/Kg 330 11/01/95 JMA 50-32-8
U ug/Kg 330 11/01/95 JMA 193-39-5
U ug/Kg 330 11/01/95 JMA 53-70-3
D ug/Kg 330 11/01/95 JMA 191-24-2
Surrogate/Recovery Data For Seml-Volatlle Organics 8270S
Surrogate
2 -fluorophenol
phenol-d5
nitrobenzene-d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
Volatile Organics
benzene
bromobenzene
bromochlorometheuie
bromodichlorometheme
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropem
1,2-dibromoetheme
dibromometheme
dichlorodifluoromethane
U
U
n
u
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
79.80
79.84
80.42
82.40
86.56
131.6
Recovery Limits
25 TO 121
24 TO 113
23 TO 120
30 TO 115
19 TO 122
18 TO 137
SW-846,8260A
10 10/09/95 MMR 71-43-2
10 10/09/95 MMR 108-86-1
10 10/09/95 MMR 74-97-5
10 10/09/95 MMR 75-27-4
10 10/09/95 MMR 75-25-2
10 10/09/95 MMR 74-83-9
10 10/09/95 MMR 104-51-8
10 10/09/95 MMR 135-98-8
10 10/09/95 MMR 98-06-6
10 10/09/95 MMR 56-23-5
10 10/09/95 MMR 108-90-7
10 10/09/95 MMR 75-00-3
10 10/09/95 MMR 67-66-3
10 10/09/95 MMR 74-87-3
10 10/09/95 MMR 95-49-8
10 10/09/95 MMR 106-43-4
10 10/09/95 MMR 124-48-1
10 10/09/95 MMR 96-12-8
10 10/09/95 MMR 106-93-4
10 10/09/95 MMR 74-95-3
10 10/09/95 MMR 75-71-8
Page#: 14
November 7, 1995 09:50 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #14, 10 FT. #625 LabID: 9509063-05A CoUected: 09/26/95 15:45:00
TEST
Volatila Organics
1,1-dichloroethame
1,2-dichloroethsme
1,1-dichloroethene
cis-1,2 -dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropane
2,2-dichloropropeme
1,1-dichloropropene
cis-1,3 -dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
i sopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethane
te trachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentemone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
U
U
u u u u u u u u u u u u u
u u a
u u
u u u u u u
u D
u
u
u D
u D
u u u u u U'
u
u 11932
6301
2633
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorometheme
1,2-dichloroetheme-d4
%Recovery
73.1
96.7
METHOD/CAS#
SW-846,8260A
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5 ^m^
630-20-6 ••
79-34-5 ^^
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
TO 112
TO 121
Page tt: 15 •
November 7, 1995 09:50 CERTIFICATE OF AN/kLYSIS
tv: RESULTS BY SAMPLE
Sample ID: GD #14, 10 FT. #625 LabID: 9509063-05A CoUected: 09/26/95 15:45:00
TEST RESULT UNITS DETECTION ANJ\LYZED BY METHOD/CAS#
LIMIT
Volatile Organics
toluene-d8
bromofluorobenzene
111
94.7
85.6 TO 143
80.6 TO 130
SW-846,8260A
Sample ID: SWMU #395 SURFACE, M-348 Lab ID: 9509063-06A CoUected: 09/27/95 08:40:00
TEST RESULT UNITS DETECTION ANJILYZED BY
LIMIT
METHOD/CAS#
pH
Acid Digestion
Chromium
Lead
^^ imony
^Hlenlc
Sulfate
8.39
10/10/95
18.5
94.7
2.2
7.3
35.3
pH Unit
DATE
ug/g
ug/g
ug/L
ug/g
ug/g
0.3
1.5
1
1.8
1
10/03/95
10/10/95
10/16/95
10/16/95
11/06/95
10/17/95
09/29/95
MTB
SJM
LVD
LVD
CRS
CRS
CRS
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 7041
SW-846, 7060
SW-846, 9056
Sample ID: SWMU #395 2 FT., M-348 Lab ID: 9509063-07A CoUected: 09/27/95 08:50:00
TEST REStJLT UNITS DETECTION ANJkLYZED BY
LIMIT
METHOD/CAS#
pH
Acid Digestion
Chromium
Lead
Antimony
Arsenic
Sulfate
9.59
10/10/95
26.8
U
U
6.0
24.7
pH Unit
DATE
ug/g
ug/g
ug/L
ug/g
ug/g
0
1
• 1
.3
.6
1
.9
1
10/03/95
10/10/95
10/16/95
10/16/95
11/06/95
10/17/95
09/29/95
^f^B
SJM
LVD
LVD
CRS
CRS
CRS
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 7041
SW-846, 7060
SW-846, 9056
Page tt: 16
November 7, 1995 09:50
Sample ID: RINSE BLANK, M-72
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9509063-08A CoUected: 09/27/95 10:55:00
•
TEST
Add Digestion
Arsenic
Beryllium
Cadmium
Chromltjm
Copper
Lead
Nickel
Thallium
Zinc
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodi chlorometheme
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropan
1,2-dibromoetheme
dibromometheme
di chlorodifluorometheme
1,1-dichloroethane
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2-dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropane
1,3 -di chloropropane
2,2-dichloropropane
1,l-dichloropropene
RESULT
10/10/95
U
U
U
U
12.8
U
U
D
156
U
U
U
U
U
U
U
u u u u u u
u
u
u
u u
u u u
u u u u
u u
u u
u
UNITS
DATE
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
50
2
2
5
2
25
10
50
4
0.20
0.20
0.20
0.30
0.10
0.40
0.20
0.20
0.20
0.30
0.20
0.40
0.40
0.60
0.20
0.20
0.30
0.20
0.20
0.20
0.20
0.10
0.20
0.60
0.20
0.20
0.20
0.20
0.20
0.20
ANALYZED
10/10/95
10/12/95
10/12/95
10/12/95
10/12/95
10/12/95
10/12/95
10/12/95
10/12/95
10/12/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
BY
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 3010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8260A^^
71-43-2 flB
108-86-1 ^^
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
Page tt: 17
November 7, 1995 09:50
Sample ID: RINSE BLANK, M-72
CERTIFICATE OF ANiU^YSIS
RESULTS BY SAMPIJ:
LabID: 9509063-08A CoUected: 09/27/95 10:55:00
TEST RESXTLT UNITS DETECTION J^ALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
cis-1,3 -dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroetheme
^•u. chloroe thene
(^H|chlorof1uoromethane
^^2,3 - trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-dS
1,4 -di chlorobenzene-d4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u u u
u u u u u
u u u u u u 47B
7.0 J
u 1.5 J
812796
616840
268836
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Surrogate/Recovery Data
Surrogate
dibromofluoromethane
1,2-'dichloroetheme-d4
toluene-d8
bromofluorobenzene
0.20
0.20
0.10
0.20
0.20
0.30
0.20
0.20
0.20
0.30
0.20
0.20
0.20
0.20
0.30
0.90
0.30
0.20
0.20
0.20
0.20
0.30
0.30
0.20
0.20
0.20
0.40
0.20
0.20
10
10
10
10
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
10/05/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
For Volatile Organics 8260
%Recovery
101
99.9
100
102
SW-a46,8260A
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Racovery Limits
80.0
80.0
80.0
80.0
TO 120
TO 120
TO 120
TO 120
Page tt: 18
November 7, 1995 09:50 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #31, 5 FT. #630, M-72 LabID: 9509063-09A CoUected: 09/27/95 11:03:00
TEST RESULT UNITS DETECTION ANALYZED
LIMIT
BY METHOD/CAS#
Acid Digestion
Beryllium
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Thallium
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodi chlorometheme
bromoform
bromome theme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropan
1,2-dibromoethane
dibromomethane
dichlorodifluoromethane
1,1-dichloroetheme
1,2-dichloroethane
1,1-di chloroethene
cis-1,2-dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropeme
2,2-dichloropropane
,1,1-dichloropropene
10/10/95
0.30
U
5.56
3.39
U
4.99
15.9
24
3.6
U
U
U
U
U
U
U
U
U
U
U
u 12
U
U
U
u
u u
u u u
u u u u u u
u u
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.1
0.1
0.3
0.1
1.6
0.62
0.2
1.9
2.5
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10/10/95
10/16/95
10/16/95
10/16/95
10/16/95
10/16/95
10/16/95
10/16/95
10/17/95
10/31/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
SJM
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
HMR
MMR
MMR
MMR
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7841
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
Page tt: 19 •
November 7, 1995 09:50 CERTIFICATE OF AN^U^YSIS
RESULTS BY SAMPLE
Sample ID: GD #31, 5 FT. #630, M-72 LabID: 9509063-09A CoUected: 09/27/95 11:03:00
TEST
Volatile Organics
cis-1,3 -dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
i sopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
frichloroethene
^Bl chl orof luorome theme
^^2,3 - trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentemone
2-hexemone
fluorobenzene
chlorobenzene-dS
1,4 -dichlorobenzene-d4
RESITLT
7.
U
U
. U
U
U
U
U
U
U
5BJ
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u u
u
u u u
u 1140671
597612
240347
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
1-0
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
J^NALYZED
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate »
dibromofluoromethane
1,2-• di chl oroe thaine - d4
toluene-d8
bron nofluorc )benze ine
%Recovery
90.2
86.7
112
103
METHOD/CAS#
SW-846,8260A
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Page ft: 20
November 7, 1995 09:50 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #27, 5 FT. #630, M-72 LabID: 9509063-lOA CoUected: 09/27/95
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS*
Acid Digestion
BeryllliUD
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Thallium
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodichloromethane
bromoform
bromome theme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropan
1,2-dibromoetheme
dibromome theme
dichlorodifluorometheme
1,1-dichloroetheme
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropeme
2,2-dichloropropeme
1,l-dichloropropene
10/10/95
0.84
U
14.8
9.60
U
12.7
38.7
4.0
0.2
U
U
U
U
U
U
U
U
U
U
u
u 10
u
u u
u
u
u
u
u
u
. u
u
u u u
u u
u
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.1
0.1
0.3
0.1
1.6
0.62
0.2
1.9
2.5
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10/10/95
10/16/95
10/16/95
10/16/95
10/16/95
10/16/95
10/16/95
10/16/95
10/17/95
10/31/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
SJM
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
6010
6010
7060
7841
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
#
Page tf: 21
November 7, 1995 09:50
Sample ID: GD #27, 5 FT. #630, M-72;
CERTIFICATE OF ANi^ULYSIS
RESULTS BY SAMPLE
LabID: 9509063-lOA CoUected: 09/27/95
TEST RESULT UNITS DETECTION IJTJI^YZED BY
LIMIT
METHOD/CAS#
Volatile Organics
cis-1,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
^1^ chloroethene
^B chlorof luorometheme
^^2,3 - trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentemone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
U
U
U
U
U
U
U
U
U
7.2BJ
U
U
U
O
U
U
U
U
U
U
U
U
U
U
U
U
U
u u
u 6.6BJ
U
U
909345
413545
141710
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Siirrogate
dibromofluorometheme
1, 2 -di chloroetheme-d4
toluene -d8
bromofluorobenzene
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
MMR
MMR
MMR
MMR
MMR
MMR
ISMk
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
For Volatile Organics 8260S
%Rocovery
84.8
73.5
123
108
SW-846, 8260A
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Page ft: 11
November 7, 1995 09:50 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #27, 10 FT. #630, M-72 LabID: 9509063-1 IA CoUected: 09/27/95 12:33:00
TEST
Acid Digestion
Beryllium
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Thallium
Volatile Organics
benzene
bromobenzene
bromochl orome thane
bromodi chlorometheme
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3 -chloropropan
1,2-dibromoethane
dibromometheme
dichlorodifluorometheme
1,1-dichloroetheme
1,2 -di chloroetheme
1,1-dichloroethene
cis-1,2 -dichloroethene
t rans-1,2 -di chloroethene
1,2-dichloropropeme
1,3-dichloropropane
2,2-dichloropropeme
1,1-di chloropropene
RESULT
10/10/95
0.33
0.20
7.42
7.37
U
8.58
18.3
6.3
4.7
U
U
U
U
U
U
U
U
U
U
U
U
7.1 J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.1
0.3
0.1
1.6
0.66
0.3
2.0
2.6
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/10/95
10/16/95
10/16/95
10/16/95
10/16/95
10/16/95
10/16/95
10/16/95
10/17/95
10/31/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
BY
SJM
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7841
SW-846, 8260A ^^
71-43-2 ^B
108-86-1 ^^
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
Page tt: 23
November 7, 1995 09:50
#
CERTIFICATE OF AlV^^LYSIS
RESULTS BY SAMPLE;
Sample ID: GD #27, 10 FT. #630, M-72 LabID: 9509063-llA CoUected: 09/27/95 12:33:00
TEST
Volatile Organics
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethame
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
|H:i chloroe thene
^K. chlorof luorome theme
^^2,3 - trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentemone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4 -dichlorobenzene-d4
RESITLT
6.
U
U
U
U
U
U
U
U
U
.8BJ
U
U
U
U
U
U
u
u u
u
u u
u
u
u
D
u
u
u
u
u
u
u 976225
471579
177464
ITNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
.^MfALYZED
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluoromethane
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
%Recovery
86.8
81.0
118
104
METHOD/CAS#
SW-846, 8260A
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Page tt: IA
November 7, 1995 09:50 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #3, 5 FT. #630, M-72 LabID: 9509063-12A CoUected: 09/27/95 13:35:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Beryllium
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Thallium
Volatile Organics
benzene
bromobenz ene
bromochloromethane
bromodi chlorometheme
bromoform
bromome theme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3 -chloropropan
1,2-dibromoethane
dibromometheme
di chlorodi fluoromethane
1,1-di chloroethane
1, 2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropeme
1,1-dichloropropene
10/10/95
0.57
0.19
9.24
4.97
U
7.89
22.8
5.2
0.4
U
U
U
U
U
U
U
U
U
U
U
U
10
U
U
U
U
U'
U
U
U
u
u
u
u
u
u
u
u
. u
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.1
0.1
0.3
0.1
1.5
0.62
0.2
1.8
2.5
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10/10/95
10/16/95
10/16/95
10/16/95
10/16/95
10/16/95
10/16/95
10/16/95
10/17/95
10/31/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
SJM
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7841
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
Page tt: 25
November 7, 1995 09:50
Sample ID: GD #3, 5 FT. #630, M-72
CERTIFICATE OF ANALYSIS
'-' RESULTS BY SAMPiJi
Lab ID: 9509063-12A CoUected: 09fllf95 13:35:00
TEST
Volatile Organic^
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
^^i chl oroe thene
^^Ml chlorof luorome theme
^^^2,3 - trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentemone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
9.
3.
U
U
U
U
U
U
u
u
u .4BJ
U
U
U
U
U
u
D
U
U
U
u
u
u
u
u u D
U
U
4BJ
U
U
D
1093823
583504
241018
Surrogat
Surrogate
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
e/Recovery Data For Volatile Organics 8260S
dibromofluorometheme
1,2-di chloroetheme-d4
toluene-d8
bromofluorobenzene
%Recovery
91.2
89.4
110
101
HETHOD/CAS#
SW-846,8260A
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Page tf: 26
November 7, 1995 09:50 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #3, 5 FT. #630,M-72 DUP LabID: 9509063-13A CoUected: 09/27/95 13:35:00
TEST
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chloromethane
bromoform
bromome theme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3 -chloropropan
1,2-dibromoetheme
dibromometheme
dichlorodifluoromethane
1,1-dichloroethane
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2- dichloropropeme
1,3-dichloropropeme
2,2-dichloropropane
1,l-dichloropropene
ci s-1,3 -dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
RESULT
U
u u u u
u u u
u u u u 9.3J
U
U
U
U
U
U
u u u
u u
u u
u
u u u u u u u u u u u u 9. IB J
u u u
u u u u u u
u
u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3 ^1^
107-06-2 flB
75-35-4 ^^
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
Page tt: 11
November 7, 1995 09:50
•
CERTIFICATE OF AN^yLYSIS
* RESULTS BY SAMPLE
Sample ID: GD #3, 5 FT. #630,M-72 DUP LabID: 9509063-13A CoUected: 09/27/95 13:35:00
TEST
Volatile Organics
trichlorofluorometheme
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentemone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
U
U
u
u
u
u
u
u
u
u
u
929150
475341
192603
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
JIO^ALYZED
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
10/09/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluoromethane
1 ,,2 -dichloroethane-d4
^^ toluene-d8
^B bromofluorobenzene
%Recovery
84.7
79.5
114
101
METHOD/CAS#
SW-846,8260A
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Racovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Sample ID: GD #3, 10 FT. #630, M-72 Lab ID: 95()9063-14A CoUected: 09/27/95 14:08:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Beryllium
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
10/10/95
0.54
U
30.0
6.80
3.80
16.4
29.2
13.6
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
0.1
0.1
0.3
0.1
1.6
0.64
0.3
1.9
10/10/95
10/16/95
10/16/95
10/16/95
10/16/95
10/16/95
10/16/95
10/16/95
10/17/95
SJM
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
6010
6010
7060
Page ft: 28
November 7, 1995 09:50 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #3, 10 FT. #630, M-72 LabID: 9509063-14A CoUected: 09/27/95 14:08:00
TEST
Thallium
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodichlorometheme
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropan
1,2-dibromoetheme
dibromomethane
di chlorodi fluorometheme
1,1-dichloroetheme
1,2-dichloroethane
1,1-dichloroethene
cis-1,2 -dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropeme
1,3 -dichloropropeme
2,2-dichloropropane
1,1-dichloropropene
cis-1,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
RESULT
3.8
U
U
U
U
U
U
U
U
U
U
U
U
IIB
U
U
U
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u u
u
u u u u
u u
u
u
u
UNITS
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
2.5
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/31/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 7841
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3 ^^.
