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HomeMy WebLinkAboutDRC-2024-005862June 6, 2024 VIA EXPRESS DELIVERY Mr. Doug Hansen Director Division of Waste Management and Radiation Control Utah Department of Environmental Quality 195 North 1950 West Salt Lake City, UT 84116 Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 www .e nero vfue ls.c o111 Div of Waste Management and Radiation Control JUN 1 0 2024 Re: Response to Request for Infonnation Ahead of Implementing Phase 2 of the Rare Earth Circuit, Radioactive Materials License Number UT 19004 79 Dear Mr. Hansen: Pursuant to the Division of Waste Management and Radiation Control's ("DWMRC's") letter dated April 25, 2024, Energy Fuels Resources (USA) Inc. ("EFRI") is providing responses to the request for infonnation. For ease of review, this letter provides the DWMRC comments verbatim, in italics, below, followed by EFRI's response. One copy of the enclosed Attachments is unredacted and complete for internal DWMRC review and use (see Attachments 4 through 6). One copy has been redacted in accordance with Utah Code 63G-2-101 et seq. as noted below (see Attachments I through 3). EFRJ is requesting that certain information enclosed with this letter be withheld from public disclosure because it is considered confidential business information ("CBI") pursuant to the provisions of the Utah Government Records Access and Management Act ("GRAMA"), Utah Code 630-2-101 et seq. The information sought to be withheld is that information in Attachments 1 through 3 that has been redacted or "blacked out" on each page of the redacted transmittals. The redacted information is also indicated by an electronic marking "Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below." All redactions were based on CBI/Proprietary Information. Pursuant to Section 63G-2-309(l)(a)(i) of GRAMA, EFRI hereby designates the redacted infonnation identified above as CBI. The documents and information qualify as CBI because they are not publicly available, and disclosure of the information therein likely would cause substantial harm to EFRI's competitive position. The documents and information have been provided for the exclusive use of the DWMRC on the express understanding that the information therein will be treated as confidential. Accordingly, the redacted information should be treated as confidential by DWMRC. Pursuant to Section 630-2-305 of GRAMA, the DWMRC should maintain the enclosed documents and information as protected and confidential, and exempt them from public records or disclosure laws, including but not limited to any subsequent requests under GRAMA or under the Freedom of Information Act ("FOIA"). If a request is made for public review of the documents or information, DWMRC must DRC-2024-005862 Letter to Doug Hansen June 6, 2024 Page 2 notify EFRI and provide the company with a reasonable time in which to object to their disclosure or seek an injunction preventing disclosure . Pursuant to Section 63G-2-107 of GRAMA, Energy Fuels also invokes relevant U .S . Nuclear Regulatory Commission regulations and guidance that protect the redactions, including but not limited to the withholding of proprietary, personally identifiable and security-related information under 10 CFR 2.390. DWMRC Comment Number 1: 1. SOPs Related to the Uranium Bearing Rare Earth Procedures License condition 9.6 requires EFRI to submit up-to-date copies of all operational and non-operational Standard Operating Procedures (SOP) to the Director of the Division (Director) by December 31 of each year. EFRI submits a list ofSOPs annually, most recently on December 19, 2022 (DRC-2022 -024175) and on December 14, 2023 (DRC-2023-078612). However, in both submissions, the SOPs included in "Book 15 -Uranium B earing Rare Earth Procedures " have been omitted with a brief statement that the SOPs are proprietary and contain confidential business information (CBI). The Division is not in receipt of a valid CBI claim relating to these SOPs. Under GRAMA , Utah Code Section 63G-2-309(1)(a)(i), a person w ho wants to claim that a record provided to the Division is protected from disclosure to a member of the public because it is CBI shall provide with the record i) a written claim of business confidentiality; and ii) a concise statement of reasons supporting the claim. Utah Code Section 63G-2-305(1) (trade secrets) and (2) (commercial information) describes the standards and requirements that apply to the kinds of information that may be subject to a CBI claim. A request for CBI treatment mus t be specific as to the rationale for the CBI claim and which records, or portions of records, are covered by th e CBI claim. Please also refer to Utah Code§ 63G-2-309(l)(a)(i). Without this information, the Division is unable to determine whether the CBI claim is valid. As such, the Division is requesting EFRI submit all SOPs contained in Book 15 and any other SOPs related to rare earth processing, along w ith a valid claim for treatment as CBI, if appropriate, as outlined in the preceding paragraphs. The Division recommends that EFRI submits both a complete and redacted version of each SOP. When performing redactions, please ensure that it is clear what has been redacted and why. To better protect any potential CBI, please submit the SOPs and CBI claim as hard copies through the mail and not electronically through dw111rcsub111it @ utah.gov. EFRI Response: As requested, the SOPs for rare earth bearing uranium , ("RE U") ore processing are included in Attachments I (redacted) and 4 (unredacted). EFRJ hereby claims for treatment of the redacted information contained in Attachment I as CBI as set out abov e in thi s letter. DWMRC Comment Numb er 2 : 2. Documentation Supporting Evaluations Conducted for the 2022 Annual SERP Report License condition 9.4 outlines the procedures EFRI must follow when evaluating whether i) a change to the facility, ii) a change to procedures , or iii) conducting an experiment would require a license amendment. Part B of condition 9.4 outlines the criterium a potential change must meet to not require a license amendment. A Safety and Environmental Review Panel (SERP), therefore, evaluates each potential change Letter to Doug Hansen June 6, 2024 Page3 against the criteria set forth in Part B to determine if the change requires a license amendment. Actions taken by the SERP must follow the most up-to-date version of SOP "PBL-1-SERP Procedure" and are required to be reported to the Director by March 31 of the following calendar year per license condition 9.4 part D. EFRI has annually submitted a report summarizing actions taken by the SERP, most recently on March 31, 2022 (DRC-2022-005502), March 30, 2023 (DRC-2023-002850), and March 26, 2024 (DRC-2024- 005046). Section 4.0 of SOP PBL-1, "SERP Procedure", requires the SERP to document its review of whether a potential change meets the criteria described in license condition 9.4 part B: Section 4. 0 SERP Review Procedure In their documented {emphasis added] review of whether a potential change, test, or experiment (hereinafter called "the change'') is allowed under the License or P BLC, without a License amendment, the SERP shall consider the following: (]) Current License Requirements: ... (2) Impacts on regulations: ... (3) Environmental Assessment: ... The documentation associated with the SERP review is typically not submitted as part of the annual summary of SERP actions. The Division requests that EFRJ submit all documentation supporting both decisions summarized in the 2022 Safety and Environmental Review Panel (SERP) Annual Report dated March 30, 2023 (DRC-2023-002850). Jf EFRI believes that this documentation contains CBI, please submit a claim/or treatment as CBI as outlined above, and the Division will assess this claim upon receipt. EFRI Response: As noted above, EFRI completed two SERP analyses in 2022. The resulting SERP Reports and associated documentation contain CBI as noted above and both redacted and unredacted copies have been provided. The redacted versions are included in Attachments 2 and 3 and the unredacted versions are included in Attachments 5 and 6. EFRI hereby claims for treatment of the redacted information contained in Attachments 2 and 3 as CBI as set out above in this letter. DWMRC Comment Number 3: 3. Documentation Supporting Forthcoming SERP Evaluations Related to Rare Earth Elements As mentioned above, during the February 5, 2024 meeting, EFRI indicated that moving forward with expansions to the rare earth circuit was a priority for the 2024 calendar year. Further expansions to the rare earth circuit would require, at a minimum, a SERP evaluation. As described above, this evaluation will require an analysis as to whether the expansion of the rare earth circuit would(]) conflict with license conditions or regulations, (2) degrade essential safety or environmental commitments, or (3) fall outside of the actions analyzed in the most recent Environmental Assessment. As discussed during the February 5, 2024 meeting, the Division requests that EFRI submit any preliminary documentation it has which would support 2024 SERP analyses and decisions concerning the rare earth Letter to Doug Hansen June 6, 2024 Page4 circuit. Any information EFRI currently has and can submit to the Division concerning 2024 expansions to the rare earth circuit could help expedite the Division's review of such decisions. EFRI Response: As discussed on February 5, 2024, the Mill is contemplating expanding its existing REU circuit by adding its Phase 2 REU separation circuit, which will include the addition of a calciner that is dedicated to REU calcining. EFRI is currently in the engineering and design process for this expanded circuit EFRI will continue to evaluate this expanded circuit relative to the Mill's licensed environmental envelope, Mill License, Groundwater Discharge Permit and Air Approval Order conditions and applicable laws and regulations to determine what parts of the expanded circuit can be approved via SERP and what, if any, License, Groundwater Discharge Permit or Air Approval Order Amendments may be required. Once the engineering has been advanced to a sufficient level of certainty and detail, EFRI will submit a detailed analysis to DWMRC explaining what matters EFRI believes can be approved via SERP and what matters, if any, may require License, Permit or Air Approval Order Amendment. Upon DWMRC concurrence with EFRI's analyses, EFRI will then proceed with the preparation of any amendment applications that may be required and perform all SERP actions that wiJI be required. DWMRC Comment Number 4: 4. Documentation Characterizing Monazite Sands from Alternative Sources On June 25, 2020, EFRI submitted a letter advising the Division of its plan to receive and process natural uranium ores in the form of monazite sands from The Chemours Company's (Chemours) Mineral Sand Separation Plant in Offerman, Georgia (DRC-2020-011981). The Division requested additional information concerning the Chemours monazite sands on July 21, 2020 (DRC-2020-012682), and EFRI responded to this request on September 9, 2020 (DRC-2020-015241). In a letter dated September 11, 2020 (DRC-2020-015094), the Division concurred that the Chemours monazite sands discussed in the above- mentioned correspondences is naturally occurring ore and that no additional licensing actions would be required for the mill to accept the material. During the February 5, 2024 meeting, EFRI indicated that they were pursuing monazite sands from sources other than Chemours. Please be advised that the aforementioned September 11, 2020 letter from the Division only considers monazite sands from Chemours June 25, 2020 and September 9, 2020 letters from EFRI. Similar monazite sand from any other source would have to be similarly evaluated to determine if the sand was natural ore and not an alternate feed This evaluation would also have to be documented. During the February 5, 2024 meeting, the Division indicated that it would need to review this natural ore determination as well as all supporting documentation on a case-by-case basis for each source of monazite. Therefore, the Division requests that EFRI submit any documentation it has pertaining to monazite sands from sources other than the Chemours Company's Mineral Sand Separation Plant in Offerman, Georgia, including but not limited to: the composition of the sand; methods used to extract, generate, or produce the sand; and any cleaning, sieving, or processing of the sand prior to potential receipt at White Mesa Again, providing this information well ahead of any planned receipts allows the Division time to review EFRI's determinations and helps mitigate any potential delays. Letter to Doug Hansen June 6, 2024 Page 5 EFRJ Response: EFRJ will submit documentation that demonstrates to DWMRC that any monazite sands from sources other than Chemours is natural ore and not an alternate feed, well ahead of any planned receipts of any such monazite sands. If you have any questions regarding this letter, please contact the undersigned at (303) 389-4134 or Mr. Scott Bakken at (303) 389-4132. Yours very truly, {tial(Jfr~ ENERGY FuELS RESOURCES {USA) INC. Kathy Weinel Director, Regulatory Compliance cc David Frydenlund Garrin Palmer Logan Shumway Scott Balcken Jo Ann T ischler (Tischler Consulting) June 6, 2024 VIA EXPRESS DELIVERY Mr. Doug Hansen Director Division of Waste Management and Radiation Control Utah Department of Environmental Quality 195 North 1950 West Salt Lake City, UT 84116 Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 www.energyfuels.com Re: Response to Request for Information Ahead of Implementing Phase 2 of the Rare Earth Circuit, Radioactive Materials License Number UT 19004 79 Dear Mr. Hansen: Pursuant to the Division of Waste Management and Radiation Control's ("DWMRC's") letter dated April 25, 2024, Energy Fuels Resources (USA) Inc. ("EFRI") is providing responses to the request for information. For ease ofreview, this letter provides the DWMRC comments verbatim, in italics, below, followed by EFRI's response. One copy of the enclosed Attachments is unredacted and complete for internal DWMRC review and use (see Attachments 4 through 6). One copy has been redacted in accordance with Utah Code 63G-2-101 et seq. as noted below (see Attachments 1 through 3). EFRI is requesting that certain information enclosed with this letter be withheld from public disclosure because it is considered confidential business information ("CBI") pursuant to the provisions of the Utah Government Records Access and Management Act ("GRAMA"), Utah Code 63G-2-101 et seq. The information sought to be withheld is that information in Attachments 1 through 3 that has been redacted or "blacked out" on each page of the redacted transmittals. The redacted information is also indicated by an electronic marking "Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below." All redactions were based on CBI/Proprietary Information. Pursuant to Section 63G-2-309(1)(a)(i) of GRAMA, EFRI hereby designates the redacted information identified above as CBI. The documents and information qualify as CBI because they are not publicly available, and disclosure of the information therein likely would cause substantial harm to EFRI's competitive position. The documents and information have been provided for the exclusive use of the DWMRC on the express understanding that the information therein will be treated as confidential. Accordingly, the redacted information should be treated as confidential by DWMRC. Pursuant to Section 63G-2-305 of GRAMA, the DWMRC should maintain the enclosed documents and information as protected and confidential, and exempt them from public records or disclosure laws, including but not limited to any subsequent requests under GRAMA or under the Freedom of Information Act ("FOIA"). If a request is made for public review of the documents or information, DWMRC must Letter to Doug Hansen June 6, 2024 Page 2 notify EFRI and provide the company with a reasonable time in which to object to their disclosure or seek an injunction preventing disclosure. Pursuant to Section 63G-2-107 of GRAMA, Energy Fuels also invokes relevant U.S. Nuclear Regulatory Commission regulations and guidance that protect the redactions, including but not limited to the withholding of proprietary, personally identifiable and security-related information under 10 CFR 2.390. DWMRC Comment Number 1: 1. SOPs Related to the Uranium Bearing Rare Earth Procedures License condition 9. 6 requires EFRI to submit up-to-date copies of all operational and non-operational Standard Operating Procedures (SOP) to the Director of the Division (Director) by December 31 of each year. EFRI submits a list ofSOPs annually, most recently on December 19, 2022 (DRC-2022-024175) and on December 14, 2023 (DRC-2023-078612). However, in both submissions, the SOPs included in "Book 15 -Uranium Bearing Rare Earth Procedures" have been omitted with a brief statement that the SOPs are proprietary and contain confidential business information (CBI). The Division is not in receipt of a valid CBI claim relating to these SOPs. Under GRAMA., Utah Code Section 63G-2-309(l)(a)(i), a person who wants to claim that a record provided to the Division is protected from disclosure to a member of the public because it is CBI shall provide with the record i) a written claim of business confidentiality; and ii) a concise statement of reasons supporting the claim. Utah Code Section 63G-2-305(1) (trade secrets) and (2) (commercial information) describes the standards and requirements that apply to the kinds of information that may be subject to a CBI claim. A request for CBI treatment must be specific as to the rationale for the CBI claim and which records, or portions of records, are covered by the CBI claim. Please also refer to Utah Code§ 63G-2-309(l)(a)(i). Without this information, the Division is unable to determine whether the CBI claim is valid. As such, the Division is requesting EFRI submit all SOPs contained in Book 15 and any other SOPs related to rare earth processing, along with a valid claim for treatment as CBI, if appropriate, as outlined in the preceding paragraphs. The Division recommends that EFRI submits both a complete and redacted version of each SOP. When performing redactions, please ensure that it is clear what has been redacted and why. To better protect any potential CBI, please submit the SOPs and CBI claim as hard copies through the mail and not electronically through dwmrcsubmit@utah.gov. EFRI Response: As requested, the SOPs for rare earth bearing uranium, ("REU") ore processing are included in Attachments 1 (redacted) and 4 (unredacted). EFRI hereby claims for treatment of the redacted information contained in Attachment 1 as CBI as set out above in this letter. DWMRC Comment Number 2: 2. Documentation Supporting Evaluations Conducted for the 2022 Annual SERP Report License condition 9.4 outlines the procedures EFRI must follow when evaluating whether i) a change to the facility, ii) a change to procedures, or iii) conducting an experiment would require a license amendment. Part B of condition 9.4 outlines the criterium a potential change must meet to not require a license amendment. A Safety and Environmental Review Panel (SERP), therefore, evaluates each potential change Letter to Doug Hansen June 6, 2024 Page 3 against the criteria set forth in Part B to determine if the change requires a license amendment. Actions taken by the SERP must follow the most up-to-date version of SOP "P BL-1 -SERP Procedure" and are required to be reported to the Director by March 31 of the following calendar year per license condition 9.4 part D. EFRI has annually submitted a report summarizing actions taken by the SERP, most recently on March 31, 2022 (DRC-2022-005502), March 30, 2023 (DRC-2023-002850), and March 26, 2024 (DRC-2024- 005046). Section 4.0 of SOP PBL-1, "SERP Procedure", requires the SERP to document its review of whether a potential change meets the criteria described in license condition 9.4 part B: Section 4. 0 SERP Review Procedure In their documented [emphasis added] review of whether a potential change, test, or experiment (hereinafter called "the change'') is allowed under the License or P BLC, without a License amendment, the SERP shall consider the following: (1) Current License Requirements : ... (2) Impacts on regulations: ... (3) Environmental Assessment: ... The documentation associated with the SERP review is typically not submitted as part of the annual summary of SERP actions. The Division requests that EFRI submit all documentation supporting both decisions summarized in the 2022 Safety and Environmental Review Panel (SERP) Annual Report dated March 30, 2023 (DRC-2023-002850). If EFRI believes that this documentation contains CBL please submit a claim for treatment as CBI as outlined above, and the Division will assess this claim upon receipt. EFRI Response: As noted above, EFRI completed two SERP analyses in 2022. The resulting SERP Reports and associated documentation contain CBI as noted above and both redacted and unredacted copies have been provided. The redacted versions are included in Attachments 2 and 3 and the unredacted versions are included in Attachments 5 and 6. EFRI hereby claims for treatment of the redacted information contained in Attachments 2 and 3 as CBI as set out above in this letter. DWMRC Comment Number 3: 3. Documentation Supporting Forthcoming SERP Evaluations Related to Rare Earth Elements As mentioned above, during the February 5, 2024 meeting, EFRI indicated that moving forward with expansions to the rare earth circuit was a priority for the 2024 calendar year. Further expansions to the rare earth circuit would require, at a minimum, a SERP evaluation. As described above, this evaluation will require an analysis as to whether the expansion of the rare earth circuit would (1) conflict with license conditions or regulations, (2) degrade essential safety or environmental commitments, or (3) fall outside of the actions analyzed in the most recent Environmental Assessment. As discussed during the February 5, 2024 meeting, the Division requests that EFRI submit any preliminary documentation it has which would support 2024 SERP analyses and decisions concerning the rare earth Letter to Doug Hansen June 6, 2024 Page4 circuit. Any information EFRI currently has and can submit to the Division concerning 2024 expansions to the rare earth circuit could help expedite the Division 's review of such decisions. EFRI Response: As discussed on February 5, 2024, the Mill is contemplating expanding its existing REU circuit by adding its Phase 2 REU separation circuit, which will include the addition of a calciner that is dedicated to REU calcining. EFRI is currently in the engineering and design process for this expanded circuit. EFRI will continue to evaluate this expanded circuit relative to the Mill's licensed environmental envelope, Mill License , Groundwater Discharge Permit and Air Approval Order conditions and applicable laws and regulations to determine what parts of the expanded circuit can be approved via SERP and what, if any, License, Groundwater Discharge Permit or Air Approval Order Amendments may be required. Once the engineering has been advanced to a sufficient level of certainty and detail, EFRI will submit a detailed analysis to DWMRC explaining what matters EFRI believes can be approved via SERP and what matters, if any, may require License, Pennit or Air Approval Order Amendment. Upon DWMRC concurrence with EFRI's analyses, EFRI will then proceed with the preparation of any amendment applications that may be required and perform all SERP actions that will be required. DWMRC Comment Number 4: 4. Documentation Characterizing Monazite Sands from Alternative Sources On June 25, 2020, EFRI submitted a letter advising the Division of its plan to receive and process natural uranium ores in the form of monazite sands from The Chemours Company's (Chemours) Mineral Sand Separation Plant in Offerman, Georgia (DRC-2020-011981). The Division requested additional i,iformation concerning the Chemours monazite sands on July 21, 2020 (DRC-2020-012682), and EFRJ responded to this request on September 9, 2020 (DRC-2020-015241). In a letter dated September 11, 2020 (DRC-2020-015094), the Division concurred that the Chemours monazite sands discussed in the above- mentioned correspondences is naturally occurring ore and that no additional licensing actions would be required for the mill to accept the material. During the February 5, 2024 meeting, EFRJ indicated that they were pursuing monazite sands.from sources other than Chemours. Please be advised that the ciforementioned September 11, 2020 letter from the Division only considers monazite sands from Chemours June 25, 2020 and September 9, 2020 letters from EFRI. Similar monazite sand from any other source would have to be similarly evaluated to determine if the sand was natural ore and not an alternate feed. This evaluation would also have to be documented. During the February 5, 2024 meeting, the Division indicated that it would need to review this natural ore determination as well as all supporting documentation on a case-by-case basis for each source of monazite. Therefore, the Division requests that EFRJ submit any documentation it has pertaining to monazite sands from sources other than the Chemours Company's Mineral Sand Separation Plant in Offerman, Georgia, including but not limited to: the composition of the sand; methods used to extract, generate, or produce the sand; and any cleaning, sieving, or processing of the sand prior to potential receipt at White Mesa. Again, providing this information well ahead of any planned receipts allows the Division time to review EFRJ 's determinations and helps mitigate any potential delays. Letter to Doug Hansen June 6, 2024 Page 5 EFRJ Response: EFRJ will submit documentation that demonstrates to DWMRC that any monazite sands from sources other than Chemours is natural ore and not an alternate feed, well ahead of any planned receipts of any such monazite sands. If you have any questions regarding this letter, please contact the undersigned at (303) 389-4134 or Mr. Scott Bakken at (303) 389-4132. Yours very truly, (M1Jr~ ENERGY FUELS RESOURCES (USA) INC. Kathy Weinel Director, Regulatory Compliance cc David Frydenlund Garrin Palmer Logan Shumway Scott Bakken Jo Ann Tischler (Tischler Consulting) REDACTED ATTACHMENTS Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below Pursuant to Utah Code 63G-2-101 et seq. each page in this attachment that contains information sought to be withheld from public disclosure is indicated based on Confidential Business Information (CBI) or Proprietary Information. ATTACHMENT I REU SOPs -REDACTED Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 -Introduction INTRODUCTION Mill Process Date: 03-21 Revision: EFR-1 Page 1 of 1 The rare earth bearing uranium, ("REU"), ore process begins with receipt, weighing, and sampling of the REU ore. The REU ore is fed into a The solid tailings from the rare earth acid leach are subsequently processed like typical uranium ore to recover uranium, which will be recovered using existing ore processing procedures. Process Controls Process control computers are located in the central control room, solvent extraction control room, vanadium control room, grind circuit below the derrick screens, and in the upper level of the counter-current decantation ("CCD") circuit. Radiation Protection Energy Fuels Resources (USA) Inc. ("EFRI") has outlined and implements a personnel radiation protection program to ensure that operations at the plant are conducted in a safe and efficient manner and in accordance with approved procedures. This radiation protection program is documented and administered in accordance with the State of Utah Division of Waste Management and Radiation Control ("DWMRC") applicable regulations detailed in the Code of Federal Regulations ("CFR") Title 10 Energy and the State of Utah regulations. Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Rare Earth Bearing Uranium Ore Operating Procedures Book 15 Section I -Receiving RECEIVING Preface Date: 03-21 Revision: EFR-1 Page 1 of 4 The following procedure applies to the acceptance, handling, and storage of rare earth bearing uranium ("REU") ore at the White Mesa Mill. It is important that all shipments are received at the mill in a safe and efficient manner while complying with required regulations during the receiving process. Prior to Shipment All radioactive shipments must conform to Titles 10 and 49 of the U.S. Code of Federal Regulations ("CPR"). Each load must have all required placards and labels affixed to the trailer and a copy of the completed shipping manifest will accompany each shipment. Energy Fuels Resources (USA) Inc. ("EFRI") must be notified when shipments are scheduled to depart and when they are expected to arrive at the White Mesa Mill for offloading. Designated Storage Area REU ores will be stored at a designated location on the ore storage pad. The material will be stored in super sacks and will be kept on pallets while waiting to be processed in the mill. No other alternate feed materials or uranium ore will be stored in the same location on the ore storage pad as the REU ores while they are in storage. If material is on the ore pad longer than one year from the date of receipt storage procedures will be modified. The dose rate around the designated storage area of the REU ores will be monitored. If the dose rate exceeds 5 mrem/hr, the storage location area will be posted as a radiation area. UT Admin Code R313-12-13 and R313-l 5-902 Material Receiving 1. Before a shipment of REU ore enters the restricted area, a qualified individual will inspect the shipment and its contents. This inspection is to verify that the material has not leaked during transport, the truck is properly placarded, and to record the beta/gamma readings of the shipment. If material has leaked out of the super sacks the spill must be documented on the Feed Material Receipt inspection form and cleaned. Leaking bags will be handled in a manner to avoid dispersing the REU ore. 2. When each truck driver enters the restricted area for the first time, the scale house operator will provide a hazard awareness training for the driver as described in EFRI Standard Operating Procedure ("SOP") in Bookl, Section 2. 3 . The onsite transportation expert will inspect all copies of the Shipping Manifest and the transporter's Bill of Lading to ensure that the shipment is destined for the Mill, to verify the contents of the shipment, and to ensure all of the required paper work is provided. If there are any discrepancies in the shipping manifest, the scale house operator will notify their supervisor and wait for guidance before off-loading. 4. The scale house operator will create a scale ticket for each shipment. The following information will be recorded on the scale ticket: Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Rare Earth Bearing Uranium Ore Operating Procedures Book 15 Section I -Receiving a. Date and time b. Truck and trailer number c. Gross, tare, net weights d. Bill of lading or shipment number e. Shipper ID Date: 03-21 Revision: EFR-1 Page 2 of 4 5. Prior to transporting the material to the offloading area, a member of the utility crew will be notified by the scale house operator and the driver will then be allowed to proceed to the off- loading location on the ore pad. Material Unloading 1. The scale house operator will direct the driver to the offloading location on the ore pad. 2. The driver will back his truck and trailer to the portable off-loading ramp on the ore pad. 3. Before using the portable offloading ramp, the safety chains will be attached to the trailer. 4. The load will then be visually inspected again for any potential damage and then the cribbing and strapping will be removed from the trailer. 5. When offloading the super sacks, the fork lift operator should take caution not to damage the super sacks or pallets and have a spotter present to assist when needed. 6. After all material is unloaded, disconnect the ramp from the trailer and guide empty truck back to the scale house followed by decon pad. 7. Before leaving the property, all placards and labels will be removed from the trailer. Additional placards or labels may be applied if the trailer is leaving as an unrestricted load. Decontamination and Release of Trailers and Trucks All trailers and trucks will be decontaminated after unloading prior to leaving the Mill. Any trailers that are to be released for restricted use will be decontaminated according to the requirements contained in Department of Transportation ("DOT") Part 49 CFR 173.428 or 173.443. Any trailers that are to be released for unrestricted use will be decontaminated according to the requirements found in Table 2 of the Nuclear Regulatory Commission's Regulatory Guide 8.30 Rev. 1 "Health Physics Surveys in Uranium Recovery Facilities" or NRC document "Guidelines for Decontamination of Facilities and Equipment Prior to Release for Unrestricted Use or Termination of Licenses for Byproduct, Source, or Special Nuclear Material" issued April 1993. For the appropriate decontamination procedures 1 refer to the procedures in Book 9, Radiation Protection Manual, Section 6. Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Rare Earth Bearing Uranium Ore Operating Procedures Book 15 Section I -Receiving Documentation Documentation of Shipments: Date: 03-21 Revision: EFR-1 Page 3 of 4 For each shipment the following records will be maintained at the mill for at least 5 years. • Shipper's Manifest and Bill of Lading. • Completed scale ticket. • Survey release forms. Hazard Identification and Safety Personal P1·otective Equipment ("PPE ) and Clothing 1. Minimum PPE requirements at White Mesa Mill while in the restricted area is hard hats, safety glasses, and steel toed shoes. No ragged or lose fitting clothing is allowed. Body jewelry, rings, wrist watches, etc. are required to be removed while working. 2 Other personal protective equipment includes, but is not limited to: ear plugs, respirators, wet suits, welding helmets, goggles, gloves, and rubber boots. Face shields and safety belts are required in designated areas and/or while performing certain jobs. If in doubt, contact your supervisor. 3 Each employee is responsible for the condition of their protective equipment. Report any defects, etc., to your supervisor. 4 The following equipment is required when working on pipelines or vessels containing acids or caustics: a. Face shield and chemical splash goggles b. Rubber coat and pants c. Rubber gloves and rubber boots d. Other equipment specified by the foreman for that particular job listed on the Safe Work Permit 5 The use of a safety belt and properly adjusted lifeline is required where there is a danger of falling four feet or more, except while performing work under the ladder and scaffold section of this manual. This rule applies when going beyond the handrails of walkways on top of any tanks in the mill area. 6 It is a condition of employment that all personnel who may be required to wear a respirator must be clean shaven to assure that the respirator fits properly. Personnel will be fully trained prior to using respirators. 1. Industrial Hazards and Safety a) Use caution when the trailers are backing to the unloading area. b) Drivers must use caution during the unloading process and be aware of any overhead hazards. c) Use caution when entering or exiting equipment. Be sure to use the ladders and hand rails. Do not jump off the equipment. Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Rare Earth Bearing Uranium Ore Operating Procedures Book 15 Section 1 -Receiving Date: 03-21 Revision: EFR-1 Page 4 of 4 d) Always use a ladder when entering and/or exiting the interior of a trailer. 2. Mobile Equipment a) Only trained and authorized persons may operate mobile equipment . b) All mobile equipment will be inspected by the operator and any safety defects corrected before the equipment is used . If safe to do so , the equipment may be driven to the shop for repairs . Otherwise, the equipment must be towed or repaired at the location. c) Equipment shall be operated at a reasonable speed consistent with road and weather conditions, subject to a maximum speed limit of 15 mph. d) Keep the cabs of equipment clean. Loose items that could jam controls or create other hazards are not allowed . e) Report all accidents to your supervisor regardless of how minor they are . If property damage or personal injury is involved, do not move the equipment until your supervisor has released it. Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Date: 03-21 Revision: EFR-1 Page 1 of 4 Book 15 Section 2 -Ore and - REU ORE AND -FEED Preface The purpose of this Standard Operating Procedure ("SOP") is to describe the procedures used to feed the REU ore to the mill and to begin processing. Additionally, The circuit consists of a bag dumping unit and an agitated feed tank. The mill building overhead crane will be used to lift bags from the null floor to the bag dumping unit. are also fed into the tank. The operators' responsibility is to add URE ore and -at the correct speed and in the right proportions. To help accomplish this, operators will take samples of the feed tank slurry and analyze it for - Communication: To be successful as an operator in achieving the desired results in your circuit good communication between you, the metallurgical department, and your supervisor should exist. Information is given the operator verbally, written, and by test results. As an operator if you do not understand any information given you have the responsibility to ask questions until you do understand. White board. In a few locations in the mill critical information about mill operations will be written on White Boards. Information such as circuit parameters, required changes in circuit operations, or special instructions about maintenance. Circuit sheets. Circuit sheets will have operating parameters on them along with sampling times for the circuit. They will also have a place for you to pass along written information about your circuit. Verbal. One of the most important times of your shift is at shift change. You have the responsibility to pass along information about your circuit to the person relieving you. You will be given verbal instructions from your supervisor or metallurgical department which you need to be sure you understand. Written. Instructions will be handed out in written form almost daily. As above if you do not understand any instruction ask your supervisor. Health and Safety Care must be taken in all aspects of the dumping procedure to ensure the continued health and safety of null employees. The super sacks must be lifted from the null floor to the bag dumping system, presenting a suspended load risk near the feed tank at all times. Additionally, REU ores (just like standard uranium ore) are radioactive. Instructions from the Radiation Safety Department regarding procedure, Personal Protective Equipment (" PPE"), etc. must be followed at all times to reduce physical and physiological risks. Hazards: • Over head loads • Radioactive solids Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 2 -Ore and - • Pinch points • Moving equipment • + Date: 03-21 Revision: EFR-1 Page 2 of 4 • Hose Pumps can fail if either the intake or discharge lines are restricted, which may spray solutions. • Pumps that require gland seal water will fail if the gland seal water is not turned on. Additionally, if the pump is off and the gland seal water is left on it will dilute process solutions and cause problems in the process. Personal Protective Equipment and Clothing 1. Minimum PPB requirements at White Mesa Mill while in the restricted area is hard hats, safety glasses, and steel toed shoes. No ragged or lose fitting clothing is allowed. Body jewelry, rings, wrist watches, etc. are required to be removed while working. 2 Other personal protective equipment includes, but is not limited to: ear plugs, respirators, wet suits, welding helmets, goggles, gloves, and rubber boots . Face shields and safety belts are required in designated areas and/or while performing certain jobs. If in doubt, contact your supervisor. 3 Each employee is responsible for the condition of their protective equipment. Report any defects, etc., to your supervisor. 4 The following equipment is required when working on pipelines or vessels containing acids or caustics: a. Face shield and chemical splash goggles b. Rubber coat and pants c. Rubber gloves and rubber boots d. Other equipment specified by the foreman for that particular job listed on the Safe Work Permit 5 The use of a safety belt and properly adjusted lifeline is required where there is a danger of falling four feet or more, except while performing work under the ladder and scaffold section of this manual. This rule applies when going beyond the handrails of walkways on top of any tanks in the mill area. 6 It is a condition of employment that all personnel who may be required to wear a respirator must be clean shaven to assure that the respirator fits properly. Personnel will be fully trained prior to using respirators. Monazite Dumping The REU ore feed will be weighed and sampled before dumping. The REU ore super sacks will be dumped using a bag dumping system into a mixing tank. The mixing tank will contain REU ore, I . Dusting and fumes will be contained using the existing leach demister system. The rate at which bags are dumped will be determined by the metallurgical and operations departments to achieve a target feed rate . Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 2 -Ore and - Bag Dumping Operating Procedures Date: 03-21 Revision: EFR-1 Page 3 of 4 1. Operators will wear complete PPE as directed by supervisors and the Radiation Safety Department. 2. The bag lifting area under the crane should be closed to access and appropriately posted. 3. The demister system should be running at all times during dumping operations. 4. Bags will be fed to the circuit on a schedule to be set by the metallurgical department (e.g. one bag of REU or Additional bags of REU ore and 5. Inspect the super sack to be dumped for any defects, leaks, etc. 6. Secure the bag to the overhead crane. 7. Vacate the area under the crane. 8. Lift and load the super sack into the bag dumping system. Be sure the bag is emptied as completely as possible into the system. 9. Empty super sacks will be collected and disposed of in tailings. Bags should be rolled or folded up from the bottom and placed in a container to avoid spillage on the ground when leaving the mill building. 10. After the addition of the super sacks, the operator will analyze a sample of the feed tank for - The sample should be taken from the sample port near the feed tank outlet. Targets will be set by a supervisor to determine acceptable ranges for these analyses. I I I Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 2 -Ore and - I ■ Date : 03-21 Revision : EFR-1 Page 4 of 4 12. The feed tank level should be maintained at a level dictated by a supervisor. The level should be controlled by the peristaltic pump feeding the crack tank. Dumping System Start-up Procedure 1. Inform other personnel that URE ore and I I I I I - 7. Inform the downstream circuits that they can begin operating. Dumping System Shut-down Procedure 1. Inform downstream circuits that the dumping circuit is shutting down. 2. Ensure that the overhead crane and any bags are safely parked and free of any stored energy . 3. - Emergency Shut Down • Take remote to the Crane and shut power off to the Crane. Be sure to follow zero energy practices, if the Crane has a load suspended lower the load to the floor before turning the Crane off. Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Date: 03-21 Revision: EFR-1 Page 1 of 4 Book 15 Section 3 -- Preface - Communication: To be successful as an operator in achieving the desired results in your circuit good communication between you, the metallurgical depa1tment, and your supervisor should exist. Information is given the operator verbally, written, and by test results. As an operator if you do not understand any information given you have the responsibility to ask questions until you do understand. White board. In a few locations in the mill critical information about mill operations will be written on White Boards. Information such as circuit parameters, required changes in circuit operations, or special instructions about maintenance. Circuit sheets. Circuit sheets will have operating parameters on them along with sampling times for the circuit. They will also have a place for you to pass along written information about your circuit. Verbal. One of the most important times of your shift is at shift change. You have the responsibility to pass along information about your circuit to the person relieving you. You will be given verbal instructions from your supervisor or metallurgical department which you need to be sure you understand. Written. Instructions will be handed out in written form almost daily. As above if you do not understand any instruction ask your supervisor. Hazards: • • Radioactive solids • Steam • Hose Pumps will fail if either intake or discharge lines are restricted. Which may spray solution. • Pumps that require gland seal water will fail if the gland seal water is not turned on. Additionally, if the pump is off and the gland seal water is left on it will dilute process solutions and cause problems in the process. Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 3 -- Personal Protective Equipment and Clothing Date: 03-21 Revision: EFR-1 Page 2 of 4 1. Minimum PPE requirements at White Mesa Mill while in the restricted area is hard hats, safety glasses, and steel toed shoes. No ragged or lose fitting clothing is allowed. Body jewelry, rings, wrist watches, etc. are required to be removed while working. 2 Other personal protective equipment includes, but is not limited to: ear plugs, respirators, wet suits, welding helmets, goggles, gloves, and rubber boots. Face shields and safety belts are required in designated areas and/or while performing certain jobs. If in doubt, contact your supervisor. 3 Each employee is responsible for the condition of their protective equipment. Report any defects, etc., to your supervisor. 4 The following equipment is required when working on pipelines or vessels containing acids or caustics: a. Face shield and chemical splash goggles b. Rubber coat and pants c. Rubber gloves and rubber boots d. Other equipment specified by the foreman for that particular job listed on the Safe Work Permit 5 The use of a safety belt and properly adjusted lifeline is required where there is a danger of falling four feet or more, except while performing work under the ladder and scaffold section of this manual. This rule applies when going beyond the handrails of walkways on top of any tanks in the mill area. 6 It is a condition of employment that all personnel who may be required to wear a respirator must be clean shaven to assure that the respirator fits properly. Personnel will be fully trained prior to using respirators. will be released from the steam coils through steam traps. Steam traps make the steam coils more energy efficient by regulating the discharge of the steam coils and only allowing condensate to exit the system. The steam traps are probably not functioning correctly if there isn't any condensate leaving the condensate line or if steam is leaving the condensate line. Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 3-- Date: 03-21 Revision: EFR-1 Page 3 of 4 ear appropriate PPE at all times. Care must also be taken to ensure that the sample is representative of the slurry. This includes purging lines before collecting samples and not leaving solids behind in the sample cup. Operating lnstructi.ons 1. Conduct a proper Shift Change with the person you are relieving. Get information about all circuit parameters, including, but not limited to: Crack temperature, feed flow rate, feed density, tank level, -concentration of the crack solution. I I I I I Sta..t-up Procedures I I I I I I I I - Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 3 -- Shut-down Procedures I I I I I I I I Emergency Shut-down Procedures I I Date: 03-21 Revision : EFR-1 Page 4 of 4 Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Date: 03-21 Revision: EFR-1 Page 1 of 4 Procedures Book 15 Section 4 - Preface Communication: To be successful as an operator in achieving the desired results in your circuit good communication between you, the metallurgical department, and your supervisor should exist. Information is given the operator verbally, written, and by test results. As an operator if you do not understand any information given you have the responsibility to ask questions until you do understand. White board. In a few locations in the mill critical information about mill operations will be written on White Boards. Information such as circuit parameters, required changes in circuit operations, or special instructions about maintenance. Circuit sheets. Circuit sheets will have operating parameters on them along with sampling times for the circuit. They will also have a place for you to pass along written information about your circuit. Verbal. One of the most important times of your shift is at shift change. You have the responsibility to pass along information about your circuit to the person relieving you. You will be given verbal instructions from your supervisor or metallurgical department which you need to be sure you understand. Written. Instructions will be handed out in written form almost daily. As above if you do not understand any instruction ask your supervisor. Health and Safety The slurry exiting the crack tank will be very hot and contains high concentrations of -Care needs to be taken to avoid exposure to this slurry. Additionally, the washing procedures will make use of centrifuges to separate the solids from the solution . Proper guarding must be in place and procedures followed to ensure the safety of personnel operating this equipment. Hazards: • • Moving equipment • Pinch points • Radioactive solids • • Hose Pumps will fail if either intake or discharge lines are restricted. Which may spray solution. Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 4 -g Date: 03-21 Revision: EFR-1 Page 2 of 4 • Pumps that require gland seal water will fail if the gland seal water is not turned on. Additionally, if the pump is off and the gland seal water is left on it will dilute process solutions and cause problems in the process. Personal Protective Equipment and Clothing 1. Minimum PPE requirements at White Mesa Mill while in the restricted area is hard hats, safety glasses, and steel toed shoes. No ragged or lose fitting clothing is allowed. Body jewelry, rings, wrist watches, etc. are required to be removed while working. 2 Other personal protective equipment includes, but is not limited to: ear plugs, respirators, wet suits, welding helmets, goggles, gloves, and rubber boots . Face shields and safety belts are required in designated areas and/or while performing certain jobs. If in doubt, contact your supervisor. 3 Each employee is responsible for the condition of their protective equipment. Report any defects, etc., to your supervisor. 4 The following equipment is required when working on pipelines or vessels containing acids or caustics: a. Face shield and chemical splash goggles b. Rubber coat and pants c. Rubber gloves and rubber boots d. Other equipment specified by the foreman for that particular job listed on the Safe Work Permit 5 The use of a safety belt and properly adjusted lifeline is required where there is a danger of falling four feet or more, except while performing work under the ladder and scaffold section of this manual. This rule applies when going beyond the handrails of walkways on top of any tanks in the mill area. 6 It is a condition of employment that all personnel who may be required to wear a respirator must be clean shaven to assure that the respirator fits properly . Personnel will be fully trained prior to using respirators. Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 4 - I. Perform a pre-shift inspection with the operator(s) coming off shift. Review flow rates, temperatures, concentrations, operational challenges, etc. Visually inspect lines, tanks, and equipment for any irregularities. 2. Appropriate PPE, dictated by the Radiation Safety Department is required while working in this circuit. 3. Follow schedules set by the maintenance depattment for greasing and cleaning the centrifuges . 4. Maintain wash water flow rates as determined by a supervisor. I I I I I. Perform periodic service based on manufactures recommendation on the centrifuges as outlined by a supervisor. 