DSHW-1991-004001 - 0901a068806c10c6

TAazbZ CORPORATION
STRATEGIC OPERATIONS
29 August 1991
3140-FY92-IJO03
I{illian J. Sinclair, Hazardous l{aste Branch ManagerDivision of Solid and Hazardous Waste
Department of Environnental Quali,tyP. O. Box 15690Salt Lake City, Utah 84114-4880
Dear lrlr. Sincla.ir
Subject:Subpart X Sampling at !I-136 Burning GroundsThiokol UTDOO908L357
Thiokol Corporation has scheduled soil boring and sampling ofthe M-136 Burning Grounds for Tuesday, 3 Sept. 1991. This {tillprovide data for the development of our subpart X strategry forthis site
If you have questions, or if a member of your-staff would liketo observe this trork, please contact'Mr. Paul Hancock at 863-
9548.
ly.S
SL-l*o
J.. Slaughter, Supervisor
Envj.ronmental Engineering
irAs/PvH/pvh
PO. 9ox 689, Srigham Cntt UT 84302-0689 BOt) 863-351t
McoRPoRAnoN
STRATEGIC OPERATIONS
I{illiam J. sincrair, Hazardous'Iaete'Br:anrilr }lanager
Division of Solid and Haz.erdpud $a9te : " ;
Departrnent of Envirorne:rtaf * QualityP. O. Box 16690 :
Salt Lake CitY, Utah 84114:498.C
9 December 1991
3140-FY91-L11
Dear Mr. Sinclair
Subject:
s
Response to Coungnts and Paftj-al- Closure ,Plaiu'$pri-zis Burning crounds :- ': -'t:
Enclosed is the latest reVisio.n,; of -the P^e,rlitil Clgsure P,.l'an, for
Xtre il-225 Burning Ground". -lifrii-pf"t tinCfuieg re=popeer' tb. .tfrq .:
27 February conrnents by the SoliQ,and Halardpus'lilaste Comiltee i
concerning the previously subrnitted lartial- Clgsgre PIan.
These revisions should be inse*nfl. j{5!Q thd' Part'ial Closure
Ptan submitted 11 Decenber 1990.
If you have any qluestions o-r require any additional
ctarification, please contact PauI Hancock at 863-9548"
S/a/+
J. A.laughter, Superrrlsor
Environmental Engineering
PO Box 689, Brignant Cttv'. i-tT 84302'0689 l80l) 863-3571
''lJ:i
;,,!i i -r .i
.. h <f,r'e '' '/':'jf
rli;'.ii.
ir.,ltj-.1
A.^. - ..i. r:i .. .Ti ill
.,ri.
j:, i :',;::,-
--1r I
v+
I i.' 'il'
'''.1': ..::li
I
RESPONSE TO COMMENTS PARTIAL CLOSURE PLAN FOR
M-225 BURNING GROUND
Comments Received February 27, l99l
In Section 2.0 the pits are stated to be "closed'. It would appear that these pits are
simply "no longer used' and have yet to undergo closure. This should be clarified in the
aoolication.
The wording in section 2.0 has been changed to more clearly reflect our desire to close
these pits in this application.
Section 2.2. two lines up from the bottom of the page contains the typogaphical error
"actin" which should read 'action"-
This typographical error has been corrected.
The entire plan revolves around the Proposed Subpart S Action Levels presented in a
draft document dated 8-31-89. These levels have yet to be adoued by the State or EPA
and therefore, cannot be accepted or enforced. Furthermore, they are 'Action' levels
and not clean-up levels. Clean-up levels for this site will have to be proposed consistent
with the State's current and accepted conective action policy (R-45G101). The Bureau
does approve the removal and proper disposal of the ten by ten by four feet section of
contaminated soil so that complete characterization of the plume of contamination can
take place. This characterization would have to take place before a final decision on
clean up standards more than background could be considered.
Closure will be in accordance with the corrective action policy for the State of Utah (R-
450-101). This corrective action pollcy states that clean-up standards shall be based on
numerical, technology-based or risk-based standards. We have chosen to use risk-based
standards. The Subpart S Action Levels are based on risk-based standards as provided
by EPA on the Integrated Risk Information System (IRIS). The health assessment
information contained in IRIS has been reviewed and agreed upon by inter-disciplinary
review groups of EPA scientists and represents an Agency consensus. These standards
reflect a 106 risk factor for carcinogens and toxicants taking into account children using
the site as a playground. Since the site is a secured area these standards should be more
than adequate for cleanup levels.
2.
3
t.
t.ll
ht..
l'
,.:.:
i.1 '.:l
:
4.
6.
5
Section 3.5 refers to progress meetings to be held after each phase of the partid closure
operation. As long as Thiokol follows the procedures of an approved plan. these
meetings will not be necessary unless Thiokol has a sgecific need or problem. If during
any phase of closure. Thiokol deems it necessary to have a mee{ng, Bureau staff are
willing to meet to discuss the technical concerns and merits of any problem encountered
as a result of the closure process.
This section has been modified to read as follows: Once the partial closure plan has
received approval from the Utah Department of Solid and Hazardous Waste, The plan
will be carried out as approved. If, however, problems and questions arise during the
implementation of the plan, Thiokol will uurange meetings with the bureau to resolve the
concerns.
In Section 3.7. 'Resolving Differences". is a mechanism used in Consent Orders rather
than closure plans. All issues relating to the closure plan should be resolved Prior to
approval of the plan. Therefore, there will be no need for Section 3.7 and it should tre
deleted from the closure plan.
This section has been deleted from the plan.
Thiokol mentions the closure of other pits within the M-225 Burning Ground in Section
4.2. Have these areas been sampled to assure no contamination exists in the sections that
are no longer being used. (see comment Number l) if so. where can the analytical results
be found?
Section 4.2 has been modified to state that analytical results for the pits undergoing
closure are located in attachment 3 and in the Tables section.
The Bureau accepts and approved the plan for installation of at least four monitoring
wells as proposed by Thiokol,and this work can begin immediately. The configuration
of the wells. as it is currently proposed. would only be accegtable only if it were to
determine flow direction with additional down-gradient wells to be added as soon as the
precise flow direction is determined. Piezometers could possibly be a less expensive
method of initially determining the groundwater flow direction.
Your office was notified that monitor well installation began in September 1991 at M-
225. In a letter sent to the DEQ on December 5, 1991 it was explained that ground
water is in excess of 600 feet at the site. Due to these great depths we are halting
drilling to better characterize the contamination at the site. If we can determine that soil
contamination is limited and that the ground water has no contamination from the site we
7
8.
will request that no more wells be installed. Section 4.3 has been modified to state our
rational for installation of the monitor wells in the configuration specified. Essentially,
a potentiometric map indicates that well X-l would be upgradient. The actual
upgradient well would be determined from static water levels once the wells have been
installed.
Table 13 does not take into consideration that more than one round of excavation.
transportation and resampling may be necessary. Where the soil borings cleady show
contamination below the four foot level. it should be clearly stated that the.costs
represented are "per each round of removal" and the costs could be doubled or triPled.
etc.
Table 13 has been changed to read cost per round ofexcavation.
In ApDendix A. "Groundwater Well Installation Specifications". Section 3.1.1.B. states
that;Thiokol will dispose of all washwaters from the wash pit'. Specify the exact
procedures Ttriokol will follow to dispose of the washwaters. Also the details of the-hit'' and assorciated liner(s) must be described. Later in the same section. it is stated
that "steam cleaning fluid and DI water will be collected and retained for future analysis.
Justify retaining these washwaters for 'future" analysis.
Section 3.1 in appendix A has been changed to include detail on how the wash waters
will be contained and disposed and why the wash waters will be retained for analysis.
In Appendix A Section 3.7.3. "Dischu'ge Water", specify the exact procFdures and
faciliiils that will be used to dispose of the groundwater generated by the monitorinSl well
drilling process (see Previous comment).
Wording has been added to Section 3.7.3 in Appendix A to detail the procedures and
facilities used for disposal ground water generated during pump tests.
Appendix A. Section 3.8.4. does not make of sense. Iast sentence. "....after receivin8
written apgroval of the Thiokol displacement bladder pump....".
This typographical error has been corrected
In several places throughout the document it is stated the apProval of the Thiokol
Engineer islequired for certain operational changes to take place. The language should
9
10
11.
t2
be changed to read. in essence: "upon approval of the Thiokol Engineer and in
compliance with dl state and federal hazardous waste regulations.
The wording in the document has been changed to include the provision that all
operational changes will be done in compliance with all state and federal hazardous waste
regulations
PARTIAL CLOSI'RE PLAN
YT-225 BI'RN GROI'NDS
Resubmittal 9 December 1991
Lh-,ePREPARED BY:
ENVIRONI{ENTAL ENGINEERING
1.0
2.O
3.0
4.O
5.0
CONTENTS
TNTRODUCTION
1. 1 Background Investigation Phase
1. 1. 1 Volatile organics
L.L.2 Hearry lletals
1.1.3 ExPlosives
L.2 summary, Conclusion - Investigation Phase
1.3 Physical Setting
L.4 Waste Characterization
1.5 Soil Characterization
PT'RPOSE AND SCOPE
2.L Partial Closure Performance Standard
2.2 Partial Closure Time Schedule
ADMINISTRATIVE AND COMMT'NICATIVE PROCEDI'RES
3.1 Contact Persons
3.2 Communication of Events
3.3 Exchange of Information
3.4 Splitting SamPIes
3.5 Facility Access
3.6 Progress Review Meetingr/Subnittals
3.7 Fulfillnent of Partial closure PIan Obligation
PARTIAL CLOSI'RE PI,AN
4.1 Azide Pit Renediation
4.2 Trench Partial closure
4.3 Ground Water Monitoring
4.3.L Ground Water Statistical Methods
4.3.2 Ground Water Monitoring Schedule
PARTIAL CLOST'RE COSTS
TABLES
Tables 1-11 Contaminate Levels Per Depth
Ground Water Monitoring Parameters
Partial Closure Costs Azide Pit Soil
Tab1e L4 Partial Closure Costs Ground Water Monitor Wells
Table L2
Table 13
F'TGURES
Figure 1 14-225 Location MaP
Figure 2 Proposed Partial Closure PIan outline
Figure 3 Location of Yl-225 Soil Borings
Figure 4 Location of Proposed M-225 Wells
F'igure 5 Burn Pan Locations
F igrure 6 Potentiometric Surface Map
Attachnent 1
Attachment 2
Attachment 3
Attachnent 4
Attachment 5
Attachment 6
ATTAC}III{ENTS
Azide Pit Ash Manifests
Yt-225 Sanpling PIan
Sample Chain-of -CustodY
Yt-225 Drill Log
Christensens Boyles Corporation Report
Analytical Results from Analysis of 14-225
Soils
Lab Results Data Base
Box Plots - Contamination Levels Per Borehole
Corrective Action Proposed Rule Appendix A
Action Levels; Phone CaIl tlemo MCL Azide in
Soil
APPENDICES
Ground Water Monitor WeIl fnstallation
SpecificationAppendix A
Appendix B Ground Water Sampling Plan
1.0
1.1
INTRODUCTION
Thiokol Corporation operates an open burning facilityfor the open burning of waste propellants, andpropellanl ingredients in the Plant III, Hig!
Feriormance Piopellant Development Area. This open
burning facility is designated as yI-225 (see Figure 1for location). Formerly, the wastes were open burnedat 14-225 in unlined trenches. As of JuIy 1990, burning
pans constructed of steel, lined with clay, and placed
on support stands are now used. This partial closureplan addresses the M-225 area and is written to neet
Lhe requirements of the partial closure standard in
R450-7-14 of the Utah Hazardous Waste Management
Regulations.
Backcrround Investigation Phase
In the summer of 1989, a portion of the soil in the gas
generate burn pit (known as the azide pit) was pushedto facilitate the burning of the gas generate. Duringthe process of moving the soilr dD area sras uncoveredthat had a solvent odor. Subsequent investigation of
the site revealed that pyridine was present in thesoil.
A four phase plan was developed for the remediation ofthe site and this was submitted to the State. Anoutline of this plan is found in Figure 2. To date,
Phase t has been completed. This entailed removal of
the ash, making shallow borings, and sampling. The
azide pit ash was sent to USPCI for treatment anddisposll. A total of l5orooo lbs were removed (copiesof manifests are found in Attachment 1. USPCI treated
the ash with a volatile stabilization method using
activated carbon prior to placing it in their hazardous
waste landfill.
Soil borings uere made and samples taken on 26 and 27April. Tha location of these borings is illustrated in
fLqrure 3. A copy of the sampling plan is found in
Attachment 2. A copy of the field notes, Chain-of-
Custody form, drill 1og, and report from Christensens
Boyles Corporation are also found in Attachment 2.
Evergreen Analytical analyzed the soil samples for the
constituents noted in the sampling plan on a dry weightbasis. The reported results from Evergreen are in
Attachnent 3.
The analytical results were placed in a data base and
sorted by constituent for each borehole (see Attachnent4'). The following constituents above detection limits
(acetone, chloroform, nethylene chloride, 2-butanone,L,L,1-trichloroethane, toluene, total xylenes, sodiumazide, pyridine, trichloroethene, and perchlorate) were
analyzed using a statistical program. The data wasgraphically illustrated by a box plot. These box plots
show the range of constituents per sample and the
borehole with the highest level of constituents (see
Attachnent 5). As can be seen by the box plots, the
contaminants are prinarily in the A1 borehole. The
remainder of the boreholes have contaminates belowregulatory levels and many are similar to thosereported in the background samples which may indicatelaboratory error. The regulatory levels referred to inthis report are from Appendix A rrConcentrations MeetingCriteria for Action Levelsrr, Corrective Action ProposedRule FR VoI. 55, 27 July 1990 (see Attachment 5).
These are health risk standards established by the EPA
based on toxicity and carcinogenicity data. Tables 1
through 11 illustrate the reported contaminate levelfor each sampling depth for detected constituents.
1.1.1 Volatile Organics
Xylene and toluene were reported in all background
samples ranging from 1-7 ppb. These same levels are
found in all samples except A1 and may representlaboratory error. 2-Butanone htas reported in the
background samples at levels of 31 and 32 ppb. Sinilarlevels for 2-butanone are also reported in boreholes S,
A3, and H, indicating laboratory error. The remainderof the samples except A1 reported 2-butanone at lessthan detection lirnits. Trichloroethene was detectedonly in borings H and S, but is below corrective actionlevels. Methylene chloride was detected in trace
amounts (below corrective action levels) in all
boreholes including the background. These reported lowlevels could also be considered laboratory error.
Acetone is the most prevalent reported constituent andis found at lower depths in most boringsl however,acetone is below corrective action levels in allborings. Pyridine was detected only in the A1 boreholeto a depth of 6 ft, also below corrective action
Ievels.
L. L.2 Hearry Metals
Cadmium, Iead, mercury, and silver Lrere below detectionlinits in all samples.
1.1.3
L.2
Explosives
Explosive constituents (ffiX, nitroglycerin,perchlorate, and nitrate) were found only at lowIevels. Most samples were reported at below detectionlimits. Perchlorate, Hl,[X, and nitrate are not listed
wastes in 40 cFR 251. They are classified ascharacteristic wastes under reactivity or ignitabilityat high concentrations. H!,tX was detected in samples
S-2, S-4, C-4, C-6, C-8, R-2, and H-2. In each of
these, the HltX is at low levels and represents noreactivity hazard. Perchlorate was reported in several
samples, but in each case it is far below a
concentration to be considered an oxidizer.
Nitrogrlycerin was not detected in any of the samples.
Hitraie-N is at 1ow levels and is not a reactivity
hazard. Sodium azide was detected in only A1.
Summarv. Conclusion - fnvestigation Phase
I{ith the exception of A1, the levels of hazardousconstituents are at low levels. Therefore, the A2 , 43,
c, H, R, and S boreholes can be designated as below
concentrations meeting criteria for action levels
(AppendiX A, Corrective Action RuIe FR Vol 55, 27 July
leeo) .
The A1 boring was made in the center of the old azidepit area. the main contamination apPears to be limitedto this pit and to a depth of approximately 8 ft. An
examination of the soil lithology from the field notes
and drill logs show that a silt clay horizon is present
at approxinately the 8 ft depth and this is restrictingvertical rnigration of the contaminates. A2 and A3
borings were made approximately 15 ft auay fron A1.
This was done to determine the extent of horizontal
migration of contaminants from A1. The amount of
contaninants (azide, pyridine, and 2-butanone) in A2
and A3 show that no horizontal migration has occurredto those points. Therefore, the main contamination
from the ielease in the azide pit is limited to the
area imrnediately adjacent to A1 and to a depth of
approximately eight feet.
The contaminate levels in the A1 boring were comparedto the Corrective Action Proposed Rule Appendix AmConcentrations Meeting Criteria for Action Levelsrr.AIl contaminates except sodium azide uere below the
action levels. The level for sodium azide was notlistedr so Susann Griffin of the EPA Risk Asslssment
Group was contacted. She stated that the action levelfor sodium azide is 320 ppm (see Telephone Call Record,
1.3
L.4
1.5
and corrective Action Appendix A Action Levels in
Attachment 6). The azide contamination above the
action level is limited to the top four feet of A1.
Phvsical Setting
T}ae ll-225 Burning Area is located in a small, natural
amphitheater in the southern end of the Blue Springs
tti11s. oquirrh Formation, consisting principally of
fractured carbonate rocks, form low hills to the north,
south, and west of the facility. The topography on the
east opens to a small drainage channel. Soils are
shallow, generally less than 50 feet thick.
Ground water is believed to be deep and may exceed 400
feet depth. The ground water, based upon available
data, appears to be restricted to movement along faults
and fractures. This is evidenced by Plant I{eII No. 3,
which was drilled 325 feet into unfractured materials
and was abandoned, as it produced only a small volume
of water. Subsequently, Plant lilel1 No. 3A was drilled
as a replacement to Plant Well No. 3 and was drilled on
a fault having a N85 I{ trend. It can produce 190 gpm
with five feet of drawdown. Well 3A is located
approximately 4rOO0 feet east of 14-225.
Waste Characterization
The type of wastes open burned at the yl-225 facility
are uNo Class 1.1 high energy propellants and waste
containi.ng RDX, Hl{X, TI,IETN BTTN, nitroglycerine, and
other high explosives. UNo Class 1.3 compositepropellants including pyrotechnic and metal powders,
waste gas generate, sodium azide materials, andpropellant contaminated solvents. Since June 1989, thepropellant contaninated solvent burn pans have not beenusea. Propellant contaminated solvent is now sent off-plant for incineration at a hazardous wasteincinerator. A sma1l amount of solvent residue remains
on rags after the wipedown of propellant contaminatedtooling. These propellant contaminated raqfs are burned
along witfr the waste propellant in the burning pans.
Soil Characterization
Soils at Yl-225 are shallolr. They are generally less
than 50 feet thick. Surficial soils consist primarilof sandy, silty loam with small scattered gravel. Th
loam is five to eight feet thick. Beneath thissurficial loam, the soil consists of stratifiedlacustrine sediments of Pleistocene Lake Bonneville.
vis
2.O
2.L
2.2
These lake sediments are laminated silt and clay with
very fine sand. Pleistocene gastropod she1ls are
cotnmon in the sedinents and occasionally form thincoquinas. These sediments are approximately 20 feetthick at the azide pit. A coarse gravel is found
beneath the lacustrine sediments.
PT'RPOSE AND SCOPE
This partial closure plan addresses remediation of the
azide pit soils and installation of ground water
monitoi wells, and closure of the following five pits:
composite, high energy, azide, barrel, and solvent burn
pan area. The plan does not address the new burn pans
or the detonation pit. These will continue to be used.
Partial Closure Performance Standard
The partial closure of this area will be in accordance
with the partial closure performance standard of R45O-
7-L4 of Adninistrative Rules for the Utah Solid and
Hazardous Waste Committee.
Partial Closure Tirne Schedule
A time schedule for partial closure is specified below.
The time schedute reflects the timely irnplementation
and approval of the partial closure plan and lists
milestones for implementing partial closure. In the
event the established time schedule is jeopardized,
Thiokol will notify the State and its representatives.Additionally, upon conference with the State, Thiokol
may request an extended time period for completionpursuant to R45O-7-L4 of the ARUSHWC.
DATE FROI'T
PARTIAL CLOSUREACTION PLAN APPROVAL
Begin Phase III ground water
monitor weII drilling, samPling
and azide pit soil renediation
Phase III progress review meeting,report results to State
Begin Phase Iv - AnY furthercorrective action as required
Phase IV progress review meeting
1O Months
17 Months
2O Months
30 Months
3.0
3.1
3.2
3.3
3.4
ADI.IINISTRATIVE AND COUUT'NICATTVE PROCEDURES
Contact Persons
On approval of this partial closure plan, the State andThiokol Corporation will designate in writing therespective contact person(s) for coordination ofactivities and communications between the parties underthe plan. The parties will provide timely writtennotification of any changes during the term of thisplan.
Communication of Events
Thiokol will provide a mininum of 10 day advance noticeto the State, through the designated Bureau contactperson(s), of any construction, sarnpling, and/ordrilling activities to be conducted under this partialclosure and post-closure plan.
Exchancre of Information
Thiokol and State representatives trill cooperate in the
exchange of data developed pursuant to this p1an.
Copies within Thiokol,s possession of results of allanalyses and other relevant technical data generated bythe parties or their agents or contractors under thisplan, including raw data field notes, laboratory benchsheets, and reports, will be exchanged as soon aspractical. Any data designated as proprietary byThiokol shall be treated as confidential by the Stateto the extent and under the procedures set forth byapplicable law.
Splitting Samples
Upon request by authorized representatives of theState, Thiokol will provide split samples of anysamples collected pursuant to this plan. If anyanalysis is made of such samples, a copy of the resultsof such analysis shall be furnished promptly to ThiokolCorporation in accordance with Section 3007(a) of theResource Conservation and Recovery Act. This includesall relevant technical data generated by the Staterepresentatives, their agents t ot contractors.
3.5
3.6
3.7
4.0
4.L
Facility Access
Upon request, Thiokol will provide reasonable access toits facility to authorized representatives of the Statefof the purpose of monitoring, sarnpling, and observingactivities carried out under this p1an. Staterepresentatives shall comply with established safetypractices. fn the event representatives of the Statewish to have photographs of U-225 or the work carriedout under this plan, the camera, film, and all other
eguipment to be used in taking photographs will beprovided by Thiokol; an authorized State representative
may specify the type of filn to be used. Thephotographs will be taken by Thiokol photographers.
The authori.zed representative of the State willdesignate the area to be photographed and may bepresent if he or she so desires. If a photograph istaken of an object or an area which would indicate or
show proprietary information or processes, it will beprovided to the State only under the proceduresspecified by applicable law for the protection ofproprietary material.
Proqress Review Meetinq/Submittals
Once the partial closure plan has received approvalfrom the Utah Bureau of Solid and Hazardous waste, theplan will be carried out as approved. It, however,problems and questions arise during the implementationof the plan, Thiokol will arrange rneetings with the
Bureau to resolve the concerns.
Fulfillment of Partial Closure Plan Obligation
This partial closure plan and post-closure plan shallbe carried out by Thiokol and its respective employees,agents, contractors, successors, and assignees.
PARTIAL CLOST'RE PLAN
Azide Pit Rernediation
Remediation of the azide pit soils will entailexcavation of the azide pit to a depth of four feet inan approximate 10' x 10' area. The soil will beshipped to an off-site hazardous waste disposal companyfor volatile stabilization and chemical oxidation orchemical reduction. An independent engineer will
4.2
4.3
sample the excavated area and the soil will be analyzedto certify the site is below action levels. If soilsare not below action levels, the excavation andsanpling process will be repeated until these levelsare reached. After certification, the area will bebackfilled with native soils to grade.
Trench Partial Closure
The open burn trenches ca1led azide pit, barrel Pit,composite pit, high energy Pit, and solvent burn pan
area are no longer be used and will be closed underthis plan. Soil sample analytical results for thesepits are found in attachrnent 3 and in the tablessection. Burn pans have been installed as a replacementto the trenches. The burn pans have been placed in M-
225 in new areas. There are no pans located on the old
burn trenches. Figure 5 shows the placement of the new
burn pans. For safety reasons, the detonation pit will
continue to be used for the disposal of high1y unstablepropellants.
Ground lilater Monitoring
One upgradient and three downgradient monitor wellswill be installed to monitor ground water. Figure 6illustrates the probable potentiometric surface of the
Regional Aquifer at Thiokol's Sface and Strategic
operations in 1962. It indicates that the flow may
roughly parallels the surface contours in the U-225area. It is therefore anticipated that the up gradientwell will be above yl-225 at X-l as illustrated infigure 4. The upgradient well will be determined fromstatic water levels following well installation.Specific information on well installation is containedin Appendix A. The ground water will be analyzed forthe constituents listed in Table L2.
4.3.L. Ground Water Statistical Methods
Statistical comparisons of ground water will be made in
accordance with Guidance Docurnent on the Statistical
Analysis of Ground Water Monitorincr Data at RCRAFacilities. Interim final quidance, April 1989.
Ground Water Monitoring Schedule
If no statistically significant hazardous constituents
are detected in the ground water, a post-closure ground
water detection monitoring schedule will be
4.3.2
5.0
implemented. The constituents in Table 12 will be theparameters of the detection monitoring. Information onground water sanpling is found in Appendix B. However,in the event that no ground water contarnination isfound, Thiokol plans to petition that routine analysisfor any constituent be discontinued.
PARTIAL CLOST'RE COSTS
Partial closure cost estimates have been made for theimplementation of the ground water monitoring program.
These are listed in Tab1e L4.
The estinated costs for the remediation of the AzidePit soils are listed in Table 13.
TABI
161 - 212 '
2
4
6
I
t0
2
1
c
I
to
t2
e
fl2
&,
78
fi
0
fi
l4
t6
l2
l4
t0
t0tc
PTaDNE (PPB)
kt SUNFACE
nxx, -gf(m'
ziln
0
0
2
0
0
0
fiIilUilEtDE @A*f SUNFACE
118
orEil E:rlctrrl Lrr! t DUPLICATE SAMPLES TAKEN
SUNFACE hf
2
1Er._
12 EI:
14 ET.
IC EE
lgtr,
2AWATW{E (PPB)
TABL
52U'
250 1ilm'
2n
47ilt
ACETONE (PPB)
*tSUNFACE
2
I
0
0
6
I
fo
l2
ll
t0
tc
0
0
0
0
0
_- 15m0
5ilX>7il0
zUO
--@il,
a
1l
___&
f20
1l
t0
orril Elutrar uur! ' DUPLICATE SAMPI-ES TAKEN
TABL
xnErw (PPB)
0'fi'
htTA.UENE (PB)
SUNFACE *I
71- ff'
til2
1
c
I
f2
ll
tc
tc
w
ff
67
I
I
I
6
I
2
I
c
I
t0
f2
l1
tc
te
0
0
2
2
2
il
I
EEn Erurur rrtt ' DUPLICATE SAMPI-ES TAKEN
friEmttENE crLonfiE*t
ll EE-L--?
tc 0
TABL
I,f,1-TRICHL@GfiIAWE*t
0
0
2U
0
n
l1
28
f2
2f
2
I
c
I
t0
t2
f1
fc
tc
10fu- :---9
0
2
I
c
I
t2
fc
O{.EIllIrl EIETnl LI'I
TABI
2-BUT
0
XYLENE
2
ACETONE
18
TOLUENE
1
METHE CL.
5
h2 uNtT=(ppB)
1, 1, 1 -TCA
27
28 17
0
11
0
5
10
2
0
0
04
1
1
0
59
59
80
27
55
73
120
72
20
2
0
2
1
2
5
2
25
12
58
34
51
55
10
c
I
to
t2
f1
tc
tc
2
1EE
1
2
0
0
0
0 9
I
0
2
210
0 11
O=LESS THAN DETECIION Lnrns
ilrm
A? UNtT=(ppB)
1, 1, 1 -TCA
4
TABI
2-BUT
0
18
26
XYLENE
0
ACETONE
58
TOLUENE
0
MEIHE CL.
0
2
2
2
5
0
0
28
10
I
4
7
10
2
I
c
e
to
1
2
2
1
2
0
0
0
0
I
9
10
25
17
18
0
70
25
5
4
5
0
1
1
1
5
5
0
5
1
I
1
t2
l1
tc
tc
1 5
1
23
40
76
1
20FT 24
od-Eis fl{AN DErEcnoN urlFs
TABL
aACKenOUND uNtT=(ppB)
1,1,1-TCA 2-BUT XYLENE ACETONE TOLUENE METHYLENE CL
0
0
0
3
4
2
5
2
32
0
0
0
51
4
5
3
7
3
2
1
0
I
to
1
0
5
0
5
1
1
1
1
15
15 5
f2
l1
tc
tc
20
O=LESS TI{AN DEfEgnON LIMIIII
TABL
suffiAcE C uNtT=(ppB)
l,l,I-TCA 2-BUT XYLENE ACETONE TOLUENE METHE CN..
18
19
11
55
45
1
5
3
1
5
o
0
0
0
0
27
15
21
20
16
2
I
c
I
t0
t2
l1
tc
t8
1
3
5
1
5
5
I
I
1
1
20m
O:d-ES!i Tll N DEIECTION LlYlfS
TABI
H uNtT=(ppB)
TCA TCE 2-BITT XYI-ENE ACETONE TOLUENE METHE CL.
1t
2
I
1
46
11
1t
37
16
69
0
0
15
10
566
t0
53
58
29
21
2
4
0
e
to
t2
l1
tc
20
10
t5
0
21
30 t
1101
t8
OIllSS nnN flECnCl LilIs
nm
TABL
l,I,l-TCA 2-BIIT XYLENE ACETONE TOI.UENE METI{E CL.
160 3t
91
n uNrT=(ppB)
0
I
0
1
10
I
t
I
I
150
220
45
5E
53
5
5
4
I
1
0
0
0
0
0
26
1
19
2
I
c
I
t2
l1
fc
t0
0=BELOI{ DEIECIION LIMITS
an
TCA TCE 2-BIIT XYLENE ACETONE TOLUENE METHE CL.
2
5
0
0
5
1
9
0
I
1
55
51
t5
11
23
1
13
I
2
5
TABI
0
0
0
0
32
.g UNtT=(ppB)
I
48
0
0
t40
20
60
2
9
2
1
0
I
f2
l1
t6
t0
20 Fr.
0=BELOW DETECIION LIMITS
TABLE L2
YI-225 GROI'ND WATER ANALYTICAL PARAI'IETERS
PARAMETER
Volatile Organics(fncluding $zridine)
rilx
Nitroglycerin
Perchlorates
Nitrate
Azide
I.IETHOD
EPA Sw845 Method 8240
Provided by Lab (IIPLC)
Provided by Lab (HPLC)
Provided by Lab
SW846 Method - 92OO
Provided by Lab (HPLC)
1
TABLE 13
PARTIAL CLOSITRE COST ESTII'IATES
(PER ROITND OF REX'{OVAL)
1
2
AZIDE PIT SOTL
Excavation 10 X 10 X 4 Area
Transportation, Treatment, Disposal(24 ton 0 $1,200/ton)
Certification Independent Engineer
SoiL Analysis (6 samples)
ST'BTOTAL
Contingency 15t Subtotal
Adninistration 15t Subtotal
TOTAL
S soo
$28, ooo
S L,2oo
$ 3rooo
$32 r ooo
$ 4,905
$ 4,905
942,'LO
3.
4
5
6.
o
o
o
o
TABLE 14
PARTIAL CLOSI'RE COST ESTTUATES
CRITERIA 1 SHALLOW WELLS, NO CONTAT'IINATTON
Drill 4 wel1s/20r000 each
Samplino
1st year/3,OOO per uellDetection nonitoring/$f,500 per nell
CRfTERIA 2 DEEP I{ELLS, NO CONTAI.IINATION
Drill complete 4 re1ls/50r00O each
Samplincr
1st yearl3,0OO per well
Detection monitoring/L, 500 per well(yearly cost)
80, 000
L2 r00o6, 000
200r 000
12 r 000
5, 000
L2,OOO
28 r 000
2O0, 000
CRITERIA 3 SHALLOW WELLS,
4 wells/20r000 each
Samplinq
1st year/3,0OO per well
WITH CONTAIT{INATION
80, o0o
Subseguent. yrs/7 r000 per well(yearly cost)
CRITERIA 4 DEEP WELLS, WITH CONTAI'IINATfON
4 wel1s/50,000 per well
Samplinq
1st year/3,OOO per well
Subsequent years 17 ,OOO per well(yearly cost)
L2 TOOO
28 r 000
l'
ABcDEFtt
9
HP8
.R7
M-224
o3A
LEGEND
Soll thit ( gec Tsbl. 2
lot DorcrlDtion)
Soil Boring Locatlon-
(Bollins. Brown & Gunnlll, lnc lgaZ:
Faoilily Unlt
Protluclion Well
't0
tl
12
Scrl.
o rooo
F.at
TIGUBE I
Soll! MrD o, th. Hlgh Pcrlormancc
Propollant Dcvrlognont Ar.a)
'+.I KrC
SGG
a
HpB
SHE AEE
It'
l,
t:
KeB MIG
stD SHE
\fI
13
84 iC l0 AFrEB: Cll.Orl3t .l. at.. lat
PHASE 1
DISPOSE OF
AZIDE PTT
ASll
FUND CORE
AMLISES
srAFr
DRILLING
& suBlrI
SAT'PTES
6/eo
hIlERPREI
RESULTS &
DEVELOP
CTEA}I-UP
PUN
. GURE 2
M-225 CLEAN-UP
12/sO
PR(MDE
FUNDING
PHASE 5
PHASE 2
REPOFT
RESULTS &
PRESEilTPtlN TO
STAIE OF
urA.l (EPA)
OBTAN
SIAIES
AFFROVAL
TO FOIIOTT
PUN
6/e1
llr ,t
,Lt 12(f f.o.bL)
AT,J
CI ho-L)
PHASE 4
REPORI
RESULTS
TO STAIE
1 /92
DEVEITOP &
IMPLEMENT
CORRECIIVE
ACNON
REMOVE SOIL
& SHIP TO
I{AZARDOUS
WASTE DISPOSAL
FACILTIY
CO].TTA'IMNTS
NOT BELOWiO FT DEPIH BO-
DEGREGAIION
SONL \IENUNG
@NIAMIMNIS
EOST BELOT'
10 FT DEPIH
DRIII IYEIJS
A}|D MONTOR
GROUNMIAIER
PnDdd br RI\rnONllAnilL BlCtEnttG
JAN teeo
l_,l
BACK(;ROUIIDB 10 ft.
F- r-. .. t rr
t
F igure r'3
$.225 BI-TN PIT LAYOTJT
t 9!!. o'
o'
rt.o'
strrolRtFO^D
A1
@
20'
BARRELn@ PTT-10 f t.u-zz5 ouRllPII CLEAI.P
AREA
ComPoo I loc% to tt,
-l
f
I
l
I
I
I
I
I
I
I
(A3 SoIvoaI it"r.la l' l' ?Fov"
I
I
I
I
I
I
I
I
I
J
S 6- lO f.t.
HIGH ff'896 ?[,
Ourlod SfO. rla.ll' got"
U.225 BLNNPII OIRT
ROTD
crtIPSIER
ZO FT. o(r-EI-E, rmR
/ 6^rE
OETONATTON PTT
o'
I
t
I
i
i
I
I
II
l;
rE,r a.s rr cH.lN Ltlx IEIEEutrH 6^r€EO wlFE \
L-
TIGURE 4
LOCATION OF I{ELLS o
i,l. I
/
(
)i
t
)
I
\\
t\- j
a
r((
:t PROBABLE
GROUND IIATER FLOI.I DIRECTION
DETERMINED I'ROU . I.
POTENTIOMETRIC SURFACE I.I,AP 1962
\
N FIGURE 5
M-225 BURN PTT LAYOUT
r95'195'
,i
i-t
U
7'
MUELEoooR
Loip i_AB!E-_L -rrl OLD COMPOSITE TRENCH
OLD
145'7
l4'l4'
90
BTJRhIIhE
TRAYS
9B
OLD HIGH ENERGY TREN r-1 L_l
OLD SOLVENT BURN PANS
6 r 26'a t2'I tz'.
HIGI{ ENERGY
BURN TNG
TRAY 39
COMPOS I TE
. BURN[N6
TRAY
\oLrplitER
\
t
s6rolRtROAO
L
&
PIPE sPFt nos
No. C
r{oRsE sPFrr{os
?! 2r
Y-221
WELL 3
corilEB SPRrrOS
t""
a
ll,
G
T
?o
LEOENO
1237, W.t.r Su;lrcr Etortlon
-J3OO- Contour of Equrl wat.r Etovttlon
Flgurc 0. Potontloneirlc surlace of thc Heglonal Aguifer at Morton' Thlolrol'r Walatch Operatton! - lecember 1962
45
I|cttat0E
lrN
o [F508
TUELL
EST I{
EA
Et
oM-€3
ilo.4
1273',
r3G
I
oooD,
rll
)
E
tres)
tl o.I
o
L
EPETTO
oAo 3(FAra
M- tt4
1237-
€r ll o.
,WELL N ot
a8aQ',
w Eftu
7
ol-I
WELL II
WELL T .3A
APPENDIX A
GROT'ND WATER MONITOR WELL INSTALI,ATION SPECIFICATIONS
SAFETY PI,AN F'OR DRILLING AND CONSTRUCTION OT' WELLS AT YI-225
MONTTOR WELL INSTALI,ATIONn-223 BURN GROUNDS
JULY r.990
t'Lc i+,q^tbLraPREPARED BY:i .Fc. Hot uDAv lJ
nfivrnolruENTAr, ENGTNEERTNG
1.0
2.O
3.0
CONTENTS
INTRODUCTION
GENERAL CONSTRUCTION PRACTICES
GROT'ND WATER UONITOR !'ELt INSTALIATTON
3.1 General
3.1. 1 Drilling Methodology
3.L.2 Penetration Rate Log
3.1.3 Drillerts Log
3.1.4 Daily Drillerrs Report
3.1.5 Sanitary Protection of Well
3.1.6 Well Plunbness and Aligrunent
3.L.7 Collecting Cuttings
3.2 Well Casing
3.2.L Well Casing Selection
3.2.2 Methods of Joining
3.2.3 Casing and Screen Storage andPreparation
3.3 Protecti.ve Cap and Posts
3.4 Well Grouting and Filter Pack
3.4.1 Surface Fornation Seal
3.4.2 Granular Bentonite Grout
3.4.3 70 Mesh Sand
3.4.4 Filter Pack Material
3.5 Well Screen and Appurtenances
3.5.1 Screen Placement
3.5.2 Joining Screen to Screen
4.0
CoNTENTS (CONTTIIUED)
3.5.3 Bottom Seal of Screen
3.5.4 Centralizers
3.5.5 Screen Selection
3.6 Well Development
3.6.1 Surging and Bailing
3.6.2 Turbidity Linits
3.5.3 Recording Measurements
3.6.4 Discharge l{ater
3.7 Punping Tests
3.7.L Constant Rate Method
3.7 .2 Aborted Test
3.7.3 Discharge Water
3.7.4 Method of Water Level Measurement
3.7.5 Site Restoration
3 .7 .6 Slug Tests
3.8 Punping System
3.8.1 Type of Purgingr Purnp
3.8.2 Type of Sanpling hrnp
3.8.3 l{ell Caps
3.8.4 Punp Colurnns
3.8.5 E-Line Access Tube
3.9 Sunrey
REPORTING RESULTS
4.L Scope Upon Conpletion of the MonitoringWell Program
4.2 Hydrogeological Portj.on of Report
1.O
1.1
L.2
YT-225 IIIONITOR WELL INSTALLATTON
INTRODUCTTON
Thiokol corporation owns and operates a hazardous wastetreatment facility identified as VI-225 for the openburning of waste propellent and propellent ingredients.
Four deep borings, one upgradient and three
downgradient, will be drilled at M-225 as part ofpartial closure and post-closure care. The boringswill be drilled to the first zone of saturation which
may exceed 300 feet depth. Air rotary methods will be
used because of the great depths to be drilled through
carbonate, sandstone, and shale units. The followingare specifications which will be followed by a
contractor for installation of nonitor weIls.
Scope of Work
A proposal for the drilling and construction of ground
water monitoring wells at ltl-225 will consist of thefollowing:
1. Four eight-inch diameter ground water raonitoring
wells
2. Hydrogeologric report of the ground water system
Base Bid
The contract for the work described in thisspecification shall be a lunp sum contract. The bidshall be broken down in the following categories and aprice subrnitted for each category:
l.Ground water wells as specified in section 3.o. Bid
should be a lunp sum for L,2OO feet of drilling andwell construction. The established quantity of L,2OOfeet is provided for bid purposes only. If the actualguantity of weII construction is less than or more than
L,2OO fl-., the contract price shall be nodified byThiokol corporation based on the unit prices provided
by the drilling contractor. The contractor shallprovide a unit price for drilling and well construction
on a cost per foot basis.
Summary Report as specified in section 4.0.
Drilling contingencies described in section L.2.L
2.
3.
4 Costs per hour of extended punp tests described inSection 3.7
The bidder rnust provide a base bid as specified. Failure to
do so will cause the bid to be considered nonresponsive.
orilling Conti.ngencies
The following iterns shall be priced in addition to the
base bid above. The bidder will provide a price forthe following contingencies:
1) If unable to keep borehole open
a. Cementing and redrilling boreholes
b. Injecting water in the borehole to keep thehole open for further drilling
c. Reducing the size of the borehole with a
smaller diameter drive casing in order to
bypass the problem area
2) fnability to retrieve the drive casing
a. Cost for leaving the drive casing in place
b. Cost to insure the drive casing is sealed as
described in Section 3.2.LG
3) If perched water zones are encountered, and it is
necessary to seal the zones,
a. Cost to drill L2 inch diameter borehole
b. Cost to ream 8 inch borehole to L2 inch
diameter
c. Cost to seal water zone with 10 inch casing
and bentonite/cement
d. Cost to drill 9 7 18 inch borehole
e. Cost to seal water zone with 8 inch casing
and bentonite/cement
f. Cost to drill 7 7 /8 inch borehole
g. Cost to seal water zone with 6 inch casing
and bentonite/cement
h. Cost to drill 5 7 l8 inch borehole
L.2.L
1.3
L.4
1.5
Alternative to Base Bid
The following items may be priced in addition to the
base bid as called out in section 1.3. These items are
alternatives to these specifications. Along with a
base bid, all alternatives to the specifications should
include written specification changes andjustification. Alternative specifications will be
considered in the following areas:
1. Material of construction for wells
2. Alternate drilling methods
3. Alternate well locations or drilling sequence
Qualifications
Eachthat
1.
2.
3.
4.
5.
6.
7.
8.
bidder shall submit a Statement of Qualificationsincludes the following:
Iwo copies of the statement of Qualifications.
In-house capabilities including available
equipment and proiect personnel.
Specialized experience and technical competence ofthe firm, especially as related to monitor wellinstallation at hazardous waste sites.
Representative projects - include a project
description, a client reference with a telephone
number, the contract amount, and the period of
performance.
Qualifications of assigned personnel and their
assigned project responsibilities.
Locations where your firm can legally andlogistically provide services on a timely basis.
A list of aII subcontractors to be enployed and a
summary of the services they will provide.
Proof that a currently licensed Utah water welldriller will drill and construct the weIls.
Project Schedule
A project schedule sha1l be subnitted by each bidder.
The schedule will be taken into consid€ration by
Thiokol during the bid evaluations. ft will be
1.6
2.O
I
I
necessary for the successful bidder to satisfy the
Thiokol Project Engineer of the contractor's ability to
achieve substantial cornpletion and final completionwithin the times designated in the bid. Completion ofthis contract is to be within 90 days of notice to
proceed.
Bid Evaluation
The bids will be evaluated on the following basis:
r The quoted price of the base bid listed in section
L.2
r The quoted price of the alternates listed insection 1.3
! The quoted price of the drillingf contingencieslisted in section 1.2.L
The contractor's and any subcontractor'squalifications listed in Section L.4
The estimated time to commencement and completionof work as listed in Section 1.5
GENERAL CONSTRUCTION PRACTICES
The work is to be performed within a RCRA designated
hazardous waste management facility located within the
Thiokol Corporation Utah-based Operations.Accordingly, the CoNTRACTOR must adhere with allgeneral and job-specific regulations regarding, but notlinited to, safety, site-access, constructionprocedures, subcontractors, contractor-company liaison,
Lonpany inspections, deliveries, and site-maintenance.Thia includes reguired two hour industrial training
courses given by thiokol to each of the CONTRACTOR'S
employees. The CoNTRAcToR will be reguired to followall provisions of the site safety plan: Safety,Planfor M-225 Monitor Well Installation. All work is to be
performed in a professional manner and to thesatfsfaction of Thiokol's Project Engineer and in
accordance with state and federal hazardous waste
regulations.
3.0 GROI'ND WATER I,IONITORING WELL INSTALI,ATION
3.1 General
The CONTRACTOR shall drill the wells at the locationdesignated by the Thiokol Project Engineer. Each wellshall be drilled and constructed in accordance withthese specifications.
The CONTRACTOR will be required to provide aII tools,derricks, and other machinery and appliances ofwhatever description necessary and adequate for theconstruction and completion of the wells in aworkmanlike manner.
The wells shall be protected from contamination andwaste materials from drilling operations includingdrill bit cuttings. They shall be removed and disposedof as outline in Paragraph 3.1.18 and 3.L.7.
Tf, in the opinion of the Thiokol Project Engineer, itis necessary to discontinue work on the well whenpartially completed, by reason of the well being out ofline more than the limited amount described in theparagraphs on alignment or on account of jammed tools,caving ground t ot by reason or negligence on the partof the CONTRACTOR, then the CONTRACTOR shallimmediately start drilling another weII at a nearbylocation designated by the Thiokol Project Engineer.The CONTRACTOR shall seal off or plug the abandonedwell with concrete at the depths prescribed by theThiokol Project Engineer to prevent water frorn one zoneentering another zone. The area between plugs shall befilled with bentonite as directed by the ThiokolProject Engineer. The CONTRACTOR lrill be entitled tono palment for any work done or materials furnished forsuch abandoned weIls.
All neasurements for depth shall be taken from anestablished point on the surface of the ground at thewell site to the lowest point of the drill hole.
3.1.1 Drilling Methodology
A.The wells shall be drilled eight inch noninaldiameter by the Air Rotary nethod. No fluidsshall be injected into the well during drillingexcept air unless written permission is given bythe Thiokol Project Engineer. In unstableunconsolidated formations, the hole may be
advanced by driving the casing. Steel casing usedfor driving casing in unconsolidated formationsshall be removed when placing the well casing.Five feet of driving case will remain in place and
B.
act as a protective covering for the well casing.
As reasonable effort must be applied to remove thecasing. The effort must be to the satisfaction ofthe Thiokol Project Engineer.
A central area will be set up to clean and
decontaminate the drilling rig, drill too1s, bits
and sub. The equipment will be steam cleaned to
remove the dirt, washed with Alconox soap, andthen rinsed with deionized (DI) water. A11
washings will be done over a lined wash pit with
washings disposed of in a manner approved byThiokol Environmental Engineering and in
compliance with state and federal hazardous wasteregulations. The pit and appropriate liningmaterial will be supplied by the CoNTRACToR. TheIiner will be a new continuous sheet of plastic orother water proof material of a sufficientthickness or strength to be tear resistant. Itwill cover the bottom and sides of a pit with the
approximate dimensions of 8x8x4 feet. The pitwill have approximate capacity of 2,OOO gallons.
Thiokol Corporation will dispose of all wash
waters from the wash pit. The wash water disposalwill involve sampling and analysis for volatile
organics and the TC metals lead, cadmiirm,
chromium, silver and mercury using EPA methods.If the water is found to be hazardous it will betransported to the M-705 waste water treatmentfacility for the appropriate treatment (eg
activated carbon ect).
Tool joints will be made up dry or with graphiteor other approved non-hydrocarbon based lubricantto mininize sample contamination. Lubricants mustbe approved in writing and samples should besubnitted for analysis L4 days prior to intendeduse. To valadate that no contamination is beingintroduced and that the equipment is clean,
samples of the steam cleaning fluid and DI washwater will be collected and retained for futureanalysis. Cleaned sanpling and downhole drilling
equipment will be stored under plastic until it istransported to another waste site. At the drillsite, cleaned equipnent will be kept off theground by storing it on cleaned racks or pallets.
Any tools, drilling equipnent laying on the groundwill be considered contaminated and will be
cleaned prior to re-use.
Four borings, located in Figure L, will be
advanced twenty feet below the uppermost saturatedwater zone or to a depth approved by the Thiokol
c
D.
E.
F
Engineer. All borings drilled deeper than 350feet must receive rrritten concurrence from theThiokol Project Engineer.
Air from the compressor on the hydraulic airrotary or an external source shall be filtered toensure that oil from the conpressor is notintroduced into the hole. This filter shall beperiodically inspected and replaced as necessaryto keep oil from the compressor out of the hole.
Four deep welIs will be drilled to twenty feetbelow the water tab1e. The hole then will becompleted with twenty feet of 316 stainless steel0.010 inch continuous-slot reI1 screen followed bya 316 stainless steel casing to ten feet above thestatic water level. The remainder will becompleted with PVC (see Section 3.2.Lt to threefeet above the ground surface. The well casingwill be capped with a vented well seal. Figure 2is a description of a typical weIl.
The bottom 25 feet of the annular space betweenthe well screen/casing and hole will be sand-filled with 0.01 to O.0O3 inch or equivalent sand.
Two feet of 70 nesh sand will be placed above thesand pack and granular bentonite will be placed inthe well-bore/casing annulus to a depth of 18 feetbelow grade. The remaining 18 feet of annularspace will then be sealed with a cement/bentonitemixture. The sand shall be placed by gravitythrough a tremie pipe. The pipe shall terminatefive feet above the bottom of the hole and shallbe lifted gradually and sections removed as thelevel of the sand rises. The top of the trerniepipe shal1 be fitted with funnel fittings tofacilitate the shoveling or durnping of the sand.The granular bentonite shall also be placed bytremie pipe. Once above the static water level,the granular bentonite can be placed without thetremie pipe. Calculations will be made to insurethe proper amount of sand and bentonite was placedin the monitoring weIl. Granular bentonj.te may bepumped in the wells as a slurry at not less than1.5 pounds bentonite per gallon of hrater.Granular bentonite may be pumped into the wells asa slurry at not less than 1.0 pounds bentonite perga1lon of water, Lf not less than 16 hours elapsesbefore the surface formation seal (Section 3.5.1)is emplaced. Bentonite shall be free fromcontaminates or additives including pollmers.
Before the addition of the filter pack, bentoniteor cement, an attempt to remove the casing rnust be
G
3.L.2
3.1.3
made. If the casing is renovable, the filter pack
and bentonite shall be addedr ES described in
Paragraph F, as the casing is being removed. Ifafter a reasonable attenpt and approval by theThiokol Project Engineer, the casing fails to be
removed, the sand and bentonite will be addedr is
described by Paragraph F, to one foot below the
bottom of the drive casing. A cement/ bentoniteslurry shall be placed by tremie pipe to the level
one foot above the bottom of the drive casing.
Granular bentonite will then be added to the depthof 18 feet below grade.
Penetration Rate Log
During the drilling of the hole, a time 1og shall bekept by the CONTRACTOR showing the actual penetration
time required to drill each foot of hole. The types ofbits used in each portion of the hole shall be noted inthis log: drag, roller, button or percussion type,
together with approxirnate weight on the bits during thedrilling of the various types of formations in thevarious sections of the hole.
Driller's Log
During the drilling of the test hole, the coNTRACToRshall prepare a complete 1og by a qualified geologistsetting forth the following:
1) Name of person(s) logging the boring
2l The reference point for all depth measurements
3) Date boring acconplished
4t Weather including average temperature for each dayof drilling
5) Boring number
6) CONTRACTOR performing drilling
7) Type of machine performing boring
8) Drilling medium used
9) Sample, size, type, Iocation, and present recovery
10)
11)
L2l
13)
14)
15)
16)
L7l
The depth at which each change of lithology occurs
The depth at which the first water lras encountered
The depth at which each stratum was encountered
The thickness of each stratum
The identification of the naterial or lithology of
which each stratum is composed, such as:
A) CIay, silt, sand, gravel t ot combination
thereof
B) Volcanic ash or shards
C) Sandstone, quartzi.te, shale, siltstone,
dolomite t ot combinations thereof
D) Include: Hardness, friability, plasticity,color, reaction to dilute HCL, grading,
carbonate classification (rnicritic, sparry,crystalline, amount of colomite, etc. )
E) Describe bioclastics encountered
Descriptions of lithology shall be based uponintervals of five feet or distinct changes oflithology, whichever is less.
The depth interval from which each water and
formation sample was taken
The depth at which hole diameters (bit sizes)
change
The depth to the static water level (SWL) and
changes in StfL with well dePth
Total depth of comPleted weII
Any and all other pertinent information for a
comptete and accurate logi e.9., temperature, PH,
and appearance (color) of any water samples taken
Depth or location of any lost drilling fluid,drilling materials, or tools
The depth of the surface seal (must be in excessof 18 feet)
The noroinal hole diameter of the well bore above
and below casing seal
18)
1e)
201
2L)
221
231
261 The sealing off of water-beari
and the exact location thereofboring locations
The amount of cement (total weight in pounds)installed for the seal as discussed in Paragraphs
3.4.1 and 3 .4.2
241 The depth and description of the well casing,
including the steel drive casings in
unconsolidated formations
25l The description (to include length, diameter, slotsizes, material, and manufacturer) and location ofweII screens or number and size
ng strata, if any,includingr depth and
3 .1.4 Daily Driller's Report
During the drilling of the we1l, a daily, detaileddriller's report shall be rnaintained and a copydelivered to the Thiokol Project Engineer at the wellsite each day. The report shall give a completedescription of all formations encountered, number offeet drilled, number of hours on the job, shutdown dueto breakdown, and water level in the well at the
beginning and end of each shift, water level at each
change of formation if readily measurable with the
drilling method used, feet of casing set, and suchother pertinent data as requested by the ThiokolProject Engineer.
3.1.5 Sanitary Protection of Well
At all times during the progress of the work, the
coNTRAcToR shall use reasonable precautions to preventeither tampering with the well or the entrance offoreign material into it.
3.1.5 Well Plumbness and Alignment
The CONTRACTOR shall drill the hole sufficientlystraight, plumb, and circular to permit theinstallation of the specified casing and to permit theinstallation and removal of whatever pump utilized byThiokol Corporation, which may be either the turbine
and shaft type or the submersible t1pe, to be installedwith ease and in such manner that the pump will operatesatisfactorily under its design specifications and willnot be danaged by the hole being out of plumb and
3.2.L
alignment.
3.L.7 Collecting Cuttings
The CONTRACTOR shall determine a method to collectcuttings from drilling operations. The method ofcollection will allow the OWNER to periodically samplethe cuttings so that a determination as to whethef thecuttings are hazardous wastes or contain hazardousconstituents. The collection process must mininize the
dispersion of the cuttings.
3.2 Well Casincr
Well Casing Selection
CONTRACTOR shall supply all well casing specifiedherein except as specified below. A11 well casingshall be nerr. The casing shall be made of 315stainless steel for those areas in contact with waterplus ten feet and PVC for those areas greater than tenfeet above the static water level. All casing shall
bear nill markings that will identify the material asthat which is specified. The CONTRACTOR shall select
and use four-inch Schedule 10 stainless steel meetingthe standards of ASTM A409 and four-inch SDR 17 PVC
neeting the standards of ASTITI A409 and four-inch SDR 17
PVC rneeting the standards of ASTI.{ F480-88A (with flush-joint threads).
3.2.2 Methods of Joining
Casingr lengths shall be joined watertight by a methodappropriate to the naterial used, as selected by the
CONTRACTOR and approved by the OIi,NER, so that theresulting joint shall have the same structuralintegrity as the casing itself. If the drive casing iswelded, the Standards of the American Welding Societyshall apply. If the length of casing is to be welded,care must be taken to prevent the introduction offoreign material into the open hole.
Casing and Screen Storage and Preparation
Casing and screen shall be stored at the site in alocation designated by the Thiokol. Engineer and shall
be protected by contamination through the use of aground cover such as plastic. Prior to installation,
3.2.3
all casing and screen shall be steam cleaned, washedwith alconox soap and then rinsed with DI water (bothinside and outside). Care shall be taken duringinstallation of the screen and casing to prevent
contamination of the naterials following cleaning.
3.3 Protective Cao and Posts
Upon completion of the well, the CONTRACTOR shallinstall a suitable threaded, flanged, or welded capover the protective steel casing so as to prevent anypollutants from entering the well. The caps shall beuniform in design for each well, and constructed in afinished, workmanlike manner. They shall be capable ofaccepting a padlock to secure the well fromunauthorized entry. The ground imrnediately surroundingthe well casingr shall be sloped away from the well. A36 inch x 36 inch x 10 inch thick pad vill beconstructed around the protective casing. The pad willextend six inches below the land surface and fourinches above. There shall be no openings in the casingwall below its top
All nonitoring wells will be conpleted with three steelbarrier posts. The posts shall be six inches indiameter and six feet long. The post will be placed toprevent any vehicle traffic from damaging themonitoring wells and be embedded in concrete
approximately three feet below the ground Ieve1. Theconcrete anchor shall be approxirnately 18 inches indianeter.
3.4 Well Groutinq and Filter Pack
3.4.L Surface Formation Seal
The annular space in the constructed well will begrouted with a portland cement/bentonite slurrymixture. The bentonite content shall consist of a
maximum of 5t by weight. The length of the grout sealshall be whatever is necessary to prevent the entranceof surface water or undesirable subsurface water intothe well. In any circumstances, the length of sealshall not be less than the minimum specified by Stateof Utah regulations, which is not less than 18 feet.
The entire space to be grouted must be open andavailable to receive the grout at the time the groutingoperation is performed. If a section of larger pipe(temporary casing) is installed to keep the entire
space open (in caving materials), this larger pipe must
be renoved from the zone where the seal is required asthe grout is installed.
3.4.2 Granular Bentonite Grout
The annular space of the well shall be filled withgranular bentonite or bentonite slurry to within
eighteen feet of the surface. The grout shall only
consist of bentonite naterial not exceedLnq L/2 inch indianeter. The slurry shall be installed as outlined in
Section 3.1.1.F.
3.4.3 70 Mesh Sand
Two foot thickness of 7O mesh sand shall be placed
above the filter pack rnaterial and below the granular
bentonite.
3.4.4 Filter Pack Materi.al
The filter pack shall consist of clean well roundedgrains that are smooth and uniform. The materialshould be mostly siliceous with not more than fivepercent calcareous material by weight. The specificgravity of the filter pack material should be 2.5 or
greater. The filter pack sand shall be 0.01 to 0.03inch or equivalent sand. The CONTRACTOR will supplycertification on the size of the filter pack material.
3.5 I{eII Screen and Aopurtenances
3.5.1 Screen Placement
Four inch nominal diameter continuous-slot well screen
manufactured in accordance with these specificationswill be placed adjacent to the apparent better vater-producing formation, as designated by the Engineer.
The screen should be positioned ten feet into thesaturated zone.
Joining Screen to Screen
Screen sections for a single interval shall be joined
by threaded joints or welded with 316 stainless steel.Resutting joint(s) must be straight, sand tight, andretain 100 percent of the screen strength.
3.5.2
3.5.5
3.5.3 Bottom SeaI of Screen
The bottom of the deepest screen shall have a 316stainless steel and plate to seal it.
3.5.4 Centralizets
Centralizers shall be placed at the bottom of the well
screen and three feet above the screen. Centralizersshall be completely constructed of 315 stainless steel.
Screen Selection
All well screen sha1l be of the continuous-sIot, wire-
wound design, reinforced with longitudinal bars. Eachadjacent coil of wire shall be shaped in such a manneras to increase in size inward. The weII screen shallbe completely fabricated of four-inch dianeter, 316stainless steel. The aperture of the screen openingshall be 0.010 inches. The CONTRACTOR shall select ascreen with an appropriate schedule for the depth ofthe well and receive written approval for the selectionbefore installing the screen.
3.5 l{ell Development
3.6.1 Surging and Bailing (Utilizing Bailer)
The development process shall include air surging andbailing the well. The surging shall be accomplished byutilizing compressed air as the surging device. Iffines have been drawn into the well and have settled onthe bottom and accumulated to depth where they block 10percent or more of the total screen length, the wellshall be bailed. The well development nay be completedby submersible pumping with written authorization fromthe Project Engineer. The entire screened intervalshall be developed by moving the unit over the entirescreen interval. Punping shalI not be used as areplacement for surging. All water pumped from thewells during development shall be containerized andtransported by the CONTRACTOR to the proper on-sitedisposal facility.
Turbidity Limits
Development will be complete, when the neII discharge
3.6.2
3 .5.3
3.6.4
3.7
3.7 .L
has a turbidity of no greater than 5 NTU as measured by
turbidimeter.
Recording Measurements
A record shall be rnade showing tine, tyPe of operation,specific capacity during pumping, punping rate and the
sand content measured and recorded. These recordsshall be submitted to the Thiokol Project Engineer.
Discharge Water
Ground water must be containerized and transported tothe proper on-site disposal facilities. These disposalfacilities will be provided by Thiokol. The coNTRAcToRshall be responsible for the transporting of the ground
water to the disposal facility.
Pumoing Tests
Constant Rate Method
The CONTRACTOR shall furnish, install, and remove if
necessary measuring instruments and pumping equipnent
capable of pumping to the reguired point of discharge a
minimum of 15 gprn, against the total head of each weII,
and rith satisfactory throttling devices that the
discharge may be reduced. The punping unit shall be
complete with an ample porrer source, controls andappurtenances, and shall be capable of being operatedwithout interruption for a period of 24 hours.
Before any pump tests are conducted the CoNTRACTORshall notify the Thiokol engineer 24 hours in advanceof such tests. The Thiokol Project Engineer must bepresent during all pump tests.
After the test punp is installed but prior to the .actual punp test, the test pump will be pre-pumped atvarious rates to remove finer grained materials, tostabilize the aquifer materials, and to determine atest puurping rate.
The well shall be punped at the selected discharge ratefor a minimum of eight hours. The well may be pumped
up to 24 hours at the written request of the ProjectEngineer. The bid should include costs to provide
extended pumping intervals. The test pump shall haveits intake at Ieast five feet below the estimatedlowest pumping level, and shall have sufficient power
and capacity to achieve the designated discharge rate.
Discharge shall be measured rith a bucket and stopwatch, a circular orifice meter t ot a Venturi meter,
any of which are subject to approval by the ProjectEngineer. Discharge shall be rnaintained within plus or
minus five percent of the designated rate by means of agate valve or throttling detice. Discharge shall be
checked and adjusted, if necessary, every 10 minutesduring the first hour of punping and at 30 minuteintervals thereafter. The discharge and tine of
measurement shall be recorded each tine it is checked
and a note made of any adjustments. The static or non-punping water level trend shall be established prior tothe start of -the test. Drawdown in the weII shall be
measured according to the following schedule: 0-1Ominutes -- every 0.5 rninutes; 10-15 minutes -- every 1minute; 15-60 minutes -- every 5 minutes, 60-300
minutes -- each half hour; 360 minutes to the end ofthe test -- each hour. The actual time of each
measurement shall be recorded. On completion ofpumping, recovery measurements shall be recorded. On
completion of pumping, recovery measurements shall be
made according to the above drawdown schedule. TheThiokol Project Engineer shall have access to allmeasuring devices and points selected for drawdownmeasurements. Data logger and transducer vill beprovided by Thiokol Corporation.
3.7 .2 Aborted Test
After continuous pumping at a uniform rate has beenspecified, failure of pump operation for a periodgreater than one percent of the elapsed pumping timeshall require suspension of the test until the waterlevel in the punped well has recovered to its originalIevel. For the purposes of this section, recoveryshall be considered tf completert after the well has been
allowed to rest for a period at least equal to the
lapsed punping tine of the aborted test -- except thatif any three successive water level measurements spacedat least 20 minutes apart show no further rise in thewater level in the pumped well, the test may be resumedinnediately. The Project Engineer shall be the solejudge as to whether this latter condition exists.
3.7 .3 Discharge Water
Ground water must be containerized in a tanker truck
and transported to il-705 waste water treatmentfacility. It will be treated by activated carbon orother treatments as appropriate. The CONTRACTOR shall
be responsible for the transporting of the ground water
to the I.{-705 facility.
3.7 .4 Method of Water Level Ueasurements
trtethod of water level measurement shall be by data
logger and a pressure transducer. Static water level,
drawdown, and recovery measurements shall be recorded.
A clearly narked and readily accessible reference pointat the top of the well shall be established. Data
Iogger and transducer will be provided by Thiokol
Corporation.
3.7 .5 Site Restoration
cONTRAcToR is responsible for site restorationincluding removal of excess materials from constructionclean up of litter, wastes, and other debris. Allmaterial remaining on-site at Thiokol for 50 days or
longer after completion of the last well, will become
the property of Thiokol Corporation.
3.7.6 SIug Tests
If sustained purnping rates of 1 gpm cannot be
naintained in a weII, a slug test rnay be performed withwritten concurrence of the Thiokol Project Engineer.ff slug tests are performed, these tests must be
performed using a data loggrer and a O-10 psi pressure
transducer to collect water-level data. The transducerwill be provided by the contractor, and data shall be
recorded at an interval not to exceed 0.5 seconds.
Recovery data shall also be recorded and analyzed.
Before performance of the slug tests, a writtenprocedure for conducting the test will be presented to
the Project Engineer and he will give written
concurrence.
3.8 Pumpinq Svstem
The CONTRACTOR will provide for a dedicated putopingr
system for purging and sanpling each monitoring well.
The specification should include:
Type of Purging Punp
The pump shall be Grundfos nulti-stage, stainless steel
3.8. 1
3.8.2
3.8.3
3 .8.4
or equivalent submersible type that has a dianeter
srnall enough to be placed as a dedicated punp in each
welI. The punp shall be capable of generating a
minimum of 15 gprn with a 350 foot head. The motor
should be a rrinffin , 48O volt 3 phase or equivalentor be compatible with a portable 44o V generator
currently being used at Thiokol for operating the
existing monitoring uells. All electric cables shall
be secuied to the purnp colurnn every ten feet with nylon
cable ties. The coNTRAcToR shall supply all equipment
and fixtures necessary to make the punp operational.
Type of Sarnpling PunP
The pump shall be pneumatically operated, 9asdisplacement bladder pumps. At a minimum, the punp
should meet specifications of Geoguard Model 5915
(Anerican Sigrma) or !{e11 Wizard }todel ST11O1P and be
able to operate using the Well Wizard Model 3013-HPController currently being used at Thiokol. The
CONTRACTOR shall supply atl equipment and fixtures
necessary to make the punp operational. The sampling
pump shall be attached to the submersible punP column
with 316 stainless steel clamps. The clamps must be
constructed totally of stainless steel parts. See
Figure 3 for pump setting details.
Well caps
Each well shall be provided with one cap. The well capshall be a sealable cap with access to both pumping
columns, access tube, and any other necessaryattachnents. The cap shall be constructed of a
material capable of supporting the weight of both
pumps. Any cap used must be approved by the Project
Engineer. The CONTRACTOR shall supply all necessaryfixtures and adapters for installing the cap. A11Iines coning out of the well cap must have caps and
should extend at least 1/2 inch out of the well cap.
The teflon bladder pumP discharge tube shall extend not
less than 36 inches above the well cap.
Pump Columns
The punp column for the submersible punp shal1 be
constructed of 316 stainless steel. The column shall
have sufficient strength to support the submersible
pump and withstand operating pressures. The punp
column shall be securely attached to the well cap. The
pump column for the gas displacement bladder PunP slall
Le Lonstructed of virgin teflon material. The airlineshall be 3/8rr OD (1/4rrID) and the discharge line shall
3.9
4.0
be Ll2n OD (3/8[ID). Other tubing may be used after
receiving written approval of the Thiokol ProjectEngineer. The tubing pump column for the bladder pumpshall be installed as one piece, without joint orsplice, from the top of the bladder pump to three feet
above the top of the well caP.
3.8.5 E-Line Access Tube
An access tube shall be installed from the well cap tothe bottom of the well. The inside diameter of this
tube will be 314 inches and al1ow for access with awater-Ievel detector. The tube will be constructed ofpolyethylene tubing and strapped to the submersible
punp column every 10 feet with nylon cable ties. Thetube shall be one piece and be installed without joint
from the wetl cap to the bottom of the wel1. ft shall
be supplied with a threaded cap at the well cap.
Survev
The CONTRACTOR shall provide a survey of the we1ls
which will describe their location by the State PIan
Coordinate System. Elevation shall be established atthe top of the well cap inside the protective well
casing uithin 0.01 ft. accuracy.
REPORTING RESULTS
4.L Scooe Upon Comnletion of the Monitoring Well Program
The CONTRACTOR shall prepare a report on the hydroloqyof the area.
4.2 Hvdrocreological Portion of the Report
The Hydrogeologic Report shall include the followinginformation and is to be delivered to the Project
Engineer 30 days after conpletion of the final pumping
tests.
1) A brief geologic description includingstratigraphic units and geologic structure
At least two cross sections of the area withtopographic map locating monitoring wel1s andpiezornetric surface. The topographic map will beprovided by Thiokol.
2l
3)
4)
s)
6)
Local hydrogeologic description including but notlinited to direction and flow rate of ground
water, hydrologic conductivities andtransmissibility values, and estimates of aquifer
thicknesses.
Description of the ground water system including adiscussion on aquifer characteristics and resultsof pumping tests.
Results of field program including the followinginformation:
DriIl hole logs
Driller's logs
Description of field tests including all dataand calculations
Final technical specifications and anydeviation from original, includingexplanation for the deviation
Copy of all field notes. All field notesshall become the property of ThiokolCorporation and a copy will be included aspart of the report. Upon written reguest,the CONTRACTOR shall provide the originalfield notes.
Complete description of completed wells includingthe following:
Total depth
Elevation
Locations and types of material used for well
casing
Location and type of well screen and plug
Location and type packing and grouting usedin well
Location and type of punping system orsampling systern for each well includingdetailed specifications of any pumps andauxiliary equiprnent
Diameter of holes
Location and type of E line access tubes as
7l
described in Paragraph 3.8.5
Static water level measured in each well
A description of punping tests and aquifercharacteristics. This description will includecalculations, all raw data, and the results of thepunping tests and/or slug tests.
SECURITY CAP
g" srEEL
PROTACflVE CASING
GROUNO SURFACE
4.s" r.0.
SDR.I7 PVC
CASING
COUPLER rO JOIN
316 SS SCH. tO TO SDR - t7 Pv.c.
4t'l.o,3t6 S.S.
scH. to
CASING
3t6 gs.
o.ol"
4" l.D.
SCH. IO SCREEN
CONTINUOUS SLOT
316 S.S. END CAP
CEMENT/ QENTONITEGROUr - td rHtcK
VENTED WELL
CAPS
PROTECTIVE
POSTS
CONCRETE
8EN SEAL EACKFILL
VARIABLE THIC'<NESS
SEAL - 2, THICK
WATER TAELER
GRAVEL PACK25' rHtcx
.
-
6rl i-rD
TYPICAL COMPLETION DETAILFIGURE 2
NOT TO SCALE
WELL CAP
ANO PUMP SUPPORT
316 s.s. CLAMPS
I SUFFACE CASING
SAFETY CORO
3t6 s.s. PiPE COLUTTN
tl
FIGURE 3 PUMP INSTALLATION DETAILS
3/4,, POLYETYLENE ACCESSrUBE
AIR ANO DISCHARGE L'NESTO ELAODER PUMP
SAMPLING PUMP
Grunc,Fos SU8MERSTBLEPUMP tN/ Fronktin MOTOR
NOT TO SCALE
APPENDIX B
YI-225 GROUND WATER
SA}IPLING PI,AN
13 JULY L990
Prepared by:J.. Ho1ladayironmental Engineering
P. V.Hancock, QAIQC off
_L-
Concurrence by:
Environmental Engineering
cer
1
2
TABLE OF CONTENTS
O PURPOSE AND SCOPE
O SAI{PLE COLLECTION
2.L !{ater Level Measurement
2.2 Purging the Monitor Wells
2.2.L High Yield We1ls
2.2.2 Low Yie1d Wells
2.3 Purging and Sanpling Equipment
2.3.L Subrnersible in Tandern with Gas Displacement
Bladder Pumps
2.4 Sanpling Procedure for Monitor Wells
2.5 Field Quality Assurance and Control Programs
2.5.L Quality Assurance and Control officer
2.5.2 Fie1d and Trip Reports
2.5.3 Blind Controls and Spiking Samples
2.5.4 Sample Handling
2.5.5 Labeling Samples
2.5.6 Fie1d Book
2.5.7 Chain-of-Custody Control Procedures
2.5.8 Field Equiprnent Calibration Procedure
2.6 Sample Collection Schedule
O ANALYSTS OF GROUND WASTE SA!,TPLES
3. L Parameters
3.2 Laboratory
O ASSESSMENT OF DATA AFTER ONE YEAR OF SAI.{PLING
4.1 Purpose and Scope
3
4
1.0
2.O
2.t
2.2
2.2.L
PURPOSE AND SCOPE
Thiokol has developed this plan to satisfy the
i"q,ri."rents ior-i' q.ou1d- triter sarnpling and analysis
pri" of 40 cFi zes.5: witr, respect to detection
rnonitoring.
Theplanspecificallyaddressesthesamplingofground,ii.i monj.toring welis at Thiokol I s 1q-225 site. The
olan addresses iff procedures for taking.ground water
Iiiif"rl-=ntpping tire samples for analysis, and methods
for analYzing samPles.
SAI,IPLE COLLECTION
I{ater Level }Ieasurement
Before sarnpling any ground water monitoring wells' a
water levei *eisur-enent will be taken using an
eiectronic water leve1 indicator to the nearest o.oL
ft. The watei-fevef will be recorded in the field book
before each monitoring well is sampled'
Purqing the Monitorincr We1ls
The ground water monitoring well_will be purged before
;;;piG;--tregins. Monitoring werrs must be purged so
ih;t stignant waters which ire not representative of
ite watei in the aq'ifer can be removed before
sampling.
