DSHW-1995-002426 - 0901a06880139ffe

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TfflOKOL CORPORAT ON
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SEMI-ANNUAL RF1[ PROGRESS REPORT
1 SEPTEMBER 1994 - 1 MAELCH 1995
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SEMI-ANNUAL RFI PROGRESS REIPORT
1 SEPTEMBER 1994 - 1 MARCH 1995
1. Description and estimation of tiie percentage of tiie RCRA Facility Investigation
completed;
Thiokol Corporation initiated Phase I soil sampling for the RFI on 13 October 1993.
To date, soils at the following SWMUs have been sam]9led:
M-19A Photographic Processing Discharge, SWMU 553;
E-517-W Surface Discharge, SWMU 282;
M-576-N Surface Discharge, SWMU 271;
M-514 Surface Discharge, SWMU 618;
S-501 Surface Discharge, SWMU 266;
M-640 Surface Discharge, SWMU 381;
M-641 Surface Discharge, SWMU 264;
M-585-N Surface Discharge, SWMtF 273;
M-606 Surface Discharge, SWMU 527;
M-628 Surface Discharge, SWMU 528;
M-593 Surface Discharge, SWMU 274;
M-636-SW Surface Discharge, SWMU 367;
M-570 Surface Discharge, SWMU 285;
M-197 Surface Discharge, SWMU 483;
M-197-BP Surface Discharge, SWMU 360;
M-702 Surface Discharge, SWMU 620;
A-9 Surface Discharge, SWMU 267;
A-2 Surface Discharge, SWMU 560;
M-66 Surface Discharge, SWMU 432;
M-72 Surface Discharge, SWMU 263;
M-67 Surface Discharge, SWMUs 261 and 433;
M-14N and M-14S Surface Discharges, SWMUs 257 and 270;
M-53-BP Surface Discharge, SWMU 260;
M-53-E Surface Discharge, SWMU 259;
M-33-B and M-33-C Surface Discharges, SWMUs 258 and 413;
M-39 Surface Discharge, SWMU 425;
Combined Surface Discharge for M-8, M-9, M-10, M-52, and M-179-N,
SWMUs 268, 611, 269, 409, 472, amd 255;
M-57 Surface Discharge, SWMU 615;
M-55-W Surface Discharge, SWMU 621;
M-9 Strand Burner Exhaust Discharge, SWMU 652;
M-40 Surface Discharge, SWMU 642;
M-205 Surface Discharge, SWMU 286;
T-21-D Surface Discharge, SWMU 559;
T-6-A Surface Discharge, SWMU 287;
Old Drum Storage Area East of M-203, SWMU 203;
M-114 Surface Discharge, SWMU 426;
M-227 Hydrofluoric Acid Treatment Unit, SWP/IU 192;
M-9-NE Surface Discharge, SWMU 651;
M-186 Industrial Waste Landfill, SWMU 212;
M-136 Old Waste Oil Disposal Pit, SWMU 208;
M-187 Old Drum Storage Area, SV^HVIU 551;
T-l Photographic Processing Drainfield, SWMU 648;
A-2 Photographic Processing Drainfield, SWMU 191;*^ t
I-IO-NE Subsurface Discharge, SWIVIU 645;v-^ ^op ^- '1'( " 'M'^^^U *^^
I-IO-SE Subsurface Discharge, SV^TVIU 436;*^ *
I-IO-S Subsurface Discharge, SWMU 234^^
T-111 Subsurface Discharge, SWMU 355; v<^
T-24A Surface Discharge, SWMU 401;*^
M-2 Laundry Drainfield C, SWMU 627; ^-^
M-19A Drywell, SWMU 444; i^
M-39 Subsurface Discharge, SWMU 425;*^
T-51A Surface Dischiarge, SWMU 402;^-^
M-2 Laundry Drainfield B, SWMU 626;*^
M-19A Strand Burner Exhaust Discharge, SW1>/IU 650;>^
M-585 Strand Burner Exhaust Discharge, SWMU 649^
Historic Burning Ground NE of M-243, SWMIf 202.^and
M-2 Laundry Drainfield A, SWMU 465.^^
JM These sites represent approximately 72 percent of the S^tVMUs in Phase I of the RFI.
2. Summaries of all findings;
The raw analytical data for the reporting period is included with this report. This
data will be compared to standards considered to be protective of health and the
environment as outlined in Section 8.0 of the Data Collection Oualitv Assurance
Plan. Volume Two, Thiokol RCRA Facility Investigation Workpians.
3. Summaries of all changes made in the RCRA Facililty Investigation during the
reporting period;
There were no changes made to the approved workpians of the RFI. Three new
SWMUs have been identified during the reporting period. These new sites and their
assigned SWMU numbers are as follows:
M-40 Magnesium Grinding Area, SWMU 655;
M-305 Transporter Maintenance Floor Wash Collection Tank, SWMU 656;
M-52 Storm Drain Discharge Area, SWMU 657 ;
Notification of these newly identified SWMUs to the E>:ecutive Secretary along with
the required Solid Waste Management Unit Assessment Plan will follow under
•• separate cover.
Ii
4. Summaries of all contact with representatives of the locail community, public interest
groups or State Goyemment during the reporting period;
Correspondence regarding RFI activities has been limited to the Division of Solid
and Hazardous Waste arid the Division of Water Qiiialiity.
5. Summaries of all problons or potential problems encountered during the reporting
period;
Laboratory analysis of the residue sample collected from M-19A Strand Burner
Exhaust Discharge (SWMU 650) revealed elevated levels of chromium, lead and
several volatile organic compounds. Further testing of the residue shows the sample
fails TCLP for chromium and lead.
The exhaust discharge is generated from the testing of small propellant samples
collected during the mixing and casting processes. Tllie samples are burned in a
pressure chamber to obtain engineering property dala for the propellant. The
exhaust gases as discharged to a 10 inch vertical pipe buried to some depth into the
soil. The contamination which has occurred at this site is expected to be confined
within the diameter of the pipe and to a very shallov." depth. The verticle pipe has
a top cover with a few small holes to dissipate tliie pressure during exhaust
discharge. The only driving force for deeper contamination would be moisture
entering through these holes, which is expected to be insignificant.
The chromium and lead contamination can be attributed to the wire used to initiate
the burn. Historically, volatile organics were used in the process. It is expected
that the hazardous levels are a result of acidic conditions created within the confines
of the discharge pipe, rather than individual burns releasing hazardous waste.
6. Actions being taken to rectify problems;
Thiokol has initiated voluntary interim measures to correct the situation. Thiokol's
facility engineering group have been notified of the need to eliminate the release of
hazardous constituents from the exhaust discharge. Environmental is investigating
the extent of contamination and will pursue corrective action.
7. Changes in personnel during the reporting period;
There has been no change in coordination and prqje<:t management for the RFI
during the reporting period. However, there have been changes in personnel
assisting with the RFL The current organization chart for Thiokol's Safety,
Environmental and Support Group is attached.
8. Projected work for the next reporting period;
Sampling will continue at the remaining sites included in the RFI Workplan with
primary focus on those sites associated with the stant up of the new wastewater
vgi^ treatment plants.
9. Copies of daily reports, inspection reports, laboratoiry and monitoring data.
Copies of the daily logs and laboratory data are included with this report.
SAFETY, ENVIRONMENTAL & SUPPORT
J. D. THOMPSON
DIRECTOR
,R43Q
FIRE PREVENTION
J. H. SANDALL
FIRE CHIEF
R400
SECURITY
K. C. FREIMUTH
MANAGER
J. C. PErr/B. H. SAVAGE*
"SECRETARY
ASST FIRE CHF/FD
M. W. MAUGHAN
A. A. MEnrNG
M. T. FONNESBECK
K D. BARFUSS
a M. STOKES
PQQQ
J. C. PETT
' SECRETARY
SAFETY
J. D. THOMPSON
MANAGER (ACTING)
D. O. MARBLE
'SECRETARY
M. AKHAVAN
ENGINEER
RRE PROTECTION
PHYSICAL SECURITY
J. a MARLOW
SUPERVISOR
SECURITY POLICE
S. T. BUXTON
GUARD CAPTAIN
INDUSTRIAL SECURITY
W.C. PHILLIPS
FACIUTY SECURITY
OFFICER
* Jointly wiih Maintenance
APPROVAL
CONCURRENCE
^ce^^s^
J. C. PETT
' SECRETARY
L E. SMTH
SUPERVISOR
SAFETY ENa - UVE
C. S. STAUFFER
W.J.MICHAELS
R. H BENTLEY
Lb.MCL^AM—
SUPERVISOR
SAFETY ANALYSIS
V. E. BACKMAN
S. E. BLAU
B. a REGAN
0. W. SWANEY
D. W. QUAYLE
SUPERVKon
SAFETY ENa INERT &
SMALL PRODUCTS
D. D. CARPENTER
V20P
COMPLIANCE
J. R. WHIMPEY
SUPERVISOR
V5QQ
WATER OPERATIONS
G. L MOWER
MANAGER
S. E. HARRIS
J. K.OJA
a L SMITH
G. W. STARTZELL
L B. TANAKA
iCJ. THACKERAY
TECH EDITOR, AUDITS,
ACCOUNTING & BUDGET
R. M. NAUMANN
DATA ENTRY, UBRARY,
& CENTRAL FILES
a RAVSTEN
SUPPORT
A. F. WALKER
P. K HOTH
J. C. PETT
' SECRETARY
PLANT ENGINEERING
K.LBALL
E. S. BERNTSEN
M. L BINGHAM
a C. MAUGHAN
A. POIROT
M-705 PLANT TECHNICIANS
W. R. ACHATZ
J. R. ANDERSON
J. M CHRISTIANSEN
F. D. HOUSTON
a K. MILLER
M. J. THORNOCK
T B WYATT
DOMESTy^ W.ASTEW.A.TE.R
TREATMENT PLANT
J. A. HOLUNGSWORTH
M.S28 AP RECLAMATION
PLANT TECHNICIANS
M. D. EARL
R. L JOHNSON
D. D. WILDE
B K. WII KFS
SUMP I RUCK OPERATIONS
K. D. PRICE
Effective: 6 February 1995
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Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWIW:
SITE: A-2 Photographic Processing Drainfield
DESCRIPTION: SWMU #191; Grid Sj^ ; 5 ft.
PARAMETERS
Cadmium
Chromiiun
Silver
Lead
DATE: S-;?-?-f-r-TIME:
METHOD
6010
6010
6010
6010
/c/:-i » SAMPLER:
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W0#: 1B940 L\VR#:
SITE: A-2 Photographic Processing Drainfield
DESCRIPTION: SVVTVIU #191; Grid #^t/ ; 10 ft.
^^ irz>
PARAMETERS
Cadmium
Chromium
SUver
Lead
METHOD
6010
6010
6010
6010
DATE: ^'P'^'^Y TIME: /"yi 3i^ SAMPLER:
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Thioltol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: ^/^0 Zf
SITE: A-2 Photographic Processing DraWjeld '
DESCRIPTION: SWMU #191; Grid # 5% ; 5 ft. Cl <iJJ J.in!i.ii\\—^///
PARAMETERS
Cadmium
Chromium
SUver
Lead
METHOD
6010
6010
6010
6010
DATE: ?/<:^r/99 TTm^O?,dC SAMPLER:-^'/^^^
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' W0#: 1B940 LWR#:£'/«»<^;2 f
SITE: A-2 Photographic Processing Drainfield ^
DESCRIPTION: SWMU #191; Grid #5!:^ OO-ftr ^
PARAMETERS
Cadmium
Chromium
SUver
Lead
METHOD
6010
6010
6010
6010
/:>)-c'a.yi •S';//
D.C-
nXTE: ^/(if^/P^ TIME: <^ ?*.'^<5 SAMPLER:-''^^J C_
£L (^•f.A-^i^
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' W0#: 1B940 LWR#: l^/cC?-^
SITE: A-2 Photographic Processing Drainfield
DESCRIPTION: SUTVIU #191; Grid MC^f ; 5 ft.
PARAMETERS
Cadmium
Chromium
SUver
Lead
DATE: 9/0P/?f TIME
METHO
6010
6010
6010
6010
6?/35
D
SAMPLER:
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.Ere w ;i £7, // r»- ^/tv-. j/
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Thiokol Corporation RCRA Facility Investigation
W0#: IB940 LWR#: S^Oi^^ 9
SITE: A-2 Photographic Processing Drainfield
DESCRIPTION: SWMU #191; Grid lt<^^ OO-ftr 9f/.
PARAMETERS
Cadmium
Chromium
SUver
Lead
METHOD
6010
6010
6010
6010
DATE: 7A/V?y TIME:G?.Yo SAMPLES::
DO
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Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:^/^ ifT^ ^
SITE: A-2 Photographic Processing Drainfield
DESCRIPTION: SWMU #191; Grid #51^ > 5 ft.
PARAMETERS METHOD
£tjjz^-ii,, /^lo^^i-f 79 h
^'il-^^ ^r^v*/^ C^h'hle dr. >!.<»
Cadmium
Chromium
Silver
Lead
DATE: ?/c7/9^ TIME
6010
6010
6010
6010
OliSo SAMPLER:
DC
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/^: c> o &r\ci-^S-^
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:i^/-' <^^9
SITE: A-2 Photographic Processing Drainfield
DESCRIPTION: SWMU #191; Grid ltX,'> OO^ <^ fi-
PARAMETERS
Cadmium
Chromium
SUver
Lead
DATE: 9'/t>//yi^ TIME:
METHOD
6010
6010
6010
6010
/i/.'eO SAMPLER:
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DC
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Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/oC^<f
SITE: A-2 Photographic Processing Drainfield
DESCRIPTION: SWMU #191; Grid #9% ; 5 ft.
PARAMETERS
Cadmium
Chromium
SUver
METHOD
6010
6010
6010
Lead
-DATE: "9/07/9^
6010
Tiim-./d^iZO SAMPLER:
Ctn
PC-
-feci_l2ll
Thiokol Corporation RCRA Facility Investigation
WO«f: 1B940 VmUl: ^/c C9-<p
SITE: A-2 Photographic Processing Drainfield
DESCRIPTION: SWMU #191; Grid ff_2SL< 1" "•
PARAMETERS
Cadmium
Chromium
SUver
Lead
METHOD
6010
6010
6010
6010
DATC: ^/o^/f^ TIME:/<i-9''=^ SAMPLER:
^u\ ^ 7f XUl-
nUokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#:
SITE: A-2 Photographic Processing Drainfield
DESCRIPTION: SWMU #191; Dup., Grid #^7^ ;/<P ft.
PARAMETERS
Cadmium
Chromium
SUver
Lead
METHOD
6010
6010
6010
6010
DATE: 9/6?/99- TIME:/C>-'2'£, SAMPLER: -* ^
>^;^T^M7>:ora^^fe^;ji^ac^^gva^ .uc:xi».'Si',
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Thiokol Corporation RCRA Facility Investigation
W0#: IB940 LWR#: £-/d:> 9
SITE: A-2 Photographic Processing Drainfield
DESCRIPTION: SWMU #191; Grid #^> ; 5 ft. haU^ Stli-, CAx-^
PARAMETERS
Cadmium
Chromium
SUver
Lead
METHOD
6010
6010
6010
6010
MKT%:^/o7/Jf -mm/^.S^ SAMPLER:
OC-
<^^:.j^ '^o-s^
/a:¥V TTtiokot Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#: ^Z*? <^Z^
SITE: A-2 Photographic Processing Drainfield
DESCRIPTION: SWMU #191; Grid #44^ ; WIT ^ fi-
PARAMETERS
Cadmium
Chromium
Silver
Lead
METHOD
6010
6010
6010
6010
V»e/«.^ ^;j/->i-<:Uw
DATE; ^/^7/f. TIME: /6'H-%' SAMPLER:
/P,.L...l ^ /^ /•/
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WO#: 1B940 \.\m»:^/cC Z-'^
SITE: A-2 Photographic Processing Drainfield
DESCRIPTION: SWMU #191; Grid #^3- ; 5 ft. St/i^ C)A^ ^ S-U^fl I^.U.LK
PARAMETERS
Cadmium
Chromium
SUver
Lead
METHOD
6010
6010
6010
6010
f DATE: f/c7/ft/. TIME: //'#5 SAMPLER:
Q^.A -^ yj>-
J/lz^
Thiokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#: S^/oC^<y
SITE: A-2 Photographic Processing Drainfield
DESCRIPTION: SWMU #191; Grid # ^j.^ ; 10 ft.
PARAMETERS
S.U'^CJj^S^. /3A^/'^c
METHOD
im
Cadmium
Chromium
SUver
Lead
-DATE: ?/^7/9^ TIME:
6010
6010
6010
6010
SAMPLER:
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: S'/Oi^Zf
SITE: A-2 Photographic Processing Drainfield
DESCRIPTION: SWMU #191; Rinse Blank, Grid ttS>Z-; /d ft.
PARAMETERS
Cadmium
Chromium
SUver
Lead
DATC: '^'7'9f
METHOD
6010
6010
6010
6010
TIME: //^O SAMPLER: ^^^
,f/m/ >^//?K
6^fif.r St?Mfif<^
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Jom Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: £'/OC>l /
SITE: I-IO-NE Subsurface Discharge
DESCRIPTION: SWMU # 645; ///-Depth
PARAMETCRS
Cadmium
METHOD
6U10
/()2^
DATC: 9-/Z-f'/ TIME: /^/^ SAMPLER: /^cj
Thiokol Corporation RCRA FacUitv Investigation
W0#: 1B940 LWR#: £^/^^ I /
SITC: I-IO-NE Subsurface Discharge
DESCRIPTION: SWMU # 645; E fj-Deptb
PARAMETCRS
Cadmium
METHOD
6010
Mast
Grave I UJ/H^.
^<?/7<y i3n</
^//Z-
UtO/s'/' *:
DATC: f-/2.'f f- TIME: /OZ,\ SAMPLER: /^^
T-/D ^E SuJ/uu 4-StL
ma Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/fi^3 I
SITC: I-IO-SE Subsurface Discharge
DESCRIPTION: SWMU # 436; /fr Depth
PARAMETCRS
VolatUe Organics
METHOD
6010
Moif>i
Clcxw ^ Grou^l
^
DATC: ^-lZ-9^ ™^= J^^^ SAMPLER •."rf^
y; f.
If.—-J, Ttuotcol Corporation RCRA Facility Investigation
fC^^^\ W0#: IB940 LWR#: /^06,5/
SITE: I-IO-SE Subsurface Discharge
DESCRIPTION: SWMU # 43d; ^/^Depth
PARAMETERS
VolatUe Organics
RiETHOD
6010
DATC: f^/Z - i4 TIME: /o3 ^ SAMPLER:
Thiola>l Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: JF/OCS /
SITC: I-IO-SE Subsurface Discharge rv -_
DESCRIPTION: SWMU # 436; ^4+ Depth ^ t'-iV) ifC ^ fe:
PARAMETERS
VolatUe Organics
METHOD
6010
DATC: 7"/'2,-^4 TIME:/(3i'^ ^5
SAMPLER: /f-^U
bss-T'/O S SiOUU 73^
Thiokol Corporation RCRA Facility Investigation
WO#: 1B940 LWR*: f"/^^^/'
STTE: I-IO-S Subsurface Discharge
DESCRIPTION: SWMU # 234; Z/?^ Depth
PARAMETERS
Cadmium
Chromium
Lead
DATC: 1'/Z'9^
METHOD
6010
6010
6010
TIME: /^S~S SAMPLER: //=;
^Z h^/^M - HJ ' C/A/// /u/t^u/r/ Mf- /)f/fr;hy,/r
b<MnJ. /^> fcJ^^f/t^J r} cIt-ciA
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10
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W0#: 1B940 LWR#: ^/C^ '^^ , n J
STTE: I-IO-S S*surface Discharge r. 20 ' bit (Srad Uen Oi^^ll
DESCRIPTION: SWMU # 234; ^«^i^£fpth
(^^A^^/ C2A/ V
PARAMETCRS
Cadmium
Chromium
Lead
METHOP
6010
6010
6010
d7/M^
DATC: ^'fl-f^ TIME: //^O SAMPLER: //=^
/ipproK/ry\d^.l</
/no
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: £'/0ltf3l
SITE: I-IO-S Mbsurface
DESCRIPTION: SWMU
PARAMETCRS
Cadmium
Chromium
Lead
Discharge 2c' Vn C''*<i min. dr^U/^K /), . ',
#234; 2^/?^epth 0 C/<gU t/^jH.
METHOD
6010
6010
6010
DATC: ^'JZ-9^ TIME: ///^ SAMPLER: /^^
lUo T'fll ^lA^S*A.rLor l)l<.<JianiX SlUJlAU "^ ^^sT r
(^ZD Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £7<5^ 3/
SITE: T-111 Subsurface Discharge
DESCRIPTION: SWMU #355; /-/f-Deptb
f^Q Grairr.f
k>TfA rc4
PARAMETERS
Sulfate
pH
METHOD
300
9045
COlo^-hehi
DATC: 9~/?-'9'^ -nm: l42Zi SAMPLER: y^u^
\>f:;...; •,.r-.;^. I /' -•' '"•
11
/43r Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: EI/O^'ZJ
SITE: T-111 Subsurface Discharge
DESCRIPTION: SWMU #355; 3 /v-Depth
;^^c:<d^ ///jy
/^•iitf OAgc/g:/
PARAMETERS
Sulfate
pH
METHOD
300
9045
M 1
iJK.
"SOfNI
San.cl(zn<i c/a t
DATC: ^"/^-f^ TIME: /^ 3 5 SAMPLER: //^t-^
I^DO T'74-A "^rfccc liiisJiai r Smilr 4c>!
IS'dSl
m-
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: t/OC?Z h
SITE: T-24A ^surface Discharge
DESCRIPTION: SWMU #401;
Jischarge Pr Of DlS^./,&rc^
MOI; Su.T&J>epth J^
('^a^/cl ^ S?/;</
"7^/-s //^uJ to/i^a
PARAMETERS
Antimony
Arsenic
Chromium
Lead
Sulfate
pH
DATC:r-;2'f<?
METHOD
6010
6010
6010
6010
300
9045
to iki SurQr.c T s
raihr^dti -ha
d/Alxl^jL 1
TIME: f^CS'' SAMPLER: /Fu)
J5XU Ttuokol Corporation RCRA Facility Investigation ^
W0#: 1B940 LWR#: , .
SITE: T-24A Subsurface Discharge Pt-OT OfSCltar^
DESCRIPTION: SWMU #401; Zfj-Depth ^
Aiof^ /
3a.ncJ ^ 5/// d/ij
PARAMETERS
Antimony
Arsenic
Chromium
Lead
Sulfate
pH
METHOD
6010
6010
6010
6010
300
9045
i rd.vc /
p^/ DATC:f'/2-f<f TIME: /iVZ SAMPLER: /F^
12
I52D TTiiokol Corporation RCRA Facility Investigation
WO#: 1B940 LWR#: £^/Oi,31
SITC: T-24A absurface Discharge ^LS"' DA (Srd <Jte>\^
DESCRIPTION: SWMU #401; X>'i£tJ)epth (z>rQoc./ .^ Jw/
/62€-
PARAMETCRS
Antimony
Arsenic
Chromium
Lead
Sulfate
pH
DATC: ^'lZ-i4-
METHOD
6010
6010
6010
6010
300
9045
TIME: /'S"20 SAMPLER: '/A^
Ttuokol Corporation RCRA FacUity Investigation .
W0#: 1B940 LWR#: ^/O^S I
SITE: T-24-A Surface Discharge; 25' Dn. Grad. 2 ft.
DESCRIPTION: SWMU #401
PARAMETCRS
Antimony
Arsenic
Chromium
Lead
Sulfate
pH
DATC: Y' 72-n
METHOD
6010
6010
6010
6010
300
9045
TIME: /TZ C
/l^Oil-f
Qrau^.1 S^// a/Id
j^2zM (^
1
•
i ' {1 ^UdJL ^=-<:^^pCdu^JL/ 1/^ i^JL^i''^^-...—
^y
1
'V-'j rff---^^''^ ••/!-</;^v'..'' i ..;.:,...'-,':;
13
Cf^p.+ i^ /m . ^r' •—•—' • ' • •
^/lUM^ 0\f^t~rn^-i~ ^ ^ f "A— //;^<£ jy^lg i^pc>»i (A/feS-/^
^^^^^7 Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: E'/06'?^
SITC: M-2 Laundry Drainfield C
DESCRIPTION: SWMU #627; Grid #^0 , 5 ft
Ci/;^
:gc_i
PARAMETERS
Cadmium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
DATC: ^-3-^4 TIME:'^-^'7 SAMPLER; ^?^^
\^r^^
M
'\' ^-7
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: BIO(i 5 Z.
SITE: M-2 Laundry Drainfield C
DESCRIPTION: SWMU #627; Grid ltZD_, 5 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
s;/r
tg^^
tH<?n ^
DATC: ^"ll-^i/ TIME: ^3 J SAMPLER: Y^^H'
llip.
m
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:
SITC: M-2 Laundry Drainfield C
DESCRIPTION: SWMU #627; Grid tf^O, 10 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC: 9-/'^-'5if TIME: 9-^7 SAMPLER; 7(/H
<;;/f i^\H\
SUMZ^ LO^^ <y_^
V(^' -VLX 0^
jrH^ ^
•^a^
14
'^ Ux>\.l>vc:'!.^
^'-^7
I-
Thiokol Corporation RCRA Facility Investigation
WO#: 1B940 LWR#: ^IC)^~Z,-.
SITE: M-2 Laundry Drainfield C ,.^
DESCRIPTION: SWMU #627; Grid #^^, 10 ft
^wf ^yjt^v^cP
Cvv- *Ts^ e.
PARAMETCRS
•VelotUc Of gaaiej
CA
df Ae
DA'^: f-f^-'?^
METHOD
-8240'
•VLC)> /'
TIME: '^''H? SAMPLER :WZf
(gos"
Thiokol Corporation RCRA Facility Investigation
WO#: 1B940 LWR#: /^ j QCP'^ •
STTE: M-2 Laundry Drainfield C
DESCRIPTION: SWMU #627; Grid #^0 , 5 ft
-^
^P'f ^^
PARAMETCRS
Cadmium
Chromiimi
SUver
Lead
! pH
-[DATC: l-IVf^
METHOD
6010
6010
6010
6010
9045
tk-\-' t\,a^'^v.^ic:sx:^ /tikSL.
"SiCU-pCg^ <gL C/i/
•f2S.lcil.c^ ^ /^i.9s^
#^
"^^ ' ( .. l^-^y^^ 7<u:. U.1-^
TIME:/^-<:^r' SAMPLER: A^^V -p-•e \;-*2J^<.S /i-oC?-.
T^ /^
-o--^-y
JSwfa,/ Corporation RCRA FacUity InvMtigation
WO#:1B940 LWR#:^/0(p%^
STTE: M-2 Laundry Drainfield C ^^
DESCRIPTION: SWMU #627; Grid »±t^, 5 tt
<^..>^e ci3 .at^y^-e^
PARAMETCRS
VolatUe Organics
METHOD
8240 :3c_i^
DAK, ? : 13 -JV ™E: /t-CS" SAMPLER, "^''tf
--v.:—- -f-*r•Jf' *-'.•••?•
"*' -^^••v'rx^ ; ^-v.
i^^^f^^j^^g^jl^^^^^lgj^^^
V
It .V r
Thiokol Corporation RCRA FacUity Investijgatiop
W0#: 1B940 LWR#;^ I OG^
SITE: M-2 Laundry Drainfield C
DESCRIPTION: SWMU #627; Grid It^ , 10 ft
PARAMETERS
Cadmium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
DATC: ^-)3-^^f TIME:/D.70 SAMPLER:^^^
;%
SITC: M-2 Laundry Drainfield C ^>^^^^
DESCRIPTION: SWMU #627; Grid #^ IQ ft
PARAMETFPg ^^
METHOD
VolatUe Organics 8240
DATC: 9~('^-'fC/
™ffi/C ' /C> SAMPLER:?^-/-/
--•^
Thiokol Corporation RCRA Facility Investigation.
W0#: IB940 LWR#: i^ / O 6 $^
SITE: M-2 Laundry Drainfield C _
DESCRIPTION: SWMU #627; Grid tt^X, S ft
PARAMETERS
Cadmium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
DATC: I'-l'^"!^ TmE: CO'.PO SAMPLER
\C'/z<;
Thiokol Corporation RCRA Facility Investigation
WO#: 1B940 LWR#: :^/^-(^5 ;
SITC: M-2 Laundry Drainfield C -, ^
DESCRIPTION: SWMU #627; Grid #>ir^ 5 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC: ^~i^ ^t\ TIME: \^.2G SAMPLER:/"/^//
Swf ^w;^r~
^-a^^.g_C g^^^f
n^ ^
Thiokol Corporation RCRA FacUitv Investigation
WD#:1B940 Lwb:^/0^^i
/^ < -^^ ?U?iJ^'? Laundry Drainfield C ' <^ DESCRIPTION: SWMU #627; Grid #3^, 10 tt
PARAMETFRS
Volatile Organics
METHOD
8240
tuc-;s.f 'z..- (t~
Sol^V-8..
^
/"BL' -t
DATC: ^~i ^ ^c^ TD,„., ^j 5^, SAMPLER: ?^y¥^
Thiokol Corporation RCRA FacUitv Investieati)
W0#: 1B940 LWR#:
SITC: M-2 Laundry Drainfield C
DESCRIPTION: SWMU #627; Duplicate; Grid #$£, Depth /^^
PARAMETCRS METHOD
i^^^v*^ f <r^'-[f-
"^•^u-^ (7lr«\^
IC: -^c'
VolatUe Organics 8240
DATC: f"/^ -^^' TTME: / ^1^ O SAMPLER:"?^^ ^^
/>.. -s-k-i* : •'.
--^' ^'^'/ ^,rV>f*.;>.:'^'^ -^-V--':'-^:'^-^,^',--'";
17
/c:3c)
TTiiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#;^ot.^^
SITC: M-2 Laundry Drainfield C
DESCRIPTION: SWMU #627; Grid tt^S^, 10 ft
V«,~r-/- j-,-//-
^ *-<t
PARAMETCRS
Cadmium
Chromium
SUver
Lead
pH
DATC:-^—X'S- ^V
METHOD
6010
6010
6010
6010
9045
TIME :W^ SAMPLER yt^M
M '^
Thiokol Corporation RCRA Facility Investigation
WO#: 1B940 LWR#:
STTC: M-2 Laundry Drainfield C
DESCRIPTION: SWMU #627; DupUcate; Grid #3F. Depth MJ^
^)^f <^;(-j~
PARAMETERS
Cadmium
Chromium
SUver
Lead
METHOD
6010
6010
6010
6010
pH 9045
DATC: ^~f^ -^"'^7^TIME:^<:r ^ ^SAMPLER: 7^/'''/'f-
Js>^ Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: ^/C> (, ^
SITC: M-2 Laundry Drainfield C
DESCRIPTION: SWMU #627; Grid »2^, 5 ft
hMMs±_3d±-
PARAMETCRS
Cadmium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
DATC:^-' / ^ ~'^^ TJME:/0 ' VX SAMPLER:
18
..__ g-^
mokol CorporaUon RCRA ^-f^0^^^ ,
W0#: 1B940 LWKff.A- '^
SITC: M-2 Laundry Drainfield ^ ,
DESCRIFnON: SWMU #627; Gnd #Z-V^. 5
.,^„e MEIHOD
PARAMETCRS
8240 VolatUe Orgamcs
Ml^^ Si^^T^
DATC ^/ 5-/^ ^••/^'"^^""^"
/o:^-
Thiokol Corporation RCRA Facilitv Investigation
W0#: 1B940 LWR#: H/C^->,
SITE: M-2 Laundry Drainfield C
DESCRIPTION: SWMU #627; Grid #Z6 ,10 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
<^oKi Sd-h.
DATC: ^-75-9^ TEVIE:/(:;5Z:> SAMPLER; y^^
r-'^^
Thiokol Corporation RCRA FaciUtv Investigation
W0#: 1B940 LWR#:
SITC: M-2 Laundry Drainfield C
DESCRIPTION: SWMU #627; Grid #^ U, 10 ft
PARAMETCRS
Cadmium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
DATC: ^-n-^c^ TEVIE:^'^ SAMPLER: 7
Uci^ 4.ii+^-
i^v^^/.v- ^>t4f<Jf^ii^y'^t*-/f^.S'; ri.''^j^yi'' i-'iA ••'.^.'V .<->>^
•»g m
19
\ ri> niokol Corporation RCRA FacUity Investigation
'(-^> WO#;iB940 LWR#:^;^^^
SITE: M-2 Laundry Drainfield C
DESCRIPTION: SWMU #627; Grid f^ \s ft
PARAMETER.S
Cadmium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
^DATC: 9-/S>-^^ TIME://."^^, SAMPLER:
/^^g^rsT^ S;/T~
~ WO#: 1B940 J siTF- M-2 Laundry Drauifield L r? > c n
^^ S^li)N: S^ *627; Grid #31- ^ «
/( '^^»J^ „ METHj PARAMETERS
VolatUe Organics
METHOD
8240
ti(x?75f q.-/ f-
DATC: 1-( S-^5^ j^^..Ji:03 SAMPLER:'T(^/'^
i^^/CL
_ fi4<^»' PARAMRTFRg
< g^f! ' Cadmiimi
Chromium
SUver
Lead
pH
SITC: M-2 Lamidry Drainfield C ^'^^^^
DESCRfPTTON: SWMU #627; Grid #3^, IQ ft
METHOD
6010
6010
6010
6010
9045
,DATC:^^^^9^ nME://V^ SAMPLER:-?//f-
20
jm.
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: f^ I C)^>
SITC: M-2 Laundry Drainfield C ,_
DESCRIPTION: SWMU #627; Grid #5^, 10 ft
PARAMFTFR«; METHOD
VolatUe Organics 824o
DATE: ^^ -l-^C^ TIME:// I/^ SAMPLERfT//^
Utcrrs f- ^(-t
l^/P-^Kt. ^ O. NTOJ^,":
Ttuokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^ I6A2
SITE: M-2 Laundry Drainfield C **»*
DESCRIPTION: SWMU #627; '»|ilii Tiiiili eit^Sft-^ '^U^J^ JOAOM. tW;^
PARAMETERS
Cadmium
Chromiiun
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
JtojjU gJh»^iJk
LaW ^ OTn>^(t>v> Go.K<:>(l '^'
J>ATC: (K'-X 5 -^t| TIME: /flH© SAMPLER: AFv^ Use •VWs San^^oU igtUx^
iV Oils. (viCveA Uivn^ iVal
fCLfW ttvAA Hf^&^
7»ioA:o/ Corporation RCRA FacUitv Investigation
WO#:1B940 LWR#: "E I ^KZL » »
SITC: M-2 Laundrv Drainfield C *= * 0»»«.
DESCRIPTION: SWMU #627; fltpiii. TuMk
PARAiVlETF.RS
VolatUe Organics
METHOD
8240
•'^^ «i^A. Tcxk. fiwi.
iA4g>4 <S?W&*;1^
DATC: ?- /3 - f ^ TIME: J| ( '.ifO SAMPLER: AFW
'ci<.Ji -f-jrXi.^ [ctJf.
^^!;/> li'tfihi^^ifir^t^^^-jr'vi^'^A''''^^^^ '.^..:^f.^':l ':'-^ J v:,., ^ /»-;'v'^v ^>v;^{r^';;^]'->/.v;^>;M:; A* .'./'
3>f>r /5^ /<?^^f
/)9/l> /)'y- A1'I9/^ to ^a^nh
rSuiMu *^^4^ ^^/- /^/dK^ -r'-^ ^/)
im. Ttuokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/O^SZ
SITC: M-19ADryweU . ^
DESCRIPnON: SWMU 444; / /l^Depth
PARAMETERS
Cadmium
Chromium
SUver
Lead
Nickel
DATC: 9-/3-- 9 f
METHOD
6010
6010
6010
6010
6010
TmEx^9S<^ SAMPLER: '^^'^
7)9^0
Ttuokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^//)y ? -2
SITC: M-19A DryweU •^ ' 6? -3 ^
DESCRIPTION: SWMU 444; J fMieyth
PARAMETERS
Cadmium
Chromium
SUver
Lead
Nicliel
DATC: 9'/S''f'f
METHOD
6010
6010
6010
6010
6010
TIME: 09^^ SAMPLER: ^PU
095'S' A-h /f/-:?y l^r^Lif^lf ^oJM.U -f^ 41%
^ 1010 Thiokol CorporaUon RCRA FacUity Investigation
WO#: 1B940 LWR#; E/O^I^
SITC: M-39 Subsurface Discharge
DESCRIPTION: SWMU # 425; /hf Depth G'^'^-e-/ .^ ^(kj
c
PARAMETCRS
Antimony
Cadmium
Chromium
SUver
Lead
DATC: ^-/i-'f^
METHOD
6010
6010
6010
6010
6010
TIME: IdJO SAMPLER: /-J H
22
ipzo Thiokol Corporation RCRA FacUity Investigation
WO#:1B940 LWR#: <f70<i,3j
STVE: M-39 Subsurface Discharge
DESCRIPTION: SWMU # 425; _iQr Depth
PARAMETCRS
Antimony
Cadmiimi
Chromium
SUver
Lead
METHOD
6010
6010
6010
6010
6010
^/QjL/^l ^Og-^«^
fkjL '>khcr
^
DATC: j-/S'9^ TIME: /020 SAMPLER: /W
^>tu<^ltA. €a/lt fCi
_[n_ T^e Sumnu^ u^ie /dcn-hfi^A '//[a.f //-e
f fi^.^c L MLLUI ^^kiiJ.^ h> ^ z:^ A- Jc (T^J-A
/^ro
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: f/Op-^f>
STTC: T-SlA-fabsurface IHscharge fi. <f-f uJrsd&i^f'
DESCRIPTION: SWMU #402; S<A,/ Depth
^^S. <^v
Sm^^l ^
3aftJ
PARAMETCRS
Antimony
Lead
Sulfate
pH
METHOD
6010
6010
300
9045
DATC: f'/?-?"/ TIME: (Z5'b SAMPLER: -^
r.u
^i^:i^4.iw^^^^^^'y U^'r'^-' ^'?- ^^^r^r;^-^-: vV;''-v:^^->- •' ^'' v^ V- ^ly y;«^^v'•}r:-r
/•3/0 Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: -d:^CC? 3 ^TT /
SITE: T-SIA Obsurface DUcharge P^ o T" t) I ^ 2-
DESCRIPTION: SWMU #402; t^f- Depth ^
PARAMETERS
Antimony
Lead
Sulfate
pH
METHOD
6010
6010
300
9045
DATC:/'/?'?'/ TIME: /^/Q SAMPLER:^ ^-
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £/^ ^2 W0#: 1B940 LWR#: £:f^Q,3'S^
\'27,0 STTE: T-51A Subsurface Discharge 2^ T^M (^racC ' W^/« c^
' "^^ DESCRIPTION: SWMU #402; So.^Depth ''
PARAMETERS
Antimony
Lead
Sulfate
pH
METHOD
6010
6010
300
9045
fTuV
DATC:^-/^-^-^ TIME: iZZ^ SAMPLER: /J«-
-JM£.. UOO ^ fB9^^ lioiz-^ £/d&l<r
T-5~//f Sur/c^uL 7>JsJt(Zrc^ '^ufAU -j«bz.
V
/^A/y/iiOfC^ -(o6lO (j./ 9^ ^4
#
7^/j Si/c UJd^ OnqtAallt. ic/^n/,Tr<J a.\ S3
$iurA,^g;
24
F: <^S-' /?!/'6i . /V^^^^ ^^cxr 6n>^AJO ' /^jt^/O^ /J/)i^je.
'^0/7^y<J //oY^^^^ <^ ///^^^-yO ^fcM'A:D <^/d S.'T'^'
0'?(P/)
Ttuokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: ^/«J'^3Sr'
Sf^E:/77^tii /<'>e^-,cj /Sy^c^^e orodAJ i>
DESCRIFTION: Manufacturing Area Background; Surface
PARAMETCRS
VolatUe Organics
METHOD
8240
DATE •.^7 S^/'r f^TiME.: ^. TIME: 'y.'SO SAMPLER:
A
3d^ ('^. A'
-jr^ r
-ZF
W r/^^
^ido
/9^^
Thiokol Corporation RCRA FaciUty Investigation
\\Tr\N 1 r>n4n T WT?#- x*** //7/rr "3 *b
SHE: ^k
. ,\
Thiokol Corporation RCRA FacUity Investigation
\ijr\u. mn,in T Mn?w- ^ /^ ^ /Z ^ ^.
DESCRIPHON: Manufacturing Area Background; Surface
pH 9045
Ni, B, Zn, Tl, Mn 6010
HMX HPLC
Nitroglycerm lU'Ll-
Perchlorates IC
Cyanide 9010 f, ^"^
Sulfate ^ 300 f\ ^| ,J
DAl'tiV/J><r/',^ TTME: ^/e^(10 SAMPLER: n
•
^^* '^iti^y^'^^'M-i/'':--:^'i/f'-^^:l-^''^<'--r:-'i^'^^^^^ tt
[j '—.
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: /^/a6 3'a"
SITE:
OESCRIPTION: Manufacturing Area Background; 2 ft.
PARAMETERS
VolatUe Organics
METHOD
8240
DATE : J?/ Jie/'f ^^ TIME: c?*^/ 6 SAMPLER: "^ r
25
AK
^
inioKol L-orporation K(..KA facility Investigation
W0#: 1B940 LWR#: ^CC 3 ^
SITE:
DESCRIPTION: Manufacturing Area Background; 2 ft.
PARAMETERS METHOD
Semi-VolatUe Organics 8270
DATEJ-^'' TIME:^^'''^^ SAMPLER: ^
^
^;sirll£L
/r,iA^^^
-9?^
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: ^/^6 3 iT"
DESCRIFTION: Manufacturing Area Background; 2 ft.
PARAMETERS METHOD
pH 9045
Cd, Cr, Ag, Pb, Be, Cu, Sb, Se, As 6010
Ni, B, Zn, Tl, Mn 6010
Mercury 7470
HMX HPLC
Nitroglycerin HPLC
Perchlorates IC
Cyanide , 9010
Sulfate
DATC: IM ii/Hfl/^.,f^/C, SAMP,XR,VV
^
iimimi
26
^^Sj-"
U^
.^'—[ft^
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £^ r Oti'^^
SITE:
DESCRIPTION: Manufacturing Area Background; 5 ft.
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC; J/ S^/^^ ^(^ TIME: ^fj .> SAMPLER; .. 6^^~>^
Thiokol Corporation RCRA FacUity Invesfigation
W0#: 1B940 LWR#: &>'^C'35>
SITE:
DESCRIPTION: Manufacturing Area Background; 5 ft.
PARAMETERS
Semi-VolatUe Organics
METHOD
8270
A
DATC: ^/ -^^^^ ^V TIME: ^f^3^SAMPLER: °^ /^
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £r^ Ou ^^
DESCRIPTION: Manufacturing Area Background; 5 ft.
PARAMETCRS METHOD
pH 9045
Cd, Cr, Ag, Pb, Be, Cu, Sb, Se, As 6010
Ni, B, Zn, Tl, Mn 6010
Mercury 7470
HMX HPLC
Nitroglycerin HPLC
Perchlorates IC
Cyanide 9010
Sulfate ^ /• ^ - / J^\ ^
DATC: cP/ S^//? f' '•/YTmE:/Yj> SAMPLER:
6<^ U t^'
-^ Qf' (J^
I..,
27
1^ ^
Thiokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#: d:'^ O C i*
SITE:
DESCRIPTION: Manufacturing Area Background; 10 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC J/Sc^y^ '^^ TIME: SAMPLER:
4^
•#
Thiokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#:
SITC:
DESCRIPTION: Manufacturing Area Background; 10 ft.
PARAMETCRS
Semi-VolatUe Organics
METHOD
8270
DATC:-^> -^<f/V f^/ TIME: /(^ ^ ^ SAMPU ER: r
¥
Thiokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#:
DESCRIFnON: Manufacturing Area Background; 10 ft.
PARAMETCRS
pH
Cd, Cr, Ag, Pb, Be, Cu, Sb,
Ni, B, Zn, Tl, Mn
Mercury
HMX
Nitroglycerin
Perchlorates
Cyanide
Sulfate , , / ,^
DATC:^^-^'^'^^ -//
Se, As
TIME:
METHOD
9045
6010
6010
7470
HPLC
HPLC
IC
9010
/aC'd SAMPIXR: y
-#-
28
IW^
Ttuokol CorporaUon RCRA FaciUty Investigation
W0#: 1B940 LWR#:
SITE:
DESCRIPTION: Manufacturing Area Background; 15 ft.
PARAMETERS
VolatUe Organics
METHOD
8240 ^A7
DATE •.J/Si '//'^ ^-Z TTm.:/0'/6 SAMPLER: ^i^ 4t^
^ D
Ttuokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#:
SITE:
DESCRIPTION: Manufacturing Area Background; 15 ft.
PARAMETCRS
Semi-VoIatUe Orgamcs
METHOD
8270
J
DKTE.J?/ J / ^ / 9</ TIME: ^^Vd SAMPLER:
/^'j
.^4^
41
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#:
DESCRIPTION: Manufacturing Area Background; 15 ft.
PARAMETCRS METHOD
pH 9045
Cd, Cr, Ag, Pb, Be, Cu, Sb, Se, As 6010
Ni, B, Zn, Tl, Mn 6010
Mercury 7470
HMX HPLC
Nitroglycerin HPLC
Perchlorates IC
Cyanide 9010
Sulfate ^ ^ / 300 ' \ /^
DATC:^/ ^r'>=V f/TTm.:/^</'0 SAMPLER: A^
^.< V
LUJR. EM36'
v (i I*' i •'<.:.->,
2^ ^> ^^
Cotni Vi •^5' Kyiu^X /vxn^v^ /Jp^e^i -^^ -Z-Oi^^.
Ttuokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#:
SITE: M-2 Laundry Drainfield B
DESCRIPTION: SWMU #626; Grid #St) , 5 ft
PARAMETERS
Cadinium
Chromium
SUver
Lead
pH
DATE: ^-23--^ M
METHOD
6010
6010
6010
6010
9045
TIME: T:i>0 SAMPLER
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:
SITE: M-2 Laundry Drainfield B
DESCRIPTION: SWMU #626; Grid ff-SO, 5 ft
PARAMETERS
VolatUe Organics
DATC: ^i~-Z^Z-^i^
METHOD
8240
TIME :S^^> ."^ SAMPIJCR:
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#:
SITE: M-2 Laundry Drainfield B
DESCRIPTION: SWMU #626; Grid /tS(} , 10 ft
PARAMETCRS
Cadinium
Chromium
SUver
Lead
pH
DATC: ^-2-2.- '^H
METHOD
6010
6010
6010
6010
9045
TTME:/(^ 'OS SAMPILER: P^^//"
30
Thiokol Corporation RCRA FQ,.IU. »
W0#: 1B940 "^'^ Investigation
!?^„^L'>™dn'Drainfield B
DESCRIPTION: SWMU #626; Grid ^T^, ,„ ft
PARAAffiTCRS
VolatUe Organics
METHOD
8240
-^
%C3-
^^I5l±I ^-Ci^ TTME: /C: ^rSAMPLER: ?W//
Sf f.?.r"""" '^^"^ ^-^'y ^v««>g«i, W0#: 1B940 LWIW:
SITC: M-2 Laundrv Drainfield B
DESCRIPTION: SWMU #626; Grid #2^, 5 ft
PARAMETFBt:
^Ui '--/fZt^c.hz
Cadmium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
''^•^••^-7-2-q_q TIME:/r tso SAMPLER:"?^^/^"
K
Thiokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#:
SITE: M-2 Laundry Drainfield B
DESCRIPTION: SWMU #626; Grid # 2<^, 5 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
.^MJ^
DATC:^ '^'Z - ^"^ TIME: fO'- 2.C= SAMPLER:/^^^^^
Thiokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#:
SITE: M-2 Laundry Drainfield B
DESCRIPTION: SWMU #626; DupUcate; Grid |?(^ , Depth
PARAMETCRS
Cadmium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
DATC: '^''Zl-^Q. TIME: .'OW^ SAMPLER: P"^ ^
Ttuokol Corporation RCRA Facility Investigation
WO#: 1B940 LWR#:
SITC: M-2 Laundry Drainfield B
DESCRIPTION: SWMU #626; DupUcate; Grid
PARAMETCRS
VolatUe Organics
»?(r ' Depth /P/^
METHOD
8240
DATC: (7 -^^ <? <• ( TIME: jC'.f^O SAMPLER
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#:
SITE: M-2 Laundry Drainfield B
DESCRIPTION: SWMU #626; Grid If? Cs 10 ft
PARAMETERS
Cadmium
Chromium
SUver
Lead
pH
DkTE:C\'-2.~2Q<U
METHOD
6010
6010
6010
6010
9045
TIME: [0 ' ^O SAMPLER: Pl/H"
Thiokol CorporaUon RCRA FacUity Investigation
W0#: 1B940 LWR#:
SITC: M-2 Laundry Drainfield B
DESCRIPTION: SWMU #626; Grid #Z^, 10 ft
PARAMETCRS METHOD
VolatUe Organics 5240
DATC: 7~^-^^-'?Y TIME fo'^o SAMPLER:
j ' •'•• /..•'• •••''••• •• •:;^:y/'^••ry::i^:^^t:i^•/li'.^/i^^i^Q^^ i-1 .••!Vfii''fV •^.I'HrVfii.Hfc-'i
32
l(^_Sc^i±JU-m^ /jr //-2 Uu/idyu, rl^^TurJrr'/r^ ^ T -iV-r -^ .s /-^^ r^ ^ ^ :^22L ^S/
///f'jir ^^/^ J
^>rr^ T^toio/ Corporation RCRA FacUity Investigation
^-^^ W0#: 1B940 LWR#: ^/oC'.^f
SITC: M-2 Laundry Drainfield B
DESCRIPTION: SWMU #626; Grid # 7 , 5 ft
PARAMETCRS
Cadinium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
^nti/'i^l
J DATE: ^0 W/}^ ff TIME: 0-^ SAMPLER: Xj H'
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £/00'^/
SITC: M-2 Laundry Drainfield B
DESCRIPTION: SWMU #626; Grid # "7. 5 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC: 2C- ^pr f^ TIME: K"^ SAMPLER: P^/^tr
Ofi'T 10
Ttuokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: /T/^^ij^f
STTE: M-2 Laundry Drainfield B
DESCRIPTION: SWMU #626; Grid # "7, 10 ft
PARAMETCRS
Cadmium
Chromium
SUver
Lead
pH
DATC: Z<^Sff^f9 'V^ TIME:
MEIHOD
6010
6010
6010
6010
9045
'^/ 5 SAMPLER: ^"^ , Xii^
'v^;^A;;:^.^>,'?^ 'o'^:'-^-'-^ "<^ • •'> '•' .' -i..<'
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: ^/OCy^/
SITE: M-2 Laundry Drainfield B
DESCRIPTION: SWMU #626; Grid # 7_, 10 ft
PARAMETCRS
Volatile Organics
METHOD
8240
L DATC: ^J^/^^f TIME: f/5^
0?4{l\ /SJ /^ fT /
Thiokol Corporation RCRA FacUity Investigation
W0#; 1B940 acUity Investigation
LWR#: £/(PG>^7 SITE: M-2 Laundry Drainfield B
DESCRffTION: SWMU #626; Grid #/^. 5 ft
PARAMETC.RS
Cadinium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
DK'TE:Z(^<^f^fn •TTm.:09-4CP SAMPLER: <nf
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/^^/
SITE: M-2 Laundry Drainfield B '
DESCRIPTION: SWMU #626; Grid #/^, 5 ft
PARAMETERS
Volatile Organics
METHOD
8240
.DATC: Z6^<^fi^1f •TlME:Of40 SAMPLER: 6 ¥
-x
34
/Dl^f tSd/io /O /
Thiokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: ^£%54^/
SITE: M-2 Laundry Drainfield B
DESCRIPTION: SWMU #626; Grid # /^, 10 ft
PARAMETCRS
Cadmium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
DATC: tO^^U TIME: lO^ SAMPLER: Ztt
/!.lau^ LM//U.
r<!^/ryY&n9C
Thiokol CorporaUon RCRA FacUity Investigation
W0#: 1B940 LWR#: ^OCs^-/
SITC: M-2 Laundry Drainfield B '
DESCRIPTION: SWMU #626; Grid # /^ 10 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC:^S?^/^f TTSTE://>^ SAMPLER: ^"^^^^
/Z?^i /7J If < /
Ttuokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^C>^ (
SITE: M-2 Laundry Drainfield B ,
DESCRIPTION: SWMU #626; Grid # 7f , 5 ft
^tl't 1/7 JK.