75-71-8 WM]
75-34-3 ^^
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
Page ff: 29
November 7, 1995 09:50
#
CERTIFICATE OF AlV^U^YSIS
RESULTS BY SAMPID
Sample ID: GD #3, 10 FT. #630, M-72 ff Lab ID: 9509063-14A CoUected: 09/27/95 14:08:00
TEST
Volatile Organics
1,1,2-trichloroetheme
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
u u u u
u u u u u 15B
3.4 J
U
U
632514
390792
194782
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
ro 10
10
10
10
10
J\NALYZED
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
^^ dibromofluoromethane 1^ .,2 -di chloroetheme-d4
^^ toluene-d8 ,
bromofluorobenzene
%Recovery
101
90.3
100
92.6
METHOD/CAS#
SW-846,8260A
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Sample ID: GD #5, 5 FT. #630, M-72 Lab ID: 9509063-15A CoUected: 09/27/95 14:27:00
TEST RESULT UNITS DETECTION ANJILYZED BY
LIMIT
METHOD/CAS*
Acid Digestion
Beryllium
Cadmium
Chromium
Copper
Lead
Nickel
Zinc
10/17/95
0.82
U-
15.4
12.0
U
11.3
55.3
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
0.1
0.1
0.3
0.1
1.6
0.64
0.3
10/17/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
KWB
LVD
LVD
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
6010
6010
Page tt: 30
November 7, 1995 09:50
Sample ID: GD #5, 5 FT. #630, M-72
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9509063-15A CoUected: 09/27/95 14:27:00
•
TEST
Arsenic
Thallium
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chlorome theme
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropem
1,2-dibromoetheme
dibromometheme
di chlorodi fluoromethane
1,1-dichloroethane
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2-dichloroe thene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropeme
1,l-dichloropropene
ci s-1,3 -dichloropropene
trans-1,3 -di chloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
RESULT
5.5
0.3
U
U
U
. U
U
U
U
U
u u u
u 5.3BJ
u u U
U
U
U
U
U
u u u
u u u
u u u u u u u u
u u u u u u u u
u u
u
u u
UNITS
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
1.9
2.6
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
11/02/95
10/31/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
CRS
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
HMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 7060
SW-846, 7841
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8 ^^,
106-93-4 ^B
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6 ^^^
Page tt: 31
November 7, 1995 09:50
Sample ID: GD #5, 5 FT. #630, M-72
CERTIFICATE OF AN^O^YSIS
RESULTS BY SAMPLE
Lab ID: 9509063-15A CoUected: 09/27/95 14:27:00
TEST RESULT ITNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
ft
U
U
U
U
u
u u u u u u u u u
u 1373475
712396
268222
Surrogate
Stirrogate
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
i/Recovery Data
^^ dibromofluorometheme
1 ,2 -dichloroetheme-d4
toluene-d8
bromofluorobenzene
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
For Volatile Organics 8260S
%Rocovery
97.0
92.1
116
106
SW-846,8260A
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Sample ID: GD #5, 5 FT. #630,M-72 DUP LabID: 9509063-16A CoUected: 09/27/95 14:27:00
TEST RESULT UNITS DETECTION ANJU.YZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Beryllium
Cadmium
Chromium
Copper
Lead
Nickel
10/17/95
0.84
U
15.4
12.8
U
10.7
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
0.1
0.1
0.3
0.1
1.6
0.65
10/17/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
KWB
LVD
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
6010
Page tf: 32
November 7, 1995 09:50 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #5, 5 FT. #630,M-72 DUP LabID: 9509063-16A CoUected: 09/27/95 14:27:00
TEST RESITLT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Zinc
Arsenic
Thallium
61.6 ug/g
4.3 ug/g
0.3 ug/g
0.3 10/19/95 LVD
2.0 11/01/95 CRS
2.6 10/31/95 CRS
SW-846, 6010
SW-846, 7060
SW-846, 7841
Sample ED: GD #5, 10 FT. #630, M-72 LabID: 9509063-I7A CoUected: 09/27/95 14:40:00
TEST
Acid Digestion
Beryllium
Cadmiiun
Chromium
Copper
Lead
Nickel
Zinc
Arsenic
Thallium
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodichloromethane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chlorometheme
2-chlorotoluene
RESULT
10/17/95
0.62
0.43
13.7
8.71
6.05
12.3
28.3
8.0
3.2
U
U
U
U
U
U
U
U
U
U
u
u IOB
U
U
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.1
0.3
0.1
1.5
0.60
0.2
1.8
2.4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/17/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
10/19/95
11/02/95
10/31/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
KWB
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010^^
6010^^
6010
6010
6010
7060
7841
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
Page tt: 33
November 7, 1995 09:50 CERTIFICATE OF AlV^^YSIS
RESULTS BY SAMPLE,
Sample ID: GD #5, 10 FT. #630, M-72 i Lab ID: 9509063-17A CoUected: 09/27/95 14:40:00
TEST
Volatile Organics
4 -chlorotoluene
dibromochlorome theme
1,2-dibromo-3 -chloropropan
1,2 -dibromoetheme
dibromometheme
dichlorodifluorometheme
1,1-dichloroethane
1,2-dichloroetheme
1,1-dichloroethene
cis-1, 2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropeme
2,2-dichloropropeme
1,l-dichloropropene
cis-1,3 -dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
^^cachlorobutadiene
^^^propylbenzene
^^isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroetheme
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m, p-xylene
acetone
2-butanone
4 -methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4 -dichlorobenzene-d4
RESITLT
U
u u
u
u u
u
u
u
u
u
u
u
u
u D
u
u u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u u
u
u
u
u
u u
u u
u
4.8BJ
u
u
u 1029784
457069
155419
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/:L0/95
IO/:LO/95
lO/JLO/95
lO/J.0/95
10/10/95
10/1.0/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Page tt: 34
November 7, 1995 09:50 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #5, 10 FT. #630, M-72 Lab ID: 9509063-17A CoUected: 09/27/95 14:40:00
TEST RESULT ITNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Volatile Organics SW-846,826OA
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorometheme
1,2-dichloroetheme-d4
toluene-d8
bromofluorobenzene
%Recovery
82.0
70.7
131
108
Recovery
58.4 TO
53.3 TO
85.6 TO
80.6 TO
Limits
112
121
143
130
Page tt: 35 ^
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identifled compounds or when the mass sf>ectral data indicated the presence of a
compound that meets the identiflcation criteria but the result is less than the specifled
detection limit but greater than zero. (e.g. 1.1J with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank ais weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specifled limits. If surrogate recoveries are out
of limits, any values reported are for indication only.
ENVIRONMENTAL LAB WORK REC>UEST /^yTi ^AZ y
Ik
^°- THIOKOL ENVIRONMENTAL LABORATORY LWR No. El 1063
~ A F Uhii^
ORGANIZATION /,
Fyiy/roAmt/fl^
EXTENSION
£^?o
MAIL STOP
SOI e
COST CENTER uzzd-o WORK ORDER
l'i^940
DATE
REPORT RESULTS TO:
HELEN WARD, MS 301
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SAMPLE
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TYPE
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SAMPLE INFORMATION
LOCATION
//.J/ Su>l^*f-^
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TIME
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^^ i/l
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-^^^1
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REMARKS
CHAIN OF CUSTODY
RELINQUISHED BY DATE TIME RECEIVED BY DATE TIME
dM/m/^ ^--zS'^^c ms^ U/CZlZC/jZauL W f-?^'9^ Z^'HT
FOR LABORATORY USE ONLY
*•
DATE COMPLETED DATE REPORTED SIGNATURE
November 9, 1995 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmetual Monitoring
TO: Helen Ward MIS 301
Thiokol Corp, Ut 84322
A.F. WALKER
EXT 5390
Work Orderly 9509067
LabID: Sample ID:
OIA GD 1)131,5 FT. #646, M-71
LabID: Sample ID:
02A GD«1, IOFT. #646, M-71
LabID: Sample ID:
03A OD #39^ 5 FT. #646, M-71
LabID: Sample ID:
04A GD #39, 10 FT. #646, M-71
ng ANALYZED
' BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Oty, Ut 84302-0707
Analytical Labs MIS 245
Atm: Dr. John Terry
Tele: 801-863-2384
Sample and Test Code Identiflcation
Test Codes and Names
PH pH
3050 Acid Digestion
BE AE2 Betyllium
HG CV2 Mercuiy
8260s Volatile Organics
Test Codes and Names
PH pH
3050 Acid Digestion
BE AE2 Betyllium
HO CV2 Metcuty
8260s Volatile Oiganics
Test Codes and Names
PH pH
3050 Acid Digestion
BE AE2 Betyllium
HG CV2 Mercuiy
8260S Volatile Organics
Test Codes and Names
PH pH
3050 Acid Digestion
BE AE2 Betyllium
HG CV2 Mereuty
8260s Volatile Otganics
Comments
Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 7471
SW-846,8260A Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 7471
SW-846,8260A
Certried By
Page#:lof ^
•
This is to certify tfiat tfie following samples were analyzed using good laboratory practices
to sfiow the following results.
Sample ID: GD #31, 5 FT. #646, M-71 LabID: 9509067-01A CoUected: 09/28/95 11:25:00
TEST
pH
Acid Digestion
Beryllium
Mercury
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodi chl orome thauie
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
^^^roform
^Hbr ome thane
z'chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropem
1,2-dibromoethane
dibromomethane
dichlorodifluoromethane
1,1-dichloroethane
1,2-dichloroethane
1,1 - di chloroet:hene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis-1,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4-isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
RESULT
7.92
10/17/95
0.78
U
U
U
U
U
U
u u
u
u u u u 9. IB J
U
U
U
u
u
u u u u u u
u
u
u
u u y
u u u u u
u u u u u u
u
TJNITS
pH Unit
DATE
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.013
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANiLLYZED
10/03/95
10/17/95
10/19/95
10/25/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
IO/:LO/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
MTB
KWB
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
Page tt: 2
November 9, 1995 13:42 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #31, 5 FT. #646, M-71 LabID: 9509067-OlA CoUected: 09/28/95 11:25:00
TEST
Volatile Organics
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentemone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESXTLT
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u u
u 1003791
466846
169307
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluoromethane
1,2-di chloroetheme-d4
toluene-d8
bromofluorobenzene
%Racovery
88.4
75.1
126
105
METHOD/CAS#
SW-846,8260A
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl ^^
INTSTD2 ^B
INTSTD3 ^^
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Sample ID: GD #31, 10 FT. #646, M-71 LabID: 9509067-02A CoUected: 09/28/95 11:35:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
PH
Acid Digestion
Beryllium
Marcury
7.69
10/17/95
0.56
U
pH Unit
DATE
ug/g
ug/g
0.1
0.010
10/03/95
10/17/95
10/19/95
10/25/95
MTB
KWB
LVD
CRS
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 7471
Page tt: 3
November 9, 1995 13:42
Sample ID: GD #31, 10 FT. #646, M-71
CERTIFICATE OF ANif^YSIS
, RESULTS BY SAMPLE
LabID: 95()9067-02A CoUected: 09/28/95 11:35:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chloromethane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chlorometheme
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3-chloropropem
1,2-dibromoethane
dibromometheme
dichlorodifluoromethane
^^^ - dichloroe theme
j^H -dichloroethane
^^^H- - dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropame
2,2-dichloropropame
1,l-dichloropropene
cis-1,3-dichloropropene
trams-1,3-dichloropropene
1,2-dichlorobenzene
1,3 -di chlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4-isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3 -trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
U
U
U
U
U
U
U
U
u u u u 9. OB J
u
u u u u
u u u u u u u u u u u u u
u
u u u u u u u
u u
u u u u u u u u u u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6 tri(
Page tt: A
November 9, 1995 13:42 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #31, 10 FT. #646, M-71 LabID: 9509067-02A CoUected: 09/28/95 11:35:00
TEST
Volatile Organics
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m, p-xylene
acetone
2-butamone
4-methyl-2-pentemone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
U
u
u u u u u u u . u
u 939984
501202
211524
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
Surrogate/Recovery Data For Volatile Organic
Surrogate
dibromofluorometheme
1 ,2 -dichloroetheme-d4
toluene-d8
bromofluorobenzene
%Racovery
93.7
82.2
112
99.7
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
s 8260S
METHOD/CAS#
SW-846,8260A
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130 i^
Sample ID: GD #39, 5 FT. #646, M-71 LabID: 9509067-03A CoUected: 09/28/95 11:55:00
TEST
pH
Acid Digestion
Beryllium
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chloromethane
bromoform
bromometheme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
RESULT
7 83
10/17/95
0 71
U
U
U
U
U
U
U
U
U
U
u
UNITS
pH Unit
DATE
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.011
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/03/95
10/17/95
10/19/95
10/25/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
MTB
KWB
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 7471
SW-846, 8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
Page tt: 5
November 9, 1995 13:42
m
CERTIFICATE OF AN^lLYSIS
RESULTS BY SAMPLE
Sample ID: GD #39, 5 FT. #646, M-71 „ LabID: 9509067-03A CoUected: 09/28/95 11:55:00
TEST
Volatile Organics
chlorobenzene
chloroethane
chloroform
chloromethane
2-chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropem
1,2-dibromoetheme
dibromomethane
dichlorodifluoromethane
1,1-dichloroetheme
1,2-dichloroethame
1,1-dichloroethene
cis-1,2 -dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropane
2,2-dichloropropeme
1,l-dichloropropene
cis-1,3 -dichloropropene
^|ans-1,3 -di chloropropene
^^K-dichlorobenzene
^^-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2- tet:rachloroe thane
1,1,2,2-tetrachloroetheme
tet rachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m, p-xylene
acetone
2-butanone
4 -methyl - 2 -pentemone
RESULT
U
u 18B
U
U
U
U
U
u u
u
u u
u
u u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u u u
u
u
u
u
u
u
u
u
u
u
u
u
u u
3.0 J
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANJU.YZED
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
IO/:LO/95
10/10/95
10/10/95
lO/J.0/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
Page tf: 6
November 9, 1995 13:42 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #39, 5 FT. #646, M-71 LabID: 9509067-03A CoUected: 09/28/95 11:55:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene
U
399801
173714
-d4 57782
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
dibromof1uoromethane
1,2-dichloroe thane-d4
toluene-d8
bromofluorobenzene
SW-846,8260A
10 10/10/95 MMR 591-78-6
10/10/95 MMR INTSTDl
10/10/95 MMR INTSTD2
10/10/95 MMR XNTSTD3
For Volatila Organics 8260S
%Racovary Recovery Limits
81.2 58.4 TO 112
62.9 53.3 TO 121
130 85.6 TO 143
108 80.6 TO 130
Sample ID: GD #39, 10 FT. #646. M-71 LabID: 9509067-04A CoUected: 09/28/95 12:05:00
TEST
pH
Acid Digestion
Beryllium
Mercury
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodi chloromethane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethame
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropem
1,2-dibromoetheme
dibromometheme
RESULT
7.90
10/17/95
0.72
U
U
U
U
U
U
U
U
U
U
U
U
U
IIB
U
U
U
U
U
U
U
UNITS
pH Unit
DATE
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.012
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/03/95
10/17/95
10/19/95
10/25/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
MTB
KWB
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
EPA 150.1 ••
SW-846, 3050
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
Page tt: 1 •
November 9, 1995 13:42 CERTIFICATE OF AN^^XYSIS
RESULTS BY SAMPLE
Sample ID: GD #39, 10 FT. #646, M-71 Lab ID: 9509067-04A CoUected: 09/28/95 12:05:00
TEST
Volatile Organics
dichlorodifluorometheme
1,1-dichloroetheme
1,2-dichloroethame
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropeme
2,2-dichloropropane
1,l-dichloropropene
cis-1,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
I-propylbenzene
^^nrene
^Bf, 1,2- tetrachloroethane
1,i,2,2 -tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3- trichloropropauie
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentamone
2-hexamone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
U
u u u
u u u
u u u u u u u u
u
u u
u u u u u u u
u
u u
u u
u
u u u u
u
u u u u u u u 145359
84540
35416
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANJkLYZED
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/-L0/95
10/10/95
10/10/95
lO/J.0/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorome thame
%Recovery
97.0
METHOD/CAS#
SW-846,8260A
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4 TO 112
Page tt: 8
November 9, 1995 13:42 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #39, 10 FT. #646, M-71 LabID: 9509067-04A CoUected: 09/28/95 12:05:00
TEST RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Volatile Organics
1,2-dichloroetheme-d4
toluene-d8
bromofluorobenzene
98.5
102
101
53.3 TO
85.6 TO
80.6 TO
121
143
130
SW-846,8260A
Page tt: 9
m
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. l.U with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration irange but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection Umits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spUce recovery was outside of the specified limits. If surrogate recoveries are out
of limits, any values reported are for indication only.