The amount of water to be removed from the wel1s is
dependent upon the ground water yield of the
iniormation- in which the wetls are located'
High-Yield Wells
Forhigh-yieldwells(whichproducegreaterthan]-
gprn) , fnr-ee casing v9]um9s of water will be removed
i;;'the well or intil the pH, temperature, and
conauctance has stabilized, whichever is greater-. . A
""-ing volume is defined as the volume of water between
the witer level measured and the total depth of tle.
,o"ii"ring weti. The casing volume.will be calculated
a,riitg ea6n sampling period, so that a-consistent
volume of standing ialer can be removed prior to each
sampling.
2.2.2 Low-Yield Wells
For low-yie1d wells (which produce less than 1 gprn),the well will be evacuated to dryness. Before anysampling, the wells will be evacuated a ninimum oi twotimes to guarantee all stagnant water has been removedfrom the weII.
2.3 Purging and Samplinq Ecruipment
Monitoring wells will be eguipped with a submersiblepump dedicated to each nonitoring well. It isanticipated that the wells will be approximately 200 to40O feet in depth. The submersible purnp will be usedfor ptrging thL monitoring wells. A ga-s ai=placemenibladder purnp will be used for sampling the monitoringwells.
2.3 .L Submersible in Tandem with Gas Displacement Bladder
Pumps
The bladder pump wiII be placed above the submersiblepunp. The submersible will be placed towards thebottom of the screen with the bladder pumprs intakebeing suspended about one foot above the subnersiblepump (see Figure 81).
To insure that the water sampled in high-yieldformations is representative of the aquifer, thestagnant water between the two pumps must be purged.The voluure of water that exists between the two pumpsis less than one gallon. To insure that this critilafvolume is well purged, the water from the bladder pumpwill also be tested for the stabilization of the pH,temperature, and conductance readings.
In low-yie1d wells, the well will be evacuated todryness.
2.4 Samnling Procedure for Monitoring Wel1s
Each well will be sampled using the followingprocedures:
1) Each well will be thoroughly purged beforeremoving a sarnple.
Each weII will have a dedicated gas displacementbladder or a submersible sampling pump (sarnplingpump) to minimize any crosg contamination.
2t
3)
4',)
s)
The sampling putrrp will be operated to produce a
stream of ground water. Before taking a sanplethe pH, specific conductance, and temperature will
be measured using portable meters. No sample willbe taken until the pH, conductance, andtemperature has stabilized. After threestabilized pH, conductance, and temperature
readings have been made, a sample from the pump
will be put into an appropriate container.
The samples will be taken in the following order:
1) Volatiles2) Explosives: Azide, Nitroglycerine, HMX,Perchlorate
ff sarnples are being split, the samples will betaken directly from the ground water monitoringwelI. This process will be done in order to
minirnize volatilization of sensitive organics.
2.5
2,5.L
Field oualitv Assurance and Control Prograrn
The field QAIQC program is set up to insure theintegrity of the ground water samples during sanpling
and shipping to the laboratory. The field QA/QC willbe overseen by a Quality Assurance and Control officer.
Quality Assurance and Control officer
A QAIQC officer has been appoint,ed to oversee the
Ground Water QA/QC Plan, implement all phases of thefield guality assurance and control program, and toperiodically audit the laboratoryts QAIQC program. The
QA/QC officer will work with the sampling staff and theIaboratoryrs QA/QC officer to assure that the datacollected from the ground water is accurate. Figure 82
shows the QAIQC responsibility chart and lists the
members of each staff. The QA/QC officers dutiesinclude:
1) Makingr sure that, the Ground Water Sampling Plan is
followed.
2l Making sure the contracted laboratory followstheir QA/QC Plan.
Send spiked samples periodically to the contractedlaboratory to audit the QAIQC program.
3)
2.5.2 Field and Trip Blanks
Each sarnpling day, a field blank will be collected andstored with the water samples. The field blank is to
ensure that no contamination of the sample occursduring shipping frorn the field to the laboratory. Thisblank will consist of a distilled water sample whichwill be analyzed for constituents.
The analysis of the Field Blank will show one of thefollowing three occurrences:
f-) No contamination. In the case where thecontamination level is below detection 1evel ordrinking water standards, no remedial action willbe necessary.
2)Low level contamination. In this case where the
contamination level is greater than an order of
magnitude when compared to the field sampleresults, the Q /QC officers from the laboratory
and Utah-based operations will discuss whetherresampling of that days wells will be necessary orif no remedial action is needed.
3)High level contarnination. In the case where thecontamination [Ievels are within an order of
magnitude when compared to the field sampleresultstt and in Case 2 the QA,/QC officer willreview sampling and L shipping practices andinstitute any changes necessary to solve thecontamination problem. High level contaminationwill necessitate resampling of that days weIls.
A trip blank for each sanpling period will be sentby the laboratory. The trip blank will insurethat no contamination of the sample has happenedduring shipping. Upon analysis of the trip bIank,the same procedures for correcting the sarnplingplan for field blanks will be followed.
2.5.3 Blind Controls and Spiking Samples
If post-closure analysis is necessary, the QA/QCofficer will annually send a spiked sarnple or a blindcontrol to the laboratory to audit the laboratoryrs
QA/QC program. Both the blind control and a spiked
sample are samples with a known arnount of solute in asolvent. The difference between a blind control and aspiked sample is the following:
EPA 1986. RCRA Ground !{ater Monitoring Technical
Enforcement Guidance Document. pp. 1L9
t_
2.5.4
2.5.5
1) Blind control - An unannounced spiked sample sentto the laboratory.
2l Spiked sample - An announced spiked sample sent to
the laboratorY.
The amount of solute and in either case is not divulged
to the laboratory. All spiked solutions will be
recorded in the Field Book with the concentration
added
A spiked sample will be sent first to the laboratory.ff the recovery is questionable, then a blind controlwill be sent to the laboratorY.
The QA,/QC officer will review the spike or blind
control recovery. If the spike or btind control
recovery is out of line with the laboratoryrs surrogate
spike and matrix spike recoveries, the laboratoryrs
AL/ac officer will be contacted to see if the problem
can be resolved. If unresolvable, a new laboratorywill be contracted.
Sample Handling
Sanpling equipment and technigues have been designed sothat the ground water sample is not contaminated oraltered in any !ray. A11 samples reguiringrefrigeration will be packed in a waterproof container
and packed with reusable freezer packs to reduce
temperature. A11 samples wiII be packed tightly with
proper packing naterial. AIl samples will be labeled
and acconrpanied by a laboratory request and Chain-of-
Custody sheets.
Labeling Samples
All sample containers will be labeled with thefollowing information.
1) Sarnpling date and time
2) Sample number
3) Name of person taking samPles
4t Parameters to be analyzed in sample
5) Location of sampling Point
6) Preservative added (if applicable)
2.5.6 Field Book
During each sarnpling period, the person sampling theground water wells will keep a field book into whichall relevant information regarding sampling will berecorded. The data must be entered in the book using
permanent ink. The following information will beentered into the field book:
1) Signature and date of person(s) conducting the
sampling
2)General weather conditions and approximatetemperature
3) Date and time each well is sarnpled
4)Sarnple number and location of sample (i.e., well
nurnber)
Static water level in weII
Volume of a casing of water
Flov rate and purge start and stop times
e)
pH, specific conductance, and temperature measuredduring stabilization of welt
Conductance and pH meter calibration date
10)Any irregularities in the sampling procedures orin the conditions of the wells
11)Any other infonnation the sampler deems necessaryor irnportant during sampling
2.5.7 Chain-of-Custody Control Procedures
All samples requiring off-plant analysis will becontrolled by Chain-of-Custody procedures. AIt samplesthat are shipped off-site, nust be accompanied by aChain-of-Custody fortrr. This form must be completelyfilled out, signed, and dated by the sampler.
AIl samples will be sealed with a Chain-of-Custody sealto guarantee sample integrity. The seal will besigned, numbered, and dated by the sampler. Care sha11
be taken to seal each sample container with the seal.
The seal will be placed so that the container cap is
sealed to the sample container.
s)
6)
7t
8)
2.5.8
2.6
3.0
3. t_
This container will be placed in a lockable coldstorage box. This box will be in the possession of theperson charged with the custody of the samples or thebox will be locked and placed in a secure p1ace. Underno circumstances will the box with samples be leftunlocked or unattended.
A copy of all the Chain-of-Custody forms will be
reviewed for accuracy and filed by the QAIQC officer.
Field Equipment Calibration Procedure
Before each quarterly sampling of the ground water, the
pH meter and conductivity/temperature meter will becalibrated. Each meter is to be internally calibrated.Before sarnpling, the meters will have the internalcalibration tested with a known standardLzed solution.
The tenperature meter will be calibrated with a mercurythennometer. If any differences arise a calibrationcurve wiII be developed between the internal andexternal standards. Before each well is sampled, themeters will be calibrated using the internal standard.
Record of these calibratioirs will be kept in the FieldLog Book.
Sanple Collection Schedule
The ground water monitoring wells will be put on a
sampling program. Each sample will be analyzed for theparameters discussed in Table 13 of the closure plan.If post-closure sampling is reguired, all wells will besanpled quarterly for the first year and semi-annuaIlythereafter per 40 CFR 265.92 (d).
ANALYSIS Of GROUND WATER SAI'{PLES
Parameters
The ground water samples initially will be analyzed forthe parameters identified in Table 13 of the closureplan. All samples will also be analyzed for the fieldwater guality parameters identified in Table XV of theclosure plan. AII analyses except nitroglycerine,azide, HI{X, and perchlorate will be approved EPA
methods.
3.2
4.O
4.1
Laboratory
All samples will be analyzed by a State certifiedIaboratory using EPA or State approved analyticalnethods. Table 13 of the closure plan identified thespecific rnethods used for analysis of the parameters.If the contracted laboratory is not State certified to
do a specific analysis, the contracted laboratory will
subcontract a qualified laboratory to do the analysis.
ASSESSITENT OF DATA AFTER ONE YEAR OF SAII{PLING
Purpose and Scope
40 CFR 265.93 states that an assessment program must be
made after one year of guarterly sampling that is
capable of determining the following:
1) Whether hazardous waste or hazardous wasteconstituents entered the ground water;
2) The rate and extent of migration of hazardous
waste or hazardous waste constituents in the
ground water; and
3) The concentrations of hazardous waste or hazardous
waste constituents in the ground water.
After one year of sampling, a report will be prepared
and submitted to the UBSIIW to address these
requirements.
FTGURE 82
QA/QC RESPONSTBILTTY CHART
UTA}I-BASED OPERATIONS
QA,/QC OFFICERP. V. HANCOCK
GROUND WATER SAIIIPLERS,I
COVINGTON
HANCOCK
HOLI,ADAY
ISON
D
P
J
s
L
v
c
B
*Current Sampling Staff as of L0 December 1989
TABLE 13
YI-225 GROT'ND T{ATER ANALYTICAL PARAMETERS
PARAMETER
Volatile Organics (fncluding gzridine)
HMX
Nitroglycerin
Perchlorates
Nitrate
Azide
METHOD
EPA Method 8240
Provided by Lab (HPLC)
Provided by Lab (HpLc)
Provided by Lab
SW846 Method - 92OO
Provided by Lab (HPLC)
lnlormation in lh€ shaded areas
is not required bY Federal law'2. Paget
of
t. Generalo/s US EPA lD No.
UNIFORM
WASTE
HAZARDOUS
FESTtrlANl Documgnt Numb€rState Manarest
'- .--,1 : t. ;B. Statecenerato/s
801-4.
Corpor
689,
ationAddrossthioko1andMailingNamoGenerato/s3.103S14lBoxPo -068984302tITc1aI[Br ty1eJ
C. Stelo ID
PhonaD.
US EPA lD Number6.Company Name5.
L ]DTransportefs
PhoneTraNports/sF
8.US EPA ID NUMbET
ComPanY Name7. TransPorter 2
10.US EPA lD Number G. State Facilit/s lD
9.Nameion and Site Addless& Contror,lnc
Mountain Facl1ity H. Facilit/s PhoneGrassvNorth0ff3}tiLes East 7 !,liles
1 1 1 Waste No.
DoscriPtion (lncluding Prcoe,r ShipPing Name,Hazard Crass and ID Number)No.11 US DOT FEoq
a.llazardous Waste Solid, N'0'S'
oRIl-E NA9189
2 I
b.
c.
d.
I K. Handling Codes for Wastes LBtedAbo/e
J- Adtlitional De$riptiong lor Materials Listed Above lo-
A. G*789-2O29-89
38 3-7{lRT/STR
goggLes, aod Protective clothing with a respirator'Gloves,
lnlormationand Additionatlnstrudions15. SPecial Handling
L
aDo\rodcacriDcd byateandaccutalolylullythi3olcollstgnmeilconloil3thethaldrdsteherobylorh19hwaybyco.rdition tran3po.tinGETERAIOR'S allin pfo9€,alrS re3p3ctsarl(llabolod,andmarkod.dasstfi€4ar6 pacxed.endnarntshipprtrgp,oPcr be,egulalio,l3.lonalbnd(bterminedhat ego1romm€olafil theinloma$onal to d€gr6etowast0applicabbolg€neraledaccordingtori.ityandvolumet116roducoinlo andrhopte36nlhavaphcoes'hidi minimizcS$tat pfognm lo mocertfyavailaDl6taatngtlc ato(quarnily o.rrsillYotdBposalrlar96slorago,traaun€ol,ol saLctandm6lhodthewa3topftldicabLsol3dedminimizogon6rationmatIlrarr6toet orl 'Iryarxtlaithamedop.actbabb€oono.fiicaIY havo EOodsmalgeieratot,a quantltyamitIoR,anvitonmeot;lheandhsallhhumenlhraelhfiJro I arlord.that canandmatoislhalavalaDle YearfnolhodDaywastob6slrnSnaoorn€ntlh6
Name\,
MaterialsololRocgipt17. Transportar 1 MonthZwru
ta-. Yans YeatMonthSignature
T
RAr3Po
RTg
R
Namo !
19. DiscrePancY lndication
Item 19.
Owner or
asolmanilestthisbycoveredmaterialshazardousol Month OaY Yeat
Signature
?Ac
IL
Ir
Y
Ploes6 lor usaon olit6
uaELiilAFK CO.. CHICAGO' lL 6OE e
Fqn $,qrcvact-OMA No.2050'0039. e,Prcs 9'30'9t
G
Eil
E
B
A
T
o
R
otlaalllAa -orrttoi' ?'i ^elrr^'6-
styl. F15REV'6 UAELM STEF' Oiv' ol AMEBICA,.
EPA Fo.m 87OO'22 (Bd 9'88) Ptwi(s 6dirm3 am obsobtc'
2. Paget lnlormation in the shaded areas
is not reguired by Fecleral law.
1. Gensrator's US EPA lD No'UNIFORM HAZARDOUS
WASTE MANIFEST
Thiokol CorporationP. O. Box 689 M/S 301
Brlgham Clty, UT 84302-0689
3. Generato/s Name and Mailing Address
4.C. State ro
D. Transporte/s Phone5. Transporter 1 ComPanY Name 6. US EPA lD Number
u.E. Stato ID
PhoneF.
7. Transporter 2 ComPanY Name US EPA ID8.
9. Designated Facility Name and Site Address
U.S. Pollutloo & Control, Inc.
Grassv3 l[iL6s t
10. US EPA lD Number
lfr8l.n oce
3.
No.
12.
1 1 . us DoT Description (ln cluding Proper Shipping Name, Hazatd class and lD Number)
F005, F0o3
F002
I
llazardous Waste Solid, N.O.S.
ORI{.E NA9189
a.
b.
c.
d
K. Handting Codes lor Wastos Listed Above
181/STR
J. Additional oescriptions tor Materials Lisled Above
A. GI,189-2C29-89
1.,47726
Gloves, goggles, and Protective clothlng wlth a resplrator.
'15, Special Handling lnstructions and Additional lnlormation
abovea16dascribed byandcoilenlsth6thisolacarralolyrhatcon99nment,ullydeclaraCERTIFICATON:herebyGE'{EAATOR'S lorcoadiliooA'Bano allin bytransport highwayandmarked,lab€led.fospecls prop6randnam€classilied.at6 packed,shiopingproper
nalionaland EOV€'nmonl regulalions.inl6rnationalappticabletoaccording bethetohaveoeterminodwast€ot loinreducevolumothe clegre€general€danclrhalahawloricilyPogramplaceaamquailitygeneraloicanily th6minimizes andtoavailaDlewhichpreseilmeololmolhoddisposalcunenllylrealmenl.th6thalandselectadhave practicaDle storago,practicablogcoriomically and s6lectminimi26wasl6madohav€a 6tlorl generalionmylatthi,a small gooclamthoandoR.envrronmenl;quantrly goneralo(threatfulure human hoalth
tha besl wasre mana06ment marhod that is availablo lo mo and lhal I can aflotd.
E
N
E
B
A
T
o
B
Month Day Yeer
a4L
Montlr Yeet
of Materials2of18.- - -'- Moilh Day Yeat
T
RA
Ns
Po
RT
E
R
Name
'if:f/Z^q'91itrliJw {qs L *r(
receipt ot hazardous matenals cowred by thts mantfest as notecl in ltem 19.Owner or20.Month Day Ydat
FAc
ILIrY Printed/TyPed
ol ,or use on olito (1
styte FI5REV-6 IJBELMASTER, Oiy. ol AMEFEA| |JEELMAFIK CO.. CHCAGO. lL 60646
.)Form Appovod. OMB No. 2050-0039. Erpres 930-9,
OBIGINAL.AETUPiIT TO GSNEPATCA
EPA Fom 87OO-22 (Rcv. 9'88) Ptess odilDns ar. obsol6t3.
to'n Aqprc,vact. OMe t/p..20il4o39. &p,r!s 9.10'9,
Pleaso o, tyP6.tor usa on olilo
E
t{
E
B
A
T
o
F
T
RAlts
Po
RT
E
R
UNIFORM HAZARDOUS
WASTE MANIFEST
r. Oenerarors US EPA lD No. B3Lltfit"t", *o.
ulrlolololsLolel r I sls lzlol ol tl el a
2. Pagal
loll
lnlormation in the shaded areas
is not rgquired by Fedoral law.
3. Generato/s Nam6 and Mailing Address Thlokol corporatlonP.0. Box 689 lfls 301Brlghao Clty, UT 84302-0689
4. Generato/sPhono( 801 )863-62
A. Stato Manilest Document Number
B. State Generatols lD
7. T.anspofiet2 Nam6 L US EPA lD Numberttrlrltlllrl
G. State Transponer's lD
O. Tramporto/sPhone /ROl\ r\L-)O(r(
E. Slate Transporte/s lD
F. Traneporte/s Phone
9. Dosionated Facility Namo and Site AddtessU.SI Pollution & Control, Inc.Grassv Mountain Faclllty3 Mlles East 7 l'l11es Noith off Exlt
10. US EPA lD Number
Clive, UT l$?r t, lg lq I r lgloltlzl+la
G. Stale Faciliys lD
H. Facilit/s Phone
[phone]
1 1 . us.DoT D e*riolion (lnclucting tuoryr shipPing Name, Hazad class and lD Number)
rFfi
13.TotalOuantity
14.
UnitWWoI
t.Wasto No.
a.
llazardous l{aste So1ld, N.0.S.
ORM-E NA9189 rloh dr i nlslnla P
F005, F003,
F002
b.
lt tlrl
c.
lr I rtll
d.
I rlll
J. Additional DescriPtions lor Materials Listed Above
Ao GtlB9-2029.89 Htr3toP K. Handling Codes for Wastes Usled Above
rRrlsrB.
15. Special Handling lnstructions and Additional lnlormation
Gloves, goggles, and Protecttve clothlng tlth a resPlrator.
J6 aeNenson's cERTlFlcATlol{: I herEbv declaro thal llro coilents ol this consignmeil ar6 ,ully and accuralely dsscribed abovo by
pioper shipping namo and ata classitied' packad'marked. and lab6lod, aftl ajo in all tospecls in prope, conoilion lor transport by h8hway
according to apPlicable inletnational and naliorlal go{,6mmaot ,egulalioos.
l, I arn a large quantity generalo..I csrtfy thd I have a Progtam in Placo lo reouco lhe volumo and torElly ol waslB genetalod lo $e degreo I have de|efmined to bt
ocono,nically ptaclicable and lhal I har6 seleclod tha ffacricable mothod ol treatmeil' slorage'or disposal airreilly available to me whacfi minimi26s lh6 ptassd and
,uturo lnreal.ro human healh and lha e,nvironm6ilt oR, il I am a small quadlly goneralot, I have mado a good lailh 6rlorr to rnintmize my wasts g6n€ra$on and solgct
lh6 bOSl wasle mana9em6nl merhod lhat is available to me ancl lhal I can arlord.
Month Day YearName
17 1 of o, Materials
Month Year
18. Transporter o, Receipt of Materials
Printedflypod Name 6ignature Month Day
I
Year
FAcILItY
19. Discrepancy lndication Space
20.ot Certitication of o, hazarclous materials covered this manit8st except as noted in ltem 19.
Name Month Ddy
styto F15 REV-6 LAEELM STEB, Oiv. ol At ERICAN [laELnAAl( CO.. CHICAGO' lL 606a6
ORIGINAL.FETI-IRN "N GENEPATOR
EPA Form 87@-22 (Rd. 9-88) PrErrixrs adibn3 8E obsobt .
A UNIFORM HAZARDOUS
WASTE MANIFEST
1. Geneiator's US EPA lD No.Manilest
ulrlololo 7 68
2. Pagel
1ol 1
lnrormation in tho shaded areas
is not required bY Fecleral law.
3. Generato/s Name and Mailing Address Thiokol CorPorationi.o. Box 689 M/s 301siiit", C1ty, t,T 84302-0689
4.EPA lD Numbe,
5.6.
8.US EPA ID7. Transponer 2 CompanY Name
9.Designated Faciliry Namo
U.S. Pollution and Site Address 10. US EPA lD Numbor
&Cootro1,Inc
Gr
3 of 1 I40T
Manil6t Documenl Number
B.ID
rl
C. State Transporle/s ]D
D.Phone
E; Stat6 ID
F.Phonc :': ;'_.-, -- i i'',!... : "
H.
801 4" --' "
ll.USDOTDescription(rncludingProperShippingName'HazardCtassandlDNunber)
a.llazardous Waste Solid, N'0'S'
; ORM-E NA9189
No.
13.' Total
Ouantity
14.Unit
WWoI
clolt dt alalzlslo P
F00z'';'
b.lr rlrl
lt I
c.
d
? qr/?@ -/*J. Addilional DescriPtions lor Materials Lislod Abovo
A. G1789-2029-89
I til
Wastes List6d Above
't5. Special Handling lnstructions and Additonal lntormation
Gloves, goggles, and ProtecLive clothiog with a respirator'
Tn
A
}{3Pont
E
R
CERTIFEATIOI{r hereoy declarg thal lh6 conlontS ol.this consgnm6nl are lully and aCCJralety describ€d abovo by
GE}TERATOR'S all raspects in propef cuEitbn ld lnnspon Dy hrgillrey
shipping name and are c!assrlied.pacrec mark6d.and labeled.and A,o inproper
and natbflal 9Or€rnlnont rogulaliom.accotding lo applicabl6 iilematonel torcity ol wasle g6neratqd lo the d69teo I ha\6 dolo,minod lo b€
ivartaOte- to me whidr manimiz63 lho Pto!€ol and
etiort ro minimiie tny wasa gan€ration atrd s€lect
I largo quanlity g6nefalot I cerlttY thel heve a prog,am in dace lo reduc6 tho volume andamaPracticauem6lhodollr6atm6lrl.slore96,ot disoosal cunsnlly
oconomically p,acticabl€and thal lrava s€bcted tl!maoe good laiththreathumanh6althandtheenvironmdil:oR.il t am e srnall quanlity 96n6rator,havoluturotoatlord,tha be3l waSta manag6m6nl method that is availabla lo rne and thal can
Month Day Year
Printedffyped Namo
I
17. Transportor 1 of B€csipt o, Materials
Day
Name
4,r&^1 Transponer 2 ol of Materials
Signature Month
Pranted/Typod Namo
1 o'u}:"'fi;ry'f;(s-larB l/)
19.20. FacilitY Owner ol receiPt ol hazardous materials coverad this as notecl in ll6m
Signature Month Yeat
FAcIL
ITY
on olit6 Fun Approwc, OMB No. 2050'0039. Exlies 9'j0'9'
(Form dosignad ror
E
N
E
F
A
T
o
R
stylo F15REV-6 IJEELMASTEF. Div. ol AM€FICAN I-ASELMAFX CO ' CITICAGO' lL 606'6
OBIGTNAL.AET'JRIU TC CENEE. TOB
EPA Fsn 87OO'22 (Bd. 9-88) Prwin3 edrrim3 at obsobtt'
ot
H2El
=(,,(FF
SPECIFICATION FOR SHALLOW BORINGS AT YI-225
PROPELI,ANT BURN PITS
SPECIFICATION NO. 503-30L4-90
PREPARED BY:
)"- i'l t.. ('i'ir' (t.'i1i
P. V. HancockEnvironmental Permits andProj ects2 October 1989
CONTENTS
1.0 INSTRUCTIONS TO BIDDERS
1.1 Background
L.2 Scope of Work
1.3 Base Bid
L.4 Alternative to Base Bid
L.5 Qualifications
1.6 Project Schedule
L.7 Bid Evaluation
GENERAL REQUIREMENTS
SHALLOW CORES SAI.{PLES
3.1 General
3.2 Drilling Methodology
3.3 Penetration Rate Log
3.4 Daily Drillers Report
3.5 Sanitary Protection of Core Borings
3.6 SoiI Sanples
3.6.2 Shallow Soil Core Sanples
3.6.2 Background Soil Samples
3.7 Sanpling Procedures
3.8 Sealing the Sample Core Boring
3.9 Site Restoration
2.O
3.0
1.0
1.1
L.2
INSTRUCTIONS TO BIDDERS FOR M-225 SHALLOW SAI,IPLE
BORTNGS
Backqround
Thiokol Corporation operates a hazardous waste openburning facility, identified at yt-225. within Nt-225there are several burning pits where different types ofpropellants, gas generant (sodiuro azide) and propellantingredients are burned. Figure 1 shows the location ofthe pits within the M-225 facility. In past yearspropellant contaminated sdlvents may have contaminatedsurrounding soils. Soil samples were taken L septenber1989 in one area called the Azide Pit. Results aresurnmarized in Table f. Indications are that thesolvent in some areas are at a soil depth of up to 3feet.
Thiokol Corporation will inplement a two phaseinvestigation of the yI-225 area. Phase I isinvestigation, to determine the extent of contaminationat the various burn pits. Phase II will address theactual cleanup and moni.toring of the contamj.nated areaif required. Phase I will be addressed in thisspecification.
Scope of l{ork
A proposal for drilling shallow borings and taking soilsamples at Thiokol Corporation will consist of thefollowing:
1) Three shallow borings of 20 feet located withinthe Azide Pit as selected by Thiokol Corporationproject engineer.
2)Five shallow borings of 10 feet, one each in thesouth pit, composite pit, barrel burn pit,contaminated solvent burn tray area, andbackground sample area. The locations within thepits and background sample area are to be selectedby Thiokol Corporation.
The work to be performed under these speaificationsincludes the furnishing of all labor, material,transportation, tools, supplies, eguipment, andappurtenances, unless hereinafter specificallyexempted, necessary to complete the drilling andsupport the sampling of shallot cores at each site.
t
1.3
r.4
1.5
Base Bid
The contract for the work described in the attached
specification sha1l be a lump sum contract. The bidsLall be for the following, and a price submitted for
borings as specified in Section 3.0. The bid should be
for the total of 110 feet of boring and sample
retrieval. The established guantity of feet is
provided for bid purposes only. If the actual quantity
of Uorings is less than or more than 1L0 feet, the
contract-price shall be rnodified by the owner based on
the unit prices provided by the drilling contractor.
The contrlctor shall provide a unit price for borinq on
a cost per foot basis and for sarnpling on a unit basis.
The bidder must provide a bid base as specified.
Failure to do so will cause the bid to be considered
nonresponsive.
Alternate Bid
Section 3.0 specifies use of a hollow stem auger and
split spoon method for drilling boreholes andrltrieving samples. Alternate methods for drilling and
sample retrievll will be considered and may be bid in
addition to the base bid (Section 1.3).
oualification
Each bidder shall subrnit a Statement of Qualificationsthat includes the following:
1) Two copies of the Statement of Qualifications.
2l In-house capabilities including available
equiprnent and project personnel.
3)Specialized experience and technical competence of
the firm, especially as related work at hazardous
waste sites.
Qualifications of assigned personnel and their
assigned project responsibilities.
Locations where your firn can lega1ly and
logistically provide services on a timely basis.
A list of aII subcontractors to be employed and a
sumnary of the services they will provide.
4)
5)
2
6)
1.6
L.7
2.O
Project Schedule
e project schedule shall be submitted by each bidder.
The schedule will be taken into consideration by the
ouner during the evaluation of bids. It will be
necessary for the successful bidder to satisfy the
Thiokol project engineer of the contractorrs ability to
achieve substantial cornpletion and final completionwithin the tines designated in the bid. Completion ofthe borings is to be within 30 days of notice to
proceed.
Bid Evaluation
The bids will be evaluated on the following basis:
o
o
o
The guoted price of the base bid listed in Section
1.3.
The contractors gualifications (and subcontractorsif applicable) listed in Section 1.5.
The estimated tirne to commencement and completionof work listed in Section 1.6.
GENERAL REQUIREI'{ENTS
The OI{NER shaIl, dt his own expense, obtain a1I
necessary petmits required by law for the execution ofthis work.
The OWNER shall provide land or right-of-way for the
work detailed in these specifications and nake suitableprovisions for ingress and egress. The CONTRACTORshall not enter or occupy with men, tools, equipnent,or material, any ground outside the property of the
OWNER without the written consent of the owner of suchground. other contractors and employees or agents orthe owner may, for all necessary purposes, enter upon
the worlc area and premises used by the coNTRAcToR, andthe CONTRACTOR shall conduct his work so as not to
inpede unnecessarily any work being done by others on
an adjacent to the site.
The work is to be performed with a RCRA designated
hazardous waste treatment site located within Thiokol
Corporation Utah-Based Operations. Accordingly, the
CONTRACTOR must adhere with all general and^job-specific regulations regirding, but not Iimited to,safety, site-access, construction procedures,subcontractors, contractor-company liaison, company
3
3.0
3.1
inspection, deliveries, and site-maintenance. Thisincludes reguired two hour industrial training coursesgiven by Thiokol Corporation to each of thecontractorrs employees.
Al1 work is to be performed in a professional manner
and to the satisfaction of Thiokol's on-siterepresentative.
SHALIOW CORE SAI,IPLES
General
The CONTRACTOR shall drill the shallow cores at thelocation designated by the OWNER. The shallow coreswill be drilled in accordance with thesespecifications; which will conBist of drilling the holein a specified manner to obtain samples.
The CONTRACTOR will be required to supply all tools andappliances necessary to complete the sample collection,except sample containers, which will be supplied by the
OWNER.
The CONTRACTOR will be required to supply all necessarypersonal protection and safety equipment, including butnot limited to: steel toed boots, t1ruek suits, safetyeyeglasses, and PVC, neoprene, or NBR gloves.
The CONTRACTOR will be reguired to provide all tools,derricks, and other machinery and applicance ofwhatever description necessary and adequate for theconpletion of the shallow cores in a workmanlike
manner.
The cores will be protected from contamination. Thewaste materi,als frorn drilling operations shall bedisposed of in a manner approved by the OWNER or hisrepresentative.
If in the opinion of the OWNER or his representative,it is necessary to discontinue work on a core vrhenpartially conpleted, on account of jammed tools, cavingground t ot by reason of negligence on the part of the
CONTRACTOR, then the CONTRACTOR shall immediately startdrilling another core at a nearby location asdesignated by the OWNER or his representative. The
CONTRACTOR sha1l seal off or plug the abandoned coreboring with bentonite.
4
3.2
A11 measurements for depth shall be taken from anestablished point on the surface of the ground at thecore site to the lowest point of the core boring.
Drillino Methodoloqv
A) The core boring shall be by auger nethods (ho1low
stem auger). The diameter of the hole wiII besufficient to sample with a 3-inch diameter
sampling tool (split spoon). The boring sha1l be
such to obtain continuous 18 inch core sections
from the surface to the core depth.
B)A central area will be set up to clean and
decontaminate the drilling rLg, drill tools, bit
and subs, and the sampling equipment, includingthe sanple extruder between each core boring. The
equipment will be steam cleaned to remove thedirt, washed with Alconox soap, and then rinsedwith distilled/deionized (DI) water. A11 washingwill be done over a lined wash pit with washing
disposed of in a manner approved by Thiokol
Environmental Engineerappropriate lining mat
The pit andwill be supplied by
ing.erial
c.
the CoNTRACTOR. The pit will have an approximatecapacity of 2,000 gallons. The OWNER will disposeof all wash waters from the wash pit. Tool jointswill be made up dry or with hydrocarbon freeIubricant, such as trGreen Stuffr, to rninimize
sample contamination. Any lubricant must beapproved by the OWNER before being used at theproject site. Samples of the steam cleaning fluid
and DI wash water will be collected and retainedfor future analysis. Cleaned sampling and
downhole drilling eguiprnent will be stored underplastic until it is transported to the waste site.At the drill site, cleaned eguipnent will be keptoff the ground by storing it on cleaned racks orpallets. Any tools, drilling equipment, otsanpling equipment laying on the ground will beconsidered contarninated and will be cleaned priorto re-use.
Decontamination procedure for drilling rig wilI berepeated before drilling each boring or samplinglocation.
5
3.3
3.4
3.5
3.6
3.6.1
3 ,6.2
Penetration Rate Loq
During the drilling of the ho1e, a time log shall !"kept by the coNTRAaTOR showing the actual penetration
time required to drlll each foot of hole. The types of
bits used in each portion of the hole shall be noted in
this 1og.
Daily Drillerrs Report
During the drilting of the well, a daily, detailed
dritltr,s report shall be maintained and delivered upon
request to the O}0NER or his representative at the
drilling site. The report shall give a completedescription of all soil types encountered, number of
feet aiiffea, number o.f hours on the job, shutdown due
to breakdown, and such pertinent data as requested by
the OWNER or his representative.
Sanitary Protection of Core Borings
At all tines during the progress of the work, the
CONTRACTOR sha}I use reasonable precautions to prevent
either tampering with the core borings or the entrance
of foreign rnaterial into it.
Soil Sanples
Shallow Soil Core Samples
Three shallow borings will be advanced to a depth of 20
feet r.rith samples collected in sptit spoons at two foot
intervals. Locations of the borings shall be as
selected by Thiokol Corporation Project Engineer at
tq-225 ezide Pit. Precise locations will be determined
t'he day of sampling. General bid locations are shown
on Figure 1.
Four shallow borings will be advanced 10 feet with
samples collected in split spoons at two foot
intLrvals. The locations will be one each in the south
pit, composite pit, and barrel burn pit. Precise
locationl witl be determined the day of sampling.
Background Soil Samples
one shallow boring will be advanced to a depth of 10
feet with samples collected in split spoons at two foot
intervals. Location of the boring is illustrated on
Figure 1.
6
3.7
3.8
3.9
D)
Sarnplinq Procedures
In order to collect samples in a manner to rninimize orpreclude contarnination from other sources, the
CONIRACTOR lrill use the following protocol.
A) Use new split-spoon sampler
B) Before each sample:
1. Wash the split spoon sampler with alconox
soap
2. Rinse with tap water
3. Final rinse with deioni.zed water
c)CONTRACTOR will carefully remove soil samples fromsanpling eguipment and transfer sample to cleancontainers supplied by OWNER.
After a split-spoon sarnpler is used in deterrnininglithology and if the sample or parts of the sampleare not saved for future analysis, the sampledmaterial will be disposed of in an approved site
and the equipment recleaned as outlined above.
Sealinq the Sanple Core Boring
After completing the shallow core boring, the
CONTRACTOR shall refill and seal the core boring. Thecore boring will be refilled with bentonite or anothersuitable material as directed by the OWNER or HIS
REPRESENTATIVE.
Site Restoration
CONTRACTOR is responsible for site restoration,including removal of excess materi.als and cleanup ofIitter, wastes, and other debris. At the completion ofborings, the washout pit shall be reclaimed andreturned to original grade. OWNER shall dispose ofliquid wastes, and CONTRACTOR shall dispose of pitliner. A11 naterial remaining on-site at ThiokolCorporation for 60 days after the completion ofborings, shall become the property of ThiokolCorporation.
7
F i gure r I
PRESENT )t-ZE A-RN PtT LAYqJT @ - Sample Polnts
r-.o'ri.O,
o'
\s(rlol11ErO
20'
6^RFEL
@
PIT
r-22:l a,F.clt rL..{I'rf,E
Conror i to
@
r 't
(
Saar..0 aa?c.aa la la.-raa
o
HrG,{ E}trcY Ptt
t
Gra I orl !llo. aa aa a a a ..aaa
L J
I-22|! a.f.Ptr otFrmAo
I
20 FrM.G.Ema6AtEGuttt'rti
o€Tol^rlo.t PIT
xEr, a.! 7? clr.tx LI'I aB.CErlD. arfED fleE \
?o.9 li'T=li3I iAl.Elj li/[=FiLB]l DETtCII0tj LIHITi (,i Fr:ni
TABI.E I
r '4qI .'i.l
lCO
EJ
I 981
10aiU. g
95.6
3{8.8
'! !tI
.1.
0
ifr
t tn .-r'lU. r
f,l,' [,
r,iit
l';.'
|', :i!r,
rf ' 't'
)!:?li. I
iiii
lti T
r'{
1
l,i
IIiTSFO
sAlrr,L
?:
l! ,'lttr r
lt l?ll I I
l,l,r i
tiii
tii T
|i,/ T
Hil
l.l,,I
l
lr/T
Irl,rJ
fl,/T
H/T
il,rI
N/T
I'l,iT
l,li I
t cn
}.!TH T,5PTl]
TUEH: :
ilr
$I{}XANE
IHLOF.
IOIALAI{E
lili PF:0341{f,1
L IHLIF;TFOfiII
uiffi|l
!: II{Cii DIPIH
CI}IIST I IUENT:
c'!F: I 0 iHE
HEIi
?{ iIi[H DIFTH !illllTITUElii: !FY[iDit{i :li!1. :
AiEir.rlii 2
L,l . [tl0IAHE :i.l Sl3IALAlii i
!-fIETHYL PBOPAI{AL :
},iETHYL CHIOF:{)FIIfiII :
CllL'jF,trFOE}i
PUIlLlrl! 0;{ili
:i II,ICH DEPIH
c0ti3T tTuEili:
FYRI IIIIi
ltEt
f,Li i tilil
.!1,i. IitU,ihil:
l.; DI0}lALA}li
:-f;ETi{iL FF:iJFAIIAL
t?: iiiiL il;L0F;0F0Fiti
iriLEi;ui3F:ll
TAIIDE.tr
L r Liii
HiTH
li-
CCl,lCElliF:Aii0ti3 ;i{ ppH
SAI.IPLE FOIIITS
n,i{r3
I
?til
irl
L
LI.JiiT i
li i'T
ltli
HiT
H/t
Ii.ITll, I
l,li i
I'li 1
ti i?Iti r
1
4.j'
.4
L
0
.8
tr)
cl,
L
lt/ D
t'l'7
45,4
4
ll,'I
t:1
lo
ti/t'
tiil
tf ,,n
i,l/t'
liit'
I'li t'
lt/D
lli I
EJ
:?8.qtr
l6l .
11 1
t rtl u-r.
Ii0
t{i D
ll,,D
o1
l, ,,?
ili1
Htl
N/T
I
a
'l
!i
iT
rt
!1
L' ! I_l
H3r'i tLi
r$
-ti
?s
j
og
I
1
li
I
9.5
!.i
4.6
.lrl
lriIn,:U.a
llrtr. -,
Nil
I r?n,, I
N/T
I'ii I
0:
t't ?lIr.!
0.8
l!I r.1
1.0
t.f
ACU. *l
N/I
NiI
lt f ?11., !
Ntl
tjg.5
48[.0
IA
tI
It !
T
I If,ACE
lr/ 0 t{/0
7
t{/D
SAIIFLE
t
H/D
8t,0
re ?lJo I
:
r{iI
H/T
ll/T
il/T
iri I
[/I
il/T
l'l,rI
|t/ T
6
il/I
l{/T
NiT
H/1
r{/I
l,l/1
N/T
!r/1
$
)ui
WT
lr/i
il/T
r{/ T
lr/ I
il/1
ti/T
NiI
6
N/T
lr,?li! |
tt ,ltt! I
It
NiT
lt t?iilt
A
ll l't
ltr t
llrill! I
L! r?,r r I
lt;:
i,ii I
,iJE.6
l,ii c
tn.i.t
B.t
/-r ?9rrt
!!
t_l ,,?l!r I
fi,t !
l.t.rT[, t
NiT
l.!.r T
l! , tlr,, t
iliT
ll;;
HiT
!i,rl
il{,4
li
lir'I
li !I
ACETOIiE
i,4. DIBIAI{Ti,] TIOTALAiIE
!.IiETi{YL PF;F9AI{fll
I,IiTHiL CHL{}F:iI!t}RH
CIiLEfiO:CF:}i
tr
?
E
q?0
,!
L
FftF5A
l,!,,7
fiii
)! ,'"ta, i
ti ,,,
ll,;i
l#i
lt,?It.' i
ll ,?It, ;
I'i/I
H!I
HiI
l{iT
il/T
!li I
N,,T
I'liI
t'l/T
4:88
:? =lisiou
{5i.:
i{5.9
42{, I
lli D
,R
0..(
,fa
HTSPCSAIIPLE
1
tt I alt, I
iliI
li,tI
4
tiil
iliI
l{/I
l{/T
I
ll,!I
l,l/T
NiD
l,l1t
.9
D
J
a
lti
ti,
Ji.
iPTA
?6.5
3si. g
1i'. . ;
I4t1
tiiE
E.i
Iti [i
tiiD !1N
Hit'
ct'L
NiT
NiT
N/T
l'liI
N/T
N/I
I'l/Ill rn,t i 1,,
!i. I
,,,?llr I
ti/I
riilu!EiliFl.'T
YI-225 SOIL SAMPLING PI.AN
APPENDIX TO SPECIFICATION NO. SO3-3014-90
SHALLOW BORINGS AT T,q-225 PROPELI.ANT BURN AREA
27 I{ARCH 1990
Prepared by:P. V. Hancoc , QA/QC Off cerEnvironmental Engineering
{,--'VCo<.,
J.. Slaughter Supervisor
Concurrence:
Environmental Engineering
O]. SITE LOCATION
Samples will be taken from propellant burn trenches locatedwithin the M-225 Burn Grounds and background soil areaoutside of Yl-225 fence. See Figure 1 for sample location.The points are for reference. The actual sample points willbe determined the day samples are taken.
02 SAI.TPLING OB.'ECTIVE
The samples will be analyzed to determine vertical extent ofsuspected soil contamination. This is an appendix toSpecification No. S03-3014-9O, Shallow Borings at yt-225.
03 SAII{PLING EQUIPMENT
L.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
L2.
13.
14.
15.
New split-spoon samplerField bookCertified clean sample bottlesDistilled water
Tape measure
Alconox soap washTap water
Steam cleaner or wash bucket-basinsCleaning brushRubber gloves
Lab labels, sealsCooler, iceStainless steel spatula
ShoveI
Steam cleaned auger rig and tooling
04 SAI{PLING TECHNIQUE
NOTE: For personal safety and to prevent crosscontamination, use new rubber gloves at each sample point
when handling samples and sanpling eguipment.
1. Clear ash and debris atay from sanple point to precludeentry into sample.
Using cleaned split-spoon and auger rig, retrj.eve acontinuous soil sample down to the prescribed depthnoted for the sample points on Figure 1. Every twofeet frorn surface down to reguired depth, a sample ofsoil will be collected into a sample tottle. this willbe accomplished as follows:
A) Carefully split open spoon
B) Measure core to find two foot interval
2
c)Using cleaned stainless steel spatula, remove a
portion of soit at two foot interval to fill
sanple bottle(s).
NOTE: Mininize the breakup and movement of the
soil when removing fron core and placing in samp
bottle to prevent loss of any volatile
constituents.
Seal sanple bottle lid with seal, note sample
location and depth on sample bottle label, and
place in cooter containing ice.
Note soil lithotogY in log book.
D)
E)
F) Scrape the remaining soil out of spoon and leave
in same area as sample Point.
After sample has been taken at two foot interval as
noted above, decontaminate the split spoon, spatula,
and any associated eguipment as follows.
A) Steam clean with alconox soap or scrub with brush
in wash basin or bucket containing alconox soap
and water.
B)Rinse with tap water contained in wash basin or
bucket.
Ie
3
c) Give final rinse with deionized water.
NOTE: Freguently change tap water rinse and
deionized rinse in bucket to prevent buildup
contamination. Containerize aL1 wash and ri
water for future analysis for hazardousconstituents.
of
nse
4 Using the same procedures as above, duplicate sampleswill be taken as follows:
o one at 4 foot interval from first boring in azidepit (A-1)
o One at the 4 foot intenral in the composite pit
The samples will be identified as follows with depth
noted hfter each assigned letter:
o Azide pit rtAtr L,2,3 (e.9., A-1, 4 t )
o High energy - [H[ (e.g., H, 6t)
o composite pit rrcrr
5
Barrel pit rrRrr
Background - ilBrr
Solvent Burn Area [Srr
05 SAI,TPLE DOCI'}IENTATION
The following information must be recorded in the Field
Book:
Date and tine of sampling
Samplerrs name and signature
Location of samples including depth
Type, number, sample number, and seals used on samplebottles
Weather
Texture and color of sarnples
Any other pertinent information
06 A}IALYTICAL PARAMETERS
The soil sarnples will be analyzed by a State certified labon a dry weight basis for the following constituents.
o
o
o
Volatile Organics
Cadmium - EP ToxicityLead - EP ToxicitySilver - EP ToxicityMercury - EP Toxicity
HMXNitroglycerinPerchloratesNitrate
Azide
EPA Method 8240
SW846 Method - 7130
SW846 Method - 7420
SW846 Method - 7760
SW846 Method - 7470
Provided by Lab (HPLC)
Provided by Lab (HPLC)
Provided by Lab
SW846 Method - 92OO
Provided by Lab (HPLC)
07 SAI,IPLE ACCOUNTABILITY AND CUSTODY
Follow procedures found in Hazardous Waste Analysis PIanPart B, Rev A, June 1985. This document detailsreguirements for sample custody and custody seals.
Ilr\O(GIOLNI)
(-'.r'1(l ll.
F igure r I
PRESENT tt-225 BLFN PtT LAYOUT @ - Sanple l'olnts
l-.O'a--ot
.a o'
a.o.
\gtoll?E^O
2(,'
6lRFrEl-c.@PTT
-10 ft.e-ztlt a.ellet r cl.€lr.JP
^eEA
Cooeol I to
,. @--7o f L.
r -l
(
Saa ta.a aa".aaa la la r-raa
. o-1O ft
)
HIGH E}q!3lb P+r
a r{ 3lO. .a aa l l. c.a.a
L )
r.-22S A.nNPtr otermAo
I
20 Ff(xr-aj@
G^ TEq!t'!ttEi
oET(I{Art(I.t PIT
f€r 11.! r? Or.lx LUr rElcErlI}t aleED rlaE \
i i1,,
| (-''i+\| 'i-,lylilrl/; li--li<-i \T_{ d..l?\\\A \\)., t r\r; \n t
ul-\'i .1, y
.Si jE .:+.,_ s1l e
= s3\n \ -$
,_lSt :t-< :
-JJ =.'a,-- P-)(s
;J o "'SHGi .{
siT'i,;: ili1...Y !
-{Q'3-rtt;T$ =-+ 'L- <TdTY
-5y
+{${{ J
:.ir.rl
"X'.uI Ij
\xrIj'qq:
IJ;(t-+
N$,X
. .l
CAx
tn'
{{
{\S.- tA
.fog
-v
3
r'0
0/
"(
$')
66\r-I\t
L
-eo
I
Ir
3
ecl
,xs
)dq
t
\n
I
i
I.
I
i
I
I
J-
\
R
*
{
eq
n
{.s\
d"
;0/
0
o5
\
$
)
..t
vs
\,
{-q
{
ul
sI
D\\
\
3
q'p
Bs
\
{\t
?a
s.i
T6
\
'.1.
\)i\
{,\I
.St\soA
t$\
\\
r
-h:
an
1
tt.
!
e
\
T
I\n
-r
\n
Trt
)
d
\\
s
\
$\tn
l
l^
\n
.
d\xj
-{
+-
h,'
li
j
16I
\,
i/t$
T
+t
]
?p
-t1{)
rl tl$I
.l-)
€,J
:
I
:
U
[t
L\
*\
G
(
$.|.
clc):
()I\a
Y.?I
$.
J
*.(.),
r\
oes
-,,4+
Nt.t
A,
-.i.
l
I
:
,ts6-l
t,
i
l
o(n
1.4
t.
t1
I
!
I
I
IA(n
-lJ
I
I
\)rr
,lrltrii
J' \^:},>-s +)
J('.'
.
0:$i
{)
I
;
,ill
1\(\ l ] ; lln f 3 $, $ K ke{I{*qslr
;i:,ri
^l
;i
i,oo\,
^/t,NF
rl
gq
Nd
i!r
itllooNi f(
NN
ii
I
1.0
el
N
i
I
I
Irl
Ii
i
.Q
I
t'
;lri:i\4..r-!. :r.A .;
{t- iUi,9 i
'2eJ\) ",.l,ti
I:l -s $-?T; -
+:ik .
"-E:b'St {
*t**,:t$: Ddal6l
d64rdei
\o
{
U
i
{$
a
tl
:
06(l")
\hsrhr, Jt Vt
c,,l nl:>$!;
F
o
J-
do)$T(
.q.t
U
r
o5$
3
{}.I.ssl
-'JL I r -'),.U - tl6\i {
IoN
,J :f
$.
U ; s$s i
r:+
t.
{
Jti)s
$ht, eqHEr- r t gsb'uu
<is,l
.
.F
3
a{f\rrlq
A
t*
sE
s.
Nt!q
' \.i(-
t
i-)
i -riITl"itt}l
rl tt
3$
:{qi )rl (\$JI!uqu
+- .\-J\^ ,:'
r {.ji ._lj ,,l'''P sira .{
i. co
J"g
rt lt
$$
?t
i0.r'
cll
l
\I..,v\
{S
rf\
IJ..f,
I
I')
J
d+l
:\\
d
!
II
I
I
I
i
I
I
II
I
!
->.--\\it.-i
E
\,,
v)
\{l'+i
$.All\l
-\d.\'n
iti
:'.'.
r\i
+-
o,
')
p{\+r|f,\
...1
I.J'-
*a{sG.
l-)')'
\,,-ui
5
J,
Jill
b
\>.r.
Jr
i
d,c
Aa'
I
U
u
N{A
sAl2
i
u)
!A
1\
5t$r
<..
.il-
?'i
AY
:
J3tI
\
^illt
i
..l
N
tt.*{
i
N
N\ItJ\,
.igilBi(,
tr-qsz!'-
+
\
r{ .t)l.1::r
k iJ'
d' ff<
.. L.'Jr$ 7,,15;-'1
.>t
.-z -Sr-9- =\[^. A
$sN
:ihzl!-i s'{
| , .1
!. j
P- -.1.t
'J tt
al\
1,, ,'1,,,l
ctx
d>
d())
\Brt*rJtl
11i
AO
i
tJtr
l-,N
ili sE .-t'i
."t
-, I
I
v
rCd
2
-t
I
IdrtrN
fllf,ig
i
lioi .3, ^l\J+o a!^
--lhr+3
' luiff,*l'
*y, : 1,'-pnyi: i, ::;l"l iiii;r'cr.r;,, x :
in'
I
LJi
(:
d'
d
d
{rz\
l^
^lCI
t
s,
I
\
UN
]-
-ejs\:3
i
-J
C)sf
<'
.<\
I
3.'- \ ')J)
\,aclir J.I3
{\L,).lT-l.
.1
a-
t
{tt
$)-
t'l
I
\i
{,rg
t$
I
J
\\t)
)\l9
ss
{
vdtv
J,
{
i
J)L,
i
e,.-)<
LII
l1
.))a,)J
I
JI
I
t
lriVi
Ho2-
\
j
r)
J
ts
{
F
5-)
..
\
5
rS
I
T
i
It
d
I
ln
--
\
f
t
s
Uo\{
*1
J-{
..p
{s
$
$...
!
d
aN
JJI
.LvJ-
i
J-r-\,
,$GJ
+
i
UN
\s
-
\s
U
1
$'\l
*
u,
ri'l:
!s
\',)s
.t:l.iOt rD3ss
JY
-\.i\'\,
I{.'\-
-\v\l
;
t,)!,b.
F
-s\Jt
\l
5
3()
_o'
Ill
{,
i(i
rl+i
I
S
-Jo
I
ITi)
T
(J
'll
S\
!l
.lur,
^S'-=.j#it\
\\ i
!I
\\t
UI
!{,j
'f .r
\A
.sr
3
a
-J)\,,
oi+-l.:.-r\
\1
\
'-J i
!
i
!,),
I.n,..i
t^
I
[n
.J:
I
Jll
{
\\
./=
$'l-
rN'-F
.-S
,<t)
(
tJ
't-.i
)
i
I
I
o1
$i
i
l^
Iq,
\
,o
\
I
.>i
Jr;
t/A
-iIJJ,3!P6-si
g:\
(\a
- ,1,
(n
,- [,..
.'1
I,/1
rl
I
I
t;
\
NUlr
*
$
,)t
t
tA
I
i
I
,1N
,.^
--l
;
Vt1
ltri\i
-s) IJJ,
0i
I'tr
!,
s(n
I
\.
-l{
(nr
JlI'r
.c{
i
$
.E
I
!
I
-\)
tn,
!
(J
a
,
:-)
Itrrs
I
I
arl Is,
c\.1iiqi
vt1
t\\n,,I
i
I
t/)
L-t
tJ
b(s
'{
Jss+t
{.,
(:
H
ud
$
i.:
,irl
;!(\ $.J\
I+{,
i
I
Isll
i!
rl
$a ot lJ,
' u
-li ri l:-.-,\$qt
s
I
' ..Ffr#., klt# '1'Taciit<n'_*rr'**,Uffi.ry.l.* .ffi
LOG OF
B NO.
HoLE ELEvAT I o r&zauzzzR I G/DR I LL ER
DATE/TIME {-zz- 7o 4tqflp,
HOLE LOCATION C,q.rrz?,y'ztzz,/r7
GROUNO WATER OBSERVATIONS
WATER I€VEL ./ -/-
OATE ,/zl
TlME
SOIL DESCRIPTION ANO DRILLING CONDITIONS
OEPTH TO BE
OEPTH TO CAVE
PVC CASING (OEPTH/OIAM)
ar
a
N NON
S SLIGHTTY
'J
. MODERATELY
H HIGHLY
V. VERY
CAL. CALIFORNIA
SS. SPLIT SPOON
ST SHELBY TUBE
D. DISTUBBED BULK
P PITCHER
DEPTH sort
SYMBOTTOFROM
?2
9-sc
s79
''Uz^rry' -9z2.7r czt<.; Za.alsr /?'i
/72 /qL
,,L/
at>
OT}TERGRAOINGPLAST|C.,coNolrroNMOETUREFIRMNESS
TYPE o
o.Eoa
u,oar
o(J
Jg,
.lci
Go
o(_,'o)
=fou,I
t9I
olr,
zu,2ulo
Ju
E
?)(
E
G
ID
too
ao
o
o
sotL
SYM.
c6
at6t u,a
lrolr,=c
oc
I
lrtt
2.u,A
9dei80
oqJi8r!lr,z
I
t?ot,
=
DEPTH
TO
roP
(FEETI
BrOW
COUNT
C-,l ?zL9-S .*k x2?'*!1^'/ /r rD.{K ,7/9 t,9.19 s?Y x kar-)/fq?)./9 z9s h.tty',1 t t .)<xcP-Qc,:Va9t lKgt w 4xYv-/n??/f4 L|e coz F Y xxD2;t1t.7 'rl)L59 -frP x
///ci:Eat o x xYkIIt/9'7 zts<CI?Vx*'tss s?-fc t(Mtt
.r4.?-k l7'4'tc x
BOTTOM HOLE OEPTH 2
9, aair9 r !raJLra Lrt t artvttattsrt I iL Lrtur,t!Lntrr9
a446 Wesr 't730 Sourh t P.O. Box nl77 I Salr Lake City. Urah 8,rr30 , Phone: (80t) 974-554a I Fax: (80r) 972{789
LOG OF nOte 14 - T JOB NAME /? 'r.f -zza *aza./ c pAcE / oF l-
. BNO DRILL;NG METHOD Zr.rz rry ENGTNEER
HOLE ELEVATIO v t[*u,r/'
'.?)V,+ Z2 za GROUND WATER OBSERVATIONSRIG/DBILLER
DATE/TIME 4-zz- 2a /2!ra
HOLE LOCATION o,77fuA,/Z
WATER LEVEL
OATE -.7-z
TIME
N NON
S SLIGHTLY
M, MODERATELY
H HIGHLY
V. VERY
SOIL DESCRIPTION ANO ORITLING CONDITIONS
TO BEDROCX
OEPTH TO CAVE
PVC CASING (DEPTH/DIAM)
3
c
CAL'CALIFORNIA
SS. SPLIT SPOON
ST SHELBY TUBE
O. DISTURBED BULI(
P PITCHER
OEPTH SOIL
SYMBOLFROMTO
27
a,
l?v
9,
cy'-sc/(7
9.*.az-.* -i-< u/,/ /Z .Xlt2, q,
Z/57 ?.a?
MOISTURE FIRMNESS GRADING PlASttC coNortror{OTHEROEPTH
TO
TOP
(FEET)
BLOW
COUNT
TYPE
SAMPLE
sotL
SYM.
Go
Fo6
=
Fu,i oo =c
oG
I
lro
zUJo-
9d;3,,o ia u,zq
:,oir,:
u,oc
oo
l!
c(!,
co
oo io)
:fotr,
=
IoI
ou,Fzlt,
=uto
CTu,G,
o
GL
F
tr
ai
Ioo
6
o
o(roA
o
oxYl^;2,//29 -,3s'9/7 Y
.l ,?,2t/9 Lss <F )x x ,rx,lr24Rvre?4,4 L9s S/LDt-tEz !P zts ,P x x r
a2t.i-'z ]4hf?L;5 Sd?v k x
**,ti/q*l-lz?z'1</-,fc.\-Y k
w v/?e Lq9 5/v v
X .t-LEq x kSPYItri,/,?x
Yv/t<,Yt 9"*Vsf x 6f,I ?
:3.V4
EOTTOM HOLE DEPTH
4446Wesr 1730south / P.O. Box 30777 I sall Lake citv. ulah 84130 ' Phone: [phone]
',
Fax: (801 ) 972'6769
LOG OF -3 JOB NAME //.//rz-z/ --2q € fa/r;za) r7a,Z ?/rs P^oE / .oF-l-
B NO. oRILLING METHOD ENGINEER
H.LE ELE,ATT9 ylLa"'''' RIG/DRTLLER GROUNO WATER OBSERVATIONS
DATE/TIME /-27- 7a // t72
HOLE LOCATION -(aa/t?az- rs.z 7Z y'27
SOIL OESCRIPTION ANO ORITLING CONDITIONS
2-a
7
arr
ccr
/
N NON
S SLIGHTTY
}J. MOOERATELY
CAL'CALIFORNIA DEPTH TO BEDROCK
SS. SPLIT SPOON
ST SHELBY TUBE
D. DISTURBED BULK
P PITCHER
OEPTH TO CAVE 4.
PVC CASTNG (DEPTH/OIAM)H HIGHLY
V. VERY
l/-WATER LEVEL
OATE 4-
TIME
OEPTH solL
SYMBOLTOFROM
4r?T r//rtz 7 .'A-A SC.zZzut-Z
./a z
?sal't.2 W cagg- tz./.r'.? gz.*az2 dc-ly'a€7a/
2r./ ..t/a-z< / Zs-uyr .bzztz Z-eP-q.,<zar.
.tz / *2zD ,4/.
>7/<.7'C/z-rv Zz.ae /,,/.
OTHERPLASTICcoNofiroilGRADINGMOETUN€FIFMN€SS
oloG,oA
(,
.J
Io
f
og,
2lttu,o
g
ar,G)()
GE
.E
ti
I(Jo
o
oulier '.Y
U'
Z
:lotr,I
[toc
o(J
u,
co
co
oC'
3oJ
=)ou,
=
Fu,,a olr,
:g
oG
7
at
zll,A iZ
TYPE
SAMPL€
sotL
SYM.
Go
F
aD6
=
DEPTH
TO
roP
(FEET)
BLOW
COUNT
11pxLt "tY!74sc e/z9 ,P/ t?,).-/,.)<k kllcl(/9s fl FB?-,lSf/'.2 r) a,,2,,l y',<rrcc -f/a?Vt f-/LLrt 7tCACz*v/a?'/tt 2s9 V?o<,>2"da xx,A.tg29 Snt"v)<7-z x x/q9 ebTs
/v f&-?ktlzx)-<<fAS1 x-r,l^1 /- ,x Kk0rCtxr a?sr f/-sc.le
BOTTOM HOLE OEPTH
11.b
'-i{f,$:-f-':,",: e. r.t,e . L.leL.t e.r t .,}!a!?t!Lr! I A5 L r! 9 I rt L L n r'! I
Wesr1730Sourtr j-p.O.Box30777, Salt Lake Ciri.'U[ar,E l3O, Phone: (8Ot) 971-554t I Fax: [phone]
HaLE E JoB NAME P^cE / oF -/--
,?.+<-
HOLE ELEVATION- RIG/DRILLER ,Z GROUND WATER OBSERVAIIONS
DATE/TIME -2-
HOLE LOCATION y'P
SOIL DESCRIPTION AND DBITLING CONOITIONS
//
1L
CAL'CAI.IFOFNlA OEPTH TO BEOROCK
LOG OF
,B NO
N NON
S SLIGHTLY
IJl. MOOERATETY
H ,FIIGHLY
V. VERY
. -J" 'lt
ct
((I(
SS. SPTIT SPOON
ST SHELBY TUBE
D. DISTURBEO BULK
P PITCHER
OEPTH TO CAVE
PVC CASING
WATER LEVEL
DATE
.Z
TIME
DEPTH SOIL
SYMBOIFROMTO
/d-rr727
:7 9?,lt1L {A **o'f6rtr/,ttc-o A.(&t)- t'A-
ir? ezrlt#{ 7tlL/,42
I
'1,6t &l/l/,t-
OTHERPLAS'IC coNDrtroNGRADINGFIAMNESS
Io?
olr,Fzu,
=u,o
Juc
3)(
E
ar
all
Iooo
ofoaoA
o
IJ
'I
t
ou,I
ltoG
otJ
u,
E(!}
aro
o(-)
,o)
t2oit:o6
o.E
I
lD
z
UJo-
ed-6i
,c,
?,rer!ar,zE
sotL
SYM.
(r6
ar,
6
=
u,*
DEPTH
TO
TOP
(FEETI
BLOW
COUNT
rYPE
SAMPLE
x rV,n/lt(9f-v x1?L<5
*,ll't/t4{<71C Ytr7arq9
,a,tl za rC7Y/lll.L x2"allv-,I ?xYYlt 15 ar <t 3p-a,
YxIx,a/L<E <r'loL tl II
BOTTOM HOLE OEPTH
44a6 West 1730 south
CHRISTENSET ENVIBONM ENTAT ENGIT{EERING
/ p.O. Box mi7 t Sett Lake City, Utah 84130 , Phone: [phone] t Fax: (801)
'*.
9726769
GOF
-oB DRILLING METHOD
HOLE ELEVATIOXhT ar lrZ RIG/DBILLER
DATE/TIME
HOLE LOCATION r Zza*fzay' -,2cr
HoLF 5 JbB NAME P^GE I OF /
2\77*/24
GROUN
GINEER
D WATER OBSEBVATTONSI
WATER LEVEL /
OATE
'-4
TIME
tlar'a€/7 z 7/r
SOIL DESCRIPTION AND ORITLING CONOITIONS
CAL. CALIFORNIA
SS. SPTIT SPOON
ST. SHELBY TUBE
D. DISTURBED BULK
P.PITCHER
C
6,?*tza
Oa
DEPTH TO BEDROCK
DEPTH TO CAVE
PVC CASTNG (OEPTH/OIAM)
t(2/22
l^r
4 t+, /
tru
ccu
N NON
S SLIGHTLY
IJ, MOOERATELY
H HIGHLY
V. VERY
DEPTH solL
SYMBOLFROMTO
Drtaerl - Z;.?z-, - ..4zrr€/ ,/OOSa .paazz_ 6.<aadZF/-*
r.a )e
l2
-CtLitt a.t)e)/2
r<.t/ ctz r I
CAt c1a72
q,-fA Sc
*1Lo
OTHERcoNorTroNGRADTNGPLASTICMOISTUB€FIBMNESS
/If
oUJFzt
=gJo
fur
?)(
E G,F6
Ioo
ao
tt,ocoa.
C'
o
a;
lr,
z_
=lot!I
UJltG
o(_)
)lrJ
Ecl
(co)oo
io)
:)ou,
=
ar,6t
FUJa
Fgoai =g
E
oarr
Brn
2UJo-
ed
3'1,o
6UJi8*t,
n'
BLOW
courur
TYPE
SAMPLE
SOIL
SYM.
Go
DEPTH
TO
TOP
(FEET)
Y\,n rDxa*dta9Y/q*Lss 6P frt{.kYxY"?"ct ;/-*Y2?rrr.,/./-,p r,(Yt1Lats9-*I )PKl*tkq>L93 k
I x1'/..'t^t k 0n/kLartcs(/-5'c7?s/g?
5'
BOTTOM HOLE OEPTH ,/a
ra. ^! s..9r.asL..r.t9
44a6 West 1730South I P.O. Box 30177 t Sall Lake Caly. Ulah 8'.130 , Phone: (801) 97a'5541 t Fax; (801) 972'6769
LOG OF HOL F JOB NAME ,r4-z-z- e ,aa,z)22rc P^GE / .oF/-
Eha:--
H9LE ELEvATto y LtrDr< t ,' n RIG/DRILLER L GROUNO WATER OBSERVATIONS
DATE/TIME
i 2a ,"*r
HOLE LOCATION fl-ltf _ fZz ,/Z.f f
SOIL DESCRTPTION ANO OFILLING CONDTTIONS
I
c!
a(!t
N NON
S SLIGHTTY
lr, MooERAIELY
CAL' CALIFORNIA OEPTH TO BEDROCK
SS. SPLIT SPOON
ST SH€LBY TUBE
D. OISTURBED BULI(
P PITCHER
oEPTH TO qAVE
PVC CASTNG (O€PTH/DIAM)H HIGHLY
V. VERY
WATER LEVEL t./-
OATE
.4-4
TIME
OEPTH sotL
SYMBOLFROMTO
a9.79
9lz I f.,c'rraz..: 1a,€,se.e /.€ y'tt 4/'
A.e2. Oa,zsz r.,.,/ 6,eetcts 7a ,4
a
/02
OTH€RGR^DINC PLAS'IC coNotttoraMOISTUREFIRMNESS
o
otroA
o
.J
Go
o.J
io)
=)ou,,
IoI
orl,Fzu,
=u,o
ctu,c,
.o
(lL
F
co
,(,o
o
o
CT
I
ttF
zu,A
9d;3lr(J ia U'
Z
2?oll,I
u,6E
oo
t!
aro
SOIL
SYM.
co
art6t u,3
goo =cr
OEPTH
ro
TOP
(FEET)
BLOW
COUNT
TYPE
SAMPLE
tY;/r',v a 7xxa<<9P x27q/,
I x x t l))62<xs"ss SPq2
^Y0P^t 1ZxSPKx72{tr L9'
02-,//d,2\.el (lrr,1/55
BOTTOM HOTE OEPTH
a446 We3t 1730 sourh / P.o. Box 307t7 t Salr Lake caty. Urah 84130 ' Phone: [phone] I Fax: 1801t 9726769
LOG OF HOL tr JOB NAME 1 ,z-zzcfl '- pAcE/ .oF/-
B NO. oRTLL|NG METHOD zzlr'-
''' ? - O446*G|NEER
HOLE ELEVATTON Mn- a 2/f Rlc/DRtLLEg C.,sarzztzz.GROUNO WATER OBSERVATIONS
DATE/TIME /- z( -7o zt z-{e^.,
H9LE LocATroN f a -z - s.az ,22;r -
WATER LEVEL
OATE .4-
TIME ..4
SOIt OESCRIPTION AND OFITLING CONOITIONS
v
,>
DEPTH TO
OEPTH TO CAVE
PvC CASTNG (OEPTH/OIAM)
?
o.q.?
!u
ctuc
N NON
S SLIGHTLY
IJl. MOOERATEIY
H HIGHLY
V; VERY
CAL'CALIFORNIA
SS. SPLIT SPOON
ST SHELBY TUBE
O. OISTURBED BULK
P PITCHER
DEPTH sotL
SYMBOLFROMTO
,a-T
S/zz
ZL
<?75
Z,
1Z/q?
It
t
PLASTIC coNor?roN OTH€RMOISTUREFIRMNESSGR^DING
I
Io?
oulFzu,:L,(J
ft)rl)(
E c
6
xoo
d
o,oaron
o
at
sorL
SYM.
(E6
o6t u,.
Fuoat =c
oar
I
I.6tr
zu,o.
9d;3,o
n,igi8*!.lr,,ZE
:)ou,:
u,o.E
oo
lr,
.Eo
aro
oC)
io)
2)ou,
=
OEPTH
ro
TOP
(FEET)
BLOW
COUNI
TYPE
SAMPLE
zhzJrul c z?s 9?\a)o/tlg itit 7neg *z x
9?Ir4kLqt
t?/3 5P
.,7 /:^ /,-Gq9 x
9
BOTTOM HOLE OEPTH
i '0446 West 1 730South I P.O. Box filtl I Salt Lahe C.ly. Utah 81130 , Phone: (801) 97a-551a t Far': [phone]
Loc oF ^;dil' v@u+ JoB NAME
BNO DRIILING METHOO(h.
,oc, / .or-/-
INEER f^-
GROUNO WAT€R OBSERVATIONSHOLE ELEYATIOXEPAI T. -RIG/DRILLER
i oarE/TIME 2 / !/d
HOLE LOCATION
6t/z,r?22 L
WATER LEVEL /
DATE %
TIME /rtr
,.
t
I
t
I
l,t/
CAL. CALIFORNIA
SS. SPLIT SPOON
ST SHELBY TUBE
O. DISTUFBEO BULK
P. PIICHER
SOIL OESCRIPTION ANO DRILLING CONOITIONS
o /rat
&,
. OEPTH TO
OEPTH TO CAVE
PVC CASING (OEPTH/DIAM}
Ni
,J
H
v
NON
SLIGHTLY
. MOOERATELY
HIGHLY
VERY
44
OEPTH solL
SYMEOtTOFROM
cq>
or't
CL7,9->
OTHERPLASTICcoNorTroNGRAOINGMOIS'UR€FIFMN€SS
o,ocroA
o
IJ
tro)o.J
io)
2
oL'!
III
ou,Fzlt
=u,()
oIUarfFo
arE
.EFo
I(Jo
o
fr
iE lr,Z
t2oUJ:
ltoc
oo
)l!
.Eo
Foa
=
Flt.oar,
=g
o
TE
I
lro
zlr,6-
ed
3'3,,o
TYPE
SAMPLE
sotL
SYM.
.Eo
DEPTH
TO
TOP
(FEET)
.BLOW
COUNT
?rffi,Y iy /C/a/z/-x(P-1r \.vzt'g<.19 {x D l)12 v YLt5Yx'29 :./=.t-r xCD-Ct l, ut^/xKxx, a"gszL v I xL,02.x Y'l 9s CL
!.o,Op,tkz(3s c(K>9
=./- /5J70
I
ts
BOTTOM HOL€ DEPTH ,/o7
I
Yr-,.2a. a
. RTIERGREEN NrArfl[rcAr,, rNC.
4036 Youngfie1d l{treht lLi.dge, cO(303r42s-602t 80033
SAI.TPLB IOC STTSET
/.r/r''r
Cl.ient Project tAirbil.t *Custody Seal ???Con intact?
Saropled Received -a-- '-9
Ilolding Ti-ne .r-,/o '- ? O
coc ?Report Due Tags ?Client ProJect *Sample TagsClient P.O. *Custodian,,e/,-963-.?.f36 DatePhone *Fax *Fax Results?Shipping ChargesSpecial Instrrrctions
Irab
ID*Rr
x
)H
I
-z4fi./3
ClientID*/|n",.n ...AnalYsis Ntx Brt Ioc Pile */Date
8- ).E Xfl ASrAES t 4t/Ttf27E *CLOI
E? r oX C/. Pb. la. la I I 2/il rlE"n 6II//I
qa
I
6
I
)IJ/o v
)/l--q e /6 oz,
it. /ul
/0l
I /2
t4
/L
/t
JO
i-J )
/
/o
v
/)
.1,/T v ^v {,t,*Sanples to be
*d g*/ 6s/,8rr"//...r.,3y. g?gas' d6a7
tc
0,lJ.tlo
{t
(,
F{..{
lq
(,
s
F{lJE
xrJ
I
uar{
o
>1FI(,c4
t6'
Ec$otr
-oA
orJ
oor.{ola
GIaI
+
aH
(t
o.H
\\
+\9
->rl\t\i
h
+
t
\s \S O!\\\s\{\S\\s \\G+
->\
n
t
+.sl
t
\\
\\
s s
ft
sl
a
\
--h.-(\--G.lI\^-al!h,-i\*S-r\^\r\-ils\-
[l-I ItTT r
rT_
tT__l
\R
rD*ID*Analysis Ntx BtI Le Fil'e *lDat-e'Rr
o2..o u tl
4
!az
Il
III
II
II
IIIIIIilIIIIIIIIII
il
IIIII
*Samples to' Ui returzred
ID*ID*Analysis Ntx BtJ Loc File *lDaBe Rr
I
)l
772.r#
?oz,i/, n.?a/dp&f4r??Vl n gt/^D .cittttta74A-s't
q
6
//I
/0
/A
lo /q
//,
/y5/3 \lJo
A-/ J
I 4
6
I
(/n
/t
/4
/t
/t
l/ 4D
?q JI4
/A
I
//
,t
1 t /,yr/0 /
IIrrilIrilililIIIl
rIrr
Il
II
IIIII
IIII rIt
*Sanples to' bL returzred,
rD+Analysis Utx Brl Loc,FiIe f/Date RrID*
)t
.L
?-9 /oz.b/1l/O,1 9lA .we*tt4a45fr,frtI
4
b
,)
I r
/0
\/qD
p' )
4
/7 t
7
7
H')
4
tr
t,/0
t-3'J
4ff tl/tJ,,t7 t 6
*Sanp!'es to' Ui retilr'Ded
COMPANY
ADDRESS
P.O. #6*q
CONTACT ?o^7 lL Euergreen Analytical, Inc.