PARAMETCRS
Cadmium
Chromium
SUver
Lead
METHOD
6010
6010
6010
6010
9045
/i{fA(i(V[. 0
fffijC f i/U/i:. •/
DATC: -5;^//^ff TIME:/^^<^ SAMPLER: V^/^
f\;>-.^:r.Xi'::!: ••>•/>•
jn-J (\ Ttuokol Corporation RCRA FacUity Investigation
/ ^^ W0#: 1B940 LWR#: ^fT^Jfe^/
SITC: M-2 Laundry Drainfield B _
DESCRIPTION: SWMU #626; Grid ftT , 5 ft
PARAMETERS
VolatUe Organics
METHOD
8240
DATC :^i^/^f^ •TTm.:/OlC^ SAMPLER: VV/^.
iDsr
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#; E^/^^C?4l
SITE: M-2 Laundry Drainfield B ,^«
DESCRIPTION: SWMU #626; Grid #/^, 10 ft
-, PARAMETERS
-< Cadinium
Chromium
-, SUver
Lead
- pH
METHOD
6010
6010
6010
6010
9045
DATC: 1(JP <^/)^ 94- ™IE: /£>SS SAMPLER;
Thinkol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: ^<iC^<^/
SITE: M-2 Laundry Drainfield B _^
DESCRIPTION: SWMU #626; Grid # /4', 10 ft
PARAMETERS
VolatUe Organics
METHOD
8240
^/
DK'TE:Z/> Q/7f-f^ TTME: ^^S^ SAMPLER: /jff
••• •••-•••-••-'r---itfa,aiai^^ /.' -. i-'./'.;.'iv-.a\^.>-ytr<ifv;«iV/4
36
•Zl ^pf ^4
/ITT^
SuJ/VLU ^ ^5g Mof --^ 90'' CoU
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#;
SITE: M-19A
DESCRIPTION: SWMU 650; Strand Bumer Exhaust Discharge
BhdL
PARAMETERS
VolatUe Organics
METHOD
8240 /)p.m^ ^A/nx^k-h
9ii mofsk^'
DATF, , ^7}^fir9</ TIME; ll^S SAMPLER: /dtr IVGS Vt/t-t- -M
Thiofcol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#:
SITE: M-19A .
DESCRIPTION: SWMU 650; Strand Bumer Exhaust Discharge
/ i2r2-
d{'^cU.X'H,<c m
PARA^iETERS
Cd, Cr, Pb, Ag
Mercury
HMX
Nitroglycerm
METHOD
6010
7470
HPLC
HPLC
fh p
w^
Ui^
DATE: 2 7J9^r*^/ •nrn.lt^^' SAMPI.FR:
IVO
^u>/X.O tj- /^4<^ 0
Thiokol CorporaUon RCRA FacUity Investigation
W0#: 1B940 LWR#:
SITE: M-585
DESCRIPTION: SWMU 649; Strand Bumer Exhaust Discharge
PARAMETERS
VolatUe Organics
METHOD
8240
DATE: ^ ^ 5^:/?^ ^/^ XTMEJ^^^ SAMPLER: /J bl
mmm iiiUi^^inH
37
.. „ ncvA FaciUty Investigation thiokol Corporation RCRA i^"^^
V/0#-- 1B940
NffiTHOD
p^A>ffiTERS
6010
Cd, Cr, Pb. Ag 7470
Mercury HPLC
HMX HPLC
Nitroglycerin pu//
DATF.:
^7^fff TIME: /3^-SAMPl^
'/Af
dixJ/)lL^ •
' 1
• 1 I
« 1 \
j
i
!
i
'
1
i
_.
1
II u
- il^
• II
mi]
m HHbig»< Miiiiiiifliitti^
38
.24^ S<>o/ /^^l^
1 /atf^ . 7h ym /o iiig Si 'fphi Op/yi^(^^ /J I a. ^ t^ /l/inJ^ /ro de/'.a/i^O^/L. .-^/y/zy ^f //^^<CfnA^.
/a^t f^v ^. Ff"/. 77^, /ii/M(^rdn A ho
-iru %h(j(^h ^/f m/d /i(i -^n/i//, a^c/
/s a/oj/f/}//?p
'cL
/^ S/i/^h^ hOsAvr^ /ar -/// kl/ld///76 OS (Qf'Jf ds
Cin />H-hie 1 ff-. 4r /M/rvia)&/. /h^ Je//(/cr ^^upim^r?/
SdM pJiK re^.//^
dMiif^/iMnyi A/ah le/i/iaoh ^ (/js^/Hi o rap
/^na/u^/s /JMS (I/J/ir^/yi/ii/yi /i'h^/oOo'j>pm. T/^
/(khirarkru ran a /is/ n/i ^a /ijiufd /rri^/^/fvi
(^nA •PcU/ir/ A/) -^tOAif/cdn/ (P/MLJP . T/us /s
Q^ pn>.(,/i^/y]a-^'j /nr/loA'kr ^71/ // /S ^/^/i^l^ (LtJ 2 T
Dri m/ ii/a/7 /n ^// //u Sepi/il ^nt kz/ftf
CoH^.t^^. ^^ri/JL- dd(/<i^ A/S /!(7ACu.rrenc€: /b S/a/i^.
&. Cfm A ^//^ ^/Y^^r{ //AA 'fSo/Us Jwn^
5& ho/fsrn /^./loa/fitf fh. J/^/i(/2 yfe/^X lAo
^ OULL C//Ar? ML ^ <Pc//. Scofi-
Hoplcin^d /InA VotA.^ fapjlflr /TU/'.rfi preUnf
-fo (x/fM/M /il dM/On/T //AJ Cdlji^c^mn
mcA Mrd /Jjf/L fj}A/}ti'k. 71(1 &7ACtt^i^ t
^:?:'t*:^iv'•# uVV^'...*>;^-v>v-'-'v'.-^^;' •*':.-:. <•<• ;••.••.-.'•:•
I /^/^,<> /^/(Jer^ as /7 7^//I ^/^ -/h a///>/J ^4^
/l^nCt-rf-r-^ /O /n6i/€. ////t> pAy ////a^' /?/fcJ /Jut/(^ r^ ro /noi/€. ////t> 7%/ ////ifu ///fo/ /^ur/<^^
/fi a /^f5:f£///r. /:>/ a/ /i^/:>sr/- yA/^.^/e^.
^//7f/7 /y(//).S /^/MHPJ d/- /:f/7pr^x//?7aA:/c^ /^ ^//7f/7 /X/OS /^/MHjc^r/ a-f- /7p7prar//?7a/,^u
fipfirGxjjyialrJu ^^z- y^^ ^^ '/^/mcr/.^ /jUas /)/a/^J
//J^ //i/l ^/^,p^
^^C
40
OchUr ^r /fff
/066\ Ar M-243 :Sa/M(7 ^ 202- ///t^^K ^^/m
i r^^"
/OIO Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £/04-f-C
SITC: Historic Buming Ground Northeast of M-243
DESCRIPTION: SWMU #202; Grid # 7 f, , 2 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
Sane/
1 ''iHr
DATC: /^-ZT-^^ TIME; : ro/^ SAMPLER: ^^i "JLi
Thiokol CorporaUon RCRA FacUity Investigation ^
WO#: 1B940 LWR#: El044 S
SITE: Historic Buming Ground Northeast of M-243
DESCRIPTION: SWMU #202; Grid # /^ ,2 ft
PARAMETCRS
Cd, Cr, Ag, Pb, Be
Mercury
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
DATC: /<^'^ •5"'^'?' TIME: /^/^ SAMPLER: /^^
ms- ^/)r./^ a/- 4 fi- /'du^J r<-/^.<J /b
pt'nt'/rvA it> //4. ^ ft J<^p//-
Ttuokol Corporation RCRA FaciUty Investigation •
W0#; 1B940 LWR#: ^j04^i
SITE: Historic Buming Ground Northeast of M-243
DESCRffTION: SWMU #202; Grid # //^^ ,-g-ff ft f-f-
PARAMETCRS
VolatUe Organics
METHOD
8240
^/,d ^^ricA_
•fro/n fh
r/>cK in
DATC: /0'2^'94 TIME: /^2 SAMPLER: l^^n
hole
Ml.
ii . t > »,- '^*1 *• *A- I*J t*.*
•
/02,S^ TWoto/ Corporation RCRA FacUity InvestigaUon
"~^ ' WO#: 1B940 LWR#: £'/044^
SITC: Historic Buming Ground Northeast of M-243
DESCRIPTION: SWMU #202; Grid # /6 .-g-ft ^ /y-
PARAMETCRS METHOD
Cd, Cr, Ag, Pb, Be
Mercury
HMX
Nitroglycerin
6010
7470
HPLC
HPLC
DATC.: Z^" 2 r-7^ TTME:/^-?^ SAMPLER: '-^^
/QS^O \ Thiokol Corporation RCRA FacUity Investigation
j W0#: 1B940 LWR#: £-/044\^
; SITE: Historic Buming Ground Northeast of M543
DESCRIPTION: SWMU #202; Grid # 3^ 2 ft
^f// a/! (A
Jt
PARAMETCRS
VolatUe Organics
METHOD
8240
^/mJl <^riZ(/cl
DATE: lO-Zf-f^ TIME: lOTd CA»™,™. 3/^ SAMPLER:
Ttuokol CorporaUon RCRA FacUity Investigation
W0#: 1B940 LWR#: £70ef^ ^
SITE: Historic Buming Ground Northeast of M-243
DESCRIPTION: SWMU #202; Grid # 3o_, 2 ft
PARAMETKR.S
Cd, Cr, Ag, Pb, Be
Mercury
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
DXTE: /d-Zr-^/ TIME:/^S-^ SAMPLER: '^IA^
42
l/)^9:> Thiokol Corporation RCRA FacUity Investigation
-^-^ ^^ W0#: 1B940 LWR#: ^/044-^
SITC: Historic Bur- Ug Ground Northeast of M-243
DESCRIPTION: SWMU #202; Grid # 3o , 5 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC: /^I'f-94 TIME: /^"^S SAMPLER: ^/ ^OM
^ilf aU
^m// ara^^f f
/f^/rt f
Thiokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#: t/Op^^
SITC: Historic Burning Ground Northeast of M-243
DESCRnmON: SWMU #202; Grid # 3i> , 5 ft
PARAMETCRS
Cd, Cr, Ag, Pb, Be
Mercury
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
DATC: ^-r5^// TIME: /^-^3 SAMPLER: ^^
IH/] \ Thiokol CorporaUon RCRA FacUity InvestigaUon
' ' W0#: 1B940 \ymt:£7^44-S
SITE: Historic Buming Ground Northeast of M-243
DESCRIPTION: SWMU #202; Grid # 5~^ , 2 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
^ilf ond
sn^0.ll (fraec/
DATC:/^'^r-^'7^ TIME: /^^^ SAMPLER: \^H
Thiokol CorporaUon RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/O^^
SITE: Historic Buming Ground Northeast of M-243
DESCRIPTION: SWMU #202; Dup.; Grid # ^7, 2. ft.
PARAMETCRS
VolatUe Organics
METHOD
8240
DATE j6-zr-9</ TIME: ifzo SAMPLER: P97, .yft
f
h ^i^_^
l'•;•^:l^*•'-•^v^•?
i/HL Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/)44^
SITC: Historic Buming Ground Northeast of M-243
DESCRIPTION: SWMU #202; Grid # _£2. 2 ft
^'
PARAMETERS
Cd, Cr, Ag, Pb, Be
Mercury
HMX
Nitroglycerin
DATC: ^6'Zr'9f
METHOD
6010
7470
HPLC
HPLC
TIME: //Zc> SAMPLER: '^* Jff
11^/ Ttuokol CorporaUon RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/d^l
SITC: Historic Buming Ground Northeast of M-243
DESCRIPTION: SWMU #202; Grid # j£2., 5 ft
PARAMETCRS METHOD
VolatUe Organics 8240
DATC: /O'Zr-ff TIME: 7^3/ SAMPI.FR-'^^/t^
Ttuokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £r704^^S^
SITC: Historic Buming Ground Northeast of M-243
DESCRIPTION: SWMU #202; Dup.; Grid # f7^ , fT" ft-
^jJ/- ///lA
:md/f f^^^^f
PARAMETERS
Cd, Cr, Ag, Pb, Be
Mercury
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
4t
n\TV.: /O'Z^-94^ TIME: //J/ .SAMPLER:
Thiokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: S/O'f^.i
STTC: Historic Buming Ground Northeast of M-243
DESCRIPTION: SV^TVIU #202; Grid # ^f , 5 tt
PARAMETCRS
Cd, Cr, Ag, Pb, Be
Mercury
HMX
Nitroglycerin
DATE: lO-ZC-if
''%»•
METHOD
6010
7470
HPLC
HPLC
U(U/
TIME: ro3/ SAMPLER: ^/r
44
IW \ J^m^ Ma/lj/. JL- lA/^C jnl^^ prjnr /n
^mpl^ ^f a/'^'74. ^ 7 /^
I l<rY) Thiokol Corporation RCRA FacUity Investigation
/''^^ I W0#: 1B940 LWR#: ^//>^^y
i SITC: Historic Buming Ground Northeast of M-243
DESCRIPTION: SWMU #202; Grid # Yf^ , 2 ft //pii- ^rdo/ri
PARAMETCRS
VolatUe Organics
METHOD
8240
i$,/t gjfi//
DATE: /^- ^S'-ff riSa, 7/S-^O SAMPLER: /^
Ttuokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £:/0<^'^
SITE: Historic Buming Ground Northeast of M-243
DESCRIPTION: SWMU #202; Grid # 7f-, 2 ft
PARAMETCRS
Cd, Cr, Ag, Pb, Be
Mercury
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
DATE; iC'zr-i^ TIME ,. //So SAMPI. ,ER: Xjif
JK^
X
Ttuokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: /:7l)^^
SITE: Historic Buming Ground Northeast of M-243
DESCRIPTION: SWMU #202; Grid # 74- , 5 ft
PARAMETCRS METHOD
VolatUe Organics 8240 5/yi&// O'/s.rcf
/^
DATE: /^^ZS^~^4^ TIME: //J^ SAMPLE ER: ^rf
I fS'c^ Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £^/C'/4S
SITC: Historic Burning Ground Northeast of M-243
DESCRIPTION: SWMU #202; Grid # 7<C . 5 ft
PARAMETERS
Cd, Cr, Ag, Pb, Be
Mercury
HMX
Nitroglycerin
DATC: /^'Z^'f"/
METHOD
6010
7470
HPLC
HPLC
TIME; //rs, SAMPLER '^; M
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Be
Mercury
HMX
Nitroglycerin
DATP /drz<r-^i TIMF-
6010
7470
HPLC
HPLC
/ZfO SAMPl.RR-^'^Z Mff-
45
IZ (0 Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £/0^i
SITE: Historic Biu-ning Ground Northeast of M-243
DESCRIPTION: SWMU #202; Rinse Blank; Grid # 7^
46
I3L.
Act ^1. /9i4
J A.{d-:7L, /Aca,l '^ ^/p/r /f'c'c?j7 doo I '/-41'
77^^ ^t yfp A ^cpi hui/\ flus %p<p7}i
131i Ttuokol Corporation RCRA Facility Investigation
WO#: 1B940 LWR*: ^/CC-7^^'
SITC: M-2 Laundry Drainfield A ^ .
DESCRIPTION: SWMU #465; Grid # .'•>^'', 5 ft
PARAMETCRS METHOD
(zyt':zcc I &,-/
(Jr..-1 %;r
Cadmium
Chromium
SUver
Lead
pH
DATC: 3/ '-''- T'-zy'
6010
6010
6010
6010
9045
TIME: /7'2i' SAMPLER: ' ^ T
Ttuokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: C/^.c- TO
SITE: M-2 Laundry Drainfield A
DESCRIPTION: SWMU #465; Grid # "T '-', 5 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC: -7/ O-^^T "7^ TIME: /.^ZC SAMPLER: A//7^
Thiokol Corporation RCRA FacUity Investigation
-O^i- W0#: 1B940 LWR#: t:lL'lr7L'
SITE: M-2 Laundry Drainfield A _^
DESCRIPTION: SWMU #465; Grid n_£j_, 10 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
-.^
^T±t (1/.
}kdl^ t
-DATC :3/0C-7V'/ TJ^\E:/3^C'• SAMPLER:
^ yjrf
:*-'^'i
»;-?-,, {• Thiokol Corporation RCRA FacUity Investigation
i^^^ \ W0#: IB940 LWR#: C/.y -,..
SITC: M-2 Laundry Drainfield A i-"• I'' < <-'
DESCRIPTION: SWMU #465; Grid #_J2., 10 ft
-j PARAMETERS
—! Cadmium
: Chromium
- SUver
Lead
- pH
METHOD
6010
6010
6010
6010
9045
DATC: 5/ <?^,' </V' TIME:/J 3C' SAMPLER:
/of ^ Thiokol CorporaUon RCRA FaciUty Investigation
W0#; 1B940 LWR#:
SITE: M-2 Laundry Drainfield A
DESCRIPTION: SWMU #465; Grid #J>^, 5 ft
PARAMETERS
VolatUe Organics
METHOD
8240
DKTE:71 c^, 'T \ '^- TIME: /5VJ SAMPLER: /'J/t
Thiokol Corporation RCRA Facility Investigation
WO#: 1B940 LWR#: £"/^'c'7t'
SITE: M-2 Laundry Drainfield A
DESCRIPTION: SWMU #465; Grid It ^4. , 5 ft
PARAMETCRS
Cadmium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
DATC : 'MCC'^'-'^ TIME: ^"^^\ SAMPLER:
48
Mo Thiokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#: S/C x^/C
SITE: M-2 Laundry Drainfield A ^
DESCRIPTION: SWMU #465; Grid # 54,10 ft
PARAMETCRS
Cadmium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
5/// L7. 'y , /;
/y/V//; Ar7.Jr\
/>-(- r>x,i''yA
11 Oi \
DATC: '^lOCi ^/<^ TIME: /^OO SAMPLER: /Jrt
Ttiiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: CzlOt /O
SITE: M-2 Laundry Drainfield A
DESCRIPTION: SWMU #465; Grid # ^S^, 10 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC: '-^l Oc f V "f TIME: /VcJ-SAMPLER
J±IA
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: dv/Vv 0
SITE: M-2 Laundrv Drainfield A
DESCRHTTON: SWMU #465; Grid If??, 5 ft
I
PARAMETERS
Cadmium
Chromium
SUver
Lead
pH
DATC: Sl il r •^/ </ TIME:
METHOD
6010
6010
6010
6010
9045
/4-/0 <; A MPT F-R. /Id
Thiokol Corporation RCRA FaciUty Investigation
WO#: 1B940 LWR#: /z/C(i-'70
SITE: M-2 Laundry Drainfield A ., ^
DESCRIPTION: SWMU #465; Grid # <-..-, 5 ft
AidMt-LAL..
\NKI duel -^'
PARAMETCRS METHOD
VolatUe Organics 8240
DATE: ff TIME: 14/0 SAMPLER: '^'X/i/
-HP
im. Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: Z/Oi:>70
SITC: M-2 Laundry Drainfield A ^ ,,
DESCRIPTION: S\VMU #465; DupUcate; Grid It ^L., DepUi _2.
PARAMETCRS
Cadmium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
DATC: 'll OC > ^i9 TIME: 19/0 SAMPLER: ''^/jtt
U^-.
JlE
#-
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: LZ/OvVC'
SITE: M-2 Laundry Drainfield A
DESCRIPTION: S\VMU #465; Grid »'Z2, 10 ft
PARAMETCRS
Cadmium
Chromium
SUver
Lead
pH
DATC: 7il 0>:..r',il
METHOD
6010
6010
6010
6010
9045 ;.- -^
TIME: J SAMPLER: /-^ li
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/Oic'.'O
SITC: M-2 Laundry Drainfield A
DESCRIPTION: si\TVIU #465; Grid # 72^ ^° ^^
PARAMETCRS
VolatUe Orgamcs
METHOD
8240
DATC: >/^< r^V TIME: /^A SAMPLER:
50
ML2U Ttuokol CorporaUon RCRA Facility Investigation
W0#: 1B940 LWR#: E/'OC'JC
SITE: M-2 Laundry Drainfield A
DESCRIPTION: SWMU #465; Grid # / ) , 5 ft
PARAMETERS
Cadmium
Chromium
SUver
Uad
pH
DATC: "31 Cu rvf TIME:
METHOD
6010
6010
6010
6010
9045
l/fl \ SAMPLER
Unf/ ^cr.il
: ^/f
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: c/C:^ 7^
SITE: M-2 Laundry Drainfield A ^.
DESCRIPTION: SWMU #465; Grid If / I , S ft
PARAMETCRS
VolatUe Organics
METHOD
8240
7^0lid (.'(/(/
r.h'U'^/ I f
DATC: lie f TIME:/V.>^> SAMPLER: ^7jif.
/»'i /
Ttuokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/£.'c ^'C
SITE: M-2 Laundry Drainfield A
DESCRIPTION: SWMU #465; Grid #// , 10 ft
PARAMETCRS
Cadinium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
DATC: r/ C^:.7 v/ TIME: - 4-S / SAMPLER;
Tu
Ttuokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: c^/O i^ 70
SITE: M-2 Laundry Drainfield A ,^
DESCRIPTION: SWMU #465; Grid # / / . 10 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
DK'TE:Z/ 0( T 7 9 TIME: -V f/ SAMPLER;
fL^/ •, /jlf-
/ijoryt CiC7^
nil: HM// -I
(jiitiihkj 0f~
^^7/:7aii ^]ni7< }
/-•-.' -.. '. •
51
jA C f Thiokol Corporation RCRA FacUity Investigation
''^ ' W0#: 1B940 LWR#: ^^C (^.y(j
SITE: M-2 Laundry Drainfield A
DESCRIPTION: SWMU #465; DupUcate; Grid #/"5?, Depth /Q
PARAMETERS METHOD
Volatile Organics 8240
DATC: ^1 OC f9'/ TIME: f9Sl F'^/ju,
' SAMPLER: /J IT
I c >.." Thiokol Corporation RCRA FacUitv Investigation
' ^i' ( WO#: 1B940 LWR#: c^/0C7C'
SITE: M-2 Laundry Drainfield A -
DESCRIPTION: SWMU #465; Grid #_/_, 5 ft
Jt
PARAMETERS
Cadinium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
DATC: tiOCf'-;^ TIME: Ai^Z SAMPLER: ^AJH
c!/ini .'Jli/
.Sl ^ JUL
JIL i—^ <uJ
( n'\Ct^ / J
Ttuokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: c'/Ci'7C'
SITE: M-2 Laundry Drainfield A
DESCRIPTION: SWMU #465; Grid # ( , 5 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC: Zi Cs'C^/'<{
t- t
TIME: SAMPLER: Zirf
#
iim]
52
••-;» '•.; .-.-J- ,'• ,r.: T ^..•'.t./*^
/V/? Thiokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#: ^"/i' ( , 7c ,
SITE: M-2 Laundry Drainfield A ^
DESCRIPTION: SWMU #465; Grid # ) , 10 ft
PARAMETCRS
Cadmium
Chromium
SUver
Lead
pH
METHOD
6010
6010
6010
6010
9045
DATC: J>ICCi'^/<9 TIME: / 5^/7 SAMPLER:
Ttuokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: (z/cCC/C
STTE: M-2 Laundry Drainfield A
DESCRIPTION: SWMU #465; Grid # ^ , 10 ft
F'.Cj JJA
PARAMETERS
VolatUe Organics
METHOD
8240
DATC: 7/ uu r 7 y' TIME: / J •' 7 SAMPLER: /j H
-U-:iJ_^
SiuiJ-
il u .(iVi^^' ^^-v.
ENVIRONMENTAL LAB WORK REQUEST
^7^.7- /
THIOKOL ENVIRONMENTAL LABORATORY LWR No. E10607
Aj./^. UJAL//^/1_ ^59o
CXISTCSMTEI)
\74OO
WORK ORDGR
IB94C7 2I7U/^ f<f
OROAMZATION
ei^ii/izo eiJGiz. 301 £
REPORT RESIX.TS TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE
^rlJ^IS , ISff
DATE
/-zi-n
TYPE
^
LOCATION
^ -/BG ^/^D. IMm L /57^
TIME TEST
f^/il2/i /U<:/<i fs - ^/c>
REMARKS
/Ty - 7^7/7
7-2/-f^ ly' is-iC^ /OC.-&-zfC7 Sr^fi 1/(04 - BzrO
i-5iOMtJU2lt. •7-Zl-f4 u' ISno i/oc - 3Z40 -SWy7"?i^ ^^^^^^
y O^iToA/ T2/f/se-
7-Z/-fe • ' 13 oc^ i/e><^'<Bz<i/c> 'pntn:^^
#
CHAIN OF CUSTODY
RELINQUISHED BV
7 'O^yA
DATE
t'Z/-f9
TIME
/h/<7
RECEIVEDBV
(PZ
DATE
n l^^h^
TIME
JlolC
7-2.t-9f g^ A za^ /* ^'^z22-l!L T^M T
FOR LABORATORY USE ONLY
PATE roMPunvD DATC REPORTED
/UiKu UUop/Hi?n-h
ENVIRONMENTAL LAB WORK REQUEST
e/o/.o-2^ TO, THIOKOL ENVIRONMENTAL LABORATORY ZLUJ^ iio. e/o/ro
nu>M>
A/^ IVALKCi^
ION
6^90 [A^AO /B940 Z/Ju/u f<7
OKGANUAHON
7^1^/RA eA/&/^ 3o/e
BBTOar BBSUL1B TOl
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCAnON HME TEST SZMASXS
\.^oj7ni/^zrZ 7'Zi-<ff ^ 7i/i-iei> /A/p^ofc. /SIS' /oc- SZ40 Sr/nl iCiiA -8Z70
l^b- £>£>/£> ^c-6 '>fO 2- 5uj/r> u Tt 212..
7-2i'H I/' RJOZA ^-cy^is CJ,Cr,/)sj&^
/4^- 74-7 o
3.,SuJ/Hi/<^ 2/2.
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Qr.U iL9. /Oft t^ l^^r /?C/^/l /<£M/h. -(>0/^
•^
1/ 1^)0 IZcj^A 7Ut^/cil\ -6>c>/o 4^ - 7^70
c?,:AS.9i isf^ y m i^oc-ei^ <tr/H) I/O A S270
^ (4iO TIC^A M<^-la/<. -^/O ^^-7470
*-5i«M.U^'ZlZ. I/' 1440 Uoc- 8240 S^/fd-l/oA -ez7A
«• SuJ/Htl-t* -z 11-\7 1^01 ZC/g/? AO/a h " 6>^/0 A/^-7470
v^SiAMttO-U-ZiU I/' r^oi l/0C'BZ4O ^i/u'-yo* ' S270
/'
^^•5U)/KO*t.2iJi. i/ 1Si7^ T^CZA Mt^/et/i - ^oro A/J-7470
ii.SiVAU'^^12..
($r,i^i:s. ISA. {/ l^/Z-"i/OC- <Bz^O Str^i VoA' ^Z70
CHAIN OF CUSTODY
BEUNQinSHQ) BY DATE TIME SECEn'ESBY DATE TIME
dJuJadU^ r-zz-f'/ /^/s-(LJZ u
y^y^/^y^^
''I'^ihi l(ol^
l-ll-f^ 8vr ^ZZz^t^=f!^...^£<±
FOR LABORATORY USE ONLY
nunooMimBD D41B BUMJimU
September 1, 1994
•
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward
MIS 301
A.F. WALKER, MIS 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs MIS 245
Atm: Dr. John Terry
Tele: 801-863-2384
Work Order # 9407021 Sample and Test Code Identification
Lab ID:
OIA
Sample ID:
M-186, GRID 8, 5 FT.
Test Codes and Names
Lab ID:
02A
Sample ID:
M-186, GRID 8, 10 FT.
•
Lab ID:
03A
Sample ID:
M-186, GRID 8, 15 FT.
Lab ID:
04A
Sample ID:
M-186, GRID 13, 5 FT.
Lab ID:
05A
Sample ID:
M-186, GRID 13, 10 FT.
BA AE2
CD AE2
CR AE2
PB AE2
AS GF2
HO CV2
SE GF2
824dS
8270S
Barium
Cadmium
Chromium
Lead
Arsenic
Mercuiy
Selenium
Volatile Organics
Semi-Volatile Orsanics
Test Codes and Names
BA AE2
CD AE2
CR AE2
PB AE2
AS GF2
HG CV2
SE'aF2
8240S
8270S
Barium
Cadmium
Chromium
Lead
Arsenic
Mercuiy
Selenium
Volatile Organics
Semi-Volatile Organics
Test Codes and Names
BA AE2
CD AE2
CR AE2
PB AE2
AS QF2
HG CV2
SE GEZ
824&S
8270S
Barium
Cadmium
Chromium
Lead
Arsenic
Mercuiy
Selenium
Volatile Organics
Semi-Volatile Organics
Test Codes and Names
BA AE2
CD AE2
CR AE2
PB AE2
AS OF2
HG CV2
SE GF2
8240s
8270S
Barium
Cadmium
Chromium
Lead
Arsenic
Mercuiy
Selenium
Volatile Organics
Semi-Volatile Organics
Test Codes and Names
BA_AE2 Barium
CD_AE2 Cadmium
CR_AE2 Chromium
PB_AE2 Lead
AS_GF2 Arsemc
HG_CV2 Mercuiy
SE 0F2 Selenium
8240S VolatUe Organics
8270S Semi-Volatile Organics
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
SW-846, 8270 Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
SW-846, 8270
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
SW-846, 8270
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
SW-846, 8270
Method
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
7060
7471
7740
8240
8270
Page #:1 of ^i?'
Work Order i(< 9407021 Sample and Test Code Identmcation
Lab ID:
06A
Sample ID:
M-186, GRID 13, 15 FT.
Test Codes and Names
Lab ID:
"OTA
Sample ID:
M-186, GRID 13, 15 FT. DUP
Lab ID:
OSA
Lab ID:
09A
Sample ID:
M-186, DECON RINSE
Sample ID:
M-186, DECON RINSE
BA AE2
CD AE2
CR AE2
PB"AE2
AS~GF2
HG'CV2
SE GF2
8240S
8270S
Barium
Cadmium
Chromium
Lead
Arsenic
Mercuiy
Selenium
Volatile Organics
Semi-Volatile Oi;ganics
Test Codes and Names
BA AE2
CD"AE2
CR AE2
PB~AE2
AS~aF2
HG~CV2
SE GF2
824flS
8270S
Barium
Cadmium
Chromium
Lead
Arsenic
Mercuiy
Selenium
VolatUe Organics
Semi-Volatile Oiganics
Test Codes and Names
8240 Volatile Oiganics
Test Codes and Names
8240 Volatile Organics
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
SW-846, 8270 Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
SW-846, 8270
Method
SW-846, 8240
Method
SW-846, 8240
Workorder Comments
A ^2::^;^
Certir^4^
Page #2
•
This is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: M-186, GRID 8, 5 FT, Lab ID: 9407021-01A Collected: 07/21/94 13:15:00
TEST
Barium
Cadmium
Chromium
Lead
Arsenic
Mercury
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
J^jnmoform
iH|Tiome thane
^IBKutcuione
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroe thouie
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trcins -1,2 -Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
RESULT
105
U
18.0
16.9
7.9
U
1.2
3.5 J
U
D
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
D
D
D
5.6 BJ
U
U
U
D
U
6.5 BJ
U
DNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.07
0.1
0.3
1.7
0.096
0.031
0.077
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANJ^YZED
08/16/94
08/16/94
08/16/94
08/16/94
08/17/94
08/16/94
08/18/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
BY
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01
10061-02
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
6010
6010
6010
6010
7060
7471
7740
8240
-5
-6
• Page #: 3
September 1, 1994 08:03
Sample ID: M-186, GRID 8, 5 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9407021-OlA Collected: 07/21/94 13:15:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
D
D
D
D
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Siirrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
Semi-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4 -Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroetheme
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroemiline
Hexachlorobutadiene
4 -Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2 -Chloronaphthalene
2-Nitroaniline
D imethyIphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
U
u u
u u u u
u D
D
U
U
D
U
D
U
U
U
D
U
D
U
u D
U
U
U
D
U
U
U
D
U
D
U
U
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240S
%RecovBry
99.6
97.3
96.8
50
330
330
190
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
SW-846, 8240
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
Page#: 4
September 1, 1994 08:03 CERTIFICATE OF A>[>^JLYSIS
' RESULTS BY SAMPLE
Sample ID: M-186, GRID 8, 5 FT. Lab ID: 9407021-OlA Collected: 07/21/94 13:15:00
TEST
Semi-Volatile Organics
4-Nitrophenol
Dibenz ofuran
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitrociniline
4,6-Dinitro-2-methyIphenol
n-Nitrosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Pheneuithrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
bis(2-Ethylhexyl)phthalate
Chrysene
ilj^kn - octylphthalate
I^P^o [b&k] fluoranthene
Benzo [a] pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h]anthracene
Benzo[g,h,i]perylene
RESULT
1990
U
U
U
U
U
U
U
U
U
U
U
U
U
U
D
D
U
U
U
U
B
U
D
U
U
U
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Phenol .-d5
Nitrobenzene -d5
2 -Fluorobiphenyl
2,4,6-
Terphe
Tribromophenol
!nyl-dl4
DETECTION
LIMIT
79
99
63
190
63
140
63
120
790
63
63
63
120
180
63
83
73
63
83
260
83
83
83
160
83
120
83
140
ANJLLYZED
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/:J0/94
07/:$0/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/;t0/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270S
%Recovery
39.89
40.99
37.90
44.53
48.41
85.35
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
Sample ID: M-186, GRID 8, 10 FT. Lab ID: 9407021-02A Collected: 07/21/94 13:45:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Barium
Cadmium
156
U
ug/g
ug/g
0.06 08/16/94 LVD SW-846, 6010
0.1 08/16/94 LVD SW-846, 6010
Page #: 5
September 1, 1994 08:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-186, GRID 8, 10 FT. Lab ID: 9407021-02A Collected: 07/21/94 13:45:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Chromium
Lead
Arsenic
Mercury
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorome thcine
Broiroform
Bromomethane
2-Butcinone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2 -Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trems-l,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
9.0
6.8
9.3
U
1.4
3.5 J
U
U
D
U
D
D
U
D
U
U
D
U
U
D
U
U
O
U
O
D
D
D
D
D
U
D
D
D
U
D
D
D
U
4 BJ
D
D
D
D
U
U
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.3
1.6
0.097
0.027
0.077
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
08/16/94
08/16/94
08/17/94
08/16/94
08/18/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-5
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-c
67-66-;
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01
10061-02
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-0F-4
75-01 i
95-47-6
6010
6010
7060
7471
"740
8240
-5
-6
Page #: 6
September 1, 1994 08:03
Sample ID: M-186, GRID 8, 10 FT.
CERTIFICATE OF ANAI.YSIS
RESULTS BY SAMPLE
Lab ID: 9407021-02A CoUected: 07/21/94 13:45:00
TEST RESULT UNITS DETECTION ANJLLYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Surrogate/Recovery Data For Volatile Organics 8240S
SW-846, 8240
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
Semi-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2 -Methylphenol
bis(2-Chloroisopropyl)ethe
4 -Methylphenol
n-Nitroso-di-n-propylamine
JijKrachloroethane
fl^B robenzene
ll^phorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)methcme
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chlorocmiline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
U
U
U
D
U
U
U
U
D
D
U
U
U
U
U
D
U
U
U
U
U
U
D
U
U
U
U
U
U
U
U
U
D
U
U
U
D
U
D
D
D
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
99.4
97.6
94.2
50
330
330
190
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
79
99
63
190
63
140
Recovery Limits
81
74
70
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/:50/94
07/:J0/94
07/:J0/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
• Page #: 7
September 1, 1994 08:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-186, GRID 8, 10 FT. Lab ID: 9407021-02A Collected: 07/21/94 13:45:00
TEST
Semi-Volatile Organics
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
n-Ni trosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoremthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
bis(2-Ethylhexyl)phthalate
Chrysene
Di-n-octylphthalate
Benzo[b&k]fluoremthene
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h]anthracene
Benzo[g,h,i]perylene
RESULT
U
u D
U
U
U
D
U
U
D
U
D
U
U
1250 B
D
U
u
u U
D
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Phenol -d5
Nitrobenzene-d5
2 -Fluorobiphenyl
2,4,6-
Terphe
Tribromophenol
nyl-dl4
DETECTION
LIMIT
63
120
790
63
63
63
120
180
63
83
73
63
83
260
83
83
83
160
83
120
83
140
ANALYZED
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270S ^^
%Recovery
39.04
40.23
35.20
42.66
46.79
82.49
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
Sample ID: M-186, GRID 8, 15 FT. Lab ID: 9407021-03A CoUected: 07/21/94 14:10:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Barium
Cadmium
Chromium
Lead
Arsenic
124
0.6
12.3
9.0
10.5
ug/g
ug/g
ug/g
ug/g
ug/g
0.06
0.1
0.3
1.6
0.084
08/16/94
08/16/94
08/16/94
08/16/94
08/17/94
LVD
LVD
LVD
LVD
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
7060
Page #: 8
September 1, 1994 08:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-186, GRID 8, 15 FT. Lab ID: 9407021-03A CoUected: 07/21/94 14:10:00
TEST RESULT
Mercury
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
3^2 -Dichloroethane
•^P Di chloroethene
^IWexanone
trans-1,2-Dichloroethene
1,2-Dichloropropame
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Te t rachl oroe thene
Toluene
1,1,1-Trichloroethane 8.6
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
Surrogati
Surrogate
Toluene-d8
0.1
1.1
u u u
u D
U
U
U
U
D
U
U
U
U
u D
U
U
U
U
D
D
U
U
u D
U
D
U
D
D
U
U
U
BJ
U
U
U
U
D
U
UNITS
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT ,
0.019
0.067
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
AN^IIiYZED
08/16/94
08/18/94
07/26/94
07/26/94
07/26/94
07/26/94
07/:26/94
07/:>6/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
e/Recovery Data For Volatile Organic
Bromofluorobenzene
%Recovery
100
98.1
BY
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
B 8240S
METHOD/CAS#
SW-846, 7471
SW-846, 7740
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
TO 117
TO 121
Page #: 9
September 1, 1994 08:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-186, GRID 8, 15 FT. Lab ID: 9407021-03A CoUected: 07/21/94 14:10:00
TEST
Volatile Organics
RESULT UNITS
1,2-Dichloroetheme-d4
Semi-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1, 2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroethane
Nit:robenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2 -Chloronaphthalene
2-Nitroaniline
D ime thyIphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4 -Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
n-Ni trosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
D
D
U
U
D
U
D
U
U
U
U
U
u D
U
U
D
U
U
U
U
a u u u u u n D
u u
u D
u D
u D
D
D
n u u D
D
U
D
D
D
D
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
94.9
50
330
330
190
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
79
99
63
190
63
140
63
120
790
63
63
63
ANALYZED
70
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
BY
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8240
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
•
Page #: 10
September 1, 1994 08:03 CERTIFICATE OF A>[ALYSIS
• RESULTS BY SAMPLE
Sample ID: M-186, GRID 8, 15 FT. Lab ID: 9407021-03A CoUected: 07/21/94 14:10:00
TEST
Semi-Volatile Organics
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoremthene
Pyrene
Butylbenzylphthalate
Benzo[a] emthracene
bis(2-Ethylhexyl)phthalate
Chrysene
Di-n-octylphthalate
Benzo[b&k]fluoranthene
Benzo[a]pyrene
Indeno[1,2,3 -cd]pyrene
Dibenz[a,h]anthracene
Benzo[g,h,i]perylene
RESULT
2600
U
U
U
D
U
U
U
U
B
U
U
U
D
D
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
11^^ Phenol .-d5
I^B Nitrobenzene
"i^ 2 - Fluorobiph(
2,4,6-
Terphe
-d5
enyl
Tribromophenol
!nyl-dl4
DETECTION
LIMIT
120
180
63
83
73
63
83
260
83
83
83
160
83
120
83
140
ANJLLYZKD
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For Scunl-Volatile Organics 8270S
%Recovery
46.49
44.54
37.83
41.81
41.55
67.90
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
Sample ID: M-186, GRID 13, 5 FT. Lab ID: 9407021-04A CoUected: 07/21/94 14:40:00
TEST RESni.T UNITS DETECTION AN.nj.YZED BY
LIMIT
METHOD/CAS#
Barium
Cadmium
Chromium
Lead
Arsenic
Mercury
Selenium
96.2
D
16.0
18.9
9.5
U
0.9
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
0.06
0.1
0.3
1.5
0.092
0.018
0.074
08/16/94
08/16/94
08/16/94
08/16/94
08/17/94
08/16/94
08/18/94
LVD
LVD
LVD
LVD
CRS
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
7060
7471
7740
Page#: 11
September 1, 1994 08:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-186, GRID 13, 5 FT. Lab ID: 9407021-04A CoUected: 07/21/94 14:40:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorometheme
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chlorofonn
Chloromethane
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans-l,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
5.9
U
U
tJ
U
O
U
U
U
U
D
U
U
a D
u
u u XJ
XJ
D
U
u D
U
D
U
U
D
D
D
D
U
D
U
BJ
D
U
U
D
D
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-
Semi-Volatile Organics
Phenol
•Dichloroethane-d4
U ug/Kg
%Recovery
98.1
99.4
95.8
50
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5 ^^
10061-01-5 ^^
10061-02-6 ^^
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
07/30/94
TO 117
TO 121
TO 121
MMR
SW-846, 8270
108-95-2
Page #: 12
September 1, 1994 08:03
Sample ID: M-186, GRID 13, 5 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9407021-04A CoUected: 07/21/94 14:40:00
TEST
Semi-Volatile Organics
Pyridine
Aniline
bis (2-Chloroethyl)ether
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroetheme
Nitrobenzene
Isophorone
2-Nitrophenol
2,4 -Dimethylphenol
Benzoic Acid
bis (2-Chloroethoxy)metheme
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naohthalene
IBihloroani 1 ine
I^F-achlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroemiline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methyIphenol
n - Nitrosodiphenyleimine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenemthrene
Anthracene
Di-n-butylphthalate
RESULT
u u
u
u u u u u u D
u D
D
U
D
D
U
D
D
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
U
U
U
D
D
D
D
D
U
U
U
U
U
U
U
U
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
190
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
79
99
63
190
63
140
63
120
790
63
63
63
120
180
63
83
ANJJiYZED
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
• Page #: 13
September 1, 1994 08:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-186, GRID 13, 5 FT. Lab ID: 9407021-04A CoUected: 07/21/94 14:40:00
TEST RESULT
Semi-Volatile Organics
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
U
D
D
U
bis(2-Ethylhexyl)phthalate 3530 B
Chrysene
Di-n-octyIphthalate n D
Benzo [b&k] fluoremthene V
Benzo [a] pyrene u Indeno[1,2,3-cd]pyrene D
Dibenz[a,h] emthracene
Benzo[g,h,i]perylene u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 - Fluorcjphenol
Phenol-d5
Nitrobenzene-d5
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
DETECTION
LIMIT
73
63
83
260
83
83
83
160
83
120
83
140
ANALYZED
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 827OS
%Recovery
43
43
38
42
46
78
.30
.49
.24
.50
.88
.93
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137 ^^^
Sample ID: M-186, GRID 13, 10 FT. Lab ID: 9407021-05A CoUected: 07/21/94 15:01:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Barium
Cadmium
Chromium
Lead
Arsenic
Mercury
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
146
D
9.1
8.4
11.1
U
1.2
6.1 J
D
D
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
0.07
0.1
0.3
1.6
0.099
0.020
0.079
10
10
10
08/16/94
08/16/94
08/16/94
08/16/94
08/17/94
08/16/94
08/18/94
07/26/94
07/26/94
07/26/94
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
6010
6010
6010
6010
7060
7471
7740
8240
Page #: 14
September 1, 1994 08:03
Sample ID: M-186, GRID 13, 10 FT.
CERTIFICATE OF AN^LLYSIS
RESULTS BY SAMPLE
Lab ID: 9407021-05A CoUected: 07/21/94 15:01:00
TEST
Volatile Organics
Benzene
Bromodi chlorometheme
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-l,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
JH^^-Dichlorobenzene
wV-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2-Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
8.0
Surrogate
Surrogate
Toluene-d8
U
U
U
U
U
U
U
U
U
u
u
u u u
u u
u
u D
u u u D
U
u
u D
U
U
U
U
BJ
D
U
U
u u u
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANJUJYZED
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
i/Recovery Data For Volatile Organics 8240S
Bromofluorobenzene
1,2-
Seml-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
D i chloroetheme-d4
D
D
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
98.7
98.6
95.6
50
330
330
190
METH0D/CAS#
SW-846, 8240
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
07/30/94
07/30/94
07/30/94
07/30/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
Page #: 15
September 1, 1994 08:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-186, GRID 13,10 FT. Lab ID: 9407021-05A CoUected: 07/21/94 15:01:00
TEST
Semi-Volatile Organics
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroetheme
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4 -Trichlorotjenzene
Naphthalene
4-Chloroemiline
Hexachlorobutadiene
4 -Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyc1opentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2 -Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
Acenaphthylene
3 - Ni troemi 1 ine
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroemiline
4,6-Dinitro-2-methyIphenol
n-Ni trosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
RESULT
U
U
u u u u
u u D
U
D
D
D
D
D
D
D
O
U
U
U
D
U
D
U
U
U
U
U
U
D
D
D
U
D
D
U
U
U
U
U
D
D
U
D
U
U
D
D
U
D
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
79
99
63
190
63
140
63
120
790
63
63
63
120
180
63
83
73
63
83
ANALYZED
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
BY
MMR
MMR
MMR
MMR
MHR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MHR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MHR
MMR
MMR
METHOD/CAS#
SW-846, 8270
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
•
Page #: 16
September 1, 1994 08:03 CERTIFICATE OF ANfALYSIS
RESULTS BY SAMPLE
Sample ID: M-186, GRID 13, 10 FT. Lab ID: 9407021-05A CoUected: 07/21/94 15:01:00
TEST RESULT
Semi-Volatile Organics
Benzo[a] emthracene U
bis(2-Ethylhexyl)phthalate 1730 B
Chrysene U
Di-n-octylphthalate U
Benzo[b&k]fluoremthene U
Benzo[a]pyrene U
Indeno[1,2,3-cd]pyrene U
Dibenz[a,h]anthracene U
Benzo[g,h,i]perylene U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Phenol-d5
Nitrobenzene-dS
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
DETECTION
LIMIT
260
83
83
83
160
83
120
83
140
ANJLLYZED
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270S
%Recovery
37.02
36.68
31.19
35.92
45.53
73.41
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
m liaple ID: M-186, GRID 13, 15 FT. Lab ID: 9407021-06A CoUected: 07/21/94 15:12:00
TEST RESULT UNITS DETECTION A](7i)I.YZED BY
LIMIT
METHOD/CAS#
Barium
Cadmium
Chromium
Lead
Arsenic
Mercury
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorometheme
Bromoform
•
127
U
13.4
12.0
15.6
D
1.3
U
U
U
U
D
U
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.06
0.1
0.3
1.5
0.091
0.016
0.073
10
10
10
10
10
10
08/16/94
08/16/94
08/16/94
08/16/94
08/17/94
08/16/94
08/18/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/:J6/94
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
6010
6010
6010
6010
7060
7471
7740
8240
Page #: 17
September 1, 1994 08:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-186, GRID 13, 15 FT. Lab ID: 9407021-06A CoUected: 07/21/94 15:12:00
TEST
Volatile Organics
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2 -Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
tremB-1, 3-Dichlorcspropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
D
D
U
U
U
D
D
U
D
U
U
U
D
D
U
U
U
U
D
U
D
U
U
U
D
U
U
U
13 B
U
D
D
D
U
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4 ^^
75-09-2 ^^
108-10-1 ^^
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Surrogate/Recovery Data For Volatile Organics 824OS
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
Semi-Volatile Organics
Phenol
Pyridine
Aniline
bis{2-Chloroethyl)ether
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
U
U
U
U
D
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
98.5
101
96.5
50
330
330
190
110
63
150
Recovery Limits
81
74
70
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
Page#: 18
September 1, 1994 08:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-186, GRID 13, 15 FT. Lab ID: 9407021-06A CoUected: 07/21/94 15:12:00
TEST RESULT UNITS DETECTION AMiliYZED BY
LIMIT
METHOD/CAS#
Semi-Volatile Organics
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis{2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)metheme
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroemiline
Hexachlorobutadiene
4 -Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadi ene
2^, 6-Trichlorophenol
Jl^k 5-Trichlorophenol
^l^^iloronaphthalene
2 - Ni troemi 1 ine
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4 -Ni troani1ine
4,6-Dinitro-2-methylphenol
n-Nitrosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
bis(2-Ethylhexyl)phthalate
Chrysene
u
u
u u
u
u u
u u D
u u D
U
U
U
u u D
U
U
U
D
U
U
D
U
U
U
U
U
u
u u
u u u
u u D
U
U
D
U
U
U
U
u u u 2360 B
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1.4 00
79
99
63
190
63
140
63
120
790
63
63
63
120
180
63
83
73
63
83
260
83
83
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/20/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MHR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
• Page #: 19
September 1, 1994 08:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-186, GRID 13, 15 FT. Lab ID: 9407021-06A CoUected: 07/21/94 15:12:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Semi-Volatile Organics
Di-n-octylphthalate
Benzo[b&k]fluoremthene
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h] emthracene
Benzo[g,h,i]perylene
1
u ! U
D
i U
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Phenol-d5
Ni trobenzene-d5
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
83
160
83
120
83
140
SW-846, 8270
07/30/94 MMR 117-84-0
07/30/94 MMR 205-99-2/2
07/30/94 MMR 50-32-8
07/30/94 MMR 193-39-5
07/30/94 MMR 53-70-3
07/30/94 MHR 191-24-2
For Semi-Volatile Organics 8270S
%Recovery
45.66
43.97
37.87
43.75
48.66
74.56
Recovery Limits
25 TO 121
24 TO 113
23 TO 120
30 TO 115
19 TO 122
18 TO 137
Sample ID: M-186, GRID 13, 15 FT. DUP Lab ID: 9407021-07A CoUected: 07/21/94 15:16:00
TEST
Barium
Cadmium
Chromium
Lead
Arsenic
Mercury
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
RESULT
119
0.6
13.1
10.2
9.7
U
1.3
D
U
U
U
D
D
U
U
U
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.07
0.1
0.3
1.6
0.095
0.018
0.076
10
10
10
10
10
10
10
10
10
ANAT.YZED
08/16/94
08/16/94
08/16/94
08/16/94
08/17/94
08/16/94
08/18/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
BY
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
HETHOD/CAS# %
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
6010
6010
6010
6010
7060
7471
7740
8240
i
Page #: 20
September 1, 1994 08:03 CERTIFICATE OF A>f^JLYSIS
RESULTS BY SAMPLE
Sample ID: M-186, GRID 13, 15 FT. DUP Lab ID: 9407021-07A CoUected: 07/21/94 15:16:00
TEST
Volatile Organics
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chl orome thane
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans -1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
^1^, 2,2 -Tetrachloroe theme
v^^ra chl oroe thene
Imuene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Tri chlorof1uorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
6.4
Surrogate
Surrogate
Toluene-d8
U
n U
U
U
u D
U
U
D
U
U
U
U
D
U
U
U
U
U
U
U
U
U
u BJ
U
u
u
u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANiLLYZED
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
07/26/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
:/Recovery Data For Volatile Organics 8240S
Bromofluorobenzene
1,2-
Semi-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
•Dichloroethane-d4
U
U
D
U
U
D
U
U
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
99.3
100
95.1
50
330
330
190
110
63
150
150
63
76
METHOD/CAS#
SW-846, 8240
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
TO 117
TO 121
TO 121
MMR
MMR
HHR
MMR
MMR
MHR
HHR
MMR
MHR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
Page #: 21
September 1, 1994 08:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-186, GRID 13, 15 FT. DUP Lab ID: 9407021-07A CoUected: 07/21/94 15:16:00
TEST
Semi-Volatile Organics
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)metheme
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadi ene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2 -Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofurem
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4 -Chlorophenyl-phenylether
Fluorene
4-Nitroemiline
4,6-Dinitro-2-methylphenol
n-Ni trosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenemthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
bis(2-Ethylhexyl)phthalate
Chrysene
Di-n-octylphthalate
Benzo[b&k]fluoremthene
Benzo[a]pyrene
RESULT
U
u u D
D
U
D
U
U
U
U
U
U
U
U
D
D
U
U
U
U
U
U
D
U
D
U
U
U
U
U
U
U
O
U
u u u
u u
u u 547
U
U
D
U
1620 B
U
D
U
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
79
99
63
190
63
140
63
120
790
63
63
63
120
180
63
83
73
63
83
260
83
83
83
160
83
ANALYZED
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
07/30/94
BY
MMR
MMR
MHR
MMR
MMR
MHR
MHR
MHR
MMR
MMR
MHR
MMR
MHR
MMR
MMR
MHR
MMR
MMR
MMR
MMR
MMR
MMR
MHR
MMR
MMR
MMR
MMR
MMF.