ENVIRONMENTAL LAB WORK REQUEST
#
7^//^^^ /
THIOKOL ENVIRONMENTAL LABORATORY LWR No. E11066
/) f l^y/i/^ 6-^^<r^
COST CENTER
uj^4C'
WORKORDER
//"2-y^'
ORGANIZATION
t::/iyirc^1/l-v,j/^d^
MAIL STOP REPORT RESULTS TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
V'
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1/
SAMPLE
1 t::uJ-iii'' ^L/.ir
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DATE
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ll
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LOCATION
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l^\'
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I'M -fZC-O
Bcz. hlc^ . I^H
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REMARKS
/jcT//y<i )
l./^l.
13, Su>/u\^ ^/i>4i^
£dil/vy '/Oft ff y 1^ f46^ /B., 4, />^
CHAIN OF CUSTODY
RELINQUISHED BY
'/J4.yfp//.
DATE
/ii-z-f'C-lUf',
TIME RECEIVED B^-DATE
J"//?';^-9r zy^z^
TIME
FOR LABORATORY USE ONLY
DATE COMPLETED
L
DATE REPORTED SIGNATURE
ENVIRONMENTAL LAB WORK REQUEST ^</0f^ I
"" TinOKOL ENVIRONMENTAL LABORATORY
ORCAM ZATION
COSTCSnTR
LWRNo. £//i^G
I I/DATE WORK ORDER 3
REPORT RESULTS TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
L/^
\y
y^
yz.
ly^:.
SAMPIX
\.^iU/H0il-6^t
^^f /ofr
'':Sumoif-UZ2'
> GA^'1 /nir
Cdd^,7-..^^
Cdi^ 2(^-5 ft-
GA-i^ZJ^-lof
8.
9.
10.
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11
DATE
/0-J-^
/I
If
II
'jJ ll
• i<
it
TVPE
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t^
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ll
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CJ.Cr,Ay,Pl>, pd
n
II
ll
ll
ll
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REMARKS
1
\
CHAIN OF CUSTODY
Rn.INQUISIIEDBV DATE TIME RFrEIVED BY DATE TIME
DATE COMPUTED
FOR LABORATORY USE ONLY
DATE REPORTED
o
November 10, 1995 CERTIFICATE OF ANA]:.YSIS
RESULTS BY SAMPLE
•
SENT Environmental Monitoring
TO: Helen Ward M/S 301
Thiokol Corp. Ut 84322
A.F. WALKER
EXT 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Oty, Ut 84302-0707
Analytical Labs M/S 245
Atm: Dr. John Terry
Tde: 801-863-2384
Work Orderly 9510001 Sample and Test Code Identification
LabID: Sample ID:
OIA GD #12, 5 FT. #628, M-19A
LabID: Sample ID:
02A GD #12, 10 FT. #628, M-19A
LabID: Sample ID:
03A RINSE BLANK, M-71
Test Codes and Names
LabID: Sample ID:
04A GD#'l01,5 FT. #646, M-71
LabID: Sample ID:
05A GD#101, IOFT. #646, M-71
LabID: Sample ID:
06A GD #106, 5 FT. #646, M-71
LabID: Sample ID:
07A GD #106, 10 FT. #646, M-71
LabID: Sample ID:
08A GD #106, 10 FT. #646 DUP.
PH
3050
CD AE2 CR AE2
PB AE2
AG AE2
pH
Acid Digestion
Cadmium Chromium
Lead
Silver
Test Codes and Names
PH
3050
CD AE2
CR AE2
PB AE2
AG AE2
pH
Acid Digestion
Cadmium
Chromium
Lead
Silver
Test Codes and Names
3010
BE AE2
CD AE2
CR AE2
PB AE2
AG AE2
HG CV3
826Q
Acid Digestion
Beryllium
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
PH
3050
BE AE2
HG CV2
8260s
pH
Acid Digestion
Beryllium
Mercury
Volatile Organics
Test Codes and Names
PH
3050
BE AE2
HG CV2
8260S
pH
Acid Digestion
Beryllium
Mercury
Volatile Organics
Test Codes and Names
PH
3050
BE AE2
HG CV2
8260s
pH
Acid Digestion
Betyllium
Mercury
Volatile Orgaiucs
Test Codes and Names
PH
3050
BE AE2
HG CV2
8260s
pH
Acid Digestion
Beryllium
Mercury
Volatile Orgaiucs
Test Codes and Names
8260S Volatile Organics
Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010 Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010 Method
SW-846, 3010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 7470
SW-846,8260A Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 7471
SW-846,8260A Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 7471
SW-846,8260A Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 7471
SW-846,8260A
Method
SW-846,8260A
Page #: lof 11
Work Order i» 9510001 Sample and Test Code Identification
LabID: Sample ID:
09A GD th, 5 FT. #628, M-19A
LabID: Sample ID:
lOA GD #9, 10 FT. #628, M-19A
Test Codes and Names
LabID: Sample ID:
11A GD #9, 10 FT. #628 DUP.
LabID: Sample ID:
I2A GD #17. 5 FT. #628, M-19A
LabID: Sample ID:
13A GD #17, 8.5 FT.,#628, M19A
LabID: Sample ID:
14A GD #26, 5 ft. #628, M-19A
LabID: Sample ID:
~i3A GD #26. 10 FT #628, M-19A
PH
3050
CD AE2
CR AE2
PB AE2
AG AE2
pH
Acid Digestion
Cadmium
Chromium
Lead
Silver
Test Codes and Names
PH
3050
CD AE2
CR AE2
PB AE2
AG AE2
pH
Acid Digestion
Cadmium
Chromium
Lead
Silver
Test Codes and Names
PH
3050
CD AE2
CR AE2
PB AE2
AG AE2
pH
Acid Digestion
Cadmium
Chromium
Lead
Silver
Test Codes and Names
PH
3050
CD AE2
CR AE2
PB AE2
AG AE2
pH
Acid Digestion
Cadmium
Chromium
Lead
Silver
Test Codes and Names
PH
3050 CD AE2
CR AE2
PB AE2
AG AE2
pH
Acid Digestion Cadmium
Chroinium
Lead
Silver
Test Codes and Names
PH
3050
CD AE2 CR AE2
PB AE2
AG AE2
pH
Acid Digestion
Cadmium Chromium
Lead
Silver
Test Codes and Names
PH
3050
CD AE2
CR AE2
PB AE2
AO AE2
pH
Acid Digestion
Cadinium
Chromium
Lead
Silver
Comments
Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010 Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010 Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
•
^/CfiyH^f-tyi^^
Certmed By
Page #:2 o
This is to certify tliat the folio-wing samples were analyzed using good laboratory practices
to sfiow the following results.
Sami pie ID: GD #12, 5 FT. #628, M-19A Lab ID: 9510001-OlA CoUected: 09/28/95 14:55:00
TEST RESULT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
pH
Acid Digestion
Cadmium
Chromium
Lead
Sliver
7.92
10/17/95
0.38
13.2
U
U
pH Dnit
DATE
ug/g
ug/g
ug/g
ug/g
0,
0.
1.
0.
.1
.3
. S'
.2
10/03/95
10/17/95
10/19/95
10/19/95
10/19/95
10/19/95
MTB
KWB
LVD
LVD
LVD
LVD
EPA 150.1
SW-846, 3050
SW-84G, 6010
SW-84G, 6010
SW-846, 6010
SW-846, 6010
Sample ID: GD #12, 10 FT. #628, M-19A LabID: 9510001-02A CoUected: 09/28/95 15:10:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
pH
Digestion
Cadmium
Chromium
Lead
Silver
8.03
10/17/95
D
10.3
D
U
pH Unit
DATE
ug/g
ug/g
ug/g
ug/g
0
0
1,
0,
.1
.3
.5
.2
10/03/95
10/17/95
10/19/95
10/19/95
10/19/95
10/19/95
MTB
KWB
LVD
LVD
LVD
LVD
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Sample ID: RINSE BLANK, M-71 LabID: 9510001-03A CoUected: 10/02/95 08:30:00
TEST RESULT UNITS DETECTION ANAiCiYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Beryllium
Cadmium
Chromium
10/10/95
U
U
U
DATE
ug/L
ug/L
ug/L
2
2
5
10/10/95
10/12/95
10/12/95
10/12/95
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
3010
6010
6010
6010
Page tt: 3
November 10, 1995 13:57
Sample ID: RINSE BLANK, M-71
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9510001-03A CoUected: 10/02/95 08:30:00 •
TEST
Lead
Silver
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chloromethane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2- dibromo - 3 - chloropropeui
1,2-dibromoethane
dibromomethane
di chlorodifluoromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2 -dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropame
2,2-dichloropropane
1,l-dichloropropene
cis-1,3-dichloropropene
trams-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
RESULT
U
U
u
u u
u u u
u u
u u D
u u u u u u u D
u u u u u u
u o
u D
u u o u u u u
u
u u u u u
u u D
D
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
25
3
0.15
0.20
0.20
0.20
0.30
0.10
0.40
0.20
0.20
0.20
0.30
0.20
0.40
0.40
0.60
0.20
0.20
0.30
0.20
0.20
0.20
0.20
0.10
0.20
0.60
0.20
0.20
0.20
0.20
0.20
0.20
0.20
0.20
0.10
0.20
0.20
0.30
0.20
0.20
0.20
0.30
0.20
0.20
0.20
0.20
0.30
ANALYZED
10/12/95
10/12/95
10/06/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 7470
SW-846,82G0A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1 M^
96-12-8 flV
106-93-4 ^^
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
Page tt: A
November 10, 1995 13:57 CERTIFICATE OF ANAJLYSIS
RESULTS BY SAMPLE
«> Ie ID: RINSE BLANK, M-71 Lab ID: 9510001-03A CoUected: 10/02/95 08:30:00
TEST
Volatile Organics
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroetheme
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m, p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4 -di chlorobenz ene-d4
^ w
RESITLT
U
u ' u
u u u u u u
u u u u u 20
u u u 925543
652306
289127
TJNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
0.90
0.30
0.20
0.20
0.20
0.20
0.30
0.30
0.20
0.20
0.20
0.40
0.20
0.20
10
10
10
10
A]!TALYZED
10/3.0/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260
Surrogate
dibromofluorometheme
1 ,2-dichloroe thane-d4
toluene-d8
bromofluorobenz ene
%Recovery
99.5
94.8
99.4
102
METHOD/CAS#
SW-846,8260A
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
80.0
80.0
80.0
80.0
TO 120
TO 120
TO 120
TO 120
Sample ID: GD #101, 5 FT. #646, M-71 Lab ID: 9510001-04A CoUected: 10/02/95 08:35:00
TEST
pH
Acid Digestion
Beryllium
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
RESULT
7.71
10/17/95
0.72
0.02
U
U
U
UNITS
pH Unit
DATE
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.014
10
10
10
ANAIiYZED
10/03/95
10/17/95
10/19/95
10/25/95
10/10/95
10/10/95
10/10/95
BY
MTB
KWB
LVD
CRS
MMR
MMR
MMR
METHOD/CAS#
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
Page tf: 5
November 10, 1995 13:57 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #101, 5 FT. #646, M-71 Lab ED: 9510001-04A CoUected: 10/02/95 08:35:00
TEST
volatile Organics
bromodi chlorometheme
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butyIbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropem
1,2-dibromoethane
dibromome theme
dichlorodifluoromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-di chloroethene
cis-l,2-di chloroethene
trans-1,2-dichloroethene
1,2-dichloropropame
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis-1,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroetheme
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropane
1,2,4-trimethylbenzene
RESULT
U
U
U
u
u U
U
u u 78B
U
D
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
U
U
O
u u u u
u
u u
u u u u u D
n u 3.3J
u u u
u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
r ANALYZED
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5 ^1^
142-28-9 ^V
590-20-7 ^^
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
Page tf: 6
November 10, 1995 13:57 CERTIFICATE OF ANAJLYSIS
RESULTS BY SAMPLE
#>: le ID: GD #101, 5 FT. #646, M-71 LabID: 9510001-04A CoUected: 10/02/95 08:35:00
TEST
Volatile Organics
RESULT
1,3,5-trimethylbenzene U
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4 -di chlorobenzene-<
U
U
u
5.3BJ
5.1J
U
U
558299
275408
14 104766
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
Surrogate/Recovery Data For Volat:
Surrogate
dibromofluoromethane
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
%Recovery
87.7
85.8
115
105
AN^LLYZED
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Lie Organics 8260S
METHOD/CAStt
SW-846,82eOA
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 13 0
pie ID: GD #101, 10 FT. #646, M-71 Lab ID: 9510001-05A CoUected: 10/02/95 08:55:00
TEST
pH
Acid Digestion
Beryllium
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodichloromethane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
RESULT
7.83
10/17/95
0.40
0.03
U
U
U
U
U
U
U
U
U
U
U
U
34B
UNITS
pH Unit
DATE
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.011
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/03/95
10/17/95
10/23/95
10/25/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
MTB
KWB
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAStt
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
Page ft: 7
November 10, 1995 13:57 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #101, 10 FT. #646, M-71 LabID: 9510001-05A CoUected: 10/02/95 08:55:00
TEST
Volatile Organics
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropan
1,2-dibromoethane
dibromometheme
di chlorodifluoromethame
1,1-dichloroethane
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2-dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropeme
1,3-dichloropropame
2,2 -di chloropropeme
1,l-dichloropropene
c i s-1,3 -di chloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3 -di chlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethame
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethame
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4 -methyl - 2 -pentemone
2-hexanone
fluorobenzene
chlorobenzene-d5
RESULT
U
U
u u u
u a o
n U
U
u u
u u u u
u u V
u D
u
u u
u u u u
u u u
u u u
u u D
u u
u
u u D
u
u
u 4.9J
u u 971938
511500
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
, 10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAStt
SW-846,8260A
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3 J^
98-82-8 ••
99-87-6 ^^
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
Page #: 8
CERTIFICATE OF ANAJLYSIS
RESULTS BY SAMPLE
November 10, 1995 13:57
^J|jle ID: GD #101, IOFT. #646, M-71 '-' LabID: 9510001-05A CoUected: 10/02/95 08:55:00
TEST RESULT UNITS DETECTION AN/LLYZED BY
LIMIT
METHOD/CAStt
Volatile Organics
1,4-dichlorobenzene-d4 204544 ug/Kg
Surrogate/Recovery Data
Surrogate
dibromofluoromethane
1,2 -di chloroethane-d4
toluene-d8
bromofluorobenzene
SW-846,8260A
10/10/95 MMR INTSTD3
For Volatile
%Recovery
93.6
85.0
113
101
Organics 826OS
Recovery Limits
58.4 TO 112
53.3 TO 121
85.6 TO 143
80.6 TO 130
Sample ID: GD #106, 5 FT. #646, M-71 Lab ID: 9510001-06A CoUected: 10/02/95 09:20:00
TEST
pH
Acid Digestion
^^^llium
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chlorome thane
bromoform
bromome t:hcuie
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroetheme
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropan
1,2-dibromoethane
dibromome theme
di chlorodifluorome theme
1,1-dichloroethame
1,2-dichloroethane
RESULT
7.79
10/17/95
0.45
0.06
u U
U
U
U
U
U
U
U
U
U
U
38B
U
U
U
U
U
U
U
U
U
U
UNITS
pH Unit
DATE
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.010
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
AliTALYZED
10/03/95
10/17/95
10/23/95
10/25/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
MTB
KWB
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAStt
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
Page it: 9
November 10, 1995 13:57 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #106, 5 FT. #646, M-71 LabID: 9510001-06A CoUected: 10/02/95 09:20:00
TEST
Volatile Organics
1,1-dichloroethene
ci s-1,2 -di chloroethene
trans -1,2-dichloroethene
1,2- dichloropropame
1,3-dichloropropane
2,2-dichloropropeme
1,1-dichloropropene
cie-1,3-dichloropropene
trems-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
Ta,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-ds
1,4- dichlorobenzene-d4
RESULT
U
U
u
u
D
D
u
U
u U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
u
u
u
u u D
u U
u
u
u
u
u
n
D
u 1324735
588162
167794
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAStt
SW-846,8260A
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3 ^^
87-61-6 ^m
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorometheme
1,2-dichloroetheme-d4
toluene-d8
bromofluorobenzene
%Recovery
88.1
73.4
129
119
Recovery
58.4 TO
53.3 TO
85.6 TO
80.6 TO
Limits
112
121
143
130
Page tt: 10
November 10, 1995 13:57 CERTIFICATE OF ANi^iLYSIS
RESULTS BY SAMPLE
