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HomeMy WebLinkAboutDSHW-2018-005076 - 0901a0688083be84Ititt UTAH DEPARTMENT OF HEALTH Final Results Div of NA-inagnrnent and Ro:l.ation Control JO 0 1 P 3 -195-10-2aek-x7b, Report To: Deborah Ng Division of Waste Management & Radiation Control ( DWMRC) PO BOX 144880 Salt Lake City, UT 84114 Bill To: Division of Waste Management & Radiation Control 195 North 1950 West Salt Lake City, UT 84114 Project ID: C2018-02009 Deborah Ng, Your sample(s) submitted to Utah Public Health Laboratory (UPHL) on Wednesday, May 16, 2018 were assigned the UPHL Project ID C2018-02009. Enclosed are the analytical results pertaining to that Project ID. Herein are the results relating only to the sample(s) received and tested for the project C2018-02009. All associated analyses were performed following the UPHL Quality Assurance Plan. This report and its contents have been reviewed and approved by the appropriate Laboratory Staff and Supervisor(s). This report shall not be reproduced, except in full, without the written permission of UPHL. If you have any questions regarding your results, please contact UPHL at (801) 965-2400 and reference the Project ID C2018-02009 Reviewed by: Kyle Ashby Reviewed on: 6/1/2018 ADDRESS 4431 South 2700 West, Taylorsville, UT 84129 PHONE. (801) 965-2400 FAX. (801) 965-2486 [Han Pi ihhr Hpalth I ahnratnry - r.hpmustry Z_UT_ProjectChemistryAnalytical.rpt Page 1 of 4 Fri, Jun 1, 2018 10:39 am Project Summary Report To: Deborah Ng (DWMRC_00) Division of Waste Management & Radiation Control ( DWMRC) PO BOX 144880 Salt Lake City, UT 84114 Phone: 801-536-0211 Fax: 801-538-6175 E-mail: dng@utah.gov Bill To: Division of Waste Management & Radiation Control 195 North 1950 West Salt Lake City, UT 84114 Phone: 801-538-6170 Fax: 801-538-6175 Project ID: C2018-02009 Project Notes: This project contains samples that were analyzed at a different laboratory. Please see the attached report for more information from that laboatory regarding your sample. Sample # Date Collected Date Received Facility Sampling Point Site Description 2125763 05/15/18 05/16/18 N/A N/A MW-109 2125769 05/15/18 05/16/18 N/A N/A MW-109 Z_UT_ProjectChemistryAnalytical rpt Page 2 of 4 Fri, Jun 1, 2018 10.39 am L.99, UTAH DEPARTMENT OF HEALTH Analytical Report Project ID: C2018-02009 Facility: N/A Sampling Point: N/A Site Description: MW-109 Sample ID: 2125763 Date Collected 5/15/2018 5:30:00PM Text ID: PSV18-0003 Collected By: ZHU, HAO Matrix: Water COC Initiated. Yes Bottle Type: Condition of Seal. Not Present SDWIS Type. Private Investigative Analysis Method - Pass Through EPA 8270 SVOCS Analyte Result Dil Fac Qualifier MDL MRL SRL Pass Through Laboratory ALS Environmental Laboratory Facility: N/A Sampling Point. N/A Site Description: MW-109 Sample ID: 2125769 Text ID: PV018-0003 Matrix: Water Bottle Type. Date Collected 5/15/2018 Collected By: ZHU, HAO COC Initiated: Yes Condition of Seal. Not Present 5:30:00PM SDWIS Type: Private Investigative Analysis Method - Pass Through EPA 8260 VOCs Analyte Result Dil Fac Qualifier MDL Pass Through Laboratory ALS Environmental Laboratory MRL SRL Z_UT_ProjectChemistryAnalytical.rpt Page 3 of 4 Fri, Jun 1, 2018 10.39 am „lb kt Report Project ID: C2018-02009 Notes UTAH DEPARTMENT OF HEALTH Report Comments This report contains only the results for analyses requested and tested. Unless otherwise noted: - Samples were received in acceptable condition - Samples have not been blank corrected. - All Quality Control Samples processed yielded acceptable results. Report Symbol Definitions MDL - Method Detection Limit, a statistically estimated concentration for instrument/method/matrix sensitivity. MRL - Method Reporting Limit, the minimum concentration that can be reported as a quantitated value. SRL - Sample Reporting Limit, the minimum concentration that can be reported as a quantitated value taking into account limitations inherent in the sample matrix. ND - Not Detected, tested result was not detected above MDL or MRL. < - Less than, tested result is