DSHW-1994-003766 - 0901a06880157b2e

TfflOKOL CORPORATION
SEMI-ANNUAL RFI PROGRESS REPORT
1 SEPTEMBER 1993 - 1 MARCH 1994
SEMI-ANNUAL RFI PROGRESS REPORT
1 SEPTEMBER 1993 - 1 MARCH 1994
1. Description and estimation of the percentage of the RCRA
Facility Investigation completed;
Thiokol Corporation initiated Phase I soil sampling for the
RFI on 13 October 1993. To date, soils at the following SWMUs
have been sampled:
M-19A Photographic Processing Discharge, SWMU 553,*^
E-517-W Surface Discharge, SWMU 282,*\
M-576-N Surface Discharge, SWMU 211;K
M-514 Surface Discharge, SWMU 618,-A
S-501 Surface Discharge, SWMU 266,•'X
M-64 0 Surface Discharge, SWMU 381,"^
M-641 Surface Discharge, SWMU 264;«<'
M-585-N Surface Discharge, SWMU 273pT
M-606 Surface Discharge, SWMU 527,-^T
M-628 Surface Discharge, SWMU 528;'^
M-593 Surface Discharge, SWMU 274,-«^
M-63 6-SW Surface Discharge, SWMU 367;X'
M-570 Surface Discharge, SWMU 285;i\-
M-197 Surface Discharge, SWMU AQ2 f><
M-197-BP Surface Discharge, SWMU 2S0 tE>C
M-702 Surface Discharge, SWMU 620 ;V
A-9 Surface Discharge, SWMU 267;>)<and
A-2 Surface Discharge, SWMU 560 >c
These sites represent approximately 20 percent of SWMUs in
Phase I of the RFI.
2. Siimmaries of all findings;
The raw analytical data for the reporting period is included
with this report. This data will be compared to standards
considered to be protective of health and the environment as
outlined in Section 8.0 of the Data Collection Oualitv
Assurance Plan, Volume Two, Thiokol RCRA Facility
Investigation Workplans.
3. S\umnaries of all changes made in the RCRA Facility
Investigation during the reporting period;
• The workplans for all SWMUs have been modified to include
the following statement in the Sampling Technique
section:
NOTE: Containerize all wash and rinse water for treatment
at M-705 Wastewater Treatment Facility,
This statement will be included with all workplans both
approved and those yet to be approved.
• The workplans for SWMU Nos. 652, 649 and 650 have been
amended to include the following:
The three discharge sites will be grouped together for
determination of the number of duplicate and QA/QC
samples. The following chart summarizes the recommended
frequency for these samples:
SAMPLE TYPE PROPOSED FREOTJENCY
Duplicate 5 % of the number of
samples to be taken under
this plan
Rinse Field Blanks 5 % of the number of
samples to be taken under
this plan
Spikes 1 % of the total RFI
samples
In addition to the revisions described above, the following
alternate analytical methods will be used by Thiokol's
Environmental Laboratory:
• SW-846 Method 6010 for Al, Sb, As, Ba, Be, B, Cd, Ca, Cr,
Co, Cu, Fe, Pb, Mg, Mn, Mo, Ni, K, Se, Si, Ag, Na, Tl, V,
and Zn
• SW-846 Method 7470 for Hg
• Method 300.0 for Sulfate
These methods are appropriate EPA approved methods and will
provide quality analytical data.
SWMU Numbers 198 and 586 are to be removed from the RFA SWMU
list. These units are on Morton International property and no
further action was proposed or required at these site.
These revisions were submitted to and approved by the DSHW in
previous correspondence.
4. Svmimaries of all contact with representatives of the local
community, public interest groups or State Government during
the reporting period;
Correspondence regarding RFI activities has been limited to
the Division of Solid and Hazardous Waste and the Division of
Water Quality.
5. Summaries of all problems or potential problems encountered
during the reporting period;
Thiokol has not encountered any problems related to the RFI
which would effect the quality of the investigation.
6. Actions being taken to rectify problems;
N/A
7. Changes in personnel during the reporting period;
The attached organization chart represents the current staff
of Waste Management and Environmental Services at Thiokol.
8. Projected work for the next reporting period;
Thiokol expects the investigation to resume mid-March, with
emphasis on completing the remaining units within the Surface
Discharge Soil Samplinq Plan. Sampling will then proceed to
the units within the Injection Well Samplinq Plan, and then to
the Group Two Units approved by the DSHW on 8 November 1993.
9. Copies of daily reports, inspection reports, laboratory and
monitoring data.
Copies of the daily logs and laboratory data are included with
this report.
WASTE MANAGEMENT AND ENVIRONMENTAL SERVICES
vooo
J. D. THOMPSON
DIRECTOR
BECRETARr
ICPETT
ENVRONMENTAL
ENGINEERING
D.C. Umil
»a»M:Rwson
ENQMEEIWia
W.E COHEN Fl£C)
K.aFax(NOUs:i)
A.POROT(CNEM)
A. F. WALKER (OV)
auwywoRE
OEOUXW
J. C. HOLLADAY
DESIGN
y.BMGHAM
vaoo
PERMflS
J.P.MARTM
UANAOER
UPDES aWATEH
S.E.IVU«S
RCRA
KRJAU8SI
An
S.HiaLl£R
RLSMTIH
Pdhiien
PfBvAmkn
K J. THACKERAY
ooe*
P.HHOTH
UAMTENANCE
ac. MAUGHAN
U.aNOOR
V3oa
MONrrORING
J.aWHIMPEV
SUPERVISOR
D.LCov»ianoN
J.C.CUUINS
J. A. HOLLMOBWORm
HAZCOM, SARA, arSCA
J.K.OJA
UaTANAKA
TECH EDTTOR, AUDOS.
ACCOUNTMa a BUDGET
aKNAUMANN
DATA ENinr, LORARY,
a CENTRAL inL£8
HWARD
VSOO
WATER OPERATIONS
a L. MOWER
MANAGER
VI00
SOUD OPERATIONS
A. K. LEMON UANAtXR
PLANT ENGMEERMQ
K.LBAIJL
ES.BERNTSEN
SECRETARY
PF.I IKAQL.
M-705 PLANTTECHMCIANS
W.aACHATZ
J.aAN0ERSON
J. M CHRISTIANSEN
F.D. HOUSTON
aKMULER
MA.SEGRAVE8
MJ.THORNOCK
T. a WYATT
HAZARDOUS
WASTE TEAM
•CaCUHIKt
a D.FULLMER
P. V. HANCOCK
"L
ENVRONMENTAL
WASTE DISPOSAL
TEAM
J.D.HEVREM)
aW.OAKESON
CLOtSEN
aw.STNTTZELL
N.A.STRANaE
a O. TOOLEY
aK. WRIGHT
DOMESTIC WASTEWATER
TREATMENT PLANT
M'S28 AP RECLAMATUN
PLANT TECHMCIANS
M.D. EARL
aLJOHN^ON
D.D.MLDE
aiCMLKES
SUMP TTtUCX OPERATIONS
K. D.PRICE
APPROVAL
CONCURRENCE
D.CMmya
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EFFECTIVE DATE 14 Febiuaiy 1994
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W0#: 1B940 LWR #: ElOtSZ-
SITE: M-19A Photographic Processing Discharge Area
DESCRIPTION: SWMU 553; Pt. of Discharge, Surface
PARAMETERS METHOD
Cadmium 6010
Chromium 6010
Silver 6010
Lead 6010
Nickel 6010
DATE:/5-^/'fcrriME:/045'SAMPLER: v/C^ Af=u-»
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W0#: 1B940 LWR #: ^tOZ^Z^
SITE: M-19A Photographic Processing Discharge Area
DESCRIPTION: SWIV1U 553; 25' Down Gradient, Surface
PARAMETERS METHOD
Cadmium 6010
Chromium 6010
Silver 6010
Lead 6010
Nickel 6010
DATE:/Stf^T-t^TIME:/<54-9 SAMPLER: slChl- Af^uJ
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #:alOZ^Z-
SITE: M-19A Photographic Processing Discharge Area
DESCRIPTION: SWMU 553; 50' Down Gradient, Surface
PARAMETERS METHOD
Cadmium 6010
Chromium 6010
Silver 6010
Lead 6010
Nickel 6010 . ,
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Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #: £'/02'Sr2^
SITE: M-19A Photographic Processing Discharge Area
DESCRIPTION: SWMU 553; 50' Down Gradient, 2'
PARAMETERS METHOD
Cadmium 6010
Chromium 6010
Silver 6010
Lead 6010
Nickel 6010
DATE:/JAyf3TIME: /OSfi-SAMPLER: >^Ct4 AFUJ
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Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #: £/02^2-
SITE: M-19A Photographic Processing Discharge Area
DESCRIPTION: SWMU 553; 75' Down Gradient, Surface
PARAMETERS METHOD
Cadmium 6010
Chromium 6010
Silver 6010
Lead 6010
Nickel 6010
DATE:/30CT?-SnME: HOI SAMPLER: JCH AF^uJ
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W0#: 1B940 LWR #: e:/02^'Z.
SITE: M-19A Photographic Processing Discharge Area
DESCRIPTION: SWMU 553; 100' Down Gradient, Surface
PARAMETERS METHOD
Cadmium 6010
Chromium 6010
Silver 6010
Lead 6010
Nickel 6010
DATE:/3P£TTSTIME: //^ SAMPLER: -JCt* AfuJ Due
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W0#: 1B940 LWR #: ^fOlSZ^
SITE: M-19A Photographic Processing Discharge Area
DESCRIPTION: SWMU 553; 100' Down Gradient, 2'
PARAMETERS METHOD
Cadmium 6010
Chromium 6010
Silver 6010
Lead 6010
Nickel 6010
DATE:'i^TViriME: UtO SAMPLER:^^^ '^P'u) P<-<1
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W0#: 1B940 LWR #: BtOZS:Z-
SITE: M-19A Photographic Processing Discharge Area
DESCRIPTION: SWMU 553; 75' Down Gradient, 2'
PARAMETERS METHOD
Cadmium 6010
Chromium 6010
Silver 6010
Lead 6010
Nickel 6010
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W0#: 1B940 LWR #: JE/CZTT^
SITE: M-19A Photographic Processing Discharge Area
DESCRIPTION: SWMU 553; R. of Discharge, 2'
PARAMETERS METHOD
Cadmium 6010
Chromium 6010
Silver 6010
Lead 6010
Nickel 6010
DATE:/5^^rgriME:/S30 SAMPLER: JcH AFU/
il^D ^:53 ; "PT dF l)i^cm2&.C , ^'
Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: £/eZSZ,
SITE: M-19A Photographic Processing Discharge Area
DESCRIPTION: SWMU 553; 25' Down Gradient, 2'
PARAMETERS METHOD
Cadmium 6010
Chromium 6010
Silver 6010
Lead 6010
Nickel 6010
DATE:/;?<47f JIME:/S^rSAMPLER: /^^'^ ^<^i'^
ISoS: 56-3 * •26" ^ 'bOoJKI C>RAT>l£NT , 2
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Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #: EldZSZ
SITE: M-19A Photographic Processing Discharge Area
DESCRIPTION: SWMU 553; RB
PARAMETERS METHOD
Cadmium 6010
Chromium 6010
Silver 6010
Lead 6010
Nickel 6010
DATEv'3^?a4'3TIME:/S/£3 SAMPLER:-^'i>/ Af*4J
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W0#: 1B940 LWR #: GOISJ-
SITE: M-19A Photographic Processing Discharge Area
DESCRIPTION: SWMU 553; DUP 6'£> Ofil^A^ 6e>^Dia,T
PARAMETERS METHOD 'SO^.^TALOT
Cadmium 6010
Chromium 6010
Silver 6010
Lead 6010
Nickel 6010 . ^.- ,
DATE:/36tr^IME: /^^/S'SAMPLER: 4C H AFuJ
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W0#: 1B940 LWR #: ^'/CZSZ
SITE: M-19A Photographic Processing Discharge Area
DESCRIPTION: SWMU 553; Background, Surface
PARAMETERS METHOD
Cadmium 6010
Chromium 6010
Silver 6010
Lead 6010
Nickel 6010
DATE:/if fly-ft TIME: /03D SAMPLER: JC¥ Af^
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W0#: 1B940 LWR #: £'/02S3
SITE: M-19A Photographic Processing Discharge Area
DESCRIPTION: SWMU 553; Background. 2'
PARAMETERS METHOD
Cadmium 6010
Chromium 6010
Silver 6010
Lead 6010
Nickel 6010
DATE:/#Oc/93nME://^)0 SAMPLER: s/C// /If^tAJ
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W0#: 18940 LWR #: ^/0/3G
SITE: E-517-W Surface Discharge
DESCRIPTION: SWMU 282; R. of Discharge. Surface
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PARAMETERS
Mercury
METHOD
7470
DATE:/gar TIME: 134^ SAMPLER: .AFuJ
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #: B/O/SQ,
SITE: E-517-W Surface Discharge
DESCRIPTION: SWMU 282; R. of Discharge, Surface
PARAMETERS
Volatile Organics
METHOD
8240
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W0#: 1B940 LWR #: ^/0/8Q
SITE: E-517-W Surface Discharge
DESCRIPTION: SWMU 282; Pt. of Discharge, 2'
PARAMETERS
Mercury
METHOD
7470
DATE:ic)CX^M-|ME: 13^ SAMPLER: /^pj
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Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #: £'1016^
SITE: E-517-W Surface Discharge
DESCRIPTION: SWMU 282; R. of Discharge, 2'
PARAMETERS
Volatile Organics
METHOD
8240
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W0#: 18940 LWR #: E'Jl>lB(:>
SITE: E-517-W Surface Discharge
DESCRIPTION: SWMU 282; 25' Down Gradient, Surface
PARAMETERS METHOD
7470 Mercury
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Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #: ^/O/Bh
SITE: E-517-W Surface Discharge
DESCRIPTION: SWMU 282; 25' Down Gradient. Surface
PARAMETERS
Volatile Organics
METHOD
8240
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W0#: 1B940 LWR #: E/0(8i:>
SITE: E-517-W Surface Discharge
DESCRIPTION: SWMU 282; 25' Down Gradient, 2'
PARAMETERS
Mercury
METHOD
7470
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Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #: £/Dl8h
SITE: E-517-W Surface Discharge
DESCRIPTION: SWMU 282; 25' Down Gradient, 2'
PARAMETERS
Volatile Organics
METHOD
8240
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Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #: £lbl90
SITE: M-576-N Surface Discharge
DESCRIPTION: SWMU 271; R. of Discharge. Surface
PARAMETERS METHOD
^ATORATeh 3AA^I>
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Lead
pH
6010
Saturated Paste
DATE:2i^^'"?3TIME:/^/3 SAMPLER: ^^^^
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W0#: 1B940 LWR #: £'/0/fO
~ SITE: M-576-N Surface Discharge
DESCRIPTION: SWMU 271; Pt. of Discharge, 2'
PARAMETERS METHOD
SATUZAT^J^ t^Al^X)
Lead
pH
6010
Saturated Paste
DATE:2^^''^iTIME:/3^4 SAMPLER: AFUJ
l3d^ Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #: e/0l9O
SITE: M-576-N Surface Discharge
DESCRIPTION: SWMU 271; 25' Down Gradient, Surface
PARAMETERS
Lead
pH
METHOD
6010
Saturated Paste
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W0#: 1B940 LWR #: e/Of9o <r/-rl/ (^/An
SITE: M-576-N Surface Discharge -^-^ 77
DESCRIPTION: SWMU 271; 25' Down Gradient. 2' ^
PARAMETERS METHOD
Lead
pH
6010
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W0#: 1B940 LWR #: E/0/90
SITE: M-514 Surface Discharge
DESCRIPTION: SWMU 618; R. of Discharge, Surface
PARAMETERS
Cyanide
METHOD
9010
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DATE:27^t7fjriME:/^2^SAMPLER: AfoJ
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W0#: 18940 LWR #: £/0/9O
SITE: M-514 Surface Discharge
DESCRIPTION: SWMU 618; Pt. of Discharge, 2'
PARAMETERS
Cyanide
METHOD
9010
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DATE:27t)t.r'/'jriME:/^iO SAMPLER: A^OtJ
1100^ Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #: E/0/90
SITE: M-514 Surface Discharge
DESCRIPTION: SWMU 618; 25' Down Gradient Surface
PARAMETERS
Cyanide
METHOD
9010
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W0#: 18940 LWR #: £/6/90
SITE: M-514 Surface Discharge
DESCRIPTION: SWMU 618; 25" Down Gradient, 2"
PARAMETERS
Cyanide
METHOD
9010
DATE:i7oa«r<nME: // / 0 SAMPLER: Af^^^
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Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: E/0f90
SITE: S-501 Surface Discharge
DESCRIPTION: SWMU 266; R. of Discharge, Surface
PARAMETERS METHOD
pH Saturated Paste
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W0#: 18940 LWR #: EtOlfO
SITE: S-501 Surface Discharge
DESCRIPTION: SWMU 266; R. of Discharge, 2'
PARAMETERS METHOD
pH Saturated Paste
DATE: 27<ai^^TIME: \3^ SAMPLER: /\/^(jJ
Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: £10I9(>
SITE: S-501 Surface Discharge
DESCRIPTION: SWMU 266; 25' Down Gradient. Surface
PARAMETERS METHOD
pH Saturated Paste
DATE:27A:^r^TIME: l2S0 SAMPLER: Aft^
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W0#: 18940 LWR #: ^/D/90
SITE: S-501 Surface Discharge
DESCRIPTION: SWMU 266; 25' Down Gradient, 2'
PARAMETERS METHOD
pH Saturated Paste
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W0#: 18940 LWR #: £/t>l9 I
SITE: M-640 Surface Discharge
DESCRIPTION: SWMU 381; Pt. of Discharge, Surface
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pH Saturated Paste
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W0#: 1B940 LWR #: lE"/^/?/
SITE: M-640 Surface Discharge
DESCRIPTION: SWMU 381; Pt. of Discharge, 2'
PARAMETERS METHOD
pH Saturated Paste
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W0#: 18940 LWR#:£7^''^^
SITE: M-640 Surface Discharge
DESCRIPTION: SWMU 381; 25' Down Gradient, Surface
PARAMETERS METHOD
pH
DATE:
Saturated Paste
TIME: SAMPLER:
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W0#: 18940 LWR #: £10191
SITE: M-640 Surface Discharge
DESCRIPTION: SWMU 381; 25" Down Gradient. 2'
PARAMETERS METHOD
pH Saturated Paste
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Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: E/0/9 /
SITE: M-641 Surface Discharge
DESCRIPTION: SWMU 264; Pt. of Discharge, Surface
PARAMETERS METHOD
pH Saturated Paste
DATE:29^r^TIME: //OO SAMPLER: DLC AFUJ
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Thiokol Corporation RCRA Facility Investigation
— W0#: 18940 LWR #: >E/^/f/
SITE: M-641 Surface Discharge
— DESCRIPTION: SWMU 264; Pt. of Discharge, 2'
~ PARAMETERS METHOD
pH Saturated Paste
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W0#: 18940 LWR #: £fOf9l
SITE: M-641 Surface Discharge
DESCRIPTION: SWMU 264; 25' Down Gradient, Surface
PARAMETERS METHOD
pH Saturated Paste
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W0#: 18940 LWR #: £10{9 /
SITE: M-641 Surface Discharge
DESCRIPTION: SWMU 264; 25' Down Gradient, 2'
PARAMETERS METHOD
pH Saturated Paste
DATE:i'^f§'TIME:///r~SAMPLER: DUC_ A^u/
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W0#: 18940 LWR #: BlOl9Z~
SITE: M-585-N Surface Discharge
DESCRIPTION: SWMU 273; Pt. of Discharge, Surface
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PARAMETERS
Volatiie Organics
METHOD
8240
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W0#: 1B940 LWR #:
SITE: M-585-N Surface Discharge
DESCRIPTION: SWMU 273; Pt. of Discharge, 2'
PARAMETERS
Volatile Organics
METHOD
8240
DATE: If ocr TIME: \3otJSAMPLER: T)i-c AFu)
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Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: E/0/9Z^
SITE: M-585-N Surface Discharge
DESCRIPTION: SWMU 273; 25' Down Gradient, Surface
PARAMETERS
Volatile Organics
METHOD
8240
DATE:^''^WlME: 13\V SAMPLER: PLC AfiO
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W0#: 18940 LWR #: E/0192-
SITE: M-585-N Surface Discharge
DESCRIPTION: SWMU 273; 25' Down Gradient, 2'
PARAMETERS
Volatile Organics
METHOD
8240
DATE:2f%^ TIME:/32^ SAMPLER: T^LC AFuJ •n
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/5-40 Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #: ei&l<\3»
SITE: M-606 Surface Discharge
DESCRIPTION: SWMU 527; R. of Discharge, Surface
PARAMETERS
Cyanide
METHOD
9010
DATE:'^"'^^TIME:/2;'c^ SAMPLER?^^.^ ^>^^^
- poi'n f__ofL_4i s cK^rt t s<t/*»v p Le, Wftt SaKAca.Ve^ ^Sa*v<l^
/SlO^ Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #: B\0\'M>
SITE: M-606 Surface Discharge
DESCRIPTION: SWMU 527; Pt. of Discharge. 2' _WvA-^cf_S «A^_ clay
PARAMETERS
Cyanide
METHOD
9010
DATE: 1/av1'5"IME: /•^•.2.JSAMPLER:0 ^Lcw-^^Le^
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(3t< Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: £/0/93
SITE: M-606 Surface Discharge
DESCRIPTION: SWMU 527; 25' Down Gradient, Surface S*^^VA^t<dl S,.i^c/
PARAMETERS
Cyanide
METHOD
9010
DATE: Uo^i^lME:/'^••^SAMPLER:V S^A^^
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W0#: 1B940 LVVR #: ElOl91)
SITE: M-606 Surface Discharge
DESCRIPTION: SWMU 527; 25' Down Gradient. 2*
Ve^ru fi^cc "^qyiA
PARAMETERS
Cyanide
METHOD
9010
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Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: £/0l93
SITE: M-628 Surface Discharge
DESCRIPTION: SWMU 528; Pt. of Discharge. Surface
PARAMETERS
Mercury
METHOD
7470
DATE:3 Nov;92 TIME: 1107- SAMPLER: ^=*V H AF\AJ
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//(.7- Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: £10/9 "i
SITE: M-628 Surface Discharge
DESCRIPTION: SWMU 528; R. of Discharge. 2'
PARAMETERS
Mercury
METHOD
7470
DATE: 3woo TIME: ^-^ SAMPLER: Pi/H- AF{J
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//2o_ Thiokol Corporation RCRA Facility Investigation
~ W0#: 18940 LWR #: £-/(>/^ 3
- SITE: M-628 Surface Discharge
DESCRIPTION: SWMU 528; 25' Down Gradient. Surface
PARAMETERS
Mercury
METHOD
7470
DATE: "^ M\J<t3TIME: UZ.O SAMPLER: Pvv^ APuJ
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Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: EiOtf'h
SITE: M-628 Surface Discharge
DESCRIPTION: SWMU 528; 25' Down Gradient, 2'
PARAMETERS
Mercury
METHOD
7470
DATE:3M0N>{inME:U 34 SAMPLER: PVH AF^
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1^2^ 777/o/co/ Corporation RCRA Facility Investigation
W0#: 18940 LWR #: f/6/94
SITE: M-593 Surface Discharge
DESCRIPTION: SWMU 274; R. of Discharge. Surface
PARAMETERS
Antimony
METHOD
6010
DATE:3Nou<riTIME:Mi:)2-SAMPLER: p\/H^ A^$^/
yx OF Pt^ei\OLir^g J Sur^acg Saiuplf, - CIfllU _
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j^Q^ Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: E/Olf^
SITE: M-593 Surface Discharge
DESCRIPTION: SWMU 274; R. of Discharge, 2'
PARAMETERS
Antimony
METHOD
6010
OA^E^.•s^^) TlME:l4|t> SAMPLER: AFU) PU H
P4. or 'blSC^^-^Rg Z' SAM^Lg - C.LA>.