2. Inform the upstream and downstream circuits that the solids washing circuit is starting up. I I I Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 4 - 6. I I I I - I I I Date: 03-21 Revision: EFR-1 Page 4 of4 Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Date: 03-21 Revision: EFR-1 Page 1 of3 Book 15 Section 5 -- Preface - Communication: To be successful as an operator in achieving the desired results in your circuit good communication between you, the metallurgical department, and your supervisor should exist. Information is given the operator verbally, written, and by test results. As an operator if you do not understand any information given you have the responsibility to ask questions until you do understand. White board. In a few locations in the mill critical information about mill operations will be written on White Boards. Information such as circuit parameters, required changes in circuit operations, or special instructions about maintenance. Circuit sheets. Circuit sheets will have operating parameters on them along with sampling times for the circuit. They will also have a place for you to pass along written information about your circuit. Verbal. One of the most important times of your shift is at shift change. You have the responsibility to pass along information about your circuit to the person relieving you. You will be given verbal instructions from your supervisor or metallurgical department which you need to be sure you understand. Written. Instructions will be handed out in written form almost daily. As above if you do not understand any instruction ask your supervisor. Health and Safety Hazards: • • Heat, steam Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 5 -- • Radioactive Solids Date: 03-21 Revision: EFR -1 Page 2 of3 • Tyvek, respirators, and chemical resistant gloves worn when handing. • Hose Pumps will fail if either intake or discharge lines are restricted. Which may spray solution. • Pumps that require gland seal water will fail if the gland seal water is not turned on. Additionally, if the pump is off and the gland seal water is left on it will dilute process solutions and cause problems in the process. Personal Protective Equipment and Clothing 1. Minimum PPE requirements at White Mesa Mill while in the restricted area is hard hats, safety glasses, and steel toed shoes. No ragged or lose fitting clothing is allowed. Body jewelry, rings, wrist watches, etc. are required to be removed while working. 2 Other personal protective equipment includes, but is not limited to: ear plugs, respirators, wet suits, welding helmets, goggles, gloves, and rubber boots. Face shields and safety belts are required in designated areas and/or while performing certain jobs. If in doubt, contact your supervisor. 3 Each employee is responsible for the condition of their protective equipment. Report any defects, etc., to your supervisor. 4 The following equipment is required when working on pipelines or vessels containing acids or caustics: a. Face shield and chemical splash goggles b. Rubber coat and pants c. Rubber gloves and rubber boots d. Other equipment specified by the foreman for that particular job listed on the Safe Work Permit 5 The use of a safety belt and properly adjusted lifeline is required where there is a danger of falling four feet or more, except while performing work under the ladder and scaffold section of this manual. This rule applies when going beyond the handrails of walkways on top of any tanks in the mill area. 6 It is a condition of employment that all personnel who may be required to wear a respirator must be clean shaven to assure that the respirator fits properly. Personnel will be fully trained prior to using respirators. - Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 5 -- If a bag is broken, wash the area down immediately and thoroughly. Date: 03-21 Revision: EFR-1 Page 3 of 3 When dumping bags be aware of traffic in the area . People without PPE should not be in the area. 1. Operators will wear complete PPE as directed by supervisors and the Radiation Safety Department. 2 . Perform a pre-shift inspection with the operator(s) coming off shift. Review flow rates, temperatures, concentrations, operational challenges, etc. Visually inspect lines, tanks, and equipment for any irregularities. 3. Ensure that the demister system is operating at all times . I I I I I I I I I I I I Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 6 -- Preface Communication: Date: 03-21 Revision: EFR-1 Page 1 of 4 To be successful as an operator in achieving the desired results in your circuit good communication between you, the metallurgical department, and your supervisor should exist. Information is given the operator verbally, written, and by test results. As an operator if you do not understand any information given you have the responsibility to ask questions until you do understand. White board. In a few locations in the mill critical information about mill operations will be written on White Boards. Information such as circuit parameters, required changes in circuit operations, or special instructions about maintenance. Circuit sheets. Circuit sheets will have operating parameters on them along with sampling times for the circuit. They will also have a place for you to pass along written information about your circuit. Verbal. One of the most important times of your shift is at shift change. You have the responsibility to pass along information about your circuit to the person relieving you. You will be given verbal instructions from your supervisor or metallurgical department which you need to be sure you understand. Written. Instructions will be handed out in written form almost daily. As above if you do not understand any instruction ask your supervisor. Health and Safety -Therefore, solids handling must be conducted carefully to limit exposure to radioactivity. Proper Personal Protective Equipment ("PPE") must be worn, and solids should be wetted at all times to prevent dusting. Any solids spills should be washed down before they dry. Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 6 -- Hazards: • • Radioactive Solids • Slow moving rakes in CCD • Heat • • Date: 03-21 Revision: EFR-1 Page 2 of 4 • Hose Pumps will fail if either intake or discharge lines are restricted. Which may spray solutions • Pumps that require gland seal water will fail if the gland seal water is not turned on. Additionally, if the pump is off and the gland seal water is left on it will dilute process solutions and cause problems in the process. Personal Protective Equipment and Clothing 1. Minimum PPE requirements at White Mesa Mill while in the restricted area is hard hats, safety glasses, and steel toed shoes. No ragged or lose fitting clothing is allowed. Body jewelry, rings, wrist watches, etc. are required to be removed while working. Other personal protective equipment includes, but is not limited to: ear plugs, respirators, wet suits, welding helmets, goggles, gloves, and rubber boots. Face shields and safety belts are required in designated areas and/or while performing certain jobs. If in doubt, contact your supervisor. 2 Each employee is responsible for the condition of their protective equipment. Report any defects, etc., to your supervisor. 3 The following equipment is required when working on pipelines or vessels containing acids or caustics: a. Face shield and chemical splash goggles b. Rubber coat and pants c. Rubber gloves and rubber boots d. Other equipment specified by the foreman for that particular job listed on the Safe Work Permit 4 The use of a safety belt and properly adjusted lifeline is required where there is a danger of falling four feet or more, except while performing work under the ladder and scaffold section of this manual. This rule applies when going beyond the handrails of walkways on top of any tanks in the mill area. 5 It is a condition of employment that all personnel who may be required to wear a respirator must be clean shaven to assure that the respirator fits properly. Personnel will be fully trained prior to using respirators. Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 6 -- Date : 03-21 Revision : EFR-1 Page 3 of 4 1. Operators will wear complete PPE as directed by supervisors and the radiation and safety departments. I I I I I I ■ Start-up Procedures I I I I Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 6-- ·-·-Shut Down Procedures Emergency Slmt Down I I I Date: 03-21 Revision: EFR-1 Page 4 of 4 Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Op erating Procedures Book 15 Section 7 --Removal Preface • • • • to separate t . . Communication Date: 01-22 Revision: EFR-1 Page I of 4 To be successful as an operator in achieving the desired results in your circuit, good communication between you, the metallurgical department, and your supervisor should exist. Information is given to the operator verbally, written and by test results. As an operator, if you do not understand any information given, you have the responsibility to ask questions until you do understand. White Board . In a few locations in the mill, critical information about mill operations will be written on White Boards. Information such as circuit parameters, required changes in circuit operations, or special instructions about maintenance. Circuit Sheets. Circuit sheets will have operating parameters on them along with sampling times for the circuit. They will also have a place for you to pass along written information about your circuit. Verbal. One of the most important times of your shift is at Shift Change. You have the responsibility to pass along information about your circuit to the person relieving you. You will be given verbal instructions from your supervisor or metallurgical department which you need to be sure you understand. Written. Instructions will be handed out in written form almost daily. As above, if you do not understand any instruction, ask your supervisor. Health and Safety The solution that is fed to the -removal circuit is rare earth metals. This solution should not be ingested. The -also contains heavy metals and should not be ingested. The organic solution is flammable. No Hot Work will be done in the solvent extraction building without a Hot Work permit. Any possible ignition source must be avoided. The solution used to strip or remove the rare earths from the organic solution is and should be handled appropriately and only when using appropriate Personal Protective Equipment (PPE). generates vapors that should be avoided. These vapors can cause extreme irritation and injury. Hazards: • • • Stairs and elevated work areas • Pressurized solutions pumping throughout the circuit • Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 7 - Personal Protective Equipment (PPE) Date: 01-22 Revision : EFR-1 Page 2 of 4 I . Minimum PPE requirements at White Mesa Mill while in the restricted area is hard hats, safety glasses, and steel toed shoes. No ragged or lose fitting clothing is allowed. Body jewelry, rings, wrist watches, etc. are required to be removed while working. 2 Other personal protective equipment includes, but is not limited to: ear plugs, respirators, wet suits, welding helmets, goggles, gloves, and rubber boots. Face shields and safety belts are required in designated areas and/or while performing certain jobs . If in doubt, contact your supervisor. 3 Each employee is responsible for the condition of their protective equipment. Report any defects, etc., to your supervisor. 4 The following equipment is required when working on pipelines or vessels containing acids or caustics: a. Face shield and chemical splash goggles b. Rubber coat and pants c. Rubber gloves and rubber boots d. Other equipment specified by the foreman for that particular job listed on the Safe Work Permit 5 The use of a safety belt and properly adjusted lifeline is required where there is a danger of falling four feet or more, except while performing work under the ladder and scaffold section of this manual. This rule applies when going beyond the handrails of walkways on top of any tanks in the mill area. 6 It is a condition of employment that all personnel who may be required to wear a respirator must be clean shaven to assure that the respirator fits properly. Personnel will be fully trained consistent with the Mill's Respiratory Protection SOP, prior to using respirators. Equipment and Important Information ■ ■ - Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 7 Raffinate pH One of the most critical aspects of this circuit is I Sampling Date : 01-22 Revision : EFR-1 Page 3 of 4 Sampling of the various solutions in this circuit is required on a regular basis. It is important to ensure that any sample taken is representative of the tank's contents. This means that tanks should be well mixed, sampling equipment should be clean, and any sample ports purged before collecting the sample. Operating Instructions 1. Conduct a proper Shift Change with the person you are relieving. Get information about all circuit parameters, including, but not limited to: flow rates, tank levels, solution concentrations. I I I I I Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 7 - Start-up Procedures I I I I I I I I I Shutdown Procedures Emergency Shutdown Procedures I I I Date : 01-22 Revision: EFR-1 Page 4 of 4 Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Date: 04-221 Revision: EFR-2 Page 1 of 4 Procedures Book 15 Section 8 - Preface As always, wearing appropriate Personal Protective Equipment ("PPE") and following all safety procedures must be done at all times. Communication: To be successful as an operator in achieving the desired results in your circuit good communication between you, the metallurgical department, and your supervisor should exist. Information is given the operator verbally, written, and by test results. As an operator if you do not understand any information given you have the responsibility to ask questions until you do understand. White board. In a few locations in the mill critical information about mill operations will be written on White Boards. Information such as circuit parameters, required changes in circuit operations, or special instructions about maintenance. Circuit sheets. Circuit sheets will have operating parameters on them along with sampling times for the circuit. They will also have a place for you to pass along written information about your circuit. Verbal. One of the most important times of your shift is at shift change. You have the responsibility to pass along information about your circuit to the person relieving you. You will be given verbal instructions from your supervisor or metallurgical department which you need to be sure you understand. Written. Instructions will be handed out in written form almost daily. As above if you do not understand any instruction ask your supervisor. Hazards: • • Elevated work areas • Pressurized process lines • Hose pumps will fail if either intake or discharge lines are restricted. Which may spray solutions. • Pumps that require gland seal water will fail if the gland seal water is not turned on. Additionally, if the pump is off and the gland seal water is left on it will dilute process solutions and cause problems in the process. Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 8 - Personal Protective Equipment and Clothing Date : 04-22 l Revision: EFR-2 Page 2 of 4 1. Minimum PPE requirements at White Mesa Mill while in the restricted area is hard hats, safety glasses, and steel toed shoes. No ragged or lose fitting clothing is allowed. Body jewelry, rings, wrist watches, etc. are required to be removed while working. 2 Other personal protective equipment includes, but is not limited to : ear plugs, respirators, wet suits, welding helmets, goggles, gloves, and rubber boots. Face shields and safety belts are required in designated areas and/or while performing certain jobs. If in doubt, contact your supervisor. 3 Each employee is responsible for the condition of their protective equipment. Report any defects, etc., to your supervisor. 4 The following equipment is required when working on pipelines or vessels containing acids or caustics: a. Face shield and chemical splash goggles b. Rubber coat and pants c. Rubber gloves and rubber boots d. Other equipment specified by the foreman for that particular job listed on the Safe Work Permit 5 The use of a safety belt and properly adjusted lifeline is required where there is a danger of falling four feet or more, except while performing work under the ladder and scaffold section of this manual. This rule applies when going beyond the handrails of walkways on top of any tanks in the mill area. 6 It is a condition of employment that all personnel who may be required to wear a respirator must be clean shaven to assure that the respirator fits properly. Personnel will be fully trained prior to using respirators. - Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures • Book 15 Section 8 - Date : 04-221 Revision : EFR-2 Page 3 of 4 IMPORTANT : This pump is a hose (peristaltic) pump . This type of pump builds high pressures. The feed and discharge line and valves must be open before the pump is turned on or the discharge line or pump will fail. - Sampling Sampling of the is required on a regular basi s. It is important to ensure that any samples taken are representative of the tank's contents. This means using clean sampling equipment and purge sample ports before sampling. Operating ln tructions 1. Conduct a proper Shift Change with the person you are relieving . Get information about all circuit parameters, including, but not limited to : temperature, feed flow rate, and tank levels. 2. Perform a pre-work exam of the precipitation circuit. Look at all lines (feed and over flow lines, steam lines, etc.) for any leaks. Check all walkways and travel s areas for general cleanliness. Ensure all process control s , readouts and safety showers are functioning properly. 3. Check the process parameters targets. Remember that process parameters may have changed since the previous shift. 4. Check and record all flow rates and tank levels. I I I Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book I 5 Section 8 - I Start-up Procedures I I I I I Shutdown Procedures I I I I I Emergency Shut-down Procedures I I I Date: 04-221 Revision: EFR-2 Page 4 of 4 Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Date : 04-22 Revision: EFR-2 Pagel of 4 Book 15 Section 9 -- Preface Communication: To be successful as an operator in achieving the desired results in your circuit good communication between you, the metallurgical department, and your supervisor should exist. Information is given the operator verbally, written, and by test results. As an operator if you do not understand any information given you have the responsibility to ask questions until you do understand. White board. In a few locations in the mill critical information about mill operations will be written on White Boards. Information such as circuit parameters, required changes in circuit operations, or special instructions about maintenance. Circuit sheets. Circuit sheets will have operating parameters on them along with sampling times for the circuit. They will also have a place for you to pass along written information about your circuit. Verbal. One of the most important times of your shift is at shift change. You have the responsibility to pass along information about your circuit to the person relieving you. You will be given verbal instructions from your supervisor or metallurgical department which you need to be sure you understand. Written. Instructions will be handed out in written form almost daily. As above if you do not understand any instruction ask your supervisor. Hazards: • Pinch points • Moving equipment • High pressure lines • Pumps, if hose pumps are restricted on either the intake or discharge the hose will fail spraying solution. • Pumps, pumps requiring gland seal water if the gland seal water is not turned on the pump will fail. If the pump is off and the gland seal water is left on it will dilute process solutions and cause problems in the process. Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 9 -- Personal Protective Equipment and CJothing Date : 04-22 Revision: EFR-2 Page 2 of 4 1. Minimum PPE requirements at White Mesa Mill while in the restricted area is hard hats, safety glasses, and steel toed shoes. No ragged or lose fitting clothing is allowed. Body jewelry, rings, wrist watches, etc. are required to be removed while working. 2 Other personal protective equipment includes, but is not limited to: ear plugs, respirators, wet suits, welding helmets, goggles, gloves, and rubber boots. Face shields and safety belts are required in designated areas and/or while performing certain jobs. If in doubt, contact your supervisor. 3 Each employee is responsible for the condition of their protective equipment. Report any defects, etc., to your supervisor. 4 The following equipment is required when working on pipelines or vessels containing acids or caustics: a. Face shield and chemical splash goggles b. Rubber coat and pants c. Rubber gloves and rubber boots d. Other equipment specified by the foreman for that particular job listed on the Safe Work Permit 5 The use of a safety belt and properly adjusted lifeline is required where there is a danger of falling four feet or more, except while performing work under the ladder and scaffold section of this manual. This rule applies when going beyond the handrails of walkways on top of any tanks in the mill area. 6 It is a condition of employment that all personnel who may be required to wear a respirator must be clean shaven to assure that the respirator fits properly. Personnel will be fully trained prior to using respirators. Equipment 1. Pumps- a. The feed pump is a centrifugal slurry pump. The feed pump transfers slurry from the precip aging tank to the 2. Piping- a. Process piping is HOPE b. Plant Air is steel c. Plant water is HOPE. 3. Valves - a . Isolation valves are manual butterfly type. Isolation valves are for flow direction control as well as isolation for maintenance. b. The feed control valve is for flow control to the - 4 . Instrumentation - I Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 9 -- I -■ ·-I Operating Instructions (Automatic): Date: 04-22 Revision: EFR-2 Page 3 of 4 1. Conduct a proper shift change with the person you are relieving. Gather information on the status and operation of the equipment as well as batches processed. 2. Prior to operating the equipment conduct a pre shift inspection. I I I I I I I I I I ■-I Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 9-- ShutDown I I I i -I Date: 04-22 Revision: EFR-2 Page4 of 4 Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 10 -Packaging Packagin& Preface Date: 04-22 Revision: EFR-2 Page 1 of2 The purpose of the bulk bag filling system is to prepare and package the finished product for shipping. Prior to packaging, ensure there are bulk bags available. Prior to operating the packaging circuit, make sure the packaging unit has been serviced and cleaned and that the scale has been zeroed out. Ensure the 480 volt power has been turned on and a clean, dry air supply is available to the packaging unit. Communication: To be successful as an operator in achieving the desired results in your circuit good communication between you, the metallurgical department, and your supervisor should exist. Information is given the operator verbally, written, and by test results. As an operator if you do not understand any information given you have the responsibility to ask questions until you do understand. White board. In a few locations in the mill critical information about mill operations will be written on White Boards. Information such as circuit parameters, required changes in circuit operations, or special instructions about maintenance. Circuit sheets. Circuit sheets will have operating parameters on them along with sampling times for the circuit. They will also have a place for you to pass along written information about your circuit. Verbal. One of the most important times of your shift is at shift change. You have the responsibility to pass along information about your circuit to the person relieving you. You will be given verbal instructions from your supervisor or metallurgical department which you need to be sure you understand. Written. Instructions will be handed out in written form almost daily. As above if you do not understand any instruction ask your supervisor. Hazards: • Pinch points • Moving equipment • Heavy product bags Personal Protective Equipment and Clothine 1. Minimum Personal Protective Equipment ("PPE") requirements at White Mesa Mill while in the restricted area is hard hats, safety glasses, and steel toed shoes. No ragged or lose fitting clothing is allowed. Body jewelry, rings, wrist watches, etc. are required to be removed while working. Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 10 -Packaging Date: 04-22 Revision: EFR-2 Page 2 of2 2 Other personal protective equipment includes, but is not limited to: ear plugs, respirators, wet suits, welding helmets, goggles, gloves, and rubber boots. Face shields and safety belts are required in designated areas and/or while performing certain jobs. If in doubt, contact your supervisor. 3 Each employee is responsible for the condition of their protective equipment. Report any defects, etc., to your supervisor. 4 The following equipment is required when working on pipelines or vessels containing acids or caustics: a. Face shield and chemical splash goggles b. Rubber coat and pants c. Rubber gloves and rubber boots d. Other equipment specified by the foreman for that particular job listed on the Safe Work Permit 5 The use of a safety belt and properly adjusted lifeline is required where there is a danger of falling four feet or more, except while performing work under the ladder and scaffold section of this manual. This rule applies when going beyond the handrails of walkways on top of any tanks in the mill area. 6 It is a condition of employment that all personnel who may be required to wear a respirator must be clean shaven to assure that the respirator fits properly. Personnel will be fully trained prior to using respirators. Procedure From here the bag liner is sealed up and the fill spout is tied closed. This bag is now moved to the shipping prep area to be loaded on containers and shipped out. Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 11 - Rare Earth Preface Communication Date : 03-23 Revision: EFR-1 Page 1 of3 To be successful as an operator in achieving the desired results in your circuit, good communication between you, the metallurgical department, and your supervisor should exist. Information is given to the operator verbally, written and by test results. As an operator, if you do not understand any information given, you have the responsibility to ask questions until you do understand. White Board. In a few locations in the mill, critical information about mill operations will be written on White Boards. Information such as circuit parameters, required changes in circuit operations, or special instructions about maintenance. Circuit Sheets. Circuit sheets will have operating parameters on them along with sampling times for the circuit. They will also have a place for you to pass along written information about your circuit. Verbal. One of the most important times of your shift is at Shift Change. You have the responsibility to pass along information about your circuit to the person relieving you. You will be given verbal instructions from your supervisor or metallurgical department which you need to be sure you understand. Written. Instructions will be handed out in written form almost daily. As above, if you do not understand any instruction, ask your supervisor. Health and Safetv Hazards: • • Elevated temperatures • Elevated work areas • Pressurized process lines • Pumps, if hose pumps are restricted on either the intake or discharge the hose will fail spraying solution. • Pumps, pumps requiring gland seal water if the gland seal water is not turned on the pump will fail. If the pump is off and the gland seal water is left on it will dilute process solutions and cause problems in the process. Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 11 Personal Protective Equipment (PPE) Date: 03-23 Revision: EFR-1 Page 2 of3 l . Minimum PPE requirements at White Mesa Mill while in the restricted area is hard hats, safety glasses, and steel toed shoes. No ragged or lose fitting clothing is allowed. Body jewelry, rings, wrist watches, etc. are required to be removed while working. 2. Other personal protective equipment includes, but is not limited to: ear plugs, respirators, wet suits, welding helmets, goggles, gloves, and rubber boots. Face shields and safety belts are required in designated areas and/or while performing certain jobs. If in doubt, contact your supervisor. 3. Each employee is responsible for the condition of their protective equipment. Report any defects, etc., to your supervisor. 4. The following equipment is required when working on pipelines or vessels containing --a. Face shield and chemical splash goggles b. Rubber coat and pants c. Rubber gloves and rubber boots d. Other equipment specified by the foreman for that particular job listed on the Safe Work Permit 5. The use of a safety belt and properly adjusted lifeline is required where there is a danger of falling four feet or more, except while performing work under the ladder and scaffold section of this manual. This rule applies when going beyond the handrails of walkways on top of any tanks in the mill area. 6. It is a condition of employment that all personnel who may be required to wear a respirator must be clean shaven to assure that the respirator fits properly. Personnel will be fully trained consistent with the Mill's Respiratory Protection SOP, prior to using respirators. Equipment and Important Information IMPORT ANT : This pump is a hose (peristaltic) pump. This type of pump builds high pressures . The feed and discharge line and valves must be open before the pump is turned on or the discharge line or pump will fail. Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 1 S Section I I -It is important to ensure that any samples taken are representative of the tank's contents. This means using clean sampling equipment and purging sample ports before sampling. Operating Instructions 1. Conduct a proper Shift Change with the person you are relieving. Get information about all circuit parameters, including, but not limited to: temperature, feed flow rate, and tank levels. Start-up Procedures I I I I Shutdown Procedures I I Emergency Shut-down Procedures I I I Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 12 - Preface Communication Date: 03-23 Revision: EFR-1 Page 1 of 4 To be successful as an operator in achieving the desired results in your circuit, good communication between you, the metallurgical department, and your supervisor should exist. Information is given to the operator verbally, written and by test results. As an operator, if you do not understand any information given, you have the responsibility to ask questions until you do understand. White Board. In a few locations in the mill, critical information about mill operations will be written on White Boards. Information such as circuit parameters, required changes in circuit operations, or special instructions about maintenance. Circuit Sheets. Circuit sheets will have operating parameters on them along with sampling times for the circuit. They will also have a place for you to pass along written information about your circuit. Verbal. One of the most important times of your shift is at Shift Change. You have the responsibility to pass along information about your circuit to the person relieving you. You will be given verbal instructions from your supervisor or metallurgical department which you need to be sure you understand. Written. Instructions will be handed out in written form almost daily. As above, if you do not understand any instruction, ask your supervisor. Health and Safetv Hazards: • • • Stairs and elevated work areas • • Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 12 - Personal Protective Equipment (PPE) Date: 03-23 Revision: EFR-1 Page 2 of4 1. Minimum PPE requirements at White Mesa Mill while in the restricted area is hard hats, safety glasses, and steel toed shoes. No ragged or lose fitting clothing is allowed. Body jewelry, rings, wrist watches, etc. are required to be removed while working. 2. Other personal protective equipment includes, but is not limited to: ear plugs, respirators, wet suits, welding helmets, goggles, gloves, and rubber boots. Face shields and safety belts are required in designated areas and/or while performing certain jobs. If in doubt, contact your supervisor. 3. Each employee is responsible for the condition of their protective equipment. Report any defects, etc., to your supervisor. 4. The following equipment is required when working on pipelines or vessels containing acids or caustics: a. Face shield and chemical splash goggles b. Rubber coat and pants c. Rubber gloves and rubber boots d. Other equipment specified by the foreman for that particular job listed on the Safe Work Permit 5. The use of a safety belt and properly adjusted lifeline is required where there is a danger of falling four feet or more, except while performing work under the ladder and scaffold section of this manual. This rule applies when going beyond the handrails of walkways on top of any tanks in the mill area. 6. It is a condition of employment that all personnel who may be required to wear a respirator must be clean shaven to assure that the respirator fits properly. Personnel will be fully trained consistent with the Mill's Respiratory Protection SOP, prior to using respirators. Equipment and Important Information Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 12 -- I I -Sampling Sampling of the various solutions in this circuit is required on a regular basis. It is important to ensure that any sample taken is representative of the tank's contents. This means that tanks should be well mixed, sampling equipment should be clean, and any sample ports purged before collecting the sample. Operating Instructions 1. Conduct a proper Shift Change with the person you are relieving. Get information about all circuit parameters, including, but not limited to: flow rates, tank levels, solution concentrations. 2. Perform a pre-work exam of the Inspect all lines and tanks for any leaks. Check all walkways and travel areas for general cleanliness. Ensure all process controls, readouts and safety showers are functioning properly . Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 12 - Date: 03-23 Revision: EFR-1 Page 4 of4 3. Check the process parameter targets. Remember that process parameters may have changed since the previous shift. 4. Check and record all flow rates and tanks levels on the Operator Sheet. 5. Ensure that the bench pH probe is calibrated and functional. I I 8. Adjust the recycle valves to achieve the specified organic to aqueous ratio in the mixers. 9. Sample the circuit as directed by the Metallurgical Department. Start-up Procedures Shutdown Procedures I I I I I I I I I Emergency Shutdown Procedures I I Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 13 - Preface Communication Date: 03-23 Revision: EFR-1 Page I of 4 To be successful as an operator in achieving the desired results in your circuit, good communication between you, the metallurgical department, and your supervisor should exist. Information is given to the operator verbally, written and by test results. As an operator, if you do not understand any information given, you have the responsibility to ask questions until you do understand. White Board. In a few locations in the mill, critical information about mill operations will be written on White Boards. Information such as circuit parameters, required changes in circuit operations, or special instructions about maintenance. Circuit Sheets. Circuit sheets will have operating parameters on them along with sampling times for the circuit. They will also have a place for you to pass along written information about your circuit. Verbal. One of the most important times of your shift is at Shift Change. You have the responsibility to pass along information about your circuit to the person relieving you. You will be given verbal instructions from your supervisor or metallurgical department which you need to be sure you understand. Written. Instructions will be handed out in written form almost daily. As above, if you do not understand any instruction, ask your supervisor. Health and Safetv Hazards: • • • Stairs and elevated work areas • • Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 13 - Personal Protective Equipment (PPE) Date: 03-23 Revision: EFR-1 Page 2 of4 1. Minimum PPE requirements at White Mesa Mill while in the restricted area is hard hats, safety glasses, and steel toed shoes. No ragged or lose fitting clothing is allowed. Body jewelry, rings, wrist watches, etc. are required to be removed while working. 2. Other personal protective equipment includes, but is not limited to: ear plugs, respirators, wet suits, welding helmets, goggles, gloves, and rubber boots. Face shields and safety belts are required in designated areas and/or while performing certain jobs. If in doubt, contact your supervisor. 3. Each employee is responsible for the condition of their protective equipment. Report any defects, etc., to your supervisor. 4. The following equipment is required when working on pipelines or vessels containing acids or caustics: a. Face shield and chemical splash goggles b. Rubber coat and pants c. Rubber gloves and rubber boots d. Other equipment specified by the foreman for that particular job listed on the Safe Work Permit 5. The use of a safety belt and properly adjusted lifeline is required where there is a danger of falling four feet or more, except while performing work under the ladder and scaffold section of this manual. This rule applies when going beyond the handrails of walkways on top of any tanks in the mill area. 6. It is a condition of employment that all personnel who may be required to wear a respirator must be clean shaven to assure that the respirator fits properly. Personnel will be fully trained consistent with the Mill's Respiratory Protection SOP, prior to using respirators. Equipment and Important Information Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 13 -- I I -Sampling Sampling of the various solutions in this circuit is required on a regular basis. It is important to ensure that any sample taken is representative of the tank's contents. This means that tanks should be well mixed, sampling equipment should be clean, and any sample ports purged before collecting the sample. Operating Instructions 1. Conduct a proper Shift Change with the person you are relieving. Get information about all circuit parameters, including, but not limited to: flow rates, tank levels, solution concentrations . 2. Perform a pre-work exam of the Inspect all lines and tanks for any leaks. Check all walkways and travel areas for general cleanliness. Ensure all process controls, readouts and safety showers are functioning properly. Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 13 - Date: 03-23 Revision: EFR-1 Page 4 of4 3. Check the process parameter targets. Remember that process parameters may have changed since the previous shift. 4. Check and record all flow rates and tanks levels on the Operator Sheet. 5. Ensure that the bench pH probe is calibrated and functional. I I I 9. Sample the circuit as directed by the Metallurgical Department. Start-up Procedures I I I I I I I I I Shutdown Procedures I I I I I I I I I Emergency Shutdown Procedures I I I ATTACHMENT 2 SERP 2022-01 -REDACTED Withold from Public Disclosure Under Utah Code 638-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information REPORT ENERGY FUELS RESOURCES (USA) INC. WHITE MESA URANIUM MILL SAFETY AND ENVIRONMENTAL REVIEW PANEL MEETING OF JANUARY 27, 2022 SOPs fo~ Removal During Uranium Rare Earth Ore Recovery SERP No. 2022-01 Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information ENERGY FUELS RESOURCES (USA) INC. WHITE l\ffiSA URANIUM MILL SAFETY AND ENVIRONl\ffiNTAL REVIEW PANEL MEETING OF JANUARY 27, 2022 SERP NO. 2022-01 1. PURPOSE The Energy Fuels Resources (USA) Inc. ("EFRI") Safety and Environmental Review Panel ("SERP") for the White Mesa Uranium Mill (the "Mill") met by telephone conference on January 27, 2022 in accordance with SERP procedures in While Mesa Mill Standard Operating Procedure PBL-1, Rev. No. R-6 (the "SERP SOP"), to consider SERP No. 2022-01, regarding the following (the "Change"): Review and approve a proposed extractant and Standard Operating Procedure ("SOP") for removal of -from Rare Earth - product ("RE-') using existing Mill equipment. The SERP followed the SERP SOP as it performed this SERP evaluation, to ensure that the change is consistent with the following three criteria (the "SERP Approval Criteria"): (a)The change, test or experiment did not conflict with any requirement specifically stated in the Mill license, and did not impair EFRI's ability to meet all applicable regulations; (b)There would be no degradation in the essential safety or environmental commitments in the license applicalion, or provided by the approved reclamation plan; and (c)The change, lest or experiment was consistent with lhe conclusions of actions analyzed and selected in the most recent Environmental Assessment (EA) conducted by the Division of Waste Management and Radiation Control ("DWMRC") from the last license renewal and/or major license amendment. 2. OVERVIEW AND BACKGROUND EFRI plans to reuse existing circuit equipment to remove -from rare earth ("RE") ~roducts. The Mill produces R~ by proces ing rare earth bearing uranium ("REU") ores. The propo ed Change, i.e., U1e removal o _, will allow the Mill to test the capability to and will also reduce the radionuclide content of RE products by reducing the levels o which will followth~ The proposed proces involves the use of an extractant from one or more of the classes of referred to as Page 2 Withold from Public Disclosure Under Utah Code 638-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information as extractants in its solvent extraction ("SX"). The classes of to be used in connection with this Change are comparable to those previously used in the Mill. The proposed proces will also use an additional quantity of one of the fiberglass tanks in the vanadium SX area, which has been converted for use in -removal. In addition to the proposed materials, the SERP evaluated the SOP, which addressed the operation described above. The proposed process is referred to in this report as the process, or the "Change." The SERP evaluated the process with respect to the requirements of condition 9.4 of the Mill's RML, worker safety, process safety, and environmental protection. 3. SERP MEMBERSHIP AND QUALIFICATIONS This SERP consisted of the following members : Resoonsibilitv Name/Position Corporate Radiation Safety Officer or Garrin Palmer equivalent; Mill Radiation Safety Officer (Member) Assuring Tests conform to radiation safety and environmental requirements Management Expertise; David Frydenlund Responsibility for managerial and financial Chief Financial Officer, General Counsel approvals and Corporate Secretary (Member) Operations and/or Construction Logan Shumway Management; Mill Manager (Member) Responsibility for implementing operational procedures Responsibility for regulatory compliance at Kathy W einel WMM Director, Regulatory Compliance Corporate responsibility for regulatory Scott Bakken compliance Vice President, Re_gulatory Affairs Independent Safety/Environmental Jo Ann Tischler Evaluation Independent Chemical Engineering Consultant Page 3 3 Withold from Public Disclosure Under Utah Code 638-2-101 et seq . and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information In addition, the following Mill or Corporate Personnel attended the SERP : Reason for Attendance Name/Position Regulatory and Legal Support to General Julia Hoffmeier Counsel Corporate Counsel Corporate Secretary 4. SERP REVIEW OF PROPOSED CHANGE AND SOP and Assistant The SERP reviewed specific details relating to the process, including the SOP and the independent consultant's Technical Memorandum. A copy of the SOP and the Technical Memorandum are provided in Attachments to this report. Specific points discussed are summarized below. The SERP reviewed all processing steps, and identified those procedures that did not need to be included in the processing SOP, or materials, specifically,., that did not need to be re-addressed because they have been approved separately. The SERP also reviewed the Document Control SOP, in place since 2000, which requires that any new SOP, or any significant change to an existing SOP, requires a SERP review. 5. REVIEW OF SERP APPROVAL CRITERIA 5.1. Review of the Criteria In order for a change in the facility or process, as presented in the license application, to be eligible for approval by the SERP, the three SERP Approval Criteria, detailed in Section 1 above, must be satisfied. The three SERP Approval Criteria, as detailed in the five steps of the SERP procedure, were reviewed and discussed, as folJows: 5. I .1. Does the change conflict with any requirement specifically stated in the license? The SOPs will not require any types of process operations not currently performed at the Mill. Processes such as solvent extraction and product stripping, have been regularly performed at the Mill. The SOPs will not require any new equipment. Existing equipment in the vanadium circuit will be converted (re-used) periodically for the -removal step in RE -recovery as needed, and returned to other service when needed. Storage of chemicals will not require constriction of new tanks or storage areas. The Change will not require use of electricity, fuel, or water resources beyond levels anticipated in the license for full Mill production. Use of the -and extractants will not require any worker protections beyond those currently in use in other Mill operations. Page4 Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information Based on the above, the SERP determined that the Change does not conflict with any requirement stated in the license or any license requirement contained in any license tie- down letters. Therefore, this criterion is met. The purified and concentrated yellowcake that will be produced will not cause the Mill to exceed the yellowcake production limit under the License. 5.1.2. Does the change impair EFRI's ability to meet all applicable regulations? No. The SERP identified that there are no RCRA CERCLA, or TSCA requirements applicable to the REU ore or proposed process chemicals. The chemicals and proposed process as described in the SOPs will not generate any new air emissions or require revision to the Air Approval Order ("AO"). Approval Order DAQE-ANl 12050020-19 on December 23, 2021. Utah DWMRC identified in the 2004 Statement of Basis for the Mill's Groundwater Discharge Permit that the Mill bas previously u. e and did not require that compounds or degradation products be monitored in groundwater or Mill tailings. Existing spill management procedures will be sufficient for the proposed process chemicals. The SERP noted that there are no EPCRA reporting quantities for any of the extractants in the classes considered. The Spill Prevention Control and Countermeasures ("SPCC") plan tables will be updated as appropriate for these materials. 5.1.3. ls the change consistent with the conclusions of actions analyzed in the most current EA? The original 1980 Environmental Assessment, subsequent environmental reports, and the DWMRC Technical and Environmental Report for the Mill contemplated that the Mill would recover secondary metals, in addition to uranium. The original EA contemplated recovery of copper and/or vanadium. The Mill has also previously been approved to recover, and has modified the process to recover, tantalum and niobium. The process will not generate any new tailings constituents not already monitored or addressed by other indicator parameters in the groundwater discharge permit ("GWDP"). The process will produce no new or increased air emissions. The tailings to be generated will be comparable to, and contain comparable non-radiological constituents, as the tailings previously generated and managed in the tailings management system. The Change will not introduce any new radionuclides. The process will involve levels of radiological constituents, comparable to other feed materials previously processed. Page 5 Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information The Mill has previou sly used compounds as extractants in the SX . The classes of extractants approved in this Change are comparable to those previously used in the Mill. 5.1.4. Does the change require any adjustment to the financial surety arrangement or approved amount? The SERP determined that there would be no change to any criterion that would affect the Mill's surety. There would be no change to the footprint of the Mill. There would be no increased volume of equipment to be disposed in the tailings management system at reclamation. The Change will not measurably increase the quantity of materials discharged to the tailings system, relative to the RE process. There will be no new equipment required. The volume of the equipment to be used for the process were anticipated within the licensed tailings capacity. The composition of tailings from the proposed process will not require any change to the cover design as noted in the September 9, 2020 letter to DWMRC. The quantity of removed and discharged -will be minimal and will not require any special management or changes to the tailings reclamation plan. 5.1.5. Does the change create any degradation in the essential safety or environmental commitments in the license application, or provided by the approved reclamation plan? The SERP assessed that there would be no change in the safety or environmental commitments in the license application or reclamation plan . Processing according to the SOP is not expected to produce any environmental impacts beyond those assessed in any EA, and is consistent with the conclusions regarding actions analyzed in the EAs. As a result, this criterion is also satisfied. Processing according to the SOP will: • Not produce any increased levels of radionuclides in processes or wastes beyond those anticipated in the EAs or previously managed under approved SOPs, • Not introduce any constituents to the tailings system that arc detrimental to the tailings solutions or tailings Jiner, • Not produce any new emissions or pathways for exposure to workers or the public, • Not require any changes to spill control or storm water management plans or drainage designs, • Not require additional tailings capacity or changes to tailings management plans, and • Not introduce any new pathways of contamination to the environment. Page 6 Withold from Public Disclosure Under Utah Code 638-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information Processing according to the SOP is within the envelope of conditions evaluated in the Mill's MILDOS model for dose to off-site receptors. Processing according to the SOP will have no effect on the commitments or quantities addressed in the Reclamation Plan. 6. CONCLUSIONS The SERP concluded that the proposed Change and SOP meet the criteria set forth in the SERP SOP for approval, and approved the SOP and extractants. The SERP authorized immediate implementation of the SOP . 7. ATTACHMENTS • Attachment 1 -Technical Memorandum of J. Tischler January 27, 2022 • Attachment 2-SOP fo-Removal Page 7 U Withold from Public Disclosure nder Utah Code 63G -2-101 t and as indi t d • e seq . All redactions wer~b:s~~ the ~edacted !ext below. on Bl/Proprietary Information SIGNATURES Report reviewed by: ~~ Scott Bakken Dute:~.,x_-:z_ _______ _ LVS}mmway c::::_:y= GamnPalmer Page 8 Withold from Public Disclosure Under Utah Code 638-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information ATTACHMENT l Technical Memorandum of Jo Ann Tischler January 27, 2022 01.27.2022 To: S . Bakken, D Frydenlund, L. Shumway, K. Weinel From: Jo Ann Tischle r Cc: Re: Technical Review of Propo~ed Rare Earth -Process SOPs -for SERP Evaluation Withold from Public Disclosure Under Utah Code 638-2-101 et seq . and as indicated in the redacted text below . All redactions were based on CBI/Proprietary Information Technical Memorandum Introduction This Technical Memorandum (the "Memorandum") describes the results of the evaluation of a proposed Change and associated Standard Operating Procedures ("SOPs") al the White Mesa Mill (the "Mill") for reuse of existing equipment to re mo v from rare earth ("RE") -products . The Mill produces RE by processing rare earth bearing uranium ("REU") ores. The proposed Change, i.e., th e removal of -will allow the Mill to test the capability to separate individual RE ·, and will also reduce the radionuclide content of RE products by reducing the levels of T his evaluation will consider both classes o f compound,, since th e compounds in both classes have very similar properties, and since the Mill may test one or more compounds from either class to id e nLi fy the optimum extraclant. The initial co mp o un d lo be used will be The Mill has previously used solvent extraction ("SX") circuits. cxtractants to be used in connection with this Change are comparabJe to those previously used in the Mill. The proposed process will also use an additional quantity of , which is used in current RE recovery process. This Memorandum assesses whether the process may pose any worker safety or environmental hazards, or be inconsistent with conditions and assumptions in the Mill's current State of Utah Radioactive Materials License No . UTI900479 (the ;'RML" or the "license") or other regulations. This evaluation was performed as part of a SERP evaluation of this potential Change or test under the RML and the Mill SOPs. The proposed_ removal process and materials will be referred to in this memo, for the purposes of SERP evaluation, as the "proposed process" or "Change." In order for a Change or test in the facility or process, as presented in the license application, 10 be eligible for approval by the SERP, three SERP Approval Criteria must be satisfied. This memorandum provides information needed to answer the three SERP criteria as follows: I. Does the Change conflict with any requirement specifically stated in the license, or impair Energy Fuels Resourct!s (USA) Inc.'s ("EFRI's") ability lo meet all applicable regulations? 