•P Ie ID: GD #106, 10 FT. #646, M-71 LabID: 9510001-07A CoUected: 10/02/95 09:40:00
TEST
pH
Acid Digestion
Beryllium
Mercury
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chloromethane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chlorofonn
chloromethane
Ja^lorotoluene
l^^nl orotoluene
clKromochlorome theme
1,2-dibromo-3 -chloropropem
1,2-dibromoetheme
dibromometheme
dichlorodifluoromethane
1,1-dichloroethane
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2 -dichloropropane
1,3-dichloropropeme
2,2-dichloropropane
1,1-dichloropropene
cis-1,3 -dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 - isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
RESULT
8.00
10/17/95
0.79
U
U
U
U
U
U
U
U
u
u
u u
u 42B
U
u
u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u D
u
u
u
u
u
u
u
vUNITS
pH Unit
DATE
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
•ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.011
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
f i^NiLLYZED
10/03/95
10/17/95
10/23/95
10/25/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
IO/:LO/95
10/10/95
10/:L0/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
Mi'B
KWB
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAStt
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 7471
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
Page#: 11
November 10, 1995 13:57 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #106, 10 FT. #646, M-71 Lab ID: 9510001-07A CoUected: 10/02/95 09:40:00
TEST
Volatile Organics
RESULT
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroetheme
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroethane
trichloroethene
tri chlorofluorome theme
1,2,3-trichloropropeme
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butemone
4-methyl-2-pentanone
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
6BJ
U
U
U
1051627
557279
223007
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
id 10
10
10
10
10
10
10
10
10
10
ANALYZED
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluoromethane
1 ,2 - dichloroethane-d4
toluene-d8
bromofluorobenzene
%Recovery
92.1
86.8
112
103
METHOD/CAStt
SW-846,8260A
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
•
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Sample ID: GD #106, 10 FT. #646 DUP. LabID: 9510001-08A CoUected: 10/02/95 09:40:00
TEST RESITLT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAStt
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chloromethane
bromoform
bromometheme
n-butyIbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
u
u
u
u u
u
u
u
u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
Page tt: 12
November 10, 1995 13:57 CERTIFICATE OF ANAJLYSIS
RESULTS BY SAMPLE
m |;;.H
le ID: GD #106, 10 FT. #646 DUP. Lab ID: 9510001-08A CoUected: 10/02/95 09:40:00
TEST
Volatile Organics
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochlorometheme
1,2-dibromo-3-chloropropan
1,2-dibromoethane
dibromomethane
di chlorodif1uorometheme
1,1-di chloroe thane
1,2-dichloroetheme
1,1-dichloroethene
cis-1,2 -dichloroethene
trems-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropane
1,1-dichloropropene
cis-1,3 -dichloropropene
trans-1,3-dichloropropene
1,2 -di chlorobenzene
igBkdi chlorobenzene
I^Bdi chlorobenzene
ec^lbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2- tetrachloroe t:hane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroethane
trichloroethene
trichlorofluorome theme
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4 -methyl-2-pentanone
RESULT
u u 2 IB
U
U
U
U
U
U
U
U
u u
u
u u
u
u u u u u u
u
u u u u u u u u
u u u u
u
u
u u
u
u
u
u u u u u
u
u u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION AJtIiLLYZED
LIMIT
10
10
10
10
10
10
10
10
10,
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
IO/:LO/95
lO/JLO/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAStt
SW-846, 8260A
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
Page #: 13
November 10, 1995 13:57 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #106, 10 FT. #646 DUP. Lab ID: 9510001-08A CoUected: 10/02/95 09:40:00
TEST
Volatile Orgemics
2-hexemone
fluorobenzene
chlorobenzene-d5
1,4 -di chlorobenzene
RESTJLT
U
350920
159659
-d4 56364
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
ANALYZED BY
10/10/95 MMR
10/10/95 MMR
10/10/95 MMR
10/10/95 MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorometheme
1,2-dichloroetheme -d4
toluene-d8
bromofluorobenzene
%Recovery
82.2
65.5
123
107
METHOD/CAStt
SW-846,8260A
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4 TO 112
53.3 TO 121
85.6 TO 143
80.6 TO 130
Sample ID: GD #9, 5 FT. #628, M-19A LabID: 9510001-09A CoUected: 10/02/95 11:05:00
TEST RESITLT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAStt
pH
Acid Digestion
Cadmium
Chromium
Lead
Silver
7.86
10/17/95
0.78
11.8
U
U
pH Unit
DATE
ug/g
ug/g
ug/g
ug/g
0
0
1
0
.1
.3
7
2
10/03/95
10/17/95
10/23/95
10/23/95
10/23/95
10/23/95
MTB
KWB
LVD
LVD
LVD
LVD
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Sample ID: GD #9, 10 FT. #628, M-19A LabID: 9510001-lOA CoUected: 10/02/95 11:27:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAStt
pH
Acid Digestion
Cadmium
Chromium
7.86
/17/95
0.38
16.1
pH Unit
DATE
ug/g
ug/g
0.1
0.3
10/03/95
10/17/95
10/23/95
10/23/95
MTB
KWB
LVD
LVD
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
Page#: 14
November 10, 1995 13:57 CERTIFICATE OF AN^^LLYSIS
RESULTS BY SAMPLE
pie ID: GD #9, 10 FT. #628, M-19A LabID: 9510001-lOA CoUected: 10/02/95 11:27:00
TEST RESULT UNITS DETECTION ANJILYZED BY
LIMIT
METHOD/CAStt
Lead
Silver
6.45
U
ug/g
ug/g
1.6 10/23/95 LVD
0.2 10/23/95 LVD
SW-846, 6010
SW-846, 6010
Sample ID: GD #9, 10 FT. #628 DUP. LabID: 9510001-llA CoUected: 10/02/95 11:27:00
TEST RESULT UNITS DETECTION ANJLLYZED BY
LIMIT
METHOD/CAStt
pH
Acid Digestion
Cadmium
Chromium
Lead
kver
7.78
10/17/95
0.58
14.4
6.65
U
pH Unit
DATE
ug/g
ug/g
ug/g
ug/g
0
0
1,
0,
.1
.3
.7
.2
10/03/95
10/17/95
10/23/95
10/23/95
10/23/95
10/23/95
MTB
KWB
LVD
LVD
LVD
LVD
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Sample ID: GD #17, 5 FT. #628, M-19A LabID: 9510001-12A CoUected: 10/02/95 11:56:00
TEST RESULT ITNITS DETECTION AliTALYZED BY
LIMIT
METHOD/CAStt
pH
Acid Digestion
Cadmium
Chromium
Lead
Silver
7.79
10/17/95
0.86
16.1
8.44
U
pH Unit
DATE
ug/g
ug/g
ug/g
ug/g
0
0
1,
0,
.1
.3
.6
.2
10/03/95
10/17/95
10/23/95
10/23/95
10/23/95
10/23/95
MTB
KWB
LVD
LVD
LVD
LVD
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Page #: 15
November 10, 1995 13:57 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: GD #17, 8.5 FT.,#628, M19A LabID: 9510001-13A CoUected: 10/02/95 12:10:00
TEST RESITLT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAStt
pH
Acid Digestion
Cadmium
Chromium
Lead
Silver
7.71
10/17/95
0.49
16.7
U
U
pH Unit
DATE
ug/g
ug/g
ug/g
ug/g
0
0
1
0
.1
.3
7
2
10/03/95
10/17/95
10/23/95
10/23/95
10/23/95
10/23/95
MTB
KWB
LVD
LVD
LVD
LVD
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Sample ID: GD #26, 5 ft. #628, M-19A LabID: 9510001-14A CoUected: 10/02/95 13:40:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAStt
pH
Acid Digestion
Cadmium
Chromium
Lead
Silver
7.82
10/17/95
0.77
14.5
U
U
pH Unit
DATE
ug/g
ug/g
ug/g
ug/g
0
0
1
0
1
3
6
2
10/03/95
10/17/95
10/23/95
10/23/95
10/23/95
10/23/95
MTB
KWB
LVD
LVD
LVD
LVD
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Sample ID: GD #26, 10 FT #628, M-19A Lab ID: 9510001-15A CoUected: 10/02/95 14:02:00
TEST RESULT ITNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAStt
pH
Acid Digestion
Cadmium
Chromium
Lead
7.81
10/17/95
0.78
12.2
U
pH Unit
DATE
ug/g
ug/g
ug/g
0.1
0.3
1.6
10/03/95
10/17/95
10/23/95
10/23/95
10/23/95
MTB
KWB
LVD
LVD
LVD
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
Page tt: 16
November 10, 1995 13:57 CERTIFICATE OF ANAJLYSIS
RESULTS BY SAMPLE
4lb le ID: GD #26, 10 FT#628, M-19A LabID: 9510001-15A CoUected: 10/02/95 14:02:00
TEST RESITLT ITNITS DETECTION AJMiJiYZED BY METHOD/CAStt
LIMIT
Silver U ug/g 0.2 10/23/95 LVD SW-846, 6010
Page it: 17
Data Reporting Qualifiers
u# U Compound was analyzed for but not detected. Indicates compound was below detection U
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1. IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of tbe instniment.
BDL Indicates an analyte which was below the detection Umits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits. If surrogate recoveries are out
of limits, any values reported are for indication only.
o
ENVIRONMENTAL LAB WORK RP:QUEST ^'^iCC^f-
€ ° THIOKOL ENVIRONMENTAL LABORATORY LWR No. El 1067
FROM: .•) /i F iVj^/Z^y 47.^^Q
COST CENTER
iu^4ii I lE'fZC'
WORK ORDER
/G-^'9r
ORGANIZATION
'lUlf'/jii/l-U /I h£7 ^UIL STOP
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RETORT RESULTS TO:
HELEN yyARD, MS 301
/
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7
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, t>ij:iU,.'-ii4<iJ
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SAMPLE INFORMATION
LOCATION
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TEST REMARKS
•Sfc-, ^^, C^y "PJ-j, Suf^'fr ^ ^td
ll
do A - €-2(.0C
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CHAIN OF CUSTODY
RELLNQUISHED BY
-4J(yat7^^
DATE
/0'3'f7~
TIME
Idd-B
RECEIVED BY
/77/dZ^^yr
DATE
'//^^ r-^r
TIME
/<//y^
FOR LABORATORY USE ONLY
PATE COMPLETED
#
DATE REPORTED
ENVIROINME :NTAL LAB wc
™= TinOKOL ENVIRONMENTAL LABORATORY
FROM: /) /~-4 /: a-'a/l^-
ORGAM ZATION
BCTENSION
MAILSTOP
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LWR No. ^//^><d 7
p>£t^jy 2—
COST CENTER WORK OROER
"" •
REPORT RESULTS TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPIX DATE TYPE LOCATION TIME TEST REMARKS
""1 -i-'^ 4^/
•//L /o-?-yr •/ St/icl Zl'1^3 Io3o PM-32L-O<7,
ll ll y II II
—^^
Zn7Ai/l'' .dd. ///Uk. l><^ l}.'d</ora/r ,CM ll n y 11 II
ViiP I I 4 ^cr ^3
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^-l~~l=6^4-^5f:f-^ ^/tcd' L—&^-^F-y>/< f/idtrch: "— -Vo- /lc/4 -c/o-•-p^^hcid^. J-
Ft /^•?•^^ / klilMMdd. ihh^ 7L-/u^^.u I iL7/k fH
X i^cdUci Uf fll^inu! tadi'
CHAIN OF CUSTODY
RF1,INQL1SIIEDBY
^4^4C^
DATE
-iP-^'^F
TIME
/4^d^
RECEIVED BY
//////d^.^ ^ b ' <» L (,.{j<ry^t^—
DATE
-y^/-7'57r
TIME
/yy<<-
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTS) SIGNATl-RE
December 11, 1995 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward MIS 301
Thiokol Corp, Ut 84322
A.F. WALKER
EXT 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham City, Ut 84302-0707
Analytical Labs MIS 245
Atm: Dr. John Terry
Tele: 801-863-2384
Work Orders 9510004 Sample and Test Code IdentiTication
LabID:
OIA
Sample ID:
SWMU #493; SURFACE
LabID:
02A
Sample ID:
SWMU #493, 2 FT DEEP
LabID:
03 A
Sample ID:
MANUF. BACKGROUND SURFACE
LabID:
04A
Sample ID:
MANUF. BACKGROUND 2 FT
Test Codes and Names
PH
3050
SB AE2
CR AE2
PB AE2
AS GF2
S04IC2
pH
Acid Digestion
Antimony
Chromium
Lead
Arsemc
Sulfate
Test Codes and Names
PH
3050
SB AE2
CR AE2
PB AE2
AS GF2
S04IC2
pH
Acid Digestion
Antimony
Chromium
Lead
Arsenic
Sulfate
Test Codes and Names
PH
Tl GF2
CL04
HMX
NG
3050
SB AE2
BE AE2
B AE2
CD AE2
CR"AE2
PB AE2
MN AE2
NI AE2
AG AE2
ZN~AE2
AS~GF2 HG" CV2
SE GF2
82T0S
CN AU2
S04IC2
8260S
pH
Titanium
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Antimony
Beryllium
Boron
Cadmium
Chromium
Lead
Manganese
Nickel
Silver
Zinc
Arsenic Mercury
Selenium
Semi-Volatile Organics
Total Cyanide
Sulfate
Volatile Organics
Test Codes aiid Names
PH
TI GF2
CL04
HMX
NG
3050
SB AE2
BE AE2
B AE2
CD AE2
CR AE2
PB AE2
MN AE2
pH
Titanium
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Antimony
Beryllium
Boron
Cadmium
Chromium
Lead
Manganese
Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 9056
Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 9056 Method
EPA 150.1
EPA 283.2
SOP 314
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,
SW-846,
SW-846,
SW-846,
SW-846, 9012
SW-846, 9056
SW-846,8260A Method
EPA 150.1
EPA 283.2
SOP 314
SOP 420
SOP 420
SW-846. 3050
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
, 7060
, 7471
, 7740
,8270
Page #: lof H
Work Order # 9510004
LabID:
04A
Sample ID:
MANUF. BACKGROUND 2 FT
LabID:
05A
Sample ID:
MANUF. BACKGROUND 5 FT
LabID:
~06A
Samp e ID:
MANUF. BACKGROUND 10 FT
LabID:
07A
Sample ID:
MANUF BACKGROUND 10 FT-DUP
Test Codes and Names
NI AE2
AG AE2
ZN AE2
AS GF2
HG CV2
SE GF2
82T0S
CN AU2
S04IC2
8260S
Nickel
Silver
Zinc
Anenic
Mercury
Selenium
Semi-Volatile Organics
Total Cyanide
Sulfate
Volatile Organics
Test Codes and Names
PH
TI GF2
CL04
HMX
NG
3050
SB AE2
BE AE2
B AE2
CD AE2
CR AE2
PB AE2
MN AE2
NI AE2
AG AE2
ZN AE2
AS GF2
HG CV2
SE GF2
82T0S
CN AU2
S04IC2 8260S
pH
TiUnium
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Antimony
Beryllium
Boron
Cadmium
Chromium
Lead
Manganese
Nickel
Silver
Zinc
Arsenic
Mercury
Selenium
Semi-Volatile Organics
Total Cyanide
Sulfate Volatile Organics
Test Codes and Names
PH
n GF2
CL04
HMX
NG
3050
SB AE2
BE AE2
B A£2
CD AE2
CR AE2
PB AE2
MN AE2
NI AE2
AG AE2
ZN AE2
AS GF2
HG CV2
SE GF2
8270S
CN AU2
8260s
pH
Titanium
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Antimony
Beryllium
Boron
Cadmium
Chromium
Lead
Manganese
Nickel
Silver
Zinc
Arsenic
Mercury
Selenium
Semi-Volatile Organics
Total Cyanide
Volatile Organics
Test Codes and Names
PH
TI GF2
CL04
HMX
NG
3050
SB AE2
BE AE2
B A£2
CD AE2
CR AE2
PB AE2
MN AE2
NI AE2
pH
Titanium
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Antimony
Beryllium
Boron
Cadmium
Chromium
Lead
Manganese
Nickel
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8270
SW-846, 9012
SW-846, 9056
SW-846,8260A
Method
EPA 150.1
EPA 283.2
SOP 314
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8270
SW-846, 9012
SW-846, 9056 SW-846,8260A
Method
EPA 150.1
EPA 283.2
SOP 314
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8270
SW-846, 9012
SW-846,8260A
Method
EPA 150.1
EPA 283.2
SOP 314
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
•
a
Page #:2
Work Order # 9510004 Sample and Test Code Identifiicaition
LabID:
07A
Sample ID:
MANUF BACKGROUND 10 FT-DUP
Test Codes and Names
•
Lab ID:
08A
Sample ID:
MANUF. BACKGROUND 15 FT
UbID:
09A
Sample ID:
SWMU #254 4 FT
•
AG AE2
ZN AE2
AS GF2
HG CV2
SE GF2
CN AU2
Silver
Zinc
Arsenic
Mercury
Selenium
Total Cyanide
Test Codes and Names
PH
TI GF2 CL04
HMX
NG
3050
SB AE2
BE AE2
B AE2
CD AE2
CR AE2
PB AE2
MN AE2
NI AE2
AG AE2
ZN AE2
AS GF2
HG CV2
SE GF2 8270S
CN AU2
8260s
pH
Titanium Perchlorate
HMX
Nitroglycerine
Acid Digestion
Antimony
Beryllium
Boron
Cadmium
Chromium
Lead
Manganese
Nickel
Silver
Zinc
Arsenic
Mereury
Selenium Semi-Volatile Organics
Total Cyanide
Volatile Organics
Test Codes and Names
PH
3050
SB AE2
S04IC2
pH
Acid Digestion
Antimony
Sulfate
Comments
Method
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 9012 Method
EPA 150.1
EPA 283.2
SOP 314
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 7060
SW-846, 7471
SW-846, 7740
SW-846, 8270
SW-846, 9012
SW-846,8260A
Method
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 9056
Report: There is the possibiUty of a matrix interference for antimony
in these samples with the 3050 digestion. Howtsver, there was
not direct evidence of this problem.
