DSHW-1994-002395 - 0901a0688013fb8c

n
TfflOKOL CORPORATION
SEMI-ANNUAL RFI PROGRESS REPORT
1 MARCH 1994 - 1 SEPTEMBER 1994
H
SEMI-ANNUAL RFI PROGRESS REPORT
Hll 1 SJ^TEftiBER 1993 - rMARCH'i99»
1. Description and estimation of tiie percentage of tiie RCRA FadtHy Investigation
completed;
Thiokol Corporation initiated Phase I soil sampling for the RFI on 13 October 1993.
To date, soils at the following SWMUs have been sampled:
M-19A Photographic Processing Discharge, SWMU 553;
E-517-W Surface Discharge, SWMU 282;
M-576-N Surface Discharge, SWMU 271;
M-514 Surface Discharge, SWMU 618;
S-501 Surface Discharge, SWMU 266;
M-640 Surface Discharge, SWMU 381;
M-641 Surface Discharge, SWMU 264;
M-585-N Surface Discharge, SWMU 273;
M-606 Surface Discharge, SWMU 527;
M-628 Surface Discharge, SWMU 528;
M-593 Surface Discharge, SWMU 274;
M-636-SW Surface Discharge, SWMU 367;
M-570 Surface Discharge, SWMU 285;
M-197 Surface Discharge, SWMU 483;
M-197-BP Surface Discharge, SWMU 360;
M-702 Surface Discharge, SWMU 620;
A-9 Surface Discharge, SWMU 267; 5^'-(- '^3 - (Mctv^ '"iH
A-2 Surface Discharge, SWMU 560j J^,^
#
O
M-66 Surface Discharge, SWMU 432; »^ M/I U'^M-C. i-WU
M-72 Surface Discharge, SWMU 263; i^ fi/waA i^x t)^-^ '^M
M-67 Surface Discharge, SWMUs 261*4id 433; "^ / y
M-14N and M-14S Surface Discharges, SVS^Js 257'^and 270;
M-53-BP Surface Discharge, SWMU 260^
M-53-E Surface Discharge, SWMU 259; / y
M-33-B and M-33-C Surface Discharges, SWMUs 258 and 413;
M-39 Surface Discharge, SWMU 425;"^^
Combined Surface Discharge for M-8, M-9, M-10, M-52, and M-179-N,
SWMUs 268r611V^269i^409,''472,'4nd ISSy^
M-57 Surface Discharge, SWMU 615;^^
M-55-W Surface Discharge, SWMU 621;^
M-9 Strand Burner Exhaust Discharge, kwMU 652; v/^
M-40 Surface Discharge, SWMU 642;^
M-205 Surface Discharge, SWMU 286;^
T-21-D Surface Discharge, SWMU 559; t^
T-6-A Surface Discharge, SWMU 287;^^ y
Old Drum Storage Area East of M-203, SWMU 203; "^
m
#
o
M-114 Surface Discharge, SWMU 426; ^ ^
M-227 Hydrofluoric Acid Treatment Unit, SWMU 192; ^
M-9-NE Surface Discharge, SWMU 651; V
*M-186 Industrial Waste LandfiU, SWMU 212; ^^
*M-136 Old Waste OU Disposal Ht, SWMU 208;^
*M-187 Old Drum Storage Area, SWMU 551;^and
*T-1 Photographic Processing Dramfield, SWMU 648;l^
Analytical results were not available from the laboratory in time to be
included with this report.
These sites represent approximately 53 percent ofthe SWMUs in Phase I ofthe RFI.
2. Summaries of all findings;
The raw analytical data for the reporting period is included with this report. This
data will be compared to standards considered to be protective of health and the
environment as outlined in Section 8.0 of the Data Collection Ouality Assurance
Plan, Volume Two, Thiokol RCRA Facility Investigation Workplans.
3. Summaries of aU changes made in the RCRA Fadlity Investigation during the
reporting period;
On 3 August 1994, Thiokol contacted Mr. Scott Hopkins ofthe Division of Solid and
Hazardous Waste seeking permission to modify the workplans for SWMUs 208 and
551 to allow a backhoe to excavate to the required depths for obtaining soil samples.
This modification was requested due to the course nature of the soils at these two
sites which caused both refusal of the hollow stem auger rig to penetrate to the
required depth and the inabiUty to obtain a sample with the split spoon sampler.
Mr. Hopkins indicated that using the backhoe would be acceptable at these sites.
4. Summaries of all contact with representatives of the local community, public interest
groups or State Government during the reporting period;
Correspondence regarding RFI activities has been limited to the Division of SoUd
and Hazardous Waste and the Division of Water QuaUty.
5. Summaries of all problons or potential problems encountered during the reporting
period;
The laboratory providing analytical services for the RFI exceeded the holding times
for the semi-volatUe organic analysis on two samples at SWMUs 259 and 621. The
laboratory reported that the two samples were contaminated with asphalt which
required that the samples be "cleaned up" prior to injection into analytical
instruments. The holding times expired before the samples were prepared for
iJH analysis. These two sites will be resampled for aU constituents of concern.
6. Actions being taken to rectify problems;
Laboratory and Thiokol personnel wiU implement communication controls to ensure
that holding times are observed.
7. Changes in personnd during the reporting period;
There were no changes in personnel during the reporting period which would affect
the RFI work.
8. Projected work for the next reporting period;
SampUng wiU continue at the remaining sites as long as weather permits. Many of
the remaining sites to be sampled are larger areas requiring significantly more
samples to be coUected. Thiokol proposes to conduct sampling at the injection weU
sites at the time the feed lines to the injection weU are intercepted to connect to the
new wastewater treatment plants. This wiU ensure that the weUs contain no free
Uquids which could otherwise travel dovm the auger fUghts and cross contaminate
the deeper soUs.
^ft 9. Copies of daily reports, inspection reports, laboratory and monitoring data.
Copies of the daUy logs and laboratory data are included with this report.
#
# jUJm^As^ 75
y/.V^ c^-S,t ^'^6 fy^kLj^L^/j^^^.
^/pJJ ^^^^^ C/^,a^ S-/^y • yay,f,ynt . ^^^P
Thiokol Corporation RCRA Faciltty Investigation
W0#: 1B940 LWR*:
gfl^. M-M Surface Discharges
DESCRimON: SWMU # 432; Pt of Discharge, Surface
PARAMETERS
Lead
pH
DATE:^/^4>-C^9^
METHOD
6010
9045
TIME: /^o O SAMPLER: pt^/i<
y^y-l hcy^ -SL^^
^
.iSrl.^
©-
k5i i==/3.^S
TUoJto/ Corporation RCRA FaciUty Investigation
W0#: 1B940 LWIW:
SITE: M-66 Surface Discharges
DESCRIPTION: SWMU # 432; Pt of Discharge, 2 ft
PARAMETERS
Lead
pH
METHOD
tiOlO
9045
Mtf/W S^M<^_ ^ .JJ^JJVJLQ
DATE: ^/U^AfzL 9*/ ^^^*^= ZS*-^ SAMPLER: rV^c
^ '^5^ tT/ff' cdoc^-fj O^XAJ^ ^(fi,J(^». - /V-tC^SK-^.^ ^ o^ /Y./> H. d-u^ ^
-^«3—^v<Lt rjjrecryj^ C. itiv-t rj" .
Thiokol Corporation RCRA Fadlity Investigation
WO#: 1B940 LWRC: /U/Fi
SITE: M-66 Surface Discharges,/"^ ^^
DESCRIPTION: SWMU H 432;/2Slt Dn Grad., Surface
PARAMETERS
Lead
pH
METHOD
6010
9045
S>A< vcjj s^ ^>AR<X
^'
H
^ATC: ^; ;^^ y^ TIME: yj»; jtJ SAMPLER: f^^<
I 4 .fSr
-«. j^.' •ft
Gi.'
76
/.g; 3-0 Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWftf: . /
SFTE: M-66 Surface Discharges ,/V/rT'.
DESCRIPTION: SWMU ft *yi;JSTl Dn Grad., 2 ft
PARAMETERS
Lead
pH
METHOD
6010
9045
DATE:^/ ^ ^^ ^y TIME: /S'llc SAMPLER: fu'/j
?|1
lu^wt I'W-S
TKokol Corporation RCRA Facility Investigation
WO#: 1B940 LWR#:
SITE: M-72 Surface Discharge
DESCRIPTION: SWMU WIG,; Pt. of Discharge, Surface
PARAMETERS
Lead
pH
METHOD
6010
9045
SA-^^.JJ ^ifish^A
l/-
^c^ Q.*-^ >
HKTE:^lhAvclH TIME:/^/K^ SAMPLER: A^/J«^_
-.j3:r^
Thiokol Corporation RCRA Facility I
^7?
1*
i^rar .i\
..--Jjm.^.--
Mi'S€ ' Corporal
W0#: 1B940
SITE:
DESCRIPTION:
PARAMETERS
Lead
pH
Facility Investigation
LWR#:
M-72 Surface Discharge
SWMU ii!263; Pt. of Discharge, 2 ft.
METHOD
6010
9045
SAJ'o.^ajtJS^yA^
^
DATE:^>h/),^cl 9V TIME:/^,'S^ SAMPLER: f^/j*
77
4TeO TTiiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: .
SITE: M-72 Surface Discharge ^/9S R.
DESCRIPTION: SWMU #263;J»4rDn Grad., Surface §4V(< t-f^ ShA. ^^V4t^0-
PARAMETERS
Lead
pH
METHOD
6010
9045
DATE^/fMlr^ 9^ TIME:/^.VZ) SAMPLER: ^'^^
Cuhrv¥ '
//^ 'X?^ Thiokol Corporation RCRA Facility Investigation
/' WOJI: 1B940 LWR#: ,
M-72 Surface Discharge _ /fSFt
WO#: 1B940
SITE: M-vz sunace iJiscnarge__ / /-^'
DESCRIPTION: SWMU #263ra5-<rEn Grad., 2 ft. /M^/<->^ S".?/ ot C/4-y . I
1^-
PARAMETERS
Lead
pH
METHOD
6010
9045
DATE: J/ ?H4y<:l 9 V TIME^S^/d 5 SAMPLER: fUl/j*^
^^
iit,**>-t^
V.'Ji^_ TIaokol Corporation RCRA Facility Investigation
W0#: 1B940 LWRjjl:
SITE: M-67 Surface Discharge
DESCRIPTION: SWMU H 261 & 433; Pt of Discharge, Surface k\/)i\r ^^fJ- '•i- G\/'»ri^J' '
PARAMETERS
Lead
pH
METHOD
6010
9045
H DATE:.y/MK^ 9y TIME; '^^/B^ SAMPLER:Pt//j '
'iS^*'\
•" •.. •» _
J^
••'•»'i#''i
78
/y/^f
^1^ CJ^.PlfcXxar<^U^ <?• r''
Thiokol Corporation RCRA Facility Investigation
WOC: 1B940 LWR#:
SITE: M-67 Surface Discharge
DESCRIPTION: SWMU His 261 & 433; Pt of Discharge, 2 ft y^^f'slr SI//- ><- C/jJi^
PARAMETERS
Lead
pH
METHOD
6010
9045
DATE: ^/ }M\fcJ~ 9 V TIME: /f f Z- O SAMPLER: FU'/^C
%> ... ^«^
• :^'vt
i ^^-/^
X l.A-
^. ^il^
^C
Pc^f.
J^^ P/r. ^Kid/^ejL
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR*:
SITE: M-67 Surface Discharge
DESCRIFTIGN: SWMU #s 261 & 433; 25 ft Dn Grad., Surface S^hcZ-'-t-'r*'4^,^
^
PARAMETERS
Lead
pH
METHOD
6010
9045
HATE: ^h\At^-^9y TIME:/V,yC? SAMPLER: A'/j<
eP^ l^gu-n .Jywtdn>J
Thiokol Corporation RCRA Faciltty Investigation
W0#: 1B940
SfTE:
DESCRIPTION:
PARAMETERS
Lead
pH
LWR*:
M-67 Surface Discharge / ^ y
SWMU #s 261 & 433; DU? 26" i?/l G.'iAd 5or_
METHOD
6010
9045
DATE: J/j^/fy TIME: /><>^1AMPLER: F^A^
i^
^
79
Thiokol Corporation RCRA Facility Investigation
WO#: IB940 LWR#: ^ "
**'*•= M-67 Surface Discharge
DESCRnmON: SWMU #s 261 & 433; 25 ft Dn Gradl, 2 ft
PARAMETER.^
hiofjT S//rs .
Lead
pH
METHOD
6010
9045
:!.:i
DATE :^/'^V^y TlME:/^y^ SAMPLER: AV/JC^
hii;
-.1
'AH
AUmycLAM^
n ^ ^:iL C^^lyi-/'^ ft^c^tyU/cjL-^ /^^ ^^^>i*
(flf
<*: •1/-; Thiokol Corporation RCRA Facility Investigation
«r:r_ W0#: 1B940 LWR#:
STTE: M-14-N & M-14-S Surface Discharges
DESCRIPTION: SWMUs #257 & 270; Pt of Discharge, Surface
iL
^M^^^^^^tJ Sf^^UM-J^J-LH
PARAMETERS
Selenium
Thallium
pH
METHOD
6010
6010
9045
DATE: 3/:^//? y TIME: jS'. '^^ SAMPLER:/^^/J
~7^rJ ^J:>.j^d...^ ^//
Thiokol Corporation RCRA Faciltty Investigation
W0#: 1B940 LWR#:
STTE: M-14-N & M-14-S Surface Discharges
DESCRIPTION: SWMUs IfZSJ & 270; Pt of Discharge, 2 ft ^<ajMttiZ^ -^z /Z "-
PARAMETERS
Seleniiim
Thallium
pH
METHOD
6010
6010
_J>«45
DATE; : S/^//?y •nm.:JS:j^ SAMPLER: /^/J <^
'a^
^^^:
. • •' .*
•••AC
80
/•^^.3-
<
J^S- p/iT C-VAA ^.AY/i.- . ^
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#:
SITE: M-14-N & M-14-S Surface Discharges
DESCRIPTION: SWMUs #257 & 270; 25 ft Dn. Grad., Surface CpX^g^^rt^/tl/
PARAMETERS
Selenium
Thallium
pH
METHOD
6010
6010
9045
DATE; 3/PZ/9y- TTME:/^'l^Z.-SAMPLER: ^<^
^Jy^ J>^r CK4J. ^Pi.
••>»y..,
W
m-
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940
SHE:
DESCRIPUON:
PARAMEIERS
Selenium
Thallium
pH
LWR#:
M-14-N & M-14-S Surface Discharges
SWMUs #257 & 270; 25 ft Dn. Grad., 2 ft
METHOD
6010
6010
9045
SMM dci^
DATE: J^/J^//?^ TIME: 1^,'S^ SAMPIXR:^^^/^
P^ ^ ^^ 'P^ G-r^d ^ f^'
Thiokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#:
SITE: M-14-N & M-14-S Surface Discharges
DESCRIPTION: SWMUs #257 & 270; paf^S' P/T Cr^/U "> '
PARAMETERS METHOD
Selenium
ThaUium
pH
^•J. ni.^
6010
6010
9045
DATE; y^^/9^r -nm./S^^S- SAMPLER: ^'^^^
• 81
/J//// (^ -kikf/i h /aionsktt/ /^^ 0/iQ/^i<.
nm^
'-a
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: ^/039C
SITE: M-53-BP Surface Discharge
DESCRIPTION: SWMU #260; Pt of Discharge, Sur
PARAMETERS
Cadmium
Mercury
pH
METHOD
6010
7470
9045
-^
II-DATC: 2/^»^ TIME/I^ ', (/ <-' SAMPLER; ..(-^b
TKokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: ^/^^ pa
SITE: M-53-BP Surface Discharge
DESCRIPTION: SWMU #260; Pt of Discharge, Sur
PARAMETERS
Volatile Organics
Bis(2-EthyUiyexyl) Phthalate
Nitrobenzene
,3o^i^
METHOD
8240
8270
8270
DATE:.y/fi^9 ^ TmE./^'.i'C^ SAMPLER:/WJ«
in ••Ijl
-jHi,
4^.
>j OL^yrj'Hr^^ie'
f
s
I
I,
ll
roi^yh c~f d/ g cA fl»-^~<-^ .a. 1 Thiokol Corporation RCRA FadUty Investigation
WO#: 1B940 LWR#: S/^3 9^^
SITE: M-53-BP Surface Discharge
DESCRIPTION: SWMU #260; Pt of Discharge, 2 ft ^•L tJ/ .^i^ ^ cl,
m
PARAMETERS
Cadmium
Mercury
pH
METHOD
6010
7470
9045
^ 1
.3o \C'
DATE; ,^/p^9y •Yim.:/dl/CI SAMPLER: Ayj <^
%
i
• ^•^t^^^;^^^^^.^:,.^y.;'.r-.-;^-:^^^^^
>
•. •*
•I
aif*^
82
/^//^
TWoJto/ Corporation RCRA FaciUty Investigation
WO#: 1B940 LWR#: ^'/(^^C? ^
SITE: M-53-BP Surface Discharge
DESCRIPTION: SWMU #260; Pt of Discharge, 2 ft Qh
PARAMETERS
VolatUe Organics
Bis(2-EtiiyUiyexyI) nitiialate
Nitroben2ene
METHOD
8240
8270
8270
^
\iATE:3/^?/99 TXm.:/C':/0 SAMPLER :r^/J<
%
•>'
* v
••i»y...
A, JLO^
Js' ,D/r. GhAci' -^*^^<t
Thiokol Corporation RCRA FadUty Investigation •» «^
W0#: 1B940 LWR#: . / &'^a3yC
srre: M-S3-BP Surface Discbarge ^^^^^ /-^
DESCRIPTION: SWMU #260^aS-ff&i. Grad., Sur
S'A.ur^// s-z/^.s^^t^
PARAMETERS
Cadmium
Mercury
pH
METHOD
6010
7470
9045
-CprJhr^*^
DATE:-3?^?/9y TIME:/^;if SAMPLER fu./^^
^:
<V;Jf-.*"
• •U'r-'i
'TKokol Corporation RCRA FadUty Investigation
WO#: 1B940 LWR#: j^ / &/o39 ^
SITE: M-53-BP Surface Discharge
DESCRIPTION: SWMU #260i
/S' liarge^^,^
D;.irtrDn. Grad., Sur
PARAMETERS
VolatUe Organics
Bis(2-EUiyUiyexyl) Phtiialate
Nitrobenzene
METHOD
8240
8270
8270
^
DATE: ^/2 ?/9¥ TIME:/' ' ^<^' SAMPLER: .'^^^J
' Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: l^/a390
SITE: M-53-BP Surface Discharge /^ '
DESCRIPTION: SWMU #260L2«rDn. Grad., 2 ft
-^J,,,r-tO ^l //-4 C/g^ r
PARAMETERS
Cadmium
Mercury
pH
METHOD
6010
7470
9045
DATE: 3/2^i?/^i^ TIME:/i5'/<^^ SAMPLER: FW-^ '
• 83
, Thiokol Corporation RCRA FaciUty Investigation
'^"..y-p W0#: 1B940 LWR#: ^/C^^^>
SITE: M-53-BP Surface Discharge /^ ^
DESCRIPTION: SWMU #260;.M-frDn. Grad., 2 ft
S^^^^J ^,'//H-CJO. T
PARAMETERS
VolatUe Organics
Bis(2-EthyUiyexyl) Phtiialate
Nitrobenzene
METHOD
8240
8270
8270
II
DATE:.JV2 P/9Y TIME:/^ / y^ SAMPLER: f^/J '
JJ^ tt
^u...^ tr ^- cLJckL. r ^ - •^-••^ I.
"^
.^4-^t. .^^M g, /.^iS^jci^
^f^\-yeY^, lAttrA ^i^/^ C.rm \*<.}%. 7 U^/JJ. rftLgy ^/^cH'^ry^tje-
Wl
1^— ^"[B'r-^'-^^^^^^-iS-.ion
/AT3^ ^: M-53.E Surface DischargJ^- ^''^^ ^ '"^
I>^CRIPnON:SWMU#259fp.ofDisd«irge,Su..ace
PARAMETggg
-f.rr:'
Jb?^t/i/ jy^TK^^L^^jA^JltS^ 2
Volatile Organics
METHOD
8240
^ric^2>u-c iixc-^Asi;^!-*'-
tl
-%\
DATC: ^/2^/;^^ TTME:>^/^3 SAMPLER: F^^/S >
ii-
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#:^/^3'Cr^
SITE: M-53-E Surface Discharge
DESCRIPTION: SWMU # 259; Pt of Discharge, 2 ft h?^'ll -f yi.^,/' /UiTr// hli/\^f Lf
PARAMETERS
Volatile Organics
METHOD
8240
^Tr^lV" ^//f vl £4-,,^:^-
If'.l3 J^ J^ DATC:3/^f/j?i^ TIME:^<^!L:^ SAMPLER: rtc//J
L^
••', . ^. ..._;-..^.,';'v-^^;-v'^;-^;lM|
^M
-^^ir . •».
f^-
-11. V
•>,-3
84
<^-^' -Ph . ^MJ- .:Sii<KZ
7%u>il:<;/ Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/^c)^^^
SITE: M-S3-E Surface Discharge
DESCRIPTION: SWMU # 259; 25 ft Dn. Grad., Surface ^/WJT,// ^is
PARAMETERS
Volatile Organics
METHOD
8240 'I'^'^'^^hlCsUjU S^,^
DATE; ,.3/jtfrfi^ TIME: //.'J^ SAMPLER: A'^/J "
U
:"^
J>S J>A^ avacL. ^ /
Thiokol Corporation RCtbV FacUity Investigation
WO*: 1B940 LWR#: {^/oyp O
SITE: M-53-E Surface Discharge
DESOUPTION: SWMU # 259; 25 ft Dn. Grad., 2 ft Mgiyf Si/^H-U^-
PARAMETERS
VolatUe Organics
METHOD
8240
\iAXE3/3^y/9V TIME://.'a25 SAMPLER:/^''/^
m
.v.t..-:^
•i3_
J^:^^<j^ft
72^5^
rUoifco/ Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: S/^J?*^
SITE: M-33-B & M-33-C Surface Discharges
DESCRIPTION: SWMU #s 258 & 413; Pt of Discharege, Surface ShJ^*^ejti>^ S^d-
PARAMETERS
Cadmium
Antimony
pH
METHOD
6010
6010
9045
DATE:^/^/^y TIME: /Sr ^O SAMPLER: A^J <
85 i
-faf^ <d/ d.iscJi^.^is^^ ^ ^ 11 • '
\\^i
Thiokol Corporation RCRA FacUity Investigation
• , ^ ^ W0#: 1B940 LWR#: ^/^S^C
'3 ^ V"^ SITE: M-33-B & M-33-C Surface Discharges
DESCRIPTION: SWMU #$ 258 & 413; Pt of Discharege, 2 ft
PARAMETERS
Cadmium
Antimony
pH
METHOD
6010
6010
9045
DATE: ^/3^/9y 'nME:/S''Y.S SAMPLER: P*^/-J '
"^ ,1^1
.""HI*;
tl.
Vi^
H^
)! I *••'
% I / c^S J>y^ ^y^J. StA-v.^^ . . -S^^*^^. -
; _ r--^ Thiokol Corporation RCRA FadUty Investigation
ISJ^^y W0#: 1B940 LWR#: l^/^S?0
SITE: M-33-B & M-33-C Surface Discharges
DESCRIPTION: SWMU #s 258 & 413; 25 ft Dn Grad., Surface
PARAMETERS
Cadmium
Antimony
pH
METHOD
6010
6010
9045
DATE:_3'/5'!>/Py TIME: Z^",'SJ? SAMPLER: Z'^' -*
-M.
.^^y<±y sk.^^ ^^n-h, \m
'^'>
^
X
<^S' p^,Ji^^, p.'
WO#: 1B940
SITE;
DESCRIPTION:
PARAMETERS
Cadmium
pH
LWR#:
M-33-B & M-33-"
SWMU #s 258 &
^/a39 o
C Surface Discharges
413; 25 ft Dn Grad., 2 ft
METHOD
6010
6010
9045
d^^QjCAy=^M~
m — DATE:^/^^/^"^ TIME:/^'i?Z> SAMPLER: A'^-''
Sa/n^ks /mnyicYkJ h:> M'6^R ALmLu ^ /^Z'T'
40A
•^. • -fl-* ' —w*
. • • • • . ' •- '.Ll .'i •r.-i'.)rU't^\f-A¥.i'
•» * •:•
«•.',••.»•
.'^.••>-r
86
hi^s^
14 /APgiL l^S^
J,£._^J^!^k^_^^jU4Z^k ScAt
.^421^
TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/63f (.
SITE: M-39 Surface Discharge
DESCRIPTION: SWMU #425; Pt of Discharge, Surface
y^Vj^.^oJL^SUto^yJ^-^L__
PARAMETERS
Cadmium
Chromium
SUver
Lead
Antimony
METHOD
6010
6010
6010
6010
6010
^r
J)ATE: ^//^f^'f TmE:/d>f.$0 SAMPLER:/<^J(
• '•Jfcr".
^i»-
^:^:je^-
j5/;L.y^<dki^..-rf..
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 VffM: /^/^39 fi
SITE: M-39 Surface Discharge
DESCRIPTION: SWMU #425; Pt of Discharge, 2 ft h^^iiLsiiPi^_aA
PARAMETERS
Cadmium
Chromium
SUver
Lead
Antimony
METHOD
6010
6010
6010
6010
6010
.s^. i<UV/'C-«^(i_-
J)ATE: ^AY/fH TIME:/^:^^ SAMPLER:/5<^J ^
^^»
%
.S}^^^.^..J[>LsA^^-^^>.-J?tSJ^&:^J^^..-
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: ^ /CSf^
SITE: M-39 Surface Discharge
DESCRIPTION: SWMU #425; 25 ft Dn. Grad., Surface
PARAMETERS
Cadniium
Chromium
SUver
Lead
Antimony
METHOD
6010
6010
6010
6010
6010
)CKOMM^ ——
DATE: Y/'Y/'^'^ 'VmE.://',a$ SAMPLER: f^/j
pii'f-:i'ATm.ytn:'-:U,xm,ff<i::^^::::':X^i^\:.-.:':'^
•
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Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR#: ^/a39(.
srre: M-39 Surface Discharge
DESCRIPTION: SWMU #425; 25 ft Dn. Grad., 2 ft
PARAMETERS
Cadmium
Chroniium
SUver
Lead
Antimony
METHOD
6010
6010
6010
6010
6010
j7}^^JIe- fZ-hf «..-.LJ^C^=~
DATE: y/z-yc/^Y TIME://V<^ SAMPLER:^Z*'^
m
hno/^t- h^^^L. s-J-l uztiL
41
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A^ ^.r/^/.^/i>Kfi-K..<) J •*
TKokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: ^/i:'^f j^
srre: M-39 Surface Discharge _ ,
DESCRffTION: SWMU #425; J^'^f • ^J 'p/\f, Gr»d , Z
'(\to m-
PARAMETERS
Cfldnuutn
Chromium
SUver
Lead
Antimony
METHOD
6010
6010
6010
6010
6010
DATE: V^/Zf / f <^ TIME: )]./ 0 SAMPLER: P(///j O
jl
• 1 IW
-r?^.
<*
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^
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/AY-^
Thiokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#: &/^S ?^
srre: Combined Surface Discharges, M-8, M-9, M-10
M-52 and M-179-N
DESCRIPTION: SWMUs No. 268, 611, 269, 409, 472, 255
Pt of Discharge, Surface
PARAMETERS
Cd, Cr, Ag, Pb, Sb
Sulfate
pH
Mercury
METHOD
6010
300
9045
7470
DATE: /////?^ TIME://;/2? SAMPLER:P«7^<
H
J-Ui
I i
tr
ii
^-tfi
WMi •M
88
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Thiokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#: ^/<X3 ? P
SITE: Combined Surface Discharges, M-8, M-9, M-10
M-52 and M-179-N
DESCRIPTION: SWMUs No. 268, 611, 269, 409, 472, 255
Pt of Discharge, Surface
PARAMETERS
VolatUe Organics
METHOD
8240
DATC: y//^/9¥ TIME:/Ay ^ SAMPLER: f^/-^<^
'*:••;• jf^
J?.:*
«4^
iat£
_^ii
Thiokol Corporatioii RCRA FaciKty Investigation
WO#: 1B940 LWR#: ^/^ 3?^
STTE: Combined Surface Discharges, M-8, M-9, M-10
M-52 and M-179-N
DESCRIPTION: SWMUs No. 268, 611, 269, 409, 472, 255
Pt of Discharge, 2 ft
_&JUjt2l.$;a^_
PARAMETCRS
Cd, Cr, Ag, Pb, Sb
Sulfate
pH
Mercury
METHOD
6010
300
9045
7470
-^ATC: ^/f^lff TIME: //'' YS SAMPLER: (^^O
,^
fAK'-'X-
••Sf
/"l-Y X^fS eAo^a->•
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWT{#: ^/o2y^
SITC: Combined Surface Discharges, M-8, M-9, M-10
M-52 and M-179-N
DESCRIPTION: SWMUs No. 268, 611, 269, 409, 472, 255
Pt of Discharge, 2 ft
PARAMETERS
VolatUe Organics
METHOD
8240
5
DATC: Y/'f/f"/ TIME://;^J'^AMPLER: A/-f^
"i
'•§^
Jfc»
-•:•¥-
Mli^
• 89
/// 7:£^
TKokol Corporation RCRA FadUty Investigation
WO#:IB940 LwL: ^59^
srre: Combined Surface Discharges, M-8, M-9, M-10
M-52 and M-179-N
DESCRmiON: SWMUs No. 268, 611. 269, 409, 472,255
25 ft Dn. Grad., Surface
PARAMETFB.i;
Cd, Cr, Ag, Pb, Sb
Sulfate
pH
Mercury
METHOD
6010
300
9045
7470
DATC: ^/H/n TIME: W^^ SAMPLER:/^/^ ^
-S^/avx£:^ c^>^^ £M.I
^c*7u Cyv frw^i c^ >^t a/tTf
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TKokol Corporation RCRA FadUty Jn'^^"",
WO#: 1B940 LWR#: klC>3,f(^
srre- Combined Surface Discharges M-«, M-9, M-10
M-52, and M-179-N
DESCRffTION: SWMU Nos. 268, 611, 269, 409, 472, 255
25 Ft Dn. Grad., Surface
PARAMETCRS METHOD
^iS
-L_Jt
liili
VolatUe Organics
DATC:
8240
. Jff/f/iif TIME: /f^^ SAMPLER:^y<
K^US.^ dU,^
fl * C^ Thiokol Corporation RCRA FadUty Investimtion
'''--*-**- W0#: 1B940 LWR#: (^/&3f/i
SFTC: Combined Surface Discharges, M-8, M-9, M-10
M-52 and M-179-N
DESCRIPTION: SWMUs No. 268, 611, 269, 409, 472, 255
m
PARAMETERS
VolatUe Organics
METHOD
8240
'f
DATC: y////f^ T\m.Al',S^ SAMPLER:/^-^O
laStasaammmm '^smmm
V,.. *r^j.:-\--.s •{•':•.:''..•••'\<ii'^'-.'if..
90
^^ Qy^ a^rj^. ^
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Thiokol Corporation RCRA FaciUty Inv^tigation
W0#: 1B940 LWR#: b/^3f^
SITE: Combined Surface Discharges, M-8, M-9, M-10
M-52 and M-179-N
DESCRIPTION: SWMUs No. 268, 611, 269, 409, 472, 255
25 ft Dn. Grad., 2 ft
PARAMETCRS
Cd, Cr, Ag, Pb, Sb
Sulfate
pH
Mercury
METHOD
6010
300
9045
7470
y^ffUi^/-—
DATE: f/^/9Y TIME.:IO''09 SAMPLER: <V-J
c^S' Dyr. a^u^. ^^
TKokol Corporation RCRA FacUtty Investigation
W0#: 1B940 LWR#: ^/<J3?P
SITE: Combined Surface Discharges, M-8, M-9, M-10
M-52 and M-179-N
DESCRIPTION: SWMUs No. 268, 611, 269, 409, 472, 255
25 ft Dn. Grad., 2 ft
PARAMETCRS
VolatUe Organics
DATC: WffffY-TIME;
METHOD
8240
SAMPLER; A/-J'
.^A^OVJ
ft
.'•^32;--
-^
.-^K^^kt4-._^2/J|je^^«^j-t==L.
TKokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: G:/<iS'^/l
SITC: M-57 Surface Discharge
DESCRIPTION: SWMU #615; Pt of Discharge, Surface
M^Lkj^^SUlk-
-O/ 4.4.
PARAMETERS
Mercury
METHOD
7470
T-
liATE:^//y/9Y TIME://-/'^ SAMPLER: ^^/^"
W^^gl§§^WM!W^W^^''
.:-«tii.ru'-~--i_ <*
•
/430 Th- of liise^t^j Z'
91
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/<^3P^
SITE: M-57 Surface Discharge
DESCRIPTION: SWMU #615; Pt of Discharge, 2 ft
PARAMETERS
Mercury
METHOD
7470
DATC:>y^//^^ TIME: J^30 SAMPLER: AV~^
/y/a!^-/ :r///- ^ Ohu
m
1
/^^r 2o' 7>A/ (S72A-h Sorfk^.
a
TKokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#: B/OS?^
SITE: M-57 Surface Discharge 3^
DESCRIPTION: SWMU #615;.M"ft Dn. Grad., Surface
PARAMETERS
Mercury
METHOD
7470
SAWb .* (STIAVSL.
%*.
P
.DATE : ^/y^/PY TIME: ^^^^ SAMPLER^^
/y/ > ^y. TKokol Corporation RCRA FaciUty Investigation
/T^-P(^ W0#: 1B940 VmM:S/oSf ^
SITE: M-57 Surface Discharge 2tf ^
DESCRIPTION: SWMU #615t3Sin5"fi.T5rad., 2 ft
PARAMETERS
Mercury
METHOD
7470
m
/{/g^:<ss5tfy A Co/lc^f- ^j- 3o' €=/uc 7^ /? ru/C/^t-^
DATE :f/f•//?¥• TIME./Y'. i-O SAMPLERA/-^^
#:
li
•it'r^
92
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-761^
)r\g>/y-/- S^yA.-l^
TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/e,3f>(^
SITC: M-55-W Surface Discharge
DESCRIPTION: SWMU #621; Pt of Discharge, Surface
^-
vfr-fc J_
PARAMETCRS
Cadniium
Zinc
Sulfate
pH
METHOD
6010
6010
300
9045
DATE:^^^/^^ TIMEr/r.V-P SAMPLER:/^^/^ ^^
v.. «?-
-^;.
vie
ls.:/o
6J. MZ-WL^?/ x«»^ *^f tf-e-^
TKokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: ^^/VS^/i
SITC: M-55-W Surface Discharge
DESCRIPTION: SWMU #621; Pt of Discharge, Surface
PARAMETERS
VolatUe Organics
Bis(2-EUiyUiexyl) phthalate
^-
METHOD
8240
8270
DATC :Y/y^/fi •nME:/SVo SAMPLER:/^^"^
m
-Pc,:.^ ^SP.iJ^.^^.^ ^ '
TKokol Corporation RCRA FacUity Investigation
W0#; 1B940 VmM: ^/oSf^
srre: M-55-W Surface Discharge
DESCRIPTION: SWMU #621; Pt of Discharge, 2 ft
—Cied^k_i^jrOMf:ti-5'lik-
PARAMETCRS
Cadmium
Zinc
Sulfate
pH
METHOD
6010
6010
300
9045
HATE .y//f/9Y TIME:/^'2.6 SAMPLER:/^^/-^ '
m^m^&WMf-''^
m
•P«rui i^V,,:^. »L'
Thiokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#: C/o^g ,
SITC: M-55-W Surface Discharge
DESCRIPTION: SWMU #621; Pt of Discharge, 2 ft
PARAMETERS
VolatUe Organics
Bis(2-EthyUiexyI) phthalate
METHOD
8240
8270
JaATEjK//^/ ? V TIMF.: /-^ 2 O
j^^ P/y^. ^trAt^,. .S;.v-v^
Thiokol Corporation RCRA FadUty Investigation
WO#: 1B940 L"WR#: S-^a^f./
1^
/ 5"' 30 STTC: M-55-W Surface Discharge
* DESCRIPTION: SWMU #621; 25 ft Dn. Grad., Surface
PARAMETCRS
Cadmium
Zhic
Sulfate
pH
METHOD
6010
6010
300
9045
-DATF /9^4vr9'/ -rvm.J^^o ^KMvxmSc^h
J^^ Py^. JAYAA. S.C4,yr^,
I^^CL
TKokol Corporation RCRA FacUity Investigation
W0#: IB940 ^"^^^-^/oSQL
SnE: M-55-W Surface Discharge ^
DESCRIPTION: SWMU #621; 25 ft Dn. Grad., Surface
PARAMETERS
VolatUe Organics
Bis(2-Eti[iyUiexyi) phthalate
METHOD
8240
8270
DATC: ^//y-/?^ TIME: fS3c) SAMPLER;
#
'•0 94
:Pu^, ^^' D/r JA^JIA. ^S.^/^
-•» "f, I f_
/5^/3^ TKokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#: l^/O^f ^
SITC: M-55-W Surface Discharge
DESCRIPTION: SWMU #621; Dup., •^aXvLlycJlJ Ciy^^yuJJ
PARAMETCRS
Cadmium
Zinc
Sulfate
pH
METHOD
6010
6010
300
9045
DATC: V//y/9y- TIME:/X'2-o SAMPLER: F'^/-S (
'••IT-
^^ ^J>yr J^^AX. > /
•il
«^
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r
1^
i5_^^_
TKokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#-.^/£>3 ^^
SITE: M-55-W Surface Discbarge
DESCRIPTION: SWMU #621; 25 ft Dn. Grad., 2 ft
PARAMETCRS
VolatUe Organics
Bis(2-EthyUiexyl) phtiialate
METHOD
8240
8270
DATC:y/'//9V •nME:/S-YJ SAMPLER:/^'/!/<
^5"^ Drr J^yJ^A. > ^
TTtoJto/ Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#: B/O^Q^
SITC: M-55-W Surface Discbarge
DESCRIPTION: SWMU #621; 25 ft Dn. Grad., 2 ft
PARAMETERS
Cadinium
Zinc
Sulfate
pH
METHOD
6010
6010
300
9045
DATC: y//^/9Y TIME:/5.Y^ SAMPLER: ^/j'
1^
r
a 95
*SAMFLg^ '12g.-^\<lqcr<i.UA ii\ 'S<acujn:i<j A rxag. ^-/^
J
fT--^"/^ g" /^ ^€^ 'TA^e^n/ To C/hBCJZA ^72-
^/; /5- y^/*;g- f^ r
^^^ i[
•^ .•' f»' '•
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:^J':
^
96
S--Z3'94
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t'Aff SMind "SuKJiLt^ l)j^cAaf^A . /^a^/2-^/ia/tc<^ <s-xcati/Q,
•ih fiUAi^jburJc/l fi'o/n Mi M.
• • < .••.
••0i^
•W Mci^t J^rK anci r&rl C/ay an<J 37/7^3 ,
Aishric ^r^n^At^l 'T^^S^ 3a/l^/c was da/la^^
jMcpanc/Anxf- flf ^ ^>^/ >SiiA^/f/?a
TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#:
SITE: M-9
DESCRIPTION: SWMU 652; Strand Burner Exhaust Discharge
PARAMETCRS
Volatile Organics
DATC: 5'-ZS'f'f
METHOD
8240
TIME: /2/J' SAMPLER: A^uJ
TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#:
SITC: M-9
DESCRIPTION: SWMU 652; Strand Bumer Exhaust Discharge
PARAMETERS
Cd. Cr, Pb. Ag
Mercuiy
HMX
Nitroglycerin
METHOD
6010
7470
HPLC
HPLC
DATC: ^•'Z3-9^ TIME: /^^ SA3VIPLER: AP'->
m
^^v
'•y\^
% t.