less than the numerical value. Please take our customer satisfaction survey at https://www.surveymonkey.com/r/environmentalchemistry Z_UT_ProjectChernistryAnalytical rpt Page 4 of 4 Fri, Jun 1, 2018 10.39 am MK)-1/ 1A4R1 -ip 1 3 'apt,' 4=3ot* c-3001 6.. water water ikot-^ LEGAL CHAIN OF CUSTODY RECORD Project Name Pennzoil Refinery 1V4/ tAft.c. Sampler Name & Initials (PRINT): Zhu, Hao 66PNZ°1—C Phone No. 801-536-0249 email:hzhu@utah.gov dng@utah.gov Mailing Address: UDEQ/WMRC, 195 North 1950 West, 2nd Floor, SLC, UT 84114-4880 Section CAS 1_2 Cost Code call Sheila Person to Address Report / Questions To: Zhu, Hao State of Utah Unified State Laboratories: Public Health Bureau of Chemical and Environmental Services Telephone: 801.965.2400 FAX: 801.969.3238 LAB USE ONLY MAY 1612 14:56 City: Salt Lake City Field ID or Location ST: UT Date Sampled Time (Mil) Phone No. (801) 536-0200 Matrix 27_7a t. 1-Lb # of Containers a 826 0 : V O C s cJ 827 0: S VO C s $59 61±) c' a a cJ Use this space for comments: a a cJ cJ a LAB Sample Number Tamper Seal Intact (Y or N) Comments (Temp.,Leaks, etc.) 1111MMENERIlli 2125761 PSV18 —00018 - 111 11111111111110111111 II 1112125762 PSV18 — 0002B El llflllllllitiillllliillfllltl 2125763 — El 111 lllIlllllllilllllJllllllll 2125766 — PV018 —0001D lllillllllllllllllllllllllllili 2125768 - El pvn1R — own 1111111111111111111111111111111 2125769 PVC/18-00030 05-15-18 0S16-11ek coriik Zip: 84114 a cJ a a 1.3 cJ cJ cJ a a LJ a a a a cJ a cJ cJ cJ a a a a a LJ DS H W r e v - 1.2.1 Z? 244v 1.1,4_ G4--ctSe Saat4-e Ler ou204.4-5( .5%A.A.of ow this oont cd /Le c-41 a‘A.,_ 51- . D. • Relinquished By: Print Name »: Date Time /c-F = 4.6, Received By: Invoice / Airbill # Print Name »: Date Time Relinquished By: Print Name »: Date Time Received By: Invoice / Airbill # — — — Print Name » Date0510_eslime /v.... Invoice /Aribill # Relinquished By: Print Name »: Date Time Received By LAB: — — — Print Name »: —Date Time Relinquishyd y: Relinq ish41 By: Relinquished By: Date and Time: 5 7/6 r Date and Time: Date and Time: d by: ived by: Received by: Dca3te leT 4 i,n4:8 Date and Time: Date and Time: 11111111111.11111111_31111111111- Unified State Laboratories: Public Health Bureau of Chemical and Environmental Services 4431 S 2700 W Taylorsville, UT 84129 801-965-2400 Fax 801-969-.3238 https://health.utah.gov/lab/chem lab CHAIN OF CUSTODY .,(6 0-136 El Hand Delivered El Shipped Samples EJ Cooler Returned System/Agency Name: System/Agency Number: Cost/ roject Code: Received Date and Time: REQUESTED TESTS REPORTING/CONTACT BILLING (list if difierent) Attn: Kyle Ashby Special Code: Address: 4431 S 2700 W Attn: Tiffany Shields Email: kdashbvutah.gov 11 0 0 0 1= 1 1 21: 1 0 ( 1, City, State, Zip: Taylorsville, Utah, 84129 Address: 4431 S 2700 W Sample Receipt Conditions No EI Documentation complete O Proper containers and in-date O Containers intact I=1 Within holding time El Coolant O Temperature within-range El Acceptable pH El N/A 1=l Custody Seals Intact LAB NUMBER 2125766 2125768 2125769 2125761 2125762 2125763 Re c e ip t t e mp er atu re EP A 8 2 6 0: VO C s EPA 8 2 70 : SV O C s Phone. 801-965-2400 City, State, Zip: Taylorsville Utah 8419 Fax: 801-969-3238 Phone: 801-965-2400 i,onection Date immmalvv) 05/15/18 05/15/18 05/15/18 05/15/18 05/15/18 05/15/18 Fax: Submitted By: K.D. Ashby Collectors Initials COLLECTION POINT DESCRIPTION Email: tshieldsautah.c1W Collection Time (24 hr) COMMENTS MW-11 MW-24 MW-109 MW-11 MW-24 MW-109 15:15 16:30 17:30 15:15 16:30 17:30 ALS-SALT LAKE CITY-RELATED INFORMATION REPORT CRIR COOLER OR CONTA R INFORMATION CHECKLIST (Fill In or Circle) Client Name.• {(A.)