PHoNE 9.2-Qs;+9 A 4036 Younglield
Wheal Ridge. Colorado 80033
(303) 425-602r
FAX [phone]AIJT. CONTACT
PROJECT #/NAME
SAMPLERS: (Signature)
No.of
Con-tafrieit.REMARKS
I
Sta.No.Date Time f;
!,rt Station Loaation
4stqo Awt x s"2, 4, b.'9. lo Y
?[.q atr*O A rvt I i, t ;)t )l "t D,i ,3 *7 I
A-2 .1-2t4D Prw Y i):i:?b;\,b lo*io^q5 10 x
A-t Zt-'t:l-$12nr,X ai t't'i ,i i n',r',i i^'. i'; o\(/o Y,
B Au \Z. q.1..9. tO s ,k4-\e9c)
4^b-4rt Lurt I\t1,lo l* tL, zo t?. Q : ,87 Y
A-z 4-zt-Qo 9a A l\ t4,to, t z,z,q.C,B,A Xu Zo, k fn xA-l a-zz -Qo ?m x 8 to.LZ 14 lA t^ u 4nfiz /o xt t " t
I
IIIIII
II
a.
. Relinquished by:
Relinquished by:
Relin rhed by:
( signature )
( signature )
( signature )
V Date/Time $r;l fl, q0 l?Atcl-Rec' d by:
Date/Tim" @aec,d by:
1
,./Time -f- /'?)Recrd by:#"//
COI'IPANY
ADDRESS
P.O. #
CONTACT ?a^1 +k^^ rorL Euergreen Analytical, Inc.
PTIONE *6-- q I A 4036 Younglield
Wh6at Ridge, Colorado 80033
(303! 425-6021
FAX [phone]A[JI. CONTACT
a
Relinquished by: (signhture)Date/Tlm e tf r; lV ?a. t ^'I Rec I d by :
Date/rim e frft ilqO 14t tlrftec ' d by :
[ 'Tirne -f-/- ?2 ' Rec r d by:
'Relinquished by: (signature
PROJECT #/NAT"IE
SAMPLERS: (Signature)tal
e7L
n
No.of
Con-
REMARKS
Sta.No.Date Time f;
aIr'Station lrocatLonsq2e -qD x st z' 4.G' . G'. to's-X
C 426-qo ,(C' 2'. 4', 6' , *' /o' ti;I
A X
R 4ob4(1 ?vvt x A 2.4 /o s. lo -f Xll+2Jt-qO Pwt x A'. ,/ 4,b. n to f X
rtz l.-z'? rio ltm K A3:6 . z .4 ,7 Ystl-u-qo A/A {5 X
L *'Zt-qa 7rt k
-lr.'a'
.' /c'b X
K tl-%-4t ?m (Lqt 5 X
H 4-2"-4s ?rA *le'5 X
r] 7,tl 'Z'?-1;A ,L,r /3 X
I
,
..k_
Eelinr hed by: (signature)*ri
CHRISITNSEN BOYTES CORPOBArION
FN( T"AllslflssloN sHEEr
NUI(BER oF PAGES (INCLUDING covER sngED'-f'--
,/ortDATB:/1
TO:/f-LE /S ,/
Ftoulz
FROM:
(r\??4cr(
€ tz? r/rD tUG
CHRISTENSEN BON.ES CORPON^TION
4446 V/EST 1730 soum
P.O. BOX $m
sAlT II\I(E Clfi, uT 8{130
(801) 974.rt14. PHoNE
[phone] - FN( #
" t.a.aartll0latt.tta.atlt?rat' laaatalto ttalaaaal.'t""
lar,;lsl ttr r r I r,t.3a rttt tttfaalaa i l. I ttl ar I Itta aaltaaltttl't
Pqe t olt
Loioled of center 'of etidt Pit
nio*Ao ol tW o! drill tnte: Not nnta7r,d'
Elsaolittt ol grfinn wata: Not entouot*ed'
.llo. A-1r"est BorLngProi
1/27/so
ect225MITldoko
-s8II45-02lYo.,IobCEE trill,iaqInters,tateqrlwhilled.metlPdustng lollorut-stcm iltger
lagged W R.Y' naenca
Well ComPletionSPI Rcsults (utowr/ft)
50 t00
oauA
Ec,a
(l,c,od(r)
=D escriP tion
5SP
with dePth
den5c,ediurn poorl vrnmoist,brownLight teredscotonditt3ithlfsondfinegrodedbrownorkdmoximum,inch4to3/grovcl
SP-
sc
densa,grodedmoist,poodvGreeoish-groy,
teredscotondsiltctoy,withfincsond sshetlfossil1n4qo:troPodtoch,/grovels red-brownscdimcrtts,evilleBonnLoke
oxido stoins 15SPfinedensegrodcdpoorlvmoist,brown,Light 54.1lenstsilcloysilt.Brown vwithsond 55.feet.otcobbleleet.t 0).to
SP-
SCwith sitt ond cloY. Red-brown
densc of 19.0 feet
v
oxide stolns.
No well
instcllcd
thru it.
CBC Erwi'ro Engtneenng
Poge I of I
Uiilea ot eost sildz ol azi'dt Pit
ii"tbo" ol to? ol clritl hote: Not tamteged'
Elatotiott ol grenn uotet Not e*ou'ntered'
A-2Test Boring rVo.ProiTlvi,okol
1/27/e0
tec522M
-38II45-02itto.,lobCED MtwInterstotebgqrlnri;lled nd,hnd,us,vng hollau-stan oilge?
Logged W R'Y' Chapnt'wrl
Well ComPletionSPT Results (Otows/ft)
50 100
!,0,4
tsU)
tlt
c)tlt
=DescriP tion
5
SP/4
den S€,medium poodymoist,vrnbroLlgh scottereddonsiltwithdsonefingroded
moximuminch3togrovels
SPdcnse,grodedvpoorlmoist,shGreeni -qrot,ossilFcloondsiltv.withsondcfin oxidered-brownwithsedimenteBonncvill
15
stoined
2A
SP
/4
finegrodeddense,poorlYGroverymoist,t,toondgrovelsscotteredwithsiltsond silwithleonGrocloymoximum.inch l,1
No well
instolled
Eottom of Test Boring
CBC Emiro Err'gine enng
\.
CEE lob No. 45-02t1-38
m*a otu 4/27/90 bY Intctstote M'lh4
usfiq trlllottt-slern (rugff motlwd
Logged W R.ll' ChaYnmt
Pqe I oll
Loiated. at stulh sid'e of ozffu ?if
itevntinl. o! tW o! drill holc: Not wrueyed
Elwetiott ol grotnd ualtt: Not etuounlned'
il0. A-sTest B oringProiectM-225
Well ComPletionSPT Results (ltows/ft)
50 100
q,o,(,o-acBU'
V,(J
aJ'tDescription
5SP
dapth
fineloosegrodedvrnoist,poorlbrown,Light to3tercdt9COondgrovelsiltwithso.ld withdenserbecominoximum,fn Iinch3/8
10
SPfinescgrodeddengoorlYoist,mbrown,Dork sgrovelondscotteredsiltwithsond
to3 inch moximum
SCsondafinpoorlydenso,grodedGrqrnoist,Y,with teredscot grovelsondsiltwithcloy
to11 moxlmum
15SC&oy, moist. dcnse,
with silt ond cloY,
poorly groded fine sond
fostil gmtroPods
No well
instolled
SC
20
Brown, moi3t, dense, poorly groded fine . .
sond with silt ond cloy, redish-bro-wn oxide
sioins. Silty cloy ioyer 18'0 to 1E'2 leet
Mdium PlosticitY
C Erwiro Engineenng
CEE Job No. 45-0211-38
Drilled, on a/27/90 by tntastotc Mllitt4
tsing tnllau-stcnl o14e" rrluttwd
Logged W RU. Ctu,Tnon
Pogc I ol I
Located of bukgrund' bot:ing
Elantirln ol tdP ol Mtt hote: Not suntqcd
Etantiort ol gtoud ttater: Not uuauntqed
Boring .,itlo. BProiect225Thi,okol M-
Wall ComPletionSPT Results (btowr/ft)tha,-4
h 50 100
q)o,.ao
1r1.)Descrip tion
SPTopsoil, fine, brown,moist silty sond
with orgonics
5
SP-
SC
Brown, moist, densc,
sond, cloy ond silt w
poorly grodcd fine
ith scottercd grovel
to 1/4 inch
ML&eenish-9roy. moist dense silt
with rond ond cloY
10
No well
instolled
SPLight brown,
groded fine
:hclls, Lckc
moist, very dense, Poorly
sond with silt, blockY-snoil
Bonneville sediments
CBC Erwiro Engtneertng
ss.E
q)
a)
^lt\.<-)UsE{
ot-'el3s
F*I
(-)I
c.9oa-
Eo(J
o
=
-!,?;o3E
oa,lz.=
N
o
=o.o
0t
3i)rl,(E
F(LLn
I
-=jJo -..,1o-
_=
=*-
=
satduros
)rr}(raar) qNao
$a Jc)$u's"'s'n *a
J!o
o
orta,o
oa)a
>o(J
'0co
(rl
c==
Ef
.Exo
E
olrU
(,
.E
o
\
-:(CU<toru5
5s8'taci'io-oG!.:a
-'oE<,
tE Ul+CC'5.i eb,' ol-ri! o-'o -e. oEEe
o-c >o.9(,5.J(JOD
Co'.=
a\.C
C)a()a
EE
BS
IE
*:os=€i:o,
}E E
B;TE t bbbB ,r e
- t .3.S
F3 S E
llrb
d!s6ctS
.spdF*nb
ii$soqt I rr\3v3FS:i
d i'3 .il s Fe€r 3tHt s\iQ hl
U
ots
Ot
€oq
+r(,
o)'a
La.
\oc\rc\l
I
=o*lo.d
;ctsr
O!^)t-.E
q)
o)
E=l
at-'c)es
ELI
()I
oo
orn
.A:}oo
tl
JorUG
Fo-tl
salduo5
in)
(L
an(L
a's'3's'n
oG'F
Eo
o@
-!,6o
=-oogDz. .g
c.9
ru
ct-
Eo(J
t0
=
ll
-c
'iocoalt
il,c
vl
,1,cm
oovl.
{,F.q
g.
.(,
'l,oo.s
EoJ
c{,ort,
oall6
o(,
-c=;
(u
Ulco!
E.46€)ot!,, S>3
E c.tl\.E-xeEo
-c(,
.E
rto\.sm
o.9{,<l sl<,.aib,e
:\ gt
O'r,ooo-b
9,6
8,H.;.1'ao-E5..;cj}roocu(tco(/,
Co'*-
o_.C
()a
CIO
E}
BS
EE
*:s*;S iji- s
FE 5
H b,E
$s g
-4bbbt c (-tlE
F3 E E
C,re
ti 1,A€
€EBst-obA)
BE B 6
s3$ BO('! I t
$RS;d+3.{I S BS€E 3tHt ts(rQ *l
E
c;
=Er
Eoq
+aut
G)St
oq)'a
La,
\oq\r
q\r
IE
I
.,
CEE Job No. 45-0211-88
Mlbd on 4/26/90 by Intrslate Drilling
usiile llo/f,an..stclln q.7 mctlud
Logged W R.Y. Ch,aynst
Pogc I ol I
Locoted ol bartel Yit
Eleuottott ol top of erill lute: Not wneged
Eleuctisn ol gtqurd uoltr: Not mcountcted
st Boring No. R5 ProiectM-
SP't Results (otows/ft)
50 100
t,Q)a-
Ecf,
6Li
U75
qt
o)
D escrip tion
SP
silt. SiltY clov
medium'sond
fine dsondenmoist,poodSE,v groded&oy,
o 1 4 feetotlenswith0
2.o fcct04ot,t
Red
5CLDork groy, stiff m oist. leon cloy
Well ComPlction
No well
instotlcd
SP
with
mt,9ro otrl'10silt.m ch 0yersondcoqu3/8
ot 1 0 fcetbrownredishTurns05.feet.
r0SPBrown, moigt, vcrY densa, PoorlY
sond with silt. Scottered grovels to
groded finc
11 inchcs moximum
llit solid object ot 2.5 fcct'
4.0 fcet to lomPlo
Hole movcd 3 feet wert ond odvonced to
CBC Enairo Engtneeri,ng
, -- -o lti J:' i6
Bottom of Test Boring
Poge I ol t
Loidca ot solPenl bonrel Pit-ttevotzrn o! toP ol itrilt holc: Not rwvqed
Elalrrtirm ol groulltt ueler. Nol eatouttted
50.Test BortngProicte2521T
-38t45-021ItloCEEJob bilktglnterstotewo',1 4/26/90Mllcd method,i$tng lwllw-stmt @tgo
Logged, W R'll' ChaPnnt
Wdl ComPlctionSPT Rcsults (btowr/ft)
50 100
q,CI tn0,
CLE(,V,
o
C)a
=Description
GPgroded
6P-
6C
poorly groded
cloy
m dense,oist,Brown-9roY,
ond sittwithsondvgrovel
SP-
SMsond with silt ond
m vI
scottered grovel
ond cloygondsittywithgrovclgroded
No well
instolied
cRC Enairo Englneenng
EVERGREEN ANAIYTICAI, INC.
4036 Youngfield St. Wheat Ridge, C0 80033(303) 425-602t
INORGANIC ANALYSIS DATA SHEET
Date Sampled
Date Received
Date Prepared
Date Analyzed
04 /26 /90
05 /0L/90
05 /04 /90
05 / L5 /90
Client Projecttab Project S
Method
Basis
vi-225
77 65
sw-846 , 13 10
EP TOXCITY
Lab Sample
Number
x20614 H-10
x206 15 A3-2
x206 16 A3-4
Client
Sample Number
RCRAElement Matrix Concentration Units timits(ne/L)
Cadmium
Lead
MercurySilver
Cadmium
LeadIlercurySiIver
Cadmiumtead
MercurySilver
Cadmium
Lead
MercurySilver
SoilSoilSoilSoil
SoilSoiISoilSoiI
SoiISoilSoiISoil
SoiISoilSoilSoil
1
5
0.2
5
01
4
002
02
<0
<0
<0
<0
1
50.2
5
01<0
<0
<0
<0
1
5
0.2
5
1
5
0.2
5
01
4
002
02
<0
<0
<0
<0
mg
mg
mg
mg
mg
/L
/L/L/L
/L
/L
/L
/L
/L
/L/L
.4 mg.002 mg.02 mg
<0
<0
<0
<0
.01
.4.002
.02
mg
mg
mg
x206t7 A3-6
Note: Results are reported on the leachate from the
EP TOX extraction. Concentrations determined by
method of standard additions using one addition.
k
ng/L
ng/L
ng/L
ng,/L
m,E, /L
Approved Quali Assurance Officer
EVERGREEN ANALYTICAL, INC.
4036 Youngfield St. Wheat Ridge, C0 80033(303) 425-6021
INORGANIC ANALYSIS DATA SHEET
Date SampledDate ReceivedDate Prepared
Date Analyzed
Lab Sample ClientNumber Samp1e Numberx20594 S-2
Element Matrix Concentration Units
04 /26 /90
05 /0L/90
05 /04 /90
05 /L5 /90
CIient ProjectLab Project S
Method
Basis
Yl-225
77 65
sI^I-846 , 13 10
EP TOXCITY
<0
<0
. 002 nC/L.02 ne/L
RCRALimits(ne/L)
0.2
5
x20595 S-4
x20596 S-6
x20597 S-8
x20598 S- 10
x20599 C-2
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Mercury
S i lver SoilSoil
Soil
Soi ISoilSoil
SoilSoiISoilSoil
SoilSoilSoilSoil
SoilSoilSoilSoil
SoilSoiISoil
Soi I
SoiISoiI
SoiLSoil
1
5
0.2
5
(0
<0
<0
<0
1
5
0.2
5
/L
/L
/L/L
1
5
0.2
5
1
5
0.2
5
01
4
002
02
<0
<0
<0
<0
1
5
4.2
5
<0.01
<0.4
<0.002
<0.02
1
5
0.2
5
<0
<0
<0
<0
.01
.4
. 002
.02
<0.01
<0.4
< 0. 002<0.02
ng /Lng/L
ng /Lng/L
ne/L
ng/Lne/Lne/L
ng/L
ng/Lng/L
ng, /L
mg
mg
mg
mg
<0.01
< 0. 4
< 0. 002<0.02
ne /L
ng,/L
ng/L
ne/L
ng/L
ng/L
ng/L
ng/L
x20600 c-4
Note: Results are reported on the leachate from the
EP TOX extraction. Concentrations determined by
method of standard additions using one addition.
/,
01
4
002
02
Approved Quali
,l
Assurance Officer
EVERGREEN ANALYTICAL, INC.
4036 younsrieilrll fffi:Brlidse, c0 80038
INORGANIC ANALYSIS DATA SHEET
Lab Sample
Number
Client
Sample Number
Date Sampled
Date Received
Date Prepared
Date Analyzed
04 /26 /90
05 /0t/90
05 /04 /90
05 / L5 /90
Element
Cadmium
Lead
MereurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Client ProjectLab Project $
Method
Basis
t7-225
77 65
sw-846 , 13 10
EP TOXCITY
RCRAMatrix Concentration Units Limits
(lll,e,/L)
rt-i 1r)(J IISoilSoil
Soi I
SoilSoilSoilSoiI 02
x20588 A-1 10
x20589 A-1 L2
x20590 A-1 t4
x20591 A-1 16
x20592 A-1 18
x20593 A-1 4D
1
5
0.2
5
01
4
002
(0.
<0.
<0.
< 0.
1
50.2
5
/L
/L/L
mg
mg
mg
01
4
002
<0
<0
<0
<0
1
5
0.2
5
1
5
0.2
5
<0
<0
<0
<0
1
50.2
5
02
ng/L
ne /L
ne /Lnc/L
ng/L
SoilSoilSoiISoiI
SoilSoilSoilSoil
SoilSoilSoil
Soi I
SoilSoil
Soi I
Soi I
.002
.02
.01
.4
.002
.02
0. 01
<0.4
< 0. 002
<0.02
ng/Lng/L
ng/L
ng/L
ng/L
liJ,g/L
ng/L
ng/L
m.g/L
ng /L
ng /Lne/L
<0
<0
<0
<0
01
4
1
50.2
5
1
5
/L/L
/L
/L
/L/L
<0
<0
<0
<0
.01 mg.4 mg.002 mg.02 mg
X20594 S-2 Cadmium Soil < 0. 01Lead Soil < 0.4Note: Results are reported on the Ieachate from the
EP TOX extraction. Concentrations determined by
method of standard additions using one addition.
mg
mg
Approved ity Assurance Officer
EVERGREEN ANALYTICAL, INC.
4036 youngfietirli
Xffi:Brlidse, c0 80033
INORGANIC ANALYSIS DATA SHEET
Date Sampled
Date Received
Date Prepared
Date Analyzed
tab Sample ClientNumber Sample Numberx2058L A-2 16
Element Matrix Concentration Units
04 /26 /90
05 ,/0 1i3 0
05 /04 /90
05 /L5 /90
Client Project
Lab Frs,js*t f
Method
Basis
Yt-225
77 B1
shl-846 , 13 10
EP TOXCITY
< 0. 002 ng/L
< 0. 02 nE/L
RCRALimits(ne/L)
4.2
5
x20582 A-2 18
x20583 A-2 20
x20584 A-1 2
x20585 A- 1 4
x20586 A-1 6
Mercury
S i lver SoilSoil
SoiI
Soi ISoilSoiI
SoilSoilSoilSoil
SoilSoiISoilSoil
SoilSoilSoil
Soi I
SoilSoilSoilSoil
SoilSoilSoilSoil
Cadmium
Lead
MercurySilver
Cadmium
Lead
Mercury
S ilver
Cadmium
Lead
MercurySilver
Cadmium
tead
MergurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
<0.01
1
5
0.2
5
nI,E/L
ng/L
ne/L
ne/L
<0.01
< 0. 4
< 0. 002
<0.02
1
5
0.2
5
<0
<0
<0
<0
1
5
0.2
5
<0
<0
<0
1
5
0.2
5
<0.01
< 0.4
< 0.002
< 0. 02
1
5
0.2
5
<0
<0
<0
<0
1
5
0.2
5
/L
/L
/L
/L
.01
.4
.002
.02
ne/L
ng/L
ng/L
ne/L
ng/L
ng/L
ne /Lne/L
ng/L
ng/L
ng/L
ng/L
ng /Lne/L
ng/L
Ifll.g/L
.4
.002
.02
.01
.4.002
.02
x20587 A-1 8
Note: Results are reported on the leachate from the
EP TC)X extraction. Concentrations determined by
method of standard additions using one addition.
01
4
002
02
<0
<0
<0
<0
mg
mg
mg
mg
{ut
Approved Iity Assurance Officer
EVERGREEN ANALYTICAL, INC.
4036 Youngfield St. Wheat Ridge, C0 80033(303) 425-802t
INORGANIC ANALYSIS DATA SHEET
Date Sampled
Date ReceivedDate PreparedDate Analyzed
04 /26 /90
05 /0L/90
05 /04 /90
05 / t5 /90
CIient Project
Lab Proiect S
Method
Basis
t(-225
77 85
sw-846,1310
EP TOXCITY
Lab Sample
Number
Client
Samp1e Number
RCRAElement Matrix Concentration Units Limits
(Ixr,s,/L)
x20575 A-2 4
x20576 A-2 6
x20577 A-2 I
x20578 A-2 10
x20579 A-2 L2
x20580 A-2 t4
Cadmium
Lead
MercurySilver
Cadmium
tead
MercurySi-lver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Cadmium
tead
MercurySilver
Cadmium
Lead
MercurySilver
SoilSoilSoilSoiI
SoilSoilSoilSoil
SoilSoilSoiISoil
SoiISoilSoiISoil
SoilSoilSoiISoil
SoilSoil
So11Soil
0. 03
<0.4
< 0. 002
<0.02
0.002
< 0. 02
ng/L
NE/L
ne/L
NE/L
If,.e/L
ng/L
'I|,g/LIf,g/L
ne/L
r,c/L
ng/L
ng/L
01
4
002
02
(0
<0
<0
<0
1
5
0.2
5
1
5
0.2
5
01
4
002
02
0
<0
<0
<0
1
E.
0.2
5
/L
/L
/L
/L
1
50.2
5
1
5
0.2
5
mg
mg
mg
mg
<0.01
<0.4
1
5
1
5
ng /Lng/L
0.2
5
.01 mg.4 mg.002 ms.02 mg
mg.4 mg.002 mg.02 mg
/L
/L
/L
/L
/L
/L
/L
/L
01
<0
<0
<0
<0
<0
<0
<0
<0
X2058 t A-2 16 Cadmium Soil < 0. 01Lead Suril < 0. 4Note: Results are reported on the leachate from the
EP TOX extraction. Concentrations determined by
method of standard additions using one addition.
l,l
k-_
Approved Qual Assurance Officer
EVERGREEN ANALYTICAT, INC.
4036 Youngfield St. Wheat Ridge, C0 80033(303) 425-602r
INORGANIC ANALYSIS DATA SHEET
Date SampledDate ReceivedDate Prepared
Date Analyzed
Lab Sample ClientNumber Sample Numberx20558 A-3 10
04 /26 /90
05 /0L /90
05 /04 /90
05 /t5 /90
Client Proiect
Lab Project f
Method
Basis
Soil
SoilSoilSoilSoil
11-225
77 65
sl^l-846 , 13 10
EP TOXCITY
Element Matrix Concentration Units
Soi.1MercurySilver mg
mg
<0
<0
002
02
/L
/L
ng /Lng/L
ng /Lng/L
RCRALimitshe/L)0.2
5
x20569 A-3 L2
x20570 A-3 t4
x2057 1 A-3 16
x20572 A-3 18
x20573 A-3 20
x20574 A-2 2
Cadmiurm
Lead
MercurySilver
Cadmium
Lead
Mercury
S ilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
1
5
0.2
5
{0
<0
<0
<0
1
5
0.2
5
<0
<0
<0
<0
1
5
0.2
5
<0
<0
<0
<0
1
5
0.2
5
<0.01
< 0.4
<0.002
<0.02
1
5
0.2
5
1
5
0.2
5
0.0
< 0.4<0.0
< 0. 0
.01
.4
. 002
.02
SoilSoilSoilSoil
SoiISoilSoilSoil
SoilSoilSoilSoil
SoilSoilSoilSoil
SoilSoilSoilSoil
.01
.4
.0a2
.02
/L
/L
/L
/L
/L/L/L
/L
/L/L/L/L
/L
/L/L/L
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
.01
.4
. 002
.02
0.
<0.
<0.
<0.
4
002
02
02
3 ng/L
'flI.c/L02 ne /L2 ng/L
Note: Results are reported on the leachate from the
EP TOX extraction. Coneentrations determined by
method of standard additions using one addition.
/-
Approved QuaI ty Assurance Officer
EVERGIIEEN ANALYT]CAL, INC.4036 Younsriets.Si [H:Srlidse' c0 80033
INORGANIC ANALYSIS DATA SHEET
Lab Sample
Number
Client
Sample Number
Date Sampled
Date Received
Date Prepared
Date Analyzed
04 /26 /90
05 /0t/90
05 /04 /90
05 /t5 /90
Client ProjectLab Projeet S
Method
Basis
: ll-225:7765: SW-846,1310: EP TOXCITY
ng /L
ng/L
ng/L
ne/L
RCRAElement Matrix Concentration Units Limitshe/L)
x20562 B-2
x20563 B-4
x20564 8-6
x20565 B-8
x20566 B-10
x20567 A-3 8
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Soi ISoilSoiISoiI
SoilSoilSoil
So i1
SoilSoilSoiI
Soi I
SoilSoilSoilSoil
SoilSoilSoil
SoiL
SoilSoilSoilSoil
.01 mg.4 mg.002 mg.02 mg
<0
<0
<0
<0
1
5
0.2
5
0. 01
<0.4
< 0. 002
<0.02
1
5
0.2
5
1
5
0.2
5
<0.01
< 0. 4
< 0. 002
< 0. 02
1
5
0.2
5
0
<0
<0
<0
1
5
0.2
5
n,E/L
ng/L
ne/L
ng/L
<0
<0
<0
<0
1
5
0.2
5
ng /L
NE/L
ng /Lng/L
<0
<0
<0
<0
01
4
002
/L/L/L/L
/L/L/L/L
/L/L
/L
/L
mg
mg
mg
mg
mg
mg
mg
mg
02
.01
.4
.002
.02
.01
.4
. 002
.02
X20568 A-3 10 Cadmium Soil < 0. 01Lead Soil < 0.4Note: Results are reported on the leachate from the
EP TOX extraction. Concentrations determined by
method of standard additions using one addition.
1
5
NE/L
ng/L
Approved Qua ity Assurance Officer
EVERGREEN ANALYTICAL, INC.
4036 Youngfield St. Wheat Ridge, C0 80033(303) 425-802L
INORGANIC ANALYSIS DATA SHEET
Date Sampled
Date Received
Date Prepared
Date Analyzed
Lab Sample ClientNumber Sample Numberx20607 R-6
04 /26 /90
05 /01/90
05 /04 /90
05 /L5 /90
Client Project
Lab Projeet S
Method
Basis
vl-225
7765
sw-846 , 13 10
EP TOXCITY
Element Matrix Concentration Units RCRALimitsha/L)
0.2
5
Mercury
5 i lver Soil
Soi I
SoilSoil
Soi ISoil
SoiISoiISoil
Soi I
SoiISoilSoiISoil
SoilSoilSoilSoil
SoiISoilSoilSoil
SoilSoilSoil
Soi I
ng/L
ne/L
L *g/L
ng/L02 ng /L2 ne/L
.01 mg.4 mg.002 mg.02 mg
.01 mg.4 mg.002 mg.02 mg
<0.01
< 0. 4
< 0. 002
< 0. 02
002
02
<0
<0
<0.01
<0.4
< 0. 002
x20608 R-8
x20609 R- 10
x20610 H-2
x20611 H-4
x206L2 H-6
x20613 H-8
Cadmium
Lead
Mercury
S ilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
Mercury
S ilver
< 0. 02
1
5
0.2
5
/L/L/L/L
mg
mg
mg
mg
1
5
0.2
5
<0.0
<0.4
<0.0
< 0. 0
1
5
0.2
5
1
5
0.2
5
<0
<0
<0
<0
1
5
0.2
5
<0
<0
<0
<0
1
5
0.2
5
ng /L
nC/L
ng/L
ng/L
<0.01
<0.4
< 0. 002
< 0. 02
/L
/L
/L
/L
/L/L
/L/L
/L
/L
/L
/L
mg
mg
mg
mg
Note: Results are reported on the leachate fr,rm the
EP TCIX extraction. Concentrations determined by
method of standard additions using one addition.
Approved Quali Assurance Officer
EVERGREEN ANALYTICAL, INC.
4036 Youngfield St. Wheat Ridge, C0 80033(303) 425-8021
INORGANIC ANALYSIS DATA SHEET
Date Sampled
Date Received
Date PreparedDate Analyzed
04 /26 /90
05 /0 L /90
05 /04 /90
05 / L5 /90
Client Project
Lab Projeet S
Method
Basis
tl-225
77 65
sw-846 , 13 10
EP TOXCITY
Lab Samp1e
Number
x20501 c-6
x20602 c-8
x20503 c-10
x20604 c-4D
x20605 R-2
x20606 R-4
Client
Sample Number
RCRAElement Matrix Concentration Units Limitsha/L)
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
MercurySilver
Cadmium
Lead
Mercury
S ilver
Cadmium
Lead
MarcurySilver
SoilSoilSoilSoil
SoilSoilSoilSoil
SoiISoilSoilSoil
SoilSoilSoilSoil
SoilSoilSoil
Soi I
SoilSoilExiISoil
.01.4.002
.02
ng /Lng/L
ng/L
n8/L
1
5
0.2
5
<0
<0
<0
<0
1
5
0.2
E.
01
4
002
02
<0
<0
<0
<0
1
5
0.2
5
01
4
002
02
<0
<0
<0
<0
1
50.2
5
01
4
002
02
<0
<0
<0
<0
1
5
0.2
5
01
4
002
AZ
<0(0
<0
<0
1
5
CI. !
5
ne/L
ng/L
na/L
IIi.g/L
ng/L
ng/L
nS/L
r,g/L
'If,e/Lnc/L
ng/L
ng/L
ng/L
ng/L
NE/L
Irl.g/L
<0
<0
r;0
<0
01
4
00r
ng/L
ng/L
ne/L
ng/L
NE iLng/L
02
X20607 R-6 Cadmium Soil { 0. 01Lead Soil < 0.4Note: Results are reported on the leachate from the
EP TOX extraction. Concentrations determined by
method of standard additions using one addition.
1
5
I
L,(4
t1
Approved ity Assurance Officer
E\TERGREEN AI{AIJYTICAL, INC.
4035 Youngfield Street Wheat Ridge, CO 80033(303) 42s-6021
Page 1 of I
Date Received 3
Date Sampled t
Date Prepared 3
Date Analyzed t
s/0L/90
4126-27 /905/07-24/905/07-24/e0
Client ProJect
Lab ProJect No.Matrix
Methods
z 14-225t 7765: Soils See below
B-2 B-4 B.5 B-8 B-10 A-3 8 A-3 10
x20562 x20563 x20s54 x20s5s x20556 x20557 x20558
Client Sample *
Evergreen Sample #
Nitrate-lCr), nglrg
Perchlorate(2), mg/xg
IuoCrt, rng./trg
Nitroglycerin (3), mg/Kg
Sodium Azide('), mg/trg
0.43 0.34 0.84 0.74 <o^20 3.31 5.03
<3.5 <3.5 <3.5 <3.5 <3^5 <3.5 <3.5
<1.0 <1.0 <1.0
I
<1.0 <'l -0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0 <1-0 <1.0
<25.0 <25.0 <25.0 <25.0 <25.0 <)3 .0
<1.0
<25.0
UethodsEEIJbo. o(2!tsg
(3hprc
(nhprc
NOTE: AII results are reported on a dry weight basis.
C r* \-t^fu
Quality Agsurance Officer
EVERGREEN ATIAIJYTICAL, INC.4036 Youngfield Street Wheat Ridge, CO 80033(303) {2s-502r
Page 2 of I
Date ReceivedDate SanpledDate Prepared
Date Analyzed
:5r4r5c5
/0L/90
126-27 /90/07-24/90
/ 07 -24/e0
Client ProJect
Lab ProJect No.Matrix
Uethods
t 14-225z 7765: Soil: See below
Client Sample *
Evergreen Sample #
Nitrate-ICl), urg/Kg
Perchlorate(2), mg./trg
IIIDa(3), mg/trg
Nitroglycerin (3), ng/xg
Sodirur Azide('), ng/trg
A-3 L2 A-3 14 A-3 16 A-3 18 A-3 20 A-2 2 A-2 4
x20569 x20570 x20s71 x20572 X20573 X20574 X2057s
7 .59 5. 10 5.37 5. s4 5. 10 2.88 2-26
<3.5 15.0 12.0 4.90 <3.5 5-01 <3.5
<1.00 <1.00 <1.00 <1.00 <1.00 <l -00 <1.00
<1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <l^00
<25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0
MethodsEpa-loo. o('tsg
(thpt c(nhpt c
NOTE: All regultg are reported on a dry weight basie.
Quality Assurance Officer
E\TERGREEN AI|ALYTTCAL, INC.
4035 Youngfield Street Wheat Ridge, CO 80033(303) 42s-5021
Page 3 of I
Date Received 3
Date Sampled 3Date Prepared 3Date Analyzed :
01/90
26-27 /90
07-24/90
07-24/90
Client ProJect
Lab ProJect No.llatrix
Itlethods
z M-225z 7765r Soil: See below
5/
4/
5/s/
A-2 5
x20575
A-2 I A-2 10 L-2 L2 A-2 14 A-2 15
x20577 X20578 x20580 x20581
A-2 18
x20582
1.17 <0.20 0.78
x20579
L.27 1.35 2.to 2.05
Client Sanple #
Evergreen Sample *
Nitrate-tdr), mg/xg
Perchlorate(2), mg/xg
moC3) , mg/xg
Nitroglycerin (3), mg/rg
Sodium Azide(r), mg/trg
<3.5 <3.5 <3.5 <3.5 4.7L <3.5 7.44
<1.00
<1.00
I'IethodsQEEIToo. o(2tsg
(3hpr,c
({hprc
NOTEI AII results are reported on a dry weight basis.
<1.00 <l -00 <l -00 <1.00 <1.00 <1.00
<1.00 <1.00 <1.00 <1.00 <1.00 <'l ^00
<25.0 <25.0 <25.0 <25 -o <25.0 <25.0 <25.0
ttC fl\.
Quality Aesurance Officer
E\TERGREEN At{AIJyrrCAr" INC.
4036 Youngfield Street t{heat Ridge, CO 80033
(303) 42s-6021
Page 4 of I
Date
Date
Date
Date
Received
Sarrpled
Prepared
Analyzed
5l0L/e0
4/26-27 /905/07-24/90
5/07-24/90
C1ient ProJect
Lab ProJect No.
Dtatrix
Methods
z il-225z 7765
s Soil: See below
Client Sanple *
Evergreen Sample *
Nitrate-ldl), ng/xg
Perchlorate(2) , mg/xg
IilDCt), mg/xg
Nitroglycerin (3), rng/rg
Sodium Azide(r), mg/Kg
A-2 20 A-1 2 A-1 4 A-1 6 A-1 I A-1 r0 A-1 L2
x20583 x20s84 x20585 X20585 X20587 x20 588 x20589
1.67 1.a?0.31 1.35 1.61 0.49 0.34
<3.5 6.19 7 .46 <3.5 7.02 4.87 <3.5
<1.00 <1.oo <1.00 <1.00 <1.oo <1.00 <1.00
<1.00 <1.o0 <1.00 <1.00 <1.00 <1.00 <1.00
<25 -o 448 2L2 62.O tL2 83.0 78 .B
MethodsEEI-5bo. o(2hsg
('hpt'c
('hpt c
NOTE: AII results are rePorted on a drlr weight basis.
ht
Quality Aegurance Officer
E\TERGREEN AIIALYTICAL, INC.4035 Youngfield Street Wheat Ridge, CO 80033(3031 425-602L
Page 5 of 8
Date Received 3Date Sanpled 3
Date Prepared 3Date Analyzed B
s/0L/90
4/26-27 /905/07-24/90
5/07 -24 / 90
Client ProJect
Lab ProJect No.Matrix
Methods
z Dl-225t 7765: SoiI: See below
A-1 14 A-1 16 A-1 18 A-1 4D s-2 s-4 s-6
x20590 x2059r x20592 x20s93 x20594 x20s9s x20595
o^42 0.29 0.49 L.25 7 .23 12.2 l^67
Client Sample #
Evergreen Sample #
Nitrate-ldr), mg/Kg
Perchlorate(2), mg/Kg
HIoCrr, mg/xg
Nitroglycerin (3), mg/rg
Sodiurn Azide(r), ag/xg
5 <3.5 <3.5<3-14.9 17.1 4.37 <3-5
<l -00 <1.00 <1.00 <1.00 9S 7 4.70 <1.00
<1^00 <1.00 <1.00 <1.00 <l -00 <1.00 <1.00
56.2 <2 36.2 154 .0 <25.0 <25.0<28
MethodsEEf--e 3oo. o('tsg
(3hprc
(ohpt c
NOTE: AIl results are reported on a dry weight basis.
C Ary\-(.-^,t?
Quality Aesurance Officer
E\TERGREEN AI|ALYTICAL, rNC.4035 Youngfield Street Tlheat Ridge, CO 80033(303) 42s-6021
Page 5 of I
Date Received rDate Sampled !Date Prepared r
Date Analyzed t
5/0L/90
4/26-27 /90
5/07-24/90
5/07-24/90
Client ProJect
Lab ProJect No.ltatrix
Uethods
z M-225z 7765: Soils See below
s-8 s-10 e-2 c-4 c-5 e-I c-10Client Sarnple *
Evergreen Sanple #
Nitrate-ldl), ng/xg
Perchlorate(z), mg/trg
moCrr , mg/xg
Nitroglycerin (3), ng/rg
Sodium Azide('), mg/xg
x20597 x20598 x2^o 599 x20500 x20501 x20602
lt
x20603
1.46 3.55 5.05 .5 8.90 6.73 L.o7
<3.5 <3.5 12 .8 37 .0 59.8 23.0 a6 2
<1.00 <1.00 **49 .5 2.s4 2.42 <l -0
<1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00
<28 .0 <25.0 <25.0 <25.0 <25 .0 <25.0 <25.0
MethodsPE-pa 3oo, o(2hsg
(3hprc
(ahpt,c
**Peak detected, but below practical quantitation limit.
NOTE: AII results are reported on a dry weight basis.
l
Quality Assurance Off
I
E\IERGREEN ANALYTICAL, INC.4035 Youngfield Street Wheat Ridge, CO 80033(303) 42s-5021
Page 7 of I
Date Received 3
Date Sampled rDate Prepared rDate Analyzed 3
5/0L/90
4/26-27 /905/07-24/90
5/07-24/90
Client ProJect
Lab ProJect No.Matrix
Iulethods
c U-225z 7765: Soil: See below
c-{D R-2 R-5 R-I R-10 H-2
x20604 x2050s x?o 506 x20507 x2 08 x20509 x20510
Client Sample *
Evergreen Sauple *
Nitrate-Id1), mg/Kg
Perchlorate(2), mg/xg
Iildt), mg/xg
Nitroglycerin (3), rng/rg
Sodium Azide(a), mg/trg
11.5 7 .02 0.71 o-7t 2.94 3.30 5.91
24.1 51.6 22.0 7 .58 45 .02?.2 <3-5
5.75 2.2L <1.00 00 <1.00 <1.00<l ^6^57
<1.00 <1.00 <1.00 <1-00 <1.00 <1.00 <l -00
<25 .0 <25.0 <25.0 <25.0 <)q .0 <25.0 <2E .0
MethodsE-pn 3oo. o(2tsE
(3hpt c('hprc
NOTBr AII results are reported on a dry weight basis.
U/7r triJi
Quality Assurance Offl,cer
EIIERGREEN AI{ALYTTCAIJ, rNC.4035 Youngfield Street l{heat Ridge, CO 90033,(303) 42s-6021
Page 8 of 8
Date Received 3Date Sampled 3Date Prepared t
Date Analyzed l
s/ 0u 904/26-27 /905/07-24/90
5/ 07 -24/90
Client ProJecttab ProJect No.ltatrix
Methods
t il-225s 7765: SoiI: See below
Client Sample *
Evergreen Sample *
Nitrate-t{l), urg/Kg
Perchlorate(2), mg/Kg
maCrt , mg/Kg
Nitroglycerin (3), nglKg
Sodium Azide('), mg./trg
H-4 H-6 H-I H-10 A3-2 A3-4 A3-5
x20511 x206L2 x20 613 x20614 x2r)615 x20516 x206t7
6.19 7^52 5.54 'l-57 2-55 2.05 2-86
4.44 <-? ^5 5.51 <3-5 <3.5 <3.5 <-3 -5
6.19 2^55 3.87 9^68 **1.21 <l ^00
<1.00 <l-00 <1.00 <l ^00 <1.00 <1.00 <1^00
<25.0 <25.0 <25.0 <25 .0 <25.0 <)q .0 <25 .0
!!ethodsffibo.o(zhsE('hprc
('hpt c
**Peak detected, but below practical quantitation limit.
NOTEc All results are reported on a dry weight basis.
CJl,rA c*;L
Quallty Aesurance Officer
,.
EVERGREEN AIIALYTICAIJ, INC4035 Younqf ield l{heat -Bidge CO------ (303)425-602L-80033
VOLATILE ORGAI|ICS AI.IALYSIS DATA
:A-'ent S M-225
77 65L24.388260 ( 8240 )SOIL>vl444R8051090
L20s845/0L/904/27 /905lL0/905/ L0/90
L5.3
x2
0
0
0
0
Y
)--teDateDateDa /Prepared
t?Drying
sea Irre
Proiect No.lecf No.fe Dilution
e No.Blank No.
Conc.ttg/Rg
ss on
ta
Compound Name
or
oride
roet v
-2-Pentanone
eneBenzene
lenes
Surrogate Recoveries:
L,2 Dichloroet,hane-d4T5luene-d8Bromofluorobenzene
8""iers a
a
0
hloroethane
zed for not detecare
tionle.
tat trumentumn
ionin
trations and
and sarnple data.-calibrhtion limitVol. 18, Part II,are less than the
Cas Number
"E?k;
7 4-87 -37 4-83-975-01-47s-00-375-09-2
67 -64-L75-15-075-35-4?5-34-3155-50-567 -66-3L07 -06-278-93-3
7 1-55-656-23-575-27 -4108-05-478-87-51005 1-02-579-01-579-00-5
7 L-43-2L24-48-t1006 1-01-5110-75-8?5-25-2108-10-1
59 1-78-579-34-5L27 -L8-4108-88-3108-90-7100-41-4100-42-51330-20-7
15
1
1
1
1
u
U
UU
U
UUu
U
U
UJuuUUUuUuUuUu
U
U
U
U
UJ
U
U
UJ
,000
5,200
300
150
t2
QC Limits
( 70-12 1 )
I 81-117 Iu 4-L2Lt
I ts.
.200'.200'.200'.200'620
,000'620
620620620620620.000'620
620620620620620620620620620620.200'620
.200'.200'620
620620620620620620
1
5
6
L2
c
2 ,
95t89t105t
an
Pr
1i
=
=
J
B
E*
,
t water
stBAts
Un1essquanti BBBi i. 5tf""3l1iot'3,"u.b1e )
UfuI#rrpproveds
on
D Parker
concent basis (NA not
Quality Assurance Officer
c.lIJ
::.i.i'.t
r{)
1.
0)
lr
1-Jo-
-l
l:]
i{\C\I'=f
:t. u\
-{=33n'n
rn,f.,l.
3..:*lul0!L ..111
'f,-- 0
O+ riL,:tt
lI 1-.C-rtrr:l :3 *
PtOc ..7(l-l
i1.3
lL,
,)L,.I ...G
"\ 4-
4
Hr-l,J\ a,l-.'= Z=:!.:'- .J..
.{rj'= ,L:;:i =-r (f.::.. .:, .-. .{ l....-,J :::r,-..f .'. ... ..i-r..,.T,o.= ..1l. i
'f,:'.. '' d A
r< '.' r:'l :n'd -:) ..,= tt J *.
^..1 . ts 'tr:':,'t ,lj,r ';n0l:.rf-0 ) -d:l "'- it: iJ' 'l) rl,I -...'j
d 'l)O ig t.1 !-t-'- +,J- ; i0 .iJ r(.r
AO- E-O
.L.rl
,TI
rl
nr{
,.U
'5,r'l
'sl,s'
OJ
ru'rl
t -$s
.s',l'
t{
f:-9r
Eit
7,-E t
u-6r
l}-rT'rT1'116Gi {l (,
T'l-rf,?Tl
:l
:i
L.
F
Erl
(ir(il(il
,r-rtr
,4,tt.'1t:.1'
rtr' t ',h
6r rn
llr fi'rir '1.'1. ',tt rrj
tgr&
-!
'4,
i1
C:iclC]
!.-1
{i
o
c?'il
'5rt
:f:tn-rt].
Itt
t..
Tutri:,
l:,l-
CIt:C.trr
C.
;it-C|-
('l
rll.:
tf
j'
,ll
EVERGREEN AIIALYTICAL, TNC.4035 Youngfiel4^ _wheat-Brdqe CO 80033- (303) 425-602L-
vor,ArrLB o*sI^68 ANAJ,YSTS REPoRT
iense-dt€DateDa ? ylN
COUPOI'ND
\rridine
rrogate Recoveries:
Toluene-d8
Client Prolect No. 3Lab Pro'lect No. aEffectife Dilution tMethod BMatrix rLab File No. 3Method Blank No. :
coNcag/Kg
ts A-1 2x2058405/0L/9004/27 /9005/ L0/9005/ L0/90
Y
u-2257765L24.388260 t 8240rSOIL>vL444
R8051090
cAs #
110-85-1
89r
not
t ta ion
ts
27 ,000
s
QC Limits
( 81-117 )
limits.
620
t water.is
POL*ugZrg
8""1 ierst.orfare
t
3t
P
toundf
J
B*
,
column.t a concentration outscgncgntrations and PQtbasis.
€s
and sample data.Vol. 1B-, Part ILare leis than the
ide the calibration limits.'s for soils are
t on
a
U1,\4
ot
Approved:
D Parker Quality Assurance Officer
;..c.1
:1.1
=tft-t -{
i{,
-{ -{
I:: ='-i -. -i0:1. o.
a).. p-.oG
FL-EB.- 01
m!(JLC(l)f,n-.rl-:l .;
.-l -.1-
11)c
E:'{
L,.
J!!l-.{
':}:+0r{
C :::'O:'r-{ / :t-
1._ u-.. o..
:l-,:
.r- +
at-lso,3'I r-
- rUrl
Dd
oo-. .. :_r-. !l)
!,i0
ErrE---J
c.lo
ri\:r.i.{
0-
o
tr
4.
_io-uf:]
trof,|3
rI
,=
-4
iC'ia=
:i:. "'
-- =.+....,!
"1.,:. '-.s.G,=.i'. .-.r'':.t
^{t .
:B "t
{D :J r-l
- a.l 'n
LL
o0)Lre'E ,ftOrf-
.J^-L
fd-al
,5r
:'
if'"rl
!-rl
nr(
OJrl
-:
.(,
..,..,
..t
,::, Cn,:i ,:i, $r'r, r:r r3 ,:r c, ,:, rn (i,irJ .lt ? ,l:i !l (rl .l .f
'r?i
ci'
d1
rlr,tt.:i'
'l'5r_jcl
ti
'.:l
u-5t
@clc)',
6l.Sl
ru
6,6l(,'
fl
6t{tt
OJ
Fl
,3
,3
t
F
-l€d
B
&
!Oir.l
Itn
ln
,-f-t
o
h.
E(I(r(!
Cl-C!
t:rtr(i
C
)irt-(:t-
..{-l
fi 'U .U nl r{ r{
E\TERGREIH iilBI[1fitto"'Et' ro o *4035 Youngfiei sos ) 42s_6ozt-
VOLATILE ORGAIIICS N{ALYSIS DATA
ts
--teDate
Loss on
Compound Name
Prepared
t?Drying
oride
we
D Parker
Client, Prolect No.Lab Proiect No.Effectife DilutionllethodMatrixtab File No.Method Blank No.
QC Limits
t70-L2Lr
I 81-117 I
17 4-L2Lt
tg.
,
A-1 4x2058505/oL/9004/27 /9005/ L0/9005/ L0/90Y15
ttL-2257765t24.698250 ( 8240 )SOIL>v1441R8051090
2
2
2
2
2
u2 v
-2-Pentanone
-Tetrachloroethaneloroethene
Xylenes
Surogate Recoveries:
L,2 Dichloroethane-d4T5luene-d8Bromofluorobenzene
t-iers:
an es irnaEPA
Cas Number
for,not detec
€.at ts s
umn.
Conc.ttg/Kg "E?k;
7 4-87 -37 4-83-975-01-475-00-375-09-267 -64-t75-15-075-35-475-34-3156-60-567 -66-3L07 -06-278-93-3
7 1-55-656-23-575-27 -4108-05-478-87 -s1006 L-02-679-01-579-00-5
7 t-43-2L24-48-L1006 1-01-5110-75-875-25-2108-10-1
59 1-78-579-34-5L27 -L8-4108-88-3108-90-7100-41-4100-42-51330-20-7
5r800
Uu
Uu
UJ
Uu
UUu
UJuuu
Uu
UUu
U
Uuu
U
U
U
U
UJ
U
U
Uu
2r500
2
2
2
2ii
L2,
1
65
ulf
2
1
Tr -Trene
UnIessquanti
L2 ,
,
,
t
74
9st88t103r
8""1 t waterJ=
B=E=*=ionin
and sample data.Calibrhti.on limits.Vol. 18, Part II,are IeSs than thea
0 ts
ta on concbasentrationsis. (NA =f;Sg 583i?"5Ei""3ltiot'3,auable )
Quality Assurance Officer
..pproved r
=rf.
=.{
$'a'=
:i:: "
.. ..i.tJ
d.c.:r.t'. ...
:{'..r{
^J,\ .tl '<r
0):iu')- :.r ".-lt:rs.i"L
oiuu!Etf
.T.r .I -tJ - .2-
f{IJ
d.it.i
F{]
1.
!u
lf
-ltr-v)|:)
vc
'[j3
(.,i
ol
f. r'lC,l.r
-t' \,
:4 c4
r0
.l-3
.J
llo-7 --.
:{ :;
:!)7=ll'r
:L -,',L::if ::
: { :t.n.{
-::.3
tll:1.. o.
3.. r,-.iuo.:
L -rf,lF rU
O+ t-lLC'11
'I jn -.g-ttr
Cl "-1-
..,:..
"-LL a"t r:.
:', .Ll -
-r. -J *;l- 'I.lllr-t- i
.tlr]-
mo* "' ,.i-(ltJ- -+,((
TJ"'n-.F --r
ct
il
,.4,rl
1.rl
t:{
ir-5s
f-tl .-.--....-- .. ..- rr=:3
t-ss
i"-:;1"
t--s;
-l
t
rsr
13
'j'Fl
F
t-st -
:,€(.t
qi ':r rliCl rn nli.t r{ r{
F;[a'TrT(ir 'a-,(n .:.('l ,:,1a.r, t:,.J
6'i5l.('
., .3, ,I,:f, ,:rrt .:,
!l,
rl:r'f
-ll.
{l
cr((
(::F(I
rax(-:
C
:it|-
'rTrarl'r-l'r*a t-r'fi
,i ,li Ii ':,1i: lr Ci :i
:f,t)
rr-r'
.t
(.-
EI/ERGREEN ANALYTICAI{, fNC.4036 YoungfieLd- -wtteqt-Bi4ge Co
( 303 t425-602L'
80033
VOLATILE ORGAIIIC AI'IAI',YSIS REPORT_ PAGE 2ent
Prepared
? Y/N
COI,TPOI'ND
Pyridine
rrogate Recoveriega
Toluene-d8
t-
tsan estima v
a CI
Client Prolect No. 3tab Prolect No. 3EfEectife Diluti.on zltethod !Matrix 3Lab FiIe No. ?uethod B1ank No. 3
coNcuglKg
140s85s/0t/904/27 /905/ L0/ 905/ L0/90
s
A-x2
00
0
0
$-225?765r24.69
8260 ( 8240 )SOIL>vl441R8051090Y
PQL*ttglKg
iers:OualO=fox,not
Bta
cAs #
110-86-1
88$
ta estrumenllllll.entration outside the calations-and PQt's for soil
620
QC Limits
( 81-117 )
ibration limits.s are
ted abovedetection reDortinq limits.Iiinits f5r reaqent water.is detected, but i.8
and samole data.Vol. 1B-, Part II,s are leSs than the
25 r 000
L
,-
B=*=al0-
weUnlesquant
E conct bas
concentris.
proved:
J Parker Quality Assurance Officer
a.l;]
r{.l
'{r
F{3
0.r
lr
a
P
lD
+'
Cof
13
t.d'7
,l' -€\ 4J,=
r-l )(.')
\HJt50,l ,J LJ:8... '!.-{
-{,J= a]]}. ='-t ,I=...1 ". 4 ''j,.. ...1d :-_'r.{,lr, ... ".1:l ..
'..1 ,|-{r .. LL C$ -, .. t/{t rl.{irri*.r .rt -) ..oq.t-J e
^.u\.. l*acD.:r ,:trr Ln
o=Ll] Q a
-i.I.-. ..Hr'i;'l.tf,. (l) oiL - ...-la0)
O0)(J !!-P
uEtQ s(0
oo- 1l-ltlO =E -F --.r
OJ
,5'
lU
rO.T
_-t:-\
I'. f,\OFf
-i, d
r-.l .{
nl
6'd
6,(l!
rl
rl
!(irl
trl
f -:;;
(5t,t'\I'r{f-:il
e-gs
t=A
:{ .-{'l1l$ll==.J=,=
ElB.':l\
*oG
EL-!oFo
Ov {JLCO),lc-.
0,f crl-3-
i:,-51C.
F-t-sso
t-sr
f,e
16
lS,'I,,!
,s,
'9
(3
mr:-itflei
ql
.S,(5i
{r
(sl
6.6,,rit
5)++
It(lr
tt(l'(9c,F(t
urC.
c.
fr
f:
rl
"t.:fr.l
0t (dr:Crll .nilO)t(.! ':U r:( CJ rl rl
:-- :'''r':'l
:..:.1
:t r'{
j. J\.0 :::
l];r.c^
:j.. +-
-rlled
L .Etf '- tlt
tO+ r-{- ,: lfr
f0
,:I
.J
:i
.Li;:.-' {l7.'
t^.::
:l
g-i - ..'t.
L'.':,:f::
.1 },.
,. "J ....:.L ;'il i:
^r -t.i -
:': .J -l.- ,n
-.r l- -
!:l.-J..
q.. ,t. .. .:-. rU
L"-+!r tQrl .'' ,E..F-
:
J'..7.{
rU
i-L
ta+'aj
vc
't:
.r
:::
t-
=3
:i. :--'
. ..:l
... :
i.l .; 'r
j. .L --.f-. ..,:{' :{
:r.'.i
,u :: .T.l
- i. (Jlr
I
cru
'' i: !1,'
'i ,! .'^, .1-
il
ii'
$.1rl
.I'rl
4'r{
.].td
rl
.'I,
!
c-';s.---*::
i--,ql ---dc:l
r.-s! ---
I -$t
T-r,I-i.n lt.?n r--.1-r-r'rJ- t 1'T-,.i:Trf ,l-.1r .:i_r C:. :r ,s. ,:i ,:l .,!
'tr a;, Cl :! .rt ,:i ,11 .'rir'ri (r (:r :r ':' .:i. r:' ,:l
't, ,.i, (i :.i ':. ,li ci ,:tirR ,'. ri {i ,' !:a f'J -{
; " :;-r;
!:-!r
J
t,
F
,S,
ftGt
rtl|f!,'-l
0r
e.tl
.:I(t
Ci-
':I
a::t
(:
rit-
.ol
EVERGREEN NIAI,YTICAL, INC.4036 Younsrietg,3ittBlr$iin" co 80033
VOI,ATILE ORGAI{ICS ANATYSIS DATA
M-2257?65L24.698260 ( 8240rSOIL>vL452
RBo5r-090
14D0s935/ 0L/ 904/27 /90
5./ LO / 905/ LO/90
15
A-x2
00
00Y
'ent S e Client Prolect No. 3Lab Proiect No. 3Effectife Dilution 3Method 3Matrix 3Lab FiIe No. 3I{ethod Blank No. :
A
DaDaDa
etete /Prepared
200200200200620000620620620620620620000620620520620620620620620520620620200620200200620620620620620620620
ii
L2,
1
6
5
U
UU
U
U7r300 J
U
U
U
UU3.000 J.U
u
U
Uu
Uu
Uu
U
U
U
UUU
U
U95J
U
U
U85J
7 4-87 -37 4-83-975-0L-475-00-375-09-267 -64-L75-15-075-35-475-34-3156-50-567 -66-3L07-06-278-93-3
7 1-55-556-23-575-27 -4108-0s-4
7 8-87 -51005 L-02-679-01-579-00-5
7 L-43-2L24-48-L1005 1-01-5110-75-875-25-2108-10-1
59 1-7 8-579-34-5L27 -L8-4108-88-3108-90-7100-4 1-4100-42-5L330-20-7
ne
Cas Number
94t84t105t
Conc.ttg/Kg "87*;
t2 ,
t?Percen Loss on Drying
Compound Name
ide
nzene
2
-2-Pentanone
zeneBenzene
lenes
,
,,
QC Linits
t70- 121)I 81-117 Iu 4-t21-t
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-dBBromofluorobenzene
fluali
J=
B=E=*=
Unlesquant
--- proved:
John Parker Quality Assurance Officer
EI/ERGREEN AT.IALYTICAL, INC.4035 Youngfield -efheat nidie e0 80033- (303) 425-602L'
VOI,ATTLE ORGAIIIC ANAI.YSIS REPORTPAGE 214D05935/0L/904/27 /905/ L0/905/L0/90
A-x2
0
0
0
0Y
e
Da
s 1e
eDate
xtract? Y/N
COUPOI'ND
Pyridine
.rogate Recoveries:
Toluene-d8
8"alifiers:
aI0-
E=Unlessquanti
Client Prolect No. z M-2Lab Pro'iec€ No. t 776Effectife Dilution z L24Method z 826Matrix : SOILab F'ile No. : >VlMethod Blank No. : RBO
coNcuglKg
25
5.699(8240)L452s1090
PQl,*ug/KgcAs #
110-85-1
84r
31r000 620
t water.
1S
QC Limits
( 81-117 )
limits.
P
T-
B=*=
on
data.
de the calibrationsoils are limits.s for
C/ff\ A"*L
and samoleVol. 18; Ps are Iess art ILthan the
ao!,
,[pproved
Jo D Parker Quality Assurance Officer
j\:\ i.rr{;.1
"-{ '-l
-t-:.1 :{
-ir ,Jr
.{i :-...--:j:: =f,l :r..,f'
iit .. +'*!UO:._ .. TJOi- 'U
rD +' (j
L 1: tll
'tt tt -ru:r ':,J -f .-
(Il
1l :{
L..
ll- :{
'i- :-l
Q'-{
:l''
rl ::.+ -:1..ll ^'.. tE..
,Y -':!'i- :r ''
-t. - r..
l!OLifr--.,8J]1:l -
fio"- ,, . ---tn0J
-L '' trrf.' t0
1-1 - (l*;- .J
i.l,:l
l.l
r3.'.t
riL
'D
ir
o-
33
I
'B
rl
,:-a,]
=;{
.,..\:4,-
l'3.r
" '' *l
Jr i-i -J.-i ' . ...:]-':{
:}. .it
t:ftn
-ll"'
-t-
oor.l.. ;f ,0,e,i-
_r,- l_
(.u
.i.,
i.!llrl
r'
r,i
'.,.ir{
r{
-r_'rt-r1-1'l' C,:tr,!,:)
--rT.Ef-r
c?,:i,.a
a,
i "..{c
1 T-.-1-J -''r-t T-fTft -r--r-r-r
rl;i (i' {l : I Ct ,.-*r:i {i, C-J El ':r rn.i' (ir c:r :i l' ' ,n
'9I (i, f;, 1J rir ,:i.r1r f.". 1.:. rr! f. il
li-.Et
,r, .,:,
G.'*.
.
llr.
G,\.'-,,
ll,
't'oJ-
Fl
,3,s..
fil
'Sl,3..,
F
rf'n'rl
tlt
E,n
6l
ar(t,:lft
CFfI
uIL
C
:I
F.
t=t
rlnl
EVERGREEN AI.IALYTfCAL, INC.4035 Youngfierd- -wbeet-Brdse co 80033
( 303 | 425-602L-
VOLATILE ORGAI{ICS AI.IALYSfS DATA
ts e
DaDa
-ete
Percent ss act?on Drying
255.38
g( 8240 )
449s1090
160s85s/0L/904/27 /905/ L0/905/ L0 /90
14
A-x2
0
0
0
0Y
Client Pro'iect No. z lt-2Lab Pro'iect No. 3 776Effectife Dilution z L24Method z 826Matrix : SOILab File No. : >V1Method Blank No. : RBO
Conc.rlg/KgCompound Name
hane
ene ChlorideAcsulf
Cas Number
97*90t1088
umn.
POL*ugZKg
,,
,
^s v v
-Met -2-Pen
-D
-DButanonel.-Tric1
,D
1
alifiers I
ta ona
oroethene
ide
oroethane
tanone
hloroethane
-d4
forE areuna
al0-
se
L.200L"200L'.200L'.200'620
12 .000'620
62062062062062012.000'620
620620620620620620620620620620L,200'620
6,2006'.200'620
620620620620620620
UUu
Uu2.800 J.U
uuuuU
U280 J
Uuuuuuuu
UUUU
U
Uu
U95J
U
UU
U
7 4-87 -37 4-83-975-01-47s-00-375-09-2
67 -54-L75-15-075-35-475-34-3155-50-5
67 -66-3L07 -06-278-93-3
7 r.-55-556-23-575-27 -4108-05-478-87 -51005 t-02-679-0t-679-00-5
7 L-43-2L24-48-L1006 r.-01-5r.10-75-875-25-2108-10-159 1-78-579-34-5L27 -L8-4108-88-3108-90-7100-4 1-4100-42-sL330-20-7
,
8"
ue
Benzene
Xylenes
surrogate Recoveries:
L,2 DichloroethaneToluene-d8Bromofluorobenzene
QC Limits
t70-L2LrI 81-117 1
17 4-L2Lt
terJ=
B=E=*=
Unlessquanti noteddry we cgncentrations and POL,s for soils aret basis. (NA = not applicaSle-oi-noE-available)
_ _ roved:
D Parker Quality Assurance Officer
tf,,:r
J
:-\
lJ
L-.o7-
:'.{a
f...1',-{:}
t.
0)
tl_
ta
rJ
Co:3
:JJ
:}.
:tr
11
-E.
:1. :?'r (\
r--i=l:: I
...,'J
:.r i' '+'r.r,=.,'. .q
,-r'. l{
ir. '
1-1 d
tu - .t',<.:1..\r :.{'-f'
^l-
fl il', il+- .:i t't
.i;- r
rl
L_ .Plr{i
F.,1.?rrl
:.iT: ,:u
i'rl
IL,
i-: ,5r
i-r{i
t-
:'-.'L,
t.
ir-u,
!'
;
'r -!'i
6J
'9t
t
1:-:is
'5'.:,
ol
,3
,Sl,.4rl
Gt,al
r{
c-Er
:.: d
.'{ 'l'\
:r. ll
i_ir{
:J1--
)) :a
-1. :'
iL ::
;1. ::
:r.
..lr f1'l:.!
!. I n..l-olllr'-
I
'l:' O
^ ...-1
-d
r,o'!l-a
..-L
l-li:i ----'--'
itr:{
l!:: ---'
- :.- :*''ll:r ,:I.
lll.. p.- ,.1, G.:
L.-r:rl-- (u
r0! tJLcq.!i[ ,ti'-t
-r.J-
7.- C
F
-rr-r..r --r r-J. 1-T-' r r-rr,I'',-1-?-r-'-r Tit
I -!iS
l-:r
-----Fr{..addl:: ::'t-T-a-la--r'
.:,1
_t
Enl
at
I
.S,
Ur
il&
.:|-,I
C;:f
t::
;if-t'
.:i
l:.,
r:;l(i,
t,: !
1.,)
r'l
-.t.-t
..,..
qr
,i.t'
,jt
n.l
:r:I:!!,li
,:ir,:'':'i:,
'i,rr-l
,.i
't,:'I
i:l..it
EI/ERGREEN AI{ALYTICAT, TNC.4035 Youngfield^ ^wheat-Bidqe CO- (303)42s-602L-80033
VOI"ATILE ORGANIC A!{ALYSIS REPORTPAGE 2- tent Sample Numberr Sample- Numberc,e RedeivedDate SamoledPate pxtiactqd/PreparedDate AnalvzedMethanol Extract? Y/N
C1ient Proiect No. rLab Pro'iect, No. 3Effectife Diluti.on 3Method 3Matrix gLab F'i1e No. 3Method Blank No. :
coNcng/Kg
2,800
1605865/ 0L/ 904/2? /90s/Lo/905/L0/90
A-x2
0
0
0
0Y
il-2776L24826sor>v1
RBO
25
5.38
g( 8240 )
449s1090
cottPot ND
Pyridine
rrogate Recoveries:
foluene-d8
t-iers:analvzedlimits for,
an est
EPAf t
umbers
v
n sco umn.
we
cAs #
110-85-1
90t
PQL*uglKg
8""1
620
QC Limits
( 81-117 )
ibration lirnits.s are
?-rJ
B=*=t8
E=UnIes siquantta miseona
at a concentration outside the calcgncentrations and PQL's for soilt basis.
ur^t**,
ca
APProved:
J D Parker Quality Assurance Officer
, .,1
- :f_r
:-l:.'
-L,':l'
.- ,!_. tll
.. . _t-.
': --. :l'
rll r- r.'
t--
-r ..- --
;i
.', ::
1.. . .-
,':
'_ _i
t' ..
I ,_
| ' ii
ri
'r] .-
,!l
...t-..
i ,-ri 1'-.,,
i...,
:t.t
.:r
:L
{i
i
't'
.::
-l .
'l
.:
[+,l'
i-
Tt.,
l- ril
t.Il.
I
I
t-I .r,
l-'-t
i
i,i.ii-.,
..i'l-l
i.
l_.!
I
l- 'i:'
t.
F.
Iri .r,
I
l. :,t
t-
t.
i"
I
1,
t
?t
t
I
1I
- - - -------t
/IIIiI-_t
{
I
Ii
t
--*:.==::-l ,(.
-tu-....:.1::::r:i:-:::: :l:'-\
i
I
I,.1.!
,|)\
II
,l
f i '['rt-r
a
t
,--t-.-,r, i',:1,, t
r:;.
a-'r" -f"r"r'' I
.t
rl:'r-r-r.1. r.-1-, ];
:1
t,
':. 'i;i
,ii
:;,.t,
!,ttlrl
,:'
')t
.:,
,s,
c,
't
i,
t.
L(
:
t
.:
F:i
nl
rn
,il.Irr\l
tr:!
l(r
'1'
.I
i(
.,I
,l
l
80033
VOI,ATILE ORGAIIICS AI{ALYSIS DATA
Cas Number
EVERGREEN AI.IAI,YTICAL, INC.4036 Youngfiel4^ -wlreqt-BlSge cO- ( 303) 42s-602L-
l,l-2257765L24.388260 ( 8240SOIL.>v1451
R8051090
C1ient Prolect No.Lab -Proiect, No.Effectife DilutionMethodMatrixLab File No.Method Blank No.
A-1 Ix2058705/oL/9004/27 /9005/ L0/9005/ L0/90
Y 13.8
.enrSts
-<.tg
Percent Loss on
Compound Name
I
D
D
or
oride
Disulfidehloroethenehloroethane,2-Dichloroetheneormhloroethane
tate
1 3
Prepared
t?Drying
roDroDeneinll Ether
POL*ugZKgConc.ug/Kg
L.2001: 200L"200L"200'620
12 ,000'620
62062062062062012 .000'620
620620520620620620620620620620L.200'620
6.2006"200'620
620620620620620620
U
U
U
UU6,200 J,U
Uu
U
U
U4,700 J
Uuuu
U
UUuuuuu
U
U
U
U67J
U
U
U
U
7-33-91-40-39-24-15-05-44-30-56-36-23-35-63-57-45-47-52-61-60-53-28-11-55-85-20-18-64-58-48-30-71-42-50-7
t
1
,-Tr
lifiers:
caI40-
ta
97*88t105t
not detecforts arean estifiaEPA
t
cose
4
4
5
5
5
7
5
5
5
6
?
7I
1
5
5II
1
9
9
14I
0
5
8
1
9
78-8-0-0-0-
?
7
7
7
7
6
7
7
?15
610
7
7
5
710
71006
7
7
7
L2100611
710597L210101010133
,
,
,
,
LimiQC
2 v
-Met -2-Pentanone
loroethane
zenezene
a Xylenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
ts
t70-L2LrI 81-117 I
l? 4-L2Lt
1 ts.rebutagent waterLa
8"'
le data.tion limits.Part II,s than the
tsEPAtion
at
J
B
E*
concentrations and PQL's for soils aret basis. (NA = not applicable or not available)
(^
we
Unlesquantsi
olfa
Quality Assurance Officer
t
D Parker
on
.-pproved:
.iEl
::.1 il\
::l :}..
:'J .{
:1 -{
.-':: J
iO :r"1.
,J.. r*&a
t:L .-'t:n-- (l]
tls U'i. t: ,l)
!i: j '-r
'-1. J ,:--1 ';-
trl
,:I:l]
.rJ
iI ::
;ri ::--{
::)lI=
'gl ' r'l-:'.
l- ::,T::-4 1':- t'
..:L :.td
..t .rJ ..-,. .J "-l'- rtl
- ;iJ- L- .i--:
&l rll
.- []
i.L. " P.s uJ'l-'J ''r.r
,:.r,J
.l
!(\.t
-{
tl
l1
o-
f,:l
.:
'cf.1
'f,1.
3
:.f
l-:f
.1....
]:ir
" "ri
.,:, .rl J.if ' ".. i . :{
J,...3
lrl:'i
qi -.. .rl
.I
ifl nl f I
r-, ;.: rr]
,1: ,: .-'
..1 .: f
,11
,-ti,l
.,t'.l
-r.rt
.tl
.S,rl
;{r r,.Il n'sr .i5 *-rl,-, r?l-r 1 I;rr al" r1l: -,{,r r r f ilT.},
,: .i;' ,:) ,::, ,4. ,:r (; (ii "i ,:;, I i.
'.-r :r ,:) ,Ll tit :l (:, '.;, rh' ,:j' r!r: ,::' .:l ::, '5, :: c:, (i, !::r i:' rtilr: .::' lrii :::L l(r ir t,-, (.], l!, t:,r tailri la' :; .t :.: (-r '.d ..t r-l
ll-il ------€i-::
t-t;s
l-s
t1- :t.
-----
f .' u,.'
;i-'il
(i.
i::r,.:,
iJ1D
,lr.,
d,q,
ft
Gl
,5:
,9r
F
I
15r
l(t
.-l
t(,
-l
0t
tiol
lIu
f-,:I
!:--,(rI
,:
,:lt.
EVERGREEN ANALYTTCAL, INC.4035 Youngfield Vfheat Ridqe CO 80033' (303) 425-602L'
VOI,ATILE ORGANIC AI{AI,YSIS REPORTPAGE 2'ient S e)tevdtBDaDa ract? Y/N
co!,tPot ND
Plrridine
rrogate Recoveries:
Toluene-d8
t-Lers 3
A-1805875/0t/904/27 /90s/ L0/905/L0/90
x2
0
0
0
0Y
C1ient Pro'iect No.Lab Prolect No.Effectife DilutionMethodMatrixLab File No.Method Blank No.
t{-2776L24826sor>v1
RBO
25
5.38
g( 8240 )
45151090
cAs #
coNcuglKg PQL*ag/Kg
8""1
110-86-1
88r
ullltl .a concentration ide the ca
U 620
QC Limits
( 81-117 )
ibration limits.s are
l-
B=*=al0-tI on
scoatB=Unlesquantsi onsea !r€!cencentrations andt basis.'s for soioutsPQLII
c,?*t.llnproved:
J D Parker Quality Assurance Officer
i'l lt\r
.{ l.( ,\
:.{o.
-{ r{
,:{B
:.{={j.',J.
.i:.:, =J],l' $
l-i .. *'
-0iGl:L..Ifn- 0i
G# UL.:t,
't, .rl '-.
:15-
'liC
'll.-{
d :'{
.:u[L:-l
,+d
rl :{
-:'.
O::':-{ .. l.
.. rIJ ..
I-il-'+ ---i- tr
leo:trL'* fi -ErTfd
rll {l. . .. .,.1d rlt.l-.- p
+' t0'n-lI]
-- F ..i
ial
LJ
::
-.1,J\.f
i-{lI
{.
tlr
It
..t
11+'lD
+'.:
o
_'r.3
,].