\^{^ SACVC (Jugj/^O-W fr
^tye %r( fHAj^'i,\<. ^OittYl^ (^t>l\^ii^iyiij U.iJi>a.vflas •;;M<xt( tJi^^
ftlU -U)4i> a^v^t<x ^n HlU,\C I'lA CA[O^-
i» T Ju*J€^ /^9f
105
/S3o OA/ syr^ Ar JU'4-Q S'UJ/UU-^ ^4-2^ — -f-EA^K CJAcJ££JS.
farHi, CycoJ^ , ^/l^AL-h^^fS. 'i<?Af Jbr<tfgtr /rn/u. "SouH^ T' 76
124^ TKokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: SI04-ZL
SFTC: M-40 Surface Discharge
DESCRIPTION: SWMU #642; Pt of Discharge, Surface
PARAMETCRS
Nickd
pH
METHOD
6010
9045
Sur-fa c^
2//^/ C/QH UJ//A [J^
DATE: Tk/yA/f^f TIME:/.7.#i SAMPLER: 'J-U'
^
J36^
IT
TKokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: €'lO'(>7.^
SITE: M-40 Surface Discharge
DESCRIPTION: SWMU #642; Pt of Discharge, 2 ft
PARAMETERS
Nickd
pH
METHOD
6010
9045
DATC: 'TyJOA/^'i^^ TIME: /3^V SAMPLER: >2-t^
lAJ\f\ TKokol Corporation RCRA FadUty Investigation
'^^^ WO#: 1B940 LWR*: ^^OfiZC
SITE: M-40 Surface Discharge
DESCRIPTION: SWMU #642; 25 ft Dn. Grad., Surface
PARAMETERS
Nickel
pH
METHOD
6010
9045
DATC: 7>JO^e9f TIME: /^OO SAMPLER: x^i/-/
G^I^V€l.^
•
XTT
106
/^/<~ TTuoito/ Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: /fVtJ^fZ^
SITE: M-40 Surface Discharge
DESCRIPTION: SWMU #642; 25 ft Dn. Grad., 2 ft
PARAMETCRS
Nickel
pH
METHOD
6010
9045
<lf/hJ .g Oy
^-ave.J
DATC: yJOASe^ 9^. TIME: /^/^^ SAMPLER: ^^'-"-J
JuML^
S JcJ^f^ <?f
^^ f:9-o ^/(j Z^^^ // ^ >o /?- ^ fy? - a-ip tr/eA^ ^/?^
/)JUZ> /Q/}^^ uJ/^/^er. A/^^^^^ r / s ^/» j?/^/C
^J'C^A^r /^/-^fz^e. J /rmP- 4^7^-T "r-^^r
^••54
TKokol Corporation RCRA FaciUty Investigation
W0#: 1B940 U
SFTC: M-205 Surface Discharge
ition^
W0#: 1B940 LWR#: ^/^^^ ^
srre: M-205 Surface Discharge
DESCRIPTION: SWMU #286; Pt of Discharge, Surface
PARAMETCRS METHOD
'/?/ty/) GA (6 fii
Lead
Cyanide
Sulfate
pH
6010
9010
300
9045
DATC: OzJwOe ^y TIME: "^ > ^^ SAMPLER ^^^
M
^:c^6
TKokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#:
SFTC: M-205 Surface Discharge
DESCRIPTION: SWMU #286; Pt of Discharge, 2 ft /7}^;,/ CJA^
PARAMETERS
Lead
Cyanide
SuUate
pH
METHOD
6010
9010
300
9045
DATC: ^iiJuA.^<S 9/^ TIME: f^/ j^ SAMPLER: /-^'^
fvr.
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: £'^ a e/3-(,
srre: M-20S Surface Discharge ^^^ ^yr^ ^ £); ^^
DESCRIPTION: SWMU #286;
PARAMETERS
Lead
Cyanide
Sulfate
pH
DATC:
METHOD
6010
9010
300
9045
/ ^*^e f/riME: f'-V^ SAMPLER:
107
_ ft'ik
' .'IS
J ! •
4|Zi:
//)\iR_
TKokol Corporation RCRA FaciUty Inve^ation^
W0#: 1B940 LWR#: C^^^<^r^>
SITC: M-20S Surface Discharge
DESCRIPTION: SWMU #286; 25 ft Dn. Grad., Surface
PARAMETCRS METHOD
Lead
Cyanide
Sulfate
pH
DATC: 6 (J-t^ ^€. ff^TlME:
6010
9010
300
9045
SAMPLER:
TKokol Corporation RCRA FaciUty Investigation ,
W0#: 1B940 LWR#: ^/O V-*- C
SITC: M-205 Surface Discharge
DESCRIFTIGN: SWMU #286; 25 ft Dn. Grad., 2 ft
PARAMETCRS
Lead
Cyanide
Sulfate
pH
METHOD
6010
9010
300
9045
^;// d CIAT'
DATC; 0 C7l^f*^<f ^</TIME: /^'-/^^ SAMPLER: ALO>
1 \.i
r^jN / C/A^ il
Til
>
Samp/f^ rIfiJ(t>tt€.J ¥o A<-6'S /a^oraLjt (^ /CS^O
%
d-
VA>^^
108
/^^ locAr^^ffj T^jb: //c^^ yJjp^h, J^i '^'A^'J_^_ /U-^
/Je^j^/irr ^'y^'ff^n'r^^ /Al/^,yy^ MJ/9. '^m
ik -
i-f'T-
r.
A/V^
TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/S)j(lS 3
SITE: T-21D Surface Discharge
DESCRIPTION: SWMU #559; Pt. of Discharge, Surface
PARAMETCRS
VolatUe Organics
METHOD
8240
DATE : / /^-^^ TIME: //V 0 SAMPLER:
v^^
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: ^?d)'^S.3 .
SITE: T-21D Surface Discbarge . C
DESCRIPTION: SWMU #559; Dup., Pt. of Discharge, u> U/Cf/JC/^
PARAMETCRS METHOD
VolatUe Organics 8240
DATC; •1/5^-^^ TIME: ://^ SAMPLER: /^-i-<^
#-
Y
'^X
••«.•,
??^
Hir
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/O^ Z 3
SITC: T-21D Surface Discharge
DESCRIPTION: SWMU #559; Pt. of Discharge, 2 ft.
PARAMETERS
VolatUe Organics
METHOD
8240
DATC :/-/^-^^ TIME: /^ X^ SAMPLER: '<l^
il,!i)^
'Yv
__^ . }••
t?*-D
r'^r
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: S'ya'I^SB.
SITC: T-6A Surface Discharge ^5>U</^/^CC.
DESCRIPTION: SWMU #287; Pt of Discharge, Surface
PARAMETCRS
Selenium
pH
METHOD
6010
9045
^
^
'^ P
DATC; /-/^ ^^ TlME-jifT^ SAMPLER:
I m
tu
jkL
^»
/f^>
_>u(^
'Il35i
l#
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/e^ /3 3
SITC: T-6A Surface Discharge
DESCRIPTION: SWMU #287; Pt of Discharge, 2 ft
PARAMETERS
Sdenium
pH
METHOD
6010
9045
^jh
—6-^
r^jt-CL
.^/^o^'
4-
f' r^^
DATC; i/i-^^ /i :•?>
^
TIME: SAMPLER:
TKokol Corporation RCRA Facility Investigatiqii^
WO#: 1B940 LWR#: ^'<^^ ^
Xy/ /">-->a ^ C SITC: T-6A Surface Discharge jj^
DESCRIPTION: SWMU #287;'5?rft Dn. Grad., Surface
PARAMETCRS
Sdenium
pH
METHOD
6010
Ylf -^
-^^^^
9045
DATCi ;^'/^- f/ TIMEr^^^^^^^AMPLER: /^»^^
IS
I m
I'V-
,.-..r.
.^ *t
*,V '
.'^ii
110
Thiokol Corporation RCRA FadUty Inv^tigaUon,
W0#: 1B940 LWR#: iS^^ -/S-S.
SITC: T.6A Surface Discharge ^^
DESCRIPTION: SWMU #287tJ?'ft Dn. Grad.,XfL'
PARAMETCRS METHOD
Selenium
pH
6010
9045
DATC: \,-)^•1^ TIME
If-4^ 0^
///
SAMPLER:
4um^
% .•fJL*
^
-Ar-^^j&ir Uu. ^ f^ad.
i
-c.
111
.^^fUirx^ jSvRFAoe.
Thiokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#: £/<5-f 5^
SITE: Old Drum Storage Area E of M-203
DESCRIPTION: SWMU #203; Grid # 7 , Surface
PARAMETERS
VolatUe Organics
METHOD
8240
f
-U-.
-^4
DATC: "20 xiu n 9 4- TIME: fO'/O fuJ
SAMPLER: /I^E, VBR 1/ X?^ /-^^-
Thiokol Corporation RCRA FacUtty Investigation
W0#: 1B940 LWR#: £/^45<^
SITC: Old Drum Storage Area E of M-203
DESCRIPTION: SWMU #203; Grid # / . Surface
_'itM
IT '
I' '
PARAMETCRS METHOD
i\ Cadmium
Chromium
SUver
Lead
BerylUum
Mercury ^ ^ , _ -
DATC: Z^Piy'^<=»4'
6010
6010
6010
6010
6010
7470
TIME:;^'''0 SAMPLER: Al^
in.
•g:sajb> ^ 7 z/_:De:&!riL
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £.^^4' 'S^
SITE: Old Drum Storage Area E of M-203
DESCRIPTION: SWMU #203; Grid # ^, 2 ft.
PARAMETERS
Volatile Organics
METHOD
8240
r^\ ril
'itii I
d»
F-'O
-DATE: %0 JuN <if TT^^E^ lO'.ZO SAMPLER: "^^
TKokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#: ^/<i>'f $^
SITC: Old Drum Storage Area E of M-203
DESCRIPTION: SWMU #203; Grid # 7 .2 ft.
PARAMETCRS
Cadmium
Chromium
SUver
Lead
BerylUum
"'"'"^^^ Ju/1
METHOD
6010
6010
6010
6010
6010
7470 -^
IMPT-FTti "^^ ..o
-l--...L.,.^;j,.;^.,;./.,
rA 4.'
• ""A • •
112
_a^-ii:? ^'^^ ^_^^^^<s
7Wo*o/ Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#: £.Jff4 3 <f>
SITC: Old Drum Storage Area E of M-203
DESCRIPTION: SWMU #203; Grid #_Z^ Surface
PARAMETERS METHOD
VolatUe Organics 8240
n.'JV.ZoJuA^^ TIME^1011_^,,,MPI,F,R: ^
Thiokol Corporation RCRA FadUty Investigation
WO#: 1B940 LWR#: ^104'H>
SITC: Old Drum Storage Area E of M-203
DESCRIPTION: SWMU #203; Grid #3*2. , Surface
PARAMETCRS
Cadmium
Chromium
Silver
Lead
BeryUium
METHOD
6010
6010
6010
6010
6010
Mercury . 7470 C \jl
DATC: %0 Jun 94- TIME: )b'-'^^ SAMPLER: ^*l5
^RfD ^3^ llp" -Oei-P^H
TKokol Corporation RCRA FaciUty Investigation
WO#: 1B940 LWR#: g;/o4"3^
SFTC: Old Drum Storage Area E of M-203
DESCRIPTION: SWMU #203; Grid # 3 Z^a^ \ ^T
PARAMETERS
VolatUe Organics
METHOD
8240
(oro.\)J i S,'U
B t^ g -fO ^OCJC^
J
DATC: 2-0 Jt/A '\^ TIME:^^'^Q SAMPLER: ^A
Thiokol Corporation RCRA FacUity Invwtigatwn
W0#: 1B940 LWR#: B/O't' > <<-
srre: Old Drum Storage Area E of M-203
DESCRIPTION: SWMU #203; Grid #_i±r:.*'*'^ • ' '
PARAMETCRS
Cadmium
Chromium
SUver
Lead
BeryUium
METHOD
6010
6010
6010
6010
6010
7470
DATCT'Z^ it>/1 14- TIME: jO: Ao SAMPLER; : n*3
--I
mMMmMmBMsmj^
DATC: 2^ ^'•"^ ^^ TIME: ^'^ ' ^^ SAMPLER: I^A^
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#. ^/^^7 V*
SITC: Old Drum Storage Area E of M-203
DESCRIPTION: SWMU #203; Grid # ^ T, Surface
S/IT
PARAMETCRS
Cadinium
Chromium
SUver
Lead
BeryUium
METHOD
6010
6010
6010
6010
6010
Mercury i - „,• 7470 p Uj
DATC: 2*^ ^Ot\ IT TIME: /D'?C> SAMPLER: ^-^
6RII:> ^5"f- / ' I><lpTH^
TKokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#: £/<D fS <^
srre: Old Drum Storage Area E of M-203
DESCRIPTION: SWMU #203; Grid #.^4'. a^tr I f- "f
PARAMETCRS METHOD
VolatUe Organics 8240
DATC: "2.0 \or\ <^4 TIME: M-Pg" SAMPLER: ^t*^
Thiokol Corporation RCRA FadUty Investigatiop
WO#: 1B940 LWR#: £/0 T^Q'
SITC: Old Drum Storage Area E of M-203
DESCRIPTION: SWMU #203; Dup., Grid #5^^ . / ^T
OeFT^ UHf/rtsrD Our..
7Z> ^oc^ejs.
PARAMETERS
Volatile Organics
METHOD
8240
7^ f^on^S
DATC: lo ioJfte'lf TIME: (1 '.O^ SAMPLER: Me>
:^[
1
'^^h^ii'M:m^^^^'^i^^M
^ vr
114
cji?iri T^s-^ / ^T: (ie.^-r-3
TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^ / D ^ 3 Q>
STTE: Old Drum Storage Area E of M-203
DESCRIPTION: SWMU #203; Grid # S4. M*. / f^
PARAMETCRS
Cadmium
Chromium
SUver
Lead
BeryUium
Mercury
DATC: Z-C? JvO If- TIME: )I'• oT SAMPLER: '^S
METHOD
6010
6010
6010
6010
6010
7470
'J
••* •••'
^f^-'^kL
"-•^KH-
V'if:
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: £/C»f'3 C»
SFTC: Old Drum Storage Area E of M-203
DESCRIPTION: SWMU #203; Dup., Grid #5T, _J__rl
PARAMETCRS
Cadinium
Chromiuni
SUver
Lead
BeryUium
Mercury .
DATC: "^^^ ax^n n 4-
METHOD
6010
6010
6010
6010
6010
_pA^
TIME; SAMPLER: %>
RiMSe^-^^ACK ^/p -^^ / f^
TKokol Corporation RCRA FacUity InvesUgation
W0#: 1B940 LWR#: B^'lP^ 3 Q>
SFTC: Old Drum Storage Area E of M-203 ^. \ jti-r
DESCRIPTION: SWMU #203; Rmse Blank, Grid #_^Tj _L_JL_T
PARAMETCRS
VolatUe Organics
METHOD
8240
\
DATC: 2^'^.\^'^ 14- TIME: H'^'^S' SAMPLER: ^M-^
I'
TKokol Corporation RCRA FacUity Investigation
WO#:1B940 Vfm. t.lO^-^(p
SFTC: Old Drum Storage Area E of M-203
DESCRIPTION: SWMU #203; RUise Blank, Grid #J23L
t>SPn'/ U^/TlS£i
_L_F:T _ja fc^g Tto I^OKLK^
PARAMETERS
Cadmium
Chromium
SUver
Lead
BeryUium
METHOD
6010
6010
6010
6010
6010
7470.
^l^-i^ ^^'^ 1 ^ TIME: \^'^< SAMPLER F;^
mtmm
?^^lf^:??»^S^V^v^:-;;..-
6rp.fi::> 4LO s^^A^pfnts
TKokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: ^/0'f'2,(^
STTE: Old Drum Storage Area E of M-203
DESCRIPTION: SWMU #203; Grid #^0 , Surface
PARAMETERS
VolatUe Organics
METHOD
8240
/
DATC: •Zo io>n %9' TIME: UifO SAMPLER: '^•^
^
^
TKokol Corporation RCRA FacUity InvK^igation
W0#: 1B940 LWR#: E/04%Cm
SITE: Old Drum Storage Area E of M-203
DESCRIPTION: SWMU #203; Grid # ^O, Surface
pJli Vaco lj y0OOj>£^AJ[
-^ur
PARAMETERS
Cadmium
Chromium
SUver
Lead
BeryUium
METHOD
6010
6010
6010
6010
6010
Mercury - f - j , 7470 poU
DATC: 2^ Jt'l Tr' TIME: //'./O SAMPLER: /ffJI
i5
II:
•1 .(
m
GifLio •1^4-0 /.<r yfc-r nsrPTff
;ation TKokol Corporation RCRA FacUity Inve
WO#: 1B940 LWR#: E'^OA-'b^
SFTC: Old Drum Storage Area E of M-203 ^
DESCRIPTION: SWMU #203; Grid # 4 O.-tH. ' • ^ fT
PARAMETERS
VolatUe Organics
METHOD
8240
DATC:'2-Oic/^ *?^ TIME: //'ZS" SAMPLER: >^^
Thiokol Corporation RCRA FadUty Inve
tiePTrt
Dv^€^ T
Llrvii-^&b n'e
O pvOC-fcIc- ill!
•if
"1 1
^
W0#: 1B940 LWR#: £,10*
SFTC: Old Drum Storage Area E of M-203
DESCRIPTION: SWMU #203; Grid »4-e> ,a-flT / .JT ^^ ^ijo To Ko^AO
PARAMETCRS
C&dnuiiED
1 .111*011111 IfH
SUver
Lead
BeryUium
Mercury ,
n n4-TIME:
METHOD
6010
6010
6010
6010
6010
ll.'Z^ SAMPLER: f^3
P^rrW u»\Arrgo
'..-3'!
•'fi:—
'iSi--^
116
^f JuAjt /99^
Pe>3o ON 3ir£: /^r li-ilj- To ^^>up>i^
•/-(> a/^ /Aja^i^tryi LU^/I J/Jtj ^uJU/U//I.S Joi/1
'lp fJo/(a<L, i^JlJ fr'iif i^ofJi": ^pa<^ E>eJ^ o^cJ
ri^ r
h
\*i
L
'•." ">_
7^/ /^/j>^^/?-y^ ^a^jeAfi./1-k //tk> UJ^/^J 7^ cy^Jg/
A':
..»rj.
'•H m
i
•:^.
.••i ^^
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £/^S0
SITE: M-114 Surface Discharge
DESCRIPTION: SWMU #426; Pt of Discharge, Surface
PARAMETCRS
Cadnuum
Chromium
SUver
Lead
METHOD
6010
6010
6010
6010
^/mAf^ ardor
DATC: Zl JuA/e/99>^^^^^-^^^^ SAMPLER:JC/FCJ
oe^t) Thiokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#; £/MZ^
SFTC: M-114 Surface Discharge
DESCRIPTION: SWMU #426; Pt of Discharge, 2 ft
PARAMETERS
Cadmium
Chromium
SUver
Lead
METHOD
6010
6010
6010
6010
DATC: Z/JuMe94- TIMEJOS*^^ SAMPLER: JV^^^'^
>r 'm-^/^\ u^ J91^
rjl|, ^/-_?^ ^/f s:.:L ^y^ >h;x^7
%
^
•-•i. "••>..'
I 1.11' III." I. ' sami^Bmmitmmmmm
h-,* .'r..-- ... ,. .., .
»
117
/^;^5 .'^y/^r,^ .S:4J^^J? .
TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £/0^'Z'Z>
SITE: M-227 Hydrofluoric Add Treatment Untt
DESCRIPTION: SWMU #192; Surface f-J
PARAMETERS METHOD
^ Cadmium
Chromium
Lead
pH
6010
6010
6010
9045
\iATE:<:^/,^//9<A TlME:/a .'SS SAMPLERr J</AUy
y/2^
y'^'fS'
^r
eP- S^yupl./}
TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 ' * LWR#: ^/0433
SITE: M-227 Hydrofluoric Add Treatment Umt
DESCRIPTION: SWMU #192; 2 ft.
PARAMETERS
Cadinium
Chromium
Lead
pH
METHOD
6010
6010
6010
9045
h\A\L
JCJ^
UlXL.
T
\ t-o CO trt
DATE: <^/Ji//?V TIME/<g-Y-S SAMPLER: ^'^/-'^
g^ I>U.p),^ct -JHkv^)
/^{^^ TKokol Corporation RCRA Facility Investigation
' ' W0#: 1B940 LWR#: Ej04'it>
SITE: M-227 Hydrofluoric Add Treatment Untt
DESCRIPTION: SWMU #192; Dup.; ^_ ft. ik^ /U >vi a V4 u/"** -a<
PARAMETERS METHOD
Cadmium
Chromium
Lead
pH
6010
6010
6010
9045
-DATE: (^/<^ /9V TIME? ya :s^ SAMPLER; /Zu/JC
m
'il.
118
////^
S^'S4y^.
TKokol Corporation RCRA FaciUty InvestigaUon
W0#: 1B940 LWR#: E/0^3V
SITE: M-227 Hydrofluoric Add Treatment Unit
DESCRIPTION: SWMU #192; 5 ft. )>?(5/5/ crK4a/ C^-y-
PARAMETCRS
Cfldmiuni
Chromiuni
Lead
pH
METHOD
6010
6010
6010
9045
DATC: <^/^/9'i TIME: //:/cf SAMPf.F.11; F^VJc
-^*i''
1'
'. .••»•'L_'-
/•^'^
r,tr
' Ait'
I
'it
^iHSiTr ^/a,wjc^
///e;^^ TKokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#: •B./O^S^
SFre: M-227 Hydrofluoric Add Treatment Unit
DESCRIPTION: SWMU #192; Rmse Blank; ^ ft.
PARAMETERS
Cadmium
Chromium
Lead
pH
METHOD
6010
6010
6010
9045
DATC , <^/2//Fy T^, //!^^ SAMPLER: f^A ^
iff-
ir
iirr
,£7..-/, O C-t.
/r.3c Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: S/0433
SFre:
DESCRIPTION: Rant HI; Background, Surface
PARAMETCRS METHOD
VolatUe Organics 8240
pH 9045
Cd, Cr, Ag, Pb, Be, Cu, Sb, Se, As 6010
Mercury 7470
HMX HPLC
Nttroglycerin HPLC
Cyanide 9010
Sulfate 300 J^/
DATE; -ZUVNeff TIME: /f20 SAMPLEVi. //^C^
Z:^f}Ljsy£ic/V.^^fjJ=-
m
%
,•>:.;.. .<^•;.•• f .--^b^f ^v-'^j-V-i^,*,:-:.., *».\-:;«.\;^*5 ^T;
••;• "*• -» .-• *•
ft^wrf^'twjt
m 7/L
-c2 S^yrupjji.
119
TKokol Corporation RCRA FadUty Investigation
W0#; 1B940 LWR#: £/0^3t>
SFTC:
DESCRDTION: Plant m; Background, 2 ft
PARAMRTRW.S METHOD
VolatUe Organics "^^
P" 9045 Cd, Cr, Ag, Pb, Be, Cu, Sb, Se, As 6010
Mercury ^^^j,
HMX gpLc
Nitroglycerin HPLC
Cyanide p^^
Sulfate jgg
DATC:Z/jCA/g-fir TIM:, //^^-^ SAMPLER;
C'l<ff.f- Aye LUU ^llj^
^ VUiup),Cc*^'^.^-^^*^^°^tjl^=^
v^ •f^l^
J J ' :? C^ Thiokol Corporation RCRA FacUity Investigation
-^V-^-iO— W0#; 1B940 LWR#; ^o43B
IT
SFre
DESCRIPTION: Plant m; Dup., Background, 2 ft.
PARAMETCRS METHOD
VolatUe Organics 8240
PH 9045
Cd, Cr, Ag, Pb, Be, Cu, Sb, Se, As 6010
Mercury 747Q
HMX HPLC
Nttroglycerin HPLC
Cyanide pg^O
Sulfate 300
DATE; -^iJUU^-f^ TIME: //2^ SAMPLER;
^>^A >ift^>t .SV JJL
Sc
u
^' SA^I^
// >^^^ TKokol Corporation RCRA FadUty Investigation
''^^^^— WO#:1B940 LWR#: £/e>^3&
SFTC:
DESCRIPTION: Plant III; Background, S ft.
PARAMETCRS METHOD
Volatile Organics 8240
pH 9WS
Cd, Cr, Ag, Pb, Be, Cu, Sb, Se, As 6010
Mercury 7470
HMX HPLC
Nttroglycerin HPLC
Cyanide 'OIO
Sulfate 300
A/AL .^jy-AtU. S^>id.
DATC: Z/^/f-VCf^ TIME: //4 "!> SAMPLER: ^^.J
-S^.UJJ
^^^Wa^^
>%^«eS»-.».V!ajW»;r^-.'vi<j,{
120
Moo on 5/Vc at- /^- 9 gu^-g O *- 6SI 7a ^am/sU
DisePiaro/' i° ^ •surfix.v 'X>Aife Goomi
%
•M-
^^
''^T>
*
•\;l|l
7*'
h, •v^;
»
!'••
*/^qhx^
^to TKokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#: £7/^5 f
srre: M-9-NE Surface Discharge
DESCRIPTION: SWMU #651; Pt of Discharge, Surface
PARAMETCRS
Cadmium
Chromium
SUver
Lead
Mercury
METHOD
6010
6010
6010
6010
7470
Mkt Grc
Si Ad aAS (. Ag. ^Ad G/Tot^yji
Vot^s, nd 't^f^f'-m
DATC: ZlJO^e^<^ TIME: <^^Z^3 SAMPLER: ^POJ_
Thiokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#: S/043.*7
SITE: M-9-NE Surface Discharge
DESCRIPTION: SWMU #651; Pt of Discharge, Surface
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC: 23 JoAJfc ^^ TIME: ^^Z.3 SAMPLER: VP^
i^r.'h-
mH-Thiokol Corporation RCRA FacUity Invest^ation
W0#: 1B940 LWR#: tzfO^^l
SITE: M-9-NE Surface Discharge
DESCRIPTION: SWMU #651; Pt of Discharge, 2 ft
PARAMETCRS
Cadmium
Chromium
SUver
Lead
Mercury
METHOD
6010
6010
6010
6010
7470
"-^^—
DATC: Uz^k^-TIME; 092^ SAMPLER: ^B RJ
'.f-
Wl-
"r-r*
•
j2Si 7 7-^- -
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#; £/042*/
SITE: M-9-NE Surface Discharge
DESCRIPTION: SWMU #651; Pt of Discharge, 2 ft
PARAMETERS METHOD
121
i
VolatUe Organics 8240 4
DATE : 6/2 ^Af TIME: 6?.?-^ SAMPLER: /f«^
/) f'^n TKokol Corporation RCRA FacUity Investigation
'^ l-^l W0#; 1B940 LWR#: £/043J
SITE: M-9-NE Surface Discharge
DESCRIPTION: SWMU #651; 25 ft Dn. Grad., Surface
Cr^- ^ LiQht ^rc^ roiv/t
PARAMETCRS METHOD
#
Cadmium
Chromium
SUver
Lead
Mercury
DATC:^/^3/4<^
6010
6010
6010
6010
7470
TIME; ^737 P' SAMPLER: %t^
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/C)f2j
SFTC: M-9-NE Surface Discharge
DESCRIPTION: SWMU #651; 25 ft Dn. Grad., Surface
!; i'.
if'
PARAMETCRS METHOD
VolatUe Organics 8240
Z>9^
DATC: ^/l.Z/'^i' TIME: ^J? SAMPLER: /F^
^^
•:
o!2!' ^^^ LWR#: ,,^Xv£-?9
srre: M-9-NE Surface Discharge '"^'^r-*/
DESCRIPTION: SWMU #651; 25 ft Dn. Grad, 2 ft
PARAMETER.S
Cadmium
Chromium
SUver
Lead
Mercury
DATC:
METHOD
6010
6010
6010
6010
7470
TWSE:6?'^ SAMPLER: VFHJ)
Mdl^^ Bjnsam
LM •m.
mi
lii]
m
\m
m
.>H
122
OW-^*"'*;^"«'"'«CRA'^'"^iUty Investigation
SITC: M-9-NE Surface Discharge ^0^3^
DESCRffnON: SWMU #651; 25 ft
PARAMRTKPg
VolatUe Organics
Dn. Grad, 2 ft
METHOD
8240
"^r^'i/zS/^ •r^,c,9/fi s.^^.%.
/ / •
TKokol Corporation RCRA FadUty Investigation ^
W0#: 1B940 LWR#: ^/OT^l
srre: M-9-NE Surface Discharge ^^ / ^ GP^D
DESCRIPTION: SWMU #651; 1)0:^ c:> l^ff^'*^'-'
-L-fh.
PARAMETERS
Cadmium
Chromium
SUver
Lead
Mercury
METHOD
6010
6010
6010
6010
7470
- DATC: (pfzSM^ TIME: 6^4^ SAMPLER: /fO^_
77u«to/Corpon/ion RCRA FadUty Inv^igatton
WO#;1B940 LWR#:^/0f3^
SFTC: M-9-NE Surface Discharge -J-^ ' Tihi G'BAb T^T-h
DESCRDTION: SWMU #651; ^^V ^-^ UN KJ>r^»
PARAMETCRS METHOD
VolatUe Organics 8240
DATC; 6A-2/^f TIME: 6l4^ SAMPLER: ^Yf^
m-
mo •pg/x/tre./ /d M-i3 iMI^ffZ^Tol^
LVdtZ- el04^f •B-
.ximi^^^^dl
f:—--
l,tvJ?Ti« ^l^5fp^^?P^^^(5?s,Hf-y^i:**;*->S*W i^?^*^^><^ <f*i^ii-Si:^'??;*;''V. ''i?*'"^-^/^.^•':.:"'-' •: •«=• '^^ »
^^^^_
IT
Clif^.r ^hi^ :^/g^/^ A/A^I ^f^ z^.^ £> Ui
TAioto/ Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#: je-/Q(^0 /
SFTC: West of M-381
DESCRIPTION: Strategic RFI Background; Surface
PARAMETERS
VolatUe Organics
Semi-VolatUes
METHOD
8240
8270
DATC: rja^^i^ TlME:a^<^7 SAMPLER: P^/^tcl
:m^^t^^cLeh .^
TUoib;/ Corporation R.CRA FadUty Investigation
W0#: 1B940 LWR#:
SFFEtWial of M-381
DESCRIPTION: Strategic RH Background; Surface
PARAMETERS
Metals
Mercury
Cyanide
HMX
Nitroglycerin
pH
SuU^ate
METHOD
6010
7470
9010
HPLC
HPLC
9045
9036W)38 .:.u.i»« ^ . . ^ 9036«»038 I ^, ,
DATC: /U^l<^ rf TIME: Cffc>^ SAMPLER: *^//=tXy>
Pia n *) TKokol Corporation RCRA FacUity Investigation
UClke/^ W0#: 1B940 LWR#: ^ //)/^ /
SFTC: West of M-381 '
— DESCRIPTION: Strategic RFI Background; 2 ft
PARAMETCRS
Volatile Organics
Semi-Volatiles
METHOD
8240
8270
^Jf f C/A T
\^
la
JUjfth—A^^iiyi^
m DATC: -^^^^Z TIME: ^^2- SAMPLER: ^^.^
124
/9gZ2-Thiokol Corporation RCRA FaciUty InvestigaUon
WO#; 1B940 LWR#; ^//O/^j /
srre: West of M-381 ^fO^t^X^f
DESCRIPTION: Strategic Rn Background; 2 ft
PARAMETCRS
Metals
Mercury
Cyanide
HMX
Nitroglycerin
pH
DS: 7JC^^ 9f
METHOD
6010
7470
9010
HPLC
HPLC
9045
9W^038
TIME: ^^ir Z^ SAMPLER: ^y^uj
iSa^-^L
TKokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#: £:/C>GC> f
SFre: West of M-381 -2. '
DESCRIPTION: Strategic RH Background; if.ft XXxi^ / ICC-l^
PARAMETERS METHOD (
VolatUe Organics
Semi-VolatUes
8240
8270
iOcy
DATE: "YiJuCjf '^7 TIME:^^'^^^ SAMPLER: /AXc->
f.
(^It^
TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: E./0(ffC?f
SFTC: West of M-381 x-
DESCRIPTION: Strategic RH Background; ;*-ft Oi>LO U&^ fx-
PARAMETCRS
Metals
Mercury
Cyanide
HMX
Nitroglycerin
pH
Sulfate
METHOD
6010
7470
9010
HPLC
HPLC
9045
9036\9038
DATC: ' ^« h ^f- TIME: C022^ SAMPLER: 'V^^
ii-
m^ TKokol Corporation RCRA FacUitv Investigation
W0#: 1B940 LWR#: A!?^^h^/
SFTC: West of M-381 C^^Oi^Cf
DESCRIPTION: Strategic RR Background; 5 ft
PARAMETCRS
VolatUe Organics
Semi-VolatUes
METHOD
8240
8270
DATC: 7ju(y(?f •xiME:09ff SAMPLER; •J^
./>,>.!,;,.v *'
ii
^^
TWofto/ Corporation RCRA Facttity InvestigaUon
WO#:1B940 LWR#: >^^,^^ /
SFTC: West of M.381 /i^<25«S? /
DESCRIPTION: Strategic RFI Background; 5 ft
PARAMETERS
Metals
Mercury
Cyanide
HMX
Nitroglycerin
pH
Sulfate
METHOD
6010
7470
9010
HPLC
HPLC
9045
9036\9038 DATC: -r^a^ <F<r ^, ,^ SAMPLER ••^^
125
— \ 09^ S^ar^p/t^ dtfiiyer^ol h /U'-^S /.dUarokta Ctndc^
i~UJR^ ^ E/o&oi
^C-JZ-^.^^^W'U^^^
M'\
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.ty^l^ C'C/y^i'^yJ^' ^ , Fi^'Cry^- iM.jhi/ "i^^m (^WMtMX .ty^^ C<f^i->*yhi ^ , f-i''('r\h i/yc^h^
hnvi..el/ii^-<'if\. f i
iV^-c^tij. '/' i^rO ^ /^^^.^ , /^ A,
S'S4^¥>/^
TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#:
SFTC: M-186 Industrial LandflU ^ \r
DESCRIPTION: SWMU # 212; Grid # _^^5 ftT
PARAMETERS
VolatUe Orgranic
Semi VolatUes
METHOD
8240
8270
DATC: l-Zl'fj- TIME: \3l SAMPLER: f^<^
/Sy^ytf^ C/)_*^
J1
m
''•-•'>M':^4^''-J,n
I'*
"h
126
£:i^y^4>A
ISW^ Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#:
SITE: M-186 Industrial LandflU
DESCRIPTION: SWMU # 212; Grid ;5ft. S^oi^ U—C/OM-
PARAMETERS
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
METHOD
DrTC?^-^'"?'/
6010
6010
6010
6010
6010
7470
TIME:/^/Sl SAMPLER; fuj/J<
^ I' .i
«j^' •-«
':/; ' ^^^
/•''*-
>.;?
f
V /^ 5^>v,pi.
IllH^ Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#:
SFre: M-186 Industrial LandflU
DESCRIPTION: SWMU # 212; Grid # h.j^
PARAMETERS
Volatile Orgranic
Semi VolatUes
J>ATE:^';il-9y
METHOD
8240
8270
TIME :l3fj SAMPLER fll^M^
•t^:r
mi
/O ' Siy^^}^
lSi^S_ TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#:
srre: M-186 Industrial LandfiU ^^ ^ O
DESCRIPTION: SWMU # 212; Grid #2^3 10 ^^
PARAMETCRS
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
METHOD
6010
6010
6010
6010
6010
7470
DATC: ^'-^/'9Y' TIME: IS'f^ SAMPLER: fi>//j^
=1
*:.
gHffjlfS?!?^^!'?^?!^!*^^!!^^?'^^^^
• y I. Jl \* / ,*\41 •:.* 'J I .' ', r. ,'. J \ . .'
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^
SFre: M-186 Industrial LandfUl -^fe-^'^ ^^
DESCRIPTION: SWMU # 212; Grid #^3^715 ft.
dijj.h i>^«n^ S^d
PARAMETERS
VolatUe Orgranic
Semi VolatUes
METHOD
8240
8270
DA TE7'^-9^ TIME:/y/^ SAMPLER: MJ<
-^ 1
1^
W •
t
_. .M/0_
i
JS^^i^U...
TKokol Corporation RCRA Fadltty Investigation
W0#: 1B940 LWR#: ^
SFTC: M-186 Industrial LandfiU -^^sl--^ ^
DESCRIPTION: SWMU # 2U; Grid it^^j 15 ft.
C^CAr J»aut** S^>i <j
PARAMETCRS
Arsenic
Barium
Cadmium
Chromium
Lead
METHOD
6010
6010
6010
6010
6010
7470
TIME: /fV^ SAMPUER-F^M^
•
Si
It
4* i
r^: I
'-'I
j^Jl^s:?**-!^/^ ^^VLUA/S.
TKokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#:
SFTC: M-186 Industrial LandfUl
DESCRIPTION: SWMU # 212; Grid #/? ; 5 ft.
PARAMETERS METHOD
VolatUe Orgranic
Semi VolatUes
8240
8270
DATC: ^'J-/-9y TIME:/9 i'O SAMPLER :f^A<
-I
t -i«l
u
-ci
1tl
ri:L?:T-ji;..<:.'j.'7-,y^;jyi>:i;iiV.»jr
128
S'^S^y^U.
ft-. /^
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#;
SITE: M-186 Industrial LandfiU .
DESCRIPTION: SWMU # 2U; Grid # /2 ; 5 ft.
PARAMETCRS
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury. _
DATC: ^-;V--P>*
METHOD
6010
6010
6010
6010
6010
7470 7470 CIAJIICL
TIME: /^^O SAMPLER:* **'^/
/5''t>l
4i>-s^^^
TKokol Corporation RCRA FacUity InvesUgation
W0#: 1B940 LWR#:
SITC: M-186 Industrial LandflU ^
DESCRIPTION: SWMU # 212; Grid # /.S ; 10 ft.
jO' JB^fie
1^01
PARAMETCRS
VolatUe Orgranic
Semi Volatiles
DATC: 9'P^hn TIME:
METHOD
8240
8270
L-7'JOI SAMPLER; /^//J«
TKokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#:
SFTC: M-186 Industrial LandfiU
DESCRIPTION: SWMU # 212; Grid # /3. ; 10 ft.
\\
PARAMETERS
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
DATC: -J. J^l' n TIME:
METHOD
6010
6010
6010
6010
6010
7470
t^\»f SAMPLER fi^hc.
fe/1 1
^•' '.•ar-
P^^^SSfc^^T^vv^^V^^?^
'J>M}"«.-:-;.'.^'.: ; .
^^ ^*lB^.r"'"''"'^°^'^"=«^I-vesUg,
129
LWR#: STTE: M-186 Industrial LandfiU
DESCRDTION: SWMU # 212; Grid # /2_; „ ^
PARAMETgPC
Volatile Orgranic
Semi Volatiles
METHOD
8240
8270
x™^ ^-^-9V ™B, /5-/6 *L™,/:^/jc
tl
- 1
"fni
/y ^ ^ir^^/^
.i^f^^_
7U<>A:o/ Corporation RCRA FadUty Investigation
WO#: 1B940 LWR#:
SFTC: M-186 Industrial LandfiU
DESCRIPTION: SWMU # 212; Grid # /S ; 15 ft.
IE
PARAMETCRS
Arsenic
Barium •^
Cadmium
Chromium
Uad
Mercury . ^ .
METHOD
6010
6010
6010
6010
6010 .
7470 J^ Mercury ^^ , n., THO •^*' ri \l \i
DATC: ^-P/-7T TIME: l^ftf- SAMPLER: r**'/"^
.GrtCJ^ /2 .J^**^/" <^^
/X/^_ JTtoko/ Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#:
SFTC: M-186 Industrial LandflU .— .—.
DESCRIPTION: SWMU # 212; Dup., Grid # /2—; /j ft-
PARAMETERS
VolatUe Orgranic
Semi VolatUes
METHOD
8240
8270
DATC : 'P^'^/'^^ TIME:/-S'/<i SAMPLER: F^/^*^
/^Z^
#
TWoto/ Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#:
SITC: M-186 Industrial LandfUl
DESCRffTION: SWMU # 212; Dup., Grid #/3 ; jT^. ft
PARAMETERS
Arsenic
Barium
Cadmium
Chromium
Lead
DATC: /^e2/-^.
METHOD
6010
6010
6010
6010
6010
7470
TIME: /Sl (> -SAMPLER: F^M ^
i,.,M'
|f.--«-r
I'*)' 130
•Ti i
:'^l^
TJkiotoZ Corporation RCRA FacUity InvestigaUon
WO#;IB940 LWR#: ^/^^Q 7
SFTC: M-186 Industrial LandflU
DESCRIPTION: DECON RINSE WATCR
PARAMETCRS
VolatUe Orgranic
Semi VolatUes
METHOD
8240
8270
DATC: 1-21'9^ TIME: /SOO SAMPLER: Pbty'
Coei^ CoajecX(5.