MMR
MMR
MMR
MMR
MMR
MMR
MHR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MHR
MHR
HHR
MMR
MHR
MHR
METHOD/CAS#
SW-846, 8270
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3 ^^
208-96-8 ^^
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
Page #: 22
September 1, 1994 08:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-186, GRID 13, 15 FT. DUP Lab ID: 9407021-07A CoUected: 07/21/94 15:16:00
TEST RESULT UNITS DETECTION AJCTJIIiYZED BY
LIMIT
METHOD/CAS#
Semi-Volatile Organics
Indeno[1,2,3-cd]pyrene
Dibenz[a,h]anthracene
Benzo[g,h,i]perylene
tJ ug/Kg
U ug/Kg
D ug/Kg
120 07/30/94 MMR
83 07/30/94 MHR
140 07/30/94 MHR
SW-846, 8270
193-39-5
53-70-3
191-24-2
Surrogate/Recovery Data For Semi-Volatile Organics 8270S
Surrogate %Recovery
2-Fluorophenol 44.49
Phenol-d5 44.05
Ni t robenz ene-d5 37.38
2 -Fluorobiphenyl 41.24
2,4,6-Tribromophenol 50.30
Terphenyl-dl4 74.96
Recovery Limits
25 TO 121
24 TO 113
23 TO 120
30 TO 115
19 TO 122
18 TO 137
Sample ID: M-186, DECON RINSE Lab ID: 9407021-08A CoUected: 07/21/94 13:00:00
TEST
^l^ratile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromoform
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
D ibromochloromethane
1,1-Dichloroethane
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
RESULT
6.7
D
D
U
U
U
u u u u u D
U
U
U
U
u u u D
U
u
u D
U
D
U
U
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
Page #: 23
September 1, 1994 08:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-186, DECON RINSE Lab ID: 9407021-08A CoUected: 07/21/94 13:00:00
TEST - RESULT
Volatile Organics
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Tri chloroethene
Trichlorofluoromethane
Vinyl Acetate
vinyl Chloride
o-Xylene
D
D
U
U
U
U
U
U
D
U
U
U
U
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
Surrogate/Recovery Data For Volatile Organic
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
%Rocovery
97.9
104
103
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
8 8240
METHOD/CAS#
SW-846, 8240
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
Sample ID: M-186, DECON RINSE Lab ID: 9407021-09A CoUected: 07/21/94 13:00:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorometheme
Bromoform
Bromometheme
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheme
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexemone
trems-1,2-Dichloroethene
RESULT
11.0
u u u D
U
U
U
U
U
u D
U
D
D
U
U
U
U
U
n
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAfl#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
Page #: 24
September 1, 1994 08:03 CERTIFICATE OF AN^JLYSIS
RESULTS BY SAMPLE
Sample ID: M-186, DECON RINSE Lab ID: 9407021-09A CoUected: 07/21/94 13:00:00
TEST
Volatile Organics
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Te t rachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
A
RESULT
-
U
U
U
U
D
U
U
U
U
D
U
U
U
U
U
D
U
U
U
U
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANi^YZED
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
^^ Surrogate
Toluene-d8
Bromofluorobenzene
1,2--Dichloroethane-d4
%Recovery
99.4
103
100
METHOD/CAS#
SW-846, 8240
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
• Page #: 25
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identifted compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. l.U with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ENVIRONIVIENTAL LAB WORK REQUEST
^^A 7 A ?- 7
P™ TinoKOL ENVIRO^fME^^^AL LABORATORY
FIIOM:
A. F. l4//^/Jie^
ORGANIZATION
E/7U/iec) eA/(^^
EXTENSION
S^39c^
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36 It:
LWR No. E10608
COSTCBflBR
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WORK ORDER
/B9^
DATE
7-z<-'r9^
REPORT RESlULTli TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE
7'?i--7i
TYPE
1^
LOCATIQN
M'/ff(:> ^^i7>imi
TIME
037
TEST
/<pd - 0-Z4O
REMARKS
// 7-2{>7^ // BS7 ^^/ UhA - e7/A>
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CHAIN OF CUSTODY
RELINQUISHKU BY
i^yy.^/i^
DATE
^-^L'f/
TIME
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//////^^^
DATE
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TIME
/(/^
FOR LABORATORY USE ONLY
<
DATE COMPLETED DATE REPORIB) SIGNATURE
ENVIRONMENTAL LAB WORK REQUEST
^A^A7/>>y
"" TmOKOL ENVIRONMENTAL LABORATORY
IBOMi
/I. A^ UJ//c/Cd/^^
OBGANIZA-nON
ECTDaiON
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HELEN WARD, MS 301
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LOCATION
M'/86 ^o/l'i
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CHAIN OF CUSTODY
. SFIJNQUISHESBY
^^L^/Jz/JL
DATE
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TIME
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DATE
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//t//7 1
• 1
FOR LABORATORY USE ONLY
lunOQMFLEIBD D41BREF0mD noNAitiu 1
September 1, 1994 CERTIFICATE OF ANAJLYSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
Ihiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs MIS 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Orderly 9407027 Sample and Test Code Identification
Lab ID:
OIA
Sample ID:
M186, GD.15, 5FT.,
Test Codes and Names
GRAB
Lab ID:
02A
Sample ID:
M186, GD.15, 10 FT., GRAB
Lab ID:
03A
Sample ID:
M186, GD.15, 15 FT., GRAB
Lab ID:
04A
Sample ID:
M186, GD.23, 5 FT., GRAB
Lab ID:
05A
Sample ID:
M186, GD.23, 10 FT., GRAB
•
BA AE2
CD AE2
CR AE2
PB AE2
AS GF2
HG CV2
SE OF2
82%S
8270S
Barium
Cadmium
Chromium
Lead
Arsenic
Mercury
Selenium
Volatile Organics
Semi-Volatile Orsanics
Test Codes and Names
BA AE2
CD AE2
CR AE2
PB AE2
AS OF2
HG CV2
SE GF2
824dS
8270S
Barium
Cadmium
Chromium
Lead
Arsenic
Mercury
Selenium
Volatile Organics
Semi-Volatile Organics
Test Codes and Names
BA AE2
CD AE2
CR AE2
PB AE2
AS GF2
HG CV2
SE GF2 8240S
8270S
Barium
Cadmium
Chromium
Lead
Arsenic
Mercury
Selenium Volatile Organics
Semi-Volatile Organics
Test Codes and Names
BA AE2
CD AE2
CR AE2
PB AE2
AS GF2
HG CV2
SE GF2
824dS
8270S
Barium
Cadmium
Chromium
Lead
Arsenic
Mereury
Selenium
Volatile Organics
Semi-Volatile Organics
Test Codes and Names
BA_AE2 Barium
CD_AE2 Cadmium
CR_AE2 Chromium
PB_AE2 Lead
AS_GF2 Arsenic
HG_CV2 Mercury
SE GF2 Selenium
8240S Volatile Organics
8270S Semi-Volatile Organics
Page #: lof X^
Method
SW-846, 6010
SW-846, 6010
SW-846,
SW-846,
SW-846,
SW-846,
SW-846, 7740
SW-846, 8240
SW-846, 8270
Method
,6010
,6010
,7060
,7471
6010
6010
6010
6010
7060
7471
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846
SW-846, 7740
SW-846, 8240
SW-846, 8270
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
SW-846, 8270
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
SW-846, 8270
Method
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
7060
7471
7740
8240
8270
Work Order # 9407027 Sample and Test Code Identification
Lab ID:
06A
Sample ID: W Test Codes and Names
M186, GD.23, 15 FT., GRAB
Lab ID:
07A
Lab ID:
08A
Sample ID:
M186, DI WATER, GRAB
Sample ID:
Ml86, DECON WATER, GRAB
BA AE2
CD AE2
CR AE2
PB AE2
AS GF2
HG CV2
SE GF2
8240S
8270S
Barium
Cadmium
Chromium
Lead
Arsenic
Mereury
Selenium
Volatile Organics
Semi-Volatile Organics
Test Codes and Names
8270 Semi-Volatile Orgamcs
Test Codes and Names
8270 Semi-Volatile Oiganics
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
SW-846, 8270
Method
SW-846, 8270
Method
SW-846, 8270
Workorder Cnminents
'^,J^-y^z^
Certified B
Page #2
This is to certify that the following samples were analyzed using good laboratory practices
to show the following resuUs.
Sample ID: M186, GD.15, 5 FT., GRAB Lab ID: 9407027-OlA CoUected: 07/26/94 08:37:00
TEST
Barlijm
Cadmliim
Chromium
Lead
Arsenic
Mercury
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
j||K)moform
m^ nome thane
^ll^^utanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2 -Chloroethylvinyl ether
Chloroform
Chlorome thcine
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2 -Dichloropropeuie
cis-1,3-Dichloropropene
treuis-1, 3 -Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroethane
Te t rachloroe thene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetheme
RESULT
124
U
18.8
15.9
6.4
U
1.1
U
D
D
D
D
U
U
U
U
U
D
U
U
U
U
D
U
U
U
U
u
u
u
u
u
u
u
u
u
u
D
u n u 3.5 BJ
u
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.06
0.1
0.3
1.5
0.099
0.010
0.080
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANJU^YZED
08/16/94
08/16/94
08/16/94
08/16/94
08/17/94
08/16/94
08/18/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
BY
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JKPL
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
• Page #: 3
September 1, 1994 07:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M186, GD.15, 5 FT., GRAB Lab ID: 9407027-OlA CoUected: 07/26/94 08:37:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
U
U
U
D
D
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
Semi-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
D
U
D
D
D
U
U
U
U
U
U
U
D
O
D
D
U
U
D
U
D
U
U
U
D
D
D
D
D
D
U
U
U
D
U
C
D
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240S
%Recovery
100
92.0
100
50
330
330
190
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
SW-846, 8240
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR .
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
Page #: 4
September 1, 1994 07:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M186, GD.15, 5 FT., GRAB Lab ID: 9407027-OlA CoUected: 07/26/94 08:37:00
TEST
Semi-Volatile Organics
4-Nitrophenol
Dibenzofurem
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
n-Nitrosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenz ene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
ButyIbenzyIphthalate
Benzo[a] emthracene
bis (2-Ethylhexyl)phthalate
Chrysene
i %
^n - octylphthalate
^zo [b&k] fluoranthene
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h]anthracene
Benzo[g,h,i]perylene
RESULT
U
u u u
u
u D
D
D
D
D
D
U
D
D
D
D
D
D
D
D
D
D
D
D
D
D
n
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Pheno] .-d5
Nitrobenzene-d5
2 -Fluorobiphenyl
2,4,6-
Terphe
Tribromophenol
!nyl-dl4
DETECTION
LIMIT
79
99
63
190
63
140
63
120
790
63
63
63
120
180
63
83
73
63
83
260
83
83
83
160
83
120
83
14 0
ANJJiYZED
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOO/CAS#
SW-846, 8270
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For S(unl-Volatile Organics 8270S
%Recovery
52.47
55.23
54.85
57.31
65.79
86.12
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
Sample ID: M186, GD.15, 10 FT., GRAB Lab ID: 9407027-02A CoUected: 07/26/94 09:01:00
TEST RESULT UNITS DETECTION ANJJiYZED BY
LIMIT
METHOD/CAS#
Barium
Cadmium
139
0.2
ug/g
ug/g
0.07 08/16/94 LVD
0.1 08/16/94 LVD
SW-846, 6010
SW-846, 6010
Page #: 5
September 1, 1994 07:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: Ml86, GD.15, 10 FT., GRAB Lab ID: 9407027-02A CoUected: 07/26/94 09:01:00
TEST
Chromium
Lead
Arsenic
Mercury
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans-l,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trams-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
11.1
11.3
8.1
U
1.6
U
U
U
D
D
D
U
D
U
U
u u u u D
u D
U
U
U
0
u
u u u u
u D
a D
u u u u 4.7 BJ
U
U
U
u
u D
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.3
1.6
0.094
0.012
0.075
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
08/16/94
08/16/94
08/17/94
08/16/94
08/18/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
BY
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01
10061-02
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
6010
6010
7060
7471
7740
8240
A' w
-5
-6
Page #: 6
September 1, 1994 07:54 CERTIFICATE OF ANALYSIS
'" RESULTS BY SAMPLE
Sample ID: M186, GD.15, 10 FT., GRAB Lab ID: 9407027-02A CoUected: 07/26/94 09:01:00
TEST RESULT
Volatile Organics
Surrogate/Rei
Surrogate
Toluene-d8
Bromofluorobenz
UNITS DETECTION
LIMIT
ANIiLYZED
covery Data For Volatile Organic
ene
1,2-Dichloroethane-d4
Semi-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Jj^achl oroe thane
fl^B.'obenzene
lIKphorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroemiline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofurem
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
U
U
U
U
U
U
U
U
D
U
U
D
U
U
U
U
D
U
U
U
U
U
D
U
U
U
U
U
U
u
D
U
U
O
U
U
D
U
U
U
U
u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
98.5
91.9
98.3
50
330
330
190
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
79
99
63
190
63
140
BY
s B240S
METHOD/CAS#
SW-846, 8240
Recovery Limits
81
74
70
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
• Page #: 7
September 1, 1994 07:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M186, GD.15, 10 FT., GRAB Lab ID: 9407027-02A CoUected: 07/26/94 09:01:00
TEST
Semi-Volatile Organics
Fluorene
4-Nitroemiline
4,6-Dinitro-2-methylphenol
n-Nitrosodipheny1amine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoremthene
Pyrene
Butylbenzylphthalate
Benzo[a] emthracene
bis(2-Ethylhexyl)phthalate
Chrysene
Di-n-octylphthalate
Benzo[b&k]fluoranthene
Benzo[a]pyrene
Indeno[1,2,3 -cd]pyrene
Dibenz[a,h] emthracene
Benzo[g,h,i]perylene
RESULT
U
u u u D
D
D
U
U
280
D
D
U
D
U
D
U
U
a u
u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Phenol -d5
Nitrobenzene-d5
2 -Fluorobiphenyl
2,4,6-
Terphe
Tribromophenol
nyl-dl4
DETECTION
LIMIT
63
120
790
63
63
63
120
180
63
83
73
63
83
260
83
83
83
160
83
120
83
140
ANALYZED
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2 ^^
For Semi-Volatile Organics 8270S ^^
%Recovery
61.75
67.53
67.88
73.55
86.73
95.35
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
Sample ID: Ml86, GD.15, 15 FT., GRAB Lab ID: 9407027-03A CoUected: 07/26/94 09:17:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Barium
Cadmium
Chromium
Lead
Arsenic
115
2.2
11.9
38.7
15.4
ug/g
ug/g
ug/g
ug/g
ug/g
0.07
0.1
0.3
1.7
0.094
08/16/94
08/16/94
08/16/94
08/16/94
08/17/94
LVD
LVD
LVD
LVD
CRS
SW-846,
SW-84e,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
7060
Page #: 8
September 1, 1994 07:54
•
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: Ml86, GD.15, 15 FT., GRAB Lab ID: 9407027-03A CoUected: 07/26/94 09:17:00
TEST RESULT
Mercury
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromoform
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
^teS-Dichloroetheme
fl^B-Dichloroethene
T^^exanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-l,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane 7.3
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
U
1.4
U
U
U
U
D
U
U
U
U
D
U
U
U
U
U
U
U
U
D
D
U
U
D
D
D
U
U
D
D
D
U
U
D
U
BJ
U
U
U
U
U
U
UNITS
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.027
0.075
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
AtTiiJiYZED
08/16/94
08/18/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/;>9/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/:>9/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
BY
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
%Recovery
99.8
103
METHOD/CAS#
SW-846, 7471
SW-846, 7740
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
TO 117
TO 121
Page #: 9
September 1, 1994 07:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M186, GD.15, 15 FT., GRAB Lab ID: 9407027-03A CoUected: 07/26/94 09:17:00
TEST
Volatile Organics
RESULT UNITS
1,2-Dichloroethane-d4
Semi-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis (2-Chloroethoxy) metheme
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4 -Chloroani1ine
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2 -Chloronaphthalene
2-Nitroemiline
D ime thyIphthalate
Acenaphthylene
3-Nitroemiline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroemiline
4,6-Dinitro-2-methyIphenol
n-Nitrosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
U
D
D
U
D
D
U
U
U
U
D
U
U
D
U
U
U
U
U
D
U
U
D
D
D
D
D
U
U
D
D
U
U
D
U
U
U
U
U
D
U
U
U
u D
U
U
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
99.7
50
330
330
190
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
79
99
63
190
63
140
63
120
790
63
63
63
ANALYZED
7C
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
BY
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MHR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8240
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0 ^^
111-91-1 ^A
120-83-2 ^m
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
Page #: 10
September 1, 1994 07:54 CERTIFICATE OF ANi^XYSIS
• RESULTS BY SAMPLE
Sample ID: Ml86, GD.15, 15 FT., GRAB Lab ID: 9407027-03A CoUected: 07/26/94 09:17:00
TEST RESULT
Semi-Volatile Organics
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoremthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
u u D
U
D
D
U
U
bi s (2 -Ethylhexyl)phthalate U
Chrysene
Di-n-octylphthalate
U
U
Benzo[b&k]fluoranthene U
Benzo[a]pyrene D
Indeno[1,2,3 -cd]pyrene D
Dibenz[a,h] emthracene
Benzo[g,h,i]perylene
I^ P
U
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2-Fluorophenol
Phenol-d5
Ni trobenzene-d5
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
DETECTION
LIMIT
120
180
63
83
73
63
83
260
83
83
83
160
83
120
83
140
ANJ^YZRD
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For Siaml-Volatile Organics 8270S
%Recovery
69
72
70
74
81
89
.52
.27
.93
.38
.78
.53
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
Sample ID: M186, GD.23, 5 FT., GRAB Lab ID: 9407027-04A CoUected: 07/26/94 10:15:00
TEST RESULT UNITS DETECTION ANJkLYZED BY
LIMIT
METHOD/CAS#
Barium
Cadmium
Chromium
Lead
Arsenic
Mercury
Selenium
117
U
15.2
11.2
6.8
U
1.3
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
0.06
0.1
0.3
1.5
0.087
0.012
0.069
08/16/94
08/16/94
08/16/94
08/16/94
08/17/94
08/16/94
08/18/94
LVD
LVD
LVD
LVD
CRS
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
7060
7471
7740
• Page#: 11
September 1, 1994 07:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M186, GD.23, 5 FT., GRAB Lab ID: 9407027-04A CoUected: 07/26/94 10:15:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromoform
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheme
1,1-Dichloroetheme
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
Tri chlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
6.9
U
U
U
U
U
U
U
u D
U
U
D
u u u u u u
u D
u D
U
u u D
U
u u D
U
U
O
U
BJ
D
D
U
D
D
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-
Semi-Volatile Organics
Phenol
Dichloroethane-d4
U ug/Kg
%Recovery
101
103
97.2
50
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5 ^^
10061-02-6 ^V
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
08/05/94
TO 117
TO 121
TO 121
MMR
SW-846, 8270
108-95-2
Page #: 12
September 1, 1994 07:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: Ml86, GD.23, 5 FT., GRAB Lab ID: 9407027-04A CoUected: 07/26/94 10:15:00
TEST
Semi-Volatile Organics
Pyridine
Aniline
bis(2-Chloroethyl)ether
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis (2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
jHfthloroani 1 ine
H^^.achlorobutadiene
4 -Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroemiline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4 -Chlorophenyl-phenylether
Fluorene
4-Nitroemiline
4,6-Dinitro-2-methylphenol
n-Nitrosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenemthrene
Anthracene
Di-n-butylphthalate
RESULT
U
u u u
u u D
U
U
U
U
u u u u u u
u u u u u u u u
u
u u
u u u u
u u
u u u D
u u u
u
u u
u D
u u u
u D
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
190
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
79
99
63
190
63
140
63
120
790
63
63
63
120
180
63
83
ACTJILLYZED
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
Page #: 13
September 1, 1994 07:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MI86, GD.23, 5 FT., GRAB Lab ID: 9407027-04A CoUected: 07/26/94 10:15:00
TEST RESULT
Semi-Volatile Organics
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
bis(2-Ethylhexyl)phthalate
Chrysene
Di-n-octylphthalate
Benzo[b&k]fluoremthene
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h]anthracene
Benzo[g,h,i]perylene
D
U
200
U
U
D
U
U
D
U
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Phenol-d5
Nitrobenzene-d5
2-Fluorobi phenyl
2,4,6-Tribromophenol
Terphenyl-dl4
DETECTION
LIMIT
73
63
83
260
83
83
83
160
83
120
83
140
ANALYZED
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270S
%Recovery
50
64
69
74
78
87
.83
.29
.71
.44
.59
.71
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137 g^^
Sample ID: Ml86, GD.23, 10 FT., GRAB Lab ID: 9407027-05A CoUected: 07/26/94 10:32:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Barium
Cadmium
Chromium
Lead
Arsenic
Mercury
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
115
0.6
14.2
14.2
5.3
D
1.1
U
U
U
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
0.06
0.1
0.3
1.5
0.098
0.024
0.078
10
10
10
08/16/94
08/16/94
08/16/94
08/16/94
08/17/94
08/16/94
08/18/94
07/29/94
07/29/94
07/29/94
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
6010
6010
6010
6010
7060
7471
7740
8240
Page #: 14
September 1, 1994 07:54 CERTIFICATE OF ANAJLYSIS
RESULTS BY SAMPLE
Sample ID: M186, GD.23, 10 FT., GRAB Lab ID: 9407027-05A CoUected: 07/26/94 10:32:00
TEST
Volatile Organics
Benzene
Bromodi chloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorome thane
1,1-Dichloroetheme
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexemone
trems-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1^2-Dichlorobenzene
^l^^-Dichlorobenzene
^l^^-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroethane
Te t rachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
Tri chlorofluorome thane
Vinyl Acetate
vinyl Chloride
o-Xylene
RESULT
5.4
U
U
U
U
U
U
U
U
U
u
u
u
D
D
U
U
U
U
U
D
U
U
U
u
u D
U
D
U
U
U
BJ
U
U
D
U
U
n
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANlJiYZRD
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/;29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
B romofluorobenzene
1,2-
Seml-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
Dichloroetheme-d4
D
u
u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
100
95.9
96.9
50
330
330
190
METHOD/CAS#
SW-846, 8240
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
08/05/94
08/05/94
08/05/94
08/05/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
Page #: 15
September 1, 1994 07:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M186, GD.23, 10 FT., GRAB Lab ID: 9407027-05A CoUected: 07/26/94 10:32:00
TEST
Semi-Volatile Organics
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroetheme .
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)metheme
2,4-Dichlorophenol
1,2,4-Trichlorobenzene Naphthalene
4-Chloroani1ine
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2 -Chloronaphthalene
2-Nitroemiline
Dimethylphthalate
Acenaphthylene
3-Nitroemiline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofurem
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
n-Ni trosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenemthrene
Anthracene
Di-n-butylphthalate
Fluoremthene
Pyrene
ButyIbenzyIphthalate
RESULT
U
u D
D
D
U
U
D
D
O
U
U
D
D
D
U
U
U U
U
O
a u
u D
u D
n o
u
u D
D
u D
u
u D
D
D
D
D
D
U
U
D
U
a D
D
U
220
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63 53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
79
99
63
190
63
140
63
120
790
63
63
63
120
180
63
83
73
63
83
ANALYZED
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94 08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/rAS#
SW-846, 8270
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1 91-20-3
106-47-8
87-68-3
59-50-7
91-57-6 ^^
77-47-4 ^y
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
Page #: 16
September 1, 1994 07:54 CERTIFICATE OF A^f^JLYSIS
RESULTS BY SAMPLE
Sample ID: Ml86, GD.23, 10 FT., GRAB Lab ID: 9407027-05A CoUected: 07/26/94 10:32:00
TEST RESULT
Semi-Volatile Organics
Benzo[a] emthracene U
bis(2-Ethylhexyl)phthalate U
Chrysene U
Di-n-octylphthalate D
Benzo[b&k]fluoranthene U
Benzo[a]pyrene U
Indeno[1,2,3-cd]pyrene U
Dibenz[a,h]anthracene U
Benzo[g,h,i]perylene U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Phenol-d5
Nitrobenzene-d5
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
DETECTION
LIMIT
260
83
83
83
160
83
120
83
140
ANfkLYZED
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For Stimi-Volatile Organics 8270S
%Recovery
56.04
59.75
58.88
60.41
71.35
88.92
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
Riple ID: Ml86, GD.23, 15 FT., GRAB Lab ID: 9407027-06A CoUected: 07/26/94 10:45:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIHIT
METHOD/CAS#
Barium
Cadmium
Chrcsmliim
Lead
Arsenic
Mercury
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
121
0.3
12.1
8.9
13.0
U
1.6
U
U
u
D
U
U
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.06
0.1
0.3
1.6
0.098
0.027
0.078
10
10
10
10
10
10
08/16/94
08/16/94
08/16/94
08/16/94
08/17/94
08/16/94
08/18/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
6010
6010
6010
6010
7060
7471
7740
8240
Page #: 17
September 1, 1994 07:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M186, GD.23, 15 FT., GRAB Lab ID: 9407027-06A CoUected: 07/26/94 10:45:00
TEST RESULT
Volatile Organics
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexemone
trems-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
X,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme 12
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
O-Xylene
Surrogate
Surrogate
Toluene-d8
D
U
U
U
U
D
D
D
U
D
U
U
D
U
U
D
D
U
U
D
D
U
U
U
U
U
U
U
B
U
U
u u a u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
07/29/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
/Recovery Data For Volatile Organics 8240S
Bromofluorobenzene
1,2-Dichloroetheme-d4
Semi-Volatile Organics
Phenol
Pyridine
Aniline
bis{2-Chloroethyl)ether
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
D
D
U
U
D
D
D
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
99.6
103
95.4
50
330
330
190
110
63
150
METHOD/CAR#
SW-846, 8240
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2 ^^
108-10-1 ^y
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
Page #: 18
September 1, 1994 07:54 CERTIFICATE OF ANi^JLYSIS
' RESULTS BY SAMPLE
Sample ID: Ml86, GD.23, 15 FT., GRAB Lab ID: 9407027-06A CoUected: 07/26/94 10:45:00
TEST
Semi-Volatile Organics
Benzyl Alcohol
1,2-Dichlorobenzene
2 -Methylphenol
bis (2-Chloroisopropyl)ethe
4 -Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroetheme
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis (2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2_^4,6-Trichlorophenol
Jlk|. 5 -Trichlorophenol
'^l^p.iloronaphthalene
2-Nitroaniline
Dimethylphthalate
Acenaphthylene
3-Nitroemiline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofurem
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Die thyIphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroemiline
4,6-Dinitro-2-methylphenol
n-Ni trosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoremthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
bis(2-Ethylhexyl)phthalate
Chrysene
RESULT
D
U
D
U
U
u
u
u
u
u
u
D
U
D
U
U
U
U
U
u
u
u
u
u D
U
D
U
U
U
U
u D
U
D
D
U
U
u
u
u
u D
u
u D
D
D
U
U
D
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
79
99
63
190
63
140
63
120
790
63
63
63
120
180
63
83
73
63
83
260
83
83
ANJkLYZED
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
Page #: 19
September 1, 1994 07:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M186, GD.23, 15 FT., GRAB Lab ID: 9407027-06A CoUected: 07/26/94 10:45:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Semi-Volatile Organics
Di-n-octylphthalate
Benzo[b&k]fluoremthene
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h]anthracene
Benzo[g,h,i]perylene
1
u ! D
U
i D
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Phenol-d5
Nitrobenzene-d5
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
83
160
83
120
83
140
SW-846, 8270
08/05/94 MMR 117-84-0
08/05/94 MMR 205-99-2/2
08/05/94 MMR 50-32-8
08/05/94 MMR 193-39-5
08/05/94 MMR 53-70-3
08/05/94 MMR 191-24-2
For Semi-Volatile Organics 827OS
%Recovery
57.61
61.22
59.67
61.37
81.05
88.86
Recovery Limits
25 TO 121
24 TO 113
23 TO 120
30 TO 115
19 TO 122
18 TO 137
Sample ID: Ml86, Dl WATER, GRAB Lab ID: 9407027-07A CoUected: 07/26/94 08:30:00
TEST
Semi-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis (2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroetheme
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroemi1ine
Hexachlorobutadiene
RESULT
U
D
U
D
D
D
U
U
U
n u
u
u u u u u u D
u D
U
D
D
U
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
1.5
10
10
5.7
3.3
1.9
4.4
4.6
1.9
2.3
5.7
4.0
12
1.6
1.4
2.2
3.6
2.7
3.4
5.3
2.7
1.9
1.6
1.8
0.90
ANALYZED
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS# |
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
i
Page #: 20
September 1, 1994 07:54
Sample ID: Ml86, DI WATER, GRAB
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9407027-07A CoUected: 07/26/94 08:30:00
TEST
Semi-Volatile Organics
4 -Chloro-3 -methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadi ene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofurem
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4 -Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
jj^Ni t ros odipheny 1 amine
m^k romophenyl-phenylether
^l^^.achlorobenzene
Pentachlorophenol
Phenemthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo[a] emthracene
bis(2-Ethylhexyl)phthalate
Chrysene
Di-n-octylphthalate
Benzo [b&k]fluoranthene
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h] emthracene
Benzo[g,h,i]perylene
RESULT
17
U
U
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
D
U
D
D
D
U
D
U
U
U
U
u
u D
B
U
U
U
U
U
U
u
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/Ii
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Phenol .-d5
Nitrobenzene -d5
2 -Fluorobiphenyl
2,4,6-
Terphe
Tribromophenol
inyl-dl4
DETECTION
LIMIT
3.0
2.2
6.0
2.7
4.0
1.9
1.5
1.6
3.5
2.4
1.9
42
2.4
3.0
1.9
5.7
1.9
4.2
1.9
3.6
24
1.9
1.9
1.9
3.6
5.4
1.9
2.5
2.2
1.9
2.5
7.8
2.5
2.5
2.5
4.8
2.5
3.7
2.5
4.1
AN^LLYZED
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
08/05/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270
%Recovery
40.9
28.3
59.7
61.4
84.7
104
Recovery Limits
21
10
35
43
10
33
TO 100
TO 94
TO 114
TO 116
TO 123
TO 141
Page #: 21
September 1, 1994 07:54 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M186, DECON WATER, GRAB Lab ID: 9407027-08A CoUected: 07/26/94 08:30:00
TEST
Semi-Volatile Orgamics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroetheme
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)metheme
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroemiline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroemiline
Dimethylphthalate
Acenaphthylene
3 - Ni troemi 1 ine
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,6-Dini trotoluene
2,4-Dinitrotoluene
Diethylphthalate
4 -Chlorophenyl-phenylether
Fluorene
4 -Nitroani1ine
4,6-Dinitro-2-methylphenol
n-Ni trosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
RESULT
U
D
a
u
u
u
u
u
u
u
u
u
u u
D
D
U
u
u D
U
D
D
U
U
U
D
D
D
O
U
D
D
D
U
U
D
U
U
0
U
U
D
U
U
D
D
D
U
D
D
U
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
1.5
10
10
5.7
3.3
1.9
4.4
4.6
1.9
2.3
5.7
4.0
12
1.6
1.4
2.2
3.6
2.7
3.4
5.3
2.7
1.9
1.6
1.8
0.90
3.0
2.2
6.0
2.7
4.0
1.9
1.5
1.6
3.5
2.4
1.9
42
2.4
3.0
1.9
5.7
1.9
4.2
1.9
3.6
24
1.9
1.9
1.9
3.6
5.4
1.9
r ANALYZED
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAR*
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
•
Page #: 22
September 1, 1994 07:54 CERTIFICATE OF ANALYSIS
'' . RESULTS BY SAMPLE
Sample ID: Ml86, DECON WATER, GRAB Lab ID: 9407027-08A CoUected: 07/26/94 08:30:00
TEST RESULT
Semi-Volatile Organics
Di-n-butylphthalate
Fluoremthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
D
D
U
U
U
bis(2-Ethylhexyl)phthalate 21 B
Chrysene
Di-n-octylphthalate
U
D
Benzo[b&k]fluoranthene U
Benzo[a]pyrene U
Indeno[1,2,3 -cd]pyrene U
Dibenz[a,h] emthracene
Benzo[g,h,i]perylene
^ \m
u D
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Phenol-d5
Nitrobenzene-dS
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
DETECTION
LIMIT
2.5
2.2
1.9
2.5
7.8
2.5
2.5
2.5
4.8
2.5
3.7
2.5
4.1
ANikLYZED
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8270
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270
%Recovery
41.0
32.5
63.9
83.0
77.7
103
Recovery Limits
21
10
35
43
10
33
TO 100
TO 94
TO 114
TO 116
TO 123
TO 141
• Page #: 23
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limu.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1. IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ENVIRONMENTAL LAB WORK REQUEST 7'/(>g-fi('s.
TfflOKOL ENVIRONMENTAL LABORATORY LWR No. E10617
A, /\ UIALKEB-
KXTEMSION
5^9o
COSTCINIHt
1/400
WORK OROOl
/B940
DATE
^ ORGANIZATION
Bno'ir-p m^ MAIL STOP
Zoit
RBWRT RESUL1S TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
^<
SAMPLE DATE
7'Zt'/i
TYPE
l/
LOCATION
/7-/ee, ^^o i-mru
TIME
Oio^
TEST
luiniui
lAoC - ^240
REMARKS
// // »/ // .5£/^i 7cA - $Z70
fl fl 1^ 11 11 M ^ehi^ :fe,/).,g..^^^^r;.) Fn -LoiO
f-
QD 35, fp/i-fl ^ Oil? T^OC - S240
y II 11 l/ // // -^ih't UOA -SZ70
ll
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11 ly ll /I 71CZA Ai'/ol^ '^ -7470
l/z>c: - Sz4o II 1/ // /)f5D
^ // i< \y ll '( Scmi i/£>4 -SZ70
tl ll ty ll ll /^c/^A ^€h/s -^ft^f/j^
Uoc - ^z4o 6T> 45 ; 6fi-ll ty fl /o^
II n ty ff /OOO ^itrhi I7od-^z7o
11 ll i/ f I /OOCI mizA AUhk ^-7470
CHAIN OF CUSTODY
RELINQUISHED BY
gj^/K//^
DATE
'7-Z9-9f
TIME
/f5<r"
RECEIVED BY DATE
•}^^f'f9
TIME
/y-if
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED SIGNATURE
ENVIRONMENTAL LAB WORK REQUEST
TOi THIOKOL ENVIRONMENTAL LABORATORY
A. f CtJALicefZ.
BON
i/4^0
WOBKOBOBB
1-8940
DAIS
'4-OBOANUAHON me
So/e
•nULIBTOi
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION HME TEST REMARKS
1. Su)//tU ZIZ.
£0 43\ //>fr 1-114 ^ /u-m L^ /M/I( /OIO A/>C' S240
II 7-t<^Af t^ n II Sr-/?// A^A- B^l^
ll II II 'KciZft Ulftils A/4^ 7/^70 f
CSD 43' is ft ll i^ If /o¥^ l7^?C'ez4D
fl // n 1/ -^//ti l/f!iA' SZ70
V // i/ II /I ;gc&4 /jml\ ~'^%47b
•^ /I ll /IdD i/oc - Sz<^
// If
1>^ //»o ^/Itl l/0A'<^Z70
f/ If //^O ^r^A lU/tk/s %^%7t^ r
n.
CHAIN OF CUSTODY
RFIJNQUISHESBY
1 /niJihiik^
DATE
Itf-^^f
TIME
/f-J.^-
RECEIVED BY
^•?ia<^..^—
DATE
i-ii-if
TIME
/t/J^
FOR LABORATORY USE ONLY
1 DAIB OOMTUERD MISBBOSnD nONATOU
#
August 31, 1994 CERTIFICATE OF ANA1.YSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward
MIS 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs MIS 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order # 9408003 Sample and Test Code Identificaition
Lab ID:
OIA
Sample ID: mp Test Codes ajnd Names
M186;GRD35, 5 FT. GRAB
Lab ID:
02A
Sample ID:
M186:GRD35, 10 FT. GRAB
•
UbID:
03 A
Sample ID:
M186; GRD 35, 15 FT. GRAB
Lab ID:
04A
Sample ID:
M186;ORD43, 5 FT. ORAB
UbID:
05A
Sample ID:
M186;GRD43, 10 FT. GRAB
BA AE2
CD AE2
CR AE2
PB AE2
AS GF2
HG CV2
SE GF2
8240S
8270S
Barium
Cadmium
Chromium
Lead
Arsenic
Mercury
Selenium
Volatile Organics
Semi-Volatile Organics
Test Codes and Names
BA AE2
CD AE2
CR AE2
PB"AE2
AS GF2
HG CV2
SE'OFZ
8240S
8270S
Barium
Cadmium
Chromium
Lead
Arsenic
Mercuty
Selenium
Volatile Organics
Semi-Volatile Organics
Test Codes and Names
BA AE2
CD AE2
CR AE2
PB'AE2
AS GF2
HG CV2
SE GF2
8240S
8270S
Barium
Cadmium
Chromium
Lead
Arsenic
Mercury
Selenium
Volatile Oi;ganic8
Semi-Volatile Organics
Test Codes and Names
BA AE2
CD AE2
CR AE2
PB AE2
AS GF2
HG CV2
SE GF2
82«)S
8270S
Barium
Cadmium
Chromium
Lead
Arsenic
Mercury
Selenium
Volatile Organics
Semi-Volatile Organics
Test Codes and Names
BA AE2
CD AE2
CR AE2
PB AE2
AS GF2
HG CV2
SE GF2
8240S
8270S
Barium
Cadmium
Chromium
Lead
Arsenic
Mercuiy
Selenium
Volatile Organics
Semi-Volatile Oiganics
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
SW-846, 8270 Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
SW-846, 8270 Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
SW-846, 8270
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
SW-846, 8270 Method
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
7060
7471
7740
8240
8270
Page#:lof ;?,i5
Work Order <}f 9408003 Sample and Test Code Identification
Lab ED:
06A
Sample ID: ^ M186;GRD43, 15 FT, GRAB
UbID:
07A
lelD:
M186; RINSE FIELD BLANK
Test Codes and Names
BA AE2
CD AE2
CR AE2
PB AE2
AS GF2
HG CV2
SE OFZ
8240S
8270S
Barium
Cadmium
Chromium
Lead
Arsenic
Mercuiy
Selenium
Volatile Organics
Semi-Volatile Organics
Test Codes and Names
HG CVI
AS AE2
BA AE2
CD AE2
CR AE2
PB~AE2
SE~AE2
824b
8270
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Volatile Organics
Semi-Volatile Organics
Workorder Comments
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846. 7471
SW-846, 7740
SW-846, 8240
SW-846, 8270
Method
EPA 245.1
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846, 8270
Certifled
^^7^
ed^
Page #2
Tliis is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: Ml86; GRD 35, 5 FT. GRAB Lab ID: 9408003-OlA Collected: 07/29/94 09:05:00
TEST
Barium
Cadmium
Chromium
Lead
Arsenic
Mercury-
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorometheme
^Mmoform
J^^Tiome thane
l^fatanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2 -Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethcine
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropame
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Te t rachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroetheme
RESULT
125
U
16.4
18.5
8.2
U
1.1
U
U
U
U
U
U
U
U
U
U
U
U
U
U
D
D
U
U
U
D
D
U
D
D
U
D
U
D
11
D
D
D
U
U
3 BJ
U
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.06
0.1
0.3
1.6
0.10
0.015
0.08
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
08/:L6/94
08/:L6/94
08/16/94
08/:L6/94
08/17/94
08/16/94
08/3L8/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
BY
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01
10061-02
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
6010
6010
6010
6010
7060
7471
7740
8240
-5
-6
Page #: 3
August 31, 1994 15:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M186; GRD 35, 5 FT. GRAB Lab ID: 9408003-01A CoUected: 07/29/94 09:05:00
TEST - RESULT
Volatile Organics
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xyl ene
U
D
D
V
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
ANALYZED
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
Surrogate/Recovery Data For Volatile Organic
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
Semi-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroemiline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2 -Chloronaphthalene
2-Ni troemi1ine
Dimethylphthalate
Acenaphthylene
3-Nitroemiline
Acenaphthene
2,4-Dinitrophenol
U
U
O
U
U
D
D
U
U
U
D
U
U
U
D
D
D
U
D
U
D
U
U
U
U
D
D
U
D
U
U
D
U
U
D
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Re covery
99.0
105
96.7
50
330
330
190
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
BY
JMA
JMA
JMA
JMA
JMA
8 8240S
HETHOD/CAS#
SW-846, 8240
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6 ^k
95-50-1 ^V
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
Page #: 4
August 31, 1994 15:01 CERTIFICATE OF ANi^XYSIS
RESULTS BY SAMPLE
Sample ID: Ml86; GRD 35, 5 FT. GRAB Lab ID: 9408003-OlA Collected: 07/29/94 09:05:00
TEST RESULT UNITS DETECTION ANiLLYZED BY
LIMIT
METHOD/CAS#
Semi-Volatile Organics
4-Nitrophenol
Dibenzofuran
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4, 6-Dinitro-2-methylphenol
n-Nitrosodipheny1amine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
bis(2-Ethylhexyl)phthalate
Chrysene «i-octylphthalate
so[b&k]fluoranthene
so[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h] emthracene
Benzo[g,h,i]perylene
u
u u u u
u u u u u u u u u D
u u
u D
U
u u u
u u D
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
SW-846, 8270
79 08/09/94 MMR 100-02-7
99 08/09/94 MMR 132-64-9
63 08/09/94 MMR 606-20-2
190 08/09/94 MMR 121-14-2
63 08/09/94 MMR 84-66-2
140 08/09/94 MMR 7005-72-3
63 08/09/94 MMR 86-73-7
120 08/09/94 MMR 100-01-06
790 08/09/94 MMR 534-52-1
63 08/09/94 MMR 86-30-6
63 08/09/94 MMR 101-55-3
63 08/09/94 MMR 118-74-1
120 08/09/94 MMR 87-86-5
180 08/09/94 MMR 85-01-8
63 08/09/94 MMR 120-12-7
83 08/09/94 MMR 84-74-2
73 08/09/94 MMR 206-44-0
63 08/09/94 MMR 129-00-0
83 08/09/94 MMR 85-68-7
260 08/09/94 MMR 56-55-3
83 08/09/94 MMR 117-81-7
83 08/09/94 MMR 218-01-9
83 08/09/94 MMR 117-84-0
160 08/09/94 MMR 205-99-2/2
83 08/09/94 MMR 50-32-8
120 08/09/94 MMR 193-39-5
83 08/09/94 MMR 53-70-3
140 08/09/94 MMR 191-24-2
Surrogate/Recovery Data For Seml-VolatllB Organics 8270S
Surrogate
2 -Fluorophenol
Phenol-d5
Nitrobenzene-d5
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
%Recovery
51.60
52.76
46.33
59.59
80.66
94.72
Racovery Limits
25 TO 121
24 TO 113
23 TO 120
30 TO 115
19 TO 122
18 TO 137
Sample ID: M186; GRD 35, 10 FT. GRAB Lab ID: 9408003-02A Collected: 07/29/94 09:17:00
TEST RESULT UNITS DETECTION ANAiLYZED BY
hJM.1T
METHOD/CAS#
Barium
Cadmium
123
0.2
ug/g
ug/g
0.06 08/16/94 LVD
0.1 08/16/94 LVD
SW-846, 6010
SW-846, 6010
Page #: 5
August 31, 1994 15:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: Ml86; GRD 35, 10 FT. GRAB Lab ID: 9408003-02A CoUected: 07/29/94 09:17:00
TEST
Chromium
Lead
Arsenic
Mercury
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromofonn
Bromome t:hcuie
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2 -Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
18.0
18.8
6.5
U
1.1
U
U
D
U
U
D
O
U
U
D
U
U
D
U
U
D
U
U
D
U
D
U
D
U
U
U
D
D
U
U
U
U
U
D
5 BJ
U
U
D
U
U
U
UNITS
ug/g
ug/g
ug/g
ug/g
• ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.3
1.5
0.1
0.02
0.08
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
08/16/94
08/16/94
08/17/94
08/16/94
08/18/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
BY
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7 ^^
75-00-3 ^^
110-75-8 ^^
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Page #: 6
August 31, 1994 15:01 CERTIFICATE OF AN^^JLYSIS
=' RESULTS BY SAMPLE
Sample ID: Ml86; GRD 35, 10 FT. GRAB Lab ID: 9408003-02A CoUected: 07/29/94 09:17:00
TEST RESULT
Volatile Organics
Surrogate/Re(
Surrogate
Toluene-d8
UNITS DETECTION
LIMIT
ANJLLYZED BY
:overy Data For Volatile Organics 8240S
Bromofluorobenzene
1,2-Dichloroethane-d4
Semi-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propyleimine
^l^^-achloroe thane
l^P robenzene
TRophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)metheme
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
Acenaphthylene
3-Nitroemiline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
U
U
U
U
U
D
D
D
U
D
U
D
U
U
U
U
U
U
D
U
U
U
U
U
U
D
U
U
U
U
D
U
U
U
U
U
U
D
U
U
D
D
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
99.0
104
99.5
50
330
330
190
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
79
99
63
190
63
140
METHOD/CAS#
SW-846, 8240
Recovery Limits
81
74
70
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
oa/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
• Page #: 7
August 31, 1994 15:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M186; GRD 35, 10 FT. GRAB Lab ID: 9408003-02A CoUected: 07/29/94 09:17:00
TEST
Semi-Volatile Organics
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
n - Ni trosodiphenyleunine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenemthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
bis(2-Ethylhexyl)phthalate
Chrysene
Di-n-octylphthalate
Benzo[b&k]fluoranthene
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h]anthracene
Benzo[g,h,i]perylene
RESULT
U
D
D
U
U
D
U
U
U
U
U
U
U
D
D
U
D
U
U
D
U
n
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Pheno] .-d5
Nitrobenzene -d5
2 -Fluorobiphenyl
2,4,6-
Terphe
Tribromophenol
!nyl-dl4
DETECTION
LIMIT
63
120
790
63
63
63
120
180
63
83
73
63
83
260
83
83
83
160
83
120
83
140
ANALYZED
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2 ^^
For Seml-Volatlle Organics 8270S ^^
%Recovery
56.00
56.43
48.88
62.74
81.03
96.00
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
Sample ID: Ml86; GRD 35, 15 FT. GRAB Lab ID: 9408003-03A CoUected: 07/29/94 09:30:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Barium
Cadmium
Chromium
Lead
Arsenic
130
D
12.8
8.0
12.5
ug/g
ug/g
ug/g
ug/g
ug/g
0.1
0.1
0.3
1.5
0.1
08/16/94
08/16/94
08/16/94
08/16/94
08/17/94
LVD
LVD
LVD
LVD
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
7060
Page ff: 8
August 31, 1994 15:01 CERTIFICATE OF A>[^J.YSIS
RESULTS BY SAMPLE
Sample ID: M186; GRD 35, 15 FT. GRAB Lab ID: 9408003-03A CoUected: 07/29/94 09:30:00
TEST RESULT
Mercury
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
D ibromochloromethane
1,1-Dichloroethane
jjj^-Dichloroe thane
fl^^-Dichloroe thene
^I^Bfexemone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane 5
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
Surrogat
Surrogate
Toluene-d8
U
1.5
U
D
U
U
U
D
U
U
U
U
U
D
D
U
D
D
U
U
D
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
BJ
U
D
U
U
U
D
UNITS
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.03
0.08
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANikLYZED
08/16/94
08/18/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
BY
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
e/Recovery Data For Volatile Organics 8240S
Bromofluorobenzene
%Recovery
97.7
96.9
METHOD/CAS#
SW-846, 7471
SW-846, 7740
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
TO 117
TO 121
• Page ft: 9
August 31, 1994 15:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M186; GRD 35, 15 FT. GRAB Lab ID: 9408003-03A CoUected: 07/29/94 09:30:00
TEST
Volatile Organics
RESULT UNITS
1,2-Dichloroetheme-d4
Seml-Volatlle Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroetheme
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4 -Chloroemi1ine
Hexachlorobutadiene
4 -Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2 -Chloronaphthalene
2-Nit roemi1ine
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofurem
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroemiline
4,6-Dinitro-2-methylphenol
n-Nitrosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
U
D
D
U
U
U
D
U
U
D
D
U
D
U
U
U
D
U
U
D
U
D
D
U
U
U
U
D
U
U
D
U
D
D
D
D
U
D
a D
D
D
U
D
U
D
D
D
D
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
98.5
50
330
330
190
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
79
99
63
190
63
140
63
120
790
63
63
63
ANALYZED
70
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
BY
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8240
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0 ^
111-91-1 ^m
120-83-2 ^^
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
Page ff: 10
August 31, 1994 15:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M186; GRD 35, 15 FT. GRAB Lab ID: 9408003-03A CoUected: 07/29/94 09:30:00
TEST
Seml-Volatlle Organics
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
bis(2-Ethylhexyl)phthalate
Chrysene
Di-n-octylphthalate
Benzo[b&k]fluoranthene
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h] emthracene
Benzo[g,h,i]perylene
RESULT
U
D
U
U
U
U
U
U
U
U
U
U
U
U
U
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
11^^ Phenol -d5
I^P Nitrobenzene -d5
^^ 2 - Fluorobiphenyl
2,4,6-
Terphe
Tribromophenol
nyl-dl4
DETECTION
LIMIT
120
180
63
83
73
63
83
260
83
83
83
160
83
120
83
140
AKMLLYZED
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For S£iml-Volatile Organics 8270S
%Recovery
48
49
43
54
71
87
.47
.38
.17
.96
.57
.03
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
Sample ID: M186; GRD 43, 5 FT. GRAB Lab ID: 9408003-04A CoUected: 07/29/94 10:00:00
TEST RESULT UNITS DETECTION AlSTALYZED BY
LIMIT
METHOD/CAS#
Barium
Cadmium
Chromium
Lead
Arsenic
Mercury
Selenium
123
U
15.5
12.5
7.9
D
1.3
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
0.1
0.1
0.3
1.6
0.1
0.02
0.08
08/16/94
08/16/94
08/16/94
08/16/94
08/17/94
08/16/94
08/18/94
LVD
LVD
LVD
LVD
CRS
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
7060
7471
7740
Page#: 11
August 31, 1994 15:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAJVIPLE
Sample ID: M186; GRD 43, 5 FT. GRAB Lab ID: 9408003-04A CoUected: 07/29/94 10:00:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2 -Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
4
U
U
D
U
U
U
U
U
0
U
U
U
D
D
U
U
D
U
U
U
U
U
U
D
D
U
D
D
U
U
D
U
U
U
BJ
D
D
U
D
U
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-
Seml-Volatile Organics
Phenol
Dichloroetheme-d4
U ug/Kg
%Recovery
99.9
96.4
102
50
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5 ^^
10061-02-6 VV 95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
08/09/94
TO 117
TO 121
TO 121
MMR
SW-846, 8270
108-95-2
Page ff: 12
August 31, 1994 15:01
Sample ID: Ml86; GRD 43, 5 FT. GRAB
CERTIFICATE OF ANALYSIS
' RESULTS BY SAMPLE
Lab ID: 9408003-04A CoUected: 07/29/94 10:00:00
TEST
Semi-Volatile Organics
Pyridine
Aniline
bis(2-Chloroethyl)ether
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
J^^iloroemiline
fl^Fdchlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2 -Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4 -Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methyIphenol
n-Nitrosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
RESULT
U
u u
D
U
U
U
U
D
U
U
U
U
U
U
U
U
U
D
U
U
U
U
D
U
U
D
D
U
D
U
U
U
U
U
D
U
U
U
U
D
U
U
U
U
U
U
D
D
U
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
330
330
190
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
79
99
63
190
63
140
63
120
790
63
63
63
120
180
63
83
ANAIiYZED
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
• Page ff: 13
August 31, 1994 15:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: Ml86; GRD 43, 5 FT. GRAB Lab ID: 9408003-04A CoUected: 07/29/94 10:00:00
TEST RESULT
Seml-Volatlle Organics
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
U
D
D
D
bis(2-Ethylhexyl)phthalate D
Chrysene
Di-n-octylphthalate
U
U
Benzo [b&)c] fluoranthene D
Benzo [a] pyrene D
Indeno[1,2,3-cd]pyrene D
Dibenz[a,h]anthracene
Benzo[g,h,i]perylene
D
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Phenol-d5
Nitrobenzene-dS
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
DETECTION
LIMIT
73
63
83
260
83
83
83
160
83
120
83
140
ANALYZED
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For Seml-Volatlle Organics 8270S
%Recovery
54
55
48
61
73
86
.70
.56
.29
.95
.96
.28
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137 ^^
Sample ID: Ml86; GRD 43, 10 FT. GRAB Lab ID: 9408003-05A CoUected: 07/29/94 10:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS«
Barium
Cadmium
Chromium
Lead
Arsenic
Mercury
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
147
U
11.1
7.5
7.4
D
1.6
D
U
D
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
0.1
0.1
0.3
1.6
0.1
0.03
0.08
10
10
10
08/16/94
08/16/94
08/16/94
08/16/94
08/17/94
08/16/94
08/18/94
08/04/94
08/04/94
08/04/94
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
6010
6010
6010
6010
7060
7471
7740
8240
Page ff: 14
August 31, 1994 15:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: Ml86; GRD 43, 10 FT. GRAB Lab ID: 9408003-05A CoUected: 07/29/94 10:20:00
TEST
Volatile Organics
Benzene
Bromodichloromethane
Bromoform
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trems-1,2-Dichloroethene
1,2-Dichloropropeme
cis-l,3-Dichloropropene
trans-1,3-Dichloropropene
1^2-Dichlorobenzene
^1^^-Dichlorobenzene
.^IPr-Di chlorobenz ene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Te t rachl oroe thene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
vinyl Chloride
o-Xylene
RESULT
U
u u D
D
U
U
U
U
U
U
D
U
D
U
D
U
U
U
U
U
U
U
U
U
D
U
U
U
U
D
6 BJ
U
U
U
D
D
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
AtTilLLYZED
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
iTMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
Seml-Volatlle Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
U ug/Kg
U ug/Kg
U ug/Kg
U ug/Kg
%Recovery
101
96.0
99.4
50
330
330
190
Recovery Limits
81 TO 117
74 TO 121
70 TO 121
08/09/94 MMR
08/09/94 MMR
08/09/94 MMR
08/09/94 MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
Page ff: 15
August 31, 1994 15:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M186; GRD 43, 10 FT. GRAB Lab ID: 9408003-05A CoUected: 07/29/94 10:20:00
TEST
Seml-Volatlle Organics
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroethane -
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)metheme
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4 -Chloroemi1ine
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofurem
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4 -Chlorophenyl-phenylether
Fluorene
4-Nitroemiline
4,6-Dinitro-2-methylphenol
n-Nitrosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenemthrene
Anthracene
Di-n-butylphthalate
Fluoremthene
Pyrene
Butylbenzylphthalate
RESULT
D
U
U
u D
D
U
U
D
U
D
U
D
D
U
D
D
U
D
D
U
D
U
U
D
D
U
U
U
D
D
U
D
U
D
U
U
D
D
U
D
D
U
D
U
D
U
D
D
U
D
U
XJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
79
99
63
190
63
140
63
120
790
63
63
63
120
180
63
83
73
63
83
r ANALYZED
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6 ^^
77-47-4 ^1^
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
Page ff: 16
August 31, 1994 15:01 CERTIFICATE OF A^[ALYSIS
RESUI.TS BY SAMPLE
Sample ID: M186; GRD 43, 10 FT. GRAB Lab ID: 9408003-05A CoUected: 07/29/94 10:20:00
TEST RESULT
Seml-Volatlle Organics
Benzo[a] emthracene U
bis(2-Ethylhexyl)phthalate U
Chrysene U
Di-n-octylphthalate U
Benzo[b&k]fluoranthene U
Benzo[a]pyrene D
Indeno[l,2,3 -cd]pyrene D
Dibenz[a,h] emthracene U
Benzo[g,h,i]perylene U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Phenol-d5
Nitrobenzene-d5
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
DETECTION
LIMIT
260
83
83
83
160
83
120
83
140
AN;LLYZED
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
08/09/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For Siaml-Volatile Organics 8270S
%Recovery
48.16
48.47
42.38
54 .06
66.24
88.28
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
1^ ample ID: Ml 86; GRD 43, 15 FT. GRAB Lab ID: 9408003-06A CoUected: 07/29/94 10:45:00
TEST RESULT UNITS DETECTION ANJ^YZED BY
LIMIT
METHOD/CAS#
Barium
Cadmium
Chromium
Lead
Arsenic
Mercury
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
124
D
16.2
10.6
12.5
U
1.6
U
U
U
U
D
U
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.1
0.1
0.3
1.5
0.1
0.02
0.08
10
10
10
10
10
10
08/16/94
08/16/94
08/16/94
08/16/94
08/17/94
08/16/94
08/18/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
LVD SW-846, 6010
LVD SW-846, 6010
LVD SW-846, 6010
LVD SW-846, 6010
CRS SW-846, 7060
CRS SW-846, 7471
CRS SW-846, 7740
SW-846, 8240
JMA 67-64-1
JMA 107-02-8
JMA 107-13-1
JMA 71-43-2
JMA 75-27-4
JMA 75-25-2
Page if': 17
August 31, 1994 15:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M186; GRD 43, 15 FT. GRAB Lab ID: 9408003-06A CoUected: 07/29/94 10:45:00
TEST
Volatile Organics
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2 -Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroetheme
Trichloroethene
Tri chlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
4
U
U
U
D
U
D
U
u u D
D
U
U
D
D
U
D
U
U
D
D
U
D
D
U
D
U
D
BJ
D
U
U
U
u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
08/04/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-
Seml-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
•Dichloroethane-d4
u D
U
U
D
U
D
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
99.9
99.0
97.7
50
330
330
190
110
63
150
METHOD/CAS#
SW-846, 8240
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2 ^^
108-10-1 ^H
100-42-5 ^^
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Llnits
81
74
70
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
Page ff: 18
August 31, 1994 15:01 CERTIFICATE OF AN^I^YSIS
RESULTS BY SAMPLE
Sample ID: Ml86; GRD 43, 15 FT. GRAB Lab ID: 9408003-06A CoUected: 07/29/94 10:45:00
TEST
Semi-Volatile Organics
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis (2-Chloroethoxy)metheme
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
^4,6-Trichlorophenol
J^k.5-Trichlorophenol
WJ^.il oronaphthal ene
^Nitroemiline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofurem
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4 -Chlorophenyl-phenylether
Fluorene
4 - Ni troemi 1 ine
4,6-Dinitro-2-methyIphenol
n-Ni trosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenemthrene
Anthracene
Di-n-butylphthalate
Fluoremthene
Pyrene
Butylbenzylphthalate
Benzo[a] emthracene
bis(2-Ethylhexyl)phthalate
Chrysene
RESULT
U
u u
u u u u D
U
u D
D
D
U
U
D
U
U
D
D
U
U
U
U
D
U
U
D
U
U
U
U
D
U
U
D
U
U
U
u u
u u
u u
u u D
D
D
U
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
79
99
63
190
63
140
63
120
790
63
63
63
120
180
63
83
73
63
83
260
83
83
ANikLYZED
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
08/
10/94
10/94
10/94
10/94
10/94
10/94
10/94
10/94
10/94
10/94
10/94
10/94
10/94
10/94
10/94
10/94
10/94
10/94
10/94
LO/94
LO/94
LO/94
10/94
LO/94
LO/94
LO/94
LO/94
LO/94
LO/94
LO/94
LO/94
LO/94
LO/94
LO/94
LO/94
LO/94
LO/94
LO/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
Page ff: 19
August 31, 1994 15:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: Ml86; GRD 43, 15 FT. GRAB Lab ID: 9408003-06A CoUected: 07/29/94 10:45:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METEOD/CAS#
Seml-Volatlle Organics
Di-n-octylphthalate
Benzo[b&k]fluoranthene
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h]anthracene
Benzo[g,h,i]perylene
1
u
! U
D
! D
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Phenol-d5
Nitrobenzene-d5
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
63
160
83
120
83
140
SW-846, 8270
08/10/94 MMR 117-84-0
08/10/94 MMR 205-99-2/2
08/10/94 MMR 50-32-8
08/10/94 MMR 193-39-5
08/10/94 MMR 53-70-3
08/10/94 MMR 191-24-2
For Seml-Volatlle Organics 8270S
%Recovery
45.46
45.90
38.67
49.27
63.79
81.92
Recovery Limits
25 TO 121
24 TO 113
23 TO 120
30 TO 115
19 TO 122
18 TO 137
Sample ID: Ml86; RINSE FIELD BLANK Lab ID: 9408003-07A CoUected: 07/29/94 11:00:00
TEST
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromometheme
2-Butemone
Carbon disulfide
RESULT
U
u
13.3
3.0
D
U
u
21.2
U
U
D
U
U
U
U
u
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
0.2
50
1
2
5
25
60
10
10
10
10
10
10
10
10
10
ANALYZED
08/16/94
08/16/94
08/16/94
08/16/94
08/16/94
08/16/94
08/16/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
BY
CRS
LVD
LVD
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS# %
EPA 245.1
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
6010
6010
6010
6010
6010
6010
8240
1
Page ff: 20
August 31, 1994 15:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: Ml86; RINSE FIELD BLANK Lab ID: 9408003-07A , CoUected: 07/29/94 11:00:00
TEST - RESULT
Volatile Organics
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexanone
trems -1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Stvrene
m^k' 2 # 2-Tetrachloroethane
^HV^rachloroe thene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroetheme
Tri chloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
U
U
U
U
U
D
D
U
U
U
U
U
U
D
D
D
U
U
U
U
D
D
D
D
D
U
D
U
U
U
U
U
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
08/01/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
Seml-Volatlle Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
D
U
U
U
D
U
D
D
U
U
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%Recovery
98.7
103
101
1.5
10
10
5.7
3.3
1.9
4.4
4.6
1.9
2.3
METHOD/CAS#
SW-846, 8240
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
Page ff: 21
August 31, 1994 15:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: Ml86; RINSE FIELD BLANK Lab ID: 9408003-07A CoUected: 07/29/94 11:00:00
TEST
Semi-Volatile Organics
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroetheme
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4 -Chloroani1ine
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroemiline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
n-Nitrosodipheny1amine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenemthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
ButylbenzyIphthalate
Benzo[a]anthracene
bis(2-Ethylhexyl)phthalate
Chrysene
Di-n-octylphthalate
Benzo[b&k]fluoranthene
Benzo[a]pyrene
RESULT
u D
D
U
D
U
D
U
U
D
U
U
D
U
D
U
D
U
D
D
U
U
D
U
D
D
U
U
D
U
u 6 BJ
U
U
D
U
11
U
U
D
U
D
D
D
U
U
U
9 J
U
D
D
D
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
5.7
4.0
12
1.6
1.4
2.2
3.6
2.7
3.4
5.3
2.7
1.9
1.6
1.8
0.90
3.0
2.2
6.0
2.7
4.0
1.9
1.5
1.6
3.5
2.4
1.9
42
2.4
3.0
1.9
5.7
1.9
4.2
1.9
3.6
24
1.9
1.9
1.9
3.6
5.4
1.9
2.5
2.2
1.9
2.5
7.8
2.5
2.5
2.5
4.8
2.5
r ANALYZED
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
08/10/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3 ^^
208-96-8 MP
99-09-2 ^
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
Page ff: 22
August 31, 1994 15:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: Ml86; RINSE FIELD BLANK Lab ID: 9408003-07A CoUected: 07/29/94 11:00:00
TEST RESULT
Seml-Volatlle Organics
Indeno[1,2,3-cd]pyrene U
Dibenz[a,h] emthracene U
Benzo[g,h,i]perylene D
UNITS
ug/L
ug/L
ug/L
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Phenol-d5
Nitrobenzene-dS
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
DETECTION
LIMIT
3.7
2.5
4.1
AJSTALYZED BY METHOD/CAS#
SW-846, 8270
08/10/94 MMR 193-39-5
08/10/94 MMR 53-70-3
08/10/94 MMR 191-24-2
For Seml-Volatlle Organics 8270
%Recovery
43.4
35.6
56.7
72.8
82.9
95.6
Recovery Limits
21 TO 100
10 TO 94
35 TO 114
43 TO 116
10 TO 123
33 TO 141
# Page ff: 23
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates conipound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. l.U with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ENVIRONMENTAL LAB WORK REQUEST 9/Pll7:^
1
^TD: THIOKOL ENVIRONMENTAL LABORATORY
WOM:
A\ f^ LiiAUCtl/^
ORGANIZATION
EMU SKiai^
EXTENSION
^Z90
MAIL STOP
Zol C
LWR No. El 0622
OOSTCSNTHI
1/4/IO
WORK ORDOt DATE
24 /h<p 94
REPORT RESIJLTi; TO: ^
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE
1 SL^A^U 206
C£ri_o£TrtSfl
DATE TYPE
l/
LOCATION
^^-l3i, dll Pit
TIME
/Ol^
TEST
l/oc '• l?z4^
REMARKS
/( /' /O/b C4, Cr, 'Ph - &0/0
Ccr of rli ID'
\Cen of P7f lo'
II ty fl /03^ l7oc~ 9z4d
II t/ II /07C Cd, Cr, PU - ^O/O
Pup.Gift o-/^Pi"h/0
b\/iP Ootcf £,
1 8 Sop/MO ids
l>Olcr e^.t /OI
I tl ty fl /o3r CJ, Cr, Ph ' Go 11^
fl 1/ /I lof^ l/oc - sz4d
:T I I f< 164-i' Voc '• 8z40
I' fl /O' 4<' CJ, Cr, PJ> - ^/O
7Ao
ll ty fl //7s-r j/oc ' ez40
'"•SajHO Zog
Ookred,j, ml ^ It n /d^< C<J,Cr, ?b- t^O/O
l( M-ie? Dru^ oftHTtt-/S-Qh VOL- ez4^
12- 5LU>RL' STS-y
li \y M-167 T)rup>. S/gTB^ /S'6 0 M» - 7470 ^<:rcAlore^ fc^ T<L.