I4C> Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #: £-/0/9f
SITE: M-593 Surface Discharge
DESCRIPTION: SWMU 274;.2S^own Gradient, Surface
37'
PARAMETERS METHOD
Antimony 6010
DATE:3 «nr<^TIME:/-4/3 SAMPLER: PxJrt APtJ
_Cuilver.t .wKlC;-ix_f>v:cucY^lcci-Jttt.^JM-iil ^M>{>Le_a'V 2^1
14 Ig; Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #:£•/©/f^
SITE: M-593 Surface Discharge
DESCRIPTION: SWMU 274;^ Down Gradient, 2'
?7'
PARAMETERS METHOD
Antimony 6010
DATE:3NoU<t3TIME:/4/6 SAMPLER: Pl^^f APuJ
27' bdU/N| (^V^A'fai^ErM'y 2' 5AAV?Lb - St\cVL>
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Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: B/0/94
SITE: M-636-SW Surface Discharge
DESCRIPTION: SWMU 367; Pt. of Discharge, Surface
Je.rM_clar^ _^ilt
PARAMETERS
Cadmium
Chromium
Silver
Lead
METHOD
6010
6010
6010
6010
DATE:4Ho\;q3riME:l2^ SAMPLER: l>\it\ MPd:>
l^OQ Ui^K'^v^e -^ peKeT^sAr\i=r •Bs^oub \'^' -s^o-Sj-^ecT iseb^ttrt:
Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: £/0/9^
SITE: M-636-SW Surface Discharge
DESCRIPTION: SWMU 367; Pt. of Discharge, 2'
PARAMETERS
Cadmium
Chromium
Silver
Lead
METHOD
6010
6010
6010
6010
jBu Acv: 5>v UT^W5L
DATE:4M6tfTiTIME: l3Qf> SAMPLER: PVH AF\^
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132Z Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: £/0/ff
SITE: M-636-SW Surface Discharge
DESCRIPTION: SWMU 367;,2S<Down Gradient. Surface
bl'
PARAMETERS METHOD
Cadmium 6010
Chromium 6010
Silver 6010
Lead 6010
DATE:4NO0*t;TlME:13-^Z^AMPLER: VMV^ ^PviJ
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)\V> Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #: J^^£>/f^
SITE: M-636-SW Surface Discharge
DESCRIPTION: SWMU 367;.25^Down Gradient..2^,,
— u>2' le
1 PARAMETERS METHOD
Cadmium 6010
Chromium 6010
Silver 6010
— Lead 60]
DATE:4. NbO<?inME: V^i
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Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #: £lDl9l
SITE: Plant 78
DESCRIPTION: Surface Background for Surface Discharges
PARAMETERS METHOD
Cd. Cr, Ag, Pb, Sb, Zn, Se, Tl, Mn 6010
Mercury ^ A*© 7470
Cyanide l^'^if*^'-* W^'^VPA ^00^ 9010
pH Saturated Paste
8is(2-Ethylhexyl)Phthalate, Nitrobenzene «ar 8Z7o
DATE:1/V0««:JTIMEJ^/5' SAMPLER: pi-^ AFUJ
^ILTS^ ClA^
_ZmE_/>AG%A/JC-
MATTeEfL
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #:
SITE: Plant 78
DESCRIPTION: Surface Background for Surface Discharges
PARAMETERS METHOD
Volatile Organics 8240
DATE: fA;*i/^3TIME: ///S^ SAMPLER: VLC AFUA
'ixE
'fck-*''.*.'
.V A..
//Z^ t' SACXC^UMH S/^PUSS TAfCersf
Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #:
SITE: Plant 78
DESCRIPTION: 2' Background for Surface Discharges
PARAMETERS METHOD
Cd, Cr, Ag, Pb, Sb, Zn, Se, Tl, Mn 6010
Mercury AX>O 7470
Cyanide (3 vx\fete-- WctVod Soo) 9010
pH Saturated Paste
8is(2-Ethylhexyl)Phthalate, Nitrobenzene ^» ^2 70
DATE:?Vtft;f3TlME://rr"SAMPLER: P/.<l >^u^
5';tr
-.>'^•.^
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tlt^ Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #: /T/^/*? 7
— SITE: Plant 78
DESCRIPTION: 2' Background for Surface Discharges
— PARAMETERS METHOD
Volatile Organics 6010
63 I
SILT AA/I? d
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DATE:f A/£'<:?fjjTIME: //ZSHSAMPLER: T>L£. AFLAJ
1420 d>A/ "SITE AT AA'S70 ^U)M.O NO ZgS"
Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: £riOl9l
SITE: M-570 Surface Discharge
DESCRIPTION: SWMU 285; R. of Discharge, Surface
PARAMETERS
Cyanide
pH
METHOD
9010
Saturated Paste
DATE: ?AJgi/97riME: /4-Z.O SAMPLER: C>L<_>^tJ
Pf. OP Vl'SjChartjA ^urfg^.^ Sdnt^/c " ^Q-htrakJ. San<J
jUtJ ^malLjQravj^t J
iM^ Thiokol Corporation RCRA Facility Investigation
'^^— W0#: 1B940 LWR#: E/O/p-J
SITE: M-570 Surface Discharge
DESCRIPTION: SWMU 285; Pt. of Discharge. 2'
PARAMETERS
Cyanide
pH
METHOD
9010
Saturated Paste
DATE:f/W>c;f?riME:/^Z5^AMPLER: DLC Aft^
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Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: £/0t9l
SITE: M-570 Surface Discharge
DESCRIPTION: SWMU 285; 3s: Down Gradient. Surface
M'
PARAMETERS METHOD
Cyanide
pH
9010
Saturated Paste
DATE.4 Wi/f JTIME: /^J-^AMPLER: Pi,C AFU)
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J44o Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #: ElO/'^f
SITE: M-570 Surface Discharge
DESCRIPTION: SWMU 285; .aS* Down Gradient. 2'
44'
PARAMETERS METHOD
Cyanide
pH
9010
Saturated Paste
DATE:?Voi^:3riME: /^^SAMPLER: T?£-^AF^LJ
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Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: £/C>3€'h
SITE: M-197 Surface Discharge
DESCRIPTION: SWMU 483; R. of Discharge. Surface
PARAMETERS
Cd, Cr. Ag, Pb
METHOD
6010
MOi^r
ItAO SOtC-MUe .^MPLE AT 0\ScUA(ti^e Pr.i«-^T- :g~^fl3
DATE:/7M^^TIME: /o40SAMPLER:^FlA^ ,
Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: E/OZ^J
SITE: M-197 Surface Discharge
DESCRIPTION: SWMU 483; R. of Discharge, 2'
PARAMETERS
Cd, Cr, Ag, Pb
METHOD
6010
•g4Mp , S>Lr A^P
C^tfFi-^ de^Y /hoisr-
'Jr
DATE: |7/Jc7j^jnME: iD -So SAMPLER: AfvO )(^ H-
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Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: £-/Ol€l
SITE: M-197 Surface Discharge
DESCRIPTION: SWMU 483; 25' Down Gradient, Surface
PARAMETERS
Cd, Cr, Ag, Pb
METHOD
6010
DATE:|-|ki(i{(AaTIME:\Ci'.c,5 SAMPLER: /vfvJ
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Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: /E'/036'Z
SITE: M-197 Surface Discharge
DESCRIPTION: SWMU 483; 25' Down Gradient, 2'
CLAyt S/Lr A>JO
PARAMETERS
Cd, Cr, Ag. Pb
METHOD
6010
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Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: £/o3£'J,
SITE: M-197-8P Surface Discharge
DESCRIPTION: SWMU 360; R. of Discharge, Surface
PARAMETERS
Volatile Organics
pH
METHOD
8240
Saturated Paste
_Fi«^ _S4/s?D
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DATE:(7(U<v'l3TIME: (lic^ SAMPLER: .M^U^
Ul7 ^)9i^C£ ^AVPLC ?0>»^T Of 0\$CHA^£ -tt^Sd^O POPUCAFE
Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: BfOZ62>
SITE: M-197-8P Surface Discharge
DESCRIPTION: SWMU 360; R. of Discharge, Surface ^^^it SAT^Q ^p
po PLICATE PARAMETERS
Volatiie Organics
pH
METHOD
8240
Saturated Paste
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Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: E/o3€^^
SITE: M-197-BP Surface Discharge
DESCRIPTION: SWMU 360; R. of Discharge. 2'
PARAMETERS
Volatile Organics
pH
METHOD
8240
Saturated Paste
DATE:f7 ^^(N/'JJTIME: \\^'^ SAMPLER:/j^^
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Thiokol Corporation RCRA Faciiity Investigation
W0#: 18940 LWR #: E/03£':::>
SITE: M-197-BP Surface Discharge
DESCRIPTION: SWMU 360; 25' Down Gradient, Surface
PARAMETERS
Volatile Organics
pH
METHOD
8240
Saturated Paste
DATE:i7»JaI'J3TIME:ilZ5 SAMPLER: /\f\^i
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Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: e/OZ^^
SITE: M-197-8P Surface Discharge
DESCRIPTION: SWMU 360; 25' Down Gradient, 2'
PARAMETERS
Volatile Organics
pH
METHOD
8240
Saturated Paste
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JZZC^ Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: £/03S4
— SITE: A-9 Surface Discharge
DESCRIPTION: SWMU 267; R. of Discharge, Surface
^ATURAEtELL
PARAMETERS
Cd, Cr, Ag, Pb
pH
METHOD
6010
Saturated Paste
DATE:/gft/cO. JIME: /izC^SAMPLER: Af^u} 1)LJ1.
SOUML/ 2C7 Pi- O-f X)i^aia.mi Sur-hcc ^OAfpIe^ T
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Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #: £:/o2^4
SITE: A-9 Surface Discharge
DESCRIPTION: SWMU 267; R. of Discharge, 2'
spa Ac/ a Ac/ ^^^u.
PARAMETERS
Cd, Cr, Ag, Pb
pH
METHOD
6010
Saturated Paste
DATE: /g %Q^ TIME: IZZO SAMPLER: f{F(jd Di-^
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W0#: 18940 LWR #: El^^^4
SITE: A-2 Surface Discharge
DESCRIPTION: SWMU 560; R. of Discharge, Surface ^ajicLaA<i^^^tut./_
PARAMETERS
Cd, Cr, Ag, Pb. Mn
pH
METHOD
6010
Saturated Paste
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TCCcn-T c/i-ic/tartje._
DATE: TlME:/3o7 SAMPLER: AFUJ ticc^
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Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: E/03S'4
SITE: A-2 Surface Discharge
DESCRIPTION: SWMU 560; R. of Discharge. Surface
PARAMETERS
Volatile Organics
METHOD
8240
DATE:^A/o^ TIME:/507 SAMPLER: AFUJ D^C.
'i;'»'
5uJAA.t> $"^0 P^ af T>iscJUij< Surft.c<. — ^<?^5
^3/(, Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: £/o2^^
SITE: A-2 Surface Discharge
DESCRIPTION: SWMU 560; R. of Discharge, 2'
GraycJ^^JdLL.
.a/ld_S/f'f^
PARAMETERS
Cd, Cr. Ag. Pb. Mn
pH
METHOD
6010
Saturated Paste
DATE:/8AJ§<^ TIME:/5/to SAMPLER: f^uj j}i.c_
3\idmj ft- of JisckojXj^ Z Jamp/c, - JlXthls
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13/(^ Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: ET/OZS^
SITE: A-2 Surface Discharge
DESCRIPTION: SWMU 560; R. of Discharge, 2'
PARAMETER.<i
Volatile Organics
METHOD
8240
DATE:/e^oo TIME: I3n^ SAMPLER: AFJ> OL^L
^f_^c/i^chara^ ^Z L.S<ifHp//^^L.^<:>C3.
71
\ZU> Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: £'fOSS-f
SITE: A-2 Surface Discharge
DESCRIPTION: SWMU 560; 25' Down Gradient, Surface
PARAMETERS
Cd. Ox, Ag. Pb. Mn
pH
METHOD
6010
Saturated Paste
DATE:/fi^'' TIME: t32D SAMPLER: fy-Fo^ t>c<. 95
Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: £r/c3Sf
SITE: A-2 Surface Discharge
DESCRIPTION: SWMU 560; 25" Down Gradient. Surface
PARAMETERS
Volatile Organics
METHOD
8240
^QnJjifiJ A? t^^ / "M
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DATE:/^^,TIME: /JZs> SAMPLER: AEtA> pLC^
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W0#: 18940 LWR #: /f/0 55-^
. SITE: A-2 Surface Discharge
DESCRIPTION: SWMU 560; 25' Down Gradient. 2'
PARAMETERS
Cd. Cr. Ag. Pb, Mn
pH
METHOD
6010
Saturated Paste
Sa^d gjiel ^ntue.1
DATE:/SAitft/TIME:/5?<D SAMPLER: bt^ Af=cJ
••»^' ?• i..r
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Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: /T/OiS'-f
SITE: A-2 Surface Discharge
DESCRIPTION: SWMU 560; 25' Down Gradient. 2'
PARAMETERS
Volatiie Organics
METHOD
8240
DATE:/6AA?«'^IME:/3?^ SAMPLER: AFLJ> VCC
26"^ VouJh/ (SZAOIEA/T Z' SOMples frir AAchls QAC/
Voiafi/'i dAqaA/£5
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13^ Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LVJRi^: E/OlS'f
SITE: A-2 Combined Surface Discharges
DESCRIPTION: SWMUs 451.560; R. of Discharge. Surface
PARAMETERS
Cd. Cr. Ag. Pb. Mn
pH
METHOD
6010
Saturated Paste
JSAMb^^3lLT__fC ZAoeiL
DATE:/ffAr*(/*3TIME:/35-/ SAMPLER: AFtu DU.
Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: e/03^4-
SITE: A-2 Combined Surface Discharges
DESCRIPTION: SWMUs 451,560; R. of Discharge. Surface
PARAMETERS
Volatile Organics
METHOD
8240
DATE:/<9A/gtY^TIME:/357 SAMPLER: AFU^ VLC
ijiT'^rf-r?^?*^
/io^_ Thiokol Corporation RCRA Facility Investigation
W0#: 1B940 LWR #: £/OSSf
SITE: A-2 Combined Surface Discharges
DESCRIPTION: SWMUs 451.560; R. of Discharge. 2'
PARAMETERS
Cd. Cr. Ag, Pb, Mn
pH
METHOD
6010
Saturated Paste
SAf/t> *• '^/LT
DATE:/gA/oc!^3TIME:/^ke SAMPLER: £>cc />tp<^
73
Thiokol Corporation RCRA Facility Investigation
W0#: 18940 LWR #: £/03S'^
SITE: A-2 Combined Surface Discharges
DESCRIPTION: SWMUs 451.560; R. of Discharge. 2"
PARAMETERS
Volatile Organics
METHOD
8240
DATE:/$<<;tf(A}fIME: 14^ SAMPLER: j)u: AFUJ
^(UMO 4E/f'S-£,0 Cl^l,/nt.J "PlduJ Pt df^ 'DisJia^ 2'
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ENVIRONMENTAL LAB WORK REQUEST f J/^ ^/
kro: THIOKOL E^rVIRO^fMENTAL LABORATORY
FHOM;
ORGANIZATION eM\//fv em/z.
EXTENSION
6'S9C>
MAIL STOP
30/^
LWR No. E10252
\/^0
WORK ORDER
/694D
DATE
REPORT RESULTS TO:
HELEN WARD. MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS
af'itUixAf^: •Stfi'^
>3 <xf
l^ M-i^A
SA/UL> SSS
l^'3. M.-\^A
ISCscf^j 1/ IMC UlD-Cd,Cr,A^,9to,^/'i
k
^/* M-J94
HAi-rqi / PT ©F "bi^^w^L' /3S0 /^^)/g- Gci^C^,A^,\>hV\
svuuL' 6-s:^ I5<3ct'i:i v/ 25"' "DCiJ^M GeAiM
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^« M-i9A^
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iZocm •25' &Ctt;^ ^^''"t^^/^^ ioiC>^CA,Cr,A^: H,/J]
incurs ^ /C^l &CIO 'C4,Cr, /\^,Pb,^>
u \Zea93 1/ 2^ /^5'S /^/c-CAXn /4f, /^^/j,
U' /Joafi t/ hcic CA,C^, Acj, Ph>/Ji
.JT Ahi9A iiicrr!, \/ /$^/f - (U,Cr, A^, Pi.,V,
/3«./fi ^ 7ir' Dcw^v <^e/»P tfUJf
M-i'^A iZic'dii i/ /CO' ZJ^t^'A/ ^I7i
IPC/O' CA, tt, f^tf: Pi>,i^'
ilOcpfj ^ IOC''OOit''tJ(i/iAV^
2'
I
lliO_ eo/c^ cj,Cr, >^, ^.^
CHAIN OF CUSTODY
REUNQUISHED BY DATE TIME RECEIVESBY DATE TIME
-a^JJM^ I40cr<ii /4S0 'J^y^-Z^-E'A^n /-(/^
FOR LABORATORY USE ONLY
DATE CXJVtPLETED DATE REPORTQ)
ENVIRONMENTAL LAB WORK REQUEST Cil IVDIE
k™ TfflOKOL ENVIRONMENTAL LABORATORY
FHOM:
ORGANIZATION
efJyjUC EA/6t
EXTENSION
6-3W
MAIL STOP
30/ r
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7- di^^-
COSTCENTEK WORK ORDER
/894^
DATE
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REPORT RESULTS TO;
HELEN WARD, MS 301
\y
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1
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SAMPLE
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3.
6.
7.
8.
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10.
11.
li
DATE
il£>u9i
{4CU'iS
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TYPE
G
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SAMPLE
LOCATION
V.tf4^E 8/.AVK
BiCk6^2^JL^ S^XF
'S^KGeCQKiD, I.'
INFORMATION
TIME
/^/D
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TEST
^010 C^,Cr,A^,P6,hJi
(oC/D OdiO, /^^,Ph,hJi
iiO/0 C^,/^r, /%, f^h, /f/
RE>L\RKS
CHAIN OF CUSTODY
R£UNQi;iSHED BY DATE TIME RECEIVED BY DATE TIME
-4^iUQjiL /40a 9.} /4rc £^//A^,r^ 7^-/^- ^/ /^P3
FOR LABORATORY USE ONLY
4 DATE COMPLETED DATE RS>ORTEO SIGNATURE
November 10, 1993 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 1
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Orders 9310015 Sample and Test Code Identification
Lab ID:
OlA
Ub ID:.
02A
Lab ID:
03A "
k 1 r
Lab ID:
04A
Lab ID:
05A
Lab ID:
06A
Lab ID:
07A
k.
Sample ID:
M-19A; PT. OF DIS. SURFACE
Sample ID:
M-19A; PT. OF DIS. 2Fr.
Sample ID:
M-19A; 25FT. DN. GRAD. SUR
Sample ID:
M-19A; 25FT. DN. GRAD. 2FT
Sample ID:
M-19A; SOFT. DN. GRAD. SUR
Sample ID:
M-19A; SOFT. DN. GRAD. 2FT
Sample ID:
M-19A;DUP SOFT DN.GRAD.SUR
Test Codes and Names
CD AE2 Cadmium
CR AE2 Chromium
PB~AE2 Lead
NI A£2 Nickel
AG_AE2 Silver
Test Codes and Names
CD AE2 Cadmium
CR AE2 Chromium
PB AE2 Lead
NI AE2 Nickel
AO_AE2 Silver
Test Codes and Names
CD_AE2 Cadmium
CR AE2 Chromium
PB AE2 Lead
WAE2 Nickel
AG_AE2 Silver
Test Codes and Names
CD A£2 Cadmium
CR AE2 Chromium
PB A£2 Lead
Nl AE2 Nickel
AG_AE2 Silver
Test Codes and Names
CD_AE2 Cadmium
CR AE2 Chromium
PB"AE2 Lead
NI"AE2 Nickel
A<r_AE2 Silver
Test Codes and Names
CD_AE2 Cadmium
CR AE2 Chromium
PB AE2 Lead
NPAEZ Nickel
AG_AE2 SUver
Test Codes and Names
CD AE2 Cadmium
CR AE2 Chromium
PB"AE2 Lead
NrAE2 Nickel
AG AE2 Silver
Method
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846. 6010
SW-846. 6010
Method
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846. 6010
Method
SW-846. 6010
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
Method
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846. 6010
SW-846, 6010
Method
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846. 6010
SW-846. 6010
Method
SW-846. 6010
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 6010
Lab ID:
~08A
Sample ID:
M-19A; 75Fr. DN. GRAD. SUR
Test Codes and Names
CD_AE2 Cadmium
CR~AE2 Chromium
PB AE2 Lead
NrAE2 Nickel
AG AE2 Silver
Method
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846. 6010
SW-846, 6010
Lab ID: Sample ID:
09A M-19A; 75FT. DN. GRAD. 2FT
Test Codes and Names
CD_AE2 Cadmium
CR2AE2 Chromium
PB_AE2 Lead
NI_AE2 Nickel
AG AE2 Silver
Method
SW-846, 6010
SW-846. 6010
SW-846. 6010
SW-846, 6010
SW-846. 6010
Lab ID: Sample ID:
IOA M-19A;100FT. DN. GRAD. SUR
Test Codes and Names
CD_AE2 Cadmium
CR~AE2 Chromium
PB"AE2 Lead
NrAE2 Nickel
AG A£2 Silver
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Lab ID:
llA
Sample ID:
M-19A;100FT. DN. GRAD. 2FT
Test Codes and Names
CD_AE2 Cadmium
CR~AE2 Chromium
PBJAE2 Lead
NI AE2 Nickel
ACJ AE2 Silver
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Lab ID: Sample ID:
12A M-19A; RINSE BLANK
Test Codes and Names
CD AE2 Cadmium
CR~AE2 Chromium
PBrAE2 Lead
NI_AE2 Nickel
AG AE2 Silver
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Sample ID:
M-19A; BACKGROUND SURFACE
Test Codes and Names
CD AE2
CR~AE2
PB_AE2
NI AE2
AG AE2
Cadmium
Chromium
Laad
Nickel
Silver
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Lab ID: Sample ID:
14A M-19A; BACKGROUND 2 FT.