:-1.{
!-1.,
,:L'='
It- "'
.r j;l'- r
...-.-d
r-{,t, ".iJ...o ='f '.. .-.
"i ' .. --{
rl'1
lD :: JId:.t'r
-:{:.3,
L!
OIDrJrr i: lri
,r.t,1 d
,Ii.l lI
(u
,1'
d
,T..{
(rrl
,d
r.:.
d
. rfJ
-,.r.
"nfTr,f r fil'-rn.rrn- ^fr
c: ..i, r: r t.r I .,'
c;, (i! rt, t:. , :,e.1 4i 'i' , j!-r (i' lf' ':. til(.J ,,1 *l r.t
nT rt l- i t'tf r tlTr r1'Ttl'arr' l'i r1_t r1-r rta4 ,'i ,t, 'n {.i' ':, lrCn .-'! ,ir ,3 C] .:i ,:i
I--!t
'.,r:;i
II:
':)':i(t
,11
,1r
.Sr'-
n..l
.t'
,r'..i''rl
,tt,:'
otr{
9t,:,'.
ri
6.rlt ,f'rrt ltiIt.ii
trt
ilt(.1'-l...
0r
ent
iI
arJ!l:t-a
Il:t.::
r:Il.
.:r,:r,!l.:,!
.r.,t'
rfr
,11,:l
r:itrf
.,
utrl-
,r:l
EVERGREEN ANALYTTCAL, INC4035 Youngf i.efd wtreat -Bidqe CO- (303)42s-602L-80033
VOI^ATILE ORGANICS ANALYSIS DATA
i-ent Samole Numberr Sample- Numberu,ate RebeivedDate Samoledpate Exttactqd/PreparedDate AnalvzedMethanol Extract?Percent Loss on Drying
Client Proiect No. 3Lab Proiecf No. 3Effectife Dilution 3I'tethod 3Matrix 3Lab File No. 3Method Blank No. 3
Conc.ug/KgCompound Name
hane
oride
ene loride
sulf
,-D oroethene
tanone1-Tric
tate
1
Tr thanezene
t s
t4-225
77 65L.L78260 t 8240rSOIL>vl394RBo50890
A-1 10x2058805/0L/9004/27 /9005/ 08 / 9005/08/90
N 14.9
1
55
4
2
1
Cas Number
4
2
andall.s are
PQL*ug/Kg
t2
L2
4
7 4-87-3
7 4-83-975-01-475-00-375-09-257 -54-L75-15-075-35-475-34-3155-50-5
67 -66-3L07 -06-278-93-3
7 L-55-656-23-575-27 -4r.08-0s-478-87-51006 L-02-679-0L-679-00-s
7 L-43-2124-48-11005 1-01-5110-75-875-25-2108-r.0-159 1-78-679-34-5L27 -L8-4108-88-3r.08-90-71.00-41-4100-42-51330-20-7
I
,
c
2
u
U
U
UJJ
U
U
U
UJ
U
U
u
UU
UUuuu
UuuuuuuuJuuuJ
1
1
1
1
1
,
3
1
20
-D
I
UnIesquant
oroDroDenevin|I Ether
-2-Pentanone
Benzene
Xylenes
lifiers:
ca
thane
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
8"'
94t93t101t
QC Limits
t70-L2LrI 81-117 1u 4-L2Lt
limifor€d,
ts.reaoentbut is waterJ
B
E*ionin
samole data.ibrhtion limit18, Part II,1e5s than thea
0
IL
-pproved:
and POL's fornot applicable or not available)soils areon
D Parker Quality Assurance Officer
S.
:c4ErElt,
1iaB88
:&'3r38
UUBUU
t'BtduuJ
T'UUET]
58r;1BB
48S60
SaAAet
A6BBS
tgbaa
-rrTgt. In,J nHF'nliATClBFAtl
2ed ?6 a-TIC
0
Uata Frle: >UlJ94zz
1 aa 1 ga
14 16
,..t
!D r.)
!a
)AB
Outpr-, Fi le: ^VL394r.Ot
r.l
Itr,6
r1
I4
i
w.It,)tt
81
Narne : ;.{! U9UUllrscz 5i5i5.
Quan t
i(P05/ov/9u;r.].9
tJE tJLlFis
D.1ui0;
NI: UI
d Frrtleast
i.?;'65 i402;0;5;
I
T
L
le: ID_u24::r1.1
i
_
TO- TTLE FUR.fTPhJLNDIXlialrbratron: rUU9UU :14
Uperator ltt:Uuant 1'rnie3l'rr3ected at:
BUd9UU5U?90u509 06.54L6r 45
. EVERGREEN AIIALYTICAL, TNC.4036 Youngfield- wheat-Brdqe CO 80033- (303)42s-602L-
VOI,ATILE ORGAI{ICPAGE ANALYSIS REPORT
2i-enrSt A-1 l-0x2058805/ 0L/ 9004/27 /9005/L2/9005/ L2/90
N
- -ceDateDate t-.ed/ed Prepared
T? Y/N
Client Pro'lect No. z 14-22Lab Pro'lect No. 3 7765Effectife Dilution z L.L7Method z 8260Matrix : SOILLab File No. : >V14Method Blank No. : RB05
coNcuglKg
5
( 8240 )Da
COUPOI'ND cAs #
97L290
PQI,*ug/Kg
Pyridine 1 10-86-1 U 5
rrogate Recoveries:
Toluene-d8
QC Limits
93r ( 81-117 )
OualO=ifiers:abovedetec I ts
rJ
B=*=
s or reaqent water, but isotland samoleVol. 1B', Ps are leSe
data.a
0 trument L art ILthan the
E=Unlequan
coat llIIlIl.concentration outsgntrations and PQLide the cal ibration limits.st concbas 's for soil s are
Cryl\Aoproved:
John Parker Quality Assurance Officer
-ii;i I t-ilj r:HFiHgTiitiFptl
i Is .iiiJ.r? iE ir-::iA tti;= ,--..
4 !-:f E
l(i il-,;::': :, r' i.7r | +il;: : h'r'rii
ntr!:t 'l Pfir:r
i i-t . itlt ; $ ; :: i Ll i l-1I..'1 i'l
I
I
IIi
I
t
I!I
i
I
I
II
I
I
II
I
i
I
I
iI
II
I
I
I
I
!
I
1. b.B l'J eqnB
...-^.-.^.-t: { r;j rt }:r { v-r
]. r:l .-. . r ,:l Ll rl-
I!13':i
l:, [1Erj
tr il;}i'l
1
ii t:r t:s
.t
-i
I :,li'!-,.i r:f-i
-l
l.;lr ;i ,-r if i*.1
1
'- i-l.-: , i i, r:nt
I
I
I
- - _--l
I
!
l;P
I
I
I
;i
,i
ia
r',
Iei
i
?144 -1. .l 1" I -'1- i' 1..!
Ur-:ant [-lr.tp,, Ftle: "t..]1411 i'::Lli
i'j i.ie: i;-.: r',1"::;;11"i it. le: l;.:rrTlltc,at inr-r ai' -r'
i...:-a t :.-S .i I l-, r.i l r .if; ! ': i-i ll'.. i2 :.
i'1dir-'ei,
l-1r,":ratrlr lLt: Lii..i::r;i.i, .r t'r 1 ; ;rre ! I :j l'- | llri.,*r, t.=,i at: tijij';, 12
., . . D rri-1:5i
EVERGREEN AI.TALYTICAL, INC.4035 Youngfield _I{heat -Bidqe CO 80033- (303) 425-602L'
VOI,ATItE ORGA}IICS A}IALYSIS DATA
ib LL205895/ 0L/904/2? /905/08/90s/08/90
A-x2
00
0
0
teDateDateDateMethanoPercent
Compound Nane
chl
vc or de
Ac
ted/Preoareded
Loss on Drying
Client Proiect No. z M-2Lab Prolect No. 3 776Effectife Dilution z L.2Method z 826Matrix a SOILab FiIe No. : >V1llethod Blank No. : RBO
Conc.uglKg
N
5
(82401
95089020.L
ormhloroethane
Cas Number
87t84t95r
not detected
ltllln.
POL*ugZrg
c
1
1 ,
,
Dhh
ride
isulfideloroetheneloroethane2-Dichloroet
7-3-1-0-9-4-
7 4-8
7 4-875-075-O75-0
67 -675-L?5-375-3156-6
67 -6107-078-9
7 1-556-275-2108-078-81006 1-0?9-079-0
? L-4L24-41006 1-01r.0-775-2108-159L-779-3L27 -L108-8108-9100-4100-41330-2
59
L4
L2L2L2L2
5L20
5
5
6
5
5
5L20
5
6
5
6
6
5
5
6
5
5
5L2
55262
5
6
6
5
5
5
5
U
U
U
U
UJU
Uu
UuU
U
Uuu
U
U
U
Uuuu
Uu
Uu
U
UJu
UUJ
,1f hene
Dic
1
1 -Trene
is ,-D
o
t1
Unlesquant
te
Pentanone
ropropene
thane
oroDroDenevin|l EtherrmL-2-
1enei Benzene
Xylenes
Surrogate Recoveries:
-d4L,2 DichloroethaneToluene-dBBromofluorobenzene
8"'
2
QC Limits
( 70-L2LrI 81-117 1u 4-L2Lt
Ii
=
=
J
BE*
iers:limits.s for reaoented, but is
and sample data.calibrition limits.Vol. 18, Part ILare less than the
t water
EPA Pracinf
t-tsEPAtion €s
at ta 11 concenght basistrations and PQL's for soils arenot aFplicable or not available)
C-/.^#. proved:
Jo D Parker
(NA
Quality Assurance Officer
-l;;1i Inii i':HFiiilLiTiriiniiil
i ia ';Jl'.if, tt-TIi
4BI,-1 BELT leFt lirrr ?Et:i.1
)
.i
;Hl;r-iqtIB
r -! Iltlit:t-
fi .1,1!1'ar-6 I
r_1x r:! g lj
l-l
!l
-l
:a.i
1-l
'H11J
aa
i.l
I;i
Li!
I;,'li1
F:
!
I
I
IlnI
€t
t46 1E 1c 1+ 1i 1.b E
lir:lnt Llr..ito,,, Fr le:'^t-J.!.-1?!r: :D.1Ll,:rte Fi le: )
' lrlllIt-,,-|!
' r,a lrrf . ,r\f: ,i tj
11 r.rc: t,;;5;h.,- ft- ..r t-t '_t ..r-l I t .,' Ur-r r '' U i
ld i- i le: it-: ;'i'.rJ: ; i':i
Iriie: lU FTL-'r: F';1= ,iF-"L.llljI;1 flil.lF- r*tl-i;:r ii-a:;t l-.s.l rbr-at i,rrri 'lt);.lt:,'',i) 'i;: iJI
Lli:, "l r'a t ,--, r I L, : ELI'-:
:,i,l-r.r r-r t I : ;;,a : '/ :.1 ,)'i )9 il d, : 0 tr,Irr-,*cte,J at: ?Llllc/l]u l"::i9
EVERGREEN A}IALYTICAIJ, INC.4036 voungfield- whcat-Btdge co 80033- ( 303) 425-602L-
VOLATILE ORGANICPAGE
AIIALYSIS REPORT
2tS1e
Ext
xtract?Y/N
COI{POI'ND
Pyridine
:rogate Recoveries:
Toluene-d8
8"alifiers:
cAs #
110-86-1
92\
not detec above
QC Limits
( 81-117 )
L I its.or reec, but
tL20589s/0L/904/27 /905/ L2/905/ L2/90
A-x2
0
0
0
0
M-22
77 65L.258260SOIL>vl4
RBO5
Client Pro'iect No.Lab Proiect No.Effectife DilutionMethodI{atrixLab File No.Method Blank No.
coNcuglKg
5
( 8240 )
98L290
PQL*ug/Kg
6U
analvIr-mr-zed forts arean estimaEPA
agent watert-sJ
B*
EUnlqua
tect
and
s9tnI 4 L
and samole data.VoI. 1B-, Part ILs are leis than the
= Comooundess othenyintitated onse rfe
outside the calibration lirnits.PQL's for soils are
c- ln ^Lproved:
Jo Parker Quality Assurance Officer
.:n
:!l.].'n
a{
rlt
rl
,.t-L
f3
ltt
l:l
).
:.r
--{l_ a.
..t:
:f _-' "
.. .- -n
i]..rl -.;l'....-
ra '.. ltllj ...:l'
i.'t
rL{ :-r -l-i" - 1 ".
J.
Il rD i-l
'r'L: :l
rO.l '_'i ':. T_
.,4
.:"t:.1
:{ : {
-ir -l
.- --'rll :I. :r.
_}.. !
"< rfi O
j- ..'rj
t: -- 'u
O+'UL ,: 0.!.L! q -.
--t -ir ..
!':.1
tlt:-t
t: .:!
rJ . -:a a -1.
l. 'o ..
I-,i1-L,-
i!o
* rtjlfTJ .{
,]j 'lI".- ..:._l
.i tlj
'-t- -' +'.-, It1
1rlao- -)
13
t
,.urf
rir
tr,
{;
'S,
r.r.,
':C.
tr:,rlj
]t -..
,7'.'rl
,.r'
ai
t,d
'!
I._'::l
,5t,:.
{|,i'
Glq'
.{
1lJ
r{
-t
fi'
3.k
i:,E,t
lr:,
,,:i
r.r.
(r.
'.1'!_J
l]r]F
f,a{l
&
Gt.a!.tl
I
':i
rcr
tIt
aI.
1..-l
.:3\
.r.f,
ri e{
;;- ,1:l "'.-
,tl,'-l---,i: r-r' ',i,' r - l:f i.--.l rf'r.r-r T'J- r-I': - r r r T-t -T .,! rl | ,:.:
,:' ,? i1 ,:., '!i, .::, r;,.r ti., ,l: ,.:,i f::t ::. .i{-t , t, rt r:,_,4 .-l r.i r"
,:I
LI
(:|-.:I
iTI,:i
;i
.:i ,t.
':.,
r:.
,::.,:)
:-
.!r
EVERGREEN AIIAI,YTICAL, TNC.4035 Youngfield^ -wbeat-Bi4qe cO 80033- ( 303)42s-602L-
VOI,ATILE ORGANICS AIIALYSIS DATA
ient Sample Number 3r Sample- Number 3te Reeei.ved 3Date Samoled !Date $xtiactqd/Prepared 3Date Analvzed - 3I'lethanol Extract? 3Percent Loss on Drying 3
c1 ent Proiect No.lect no.fe Dilution
A-1 14x20590
05 / oL/ 9004/2? /9005/ 08 / 9005/ 08/90
N 15.8
E
F No
5
( 8240 )
960890
M-227?651. 198260SOIL>vl3
RBO5No.
Compound Name
lene
-D
ide
thene
an est
EPA
se notedadrywe
Cas Number
not1yueta
Conc.u.g/Kg "E?k;
cI
2
1
L2L2L2L2
5L20
6
6
5
5
6
5L20
5
6
6
6
6
66
6
6
6
6L2
65050
6
6
6
5
55
5
Uu
Uu3JL2O J
UUuu2J
U
U28
Uuuuuu
UUuU
Uuu
U
U
U1J
UuU2J
7 4-87 -37 4-83-975-0L-475-00-375-09-267 -64-L75-15-075-3s-475-34-3155-60-567 -66-3L07 -06-278-93-3
7 1-55-555-23-575-27 -4108-05-478-87 -51005 L-02-679-01-579-00-5
7 L-43-2L24-48-L1006 1-01-5110-75-875-25-2108-10-1
59 1-78-579-34-5
L27 -L8-4108-88-3108-90-7100-4 1-4100-42-51330-20-7
vc
v
i
ateo
,Tr c'L
isni v
-Met -2-Pentanone
hloroethane
Benzene
Xylenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-dBBromofluorobenzene
oroDroDenevinll Ether
analvzedIimj.ts for,
89t83t105t
abovedetec
QC timits
t 7 0-L2tr
I 81-1r7 1
17 4-L2Lt
ts.1i
=
=
J
B
E*
8""Lers 3
me
rePor!,ilgton Iunr.tsis detect reaqentbut is
limifored,
samole data.ibrhtion limit18, Part II,leSs than the
water
ti-onIe.POLI.615nk andide the calSW845, Vol.limits aretIal0-
at
co
L
Unlessquanti cOncentrations and POt's for soi.ls aret basis. (NA = not applicable-oi-noE-available)
3
ca
. proved:
on
Parker Quality Assurance Officer
s.
TNTgI. I N'J CHFDIIATIIGRA},,
ile
4 a
6!5ASB
6EB
55BBB
EAEAE
+54
4BE
?r-a fr ra q
AFBBB
2Er:rBB
15EBA
].ABB
SEBA
amu.I g 9B
14 16 B I
Quant Butpu Fr le:'^U:1J96: :D}
Il I NE UUFre
U1
Data Fr le: )U1i96t tU4l..larne: ;(2 U5y D i i',t65; +UUllrsc: 5;5;4.9H;0i5;0i
ld Fries lD U24::l1ITTTIE: IIJ FTLE FUI+ APHENDIXLast l-airbratrr:n: ?UU'7US .1.4:
Dperator ID: BUuan t l-r nre : !Inlected at: I
iHPBbtlt\:'90;
1q
u6:09L7242
IJH
UUbU9
UU5O8
EVERG-BEEN AI.IALYTICAI, INC.4035 Youngfiel4^ -wheat -Eidqe-C6 80033- ( 303)42s-502L-
VOLATILE ORC,AI.IIC ANALYSIS REPORTPAGE 2'.ent Samole Numberr Sample- Nurnberte ReEeivedDate Samoledpale lxtiactgd/PreparedDate AnalvzedIt{ethanol Extract? Y/N
COMPOI'ND
Pyridine
A-1 14x20590
05 / 0L/ 9004/27 /9005/L4/9005/ L4/90
N
Client Proiect No.Lab Proiect No.Effectife DilutionMethodMatrixtab File No.Method Blank No.
M-27761.1826sor>v1
RBO
25
5
9
g( 8240 )
51451490
CAS #
110-86-1
82r
coNcuglKg PQl,*uglKg
U
QC Limits
( 81-117 )
6
rogate Recoveriest
Toluene-d8
I Lers 38""1
?-
B=*=tI sco TUIUI .E=Unlesquant ta onsea we
st
at a concentration outside the calibration lirnits.cgncgntrations and PQL,s for soils aiet basis.
C,q'* l^^Z.llnproved:
Jo Parker Quality Assurance Officer
./n:TI
., :! . . i,
lrI.ri'l n fr i +g Fra.i::r? ! r-l I
iT,::l': l': .. :err-'II ll,!''1:':
It-:E :LlI rl+E-! :;':i--l
f 1 :.i., . : l.ir- i c'.r r-r: i E,'l ; :':' -'1
j,:, '_rr:l..te_':-.1 I jr-.;,:rl :;:j i i
li:::.-l !.-' .:l :-cI t.'1 E'
3LI I Fr t 'l
IT,td
;10::nT6lr't- :el t.i , 'dinO luEr-'i='
: t.it.'t'i . ll.!: n j: : li i "6' 9'i r,f c-,'
A.,.. :.-r:ii:: i:,i..,'! fl*..:ii'j ;'.1::l
Lr,i: :i:l.ilii,,t :el I
::'!1u
-{ E; t-':-l
72 tJ ,jT : t t'T :I rlr-:-i
;-it
H::!r:'tra
I
ii
ti
li
li
li
t.
t:
li
t
I
I
i
I
i
t
it
li
l,
l:
!t
lilr
!:
t,!
iIri
I
I
iI
II
I
I
I
I
I
I
II
I
I
t
aI
I
t
I
i
I
lj.
H:;ir- .; -:
I
q:.
I
-i1
LI
L
':':' ,,' ':' :'
i.lj :.: it :'
:
?
i-
SirB l:rr:1F
:,! iEr:t[la Btl:rI 13c: ? 1
i-rtu? I'
tJ'1.5.-rl-l..i.Il.l'-l YH:-! l'.lr.l I ll-' j '.,!:
e ?-€"';':1.2|.:\..41.:.:
EVERGREEN AI{ALYTICAL, INC.4035 Youngfield- _wbeat Ridge-eO 80033( 303 1425-602L'
VOI.ATIIE ORGAIIICS AT\TALYSIS DATA
ADateDate E
toss on
Compound Nane
ene lorideAcsulf
?Drying
oroethene
thane
ne
arean estimaEPA P
tat
Cas Number
85r111t113t
not
C1ient Proiect No.Lab Prolect, No.Effectife DilutionI{ethodMatrixLab File No.Ittethod Blank No.
A-1 15x2 059 10s/oL/9004/27 /9005/08/9005/ 08 / 90N13.6
/Prepared
M-22
77 65L.t78250sorL>vl3
RBO5
QC timits
5
( 8240 )
970890
Conc.rq/Kg PQl,*uglKg
7 4-87 -37 4-83-975-01-475-00-3?5-09-2
57 -64-L75-15-075-35-475-34-3r.55-50-5
67 -66-3L07 -06-278-93-37L-55-656-23-575-27 -4108-0s-478-87 -51006 L-02-6
7 9-0 1-679-00-s7t-43-2t24-48-L10051-01-5110-75-875-2s-2108-10-159 1-78-679-34-st27 -L8-4108-88-3108-90-7100-4 1-4100-42-51330-20-7
-Tr
4L
2
L2
L2t2L2L2
6L20
6
6
5
5
6
5L20
5
6
6
6
6
5
6
6
5
6
5L2
6s858
5
6
5
6
6
6
5
Uuu
U
UJ
U
U
UUJ
U
U
u
Uuu
U
Uuu
U
U
U
U
Uu
U
UJuuuJ
rromochloromethane
= -s, 1, 3-DichloroDroDene!-Chlgroethylvinlt EtherBromoform
! -!-{ethyl - 2 - Pent anonez-Hexanone
i al *t?,i3i3E s f; ! * o roe t ha ne
TolueneChlorobenzeneEthvl BenzeneStv?eneTotal Xylenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
8"'lifiers:ed for
tanone1-Trichl
s
t-
.D
1
2
t70-L2LrI 81-117 1
17 4-L2Lt
ter
B=E=*=tra
uIlD.Unlesquang Lse cgncentrations and POL,s for soils aret basis. (NA = not applica6-Ie-oi-not-availablel
roved:
J
on
D Parker Quality Assurance Officer
TNTgI I OH I]I{RI-]HQTOGRgH. :,!r1:r3 B . B am.-t.1i ,.1TtcIB B 1 AB
9r:rBget
?Bqrl
6tr88B
4rJ!,.t19J9!ii
il
ll
il
ll
ti
ti
ll
ltli
t4
I,:A
!8[r€r86 r\J
It2,
tl
I{)'l
r!
I
'il
/!!r.1H t:7 Itht4
1 'tA
18 1e 14 1b 18
Data Frle: >UL)9/!:U4Name: X2 Ut1 l/'L 1 ,t."6'r; *UU;'nF'l'lrsc: 5;5 i4.95;0;5i U;0?,'Uti,'rU i
Id l-rle: IU_U24::illl"rtle: lD FILE FUt( iiFF-'Ll'lUl)( l'.lll'.lLLast Lalrbratlon: 1, ll[l '2i-i H 14:U'I
Suant Outpu Frle: "'U11972:DJ
tJLiA5
Up
UuIrr
er.ator IU: Bl-lHant lrrne: ,UUIUPlected at: 9tlUr0H Do: LJ
.l.B ! 09
EVERGREEN AI{ALYTICAL, INC.4035 Younofield l{heat Ridoe CO- (303)42s-602L-80033
VOI,ATILE ORGAT{IC AIIIAIJYSIS REPORTPAGE 2'.ent Samole Number 3r Sample'Nnrnber 3-;t€ ReBeived 3Date Samoled .D;I; -EftiiEied/Prepared ;Date Analvzed - 3Methanol Extract? Y/N 3
A-1 15x2059 1
05 / 0L/ 9004/2? /9005/ L2/9005/L2/90
N
Client Pro'iect No. 3Lab Prolect, No. 3Effectife Dilution 3Method 3Matrix 3Lab File No. iMethod B1ank No. 3
coNcuglKg
U
M-22
77 651. 158260SOIL>vl5
RBO5
5
( 8240 )
00t290
couPot ND
Pyridine
rrogate Recoveries:
Toluene-d8
8""lifiers:
low BPAfoundtIumbersE=UnIesquant
CAS #
110-85-r.
92t
PQL*ug/Kg
5
but notlyue
abovedetec
rtnt
n €s
ion outside the c
and samole data.Vol. 1B-, Part II.are leis than the
QC Limits
( 81-117 )
I ts.or rea, but
ali.brationils are
gentt-s water
B=*=
limits.si seona and PQL's for sota
C/FNl*-/A^proved:
Parker Quality Assurance Officer
.r. : .l
', :'l
-. J'- !?1
:'l :",:{ -{- "t::-..'-:. ',,
_ii I :|
::
-- {] r!
._ t:
.: | .. it.i
m# r-r
i.. il 'Lr
i. ,. ,:
..'.i'-
:L'
...,
:-1:',.
:! .r
r. :.,tj"-
(-. : ,
--t.',
' 'f: ''.. r.i :i
i. .l
i.:- ,:
-' t: !lr1 ...
rll iR
.. rll
- rrJa.-i
'i i,
". .. t-l
::,
..--,
-r, -f'
,! :-. .li
.t.
lll dt i.!-- 1 trl,ll ,1 -.
-.i .. I:
:--:_)
r{
[r
:,.
(.t-
1
'+'
iI
-.1 I
,:,
._.:11;,t:rI
.) r't;'ii '''
I i"'
,.t ,t,
':_:.ii.
i'- !i "--'.-'"r=:
:" -- l':
rf
r.i'.-
.;
:..:
t:
(i..:
:.
':,",.tl:
..a -
,i. -
..
:
.;.
'i! r
l
1
l.l'r.l
':,.1-rl'1
l
l
!:
'-;.
i'':.
Il-
I".l-i:t....
l-'
I
;l l:
t.'
!'.
:.f!.'
i:,lrlf
!.'
-:t-
,?l
I,:r
lal
r::,t:,
!
qr
,:!
i!
':!l::,-1I
'::
-t:
EI/ERGREEN AI.IAI.YTICAL, INC.4035 Youngfield -wheat-Brqge CO 80033' (303)42s-602L-
VOI,ATIIE ORGA}IICS ANATYSIS DATA
11805925/0L/904/27 /905/08/905/08/90
15. 1
A-x2
00
0
0
N
DaDaDa
MePe
'ent Samole NumberSamole^ Numberte Rebeivedte Samoledte gxtfactqd/Preparedte Analvzedthanol Extract?
C1ient Pro'iect No. 3Lab Proiect, No. 3nffectife Dilution 3I{ethod !Matrix 3Lab E'ile No. tMethod Blank No. 3
Conc.ttg/Kg
r4-27761.1826sor>v1
RBO
5
(82401
rcent Loss on Drying
Compound Name
Chlo
v I
ene orideAc
Cas Number
"E?k;
980890
L2
,,
,
,
-D1-D
t
1
I
1C
1
I -TrrZeII€
Disulfidehloroethenehloroethane
, 2-Dichloroetheneormhloroethane
te
7 4-87 -37 4-83-975-0L-475-00-375-09-2
6? -64-L75-15-075-35-475-34-3155-60-5
67 -66-3L07 -06-278-93-3
7 1-55-655-23-575-27 -4108-05-478-87-51005 L-02-679-01-679-00-5
7 L-43-2t24-48-L1006 1-0 1-5110-75-875-25-2108-10-1
59 1-7 8-579-34-5L27 -t8-4108-88-3108-90-7100-4 r.-4100-42-5L330-20-7
2
2L
I
1
1
1
L2140
1
55
U
U
U
U
U
U
U
U
UJU
U
U
U
Uu
U
U
U
Uu
Uu
U
UU
UUJU
UUJ
v
1
!r
L
2
TolueneChlorobenzeneEthvl BenzeneStvteneTotal Xylenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
OualiO=
as
J
B
E*
Unlesquant
roDroDeneinlI Etherv
-2-Pentanone
hloroethane
QC Limits
t70-LzLrI 81-117 I
17 4-L2Lt
1
1
71t90r
10 1t
for,not detec
sco
I ts.re
,butagent waterl-s
s
t n
samole data.ibrhtion limit18, Part II,leis than the
all concentrations and POL's foright basis. (NA = not applicable or not avaS.lable)soils are
c4"\Jh",-L. proved:
J D Parker Quality Assurance Officer
s
TnTF.l.,0N illrFO|lQTnriFgrl
il6'rtr'l?'t ?E a-.f d rntt
g
lBBBEB
ggBs&
?ssqg
ri88[18
.{ 86}lB
lAAEf,.
?afi'rA
Uata F
Narne:l"lrse:
TICI B L B 1 aa
t)
I(4r-.1
Ia
q{
I
LN
?$
I
ll
ILGto
Ig
Lq 1e 14 LF, 18
Idir
1- cl
u6: 16
Lg :40
BUB
TUUl,UP
?UO5UB
titp
UuIn
rle:'2UlJPBt.U4
><2 i)rv's. i t ..: 65.: -r U C ! HP
5 ;5;5 . ni i 0 i5; 0 i 05r'08 l90 i
Frle: llJ H24::flItIC: ItJ FTLL FUH fIF,HINUIX I.IIst talrbratron: '/U0:ilJiJ 14:U'I
erator Iu:ant Irnre:3ected at:
Suent Dutpu Frle: '^Ul.frBz:D)
t'lt trLlxs
EVERGRSEN4035 YoungfielQ(3
CAJ., INC.Ridqe CO 8003302L-
A}.IALYTIWheat03r 42s-6
VOI,ATILE ORGAI{IC A}IALYSIS REPORTPAGE 2ient
/Prepared
T? Y/N
CO!{POUND
Pyridine
:rogate Recoveries:
Toluene-d8
Pro'iect No.iecf, no.fe Dilution
le No.Blank No.
coNcug/Kg
)tete
A-x2
0
0
0
0
11805925/ 0L/904/27 /905/L2/905/L2/90
vt-2277651.188260SOIL>vl5
RBO5
5
(8240)
01L290
PQI,*uglKg
DaDaDalle N
cAs #
110-85-r.
ta
5U
QC Limits
( 8r.-117 )94r
analvzedlimits for, bu not detecaretan est
OuaIi.f iers:U = ComDound_ BepbrringJ = Intlicate5below theB = Compound* = Praaticalpa. 8240-ilumbers sE = ComDoundUnless othensiquantitated on
water
EPAfound
Qu
calank tionle.ntamit on samDts Ii strumentscollllltl.
sea rfe
at a concentratconcentrationst basis.
ionandoutside the calibration limits.PQL's for soils are
c ?.A h*2,Approved:
John Parker Quality Assurance Officer
:.1
.:.1,-
t!:'r-l
rtt
:-r.-
(:).
'I
rll
nl
-;:t
1.1 ...-
-0!'I':L .,11
rf,-.. ttl
rll s !-
t- q: rllt' ,n '-'
-l ..t*
| +, ,1,1
:.f!-. ,t -tJ]j..
rli. rfl--. "..1- rll
{[(
lf-',l]
-.. l-- .-i
r
.: .l
-t':r. ' .
. ' .:-l
: r -. j'.
.- .-.ll
,:l .ir '::
...1 ',t
:i. t.
(i : r'j-!
-':l"il.;J.,
:I
fll rlr r-)r. ;: trrtl,rj -.:-) ,.. 't-
rli
t:
'r: "'.,
.:_".
Fl
i,
-i'tl
.:r-i
.I,'-{
r- -tr
.i d_l
l. irnLt\
tl .1.
lr:.{
':r:{
. {.:{
:r-:.1
r--1,.{
rl :.
.,
:lt:nl
F (.
dC.. . r!-1 ..
-L " .-::-.,- .-
..t,
,
'!t
'li.n ,J'rtt .3.It
GT
r,
Or
-l
lir
-t
,-I
a(
i:.
':l
i;
C
:Ii-
.r-l -r".1-T.r-.-l:1-:--
,:: I
:'.:'
-!
-r-t T-rf-r'a--."rr',r-a'-rr J-'1"-[-r'7',
,:l
,i:
:,
. t-l
:,!.,
.l
,:r
::,
rl
r_t
qj
l:.
f..
L:;I:i
-i
r:..
,:1
!:f,
.::l.{rl
,lr
tt,,t',:.'ol
tt,
..r.-
d
'i.r:d"
H
.ir.l
.lr
EVERGREEN ANAI,YTICAI,, INC.4035 Youngfiel4^ -wtrqet-Br4ge CO 80033- ( 303)42s-602L-
VOI,ATILE ORGANICS AIIALYSIS DATA
'.ent Sample Number 3r Sample- Number 3--te ReEeived 3Date Samoled .D;t; EltiiEEed/Prepared ;Date Analvzed - .Methanol Extract? 3Percent Loss on Drying 3
Compound Name
22057 4s/oL/904/27 /905/08/90s/08/90
14.1
A-x2
0
0
0
0
N
Client Proiect No. 3tab Pro'iect No. 3Effectife Dilution 3Method 3Matrix 3Lab FiIe No. 3Ilethod Blank No. :
5M-22
77 651.158260SOIL>vl3
RBO5
( 8240 )
850890
eneBenzene
Xylenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
r-ers 3
an es
-2-Pentanone
hloroethaneoroet
are
PracinLa
0
I t t t
ta on
Jo D Parker
analvzedlimits for, bu not detec
Cas Number
ta ion
ts trationsted intrument deteccoumn.
or reaoent rrater, but is
Conc./Kqug POL*ug/Kg
chl
vcl'letAce
or
ide
L2L2L2L2
5L20
5
5
6
6
5
5L20
6
5
6
5
6
6
6
6
5
5
5
1.2
65858
5
6
6
6
6
5
6
U
U
U
U3J18Ju
U
UUUU
U27
Uu
Uuuuu
Uu
U
U
U
U
U
U
U1Ju
UU2J
7 4-87 -37 4-83-975-01-47s-00-375-09-257 -64-L75-15-075-35-475-34-3155-50-5
67 -66-3LO7 -06-278-93-3
7 L-55-656-23-575-27 -4108-05-478-87-51006 t-02-579-01-579-00-s
7 L-43-2L24-48-L1006 1-01-5
1 10-75-875-25-2108-10-1
59 1-78-579-34-5L27 -L8-4108-88-3108-90-7r.00-41-4100-42-51330-20-7
c
1
1
Disulfidehloroethenehloroethane,2-Dichloroetheneornhloroethane
,
,Bu
,1
t
1
ot-s f -D oroDroDenevin|l Ether
2,ac
89t97t9lt
QC Limits
(70-L2Lr
I 81-117 1
17 4-L2Lt
I ts.
Pr
$uali
?-
B=E=*=
v s
at
EPAtion
andcalVol.are
samole data.ibrhtion limits.LB, Part ILleis than thet.
Unlesquant si cgncentrations and PQL,s for soils arebasis. (NA = not applicable or not available)
Quality Assurance Officer
. proved:
ow
TOT}tL I DN f,HRDT1RTO6RBI1ri !e )?1-?86
4
SSBBO
;008
n8r-lB
5tr8Et
4804
:{ t4 H l.'i
EL]BB
1r-10 r:1
6 .emu.Ttc
a 1 aa aa1
?14 16 18 a
o4 Euant Outpu Frle: ^t..tLJE6::D3
:RP
i r)i ,, L'l B./rr D ;
L4: 0'Il2: 4:L
ft
I,1
1..!
Itl
(\
I:;!,i.1
t4
Iill
4.1
Ia,'t
I
0i
4
U'If BE:.-t-,t C. .
01;r-r;5
Fr:i
5
O L'I5 DB00508
18 1
DataNanre:
11 iec:
le: :)20574 L]
iD
lrl File: ID 824::l{lTitle: ID FTLE FL]R APPET'IDI:{ I'llNE t.rt-lFisLast tlal rbrat ion: 9DL-l5DB'14:01
L-loeratDr ID: BtJi.lant Time: '.?ln letted at : I
NB
EVERGREEN A}IALYTICAL, INC.403G younsriet$orTliBlr$itr" co s0033
VOI,ATILE ORGANIC A}IALYSIS REPORT
'ent Samo1e Number 3Samole-Number tte Rebeived tDate Samoled 3Date Exttactqd/Prepared tDate Analvzed - 3Methanol Extract? Y/N 3
Client Prolect No. 3Lab Proiect No. 3Effectife Diluti.on 3Method :Matrix 3Lab File No. 3Method Blank No. 3
coNcuglKg
A-2 2x20574
05 / oL/ 9004/27 /900s/Lt/9005/ LL/90
N
yt-225
?7 651. 158260 ( 8240rSOIL>v1481
RBo51190
COMPOI'ND
Pyridine
:rogate Recoveries s
Toluene-d8
OualiO=iers:
cAs #
r.10-85-1
99r
I ed for but not detect,
PQ1,*ng/Kg
5U
tsst
abovedetec .L
L
ion outsideand PQt's
irni reaoentbut is
QC Limits
( 81-117 )
I ts.or
,
water?-
B=*=
Iow ane ima
ststrument
s
a10-
a
on and samole data.Vol . 1B-, Part I Ls are 1e5s than thet8
a concentratoncentrationsbasis.
L
caloi1the ibration limits.for s s areseawe
t nh sco IIIIIII .atcon
C,'/rv f, "fr'-proved:
Jo D Parker Quality Assurance Officer
':'rI
."1
.ir
J
t:.
rll
'.r-
.U.
{f
1:l
P
'n
_1a
t- - --.: ::::-i .' :r
.'r - ,-., ,[ ,"
J: - r'j'-:.ts .-
! ' --
l! tl
-ir:L_, :. _lJI:i .-
ili ir.i"..r
", tI
l. ,n
It "':l-- -- l
:-.I
-a:1
1-'
.. .J "'.. "".:n
'n' ..
:i . -.j
,:...r .
U:'1 -l.l
.L
'n ni .i
... :: .!-i
'!l , ' ''
- J r:-
!f
-11 rl
.< :'
1....
.:r -..
n'r']]
:'i r'{
:li-eI:I
it- ri
Oc
-{ r_l
:{ iJ
'. c.
"-l :.: ::r
I r. ,-t.
_.i...-* r-!.: 'tt
L.:l
r.-t -.- []
Og U.':11
it .,1 '
r..1. !:
,.il'fiJ
,:,
i: -:l
:'- ra
,:(,r{
rt,rl
"lta
NJrl
,2.rl
.r'rt
:,
*-r',,i;-'-T-.'];'''r -',l-1--i-.,r-a-.r-
.lr
.l
.t,i
T-J-r -l-1-'i-r -l;- -.*,1,
a.'r'J
':J,:]
.1i
.11
l:
-l
3,
at
'j'
jt'n
.'.t':i
i,l
,r'
i:,
l'-
i,..t,it*
l'rt.-I.*
l;,i
t,,;.-t..
l,;t-[:
1,":'
iill-.
I,LIt ,
i.l-
t:,
.,.n.n
.: (.-'
":a l-
,!,,:'..{
nl
'i'
,3r'tt(il
I19't
tc!
'-t, (t
'1'
-i
r:r.l
,:.
::.,:,
FI
EVERGREEN AIIAI.YTICAL, INC.4035 Youngfield tlheat Ridqe CO 80033- (303)425-602L-
VOLATILE ORGAIIICS AI.IALYSIS DATA
e-2x200504
0505
N
4575/0L/90/27 /90/07 /90/07 /90
Lt.2
Client Prolect No.Lab Pro{ecf, No.Effectife DilutionMethodMatrixLab FiIe No.Method Blank No.
tq-22
77 65L.L28260SOIL>vl3
RBO5
5
Loss on
Compound Name
-Tr
Prepared
t?Drying
s are
Cas Nurnber Conc.l.g/Kg
( 8240 )
680790
POL*lqzKq
oride
ide
Disulfidehloroethenehloroethane,2-Dichloroetheneormhloroethane
7 4-87 -37 4-83-975-01-475-00-375-09-267 -64-L75-15-075-35-4?5-34-3156-50-5
67 -66-3107-06-278-93-3
7 1-55-6s5-23-575-27 -4108-05-478-87-51006 1-02-579-01-579-00-5
7 t-43-2L24-48-L1005 1-01-5110-75-875-25-2108-10-159 1-78-579-34-5L27 -L8-4108-88-3108-90-7100-41-4100-42-51330-20-7
L739
11111111
5110
5
5
6
5
5
5110
5
5
6
6
6
6
6
6
5
5
611
55656
5
6
6
6
6
6
6
u
U
U
U
J
Uu
U
U
Uu
U
U
Uu
Uu
Uuu
UUU
U
U
U
U
UBJ
UJU
28
v
1
te
,Dic
,
1
-Tr oroethanetzenebromochloromethane-is , 1 , 3-Dichloroorooenel-Chlqroethylvin|l EtherBromoform
4 -I{ethvl - 2 -Pentanone2-HexahoneL, L, 2, 2-TetrachloroethaneT6tfachloroetheneTolueneChlorobenzeneEthv1 BenzeneStvteneTotal Xylenes
2
2
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
iers:
an estimalowEPA Pfound
cal40-
88$10st80t
2BJ
QC Limits
170-L2Lr
I 81-117 t
17 4-L2Lt
ts.QuaIiu=
B=E=*=
for reaoent waterbut is
le data.
E)o
aiUnlesquant onsea noteddry we
tion limitPart ILs than the
concentrations and POL's for soils aret basis. (NA = not applicable or not available)
e-fflr,,"-t
Quality Assurance Officer
---proved:
D Parker
TOTFL IOH EHPDNPIOGRBT1
i I e )t/13o
teagas
11800
6 ariLt.
4 g
ID 824::11D FTLE FBRib rat i on:
1 gg 1 )
18
fluant Dutput File: '^ULf68tzDJ
tsg
9E
8g
79
66
5a
40
g
a
B
gs
38s00
?ggag
16488
rY
I
i.t
t4
Ia6,1
I|,|
n
Ingl
Iiorn
F
In
18 1
Data
l'lame:
11i sc :
Id Fi le:Title: ILaat Ca I
Fi le:x2D575;s;5
> U'lf 6B z :D4
5 27765 : ziDf : RP
. 0l ; o ;S; o ; isltnz,'oD i
L APPENDIX NII'lE trDAs9DDED7 lA:29
Lloerator ID:0Lant Time:Injected at:LP 255L9229
BDB9D05D7P00507
EVERGREEN A}TALYTICAL, INC.4036 Youngfierd wheat-Br4ge co 80033
( 303 | 425-602L-
VOLATILE ORGANIC AI.IALYSIS REPORT
A-x2
0
0
0
0
N
DaDa
'ent
,tS 2405755/0L/904/27 /905/ LL/905/ LL/90
Client Proiect No.Lab Pro'iect, No.Effectife DilutionMethodMatrixLab F'ile No.I.{ethod B1ank No.
tt-22
77 65L.L28260sort>v14
RBO5
U
QC Limits
( 81-117 )
ts.
5
( 8240 )
Da
Met
Prepared
T? Y/N
we
coNcng/Kg
821190
POI*uglKgCO}TPOI'ND
Pyridine
:rogate Recoveries:
Toluene-d8
OualiO=iers:
low
on
110-85-r.
94t
fox,not detec
cAs *
6
waterJ=
B=*=
ec ,ionAtedtdenstrurnen tect
and samole data.Vol. 1B-, Part ILare 1e3s than the
itat
TB}
POt).El6nksw845,limits
E=sco unn.at a concentratoncentrationsbasis
ion outside the caland PQL's for soi.l ibration limits.s aresea
vA^proved:
Jo D Parker Quality Assurance Officer
l.l5
:.J,n.f
-{
'Ll
II
o-
lrl
!
tro:
:1 -{:{ -{r. f.
,x ]-.tr
:J.. !-'lI} 'r]!.:
L,.'ljR:- 0tF!o#0Ll:rU
'l"t !X'-1(a-: (,:3-
r:i
B:E
.:::
rl:l:{ - ':}.!: *',. 4..
I-,1
l.- + ..
J- -+'l*'o
- .L'.o.I:-
0iG- ..:j
d'l]
+' t0
TJ - ,ll_-; -!
-,f.
-f
"-t.a't,
...=
-{ _, 'a
.'".J']
1 .1 -,i'. ".,]].r1.=
'il r "'
/'. -fr '
0i:: J'!<-!":
.L
Q 0] r-ltE!.0
E.rl .-
:1.: E
,3.i.r'.5i'
OJ
,Sl
15'..tl
rl
,5'
f.d'
rl
;;3
(t
6'6r.t
+:4
'xd
,.li
rl rU
C
.lf,:B
-".:o:l- -r
it-1;t .it
't .o
=tl
:! tn
...1
(:.,
rl
o-.:5
...t'
.l
-l
€;n,
(tl
I.D
lr,
lItr(3.
Fa
[,(tx
(:
':tl-
;I1 -.4-'1r-T'trrn'ar.r-5t'rr- {1nr.llt.:i:..! 6. (i 'i. ti '1 ,:r €, r:rr;-r € (;i ,n Ci 'i.' €, .S. t\,,1 {i an r! .:i r:.r ,I' (lr tir€r ti ..it 11 ,: t:' 't. 6, r:Jrn ..G t... ..! lr: 'f (.' nl '-l
r,--i[r--',]i (3(n
,i. (,
('n
"r.r{
0r
r{
EVERGREEN A}IAI,YTTCAIJ, INC.4036 YounsfiEl(i -IihEat-Brdse co 80033- (303) 425-602t-
VOI,ATILE ORGAIIICS AIIAI,TSIS DATA
DateDate
Loss on
Compound Nane
-Tr
-r
1 -Tri
v
-2-Pentanone
hloroethane
eneBenzene
s
forts are
racin
Client Prolect No. z M=22r.aE-Fioiect uo. 3 7765Effectife Dilution : 1,15uethod- - z 826OMatiii : SOI!r,a5-File tlo. : >v13ueEhoal-Blank No. : RB05t?Drying
2505765/0Li904t27 t905/08/905/08/90
L2.7
A-x2
0
0
0
0
N
5
(82401
8?0890
e
2
9o"l
7 4-87 -37 4-83-975-01-475-00-375-09-2
67 -64-L75-15-075-35-475-34-3156-50-567 -66-3L07 -06-278-93-3
7 1-55-655-23-575-27 -4108-05-478-8? -51006 1-02-579-01-579-00-5
7 L-43-2L24-48-L1006 1-0 l-s110-75-875-25-2108-10-1s9 1-78-679-34-5L27-L8-4108-88-3108-90-7100-41-4100-42-s1330-20-7
Cas Number
not
Conc.ttg/Kg "E?k;
11L11111
6110
6
6
6
6
5
6110
6
6
56
66
5
6
6
5
611
65757
6
6
6
6
6
6
6
uU
U
Uu39J
UUuUuUu4J
UuuU
U
U
UU
U
U
Uu
Uu
Uu
U
U
UuU
Surogate Recoveries:
L, 2 Di-chloroethane-d4Toluene-d8Bromofluorobenzene
a iers:
89t102t99t
4
B=E=*=
QC Limits
( 7 0-t2LrI 81-117 I
l7 4-L2Lt
I ts.
,
and I dac
t water
Quantand sat t
ta ion
strument
above
ts
s
ta.limits.
se
L
co tions and POt's for(NA = not applicable
Ls are Part II,s than the
soils areor not available)
k^a
Unlessquanti
a/71/\Approved:
on
D
we t c umn
Quality Assurance Officer
OTBL I OH L]HROT,RTO6RRI1
I anu,
I a o ?
14
130090
1ea0sa
11&69
Lg6sg
9AOg
gB
7g
b
50sgg
4gooa
300sq c\l
In
c.a
I6'lo
tq
Ia lo
Ist)tn?ggaa Iq I
lftta0g
IB ?4 1 18 g
Data Fi le 2 >VLTB7: : D4 QuantName z X20576.7765:4Ll :RPllisc: 5 iS t4.99 i 0;S ,0i05/08/90;L2.7
0utput Fi le: "Vt3B7z rD3
IdTi File: ID B24zz11tIE: ID FTLE FOR
'l
APP
98CI5
ENDI>I NINE LIOAs0B 14: D'ILast Catibration:
0oerator ID:Euant Time:Injected at:
BI]B9Dll50B900508 L4t O6LJzL9
EVERGREEN ANALYTICEI, INC.4036 Youngfield Wheat Bidqe CO 80033- (303) 425-602L'
VOLATITE ORGANIC A}IALYSIS REPORTrs
? Y/N
couPot ND
Pyridine
' rrogate Recoveries:
Boluene-d8
Quali iers l
ona
5576/0L/90/27 /90/ LLl90/Lt/90
s
E
Date
A-2x2005040505
but not
le No.Blank No.
coNcuglKg
831190
PQl,*uglKg
ect No.No.lution
I or
5
( 8240 )
M-27?61.1826sor>v1
RBO
N
cAs *
110-86-1
94t
U
QC Limits
( 81-117 )
t tB.reaoentbut is
6
waterJ=
B=*=
,tb and sVol.a are
amole data.1B-, Part IL1e6s than the
ststrumentcoatlltrur.concentration outside the calgntrations and PQL's for soilis.
O*/I-U*L
ibration li.mits.s are
D
'.-proved:
J ker Quality Assurance Officer
!.\ €t\,=
=,O
C.IN.{-l
s. lnn =c=J:-r,=
t:o.1. o.
*11ro
EL -11oF- 0,
Op ULCO)lll ,rl -'
d- _-l cD3*
oc
EA
>,orB-.{
'+:{
O-{
:rC=o=rl dal.
=+,." o..
ilr-o
:h:f <
il- -+l+o3ct-'- tll.t]1l .-
0)0
- .. ,...1
<0)
l.L- #!10
IJd(]
- F- -.1
$l
LJ
iD.:t
i{
o
LL
-lo-
l
'f
(l
f,13
').
-l
F{
(L ,.
:r.: 'J'{iJ ".
.. !l .4.' .'..n
rcr .31 ...
Jl .O=\if:.\ .-..
:< i\ $.]}...'f,'
^.D .'\'d
0]=rJ<..1 .'1
LL
o(t)(J+'F t0|Eo-):?E
Glrl
.1.
Fl
trl
OJrl
'5'
.Srrt,s,rIr
':!
I -5t
i-ss
|trrl.rl!n-1:,,r!
(-,
(i;(n(i,
ci'
,:n
rllf!
'!
t:rjr'l
(l(i'
a.ir(ll(lr,
rJ
6r6t,s'
OJ
(s,.
Gr(fr-rl
E6,ol'r.l
ts,
4..m
6t$-:l
F
f,E,l
&
o(o
ot
I(s!
-t'
0r
a
CTec.LFCI
i:,
Cra.(-:
7C
{tt-
EVERGREEN AIIALYTICAL, INC.4036 Youngfield_ _I{heat _Bidge CO 80033
( 303 1425-602L-
VOI,ATTLE ORGANICS ANALYSIS DATA
tetete
yt-22
77 65L.L78260SOIL>vl3
RBO5
No.ank
A-2 Ix2057705/0L/9004/27 /9005/07 /9005/07 /90
N L3.7
ec 5
( 8240 )
700790
DaDaDate AnaMethanolPercent
Compound Name
1
Prepared
Loss on Drying
-2-Pentanone
Benzene
Ienes
Cas Number
not detec
unn.
Conc.ug/Kg "E?k;
No.
uUU2BJ
QC tturits
t70-L2tr
I 81-117 1
17 4-L2Lt
I
ide
L2L2L2L2
5L20
6
6
5
5
6
6L20
6
6
6
6
6
6
6
65
5
6L2
65959
6
6566
6
6
uUUU1180J
Uu
U
U2J
U
U25
U
Uuu
UuuU
Uu
U
U
U
Uu
UBJ1
3-1-0-9-4-5-5-4-0-5-6-3-5-3-7-
7 4-8
7 4-875-075-075-0
67 -575-L75-375-3155-6
67 -6107-078-9
7 L-556-275-2108-078-81005 1-079-079-0
7 L-4L24-41005 1-0110-775-2108-159L-779-3
L27 -L108-8108-9100-4100-41330-2
Ac
,
Disulfidehloroethenehloroethane,2-Dichloroetheneormhloroethane
v
1
,
Unlesquant
-Trene
gi
te
seona
,1
oroDroDenevinfl Ether
Surrogate Recoverles:
1,2 Dichloroethane-d4Toluene-dBBromofluorobenzene
8""lifLers a
88r82*86t
ts t waterJ
B
E*
,Eow
at s ca1Vol.
and
are
samole data.ibrhtion limi,ts18, PArt II,leis than thetts
noteddry we cgncentrations and PQL's for soils aret basis. (NA = not applic-ble oi-not avallable)
C ?t*h*l
Quality Assurance Officer
- proved:
D Parker
T l'l; Il i nt'l IHnD]lF.TnGFf.]1
ic 1 -{3 .9-ghr,t . u tmLt.
468
TiL
8EE lEBB {r$Ar,e0.84
1E BL1LlL1rt
1_.rffnnRr1
I
1I -- ir.ivliEll----'--.i
J
I
1.,:a6.t.t6,
I-lI
A ! .t i:r /-r gFl
I
II
I
I
;
il
ii
ll
ii
il
4il;;lEft n
Ig
tt)Itnut
.J
I.n
FI
tl)in
ti
IL,lt4
Eri irlEtlr
l
B 14 1,i 18 B c
[Jat a Fii::me !
['1 rsc:
I le: >t-r 1]70::D4)i:t l-i b )r-t i.;..'o? : -+Ul- :,iFr
5 i5i4. rrl) ! U i!; u i ii5,'0?,'9A i
Ouant OutpL,t Frlei "U'L17OirD2
1d Fr 1e:Trtle: ILast La I
IL) ij!.+::li1D FTLL FLiu fiFPtl'iDIX Nll.lE Urlnsrbrdi .inn:'Ji-liji-. 1tl l"U: U6
Liaaratcrr' ltJ: BLiHLiu,:nt ii;;ieZ ';\l-! l:10lrrrected at: ?UVttBT ]u:2t.) 11 . ')tr,L V . LU
EI'ERGREEN ANALYTICAIJ, INC.4035 Yonngfield wheat-Br4ge Co 80033- (303) 425-602L-
VOI,ATTLE ORGAI.IIC ANALYSIS REPORT
rrdt€DateDate Prepared
A-x2
0
0
0
0
28
9711,rc,4/27190s/ LL/90s/ LL/90
Client Prolect No.Lab Pro'lect No.Etfectife Di.lutionMethodMatrixtab Fi.le No.Method Blank No.
t4-27761.1826sor>v1
RBO
5
( 8240 )Da ? Y/N N 841190
COUPOI'ND cAs *coNcuglKg PQI,*uglKg
Pyridine 110-85-1 U 6
:rogate Recoveriesr
Toluene-d8
QC timits
97N ( 81-117 )
8""1 iers:not detec ts.forts arcr or reaqent water, but is
B=*=
E=Unlesquant
samDts li
tionle.and samole data.Vol. 1B-, Part If ,s are leSs than thetItrunentECOllllln.ion outsideand PQL's the calibration limits.ti ae a concentratoncentrationsbasis.for soila areonawe
Ch^- proved:
D Parker Quality Assurance Officer
-i.o
a |.1
.-! .:l
ll;{.{ .{
Jl$l0::='1 --. -f
rn ].$.
:*(r[]€L ..1f
'li- O
(]s ULCOrll ,a -1
:llt ll -
(U
tr
E.T
l-..
;Y-o0- -r
:}.{
B.'1
-,;
O:-;
i{ di,
I: +'
.. rll ..
,1*rl':- 1- .-
le ,l-1ll ,:i-- 'nD1l-
IDG..r .. :_i.. 'llq trl
1.f - r0*-.-l
a.la
.{t
rI\t
-{
(I}
U-
:r
o-
f!:l
f,o
tr3
,.J
$
-{:.|
0- 1'
...=
.r"{ j ".
.. .1 .q
'. .-d1
'$ .t', ."
:J-1 .&,:f'i"''J-.l.:, .-..:r\
:if
0, =,r'j-:'l "'
LL
o(l).J+'Erl(l ,tl -:J, i_
':l
II-r
d
.Il
rl
.r'
rl
(ili
rl
:.rD,5,.l
clc:'clclq)
r-st
z-ss
(:,
i:,
t-r
r-r-l'rrrT-r
€',:r
,:'
-J
-!_
5:r
r')
fJCi6,
,:,{il:ti.
f.-
,St,:,,:r
15',r.
'!,r3
rl
4l
t
L'
F
J€ill
($
ltr.ofrl
I(lr
0r
E
CI(r1(!LFct:
@rc:
C
'Il-r
EIIERGREEN AI'IALYTICAL, fNC.4036 younsriet$oriliBlr$itr" co 80033
VOI,ATILE ORGANICS ANAI.,YSIS DATA'ent S es 21005785/0L/904/27 /905/08/905/08/90
L9.2
A-x2
0
0
0
0
N
6;
Da
Da
tetete
Client Prolect No. 3Lab Pro'lecf, No. 3Effectife Dilution 3Method 3Matrix 3Lab File No. 3Method Blank No. 3
u-22
77 65L.238260SOIL>vl3
RBO5
5
( 8240 )
880890Lossract?on Drying
Compound Name
ide
-Dt
1
oroethane
o
Cas Number Conc.ug/Kg PQL*ug/Kg
7 4-87 -37 4-83-975-0L-475-00-3?5-09-2
67 -64-L75-15-075-35-475-34-3156-50-5
67 -66-3L07-06-278-93-3
7 1-55-5s5-23-575-27 -4108-05-478-87-s1006 L-02-679-01-579-00-5
7 L-43-2L24-48-L10061-0 1-5110-75-875-25-2108-10-1
59 1-78-579-34-5L27 -L8-4108-88-3108-90-7100-4 1-4100-42-s1330-20-7
27
Uu
U
UuJUu
UuuUu
U
Uuu
Uu
UUuuu
Uu
U
UUJU
U
UJ
t2L2L2L2
5L20
6
6
6
6
5
6L20
6
5
6
6
6
5
66
6
65
L26
,
,t2
t-s
thane
-2-Pentanone
Benzene
Xylenes
iers:
ae
loroethane
ts arean estima vEPA
at
5151
66
6
6
6
6
6
I
1,T6
ti
=
=
J
B
E*
Surrogate Recoveriesl
1,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
103t102t110t
not above1yuedetec
s €.ionin tsEPA 4trumentI
samole data.ibrhtion limits.18, Part II,1e3s than the
1
and
ts are
QC Limits
t70-L2LrI 81-117 1
l7 4-L2Lt
I ts.8"u
UnLesquant
orf or
,
reaoentbut is lraters
t
8 ts s
co ollln.si cgncentrations and PQL's for soils aret basis. (NA = not applicabl,e oi-not available)we
..oproved:
on
D Parker Quality Assurance Officer
N.@
-{ \t
$}\
F{F{
@(Doo
u\ u\Oooooc,GlO.o.
(f.'vHoo
EL.d.rJoF{}
o#oLC0)0)(l-o-l cO13*
o(tlf>
IJZE-tza
x$
-rlozm[d1=&l(Lo
<E(3
-l CNE(r..8 ....tL C$o
or [rJ.i@J+,FooL.rHl]
Q.a
oma..fJ.a il)[L- +,+ro!'- o*FJ
rq
?
tn
m
far
-l>(
o
tr
+,
lo-
tP
3trl
v
Lo:l c!g
|}.
-l
13
ct.
mF
O-$.Eat....,.O'3cf,.. {'.1...^m
(fl lfr '^
€() \oc)r\N.qerf\t$>.c.(3.\m 'Ntf\.. t$ .^oond6l 'n.aXuru
c;;#EoOO-ozE
(u
o
@rl
t
(u
Glrl
ooo(Doo@t
1-SS
t -st
ru(Yl (Y, C'J Ol OJ rl rl
6Ea@E\o
z-ss
z-sr
E-SS
c-sl
o&OG\t49t:t
TD
G,
OJ
oG,
d
o
Gl
ra
o
.G.aE6
o
crc(ooF(I
oa-CJ
o
J(IFo
EVERGREEN AIIAIJYTICAL, INC.4036 Youngfield -wbeat-Bidge cO 80033
( 303 )42s-602L'
VOIJATTLE ORGAI{IC N{ALYSIS REPORTPAGE 2en
S__teDateDateDateIt{etha
ts
Ananol
A-x2
0
0
0
0
21005785/0L/904/27 /905/ L2/905tL2/90
Client Prolect No. z 14-22Lab Proiect, No. B ?765Effectife Diluti.on z L.24Method t, 8260Matrix : SOILLab File No. : >V14Method Blank No. : RB05
5
( 8240 )
91L290N
CO}TPOI'ND
Pyridine
:rogate Recoveries:
Toluene-d8
t-iers:analvzedlimits fot,
cAs *
110-86-1
87r
s etsstrumen
coNcrug/Kg PQt *
ug/Kg
abovedetec
U
QC Limits
( 81-117 )
I ts.or
,
5
8""1
J
B*
aneEPA t s reaqent waterbut is
al0-
seona we
and sample data.Vol. 1B-, Part ILare leis than thetIurnberstsacolllllrl.E=Unles sLquantta
at a concentration outside the calibration Linits.cgncentrations and PQL,s for soils aiet basis.
( rl"-Jrd,,"-proveda
D Parker Quality Assurance Officer
;TAr- r irfr f:HF0rtlT,'.r6F trf'l
ile .,rJ1491 35.8-a64.8 amur. i(fi-r:l7air7b5i48r.: iEF Ei-.ri5,tr1 iEiFi'4it7A,/LTII4ga Barr laEB 1686 e6BB- t --l l. . i- i - I r -. I ..i. .l ..1
tp.-,r:{a-l
a
1t
+ r_. u .-! L1 lJiI
1:1; i3 i s{
-{
't:J r r.'i !i rH
I4
.-., .-1
t
fri
I grJEl'
8[1
43i.t8
4
t.1
U,
In1t.o
i
uJ la 14 16 ?a
Uets Frie: >UI4?.1 ::tlL
i.;.3 me : i{t l-l t ,}B : ,",'61.r : j+ U l- : l-.'PHr':c : t i5i9. 0T ; U i5i 0 ; tJ5,,!'2./9l i
Llu.rnt Dutput Fi le: '\Ul.49tzzO2
ld Frie: IL] i-''Yl'.] ::iilTrt le: lderrf rf rcat ron olLast Lalrbratrotr! ';ll iJ!, 1?
t]oerator 1O: EUHLiLan t 'l- r;i,e : I it ttli 12In.iected at: 9UUDLz
PviD r^idrne
.1./
'|'rr")|LL.ZLl0:54
EI/ERGREEN AIIAJ,YTICAL, INC.4036 Youngfield _wheat-Bidqe Co 80033' (303) 425-602L-
VOLATILE ORGAI{ICS AT{ALYSIS DATA
La.
DaDaDate Ana&tethanolPercent
c
1
1
Es
tetete
Loss on
Compound Name
-Tr
-2-Pen
I
Unlesquant
Prepared
?Drying
2L205795/0L/904/27 t905/08/90s/08/90
24.7
A-x2
0
0
0
0
N
Client Pro'lect No. 3tab Pro{ect, No. !Effectife Dilution :Method 3I{atrix 3Lab File No. 3Dtethod Blank No. 3
M-27?61.3826sor>v1
RBO
5
( 8240 )
890890
Cas Nurnber Conc.uglKg POL*ugZKg
13131313
7130
7
7
7
7
77130
7
7
7
7
7
7
7
7
?
7
713
76767
?
7
7
7
7
7
7
Uu
Uu3J35J
Uu
U
U
U
Uu38UU
U
Uuu
Uu
U
U
U
U
U
UuU1J
U
Uu2J
7 4-87 -37 4-83-975-01-475-00-375-09-267 -64-L75-15-075-35-475-34-3155-50-5
67 -65-3L07 -06-278-93-3
7 1-55-556-23-575-27 -4r.08-05-4
7 8-97 -51006 1-02-579-01-579-00-5
7 L-43-2L24-48-L1006 1-01-5110-75-875-25-2108-10-1
59 1-78-579-34-5L27 -L8-4108-88-3108-90-7100-4 1-4100-42-51330-20-7
1
,
Tr
ide
Disulfidehloroethenehloroethane,2-Dichloroetheneormhloroethane
r
ate
hane
Benzene
Xylenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
Lers:
t
tanone
hloroethane
for,
racin
104tLL2N116t
QC Li-nits
t70-t2lr
I 81-117 Iu 4-L2Ll
I tE.fiuali
B=E=*=
detec
t ta 10ngtr
terv
at ststtcollllln.
^pproved:
se we
D Parker
otta onIt concentrations and POL's for soils aret basis. (NA = not applicable or not available)
Quality Assurance Officer
ow
TOTEL ION CHRONNTOBRRN
F e )\11389 3 .g-
6
6009o
55040
50066
4564
4a
:15
3
a
15
t
6
aDu.
I 114 ?
F,
I.4
Jr,
Ifii1
,r1n,$t
I!!
Ia
Ia
1 4 bJ.
ld File: ID 82Title: I0 FTLELast Ea I ibrat i
Data Fi le: >ULlBName: X20579 2775Ilisc: 5;5;a.99;0
Doe ra t o r I D:Quant Time:Injected at:
9::04 Suant Dutput5 r40 tRP;Si0;05/0Bi9D;24.7
File: "U1fB9zzDJ
4| zlllFER APPENDIX NINE UOAson: 900508 14:01.
BD50B L4:490508 I4tL7
BO90
9D
EVERGREEN AT{ALYTICAL, INC.4035 Youngfield _wbeat_Brdge CO 80033- (303) 425-602L-
VOIJATILE ORGA}IIC ANALYSIS REPORTPAGE 2L2790127/90/90/90/901414
2055/4t5/5t
A-x2
0
0
0
0
N
Pro'lect No.'lect No.fe DilutionreEDaDaDa
tete
act? Y/N
COUPOI'ND
Pyridine
rrogate Recoveries:
Toluene-d8
iers g
Prepared
ona
vt-22
77 651.338250SOIL>v15
RBO5
u
QC Limits
( 81-117 )
limits.
5
( 8240 )
131490NoNo.
cAs #
110-85-1
83r
trument
coNclug/Kq
andVol.
PQL*uglKg
7
OualO=
J=
B=*=
ed for,not
ts
t water.Ls
a
0
samole data.1B', Part ILle3s than thefsare
ide the cal's for soil
llllll.sE a ibration limits.s areUnlessguantig
- proved:
J D Parker Quality Assurance Officer
:1 'il-f, tf\
4-{
'1 if
i.{ .-l
l\i$-il ::i i:f,
i --j ..-'
iD f. '1.
::
H(Uil]
EL -ItE:-- trl
OP(JLC{.)
1; ,R -,J-1,:;:l :-r -
0.1
C
Tf r'.1i .,.r
L,.]rr
O- rl
+..f
O:{
': :l
fi:lj r.!i
.. o..
1-,1r-.+ ..
1. --
l! (l
JLL* 'U .t.l'tl i
'l! o
..u
I.1--*'
4- I-!
1-r a r0
- - ;- ..-J
i.lo
rn-{(r.
et
0)
lr
.:o-
f
'f
trof
:13
,]\
-1_ i'1...{
u...rl-r
:n ':..J ' i
l: ;; :a...t ''....-.J-'l
-r\ U'. '.
-{ ..r-r '='j.-...,.4,' . .'t\].... .,\'3''.. 't
rD:r -0- ;'.1 ".a jr(.,J.
I
O'D.J{,8,0
Orl",:J.:- r'-
i\l
.5.
OJ
crrl
qI'
-l
t,.{
'u
.tr
Fl
{
ai.(i'
(11
-41-;la-r. I'rTalf -r"[rl't J T' a'tr r-T'r l;1 la'l-."r-f,T
.:,.:l,:i,lt
4-:;l;
-G-d-:
3a't
llnt:!(:,
.:,:.
,:,1
f-st .----
*.):i.:)
':r I
r_t
t,j,c,
t.'l
fJ
,sr'-
OJ
r5.
'S'rO"rl
,:.
E.
oJ'
ai,5...
CT
{l
'(, 5.r'.1 (s...tn'
tfl
--lrf,.-l
lr
F
,:l
&
t-ft
:_r(-(,:-'
a:
;it-,::
l-
ti,
'!''i,
':l
,:j.lrt
t3{l
(t
E\TERGREEN N{ALYTICAIJ, INC.4036 Youngfield wheat-Brdge CO 80033- (303) 42s-602L-
VOI,ATILE ORGAIIICS N{ALYSIS DATA
A-x2
0
0
0
0
N
JrrdtBDate Prepared
t?
Disulfidehloroethenehloroethane
, 2-Dichloroetheneormhloroethane
Client Prolect No. z, M-22Lab Proiect, No. r 7765Effectife Dilution z L.2LMethod : 8250l'latrix : SOILLab File No. : >V13Method B1ank No. : RB05
Conc.ug/Kg
2L40s805/OL/904/27 /905/07 /905/07 /90
L7.7
5
( 8240 )
730790Percent Loss on Drying
Compound Name
or
oride
Cas Number
",n?k;
,
,
,
7 4-87 -37 4-83-975-01-47s-00-375-09-267 -64-L75-15-0?5-35-475-34-31s6-50-5
67 -66-3t07 -06-278-93-3
7 1-55-656-23-575-27 -4108-05-4
7 8-87 -51006 1-02-579-01-579-00-57L-43-2L24-48-t1005 1-01-5110-75-875-25-2108-10-159 1-78-579-34-5L2? -L8-4r.08-88-3108-90-7100-41-4100-42-51330-20-7
c2
1-D
t
1-Tr
u
Uu
U10?3J
U
U
U
U4J
Uu34uU
UU
Uu
Uuu
Uuu
UU
U
L2L2t2L2
6L20
6
6
6
6
6
5L20
6
6
6
5
6
6
6
6
6
66
L2
66161
5
6
5
6
65
6
ac
atev
1
1
,oroethane
is v
-2-Pentanone
ene
Es Benzene
Xylenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-dBBromofluorobenzene
8""iers:
-Tetrachloroethaneloroethene
analvzedlimits afor, bu
an estima
2
uBJ
U
98t109t87t
uU5BJ
QC Limits
t70-L2Lr
I 81-117 Iu 4-L2Lt
I tg.1i
=
=
J
B
E*
abovedetec t waters,
a
0 ts
andcalVol.are
samole data.ibrhtion limits.18, Part II,1e5s than theulllo.Unlessquanti concentrations and POL's for soils arebasis. (NA = not applicable or not available)
rrpptOveds
on
D Parker Quality Assurance Officer
amu.
ULl73i77650r;o;
1 oo
2
RP5.,07/90 i
1 oo
14 6 I
rOTRL IOH CHBOI,BTOGRSN
4
Lgggog
9400
ssao
Sgggg
?agoa
10a8
Data FName:Ilise:
Id File:Title:Last Ea
D
6
5
49AgA
ro
In
Quant 0utput Fi le z ^UI171: : D]D4
lr)
II
ID 824::l't'lO FTLE FBR APPEND I X I.{ I NE I-'OASibration: 900507 L6229II
N
In
1\l
Ia
It^vl
.,2
S;x2 058 05;5;5.
BOB9005090050
Ia
0rl;0;0
7 222247 2It57
Ooe ra t o r I D:Quant Time:Injected at:
403G,BYHEEIEIU iiltEl[1ffita"'86''rors- (303) 425-602L'
VOI,ATTLE ORGAIIIC AMLYSIS REPORTPAGE 221405805/ 0L/ 904/2? /905/ L2/905/L2/90
A-x2
0
0
0
0
N
Date
.ent
/Prepared
? y/N
COUPOI'ND
Pyridine
'rogate Recoveries:
Toluene-d8
$uali
Client Pro'lect No. z M-22Lab Proiect No. r 7765Effectife Dilution z L.22Method t 8260Matrix : SOiLLab File No. : >V14Method Blank No. : RB05
coNcuglKg
5
( 8240 )
93L290
cAs #
110-85-1
9lt
not
ta ion
PQt *uglKg
u
QC Linits
( 81-117 )
ts.
6
iers:forare t water
Pr
J
B*
ts
t
a
s
!tre
v
t and sample data.VoI . 1B-, Part I Lare leis than theonfsB
iseon
rrmn.
- at a concenEration -outside -the calibration limi.ts.I cgncentrati.ons and peL,s for soils aieht basis.
ow
anproved:
D Parker Quality Assurance Officer
E{trlt$
,-\ r
<1.1
f,ll\'1'-lrji l,r$i0:--,,=
J _r --'mo. cl.
::
*0)(,
r- lluoFof+'
Og rJLCII),l] rF -,O-f, !:Dti*
rur
TJT\*l1
lr;:,!l-:'{
'+ f.lO.-l
!:::r-1.-,{ -:}.J: !,.. o..
'}. - ':,l:-.:ts .-
'll- -*lPo,1 C.L'-. tD .oT1 a
(l)(,* "i-l<'D
IJ--#+. t,lo-o-.F J
':..lo
.N'd
-,
0)
ll.
-.,1o-
Plr:l
+'Lo-1a
$
c.tJ
'L\-r:1,.f.
-f ,J ...),=,=
"...t,F\5"''
']\ .B{f'f i'. ".:{ i\. €]i...,].A'=.:'l'f,
0) =in-;.1 "
lr
o0t(J+rEil)(ro-.
lsr
rfirl
..t,
r{
t
r.'Jrl
A,rl
l??.tr--(1.
ti
ci'
?.|
G'
,t.
4..-t
_ 4.t,
rTl'rfT
.!}
':J*"1,:i
.1,
t"
-r1 -r
.il,!.i.t
rTr-r4Tt
Ifi
'rrrJ'rrnE.fl"er-r-d
4r 15 €t In.Ir fit Gt 'tfir '::t r5l I !G, (i 6' tAtt, Cn f.. ..O
arl6
Ll
ci,ri
C;t
':'r{
.
.S',
E€.-*.
,5, .G,rn-4,.
:E.,.5.ot-,_
,:r'
6E*:
j
:
.3,.l6.-t.