_Prior_ip_CoJkc'h
TKokol Corporation RCRA FacUity Investigation
WO#; 1B940 LWR#: £>^^^ 7
SFTC: M-186 Industrial LandfiU
DESCRIPTION: DECON RINSE WATER
METHOD
Q.lt<^ S-Q// S<?»y
j^__drd/cc_yp^_^
^£c&/j^j^>^f/y-^
^®*j^??^;.-ftv^'^^'•;.;--•••:•
• /7-/^<^ 2^ Jof.L^ /^f-f
131
b"^^^ 5;V^f/ fjr-r yvnj?4 p^Sr U^^f^Tt+ee. : S<^^^ , ujfi^^/i^
Sc' 6 «-^r ^ g^^ ^g ^1^ ^ ^ o^r^-f -'^^ §6'/=-
p^i^b UJAt-t^^*^. JV^JE <C^i/t^<S^T-z>, cJfct4»J HT?U-.>rP ^^ -i
rod^p -<^ tg" SAAIPLC:
TKokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#;
SFTC: M-186 Industrial LandfiU
DESCRIPTION: SWMU # 212; Grid # /S~ls ft.
PARAMETERS
VolatUe Orgranic
Semi VolatUes
METHOD
8240
8270
^fo^Cou^ /
i9 '/ro
•Sur <^ CLA<^
i I
CAlL£ gb>-)oeOtcc^eD/M£Ors
#
DATC: T-Z^-ff miE: ^^ 7 SAMPLER: '^;^^
TKokol Corporation RCRA FaciUty Investigation
W0#: 1B940 -V LWR#:
SFTC: M-186 Industrial LandfiU
DESCRIPTION: SWMU # 212; Grid # / STs ft.
PARAMETCRS
Arsenic
Barium
Cadmium
Chromium
Lead
DATC: I^ZO^f^ TIME: g 5 7 SAMPLER: y^^*^
METHOD
6010
6010
6010
6010
6010
170
">ll
1l'
/t) -$t/)a/?/^
P^iOJOL
Thiokol Corporation RCRA FadUty Investigation
WO#; 1B940 LWR#:
SFTC: M-186 Industrial LandfiU
DESCRIPTION: SWMU # 212; Grid # /S^; 10 ft. /=
/7/,^
PARAMETCRS
VohitUe Orgranic
Semi Volatiles
METHOD
8240
8270
CiAvf \ Sicr
DATC: 7S>6f^ TIME:^?^^^
nOLO
SAMPLER: J" •/''»'
111
132
SITC: M-186 Industrial LandfiU
DESCRIPTION: SWMU # 212; Grid # /',"., IQ ft.
PARAMETTBS
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
DATC: •p.'^i fy TIME:
METHOD
6010
6010
6010
6010
6010
7470
SAMPLER: S it-
isf €H/viP/^
'K/ococovA'/
•-^
^(^ho
f>rn
Thiokol Corporation RCRA FacUity Investigation
W0#: IB940 LWR#:
SFTC: M-186 Industrial LandfiU ^
DESCRIPTION: SWMU # 212; Grid # __/^15 ft.
PARAMETERS
VolatUe Orgranic
Semi VolatUes
METHOD
8240
8270
^
C/3 ^ ft
DATE: -?-^^f'^
/* AJ
TIME: ^f/^ SAMPLER: ^d
Thiokol Corporation RCRA FaciUty Investigation
WO#: 1B940 LWR#:
SFTC: M-186 Industrial LandfiU
DESCRIPTION: SWMU # 212; Grid # /^ ; 15 ft.
PARAMETCRS
•$<r/'(f/,/i^<w
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
DATC: 7-J?^-/V TIME:
METHOD
6010
6010
6010
6010
6010
7470 CJ^
^fi/-p SAMPLER: £><!
^i^^s^S^Si^!!^ ^m
*i "^V ' \.\L slH -^'i ' '• ' * ' J Jl"* *" * '-- ^ •
>l a V/.*V»Ji';.?.'*/. '• • .-••< •.. .
#
/^'^/
Thiokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#:
SFTC: M-186 Industrial LandfiU
DESCRIPTION: SWMU # 212; Grid # ^J ; 5 ft.
PARAMETCRS
VolatUe Orgranic
Semi VolatUes
METHOD
8240
8270
^ />^/^
133
r/^ • s:i/' ^
/^/r^
DATC: 7-^ If'' TIME: /^?»' SAMPLER:
•,<to
#
TWotol Corporation RCRA FacUtty Investigation
W0#: 1B940 LWR#:
SFTC: M-186 Industrial LandfiU
DESCRDTION: SWMU # 212; Grid # ^5 ; 5 ft.
PARAMETCRS
Arsenic
Barium
Cadmium
Chromium
Uad
Mercury
DATC: 1-91 r^
\
TIME:
METHOD
6010
6010
6010
6010
6010
7470
/C ,5 SAMPl,ER:
£^
Mil Sz^^
"B/O^Courj f
(^Vs-^
161^
TKokol Corporation RCRA Facttity Investigation
WO#: 1B940 LWR#:
SFTC: M-186 Industrial LandfUl S 7
DESCRIPTION: SWMU # 212; Grid # Tf ; 10 ft.
PARAMETCRS METHOD c/^ r .57^/
#
VolatUe Orgranic
Semi VolatUes
8240
8270
DATC: 7-.^^ JV TIME: iT4tf^ SAMPLER: ^^
/*-r
i'-
134
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#;
SFTC: M-186 Industrial LandfiU
DESCRIPTION: SWMU # 212; Grid # J^? ; 10 ft.
PARAMfeTCRS
S*/e/l(t>AVr
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
DATC: 7- 5>/' /V TIME:
MEIHOD
6010
6010
6010
6010
6010
7470
/<J.'^^ SAMPLER
/J 1^ JPC •
J± _ /
JOlMSl.
Thiokol Corporation RCRA FaciUty InvesUgation
W0#: 1B940 LWR#:
SFTC: M-186 Industrial LandfiU
DESCRIPTION: SWMU # 212; Grid # ^3 ; 15 ft.
^<r_/j,:^
PARAMETCRS
5c/e/7 / u /v
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
DATC: 7-^^ -fV TIME:
METHOD
6010
6010
6010
6010
6010
7470
/c:<L/s' SAMPLER:
K^
S^
i?C
J^JA^^ fh
\j^r>iS)r
tluokol Corporation RCRA FaciUty Investigation
W0#: 1B940 Vf/^:
SFre: M-186 Industrial LandfiU
DESCRIPTION: SWMU # 212; Grid # ^2 ; 15 ft.
PARAMETERS METHOD
VolatUe Orgranic
Semi VolatUes
8240
8270
^)\TC: ~P-J>^ ~fu TIME: /i):i/£' SAMPLER:
!^M&h^^
r^ |iJiW!l^ajpi^#MpiWj,W^
^fe»'»'-»••'*•'LA"»' '•*''?i^.' .'•*."'* •. ' • •
i
OeS-l
2^ Joii^ l^n
135 f
-O^ SlTb A-7 M'/^C TAIT^ 1JJA^1£ LA-tJQflLM. S ^ KL U ^ z^lZ^ '
j£J^<.UL. ^ eo' \
Ma^L Thiokol Corporation RCRA FacUity InvestigaUon
W0#: 1B940 LWR#: If- {I^H^ 5./0i,/ 7
SFTC: M-186 Industrial LandfUl
DESCRIPTION: SWMU # 212; Grid # j?S" ; 5 ft.
PARAMETERS
VolatUe Orgranic
METHOD
8240
DATC: ^^s/U-l «f 94 TIMEh<^ "^^ "T'SAMPLER: (s>-\
-^/S'n
^jJlhi__CM^
b
•
TKokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: EdOU>l 7
SFTC: M-186 Industrial LandflU
DESCRIPTION: SWMU # 212; Grid # Skhlj 5 ft-
PARAMETERS
Barium
Cadmium
Chromium
Lead
Mercury
METHOD
Oof1>
6010
6010
6010
6010
6010
7470 wiercury 7470 -r^ r
DATC: Z-'r J^lj T*M TIME:C>f OS SAMPLER: ^%-]
Thiokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#: £/06f 7
SFTC: M-186 Industrial LandfiU
DESCRIPTION: SWMU # 212; Grid # ~S^~^S ft.
PARAMETCRS
Semi VolatUes
METHOD
8270
^
DATC: ZfJu(:i fj: TIME: ^'^^'^'^ SAMPLER: <^J
136
C^f "J- TKokol Corporation RCRA FacUity Investigation
-''-^ W0#: 1B940 LWR#: iL.i>0,<<^ &/0(a/ /
SITE: M-186 Industrial LandfiU
DESCRIPTION: SWMU # 212; Grid # 3 b ; 10 ft.
PARAMETERS METHOD
I^A
Semi VolatUes 8270
_DATC: ~^f^^/ '5"/- TIME: ^ t / 7^ SAMPLER: ^£)' he>cJ~ S^l-K^
^"k
TTiioJto/Corporation RCRA FacUity InvesUgation
W0#: 1B940 LWR#; -T^-H^l^ E/0(i>/-J
SFTC: M-186 Industrial LandfiU --
DESCRIPTION: SWMU # 212; Grid # _2_£.'. I" ft-
PARAMETCRS
VolatUe Orgranic
SuUl IfUfcilW _^
METHOD
8240
8270
DATC: 2-4^ ^/"^^ TlME:0^l'^ SAMPLER •,f>l
\h^v TKokol Corporation RCRA FacUity Investigation
WO#; 1B940 LWR#: -if ^ ^^ C^ B/O (a I f
SITC: M-186 Industrial LandfiU
DESCRIPTION: SWMU # 212; Grid # 3'-, ; 10 ft.
PARAMETCRS
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
METHOD
6010
6010
6010
6010
6010
7470 r
DATC: ZJ-^^I ^^ TIME: O ?/?- SAMPLER:
f-tJ^^
r-X> •-•.;,'»•. r .-yii-a, iiJ
#
^?S'^'?^'vi.^''A:vy'^
137
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^! W0#: IB940 LWR#: £JCI/(^ E./Oi>f 7
SFre: M-186 Industrial LandflU
DESCRIPTION: SWMU # 212; Grid # ?<- ; 15 ft.
PARAMETCRS METHOD
"h-^/TO
"'K
t
VolatUe Orgranic
•'''"ni Viilnfilftf <^
8240
82aa
DATC: "^9 >/u. / -?^ TIME: ^ 7 3£> SAMPLER: Q C
OH ^ I ''Y ^ '^/ \
Thiokol Corporation RCRA FadUty Investigation ^
W0#: IB940 LWR#: t- fl^i'(^ t:/OG/y
SITC: M-186 Industrial LandfUl _
DESCRIPTION: SWMU # 212; Grid # lh ; 15 ft.
METHOD
Semi VolatUes 8270
DATC: ^"^J v..>~\'^*4 TIME: (^f 30 SAMPLER: £>
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: (• fG fU> tifOGH
SITC: M-186 Industrial LandfiU
DESCRIPTION: SWMU # 212; Grid # 3fe ; 15 ft.
PARAMETCRS
^lefii^^
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
DATC: ^f-/ w-f? O-TIME:
METHOD
hofO
6010
6010
6010
6010
6010
7470
CP^ "SS^ SAMPLER:
P-^
138
r'^r.-
lOG0
Thiokol Corporation RCRA FaciUty InvestigaUon _
WO#: 1B940 LWR#: ^[QILJ t./0<h/'/
SFTC: M-186 Industrial LandfiU
DESCRIPTION: SWMU # 212; Grid # TCS; 5 ft.
PARAMETCRS METHOD
_Z^
Semi VolatUes 8270
DATC: if-J c^t f ^ TIME: f0^t> SAMPLER: (S-T
SL
Thiokol Corporation RCRA FaciUty Investigation
WO#:1B940. LWRIt: ^+^j.(^ E/Ch/1
SFTC: M-186 Industrial LandfiU
DESCRIPTION: SWMU # 212; Grid # V3 ; 5 ft.
PARAMETERS
VolatUe Orgranic
Sem^^riatUes
METHOD
8240
-S\£j^—c^i Q^^
DATC: ':2_'fWu. ( *? W-TIME: /C'^i^ SAMPLER: <J-T
TKokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#: B-fO(sl']
SITE: M-186 Industrial LandfiU ^
DESCRIPTION: SWMU # 212; Grid # /• S ; 5 ft.
PARAMETCRS
TLrsemc
Barium
Cadmium
Chromium
Lead
Mercury
DATC: 'Z9Ax^\ Itf TIME:
METHOD
i/OlS
6010
6010
6010
6010
6010
7470
IOO'O SAMPLER:
f^i
fr-f
Vxk'-
W-r
?*^^^55^sl^^^^f^
(» 139
/oto TKokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#: ^'
SFTC: M-186 Industrial LandfiU
DESCRIPTION: SWMU # 212; Grid # //JS ; 10 ft.
^/^y7 LS/j^
PARAMETCRS METHOD
Semi VolatUes 8270
/-UJ
DATC: -2.^^/^Lj TIME: /OQ-O SAMPLER: i-^C_
TKokol Corporation RCRA FaciUty Investigation
WO#: 1B940 L\VR#: B^O f U
SFTC: M-186 Industrial LandfiU
DESCRIPTION: SWMU # 212; Grid # £/3j, 10 ft.
PARAMETCRS
VolatUe Orgranic
METHOD
8240
8270
<f/^6/7
S
DATC , •i'Vg^l ^ 4- TIMF.:/«';^'^ SAMPLER: 6-T
•
TKokol Corporation RCRA FaciUty InvestigaUon
W0#: 1B940 LWRM: ^J^s^^^ S/Ob/l
SFTC: M-186 Industrial LandfUl
DESCRimON: SWMU # 212; Grid # H-^ \ 10 ft.
PARAMETERS
*^/il1C(Ji.ll* Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
METHOD
6010
6010
6010
6010
6010
7470
DATC: ^-'r^w-l '^ V TIME: / 0 ^Q SAMPLER: 3^
1-
140
lOUr^ TKokol Corporation RCRA FacUity InvestigaUon
W0#; 1B940 LWR#; ^ (O-f L, S/06f 7
SITE: M-186 Industrial LandflU
DESCRIPTION: SWMU # 212; Grid # ^3; 15 ft.
PARAMETERS
VolatUe Orgranic
Semi VolatUes
METHOD
8240
8270
^u
DATC: 1-%A^\ ^1-1 TIME: IC.<~4'i SAMPLER: ^C.
-2. I/TT.
77.i»*./Corporation RCRA FaciUty Investig^on^_^ ^^6/?
W0#: 1B940 LWR#: CTT^ C-'
SFre: M-186 Industrial LandfiU
DESCRIPTION: SWMU # 212; Grid # _2o.; 15 ft.
PARAMETCRS
Arsemc
Barium
Pnilmiiim
Chromium
Uad
Mercury
DATC:2^i^l^tV
METHOD
6010
6010
6010
6010
6010
7470
TIME:/©'-/-^ SAMPLER:
.r i^
^
>3^.^..jLy ^/. a-^
//^<:? A^//7^ 'E/CtnK^ -ti/an ;^V ^?^ /2MM?I^
of -th. SAmi />^ranukrs CL^ //TjkJ
Qhoi/£^ )S/lmp/£S '/aL./^ /^ A/.^^R
falod^r.j^yr, /j/?r/er Liv/^ ^ /^/06/7 t JUMJL^
K^!^i^^y*si?^^^55v3Jr^
•
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TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#:
SFTC: M-136 Old Waste OU Disposal Pit
DESCRIPTION: SWMU #208; Center of Pit, 5 ft.
PARAMETER»-
VolatUe Organics
METHOD
8240
S/H
DATE: //hj-£> 9^ TIME: ^I^O SAMPLER: TVUD
52), Sll.
^gJob/es, ^ ^ray/cj
LlA f
^/rajlf dtit^l^, ^Jcr
W ltf\ ^<0^^ ^ Ul
TKokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#:
SITE: M-136 Old Waste OU Disposal Pit
DESCRIPTION: SWMU #208; Center of Ptt, 5 ft.
PARAMETCRS
Cadinium
Chromium
Uad
METHOD
6010
6010
6010
DATE: / A06 '?i^ TIME: IlOO SAMPLER: /U ^
hit ac//^tU'
^^
#
•^^•^MM
'^TV J
142
-Au^ 3 ,l99f
/)?fS' /C>fi Si/c af -/UL ^/^ c/ru^ ^Mir^^X Ar^r. /J-/B7 ^ID/UU r-
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: B/0(oZZ.
srre: M-187 Old Drum storage Area
DESCRIPTION: SWMU # 551; Grid # 24 . Surface
PARAMETERS
VolatUe Organics
METHOD
8240
DATC: ^-"5-f^ TIME: ^.'-2-? SAMPLER:A^^
TKokol Corporation RCRA FaciUty InvestigaUon
W0#: 1B940 LWR#: £/OiiZZ.^
SITE: M-187 Old Drum Storage Area
DESCRIPTION; SWMU # 551; Grid # c4 . Surface
PARAMETCRS METHOD
Cadmium
Chromium
Uad
SUver
Mercury
Perchlorates
DATC: %-^-^^ TIME:
6010
6010
6010
6010
7470
IP
-^f-'^T SAMPLER:/f •A^
0 Sacddc a/- /ft/s S/7f
^a.. X a^^fimfMY r^o U^
^^ff^rff.
SL
.CBQB Tl S^r-nc^ X>Rfi<it^eiEi^^ ARefl ^ Ubiei-^^f^ Tl-A ^ Suiw^ 4^^4?
4
#
TKokol Corporation RCRA FacUity InvestigaUon
W0#: IB940 LWR#:
SITC: T-l Photographic Processing Drainfield
DESCRIPTION: SWMU #648; Grid # <y^ . 5 ft.
PARAMETC.R.S METHOD
SILT u^'fH S-OA^e:
riiJE SAQf^ Ai^^ CLAX,
Cadmium
Chromium
SUver
Lead
6010
6010
6010
6010
-Moiii-.
-Ul ^.j-Sio^
OATC:23 AOG> TIME: 2>© 2^) SAMPLER: '^/FO^
TKokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#:
SITE: T-l Photographic Processttig Drai^ield
DESCRIPTION: SWMU #648; Grid #_T_, 10 ft.
.g(;.T A-i-jQ CLAT^
PARAMETERS
Cadmium
Chromium
SUver
Lead
METHOD
6010
6010
6010
6010
^noi ST^
-^/Si ./ro.
DATC: Z?>^0&^^ TIME: ^^ ^^ SAMPLER: /^
w)
1
#
-^uun^t^ <A^PL^ f=ejor^ ^pric rAO'fL.
Thiokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#:
SFTC: T-l Photographic Processuig Septic Tank
DESCRIPTION: SWMU #648; Sample #_0i—;
PARAMETCRS
Cadmium
Chromium
SUver
Lead
METHOD
6010
6010
6010
6010
DATC: 'Z-'bP^^ ^^ TIME: 0^ ^O SAMPLER; -^H^
$tv^P6£
mmm
•••..:.• {'iA:r-.^^fJ\,,^'^iXj.
144
e^^}-ii/
OIL J<p/tt -fa^l^ pyaii^_ l^/^/^
^df-'Tfi
L'ija+.
Thiokol Corporation RCRA FacUity InvestigaUon
W0#; IB940 LWR#:
SITE: T-l Photographic Processing Drainfield
DESCRIPTION: SWMU #648; Grid # ^/^ , 5 ft.
PARAMETERS
Cadinium
Chromium
SUver
Lead
DATC: 6>S'- ^i
METHOD
6010
6010
6010
6010
TIME: <P^;>V SAMPLER: L^C
^-0
Thiokol Corporation RCRA Facttity Investigation
W0#: 1B940 LWR#:
SFre- T-l Photographic Processuig Drainfield
DESCRIPTION: SWMU #648; DUP; Grid #_£K^
PARAMETERS
Cadinium
Chromium
Silver
Lead
DATC: l?''d'^
METHOD
6010
6010
6010
6010
_Cft-
•HME: tf^'i'Z' SAMPI.ER: J^ <-
W:\0
TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#:
SITE: T-l Photographic Processing Drainfield
DESCRIPTION: SWMU #648; Grid #,. ^ y ,10 ft.
PARAMETCRS METHOD
'?/ -^
Cadmium
Chromium
SUver
Lead
DATC: 9-^-ini
6010
6010
6010
6010
TIME: lot 1. SAMPLER: P^
4^/^
S^^ / ^ eyy^
j^?sma»«gA<!j-jjii#m'Amijiii.^
m¥im//i^!^m'>^^'YyM/^iii^
m i
145
.l^bJIS.
TKokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#:
SFTC: T-l Photographic Processing Drainfield
DESCRIPTION: SWMU #648; Grid # .^/y , 5 ft.
PARAMETCRS
Cadmium
Chromium
SUver
Lead
METHOD
6010
6010
6010
6010
^''(^ ' C/l ^^
^^o
DATC: ^PS^^"^ TIME: /A <.i>i^ SAMPLER: iP ^
-#, IP'. V-Thiokol Corporation RCRA FacUity Investigation
'W0#: 1B940 LWR#:
SITE: T-l Kiotographic Processing Drainfield
DESCRIPTION: SWMU #648; Grid # ,10 ft.
^^ s-^
PARAMETERS
Cadmium
Chromium
SUver
Lead
METHOD
6010
6010
6010
6010
s.'// ; ^/. V^
DATE: fPJ-'fi' TIME: /O'.HO SAMPLER: f^ ^
/"•iT
^1
TKokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#;
SITE: T-l Photographic Processing Drainfield
DESCRDTION: SWMU #648; Grid #5? ,5 ft. "^
PARAMETCRS METHOD
HI
Cadmium
Chromitnn
SUver
Lead
DATC:
6010
6010
6010
6010
f-^?-^"^ TIME: /^-fr SAMPLER: P(
146
TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#:
SITE: T-l Photographic Processing Drainfield
DESCRIPTION: SWMU #648; RINSE BLANK; Grid #j? , ^ ft.
PARAMETERS
Cadinium
Chromium
SUver
Uad
METHOD
6010
6010
6010
6010
-OATC: ^V; 7^ TIME: /f'-Cf^ SAMPLER: /P c
.LLUIL
Thiokol Corporation RCRA FaciUty Investigation
W0#; 1B940 LWR#:
SITE: T-l Photographic Processing Drainfield
DESCRIPTION: SWMU #648; Grid # ^J , 10 ft.
PARAMETERS
Cadinium
Chromium
SUver
Lead
DATE: ^-^P-fl^
'5.
^
METHOD
6010
6010
6010
6010
TIME: Iifli i SAMPLER: ^^
i'f/ .' <r4 7--
\l
i-^
y^*R¥f^^^^y^f^yt
/OOP
24 Au^u^i- Qj-
0/d coas/c ^/7 f>i/ /Of M'/^L ^/jjA/u ^208
Uii^^ bacKhc /o eKCaoak, Az> fSQui'-cJ Jc^ft. ^
f^arxL /)ak.eS(^n - l?dr.liO€. Of>c*'aifnr. fSJ'<fAf Drd.£-l<
II XOl 2o-U fk T- 7d
TKokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#: E/OlaZZ
SITE: M-136 Old Waste OU Disposal Pit
DESCRIPTION: SWMU #208; Center of Ptt, 5 ft.
/P/r-
^
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC: Z4 fh^O 9<f TIME: /OI "^ SAMPLER: f^i^
TKokol Corporation RCRA FaciUty InvesUgation
W0#: 1B940 LWR#: £'/0(aZ2.^
SFTC: M-136 Old Waste OU Disposal Pit
DESCRIPTION: SWMU #208; Center of Pit, 5 ft.
PARAMETERS
Cadmium
Chromium
Uad
METHOD
6010
6010
6010
VA'R.t^ 'B'RQLLUJ^
^artc/ d/lc/ ^ra(/ff
^^cciks £rf
appi^ami^Cc. a^
^/'/. ^^or
breu/^/ /Ac/tad&firf
O^ bjQ ' ac.fiurk
/D3jr
DATC: Z4- AU<^ '9^ TIME: /d) IS~ SAMPLER: Ac^
TKokol Corporation RCRA FadUty InvestigaUon
W0#; 1B940 LWR#: E/0(e>2-.~L^
srre: M-136 Old Waste OU Disposal Pit
DESCRIPTION: SWMU #208; Center of Pit, 10 ft.
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC: 24 /hJ<^ fi- TIME: /OjC SAMPLER: /^'O'
'Pdr^K. 'ZrouOn
//oist /^ra,<y<-l
^nJ ^ilh
A)r/o,^ 6 Avrfe'/? A
Jbut Co/orlACf ti-f
A11 Co^-fam/na tter>y^
Adt fJ/Ssd/^/x.
p
• y.
• 1^'
148
/l)3^ Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#; ^/O ^Z "L.
SFTC: M-136 Old Waste OU Disposal Pit
DESCRIPTION: SWMU #208; Center of Pit, 10 ft.
PARAMETERS
Cadmium
Chromium
Uad
METHOD
6010
6010
6010
At
•ft.;.
•r
ri^
%
f
1-1'
iif—
/04€
BATE: 24/h'^ 9'f TIME: /^J^ SAMPLER: A^
TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/di>ZZ.
srre: M-136 Old Waste OU Disposal Pit
DESCRIPTION: SWMU #208; DUP., />/7 Or Pi+ , M-FXi.
/a .i^
PARAMETCRS
Cadmiimi
Chromium
Lead
METHOD
6010
6010
6010
DATC: Z4 Av^ 9^ TIME: /^> 5 S"^ SAMPLER: J^oJ
TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#; fc7<5^ Z T—
SFTC: M-136 Old Waste OU Disposal Pit
DESCRIPTION: SWMU #208; Outer edge of Pit, 5 ft.
PARAMETERS
VolatUe Organics
METHOD
8240
'Sa^J S drear c/
DATC: Z4 >4/f '/4 TIME: /^^ SAMPLER: f=tU
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#; £7Z?4Z Z_
SFTC: M-136 Old Waste OU Disposal Pit
DESCRIPTION: SWMU #208; DUP., AOkr ^A^ ' ^ "'
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC: 24 Au^ 14 TIME: /O^C SAMPLER: ^"-^
Oll Jf'sCo/o rg-ho
B
//)4S TKokol Corporation RCRA FaciUty Investigation
WO#; 1B940 LWR#: ^/ICXeiZ Z-
SFre: M-136 Old Waste Ott Disposal Ptt
DESCRIPTION: SWMU #208; Outer edge of Pit, 5 ft.
PARAMETCRS METHOD
149
Cadmium
Chromium
Lead
6010
6010
6010
.DATC: Z4 Au^ 9^ TIME: /04^ SAMPLER: F(^
Hi
/0S€' Thiokol Corporation RCRA FacUity Inv^tigation
W0#: 1B940 LWR#: £:i/OGZ "5^
SITC: M-136 Old Waste OU Disposal Pit
DESCRIPTION: SWMU #208; Outer edge of Pit, 10 ft.
/A/)ist McJtotn
E^o(^t^ "^y/^,
PARAMETCRS
VolatUe Organics
METHOD
8240
z?/;^ ^//^ UflH
<20/«I ^ m(/c I.
A/0 Acifcalalc'
DATC: ^ ^/l*^ 9^ TIME: /G^"^ SAMPLER: f-^
nJor 6r c/isO>r6/a'ht toj
Thiokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#: £/Oifl'Z-
SFTC: M-136 Old Waste OU Disposal Pit
DESCRIPTION: SWMU #208; Outer edge of Pit, 10 ft.
PARAMETCRS
Cadmium
Chronuum
Uad
DATC: 24 A/uf U TIME:
METHOD
6010
6010
6010
/^^^^ SAMPLER: /=^
li
^^'^'••iyS^)!
150
/5do ML <Jra/\/l ^fz^a^^ QdrJ ik-(Ql 'ScO/ULI ^ S^f_
TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^O^Z Z.
SITC: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid # 2'^ , Surface
PARAMETERS
VolatUe Organics
METHOD
8240
^rau<^/ ^
DATC: Z4Au^ f<f TIME:y^^*^ SAMPLER: /^^^^
TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: d:/OG,Z 1^
SFTC: M-187 Old Drum Storage Area
PARAMETCRS
Cadmium
Chromium
Uad
SUver
Mercury
Perchlorates
DATC: 24 Af 94 TIME:
... J.
MEIHOD
6010
6010
6010
6010
7470
/^<3 SAMPLER: fuJ
v5k?W
Koad ha^ AAQA
i'S'lD Thiokol Corporation RCRA FaciUty Investigation
W0#: IB940 LWR#: S/O^ZZ^
SITC: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid # 2-f-. 2 ft. (Srt2c/cf j-S7/7V
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC: ZfYfu/j 9 7 TIME: I'i f£> SAMPLER: /^i-*J
TKokol Corporation RCRA FacUity Invjstigation
W0#: 1B940 LWR#: <t:/<362Z
SFTC: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid # Zrt , 2 ft.
PARAMETCRS METHOD
Cadinium
Chromium
Uad
SUver
Mercury
Perchlorates *^ V
DATC: 24 Ah^'i4 TIME: /S-/0 SAMPLER: fTuJ
6010
6010
6010
6010
7470
IC
i
/530 Thiokol Corporation RCRA Faciltty Investigation
W0#: 1B940 LWR#: £^/0C>Z'2~
SFTC: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid # ZA" , 5 ft.
PARAMETCRS
VolatUe Organics
METHOD
8240
151
HATE: 2^ Auf 9^ TmE:/^3d SAMPLER: Au^
TKokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: S/OCaT-Z..
SITC: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid # 2^ . 5 ft.
PARAMETERS METHOD
%
Cadinium
Chromium
Uad
SUver
Mercury
6010
6010
6010
6010
7470
Perchlorates A .^ ^^ /—, /
DATC: 24 A^-^S 94 TIME: /£Z0 SAMPLER: ^^"^
Thiokol Corporation RCRA FaciUty Investigation
7^5^ WO#: 1B940 LWR#: £7^6 Z 2.
SITC: M-187 Old Drum Storage Area
DESCRDTION: SWMU # 551; Grid # ^ , Surface
PARAMETERS
VolatUe Organics
METHOD
8240
DATC: Z4 A*^ 9^ TIME: /S3^ SAMPLER: F^^
%
Thiokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#: £/C^Z Z.
srre: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid # 4 , Surface
PARAMETCRS
Cadmiimi
Chromium
Uad
SUver
Mercury
Perchlorates
METHOD
6010
6010
6010
6010
7470
IC rerciuorates »»- ^ .
DATC: Z4 Aut. '^i- TIME: /SSS SAMPLER:^ ^
I
•.•V'K
I*;.-"
152
/^40 TKokol Corporation RCRA FaciUty Investigation
WO#:1B940 LWR#:^/^67p
srre: M-187 Old Drum storage Area
DESCRIPTION: SWMU # SSI; Grid # ^ . 2 ft.
PARAMETCRS METHOD
VolatUe Organics g240
TIME: /^AO SAMPLER: AtxJ DATC: Z4Ah^ j9^
Thiokol Corpor^on RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/O^Z 2.
SFTC: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid # 4- , 2 ft.
PARAMETERS
Cadmium
Chromium
Lead
Silver
Mercury
Perchlorates
DATC: T'4 Au^ 'P'f TIME
MEIHOD
6010
6010
6010
6010
7470
IC
••/S^C) SAMPLER :/=C^
t^^ TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £/C^ZZ.
SFre: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid # 4 . 5 ft
PARAMETCRS
VolatUe Organics
METHOD
8240
HATE: 24 Au<^ 94 TIME:/5:^0 SAMPLER: /=iO
TKokol Corporation RCRA FadUty Investigation
W0#; 1B940 LWR#: £'/Oi,2Z.
SFre: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid # 4 ,5 ft.
PARAMETERS
Cadmium
Chromium
Uad
SUver
Mercury
Perchlorates .
DATC: •Z4Akl:f 9^ TIME
METHOD
6010
6010
6010
6010
7470
IC
/^:SZ> SAMPLER: /^^CAJ
-ti>^^
153
//ifyC'^Thiokol Corporation RCRA FacUity Investigation
-i^LL&_ wO#: 1B940 LWR#: S/CbZ Z.
SFTC: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid # C^ , Surface
Ataiy<^/ ^ 5<2^«/
PARAMETCRS
Volatile Organics
METHOD
8240
/4» ^
HATE: Z4 4u^ 94 TIME: -A^^^ SAMPLER: f'uJ
' "^
rolHMe.ir
y^ -AJU ^t
/flh A/aaMa/<-
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: £:/OC>Z 2.
SFTC: M-187 Old Drum Storage Area .
DESCRIPTION: SWMU # 551; Grid # (o , Surface
0
PARAMETCRS
Chromium
Lead
SUver
Mercury
Perchlorates
DATC: i< Ai0f f < TIME
METHOD
6010
6010
6010
6010
7470
/fe>ld*^
: A40^ SAMPLER Fed
>^ i<a^ Thiokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#: ^/O^Z'Z.
SITC: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid # fo , 2 ft.
PARAMETERS
VolatUe Organics
METHOD
8240
^IH- < ^Ari
DATC: 14- AuJCj 9^ TIME:J49'C? SAMPLER: A^
m^
Thiokol Corporation RCRA FadUty Investigation
W0#; 1B940 LWR#: ^/O^Z ^
SFTC: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid # C> . 2 ft.
PARAMETERS
Cadmium
Chromium
Lead
SUver
Mercury
Perchlorates
DATC: ZA-Auf 9^
METHOD
6010
6010
6010
A *•!" Jb7470
y<?ic
TlME:r^^7D SAMPLER: /^
1 .>.'.-•'
154
TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 hmut: £/OijZ T
SFre: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; DUP. Grid # to . Z- ft.
PARAMETCRS
Volatile Organics
METHOD
8240
DATC: 24 Aktf 94 /^
TTME.-A^^O
^
SAMPLER: A^
A J) TKokol Corporation RCRA FadUty Investigation
—jtt^J*^- W0#: 1B940 LWRjf: S^/ObZ "^
1/^7) SFTC: M-187 Old Drum Storage Area J
^*-^-*^^ DESCRIPTION: SWMU # 551; Grid # <b , 5 ft. S//f ^ 3a*vcL
PARAMETCRS
VolatUe Orgamcs
METHOD
8240
/c?
DATC: Z4 ALUS f< TIME: 44 ZO SAMPLER: A^'^
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#:
SFTC: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid #
PARAMETCRS
Cadmium
Chromium
Lead
SUver
Mercury
Perchlorates
<0, 5 ft.
METHOD
6010
6010
6010
6piO
,^70
mc
DATC: Z4 Auf ?«f TmE:j4^ZO SAMPLER: f^uJ
~Zj^J]^^Z^
lltl!F-IUt4lltU|ll»U!U!W..U>|iaiLUlliJPWW«IIJW)W^
155
IZoo On siJK 0-h ll-101 lirutvi z-hM.^f iMrA •/» /h/u/Zch.
I U'-^
y^
>
'f± San ph 110 a-t .^ijyMU '^:S<:f ^ /^JfiQr 3-//^^ f^/y^/cA
l/Jo/i
UJartl_ L
'/^ ^/7Q/ ^Q/t</u /^^y^Cifyy ^/)^jrtl^/t /f/to /^ ^acJ^/c f a<L.
TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/O^.^O
SITC: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid # S"^. Surface
PARAMETCRS
VolatUe Organics
METHOD
8240 9 1^^
DATC: Zi^ Aluef 9f TIME: /rA ^ ^5 SAMPLER: A^//ft^
^
-A-
^# _' /
TKokol Corporation RCRA FaciUty Investigation
WO#: 1B940 LWR#:^/^^2P
SITC: M-187 Old Drum Storage Area ^_
DESCRIPTION: SWMU # 551; Grid # S^ , Surface
PARAMETCRS
Cadmium
Chromium
Uad
SUver
METHOD
6010
6010
6010
6010
7470 ^,^^ Mercury 7470 Ji*..-'
Perchlorates IC^ / -•^^ // i
DATC: 2t Au^ 94 TIME: A$:A^ SAMPLER: r**y/AA
TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^/<S6><^8
SITE: M-187 Old Drum Storage Area r -j-aC
DESCRIPTION: SWMU # 551; lUnse Bhmk Grid # §•% ,o^i^"-T\..
r
<r ^.
h^^-"^' ^
p b'
¥^^
w
PARAMETCRS
VolatUe Organics
METHOD
8240
•P^
A"^) A
VATE:Jl<^ /4ub 9^ TIME: /^^ SAMPLER: AM^
filV'
^%
l1'-
11 >-f
'if^
156
^
7^'
Thiokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#: £/6i:>ZB
SITC: M-187 Old Drum Storage Area ^—
DESCRIPTION: SWMU # 551; Grid # $S , 2 ft.
PARAMETERS
VolatUe Organics
METHOD
8240
HATE: '2(i> Alt^ 99^ TIME:/©^3 SAMPLER: /^/!^
-^
W^ ^-
V
TTUoJto/ Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#: EJO G 2 fc
SFTC: M-187 Old Drum Storage Area ^ ^
DESCRIPTION: SWMU # 551; Grid # I>-^ , 2 ft.
PARAMETCRS METHOD
Cadmium
Chromiuni
Lead
SUver
Mercury
Perchlorates . IQ^ ^
DATC: Z«^ %t^ 94 TIME: /^ ^ 5 SAMPLER
6010
6010
6010
6010
747^1^
..^"^^
TKokol Corporation RCRA FaciUty Investigation
W0#: IB940 LWR#: ^//IA 2©
SFTC: M-187 Old Drum Storage Area ^ ^^^
DESCRIPTION: SWMU # 551; Grid # ^5^ 5 ft.
PARAMETERS
VolatUe Organics
METHOD
8240
HATE: Zb ^^94- TIME: A^ S'e SAMPLER: A^/l^
\
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#; iT/a^ Z,g
SITE: M-187 Old Drum Storage Area _
DESCRIPTION: SWMU # 551; Grid # S^. 5 ft.
PARAMETCRS
Cadmium
Chromium
Lead
SUver
Mercury
Perchlorates
METHOD
6010
6010
6010
6010
7470
fercmorates . IC iX r y^j/
DATC; Z6i> 4ct^ f4 TIME: /3S'& SAMPLER: ^^7>t^
•
157
TKokol Corporatibn RCRA FacUity Investigation
W0#; 1B940 LWR#: ^/^^^C/
SITC: M-187 Old Drum Storage Area -
DESCRIPTION: SWMU # 551; Grid # ^"^ . Surface
7^ ff^ PARAMETERS
VolatUe Organics
METHOD
8240
Sir
DATC: ZG /klf ^f TIME:^^^ SAMPLER: '^W
Thiokol Corporation RCRA FaciUty InvestigaUon
W0#: 1B940 LWR#: ^^^ 2&
SFre: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid # 77. Surface
PARAMETERS METHOD
Hi
Cadmium
Chromium
Lead
SUver
6010
6010
6010
6010
Mercury 7470
Perchlorates IC
DATC: Zo AtJL^ 94 TIME: /3<^> O SAMPLER: /V^*-
/-^
TKokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: £:/0 fe, 28
SITC: M-187 Old Drum Storage Area
DESCRHTIONLSWMU # 551; Grid # /7 . 2 ft.
PARAMETCRS
VolatUe Organics
METHOD
8240
^
#
7»J
,/?''
^ ^
DATC: *^^ /hof y^ TIME: /^ ^^ SAMPLER: 'y^/t-i
#
TKokol Corporation RCRA FaciUty Investigation
W0#: 1B940 LWR#:
SFTC: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid # 7"? . 2 ft.
PARAMETCRS
Cadinium
Chromium
Lead
SUver
Mercury
Perchlorates
METHOD
6010
6010
6010
6010
7470
IC /^y DATC:^^^^^^ TIME: Z;^^ if SAMPLER: y/fU
158
ITTS
TKokol Corporation RCRA FaciUty Investigation
W0#: 1B940 "-^^^^^/^Sfi
SFTC: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid # 97, 5 ft.
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC: '^0Atl4 44^ TIME: i^Z ^ SAMPLER: ^/ AAlCi
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^//^^Z&
SITC: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid # f 7' ^ ft-
PARAMETERS
Cadmium
Chromiuxn
Uad
SUver
Mercury
METHOD
6010
6010
6010
6010
7470
Perchlorates . IC /u//^ .