Test Codes and Names
CD_AE2 Cadmium
CR~'AE2 Chromium
PB~AE2 Lead
NI~AE2 Nickel
Ad AE2 Silver
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Workorder rnmmente
:^=^2::3^2_
Certifi^5y
This is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: M-19A; PT. OF DIS. SURFACE Lab ID: 9310015-01A CoUected: 10/13/93 10:45:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Laad
Nickel
Sliver
u
11.010
9.3757
11.212
U
ug/g
ug/g
ug/g
ug/g
ug/g
0,
1.
5,
2.
0.
.6
.0
.0
.0
.5
11/05/93
11/05/93
11/05/93
11/05/93
11/05/93
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
Sample ID: M-19A; PT. OF DIS. 2FT. Lab ID: 9310015-02A CoUected: 10/13/93 13:30:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
L^ad
•:.l
Silver
16
12.
32.
U
.039
.156
.390
U
ug/g
ug/g
ug/g
ug/g
ug/g
0,
1,
5,
2,
0,
.6
.0
.0
.0
.5
11/05/93
11/05/93
11/05/93
11/05/93
11/05/93
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
Sample ID: M-19A; 25FT. DN. GRAD. SUR Lab ID: 9310015-03A CoUected: 10/13/93 10:49:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Lead
Nickel
Silver
u
10.970
7.6592
10.576
U
ug/g
ug/g
ug/g
ug/g
ug/g
0.6
1.0
5.0
2.0
0.5
11/05/93
11/05/93
11/05/93
11/05/93
11/05/93
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
Sample ID: M-19A; 25FT. DN. GRAD. 2FT Lab ID: 9310015-04A CoUected: 10/13/93 15:05:00
TEST RESXHiT UNITS LIMIT ANALYZED BY METHOD/CAS#
9 ium ug/g 0.6 11/05/93 LVD SW-846, 6010
November 10, 1993 11:27 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 2
^ple ID: M-19A; 25FT. DN. GRAD. 2FT Lab ID: 9310015-04A CoUected: 10/13/93 15:05:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Chromium
Lead
Nickel
Silver
26.283
16.020
22.357
D
ug/g
ug/g
ug/g
ug/g
1.
5.
2.
0,
.0
.0
.0
.5
11/05/93
11/05/93
11/05/93
11/05/93
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
Sample ID: M-19A; SOFT. DN. GRAD. SUR Lab ID: 9310015-05A CoUected: 10/13/93 10:52:00
TEST RESI7LT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Lead
Nickel
TBV l^^^ve
u
18.778
12.828
14.598
1.5148
ug/g
ug/g
ug/g
ug/g
ug/g
0.6
1.0
5.0
2.0
0.5
11/05/93
11/05/93
11/05/93
11/05/93
11/05/93
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
Sample ID: M-19A; SOFT. DN. GRAD. 2FT Lab ID: 9310015-06A CoUected: 10/13/93 10:55:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmi\im
Chromium
Lead
Nickel
Silver
8.2013
506.81
20.293
18.022
96.312
ug/g
ug/g
ug/g
ug/g
ug/g
0,
1.
5,
2.
0.
.6
.0
.0
.0
.5
11/05/93
11/05/93
11/05/93
11/05/93
11/05/93
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
Sample ID: M-19A;DUP SOFT DN.GRAD.SUR Lab ID: 9310015-07A CoUected: 10/13/93 15:15:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmiiim
^kcomium
D
12.884
7.6448
ug/g
ug/g
ug/g
0.6
1.0
5.0
11/05/93
11/05/93
11/05/93
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
6010
6010
6010
November 10, 1993 11:27 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 3
s!I5iple ID: M-19A;DUP SOFT DN.GRAD.SUR Lab ID: 9310015-07A CoUected: 10/13/93 15:15.00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Nickel
Silver
8.8478
1.0083
ug/g
ug/g
2.0
0.5
11/05/93
11/05/93
LVD
LVD
SW-846,
SW-846,
6010
6010
Sample ID: M-19A; 7SFT. DN. GRAD. SUR Lab ID: 9310015-08A CoUected: 10/13/93 11:01:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Lead
Nickel
Silver
0.62033
19.539
12.662
14.229
2.9978
ug/g
ug/g
ug/g
ug/g
ug/g
0.6
1.0
5.0
2.0
0.5
11/05/93
11/05/93
11/05/93
11/05/93
11/05/93
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-84e,
SW-a46,
SW-846,
6010
6010
6010
6010
6010
laple ID: M-19A; 7SFT. DN. GRAD. 2FT Lab ID: 9310015-09A CoUected: 10/13/93 11:15:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Lead
Nickel
Silver
3.6946
41.311
13.275
12.945
46.252
ug/g
ug/g
ug/g
ug/g
ug/g
0.6
1.0
5.0
2.0
0.5
11/05/93
11/05/93
11/05/93
11/05/93
11/05/93
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
Sample ID: M-19A;100FT. DN. GRAD. SUR Lab ID: 9310015-lOA CoUected: 10/13/93 11:04:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Lead
Ekel
i>...j.ver
0.60093
19.339
14.294
16.009
31.097
ug/g
ug/g
ug/g
ug/g
ug/g
0.6
1.0
5.0
2.0
0.5
11/05/93
11/05/93
11/05/93
11/05/93
11/05/93
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
November 10, 1993 11:27 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 4
S!!":ple ID: M-19A;100FT. DN. GRAD. 2FT Lab ID: 9310015-llA CoUected: 10/13/93 11:10:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromi\im
Lead
Nickel
Silver
1.3747
20.053
20.984
28.017
104.00
ug/g
ug/g
ug/g
ug/g
ug/g
0,
1,
5,
2,
0,
.6
.0
.0
.0
.5
11/05/93
11/05/93
11/05/93
11/05/93
11/05/93
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
Sample ID: M-19A; RINSE BLANK Lab ID: 9310015-12A CoUected: 10/13/93 15:10:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Lead
Silver
4.3884
U
U
14.8913
U
ug/L
ug/L
ug/L
ug/L
ug/L
3.5
5.0
25
10
3.0
11/05/93
11/05/93
11/05/93
11/05/93
11/05/93
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
Sample ID: M-19A; BACKGROUND SURFACE Lab ID: 9310015-13A CoUected: 10/14/93 10:30:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS«
Cadmium
Chromium
Lead
Nickel
Silver
19
14
18
U
.272
.466
.194
n
ug/g
ug/g
ug/g
ug/g
ug/g
0.6
1.0
5.0
2.0
0.5
11/05/93
11/05/93
11/05/93
11/05/93
11/05/93
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
Sample ID: M-19A; BACKGROUND 2 FT. Lab ID: 9310015-14A CoUected: 10/14/93 11:00:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
^^•ium
C_omium
D
26.371
ug/g
ug/g
0.6
1.0
11/05/93
11/05/93
LVD
LVD
SW-846,
SW-846,
6010
6010
November 10, 1993 11:27 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 5
^ple ID: M-19A; BACKGROUND 2 FT. LabID: 9310015-14A CoUected: 10/14/93 11:00:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Lead
Nickel
Silver
13.690
18.420
U
ug/g
ug/g
ug/g
5.0
2.0
0.5
11/05/93
11/05/93
11/05/93
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
6010
6010
6010
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1.1J with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ENVIRONMENTAL LAB WORK REQUEST f J/i?^/^^
r THIOKOL ENVIRONMENTAL LABORATORY
f - —
^A>P^ k/ALlc^
1 OaOAMZAnoN 1 ^M/w em/z.
LWR No. £10252
- - II
cnroMH
S59o
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'Zo/6'
cor^a^m• WORK ORDSS
/694d
ten II
/^/)^r95 II
UPOITKBULXS TOi
HELEN WARD. MS 301
SAMPLE INFORMATION
SAMPLE OATE TYPE LOCAHON TIME TEST XEMARXS
-i-^>3_JLJ^
.WT<ifi(iinj' t5M»
M-H/V
SWUU SSS
V iW.-v9A
^OifA-O SSS
lB0cI«i2
rvcw:
l3-acrn
v
^
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fc^lO-Ca,Cr,A^j?b,fc/'l
^tf;g'QJ,Ci'^A^^f>W^A/i
ld*-9 ^tf/C' Cj,Cr,A<^,Ph,ili
/3^7^
/2<»«3
•"
I/"
•25' 2>c«/^ ^Z^P'^ ^^/€d^
AOKiear
^OlO^CA,Cr,A^. Ph,M'l
/o^t lifQ/O'CJA* ^^.Pb,Mi
(^'^ 1/ ZL /O^^' ^/0'CJ,C^> /^f; ^^A^<
:SUiti\) SS3 l^cafji t/ t 757^' ^Q/g " 6/, ^z-. A^, Pb, U\
, y^/>ht9A
/3^icr?3
GfiN^T
ML IC/D' CJ,Cr, A^, Ph,N\
;3aa* fc/ ni^'ho/o-QA,Cr, At^,Pb,/ifi
, ^'•Ai-/<?A FZici<f^ 1/ &BApi0>T
//df /i?O/0' CA, tr, A^, Ph,lii
nocpfj i/
//^^ ' "DOtt/UaZAVyeUT
J1ID_ 6o/o-CJ,Cr, Af, Pi,^
CHAIN OF CUSTODY
RELINQUISHES BY DATE TIME RECETVESBY OATE TIME
-^-MJMi^ f40cr9i, /4S0 A ^A^^y.^-Zi^'E^-'^i /'^^
/
FOR LABORATORY USE ONLY
DATSCOMPLCnS DATSREMims SIC^ATW
December 21, 1993 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 1
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Orders 9311020
LabID: Sample ID:
OlA M-19A; SOFT. DN. GRAD. 2FT
Sample and Test Code Identification
Test Codes and Names Method
CD_AE2 Cadmium SW-846. 6010
CR AE2 Chromium SW-846,6010
PB_A£2 Lead SW-846, 6010
NI_AE2 Nickel SW-846, 6010
AG AE2 Silver SW-846, 6010
Wnrknrder Comments
Report: THIS SAMPLE IS A RERUN FROM WORK ORDER 9310015, LWR E10252
SAMPLE #06A.
This is to cenify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: M-19A; SOFT. DN. GRAD. 2FT Lab ID: 9311020-OlA CoUected: 10/13/93 10:55:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium 7.206 ug/g 0.2 12/03/93 LVD SW-846, 6010
Chromium 514.5 ug/g 0.62 12/03/93 LVD SW-846, 6010
Lead 18.05 ug/g 3.1 12/03/93 LVD SW-846, 6010
Nickel 18.54 ug/g 1.2 12/03/93 LVD SW-846, 6010
Silver 93.66 ug/g 0.1 12/14/93 LVD SW-846, 6010
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. I.IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
C-Ki
ENVIRONMENTAL LAB WORK REQUEST ^1//D:^1
L TO! TfflOKOL ENVmONMFNTAL LABORATORY
FSOM:
ORGANIZATION
SmNSION
MAO. STOP
3oi er
LWR No. E10356
\f^0
WOBKOBDBI DATS
2.2 >J0U<?'3
BVOrr BBnjLTI TOi 1
HELEN WARD, MS 301
i/
1/
• I
SAMPLE
5^' Dou/t/Ctifip
1 /W-/^-*
3.
4.
5.
«.
7.
t.
^ 9.
10.
11.
a
DATE
D/evr
Ttre.
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K
K
c
SAMPLE INFORMATION
LOCATION
A/'/f/l
/A-/fA
TIME
/4Ze>
/45D
TEST
^1/Ve.r - 6>0/0
^i/y£r - SO/C
KEMAKX.S
CHAIN OF CUSTODY
RELINQUISHED BY DATE TIME RECETVESBY DATE TIME
4:^1 ^HL -ISNDV^ /52© //A/Z/j^y..,.^ v/- A^i' rr y"^-^^
T
FOR LABORATORY USE ONLY i DATE COMFLETQ) DATE REPORTED acruTUBB
December 21, 1993 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 1
SENT
TO:
Environmental Morutoring
Helen Ward
M/S 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Oty, Ut 84302-0707 Analytical Labs M/S 245 Attn: Dr. John Terry
Tele: 801-863-2384
Work Order # 9311027 Sample and Test Code Identification
LabID:
OlA
Lab ID:,
02A
Sample ID:
M-19A;50FT. DN. GRAD. 2FT.
Sample ID:
M-19A;250FT. DN.GRAD.1-2FT
Test Codes and Names
AG_AE2 Silver
Test Codes and Names
AG_AE2 Silver
Workorder Comments
Method
SW-846, 6010
Method
SW-846, 6010
Workorder: Analysis of a dupUcate of the sample labeled M-19A;250 ft.
Dn. Grad. 1-2 ft. shows a sample homogeneity problem. The
matrix spikes also indicated this problem. The higher of the
dupUcate results is reported here.
This is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
m
Sample ID: M-19A;50FT. DN. GRAD. 2FT. LabID: 9311027-OlA CoUected: 11/22/93 14:20:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Silver 46.45 ug/g 0.1 12/14/93 LVD SW-846, 6010
Sample ID: M-19A;250FT. DN.GRAD. 1-2FT LabID: 9311027-02A CoUected: 11/22/93 14:30:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Silver 135.8 ug/g 0.1 12/14/93 LVD SW-846, 6010
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1. IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ENVIRONMENTAL LAB WORK
^^/,^M /"^//^^'i ^'^f^
ORK REQUEST —Y 7 /U
^ ^EE^ E
^^^OKOL ENVIRONMENTAL LABORATORY
p^ k/AUez. ocnmiaM
6-590
MAO. STOP
3^/r
LWR No. E10252
ooiTcarma
\A^0
WO«KOM>a
/694D
OATR
RHPORT RBWLTS TOi
HELEN WARD. MS 301
- SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS
fit" 'jiiiMKat n
V
V
l3CicT«vs \/
r5Air<t! PT of t>r4t«A^r
4>6lO»Cci,Cr,/\^j?b,^/'>
/330 ^<3/g' <2e:<^(:i'^A^, f>k^A/i
^^. /3<acrn v/ 2<r' "DeoiM GeAl <ad
^v;r^
u.^' >W-/9/»
,<iiiXill ^^^ izocm \A -25' licui^ (Sz^on ^r^^
/D49 &d/C ' Cd, Cr, A<^, Ph, ki'i
UiO-CA,Cr,At^, Pb,A/i
J^ M-t9A-
iZCCZ^Z 1/ •SURFACE'
^a/ta&T /O^l laOlD'CJ,Cr, A^,Ph,^/i
u llSCi'n 1/ ZL /0^€' ^/D'CJXr, /4f; Ph.fi, ^c^/>. yi-1
m iA/Vi-i9A
SIOUX) SS3 Tiai9S t/
Dc'P £"0' Dew*/
3V/^5NT ,^^SF^/SI^ hOfC' (U,Cr, A, Pbt/ii
l36cr9S V SiiOFACE
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/30a* i/ 7£"' DO(PU 6SAP.
2-L. ni^'to/0'QA,Cr, A^,Pb,A^,
JZiCT^i [/ /CO' ticuftj
2ijS£Ai£L
^fiApiGvT
//of /ffOfO'CA, tr, A^, Ph,kJt
iiDcvij\ \y 2' iflO ^010- C4,Cr, Aif, Pi,^
CHAIN OF CUSTODY
RFIXVQl/ISHED BY
-ffU/.lh/i^
OATE
1400791
TIME
/4S0
RECEIVED BY
//////'E^^y^.
DATE
-/t^-/^^^-^
TIME
/•^^
FOR LABORATORY USE ONLY
DATE COMPLETED DATE RUHIKUD SIGNATURE
February 11, 1994
SENT
TO:
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 1
Environmental Monitoring
Helen Ward
M/S 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707 Analytical Labs M/S 245 Attn: Dr. John Terry
Tele: 801-863-2384
Work Order # 9401007 Sample and Test Code Identification
LabID:
OlA
Sample ID:
M-19A; SOFT. DN. GRAD. 2FT
Test Codes and Names
1311 TCLP Meuls/SemiVols Extr.
CD AE2 Cadmium
CR AE2 Chromium
PB AE2 Lead
AG_AE2 Silver
Workorder Comments
Method
SW-846. 1311
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Report: THIS SAMPLE IS A RERUN FROM WORK ORDER #9310015,
SAMPLE 06A.
dertifi^jl^
TTiis is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: M-19A; SOFT. DN. GRAD. 2FT LabID: 9401007-OlA CoUected: 10/13/93 10:55:00
TEST
TCLP Metali
Cadmium
Chromium
Lead
Silver
s/SamiVols Extr.
RESULT
01/27/94
62.6
5.00
U
162
TJNITS
DATE
ug/L
ug/L
ug/L
ug/L
LIMIT
2
5
25
3
ANALYZED
02/02/94
02/02/94
02/02/94
02/02/94
BY
LVD
LVD
LVD
LVD
LVD
METHOD/CAS#
SW-846, 1311
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1. IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
^"h,-.i
ENVIRONMENTAL LAB WORK REQUEST
THIOKOL ENVIRONMENTAL LABORATORY ^LWR No. E10186IM
A.F.' WA/-<B/^ 5-390
OOVTUMUI
V4i>o
WOWCI
1B94^
MIS
ORCAraZATION
E/dU/2.0 Ei/QR
MAO. (TOP
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RDOBT RBU.n TOI
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME Tisrr REMARKS
u
V
/B-DcFh X /34^ MFRCOIZH (7^70)
"• iT-SJT UJ /P-OTf. K /3^3 lA>iAT/L, £-A^6AM/c5 (e Z^, ^)
u •iix)tx\j -2.0Z. /6-ccr93 tr pr. ^ tm<MA26B /34S' MFTecoeu (7^70)
V
v/
v./
/B-cafz
f>T- 6F 7:)ii.uMQu
2' /34S' I/OCATICE de5Ah(lCS(924C I
' £snw /e-aats K 2S ^ 7>oiPM Q3Wi)f /l^EPCUI^tJL (74-70)
<• EScruJ Id-OcTfJ K 25"' T>oujM'S^'HX&tr
SufZFAc^ I /J5"3 |/(3^/}-r/^^ OTl&AAl/es(eZii^
V t^LU/Ut^ 282. /6-ccr<G K '2S tiOum&S2Ai3i0A'
2' J5^e> /U£f?Cu£ 'l (•7^70)
/B'OcTfJ K •Z'
(SeAtiii i/r
/359 I/O LATIUE C2C>Afi/ICS ( eZ'fQ d -7
CHAIN OF CUSTODY
RI-IJNQUISHED BY
=^M/yi9i//_
DATE
/9>Ccr9l
TIME
/soz—
RFrEIVED BY
^^x^^.^
DATE
V^/^ //^
TIME
/^^-^
FOR LABORATORY USE ONLY
#
DATE COMn.Em> DATE REPOimD SICNATUIE
November 2, 1993 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 1
SENT Environmental Morutoring
TO: Helen Ward
M/S 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order # 9310018
LabID: Sample ID:
01A E-517W;PT. OF DIS. SURFACE
LabID: Sample ID:
02A E-517W;PT. OF DIS. SURFACE
LabID: Sample ID:
03A E-517W;PT. OFDIS.2FT.
LabID: Sample ID:
04A E-517W:PT. OF DIS. 2 FT.
.LabID: Sample ID:
05A E-517W;25FT. DN. GRAD. SUR
LabID: Sample ID:
06A E-517W;25FT. DN. GRAD. SUR
LabID: Sample ID:
07A E-517W;25FT. DN.GRAD. 2FT.
Lab ID: .Samplft ID:
08A E-5l7W;25Fr. DN.GRAD. 2FT.
Sample and Test Code Identification
Test Codes and Names
HO_CV2 Mercury
Test Codes and Names
8240 Volatile Organici
Test Codes and Names
HG_CV2 Mercury
Test Codes and Names
8240 Volatile Organics
Test Codes and Names
HG_CV2 Mercury
Test Codes and Names
8240 Volatile Organics
Test Codes and Names
HG_CV2 Mercury
Test Codes and Names
8240 VoUtile Organics
Workorder Comments
Method
SW-846, 7470
Method
SW-846, 8240
Method
SW-846, 7470
Method
SW-846, 8240
Method
SW-846, 7470
Method
SW-846, 8240
Method
SW-846, 7470
Method
SW-846. 8240
Certifi«rBy
This is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Siample ID: E-517W;PT. OF DIS. SURFACE LabID: 9310018-OlA CoUected: 10/18/93 13:40:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Mercury 95.99 ug/Kg 10 11/29/93 CRS SW-846, 7470
Sample ID: E-517W;PT. OF DIS. SURFACE Lab ID: 9310018-02A CoUected: 10/18/93 13:43:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chl orome theuie
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-chloroethylvinyl ether
^^oroform
^^Borome theme
^bromochloromethane
1,1 -Dichloroetheine
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
Trans 1,2-Dichloroethene
1,2-Dichloropropane
Cis 1,3-Dichloropropene
Trans 1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl- 2 -Pentanone
2-Propanol (IPA)
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2 -Tri chl oroe thouie
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
Chlorobenzene- d5
1,4-Difluorobenzene
jgl^Dichlorobenzene - d4
^M.af luorobenzene
RESULT
U
u
u
a
u
a
u u
u
u u
u
u
u
u u u
u
D
u
u
a
u
u
n u u
u
u
u
u u
u
u u
u
u
u
u
u
u
u
Int. std.
Int. Std.
Int. Std.
Int. Std.
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
LIMIT
100
20
20
5
5
5
10
100
5
5
5
10
10
5
10
5
5
5
5
50
5
5
5
5
5
5
5
5
5
50
500
5
5
5
5
5
5
5
5
50
10
5
ANALYZED
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA.