y^ Certified By
Page #:3
TTiis is to certify that the folio-wing samples were analyzed using good laboratory practices
to show the following results.
Sample ID: SWMU #493; SURFACE LabID: 9510004-OlA CoUected: 10/03/95 08:58:00
TEST RESULT tJNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
pH
Acid Digestion
Antimony
Chromiuin
Lead
Arsenic
Sulfate
7.84
10/17/95
U
22.0
5.03
7.3
U
pH Unit
DATE
ug/g
ug/g
ug/g
ug/g
mg/L
3
0
1
1
.0
.3
.5-
8
3
10/09/95
10/17/95
10/23/95
10/23/95
10/23/95
11/02/95
11/08/95
AA
KWB
LVD
LVD
LVD
CRS
CRS
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 9056
Sample ID: SWMU #493, 2 FT DEEP LabID: 9510004-02A CoUected: 10/03/95 09:15:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
pH
Acid Digestion
Antimony
Chromium
Lead
Arsenic
Sulfate
7.92
10/17/95
U
28.3
7.08
5.7
26
pH Unit
DATE
ug/g
ug/g
ug/g
ug/g
mg/L
3
0
1
1
.2
.3
.6
.9
3
10/09/95
10/17/95
10/23/95
10/23/95
10/23/95
11/02/95
11/08/95
AA
KWB
LVD
LVD
LVD
CRS
CRS
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 9056
Sample ED: MANUF. BACKGROUND SURFACELab ID: 9510004-03A CoUected: 10/03/95 10:00:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
pH
Titanium
7.67 pH Unit
466 ug/g
10/09/95 AA EPA 150.1
64 11/22/95 CRS EPA 283.2
Page #: 4 a
December 11, 1995 07:49 CERTIFICATE OF ANi^iLYSIS
RESULTS BY SAMPLE
• pie ID: MANUF. BACKGROUND SURFACELab ID: 9510004-03A CoUected: 10/03/95 10:00:00
TEST
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Antimony
1
Beryllium
Boron
Cadmium
Chromium
Lead
Manganese
0el
Silver
Zinc
Arsenic
Mercury
Selenium
Semi-Volatile Organics
phenol
bis(2-chloroethyl)ether
2-chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis (2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
RESULT
u
u
u
10/17/95
U
0.77
2.80
0.66
18.7
U
373
13.6
U
54.8
8.2
U
1.5
U
U
U
u u u
u u u
u u
u
u u u
tJNITS
ug/g
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
3.8
0.500
0.500
3.2
0.1
0.4
0.1
0.3
1.6
0.1
0.64
0.2
0.3
1.9
0.014
1.5
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANJ^YZED
10/18/95
10/13/95
10/13/95
10/17/95
10/23/95
10/23/95
10/23/95
10/23/95
lO/:23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
11/02/95
10/25/95
11/02/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
BY
CRS
KMS
KMS
KWB
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SOP 314
SOP 420
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
3050
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
7060
7471
7740
8270
Page U: 5
December 11, 1995 07:49 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MANUF. BACKGROUND SURFACELab ID: 9510004-03A CoUected: 10/03/95 10:00:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Semi-Volatile Organics
bis(2-chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4-chloroaniline
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroaniline
dimethylphthalate
acenaphthylene
3-nitroemiline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4 -nitrociniline
4,6-dinitro-2-methylphenol
n-nitrosodiphenylamine
4 -bromopheny1-phenylether
hexachlorobenzene
pentachlorophenol
phenanthrene
anthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoremthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz (a, h) auithracene
benzo (g,h, Dperylene
u
u
u u
u u
u u
u u u u u u u u u u u u u u u u
u u
u u
u u u u u 39 BJ
u u u u u
u
u
u u u u u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
11/01/95
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8270
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
Page #: 6 o
December 11, 1995 07:49 CERTIFICATE OF ANAJLYSIS
RESULTS BY SAMPLE
pie ED: MANUF. BACKGROUND SURFAfcELab ID: 9510004-03A: CoUected: 10/03/95 10:00:00
TEST REStTLT UNITS DETECTION AN;LLYZED BY
LIMIT
METHOD/CAS#
Semi-Volatile Organics SW-846, 8270
Surrogate/Recovery Data For Semi-Volatile Organics 8270S
Surrogate
2 -fluorophenol
phenol-d5
nitrobenzene-d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
Total Cyanide
Sulfate
Volatile Organics
benzene
bromoben zene
bromochloromethane
bromodichloromethane
bromoform
bromome thane
n-butylbenzene
j^^ butylbenzene
^^K - butylbenzene
CTffoon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
4-chlorotoluene
dibromochlorome thane
1,2-dibromo-3 -chloropropan
1,2-dibromoethane
dibromomethane
dichlorodifluoromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-l,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
0.17
U
ug/g
mg/L
u
u u
u u
u u
u u
u
u u 4 OB
U
u u u
u
u u u u u u u u u u u
u
u
u u u u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
60.40
63.60
61.68
68.74
88.68
124.3
0.15
3
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/13/95
11/08/95
10/10/95
IO/:LO/95
IO/:LO/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
TO 121
TO 113
TO 12 0
TO 115
TO 122
TO 137
KEN
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 9012
SW-846, 9056
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
Page it: 7
December 11, 1995 07:49 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MANUF. BACKGROUND SURFACELab ID: 9510004-03A CoUected: 10/03/95 10:00:00
TEST
Volatile Organics
hexachlorobutadi ene
isopropylbenzene
4 - isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl- 2-pentanone
2-hexanone
fluorobenzene
chlorobenzene- d5
1,4 -dichlorobenzene-d4
RESULT
u U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
792331
326632
96932
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
,
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data Por Volatile Organics 8260S
Surrogate
dibromofluorometheme
1,2-di chloroe thane -d4
toluene-d8
bromofluorobenzene
%Recovery
86.7
78.0
133
115
Recovery Lim
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
METHOD/CAS#
SW-846,8260A
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1 j^
78-93-3 WM
108-10-1 ^^
591-78-6
INTSTDl
INTSTD2
INTSTD3
its
Sample ID: MANUF. BACKGROUND 2 FT LabID: 9510004-04A CoUected: 10/03/95 10:10:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
PH
Titanium
8.01 pH Unit
245 ug/g 66
10/09/95 AA
11/22/95 CRS
EPA 150.1
EPA 283.2
Page #: 8
•
December 11, 1995 07:49 CERTIFICATE OF AN^kLYSIS
RESULTS BY SAMPLE
# pie ID: MANUF. BACKGROUND 2 FT Lab ED: 9510004-04A CoUected: 10/03/95 10:10:00
TEST
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Antimony
Beryllium
Boron
Cadmium
Chromium
Lead
Manganese
^^kel
Silver
Zinc
Arsenic
Mercury
Selenium
Semi-Volatile Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
RESULT
U
u
u
10/17/95
U
0.50
6.90
0.58
14.0
U
218
11.4
U
38.4
10
U
2.4
U
U
U
U
U
U
U
u u
u
u u
u u u
UNITS
ug/g
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
• ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
4.0
0.500
0.500
3.3
0.1
0.4
0.1
0.3
1.6
0.1
0.66
0.2
0.3
2.0
0.011
l.G
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANJ.^LYZED
10/18/95
10/13/95
10/13/95
10/17/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
11/02/95
10/25/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
BY
CRS
KMS
KMS
KWB
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SOP 314
SOP 420
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
3050
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
7060
7471
7740
8270
Page a: 9
December 11, 1995 07:49 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MANUF. BACKGROUND 2 FT LabID: 9510004-04A CoUected: 10/03/95 10:10:00
TEST RESULT TJNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Semi-Volatile Organics
bis(2-chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4 -chloroaniline
hexachlorobutadiene
4-chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroaniline
dime thyIphthalate
acenaphthylene
3-nitroaniline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroaniline
4,6-dinitro-2-methylphenol
n-nitrosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenz ene
pentachlorophenol
phenanthrene
emthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h) emthracene
benzo(g,h,i)perylene
u
u u u u u u u u u u u u u u
u u u
u u u
u u
u
u
u u u u u u u u 31 BJ
u u
u u
u u u u u
u
u u u u
ug/Kg
ug/Kg.