CHAIN OF CUSTODY
RELINQUISHED BY
•4l:477./377^
DATE
^^/kiife/
TIME
^fA>o>
RECEIVED BY
.^T^/AJf/^au.
DATE
^-s/i^-A fV
TIME
^ft^
\
FOR LABORATORY USE ONLY
DATE rr)MPI.ETED
#
DATE RB>ORTED
ENVIRONMENTAL LAB WORK REQUEST 1^09O>ly
"• THIOKOL ENVIRONMENTAL LABORATORY /^/oCZZ. pa^ 2-i
^/^ l/j/H^teiL
ORGANUAHON
^hJL^ BhJCR
^S90
MAIL nor
COCTCBNTBB WOBKOBDOl
U4c^ I IEf4c) \//^/h(6 9A
PDIT BBULTC TOi 7
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TE?r REMARKS
I. iUAAtU S^S-t
a 24 -Z' £l±i /X-187 t?ft«»^i ^. /570 //Od- gzfo
^f h^ \y 11 n <7J, Cr, fit^ ,Ph ' ^O 'O
-Tc.
^y< ^"i^ 11 I^Ed l/oc - ©Z^
/^4 ti ^' M
fl
ty / /S'3o ^<^^l ^, % -,^'''\ /4<^~ 74li. R-jyLlnr^k.\ •' XC.
i-csMl\^.0 SS'I i/ // /i'05' Voc - SZ40
/I «/ / / /i'D^ CJ,C^, A^, Pb-Goio
Ma - 74 10 P<'r^U loralr s ^ -zc
7. SuJMO •S'S'I /I iX /I /&/0 lAoc - ez4o
*-Su^/liO S'S'I fl ly /I /le/D /^,C^, i4^, Pb- f^oio
M^=- 7^1.-7^ Pcr^lilora/^S -IC
'•5c*^Af SSI
II y f I /Uio l/oc ' 8z40
ly II 16, ZO l/oc - 9Z40
'^^ €-fr If 1^' ll /CZo <2d, Cr, A^ ,Pt>-' 00/O
1-/^- -74 70 . T^r^.ii/or^lcy .IL^
71 /I t/ // /6'«S5" l/oc " ^Z40
9ff^l
CHAIN OF CUSTODY
RBJNQUISHB) BY DATE TIME RECQVESBY OATE TIME
^ff^tmL. tC/^M 9<f d?dJ /^^^,,. ^A^Y^f /y^^i^
FOR LABORATORY USE ONLY
MISOOMIUnD MTCRBPOnBD BONATVai
ENVIRONMENTAL LAB WORK REQUEST
4
^^/^^P>^
THIOKOL ENVIRONMENTAL LABORATORY £/0li>2Z y^'^
Af lo/^bt^A^ sa?o
OOSTLBNIkK WORKOBDBK
/R?40 WAf.'fc/
^ o•CA^azA'^ON MAIL STOP
^i'/ ^/^r :^7e
B8POBT KDULTS TOt
HELEN WARD, MS 301
SAMPLE INFORMATION
DATE TYPE
14/^^ y
LOCATION TIME
/U'lBT Vnjfi, ^ie. ^. /S6^
TEST REMARKS
dJ, Cr, A^, Pb - OO/O
/lj - 74-70 ?irr/M/orJtr. \ -Z<L.
Z4Au
^
«/ /I /€40 l/oc- -9Z40
~C<iiC^,'^^, Pi,' 1^0IO
uj - 7470 . 7^e:rckloralc\ fl i-^ 11 /^'40 -2:<r
/I /f /rso ^oc - t3Z40
/I /^SO
£d, Cr, A^j, fih -^^fo
/fa- 747o p£.r6/i/ore.le. Z-lL.
CHAIN OF CUSTODY
RBJNQUISaES BY
lUf^lhf
DATE HME
^r? ^
/^906
RBCSVOlliY
^M/^f-^'
DATE
<^::; f/z^/fiT-
TIME
//^^(^
FOR LABORATORY USE ONLY r""-mCNAIISB
November 1, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward
MIS 301
A.F. WALKER, MIS 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Oty, Ut 84302-0707
Analytical Labs MIS 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order # 9408026 Sample and Test Code Identification
Lab ID: Sample ID:
OIA M-136, CEN. OF PIT 5 FT.
Lab ID: Sample ID:
02A M-136, CEN. OF PIT 10 FT.
Lab ID:
03A
Lab ID:
04A
Lab ID:
05A
Lab ID:
06A
Lab ID:
07A
Lab ID:
OSA
Sample ID:
M-136,CEN. OF PIT lOFT.DUP
Sample ID:
M-136, OUTER EDGE 5 FT.
Sample ID:
M-136, OUTER EDGE SFT. DUP
Sample ID:
M-136, OUTER EDGE 10 FT.
Sample ID:
M-187, GRD 24 SURFACE
Sample ID:
M-187, GRD 24, 2 FT.
Test Codes and Names
CD_AE2 Cadmium
CR_AE2 Chromium
PB AE2 Lead
824t)S Volatile Organics
Test Codes and Names
CD_AE2 Cadmium
CR_AE2 Chromium
PB_AE2 Lead
8240S Volatile Organics
Test Codes and Names
CD_AE2 Cadmium
CR_AE2 Chromium
PB_AE2 Lead
Test Codes and Names
CD_AE2 Cadmium
CR_AE2 Chromium
PB_AE2 Lead
8240S Volatile Organics
Test Codes and Names
Lab ID:
09A
Sample ID:
M.187, GRD24, 5 FT.
8240S Volatile Organics
Test Codes and Names
CD AE2
CR AE2
PB AE2
8240S
Cadmium
Chromium
Lead
Volatile Organics
Test Codes and Names
CL04
CD AE2
CR AE2
PB AE2
AG AE2
HO CV2
8240S
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
CL04
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8240s
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
CL04
CD AE2
Perchlorate
Cadmium
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
Method
SW-846, 8240
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
Method
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SOP 314
SW-846, 6010
Page ff:l of ;J.^
Work Orders 9408026
0! b ID: Sample ID:
09A M-187, GRD 24, 5 FT.
Lab ID: Sample ID:
lOA M-187, GRD 6 SURFACE
Lab ID:
llA
Sample ID:
M-187, GRD 6, 2 FT.
Lab ID:
12A
Lab ID:
I3A
Sample ID:
M-187, GRD 6, 2 FT. DUP.
Sample ID: impl M-187, GRD 6, 5 FT.
Lab ID:
•
14A
Sample ID:
M-187, GRD 4 SURFACE
Lab ID:
^3A—
Sample ID:
M-187, GRD 4, 2 FT.
Lab ID:
16A
Sample ID:
M-187, GRD 4, 5 FT.
Sample and Test Code Identificaition
Test Codes and Names
CR AE2
PB AE2
AG AE2
HG CV2
8240S
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
CL04
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8240s
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
CL04
CD_AE2
CR_AE2
PB_AE2
AG_AE2
HG CV2
8245s
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
8240S Volatile Organics
Test Codes and Names
CL04
CD_AE2
CR_AE2
PB_AE2
AG_AE2
HG CV2
8240s
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
CL04
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8240s
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercuty
Volatile Organics
Test Codes and Names
CL04
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8240S
Perchlorate
Cadmium
Chromium
Lead
Silver
Mereury
Volatile Organics
Test Codes and Names
CL04
CD_AE2
CR_AE2
PB_AE2
AG_AE2
HG CV2
8240s
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SW-846, 8240
Method
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SOP 314
SW-846, 6010
SW-846,
SW-846,
SW-846,
SW-846,
SW-846, 8240
Method
, 6010
,6010
,6010
, 7471
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SOP 314
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
7471
8240
Page ff:2
Workorder Comments
Report: The results for metals of sample 94-08-026-06A (M-136, Outer
Edge 10ft.) indicated a large degree of nonhomogeneity. The
average of the replicates is reported.
rY^^^?-^-^
Xeirtifi^^
Page #:3
This is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: M-136, CEN. OF PIT 5 FT. Lab ID: 9408026-01A Collected: 08/24/94 10:15:00
TEST
Cadmium
Chromiiun
Lead
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
B romodi chloromethane
Bromoform
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2 -Chloroethylvinyl ether
Chloroform
jjjj^orome thfuie
AM romochlorometheuie
^l|^ - Di chloroe thane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2 -Dichloropropsuie
cis-l,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
U
29.9
82.0
D
D
D
46 J
U
D
U
U
U
U
U
U
U
U
U
U
D
U
U
D
U
U
D
U
U
D
U
U
D
D
D
D
D
65 J
D
U
890 J
D
D
D
U
DNITS
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
1.6
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
ANJ;i.YZED
09/13/94
09/13/94
09/13/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
BY
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
• Page #: 4
October 28, 1994 08:05 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-136, CEN. OF PIT 5 FT. Lab ID: 9408026-01A Collected: 08/24/94 10:15:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Surrogate/Recovery Data For Volatile Organics 8240S
SW-846, 8240
Surrogate %Recovery
Toluene-d8 100
Bromofluorobenzene 95.0
1,2-Dichloroetheme-d4 95.6
Recovery Limits
81 TO 117
74 TO 121
70 TO 121
Sample ID: M-136, CEN. OF PIT 10 FT. Lab ID: 9408026-02A CoUected: 08/24/94 10:35:00
TEST
Cadmium
Chromium
Lead
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chlorofonn
Chlorome theme
Dibromochlorone theme
1,1-Dichloroethane
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexanone
trems-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
RESULT
0.42
' 22.9
36.1
U
U
D
U
U
D
U
U
U
D
U
D
U
D
D
U
U
U
XJ
U
U
U
U
D
U
U
U
D
UNITS
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
1.4
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
ANALYZED
09/13/94
09/13/94
09/13/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
BY
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS«
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240 ^B
67-64-1 ^^
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
Page ff: 5
October 28, 1994 08:05
Sample ID: M-136, CEN. OF PIT 10 FT.
CERTIFICATE OF ANAJLYSIS
RESULTS BY SAMPLIE
Lab ID: 9408026-02A Collected: 08/24/94 10:35:00
TEST
Volatile Organics
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
RESULT
U
U
u
1,1,2,2-Tetrachloroethane D
Te trachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
u
u
u
u 2000
Trichlorofluoromethane U
Vinyl Acetate
Vinyl Chloride
o-Xylene
D
D
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
ANILLYZED
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
%Recovery
101
94.7
95.8
METHOD/CAS#
SW-846, 8240
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
m
Sample ID: M-136,CEN. OF PIT lOFT.DUP Lab ID: 9408026-03A Collected: 08/24/94 10:35:00
TEST RESULT UNITS DETECTION ANikLYZED BY
LIQSIT
METH0D/CAS#
Cadmium
Chromium
Lead
0.12 ug/g
21.2 ug/g
26.9 ug/g
0.1 09/13/94 LVD
0.3 09/13/94 LVD
1.7 09/13/94 LVD
SW-846, 6010
SW-846, 6010
SW-846, 6010
Sample ID: M-136, OUTER EDGE 5 FT. Lab ID: 9408026-04A CoUected: 08/24/94 10:45:00
TEST RESULT UNITS DETECTION ANi^YZED BY
hIU.1T
METHOD/CAS#
Cadmium
Chromium
Lead
U ug/g
19.9 ug/g
44.9 ug/g
0.1 09/13/94 LVD
0.3 09/13/94 LVD
1.7 09/13/94 LVD
SW-846, 6010
SW-846, 6010
SW-846, 6010
• Page ff: 6
October 28, 1994 08:05 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-136, OUTER EDGE 5 FT. Lab ID: 9408026-04A CoUected: 08/24/94 10:45:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorometheme
Bromoform
Bromometheme
2~Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chl orome thane
Dibromochlorcmetheme
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trems-1,3 -Di chloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
22
870
400
350
140
U
U
D
J
D
U
D
D
U
D
J
U
D
U
U
D
D
D
D
U
D
U
D
D
D
D
U
U
U
U
D
J
J
J
U
D
12000
U
D
D
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
ANALYZED
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
%Recovery
101
90.8
95.6
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5 ^^
10061-02-6 ^P
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
Page#: 7
October 28, 1994 08:05 CERTIFICATE OF ANALYSIS
'• RESULTS BY SAMPIilE
Sample ID: M-136, OUTER EDGE SFT. DUP Lab ID: 9408026-05A CoUected: 08/24/94 10:45:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorometheme
Bromoform
Bromometheme
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropane
J^ 1,3 - Di chloropropene
IBKs -1,3- Dichlorpprppene
r^-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Tri chloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
110
920
390
410
160
760
U
D
D
J
U
D
U
D
U
U
J
D
U
J
U
D
U
D
U
D
U
D
D
D
U
D
U
U
U
D
U
U
J
J
J
D
27000
D
U
D
0
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
ANALYZED
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 6240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
%Recovery
100
91.3
95.1
METHOD/rAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
• Page ff: 8
October 28, 1994 08:05 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-136, OUTER EDGE 10 FT. Lab ID: 9408026-06A CoUected: 08/24/94 10:55:00
TEST
Cadmium
Chromium
Lead
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroe thane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexanone
trans-l,2-Dichloroethene
1,2-Dichloropropeme
ci s-1,3 -Di chloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2-Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Tri chlorofluorome theme
vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
0.25
23.0
179
D
U
U
2600
D
D
U
D
U
U
18000
U
D
3100
U
U
D
U
D
D
U
U
U
D
U
U
D
1600
U
D
U
D
2400
8700
5600
U
156000
D
D
U
2800
UNITS
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
1.7
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
1300
ANALYZED
09/13/94
09/13/94
09/13/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
BY
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAfl#
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1 ^^
75-34-3 ^P 107-06-2 ^^
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Page#:9
October 28, 1994 08:05 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLIE
Sample ID: M-136, OUTER EDGE 10 FT. Lab ID: 9408026-06A CoUected: 08/24/94 10:55:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Surrogate/Recovery Data For Volatile Organics 8240S
SW-846, 8240
Sxirrogate %Recovery
Toluene-d8 101
Bromofluorobenzene 89.4
l,2-Dichloroetheme-d4 95.0
Recovery Limits
81 TO 117
74 TO 121
70 TO 121
Sample ID: M-187, GRD 24 SURFACE Lab ID: 9408026-07A CoUected: 08/24/94 15:00:00
TEST
Perchlorate
Cadmium
Chromium
#
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloronethane
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
RESULT
U
U
15.5
13.8
0.39
D
U
U
D
U
n u D
D
XJ
D
U
D
D
D
U
U
U
U
U
U
D
U
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
4.7
0.1
0.3
1.7
0.2
0.026
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/23/94
09/13/94
09/13/94
09/13/94
09/13/94
10/20/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
BY
CRS
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
Page ff: 10
October 28, 1994 08:05 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-187, GRD 24 SURFACE Lab ID: 9408026-07A CoUected: 08/24/94 15:00:00
TEST
Volatile Organics
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
U
U
u u
u D
U
U
U
U
U
u 4 BJ
U
3 J
U
U
o
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
%Recovery
97.3
91.9
95.9
METHOD/CAS#
SW-846,
10061-01-
10061-02-
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
8240
5
6
.^M^..
#
Sample ID: M-187, GRD 24, 2 FT. Lab ID: 9408026-08A CoUected: 08/24/94 15:10:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
a
u
17.5
17.6
3.5
U
U
U
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
4.0
0.1
0.4
1.8
0.2
0.023
10
10
10/23/94
09/13/94
09/13/94
09/13/94
09/13/94
10/20/94
09/01/94
09/01/94
CRS
LVD
LVD
LVD
LVD
CRS
JMA
JMA
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
Page#: 11
October 28, 1994 08:05
Sample ID: M-187, GRD 24, 2 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9408026-08A CoUected: 08/24/94 15:10:00
TEST RESULT
volatile Organics
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
B romome thane
2'Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochlorometheme
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexanone
trems-1,2 -Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
^I^^Di chl orobenzene
I^BD i chl orobenzene
r^ Di chl orobenz ene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane 4
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
vinyl Chloride
o-Xylene
Surrogate
Surrogate
Toluene-d8
U
U
U
U
D
U
U
U
U
U
U
D
U
U
D
D
D
D
D
U
D
D
D
D
U
U
U
U
U
U
U
U
BJ
D
D
U
D
U
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/0:L/94
i/Recovery Data For Volatile Organic;
Bromofluorobenzene
1,2-Dichloroethane-d4
%Recovery
98.3
97.3
97.2
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
B 8240S
METHOD/CAS#
SW-846, 8240
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
• Page ff: 12
October 28, 1994 08:05 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-187, GRD 24, 5 FT. Lab ID: 9408026-09A CoUected: 08/24/94 15:30:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorome Chane
Bromofonn
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chlorofonn
Chloromethane
Dibromochloronethane
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Trichlorof luorcoietheme
Vinyl Acetate
D
D
17.8
17.5
U
D
U
U
U
U
U
D
U
U
D
a D
U
U
U
a
u
u
n u
u
u u
a
u
u
u
D
u 10
u
u D
U
U
4 BJ
U
U
U
U
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
5.0
0.2
0.4
1.9
0.2
1.5
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10/23/94
09/13/94
09/13/94
09/13/94
09/13/94
10/20/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
09/01/94
CRS
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SOP 314
SW-846, 6010
SW-846, 6010
SW-646, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
Page ff: 13
October 28, 1994 08:05 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-187, GRD 24, 5 FT. Lab ID: 9408026-09A CoUected: 08/24/94 15:30:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Vinyl Chloride
o-Xylene
D ug/Kg
O ug/Kg
Surrogate/Recovery Data
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
SW-846, 8240
10 09/01/94 JMA 75-01-4
10 09/01/94 JMA 95-47-6
For Volatile Organics 8240S
%Recovery Recovery Limits
99.1 81 TO 117
97.3 74 TO 121
97.4 70 TO 121
Sample ID: M-187, GRD 6 SURFACE Lab ID: 9408026-lOA CoUected: 08/24/94 16:05:00
TEST
Perchlorate
C^nlum
CKomlum
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromofonn
Bromometheme
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chlorofonn
Chlorometheme
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
RESULT
U
0.67
21.8
63.9
D
0.07
28
O
U
U
D
U
O
25
U
D
U
U
U
U
D
U
3 J
U
D
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
5.2
0.1
0.3
1.7
0.2
0.029
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/23/94
09/13/94
09/13/94
09/13/94
09/13/94
10/20/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
BY
CRS
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
Page ff: 14
October 28, 1994 08:05 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-187, GRD 6 SURFACE Lab ID: 9408026-lOA CoUected: 08/24/94 16:05:00
TEST
Volatile Organics
2-Hexanone
trems-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroetheme
Tr i chloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
3 J
U
D
D
D
U
D
U
D
D
U
U
U
U
D
13 B
D
8 J
U
U
D
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
%Recovery
95.3
91.8
100
METHOD/CAS#
SW-846, 8240
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6 ^^
#
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
Sample ID: M-187, GRD 6, 2 FT. Lab ID: 9408026-11A CoUected: 08/24/94 16:10:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercury
u
u
15.8
9.5
U
u
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
4.8
0.1
0.3
1.7
0.2
0.028
10/23/94
09/13/94
09/13/94
09/13/94
09/13/94
10/20/94
CRS
LVD
LVD
LVD
LVD
CRS
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
Page ff: 15
October 28, 1994 08:05
Sample ID: M-187, GRD 6, 2 FT.
CERTIFICATE OF ANALYSIS
^ RESULTS BY SAMPLE
Lab ID: 9408026-11A CoUected: 08/24/94 16:10:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Acetone U ug/Kg
Acrolein U ug/Kg
Acrylonitrile U ug/Kg
Benzene U ug/Kg
Bromodichloromethane U ug/Kg
Bromofonn D ug/Kg
Bromomethane U ug/Kg
2-Butemone U ug/Kg
Carbon disulfide D ug/Kg
Carbon tetrachloride D ug/Kg
Chlorobenzene D ug/Kg
Chloroethane D ug/Kg
2-Chloroethylvinyl ether D ug/Kg
Chlorofonn D ug/Kg
Chloromethane U ug/Kg
Dibromochloromethane U ug/Kg
1,1-Dichloroetheme U ug/Kg
1,2-Dichloroetheme D ug/Kg
1,1-Dichloroethene - D ug/Kg
2-Hexemone D ug/Kg
trans-1,2-Dichloroethene D ug/Kg
^2 -Dichloropropane D ug/Kg
Jl^^-l, 3-Dichloropropene D ug/Kg
^l^^ns-1,3-Dichloropropene D ug/Kg
1,2-Dichlorobenzene D ug/Kg
1,3-Dichlorobenzene D ug/Kg
1,4-Dichlorobenzene U ug/Kg
Ethylbenzene D ug/Kg
Methylene Chloride D ug/Kg
4-Methyl-2-Pentanone U ug/Kg
Styrene D ug/Kg
1,1,2,2-Tetrachloroethane U ug/Kg
Tetrachloroethene U ug/Kg
Toluene U ug/Kg
1,1,1-Trichloroetheme 9.7 BJ ug/Kg
1,1,2-Trichloroetheme D ug/Kg
Trichloroethene U ug/Kg
Trichlorofluoromethane U ug/Kg
vinyl Acetate XJ ug/Kg
Vinyl Chloride U ug/Kg
o-Xylene U ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate %Recovery
Toluene-d8 100
Bromofluorobenzene 96.6
1,2-Dichloroetheme-d4 101
Recovery Limits
81 TO 117
74 TO 121
70 TO 121
Page #: 16
October 28, 1994 08:05 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-187, GRD 6, 2 FT. DUP. Lab ID: 9408026-12A CoUected: 08/24/94 16:10:00
TEST RESULT
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochlorometheme
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
cis-l,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane 4
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
U
D
D
D
U
D
U
D
U
n D
U
D
U
D
D
D
D
U
D
D
D
n D
D
D
U
O
D
U
D
U
U
D
BJ
D
D
D
D
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
%Recovery
99.6
99.8
99.2
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5 J^
10061-02-6 ^V
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
Page ff: 17
October 28, 1994 08:05 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-187, GRD 6, 5 FT. Lab ID: 9408026-13A CoUected: 08/24/94 16:20:00
TEST RESULT UNITS DETECTION ANJLLYZED BY
LIMIT
METHOD/CAS#
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
jC^bon disulfide
J^^^bon tetrachloride
^l^r orobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochlorometheme
1,1-Dichloroetheme
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1.2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
u
0.13
15.7
7.7
D
U
U
U
U
U
U
U
U
D
U
U
U
D
D
U
U
U
D
U
D
U
U
U
U
U
U
u u u D
D
D
U
D
D
6 BJ
D
U
U
D
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
4.2
0.1
0.4
1.8
0.2
0.020
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10/23/94
09/13/94
09/13/94
09/13/94
09/13/94
10/20/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
CRS
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SOP 314
SW-846, 6010
SW-e46, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
Page ff: 18
October 28, 1994 08:05 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-187, GRD 6, 5 FT. Lab ID: 9408026-13A CoUected: 08/24/94 16:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
vinyl Chloride
o-Xylene
0 ug/Kg
U ug/Kg
Surrogate/Recovery Data
Surrogate
Toluene-d8
Bromofluorobenzene
1,2 -Dichloroethane-d4
SW-846,
10 09/06/94 JMA 75-01-4
10 09/06/94 JMA 95-47-6
For Volatile Organics 8240S
%Recovery Recovery Limits
99.8 81 TO 117
98.7 74 TO 121
101 70 TO 121
8240
Sample ID: M-187, GRD 4 SURFACE Lab ID: 9408026-14A CoUected: 08/24/94 15:35:00
TEST
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromofonn
Bromometheme
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorcmetheme
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
RESULT
o
0.13
21.7
45.4
1.67
U
13
U
D
D
U
U
U
D
U
D
U
U
D
D
U
U
D
D
D
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
vg/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
4.2
0.1
0.3
1.7
0.2
0.029
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/24/94
09/13/94
09/13/94
09/13/94
09/13/94
10/20/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
BY
CRS
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SOP 314
SW-846, 6010 g^
SW-846, 6010 ^^
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
Page ff: 19
October 28, 1994 08:05
Sample ID: M-187, GRD 4 SURFACE
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPUE
Lab ID: 9408026-14A CoUected: 08/24/94 15:35:00
TEST
Volatile Orgemlcs
2-Hexemone
trems-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2 -Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Te t rachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Tri chlorofluorometheme
Vinyl Acetate
Vinyl Chloride
i^Xylene
RESULT
D
D
U
D
D
D
D
D
D
D
D
D
D
D
D
7 BJ
U
4 J
D
U
D
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANlkLYZED
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
"^ Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dic :hloroetha ine-d4
%Recovery
99.2
98.6
101
METHOD/CAS#
SW-846, 8240
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
Sample ID: M-187, GRD 4, 2 FT. Lab ID: 9408026-15A CoUected: 08/24/94 15:40:00
TEST RESULT UNITS DETECTION ANiLLYZED BY
LIMIT
METHOD/CAS#
Perchlorate
Cadmium
Chrcmluffl
Lead
Silver
Mercury
u
u
17.3
14.2
U
U
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
4.8
0.1
0.3
1.6
0.2
0.022
10/24/94
09/13/94
09/13/94
09/13/94
09/13/94
10/20/94
CRS
LVD
LVD
LVD
LVD
CRS
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
Page ff: 20
October 28, 1994 08:05 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-187, GRD 4, 2 FT. Lab ID: 9408026-15A CoUected: 08/24/94 15:40:00
TEST RESULT
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromofonn
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibramochlorome theme
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trems-1,2-Dichloroethene
1,2-Dichlorpprppeme
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3 -Dicdilorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2-Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane 5
1,1,2-Trichloroethane
Tri chloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
U
D
U
D
D
D
D
U
D
D
D
D
U
D
U
U
U
U
U
D
U
U
D
U
U
D
U
D
D
D
U
D
n D
BJ
U
U
D
U
D
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
Surrogate/Recovery Data For Volatile Organic
Surrogate
Toluene-d8
Bromofluorobenzene
1,2 -Di chloroetheme-d4
%Racovery
99.5
98.4
99.7
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
s 8240S
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5 ^^
10061-02-6 ^V
95-50-1 ^
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
Page ff: 21
October 28, 1994 08:05
Sample ID: M-187, GRD 4, 5 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLIE
Lab ED: 9408026-16A CoUected: 08/24/94 15:50:00
TEST
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromofonn
Bromometheme
2-Butemone
C^bon disulfide
aW3on tetrachloride
fluorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorcmetheme
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1 -Trichloroetheme
1,1,2-Trichloroetheme
Trichloroethene
Trichlorof luorcanethane
Vinyl Acetate
RESULT
D
U
18.4
13.6
D
U
D
U
U
D
D
U
U
D
D
D
U
U
U
D
D
D
U
D
U
D
U
U
D
U
D
U
U
O
U
U
U
D
D
U
5 BJ
D
D
U
U
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
4.7
0.2
0.4
1.9
0.2
0.031
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/:>4/94
09/13/94
09/3.3/94
09/13/94
09/13/94
10/20/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
BY
CRS
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
Page ff: 22
October 28, 1994 08:05 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-187, GRD 4,5 FT. Lab ID: 9408026-16A CoUected: 08/24/94 15:50:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
vinyl Chloride
O-Xylene
U ug/Kg
D ug/Kg
Surrogate/Recovery Data
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
SW-846, 8240
10 09/06/94 JMA 75-01-4
10 09/06/94 JMA 95-47-6
For Volatile Organics 8240S
%Recovery Recovery Limits
99.3 81 TO 117
98.9 74 TO 121
101 70 TO 121
Page ff: 23
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but gieater than zero. (e.g. l.U wiith a detection liniit of 5.0)
B This flag is used when an analyte is found in the blanii: as weU as the sample.
E Estimated value. Result was outside of the caUbration ninge but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ENVIRONMENTAL LAB WORK REQUEST
10^ ^:^
TfflOKOL ENVIRONMENTAL LABORATORY LWR No. E10625
^ F /U?/J^f^
COSTCBOSn
(^/?.
WORKOROeR
/^"/^/y Zl/hJi^ 94
ORGANIZATION
Bl^U ^M/nP^ ^Of^
REPORT RES11.TS TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
V
V
SAMPLE DATE TVPE
y
LOCATION
•Stt^/UV ^^^
TIME TEST
"Jlo Cd,Cr,/l.j ,Pij '/^o/Q
REMARKS
2iA ? »/ T'l P/Uf/oVraiM^iiU /^c/,Cr,^fl, Ph -6>^>'l^
\y zaAu-
^
Ly /I &^40 /I
\y
*s,tx}MO ^4e /I ty / ( ^^o ll
\y y^ stv mo 6yf-t> Vi/p /SJ*^i4 £'± tf /f <=f^O /(
^^SJ±J4J0^ /I /I /O/O /i
\y
.y^^tjU/klP ^4&
/I ty /I m-^ 1/
y». SU>/UU £>4&
(U^r9 /oft
)/'• •So/My) Cf^ei m 1/ t^' /I /0¥o /I
'I /£>S^ //
L. Zn^ •BtoAJi. fS^i7. ^/-> ^' // //^r" //
y\\.Siuitf\o o4e fl f/ //lO //
CHAIN OF CUSTODY
RELINQUISHED BY
^5 ^
DATE
7l/ftJ^f/
TIME
/3'/^
RECEIVED BY
nmniM
z in iZ; V-^-
DATE
•^-Z^iUzl^i
TIME
///-T^
/
FOR LABORATORY USE ONLY
DATE OOMFLETED
#
DATE REPORTED
October 19, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER, MIS 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham aty, Ut 84302-0707
Analytical Labs MIS 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order jj^ 9408023 Sample and Test Code Identification
Lab ID:
OIA
Lab ID:
02A -
Lab ID: 03A
Lab ID:
04A
Lab ID:
^5A
Lab ID:
06A
LabTDi
07A
Lab ID:
08A
UbID:
09A
"-
Sample ID:
T-l PHOTO.PROC. SEPTIC TMK
-
Sample ID:
T-l PHOTO, GRID 9, 5 FT.
Sample ID:
T-l PHOTO, GRID 9. 10 FT.
Samole ID:
T-l PHOTO, GRID 14, 5 FT.
Sample ID:
T-l PHOTO.ORD 14,5 FT. DUP
T-l pkOTO.^RID 14, 10 FT.
Sample ID:
T-l PHOTO, GRID 19, 5 FT.
Sample ID:
T-l P^arO,"ORID 19, 10 FT.
Sample ID:
T-l PHOTO, GRID 32, 5 FT.
Test Codes and Names
CD_AE2 Cadmium
CR~AE2 Chromium
PB~AE2 Lead
AO_AE2 SUver
Test Codes and Names
CD_AE2 Cadmium
CR~AE2 Chromium
PB~AE2 Lead
AG_AE2 Silver
Test Codes and Names
CD AE2 Cadmium
CR~AE2 Chromium
VB'AEl Lead
AG_AE2 SUver
Test Codes and Names
CD AE2 Cadmium
CR AE2 Chromium
PB~AE2 Lead
AOlAE2 SUver
Test Codes and Names
CD_AE2 Cadmium
CR~AE2 Chromium
PB~AE2 Lead
A0~AE2 SUver
Test Codes and Names
CD_AE2 Cadmium
CR~AE2 Chromium
PB"AE2 Lead
AG1AE2 SUver
Test Code.<J and Namfts
CD_AE2 Cadmium
CR-AEZ Chromium
PB~AE2 Lead
ASTjja SUver
Test Codes and Names
CD_AE2 Cadmium
CR~AEi Chromium
PB'AE2 Lead
AG_AE2 SUver
Test Codes and Names
CD AE2 Cadmium
CR"AE2 Chromium
PB~AE2 Lead
AOlAEi SUver
Page r.l Of 6^
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Work Order J» 9408023 Sample and Test Code Identification
€H bID: Sample ID:
lOA T-l P110TO,GRD32,SFT,RNS.BL
Lab ID: Sample ID:
llA T-l PHOTO, GRID 32, 10 FT.
Lab ID: Sample ID:
OIB T-l PHOTO.PROC. SEPTIC TMK
Test Codes and Names
CD_AE2 Cadmium
CR AE2 Chromium
PB~AE2 Lead
Aa_AE2 Silver
Test Codes and Names
CD_AE2 Cadmium
CR_AE2 Chromium
PB_AE2 Lead
AG_AE2 Silver
Test Codes and Names
AG AE2 SUver
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010 Method
SW-846, 6010
Workorder Cnmnment*;
Report: NITRIC ACID WAS USED FOR THE SILVER EXTRACTION
ON SAMPLE #01B.
•
Z^.^27*X-
Cerl.ifi( S^
• Page #:2
Tlus is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: T-l PHOTO,PROC. SEPTIC TNK Lab ID: 9408023-OlA CoUected: 08/23/94 09:20:00
TEST RESULT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Cadmium
Chromium
Lead
Silver
2.9
636
44.9
84.3
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.3
0.2
09/13/94
09/13/94
09/13/94
09/13/94
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
Sample ID: T-l PHOTO, GRID 9, 5 FT. Lab ID: 9408023-02A CoUected: 08/23/94 08:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Cadmium
Chromium
Lead
Silver
u
10.2
6.0
3.3
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.8
0.2
09/13/94
09/13/94
09/13/94
09/13/94
liVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
Sample ID: T-l PHOTO, GRID 9, 10 FT. Lab ID: 9408023-03A CoUected: 08/23/94 08:40:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Cadmium
Chromium
Lead
Silver
u
14.3
5.3
2.8
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.7
0.2
09/13/94
09/13/94
09/13/94
09/13/94
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
Page #: 3
October 19, 1994 13:41 CERTIFICATE OF AIS AJLYSIS
RESULTS BY SAMPUE
Sample ID: T-l PHOTO, GRID 14, 5 FT. Lab ID: 9408023-04A CoUected: 08/23/94 09:50:00
TEST RESULT UNITS DETECTION AltTJiliYZED BY
LIMIT
METHOD/CAS#
Cadmium
Chromium
Lead
Silver
u
10.0
5.8
1.6
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.5
0.2
09/13/94
09/13/94
09/13/94
09/13/94
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
Sample ID: T-l PHOTO.GRD 14,5 FT. DUP Lab ID: 9408023-05A CoUected: 08/23/94 09:50:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Cadmium
Chromium
Lead
F/er
u
12.1
5.7
1.2
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.6
0.2
09/13/94
09/13/94
09/13/94
09/13/94
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
Sample ID: T-l PHOTO, GRID 14, 10 FT. Lab ID: 9408023-06A CoUected: 08/23/94 10:10:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Cadmium
Chromium
Lead
Silver
u
13.2
6.4
1.5
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.6
0.2
09/13/94
09/13/94
09/13/94
09/13/94
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
Sample ID: T-l PHOTO, GRID 19, 5 FT. Lab ID: 9408023-07A CoUected: 08/23/94 10:25:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Cadmium
•
ug/g 0.1 09/13/94 LVD SW-846, 6010
Page ff: 4
October 19, 1994 13:41 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: T-I PHOTO, GRID 19, 5 FT. Lab ID: 9408023-07A CoUected: 08/23/94 10:25:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Chromium
Lead
Silver
11.7
8.2
0.2
ug/g
ug/g
ug/g
0.3
1.7
0.2
09/13/94
09/13/94
09/13/94
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
6010
6010
6010
Sample ID: T-l PHOTO, GRID 19, 10 FT. Lab ID: 9408023-08A CoUected: 08/23/94 10:40:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Cadmium
Cliromium
Lead
Silver
D
14.0
8.5
1.0
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.6
0.2
09/13/94
09/13/94
09/13/94
09/13/94
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
Sample ID: T-l PHOTO, GRID 32, 5 FT. Lab ID: 9408023-09A CoUected: 08/23/94 10:55:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Cadmium
Chromium
Lead
Silver
0.1
2.3
3.7
U
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.5
0.2
09/13/94
09/13/94
09/13/94
09/13/94
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
Sample ID: T-l PHOTO,GRD32,5FT,RNS.BL Lab ID: 9408023-lOA CoUected: 08/23/94 11:05:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Cadmium
Chromium
u
D
ug/L
ug/L
2
5
09/13/94
09/13/94
LVD
LVD
SW-846,
SW-846,
6010
6010
Page ff: 5
October 19, 1994 13:41 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: T-l PHOTO,GRD32,5FT,RNS.BL Lab ID: 9408023-lOA CoUected: 08/23/94 11:05:00
TEST RESULT UNITS DETECTION AISTALYZED BY
LIMIT
METHOD/CAS#
Lead
Silver
U
17.4
ug/L
ug/L
25 09/13/94 LVD SW-846, 6010
3 09/13/94 LVD SW-846, 6010
Sample ID: T-l PHOTO, GRID 32, 10 FT. Lab ID: 9408023-11A CoUected: 08/23/94 11:10:00
TEST RESULT UNITS DETECTION Al^ALYZED BY
LIMIT
METHOD/CAS#
Cadmliui
Chromium
Lead
Silver
D
13.8
4.9
U
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.7
0.2
09/13/94
09/13/94
09/13/94
09/13/94
LVD
LVD
LVD
LVD
SW-e46, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
a pie ID: T-l PHOTO.PROC. SEPTIC TNK Lab ID: 9408023-OlB CoUected: 08/23/94 09:20:00
TEST RESULT UNITS DETECTION Al^ALYZED BY
LIMIT
METHOD/CAS#
Silver 4500 ug/g 0.3 10/12/94 LVD SW-846, 6010
• Page ff: 6
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1.IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ENVIRONMENTAL LAB WORK REQIFEST Hf}S/i>7
TfflOKOL ENVIRONMENTAL LABORATORY LWR No. E10628
A 1
/{ f I^J/^i^iCeR^
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DATE
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ORGANIZATION MAIL STOP REPORT RESin.TS TO:
gMUlRO 0Jifeg--ZOf E ^
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE ^-TYPE
'ly
LOCATION
XA'197 Dry.L».. s^^,
TIME TEST
7^4 f~
¥ l/oc- SZ4d
REMARKS
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FOR LABORATORY USE ONLY
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HELEN WARD, MS 301
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SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TME TEST
i^
KEMABKS
^07 h. ^^^
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SnJNQinSHED BY DATE TIME BECOVESBY DATE TIME
747/1 V' f£ ^^ /////y/A.,.JrS-Zr' 9¥ /^//^
FOR LABORATORY USE ONLY
MnoOMFinBD nATSBBPOKIBI HCNAIVBK
October 28, 1994
•
CERTIFICATE OF ANA1.YSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward
MIS 301
A.F. WALKER, MIS 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
PO. Box 707
Brigham City, Ut 84302-0707
Analytical Labs MIS 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order # 9408029
Lab IP:
OIA
Lab IP:
02A
Lab IP:
03A
Lab IP:
04A
Lab ID:
~O3A
Lab ID:
06A
Lab ID:
07A
Sample ID:
M-187, GRD 55 SURFACE
Sample and Test Code Identification
Test Codes and Names
Sample ID:
M-187,QD 55 SURF. RNS BLNK
Sample ID:
M-187, GRD 55, 2 FT.
Sample ID:
M-187, ORD 55, 5 FT.
Sample ID:
187, ORD 77 SURFACE M
Sample TD:
M-187, C QRD 77, 2 FT.
Sample ID:
M-187, ORD 77, 5 FT.
CL04
CD AE2
CR AE2
PB AE2
AG AE2
HO CV2
824CS
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercuiy
Volatile Organics
Test Codes and Names
8240 Volatile Orsanica
Test Codes and Names
CL04
CD AE2
CR AE2
PB AE2
AO AE2
HO CV2
8240S
Perchlorate
Cadinium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
CL04
CD AE2
CR AE2
PB AE2
AG AE2
HO CV2
824QS
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Orsanics
Test Codes and Names
CL04
CD AE2
CR AE2
PB AE2
AO AE2
HG CV2
8240s
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Orgamcs
Test Codes and Names
CL04
CD AE2
CR AE2
PB AE2
AG"AE2
HO CV2
8240s
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercuiy
Volatile Organics
Test Codes and Names
CL04
CD_AE2
CR AE2
PB~AE2
Perchlorate
Cadmium
Chromium
Lead
Method
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SW-846, 8240
Method
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240 Method
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240 Method
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
Page #:1 of / ^
Lab ID:
IIA
WorkOrder^ 9408029
Lab ID: Sample ID:
~57A M-J187, ORD 77,5 FT.
Lab ID: Sample ID:
08A M-187, QRD 77, 5 FT. DUP.
Lab ID: Sample ID:
09A M-187, ORD 88 StniFACE
Sample and Test Code Identification
Lab ID: Sample ID:
lOA M-187, ORD 88, 2 FT.
Sampl
M-187,
lelD:
GRD 88. 5 FT.