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
-
540-36-3
-
363-72-4
November 2, 1993 10:35 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 2
cjample ID: E-S17W;PT. OF DIS. SURFACE LabID: 9310018-02A CoUected: 10/18/93 13:43:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Volatile Organics SW-846, 8240
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate %Recovei:y
Dibromofluoromethane 98.9
Toluene-d8 98.8
4-Bromofluorobenzene 104
Recovery Limits
75 TO 125
75 TO 125
75 TO 125
Sample ID: E-S17W;PT. OF DIS. 2 FT. LabID: 9310O18-03A CoUected: 10/18/93 13:45:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Mercury ug/Kg 11/29/93 CRS SW-846, 7470
Sample ID: E-S17W;PT. OF DIS. 2 FT. LabID: 9310018-04A CoUected: 10/18/93 13:45:00
TEST
^Katile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethame
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethy1vinyl ether
Chloroform
Chl orome theuie
Dibromochloromethane
1,1-Dichloroethane
1,2 -Dichloroetheuae
1,1-Dichloroethene
2-Hexanone
Trans 1,2-Dichloroethene
1,2-Dichloropropane
Cis 1,3-Dichloropropene
Trans l,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
^^hylene Chloride
^^•ethyl - 2 - Penteuione
^^ropanol (IPA)
RESULT
U
u
n
u u
u
u
u
u
u D
n
D
u D
u D
u
D
u
o
u
u
u
u u
u
u
u u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
LIMIT
100
20
20
5
5
5
10
100
5
5
5
10
10
5
10
5
5
5
5
50
5
5
5
5
5
5
5
5
5
50
500
ANALYZED
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
November 2, 1993 10:35 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 3
^hple ID: E-S17W;PT. OF DIS. 2 FT.
TEST RESULT
LabID:
UNITS
9310018-04A CoUected: 10/18/93 13:45:00
LIMIT ANALYZED BY METHOD/CAS#
Volatile Organics
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1 -Trichloroetheuie
1,1,2-Trichloroethane
Tri chloroe thene
Trichlorof luorome thauie
Vinyl Acetate
Vinyl Chloride
o-Xylene
Chlorobenz ene-d5
1,4-Difluorobenzene
1,4-Dichlorobenzene-d4
Pentafluorobenzene
lane
.
Int.
Int.
Int.
Int.
U
U
U
U
U
a n u
u
u u Std.
std.
std.
std.
Surrogate/Recc
Surrogate
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
)very Data
Dibromofluoromethane
Toluene-d£ !
4-Bromofluorobenzene
5
5
5
5
5
5
5
5
50
10
5
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240
%Racovery
101
99.0
102
SW-846, 8240
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
-
540-36-3
-
363-72-4
Recovery Limits
75
75
75
TO 125
TO 125
TO 125
Sample ID: E-S17W;2SFT. DN. GRAD. SUR LabID: 9310018-05A CoUected: 10/18/93 13:52:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS*
Mercury ug/Kg 10 11/29/93 CRS SW-846, 7470
Sample ID: E-517W;25FT. DN. GRAD. SUR LabID: 9310018-06A CoUected: 10/18/93 13:53:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
B romodi chlorome thane
Bromoform
Bromomethane
2-Butauione
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
^^iloroethvlvinvl ether
^^^roform
^K>r ome thane
RESULT
U
u u
u
u u
u D
U
U
U
U
u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
LIMIT
100
20
20
5
5
5
10
100
5
5
5
10
10
5
10
ANALYZED
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
November 2, 1993 10:35 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 4
^ple ID: E-517W;25FT. DN. GRAD. SUR Lab ID: 9310018-06A CoUected: 10/18/93 13:53:00
TEST
Volatile Organics
Dibromochlorome thame
1,1-Dichloroethane
1,2-Dichloroetheme
1,1-Dichloroethene
2-Hexcuione
Trans 1,2-Dichloroethene
1,2-Dichloropropsme
Cis 1,3-Dichloropropene
Trans 1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
2-Propanol (IPA)
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethame
1,1,2-Trichloroethane
Tri chloroe thene
^1^ chlorofluoromethane
l^^yl Acetate
^^lyl Chloride
o-Xylene
Chlorobenzene- d5
1,4-Difluorobenzene
1,4-Dichlorobenzene-d4
Pentafluorobenzene
•
RES17LT
Int.
Int.
Int.
Int.
U
U
u
u
u
u u
u
u 0
u
u
u
n u
n
u n D
u u
u u
u
u
u
u std.
std.
std.
std.
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Suirx-ogata
D ibromofluoromethane
Toluene-d8
4-Bromofluorobenzene
LIMIT
5
5
5
5
50
5
5
5
5
5
5
5
5
5
50
500
5
5
5
5
5
5
5
5
50
10
5
ANALYZED
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240
%Recovery
98.3
99.0
104
METHOD/CAS#
SW-846, 8240
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
-
540-36-3
-
363-72-4
Recoveiry Iilmlta
75
75
75
TO 125
TO 125
TO 125
Sample ID: E-S17W;25FT. DN.GRAD. 2FT. LabID: 9310018-07A CoUected: 10/18/93 13:58:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Mercury 16.7 ug/Kg 10 11/29/93 CRS SW-846, 7470
November 2, 1993 10:35 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 5
rlnple ID: E-S17W;25FT. DN.GRAD. 2FT. Lab ID: 9310018-08A CoUected: 10/18/93 13:59:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Volatile Organics Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chlorometheme
Dibromochlorometheme
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
Trans 1,2-Dichloroethene
1,2-Dichloropropane
Cis 1,3-Dichloropropene
^•uis 1,3-Dichloropropene
^^B- D i chl orobenz ene
^^-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl- 2 -Pentanone
2-Propanol (IPA)
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroechane
1,1,2-Trichloroethane
Trichloroethene
Tri chlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
Chlorobenzene- dS
1,4-Difluorobenzene
1,4-Dichlorobenzene-d4
Pentafluorobenzene
Int.
Int.
Int.
Int.
a
U
U
a
u
u
u
u
cr
u
u
u
u
n
u
D
u
u
u
u
u u u
u
u
D
u
u
D
u u
u
D
u u
u
D
D
D
U
U
U
Std.
Std.
Std.
Std.
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
100
20
20
5
5
5
10
100
5
5
5
10
10
5
10
5
5
5
5
50
5
5
5
5
5
5
5
5
5
50
500
5
5
5
5
5
5
5
5
50
10
5
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
10/26/93
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
-
540-36-3
-
363-72-4
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate %Recovery
Dibromofluoromethane 102
Toluene-da 99.9
4-Bromofluorobenzene 102
Recovery Limits
75 TO 125
75 TO 125
75 TO 125
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. I.IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spUce recovery was outside of the specified limits.
ENVIRONMENTAL LAB WORK REQUEST "f//^^^^
m°' TinOKOL ENVIRONMENTAL LABORATORY
mOM:
A. f- n/ALKER-^
ORGANIZATION
E/^i//PO EK/QZ,
EXT¥KSION
^59 O
MAIL STOP
Zo/ E'
LWR No. E10190
COSTCBXTEB
V40O
WORK ORDES
/B'^40
DATIE
2e ocr 9^
Ra>ORT RESULTS TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE UK:ATION TIME TEST l<^ REMARKS
j/> Fr.of D/tiMi^W
TbUTfi i/ AA-S7(,-fJ J/3 S/Vro RATED
2' tbou^i t^ SiiiAiU-Z7f J3z^
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CHAIN OF CUSTODY
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DATE
tecc r^Ef,
TIME
/fZ^
RFJTEIVED BY
I<:71J~-
DATE
^ CtT '^-
TIME
1^/72
4.
FOR LABORATORY USE ONLY
DATE COMPLETE!) DATE REPORTO) SIGNATURE
November 30, 1993 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 1
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Orders 9310028 Sample and Test Code Identification
Lab ID: Sample ID:
OlA M-576-N;PT. OF DIS.SURFACE
LabID: Sample ID:
02A M-576-N;PT. OF DIS. 2 FT.
LabID: Sample ID:
03A M-576-N;25 FT. DN.GRAD.SUR
LabID: Sample ID:
04A M-576-N;25 FT. DN.GRAD.2FT
LabID: Sample ID:
05A M-514;PT. OF DIS. SURFACE
LabID: Sample ID:
06A M-514;PT. OF DIS. 2 FT.
LabID: Sample ID:
07A M-S14;25 FT. DN. GRAD.SUR.
LabID: Sample ID:
08A M-514;25 FT. DN. GRAD. 2FT
LabID: Sample ID:
09A S-501;Fr. OF DIS. SURFACE
LabID: Sample ID:
IOA S-501;PT. OF DIS. 2 FT.
LabID: Sample ID:
llA S-501;25 FT. DN.GRAD. SUR
LabID: Sample ID:
12A s-501 ;25 FT. DN. GRAD. 2FT
PB
PH"
PB
PH
PB
PH
PB
PH
CN
CN
CN
CN
PH.
PH.
PH
Test Codes and Names
A£2 Lead
> pH
Test Codes and Names
AE2 Lead
> pH
Test Codes and Names
AE2 Lead
> pH
Test Codes and Names
AE2 Lead
> pH
Test Codes and Names
_'WT2 Total Cyanide
Test Codes and Names
_WT2 Toul Cyanide
Test Codes and Names
_WT2 Total Cyanide
Test Codes and Names
_WT2 Total Cyanide
Test Codes and Names
_S pH
Test Codes and Names
_S pH
Test Codes and Names
_s pH
Test Codes and Names
PH S pH
Method
SW-846, 6010
SW-846, 9045
Method
SW-846, 6010
SW-846, 9045
Method
SW-846, 6010
SW-846, 9045
Method
SW-846, 6010
SW-846, 9045
Method
SW-846, 9010
Method
SW-846, 9010
Method
SW-846, 9010
Method
SW-846, 9010
Method
SW-846, 9045
Method
SW-846, 9045
Method
SW-846, 9045
Method
SW-846, 9045
WorkorriPr Cnmm^nt^
ITiis is to certify that the following samples were aruilyzed using good laboratory practices
to show the following results.
Sample ID: M-576-N;PT. OF DIS.SURFACE LabID: 9310028-OlA CoUected: 10/26/93 13:13:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Lead
pH
2 7.1 ug/g
10.12 pH Unit
2.0 11/22/93 LVD SW-846, 6010
10/29/93 KEN SW-846, 9045
Sample ID: M-576-N;PT. OF DIS. 2 FT. Lab ID: 9310028-02A CoUected: 10/26/93 13:26:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS #
Lead
pH
10.1 ug/g
7.89 pH Unit
2.6 11/22/93 LVD SW-846, 6010
10/29/93 KEN SW-846, 9045
Sample ID: M-576-N;25 FT. DN.GRAD.SUR Lab ID: 9310028-03A CoUected: 10/26/93 13:39:00
TEST RESULT tJNITS LIMIT ANALYZED BY METHOD/CAS#
ph
16.4 ug/g
9.78 pH Unit
1.86 11/22/93 LVD
10/29/93 KEN
SW-846, 6010
SW-846, 9045
Sample ID: M-576-N;25 FT. DN.GRAD.2FT LabID: 9310028-04A CoUected: 10/26/93 13:41:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Lead
pH
18.0 ug/g
8.39 pH Unit
1.88 11/22/93 LVD
10/29/93 KEN
SW-846, GOlO
SW-846, 9045
Sample ID: M-514;PT. OF DIS. SURFACE LabID: 9310028-05A CoUected: 10/27/93 10:25:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Total Cyanide U mg/Kg 0.25 11/08/93 KEN SW-846, 9010
Sample ID: M-514;PT. OF DIS. 2 FT. Lab ID: 9310028-06A CoUected: 10/27/93 10:30:00
.V RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Towal Cyanide mg/Kg 0.25 11/08/93 KEN SW-846, 9010
November 30, 1993 10:21 CERTIFICATE OF ANALYSIS Page 2
RESULTS BY SAMPLE
Simple ID: M-514;25 FT. DN. GRAD.SUR. LabID: 9310028-07A CoUected: 10/27/93 11:00:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Total Cyanide .34 mg/Kg 0.25 11/08/93 KEN SW-846, 9010
Sample ID: M-514;25 FT. DN. GRAD. 2FT Lab ID: 9310028-08A CoUected: 10/27/93 11:10:00
TEST RESI7LT UNITS LIMIT ANALYZED BY METHOD/CAS#
Total Cyanide .30 mg/Kg 0.25 11/08/93 KEN SW-846, 9010
Sample ID: S-501 ;PT. OF DIS. SURFACE LabID: 9310028-09A CoUected: 10/27/93 13:30:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
pH 7.73 pH Unit 10/29/93 KEN SW-846, 9045
li plelD: S-501;PT. OFDIS. 2FT. LabID: 9310028-lOA CoUected: 10/27/93 13:40:00
T^T RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
pH 7.87 pH Unit 10/29/93 KEN SW-846, 9045
Sample ID: S-501 ;25 FT. DN. GRAD. SUR Lab ID: 9310028-11A CoUected: 10/27/93 13:50:00
TEST REStTLT tJNZTS LZMZT ANALYZED BY METHOD/CAS#
pH 7.79 pH Unit 10/29/93 KEN SW-846, 9045
Sample ID: S-501;25 FT. DN. GRAD. 2FT Lab ID: 9310028-12A CoUected: 10/27/93 14:15:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
pH 7.89 pH Unit 10/29/93 KEN SW-846, 9045
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection Umit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1. IJ with a detection Umit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ENVIRONMENTAL LAB WORK REQUEST f/.v.^^;^
i"^^ TfflOKOL ENVIRONMENTAL LABORATORY
FROM:
A- f- W4LfCER^
ORGANIZATION
EXTDeiON
5S90
MAIL STOP
LWR No. E10191
COST (INTER
\/4dD
WORK ORDER
/B94d
DATE
z9 ^cr 9 z
RQ>ORT RESULTS TO:
HELEN WARD, MS 301
xy
w
l^
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LOCATION
M-MO
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TIME
idBO
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REMARKS
CHAIN OF CUSTODY
^
RF7 JNQUSHED BY
^Jnil.
DATE
t9^'cr 9\7
TIME
/^^'d
RFCEIVfD BY
//Er./'^yE/^/^^^yf^
DATE
-/y^ ->?^ ^J
TIME
E>?y
FOR LABORATORY USE ONLY
DATE COMPLETE DATE REPORTED SIGNATURE
ENVIRONMENTAL LAB WORK REQUEST ^ /^ 'E :EIE >
'r /CI 9 '
\'^' THIOKOL ENVIRONMENTAL LABORATORY
FROM: ,
A, P. WALICES
ORGANIZATION
EXT1NSION
MAIL STOP
5ol ET
LWR No. E1019r ^ .
COSTCBtm
^/4b0
WORKORDEX
ISS4D
DATE
Z^ OCT 9 3
Ra>ORT RESULTS TO:
HELEN WARD, MS 301
y
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v-'
,x
^
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SAMPLE
J- 5U)iUkO 273
s.iuJNto ITS
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LOCATION
M-5"e&- N
AA-^a^^-A/
AA-S-SS-A/
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/W-f55"-A/
M' £35-- Af
TIME
l-SCaO
1506
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B/<^
/320
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TEST
N/oia-^^Vc C)Yc^a»v\cs -S2.40
ll
M
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//
//
REMARKS
CHAIN OF CUSTODY
REIJNQLTSIIEDBY
JLJ/H/L
DATE
^•HCC-T
TIME
isoc
RECEIVED BY
///^/Ef^/7,-f...^
DATE
^^-^9-77
TIME
OV^
^
FOR LABORATORY USE ONLY
DATS COMPLCTB) DATE IIB>ORTn>
November 23, 1993 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 1
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs M/S 245
Atm: Dr. John Terry
Tele: 801-863-2384
Work Order # 9311002
LabID:
OlA
LabID:
02A
Lab ID:
03A
LabID:
04A
LabID:
k 05A
Lab ID:
06A
UbID:
07A
LabID:
08A
LabID:
09A
LabID:
IOA
Lab ID:
llA
1^^
LabID:
13A
Samole ID:
M-640;PT. OF DIS. SURFACE
Samole ID:
M-640;PT. OF DIS. 2 FT.
Sample ID:
M-640;25 FT. DN. GRAD. SUR
Samole ID:
M-640;25 FT. DN. GRAD.2FT.
Sample ID:
M-641 ;PT. OF DIS. SURFACE
Samole ID:
M-641;PT. OFDIS. 2FT.
Sample ID:
M-641;25 FT. DN. GRAD. SUR
Samole ID:
M-641 ;25 FT. DN. GRAD.2FT.
Sample ID:
M585-N;PT. OF DIS. SURFACE
Sample ID:
M585-N;PT. 6FD1S.2FT.
Samole ID:
M585-N;DUP.PT.0F DIS. 2FT.
Samp e ID:
M585-N;25 FT. DN. GRAD.SUR
Sample ID:
M585-N;25 FT. DN. GRAD.2FT
Sample and Test Code Identification
PH_S
PH_S
PH_S
PH_S
PH_S
PH_S
PH_S
PH_S
8240
8240
8240
8240
8240
Test Codes and Names
pH
Test Codes and Names
pH
Test Codes and Names
pH
Test Codes and Names
pH
Test Codes and Names
pH
Test Codes and Names
pH
Test Codes and Names
pH
Test Codes and Names
pH
Test Codes and Names
Volatile Organics
Test Codes and Names
Volatile Orginici
Test Codes and Names
Volatile Organics
Test Codes and Names
Volatile Organici
Test Codes and Names
Volatile Organics
Method
SW-846, 9045
Method
SW-846. 9045
Method
SW-846, 9045
Method
SW-846, 9045
Method
SW-846, 9045
Method
SW-846, 9045
Method
SW-846, 9045
Method
SW-846, 9045
Method
SW-846, 8240
Method
SW-846, 8240
Method
SW-846, 8240
Method
SW-846, 8240
Method
SW-846, 8240
LabID:
14A
•Sample ID:
M585-N;25FT.DN.GRD.2Fr.RB Test Codes and Names
8240 Volatile Organics
Wnrknrder Cnmnientji:
Method
SW-846, 8240
TTiis is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: M-640;PT. OF DIS. SURFACE LabID: 9311002-OlA CoUected: 10/29/93 10:30:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
pH 7.66 pH Unit 11/01/93 KEN SW-846, 9045
Sample ID: M-640;PT. OF DIS. 2 FT. LabID: 9311002-02A CoUected: 10/29/93 10:35:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
pH 7.54 pH Unit 11/01/93 KEN SW-846, 9045
Sample ID: M-640;25 FT. DN. GRAD. SUR Lab ID: 9311002-03A CoUected: 10/29/93 10:40:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
pH 7.72 pH Unit 11/01/93 KEN SW-846, 9045
#± ID: M-640;25 FT. DN. GRAD.2FT. LabID: 9311002-04A CoUected: 10/29/93 10:50:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
pH 7.79 pH Unit 11/01/93 KEN SW-846, 9045
SamplelD: M-641 ;PT. OFDIS. SURFACE LabID: 9311002-05A CoUected: 10/29/93 11:00:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
pH 7.75 pH Unit 11/01/93 KEN SW-846, 9045
SamplelD: M-641;PT. OF DIS. 2 FT. LabID: 9311002-06A CoUected: 10/29/93 11:03:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
pH 7.41 pH Unit 11/01/93 KEN SW-846, 9045
November 23, 1993 10:18
sK
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 2
!!!liple ID: M-641 ;25 FT. DN. GRAD. SUR Lab ID: 9311002-07A CoUected: 10/29/93 11:05:00
TEST REStILT UNITS LIMIT ANALYZED BY METHOD/CAS#
pH 7.66 pH Unit 11/01/93 KEN SW-846, 9045
SamplelD: M-641 ;25 FT. DN. GRAD.2FT. Lab ED: 9311002-08A CoUected: 10/29/93 11:15:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
pH 7.49 pH Unit 11/01/93 KEN SW-846, 9045
Sample ID: M585-N;PT. OF DIS. SURFACE LabID: 9311002-09A CoUected: 10/29/93 13:00:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
||B|inodi chloromethane
IBnoform
l^mome thane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethauie
D i bromoch1oromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2 -Hexanone
Trsins 1,2-Dichloroethene
1,2-Dichloropropane
Cis 1,3-Dichloropropene
Trans 1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4 -Methyl - 2 - Pentauione
2-Propanol (IPA)
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
j*k, 1-Trichloroethane
^B 2-Trichloroethane
i _... chl oroe thene
RESULT
U
u
u u
u u
u u u u u u u u u
u u u
u
u u
u u u u u u u
u u u D
u u
u u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
LIMIT
100
20
20
5
5
5
10
100
5
5
5
10
10
5
10
5
5
5
5
50
S
5
5
5
5
5
5
5
5
50
500
5
5
5
5
5
5
5
ANALYZED
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA.
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
November 23, 1993 10:18 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 3
SaAiiple ID: M585-N;PT. OF DIS. SURFACE LabID: 9311002-09 A CoUected: 10/29/93 13:00:00
TEST
Volatile Organics
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
Chlorobenzene- d5
1,4-Difluorobenzene
1,4-Dichlorobenzene-d4
Pentafluorobenzene
RESULT
U
a u u Int. Std.
Int. Std.
Int. Std.
Int. Std.
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
LIMIT
5
50
10
5
ANALYZED
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
75-69-4
108-05-4
75-01-4
95-47-6
-
540-36-3
-
363-72-4
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
D ibromofluoromethane
Toluene-d8
4-Bromofluorobenzene
%R8Covery
101
100
103
Recovery
75 TO
75 TO
75 TO
Limi
125
125
125
Lts
Sample ID: M585-N;PT. OF DIS. 2 FT. LabID: 9311002-lOA CoUected: 10/29/93 13:06:00
TEST
^^itile Organics
>»wjtone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
B r omome theine
2-ButeUione
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chl oroe theuie
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethame
1,1 -Dichloroethene
2-Hexanone
Trans 1,2-Dichloroethene
1,2-Dichloropropane
Cis 1,3-Dichloropropene
Trcuis 1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
^Bj'^thyl - 2 - Pentanone
^^p.-opanol (IPA)
Su/rene
RESULT
u u u D
u u U
U
u u u u u
u u u
u u
u u u u
u u
u u u u
u u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
LIMIT
100
20
20
5
5
5
10
100
5
5
5
10
10
5
10
5
S
5
5
50
5
5
5
5
5
5
5
5
5
50
500
5
ANALYZED
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
100-42-5
November 23, 1993 10:18 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 4
Sziaple ID: M585-N;PT. OF DIS. 2 FT. LabID: 9311002-lOA CoUected: 10/29/93 13:06:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Volatile Organics
1,1,2,2-Tetrachloroethane Tetrachloroethene
Toluene
1,1,1-Trichloroethame
1,1,2-Trichloroethame
Trichloroethene
Trichlorofluoromethame
Vinyl Acetate
Vinyl Chloride
o-Xylene
Chlorobenzene-d5
1,4-Difluorobenzene
1,4-Dichlorobenzene-d4
Pentafluorobenzene
,ane
Int.
Int.
Int.
Int.
U
U
U
U
u u u u
o u std.
Std.
std.
Std.