\64--t.; Project/Task/Site: l CS(035* Date/Time of Receipt: 1.31tr1g ((0.1Sli Number of Coolers Received: 1 Condition of Coolers: (Lc e/Unacceptable Temperature Control: Present/N chi& Cooler Custody Seals: Present/ A 1ntact1Bro'nsTÄ Location Temp Taken: Control/Be een S. i les Container Custody Seals: Present/ t/Broke Are all temperatures within Yes/NoW Ice Present: /NA project specific guidelines? roze elted/NA VOA Headspace Present? Ye /N A pH Check Metals es/No/NA Total Phenolics Yes/No/NA NO3/NO2 Yes/No/NA Performed: Cyanide Yes/No/NA TPH — 418.1 Yes/No/NA Oil & Grease Yes/No/NA Sulfide Yes/No/NA COD Yes/No/NA Total Phosphorous Yes/No/NA Ammonia Yes/No/NA TKN Yes/No/NA Gross A.B, Gamma Spec Yes/No/NA Cooler Cooler Cooler Received DCL Cooler No. Temp. Iteceived DCL Cooler No. Temp Received pa, Cooler No. Temp. 1 C18 61-4- 10 °C 4 C18 °C 7 C18 °C 2 C18 .0 5 C18 °C 8 C18 °C 3 C18 °C 6 C18 °C 9 C18 °C Taken By: signamm Printed Name Dale CLIENT-RELATED INFORMATION 0 Missing Cooler 0 Cooler Conditions 0 Missing Paperwork 0 Missing/Incorrect Bottle Labels 0 Missing Samples/Bottles Out D Incorrect Preservation 0 pH Criteria Not Met 0 Insufficient Sample Volume 0 Chain of Custody Problems 0 Other: II Broken/Leaking Samples 0 Incorrect Bottle Type El Residual Chlorine Present 0 Head Space in Bottles III Cooler Temperatures of Range BRIEFLY DESCRIBE THE PROBLEM AND THE ACTION TAKEN: 0)It i i ja4 - P L rit 4/ 0 tja 6 Wdl ( Client Notified? YES ii No l=1 Response Required Within 24 Hours PROJECT MANAGEMENT PROJECT MANAGER COMMENTS: ALS Project Manager: Returned to Sample Receipt by: Date: PnntedName sipature CR1R.doe Revised 01/01/2018 ANALYTICAL REPORT Report Date: May 31, 2018 Kyle Ashby Unified State Laboratories Bureau of Chemical and Env Ser 4431 S 2700 W Salt Lake City, UT 84119-8600 Phone: (801) 965-2400 E-mail: kdashby@utah.gov Workorder: 34-1813735 %lent Sample ID a' Lab ID Collect Date Project ID: Utah Dept of Health Purchase Order: NA Project Manager Kevin W. Griffiths Receive Date Sampling Site MW-11 1813735001 05/15/18 05/16/18 2125766 MW-24 1813735002 05/15/18 05/16/18 2125768 MW-109 1813735003 05/15/18 05/16/18 2125769 MW-11 1813735004 05/15/18 05/16/18 2125761 MW-24 1813735005 05/15/18 05/16/18 2125762 MW-109 1813735006 05/15/18 05/16/18 2125763 ADDRESS 960 West LeVoy Drive, Salt Lake City, Utah, 841 23 USA j PHONE +1 801 266 7700 FAX +1 801 268 9992 ALS GROUP USA, CORP. An ALS Limited Company ipicolionmerstal RIGHT soLuTions Page 1 of 19 Thu, 05/31/18 3:21 PM ENVREP-V4.8 ANALYTICAL REPORT Workorder: 34-1813735 Client: Utah Department of Health Project Manager: Kevin W. Griffiths Analytical Results Sample ID: MW-11 Lab ID: 1813735001 Matrix: Water Sampling Site: 2125766 Media: 40 mL Amber Glass VOA Sampling Parameter: NA Collected: 05/15/2018 Received: 05/16/2018 Atialiiielhotlt;1SW, 8260 Preparation: Not Applicable Analysis: SW 8260C, Water Batch: EVO/7139 (HBN: 214983) Analyzed: 05/17/2018 13:45 Instrument ID: 5975-J Percent Solid: NA Report Basis: Wet 'Analyte Result (ug/L) MDL (ug/L) RL (ug/L) Dilution Qual Dichlorodifluoromethane ND 0.30 1.0 1 U Chloromethane ND 0.30 1.0 1 U Vinyl chloride ND 0.30 1.0 1 U Bromomethane ND 0.30 1.0 1 U Chloroethane ND 0.30 1.0 1 U Dichlorofluoromethane ND 0.30 1.0 1 U Trichlorofluoromethane ND 0.30 1.0 1 U Ethyl ether . ND 0.30 1.0 1 U 1,1-Dichloroethene ND 0.30 1 0 1 U Freon 113 ND 0.30 1.0 1 U Acetone ND 1.5 5.0 1 U lodomethane ND 0.30 1.0 1 U Carbon disulfide ND 0.30 1.0 1 U Methyl Acetate ND 1.5 5.0 1 U Ally! chloride ND 0.30 1.0 1 U Methylene chloride ND 0.30 1.0 1 U trans-1,2-Dichloroethene ND 0.30 1.0 1 U Methyl-t-butyl ether ND 0.30 1.0 1 U cis-1,2-Dichloroethene ND 0.30 1.0 1 U 1,1-Dichloroethane ND 0.30 1.0 1 U 2,2-Dichloropropane ND 0.30 1.0 1 U 2-Butanone ND 1.6 5.0 1 U Ethyl acetate ND 1.5 5.0 1 U Bromochloromethane ND 0.30 1.0 1 U Tetrahydrofuran ND 2.1 5.0 1 U Chloroform ND 0.30 1.0 1 U 1,1,1-Trichloroethane ND 0.30 1.0 1 U Cyclohexane 9.6 0.30 1 0 1 1,1-Dichloropropene ND 0 30 1.0 1 U 1,2-Dichloroethane ND 0.30 1.0 1 U Carbon tetrachloride ND 0.30 1.0 1 U Benzene 21 0.30 1.0 1 Trichloroethene ND 0.30 1.0 1 U Methylcyclohexane 3.0 0.30 1.0 1 1,2-Dichloropropane ND 0.30 1.0 1 U Results Continued on Next Page Page 2 of 19 Thu, 05/31/18 3:21 PM ENVREP-V4.8 ANALYTICAL REPORT Workorder: 34-1813735 Client: Utah Department of Health Project Manager: Kevin W. Griffiths Analytical Results Sample ID: MW-11 Lab ID: 1813735001 Matrix: Water Sampling Site: 