2 . Does the Change create any degradation in the essential safety or environmental commitments in the license application, or provided by the approved reclamation plan? ischler Consulting Services , LLC J)fc Tel 303-501 -9226 8015 South Krameria Way Centennial, CO 80112 japmst55@gmail.com 01.27.2022 Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information Technical Memorandum Pg.02 3. The change, test or experiment was consistent with the conclusions of actions analyzed and selected in the most recent Environmental Assessment (EA) conducted by the Division of Waste Management and Radiation Control ("DWMRC") from the last license renewal and/or major license amendment The following report provides an evaluation of potential safety and environmental hazards, of consistency with the RML, and provides information for comparison to the SERP criteria. To perform this evaluation, we have considered the following questions: 1. What, if any, new chemicals or reagents will be required for the proposed process? 2. Are there any new or different environmental or safety issues associated with the storage, use, handling, or disposal of the new chemicals or reagents? 3. Would use or new chemicals or reagents create any additional requirements for spill or emergency response equipment or training? 4. Would the use of new chemicals or reagents create any additional environmental emissions? 5. Are the existing and the proposed SOPs appropriate and sufficient for the reagents to be used? 6. ls the implementation of the proposed process and SOPs consistent with the Mill's RML, RML application, other permits, and plans? 7. Does the implementation of the proposed process and SOPs conflict with any EFRI environmental or safely commitment made in any other plan or document? 8. Do any of the following requirements apply to the materials proposed to be used or produced in this Change: • Resource Conservation and Recovery Act ("RCRA"), • Toxic Substances Control Act ( "TSCA"), or • Comprehensive Environmental Response, Compensation and Liability Act/Superfund Amendment and Reauthorization Act ("CERCLNSARA") • Clean Air Act ("CAA") and regulations in Utah Administrative Code R307- 401 01.27.2022 Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information Technica l Memorandum 1.0 Basis and Limitations of this Evaluation The evaluation in Lhis report is based on the following documents: • Schematic process flow information provided by Mill personnel. Pg.03 • Safety Data Sheets ("SDSs") for the proposed matc1ials, provided by Mill personnel, and internet access • Communications with Mill personnel during January and February 2022. • Additional technical references listed at the end of this memorandum. 2.0 Description of Proposed Change and SOPs A potential flow configuration for the proposed Change is depicted in the schematic flow diagram in the attached Figure I. The proposed Change would involve reuse of existing equipment within the existing buildings/footprint of the Mill for the removal of -from the RE -with no significant changes at this time. The Mill has processed REU to produce mixed RE _since the second quarter of 2021 . The REV process was described and evaluated in SERP 2021-0 I. Since its inception, the REV process included steps for the removal of the following radionuclides: • uranium and thorium, which are advanced to the uranium circuit for uranium recovery, and • radium, which is currently transferred to the TMS. The proposed change involves adding a comparable step following the radium removal, lo re move on e r::i re earth -fr om 1h e mi xe d rar eanh -prod uc t. To operate the -removal step, the following reagents will be used: • I• -will be prepared at amb ie nt tem pera ture in one of the rubber-lined steel leach tanks by dilution of th e as purc ha. ed form the supplier. The -will be transfen-ed to one of the fiberglass tanks in the vanadium SX area, which has been converted for use in -removal. Calculations discussed in this evaluation are based on an assumed case of pr oc s. in g tons per year of REU ore. On this basis, up to -pet year of the trace levels o-would be removed and transferred to tailings. Regardless of the 01.27.2022 Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information Technical Memorandum Pg.04 ore source, the proposed throughput will not cause the Mill to exceed the RML limit of 4,380 tons of yellowcake production per year. As a result of the proposed process: • There will be no change to the uranium drying or packaging areas, • Existing equipment in the vanadium circuit will be converted (re-used) periodically fo r the -re moval . te p in RE -re cove ry as nee ded , a nd return ed to other service when needed, • approved by Air Approval Order DAQE-AN 11 20 002 0-19 on Dece mb e r 23, 2021. • Vanadium recovery cannot be conducted in the same time period as rare earth -recovery. • There will be no change to the vanadium drying or packaging areas. These areas will not be used for R~ recovery. 3.0 Properties of Proposed Chemicals and Reagents As mentioned above, the proposed either of two classes of compounds: These two classes differ as follows: Parameter 2 2 type -formula - In the table above, "R" represents an 3 2 -- As can be seen from the table, the two classes differ in the number of oxygen atoms associated with the central -atom, and can differ in the size ofth (number 01.27.2022 Withold from Public Disclosure Under Utah Code 638-2-101 et seq . and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information Technical Memorandum Pg.05 of As a result, they have very simi Jar chemical prope,ties and can be considered collectively . The physical state of the potential extractants is discussed in Section 4.0 below. Hazardous properties are discussed in Sections 4.0 and 5.0, below. Each of the remaining additives is discussed in the TechnicaJ and Regulatory Review in Attachment 1. All other chemicals will be those historically used in ore processing, with no other changes. 4.0 Proposed Storage and Use of Chemicals and Reagents The storage location, and the storage and use quantities of additives for the proposed process are detailed in the Technical and Regulatory Review in Attachment I. For ease of reference, storage locations of proposed additives are summarized below. New Additive or Product Form Storage & Use Location Incompatibilities - approved under the most recent Air Approval Order. The tanks have been constructed near the pre-leach thickener northwest of the counter-cun-ent decantation ("CCD") area of the main Mill building, and will be loaded by periodic deliveries from bulk tank trucks. closed area within the particular circuit or building where it will be used near the location where it will be introduced into the circuil, or possibly in the additional covered outdoor storage area referred to as the "manger," or both. The extractant 01.27.2022 Withold from Public Disclosure Under Utah Code 63G-2-101 et seq . and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information Technical Memorandum Pg.06 will be received in plastic drums or plastic totes, and will be charged via plastic pumps and piping in to the fiberglass SX equipment. Any remaining extractant not charged into the system will be stored in the drums or totes in which it was received. Up to - may remain stored in drums or totes . Regardless of how the additive is introduced into the process, each additive will leave the system only when discharged periodically to the tailings management system (''TMS"), or when vessels are emptied for transition back to other uses. 4.1 Compatibility of-Removal Chemicals with Mill Process and Equipment are not corrosive to metals, as identified in their SDSs . The Mill plans corrosion monitoring as indicated below . • --routine monitoring -similar to tanks in sulfuric acid service. • --no additional corrosion monitoring required. id Tncom atibilities Combustion Products Reactivit Stability rocess conditions rocess conditions Volatility (flash point) 5.0 Health and Safety in Mill Process The hazard properties of the proposed reagents are discussed in the attached Technical and Regulatory Review, the attached Table l. and summarized here. 01.27.2022 Withold from Public Disclosure Under Utah Code 63G-2-101 et seq . and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information Technical Memorandum 5.1 Extractants Pg.07 The compound mono extractant is evaluated below as representative of the two classes of compounds considered in this SERP. The remaining compounds in these classes have similar properties as described in the attached Table 1, which also com a re · the ro osed extractants to those pre iou:ly u • in the Mill. The representative extractant has a tlash point of It is anticipated that it will be added to the process at ambie.nt temperature condition, or possibly at conditions up to 11111111 Therefore, it is not expected that the extractant will be volatilized at process conditions. The extractants in both classes considered have no published occupational exposure limits, that is, in normal conditions, no respiratory protection requirements are identified. Because the compounds in these classes are irritating to membranes of the eye, skin, mouth, respiratory tract and digestive tract, prevention of dermal and eye contact, breathing and ingestion is required, both during introduction/charging of product into the system and during operation of the -removal process. The cun-ent procedures for splash protection from other solutions in the vanadium SX area will be sufficient for worker protection from contact with the extractant, and they do not need to be modified regardless of the quantity of extractant to he used. The operation with the highest potential for worker contact with the cxtractant will be during introduction/charging of pure product into the system. In fires or hi gh tern era ture conditions, the extractant decomposes to produce - The Occupational Sa fety and Health Administration ( 'O HA ") Permissible Exposure Lim it 'PE L") fo r The level f -con ·id e red imminently dangerous to life and The Emergency Response Plan ("ERP") has previously been reviewed during the 2020 SERP for use of -• to confirm that it addresses the re. piratory protection for fire response in the potential presence of minor quantities of . during the period that -is in use . Any increases in extractant to be stored, or used in the system. will not change the respiratory protection requirements for fire responders . Mill personnel are experienced with addition and use of compounds. The Mill has pre viou . ly used llllllin solvent extraction, and more recently, in 2019 and 2020, used for chloride pond return extraction. Both are comparable, but more aggressive, than the ones currently proposed . 01.27.2022 Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information Technical Memorandum Pg.OB The operations under the Change will be conducted in the same building that houses the vanadium SX area. The fire protection system in place for an organic (kerosene) fire is more than sufficient for the quantities of extractant to be used in the proposed Change. The SOS for whichever extractant is selected from the above classes should be added to the records available on site. 5.2 Mill personnel have experience with the use of strong mineral acids, based on the extensive presence of sulfuric acid throughout the Mill's leach area and TMS. Mill personnel are also . pec if ically experienced with use o f . in the ongo ing REU process in g fo r reco ve ry of RE -The anticipated additi o na l q ua nti ty f -~ cd [o r -re moval will be minimal compared to the ongoing us e fo r ~-proces ·in g. Rcq uireme,nl s for use of-in the process have been evaluated in SERP 2021-01, and will not be re- addressed here. 5.3 General/Other The REU process may operate at temperatures up to -The process will generate regular hazards of hot steam lines. heated equipment, and hot condensate lines. Mill personnel are experienced with operation of processes at these temperatures from the ongoing REU processing. None of the extractants or the removed -residual solutions are volatile or flammable. None of the extractants or product have been repmted to be carcinogenic or teratogenic. SDSs for the extractant , or other extractants, would need to be added to the records available on site. The respiratory protection progra m should be modified to address the required protection for the combustion products of based extractants, that is phosphine ga , in the event of a fire. Derived Air Concentrations ("DACs") may need to be developed for activities in connection with the concentrated residuals removed and transferred to tailings. 6.0 Environmental Considerations Environmental and other regulatory considerations are described in Attachment 1 and discussed below. 01.27.2022 Withold from Public Disclosure Under Utah Code 638-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information Technical Memorandum 6.1 Air Emissions Pg.09 There will be no new emissions other than potential minor vaporization of . evolved during dilution in the As discussed in Section 5.1, above, it is not expected that the proposed solvents would evolve vapors requiring air pollution control equipment. There will be no new stacks and no new air pollution control devices required. - is water soluble and will be absorbed in the existing demislers in the leach area. The removed -will be will be in the form of aqueous solutions or slurries that will not generate dust. 6.2 Tailings Management System The Mill proposes to discharge process solutions from the proposed process to Cell I, Cell 3 and/or to Cell 4A,. For conservatism, the discussion below af:sumes the entire mass of chemical residual from the process is discharged to one cell, either Cell 1, Cell 3 or Cell 4A. The chemical constituent, will be transferred to the Mill's TMS in res idu a ls d isc ha rge d peri od ica ll y fr o m the process. Based on an anticipated -use rate of -during processi ng, and ass umin g a full ye ar of pr oc ·ing, the annual addition of to th e T M S -be a pproxim ate ly --Th e qu a ntily is comp ara ble to antily of d e from th which are u ·ed in t he ongoing RE process . The will be recycled and reused lo the extent possible. It will be d isc harged to the TMS when the. equipment in the vanadium area is to be converted to reuse from REs to vanadium proces . ing. For th e foll owing di c u. ion, it has been a-;sumed that the entire quantity of up k , 0 1 . in th e process could be discharged to the TMS at one time. Based on current estimates of total mass in each cell: Cell I Cell 3 Cell 4A Current Total Mass in Cell 556,450 2,700,000 911.700 (tons) Current Total Mass in 1,112,888,000 5,400,000,000 1,823,400.000 Cell (lbs) 01.27.2022 Withold from Public Disclosure Under Utah Code 638-2-101 et seq . and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information Technical Memorandum Concentration of if total mass is di ·pos e d (mg/kg or ppm) ■ I Pg.10 ■ Note : The mass in Cell I was approximated assuming solutions have :.i dl!nsity of 8.33 lbJgal. Due to the high metal and anion content, the densily is likely higher, am! the coneentration shown is conservative. In all cases, the residuals will be transferred initially to Cell 1, Cell 3, or to Cell 4A, and potentially re-circulated through the TMS., Cells I and 3 were each constructed with a polyvinyl chloride ("PVC'') membrane liner. Cell 4A and Cell 4B have high-density polyethylene ("HOPE") liners. A number of studies evaluated both PVC and HOPE in conditions similar lo or more aggressive than those anti ip ate d in the Mill 's TMS. The tests included cati o ns acidic anions (s uch as -th an th e Mill's k rose ne . Haxo, el. al. (EPA 1985) and Battelle Laboratories (Farnsworth and Hymas, 1989) and EPA (EPA, I 988) evaluated the performance of PVC and other vinyl and polyethylene liner materials in leachate solutions containing metals, salts and volatile hydrocarbons in field tests in some cases up to 18 years exposure. Battelle's studies included the - Polyelhylenc was unaffected; PVC had good retention of properties . Performance data on HDPE and PVC liners in service since the 1970's was tabulated for leachate mixtures in the presence of oxy organics (phenols) up to 29,000 mg/L; sulfates up to 950 mg/L; and BTEX and naphthalene up to 2,500 mg/L. Both showed good performance over the lifetime in service. (Haxo. 1991) As mentioned above, compounds have previously been introduced to the Mill and disposed in the Mill's TMS, with no apparent adverse effects. The estimated concentrations calculated above should not be considered as a threshold or allowable limit for concentrations in Lai lings. The TMS is expected to be able to handle substantially higher levels as explained below . 01.27.2022 Withold from Public Disclosure Under Utah Code 638-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information Technical Memorandum Pg.11 Other studies including laboratory tests up to l 9 months and field service up to IO years including hydrocarbons up to O.Dl mg/L (Artieres et. al, no date) showed no degradation of PVC or HDPE. It can be concluded that both the PVC and HOPE liners will have suitable resistivity to the concentrations of any of the chemicals to be discharged to the TMS as a result of the proposed process. 6.3 Worst Case Spill Results and CERCLA/SARA Title II Section 302 Reportable Quantities (RQs) The worst-case spill estimates and CERCLA reportable quantities ("RQs"), where applicable, for each additive or product are summarized below. As mentioned above, extractant will be received in either 55-gallon plastic drums or 250- gallon plastic totes. The worst-case spill of solvent would potentially consist of the loss of either a pallet of 4 drums (220 gallons) or a full tote (250 gallons) before it was introduced into the process. For conservatism, this evaluation assumes the worst-case spill is 250 gallons or 1,980 pounds. Spills of solvent from the storage area, or leaks or spills of extractant from the vessels used in the vanadium SX area, would be managed consistent with the Mill's Spill Prevention, Control, and Countermeasures Plan ("SPCC") plan. Residual material would flow to the Mill's TMS. None of the compounds in the two solvent categories evaluated have any reportable quantity ("RQ") under SARA Section 302. As discussed above, the tailings cell liners have suitable resistivity to to receive many times the worst-case pill of one tote or one pallet, as well as the discharge of the full quantity of extractant in the circuit at any one time. A worst-case spill of -has been addressed previously in SERP 2021-01 and is not re- visited in this document. SERP 2021-01 addressed the spill of a full 5,000-gallon truck. Whether -is delivered in a truck of 5,000 gallons or larger, the spill response consistent with the Mill's SPCC would be the same. The on-site -storage tanks are in a secondary containment structure and any spill would be returned to the tanks or transfen-ed to the Mill's TMS 01.27.2022 Withold from Public Disclosure Under Utah Code 638-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information Technica l Memorandum Additive or Product extractant Worst Case Spill 1111 6.4 Reclamation and Surety Considerations CERCLA RQ or Other Reporting Requirement NoCERCLARQ Pg.12 The proposed Change will utilize existing equipment within existing Mill buildings on site. The Change requires no construction and no change to the Mill footprint. The Change will not require new equipment that would increase the reclamation tailings volume beyond the current estimate for full Mill production. The Change will not require any additional procedures or special provisions or monitoring beyond those proposed in the approved Reclamation Plan. The Change will therefore not require any change to the reclamation plan or adjustment to the financial surety amount. 6.5 Drainage and Surface Water Spills of solvent would occur within its storage area or the vanadium area within the Mill buildings, and will drain to the Mill's TMS. Spills of -would be contained in the storage tank diked area and would be returned to the tanks or transferred to the Mill's TMS. Drainage maps in the Mill's SPCC and Storm Water Best Management Practices Plan ("SWBMPP") will need to be updated to indicate the location of thellllllstorage tanks and the storage areas for the extractant. 01.27.2022 Withold from Public Disclosure Under Utah Code 63G-2-101 et seq . and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information Techn ica l Memorandum 7.0 Consistency with License, Permits, Plans and SOPs. 7.1 Groundwater Discharge Permit ("GWDP") The reagents and additives for the proposed process are phosphonic or Pg.13 has been addressed in Lhe 2020-01 SERP for REU processing. the ion is currently monitored in the TMS and groundwater. and will not be further revisited here. The extractant classes are comparable to other organic compounds previously or currently used in the Mill and historically present in the TMS. The 1997 EA for the Mill anticipated the use of similar compounds in the lab, which would be discharged to the TMS . None were required as analytes in tailings solution monitoring or groundwater monitoring. Utah DWMRC's 2004 GWDP Statement of Basis ("SOB") identified that the more aggressive had previously been used with kerosene in the Mill's uranium solvent extraction step. The SOB included tailings data showing that following the historic use of- the TMS ·a mples indic ated up to , and immeasurably small levels of -in tailings soluti o n . DWMRC determined, based on this SOB, that even following use and introduction of inl'o the TMS, it would not be necessary to include monitoring of compounds, in groundwater or in tailings solutions . All of the compounds in the two -extractant classes considered in this SERP are less aggressive and less mobile than the -addressed by DWMRC in the 2004 SOB. Hence, no modification of the GWDP should be required to address these chemicals. 7.2 Air Approval Order ("AO") As discussed in Section 6.1, there will be no new air emissions and no new air pollution co11trol devices required. No amendment to the Mill's AO will be required. 7.3 Other Permits, Plans and SOPs Based on the discussion above, the following documents may require amendments or revisions to address the proposed process: • SPCC tables, • SWBMPP, 01.27.2022 Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information Technical Memorandum • SOP books, • ERP to address the -storage tanks, • SDS books throughout the Mill. Pg.14 The SOPs describing the proposed Change evaluated in this memorandum are provided in Attachment 3. All needed items are listed in detail in the Action Item list in Section I 0.0 of this memorandum. 8.0 Compliance with Other Regulations 8.1 Resource Conservation and Recovery Act (RCRA) RCRA regulates the treatment, storage and disposal of hazardous wastes. None of the proposed chemicals are associated with any RCRA waste listings. As described above, compounds will be transferred to the TMS, which already has received these or comparable compounds from sources in the Mill and alternate feed materials. 8.2 Toxic Substances Control Act (TSCA) All chemicals identified for the proposed process have active status on the TSCA Chemical Substances Inventory, that is, they are approved for sale, use and transport. 8.3 Emergency Preparedness and Community Right-to-Know (EPCRA) Section 313 Toxic Release Inventory (TRI) Reporting lndustries under SIC Code I 094, which include uranium, thorium and radium extraction and recovery, are exempt from reporting under EPCRA Section 313. 8.4 OSHA Hazard Communication Standards ("HCS'') The OSHA HCS in 29 CFR 1910.1200, as accepted by MSHA, require that the Mill update all copies of the SDS binders to include the proposed new extractants. 9.0 Sustainability EFRJ evaluates each new project to determine whether there is any alternative that will have measurably lower environmental impacts. This step confirms that the chosen alternative is as sustainable as is reasonably possible ("ASARA"). The following considerations have been considered. 01.27.2022 Withold from Public Disclosure Under Utah Code 638-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information Technical Memorandum Pg.15 • Removal of the , REs wil I reduce the quantity to be shipped, with an associated reduction in transportation, specifically o Fewer supersacks o Fewer truck trips and less fuel consumption • The removal of , will improve the quality and salability of the product, reducing the quanlity that must be reprocessed or disposed. • The proposed change is the first step in allowing eventual separation of RE _ Producing REs in the US will greatly reduce the environmental impacts of transporting RE metal products from foreign producers such as China. 10.0 Conclusions and Recommendations Based on the foregoing information, it can be concluded that: I . The proposed change will not produce any environmental impacts outside the envelope of those already addressed in the approved ERs for the Mill. No license amendment is required for the proposed change. 2. SOPs have addressed appropriate Personal Protective Equipment ("PPE") for the additional respiratory hazards from phosphoric oxides in a fire. 3. The proposed Change generates no additional environmental emissions. 4. All chemicals or material to he discharged to the TMS under the proposed change. are already monitored, or well represented by other analytes already monitored in the tailings solutions and under the GWDP. The proposed change will not require any modification of the Mill's GWDP. 5. No RCRA requirements apply to the proposed change. 6. All proposed materials arc acceptable under TSCA. 7. As listed above, revisions will be required to certain documentation referred to in lhe RML application as itemized in Section 10.0, below. 