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
Dibromofluoromethane
Toluene-d8
4-Bromofluorobenzene
5
5
5
5
5
5
5
50
10
5
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
For Volatile Organic
%Recovery
103
101
97.3
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
IS 8240
SW-846, 8240
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
-
540-36-3
-
363-72-4
Recovery Limits
75
75
75
TO 125
TO 125
TO 125
Sample ID: M585-N;DUP.PT.OF DIS. 2FT. LabID: 9311002-1 IA CoUected: 10/29/93 13:07:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethame
1,1-Dichloroethene
2-Hexanone
Trans 1,2-Dichloroethene
1,2-Dichloropropame
Cis 1,3-Dichloropropene
l^^ns 1, 3 -Dichloropropene
1^^-Dichlorobenzene
J., J -Dichlorobenzene
RESULT
U
D
U
U
U
U
U
u D
U
U
U
U
U
D
u D
U
U
U
U
D
U
U
U
U
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
LIMIT
100
20
20
5
5
5
10
100
5
5
5
10
10
5
10
5
5
5
5
50
5
5
5
5
5
5
ANALYZED
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90'7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
November 23, 1993 10:18 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 5
simple ID: M585-N;DUP.PT.OF DIS. 2FT. LabID: 9311002-11A CoUected: 10/29/93 13:07:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Volatile Organics
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentamone
2-Propanol (IPA)
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Tri chloroe thene
Tri chlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
Chlorobenzene-d5
1,4-Difluorobenzene
1,4-Dichlorobenzene-d4
Pentafluorobenzene
•
tane
Int.
Int.
Int.
Int.
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u Std.
Std.
Std.
Std.
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogati a
D ibromofluoromethame
Toluene-d8
4-Bromofluorobenzene
5
5
5
50
500
5
5
5
5
5
5
5
5
50
10
5
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240
%Recovery
103
103
96.7
SW-846, 8240
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
-
540-36-3
-
363-72-4
Recovery Limits
75
75
75
TO 125
TO 125
TO 125
Sample ID: M585-N;25 FT. DN. GRAD.SUR Lab ID: 9311002-12A CoUected: 10/29/93 13:16:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethame
2-Butemone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethame
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethame
1^1 -Dichloroethame
i^^Dichloroe thame
1^^ Dichloroethene
^ .lexamone
RESULT
U
U
u
u
u u u
u
u
u
u
u
u
u
u
u
u
u
u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
LIMIT
100
20
20
5
5
5
10
100
5
5
5
10
10
5
10
5
5
5
5
50
ANALYZED
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
November 23, 1993 10:18 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 6
g!^ple ID: M585-N;25 FT. DN. GRAD.SUR Lab ID: 9311002-12A CoUected: 10/29/93 13:16:00
TEST REStJLT UNITS LIMIT ANALYZED BY METHOD/CAS#
Volatile Organics
Trams 1,2-Dichloroethene
1,2-Dichloropropame
Cis 1,3-Dichloropropene
Trams 1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl- 2 -Pentanone
2-PropEmol (IPA)
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethame
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethame
Vinyl Acetate
vinyl Chloride
o-Xylene
Chlorobenzene-d5
•
- D i f 1 uorobenz ene
hDichlorobenzene-d4
.cafluorobenzene
Int,
Int.
Int.
Int.
U
U
U
U
U
U
U
U
U
U
U
U
U
U
22
U
U
U
U
U
U
U
Std.
Std.
Std.
Std.
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
SW-846, 8240
5 11/04/93 JMA 156-60-5
5 11/04/93 JMA 78-87-5
5 11/04/93 JMA 10061-01-5
5 11/04/93 JMA 10061-02-6
5 11/04/93 JMA 95-50-1
5 11/04/93 JMA 541-73-1
5 11/04/93 JMA 106-46-7
5 11/04/93 JMA 100-41-4
5 11/04/93 JMA 75-09-2
50 11/04/93 JMA 108-10-1
500 11/04/93 JMA 67-63-0
5 11/04/93 JMA 100-42-5
5 11/04/93 JMA 79-34-5
5 11/04/93 JMA 127-18-4
5 11/04/93 JMA 108-88-3
5 11/04/93 JMA 71-55-6
5 11/04/93 JMA 79-00-5
5 11/04/93 JMA 79-01-6
5 11/04/93 JMA 75-69-4
50 11/04/93 JMA 108-05-4
10 11/04/93 JMA 75-01-4
5 11/04/93 JMA 95-47-6
11/04/93 JMA
11/04/93 JMA 540-36-3
11/04/93 JMA
11/04/93 JMA 363-72-4
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate %Recovery
D ibromofluorome thane 93.4
Toluene-d8 97.1
4-Bromofluorobenzene 119
Recovery Limits
75 TO 125
75 TO 125
75 TO 125
Sample ID: M585-N;25 FT. DN. GRAD.2FT LabID: 9311002-13A CoUected: 10/29/93 13:20:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethame
Bromoform
Bromomethame
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
ij^pr oe thame
f^Biloroethylvinyl ether
^^oroform
RESULT
U
u U
U
D
U
D
U
U
U
U
U
U
U
tINITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
LIMIT
100
20
20
5
5
5
10
100
5
5
5
10
10
5
ANALYZED
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
November 23, 1993 10:18 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 7
S3ple ID: M585-N;25 FT. DN. GRAD.2FT Lab ID: 9311002-13A CoUected: 10/29/93 13:20:00
TEST
Volatile Organics
Chloromethane
Dibromochloromethame
1,l-Dichloroetheme
1,2-Dichloroethane
1,1-Dichloroethene
2 -Hexanone
Trans 1,2-Dichloroethene
1,2-Dichloropropane
Cis 1,3-Dichloropropene
Trans 1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
2-Propanol (IPA)
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethame
1,1,2-Trichloroethane
^aB|phl oroe thene
V^P chlorof luorome thame
v^/1 Acetate
Vinyl Chloride
o-Xylene
Chlorobenzene-d5
1,4-Difluorobenzene
1,4-Dichlorobenzene-d4
Pentafluorobenzene
RESULT
Int.
Int.
Int.
Int.
U
D
U
U
U
U
U
U
U
u u
u
u u
D
U
U
D
U
U
U
U
U
U
U
D
U
U
Std.
Std.
Std.
Std.
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
Dibromofluoromethane
Toluene-d8
4-Bromofluorobenzene
LIMIT
10
5
5
5
5
50
5
5
5
5
5
5
5
5
5
50
500
5
5
5
5
5
5
5
5
50
10
5
ANALYZED
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240
^Recovery
103
102
96.6
METHOD/CAS#
SW-846, 8240
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
-
540-36-3
-
363-72-4
Recovery Limits
75
75
75
TO 125
TO 125
TO 125
Sample ID: M585-N;25FT.DN.GRD.2FT.RB LabID: 9311002-14A CoUected: 10/29/93 13:30:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
I^Bioform
^ly tome thame
2 .lutamone
D
U
U
U
U
U
U
31J
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
100
20
20
5
5
5
10
100
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
November 23, 1993 10:18 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 8
# STliple ID: M585-N;25FT.DN.GRD.2FT.RB LabID: 9311002-14A CoUected: 10/29/93 13:30:00
TEST
Volatile Organics
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethame
Dibromochloromethane
1,1-Dichloroethame
1,2-Dichloroethame
1,1-Dichloroethene
2 -Hexanone
Trams 1,2-Dichloroethene
1,2-Dichloropropame
Cis 1,3-Dichloropropene
Trans 1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentamone
2-Propanol (IPA)
^terene
•B 2,2 -Tetrachloroethane
T^rachloroe thene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
Chlorobenzene-d5
1,4-Difluorobenzene
1,4-Dichlorobenzene-d4
Pent afluorobenz ene
RESULT
Int.
Int.
Int.
Int.
U
U
U
U
U
U
U
U
u u u u D
U
U
U
u u u u
u
u u
u
u u
u
u u u u u
u D
std.
Std.
Std.
Std.
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Surrogate/Recovery Data
Surrogate
D ibromofluoromethame
Toluene-d8
4-B: romofli aorober izene
LIMIT
5
5
5
10
10
5
10
5
5
5
5
50
5
5
5
5
5
5
5
5
5
50
500
5
5
5
5
5
5
5
5
50
10
5
ANALYZED
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
11/04/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240
%Recovery
104
101
96.7
METHOD/CAS#
SW-846, 8240
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
-
540-36-3
-
363-72-4
Recovery Limits
75
75
75
TO 125
TO 125
TO 125
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1. IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
Notes and Comments for Workorder# 9311002
J'entatively Identified Compounds:
Sample ED Compound Amount
9311002-12A methyl(l-methylethyl)benzene 5.5ug/Kg
9311002-14A tetrahydrofuran (JHF) 12ug/L
<i
ENVIRONMENTAL LAB WORK REQUEST / //^Epy ^
W" TfflOKOL ENVIRONMENTAL LABORATORY
FROM:
A. "F WAuK-e^P^
ORGANIZATION
eXTBNSION
MAIL STOP
•3o\e"
LWR No. E10193
OOSTCSNm
V4CO
WORKORDeS DATE
4uo\; (<^qi
REPORT RBSULTS TOi
HELEN WARD, MS 301
y
.y
\y
u
y
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SAMPLE
1 ^\U»U) «"27
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DATE
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TYPE
G
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PC
X.
K
K
)C
X
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SAMPLE INFORMATION
LOCATION
»A-fcGfe>
AA-tCfe)
A\-t6t»
M-(oOU
AA-fel8
M-(oZ8
M-«o28
M-(PZ6
M-IPZ6
TIME
l^\C>
\'a2o
13ZS"
1335-
llOZ.
1117
1\20
IVS4
\\%o
TEST
CvjarvxAc. ^0\0
\1
iV
W
AA.e<iCO«l>f 7470
It
l\
U
l\
REMARKS
CHAIN OF CUSTODY
RFI.TNQUISHEDBY
^laiL—
DATE
Afmu^j.
TIME
IS70
RECEIVED BY
///^//A^..u^
E^'' ''''v
DATE
-//'^-fj
TIME
tf
FOR LABORATORY USE ONLY
DAT^ COMPlfTBD DATE RfTORTH)
ENVIRONMENTAL LAB WORK REQUEST ^"7// ^Of
W°' TfflOKOL ENVIRONMENTAL LABORATORY
FROM:
ORGANIZATION
EXTtMSION
MAIL STOP
"S>OIE:
LWR No. E10194 ^ >
COSTCBNTBR
V40O
WORK ORDOI DATE
4 Mmi 93
REPORT RESULTS TO:
HELEN WARD, MS 301
LX
y
t^
•'
./
1^
^
w/
SAMPLE
1 SOAWLO n4
3. Sli>M,U 274 ,•
4.SWU.U a.14,-
Sur<.u.e. '
7. S\0«AO iW7
TicU R,^%t "BVii,
9. SWJIM; 347
loSuiUwv; 3WT,
1*"
II.
11
DATE
3»404<i2
SMDUn
^•SNog^
^3M0U«
4 WWW
-4Nootl
<^4KW«fJ
<» 4MWX3
"^-^MH^J
TYPE
G
x>
)(
>c
X
K
)C
)(.
)C
^
<
c
SAMPLE INFORMATION
LOCATION
AA-S^3
M-5*^3
M-'S*^^
M-5"T3
M- t.3t»'SvJLl
/U-tSt-'SW'
M-WU-Su;
AA-t3t,-"SbJ
XA^-tSt'-SuO
XA-U3t-SW
TIME
1462.
\4\0
I4\3
\Aie>
125-0
lEoo
lBd>*^
I3Z2-
1330
I33i
TEST
An+imor\v^ - C30IO
\l
II
IV
CdiCr, A^,?b - GOlO
IV
iv
ll
l\
iv
REMARKS
CHAIN OF CUSTODY
REUNQUISnn) RY DATE TIME RECEIVBDBY DATE TIME
JkLh^L_ 4u^i^^:> /S~/0 ///^r/^-... '7/-^'fi /y'/Q
4
FOR LABORATORY USE ONLY
DATE COMPLETED DATE REPORTED
December 6, 1993 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 1
SENT Environmental Monitoring
TO; Helen Ward
M/S 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order # 9311009
LabID:
OlA
LabID:
02A
LabID:
03A
LabID:
04A
LabID:
|0^A
LabID:
06A
LabID:
07A
Lab ID:.
08A
LabID:
09A
LabID:
IOA
LabID:
llA
LabID:
12A
Ub ID:
. 13A
Sample ID:
M-«)6;PT. OF DIS. SURFACE
Samole ID:
M-606;PT. OF DIS. 2 FT.
Sample ID:
M-606;25 FT. DN. GRAD.SUR.
Samole ID:
M-606;25 FT. DN. GRAD.2 FT
Sample ID:
M-628;PT. OF DIS. SURFACE
Sample ID:
M-628;PT. OF DIS. 2 FT.
Sample ID:
M-628;25 FT. DN. GRAD.SUR.
Sample ID:
M-628;25 FT. DN. GRAD.2 FT
Sample ID:
M-628;FIELD RINSE BLAffK
Sample ID:
M-593;PT. OF DIS. SURFACE
Sample ID:
M-593;PT. OF DIS. 2 FT.
Sample ID:
M-593;37 FT. DN. GRAD.SUR.
Sample ID:
M-593;37 FT. DN. GRAD.2 FT
Sample and Test Code Identification
Test Codes and Names
CN_WT2 Toul Cyanide
Test Codes and Names
CN_'WT2 Toul Cysnide
Test Codes and Names
CN_WT2 Toul Cy«nide
Test Codes and Names
CN_WT2 Toul Cyinide
Test Codes and Names
HG_CV2 Mercuiy
Test Codes and Names
HG_CV2 Mercury
Test Codes and Names
Ha_CV2 Mercury
Test Codes and Names
HG_CV2 Mercury
Test Codes and Names
HG_CV2 Mercury
Test Codes and Names
SB_AE2 Antimony
Test Codes and Names
SB_AE2 Antimony
Test Codes and Names
SB_AE2 Antimony
Test Codes and Names
SB AE2 Antimony
Method
SW-846, 9010
Method
SW-846, 9010
Method
SW-846, 9010
Method
SW-846, 9010
Method
SW-846, 7470
Method
SW-846, 7470
Method
SW-846, 7470
Method
SW-846, 7470
Method
SW-846. 7470
Method
SW-846. 6010
Method
SW-846, 6010
Method
SW-846, 6010
Method
SW-846, 6010
Lab ID: Sample ID:
14A M-636-SW;PT. OF DIS. SUR.
Test Codes and Names
CD_AE2 Cadmium
CR_AE2 Chromium
PB_AE2 Lead
AG AE2 Silver
Method
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 6010
LabID: Sample ID:
15A M-636-SW;PT. OF DIS. 15 IN.
Test Codes and Names
CD_A£2 Cadmium
CR_AE2 Chromium
PB_AE2 Lead
AG AE2 Silver
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
LabID: Sample ID:
16A M-636-SW;FIELD RINSE BLANK
Test Codes and Names
CD_AE2 Cadmium
CR_AE2 Chromium
PB_AE2 Lead
AG AE2 Silver
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
LabID: Sample ID:
17A M-636-SW;62FT. DN.GRAD.SUR
Test Codes and Names
CD_AE2 Cadmium
CR_AE2 Chromium
PB_AE2 Lead
AG A£2 Silver
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
LabID: Sample ID:
18A M-636-SW;62FT.DN.GRAD.18IN
Test Codes and Names
CD_AE2 Cadmium
CR_AE2 Chromium
PB_AE2 Lead
AG AE2 Silver
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
UbID:
19A
Sample ID:
M636SW;DUP.62FT.DN.GR. 1 SIN
Test Codes and Names
CD_AE2 Cadmium
CR_AE2 Chromium
PB_AE2 Lead
AG AE2 Silver
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Workorder Comments
Report: The matrix spike recovery for antimony in this sample set
shows a negative interference. There is currently no approved
EPA method for the digestion of antimony in a soU matrix. We
estimate that Sb must be present at 30-50 ug/g to be detected.
(/ Certified^
'/yi^^
This is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: M-606;PT. OF DIS. SURFACE LabID: 9311009-01A CoUected: 11/01/93 13:10:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Total Cyanide 0.30 mg/Kg 0.25 11/08/93 KEN SW-846, 9010
Sample ID: M-606;PT. OF DIS. 2 FT. Lab ID: 9311009-02A CoUected: 11/01/93 13:20:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Total Cyanide 0.33 mg/Kg 0.25 11/08/93 KEN SW-846, 9010
Sample ID: M-606;25 FT DN. GRAD.SUR. LabID: 9311009-03A CoUected: 11/01/93 13:25:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Total Cyanide 0.32 mg/Kg 0.25 11/08/93 KEN SW-846, 9010
)\ple ID: M-606;25 FT. DN. GRAD.2 FT Lab ID: 9311009-04A CoUected: 11/01/93 13:35:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Total Cyanide 0.35 mg/Kg 0.25 11/08/93 KEN SW-846, 9010
Sample ID: M-628;PT. OF DIS. SURFACE LabID: 9311009-05A CoUected: 11/03/93 11:02:00
TEST RESX7LT UNITS LIMIT ANALYZED BY METHOD/CAS#
Mercury U ug/Kg 10 11/24/93 CRS SW-846, 7470
Sample ID: M-628;PT. OF DIS. 2 FT. LabID: 9311009-06A CoUected: 11/03/93 11:17:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Mercury U ug/Kg 20 11/24/93 CRS SW-846, 7470
December 6, 1993 13:00 CERTIFICATE OF ANALYSIS Page 2
RESULTS BY SAMPLE
s!?ple ID: M-628;25 FT. DN. GRAD.SUR. LabID: 9311009-07A CoUected: 11/03/93 11:20:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Mercury U ug/Kg 10 11/24/93 CRS SW-846, 7470
Sample ID: M-628;25 FT. DN. GRAD.2 FT Lab ID: 9311009-08A CoUected: 11/03/93 11:34:00
TEST REStJLT UNITS LIMIT ANALYZED BY METHOD/CAS#
Mercury U ug/Kg 10 11/24/93 CRS SW-846, 7470
Sample ID: M-628;FIELD RINSE BLANK LabID: 9311009-09A CoUected: 11/03/93 11:30.00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Mercury U ug/L 0.2 12/02/93 CRS SW-846, 7470
IP pie ID: M-593;PT. OF DIS. SURFACE LabID: 9311009-lOA CoUected: 11/03/93 14:02:00
^I^T RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Antimony U ug/g 6.0 11/23/93 LVD SW-846, 6010
Sample ID: M-593;PT. OF DIS. 2 FT. Lab ID: 9311009-11A CoUected: 11/03/93 14:10:00
TEST REStJLT UNITS LIMIT ANALYZED BY METHOD/CAS#
Antimony U ug/g 5.4 11/23/93 LVD SW-846, 6010
Sample ID: M-593;37 FT. DN. GRAD.SUR. Lab ED: 9311009-12A CoUected: 11/03/93 14:13:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Antimony D ug/g 5.6 11/23/93 LVD SW-846, 6010
Sample ID: M-593;37 FT. DN. GRAD.2 FT Lab ID: 9311009-13A CoUected: 11/03/93 14:18:00
RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
XrTxmony U ug/g 6.2 11/23/93 LVD SW-846, 6010
December 6, 1993 13:00
.•
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 3
S»^ple ID: M-636-SW;PT. OF DIS. SUR. LabID: 9311009-14A CoUected: 11/04/93 12:50:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Lead
Silver
7.77
126.0
6.95
86.4
ug/g
ug/g
ug/g
ug/g
0.14 11/23/93 LVD
0.40 11/23/93 LVD
1.82 11/23/93 LVD
0.2 11/23/93 LVD
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Sample ID: M-636-SW;PT. OF DIS. 15 IN. LabID: 9311009-15A CoUected: 11/04/93 13:00:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Lead
Silver
37,
37
23,
70,
.2
.4
.2
.6
ug/g
ug/g
ug/g
ug/g
0.2
0.6
2.8
0.4
11/23/93
11/23/93
11/23/93
11/23/93
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
Sample ID: M-636-SW;FIELD RINSE BLANK LabID: 9311009-16A CoUected: 11/04/93 13:09:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Lead
Silver
11.3
9.3
U
251.8
ug/L
ug/L
ug/L
ug/L
2
5
25
3
11/23/93
11/23/93
11/23/93
11/23/93
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-84 6,
SW-846,
6010
6010
6010
6010
Sample ID: M-636-SW;62FT. DN.GRAD.SUR LabID: 9311009-17A CoUected: 11/04/93 13:22:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS«
Cadmium
Chromium
Lead
kver
183.0
360.0
6.66
159.0
ug/g
ug/g
ug/g
ug/g
0,
0,
3
0,
.2
.6
.2
.4
11/23/93
11/23/93
11/23/93
11/23/93
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
December 6, 1993 13:00 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 4
riplelD: M-636-SW;62FT.DN.GRAD.18IN LabID: 9311009-18A CoUected: 11/04/93 13:30:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmitim
Chroml\un
Lead
Silver
61.7
75.0
17.7
123.0
ug/g
ug/g
ug/g
ug/g
0.16
0.4
2.0
0.2
11/23/93
11/23/93
11/23/93
11/23/93
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
SamplelD: M636SW;DUP.62FT.DN.GR.18D^ LabID: 9311009-19A CoUected: 11/04/93 13:32:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromiiim
Lead
Silver
16.3
35.4
20.2
166.0
ug/g
ug/g
ug/g
ug/g
0.2
0.6
3.0
0.4
11/23/93
11/23/93
11/23/93
11/23/93
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection Umit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1.1J with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ENVIRONMENTAL LABWORKREQUEST —
f^ THIOKOL ENVIRONMENTAL LABORATORY LWR No. E10194^^
1 nuiMi
A.f*. WAUCE^
OSOAMZATION
S"3*?o
MAO. STOP
ooaroDfRB
^ V4CO
WORKOmOl
4 Mw*?3
aBfl«T«BU.nTOl
HELEN WARD, MS 301
SAMPLE INFORMATION
•-1 su»MkU ii4
w Pt- «P ot**x<»*y
^^
• k^
\y
SAMPLE
i.SlUUU Z74
TV OF -DMCWM^
t7"0ftOi\ft'M*"f'
DATE
3H0V43
SNDUn
SNewfl
7. SvUAfcU &W7
i-SMMU) ItoT ,- .
fcZ' 'Dptoin er«^<i 4MOU<3 _*»rCi»«
9. SiWikU 347 ftn^JwrJ-
4A<WI:J
TYPE LOCATION
-4MO0t3
^SM^^
(SniU^
,^lttiil3
a
JU-S^3
M-5*) 3
M-5'13
M-yT3
TIME
1402.
14 IO
1413
M- tat^^vO
A-^20-'Sv^
M-U3U-iu;
AA-WU-"SVO
/x-{.3t-'SiO
iv-tlCf-SW
I4i&
TEST SEMAftXS
An^hmo^vj - (gO'O
tt
ll
- a
125-D
i3oo
vze>*\
1322.