Lab ID:
IiA
S^pleTO:
M-187,GRD 88,5Fr. RNS BLNK
Test Codes and Names
AG AE2 SUver
HG"CV2 Mercury
8240s VolatUe Organics
Test Codes and Names
CL04 Perchlorate
CD_AE2 Cadmium
CR"'AE2 Chromium
PB AE2 Lead
AG'AE2 SUver
HO~CV2 Mercuiy
Test Codes and Names
CL04 Perchlorate
CD AE2 Cadinium
CR~AE2 Chromium
PB~AE2 Lead
AG"AE2 SUver
HG CV2 Mereury
8240s VolatUe Oiganics
Test Codes and Names
CL04 Perchlorate
CD_AE2 Cadmium
CR AE2 Chromium
PB AE2 Lead
AO AE2 SUver
HO CV2 Mercuiy
8740s VolatUe Organics
Test Codes and Names
CL04 Petchlonte
CD_AE2 Cadmium
CR~AE2 Chromium
PB~AE2 Lead
ACTAEZ SUver
H0"CV2 Mercuiy
8240s VoUtUe Oiganics
Test Codes and Names
CL04 Perchlorate
CD_AE2 Cadmium
CR~AE2 Chromium
PB"AE2 Lead
AG AE2 SUver
HGICV2 Mercuty
Workorder Comnients
Method
SW-846, 6010
SW-846. 7471
SW-846, 8240
Method
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
Method
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
Page #:2
This is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: M-187, GRD 55 SURFACE Lab ID: 9408029-OlA CoUected: 08/25/94 12:45:00
TEST
Perchlorate
Cadmium
Chromium
Laad
Sliver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromofonn
Bromome thsine
2-Butanone
Jl^kbon disulfide
V^Voon tetrachloride
CTU orobenz ene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheme
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexanone
trems-l,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluorometheme
RESULT
U
0.36
12.4
18.4
U
U
73
U
U
U
D
U
D
39
D
U
U
U
D
U
U
D
U
U
D
27
D
D
U
U
U
D
D
D
U
4 J
D
D
U
U
6 BJ
U
1 J
U
TJNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
4.8
0.1
0.3
1.7
0.2
0.026
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANJ!JiYZED
10/24/94
09/20/94
09/20/94
09/20/94
09/:20/94
10/20/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
O9/0'6/94
09/06/94
BY
CRS
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
# Page ff: 3
October 28, 1994 08:31 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sstmple ID: M-187, GRD 55 SURFACE Lab ID: 9408029-OlA CoUected: 08/25/94 12:45:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
v^olatile Organics
Vinyl Acetate
Vinyl Chloride
o-Xylene
U ug/Kg
U ug/Kg
U ug/Kg
Surrogate/Recovery Data
Surrogate
Toluene-d8
Bromofluorobenzene
1,2 -Dichloroetheme-d4
SW-846, 8240
10 09/06/94 JMA 108-05-4
10 09/06/94 JMA 75-01-4
10 09/06/94 JMA 95-47-6
For Volatile Organics 8240S
%Recovery Recovery Limits
88.3 81 TO 117
85.4 74 TO 121
101 70 TO 121
Sample ID: M-187,GD 55 SURF. RNS BLNK Lab ID: 9408029-02A CoUected: 08/25/94 12:40:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2-Pentemone
Styrene
RESin:.T
250
U
O
U
U
O
u 53
D
U
D
U
U
O
U
U
D
U
0
6.1 J
U
U
U
D
U
U
D
U
D
D
D
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-84e, 8240
67-64-1 ^^
107-02-8 ^^
107-13-1 ^^
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
Page ff: 4
October 28, 1994 08:31 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-187,GD 55 SURF. RNS BLNK Lab ID: 9408029-02A CoUected: 08/25/94 12:40:00
TEST RESULT
Volatile Organics
1,1,2,2-Tetrachloroetheme D
Tetrachloroethene D
Toluene U
1,1,1-Trichloroethane 4.3 BJ
1,1,2-Trichloroethane U
Trichloroethene D
Trichlorofluoromethane U
Vinyl Acetate U
Vinyl Chloride U
o-Xylene D
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
A](TJ)IiYZRD
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
%Recovery
99.9
102
100
METHOD/CAS#
SW-846, 8240
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
88
86
76
TO 110
TO 115
TO 114
ample ID: M-187, GRD 55, 2 FT.
TKT
Lab ID: 9408029-03A CoUected: 08/25/94 12:53:00
RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromofonn
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
D
0.50
16.5
11.5
U
D
U
U
U
U
U
U
D
U
U
D
U
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
4.2
0.1
0.3
1.7
0.2
0.026
10
10
10
10
10
10
10
10
10
10
10
10/24/94
09/20/94
09/20/94
09/20/94
09/20/94
10/20/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
CRS
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
Page ff: 5
October 28, 1994 08:31 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-187, GRD 55, 2 FT. Lab ID: 9408029-03A CoUected: 08/25/94 12:53:00
TEST
Volatile Organics
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2-Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
vinyl Chloride
o-Xylene
RESULT
U
U
D
U
U
u D
D
D
U
D
U
U
D
U
U
U
D
U
D
U
a u 7 J
D
D
U
D
U
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
%Recovsry
99.3
97.9
99.7
METHOD/CAS#
SW-846, 8240
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3 ^^
71-55-6 ^m
79-00-5 ^
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
Sample ID: M-187, GRD 55, 5 FT. Lab ID: 9408029-04A CoUected: 08/25/94 12:56:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Perchlorate
Cadmium
D
D
ug/g
ug/g
4.6
0.1
10/24/94
09/20/94
CRS
LVD
SOP 314
SW-846, 6010
Page ff: 6
October 28, 1994 08:31
Sample ID: M-187, GRD 55, 5 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLIE
Lab ID: 9408029-04A CoUected: 08/25/94 12:56:00
TEST
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2 -Chloroethylvinyl ether
JjtaLproform
I^Birome theme
sKromochlorome thane
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexemone
trems-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluorometheme
vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
17.8
10.4
D
U
U
U
D
U
U
U
U
D
U
D
D
U
U
U
U
D
U
D
U
D
U
U
U
U
U
U
U
U
D
U
U
U
U
U
7 J
D
D
U
U
D
U
UNITS
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.4
1.8
0.2
0.029
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
A](TilIiYZED
09/20/94
09/:20/94
09/;20/94
10/20/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
09/06/94
BY
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Page ff: 7
October 28, 1994 08:31 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-187, GRD 55, 5 FT. Lab ID: 9408029-04A CoUected: 08/25/94 12:56:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics SW-846, 8240
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate %Recov0ry
Toluene-d8 98.5
Bromofluorobenzene 99.1
l,2-Dichloroetheme-d4 101
Recovery Limits
81 TO 117
74 TO 121
70 TO 121
Sample ID: M-187, GRD 77 SURFACE Lab ID: 9408029-05A CoUected: 08/25/94 13:00:00
TEST
Perchlorate
Cadmium
Chromium
Lead
Silver
Mdrcuzy
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene -
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane -
2-Chloroethylvinyl ether
Chloroform
Chlorometheme .
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichlorqprppane
RESULT
U
0.47
16.1
22.5
D
U
34
D
U
U
U
D
U
22
D
D
U
O
U
U
U
D
U
U
U
D
U
U
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
4.6
0.1
0.3
1.7
0.2
0.027
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/24/94
09/20/94
09/20/94
09/20/94
09/20/94
10/20/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
BY
CRS
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010 ^P
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
Page ff: 8
October 28, 1994 08:31 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-187, GRD 77 SURFACE Lab ID: 9408029-05A CoUected: 08/25/94 13:00:00
TEST
Volatile Organics
RESULT
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Tri chlorofluorometheme
vinyl Acetate
Vinyl Chloride
o-Xylene
m
1^
-
D
D
U
U
D
U
36
U
u
D
U
U
10
U
2 J
D
V
U
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMTT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
%Recovery
95.3
88.9
105
METHOD/CAS#
SW-846, 8240
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
Sample ID: M-187, GRD 77, 2 FT. Lab ID: 9408029-06A CoUected: 08/25/94 13:05:00
TEST RESULT UNITS DETECTION ANAILYZED BY
LIMIT
METHOD/CAS#
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
u
0.12
17,1
10.2
D
U
U
D
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
4.8
0.1
0.3
1.7
0.2
0.027
10
10
10/24/94
09/20/94
09/20/94
09/20/94
09/20/94
10/20/94
09/07/94
09/07/94
CRS
LVD
LVD
LVD
LVD
CRS
JMA
JMA
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
Page ff: 9
October 28, 1994 08:31 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-187, GRD 77, 2 FT. Lab ID: 9408029-06A CoUected: 08/25/94 13:05:00
TEST RESULT
Volatile Organics
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibramochlorome theme
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trems-1,2-Dichloroethene
1,2-Dichloropropane
cis-l,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2-Pentanone . .
Styrene -
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Tri chlorofluorometheme
Vinyl Acetate -
Vinyl Chloride
o-Xylene
U
U
D
U
U
10
U
U
V
D
D
U
D
D
U
U
D
U
U
U
D
U
D
U
D
U
3 J
D
U
U
D
D
4 J
U
D
D
U
D
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
Surrogate/Recovery Data For Volatile Organic
Surrogate
- Toluene-d8
Bromofluorobenzene
1,2 -Dichloroethane-d4
%Racovery
100
97.5
105
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
s 8240S
METHOD/CAS#
SW-846, 8240
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6 ^
95-50-1 ^^
541-73-1 ^^
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
Page ff: 10
October 28, 1994 : 08:31
•
Sample ID: M-187, GRD 77, 5 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9408029-07A CoUected: 08/25/94 13:15:00
TEST
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi ch1orometheme
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
JBbon tetrachloride
fluorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochloronetheme
1,1-Dichloroethane
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexemone~
trans-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride -
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
RESULT
D
U
14.8
12.5
U
D
D
U
U
D
U
U
D
11
U
U
U
U
O
D
U
D
D
D
n U
D
D
D
U
D
D
D
U
U
U
U
D
D
U
5 J
U
U
U
U
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.1
0.3
1.7
0.2
0.028
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANJiJiYZED
10/20/94
09/20/94
09/20/94
09/20/94
09/20/94
10/20/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
BY
CRS
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-G0-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
Page#: 11
October 28, 1994 08:31 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-187, GRD 77, 5 FT. Lab ID: 9408029-07A CoUected: 08/25/94 13:15:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
vinyl Chloride
o-Xylene
D ug/Kg
U ug/Kg
Surrogate/Recovery Data
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
SW-846, 8240
10 09/07/94 JMA 75-01-4
10 09/07/94 JMA 95-47-6
For Volatile Organics 8240S
%Recovery Recovery Limits
101 81 TO 117
98.9 74 TO 121
107 70 TO 121
Sample ID: M-187, GRD 77, 5 FT. DUP. Lab ID: 9408029-08A CoUected: 08/25/94 13:15:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercury
D
D
16.7
13.1
D
D
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
3.8
0.1
0.3
1.6
0.2
0.025
10/24/94
09/20/94
09/20/94
09/20/94
09/20/94
10/20/94
CRS
LVD
LVD
LVD
LVD
CRS
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
Sample ID: M-187, GRD 88 SURFACE Lab ID: 94O8029-09A CoUected: 08/25/94 13:25:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Perchlorate
Cadmium
Chromium
Lead
Silver
u
0.45
18.0
19.1
D
ug/g
ug/g
ug/g
ug/g
ug/g
4.3
0.1
0.3
1.6
0.2
10/24/94
09/20/94
09/20/94
09/20/94
09/20/94
CRS
LVD
LVD
LVD
LVD
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Page ff: 12
October 28, 1994 08:31
Sample ID: M-187, GRD 88 SURFACE
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9408029-09A CoUected: 08/25/94 13:25:00
TEST - RESULT
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromoform
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
^^exanone
|B^a8 -1,2-Dichloroethene
^IBI-Dichloropropane
ci s-1,3 -Di chloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4 -Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
vinyl Chloride
o-Xylene
U
27
U
U
U
D
D
U
25
U
D
U
U
U
n U
U
U
U
U
u
u u D
D
D
D
U
U
2 J
U
U
U
U
D
50
U
U
U
U
D
D
UNITS
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.024
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
KHMiYZED
10/20/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
BY
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
:—' _ Bromofluorobenzene
- : --. 1,2-Dichloroetheme-d4
%Recovery
96.4
91.2
103
METHOD/CAfl#
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
Page ff: 13
October 28, 1994 08:31
Sample ID: M-187, GRD 88,2 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9408029-lOA CoUected: 08/25/94 13:35:00
TEST
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromoform
Bromometheme
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibramochlorome theme
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trems-1,2-Dichloroethene
1,2-Dichlorqprppane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4 -Mfethyl-2-Pentemone_
Styrene
1,1,2,2 -Tetrachloroetheme
Te trachloroe thene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
vinyl Acetate
RESX7LT
D
a
18.5
11.4
U
U
D
U
U
D
U
U
D
14
U
D
U
U
D
U
U
n D
o u
u D
D
D
D
U
D
D
U
D
U
D
U
D
U
55
U
u u D
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
4.4
0.1
0.4
1.8
0.2
0.026
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/24/94
09/20/94
09/20/94
09/20/94
09/20/94
10/20/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
BY
CRS
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAfl#
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0 ^_.
56-23-5 ^^
108-90-7 ^P'
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
Page ff: 14
October 28, 1994 08:31 CERTIFICATE OF ANAJLYSIS
RESULTS BY SAMPLE
Sample ID: M-187, GRD 88, 2 FT. Lab ID: 9408029-lOA CoUected: 08/25/94 13:35:00
TEST RESULT UNITS DETECTION ANJkLYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Vinyl Chloride
o-Xylene
D ug/Kg
D ug/Kg
Surrogate/Recovery Data
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
SW-846, 8240
10 09/07/94 JMA 75-01-4
10 09/07/94 JMA 95-47-6
For Volatile Organics 8240S
%Recovery Recovery Limits
98.9 81 TO 117
96.9 74 TO 121
103 70 TO 121
Sample ID: M-187, GRD 88, 5 FT. Lab ID: 9408029-llA CoUected: 08/25/94 13:40:00
TEST
Perchlorate
^n^^bniuxn
^^nr^unT \iin ~
Lead
Silver
Mercury '....~~'i:
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromoform
Bromometheme j" -
2-Butanone " - :
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform :.z:r-
Chloromethane M.
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
RESULT
D
0.83
14.7
11.3
D
D
D
D
D
U
D
U
U
11
D
D
D
D
U
U
U
U
U
U
U
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
4.8
0.1
0.3
1.7
0.2
0.022
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/24/94
09/20/94
09/:J0/94
09/20/94
09/20/94
10/20/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
BY
CRS
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
• Page ff: 15
October 28, 1994 08:31 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-187, GRD 88, 5 FT. Lab ID: 9408029-llA CoUected: 08/25/94 13:40:00
TEST
Volatile Organics
2-Hexemone
trems-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-l,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Tri chlorofluorcmethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
D
U
U
U
U
U
D
U
D
V
D
U
U
U
U
16
D
U
n U
U
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
09/07/94
Surrogate/Recovery Data For Volatile Organic
Surrogate
Toluene -d8
Bromofluorobenzene
- "' 1,2-Dic iilor oetha ine-d4
^Recovery
101
98.7
103
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
s 8240S
METHOD/CAS#
SW-846, 8240
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6 ^^
#
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
Sample ID: M-187,GRD 88,5FT. RNS BLNK Lab ID: 9408029-12A CoUected: 08/25/94 14:05:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Perchlorate
Cadmium
Chromium
Lead
Silver
Mercury
u
D
U
U
U
U
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
0.10
0,2
0.5
2.5
0.3
0.15
10/24/94
09/20/94
09/20/94
09/20/94
09/20/94
10/20/94
CRS
LVD
LVD
LVD
LVD
CRS
SOP 314
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
Page ff: 16
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification cdteria but th<; result is less than the specified
detection limit but greater than zero. (e.g. 1. IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blanlc as weU as the sample.
E Estimated value. Result was outside of the CEiUbration cinge but within the linear
range ofthe instniment.
BDL Indicates an analyte which was below the detection Umits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the ispecified limits.
m
ENVIRONMENTAL LAB WORK REQUEST ^^^ f ^^?
W'^'- TfflOKOL ENVraOPflVlENTAL LABORATORY
FROM: .
ORGANIZATION
EXTENSION
MAIL STOP
\M/iO
LWR No. E10629
WORK ORDER DATE
</' 7- 9/-
Rn>ORT RESIJLTIi TO:
HELEN WARD, MS 301
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LOCATION
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REMARKS
C'.*r CA ^*.^'
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CHAIN OF CUSTODY
REUNQUISHED BY
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DATE
9-7-^
TIME
/S^IT
RECEIVED BY
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DATE
—^^-7-^^
TIME
//^^
FOR LABORATORY USE ONLY
DATE CX)MFLEm>
#
DATE REPORTED SIGNATURE
ENVIRONMENTAL LAB WORK REQUEST f^^J
THIOKOL ENVIRONMENTAL LABORATORY j
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ORCAMZAnOM
£^l//yo ^/Tg tr-
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HELEN WARD. MS 301
SAMPLE INFORMATION
y
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i^i**.« /9i'
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CHAIN OF CUSTODY
BEUNQUISHESBY
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DATE
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TIME
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SECHVEDBY DATE
'7^y,,y^'9'9^
TIME
//^^
FOR LABORATORY USE ONLY
MIBOOMFLKnD nCNAIVU
September 23, 1994 CERTIFICATE OF ANM.YSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward
MIS 301
A.F: WALKER, MIS 301E
Ext 5390
ANALYZED
BY:
Vtiokol Corporation
Science & Engineering
P.O. Box 707
Brigham aty, Ut 84302-0707
Afialytical Labs MIS 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Orderly 9409003
Lab ID: Sainple ID:
OIA A-2 PHOTO, GD 56, 5 FT.
Lab ID: Sample ID:
02A A-2 PHOTO, GD 56, 7 FT.
Lab ID: Sample ID:
03A A-2 PHOTO, CD 64, 5 FT.
Lab ID: Sample ID:
04A A-2 PHOTO, GD 64, 7 FT.
Sample and Test Code Identification
Lab ID:
~O5A
Lab ID:
06A
Sample ID Nnmpift IL>:
A-2 PHOTO, OD 52, 5 FT.
Sample ID •Sample lu:
A-2 PHOTO, QD 52, 6 FT.
Lab ID: .Samplp. TD:
OTA A-2 PHOTO, GD 78, 5 FT.
Lab ID: Sample ID:
OSA A-2 PHOTO, OD 78, 10 FT.
Test Codes and Names
3050
CD AE2
CR AE2
PB AE2
AG AE2
Acid Digestion
Cadmium
Chromium
Lead
SUver
Test Codes and Names
3050
CD AE2
CR AE2
PB AE2
AG"AE2
Acid Digestion
Cadmium
Chromium
Lead
Silver
Test Codes and Names
3050
CD AE2
CR~AE2
PB AE2
AG AE2
Acid Digestion
Cadmium
Chromium
Lead
Silver
Test Codes and Names
3050
CD AE2
CR AE2
PB AE2
AG AE2
Acid Digestion
Cadmium
Chromium
Lead
Silver
Test Codes and Names
3050
CD AE2 CR AE2
PB AE2
AG AE2
Acid Digestion
Cadmium Chromium
Lead
Silver
Test Codes and Names
3050
CD AE2
CR"AE2
PB AE2
AQ AE2
Acid Digestion
Cadmium
Chromium
Lead
Silver
Test Codes and Names
3050
CD AE2
CR AE2
PB AE2
AG AE2
Acid Digestion
Cadmium
Chromium
Lead
Silver
Test Codes and Names
3050
CD AE2
CR AE2
Acid Digestion
Cadmium
Chromium
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 3050
SW-846, 6010 SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
Page#:lof ^
Work Order ji> 9409003 Sample and Test Code Identification
Lab ID: Sample ID:
OSA A-2 PHOTO, QD 78, 10 FT.
Lab ID: Sample ID:
09A A-2 PHOTO,QD 78, lOFT. DUP
Test Code.1 and Nflme.<
PB AE2 Lead
A(r,AE2 Silver
Test Codes and Names
Lab ID:
lOA
Lab ID:
UA
Lab ID:
12A
Lab ID:
13A
Lab ID:
14A
Lab ID:
15A
Lab ID:
16A
Lab ID:
I7A
A-2 PHOTO, QD 42, 5 FT.
Sample ID:
A-2l!Haro,aD42, 8FT.
-
Sample ID:
A-2 PHOTO, QD 82, 5 FT.
A-2raOTO, OD 82, 10 FT.
•Samplft ID:
A^^Hdro, QD 7, 5 FT.
Sample ID:
A-2 PHOTO, QD 44, 5 FT.
Samnle ID:
A-2 PHOTO, QD 44, 10 FT.
SanrolelD:
A-2PHOTO,QD82,10FT.RNSBLK
3050 Acid Digestion
CD_AE2 Cadmium
CR~AE2 Chromium
PB AE2 Lead
AG AE2 Silver
Test Codes and Names
3050 Acid Digestion
CD AE2 Cadmium
CR AE2 Chromium
PB AE2 Lead
AG AE2 Silver
Test Codes and Names
3050 Acid Digestion
CD AE2 Cadmium
CR AE2 Ctuonuum
PB AE2 Lead
AQ AE2 SUver
Test Codes and Names
3050 Acid Digestion
CD_AE2 Cadmium
CR~AE2 Chromium
PB"AE2 Lead
Aa~AE2 SUver
Test Codes and Mnme.ii
3050 Acid Digestion
CD_AE2 Cadmium
CR AE2 Chromium
PB AE2 Lead
Ad'AE2 Silver
Test Codes and Names
3050 Acid Digestion
CD AE2 Cadmium
CR AE2 Chromium
FB AE2 Lead
AQ AE2 SUver
Test Codes and Names
3050 Acid Digestion
CD_AB2 Cadmium
CR AE2 Chromium
PB"AE2 Lead
ACT AE2 SUver
Test Codes and Names
3050 Acid Digestion
CD AE2 Cadmium
CR AE2 Chromium
PB AE2 Lead
AO AE2 SUver
Test Codes and Namra
3010 Acid Digestion
CD AE2 Cadmium
CR AE2 Chromium
PB AB2 Lead
AQ AE2 SUver
Method
SW-846, 6010
SW-846, 6010
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010 Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010 Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 3010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
•
Page#:2
•
Wnrkordpr CnmmPnfs
Page #:3
This is to cenify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: A-2 PHOTO, GD 56, 5 FT. Lab ID: 9409003-OlA CoUected: 09/07/94 09:05:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
Chromium
Lead
Sliver
09/16/94
D
17.3
7.9
U
DATE
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.6
0.2
09/16/94
09/20/94
09/20/94
09/20/94
09/20/94
MTB
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
Sample ID: A-2 PHOTO, GD 56, 7 FT. Lab ID: 9409003-02A Collected: 09/07/94 09:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
Chromium
Lead
Sliver
09/16/94
0.6
101
9.2
21.7
DATE
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.7
0.2
09/16/94
09/20/94
09/20/94
09/20/94
09/20/94
MTB
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
Sample ID: A-2 PHOTO, GD 64, 5 FT. Lab ID: 9409003-03A Collected: 09/07/94 09:35:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Add Digestion
Cadmium
Chromium
Lead
Sliver
09/16/94
U
19.3
11.0
U
DATE
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.7
0.2
09/16/94
09/20/94
09/20/94
09/20/94
09/20/94
MTB
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
Page ff: 4
September 23, 1994 13:43
•
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: A-2 PHOTO, GD 64, 7 FT. Lab ID: 9409003-04A CoUected: 09/07/94 09:40:00
TEST RESULT UNITS DETECTION Al^ALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
Chromium
Lead
Silver
09/16/94
0.4
25.5
10.0
6.0
DATE
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.6
0.2
09/16/94
09/20/94
09/20/94
09/20/94
09/20/94
MTB
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
Sample ID: A-2 PHOTO, GD 52, 5 FT. Lab ID: 940S)003-05A CoUected: 09/07/94 09:50:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
^l^smlum
Lead
Sliver
09/16/94
U
17.7
11.6
D
DATE
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.7
0.2
09/16/94
09/20/94
09/20/94
09/20/94
09/20/94
MTB
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
Sample ID: A-2 PHOTO, GD 52, 6 FT. Lab ID: 9409003-06A CoUected: 09/07/94 10:00:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
Chromium
Lead
Sliver
09/16/94
D
16.8
10.4
D
DATE
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.6
0.2
09/16/94
09/20/94
09/20/94
09/20/94
09/20/94
MTB
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
Page ff: 5
September 23, 1994 13:43 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: A-2 PHOTO, GD 78, 5 FT. Lab ID: 9409003-07A CoUected: 09/07/94 10:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Add Digestion
Cadmium
Chromium
Lead
Silver
09/16/94
U
17.8
7.7
U
DATE
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.7
0.2
09/16/94
09/20/94
09/20/94
09/20/94
09/20/94
MTB
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
Sample ID: A-2 PHOTO, GD 78, 10 FT. Lab ID: 9409003-08A CoUected: 09/07/94 10:25:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Add Digestion
Cadmium
Chromium
Lead
Sliver
09/16/94
U
21.0
7.9
U
DATE
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.6
0.2
09/16/94
09/20/94
09/20/94
09/20/94
09/20/94
IfTB
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
Sample ID: A-2 PHOTO,GD 78, lOFT. DUP Lab ID: 9409003-09A CoUected: 09/07/94 10:25:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Add Digestion
Cadmium
Chromium
Lead
Sliver
09/16/94
D
27.0
7.9
U
DATE
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.3
0.2
09/16/94
09/20/94
09/20/94
09/20/94
09/20/94
MTB
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
Page ff: 6
September 23, 1994 13:43
Sample ID: A-2 PHOTO, GD 42, 5 FT
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPUC
LabID: 94051003-lOA., CoUected: 09/07/94 10:38:00
TEST
Add Digestion
Cadmium
Chromium
Lead
Sliver
RESULT
09/16/94
U
17.6
8.7
U
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
DETECTION
LIMIT
0.1
0.4
1.8
0.2
AITALYZED
09/16/94
09/20/94
09/20/94
09/20/94
09/20/94
BY
MTB
LVD
LVD
LVD
LVD
METHOD/CAS#
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Sample ID: A-2 PHOTO, GD 42, 8 FT. Lab ID: 940S'003-11A CoUected: 09/07/94 10:48:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Add Digestion
Cadmium
alum
Lead
Silver
||u.
09/16/94
U
20.6
9.2
D
DATE
ug/g
ug/g
ug/g
ug/g
0.
0
1
0
.1
.4
.8
.2
09/16/94
09/20/94
09/20/94
09/20/94
09/20/94
MTB
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
Sample ID: A-2 PHOTO, GD 82, 5 FT. Lab ID: 94O5I0O3-12A CoUected: 09/07/94 11:05:00
TEST
Add Digestion
Cadmium
Chromium
Lead
Sliver
RESULT
09/16/94
U
16.3
8.3
D
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
DETECTION
LIMIT
0.1
0.3
1.3
0.2
AITALYZED
09/16/94
09/20/94
09/20/94
09/20/94
09/20/94
BY
MTB
LVD
LVD
LVD
LVD
METHOD/CAS#
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
# Page ff: 7
September 23, 1994 13:43 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: A-2 PHOTO, GD 82, 10 FT. Lab ID: 9409003-13A CoUected: 09/07/94 11:10:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Add Digestion
Cadmium
Chromium
Lead
Silver
09/16/94
D
15.4
6.7
U
DATE
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.6
0.2
09/16/94
09/20/94
09/20/94
09/20/94
09/20/94
MTB
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
Sample ID: A-2 PHOTO, GD 7, 5 FT. Lab ID: 9409003-14A CoUected: 08/29/94 14:30:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Add Digestion
Cadmium
Chromium
Lead
Silver
09/16/94
U
14.9
10.5
D
DATE
ug/g
ug/g
ug/g
ug/g
0.1
0.4
1.9
0.2
09/16/94
09/20/94
09/20/94
09/20/94
09/20/94
MTB
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
Sample ID: A-2 PHOTO, GD 44, 5 FT. Lab ID: 9409003-15A CoUected: 08/29/94 15:07:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
Chromium
Lead
Silver
09/16/94
D
26.9
8.0
U
DATE
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.7
0.2
09/16/94
09/20/94
09/20/94
09/20/94
09/20/94
MTB
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
Page ff: 8
September 23, 1994 13:43 a
Sample ID: A-2 PHOTO, GD 44, 10 FT
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLli
Lab ID: 94a)003-16A CoUected: 08/29/94 15:20:00
TEST
Add Digestion
Cadmium
Chromium
Lead
Silver
RESULT
09/16/94
0.9
16.1
10.5
U
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
DETECTION
LIMIT
0.1
0.3
1.7
0.2
ANAT.YZED
09/16/94
09/20/94
09/20/94
09/;!0/94
09/20/94
BY
MTB
LVD
LVD
LVD
LVD
METHOD/CAS*
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Sample ID: A-2 PHOTO,GD82,10FT.RNSBLK Lab ID: 9409003-17A CoUected: 09/07/94 11:40:00
TEST RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Add Digestion
Cadmium
^l^jmlum
Lead
Silver
09/16/94 DATE
D ug/L
0.8 ug/L
U ug/L
U ug/L
09/16/94 MTB SW-846, 3010
0.2 09/20/94 LVD SW-846, 6010
0.5 09/20/94 LVD SW-846, 6010
2.5 09/20/94 LVD SW-846, 6010
0.3 09/20/94 LVD SW-846, 6010
• Page ff: 9
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1. IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ElVfVIRONMENTAL LAB WORK REQUf:ST
ii
^^, TfflOKOL ENVraONMENTAL LABORATORY
fHOM:
ORCAMZAnON
E/iLuro EHQy
EXTENSION
MAIL STOP
LWR No. E10631
COITCBOai
1/47)0
WORK ORDBa
/S?^o
DATE
REPORT RESULTS TO:
IhlELEN WARD, MS 301
SAMPLE INFORMATION
y
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TIME RECEIVED BY
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/^^"/^
FOR LABORATORY USE ONLY
DATP. rOMFLETED DATSBBFOimB
ENVIRONMENTAL LAB WORK REQUEST
'-^f^//^f>^i^9 7
THIOKOL ENVIRONMENTAL LABORATORY lUJK - ^/'^^^Z p^f
T^.t^. UL/4L/^i
OBauazAnoN
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BRBOiaH
2oie
t/^o /B^40
Mn
9-/2- 94
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPUE DATE TYPE LOCATION
^ \.^oAno 4ci
tS^VA/4roJ. Sur ^-^2'i4 ly r-z4A l^'ZQ
^1,, As, Cr, Pi> -<^o/o
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BEUNQinSHBiBY 0AXE TIME •BCSVCDBY DAIS HUE
T f-/Z^O&^<r-\///£{/M,_...l 9'/M^ /^^^
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/
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ENVIRONMENTAL LAB WORK REQUEST f^////^^0
" THIOKOL ENVIRONMENTAL LABORATORY LWR No. E10633
nioMi /^. /T UJ/huiCell^
BKICmiON
SSfci
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l/i/TiO /B9i/c/
DATS
f-7S-ff
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BEPORT RESULTS TOl
HELEN WARD, MS 301
' y
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LOCATION
M-lfA
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CHAIN OF CUSTODY
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TIME
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^^i^Jz^/^-^
DATE
f//^/W
TIME
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FOR LABORATORY USE ONLY
nAnCOMTLEnD MTBRITORTES
January 17, 1995 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
TTiiokol Corporation
Science & Engineering
P.O. Box 707
Brigham aty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order # 9411050
Lab ID:
OIA
Lab ID:
02A
Lab ID:
03A •
Lab ID:
04A
Sample ID:
HO S, 1 FT.
Sample ID:
T-24A, 25 DN GD 2 FT.
Sample ID:
Ml 9 A, DRYWELL 3 FT
M-39, DRYWELL 1 FT.
Sample and Test Code Identification
Test Codes and Names
1311 TCLP Metals/SemiVols Extr.
PB_AE2 Lead
Test Codes and Names
1311 TCLP MeUls/SemiVoU Extr.
CR_AE2 Chromium
Test Codes and Names
1311 TCLP Metals/SemiVoIs Extr.
CR_AE2 Chromium
PB_AE2 Lead
AO_AE2 Silver
Test Codes and Names
1311 TCLP MeUls/SemiVols Extr.
AG AE2 Silver
Method
SW-846, 1311
SW-846, 6010
Method
SW-846, 1311
SW-846, 6010
Method
SW-846, 1311
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 1311
SW-846, 6010
Commente
Report: THESE SAMPLES ARE RERUNS THAT WERE ORIGINALLY SUBMITTED O
WORK ORDERS #9409007 SAMPLES 06A & 14A AND #9409009 SAMPLES
02A & 03A.
#
Page #:1 of ^
#
This is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: I-IO S, 1 FT. Lab ID: 9411050-OlA CoUected: 09/12/94 10:55:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
TCLP Metals/SemlVols Extr.
Lead
01/10/95
102
DATE
ug/L 25
01/10/95
01/13/95
LVD
LVD
SW-846,
SW-846,
1311
6010
Sample ID: T-24A, 25 DN GD 2 FT. Lab ID: 9411050-02A Collected: 09/12/94 15:25:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
TCLP Metals/SemiVols Extr. 01/10/95 DATE
Chromium 104 ug/L
01/10/95 LVD SW-846, 1311
5 01/13/95 LVD SW-846, 6010
Sample ID: M-19A, DRYWELL 3 FT. Lab ID: 9411050-03A Collected: 09/15/94 09:40:00
0T RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
TCLP Metals/SemlVols Extr.
Chromium
Lead
Silver
01/10/95
265
8060
4.14
DATE
ug/L
ug/L
ug/L
5
25
3
01/10/95
01/13/95
01/13/95
01/13/95
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
1311
6010
6010
6010
Sample ID: M-39, DRYWELL 1 FT. Lab ID: 9411050-04A . CoUected: 09/15/94 10:10:00
TEST RESULT UNITS DETECTION AlifAiLYZED BY
LIMIT
METHOD/CAS#
TCLP Metals/SemiVols Extr. 01/10/95 DATE
Silver U ug/L
01/10/95 LVD
3 01/13/95 LVD
SW-846, 1311
SW-846, 6010
# Page ff: 2
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1.IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ENVIRONMENTAL LAB WORK REQlfEST ^<-//i f ^^7
^' rmOKOL ENVIRONMENTAL LABORATORY LWR No. E10631
A.^^ Wa//^
EXTQ4SION OOSTCSNTEn
iMoo
WORK ORDER
/Sf^o ^-/Z-ff
ORGAM ZATION
£/ii^tro ^n/^ y
MAIL STOP
-Zol£-
REPORT RESlJLTIi TO:
HELEN WARD, MS 301
y
/
•'
y
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^
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\-'
..
u
SAMPLE
/fil-
2- ^tJOltO 645"
3/¥
3 Suoiuo4^i3
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.'• SOJAAO 43jt,
•^ SU/A\X/ 2.34
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9- ^uJini/3£'£'
//V
3/^r
n.sui/Hl/ 40f
/V &/ ViS.'^r
>i 5to/«(/' 4ot
DATE
9-it-^
^.-n-h
f'/Z-f4
"1-11'%
f-ii'f^
9-/744
"i'/r-fi
f-/2-f^,
9'l24i
9-124^
9-iz-H
9-1144
TYPE
G
i/
y
y
y^
v^
\/
y
y
y
ty
^y
1^
c
'
SAMPLE INFORMATION
LOCATION
T-/0 A/e
•T-/0 //€
-X'/o sa'
-I-/oSe
T'lD 5e
- T'/OS
r-i/^s
x-/^s
T'/ll
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TIME
loio
/oa^
/03o
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CojMltJfyi - C>0//>
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Vac- ^2^0
CJ, Cr, Ph -h/>/0
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p// - ^^«5"
Sb//h,f7r, P6 '6?oi^
Siiffii-k - yioo z)//- 904^
/(
REMARKS
CHAIN OF CUSTODY
RFIJNQUISnEDBY
UM(/a7i
DATE
'?'/s-n
TIME
694^
RFrETVED BY
//yy^//./Zti.! /^.yf-
DATE
. ^,/J-f4^
TIME
/^<^V^
FOR LABORATORY USE ONLY
4 DATE COMPLETED DATBRQ>ORTED
"* THIOKOL ENVIRONMENTAL LABORATORY
ENVIRONMENTAL LAB WORK REQUEST
-^/^//"^CY^
IU7I^ - ^/O^^/ p^ ^
/^./C. Ut74LlCet
OBOAraZAHON
B/iuiro ^4^^
SAMPLE INFORMATION
SAMPLE
Jl \.StiMni) 4c 1
\zs'x>A/Cr€JSur
^•StM/HU 40/
\tS'Dy £ri>J.2h
3.
4,
i.
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7.
1.
9.
IQL
1 "'
11
DATE
^-^744
9-lt'l4
Tm
6
ty
L^
c
LOCAnON
r-244
r-z4^4
HME
Irzo
/szs-
TEST REMARKS
^k,As,Cr,Py -&0/0 1
//
1
CHAIN OF CUSTODY
SEUNQUISHEI) BY
'MZ-
DATE
f-n-^'om.
TIME SECQVEDBV
///^f77.^..\f'fx-f.^
DATE TIME
/^^r
FOR LABORATORY USE ONLY
r""*™ DATsairanB) niauiua
November 11, 1994 CERTIFICATE OF ANAll^YSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward
MIS 301
A.F. WALKER, MIS 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Oty, Ut 84302-0707
Analytical Labs MIS 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order # 9409007
Lab ID:
OIA
Lab ID:
02A
Lab ID:
03A
Lab ID:
04A
Lab ID:
OSA
Lab ID:
06A
Lab ID:
09A
Lab ID:
lOA
Sample ID:
I-10NE,1 FT.
Sample ID:
I-IO NE,3 FT.
Sample ID:
I-10SE,1 FT.
Sample ID:
I-IO SE,3 FT.
Sample ID:
I-IO SE,3 FT. DUP
Sample ID:
I-IO S, 1 FT.
Lab ID: Sample ID:
07A 1-10 S, 20 DN.GD.SURFACE
Lab ID: Sample ID:
08A I-IO S,20'DN. aD.2 FT.
Sample ID:
T-l II, 1 FT.
Sample ID:
T-in,3 FT.
Sample and Test Code Identification
Test Codes and Names
3050 Acid Digestion
CD_AE2 Cadmium
Test Codes aiid Names
3050 Acid Digestion
CD_AE2 Cadmium
Test Codes arid Names
82408 Volatile Organics
Test Codes and Names
8240S Volatile Organics
Test Codes and Names
8240S Volatile Otganics
Test Codes and Names
3050 Acid Digestion
CD_AE2 Cadmium
CR_AE2 Chromium
PB_AE2 Lead
Test Codes and Names
3050 Acid Digestion
CD_AE2 Cadmium
CR_AE2 Chromium
PB_AE2 Lead
Test Codes and Names
3050 Acid Digestion
CD_AE2 Cadmium
CR_AE2 Chromium
PB_AE2 Lead
Test Codes and Names
Lab ID: Sample ID:
11A T-24A, PT OF DIS SURFACE
S04IC1
PH S
S04IC1
PH S
S04IC1
3050
SB AE2
CR AE2
PB AE2
AS GF2
PH S
Sulfate
pH (Soil)
Test Codes and Names
Sulfate
pH (Soil)
Test Codes anid Names
Sulfate
Acid Digestion
Antimony
Chromium
Lead
Arsenic
pH (Soil)
Method
SW-846, 3050
SW-846, 6010
Method
SW-846, 3050
SW-846, 6010
Method
SW-846, 8240
Method
SW-846, 8240
Method
SW-846, 8240
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010 Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846. 6010
Method
EPA 300.0
SW-846,9045A
Method
EPA 300.0
SW-846,9045A
Method
EPA 300.0
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846,9045A
Page#:lof ^
Work Order # 9409007
Lab ID:
12A
Lab ID:
13A
Lab ID:
14A
Sample ID:
T-24A, FT OF DIS 2 FT.
Sample ID:
T-24A, 25 FT DN GD SURFACE
Sample ID:
T-24A, 25 FT DN GD 2 FT.
Sample and Test Code Identification
Test Codes and Names
S041C1
3050
SB AE2
CR AE2
PB AE2
AS GF2
PH_S
Sulfate
Acid Digestion
Antimony
Chromium
Lead
Arsenic
pH (Soil)
Test Codes and Names
S04IC1
3050
SB AE2
CR AE2
PB AE2
AS GF2
PH_S
Sulfate
Acid Digestion
Antimony
Chromium
Lead
Arsenic
pH (Soil)
Test Codes and Names
S04IC1
3050
SB AE2
CR AE2
PB AE2
AS GF2
PH_S
Sulfate
Acid Digestion
Antimony
Chromium
Lead
Arsenic
pH (Soil)
Workorder Comments
Method
EPA 300.0
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846,9045A
Method
EPA 300.0
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846,9045A
Method
EPA 300.0
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846,9045A
Page #:2
This is to certify that the following samples were analyzed using good laboratory practices
to show the following resulis.
Sample ID: I-10NE,1 FT. Lab ID: 9409007-OlA CoUected: 09/12/94 10:10:00
TEST RESULT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
09/21/94
4.78
DATE
ug/g 0.1
09/:;i/94
09/23/94
MTB
LVD
SW-846,
SW-846,
3050
6010
Sample ID: I-10 NE,3 FT. Lab ID: 9409007-02A CoUected: 09/12/94 10:25:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
09/21/94 . DATE 09/21/94 MTB SW-846, 3050
3.81 ug/g 0.1 09/23/94 LVD SW-846, 6010
Sample ID: M0SE,1 FT. Lab ID: 9409007-03A CoUected: 09/12/94 10:30:00
0T
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
RESULT
3 J
U
U
U
U
U
U
u- • u u u u u u u
u u
u
u u
u u u D
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
• Page #: 3
November 11, 1994 12:33 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: I-IO SE,1 FT. Lab ID: 9409007-03A CoUected: 09/12/94 10:30:00
TEST
Volatile Organics
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
RESULT
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
Surrogat
Surrogate
Toluene-d8
U
D
U
4 J
D
U
U
U
U
f BJ
U
2 J
U
U
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
e/Recovery Data For Volatile Organics 8240S
Bromofluorobenzene
1,2-Dichloroethane-d4
%Recovery
99.4
98.6
98.5
METHOD/CAS#
SW-846, 8240
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
^^^.
^^B
Sample ID: I-IO SE,3 FT. Lab ID: 9409007-04A CoUected: 09/12/94 10:35:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
RESULT
D
U
U
U
U
U
D
U
U
u u u u u D
D
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
Page ff: 4
November 11, 1994 12:33
Sample ID: 1-10 SE,3 FT.
CERTIFICATE OF ANALYSIS
^ RESULTS BY SAMPLE
Lab ID: 9409007-04A CoUected: 09/12/94 10:35:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane fi
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
JB^-Iene
Surrogat
Surrogate
Toluene-d8
U
U
U
O
U
U
U
U
U
U
3 J
U
U
U
U
U
BJ
U
8 J
U
U
D
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
e/Recovery Data
Bromofluorobenze 3ne
1,2-Dichloroethane-d4
10
10
10
10
10
10
10
10
10
10
10
10
10
10 •
10
10
10
10
10
10
10
10
10
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240S
^Recovery
95.1
93.3
99.1
SW-846, 8240
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
Sample ID: I-IO SE,3 FT. DUP Lab ID: 9409007-05A CoUected: 09/12/94 10:35:00
TEST RESULT UNITS DETECTION ANAILYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
D
U
U
U
u
u
u
13
U
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
09/16/94
09/16/94
09/16/94
09/li5/94
09/16/94
09/1(5/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
Page ff: 5
November 11, 1994 12:33 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: I-10 SE,3 FT. DUP Lab ID: 9409007-05A CoUected: 09/12/94 10:35:00
TEST
Volatile Organics
Chloroethane
2 -Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Te t rachl oroe thene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
Tri chlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
D
U
D
D
U
D
U
U
U
U
U
U
D
D
U
D
U
2 J
U
U
U
U
U
11 B
Surrogat
Surrogate
Toluene-d8
U
14
D
U
U
D
e/Re<
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
rovery Data For Volatile Organics 8240S
Bromofluorobenzene
1,2-Dichloroetheme-d4
%Recovery
92.5
89.5
96.3
METHOD/CAS#
SW-846, 8240
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3 ^B
71-55-6 ^P
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
Sample ID: l-io S, 1 FT. Lab ID: 9409007-06A CoUected: 09/12/94 10:55:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
09/21/94
28.7
DATE
ug/g
09/21/94 MTB SW-846, 3050
0.1 09/23/94 LVD SW-846, 6010
Page ff: 6
November 11, 1994 12:33 o
Sample ID: I-IO S, 1 FT.
CERTIFICATE OF ANALYSIS
' RESULTS BY SAMPDli:
Lab ID: 9409007-06A CoUected: 09/12/94 10:55:00
TEST RESULT UNITS DETECTION AITALYZED BY
LIMIT
METHOD/CAS#
Chromium
Lead
4.5
909
ug/g
ug/g
0.3
1.4
09/23/94
09/23/94
LVD
LVD
SW-846,
SW-846,
6010
6010
Sample ID: 1-10 S, 20'DN.GD.SURFACE Lab ID: 9409007-07A CoUected: 09/12/94 11:00:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
Chromium
Lead
09/21/94
3.16
20.9
226
DATE
ug/g
ug/g
ug/g
0.1
0.3
1.5
09/21/94
09/23/94
09/23/94
09/23/94
MTB
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
a pie ID: I-IO S,20'DN. GD.2 FT. Lab ID: 9409007-08A CoUected: 09/12/94 11:10:00
TEST RESULT UNITS DETECTION AKFAJEiYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
Chromium
Lead
09/21/94
0.47
14.2
25.5
DATE
ug/g
ug/g
ug/g
0.1
0.3
1.8
09/21/94
09/23/94
09/23/94
09/23/94
MTB
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
Sample ID: T-l 11, 1 FT.
TEST
Lab ID: 9409007-09A CoUected: 09/12/94 14:20:00
RESULT UNITS DETECTION ANAJJYZED BY
LIMIT
METHOD/CAS#
Sulfate
pH (Soil)
105 mg/L
8.54 pH Unit
2 10/25/94 CRS
09/14/94 MTB
EPA 300.0
SW-846,9045A
m Page #: 7
November 11, 1994 12:33 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: Tin, 3 FT. Lab ID: 9409007-lOA CoUected: 09/12/94 14:35:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Sulfate
pH (Soil)
107 mg/L
8.17 pH Unit
3 10/26/94 CRS
09/14/94 MTB
EPA 300.0
SW-846,9045A
Sample ID: T-24A, FT OF DIS SURFACE Lab ID: 9409007-11A CoUected: 09/12/94 15:05:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Sulfate
Acid Digestion
Antimony
Chromium
Lead
Arsenic
pH (Soil)
47.2
09/21/94
U
' 8.99
13.0
2.29
7.49
mg/L
DATK
ug/g
ug/g
ug/g
ug/L
pH Unit
2
10.0
0.3
1.4
0.081
10/26/94
09/21/94
09/23/94
09/23/94
09/23/94
10/23/94
09/14/94
CRS
MTB
LVD
LVD
LVD
CRS
MTB
EPA 300.0
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846,9045A
Sample ID: T-24A, PT OF DlS 2 FT. Lab ED: 9409007-12A CoUected: 09/12/94 15:12:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Sulfate
Acid Digestion
Antimony
Chromium
Lead
Arsenic
pH (Soil)
25
09/21/94
U
420
9.45
2.37
7.39
mg/L
DATE
ug/g
ug/g
ug/g
ug/L
pH Unit
3
10.0
0.3
1.6
0.092
10/26/94
09/21/94
09/23/94
09/23/94
09/23/94
10/23/94
09/14/94
CRS
MTB
LVD
LVD
LVD
CRS
MTB
EPA 300.0
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846,9045A
Page ff: 8
November 11, 1994 12:33 o CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: T-24A, 25 FT DN GD SURFACE Lab ID: 9409007-13A CoUected: 09/12/94 15:20:00
TEST RESULT UNITS DETECTION AMil.YZED BY
LIMIT
METHOD/CAS#
Sulfate
Acid Digestion
Antimony
Chromium
Lead
Arsenic
pH (Soil)
105
09/21/94
U
19.0
49.3
1.77
mg/L
DATE
ug/g
ug/g
ug/g
ug/L
7.54 pH Unit
3
10.0
0.3
1.5
0.10
10/26/94
09/21/94
09/23/94
09/23/94
09/23/94
10/23/94
09/14/94
CRS
MTB
LVD
LVD
LVD
CRS
Ml'B
EPA 300.0
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846,9045A
Sample ID: T-24A, 25 FT DN GD 2 FT. Lab ID: 9409007-14A CoUected: 09/12/94 15:25:00
TEST
•
RESULT UNITS DETECTION ANJ^YZED BY
LIMIT
METHOD/CAS#
.fate
Acid Digestion
Antimony
Chromium
Lead
Arsenic
pH (Soil)
29
09/21/94
U
790
8.28
3.98
mg/L
DATE
ug/g
ug/g
ug/g
ug/L
7.44 pH Unit
3
10.0
0.3
1.6
0 .093
10/26/94
09/21/94
09/23/94
09/23/94
09/23/94
10/23/94
09/14/94
CRS
MTB
LVD
LVD
LVD
CRS
MTB
EPA 300.0
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846,9045A
# Page ff: 9
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1. IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the calibration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not applicable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ENVIRONMENTAL LAB WORK REQUEST
IF
^//^/p^Tp/^g'
TfflOKOL ENVIRONMENTAL LABORATORY LWR No. E10632
A T^wtc [\-^A^^^gcp .^B7ts
OOSTGEKTBR
t/^cc:'
WORKORDm
\^'i[/& ^~\-\-^^
ORGAM ZATION
% Isl.
REPORT RESULTS TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE
^-\\4M
TYPE
1
LOCATION
Q'^-zo r^
TIME
111?
TEST
/^4^^. VQ/^ ^ft
REMARKS
^oA
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CHAIN OF CUSTODY
RELINQUISHED BY
Y/MU^
DATE
f-/3-H
TIME
/ZtPO
RECEIVEDBY DATE
^.yT—^^/f-f^-
TIME
/>'^^
FOR LABORATORY USE ONLY
DATE COMPLETED
^
DATERB«RTED SIGNATURE
October 18, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmeraal Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER. M/S 301E
Ext 5390
ANALYZED
BY:
TTiiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order # 9409008 Sampie and Test Code Identification
Lab ID:
OIA
Sample ID:
M-2 LAUNDRY.GD 20,5 FT.
Test Codes and Names
Lab ID:
02A
Sample ID:
M-2 LAUNDRY.GD 20,10 FT.
Lab ID:
03A
Sample ID:
M-2 LAUNDRY.GD 40,5 FT.
Lab ID: Sample ID:
04A M-2 LAUNDRY.GD 40,10 FT.
Lab ID:
~05A
Sample ID:
M-2 LAUNDRY.GD 38,5 FT.
Lab ID:
06A
Sample ID:
M-2 LAUNDRY.GD 38.10 FT.
3050
CD AE2
CR AE2
PB AE2
AG AE2
8240S
PH S
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
pH (Soil)
Test Codes and Names
3050
CD AE2
CR AE2
PB AE2
AG AE2
8240s
PH S
Acid Digestion
Cadmium Chromium
Lead
Silver
Volatile Organics
pH (Soil)
Test Codes and Names
3050
CD AE2
CR AE2
PB AE2
AG AE2
8240s
PH S
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Oiganics
pH (SoU)
Test Codes and Names
3050
CD AE2
CR AE2
PB AE2
AG AE2
8240S
PH S
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Oiganics
pH (SoU)
Test Codes and Names
3050
CD AE2
CR AE2
PB AE2
AO AE2
8240s
PH S
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Oiganics
pH (SoU)
Test Codes and Names
3050
CD AE2
CR2AE2
PB_AE2
AO AE2
8240s
PH S
Acid Digestion
Cadmium
Chromium
Lead
SUver
VolatUe Oiganics
pH (SoU)
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,9045A Method
SW-846, 3050
SW-g46, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846.9045A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846. 8240
SW-846,9045A Method
SW-846. 3050
SW-846. 6010
SW-846. 6010
SW-846. 6010
SW-846. 6010
SW-846. 8240
SW-846,9045A Method
SW-846, 3050
SW-846. 6010
SW-846. 6010
SW-846. 6010
SW-S46. 6010
SW-846. 8240
SW-846.9045A Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846.9045A
Page#:lof f^
Work Order # 9409008
iLablD:
K7A '
W
Lab ID:
08A
Lab ID:
09A
Lab ID:
lOA
Lab ID:
llA
k
1 r.
Lab ID: 12A
Sample ID:
M-2 LAUNDRY.GD 38.10FT DUP
Sample ID:
M-2 LAUNDRY.GD 26.5 FT.
Sample ID:
M-2 LAUNDRY.GD 26.10 FT.
Sample ID:
M-2 LAUNDRY.GD 33,5 FT.
Sample ID:
M-2 LAUNDRY.GD 33.10 FT.