01.27.2022 Withold from Public Disclosure Under Utah Code 63G-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information Technical Memorandum 11.0 Action Items Based on the above evaluation, the following action items need to be implemented. • Update the SPCC tables. • Update the SWBMPP. • Update the SOPs books to include appropriate additional SOPs. • Confirm the SOPs have been reviewed for proper PPE. • Update the ERP to address • Add SDSs for the new extractant(s). Pg.16 01.27.2022 Withold from Public Disclosure Under Utah Code 638-2-101 et seq. and as indicated in the redacted text below. All redactions were based on CBI/Proprietary Information Technical Memorandum 11.0 References Pg.17 Artieres, 0., F. Gousse and E. Prigent laboratory Ageing of GeomembraneJ· in Municipal l..andjill Leachares no date Centers for Disease Control ("CDC") National Instilute for Occupational Safety and Health ("NIOSH ") accessed at hu ~://v W \ .c dc .crov/ni os h/n w n gd0492 .hLml January 2022 Dames & Moore Environmental Rep011 White Mesa Uranium Mill San Juan County, Utah January 30, 1978 Farnsworth, R.K. and C.R. Hymas, August 1989 The Compatibility of Various Polymeric li1ter and Pipe Materials wirh Simulated Double-Shell Slurry Feed at 9(J'C. Pacific Northwest Laboratory, US. Department of Energy, Battelle Memorial Institute Haxo, Henry E., Jr. Compatibility of Flexible Membrane Liners and Municipal Solid Waste Leachates US EPA Risk Reduction Engineering Laboratory August I 991 Haxo. H.E., Jr., Robe11 S. Haxo, Maney A. Nelson, Paul 0. Haxo, Richard M. White, and Suren Dakess ian Liner Materials Exposed to Hazardous and Toxic Wastes US EPA Hazardous Waste Engineering Research Laboratory EPA-600/S2-94-I 69 January 1985 National Institute of Occupational Safety and Health Online NIOSH Pocket Guide to Chemical Hazards hllpl:.:ll ww ,v.cd c.gov/n i . h/npg/sca rc h .html accessed January 2022 OSHA Hazard Communication Standards as stated in 29 CFR 1900.] 200 US EPA list of lists Consolidated list of Chemicals Sub jeer to EPCRA, CERCLA and CAA 550- B-19-03 June 2019 US EPA, 1988. Risk Reduction Engineering Laboratory . lining of Waste Containment a11d Other Impoundmenr Facilities EPN600/2-88/052 September 1988 US EPA Toxic Substances Control Act Chemical Inventory Chemical Substance Invento1)• February 20 I 9 US Nuclear Regulatory Commission Environmental Assessment for Renewal of Source Material License SUA-1358 Energy Fuels Nuclear. Inc . White Mesa Uranium Mill March 14, 1997 01.27.2022 Technica l Memorandum Pg.18 ACGIH AO BaCb CAA CCD CDC CERCLA EFRI EPCRA ER GWDP • HCS HOPE NTOSH OSHA PPE PVC RCRA REE REU RML RQ SARA SDS SERP SOP LIST OF ACRONYMS American Conference. of Government Industrial Hygienists Air Approval Order Barium Chloride Di hydrate Clean Air Act Counter Current Decantation Centers for Disease Control Comprehensive Environmental Restoration, Compensation and Liability Act ("Supcrfund'') Energy Fuels Resources (USA) Inc. Emergency Preparedness and Community Right-to-Know Act Environmental Report Groundwater Discharge Permit Hazard Communication Standard High density polyethylene National Institute for Occupational Safety and Health Occupational Safely and Health Administration Personnel Protective Equipment Polyvinyl Chloride Resource Conservation and Recovery Act Rare Earth Elements Rare Earth Bearing Uranium Ore Radioactive Material License Reportable Quantity Superfund Amendments and Reauthorization Act Safety Data Sheet Safety Environmental Review Panel Standard Operating Procedure 01.27.2022 Technical Memorandum SPCC SWBMPP sx TMS TRI TSCA Attachments • Figure 1 Spill Prevention, Control, and Countermeasure Plan Storm Water Best Management Practices Plan Solvent Extraction Tailings Management System Toxic Release Inventory Toxic Substances Control Act Schematic Flow Diagram for • Table l Comparison of Extractants • Attachment I Technical and Regulatory Review • Attachment 2 Safety Data Sheets Pg.19 Removal Q) Ol (ti C. -~ c Q) t5 (ti Q) a: I -II I 111 I I I I I I I I I I I Ill I ATTACHMENT I TECHNICAL AND REGULATORY REVIEW Redact entire page Chemical and Regulatory Summary - ATTACHMENT 2 SAFETY DATA SHEETS ------ ~ ... -~--_____ __J •• SAFETY DAT A SHEET -'-------------~ -------1=----+-I=----- --------------~ --- ■ __, __ - SAFETY DATA SHEET -available - SAFETY DATA SHEET ■ -'---------------------' ■ c loth ing/equipment in Section B, wear a two p iece PVC suit with hood or PVC overalls w ith hood . ■ ■ ■ --- -- SAFETY DATA SHEET --.. -- -.... _c__c__c__c__c__c__c__c__----------=--------=--------=--------=--------=--------=--------=--------=----=- -- -================-=:::, --- --- --- -- SAFETY DATA SHEET -- -- Chronic toxicity to daphnia and • -- 10/ 13 Organophosphorus ester 12.6 Other adverse effects Ecotoxicity assessment Short-term (acute) aquatic hazard SAFETY DATA SHEET -'--------------~ ---------------._ ._ --... ... ____________________ __. --- r r ~- -- -- - - 2 1 0 2 1 0 Page 1 of 6 '.- - ____,,,, _________ _ ----~ -■ -- -- - - --■--- - -- - Aldrich -223301 Page 6 of 6 00 -- --- Plctogram(s) or Symbol(s}: ---- ---- --------- - - ----- TCIAMERICA ---- --- No data available ~o data available o data available No data available No data available No data available No data available No data available ---- 11111111. ------------------- ... ------ .. - - Preparation Date 2/24/2015 Latest Revision Date (If Revised) 3/6/2018 I -----.. -- WHMIS Symbols (Canada) ~~ ... Eye/Face Protection Safety goggles or face shield . All equipment should have been tested and approved under appropriate standards, such as NIOSH (US), CSA (Canada), or EN 166 (EU). - - ·- - ------ - - - -- - ■ -- - --- --------------- - -... - -I I -I I - --- -.. -- ATTACHMENT 2 -Removal SOP White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 7 ■■■■Removal Preface • • • • ate t Comm uni cation Date: 01-22 Revision: EFR-1 Page I of 4 To be successful as an operator in achieving the desired results in your circuit, good communication between you, the metallurgical department, and your supervisor should exist. Information is given to the operator verbally, written and by test results. As an operator, if you do not understand any information given, you have the responsibility to ask questions until you do understand. White Board. In a few locations in the mill, critical information about mill operations will be written on White Boards. Information such as circuit parameters, required changes in circuit operations, or special instructions about maintenance. Circuit Sheets. Circuit sheets will have operating parameters on them along with sampling times for the circuit. They will also have a place for you to pass along written information about your circuit. Verbal. One of the most important times of your shift is at Shift Change. You have the responsibility to pass along information about your circuit to the person relieving you. You will be given verbal instructions from your supervisor or metallurgical department which you need to be sure you understand. Written. Instructions will be handed out in written form almost daily. As above, if you do not understand any instruction, ask your supervisor. Health and Safety The solution that is fed to the -removal circuit is -and has high concentrations of rare eruth metals. This solution should not be ingested. The ~!so contains heavy metals and should not be ingested. The organic solution is flammable. No Hot Work will be done in the solvent extraction building without a Hot Work permit. Any possible ignition source must be avoided. The solution used to strip or remove the rare earths from the organic solution is and should be handled appropriately and only when using appropriate Personal Protective Equipment (PPE). generates vapors that should be avoided. These vapors can cause extreme irritation and injury. Hazards: • I • Stairs and elevated work areas • Pressurized solutions pumping throughout the circuit • White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 7 -Removal Per onal Protective Equipment (PPE) Date: 01-22 Revision: EFR-1 Page 2 of 4 1. Minimum PPB requirements at White Mesa Mill while in the restricted area is hard hats, safety glasses, and steel toed shoes. No ragged or lose fitting clothing is allowed. Body jewelry, rings, wrist watches, etc. are required to be removed while working. 2 Other personal protective equipment includes, but is not limited to: ear plugs, respirators, wet suits, welding helmets, goggles, gloves, and rubber boots. Face shields and safety belts are required in designated areas and/or while performing certain jobs. If in doubt, contact your supervisor. 3 Each employee is responsible for the condition of their protective equipment. Report any defects, etc., to your supervisor. 4 The following equipment is required when working on pipelines or vessels containing acids or caustics: a. Face shield and chemical splash goggles b. Rubber coat and pants c. Rubber gloves and rubber boots d. Other equipment specified by the foreman for that pa1ticular job listed on the Safe Work Permit 5 The use of a safety belt and properly adjusted lifeline is required where there is a danger of falling four feet or more, except while performing work under the ladder and scaffold section of this manual. This rule applies when going beyond the handrails of walkways on top of any tanks in the mill area. 6 It is a condition of employment that all personnel who may be required to wear a respirator must be clean shaven to assure that the respirator fits properly. Personnel will be fully trained consistent with the Mill's Respiratory Protection SOP, prior to using respirators. While Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 7 ■■■■I Removal -One of the most critical aspects of this circuit is I I Sampling Date: 01-22 Revision: EFR-1 Page 3 of 4 Sampling of the various solutions in this circuit is required on a regular basis. It is important to ensure that any sample taken is representative of the tank's contents. This means that tanks should be well mixed, sampling equipment should be clean, and any sample ports purged before collecting the sample. Operating ln tructions 1. Conduct a proper Shift Change with the person you are relieving. Get information about all circuit 2. I I I I I I I parameters, including, but not limited to: flow rates, tank levels, solution concentrations. White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 7 ■■■■1 Removal tart-up Procedures Shutdown Procedures I I I I I I Emergency Shutdown Procedures I I I Date: 01-22 Rl!vision: EFR-1 Page4 of 4 ATTACHMENT 3 SERP 2022-02 -REDACTED REPORT ENERGY FUELS RESOURCES (USA) INC. WHITE MESA URANIUM MILL SAFETY AND ENVIRONMENTAL REVIEW PANEL MEETING OF DECE:MBER 14, 2022 SOPs for Separation During Uranium Rare Earth Ore Recovery SERP No. 2022-02 ENERGY FUELS RESOURCES (USA) INC. WHITE MESA URANIUM MILL SAFETY AND ENVIRONMENTAL REVIEW PANEL MEETING OF DECEMBER 14, 2022 SERP NO. 2022-02 1. PURPOSE The Energy Fuels Resources (USA) Inc. ("EFRI") Safety and Environmental Review Panel ("SERP") for the White Mesa Uranium Mill (the "Mill") met by telephone conference on December 14, 2022 in accordance with SERP procedures in White Mesa Mill Standard Operating Procedure PBL-:1, Rev. No. R-6 (the "SERP SOP"), to consider SERP No. 2022-01, regarding the following (the "Change"): Review and approve a proposed Procedure ("SOP") for separation of the currently-produced mixed rare earth intermediate stream ("the Change"). The SERP followed the SERP SOP as it performed this SERP evaluation, to ensure that the change is consistent with the following three criteria (the "SERP Approval Criteria"): (a)The change, test or experiment did not conflict with any requirement specifically stated in the Mill license, and did not impair EFRI' s ability to meet all applicable regulations; (b)There would be no degradation in the essential safety or environmental commitments in the license application, or provided by the approved reclamation plan; and ( c) The change, test or experiment was consistent with the conclusions of actions analyzed and selected in the most recent Environmental Assessment (EA) conducted by the Division of Waste Management and Radiation Control ("DWMRC") from the last license renewal and/or major license amendment. 2. OVERVIEW AND BACKGROUND The Mill intends to modify its existing solvent extraction ("SX") facility by removing an existing rare earth ("RE") SX circuit and some redundant vanadium SX tanks and replace them with an expanded RE SX circuit to be used to purify the currently- produced mixed rare ea intermediate stream. The mixed rare earth solution will be separated into Page2 -similar to what is currently produced from the existing RE circuit that will be removed and replaced by the expanded RE SX circuit. The will be calcined to produce The Mill is evaluating and this SERP assumes packaging and selling an interim 111111 -_pro~quirements and equipment related to oxidation are finalized. ~tep and associated equipment will be evaluated in a separate SERP process and, if required, air approval order ("AAO") revision process. The SERP evaluated the remainder of the proposed process described above. In addition to the proposed process and chemicals, the SERP evaluated the SOPs, which addressed the operation described above. The proposed process is referred to in this report as the 111111 process, or the "Change." The SERP evaluated the process with respect to the requirements of condition 9.4 of the Mill's RML, worker safety, process safety, and environmental protection. 3. SERP MEMBERSIDP AND QUALIFICATIONS This SERP consisted of the following members: Resoonsibilitv Name/Position Corporate Radiation Safety Officer or Garrin Palmer equivalent; Mill Radiation Safety Officer (Member) Assuring Tests conform to radiation safety and environmental requirements Management Expertise; David Frydenlund Responsibility for managerial and financial Executive Vice President, Chief Legal approvals Officer and Corp Secretary (Member) Operations and/or Construction Logan Shumway Management; Mill Manager (Member) Responsibility for implementing operational procedures Responsibility for regulatory compliance at Kathy Weinel WMM Director, Regulatory Compliance Corporate responsibility for regulatory • Scott Bakken compliance Vice President Environmental Affairs Independent Safety /Environmental Jo Ann Tischler Evaluation Independent Chemical Engineering Consultant Page 3 In addition, the following Mill or Corporate Personnel attended the SERP : Reason for Attendance Name/Position Technical Expertise on proposed process Timo Groves Chief Metallundst, PE Worker Safety Expertise Dax Jacobsen 4. SERP iu:VIEW OF PROPOSED CHANGE AND SOP The SERP reviewed specific details relating to the process, including the SOPs and the independent consultant's Technical Memorandum. A copy of the SOPs and the Technical Memorandum are provided in attachments to this report. Specific points discussed are summarized below. The SERP reviewed all processing steps, and identified those procedures that did not need to be included in the processing SOP, or materials, specifically, _, that did not need to be re-addressed because they have been approved separately. The SERP also reviewed the Document Control SOP, in place since 2000, which requires that any new SOP, or any significant change to an existing SOP, requires a SERP review. 5. REVIEW OF SERP APPROVAL CRITERIA 5.1. Review of the Criteria In order for a change in the facility or process, as presented in the license application, to be eligible for approval by the SERP, the three SERP Approval Criteria, detailed in Section 1 above, must be satisfied. The three SERP Approval Criteria, as detailed in the five steps of the SERP procedure, were reviewed and discussed, as follows: 5.1.1. Does the change conflict with any requirement specifically stated in the license? The SOPs will not require any types of process operations not currently performed at the Mill. Processes such as solvent extraction and product stripping, have been regularly performed at the Mill. The Change will involve an additional stage of RE product separation using the same types of solvent extraction equipment, such as feed tanks and as currently and historically used. The Change will require the relocation of some existing installation of addit ional SX equipment of the same type as currently used, which will be installed within existing buildings. Storage of chemicals will not require construction of new tanks or storage areas. The Change will not require use of electricity, fuel, or water resources beyond levels anticipated in the license for full Mill production. Page4 There are no reported incompatibilities for -and it can be stored near other products or reagents. Use of the will not require any worker protections beyond those currently in use in other Mill operations. The Mill's License anticipates the recovery of secondary metals, such as vanadium, from uranium ores, via additional SX circuits. Based on the above, the SERP determined that the Change does not conflict with any requirement stated in the license or any license requirement contained in any license tie- down letters. Therefore, this criterion is met. The purified and concentrated yellowcake that will be produced from the ore 1111 to the RE recovery step will not cause the Mill to exceed the yellowcake production limit under the License. 5.1.2. Does the change impair EFRI's ability to meet all applicable regulations? No. The SERP identified that there are no Resource Conservation Recovery Act ("RCRA") Comprehensive Environmental Response, Compensation and Liability Act ("CERCLA"), or Toxic Substances Control Act ("TSCA") requirements applicable to the ore, -or proposed process chemicals, The chemicals and proposed Change and SOPs will not generate any new air emissions or r uire revision to the AA O. -will be supplied in It has previously been used at the Mill in laboratory test quantities and transferred to tailings from the Mill laboratory. The SERP reviewed the facts that: • -is a natural, non-hazardous compound present in plant material with minimal environmental lifetime and no hazardous effects if spilled or released to the environment, • it forms inert, stable, insoluble precipitates with many metals and will not be reactive within the tailings solution environment, • it is far less aggressive than the mineral acids currently present in the tailings management system ("TMS''), and will not have any effect on the tailings cell liners, • it will be present only as , and will be present at immeasurably small, non-detectable levels in the TMS and could not be identified or measured in any way in groundwater. Utah DWMRC identified in the 2004 Statement of Basis for the Mill's Groundwater Discharge Permit specific organic compounds targeted for monitoring in the Mill's Page 5 groundwater and justified why other organic compounds were not of significant concern to be monitored. Existing spill management procedures will be sufficient for the proposed process chemicals. The SERP noted that there are no Emergency Planning and Community Right-to-Know Act ("EPCRA") reporting quantities for The Spill Prevention Control and Countermeasures ("SPCC") plan tables will be updated as appropriate for- 5.1 . 3. Is the change consistent with the conclusions of actions analyzed in the most current EA? The original 1980 Environmental Assessment ("EA"), subsequent environmental reports, and the DWMRC Technical and Environmental Report for the Mill contemplated that the Mill would recover secondary metals, in addition to uranium. The original EA contemplated recovery of copper and/or vanadium. The Mill has also previously been approved to recover, and has modified the process to recover, tantalum and niobium. The process will not generate any measurable new tailings constituents not already monitored or addressed by other indicator parameters in the groundwater discharge permit ("GWDP"). Precipitates of -are so insoluble and so immobile they would not be measurable or detectable in tailings solutions or groundwater. The process will produce no new or increased air emissions. The tailings to be generated will be comparable to, and contain comparable non-radiological constituents, as the tailings previously generated and managed in the tailings management system. The Change will not introduce any new feed materials or new radionuclides. The process will involve no change to the uranium recovery circuit or radionuclide levels in the uramum recovery process. 5.1. 4. Does the change require any adjustment to the financial surety arrangement or approved amount? The SERP determined that there would be some required change to the Mill's surety. There would be some increase to the Mill building footprint but no change to the footprint of the Mill's disturbed area. There would be a minor increase to the volume of equipment to be disposed in the tailings management system at reclamation. This will be addressed in the next revision to the tailings volume capacity estimate and surety estimate. The Change will not measurably increase the quantity of materials discharged to the tailings system, relative to the RE process. The volume of any new equipment to be used for the process was anticipated within the licensed tailings capacity. Page 6 The composition of tailings from the proposed process will not require any change to the cover design as noted in the September 9, 2020 letter to DWMRC. The composition and quantity of tailings generated will not require any special management or changes to the tailings reclamation plan. 5.1.5. Does the change create any degradation in the essential safety or environmental commitments in the license application, or provided by the approved reclamation plan? The SERP assessed that there would be no change in the safety or environmental commitments in the license application or reclamation plan. Processing according to the SOPs is not expected to produce any environmental impacts beyond those assessed in any EA, and is consistent with the conclusions regarding actions analyzed in the EAs. As a result, this criterion is also satisfied. The proposed process will: • Not produce any increased levels of radionuclides in processes or wastes beyond those anticipated in the EAs or previously managed under approved SOPs, • Not introduce any constituents to the TMS that are detrimental to the tailings solutions or tailings liner, • Not produce any new emissions or pathways for exposure to workers or the public, • Not introduce any new pathways of contamination to the environment, • Not increase the disturbed area footprint, • Require no changes to the Radiation Protection Manual ("RPM"), • Require no changes to the Environmental Protection Manual ("EPM"), • Require no changes to the Emergency Response Plan ("ERP"), • Require no changes to the ALARA SOP, • Require no change to the GWDP, • Require no changes to the training program, and • Not require additional tailings capacity or changes to tailings management plans, The Change will Require an update of the SPCC and Stormwater Best Management Practices Plan (' SWBMPP") to incorporate -All other chemicals have been historically used at the Mill and have been evaluated in previous SERPs. Processing according to the SOP is within the envelope of conditions evaluated in the Mill's MILD OS model for dose to off-site receptors. All changes involve additional aqueous and solvent extraction steps on non-radioactive metals. There will be no new sources of radionuclide emissions. The tailings capacity evaluation 2023 update will confirm that suitable tailings capacity exists for equipment associated with the proposed Change. The Mill sought to meet EFRI's sustainability goals by: • optimizing the re-use of existing equipment Page7 • minimizing the footprint of new or relocated equipment to maintain and minimize the footprint of the Mill's disturbed area, and • selecting the least hazardous chemical suitable to perform the precipitation. 6. CONCLUSIONS The SERP concluded that the proposed Change and SOPs meet the criteria set forth in the SERP SOP for approval, and approved the proposed process and SOPs. 7. ATTACHMENTS • Attachment 1 -Technical Memorandum of J. Tischler December 14, 2022 • Attachment 2 -SOPs for separation Page 8 SIGNATURES Re )Ort reviewed bv : ~~-__ __ _ Date:J~1?---'---_ Scott Balcken Date: ?' /f C/ / l-./ ~,~'; ~Bl~- (i.1 ,Tin Palmer Date: __ L_t~/_l _._1 /--=2"---->-=------- Date: __ ~___,__/ 3:.....0_,i--'-~-=-=,;__;;;;_3 ___ _ Ka~y Weinel I I I Date: ---t/1/('Z',3 _ __.____.__ _______ _ ~ ~~ ~ 1 Date: /11\or ~o rz..o Z.~ ------------------I--------Timo Groves PaPe 9 ATTACHMENT 1 Technical Memorandum of Jo Ann Tischler December 14, 2022 12.14.2022 To: S . Bakken, D. Frydenlund, T. Groves, P. Keller L. Shumway, K. Weinel From: Jo Ann Tischler Cc: Re: Draft Technical Review of Proposed Rare Earth Separation and Rare Earth _ Production Technical Memorandum Introduction This Technical Memorandum (the "Memorandum") evaluates a proposed change at the White Mesa Mill (the "Mill") to produce alllllllrare earth ("RE") product, along with uranium from its uranium-bearing natural monazite ores. The Mill intends to modify its existing solvent extraction ("SX") facility by removing an existing RE SX circuit and some redundant vanadium SX tanks and replace them with an expanded RE SX circuit to be used to purify the currently-produced mixed rare earth stream. The mixed rare earth stream will be precipitated using to produce --The stream will be to produce -product, similar to what is currently produced from the existing RE circuit that will be removed and replaced by the expanded RE SX circuit. The -will be -to produce -• a The step will be evaluated in a separate SERP . Tbe Mill is evaluating packaging and selling an interim -product while requirements and equipment related to are finalized, as discussed in Section 6.1. This Memorandum assesses whether the Change may pose any worker safety or environmental hazards, or be inconsistent with conditions and assumptions in the Mill's current State of Utah Radioactive Materials License No. UT1900479 (the "RML'' or the "license") or other regulations. This assessment was performed as part of a SERP evaluation of this potential change or test under the RML and the Mill Standard Operating Procedures ("SOPs"). The proposed RE recovery process expansion and SOPs will be referred to in this memo, for the purposes of SERP evaluation, as the "proposed process" or "Change". In order for a Change or test in the facility or process, as presented in the license application, to be eligible for approval by the SERP, three SERP Approval Criteria must be satisfied. This memorandum provides information needed to answer the three SERP criteria as follows: la) Does the change conflict with any requirement specifically stated in the License? 1 b) Does the change impair EFRI's ability to meet all applicable regulations? 