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, i
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
8270
•
Page it: 10
December 11, 1995 07:49 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
#> le ID: MANUF. BACKGROUND 2 FT ''Lab ID: 9510004-04A CoUected: 10/03/95 10:10:00
TEST
Semi-Volatile Organics
Total Cyanide
Sulfate
Volatile Organics
benzene
bromobenzene
bromochlorome thane
bromodichloromethane
bromoform
bromomethane
n-butylbenzene
1^^ butylbenzene
f^B-butyli3enzene
cHoon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
RESULT
Surrogate
UNITS
/Recovery Data
Surrogate
2 -fluorophenol
phenol -d5
nitrobenzene-d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl
1,2-dibromo-3-chloropropan
1,2-dibromoethane
dibromome thane
dichlorodifluoromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-l,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
-dl4
U
U
U
U
U
U
U
U
U
U
U
U
U
u 34B
u U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/g
mg/L
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
AwiliYZED BY METHOD/CAS#
SW-846, 8270
For Semi-Volatile Organics 8270S
%Recovery
67.84
67.08
66.95
72.69
88.84
130.8-
0.15
3
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/13/95
11/08/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
TO 121
TO 113
TO 12 0
TO 115
TO 122
TO 137
KEN
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 9012
SW-846, 9056
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
Page#: 11
December 11, 1995 07:49 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MANUF. BACKGROUND 2 FT Lab ED: 9510004-04A CoUected: 10/03/95 10:10:00
TEST
Volatile Organics
hexachlorobutadi ene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2- tetrachloroetheme
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
RESULT
U
U
U
U
U
u u u u u u u
u
u
u u u u u u u u u 15B
u u
u 662202
275028
100348
Surrogat
Surrogate
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
e/Recovery Data For Volat
dibromofluoromethane
1,2-di chloroe thane -d4
toluene-d8
bromofluorobenzene
%Recovery
74.1
66.2
136
104
ANALYZED
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
ile Organics 8260S
METHOD/CAS#
SW-846,8260A
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1 J^
78-93-3 !•
106-10-1 ^^
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Sample ID: MANUF. BACKGROUND 5 FT Lab ID: 9510004-05A CoUected: 10/03/95 10:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
pH
Titanium
8.26 pH Unit
621 ug/g
10/09/95 AA
66 11/22/95 CRS
EPA 150.1
EPA 2 83.2
Page #: 12
December 11, 1995 07:49 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
#> le ID: MANUF. BACKGROUND 5 FT ' LabID: 9510004-05A;' CoUected: 10/03/95 10:20:00
TEST RESULT UNITS DETECTION ANiiLYZED BY
LIMIT
METHOD/CAS#
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Antimony
Berylliijm
Boron
Cadmium
Chromitim
Lead
Manganese
#" S i-l ver
Zinc
Arsenic
Mercury
Selenium
Semi-Volatile Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
U
U
U
10/17/95
4.86
0.89
U
0.28
20.7
U
340
15.5
U '
53.4
13.7
U
1.7
u u u u u u u u u
u u u u
u u
ug/g
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
4.0
0.500
0.500
3.3
0.1
0.4
0.1
0.3
1.6
0.1
0.66
0.2
0.3
2.0
0.012
1.6
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
10/18/95
10/13/95
10/13/95
l0/:^7/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
11/02/95
10/25/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/0:2/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
CRS
KMS
KMS
KWB
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SOP 314
SOP 420
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
3050
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
7060
7471
7740
8270
Page #: 13
December 11, 1995 07:49 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MANUF. BACKGROUND 5 FT Lab ID: 9510004-05A CoUected: 10/03/95 10:20:00
TEST
Semi-Volatile Organics
bis(2-chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4-chloroemiline
hexachlorobutadiene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroaniline
dimethylphthalate
acenaphthy1ene
3-nitroaniline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroaniline
4,6-dinitro-2-methylphenol
n-nitrosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
phenanthrene
anthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3 -cd)pyrene
dibenz(a,h) emthracene
benzo(g,h, Dperylene
RESULT
u U
u u
u u u
u u u u u
u u
u u u
u u
u u u u
u u u u
u u u u
u u 27 BJ
u u u
u
u u
u u u u u
u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
330
330,
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3 J^
86-73-7 IV
100-01-06 ^^
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
Page tt: 14
•
December 11, 1995 07:49 CERTIFICATE OF AN^XYSIS
RESULTS BY SAMPLE
#> le ID: MANUF. BACKGROUND 5 FT * LabID: 9510004-05A CoUected: 10/03/95 10:20:00
TEST RESULT UNITS DETECTION AN;kLYZED BY
LIMIT
METHOD/CAS#
Semi-Volatile Organics SW-846, 8270
Surrogate/Recovery Data For Semi-Volatile Organics 8270S
Surrogate
2 - fluorophenol
phenol-d5
nitrobenzene-d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
Total Cyanide
Sulfate
Volatile Organics
benzene
bromobenzene
bromochlorome thane
bromodichloromethane
bromoform
bromomethane
n-butylbenzene
fr butylbenzene
^-butylbenzene
bon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3-chloropropan
1,2-dibromoethane
dibromomethane
dichlorodifluoromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
u
451.4
u
U
U
U
U
u u
u u U '
u u 39B
u u u
•u
u u u u
u u u
u
u u u u u u u u u u u
ug/g
mg/L
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
60,
54
57
59
62,
.44
.40
.08
.46
.88
126.8
Recovery Limits
25 TO 121
24 TO 113
23 TO 120
30 TO 115
19 TO 122
18 TO 137
0.15 10/13/95 KEN SW-846, 9012
3 11/08/95 CRS SW-846, 9056
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10/10/95
10/10/95
10/:'.0/95
10/:'.0/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
10/10/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
Page it: 15
December 11, 1995 07:49 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MANUF. BACKGROUND 5 FT LabID: 9510004-05A CoUected: 10/03/95 10:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
hexachlorobutadiene U ug/Kg
isopropylbenzene U ug/Kg
4-isopropyltoluene U ug/Kg
methylene chloride U ug/Kg
naphthalene U ug/Kg
n-propylbenzene U ug/Kg
styrene U ug/Kg
1,1,1,2-tetrachloroethane U ug/Kg
1,1,2,2-tetrachloroetheme U ug/Kg
tetrachloroethene U ug/Kg
toluene U ug/Kg
1,2,3-trichlorobenzene U ug/Kg
1,2,4-trichlorobenzene U ug/Kg
1,1,1-trichloroethane U ug/Kg
1,1,2-trichloroethane U ug/Kg
trichloroethene U ug/Kg
trichlorofluoromethane U ug/Kg
1,2,3-trichloropropane U ug/Kg
1,2,4-trimethylbenzene U ug/Kg
1,3,5-trimethylbenzene U ug/Kg
vinyl chloride U ug/Kg
o-xylene U ug/Kg
m,p-xylene U ug/Kg
acetone U ug/Kg
2-butanone U ug/Kg
4-methyl-2-pentemone U ug/Kg
2-hexanone U ug/Kg
fluorobenzene 669118 ug/Kg
chlorobenzene-d5 310372 ug/Kg
1,4-dichlorobenzene-d4 110538 ug/Kg
SW-846,8260A
10 10/10/95 MMR 87-68-3
10 10/10/95 MMR 98-82-8
10 10/10/95 MMR 99-87-6
10 10/10/95 MMR 75-09-2
10 10/10/95 MMR 91-20-3
10 10/10/95 MMR 103-65-1
10 10/10/95 MMR 100-42-5
10 10/10/95 MMR 630-20-6
10 10/10/95 MMR 79-34-5
10 10/10/95 MMR 127-18-4
10 10/10/95 MMR 108-88-3
10 10/10/95 MMR 87-61-6
10 10/10/95 MMR 120-82-1
10 10/10/95 MMR 71-55-6
10 10/10/95 MMR 79-00-5
10 10/10/95 MMR 79-01-6
10 10/10/95 MMR 75-69-4
10 10/10/95 MMR 96-18-4
10 10/10/95 MMR 95-63-6
10 10/10/95 MMR 108-67-8
10 10/10/95 MMR 75-01-4
10 10/10/95 MMR 95-47-6
10 10/10/95 MMR 108-38-3
10 10/10/95 MMR 67-64-1
10 10/10/95 MMR 78-93-3
10 10/10/95 MMR 108-10-1
10 10/10/95 MMR 591-78-6
10/10/95 mm INTSTDl
10/10/95 MMR INTSTD2
10/10/95 MMR INTSTD3
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate %Recovery
dibromofluoromethane 84 .8
1,2-dichloroethane-d4 76.5
toluene-d8 123
bromofluorobenzene 108
Recovery Limits
58.4 TO 112
53.3 TO 121
85.6 TO 143
80.6 TO 130
Sample ID: MANUF. BACKGROUND 10 FT Lab ID: 9510004-06A CoUected: 10/03/95 10:30:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
pH
Titanium
7.90 pH Unit
522 ug/g
10/09/95 AA EPA 150.1
65 11/22/95 CRS EPA 283.2
Page #: 16
December 11, 1995 07:49 CERTIFICATE OF ANAJLYSIS
RESULTS BY SAMPLE
i^ -.U'\
le ID: MANUF. BACKGROUND 10 FT ' LabID: 9510004-06A CoUected: 10/03/95 10:30:00
TEST
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Antimony
Beryllium
Boron
Cadmium
Chromium
Lead
Manganese
pel
S^rer
Zinc
Arsenic
Mercury
Selenium
Semi-Volatile Organics
phenol
bis(2-chloroethyl)ether
2-chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
RESULT
u
u
u
10/17/95
u
0.88
7.70
0.38
18.3
U
333
12.8
U
57.0
7.8
U
2.5
U
U
U
U
u
u u u u u u u u
u
u
UNITS
ug/g
MG/KG-
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
3.9
0.500
0.500
3.3
0.1
0.4
0.1
0.3
1.6
0.1
0.65
0.2
0.3
2.0
0.013
1.6
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANAIiYZED
10/18/95
10/13/95
10/13/95
10/17/95
10/:!3/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
11/01/95
10/25/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
BY
CRS
KMS
KMS
KWB
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SOP 314
SOP 420
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
3050
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
7060
7471
7740
8270
Page #: 17
December 11, 1995 07:49 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample DD: MANUF. BACKGROUND 10 FT LabID: 9510004-06 A CoUected: 10/03/95 10:30:00
TEST
Semi-Volatile Organics
bis (2-chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4-chloroaniline
hexachlorobutadi ene
4 -chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroaniline
dimethylphthalate
acenaphthylene
3-nitroemiline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroaniline
4,6-dinitro-2-methylphenol
n-ni trosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenz ene
pentachlorophenol
phenanthrene
emthracene
di -n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h)anthracene
benzo(g,h, Dperylene
RESULT
u u u u u u u
u u
u
u u
u u
u u u
u u u u u u
u
u u u u u u u u u u
u u u
u u u
u u
u u u
u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3 J^
86--'3-7 VV
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
Page#: 18
December 11, 1995 07:49 CERTIFICATE OF ANi^ULYSIS
RESULTS BY SAMPLE
'i:'f 'ii:
pie ID: MANUF. BACKGROUND 10 FT ?^ -Lab ID: 9510004-06A CoUected: 10/03/95 10:30:00
TEST
Semi-Volatile Organics
Total Cyanide
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodi chlorome thane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
^y*on tetrachloride
^^Brobenzene
VBroroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
RESULT tJNITS
Surrogate/Recovery Data
Surrogate
2-fluorophenol
phenol -d5
nitrobenzene i-d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
1,2-dibromo-3 -chloropropem
1,2-dibromoethane
dibromomethane
dichlorodifluoromethane
1,1-dichloroethane
1,2-dichloroethcme
1,1-dichloroethene
cis-1,2-dichloroethene
trans -1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropeme
2,2-dichloropropane
1,l-dichloropropene
cis-1,3 -dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
u
U
U
U
u
u
u
u u u u u
u .
u u
u u u u u u
u u u
u
u u
u u u u .
u
u u u u u
u u
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
ANJLLYZED BY METHOD/CAS#
SW-846, 8270
For Semi-Volatile Organics 8270S
%Recov6ry
73.08
72.76
74.25
77.60
76.88
134.9
0.15
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Recovery Limits
25
24
23
30
19
18
10/13/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
TO 121
TO 113
TO 12 0
TO 115
TO 122
TO 137
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 9012
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
Page if: 19
December 11, 1995 07:49 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MANUF. BACKGROUND 10 FT Lab ID: 9510004-06A CoUected: 10/03/95 10:30:00
TEST
Volatile Organics
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
REStJLT
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,l-trichloroethane
1,1,2-trichloroethane
trichloroethene
tri chlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl- 2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
u
u u U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u u u
u 926891
400572
124406
tJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10,
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluorometheme
1 ,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
%Recovery
85.5
76.2
131
111
METHOD/CAS#
SW-846,8260A
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1 4^
591-78-6 ^V
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Sample ID: MANUF BACKGROUND 10 FT-DUPLab ID: 9510004-07A CoUected: 10/03/95 10:30:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAStt
PH
Titanium
Perchlorate
7.90 pH Unit
519 ug/g
U ug/g
10/09/95 AA EPA 150.1
66 11/22/95 CRS EPA 283.2
3.9 10/18/95 CRS SOP 314
Page #: 20
CERTIFICATE OF AN/O^YSIS
RESULTS BY SAMPLE
December 11, 1995 07:49
^^ple ID: MANUF BACKGROUND 10 FT-DUPLab ID: 9510004-07A CoUected: 10/03/95 10:30:00
TEST RESULT TJNITS DETECTION JaT.?^YZED BY
LIMIT
METHOD/CAS#
HMZ
Nitroglycerine
Acid Digestion
Antimony
Beryllium
Boron
Cadmium
Chromium
Lead
Manganese
Nickel
Zinc Zinc
Arsenic
Mercury
Selenium
Total Cyanide
u
u
10/17/95
U
0.81
5.50
0.38
18.3
U
310
13.1
U
51.6
11
U
U
u
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
0.500
0.500
3.3
0.1
0.4
0.1
0.3
1.6
0.1
0.66
0.2
0.3
2.0
0.0093
1.6
0.15
10/13/95
10/13/95
10/17/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
11/02/95
10/25/95
11/02/95
10/13/95
KMS
KMS
KWB
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
KEN
SOP
SOP
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
420
420
3050
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
7060
7471
7740
9012
Sample ID: MANUF. BACKGROUND 15 FT Lab ID: 9510004-08A CoUected: 10/03/95 10:44:00
TEST RESULT UNITS DETECTION ANJflLYZED BY
LIMIT
METHOD/CAS#
pH
Titanium
Perchlorate
HMX
7.82 pH Unit 10/09/95 AA EPA 150.1
421 ug/g 65 11/22/95 CRS EPA 283.2
U ug/g 3.9 10/18/95 CRS SOP 314
U MG/KG 0.500 10/13/95 KMS SOP 420
Page #: 21
December 11, 1995 07:49 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MANUF. BACKGROUND 15 FT LabID: 9510004-08A CoUected: 10/03/95 10:44:00
TEST
Nitroglycerine
Acid Digestion
Antimony
Beryllium
Boron
Cadmium
Chromium
Lead
Manganese
Nickel
Silver
Zinc
Arsenic
Mercury
Selenium
Semi-Volatile Organics
phenol
bis(2-chloroethyl)ether
2 -chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
RESULT
U
10/17/95
3.22
0.79
9.12
0.38
18.96
U
278.65
12 .15
U
44.28
16.3
0.013
2.7
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
UNITS
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.500
3.2
0.1
0.4
0.1
0.3
1.6
0.1
0.65
0.2
0.3
1.9
0.013
1.5
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
10/13/95
10/17/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
11/02/95
10/25/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
BY
KMS
KWB
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAStt
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
3050
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010 Jj^
7060
7471
7740
8270
Page tt: 11
•
December 11, 1995 07:49 CERTIFICATE OF AN/ULYSIS
RESULTS BY SAMPLE
^^ple ID: MANUF. BACKGROUND 15 FT • LabID: 9510004-08A CoUected: 10/03/95 10:44:00
TEST RESULT
Semi-Volatile Organics
4-chloroaniline
hexachlorobutadiene
4 -chloro- 3 -me thyIphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroaniline
dimethylphthalate
acenaphthylene
3-nitroaniline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4 -chlorophenyl-phenylether
fluorene
4-nitroaniline
4,6-dinitro-2-methylphenol
^•nitrosodiphenylamine
^^Bromophenyl -phenylether
^^xachlorobenzene
pentachlorophenol
phenanthrene
anthracene
di-n-butylphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3 -cd)pyrene
dibenz(a,h)anthracene
benzo (g,h, Dperylene
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Surrogate/Recove
Surrogate
2 -fluorophenol
phenol-d5
nitrobenzene -d5
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
iry Data
DETECTION
LIMIT
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
AN.ALYZED
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
11/02/95
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAStt
SW-846, 8270
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270S
%Recovery
67.44
64.92
66.23
Recovery Limits
25
24
23
TO 121
TO 113
TO 120
Page #: 23
December 11, 1995 07:49 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MANUF. BACKGROUND 15 FT LabID: 9510004-08A CoUected: 10/03/95 10:44:00
TEST RESULT TJNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAStt
Semi-Volatile Organics 2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
Total Cyanide U
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodichloromethane
bromoform
bromome theme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chl oroe thane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3-chloropropan
1,2-dibromoethane
dibromomethane
dichlorodifluoromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2 -dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
cis-l,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethane
ug/g
u
u
u
u u u u u u u u u u u
u u u u u u u
u u u u
u u u
u
u
u u u u
u u
u u
u u u u u
u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
71.14
75.28
132.5
0.15
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
30
19
18
10/13/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
TO 115
TO 122
TO 13 7
KEN
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
SW-846, 9012
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
Page it: IA
CERTIFICATE OF AN^LLYSIS
RESULTS BY SAMPLE
December 11, 1995 07:49
^|ple ID: MANUF. BACKGROUND 15 FT " Lab ID: 9510004-08A CoUected: 10/03/95 10:44:00
TEST
Volatile Organics
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroetheme
1,1,2-trichloroethane
trichloroethene
trichlorofluorometheme
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m, p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
A w
RESULT
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u 1071312
520439
190370
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANiVLYZED
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
Surrogate/Recovery Data For Volatila Organics 8260S
Surrogate
dibromofluorometheme
1 ,2 -di chloroe thane -d4
toluene-d8
bromofluorobenzene
%Recovery
89.6
86.5
119
104
METHOD/CAStt
SW-846,8260A
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
58.4
53.3
85.6
80.6
TO 112
TO 121
TO 143
TO 130
Sample ID: SWMU #254 4 FT Lab ID: 9510004-09A CoUected: 10/02/95 15:57:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAStt
pH
Acid Digestion
Antimony
Sulfate
7.97
10/17/95
4.26
32
pH Unit
DATE
ug/g
mg/L
3.1
3
10/09/95
10/17/95
10/23/95
11/08/95
AA
KWB
LVD
CRS
EPA 150.1
SW-846, 3050
SW-846, 6010
SW-846, 9056
Page #: 25
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection #
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1.1J with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits. If surrogate recoveries are out
of limits, any values reported are for indication only.
ENVIRONMENTAL LAB WORK REQUEST
^//"/
tak THIOKOL ENVIRONMENTAL LABORATORY LWR No. £11067
FROM: ,1 / /^
A A- iFj}///yy
ORGANIZATION _
i^/1iyr/?;i/i,u // /JF
EXTENSION
\U1LST0P
COST CENTER WORK ORDER
I'i'rZC'
DATE 1
REPORT RESULTS TO:
HELEN WARD. .MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION
C
TIME IEST REMARKS
1f/l-^pl\ -TT-•7W4-:SS6-^h, Ai, Cr^T'hu'^if'-'^ , |3r/
•l£-^^'/i H 9-/-r
3. JC'U/IUt'tte.ftij'int •^ $•-?"/! ^^ /l-l^l /OOO do A ~ 'e>ZL.o<
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Wf
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5" II y II 5a^^A.