Sample ID: M-2 LAUNDRY .RINSATE BLANK
Sample and Test Code Identification
Test Codes and Names
3050
CD AE2 CR AE2
PB AE2
AG AE2
8240s
PH_S
Acid Digestion
Cadmium Chromium
Lead
Silver
VolatUe Organics
pH (SoU)
Test Codes and Names
3050
CD AE2
CR AE2
PB AE2
AG AE2
8240s
PH_S
Acid Digestion
Cadmium
Chromium
Lead
Silver
VolatUe Oiganics
pH (Soil)
Test diodes and Names
3050
CD AE2
CR AE2
PB AE2
AG AE2
8240S
PH_S
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
pH (Soil)
Test Codes and Names
3050
CD AE2
CR AE2
PB AE2
AG AE2
8240s PH_S
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
pH (Soil)
Test Codes and Names
3050
CD AE2
CR AE2
PB"AE2
AG AE2
8240s
PH_S
Acid Digestion
Cadmium
Chiomium
Lead
Silver
VolatUe Organics
pH (Soil)
Test erodes and Names
8240 Volatile Organics
Method
SW-846, 3050
SW-846, 6010 SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 8240
SW-846,9045A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,9045A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 8240
SW-846,9045A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,9045A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 8240
SW-846,9045A
Method
SW-846, 8240
Workorder Comimenfig
^./f, "^^y^.
Certilii T
m Page #:2
This is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: M-2 LAUNDRY.GD 20,5 FT. Lab ID: 9409008-OlA CoUected: 09/13/94 09:37:00
TEST
Add Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromome thane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexanone
trems-1,2-Dichloroethene
1,2-Dichloroprpp2me
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethame
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl cailoride
RESULT
09/21/94
0.1
18.8
10.2
U
U
U
U
U
XJ
U
U
3 J
U
D
U
U
U
U
D
D
D
D
U
U
U
U
U
D
D
U
U
U
2 J
D
U
D
U
D
4 BJ
D
U
U
U
D
DNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.4
1.8
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/21/94
09/23/94
09/23/94
09/23/94
09/23/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
BY
MTB
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JM;^
JMA.
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7 ^^
75-00-3 ^M
110-75-8 ^^
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
Page ff: 3
October 18, 1994 10:43
o
Sample ID: M-2 LAUNDRY,GD 20,5 FT.
CERTIFICATE OF ANAJLYSIS
* RESULTS BY SAMPIilE
Lab ID: 9409008-OlA Collected: 09/13/94 09:37:00
TEST RESULT UNITS DETECTION AISTALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
o-Xylene
SW-846, 8240
10 09/16/94 JMA 95-47-6 U . ug/Kg
Surrogate/Recovery Data For Volatile Organics 8240S
pH (Soil)
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichlorpethane-d4
7.7 pH Unit
%Recovery
99.9
98.5
96.4
Recovery Limits
81 TO 117
74 TO 121
70 TO 121
09/14/94 MTB SW-846,9045A
Sample ID: M-2 LAUNDRY,GD 20,10 FT. Lab ID: 9409008-02A Collected: 09/13/94 09:47:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
I^Baium
Chromium
Lead
Silver
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorome thane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2 -Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
09/21/94
U
17.8
11.2
U
3 J
U
U
D
D
U
U
U
U
u u
u
u
u u u u
u
u
u
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.1
0.3
1.4
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/21/94
09/23/94
09/23/94
09/23/94
09/23/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
MTB
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
3050
6010
6010
6010
6010
8240
Page ff: 4
October 18, 1994 10:43 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-2 LAUhfDRY,GD 20,10 FT. Lab ID: 9409008-02A Collected: 09/13/94 09:47:00
TEST
Volatile Organics
-
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroetheme
Tri chloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
pH (Soil)
RESULT
U
u
u u
D
D
U
U
1 J
U
n
u
u u
3 BJ
D
D
U
U
D
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
7.7 pH Unit
%Recovery
101
102
94.2
METHOD/CAS#
SW-846, 8240
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
•
Recovery Limits
81
74
70
09/14/94
TO 117
TO 121
TO 121
MTB SW-846,9045A
Sample ID: M-2 LAUNDRY,GD 40,5 FT. Lab ID: 9409008-03A CoUected: 09/13/94 10:05:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
CadmiiuD
Chromium
Lead
Silver
09/21/94
U
21.9
11.1
U
DATE
ug/g
ug/g
ug/g
ug/g
0.1
0.4
1.8
0.2
09/21/94
09/23/94
09/23/94
09/23/94
09/23/94
MTB
LVD
LVD
LVD
LVD
SW-646,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
Page ff: 5
October 18, 1994 10:43 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-2 LAUNDRY,GD 40,5 FT. Lab ID: 9409()08-03A Collected: 09/13/94 10:05:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
B romome thane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexcmone
trems-1,2-Dichloroethene
lj,2 -Dichloropropane
J||^-1,3 -Dichloropropene
^I^Pas -1,3 -Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4 -Me thyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Tri chlorof1uoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
3 J
U
U
U
U
U
U
u
u u u u u
u u u u u u u u u
u u
u u
u u 2 J
u u •
u u D
9 BJ
u u
u
u
u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/:L6/94
09/16/94
09/:L6/94
09/16/94
09/:L6/94
09/:L6/94
09/:L6/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
09/16/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-
pH (Soil)
D i chloroethane-d4
7.6 pH Unit
%Recovery
100
100
93.8
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
09/14/94
TO 117
TO 121
TO 121
MTB SW-846,9045A
Page ff: 6
October 18, 1994 10:43 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-2 LAUNDRY,GD 40,10 FT. Lab ID: 9409008-04A Collected: 09/13/94 10:15:00
TEST
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
D ibromochlorome thane
1,1-Dichloroethane
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexanone
trems-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Tri chloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
09/21/94
u
22.1
12.0
U
U
U
U
U
U
U
D
u u u
u
u
u
u u u u u u u u u u u u u u u u
u u u u u 9 BJ
u
u
u
u u u
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
1.5
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/21/94
09/23/94
09/23/94
09/23/94
09/23/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
BY
MTB
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
OMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-e46,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01
10061-02
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
3050
6010
6010
6010
6010
8240
^ V
-5
-6
Page ff: 7
October 18, 1994 10:43 CERTIFICATE OF ANALYSIS
) RESULTS BY SAMPLE
Sample ID: M-2 LAUNDRY.GD 40,10 FT. Lab ID: 9409008-04A Collected: 09/13/94 10:15:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics SW-846, 8240
Surrogate/Recovery Data For Volatile Organics 8240S
pH (Soil)
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
7.5 pH Unit
%Recovery
102
103
98.7
Recovery Limits
81 TO 117
74 TO 121
70 TO 121
09/14/94 MTB SW-846,9045A
Sample ID: M-2 LAUNDRY,GD 38,5 FT. Lab ID: 9409008-05A Collected: 09/13/94 10:20:00
TEST RESULT UNITS DETECTION AITALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
fl^Bimium
Lead
Silver
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
09/21/94
U
18.1
11.7
U
U
U
U
U
U
U
U
u u u u u u u u u u
u
u
u u u
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.1
0.3
1.5
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/21/94
09/23/94
09/23/94
09/23/94
09/23/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
MTB
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
3050
6010
6010
6010
6010
8240
Page ff: 8
October 18, 1994 10:43 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ED: M-2 LAUNDRY,GD 38,5 FT. Lab ID: 9409008-05A Collected: 09/13/94 10:20:00
TEST
Volatile Organics
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Tri chlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
pH (Soil)
RESULT
7
Surrogat
Surrogate
Toluene-d8
U
U
u u u u u u u u u u BJ
u u u
u u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
e/Recovery Data For Volatile Organics 8240S
Bromofluorobenzene
1,2-Dichloroetheme-d4
7.5 pH Unit
%Recovery
102
102
96.8
METHOD/CAS#
SW-846, 8240
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits ^B
81
74
70
09/14/94
TO 117
TO 121
TO 121
MTB
^^
SW-846,9045A
Sample ID: M-2 LAUNDRY.GD 38,10 FT. Lab ID: 9409008-06A CoUected: 09/13/94 10:30:00
TEST
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
Acetone
Acrolein
RESULT
09/21/94
U
22.5
11.3
U
U
U
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
1.4
0.2
10
10
ANALYZED
09/21/94
09/23/94
09/23/94
09/23/94
09/23/94
09/19/94
09/19/94
BY
MTB
LVD
LVD
LVD
LVD
JMA
JMA
METHOD/CAS*
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
3050
6010
6010
6010
6010
8240
Page ff: 9
October 18, 1994 10:43 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPIIE
Sample ID: M-2 LAUNDRY,GD 38,10 FT. Lab ID: 9409008-06A Collected: 09/13/94 10:30:00
TEST - RESULT
Volatile Organics
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexanone
trems-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
^ll^-Dichlorobenzene
^^P'D i chl orobenz ene
^^-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane 4
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
Surrogat
Surrogate
Toluene-d8
U
U
U
u u u
u u u
u u u .
u u u u u
u u u
u u u u
u
u
u u u u u u BJ
u
u u
u
u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Al^ALYZED
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
e/Recovery Data For Volatile Organics 8240S
Bromofluorobenzene
1,2 -Dichloroetheme-d4
pH (Soil) 7.6 pH Unit
%Recovery
102
102
96.0
METHOD/CAS#
SW-84e, 8240
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
09/14/94
TO 117
TO 121
TO 121
MTB SW-846,9045A
Page ff: 10
October 18, 1994 10:43 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-2 LAUNDRY,GD 38, lOFT DUP Lab ID: 9409008-07A Collected: 09/13/94 10:30:00
TEST
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2 -Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Tri chlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
09/21/94
U
19.0
11.2
U
U
U
U
U
U
U
D
U
u
u u u
u
u u
u
u u
u
u u u
u u u u u u u
u u u u u 8 BJ
u u u u
u u
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
1.6
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/21/94
09/23/94
09/23/94
09/23/94
09/23/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
BY
MTB
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
OMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846.
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01
10061-02
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
3050
6010
6010
6010
6010
8240
^ V
-5
-6
Page#: 11
October 18, 1994 10:43 CERTIFICATE OF ANALYSIS
'''-'^ . RESULTS BY SAMPLE
Sample ID: M-2 LAUNDRY,GD 38, lOFT DUP Lab ID: 9409008-07A Collected: 09/13/94 10:30:00
TEST RESULT UNITS DETECTION A]!7ALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics SW-846, 8240
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate %Recovery
Toluene-d8 102
Bromofluorobenzene 103
1,2-Dichloroethane-d4 94.9
Recovery Limits
81 TO 117
74 TO 121
70 TO 121
pH (Soil) 7..6 pH Unit 09/14/94 MTB SW-846,9045A
Sample ID: M-2 LAUNDRY.GD 26,5 FT. Lab ID: 9409008-08A Collected: 09/13/94 10:43:00
TEST
Acid Digestion
Cadmium
flBjfflium
Lead
Silver
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroetheme
1,1 -Dichloroethene
2-Hexanone
trans-i,2-Dichloroethene
1,2-Dichloropropane
RESULT
09/21/94
u
19 .6
11.0
U
U
U
U
• U
U
u u u u u u u u
u u
u u
u
u u u u
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
1.6
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/21/94
09/23/94
09/23/94
09/23/94
09/23/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
BY
MTB
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
Page #: 12
October 18, 1994 10:43 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-2 LAUNDRY,GD 26,5 FT. Lab ID: 9409008-08A Collected: 09/13/94 10:43:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
cis-l,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
vinyl Chloride
o-Xylene
U
U
U
U
U
U
U
U
U
U
U
u
BJ
U
U
U
U
U
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8240
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Surrogate/Recovery Data For Volatile Organics 8240S
pH (Soil)
Surrogate %Recovery
Toluene-d8 101
Bromofluorobenzene 100
l,2-Dichloroetheme-d4 94.7
Recovery Limits
81 TO 117
74 TO 121
70 TO 121
7.5 pH Unit 09/14/94 MTB SW-846,9045A
Sample ID: M-2 LAUNDRY.GD 26,10 FT. Lab ID: 9409008-09A Collected: 09/13/94 10:50:00
TEST
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
Acetone
Acrolein
RESULT
09/21/94
U
18.2
10.8
U
U
U
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
1.6
0.2
10
10
ANALYZED
09/21/94
09/23/94
09/23/94
09/23/94
09/23/94
09/19/94
09/19/94
BY
MTB
LVD
LVD
LVD
LVD
JMA
JMA
METHOD/CAS#
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
Page ff: 13
October 18, 1994 10:43 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-2 LAUNDRY,GD 26,10 FT. Lab ID: 9409008-09A Collected: 09/13/94 10:50:00
TEST
Volatile Organics
Acrylonitrile
Benzene
Bromodi chlorometheme
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chlorofonn
Chloromethane
Dibromochlorometheme
1,1-Dichloroetheme
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexemone
t rans -1,2-Di chl oroe thene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
m^-Dichlorobenzene
IV-Dichlorobenzene
174-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2 -Trichloroethctne
Trichloroethene
Trichlorofluoromethane
vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
9
Surrogat
Surrogate
Toluene-d8
U
U
U
U
U
U
U
U
. U
U
U
U
U
U
U
U
U
U
U
u u u u u
u u
u u u u u u BJ
V
u
u u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/19/94
09/19/94
09/19/94
09/:L9/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
e/Recovery Data For Volatile Organics 8240S
Bromofluorobenzene
1,2-
pH (Soil)
•Dichloroetheme-d4
7.7 pH Unit
%Recovery
101
103
97.3
METHOD/CAS#
SW-846, 8240
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
09/14/94
TO 117
TO 121
TO 121
Ml'B SW-846,9045A
• Page ff: 14
October 18, 1994 10:43 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-2 LAUNDRY,GD 33,5 FT. Lab ID: 9409008-lOA CoUected: 09/13/94 11:03:00
TEST
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromome thane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
D ibromochlorometheme
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexanone
trems-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
09/21/94
U
18.8
11.3
U
U
U
U
U
U
U
U
U
U
U
U
U
u u u u u u u u u u
u u u u u
u u
u
u
u u
u 8 BJ
u u u u
u
u
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
1.7
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/21/94
09/23/94
09/23/94
09/23/94
09/23/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
09/19/94
BY
MTB
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01
10061-02
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
3050
6010
6010
6010
6010
8240
A w
-5
-6
Page ff: 15
October 18, 1994 10:43 CERTIFICATE OF ANALYSIS
RESUI.TS BY SAMPLE
Sample ID: M-2 LAUNDRY,GD 33,5 FT. Lab ID: 9409008-lOA Collected: 09/13/94 11:03:00
TEST RESULT UNITS DETECTION ANilJjYZED BY
LIMIT
METHOD/CAS#
Volatile Organics SW-846, 8240
Surrogate/Recovery Data For Volatilct Organics 8240S
Surrogate %Recovery
Toluene-d8 101
Bromofluorobenzene 103
l,2-Dichloroethane-d4 97.2
Recovery Limits
81 TO 117
74 TO 121
70 TO 121
pH (Soil) 7.6 pH Unit 09/14/94 MTB SW-846,9045A
Sample ID: M-2 LAUNDRY,GD 33,10 FT. Lab ID: 9409008-llA Collected: 09/13/94 11:10:00
TEST
Acid Digestion
Cadmium
H^Bjmlum
Lead
Silver
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2 -Chloroethylvinyl ether
Chloroform
Chlorometheme
D ibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexemone
trems-1,2-Dichloroethene
1,2-Dichloropropeme
RESULT
09/21/94
U
20.4
11.4
U
U
U
U
U
u u u u u u u u u u u
u
u
u u u u u
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
1.7
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/21/94
09/23/94
09/23/94
09/23/94
09/23/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
BY
MTB
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-84e, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
# Page ff: 16
October 18, 1994 10:43 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-2 LAUNDRY.GD 33,10 FT. Lab ID: 9409008-11A Collected: 09/13/94 11:10:00
TEST
Volatile Organics
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Tri chlorofluoromethane
vinyl Acetate
vinyl Chloride
o-Xylene
RESULT
4
Surrogat
Surrogate
Toluene-d8
u
u
u u u
u
u
u u u u u BJ
u u
u
u u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
09/20/94
e/Recovery Data For Volatile Organic
Bromofluorobenzene
1,2-
pH (Soil)
Dichloroetheme-d4
7.5 pH Unit
%Recovery
101
100
97.1
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
B B240S
METHOD/CAS#
SW-846, 8240
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits ^^
81
74
70
09/14/94
TO 117
TO 121
TO 121
MTB
^•^
SW-846,9045A
Sample ID: M-2 LAUNDRY,RINSATE BLANK Lab ID: 9409008-12A Collected: 09/13/94 11:40:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorometheme
Bromoform
Bromometheme
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2 -Chloroethylvinyl ether
RESULT
130
U
U
U
U
U
U
22
U
U
U
U
U
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/14/94
09/14/94
09/14/94
09/14/94
09/14/94
09/14/94
09/14/94
09/14/94
09/14/94
09/14/94
09/14/94
09/14/94
09/14/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
Page ff: 17
October 18, 1994 10:43 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-2 LAUNDRY,RINSATE BLANK Lab ID: 9409008-12A Collected: 09/13/94 11:40:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Chloroform
Chlorometheme
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
JUJ-' 1 -Trichloroethane
m^. 2 -Trichloroetheme
^1^^ chloroe thene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
D
u
u
u
u
u
u
u
u
u
u
u
u
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
SW-846, 8240
10 09/14/94 JMA 67-66-3
10 09/14/94 JMA 74-87-3
10 09/14/94 JMA 124-48-1
10 09/14/94 JMA 75-34-3
10 09/14/94 JMA 107-06-2
10 09/14/94 JMA 75-35-4
10 09/14/94 JMA 591-78-6
10 09/14/94 JMA 156-60-5
10 09/14/94 JMA 78-87-5
10 09/14/94 JMA 10061-01-5
10 09/14/94 JMA 10061-02-6
10 09/14/94 JMA 95-50-1
10 09/14/94 JMA 541-73-1
10 09/14/94 JMA 106-46-7
10 09/14/94 JMA 100-41-4
10 09/14/94 JMA 75-09-2
10 09/14/94 JMA 108-10-1
10 09/14/94 JMA 100-42-5
10 09/14/94 JMA 79-34-5
10 09/14/94 JMA 127-18-4
10 09/14/94 JMA 108-88-3
10 09/14/94 JMA 71-55-6
10 09/14/94 JMA 79-00-5
10 09/14/94 JMA 79-01-6
10 09/14/94 JMA 75-69-4
10 09/14/94 JMA 108-05-4
10 09/14/94 JMA 75-01-4
10 09/14/94 JMA 95-47-6
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate %Recovery
Toluene-d8 100
Bromofluorobenzene 102
l,2-Dichloroethane-d4 98.4
Recovery Limits
88 TO 110
86 TO 115
76 TO 114
Page#: 18
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identiTication criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1.1J with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as well as the sample.
E Estimated value. Result was outside of the calibration range but within the linear
range of the instrument.
BDL Indicates an analyte wliich was below the detection limits for the test.
NA Not applicable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
.^ike ^/^fk^ ^^^ Fn^-o /Pt :$/id'//'S
ENVIRONMENTAL LAB WORK REQUEST
1^^
^(7^P9/^^?
TmOKOL ENVIRONMENTAL LABORATORY LWR No. E10633
noM-. /I, E (AJ/huCe/L^ SSfO
COSTCB<TQI
l/po
WORKORDBl
/B9i/c> f'/S-fjC
ORGANIZATION ^/U(7/rzd ^^v^/^
RBVRT RESULTB TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE
f-/5'-f4
TYPE
y'
LOCATION
lU-lfA
TIME
[] niimiiffii
Df3/>
TEST REMARKS
C<//Cr,ApPi;, A/i -/PC/O
Vruu^^fl- 3 f-l ruJi ^
JL^ WIS 9
^'/S'9A y 7U-/'/A /7940 eJ, Cr, 4^ ji,^ 7//^ So JO
^
lOdt'l^i-^'f^'f4 uT M'21 /did Sh, Cc/, Cr, /{c^ t^lo - Son)
/
/
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* 'v F/'^SC ^o</f^ a/s^ o(2r/;^ 77//i7^ <ex/ra^/^j^i
CHAIN OF CUSTODY
- Rail UiuK Altd
RELINQUISHED BY
-^UJ/atii' >Vy^<-.,
DATE
9-(C^4
TIME
[Ci/t/C
REX:EIVEDBY
BWIWHIIIIII
^i^!
DATE
W/^/^\
TIME
/oii^r
FOR LABORATORY USE ONLY
DATE COMFUmOl DATERBVR1BD
October 19, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward
MIS 301
A.F. WALKER, MIS 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Anatytical Labs MIS 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Orders 9409009 Sample and Test Code Identification
Lab ID: Sample ID:
OIA M-19A DRYWELL, 1 FP.
Lab ID: Sample ID:
02A M-19A DRYWELL, 3 FT.
Test Codes and Names
Lab ID: Sample ID:
03A M-39 DRYWELL, 1 PT.
Lab ID: Sample ID:
04A M-39 DRYWELL, 3 FT.
Lab ID: Sample ID:
OIB M-19A DRYWELL, 1 FT.
Lab ID: Sample ID:
02B M-19A DRYWELL, 3 FT.
Lab ID: Sample ID:
OBB M-39 DRYWELL, 1 FT.
Lab ID: Sample ID:
04B M-39 DRYWELL, 3 FT.
3050
CD AE2
CR AE2
PB AE2
Nl AE2
AO AE2
Acid Digestion
Cadmium
Chromium
Lead
Nickel
Silver
Test Codes and Names
3050
CD AE2
CR AE2
PB AE2
NI AE2
AG AE2
Acid Digestion
Cadmium
Chromium
Lead
Nickel
Silver
Test Codes and Names
3050
SB AE2
CD AE2
CR AE2
PB AE2
AO AE2
Acid Digestion
Antimony
Cadmium
Chromium
Lead
Silver
Test Codes and Names
3050
SB AE2
CD AE2
CR AE2
PB~AE2
AO AE2
Acid Digestion
Antimony
Cadmium
Chromium
Lead
Silver
Test Codes and Names
AQ_AE2 Silver
Test Codes and Names
AG_AE2 Silver
Test Codes and Names
AG_AE2 Silver
Test Codes and Names
AG AE2 Silver
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010 Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010 Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010 Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010 Method
SW-846, 6010
Method
SW-846, 6010
Method
SW-846, 6010
Method
SW-846, 6010
Page #:1 of r
Workordfir CnrnmantJi
Report: NITRIC ACID WAS USED FOR THE SlLVEBl EXTRACTIONS ON
SAMPLES OIB, 02B, 03B, AND 04B.
Certifiedk^y
Page #:2
This is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: M-19A DRYWELL, 1 FT. Lab ID: 9409009-OlA Collected: 09/15/94 09:30:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
Chromium
Lead
Nickel
Silver
10/04/94
2.26
855
366
370
234
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
0.1
0.4
1.8
0.70
0.2
10/04/94
10/06/94
10/06/94
10/06/94
10/06/94
10/06/94
MWB
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
Sample ID: M-19A DRYWELL, 3 FT. Lab ID: 9409009-02A CoUected: 09/15/94 09:40:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
Chromium
Lead
Nickel
Silver
10/04/94
4.73
1510
325
395
253
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.3
0.51
0.2
10/04/94
10/06/94
10/06/94
10/06/94
10/06/94
10/06/94
MWB
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
Sample ID: M-39 DRYWELL, 1 FT. Lab ID: 9409009-03A CoUected: 09/15/94 10:10:00
TEST RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Acid Digestion
Antimony
Cadmium
Chromium
10/04/94
7.34
8.15
75.2
DATE
ug/g
ug/g
ug/g
3.4
0.1
0.3
10/04/94
10/06/94
10/06/94
10/06/94
MWB
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
Page ff: 3
October 19, 1994 14:09 CERTIFICATE OF ANAJLYSIS
RESUITS BY SAMPLE
Sample ID: M-39 DRYWELL, 1 FT. Lab ID: 9409009-03A CoUected: 09/15/94 10:10:00
TEST RESULT UNITS DETECTION A](T£LYZED BY
LIMIT
METHOD/CAS#
Lead
Silver
246
118
ug/g
ug/g
1.7
0.2
10/06/94
10/06/94
LVD
LVD
SW-846,
SW-846,
6010
6010
Sample ID: M-39 DRYWELL, 3 FT. Lab ID: 9409009-04A CoUected: 09/15/94 10:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Antimony
Cadmium
Chromium
Lead
#^
10/04/94
5.99
2.75
26.4
156
43.6
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
2
0,
0,
1,
0.
.7
.1
.3
.4
,2
10/04/94
10/06/94
10/06/94
10/06/94
10/06/94
10/06/94
MWB
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
Sample ID: M-19A DRYWELL, 1 FT. Lab ID: 9409009-OlB CoUected: 09/15/94 09:30:00
TEST RESULT UNITS DETECTION Al^ALYZED BY
LIMIT
METHOD/CAS#
Silver 7140 ug/g 0.3 10/12/94 LVD SW-846, 6010
Sample ID: M-19A DRYWELL, 3 FT. Lab ID: 940^)009-026 CoUected: 09/15/94 09:40:00
TEST RESULT UNITS DETECTION AI7ALYZED BY
LIMIT
METHOD/CAS#
Silver 53500 ug/g 0.3 10/12/94 LVD SW-846, 6010
Page ff: 4
October 19, 1994 14:09 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-39 DRYWELL, 1 FT. LabID: 9409009-03B CoUected: 09/15/94 10:10:00
TSST RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Silver 255 ug/g 0.3 10/12/94 LVD SW-846, 6010
Sample ID: M-39 DRYWELL, 3 FT. LabID: 9409009-04B CoUected: 09/15/94 10:20:00
TEST RESULT tINITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Silver 114 ug/g 0.3 10/12/94 LVD SW-846, 6010
Page ff: 5
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates conipound was below detection liniit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identiHed compounds or when the mass spjctral data indicated the presence of a
compound that meets the identiftcation criteria but the: result is less than the specified
detection limit but greater than zero. (e.g. l.U with a detection limit of 5.0)
B This flag is used when an analyte is found iii the blanlc as weU as the sample.
E Estimated value. Result was outside of the <;aUbration rainge but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limit!? for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
•
ENVIRONMENTAL LAB WORK REQUEST
I^P ^<^/f^/4^
TfflOKOL ENVIRONMENTAL LABORATORY LWR No. El0635
/. r. UJAuceR-
EVTDQION OOSTCBnER WORK OROGR
/S<?4o f v^- ^^
ORGANIZATION
£./?(/1 ro Efn<^ir
^
3ol£'
REPORT RESULTS TO:
HELEN WARD, MS 301
SAMPLE INFORMATIION
SAMPLE
\y
2. 5tt>AU 40 ;z_
PATE
^^''^<f
TYPE
6^
LOCATION
T-S/A
TIME
/ZCo
TEST
imiDi
^L, Ph ~f>o/o ^ <^,.^_4-
REMARKS
// f /3/0 r I
^ i^ /( /-^zo //'
1/
!w^
/f i^ /'I /37\ / I
f>i,^Be Cu,-5i,,sA,/is] <7''ji/'>>j
y Of/iO ^^<^, Sf/tit -i/oc , Cti. Cr, /*,
l^ /ii/(^ //
y \yMiHuftu/tlrt
Ar^^ ISK&UX> Sfi. y ^yjr /f
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\<tru. ^Kaidn hA. y" //IOO /I
Z^Ji. , [Oiaifoda^ 7*<
I££^ y' /040 /(
•Sbs MsfyKcfrtrtj -^H (40 raa IAI/. 1 xi
CHAIN OF CUSTODY
RELINQUISHED BY
.^^IML
DATE
^'71-^
TIME
/7<d
RECEIVED BY DATE
^-f^>/>-f^
TIME
//•^
FOR LABORATORY USE ONLY
DATECOMFUCTGD DA1ERa>ORTES
November 28, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward
MIS 301
A.F. WALKER, MIS 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham aty. Ut 84302-0707
Anatytical Labs MIS 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Orders}' 9409014
LabID: Sample ID:
OIA T-51A, FT OF DIS SURFACE
LabID: Sample ID:
02A T-51A, PT OF DIS 2 FT.
Sample and Test Code Identification
Test Codes and Names
LabID: SMnple ID:
03A T-51A,25FT. DN ORD SURF.
LabID: Sample ID:
04A T-51A, 25 FT. DN GRD 2 FT.
LabID: .Sample. TD:
~05A MFG . AREA BKGND SURFACE.
S04IC1
3050
SB AE2
PB"AE2
pri^s
Sulfate
Acid Digestion
Antimony
Lead
pH (SoU)
Test Codes and Names
S04IC1
3050
SB AE2 PB AE2 PH~S
Sulfate
Acid Digestion
Antimony Lead
pH (Soil)
Test Codes and Names
S04IC1
3050
SB AE2
PB~AE2
PH_S
Sulfate
Acid Digestion
Antimony
Lead
pH (SoU)
Test Codes and Names
S04IC1
3050
SB AE2
PB AE2
PH_S
Sulfate
Acid Digestion
Antimony
Lead
pH (SoU)
Test Codes and Names
S04IC1
CL04
HMX
NO
3050
SB A£2
BE AE2
B AE2
Cb AE2
CR AE2
CU~AE2
PB"AE2
MN AE2
Nl AE2
AG AE2
ZN AE2
AS GF2
HO CV2
SE GF2
TL GF2
824DS
8270S
CN AU2
PH~S
Sulfate
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Antimony
Beryllium
Boron
Cadmium
Chromium
Copper
Lead
Manganese
Nickel
SUver
Zinc
Arsenic
Mercuty
Selenium
Thallium
VolatUe Oiganics
Semi-VolatUe Organics
Total Cyanide
pH (SoU)
Method
EPA 300.0
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846,9045A Method
EPA 300.0
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846,9045A
Method
EPA 300.0
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846,9045A Method
EPA 300.0
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846,9045A
Method
EPA 300.0
SOP 314
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 7841
SW-846, 8240
SW-846, 8270
SW-846, 9012
SW-846,9045A
Page#:lof '^^
Work Order # 9409014 Sample and Test Code Identification
•
abID:
06A
Sample ID:
MFG. AREA BKGND 2 FT.
LabID:
07A
Sample ID:
MFG. AREA BKGND 5 FT.
LabID:
08A
Sample ID:
MFG. AREA BKGND 10 FT.
Test Codes and Names
S04IC1
CL04
HMX
NG
3050
SB AE2
BE AE2
B AE2
CD AE2
CR AE2
CU AE2
PB AE2
MN AE2
Nl AE2
AG AE2
ZN AE2
AS OF2
HG CV2
SE GF2
TL GF2
8240s
8270S
CN AU2
PH_S
Sulfate
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Antimony
Betyllium
Boron
Cadmium
Chromium
Copper
Lead
Manganese
Nickel
Silver
Zinc
Arsenic
Mercury
Selenium
Thallium
Volatile Organics
Semi-Volatile Organics
Total Cyanide
pH (Soil)
Test Codes and Names
S041C1
CL04
HMX
NG
3050
SB AE2
BE~AE2
B AE2
CD AE2
CR AE2
CU AE2
PB AE2
MN AE2
NI AE2
AG AE2
ZN AE2
AS OF2
Hd"CV2
SE GF2
TL GF2
8240s
8270S
CN AU2
PH_S
Sulfate
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Antimony
Beryllium
Boron
Cadmium
Chromium
Copper
Lead
Manganese
Nickel
Silver
Zinc
Arsenic
Mercury
Selenium
Thallium
Volatile Organics
Semi-Volatile Organics
Total Cyanide
pH (Soil)
Test Codes and Names
S04IC1
CL04
HMX
NG
3050
SB AE2
BE AE2
B AE2
CD AE2
CR AE2
CU AE2
PB AE2
MlT AE2
NI AE2
AG AE2
ZN AE2
AS GF2
HG CV2
SE'aF2
TL GF2
824&S
8270S
CN AU2
Sulfate
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Antimony
BeiyUium
Boron
Cadmium
Chromium
Copper
Lead
Manganese
Nickel
Silver
Zinc
Arsenic
Mercuiy
Selenium
Thallium
VolatUe Organics
Semi-Volatile Organics
Total Cyanide
Method
EPA 300.0
SOP 314
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 7841
SW-846, 8240
SW-846, 8270
SW-846, 9012
SW-846,9045A
Method
EPA 300.0
SOP 314
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 7841
SW-846, 8240
SW-846, 8270
SW-846, 9012
SW-846,9045A
Method
EPA 300.0
SOP 314
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 7841
SW-846, 8240
SW-846, 8270
SW-846, 9012
Page #:2
Work Order jj^ 9409014 Sample and Test Code Identification
LabID:
08A
LabID:
09A
Sample ID:
MFG. AREA BKGND 10 FT.
Sample ID:
MFG. AREA BKGND 15 FT.
Test Codes and Names
LabID:
lOA
Sample ID:
Q.C. STANDARDS
PH_S pH (Soil)
Test Codes and Names
S04IC1
CL04
HMX
NG
3050
SB AE2
BE~AE2
B AE2 CD AE2
CR AE2
CU AE2
PB AE2
MN AE2
Nl AE2
A<TAE2
ZN AE2
AS OF2
HG CV2
SE GF2
TL OF2
824DS
8270S
CN AU2
PH_S
Sulfate
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Antimony
BeryUium
Boron Cadmium
Chromium
Copper
Lead
Manganese
Nickel Silver
Zinc
Arsenic
Mercury
Selenium
ThaUium
VolatUe Organics
Semi-Volatile Oiganics
Total Cyanide
pH (Soil)
Test Codes and Names
AL AE2
SB AE2
BA AE2 BE AE2
CD AE2
CA AE2
CR AE2
CO~AE2
CU AE2
FE AE2
PB"AE2
M<J AE2
MN AE2
MO"AE2
NI AEZ
K AE2
AG AE2
NA AE2
V AE2
ZR AE2
AS~0F2
HO CV2
SE OF2 TL"OF2
8080
8240S
8270S
CN AU2
Aluminum
Antimony
Barium Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
SUver
Sodium
Vanadium
Zinc
Arsenic
Mercury
Selenium ThaUium
Chlorine Pesticides/PCBs
VolatUe Organics
Semi-VolatUe Oiganics
Total Cyanide
6010
,6010
,6010
6010
Method
SW-846,9045A
Method
EPA 300.0
SOP 314
SOP 420
SOP 420
SW-846, 3050
SW-846,
SW-846,
SW-846,
SW-846,
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 7841
SW-846, 8240
SW-846, 8270
SW-846, 9012
SW-846,9045A Method
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
7060
7471
7740
7841
8080
8240
8270
9012
Page #:3
Workorder Comments
Report: Initial run for metals was on 10/10/94. Second run data is
reported except in a few instances.
Certrie^?^
Page #:4
This is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: T-51A, PT OF DIS SURFACE Lab ID: 9409014-OlA CoUected: 09/19/94 12:50:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Sulfate
Acid Digestion
Antimony
Lead
pH (Soil)
48.8
10/04/94
7.96
9.99
8.11
ug/g
DATE
ug/g
ug/g
pH Unit
3
3.3
1.6
10/26/94
10/04/94
10/10/94
10/10/94
09/22/94
CRS
MWB
LVD
LVD
AA
EPA 300.0
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846,9045A
Sample DO: T-51A, FT OF DIS 2 FT. LabID: 9409014-02A Collected: 09/19/94 13:10:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Sulfate
Acid Digestion
Antimony
Lead
pH (Soil)
126
10/04/94
9.58
4.18
8.09
ug/g
DATE
ug/g
ug/g
pH Unit
3
3.5
1.7
10/26/94
10/04/94
10/10/94
10/10/94
09/22/94
CRS
MWB
LVD
LVD
AA
EPA 300.0
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846,9045A
Sample ID: T-51 A, 25 FT. DN GRD SURF. Lab ID: 9409014-03A CoUected: 09/19/94 13:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Sulfate
Acid Digestion
Antimony
Lead
pH (Soil)
583.4
10/04/94
7.69
9.92
8.69
ug/g
DATK
ug/g
ug/g
pH Unit
3
3.1
1.6
10/26/94
10/04/94
10/10/94
10/10/94
09/22/94
CRS
MWB
LVD
LVD
AA
EPA 300.0
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846,9045A
Page ff: 5
November 28, 1994 12:41 CERTIFICATE OF A^fi^JLYSIS
RESULTS BY SAMPLE
Sample ID: T-51 A, 25 FT. DN GRD 2 FT. Lab ID: 9409014-04A Collected: 09/19/94 13:25:00
TEST RESULT UNITS DETECTION ANlLLYZED BY
LIMIT
METHOD/CAS#
Sulfate
Acid Digestion
Antimony
Lead
pH (Soil)
164
10/04/94
6.88
7.92
7.85
ug/g
DATE
ug/g
ug/g
pH Unit
2
3.2
1.6
10/26/94
10/04/94
10/10/94
10/10/94
09/22/94
CRS
MWB
LVD
LVD
AA
EPA 300.0
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846,9045A
Sample ID: MFG. AREA BKGND SURFACE. Lab ID: 9409014-05A CoUected: 09/21/94 09:00:00
TEST RESULT UNITS DETECTION AtTJJLiYZED BY
LIMIT
METHOD/CAS#
Sulfate
Perchlorate
Nitroglycerine
Acid Digestion
Antimony
Beryllium
Boron
Cadmium
Chromium
Copper
Lead
Manganese
Nickel
Silver
Zinc
•
28
U
U
D
10/04/94
10.4
0.67
10.1
0.22
17.2
U
14.8
340
10.3
U
52.5
ug/g
ug/g
ug/g
ug/g
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
3
4.5
.01
.02
3.4
0.1
0.4
0.1
0.3
0.1
1.7
0.1
0.69
0.2
0.3
Page ff: 6
10/26/94
11/10/94
09/27/94
09/27/94
10/04/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
CRS
CRS
CFP
CFP
MWB
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
EPA 300.0
SOP
SOP •
SOP •
SW-846,
SW-846,
SW-846,
SW-84 6,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
314
420
420
3050
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
November 28, 1994 12:41 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MFG. AREA BKGND SURFACE. Lab ID: 9409014-05A CoUected: 09/21/94 09:00:00
TEST
Arsenic
Mercury
Selenium
Thallium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2 -Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
13.06
D
0.924
0.36
37
U
U
U
D
O
U
11
o
U
U
U
D
D
D
U
D
D
D
D
D
U
D
U
U
U
U
U
D
U
U
D
D
D
D
D
D
D
U
D
D
UNITS
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.092
0.022
0.073
0.12
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/23/94
10/06/94
10/25/94
10/25/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
BY
CRS
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA.
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-84e,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01
10061-02
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
7060
7471
7740
7841
8240
^^^ 19
-5
-6
Page ff: 7
November 28, 1994 12:41 CERTIFICATE OF ANALYSIS
' • ' RESULTS BY SAMPLE
.Sample ID: MFG. AREA BKGND SURFACE. Lab ID: 9409014-05A CoUected: 09/21/94 09:00:00
TEST RESULT
Volatile Organics
UNITS DETECTION
LIMIT
ANALYZED BY
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
Seml-Volatlle Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
J^achloroe thane
J^BL obenz ene
^Hphorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2 -Chloronaphthalene
2-Nitroemiline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
U
U
U
D
D
D
D
U
U
U
D
D
D
U
U
D
D
U
U
U
U
U
U
U
U
D
D
D
U
U
U
U
u. U
D
U
U
D
U
U
U
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
99.1
90.6
98.1
50
330
330
190
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
79
99
63
190
63
140
METHOD/CAS#
SW-846, 8240
»
Recovery Limits
81
74
70
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
• Page ff: 8
November 28, 1994 12:41 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MFG. AREA BKGND SURFACE. Lab ID: 9409014-05A CoUected: 09/21/94 09:00:00
TEST
Seml-Volatlle Organics
Fluorene
4 -Nitroemiline
4,6-Dinitro-2-methylphenol
n- Ni trosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
bis(2-Ethylhexyl)phthalate
Chrysene
Di-n-octylphthalate
Benzo[b&k]fluoranthene
Benzo faJ pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h]anthracene
Benzo[g,h,i]perylene
RESULT
U
U
U
U
D
U
U
U
U
U
D
D
U
U
D
U
U
D
U
U
D
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Phenol -d5
Nitrobenzene -d5
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terpheny1-dl4
Total Cyanide
pH (Soil) 7.
U
49
ug/g
pH Unit
DETECTION
LIMIT
63
120
790
63
63
63
120
180
63
83
73
63
83
260
83
83
83
160
83
120
83
140
ANALYZED
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MHR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For Seml-Volatlle Organics 8270S '^^
%Recovery
40.88
47.75
65.50
72.98
59.35
98.47
0.250
Recovery Limits
25
24
23
30
19
18
10/04/94
09/22/94
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
KEN
AA
SW-846, 9012
SW-846,9045A
Sample ID: MFG. AREA BKGND 2 FT. LabID: 9409014-06A CoUected: 09/21/94 09:16:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/C:AS#
Sulfate
Perchlorate
HMX
29
U
U
ug/g
ug/g
ug/g
2
5.0
.01
10/26/94
11/10/94
09/27/94
CRS
CRS
CFP
EPA 300.0
SOP 314
SOP 420
Page ff: 9
November 28, 1994 12:41 CERTIFICATE OF AN^LLYSIS
RESULTS BY SAMPLE
Sample ID: MFG. AREA BKGND 2 FT. LabID: 9409014-06A CoUected: 09/21/94 09:16:00
TEST
Ni troglycerine
Acid Digestion
Antimony
Beryllium
Boron
Cadmium
Chromium
Copper
Lead
Manganese
Nickel
^^^«rer
Zinc
Arsenic
Mercury
Selenium
Thallium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorometheme
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2 -Chloroethylvinyl ether
Chloroform
Chlorometheme
RESULT
U
10/04/94
9.15
0.77
12.5
0.65
20.3
U
8.87
333
14.5
U
50.7
5.54
U
0.62
0.36
U
U
U
U
U
U
U
U
U
U
u
u u u u
UNITS
ug/g
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
.02
3.3
0.1
0.4
0.1
0.3
0.1
1.7
0.1
0.66
0.2
0.3
0.098
0.024
0 .079
0.13
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANJU^YZED
09/27/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/23/94
10/06/94
10/25/94
10/25/94
10/03/94
10/C3/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
BY
CFP
MWB
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-84 6,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
3050
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
7060
7471
7740
7841
8240
Page ff: 10
November 28, 1994 12:41 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MFG. AREA BKGND 2 FT. LabID: 9409014-06A CoUected: 09/21/94 09:16:00
TEST
Volatile Organics
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trems-l,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
Tri chlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
-
7.9
U
u u u u u u
u D
U
D
U
U
U
D
U
U
V
U
BJ
U
U
D
U
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene -d8
Bromofluorobenzene
1,2-Dichloroethane-d4
Semi-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Ni troso-di-n-propylamine
Hexachloroetheme
Nitrobenzene
Isophorone
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
101
96.0
99.2
50
330
330
190
110
63
150
150
63
76
190
130
400
53
46
73
METHOD/CAS#
SW-846, 8240
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4 ^^
108-05-4 ^V
75-01-4
95-47-6
Recovery Limits
81
74
70
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
Page#: 11
November 28, 1994 12:41 CERTIFICATE OF ANALYSIS
i i RESULTS BY SAMPEE
Sample ID: MFG. AREA BKGND 2 FT. LabID: 9409014-06A CoUected: 09/21/94 09:16:00
TEST
Semi-Volatile Organics
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)metheme
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4 -Chloroemi1ine
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroemiline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Sjl^^'^nz of uran
•^•Dinitrotoluene
z^- Dini trotoluene
Diethylphthalate
4 -Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
n-Nitrosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenemthrene
Anthracene
Di-n-butylphthalate
Fluoremthene
Pyrene
Butylbenzylphthalate
Benzo[a] emthracene
bis (2-Ethylhexyl)phthalate
Chrysene
Di-n-octylphthalate
Benzo[b&k]fluoremthene
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h] emthracene
Benzo[g,h,i]perylene
RESULT
U
U
U
U
u u u u u u u D
u
u u
u
u
u.
u u u
u u u u u
u u u u
u
u
u D
u
u D
u u
u u 460
U
u u u u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
14 00
79
99
63
190
63
140
63
120
790
63
63
63
120
180
63
83
73
63
83
260
83
83
83
160
83
120
83
140
ANALYZED
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
• Page ff: 12
November 28, 1994 12:41 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MFG. AREA BKGND 2 FT. LabID: 9409014-06A CoUected: 09/21/94 09:16:00
TEST
Semi-Volatile
Total Cyanide
pH (Soil)
RESULT
Organics
UNITS
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Phenol-d5
Nitrobenzene-d5
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
u
7.56
ug/g
pH Unit
DETECTION
LIMIT
ANALYZED BY METHOD/CAS#
SW-846, 8270
For Semi-Volatile Organics 8270S
%Recovery
45.79
50.15
66.84
73.72
67.19
87.83
0.250
Recovery Limits
25 TO 121
24 TO 113
23 TO 120
30 TO 115
19 TO 122
18 TO 137
10/04/94 KEN
09/22/94 AA
SW-846, 9012
SW-846,9045A
Sample ID: MFG. AREA BKGND 5 FT. LabID: 9409014-07A CoUected: 09/21/94 09:35:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Sulfate
Perchlorate
Nitroglycerine
Acid Digestion
Antimony
Beryllium
Boron
Cadmium
Chromium
Copper
Lead
Manganese
25
U
U
U
10/10/94
6.80
0.83
15.4
D
22.5
U
9.87
324
ug/g
ug/g
ug/g
ug/g
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
3
4.3
.01
.02
3.5
0.1
0.4
0.1
0.4
0.1
1.8
0.1
10/26/94
11/10/94
09/27/94
09/27/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
CRS
CRS
CFP
CFP
MWB
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
EPA 300.0
SOP
SOP
SOP
SW-846
SW-846
SW-846
SW-846
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
314
420
420
3050
6010
6010
6010
6010
6010
6010
6010
6010
Page ff: 13
November 28, 1994 12:41 CERTIFICATE OF AN^I^YSIS
RESULTS BY SAMPLE
Sample ID: MFG. AREA BKGND 5 FT. Lab ID: 9409014-07A CoUected: 09/21/94 09:35:00
TEST
Nickel
Silver
Zinc
Arsenic
Mercury
Seleniiun
Thallium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
^-nmometheme
^^^jtanone
^l^bon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2 -Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3 TDichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
RESULT
14.6
U
49.3
5.77
U
0.639
0.45
1.4 J
U
U
u u u
u u u D
U
U
U
U
U
U
U
u u
u u u u
u u u u u
u u
u
u u
u
u u u
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.70
0.2
0.3
0.094
0.025
0.075
0.13
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANJkLYZED
10/10/94
10/10/94
10/10/94
10/23/94
10/06/94
10/25/94
10/25/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
BY
LVD
LVD
LVD
CRS
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
OMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01'
10061-02-
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
6010
6010
6010
7060
7471
7740
7841
8240
-5
-6
Page ff: 14
November 28, 1994 12:41 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MFG. AREA BKGND 5 FT. Lab ID: 9409014-07A CoUected: 09/21/94 09:35:00
TEST RESULT
Volatile Organics
Tri chlorof1uoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
u U
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
ANALYZED
10/03/94
10/03/94
10/03/94
10/03/94
BY
JMA
JMA
JMA
JMA
Surrogate/Recovery Data Por Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
Semi-Volatile Organics
Phenol
Pyridine
Aniline
bis (2-Chloroethyl) et:her
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-prppylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4 -Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2 -Chloronaphthalene
2 -Ni troani1ine
Dimethylphthalate
Acenaphthylene
3-Nitroemiline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
U
U
U
O
U
U
U
U
U
U
u U
u U
D
U
U
U
U
u u
u u
u D
0
D
U
U
D
u U
U
u u D
u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
104
97.1
99.9
50
330
330
190
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
79
METHOD/rAS#
SW-846, 8240
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1 J^
95-48-7 ^B
108-60-1 ^^
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
Page ff: 15
November 28, 1994 12:41 CERTIFICATE OF ANALYSIS
'i' RESULTS BY SAMPLE
Sample ID: MFG. AREA BKGND 5 FT. LabID: 9409014-07A CoUected: 09/21/94 09:35:00
TEST RESULT UNITS DETECTION AITALYZED BY
LIMIT
METHOD/CAS#
Semi-Volatile Organics
Dibenzofurem
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
n-Nitrosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoremthene
Pyrene
Butylbenzylphthalate
Benzo[a] emthracene
bis(2-Ethylhexyl)phthalate
Chrysene
Di-n-octylphthalate
•
>^o [b&k] fluoranthene
EO[a]pyrene
eno[1,2,3-cd]pyrene
Dibenz[a,h] emthracene
Benzo[g,h,i]perylene
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
SW-846, 8270
99 09/27/94 MMR 132-64-9
63 09/27/94 MMR 606-20-2
190 09/27/94 MMR 121-14-2
63 09/27/94 MMR 84-66-2
140 09/27/94 MMR 7005-72-3
63 09/27/94 MMR 86-73-7
120 09/27/94 MMR 100-01-06
790 09/27/94 MMR 534-52-1
63 09/27/94 MMR 86-30-6
63 09/27/94 MMR 101-55-3
63 09/27/94 MMR 118-74-1
120 09/27/94 MMR 87-86-5
180 09/27/94 MMR 85-01-8
63 09/27/94 MMR 120-12-7
83 09/27/94 MMR 84-74-2
73 09/27/94 MMR 206-44-0
63 09/27/94 MMR 129-00-0
83 09/27/94 MMR 85-68-7
260 09/27/94 MMR 56-55-3
83 09/27/94 MMR 117-81-7
83 09/27/94 MMR 218-01-9
83 09/27/94 MMR 117-84-0
160 09/27/94 MMR 205-99-2/2
83 09/27/94 MMR 50-32-8
120 09/27/94 MMR 193-39-5
83 09/27/94 MMR 53-70-3
140 09/27/94 MMR 191-24-2
Surrogate/Recovery Data For Sami-Volatile Organics 8270S
Total Cyanide
pH (Soil)
Surrogate
2 -Fluorophenol
Phenol-d5
Nitrobenzene-ds
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
1.14 ug/g
7.72 pH Unit
%Recovery
44.44
49.67
67.09
74.22
63.98
90.32
Recovery Limits
25 TO 121
24 TO 113
23 TO 120
30 TO 115
19 TO 122
18 TO 137
0.250 10/04/94 KEN SW-846, 9012
09/22/94 AA SW-846,9045A
Page ff: 16
November 28, 1994 12:41 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MFG. AREA BKGND 10 FT. LabID: 9409014-08A CoUected: 09/21/94 10:00:00
TEST
Sulfate
Perchlorate
HMX
Nitroglycerine
Acid Digestion
Antimony
Beryllium
Boron
Cadmitun
Chromium
Copper
Lead
Manganese
Nickel
Silver
Zinc
Arsenic
Mercury
Selenium
Thallium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromoform
Bromomethane
2-Butemone
RESULT
46
U
U
U
10/10/94
12.4
1.02
14.3
0.73
18.4
U
8.15
289
10.9
U
37.5
7.98
D
0.58
0.46
1.1 BJ
U
U
U
U
D
U
U
UNITS
ug/g
ug/g
ug/g
ug/g
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
3
4.8
.01
.02
3.7
0.1
0.4
0.1
0.4
0.1
1.9
0.1
0.75
0.2
0.3
0.089
0.028
0.071
0.12
10
10
10
10
10
10
10
10
ANALYZED
10/27/94
11/10/94
09/27/94
09/27/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/23/94
10/06/94
10/25/94
10/25/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
BY
CRS
CRS
CFP
CFP
MWB
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METEOD/CAS#
EPA 300.0
SOP 314
SOP 420
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
3050
6010
6010
6010
6010
6010
6010
6010 ^P
6010
6010
6010
6010
7060
7471
7740
7841
8240
Page ff: 17
November 28, 1994 12:41 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MFG. AREA BKGND 10 FT. Lab ID: 9409014-08A CoUected: 09/21/94 10:00:00
TEST RESULT
Volatile Organics
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexanone
trans-l,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3 -Di chlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
^ll^rene
^I^P, 2,2 -Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane 4.4
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
U
U
U
U
U
U
U
U ,
U
U
U
U
U
U
u U
u u u u u u u u . u
u BJ
•u
- u
u D
u .
u
UNITS
ug/Kg
, ug/Kg
ug/Kg
ug/Kg
ug/Kg
. ug/Kg
ug/Kg
ug/Kg
. ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
A](TJ)LYZED
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
Semi-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
u , u
: u
u u u u . u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
102
98.3
100
50
330
330
190
110
63
150
150
63
METHOD/CAS#
SW-846, 8240
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
• Page #: 18
November 28, 1994 12:41 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MFG. AREA BKGND 10 FT. Lab ID: 9409014-08A CoUected: 09/21/94 10:00:00
TEST
Semi-Volatile Organics
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroetheme
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroemiline
Hexachlorobutadiene
4 -Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyc1opentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroemiline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofurem
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4 -Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
n-Ni trosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoremthene
Pyrene
ButyIbenzyIphthalate
Benzo[a]anthracene
bis(2-Ethylhexyl)phthalate
Chrysene
Di-n-octylphthalate
Benzo[b&k]fluoremthene
RESULT
U
U
U
u u u
u u D
U
u
u u u u D
U
U
U
U
D
U
U
U
U
U
U
U
U
U
u U
u
u u u
u D
u U
U
u U
u
u u u D
u u D
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION ANALYZED
LIMIT
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
79
99
63
190
63
140
63
120
790
63
63
63
120
180
63
83
73
63
83
260
83
83
83
160
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS*
SW-846, 8270
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4 ggj^
131-11-3 Hip
208-96-e ^"^
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
Page ff: 19
November 28, 1994 12:41 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MFG. AREA BKGND 10 FT. LabID: 9409014-08A CoUected: 09/21/94 10:00:00
TEST RESULT
Semi-Volatile Organics
Benzo[a]pyrene U
Indeno[1,2,3-cd]pyrene U
Dibenz[a,h]anthracene U
Benzo[g,h,i]perylene U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Phenol-d5
Nitrobenzene-dS
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Te rphenyl-dl4
Total Cyanide U
pH (Soil) 7.64
ug/g
pH Unit
DETECTION
LIMIT
83
120
83
140
AllTALYZED BY
09/2 7/94 MMR
09/27/94 MMR
09/27/94 MMR
09/27/94 MMR
METHOD/CAS#
SW-846, 8270
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270S
%Recovery
51.95
55.71
7S.12
78.89
66.07
96.38
0.250
Recovery Limits
25 TO 121
24 TO 113
23 TO 120
30 TO 115
19 TO 122
18 TO 137
10/04/94 KEN
09/22/94 AA
SW-846, 9012
SW-846,9045A
(Hiple ID: MFG. AREA BKGND 15 FT. Lab ID: 9409014-09A CoUected: 09/21/94 10:40:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Sulfate
Perchlorate
HHZ
Nitroglycerine
Acid Digestion
Antimony
Berylliiiffl
Boron
Cadmium
Chromium
Copper
148
U
D
. U
10/10/94
8.09
1.06
13.7
0.31
21.1
U
ug/g
ug/g
ug/g
ug/g
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
3
4.8
.01
.02
3.2
0.1
0.4
0.1
0.3
0.1
10/26/94
11/10/94
09/27/94
09/27/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
CRS
CRS
CFP
CFP
MWB
LVD
LVD
LVD
LVD
LVD
LVD
EPA 300.0
SOP
SOP
SOP
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
314
420
420
, 3050
, 6010
, 6010
, 6010
, 6010
, 6010
, 6010
Page ff: 20
November 28, 1994 12:41 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MFG. AREA BKGND 15 FT. LabID: 9409014-09A CoUected: 09/21/94 10:40:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Lead
Manganese
Nickel
Silver
Zinc
Arsenic
Mercury
Selenium
Thallium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorometheme
Bromoform
Bromometheme
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
D ibromochlorome thane
1,1-Dichloroethane
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trans-l,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2-Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
9.53
286
10.1
U
43.9
11.85
U
1.14
0.51
11
O
U
u u
u
u D
u U
U
U
U
U
u u u u u u
u u
u D
u u u u 2.2 J
U
U
U
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
1.6
0.1
0.65
0.2
0.3
0.10
0.027
0.12
0.14
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/23/94
10/06/94
10/25/94
10/25/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 7841
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
Page ff: 21
November 28, 1994 12:41 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sumple ID: MFG. AREA BKGND 15 FT. Lab ID: 9409014-09A CoUected: 09/21/94 10:40:00
TEST RESULT
Volatile Organics
Te t rachl or oe thene
Toluene
1,1,1-Trichloroethane 5.0
1,1,2-Trichloroetheme
Trichloroethene.