I330
133Z
CJ»Cr, Aa,?b - GolO
ll
ll
ll
i\
• i'l^. ,.i-'i.'i-5"ris j.,»
CHAIN OF CUSTODY
REUNQUISnES BY DATE TIME lECHVEDBY DATE TIME
JhLk^L. 4u^(y^:> /T/o ^^rfZL..A //-^-fi /^AO
m
FOR LABORATORY USE ONLY
DAnCOMTLEnD DAn upoRrm aciuiuit
January 7, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 1
# SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER. M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order # 9312008
LabID: Sample ID:
OlA M-636-SW;62FT. DN.GRAD.SUR
Sample and Test Code Identification
Test Codes and Names Method
CD AE2 Cadmium SW-846, 6010
CR'AE2 Chromium SW-846,6010
PB~AE2 Lead SW-846, 6010
AG" AE2 Silver SW-846, 6010
Workorder Comments
Report: THIS SAMPLE IS A RERUN FROM WORK ORDER #9311009 (17A),
LWR#E10193.
•
TTiis is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: M-636-SW;62FT. DN.GRAD.SUR Lab ID: 9312008-01A CoUected: 11/04/93 13:22:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Lead
Silver
282
422
7.93
53.5
ug/g
ug/g
ug/g
ug/g
0
0,
1,
0,
.1
.3
,6
.2
12/14/93
12/14/93
12/14/93
12/14/93
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
•
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1. IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ENVIRONMENTAL LAB WORK REQUEST ^J//^/Z-
I^TO: THIOKOL ENVIRONMENTAL LABORATORY
FROM:
ORGANIZATION
EXTOAION
MAIL STOP
LWR No. E10197
CUSTCEMmi
V40O
WORKORDQl DATE
ICM0\J^3
REPORT RESULTS TO:
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME TEST REMARKS
y
y
1/
[WUVU
n^ 9-Mti S.. a< )a.-S^(o lU^
< jx4
a- 7^'*tO \ tHaivAt- 90IO •, V\ - •^(i.Jt\»Ta.><c<i pa-sVeJ
.4ro\nr»v.T.»vta- -»Z7
9-HPv/ •5- (»? M-3-3U \\\^ \/6la+»\« 6/«avi\4S - SZ40
' 2"8o.ct!.«>'(»o«l
«^-Mov/ A •S*. of M-SSCo IIZ5"
^*\2' SatVOj-oorvi
•for ^ULf^eoA 'I?\*C4A,I
<^-MO0
K <=.. o? M-33C az5-Vok+AVc OYociwics -<S2<0
5. 'SWMkU 2e>'5'
/. M- S70 (420
CVJ ani ^fc - 90\0
.^^
H.--Z10 14Z^ ^
' 7. •SvuM.O Z'&S'.
St. iorfflx^
i<i\+
<»-Kft>> )C K-STO l4s^ C\ia.^kA< _<^oio
8. %UM.\> "Z^"^.
e*tr C^-M6U X. AX-570 1440 •i^n.
CHAIN OF CUSTODY
Rn,INQUISim)BY
si/O^.
DATE
/OklQ09^
TIME
/^ZC^
RFCETVED BY
/^//ky..,.,:.^
DATE
- // - /C fi
TIME
' </ X c
FOR LABORATORY USE ONLY
4 DATE COMPLETED DATE REPORTQ)
February 11, 1994
#
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page l
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order <i> 9311012 Sample and Test Code Identification
Lab ID: Sample ID:
OlA M-336-S;SUR.BKGND./SUR.DIS
Test Codes and Names
•
LabID:
02A
Lab ID:
03 A
Samole ID:
M-336-S;SUR.BKGND./SUR.DlS
Sample ID:
M-336-S;2FT.BKGND./SUR.DlS
LabID: Sample ID:
04A M-336-S;2FT.BKGND./SUR.DlS
LabID: Sample ID:
05A M-570; PT. OF DIS. SURFACE
LabID: Sample ID:
06A M-57b; PT. OF DIS. 2 FT.
S04IC1
SB A£2
CD AE2
CR AE2
PB AE2
MN A£Z
SE AE2
AG AE2
TL AE2
ZtfAEl
HG"CV2
8270S
CN WT2
PH_S
Sulfate
Antimony
Cadmium
Chromium
Lead
Manganese
Selenium
Silver
Thallium
Zinc
Mercury
Semi-Volatile Organics
Toul Cyanide
pH (Soil)
Test Codes and Names
8240 Volatile Organics
Test Codes and Names
S04IC1
SB AE2
CD AE2
CR AE2
PB AE2
MN AE2
SE AE2
AG AE2
TL AE2
ZI^AE2
HO CV2
8270S
CN WT2
PH_S
Sulfate
Antimony
Cadmium
Chromium
Lead
Manganese
Selenium
Silver
Thallium
Zinc
Mercury
Semi-Volatile Organics
Total Cyanide
pH (Soil)
Test Codes and Names
8240 Volatile Organics
Test Codes and Names
CN WT2
PH_S
Total Cyanide
pH (Soil)
Test Codes and Names
CN_WT2 Total Cyanide
PH_S pH (Soil)
Method
EPA 300.0
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846, 9010
SW-846, 9045
Method
SW-846, 8240
Method
EPA 300.0
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
SW-846, 9010
SW-846, 9045
Method
SW-846, 8240
Method
SW-846, 9010
SW-846, 9045
Method
SW-846, 9010
SW-846, 9045
LabID: Sample ID:
07A M-57D; 44FT. DN. GRAD.SUR.
Test Codes and Names
CN_WT2 Total Cyanide
PH_S pH (Soil)
Method
SW-846, 9010
SW-846, 9045
I^b ID: Sample ID: Test Codes and Names . Method
08A M-570; 44FT. DN. GRAD. 2FT
#
CN_WT2 Toul Cyanide SW-846, 9010
PH_S pH (Soil) SW-846, 9045
Workorder Comments
Report: Matrix interferences were found for Sb, Se, and Tl. The high
concentrations of Al and Fe created a positive interference
for Se and a negative interference for Tl. The Se results
were corrected based on the spectral interference check.
-^J^'l^^
Certified r
m
m
This is to certify that the following samples were analyzed using good laboratory practices
to show thejbllowing results.
Sample ID: M-336-S;SUR.BKGND,/SUR.DIS LabID: 9311012-OlA CoUected: 11/09/93 11:15.00
TEST
Sulfate
AntlBony
CadmiuB
Chroaiua
Lead
Manganese
Hiokel
Selealua
Silver
ThalliuD
11° iKniury
Semi-volatile Organics
Phenol
Pyridine
Aniline
bis(a-Chloroethyl)echer
2-Chlorophenol
1,3-Oiehlorobenaene
1,4-Diehlorobenaene
Bensyl Alcohol
1,2-Dichlorobenaene
2-Methylphenol
bis(2•chloroiBoprQpyl)ethe
4-Methylphenol
n-Nitroso-di-n-propylsinine
Hexachloroethane
Nitrbbeniene
isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Triohlorobensene
Naphthalene '
4-Chloroaniline
Hexachlorobutadiene
4'Chloro-3-methylphenol
ia^-.hylnaphthlene
^•1 hlorocyclopentadiene
^^, 6-Trichlorophenol
2,4,5-Trichlorophenol
RESULT
a
u
0.557
20.74
22.92
526.7
18.5
U
U
U
66.75
n
u D
u U
u n
u u
u u
u u u u tJ
u n u u u
u u u u u u
u u u u
UNITS
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
LIMIT
0.07
6.44
0.3
0.64
3.2
0.3
1.3
51.5
0.1
6.44
2.6
20
1.5
10.0
10.0
5.7
3.3
1.9
4.4
4.6
1.9
2.3
5.7
4.0
12.0
1.6
1.4
2.2
3.6
2.7
3.4
5.3
2.7
1.9
1.6
l.fi
0.9
3.0
2.2
6.0
2.7
4.0
ANALYZED
11/30/93
12/03/93
12/03/93
12/03/93
12/03/93
12/03/93
12/03/94
12/03/93
12/14/93
12/03/93
12/03/93
11/24/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
BY
CRS
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
MMR
MUR
MMR
MNR
MMR
MMR
HHR
hOSR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MKR
MMR
MMR
KETHOD/CAS#
EPA 300.0
SW-846, 6010
SW-846, 6010
SW-B46, 6010
BW-846, 6010
SW-846, 6010
SW-e46, 6010
SW-846, 6010
SW-846. 6010
Sff-B4e, 6010
SW-846, 6010
SW-e46, 7471
8W-846, 8270
108-95-2
110-86-1
£2-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-SO-l
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
Febniary 24,1994 09:52 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 2
Sample ID: M-336-S;SUR.BKOND./SUR.DIS LabID: 9311012-OlA Collected: 11/09/93 11:15:00
TEST
Sstti-Volatlla Organics
2-Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Difaensofuran
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
n-Nitrosodiphenylamine
4-Bromophenyl-phenylether
HeseachlorobenBene
Pentachlorophenol
Phenanthrene
Anthracene
M^ -butylphthalate
VH* anthene
P^ene
aucylbensylphchalate
Benso [a] anthracene
bi B(2•Bthylhexyl)phthalate
Chyrsene
Di-n-octylphthalate
Banso[b&k]fluoranthene
Benzo[a]pyrene
Indeno[l,2,3 -ed]pyrene
Dibenz ta,hj anthracene
Benzo [g,h,ilperyleiie
1,4•DichlorobenBene-d4
Naphthalene-d8
Acenaphthene-dl0
Phenanthrene-dl0
Chyrsene-dl2
Perylene-dia
SBSOLT
Int.
Int.
Int.
Int.
Int.
Int.
U
u
n
u
u
D
n
u
u
u u • u
u
u D
u u
u
a u
u u
D
u 0
n
\j
39B
U
D
U
U
U
0
U
Std.
Std.
Std.
Std.
Std.
Std.
imiTS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Xg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data :
Surrogate
2-FLUOROPHENOL
Phenol-dS
Nitrobenaene-d5
2-Fluorobiphenyl
2,4,6-Tribrcnophenol
Terphenyl'
a^/>l Cyanide
W^lSoll)
-dl4
U
7.57
mg/Kg
pH Utait
LIMIT
1.9
1.5
1.6
3.5
2.4
1.9
42.0
2.4
3.0
1.9
S.7
1.9
4.2
1.9
3.6 24.0
1.9
1.9
1.9
3.6
5.4
1.9
2.5
2.2
1.9
2.5
7.8
2.5
2.5
2.5
4.8
2.5
3.7
2.5
4.1
AKALYZED
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
BY
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR MMR
MMR
MMR
MMR
MHR
MMR MMR
MMR
lasR
MMR
MMR
MHR
MMR
MHR
MMR
MMR
MMR
MMR
MMR
MHR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MHR
METBOD/CAS#
SW-846, 8270
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
606-20-2
121-14-2
84-66-2
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
S5-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
-
.
-
.
-
-
For Seal-volatile Organics 82708
%Recovecy
64.0
64.5
52
79
89.5
107
150
Recovery Llalts
30
24
23
30
19
18
11/22/93
11/10/93
TO 115
TO 113
TO 120
TO 115
TO 122
TO 137
KEN
AA
SW-846, 9010
8W-846, 9045
February 11, 1994 13:33
#
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 3
S-uiple ID: M-336-S;SUR.BKGND./SUR.DIS LabID: 9311012-02A CoUected: 11/09/93 11:15:00
TEST RESULT
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2 -Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1 -Dichloroetheuie
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
trans -1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
^^ns -1,3 -Dichloropropene
^•l-Dichlorobenzene
^^-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Te t rachloroe thene
Toluene
1,1,1 -Trichloroe theine
1,1, 2-Trichloroethcuie
Tri chloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
Bromochloromethane
1,4-Difluorobenzene
Chlorobenzene-dS
Surrogat(
Surrogate
Toluene-d8
U
U
U
U
U
U
u u u u u u u
u u
u u
u
u u
u u
u u u u u u u u u
u u
u
u u u D
u D
u
tJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
3/Recovery Data
Bromofluorobenzene
1,2-Dichlorc jethe ine-d4
LIMIT
500
100
100
30
30
30
50
500
30
30
30
50
50
30
50
30
30
30
30
250
30
30
30
30
30
30
30
30
30
250
30
30
30
30
30
30
30
30
250
50
30
ANALYZED
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
.11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA.
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240
^Recovery
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
TO
TO
TO
Februaiy 24,1994 09:52
Sample ID: M-336-S;2FT.BKGND./SUR.DlS
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 4
LabID: 9311012-03A Collected: 11/09/93 11:25:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Sulfate
Antlaony
CadaluB
Chreaium
Lead
Manganese
Nickel
Selenlua
Silver
Thallium
Zinc
Semi-Volatile Organics
Phenol
Pyridine
Aniline
bis(2-Chloroethyl)ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Bensyl Alcohol
1,2-Dichlorobenaene
2-Methylphenol
bis(2-chloroiBOpropyl)ethe
4-Methylphenol
n • Ni troso • di - n-propyl amine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic Acid
bis (2-Chloroethosty) methane
2,4 -Dichlor^henol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2 -Methy Inaphthlene t rAilorocyclopentadiene
i-Trichlorophenol
.5-Trichlorophenol
26.5
U
0.582
38.60
18.92
569.8
29.1
U
U
U
74.40
U
U
U
U
U
U
D
U
u U
u u u u u u a u u u u u D
U
U
n D
u
n
u
u
ug/g
ug/g
ug/g
ug/g
ug/g
ug/g
ug|/g
ug/g
ug/g
ug/g
ug/g
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
0.07
6.03
0.2
0.6
3.0
0.2
1.2
7.23
0.1
6.03
2.4
20
1.5
10.0
10.0
5.7
3.3
1.9
4.4
4.6
1.9 2.3
5.7
4.0
12.0
1.6
1.4
2.2
3.6
2.7
3.4
5.3
2.7
1.9
1.6
1.8
0.9
3.0
2.2
6.0
2.7
4.0
11/30/93
12/03/93
12/03/93
12/03/93
12/03/93
12/03/93
12/03/93
12/03/93
12/14/93
12/03/93
12/03/93
11/24/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
CRS
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
LVD
CRS
MMR
MMR
MMR
MMR
MMR
MHR
MMR
MMR
MMR MMR
MMR
MMR
MMR
MHR
MHR
MHR
MMR
MMR
MMR
MMR
MMR
MHR
MHR
MMR
MMR
MMR
MHR
MMR
MHR
MHR
EPA 300.0
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 6010
8W-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 7471
SW-846, 8270
108-95-2
110-86-1
62-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
Febiuaiy 24, 1994 09:S2
Sample ID: M-336-S;2FT.6KGND./SUR.DIS
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 5
LabID: 9311012-03A Collected: 11/09/93 11:25:00
TEST
Semi-Volatile Organics
2•Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,6-Dinitrotoluene
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2'fflethylphenol
n-NitroBOdiphenylamine
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
JlH" -butylphthalate
••) uithene
?^rte
Bucylbenzylphthalate
Benzo [a] anthracene
bis (2 -Ethylheicyl) phthalate
Chyrsene
Di-n-octylphthalate
Benzo [b&lc] fluoranthene
Benzo [a] pyrene
indeno [ 1,2,3 - cd] pyrene
Dibenz[a,h]anthracene
Benao[g,h,i]perylene
1,4-Dichlorobenzene-d4
Naphthalene-da
Acenaphthene-dl0
Chyrsene-dl2
Perylene-dl2
RESULT
Int.
Int.
Int.
Int.
Int.
Int.
U
U
U
tJ
U
U
U
u tJ
D
U
U
u
n D
u
u 0
u u u u u u u u D
SOB
u D
U
u tJ
D U
Std.
Std.
Std.
Std.
Std.
Std.
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Xg
ug/Kg
ug/Xg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Xg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Xg
ug/Kg
ug/Xg
ug/Kg
ug/Kg
ug/Xg
ug/Kg
Surrogate/Recovery Data :
Surrogate
2-FU70ROPHBNOL
Phenol-dS
Nitrobenzene-dS
2 -Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl
^^1 Cyanide
™iSoil)
-di4
U
7.75
mg/Kg
pH unit
LIMIT
1.9
1.5
1.6
3.5
2.4
1.9
42.0
2.4
3.0
1.9
5.7
1.9
4.2
1.9
3.6
24.0
1.9
1.9
1.9
3.6
5.4
1.9
2.5
2.2
1.9
2,5
7.8
2.5
2.5
2.5
4.8
2.5
3.7
2.5
4.1
ANALYZED
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
11/13/93
BY
MMR
MHR
MMR
MMR
MHR
MMR
MHR
MHR
MMR
MMR
MMR
MMR
MMR
MHR
MHR
MMR
MMR
MMR
MMR
MHR
MMR
MHR
MMR
MMR MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
MMR
UHR
MMR
MMR
MHR MMR
MBTBOD/CAS«
SW-846, 8270
91-58-7
88-74-4
131-11-3
208-96-8
99-09-2
83-32-9
51-28-5
100-02-7
132-64-9
S06-20-2
121-14-2
84-66-a
7005-72-3
86-73-7
100-01-06
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
129-00-0
85-68-7
56-55-3
117-81-7
218-01-9
117-84-0
205-99-2/2
50-32-8
193-39-5
53-70-3
191-24-2
For Semi-volatile Organics 82708
48
52.0
41
60
82.5
91
150
Recovery Limits
30
24
23
30
19
18
11/22/93
11/10/93
TO 115
TO 113
TO 120
TO 115
TO 122
TO 137
KSH
AA
8W-846, 9010
8W-846, 9045
Febmary 11, 1994 13:33 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 6
Sample ID: M-336-S;2FT.BKGND./SUR.DIS LabID: 9311012-04A CoUected: 11/09/93 11:25:00
TEST RESULT
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethzme
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1,2-Diehloroetheme
1,1-Dichloroethene
2-HexcLnone
trans-1,2-Dichloroethene
1,2 -Dichloropropcuie
cis-1,3-Dichloropropene
^^ips-1,3 -Dichloropropene
f^H -Dichlorobenzene
J., 3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,l-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Tri chlorofluorome thane
vinyl Acetate
Vinyl Chloride
o-Xylene
B r omochl or ome thcuie
1,4-Difluorobenzene
Chlorobenzene-dS
Surrogatf
Surrogate
Toluene-d8
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
a 0
n
u
u
u
u
u
u
u
u
u
a
u
u
u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
2/Recovery Data
Bromofluorobenzene
1,2-Dichlorc jethe me-d4
LIMIT
500
100
100
30
30
30
50
500
30
30
30
50
50
30
50
30
30
30
30
250
30
30
30
30
30
30
30
30
30
250
30
30
30
30
30
30
30
30
250
50
30
ANALYZED
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
.11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
11/19/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 6240
%Recovery
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
INTSTDl
INTSTD2
INTSTD3
Recovery Limits
TO
TO
TO
m
Febniary 11, 1994 13:33
m
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 7
Scunple ID: M-570; PT. OF DIS. SURFACE Lab ID: 9311012-05A CoUected: 11/09/93 14:20:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Total Cyanide
pH (Soil)
U mg/Kg
7.76 pH Unit
150 11/22/93 KEN
11/10/93 AA
SW-846, 9010
SW-846, 9045
Sample ID: M-570; PT. OF DIS. 2 FT.
TEST RESULT
LabID:
UNITS
9311012-06A CoUected: 11/09/93 14:25:00
LIMIT ANALYZED BY METHOD/CAS#
Total C:yanide
pH (Soil)
U mg/Kg
7.23 pH Unit
150 11/22/93 KEN
11/10/93 AA
SW-846, 9010
SW-846, 9045
Sample ID: M-570; 44FT. DN. GRAD.SUR. Lab ID: 9311012-07A CoUected: 11/09/93 14:35:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
§' al Cyanide
(Soil)
178
7.61
mg/Kg
pH Unit
150 11/22/93
11/10/93
KEN
AA
SW-846,
SW-846,
9010
9045
Sample ID: M-570; 44FT. DN. GRAD. 2FT LabID: 9311012-08A CoUected: 11/09/93 14:40:00
TEST RESULT UNITS LIMIT ANALYZED BY METEOD/CAS#
Total Cyanide
pH (Soil)
u
7.70
mg/Kg
pH Unit
150 11/22/93
11/10/93
KEN
AA
SW-846,
SW-846,
9010
9045
•
•
•
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1. IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the linear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spUce recovery was outside of the specified limits.
ENVIRONMENTAL LAB WORK REQUEST
4 THIOKOL ENVIRONMENTAL LABORATORY LWR No. E103S3
nOM:
A, P. WALceR^
ORGANIZATION
53*^0
"^o\e
MAOO lSi4D
DATC
l7Mb\; '^Z>
.nroi
HELEN WARD, MS 301
SAMPLE INFORMATION
y
iy
SAMPLE
2. SV»MM A9S
DATE TYPE LOCATION
M-\<^1
AX-1^1
11ME nsT
IMO C^)Cr, A^>Pb - (oOlO
I OSO CiijCr, A-^.TVi - feo'O
ZEMASKS
t^ A-I'^l IDSS" ca,Cr, A^, Pb - fpoio
4. Su>uu 4e3 . .
JU-i<il IIOO CA,Cr, Aa, Tb - i^oio
iy I7A(0V«3 Ail-iST-'B^ ins-
*
«.9\t<u.u Sbo
Voia4\\c Cr«»a»».iti -ex40
M-nT-BP /II7
M-l<^7-B? (112. Vela4ilc 6m«n»t&-et40
i. 3\»*u>v* %it,o •
t sJrZ:^^ /7UOU12 JU-/97- BF H2S-
I Z t7UCUf3 AA'/97- &F /IBS
H'TOZ /3/-f e^4*»*^ - ^f>^P.
'-pi-- S!»^ra.ieA %gfe
u t^'tOl. ttz^ -^
/U'loZ. I3SO CuMiAe. - 9cto
AIN OF CUSTODY
SEUNQUISBiSBY DATE TIME KBCEZVEDBV DATE TIME
{LMJa/L^ //of/n,n /^oS' 4±i^ ^-^/-/y-fJ /^^.
7
FOR LABORATORY USE ONLY
#
1 DATCCOMFIXTB) nAnsBPOirra) SMIUIVM
December 21, 1993 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 1
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs M/S 245
Attn: Dr. John Terry
Tele: 801-863-2384
Work Order # 9311022 Sample and Test Code Identification
LabID:
OlA
Sample ID:
M-197;PT. OF DIS. SURFACE
Test Codes and Names
LabID: Sample ID:
02A M-197;PT. OF DIS. 2FT.
LabID: Sample ID:
03A M-197;25FT. DN. GRAD. SUR.
LabID: Sample ID:
04A M-197;25Fr. DN. GRAD. 2FT.
LabID: Sample ID:
05A M-197-BP;PT. OF DIS. SUR.
LabID: Sample ID:
06A M-197-BP;PT. OF DIS. DUP.