DATE: Z/oA*^ ^4 TIME: 7.:^^ 5- SAMPLER:^ /-«>*>
TKokol Corporation RCRA FacUity Investigation
W0#; 1B940 LWR#; ^^S>0
SFTC: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; DUP. Grid # 77 . J^ ft
PARAMETCRS
Cadmium
Chromium
Uad
SUver
Mercury
Perchlorates
METHOD
6010
6010
6010
6010
7470
IC A^^/
DATE:^^A^f6, 9A TTME:A^^^ SAMPLER: ^^^
-1^
Thiokol Corporation RCRA FacUity Investigation
W0#; 1B940 LWR#: ^0^2&
SFTC: M-187 Old Drum Storage Area ^^
DESCRIPTION: SWMU # 551; Grid # t^^ . Surface
PARAMETCRS
VolatUe Organics
METHOD
8240
O—
^>^
^
P'
DATC: 26 /kl*7 ^ TIME: /^-^ ^ SAMPLER: ^^^AuS
p-{
TKokol Corporation RCRA FacUity Investigation
WO#: 1B940 LWR#: ^0^Z&
SITC: M-187 Old Drum Storage Area _,
DESCRIPTION: SWMU # 551; Grid # ffS . Surface
PARAMETERS
Cadmium
Chromium
Lead
SUver
Mercury
Perchlorates .
METHOD
6010
6010
6010
6010
7470
IC
159
DATC: Z/b Aaf 94 TIME: A^>'=> SAMPLER -."Ykj
T^ ^ ?"
#
Thiokol Corporation RCRA FacUity Investigation
W0#: 1B940 LWR#: ^^^22>
SFTC: M-187 Old Drum Storage Area ^
DESCRIPTION: SWMU # 551; Grid # <^8 .2 ft.
PARAMETCRS
VolatUe Organics
METHOD
8240
DATC: 7(; /klf 9^ TIME: /:^3 i>"" SAMPLER: >^. ^'
t^^-/^^
,^ ;^
xT
^
-^-
Thiokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#: ^/C^t 3^
SITE: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid # ff2> , 2 ft.
PARAMEIERS
Cadmium
Chromium
Lead
SUver
Mercury
Perchlorates. *
DATE: *^6 /^ <)6/ TIME:
METHOD
6010
6010
6010
6010
7470
'S^'T'l
71f«
#
J] ^ TAioto/ CorporatiAh RCRA Facttity Investigation
W0#: 1B940 LWR#: Bf^^Z^
SITE: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid # .£^, 5 ft.
PARAMETCRS
VolatUe Organics
METHOD
8240
-^fc
^--fc
^W v^
^~
DATC: ? C? A^ <f ^ TIME: /;^><? SAMPLER: /lA^
160
TKokol Corporation RCRA FacUtty Investigation
W0#: IB940 LWR#: ^/C^-Z^
SFTC: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Grid # S8 , 5 ft
PARAMETERS
Cadmium
Chromium
Uad
SUver
Mercury
Perchlorates ,
\>ATE:Zjb AfU<i 9f
METHOD
6010
6010
6010
6010
7470
IC
TIME: /3^ii> SAMPLER /v^
# r Thiokol Corporation RCRA FadUty Investigation
W0#: 1B940 LWR#: ^/£>(PZS
SITE: M-187 Old Drum Storage Area
DESCRIPTION: SWMU # 551; Ruise Blank Grid # <^>. S~ft.
PARAMETERS
Cadmium
Chromium
Lead
SUver
Mercury
Perchlorates ^
DATC: 'Zk>Auf(9^ TIME:
METHOD
6010
6010
6010
6010
7470
IC ^ f.
/4^i SAMPLER: ^A 7/u-J
^JUMiiU
ENVIRONMENTAL LAB WORK REQUEST
^AAPJ^X
kP" TfflOKOL ENVIRONMENTAL LABORATORY
nOM:
ORGANIZATION
^NlAilZO ^/uaR_
KXIVSION
S390
MAIL STOP
LWR No. E10388
OOSTCBNTBK
V400
WORK ORDBR
IB94A)
DATC
2Z-MAR-94
REPOBT IBSULTS TOl
HELEN WARD, MS 301
1/
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SAMPLE
1. 5WM0 43a
Pf */ i»^ , SoE.
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141 ft Dn &raJ. ?6
Pfcf-Vri. ZU
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12SOMO 26>/f433
DATE
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TYPE
6
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SAMPLE INFORMATION
LOCATION
/^-^i.
/K'^6
M'6>C^
A^^6(^
M'TQ^
M-7Z.
M'72.
M'7Z.
M'^r
^'C7
M'C7
44-67
TIME
/3^^
/5'>'5-
/i-rs^
/33e>
1344
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TEST
U,ad
lead.
L£Qd,
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Li:a</.
/j^aJ
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/^aJ.
/ufocA.
Aeae/,
AiroJ,
IjTOe/ ,
1 P^
Pff
pf/
iP//
of/-
Pf^
Pff
P^
7/f
F^
p/^
P^
REMAKICS
?b 'i>0/D p\ M
CHAIN OF CUSTODY
RfXINQinSHED BY DATE TIME KECEIVED BY DATE TIME
-^umiL tz-/,m-94 ^//"' (SIO /i^//Mf,1rt,. '^X- 9 5^ / T/c?
4
FOR LABORATORY USE ONLY
DATC COMPLETED DATCKEPORTCD nCNATVBE
ENVIRONMENTAL LAB WORK REQUEST ^^J^>z-
"• TfflOKOL ENVIRONMENTAL LABORATORY
fBOMi
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RBPORT RmULTB TOi
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TTME TTSST REMARKS
DoF
\y
•^ M'G7
T.'Sutmo 07* ire
/440 UaJ, p^ n-U>IO y//-f^^
2lMAr9^ >/ /U'I4KI i M'14--^ l^'zo ^c/eAiOM , TM///'"*^ / P^ (t>t>IO 'pli-%4i '
i^u)M tsrf no
?ro(Dn. 2 ft ilMtrff M'/4t/ ^ H'I4-S /^Z€ ^/jAion^, TMoAivfh. , pH
timcr^4 M'I4^ ^ /U-IA-'S. /€^^ Se/r4/VM , 7kQ///i>M> , pH-
^L
»^ M-l^-U t M'li-'^ /53e StlemotU^ . TAC//(OM^. pff
xt
Vr&yU \(r
M»rtlf
ir^ M'14'V P AA-/4-5 /rsg Ss/^/tfVM ^ Tkaf/iof^ , pf^
CHAIN OF CUSTODY
KFIJNQUISHES BY
\Q^(.kAl.^
DATE
zz-liAt-^
TIME
/^IL'
SECQVBJBY
/A/YAy.A7^^..^ .^
DATE
-J -:LX-9y^
TIME
/Z/O
FOR LABORATORY USE ONLY
DATCOOMFLEIBI nAIS REPORTBI SIGNATinB
May 9, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 1
#
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER. M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order # 9403025 Sample and Test Code Identification
LabID: Sample ID:
OIA M-*6;Fr OF DIS. SURFACE
Test Codes and Names
PB_AE2 Lead
PH_S pH (Soil)
Method
sw-846, 6010
SW-846,9045A
Lab ID: Sample ID:
02A M-66;PT OF DIS. 2 FT.
Test Codes and Names
PB_AE2 Lead
PH_S pH (Soil)
Method
sw-846, 6010
SW-846,9045A
Lab ID: Sample ID:
03A M-66;141 FT DN GRAD SUR.
Test Codes and Names
PB_AE2 Lead
PH_S pH (Soil)
Method
SW-846, 6010
SW-846,9045A
04A
it LabID:
O^A
Sample ID:
M-66; 141 FT DN GRAD 2 FT.
Sample ID:
M-72;Pr OF DIS SURFACE
Test Codes and Names
PB_AE2 Lead
PH_S pH (Soil)
Test Codes and Names
PB_AE2 Lead
PH_S pH (Soil)
Method
SW-846, 6010
SW-846,9045A
Method
sw-846, 6010
SW-846,9045A
Lab IDl Sample ID:
06A M-72;PT OF DIS 2 FT.
Test Codes and Names
PB_AE2 Lead
PH_S pH (Soil)
Method
SW-846, 6010
SW-846,9045A
Lablp: Sainple ID:
07A M-72; 195 FT DN GRAD SUR.
Test Codes and '^'Jamr.s
PB_AE2 Lead
PH_S pH (SoU)
Method
SW-846, 6010
SW-846,9045A
LabID: Sample ID:
08A M-72; 195 FT DN GRAD 2 FT.
Test Codes and Names
PB AE2 Lead
PH"S pH (Soil)
Method
sw-846, 6010
SW-846,9045A
Lab IDl Sample ID:
09A M-67;PT OF DIS SURFACE
Test Codes and Names
PB_AE2 Lead
PH_S pH (Soil)
Method
sw-846. 6010
SW-846,9045A
Lab ID: Sample ID:
IOA M-67;FT OF DIS 2 FT.
Test Codes and Names
PB_AE2 Lead
PH_S pH (SoU)
Method
sw-846, 6010
SW-846,9045A
0 Lab ID: Sample ID:
11A M-67;25 FT DN GRAD SUR.
Test Codes and Names
PB_AE2 Lead
PH_S pH (Soil)
Method
SW-846, 6010
SW-846,9045A
LabID: Sample ID:
12A M-67;25 FT DN GRAD 2 FT.
Test Codes and Names
PB_AE2 Lead
PH_S pH (Soil)
Method
SW-846, 6010
SW-846,9045A
LabID: Sample ID:
13A M-67;25 FT DN GRAD SUR DUP
Test Codes and Names
PB_AE2 Lead
PH_S pH (Soil)
Method
SW-846, 6010
SW-846,9045A
Lab ID: Sample ID:
14A M-14;PT OF DIS SURFACE
Test Codes and Names
SE_GF2 Selenium
TL_GF2 Thallium
PH_S pH (Soil)
Method
sw-846, 7740
SW-846, 7841
SW-846,9045A
LabID: Sample ID:
ISA M-14;PTOFDIS2FT.
Test Codes and Names
SE_GF2 Selenium
TL_GF2 Thallium
PH S pH (Soil)
Method
sw-846, 7740
SW-846, 7841
SW-846,9045A
LabID: Sample ID:
16A M-14;25 FT DN GRAD SUR.
Test Codes and Names
SE_GF2 Selenium
TL_GF2 Thallium
PH_S pH (Soil)
Method
SW-846, 7740
SW-846, 7841
SW-846,9045A
LabID: Sample ID:
17A M-14;25 FT DN ORAD 2 FT.
Test Codes and Names
SE_aF2 Selenium
TL GF2 Thallium
PHlS pH (Soil)
Method
sw-846, 7740
SW-846, 7841
SW-846,9045A
Lab ID: Samplft ID:
18A M-14;25 FT DN GRAD 2FT.DUP
Test Codes and Names
SE_GF2 Selenium
TL_GF2 Thallium
PH S pH (Soil)
Method
SW-846, 7740
SW-846, 7841
SW-846,9045A
Workorder Comments
This is to cenify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: M-66;PT OF DIS. SURFACE Lab ID: 9403025-OlA CoUected: 03/21/94 13:00:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Lead
pH (Soil)
11.5 ug/g
8.05 pH Unit
1.6 04/12/94 LVD
03/23/94 AA
SW-846, 6010
SW-846,9045A
Sample ID: M-66;PT OF DIS. 2 FT. LabID: 9403025-02A CoUected: 03/21/94 13:15:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Lead
pH (Soil)
5.04 ug/g
8.05 pH Unit
0.76 04/12/94 LVD
03/23/94 AA
SW-846, 6010
SW-846,9045A
Sample ID: M-66; 141 FT DN GRAD SUR. LabID: 9403025-03A CoUected: 03/21/94 13:25:00
w RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Lead
pH (Soil)
10.8 ug/g
8.73 pH Unit
1.1 04/12/94 LVD
03/23/94 AA
SW-846, 6010
SW-846,9045A
Sample ID: M-66; 141 FT DN GRAD 2 FT. Lab ID: 9403025-04A CoUected: 03/21/94 13:30:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Lead
pH (Soil)
12.3 ug/g
11.02 pH Unit
1.2 04/12/94 LVD SW-846, 6010
03/23/94 AA SW-846,9045A
Sample ID: M-72;PT OF DIS SURFACE Lab ID: 9403025-05A CoUected: 03/21/94 13:44:00
TEST RESXTLT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Lead
#
Soil)
9.04
7.97
ug/g
pH Unit
1.1 04/12/94
03/23/94
LVD
AA
SW-846, 6010
SW-846,9045A
May 9, 1994 12:23 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 2
Sample ID: M-72;PT OF DIS 2 FT. LabID: 9403025-06A CoUected: 03/21/94 13:50:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Lead
pH (Soil)
4.64 ug/g
7.94 pH Unit
0.64 04/12/94 LVD
03/23/94 AA
SW-846, 6010
SW-846,9045A
Sample ID: M-72; 195 FT DN GRAD SUR. Lab ID: 9403025-07A CoUected: 03/21/94 14:00:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Lead
pH (Soil)
10.7 ug/g
7.92 pH Unit
1.3 04/12/94 LVD
03/23/94 AA
SW-846, 6010
SW-846,9045A
Sample ID: M-72; 195 FT DN GRAD 2 FT. Lab ID: 9403025-08A CoUected: 03/21/94 14:05:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Lead
pH (Soil)
11.9
8.52
ug/g
pH Unit
1.4 04/12/94
03/23/94
LVD
AA
SW-846, 6010
SW-846,9045A
Sample ID: M-67;PT OF DIS SURFACE Lab ID: 9403025-09A CoUected: 03/21/94 14:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Lead
pH (Soil)
5.78 ug/g
8.12 pH Unit
0.85 04/14/94 LVD
03/23/94 AA
SW-846, 6010
SW-846,9045A
Sample ID: M-67;PT OF DIS 2 FT. Lab ID: 9403025-lOA CoUected: 03/21/94 14:28:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Lead
pH (Soil)
8.16 ug/g
7.77 pH Unit
1.1 04/14/94 LVD
03/23/94 AA
SW-846, 6010
SW-846,9045A
May 9, 1994
SSK
12:23 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 3
pie ID: M-67;25 FT DN GRAD SUR. LabID: 9403025-11A CoUected: 03/21/94 14:40:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Lead
pH (Soil)
10.2 ug/g
7.96 pH Unit
1.3 04/14/94 LVD
03/23/94 AA
SW-846, 6010
SW-846,9045A
Sample ID: M-67;25 FT DN GRAD 2 FT. LabID: 9403025-12A CoUected: 03/21/94 14:45:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Lead
pH (Soil)
7.65 ug/g
7.82 pH Unit
1.2 04/14/94 LVD SW-846, 6010
03/23/94 AA SW-846,9045A
Sample ID: M-67;25 FT DN GRAD SUR DUP Lab ID: 9403025-13A CoUected: 03/21/94 14:40:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/C:AS#
Lead
pH (Soil)
7.92
8.06
ug/g
pH Unit
1.7 04/14/94 LVD SW-846, 6010
03/23/94 AA SW-846,9045A
Sample ID: M-14;PT OF DIS SURFACE LabID: 9403025-14A CoUected: 03/21/94 15:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METH0D/CAS#
Selenium
Thallium
pH (Soil)
0.54 ug/g
0.23 ug/g
9.79 pH Unit
0.2 05/04/94 CRS
0.2 05/04/94 CRS
03/23/94 AA
SW-846, 7740
SW-846, 7841
SW-846,9045A
Sample ID: M-14;PT OF DIS 2 FT. LabID: 9403025-15A CoUected: 03/21/94 15:25:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
w
rSVi]
nlum
Hum
0.50
0.30
ug/g
ug/g
0.2
0.2
05/04/94
05/04/94
CRS
CRS
SW-846,
SW-846,
7740
7841
May 9, 1994 12:23 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 4
Sample ID: M-14;PT OF DIS 2 FT. Lab ID: 9403025-15A CoUected: 03/21/94 15:25:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
pH (Soil) 8.15 pH Unit 03/23/94 AA SW-846,9045A
Sample ID: M-14;25 FT DN GRAD SUR. Lab ID: 9403025-16A CoUected: 03/21/94 15:32:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Selenium
Thallium
pH (Soil)
0.29 ug/g
U ug/g
10.13 pH Unit
0.2 05/04/94 CRS
0.2 05/04/94 CRS
03/23/94 AA
SW-846, 7740
SW-846, 7841
SW-846,9045A
Sample ID: M-14;25 FT DN GRAD 2 FT. LabID: 9403025-17A CoUected: 03/21/94 15:38:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Selenium
Thallium
pH (Soil)
0.33
0.39
8.47
ug/g
ug/g
pH Unit
0.2
0.2
05/04/94
05/04/94
03/23/94
CRS
CRS
AA
SW-846, 7740
SW-846, 7841
SW-846,9045A
Sample ID: M-14;25 FT DN GRAD 2FT.DUP Lab ID: 9403025-18A CoUected: 03/21/94 15:38:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/C:AS#
Selenium
Thallium
pH (Soil)
0.82 ug/g
0.36 ug/g
8.71 pH Unit
0.2 05/04/94 CRS
0.2 05/04/94 CRS
03/23/94 AA
SW-846, 7740
SW-846, 7841
SW-846,9045A
•
#
m
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates coinpound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identiiication cnteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1.1J with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instmment.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ENVIRONMENTAL LAB WORK REQUEST
^^/<*^/^
™' TfflOKOL ENVmONMFNTAL LABORATORY
IKOMi
o>GA^azA'^ON
KcnaaioH trsfo
UAO-mr
3c/^
LWR No. £10390 d
ooncwm
l/^O
WQKKOBim
IS940 'ZO A/AS. 94
RBPOBT IBHILTR TOl 11
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEBT KEMARKS
\y iCit^t^f^ 1/ Al-63 6P ttco <^. ^f • ^^
i^ Ztu>^'f{-/lA-^Z' SP /{CO
VCf. - 924^)
ucric
&2^70
?tJMAR»Ji 1/ AA-S3'BP /OiO
ctfvc
74.70 •pfg-- 9C4<-
lA
3c<Me» /A'^3'&? iOlo ez4^
r^ -Q2aSL
i^ AI-65-6P //;^6 'i:^. p"-^°4r
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CHAIN OF CUSTODY
REUNQUISHEDBY
AJ/yJ/jyfif^
DATE
30-/1tf/"?^
TIME
/4z^
KECEIVED BY
/Y^//A^^.^
DATE
7/A/1ifif^9^
TIME
A^^'-S-
FOR LABORATORY USE ONLY
DATsamffLEnD •UnBEKMnSD i
ENVIRONMENTAL LAB WORK REQUEST ^^^/^ J ^
THIOKOL ENVIRONMENTAL LABORATORY f/0690 CON7 p^.z
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•BOBT UBULIS TOl
HELEN WARD, MS 301
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SAMPLE INFORMATION
SAMPLE
25' r>id G1KAX5
5.
i.
7.
t.
9.
IL
11.
12.
DATE
V-J
)40
7. ^OA
TYPE
G
"^
•
C
LOCATION
AA-55-B f /U-S-c
/(A-3S-B*^-^3<
M-^ 5-B* Mli
M-l3-'P y^-ijc
-
TIME
/S-^fi
/5f^
/ii-S
H^Z.
TEST REMARKS
/»
</
//
CHAIN OF CUSTODY
SEUNQUISHED BY DATE TIME •BCHVEDBY DATE TIME
l^/U-^ 2o'4iac^4 /4t<r AA
^ ^,£^^^ ^ ^/Py^^9^ A^^^
FOR LABORATORY USE ONLY
MncOMTLnBD MIS BHPUHIU
m
June 17, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page l
# SENT Environmemal Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER. M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty. Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order # 9403036 Sample and Test Code Identification
LabID: Sample ID:
OIA M-53BP;PT OF DIS. SURFACE
Test Codes and Names
CD_AE2 Cadmium
HG CV2 Mercuty
PH~S pH (SoU)
Method
SW-846, 6010
SW-846, 7471
SW-846,9045A
LabID: Sample ID:
02A M-53BP;Pr OF DIS. SURFACE
Test Codes and Names
8240 VoUtile Oiganica
8270 Semi-VoUtile Orgtnici
Method
sw-846, 8240
SW-846, 8270
LabID: Sample ID:
03A M-53BP;Fr OF DIS. 2 FT.
Test Codes and Names
CD AE2 Cadmium
H0~CV2 Mercury
PH_S pH (Soil)
Method
SW-846, 6010
sw-846, 7471
SW-846,904SA
#
LabID: Sample ID;
~54A M-53BP; PT OF DIS. 2 FT.
Test Codes and Names
8240 VoUtile Organics
8270 Semi-Volatile Organica
Method
sw-846, 8240
SW-846, 8270
LabID: SamplelD:
~05A M-53BP;15FT DN GRAD SUR.
Test Codea And Names
CD AE2 Cadmium
HG~CV2 Mercury
PH~S pH (SoU)
Method
sw-846, 6010
SW-846, 7471
SW-846,9045A
LabID: Sample ID:
~5SA M-53BP;15 FT DN GRAD SUR. 8240 8270
Test Codes antl Names
VoUtiie Otganica
Semi-VoUSe Organica
Method
SW-846, 8240
SW-846, 8270
LabID: Sample ID:
07A M-53BP;15 FT DN GRAD 2 FT.
Test Codes and Names
CD AE2 Cadmium
HG~CV2 Mercury
PH~S pH (Soil)
Method
SW-846, 6010
SW-846, 7471
SW-846,904SA
LabID: Sample TD;
OSA M-53BP;15 FT DN ORAD 2 FT.
Test Codes and Names
8240 VoUtile Organics
8270 Semi-VoUtile Oiganica
Method
SW-846, 8240
SW-846, 8270
LabID:
~59A
LabID:
IOA
#
pie ID:
M-53E; PT OF DIS SURFACE
Sample TD:
M-53E; PT OF DIS 2 FT.
8240
8240
Test Codes and is^ames
VoUtile Organics
Test Codes and Names
VoUtile Organics
Method
SW-846, 8240
Method
SW-846, 8240
LabID:
llA
LabID:
~I2A
LabTO:
^lelD:
M-53E; 25 FT DN ORAD SUR.
Jle ID:
M-53E; 25 FT DN ORAD 2 FT.
13A M-33B&C;Pr OF DB SURFACE
LabID: SamplelD:
14A M-33B&C;PT OF DIS 2 FT.
LabID: Sample ID:
15A M-33B&C;25 FT DN GRAD SUR.
LabID: SamplelD:
16A M-33B&C;25 FT DN GRAD 2 FT
Test Codes and Names
8240 VoUtile Organics
Test Codes and Names
8240 VoUtile Organics
T&st Codea and Namivi
SB_AE2 Antimony CD AE2 Cadmium PHJS pH (Soil)
Test Codes and Names
SB AE2 Antimony
CD AE2 Cadmium
PHjS pH (SoU)
Test Codes and Names
SB_AE2 Antimony
CO AE2 Cadmium
PH_S pH (SoU)
Test Codes and Names
SB_AE2 Antimony
CD AE2 Cadmium
PH_S pH (SoU)
>
Wnrknrdar Cnmmt^nis
Method
sw-846, 8240
Method
sw-846, 8240
Method
sw-846, 6010
sw-846, 6010
SW-846,9045A
Method
SW-846, 6010 SW-846, 6010 SW-846,9045A
Method
sw-846. 6010 SW-846, 6010 SW-846,9045A
Method
SW-846. 6010
SW-846, 6010
SW-846.9045A
Rqwrt: The surface samples for semi-voIatUe orgamc analyses were
received contaminated with asphalt from paving activity
rendering the samples unusable. Clean re-samples are required
to complete analyses by Method 8270.
#
This is to cenify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: M-53BP;PT OF DIS. SURFACE LabID: 9403036-OlA CoUected: 03/30/94 10:00:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Cadmium
litorcury
pH (Soil)
0.452 ug/g
2.47 ug/Kg
7.54 pH Unit
0.1 05/05/94 LVD
0.010 04/22/94 CRS
03/31/94 AA
SW-846, 6010
SW-846, 7471
SW-846,9045A
Sample ID: M-53BP;PT OF DIS. SURFACE Lab ID: 9403036-02A CoUected: 03/30/94 10:00:00
TEST
Volatila Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichioromethane
Broinoform
^[Romomethane
^ Huteuione
(Carbon disulfide
Carbon tetrachloride
iZhlorobenzene
iZhloroetheUie
2-Chloroethylvinyl ether
iZhloroform
Chlorometheuie
Dibromochlorometheme
1,1 -Dichloroethcuie
1,2 -Dichloroetiheune
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2 -Dichloropropeuie
cis-1,3-Dichloropropene
treuis -1,3 -Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
il^L chlorof luoromethauie
|Hyl Acetate
v&yl Chloride
RESULT
8 J
U
U
U
U
U
U
U
D
D
U
D
U
U
U
U
U
U
U
D
U
U
D
U
U
U
U
U
U
D
U
U
O
U
3 JB
U
U
U
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
50
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
ANALYZED
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
June 17, 1994 14:21 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 2
Sample ID: M-53BP;PT OF DIS. SURFACE Lab ID: 9403036-02A CoUected: 03/30/94 10:00:00 •
TEST
Volatile Organics
o-Xylene
Bromochloromethane
1,4-Difluorobenzene
Chlorobenzene-d5
RESULT
D
215839
971473
776753
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
ANALYZED
04/01/94
04/01/94
04/01/94
04/01/94
BY
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene
Bromofl
-d8
uorobenzene
1,2-Dichloroethane-d4
Seal-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2 -Methylphenol
bis(2-chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis (2 -CSiloroethoxy) methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
%Racovery
98.6
99.1
93.9
1.5
10
10
5.7
3.3
1.9
4.4
4.6
1.9
2.3
5.7
4.0
12
1.6
1.4
2.2
3.6
2.7
3.4
5.3
2.7
1.9
1.6
1.8
0.90
3.0
2.2
6.0
2.7
4.0
1.9
1.5
1.6
3.5
2.4
1.9
42
2.4
3.0
1.9
5.7
1.9
METHOD/CAS*
SW-846, 8240
95-47-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
88
86
76
TO 110
TO 115
TO 114
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1 ^^
95-48-7 ^B
108-60-1 ^^
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2 ^^
121-14-2 ^B
84-66-2 ^^
June 17, 1994 14:21
^m
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 3
pie ID: M-53BP;I»T OF DIS. SURFACE Lab ID: 9403036-02A CoUected: 03/30/94 10:00:00
TEST
Semi-Volatile Organics
4 -Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
n-Nitrosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo [a] euithracene
bis(2-Ethylhexyl)phthalate
Chyrsene
Di-n-octylphthalate
Benzo[b&k]fluoranthene
Benzo[a]pyrene
Indeno[1,2,3 -cd]pyrene
Dibenz [a,hj euithracene
Jl^zo [g, h, i] perylene
• ^^ - Di chlorobenzene - d4
Waphthalene-d8
.^Acenaphthene - dl 0
Pheneuithrene - dl 0
Chyrsene-dl2
Perylene-dl2
RESULT UNITS DETECTION ANALYZED BY
Int.
Int.
Int.
Int.
Int.
Int.
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Std.
Std.
Std.
Std.
Std.
Std.
LIMIT
4.2
1.9
3.6
24
1.9
1.9
1.9
3.6
5.4
1.9
2.5
2.2
1.9
2.5
7.8
2.5
2.5
2.5
4.8
2.5
3.7
2.5
4.1
METHOD/CAS#
SW-846, 8270
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
-
-
-
-
-
-
Surrogate/Recovery Data For Seml-Volatlla Organics 8270
Surrogate
2 - FliUOROPHENOL
Phenol-d5
Nitrobenzene-d5
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
%Racovery
Q
Q
Q
Q
Q
Q
Racovary Limits
21 TO 100
10 TO 94
35 TO 114
43 TO 116
10 TO 123
33 TO 141
Sample ID: M-53BP;PT OF DIS. 2 FT. LabID: 9403036-03A CoUected: 03/30/94 10:10:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Cadmium
Mercury
(Soil) #
0.469 ug/g
0.161 ug/g
7.42 pH Unit
0.1 05/05/94 LVD
0.016 04/22/94 CRS
03/31/94 AA
SW-846, 6010
SW-846, 7471
SW-846,9045A
June 17, 1994 14:21 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 4
Sample ID: M-53BP; PT OF DlS. 2 FT. LabID: 9403036-04A CoUected: 03/30/94 10:10:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butcmone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2 -Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,l-Dichloroethene
2-Hexanone
treuis-1,2 -Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloroprqpene
trsms-l,3-Dichloropropene
1,2 -Dichlorolaenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2-Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1 -Trichloroethane
1,1,2 -Trichloroetheuie
Trichloroethene
Tri chlorof luoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
Bromochloromethane
1,4-Difluorobenzene
Chlorobenzene-d5
RESULT
0
a u u D
D
u u u D
D
U
u
2 J
a D
n D
D
u u u
u
u
u u D
u
u u D
u u u 10 B
u a u u u
u 203737
922450
750464
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ua/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
50
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene-d8
Bronofluorobenzene
1,2
Seal-Volatile Organics
Phenol
Pyridine
-Dichloroethane-d4
U
U
ug/Kg
ug/Kg
%Recovery
100
102
91.6
10
10
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5 ^^
10061-02-6 ^B
95-50-1 ^^
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
88
86
76
04/13/94
04/13/94
TO 110
TO 115
TO 114
MMR
MMR
SW-846, 8270 ^
108-95-2 ^B
110-86-1 ^W
June 17, 1994 14:21
ISan
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 5
ample ID: M-53BP; PT OF DIS. 2 FT. LabID: 9403036-04A CoUected: 03/30/94 10:10:00
TEST
Seal-Volatile Organics
.ftniline
bis(2-Chloroethyl)ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroetheme
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
I^Chloroamiline
^ Bcachlorobutadiene
1| Hchloro - 3 - methylphenol
Z-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2 -CSiloronaphthalene
2-Nitroemiline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran 2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methyIphenol
n-Nitrosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenemthrene
Anthracene
Di•n-butylphthalate
Fluoranthene
Pyrene
ilBtylbenzylphthalate
tHPizo [a] anthracene Bis(2-Ethylhexyl)phthalate
RESULT
U
D
U
U
U
U
U
D
U
U
U
D
D
U
U
U
U
U
U
U
U
D
D
D
D
U
D
U
U
U
D
U
U
U
U
D
U
U
U
0
U
D
U
U
D
U
U
U
D
D
120 B
U
D
O
U
620 B
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
20
10
10
10
10
10
10
10
10
10
10
50
10
10
10
10
20
10
20
10
10
10
10
10
50
10
10
50
10
50
50
10
10
10
10
10
10
20
50
10
10
10
50
10
10
10
10
10
10
10
10
ANALYZED
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMU
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
June 17, 1994 14:21 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 6
Sample ID: M-53BP; PT OF DIS. 2 FT. LabID: 9403036-04A CoUected: 03/30/94 10:10:00
TEST
Semi-Volatile Organics
Chyrsene
Di-n-octylphthalate
Benzo[b&k]fluoremthene
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h] emthracene
Benzo[g,h,i]perylene
1,4 -Dichlorobenzene-d4
Naphthalene-d8
Acenaphthene-dl0
Phenanthrene-dl0
Chyrsene-dl2
Perylene-dl2
2
RESULT
Int.
Int.
Int.
Int.
Int.
Int.
U
U
U
U
U
a U
Std.
Std.
Std.
Std.
Std.
Std.
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
-FLUOROPHENOL
Phenol-d5
Nitrobenzene-dS
2
2
T
-Fluorobiphenyl
'
,4,6-Tribromophenol
erphenyl -dl4
DETECTION
LIMIT
10
10
10
10
10
10
10
ANALYZED
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
-
-
-
-
-
-
For Seal-Volatile Organics 8270
%Recovery
50
55
57
61
68
83
.52
.05
.17
.24
.08
.61
Recovery Llalts
21
10
35
43
10
33
TO 100
TO 94
TO 114
TO 116
TO 123
TO 141
^^^
^^1
Sample ID: M-53BP;15 FT DN GRAD SUR. Lab ID: 9403036-05A CoUected: 03/30/94 10:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Cadalua
Mercury
pH (Soil)
D ug/g
0.316 ug/g
7.72 pH Unit
0.1 05/05/94 LVD
0.021 04/22/94 CRS
03/31/94 AA
SW-846, 6010
SW-846, 7471
SW-846,9045A
Sample ID: M-53BP;15 FT DN GRAD SUR. LabID: 9403036-06A CoUected: 03/30/94 10:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromofonn
D
D
D
D
D
D
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
50
10
10
10
10
10
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
June 17, 1994 14:21
#
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 7
Sample ID: M-53BP;15 FT DN GRAD SUR. Lab ID: 9403036-06A CoUected: 03/30/94 10:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2 -Chloroethylvinyl ether
Chlorofonn
Chlorometheme
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroetheme
1,l-Dichloroethene
2-Hexemone
trems-1,2-Dichloroethene
1,2-Dichlorpprppane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
J^hy Ibenzene
JBhylene Chloride
HPftethyl - 2 - Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Tri chlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
Bromochlorometheme
1,4-Difluorobenzene
Chlorobenzene-dS
3
n
U
U
D
U
U
U
O
U
U
U
n u u u u
u u u D
u u BJ
u u D
D
u 10 B
u D
u
u u
u 209132
959151
764974
Surrogat
Surrogate
Toluene-d8
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
e/Recovery Data
Bromofluorobenzene
1,2
Seal-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2 -Chlorophenol
i(l|| -Dichlorobenzene
IjHI -Dichlorobenzene
Benzyl Alcohol
-Dichloroetheme-d4
NT
NT
NT
NT
NT
NT
NT
NT
10
50
10
10
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240
%Recovery
98.9
98.7
93.5
1.5
10
10
5.7
3.3
1.9
4.4
4.6
SW-846, 8240
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
INTSTDl
INTSTD2
INTSTD3
Recovery Llalts
88
86
76
TO 110
TO 115
TO 114
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
June 17, 1994 14:21 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 8
Sample ID: M-53BP;15 FT DN GRAD SUR. Lab ID: 9403036-06A CoUected: 03/30/94 10:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Seal-Volatile Organics
1,2-Dichlorobenzene
2-Methylphenol
bis(2-chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroetheme
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis (2 -CSiloroethoxy) methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4 -Chloroani1ine
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofurem
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
n-Nitrosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
bis(2-Ethylhexyl)phthalate
Chyrsene
Di-n-octylphthalate
Benzo[b&k]fluoranthene
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h] emthracene
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
1.9
2.3
5.7
4.0
12
1.6
1,
2.
3,
2.
3,
5.
2.
1.9
1.6
1.8
0.90
3.0
.4
.2
.6
.7
.4
.3
.7
2
6.
2
4.
1.9
1.5
1.6
3.5
2.4
1.9
42
2.4
.0
.9
.7
.9
.2
.9
.6
24
1.9
1.9
1.9
3,
1.
5.
1.
4.
1.
2.
3,
5.
1,
2.
2.
1.
2.
7.
2.5
2.5
2.5
4.8
2.5
3.7
2.5
SW-846, 8270
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7 .
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
June 17, 1994 14:21 CERTIFICATE OF ANALYSIS
RESULTS BY SAIMPLE
Page 9
sKni pleID:M-53BP;l5FTDNGRADSUR. Lab ID: 9403036-06A CoUected: 03/30/94 10:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Seal-Volatile Organics
Benzo[g,h,i]perylene
1,4 -Dichlorobenzene-d4
Naphthalene-d8
Acenaphthene-dl0
Phenemthrene-dlO
Chyrsene-dl2
Perylene-dl2
NT 4.1
Int. Std.
Int. Std.
Int. Std.
Int. Std.
Int. Std.
Int. Std.
19
-
-
-
-
-
-
Surrogate/Recovery Data For Seal-Volatile Organics 8270
Surrogate %Racovary
2-FLUOROPHENOL Q
Phenol-d5 Q
Nitrobenzene-d5 Q
2 -Fluorobiphenyl Q
2,4,6-Tribromophenol Q
Terphenyl-dl4 Q
Recovery Llalts
21 TO 100
10 TO 94
35 TO 114
43 TO 116
10 TO 123
33 TO 141
SW-846, 8270
191-24-2
m pleID:M-53BP;15FrDNGRAD2FT. LabID: 9403036-07A CoUected: 03/30/94 10:45:00
RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Cadalua
Mercury
pH (Soil)
0.203
0.154
9.58
ug/g
ug/g
pH Unit
0.1
0.0063
05/05/94
04/22/94
03/31/94
LVD
CRS
AA
SW-846, 6010
SW-846, 7471
SW-846,9045A
SampleID:M-53BP;15FTDNGRAD2Fr. LabID: 9403036-08A CoUected: 03/30/94 10:45:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/C:AS#
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromoform
Bromometheme
2-Butemone
Carbon disulfide «rbon tetrachloride
lorobenzene
[oroethane
u
u u u u u u u u u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
50
10
10
10
10
10
10
50
10
10
10
10
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
June 17, 1994 14:21 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
PagelO
SampleID:M-53BP;15FrDNGRAD2FT. LabID: 9403036-08A CoUected: 03/30/94 10:45:00
TEST
Volatile Organics
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroethane
1,l-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trems-l,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Tri chlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
Bromochlorometheme
1,4-Difluorobenzene
Chlorobenzene-d5
RESULT
D
2.5 J
D
u U
U
U
U
U
U
D
U
U
U
U
U
U
U
o
U
U
U
11 B
U
U
U
U
U
U
201856
951519
779525
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
04/01/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JHA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene -d8
Bromofluorobenzene
1,2 -Dicdiloroetheme-d4
Seal-Volatile Organics
Phenol
Pyridine
Aniline
bis (2-cailoroethyl) ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-chloroispprppyl)ethe
4-Methylphenol
n-Nltroso-di-n-prppyleunine
Hexachloroethane
U
U
U
U
V
U
U
U
U
u u u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Racovery
99.3
102
93.7
10
10
10
10
10
10
10
20
10
10
10
10
10
10
METHOD/CAS#
SW-846, 8240
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6 J^
79-00-5 ^B
79-01-6 ^^
75-69-4
108-05-4
75-01-4
95-47-6
INTSTDl
INTSTD2
INTSTD3
Recovery Llalts
88
86
76
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
TO 110
TO 115
TO 114
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5 ^^
621-64-7 ^B
67-72-1 ^F
June 17, 1994 14:21
San
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page11
lample ID: M-53BP;15 FT DN GRAD 2 FT. Lab ID: 9403036-08A CoUected: 03/30/94 10:45:00
TEST
Seal-Volatila Organics
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)metheme
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroemiline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2 -Chloronaphthalene
2-Nitroemiline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
jna-Dinitr(3phenol
fjHlitrophenol
Dibenz of urem
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-binitro-2-methylphenol
n-Nitrosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenemthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
bis(2-Ethylhexyl)phthalate
Chyrsene
Di-n-octylphthalate
Benzo[b&k]fluoremthene
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h] emthracene
Benzo[g,h,i]perylene
1,4-Dichlorobenzene-d4
Naphthalene-d8
^iBtenaphthene - dlO
\ ^Bnemthrene - dl 0
(Syrsene-dl2
RESULT
D
D
U
D
U
U
u u u u u
u u u u u u u u
D
u u D
u u u u u u
u u u
u
u D
u D
U
u u u u u 4890 B
U
U
U
D
D
U
U
Int. Std.
Int. Std.
Int. Std.
Int. Std.
Int. Std.