2125766 Media: 40 mL Amber Glass VOA Sampling Parameter: NA Collected: 05/15/2018 Received: 05/16/2018 rAff*SiiiMettiod SW_826:0 5910AMaanWit„ _ . Preparation: Not Applicable Analysis: SW 8260C, Water Batch: EVO/7139 (HBN: 214983) Analyzed: 05/17/2018 13:45 Instrument ID: 5975-J Percent Solid: NA Report Basis: Wet r Analyte Result (ug/L) NIDL (ug/L RL (ug/L) Dilution Qual Dibromomethane ND 0.30 1.0 1 U Bromodichloromethane ND 0.30 1.0 1 U cis-1,3-Dichloropropene ND 0.30 1.0 1 U 4-Methy1-2-pentanone ND 1.5 5.0 1 U trans-1,3-Dichloropropene ND 0.30 1 0 1 U Ethyl methacrylate ND 0.30 1 0 1 U 1,1,2-Trichloroethane ND 0.30 1.0 1 U 2-Hexanone ND 1.5 5.0 1 U 1,2-Dibromoethane ND 0.30 1.0 1 U Toluene ND 0 30 1.0 1 U 1,3-Dichloropropane ND 0.30 1.0 1 U Dibromochloromethane ND 0 30 1.0 1 U Bromoform ND 0.30 1.0 1 U Tetrachloroethene ND 0.30 1.0 1 U 1-Chlorohexane ND 0.30 1.0 1 U Chlorobenzene ND 0.30 1.0 1 U 1,1,1,2-Tetrachloroethane ND 0.30 1.0 1 U Ethylbenzene 2.9 0.30 1 0 1 m,p-Xylene ND 0.30 2.0 1 U o-Xylene 1.9 0.30 1 0 1 Styrene ND 0.30 1.0 1 U lsopropylbenzene 0.74 0.30 1.0 1 J 1,1,2,2-Tetrachloroethane ND 0.30 1.0 1 U Bromobenzene ND 0.30 1.0 1 U 1,2,3-Trichloropropane ND 0.30 1.0 1 U trans-1,4-Dichloro-2-butene ND 1 5 5.0 1 U Pentachloroethane ND 0.30 1.0 1 U n-Propylbenzene 0 41 0.30 1.0 1 J 1,3,5-Trimethylbenzene ND 0.30 1.0 1 U 2-Chlorotoluene ND 0.30 1 0 1 U 4-Chlorotoluene ND 0.30 1.0 1 U tert-Butylbenzene ND 0.30 1.0 1 U 1,2,4-Trimethylbenzene ND 0.30 1.0 1 U sec-Butylbenzene ND 0.30 1.0 1 U p-lsopropyltoluene ND 0.30 1.0 1 U Results Continued on Next Page Page 3 of 19 Thu, 05/31/18 3.21 PM ENVREP-V4.8 ANALYTICAL REPORT Workorder: 34-1813735 Client: Utah Department of Health Project Manager: Kevin W. Griffiths Analytical Results Sample ID: MW-11 Lab ID: 1813735001 Matrix: Water Sampling Site: 2125766 Collected: 05/15/2018 Media: 40 mL Amber Glass VOA Received: 05/16/2018 Sampling Parameter: NA rAiiiiiiiiiMletff-64,L1SW8260 . '' . ,,ItaZit:, MST ' le r Preparation: Not Applicable Analysis: SW 8260C, Water Batch: EVO/7139 (HBN: 214983) Analyzed: 05/17/2018 13:45 Instrument ID: 5975-J Percent Solid: NA Report Basis: Wet 'An 1 Result (ug/L) MDL (ug/L) RL (ugh.) Dilution Quai 1,3-Dichlorobenzene ND 0.30 1.0 1 U 1,4-Dichlorobenzene ND 0.30 1.0 1 U n-Butylbenzene ND 0.30 1.0 1 U 1,2-Dichlorobenzene ND 0.30 1.0 1 U 1,2-Dibromo-3-Chloropropane ND 1.5 5.0 1 U 1,2,4-Trichlorobenzene ND 0.30 1.0 1 U Hexachlorobutadiene ND 0.30 1.0 1 U Naphthalene ND 0.36 1.0 1 U 1,2,3-Trichlorobenzene ND 0.30 1.0 1 U Sample ID: MW-24 Lab ID: 1813735002 Matrix: Water Sampling Site: 2125768 Media: 40 mL Amber Glass VOA Sampling Parameter: NA Collected: 05/15/2018 Received: 05/16/2018 cAtiAliiiiilMithoit SVitt8260 tRIVATEW - 'WV:9Sr- Préparation: Not Applicable • Analysis: SW 8260C, Water Batch: EVO/7139 (HBN: 214983) Analyzed: 05/17/2018 14:18 Instrument ID: 5975-J Percent Solid: NA Report Basis: Wet Analyte Result (ug/L) lkfiDL (ug/L RL (ug/L) Dilution Qual . 1,2-Dichloroethane 480 6.0 20 20 Benzene 1200 6.0 20 20 AffališreltithoilW 8260 itrAZ 44$04%,. ATM Preparation: NM Applieable Analysis: SW 8260C, Water Batch: EVO/7139 (HBN: 214983) Analyzed: 05/17/2018 14:34 Instrument ID: 5975-J Percent Solid: NA Report Basis: Wet P. Analyte Result (ug/L) MDL (ug/L) RL (ug/L) Dilution Qual Dichlorodifluoromethane ND 0.60 2.0 2 U Chloromethane ND 0.60 2.0 2 U Vinyl chloride ND 0.60 2 0 2 U Bromomethane ND 0.60 2.0 2 U Chloroethane 3.2 0.60 2.0 2 Dichlorofluoromethane ND 0.60 2.0 2 U Trichlorofluoromethane ND 0.60 2.0 2 U Ethyl ether 2.6 0.60 2.0 2 1,1-Dichloroethene ND 0.60 2.0 2 U Freon 113 ND 0.60 2.0 2 U Acetone ND 3.0 10 2 U Results Continued on Next Page Page 4 of 19 Thu, 05/31/18 3.21 PM ENVREP-V4.8 ANALYTICAL REPORT Workorder: 34-1813735 Client: Utah Department of Health Project Manager: Kevin W. Griffiths Analytical Results Sample ID: MW-24 Lab ID: 1813735002 Matrix: Water Sampling Site: 2125768 Media: 40 mL Amber Glass VOA Sampling Parameter: NA Collected: 05/15/2018 Received: 05/16/2018 Analiiiilkethod - SW 8260 WORIP414- •:g -‘ - . v . Preparation: Not Applicable Analysis: SW 8260C, Water Batch: EV0/7139 (HBN: 214983) Analyzed: 05/17/2018 14:34 Instrument ID: 5975-J Percent Solid: NA Report Basis: Wet Analyte Result (ug/L) MDL (ugh.) RL (ug/L) Dilution Qual lodomethane ND 0.60 2.0 2 U Carbon disulfide ND 0.60 2.0 2 U Methyl Acetate ND 3.0 10 2 U Allyl chloride ND 0.60 2.0 2 U Methylene chloride ND 0.60 2.0 2 U trans-1,2-Dichloroethene ND 0.60 2.0 2 U Methyl-t-butyl ether 4.5 0.60 2.0 2 cis-1,2-Dichloroethene ND 0.60 2.0 2 U 1,1-Dichloroethane ND 0.60 2.0 2 U 2,2-Dichloropropane ND 0.60 2 0 2 U 2-Butanone ND 3.2 10 2 U Ethyl acetate ND 3.0 10 2 U Bromochloromethane ND 0 60 2.0 2 U Tetrahydrofuran ND 4 2 10 2 U Chloroform ND 0.60 2.0 2 U 1,1,1-Trichloroethane ND 0.60 2.0 2 U Cyclohexane 90 0.60 2.0 2 1,1-Dichloropropene ND 0.60 2.0 2 U Carbon tetrachloride ND 0.60 2.0 2 U Trichloroethene ND 0.60 2.0 2 U Methylcyclohexane 47 0.60 2.0 2 1,2-Dichloropropane ND 0.60 2.0 2 U Dibromomethane ND 0.60 2.0 2 U Bromodichloromethane ND 0.60 2.0 2 U cis-1,3-Dichloropropene ND 0.60 2.0 2 U 4-Methy1-2-pentanone ND 3.0 10 2 U trans-1,3-Dichloropropene ND 0.60 2.0 2 U Ethyl methacrylate ND 0.60 2 0 2 U 1,1,2-Trichloroethane ND 0.60 2.0 2 U 2-Hexanone ND 3.0 10 2 U 1,2-Dibromoethane ND 0.60 2.0 2 U Toluene 11 0.60 2.0 2 1,3-Dichloropropane ND 0.60 2.0 2 U Dibromochloromethane ND 0.60 2.0 2 U Bromoform ND 0.60 2.0 2 U Results Continued on Next Page Page 5 of 19 Thu, 05/31/18 3.21 PM ENVREP-V4.8 ANALYTICAL REPORT Workorder: 34-1813735 Client: Utah Department of Health Project Manager: Kevin W. Griffiths Analytical Results Sample ID: MW-24 Lab ID: 1813735002 Matrix: Water Sampling Site: 2125768 Collected: 05/15/2018 Media: 40 mL Amber Glass VOA Received: 05/16/2018 Sampling Parameter: NA lkiiitMettiogl - $W 8260 • Wiegtiar Preparation: Not Applicable Analysis: SW 8260C, Water Batch: EVO/7139 (HBN: 214983)‘ Analyzed: 05/17/2018 14:34 Instrument ID: 5975-J Percent Solid: NA Report Basis: Wet lAnalyte Result (ug/L) MDL (ug/L RL (ug/L) Dilution Qua! Tetrachloroethene ND 0.60 2 0 2 U 1-Chlorohexane ND 0.60 2.0 2 U Chlorobenzene ND 0.60 2.0 2 U 1,1,1,2-Tetrachloroethane ND 0.60 2.0 2 U Ethylbenzene 120 0.60 2.0 2 m,p-Xylene 110 0.60 4.0 2 o-Xylene 4.7 0.60 2.0 2 Styrene ND 0.60 2.0 2 U lsopropylbenzene 4.5 0.60 2.0 2 1,1,2,2-Tetrachloroethane ND 0.60 2.0 2 U Bromobenzene ND 0 60 2 0 2 U 1,2,3-Trichloropropane ND 0.60 2.0 2 U trans-1,4-Dichloro-2-butene ND 3.0 10 2 U Pentachloroethane ND 0.60 2.0 2 U n-Propylbenzene 11 0.60 2.0 2 1,3,5-Trimethylbenzene 79 0.60 2.0 2 2-Chlorotoluene ND 0 60 2.0 2 U 4-Chlorotoluene ND 0.60 2.0 2 U tert-Butylbenzene ND 0.60 2.0 2 U 1,2,4-Trimethylbenzene 100 0.60 2.0 2 sec-Butylbenzene 0.71 0.60 2.0 2 J p-lsopropyltoluene 0.67 0.60 2.0 2 J 1,3-Dichlorobenzene ND 0 60 2.0 2 U '1 ,4-Dichlorobenzene ND 0.60 2.0 2 U n-Butylbenzene 1.4 0.60 2.0 2 J 1,2-Dichlorobenzene ND 0.60 2.0 2 U 1,2-Dibromo-3-Chloropropane ND 3.0 10 2 U 1,2,4-Trichlorobenzene ND 0.60 2.0 2 U Hexachlorobutadiene ND 0.60 2.0 2 U Naphthalene 72 0.72 2.0 2 1,2,3-Trichlorobenzene ND 0.60 2.0 2 U Page 6 of 19 Thu, 05/31/18 3:21 PM ENVREP-V4.8 ANALYTICAL REPORT Workorder: 34A813735 Client: Utah Department of Health Project Manager: Kevin W. Griffiths Analytical Results Sample ID: MW-109 Lab ID: 1813735003 Matrix: Water Sampling Site: 2125769 Media: 40 mL Amber Glass VOA Sampling Parameter: NA Collected: 05/15/2018 Received: 05/16/2018 4-iiiilViji-Pilittiod - SW 3200 Preparation: Not Applicable Analysis: SW 8260C, Water Batch: EV0/7139 (HBN: 214983) Analyzed: 05/17/2018 14:01 Instrument ID: 5975-J Percent Solid: NA Report Basis: Wet 'Analyte Result (ug/L) MDL (ug/L) RL (ug/L) Dilution Qual Dichlorodifluoromethane ND 0.30 1.0 1 U Chloromethane ND 0.30 1.0 1 U Vinyl chloride ND 0.30 1.0 1 U Bromomethane ND 0.30 1.0 1 U Chloroethane ND 0.30 1.0 1 U Dichlorofluoromethane ND 0.30 1.0 1 U Trichlorofluoromethane ND 0.30 1.0 1 U Ethyl ether ND 0.30 1.0 1 U 1,1-Dichloroethene ND 0.30 1.0 1 U Freon 113 ND 0.30 1.0 1 U Acetone 16 1.5 5 0 1 lodomethane ND 0.30 1.0 1 U