LabID: Sample ID:
07A M-197-BP;PT. OF DIS. 2FT.
LabID: Sample ID:
08A M-197-BP;25FT. DN.GRAD.SUR
LabID: Sample ID:
09A M-197-BP;25FT. DN.GRAD.2FT
CD AE2
CR AE2
PB AE2
AG_AE2
Cadmium
Chromium
Lead
Silver
Test Codes and Names
CD AE2
CR AE2
PB AE2
AG_AE2
Cadmium
Chromium
Lead
Silver
Test Codes and Names
CD AE2
CR AE2
PB AE2
AG_AE2
Cadmium
Chromium
Lead
Silver
Test Codes and Names
CD AE2
CR AE2
PB AE2
AG_AE2
Cadmium
Chromium
Lead
Silver
Test Codes and Names
8240
PH_S
Volatile Organics
pH (Soil)
Test Codes and Names
8240
PH_S
Volatile Organics
pH (Soil)
Test Codes and Names
8240
PH_S
Volatile Organics
pH (Soil)
Test Codes and Names
8240
PH_S
Volatile Organics
pH (Soil)
Test Codes and Names
8240
PH S
Volatile Organics
pH (Soil)
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 8240
SW-846, 9045
Method
SW-846, 8240
SW-846, 9045
Method
SW-846, 8240
SW-846, 9045
Method
SW-846, 8240
SW-846, 9045
Method
SW-846, 8240
SW-846, 9045
LabID: Sample ID:
IOA M-702; PT. OF DIS. SURFACE
Test Codes and Names
CN_WT2 Total Cyanide
PH_S pH (Soil)
Method
SW.846, 9010
SW-846, 9045
Sample ID:
M-702; PT. OF DIS. 2 FT.
Test Codes and Names
CN_WT2 Toul Cyanide
PH_S pH (Soil)
Method
SW-846, 9010
SW-846, 9045
LabID:
12A
Sample ID:
M-702; 25FT. DN. GRAD. SUR
Test Codes and Names
CN_WT2 Toul Cyanide
PH_S pH (Soil)
Method
SW-846, 9010
SW-846, 9045
LabID: Sample ID:
13A M-702; 25FT. DN. GRAD. 2FT
Test Codes and Names
CN_WT2 Toul Cyanide
PH_S pH (Soil)
Method
SW-846, 9010
SW-846, 9045
Workorder Cnrnments
Certifie^:^
This is to certify that the following samples were aruilyzed using good laboratory practices
to show the following results.
•
Sample ID: M-197;PT. OF DIS. SURFACE LabID: 9311022-OlA CoUected: 11/17/93 10:40:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Lead
Silver
0.382
12.49
15.44
73.82
ug/g
ug/g
ug/g
ug/g
0.2
0.39
2.0
0.08
12/03/93
12/03/93
12/03/93
12/14/93
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
Sample ID: M-197;PT. OF DIS. 2FT. LabID: 9311022-02A CoUected: 11/17/93 10:50:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Lead
Silver
D
13.59
8.492
13.16
ug/g
ug/g
ug/g
ug/g
0.2
0.39
2.0
0.08
12/03/93
12/03/93
12/03/93
12/14/93
LVD
LVD
LVD
LVD
SW-846,
SW-84 6,
SW-846,
SW-846,
6010
6010
6010
6010
Sample ID: M-I97;25FT. DN. GRAD. SUR. LabID: 9311022-03A CoUected: 11/17/93 10:55:00
TEST RESITLT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadfflixim
chromium
Lead
Silver
2.60
10.43
5.534
21.75
ug/g
ug/g
ug/g
ug/g
0.1
0.28
1.4
0.06
12/03/93
12/03/93
12/03/93
12/14/93
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
Sample ID: M-197;25FT. DN. GRAD. 2FT. LabID: 9311022-04A CoUected: 11/17/93 11:00:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Lead
I ver
u
19.88
9.526
U
ug/g
ug/g
ug/g
ug/g
0.2
0.56
2.8
0.1
12/03/93
12/03/93
12/03/93
12/14/93
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
December 21, 1993 13:55 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 2
# S3iple ID: M-197-BP;PT. OF DIS. SUR. LabID: 9311022-05A CoUected: 11/17/93 11:15:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethcuie
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
D ibromochlorome thane
1,1-Dichloroe thane
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
Trans 1,2-Dichloroethene
1,2-Dichloropropane
Cis 1,3-Dichloropropene
a^is 1,3-Dichloropropene
^^B- Dichlorobenzene
^^-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4 -Methyl - 2 - Penteuione
2 -Propanol (IPA)
Styrene
1,1,2,2 -Tetrachloroetheuie
Tetrachloroethene
Toluene
1,1,l-Trichloroethane
1,1,2-Trichloroethame
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
Chlorobenzene-d5
1,4-Difluorobenzene
1,4-Di chlorobenzene-d4
Pentafluorobenzene
REStJLT
Int.
Int.
Int.
Int.
U
U
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u u
u D
U
U
U
U
u u
u
u
u
u
u
u
u
u Std.
Std.
Std.
std.
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Surrogate/Recovery Data
Surrogati 3
Dibromofluoromethane
Toluene-d8
4-Bromofluorobenzene
^HSoil) 7.8 pH Unit
LIMIT
500
100
100
30
30
30
50
500
30
30
30
50
50
30
50
30
30
30
30
250
30
30
30
30
30
30
30
30
30
250
2500
30
30
30
30
30
30
30
30
250
50
30
ANALYZED
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240
%Recovery
101
99.2
103
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
-
540-36-3
-
363-72-4
Recovery Limits
75
75
75
11/18/93
TO 125
TO 125
TO 125
AA SW-846, 9045
December 21, 1993 13:55 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 3
'5!^ple ID: M-197-BP;PT. OF DIS. DUP. LabID: 9311022-06A CoUected: 11/17/93 11:17:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromome theine
2-Butanone
1 Carbon disulfide
\Carbon tetrachloride Chlorobenzene
Chloroethane
2 -Chloroethylvinyl ether
Chloroform
Chloromethame
Dibromochloromethane
1,l-Dichloroetheme
1,2-Dichloroethane
1,1-Dichloroethene
2 -Hexanone
Trans 1,2-Dichloroethene
1,2-Dichloropropane
Cis 1,3-Dichloropropene
^Kans 1,3-Dichloropropene
^^V. -Dichlorobenzene
^^J -Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
2-Propanol (IPA)
Styrene
1,1,2,2-Tetrachloroethame
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethame
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
Chlorobenzene- d5
1,4-Difluorobenzene
1,4-Di chlorobenzene-d4
Pentafluorobenzene
RESULT
Int.
Int.
Int.
Int.
102J
U
U
U
o U
U
U
U
U
U
U
U
u
u u u 0
u u u u
u
u u u u u u
u
u u
u u u V
u u
u u u D
Std.
std.
std.
std.
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Surrogate/Recovery Data
Surrogate
D ibromofluorometheme
Toluene-d8
4-Bromofluorobenzene
^^ (Soil) 8.0 pH Unit
LIMIT
500
100
100
30
30
30
50
500
30
30
30
50
50
30
50
30
30
30
30
250
30
30
30
30
30
30
30
30
30
250
2500
30
30
30
30
30
30
30
30
250
50
30
ANALYZED
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240
%Recovery
99.4
99.8
103
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
-
540-36-3
-
363-72-4
Recovery Limits
75
75
75
11/18/93
TO 125
TO 125
TO 125
AA SW-846, 9045
December 21, 1993 13:55 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 4
SSliple ID: M-197-BP;PT. OF DIS. 2FT. LabID: 9311022-07A CoUected: 11/17/93 11:22:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Volatile organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethame
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethauie
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethame
1,2-Dichloroethame
1,1-Dichloroethene
2 - Hexamone
Trans 1,2-Dichloroethene
1,2-Dichloropropame
Cis 1,3-Dichloropropene
^•|ns 1, 3 -Dichloropropene
••-Dichlorobenzene
^^-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentamone
2-Propanol (IPA)
Styrene
1,1,2,2-Tetrachloroethame
Tetrachloroethene
Toluene
1,1,l-Trichloroethane
1,1,2-Trichloroethame
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
Chlorobenzene-d5
1,4-Difluorobenzene
1,4 -Di chlorobenzene-d4
Pentafluorobenzene
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u u
D
U
U
U
U
U
U
u
u
u
u
u u
D
U
u
u
u u
u
u
Int.
Int.
Int.
Int.
Std.
Std.
Std.
Std.
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
500
100
100
30
30
30
50
500
30
30
30
50
50
30
50
30
30
30
30
250
30
30
30
30
30
30
30
30
30
250
2500
30
30
30
30
30
30
30
30
250
50
30
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
-
540-36-3
-
363-72-4
Surrogate/Recovery Data For Volatile Organica 8240
Surrogate
Dibromofluoromethame
Toluene-d8
4-Bromofluorobenzene
^Recovery
101
101
104
Recovery Limits
75 TO 125
75 TO 125
75 TO 125
(Soil) 7.7 pH Unit 11/18/93 AA SW-846, 9045
December 21, 1993 13:55 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 5
SZhple ID: M-197-BP;25FT. DN.GRAD.SUR LabID: 9311022-08A CoUected: 11/17/93 11:25.00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethame
Bromoform
Bromomethame
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2 - Hexamone
Trans 1,2-Dichloroethene
1,2-Dichloropropame
Cis 1,3-Dichloropropene
^•|ns 1, 3 -Dichloropropene
^^P-Dichlorobenzene
^^ -Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
2-Propanol (IPA)
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,l-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorof1uoromethame
Vinyl Acetate
Vinyl Chloride
o-Xylene
Chlorobenzene-d5
1,4-Difluorobenzene
1,4-Dichlorobenzene-d4
Pentafluorobenzene
REStJLT
Int.
Int.
Int.
Int.
lOOJ
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u u
D
u
u
u
u
u
std.
Std.
Std.
Std.
tJNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Surrogate/Recovery Data
Surrogate
Dibromofluoromethane
Toluene-d8
4-Bromofluorobenzene
^B(Soil) 7.6 pH Unit
LIMIT
500
100
100
30
30
30
50
500
30
30
30
50
50
30
50
30
30
30
30
250
30
30
30
30
30
30
30
30
30
250
2500
30
30
30
30
30
30
30
30
250
50
30
ANALYZED
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240
%Recovery
106
99.7
104
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
-
540-36-3
-
363-72-4
Recovery Limits
75
75
75
11/18/93
TO 125
TO 125
TO 125
AA SW-846, 9045
December 21, 1993 13:55 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 6
• Kiple ID: M-197-BP;25FT. DN.GRAD.2FT LabID: 9311022-09A CoUected: 11/17/93 11:33:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethame
Bromoform
Bromomethame
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethame
Dibromochloromethame
1,1-Dichloroethane
1,2-Dichloroethame
1,1-Dichloroethene
2 -Hexanone
Trams 1,2-Dichloroethene
1,2-Dichloropropame
Cis 1,3-Dichloropropene
flKams 1,3-Dichloropropene
^B' -Dichlorobenzene
^^j -Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4 -Methyl-2 -Pentanone
2-Propanol (IPA)
Styrene
1,1,2,2-Tetrachloroethame
Tetrachloroethene
Toluene
1,1,1-Trichloroethame
1,1,2-Trichloroethane
Tri chloroe thene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
Chlorobenzene-d5
1,4-Difluorobenzene
1,4-Dichlorobenzene-d4
Pentafluorobenzene
REStJLT
Int.
Int.
Int.
Int.
U
U
U
U
U
U
U
U
U
U
U
U
u
u
u
u
u
u u
u
u
u
u u u u
u
u u u
u u
u u u
u u u
u u u
a std.
std.
std.
std.
tJNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Surrogate/Recovery Data
Surrogate
Dibromofluoromethane
Toluene-d8
4-Bromofluorobenzene
ft (Soil) 7.7 pH Unit
LIMIT
500
100
100
30
30
30
50
500
30
30
30
50
50
30
50
30
30
30
30
250
30
30
30
30
30
30
30
30
30
250
2500
30
30
30
30
30
30
30
30
250
50
30
ANALYZED
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
12/02/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240
%Recovery
103
100
103
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
-
540-36-3
-
363-72-4
Recovery Limits
75
75
75
11/18/93
TO 125
TO 125
TO 125
AA SW-846, 9045
December 21, 1993 13:55 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 7
• S!^ple ID: M-702; PT. OF DIS. SURFACE LabID: 9311022-lOA CoUected: 11/17/93 13:14:00
TEST REStJLT UNITS LIMIT ANALYZED BY METHOD/CAS#
Total Cyanide
pH (Soil)
U mg/Kg
7.7 pH Unit
150 11/22/93 KEN
11/18/93 AA
SW-846, 9010
SW-846, 9045
Sample ID: M-702; PT. OF DIS. 2 FT. LabID: 9311022-llA CoUected: 11/17/93 13:25:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Total Cyanide
pH (Soil)
U mg/Kg
8.2 pH Unit
150 11/22/93 KEN
11/18/93 AA
SW-846, 9010
SW-846, 9045
Sample ID: M-702; 25FT. DN. GRAD. SUR Lab ID: 9311022-12A CoUected: 11/17/93 13:30:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Total Cyanide
'(Soil)
175 mg/Kg
7.8 pH Unit
150 11/22/93 KEN SW-846, 9010
11/18/93 AA SW-846, 9045
Sample ID: M-702; 25FT. DN. GRAD. 2FT Lab ID: 9311022-13A CoUected: 11/17/93 13:33:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Total Cyanide
pH (Soil)
U mg/Kg
7.7 pH Unit
150 11/22/93 KEN
11/18/93 AA
SW-846, 9010
SW-846, 9045
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. I.IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the Unear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spike recovery was outside of the specified limits.
ENVIRONMENTAL LAB WORK REQUEST VAQ^ /
•°' XmOKOL ENVIRONMENTAL LABORATORY
niOM:
1 ORGANIXAIION
1 ENV/JZo EJf<B/Z.
BCnSNSION
S390
3o/£
LWR No. E10354
OOfTONra*
I/40O
WORKOUm
IB940
DATS
•VOBT kBULII TOI
HELEN WARD, MS 301
SAMPLE INFORMATION
SAMPLE DATE TYPE LOCATION TIME nsT REMARKS
1/ *v7^72.
.T-StUMO .Z^7
/B*JV0f3 A-f /22S' ^/Cr,Aj,Pk -(^to
/Bmi3 A-f IZ30 "''1'^.'^^^::^%.^
tlmJ^'-stf
, 1. SlO»U> ZU 7
1/ P^ pf Di%tU>y.
/dM»*9i All. /24I tf
pit - 5»<«nt/fa/af/4. iSttoffg A'Z Ii07
y' tSAtCiff)
l4U»*9y
A-i^ (-507 l^o/a^/e ^rao/tKS - SZ40
A'T. /SK" ^' ^r, A^, ^I'^f^TJ^^'lr
y •Ft ^'f^pisdi»ff{0ifiJ9z A'T-13/C^ l/a/a'^/e ^Kfa/t/cS -3Z4^
m 25-afrnJiiJ^, iff/Off-:' y A-'Z-J3ZO Cd, Ct. Am, ^Phj M^ " e^oio
• '
ar^Jttn*
ten»ofy
G^^.. le^t ^
A-Z. fSzo \r9lahl€ Oraa/tfcs ^0X4^
/f-2-
^
l330 ''• ^;'/t-^<^l^^.^
JL:
Cr^^.. teuoof, ^ A'-i^ i330 \/ch/i/v ^yg/y/^ '^rfp
y if* ZiB' Vovf fA'c*<l
teufts A-1 /^4f ^J, Cr, A^) Pb. -Go/o
CHAIN OF CUSTODY
REZJNQLISUED BY
>0/^. ^^
^
DATE
//'/f-^-S
TIME
///r s'"
RECEIVED BY
//JE/E^.....^
DATE
^X/-/^' ^7
TIME
//^^
FOR LABORATORY USE ONLY
4 DATE COMPLns) DAlSUrORTED MCNAIVU
/
ENVIRONMENTAL LAB WORK REQUEST
'PAGE- Z—
4
^^//P>S
TraOKOL ENVIRONMENTAL LABORATORY LWR No. E10354 -CbAi%uc<^
A,f' (JUALKE/K
o•CA^a^A^ON
Mil
HELEN WARD, MS 301
1./
y
y
y
\y
i/
n II
SAMPLE
:-SitMi.O*.4U,SU
T>ea»M U)MeR.
. 6.
PeCOM (UATBB.
7.
i. 1 w-
lOL
11.
12.
DATE
mmiftt
teuoofi
leumiz
3
/BU)0i3
IftiSeo^
I^MOOO
SAMPLE INFORMATION
TVPE
6
<
K
K
JC
<
K
c
^
LOCATION
/4-2 Ccm/t/nUfko.
A-ZM'ttmlr/pu
A-Z (UM4icm
firZ (U/ti^Fh*
Ail-Ids'
K-70T
^[^ 'T<'+
\^ ^
TIME
/35-/
/557
l4o^
14*6
n 1 xX. ^
•nn KEMASXS
C4,Cr, Ac, Pb,Mn -(sO/o 11
fo/a^f^ d^A/cs 'S!f»
^is '''A.^rJ/'iA
f^<?>&>f/c Arsenica '6140
AXc-Wl-b - (i,o\o /^
\/«lrtrk OfttCHlilS -eZ40
0
.«zo^^^
\„,--'
CHAIN OF CUSTODY
^
RfUNQUISBH) BY
L—^/-^o ''^E
DATE
//'/9-9:3
TIME
//'^^
BBCQVEDBY
^Ef^. r-fr^/y*
DATE
-y/^y^-^^
TIME
// ^sr-
FOR LABORATORY USE ONLY
4 DATECOMnflCD DAIB RETORTED aCHATOB
January 4, 1994 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 1
SENT Environmental Monitoring
TO: Helen Ward
M/S 301
A.F. WALKER, M/S 301E
Ext 5390
ANALYZED
BY:
Thiokol Corporation
Science & Engineering
P.O. Box 707
Brigham Gty, Ut 84302-0707
Analytical Labs M/S 245
Atm: Dr. John Terry
Tele: 801-863-2384
Work Order # 9311023 Sample and Test Code Identification
LabID: Sample ID:
OlA A-9; PT. OF DIS. SURFACE
Test Codes and Names
LabID: Sample ID:
02A A-9; PT. OF DIS. 2 FT.
LabID:
03 A
LabID:
04A
Sample ID:
A-9; 318 FT. DN. GRAD. SUR
Sample ID:
A-2; PT. OF DIS. SURFACE
CD AE2
CR A£2
PB AE2
AG AE2
PH_S
Cadmium
Chromium
Uad
Silver
pH (Soil)
Test Codes and Names
CD AE2
CR AE2
PB AE2
AG AE2
PH_S
Cadmium
Chromium
Lead
Silver
pH (Soil)
Test Codes and Names
CD AE2
CR AE2
PB AE2
AG AE2
PH_S
Cadmium
Chromium
Lead
Silver
pH (Soil)
Test Codes and Names
CD_AE2
CR_AE2
PB_AE2
MN_AE2
AG_AE2
PH S
Cadmium
Chromium
Lead
Manganese
Silver
pH (Soil)
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 9045
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 9045
Method
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 9045
Method
SW-846, 6010
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 9045
Lab ID: Sample ID:
05A A-2; PT. OF DIS. SURFACE
Test Codes and Names
8240 Volatile Organics
Method
SW-846, 8240
LabID:
06A
LabID:
07A
LabID:
08A
Sample ID:
A-2; PT. OF DIS. 2 FT.
Test Codes and Names
Sample ID:
A-2; PT. OF DIS. 2 FT.
Sample ID:
A-2;25FT. DN. GRAD. SUR.
CD
CR
PB
AE2
A£2
AE2
MlT AE2
AG
PH_
8241
CD
CR
PB
MN
AG
AE2
S
I
3
I
AE2
AE2
AE2
AE2
AE2
Cadmium
Chromium
Lead
Manganese
Silver
pH (Soil)
est Codes and Names
Volatile Organics
est Codes and Names
Cadmium
Chromium
Lead
Manganese
Silver
Method
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846, 9045
6010
6010
6010
6010
6010
Method
SW-846, 8240
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
LabID: Sample ID:
08A A-2; 25FT. DN. GRAD. SUR.
Sample ID:
A-2; 25FT. DN. GRAD. SUR.
Test Codes and Names
PH_S pH (Soil)
8240
Test Codes and Names
Volatile Organics
Method
SW-846, 9045
Method
SW-846, 8240
LabID: Sample ID:
10A A-2; 25FT. DN. GRAD. 2 FT.
Test Codes and Names
CD_A£2 Cadmium
CR_AE2 Chromium
PB_AE2 Lead
MN_AE2 Manganese
AG_AE2 Silver
PH_S pH (Soil)
Method
SW-846. 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 9045
LabID: Sample ID:
llA A-2; 25FT. DN. GRAD. 2FT.
8240
Test Codes and Names
Volatile Organics
Method
SW-846, 8240
LabID:
12A
UbID:
13A
Sample ID:
A-9; 3l8Fr. DN. GRAD. 2FT.
Test Codes and Names
Sample ID:
A-2 COMB.;PT. OF DIS.SUR.
CD
CR
PB
AG
PH.
CD
CR
AE2
AE2
AE2
AE2
S
I
AE2
AE2
PB A£2
MN
AO
AE2
AE2
Cadmium
Chromium
Lead
Silver
pH (Soil)
est Codes and Names
Cadmium
Chromium
Lead
Manganese
Silver
PH S pH (Soil)
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 9045
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 9045
Lab ID: Sample ID:
14A A-2 C0MB.;PT. OF DIS. SUR.
Test Codes and Names
8240 Volatile Organics
Method
SW-846, 8240
LabID: Sample ID:
15A A-2 C0MB.;PT. OF DIS. 2FT.
Test Codes and Names
CD_AE2 Cadmium
CR AE2 Chromium
PBJAE2 Lead
MN A£2 Manganese
AG ~AE2 Silver
PHJS pH (Soil)
Method
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846. 6010
SW-846, 9045
LabID:
16A
Sample ID:
A-2 COMB.:PT. OF DIS. 2FT.
Test Codes and Names
8240 Volatile Organics
Method
SW-846, 8240
LabID: Sample ID:
TTA M-705; DECON WATER, GRAB
Test Codes and Names
LabID: Sample ID:
ISA M-705; DECON WATER
PH
CD AE2
CR AE2
PB AE2
MN AE2
NI AE2
AG AE2
ZN_AE2
pH
Cadmium
Chromium
Lead
Manganese
Nickel
Silver
Zinc
Test Codes and Names
8240 Volatile Organics
Method
EPA 150.1
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
Method
SW-846, 8240
Workorder Comments
Workorder: Duplicate analysis ofthe sample labeled A-2; 25 ft. Dn. Grad.