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
50
10
10
10
10
20
10
20
10
10
10
10
10
50
10
10
50
10
50
50
10
10
10
10
10
10
20
50
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
04/13/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
-
-
-
-
-
June 17, 1994 14:21 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Pagel2
Sample ID: M-53BP;15 FT DN GRAD 2 FT. Lab ID: 9403036-08A CoUected: 03/30/94 10:45:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Seal-Volatile Organics
Perylene-dl2 Int. Std. ug/Kg
SW-846, 8270
Surrogate
2-FLUOROPHENOL
Phenol-d5
Nitrobenzene-d5
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
04/13/94 MMR
r Seal-Volatile Organics 8270
%Recovery
45.94
53.41
56.82
64.85
70.89
92.21
Recovery Llalts
21 TO 100
10 TO 94
35 TO 114
43 TO 116
10 TO 123
33 TO 141
Sample ID: M-53E; PT OF DIS SURFACE LabID: 9403036-09A CoUected: 03/30/94 11:03:00
TEST
Volatila Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetracdiloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chlorofonn
Chlorometheme
Dibromochloromethane
1,1-Dichloroethane
1,2 -Dichlor(Mthane
1,1 -Dicdiloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloroprppeme
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4 -Met:hyl - 2 - Pentemone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
RESULT
13 J
U
D
U
U
U
U
U
U
U
U
U
U
U
U
U
78
U
U
U
U
U
U
D
U
a U
U
7 BJ
U
u u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
100
20
20
20
20
20
20
100
20
20
20
20
20
20
20
20
20
20
20
100
20
20
20
20
20
20
20
20
20
100
20
20
20
ANALYZED
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240 ^^
67-64-1 ^B
107-02-8 ^P
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5 ^B
127-18-4 ^P
June 17, 1994 14:21
S^
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page13
pie ID: M-53E; PT OF DIS SURFACE LabID: 9403036-09A CoUected: 03/30/94 11:03:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
Bromochlorometheme
1,4-Difluorobenzene
Chlorobenzene-d5
u 360 B
u U
! U
U
U
U
184818
837656
681211
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
For
20
20
20
20
20
20
20
20
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Volatile Organics 8240
%Rscovary
99
98
97
.4
.6
.3
SW-646, 8240
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
INTSTDl
INTSTD2
INTSTD3
Recovery Llalts
88
86
76
TO 110
TO 115
TO 114
l^pple ID: M-53E; PT OF DIS 2 FT. LabID: 9403036-lOA CoUected: 03/30/94 11:13:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroetheme
1,l-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichlorppropeme
cis -1,3-Dichlor(3propene
jyuns-1,3-Dichloropropene
4 B-Dichlorobenzene
^IBi-Dichlorobenzene
RESULT
U
U
U
U
o D
U
U
U
U
U
U
U
u u
u
u D
U
U
U
U
U
D
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
50 10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
ANALYZED
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
June 17, 1994 14:21 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page14
Sample ID: M-53E; PT OF DIS 2 FT. LabID: 9403036-lOA CoUected: 03/30/94 11:13:00
TEST
Volatile Organics
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
RESXTLT
U
D
3 BJ
U
U
1,1,2,2-Tetrachloroetheme U
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
i,1,2-Trichloroethane
Trichloroethene
U
U
9 BJ
U
u trichlorofluoromethane U
/inyl Acetate
\'inyl Chloride
o-Xylene
Bromochl orome theme
1,4-Difluorobenzene
Chlorobenzene-d5
o u u 217003
992459
823281
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
%R«covary
101
102
93.8
METHOD/CAS#
SW-846, 824(}
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
INTSTDl
INTSTD2
INTSTD3
Recovery Llalts ^^^
88
86
76
TO 110
TO 115
TO 114
^
^
Sample ID: M-53E; 25 FT DN GRAD SUR. LabID: 9403036-11A CoUected: 03/30/94 11:20:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromcsmethane
2-Bu'temone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroetheme
1,l-Dichloroethene
RESULT
u u u D
U
U
U
U
U
U
U
u u u D
u u u U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
50
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS«
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2 ^^
75-35-4 ^B
June 17, 1994 14:21
Sam
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
PagelS
pie ID: M-53E; 25 FT DN GRAD SUR. Lab ID: 9403036-11A CoUected: 03/30/94 11:20:00
TEST
Volatile Organics
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
d j^pmochlorome theme
^ B-Difluorobenzene
chlorobenzene-d5
RESULT
U
U
u
u u u u
u u
6 BJ
u U
U
U
U
9 BJ
U
U
U
U
U
U
180658
842376
672227
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/kg
ug/Kg
ug/Kg
DETECTION
LTMTT
50
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene-d8
Bromofluorobenzene
I.2. •Dichloroethane-d4
%Recovery
99.6
101
95.6
METHOD/CAS«
SW-846, 8240
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
INTSTDl
INTSTD2
INTSTD3
Recovery Llalts
88
86
76
TO 110
TO 115
TO 114
Sample ID: M-53E; 25 FT DN GRAD 2 FT. Lab ID: 9403036-12A CoUected: 03/30/94 11:25:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloronethane
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
X^bon tetrachloride
^Borobenzene
^IB oroe thane
u
D
U
U
U
U
U
U
U
u
u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
50
10
10
10
10
10
10
50
10
10
10
10
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
June 17, 1994 14:21 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Pagel6
Sample ID: M-53E; 25 FT DN GRAD 2 FT. LabID: 9403036-12A CoUeaed: 03/30/94 11:25:00
TEST
Volatile Organics
2-<3iloroethylvinyl ether
Chloroform
cnilorome theme
Dibromo<dilorome thane
1,l-Dichloroethane
1,2-Dichloroetheme
1,l-Dichloroethene
2-Hexanone
trems-1,2-Dichloroethene
1,2-Dichloropropeme
ci s-1,3 -Di chloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluorometheme
vinyl Acetate
Vinyl Chloride
o-Xylene
Bromochloromethane
1,4-Difluorobenzene
Chlorobenzene-65
RESULT
D
u U
U
U
U
U
U
U
D
U
U
U
U
U
U
10 B
a D
U
u u 8 BJ
u u u u u u 199426
921570
766068
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LTMTT
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
04/05/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene - d8
Bromofluorobenzene
1,2 -Dichloroethane-d4
%Recovery
100
102
94.7
METHOD/CAS#
SW-846, 8240
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
XOO-42-5
79-34-5
127-18-4
108-88-3
71-55-6 ^^
79-00-5 ^B 79-01-6 ^^
75-69-4
108-05-4
75-01-4
95-47-6
INTSTDl
INTSTD2
INTSTD3
Recovery Llalts
88
86
76
TO 110
TO 115
TO 114
Sample ID: M-33B&C;PTOF DIS SURFACE LabID: 9403036-13A CoUected: 03/30/94 13:40:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Antiaony
Cadalua
pH (Soil)
D ug/g
0.271 ug/g
7.57 pH unit
2.9 05/05/94 LVD
0.1 05/05/94 LVD
03/31/94 AA
SW-846, 6010
SW-846, 6010
SW-846,9045A
June 17, 1994 14:21
l^mi
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page17
pie ID: M-33B&C;PT OF DIS 2 FT. Lab ID: 9403036-14A CoUected: 03/30/94 13:45:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Antimony
Cadalua
pH (Soil)
U ug/g
0.247 ug/g
9.36 pH Unit
2.6 05/05/94 LVD
0.1 05/05/94 LVD
03/31/94 AA
SW-846, 6010
SW-846, 6010
SW-846,9045A
Sample ID: M-33B(tC;25 FT DN GRAD SUR. Lab ID: 9403036-15A CoUected: 03/30/94 13:53:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Antiaony
Cadalua
pH (Soil)
U ug/g
U ug/g
8.27 pH Unit
2.9 05/05/94 LVD
0.1 05/05/94 LVD
03/31/94 AA
SW-846, 6010
SW-846, 6010
SW-846,9045A
Ift, pie ID: M-33B&C;25 FT DN GRAD 2 FT Lab ID: 9403036-16A CoUected: 03/30/94 14:02:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Antiaony
Cadalua
pH (Soil)
U ug/g
2.90 ug/g
8.28 pH Unit
2.9 05/05/94 LVD
0.1 05/05/94 LVD
03/31/94 AA
SW-846, 6010
SW-846, 6010
SW-846,9045A
#
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection linn
J Indicates an estimated value. Tbis flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection liinit but greater than zero. (e.g. 1. IJ with a detection liinit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recoveiy was outside of the speciiied limits.
ENVIRONMENTAL LAB WORK REQUEST
^^ ^/^ / 7-
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TraOKOL ENVIRONMENTAL LABORATORY LWR No. E10396
A.f. V/AuKe^ ^5fo
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OBGAMZAnOHr
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BIPOBT BBBU.T8 TDi
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS
1/14
1. •S'^^MO •42S"
Pt of "Dts -sog. \AM»«. A A\-^'1 |or<& Cd,Cr . Ae^^ . "Pb . -^ato -fco to
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(i^c^^TJi^vr^v^. ^u\^\o 14 AiTtJ t^ Wof AX-i37A-mo
7. Nk-«,i,»o,«"a,rs-M A \>> 0<- /U.-S57A VV^A? VOCs ©"Z-'iO
CbOlOl (-300;
Cd,Cr,M, Pb,-5*o , SM.\Q^\t.
Cie^r) (i47oj ii^ \4AV«_ •-^ 0^ )U.-iS7A vV4r' , P*'V , Mercur ^ «.Ak-«,%io,y2.^
v4*iFg, ^ W of A-537A V14^ VoCj ez4o
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T^H»c'QcAm)L OJ of K-WTA u«-^ VOCs - eZfD
CHAIN OF CUSTODY
REUNQUISHEDBY DATE TIME RECDVED BY DATE TIME
c^^Ml /^AfiZff looo '//A^yJa^.^y^ -^yr/9 H /^^^
FOR LABORATORY USE ONLY
•I
MIB OOMFLBISD IMRBBVBTBD
ENVIRONMENTAL LAB WORK REQUEST
THIOKOL ENVIRONMENTAL LABORATORY
4.t^. WAUC^g^
(MtSANUAIlON
€i\\)ivo 6^l(^u.-
BON
3oie-
\/4O0 (1S*)40
Mim
.WTOi
HELEN WARD, MS 301
14 Al>vJl^
SAMPLE INFORMATION
Io
^11
SAMPLE
J. SW«\U ^|5'
P^^?^ Dis'Zf*
3o' n>^ OBAD
"5 JE^
DATE
KAr«.
I4AVP.
/4/ff*
»5-A?C
TYPE
t/
/
»^
vA
»/
LOCATION
W of AJC-il7A
\Ar ^^f- AA'S37A
A-S?
/K'iS-7
M-S-7
TIME
IZPT
120^
I4zr Mc^rcixr^ - "^^-TD
/^3C?
>435- Xfemttr.^ ~ 7-f70
TEST
Vocs - SZ40
t McrcttrJi ~ 7-^70
REMARKS
(^o45T C^^W^
H ^£:
14AP1L »/ A-^7 <44^
14 A?^ >/ AA.-•W l-s-jo C^ "(j»5io «6o) ;3o4s7
•SM^^Jk- i-pW
i+Ape ^/ M-^S'-W /'S'/O Voc'i. > gr^ g/s (-2. enhki fsx^l) fJtiakh- "Z
\A /£h££^!L-iSt Ji££L \/ M-'gS-NN/ IS2.0
Ttoio) C^ckft)
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-^7
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(fccxo) ^
\^-8zf
V4A^«. • AA.--SS«VA; fs-j* CH 4S7
VV
CHAIN OF CUSTODY
RELINQUISHED BY DATE TIME RECEIVED BY DATE TIME
.^k ^f/a/A^ /^/¥i^^i /^^^ .^^^^^.....^^Ax A^ii7(7
T
FOR LABORATORY USE ONLY r""^ MnsBFOBra aoiuivu
ENVIRONMENTAL LAB WORK REQUEST ''AJ^£A>
«
THIOKOL ENVIRONMENTAL LABORATORY ao3?^ "paJ. 3
A. P. \JL>AUCgR_
BCIBOiaN
\/^Q
WOBXC
l'B^40
MIS
i4A?g-?f
OBCANIZAIION
eHy\e.o eusT^^ 3o|te"
•BOOT laSUU* TOl
HELEN WARD, MS 301
^1
%
m
SAMPLE INFORMATION
1
SAMPLE
] 1. SuJU-VV bZI
25'''DKSBA©-
ks''DN 6e*iT> ?
1 5 SuXlM*, fcXI
2?' -DM felZXb ^
1 ^
1 J.
1 ^
1 ''•
1 L
1 *'
lOl
11.
13.
DATE
HAhL.
TYPE
G
•^
A
y
c
LOCATION
/jL-r^-vO
M-S^S-XU
M'-sr-u;
,
TIME
JSBX)
i54r
1-5-4^
TEST REMARKS
1
\/ocs -Sz-io ', 'g)is(z^>LLV^a.»^i)vk-^AU'4
. CIPOIO) C3OO^ ^HO
"vcc-s --ea«fO', 'BriCz^^'^f^^O"^'^'^^*^ "n
1 =^^=^^=
1
g^
CHAIN OF CUSTODY
RELINQUISHED BY DATE TIME RBCQVESBV DATE TIME
^M/alL^ i^APlL</^ AOOd) ^A (^^y.^,r^^- ^/^A9Y AA^A^AP
tr /
#
FOR LABORATORY USE ONLY r^ MIKBDOXnO •ciunu 1
V'/r- 9*/
June 17, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page i
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty. Ut 84302-0707
Analytical Labs M/S 245
Atm: Dr. John Terry
Tele: 801-863-2384
Work Orderly 9404012 Sample and Test Code Identification
LabID: .Sample IDt
OIA M-39;Pr OF DIS. SURFACE
Test Codes and Names
LabID: RumrAe. ITi-
02A M-39;Fr OF DIS. 2 FT.
LabID: .Sample ID;
~!BA M-39;25 FT DN ORAD SURFACE
LabID: .Sample ID:
04A M-39;25 FT DN ORAD 2 FT.
LabID:
(AA
LabID:
MA
.Sample TD;
M-39;25 FT DN ORAD 2FT DUP
^leTD;
W-M337A;Pr OF DB SURFACE
LabID: .Sample ID:
~37A W-M337A;Fr OF DB 2 FT.
SB AE2
CD AE2
CR AE2
PB~AE2
Aa_AE2
Antimony
Cadmium
Chromium
Lead
SUver
Test Codes and Names
SB AE2
CIJAE2
CR~AE2
PB AB2 AC31AE2
Antimony
Cadmium
Chromium
Lead Silver
Test Codes and Names
SB AE2
CD AE2
CR~AE2
PB AE2
Aa_AE2
Antimony
Cadmium
Chromium
Lead
Silver
Test Codes and Names
SB AE2
CD"AE2
CR AE2
ra~AE2 ACTAEZ
Antimony
Cadmium
Chromium
Lead
Silver
Test Codes and Names
SB AEZ
CD"AE2
CR~AE2
PB AEZ
A<r_AE2
Antimoiiy
Cadmium
Chromium
Lead
Silver
Test Codes and Names
S04IC1
SB AE2
Clf AE2
CR~AE2
PB AE2
ACT AEZ
Ha~CV2
824S
PH_S
Sulfate
Antimony
Cadniium
Cnromium
Lead
Silver
Mercury
Volatile Organici
pH(Soil)
Test Codes and Names
S04IC1
SB AE2
CITAEZ
Sulfate
Antimony
Cadmium
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
sw-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 6010
SW-846, 6010
SW-S46, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 6010
SW-S46, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
EPA 300.0
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
SW-846,9045A
Method
EPA 300.0
SW-846, 6010
SW-846, 6010
LabID: Sample ID:
W-M537A;Fr OF DB 2 FT.
•
Test Codes and Names
CR_AE2
PB AE2
Ad"AE2
HO"CV2
8240
PH S
Chromium
Lead
Silver
Mercuiy
Volatile Organica
pH (SoU)
Method
sw-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
SW-846,9045A
LabID:
08A
Sample ID Sample ID:
W-M33^A;25 FT DN ORAD SUR.
Test Codes and Names
S04IC1
SB AE2
CD;.AE2
CR_AE2
PB AE2
AdlAE2
HO CV2
8240
PH S
Sulfate
Antimony
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
pH (SoU)
Method
EPA 300.0
sw-846, 6010
SW-846, 6010
sw-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
SW-846,9045A
LabID: Sample ID:
09A W-M537A;Pr/DB 2'RNS BLANK
LabID: Sample ID:
IOA W-M337A;25FT DN ORAD 2 FT.
Test Codes and Names
8240 VolatUe Organics
Test Codes and Names
S04IC1
SB AE2
CD.AE2
CR AE2
PB~AE2
AG AE2
Ha"CV2
8240
PH S
Sulfate
Antimony
Cadmium
Chromium
Lead
SUver
Mercuty
VolatUe Organics
pH (SoU)
Method
SW-846, 8240
Method
EPA 300.0
sw-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
SW-846,9045A
LabID: SamplelD:
UA M-57;PT OF DB SURFACE.
LabID:
12A
LabID:
IJA
Sample
M-57;Pr
ID:
PT OF DB 2 FT.
.Sample TT>;
M-57;30 FT I DN ORAD SURFACE
Test Codes and Names
HO_CV2 Mercury
Test Codes and Names
Ha_CV2 Mercury
Test Codes and Names
HO_CV2 Mercury
Method
sw-846, 7471
Method
sw-846, 7471
Method
sw-846, 7471
LabID:
14A
LabID:
ISA
ale ID:
M-57;30 FT DN ORAD 2 FT.
.Sample ID:
M55-W;PT OF DB SURFACE.
LabID: lelD:
16A M55-W;Pr OF DB 2 FT.
LabID: Sample TD:
17A M55-W;25FT DN ORAD SURFACE
#
Test Codes and Names
HO_CV2 Mercury
Test Codes and Names
S04IC1
CD AE2
ZN AE2
8240
8270
PH_S
Sulfate
Cadmium
Zinc
VolatUe Otganics
Semi-VolatUe Otganics
pH (SoU)
Test Codes and Names
S04IC1
CD AE2
ZN AEZ
8240
8270
PH_S
Sulfate
Cadmium
Zinc
VolatUe Otganics
Semi-VolatUe Otganics
pH (SoU)
Test Codes and Names
S04IC1
CD AEZ
ZN AEZ
8240
Sulfate
CAdmiuin
Zinc
VolatUe Organics
Method
SW-846, 7471
Method
EPA 300.0
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846, 8270
SW-846,9045A
Method
EPA 300.0
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846, 8270
SW-846,904SA
Method
EPA 300.0
SW-846, 6010
SW-846, 6010
SW-846, 8240
UbID:
I7A
LabID:
18A
LabID:
Sample ID:
M55-W;25FT DN ORAD SURFACE
.Sample TD
•SFT DN ORAD SUR DUP
le ID:
19A M55-Wa5FT DN ORAD 2 FT.
Test Codes and Names
8270 Semi-VolatUe Otganics
PH_S pH (Soil)
Test Codes and Names
S04IC1 Sulfate
CD AEZ Cadmium
ZN"AE2 Zinc
PHJS pH (SoU)
Test Codes and Names
S04IC1
CD AE2
ZN AEZ
8240
8270
PH_S
Sulfate
Cadmium
Zinc
VolatUe Organics
Semi-VolatUe Organics
pH (SoU)
Workorder Comments
Method
SW-846, 8270
SW-846,9045A
Method
EPA 300.0
SW-846, 6010
SW-846, 6010
SW-846,9045A
Method
EPA 300.0
SW-846, 6010
SW-846, 6010
SW-846, 8240
SW-846, 8270
SW-846,9045A
Report: The surface samples for semi-volatUe organic analyses were
received contaminated with asphalt from paving activity
rendering the samples unusable. Clean re-samples are required
to complete analyses by Method 8270.
This is to cenify that the following samples were analyzed using good laboratory practices
to show the following results. m
Sample ID: M-39;PT OF DIS. SURFACE Lab ID: 9404012-OlA CoUected: 04/14/94 10:50:00
TEST RESTJLT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Antimony
Cadmium
Chromium
Lead
Silver
D
592
93.7
19.8
187
ug/g
ug/g
ug/g
ug/g
ug/g
2.7
0.1
0.3
1.3
0.2
05/05/94
05/05/94
05/05/94
05/05/94
05/05/94
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
Sample ID: M-39;PT OF DIS. 2 FT. Lab ID: 9404012-02A CoUected: 04/14/94 10:55:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Antimony «miuffl
omium
Lead
Silver
2.77
2.06
14.1
11.1
45.8
ug/g
ug/g
ug/g
ug/g
ug/g
2.6
0.1
0.3
1.3
0.2
05/05/94
05/05/94
05/05/94
05/05/94
05/05/94
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
Sample ID: M-39;25 FT DN GRAD SURFACE LabID: 9404012-03A CoUected: 04/14/94 11:05:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Antimony
Cadmium
Chromium
Lead
Silver
u
1350
79.2
12.5
107
ug/g
ug/g
ug/g
ug/g
ug/g
2.8
0.1
0.3
1.4
0.2
05/12/94
05/12/94
05/12/94
05/12/94
05/12/94
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
#
June 17, 1994 14:27 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 2
Sample ID: M-39;25 FT DN GRAD 2 FT. LabID: 9404012-04A CoUected: 04/14/94 11:10:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS*
Antimony
Cadmium
Chromium
Lead
Silver
D
4.38
11.6
7.70
32.5
ug/g
ug/g
ug/g
ug/g
ug/g
2.8
0.1
0.3
1.4
0.2
05/12/94
05/12/94
05/12/94
05/12/94
05/12/94
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
Sample ID: M-39;25 FT DN GRAD 2FT DUP Lab ID: 9404012-05A CoUected: 04/14/94 11:10:00
TEST RESXTLT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Antimony
Cadmium
Chromium
Lead
Silver
u
0.777
12.640
9.643
9.129
ug/g
ug/g
ug/g
ug/g
ug/g
2.9
0.1
0.3
1.5
0.2
05/12/94
05/12/94
05/12/94
05/12/94
05/12/94
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
Sample ID: W-M337A;PTOF DIS SURFACE LabID: 9404012-06A CoUected: 04/14/94 11:40:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Sulfate
Antimony
Cadml\im
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
u
u
0.711
21.3
37.6
2.10
0.033
31 J
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
.7
2.7
0.1
0.3
1.3
0.2
0.020
50
04/26/94
05/12/94
05/12/94
05/12/94
05/12/94
05/12/94
04/22/94
04/22/94
CRS
LVD
LVD
LVD
LVD
LVD
CRS
JMA
BPA 300.0
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
6010
6010
6010
6010
6010
7471
8240
June 17, 1994 14:27
f
San
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 3
imple ID: W-M337A;PT OF DIS SURFACE Lab ID: 9404012-06A CoUected: 04/14/94 11:40:00
TEST
Volatile Organics
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromoform
Bromome theuie
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheuie
1,1-Dichloroethane
1,2-Dichloroethsme
1,l-Dichloroethene
2-Hexanone
treuis -1,2-Dichloroethene
1,2-Dichloropropeme
^is -1,3 -Dichloropropene
^^ans -1,3 -Dichloropropene
^11^ -Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,l-Trichloroethane
1,1,2-Trichloroetheme
Tri chloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
Bromochloromethane
1,4-Difluorobenzene
Chlorobenzene-d5
RESULT
U U
u u u u
n u a u u
n
u u
u u u
u u u
u u u u 0
u u u n a u u
a 9 BJ
U
U
U
U
D
7 J
200922
880675
650229
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
ANAT.YZED
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene-d8
Bromofluorobenzene
1,2
pH (Soil)
-Dichloroethane-d4
8.81 pH Unit
%Recovery
95.8
94.8
94.5
METHOD/CAS#
SW-846, 8240
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
88
86
76
04/15/94
TO 110
TO 115
TO 114
KEN SW-846,9045A 4
June 17, 1994 14:27 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 4
Sample ID: W-M337A;PT OF DIS 2 FT. LabID: 9404012-07A CoUected: 04/14/94 11:45:00
TEST
Sulfate
Antimony
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorometheme
Bromoform
Bromcoie theme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexanone
trems-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2-Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
RESULT
143
U
0.372
11.8
9.83
0.337
D
D
U
U
U
U D
U
U
D
D
U
U
U
U
U
U
U
U
U
U
D
U
U
U
D
D
U
U
D
U
U
D
U
D
4 BJ
U
U
D
U
D
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
3
2.7
0.1
0.3
1.3
0.2
0.0093
50
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
ANALYZED
04/26/94
05/12/94
05/12/94
05/12/94
05/12/94
05/12/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
BY
CRS
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS*
EPA 300.0
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01
10061-02
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
6010
6010
6010
6010
6010
7471
8240
^^ A V
-5
-6
A w
June 17, 1994 14:27
sSn;
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 5
pie ID: W-M337A;PT OF DIS 2 FT. LabID: 9404012-07A CoUected: 04/14/94 11:45:00
TEST
Volatile Organics
o-Xylene
Bromochlorometheme
1,4-Difluorobenzene
Chlorobenzene-d5
pH (Soil)
RESULT
U
233734
1075922
885842
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
ANALYZED
04/22/94
04/22/94
04/22/94
04/22/94
BY
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
8.99
Sample ID: W-M337A;25 FT DN GRAD SUR.
TEST
IRfate
Antimony
Cadmium
Chromiiim
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorcoie theme
Bromofonn
Brcmcanethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
RESULT
U
u
0.927
24.4
39.9
1.92
0.025
38 J
U
D
D
U
D
U
U
U
U
U
U
2-Chloroethylvinyl ether D
^[•^orofonn
1 HLoromethane
^Wbromochlorometheme
U
D
U
pH Unit
%Recovery
101
103
90.1
METHOD/CAS*
SW-846, 8240
95-47-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
88
86
76
04/15/94
TO 110
TO 115
TO 114
KEN SW-846,9045A
LabID: 9404012-08A CoUected: 04/14/94 11:55:00
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
5
2.6
0.1
0.3
1.3
0.2
0.0096
50
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
ANALYZED
04/26/94
05/12/94
05/12/94
05/12/94
05/12/94
05/12/94
04/22/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
BY
CRS
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS«
EPA 300.0
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
June 17, 1994 14:27 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 6
Sample ID: W-M337A;25 FT DN GRAD SUR. LabID: 9404012-08A CoUected: 04/14/94 11:55:00
TEST
Volatile Organics
1,1-Dichloroethane
1,2-Dichloroetheme
1,l-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Tri chloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
Brcmochlorometheme
1,4-Difluorobenzene
Chlorobenzene-d5
pH (Soil)
RESULT
D
U
U
U
U
U
U
U
n n u 1 J
u
u D
u u u 8 BJ
u
u u
u
u 13
85921
375614
303183
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
50
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene - d8
Bromofluorobenzene
1,2-•Dichloroethane-d4
8.58 pH Unit
%Recovery
99.7
98.4
103
METHOD/CAS#
SW-846, 8240
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4 ^^
75-01-4 ^B
95-47-6 ^^
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
88
86
76
04/15/94
TO 110
TO 115
TO 114
KEN SW-846,9045A
Sample ID: W-M337A;PT/DIS 2'RNS BLANK LabID: 9404012-09A CoUected: 04/14/94 11:58:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromometheme
u
u u u
u u u
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
50
10
10
10
10
10
10
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
June 17, 1994 14:27
f
San
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 7
ample ID: W-M337A;PT/DIS 2'RNS BLANK Lab ID: 9404012-09A CoUected: 04/14/94 11:58:00
TEST
Volatile Organics
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheme
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexemone
trems-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
Jl^fethyl - 2 - Pentemone
"yrene
TTl,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
Bromochloromethane
1,4-Difluorobenzene
Chlorobenzene-dS
RESULT
5
U
U
u u u u
u u u u u
u
u u
u
u u u u u
u u
u
u u
u
u BJ
u u u u
u u 208298
956301
793897
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
50 10
10
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene-d8
Bromofluorobenzene
1.2 -Dichloroetheme-d4
%Racovery
101
103
95.8
METHOD/CAS#
SW-846, 8240
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
88
86
76
TO 110
TO 115
TO 114
Sample ID: W-M337A;25FT DN GRAD 2 FT. Lab ID: 9404012-lOA CoUected: 04/14/94 12:05:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
fate ug/g 04/26/94 CRS EPA 300.0
June 17, 1994 14:27 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 8
Sample ID: W-M337A;25FT DN GRAD 2 FT. LabID: 9404012-lOA CoUected: 04/14/94 12:05:00
TEST
Antimony
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroethane
1,l-Dichloroethene
2-Hexanone
trems-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2-Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Tri chlorofluorometheme
Vinyl Acetate
vinyl Chloride
o-Xylene
Brcsnochlorometheme
REST7LT
U
0.406
13.5
10.1
0.371
0.014
U
U
U
U
D
o
U
U
U
U
U
U
U
U
U
U
U
U
u u
u u
u u u u D
u u u u u u u 4 BJ
U
U
U
U
u u 68190
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
2.9
0.1
0.3
1.5
0.2
0.013
50
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
05/12/94
05/12/94
05/12/94
05/12/94
05/12/94
04/22/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
BY
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01
10061-02
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
INTSTDl
6010
6010
6010
6010
6010
7471
8240
^ V
-5
-6
^^^ w
June 17, 1994 14:27
f
San
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 9
^ple ID: W-M337A;25FT DN GRAD 2 FT. Lab ID: 9404012-lOA CoUected: 04/14/94 12:05:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatila Organics
1,4-Difluorobenzene
Chlorobenzene-d5
pH (Soil)
318042 ug/Kg
262304 ug/Kg
Surrogate/Recovery Data
Surrogate
Toluene-d8
Bromofluorobenzene
l,2-Dichloroethane-d4
8.60 pH Unit
SW-846, 8240
04/25/94 JMA INTSTD2
04/25/94 JMA INTSTD3
For Volatile Organics 8240
%Recovery Recovery Limits
99.5 88 TO 110
101 86 TO 115
99.3 76 TO 114
04/15/94 KEN SW-846,9045A
Sample ID: M-57;PT OF DIS SURFACE. LabID: 9404012-llA CoUected: 04/14/94 14:25:00
TEST RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
m cury ug/g 0.023 04/22/94 CRS SW-846, 7471
Sample ID: M-57;PT OF DIS 2 FT. LabID: 9404012-12A CoUected: 04/14/94 14:30:00
TEST RESULT UNITS DETECTION ANALYZED BY METEOD/CAS#
LIMIT
Mercury ug/g 0.019 04/22/94 CRS SW-846, 7471
Sample ID: M-57;30 FT DN GRAD SURFACE Lab ID: 9404012-13A CoUected: 04/14/94 14:35:00
TEST RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Mercury 0.197 ug/g 0.016 04/22/94 CRS SW-846, 7471
Sample ID: M-57;30 FT DN GRAD 2 FT. LabID: 9404012-14A CoUected: 04/14/94 14:40:00
TEST RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT m cury ug/g 0.017 04/22/94 CRS SW-846, 7471
June 17, 1994 14:27 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
PagelO
Sample ID: M55-W;PT OF DIS SURFACE. Lab ID: 9404012-15A CoUected: 04/14/94 15:10:00
TEST
Sulfate
Cadmium
Zinc
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromometheme
2-Butemone
Carbon disulfide
Carbon tetrachloride
chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochlorcsnetheme
1,1 -Dichloroetheme
1,2-Dichloroethane
1,l-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
Bromochloronetheme
1,4-Difluorobenzene
Chlorobenzene-dS
RESULT
u
0.298
87.6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
5 BJ
U
U
O
U
U
U
108567
493334
391088
UNITS
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
5
0.1
0.2
50
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
04/26/94
05/12/94
05/12/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
BY
CRS
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
EPA 300.0
SW-846, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1 ^^
75-34-3 ^B
107-06-2 ^^
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
INTSTDl
INTSTD2
INTSTD3
June 17, 1994 14:27
San
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page11
Smple ID: M55-W;PT OF DIS SURFACE. Lab ID: 9404012-15A CoUected: 04/14/94 15:10:00
TEST RESULT UNITS
Volatile Organics
DETECTION ANALYZED
LIMIT
BY
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene-d8
Bromofluorobenzene
l,2-Dichloroetheme-d4
Seml-Volatlla Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2 -Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-prppyleunine
^|Hcachloroe thane
fl^robenzene
^IBophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)metheme
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4 - cail oroani 1 ine
Hexachlorobutadiene
4 -Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
Acenaphthy1ene
3-Nitroemiline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
^l^^i troani 1 ine
i B-Dinitro-2-methylphenol
^l^nitrosodiphenylamine
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
%Recovery
98.3
100
95.8
1.5
10
10
5.7
3.3
1.9
4.4
4.6
1.9
2.3
5.7
4.0
12
1.6
1.4
2.2
3.6
2.7
3.4
5.3
2.7
1.9
1.6
1.8
0.90
3.0
2.2
6.0
2.7
4.0
1.9
1.5
1.6
3.5
2.4
1.9
42
2.4
3.0
1.9
5.7
1.9
4.2
1.9
3.6
24
1.9
Recovery
88
86
76
TO
TO
TO
ME7B0D/CAS#
SW-846, 8240
Limits
110
115
114
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
June 17, 1994 14:27 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Pagel2
Sample ID: M55-W;PT OF DIS SURFACE. LabID: 9404012-15A CoUected: 04/14/94 15:10:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Semi-Volatila Organics
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorpphenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoremthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
bis(2-Ethylhexyl)phthalate
Chyrsene
Di-n-octylphthalate
Benzo [b&k] fluoremthene
Benzo[a]pyrene
Indeno(1,2,3-cd]pyrene
Dibenz[a,h] emthracene
Benzo[g,h,i]perylene
1,4-Dichlorobenzene-d4
Naphthalene-dS
Acenaphthene-dl0
Phenemthrene-dl0
Chyrsene-dl2
Perylene-dl2
Int.
Int.
Int.
Int.
Int.
Int.
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Std.
Std.
Std.
Std.
Std.
Std.
1.9
1.9
3.6
5.4
1.9
2.5
2.2
1.9
2.
7,
2.
2.
2.
4.
2.
3.
2.
4.
SW-846, 8270
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
Surrogate/Recovery Data For Sami-Volatile Organics 8270
Surrogate
2-FLUOROPHENOL
Phenol-d5
Ni trobenzene-d5
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
pH (Soil) 7.82 pH Unit
%Recovery
Q
Q
Q
Q
Q
Q
Recovery Limits
21 TO 100
10 TO 94
35 TO 114
43 TO 116
10 TO 123
33 TO 141
04/15/94 KEN SW-846,9045A
Sample ID: M55-W;PT OF DIS 2 FT. LabID: 9404012-16A CoUected: 04/14/94 15:20:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Sulfate
Cadmium
Zinc
Volatile Organics
Acetone
Acrolein
267
0.793
48.6
U
U
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
7
0.1
0.2
50
10
04/26/94
05/12/94
05/12/94
04/25/94
04/25/94
CRS
LVD
LVD
JMA
JMA
BPA 300.0
SW-846, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
June 17, 1994 14:27
S^
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
PagelS
Smple ID: M55-W;PT OF DIS 2 FT. LabID: 9404012-16A CoUected: 04/14/94 15:20:00
TEST
Volatile Organics
Acrylonitrile
Benzene
Bromodichlorometheme
Bromofonn
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroetheme
1,l-Dichloroethene
2-Hexemone
trans-l,2-Dichloroethene
1,2-Dichloroprppeme
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
J fel-Dichlorobenzene
^ ^^-Dichlorobenzene
1^-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1 -Trichloroetheuie
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
Brcmochlorometheme
1,4-oifluorobenzene
Chlorobenzene-d5
RESULT
4
U
U
U
U
U
U
U
U
U
u
u u n
u u u u u u u
u u u u u
u
u u u u u u BJ
u a u u
u u 77593
373266
298771
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
04/25/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JHA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatila Organics 8240
Surrogate
Toluene-d8
Bromofluorobenzene
1,2
Semi-Volatile Organics
Phenol
jnudine
IHL ine DK(2-Chloroethyl) ether
-Dichloroetheme-d4
u u u u
ug/L
ug/L
ug/L
ug/L
%Recovery
101
101
97.1
330
330
330
330
METHOD/CAS#
SW-846, 8240
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
88
86
76
04/22/94
04/22/94
04/22/94
04/22/94
TO 110
TO 115
TO 114
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
June 17, 1994 14:27 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Pagel4
Sample ID: M55-W;PT OF DIS 2 FT. LabID: 9404012-16A CoUected: 04/14/94 15:20:00
TEST
Semi-Volatile Organics
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4 -Chloroani1ine
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2 -Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofurem
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
n - Nitrosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
bis(2-Ethylhexyl)phthalate
Chyrsene
Di - n - octyIphthal ate
RESULT
U
U
u
u
u u
u u
u u u
u
u u u u u D
u
u o
u
u u u u u u u u u u u u u u n u
u u u
u u u u u u u u u u u
u 3600B
u
u
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
330
330
330
660
330
330
330
330
330
330
330
330
330
330
1700
330
330
330
330
660
330
660
330
330
330
330
330
1700
330
330
1700
330
1700
1700
330
330
330
330
330
330
660
1700
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
r ANALYZED
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6 ^^
77-47-4 ^H
88-06-2 ^^
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-S
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7 ^Mv
218-01-9 M|
117-84-0 ^^
June 17, 1994 14:27
Sam]
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
PagelS
iple ID: M55'W;PT OF DIS 2 FT. LabID: 9404012-16A CoUected: 04/14/94 15:20:00
TEST RESULT
Semi-Volatile Organics
Benzo[b&k]fluoranthene U
Benzo[a]pyrene U
Indeno[1,2,3-cd]pyrene U
Dibenz[a,h]anthracene
Benzo[g,h,i]perylene u u l,4-Dichlorobenzene-d4 Int. Std.
Naphthalene-d8
Acenaphthene-dl0
Phenemthrene-dl0
Chyrsene-dl2
Perylene-dl2
1^^ B(Soil)
Int. Std.
Int. Std.
Int. Std.
Int. Std.
Int. Std.
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Surrogate/Recovery Data
Surrogate
2-FLUOROPHENOL
Phenol-d5
Ni trobenzene-d5
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
7.64 pH Unit
DETECTION
LIMIT
330
330
330
330
330
ANALYZED
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
-
-
-
-
-
-
For Semi-Volatile Organics 8270
%Recovery
43.07
49.90
54.34
59.68
63.81
100.7
Recovery Limits
21
10
35
43
10
33
04/15/94
TO 100
TO 94
TO 114
TO 116
TO 123
TO 141
KEN SW-846,9045A
Sample ID: M55-W;25FTDN GRAD SURFACE LabID: 9404012-17A CoUected: 04/14/94
TEST
Sulfate
Cadmium
Zinc
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
il^Khloroethylvinyl ether
^jHoroform
Oilorome theme
RESULT
u
0.463
76.1
U
U
U
U
U
U
U
U
U
U
U
U
U
2 BJ
U
UNITS
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
3
0.1
0.2
50
10
10
10
10
10
10
50
10
10
10
10
10
10
10
ANALYZED
04/26/94
05/12/94
05/12/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
BY
CRS
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
EPA 300.0
SW-846, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
June 17, 1994 14:27 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Pageie
Sample ID: M55-W;25FT DN GRAD SURFACE Lab ID: 9404012-17A CoUected: 04/14/94
TEST
Volatile Organics
Dibromochlorometheme
1,1-Dichloroetheme
1,2-Dichloroethane
1,l-Dichloroethene
2-Hexemone
trems-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-bichloroprppene
1,2 -Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroethane
Te t rachl oroe thene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
Bromochloromethane
1,4-Difluorobenzene
Chlorobenzene-d5
RESULT
3
U
U
U
U
U
U
U
u
u u u u u
u u u
u u u BJ
u u u
u
u
u 224467
1009693
792280
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
50
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatila Organics 8240
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
Semi-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2 - Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2 -Dichlorobenzene
2 -Methylphenol
bis(2-chloroisoprppyl)ethe
4-Methylphenol
n-Nitroso-di-n-prppylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
%Recovery
96.5
96.3
93.4
1.5
10
10
5.7
3.3
1.9
4.4
4.6
1.9
2.3
5.7
4.0
12
1.6
1.4
2.2
3.6
METHOD/CA.S#
SW-846, 8240
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4 M^
108-05-4 ^V
75-01-4 ^
95-47-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
88
86
76
TO 110
TO 115
TO 114
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3 £^
78-59-1 ^B
88-75-5 ^^
June 17, 1994 14:27
S^]
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Pagel?
pie ID: M55-W;25FT DN GRAD SURFACE Lab ID: 9404012-17A CoUected: 04/14/94
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Semi-Volatile Organics
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2 - Ni troemi 1 ine
Dimethylphthalate
Acenaphthy1ene
3 - Ni troemi 1 ine
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
^n| -Dinitrotoluene
wH -Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4 -Nitroemiline
4,6-Dinitro-2-methylphenol
n-Nitrosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo[a] emthracene
bis(2-Ethylhexyl)phthalate
Chyrsene
Di-n-octylphthalate
Benzo[b&k]fluoranthene
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h] emthracene
Benzo[g,h,i]perylene
1,4-Dichlorobenzene-d4 Int.
Naphthalene-d8 Int.
Acenaphthene-dl0 Int.
Phenemthrene-dl0 Int.
Chyrsene - dl 2 Int.
i|Kprlene-dl2 Int.
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
Std.
Std.
Std.
Std.
Std.
Std.
,7
.4
,3
.7
.9
2.
3,
5.
2.
1.
1.6
1.8
0.90
3.0
2.2
3.5
2.4
1.9
42
2.4
3.
1.
5.