Carbon disulfide ND 0.30 1.0 1 U Methyl Acetate ND 1.5 5.0 1 U Allyl chloride ND 0.30 1.0 1 U Methylene chloride ND 0.30 1.0 1 U trans-1,2-Dichloroethene ND 0.30 1.0 1 U Methyl-t-butyl ether ND 0.30 1.0 1 U cis-1,2-Dichloroethene ND 0.30 1.0 1 U 1,1-Dichloroethane ND 0.30 1.0 1 U 2,2-Dichloropropane ND 0.30 1 0 1 U 2-Butanone ND 1.6 5.0 1 U Ethyl acetate ND 1.5 5.0 1 U Bromochloromethane ND 0.30 1.0 1 U Tetrahydrofuran ND 2.1 5.0 1 U Chloroform ND 0.30 1.0 1 U 1,1,1-Trichloroethane ND 0 30 1.0 1 U Cyclohexane ND 0.30 1.0 1 U 1,1-Dichloropropene ND 0.30 1.0 1 U 1,2-Dichloroethane 17 0 30 1.0 1 Carbon tetrachloride ND 0 30 1.0 1 U Benzene 4.0 0.30 1.0 1 Trichloroethene ND 0.30 1 0 1 U Methylcyclohexane ND 0.30 1.0 1 U 1,2-Dichloropropane ND 0.30 1.0 1 U Results Continued on Next Page Page 7 of 19 Thu, 05/31/18 3.21 PM ENVREP-V4 8 ANALYTICAL REPORT Workorder: 34-1813735 Client: Utah Department of Health Project Manager: Kevin W. Griffiths Analytical Results Sample ID: MW-109 Lab ID: 1813735003 Matrix: Water Sampling Site: 2125769 Media: 40 mL Amber Glass VOA Sampling Parameter: NA Collected: 05/15/2018 Received: 05/16/2018 AnalYSW-Method - SW,8200 _ Preparation: Not Applicable Analysis: SW 8260C, Water Batch: EVO/7139 (HBN: 214983) Analyzed: 05/17/2018 14:01 Instrument ID: 5975-J Percent Solid: NA Report Basis: Wet Analyte Result (ug/L) MDL (ug/L) RL (ug/L) Dilution Qua! Dibromomethane ND 0.30 1.0 1 U Bromodichloromethane ND 0 30 1.0 1 U cis-1,3-Dichloropropene ND 0.30 1.0 1 U 4-Methy1-2-pentanone ND 1.5 5.0 1 U trans-1,3-Dichloropropene ND 0.30 1.0 1 U Ethyl methacrylate ND 0 30 1.0 1 U 1,1,2-Trichloroethane ND 0.30 1.0 1 U 2-Hexanone ND 1.5 5.0 1 U 1,2-Dibromoethane ND 0.30 1.0 1 U Toluene ND 0.30 1.0 1 U 1,3-Dichloropropane ND 0.30 1.0 1 U Dibromochloromethane ND 0.30 1 0 1 U Bromoform ND 0.30 1.0 1 U Tetrachloroethene ND 0.30 1.0 1 U 1-Chlorohexane ND 0.30 1.0 1 U Chlorobenzene ND 0.30 1.0 1 U 1,1,1,2-Tetrachloroethane ND 0.30 1.0 1 U Ethylbenzene ND 0.30 1.0 1 U m,p-Xylene ND 0.30 2 0 1 U o-Xylene ND 0.30 1.0 1 U Styrene ND 0.30 1.0 1 U lsopropylbenzene 3.4 0.30 1.0 1 1,1,2,2-Tetrachloroethane ND 0.30 1.0 1 U Bromobenzene ND 0.30 1.0 1 U 1,2,3-Trichloropropane ND 0.30 1.0 1 U trans-1,4-Dichloro-2-butene ND 1.5 5.0 1 U Pentachloroethane ND 0.30 1.0 1 U n-Propylbenzene ND 0.30 1.0 1 U 1,3,5-Trimethylbenzene ND 0.30 1.0 1 U 2-Chlorotoluene ND 0.30 1.0 1 U 4-Chlorotoluene ND 0.30 1.0 1 U tert-Butylbenzene ND 0.30 1.0 1 U 1,2,4-Trimethylbenzene ND 0.30 1.0 1 U sec-Butylbenzene 2.5 0.30 1.0 1 p-lsopropyltoluene ND 0.30 1.0 1 U Results Continued on Next Page Page 8 of 19 Thu, 05/31/18 3:21 PM ENVREP-V4 8 ANALYTICAL REPORT Workorder: 34-1813735 Client: Utah Department of Health Project Manager: Kevin W. Griffiths Analytical Results Sample ID: MW-109 Lab ID: 1813735003 Matrix: Water Sampling Site: 2125769 Media: 40 mL Amber Glass VOA Sampling Parameter: NA Collected: 05/15/2018 Received: 05/16/2018 AtifilVSESIlettiod SW82:80 ittritme&%-,,ykttatin,.-, _ • • Preparation: Not Applicable Analysis: SW 8260C, Water Batch: EV0/7139 (FIBN: 214983) Analyzed: 05/17/2018 14:01 Instrument ID: 5975-J Percent Solid: NA Report Basis: Wet 'Analyte Result (ug/L) MM. (ug/L) RL (ug/L) Dilution Qual 1,3-Dichlorobenzene ND 0.30 1.0 1 U 1,4-Dichlorobenzene ND 0.30 1.0 1 U n-Butylbenzene ND 0.30 1.0 1 U 1,2-Dichlorobenzene ND 0.30 1.0 1 U 1,2-Dibromo-3-Chloropropane ND 1.5 5.0 1 U 1,2,4-Trichlorobenzene ND 0.30 1.0 1 U Hexachlorobutadiene ND 0.30 1.0 1 U Naphthalene ND 0.36 1.0 1 U 1,2,3-Trichlorobenzene ND 0.30 1.0 1 U Sample ID: MW-11 Lab ID: 1813735004 Matrix: Water Sampling Site: 2125761 Media: 1000 mL Amber Glass Sampling Parameter: NA Collected: 05/15/2018 Received: 05/16/2018 Arialiiiiethod - SW 8270 Preparation: EPA 3510, Sep Funnel SVOA Batch: ENVX/26778 (HBN: 215063) Prepared: 05/18/2018 Weight/Volume Analysis: SW 8270D, Water Batch: ESVO/6416 (HBN: 215718) Analyzed: 05/29/2018 18:12 Instrument ID: 5975-H Percent Solid: NA Report Basis: Wet Initial: 1000 mL Final: 1 mL Analyte Result (ug/L) MDL (ug/L) RL (ug/L) Dilution