:
f,
F
f,
Ea
o
{$r(t(u
I(9
tlt-t
rl
0r
CIa((!,
C:Fd
L.'c:x
l::
fi)-
l::
.nJ
E1IERGREEN AIIAI,YTTCAL, INC.4036 Youngfield _wheat_Bidqe CO 80033- (303) 42s-602L'
VOI,ATILE ORGAIIICS AI{ALYSIS DATA
-2 1620s8105/ 0L/ 9004t27 /9005/07 /9005/07 /90
24.9
Ax
NPercen
)tetete
Client Pro'lect No.Lab Prolecf No.Effectife Di.lutionMethodMatrixLab File No.Method Blank No.
225Irl-
/Prepared
Loss on Drying
7761.3826sor>v1
RBO
( 8240 )
740790
POL*ugTKg
Compound Name
or
Ac sulf
Cas Number
97*104t99r
not
ta
co
Conc.ug/Kg
2
7 4-87 -37 4-83-975-01-47s-00-375-09-267 -64-L75-15-075-35-475-34-31s5-60-5
67 -66-3t07-06-278-93-3
7 1-55-656-23-575-27 -4108-0s-478-87 -51006 L-02-679-01-579-00-s
7 L-43-2L24-48-Lr.0061-01-5110-75-875-25-2108-10-1s9 1-78-679-34-5L27 -L8-4108-88-3108-90-7100-41-4100-42-51330-20-7
te
1
1c
v
1
Trt c
loride 9L20
uuu
U
J
UU
U
UJ
U
U
u
U
U
Uuuuuu
Uuu
U
U
UuBJUU
UBJ
3
51
13131313
7130
7
7
7
7
7
7130
7
7
7
7
7
7
7
7
7
7
71376666
7
7
?
7
7
7
7
,,-D-D
,-D
h
2
-2-Pentanone
Tetr hloroethane
zeneBenzene
Xylenes
Surrogate Recoveries:
Lr? Dichloroethane-d4Toluene-dBBromofluorobenzene
fluaIi iers l
,-Trrzenc)
oroDroDenevin|l Ether
2
QC Limits
t70-L2LrI 81-117 I
17 4-L2Lt
abovedetec I ts.
s or reaoent, but is
samole data.ibrhtion limit18, Part II,leSs than the
soils are
J
B
E*aI0-t
8
tionle.
water
t
Unlessquanti ot setat we POL's forapplicable or not available)and
_ _ roved:
J
ona
Parker
concentrationst basis. (NA =not
Quality Assurance Officer
s.
OTFL I LlN CHROI1RTOBRAII
,'I llDU.TIC
4 o I so 1 aa e ag
14
t.l
1B
8A86
60gg
4AAOg ta,
II$t
II
(\l
Ir/,1t,
la
I(r,m
zgsog Ia I(,?aa
1A ?4 16 ?
Data
Name:llisc:
File:x2 0595;5;5
>VL374z zD4
L 27765 ;40E ;.65 ;0;S; D;0
Euant Output Fi le z ^ULJ74z zD3
RP5,,87t90;
IdTitLas
Fi lele:tEa
: ID 824: :111ID FTLE FOR APPENDIX NINE UOASI ibrat ion z 900507 15229
Ooerat0Lan tI'nject
orTimed
ID:e:at:
BDB9805879fi0507 2225422227
EVERGREEN A}IALYTICAL, INC.4036 Youngfield -wheat Ridqe CO 80033- (303) 425-602L-
VOI.ATILE ORGAIIIC A}IALYSTS REPORTPAGE 2enst
DaDaDa ? YlN
COUPOI'ND
Pyridine
rrogate Recoveries:
Toluene-d8
I iers l
Client Pro'iect No. z lrl-2tab Prolect No. t 776Effectife Dilution : 1.3Method z 826Dtatrix : SOILab File No. : >V1Method Blank No. c RBO
coNcuglKg
QC Limits
( 81-117 )
A-2 16x2058105/ 0L/9004/27 /9005/L2/9005/ L2/90
N
tetete
5
( 8240 )
94t290
cAs #
110-86-1
8lt
PQI,*ug/Kg
7U
9r.lL'not
sco uIIltI .
abovedetec I ts.r.ml s or reaqentbut is water
B=*=
s ,
fs
and sanple data.Vol . 1B-, Part I Lare leSs than the
E=UnIesquant ge
we
s
Lta on
at a concentration outside the calibration linits.cgncgntrations and PQL,s for soils aret basis.
C./'h/\Ir^-t'-proved:
D Parker Quality Assurance Officer
ftT2t I nt{ nHFUrlATflRFli}t
! ! : i : L.l34 35 .4-a64 .8 amu a5:ii ;7755;48f ;PP a i3 ;4.9? i9 ii ;etl88;7
8Bt-r 'l aa 1 8A
,\cTI I
I
I
I
I
I
+t
1
,lq
i
r:l
8E* El-1gH
I1
4
)
ir-rri;di&r l
I
J
a
4"-1gq
r it 'r.l
f.vH
1
f- -.4
f.t
Iv.l
a1t,l
I
Da t,=
i rdlllE a
11 rec:
1rl 12 14 b1 13
>U1.494::tJLl;,r,'tr1,;3[L:.9ei0isiu.;
id Frle: iD i-'\'R::i''1L'Irt ie: I,jerififrcatron ofLast [aIrhr'atri]n: ?;-l lil:;I?
OL,eratDr ID: tsl-lulilr.,nt -[i;i,eZ ?bi.l h12In.rected at: 90u512
Euant Outpr,r Frle: ^UL414iz02. uLl
itr t'LZ,,9a :
Frle:X! tl t:8
5 i5;4
Pv
1B
ridrne,,))
'ti | 2sL2225
EVERGREEN ANALYTICAJ,, INC.4035 Youngfield- wheat-Bidse cO 80033- (303) 425-602L'
VOI,ATILE ORGANICS A}IALYSIS DATA
--t€tDateteDaDa
Percent Loss on Drying
Compound Name
or
rideAc
tate
-D
-2-Pentanone
C1ient Prolect No. z lt-22Lab Pro'lect No. r 7?65Effectife Dilution z L.23Method : 8250I{atrix : SOILLab File No. : >V13Method Blank No. : RB05
Conc.uq/RqCas Number
not detec
tita ion
tra
runn.
e-2 18x2058205/0L/9004/27 /9005/o7 /9005/07 /90
N 18
5
( 8240 )
750790
POL*ug7Kq
7 4-8? -37 4-83-975-01-475-00-375-09-2
67 -64-L75-r.5-075-35-475-34-31s5-60-557 -66-3L07 -06-278-93-3
7 1-55-6s6-23-575-27-4108-05-478-87-51005 t-02-679-01-679-00-5
7 L-43-2L24-48-L1006 1-01-5110-75-875-25-2108-10-159 1-78-679-34-sL27-L8-4108-88-3108-90-7100-4 1-4100-42-51330-20-7
uu
Uu
872J
Uu
Uu10
Uu53
Uuuuu
U
Uu
U
Uu
U
UU
U
U
L2L2l2L2
6L20
5
6
6
6
6
6L20
6
6
6
5
6
6
6
56
6
5L2
66151
6
6
5
6
6
6
6
42
L
ifiers:OualO=
eneBenzenetIlenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
-TetrachloroethaneIoroethene
Practinb
ta on
BJ
U
2
1
U
UBJ
QC timits
t70-L2Lr
I 81-117 1
17 4-L2Lt
ts.
,
t water
s
97*102t98t
owJ=
B=E=*=
ts
Unlesquant st ea cqncentrations and PQL,s for soils arebasis. (NA = not applicable or not availablel
Quality Assurance Officer
-rproved;
John D
DTFL I ON CHPOT,IFTO6RA}Itri !a \t)127
868S8
?ggg
600a
f8qffu
60.9.!mu.
4 0
ID 824::M1D FTLE FOR APPENDIXibrat ion: ?00907 t6
224r56
1 o
L
4Aggs
3sssg
err999
1SAO0
rO
Ia
r.tIg1oc.t
I
ln
>VL375. .D482 27765;408 ; RP4.97, o;S ;B;05tD7t9o,
N
Ia
Ig It!'to
L+161
Data File:
Name z X205lliscz 5;5i
Id Fi leTitle:Last Ea
Euant Dutput Fi Ie z ^UL775z zDj
i
I
I
N I l'{E UOAs229
Doerator ID: BOBQi-rant Time: 9Dt507 2tInjected at: 900507 22
EI/ERGREEN AI.IALYTICAL, INC.4036 Youngfield wheat-Bidqe CO 80033------ (3031425-602t'
VOI,ATILE ORGA}IIC A}IAIYSIS REPORTPAGE 2rsleA-x2
0
0
0
0
21805825/0L/904/27 /905/ L2/905/ L2/90
r-,dt€Date
Client Proiect No. z 14-22Lab Proiect, No. 3 7765Effectife Dilution z L.2LMethod : 8260I'tatrix : SOILLab File No. : >V14Method Blank No. : RB05
coNcrtg/Rg
5
( 8240 )DaDate Ext
xtract?Y/N N 95L290
PQt *
uglKgCOI,TPOI'ND cAs #
Pyrridine 110-85-1 U 6
rrogate Recoveries:
Toluene-d8
QC Limits
82N ( 81-117 )
8""1t iers:analvzed forlimits are not abovedetec I ts.3 t watert-
B=*=
an estima ,t sEPAfsand sVol.amole data.1B', Part ILleis than thetstsstrumentare
E=scato umn.ibration li.urits.Unlessquanti
a concentration outsgncentrations and PQLbasis.
ide the caloilseac'g for s s areonlret
proved:
Jo Quality Assurance Officer
No
$.r]l\d-{
o
tl-
-lrl-
Pf|f
ColE 0)
C
Tt6.d "alL..>triL 'r
+f.tO'{
jr
o--r -. ,1.
f_v.. o..
t'-,1l.- + ..
.t- --lPo:r':L.- {ul]Ia
[,(}.- .. ,1..)a ll)
'f.
,:{
-l[\.:ri,
.-r i,..) 3'=
,...,:n.3 J.'-,]..O=..f,:\ .'.
I'ti''l
/. q'{ '
-11'$
0) :i r',
-:.1 "'- )<6\
LL
.nil
.3.{
:frl
..u
.U
rE(s
{lrl
t-sr
,:}
=$F rlA
1i.l
:-t -l
c.li{
-{ .{islltr3-=
01.f,.,f,r
{-l .. p*0lo
O+ 0LC[]llt '1 -traf, !:'-l r-
Z- :1iil
,Sl
rl
F
fil
EL-E
tf r- fi
{t'
t
Janl
o
.D.{.
ru
I.$
lJ- <P/JaTJ'q*l- -J
o(l)fJ! E't]t! 'rl ".]::EFl
,5!6il5l-i.
E
CI(t.(I'c.F(I.
ttIL
c
n
t:
lit(i!
(r-'
l:
'ur{
G!
..('
c]ci{},::,
1i{,
Tc,
c.1
r,-
r:i,
(:l
olol
!
:!{l,,,
,l
h.
.il
'--1''i'a'
c)
EVERGREEN ANALY]TICAL, INC.4036 Youngfield _wheat-Brdqe CO 80033- (303) 425-602L-
VOLATILE ORGANICS AI.IALYSfS DATA
--teDateDate tqd/Preparedect
?Drying
ide
oroethane
v
-2-Pentanone
hloroethane
zeneBenzene
lenes
iers:
ts arean est
se
Proiect No.lect, No.fe Dilution
le No.Blank No.
Conc.uglKg
2200s835/0L/904/2? 1905/08/905/09/90
15.4
A-x2
0
0
00N
il-22
7? 65L.l78250SOIL>vl3
RBO5
5
( 8240 )
900890LoEs on
Compound Name
Chlo
t
ene
sulf
,,1-D
,
Tr
Cas Nurnber
"E?k;
1
1
1
1
1
5542
1
7 4-8? -37 4-83-975-01-47s-00-375-09-267 -64-L75-15-075-35-475-34-3156-50-s
67 -66-3L07 -06-278-93-3
7 1-55-656-23-575-27 -4108-05-478-87 -51006 L-02-679-01-679-00-5
7 L-43-2L24-48-L1005 1-01-5r.10-75-875-25-2108-10-1
59 r.-78-679-34-5L27-L8-4108-88-3108-90-7100-41-4100-42-5L330-20-7
L220
Uuu
UuJu
Uu
U
Uu
U
uu
U
Uuuu
Uu
U
U
U
U
U
U
UuuuuJ
L2
10
Il-
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
8""orf
85r89r9lt
s sstrr ment
abovedetec
1
andcalVol.ts are
QC Lirnits
t70-L2LrI 81-117 1
17 4-L2Lt
ts.1i
=
=
J
B
E*
reaoentbut is waterv
at
co umn.
ta LsA
i.onin 4
samole data.ibrhtion limits.18, Part II,leis than thetI
Unlessquanti noteddry we concentratlons and PQL's for soils aret basis. (NA = not appllcable or not avallable)
..rproved:
D Parker Quality Assurance Of ficer
OTFL ION CHROMRTOBRATIFile >\,1398 35.0 .0 amu.
6 1 AB 1 6A da
6
55
5g
45
40gog rn
Ia35r_1AB
30sBs NI!2
c{
Ilr7
ie
Iotn
a5088
?BggD
Ia15BB
IoatgSg
5AS
16 1 4L 6 1 a
Data Fi le: )UL390z tName: X2058] .7765:.4llisc: 5;St5.0?;0iS;
D40;0;
Suant Dutput File: ^VL390::D]RP
D5 /08/90 t24.7
Id File: ID_824::I11.Title: ID FILE FBR APPENDIX NII'IE \JOAsLast Ealibratron: 9005D8 L4:0'l
QpUu
erator ID: BOBant Time: 90t]508 L5225
1-4z 48Injected at: 900508
EVERGREEN AT{ALYTICAL, INC.4036 Youngfield Wheat -Bidqe CO 80033' (303) 425-602L-
)vdteDate e
DaDa xtract? Y/N
COITPOI'ND
Pyridine
rogate Recoveries:
Toluene-d8
OualiO=iers I analvzedlimitsan estima vEPA P
t t
Client Prolect No. ?Lab Prolecf No. tEffectife Di.lution 3Iulethod 3llatrix ZLab File No. 3Method Blank No. 3
coNcug/Kg
A}IALYSIS REPORT
2
LE ORGAIIICPAGEA-2 20x20583os/0L/9004/27 /900s/ L219005/ L2/90
N
cAs *
VOI,ATI
t4-2257765t.L78260 ( 8240 ISOIL>v1496R8051290
PQL*ug/Kg
110-85-1
92*
detec
t ta ion
ts t
POL).6lAnksr{845,limits
outside the c
6U
forare
QC Limits
( 81-117 )
I ts.
t water
owJ=
B=*=
,
and sample data.Vol. 1B-, Part ILare leie than thecoumn.ata concentrationgntrations and alibrationils are limits.1l concght bas PQL's for so
a,h\'-proved:
Parker Quality Assurance Officer
,=.{\
tc.c!
"': lt\
A4
f\f{-{ -l.tr$Itl:: =
m.f,.,).
-ttlo
L -fin+ fl
OvULC0l
{1, o -'o..l trr:l 3-
(l)
tr
Eh
-,:.1L..>;r[Lr
+,.\
O.<
-f'
O;-1
:{ ar}.
iP.. o....t}cU*rtl-.r.-
.1. --lvolll c r-... ,Ll l]TfH
ali o. . .. ,:_r.. o.U--!P$l
TJ-A* l- --i
r.r,3
€
t).rt
,1
0)
LL
4:
a
P)a
o
3|]
=
'J\
Nr{a'r
:l! 'n
.{,j,,.]==
.. .-'J',)€..l"n
1.}' .rl:f.il -.. '.r{'.. $
3.f'
0t -*,iJ)< ''..1 "'- )i- t9.
LL
otDo-E'fttO,n-
!I.d
'tr'l
:t
(]J
r'l
'{
-*=:
It:i3:,.{C1(.J
i:-$s
'!,:i
\1l
t.-sr
"r-
-?-l-i'f-r
'n,::r
'a'l:.
Ul
tgrla'1e-rrt
'!l 'S!6rf!
EI.(.
airs!
'5ia-
rt
6r
Gr
ru
rl
6r
tsr
rl
.I
t
LI
lft
6
rt
n
lft
lr'j
0-q
Li6n
It\a
r.-t.-
l'tti
!-_r
((H)(F
ent
a
.n\o(U
I
Gt
Lt(.i
1Go.+Fl
ill
lr,
E
CI&'
G.
F
CI
C.cI(_.
7C
frF
EV-ERGREEN AI{AI,YTICAI, TNC.4035 Youngfield _Wheat_Bidqe CO 80033- (303) 42s-602L-
VOLATILE ORGAI|ICS AI.IAL,YSIS DATA
ts M-2277651.168260SOIL>v14
RBO5
A-x2
00
0
0
N
32
06 155/0L/904/27 /905/ L0/905/ L0/90
L3.7
)--t€DateDate Prepared
t?
isulfideloroetheneloroethane2-Dichloroethene
oroethane
arean estima
t
I
John
Client Prolect No. 3Lab Proiecf No. iEffectife Dilution BMethod 3Matrix !Lab File No. 3l,tethod Blank No. 3ent toss on Drying
Compound Name
or
ene ride
5
( 8240 )
371090
Da
Cas Number Conc.uglKg "B?k;
MeAc
7 4-87 -37 4-83-975-01-475-00-375-09-267 -64-L75-15-075-35-475-34-3155-50-567 -66-3L07 -06-278-93-37L-55-656-23-575-27 -4108-05-478-87 -51005 L-02-679-01-579-00-5
7 L-43-2L24-48-L1005 1-01-5110-75-875-25-2108-r.0-159 1-78-679-34-5L27-t8-4108-88-3108-90-7100-41-4100-42-51330-20-7
I
38
4
uUU
U
UJ
U
Uuu
UUuJuuuuuuuu
Uu
U
U
U
U
Uu
U
Uu
Uu
L2
t1
1
1
1
55
,
,L2
,Tr
ene
-2-Pentanone
Xylenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
iers r analvzedlimits for
89r86r99t
QC Limits
t70-L2LrI 81-117 1
17 4-L2Lt
Pr
Ro"l
J=
B=E=*=
ter
at
runn.Unlessquanti
-pproved:
eaon concentrations and POL's for soils arebasis. (NA = not applicable or not available)
c.?t^ )",^L
Quality Assurance Officer
ITEL I OH CHFONATOGRCI1
! ! e )t/1437 amu.TI g 6g g
TAASO
65AgO
55800
SAAgA
4aago
..!2lO2t
ORAAD
30aog
?5gaa
?9609
i5608
N
Ing)
r!
Ia ritI
..ltGI
Ia?
It4 It,tn
5
1 4 6 I a
Data Fr le z >VL477z zUName: X2U6',L5r7765i4Ullrsc: 5 ;S i5.O'I ; 0 ;S;0
LC;iu
Quant Output File: ^Vt4r7z:D2RP5/LO/9D i
IdTrtLas
Filet
le
Ea
ioIt
IDFTi324: : m].LE FOR APPENDIX NINE UOAs1,09'10 1.0 : 06bratron: I
Ooerator ID: BQLant T rme: 9Inlected at: 9
tJB
0 05'r 0
0 u51.0
LlzL912217
EVERGREEN AI.IALYTICAI,, INC.4036 Youngfield _wheat-Bidge CO 80033
( 303 l42s-602L-
VOI,ATILE ORGANIC AIIALYSIS REPORTPAGE 2
.,'
r-,E.te
Prepared
? Y/N
COUPOI'ND
Pyridine
^rogate Recoveriesl
Toluene-d8
fluali iers:
Client Proiect No. 3Lab Pro'iec€ No. !Effectife Dilution 3Method 3Matrix 3Lab File No. rMethod Blank No. !
coNcng/xg
A-3 2x20615
0s / 0L/ 9004t27 /9005/ L0/9005/ L0 / 90
N
$-22577 651.158260 ( 8240 )SOIL>vl437R8051090
cAs *
110-86-1
85r
ta
PQL*ug/Kg
U
QC Linits
( 81-117 )
6
J=
B=*=
fot, but not
sts
sco lllllll.
water.t-stionIe.a10-
seasiUnIesquant
tI t fs
and sample data.Vol . 1B-, Part I Lare leSs than the
E at a concentration outside the calibration li-mits.cgneentrations and PQL,s for soils aret basis.ta on we
( -/lrt^
P
ca
--proved:
Quality Assurance Officer
TflT:ll. , nu iHF iitATnRRgH
r'0 . B :mu.TI
48a 88ts !?tlq 1bt3Q eqaB. i . i-. . I .-i-. i . I I i I i , i
I
I
a'JT"-r$En
I
I
I
I
I
I
l
i
I
I
I
I
I
,lil
il
ii
:t
J
,H
1
t
,J
I1
.l
J
)
.I-rlr* _1
4:ai;t B
iirj
,-, at {F',
a
iw
i
I
ii
I
I
1!:r 1a 14 tr 18 rt
L).: t o
'1.:/rtE.
I'l t sr: I
Fr
?
le: >1,..r i4_1 ,.'::UIi Uo i!i : ..r."'a!' : iLi L. : itP
i5;9. l:l1i U i5 i 0 i lj(.:,'lU"'Y0 i
Uuant L)utpr,'- F r le:'tPl.417z zD2
id Fi i.lrti,e:
L--dl] I- t-
e: iil_l-'r'R::;"i II'fer,t if rcat:orr ofal ll.lrat r'lr1: '.i;i;-;'.'.ii Pv1ii rrdrne
. rl-
IjttrBr-ator' IU: E,rbj
Lii-r,=rn t l"i i;,e Z 'iU.Jb i Llrr-rected at : 9ulJb.Lu Lt . L-.|
EVERGRBEN A}IALYTICAL, INC.4035 Youngfiel4- wbeat-Bidqe C0 80033- (303) 42s-602L'
A-3 4x2 05 1605/0L/9004/27 /9005/L0/9005/ L0/90
N 10.8
I
- _teDateDate
VOI,ATILE ORGANICS AI{AIYSIS DAIIA
c
/Prepared
?Drying
Prolect No.iect No.fe Dilution
No No
Conc.ug/Kg
5
(8240)
381090
P vr-22
77 65L.L28260SOIL>vl4
RBO5
xtractrcent Loss on
Compound Name
ch1
Dh
Unlesquant
oroethene
-Tr
-Tr oroethane
her
-2-Pentanone
loroethane
Benzene
Xylenes
surrogate Recoveri.es I
iers:ed forts aretlma
L,2 Dichloroethane-d4Toluene-dBBromofluorobenzene
ide
sulf
ona
Cas Number
90t84t100t
not de
ta 10n
llllln.
POL*ugTKg
11111111
611.0
6
6
5
5
6
6110
5
6
6
5
6
6
5
65
6
611
65656
66
5
6
5
5
6
U
Uuu3J70J
UUuuu
Uu
9
UuuUuu
Uu
U
UuuuuuU1Ju
Uu2J
7 4-87 -37 4-83-975-0L-475-00-375-09-267 -64-L75-15-075-35-475-34-3156-50-5
67 -66-3L07 -06-278-93-3
7 1-55-556-23-575-27 -4108-05-478-87 -51006 L-02-679-OL-679-00-s
7 L-43-2L24-48-L1005 1-01-5110-75-875-25-2108-10-1s91-78-679-34-sL27-L8-4108-88-3108-90-7100-41-4100-42-5L330-20-7
.I
s
Tr
QC Limits
t70-L2]-rI 81-117 1
17 4-LzLt
QuaIi
B=E=*.=
f
t_at
water
si cgncentrations and PQL,s for soils arebasis. (NA = not ipplica6le-oi-noE-available)
C,%L- proved:
John Parker Quality Assurance Officer
S.
TflTAt. l rir.l IHR(rmATl'lG?gtl
F i i: .,tr14 ii 3 B amu.T i':.
J
-i
4?a 8€E
e : :' t.J.L 4-1 ! : : 1., .1.
il i, I e, , ;:' ,,';, ';, ; j iJ i..:i;4. 96 ;',i ;5: 0 i
I
LJ
t'\
FT
18 1i 14 1a
1qr-i6 16BE
.,c)
?Britr
1B I
Lluant [lutp,- ; Fr le: "Uj-4]B: :D2
-l
ti o |:' 'J r-l rtlII
: --. .- .-,,r,
1: r Ut3
1 .: i.r tr tr
-iI
J.l
-t
rlJ
I{
-l
/,II
;ft
!inln+l
I!!
I.'!:
L.I
i -Ittt6
4
D.-ta
la.arilE .
Pl reci ui!rr
B,r ,' L iJ
Frl
r:'
i rl=.e: t
t-t) !
ld r:l'rtl
L-,= i I rbrdl- rr:n!'il-iiir: iiJ iti
.-r,1.4 , , l.{.trf i + . . , r ILE FI-!i,J iiF.:-E.IJLt I X t'l i i.lE tll-lH.i
t)r-,
Ur-crBtrfp lLi: $i-:l:li=i'-.3nt'[rine:'+::iiL-.illlrr.tected at : 9i-lli510
'r-.a.?'l
IlzB4
E\'-ERGREEN AIIALYTICAL, INC.4036 Youngfield- _wheat _Bidge CO 80033- ( 303) 425-602L-
VOI.ATILE ORGA}IIC
PAGEA-3 4x2051505/0L/9004/27 /9005/ t0/9005/ L0/90
N
cAs #
A}TALYSIS REPORT
2
-r-teDate
Client Proiect No. !Lab Pro{ecf, No. 3Effectife Dilution 3Method 3Matrix 3tab File No. 3Method Blank No. 3
coNcuglKg
t{-22
77 651.138260SOIL>v14
RBO5
5
( 8240 )Date Prepared
T? Y/N 381090
CO}IPOI'ND PQt *
ug/Kg
Pyridine 110-86-1 U 6
:rogate Recoveries:
Toluene-d8
QC Limits
84t ( 81-117 )
8"'lifiers:
T-
B=*=
water.is
t t,s
and sample data.Vol. 1B-, Part ILare leis than theumn.on
tsBaaconcentrationentrations andis.
ou ide the calibration linits.l-se concbas PQL's for soi ls areona
r ,//+\-fdu'-proved:
J D Parker Quality Assurance Officer
..o.1it::!rr.i .<
:{:{
.i'..fi
il:t'+
'3.. v
-lllo
r- ..u
r-l -- ql
ta) v .)LCO),tl rI -,
'"] '"-
IU
tr
1l :{
)ril'0-r
+{
Cr{
-t.::--.13::,
- r-n
:: +'.. o".
!--,:i-+ ..
l- -*lPo
-- rlt lltl .-
.l)'n
-..:j.. [,
'I-r'!tQ
E -,ll--:. --!
f.rl:]
rurn\s
.-{
a-
(l
TL
J
lf-
l',:l
#co
--1E
:--'+
,=,
A
a- a.
-t ;l'.
._t .;:
". . . -l--l'lo;"-.rt\ 'l]'=J.f,'. .-
"{'.€>..,1
^.o ..{.tr
(l)::il'l
-'l'l "'-:{:r.'!L
o (l) f-.)
'-Er0rE,! -
,:,-l
'5,
ql
r{
.I,
rl
rf
Fl
,rJ
t4
r1,
rJ
:i5(,J 'I' rl (j. .lr ri.l ,:.-r ..tl]] .\l (r! (, -t rl
i--st -
'-ra frrr.l,r-n;!!a'rrT !'r' .F''1-1l:-t1;r'Ct .lr (i 13 .r, ,Sr C.1{} rst (i fi' ,:r 't' C:,'l .5' ':, ( t .:t G. t-d
;[i'rr;^r,r:r .11r!. r'J
,S, 'r:,.1- r.',
alT
,:,,:'
OJ
i-l
,5'
'3
,I.
..s,.
4
t
F
4l
'3
,!'.0
(U
I
'n
to
(t
n-t
'[
L
It((
CF
CI
c,ftI(-
=t:
;t-c|-
EVERGREEN N{ALYTICAL, INC .4035 Youngfield tf,heat Ridge CO 80033- (303) 425-602L-
t No.
ution
No.
5
(8240t
391090
PQL*uglKg
M-22
77 551. 118260SOIL>v14
RBO5
VOLATILE ORGAIIICS AI,IALYSIS DATA
c1 ent
E
No
Cas Number
A-3 6x206L7
05 / 0L/ 9004/27 /900s/L0/9005/ L0/90
N g .93Loss on Drying
)--teDateDateDa
Compound Name
v
sulf
Prepared
t?
Conc.ug/Kg
1111t1Ll.
6110
6
6
6
66
6110
6
6
6
5
5
6
6
5
6
6
611
656s6
6
6
6
6
6
5
5
u
U
U
U4J25J
Uu
U
UuUu10
U
Uu
Uu
U
U
Uuu
UUuU
U
U1J
U
Uu2J
QC Limits
( 70-121 I
I 81-117 1u 4-L2Lt
7 4-87 -37 4-83-975-0 1-475-00-375-09-267 -64-L75-15-075-35-475-34-3156-50-5
67 -66-3t07 -06-278-93-3
7 1-55-556-23-575-27 -4108-05-4
7 8-87 -51005 L-02-679-01-579-00-s
7 L-43-2t24-48-L1006 1-0 1-5110-75-875-25-2108-10-159 1-78-579-34-5L27 -L8-4108-88-3108-90-7100-41-4100-42-51330-20-7
ide
,ormhloroethane
,
,
I
te
-Tr
-Tr,.z ene
o
J.S
1 ,
Unlesquant
v
1
oroDroDenevinfl Etherrm1-2-Pentanone
Benzene
Xylenes
2,ac
89r84t98r
not
Quqntancl s ion
ullln.
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
fluali fiers:lirnite.
I t waterforareima
samole data.ibrhtion limits.18, Part II,1e5s than the
and
ts arc)
B=E=*=al0-t
8
cgncentrations and POL,s for soils arebasis. (NA = not applicable-oi-noE-available)
CryA
ILta ona
Quality Assurance OfficerD ParkerJ
- proved:
;;-;'iifi inil iHFilHETnREgtl
a;s r'.,;-i amr-1 .rI':
BB',48rl l?qa 1ar:rr:t agrjo
4 ii.j !i a:i i:h
I-l
1
i
I I
l\
I0
a$r
I_lIt+i
J
--t
J
1
1I
"i
r.!
a /i
ILrl,"1|e.l
i
I:'?,-t
I
LNr./t
Ut
t
I.,!
1E 11 14 1r, 1g ,l
Ouant |1utpr-rr Fr le: 'uU].t+792:D2
Uflt,a
Dala F"r ie: )[,t1.4J9: :t"rlii.l;;ie : ;ii Li i, 1,2: .;' .'l-r11 ;.+l:l-. I i-,'Pl"lrse: 5;5i5. 0U : ll:5i tJ:09;.,'111.."90 i
id Frle: lL: il i4::lillrtle: IL) FTLE Fliit iit,i-'LHUi>( ttti..lEi-,;st Lal ihrat :,:n! !ijUtiiiJ i:-i: ij6
L)u;ratDr IU:ili.;rrt T:;ne!Inler:ted at:
ELI[,il,j iii:, i 0I ll :.i9, 1 Ll
14:1:'-ta.zr
EVERGREEN NIALYTICAL, INC .4036 Youngfield- -Wheat Ridqe C0 80033- (303) 425-602L-
VoLATTLE ORGANTC Ar.grysrs REPORT
ens A-3 6x206L705/0L/9004/27 /90os/ L0/9005/L0/90
N
ent ro ect No.il-225
77 651. 118260 ( 8240 )SOIL>v1439
R8051090
teDateDate
No.lution
Da ? YlN le No.Blank No.
coNcttg/RgCOUPOI'ND cAs *PQt*ug/Kg
Pyridine 110-86-1 U 6
:rogate Recoveries:
Toluene-d8
QC Limits
84t ( 81-117 )
Po"l ifiers:not ted abovedetection limits.
J=
B=*=
s water.iss,tttaion
tI a
0 ts ts
and sVol.are
amole data.1B-, Part ILle3s than thetrumentunn.a concentration outside the ca1gncgntrations and PQL,s for soilbasis.
ibration limits.s areonalre
c .7r\Approved:
D Parker Quality Assurance Officer
TiiT At tr-rrJ nHFi'tHttTnBPittl
ii !.e i,ti14 3 6& . 0 eor,-r.ITI!:
4 f)!.t Eri 1 ErB a qE
4 i_. i.t { rj
;. a r,) r-t
$l
Ii-tl
L1
I
s1
1
1et
'1.1
1..:'-i
1.'l
-l
B
?(l
4.4
AE
ra
!!AA t)
i: !:,
., rr0u
!4 1 a 1"1 th
Uata
I r'J lllEl .
lll5Ur
Frle:
zii,Jh L
5 :5;5
)t.rI4iiJ::tJ1.:ti,)'"'f-,1,;iUL..0u;UtS;tt;;iP
, / Lti),/p ti i
PvI t.i
Ut-rant [-.!r-.ito,-, I Frle: "P'l 439:.zDZ
iJ
ld f-rie: i[) P"iR:;ili-['ri.ie: IdErrTrf t,:dttr-:rn olLa;t ;-alrbr'atr--,n: ':;.i l-l '11 ;-1
Llc,er€t'lr lU: EL|Hi.lU,::rrt J r,ir8 i ?i-ti-lr.r 1 IInlected at: 9l-lU$l.0
ridrr-ie
.1I
iU:;iLltJi
EI/ERGREEN NIALYTICAL, INC .4035 Youngfield wheat Ridqe CO 80033' (303) 425-602t'
VOLATILE ORGANICS AIIALYSIS DATA
A-x2
0
0
0
0
3805675/OL/904/2? /905/04/905/04t90
L3.2N
--teDate e
DaDate
Perc Loss on
Compound Name
Prepared
t?Drying
Conc.ug/Rg
5
( 8240 )
390490
"E?*;
Cas Number
nott
Client Proiect No. z M-22Lab Pro'lect, No. I ?765Effectife Dilution : 1.15Iuiethod t 8260Uatrix : SOILLab File No. : >V13Method Blank No. : RB05
11111111
5110
6
5
5
6
6
61106
6
6
6
5
6
6
6
6
6
611
65757
5
6
6
6
5
5
6
UuU
U3J25J
U
U
U
Uuu28JIUUuUuU
U
Uu
U
U
U
Uu
Uu1J
U
7 4-87 -37 4-83-975-01-475-00-375-09-2
57 -64-t75-15-075-35-475-34-3r.55-50-5
6? -66-3t07 -06-278-93-3
7 1-55-555-23-s75-27 -4108-05-478-87 -51005 L-02-679-01-679-00-s7L-43-2L24-48-L1006 1-01-5110-75-875-25-2108-10-159 1-78-579-34-5L27 -L8-4108-88-3108-90-7r.00-41-4100-42-5L330-20-?
II
,
,
,
oride
f
roethane
-2-Pentanone
Benzene
Xylenes
iers:analvzedlimitsan estima
n tb
a
0
2
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
,zene
Unlessquanti
88t103t96t
abovedetec
U
UBJ
QC Limits
t70-L2Lr
I 81-117 Iu 4-L2Lt
I ts.s
Po"l forare
B=E=*=
c s or reaoent water, but iscaIankQuanands
Qu
at and sarrole data.calibrhtion limits.Vol. 18, Part ILare less than the
s
ts strument
ts
4 tsrunn.trations and POL's for soils are. (NA = not applicable or not available)
t-U/1.- t *,fr---proved:
rs
ona
Parker
co
Quality Assurance Officer
OTFL ION CHRONCTO6RAH
i le >V1 g
L6ggg
L4A88
L"gga
Egasa
6ASgS
48968
?gsas
amu.
T
2o6go
16 18
Euant 0utput Filez ^UL379zzD7
tag
r\r
Itt'nJ{
IL4
lo
I
ltt
rO
I
!J
IIAo
II
Lg 14
BLDC;0:0
DBFTLrat
e:
B5c.at
I
Dib
d Fi le:itle: Iast Ca I
Data Fi IName: X2Misc: 5;
I
TL
>UL1J9 z z
67 ;7765 ;45 .01; 0 ;5;RP5t04/90;
242 tYlLE FDR APPENDIX NINE !'OASion:900504 L5zL4
Ooerator ID:Euant Time:In jeeted at:2Lz D42O237
11I KE9005D4900504
EVERGREEN NIALYTICAL, INC.4036 Youngfield _wheat -Bidge CO 80033
( 303 1425-6O2L'
DaDaDa
'.ent
te
38056?sl0L/904/27 /90
5./ LLl905/ LLl90
tete
VOI,ATILE ORGANIC ANALYSIS REPORT
A-x2
0
0
0
0
Client Prolect No. z lt-22Lab Prolect, No. 3 7765Effectife Dilution : 1.14Method z 8260Matrix : SOILLab File No. : >V14Method Blank No. : RB05
5
( 8240 )
741190
Prepared
t? v/N N
couPot ND
Pyridine
:rogate Recoveries:
Toluene-d8
$uali iers:
an estimaEPAfound
ed forare
L
n sco umn.
we
reaoent waterbut is
and sample data.Vol. 1B-, Part If ,s are IeSs than the
cAs *
110-86-1
11lt
de
coNcug/Rg PQL*uglKg
abovedetec
U
QC Limits
( 81-117 )
ts.
5
B=*=
siUnlesquant
L
L
E at a concentration outside the calibration limits.cgncentrations and PQL's for soils aret basis.
Cfn
ta on
ge
a
anproved:
D Parker Quality Assurance Officer
"i'i2\. InH nHFr'lilATflGPgtl
: !. = itjl{7{.9-e69.8 amu.TI'j
4 V h 1 Arl 1 8B B
OB
1ri,:rr?ftr?l}.
1I---{!'!aSalyJI
-t
9!rL*r!rlff l)I?.-{!ii{fira.i' ' - - - -Jt
itrii;iAFA'- --l
J
'J y-r r:r ! r-r rtF
.:
.1,-i i;13 fll
.l
30rri6O-ll
I'-rri t, 14tt t!
e{
I
u1
n',
It4
iLt
1 ? L4 1'5 18 [t c
t-;d t ct
I rE ttlE: .iil.=tr;
Fr
,
lE.
2 Ulre,:'rlrc:,.)./.
t-.l l{}ri; ; l,,ti
,i rr r'fy t_;, : ,, L] L.tt4;u;5!u;: i?P
U 5 r'.1- l,'11 U :
Ou, nt Outpu,t Frlei ^V'L4742rA2
id t-r il'rtle:
L'=.) L L
e: lLi i:r'iH::11 LI,Jer,Trf rcatrsrr Bfa I rbrat r'rn: lliLi':ril.$lr r', l'I Ll
rrdlne: ;-lB
ug=
Ur.;a-t tt
erator Iu: BLIHant Tin'ra. li)Ub'1 'I
lected at: 17U051:L
2U:0$19:lB
EVERGREEN AIIALYTICAL, INC.4035 Youngfield -wheat-Bidge co 80033
( 303 )42s-602L-
VOI,ATILE ORGAIIICS N{AI,YSIS DATA
act?ss on Dry
ene loride
sulf
Client Prolect No. z lt-22Lab Prolect, No. ? ?765Effectife Dilution : 1.16Method : 8260Matrix : SOILLab File No. : >V13Method Blank No. : RB05
Conc.ug/KgCas Nurnber
not
t ta ion
ts
umn.
A-3 10x2056805/0L/9004/27 /9005/04/9005/04/90
N 13.5
5
( 8240 )
tete
chl
-D1-D
ene
ing 400490
Compound Nanre
"E?k;
L2t2L2L2
6L20
6
6
5
5
66L20
5
6
6
6
6
66
6
6
6
6L2
55858
6
6
6
6
5
6'6
Uu
U
U
UL7J
U
U
U
U
Uu18J4J
UUuu
Uuu
Uu
U
U
U
Uu
UU1J
U
7 4-87 -37 4-83-975-01-47s-00-375-09-267 -64-L75-15-075-35-475-34-3155-50-5
67 -66-3L07-06-278-93-3
7 1-55-656-23-575-27-4108-05-4?8-87 -51006 L-02-679-01-679-00-s
7 L-43-2L24-48-L1006 1-01-5110-75-875-25-2108-10-1
59 1-78-579-34-5L27-L8-4108-88-3108-90-7100-41-4100-42-51330-20-7
2
oroethene
v
-2-Pentanone
zenezene
r
Xylenes
Surogate Recoveries r
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
hloroethane
analvzedlimits for, buarean esti"ma vAtbat
3
U
UBJ
QC Ltmits
170-L2Lr181-1r.71
l? 4-L2Lt
I tg.
77*85t86r
iers:QuaIiu=
J=
B=E=
abovedetec
t
andcalVol.are
CI
or reaoent water, but is
concentratlons and POL's forbasis. (NA = not applicable
samole data.ibrhti.on limits.18, Part If,leis than the
s arenot available)
n
€,s
eL
noteddry wea so11or
C-r'11-hL---proved:
Parker Quality Assurance Officer
OTAL ION CHROTiPTO6RAIia)v .O anu.
4 1 s
4400
4gogo
36000
3zggo
e80go
tq
Itt
?-4gg NI.a
D
I8
zsgsa
t60so
L?gao
cl
Iar)bl
Ian
Ia
1e t4 6 ?
Data Fi le: >U1f40: : B! - Auant OutPu t
Nama z X2D568 i7765;408;RPMisc z 5 i5r4.99, 0iS i0 iB5/04t90 i
Id File: ID B24z:l1tTitIE: ID FTLE FOR APPENDIX NII.]E UOASLast Ealibration: 900504 L5:L4
Fi le z ^UL140z zD3
OoeratorUuant lrInjected
ID:
m6:at:
MIKE980584908504 2L2142Lz D7
EVERGREEN NIALYTICAI,, INC .4036 Youngf ield_ _wheat -Birige C0 80033
( 303 ,425-602L'
VOLATILE ORGANIC AI{ALYSIS REPORT
A-31005685/0L/904/27 /905/ LL/ 905/ LL/90
DateDate /Prepared
x2
0
0
0
0
Client Proiect No.Lab Proiect l[o.Effectife DilutionMethodMatrixtab File No.Method Blank No.
t4-225
77 651.158260 (
SOIL.>vL47RBO5l
82401
? Y/N N 5190
couPorrND CAS *coNc:uq/Kg PQL*uglKg
Plrridine 110-86-1 u 6
Surrogate Recoveries:QC Limits
Toluene-d8 100t ( 81-117 )
8""1l-iers l t for,abovedetec repo5ti4gr-on lrmLt,is detec
limits.for reaoened, but istsS t water
B=*=
v tcalanktal-on '8tk*sr{845,limits
s a and sample data.Vol. 1B-, Part ILare leis than thet
8 tstrument tscounn.at a concentration outside the caIil ibration lirnits.e noteddry we cgncgntrations and pQL,s for sot basis.s areLat
c nt a^^^LArrroved:
ona
Parker Quality Assurance Officer
: l:,f,r l'
::=' I i'.1
<.{
r.l :-l
.a. $.
' i ': :.i.
.fl -t. .:t.
:.' "
-- trr r0
::L .-'tl
':1-- t
!f !'Ui.,:o.1 .1' -
{-r. j f''i"-t*
tl,;
1-1:ll
-'..t_JrI -{
+:1
E :,1rl ::.., .-:t.:. -'.. ,n ..."u.:
'1.. - ,-:
-4'l- a r'l+' ,n
-.i ,.- I.'rI'f)'n-
rU i.l
- rll
.t. '_. 4-'.-. rr)1l -'o
--- J
,.1
t
r-f ,
!"..t
Itt
."L
:U.
--.t
t-'
,t'
J,:3
i].
,l
-t
,:t.'t. .f,...:]
.l ..
-,l :.-,.-t"
"-...11
''..tr-T- .-
,r'.:J
'. lr
rU :' -l'J--: I ..
- ;.!.
-.,..
rf O r-,
-f,:,
'!-l ,,j .-
::r.: ::
.!iu
"at.t
rl
,:,r!
-trl
,.1_it
_t{
,:i
::lli,
-......4.--.-. -r::--- 1.:..:'Ir
,.i.i
a-c
';'-:il
i1--- ---
:,,j,
NJ
..a.
"{
,r, .,i,
(r.l '*:
,!'
Gr.-fi..
'it'3.'t
t':.;,
,:.
..;
l.-l
t-.
ir..
L:
L'ri(
U
t--,lL.
r-t-
,c
t,
ri,-t
i'J H
it i-
-te
fll
(!
rn.(l
rU
Ifrr
r,
rlt-'1.
-l
0r
,:I
at(!(:|-fl
CII.:-
,:
,.rt-
f-il:
Date
EVERGREEN A}IALYTICAIJ, INC4036 younsriet$o3ytillr8ltr" .o 80033
VOI.ATILE ORGANICS AT.IALYSIS DASA
Prolect No.'lect No.fe Dilution
t Loss on ?Drying No.ank
A-3 L2x2055905/oL/9004/27 /9005/04/9005/04/90
N 22.5 No
5M-2277 651.318260SOIL>vl3
RBO5
( 8240 )
4L0490
POL*uqZrgCompound Name
ide
sulf
ropropenec
1 L,-Tr oroethane
13131313
7130
7
7
7
7
7
7130
7
7
7
7
7
7
7
7
7
77
13
7
6555
77
7
7
7
7
7
Uu
U
U3J18Ju
U
U
U
UU26J
7
Uu
U
Uuu
U
Uu
Uu
U
Uuuu1J
U
Uu
7 4-87 -374-83-9
7 5-0 1-47s-00-375-09-2
67 -64-L75-15-075-35-475-34-31s5-60-567 -66-3L07 -06-278-93-3
7 1-55-5s5-23-575-27 -4108-05-4
7 g-87 -51006 L-02-679-01-679-00-5
7 L-43-2L24-48-L1005 1-01-5110-75-875-25-2108-10-1
59 1-7 8-579-34-5L27-L8-4108-88-3108-90-7100-4 1-4100-42-51330-20-7
Cas Number
89t94r1031
Conc.ug/Rg
,v
-2-Pentanone
hloroethane
eneBenzene
Xylenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
ifiers:
'Art
,
OualO=
B=E=*=
abovedetec
1BJ
QC Limits
t70-121)
I 81-117 1u 4-L2Lt
I ts.
ec
and
or reaoent water, but is
ide thesw846,limits
calVoI.
samole data.ibrhtion lirnit18, Part II,IeSs than theare
and POL's for soils arenot applicable or not available)
Approved:
John D Quality Assurance Officer
E
TDTNL ION CHROTIFTO6RAI'IFile >?1 1 g
34000
e8a6B
e4
1b
,.EBBA
8089
Data Fi IName: i,{2l'lisc: 5;
amu.TI
1
A
a'
r+
Itn6
tl
I,4
l.{I
FI
Ilr)t't
It4
Ie
e. >U'1741::BL
B56F i7765 :4Drl;5;4.94it) iSitl;t-r
IO 824: : l'11D FTLE FDR APPEND I:( N I I"IEibrat rDn: P00504 15: l4
14 16 B
Quant DrrtPUi File: "u1]41::Of
I.JDA:
B e
RP
5 ,, i4,'9 t) i
e
ld File:Trtle: ILas t lla I
Bnerator ID:rf,uant Time:Injected at:222 042L277
11 I F:El?0D504t?00504
EI/ERGREEN AI{ALYITICAI,, INC.4035 YounsfietSorTt3Slr$itg" .o 80033
DateDate PreparedAnaxtract? Y/N
COUPOI'ND
Pyridine
Surrogate Recoveries:
Toluene-d8
VOI,ATTLE ORGANIC AI.TALYSIS REPORTPAGE 2A-x2
0
0
0
0
Client Pro'iect No. z 14-22Lab Proiect No. z 7765Effectife Dilution z L.28ltethod z 8260![atrix : SOILLab File No. 3 >V14Method Blank No. : RB05
3L205695/OL/904/27 /905/ L2/905/ L2/90
5
( 8240 )
N 90L290
cAs #
110-85-1
116t
coNcug/Kg PQL*ug/Kg
U
QC Limits
( 81-117 )
CfzL f,-,*L
6
8""lifiers:
ter?-
B=*=
E=UnIesguant
A-.roved:
Parker Quality Assurance Officer
:.1:J
=:-l'.f,
:-{
tll
I
,l-
+.
f3
4-',
ro.ll
+ (.1f) ,t
L .:J
-. .::t.
i.,n..
tL"':....:s r
l'' ,n'.; C'-< 'lt.01la
lD 'Il--...-!
.. tli
.t- -'+'r.t0
1--l i ,!:
-.L-.)
::
:a
:{Jl.\.r.:,. . .-:1,...r .-.
......f]
]..u=1' .-.:, .. .o
,' :r. ..8 -1.
o :l-.-r,t
-':1"
.I
ill d) Jtr.. il: rntr ..1 --
-./. :._
;lJ
r:,
6,
,!.o
ot
ltr
h
(:''oJ
'r-l
.ir'rl
nr{
,.11r{
tr
.,.I,
..r'
.n
.'1-l
':!'
'jj
.t.
..t "
rl
i:'
,:iol'r-l
t'r
n
l!
T
I
F
n
c'
t..
c:
t:
-,efn
of,
Il r\.
d:{
atr
t
:{=
'J,,l.l
:-r J
':{:{
--.{ i{
.,.1 J,.r:r:: =
...------.:-
( -:\1r
Irl..,}.
-1..s
-rDt!
L -Er:'- lll
rll +, r_iL.:[){' ,. -'
,-r..i-
,n
(sr..(,
GrGr-rt
.,
I
Sr
ri
s.t,
_t i'ia
':il,:]
'.i.t
...1
.t.
rl I;t\,
i:...:'
;l,i'-l-r,
:i!:iil
,.1
l't r -r'-
G.
,::.::.,
';1,'' r',1;T'l-r't,"' rr .l-r' t'r ---'r1
r.r :t (i, :r {:,r:1 :r (i .:r ci
f:., .ri ltt ,tr !tilt el r.t
'r'l-T'j,,r
TTt:
(:
F(l
nIL
.:
;it.(-
l-
EVERGREEN ANALTTICAL, INC.4036 Youngfield_ -wheat -Bidge CO 80033(3031425-602L' .
VOLATITE ORGAIIICS ANALYSIS DATA
DateDate
Compound Nane
sulf
-D
Prepared
xtract?Loss on Drying
C1ient Prolect No.Lab Prolect llo.Effectife DilutionMethodMatrixLab File No.Method Blank No.
31405705/0L/904/27 /90s/04/905/ 04/90
2L.5
A-x2
0
0
0
0N
M-227765L.278260SOIL>v13
RBO5
5
( 8240 )
420490
1
1
1
1
ride
seona
for,
13
13
1313
6130
6
5
6
6
6
6130
5
5
6
6
6
6
6
6
5
6
6
13
66464
6
6
5
6
6
6
5
7 4-87 -37 4-83-9
7 5-0 1-475-00-375-09-267 -64-t75-15-0?5-35-475-34-3155-60-567 -66-3L07 -06-278-93-3
7 1-55-556-23-575-27 -4108-05-478-87 -51005 L-02-679-0 1-679-00-5
7 L-43-2L24-48-t1005 1-0 1-5110-75-875-25-2108-10-159 1-78-579-34-5L27 -L8-4108-88-3108-90-7100-4 1-4r.00-42-51330-20-7
Cas Number
not1yue
Conc.ug/Kg POL*ugZKg
Uuuu5Juuuuu
Uuu10
UUuUuuuU
Uuuuuuu
U1JU
U
U2BJ
QC Limits
(70-L2Lr
181-1r.71
l7 4-L2Lt
1f
tanone1-trric
,
c IC-Tr1ene
,
,,
v I
-2-Pentanone
Tetrachloroethaneoroethene
zene
neXylenes
Surrogate Recoveries:
J an esEPA PIow
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
fluali iers:
89t96t98r
r-onB
E*=
lccrti \fe concentrations and POL's for soils arebasis. (NA = not applicable or not available)
C-n^-h^3Approved:
D Parker
el-
Quality Assurance Officer
'LlTiL I ON EHRONRTD6RB}1e >v134
3600
3aB8
a8860
?44
egog
t6gaa
teBgg
BA68
4qF)D
Data F
Name:llisc:
0.0 amu.
24: : 11LE FDRbrat ron!
>rJtJ42z zBL
D :??s5 : ciDl: : RP
. 0r ; o ; 5 ; D ; Li' 1Dl"ct) i
4 aa ga
q
r"l
Ita
at
Ia
aJt
IL,)stl
a{
Iantt
I9
Ib\o
1a 414 16 1
i le::{20575i5;5
D
I
e
lla
d Firtleast
Quant Dutput Fr le: "'U'13+22 zO3
I
TL
ID BFTL
Doerator ID:Uu.3nt lrmE3Inlected at:
NIKE9DD5D.t?00504
AppENEtIX NIt{E r.JDAs9D0504 l5: .1.4
214:072222
EVERGREEN NIAIYTICAL, INC.4036 Youngfierd- -wheat -Bidge CO 80033
( 303 1425-602L',
VOI,ATILE ORGA}IIC NSALYSIS REPORT
t 1e A-x2
0
0
0
0
31405705/0L/904/27 /905/ LLl905/ LL/90
e Client Proiect No. 3Lab Prolect No. 3Effectife Di.lution 3Method 3Dlatrix :Lab File No. 3Method Blank No. 3
yt-225
77 65L.278260 tsorl.'>vL47
RBOs1
DaDaDa
Da
tetete ./Prepared 8240)
T? Y/N N 7190
COI{POI'ND cAs *coNcug/Kg PQ1*ug/Kg
Pyridine 110-86-1 U 5
Surrogate Recoveries:
Toluene-d8
QC Limits
97*( 81-117 )
fluali Lerg 3 analvzed forlimits are limits.for reaqent watered, but is
B=*=
a an estina tectowEPAfoundtbPOL) .616nk andSI{845, Vol.limits areInsamole data.1B-, Part ILleSs than thetrumentQcoIIIIIII.s at a concentration outside the calibration li:nits.I cgncgntrations and PQL's for soils areht basis.ta on a
onu;it-roved:
J D Parker
g
Quality Assurance Officer
l\.'r'J
'i:.{
: ra.l
--{:l:{{
': il"
. 1 ._-, ::r
;o .t ,l'
ii .. .,*lll 0.:
L..TJrl'...o
rF+. UL '--,Li,rj,n -l
'__l ' :1 -a
tti.:
rJ :od ::r
L..
-.\-l-l
[:-l
! :..{rl --l
-, 1.,
.L. !n..
It. - ':,
l!, rtl
.-i': i-< rt 1l1l -.
0.1 tE-{.. _-t- rll
.,-. re'rl .' o.---._t
:r.f
i\
'1-{
()
lJ_
o
.lr:l
+'
tr
rE
.lr_l
:.
':l^
:.1
:f,r'
.. :,:
- =..-'-. l "'
1. u ._'
'f- --
. { :-l
/: -..'.. J'.
'Ll :'t -lJ*...t ".
!L
.fl |lr {.!
r; i: illr0 ,| '-.
-..r.^ i.
o-t
,i:,
Fl
.tr
rr'
fl
,:.J
t{
j,
r{
,l\
t.-.sl
--:-:--
'r'la'r l_f rC. (ir{i (;.tl ..;:,'i' fi'C:, 1;,,, r"l
i--:;!i
r l'l-f rrt r1 i'l;rI
t:'
't,
,l
.:
tt.
:r
4.,.
r: ;.,:i.l
t.'rrtl'tlii,
::,
':r.:i(it.
,!,r'r'1-'.3r 3.:. :.,,i' :!i!. :ii
l'I!1-l,
rli.rl
:
t:i
iF------
l-r
l5l
:: l..t .,. l:.
.rl;t-(:
t-
lr'
,5'.:,-7
ir:,
EVERGREEN AI'IALYTTCAL, INC .4036 Youngfierd^^wbeat-Bidge CO 80033
( 303 )425-602L
VOI.ATILE ORGA}IICS A}IALYSIS DATA
rnt S
xtract?Percent Loss on Drying
Compound Nane
ene oride
frr
-Tr
Client Proiect No.Lab Prolecf No.Effecti.fe DilutionltethodMatrixLab File No.Method Blank No.
1657L/ 0L/90/27 /90/04/90/04/90
15.6
A-3x2005040s0s
N
l,l-2277651. 188260SOIL>vl3
RBO5
5
(8240)
430490
POL*ugZKgCas Number Conc.uglKg
c
1
1
2
1
,
,
L2
L2L2L2
6L20
5
6
6
6
6
6L20
6
6
6
6
6
6
6
6
5
6
6L2
65959
5
5
6
6
6
6
6
U
Uuu3J23JU
Uuuu
U
U
8
U
U
Uuuuu
U
U
U
Uuu
U
Uu1J
Uuu
7 4-87 -37 4-83-975-01-475-00-375-09-267 -64-L75-15-075-35-475-34-3156-60-s67 -66-3107-05-278-9 3-3
7 1-55-655-23-s75-27 -4108-05-478-87 -51005 L-02-679-01-579-00-57L-43-2L24-48-L1006 1-01-5t t 0-75-875-25-2108- 10-159 1-78-679-34-5L27-L8-4108-88-3108-90-7100-4 1-4100-42-51330-20-7
ne
te
1
,
4
2
U-'est
zene
2h
si
Benzene
a Xylenes
Surrogate Recoveries:
iers:
ow
oroproDenevinll Ether
-2-Pentanone
hloroethane
tb
tat L
m]-nhnt co
2BJ
QC Limits
t70-L2LrI 81-117 1u 4-L2Lt
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
8""analvzed forlimits are
92t98t104t
B=E=*=at
water
Sr
Approved:
onsea
J D Parker
edawei cgncentrations and PQL,s for soils aret basis. (NA = not applicaEle-oi-noE-ivailable)
Quality Assurance Officer
t1o
r\
'..:f
tnrd]
&t
LL
f,
o_
f,r:l
ColBi
.!
r0iI(f
UJ
Hd
7-1
EU... r:l ..
.. lr c.f,o
f.lLJ a
olJ!Fo0l-t- l-
-of1 a
'. ".nI tf\ .-$€otrrr' ..,
FlN}\
lr U:..r....
ood..tJ'd cth-p+.t0
T-O
-F-J
o; Ll+,8 ot0O-ozE
clo
.f,
l='
tt'
C.ril
@r{
,r{
OJr{
ql
r{
s-5s
E-S
u -s5
e-sr
li tf.
oz'tulc:rtIIJ\(L6
<f (f
G.
rt ['.Clt \
tf\ c..lC{r:'l
it \i.aa
tdtf.tnYoo
Eo.l}..
..1
0_o:.nJ
-{fJ "'COc:c=.... .-.
ll!6fJ)
-c\'1-:\t(\h
t-ss
t-sr
O.. +,
-rDlI!ELiEof- fl)
|IJ+,OLC(|(lO-,o_l cr_rCf*aGoodul+
(oOOGTO(D15G@O6r.9G,G,O6o.(T,t-rOr{
Gt {96,66rO6rO(tJ flr{ rl
6l
Gt(ll-
o.,
GGiO-rl
&G,ol"r{
o@-@
@o-:t
aC.l
FTtc)FI
o
l&
(lc.9
CtF(t
cICl
.:t
J(f
F.Ci
EVERGREEN AIIALYTICAL, INC.4035 Youngfiefd _wheat-BlQge CO
( 303 )425-602L'
80033
VOI.ATIIE ORGAIIIC AIIATYSIS RAPORIT
DateDateDate PreparedDaact? Y/N
COUPOI'ND
Pyridine
SuEogate Recoveries;
Toluene-d8
8"'1i
A-3x2005040505
1657t/0L/90/27 /90/ LLl90/ LL/90
Client Proiect No.tab Proiec€ No.Effectiie DilutionMethodMatrixLab FiIe No.llethod Blank No.
t4-22
77 651. r.88260sorL>v14
RBO5
5
( 8240 )
N
coNcuglKg
781190
PQt *
uglKgcAs #
110-85-1
91t
not
ronstss
u
QC Limits
( 81-r.17 )
1 ts.reaoentbut iss
,
ibration limits.s are
6
ters 3 analvzed forlimits are abovedet,ec
n
waterJ
B*
an estirna
EPA ac afound "8thnsw846,limits
stb=Pr a
0
and sample data.VoI. 1B-. Part ILare IeSs than thescounn.E=Unlesquant henriseedona
s at a concentration outside the ccgncgntrations and PQt's for sot basis.
alilsitatlre
C //L h-LApproved:
D Parker Quality Assurance Officer
'Ll
1J -t:'
:.1
:
1la:...i
.-t
7
o
I
j
o.
_1
t_1
4.r
tr!
_1:l
::.
t.
:J
-a,1.
".:r. -f'
-r ..-r .:.
" " lll
.r1 .t....
,' .-
-:....-
., l.'.. j'".
rll :-i -l-l
.. ... .J\
I
o|l]rj'r.. 1! r,'if ,t: -.
_l :: r-
j.,-.
f,$r
1.,:' I .:\t
:'l :{
:{ e{
:t-J :t. ,--t'.
.f.'J.
-F:{
f_ -l
r.'l :tr
: ..... r0 ..
I-,:l- !.'l -+
l.r.,tl
.J1:L- . 'li .t-J.'-i -
rl-' In-- .. .-l.(Ll
:\,:rllL<
-,lr tf
L -.'rt
r:r -- ili
O r, r-':..i lL,,li t -,
J..:i'"
,:,.i'']J
,5'il
,l':lrl
.4,r!
.,
rl
rrJ
rl
': -t:il
,5,
.1,
,J,
OJ
.9
.f''
r{
,s,
otd
;;;
ar
5r,3!t
L.'- :, : --
.'T..
:lEal
,
tri
.tlh.,'-t
0r
tr.
a
CI
Fcl
ua
':
;i
1:
:d*''.i..;
h-'.
'll'-r-l:'I-'. -'r-'t 'T' !-. r'.:. :,, ...i rtJ rIr:;, :.! .l ..:i ,;)r:.! lr ,.r fi. r:i.:.r :. {,, ':l' .;i:J ,r rr tl r?it r..l rl r.l
" .}-'- l;-.:r '!r':r ':l
.:) t(!
t' - - '----;[, ''-;1, ''_-'_t-
(i
r::.(i
t;,.,
e;,
cir::,
lr:,'t'r! lal
-l- '4f..rOn-,n-.-..:
.l
'!,'lIr0i
EVERGREEN AI,IALAICA!, INC .4036 Youngfield -wheat-Brdge Co 80033
( 303 )425-602L'
VOLATILE ORGANICS ANALYSIS DATA
40)82
vt-225
77 65L.228260 tSOIL.>v136
RBO5O
31805725/0L/904/27 /905/07 /905/07 /90
18.3
A-x2
0
0
0
0
N
DateDate
s
Loss on
tqd/Prepareded
?Drying
Client Pro'iect No.Lab Prolecf No.Effectife DilutionMethodMatrixLab File No.Method Blank No.3
7 90
Ii[e
7 4-87 -37 4-83-9
7 5-0 1-475-00-37s-09-267 -64-t75-r.5-075-35-475-34-3155-60-5
67 -66-3L07 -06-278-93-3
7 1-55-656-23-575-27 -4108-05-478-87 -51005 L-02-6
7 9-0 1-679-00-57L-43-2L24-48-L1005 1-0 1-5110-75-875-25-2108-10-159 1-78-579-34-5L27 - 18-4108-88-3108-90-7100-4 1-4100-42-5L330-20-7
,
,
Compound Name
or
ide
oroethene
oroethane
roProPene
Tr oroethane
,I I
-2-Pentanone
,oroethane
Benzenet
8""Lers 3
EPA Pracin
al0-
si tse tedwe
Xylenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
Cas Number
v
Conc.uglKg POL*ugZKg
Uu
U
U
UJ
U
Uuu
U
U
U
U
U
U
U
Uu
U
U
U
U
U
U
U
UuuBJ
U
UuBJ
QC
t
1
1
L2L2
L2L2
5L20
5
5
5
5
5
6L20
5
5
5
6
5
5
6
6
6
6
6L2
66161
6
5
5
6
6
6
5
40
10
nschl
- r2-
9lt85t8lt
abovedetec
Limits
70-121)81-117 1
7 4-L2Lt
1 ts.or
,
1i
=
=
esIt
analvzed forlimits are bu not detec
an estima s reaoent waterbut isJ
B
E*
a
CIon
s
1hr
s ta t-on
Cl
andsca11.
soils areor not available)
C,tl/L fr*L
samole data.ibrhtion limits.18, Part ILless than the
ionintIect €s are
concentrations and POL's forbasis. (NA = not applicable
Approved:
on
D Parker Quality Assurance Officer
Tn Till I nH ,lHF'nnOTfl6Fgt1
35 . a-a6a .a0Du.
53':rEEtrrJ
.l
i,i ri*;:.r'ri
l
+i,.tziii|_H
:; i.r tl.l t:la
I
q I 6
I
I
I
I
I
I
I
I
I
I
{
llrl
ii
ti
il
6
llji:..:r6tr-,r' IL' : Bl-;U.,' - - r T .. . ' ,'-t.,t),':t'tl I riirE; i,l.:'1."-'tir'rlected at :')tiu'7U?
el:t.18
r..,1
I.:.i
.{
fij
i
j
ia
I
I
I
I
I
f.
'r)i -: ri ir r:t irr-" "'I t
i
I1r,rir:ir:rr-r
!
I
a
1rl 1: 11 16 1ts hal
C,si:a Fi ie: >t,rL:,ta)'::Ui [luanti,,,iir€: . lU'r.'::.i.''rti :-;-; i.. ..:Pl"li :c : 5 iS:9. U2 i u ;l-,i,i i U':' ;0)i'YtJ :
.,i i-rie: iU-::; 'Ji:::i:
rrrle: Iu FTLL FU;'rjiFl-'i-l'iul)( t'.{ltlE tJu;-:
.-,i5t i-a I lBrai i':,r-,: 'ri-l i-i!';j 'r !1i"")
Ur-i tpi .Fr le:'.t.tl_jo-t:: u-}
L/ . !.,L6:5Y
EI'ERGREEN AIIALNICAI,, INC.4036 younsriet$or}XEtlr$ltn" .o 80033
VOI,ATILE ORGAIIIC NIALYSIS REPORT
A-3 18x2057205/0L/9004/27 /9005/ LL/9005/ LLl90
N
DateDate
Prolect No.'lecf No.fe Dilution
it-22
77 65L.2L8260SOIL>vl4
RBO5
5
( 8240 )
? Y/N
COMPOI'ND
Pyridine
Surrogate Recoveries:
Toluene-d8
Qualiu=r-ers r analvzedIimits for,
le No.Blank No.79
1 190
cAs #
110-85-1
97t
coNcng/Kg PQL*ug/Kg
u
QC Ltutits
( 81-117 )
ts.reaoent waterbut is
e data.Part II,than the
ibration limits.s are
6
?-
B=*=
ot a an estEPAfound
s
a
are
tcal40-s
on
scEat a concentrat,ion outside the calcgncentrations and PQL's for soilt basis.
f ?rL
Unlessquantita
*Approved:
D Parker Quality Assurance Officer
.t -'
_ , :.1
.; ':'I
.-l :{.{{
.-tl -l :}.
.1..-'- 'll o
(- 1:r'l rli
O ar f-r. rl tll| .r' .'
..1.-l-
'L'
1:l ll
a :'-
t-. .,
:..1.{
i'
,a
.;-
.:
,T
rn
4l
+
r)
r-1
:--.!n.. ,-r
.l- '..:.,i: -l+'
a:
,(
t-l
tlr
I .-'i'l '-
f,
.,]
li
tr tt' ..:
;.!J
.].
',.i
!l!
:-t.-
t_.i-
f-'
,]
-.1
+'
r!.)
l
t.,.,,
' ::
.. I
t.-{
:tj
t-
(1,
i:
'tr{
r'l
,:..1
I
r
I
l'
Il-
I
)
..-4=::::F:-:--
i -...1 ----,=.:-:
I 'a'l
t...t
!.'i
,!,,l;-',t'
,:l.:.
t(- |l('
,:.,i,
ii.
'4.
rt.
'5,'iJ
,t,
,.t,
r,Jrl
F .:,
q:'
,!'..,
€:nt
t(r
,lr
t...-t
-l':.
0r
lr.
tl(!
(:
t-rl
r.l
ic
:(.
|::
;it-.:|-
t--c,'" c. 't',1
a' a'lr'r C. I 1
!'t
:ri!
EVERGREEN N{ALYTICAIJ, INC.4036 Youngfield -wheat-Bi4ge Co
( 303 l42s-602]-'.
80033
VOI,ATILE ORGA}IICS AI{AI.,YSIS DATA
Cr.r.€DLab SDateDate
tS
Compound Name
loromethane
or
ene
,.D
1 -D
Prolect No.lecf, No.fe Dilution
t{-225
Limits
t 7 0-L2Lr
I 81-117 1u 4-L2Lt
A-3 20x2057305/ 0L/9004/27 /9005/07 /900s/07 /90
N 18.3 No.ank No.
( 8240 )
640790
77 65L.2L8250SOIL>vl3
RBO5
ide
ormhloroethane
Disulfidehloroethenehloroethane,2-Dichloroethene
Cas Nunber
107t102t113t
Conc.rtg/Kg "E?k;
L2t2L2L2
5L20
6
6
5
6
5
6L20
5
6
5
6
5
6
6
6
5
6
6l2
65151
6
5
6
5
5
6
6
uUu
UJJuu
Uuu
U
U
U
U
U
U
Uu
U
U
Uuu
Uuu
UUBJ
U
UuBJ
Qc
1
2
7 4-87 -37 4-83-9
7 5-0 1-475-00-375-09-267 -64-L7s-15-075-35-475-34-3155-60-567 -66-3L07 -06-278-93-3
7 1-55-655-23-575-27 -4108-05-478-87 -51005 L-02-679-0 1-579-00-s
7 L-43-2t24-48-L1.0051-01-5
1 10-75-875-25-2
1 08- 10- 159 1-7 8-579-34-5L27-L8-4108-88-3108-90-7100-4 1-4100-42-5L330-20-7
376
,-D
QuaIi
B=E=*=
tanone1-Tric 24
,
1 -Tr oroethane
-2-Pentanone
oroethane
te
fiers:
cal40-
tat we
TolueneChlorobenzeneEthvl BenzeneStvteneTotal Xylenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
limis forted,
samolibrht
ts.rebutagentLs water
e data.ion I imitsIT,t,he
essnti
18, Partless than
concentrations and POL's for soils aret basis. (NA = not applicable or not available)
c,*4#Approved:
Jo
ona
Parker
ai
Quality Assurance Of ficer
No.u\nt
NT\
-l el
n.Nclott tf.0IEcfCl,3o(I),f,ro.
O.. +.*oo
EL.i!aF o)
Ov LlLCtrr(l)O-
TLf, CEB*
t0{lcl-:
trjzHo.Zm
x€
C)Zf'.[doLlr.(LE.t^
-{ t}
E(L..cr....tr c.rt o
c.{ Lrj -CDJ rFmOtr Ltt(f 'a
o(,a..Q.r 0lLl-ry+' t0'If,-(l
-FJ
to
.t
.o
r',
-l
0
tr
l
o_
iJ
la
cof13
o.
r\aTL\trtf.
"f,fJ'-C)6o.. .1.-......t,$tr..-.'€€t3r\r\ .^-{f\'t]'^c' . tfr .f\r... u\, ...
ol=(,d r...1 . \.-xu\t!
,0Cl(Jr-EOOlO-ozE
(Y)
rl
,G,{
t
AT
f{
r-ss
l-sl
O{l,O(3Org66l(o(ll6.6Gr'3&6,o(s'o6'6',s,o@G! lr., 13 l:, O lf, O u.!'' (.rr F, (rJ a.r, -t r{
i-ss
z-st
c-ss
c-sr
lf, n
(o0oo'@ u)!Om
oGl
6tts
il
U
F
o
aea|
a,
cta,tlt
Fq
EoeI(J
2o
J(I
Fo
EVERGREEN A}IATYTICAI,, INC .4035 Youngfiel4- wbeat^BlQge co 80033
( 303 1425-602L
VOI,ATILE ORGAI{IC A}IAI,YSIS REPORT
32005735/0L/904/27 /905/ tL/90s/ tL/90
DateDateDateDa
A-x2
0
0
0
0
Client Prolect No.Lab Prolect No.Effectife DilutionMethodl'latrixLab Fi.le No.Dtethod Blank No.
8240 )
0190
tq-22577 65L.2L8260(SOIL.>v148
RBO51
/Prepared
T? Y/N
COMPOI'ND
Pyridine
Surrogate Recoveries:
Toluene-d8
I iers:
E=
N
cAs #
110-86-1
94t
coNcug/Rg PQt *uglKg
U
QC Limits
( 81-117 )
ts.reaoent vraterbut is
e data
5
Ro"l
B=*=al0-s
Part Ithan i.the
UnIquaessnti r-setat !9e
sco umn.at, a concentration outside the calibration limits.cgncentrations and PQL's for soils aret basis.
C'?TL hr^r-lo---=roved:
ona
Parker Quality Assurance Officer
3
:t:rI
,t!
I
tt-
..:!
n
I'I
,J
I
I
I
I
r!
'..
11 _tii -:11 -
i.-,i!
,I'
!S,,n
'{
,ir.t'
':qt'
'$,
.r t-
:: ..
.l,'.t
..{ _{
.i, ', _l
'" ,1.. r
,.- . ll
r['+. I r
i.- . - .tr
!'
I r{
'1 ,,...
-. t "
-t-tI -.
rl! ..
., l:.'-t:. .- ..
l-r-: !i
-''il tlt
i.l
rl1 I
I..?::
I
F
E,tl
Gt
G|
t.
rll
t_
an
',
7.-l
.lr
lr
fltri!Cl.rt
(a
l.:
;f-
t.