<•' ll y ll ^<!C^€
CHAIN OF CUSTODY
RELINQUISHED BY
^OJ/lttH^
DATE
JD'3'?r\
TIME
I4^P>
RECEIVED BY
•
^7/////;..yy
• ' /
DATE
' //!^r .^y
TIME
/(/^y4^
FOR LABORATORY USE ONLY
DA FE COMPLETED DATE REPORTED SIGNATURE
ENVIRONMENTAL LAB WORK REQUEST
il 1^1 o Iiif ^/
™= TinOKOL ENVTRONMENTAL LABORv\TORY
FROM: /) r 4 7^ a-'a/t^-
ORGAM ZATION
EXTEMSION
MAU. STOP
LWR No. /EZ/^O 7
COSTaXTtX WORK OROER tJATC -1
RIPOflT RCSULn TOi
HELEN WARD. .MS 301
1
s
<
/
\
SAMPIX DATE TITE
G 1 C
SAMPLE INFORMATION
LOCATION
'• ^^y vf'^1 t/^^-f-J y ^->^ ^1 zi'i^^
/I
ll
n
II
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TIME
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i'^A- ^ZL-O<7.
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fiii^ OJ, Cr, /)i, py, 3^^ i/.; .^
m^M/T , d^. -^/iu. ^ A
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-i^ ^1
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5, —" *c^O Z^iy 1 c^iy
REMARKS
^.'ddo/aZc: , C/7
—!-•. f -yd L<r.^ ,w u 1 M ^ J
(L-L^.. r Li/^d> ed
</' ^ '. .
' CHAIN OF CUSTODY
RELXSQClSirED BV DATE TIME
,/^=U0/^Z7CdL^^__.j--f,.gf-\ /(/^a^
=^=^^1^=^
RECnVEDBY
//yy///;.. /
1^ " ' - •'^^•'' 'Vfi^--
DATE TBIE
' ir-'- 7-'/Z\ /tyy<-
FOR LABORATORY USE ONLY
DATE COMPIXTTB OATE REPORTED SICNATTRE
CERTIFICATE OF ANALYSIS
RESULTS LISTED BY SAMPLE
Friday, February 09,1996
TESTED FOR Thiokol: DLV
Environmental Monitoring
Helen Ward M/S 301
Thiokol Corp.UT 84322
Frank Walker
Project: Solid Wast Mgmt Invest.
Listing of Sample Information and Testing Requested
ANALYZED BY Thiokol Environmental Laboratory
Thiokol Corporation
P.O. Box 707 M/S 245
Brigham City, UT 84302-0707
801-863-5445
800-863-8080
Work Order Login Number Lll7
L^b Number Cllent Number Fteceived Collect Date/Time
L117-1 BACKGROUND SURFACE SOUTH OF M-1S3
Test Method Description
ASTMD2488-84 Unified Soil Classification
1 L117-2 BACKGROUND 2 FT. ROUTH OF M-1S3
Test Method Description
ASTM D2488-84 Unified Soil Classification
1 L117-3 BACKGROUND 6 FT. SOUTH OF M-153
Test Method Description
ASTM D2488-84 Unified Soil Classification
1 L117-4 BACKGROUND 10 FT. SOUTH OF M-153
Test Method Description
ASTM 02488-84 Unified Soil Classification
L117-6 BACKGROUND 15 FT. SOUTH OF M-153
-I0/3/9S
Matrix
Soil
110/3/95
Matrix
Soil
10/3/95
Matrix
Soil
10/3/95
Matrix
Soil
10/3/95
10/3/95 10:00:00 AM
10/3/95 10:10:00 AM
10/3/95 10:20:00 AM
10/3/95 10:30:00 AM
10/3/95 10:44:00 AM
Description
Unified Soil Classification
Test Method
ASTM D2488-84
Work Order Comments
These samples were originally submitted on wori< order #9510004.
Matrix
Soii
^ Certified By
==> ^~/^-96>
Date
Tkis is to certify that the following samples were analyzed using good lahoratory -practices to show
the folowing results:
Page 1 of 3
Sample ID: BACKGROUND SURFACE SOUTH OF M-153 UbID: L117-1 Collected: 10/3/95 10:00:00 AM
Test Method: ASTM D248B-84 Description: Unified Soil Classification Completed: 1/4/96
Sample ID: BACKGROUND 2 FT. ROUTH OF M-153 LabID: L117-2 Collected: 10/3/95 10:10:00 AM
Test Method: ASTM 02498-84 Description: Unified SoU Classification Completed: 1/4/96
Sample ID: BACKGROUND 5 FT. SOUTH OF M-153 LabID: L117-3 Collected: 10/3/95 10:20:00 AM
Test Method: ASTM 02488-84 Description: Unified Soil ClassiUcatlon Completed: 1/4/96
Sample ID: BACKGROUND 10 FT. SOUTH OF M-153 LabID: L117-4 Collected: 10/3/95 10:30:00 AM
Test Method: ASTM D2488-84 Description: Unified Soii Classification Completed: 1/4/96
Sample ID: BACKGROUND 15 FT. SOUTH OF M-153 LabID: L117-5 Collected: 10/3/95 10:44:00 AM
Test Method: ASTM D2488-84 Description: Unified Soil Classification Completed: 1/4/96
Page 2 of 3
Data Reporting Qualifiers
U Indicates compound was analyzed for and was not detected or was below the detection limit.
J Gas Chromatography and Mass Spectral Data Flag. Indicates an estimated value. This
flag is used either when estimating a concentration for tentatively identified compounds or
when the mass spectral data indicated the presence of a compound that meets the
identification criteria but the result is less than the specified detection limit (e.g. 0.8 J with a
method detection limit of 1.0)
B This flag is used when an analyte is found in the blank as welll as the sample
Detection Limit Method Detection Limit (approximately three times the signal noise level)
Reporting Limit Reporting Limit is normally the value ofthe loweirt standard run with the
analysis. The value is approximately 5 to 10 times the Method Detection Limit.
Page 3 of 3
CORPORATION
SCIENCE & ENGINEERING
9 February 1996
LWR-FY95-335
TO:
CC:
FROM:
LWR:
WO:
SUBJECT:
Frank Walker
F. E. Bares
A. Alpisa
Chemical and Physical Analysis
L117
18940
Soil Classification
Five samples of soil were examined on 01/04/96. The samples were classified according to
the visual method as described in ASTM D-2488-90.
L117-1 Characterized as Silt (ML)
Comments
Particles
HCI Rxn
Weight
Color
Dry Strength
Plasticitv
Toughness
Dilatancy
No Gravel, No Sand, Material is all fines
Positive
258 grams
Tan
Natural Lumps, Low
Low
Low
Rapid
P.O. Box 707, Brigham City, UT84302-0707 18011 863-3511
Ll 17-2 Characterized as Lean Clay (CL)
Comments
Particles
HCI Rxn
Weight
Color
Dry Strength
Plasticity
Toughness
Dilatancy
95 + % Fines, <5% Coarse Sand, just a few bits
Positive
209 grams
Tan-Yellow
Natural Lumps, Medium to High
Medium
Low
Slow
Ll 17-3 Characterized as Elastic Silt (MH)
1 Comments
Particles
HCI Rxn
Weight
Color
Dry Strength
Plasticity
Toughness
Dilatancy
Largest particles are less than 4.75 mm
Positive
178 grams
Tan-Yellow
None-Low
Medium
Low
None
Ll 17-4 Characterized as Silt (ML)
Comments
Particles
HCI Rxn
Weight
Color
Dry Strength
Plasticitv
Toughness
Dilatancy
Moist soil
No Gravel, No Sand, Material is all fines
Positive
218 grams
Light brown
None
Low
Low
Rapid
Ll 17-5 Characterized as Lean Clay (CL)
Comments
Particles
HCI Rxn
Weight
Color
Dry Strength
Plasticity
Toughness
Dilatancy
All Fines
Positive
170 grams
Yellow-Tan
Naturally Occuring Lumps, Medium
Medium
Medium
None
o
November 30, 1995 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
IB SENT Environmental Monitoring
w TO: Helen Ward M/S 301
Thiokol Corp, Ut 84322
A.F. WALKER
EXT 5390
ANALYZED
BY:
Tfiiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Oty, Ut 84302-0707
Analytical Labs M/S 245 Attn:
Tele:
Work Order tt 9511018 Samole and Test Code Identification
LabID:
OIA
LabID:
02A
LabID:
03 A
LabID:
04A
Lab ID:
05A
Sample ID:
BACKGROUND SURFACE M-136
USC
Sample ID:
BACCGROUND 2 FT., M-136
USC
Sample ID:
BACKGROUND 5 FT., M-136
USC
Sample ID:
BACKGROUND 10 FT., M-136
USC
Sample ID:
BACKGROUND 15 FT., M-136
USC
Test Codes and Names
Soil Classification
Test Codes and Names
Soil Classification
Test Codes and Names
Soil Classification
Test Codes and Names
Soil Classification
Test Codes and Names
Soil Classification
Comments
Dr. John Terry
801-863-2384
1
Method
ASTM D2488
Method
ASTM D2488
Method
. ASTM D2488
Method
ASTM D2488
Method
ASTM D2488
//-^^^^
Certried By
Page #: lof ^
This is to certify tfiat the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: BACKGROUND SURFACE M-136 LabID: 9511018-OlA CoUected: 09/18/95 15:27:00
TEST REStJLT DNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Soil Classification 11/22/95 DATE . 11/22/95 AA ASTM D2488
** See Attached Memo for Soil Classification **
Sample ID: BACKGROUND 2 FT., M-136 Lab ID: 951I018-02A CoUected: 09/18/95 15:40:00
TEST RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Soil Classification 11/22/95 DATE 11/22/95 AA ASTM D2488
** See Attached Memo for Soil Classification **
Sample ID: BACKGROUND 5 FT., M-136 LabID: 9511018-03A CoUected: 09/18/95 15:48:00
TEST RESULT tJNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Soil Classification 11/22/95 DATE 11/22/95 AA ASTM D2488
** See Attached Memo for Soil Classification **
Sample ID: BACKGROUND 10 FT., M-136 LabID: 9511018-04A CoUected: 09/19/95 08:50:00
TEST RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Soil Classification 11/22/95 DATE 11/22/95 AA ASTM D2488
** See /Attached Memo for Soil Classification **
Sample ID: BACKGROUND 15 FT., M-136 Lab ID: 9511018-05A CoUected: 09/19/95 09:00:00
TEST RESULT DNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Soil Classification 11/22/95 DATE 11/22/95 AA ASTM D2488
** See Attached Memo for Soil Classification **
Page it: 1 •
m lA GROUP:
02A GROUP:
03A GROUP:
04A GROUP:
ML;
ML;
ML;
ML;
Notes and Comments for Workorder# 9511018
90% SILT WITH SAND,
80% SILT WITH SAND,
80% SILT WITH SAND,
10% FINE GRAVEL.
10% FINE GRAVEL.
TRACE OF FINE GRAVEL.
80% SILT WITH ABOUT 15% SAND.
05A GROUP: ML; SILT WITH SAND.
^5
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection liniir
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1.1J with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the Unear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not applicable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits. If surrogate recoveries are out
of limits, any values reported are for indication only.
•
ENVIRONMENTAL LAB WORK REQUEST I J 1^ O'--1 ( ^ i\j ^-^
^' TinOKOL ENVTOONME>rrAL LABORATORY
P"' 4 // a-'a//-
ORGANIZATION
EXTENSION
.MAIL STOP
LWR No. £'///)(p 7
COSTOTfTES WORK ORDEX <iATE <J
REPORT RESULIS TO:
HELEN WARD. MS 301
SAMPLE INFORMATION
^ AcirUV fJ-i d^^ iaJ h frc^i^^o- lio-H-?^)^7'
CHAIN OF CUSTODY
Rn.rSQUlSHEDBY
/M//^^:y(^ 1
DATE
_;/-;'^r1
TIME
/4-^
RECEIVED BY
/7/77^//...y
DATE
- /^^-7^'9<r
TIME
/<yy<-
FOR LABORATORY USE 0^fLY
DATE COMPLETHJ DATE REPORTED SICNATLUE
December 11, 1995 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward MIS 301
Thiokol Corp, Ut 84322
A.F. WALKER
EXT 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Oty, Ut 84302-0707
Analytical I/lbs MIS 245
Atm:
Tele:
Work Order # 9510005 Samole and Test Code Identification
Lab ID: Sample ID: Test Codes and Names
OIA PE SAMPLE LOT #324 / #218
AL AE2
BA AE2
BE AE2
CD"AE2
CA AE2
CR AE2
CU"AE2
FE AE2
PB~AE2
MG AE2
MN AE2
MO AE2
NI AE2
K AE2
AG AE2
NA AE2 ZN AE2
SB GF2
AS~GF2
HG CV2
SE GF2
TL GF2
827DS
CN AU2
8260s
AJuminum
Barium
Beiylfium
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Silver
Sodium
Zinc
Anlimony
Arsenic
Mercuty
Selenium
Thallium
Semi-Volatile Organics
Toul Cyanide
Volatile Organics
Comments
Dr. John Terry
801-863-2384
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010 SW-846, 6010
SW-846, 7041
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 7841
SW-846, 8270
SW-846, 9012
SW-846,8260A
Report: Method 8270 (semi-volatUe) TICs
Carbazol 939ug/Kg
^97. Qiyi4yVX4n^\.
Certified By
Page #:1 of 6/
This is to certify tfiat the following samples were analyzed using good laboratory practices
to show the folio-wing results.
m. ie ID: PE SAMPLE LOT #324 / #218 LabID: 9510005-01A CoUected:
TEST
Aluminum
Barium
Beryllium
Cadmium
Calcium
Chromium
Copper
iron
Lead
Magnesium
Manganese
I^^Bdenum
Nickel
Potassium
Silver
Sodium
Zinc
Antimony
Arsenic
Mercury
Selenium
Thallium
Semi-Volatile Organics
phenol
bis(2-chloroethyl)ether
2-chlorophenol
RESULT
5570
290
101
90.4
3440
157
117
9140
129
1880
197
138
151
2660
79.7
635
106
48.3
152.2
4.17
101
96.5
U
U
2100
DNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
1.5
0.06
0.1
0.1
0.61
0.3
0.1
0.3
1.5
0.06
0.1
0.2
0.61
24.5
0.2
0.61
0.2
1
2.0
0.0088
1.6
2.6
330
330
330
ANALYZED
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
10/23/95
11/06/95
11/01/95
10/25/95
11/02/95
11/09/95
10/25/95
10/25/95
10/25/95
BY
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
CRS
CRS
JMA
JKA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
108-95-2
111-44-4
95-57-8
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
7041
7060
7471
774a
7841
8270
Page ft: 2
December 11, 1995 08:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: PE SAMPLE LOT #324 / #218
TEST RESULT
LabID: 9510005-OlA
UNITS DETECTION ANALYZED BY
LIMIT
Collected: ^^
METHOD/CAS#
Semi-Volatile Organics
1,3-dichlorobenzene
1,4 -di chlorobenzene
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ethe
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
bis(2-chloroethoxy)methane
2,4-dichlorophenol
1,2,4-trichlorobenzene
naphthalene
4-chloroaniline
hexachlorobutadiene
4-chloro-3-methylphenol
2-methylnaphthalene
hexachlorocyclopentadiene
2,4,6-trichlorophenol
2,4,5-trichlorophenol
2 -chloronaphthalene
2-nitroaniline
dimethylphthalate
acenaphthy1ene
3-nitroemiline
acenaphthene
2,4-dinitrophenol
4-nitrophenol
dibenzofuran
2,6-dinitrotoluene
2,4-dinitrotoluene
diethylphthalate
4-chlorophenyl-phenylether
fluorene
4-nitroaniline
4,6-dinitro-2-methylphenol
n-nitrosodiphenylamine
4-bromophenyl-phenylether
hexachlorobenzene
pentachlorophenol
di-n-butyIphthalate
fluoranthene
pyrene
butylbenzylphthalate
benzo(a)anthracene
3,3'-dichlorobenzidine
bis(2-ethylhexyl)phthalate
u
570
4770
D
U
120 J
U
U
U
U
U
U
U
U
630
870
U
U
U
U
U
1900
4070
U
U
U
U
U
U
D
U
3930
U
3400
U
U
2100
U
U
U
U
U
6030
1000
220 J
230 J
U
5370
10300
1200
U
8370
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
330
330
330
330
330
330
330
330
330.