Qua! Pyridine ND 1.5 5 0 1 U Phenol ND 1.5 5.0 1 U Bis(2-chloroethyl)ether ND 1.5 5 0 1 U 2-Chlorophenol ND 1.5 5.0 1 U 1,3-Dichlorobenzene ND 1.5 5.0 1 U 1,4-Dichlorobenzene ND 1.5 5.0 1 U Benzyl alcohol ND 1 5 5.0 1 U 1,2-Dichlorobenzene ND 1.5 5.0 1 U 2-Methylphenol ND 1.5 5 0 1 U bis(2-Chloroisopropyl)ether ND 1.5 5.0 1 U 4-Methylphenol ND 1.5 5.0 1 U N-Nitrosodi-n-propyl amine ND 1.5 5.0 1 U Hexachloroethane ND 1.5 5.0 1 U Nitrobenzene ND 1.5 5.0 1 U lsophorone ND 1.5 5.0 1 U 2-Nitrophenol ND 1.5 5.0 1 U 2,4-Dimethylphenol ND 1.7 5.0 1 U Results Continued on Next Page Page 9 of 19 Thu, 05/31/18 3.21 PM ENVREP-V4 8 ANALYTICAL REPORT Workorder: 34-1813735 Client: Utah Department of Health Project Manager: Kevin W. Griffiths Analytical Results Sample ID: MW-11 Lab ID: 1813735004 Matrix: Water Sampling Site: 2125761 Collected: 05/15/2018 Media: 1000 mL Amber Glass Received: 05/16/2018 Sampling Parameter: NA AliiiiiMethod SWIM -allyir- -TRWAftiff Preparation: EPA 3510, Sep Funnel SVOA Batch: ENVX/26778 (HBN: 215063) Prepared: 05/18/2018 Weioht/Volume Analysis: SW 8270D, Water Batch: ESVO/6416 (HBN: 215718) Analyzed: 05/29/2018 18:12 Instrument ID: 5975-H Percent Solid: NA Report Basis: Wet Initial: 1000 mL Final: 1 mL Analyte Result (ug/L) MDL (ug/L) RL (ug/L) Dilution Qual F' A Benzoic acid ND 15 20 1 U Bis(2-Chloroethoxy)methane ND 1.5 5.0 1 U 2,4-Dichlorophenol ND 1.5 5.0 1 U 1,2,4-Trichlorobenzene ND 1.5 5.0 1 U Naphthalene ND 1.5 5.0 1 U 4-Chloroaniline ND 1.5 5.0 1 U Hexachlorobutadiene ND 1.8 5.0 1 U 4-Chloro-3-methylphenol ND 1.5 5.0 1 U 2-Methylnaphthalene ND 1.5 5.0 1 U Hexachlorocyclopentadiene ND 1.7 5 0 1 U 2,4,6-Trichlorophenol ND 1.5 5.0 1 U 2,4,5-Trichlorophenol ND 1 5 5.0 1 U 2-Chloronaphthalene ND 1.5 5.0 1 U 2-Nitroaniline ND 1.5 5.0 1 U Dimethylphthalate ND 1.5 5.0 1 U 2,6-Dinitrotoluene ND 1.5 5.0 1 U Acenaphthylene ND 1.5 5.0 1 U 3-Nitroaniline ND 1.5 5.0 1 U Acenaphthene ND 1 5 5.0 1 U 2,4-Dinitrophenol ND 11 20 1 U 4-Nitrophenol ND 7.5 20 1 U Dibenzofuran ND 1.5 5.0 1 U 2,4-Dinitrotoluene ND 1.5 5.0 1 U Diethylphthalate ND 1.5 5.0 1 U 4-Chlorophenyl phenyl ether ND 1.5 5.0 1 U Fluorene ND 1.5 5.0 1 U 4-Nitroaniline ND 1.5 5.0 1 U 4,6-Dinitro-2-methylphenol ND 7.6 20 1 U N-Nitrosodiphenylamine ND 1.5 5.0 1 U 4-Bromophenyl phenyl ether ND 1.5 5.0 1 U Hexachlorobenzene ND 1.5 5.0 1 U Pentachlorophenol ND 7 5 20 1 U Phenanthrene ND 1.5 5.0 1 U Anthracene ND 1.5 5.0 1 U Carbazole ND 1.5 5.0 1 U Results Continued on Next Page Page 10 of 19 Thu, 05/31/18 3:21 PM ENVREP-V4.8 ANALYTICAL REPORT Workorder: 34-1813735 Client: Utah Department of Health Project Manager: Kevin W. Griffiths Analytical Results Sample ID: MW-11 Lab ID: 1813735004 Matrix: Water Sampling Site: 2125761 Media: 1000 mL Amber Glass Sampling Parameter: NA Collected: 05/15/2018 Received: 05/16/2018 rAllfarÿiwnithoasyv 8270 - WINAPINZP Preparation: EPA 3510, Sep Funnel SVOA Batch: ENVX/26778 (HBN: 215063) Prepared: 05/18/2018 WeiahtNolume Analysis: SW 8270D, Water Batch: ESVO/6416 (HBN: 215718) Analyzed: 05/29/2018 18:12 InstrUment ID: 5975-H Percent Solid: NA Report Basis: Wet Initial: 1000 mL Final: 1 mL 'Analyte Result (ug/L) MDL (ug/L) RL (ug/L) Dilution Qual Di-n-butylphthalate ND 1.5 5.0 1 U Fluoranthene ND 1.5 5.0 1 U Pyrene ND 1 5 5.0 1 U Butylbenzylphthalate ND 1.5 5.0 1 U 3,3'-Dichlorobenzidine ND 1.6 5.0 1 U Benzo(a)anthracene ND 1.5 5 0 1 U Chrysene ND 1.5 5.0 1 U Bis(2-ethylhexyl)phthalate ND 1.5 5 0 1 U Di-n-octylphthalate ND 1.5 5.0 1 U Benzo(b)fluoranthene ND 1.5 5.0 1 U Benzo(k)fluoranthene ND 1.5 5.0 1 U Benzo(a)pyrene ND 1.5 5.0 1 U indeno(1,2,3-c,d)pyrene ND 1.5 5.0 1 U Dibenzo(a,h)anthracene ND 1.5 5.0 1 U Benzo(g,h,i)perylene ND 1.5 5.0 1 U ?