,t.
r t'1'a l
.:
t
1,,(;.(.
t..l,
rrLlla-r,fr-rir l;'rr. j-rrr rlrl . ' )
!9t
fl
':.:,:!:i
,:1 .:
,:]
,::'
,:r.:r
:,
rl
,.:,
|:;
,,.:
ol
' ,.1
EVERGREEN AISAI,YTICAL, INC.4035 Youngfield_ -rf,heet -Bfdge CO
( 303 )425-602L'
80033
VOI.ATTLE ORGAIIICS ANALYSIS DATA
DaDaDaDate
tete
s
e
tanone1-Tric
,ene
-D
220s9905/oL/90
04 /26 / 9005/09 /9005/09 /90
15.5
cx
N
Client Pro'lect No. z ltl-22Lab Proiect, No. t 7765Ef fectife Diluti.on : 1. 18Method z 8260Matrix : SOItLab File No. : >V14Itethod Blank No. : RB05
318
5
( 8240 )
150990
acted/PreparedwzedExtract?ent Loss on Drying
Compound Nane
rideAc
Cas Number Conc.uglKg "E?k;
7
7
7
7
7
5
7
7
L2L2L2L2
6t20
5
6
6
5
5
6L20
5
6
5
5
5
6
6
6
6
6
6L2
65959
5
6
6
6
6
6
6
u
U
UuJJ
U
U
U
U
U
Uu
u
U
Uuu
U
U
U
U
U
U
Uu
U
UuJu
U
UBJ
27
4-87 -34-83-95-0 1-45-00-35-09-2
7 -64-L5-15-05-35-4s-34-35-60-5
7 -66-37 -06-28-93-31-55-66-23-55-27 -48-05-48-87-5L-02-69-0r.-69-00-5L-43-24-49-L1-0 L-50-75-85-25-28-10-1L-78-69-34-s
7 -L8-48-88-38-90-70-4 1-40-42-50-20-7
Disulfidehloroethenehloroethane,2-Dichloroetheneormhloroethane
715
6
1.0
7
7
5
7
10
71006
7
7
7L2100511
71059
7L2
1010
1010133
te
c
c
2
,
v ny
-2-Pentanone
Tetrachloroethaneoroethene
1
4Xylenes
Surogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
Approved:
J D Parker
103t96t108t
QC Limits
(70-121 )
I 81-117 1u 4-L2Lt
fiers:Suali
B=E=*=
esnt
abovedetec limits.s for reagent waterted, but is
samole data.ibrbtion timits.18, Part II,less than the
s arenot available)si andnoton
al1.
POL's for soilapplicable or
and
are
Quality Assurance Officer
.,
I Irrr r.Fnrrrtx r rrllitsll
. '., l-'; 6 -'E A-;;'i.r-'l i,n,-r. ll;ri;5f'l:i165;at:l'iiR" i;i :r i:.i i:' .;.t]' i u i !i 1;:i i Lli,., r1''l
r8.l
I Btl u 1i:rir 'l i.rr:r .lrliia
ll: :,.,r:rir:r.t
i
i -.r!i!1rr:H
.t
i I r,!r!rIr.F
I
'. r-r ..r .'1:1:1r. '
{i
rr !:t,::1rts r
I
..
t
!
I-
a4
tt
:')
I
L1
l
r.F
1i 1+ 1':. 1;-!.1 2
i,. ar-' ilr
'1lJ.r3'r
-L-:. .--- Llr- ' ::t
:'J;':iiJ :U. ;i'r'ii-: :
ii,,ar-ri ULtp Fr ie: "l.,i4li',: :O-l
l,j i t,z: l!r-,j-i:.i'i r : !.* : t[. :- lLt: F:.-;:'
L:.3I- '-.. --t::-tt =t :..'it.
-t :- i ii-; i . ':I'l i t iE 1..rt- r.:.
i-,,_-rai'.1 r lLll E,..i.. --11 t i' i i,.,a i ':i.:'.e,:..\t.7 ai.;'1
,)
.J i ..:
Lu
EVERGREEN N{ALYTTCAT, INC4036 Youngfield wheat-Bldge CO
( 303 1425-602L'
80033
vor,ATILE ORGA$TCEAI.IAT.YSIS REPORT
-^4.LabDateDate
le NumberNumber cx2
0
0
0
0
M-225
77 651. 198260(SOIL.>v151RBOsl
8240,)
20s995/0L/904/ 26 /905/ L4 /905/ L4/90
veded
Client Proiect No. 3Lab Proiecf, No. 3Effectife Dilution 3Method 3Iutatrix 3Lab File No. !![ethod Blank No. 3
coNcug/xgcouPot ND
Pyridine
Surrogate Recoveries:
Toluene-d8
8""1i iers:
Prepared
i? Y/N
an tima
cAs *
r.10-85-1
82t
tsts
PQt *
ug/Kg
5490N
6U
analvzed forlimits are no,
QC Limits
( 81-117 )
ibration linits.s are
J
B*
EPAfound tbt
alligh
=Pr cr.
0 IN co umn.E=Unlesguant si ota !9e
at a concentration outside the calcgncgntrations and PQL's for soilt basis.
Arrroved:
ona
Parker Quality Assurance Officer
tl , r-rri iHFr'lllATnGE Arl
4r?B
rm'-i - ,+;;15 :i:i i i;F-,5 i +Lf i: i
88,.' 1t8,3
(Fir 1:- i+..r?;l:l i:i itl;irlr, 1
1it1u] 2l]!-,{
-l
J
'1
ta
i
J
.l
:. ,-, .-, .i r-1 n r-i
i- ':. ir,lrrlt
-l
J
1'l
It
r'r
1
{
l r.t it.,l
.l i'r iir .-r 'i, rli
t
II
':
I
i
I
I
I
I
iI
;.l 1g 1- 1. 1::,fr
i,J ;t'.. !r i.I
l- :r.-r t-
, ! ^ . L.. ..:r . . ., :I i?-. IL r ,11.r. IIe: i,j*r,Tiil':.atl,3t.r ni P,..rridti-r e
-5; ..:,,.3t . :,i-r: J ;l.i11 -: ii: +:
Lira Fr ie: )t..t"L'rI$: :r,tJ
iiorrie : ::'{.:!-ii'l! :,';,'-.l :-:;i:: hli
11r.;,:: t) !l:l-.'j'l:l.i:':;:iJ li.tr:, 'l*. 'it-l i
l-iicr,3rrrri lU: Bl-;t;
i..iir,;:-r t l- , ',,e i 1: ':' i-r i -: : 1i-;Ir-rrecied st: ,i-i;1514 ll:4lil
l.ir..i.errt lJr.1 lp;.. - F r le: 't.,r i',:, 15 z iO'2
EVERGREEN ANAIJY:TICAL, INC.4035 Youngfiefd_ wheat-BfQge cO 80033
( 303 | 42s-602L'
VOI,ATIIE ORGANICS ANATYSTS DATA
ts 405005/OL/904/26/905/09/905/09/90
L6.7
cx2
0
0
0
0
N
DaDaDaDa
tetete /Prepared
?Drying
Client Proiect No. 3Lab Proiect No. !Effectife Dilution 3Method 3Matrix 3Lab File No. 3Dtethod Blank No. 3
vt-22
77 651. 198250SOIL>v14
RBO5
5
( 8240 )
150990
POL*ugZKg
L2
Percen Loss on
Compound Name
1
iers:
J
B
E*=t
esnt
Approved:
roethane
Cas Number Conc.ng/Rg
I 7 4-87 -37 4-83-9
7 5-0 1-475-00-375-09-2
67 -64-L75-15-075-35-475-34-3155-50-5
67 -66-3L07 -06-278-93-3
7 1-55-656-23-575-27 -4108-05-478-87 -51005 L-02-679-01-679-00-5
7 L-43-2t24-48-L1005 1-0 1-51L0-75-8?5-25-2108- 10- 1
59 1-78-679-34-5L27 -L8-4108-88-3108-90-7100-4 1-4100-42-51330-20-7
1
1
1
1
L2
U
U
UuJJ
U
U
U
Uu
Uu
U
U
U
U
Uu
U
U
U
U
U
U
U
U
UuJ
U
U
U
or
tneChIorene de 319
D1
,
,Lar
Disulfidehloroethenehloroethane,2-Dichloroetheneormhloroethane
15
ic
1
D
1c
,
t
5
5
Surogate Recoveries:
L,2 Di.chloroethane-d4Toluene-d8Bromofluorobenzene
flualiIJ
3BJ
QC Limits
t 70-L2Lr
1 81-1L7 1u 4-L2Lt
90r94r92\
trument ecti.on
1
andcalVol.
ts.reaoentbut is water
s are
samole data.ibrhtion li:nits.18, Part II,leis than the
se tedawe
J D Parker
POt's forafplicable ailable)
runn.
s t,ions(NA =
andnot soils areor not av
Cn^ c"*t
Quality Assurance Officer
aowt
i'-i€:l'l
:{,1
: {-{
'].,].
=..1
't-r ::, ::
r.Jl l. 1
-J .. 4-,
-'Llo::L,L1
'l -.- {l
,tr! rJ! ,.:'Lt.tt | -'.
'::r .l .-
?.:
.u:{
..:f,
.{:,
tl)
:I
..
o-
:a]
a-. to
:rf(|,f::,']U];:a4
lr -.r
.}.
,i. ..\ .,
-t' :<=,-t
7L
L. .,: .rJ :.:
. . :-i .t- ,-,.',.i :.... l-
-r -: :': lr ::.. t"' -{ :}......r.1 : -r::,- f..-{ t:,.:l ..'-L ft .t ,:.:-r .l - r r.ll -
... :.: . l- ,rl:t J', ..ir.r- L
l:a:.r -l'! :.j -
-,:.1 ".-.1. .fi ,tl O.-r- . .- '. i'. tl
O (11 (-.! '.1. -- 4-., i:,.,1 ;: ro
'0 ,11 .. i:l a r0
-J. :__ .--.i
,.Jnl
.:.
il
r'{
.trr{
n'r{
.tiJ
d
-t
.,t!
.1(,
t -.ts
| -I:l
'r-l a',1-'rfr',J- 1-]-T
,tl,r,
.:.
,i-sl:
c-sr
:i-!s
r--sr
,1r
:.!
,:l
,5
.:trri
..1
.:,'r!
,l;
:r,:'
I'i'r-r' tr'r1-r' [-.'r-t I--t -t'
('J,:l
-'3
tl{:',:l
(.1r{
{lql
a7.:l-ttt
G.
G.
{i..(
.n
:5,.sru
Arlsl
rl
.?
,5,
il
,51
.fi|
C:ol
($
.sr{r .:,
-f,
.(lrt1'ft
0r
Eo(r
C.For-(:.
h!C
C
--l,:l|-
l::f-
,1.
'a'r-[
:,rfJr{
EVERGREEN ANALTTICAI., TNC.4036 Younsriet$or}liBlr$ltr" .o 80033
VOI,ATILE ORGAIIIC AIIALYSTS REPORTPAGE 2ClienLab SDateDate e
DaDate
? Y/N
couPot ND
Pyri.dine
Surrogate Recoveries:
Toluene-d8
i iers:analvzedIimi-ts for,
ate aneEPA
Client Proiect No. 3Lab Proiecf No. 3Effectife Dilution zMethod 3Matrix 3Lab File No. :llethod Blank No. 3
coNcuglKg
c4x2060005/0L/9004/26/9005/ L4/900s/L4/90
N
st M-22
77 651.198260sort>vl5
RBO5
5
( 8240 )
151490
PQt*uglKgcAs #
110-85-1
8It
sco runn.at a concentrat
QC Limits
( 81-117 )
a1ilide the c ibration limits.'s for so s are
c*n-f.,*L
5u
9o"1
B=*=
EUnlAC ion outsand PQLquant
Approved:
J Parker
concentrationst basis.
Quality Assurance Officer
:n
.J
.[,.{
J.
i-{
Itl
i.L
r-i-
ll
,rf:.{),,
1..1 ': lr{ t
:=,-{ -{
' ,:"1-{-{
{
t
':'_ .
!
rJ
':t
:l
:r- ",
..: "l
:-'l ,' -''
t:t
i:-{
-u : ::'.i' :ri3' 1..
-J .. r-'_. ,r ,n
'::rl
l'1 .-
. rt-l ..
-r--
l-'tl-t
. ,ti .1.:rl ..
rli rl
- rl,
:l- '.,.
1l -'n:.--.|
,.. ::, .
L .IJ
rJi-- [i
In +. r-,! ;. rlt
{tt'-
.-l- ,:'!,. *
.fi
,r
!:-
11)::
t.
,..:
,i
.:,
6r'r!
,Jr
r(i"
Fl
,tir:r
,:U'
i-,s,,Ir"
.\.1
i:.rt
!r{
-l
..1
.l'-$l .---r:::::=:
.--i-:
6ol
.:l'ar ,tJrll 13.tn .t
,-t
r--r-1
''j.':,i
'.4
't- t'1'-t' i -r-l- -r,l'-r
(n Li. ,:'t.ir {i ,:(
( i {:.. ':'
4.,t:'.1 t) r-a'
1.1 r{
:.,:,t
.{":.
!tr
Jl',"r
13
i,,
::.1..tr
rl
,t;
.ii.l
l'-'l.
llrt
's,,S'
,1,.,t.
-l
.Irt
t:1-a
(rI(:
;i
EVERGREEN N{ALYTICAL, INC . .4035 Yofidfield- -whEqt -E-iEge co 80033
( 303 1425-602t'
VOI,ATILE ORGA}IICS ANALYSIS DATA
Prolect No.{ecf No.fe Dilution
M-225
77 651.198260 ( 8240 )SOIL>vl434RBo51090
c4Dx2060405/0L/9004/26/9005/ LO/9005/ LO /90
N 15.3
DateDate
No.ank No.
LaoDate
Percent Loss on
Compound Name
or
ene loride
iers:
J
B
?Drying
hene
D Parker
Cas Number
94t115t9lt
Conc.uglKg PQL*uglKg
,
,
tI
Surogate Recoveries:
L,2 Di.chloroethane-d4Toluene-d8Bromofluorobenzene
OualiO=
QC Limits
( 7 0-L2Lr
I I 1-117 Iu 4-L2Lt
L-t1.ru1#
Quality Asgurance Officer
L2L2L2L2
6L20
6
6
6
6
6
6L20
5
5
6
6
6
6
6
6
5
6
6
L2
55959
6
6
6
6
6
6
6
Uu
U
U
U44J
UU
U
Uuu
U4Ju
U
UuuUu
U
Uuu
U
U
U
U
U1J
U
UU
U
7 4-87 -37 4-83-975-01-47s-00-375-09-2
67 -64-L75- 15-075-35-475-34-3156-60-5
67 -66-3L07 -06-278-93-3
7 1-55-656-23-s75-27 -4108-05-478-87 -51006 1-02-579-0L-679-00-5
7 L-43-2L24-48-Lr.0061-01-5
1 10-7 5-875-25-2108- 10-159 1-78-679-34-5L27 -L8-4108-88-3108-90-7100-4 1-4100-42-51330-20-7
1-D1-D
ter
E*
essntitat
Approved:
h,=
::
Sl"-r
-{ -l
(fo
J-{
tfrt$'Il.==Doc:O,1'tl.
J.. y*oa0
EL -lloFo
o!OLCOoo-otrc.tl3*
10rI.:l]
UJz
Z=
Xcr<--l.:)Za
UJ.<rurrL='.'I=
.{ 6t::,v.. ']....lr c'1 0
':.|uJ -sJstsoOLt- t-o
Qa
ood ...Jdo
Lr- - +,+'10o-o
-FJ
a.lo
.f,
l^{r
-l
C}
tr
.lrl
P
arl
coa3
r].
ra'f,}-{
r$
-r,J.^
...f, .n
.....t,'.i,f...ti'o-..?r\.-
dCr,I)) ...Ctra.f, .
=f.. \o 'i0)3r,
-:{rf,.It
oo(JPEO.no-
'fZE
6l
mi
rO
-l
!i
rl
d
6trl
z-sl
r-s
r-st
f-s5
t-sr
z-ss
-5
oo.!,
{D:t
ooGo
Gtrl
@.s,
d
($
6t
d
a
qr
JEet
t.l
0r
CIeG,c,F
CT
c,&Ia:
C
(l
ru,o(D
EVERGREEN AIIAI,YTICAL, INC.4036 Youngf5.eld_ _I{heat-B!{ge cO 80033
( 303 1425-6O2t'
VOI.ATTLE ORGAIIIC AIIALYSIS REPORTPAGB 2
DateDate
cx2
000
0
D
6 04012610
10
/90/90/90/90
Pro'llectfeD
ect No.No.ilution
Nt-225
77 651. 198260(SOIL.>v143
RBO51
8240 )/Prepared
? tlN N No 4090No.
COI{POI'ND cAs *coNcug/Kg PQL*uglKg
Pyridine 110-85-r.u 5
Surrogate Recoveries r QC Linits
Toluene-d8 115t ( 81-117 )
8""1 ifiers:not water.J v isttationle.B and samole data.Vol . 1B', Part I Lare IeSs than the*=s tstrunentcoTIIIIII.alibration limits.ils areataconcentraentrationis.
tion outside the cconct bas s and PQL's for soona
L 4N h,,*L
o!,a
roved:
John arker Quality Assurance Officer
,:..to
..f
tl.f,
-{iL
(Ll
LL
a.
:,r:l
rrf
f._l rlt
rl =t.{{
:'{ , .-l "
| .:l
:]:
:::-{
-l -{
:l
,:r
:! '-r,
'' -l
....t]
J, "..rl,-f,
.. :r:i... --tr-i
-.1
'- _0
.1...L ,lJ
,:lr- 'f'
rtl e-. r_lL,:'1l
'li 11 .-t
'.1. --r ri.l .:r -
o ql t-lr- l: (i
,R ,tr -.
:J. . a-
:r- - -{n ".'
rJ:.r
:{ ." :r.
:-!
.. lJ.:
.t, " .l
'-L .,
.t- " -.
lg ql
:) ': i-
-- l. -r:!l-l -
rD 'n,{t
.L n r-'
J...rft
Tl'tl
.-i-
-{,:f
i
.:r
1l
rU
it
.'l :r
' :.-l
:. f'
'l .. r-'-tto
.r"!
6',n
(s,|Il
6,
't,
rl .(,
d
:,
,.1
rl
6'.t'il'rl
:1.,3.
fit
':jfJ!l':i'il,{
.,
Fl
.!
;- 5l
-C:a'
i-!ti ---
€nl
'1
'lt.&,u
I
G'
,5trfl
a((!
CF
CI!:t:t(I
;it.
t
?!
t r-r- Ia'rr-sT-rr-f T-f-r'.-,1-'r'-f"r6--r-.t,:i
{;!
'r'l -r-J-a--r.-
.i,
5..r.l
t'
.:i
,:l
..t.
G.(:(ifi..c
ti :'.:'
,:i
Gt€'cl.:J
|.r'r{,:.1
.:'.r'.:i..l
EVERGREEN A}IALYTICAIJ, INC4036 Youngfiel4^ -wbeat-Bi4ge Co 80033
( 303 1425-602L
VOI,ATILE ORGA}IICS N{ALYSIS DATA
vt-2776L.2826sor>v1
RBO
DaDaDaDa
Larr
/Prepared
t Loss on Drying
Compound Name
ide
v
4
2 -2-Pentanone
-Tetr hloroethane
zeneBenzene
Xylenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-dBBromofluorobenzene
fluali Lers 3
J
B
E*=
U-'est
Client Pro'lect, No.Lab Proiect No.Effectife DilutionMethodMatrixLab File No.Method Blank No.
505015/0L/904/26/90s/09/905/ 09 /90
15.9
cx2
0
0
0
0N
tetete
25
5
0
g( 8240 )
4L7s0990
1
1
1
L
1
6
6
Cas Number Conc.ug/Kg "E?k;
L2
uuu
U4J53J
U
U
Uuuu
U2L
U
U
UUuU
U
U
Uuuuuuuu1J
U
U
U
7 4-87 -37 4-83-9
7 5-0 1-475-00-375-09-267 -64-L75-15-075-35-475-34-3155-50-567 -66-3L07 -06-27 8-9 3-3
7 1-55-556-23-575-27-4108-05-478-87 -51005 L-02-679-0L-679-00-5
7 L-43-2L24-48-L1005 1-0 1-5110-75-875-25-2108-10-159 1-78-579-34-5L27-L8-4108-88-3108-90-7100-4 1-4100-42-51330-20-7
oD
t2
102t96t109r
3BJ
QC Limits
t 7 0-L2LrI 81-117 1
l7 4-LzLt
ts.reaoentbut is water
and
s are
satmDibrh
1B,les Part II,s than the
Ie data.tion limits.
POL's for soils areapplicable or not availablel
t46
CApproved:
D Parker Quality Assurance Officer
!n€
t$...1
.1.'4
:1.{
,,'r. l.
-l '$.-lJ ::, :l
il).:r ,l'
;..::*(Ltrn
r i:o
Llt- (,
I.1 p l-l
Larll
'r ,E -'
t-1-.1 c,:t -.1 *
rOrI
_l
i.rJ
-i .{i:.r
..< .::
.::l
2,:}:-l:l :-,
lt- -r .
0_ ::,:I :::J :r.:- -':,.,_J....lt r
'1 i:,
:l.rJ -
li J r-,
l- r(l
-lllr i
!1_'t .-
rtl ,ll-- .. :_l' rl)
,.. t01! -,n.-F. J
!'at
!'\..{.il
J
0)
!L
o-
f
':l
o
"'-1
=
:.s.
f'a
:1:,
.. ...-0
.-'{ '|:|:-.r.if '.. ...
.. ..t1 ".o-Jl<..!.'
:!
tO rD lJ! r'i r,'!
'Srfl--J:: =
rl
.t'
H
.,
r{
o-tr{
'itrl
rt
,;-sr
t -ss
r-rT-6'rl
6l
,1(i
.iJ
t-S:i
e--s
z-s-s.
t
'.-T-f7:'r-rT'.]-'r- r1' I'TT'!-l*"' t'r'[-.:, rqr,:1 '3'.!, ,i,*! 'tr
6.
Gtinf.(
t5),:t.ti
,31.t
,:!'
lirt
l.ra,
€'
.Sr.s.
t,'t
-.{
c,clclc:.
\:tr{
,3,:,
^,
Fl
i
':l
6
!t
u
F
Jc
trl
G.(,.u
I
rl*
-t
0l
tr.
C(I(!(:F
Ct
(:(rIL.
(:
ii 'it.,Ji,J
?{
403 6 "3IHlgi3iH,ffiHil$i?*'ds 80033
ANAEYSTS REPORa
DaDat-tete
cx2
0
0
0
0
N
c1La
VOIAATLE ORGANTC
6 PAGE
501/0L/90/26/90/.L4/90/L4/90
a
a
aaaa
a
0
54
55 le No.Blank No.
coNcug/Rq
No.
tion
QC Limits
( 81-117 )
PQL'tng/Rg
14-2257765L.208260 ( 8240rSOIL I '>v1517R8051490
? Y/N
]OUPOI'ND
lrridine
ur te Recoveries:
cluene-d8
ralif iers:
sea
ample data.18; Part rr,IeSs than the
cAs *
110-85-1
85r
Lon
6u
t . water.Ls
and sVo1.s are
tat tonand"BEi+3"f31"#?i ibration limits.s arewe
pr, r
on
Parker Quality Assurance Officer
f.l
LJ
i...-lItr
J
!
0l
,J-
ll-
+-'
_lrJ
r
r0
.l
:-1
:f
,I'f-i -r
'.t
.. :l
:.lr--t.'.
"'rl..,L,:: -0<:l "
- :..'J.
J-
(,' [l ''-ir- l.: r(r,f -:i :: i:
.it
f,U
::,(tJ
t'.-tIti t-l
lr: ':
'-t ,t,
,=;,: ,-d
lr:.
.9.t:' ..n'*'{
'..t:.t ,9
'. ,s,:i. ,ir'
1. dr.
ii
a.:,-.
,s,
, tl
d
.i,
,i.
'(. 5l.rl ,S,t{
r'
rll
::
1-'1 ,:l-t(--..
..!'..
:{ tr\
:i.;\l.{:{
-r.-
-1r{:l- :{
rl,r{
I.
1rl
rll
,'t
- /:4
i. --' -'
.Jl .r it
_|.. {-'-'fl!o
::r,-11
'l F. lll
O+'U': .: (Ll
.1. t-t --.)- . ',:,.-t..l-
r.f
B-i
c::
lJ "-i
r{ '' -t:. ,.. t.|.1 ..
t- -,)- + "i. /+
l+' rr-l
-- rli -r:)rl -,
a(|
- .. . -t.{lll
'1. -r +'
!r tO1l '- 'tl-. ._ ,' .,
.'i
I:- .jl _. .-=.::!:
*' 't ''
..i.
.,
r-'-;!;
,:
':.,
I'a "t-
,5'
.:r
:rrt
l'-rr'-'i;
a'
:i:,:i,!.l
'-r-'-I"'"
rEr|:,,:''l.-l
{r
',1u
i-,.t
i;
r.j
,li
rI
t-
EVERGREEN AIIAI,YTICAL, INC.4036 Youngfield- -wbeat -Bidge CO 80033
( 303 t 425-602L'
VOLATTLE ORGAI,IICS AIIALYSIS DATA
LabDateDateDaDate
-Me
Conc.rug/Kg POL*ugZKg
eveded
xtractent Loss on
Ie NurnberNumber
Prepared
2Drying
Client Proiect No. 3Lab Prolect, No. 3Effectife Dilution 3ltethod 3Dtatrix 3Lab File No. !Method Blank No. 3
u-225
77 651.048260 ( 8240rSOIL>vl418RBo50990
c8x2060205/oL/9004/26/900s/09/9005/09/90
N 3.5
10t0
1010
51005
55555100555
5
5
55
5
5
5510
55252
5
5
55
55
5
uu
U
U3J4LJUUUuUu
U20
U
U
Uuu
Uuu
U
U
UUu
U
U
U1J
Uu
7 4-87 -37 4-83-9
7 5-0 1-475-00-375-09-267 -64-L75-15-075-35-475-34-3156-50-567 -66-3L07 -06-278-93-3
7 1-55-656-23-575-27 -4108-05-4
7 8-87-51005 L-02-6
7 9-0 1-679-00-5
7 L-43-2t24-48-L1005 1-0l-s110-75-875-25-2108- r.0- 1
59 1-78-579-34-5L27 -L8-4108-88-3108-90-7
1 00-41-4100-42-51330-20-7
1-D1-D
t
Compound Nane
lene oride
tanone1-Tric
zene
-D
Cas Number
100t97*106t
oroDroDenevinll Ether,
ormL-2-Pentanone
Es
ze,aeBenzene
Xylenes
ierE:
d.
Approved:
analvzed forlimits are
loroethane
an estimaEPAPractinb
t
D Parker
4
uBJ
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bronofluorobenzene
QC Limits
t 7 0-L2LrI 81-117 1u 4-L2Lt
Quality Assurance Officer
flua1i
B=E=*=
ter
cal40-c,ss other*rise,titated on a concentrations and POL's for soils aret basis. (NA = not applicable oi not available)
u/4,\-l#
ow
-{\
l.{{i
.1.J.
-tJ :::, :rJ:::::o 1.,1
-li .. r-'-.qrO
L ,-l:lrl-- rtl
rfl +. r-,(_ ;: tl,!, ! ',,rf :,:J -.1--
In
'rI
-l
--t
)J::
Il :.r
:lI:}.
-r.l 't.t-;-L=tI:J-{ :}.:- li.. .-'l ..
:{-rJ .
.{ J*l*.9
-.i.t- L
.D.J-
4! rrl.-.. -J... rll
.L '!...r0'n ..,!---- -_l
i
:tl:'{.f,:{
-'(
rlt
iI
-!o-+':,:l
L
rrl
il
::!
3'
lf,
.,.=r
I-i"'
li -:,.=
.....-rl
:n,j. ".drlll.r'. .-.
.-{' .i'
--: ...1.
":l ':f':l
rll : I -ll-'lt ''
.L
O rLl a-)tr.' i: ,'i
rll rl,i ..
_J,-i_
tl
td
.t]r{
.nFr
,,
?.t
ill
r.{
r{
.'L,
..n
,t
e-l:1 .-:-.
T'-r'r!--t'a-l' 1-l
i | !i:., ,:r
', .!rF. rtt
"t i,
t -tli
t::51
r -.:t'
f:-$r
lrj
ci.:il,:l
:l.:l.o
-!--r;r;1-T
{i,r:;,( i.
,: t,
'+T'r-: 1'r1'.1-:-l't-rr-T-r,[, r'1-r,11
Ct ,1i 11, rl, r':.
f I ', r3, ,!t ,:'C:' j! ,:' .at ri
{i .:i r:, ':r ' .(:, ,r 'it r(t ':,rl .-{ .-l ..{
6,
':',3',u
€t,sl,.!'
t{
€',5t
oJ'rf
,t',5l,
cl
6ra,.t
lfJ6,
t.-o,
t
It)
lfr
.r.
fl
1'-l
{lr-t
il
':!rt
ci-il
arI
ii:-
1i
-l-
enLab S
t
DaDa
couPot ND
Pyridine
Surrogate Recoveries:
Toluene-d8
A!{AI,YlrIWheat
03 ) 42s-6
cAs #
110-86-1
90t
Client Proiect No.Lab Proiec€ No.Effectife DilutionMethodI{atrixLab File No.l{ethod Blank No.
EI/ERGREEN4035 rounsfief$gAL, INC .Ridce CO 8003302L-
VOI,ATILE ORGAIIIC AIIALYSIS REPORSPAGE 2I602/0L/90/26/90/ L4 /90/L4/90
2005040505
DateDate
cx vt-22
77 651.048250SOIL>v15
RBO5
5
( 8240 )
181490
PQL*ug/Kg
N
coNclug/Kg
U
QC Limits
( 81-117 )
C.,ht-Ar^^L
5
OualiO=
E=Unlesquant
Lers 3
B=*=
si
roved:
John Parker Quality Assurance Officer
: J,:l.
- {--l
,i,
tr --.{
,. .j.'rl :--,
,n.r ]
j.. +:d rt) rtt
. -.'rlt-ii-- tU
Os t-lt- 1: tlt,L 'r' '-i
,f .-.--
'l!
ot,..,.!
(.
l-.r
:L.1
F.
f :t:.'f, ..
-...n t
.. ,rl ..
:E'-,l.,ts
l,-,r-l'l ,: ;.-. ,lr rf
't_.
ttl rn
. rtl
,. u!u "'n--l--.1
:l].
l-r':{
!.t...=
. I r.._l ..
.. , .:.1-.1
.,'j' .-f. . --{ - ::,
rJ..
,r, o
-1 .r].
ri : i ... .,t
{L':::.ilJ
-:I"a.:1.fl
'-!-.
,.(t iD f_),- i.:'0'!tr| -..i:: r
':{a
;
,f.J
(Ll
l-L
fi-
,a
rJ
rrl
,i
r\.1
r.rl
'.!.,
t.
1
.:
-.<:==:
1'5l '---
i '\:; -----::::'
li ''- t
:'
i.,
T'-I-'l-I
.:
,.4.
|:
Ir"r.t;.:,
it
:l
.:. Irl
-r'I
.t,i.:-t
.."',
-r-r-tr
t,:.i:r:.
J,I
,l
ta
!-,
;rs.i...t ,5,
5: 'u
qi'(r
1.
t: ,:,l': 'i:tLdtt-
'.::,:i,.,
r, 'S':r ..u'
t-df-
.;;
..t
lir ;;;.d,
:iE
,11
Il.?,t.I'i,l.a. ,S'1,,.t ,r'.Ir nItit
I
lrr,
I
I
1...
l--tiltrl-lt:
t
t,,
,I(r
i:t-fI
(:tt
l::
It-
-r--.
EVERGREEN N{AI,YTICAI, INC .4035 Youngfield- _wheat _Bidge CO 80033
( 303 ) 425-602L'
VOI,ATILE ORGAISICS ANALYSIS DATA
DateDate
Percent Loss on Drying
Compound Nane
ide
sulfi
,1-D
,But
1 1
te
Client Prolect No. z 14-22Lab Proiecf No. z 7765Effectife Dilution : 1.18Method : 8260Matrix : SOILLab File No. : >V14I'tethod Blank No. : RB05
CO nc./KqCas NuaDer
umn.concentrationsbasis. (NA =
Prepared
102060305/ 0L/9004/26/9005/09/9005/09 /90
14 .9
cx
N
5
( 8240 )
190990
POt*ugZKgu9
Me
7 4-87 -374-83-975-0L-475-00-375-09-267 -64-L
7 5- 15-075-35-475-34-3156-60-5
67 -66-3L07 -06-278-93-3
7 1-55-656-23-575-27 -4108-05-4
7 8-87 -51005 L-02-679-0 1-579-00-5
7 L-43-2t24-48-L1006 1-0 1-5110-75-875-25-2108-r.0- 1.59 1-78-679-34-5t27-L8-4108-88-3108-90-7100-4 1-4100-42-51330-20-7
U
U
Uu3J45Juu
U
U
Uuu16
Uuuu
U
U
Uu
U
U
U
U
U
U
U
U1J
U
UU
L2L2L2L2
5L20
6
6
6
6
6
6L20
6
6
6
6
5
5
6
5
6
6
6L2
65959
6
6
6
5
5
6
6
Dc
2
-Tr
v
4
2 -2-Pentanone
1 hloroethaneIoroe
Et Benzene
Xylenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
-MetBromo
ia
3 BJ
QC Limits
t70-L2L)I 81-117 Iu 4-L2Lt
107t99t113t
fluali t-ers 3
B=E=*=
limits.s for reaoent Yraterted, but is
samole data.ibrhtion limits.18, Part II,1e3s than the
esrtsi
al0-
seona lre and POL's forapplicable or not available)soils are
C ryah.,r*LApproved:
J D Parker
not
Quality Assurance Officer
il-1
i.IJ
:!i
:r'i
.:J
.:}.
1.i
::
rL'
r-l
o.
.a-
;-!
C
r0f'?
' i ,-(:
;.r, i:.1
:.r':.1
:-l :{
:1.f
].,=
::
: .-,
r
.:-).. !-. llt r0,:
L..Ur:,:-- tfi,t
t0 s t-.,,-a{,t .rl -,
--l:i -
o0.rL}.r; i rf,
!.' r
I.1.-rJ''
-l
,[ _:
-{ _f.
: :t-
..lr,:., .:
.:', .t.; , --,: .-t .'-
t.-- ,r
-:i.r- -
-i .-
,!! 'q--, - -i.- ,t!
lr-'r.J..'nTl '' rll
- -- .-l
...=,
.fi"
::i -!lIr "(U
:L
ttru
.:'1
rl
.(.
rl
-trl
:tJ
,::l
i -!,1i
! --rl
I -- !.::;
;l-:,.l -.=
t -!;i
t -:]
.t,
6,
C'J
,tl.:r,.tl
rl
.3.
Gr.-:t.
G..
11 '
d
,:.,l|..
'):, .
t-
.,:c,
,
!:ol
4,.llol
I,1,
t(l
o.rt1'-l
.rt
r:Irt
+-'I.:
atI
c
':l:-Ct
a .f,-rt1"I--'r-r'ta-"r'r' l-".'T'1-t r-".l1, r.-f --I-.rI.a--I--l--
.?t1.:
'1!
:.i
:t'
(::(i
{l
1;'
:.r
':!
.:
rn
l:.t
.,u
.5,{l
r:.
,tl.i.,t'.rl.-t
.5|.:i
:,1,:l r.ll
A
EVERGREEN AllAIYltICAIr, INC.4035 Youngfiel4 -wheet-Bi4ge CO
( 303 1425-602L
80033
VOI,ATILE ORGAUIIq-N4LYSIS REPORTPAGE 2
teDate
J
B
Prepared
T? Y/N
analvzedlimits for, bu
C1ient Prolect No. 3Lab Proiect No. !Effectife Dilution 2Method !Matrix !Lab File No. 3Method Blank No. 3
coNcug/Kg
c10x20503os/0L/9004 / 26 /9005/ L4/9005/L4/90
N
vt-22
?7 65L.178260SOIL>vl5
RBO5
5
( 8240 )
xtrac 191490
POL*ug/KgcouPot ND
Pyridine
Surrogate Recoveries:
Toluene-d8
fluali lers 3
cAs #
110-86-1
84t
6U
QC Limits
( 81-117 )
arecatan esow
*=
E=Unlesquant we
t-on ide the calibration limits.outs
PQL 's for soils are
C-%ayptOv€d !
John
se
Parker
and
Quality Assurance Officer
tai ilrlr,.nGir'lFlrlltnFl.
i : ..', !Ei i 3i .4-:.:.;r ' A
4r.18
3r,1,tr.TII'
;.;:f; i;a5 i.3;ll-: i '-'r';-';ti;5.|ile;;1 i5;t;tl5,'1 1
I
I
I
I
I
I
I
I
;
:
1 ft,:t 1.i4q )
tI
I1
:+, ..l-r,-ir.H
i
1 ...r 'l.lt.it.9
1IIa','.1;t.;.lLtiti
,
1)
;
:: -r;.:.tl
:
'!
i
I
,'Iit
I
I
.:..:
I
\i
I
I
a:
',;-l
i
I
I
il
it
rl
4 1ri lr 11 1n 1ii 2q -tir
!:;3 F t Ie: )'r..,!itaI'r::l,r:
I ': / . '",i ri . tt-1..:lrfE . r.;-.t,-, Lr-r t ; -: / .1- (-
l"'l ; -..c: ir:5:'.). Uj.: Li;': : Ll ;
Urrant lJutF,,' F r ie : ^l.ri5l'r : :L]:
i "F)
i.l ''.? .' l;i. '.r l-i ;
.d f ,;e: :U-;- r:::1I
1 r i le: l,jc:-rt tf 1t:,31.',or1,-Jf
L,3 1t i-A, iDr'.3i,,:rrri 't.",;r' "P.-,
!i
r' I d 111 e.'1
l-i:,er,3 l,lr iLl:'.-"..,.afit I i'ireiIn.ia,-:t;'J 6t:
+ i-: i^;': i. {
",
Li r-i i 1r|i -: [l'].1.-r:4[
E1TERGREEN AIIALYTICAI, INC.ounqfield Vflheat Ridqe CO 80033- (303) 425-602L-4036 Y
VOI,ATILE ORGANICS ANATYSIS DATA
le No.Blank
5
(8240t
240990
r{-227765t.278260SOIL>vl4
RBO5
Prolect No.iecf No.fe Dilution
2206 100sl0 L/9004/26/900s/09/9005/09 /90
2L.8N
LabDate
Hx
13131313
6130
5
6
6
6
5
5130
6
5
6
6
6
6
6
6
6
6
513
56464
5
6
6
6
5
6
5
U
UuU4J46J
Uu
U
U
U
U59J33
U
Uuu
U
Uuu
Uuu
Uuu
Uu1J
U
7 4-87 -37 4-83-9
7 5-0 1-475-00-375-09-267 -64-L75-15-075-35-475-34-3156-50-s67 -66-3L07 -06-2. 78-93-3
7 1-55-556-23-575-27 -4108-0s-478-87 -51005 1-02-5
7 9-0 1-579-00-5
7 L-43-2L24-48-L1006 1-01-5110-75-875-25-2108-10-159 1-78-679-34-5L27 -L8-4108-88-3108-90-7100-4 1-4r.00-42-51330-20-7
?Drying
Cas Nurnber
94t85t96r
Conc.ttg/Kg PQL*ug/Kg
No.
4
actrcent Loss on
Compound Name
-DL-Di
oride
oroe-Dic
hane
-2-Pentanone
-Tetr loroethane
Benzene
lenes
,
uuBJ
QC Limits
t70-L2LrI 81-117 1
17 4-L2Lt
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-dBBromofluorobenzene
8"alifiers c
J
B
E*=
esrtsoita
C4)\ h^^
Quality Assurance OfficerD Parker
Approved:
Tol- I nN CHFOIIATOGPIIII
F!la )L1?4 3
Ilaaaqr*.1).l
?9A6SO1I
ARfir,f l19d' '-1
.ooo*aJ- - - - - -1
J,J IJTJ4
cuut lc
1Bge3B
Datal.lame:ll r ac i
I
TL
.tlDu.Ttc
0 1 sa
a
irJ
lgcJr1
'l tz a14161 2?
d Fr
r t le
65 L
Frle: iU1424::Ul Ouant Dutpr-r Frle: "Ul+2+zz9-iX2U6 I'Ji7,'a5;4UL;R
5 ; 5 ; 5 . 0'2i 0 ;5 i t) i 05 t t)'t /90 i
le: IU_'i21i::l1l: I D F r LL FUR fifrpE I.lO l )( r'{ l ilL tluFr,:llal rbrat roni')lJUrr0? U?i'2L
lloerator ID: BUU
"li-rant Ttmei )UU2U9In;ected at: 9UU5O9
'15 222
L4255
EVERGREEN AIIALYTICAI.,, INC. -4036 Youngfiel4- -wtteet-ElQge co 80033
( 303 ,425-602L'
VOI,ATILE ORGA}IIE ANAI.YSIS REPORTPAGE 2
---gl1Lab SDateDateDateDate /Prepared
Methano T? Y/N
COUPOI'ND
Pyridine
Surrogate Recoveries:
Toluene-d8
fluali Lers r
EPA
al0-
Ci
ta nriseona
C1ient Prolect No. z M-22Lab Proiecf No. z 7765Effectife Dilution z L.29!{ethod z 8260Matrix I SOIItab File No. : >V15Dtethod Blank No. : RB05
coNcug/Kg
Hx2
0
0
0
0
2
06 105/0L/904/26/90
5 / L4/905/ L4/90
U
QC Limits
( 81-117 )
5
(8240)
221490
PQL*ug/Kg
5
t water.t-s
N
otr
cAs #
110-86-1
85r
not1yue on
B=*=and samole dataVol. 1B', Part, Is are less than I,thecoat, a concentration outside the calibration limits.cgncentrations and PQL's for soils aret basis.
C ?/\tu^^ k----roved:
Parker Quality Assurance Officer
'li
'r-1 : .!
-. 1
':.'l.:J
':.t,:l
l.1'.
1{:.
(Li
i.L
o.
-1
i_J
rfl:
r.-l
::.
.:r
'-i'1'i : {
....1:'
- I .r "
.-t".. .. .ft
:I i.::,
.-t' i..
. : ...1... ::, .
,tl". c' "rll.1.1'l-':,"..'.J..
.t_
It trr
tr'l i{
.: J.td
- ..-l!:t- -{
'- .t
lJr
7
--{
.t,
t:
r:l
:- ,
. . r-i r,...'l- '' ..,
'':F't r..
l. .r
.-i'- i.
- r 'l .,-rYl ..
'U itl
:-U.l ,:1.
,^-; .. .-''-!'t.|
L..11
!:r:- qt
r! +' fJ
i rl tl!L.r-,
'i- ' L
-t.l:--
"' 'l!.[_ -' r]
r t('
r-] " tr.t
rO rU .-,
r.1 i, .;
,. r I I..
,5.
:'
lr-rti
tr
i.a.'
irl
t.c.
.t
,n
l,-r
.:,.!
.i.
1
.U
"'{
I .Il-.-.._...-.r-
r . i ,'- -- --. ...--
,S,-,u:
9,,5r{-
!!
(U-
rl
l.::
it
t:,
t-t-
rA,t
': .
:!-t-
,i:
't, .3,tl 6,-It,r:.t
ta.
r(lrrlri.
I .l
I
I
)
I
a,-.r:
.._ ).n
.l
t l rl.r 1r-.-1,,t: {:i.: .:r-: ci
;1,
,::,
t_r'.r_rl r'
:
li
't
,:.
, l;.' ,-;1,I rt '1'fi
CJ.:?
':f,,:t
rl
t{
!tt
r:J,il
,::'(:lt-
l';'
f:rr1
':':l.t
r:tt(
{:|-r:l
lc
l::
.;,tt-
EVERGREEN AI|AJ.YTICAIJ, INC.4036 Yonngfield- -wheat-Brdge co 80033
( 303 1425-602L'
VOI"ATILE ORGA}IICS AIIALYSIS DATA
_ __enLab SDateDateDaDate /Prepared
t?Drying
t $-225
77 65r.238260 { 8240 )SOIL>vL425R80s0990
406 115/0L/904/26/905/09/905/09/90
18.1
Hx2
0
0
0
0
N
7
2
1
7
3
1I
9
4
4
2
t Loss on
Client Proiect No. ?Lab Prolecf, No. 3Effectife Dilution z![ethod 3Matrix 3Lab File No. 3Method Blank No. 3
Conc.ug/KgCas Number
104t93t99t
Compound Nane
ide
Ac
,-D
Brorno v ther
-2-Pentanone
-TetrachloroethaneIoroethene
"E?k;
7
7
7
7
7
6
7
7
7
5
50
1
7
0
9
7
2
000
0
3
L2L2L2L2
6L20
5
6
6
6
6
5L20
6
5
6
6
6
6
6
6
6
6
6t2
55161
6
6
6
6
6
5
6
U
U
Uu204LJ
U
Uuuu
U
U38uu
U
Uu13
UU
UUuu
Uu
Uu2J
U
U
7-33-91-40-39-24-15-05-44-30-55-36-23-35-63-57-45-47-52-61-50-53-28-1r.-55-85-20-r.8-54-58-48-30-71-42-5o-7
II
0
0
0
6
1
3
3
6
6
0
9
5
2
2
0I
0
0
0
4
4
0
ide
,1
1f 1
1
v
1
7
7
5
7
0
7
6
7
7
7
2
6
1
100
hane
o
tanone1-Trichl
teaLc
,
,
1100
1
1
5
I
1
1
1
113
4-2-
,
I
4
1
0
5
8
1
9
7II
0
0
0 4
I Benzene
a Xylenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
OualiO=
t-
B=E=*=
esnt
UBJ
QC Limits
t70-121)
1 81-L17 1u 4-L2Lt
ter
C-'IWApproved:
D Parker Quality Assurance Officer
nrol r olr cHFOtlATnGRAlt
- 'rlrl
I].4BrrUUr{
't
r a^-+^^^ IL )rJ"laqa
1 ",,a',,,il--- - - -'l
11oB0Ail.l
1 aa!'tq!-.ril
1..]UUL'Url
^^^^^^1.1OUs't,(,.l
"9,aada)-"--j
r.BoB6Gil
5BBA6*l
IIU6UU
Jr)wLtt)
e,2.a,1a
idTrtLas
68..!tmu.TIC
4gg,l eqa,1q66,L1A??aqs
c.t
It/,rn
NIa
i,
Ie
rt
I,4
T=hsl
1 1e141 618 r?
Uata F r le: >U1425: :i./'I
rlarne : )i2 Uo'L'L i7;)65 i iUEllrsc: 5;5.:+.98;0 i5! 0 i
l-luant Dutpr,' Fr le2^VL425: :D2
R, ,, o') ,,'l t) |U
Frlet
Ia: lU 824::111: I IJ F TLE FUH TTPHEI..IU I Xtlal rbrat ron: 9UU'-rU9 0;I.l I NL uUrts
2'l
Oeerator lbz BUHULant Irrne: 9UU5u')ln;ected at: 9OUr0')L:.' i 1'?L5 :'25
4036 Y
EVERGREEN A}IALYTICAI, INC.ounofield lilheat, Ridqe CO 80033- ------ (303 1425-602L-
VOI"ATILE ORGAIIIC A}IALYSIS REPORTPAGE 2
DateDateDaDa
COUPOI'ND
Pyridine
Surrogate Recoveries:
Toluene-d8
Client Pro'lect No.Lab Proiect No.Effectife DilutionMethodMatrix
4206LL05/0L/90
04 /26 t9005/L4/9005/ L4/90
llx
N
M-2277 65
L .228260sort>vl5
RBO5
5
( 8240 )
Lab Fi.le No.Method Blank No.
CONCrtg/Rg
231490
PQL*uglKgcAs #
110-86-1
88t
U
QC Limits
( 81-117 )
limits.
6
r reaoent waterted, 6ut is
samole data1B', Part IIeSs than i,the
ibration limits.s are
f ..ryr'\t L-,J"
OI'
roved:
J Parker Quality Assurance Officer
:,r O.
il ti'i
L, iJ'
-{d
., ',
--l-{
,Jl:r :t
lt.. e'
-< rlr rl-l
. . -t_1
: -- tll
rll +, i-l
r. ,- rli
.f :. '
'J- I .:
rL,
:-
ll:l_.t
.r: {
J.. .-l
:r .t
(!
1: ::.
,-1 .:
:l-.:: .,
,i".,
l-:rIt ''.
I r., rn
. i': r-
r-l .
4r ,rl
.- rllt.L -' a-'r r!!
1r- - i!
--..,;- . j
:.t.f
i.l
rll
l.t-
t -,.
l
_t
.T
:l
-.i
_:.l
:l 'l.; :,
.t.'. ..::.'
,:'! . .i ,..
'' r L(' "': l.n:-,:J','
:l J'l
'li : :. -l'J-- : r "'..:r..-,.
.t-
rB rD r-l
' ': :rf
ll,.-..r.tll
',':
.5,
,r:.
r{
i!rI
'7rl
r{
..:,
r'l
rr
-j[ .
_jI::r:-,i,l '" '
f -:i ------------
i,,::
t' .l -'
I
[;-r'T;:.'--r'.I.
:, li :t
.. ct ,:.r. 1.. f:
r-_i "l-'l1
c:.r::,ti
da
t-
I
E]
,l
,,1
,:l
:1,]
'.- -,f-- ''
,:i.:i
::
t{
lr:.
':tl
'3
r:|r
tr-l
:,;
rr:,
(L
(r.
!
+
lr:.,..(,t-f.
c
,tl
.il
,i'.('
.rl
Ir:.
l{l
-l::.
'll
.:t
ar|::
l-.:l
d
.T.::
..:
tl
ll
t'
EVERGREEN AIiIALYTICAL, INC .403G younsriet$ori}ifilrglto" .o s0033
5M-22
77 65L,288260SOIL>vl4
RBO5
aClient Proiect No.Lab Pro'iect No.Effectife DilutionUethodDtatrixLab File No.ltethod Blank No.
H6x206L205/0L/90
04 / 26 /9005/09/9005/09/90
N 2L.9
VOI,ATILE ORGA}IICS ANALYSIS DATA
Cas Number
---ent Samole Nurnber 3Lab Samole'Number rDate Rebeived 3Date Sampled 3Date Exttactgd/Prepared 3Date Analvzed - 3Methanol Extract? 3Percent Loss on Drying 3
(82401
260990
Conc.ug/Kg POL*uglKgCompound Name
c ide
sulf
tanone1-Tric
teL,
,
v
-2-Pentanone
1
Xylenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-dBBromofluorobenzene
OualiO=
13131313
6130
5
5
6
6
6
6130
5
6
5
6
5
6
6
6
5
6
613
66464
6
6
5
6
6
6
5
U
U
U
U1041 Ju
U
U
UuU56J29u
U
Uuu6Ju
U
Uu
U
U
U
U
U
U2J
U
Uu
7 4-87 -37 4-83-975-0 1-475-00-375-09-267 -64-L75-15-075-35-475-34-3155-50-567 -66-3L07 -06-278-93-3
7 1-55-656-23-575-27 -4108-05-478-87 -51005 L-02-679-0 1-679-00-5
7 L-43-2t24-48-L1006 1-0 1-5110-75-875-25-2r.08-10-r.
5 9 1-7 8-579-34-5L27 -L8-4108-88-3108-90-7100-4 1-4100-42-51330-20-7
I
ne
,
,
4BJ
QC Limits
t 70-LzLrI 81-117 1u 4-L2Lt
100t95t
10 1t
ter
Lers 3
ot
c
P
J
B
E*=tI
C,W\ #
essntit
Quality Assurance OfficerD ParkerJ
Approved:
. LTAL ! nr{ Ct{F0IOT0BFA}i
I 6 :nr r
Frie: ilj,3i+::i]I
i e : I U F-TLL FUI-': fiF,I.,LNtJ I )i ]tJ It Lalrbratroni vdU5U9 07:'l'L
a6
16 18
Ouant Outpr:: Frle: "U14'162zDz
].lE tJUxs
1
I .: nlaa
l.tddddo
1 zddaaa
i It!trtlrH!T,
;;Al]Aa',-
6BBOOS
4BBragS
araE66F I
n
It,|,L,)
rO
!lt)
Al
Inv,I4,I,fi
1B 2L4 ?
Uata F r
i{a nre i )i
t1 rsc: 5
le: >U142fJ::t", 1
2 U61'2 1 t" o5 : +UUi5i5.02;U;5iD.i R5,'Ov /9 u it
U
I r:,'[rt
L,= s
tJoerator IO: Bulsnt l'tme. ')In;ected at: I
UH
utJS $')
UUSU,7
L:; | 42
L5 :55
EVERGREEN AI\IALYTICAL, INC .4035 Youngfield wbeat-Brdge CO 80033( 303 ,425-602L'
vor.ATILE ORGATIq_ANALYSIS REPORTPAGE 2rsensHx2
0
0
0
0
umn.
coNcng/Rg PQt *
uglKg
606L25/0L/904t26/905/t4/905/ L4 /90
Lab ect No.No.ilution
5
( 8240 )
241490
u-771.82so>v
RB
DateDateDaDa ? Y/N
COUPOI'ND
Pyridine
Surrogate Recoveries:
Toluene-d8
r-ers 3
N e No.Blank No.
cAs #
110-85-1
91r
U
QC Limits
( 81-117 )
5
8,,'
B=*=
I analvzedlimits for, bu
fal0-4
arean estimaEPA
tt
8
EUnlquant sies at a concentration outside the calI cgncgntrations and PQL's for soilht basis.
ibration limits.s areseonaw€!
C-hL WrL'oved:
John Parker Quality Assurance Officer
:':i I|ir3
rt .o
-<:{
.1
..t .. .-'* {' to
.::
L .1-1
r-t I ,ti
lll +. t-t
r.:{).l ,ii -
rJ-!:
--l - -i --
rlr,:
1:1:{
-. .t
-i,r[.-'
+.t(]
r:! :
,' J-.. '11 ... a, '::P- '- ,l
'- 4.
l" tr.l:l !: --- ,lr .rlt-1 ,".
'I ,n
a r[i'-t-'" +
lll ." ,tt
--. i
i.
r- '1
-t
:1..1 "
...i ".. .,.n
if .ir "
,.. "'
: .,,f.
/',:.1 '-., .t
.. .t-1 ..
(l :-1 .n.".|..
.-'.a_,f
i.t-
o (Ll ,-)
't-'E "'r0 .0 .-
i.i:-'. i:
,:{
13
.f,
r-..1
iJ.-.{
_:.
tr
:ir
t:,-
fa
'ti:r'-l
,:r.l
,r,
rl
.lt
,
"{
,.1rl
"-l
i.-!:l ---#=:
:. r;.:: _r__:-.=:
,{.'--d, -.'r "r':f,'-
f:. i;, i? r'r'
.':r r: 'l rj!
r;, ': .. r:1
rI (.1 rr, "{
;I.;l; ''-;{; ''"
(i, ",'(i. 11,4.,' tir
(,, l-
--,1,"'-
a.:.1(;,
':;,
(r.
C1et
{1
,5.
?{
---.li-'' r-,!)
,!?
.ttl
.:,
:)
.:'
^j
,:'
,.r.'
"{
.,U
Fl
t,,s..
4l
3,3.n
F
lr-r€.
ll,
r:i
'...
.t
lr:....n,.
a-
i
-tEnl
.:t
{r..!
F(,
i;I
.:
,:l
l-
,.\l
,::,
':
!r:'
.!
.11
-l
EVERGREEN AIIALYTICAL, TNC.4036 YounsrietSogT[iBlr$ltn" .o 80033
VOI,ATIIE ORGAIIICS AIIATYSIS DATA
LabDateDateDate
Compound Nane
hane
Loss on Drying
Client Proiect No.Lab Proiect llo.Effectife Di.lutionMethodltatrixLab File No.I'tethod Blank
H8x2061305/0L/9004/26 /9005/09/9005/ 09 /90
N L7 No.
M-227765L.2L8260SOIL>vl4
RBO5
5
(82401
270990
Cas Number Conc.ug/Kg "3?k;
L2L2L2L2
6L20
6
5
6
6
5
5L20
6
6
6
6
6
6
6
6
6
6
5L2
66060
6
5
6
5
6
6
5
Uuu
U
1337JUuuUuU
U24
Uuu
U
U10
Uuuuu
UuU
U
U1J
U
UU
7 4-87 -37 4-83-975-01-475-00-375-09-267 -64-L75-15-075-35-475-34-3156-60-5
6? -66-3L07 -06-278-93-3
7 1-55-656-23-575-27 -4108-05-478-87-51006 L-02-679-01-579-00-5
7 L-43-2L24-48-L1006 1-01-5110-75-875-25-2108- 10-159 1-78-679-34-5L27 -L8-4108-88-3108-90-7100-4 1-4100-42-51.330-20-7
1
,
de
ene ide
ulf
IT
c
AcetateichloroproDane
_ 1,3 D-iEhl6ropropeneIoioethene-Trichloroethane
oromethanechlorooroDenehylvin|I Ether
Es
4
2 -2-Pentanone-He
-lFa hloroethane
zeneBenzeneneXylenes 3BJ
QC LinitsSurogate Recoveries:
1,2 Dichloroethane-d4 103t (70-L2llToluene-d8 97t 181-1171Bromofluorobenzene 101t 174-L2Lt
Oualifiers:O = ComDound analvzed for, but not detected above reportinq limits.Repbrtino limits are iouohlv the method detectioh limi€s for reasent waterJ = IntU.cate5 an estimated v6luB when the compound is detected, but isbelow the EPA Practical Ouantitation Limit (POL).B = Compound found in blank 6nd samole. Compard EIAnk and sample data.E = Combound i.s detected at a concehtration butside the calibrhti.on lirnits.* = Praetical Ouantitation Limits listed in EPA SI{845, Vol. 18, Part II,pa. 8240-4. The minimum instrument detection limits are less than the?rumbers shown in this column.ess othenrise noted all concentrations and POL's for soils arentitated on a dry weight basis. (NA = not applicable or not, available)
Approved:('
J D Parker Quality Assurance Officer
To
€.f,'f,:-'l
fr€
.-1 14
rf,\']\
=,3Jr J'll==3==0l 1.,1.
*lDo
EL -Eo,- o
Gp tJLCtu
(D tll -t0f ,:il3-
t0rf
ft,
U
4?1Z:.r
)".: r\<t3
U=l- s..-t -{=
r{ :}':: 1:..o..
.iD
I'l .tJ -llJrl-Ojflrr
.oi]a
0)(l
- ...-J.{ 0).J-dP.Lo
TJ'O-* -.)
,l.la
lr(\.t
-l
0)
lr
t.'
-lo-
Pl
13
co)l]
'f,Jr.
,-i.
?'$'
J.J ..
-.., '-" "'.0[\,$'*
f.l .rl l.t:....-Jii;l)..,1!r
.{'i
0i=-o
- :.1 '-'-:<trit
oo.JeEot[q-
JLL
al
|ttd
r(,
rt
:lrl
il
13
r-l
ot50.lt.!
-l
('-ss
z-sr
r-ss
t-$t
-e.---6--6-
6.6r(D(i,Gtl:,
616(,r-5 CO O-, Cl OJ
c-sl
z--s9
'-?.;--d;-'1r 6'C:' 6t8i 6r,:i r3l{! tri
-tr-tr':trr{-.r;r.a_lr
C!
':l
n-
(n(i(ii(n(l'
.B
€tatr
l:'r:r-{
,3r!r!l
rA.{{
,!!!5:,1d
6{ntii
GI
"7rl
6t.3
Gr-ol
r!'
G,{''rl
(sl
Gr(U'd
Gt@-tfr
a&.t
Lr
€nl
rr
.\.(t:t.rl
0r
ECc€
F€lE
CLIC
2C
6Fc
t1
c1
Ci
e.,
C'J
EI/ERGREEN ANALYTICAI,, INc.4036 Youngfield- -I{heat Ridqe CO 80033- (303) 425-602L'
VOI,ATILE ORGAIIIC AI{ALYSIS REPORTPAGE 2--ient, Sample NumberSample- Numbere Reeeivedvdt€ Sanoledpage pxtlactgd/preparedDate AnalvzedMethanol Extract? y/N
C1ient Pro'lect No. 3Lab Pro'iecf No. 3Effectife Dilution BUethod !Matrix 3Lab t'iIe No. 3Method Blank No. 3
coNcng/Kg
8513/ 0t/ 90/25 / 90/ L4/90/ L4/90
Hx2005040505N
vt-22
77 65L.208260SOIL>v15
RBO5
5
( 8240 )
251490
COUPOI'ND
Pyridine
rogate Recoveries:
Toluene-d8
iers:
ane
a10-
E=Unlesquant
for,not
ststrumenscoatullln.a concentrat
rtinq limits.tB f5r reaqent water.detected, 5ut is
and sample data.Vol. 1B-, Part f Lare leis than the
cAs *PQl,*ug/Kg
110-86-1
87t
s
U
QC Limits
( 81-117 )
6
9oul
?-
B=*=tI
ta onsea we
Bi concentrationst basis.
ion -outside the calibration limits.and PQL's for soils aie --
(*Approved:
J D Parker Quality Assurance Officer
I iil
.-{ tar
.'Lr--13
'ir'i:.i,-{
it-l,l ,l'
rli .. +'+ rll lE
i:!."D
'l r- ill
rO! fJ':- f ,Lll' '0 -,
:i "t-
rll
tr
r-l :.1
L..
-:ra t
Il.- -
!drl:r
r.<-1.
:: 4'.. tB ....aJ:
::r: -' ,-:
".- ! ..,-.i- n r-
lvO:l t-- !-* rI ;i.rf ..
,'u rn--.-,:.i
-' qJ
I- !'_rCTf-o-- r- I
':.1il
g\
it
lX.
.:
(L|
TL
E-
l
LJ
a-,:]
.-
,f'
J- 'x
It- 'r
-,;'...11
l.t -.i ...
" "l|l
.:.1 .n =
:-r J." 'll "'fi:r -t'l*:\r ...
,--..r.,J.
:I
rn iu aJr-::,4
'ql.-:i.:r
r-r;,r{
.Ir
d
nrl
(i.l
r-l
':.rl
d
z--ql: --*::*=:
--:gj
fj,:l
,:;,l:trl
r;r-'-rr -r'1-'l;'r':li-''"5-.,I;--d,',";l;-''
C1 r:i(i ri,4: ,lr
f :-:rl *'
r: r
':,,':''1'
': il
i:,
U-!
,:
':;1.,,t!
::!
:i
6)f..
,t ,::ii
':.) ':i,lr ,:.:
{t.titi.
r:;.{ir{
-r-J
ir
:'.1
r1
CIc(t
F,x
(:.
(E
I
iii-(:t-
.11{i
EVERGREEN AI{ALYTICAL, INC.4035 Youngfield^-lrbeet-B!{ge co- (303) 425-602L-80033
VOI,ATILE ORGAIIICS AIIALYSIS DATA
enrS
,eDate
DaDate
xtract?Percent Loss on Dry
Compound Narne
ide
h thanes-D vBromo-2-Pentanone
Client Prolect No. 3Lab Proiect, No. 3Effectife Dilution 3![ethod 3I'tatrix 3Lab File No. 3Method Blank No. :
ts
s
t-
ing
$-2257765L.2L8260 ( 8240 rSOIL>v1435R8051090
10
05 145/0L/904/26/905/ LO/905/ L0/90
18.6
Hx2
00
0
0
N
zerreBenzene
Xylenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-dBBromofluorobenzene
Cas Nurnber
90r89r99r
cconcentrat basis.
Conc.ug/Kg POL*ugZKg
Carbon Disulfide1, 1-DichloroetheneI , 1-DichloroethaneTians 1, 2-DichloroetheneChloroform
1 , 2-Dichloroethane2-Butanone
L , L ,1-TrichloroethaneCArbon TetrachlorideBromodichloromethaneVinvl AcetateI' 2:DichloroorooanelianS_ 1, 3 Diehl^oropropeneTrichloioethene' Lr2-Trichloroethanenzene
L2t2L2L2
6L20
6
6
6
6
6\5
L20
5
66
6
6
66
6
5
6
5t2
65050
6
6
6
6
6
6
6
U
U
U
Uu46J
UU
Uuuuu4Ju
U
U
U
U
U
UuuUuuuU
U
U1J
U
U
U1J
7 4-87 -37 4-83-975-01-475-00-375-09-26? -64-L75-15-075-35-475-34-3156-60-5
67 -66-3L07 -06-278-93-3
7 1-55-556-23-575-27 -4108-0s-478-87-51006 L-02-6?9-0L-679-00-5
7 L-43-2L24-48-L1006 1-0 1-5110-75-875-25-2108-10-1
59 1-78-679-34-5
L27 -t8-4108-88-3108-90-7100-4 1-4100-42-51330-20-7
42
1
Es
-Tetrachloroethaneloroethene
fluali r.erg t
t70-L2Lr
I 81-117 1u 4-L2Ll
tions and soils arePOL's forapplicabl e or not available)
QC Limits
C4r ["r^/
J an e9 r-ma
fot,t arest
a
we
ow
tI
seta
EPABE*
Unlesquant
_ proved:
ona
Parker
(NA not
Quality Assurance Officer
NTCI. I OH CHRDITATCIGRAh
ile 436 35.6-e
4
5aB
488
440
4[1[rBU
.J|}r.7i7t4
2ea6B
?4813
?geg
764tl
1e0a
86
4B
amu.
I TIC
0 1 AB 1 BB aa
16
Ilr)
I F)
ae,lI
afq
I{t
I
I
,tltg)
1S
L'2 | 4412:06
2141618 ?
Data Frle: >U14J6.tV'L
Name : X2 U6 L4r )];)6r;4Ut- i HPllrsc: 5;5 i5.$4; U;5; U i U9 /1Oz9Oi
Id Frle: ID_82ji::mITrtle: ID FILE FUR APF'tNDIX Nil',lELast Lalrbratron: ?UODLO L0:U6
llperator ID: BUBUi-rant Trmez gUt)5Iniected at: 9045
Suant Outpur Frlez n'UL416:zD2
UOfis
'10
:10
4036
are
rf,e
E\TERGREEN AI.IALYTICAL, rNC.Younsfield Wheat niEie C0 80033- (303)42s-602L'
VOI,ATILE ORGAIIIC ANALYSIS REPORTPAGE 2
DaDa
Dle
t'ien,s
/Prepared
? ylu
Pyridine
rrogate Recoveriest
Toluene-d8
Client Pro'lect No. 3Lab Proiec€ No. BEffectife Dilution 3Method !ltatrix 3Lab File No. 3llethod Blank No. 3
coNcuglKg
10
06 14s/oL/904/26/905/L0/90s/ Lo/90
Hx2
0
0
0
0
N
vL-22
7? 65L.228260SOIL>v14
RBO5
5
( 8240 )
361090
COUPOTJND cAs #PQt *uglKg
110-85-1
89r
not
tstrument
u
QC Limits
( 81-117 )
5
ali
=
8"
J
B*
iers:
ow
E=
analvzedlimits for,ted abovedetectionan es water.isEPAfound
ts
and .sample data.VoI. LB-, Part ILare leis than theSE
ona
umn.a concentration outsgncentrations and PQLbasis.
ide the c ibration lirnits.'s for so s are
h-
a1iI
Approved:
D Parker Quality Assurance Officer
I
j''€
,:!l'=
:.:. : {:..3
il:r',].
Ii..rHlu|D
r- ..1-1
a-r.- (1,
+'paB+ U'-cait ,n -.
IJ.J-
UJr
1:I-{
C- :'r
{- :.i0'<
-,:..f,:-1|']::
rr - -I.Il -'.. rO ,.
.-(. * ,i
.l- + .-1--ul#o-lr';.. rl!.r-.-r
E..
l! ro- -. ...!.- iljiJ-4 4+r0
1.1 * :ll"-F *i
a.l
13
.o
if.,.i
-{a
o
!"L
l
tl-
=
i:ol,l
,=,)
'=l-t'^t.'..
-i:- I'.",=
'--{ J .-.
...:I ..
" "'fi.tlr.) ".t1.! :l'1'. .,
:-{.'..'T
/\ ,:t .
:t.la...F".
'D ::. JJ
"'':'.,1 "'
- :1' Li.
Ll-
otrlrJ-. :: (l
,t-1 q _:;:::
,U
frJ
'5'
,l:lr{
..i
H
.J
rl
r.i.l
14
:.,:i,{-
------d-i-":::
i-st; ----
l-T-l:'-;r,'rl!---e,-"'l; ' e, ,-
c, ,:l .:! ,:, .ti {:,(l :l ,::) .S. ':: ,:lI .:1 ,:'r ':r r: Cii:: :' ,:'r .(r .:'. f..)i-: .i, ,i, Fl
i-:;i .--
(t,(i.(il
(,-1
C"l
r!,,rl
r.;
:;rI'
(i
.:i,
*t
,5' r!,:' ,'.'n ':',u rlti1 ,
,i.:,
tu
a
.:'
t{
(,1
Gt
6r
(-1
:tc',
rU
I-.:
ll,("t
.(r
:f-{:!.
0r
le.
r{
fl(l(!(:F
CT
t:::
ar:tL
C
;i
f-(:
f-
.I'!r
t
EI/ERGREEN AI{AI.YTICAL, INC. -,4036 Youngfiefd- -wheet,-!,iQge CO 80033
( 303 ) 425-602].',
VOI,ATILE ORGAIITCS AI{ALYSIS DATA
5
( 8240 )
451090
vt-22
77 656.338260SOIL>vl4
RBO5
DateDateDate
Percent Loss on Drying
Compound Nasre
or de
Met idee
Client Proiect No. 3Lab Proiect, No. 3Effectife Di.lution 3Method tIrtatrix :Lab File No. 3Itethod Blank No. t
Conc.ug/Kg
22060505/0L/9004/26/9005/L0/9005/ L0/ 90
22.6
Rx
N
Cas Nurnber POL*ugZKg
5
6
soils areor not available)
535353633230
3232
3232
32323032
3232
32323232323232326332202032323232323232
33
u
U
Uu31 J150 J
Uu
Uuu
Uu160uuu
Uuu
U5JuUu
U
Uuuu10J
U
Uu5J
7 4-87 -374-83-975-0 1-475-00-375-09-2
67 -64-L75- 15-075-35-475-34-3156-60-5
67 -66-3L07 -06-278-93-3
7 1-55-655-2 3-575-27 -4108-05-4
7 8-87 -51006 1-02-6
7 9-0 1-579-00-5
7 L-43-2L24-48-Lr.0051-01-5110-75-875-25-2108-10-159 1-78-679-34-5L27 -L8-4108-88-3108-90-7100-4 1-4100-42-5L330-20-7
v
c
2
Disulfidehloroethenehloroethane,2-Dichloroetheneormhloroethane
ate
1 D
Tr oroethane
-D
Bu
1
Di
.s.hl
_ 12-
,
,
v
1
ts
1r
711,
ts.reaoent waterbut is
e data.ion lirnits.Part II,than the
Limi
0-L21-114-L2
7I
7
1t
s
Qc
t
Surrogate Recoveries:
1,2 Dichloroethane-d4 97*Toluene-d8 101tBromofluorobenzene 84t
bu
v
Lt
or
aon
f
t
ed
t
A
EPAan
andcalVol.aresL4
st
t
r-ont-nec
Ara
t,
s
al0-
iersfciOualO=Inots
,snt
.t-ota
concentrations and POL's forbasis. (NA = not applicable
J
B
E*
samDibrh
1B,IescoaiI'EseaISS O', rtita
Quality Assurance Officer
g
D Parker
on
Approved:
O
j ',:.1.-l}1
.. .u
..r :{
:.: ='-.. -{
.r.l -' -:
,-D :r f.
-j .. r,
- ,ll
'I.lr!L.-rJ
'1.- tLl
,O 4. ,l
L,:(L,{! r. -"
,l:
:1.
-d.:
)
.tl''
-L .:.t- -:.r' ._t.
. . --, ..
..i.1- Lt"
.. t; -,.Jr-
l'- ,ll
:: .t- 1.
.l'.:J.
'll (1-. .,.i
-- rll
-(. _'.j
.r_. r:r
't--1 .' ,n
:,
.1
n
-r
tLl
Ir
11
!'
ff
+
q
a
::J
=_.1
:l
:-|
-t- '
. :i
.. :: ---
.l r'=.1
: t' . ..1
/\i'
i.1 :{
'Ll .r 'fl
'- l'l ''- :,:. r\
-1.
tn ilr dl
'r_';: ll-1.rl ,t:
-:. t-
qr'a,
.t
':..l
6t
.4,rl
':u-t
t-',1
j-1i1 ---:-
l-!s -..
['-$, =-e
l'r
l.!:r
LJl,l
:t:- -
':..:.rt
r:,
._-4r
::- sl
r1-r,r rt'J:r rl rrrl-1,.1 rr.l,--,r,1!l-tr.l' -n' trr
rl
.j.rl
.t'.:,,:J
{i,|,..
.{
:ti,,5,
:rrlrl
F
Irll
f.
l(ri't'-l
8r
(
6ill
.Iu(g
t-(l
uI
.::
;it-
,,r
rl
,i
,
(i),i).i),i)
'r!
C1(1
ci'
CJ
tali!',r.
EI/ERGREEN AI.IATYTICAL, INC.4036 Youngf ield l{heet -Bidge CO
( 303 )42s-602L'
80033
VOI.ATTLE ORGA}IIC AIIALYSIS REPORAPAGE 2
Date
? Y/N
COUPOI'ND
Pyridine
Surrogate Recoveries:
Toluene-dB
E=Unlesquant
)roved:
Client Prolect No. 3Lab Pro{ect No. 3Effecti.fe Dilution !Method 3Matrix 3Lab File No. 3Method Blank No. 3
coNcr.g/Kg
2050s5/0L/904/26/905/ L0/905/ L0 /90
Rx2
0
0
0
0
N
l'l-2277 65
5 .338260SOIL>vl4
RBO5
5
( 8240 )
451090
cAs *PQL*ug/Kg
110-85-1
10 1t
U 32
8""1i fiers:Compound analvzed for, but not detected above reDortinq lirnits.Reobrtino limits are iouahlv method detection liinits f5r reaqent water.InQicateS an estimated v61u6 when the compound is detected, 6ut isbelow the EPA Practical Ouantitation Limit (POt).
Comoound found in blank End samole. Comoard 616nk and sample data.Prabtical Ouanti.tation Limits listed in EPe Sw845, Vol. 1B-, Part TT,pa. 8240-4I The minirnum instrument detection limits are le5s than thehurnbers shown in this column.Compound is detected at a concentration outside the calibration limits.g othenrise 4oted all cpncentrations and PQL's for soils areitated on a dry weight basis.
QC Limits
( 81-117 )
c-ryr\hJ
J
B*
John Parker Quality Assurance Officer
:l
i-, I aal
.ro
'-{ -l
r-1
,Ll
,ll
.-
rf
1l:{
,l_ -f
:t --l
r-l . r
:ir
I
J
,li
nr ilt 't I
t)
.1
.1
-.t
,-t.