Trichlorofluoromethane
vinyl Acetate
Vinyl Chloride
o-Xylene
U
U
BJ
U
U
U
u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
ANALYZED
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
10/03/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
Semi-Volatile Organics
Phenol
Pyridine
Aniline
J|^(2-Chloroethyl) ether
I^B ilorophenol
i^-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis (2-Chloroisopropyl)ethe
4 -rMethy Iphenol
n-Nitroso-di-n-propylamine
Hexachloroetheme
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis (2-Chloroethoxy)metheme
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroemiline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2 -Chloronaphthalene
2-Ni troani1ine
D ime thyIphthalate
u . u
u u
u u
u u
u
u u u u u D
u
u
u u u
u u u u u u u u
u u
u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
103
98.7
99.7
50
330
330
190
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
METHOD/CAS#
SW-846, 8240
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
Page ff: 22
November 28, 1994 12:41 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: MFG. AREA BKGND 15 FT. Lab ID: 9409014-09A v CoUected: 09/21/94 10:40:00
TEST
Semi-Volatile Organics
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroemiline
4,6-Dinitro-2-methylphenol
n-Ni trosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoremthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
bis(2-Ethylhexyl)phthalate
Chrysene
Di-n-octylphthalate
Benzo [b&k] fluoremthene
Benzo [a] pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h] emthracene
Benzo[g,h,i]perylene
REStJLT
u U
U
u u u u u u u u u u D
u u u D
u u u D
u U
U
U
u u D
u U
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Phenol -d5
Nitrobenzene -d5
2 -Fluorobiphenyl
2,4,6-
Terphe
Tribromophenol
nyl-dl4
DETECTION
LIMIT
120
79
63
1400
79
99
63
190
63
140
63
120
790
63
63
63
120
180
63
83
73
63
83
260
83
83
83
160
83
120
83
140
ANALYZED
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7 ^^
56-55-3 ^V
117-81-7 ^
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For Seml-Volatlle Organics 8270S
%Recovery
46.16
48.02
62.53
65.63
57.87
79.22
Recovery Limits
25
24
23
30
19
18
TO 121
TO 113
TO 120
TO 115
TO 122
TO 137
Total Cyanide
pH (Soil)
0.98 ug/g
7.68 pH Unit
0.250 10/04/94 KEN SW-846, 9012
09/22/94 AA SW-846,9045A
Page ff: 23
November 28, 1994 12:41 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: Q.C. STANDARDS
TEST
,•>...:-..
RESULT
•.I LabID: 9409014-lOA
UNITS DETECTION ANALYZED BY
LIMIT
CoUected:
METHOD/CAS#
Aluminum
Antimony
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
M
^l^fneslum
Manganese
Molybdenum
Nickel
Potassium
Silver
Sodium
Vanadium
Zinc
Arsenic
Mercury
Selenium
Thallium
7090
43 .5
.305
96.4
104
3440
165
94.3
105
10500
147
2100
207
190
149
3100 •
87.2
725
70.5
113
135.1
5.08
97.2
82.1
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
1.7
3.2
0.07
0.1
0.1
0.66
0.3
0.2
0.1
0.3
1.7
0.07
0.1
0.2
0.66
26.4
0.2
0.66
0.2
0.3
0.11
0.028
0.084
1.0
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/:L7/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/14/94
10/06/94
11/21/94
11/23/94
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
7060
7471
7740
7841
Page ff: 24
November 28, 1994 12:41 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: Q.C. STANDARDS LabID: 9409014-lOA CoUected:
TEST _-
Chlorine Pesticides/PCBs
alpha-BHC
gamma-BHC (lindane)
beta-BHC
Heptachlor
delta-BHC
Aldrin
Heptachlor epoxide
Endosulfem I
4,4'-DDE
Dieldrin
Endrin
4,4'-DDD
Endosulfem II
4,4'-DDT
Endrin aldehyde
Endosulfan sulfate
Endrin ketone
4.4'-Methoxychlor
Chlordane
Toxaphene
PCB-1016
PCB-1221
PCB-1232
PCB-1242
PCB-1248
PCB-1254
PCB-1260
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromometheme
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
RESULT
U
0.476
0.192
0.334
U
0.252
U
U
0.566
0.114
0.554
0.423
U
0.327
U
U
U
D
U
U
U
U
U
U
U
U
U
UNITS
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
DETECTION
LIMIT
0.0040
0.0040
0.0060
0.0040
0.0040
0.0040
0.083
0.014
0.0040
0.0020
0.0060
0.012
0.0040
0.012
0.023
0.066
0.012
0.18
0.014
0.14
0.010
0.010
0.010
0.065
0.050
0.045
0.065
Surrogate/Recovery Data For Chlorine
Surrogate
TCmX
DCB
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheme
15.9
U
U
36.2
53.0
56.5
U
35.4
U
182
20.4
U
U
121
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
110
110
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
10/10/94
BY
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
BLW
METHOD/CAS#
SW-846, 8080
319-84-6
58-89-9
319-85-7
76-44-8
319-86-8
309-00-02
1024-57-3
959-98-8
72-55-9
60-57-1
72-20-8
72-54-8
33213-65-9
50-29-3
7421-93-4
1031-07-8
53494-70-5
72-43-5
57-74-9
8001-35-2
12674-11-2
11104-28-2
11141-16-5 ^^
53469-21-9 ^W
12672-29-6 ^
11097-69-1
11096-82-5
Pesticides/PCBs 8080
Recovery Limits
75
75
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
TO 125
TO 125
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
Page ff: 25
November 28, 1994 12:41 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: Q.C. STANDARDS LabID: 9409014-lOA CoUected:
TEST
Volatile Organics
1,1-Dichloroethane
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Te trachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Tri chlorofluoromethane
^l^^vl Acetate
fl^B/l Chloride
c^ylene
RESULT
U
121
U
U
U
U
U
U
42.0
U
75.9
98.1
151
184
50.0
U
50.5
53.2
43.8
D
60.3
, U
u
u
124
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
• ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
"AJbLYZED
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene :-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
Seml-Volatlle Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
U
U
U
U
3100
U
910
U
6100
U
U
U
U
U
U
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
98.9
96.9
101
50
330
330
190
110
63
150
150
63
76
190
130
400
53
46
73
120
METHOD/CAS#
SW-846, 8240
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/:J7/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
• Page ff: 26
November 28, 1994 12:41 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: Q.C. STANDARDS
TEST RESULT
LabID: 9409014-lOA
UNITS DETECTION ANALYZED BY
LIMIT
CoUected:
METHOD/CAS#
Semi-Volatile Organics
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)metheme
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
D ime thyIphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofurem
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4 -Chlorophenyl-phenylether
Fluorene
4 -Ni troani1ine
4,6-Dinitro-2-methyIphenol
n-Nitrosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butyIphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo[a] emthracene
bis(2-Ethylhexyl)phthalate
Chrysene
Di-n-octylphthalate
Benzo[b&k]fluoranthene
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h]anthracene
Benzo[g,h,i]perylene
U
u u D
1030
1300
U
U
U
U
U
3600
8200
U
D
U
U
u U
U
u 8100
U
6400
U
U
4700
U
U
U
U
U
13100
2000
520
500
U
10400
21000
2100
15400
2800
U
U
u u
u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
53
120
79
63
1400
79
99
63
190
63
140
63
120
790
63
63
63
120
180
63
83
73
63
83
260
83
83
83
160
83
120
83
140
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
09/27/94
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
Page ff: 11
November 28, 1994 12:41 CERTIFICATE OF A^fi^LYSIS
RESULTS BY SAMPLE
Sample ID: Q.C. STANDARDS
TEST RESULT
'" LabID: 9409014-lOA
UNITS DETECTION ANJkLYZKD BY
LIMIT
CoUected:
METHOD/CAS#
Semi-Volatile Orgi
Total Cyanide
anlcs
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
Phenol-d5
Nitrobenzene-dS
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
146.6 ug/g
For Semi-Volatile
%Recovery
45.61
51.07
71.05
82.35
75.80
98.11
0.250
SW-846,
Organics 8270S
Recovery Limits
25 TO 121
24 TO 113
23 TO 120
30 TO 115
19 TO 122
18 TO 137
10/04/94 KEN SW-846,
8270
9012
Page ff: 28
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limu.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1.1J with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA " Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ENVIRONMENTAL LAB WORK REQUEST ^(/'P^p/(p
^- XraOKOL ENVIRONMENTAL LABORATORY LWR No. E10639
/i^r \A/d/^cK EXTDtSION
S390
COSTCBnEH
/4OO
WOKK ORDER
/B9^ \9-^Z'^
ORGANIZATION
E/lL/ro ^/^(fl^-2oie
RB>ORT RES1JLTII TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
/>
SAMPLE
1. •S(X'ir)U*t-i-2i^
DATE TYPE
•^-174^ y^
LOCATION
M-t BDranJi// g^
TIME TEST
d.d,Cr,/^,P/}; f>H-
REMARKS
7 // ! I sy /) 11 l/cc<.
.. \
/ •i.SU'fiW^lc;'H^
/Jr^^sc;/cf, 11-y im /'^.Cr,A^.{>b, P//
U n y /I f I MC^
/
y 1
ll ll \a%o {ij,Cr,/)^,/^y,p//
ll /1 y /I /02c Wc
y\ f
fl w /I 1040 cj,C.,A^,Ph, f^H-
II a /I lt'4-o i^o/:<.
fi-T^ii-^U'in-ft
I <-
/< /C'4c 0^,r...A\^ Pb. f>l4
I I I I JCM ilCL^.
CHAIN OF CUSTODY
RELINQUISHED BY DATE
rf/7\7lll//^—^^^^
TIME
/2^7
RECEIVED W
™F
/7./y///^...^.x^''?^>^-f¥
DATE TIME
/>J7
FOR LABORATORY UJrE ONLY
DATE COMPLETED DATE REPORTS)
October 31, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmemal Monitoring
TO: Helen Ward
MIS 301
A.F. WALKER, MIS 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham aty, Ut 84302-0707
Analytical Labs MIS 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Orderly 9409016
LabID: Sample ID
Sample and Test Code Identification
Test Codes and Names
OIA
LabID:
«A
LabID:
^^
"
LabID:
04A
LabID:
^J5A
M2-B DRNFLD.OD 50, 5 FP.
Mi-B DRNFLD.OD 50, 10 FT.
-. -
SMTOlelD:
M2-B DRNFLD.OD 26, 5 Fr.
- . . •
— .....- .
""" . • '
SampleP:
M2-B DRNFLD.OD 26, 10 FT.
_.; "• ^T::. :• •-• • .. -.
. ' ~ ' ' '
• .-••••'-'•'
'". •" "• •• • '.^. •
••-••• ...
M2^DRNFLD.OD26,10 Fr.DUP
.. . .. • -~_':?!:rr " .
—
3050
CD AE2
CR AE2
PB"AE2
ACrAE2
8240S
PH_S
Acid Dilution
Cadmium
Chromium
Lead
Silver
Volatile Organics
pH (SoU)
Test Codes and Names
3050
CD AE2 CR~AE2
PB~AE2
AO AE2
824n.S
PH_S
Acid Digeitioii
Cadmium Chromium
Lead
Silver
Volatile Organics
pH (SoU)
Test Codes and Names
3050
CD AEZ
CR~AE2
PB"AE2
Ad" AEZ
8240s
PH_S
Acid Digestion
Cadmium
Chromium
Lead
SUver
Volatile Oiganics
pH(SoiI)
Test Codes and Names
3050
CD AEZ
CR"AEZ
PB~AEZ
Ad" AEZ
874ns
PH_S
Acid Digestion
Cadmium
Chromium
Lead
SUver
VolatUe Organics
pH(SoU)
Test Codes and Names
3050
CD AEZ
CR~AE2
PB~AE2
Ad" AEZ
8Z40S
PH S
Acid Digestion
Cadmium
Chromium
Lead
SUver
Volatile Organics
pH(Soil)
Method
SW-g46, 3050
SW-g46, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,9045A Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,904SA Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,9045A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,9045A Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,9045A
Page#:lof ^
•
Workorder Cnmmmfs
CerimedBj^
Page ff:l
TTtis is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: M2-B DRNFLD,GD 50, 5 FT. Lab ID: 9409016-OlA CoUected: 09/22/94 08:30:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmluat
Chromluffl
Lead
Silver
Volatile Organics
Acetone
Acrolein
Acrylonitrile.
Benzene
Bromodichlorometheme
Bromoform
Bromomethane
2-Butanone _
Carbon disulfide'
Carbon tetrachloride
Chlorobenzene _
Chloroethane
2-Chloroethylvinyl.ether
Chloroform :...-—-
Chloromethane
Dibromochloromethsaie
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloroprppene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4 -Dichlorobenzene 7:!^ -
Ethylbenzene -; -
Methylene Qiloride ---
4-Methyl-2-Pentanone
Styrene_:._...,,.. :_-—^rr--.
1,1,2,2-Tetrachloroethane
Tetrachloroethene "
Toluene" T ' '^ -
1,1,1 -Trichloroet:hane .
1,1,2-Trichloroethane
Trichloroethene^-^ ^
Trichlorofluoromethane '_
Vinyl"Acetate--£i^7^ ,' :
Vinyl Chloride -•^ ": ". ^_
10/13/94
0.41
21.2
8.93
U
D
U
D
U
D
U
U
D
D
U
U
U
D
U
U
U
U
U
U
D
D
U
D
D
D
D
D
D
D
U
D
U
U
D
6.0 BJ
- U
- U
- U
U
D
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.1
0.4
1.8
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10/13/94
10/26/94
10/26/94
10/26/94
10/26/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
LVD
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
Page#:3
OctoberSl, 1994 14:29 CERTIFICATE OF ANAJLYSIS
i" RESULTS BY SAMPUE
Sainple IDrM2-B DRNFLD.GD 50, 5 FT: . '- Lab ID: 940IW16-01A CoUected: 09/22/94 08:30:00
TEST RESULT UNITS DETECTION A](TJ)IJYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
o-Xylene
pH (Soil)
D ug/Kg 10 10/04/94 JMA
Surrogate/Recovery" Data For Volatile Organics 8240S
SW-846, 8240
95-47-6
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
7.65 pH Unit
%Recovery
103
97.5
98.0
Recovery Limits
81 TO 117
74 TO 121
70 TO 121
09/22/94 AA SW-846,9045A
Sample ID: M2-BDRNFLD.GD50, 10FT LabID: 9409016-02A CoUected: 09/22/94 10:08:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid DlgestioaT;.;.^ " • -_--
l^^alum .....••';•.'•' ::.-^_
Chromium — _ ;_..
Lead-:-...•.•- '"'"'' •••'••••'
Silver " -- -::7'^.'..' '"•"-
Volatile Organics.: iz-:'i
Acetone . .••-•'-:' •/••—:-.
Acrolein . • ,. -
Acrylonitrile _— :•
Benzene- -
Brofnodlchloromethane - - - -iii.
Bromoforin—--_:.L^-;-i-~:
Bromomethane •^'— V"
2-Butanone 1- ~--
Carbon disulfide ~
Carbon tetrachloride — - .
Chlorobenzene:^— - .
Chloroe thane __•: ' • - • •.
2-Chloroethylvinyl ether
Chlorofonnv-:"^'-; "i -._-- _.
Chloromethane •^"- "1" - " - " -
Dibromochloromethane • -i-^-._.:
1,1 ^Dichloroethane -^ : ~ ~:;
1,2-DichloroetJiane .
1,1-Dichloroethene — ~ " :
2-Hexanone --:i^^ •; - - --
•-::.7>^f::.-...
•• —.•• • • -.—'•-•-
-.-. —r.~ -^.,—•—••••--- ~-:r. •••. •
'.. :-'.,'-'' \K''"'i-'/: • •:.'': '^-.•. " •• •
10/13/94
- 0.24
19.3
.: 12.1
• -•-•'-• u. •;
•-^•-i.;;
D
"';--•--U
——^- V "
: D
__ . : U
u - D
- u D
- . - u _ u -^---...:." D.
D
- D
• u ••
.'• _ _ -u 7:
^-;-~:i::,u--
..•."•--:U-_-
- : .-^•^.- u ..::
-^ ::r~" v _. •...
.—
DATK
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
--•
(3.1
0.3
1.6
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10/:L3/94
10/:>6/94
10/:>6/94
10/26/94
10/26/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
LVD
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
3050
6010
6010
6010
6010
8240
Page ff: 4
October 31; 1994 :.; 14:29 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M2-B DRNFLD,GD 50, 10 FT. LabID: 9409016-02A CoUected: 09/22/94 10:08:00
TEST
Volatile Organics
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2-Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene - -- .
1,1,1-Trichloroethane - -
1,1,2-Trichloroethane
TrichloroetheneT-
Trichlorofluoraaiet:liane _
Vinyl Acetate -
Vinyl Chloride
o-Xylene ' .-
RESULT
U
u u u D
U
D
D
D
U
D
D
U
U
8.4 BJ
U
U
U
U
U
- D
• j=_'-^^ - Surrogate/Rece
~ ' r=-_-^ .- Surrogate
—— .:_ -^ Toluene-d8
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JUA
JMA
JMA
JMA
JMA
JMA
JMA
)very Data For Volatile Organics 6240S
. ^ 'l-7::hxcmotluoxatoenzene
.:..7' '\7x"^'~"i.2-
pH (Soil)~~^^^^-^ -
Dichloroethane-d4
~ 7.51 pH Unit
^Recovery
102
99.7
100
METHOD/CAS#
SW-846, 8240
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
•
Recovery Limits
81
74
70
09/22/94
TO 117
TO 121
TO 121
AA SW-846,9045A
Sample ID: M2-B DRNFLD.GD 26, 5 FT. LabID: 9409016-03A CoUected: 09/22/94 10:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
10/13/9.4"-
-4.43
33.9
21.1 .-
^=?^ 39.1
DATB
ug/g
ug/g
ug/g
ug/g
0.1
0.4
1-8
0.2
10/13/94
10/26/94
10/26/94
10/26/94
10/26/94
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
Page #: 5
Octobers!, 1994— 14:29 CERTIFICATE OF A^[i%JLYSIS
- RESULTS BY SAMPLE
Sumple ID: M2-B DRNFLD.GD 26. 5 FT. LabID: 9409016-03A CoUected: 09/22/94 10:20:00
TEST RESULT UNITS DETECTION ANJLLYZED BY
L][MIT
METHOD/CAS#
Volatile Organics
Acetone 2.4 J
Acrolein IJ
Acrylonitrile , D
Benzene D
Bromodichloromethane U
Bromoform D
Bromomethane XJ
2-Butemone U
Carbon disulfide U
Carbon tetrachloride U
Chlorobenzene—. U
Chloroetheme U
2-Chloroethylyinyl ether- U
Chloroform U
Chloromethane " "~. U
Dibromochloromethane - ~ U
1,1-DichloroetJMme ', :. -_ U
1,2-Dichloroethane - - U
1,1-Dichloroethene U
2-Hexanone—.v- - D
trans T.,2-Dichloroethene ~ ^ D
1.2-Dichloropropahe. ' -.—[j-
||^-l,3-DichloroproDene" —-_.: -^—tJ-
I|VJIB-1,3-Dichloropropene „ XJ
T72-Dichlorobenzene===^----- -•.••.• D
l,3-Dichlorobenzene"~^~ D
1,4 -Dichlorobenzenes— -_r—— D
Ethylbenzene r7=r=r7^ri^ • . — U
Methylene Chloride --—— —_-.— u
4-M6thyI-2-Pentemone": • --- D
Styrene-- __-'—^ '• ;_. _. U
1,1,2,2-Tetrachloroethane : D
Tetrachloroethene : U
Toluene - - D
1,1,i-Trichloroethane — 14 B
1,1,2-Trichloroethane •—— U
Trichloroethiane-—- , • • Ur
Trichlorofluorometiiane::.....- •.::,:;, D.
vinyl "Acetate--—r.-- - . : • --—u "
Vinyl Chloride : — - .—: u
o-Xylene—•-'. V= :, — U;
• rm.-:-,:-^v^. . - ~ Surrogate/Rec
•---~B~--—- .J.;;:.-.;,,--••• Surrogate-^'"
^-^=^=i^i-wv' "'^^^^^^lEoiuene-da
—-— ',.:••-i/^r; ^ Bromof luorobenze
". r-cr"r -•:-^ -" lr2-Dichlbroetha
pH (Soil) ^-. - :: 7.52
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
.ug/Kg
overy Data
me
Ae-d4
pH Unit
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 .
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
.10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94 -
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
10 10/04/94 JMA
For Volatile it>rganlcs 8240S
%Recovery Recovery Llm
102
96.4
100
81
74
70
09/22/94
TO 117
TO 121
TO 121
AA
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
its
SW-846,9045A
Page ff: 6
October 31,1994 •^^14;29 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
• • """-".^jTi...J •'. •'.-'••'.'.r^' •"
• "'•""". '—7*. . ,
-""",'
• -^^- .
Sample ID: M2-B DRNFLD.GD 26. 10 FT.
TEST
Add Digestion
CadmluB
Chromium
Lead
Silver
Volatile Organics
Acetone -
Acrolein
Acrylonitrile - . r 77' .
Benzene -. i : --.;____--• ;i
BromodichloroTOthane -
Bromoform— •_>:_./"'.
Bromamethane /! - • -
2-Butanone ;>-_^il . _-
Carbon disulfide;^ .-
Ceurbon tetrachloride :••;—
Chlorobenzene ^ —- - .
Chloroethane' - — : r:_
2-Chloroethylyinyl et^er !
Chloroform.-i^^--^:- ;^—1.7.= ;i^^
Chloromethane^. ^" .-:^- -
Dibrcmochloromet:hane ~~:.. .
1,1-Dichloroethane -
1,2-Dichloroethane^ ^r:=^ • ~
1,1-Dichloroethene—-. -"
2-Hexanone V" - - —
trems-1,2-Dichloroethene -
1,2 -Dichloropropane r" .
cis-1,3-Dichloropropene-
trans-1,3-bichloropropene~
1,2 -Dichlorobenzene - - -•^—
1,3-DichlorobenBeuae —;
1,4 -Dichlorobeiii«e'ne — 1::
Ethylbenzene ---•^^- ..
Methylene ChToridei.';->';.
4-Methyl - 2 TPentemoae-^
Styrene "--•- - —^- - _. ,
1,1,2,2 -Tetrachlcnroethane Ti-
Tetrachloroethene:_:. .
Toluene- ,; : ^ - - :".
1,1,1-Trichloroethane " t
1,1,2-Trichloroethwie - -
Trichloroethene •' - '' -
Trichlorofluoromethane
Vinyl Acetate .•.:^;- ^ .
Vinyl Chloride • - •' ••• - -
o-Xylene -.li.-il;••••->--i-^:-.- ' *;.
-.'. . : ...•.•..•.•^.i^-^._^^;_.
' - * • • -jJ "^ * "-"' ' —
.. . —;—V;_tZ:—...;. .
'.:•"_ /:•..'' .^—~^~-".'''. '•' ••-
,.^ .. •• VV-.0---J.-,:;;-... r:./- .;.
--—• • .-'-r.' -^ .-.....,. ,^..:^-•^C^^^Vv.
RESULT
10/13/94
0.32
22.7
10.8
U
3.4 J
U
D
D
u : u u
u D -
u ..:...: _ :U :
" - u : -— D
=r- --. U
U
U
D
- u U
U
U
. -_ . U
•"•;•_ V- --"U •
:: —r._D
V U
U
- ' - u
7^- • U
-U
":.-.•:•: xj
.•,--:--.-u •
u r .7 XJ
' XJ
~. - : U
' XJ
XJ
XJ
_-. __ u
.-;•.-,-.-... XJ :•
::Z:.:..':'- -XJ. ..
••; ;.• •":——'. . •
_: .~ :r^---:r-. .
• .. .• —• -:
~:-_..—-
' l^J;.---^ " •
#
LabID: 9409016-04A CoUected: 09/22/94 10:40:00
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
'-
DETECTIOM
LIMIT
0.1
0.3
1.4
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Page ff: 7
—
r ANALYZED
10/13/94
10/26/94
10/26/94
10/26/94
10/26/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
-
BY
LVD
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01
10061-02
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
3050
6010
6010
6010
6010
8240
•
•5
-6
•
October 3r;a994v-a4:2SL CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M2rBDRNFLD.GD26, 10FT. LabID: 9409016-04A CoUected: 09/22/94 10:40:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Surrogate/Recovery Data For Volatile Organics 8240S
SW-846, 8240
pH (Soil)
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Di chloroethane-d4
7.36 pH Dnit
%Recovery
103
98.5
101
Recovery Limits
81 TO 117
74 TO 121
70 TO 121
09/:J2/94 AA SW-846,9045A
Sample ID: M2-B DRNFLD,GD26,10 FT.DUP Lab ID: 9409016-05A CoUected: 09/22/94 10:40:00
TEST RESULT UNITS DETECTION ANJIIiYZED BY
:Z_li - LIMIT
METHOD/CAS#
Add Digestion
Cadmium .":1J_"
'omlua - . •'•"
Lead-
Silver.
Volatile _prganic«^_£
Acetone - •• •'" -^f~:=-^^~
Acrolein —-' ^;":-iiv> - v-
Acrylonitrlleli::;;:^^;^^^ ?
Benzene -' : rr^ ^_LZ_
Bromodi chloromet^hane..
Bramoform -•.' - •"'' :.-•'.-
BromcmetAemiBTji^t!^^ —
2 -Butanonei:.r:f^rrr: —^~
Carbon di sulfide
Carbon: tetra^ioride-ii--
Chlorobenzeher-!^:^'.:"^' -^-^-^ -r:^--
Chlproet:hane-'-r^==i^ , '" ~
2 -Chlorbetihylvinyl. ether'
Chloroform:-•"':•/iL,' '•
Chloromethanein ; - L_.".
Dibromochlorooiethane -—-
1,l-Dichloroej:)uu()e .r^ ^,
1,2 - Dichlproiethane; i' £j:£i;
1,1 -DichlbYoethene •;;:• -. ;'LI_
2 -Hexanone'TrT^">4^r^i-7-' '•.•"'':
trans-1, 2rDiciOnbfoethene'
1,2-
10/13/94 '
U
20.9
-:L9.52
•-•: ..;.^-u_.
- ~~-.?''~''.' '•
— 1.5 J.-.-
... ^o--
.:••"•;TJ•^^^•
X3
__-u-
--"."•;. • u ,-•
:T:^--D".
0
-,-. . -•-•-D
.=^:.-CZ^ U
-^•^- D
—-U
u
••...u -..
.:• r-U—••
"••••• •• u-
V _ Xi -
:.,^=^^-.-
.-t-v-.-XT"-'-:
'•'rz:.:i:r^ .-.U^r—
^_^_:^U
-- -r^J
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
: ug/Kg
-ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
-ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.1
0.3
1.6
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10/13/94
10/26/94
10/26/94
10/26/94
10/26/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
LVD
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
Page#:8
OctoberSl, 1994 ::;14:29 CERTIFICATE OF ANALYSIS
7^-" RESULTS BY SAMPLE
Sample ID; NC^PRNFLD.GD26.10FT.DUP LabID: 9409016-05A CoUected: 09/22/94 10:40:00
TEST RESULT
Volatile Organics
cis-1,3-Dichlorppropene D
trems-l,3-Dichloropropene D
1,2-Dichlorobenzene . . U
1,3-Dichlorobenzene • - " tJ"
1,4-Dichlorobenzene XJ
Ethylbenzene U
Methylene Chloride U
4-Methyl-2-Pentanone U
Styrene D
1,1,2,2-Tetrachloroethane n
Tetrachloroethene D
Toluene — U
1,1,1-Trichloroethane 6.8 BJ
1,1,2-Trichloroethane _. U
Trichloroethene U
Trichlorofluoromethane ;--: _: . U-
Vinyl Acetate ^1 - U"
vinyl Chloride U
o-Xylene 'z^- i_" _ . . - U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
^ ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
-, "--"-vl Surrogate/Recovery Data For Volatile Organics 8240S
•-*— ~ Surrogate
Toluene-d8
• _i. ", .—-Bromofluorobenzene
. "•-•• —- 1,2-Dichloroethane-d4
pH (Soil) -— - ; ^'^^^ -7.40 pH Dnit
%Recovery
103
99.0
101
METHOD/CAS#
SW-846, 8240
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits ^H
81
74
70
09/22/94
TO 117
TO 121
TO 121
AA
"^^
SW-846,9045A
Page ff: 9
Data Reporting Qualifieis
U -Compound was analyzed for but not detected. Indicates conipound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. l.U with a detection limit of 5.0)
B — This flag is used when an analyte is found in the blanlc as weU as the sample.
E Estimated value. Result was outside of the caUbration nmge but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT'— Indicates that an analyte was not tested for.
Q":^ :JSiirrogate/spike recovery was outside ofthe specified limits.
•
#
,y •J-.t'.^V
ENVIRONMENTAL LAB WORK REQUEST
rraOKOL ENVIRONMEI>JTAL LABORATORY LWR No. E10641
// ^ ///^(yf^ :f39n '-'4^£>
COSTCEMTBR WORK ORDER
/6f40 2^ ^/i/f4
ORGANIZATION
/^iJ ^6h
MAIL STOP KEPORT RESlULTli TO:
1o/^ HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE
i l^d 7 Sft
DATE
9-Zo^4
TYPE
y^
1X)CAT10N
77-Z Vramd/i/B
TIME
e>^^ ^^ -^^^
TEST
iiuuu
REMARKS
I/' fl )l i/ ll CJ, Cr, 4 , /^i -^/^ /> ^- ?/^S^
c^y /oft II y II "//S i/^> ^ - ^Z. 40
// I I ^ I / 'f CJ/C^j A^,//p, '^^/o ///' f^r~
r / /^ II' ^^ U H 940 ML^ fZ.4-^
,1
/XA 11. /Qfi-
K y /I a±(z. CJ.Cr. A.r^. {>L-/.i?/0 fO//-9^s:
y ll 1004 UOC-3L4D
m ll
CJ74 £'(^
,1 i/ /004 CJ, Cr, .4^, Pj, -^d/o f-//- '?'04<^
y
\
r
ll y
ll L^^
/I /ozo l/Cc- 3240
If /ozo cjX'^i /^f, f^y- c>^/o ^u-9a4y
aA/4. f^a-f\ y /( /PSV i/z>^' ez4o
y^ l/ /o^<r CJ. C^, Af, fJ^ -/^^/o ^//-•f^j'
CHAIN OF CUSTODY
REUNQUISHED BY
'X/d'Hi,
DATE
ZhScff'/zj
TIME
Z//^-
RECEIVED BY
^ZMk^ A
DATE
^_^,2£^£-V
TIME
•' •- ,2-
FOR LABORATORY USE ONLY
DATCCOMPLETa) DATE KEPORTED SIGNATURE
October 31, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER, MIS 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham aty, Ut 84302-0707
Anatytical Labs MIS 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order j}> 9409018 Sample and Test Code Identification
LabID: Sample ID:
OIA M-2 DRNFLD-B,OD 7,5 FT.
Test Codes and Names
LabID:
02A
lelD: M-2 DRNFLD-B,OD 7,10 FT.
LabID:
03A
pie ID:
M-2 DRNFU>-B,OD 16,5 FT.
LabID: I
04A M-2 DRNFLI>-B,OD 16,10 FT.
Pie ID:
LabID:
65A
ale ID:
: M-2 DRNFU>-B,OD 74,5 FT.
LabID:
~5SA
lie ID:
M-2 DRNFIJ[>-B,OD 74,10 FT.
3050
CD AE2
CR AE2
PB AEZ
Ad'AEZ
8240s
PH S
Acid Digestion
Cadinium
Chromium
Lead
Silver
Volatile Oiganics
pH (SoU)
Test Codes and Names
3050
CD AE2 CR AE2
PB AE2
AQ AE2
8240s
PH S
Acid Digestion
Cadmium Chromium
Lead
Silver
Volatile Organics
pH (SoU)
Test Codes and Names
3050
CD AE2
CR AE2
PB AE2
Ad"AE2
8240s
PH S
Acid Digestion
Cadmium
Cliromium
Lead
Silver
Volatile Organics
pH (SoU)
Test Codes and Names
3050
CD AEZ
CR~AE2
PB AE2
ACrAE2
8240s
PH S
Acid Digestion
Cadmium
Chromium
Lead
Silver
VolatUe Oiganics
pH(SoU)
Test Codes and Names
3050
CD AE2
CR"AE2
PB AE2
AO AE2
8240s
PH S
Acid Digestion
Cadmium
Chromium
Lead
SUver
VolatUe Organics
pH(SoU)
Test Codes and Names
3050
CD AEZ
CR AE2
PB AE2
ACrAE2
8240s PH S
Acid Digestion
Cadmium
Chromium
Lead
SUver
VoUtUe Oiganics
pH(SoU)
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,9045A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,9045A Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,904SA
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,9045A Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,9045A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,9045A
Page#:lof /(J
•
Workorder Comments
#
Certifi^^
• Page #:2
This is to certify that the following samples were analyzed using good laboratory practices
to show tlie following results.
Sample ID: M-2 DRNFLD-B,GD 7,5 FT. LabID: 9409018-OlA CoUected: 09/26/94 08:55:00
TEST
Acid Digestion
Cadmitun
Chromi vm
Lead
Silver
Volatile Organics
Acetone
Acrolein
Acrylonitrile'
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene- "
Chloroetheme - -
2-Chloroethylvinyl ether
Chloroform
Chloromethane'" ^ T
Dibromochlorcmethane
1,1-Dichloroethane
1,2 -Dichloroet::hane
1,1-Dichloroethene
2-Hexanone ''—'--
trans -1,2 -Dichloroe t:hene
1,2-Dichloropropane
cis-1,3-Dichlorpprppene
trans-1,3-Dichlorpprppene
1,2-Dichlorobenzene ..
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene-^r-
Methylene Chloride
4-Methyl-2-Pentanone .
Styrene.
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene - '^" ---- — '
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene - —•~ .;_
Trichlorofluorbmethahe
Vinyl Acetate •
Vinyl Chloride 2^^
• --.- Z " ~—^-~>'- :—^ .-••-—•- "• •-•-—.
'•" •; ^.-jr.:—^ ' •' •-
RESULT
10/13/94
1.84
20.5
6.60
9.07
D
U
U
U
U
U
U
U
n
u
u
u
u
D
U
U
D
U
U
D
U
D
D
D
U
U
D
U
D
U
u
D
U
U
5.2 BJ
U
D
. _ U
u
u
_. ;
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.4
1.8
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Page ff: 3
ANALYZED
10/13/94
10/26/94
10/26/94
10/26/94
10/26/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
BY
LVD
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA.
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7 ^^
75-00-3 ^V
110-75-8 ^^
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
•
October 31,1994- 14:46 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLIE
Sainple ID: M-2 DRNFLD-T8,GD 7,5 FT. LabID: 9409018-OlA CoUected: 09/26/94 08:55:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
o-Xylene
pH (Soil)
U ug/Kg
Surrogate/Recovery Data
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
7.77 pH Dnit
SW-846, 8240
10 10/04/94 JMA 95-47-6
For Volatile Organics 8240S
%Recovery Recovery Limits
102 81 TO 117
97.2 74 TO 121
101 70 TO 121
09/:26/94 AA SW-846,9045A
Sample ID: M-2 DRNFLD-B,GD 7,10 FT. LabID: 94a)018-02A CoUected: 09/26/94 09:15:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Dlgestlba,.?p
I lium
Chromium
Lead
Silver
Volatile Organics
Acetone ---—.:_- -
Acrolein
Acrylonitrile
Benzene '.:-..-'--..:•••.
Bromodichlor6met:hJBne
Bromoform .._ ' —
Bromometheuie'7-~—.=1:-'— "
2-Butanone -=?^,.
Carbon disulf ide:::- -^— -^
Carbon tetrac*iloride ~~
Chlorobenzene--_
Chloroetheme"—'-'-
2-Chloroethylvinyl ether
Chloroform j_^ • ~ . -_ -
Chloromet:hane-7-"^li^—VJ: -
Dibromochloramet:)iane --^ ~
1,1 -Dichloroethane .:""..
1,2-Dichloroethane. . ..
1.1-Dichloroethene." -
2 -Hexanone — 1. "v - -" L
10/13/94
0.80
20.0
7.34
~: D
D
u . — :— U
.---.•;•- D
'•- • -. .-.vU-v.
"- D
U
u
D
U
. D
u U
•.. • :-.n-.
- -D :
s :xj
;.......• ;v--. --.D .
..-."r:^^^- - •-- U
D
_ ; U .
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
•
0.1
0.3
1.7
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10/13/94
10/26/94
10/26/94
10/26/94
10/26/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
LVD
LYD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
3050
6010
6010
6010
6010
8240
Page ff: 4
October 31, 1994 14:46 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-2 DRNFLD-B,GD 7,10 FT. LabID: 9409018-02A CoUected: 09/26/94 09:15:00
TEST
Volatile Organics
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-l,3-Dichloropropene
trans-1,3 ^Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene - —
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene —
Tri chlorofluoroinethane
Vinyl Acetate-
Vinyl Chloride -
o-Xylene :_:-
RESULT
u D
D
U
U
U
U
U
U
D
O
U
U
O
6.4 BJ
O "
u V
u
u u
Surrogate/Rec
.-y'-- Surrogate;.^
- -.: - Toluene-d8
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JISA
JMA
JMA
JMA
overy Data For Volatile Organics 8240S
- — T.~ -. - .Bromofluorobenzene
: . _:. .:..,.^—-/v .1/2-
pH (Soil) :._—_
Dichloroethane-d4
7,65 pH Unit
%Recovary
104
98.5
102
Recovery Llm
81
74
70
09/26/94
TO 117
TO 121
TO 121
AA
METHOD/CAS#
SW-846, 8240
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
•
its
SW-846,9045A
Sample ID: M^DRNFLD-B,GD 16,5 FT. Lab ID: 9409018-03A Collected: 09/26/94 09:40:00
TEST. RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
10/13/94
2.75
40.1
" ri5".3
-~9.40
DATE
ug/g
ug/g
ug/g
ug/g
0.1
0.4
1.8
0.2
10/13/94
10/26/94
10/26/94
10/26/94
10/26/94
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
Page ff: 5
October 31, 1994^^-14:46 CERTIFICATE OF ANALYSIS
' RESULTS BY SAMPLE 9 --CS:..-:.-:.,^;
Sample ID: M-2 DRNFLD-B,GD 16,5 FT.
TEST RESULT
Volatile Organics
Acetone 1.5 J
Acrolein D
Acrylonitrile D
Benzene U
BromodichloromethcUie U
Bromoform D
Bromomethane U
2-Butanone U
Carbon disulfide U
Carbon tetrachloride U
Chlorobenzene U
Chloroethane D
2-Chloroethylvinyl ether . D
Chlorofonn--: :-v^ U
Chloromethane"-"- "r-- U
Dibromochlorcmethane -~ - . _ U
1,1-Dichloroetheme:-:.-- D
1,2-Dichloroethane - D
1,1-Dichloroethene D
2-Hexanone - - — D
trans-1,2-Dichloroethene .D
1,2-Dichlorpprppeme —-•..-. u
j^-1,3-Dichlorpprppene . U
•BIB-1,3-Dichlorppropene . D
i^-Dichloroben«ene^ ^ . U
1,3-Dichlorobenzene""-'-- ~-. tJ
1,4-Dichlorobenzene -•"—- D
Ethylbenzene -' -v u ^ i,-'": ; - D
Methylene Chloride ' U
4-Methyl-2-Pentanone - : U
Styrene. -—; • :i:. .^ " D
l,l,2,2-Tetrachloroet:hane U
Tetrachloroethene/--- U
Toluene ^^^^-—^^^---- _ - U
1,1,1-Trichloroethane -: 6.6 BJ
i,l,2-Trichloroet:heme-. U
Trichloroethene - " ,, U
Trichlorofluoromethane . XJ
Vinyl Acetate-— ~ \ _:;;D..
Vinyl Chloride , -" U.
o-Xylene. .:—.-- —-- — u
• •~:^^:7^^7^r''77~'Surrogate/Rec
..-••• " •'•.— .. •-.-.: .. . . •
Surrogate --
" "„.::^'l~^^l.::;;r-:ToIuene-d8 ::: ;
. . -
Lab ED: 9409018-03 A .CoUected: 09/26/94 09:40:00
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 -
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
10/04/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
overy Data For Volatile Organics 8240S
%Recovery Recovery Llm
-: •--'^^~- .^ Bromofluorobenzene
-r^-^-^^^^'^ ;lv2-Dichloroetha
pH (Soil)-- ' : -vi,~- -.-_.- 7.73
• -•-- -— *-.f *..-:— ^ ^ • '• ~—..... _ •..---
m^-7:Wm-^-ff-
"7 •- •- '-•~:7^J.:^i~r' '.\. •• '•''-'
••-"••"\J--: -^i^rf-^"'-•"•'••'/• •"---" •••••-.
._._ ..._-..,, .,^^^;^_^..^.._,^_^ _.^^ . ..^
ne-d4
pH Unit
101
97.8
102
Page ff: 6
81
74
70
09/26/94
TO 117
TO 121
TO 121
AA
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
its
SW-846,9045A
October31, 1994 ;^14;46 CERTIFICATE OF ANALYSIS
- RESULTS BY SAMPLE
...; • - „: • „ , • . • ._.
• .. . • -^ :^- ••.^^•.; '-'ri.'
-• . . •
• ~""
Sample ID: M-2 PRNFLD-B,GD 16,10 FT.
TEST
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
Acetone
Acrolein
Acrylonitrile • —z-.r
Benzene
Bromodichloroinethane
Bromoform '
Bromomethane ~
2-Butanone ..
Carbon disulfideT :r
Carbon tetrachloride"' .
^*l«l 'l^«.^W^^IW^W.««
vxixorooenseue Chloroethane —---:--._
2 -Chloroethylvinyl ether
Chlorofonn ..v ; "• . ; ,7
Chloromethane =":. - --_
Dibroanochloromiathane
l,l-Dichloroet:hane_:
1,2-DichloroetJieme
1,1 -Dichloroethenerr-
2-Hexanone V: ;-
trans -1,2 -Dichloroe tihene
1,2-Dichlorpprppene
cis-1,3-Dichlprpprppene -
trans-1,3-Dichlorpprppene
1,2-Dichlorobenzene • -
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene -T' -
Methylene Chloride ....
4 -Methyl - 2 - Pentanone - - -
Styrene • • • -'••-';.":-^•—:-^::
1,1,2,2 -TetrachloroetJiane
Tetrachloroethene
Toluene ^ __^ _..^.-,-_. ~
1,1,1-Trichloroethane- :
1,1,2-Trichloroethane ~"
Trichloroethene
Trichlorof luoroaiBthahe —:[.
Vinyl Acetate^-r" . ;. 3/
Vinyl Chloride;: . .•.'^~.-
o-Xylenej:^;; •:; _^^•^••';• - . ..^^; •
— •'—-—----- -•. '.
••" ••*.••.-' . !•••
^.'i' -•-. •••••••:• -.::• ...
. . .. • .-• •'"- -.—. "--.i-rr^-T--^-- .• .-
• - • -^-^-T—-^.i^T- •"• —— ..
RESULT
10/13/94
0.80
24.8
10.7
U
5.8 J
U
D
U
. D
U
U
D
U
..•-.•••••. u •
- u - - XJ
u
- - - •• u
- 'XJ
r —U
D
U
u
U
u
u
D
U
U
D
_ _ U
U
D
— V u
D
..__ u -D
_.: 7 u
--^.8 BJ
•-••—:_.-u
__-_. n :./• XJ
_,_.._: Q
u
u
"•' -• .- . •• —-
:_. ....SZJJ7. -
_...'.",' ".
. ..:__' —-'" '
^^V
^^^
LabID: 9409018-04A CoUected: 09/26/94 10:04:00
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.4
1.8
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Page ff: 7
ANALYZED
10/13/94
10/26/94
10/26/94
10/26/94
10/26/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
BY
LVD
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
•-•
METHOD/CA.S#
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3 ^^
110-75-8 ^^
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
•
:: 'rtr^.'
October 3M994^ 14:46 - - -CERTIFICATE OF ANALYSIS
_ -^~- _ RESULTS BY SAMPLE mr7:--mm^^-T'':'-./ i •
Sample ID: M-2DRNFLD-B,GD 16,10FT. LabID: 9409018-04A CoUected: 09/26/94 10:04:00
TEST RESULT UNITS DETECTION A:(TJ)LYZED BY
LIMIT
METH0D/CAS#
Volatile Organics SW-846, 8240
Surrogate/Recovery Data For Volatile Organics 824OS
pH (Soil)
Surrogate
Toluene-d8
Bromofluorobenzene
1,2 -Dichloroeth£uie-d4
7.55 pH Unit
%Recovery
104
98.9
101
Recovery Limits
81 TO 117
74 TO 121
70 TO 121
09/;26/94 AA SW-846,9045A
Sample ID: M-2 DRNFLD-B,GD 74,5 FT. Lab ID: 940<)018-05A CoUected: 09/26/94 10:20:00
TEST' '•••:.::L. •• -•-:-••• •
• -;tf£- •'•.• :•• •• "
Add Digestion -vlv;--
Cadmluffl T" •,"-'" r" -
fl^Bomlum '..'-.'— ...-:
Lead . •.- •-""---. ' "••'"•
J Silver^"~-=^--.'/:-^- 7- '—••
Volatile Organics
Acetone _.
Acrolein
Acrylonitrile .-i- '
Benzene -- .-_-^^^^
Bronodichloromethane ~
Bromoform jtzzi---..-,.- -zrr- - T-
Bromonetheme - -
2-Butemone - - .v.:-. .-:
Carbon disulf ide'^::^- - -
Carbon tetrachloride ^ >-—--
Chlorobenzene ..~-.^-. T'
Chloroet:heme~-".~ -, - Is • : :
2-Chloroethy 1 vinyl etJier ::.-
Chloroform ; —-'T^'".-. ."V. —
Chlorometawmer:-—---• ^-•-
Dibromochloraa»etheme~7 -—
1,1-DichloroetJiane -—. r-
1,2-Dichloroethane
1,1-Dichloroethene r-r^—-; .
2-Hexanone - —~;
trans-1,2-Dichloroethene
1,2 -Dichloropropeme - • — '—-..
... • •• .- •" .• - •' .._ •
..."- • _-r:..-V^"----;-^".'r_
. --••,•, • . p-- -J.^^jr^c^ —- -^
.. .- ' ~ ———^— '^." - . ...* . . .. r" . ••—
RESULT -
—;-:-; •-
10/13/94
7:^ X.01
23.4
- -"^ivl -
••^-'7E7^i72i"
7.7 J
u
u
U
-.-u^-
- -- : D
- D
D
^^_.. ._^
: -r-r- U
• _ __-.; .1:^X1^-=
.=.-1-::::rV:-
-: -- U
D
-l~-X3
XJ
XJ
XJ
. XJ
. D
-..~:: :.^-'.'-o
_ ._:_• U
-.::-:; .. •-- .-•:;:.•
•^_ '•
^' -...:.• -..."'7
•7. . • :': '~^-'---
—'^p^7-;.- —-"t^^i
XJNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
: ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
•• -'
DETECTION
LIMIT
0.1
0.3
1.7
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Page ff: 8
^
AltTALYZED
10/13/94
10/26/94
10/:26/94
10/:J6/94
10/:J6/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
-..._-.
BY
LVD
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
October 3i; I99fbi34i46:r: CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-2 DRNFLD-B,GD 74,5 FT. Lab ID: 9409018-05A CoUected: 09/26/94 10:20:00
TEST RESULT
Volatile Organics
cis-1,3-Dichloropropene U
trems-l, 3-Dichlorppropene TT
1,2-Dichlorobenzene n
1,3-Dichlorobenzene -- D
1,4-Dichlorobenzene XJ
Ethylbenzene U
Methylene Chloride XJ
4 - Me thyl - 2 - Pentanone XJ
Styrene U
1,1,2,2-Tetrachloroetheme U
Tetrachloroethene n
Toluene U
1,1,1-Trichloroethane 6.2 BJ
1,1,2-Trichloroethane U
Trichloroethene -• U
Trichlorofluoromethane- D ;
Vinyl Acetate :~~_r:-^: U
vinyl Chloride':-"^ : U.
o-Xylene D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
ug/Kg 10 10/05/94 JMA
,^nrAT-\r Hat-fl Vr\ir Vt^lmhAtm /Vv/raTi^na A9^nfi
— '-^—. '•'.' - Surrogate . -
— ... -.^^Toluene-d8
-..-• '•--:--• Bromof luorobenze
.V; .,- -- ^ a, 2 -Dichloroetha
pH (SOIDL- _-^ :^— - - 7.56 -
ne
ne-d4
pH Unit
%Recovary
102
97.8
101
MBTHOD/CAS#
SW-846, 8240
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits ^H
81
74
70
09/26/94
TO 117
TO 121
TO 121
AA
"^^
SW-846,9045A
Sample ID: M-2DRNFLD-B,GD 74,10FT. LabID: 9409018-06A CoUected: 09/26/94 10:35:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Silver
Volatile.Organics
Acetone • 1——i.^
Acrolein -- . -- . -.^ -jlrtBtr;,
.10/13/94
-^-- 0.78
^7'^:-"- ... "23.6
7.44
"'•-.7~'~'-- -. U.:!