2) Does the change create any degradation in the essential safety or environmental commitments in the license application or provided by the approved Reclamation Plan? 3) Is the change consistent with the conclusions and actions analyzed in the most recent Environmental Assessment conducted by the Division from the last license ren~wal and/or major license amendment? Tischler Consulting Services, LLC J1JC Tel 303-501-9226 8015 South Krameria Wa y Centennial, CO 80112 japmst55@gmai l.com 12.14.2022 Technical Memorandum Pg.02 The following report provides an evaluation of potential safety and environmental hazards, consistency with the RML, and provides information for comparison to the SERP criteria. To perfonn this evaluation, we have considered the following questions: 1. Will the footprint of the disturbed area increase, e.g., for new buildings, storage pads, tanks? 2. What, if any, new chemicals or reagents will be required for the proposed process? 3. Are there any new or different environmental or safety issues associated with the storage, use, handling, or disposal of new chemicals or reagents? 4. Would use of new chemicals or reagents create any additional requirements for spill or emergency response equipment or training? 5. Would the use of new chemicals or reagents create any additional environmental emissions? 6. Are the existing and the proposed SOPs appropriate and sufficient for the reagents to be used? 7. Is the implementation of the proposed process and SOPs consistent with the Mill's RML, RML application, reclamation bond, other permits, and plans? 8. Does the implementation of the proposed process and SOPs conflict with any EFRI environmental or safety commitment made in any other plan or document? 9. Do any of the following requirements apply to the materials proposed to be used or produced in this Change: • Resource Conservation and Recovery Act ("RCRA"), • Toxic Substances Control Act ("TSCA"), or • Comprehensive Environmental Response, Compensation and Liability Act/Superfund Amendment and Reauthorization Act ("CERCLA/SARA") • Clean Air Act ("CAA") and regulations in Utah Administrative Code R307- 401 12.14.2022 Technical Memorandum Pg.03 10. Is the proposed Change being implemented in a manner that satisfies the Mill's As Sustainable as Reasonably Achievable ("ASARA") objective? 1.0 Basis and Limitations of this Evaluation The evaluation in this report is based on the following documents: • Schematic process flow infonnation provided by Mill personnel. • Safety Data Sheet ("SOS'') for from • Process schematic diagram for the proposed process provided by Mill personnel. • Communications with Mill personnel from October through November 2022. • Additional technical references listed at the end of this memorandum. 2.0 Description of Proposed Change A potential flow configuration for the proposed Change is depicted in the schematic flow diagram in the attached Figure 1. The recovery of REs from Rare Earth-bearing Uranium ("REV") ores at the proposed scale would use the same initial steps as the previous test scale process approved by the April 19, 2021 SERP. As evaluated previously, ores would be received , weighed , and sam led using existing equipment. The REV ore will be dum ed into a using existing uranium o will be treated to remov which is commonly used in the Mill, and the rare earth 12.14.2022 Technical Memorandum in the Mill's tailings management system ("TMS"). The for disposal in the TMS in a similar fashion -elution will be precipitated with Pg.04 will be disposed generated as a byproduct of the precipitation step may be recycled to the process or disposed ofin the TMS. Th product. The proposed Change would require the modifications listed below, to produce a modified RE solvent extraction circuit for the above process. • Some vanadium be moved to another location to accommodate the new RE SX equipment. Other vanadium SX equipment would remain in place, but would not be used for the RE SX. • The mini SX equipment that was previously used for RE separations will be removed. Additional units will be installed in the building extension that formerly housed additional vanadium mixer-settlers. Mill is evaluating This equipment is discussed further in Section 6.1. The SERP of April 19, 2021 evaluated all of the process steps and chemical use and disposal required for processing of 15,000 tons per year ("TPY") ofREU ore for production of a mixed RE -product. The SERP of January 22, 2022 evaluated the modification of the SX facility to add RE SX equipment to se arate from the -product, which is currently being done (the being sent to the tailings to allow for production of a ). The current evaluation addresses installing additional SX equipment (similar to equipment already installed) to allow for more complete separation of the REs. The more complete separations would produce report to tails similar to the current process. The following chemicals have historically been used in the Mill's circuits and are not re- evaluated here. 12.14.2022 Technical M emorandum ·-·-I Pg.05 The following chemicals and their use at rates to support processing of 15,000 TPY REU ores have been evaluated and approved in the SERP of April 19, 2021 and are not re-evaluated here. I I The following chemical and its use at rates to support processing of 15,000 TPY REU ores has been evaluated and approved in the SERP of January 22, 2022 and is not re-evaluated here. ·- The use and discharge to tailings o-at levels required for the Change is discussed in Section 6.2. -will also be used, specifically in the precipitation step, to produce the- tltrough the above-described process. -has historically been used in the Mill laboratory, but has not been used for process operations in the Mill circuits. The current technical memorandum and SERP will evaluate the effects of adding to the RE circuit , a:n d producing and handling -in addition to the wastewater and Calculations discussed in this evaluation are based on an assumed case of processing approximately 15,000 TPY of monazire ores to produce approximately 11111111 TPY ofllllll -Regardless of the ore source, the proposed throughput will not cause the Mill to exceed the RML limit of 4,380 tons of yellowcake production per year. -acid is discussed under Section 4.1, 5.1 and 6.2, below, and in the Technical and Regulatory Review in Attachment 1. As mentioned above, all other chemicals will be those historically used in ore processing, and have been evaluated at use rates greater than the proposed Change. As a result of the proposed Change: • There will be no change to the uranium leaching and recovery circuit or alternate feed circuit. • There will be no change to the uranium drying or packaging equipment. 12.14.2022 Technical Memorandum Pg.06 • The mini SX equipment will be removed, but the uranium circuit can operate without this equipment • Vanadium mixer-settlers will be removed, but the vanadium circuit can operate without this equipment. • A vanadium -which was approved in the Mill's Air Approval Order ("AAO"), was never constructed, but has remained as an approved portion of the Mill's Potential to Emit in the AAO. The vanadium Ill will be removed from the AAO and will be replaced by the (any required amendments to the AAO will be obtained). • Vanadium the operate with existing vanadium ~quipment and without o be removed from the AAO. • The Mill's TMS will not receive any new radiological wastes. • There will be no increase to the footprint of the Mill's disturbed area. 2.1 Past History of Uranium Extraction from Ores with Secondary Metals The Mill has extensive experience with the extraction and recovery of secondary metals from natural uranium ores or alternate feed materials. The Mill has recovered, and continues to recover, REs from uranium monazite ores, vanadium from vanadium-bearing uranium ores as well as tantalum and niobium from alternate feed materials, as approved by the US NRC in RML Amendment 5. The majority of the process steps for the Change are the same as those currently used for ongoing RE recovery at the Mill. The additional steps, such as - are similar to those used for of uranium, and of secondary metals previously recovered at the Mill. 12.14.2022 Technical M emorandum Pg.07 3.0 Properties of Proposed Chemicals and Products The properties of each of the proposed chemical additives are described in detail in the attached Technical and Regulatory Review. The physical state is discussed in Section 4.0 below. Hazardous properties are discussed in Sections 4.0 and 5.0, below. 4.0 Proposed Storage and Use of Chemicals and Reagents Storage location, and storage and use quantities of additives for the proposed process are detailed in the attached Technical and Regulatory Review. For ease of reference, storage locations of proposed additives are summarized below. New Additive or Product - Form Dry powder added to solution Dry powder Storage & Use Location Stored in closed or covered building. Incompatibilities Strong acids, strong oxidizers , silver compounds, strong alkalis, chlorites. - ~ill not be in direct contact with any of these materials in the Mill. Oxidizing agents. will be stored in sealed product drums or super sacks and will not be in contact with oxidizers. The storage of all reagents, extractants and additives associated with RE recovery through the -production have been addressed in the April 19 , 2021 and January 22, 2022 SERPs. -will be stored in -in one of the Mill's buildings or storage areas. The-storage drums/super sacks and product drums/super sacks will also be stored in one of the Mill buildings or storage areas. There are no reported incompatibilities for-and it can be stored near other products or reagents. 12.14.2022 Technical Memorandum Pg.08 product containers, and transport vehicles will undergo surface radiological scanning before leaving the Mill. Either product may potentially undergo analysis for uranium, thorium isotopes or other radiological constituent levels, if required by the customer, as has been done for vanadium products. 4.1 Compatibility ofREU Processing Chemicals with Mill Process and Equipment -As mentioned above, -has been used historically in the Mill laboratory but has not previously been introduced into the Mill's process circuits, so is evaluated here. Compatibility of all other chemicals has been evaluated in the SERPs of April 2021 and January 2022. , reacted with~ The precipitation reaction does not produce hazardous off-gases or byproducts. -has no recorded upper or lower explosive limit. -The only new product will be-. After it is produced in the~ide product will be packaged and will not be in further contact with any Mill chemicals or equipment. 5.0 Health and Safety in Mill Process As mentioned above, the only new chemical to be introduced in the RE separation process is -· Compatibility of all other chemicals with the Mill process have been evaluated in the SERPs of April 2021 and January 2022. The hazard properties of-and -are discussed in the attached Technical and Regulatory Review and summarized here . 5.1 - -in its -form is a nutrient present in edible plants such as parsley, chard, spinach, buckwheat, most nuts and berries, beans, and tea leaves. It's important in plant tissues 12.14.2022 Technica l M emorandum Pg.09 for its ability to bind and store minerals. It's also present in humic components of soils as the decay product of many other types of vegetation. For -in its dry powdere~ form, manufacturer SOSs recommend sufficient ventilation to keep occupational exposures lower than the limits below. The NIOSH REL and OSHA Permissible Exposure Limit ("PEL") for powder Threshold Limit Value ("TLV") Time Weighted Average ("TWA") is 1 mg/m3. The Short-Term Exposure Limit ("STEL") is 2 mg/m 3 . If ventilation is sufficient to maintain concentrations below these levels, no additional respiratory protection is required. Mill employees are experienced in working with far more corrosive agents, such as sulfuric acid (liquid), hydrochloric acid (liquid), and sodium hydroxide (powder and liquid solution). No additional protections will be required beyond the Mill's current worker protection measures for handling these types of materials. 5.2 - , are both considered to be of low to moderate toxicity. Neither has any published occupational exposure limits. SOS information does not require any specific respiratory protection or other personal protective equipment ("PPE") beyond common dust protection measures, such as gloves, safety glasses, and possible dust mask. No additional protections will be required beyond the Mill's current worker protection measures for powdered materials. 5.4 General/Other Neither-nor~products have been reported to be carcinogenic or teratogenic. An SOS for-should be added to the records available on site. An SOS will need to be developed or adapted for-product. I~ is sold as an -• an SOS needs to be developed. The proposed process will require operation o ~efore storage. The Mill currently operates two Mill personnel are trained in the use of this type of equipment. 12.14.2022 Technical Memorandum Pg.10 6.0 Environmental Considerations 6.1 Air Emissions is water soluble, will be added to an aqueous solution, and will react with .. solution. Any spills from bag handling would be immediately cleaned up. There will be no opportunity for dust or fugitive emissions, once it is added to the system. As discussed in previous SERPs, the RE-product will be a moist solid that will not generate dust or fugitive emissions. The-product will be packaged, sealed, and stored prior to sale and shipment off- site. The drums/bags will be stored in one of the Mill's storage areas. Any product spills will be cleaned up. I Either selection will require modification of the Mill's Air Approval Order ("AAO"). Either option may result in fewer air emissions th~ but not constructed, vanadium~hich it would replace. The .............. result in low enough air emissions that credit for an emissions offset, and reduced air permitting requirements and schedule, may be possible. The Mill will select an equipment type after design and price information is provided by the manufacturers in early 2023. The AAO and any required revisions are not part of, nor subject to, the Mill's RML. They are discussed in this assessment for the sake of completeness, but will be addressed separately. Depending on the length of time to complete selection, permitting, and construction of the -equipment, the Mill may package and ship .. as an -product until such time as the facilities are competed to producei. as the JIii product. 12.14.2022 Technical Memorandum Pg.11 6.2 Tailings Management System The April 19, 2021 SERP evaluated the addition of cations (such as Ba and Na), anions (such as-• at levels resulting from 15,000 TPY REU ore processing. The potential effect of the only additional additive, -is evaluated below. -As mentioned in Sectio~ was previously evaluated in the SERP of January 2022. Haxo, et. al. (EPA 1985) and Battelle Laboratories (Farnsworth and Hymas, 1989) and EPA (EPA, 1988) evaluated the performance of PVC and other vinyl and polyethylene liner materials in leachate solutions containing metals, salts, volatile hydrocarbons, as well as sulfuric and nitric acid environments in field tests in some cases up to 18 years exposure. Battelle's studies included assessment of resistance to acidic mixtures containing the which is the same functional group as in-including 0.05 molar phosphate, 0.05 molar sulfate, 0.1 molar chloride and in the presence of radionuclides. PVC had good retention of properties; polyethylene was unaffected. These conditions approximate or are more aggressive than the conditions in the Mill's tailings, and represent phosphate levels substantially higher than could be produced by ~ischarge from the Mill for the proposed Change evaluated in this memorandum. -As mentioned in Section 2.0, -will be added to react with the to produce , which will be to yield and, potentially, The Mill proposes to discharge process solutions from the proposed process to Cell 3 and/or Cell 4A, depending on conditions, capacities and recirculation. At the acidic conditions of the Mill's tailings discharge and cell solutions, - discharged to tailings from the small process excess would immediately react with dissolved metals such as iron, uranium, vanadium, and residual REs in the tailings solution to form would settle to the bottom of the tailings cells. Historica ll y , the Mill has used other forms of in the laboratory to Hence the Mill has historically been introducing At more aggressive acidic conditions, i.e., at higher sulfuric acid levels, immediately degraded to form inert molecules of presence of cations such as sodium or potassium, which are in the tailing solution, the CO2 will 12.14.2022 Technical Memorandum Pg.12 further be consumed in forming inert carbonates. That is, even in the most aggressive acidic tailings environment,_ will not fonn hazardous byproducts in the TMS. The EPA Risk Reduction Engineering Laboratory study cited above, (EPA, 1988) evaluated data from a number of short and long-tenn test studies on liner material behavior in leachate and waste solutions of As discussed above, PVC had good retention of properties; polyethylene was unaffected . It can be concluded that -will not have harmful effects on either the PVC or HDPE liners in the Mill's TMS. The only other mechanism by which a spill of aqueous solution. would reach the TMS would be by cleanup of which would be washed to the TMS in For conservatism, the introduction of a spill volume to the TMS has been estimated for each cell in Section 6.3, below, assuming the entire mass of a spill has been discharged to one cell, ether Cell 3 or Cell 4A. -Introduction of REs into the tailings system was evaluated in the SERPs of April 2021 and January 2022 . The only additional means for introduction of additional REs into the TMS is the cleanup of a spill of a product container of product. Potential worst-case spills are quantified in Section 6.3, below. These metals are already present in the TMS as residuals from 42 years of processing of conventional ores and alternate feeds from which they were not recovered as a product, but disposed as a process residual (tailings). Numerous studies, including those cited in the SERPs of April 2021 and January 2022 (e.g.,Famsworth and Hymas, 1989), demonstrate that both polyethylene and PVC are resistant to metal-metal carbonates, metal salts, and other inorganic compounds in all proportions even in the presence of fluorides, phosphate ions, sulfuric acid and elevated temperatures. It can be concluded that both the PVC and HDPE liners will have suitable resistivity to the minute concentrations of RE compounds that might reach the TMS from cleanup of a spill. Each of the chemicals or classes of chemicals proposed for use in the proposed process, which could reach the TMS is already present in the tailings system from historic operations. The following table summarizes the status of each chemical considered . 12.14.2022 Technical Memorandum Pg.13 Chemical Status --are already present in the tailings from historic use in the laboratory. Rare earths are already present in tailings from previous REU processing. Uranium and heavy RE residuals or spills metals, which are more mobile than any of the rare earths based on their lower soil partition coefficient KD values, are already monitored in groundwater. 6.3 Worst Case Spill Results and CERCLA/SARA Title II Section 302 Reportable Quantities (RQs) -If a full were spilled and washed to either Cell 3 or Cell 4A, the resulting concentration o in either cell would be immeasurably small compared to the mass of any tailing cell, approximately: As discussed above, -would not exist in the tailings environment as unreacted chemical. It would immediately react with and precipitate with metals in tailings and be present only in insoluble, immobile, metal -forms. Lithologic log s forthe Mill typically show that very shallow soils at the Mill react moderately to strong ly with dilute .; and deeper soils that presumably represent mainly weathered Mancos Shale, react strongly to very strongly with dilut •. If-were to be spilled directly on Mill soil the reactivity of the soils to dilute suggests relatively large calcium carbonate contents . -would react with calcium carbonate in soil to form insoluble preci.pitate,just as it would form metal-precipitates in tailings. Even if-were to be spilled directly on soil without calcium present, it would be rapidly biodegraded in soil ultimately into CO2, H2 and H20, with an environmental lifetime less than a few hours, even at full strength. It would have virtually no environmental effect even it was not remediated. 12.14.2022 Technical Memorandum Pg.14 However, all spills are subject to the Mill's spill response and spill documentation procedures. As mentioned in Section 7. I, below, -in soils is being evaluated for its potential to actually retard the environmental mobility of heavy metals and other contaminants. -A product spill o-would likewise be immeasurably small compared to the mass of any tailing cell. The published bulk density of a heavier Assuming a spill of a full 55-gallon drum of dry powder density with no beadspace would yiel . For conservatis m, this evaluation uses 1,000 lbs./drum, as follows. Cell 3 Cell 4A 1,000 lbs. (0.5 tons) /2.6 million tons= 0.000019% 1,000 lbs. (0.5 tons) /700,000 tons= 0.000071 % The above values are worst-case overestimates. As shown below, neither -nor the -product have any CERCLA reportable quantities ("RQ's") for a spill. Additive or Product - Worst Case Spill 6.4 Reclamation and Surety Considerations CERCLA RQ or Other Reporting Requirement -- The proposed Change will require new equipment and potentially an increase to the Mill building footprint. However, any new buildings would be constructed on previously-disturbed land . To the extent possible, at the termination of the RE program or at the end of Mill life, equipment will either be decontaminated for transport for offsite sale or will be disposed in a designated reclamation cell consistent with the Mill's approved Reclamation Plan. The reclamation volume and surety estimate will be reviewed in Spring 2023 to confirm it accommodates the volume of additional equipment associated with the RE process, and any required adjustments to the surety will be made at that time. 12.14.2022 Technical Memorandum Pg.15 The Mill currently assumes that the -which will not be in contact with any radioactive materials, will be decontaminated for sale and off-site transport. If for some reason it were to be disposed in the TMS, the Reclamation Surety estimate would be modified to address its volume and disposal cost. 6.5 Drainage and Surface Water As mentioned above, spills of-or product materials wou ld drain or be washed to the Mill's TMS . There are no RQs for off-site releases of-or 7.0 Consistency with License, Permits, Plans and SOPs. 7.1 Groundwater Discharge Permit ("GWDP") The products from the proposed process are all inorganic compounds except -As mentioned above, they could only reach the TMS via a spill. Each of the inorganic compounds is represented by an indicator chemical or cation that is monitored under the GWDP as discussed in the SERPS of April 2021 and January 2022. Each of the reagents, diluents and other chemicals used in the process have previously been evaluated in the SERPs of April 2021 and January 2022, except-. ·s the single new chemical proposed for use in the process. In nonnal operations, would be consumed by reaction with the stream and would be Unreacted would be discharged to tailings, but would reci itate immediately in the tailings, fonning insoluble As discussed above, i-reached the soil environment at the Mill it would react with calcium carbonate in Mill soil to form insoluble calcium -• just as it would fonn in tailings. Even if-were to be spilled or reach soils without calcium present, it would be rapidly biodegraded in soil ultimately into CO2, H2 and H2O, with an environmental lifetime less than a few hours, even at full strength. In either case, it would not exist long enough in the soil environment to reach groundwater. As a result, soil water partition coefficients, l<d, for-in alkaline or calciferous soils are not published. 12.14.2022 Technical Memorandum Pg.16 The Utah DWMRC December 1, 2004 Statement of Basis for the Mill's GWDP addressed which volatile organic compounds should be considered as monitoring parameters under the GWDP. After reviewing the historic data for chemical constituents known to be present in the Mill's TMS based on tailings analytical and historic process information, DWMRC selected a limited list of classes of volatile organic compounds ("VOCs") known to be present in tailings, which would be required to be monitored in groundwater, specifically two ketones, chlorinated VOCs, tetrahydrofuran, naphthalene, and BTEX compounds . DWMRC defended their selection of this list in order to streamline the agency's monitoring by focusing on parameters with known environmental persistence and very low Ki values in the literature, that is, parameters that are expected to be more mobile than, and can be expected to be indicators for, other species known to be present in the Mill's TMS. As discussed above, -has very limited environmental lifetime, and soil reactivity high enough that K,i values have not been published. At the conclusion of RE operations or the end of Mill life, any unused-would either be sold or potentially disposed in the TMS. If afull Cell 3 Cell 4A solution was disposed in Cell 3 or Cell 4A, the resulting in either cell would be immeasur ably sm a ll com pared to the mass Based on the m aximum so lubil ity of-in water, appro ximately: 1,000 lbs. (0.5 ton) /2.6 million tons= 0.000039% or 0.39 mg/kg 1,000 lbs. (0.5 ton)/700,000 tons= 0.000071% or 0.71 mg/kg In either case,just as with exce ss -d is charged from the process, any unused disposed -would reac t and precipitate as in soluble metal - No amendment of the GWDP will be required. 7.2 Air Approval Order ("AAO") As discussed in Section 6.1, any required revisions to the AAO will be evaluated following receipt of..ilJiesign information and selection of an appropriate equipment type, and are not the subject of this assessment. 7 .3 Other Permits, Plans and SOPs Based on the discussion above , the following documents may require amendments or revisions to address the proposed process: • Spill Prevention, Control and Countermeasures ("SPCC") Plan tables, 12.14.2022 Techn ical Memorandum • Stonnwater Best Management Practices Plan ("SWBMPP"), • SOPs, • Emergency Response Plan ("ERP"), • Tailings Capacity Evaluation, • Surety Estimate, • SOS books throughout the Mill. All needed items are listed in detail in the Action Item list in Section 10.0 of this memorandum. 