(l
:.r..
ir
4.
f
;--:l
l-'
'Iil.l
.'f ' .'
.{ .,Ili . . :.:i
:::i -{
.,i . .ii
.., ' ..i.
.i.
j..i
,-{
n
rt'
.f.
..(,
j-5; - "-*:'::j::
.:!
j
)
I
I
il
';l '
i:.
t..
_.l.:),::,
:1!::t:,i
.r .[
.::
:
.t
l"*'li,t r:r
.tr r'. tlrl -.11-'! l'.f t r-[. J rlr ':.': ,::r ,S' {;.:, i:.i 'i, ti,
:' :i ,:, t:,: ,:j' ,r. i'{ r{
tf.
':,.:,,:r
Ir:,
,:l.:',3
'9r
'3..(,
,(l .;:
,1, f
t(;
t..i':
!(
':i ...,
'-.. l-"
21,tl
!:..'t.,
-l
!
ii!1:,: i
" ,1:
,.t!t
l:|-..t
tq
.:
t.l.
EVERGREEN AIIALYTICAT, INC.4035 Youngfield--wbeat-tslSge Co 80033
( 303 1425-602L'
VOI,ATILE ORGANICS A}IALYSIS DATA
ent Samole Number .Lab Sanple- Nunber 3Date ReEeived 3Date Samoled 3pate pxtiactqd/Prepared 3Date Analvzed - 3Methanol Extract? 3Percent toss on Drying 3
yt-225
77656.348260 ( 82401SOIL>vl455R8051190
R4x206050sl0 Ll9004/26/9005/ LO/9005/ LL/90
N 2L.L
Client Proiect No.Lab Pro'iect, No.Effectife DilutionItethodMatrixLab File No.lr[ethod Blank No.
Compound Nane
v o
Cas Nurnber
104t100t95t
Conc.ug/Kg PQL*ug/Kg
7 4-87 -37 4-83-975-0L-475-00-375-09-2
67 -64-L75-15-075-35-475-34-3156-60-557 -66-3t07 -06-278-9 3-3
7 1-55-556-23-575-27 -4108-05-4
7 8-87 -51006 L-02-6
7 9-0 1-6
7 9-00-5
7 L-43-2L24-48-L1006 1-01-5
1 10-7 5-875-25-2108-10-1
59 1-78-579-34-5L27 -L8-4108-88-3108-90-7100-4 1-4100-42-51330-20-7
te
o
D
C
2
-D-D1
vrm1-2-Pentanone
oride
ide
loroethane
U
Uu
U
UJ
U
U
U
U
Uu
U
uu
UU
U
U
U
U
U
Uu
U
U
U
U
UJ
Uu
UJ
220
5363636332530
3232
3232323263032
32323232323232323232633232032032323232
323232
,But
1 1 91
1
-Tr
o
4ene
Qualiu=
B=E=*=
ne
a Xylenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
ACI
Pt
5
QC Limits
(70-L2Lrl8r.-1171
( 74-L2Lt
c, y//\(_
ter
ot,
Approved:
D Parker Quality Assurance Officer
1 :'"1
=,:fi
'L J'
-{i{
:{:{
:_l:{
.i.-:.1
.-, t.j .t'
,.u f. .h
:J.. 1,
'-tt[
::L -11,:'".- t'
ill + (-r
,_ ,: {!,ll ll -
rJ. : 1:
:J _1*
lli
t..J
.tl. .tlII
''i' : I
I.t
-tJ 't"t. .,;.iL:::lI''
-{ '1.
., --1 ....r,:.l .:':1.,J -, -_J .,l-- rn
.., -l- L. r:)j-
'l! ,0-",.,_l.. lll
'., rij
I.1A--,! |
't.
:t. 1r
l. .{
.r-l
.....-il
j'."f . .-.
'O r-l :l.t
..". r: '
. 'f -l
tu: r.ll'': I "'-. :1: ul
:J_
tll rll f.!
I f'rl,l: .(1 i
q,.. i._
:-.J
.t.
&.1
ill
l-t-
tr-
f,_l
Cc
_1:i
. ..1
r1.l
,u
.!.
1
"{
d
,\l
r{
..:,:,
1
l.-(J .--::
.l- 51 -€:=:
l. -!rl
r.-gr
-..-t -.,{-, tr-i r-l-'--- r-.r-r.;[. r-1"r.
r _.tf
r'l,i
,|'
'i
.r"' .1.t- r- :;
,: ' .:.r
':! ,::!
,:I
.1, ,:;i
.l t.t
T' .'l-1 J' r--""f"r
'5l ,i,:, ,;'
':!) ':'.:l ,n
,:ri .8
- i ".1.
.5'
.5,
r1l
,:,..i'rl
,:,!t ,3
b:', 'tt..c ol
1- r{r-
'(,ii...(
,:,-!
:;- ,l
,sl-
. 6.rJenl
.$
6i'4. ,Slr\l ,5t.lrtrll
ln
lr'l.(,
"1.FI
if
lr-,.
l-_{
{4.,
Cr,
r:,(t
r.t
tir
it..
ttu
t:[-a
CtI
;i,:
,i
,5
c:.
:l
EVERGRAEN AI.IALYI ICAL, INC .4036 Yonnsfield -Xtteat-Bidge co 80033
( 303 \ 42s-602].'.
VOI,ATTLE ORGANIC ANALYSIS REPORT
Datetete
Rx2
0
0
0
0
406065/0L/904/26/905/ L0/905/ LLl90
Client Proiect No. 3Lab Prolect No. 3Effectife Dilution 3Dtethod !Matrix 3Lab E'ile No. 3Method Blank No. r
coNcug/Kg
tq-225
77 655.348260 (SOIL.>v145RBO5l
8240 )
xtrac
Prepared
T? Y/N N 5190
COUPOI'ND cAs #
PQL*ug/Kg
Pyridine 110-86-1 U 32
Surrogate Recoveries:QC Limits
Toluene-dB 100t (81-117)
8""1 ifiers:analvzedtimits for, buare?-
B=*=
rma
s column.at a Concentration outside the calcgncentrations and PQL's for soilt basis.
E=Unlesquant FL
ibration limits.s aretat
C'/),-t"*r,1--^-^-roved!
Jo
ona
Parker Quality Assurance Officer
i; i'it I i,i i:Hf,'r)trA rniiE ctl
! i: l.!;1.lr5 :1 8 lm't.
4BE.t...
T!i
aBa 1ct-iat-1i-.ri8.i ttlqtd
J
r i. ri ;, r;r (i
1t
'. i .. ir r-i i-t rlr
-1
L.-..)Lto.-t.-. '
1
-1
I
I
I
I
I
i
I
I
I
I
Iii
Iil
I
I
I
J.
'1
i
:rfiirirrirH
I
-t
ar
i
lJ,
"? ir.1i 14 1,:.1,c
t
lt
IIII
r .,1 ,'lEl .
Ur-.:i-,t Uutp' F r Ie: "Pi.46t: : :U!
': iJ' .i. :-: ", il :
P,...,
I i-t
r'I 'f r ni
. rI
;-i6-rat,:,r IL,: E,,- ::rJ: :l-.'r j ':l L t -."1=ir'i,ei ie,l at :'l:ilJ}
:-.1i
I Ll. iil
E\'-ERGREEN AIIATYTICAIJ, INC.4036 Youngfield- -wheat-BfQge cO
( 303 1425-602L'
80033
VOI.A:TILE ORGAI.IICS AIIALYSIS DATA
teDate
Percent LoEs on
v
1
I
1
606075/OL/904/26/905/09/905/09/90
20.8
Rx2
0
0
0
0
N
Client Proiect No. 3tab Pro'iect No. 3Effectife Dilution 3Method !Matrix 3Lab E'ile No. 3Method Blank No. 3
vt-227765L.258260SOIL>v14
RBO5
5
(82401
2L0990
POL*uglKgCompound Nane
ide
loride
Disulfidehloroethenehloroethane,2-Dichloroetheneormhloroethane
1 D roproPenene-Tr thane
Prepared
t?Drying
oroDroDenevinll Ether
Cas Nur[ber Conc.uq/Kg
L2L2L2L2
6L20
6
6
5
6
6
6L20
6
5
5
6
6
5
6
6
6
6
6
L2
56262
6
6
6
5
5
6
5
4
3
26
1
7 4-87 -37 4-83-975-01-475-00-375-09-267 -54-L7 5- 15-075-35-475-34-3156-60-567 -56-3L07 -06-27 8-9 3-3
7 1-55-656-23-5
7 5-27 -4108-05-478-87 -51005 L-02-679-01-679-00-5
7 L-43-2L24-48-L1005 1-01-5
1 10-75-875-25-2108-10- 1
5 9 1-7 8-579-34-5L27-L8-4108-88-3108-90-7100-4 1-4100-42-51330-20-7
o
-D-D
,
4
Uu
UuJJuuu
U
Uu
U
u
Uuu
U
Uuu
U
U
U
Uu
Uu
UJu
U
UBJ
QC Linits
t70-121)181-1171
( 74- L2Lt
,
,
o
oroethane
nzenenzene
lenes
Lers 3
OIr,
Il-ta ona we
rm1-2-Pentanone
4
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-dBBromofluorobenzene
Quali
104t98r104t
terJ = I
B=E=*=
esrt
co umn.concentrations and POL's for soils arebasis. (NA = not applicable or not available)
C N'YApproved:
J D Parker Quality Assurance Officer
,:.1 rf,.
rJ.':.1
:f.-l
,].']
.l.i : ^ :-t
iI) -r r:
.-J -. !."tuo
L'.11
r_, "- rtl
! 4-'
O +' t-J{- ,: 0).t:-
i-t':i,n
r(,I
:_r
*-
-a4
1- ^.,
:.{: ,j :*- a--1.3I:}.
.ri ::.'l
-l-:l.I:.
:l l:. l_.. _1..
.:l ,:l
:i.JJ '".,: ) -.l- ,E
,: li l.t- l-..... Jf
llt 'I.- ..,.J
- tll
.1.. < 4r.r rfJ
1-'l -. n
i'f ra
di.l.t
-l
I
tl
:.L
D.4-'ll
rl,r
.l'=l
.:l
:l
:r'
=
}.1'
-l -t".-: ::.--'-- f "
" '' ll
: .l .L1 :-J':l - . .-.
.'! . 'L1
:-f J... r: "o -r .f!-..-|".-
.L
rll 'tr i I
-' : '!'l,I-l r' -.J,_L
.u
'rril
.lt
F{
",Fl
,:d
rl
'j'
.iIt
T.-;t;"-;.1 I -:'-' -l'-'e-T $-,1;-..:r
,:i,:l
r{
i-:;l
T-S!;
l.-:il
c-55
(-sl
e"s::
.:i
t::
(;.
(:!(i.
t
rl',1 ,!'*,',Itv r: ,:n a, ,1,
'n il r:. :"1 r: .r':. ,-tt 1? ii' ti'.i ':1 ':r :;r r:fttj ,' rJ .:rr r'!!.{ ,.r rl
T'.I;.:.,:,,:r
?|
r'
,3,36''ol
.:,
6t..(r-
rl
,i
,51
rU'rl
,:'
6r..
o-.
6tG,-tt
F
J€nl
61
6r1(,
'-t
.1..-l
.i-
0l
u.
Ecl(:
EF(l
u
a,L-
,:l
;it-
l.:
.ot
c3cl.11
l:)ol
.:'
,S.
,3.
!:,'t
,:!
.:l
r(!
(i
ct{:ciil
EVERGREEN AIIALYTICAI., INC4035 Youngfiefd_ -wheat_Bidge CO
( 303 \ 425-602L'80033
VOI,ATILE ORGAIIIC AI,TALPAGE 2 YSIS REPORT
R5x2060705/0L/9004/26/9005/ L4 /9005/L4/90
N
sentLabDateDateDate
Client, Proiect No. z, l{-22Lab Proiec€ No. z 7765Effeetife Dilution z L.25Method t 8260Matrix : SOILtab File No. : >V15Method Blank No. : RB05act? Y/N
COUPOT'ND
Pyridine
Surogate Recoveries:
Toluene-d8
5
( 8240 )
201490
CAS #
110-85-1
85r
PQL*ug/KgcugoNc/Kg
u
QC Limits
( 81-117 )
6
8""1
E=Unlesquant
ifiers:
?-
B=*=
roved:
John Parker Quality Assurance Officer
,l.r
,:)
,:{
.1
:.
(!
iJ-
;
{J
a
r:l
rll
f ,t
C
'tl ::.1
A.,|
.ll
l:l
a_! r{
'f'1
.. -{
'r. 1
r:t . -.
:-'
1.
l-,"l. i{
.. : i
=I .'
... -r i
. , -1.,'
:r.. rR ..
-t.".'-. t ,
I r. rt:^
... rf lll-'l ..'
,1, rl
-, 'Lt
.L -- +'
,^ll.r :r.
.-.1 . . a.
-, 'L ,!l
:,;- -.'u
'1 -- ili
tl.l u a:
- -l rlt
!' ,' '
j -1--
: I t'l:-'
.t.:-t._ 1
..t...
{! -r'}
a 1,j\J.
O 'Ll .J' i'n,r!-j '!:
iL-
--.- -J
-l
.5,
I
I
't!- -(i;
il .i.'i ----<-
- --.d.-.:-..-:-::::
.i.
.lr1'r-t t'1 -'t' r-'f.r-a-rt.I-r+ r1 .i f '-'
,2t (ir i i ,: ,:.!,si (i, .i .:. .:.)
':i r.i, ;' '!,:1 r:t. ,:r ':J,:'j a-.. r''. ii '.
r r'&,ra'-r,
r:l.l
'i1, -''-
4,,
r.:,t:'
.,,1
l;,'
::,
:t
EVERGREEN AI{AI,TTICAI., INC.4035 younsrietSoglliBlr$itr" .o 80033
*t-225
77 651. 158260 ( 8240 )SOIL>vt 435RBo5 1090
Client Proiect, No.Lab Proiect No.Effectife DilutionMethod![atrixLab File No.Method Blank No.
R8x2050805/0L/9004/26/9005/ LO /9005/ L0/90
N L2.9
DateDate
1
1
1
1
11
VOI,ATILE ORGAI{ICS A}IALYSIS DATA
Cas Number
11
Loss
t,at ona
act?on Drying
D Parker
Conc.ug/Kg "E?k;
U
Uuuu58J
U
U
U
U
Uu
U4J
U
U
Uuuu
U
Uu
U
U
U
Uu
UU1Ju
Uu1J
7 4-87 -374-83-975-01-475-00-375-09-2
67 -64-L75-15-075-35-475-34-3155-50-5
67 -66-3L07 -06-278-93-3
7 1-55-656-23-575-27 -41.08-05-478-87 -51005 L-02-679-01-579-00-5
7 L-43-2L24-48-L1005 1-0 1-5r.10-75-875-25-2108-10-1
5 9 1-7 8-579-34-5
L27 -L8-4108-88-3108-90-7100-4 r-4100-42-5L330-20-7
1
Compound Name
Chloride
sulf
c -Tr
-2-Pentanone
lenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
ifiers:
40-
analvzedlimits for, but not detectedarean estima
2
1
8""1
Dc
2 1
55
QC Limits
( 7 0-L2LrI 81-117 1
17 4-L2Lt
101t108rr.08t
ts.waterreaoentbut is
QuanandB=E=*=
e data.ion limits.Part II,than the
oninattstrunent,co umn.concentrations and POL'st basis. (NA = not applic for soils areable or not available)
C f/,-A*"L
Quality Assurance Officer
essnti
Approved:
NTAI. I NH NHFOIIATOGR9II
1 x5.o-
4 6
A tmu.TIC
Data Frle: >U1+)5iivI
l'fame : )(2 U6 U'd i 7..'65.i 4Lll:l'lrsc z 5;5;5.02;0;5i D;
1 6B ?ga
1B
Suant Outpr I Frle: "UI4)rtzfJz
I a
18 L? L4 16
1 6B
HP
5 ..' J. 0,'9 0 ;
1
'1888811
788890
6A06aO
50BBBr1
.rEuuEu
EBB
! na...
t4
Ii,rn
n
Ia
fr
.,1
"isa
It4
I IUI(r!
,
rJ
Id Ft leTrtle:
LaS t UA
: lD 924::l1LID FTLE FOH ATJr'LTiUIX I.1II..IE UUXSI rbrat rsn:',rUU5i0 l0: iJ6
Ooerator' lU:,.ilant Ttnie:
In.1 ected at:
Euu?UUSIl]
17 U U5.1.0
12:4Ll1:40
EVERGREEN AIIALYTICAT, INC.4035 Youngfiefd l{beat^B!{ge Co
( 303 t 425-602L 80033
VOI,ATIIE ORGAI{TC ATIALYSIS RSPORTPAGE 2---enLab SDateDateDate
COUPOI'ND
Pyridine
Surogate Recoveries:
Toluene-d8
Client Prolect No. z lt-2Lab Proiect, No. z 776Effectife Dilution : 1.4Method z 826Matri-x : SOItab ['ile No. : >VlMethod Blank No. : RBO
coNcuglKg
I0508s/oL/904/26/905l L0 /905/ L0/90
Rx2
0
0
0
0
N
5
( 8240 )
351090
cAs #
PQt *
uglKg
110-85-1
108t
t
ta Lon
snt
U
QC Limits
( 81-117 )
7
9o"lIJ
ifc iers:analvzedlimits fox,ted abovedetectionc
reDortiliinitsis det
4q limits.tor reaqenected, 6ut,isarean estirnaEPAac afoundt and samoVol. 1B^,are lei Part II,s than the
t water.
le data.
ibration limits.s are
J
B*
POL).6lAnksw846,limits
E=Unlesquant,
tI a
0
I s
gco runn.ataconct bassir.seta tte
concentratentrationsis.
ion outside the caland PQL's for soil
C?)\ )'t*t*. ^-
roved!
ona
Parker Quality Assurance Officer
rrHl
ls ..','ig :.5 -15 .'l'-i,ir:i - i ratu..ji:-ii;,Jii i ;;4.5 i +tra. iiiF,l'-:,;.iii,-i'i.:r ; rl i:1 ; g i.l5' 1
ttlt \4,:i --tlLr 1i,..i .r t: !l it
I
iI
i
I
I
!
i
I !lr'tlrrru!H
al
ii-,.',J:Jr_H i
J,
a
a
I)
I
I
t
i
I
I
,t
;l
1t1
:,J -i;e; ll:_i'','i.':: ll: i l' iaI i,i-..,t i i t!-..ir'r.:rr-:,tri
'-:1' 1 r r i- ( o;. ,il ,
!-h.,ir-,t l-i'.jtc, F r la : -Pi.il5 : :l-,2
. r.i'- iil4
^l
i I : rij
, .,-.ir
? i.j i.i t:r i :J
EVERGREEN AI.IALYTICAL, INC .4036 Youngfiel4 -wbeet-BlQge CO
( 303 )425-602L'
80033
VOI"ATfLE ORGAIIICS AI.IALYSIS DATA
ent Sanple Number 3Lab Sample- Nurnber 3Date Redeived zDate Samoled 3Date Extiactqd/Prepared .Date Analvzed - 3Methanol Extract? 3Percent Loss on Drying !
Client Proiect No.Lab Proiecf, No.Effectife DilutionMethodIdatrix
225It[-R10x2060905/0L/9004/26/9005/09/9005/09/90
N 2L .8 Lab File No.I{ethod Blank No.
z 7765z L.28z 8260(8240): SOIL'z >YL423: R8050990
PQL*ug/KgConc.uglKgCompound Name
ters 3
ide
sulfideoroetheneoroethane-Dichloroethene
Cas Nurnber
a,
at
co lllflll .concentrations andt basis. (NA = not
A
7 4-87 -37 4-83-9
7 5-0 1-475-00-375-09-267 -64-L75-r.5-075-35-475-34-3156-60-567 -66-3L07 -06-278-93-3
7 1-55-656-23-575-27 -4108-05-478-87-51006 L-02-679-0L-679-00-5
7 t-43-2L24-48-L1005 1-0 1-5110-75-875-2s-2108-10-1
5 9 1-7 8-579-34-5L27 -L8-4108-88-3108-90-7100-4 1-4100-42-51330-20-7
4
35
Uu
U
UJJuuuU
U
Uu
u
U
U
U
U
U
Uu
Uuuu
Uu
UuJ
U
UU
1
1
1
1
1
13
1
6
6
1
1,
,
,
,ormhloroethane
et
oroethane-Tr
13
19
v
1
c
v
-2-Pentanone
Benzene
Xylenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
OualiO=
BJ
QC Limits
t70-L2LrI 81-117 Iu 4-L2Lt
POL's for soils areafplicable or not availablel
JLC h,\i-,^,ib
4
95t92t99r
analvzedlimits for,are terJ
B
E*
ca an estottEP.E.f
.t-
ncPtIrtat
itr.setaon we
J D Parker
a
0
I
essnti
Approved:
Quality Assurance Officer
rnTsL ION r.lHPoltATnGFsll
e )r/1423 3
Lea6g&
11U68U
1U{ilru8
!ULiU6
.]OB8B
7B6EB
o
5Et[tB
.rEEtE
36880
eBE,Sg
1!ila!ifi
.arru.
I g 1 1E ga
1B
Iq!lri:
le 14 16 18
Uata Fr Ie: )Ul:'2): zt)'L
l'.lame : X20oU'7 ;,' i'r'5 ;'iUU ; ry
Pl r sc: 5;5 ;4.?9; rJ;5 i U i U5.'u9,'9u;
Id Frle: lU 3!i::illTrtIE: IO TTUU FUH APF'E.NSI,.(Laet llal rbrat lon:'rlJUrU9 0,:'
Oc,eratDr lU: BUHUi.rant l- tirie i ?UU>'ri9lnlected at: YUU509
Uuant OutpL,: Frle: "UL423::DJ
l'.1 I l'.lE t-tUrrs:l
5t'26
EVERGREEN AIIALYTICAI{, INq.4035 Youngfield- -wlteqt-E!$ge co
( 303 )425-602t'
80033
VoLATTLE ORGAlfrEErNltYSrs REPORT
R 100609s/0L/904/ 26 /90s/t4/905/ L4/90
Client Prolect No. z A-2r,aE-Fio-iect, no. z 776EfEecEife Pitution z L,2I.{e[[od- z 926![atrix : SOILeE Fife No. 3 >vlfieEnoil-glank No. : RBO
5
( 8240 )
2L1490
DateDate Prepared
t? Y/N
x2
0
0
0
0
Date
xtrac N
couPot ND cAs #
coNcuglKg PQL*uglKg
Pyridine L10-85-1 U 6
Surrogate Recoveries:
Toluene-d8
QC Limits
82*( 81-117 )
OuaIifO =Q iers c for,
J an esEPA
B*=
co umn.tion outside the calibration limits.s and PQL's for soils arenoted aIIdry weigh
at a concentraconcentrationt basis.
(.c/r\- ... roved3
John Parker Quality Assurance Officer
.1 r:l
:''l:-{:"{
.'t',.:{
' ::.: .:'
t]
tL' tll
i-,- l-:
:,-- tt,
rF +. r-l
-,:(!
: .r'
L
-_l . .. --
I
]J
_l
rl.
'tl:.1
.-l
ll- -{
..:- . ,q:
--r ..:.
., tn ..
'Ir- -' ' ,
'-!
l, ,n
:-l 1: ,-
' I r',
...:,,ti ,l
." ili.t '+
r.' rl.l
rt !. rll
:4.
-
=
r,
-tl
ln rU r-t
t ,.:: 't!f .n -.,-t. l:
,1,
a,*: l
-l-
f.l
,:1
:{
r:.1
..i
tLl
.,t-
:L!
+.
l
,..--t
+.
C
rfl
-l.a
.l
. r.lol
irl
.i
..t.
..r,
t'l.['r
i
:i,i.
'' ' ,{,- '' -
titt|.
,i
,l
|.:.,'
l:,
'a- :tl
t1
rj.1.;.
t.
Tjlr
:,.
:.,
:,
:.,
:.!:!
:.,
:.'tl
;tt:'
':i,'t,r: .
..1
-t
--r-,1;
r:.'r't
I,i:l
,rl.t
r{
t:,
t:
.- ,s. .arl ,:,
q, rl., .
t',
-_ ,i.
: lt.+ d'tc
't .fr
ri, €'..o tll
t-ilt-
,.(
i
-!.> .i..01
,
f;
,'i.
,r:
'4,.11
I
t.
I k'rt,o
1..,l'qlllC.l-rt;
t::
.:I
tfl:
f-(l
a::t
(:
.lt-
I
.Q-l
EI/BRGREEN AI,IALYTICAL, fNC.4036 Youngfield- _tfheet-Bidge CO
( 303 )425-602].'.
80033
VOI.ATILE ORGAI{ICS ANALYSIS DATA
1ie..abS e
ateateate
e
/Preparedat?ercen toss on Drying
ompound Nane
h1 hane
ide
f
,-D1-D oroe-Dic oroethene
vt-22
77 651. 108260SOIL>vl4
RBO5No.ankeB
20s945/0L/904/26/90s/08/905/08/90
8.9
sx2
0
0
0
0
N
ClientLab Progffecti
MethodMatrixtab FilMethod
Proiect No.iect No.fe Dilution
5
I No
( 8240 )
000890
PQL*ug/KgCas Nunber Conc.uglKg
h
,
1111
1111
6110
6
5
6
5
5
6110
5
6
6
6
6
6
6
6
6
6
611
65555
6
6
6
6
6
6
6
U
U
U
U2J33Juu
U
U
Uu
U20
U
U
U
U
U1Juuuuuu
U
U
UU1Ju
UU4J
7 4-87 -37 4-83-975-0 1-475-00-375-09-2
67 -64-L75-15-075-35-475-34-3155-50-567 -65-3L07 -06-278-93-3
7 1-55-656-23-575-27-4108-05-478-87 -51005 L-02-679-0t-679-00-5
7 L-43-2L24-48-L1006 1-0 1-5110-75-875-25-2108- 10-1
59 1-78-679-34-5t27 -L8-4108-88-3108-90-7100-4 1-4100-42-51330-20-7
or
t
oromethanechlorooroDenehylvin|l Etherorm1-2-Pentanone
-1[etr hLoroethane
o zeneBenzene
Xylenes
urrogate Recoveries:
,2 Dichloroethane-d4oluene-d8romofluorobenzene
ualif
=l-
r.ers:
a10-
106r99t88t
QC timits
t70-121)I 81-117 1u 4-L2Lt
Quality Assurance Officer
,terv
atL
con1ua
pproved:
ona I'E gseed+t-
concentrations and POt's for soils aret basis. (NA = not applicable or not available)
John
romo
AL I NH CHFO'IATOGRCTI
Fi lr
tJ.il(,?lo
108Erao
9ABBA
EAaaa
4B
LAur,tt
)3,C d tott
B 1 ga
a
tJuant Butpr-t Fr le: "UI400::D-i
I
I
I
I
I
I
I
I
I
I
I
I
tl
ll
il
I
it
I
ii
!l
ra
I0
F.Ii
r.l
I
L,:tr,
ro
Iall(rt
It2 ITA!,
at?1416 ?
Data Fr le: >t./1400: :D.r
Name : )(2UbY4 i "';'65 ;4UUllrsc | 5 i5t4.97. 0 i5;0 ;
ld Fr Ie: lU-U:4: :i']:L'[rtie: ID FILf FIJH APPLI']D1;(Last Ual rbrat tan:'/UUbUU'L4
erator IUt: BUBant Irmez ')0U?U9lected at: 9UU50g
; i{P
O, /l0'\.'Y 0 ;
U6 222
L9219
Op
Uu
1n
N I l'.lE tJtJn.;
: uL
E\IERGREEN AI{ALYTICAL, INC.4036 Youngfiel4_ -wheat Bidge CO 80033
( 303 | 425-602t'
VOI,ATILE ORGA}IIC A}TALYSIS REPORTPAGE 2
DateDate
lte
s2x2059405/0L/90
04 /26 /900s/ L2/9005/ L2/90
N
e
s Client Proiect No. 3Lab Pro'lecf, No. 3Effectife Dilution 3Method 3Matrix 3Lab File No. 3ltethod Blank No. 3
lrl-27761.0826SOI>v1
RBO
25
5
9
g( 8240 )
502s1290act? Y/N
COUPOI'ND
Pyridine
Surrogate Recoveries:
Toluene-d8
cAs *
r.10-85-1
93r
coNcuglKg PQt *
ttg/Rg
u
QC Limits
( 81-117 )
5
8,,'lifiers a
J
B*=
EUnlesquant
bu
tima v
analvzed forlimj.ts areaneEPA
se Ige
a
s column.at a concentration outside the calibration limits.l. cgncentrations and PQL's for soils areht basis.
Cr'/t:- tJ----.iioved:
J D Parker Quality Assurance Officer
l',1.t.t: l
.r:.o
:J-{
.:'.r :.1:{:{
-, . -r'.
!.1 ::, '.1
,-0:'. 1
.J.. L
-llro
L .,U
r:, - !D
rD s r-rLC'l),l''-
r.1 - ,J
,:l . -r --
rL,.:
1.1 '..
" :.1
l_a
i:,1Q.l
r:1 : .l. I '-:r"
:s. {t..
.- ,-l .:
.t- - ':,.,. :; .
l+ ,tr
- - .'u t:lrl..
(r ,!
-- .. '--l,.u
-t. "< +'( tfl1l -, ,r'-". .l
:t:)
:.J:.)
r.f1
.4
{.
{.1
lJ.-
o-
4J
.l
-tl
r0I-1
fl,
:.1
J
'-t_
.. ::
. J _ -r "'
:. ::1 :::
-. , Ji
.i .. : j
_i r',
,u ", J'l-'Ir "
!t-
(l rli t-'
' i"l
'q rl-
:-:i .' i:
rr-l'riJ
'u
,l:'
t.a
:,.
!-l
'ql-l
ti
,n
r"'t:. 'r' r -r-"I. -",I--r'
;.-:;i -----
.9,
:i
'I
et
t -!il
'i,
,1.
(i'
(::.
-a
r
k,
i:i'.:.,i'r:,.!f'.
,-l
i.i
4.,
,tl
q)
6i,i,
Fl
rl
,t,
rI|
'5'
:,
It:ifi
6
ii
ru6
[-,
ir,
lf'
o.((
{-r.t
tr',,('t.r.
',int',5 t-,l,;t-t(F
:leql
6,l
,t.n,ll
I
13r
lfr('r
'it€,lftrt
tlt
i::i"
C'c,c
FCIE
at:t,:-
(:
;it-(il
EVERGREEN NIALYTICAL, INC .4035 Youngfield_ _wbeat -Brdge CO 80033
( 303 ) 42s-602L'
VOI,ATILE ORGA}ITCS AIIALYSIS DATA
ssDateDateDateDa act?t Loss on Drying
Compound Nane
hane
ene ide
sulf
,,
oroethane
tate
v
-2-Pentanone
Xylenes
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
s4x2059505/0L/9004/26t9005/08/9005/08/90
N L2.6
e Client Proiect No. z l4-2Lab Pro'lecf, No. z 776Effectife Dilution : 1.1Method z 826Matrix : SOILab File No. : >VlMethod Blank No. : RBO
5
( 8240 )
010890
Cas Number
92*114 t90t
t not detec
Conc.ug/Kg "E?k;
2
7 4-87 -37 4-83-975-01-475-00-37s-09-26? -64-L75-15-075-35-475-34-3156-50-5
67 -66-3L07 -06-278-93-3
7 L-55-556-23-575-27-4108-05-478-87 -51005 L-02-679-01-679-00-s7L-43-2t24-48-L1006 1-0 1-s110-75-875-25-2108-10-r.
59 1-7 8-679-34-5L27 -t8-4108-88-3108-90-7100-4 1-4100-42-51330-20-7
351
1111L111
6110
6
6
6
6
6
6110
5
6
5
6
6
6
6
6
5
6
611
65757
6
5
6
6
5
6
5
U
U
UUJJu
U
UuJ
U
U
UUuUu
UJ
U
Uu
Uu
U
UJ
UJ
U
1
1
,
,50
48
3
5
9
3
13
QC Limits
( 7 0-L2LrI 81-117 1
17 4-L2Lt
Quali
B=E=*=
Lers 3 apalyzed for, buIrm.r.ts . are rougan estimated vi hIv1u6
rtincr limits.l.imi€s for- reagendetected, but is t water
ot
a
0
tat ona
EPA Quqnano.ti onLsA
ts st
i,
andtscEPAtectiontsare
sanole data.ibrbtion limits.18, Part II,leis than thecoumrl .essnti concentrations and POL's for soils aret basis. (NA = not applicable or not available)
Quality Assurance Officer
Approved:
Parker
l''
I
AL I O}I CHFDI1BTOGRBII
1686S
lEBABE
r rlnfifr.i
oE r:tq,E
tt611rJ
6 :rrr !
1
cII a ag ?aq
?
IIaVI
IQ
.n
Iao.t
Ia^
.)
,a t,
I
E
B1e14L618 a
0ata F'r le: >rJt4tJl.: :D4l{ame : )(2 Ur.,'t i,;..'o5 i 4Ul- i HPi'lrsc: 5;S i4.99: u i5 iU iut2.-Dii,.'90 i
id Frle: lU'd'142.il'LTTTIE: II] FTLE FIJR APHL.I]DI){L.rst UairbratrEn: /UU'.iUB 14:
Uperator IU:8UHljuant frnre2 ?UU?U9In.)ected at: 9U05BB
Quant Butpr-.;: Fr Ie: "(rl-+01: :D-t
N t l{E t-,Uas
iJl
0a:25
2AzO9
EVERGREEN AI{ALYTICAI{, INe .4035 Youngfield -wheat-Bidge Co
( 303 1425-602].',
80033
CIienLab S
t
s
E
l,l-22577 651. 158260 (
SOIL.>vl50
RBO51
8240)
4s95/oL/90/26/90/ t2/90/ L2/90
2005040505
e
VOI.ATILE ORGAIIIC ANATYSIS REPORTPAGE 2sx Client, Pro'iect No. 3Lab Pro'iect No. 3Effectife Dllution :Method 3llatrix 3Lab File No. :lrlethod Blank No. 3
coNcug/Kg
DateDateDateDate AnaMethanol
/Prepared
T? Y/N
COUPOI'ND
Pyridine
Surrogate Recoveries:
Toluene-d8
N 3290
5U
PQL*ug/KgcAs #
110-85-1
11Lt
8""li6tfi53,irra anatvzed for, but not detected above repgrti4g rimits.- ReD,Siiino-IimiEa-aie-iouqhlv method detection lifttits f5r 4eagent.Itater.J = inaIE;EaE an-eiEimEEed-vE1[e when-ahe compound is detected, but isbelow the EPA Practical Ouantitation Limit (PQI.).-B = E5fr65unii-roiriia--fi-5linE end--aample:-- eompard 616nk and sample data.7 = FidEtl6Sr-oufnti[aEio-ri--riilit5-1-i5ied in EFA SW846, vol. 1B; Papt rltDa. 8240-4I The minimum i.nstrument detection limi.ts are Iess tnan Enehumbers shown in this column.E = d6-ri65iia-ii'-iieEiicfiiii-at-a-Ccincentration out,side ,the calibration linits.UnIesS-othanrise notea all-concentrations and PQL's for soils arequantS.tated on a dry weight basis.
QC Limits
( 81-117 )
C,-V/L frApproved:
D Parker Quality Assurance Of ficer
I ,:'l
-ll$'.o
:..|.2-t
:.r:l:{:'l
.:l :.! =,-lt :t =t]]'-r.:.
. j .. r---(l!rn
t:L " Jrl .- 01
O+'uLtrILI,L.''
:1 :l -
rLl
C
D'i*: I
..t. :rL 'r
L,:.trl:r
l't
!l'-a
:-' r^
,.t0..
:r -":'..-.i -.
'.:. a,
l! ,r
...t rl :-,,Lrrl'l.l -.
rll a-. ".,.i'' rll
.!. - +',, tt1a] _,t].r--_l
:{:J
:.1,fjr
:.{
rLr
.t-.
o+'
lrl
+'
rf
l
-J
:l'l
_l
.i- '.. -'i',.:l
:.1 .-l ".
..., "
".....t]
ilt :1i 3
tt U_:..,]..'..:'
l'if
rl' ::, -li
a;. | ...
.t.-
o()Lr
' i.:'rlrn.,i
:J,.-::
I
,1"1
OJ
!l:,
-t
l!
1
t{
,.J
.{
.,t.
. ..(,
i,
-= ,jl
,
-. -t -,.,1,
,]
I'l
Jc='_
.lJ
,::'fj
::,.::.
'1!
l -sl
;-$1i
-ri1-a-T'r -Ia- r-r'.IT +,f, -r'[-r'1- t - "l-'r't-.T- r -l--i-r
,r.
i5,
(il
l::
t:i'
1tr:.,
,:lr:i
q:
.::
't
,:)
':l':i
'll
.::
:.,
nt
,t.
.t'
d
,5r
€,
.:r
'Xi
;t;,i',l',:.
t:..
"t
ET
lr:,:.
c'
,:':.
G.
.r:,it,
.,
;;.
lri
Cr(r.
'.:.':',
!:,..r:,t.r.
u:,
t:
': ,-i
';<.F
_l
a:al
Gr
rl,.llrlf
l,l,l.lr,
l"'t,' ,
Irr'l*r
l':ll
il-
,1(t
(-
Fql
rlx,::
l::
;i
t-(:i
,:r
.i
l.r.',
rl
..1
EVERGREEN NIALYTICA^IJ, INg.4036 youndriela- -iihEat-B-i4ge co 80033- (303) 425-602L'
VOI.ATIIE ORGA}IICS AIIALYSIS DATA
Cr.r-Lab Sx20
05040505
6s96/0L/90/26/90/ 09 /90/ 09 /e0
L2
ProiiectieD
ect No. :NL-27751.1826sor>v1
RBO
255
3
g( 8240 )
4L2s0990
DateDate No.ilution
act?on Drying N le No.Blank No.Loss
Compound Name Cas Number Conc.uglKg "E?k;
Chlo 7 4 UUU
U
UJu
U
U
Uu
UuJ
Uu
U
U
U
Uu
U
Uuuu
U
U
Uu
U
Uu
U
11111111
6110
6
6
6
6
5
5110
5
5
6
6
5
6
6
6
5
6
51L
65757
6
5
6
6
5
5
5
ene loride 13
1f
5-05-44-30-55-36-23-35-53-57-45-47-52-51-60-53-28-1L-55-85-20-18-54-58-48-30-71-42-5o-7
t
1 2
teDi
D roProPene 10
I -Tr oroethane
3 oroDroDenevinlI Ether r.0
orml-2-Pentanone
,hloroethanene
Benzene
Xylenes 1 1BJ
QC LimitsSurrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
102t107t104t
r 70-12 1 )I 81-117 1
17 4-L2Lt
8""lifiers:
terJ
B
E*
ess ontita
^LApproved:
D Parker Quality Assurance Officer
.a _.\..r!a ::,.|J-aatr.!l inrr-{. -' i-l' : ai'i ; iF
L :,: ..
5 ; .- ; .- .;1.: .;:i .i -1 :r,a!'., ',,
1.,..,r
.:i'ria:
'l
:.i.,.ir-ii t_l;,:;, .. l- i i;: "r.,r.L;'i.:! ir-.: -i
L!L
!t:
:=i
EVERGREEN AI{AI.YTICAL, INC.403G rounsriE1Brrl[EBlegitse co 80033
VOI.AULE ORGANIC ANALYSIS REPORTPAGE 2Client Samole NumberLab Samole- NumberDate RebeivedDate Samoledpate lxtfactqd/PreparedDate AnalvzedMethanol Extract? Y/N
couPot ND
Pyrridine
60s965/0L/904/26/905/ L2/905/ L2/90
sx2
0
0
0
0
N
Client Proiect, No. z 14-22r,iE-Frolecf, No. z 7765Effectife Dilution z L.L2uethod z 8260Matrix 3 SOI!taU f ite llo. : >V15
l,teEhoal Blank No. : RB05
coNcug/Kg
5
( 8240 )
04L290
cAs #
PQL*uglKg
1r.0-85-1
95t
U
QC Limits
( 81-117 )
lirnits.
5
9o"l
Surrogate Recoveries:
Toluene-d8
L iers:
an estEPA Pfound
E=Unlessquanti
r reaoentted, 6ut water.asl-
B=*=cal40-
amole data.1B'. Part I L1e5s than the
s
ibration lirnits.s aretatona
C.rL#
I
Approved:
J Parker Quality Assurance Officer
..1;.i
r
j:
.,n
'l!
1.1..
::l
,:1.
:l-
. . -,:1
:.t J.'
-. l,'.. . ...t''l:. "':.r e :-l
.t' ' ".., ri.
i. .n
:'. j
,Ll:: .ll-r-1..
. t-.
;i
1..
.l
:J
rtl
__l
J
'rij
,.1
!'r
r:.
(.1
fr
rI;.,ii..t
lr:,
t.
Etrl
.$
6l.1,
(.1
I
':
r:r
-l
0r
L.
.:,..r
.5,'
OJ
,i
l::
,.tJd
.t,.5j..
0.t
'.(,.l
t'
,rl
il.l
rl
rr:'
.t,:j
l-r
:{ ,j.:,i[, ..(,
t{
{!
-.
..:.,
-l i. :i,I -{
( -1!l
;.- (. ':i <-{:1:.t..'{.:l,:,1
--t -{
:.t.:.1
: l-{
-.. J,
! :,tn...,
;-, :-.:r - l
,. {1 ..
:1. -' ,
.:r
l! i|
-.r rl'.-
-... l: .(l,.1 -.
rl' ,n
., rl!
!.
{F
lJ :.:. ::
:1.! 1 r'1.
-..: .. -'_- ,L, ,.1"1:
]f.- rt
+! r-l.: ,t'
's,
'S'-,
'r'
(l(r
l:(:
l-{l
t!
--tl.:
;it-
t.
.t- "'' +'i. r(
Tf 'r
rn rll t.l
i. : rt1
'ni--.'i.-::'--l-1-,{;,t'r:.
'r-J-r -f ..1-T'-r-'t-l' T-1' .1 'a--l -"
r::.
,: i.
ri"r -'.'r'T
'::,
t::
tl ':.t..,1
t{
i:|.;(i(i,
r:r:.
r:.,
't,
o
, I-r',1;
t7,
r:.,
r:.. ''irrtl
,:.
't,'1'
E\IERGREEN AI.IALYTICAL, INC.4035 Youngfiefd- -I{heet-Bidge CO 80033
( 303 )425-602L'
VOI,ATItE ORGAIIICS N{ALYSIS DATA
5
( 8240 )
030890
22651560SOIL>v14
RBO5
u-771.
82
Client Pro'lect No.Lab Pro{ect No.Effectife DilutionMethodDtatrixLab File No.Dtethod Blank No.
Conc.ttg/KgCas Nurnber
8597/0L/90/26/90/08/90/08/90
13.8
Dx2005040505
N
s
DateDateDateDateMethanoPercent
Compound Narne
ene
tanone1-Tric
D
ic
D
Loss on Drying
PQt *ug/Kg
111L
1111
5r.10
5
6
6
5
5
6110
6
6
6
6
6
6
6
5
6
6
511
65757
5
6
6
6
5
6
6
uu
U
U
U14J
U
U
U
Uuuu
9
U
U
Uu
U
U
Uu
U
U
U
U
U
U
U
U1J
U
U
U2J
7 4-87 -374-83-9
7 5-0 1-475-00-375-09-267 -64-t75-15-075-35-475-34-3156-60-5
67 -66-3t07 -06-278-93-3
7 L-55-656-23-575-27 -4108-05-478-87-51006 L-02-679-01-679-00-5
7 L-43-2L24-48-L1005 1-01-s110-75-875-25-2108-10-1
59 1-78-679-34-5L27 -L8-4108-88-3108-90-7100-4 1-4L00-42-51330-20-7
D
D
Disulfidehloroethenehloroethane,2-Dichloroetheneormhloroethane
ide
2-Pentanone
hloroethane
oroDroDenevinlI Ether
,,
,
a
2
1
orml-
zeneBenzene
lenes
Sumogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
,,
i.ers:
t
QC Limits
t 7 0-L2LrI 81-117 Iu 4-L2Lt
I ts.orabovedetec
Et
83r94r85t
SuaIi
reaqent waterbut isJ
B
E*caVolare
Lt4'1'L
Quality Assurance Officer
samole data.Iibrhtion limirs.18, Part II,less than the
and
POL's for soils areapplicable or not available)
-c
rSS othe
'titated
ca140-
on
Johri
Approved:
D Parker
AL I ON CHPOTIATOBRA},|e )y1+a3 A-2AA O rrrr
DataNerne:llrsc:
TTC
1
1auu6u5
't
11UUUi'EF1
, -.....1,::::::
:e'r-tpdU.l
nnn^n^1,j I I r-,r-,,--l
zat*t.), ""*"- J
!i rrnrearej----'-
16aaaaa.,i------l
4aaaarll
3S80od
.l
PB88S&tl
i
I
I
I
I
I
I
I
I
I
I
t
I
I
il
il
il
I
ii
ll
ii
"',I4N
ir.4
Uo.322L:08
Op
UuIn
cl
It1rn I
'r1IaI
v)lgrrO
16 e1{1618 9"2
Ouant Outpr-ri FrIe: "UL+0'52zA-t>UI4UJ. iA4';:' ;, ).'/6: ; -lUU i t(P
. 05 : 0 i5 i 0 ; 05,'Dd,'9U :
Id FrIe: lLr lJ:{::illTrtle: ID fTue. FDH rjiFpLftDl;-i t.llt.lE rJuxsLast [alrbratron: irUiJbUg I4:U1
enator lU: BUBant frnez ',UUbUPlected at: 9UUr0g
Frle:7.'2Ur')E.c.(/tJt/
EVERGREEN AI{ATYTICAT, INC.4035 Youngfiefd- -wheat-gldge CO 80033( 303 | 425-602L'
te
VOI.ATILE ORGAIIIC ANAI,YSIS REPORTPAGE 2:Sgz X20597 Client Pro'lect No. 3: 05 /0L/9O Lab Proiect tlo. 3: 04 /26/90 Effectife Dilution 3: 05 / L2/90 I'tethod B: 05 /L2/90 Matrix 3: N Lab File No. 3Method Blank No. 3
t{-225
77 651. 168260 ( 8240 )SOIL>vl505R8051290
DateDate Prepared
xtract? Y/N
COUPOI'ND cAs *coNcuglKg PQI,*rq/Kg
Pyridine 110-86-1 u 5
Surrogate Recoveries:
Toluene-d8
QC Limits
108r ( 81-117 )
Quali
.J
B='*=
E=Unlesquant
iers analvzed forlimits arGraneEPAstfutraotfoundntt
8
a
0 r.n s c r.unn.
si isnea
at a concentration outside the calcgncgntrations and PQL's for soilt basis.
ibration li-mits.s arewe
C%,\L(^*'(*A.,.,roved:
Parker Quality Assurance Officer
-t
T
:'!l:f)
:;
D{tr])4D:t
rl
tl
t-,r,'l
r.rt
rrl
r5t
Ilt,t.
E,I
t:,
lu3
{)
|-':
l.
i-r l,i' ,..;. ,l:, .;.: ' ;':
..!rl I -!1.-r r-
I
.4.
::::il
r:! 'lrrli ':,l i r::
,l;, 1L,-,-:l.i
,.:'l
3),:!
l..rr
,: ,t
':i
.'i
..i,
,.. i,t.-r lJ
;>
:i ,' r:...n,:it il' u'
i-.,'l.it-
ttl t
-t -. l'
tlri -.ui r-ll
,. tIrT .'. -.-t --, .
Dr ,-r-l
,-t p 'l-
-,'t:-.
i, " --i-
.. r:i: . .
' .i'f.-' t'
'-. l,l
,.: :i
r', Clt-",-
:r l.!
, .l'
.1, -, 'i
l-r .+ [lt
il' ' L'
[J- ' -]
(!t t:1, '-.-r .. q.
.l:r ,: t[l
iU
t-
-t',.-r.' ,.,
Lr il'
t'r
'r: .; :.:i. .,:
._'rJ ,-
.. i' r-:
rl.lir.', .r
t:l-
:l-,
!-
II
F: !--
t.: f.:.
:nl'".
F
., -, .'.
rtr'
r [,]
,-.--E. |f,-,.I
r',
lr
P
'!,
P,t{,
t: -f
.. i
..,it
.],
TU.:i
t:
t
!r
tr
C
.-t-Ll
-I''
(lt
F..,,:i,
E\l;
f-it.
J:.'E:'
.g,
'$)
-,S,. 't'
,tf
-. r!,:,',5
;P.t.i,i.I rlr
I
I
i
I
t_.
.4,r1,i 's,L
t
L
I
EVERGREEN ANALYTICAL. INC.4036 Youngfief4 -wbeat,-BiQge cO 80033
( 303 | 425-602L'
VOI,AtrILE ORGA}IICS AIIALYSIS DATA
DateDa
Da
100598s/oL/904/26/905/09/905/ 09 /90
18.4
sx2
0
0
0
0
N
Da
1e
/Prepared
t?t Loss on Drying
Compound Name
Client Proiect No. z l4-2Lab Proiecf, No. 3 776Ef fecti.fe Di.lution z L.2Method z 826ltatrix : SOILab File No. : >V1Method Blank No. : RBO
5
( 8240 )
110990
PQt*uglKg
tete
1o
t
1
I
2 oroethane
o
ene oride
ans
ateo
Cas Number Conc.ng/Kg
U
U
UU3J23J
U
U
Uu
U
U32J14
U
U
U
U
U
Uuu
U
Uu
U
U
U
U
U1JuU
7 4-87 -37 4-83-975-0 1-47s-00-375-09-267 -64-L75-15-075-35-475-34-3156-60-5
67 -66-3L07 -06-27 8-9 3-3
7 1-55-556-23-575-27 -4108-05-478-87-51006 L-02-579-01-579-00-5
7 L-43-2L24-48-L1005 1-0 1-5110-75-875-25-2108-10-159 r.-78-579-34-5L27 -t8-4108-88-3108-90-7100-4 1-4100-42-5r.330-20-7
oro-Di,
vc
v
1
1
1
1
,
L2
L2
I
-2-Pentanone
zeneBenzene
Xylenes
Surrogate Recoveries:
1,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
roProPene
oroethanecne
oroDroDenevinll Ether 1
6
6
3
uBJ
QC Limits
t70-L2Lr
I 81-117 1u 4-L2Ll
ts.
96r98r99r
8""iers a
J
B
E*
or reaoent \fater, but is
samole data.librhtion limits.
€s are 18, Part II,1e5s than the
POL's for soils areapplicable or not available)
f- *fV',*,J
andcaVol
and
Approved:
D Parker
not
Quality Assurance Officer
TnTAt-. I0r.J DHF0tIATn6FOH
trila'rtjlrl'11 .s-?6 .9 anu.TIE
4 o I R EB 1 ga o
b
5
5
4
4
a
,)Ytau)
SqqE
6Sg6
5888
tttl7J9
EUBO
6gqa c{
Itnu)
I!8
I
I
rr,
I,Jt
t)t,6{
al,
It I.A1/)
1:1 LA 14 1,i B g"?
Uata Fr le: itJ:14'ILzzb4
I'iame 2 "/:,'2U,'t'd ;;'."65;4UEllrsc: 5;S i5.0j;U;5iU;! r{PU5t0')i'90i
llluent Output Fi le:'^Ul41l: :D]
Ld Frle: lO_L-;24::mIlrtle: lD FILE FOR flfrPLt'tDI)( r.llNE UOnsLast La I rbret ron: '/UU'.jU9 07:2L
Dperator IE: BUHUuant Trrrre i')Uljt.U9In Sected at : 9UU509
'I0:2J
O7 z5l
EVERGREEN AIIAI.Y TCAL, INC .4035 Youngfiel4 wbeqt-Bidge co 80033
( 303 \ 42s-602L'
/90/90/90/90
980126L2L2
10055/4/5/5/
DateDate
---entab SDate
couPot ND
Pyridine
Surrogate Recoveriesl
Toluene-d8
t iers r
sE=Unlesquant
VOI,ATII,E ORGAIIIC AT{ALYSIS REPORTPAGE 2sx2
0
0
0
0
cAs #
110-85-1
87t
above
Client Proiect No. 3Lab Proiect No. 3Effectife Dilution 3Method !Matrix 3Lab File No. 3Method Blank No. 3
M-2277 65L.2L8260SOIL>v15
RBO5
5
( 8240 )
06L290N
coNcuglKg PQL*uglKg
reDortinolifirits f6is detec
u
QC Limits
( 81-117 )
ibration limits.s are
limits.r reaoent water.ted, Eut is
samole data.1B', Part IL1e3s than the
6
flo.l
on
B=*=andVol.€s are
outside the ca1l-lCompounds othenriitated on PQL's for so
C?rL--.-.-roved:
J Parker Quality Assurance Officer
.l-t -{
':l i.,
: , .'rlr-{
:.r.: I
1 1:{
: i,: :,:
:t l.
-.. ,1, In
:L..1f,r..- t
IIJ +. rj
.- ': illt-
i.,.. :, .:
lL!
,.
1l'.
I.r
:& :rt
I rr 'rl
1'l .
,t ,nr.. --1' ttr
l. '' !'
-'.. rl'n .-..:...'
:t
t
:1
:.{
,ll
'J..
:.t-r
:!
-.t
rIl
-t
..1
:
--l
.i. ..
::'- i r -.
o......
:j t:. -j
J "'' :rl: ." il1
.| -i'
,li - j .ai
,-t.
|l: 'tl i-'
,i, : li
'!l -
'-.J . .:
,i I'tl
rr!
I'
.{
i!-:i ----..'
ra-r'-{'.-r i . J-rr-r'.1.
:: '51'r ,:,j' ':,lj Gl
:'., F I
l..j,
,!r
r'?rr'_ r' ' r',ctI,:r
,:i
lri
11'l:
.?
,t,ri
I f nr"I-rr
'i'.:'r:'
ril
rt.
:,
(U
,:.
,.t'r{
':'
rJ'rl'
i- ,i..o!,
.3'
ls..-,,
It.
,
L.
r
€:nl
lr
aril
1ir
Ir
4r
lr.
(l
tl!(!.
|-lI
rltI
ii].(:
l-
,: i'it
ra'i a 't_. a-t€
::i.:J.:lr
'a-1'fr
(;,ii,.::.
'i:t.-
EI/ERGREEN NIALYTTCAL, INC.4036 Youngfiefd^ -wbeqt,-!!Qge co
( 303 )42s-602L'80033
VOI,ATILE ORGAIIICS ANAIYSIS DATA
Pro ect No. :No.ilution
le No.Blank No
ient Sample Number : B, Sample- Nurnber t X2te Reeeived r 0Date Sanpled . 0D"g" E#iiEEed/Prepared ; 0Date Analyzed : 0Methanol Extract? : NPercent toss on Drying 3
Jecve
205625/0L/904/27 /905/04/905/04/90
9.6
I
D
Conc.ng/Rg
5
(8240!,
340490
POL*lg7Kg
u-771.82
22651060sorL>vl3
RBO5
Compound Name
h1
Cas Number
,
,
1111
1111
6110
6
6
5
5
6
6110
6
6
5
6
5
6
6
6
6
6
611
55555
6
6
6
6
6
6
6
U
UUU
U
U
U
U
U
U
U
U32J4J
UU
UU
Uu
UU
U
U
U
U
U
U
Uu1J
U
U
7 4-87 -37 4-83-975-0 1-47s-00-375-09-2
67 -64-L75-15-075-35-475-34-3156-60-567 -66-3L07 -06-278-93-371-55-656-23-575-27 -4108-0s-478-87 -51006 L-02-679-01-679-00-57L-43-2L24-48-L1006 r.-01-s110-75-875-25-2108-10-159 1-78-679-34-5L2?-L8-4108-88-3108-90-7100-4 1-4100-42-51330-20-7
or
1
-Tr o
te
ene
-2-Pentanone
eneene
Lenes
Surrogate Recoveries:
1,2 Dichloroethane-d4Toluene-dBBromofluorobenzene
ide
Disulfidehloroethenehloroethane,2-Dichloroetheneormhloroethane
iers r
ts arean estEPA
2
1
8""
Unlesquant
orf1t
J
B
E*
v
at
co umn.
87r115t101t
no
tas e
ts strument
abovedetec
EPA
3
andcaIVol.€s are
UBJ
QC Limits
( 70-121 )I 81-117 1
17 4-r2]-t
I ts.s
,
water
t
l-on1n
sarnole data.ibrhtion limirs.18, Part II,1e3s than the
sita on noteddry we
Parker
sea concentrations and POL,s for soi.ls aret basis. (NA = not applicable oi not available)
C-.t/h,proved:
Quality Assurance Officer
ao!,
TOTAL I OH CHROT,,RTOGRRT,|
i le )V1334 .o artlu
T
a a 1 og ?gs
11
10
.l
B
I
7gsgg
6ASAO
588A8
4aaaa
sqaDa
?oaBa
tgSgg
sl
I.4
c!
Io
ro
lv,ro
I8
Ia IIAIA
LA 14 16 1
Data File: >U1334::81
Name z X20562 t7765 ;40D ;RPllisc z 5 iSt5. 02i 0 ;S iD i05/04/90 i
Euant Dutpur Fi le z ^UL174: : D]
Id FiTitleLast
le: lO 924::11'l: ID FTLE FOR APPENDIX NINE L'OAStlal ibrat ion: 9005D4 t5:L4
Ooeraton ID:rf,'uant Time:Injected at:
11I KE900504900584 LBz75
1.8: 0l
EVERGREBN AI{ALYTICEI., INC.4035 YoungfS.eld wheat Ridqe CO 80033- (303) 42s-602L-
VOI,ATILE ORGAIIIC NIALYSIS REPORT'ent S
teDate
quant
Prepared
T? Y/N
205625/OL/904/27 /90s/tLl905/LLl90
Bx2
0
0
0
0N
Client Prolect No. rLab Pro{ecf No. 3Effectife Dilution 3Method rDlatrix 3Lab File No. 3Method Blank No. 3
lt-2277651. 108260sorL>vl4
RBO5
5
( 8240 )
691190
couPot ND
Pyridlne
rrogate Recoverieg:
Toluene-d8
Lers:
cAs #
coNcttg/Kg PQL*ug/Kg
for, bu
v
t
a a
110-86-1
96r
t ta ion
ts
t are
EPAfound
sea we
U
QC Llmits
( 81-117 )
I ts.reaoentbut isor
,
ibration linits.g ar€l
6
9""1 abovedetec
t
wateran
B=*=
s
€,s
amole data.1B-, Part If ,1e5e than the
and sVol.arenIIIIIII.
on concbas
concentration outside the calentrationg and PQL's for soilis.
nnproved 3
D Parker Quality Assurance Officer
r;reL I nN iFF:irl'lFr06FAn
i ! e i\r1.1 869.6 amu.rtc
4 I o 1 1668 e a8
1eg-186e
ItJB.3ge
7F-rBaAtl
f.tr |3rJ66
---."--1
J
t aetartr*)r ceees.l
l (\.t
I
JA
I,:!',
:lE[8r:r&l
!r$t-lrJ
tra 1e 14 1b 18 B e
Lt,aia Frle:rt_ _--. r!rr_.rtt-I td lllE . !\L U -'11r;c : I ;5;6t(:
Ul46li: : \J1
. -'...1ti' ..!i'r./ .)t.HrJUafur;u;'.i;tr ;fi
f,iuant Outpur Filez nVL469i202
icP
5 /L',L/90 |
id FiIe: IL.l_i-,'r,R::l,l IIr t le ! Iderrt t f rcat lrlnLast l-al rbrat tan: T :Jij oft:1I Pvrtdttre't O, ,r|f
Uc,arator IU: EL;i:i
lJr.r.3,-t t -[ r rne : '.) Ll :.1t, ]. IIniected at: 9UU51'I 1g: 09L7: L0
EVERGREEN AT{ALYTICAL, INC.4036 Younsfiet$or}lStlr$itr" co 80033
VOI,ATILE ORGAIIICS AIIALYSTS DATA
r-,6tODateDate AnaMethanolPercent
t
J
B
E*
Unlessguanti
)roved s
Loss on Drying
noteddry we
405635/0L/904/27 /905104/90st04t90
10.7
Bx2
00
0
0
N
Client Prolect No. z 14-22Lab Prolect, No. I 7765Effectife Dilution z L.L2Method : 8250Matrix : SOILLab File No. : >V13Itethod Blank No. : RB05
5
( 8240 )
350490
111111
11
6110
6
66
6
6
6110
6
65
5
5
6
6
6
6
6
611
6s656
6
6
6
6
55
6
UuuuJuUuUuuu
UJ
UUuU
UU
U
Uu
Uu
U
Uu
U
UJuuu
3
5
1
7 4-87 -37 4-83-975-0L-475-00-375-09-2
67 -64-L75-15-075-35-475-34-3156-60-s
67 -66-3L07 -06-278-93-3
7 1-55-5s6-23-575-27 -4108-05-478-87 -51005 L-02-679-01-579-00-57L-43-2L24-48-L1005 1-0 l-s110-75-875-25-2108-10-159L-78-679-34-5L27-L8-4108-88-3108-90-7100-41-4100-42-51330-20-7
2
Conpound Name
llet
sulf
tanone1-TrLc
ide
oroethene
-2-Pentanone
thane
en€!Benzene
Ienes
lers:for
an estowEPA
Cas Number
not detec
tationle.
flIIltI.
Conc.uglKg POt*ugTRg
4BJ
QC Limits
t70-L2LrI 81-117 1u 4-L2Lt
4
2
1
Sumogate Recoveries r
L,2 Di.chloroethane-d4Toluene-d8Bromofluorobenzene
$uali
83t95t95r
ts.
t t water
,
and samole data.ibrhtion li-urits.18, Part ILleis than theEPAtionts
caIl.are
ona concentratlons and POL's for soils arebasis. (NA = not afrp1ic-ble oi-not-availablel
-",.t*{Quality Assurance OfficerJD Parker
TOTAL I O}I CHRO},RTO6RAN
e
4
?6Agg
e4gga
2?gos
?osgo
LABOO
L6
t4
.D
1B
I
6
4
e
s
g
s
a
I
g
o
o
o
g
a6
a
Data FName:
11i sc :
.6 anu.
erator ID:ant Time:jected at:
TIC
D4 L9zD504 18: fB
1
N
Io
ro
Ia
14
Ilt)a,
c!
Itnv,
II
Iah(4
84
i lex2 t)5;5
Id Fi le:Title: IDLast Ea I i
z >Ut3J5z zBL Suant563 27765 :4DC ; RP
;5 . frt; o; S ;o i15/a4t90 i
lD 924: : MlFTLE FOR APPENDIX NINE I.'DASbrat ion: 900504 L5zL4
Outpur File: ^VLr35: :D]
Oo
AirIn
NIKE90059005
EI/ERGREEN ANALYTTCAL, INC.4036 Yonnsf iElii -liheat -Bi4ge co 80033- (303) 425-602L-
VOI,ATILE ORGANIC ANALYSTS REPORT
e
B4x20s5305/0L/9004/27 /900s/LL/9005/LL/90
N
Client Proiect No. z 14-225r.iE-Froiect, No. B 7765efEecEife Dilution z L.L2letlad- - 3 q209(8240)Uatrix : SOIIr- -r,a5-Fite llo. z >YL470 ^MeEtroii-Elank tlo. : R8051190
CONC PQL*ug/Kg ug/Kg
DateDate
? Y/N
COUPOI'ND cAs *
Pyridine 110-85-1 u 6
':rogate RecoverLes n QC timits
( 81-117 )Toluene-d8 92\
8,'"l l.ierE e analvzedlimits for detec 1 ts.are t water
B=*=
an estima v ,a and samole data.Vol. 1B-, Part II,are leis than the
sts fs
s trumentsco ion outsand PQLide the calsoil ibration limits.s areEaat a concentratI concentrationsht basis.'s forona
_,C/%- h*AAoproved:
D Parker Quality Assurance Officer
'r:Ttrl_ ! nu IHFr'lilgTfi6Fq]t
J
1a,.r rr I qtEr
14 [ir]AE qF
1e.iri8L1+
1 t_t tr !-rri il +
8i:lriQ
h14Elt
4q6tJ
trltltH
.S-e65.9 amu.
a I T T
q 1
18 1a 14 16 1E
1 8u1 ao t:t.l2
rr!
,t&r!
Io,.n
B a
Uato F
lYcr,llE.
11 r se :
1d Frl-rtle
t-cl 5 L
I Ie: >Ui4;rtj::ULlil r)t63 i ,:'.';,5:;;iu;5;5;4.9e!Di5:0;U
lilr,ant Outp,,' Fr le: ^U'1470: :D2
HP
5,. li,t9ult
le: l[:] P'i't?::lil: I'JEr'f rf 1trat1'lnUalrbrationl'rUii'l of
1.1
Pv
1!a
ridrne. !tD
Oc'erator ItJ: BLiH
t-JL ', rr t f :, rne : 1l Ll Li 1^, ]. Llrr.1eeted at: ?UB5'I1 1iJ: 09t7r4t
EVERGREEN AI{ALYTICAL, TNC.4035 Youngfield tfheat Ridge CO 80033' (303) 425-602L-
VOLATILE ORGAI.IICS AI.IALYSIS DATA
6;
Da
etete
s 640127
0404
B6x20505/04t05/05/
N
Client Prolect No.Lab Proiect No.Effectife DilutionMethodMatrixLab File No.Method Blank No.
5u-22
77 65L.268260SOIL>vl3
RBO5
/Prepared
t?Drying
/90190190'/90
0.52
UuBJ
QC Limits
t70-L2LrI 81-117 1
17 4-L2Lt
,.limits.
( 8240 )
360490
"E?k;
reaoentbut is
Percent Loss on
Compound Name
ene
-2-Pentanone
Benzene
Xylenes
Surrogate Recoveries:
1,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
I iers:
EPA
Cas Number
detec
tionle.ionintruslent
trations and POL'g forapplicabl
samole data.ibrhtion limits.18, Part II,leis than the
s arenot available)
Conc.ug/Kg
13131313
6130
6
5
6
5
5
6130
6
6
6
6
6
5
6
5
5
6
613
66363
5
6
5
6
6
6
5
uu
UU
UUuUUu
U
U
U3J
UU
Uu
UU
Uu
UU
UUuu
UU1Ju
7 4-87 -37 4-83-975-01-475-00-375-09-2
67 -64-L75-15-075-35-475-34-3155-50-567 -66-3L07 -06-278-93-3
7 1-55-656-23-575-2? -4108-05-478-87 -51006 L-02-679-01-579-00-s
7 L-43-2L24-48-L1006 1-01-5
1 10-7 5-875-25-2108-10-159 1-7 8-679-34-5L27 -L8-4108-88-3108-90-7100-4 1-4100-42-51330-20-7 2
84t92*94t
8""1 for,waterJ=
B=B=*=
,
at and
ts are
soileor
tI umn.Unlessguantl.ona we
proved:
J D Parker
(NA not
Quality Assurance Officer
OTAL IO}I CHRO}1ATO6RA}1
ile 3 6 anu.TIC
6 o o ga ag
4
4
4
36069
3?Sgo ia
It2
zBOOg ,Jt
Iu7.,lt2406N,l
sl
I(^!1
?604
L600
L?46 It6
aaaa
4ggg
1 L?4 61
Data File. >VLrr6
Name I X20564,7765lliscz 5i5;4.99;0;
::BL
;4Dt) ;s;o;o RP5/04/98 i
Quant Output Filez ^UL376z:D3
Id FiTitleLas t
le: ID 824::l1li- io-FTIE'FBFi-AppENDrx NINE rJoAs
Ca I ibrat ion: 900504 LDz L4
Doerator ID:Q'uant Time:Injected at:
11I KE90050498O504 LP 235
1,9: 08
E\TERGREEN AIIALYTICAL, INC.4036 Youngfiefd wheat-Bidqe CO 80033- (303) 42s-602L-
'ent Samole Number 3Sample'Number 3e ReEeived 3Date Samoled rpate Extfactqd./Prepared 3Date Analvzed - Bilethanol Extract? Y/N r
VOI.ATIT,E ORGA}IIC ANAI,YSIS REPORT
Bx
ldatrLab F
620s64os/0L/9004127 /9005/ LL/9005lLL/90
ect No.il-22
7? 65L.268260SOIL>v14
RBO5
No.lution
5
N No.ank No.
( 8240 )
7L1190
couPot ND
Pyrldine
rrogate Recoveries:
Toluene-d8
iers:
aI0-
foranalvzedlim1ts not detecare
found sL
co rrmn.
and samole data.Vol . 1B-, Part I Ls are leis than the
,
ibration limits.s are
cAs #
110-86-1
97t
coNcrug/Kg PQl,*ug/Kg
U
QC Ll-oits
( 81-117 )
tg.
6
8""1 waterJ
B*
E
L
seona
a
we t
t a concentration outscgncentrations and PQLbasig.
ide the's for calsoilUnlesquantBl-
Approvbd:
D Parker Quality Assurance Officer
iTti I nll i:HFOf ATTIFFCn
i ic rtllrl 3 .6-amu.
1E 1
l]ata Frle:
t'Ia rrre z .:,!.'l\'tllrac: 5;5.i
Id Fr le: lO-ri'R: :l':.1l'rtle: Iijentrf tr:attrrn ofLast Lalrbraticrn: ?ll Ul-1L
Ouent Outpr-,i Frle: "Ul471::Dt
c
s EB 1 BE 2 6
4 rl'i;:t E
'il lj t-l lJ tJ
ee Brr P
1'i6i ir
Eq
>U1.1,,'i::U'Ia4 i .,'.'o,": I 4Lll_ i HP .9at U i ti tJ : iJ5./I I/'9 Lt ;
?f)
r:
,|.,
P,;r r d r nelij: ;.iB
14 1b 18
tlgeratDr ILr: EUtluLant Ti;ie? 9l)U(, 1lIn.recterJ at : 9Utl5'l'I lLr: f 61,8: 09
EVERGREEN N{ALYTICAL, TNC .4036 Youngfiel4 nbeat Bidqe C0 80033- (303) 425-602t'
VOLATILE ORGAI.IICS N{ALYSIS DATA
',enrSt
rrdt€DateDateDate AnaMethanolPercent
Compound Nane
ene loride
sulf
1-D
-Dtanone1-Tric
ate
-2-Pentanone
act?toss on Drying
Client Prolect No. 3Lab Prolecf, No. !Effectife Dilution rMethod 3Dlatrix 3Lab File No. .Method Blank No. 3
I0s655/0L/904/27 /90s/ 041 905/04/90
2L.g
Bx2
0
0
0
0
N
u-22
77 65L.278260SOIL>vl3
RBO5
5
( 8240)
370490
Cas Number Conc.uglKg POL*ugZKg
13131313
5130
6
6
6
6
5
5r38
6
6
6
5
6
6
6
5
5
613
66464
66
6
6
6
6
6
UUuu3J13Ju
U
UUuuu7
U
U
U
U
Uuu
U
Uuu
U
UuuU1J
Uuu
4-87-34-83-95-01-4s-00-35-09-27-64-L5-15-05-35-45-34-35-50-5
7 -66-37 -06-28-93-31-55-66-23-55-27-48-0s-48-87-5L-02-69-01-69-00-sL-43-24-48-11-01-50-75-85-25-28-10-11-78-59-34-5
7 -L8-48-88-38-90-70-41-40-42-50-20-7
7
7
7
7
7
6
7
7
715
510
7
7
5710
71005
7
7
7L2100511
71059
?L210101010133
ilTr
e2
oroethane
Benzene
Xylenes
Surrogate Recoveries:
1,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
8"'Lers:
92r102t103t
3BJ
QC Linits
t70-LzLrt 81-117 1
17 4-L2Lt
1i
J
B
E*
not detec
Quqntano s ion
umn.
tB.
at
water
onUnlessguanti cgncentrations and PQL,s for soils arebasis. (NA = not apflic-6le-oi-not-ivailable)
aPproved!
J Parker Quality Assurance Officer
S.
OTCL ION CHRO}'RTOORRI,e >v1 R
4
13600
t[u.
11 )
L?g
110
LSO
9g
go
76
66
g
o
o
o
go
?4906
LASOg
NIt4
?Ie.lIttltn
oIahan
In
1l,
1 4 6 1
DataNama:
11i sc :
Fix
5
le
Ca ioli
Id FiTitleLas t
202 05L9 ziB
MIKE900504900504
Oo
ALrIn
la: >VL3r7::Bl
2CI565 27765 :40C ! RPi5i5 . 0a ;0;S; o ;65 toqtso ;
lD 824: : M1FTLE FOR APPENDIX NINE UOASbiat ion: 9OO5O4 L5zL4
Quant 0utput Fi le z ^UL337: : D,
erator ID:ant Tima:jected at:
EVERGREEN AI.IALYTICAL, INC.4036 Youngf ield l{heat -Bidge CO 80033
( 303 )42s-602L-
VOLATILE ORGAIIICS ANALYSIS DATA
-- ienrSteudt€Date
rs 1e
?Percent Loss on Drying
Conpound Name
chl
ide
1f
-D
tt-227765L.L78260SOIIr>vl3
RBO5N
100s565/0L/904/27 t905/04/905/04t90
14.1
Bx2
0
000
Client Proiect No. 3Lab Pro'lecf No. tEffectife Dilution 3Method 3Dtatrix 3Lab File No. 3Method Blank No. r
5
( 8240 )
380490
Cas Nurnber
IIIIIIT.
Conc.ug/Kg "E?k;
?4-74-75-75-
U
Uuu3J15JU
U
Uu
U
U31 J3J
Uu
Uuuuu
Uu
UUU
UuuU1JU
UUBJ
t2L2L2L2
6L20
5
5
65
5
5L20
6
6
6
5
6
66
66
56L2
6s8s8
6
5
6
5
6
6
6
,
7
6
7
7
7
1.5
510
7
7
5
7
10
71005
7
7
7L21006L1
71059
7L2
10101010133
,
,
,
tanone1-Tric
L ,-fr oroethane
.lS
ia
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
Qualiu=
J=
B=
E*
-2-PentanonGl
Benzene
Xylenes
1erB 3
ta
2
85r95t97N
abovedetec
QC Limite
t70-L2Lr
I 81-117 I
17 4-L2Lt
I ts.fox,or reaoent, but is water
B
andcalVoI.