Sur. indicated a homogeneity problem greater than the norm for
the sUver and lead analysis. The matrix spUces did not
exhibit the same problem. The greater of the dupUcate
results are reported here.
%r^E.^ ^O"'*^
(/ Certifiec^*^
^
This is to certify that the following samples were analyzed using good laboratory practices
to show the following results.
Sample ID: A-9; PT. OF DIS. SURFACE LabID: 9311023-OlA CoUected: 11/18/93 12:25:00
TEST REStJLT tJNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Lead
Silver
pH (Soil)
0.22
12
11
U
10.1
ug/g
ug/g
ug/g
ug/g
pH Unit
0.2
0.57
2.9
0.1
12/03/93
12/03/93
12/03/93
12/03/93
11/19/93
LVD
LVD
LVD
LVD
JWJ
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
9045
Sample ID: A-9; PT. OF DIS. 2 FT. LabID: 9311023-02A CoUected: 11/18/93 12:30:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Lead
pH (Soil)
0.496
13.82
9.376
U
8.8
ug/g
ug/g
ug/g
ug/g
pH Unit
0.2
0.38
1.9
0.08
12/03/93
12/03/93
12/03/93
12/03/93
11/19/93
LVD
LVD
LVD
LVD
JWJ
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
9045
Sample ED: A-9; 318 FT. DN. GRAD. SUR Lab ID: 9311023-03A CoUected: 11/18/93 12:41:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Lead
Silver
pH (Soil)
0
7
3
.163
.439
.866
U
9.5
ug/g
ug/g
ug/g
ug/g
pH Unit
0.1
0.27
1.4
0.05
12/03/93
12/03/93
12/03/93
12/03/93
11/19/93
LVD
LVD
LVD
LVD
JWJ
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
9045
Sample ID: A-2; PT. OF DIS. SURFACE LabID: 9311023-04A CoUected: 11/18/93 13:07:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
^^vnium 1.368 ug/g 0.2 12/03/93 LVD SW-846, 6010
^
January 4, 1994 08:15 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 2
•
L^^ple ID: A-2; PT. OF DIS. SURFACE LabID: 9311023-04A CoUected: 11/18/93 13:07:00
TEST RESULT tJNITS LIMIT ANALYZED BY METHOD/CAS#
Chromiiun
Lead
Manganese
Silver
pH (Soil)
15.78 ug/g
32.65 ug/g
249.2 ug/g
13.64 ug/g
8.3 pH Unit
0.61 12/03/93 LVD
3.0 12/03/93 LVD
0.2 12/03/93 LVD
0.1 12/03/93 LVD
11/19/93 JWJ
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-846, 6010
SW-a46, 9045
Sample ID: A-2; PT. OF DIS. SURFACE LabID: 9311023-05A CoUected: 11/18/93 13:07:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
^^Hpmof orm
^|P mome thane
.. dutcmone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1 -Dichloroetheine
1,2-Dichloroe theine
1,1-Dichloroethene
2 -Hexanone
Trans 1,2-Dichloroethene
1,2-Dichloropropane
Cis 1,3-Dichloropropene
Trans 1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl- 2 -Pentanone
2-Propanol (IPA)
Styrene
1,1,2, 2 -Tetrachloroetheuie
Tetrachloroethene
Toluene
^^^1,1 -Trichloroetheme
'^Bj' ,2-Trichloroethane
^^ chloroethene
•ixichlorof luoromethane
RESULT
U
U
U
u u u
u u u u u u
u u u
u o u u u u u
u u
u u u
u u u u
u
u u u u
u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
LIMIT
500
100
100
30
30
30
50
500
30
30
30
50
50
30
50
30
30
30
30
250
30
30
30
30
30
30
30
30
30
250
2500
30
30
30
30
30
30
30
30
ANALYZED
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JldA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
January 4, 1994 08:15
sISpIe ID: A-2; PT. OF DIS. SURFACE
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 3
LabID: 9311023-05A CoUected: 11/18/93 13:07:00
TEST
Volatile Organica
Vinyl Acetate
Vinyl Chloride
o-Xylene
Chlorobenzene-d5
1,4-Difluorobenzene
1,4-Dichlorobenzene•
Pentafluorobenzene
REStJLT
U
u
u
Int. Std.
Int. Std.
•d4 Int. Std.
Int. Std.
Surrogate/Re
Surrogate
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
icovery Data
Dibromofluoromethane
Toluene - d8
4-Bromofluorobenzene
LIMIT
250
50
30
ANALYZED
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240
%Recovery
99.4
98.6
111
METHOD/CAS#
SW-846, 8240
108-05-4
75-01-4
95-47-6
-
540-36-3
-
363-72-4
Recovery Limits
75
75
75
TO 125
TO 125
TO 125
Sample ID: A-2; PT. OF DIS. 2 FT. LabID: 9311023-06A CoUected: 11/18/93 13:16:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Oa^ium
C??omium
Lead
Manganese
Silver
pH (Soil)
0.410
19.01
18.03
339.6
6.064
8.3
ug/g
ug/g
ug/g
ug/g
ug/g
pH Unit
0.2
0.58
2.9
0.2
0.1
12/03/93
12/03/93
12/03/93
12/03/93
12/03/93
11/19/93
LVD
LVD
LVD
LVD
LVD
JWJ
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
9045
Sample ID: A-2; PT. OF DIS. 2 FT.
TEST RESULT
LabID:
UNITS
9311023-07A CoUected: 11/18/93 13:16:00
LIMIT ANALYZED BY METHOD/CAS#
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
B romome thane
2-Butanone
Carbon disulfide
^A)on tetrachloride
IJ^^robenzene
j^^-roe thane
u
u
u
u
u
u
u
u
u
u
u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
200
40
40
10
10
10
20
200
10
10
10
20
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
January 4, 1994 08:15
S^ple ID: A-2; PT. OF DIS. 2 FT.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 4
LabID: 9311023-07A CoUected: 11/18/93 13:16:00
TEST
Volatile Organics
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochlorome thcuie
1,1-Dichloroetheine
1,2 -Dichloroetheuie
1,1-Dichloroethene
2-Hexanone
Trams 1,2-Dichloroethene
1,2-Dichloropropane
Cis 1,3-Dichloropropene
Trans 1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl- 2 -Pentanone
2-Propanol (IPA)
Styrene
1,1,2,2-Tetrachloroethane
Tet rachloroe thene
Toluene
^tal, 1-Trichloroethane
1B, 2 -Trichloroethane
^•^chloroethene
Tri chlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
Chlorobenzene-d5
1,4-Difluorobenzene
1,4-Dichlorobenzene-d4
Pentafluorobenzene
REStJLT
Int.
Int.
Int.
Int.
U
U
U
U
u u u u u u
u u
u u u u
u
u u u
u u u
u u u 0
u u u std.
std.
std.
std.
tJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogate
Dibromofluoromethane
Toluene-d8
4-Bromofluorobenzene
LIMIT
20
10
20
10
10
10
10
100
10
10
10
10
10
10
10
10
10
100
1000
10
10
10
10
10
10
10
10
100
20
10
ANALYZED
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240
%Recovery
96.9
98.8
105
METHOD/CAS#
SW-846, 8240
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
-
540-36-3
-
363-72-4
Recovery Limits
75
75
75
TO 125
TO 125
TO 125
Sample ID: A-2; 25FT. DN. GRAD. SUR. LabID: 9311023-08A CoUected: 11/18/93 13:20:00
TEST RESTJLT tJNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
#
0.866
15.69
25.33
ug/g
ug/g
ug/g
0.3 12/03/93 LVD SW-846, 6010
0.63 12/03/93 LVD SW-846, 6010
3.2 12/03/93 LVD SW-846, 6010
January 4, 1994 08:15 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 5
m Sample ID: A-2; 25FT. DN. GRAD. SUR. LabID: 9311023-08A CoUected: 11/18/93 13:20:00
TEST RESULT tJNITS LIMIT ANALYZED BY METHOD/CAS#
Manganese
Silver
pH (Soil)
195.4 ug/g
19.21 ug/g
7.6 pH Unit
0.3 12/03/93 LVD
0.1 12/03/93 LVD
11/19/93 JWJ
SW-846, 6010
SW-846, 6010
SW-846, 9045
Sample ID: A-2; 25FT. DN. GRAD. SUR. LabID: 9311023-09A CoUected: 11/18/93 13:20:00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chl orome theuie
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
J{Bg3on tetrachloride
IBirobenzene
c^sroe thane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,1-DichloroethcUie
1,2-Dichloroethane
1,1-Dichloroethene
2 - Hexcuione
Trans 1,2-Dichloroethene
1,2-Dichloropropane
Cis 1,3-Dichloropropene
Trans 1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
2-Propanol (IPA)
Styrene
1,1,2, 2 -Tetrachloroetheuie
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
il^^l Chloride
(•flene
1 orobenzene-d5
REStJLT
U
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u u
u u
u u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u u
Int. std.
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
LIMIT
500
100
100
30
30
30
50
500
30
30
30
50
50
30
50
30
30
30
30
250
30
30
30
30
30
30
30
30
30
250
2500
30
30
30
30
30
30
30
30
250
50
30
ANALYZED
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
-
January 4, 1994 08:15
19 le ID: A-2; 25FT. DN. GRAD. SUR.
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 6
LabID: 9311023-09A CoUected: 11/18/93 13:20:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Volatile Organics
1,4-Difluorobenzene
1,4-Dichlorobenzene-d4
Pentafluorobenzene
Int. Std. ug/Kg
Int. Std. ug/Kg
Int. Std. ug/Kg
Surrogate
Dibromofluoromethane
Toluene-d8
4-Bromofluorobenzene
12/06/93
12/06/93
12/06/93
For Volatile Organic
%Recovery
110
98.3
111
JMA
JMA
JMA
8 8240
SW-
540
363
Recovery Limits
75 TO 125
75 TO 125
75 TO 125
846
-36-
-72-
t
3
'4
8240
Sample ID: A-2; 25FT. DN. GRAD. 2 FT. LabID: 9311023-lOA CoUected: 11/18/93 13:30:00
TEST REStJLT tJNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Lead
B^fi nese
Silver
pH (Soil)
0.753
26.03
21.19
184.3
17.87
8.1
ug/g
ug/g
ug/g
ug/g
ug/g
pH Unit
0.2
0.60
3.0
0.2
0.1
12/03/93
12/03/93
12/03/93
12/03/93
12/14/93
11/19/93
LVD
LVD
LVD
LVD
LVD
JWJ
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
9045
Sample ID: A-2; 25FT. DN. GRAD. 2 FT. LabID: 9311023-llA CoUected: 11/18/93 13:30.00
TEST
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chlorome thane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Ch^^ome thane
I^^h lochloromethane
RESULT
u u
u
u
u u u u
u u
u u u
u u u
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
LIMIT
500
100
100
30
30
30
50
500
30
30
30
50
50
30
50
30
ANALYZED
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
METHOD/CAS#
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
January 4, 1994 08:15 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 7
m SuHiple ID: A-2; 25FT. DN. GRAD. 2 FT. LabID: 9311023-llA CoUected: 11/18/93 13:30:00
TEST
Volatile Organics
1,1-Dichloroethame
1, 2 -Dichloroethauie
1,1-Dichloroethene
2 - Hexauione
Trans 1,2-Dichloroethene
1,2-Dichloropropane
Cis 1,3-Dichloropropene
Trans 1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4 -Methyl - 2 - Pentauione
2-Propanol (IPA)
Styrene
1,1,2,2-Tetrachloroethame
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethame
.lA^l Acetate
IBl Chloride cl^flene
Chlorobenzene-d5
1,4 -Difluorobenzene
1,4-Dichlorobenzene-d4
Pentafluorobenzene
REStJLT
Int.
Int.
Int.
Int.
U
U
U
U
U
U
U
U
U
U
U
u
u u u u
u u u u
u
u u
u u
u std.
std.
std.
Std.
tJNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
Surrogate/Recovery Data
Surrogati a
D ibromofluorome thane
Toluene-d8
4-B: romofli jorober izene
LIMIT
30
30
30
250
30
30
30
30
30
30
30
30
30
250
2500
30
30
30
30
30
30
30
30
250
50
30
ANALYZED
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
12/06/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240
%Recovery
104
97.6
108
METHOD/CAS#
SW-846, 8240
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
-
540-36-3
-
363-72-4
Recovery Limits
75
75
75
TO 12 5
TO 125
TO 125
Sample ID: A-9; 318FT. DN. GRAD. 2FT. LabID: 9311023-12A CoUected: 11/18/93 12:49:00
TEST RESULT tJNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Lead
Silver
Isoil)
u
11.04
10.95
U
8.5
ug/g
ug/g
ug/g
ug/g
pH Unit
0.1
0.33
1.7
0.07
12/03/93
12/03/93
12/03/93
12/14/93
.11/19/93
LVD
LVD
LVD
LVD
JWJ
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
9045
January 4, 1994 08:15
#
CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 8
Su-^ple ID: A-2 COMB.;PT. OF DIS.SUR. LabID: 9311023-13A CoUected: 11/18/93 13:51:00
TEST REStJLT tJNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Lead
Manganese
Silver
pH (Soil)
0.200
10.53
14.03
155.3
0.659
7.8
ug/g
ug/g
ug/g
ug/g
ug/g
pH Unit
0.2
0.62
3.1
0.2
0.1
12/03/93
12/03/93
12/03/93
12/03/93
12/14/93
11/19/93
LVD
LVD
LVD
LVD
LVD
JWJ
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
9045
Sample ID: A-2 COMB.;PT. OF DIS. SUR. LabID: 9311023-14A CoUected: 11/18/93 13:51:00
TEST RESULT tJNITS LIMIT ANALYZED BY METHOD/CAS#
Volatile Organics
Acetone
Acrolein
Acrylonitrile
JI^Kene
^l^r lodi chl orome thane
Bromoform
Bromome thcuie
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochl orome theine
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
2 - Hexamone
Trams 1,2-Dichloroethene
1,2-Dichloropropame
Cis 1,3-Dichloropropene
Trans 1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene.
Ethylbenzene
Methylene Chloride
4-Methyl-2 -Pentanone
2-Propamol (IPA)
Styrene
1,1,2,2-Tetrachloroethame
T^^achloroethene
l^^vene
7^^ 1 -Trichloroethame
u
u
u u u
u u u u u u u u
u u u u
u u u
u u u u
u
u u u u
u
u u u u u u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
200
40
40
10
10
10
20
200
10
10
10
20
20
10
20
10
10
10
10
100
10
10
10
10
10
10
10
10
10
100
1000
10
10
10
10
10
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
January 4, 1994 08:15 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page 9
S!^ple ID: A-2 COMB. ;PT. OFDIS. SUR. LabID: 9311023-14A CoUected: 11/18/93 13:51:00
TEST
Volatile Organics
1,1,2-Trichloroethame
Trichloroethene
Trichlorofluoromethane
vinyl Acetate
Vinyl Chloride
o-Xylene
Chlorobenzene- d5
1,4-Difluorobenzene
1,4-Dichlorobenzene-d4
Pentafluorobenzene
REStJLT
k
Int.
Int.
i Int.
Int.
U
U
U
U
U
U
Std.
Std.
Std.
Std.
Surrogate/Re
Surrogate
UNITS
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
covery Data
Dibromofluoromethame
Toluene-d8
4-Bromofluorobenzene
LIMIT
10
10
10
100
20
10
ANALYZED
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240
%Recovery
91.9
95.5
110
METHOD/CAS#
SW-846, 8240
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
-
540-36-3
-
363-72-4
Recovery Limits
75
75
75
TO 125
TO 125
TO 125
Sample ID: A-2 COMB.;PT. OF DIS. 2FT. LabID: 9311023-15A CoUected: 11/18/93 14:08:00
mi REStJLT tJNITS LIMIT ANALYZED BY METHOD/CAS#
Cadmium
Chromium
Lead
Manganese
Silver
pH (Soil)
0.468
17.91
13.45
201.4
1.014
7.8
ug/g
ug/g
ug/g
ug/g
ug/g
pH Unit
0.2
0.58
2.9
0.2
0.1
12/03/93
12/03/93
12/03/93
12/03/93
12/14/93
11/19/93
LVD
LVD
LVD
LVD
LVD
JWJ
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
9045
Sample ID: A-2 COMB.;PT. OF DIS. 2FT. LabID: 9311023-16A CoUected: 11/18/93 14:08:00
TEST RESULT UNITS LIMIT ANALYZED BY METHOD/CAS#
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodi chloromethane
Bromoform
^^ome thane
il^Hitanone
^J^FJon disulfide
u
u
u
u
u
u
u
u
u
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
200
40
40
10
10
10
20
200
10
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
January 4, 1994
li,
08:15 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Pagel0
pie ID: A-2 COMB.;PT. OF DIS. 2FT. LabID: 9311023-16A CoUected: 11/18/93 14:08:00
TEST REStJLT tJNITS LIMIT ANALYZED BY METHOD/CAS#
Volatile Organics
Carbon tetrachloride
Chlorobenzene
Chloroethame
2-Chloroethylvinyl ether
Chloroform
Chloromethame
Dibromochloromethane
1,1-Dichloroethane
1,2-Dichloroethame
1,1-Dichloroethene
2-Hexanone
Trams 1,2-Dichloroethene
1,2-Dichloropropame
Cis 1,3-Dichloropropene
Trams 1,3-Dichloropropene
1,2 -D i chlorobenz ene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl- 2 -Pentamone
2-Propanol (IPA)
Styrene
1^, 2, 2 -Tetrachloroethame
I Brachloroe thene
^l^rjene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethame
vinyl Acetate
Vinyl Chloride
o-Xylene
Chlorobenzene-d5
1,4-Difluorobenzene
1,4-Dichlorobenzene-d4
Pentafluorobenzene
u
u u u u u u u u
u u
u
u u u u u u u u u u u u u u u u u
u
u u
u Int. std.
Int. std.
Int. Std.
Int. std.
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
10
10
20
20
10
20
10
10
10
10
100
10
10
10
10
10
10
10
10
10
100
1000
10
10
10
10
10
10
10
10
100
20
10
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8240
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
-
540-36-3
-
363-72-4
Surrogate/Recovery Data For Volatile Organics 8240
Surrogate
D ibromofluoromethane
Toluene-d8
4-Bromofluorobenzene
%Recovery
95.7
98.7
108
Recovery
75 TO
75 TO
75 TO
Limits
125
125
125
Sample ID: M-705; DECON WATER, GRAB Lab ID: 9311023-17A CoUected: 11/18/93
TEST REStJLT UNITS LIMIT ANALYZED BY METHOD/CAS#
pH
'liuffl
8.3 pH Unit
U ug/L
11/19/93 JWJ EPA 150.1
2 12/14/93 LVD SW-846, 6010
January 4, 1994 08:15 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Page11
• ^!zliple ID: M-705; DECON WATER, GRAB Lab ID: 9311023-17A CoUected: 11/18/93
TEST REStJLT tINITS LIMIT ANALYZED BY METHOD/CAS#
Chromium
Lead
Manganese
Nickel
Silver
Zinc
u
u
2.69
U
u
246
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
5
25
2
10
3
4
12/14/93
12/14/93
12/14/93
12/14/93
12/14/93
12/14/93
LVD
LVD
LVD
LVD
LVD
LVD
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
SW-846,
6010
6010
6010
6010
6010
6010
Sample ID: M-705; DECON WATER
TEST REStJLT
LabID:
tJNITS
9311023-18A CoUected: 11/18/93
LIMIT ANALYZED BY METHOD/CAS#
Volatile Organics
Acetone
Acrolein «rylonitrile
|zene
"modichloromethane
b J. omof orm
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethame
2 -Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethame
1,l-Dichloroetheme
1,2-Dichloroethane
1,1-Dichloroethene
2-Hexanone
Trans 1,2-Dichloroethene
1,2-Dichloropropame
Cis 1,3-Dichloropropene
Trams 1,3-Dichloropropene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methylene Chloride
4-Methyl- 2 -Pentanone
2-Propanol (IPA)
Styrene
1,1,2,2-Tetrachloroethame
JS^ rach 1 oroe thene
ffl^^uene
^I^F, l-Trichloroethane
u
u
u
u I.IJ
23.0
U
U
U
U
U
U
U
u
u 5.1
u
U
U
U
U
U
U
u
u
u
u
u
u
u
u
u
u
u
u
u
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
100
20
20
5
5
5
10
100
5
5
5
10
10
5
10
5
5
5
5
50
5
5
5
5
5
5
5
5
5
50
500
5
5
5
5
5
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
vTMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
SW-846, 8240
67-64-1
107-02-8
107-13-1
71-43-2
75-27-4
75-25-2
74-83-9
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
107-06-2
75-35-4
591-78-6
156-60-5
78-87-5
10061-01-5
10061-02-6
95-50-1
541-73-1
106-46-7
100-41-4
75-09-2
108-10-1
67-63-0
100-42-5
79-34-5
127-18-4
108-88-3
71-55-6
January 4, 1994 08:15 CERTIFICATE OF ANALYSIS
RESULTS BY SAMPLE
Pagel2
fi pie ID: M-705; DECON WATER LabID: 9311023-18A CoUected: 11/18/93
TEST
Volatile Organics
1,1,2-Trichloroethame
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
o-Xylene
Chlorobenzene-d5
1i4-Difluorobenzene
1,4-Dichlorobenzene-d4
Pentafluorobenzene
REStJLT
U
U
! U
U
u
u
Int. Std.
Int. Std.
Int. Std.
Int. Std.
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Surrogate/Recovery Data
Surrogate
Dibromofluoromethane
Toluene-d8
4-Bromofluorobenzene
LIMIT
5
5
5
50
10
5
ANALYZED
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
12/07/93
BY
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
JMA
For Volatile Organics 8240
%Recovery
96.6
98.6
104
METHOD/CAS#
SW-846, 8240
79-00-5
79-01-6
75-69-4
108-05-4
75-01-4
95-47-6
-
540-36-3
-
363-72-4
Recovery Limits
75
75
75
TO 125
TO 125
TO 125
m
#
•
#
•
Data Reporting Qualifiers
U Compound was analyzed for but not detected. Indicates compound was below detection limit.
J Indicates an estimated value. This flag is used either when estimating a concentration for
tentatively identified compounds or when the mass spectral data indicated the presence of a
compound that meets the identification criteria but the result is less than the specified
detection limit but greater than zero. (e.g. 1. IJ with a detection limit of 5.0)
B This flag is used when an analyte is found in the blank as weU as the sample.
E Estimated value. Result was outside of the caUbration range but within the Unear
range of the instrument.
BDL Indicates an analyte which was below the detection limits for the test.
NA Not appUcable.
NT Indicates that an analyte was not tested for.
Q Surrogate/spUce recovery was outside of the specified limits.