1,
4,
1.9
3.6
24
1.9
1.9
1.9
3.6
5.4
1.9
2.5
2.2
1.9
2.5
7.8
2.5
2.5
4.1
SW-846, 8270
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
June 17, 1994 14:27 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Pageie
Sample ID: M55-W;25FT DN GRAD SURFACE Lab ID: 9404012-17A CoUected: 04/14/94
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Semi-Volatile Organics SW-846, 8270
Surrogate/Recovery Data For Semi-Volatile Organics 8270
pH (Soil)
Surrogate
2-FLUOROPHENOL
Phenol-d5
Nitrobenzene-d5
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
7.45 pH Unit
%Recovery
Q
Q
Q
Q
Q
Q
Recovery Limits
21 TO 100
10 TO 94
35 TO 114
43 TO 116
10 TO 123
33 TO 141
04/15/94 KEN SW-846,9045A
Sample ID: M55-W;25FT DN GRAD SUR DUP Lab ID: 9404012-18A CoUected: 04/14/94 15:30:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS«
Sulfate
Cadmium
Zinc
pH (Soil)
U
0.363
42.1
7.44
ug/g
ug/g
ug/g
pH Unit
5
0.09
0.2
04/26/94
05/12/94
05/12/94
04/15/94
CRS
LVD
LVD
KEN
EPA 300.0
SW-846, 6010
SW-846, 6010
SW-846,9045A
Sample ID: M55-W;25FT DN GRAD 2 FT. Lab ID: 9404012-19A CoUected: 04/14/94 15:45:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Sulfate
Cadmium
Zinc
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
U
0.608
39.0
U
U
U
U
U
U
U
U
U
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
5
0.1
0.2
50
10
10
10
10
10
10
50
10
04/26/94
05/12/94
05/12/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
CRS
LVD
LVD
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
EPA 300.0
SW-846, 6010
SW-846, 6010
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
June 17, 1994 14:27
S^]
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page19
pie ID: M55-W;25FT DN GRAD 2 FT. Lab ID: 9404012-19A CoUected: 04/14/94 15:45:00
TEST
Volatile Organics
Carbon tetrachloride
Chlorobenzene
Chloroethane
2 -Chloroethylvinyl ether
Chloroform
Chlorometheme
D ibromochloromethane
1,1-Dichloroethane
1,2-Dichloroetheme
1,l-Dichloroethene
2-Hexanone
trems-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
^^ ,2,2 -Tetrachloroethane
^ Hrachloroe thene
^roluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Tri chlorof luoranetheme
vinyl Acetate
Vinyl Chloride
o-Xylene
Bromochloromethane
1,4-Difluorobenzene
Chlorobenzene-d5
1
RESULT
3
4
U
U
U
U
BJ
U
U
U
U
U
U
U
U
U
U
u u u u u
u u u u u BJ
u u u
u
u
u 206539
990121
822173
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
04/26/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene - d8
Bromofluorobenzene
1,2-
Seml-Volatlla Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
^A2-Dichlorobenzene
1 Bethylphenol
• Dichloroetheme-d4
THS (2-chloroisopropyl) ethe
u
u
u
u u u u u u u u
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%Recovery
101
101
94.3
330
330
330
330
330
330
330
660
330
330
330
METHOD/CAfl#
SW-846, 8240
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
88
86
76
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
TO 110
TO 115
TO 114
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
June 17, 1994 14:27 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page20
Sample ID: M55-W;25FT DN GRAD 2 FT. LabID: 9404012-19A CoUected: 04/14/94 15:45:00
TEST
Semi-Volatile Organics
4 -Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroemiline
Hexachlorobutadiene
4 -Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroemiline
Dimethylphthalate
Acenaphthylene
3-Nitroemiline
Acenaphthene
2,4-Dinitrophenol
4-Nitrpphenol
Dibenzofuran
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methyIphenol
n-Nitrosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
bis (2-Ethylhexyl)phthalate
Chyrsene
Di-n-octylphthalate
Benzo [b&k] fluoremthene
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h] emthracene
Benzo[g,h,i]perylene
1,4 -Dichlorobenzene-d4
Naphthalene-d8
RESULT
u u u u u
u u u u u u u u D
u u
u u
u u u u
u
u u
u
u
u u u u
u u u u u
u u u
u u u
u u u
u 8 04 OB
u u u u u u u Int. Std.
Int. Std.
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DETECTION
LIMIT
330
330
330
330
330
330
330
1700
330
330
330
330
660
330
660
330
330
330
330
330
1700
330
330
1700
330
1700
1700
330
330
330
330
330
330
660
1700
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
r ANALYZED
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
04/22/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8 ^^
99-09-2 ^^
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3 ^^^
191-24-2 ^^
-
June 17, 1994 14:27 CERTIFICATE OF ANALYSIS
RESULTS BY SAIMPLE
Page2l
Sample ID: M55-W;25FT DN GRAD 2 FT. LabID: 9404012-19A CoUected: 04/14/94 15:45:00
TEST
Semi-Volatile
Acenaphthene-
Phenanthrene-
Chyrsene-dl2
Perylene-dl2
pH (Soil)
RESULT
\ Organics
dlO
dlO
Int. Std.
Int. Std.
Int. Std.
Int. Std.
UNITS
ug/L
ug/L
ug/L
ug/L
Surrogate/Recovery Data
Surrogate
2-FLUOROPHENOL
Phenol-d5
Nit robenz ene-d5
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
7.59 pH Unit
DETECTION
LIMIT
ANALYZED BY METHOD/CAS#
SW-846, 8270
04/22/94 MMR
04/22/94 MMR
04/22/94 MMR
04/22/94 MMR
For Semi-Volatile Organics 8270
%Recovery
51.60
53.06
59.12
61.19
66.33
93.18
Recovery Limits
21 TO 100
10 TO 94
35 TO 114
43 TO 116
10 TO 123
33 TO 141
04/15/94 KEN SW-846,9045A
m
m
Data Reporting Qualifiers
ni^ U Compound was analyzed for but not detected. Indicates compound was below detection limiP
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. l.U with a detection liinit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recoveiy was outside of the speciiied limits.
ENVIRONMENTAL LAB WORK REQUEST
^f'^^usviCSL ENVIRONMENTAL LABORATORY
"^A.f. WALkle^
"^OAMZATtON
snwaoN
.MAO. STOP
LWR No. E10396
COSTONm WOUOUMB
14 APe ^4
UPOBT RBBULIB TOt
HELEN WARD, MS 301
SAMPLE INFORMATION
i
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS
%'^t*U '42'5'
2.%UjMkO 425"
J. 'SU)MU H^'S"
•25"'-DM <aBKD-
4. SVOULU -4^^
DOP>-2?^-DM
HA^m
[^-A-P^
^
V^
3:_
I't APR.
<3ltA«X> -1'
4. M-«,^, lO,«7,
14 A,TtJ
^
7. Ai-«,1,l(>,«^, rs
•Seg.
25" ^OH 6eKT)
\4 Av^
Itn-*/
v4 A,yg.
>/
\/
t^
A^•5°l
AA-^q
A\-3*^
AX-€?=^
M-^'^
Viof AX-i37/»r
/
^'
•^
dug. M «M.
171-M
•SJg.
Tii use'
/
v^
"guAiUtiC
toTO
los-r
uor
\\io
-CdyCf . Aai^ ,Pb . -^b
-tV
^ J±A^
-\S
llio
IWO
\Ji> o;- JU.-557A Vl4o
^ O-f AL-i37A
W of M-S37A
vi of A-i37A
W O^ >CL-S37A.
\\A<'
114^
U75
»4S^
OJ o?- M.-'%37A
7^
C<V)4S-) Cl^tTO)
Voc-s-z^o
Cfaoio^ (^300;
Cj,Cr,A^, Pb,-Sfa , •SwcV<;i^Vg.
'V>1\ Mercur ^
Clods'/ (7470)
VoC: ©240
sjoc-s. - e?4o
U^^ VOCis. - SZfO
, ^Hr , Mcrco
^
CHAIN OF CUSTODY >^ U^^/A4)} /- ^^^^^
RELINQUISHED BY DATE TIME RECHVEDBY DATE HME
// ^M ^d. I^APZU looo y^/^^.. ^^ -'A//r/9'\ /A(7(^
FOR LABORATORY USE ONLY i MIKCOMFUTED IMnBEFOnSD SIGNAITOB
July 25, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER. M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty. Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Orderly 9406037
LabID: Sample ID:
OIA M-39; FT OF DIS SimFACE.
LabID: Sample ID:
02A M-39;25 FT DN GRAD SURFACE
Sample and Test Code Identification
Test Codes and Names
1311 TCLP Meuls/SemiVoU Extr.
CD_AE2 Cadmium
CR~AE2 Chromium
AG_AE2 Silver
Test Codes and Names
1311 TCLP Metals/SemiVols Extr.
CD AE2 Cadniium
CR~AE2 Chromium
AG~AE2 Silver
Method
sw-846, 1311
sw-846, 6010
SW-846, 6010
sw-846, 6010
Method
sw-846, 1311
SW-846, 6010
SW-846, 6010
SW-846, 6010
Workorder Comments
Report: THESE ARE RERUN SAMPLES ORIGINALLY SUBMITTED AS SAMPLES
OIA AND 03A ON WORK ORDER #9404012.
Page 1 of 3
TTiis is to certify that the following samples were anatyzed using good laboratory practices
to show the following results.
Sample ID: M-39; PT OF DIS SURFACE. Lab ID: 9406037-OlA CoUected: 04/14/94 10:50:00
TEST
TCLF Metals/SemiVols Extr.
Cadmium
Chromium
Silver
RESULT
06/30/94
16600
U
70.1
UNITS
DATE
ug/L
ug/L
ug/L
DETECTION
LIMIT
2
5
3
ANALYZED
07/05/94
07/05/94
07/05/94
BY
LVD
LVD
LVD
LVD
METHOD/CAS#
SW-846, 1311
SW-846, 6010
SW-846, 6010
SW-846, 6010
Sample ID: M-39;25 FT DN GRAD SURFACE Lab ID: 9406037-02A CoUected: 04/14/94 11:05:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
TCLP Metals/SemiVols Extr. 06/30/94 DATE
Cadmium 11700 ug/L
Chromium 21.1 ug/L
/er 106 ug/L #e
LVD
2 07/05/94 LVD
5 07/05/94 LVD
3 07/05/94 LVD
SW-846, 1311
SW-846, 6010
SW-846, 6010
SW-846, 6010
#
Page 2 of 3
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was beiow detection lim^
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. l.U with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the calibration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
Page 3 of 3
ENVIRONMENTAL LAB WORK REQUEST
#
^^^^/ 7
TfflOKOL ENVIRONMENTAL LABORATORY LWR No. E10412
/}i F. \/[/AL/(£rf^
BTRNaON
6'590
contxmtR
lA40^
WOBKOUBR
/6940 S--23-94
ORGAraZATION
ENVlfZO £vVfijS_
MAIL STOP
:5o/e'
UPOBT UBU.T8 TOi
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS
1. ^UiMU ^^Z
:5>/j-ff AA-9 (Z/S' \AOc - S^4o
Mercur.4 - 7*7^
/2/5T CJ^Cr^_Fi^
IfAJit.HJihvjI^CCri'i ' lAtu^
^'ZZ-^ y^ AA-i ^o/o
i'^ ^K .-^^^ .^:n. ~
\.Al Trr^o'tr^rTTTTi.
Cd, Cr, A9, Fh -G>o7o'
Ata - •f47o ~-7»gr^ga^ IP -ytt^ -fZtcr M>r a R^i
.J' ^' I'J ^-^
la
CHAIN OF CUSTODY
RRUNQUSHEDBY
1 .liJ^/L.
DAIE
s-zz'f4
TIME
/46d
RECEIVED BY
//^//J?..y^^
DATE
-^->/'f)^
TIME
/(AAA
FOR LABORATORY USE ONLY
4 DATC COMnnVD DATCUFORTCD aCNAIVIIB
June 29, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page l
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty. Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order # 9405027
LabID: Sample ID:
OIA M-9 STRAND BURNER, ORAB
Sample and Test Code Identification
Test Codes and Names
NO
CD FL2
CR FL2
PBn.2
HG CV2
AG FL2 8240
HMX
Nitroglycerine
Cadinium
Chromium
Lead
Mercuiy
Silver
Volatile Organics
HMX
Workorder Cnmments
Method
SOP
sw-846, 7130
SW-846, 7190
SW-846, 7420
SW-846, 7471
SW-846, 7760
SW-846, 8240
SW-846, 8330
TTiis is to cenify that the following samples were analyzed using good laboratory practices
to show the following results.
m
Sample ID: M-9 STRAND BURNER, GRAB Lab ID: 9405027-01A CoUected: 05/23/94 12:15:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
^ -OUL
Nltroglycerine
Cadmium
Chromium
Lead
Mercury
Silver
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorometheme
Bromofonn
Bromomethane
2-Butanone
r
3on disulfide
bon tetrachloride
orobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexanone
trans-l,2-Dichloroethene
1,2-Dichloropropeme
cis-l,3-Dichloropropene
trans-l,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2-Pentemone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Tri chloroethene
Trichlorofluorometheme
Vinyl Acetate ttorl Chloride pyiene
omochlorometheme
u
u
3590
125
0.509
1.6
410 B
U
U
U
U
U
U
D
U
U
D
U
D
U
U
U
U
D
D
D
U
U
U
U
D
D
U
U
U
U
U
U
U
D
11 B
U
3
U
D
D
U
166094
mg/Kg
ug/g
ug/g
ug/g
mg/Kg
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.04
0.25
2.5
2.5
0.043
0.25
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
06/24/94
05/26/94
05/26/94
05/26/94
05/25/94
05/26/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
05/24/94
CFP
LVD
LVD
LVD
CRS
LVD
JMA
OMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SOP
SW-846, 7130
SW-846, 7190
SW-846, 7420
SW-846, 7471
SW-846, 7760
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
INTSTDl
June 29, 1994 08:45 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 2
Sample ID: M-9 STRAND BURNER, GRAB Lab ID: 9405027-01A CoUected: 05/23/94 12:15:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
1,4-Difluorobenzene
Chlorobenzene-dS
HMZ
784837 ug/Kg
615648 ug/Kg
Surrogate/Recovery Data
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
D mg/Kg
SW-846, 8240
05/24/94 JMA INTSTD2
05/24/94 JMA INTSTD3
For Volatile Organics 8240
%Recovery Recovery Limits
97.6 88 TO 110
94.7 86 TO 115
91.1 76 TO 114
0.01 06/02/94 CFP SW-846, 8330
#
•
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1.1J with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ENVIRONMENTAL LAB WORK REQUEST
^'/'A^^A 9
"= THIOKOL ENVIRONMENTAL LABORATORY
FBOM:
1 ORGAraZAHON
RXTBhBION
5^9o
MAIL (TOP
-30/6'
LWR No. E10426 1
COSTCSNTOt
A460
woBKoaiai
/B940
DATC
7Jcw^9^
BDORT BBBULTS TOi
HELEN WARD, MS 301
u
\y
v^
«y
t^
u-
1/
SAMPLE
1. £i4/i11C^*<i>*2.
3. S'fa'^o •'C'*?-
Pt of •Di\ J t-U
la
11.
11
DATE
7iJtiiim94
TJovef^
iJUMSff
7Jumrff
©Jwuffi
5 Ju«»f^
$>)-«•?<
eju«.?i
ej^'^-T'
TVPE
G
y/
i^
^
1^
^
1^
y
•-
1^
c
SAMPLE INFORMATION
UX:ATION
M-40
/A-40
/U'4o
/U-40
IU -205"
AA.- ZO'S"
/U-I0T
M- 7.0 S~
^('^i>$^
TIME
1346-
/s^s-
/4£>0
/4r^
9:%1
<?;-?<-
9:4C
/o:oz
/0\/O
TEST
/(//Zi<ft/' - ^/<s>
AifCCiA-6<f/o
A/'Cik( - 6O/0
M/c/t^ -6O/0
Lee.J -^olO
<^Uan7<L9 - 9o/0
p// - ia4<^
j>*/- /b^fr
pH-f04^
pf^'ie>4^r
REMAiRKS
1
5<*tfifc'Soo\ 1
pH -9o4rr II
/(
n
^(
1 t
. i
CHAIN OF CUSTODY
KFUNQUISHESBY
ALX//JielJ~-~^
DATE
9^0^94
TIME
(OSO
RBCQVBJBY
//A^y/A.... ^
DATE
'A.'^'^y-
TIME
/£> 91>
FOR LABORATORY USE ONLY
II iMTCa>Mium> DATC REFOItTB) acNAivnt
July 21, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
•
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
WorkOrder);^ 9406009 Sample and Test Code Identification
LabID: Sample ID:
OIA M-40; PT. OF DIS SURFACE.
LabID: Sample ID:
02A M-40; PT OF DIS 2 FT.
LabID: Sample ID:
03A M-40; 25 FT DN GRAD SUR.
LabID: Sample ID:
04A M-40; 25 FT DN GRAD 2 FT.
#
LabID: Sample ID:
^05A M-205; FT OF DIS SURFACE
LabID: Sample ID:
06A M-205; PT OF DIS 2 FT.
LabID: Sample ID:
07A M-205;PT OF DIS 2 FT. DUP.
LabID: Sample ID:
08A M-205; 25 FT. DN ORAD SUR.
LabID: Sample ID:
09A M-205; 25 FT. DN ORAD 2 FT
Test Codes and Names
NI AE2 Nickel
Pri^S pH (SoU)
Test Codes and Names
NI_AE2 Nickel
PH_S pH (Soil)
Test Codes and Names
NI AE2 Nickel
PH^^S pH (Soil)
Test Codes an A Names
NI A£2 Nickel
PHlS pH (Soil)
Test Codes and Names
S04IC1 Sulfate
PB AEZ Lead
CI>r^WT2 ToUl Cyanide
PH_S pH (Soil)
Test Codes and Names
S04IC1 Sulfate
PB AE2 Lead
CN^WT2 Total Cyanide
PH_S pH (Soil)
Test Codes and Names
S04IC1 Sulfate
PB AE2 Lead
Cl^ vm Totol Cyanide PH_S pH (Soil)
Test Codes and Names
S04IC1 Sulfate
PB AE2 Lead
CN^WT2 Total Cyanide
PH_S pH (Soil)
Test Codes and Names
S04IC1 Sulfate
PB_AE2 Lead
CN_WT2 Total Cyanide
PH_S pH (Soil)
Method
SW-846, 6010
SW-846,9045A
Method
SW-846, 6010
SW-846,9045A
Method
SW-846, 6010
SW-846,9045A
Method
SW-846, 6010
SW-846,9045A
Method
EPA 300.0
SW-846, 6010
SW-846, 9010
SW-846,9045A
Method
EPA 300.0
SW-846, 6010
SW-846, 9010
SW-846,9045A Method
EPA 300.0
SW-846, 6010
sw-846, 9010
SW-846,9045A
Method
EPA 300.0
sw-846, 6010
SW-846, 9010
SW-846,9045A
Method
EPA 300.0
sw-846, 6010
SW-846, 9010
SW-846,9045A
#
Workorder rnnnnftnts
Certmed ^
This is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: M-40; PT. OF DIS SURFACE. Lab ID: 9406009-OlA CoUected: 06/07/94 13:45:00
TEST RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Niclcel 12.2 ug/g 0.64 07/06/94 LVD SW-846, 6010
pH (Soil) 8.44 pH Unit 06/08/94 AA SW-846,9045A
Sample ID: M-40; PT OF DIS 2 FT. Lab ID: 9406009-02A CoUected: 06/07/94 13:55:00
TEST RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Hickel 16.3 ug/g 0.58 07/06/94 LVD SW-846, 6010
pH (Soil) 8.26 pH Unit 06/08/94 AA SW-846,9045A
Sample ID: M-40; 25 FT DN GRAD SUR. Lab ID: 9406009-03A CoUected: 06/07/94 14:00:00
m RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Nickel 7.28 ug/g 0.59 07/06/94 LVD SW-846, 6010
pH (Soil) 8.25 pH Unit 06/08/94 AA SW-846,9045A
Sample ID: M^W; 25 FT DN GRAD 2 FT. Lab ID: 9406009-04A CoUected: 06/07/94 14:15:00
TEST RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Nickel 12.9 ug/g 0.60 07/06/94 LVD SW-846, 6010
pH (Soil) 8.13 pH Unit 06/08/94 AA SW-846,9045A
Sample ID: M-205; PT OF DIS SURFACE Lab ID: 9406009-05A CoUected: 06/08/94 09:39:00
TEST RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Sulfate
d #
35
20.8
ug/g
ug/g
3
1.4
06/28/94
07/06/94
CRS
LVD
EPA 300.0
SW-846, 6010
July 21, 1994 07:20 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 2
Sample ID: M-205; PT OF DIS SURFACE Lab ID: 9406009-05A CoUected: 06/08/94 09:39:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Total Cyanide
pH (Soil)
0.307 mg/Kg
8.40 pH Unit
0.150 06/21/94 KEN
06/08/94 AA
SW-846, 9010
SW-846,9045A
Sample ID: M-205; PT OF DIS 2 FT. Lab ID: 9406009-06A CoUected: 06/08/94 09:46:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Sulfate
Lead
Total Cyanide
pH (Soil)
99.5
11.2
0.182
8.31
ug/g
ug/g
mg/Kg
pH Unit
3
1.6
0.150
06/28/94
07/06/94
06/21/94
06/08/94
CRS
LVD
KEN
AA
EPA 300.0
SW-846, 6010
SW-846, 9010
SW-846,904 5A
Sample ID: M-205;PT OF DIS 2 FT. DUP. Lab ID: 9406009-07A CoUected: 06/08/94 09:46:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Sulfate
Lead
Total Cyanide
pH (Soil)
161
9.22
0.229
8.39
ug/g
ug/g
mg/Kg
pH Unit
3
1.5
0.150
06/28/94
07/06/94
06/21/94
06/08/94
CRS
LVD
KKN
AA
EPA 300.0
SW-846, 6010
SW-846, 9010
SW-846,9045A
Sample ID: M-205; 25 FT. DN GRAD SUR. Lab ID: 9406009-08A CoUected: 06/08/94 10:02:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Sulfate
Lead
Total Cyanide
pH (Soil)
88.2
13.3
0.245
8.86
ug/g
ug/g
mg/Kg
pH Unit
3
1.5
0.150
06/28/94
07/06/94
06/21/94
06/08/94
CRS
LVD
KEN
AA
EPA 300.0
SW-846, 6010
SW-846, 9010
SW-846,9045A
July 21, 1994 07:20 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 3
sRi pie ID: M-205; 25 FT. DN GRAD 2 FT Lab ID: 9406009-09A CoUected: 06/08/94 10:10:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Sulfate
Lead
Total Cyanide
pH (Soil)
87.0
12.9
0.261
8.27
ug/g
ug/g
mg/Kg
pH Unit
3
1.5
0.150
06/28/94
07/06/94
06/21/94
06/08/94
CRS
LVD
KEN
AA
EPA 300.0
SW-846, 6010
SW-846, 9010
SW-846,9045A
#
•
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection Um9
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectnd data indicated the presence of a
compound that meets the identiiication criteria but the result is less than the specified
detection Umit but greater than zero. (e.g. 1. IJ with a detection Umit of 5.0)
B This flag is used when an analyte is found in the blank as weU as die sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ENVIRONMENTAL LAB WORK REQUEST
'7<^Y'^Y^/ -?
Wt- THIOKOL ENVIRONMENTAL LABORATORY
niOM:
ORGAha ZATION
1' =— =^
BmNSON
:5-39o
MAILITOP
LWR No. E10433
ll
OOSTCSMTBl
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WORK ORDSa
/3J40
DAIS
/SjuMtr94
REPORT RBSULTB TOi 1
HliLEN WARD, MS 301
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SAMPLE INFORMATION
LOCATION
T'2IL:>
T'ZiV
T'ZID
r-c>A
r-(^A
r-(,A-
T^GA
TIME
/44D
J440
/45C
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Ser Icrt/OiV
- 'B24^>
- 'B24(^
- 9 24^
- 6^/0 yH -
II
ll
/{
REMARKS
9HT
CHAIN OF CUSTODY
REUNQUISHEDBY
/
SUiLi^c^ U-^AAi
DATE
y^y/.i/
TIME
<^f/J-
RECEIVQ>BY
//yf^/^^y....^
DATE
-Y^./^^f^
TIME
AP9/X-
FOR LABORATORY USE ONLY
^
DATE COMPLETED OATBREFORTBD nCNATURB
July 15, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page l
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty. Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Orders 9406017
LabID: Sample ID:
OTA T-21D; PT OF DIS SURFACE
Lab ID: Sample ID:
^ T-2 ID; PT OF DIS SUR. DUP.
LabID: Sample ID:
03A T-21D; FT OF DIS 2 FT.
04A T-6A; FT OF DIS SURFACE
tab ID: SamplelD:
05A T-6A; PT OF DIS 2 FT.
Sample and Test Code Identificatinn
Test Codes and Names
8240 Volatile Organics
Test Codes and Namas
8240 Volatile Organics
Test Codes and Names
8240 VoUtile Organics
Test Codes and Namas
SE OF2 Selenium
PH^S pH (Soil)
LabID: Sample ID:
06A T-6A; 22FT DN ORAD SURFACE
l4bID: SamplelD:
07A T-6A; 22FT DN ORAD 1.5 FT.
Test Codes and Names
SE aF2 Selenium
PlTs pH (Soil)
Test Codes and Names
SE 0F2 Selenium
PH~S pH (SoU)
Test Codes and Names
SE OF2 Selenium
PUTS pH (SoU)
Method
sw-846, 8240
Method
SW-846, 8240
Method
SW-846, 8240
Method
sw-846, 7740
SW-846,904SA
Method
sw-846, 7740
SW-846,9045A
Method
sw-846, 7740
SW-846,904SA
Method
sw-846, 7740
SW-846,9045A
Workorder Cnmmpnts
Certri
^^^7-^
m^f
77MS is to certify that the following samples were anatyzed using good laboratory practices
to show the following results.
•
Sample ID: T-21D; PT OF DIS SURFACE Lab ID: 9406017-OlA CoUected: 06/13/94 14:40:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromometheme
2-ButcUione
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroetheme
1,l-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
ijj^-Dichloropropane
HB-1,3 -Dichloropropene
irons -1,3 -Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Te trachloroethene
Toluene
1,1,l-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Tri chlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
35
U
D
U
D
U
U
D
D
U
D
U
D
D
U
D
U
D
U
U
D
U
U
D
O
U
U
D
U
U
D
U
D
D
U
BJ
U
U
U
D
U
D
DNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
50
50
50
50
50
50
50
50
50
SO
50
50
50
SO
SO
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
ANALYZED
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
oe/is/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA.
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene-d8
Bromofluorobenzene
1,2 -Dichloroetheme-d4
%Racovary
94.9
92.6
86.4
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
88
86
76
TO 110
TO 115
TO 114
•
July 15, 1994 13:42 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 2
Sample ID: T-21D; PT OF DIS SUR. DUP. Lab ID: 9406017-02A CoUected: 06/13/94 14:40:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromoform
Bromomethane
2-But6mone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexcmone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-l,3-Dichloropropene
trans-1,3 -Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
28
U
D
U
U
U
D
U
U
U
D
D
O
a U
U
U
D
U
U
u u u
u u D
U
D
U
U
U
U
U
U
U
BJ
U
U
U
D
D
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
ANALYZED
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene-d8
Bromofluorobenzene
1,2 -Dichloroetheme-d4
%Recovary
95.8
93.6
85.7
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5 ^^
10061-02-6 ^^
95-50-1 ^^
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
88
86
76
TO 110
TO 115
TO 114
July 15, 1994 13:42 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 3
Sffi] pie ID: T-21D; PT OF DIS 2 FT. Lab DD: 9406017-03A CoUected: 06/13/94 14:50:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromofonn
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chl orobenz ene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropane
^|*B-1,3-Dichloropropene
W Hbs -1,3 -Dichloropropene
x^-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroetheme
Trichloroethene
Tri chlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
15
Surrogati
Surrogate
Toluene-d8
U
u U
D
D
U
u U
U
u u D
U
U
D
D
U
U
D
U
U
D
U
U
D
U
U
U
U
U
D
U
U
U
BJ
U
U
U
D
U
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
50
50
50
50
SO
50
50
50
50
50
50
50
50
50
SO
SO
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
ANALYZED
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
06/16/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
OMA
JMA
JMA
JMA
JMA
JMA
JMA
s/Recovery Data For Volatile Organics 8240
Bromofluorobenzene
1,2 -Di chloroethane-d4
%Recovery
97.0
96.7
87.8
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
88
86
76
TO 110
TO 115
TO 114
m
July 15, 1994 13:42 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 4
Sample ID: T-6A; PT OF DIS SURFACE LabID: 9406017-04A CoUected: 06/13/94 15:18:00
TEST RESXTLT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Selenium
pH (Soil)
0.45 ug/g
9.56 pH Unit
0.093 07/08/94 CRS
06/08/94 AA
SW-846, 7740
SW-846,9045A
Sample ID: T-6A; PT OF DIS 2 FT. LabID: 9406017-05A CoUected: 06/13/94 15:22:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METEOD/CAS#
Seleniiun
pH (Soil)
0.49 ug/g
8.59 pH Unit
0.086 07/08/94 CRS
06/08/94 AA
SW-846, 7740
SW-846,9045A
Sample ID: T-6A; 22FT DN GRAD SURFACE Lab ID: 9406017-06A CoUected: 06/13/94 15:33:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Selenium
PH (Soil)
0.19 ug/g
8.81 pH Unit
0.084 07/08/94 CRS
06/08/94 AA
SW-846, 7740
SW-846,9045A
Sample ID: T-6A; 22FT DN GRAD 1.5 FT. Lab ID: 9406017-07A CoUected: 06/13/94 15:40:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METEOD/CAS#
Selenium
pH (Soil)
0.20 ug/g
8.54 pH Unit
0.079 07/08/94 CRS
06/08/94 AA
SW-846, 7740
SW-846,9045A
•
m
m
Data Reportmg Qualifiers
U Compound was analyzed for but not detected. Indicates conipound was below detection liinit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection Umit but greater than zero. (e.g. 1.IJ with a detection liinit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection Umits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
June 15, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page l
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER. M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order << 9403026
LabID: Sample ID:
OIA 0322941; LOT #218
LabID:
02A
Sample ID:
0322M2; LOT #218
LabID:
03A
lelD:
0322943; LOT «24
Sample and Test Code Identification
Test Codes and Names Method
CN_WT2 Toul Cyanide SW-846, 9010
Test Codes and Names
3050
AL AE2
SB AE2
BA AE2
BE AE2
CD AE2
CA AE2
CR AEZ
CO AE2
CU AEZ
FE AE2
PB AE2
MG AE2
MN AE2
MO AE2
Nl AE2 K AE2
AG AE2
NA AEZ
V AE2
ZR AE2
AS aF2
HO CV2
SE GF2
TL_aF2
Acid Digestion
Aluminum
Antimony
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel Potassium
Silver
Sodium
Vanadium
Zinc
Arsenic
Mercury
Selenium
Thallium
Test Codes and Names
8240
8270
Volatile Organics
Semi-Volatile Organics
Workorder Comments
Method
SW-846, 3050
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 7841
Method
SW-846, 8240
SW-846, 8270
Certmed By
This is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
•
Sample ID: 0322941; LOT #218 LabID: 9403026-OlA CoUected: 03/22/94
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Total Cyanide 178.2 mg/Kg 10.0 04/22/94 KEN SW-846, 9010
Sample ID: 0322942; LOT #218 LabID: 9403026-02A CoUected: 03/22/94
TEST RESULT UNITS DETECTION ANALYZED
LIMIT
BY METHOD/CAS#
Acid Digestion
Aluminum
Antimony
Barium
Beryl li\im
ffl mlum
cium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Silver
Sodium
y;MSdium 1
05/11/94
7070
33.5
279
95.4
95.2
3780
159
92.5
105
9640
139
2050
196
183
149
2970
84.5
684
73.0
109
DATE
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
2.3
4.6
0.09
0.2
0.2
0.92
0.5
0.3
0.2
0.5
2.3
0.09
0.2
0.3
0.92
36.6
0.3
0.92
0.3
0.4
05/11/94
05/16/94
05/16/94
05/16/94
05/16/94
05/16/94
05/16/94
05/16/94
05/16/94
05/16/94
05/16/94
05/16/94
05/16/94
05/16/94
05/16/94
05/16/94
05/16/94
05/16/94
05/16/94
05/16/94
05/16/94
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
3050
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
6010
June 15, 1994 14:09 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 2
Sample ID: 0322942; LOT #218 LabID: 9403026-02A CoUected: 03/22/94
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Arsenic
Mercury
Selenium
Thallium
134
5.56
108
98
ug/g
ug/g
ug/g
ug/g
0.05
0.027
0.05
0.05
04/25/94
04/22/94
04/25/94
04/25/94
CRS
CRS
CRS
CRS
SW-846,
SW-846,
SW-846,
SW-846,
7060
7471
7740
7841
Sample ID: 0322943; LOT #324 LabID: 9403026-03A CoUected: 03/22/94
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chl oroe thauie
2-Chloroethylvinyl ether
Chloroform
ChlorometheUie
Dibromochloromethcine
1,1-Dichloroethane
1,2-Dichloroethane
1,l-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,l-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
Tri chlorofluoromethane
RESULT
17.3BJ
U
U
35.9
53.0
58.3
U
32.6
U
189
20.3
U
U
120
U
U
U
120
U
U
U
U
U
U
50.6
99.7
95.8
103
155
182
47.8
U
48.8
53.3
41.6
U
59.4
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
50
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
10
50
10
10
10
10
10
10
10
10
ANALYZED
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
67-G4-1
107-02-8
107-13-1
71-43-2
75-27-4 ^^
75-25-2 ^M
74-83-9 ^m
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5 ^^
79-01-6 ^B
75-69-4 ^^
June 15, 1994 14:09
Sample ID: 0322943; LOT #324
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 3
LabID: 9403026-03A CoUected: 03/22/94
TEST
Volatile Organics
Vinyl Acetate
vinyl Chloride
o-Xylene
Bromochlorometheme
1,4-Difluorobenzene
Chlorobenzene-d5
RESULT
U
U
117
219953
1019466
848005
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
ANALYZED
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
Semi-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2 -Chlorophenol
1^ -Dichlorobenzene
^II^Dichlorobenzene
^j^^yl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)metheme
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
Acenaphthylene
3-Nitroemiline
Acenaphthene
2^-Dinitrophenol
iBitrophenol
^lyinz of urem
2,6-Dinitrotoluene
U
U
U
U
3710
U
950
U
6430
187J
U
922
U
U
U
U
U
U
U
U
U
1080
1590
U
U
U
U
U
4210
8410
U
U
U
U
U
U
U
U
9020
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
102
101
99.1
330
330
330
330
330
330
330
660
330
330
330
330
330
330
330
330
330
330
1700
330
330
330
330
660
330
660
330
330
330
330
330
1700
330
330
1700
330
1700
1700
330
330
METHOD/CAS#
SW-846, 8240
108-05-4
75-01-4
95-47-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
88
86
76
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
TO 110
TO 115
TO 114
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-G7-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
June 15, 1994 14:09 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 4
Sample ID: 0322943; LOT #324 LabID: 9403026-03A CoUected: 03/22/94
TEST
Semi-Volatile Organics
2,4-Dinitrotoluene
Diethylphthalate
4 -Chlorophenyl-phenylether
Fluorene
4-Nitroemiline
4,6-Dinitro-2-methylphenol
n-Ni trosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenemthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
bis (2-Ethylhexyl)pht:halate
Chyrsene
Di-n-octylphthalate
Benzo[b&k]fluoremthene
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h]anthracene
Benzo[g,h,i]perylene
1,4-Dichlorobenzene-d4
Naphthalene-d8
Acenaphthene-dl0
Phenemthrene-dl0
Chyrsene-dl2
Perylene-dl2
2
RESULT
6080
U
U
5340
U
U
U
U
U
10500
2150
785
402
U
10600
16900
2190
llOOOB
Int.
Int.
Int.
Int.
Int.
Int.
Surrogat
2750
U
U
U
U
U
U
Std.
Std.
Std.
Std.
Std.
Std.
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
e/Recovery Data
Surrogate
-FLUOROPHENOL
Phenol-d5
Ni t robenz ene-dS
2
2
1
-Fluorobiphenyl
,4,6-Tribromophenol
•erpt lenyl -dl4
DETECTION
LIMIT
330
330
330
330
660
1700
330
330
330
1700
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
ANALYZED
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
03/29/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5 ^
53-70-3 ^P
191-24-2
-
-
-
-
-
-
For Semi-Volatile Organics 8270
%Recovery
53.11
57.37
55.99
71.25
88.94
92.72
Recovery Limits
21
10
35
43
10
33
TO 100
TO 94
TO 114
TO 116
TO 123
TO 141
•
#
#
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identiiication criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1. IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ENVIRONMENIAL
RESOURCE ASSOCIATES
Arvada, Colorado 80002 1-800-ERA-0122 ^
Certification
PrlorltyPollutnT7CLP Quality Control Standards
Organics In Soil
Parameter
Volatiles
Benzene
Bromodichloromethane
Bromofomi
Cart>on tetrachloride
Chlorobenzene
Chloroform
1.2-Dibromoethane
1.2.0ichlorobenzene
1,4.0ichlorot>enzone
1.2.Dichloroethane
Ethylbenzene
Methylene chloride
4-Methyl-2.pentanone
Styrene
Tetrachloroethylene
1,1,1 'Trichloroethane
Trichloroethylene
Toluene
p-Xylene
Base/Neutrals
Anthracene
Benzo(a)anthr8cene
Butylbenzylphthalate
Carbazole
Ctvysene
OilMnzofuran
1,2.0ichlorot>enzene
1,4.Dichlorobenzene
2,4-Dinitrotoluene
bis(2-Ethylhexyl)phthalate
Fluorene
Naphthalene
Phenanthrene
Pyrof»e
1,2,4-Trichloroberaene
Adds
2-ChloFophenol
244ethylphenol
4-Methylplienol
Pentachlorophenol
2.4.5-Trichlorophenol
2,4,6-Trichlorophenol
Pesticides
Aldrin
beta-BHC
gamma-BHC (Undane)
4,4'-DDD
4,4'-ODE
4,4'-DDT
Dieidrin
Endrin
Heptachlor
Methoxycttlor
Lot No. 324
Certified
Value
ug/Kg
36.5
60.0
59.0
1S2
21.3
127
109
44.4
62.4
127
105
166
180
50.8
52.1
45.6
63.5
55.9
119
1010
2030
10600
1540
2350
6790
13100
2550
5000
7120
6060
1640
1570
8030
1210
5080
2020
10000
12200
7990
4560
246
145
219
334
455
287
101
407
297
160
Advisory
Range
ugrtCg
14
21
27
134
7.8
65
60
26
49
62
39
58
54
15
33
24
45
26
56
273
670
1590
462
400
3820
3760
550
1950
1140
2670
623
848
4180
532
1170
283
1400
1710
2960
1690
103-
25-
70-
104-
137.
72-
36-
122-
101 •
61 .
-55
-93
-100
-269
-34
-175
-142
-69
-129
-197
-170
-367
-288
•81
-77
-74
-100
•84
-159
-1340
-2900
-16100
• 2460
• 3950
•7670
• 16900
-3160
-6950
-11200
-7330
-2180
-1880
• 0230
• 1720
• 6810
• 2320
•10900
.21500
11500
6570
300
213
278
471
660
459
147
598
330
253
(1) CartilM values tn equal to 100% of OKti paramstor kl the MicaM (tandwd.
(2) Advisory ranges are listed as guidelines for acoeptabia leceveries given the imilationt of the EPA methodolagies commonly used to
detemiine these parameteis. The range dosely approximates the 05% oonlidenca interval (or parametert based upon the experimental
data generated by ERA and data Itom ttie USEPA Vff>, WS and CU> intertalwratory perfonnance evaluation program.
-4^
EIMVIROIMIMENIAL
RESOURCE ASSOCIATES
Arvada. Colorado 80002 1-800-ERA-0122 (^
# Certification
PrlorltyPollutnT"/CLP Quality Control Standards
#
Inorganics In Soil
Parameter
Trace Metals PrlorttyPollutnT''
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
CobaH
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Molyl>dsnum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Cyanide PriorityPollutnT™
Total cyanide
Lot No. 218
Certified
Value
mg/Kg
4800
43.9
128
276
95.1
102
3680
154
95.8
119
8640
147
1830
191
4.85
154
163
2200
101
82.5
594
102
81.8
120
mg/Kg
177
Advisory
Range
mg/Kg
1920
18
48
193
57
51
2580
69
53
60
5180
66
1010
134
2.7
85
81
1320
52
37
327
51
57
60-
-6720
-205
-190
-358
-143
-164
-5150
-215
-144
-179
-12100
-213
-2750
-267
• 7.5
.253
252
2830
162
136
891
152
115
186
mg/Kg
71 • 301
#
(1) T))e Trace Metals Certitied Values are equal to the mean recoveries for each parameter as determined in an interlaboratory round robin
study. The standard was digested using Method 3050, SW-B48 and ttie digest analyzed by ICP and atomic absorption spectroscopy.