€,s are
samole data.ibrhtion limits.18, Part II,less than the
Unlessquanti trations and POL'g for soils areappticable or not available)
^Lproved:
J D Parker
co
(NA not
Quality Assurance Officer
TOTRL ION CHRONRTOGRNfle >v1 35.9-?60.9 anu.
T
1
130
1e
11
1
Ebaas
?ggga
6560
56
4
J sl
Io1n
ro
Ia io
I?t,tn
"9060
tsog6
Ia
6t
It4
In
1 14 6L
Data Fi I e3
055;
I
>Ul.]f B: : Bl.66 t7765;40E : RP4.98; 0;S t0 tf,/04/90 i
Quant Output Fi le z nUt3l9: : OJName:
11i sc :
x25;
Id Fi le:Tit le: ILast Cal aI
DBFTL 242 tl11E FOR APPENDIX Nion:980504 LSzl INE UOAs4brat
Ooerator ID:QLant Time:Injected at:
T1I KE90a504990904 2021420:08
E\IERGREEN N{ALYTICA!, INq .4035 Youn6fiElil --Xheat-Bi4ge co 80033
;;;," liRI'*ri,,, *,,o**
ent Bx2
0
0
0
0
I05655/0L/904/271905/LL/905/ tll90
Client Prolect No. z 14-225
ti?":rt+3"8'I3rio,, z TrAuAElod--- 3 92A9(8240)I'tatrix : SOIIr- -r,a5-Fire no. z >vL472 - -frEEtroii-Eldnk uo. : RB051190
--tBDateDateDate AnaMethanol N
COI.IPOI'ND cAs #
coNcug/Kg PQ1,*ug/Kg
Pyridine 110-86-1 U 6
:rogate Recoveries:
Toluene-d8
QC Limits
100t ( 81-117 )
OualiO=iers:for,not I ts.
s s agent waterr-s?-
B=*=
an esti.ma v ,EPA P ts a ion and samole data.VoI. 1B-, PArt II,are IeSs than the
f L tstscatorrmn.ion outside the caland PQL's for soil ibration limits.E E a concentratoncentrationsbagis.UnleEsguanti BCta c s areonwet
( /4vL'oproved:
D Parker Quality Assurance Officer
,lTsl- I0r.l nHR0ilqT06F9n
.s-
4 B
16n;-ri&Fl.t
1.lir
4 ,13e
.tfiu.
I 1 BB
c
113 )
t Lll
-l
^ _ _ -'1
f
J- - _ -'trtitHrH". '-l
-,!
;.rrf A+i"" 1
1
1ur?LlslIi
ULlLltH
J
1
Eq
dE
BB
J ,_r
L.l
In
r}
I
:it 1Ll 1I 14 18. 1E
Uata F r le: )(rL47'^!.i itJll,iarrie: }(2Ll t a'; 1t"i,i:;+Ui-.:i-lPP'lr;c: $ i5 iD.Ou; U ;5!!J i ilr:"/11./'9U ;
iluant Outpr-i ; FrIet "U!472::D2
ld Ft ie: lU-l-''iR: :i'?IIrtle: l11 enttiru:attorr ofLast ualrbrattilrr: lrULl h1l.
Ff,,'t'l,l!U
r'rdrne: ilg
Lloerat'er IU: EUtsiUi-,ant T i i-i'e z )i.)l:tr 1'IlrrlecterJ at: 9ULl511 I /: DC'].8: }B
EI'ERGREEN AIIALYTICAIJ, INC.4036 Youngfief4^ -wlreat-Bi$ge CO
( 303 | 425-602L-80033
VOI,ATILE ORGA}IIC AI{ALYSIS REPORT
810x20566os/0L/9004/27 /9005lLL/9005/ LL/90
N
DaDa
',ent S e
)
- -teDate e
/Prepared
? t/N
COUPOI'ND
Pyridine
mogate Recoveries:
Toluene-d8
OuaIiO=iers:
ta on6ea
Client Proiect No. 3Lab Proiect No. 3Effectife Dilution tMethod 3Matrix 3Lab File No. 3Method Blank No. 3
coNcug/Rg
M-22
77 651.168260sorL>vl4
RBO5
5
( 8240 )
731190
cAs #
110-85-1
a concentratoncentrationsbasis.
PQt *uglKg
U
QC Limits
( 81-117 )
1 ts.
5
J=
B=*=
87t
for,not
an estima 1yue tare
EPA ststrumentBCatolltrltl .
or reaoent water, but is
and samole data.Vol. 1B-, Part If ,are 1e3s than the
t
ion outsideand PQL'sc
ts
calsoilthe ibration limits.for s arewet
Cqt h*r"LA-proved:
J Parker Quality Assurance Officer
-iTii InN r.:HFii,1trT0EPgil
i!e ii;14i3 35,0-e65.6 .rmu. Xii?t-,o6 I 7?fr! ia[[ iR? .i i';; i5,tll. i h ti:A t9n. 1
1
I
I
408 8AE leBA !6A6 'aBE8
,-*8",,a,ra.hI
I:.:rltBBrliI
1
I .- +r..a !t !{ f
.. --^^^i!ry-!Z'rrUEri
-l
- ----t
t
'iIl;:rl;,1il
l
. iaul rlrirH j
f, ij rl 11'.J r}i
;1
| :.-' j'jt::t:l1
1 1.,
I
') '7.4 ,.a ta
?;4r.1rtfr
,]I
II
{i
I
t!1
il
1 !-1 11 14 1t Lr-.li
Uata F
i i.l lilE .f"lr,.ci
rlE|: >t-,14/'j::t..,1lii U'.:rtrr:. : .'..!Rir : 4Lll- : HF
S i=ib . []1 ; u iu I u i Lt(r',''l I,'Yll :
Uuarrt Cutor-,i Filei "UL471::D2
id F r'1.itle
Lds f
ie: lLr-P'iR:;:1I: Ider'rt r + ica i tr:n ol-al rbrat inrr: !li Li"-:, I f P."r'I ',t.JI tu
r rdrne. r:tJ
Ucl-ratur lU: EL:iiul,:nt I r;i'e i rLt:-r:11irr.;*cted at: Yl-l ll5ll ).'l z 1F"t19: 08
VOLAT
hod Blank Nunber ! RBe Extfactgd/Prepared : QuateAnalyzed - 3 0
B1IERGREEN ANALTrICAL, INC .4035 Youngfield l{heat Bidse CO 80033- (303) 425-602L-
ILE ORGA}IICS AI.IALYSISIIETHOD BLAI{K REPORT
DATA
C1ient Prolect No. : M-Lab Prolecf No. 3 77Effectife Dilution : 1.ltethod t 82Lab File No. : >V
Conc.rtg/LCompound Nane
-Tr
nzene
_s
Cas Nunber
fox, bu not
ts
225
650060 ( 8240 )1353
0s0790sl07 /905/07 /90
PQDltlgl l)
Unlesguant
i.de
se we
1
1
1
1
10
1
5
5
U
Uu
Uu
UuU
Uu
Uuuuu
U
Uu
U
Uuuuu
U
UuuuUJuu
UJ
I
1
7 4-87 -37 4-83-975-01-47s-00-3?5-09-267 -64-L75-15-075-35-4?5-34-3156-60-5
67 -66-3t07 -06-278-93-3
7 L-55-656-23-575-27-4108-05-4
7 8-87 -51005 1-02-679-01-679-00-5. 7L-43-2L24-48-L1006 1-0 1-5110-75-875-25-2108-10-1
59 1-78-679-34-5L27-L8-4108-88-3108-90-7100-41-4100-42-51330-20-7
10
oroDroDenevinll Ether
2-Pentanone
Xylenes
Surrogate Recoverles:
L,2 Dichloroethane-d4Toluene-dBBromofluorobenzene
iers:
88t95t106t
ow
Suali
B=E=*=
ter
ion
t
si tions and POL'g for soils are(NA = not aFplicable or not available)
proved l
on
D Parker
umn
Quallty Assurance Officer
ct.(h
t^i a:l
N$lr{ -l
r\N,=c,
r. Ll\l0= =:-1 .-.,-gl,].o'
It-l .. P-ooEL -tfoFovuO#fJLCO
tL) rB 6g..l C
Cl C3*
a.:I
13
!JZ
H€z.t
X,tl
tl
jJ-
iL.f,t-=C-
'{S
.. if....LL c..1 0l.l.tJ a
^t-r J #l* ro(]lr r-
-oQa
(1(}d..._Ja !l)
LL <.r.
#(0
T-O*F-l
lf)o
t\t$r\r{>
o
l!
Jo-P1o
ucoa13
'J\
NaE'iz'.{3.*'l\'..i-J'=
l^,':l O
rr...3:{cf .^.)o\.=
lf3
oi:r3-ttr ".-li$.ir
oofJ
-810rlll!a
ulr2_
o
'n
.G
rl
Erl
r-5s
'5t Nl /3 Gr f] o (i,6)Clr!€!3Ci(l}{$ Ci' ,! (li ,t A (S$t rr 15! {r i'J o} t
'u CJ (t.J rl .l
t- $r
c.-ss
C-SS
rt!
r5r.utrr
c.-sr
Gi6'(:,(,fi,
ai6?
ol
rsl.s
rl
6l
(J
F
G,to
rl:-
0l
f,Eal
CIc:(!.
LF(I
c,.I.C
L
a
F.C,
EVERGREEN AI{ALY]TICAL, INC.4035 Youngfield- _wheat -Bidqe CO 80033- (303) 425-602L'
thod Blank Number : R8050490 Client pro'lect No. z il-2te Extracted/Prepared z Q5l.Qq/.98 laD Prqject.No.. z 776-ate Analyzed - 3 05704790 EffecEiie Dilution i !.QMethod t, 825Lab File No. : >Vl
VOI,ATTLE ORGAIIICS N{AI.YSIS DATAITETHOD BI.,AI{K REPORT
Cas Number
25
500(8240)328
Compound Name
cI
1
ide
oroethane
Conc.rtg/L PQIrllqt L
74-8
7 4-875-075-075-0
67 -675-L75-3?5-3156-6
67 -6107-078-9
7 L-556-275-2108-078-81005 1-079-079-0
7 L-4L24-410051-0110-775-2108-159L-779-3
L27 -L108-8108-9100-4100-41330-2
TrL,-Tr
-I{e -2-Pentanone
eneene
Xylenes
Surrogate Recoveries:
iers:
1,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
10101010
51005555
5
51005555
5
55555510550505555555
uuuuuuuUU
U
Uu
U
U
UUu
Uu
Uu
Uuuuu
Uuuuu
U
Uu1J
ene
oroDroDenevinfl Ether
90t90t104t
Pr
8""1
B=E=*=
for,not
llllln.
tB.water
Practinb ion and samole data.ibrhtion limits.18, Part ILleis than the
at al1.area
0 trument
concentrations and POL,s for solls arebasis. (NA = not applicable or not availablel
rroved:
on
D Parker Quality Assurance Officer
TAI.. I NN l]lIFOHATO6PQt'
d-)ae IIE
4 o g
Ic, Frle: ID-H24::',11Trt Ie: ID FILE FORLast Lal rbrat ton: ,
B L1
Quant Output File: ^U'l32BzzDj
,,
1 BA 1 $a ?aaa
aah
?ELl8E
5cEr-iE
3468i
?aBaa
1LI'U
Le9B€
aAEra
a rrah
nIt4
r)
It)
i\
a,,,s{
I
I,4
!n
e1416 ?
Data Fr le: >U1-i2B: :BlL
ii.:n-re : i<EU9U4irU ; ;;l-il:; RPllrsc z 5 iu; 0 ; 0 ;1.,,; 0 ; 85 /44/90 :,
PFENDIX l'{Ir'iE UOAs
Li5 U4 '15: L4H
0
Doerator IIJ:uLant Trrne!In.;ecterJ at:
t1l iiE9u0504
90U50ci
}5:'I4LczSL
BI/ERGREEN AI.IALYTICAL, INC.4036 younsfiet$orixiBlrglin" co 80033
VOI,ATILE ORGANTCS AI{ALYSIS
I.IETHOD BLAI,IK REPORT
DATA
:hod Blank Nunber : RB:e Extfactqd/Prepared : Q-ateAnalyzed - ! 0
Client Prolect No. BLab Prolect No. 3Effectife Dilution rMethod 3Lab Pile No. r
Conc.ng/L
u-225
77 651.008260( 8240r>vl381
0s08905/ 08/ 905108/90
Compound Name
or
-Tr
ide
Disulfidehloroethenehloroethane,2-Dichloroetheneormhloroethane
te
Cas Number
not
PQIrlug/L
v
10101010
5100
555
5
5
51005
5555
55
5555105505055
55
5
5
5
u
Uu
U
U
U
Uuuu
U
Uu
U
UuuUuuuu
Uu
UuuuuUuuuu
U
74-87-374-83-975-01-475-00-375-09-267 -64-L75-15-075-35-47s-34-3155-50-s
67 -66-3L07 -06-278-93-3
7 1-55-6s6-23-s75-27-4108-05-478-87-51005 L-02-679-01-679-00-5?L-43-2L24-48-L1006 1-0 1-5110-75-875-25-2108-10-1s9 1-78-579-34-5
L27 -L8-4108-88-3108-90-7100-4 1-4100-42-51330-20-7
1
,
,
,
2
ene
Unlessquanti
rroved:
-2-Pentanone
oroethane
Surrogate Recoveries:
L,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
Benzene
Xylenes
iers:
90r104t108t
$uali
?-
B=E=*=
analvzedlimits forarean estina
D Parker
abovedetec ts.or reaoent, but is water
tBA
concentrationst basis. (NA =
POL'g forapplicablandnot
sanole data.ibrhtion limits.18, Part ILleis than the
h*andatcalVol.ts are
soils aree or not available)
Quality Assurance Officer
TOTFI. ION Cr{ROtlETO6R9lte )v1381 .o .9 anu.t,TIC
og og
4Agqo
440D
409
ta
Io
36gO NIo(A
,n
tB
JCg9
a8600
{\{
II
?4Agg
c .t9'
1 Ia
1
I
4g
?14 18
Data Fi le: >ULJBL::Nama: RB050B9U; ; 4llrsc z 5 i$i 0 i 0;L'.J;0;0
o40rl;5/O
Quant Output Fi le: ^ULf8L::Df
RP8/9O i
td File: ID 8'24zzl1].TitIC: ID FTLE FtrR APPENDIX NINE UOASLast Ealrbratron: 9005Llg LD'.44
Ooerator ID: BUtsQi:ant Trmez ?00508In jected at: 900508 lBz45
09 z2t
4036 yBXHEgIEiH iilf"X[1fitta"'86' eoos g' ------ - ( j03 r42 s_602L-
vor.Ar rffi ,g8silIis*ffir6f,f; s DATA
hod Blank Nrrnber : RBO50ggQ Clielt lroJect No' z \--2ii-ExEiadteiirEiared i -X17,8?7,t8 gi?":Ut+3.Erl3tio,, ,,
1r,8r.rdr. Anaryzed , ostoeteo
fiiif;Fii"="]].o".o' : q?H
25
5
0
8[8240 )
Compound Name
ene
-D
J
1-
TrL,
2
ide
v
-2-Pentanone
sea
Cas Number
not
Quanancl ta
at
nstrument
Conc.ng/L PAqlttgl tr
te
7 4-87 -37 4-83-975-01-4?5-00-375-09-2
6? -64-L7s-15-07s-35-475-34-3156-50-567 -66-3L0? -06-278-93-3
7 1-55-656-23-5
7 5-2? -4108-05-478-87-51005 1-02-679-0L-679-00-57L-43-2L24-48-L1006 1-0 1-5110-75-875-25-2108-10-159 1-78-679-34-5L2? -L8-4108-88-3108-90-7100-41-4100-42-51330-20-7
10
r.01010
5100
55
55
5
51005
5555555555105s050
55
555
5
5
U
U
Uu
U
UuuuU
Uu
U
Uuu
UU
Uuu
UuuuU
Uu
Uuuuu
UJ1
I ,
Benzene
Xylenes
Surrogate Recoveries:
1,2 Dichloroethane-d4Toluene-d8Bromofluorobenzene
8""r-erB 3
93t109t98r
rL
J
B
E*
forare
lre
abovedetec
ts
I tE.t water
s ,t a
co umn.concentratt basis. (
ions and POL's forNA = not applicable
and 1c
ts are
soil B arenot avaj.lablelor
s18, PIess
Un1essquanti
proved:
on
D Parker Quality Assurance Officer
TNTAL ION EHRO}IATOGRAh
a \trl a
9gsg
SBSgg
7g&
6AA
58
480
306
a8
LSg
d-2ad
4
18 1a 14 16
TIIo 11 a
?
Quant Output Fi le: ^UL410::Df
r\l
Iu
ro
Ig
,.)
IA
N
Ia
I0
.t
ll't
Data Fi le: >V1.410: :D4Name: R8050990;;4UCi RPllrsc z 5 itt; 0 i 0 ;Ui tl ;D5t09t9O i
lD ts24::m'lD FTLE FORrbrat ron: ')
ld Ft le:Trtle: ILas t lla I
Uoerator lD: BUBQi.rant Tima: 9U05U9lnjected at: 9o0509
IX NINE UOAs
D7 z'2LAPPENO
DUSU?
872280a:58
BVBRGREEN ANALYTICAL, INC.4035 Younqfield tfheat Ridqe CO 80033- 1303) 425-602L-
VOI,ATILE ORGAIIIC ANALYSIS REPORT!{ETHOD BI,AT{K RBPORITPAGE 2thod Blank Number : R8051090 Client Proiect No. 3_ te Extracted/Prepared 3 Q5/.L8/.9Q laD PrejecE-$o.. 3Date Analyzed - 2 051L0/90 Effectife Dilution 3I'tethod tLab File No. 3
$-225
77 651.008260(8>vL432240l
CO!,IPOI'ND cAs #
coNcug/L PQI{*rtglL
Plrridine 110-85-1 U 5
irogate Recoveries:
Toluene-d8 9r.t
flo.lL'
L iers:fox,detec ts.are waterJ
B*found lon POL} .ElAnk andSW845, Vol.limits arePrsamollB;Iess
e data.Part If,than the
E=Unles
umn.sea
a concentration outside the calibration li.mits.ions and PQL's for soils arequantEl-on we concentratt basis.
A/r-t^rt"Approved:
D Parker Quality Assurance Officer
TilTBl. I0tr nHF'0|lBTOriF Am
F: !: ;'V143?lmu.,,TII
446 8P'4 1a[iB 1,iEA eEelB
44i:rE 6
.-ir.r,Ht r!
3iuS6&
euesE$
e4aEBS
383BBLltJj{r a.:'lr'inrl{-'- --.t
1
lc
I ntl
413ri'E
ia
I
V'
I.nNI
I
Iw
II
I
I
I
!t
!l
I
lt1
18 1a 14 1r. 1Er
lJaia Frle:i:.rrne: :-:LiUr'I
11 rsc: 5,it^,;ll
i.;IP
..,1.0.,,911:
>r"ri4.i2::tJi:',iJ: i;iii::
: tl : t^! : ll : Ui,
1i; :41
o9 |55U l.iir 1 U
llr-1510
Suant Dutput Frle: ^U'14]2zrD2
ld F rlrtie
r.-d5 L
lic
,-lUIn
Ir'\ ,.-t,t!,. - tlliEi lU r.,at.. ,l: IL) FTLb. FUr..: AFF',fi'{DiX I'lit'.iE UllinsLalrhr.ati,:n: ;i-t l_t r.;,j.0 li.i :U6
erator l0:,3nt Tl;,ie!
letrted at:
l-'DE'7
9
EI'ERGREEN NIAI.YTICAL, TNC.4036 Younofield tlheat Ridqe CO' (303) 425-602L-80033
VOLATILB ORGANTC ANALYSIS REPORTUEAHOD BI,AI{K REPORT
hod Blank NurnberDate Extracted/PreparedDate Analyzed
a
RB0511900sltL/9005/LLl90
Client Prolect No. z ll-2Lab Proiect No. 3 776Ef fectife Di.lution : 1.0Method r 826Lab File No. : >Vl
coNcug/L
25
5
00[8240 )
couPot ND cAs #
PQrrltJgl l)
Pyridine 110-85-1 u 5
rrogate Recoveries:
Toluene-d8 87t
QualiU=r.ers 3 analvzed forIi.nits are abovedetec I ts.or reaoentbut is water
B=*=
aneEPA tima ,tationsamolts lis and sa.mole data.Vol. 1B-, Part If ,are less than thetrument
E=Unles
9Cato lltrlll .ibration limits.se c a concentration outEide the calgncentrations and PQL's for soilbagis.s arequant5.ona
L.74f\-rhrv,kprovedl
D Parker
t
Quality Assurance Officer
lrpi. IttrJ cHR0irsrn6Bsn
,|2B
4AA
i,
L?64 lqaa
.tmu.TI
Ii, ^ - - .a<l<lEuut'tI
{aiBadI. __-_iJbgauw
1
^^^^^^1J C.J 'JZrZ:li
eBE BB;3jj- ....:-.l
I2BA3B&l
i
I
I
I
I
ll
ll
I
c.l
0,
I
,r 18
?4.$q
t!
168.3r!
BBEB
46rl i
1B
iti: 89
L6z 4$
e14
Oata F
i;,- me :ll r sc !
I le: >U14C,E|::tJl
HBU5I1'-ru i i4i-1.-.: hlP
5 ;il i U .: 0,: t^t i 0 .; $5,'L L,'9 0 i
Ouent Uutpu: Fr le:'\UL468: :D2
ld Frle: ilj t}rR::111.Trtle: I,ierrTif rcatron ofLast llalrbratiorr: 9ULi 5LL
,.,oerator IU: BljUULant Tirne: 9uij5L1Irr-rected at : 9U1.,51"I
Ps1
rirJrne. !tt:,
4 036,3YHBEI3ii-iiBEI[1Etta"'d6' s oos,( 303 ) 425-602t'
VOI,ATTLE
uIIlIl .
a.
Client Prolect No.Lab Prolect No.Effectife DilutionMethodLab File No.
I REPORT
fs
2thoq Blank Nqmber : R80512
_-.3 xf;Efff83d/PrePared i gllil 00
69240 )
u-2277651.008260>v14
5
couPot ND
Pyridine
rrogate Recoveries:
Toluene-d8
SuaIi iers:
a
cAs #
110-85-1
115t
not detec
ionstB
coNcug/L PQI{*rtg/L
U 5
ts.
?-
B=*=
or reagent water, but is
and sample data.Vol. 1B-, Part ILare le3s than the
slAe t a concenlration -outside _the calibration li-mits.cpncgntrations and pel.,s foi soIIB-a-e--Dasl-g.on
Approved:
Parker Quality Assurance Officer
f.{
:
.:N0$
f{>
o
tL
fo-
lif
v
Cofi3
r'{
'.t'rl
trf--
':d
r,
|.drt
tr!
3
s
3
=
0!c
El\-;.1
>'=rL.<
t'-!ir
6r6'6''*.
.6',rsl(r-rl
.
ls,,6(u-il
trr.6r-
ocr.
.
as'6-o.
.{ O\!..l.if
- C'\
:-{ @
+c.l
O '-r.i,\
O=
i-l i+
i: +'.. o..
,I-o';r- + a
--l -plslol3Cr-.* rLl fi1l ..
oo<..Jd0)
iJ-- g
si0?-o
-F _J
r]\
f'lc-.-ld:L: \f ...'J\..;,=..,3 ".l.i=)'Jl 'q'a
'f,.-.=:{,3 ".>, ,.'=
,\ ;{ 'nr-l r:f
llli:l 3..,ll ...
-:I tc.lr
ooo!Et0n!lllr
IJ^IL
t
"{
ftlr(
l:,rl
Lr:(
C,E+
c3(r'
C'Jr{
Ii:6L!tr,E01F
Jertt
{s
(B
10(u
I
{st
r)(v)
Ot(n
-.t.
FI
>-
OJ
e.lc.l-{ .{
z-ss
TiT"T
(ir(a(i
'J. !J'
--tl:: =
Ultr '1
LJ..#-oo
r- Ir:oFo
Os rJLC0)tU ,t1 -tO--i cl-'i ae -
<-:
ci,()t
r{
(n(i,(o
t-&-T-,5t-t-T-r-r r$a- r
Gl6,!,:lGr'sts,!)6i qr :U C)(.tl qt $ 4)nt ru ,:'.! {1,
rlJ
{1
'3.,rJ
r{n'(G(a
E(re&
FClE
uIC.
c.
CTt-Cl-
EI'ERGREEN ANALYTICAL, INC.4035 Youngfield- _l{heat-Ridge CO 80033
( 303 1425-602L-
MeDaDat-
vor,ArrLBr98ffilIf;^*N/ffi$8f;f; REPoRT
PAGE 2r Blank Number : R8051490 Client Pro'lect No. z ll-2lxtracted/Preoared : 051L4/9O Lab Prolect No. 3 776Analf-ed- ' 3 05/L4/90 EffecqifeDilution:l'QMethod z 826Lab File No. : >Vl
52500
5
coNcrtg/I'
69240)
POqlvql bCOMPOI'ND
Pyridine
Sr gate Recoveries:
loluene-d8
Qualiu=iers:
an esEPA
for, bu notare
ts
u[r[.a conc
cAs *
110-85-1
82*
ion
entration outsations and PQL
amole data.1B-, Part ILleis than the
u 5
t water.isT
B*
E ide the's for
and sVol.g are
calsoil ibration linits.s areonllye
concentrbagig.
Uvr h,t*tApproved:
Parker Quality Assurance Officer
Ti'lTAi l nu nHFffilgTfrGegil
r ll* .)vLflr! ,{a.l,-
b3,,UULt
+ l-j t:: l:t E }J
4 4.-iE'1r1
)n i:.
I
-- l
4r:.4
Llata Filao')e:
11 t a'::
ADLI .
1E 1P 14 1r.
TIL:4oa 8BB 12r,1 t6r1!, PAAE
, i .'i-: I . i I . i I i | : I
rt
I
ll
I
Ll
I
a
I
I
il
:I
4 19 Q .)
rle: >U150?::u!
i":B Lr
'
i 4'J L'l : ; -;.i il i ;-jPr I u ; o ; o ; i,t ": o ; Ltii ." L4,'9 fi i
(Juarrt [utput File: "Pf509::D2
Id Fr iTriie:
L,J3 L
E: lu i}i"R:::'i.Ll,lenf rf 1c,3ttorr ofai ltrr',3t it:ni 'j:il.l ';'iii Pv
1L
rl:l ,J r ne
2
lljr-';rator ltt: EUti..'.i:ar',t Ti;;ei ')i: :-l trr14
Inrected at: ?[U5].4 l- a . {-'07242
YI-225 SOIL BORINGS
CONSTITUENT
I,{ETHYLENE CHIORfDE
METHYLENE CHIORIDE
METHYI,ENE CHIPRIDE
METHYLENE CHIORIDE
METHYLENE CHIPRIDE
METHYLENE CHIPRIDE
METHYLENE CHI,ORIDE
},TETHYLENE CHIPRIDE
METHYLENE CHIORIDE
I,{ETHYLENE CHIORIDE
I{ETHYI,ENE CHIORIDE
I,TETHYLENE CHI.,ORTDE
I,fETHYLENE CHI,oRIDE
METHYLENE CHIORTDE
METHYLENE CHI,ORIDE
I.{ETHYI,ENE CHIORIDE
I.{ETHYI,ENE CHIPRTDE
METHYLENE CHI,ORIDE
METHYI,ENE CHI,ORIDE
METHYLENE CHIORIDE
I,TETHYIfiNE CHI,ORIDE
I'{ETHYLENE CHIPRIDE
II{ETHYI.ENE CHIPRIDE
I,TETHYLENE CHIORIDE
I.{ETHYLENE CHIORIDE
METHYLENE CHI,ORIDE
METHYTENE CHI,ORIDE
ME?HYI,ENE CHIPRIDE
METHYLENE CHIORIDE
I,TETHYLENE CHIORIDE
I,TETHYLENE CHISRIDE
METHYI,ENE CHIORIDE
METHYLENE CHIPRIDE
I,TETHYLENE CHIORIDE
I,TETHYLENE CHIPRIDE
MEPHYI,ENE CHIPRIDE
I{ETHYI,ENE CHI.,ORIDE
METHYI,ENE CHI.ORIDE
I'IETHYLENE CHIPRIDE
I,TETHYI,ENE CHIPRIDE
METHYI,ENE CHIORIDE
I{ETHYLENE CHIORIDE
I'{ETHYLENE CHI0RIDE
METHYLENE CHIORIDE
METHYLENE CHIORTDE
I,TETHYI,ENE CHIPRIDE
METHYLENE CHIPRIDE
I'IETHYLENE CHIORIDE
I.TETHYLENE CHIORIDE
LOC
B
B
B
B
B
A1
A1
At
A1
A1
A1
A1
A1
A1
A1
A2
A2
A2
A2
A2
A2
A2
A2
A2
A2
A3
A3
A3
A3
A3
A3
A3
A3
A3
A3
c
c
c
c
c
c
H
H
H
H
H
R
R
R
UNIT
ttg/Kglg/Kg
uq/Kq
vq/Kq\q/Kglg/Kg
ttg/Kglg/Kg
ug/Kg
ug/Kg
og/Kglg/Kq
vg/Kg
Dg/Kg!q/Kg
ug/Kg
!9t/Kg!q/Kg
ug/Kg
ttg/Kgt
ug/Kgt
ug/Kg\q/Kq
\9t/Kglg/Kq
oq/Kg\g/Kq
ng/Kglg/Kg
ug/Kglg/Kqlq/Kg
ng/Kg!9/Kg
vg/Kg
ng/Kg!g/Kg!g/Kglg/Kg
trg/Kglg/Kg
ug/Kglg/Kg
ug/K9\q/Kg
ng/Kg
ug/Kg
ttg/Kglg/Kg
DEPTH CONC.
6
GROUPPQL
6
6
6
6
6
6
620
6
620
10 3
3
3
3
3
3
5
3
4
3
3
3
13
4
4
2
8
L2
2
L6
4
18I
4D
10
L4
6
2
20
16
4
L2
6
18
10
L4I
L2I
16
4
18
6
20
10
2
L4
9
L7
3
10
11
3
3
3
3
20
10
6
620
5
6
6
620
5
6
7
6
7
6
6
6
6
6
7
6
6
6
6
6
6
6
6
6
5
6
6
6
6
6
6
6
6
6
6
32
5
32
1
t
t
1
L
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
3
4
4
4
4
4
4
4
4
4
4
5
5
5
5
5
5
6
6
6
6
6
7
7
7
I
4
3
8
4D
6
2
4
10
8
2
4
6
10
2I
4
31
M-225 SOIrr BORINGS
METHYI,ENE
METHYI,ENE
I.{ETHYIENE
I,IETHYTENE
METHYI,ENE
I'IETHYIANE
UETHYLENE
CHIORTDE
CHIORIDE
CHIORIDE
CHIPRIDE
CHI'RIDE
CHI'RIDE
CHIPRIDE
R
R
s
s
s
s
s
6
10I
6
4
2
10
4
4
6
6
6
6
6
6
6
lg/Kglg/Kg
uq/Kg
og/Kg
ug/Kq
rtg/K9t
lg/Kg
7
7
8IIII
3
2
3
NI-225 SOIL BORINGS
CONSTITUENT
PERCHLORATE
PERCHI,ORATE
PERCHLORATE
PERCHLORATE
PERCHI,oRATE
PERCHLORATE
PERCHLORATE
PERCHI,ORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHI,ORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
LOC DEPTH CONC.
B
B
B
B
B
At
At_
AL
A1
A1
AL
Al_
A1_
A1
A1
A2
A2
A2
A2
A2
A2
A2
A2
A2
A2
A3
A3
A3
A3
A3
A3
A3
A3
A3
A3
c
c
c
c
c
c
H
H
H
H
H
R
R
R
12
5
PQL
3.5
UNIT
mg/Kg
GROUP
6
10
L
1
L
1
L
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
3
4
4
4
4
4
4
4
4
4
4
5
5
5
5
551'
6
6
6
6
6
7
7
7
3.53.53.53.53.53.5
3.5
3.5
3.5
3.5
3.5
3.53.53.53.53.53.53.53.5
3.53.5
3.53.5
3.5
3.5
3.5
3.5
3.5
3.5
3.53.53.53.53.53.53.53.53.53.53.53.53.53.5
3.53.5
3r53.53.5
8
4D
6
2
4
L0I
2
4
6
1_0
2I
4
4
2
8
L2
2
t_6
4
18I
4D
l_0
t4
6
2
20
L6
4t2
6
18
l_0
L4It2I
L6
4
t_8
6
t_8
L0
2
L4
6.t9
7 .45
7.O2
1-4.9
4.87
5.08
7 .44
4.7L
1_5
23
24
69.9t2.8
37
462
6.6L
45
4 .44
6L.6
22
27.2
mg/Kq
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mq/Kq
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kq
mg/Kg
mq/Kg
mg/Kg
mg/Kg
mg/Kg
ng/Kg
mg/Kg
mg/Kg
mg/Kg
mg/Kg
ng/Kg
mg/Kg
mg/Rg
IfI.g/Kg
mg/Kg
ntg/Kg
mg/Kg
mq/Kg
^q/Kgmg/Kg
mg/Kg
mq/Kq
mg/Kg
mg/Kg
mg/Kg
mg/Kg
II,|.g/Kq
mg/Kg
mg/Kg
mg/Kq
14-225 SOIL BORINGS
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
PERCHLORATE
3.53.5
3.53.5
3.5
3.5
3.5
6
L0I
6
4
2
t_0
R
R
S
D
s
S
s
7.58
4.3
t7.L
mq/Kg 7mg/Kg 7mg/Kg Img/Kg Img/Kg Img/Kg Img/Kg I
M-225 SOIL BORINGS
CONSTITUENT
CHLOROFORU
CHLOROFORM
CHLOROFORI,T
CHLOROF'ORM
CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORI{
CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORIT{
CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORIT{
CHIOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROFORM
CHLOROF'ORII{
CHLOROFORIT{
CHI,OROTORM
CHLOROFORM
CHLOROFORM
CHLOROF'ORM
CHLOROFORM
CHLOROFORM
CHLOROFORU
CHLOROFORM
CHLOROFORII{
CHLOROFORM
CHLOROFORM
CHLOROFORM
LOC
B
B
B
B
B
At
A1
At
AL
At-
AL
At
AL
Al_
AL
A2
A2
A2
A2
A2
A2
A2
A2
A2
A2
A3
A3
A3
A3
A3
A3
A3
A3
A3
A3
c
c
c
c
c
c
H
H
H
H
H
R
R
R
4I
2
10
6
l_o
t_8
8
2
L2
4
L6t4
4D
6
20
L0
l-5
t-8
6
L4
2
4
L2
8
L5
20
L4
1_8
3
L0
4
PQL
6
6
6
6
6
6
6
620
620
6
620
6
6
5
620
6
6
7
6
6
6
6
6
7
6
6
6
6
6
6
6
6
6
6
7
6
6
5
6
6
6
6
6
6
6
6
6
32
32
DEPTH CONC UNIT GROUPlq/Kg 1ug/Kg 1uq/Kg Lttg/Kg Llq/Kq 1ug/Kg 2ug/Kq 2Dq/Kq 2lq/Kg 2lg/Kq 2\g/Kg 2ttg/Kg 2ug/Kg 2lg/Kg 2vg/Kg 2lg/Kg 3Dg/Kg 3lq/Kq 3ug/Kg 3lq/Kg 3\q/Kq 3ug/Kg 3Dg/Kg 3ug/Kq 3lg/Kq 3ug/Kg 4\q/Kg 4vg/Kg 4lg/Kg 4Dg/Kg 4vg/Kq 4uq/Kg 4ng/Kg 4Dg/Kg 4ug/Kq 4lrg/Kg 5\g/Kg sug/Kq srtg/Kg 5lq/Kq sttg/Kg 5ng/Kg 6vg/Kg 6Dg/Kq 6vg/Kg 6vq/Kg 6ug/Kq 7\g/Kq 7lrg/Kg 7
4
2
2
2
2
6
10
2
4I
L2
6
4D
8
2
4
10I
2
4
6
l_0I
2
4
YT-225 SOTL BORINGS
CHI,OROFORM
CHLOROFORI{
CHLOROFORI'{
CHI,OROFORM
CHLOROFORIT{
CHLOROT'ORM
CHLOROFORM
2
6
10I
6
4
2
l-o
R
R
S
s
s
S
S
6 ag/Kg 76 ug/Kg 76 ug/Kg I6 vq/Kg I6 \g/Kg I6 \g/Kg I6 Dq/Kg I
YT-225 SOIL BORINGS
CONSTITUENT
SODIW AZIDE
SODII'M AZIDE
SODIT'M AZIDE
SODIUM AZIDE
SODIUM AZIDE
SODIT'I{ AZIDE
SODIW AZIDE
SODIT'U AZIDE
SODII'M AZIDE
SODIT'M AZTDE
SODIUM AZTDE
SODII'M AZIDE
SODIUM AZIDE
SODIUI{ AZIDE
SODIT'M AZIDE
SODIT'M AZIDE
SODIW AZT.DE
SODIT,II{ AZIDE
SODIUM AZIDE
SODIT'U AZIDE
SODII'U AZIDE
SODII'U AZIDE
SODIT'I{ AZIDE
SODIUM AZTDE
SODItru AZIDE
SODIT'U AZIDE
SODIT'I'{ AZIDE
SODII'M AZIDE
SODII'M AZIDE
SODIUM AZIDE
SODIUM AZIDE
SODII l,l AZIDE
SODIT'U AZIDE
SODII'I{ AZIDE
SODIT'M AZIDE
SODTW AZIDE
SODTW AZIDE
SODIT'M AZIDE
SODIT'M AZIDE
SODIW AZIDE
SODIW AZIDE
SODIW AZIDE
SODIW AZIDE
SODIT'M AZIDE
SODIUM AZIDE
SODIUI'{ AZIDE
SODIUM AZIDE
SODIT'M AZTDE
SODIT'M AZIDE
LOC
B
B
B
B
B
A1
A1
AL
At
A1
A1
Al_
A1_
A1
A1
A2
A2
A2
A2
A2
A2
A2
A2
A2
A2
A3
A3
A3
A3
A3
A3
A3
A3
A3
A3
c
c
c
c
c
c
H
H
H
H
H
R
R
R
4
L8I
4D
l_0
t4
6
2
20
L6
4
L2
6
18
L0
L4
8
T2I
t6
4
t_8
6
l_8
L0
2
L4
78.
448
2L2
36.
LL2
164
83
66.
PQL
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
DEPTH CONC.UNIT GROUPmg/Kq Lmq/Kq Lmg/Kq 1mg/Kg Lmg/Kg Lmq/Kg 2ng/Kg 2mg/Kg 2mg/Kg 2mg/Kg 2mg/Kg 2mg/Kg 2mg/Kg 2mg/Kg 2mg/Kg 2mg/Kg 3mg/Kg 3mg/Kg 3mg/Kg 3mg/Kq 3mg/Kg 3mg/Kq 3mq/Kg 3mq/Kg 3mq/Kg 3mg/Kg 4mg/Kg 4mg/Kg 4mg/Kg 4mg/Kg 4mg/Kg 4ng/Kg 4mg/Kg 4mg/Kg 4mg/Kq 4mg/Kg smg/Kg 5mg/Kg smg/Kg smg/Kg 5mg/Kq smq/Kq 6mg/Kg 6mg/Kq 6mg/Kq 6mq/Kg 6mg/Kg 7mg/Kg 7mq/Kq 7
6
10
4
2
8
L2
2
16
I
4D
6
2
4
l_0I
2
4
6
l_0
2I
4
YI-225 SOIL BORINGS
SODIT'M
SODIT,It{
SODII,II{
SODTI'}T
soDrul,l
SODII'}!
SODIUM
AZTDE
AZTDE
AZIDE
AZTDE
AZIDE
AZIDE
AZIDE
6
10I
6
4
2
l_0
R
R
s
s
S
s
S
25
25
25
25
25
25
25
mg/Kg 7mq/Kg 7nq/Kg Ing/Kg Img/Kg Img/Kg Img/Kg I
NI-225 SOIL BORINGS
CONSTITUENT
t , t-, 1-TRTCHT.,OROETHANE
1, 1, I-TRTCHIOROETHANE
1, 1, I-TRICHIOROETHANE
1, 1, I-TRTCHT,OROETHANE
1, 1, I-TRTCHIOROETHANE
1, ]., 1-TRICHIOROETHANE
1, ]., I-TRICHIOROETHANE
1, 1, 1-TRICHI,OROETHANE
1, 1, 1-TRICHIPROETHANE
1, 1, I-TRTCHT,OROETHANE
1, 1, I-TRTCHT,OROETHANE
1, 1, I-TRICHT,OROETHANE
1, 1, I-TRTCHT,OROETHANE
1, 1, I-TRTCHTOROETHANE
1, l-, I-TRICHT,OROETHANE
1, 1, I-TRICHI,OROETHANE
1, 1, I-TRICHIOROETHANE
1, 1, I-TRTCHTOROETHANE
1, 1, I-TRTCHTOROETHANE
1, 1, I-TRTCHIOROETHANEt, 1, I-TRTCHIpROETHANE
1, t , I-TRICHTTROETHANE
1, L, 1-TRTCHTpROETHANE
1, ]-, I-TRICHIOROETHANE
1, 1, 1-TRTCHTpROETHANE
1, 1, I-TRTCHT,OROETHANE
1, 1, I-TRICHIOROETHANE
1, ]., I-TRICHI,OROETHANE
1, 1, I-TRTCHT,OROETHANE
1, 1, I-TRICHIOROETITAI'IE
1, t, I-TRTCHTOROETHANE
1, 1, I-TRICHIOROETHANE
1, 1, I-TRTCHTOROETIIANE
1, 1, I-TRTCHIOROETHANE
1, t , 1-TRICHTpROETHANE
1, 1, 1-TRTCHTpROETHANE
L, t, 1-TRTCHToRoETHANE
1, 1, I-TRICHIOROETHANE
1, 1, I--TRTCHLOROETHANE
1, 1, I-TRICHIPROETHANEt, 1, I-TRICHTOROETHANE
1, t, 1-TRTCHTpROETHANEt , 1, I-TRICHTOROETHANE
t , 1, I-TRTCHT,OROETHANE
1, 1, I-TRICHIOROETHANE
1, t , I-TRICHI0ROETHANE
1, 1, 1-TRTCHTpROETHANE
1, 1, t -TRTCHTTROETHANEt, 1, I-TRICHToROETHANE
roc
A1
A1
A1
Al_
A1
A1
A1
A1
A1
A1
A2
A2
A2
A2
A2
A2
A2
A2
A2
A2
A3
A3
A3
A3
A3
A3
A3
A3
A3
A3
B
B
B
B
B
c
c
c
c
c
c
H
H
H
H
H
R
R
R
coNc.
2L
L2
28
L4
20
25
4
28
27
L0
53
51
34
38
L2
8
10
9
4
24
10
20
2L
15
27
4
16
24
29
38
33
4
4
26
91
PQL
620
620
620
620
5
6
6
6
6
6
6
6
6
6
6
6
7
6
7
6
6
6
6
6
6
6
6
6
7
6
6
6
6
6
6
5'6
6
6
6
6
6
6
6
6
6
6
6
32
UNIT
ug/Kg
ug/K9lg/Kglg/Kg
rtg/Kg
vg/Kg
rtg/Kg
ug/Kg!g/Kq
ug/Kq
ug/Kg
uq/Kqlg/Kg
rtg/Kg
rtg/Kg
1rg/Kg
tlg/Kg
rtg/Kglg/Kq
rlg/Kg
ug/Kg\g/Kqlg/Kglq/Kg
rtg/Kg
Dg/Kq
vg/Kglg/Kg
vq/Kg
ug/Kg\g/Kg!g/Kglg/Kg
ug/Kg
vg/Kgt
1rg/Kg
ug/Kq
\g/K9t
rtg/Kg
ug/Kglg/Kgtrg/Kglg/Kg
ttg/Kg
vg/Kq
vg/Kg
ttg/Kg
rtg/Kg!g/Kg
GROUP
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
3
4
4
4
4
4
4
4
4
4
4
1
1
1
1
t
5
5
5
5
5
5
6
6
6
6
6
7
7
7
DEPTHI
6
4
2
4D
18
15
L4
L2
L0I
6
4
2
20
18
15
L4
L2
L0I
6
4
2
20
18
16
L4
L2
4D
10
280
I
10
7
4
7
3
5
4
3
10I
6
4
2
10I
6
4
2
I
6
4
2
l_0I
6
4
VI-225 SOIL BORINGS
,1
1
1
1
1
1
1
7
?IIIII
32
6
6
6
6
6
6
2
10I
6
4
2
10
R
R
s
s
s
s
s
1
1
1
1
1
t
t
, 1-TRTCHTOROETHANE
, I-TRTCHTpROETITANE
, L-TRICHIOROETITN{E
, 1-TRTCHTpROETEANE
, I-TRTCHT,OROETHANE
, I-TRTCHTOROETHANE
, I-TRICHT,OROETHANE
160
L9
9
2
60
20
L4
ug/Kg
ug/Kg\g/Kg
lq/Kg
ug/Kg
ug/Kg\9/Kg
Y1225 SOIL BORINGS
CONSTITUENT
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
LOC
B
B
B
B
B
At
At_
At
A1
A1
AL
A1
AL
AL
AL
A2
A2
A2
A2
A2
A2
A2
A2
A2
A2
A3
A3
A3
A3
A3
A3
A3
A3
A3
A3
c
c
c
c
c
c
H
H
H
H
H
R
R
R
coNc.
31
32
52 00
2500
47 00
3 000
280
26
28
t_8
69
PQL
L30
L20
tL0
110
130
L20
r_2000
L20
l_2 000
L20
l_2000
r.00
L20
L20
12 000
L20
L20
L30
L10
130
110
L20
L20
L20
L20
130
r.L0
L20
LL0
L20
110
L20
L20
L20
130
100t20t20
L20
L20
L20
L20
130t20
l_3 0
L20
630
110
630
DEPTH UNIT GROUPvg/Kq l-lg/Kq L\q/Kg L\g/Kg 1lq/Kq 1lg/Kg 2ug/Kg 2lg/Kg 2rtg/Kg 2lg/Kg 2rtg/Kg 2ug/Kg 2lg/Kg 2tg/Kg 2\g/Kg 2lg/Kg 3uq/Kq 3vg/Kg 3\q/Kg 3lg/Kq 3lg/Kg 3lrg/Kg 3ug/Kg 3vg/Kg 3Dq/Kg 3lg/Kg 4rtg/Kg 4\g/Kq 4ug/Kq 4lg/Kq 4og/Kq 4rlg/Kg 4ug/Kg 4tg/Kg 4vg/Kg 4uq/Kg 5\q/Kg sug/Kg 5\g/Kg srtg/Kg 5rtg/Kg 5lg/Kg 6lg/Kg 6rtg/Kg 6uq/Kg 6Dq/Kg 6\g/Kg 7ng/Kg 7lq/Kg 7
6
10
4
2
8
L2
2
L6
4
18
8
4D
10
L4
6
2
20
16
4
L2
6
18
L0
l_4
8
L2I
16
4
18
6
20
10
2
L4
8
4D
6
2
4
l_0I
2
4
6
l_0
2
8
4
56
Y1225 SOTL BORTNGS
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
2-BUTANONE
6
10I
6
4
2
l_o
R
R
s
s
S
S
S 32
L20
130
110
110
110
1t_ot20
lg/Kg 7lg/Kg 7ltg/Kg 8uq/Kg IDg/Kg Irtg/Kg I\g/Kq I
YT-225 SOIL BORINGS
CONSTITUENT
PYRTDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDTNE
PYRIDINE
PYRTDINE
PYRTDINE
PYRIDINE
PYRIDINE
PYRIDTNE
PYRIDINE
PYRIDTNE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRTDTNE
PYRIDINE
PYRIDINE
PYRIDINE
PYRTDTNE
PYRIDINE
PYRIDINE
PYRTDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRTDTNE
LOC
B
B
B
B
B
A].D
AL
A1
AL
A1
A1
At-
AL
A1
A1
A2
A2
A2
A2
A2
A2
A2
A2
A2
A2
A3
A3
A3
A3
A3
A3
A3
A3
A3
c
c
c
c
c
c
H
H
H
H
H
H
R
R
R
27 000
26000
2
2800
DEPTH CONC.
3 t-000
t0
2
4
t4I
18t8t2
6
2
20
L6
4
L2
6
l-8
10
L4It2I
4
18
6
20
L0
2
L4
UNIT GROUPlg/Kq 1ng/Kg l-vg/Kq l-og/Kg Llg/Kg 1rtg/Kg 2Dg/Kg 2vg/Kg 2ug/Kg 2vg/Kg 2ug/Rg 2ug/Kg 2uq/Kg 2Dq/Kg 2lg/Kq 2ug/Kg 3lq/Kg 3vq/Kg 3rtg/Kg 3lg/Kg 3lrg/Kg 3lg/Kg 3lg/Kg 3rtg/Kg 3ug/Kg 3vg/Kg 4ug/Kg 4vg/Kg 4Dg/Kg 4ng/Kq 4vq/Kg 4lg/Kg 4lg/Kg 4rtg/Kg 4vg/Kg 5lg/Rg 5lq/Kq slg/Kq 5lq/Kg 5ug/Kq 5vg/Kg 6ug/Kg 6uq/Kg 6vq/Kq 6lrg/Kg 6lg/Kg 61rg/Kg 7ng/Kg 7vq/Kg 7
6I
2
10
4
4
PQL
6
6
6
6
6
5
6
620
620
6
620
6
6
6
620
6
6
7
6
7
6
6
6
6
6
7
6
6
6
6
6
6
6
6
5
6
6
6
6
6
6
6
6
6
6
6
32
6
6
I
4D
6
2
4
10
8
2
6
2
4
L0
4
6
8
YI-225 SOIL BORTNGS
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
PYRIDINE
32
6
6
6
6
6
2
6
I
4
2
10
R
s
s
S
s
S
lq/Kq 7\g/Kq Iltg/Kg Ilq/Kq IDg/Kg I\g/Kg I
M-225 SOIL BORTNGS
CONSTITUENT
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONB
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
LOC
B
B
B
B
B
AL
A1
A1
AL
AL
AL
A1
A1
At
_At
A2
A2
A2
A2
A2
A2
A2
A2
A2
A2
A3
A3
A3
A3
A3
A3
A3
A3
A3
_L3
H
c
c
c
c
c
c
H
H
H
H
R
R
R
DEPTH
6
10
4
2I
L2
4
L6
4
18I
2
L0
L4
6
2
20
t6
4
T2
6
l_8t0
L4I
L2
2
L6
4
L8
6
20
t_0t4II
8
10
4
4D
2
6
6
4
2
t_0I
2
4
coNc.
t5
13
59
73 00
4L
5800
L40
6200
15000
4L
L20
2800
18
20
]..20
39
35
39
72
27
73
80
L8
38
23
70
40
25
76
17
25
37
4L
45
19
44
L8
53
4L
4L
46
46
58
r_50
220
PQT,
130
L20
LL0
1L0
L30
L20
t_oo
L20
l_2000
L20
t-2000
12000
t20
].20
r.2 000
L20
L20
130
r.10
130
LL0
L20
L20
L20
L20
130
L20
L20
Lt0
L20
1L0
L20
t20
L30
l_l_0
t20
l_00
]-20t20
L20t20t20
130
L20
130
L20
L10
630
630
UNIT GROUPug/Rq l-uq/Kg Llg/Kg 1ug/Kg 1-Dg/Kg 1oq/Kg 2lq/Kg 2ug/Kg 2vg/Kg 2rtg/Kg 2vg/Kg 2lg/Kq 2lg/Kg 2ttg/Kg 2lq/Kg 2lq/Kq 3lg/Kq 3ug/Kg 3ug/Kg 3lg/Kg 3lg/Kq 3trg/Kg 3rtg/Kg 3rtg/Kg 3ttg/Kg 3lg/Kq 4lg/Kq 4vq/Kq 4lq/Kg 4ng/Kg 4rtg/Kg 4uq/Kg 4uq/Kq 4ttg/Kg 4rtg/Kg 4rtg/Kg slg/Kg 5lg/Kg slq/Kq sug/Kq svg/Kg 5lg/Kg 5\g/Kg 6ttg/Kg 6trg/Kg 6vg/Kg 6ug/Kg 7ug/Kq 7ttg/Kg 7
YT-225 SOIL BORINGS
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
ACETONE
6
l_0I
6
4
2
10
R
R
s
s
s
S
S
43
53
L4
13
51
33
23
L20
130
110
110
Lto
Lt_0
L20
vg/Kg 7ug/Kg 7vg/Kg Itlg/Kg 8ug/Kg 8Dg/Kq 8vg/Kq 8
M-225 SOIL BORINGS
CONSTITUENT
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
TOTAL XYLENES
LOC DEPTH CONC. PQL UNIT GROUP
B
B
B
B
B
A1
Al_
AL
AL
AL
A1
Al_
Al_
At-
AL
A2
A2
A2
A2
A2
A2
A2
A2
A2
A2
A3
A3
A3
A3
A3
A3
A3
A3
A3
A3
c
c
c
c
c
c
H
H
H
H
H
R
R
R
6
6
6
6
6
6
620
6
620
6
L0
4
2I
L2
2
15
4
18
8
4D
10
L4
6
2
20
l_6
4
L2
6
t-8
1o
L4
8
t2
8
L6
4
18
6
20
l_0
2
L4
2
2
4
3
3
2
L50
30
1
ttg/Kg Log/Kg 1lg/Kg 1uq/Kq 1lg/Kq l-119/Kg 2Dg/Kg 2uq/Kg 2ug/Kg 2vg/Kq 2ug/Kg 2lg/Kg 2vg/Kq 2vq/Kg 2vg/Kq 2lg/Kg 3rtg/Kg 3ug/Kg 3lg/Kg 3Dq/Kg 3rlg/Kg 3Dq/Kg 3ug/Kg 3rtg/Kg 3lq/Kg 3ug/Kg 4rtg/Kg 4vg/Kg 4lq/Kg 4Dg/Kg 4lg/Kg 4rtg/Kg 4ug/Kg 4ng/Kq 4ug/Kg 4uq/Kg suq/Kg sDg/Kg 5ug/Kg 5\g/Kg srtg/Kg 5Dq/Kq 6\g/Kg 6ug/Kg 6iq/Kg 6lg/Kg 6vq/Kq 7ig/Kq 7uq/Kq 7
86
2
2
62
62
6
0
5
6
6
o
6
6
7
6
7
6
6
6
6
6
7
6
6
6
6
6
6
6
6
6
5
6
6
6
6
6
6
5
6
6
6
2
6
3
2
t
2
2
2
1
1
5
2
l_
2
2
2
1
2
2
3
2
4
3
4
3
3
3
4
4
4
t-
5
1
5
I
4D
6
2
4
l_0I
2
4
6
l_0
2
8
4 32
YI-225 SOTL BORINGS
TOTAL
TOTAL
TOTAL
TOTAL
TOTAL
TOTAL
TOTAL
XYLENES
XYLENES
XYLENES
XYLENES
XYLENES
XYLENES
XYLENES
4
4
2
t
13
4
3
6
Lo
8
6
4
2
L0
R
R
s
s
s
S
S
6 ug/Kg 76 Dg/Kq 76 ug/Kg I6 Dq/Kg 86 ug/Kq I6 ug/Kg I6 ug/Kg I
YI-225 SOIL BORINGS
CONSTITUENT
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE,
LOC DEPTH CONC. PQL UNIT GROUP
B
B
B
B
B
AL
AL
At
A1
A1
Al_
A1
Al-
A1
At
A2
A2
A2
A2
A2
A2
A2
A2
A2
A2
A3
A3
A3
A3
A3
A3
A3
A3
A3
A3
c
c
c
c
c
c
H
H
H
H
H
R
R
R
r_6
4
L8I
4D
l_0
L4
6
2
20
L5
4l2
6
l_8
Lo
L4
8
L2I
L6
4
18
6
20
t_0
2
L4
74
L
67
95
L
1
95
t_
1
l_
l_
l_
l_
t_
300
5
6
L0
4
2I
t2
2
6
6
6
6
6
6
620
6
620
6
620
5
6
6
620
6
6
7
6
7
6
6
6
6
6
7
6
6
6
6
6
6
6
6
6
5
6
6
6
6
6
6
6
6
6
6
32
6
32
vg/Kq 1\q/Kg l-lq/Kg l-vg/Kq l-lq/Kg 1ug/Kg 2lrg/Kg 2ug/Kg 2lg/Kg 2ug/Kg 2uq/Kg 2lg/Kg 2ug/Kg 2vg/Kg 2ug/Kg 2lg/Kq 3vq/Kg 3uq/Kg 3vg/Kg 3rlg/Kg 3lg/Kg 3ug/Kg 3vg/Kq 3ug/Kq 3vg/Kq 3ug/Kg 4ug/Kg 4ug/Kg 4rlg/Kg 4rtg/Kg 4ug/Kg 4\q/Kg 4lg/Kg 4ng/Kg 4119/Kg 4Dq/Kg 5ug/Kg sug/Kg 5Dq/Kg 5ug/Kg 5vg/Kq 5ug/Kg 6Dq/Kg 6vg/Kg 6lq/Kg 6vg/Kg 6lg/Kg 7\tg/Kg 7vq/Kg 7
2
2
1
2
L
2
l_
t_
1
1_
1
L
l_
L
1_
1
L
L
L
L
L
L
l_
1
2
2
L
t_0
1
4
I
4D
6
2
4
L0
8
2
4
6
L0
2
8
4
yt-225 SOrL BORTNGS
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
TOLUENE
6
10
8
6
4
2
L0
R
R
S
S
s
s
S
t
1
t
9
l_
L
6 ug/Kg 76 lg/Kg 76 lg/Kg I6 ug/Kg I6 lg/Rq I6 lq/Kg I6 Dq/Kq I
YT-225 SOTL BORINGS
CONSTITUENT
TRTCHI,OROETHENE
TRICHI,oROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHI,OROETHENE
TRICHI,OROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRTCHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRTCHLOROETHENE
TRICHI,OROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRTCHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRTCHLOROETHENE
TRICHLOROETHENE
TRTCHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROETHENE
TRTCHLOROETHENE
TRICHLOROETHENE
TRTCHLOROETHENE
LOC DEPTH CONC. PQL UNIT GROUP
B
B
B
B
B
AL
AL
AL
A1
AL
Al_
At_
A1
At_
Al_
A2
A2
A2
A2
A2
A2
A2
A2
A2
A2
A3
A3
A3
A3
A3
A3
A3
A3
A3
A3
c
c
c
c
c
c
H
H
H
H
H
R
R
R
t-0
6
l_0
6
6
6
6
6
6
620
6
620
Dg/Kg 1ug/Kg Lug/Kq Lug/Kq 1vg/Kq 1ug/Kg 2ug/Kg 2ttg/Kg 2ug/Kg 2Dg/Kg 2vg/Kg 2uq/Kg 2vg/Kg 2Dg/Kg 2og/Kg 2lrg/Kg 3ug/Kg 3lq/Kg 3vg/Kq 3uq/Kg 3vg/Kg 3\g/Kq 3vg/Kg 3lg/Kg 3lg/Kq 3vg/Kg 4vg/Kg 4ug/Kq 4lg/Kg 4lq/Kg 4Dq/Kg 4vg/Kg 4uq/Kg 4\g/Kg 4lg/Kq 4Ltg/Kg 5vg/Kg 5og/Kg srtg/Kg 5ttg/Rg 5ttg/Kg 5vg/Kg 6nq/Kg 6rtg/Kg 6lg/Kq 6lg/Kg 6ug/Kg 7rtg/Kg 7ug/Kg 7
4
2I
L2
2
L6
4
t_8I
4D
L0l4
6
2
20t6
4t2
6
1_8
10
L4
8
t2I
t_6
4
18
6
20
L0
2
L4
6
620
5
6
6
620
6
6
7
6
7
6
6
6
6
6
7
6
6
6
6
6
6
6
6
6
5
6
6
6
6
6
6
6
6
6
6
32
6
32
I
4D
6
2
4
l_0I
2
4
6t0
2I
4
13
6
10
YT-225 SOIL BORINGS
TRTCHI,OROETHENE
TRICHI,oROETHENE
TRICHIPROETHENE
TRTCHI.oROETHBNE
TRICHI,OROETHENE
TRTCHI,OROETHENE
TRICHI,OROETHENE
6
10
8
6
4
2
10
R
R
s
s
S
S
s
48
t-
6 vg/Kg 76 ng/Kg 76 ug/Kg I6 vg/Kq I6 ug/Kg 86 ttg/Kg I6 lg/Kg 8
NI-225 SOIL BORINGS
HMX
HMX
HMX
HMX
HMX
HMX
HMX
HMX
HMX
HMX
HMX
HMX
HMX
HMX
HMX
Hl,lX
HMX
HMX
HMX
HMX
HMX
HMX
HMX
HMX
HMX
HMX
HI,IX
HMX
Hl,lX
Ht',lX
HMX
HMX
HMX
HMX
HI'{X
HMX
HMX
HMX
HMX
HMX
HMX
HMX
HMX
HMX
HMX
HMX
HMX
HMX
HMX
HMX
B
B
B
B
B
AL
Al_
A1_
A1
AL
AL
AL
A1
Al_
A1
A2
A2
A2
A2
A2
A2
A2
A2
A2
A2
A3
A3
A3
A3
A3
A3
A3
A3
A3
A3
c
c
c
c
c
c
H
H
H
H
H
R
R
R
R
I
6
4
2
l_0I
6
4
2
4D
18
16
L4
t2
l_0I
6
4
2
20
l-8
1-5
L4t2
l_0I
6
4
2
l_8
L8
16
L4
L2
10I
6
4
2
L ng/Kg LL mg/Kq LL ng/Kg 1L ng/Rg 1-L mg/Kg l-L mg/Kg 2L mg/Kg 2L mg/Kg 2l- nq/Kg 2L mg/Kg 2L mq/Kg 21 mq/Kg 2L mg/Kg 2L mg/Kg 2l- ng/Kq 2l- ng/Kg 3L mg/Kq 3l- mg/Kg 3L mq/Kg 3L mg/Kg 31 mg/Kg 3L mg/Kg 31 mg/Kq 3L mq/Kg 3l- mg/Kq 31 nq/Kg 4L mq/Kg 41- mg/Kg 4L ng/Kg 41 ng/Kg 4L ng/Kg 4L mq/Kg 4l- mg/Kg 41 mg/Kg 41 mg/Kg 4l- mg/Kg 5L nq/Kg 5L mg/Kg 51 mq/Kg 51 ng/Kg sL ng/Kg sL ng/Kg 6L ng/Kg 61 mg/Kg 6l- mg/Kg 61 mq/Kg 6l- ng/Rg 7L mg/Rg 7L mg/Kg 71 ng/Kg 7
4D
L0
L.2L
2.42
2.54
49.9
5.75
3.87
2.556.t9
6.57
9.68
I
6
4
2
10I
6
4
2 2.21
Iq-225 SOIL BORINGS
HMX
HMX
HMX
HMX
HMX
HMX
10I
6
4
2
10
R
S
S
s
s
S
4.7
99.7
L mg/Kg 7L mg/Kg 8L mg/Kg 8L mg/Kg 81 mg/Kg 8L mq/Kg I
1,4-225 SOIL BORINGS
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NTTRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NTTRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
mg/Kg 1mg/Kg 1mq/Kg l-mg/Kg Lmg/Kq l-mg/Kg 2mg/Kg 2mq/Kg 2mg/Kg 2mg/Kg 2mq/Kg 2mg/Kg 2mg/Kg 2ng/Kq 2mg/Kg 2mq/Kq 3mg/Kg 3mq/Kg 3mq/Kg 3mg/Kq 3mg/Kg 3mq/Kg 3mg/Kg 3mg/Kq 3mq/Kg 3ng/Kg 4ng/Kg 4ng/Kg 4mq/Kg 4nq/Kg 4mg/Kg 4mg/Kg 4mg/Kg 4ng/Kg 4mg/Kg 4nq/Kg 5ng/Kg 5mg/Kq 5mg/Rg snq/Kg 5ng/Kg 5mg/Kg 6ng/Kg 6mg/Kg 6mg/Kg 6mq/Kg 6nq/Kg 7nq/Kq 7ng/Kg 7ng/Kg 7
B6BL0B4B2B8A1 L2
Al_ 2
AL r-6At4AL LSAL8A1 4DA1 10A]. L4A1 6A22
A2 20A2 16A24A2 12A26A2 t_8
A2 10A2 t4
A,28A3 T2A38
A3 r-6434
A3 18A36
A3 20
A3 L0A32A3 L4c8c4Dc6c2c4c t0H8H2H4H6H10R2R8R4R6
0.84
0.34
0.43
o.7 4
0.34
L.47
o.29
0.3r_
0.48
L. 61
L.25
o .49
o.42
1. 35
2.88
L.672.L
2.26t.L7
L.L7
2.05
0.78
L. 35
0.2
o.2
0.2
o.2o.2
o.2
o.2
o.2
o.2
0.2
o.2
o.2
o.2
o.2
o.2
o.2
o.2
o.2o.2
o.2
o.2
o.2
o.2
o.2
o.2
o.2
o.2
o.2
o.2
o.2
o.2
0.2
o.2
o.2
o.2
o.2
o.2
o.2
o.2
o.2
o.2
o.2
o.2
o.2
o.2
o.2
o.2
o.2
o.2
o.2
2
5
2
5
2
7 .69
3.3r.
5.37
.05
.54
.86
6.L
.03
.65
5. t-
6.73
LL. 6
8.9
5. 05
1l_.5
4.07
6.54
5.91
6.L9
7 .52
L.57
7.O2
2.92
o.7L4.7t
YI-225 SOIL BORTNGS
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
NITRATE-N
o.2
o.2
o.2
o.2
o.2
o.2
10I
6
4
2t0
R
S
S
s
s
s
3.3
L.46
L.67
L2.2
7.23
3 .66
ng/Kg 7mg/Kg Img/Kg Ing/Kg 8mg/Kg Img/Kq I
|n
F2FI
E(,
ErH.<
g)
>z
o)l
;oHF
CEFz.lrlO
o
CJ
1=BACKGH0UND$ Concentnation
50000
40000
30000
20000
1 0000
4
PYRIDINE
V1225 SOIL BORINGS
STara"
Z=AL 3=AZ 4=A3 5=C 5=H 7=R 8=S
Svmbols
o Outlier
Upper Adjacent Value
2sth Percenti.le
Median75th Percentile
Lower Adjacent, Value
Adjacent values are three-halves the interqrrartile range,
back to where there is data.
0
1 8
rol1ed
1=BACKGH0UND
Q Concentnatlon
50
40o,Y.
C,))
;o
F
CEF
lJlOz.oCJ
30
20
10
_-__l o
0
I 2
CHLOHOFORM
tvl-22= SOIL BORINGS
STaTa"
2=41 3=A? 4=A3 5=C 6=H 7=R g=S
Synbols
o Outlier
Upper Adjacent Value
25th Percentile
Median75th Percentile
Lower Adjacent Value
{
Adjacent values are three-harves the interquartire range,back to where there is data.rolled
1 =BACKGH0UNDfr Concentnatlon
o
q,
:z
o,
=;o
F
CEF2
LIJ
CJzo(J
250
200
150
100
50
0
+o
o
2 4T,1,7 THICHLOROETF'ANE
1,1225 SOIL BORINGS
5r=-E-;
2--Al 3=A2 4=A3 5=C 6=H 7=R 8=S
-----
-=
Svmbols
o
E
Outlier
o
I
Upper Adjacent Value
25th Percentile
Median75th Percentile
Lower Adjacent Value
Adjacent, values are three-halves the interquartile range,back to where there is data.roIled
1=BACKGH0UND
S Concentnation
5000
5000
Cf):<
o)
z.
LJHF
ccFz.
Lu
CJzoO
4000
3000
2000
1 000
0 o
I 2 4 6 I
2-BUTANONE
V1_225 SOIL BORINGS
-=T=:
2=Al 3--A2 4=A3 5=C 6=H 7=R 8=S
Svmbols
o Outlier
Upper Adjacent Value
25th Percentile
Median75th Percentile
Lower Adjacent Value
Adjacent, values are three-halves the interquartile range,back to where there is data.rolled,
1=BACKGFCUND
S Concentnation
300
250
o,
>Z
cr))
;o
CEFzl!L)z.o
CJ
200
150
100
50
0
2 3
TOTAL XYLENE
VI22= SOIL BORINGS
STaTa"
2=A! 3=AZ 4=A3 5=C 6=H 7=R 8=S
Svnbols
o Outlier
Upper Adjacent Value
E
25th Percent,ile
Median75th Percentile
Lower Adjacent Value
Adjacent, values are three-halves tlre interquartile range, rolledback to where there is data.
1=BACKGH0UNDfi Concentnation
100
80
50
g,
><
o))
;O
F
CEFz
lJ-lO
o(J
40
20
Lt'
0
2
TH
4ICHLOETHENE
6
tvt225 SOIL B0RINGS
STaTa-
?--AL 3=A2 4=A3 5=C 6=H 7=R 8=S
Srnnbols
o Outlier
Upper Adjacent Value
25th Percentile
Median75th Percentile
Lower Adjacent, Value
Adjacent values are three-halves the interquartile range, ro11edback to where there is data.
IT
c,)Y,
olE
ioHF
crF2
l!
CJzoCJ
t=BACKGH0UND
S ConcentPation
1 5000
5000
4000
3000
2000
1000
0
-
+
2 4
ACETONE
V1225 SOIL BORINGS
STaTa-
Z=AL 3=42 4=A3 5=C 6=H 7=R 8=S
Svmbols
o Outlier
Upper Adjacent Value
25th Percentile
Medi.an75th Percentile
Lower Adjacent Value
Adjacent values are three-halves the interquartile range,back to where there is data.
L 86
rol1ed
1=BACK.GflCUiID
Q Concentnation
500
o
400
o,Y.
q,)
tE
ioHF
CEF7
IJJ
CJzo
CJ
300
200
100
50
0
I 3
PERCHLOFATE
14225 SOIL BORINGS
STara"
z=AL 3=A2 4=A3 5=C 6=H 7=R 8=S
Svmbols
o Outli,er
Upper Adjacent Value
25th Percentile
Median75th Percentile
Lower Adjacent Value
Adjacent values are three-halves the interguartj.le range, rolled
back to where there is data.
o)
cJ)
;oH
F
CEF7
t-rJ(Jz,oCJ
1=BACKGH0UND$ Concentnation
o
o ---
5
TOLUENE
V122= SOIL BORINGS
ffiF
2=Al 3=A2 4=A3 5=C 6=H 7=R 8=S
Svmbols
o Outlier
Upper Adjacent Value
25th Percentile
Median75th Percenti.le
Lower Adjacent, Value
Adjacent, values are three-halves the interquartile range, rolledback to where there is data.
125
100
75
50
25
0
1
1=BACKBR0UN0$ Concentnation
500
o
400
g)
>Z
c,,
zo
H.F
CEFZo
C-)
300
200
100
0
I
SODIUM AZIDE
I/_225 SOIL BOFINGS
sTara"
2=Al. 3=42 4=A3 5=C 6=H 7=R 8=S
Svmbols
o Outlier
Upper Adjacent Value
2sth Percenti.le
Median75th Percentile
Lower Adjacent, Value
Adjacent, varues are three-halves the interquartile range,back t,o where there is data.rolled
1=BACKGPOUND
S Concentnatton
ol
>Z
c,))
io
F
CEt-zlJlo
oL)
50
40
30
20
10
Svmbols
o-:=-.,
0
METHYLENE CHLOFIDE
P1225 SOIL BORINGS
STara*
?=AL 3=AZ 4=A3 5=C 6=H 7=R 8=S
?
o Outlier
Upper Adjacent Value
25th Percent,ile
Median75th Percentile
Lower Adjacent Value
Adjacent values are three-halves the interquartile rangie, rolledback to where there is data.
TELEPHONE CALL RECORD
3014-8Y91-n031
i"tERat.ct OA'E O" CALL
'' coMPAr{Y
EPA
t?iEg?'' 'E D. C.
cor{fac?ED ?ELEFHOI'E
Susanne Griffin 202) 382-6392
REraair(t ll"E,at, a"c
I asked Susanne Griffin lf, there uas a loaxitDum concentration 1evel for sodlulD azide in soil
esrablished by rhe EPA. Ms. Griffin accessed the Intigrated Risk Infomation System (IRIS),
a corDputer-housed, electronically coroouni.cated catalog, for the lnforrnatlon. (This system
is a source of the latest information about Agency health assessruents and regulatory deci.sions
for specific chernicals).
The IRIS inforuation for the MCL in soil for sodi.um azLde is 320 ppto.
I asked if rhis leveL is equivalent to rhe action levels fouod in Appendlx A of the
ective Action Rules FR55 July 27, 1990. She stated that this would be the sznDe as
an agtlon leveL in Appendix A; in fact the appeodix A actlon 1eve1s were taken from IRIS.
rEixa
tr
trtr
tr
tr
collnnrtNo ouorE To FoLLor
IAXA'LE
corPEtt?tvE ttD3
stl{oLE on soLE souicE
O'}IER THAI' LOU BIOOER
OELIVgRV
t'.tt vta
3t oilatu RE
ct?Y
Washington
TI'LE
Risk Assessnent
FORM tC NO.9t
LI
II?LE El1y'ivutl
coRREcTIVE ACTIoN; PRoPosED nuis
APPENDIX A
EXAUPLES OF CONCENTRATIONS I.TEETING CRITERIA FOR ACTION LEVELS
FR/VOL. 55, NO. l4s/FRIDAY, Jt LY 27, 1990/30865
CONSTITUENT
Acetone
Pyridine
2-Butanone
Toluene
Xy1ene
Methylene Chloride
L, L, l-Trichloroethane
Sodium Azide
SOIL ACIION LEVEL (ppm)
8x1o3
8x1Or
4x1o3
2x1o4
2x1o5
9x10r
"1 x Lo3
320
TtE 6x l,J'
1t 1"wl