-_.-.:y7:\ ..... xj_
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
0.1
0.3
1.7
0.2
10
10
10/13/94
10/26/94
10/26/94
10/26/94
10/26/94
10/05/94
10/05/94
LVD
LVD
LVD
LVD
LVD
JMA
JMA
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
3050
6010
6010
6010
6010
8240
Page#:9
October 31,-1994f 14:46 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-^pRNFLD-B,GD 74,10FTT- LabID: 9409018-06A CoUected: 09/26/94 10:35:00
TEST RESX7LT UNITS DETECTION ANJlLYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Acrylonitrile D
Benzene U
Bromodichloromethane D
Bromofonn " U'
Bromomethane tJ
2-Butemone U
Carbon disulfide U
Carbon tetrachloride U
Chlorobenzene U
Chloroetheme D
2-chloroethylvinyl ether D
Chlorofonn U
Chloromethane i;.-!.,-,.- U
Dibromochloromethane. : - .U
1,1-Dichloroetheme ~—;' ' " - D
1,2-Dichloroethane ==;.:-. —-.-^ „:
1,1-Dichloroethene - - - "" u
2-Hexemone . .-r.l . D
trans-1,2-DichloroetJiene- U
1,2-Dichloropropane' :.- '.. XJ ,
cis-l,3-Dichlorpprppenei _ --• v—--_.D
trans-1,3-Dichlprpprppene . U
Jfc-Dichlorobenzene— _r-i— U
••-Dichlorobenzene __-•_, U
^4-Dichlorobenzene;.- U
Ethylbenzene U
Methylene Chloride - 1.4 J
4-Methyl-2-Pentemone U
Styrene :; • . ^~_ U .
1,1,2,2-Tetrachloroetheme . -- u
Tetrachloroethene---^—: .: U
Toluene -•-•~''':it.::^.r:~.. -:... "•• ^'.'•
1,1,1-Tritihloroethane :-_ 12B
1,1,2-Trichloroethane - ": _ . U
Trichloroethene-. •-^-—-^-.-..-. .-—- --r u
Trichlorofluoromethane D
Vinyl Acetate.. :—-.r-^.-. ••- —., xJ Vinyl Chlpride--, • :.U..
o-Xylene _^..^ - —U
" . •-.-..v:.\;:.t;:,;.^; ; ..• —rr..-_
•-;.:, -s^^' rrr^—- ': Surrogate/Reci
;•- — Surrogate
•-- ="'":. Toluene-d8
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
.__ ug/Kg
- ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
-ug/Kg
ug/Kg ug/Kg
ug/Kg
overy Data
—:-- •- '^T--r^; Bromof luorobenzene
--—- ;_ :,-'.-- ,;:u_r7-i-,2-Dichloroetha
pH (Soll)^..-:^—.--^^^-^^^ ;:-.;:• . ;._ ;^.-67 -. .
ne-d4
pH Dnit
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10 _
10
10
10
10
10
10
10
10
10
10
10
10
10
10 10
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94 10/05/94
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA JMA
10 _ lU/Ub/S4 UMA
For Volatile Organics 8240S
%Recovery Recovery Llm;
102
98.5
98.1
81
74
70
09/26/94
TO 117
TO 121
TO 121
AA
SW-846, 8240
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4 75-01-4
95-47-6
its
SW-846,9045A
Page ff: 10
-^r^ - - Data Reporting Qualifiers
:U T^T^jCpmpound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. l.U with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT :J_. Indicates that an analyte was not tested for.
.Q j- .Surrogate/spike recovery was outside of the specified limits.
- .
"^.
...-.•
-
•
_-!.
'.T:
^
..-...—.::• "-J,.: -
-••••' -:ir^~ •' •..' -
-- • • • >
• - •. • . • • . r '
• - •. • ••"";.. •*•' •'.•
.: ,^;^--- -.-—--—
•'-*-"'.•.^—..-.'—-' " •
-• • .J '• • •• r; -
• -.Z-^r-J; •_-• •••..'-;
'-'•- f- "'••• ^~
. 1.. -'• -•. , . -• v-7: .-..
''-.:':'-r-:i:-^\.-:.'. .v, -•-
-..^;-_3:=:=^-r^— .
.-i. . . . . . —
1 -••' 1-—^ .'.!_ •-
••-'-. ••- -.^^ ..-• •::.—
—..-.=-^.-.-
—""• - •-
--^ : . —
—
::z
• '
— .
—:
_-•..
_ •--
7,
ENVIRONMENTAL LAB WORK REQUEST
w •f^^-J
TraOKOL ENVIRONMENTAL LABORATORY LWR No. El0643
/^.r lA/d/lUr
EXTENSION
S3^o
COSTCENTES
[/40C'
WORK ORDER
/B/40
DATE
27 ^pA/i}
ORGAraZATION
i^/iL'/r/ CHQr 3oie
RBMRT RESULT! TO:
HELEN WARD, MS 301
7 SAMPLE INFORMATION
^y
SAMPLE
I. M-19^
^l{'l.<l/l
'• /4-se^
•"-SU'AtO I,r4 9
<u'/Mi.'/.-4'i'
i.
6.
7.
8.
9.
10.
II.
12.
DATE
iT^pt
r 1
ft
ll -.
TYPE
G
^
^
1/
C
IJOCATION
/A-ltfi S/rorJ^ou^
1 1
yCf-S-e^ -^..^c/Su
. //
TIME
/Z4S^
/ /
/^zo
IITI-
//
TEST
y/'C - Bz^D
f7cl,C,;7b,/^^^ -UIC'-, ^^-74
y^'^ - €2io
Z"^, dr, ply, /l^ - C-^/f^'; i/^-Z'f- 70
REMARKS
V; 7/X()<,7'f/)-.^
; //4i/ ^fUr/ra
CHAIN OF CUSTODY
RELINQUISHED BY
<=^L^//a7L .
DATE
t^^t^/LJ.
TIME
9Z7
RECEIVED BY DATE
<i/^9'l4Y
TIME
?:^7
FOR LABORATORY USE ONLY
DATE COMPLETES
#
DATE SEPORTGS
October 31, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham aty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order # 9409023 Sample and Test Code Identification
LabID:
OIA
LabID:
02A
Sample ID:
M-19A STRAND BURNER
Sample ID:
M-585 STRAND BURNER
Test Codes and Names
HMX
NG
3050
CD AE2
CR AEZ
PB AE2
AG AE2
HG CV2
8240S
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NG
3050
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8240S
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Workorder CommGnts
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Certified^"^^
Page#:lof ^
This is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: M-19A STRAND BURNER Lab ID: 9409023-OlA CoUected: 09/27/94 12:45:00
TEST
HMX
Nitroglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury-
Volatile Organics
Acetone
Acrolein
Acrylonitrile
P^Tzehe
^iBjiodi chloromethane
^ll^Pioform
B romome thane
2-Butcinone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
D ibromochl orome thauie
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl- 2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
RESULT
U
u
10/13/94
0.60
2250
162
U
U
610
3.2 J
U
4.8 J
U
U
U
29
240
U
U
7.5 J
U
3.5 J
2400
U
U
U
U
1.3 J
49
U
U
U
U
U
U
1.4 J
31
13
U
U
U
5.5 J
UNITS
ug/g
ug/g
DATE
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
.01
.02
0.1
0.3
1.4
0.2
0.013
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
09/29/94
09/29/94
10/13/94
10/26/94
10/26/94
10/26/94
10/26/94
10/06/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05,'94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
BY
CFP
CFP
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
• Page ff: 2
October 31, 1994 15:20 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-19A STRAND BURNER LabID: 9409023-OlA CoUected: 09/27/94 12:45:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Tri chloroe thene
Trichlorof luorome theuie
Vinyl Acetate
Vinyl Chloride
o-Xylene
4.1 BJ
U
2.0 J
i U
u
2.9 J
1.8 J
Surrogate/Re
Surrogate
Toluene -d8
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
covery Data
Bromofluorobenzene
1,2-Dichloroethane-d4
10
10
10
10
10
10
10
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240S
%Recovery
101
92.0
102
SW-846,
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
8240
Sample ID: M-585 STRAND BURNER Lab ID: 9409023-02A CoUected: 09/27/94 13:20:00
TEST
HMX
Ni troglycerine
Acid Digestion
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
RESULT
18.7
U
10/13/94
0.64
798
20.0
U
0.08
8.5 J
U
U
U
U
U
U
U
U
UNITS
ug/g
ug/g
DATE
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
.01
.02
0.1
0.3
1.7
0.2
0.024
10
10
10
10
10
10
10
10
10
ANALYZED
09/29/94
09/29/94
10/13/94
10/26/94
10/26/94
10/26/94
10/26/94
10/06/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
BY
CFP
CFP
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS# _ m
SOP 420
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
3050
6010
6010
6010
6010
7471
8240
Page ff: 3
October 31, 1994 15:20 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-585 STRAND BURNER Lab ID: 9409023-02A CoUected: 09/27/94 13:20:00
TEST
Volatile Organics ,
.Carbon tetrachloride
. Chlorobenzene
Chloroetheme
2 -Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trems-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
jflk, 2,2-Tetrachloroethane
flHrachloroe thene
Tmuene
1,1,1-Trichloroethane
,1,1,2 -Trichloroetheme
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
3.0
Surrogate
Surrogate
Toluene-d8
U
U
U
U
U
U
U
U
U
U
U
u u
u u ,
u u u
u
u u
u
u u
u BJ
u
u u
u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
A]!?ALYZED
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
10/05/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
i/Recovery Data For Volatile Organics 8240S
Bromofluorobenzene
1,2-Dichloroethane-d4
%Recovery
94.5
91.9
99.0
METHOD/CAS#
SW-846, 8240
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
Page ff: 4
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limu.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1. IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the calibration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ENVIRONMENTAL LAB WORK REQUEST /; , _
r
"^ TFnOKOL ENVIRONMENTAL LABORATORY
FROMl .
.'^.^ k/d/lUr
IHUiAMIZATIOM
f^/lL/r/: cnqr
scnnsioN
.-7-^90
MUL STOP
OOfT COTTER
V40C'
LWR No. £10643
woRKORoea
/f.'/40
DATB
27'^/^9a
»B»0«r«S»ULT»TI>i /
HELEN WARD. MS 301
{/ SAMPLE INFORMATION
S/VMPLE OATE TYPE LOCAnON TIME TEST XEMAKXS
L/
\. M-l</rt
tl'^or /7-l^/l ^/rt>f)J'^nM, WC - S24D
^M-194 ll C4,C,%/>b,.^^ -6^/^; '^^-/V V ; 7/xiil,7'i/r<)
\.y ^' //' '<i'-SST 'S/rW^ (^i?d. - 5^1^^
,f CJ- Cr. f>h, At - C^/O ; ^f - 7470 //ALiC , T/rn-a
/
~7H^ ll i Pll ^^^
/If^ f. lildU/^-
12.
CHAIN OF CUSTODY
KF3JNQUISHED BY
c^^Z^^
DATE
t'&^t4cL
7 T
TIME
^Z7
RECEIVEDBV
XT/MO^^
••
DATE
?Af/ff
TIME
fr37
FOR LABORATORY USE ONLY
MISCDMnSnD •UISRSPOKIED .1ICNATVBK
November 18, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT
TO:
Environmental Monitoring
Helen Ward
MIS 301
A.F. WALKER, MIS 301E
Ext 5390
ANALYZED
BY:
TTiiokol Corporation
Science tk Engineering
P.O. Box 707
Brigham aty. Ut 84302-0707 Analytical Labs MIS 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order )tf 9411Q24
LabID:
OIA
Sample ID:
M-19A STRAND BURNER
Sample and Test Code Identification
Test Codes and Names
1311 TCLP MeUls/SemiVols Extr.
CR_AE2 Chromium
PB AE2 Lead
Method
SW-846, 1311
SW-846, 6010
SW-846, 6010
Workorder CnmmBnta
Report: TfflS SAMPLE IS A RERUN THAT WAS ORIGINALLY SUBMITTED
ON WORK ORDER 9409023 AS FRACTION OIA.
Page ff.lof ;^
#
This is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: M-19A STRAND BURNER LabID: 9411024-OlA Collected: 09/27/94 12:45:00
TEST RESULT UNITS DETECTION AN.BJ:,YZED BY METHOD/CAS#
LIMIT
TCLP Metals/SemiVols Extr. 11/09/94 DATE 11/09/94 LVD SW-846, 1311
Chromium 49600 ug/L 5 11/16/94 LVD SW-846, 6010
Lead 4540 ug/L 25 11/16/94 LVD SW-846, 6010
#
Page ff: 2
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limu.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1.IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as well as the sample.
E Estimated value. Result was outside of the calibration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not applicable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ENVIRONMENTAL LAB WORK REQUEST ^////^/P ^
|P*= TraOKOL ENVIRONMENTAL LABORATORY
FBOM:
A f ii/ALKez,
ORGA^a ZATION
EXTENSION
MAIL STOP
3oie
LWR No. E10670
cosTCsrnm, WORKORDER DATE
REPORT RESULTS TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE
1. -SUC/AU 4t:<
DATE
'M'C'Ci
TYPE LOCATION
/.auiiiliJ..
M-2 hvAhM/ '^-
TIME TEST
C^,Cr;^ii^^'I ^^
REMARKS
2- ijL'.'t:^ \J
7>ei :\C
ic 7
SB /' /37c' Vc^ c
(S^ •?(? fC fr 132 .'i<-' dJ,c^,/k, fh, PH
c-J u- icf, 17 ru> Ibc
i.-3u:iuv •ii..<7
L' IML ddJjjMuIk^M.
*• SijJ/ViV 4iiY i^ 1211 hoc
' :5ix.>/icu ^^
^d ^4 li (r IM. AskCaAun^M.
// IML i/oC
/
9. 5u-','./c' .4c.\' i^ WD_ Cci, C7, A-- . Pb^. p/l
(Ad 21 ^f-t y
JML I'O c.
y' l4io CJ,6t.^^^j^ A^,/)//
f-TKi 22 /oft I Ho U, Cr, /) c,, /V^, fs H
CHAIN OF CUSTODY
RELINQUISHED BY
-fjLXf^/a/Ji^
DATE
/lOlAj?^
TIME RECEIVED BY
^f^•^-' M 'iCd^ijj. '.di.1 LL yf'
DATE
///- f^
TIME
/^y>>
FX)R LABORATORY USE ONLY
DATS OOMPLEnD
%r
DATE REPORTS) SIGNATURE
ENVIRONME
^ XmOKOLENVIRONMKNTAL LABORATOI
noMi
A r ifi'ALjccfi
OBOANIZATION
emiBc r/i''7>/t
WTAL LAB WORK REQUEST ^/J^ // ^^ ^
BCIBaOH
MAn.mp
i^</oo 1^940 3/ c^r<7<7 II
HELEN WARD, MS 301 |
SAMPLE INFORMATION
A
/i)o
SAMPLE
1- Su'Ak.' 4^!^
(^^ /^/ ,r/'^
^V/ /v ^"f/-
GA l^i /oft
1- Si<.'/.tf 4t.r
Cd t^ /oPf
6V/y /^/r
•• Su'^tC' 4c'\
Cid ^ ff
DATE
1\C:
TYPE LOCATION
>^-2 ^g::::^/;.^ /f7-0
/43Z
/41Z
iiSl
/^r/
JML
IS-df
I So J
TEST
l/oc
CJ, C^. A}^ .. h>h, P^
Vi'C
Crl,C,,Ay Ph pH
[loc
1^0 C
C^'.C'y.Ac.f'h^pH
i/OC
REMARKS
7-
9. SK.)/»vf -^ur
^±1 /cfr
isn Cci.Cr.A^,f>hpH
ISU V6C
CHAIN OF CUSTODY
BEUNQUISHESBY
-QLAf/7t)gA^
DATE
(Uoug4
TIME
D^^t-
4
BBCUVUDBY
•''/77//A,.,.^
DATE
//'/ - ^J^
TIME
C^>^
FDR LABORATORY USE ONLY
SATtOOMFiniD DARBBFOVnD aCNATUBS
November 18, 1994 CERTIFICATE OF ANAI.YSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward
MIS 301
A.F. WALKER, MIS 301E
Ext 5390
ANALYZED
BY:
Tluokol Corporation
Science & Engineering
P.O. Box 707
Brigham aty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order # 9411008 Sample and Test Code Identification
LabID:
OIA
LabID:
02A
tab ID:
i03A "
w
LabID:
04A
LabID:
OSA
LabID:
06A
Sample ID:
M-2 GRID 30,
Sample ID:
M-2 GRID 30,
Sample ID:
M-2 GRID 54,
Sample ID:
M-2 GRID 54,
Sample ID:
M-2 GRID 22,
Sample ID:
M-2 GRID 22,
;5FT.
:ioFr.
_.
5 FT.
10 FT.
SFT.
5 FT. DUP.
Test Codes and Names
3050
CD AE2
CR AE2
PB AE2
AG AE2
8240S
PH_S
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
pH (Soil)
Test Codes and Names
30S0
CD AE2
CR AE2
PB AE2
AG AE2
8245s
PH_S
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
pH (Soil)
Test Codes and Names
30S0
CD AE2
CR AE2
PB AE2
AG AE2
82405
PH_S
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
pH (Soil)
Test Codes and Names
30S0
CD AE2
CR AE2
PB AE2
AG" AEZ
8240S
PH_S
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
pH (Soil)
Test Codes and Names
3050
CD AE2
CR AE2
PB AE2
AG AE2
824SS
PH_S
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
pH (Soil)
Test Codes and Names
3050
CD AE2
CR AE2
PB AE2
AG AE2
PH S
Acid Digestion
Cadmium
Chromium
Lead
Silver
pH (Soil)
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,904SA
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,904SA
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,9045A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,9045A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,904SA
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,9045A
• Page #: lof /7
Work Order # 9411008
LabID: Sample ID:
07A M-2 GRID 22, 10 FT.
Sample and Test Code Identification
LabID:
08A
Sample ID:
M-2 GRID 19, 5 FT.
LabID:
09A
Sample ID:
M-2 GRID 19, 10 FT.
LabID:
lOA
LabID:
llA
Sample ID:
M-2 GRID 19, 10 FT.
Sample ID:
M-2 GRID 9, 5 FT.
LabID:
12A
Sample ID:
M-2 GRID 9, 10 FT.
Test Codes and Names
3050
CD AE2
CR AE2
PB AE2
AG AE2
8240s
PH_S
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
pH (Soil)
Test Codes and Names
3050
CD AE2
CR AE2
PB AE2
AG AE2
8240s
PH_S
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
pH (Soil)
Test Codes and Names
3050
CD AE2
CR AE2
PB AE2
AG AE2
8240S
PH_S
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
pH (SoU)
Test Codes and Names
8240S Volatile Organics
Test Codes and Names
3050
CD AEZ CR AE2
PB AE2
AG AE2
8240s
PH_S
Acid Digestion
Cadmium Chromium
Lead
Silver
Volatile Organics
pH (Soil)
Test Codes and Names
3050
CD AE2
CR AE2
PB AE2
AG AE2
8240S
PH_S
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
pH (Soil)
Workorder Comment*!
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,9045A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,9045A
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,9045A
Method
SW-846, 8240
Method
SW-846, 3050
SW-846, 6010 SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,904SA
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846,9045A
Page #:2
This is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample' ID: M-2 GRID 30, 5 FT. LabID: 9411008-OlA Collected: 10/31/94 13:20:00
TEST RESULT DNITS DETECTION ANALYZED BY
LIMIT
METH0D/C1AS#
Acid Digestion
Cadinium
Chromium
Lead
Silver
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Qj^orobenzene
Jroethane
Rloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
11/02/94
1.44
15.8
10.8
U
U
U
U
U
U
U
, U
D
. U
u u u u u u u u u u
u
u
u D
u D
u u
u u u u D
U
U
U
u u u
u u
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.1
0.3
1.7
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
LVD
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
Page ff: 3
November 18, 1994 12:23 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-2 GRID 30, 5 FT. LabID: 9411008-OlA Collected: 10/31/94 13:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
o-Xylene U ug/Kg 10 11/10/94 JMA
SW-846, 8240
95-47-6
Surrogate/Recovery Data For Volatile Organics 8240S
pH (Soil)
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
7.82 pH Unit
%Recovery
98.8
97.2
92.2
Recovery Limits
81 TO 117
74 TO 121
70 TO 121
11/03/94 MTB SW-846,9045A
Sample ID: M-2 GRID 30, 10 FT. LabID: 9411008-02A Collected: 10/31/94 13:30:00
TEST
Acid Digestion
Cadmliim
Chromium
Lead
Silver
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chl orobenz ene
Chloroethane
2-Chloroethylvinyl ether
Chlorofonn
Chloromethane
Dibromochlorometheme
1,1-Dichloroetheme
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
REStTIiT
11/02/94
0.
16
IC
0.
53
.7
.8
20
U
U
U
U
D
a U
U
U
U
D
D
U
U
D
U
U
U
U
D
tJNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
1.6
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
BY
LVD
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
3050
6010 ^H
6010
6010
6010
8240
Page ff: 4
November 18, 1994 12:23
Sample ID: M-2 GRID 30, 10 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9411008-02A CoUected: 10/31/94 13:30:00
TEST
Volatile Organics
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2-Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Tri chloroe thane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
U
U
U
U
U
U
U
U
U
u u
u u u u D
D
D
U
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
.10
10
10
10
10
10
10
10
10
10
10
Al^ALYZED
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
i^k Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-
pH (Soil)
Dichloroethane-d4
7, .80 pH Unit
%Recovery
99.6
97.5
91.8
METHOD/CAS#
SW-846, 8240
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
11/03/94
TO 117
TO 121
TO 121
MIB SW-846,9045A
Sample ID: M-2 GRID 54, 5 FT. LabID: 9411008-03A CoUected: 10/31/94 13:45:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmliim
Chromium
Lead
Silver
11/02/94
0.97
14.2
11.6
0.74
DATE
ug/g
ug/g
ug/g
ug/g
0.2
0.4
1.8
0.2
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
0. Page ff: 5
November 18, 1994 12:23 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-2 GRID 54, 5 FT. LabID: 9411008-03A CoUected: 10/31/94 13:45:00
TEST RESULT
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromoform
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2 -Chloroethylvinyl ether
Chloroform
Chloromethane
D ibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexsmone
trems-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroethane
Te trachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
Tri chlorofluoromethane
Vinyl Acetate
vinyl Chloride
o-Xylene
U
U
D
D
D
U
U
U
D
D
U
U
D
D
U
U
D
U
U
D
D
D
D
U
U
D
U
U
U
U
D
D
U
D
D
U
D
U
U
D
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 824OS
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
pH (Soil) 7 .59 pH Dnit
%Recov8ry
100
98.9
92.1
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5 ^^
10061-02-6 ^m
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
11/03/94
TO 117
TO 121
TO 121
MTB SW-846,9045A
Page ff: 6
November 18, 1994 12:23
#
Sample ID: M-2 GRID 54, 10 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9411008-04A CoUected: 10/31/94 14:00:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene toroethane
nloroethylvinyl ether
oroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexemone
trems-1,2-Dichloroethene
1,2-Dichloropropane
cis-l,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
11/02/94
0.45
14.6
9.93
0.51
U
U
U
U
U
D
D
D
U
U
U
U
D
D
U
U
U
U
U
U
U
U
U
D
U
U
D
U
U
U
U
U
U
U
U
U
U
D
D
U
D
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.1
0.4
1.8
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
11/10/94
11/10/94
11/10/94
II/:LO/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/:L0/94
11/10/94
11/10/94
11/10/94
lX/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
11/10/94
LVD
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Page ff: 7
November 18, 1994 12:23 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-2 GRID 54, 10 FT. LabID: 9411008-04A CoUected: 10/31/94 14:00:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
pH (Soil)
SW-84e, 8240
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate %Recovery
Toluene-d8 99.3
Bromofluorobenzene 97.0
1,2-Dichloroethane-d4 91.7
7.65 pH Unit
Recovery Limits
81 TO 117
74 TO 121
70 TO 121
11/03/94 MTB SW-846,9045A
Sample ID: M-2 GRID 22, 5 FT. LabID: 9411008-05A CoUected: 10/31/94 14:10:00
TEST
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2 -Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexcmone
trans-1,2-Dichloroethene
1,2-Dichloropropane
RESULT
11/02/94
0 58
19.6
9
4
91
U
BJ
D
U
U
D
D
U
U
U
U
U
U
D
D
U
U
U
U
U
D
U
U
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
1.7
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
BY
LVD
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 3050
SW-846, 6010
SW-846, 6010 ^P
SW-846, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
Page ff: 8
November 18, 1994 12:23
•
Sample ID: M-2 GRID 22, 5 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9411008-05A CoUected: 10/31/94 14:10:00
TEST
Volatile Organics
cis-l,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Te t rachl oroe thene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
A w
pH (Soil)
RESULT
U
U
u u D
U
U
U
U
U
u
u 3 BJ
U
U
D
U
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
7.72 pH Unit
%Recovery
100
100
102
METHOD/CAS#
SW-846, 8240
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
11/03/94
TO 117
TO 121
TO 121
MTB SW-846,9045A
Sample ID: M-2 GRID 22, 5 FT. DUP. LabID: 9411008-06A CoUected: 10/31/94 14:10:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
Chromium
Lead
Silver
pH (Soil)
11/02/94
U
16.8
10.3
0.20
7.74
DATE
ug/g
ug/g
ug/g
ug/g
pH Unit
0
0
1,
0,
.1
.3
.7
.2
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
11/03/94
LVD
LVD
LVD
LVD
LVD
MTB
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,9045A
•
Page ff: 9
November 18, 1994 12:23 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-2 GRID 22, 10 FT. LabID: 9411008-07A CoUected: 10/31/94 14:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Add Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromome thane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2 -Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexemone
trems-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Tri chlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
/02/94
0.44
17.5
9.81
U
4 BJ
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u u
u
u
u u u u u 2 BJ
U
U
U
U
U
5 BJ
U
U
U
U
U
u
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.1
0.3
1.7
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
LVD
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Page ff: 10
November 18, 1994 12:23
Sample ID: M-2 GRID 22, 10 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9411008-07A CoUected: 10/31/94 14:20:00
TEST RESULT UNITS DETECTION AtTilLLYZED BY
LIMIT
METHOD/CAS#
Volatile Organics SW-846, 8240
Surrogate/Recovery Data For Volatile Organics 8240S
pH (Soil)
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
7.87 pH Unit
%Recovery
101
100
98.9
Recovery Limits
81 TO 117
74 TO 121
70 TO 121
11/03/94 MTB SW-846,9045A
Sample ID: M-2 GRID 19, 5 FT. LabID: 9411008-08A CoUected: 10/31/94 14:32:00
TEST RESULT UNITS DETECTION ANilJiYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
omlum
Lead
Silver
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromome theme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroe thane
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropane
11/02/94
1.47
18.1
11.7
0.39
4 BJ
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.1
0.3
1.7
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
LVD
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
3050
6010
6010
6010
6010
8240
# Page#: 11
November 18, 1994 12:23 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-2 GRID 19, 5 FT. LabID: 9411008-08A CoUected: 10/31/94 14:32:00
TEST
Volatile Organics
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
Tri chlorofluorome thane
Vinyl Acetate
vinyl Chloride
O-Xylene
pH (Soil)
RESULT
6
Surrogate
Surrogate
Toluene-d8
U
U
u
u
u
u
u
u
u
u
u
u BJ
u
u
u
u
u D
i/Re
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
::overy Data For Volatile Organics 8240S
Bromofluorobenzene
1,2-Dichloroethane-d4
7 73 pH Unit
%Recovery
99.9
98.5
101
METHOD/CAS#
SW-846, 8240
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits ^B
81
74
70
11/03/94
TO 117
TO 121
TO 121
MTB
^^
SW-846,904 5A
Sample ID: M-2 GRID 19, 10 FT. LabID: 9411008-09A CoUected: 10/31/94 14:51:00
TEST
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
Acetone
Acrolein
RESULT
11/02/94
1.03
20.5
14.0
0.48
4 BJ
U
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
1.7
0.2
10
10
ANALYZED
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
11/14/94
11/14/94
BY
LVD
LVD
LVD
LVD
LVD
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
3050
6010
6010
6010
6010
8240
Page ff: 12
November 18, 1994 12:23
Sample ID: M-2 GRID 19, 10 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
: LabID: 9411008-09A CoUected: 10/31/94 14:51:00
TEST RESULT
Volatile Organics
Acrylonitrile
Benzene
Bromodichlorometheme
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2 -Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheme
1,1-pi chloroe thane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexcmone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
^1^^-Di chlorobenzene
•Hv-Dichlorobenzene
1^-Dichlorobenzene
Ethylbenzene
Methylene Chloride 2
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane 6
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluorometheme
vinyl Acetate
Vinyl Chloride
o-Xylene
Surrogate
Surrogate
Toluene-d8
U
U
U
u
u u u u u u u u u u u u u u u u u u u u u u BJ ,
u u u u u BJ
u
u
u
u u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
A17ALYZED
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/:L4/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/:L4/94
11/:L4/94
(/Recovery Data For Volatile Organlci
Bromofluorobenzene
1,2 -Dichloroethane-d4
pH (Soil) 7. ,74 pH Unit
%Recovery
102
100
101
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
3 8240S
METHOD/CAS#
SW-846, 8240
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
11/03/94
TO 117
TO 121
TO 121
MTB SW-846,9045A
Page ff: 13
November 18, 1994 12:23 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-2 GRID 19, 10 FT. LabID: 9411008-lOA CoUected: 10/31/94 14:51:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorometheme
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
4
-
6
BJ
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0
u u
u u
u
u u u u
u u u u u u u BJ
u u u u
u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-dB
Bromofluorobenzene
1,2-Dichloroetheme - d4
%Recovery
99.8
101
101
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5 ^^
10061-02-6 ^^
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
Page ff: 14
November 18, 1994 12:23
Sample ID: M-2 GRID 9, 5 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9411008-llA CoUected: 10/31/94 15:09:00
TEST RESULT XJNITS DETECTION ANACiYZED BY
LIMIT
METHOD/CAS#
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
foroethane
|loroethylvinyl ether
oroform
Chloromethane
Dibromochlorometheme
1,1-Dichloroetheme
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trems-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
11/02/94
0.57
17.2
8.98
0.60
4 BJ
U
U
U
U
U
U
U
U
1 J
u u u u u u u u u u u u u
u u u u u u u u u u u 7 BJ
u u
u u
u u
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.1
0.3
1.7
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
LVD
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Page ff: 15
November 18, 1994 12:23 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-2 GRID 9, 5 FT. LabID: 9411008-llA CoUected: 10/31/94 15:09:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/C:AS#
Volatile Organics
pH (Soil)
Surrogate/Recovery Data For Volatile
Surrogate %Recovery
Toluene-d8 100
Bromofluorobenzene 98.4
l,2-Dichloroeth6me-d4 104
7.77 pH Unit
SW-846, 8240
Organics 824OS
Recovery Limits
81 TO 117
74 TO 121
70 TO 121
11/03/94 MTB SW-846,9045A
Sample ID: M-2 GRID 9, 10 FT. LabID: 9411008-12A CoUected: 10/31/94 15:17:00
TEST
Acid Digestion
Cadmium
Chromium
Lead
Silver
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorometheme
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trems-1,2-Dichloroethene
1,2-Dichloropropane
RESULT
11/02/94
1.
22
i:
0.
3
14
.1
.4
58
BJ
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
UNITS
DATE
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
1.7
0.2
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
BY
LVD
LVD
LVD
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 3050
SW-846, 6010
SW-846, 6010 ^P
SW-846, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
Page ff: 16
November 18, 1994 12:23
Sample ID: M-2 GRID 9, 10 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9411008-12A CoUected: 10/31/94 15:17:00
TEST
Volatile Organics
cis-l,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
vinyl Acetate
Vinyl Chloride
o-Xylene
§ I^F
pH (Soil)
RESULT
6
Surrogate
Surrogate
Toluene-d8
U
U
U
U
U
U
u
u u u u u BJ
U
U
U
u
u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANi^liYZED
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
11/14/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
i/Recovery Data For Volatile Organics 8240S
Bromofluorobenzene
1,2-Dichloroetheme-d4
7, .84 pH Unit
%Recovery
101
97.7
101
METHOD/CAS#
SW-846, 8240
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
11/03/94
TO 117
TO 121
TO 121
MTB SW-846,9045A
Page ff: 17
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1. IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the calibration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
w y"
ENVIRONMENTAL LAB WORK REQlfEST
<g^ ^O
"• TfflOKOL ENVIRONMENTAL LABORATORY LWR No. EI0445
/I f^uJAL/CifJ2^
EXTENSION
6S7io
OOSTCBNTESL
1/400
WOBKOBDBB
/Ei^
DAIS
^ ORGAMZAIION
EMI/IZO ^^6tl^
MAILBTOP
Zo/€:
•EPORT BESULIS TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TVPE LOCATION TIME TEST KEMARKS
/C'lf'i^ ^ MP of M'243 /o/o
2- StJiru zoz^
CJ 1/n^ T-Pi-II /O/O
So//nu Toz.. II y Ithf l/QC ' €>Z4-0
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1131 Kfc - 82^0
CHAIN OF CUSTODY
KEUNQVISHED BY
\^?/I/^JL^
DATE
//>-zy-f<f
TIME
/-Z'.i/J
RECEIVED BY DATE
7/7- ^r-f^
TIME
/^f'^
FOR LABORATORY USE ONLY
DATCOOMFlEnD DATSREFORIBD
ENVIRONMET^TAL LAB WORK REQUEST
THIOKOL ENVIRONMENTAL LABORATORY
f^/f977D
Af U}/t(Jj^it-^370 1/460 I /3?40 I Ca-l^-f^
DAIS
OBGANUAHON
^ur/^ ^/v^/^^ 3o/e •voBT antiLn TOl
HELEN WARD. MS 301
SAMPLE INFORMATION
SAMPLE DATE TVPE LOCATION TIME TEn REMARKS
1. 5tt)Mt' ZcZ. y kt£o-f/A'24Z If^f f2<l Cr^ A^, Ph/Sc:
fi^ /f/kk MCr ^ 2- S'tJAiU ZOZ.
GJ-H^ <:Pt-'I If \m II
CJ ^74 -LU {/
*• SUIACII 20 Z.
cj^74 -za
y
//STD l/Oc-ez^O
l/ff CJ Cr, fi^,pi^ R<^
//^ ///riy: hr^ 5 "SijUMU 2^2-
^frt'i^ Bfartt ^
y IHO \7oC' <B^o
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CHAIN OF CUSTODY
RELINQUISHED BY
v^y^^.
DAIE
//>'ZT^^
TIME
/t4^
RECEIVED BY
7//7^//A....^
DATE
- y^ - isr- 9<^
TIME
/>yc
1
FOR LABORATORY USE ONLY
DAIBOOMIlEnD DAIESEPOnBD •GNAnna
November 23, 1994 CERTIFICATE OF ANAI.YSIS
# SENT Environmental Monitoring
TO: Helen Ward
MIS 301
A.F. WALKER, MIS 301E
Ext 5390
RESULTS BY SAMPLE
ANALYZED
BY:
Tluokol Corporation
Science & Engineering
P.O. Box 707
'Brigham aty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Orderly 9410020 Sample and Test Code Identification
LabID:
OIA
LabID:
02A
^ 1 r
LabID:
03A
LabID:
04A
LabID:
05A •
1
Sample ID:
M-243,N.E.; GD 16
Sample ID:
M-243,N.E.; OD 16,
Sample ED:
M-24i,N.E.;GD30,
Sample ID:
M-243,N.E.;aD30,
Sample ID:
M-24^,N.E.;GD59,
,2 FT.
,4 FT.
2 FT.
SFT.
2 FT.
Test Codes and Names
HMX
NG
3050 BE AE2
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
824DS
HMX
Nitroglycerine
Acid Digestion Beryllium
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NG
3050
BE AE2
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8240s
HMX
Nitroglycerine
Acid Digestion
Beryllium
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NG
3050
BE AE2
CD AE2
CR AE2
PB AE2
AG AEZ
HG CV2
8240S
HMX
Nitroglycerine
Acid Digestion
Beryllium
Cadmium
Chromium
Lead
Silver
Mercuty
Volatile Organics
Test Codes and Names
HMX
NG
3050
BE AE2
CD AE2
CR AE2
PB AE2
AG AE2
HG~CV2
824SS
HMX
Nitroglycerine
Acid Digestion
Betyllium
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Orgatucs
Test Codes and Names
HMX
NO
3050
BE AE2
CD AE2
HMX
Nitroglycerine
Acid Digestion
Beryllium
Cadmium
Page #: lof
Method
SOP 420
SOP 420
SW-846, 3050 SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
Work Order <^ 9410020 Sample and Test Code Identification
LabID:
OSA
LabID:
06A
LabID:
07A
LabID:
08A
LabID: 09A
LabID:
lOA
LabID:
llA
LabID:
12A
Sample ID:
M-243,N.E.; GD 59, 2 FT.
Sample ID:
M-243,N.E.; GD59,2 FT. DUP
Sample ID:
M-243,N.E.; GD 59, 5 FT.
Sample ID:
M-243,N.E.; GD59,5 FT. DUP
Sample ID:
M-243,N.E.; GD 74, 2 FT.
Sample ID:
M-243,N.E.; RINSE BLANK
Sample ID:
M-243,N.E.; OD 74, 5 FT.
Sample ID:
M-243,N.E.; RINSE BLANK
Test Codes and Names
CR AE2
PB AE2
AO AE2
HG CV2
8240S
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
8240S Volatile Organics
Test Codes and Names
HMX
NG
3050
BE AE2
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
8240s
HMX
Nitroglycerine
Acid Digestion
Beryllium
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
HMX
NG
3050
BE AE2
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
HMX
Nitroglycerine
Acid Digestion
Beryllium
Cadmium
Chromium
Lead
Silver
Mercuty
Test Codes and Names
HMX NG
3050
BE AE2
CD AE2
CR AE2
PB AE2
AG AE2
HO CV2
8240S
HMX
Nitroglycerine
Acid Digestion
Beryllium
Cadmium
Chromium
Lead
Silver
Mercuiy
Volatile Organics
Test Codes and Names
8240 Volatile Organics
Test Codes and Names
HMX
NG
3050
BE AE2
CD AEZ
CR AE2
PB AEZ
AG AEZ
HG CV2
8240s
HMX
Nitroglycerine
Acid Digestion
Beryllium
Cadmium
Chromium
Lead
Silver
Mercuiy
Volatile Oiganics
Test Codes and Names
HMX
NG
3010
BE AEZ
CD AEZ
CR AEZ
PB AEZ
AG AEZ
HG CV2
HMX
Nitroglycerine
Acid Digestion
Beryllium
Cadnuum
Chromium
Lead
Silver
Mercury
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SW-846, 8240
Method
SOP 420
SOP 420
SW-846, 3050
SW-84«, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846. 8240
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 7471
SW-846, 8Z40
Method
SW-846, 8240
Method
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SOP 420
SOP 420
SW-846, 3010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
Page #:2
Workorder Comnments
J^<y^
Certifterf^y
Page #:3
This is to cenify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: M-243,N.E.; GD 16, 2 FT. LabID: 9410020-01A Collected: 10/25/94 10:10:00
TEST RESULT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HHZ
Ml troglycerine
Acid Digestion
Beryllium
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromoform
Bromomethane
2-Buteuione
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2 -Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexemone
trems-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
U
D
11/02/94
U
0.53
13.4
D
D
D
13 B
U
D
D
U
D
D
10 B
D
D
D
U
U
D
D
D
D
D
D
U
D
D
U
D
D
D
D
D
2 BJ
U
U
ug/g
ug/g
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
.01
.02
0.1
0.1
0.3
1.6
0.2
0.023
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
11/04/94
11/04/94
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/10/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
CFP
CFP
LVD
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
Page ff: 4
November 23, 1994 15:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample BD: M-243,N.E.; GD 16, 2 FT.., LabID: 9410020-01A CoUected: 10/25/94 10:10:00
TEST
Volatile Organics
RESULT
1,1,2,2-Tetrachloroethane . U
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
U
u 6 BJ
U
D
Trichlorofluorometheme U
vinyl Acetate
Vinyl Chloride
o-Xylene
. U
U
u
tJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
ANALYZED
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
%Recovery
106
108
111
METHOD/CAS#
SW-846, 8240
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
S-'mpIe ID: M-243,N.E.; GD 16, 4 FT. LabID: 9410020-02A Collected: 10/25/94 10:25:00
«T
HMX
Nitroglycerine
Add Digestion
Beryllium
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
RESULT
D
U
11/02/94
U
0.91
12.9
U
U
U
16 B
U
U
U
UNITS
ug/g
ug/g
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
.01
.02
0.1
0.1
0.3
1.5
0.2
0.015
10
10
10
10
AflACiYZED
11/04/94
11/04/94
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/10/94
11/03/94
11/03/94
11/03/94
11/03/94
BY
CFP
CFP
LVD
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
METHOD/CAS#
SOP 420
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
3050
6010
6010
6010
6010
6010
7471
8240
•
Page ff: 5
November 23, 1994 15:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ED: M-243,N.E.; GD 16, 4 FT. Lab ID: 9410020-02A Collected: 10/25/94 10:25:00
TEST
Volatile Organics
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochlorometheme
1,1-Dichloroetheme
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
Tlichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
u
u
u 10 B
U
U
U
U
U
u
u
u
u
u
u
u
u V
u
u
u D
D
U
2 BJ
u
u u u
u
15 B
U
U
U
U
D
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
%Recovery
106
106
109
METHOD/CAS#
SW-846, 8240
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7 ^^
100-41-4 ^M
75-09-2 ^^
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
Page ff: 6
November 23, 1994 15:03
.Sample ID: M-243,N.E.; GD 30, 2 FT,
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9410020-03A Collected: 10/25/94 10:50:00
TEST RESULT UNITS DETECTION A:raijYZED BY
LIMIT
METHOD/CAS#
HMX
Nltroglycerine
Acid Digestion
Beryllium
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
JJH^lonitrile
fl^Bzene
ilKmodi chl orome thane
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2-Pentemone
Styrene
1,1,2,2-Tetrachloroethane
u
u
11/02/94
0.37
0.91
18.2
5.26
U
U
9 BJ
D
U
U
U
U
U
U
D .
U
U
D
U
U
U
U
u u D
U
U
U
U
D
U
D
U
U
2 BJ
U
U
D
ug/g
ug/g
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
.01
.02
0.1
0.1
0.3
1.5
0.2
0.032
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
11/04/94
11/04/94
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/10/94
11/03/94
11/03/94
.11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
CFP
CFP
LVD
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
• Page ft: 7
November 23, 1994 15:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-243,N.E.; GD 30, 2 FT. Lab ID: 9410020-03A Collected: 10/25/94 10:50:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Te trachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Tri chlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
u
u 9 BJ
U
U
D
U
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
Toluene-d8
Bromofluorobenzen e
1,2-Dichloroetheme-d4
10
10
10
10
10
10
10
10
10
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 824OS
%Recovery
107
104
109
SW-846, 8240
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
Sample ID: M-243,N.E.; GD 30, 5 FT. Lab ID: 9410020-04A CoUected: 10/25/94 10:58:00
TEST
HMX
Nltroglycerine
Acid Digestion
Beryllliun
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorome thane
RESULT
U
u
11/02/94
0.26
0.12
16.5
4.48
U
D
10 B
U
U
D
U
UNITS
ug/g
ug/g
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
.01
.02
0.1
0.1
0.3
1.5
0.2
0.026
10
10
10
10
10
ANALYZED
11/04/94
11/04/94
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/10/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
BY
CFP
CFP
LVD
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
METHOD/rAS# i
^
SOP 420
SOP 420
SW-846,
SW-846,
SW-84 6,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
3050
6010
6010
6010
6010
6010
7471
8240
i
Page ff: 8
November 23, 1994 15:03
m
>„^ple ID: M-243,N.E.; GD 30, 5 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9410020-04A CoUected: 10/25/94 10:58:00
TEST
Volatile Organics
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Oji^'lbenz ene
«^Pylene Chloride
SIRthyl - 2 - Pentemone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
U
U
22 B
U
U
u u u u u u u u D
U
U
u u - D
u u u D
2 BJ
D
D
U
U
U
11 B
U
D
D
n D
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
%Recovery
106
109
110
METHOD/CAS#
SW-846, 8240
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
#
Page ff: 9
November 23, 1994 15:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-243,N.E.; GD 59, 2 FT. LabID: 9410020-05A CoUected: 10/25/94 11:20:00
TEST
HMX
Nltroglycerine
Acid Digestion
Beryllium
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorometheme
Bromoform
Bromometheme
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
D ibromochlorome thane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2-Pentemone
Styrene
1,1,2,2-Tetrachloroethane
RESULT
U
u
11/02/94
0.15
0.94
12.7
4.84
U
U
11 B
U
U
D
U
D
U
20 B
D
U
U
D
U
D
U
D
U
U
D
U
U
U
U
U
U
U
U
u D
U
U
U
UNITS
ug/g
ug/g
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTIOM
LIMIT
.01
.02
0.1
0.1
0.3
1.6
0.2
0.023
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
r ANALYZED
11/04/94
11/04/94
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/10/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
BY
CFP
CFP
LVD
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SOP 420
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01
10061-02
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
3050
6010
6010
6010
6010
6010
7471
8240
^^
^
-5
-6
Page ff: 10
November 23, 1994 15:03
#
Sample ID: M-243,N.E.; GD 59, 2 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 941(XI20-05A CoUected: 10/25/94 11:20:00
TEST
Volatile Organics
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene.
RESULT
U
U
7 BJ
U
U
Trichlorofluoromethane U
Vinyl Acetate
Vinyl Chloride
o-Xylene
U
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
A].^ALYZRD
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
%Recovery
105
104
112
METHOD/CAS#
SW-846, 8240
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
Sample ID: M-243,N.E.;GD59,2 FT. DUP LabID: 9410020-06A CoUected: 10/25/94 11:20:00
^T
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorometheme
Bromoform
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexemone
trems-l,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
RESULT
8 BJ.
D
U
U
u
u u 17 B
D
U
- u
u - u
u u u u u u u u ,u D
D
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
AITALYZED
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
Page#: 11
November 23, 1994 15:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-243,N.E.; GD59,2 FT. DUP LabID: 9410020-06A CoUected: 10/25/94 11:20:00
TEST
Volatile Organics
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
RESULT
U
u u 2 BJ
D
U
1,1,2,2-Tetrachloroethane U
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Tri chloroethene
D
D
6 BJ
U
U
Trichlorofluoromethane D
Vinyl Acetate
Vinyl Chloride
o-Xylene
U
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
%Recovery
106
106
108
METHOD/CAS#
SW-846, 8240
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
^^^
MKk
Sample ID: M-243,N.E.; GD 59, 5 FT. LabID: 9410020-07A CoUected: 10/25/94 11:31:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMX
Nltroglycerine
Add Digestion
Beryllium
Cadmium
Chromium
Lead
Silver
Mercury
u
u
11/02/94
D
0.78
10.8
2.64
U
D
ug/g
ug/g
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
.01
.02
0.1
0.1
0.3
1.3
0.2
0.016
11/04/94
11/04/94
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/10/94
CFP
CFP
LVD
LVD
LVD
LVD
LVD
LVD
CRS
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
Page ff: 12
November 23, 1994 15:03
m
Sample ID: M-243,N.E.; GD 59, 5 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 941()020-07A CoUected: 10/25/94 11:31:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chloromethane
D ibromochlorometheme
1,1-Dichloroetheme
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
^1^-1,3 -Dichloropropene
flHns -1,3 -Dichloropropene
j^ -Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Tri chloroethane
Trichloroethene
Tri chlorofluorome thane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
8 BJ
U
U
U
U
U
U
18 B
U
U
U
U
U
U
U
U
U
U
U
u
u u
D
U
D
U
D
U
2 BJ
U
U
U
U
U
25 B
U
U
U
U
D
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
11/03/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-•Dichloroethane-d4
%Recovery
106
109
110
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
# Page ff: 13
November 23, 1994 15:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-243,N.E.; GD59,5 FT. DUP LabID: 9410020-08A CoUected: 10/25/94 11:31:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMX
Ml troglycerine
Acid Digestion
Beryllium
Cadmium
Chromium
Lead
Silver
Mercury
u
u
11/02/94
D
0.78
13.7
2.40
0
U
ug/g
ug/g
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
.01
.02
0.1
0.1
0.3
1.5
0.2
0.021
11/04/94
11/04/94
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/10/94
CFP
CFP
LVD
LVD
LVD
LVD
LVD
LVD
CRS
SOP
SOP
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
420
420
3050
6010
6010
6010
6010
6010
7471
Sample ID: M-243,N.E.; GD 74, 2 FT. LabID: 9410020-09A CoUected: 10/25/94 11:50:00
TEST
HMX
Nitroglycerine
Acid Digestion
Beryllium
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
RESULT
D
U
11/02/94
0.42
1.02
15.5
7.08
U
U
12 B
D
D
U
UNITS
ug/L
ug/g
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
.01
.02
0.1
0.1
0.3
1.7
0.2
0.021
10
10
10
10
ANALYZED
11/04/94
11/04/94
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/10/94
11/07/94
11/07/94
11/07/94
11/07/94
BY
CFP
CFP
LVD
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
METHOD/CAS# ^^
SOP 420
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
3050
6010
6010
6010
6010
6010
7471
8240
Page ff: 14
November 23, 1994 15:03
Sample ID: M-243,N.E.; GD 74, 2 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9410020-09A CoUected: 10/25/94 11:50:00
TEST
Volatile Organics
Bromodichloromethane
Bromoform
B romome thane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trems T1,3-Dichloropropene
,1,2-Dichlorobenzene
1,3-Dichlorobenzene
.^l^rDichlorobenzene
VHylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Te t rachl oroe thene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
u u
u 15 B
U
U
U
0
U
4 J
U
U
U
U
U
U
U
D
U
U
U
U
U
D
U
U
D
U
D
U
5 BJ
U
D
U
U
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
%Recovery
105
103
112
METHOD/CAS#
SW-846, 8240
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
• Page ff: 15
November 23, 1994 15:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-243,N.E.; RINSE BLANK LabID: 9410020-lOA CoUected: 10/25/94 11:40:00
TEST RESULT
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromoform
Bromometheme
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
D ibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexemone
trems-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2, 2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Tri chlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
Surrogat
Surrogate
Toluene-d8
170
U
D
U
U
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
u
u
u
u
u D
D
D
D
D
D
D
D
D
D
D
U
D
D
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
2.5
10
3.1
0.83
1.1
2.1
2.2
3.3
1.6
1.1
0.97
1.2
1.7
0.90
3.1
0.83
1.0
1.3
1.4
1.7
1.8
1.1
1.3
1.1
0.71
0.54
1.2
1.0
1.5
1.4
1.3
1.4
1.1
0.57
0.95
1.5
1.2
1.3
10
1.4
1.3
ANALYZED
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
e/Recovery Data For Volatile Organics 8240
Bromofluorobenzene
1,2-Dichloroetheme-d4
%Recovery
98.5
97.1
95.6
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5 ^^
10061-02-6 ^V
95-50-1 ^
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
88
86
76
TO 110
TO 115
TO 114
Page ff: 16
November 23, 1994 15:03
Sample ID: M-243,N.E.; GD 74, 5 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9410020-11A CoUected: 10/25/94 11:58:00
TEST
HMX
Nitroglycerine
Acid Digestion
Beryllium
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
^l^ylonitrile
vVzene
Bromodi chlorometheme
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheme
1,1-Dichloroetheme
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexemone
trems-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroethane
RESULT
U
D
11/02/94
0.13
1.48
10.9
3.98
D
U
5 BJ
D
D
U
D
U
U
15 B
U
U
U
U
D
2 J
D
D
D
U
U
U
U
U
D
D
D
U
U
U
U
U
D
D
UNITS
ug/g
ug/g
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
.01
.02
0.1
0.1
0.3
1.4
0.2
0.021
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
11/04/94
11/04/94
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/10/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
BY
CFP
CFP
LVD
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SOP 420
SOP 420
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
G7-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
Page ff: 17
November 23, 1994 15:03 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-243,N.E.; GD 74, 5 FT. LabID: 9410020-llA CoUected: 10/25/94 11:58:00
TEST
Volatile Organics
Te t rachl oroe thene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
RESULT
U
u 5 BJ
D
D
Trichlorofluoromethane U
Vinyl Acetate
Vinyl Chloride
o-Xylene
U
D
D
Surrogate/Re
Surrogate
Toluene-d8
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
ANALYZED
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
11/07/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
covery Data For Volatile Organics 8240S
Bromofluorobenzene
1,2-Dichloroetheme-d4
%Recovery
106
103
111
METHOD/CAS#
SW-846, 8240
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
TO 117
TO 121
TO 121
Sample ID: M-243,N.E.; RINSE BLANK LabID: 9410020-12A CoUected: 10/25/94 12:10:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
HMX
Nltroglycerine
Acid Digestion
Beryllium
Cadmium
Chromium
Lead
Silver
Mercury
u
u
11/02/94
D
8.53
U
46.1
U
U
ug/g
ug/g
DATE
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
.01
.02
2
2
5
25
3
0.15
11/04/94
11/04/94
11/02/94
11/08/94
11/08/94
11/08/94
11/08/94
11/08/94
11/10/94
CFP
CFP
LVD
LVD
LVD
LVD
LVD
LVD
CRS
SOP
SOP
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
420
420
3010
6010
6010
6010
6010
6010
7471
Page ff: 18
•
Data Reporting Qualifierj;
U Compound was analyzed for but not detected. Indicates (X)mpound was below detection limit.
J Indicates an estimated value. This flag is used either whe;n estimating a concentration for
tentatively identified compounds or when tlie mass spectral data indicated the presence of a
compound that meets the identification crite^ria but tlie result is less than the specified
detection limit but greater than zero. (e.g. 1. IJ witli a. detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
£ Estimated value. Result was outside of the calibration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the ispeciiled Umits.
•