(2) The Cyanide Certified Value is equal to ttie mean recover as detennined in an intertaboratory round robin study. The standard was
digested and analyzed following ttie procedure outtined in Method 0010, SW.84S.
(3) Advisory ranges are listed as guidelines (or acoeptable recoveries given the limitations o) the EPA methodolagies commonly used to
determine these parameters. The range closely approximates ttie 85% confidence interval lor parameters based upon ttie experimental
data Irom ttiis lot. previous ERA lots, and published USEPA data.
A^
ENVIRONMENIAL
RESOURCE ASSOCIATES
Arvada, Colorado 80002 1-800-ERA-0122
^
Certification
PriorltyPollutrir"/CLP Quality Control Standards
Inorganics in Soil
Parameter
Trace Metals PriorityPollutnT^
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
MolytxJanum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Cyanide PriorityPollutnT^
Total cyanide
Lot No. 218
Certified
Value
mg/Kg
4800
43.9
128
276
8S.1
102
3680
154
95.8
119
8640
147
1830
181
4.85
154
163
2200
101
92.5
594
102
81.8
120
mg/Kg
in
/Ulvlsory
Range
mg/Kg
1920
18
48
193
57
51
2580
69
53
60
5180
66
1010
134
2.7
85
61
1320
52
37
327
51
57
60
-6720
-205
-190
-358
-143
-164
-5150
•215
-144
-179
•12100
-213
• 2750
•267
•75
•253
252
-2030
•162
•136
• 881
•152
•115
-186
mg«g
71 -301
(1) The Trace Metals Certified Values are equal to ttie mean recoraries for each parameter at detenmined In »i> interUboratory round robin
study. The standanl was digested using Mettiod 3050, SW-B4e and ttie digest analyzed by CP and atomic abtoiptton specttoecopy.
(2) The Cyanide Certified Value is equal to the mean recovery as detennined in an intertaboratory round robin study. The standard wat
digested snd analysed tollmving ths pioesdura outtined in IMattiod S010, SW.S46.
(3) Advisory ranges are listed aa guidelines tor aeeeptable leooveries given ttie limitatiant cf ttie EPh methodologies commonly used to
detennine ttiesa parameters. The range closely approximates ttia 65% confidence intoival for parameters baaed upon ttie experimantal
data (rom this tot, previous ERA lots, and published USEPA data.
Environmental Resource Associates
Interlaboratory Analytical Data - PriorityPoiiutnT/CLP™
#
•
Organics In Soil
Parameter
Volatiles
Benzene
Bromodkrhkxomethane
Bromoform
Cartxin tetrachloride
ChkMobenzene
Chlorofonn
1,2-Dibroinoethane
1,2-DichlorDbenzer)e
1,4-Dichlorobefuene
1,2-Dichloroethane
Ethylbenzene
Methylene chloride
4-Methyl-2-pentanone
Styrene
Tetrachkiroethylene
1,1,1-Trichloroethane
Trichloroethylene
Toluene
p-Xylene
Base/Neutrals
Anthracene
Benzo(a)anthracene
Butylbeiizylphthalate
Cait>azole
Chrysene
Ditienzofuran
1,2-Oichlorobenzene
1,4-Dichk>rot>enzene
2,4-Dinitrotoluene
bis(2-Ettiylhexyl)phthalate
Fluorene
Naphthalene
Phenanthrene
Pyrene
1,2,4-Trichlorobenzene
Acids
2-Chlorophenol
2-Methylphenol
4-Methylphenol
Pentachlorophenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Pesticides
Aldrin
beta-BHC
gamma-BHC (Lindane)
4,4'-DDD
4,4'-DDE
4,4'-DDT
Oieldrin
Endrin
Heptachlor
Metfwxychkir
Lot No. 324
Certified
Value
ugn<g
36.5
60.0
58.0
192
21.3
127
109
44.4
82.4
127
105
166
180
50.8
52.1
45.6
63.5
55.9
119
1010
2030
10600
1540
2350
6790
13100
2550
5000
7120
6060
1640
1570
8030
1210
5080
2020
10000
12200
7990
4560
246
145
219
334
455
287
101
407
287
160
Mean
Recovery
ug/Kg
36.0
54.7
64.7
185
22.0
125
121
48.8
85.3
129
109
146
188
53.9
522
44.7
59.1
56.4
128
552
1140
8570
869
1420
4530
5880
829
3170
6110
3720
1050
1090
4570
788
2850
625
3340
5220
5170
2780
188
135
154
262
378
239
89
324
242
154
Mean
Recovery (%)
98.6%
91.2%
110%
96.4%
103%
88.7%
111%
110%
103%
101%
104%
88.2%
105%
106%
100%
88.1%
93.1%
101%
108%
54.7%
56.2%
80.8%
56.4%
60.4%
66.7%
44.9%
36.4%
63.4%
85.8%
61.4%
64.0%
69.4%
56.9%
65.2%
56.1%
31.0%
33.4%
42.8%
64.7%
61.0%
80.4%
93.3%
70.2%
78.4%
83.3%
83.3%
87.7%
79.6%
81.5%
96.0%
n
9
9
8
9
9
8
4
8
8
8
8
7
8
8
8
8
9
9
9
9
10
10
9
10
10
10
10
10
8
10
9
10
10
9
10
10
10
10
10
10
10
7
7
10
10
7
7
10
10
7
(1) The interlatxiratory /knalyt'cal Oata Summary illustrates typical recoveries obtained by laboratories
using EPA methodologies.
ENVIRONMENTAL LAB WORK REQUEST '^JAl^AlA/
]» THIOKOL ENVIRONMENTAL LABORATORY LWR No. E10436
A. P. WALJ^F^ S^9D
COSTCSNTBR
\A4DZ>
woBKoaneB
im4d
MIS
^ OBCAMZATION
^NUiTtp e^GK 30//:^
BEFOBT BBSULIS TOt
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYFE LOCATION TIME TEST KEMASKS
A( &ri 7 / SurA, t^/to/t^ e of H- 20S /OlO fAoc ' SZ4o
^S Iff MO Z03 'Aio^fj b, \^ E o/-M'Zo'i^ /OIO
Cd ,Cr,A'i.Ph,^c-iO'o
H-^ ' f4lQ
'••SlOMO X0%
&rd 7,. -i. fr Ci/zo/ff t^ £• c>/ M- 203 lOZO VDC - <8Z^O
'/^/n 1/ ^ o/M'Zo3 /Oto Cd, Ct, As, f*i>t Bc-C>otD
Ht -• 74-7g
OrA 3Z,SurL ib. 0,, 5^ l^ E o/M-7»Z /03© i/dc ' &i4^
QfA-ht. IU
y^^f 1/
7^-7
^ ^)yg >Q'203 /o3& 1 /7^ - -7^7^
tMa 1/
7—7
1^ oA/U'tdl> Ib^O Voc ' BZ4o
1^' ^ oAlX'Zo-b tt4o /V^- 741Q
JC ^, '»f «^ Sc>/M'Zc)l, /OS'O VOC' ^Z4o
ard^4 ^SwL. ''H"^ <^ £oA /U-203 IPSO
Cd,Cr,A^ ,?h, Sc-^/c
/^j - 7f 7n
^^10/4^ £-of ^-7^3 //or Voc- ^Z'fCi
i3-S(OfUU 20 Z
<Srds-4. ffl-i/2o/9f i/ e^oA^-zoy //D^
ad,Crr A^,P6 ,&^'
a^ - 7^7P Gcft>
CHAIN OF CUSTODY
RRriNQUISHEDBY
sJi/JA^Sd.
1
DATE
^/z^/?d
/ / /
TIME
m^
1
RECEIVED BY
^A-^—
DATE
^l^/f^
TIME
/9:it
FOR LABORATORY USE ONLY
1 DAIS O0Mn.EnD DAIS SEFUlriUt SGIMTUIB
ENVIRONMENTAL LAB WORK REQUEST ^fOlf^>%
F ^ 2^
THIOKOL ENVIRONMENTAL LABORATORY B/043^ -CONT-
/I, /r WAL/ce2-:5^9o
COSTCBniR
\A4A>o
WORKOBSai
/E9^
DAIS
'ZZ>JoA/9f
oacANizAnoN
i^N\/iZD eNC>lL-2o/i^
aVOBT KBULTS T0>
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION HME TEST REMARKS
I. ^tO^lKO tol
T)oT> (5gt>5?,/, ''Hl4 </ t^af /U'ZOZ //^r Voc - ^Z4o
A^ eof M-z/>^ //p^' C4,Cr,A^,n, B^'^fC
3" ysUJMV to3 ^^AAf-2^3
*. :Su>Mi/ 3P 3
2tNiCStNK. /k
Grd Ao, Su-rLu.
fg^ 2f i/' ^^y /ji-2^z //^ -^^, <:>, -4-, Ps, 84i'^/o
A/^- •?4.'70
^/M>f ./ ^0fAA'7j>3 l/fO
(t/t&ft^ c^' i^^?^ /Ji'ZP3 /(fA> ^<l, ^r; A/^A '74?o
^n 40, /.s-ft Oftf/<f4 •' eofAA-Zo3 fi^^ lAoc. - SZ4<^
'2E.n40 /.<rfr (>/u/f4 t/" e'oAAi-io'i //zr
CHAIN OF CUSTODY
RQJNQTJISHQ) BY DATE TIME RECQVESBY DATE TIME
^ih/L 2L^ '^/^/y i^ '^^^Ck^^.^.^J— M-^f99 /'/'I'T
m
FOR LABORATORY USE ONLY
,„„_ SICNATUaS 1
July 28, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmental Momtoring
TO: Helen Ward
M/S 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order jy 9406024 Sample and Test Code IdentiTication
LabID:
OIA
Sample ID:
EAST-M203, ORD 7 SURFACE
Test Codes antl Nampji
LabID: 02A Sample ID:
EAST-M203, GRD 7, 2 FT.
LabID:
03A
Sample ID:
EAST-M203, GRD 32 SURFACE
LabID:
04A
Sample ID:
EAST-M203, GRD 32, 1 FT.
LabID:
~S5A
Sample ID:
EAST-M203, ORD 54 SURFACE
LabID:
~55A
Sample ID:
EAST-M203, ORD 54, 1 FT.
LabID:
07A
Sample ID:
EAST-M203,GRD 54,1 FT. DUP
BE AE2
CD AE2
CR AE2
PB AE2
AG AE2
HG CV2
824S
Beryllium
Cadmium
Chromium
Lead
Silver
Mercury
Voiatiie Organics
Test Codes and Names
BE AE2
CD AEZ
CR AEZ
PB AE2
AG AE2
HO CV2
8240
Beiyllium
Cadmium
Chromium
Lead
Silver
Mercuiy
Volatile Oiganici
Test Codes and Names
BE AE2
CD AE2
CR AE2
PB AE2
AG AE2
HO CV2
824S
Beiyllium
Cadmium
Chromium
Lead
SUver
Mercuiy
VoUtile Organics
Test Codes and Names
BE AE2
CD AE2
CR AE2
PB AEZ
AO AE2
HO CV2
8240
Beiyllium
Cadmium
Chromium
Lead
Silver
Mercuiy
VoUtile Organics
Test Codes and Names
BE AE2
CD AE2
CR AE2
PB AE2
AO AE2
HG CV2
8240
Beiyllium
Cadmium
Chromium
Lead
Silver
Mercuiy
VoUtile Organics
Test Codes and Names
BE AE2
CD AE2 CR AE2
PB AE2
AO AEZ
HO CV2
8240
Beryllium
Cadmium Chromium
Lead
Silver
Mercuiy
VoUtile Organics
Test Codes and Names
BE AE2
CD AEZ
CR AEZ
Beiyllium
Cadmium
Chromium
Method
S'W-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8Z40
Method
sw-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8Z40
Method
sw-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
Page 1 of 16
Work Orderly 9406024 Sample and Test Code Identification
LabID: Sample ID:
I7A EAST-M203,aRD 54,1 FT. DUP
#
LabID: Sample ID:
08A EAST-M203,aRD 54,1 FT,R-BLK
Test Codes and Names
PB_AE2 Lead
AG AE2 Silver
HG~CV2 Mercuiy
8240 VoUtile Organics
Test Codes and Names
UbID:
09A
Sample ID:
EAST-M203, ORD 40 SURFACE
LabID:
IOA
Sample ID:
EAST-M203, ORD 40, 1.5 FT.
BE AEZ
CD AEZ
CR AEZ
PB AEZ
AO AEZ
HG CV3
8240
Beryllium
Cadmium
Chromium
Lead
Silver
Mercuty
VoUtile Oi;gaiiics
Test Codes and Names
BE AE2
CD AEZ
CR AEZ
PB AEZ
AG AEZ
HG CV2
8240
Beryllium
Cadmium
Chromium
Lead
Silver
Mercury
VoUtile Organics
Test Codes and Names
BE AE2
CD AE2
CR AEZ
PB AEZ
AO AEZ
HO CV2
8Z40
Beryllium
Cadmium
Chromium
Lead
Silver
Mercuiy
VoUtiie Organics
Workorder Comment
Method
sw-846,6010
sw-846, 6010
SW-846, 7471
SW-846, 8240
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7470
SW-846, 8240 Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
sw-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
#
Certm^
•
Page 2 of 16
This is to cenify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: EAST-M203, GRD 7 SURFACE
TEST
Beryllium
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
ChlorometheUie
Dibrcsmochlorome thane
1,1-Dichloroethane
1,2-Dichloroetheme
1,l-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropame
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3 -Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4 -Methyl - 2 - Pentemone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
1.08
1.01
25.8
53.6
U
U
77
U
D
U
U
D
U
O
O
U
U
U
D
U
D
D
U
D
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
3 B
U
D
U
U
U
U
LabID
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Page
• 9406024-01A CoUected: 06/20/94 10:10:00 '^
DETECTION
LIMIT
0.1
0.1
0.3
1.5
0.2
0.024
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
3 Of 16
ANALYZED
07/06/94
07/06/94
07/06/94
07/06/94
07/06/94
07/20/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
BY
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JHA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01
10061-02
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-68-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
6010
6010
6010
6010
6010
7471
8240
m
^
-5
-6
•
July 28, 1994 11:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Pagei
Jl le ID: EAST-M203, GRD 7 SURFACE Lab ID: 9406024-OlA Collected: 06/20/94 10:10:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics SW-84e, 8240
Surrogate/Recovery Data For Volatila Organics 8240
Surrogate %Recovery
Toluene-d8 94.9
Bromofluorobenzene 88.7
l,2-Dichloroethane-d4 91.8
Recovery Limits
88 TO 110
86 TO 115
76 TO 114
Sample ID: EAST-M203, GRD 7, 2 FT. Lab ID: 9406024-02A Collected: 06/20/94 10:20:00
TEST
Beryllium
Cadmivim
Chromium ~
m
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroethane
1,l-Dichloroethene
2-Hexanone
trems-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
|iacs-1,3 -Dichloropropene
1 ^pDi chlorobenzene
RESULT
0.969
0.118
27.5
18.1
D
D
U
D
U
U
U
U
U
U
U
U
D
U
U
U
D
U
U
U
D
U
U
D
U
U
U
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.1
0.3
1.5
0.2
0.025
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Page 4 of 16
ANALYZED
07/06/94
07/06/94
07/06/94
07/06/94
07/06/94
07/20/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
BY
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA.
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JtSA
METHOD/CAS#
SW-846,
SW-846,
SW-846,
SW-846,
SW-S46,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01
10061-02
95-50-1
6010
6010
6010
6010
6010
7471
8240
-5
-6
July 28, 1994 11:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page j
Sample ID: EAST-M203, GRD 7, 2 FT. LabID: 9406024-02A Collected: 06/20/94 10:20:00
TEST
Volatile Organics
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Me thyl-2 -Pentanone
Styrene
RESULT
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
•. ,1,2 -Trichloroethane
richloroethene
rrichlorofluoromethane
Vinyl Acetate
•/inyl Chloride
o-Xylene
D
D
a D
U
U
U
U
U
2 B
U
U
D
U
O
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
%Recovery
99.0
96.9
91.3
METHOD/CAS#
SW-846, 8240
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
88
86
76
TO 110
TO 115
TO 114 1 i
Sample ID: EAST-M203, GRD 32 SURFACE Lab ID: 9406024-03A CoUected: 06/20/94 10:30:00
TEST RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Beryllium
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorometheme
Bromoform
Bromometheme
2-Butemone
0.917
1.70
30.9
17.8
U
U
29
U
U a u
u
u
u
ug/g
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Page
0.1
0.1
0.3
1.6
0.2
0.029
10
10
10
10
10
10
10
10
5 of 16
07/06/94
07/06/94
07/06/94
07/06/94
07/06/94
07/20/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
6010
6010
6010
6010
6010
74 71
8240
July 28, 1994 11:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page
M-le ID: EAST-M203, GRD 32 SURFACE Lab ID: 9406024-03A Collected: 06/20/94 10:30:00
TEST
Volatile Organics
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroetheme
1,l-Dichloroethene
2-Hexanone
trems-1,2 -Di chloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride-
4-Methyl-2-Pentanone
Styene
•M2,2 -Tetrachloroetheme
^Prachloroe thene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluorometheme
vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
4
U
U
U
U
U
D
U
D
U
U
U
U
U
n
u D
u u u XJ
u u u u u u B
u u u u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene-d8
Bromofluorobenzene
1,2 -Dichloroetheme-d4
%Recovery
97.6
94.7
91.1
METHOD/CAS#
SW-846, 8240
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
88
86
76
TO 110
TO 115
TO 114
Sample ID: EAST-M203, GRD 32, 1 FT. Lab ID: 9406024-04A Collected: 06/20/94 10:40:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Beryllium
Cadmium
aium #..
0.798
0.127
27.0
ug/g
ug/g
ug/g
Page 6 of 16
0.1 07/06/94 LVD
0.1 07/06/94 LVD
0.3 07/06/94 LVD
SW-846, 6010
SW-846, 6010
SW-846, 6010
July 28, 1994 11:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page
Sample ID: EAST-M203, GRD 32, 1 FT. LabID: 9406024-04A CoUected: 06/20/94 10:40:00
TEST
tad
Iver
•mry
.atlle Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheme
1,1-Dichloroetheme
1,2-Dichloroethane
1,l-Dichloroethene
2-Hexemone
trems-1,2-Dichloroethene
1,2-Dichloropropeme
cis.-1,3 -Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2-Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
14.2
D
U
U
U
D
U
U
U
U
U
D
U
U
U
U
U
U
U
U
D
U
U
O
U
U
U
U
D
U
O
U
U
U
U
0
U
3 B
U
U
U
D
D
U
UNITS
ug/g
ug/g
mg/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
1.5
0.2
0.021
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
07/06/94
07/06/94
07/20/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
Surrogate/Recovery Data For Volatila Organic
Surrogate
Toluene-d8
Bromofluorobenzene
1,2 -Dichloroethane-d4
Page
%Recovary
99.1
96.2
88.9
7 of 16
BY
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA.
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
•s 8240
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3 m
107-06-2 •
75-35-4 ^
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
88
86
76
TO 110
TO 115
TO 114
^^
•
July 28, 1994 11:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page ill
m le ID: EAST-M203, GRD 54 SURFACE Lab ID: 9406024-05A CoUected: 06/20/94 10:50:00
TEST
Beryllium
Cadmium-
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorome thane
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Cujbon tetrachloride
i ^robenzene
alBiroetheme
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochl orcsme thane
1,1-Dichloroethane
1,2-Dichloroethane
1,l-Dichloroethene
2-Hexanone
trems-1,2-Dichloroethene
1,2 -Dichloropropane
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4 -Methyl - 2 - Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
Q^^lene
RESULT
1.03
0.965
20.7
50.6
U
U
86
U
U
D
D
U
U
26
U
U
U
U
U
U
D
U
U
U
U
D
U
U
U
U
D
U
U
U
U
D
U
D
a D
14 B
D
U
U
U
U
U
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.1
0.3
1.5
0.2
0.026
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Page 8 of 16
ANALYZED
07/06/94
07/06/94
07/06/94
07/06/94
07/06/94
07/20/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
OG/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
BY
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
July 28, 1994 11:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page'
S.. simple ID: EAST-M203, GRD 54 SURFACE Lab ID: 9406024-05A CoUected: 06/20/94 10:50:00
SST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Surrogate/Recovery Data For Volatile Organics 8240
SW-846, 8240
Surrogate %Recovery
Toluene-d8 91.7
Bromofluorobenzene 85.1 Q
1,2-Dichloroetheme-d4 87.5
Recovery Limits
88 TO 110
86 TO 115
76 TO 114
Sample ID: EAST-M203, GRD 54, 1 FT. LabID: 9406024-06A CoUected: 06/20/94 11:05:00
-EST
Beryllium
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorome thane
Bromoform
Bromometheme
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroethane
1,l-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
RESULT
0.901
0.343
26.3
22.8
U
D
U
U
D
U
D
U
D
D
U
O
U
D
D
D
U
D
U
U
D
U
U
U
U
U
D
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.1
0.3
1.7
0.2
0.027
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Page 9 of 16
ANALYZED
07/06/94
07/06/94
07/06/94
07/06/94
07/06/94
07/20/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
BY
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 6010
SW-a46, 6010
SW-846, 6010
SW-846, 6010 ^
SW-846, 6010 ^
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1 ^^
July 28, 1994 11:01
Ssl^le ID: EAST-M203, GRD 54, 1 FT
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page
LabID: 9406024-06A CoUected: 06/20/94 11:05:00
TEST
Volatila Organics
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2-Pentanone
Styrene
RESULT
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
5
Tri chlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
J^
Surrogate
Surrogate
Toluene-d8
D
O
U
U
D
U
D
U
D
B
U
u
u
u
D
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
06/23/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
s/Recovery Data For Volatile Organics 8240
Bromofluorobenzene
1,2 -Dichloroethane-d4
%Recovery
98.8
95.8
89.1
METHOD/CAS#
SW-846, 8240
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
88
86
76
TO 110
TO 115
TO 114
Sample ID: EAST-M203,GRD 54,1 FT. DUP Lab ID: 9406024-07A CoUected: 06/20/94 11:05:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Beryllium
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Orgsmics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorome theme
Bromoform
•
ometheme
temone
0.834
0.700
24.0
17.0
U
U
U
U
U
U
D
U
D
U
ug/g
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Page
0.1
0.1
0.3
1.5
0.2
0.027
10
10
10
10
10
10
10
10
10 of 16
07/06/94
07/06/94
07/06/94
07/06/94
07/06/94
07/20/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
6010
6010
6010
6010
6010
7471
8240
July 28, 1994 11:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page
Sample ID: EAST-M203,GRD54,1 FT. DUP LabID: 9406024-07A CoUected: 06/20/94 11:05:00
TEST RESULT
Volatile Organics
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroetheme
1,l-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2 -Di (Chloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2-Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme 2
1,1,2-Trichloroethane
Tri chloroe thene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
Surrogate
Surrogate
Toluene-d8
D
U
D
D
U
U
O
U
U
U
D
U
U
D
U
D
U
U
U
a D
u D
U
D
U
B
D
U
D
U
D
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
i/Recovery Data For Volatile Organics 8240
Bromofluorobenzene
1,2-Dichloroetheme-d4
%Recovery
97.7
92.9
91.6
METHOD/CAS#
SW-846, 8240
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5 gM
127-18-4 ^
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
88
86
76
TO 110
TO 115
TO 114
Sample ID: EAST-M203,GRD 54,1FT,R-BLK LabID: 9406024-08A CoUected: 06/20/94 11:05:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Beryllium
CatSmlum
Chromium
U ug/L
U ug/L
D ug/L
0.2 07/06/94 LVD
0.2 07/06/94 LVD
0.5 07/06/94 LVD
SW-846, 6010
SW-846, 6010
SW-846, 6010
Page 11 of 16
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
PageJ July 28, 1994 11:01
s!^)leID:EAST-M203,GRD54,lFT,R-BLK LabID: 9406024-08A CoUected: 06/20/94 11:05:00
TEST
Lead
Silver
Hercniry
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2 -Chloroethy1viny1 ether
Chloroform
Chlorometheme
Dibromochloromethane
J}^-Di chl oroe thane
yMp- D i chl oroe thane
i^-Dichloroe thene
2-Hexanone
trems-1,2-Dichloroethene
1,2-Dichloropropeme
cis -1,3 -Dichloropropene
trans-l,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,l-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Tri chlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
u
n
0.37
98
D
D
D
U
D
U
40
U
D
U
U
U
U
U
U
U
U
D
7 J
D
U
U
D
D
D
U
U
U
O
U
D
U
U
44 B
D
U
D
U
D
D
UNITS
ug/L
ug/L
ug/L
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
2.5
0.3
0.15
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
07/06/94
07/06/94
07/20/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
BY
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene-d8
^1^ Bromofluorobenzene w -Dichloroethane-d4
Page
%Recovery
99.9
101
88.4
12 of 16
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 7470
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limita
88
86
76
TO 110
TO 115
TO 114
July 28, 1994 11:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Pagel
Sample ID: EAST-M203, GRD 40 SURFACE LabID: 9406024-09A CoUected: 06/20/94 11:10:00
TEST
Beryllium
Cadmium
Chromium
Lead
Silver
Merctjry
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromoform
Bromome thane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2 -Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochlorometiheme
1,1-Dichloroethane
1,2-Dichloroethane
1,l-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetihane
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
0.932
0.493
24.3
30.0
D
0.045
52
U
U
U
D
U
a u
u D
U
U
D
U
U
D
U
U
O
U
D
a
u u D
u u u
u D
D
D
U
D
7 B
U
U
D
U
D
D
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Page
DETECTION
LIMIT
0.1
0.1
0.3
1.5
0.2
0.023
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
13 of 16
ANALYZED
07/06/94
07/06/94
07/06/94
07/06/94
07/06/94
07/20/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
BY
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7 ^
75-00-3 ^
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6 ^^
July 28, 1994 11:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page J
s9i le ID: EAST-M203, GRD 40 SURFACE Lab ID: 9406024-09A CoUected: 06/20/94 11:10:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics SW-846, 8240
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate %Recovery
Toluene-d8 98.8
Bromofluorobenzene 95.1
1,2-Dichloroetheme-d4 91.4
Recovery Limits
88 TO 110
86 TO 115
76 TO 114
Sample ID: EAST-M203, GRD 40, 1.5 FT. LabID: 9406024-lOA CoUected: 06/20/94 11:25:00
TEST
Beryllium
Cadmium
Chromi um
m
Silver
Merciiry
Volatila Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2 -Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroethane
1,1-Dicdiloroe thene
2-Hexemone
trans-1,2-Dichloroethene
1,2 -Dichloroprcjpeme
cis-1,3-Dichloropropene
JjBtfiB -1,3 -Dichloropropene
1 ^B-Dichlorobenzene
RESULT
0.894
0.188
24.8
15.9
n
O
11
U
D
U
D
U
U
D
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
D
U
tINITS
ug/g
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Page
DETECTION
LIMIT
0.1
0.1
0.3
1.5
0.2
0.026
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
14 of 16
ANALYZED
07/06/94
07/06/94
07/06/94
07/06/94
07/06/94
07/20/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
BY
LVD
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
July 28, 1994 11:01 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page(
Sample ID: EAST-M203, GRD 40, 1.5 FT. LabID: 9406024-lOA CoUected: 06/20/94 11:25:00
TEST
Volatile Organics
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
RESULT
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
U
U
U
U
U
D
U
D
U
5 B
D
D
U
D
U
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
%Recovery
98.2
95.9
88.7
METHOD/CAS#
SW-846, 8240
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
88
86
76
TO 110
TO 115
TO 114 ^^
Page 15 of 16
•
m
m
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates conipound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the speciHed
detection limit but greater than zero. (e.g. 1.IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
Page 16 of 16
ENVIRONMENTAL LAB WORK REQUEST
fj/A^_^2-C>
™' TfflOKOL ENVIRONMENTAL LABORATORY
HlOMi
ORGAMZAHON
i^A/ty/fu e/^(in-
EXTOBION
SSfo
MAIL STOP
:so/^
LWR No. E10438
oosTcsrmB WORKORDBS
/B9A^
MTC 1
Z(Jo/vA^7<\
R8FORT BBSULTB TOi 11
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS
1. StjJ4H.O 4Z.C
l^?.- of Vii'2
^/I-I/H i^ iU'ii4 34^^ Cd ,Cr, A^i H- (^o/O
£:^ 'tjhl ^' AA'/l4 3£ro C<i^ Cr, A^ , 7b - <^a/o
^' 3 5i^^w lij.
^urfv-i £^ ^^ 1^ A(-zz7 /02^
^*- SafAiO I9Z.
^/uM t/ A'2Z7 /04^' Cd, Cr, Ph '
Cd. cK fb -
kk -
CfOJO
*• SttMtu 19 Z
'A^ L^' /k'^^^ /ti^-^s--i. 0?o/O
A^.o itz. Ww't-^ AA'ZZ7 flip Cd, r, Pb-
jd:.-=--A^
^z%ii <^' AA-lil //ZS'
f VoC^
Cd,Cr,^^,ffs,B^,
i>4r^ / v^Ws Wo9 M-t^^ //3£> Z4e>)
^1 , th'7^70
pH -'9e>4 r HHX
/ 5
Pui-TIL OA, ^ 2dm u^ Uy'^f A^'ZZZ fisc-// , -Sufi
V
-V
10. fu- TIL
^L^ ''ll. "Per TJL ^ l^' luof AL-ZZI //^ //
^'Attft^ t^" u/ofAt-zzn //^3 //
RFIINQVISBESBY
•'-- -^ ^••.' ^T ./.••,
DATE
..• /' z 1 ~ —•'
CHAIN OF CUSTODY
TIME
•'£7--.: 21
f^^-r
SFrEIVED BY
A^^,W tn .j<~-. J
jf - 13 V.
DATE
frX\ -rv
*^
TIME
1'^>11.
FOR LABORATORY USE ONLY
DATC OOMFUTCD DATCBSPOimD nCNATUSE 1
August 9, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
•
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER. M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order ;{f 9406026
LabID: Sample ID:
OlA M-114; PT OF DIS SURFACE
LabID: Sample ID:
~52A M-114: PT OF DIS 2 FT.
UbID:
03 A
m b ID:
04A
UbID:
OSA
UbID:
06A
UbID:
07A
UbID:
08A
Sample ID:
M-227; SURFACE
Sample ID:
M-227; 2 FT.
Sample ID:
M-227; 2 FT. DUP.
Sample ID:
M-227; 5 FT.
Sample ID:
M-227; 5 FT. RINSE BLANK
Sample ID:
W. M-227; BKGRND SURFACE
Sample and Test Code Identification
Test Codes and Names
CD_AE2 Cadmium
CR_AE2 Chromium
PB AE2 Lead
AG^AE2 Silver
Test Codes and Names
CD_AE2 Cadmium
CR AE2 Chromium
PB~AE2 Lead
AG2_AE2 Silver
Test Codes and Names
CD_AE2 Cadmium
CR_AE2 Chromium
PB_AE2 Lead
PH_S pH (Soil)
Test Codes and Names
CD_AE2 Cadmium
CR_AE2 Chromium
PB AE2 Lead
PH~S pH (Soil)
Test Codes and Names
CD_AE2 Cadmium
CR_AE2 Chromium
PB AE2 Lead
PH~S pH (Soil)
Test Codes and Names
CD_AE2 Cadmium
CR_AE2 Chromium
PB_AE2 Lead
PH S pH (Soil)
Test Codes and Names
#
CD AE2
CR AE2
PB AE2
PH S
Cadmium
Chromium
Lead
pH (Soil)
Test Codes and Names
S04IC1
HMX
NG
SB AE2
BE AE2
CD AE2
CR AE2
CU AE2
PB AE2
AG AE2
AS GF2
HG CV2
SE GF2
8240
CN_\VT2
Sulfate
HMX
Nitroglycerine
Antimony
Beryllium
Cadmium
Chromium
Copper
Lead
Silver
Arsenic
Mercury
Selenium
Volatile Organics
Total Cyanide
Page 1 of 13
Method
SW-846, 6010
sw-846, 6010
SW-846, 6010
sw-846, 6010
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,9045A Method
sw-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,9045A Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,9045A
Method
sw-846, 6010
sw-846, 6010
SW-846, 6010
SW-846,9045A
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,9045A Method
EPA 300.0
SOP 420
SOP 420
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
SW-846, 9010
Work Orderly 9406026 Sample and Test Code Identification
UbID:
08A
UbID:
09A
Sample ID:
W. M-227; BKGRND SURFACE
Sample ID:
W. M-227; BKGRND 2 FT.
Test Codes and Names
PH_S pH (Soil)
Test Codes and Names
Ub ID:
IOA
UbID:
IIA
Sample ID:
W. M-227; BKGRND 2 FT. DUP
Sample ID:
W. M-227; BKGRND 5 FT.
S04ICI
HMX
NG
SB AE2
BE AE2
CD AE2
CR~AE2
CU AE2
PB"AE2
AG AE2
AS"GF2
HG CV2
SE GF2 824b
CN WT2
PH_S
Sulfate
HMX
Nitroglycerine
Antimony
Beryllium
Cadmium
Chromium
Copper
Lead
Silver
Arsenic
Mercury
Selenium Volatile Organics
Total Cyanide
pH (Soil)
Test Codes and Names
S04ICI
HMX
NG
SB AE2
BE AE2
Cb"AE2
CR AE2
CU~AE2
PB AE2
AG AE2
AS GF2
HG"CV2
SE'GF2 8240
CN WT2
PH_S
Sulfate
HMX
Nitroglycerine
Antimony
Beryllium
Cadmium
Chromium
Copper
Lead
Silver
Arsenic
Mercuty
Selenium Volatile Organics
Total Cyanide
pH (Soil)
Test Codes and Names
S04IC1
HMX
NG
SB AE2
BE AE2
CD AE2
CR~AE2
CU AE2
PB AE2
AG AE2
AS GF2
HG CV2
SE GF2
8240
CN WT2
PH S
Sulfate
HMX
Nitroglycerine
Antimony
Beryllium
Cadmium
Chromium
Copper
Lead
Silver
Arsenic
Mercury
Selenium
Volatile Organics
Toul Cyanide
pH (Soil)
Method
SW-846,9045A
Method
EPA 300.0
SOP 420
SOP 420
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
SW-846, 9010
SW-846,9045A Method
EPA 300.0
SOP 420
SOP 420
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
SW-846, 9010
SW-846,9045A
Method
EPA 300.0
SOP 420
SOP 420
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
SW-846, 9010
SW-846,9045A
Page 2 of 13
•
Workorder Cnfnini>nt!B
Report: The cyanide samples were tested per SW-846 Method 9010.
Samples could not be tested by automated method due to gas
formation which interfered with the detector.
Certified gy^
#
m
Page 3 of 13
This is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: M-l 14; PT OF DIS SURFACE Lab ID: 9406026-OlA CoUected: 06/21/94 08:45:00
TEST RESULT DNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Cadmium
Chromliim
Lead
Silver
46.1
25.5
35.2
196
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.5
0.2
07/22/94
07/22/94
07/22/94
07/22/94
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
Sample ED: M-l 14; PT OF DIS 2 FT. Lab ID: 9406026-02A CoUected: 06/21/94 08:50:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METEOD/CAS#
Cadmium
Chromium
Lead
Silver
56.7
23.1
17.8
514
ug/g
ug/g
ug/g
ug/g
0.1
0.3
1.6
0.2
07/22/94
07/22/94
07/22/94
08/02/94
LVD
liVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
Sample ID: M-227; SURFACE Labro: 9406026-03A CoUected: 06/21/94 10:35:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIHIT
METHOD/CAS#
Cadmium
Chromium
Lead
pH (Soil)
7.50
89.8
104
7.58
ug/g
ug/g
ug/g
pH Unit
0.1
0.3
1.5
07/22/94
07/22/94
07/22/94
06/23/94
LVD
LVD
'LVD
AA
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,9045A
Sample ID: M-227; 2 FT. Lab ID: 9406026-04A CoUected: 06/21/94 10:45:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Cadmium
Chromium
1.99 ug/g
22.9 ug/g
0.1 07/22/94 LVD
0.3 07/22/94 LVD
SW-846, 6010
SW-846, 6010
Page 4 of 13
August 9, 1994 10:20
li pie ID: M-227; 2 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9406026-04A CoUected: 06/21/94 10:45:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Lead
PH (Soil)
21.1 ug/g 1.6 07/22/94 LVD SW-846, 6010
7.89 pH Unit 06/23/94 AA SW-846,9045A
Sample ID: M-227; 2 FT. DUP. Lab ID: 9406026-05A CoUected: 06/21/94 10:55:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Cadmium
Chromium
Lead
pH (Soil)
u
26.2
24.7
7.94
ug/g
ug/g
ug/g
pH Unit
0.1
0.3
1.6
07/22/94
07/22/94
07/22/94
06/23/94
LVD
LVD
LVD
AA
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,9045A
Hpiple ID: M-227; 5 FT. LabID: 9406026-06A CoUected: 06/21/94 11:10:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Cadmium
Chromium
Lead
pH (Soil)
1.09
32.5
25.3
7.90
ug/g
ug/g
ug/g
pH Unit
0.1
0.3
1.5
07/22/94
07/22/94
07/22/94
06/23/94
LVD
LVD
LVD
AA
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,9045A
Sample ID: M-227; 5 FT. RINSE BLANK LabID: 9406026-07A CoUected: 06/21/94 11:25:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Cadmium
Chromiiim
Lead
#
(Soil)
25.8
U
U
8.01
ug/L
ug/L
ug/L
pH Unit
Page 5 of 13
2
5
25
07/22/94
07/22/94
07/22/94
06/22/94
LVD
LVD
LVD
AA
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846,9045A
August 9, 1994 10:20 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: W. M-227; BKGRND SURFACE Lab ID: 9406026-08A CoUected: 06/21/94 11:30:00
TEST
Sulfate
HMX
Nitroglycerine
Antimony
Beryllium
Cadmium
Chromium
Copper
Lead
Silver
Arsenic
Mercury
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromofonn
Bromometheme
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2 -Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Di chloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
RESULT
20
U
U
4.10
0.289
U
18.4
3.53
19.3
1.74
7.251
U
U
18
U
U
U
u u u
u u
u u u u
u u
u u u u
u u u
u u u u u
UNITS
ug/g
mg/Kg
mg/Kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
3
0.12
.02
3.3
0.1
0.1
0.3
0.1
1.6
0.2
0.01
0.022
0.090
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Page 6 of 13
ANALYZED
06/28/94
06/27/94
06/26/94
07/22/94
07/22/94
07/22/94
07/22/94
07/22/94
07/22/94
08/02/94
07/29/94
07/20/94
08/01/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
BY
CRS
CFP
CFP
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
'JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
EPA 300.0
SOP 420
SOP 420
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471 ^fe
SW-846, 7740
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1 ^^
106-46-7 ^B
August 9, 1994 10:20 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
A pie ID: W. M-227; BKGRND SURFACE LabID: 9406026-08A CoUected: 06/21/94 11:30:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METEOD/CAS#
Volatile Organics
Ethylbenzene
Methylene Chloride
4 -Methyl-2 -Pentanone
Styrene
U
U
a u 1,1,2,2-Tetrachloroethane U
Te trachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
u u 3 B
u u Trichlorofluoromethane U
Vinyl Acetate
Vinyl Chloride
o-Xylene
Ij^l Cyanide
pH (Soil)
a u D
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
0.19
7.79
mg/Kg
pH Unit
For
10
10
10
10
10
10
10
10
10
10
10
10
10
10
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Volatile Organics 8240
%Recovery
93
88
89
0.:
.6
1.6
M
150
SW-846, 8240
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
88
86
76
07/05/94
07/06/94
TO 110
TO 115
TO 114
KEN
MTB
SW-846, 9010
SW-846,9045A
Sample ID: W. M-227; BKGRND 2 FT. LabID: 9406026-09A CoUected: 06/21/94 11:35:00
TEST RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Sulfate
HMX
Mi troglycerine
Antimony
Beryllium
Cadmium
Chromium
Copper
id
20
U
D
5.37
0.286
1.39
15.4
1.38
11.4
ug/g
mg/Kg
mg/Kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
3
0.12
.02
3.0
0.1
0.1
0.3
0.1
1.5
Page 7 of 13
06/28/94
06/27/94
06/26/94
07/22/94
07/22/94
07/22/94
07/22/94
07/22/94
07/22/94
CRS
,CFP
CFP
LVD
LVD
LVD
LVD
LVD
LVD
EPA 300.0
SOP 420
SOP 420
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
August 9, 1994 10:20 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: W. M-227; BKGRND 2 FT. LabID: 9406026-09A CoUected: 06/21/94 11:35:00
TEST
Silver
Arsenic
Mercury
Selenitim
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tet:rachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroe thane
1,l-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Te trachloroe thene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Tri chloroethene
Tri chlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
0.950
7.833
0.024
U
U
U
U
U
U
U
U
U
U
n u U
U
u u u u u u u u u
u u u
u u
u
u u
u
u u u 4 B
u
u
u
u u u
Surrogate/Re
Suzrogate
Toluene -d8
UNITS
ug/g
ug/g
mg/Kg
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.2
0.01
0.024
0.092
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
08/02/94
07/29/94
07/20/94
08/01/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
BY
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA.