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
1700
330
330
1700
330
330
1700
330
330
330
330
330
330
660
330
330
330
330
1700
330
330
330
330
330
330
330
330
330
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
10/25/95
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8270
541-73-1
106-46-7
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
91-94-1
117-81-7
Page it: 3
December 11, 1995 08:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
S^|)le ID: PE SAMPLE LOT #324 / #218'
TEST RESULT
LabID: 9510005-01A§
UNITS DETECTION ANALYZED BY
LIMIT
Collected:
METHOD/CAS#
Semi-Volatile Organics
chrysene
di-n-octylphthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
indeno(1,2,3-cd)pyrene
dibenz(a,h)anthracene
benzo(g,h,i)perylene
1600
U
U
U
XJ
U
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
SW-846, 8270
330 10/25/95 JMA 218-01-9
330 10/25/95 JMA 117-84-0
330 10/25/95 JMA 205-99-2
330 10/25/95 JMA 207-08-9
330 10/25/95 JMA 50-32-8
330 10/25/95 JMA 193-39-5
330 10/25/95 JMA 53-70-3
330 10/25/95 JMA 191-24-2
Surrogate/Recovery Data For Semi-Volatil« Organics 8270S
Total Cyanide
Surrogate
2 -fluorophenol
phenol-dS
nitrobenzene-d5
2 -fluorobiphenyl
2,4,6-tribromophenol
terphenyl-dl4
158.5 ug/g
%Recovery
92.88
78.88
82.57
89.52
86.72
115.7
Recovery Limits
25 TO 121
24 TO 113
23 TO 120
30 TO 115
19 TO 122
18 TO 137
0.15 10/13/95 KEN SW-846, 9012
Volatile Organics
ll^^Bbenzene
b^Bochl orome theine
bromodichloromethane
bromofonn
bromome thane
n-butyIbenz ene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo- 3 -chloropropan
1,2-dibromoethane
dibromome thane
di chlorodifluoromethane
1,1-di chloroe theine
1,2 -di chloroe thane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropane
31
U
U
47
72
10
U
U
U
167
23
U
145
U
U
U
U
U
111
U
U
U
115
U
U
u
u
u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
SW-846,8260A
10 10/17/95 MMR 71-43-2
10 10/17/95 MMR 108-86-1
10 10/17/95 MMR 74-97-5
10 10/17/95 MMR 75-27-4
10 10/17/95 MMR 75-25-2
10 10/17/95 MMR 74-83-9
10 10/17/95 MMR 104-51-8
10 10/17/95 MMR 135-98-8
10 10/17/95 MMR 98-06-6
10 10/17/95 MMR 56-23-5
10 10/17/95 MMR 108-90-7
10 10/17/95 MMR 75-00-3
10 10/17/95 MMR 67-66-3
10 10/17/95 MMR 74-87-3
10 10/17/95 MMR 95-49-8
10 10/17/95 MMR 106-43-4
10 10/17/95 MMR 124-48-1
10 10/17/95 MMR 96-12-8
10 10/17/95 MMR 106-93-4
10 10/17/95 MMR 74-95-3
10 10/17/95 MMR 75-71-8
10 10/17/95 MMR 75-34-3
10 10/17/95 MMR 107-06-2
10 10/17/95 MMR 75-35-4
10 10/17/95 MMR 156-59-4
10 10/17/95 MMR 156-60-5
10 10/17/95 MMR 78-87-5
10 10/17/95 MMR 142-28-9
10 10/17/95 MMR 590-20-7
Page #: 4
December 11, 1995 08:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: PE SAMPLE LOT #324 / #218 LabID: 9510005-01A Collected:
TEST
Volatile Organics
1,1-dichloropropene
cis-1, 3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 - isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2 -butanone
4-methyl-2-pentanone
2 -hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
REStJLT
U
u u 64
U
115
117
U
U
U
200B
U
D
66
U
U
47
48
U
U
33
U
54
U
U
U
U
U
U
151
16
33
261
U
633049
434811
236625
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
10/17/95
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846,8260A
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4 gM
96-18-4 W
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluoromethane
1, 2 - di chl oroe theine - d4
toluene-d8
bromofluorobenzene
%Recovery
116 Q
90.0
95.1
87.6
Recovery Limits
58.4 TO 112
53.3 TO 121
85.6 TO 143
80.6 TO 130
Page it: 5
#
Data Reporting Qualifiers
U Compound was analyzed fbr but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either whien estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. l.U with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as well as the sample.
E Estimated value. Result was outside of the calibration nmge but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not applicable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits. If surrogate recoveries are out
of limits, any values reported are for indication only.
ENVIRONMENTAL LAB WORK REQUEST ^f7//^>->-
W°- THIOKOL ENVIRONMENTAL LABORATORV
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ORGANIZATION
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REPORT RESULTS TO:
HELEN WARD, MS 301
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LOCATION
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CHAIN OF CUSTODY
RELLNQL'ISHED BV
^a^Tuu^ni^
DATE
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RECEIVED BY
//7y'//£.^y
DATE
-/A/f^-^r
TIME
• /IZ^
FOR LABORATORV USE ONLV
m DATE COMPLETED DATE REPORTED SIGNATURE
December ll, 1995 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward MIS 301
Thiokol Corp, Ut 84322
A.F. WALKER
EXT 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Oty, Ut 84302-0707
Analytical Labs MIS 245
Atm: Dr. John Terry
Tele: 801-863-2384
m
Work Order # 9511022 Sample and Test Code Identification
LabID:
OIA
Sample ID:
LOC #1 SURFACE, M-622
Test Codes and Names
Lab ID:
02A
Sample ID:
LOC #1, 1 FT., M-622
LabID:
03 A
Sample ID:
LOC ta SURFACE. M-622
UbID:
04A
Sample ID:
LOC n. 1 FT., M-622
LabID:
05A
Sample ID:
use M-622
CL04
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
N03IC2
8260S
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Nitrate-N
Volatile Organics
Test Codes and Names
CL04
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
N03IC2
8260S
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Nitrate-N
Volatile Organics
Test Codes and Names
CL04
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
N05IC2
8260S
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Nitrate-N
Volatile Organics
Test Codes and Names
CL04
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
N03IC2
8260S
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Nitrate-N
Volatile Organics
Test Codes and Names
USC Soil Classification
Method
SOP 314
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 9056
SW-846,8260A
Method
SOP 314
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 9056
SW-846,8260A Method
SOP 314
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 7471
SW-846, 9056
SW-846,8260A
Method
SOP 314
SOP 420
SOP 420
SW-846. 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 7471
SW-846, 9056
SW-846.8260A
Method
ASTM D2488
Page #: lof //
Comment.*!
Report: USC RESULTS: Sample is inorganic fme graijied soil with a
strong reaction to dilute HCl. Group is (ML) a silt with a
trace of medium sand.
'^ZoMii^ rv\. \ J^^J^/^^
X Certried By
Page #:2
This is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ED: LOC. #1 SURFACE, M-622 LabID: 9511022-OlA CoUected: 11/14/95 13:00:00 •
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Nitrate-N
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodi chlorome thane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo- 3 -chloropropan
1,2-dibromoethane
dibromomethane
dichlorodifluoromethane
1,1-di chl oroe theine
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropame
u
u
u
11/28/95
U
21.7
U
U
U
30.8
U
U
U
U
u u u u u u u u u u u
u u
u u u u u u u u u u
u
u
mg/L
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
mg/L
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
1.8
0.500
0.500
0.1
0.3
1.5
0.2
0.011
1.9
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
11/16/95
11/15/95
11/15/95
11/28/95
12/06/95
12/06/95
12/06/95
12/06/95
12/05/95
11/29/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
CRS
KMS
KMS
CRS
LVD
LVD
LVD
LVD
CRS
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SOP 314
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 9056
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
Page it: 3
December 11, 1995 08:52
^Aple ID: LOC. #1 SURFACE, M-622
CERTIFICATE OF AN/!kLYSIS
RESULTS BY SAMPLE
LabID: 9511022-OlA CoUected: 11/14/95 13:00:00
TEST RESULT UNITS DETECTION AN-\LYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
1,l-dichloropropene
cis-1,3-dichloropropene
trans-l,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 - isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
J^^hl orof luorome thane
^^B 3-trichloropropane
^^, 4 - trimethylbenzene
1,3,5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl-2-pentanone
2 -hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
u
u u u
u u u u u u u u u u u u u
u u u
u u u
u u
u u u
u u u u u
u 868295
422169
135162
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
563-58-6
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluoromethane
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
%Recovery
93.8
84.8
123
108
Recovery
59.4 TO
50.6 TO
80.2 TO
82.7 TO
Limits
115
120
149
126
Page #: 4
December 11, 1995 08:52 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: LOC. #1, 1 FT., M-622 LabID: 9511022-02A CoUected: 11/14/95 13:10:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Nitrate-N
Volatile Organics
benzene
bromobenzene
bromochloromethane
bromodichloromethane
bromoform
bromome thane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3 -chloropropan
1,2-dibromoethane
dibromomethcme
dichlorodifluoromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
u
u
u
11/28/95
0.15
24.0
U
U
U
27.4
U
u u u u
u u
u u
u u u
u u u u u
u
u
u u u u u u
u u
u
u u
mg/L
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
mg/L
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
1.9
0.500
0.500
0.1
0.3
1.6
0.2
0.012
2.0
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
11/16/95
11/15/95
11/15/95
11/28/95
12/06/95
12/06/95
12/06/95
12/06/95
12/05/95
11/29/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
CRS
KMS
KMS
CRS
LVD
LVD
LVD
LVD
CRS
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SOP 314
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-a46, 9056
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
Page #: 5
December 11, 1995 08:52 CERTIFICATE OF AN/O^YSIS
RESULTS BY SAMPLE
H|ple ID: LOC. #1, 1 FT., M-622 LabID: 9511022-02A CoUected: 11/14/95 13:10:00
TEST RESULT UNITS DETECTION AN^IVLYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene- chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3- trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
J^^ 3 - trichloropropane
^^P 4 -trimethylbenzene
^^S,5 -trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl- 2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1, 4 -dichlorobenzene-d4
u
u u u u u u u u
u u u
u u
u u u
u u u u u u u u u u u u u u
u
u 1260048
574308
164088
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluoromethane
1,2-dichloroethane-d4
toluene-dS
bromofluorobenzene
%Recovery
94.0
89.2
128
115
Recovery
59.4 TO
50.6 TO
80.2 TO
82.7 TO
Limits
115
120
149
126
H Page #: 6
December 11, 1995 08:52 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: LOC. #2 SURFACE, M-622 LabID: 9511022-03A CoUected: 11/14/95 13:15:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Perchlorate
HMX
Ni troglycerlne
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Nitrate-N
Volatile Organics
benzene
bromobenzene
bromochlorometheme
bromodi chlorome thane
bromoform
bromome theme
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo- 3 -chloropropan
1,2-dibromoethane
dibromome thane
dichlorodifluoromethane
1,1-dichloroethane
1,2-dichloroethane
1,1-dichloroethene
cis-l,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1,3-dichloropropane
2,2-dichloropropane
1,1-dichloropropene
u
u
u
11/28/95
0.59
20.6
U
u
0.013
11
U
U
u u u u u u u u u u u u
u
u
u u u u u u
u u
u
u u u u u
mg/L
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
mg/L
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
2.0
0.500
0.500
0.1
0.3
1.4
0.2
0.013
1.8
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
11/16/95
11/15/95
11/15/95
11/28/95
12/06/95
12/06/95
12/06/95
12/06/95
12/05/95
11/29/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
CRS
KMS
KMS
CRS
LVD
LVD
LVD
LVD
CRS
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SOP 314
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 9056
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
Page it: 1
December 11, 1995 08:52 CERTIFICATE OF AN/^LLYSIS
RESULTS BY SAMPLE
m pie ID: LOC. #2 SURFACE, M-622 LabID: 9511022-03A CoUected: 11/14/95 13:15:00
TEST RESTJLT .UNITS DETECTION ANJ^YZED BY
LIMIT
METHOD/CAS#
Volatile Organics
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroethane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane t3 - trichloropropane
4 -trimethylbenzene
. .5-trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl- 2-pentanone
2-hexanone
fluorobenzene
chlorobenzene-d5
1,4-dichlorobenzene-d4
u
u u u u u u u
u u
u u
u u
u u u
u u u u
u u u u u u
u u u
u u
u 960973
425910
110033
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Surrogate/Recovery Data For Volatile Organics 8260S
Surrogate
dibromofluoromethane
1,2-dichloroethane-d4
toluene-d8
bromofluorobenzene
%Recovery
92.9
84.7
132
119
Recovery
59.4 TO
50.6 TO
80.2 TO
82.7 TO
Limits
115
120
149
126
•
Page ff: 8
December 11, 1995 08:52 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: LOC. #2, 1 FT., M-622 LabID: 9511022-04A CoUected: 11/14/95 13:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Nitrate-N
Volatile Organics
benzene
bromobenzene
bromochlorome thane
bromodi chlorome thane
bromoform
bromomethane
n-butylbenzene
sec-butylbenzene
tert-butylbenzene
carbon tetrachloride
chlorobenzene
chloroethane
chloroform
chloromethane
2 -chlorotoluene
4 -chlorotoluene
dibromochloromethane
1,2-dibromo-3-chloropropan
1,2-dibromoethane
dibromomethane
dichlorodifluoromethane
1,1-dichloroethcme
1,2-dichloroethcme
1,1-dichloroethene
cis-1,2-dichloroethene
trans-1,2-dichloroethene
1,2-dichloropropane
1, 3-dichloropropane
2,2-dichloropropane
1,l-dichloropropene
u
u
u
11/28/95
0.35
22.3
U
U
0.014
8.6
U
U
U
U
U
U
U
U
U
U
U
u u u u u
u u u u u u u u u
u
u
u u u
mg/L
MG/KG
MG/KG
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
mg/L
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
1.9
0.500
0.500
0.1
0.3
1.5
0.2
0.014
2.0
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
11/16/95
11/15/95
11/15/95
11/28/95
12/06/95
12/06/95
12/06/95
12/06/95
12/05/95
11/29/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
CRS
KMS
KMS
CRS
LVD
LVD
LVD
LVD
CRS
CRS
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SOP 314
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 9056
SW-846,8260A
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
96-12-8
106-93-4
74-95-3
75-71-8
75-34-3
107-06-2
75-35-4
156-59-4
156-60-5
78-87-5
142-28-9
590-20-7
563-58-6
Page it: 9 41
December 11, 1995 08:52 CERTIFICATE OF ANi^iLYSIS
RESULTS BY SAMPLE
i^ iple ID: LOC. #2, 1 FT., M-622 LabID: 9511022-04A CoUected: 11/14/95 13:20:00
TEST RESULT 'UNITS DETECTION JLNJ^LYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
cis-1,3-dichloropropene
trans-1,3-dichloropropene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
ethylbenzene
hexachlorobutadiene
isopropylbenzene
4 -isopropyltoluene
methylene chloride
naphthalene
n-propylbenzene
styrene
1,1,1,2-tetrachloroetheme
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,1,1-trichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
Jg^, 3-trichloropropane
^^B, 4 - trimethylbenzene
^^, 5 - trimethylbenzene
vinyl chloride
o-xylene
m,p-xylene
acetone
2-butanone
4-methyl- 2-pentanone
2 -hexanone
fluorobenzene
chlorobenzene-d5
1,4 -dichlorobenzene-d4
u
u u u u
u u
u
u u
u
u u u u D
u u u u u u u u u u u u u u
u
u
u 1178788
535510
144737
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
11/16/95
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846,8260A
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
95-47-6
108-38-3
67-64-1
78-93-3
108-10-1
591-78-6
INTSTDl
INTSTD2
INTSTD3
Surrogate/Recovery Data For Volatilts Organics 8260S
Surrogate
dibromofluoromethane
1,2-dichloroethane-d4
toluene-d8
bromofluorobenz ene
%Recovery
93.0
89.3
129
117
Recovery
59.4 TO
50.6 TO
80.2 TO
82.7 TO
Limits
115
120
149
126
Page #: 10
December 11, 1995 08:52 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: USC, M-622 LabID: 9511022-05A CoUected: 11/14/95 13:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Soil Classification 11/22/95 DATE
** See /Attached Memo for Soil Classification **
11/22/95 AA ASTM D2488
Page#: 11
Data Reporting Qualifiers
U Compound was analyzed for but not detecte-d. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either When estimating a concentration for
tentatively identified compounds or when the mass sp^ectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1.1J with a detection limit of 5.0)
B This flag is used when an analyte is found in the blanic as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits. If surrogate recoveries are out
of Umits, any values reported are for indication only.