8.0 Compliance with Other Regulations 8.1 Resource Conservation and Recovery Act (RCRA) Pg.17 RCRA regulates the treatment, storage and disposal of hazardous materials. -is not associated with any RCRA hazardous waste listings. are not associated with any RCRA hazardous waste listings. 8.2 Toxic Substances Control Act (TSCA) All chemicals identified for the proposed process have active status on the TSCA Chemical Substances Inventory, that is, they are approved for sale, use and transport. Each chemical is identified in the attached Technical and Regulatory Review. 8.3 Emergency Preparedness and Community Right-to-Know (EPCRA) Section 313 Toxic Release Inventory (TRI) Reporting Industries under SIC Code I 094, which include uranium, thorium and radium extraction and recovery, are exempt from reporting under EPCRA Section 313. 8.4 OSHA Hazard Communication Standards (HCS) The Occupational Safety and Health Administration ("OSHA") hazard communication standards ("HCS") in 29 CFR 1910 .1200, as accepted by MSHA, require that the Mill prepare an SOS for the product, . The Mill will also need to update all copies of the SDS binders to include 9.0 Sustainability Objectives The proposed Change represents an inherently sustainable opportunity as detailed below . 12.14.2022 Technical Memorandum Pg.18 First, the ongoing recovery of valuable REs by the processes and equipment currently in place at the Mill actually reduces the consumption of non-renewable resources. The Mill recovers RE products, such as the currently produced mixed RE _, from natural uranium monazite ore feeds, that are received at the Mill for the recovery of uranium product. Recovering of secondary products, such as REs, from the same ore source at the Mill does not require the excavation of new or expanded mining operations to provide the feedstock. The alternative to the proposed Change, that is, continuing the current method production, would require the Mill to continue producing REs as mixed RE RE urrently must be acka ed and shipped internationally to the The facility performs the additional processing steps to the and ultimately produce - -The must be repackaged for a second round of shipment to the customer facilities in the US or elsewhere. The Change would allow the Mill to separate the REs at the ~itate an -product at the Mill, and ultimately, produce a marketable 11111111111111 product at the Mill. The Change would therefore allow the Mill to: • Eliminate the RE _,roduction with associated consumption of chemicals and energy, • Eliminate one set of packaging steps with associated consumption of packaging materials, • Eliminate shipping of RE , therefore eliminating the consumption of fuel and generation of greenhouse gases ("GHGs") associated with international shipping, and • Eliminate shipping of product from -to US customers, allowing direct shipping from the Mill to US customers with overall reduction of fuel use and GHG generation. The Mill evaluated the proposed Changes in comparison to EFRI's specific sustainability objectives, including the following: • Will the Change be implemented with the least hazardous or non-hazardous chemicals? Yes. The Mill evaluated a number of precipitation agents for preparation of_ is both the most effective and least hazardous material that pplication, as discussed in Section 5.1. • Did the design of the change attempt to minimize the footprint of environmental disturbances? Yes. The Mill developed an equipment layout that reuses equipment to the extent possible, minimizes the need to construct pads or foundations outside the existing built areas, and does not require any construction outside the Mill's existing disturbed area. 12.14.2022 Technical Memo ra ndum Pg.19 10.0 Conclusions and Recommendations Based on the foregoing information, it can be concluded that: I . The proposed change will not produce any environmental impacts outside the envelope of those already addressed in the approved Environmental Reports ("ERs") for the Mill. No license amendment is required for the proposed change. 2 . The proposed Change generates no additional environmental emissions. Once the type of-equipment is specified, it will be determined whether the Change may produce fewer emissions than the previously-approved vanadium - which will be replaced in the AAO. 3 . All chemicals or material to be discharged to the TMS under the proposed change are already present in the tailings system and/or well represented by other analytes already monitored in the tailing solutions and under the GWDP., The proposed change will not require any modification of the Mill's GWDP. 4. No RCRA requirements apply to the proposed change . 5. All proposed materials are acceptable under TSCA. 6. As listed above, revisions will be required to certain documentation referred to in the RML application as itemized in Section 10.0, below. 7. The AAO revision, as required, will be addressed separately. 8. The proposed Change is consistent with the Mill's sustainability objectives. 11.0 Action Items Based on the above evaluation, the following action items need to be implemented. • Update the SPCC tables. • Update the SWBMPP. • Update the SOPs books to include appropriate additional SOPs. • Confirm the SOPs have been reviewed for proper PPE. 12.14.2022 Technical Memo ra ndum Pg.20 • Update the ERP. • Update the Tailings Capacity Evaluation. • Confirm or update the Surety estimate • Add SDSs for each of the new chemicals to be used or produced in the RE process, specifically: • is to be packaged and sold as an interim product, prepare an SDS for this product. 12.14.2022 Techn ical Memorandum Pg.21 11.0 References Dames & Moore Environmental Report White Mesa Uranium Mill San Juan County, Utah January 30, 1978 Farnsworth, R.K. and C.R. Hymas, August 1989 The Compatibility of Various Polymeric Liner and Pipe Materials with Simulated Double-Shell Slurry Feed at 900C. Pacific Northwest Laboratory, US. Department of Energy , Battelle Memorial Institute Haxo, H.E., Jr., Robert S. Haxo, Maney A. Nelson, Paul 0. Haxo, Richard M. White, and Suren Dakessian Liner Materials Exposed to Hazardous and Toxic Wastes US EPA Hazardous Waste Engineering Research Laboratory EPA-600/S2-94-169 January 1985 Impact Environmental Consultants, Inc. Amendment to Final Environmental Statement US Nuclear Regulatory Commission White Mesa Uranium Project May 1981 Lichty, D. M . Journal of Physical Chemistry 1907, 11, 3 , 225-272 accessed at hnps ://doi .org/10 .102 1/j l 50 08 4a 003 March J, 1907 McBride, Murray, Kelch, Sabrina, Michael Schmidt, et. al. Lead Solubility and Mineral Structures ofCoprecipitated Lead/Calcium Oxalates American Chemical Society Publications, Environmental Science & Technology Nov. 12, 2019 National Institute of Occupational Safety and Health Online NIOSH Pocket Guide to Chemical Hazards https ://www.c dc.go /nio sh/np g/se arch.html accessed November 2022 OSHA Hazard Communication Standards as stated in 29 CFR 1900.1200 Union Oil Company US Patent 4497785A Production of Rare Earth Compounds 1983 US EPA EPCRA Section 313 Chemical List for Reporting Year 2018, Table II 2019-03 accessed at h lt ps://ww w.ep a .gov/sites/p roduction/files/2019- 03/documents/ry 2018 tri chemical list.pdf 9/26/19 US EPA List of Lists Consolidated List of Chemicals Subject to EPCRA, CERCLA and CAA 550- B-19-03 June 2019 US EPA Toxic Substances Control Act Chemical Inventory Chemical Substance Inventory February 2019 US EPA, 1988. Risk Reduction Engineering Laboratory . Lining of Waste Containment and Other Impoundment Facilities EPN600/2-88/052 September 1988 12.14.2022 Technical Memorandum Pg.22 US Nuclear Regulatory Commission Environmental Assessment for Renewal of Source Material License SUA-1358 Energy Fuels Nuclear, Inc. White Mesa Uranium Mill March 14, 1997 Attachments • Attachment 1 Technical and Regulatory Review • Attachment 2 Safety Data Sheets Ir 12.14.2022 Technical Memorandum Pg.23 ACGIH AO CAA CCD CDC CERCLA EFRI EPCRA ER GWDP • HCS HDPE NIOSH OSHA PEL PPE PVC RCRA REE REU RML RQ SARA sos SERP SOP LIST OF ACRONYMS American Conference of Government Industrial Hygienists Air Approval Order Clean Air Act Counter Current Decantation Centers for Disease Control Comprehensive Environmental Restoration, Compensation and Liability Act ("Superfund") Energy Fuels Resources (USA) Inc. Emergency Preparedness and Community Right-to-Know Act Environmental Report Groundwater Discharge Permit Hazard Communication Standard High density polyethylene National Institute for Occupational Safety and Health Occupational Safety and Health Administration Permissible Exposure Limit Personnel Protective Equipment Polyvinyl Chloride Resource Conservation and Recovery Act Rare Earth Elements Rare Earth Bearing Uranium Ore Radioactive Material License Reportable Quantity Superfund Amendments and Reauthorization Act Safety Data Sheet Safety Environmental Review Panel Standard Operating Procedure 12.14.2022 Technical Memorandum SPCC STEL SWBMPP sx TLV TMS TRI TSCA TWA Spill Prevention, Control, and Countermeasure Plan Short-Term Exposure Limit Storm Water Best Management Practices Plan Solvent Extraction Threshold Limit Value Tailings Management System Toxic Release Inventory Toxic Substances Control Act Time-Weighted Average Pg.24 ATTACHMENT 1 TECHNICAL AND REGULATORY REVIEW Chemical and Regulatory Summary Chemical Composition Physical State Storage Location, Method, Quantity Where Introduced in Process, Quantity Used Properties Hazards Worst Case S Emissions Compatibility with Tailings Management System Solutions Compatibility with Tailings Management System Liners Compliance with RML, License Application RCRA/TSCA SARA Title II Section 302 R Section 313 TRI Reporting Other Regulatory Considerations References for- No flashpoint. Not flammable. Incompatible with strong acids, bases, oxidizers. Can form an explosive dust mixture with air. Keep surfaces free of dust. Will be added to the circuit and present in the circuit in solution only. Mist will be scrubbed by wet demister. No emissions to stacks. Will react with dissolved metals to form re will be no residual in solution. te as -and will not be accumulated or tact with the liners. cation • cipates other similar materials will be osed in taili (from laboratory). Not a RCRA hazardous waste. Not regulated under TSCA. No RQ in Consolidated List of Lists Not subject to TRI reporting. Uranium-vanadium-radium industries, SIC code I 094, are exempt from TRI reporting. No listin s in Consolidated List of Lists. None. US EPA EPCRA Section 313 Chemical List for Reporting Year 2018, Table II 2019-03 accessed at https://www.epa.gov/sites/production/files/2019 -03/documents/ry 2018 tri chemical list.pdf 4/6/2021 US EPA List of Lists Consolidated List of Chemicals Subject to EPCRA, CERCLA and CAA 550-B-19-03 June 2019 US EPA Toxic Substances Control Act Chemical Inventory Chemical Substance Inventory February 2019 Chemical and Regulatory Summary Chemical Com osition Physical State Storage Location, Method, Quantity Where Introduced in Process, Quantity Used Properties Hazards Worst Case S Emissions Compatibility with Tailings Management System Solutions Compatibility with Tailings Management System Liners Compliance with RML and License A lication Compliance with GWDP Compliance with AO RCRA/TSCA SARA Title Il Section 302 RQ Section 313 TRI Reporting Other Regulatory Considerations ntainers. One drum , 1,000 lbs. No stack emissions associated with process through- intennediate . to be determined for Air A roval Order, based on e ui ment selected. Compatible with solutions in all proportions. Compatible with liners in all proportions . -have been present in previously processed and a roved alternate feeds and some natural ores. Previous SERPs determined REs do not require amendment to GWDP. No dust or fugi tive emission thro ugh -pro duction step . Amen dment to AAO will be requir ed fo r-when selected. NoCERCLARQ Uranium-vanadium-radium industries, SIC code 1094, are exempt from TRI reporting. No TRI reporting requirements associated with rare earths. SDSs need to be developed for ~roduct, and potentially for roduct ifit is acka ed and sold in the interim . .__ _________________ _,___, References for CDC Center for Disease Control NIOSH National Institute for Occupational Safety and Health accessed at https://www .cdc.gov/niosh/npg/npgd0492.htm I 11/15/22 Union Oil Company US Patent 4497785A Production of Rare Earth Compounds 1983 USEPA EPCRA Section 313 Chemical List for Reporting Year 2018, Table II 2019-03 accessed at https://www.epa_gov /sites/production/fi les/20 19-03/documents/ry 2018 tri chemica l lis t.pdf 11/15/22 US EPA List of Lists Consolidated List of Chemicals Subject to EPCRA, CERCLA and CAA 550-B-19-03 June 2019 US EPA Toxic Substances Control Act Chemical Inventory Chemical Substance Inventory February 2019 ATTACHMENT 2 SAFETY DATA SHEETS 3 ---- - ---.. ------- ----"------- ;;: .------------- .________ ---'---___ ___. --I •L-----__._I _ -.,. - - ~---~----------' ;-----'------' LD50 Dermal •1 ACGIH I -I aj -·---------- ~~------'------' -.---------------1 -, I • I I I -1•1 ~ ·---- I ----- 7 - - I I Safety Data Sheet ------~------' I -- Safety Data Sheet --- Safeo/ Data Sheet - - - Safety Data Sheet - Safety Data Sheet -- Other information ATTACHMENT 2 -SOP White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 11 Rare Earth Preface Communication Date : 03-23 Revision: EFR-1 Page I of3 To be successful as an operator in achieving the desired results in your circuit, good communication between you, the metallurgical department, and your supervisor should exist. lnfonnation is given to the operator verbally, written and by test results. As an operator, if you do not understand any information given, you have the responsibility to ask questions until you do understand. White Board. In a few locations in the mill, critical information about mill operations will be written on White Boards. Information such as circuit parameters, required changes in circuit operations, or special instructions about maintenance. Circuit Sheets. Circuit sheets will have operating parameters on them along with sampling times for the circuit. They will also have a place for you to pass along written information about your circuit. Verbal. One of the most important times of your shift is at Shift Change. You have the responsibility to pass along information about your circuit to the person relieving you. You will be given verbal instructions from your supervisor or metallurgical department which you need to be sure you understand. Written. Instructions will be handed out in written fonn almost daily. As above, if you do not understand any instruction, ask your supervisor. HeaJth and Safety Hazards: • Acidic solutions • Elevated temperatures • Elevated work areas • Pressurized process lines • Pumps, if hose pumps are restricted on either the intake or discharge the hose will fail spraying solution. • Pumps, pumps requiring gland seal water if the gland seal water is not turned on the pump will fail. If the pump is off and the gland seal water is left on it will dilute process solutions and cause problems in the process. White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 11 - Personal Protective Equipment (PPE) Date : 03-23 Revision : EFR-1 Page 2 of3 1. Minimum PPE requirements at White Mesa Mill while in the restricted area is hard hats, safety glasses, and steel toed shoes. No ragged or lose fitting clothing is allowed. Body jewelry, rings, wrist watches, etc . are required to be removed while working. 2. Other personal protective equipment includes, but is not limited to: ear plugs, respirators, wet suits, welding helmets, goggles, gloves, and rubber boots. Face shields and safety belts are required in designated areas and/or while performing certain jobs. If in doubt, contact your supervisor . 3. Each employee is responsible for the condition of their protective equipment. Report any defects , etc., to your supervisor. 4. The following equipment is required when working on pipelines or vessels containing acids or caustics: a. Face shield and chemical splash goggles b. Rubber coat and pants c . Rubber gloves and rubber boots d. Other equipment specified by the foreman for that particular job listed on the Safe Work Permit 5. The use of a safety belt and properly adjusted lifeline is required where there is a danger of falling four feet or more, except while performing work under the ladder and scaffold section of this manual. This rule applies when going beyond the handrails of walkways on top of any tanks in the mill area. 6. It is a condition of employment that all personnel who may be required to wear a respirator must be clean shaven to assure that the respirator fits properly. Personnel will be fully trained consistent with the Mill's Respiratory Protection SOP, prior to using respirators . IMPORTANT: This pump is a hose (peristaltic) pump. This type of pump builds high pressures. The feed and discharge line and valves must be open before the pump is turned on or the discharge line or pump will fail. White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 11 - - ---- It is important to ensure that any samples taken are representative of the tank's contents. This means using clean sampling equipment and purging sample ports before sampling. Op erating In s tructions I . Conduct a proper Shift Change with the person you are relieving. Get information about all circuit parameters, including, but not limited to: temperature, feed flow rate, and tank levels. 2. I I I I I I I Start-up Procedures I I I I Shutdown Procedures I I Emergency Shut-down Procedures I I I White Mesa Mill-Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 12 - Communication Date: 03-23 Revision: EFR-1 Page 1 of4 To be successful as an operator in achieving the desired results in your circuit, good communication between you, the metallurgical department, and your supervisor should exist. Information is given to the operator verbally, written and by test results. As an operator, if you do not understand any information given, you have the responsibility to ask questions until you do understand. White Board. In a few locations in the mill, critical information about mill operations will be written on White Boards. Information such as circuit parameters, required changes in circuit operations, or special instructions about maintenance. Circuit Sheets. Circuit sheets will have operating parameters on them along with sampling times for the circuit. They will also have a place for you to pass along written information about your circuit. Verbal. One of the most important times of your shift is at Shift Change. You have the responsibility to pass along information about your circuit to the person relieving you. You will be given verbal instructions from your supervisor or metallurgical department which you need to be sure you understand. Written. Instructions will be handed out in written form almost daily. As above, if you do not understand any instruction, ask your supervisor. Health and Safety Hazards: • I • Stairs and elevated work areas • I White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 12 - Personal Protective Equipment (PPE) Date: 03-23 Revision: EFR-1 Page 2 of 4 l. Minimum PPE requirements at White Mesa Mill while in the restricted area is hard hats, safety glasses, and steel toed shoes. No ragged or lose fitting clothing is allowed. Body jewelry, rings, wrist watches, etc. are required to be removed while working. 2. Other personal protective equipment includes, but is not limited to: ear plugs, respirators, wet suits, welding helmets, goggles, gloves, and rubber boots. Face shields and safety belts are required in designated areas and/or while performing certain jobs. If in doubt, contact your supervisor. 3. Each employee is responsible for the condition of their protective equipment. Report any defects, etc., to your supervisor. 4. The following equipment is required when working on pipelines or vessels containing acids or caustics: a. Face shield and chemical splash goggles b. Rubber coat and pants c. Rubber gloves and rubber boots d. Other equipment specified by the foreman for that particular job listed on the Safe Work Permit 5. The use of a safety belt and properly adjusted lifeline is required where there is a danger of falling four feet or more, except while performing work under the ladder and scaffold section of this manual. This rule applies when going beyond the handrails of walkways on top of any tanks in the mill area. 6. It is a condition of employment that all personnel who may be required to wear a respirator must be clean shaven to assure that the respirator fits properly. Personnel will be fully trained consistent with the Mill's Respiratory Protection SOP, prior to using respirators. Equipment and Important Information White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 12 -- - I I -Sampling Sampling of the various solutions in this circuit is required on a regular basis. It is important to ensure that any sample taken is representative of the tank's contents. This means that tanks should be well mixed, sampling equipment should be clean, and any sample ports purged before collecting the sample. Operating Instructions l . Conduct a proper Shift Change with the person you are relieving. Get information about all circuit parameters, including, but not limited to: flow rates, tank levels, solution concentrations. 2. Perform a pre-work exam of the Inspect all lines and tanks for any leaks . Check all walkways and travel areas for general cleanliness. Ensure all process controls, readouts and safety showers are functioning properly. White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 12 - Date: 03-23 Revision: EFR-1 Page 4 of4 3. Check the process parameter targets. Remember that process parameters may have changed since the previous shift. 4. Check and record all flow rates and tanks levels on the Operator Sheet. 5. Ensure that the bench pH probe is calibrated and functional. 6. I 8. Adjust the recycle valves to achieve the specified organic to aqueous ratio in the mixers. 9. Sample the circuit as directed by the Metallurgical Departmen t. Start-up Procedures I I I I I I I Shutdown Procedures I I I I I I I I I Emergencv Shutdown Procedures I I White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 13 - Communication Date: 03-23 Revision: EFR-1 Page 1 of4 To be successful as an operator in achieving the desired results in your circuit, good communication between you, the metallurgical department, and your supervisor should exist. Information is given to the operator verbally, written and by test results. As an operator, if you do not understand any information given, you have the responsibility to ask questions until you do understand. White Board. In a few locations in the mill, critical information about mill operations will be written on White Boards. Information such as circuit parameters, required changes in circuit operations, or special instructions about maintenance. Circuit Sheets. Circuit sheets will have operating parameters on them along with sampling times for the circuit. They will also have a place for you to pass along written information about your circuit. Verbal. One of the most important times of your shift is at Shift Change. You have the responsibility to pass along information about your circuit to the person relieving you. You will be given verbal instructions from your supervisor or metallurgical department which you need to be sure you understand. Written. Instructions will be handed out in written form almost daily. As above, if you do not understand any instruction, ask your supervisor. Health and Safety Hazards: I I • Stairs and elevated work areas I I White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 13 - Personal Protective E quipment (PPE) Date: 03-23 Revision: EFR-1 Page2 of4 1. Minimum PPE requirements at White Mesa Mill while in the restricted area is hard hats, safety glasses, and steel toed shoes. No ragged or lose fitting clothing is allowed. Body jewelry, rings, wrist watches, etc. are required to be removed while working. 2. Other personal protective equipment includes, but is not limited to: ear plugs, respirators, wet suits, welding helmets, goggles, gloves, and rubber boots. Face shields and safety belts are required in designated areas and/or while performing certain jobs. If in doubt, contact your supervisor. 3. Each employee is responsible for the condition of their protective equipment. Report any defects , etc., to your supervisor. 4. The following equipment is required when working on pipelines or vessels containing acids or caustics: a. Face shield and chemical splash goggles b. Rubber coat and pants c. Rubber gloves and rubber boots d. Other equipment specified by the foreman for that particular job listed on the Safe Work Permit 5. The use of a safety belt and properly adjusted lifeline is required where there is a danger of falling four feet or more, except while performing work under the ladder and scaffold section of this manual. This rule applies when going beyond the handrails of walkways on top of any tanks in the mill area. 6. It is a condition of employment that all personnel who may be required to wear a respirator must be clean shaven to assure that the respirator fits properly . Personnel will be fully trained consistent with the Mill's Respiratory Protection SOP, prior to using respirators. White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 13 -- - I I -Sampling Sampling of the various solutions in this circuit is required on a regular basis. It is important to ensure that any sample taken is representative of the tank's contents. This means that tanks should be well mixed, sampling equipment should be clean, and any sample ports purged before collecting the sample. Operating Instructions 1. Conduct a proper Shift Change with the person you are relieving. Get information about all circuit parameters, including, but not limited to: flow rates, tank levels, solution concentrations. 2. Perform a pre-work exam of the Inspect all lines and tanks for any leaks. Check all walkways and travel areas for general cleanliness. Ensure all process controls, readouts and safety showers are functioning properly. White Mesa Mill -Uranium Bearing Rare Earth Ore Operating Procedures Book 15 Section 13 - Date: 03-23 Revision: EFR-1 Page 4 of4 3. Check the process parameter targets. Remember that process parameters may have changed since the previous shift. 4. Check and record all flow rates and tanks levels on the Operator Sheet. 5. Ensure that the bench pH probe is calibrated and functional. 6. I I I -the circuit as directed by the Metallurgical Department. 10. Start-up Procedures I I I I I I I I Shutdown Procedures I I I I I I I I Em.er encv Shutdown I I I