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
'JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
covery Data For Volatile Organics 8240
%Recovery
98.7
Page Sof 13
METEOD/CAS#
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3 ^
124-48-1 i
75-34-3 "
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits ^^
88 TO 110 1
^. m w
>
August 9, 1994 10:20 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
S<H^)i le ID: W. M-227; BKGRND 2 FT. LabID: 9406026-09A CoUected: 06/21/94 11:35:00
TEST
Volatile Organics
Total Cyanide
pH (Soil)
RESULT UNITS
Bromofluorobenzene
1,2-Dichloroethane-d4
U mg/Kg
8.04 pH Unit
DETECTION
LIMIT
95.9
88.2
0.150
ANALYZED
86
76
07/05/94
07/06/94
BY METHOD/CAS#
SW-846, 8240
TO 115
TO 114
KEN SW-846, 9010
MTB SW-846,9045A
Sample ID: W. M-227; BKGRND 2 FT. DUP Lab ID: 9406026-lOA CoUected: 06/21/94 11:38:00
TEST RESXTLT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Sulfate
HMX
Nltroglycerine
Jjl^mony
Beryllliim
Cadmium
Chromium
Copper
iiead
Silver
Arsenic
MercTiry
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromometheme
^Butanone
ilBbon disulfide
^l^^on tetrachloride
21
U
U
U
U
0.293
14.7
1.11
10.2
3.53
7.875
U
U
13
U
U
U
U
U
U
U
U
U
ug/g
mg/Kg
mg/Kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Page
3
0.12
.02
2.9
0.1
0.1
0.3
0.1
1.4
0.2
0.01
0.025
0.096
10
10
10
10
10
10
10
10
10
10
9 of 13
06/28/94
06/27/94
06/26/94
07/22/94
07/22/94
07/22/94
07/22/94
07/22/94
07/22/94
07/22/94
07/29/94
07/20/94
08/01/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
CRS
CFP
CFP
LVD
LVD
LVD
LVD
LVD
LVD
LVD
JCRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
EPA 300.0
SOP 420
SOP 420
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
6010
6010
6010
6010
6010
6010
6010
7060
7471
7740
8240
August 9, 1994 10:20 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: W. M-227; BKGRND 2 FT. DUP Lab ID: 9406026-lOA CoUected: 06/21/94 11:38:00
TEST
Volatile Organics
Chlorobenzene
Chloroethane
2 -Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheme
1,1 -Dichloroetheme
1,2-Dichloroethane
1,l-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4 -DicSilorobenzene
Ethylbenzene
Methylene Chloride
4-Me thyl-2-Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroetheme
1,1,2-Trichloroethane
Triciiloroe thene
Tri chlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
2
U
U
u u u u u u u u u u
u u u u u
u
u u u u u
u B
u u u u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene-d8
Bromofluorobenzene
1,2
Total Cyanide
pH (Soil)
- Dichloroetheme-d4
8.
u
08
mg/Kg
pH Unit
%Recovery
99.0
97.4
85.5
0.150
METHOD/rAR#
SW-846, 8240
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3 J^
71-55-6 ^1
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
88
86
76
07/05/94
07/06/94
TO 110
TO 115
TO 114
KEN
MTB
SW-846, 9010
SW-846,9045A
Sample ID: W. M-227; BKGRND 5 FT. LabID: 9406026-11A CoUected: 06/21/94 11:43:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Sulfate
HMX
21
U
ug/g 3
mg/Kg 0.12
Page 10 of 13
06/28/94
06/27/94
CRS
CFP
EPA 300.0
SOP 420
August 9, 1994 10:20
^Bple ID: W. M-227; BKGRND 5 FT
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
LabID: 9406026-llA CoUected: 06/21/94 11:43:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Nitroglycerine
Antimony
Beryllium
CacSmium
Chromium
Copper
Lead
Silver
Arsenic
Mercury
Selenium
• Atile Organics
JIIBcone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorometheme
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroetheme
1,l-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4jJtethyl - 2 - Pentanone
^l^ne
u
u
0.126
U
12.2
U
9.59
0.379
7.897
U
U
8 J
U
U
U
U
U
U
U
U
U
a u D u u u
u u
u u u u u u
u u
u u u u u
mg/Kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.02
3.2
0.1
0.1
0.3
0.1
1.6
0.2
0.01
0.027
0.098
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Page 11 of 13
06/26/94
07/22/94
07/22/94
07/22/94
07/22/94
07/22/94
07/22/94
08/02/94
07/29/94
07/20/94
08/01/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
CFP
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
<JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SOP 420
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
August 9, 1994 10:20 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
;]ample ID: W. M-227; BKGRND 5 FT. LabID: 9406026-11A CoUected: 06/21/94 11:43:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
1,1,2,2-Tetrachloroethane U
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
U
u 4 B
U
U
Trichlorofluoromethane U
Vinyl Acetate
Vinyl Chloride
o-Xylene
Total Cyanide
pH (Soil)
U
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
u
8.15
mg/Kg
pH Unit
10
10
10
10
10
10
10
10
10
10
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
06/24/94
For Volatile Organic
%Recovery
100
99.5
87.6
0.150
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
s 8240
SW-846, 8240
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
88
86
76
07/05/94
07/06/94
TO 110
TO 115
TO 114
KEN
MTB
SW-846, 9010
SW-846,9045A
Page 12 of 13
•
#
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1. IJ with a detection limit of S.O)
B This fiag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
Page 13 of 13
ENVIRONMENTAL LAB WORK REQUEST /^//^/ 7 k TOI THIOKOL ENVIRONMENTAL LABORATORY LWR No. E10439
Ar. LU/UZE^ ^3fO
OOSTUINlUt
IA4^>G
WOSKOUKR
/•594O I^JoA/^ 9AI
ORCANUAHON MAO. STOP
mo 1(^0 si^&Z-, 301 e'
REPO«T MSULTa TOl
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMnE DATE TYPE U>CATION TIME TCST KEMARKS
^y?^ M'9Ui A>m. <w, ^^ figl ^^_ ^(ooio
7^70
?r^V)\ *^!tA 0^^f4 1/ /^-? k\fi C^Zl \/0C - 'SZ4C
/f/vih< • ' //t"^ /|g ^?f:?-^ —^ /ij-^^ I4^1i^
^^ Azlm ^^ 1/^ - ^^4Q
/ y^ M f ''M iSlPMO bS-t
i^ /^'t<r AP'ill ^^/^'.^^^:^.^i?< l41Ci
i^ ^' f m^ 09Z1 Voc - ez4o
^•5u>M0 b^l
Zs^7>n^&i,n-Zt. (>f^^b^ 1/ /i(-^/Ufc /^^-i^e
^k-ihd //-1 Mf oi4e \7ncL ' f^74C
bop 2^'DNGMt f^jM i^ Jizlit£L /msi ad ,Cr A^, f^h 'bc>i<^ ^ 4^ -I47t
'o^yO^/UU bSI ^r/^^ ^-^'A^g 09^ Voc- P^7_dL6
CHAIN OF CUSTODY
RFI JNQUISHED BY
.44 l(lan.
DATE
Z5JaA/£fA
TIME
ro4d
RECEIVED BY
A//^//A y/-
DATE
-^ ->/' ^/
TIME
/AA^
FOR LABORATORY USE ONLY
DATC COMFLEIB) DATCSEPORTCD aCNATUSB
August 4, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
•
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order # 9406027
LabID: Sample ID:
OIA M-9 NE., PT OF DIS SURFACE
Lab ID: Sample ID:
02A M-9 NE., PT OF DIS 2 FT.
Sample and Test Code Identification
#
LabID: Sample ID:
03A M-9 NE., 25 FF DN GRAD SUR
LabID: Sample ID:
04A M-9 NE., 25 FT DN ORAD 2Fr
LabID: Sample ID:
05A M-9NE.,25FT DN ORD 2Fr DUP
Test Codes and Names
CD AE2
CR AE2
PB AE2
AO AE2
HG CV2
8240
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
CD AE2
CR AE2
PB AE2
AO AE2
HO CV2
8240
Cadmium
Chromium
Lead
Silver
Mercuiy
Volatile Organics
Test Codes and Names
CD AE2
CR AE2
PB AE2
AG"AE2
HG CV2
8240
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Test Codes and Names
CD AE2
CR AE2
PB AE2
AG AEZ
HG CV2
8240
Cadmium
Chromium
Lead
SUver
Mercury
Volatile Organics
Test Codes and Names
CD AE2
CR AE2
PB AEZ
AG AE2
HG CV2
8240
Cadmium
Chromium
Lead
Silver
Mercuiy
Volatile Organics
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
sw-846, 6010
sw-846, 6010
sw-846, 6010
sw-846, 6010
sw-846, 7471
sw-846, 8240
Method
SW-846, 6010
sw-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
sw-846, 8240
Method
sw-846, 6010
SW-846, 6010
sw-846, 6010
SW-846, 6010
sw-846, 7471
SW-846, 8240
•
Page 1 of 10
Workorder Comments
Certrifirf^y
Page 2 of 10
This is to cenify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ED: M-9 NE., PT OF DIS SURFACE Lab ID: 9406027-OlA CoUected: 06/23/94 09:23:00
TEST
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenz ene
4 ^proe thcine
^I^iloroethylvinyl ether
Chlorofonn
Chloromethane
Dibromochloromethane
1,l-Dichloroethane
1,2-Di chloroethane
1,l-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-l,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene ^
Ethylbenzene
Methylene Chloride
4 -Methyl - 2 - Penteinone
Styrene
1,1,2,2-Tetrachloroethane
Te t rachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
8.22
58.0
350
6.88
284.4
D
U
D
n
U
D
D
U
U
U
U
D
U
U
D
U
U
U
U
U
D
U
U
D
U
D
U
U
U
u
u
D
U
U
1.4 B
D
U
U
U
U
U
UNITS
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
1.5
0.2
n ni/-
TCLP
^^5
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
07/22/94
07/22/94
07/22/94
07/22/94
— .- - •
o<:5.^^
Avg. '?f
_V / »-*
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
BY
LVD
LVD
LVD
LVD
S
A
A
FV
\
\
\
V
ucaA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
^JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
#
Page 3 of 10
August 4, 1994 13:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-9 NE., PT OF DIS SURFACE Lab ID: 9406027-OlA CoUected: 06/23/94 09:23:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics SW-846, 8240
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate %Recovery
Toluene-d8 96.4
Bromofluorobenzene 89.5
1,2-Dichloroetheme-d4 94.5
Recovery Limits
88 TO 110
86 TO 115
76 TO 114
Sample ID: M-9 NE., PT OF DIS 2 FT. Lab ID: 9406027-02A CoUected: 06/23/94 09:34:00
TEST
Cadmium
Cluroalum
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trams-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
RESULT
0.919
19.7
21.0
n
0.293
a a u
u u
u u
u D
u u 0
u o u u
u
u
u u D
u D
u u D
u D
UNITS
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Page
DETECTION
LIMIT
0.1
0.3
1.5
0.2
0.020
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
4 of 10
ANALYZED
07/22/94
07/22/94
07/22/94
07/22/94
07/20/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
BY
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
,JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010 ^^
SW-846, 7471 ^^
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5 .
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1 ^^
106-46-7 ^^
100-41-4 ^y
August 4, 1994 13:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sini pie ID: M-9 NE., PT OF DIS 2 FT. Lab ID: 9406027-02A CoUected: 06/23/94 09:34:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Tri chloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
u
u u teme U
U
U
1.6 B
U
U
U
U
U
a
Surrogate/Recc
Surrogate
Toluene-d8
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
)very Data
Bromofluorobenzene
1,2-Dichloroetheme-d4
For
10
10
10
10
10
10
10
10
10
10
10
10
10
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
Volatile Organic
%Recovery
99
98
91
.8
.3
.2
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
IS 8240
SW-846, 8240
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
88
86
76
TO 110
TO 115
TO 114
s^ni pie ID: M-9 NE., 25 FT DN GRAD SUR Lab ID: 9406027-03A CoUected: 06/23/94 09:37:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Cadmium
Chromium
Lead
Silver
Mercury
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromoform
Bromometheme
2-Butemone
Carbon disulfide
Carbon(tetrachloride
Chlorobenzene
in|l oroe theme
^|Hbhloroethylvinyl ether
2.28
27.7
56.6
U
27.15
U
U
U
U
U
U
a U
U
U
D
U
D
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0
Page 5 of 10
0.1
0.3
1.4
0.2
.023
10
10
10
10
10
10
10
10
10
10
10
10
10
07/22/94
07/22/94
07/22/94
07/22/94
07/20/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
LVD
LVD
LVD
LVD
*CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
August 4, 1994 13:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-9 NE., 25 FT DN GRAD SUR Lab ID: 9406027-03A CoUected: 06/23/94 09:37:00
TEST
Volatile Organics
Chloroform
Chlorometheme
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroetheme
1,l-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
I., 2 -Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4 -Methyl - 2 - Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Te trachloroethene
Toluene
1,1,l-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
-
RESULT
10
Surrogate
Surrogate
Toluene-d8
U
O
U
D
U
a U
U
n
u u D
u D
U
U
n D
a u u B
a u u D
u D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
/Recovery Data For Volatile Organic
Bromofluorobenzene
1,2 -Dichloroethane-d4
%Recovery
95.7
94.6
92.7
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
:s 8240
METHOD/CAS#
SW-846, 8240
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6 ^^
75-69-4 ^M
108-05-4 ^^
75-01-4
95-47-6
Recovery Limits
88
86
76
TO 110
TO 115
TO 114
Sample ID: M-9 NE., 25 FT DN GRAD 2FT Lab ED: 9406027-04A CoUected: 06/23/94 09:48:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Cadmium
Chromium
Lead
Silver
Mercury
0.452
19.4
18.2
U
0.400
ug/g
ug/g
ug/g
ug/g
mg/Kg 0
Page 6 of 10
0.1
0.3
1.5
0.2
.015
07/22/94
07/22/94
07/22/94
07/22/94
07/20/94
LVD
LVD
LVD
LVD
CRS
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
7471
August 4, 1994 13:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
siHp. le ID: M-9 NE., 25 FT DN GRAD 2FT Lab ID: 9406027-04A CoUected: 06/23/94 09:48:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromometheme
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2 -Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochlorometheme
1,l-Dichloroethane
1,2-Dichloroetheme
1,l-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
ffl^-1,3-Dichloropropene
I V^^B-1,3-Dichloropropene
llj^ Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4 -Methyl - 2 - Pentemone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
3.
1.
D
U
U
U
U
U
U
U
D
U
U
U
U
D
U
U
U
D
D
D
U
U
U
U
U
U
U
U
U
U
U
D
D
U
3 B
U
,9 J
U
D
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
OG/28/94
06/28/94
06/28/94
06/28/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
06/28/94 ^JMA
06/28/94
06/28/94
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene-d8
Bromofluorobenzene
1,2 -Dichloroethane-d4
%Recovery
98.9
99.1
91.0
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
88
86
76
TO 110
TO 115
TO 114
•
Page 7 of 10
August 4, 1994 13:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: M-9NE.,25FT DN GRD 2FT DUP Lab ID: 9406027-05A CoUected: 06/23/94 09:48:00
TEST
Cadmiiim
Chromium
Lead
Silver
Mercury
Volatila Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichlorometheme
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochlorometheme
1,1-Dichloroetheme
1,2-Dichloroethane
1,l-Dichloroethene
2-Hexanone
trems-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
RESULT
1.29
20.5
23.5
D
0.466
D
U
U
U
U
U
U
U
O
D
U
a D
U
U
U
U
U
U
U
D
D
U
U
U
U
U
D
U
U
U
D
U
U
8.7 B
D
U
U
U
U
U
UNITS
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
0.1
0.3
1.6
0.2
0.025
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
07/22/94
07/22/94
07/22/94
07/22/94
07/20/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
06/28/94
BY
LVD
LVD
LVD
LVD
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
OMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
^JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8 i
67-66-3 \
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
B P
Page 8 of 10
August 4,1994 13:02 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sanpl lie ID: M-9NE.,25FT DN GRD 2FT DUP Lab ID: 9406027-05A CoUected: 06/23/94 09:48:00
TEST RESULT UNITS DETECTION ANALYZED BY METHOD/CAS#
LIMIT
Volatile Organics SW-846, 8240
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
%Recovery
100
99.5
93.2
Recovery
88 TO
86 TO
76 TO
Limits
110
115
114
#
m
Page Sof 10
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection Ui^B
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identiiled compounds or when the mass spectral data indicated the presence of a
compound that meets the identiiication criteria but the result is less than the speciiied
detection limit but greater than zero. (e.g. 1. IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
Page 10 of 10
i
ENVIRONMENTAL LAB WORK REQUEST ^''/'O-y A'// f
#
TinOKOL ENVIRONMENTAL LABORATORY LWR No. E10601
^A/lA/dO eN& it SB^CP
COSTCENTGR
l/4do
WORK ORDBl
//S940 -7M(c ••P^ OMiANirATION
^f^l/t2^ ^htCR^
MAIL STOP
-S0/&
REPORT RESULTS TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS
\-Siirol€yC 7J-^ ir ^ \JU6f^/U-^l bSol Voc -SZiO
:Sey*t/ j/ac - 8Z70
i{ • /( ddol Mcttu^ '^atoi CM- I'o/o
7470 . DH- -9<:>4^ M -fi^
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Bck^hd 2 do-i •
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^
// •^ // ^:?644
A4.e/G/s - (oo/o Cf/~9a/o
A^ - 74-70 p//'9o4
CHAIN OF CUSTODY
REIJNQUISHED BY DATE TIME RECEIVED BY DATE TIME
•.=^/m/A^_ 74iU^^ 9<^ ^£A<y A ."S^ :2=. d^^ ^.?7,."^ 'A '77-f'A f-Yr y^^/rm^^u^rr 'A 7-^4^ ^f'^^C
•^^
FOR LABORATORY USE ONLY
i[
DAT>: n>M11J!TH)
,
DATE REPORTED SIGNA1VRE
August 9, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER. M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Orders 9407009
LabID:
OIA
Sample ID:
W. OF M-381, BKGRND SURF.
Sample and Test Code Identification
Test Codes and Names
LabID:
"MA
Sample ID:
OF M-381, BKGRND 2 FT. W
LabID:
~03A
Sample ID: -
W. OF M-381,BKGRND 2FT.DUP
LabID:
04A
Sample ID:
W. OF M-381, BKGRND 5 FT.
S04IC1
HMX
NG
SB AE2
BE"AE2
CD~AE2
CR"AE2
CU~AE2
PB"AEZ
AG~AE2
AS"GE2
HG~CV2
SE aF2 824bS
8270S
CN AU2
PH_S
Sulfate
HMX
Nitroglycerine
Antimony
Befyllium
Cadmium
Chromium
Copper
Lead
Silver
Arsenic
Mercuty
Selenium VolatUe Organics
Semi-Volatile Otganics
Total Cyanide
pH (SoU)
Test Codes and Names
S04IC1
HMX
NO
SB AE2
BE"AE2
CD AE2
CR AE2
CU"AE2
PB"AE2
AO"AE2
AS"GF2
HG CV2
SE OF2
8240S
8270S
CN AU2
PHJS
Sulfate
HMX
Nitroglycerine
Antimony
BeryUium
Cadmium
Chromium
Copper
Lead
Silver
Arsenic
Mercuty
Selenium
VolatUe Organics
Semi-VolatUe Organics
Toul Cyanide
pH (SoU)
Test Codes and Names
S04IC1
HMX
NG
SB AE2
BE"AE2
CD"AE2
CR"AE2
CU AE2
PB"AE2
Ad"AE2
AS GF2
HG CV2
SE OF2
824bS
8270S
CN AU2
PH_S
Sulfate
HMX
Nitroglycerine
Antimony
Beryllium
Cadmium
Chromium
Copper
Lead
SUver
Arsenic
Mercuiy
Selenium
VolatUe Organics
Semi-Volatile Organics
Total Cyanide
pH (SoU)
Test Codes and Names
S04IC1 Sulfate
Method
EPA 300.0
SOP 420
SOP 420
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, T740
SW-846, 8240
SW-846, 8270
SW-846, 9012
SW-846,9045A
Method
EPA 300.0
SOP 420
SOP 420
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
SW-846, 8270
SW-846, 9012
SW-846,9045A
Method
EPA 300.0
SOP 420
SOP 420
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
SW-846, 8270
SW-846, 9012
SW-846,9045A Method
EPA 300.0
Page 1 of 15
Work Orderly 9407009 Sample and Test Code Identification
•
Lab ID:
04A
Sample ID:
W. OF M-381, BKGRND 5 FT.
Test Codes and Names
HMX HMX
NO Nitroglycerine
SB AEZ Antimony
BE^AEZ Beryllium
CD_AE2 Cadmium
CR AE2 Chromium
CU~AE2 Copper
PB_AE2 Lead
AQ_AE2 Silver
AS aF2 Arsenic
Hti^CV2 Mercury
SE GF2 Selenium
8240s Volatile Organics
8270S Semi-Volatile Organics
CN AU2 Total Cyanide
PH~S pH (Soil)
Method
SOP 420
SOP 420
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
SW-846, 8270
SW-846, 9012
SW-846,9045A
Workorder Comment*;
#
Page 2 of 15
This is to cenify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: W. OF M-381, BKGRND SURF. LabID: 9407009-01A CoUected: 07/07/94 08:07:00
TEST
Sulfate
HMX
Ni troglycerine
Antimony
Beryllium
Cadmium
chromium
Copper
Lead
Silver
Arsenic
Mercury
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethcuie
Bromoform
Bromometheme
2-Butcinone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2 -Cailoroethylvinyl ether
(Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroetheme
1,l-Dichloroethene
2-Hexemone
trans-1,2-Di chloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
RESULT
3.1
U
U
u
0.838
0.949
21.9
U
32.5
0.681
9.589
0.035
0.29
23
U
U
D
U
U
D
7 J
U
U
U
D
D
U
D
U
U
D
U
U
D
U
U
U
U
U
tJNITS
ug/g
mg/Kg
mg/Kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
3
.01
.02
3.1
0.1
0.1
0.3
0.1
1.5
0.2
0.01
0.020
0.096
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Page 3 of 15
ANALYZED
08/03/94
07/20/94
07/20/94
07/22/94
07/22/94
07/22/94
07/22/94
07/22/94
07/22/94
08/02/94
07/29/94
07/20/94
08/01/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
BY
CRS
CFP
CFP
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JIIA
JMA
OMA
JMA.
JMA
JMA
JMA
JMA
JMA
-•OMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
EPA 300.0
SOP 420
SOP 420
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471 fl
SW-846, 7740
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1 ^^
541-73-1 ^^
August 9, 1994 10:46
sV^)le ID: W. OF M-381, BKGRND SURF
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9407009-OlA, CoUected: 07/07/94 08:07:00
TEST RESULT
Volatile Organics
1,4-Dichlorobenzene
Etihylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroetheme
Tetrachloroethene
Toluene
1,1,1-Trichloroethane 8
1,1,2-Trichloroetheme
Trichloroethene ,
Tri chlorof1uorome theme
Vinyl Acetate
Vinyl Chloride
o-Xylene
U
U
D
U
U
U
U
O
BJ
U
u
u u
u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
'H.-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)metheme
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroemiline
Hexachlorobutadiene
4 -Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
^^, 6-Trichlorophenol
i^^ 5-Trichlorophenol
^I^Piloronaphthalene
u
u D
D
U
U
O
U
U
u u
u
D
U
U
u
u
u
u u
o D
U
U
U
D
U
U
U
a
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
: ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
%Recovery
101
94.4
94.2
50
330
330
190
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
Page 4 of 15
METHOD/CAS#
SW-846, 8240
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
'MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
August 9, 1994 10:46 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: W. OF M-381, BKGRND SURF. Lab ID: 9407009-OlA CoUected: 07/07/94 08:07:00
TEST
Semi-Volatile Organics
2-Nitroaniline
Dime thylphthalate
Acenaphthylene
3 - Ni troemi 1 ine
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofurem
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4 -Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
n-Ni trosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
bis(2-Ethylhexyl)phthalate
Chrysene
Di-n-octylphthalate
Benzo tb&k]fluoranthene
Benzo[a]pyrene
Indeno(1,2,3-cd]pyrene
Dibenz[a,h]anthracene
Benzo[g,h,i]perylene
RESULT
378
O
D
U
D
U
U
D
D
D
U
U
U
U
U
U
D
D
U
V
U
U
U
u D
D
U
41
D
U
U
D
U
u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2-Fluorophenol
Phenol .-d5
Ni t robenzene-d5
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terpheny1-dl4
Total Cyanide
pH (Soil)
0
7.
20
74
mg/Kg
pH Unit
DETECTION
LIMIT
50
53
120
79
63
1400
79
99
63
190
63
140
63
120
790
63
63
63
120
180
63
83
73
63
83
260
83
83
83
160
83
120
83
140
ANALYZED
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0 ^^
85-68-7 ^M
56-55-3 ^^
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 8270S
%Recovery
43.65
45.04
48.83
50.17
61.34
69.39
0.15
Recovery Limits
25'^O 121
24
23
30
19
18
07/21/94
07/07/94
TO 113
TO 120
TO 115
TO 122
TO 137
AA
MTB
SW-846, 9012
SW-846,9045A
Page 5 of 15
August 9, 1994 10:46
9UQ)Ie ID: W. OF M-381, BKGRND 2 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Lab ID: 9407009-02A CoUected: 07/07/94 08:22:00
TEST RESXTLT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Sulfate
HMX
Ni troglycerine
Antimony
Beryllium
Cadmium
Chromium
Copper
Lead
Silver
Arsenic
jury
Selenium
#>
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromometheme
2-Butcmone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trems-1,3-Dichloropropene
1^ 2 -Di chlorobenzene
-Dichlorobenzene
-Dichlorobenzene
19
O
U
5.12
0.882
0.302
20.6
U
23.8
12.8
8.892
0.023
U
D
U
/U
•D
U
U
D
U
o
u n
u u D
U
u u u u
u
u D
U
U
u
u u
ug/g
mg/Kg
mg/Kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
3
.01
.02
3.0
0.1
0.1
0.3
0.1
1.5
0.2
0.01
0.021
0.099
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Page 6 of 15
08/03/94
07/20/94
07/20/94
07/22/94
07/22/94
07/22/94
07/22/94
07/22/94
07/22/94
07/22/94
07/29/94
07/20/94
08/01/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
CRS
CFP
CFP
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
-"SKA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
EPA 300.0
SOP 420
SOP 420
SW-846, 6010
SW-a46, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
August 9, 1994 10:46 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: W. OF M-381, BKGRND 2 FT. Lab ID: 9407009-02A CoUected: 07/07/94 08:22:00
TEST RESULT X7NITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentemone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
U
D
U
U
U
D
U
D
U
U
D
O
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroethane-d4
Semi-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2-Chlorophenol
1,2-Dichlorobenzene
1,4 -Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)metheme
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-cailoro-3-me thy Iphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroemiline
U
U
U
U
U
D
U
U
D
U
D
U
U
D
D
U
U
D
D
D
U
U
U
a U
U
u u D
U
U
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
10
10
10
10
10
10
10
10
10
10
10
10
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240S
%Recovery
99.6
98.3
95.7
50
330
330
190
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
Page 7 of 15
SW-846, 8240
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
"IMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
August 9, 1994 10:46 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
H, pie ID: W. OF M-381, BKGRND 2 FT. , Lab ID: 9407009-02A CoUected: 07/07/94 08:22:00
TEST
Semi-Volatile Organics
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofurem
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methyIphenol
n-Nitrosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Jtoene
1 Bylbenzylphthalate
^itmzo [a] anthracene
bi s(2 -Ethylhexyl)phthalate
Chrysene
Di-n-octylphthalate
Benzo[b&k]fluoranthene
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h]anthracene
Benzo[g,h,i]perylene
RESULT
2542
U
U
U
D
U
U
U
D
U
U
U
U
U
U
U
U
U
U
u u
u
u
n
u D
.2
D
D
D
U
D
U
D
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2-Fluorophenol
'Phenol .-d5
Nitrobenzene i-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
Total Cyanide
pH (Soil) 8.
u
25
mg/Kg
pH Unit
DETECTION
LIMIT
53
120
79
63
1400
79
99
63
190
63
140
63
120
790
63
63
63
120
180
63
83
73
63
83
260
83
83
83
160
83
120
83
140
ANALYZED
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Ox-ganlcs 827 OS
%Recovery
41.85
43.23
46.79
45.56
58.00
67.00
0.15
Recovery Limits
25
24
23
30
19
18
07/21/94
07/07/94
TO 121
"Yo 113
TO 120
TO 115
TO 122
TO 137
AA
MTB
SW-846, 9012
SW-846,9045A
Page 8 of 15
August 9, 1994 10:46 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: W. OF M-381,BKGRND 2FT.DUP Lab ID: 9407009-03A CoUected: 07/07/94 08:22:00
TEST
Sulfate
HMZ
Ni troglycerine
Antimony
Beryllium
Cadmium
Chromium
Copper
Lead
Silver
Arsenic
Mercury
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorometheme
Bromoform
Bromomethane
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroetheme
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochloromethane
1,1-Dichloroetheme
1,2-Dichloroethane
1,l-Dichloroethene
2-Hexanone
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
RESULT
12.0
U
D
U
0.841
0.472
20.8
U
30.5
0.302
9.959
U
0.27
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
u
u u u
u
u u
u
u u
u
u
UNITS
ug/g
mg/Kg
mg/Kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Page
DETECTION
LIMIT
3
.01
.02
3.1
0.1
0.1
0.3
0.1
1.6
0.2
0.01
0.019
0.093
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
9 of 15
ANALYZED
08/03/94
07/20/94
07/20/94
07/22/94
07/22/94
07/22/94
07/22/94
07/22/94
07/22/94
08/02/94
07/29/94
07/20/94
08/01/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
BY
CRS
CFP
CFP
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
-OMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JHA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
EPA 300.0
SOP 420
SOP 420
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471 ^
SW-846, 7740
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1 ^^
106-46-7 ^M
August 9, 1994 10:46 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE m le ID: W. OF M-381,BKGRND 2FT.DUP Lab ID: 9407009-03A CoUected: 07/07/94 08:22:00
TEST RESULT UNITS DETECTION ANALYZED BY
LIMIT
METHOD/CAS#
Volatile Organics
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Te trachloroethene
Toluene
1,1,l-Trichloroethane
1,1,2-Trichloroetheme
Trichloroethene
Trichlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
U
U
U
U
U
U
U
U
U
U
U
U
U
U
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
SW-846, 8240
10 07/19/94 JMA 100-41-4
10 07/19/94 JMA 75-09-2
10 07/19/94 JMA 108-10-1
10 07/19/94 JMA 100-42-5
10 07/19/94 JMA 79-34-5
10 07/19/94 JMA 127-18-4
10 07/19/94 JMA 108-88-3
10 07/19/94 JMA 71-55-6
10 07/19/94 JMA 79-00-5
10 07/19/94 JMA 79-01-6
10 07/19/94 JMA 75-69-4
10 07/19/94 JMA 108-05-4
10 07/19/94 JMA 75-01-4
10 07/19/94 JMA 95-47-6
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2 -Dichloroethane-d4
%Recovery
99.1
99.4
94.2
Recovery Limits
81 TO 117
74 TO 121
70 TO 121
gjj^-Volatile Organics
Pyridine
Aniline
bis(2-Chloroethyl)ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)metheme
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2^, 5-Trichlorophenol
i Hploronaphthalene
^j^^troemiline
U
U
U
U
U
U
U
D
U
U
D
U
U
U
U
U
U
u
u
u u
D
U
U
U
U
U
u u u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
SW-846, 8270
50 07/19/94 MMR 108-95-2
330 07/19/94 MMR 110-86-1
330 07/19/94 MMR 62-95-2
190 07/19/94 MMR 111-44-4
110 07/19/94 MMR 95-57-8
63 07/19/94 MMR 541-73-1
150 07/19/94 MMR 106-46-7
150 07/19/94 MMR 100-51-6
63 07/19/94 MMR 95-50-1
76 07/19/94 MMR 95-48-7
190 07/19/94 MMR 108-60-1
130 07/19/94 MMR 106-44-5
400 07/19/94 MMR 621-64-7
53 07/19/94 MMR 67-72-1
46 07/19/94 MMR 98-95-3
73 07/19/94 l4MR 78-59-1
120 07/19/94 MMR 88-75-5
89 07/19/94 MMR 105-67-9
110 07/19/94 MMR 65-85-0
170 07/19/94 MMR 111-91-1
89 07/19/94 MMR 120-83-2
63 07/19/94 MMR 120-82-1
53 07/19/94 MMR 91-20-3
59 07/19/94 MMR 106-47-8
30 07/19/94 MMR 87-68-3
99 07/19/94 MMR 59-50-7
73 07/19/94 MMR 91-57-6
200 07/19/94 MMR 77-47-4
89 07/19/94 MMR 88-06-2
130 07/19/94 MMR 95-95-4
63 07/19/94 MMR 91-58-7
50 07/19/94 MMR 88-74-4
Page 10 of 15
August 9, 1994 10:46 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: W. OF M-381.BKGRND 2FT.DUP Lab ID: 9407009-03A CoUected: 07/07/94 08:22:00
TEST
Semi-Volatile Organics
D ime thyIphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4 -Chlorophenyl-phenylether
Fluorene
4 -Nitroemiline
4,6-Dinitro-2-methylphenol
n-Ni trosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
Benzo[a]anthracene
bis(2-Ethylhexyl)phthalate
Chrysene
Di-n-octylphthalate
Benzo[b&k]fluoremthene
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
Dibenz[a,h] emthracene
Benzo[g,h,i]perylene
Total Cyanide
pH (Soil)
RESULT
3324
U
U
U
U
U
U
u D
U
U
U
U
U
D
U
U
U
U
D
a u
u u
u u .6
u u u u u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
2 -Fluorophenol
• Phenol -65
Nitrobenzene -d5
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-dl4
8.
u
17
mg/Kg
pH Unit
DETECTION
LIMIT
53
120
79
63
1400
79
99
63
190
63
140
63
120
790
63
63
63
120
180
63
83
73
63
83
260
83
83
83
160
83
120
83
140
ANALYZED
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7 ^^
56-55-3 M
117-81-7 ^
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-Volatile Organics 827OS
%Recovery
41.61
43.54
47.37
46.90
49.86
59.98
0.15
Recovery Limits
25 TO 121
24 -TO 113
23
30
19
18
07/21/94
07/07/94
TO 120
TO 115
TO 122
TO 137
AA
MrB
SW-846, 9012
SW-846,9045A
Page 11 of 15
August 9, 1994 10:46 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
pie ID: W. OF M-381, BKGRND 5 FT. Lab ID: 9407009-04A CoUected: 07/07/94 08:44:00
TEST
Sulfate
BMZ
Ni troglycerine
Antimony
Beryllium
Cadmium
Chromium
Copper
Lead
Silver
Arsenic
tf P=ury
Selenium
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorometheme
Bromoform
Bromomethane
2 -Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroe thene
2-Hexemone
trans-1,2-Dichloroethene
1,2-Dichloropropeme
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1^ -Dichlorobenzene
^l^-Dichlorobenzene
^j^- Di chlorobenzene
RESULT
31
D
D
U
0.775
U
18.8
D
23.9
0.451
10.06
U
D
U
U
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
UNITS
ug/g
mg/Kg
mg/Kg
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
mg/Kg
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Page
DETECTION
LIMIT
3
.01
.02
3.3
0.1
0.1
0.3
0.1
1.7
0.2
0.01,
0.022
0.10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
12 of 15
ANALYZED
08/03/94
07/20/94
07/20/94
07/22/94
07/22/94
07/22/94
07/22/94
07/22/94
07/22/94
08/02/94
07/29/94
07/20/94
08/01/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
BY
CRS
CFP
CFP
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
CRS
CRS
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
•tIMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
EPA 300.0
SOP 420
SOP 420
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7060
SW-846, 7471
SW-846, 7740
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
August 9, 1994 10:46 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Sample ID: W. OF M-381, BKGRND 5 FT. Lab ID: 9407009-04A CoUected: 07/07/94 08:44:00
TEST RESULT
Volatile Organics
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluerie
1,1,1-Trichloroetheme
1,1,2-Trichloroetheme
Trichloroethene
Tri chlorofluorometheme
Vinyl Acetate
Vinyl Chloride
o-Xylene
U
U
U
U
D
U
U
U
u u u u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
DETECTION
LIMIT
10
10
10
10
10
10
10
10
10
10
10
10
10
10
ANALYZED
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
Surrogate/Recovery Data For Volatile Organics 8240S
Surrogate
Toluene-d8
Bromofluorobenzene
1,2-Dichloroetheme-d4
Semi-Volatile Organics
Phenol
Pyridine
Aniline
bis (2-Chloroethyl)ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ethe
4 -Methylphenol
n-Nitroso-di-n-propylamine
Hexachloroetheme
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis (2-Chloroethoxy)metheme
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4 -Chloroemiline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthlene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
u
u u u u u u
u u u u
u
u
u u u
u
u u u
u u u
u u
u u u
u u
u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Page
%Recovery
99.9
97.1
93.2
50
330
330
190
110
63
150
150
63
76
190
130
400
53
46
73
120
89
110
170
89
63
53
59
30
99
73
200
89
130
63
50
13 of 15
METHOD/CAS#
SW-846, 8240
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
Recovery Limits
81
74
70
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
TO 117
TO 121
TO 121
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
"^MR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
SW-846, 8270 ^
108-95-2 fH
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7 ^^
88-74-4 ^P
August 9, 1994 10:46 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
M pie ID: W. OF M-381, BKGRND 5 FT. Lab ID: 9407009-04A CoUected: 07/07/94 08:44:00
TEST
Semi-Volatile Organics
Dimethylphthalate
Acenaphthylene
3 -Ni troani1ine
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofurem
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
1
4-Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
n-Ni trosodiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenemthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
E^ene
m ^rlbenzylphthalate
^IPIzo [a] anthracene
bis(2-Ethylhexyl)phthalate
Chrysene
Di-n-octylphthalate
Benzo[b&k]fluoremthene
Benzo[a]pyrene
Indeno[1,2,3 -cd]pyrene
Dibenz[a,hj anthracene
Benzo[g,h,i]perylene
REStTLT
320.
2904
Surrogate/Re
Surrogate
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
U
U
09
U
U
U
U
.5
U
O
U
U
U
U
u
scove
2 -Fluorophenol
Phenol .-d5
Nitrobenzene -d5
2 -Fluorobiphenyl
2,4,6-
Terphe
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ry Data
Tribromophenol
inyl-dl4
DETECTION
LIMIT
53
120
79
63
1400
79
99
63
190
63
140
63
120
790
63
63
63
120
180
63
83
73
63
83
260
83
83
83
160
83
120
83
140
ANALYZED
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
07/19/94
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
METHOD/CAS#
SW-846, 8270
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For Seml-Volatlle Organics 8270S
%Recovery
40.63
42.60
45.03
45.98
58.80
69.68
Recovery Limits
25 TO 121
24'^O 113
23
30
19
18
TO 120
TO 115
TO 122
TO 137
Total Cyanide
pH (Soil)
U mg/Kg 0.15 07/21/94 AA SW-846, 9012
8.43 pH Unit 07/07/94 MTB SW-846,9045A
t»
Page 14 of 15
Data Reportmg Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection lim
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identifted compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1. IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection Umits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spUce recovery was outside of the specified Umits.
Page 15 of 15