•.AtialliSikitiathidiiiiS,W,'827,0 daak..A.1 PreparatiOn: EPA 3510, Sep Funnel SVOA Batch: ENVX/26778 (HBN: 215063) Prepared: 05/18/2018 Weiaht/Volume Analysis: SW 82700, Water Batch: ESVO/6416 (HBN: 215718) Analyzed: 05/29/2018 18:12 Instrument ID: 5975-H Percent Solid: NA Report Basis: Wet Initial: 1000 mL Final: 1 mL o Tentatively identified Compound Retention Result (ug/L) Time Dilution Qual i Unknown Aromatic Acid 12 10.76 1 J Unknown Aromatic Acid 8.7 11.01 1 J Unknown Aromatic Acid 18 11.18 1 J Unknown Aromatic Acid 19 11.24 1 J Unknown Aromatic Acid 30 11.36 1 J Benzene, 1-methoxy-4-phenoxy- 33 11.41 1 J 1-Hydroxy-4-methyl-2-oxo-1,2- dihydro-3-quinoline 34 11.44 1 J Unknown Aromatic Acid 18 11.49 1 J Unknown Aromatic Acid 34 11.67 1 J Unknown Aromatic Acid 26 11.75 1 J Unknown Aromatic Acid 20 11.79 1 J Unknown Aromatic Acid 29 11.82 1 J Unknown Aromatic Acid 32 11.85 1 J Unknown Aromatic Acid 5.9 11.90 1 J Unknown Aromatic Acid 7.1 11.98 1 J Results Continued on Next Page Page 11 of 19 Thu, 05/31/18 3:21 PM ENVREP-V4 8 ANALYTICAL REPORT Workorder: 34-1813735 Client: Utah Department of Health Project Manager: Kevin W. Griffiths Analytical Results Sample ID: MW-11 Lab ID: 1813735004 Matrix: Water Sampling Site: 2125761 Collected: 05/15/2018 Media: 1000 mL Amber Glass Received: 05/16/2018 Sampling Parameter: NA MalielOattiod - SW 8270 • . ---- --4,2=210isttc Preparation: EPA 3510', Sep Funnel SVOA Batch: ENVX/26778 (HBN: 215063) Prepared: 05/18/2018 Weight/Volume Analysis: SW 8270D, Water Batch: ESVO/6416 (HBN: 215718) Analyzed: 05/29/2018 18:12 Instrument ID: 5975-H Percent Solid: NA Report Basis: Wet Initial: 1000 mL Final: 1 mL it Tentatively Identified Compound Retention Result (ug/L) Time Dilution Qual Unknown Aromatic Acid 25 12.09 1 J Unknown Aromatic Acid 26 12.14 1 J Unknown Aromatic Hydrocarbon 6.6 17.35 1 J Unknown Aromatic Hydrocarbon 5.9 17 57 1 J Sample ID: MW-24 Lab ID: 1813735005 Matrix: Water Sampling Site: 2125762 Media: 1000 mL Amber Glass Sampling Parameter: NA Collected: 05/15/2018 Received: 05/16/2018 LAria101e,,Metliiid - SW 8270 Preparation: EPA 3510, Sep Funnel SVOA Batch: ENVX/26778 (HBN: 215063) 05/18/2018 ,prepared: WeightNolume Analysis: SW 8270D, Water Batch: ESVO/6416 (HBN: 215718) Analyzed: 05/29/2018 18:44 Instrument ID: 5975-H Percent Solid: NA Report Basis: Wet Initial: 1000 mL Final: 1 mL 1 Ania e Result (ug/L) MDL (ug/L RL (ugh.) Dilution Qual Pyridine ND 1 5 5.0 1 U Phenol ND 1.5 5.0 1 U Bis(2-chloroethyl)ether ND 1.5 5.0 1 U 2-Chlorophenol ND 1.5 5.0 1 U 1,3-Dichlorobenzene ND 1.5 5.0 1 U 1,4-Dichlorobenzene ND 1.5 5.0 1 U Benzyl alcohol ND 1.5 5.0 1 U 1,2-Dichlorobenzene ND 1.5 5.0 1 U 2-Methylphenol ND 1.5 5.0 1 U bis(2-Chloroisopropyl)ether ND 1.5 5.0 1 U 4-Methylphenol ND 1.5 5.0 1 U N-Nitrosodi-n-propyl amine ND 1.5 5.0 1 U Hexachloroethane ND 1.5 5.0 1 U Nitrobenzene ND 1.5 5.0 1 U lsophorone ND 1.5 5.0 1 U 2-Nitrophenol ND 1.5 5.0 1 U 2,4-Dimethylphenol ND 1.7 5.0 1 U Benzoic acid ND 15 20 1 U Bis(2-Chloroethoxy)methane ND 1 5 5.0 1 U 2,4-Dichlorophenol ND 1.5 5.0 1 U 1,2,4-Trichlorobenzene ND 1.5 5.0 1 U Results Continued on Next Page Page 12 of 19 Thu, 05/31/18 3:21 PM ENVREP-V4.8 ANALYTICAL REPORT Workorder: 34-1813735 Client: Utah Department of Health Project Manager: Kevin W. Griffiths Analytical Results Sample ID: MW-24 Lab ID: 1813735005 Matrix: Water Sampling Site: 2125762 Collected: 05/15/2018 Media: 1000 mL Amber Glass Received: 05/16/2018 Sampling Parameter: NA WtialYiti:MethVd SW8271) 1.111er lretitUdit ,. Preparation: EPA 3510, Sep Funnel SVOA Batch: ENVX/26778 (HBN: 215063) Prepared: 05/18/2018 WeightNolume Analysis: SW 8270D, Water Batch: ESVO/6416 (HBN: 215718) Analyzed: 05/29/2018 18:44 Instrument ID: 5975-H Percent Solid: NA Report Basis: Wet Initial: 1000 mL Final: 1 mL 'Analyte Result (ug/L) MDL (ug/L RL (ug/L) Dilution Qual Naphthalene 35 1.5 5.0 1 4-Chloroaniline ND 1.5 5.0 1 U Hexachlorobutadiene ND 1.8 5.0 1 U 4-Chloro-3-methylphenol ND 1.5 5.0 1 U 2-Methylnaphthalene 20 1.5 5.0 1 Hexachlorocyclopentadiene ND 1.7 5.0 1 U 2,4,6-Trichlorophenol ND 1.5 5.0 1 U 2,4,5-Trichlorophenol ND 1.5 5 0 1 U 2-Chloronaphthalene ND 1.5 5.0 1 U 2-Nitroaniline ND 1.5 5.0 1 U Dimethylphthalate ND 1.5 5.0 1 U 2,6-Dinitrotoluene ND 1.5 5.0 1 U Acenaphthylene ND 1.5 5.0 1 U 3-Nitroaniline ND 1.5 5.0 1 U Acenaphthene ND 1.5 5.0 1 U 2,4-Dinitrophenol ND 11 20 1 U 4-Nitrophenol ND 7.5 20 1 U Dibenzofuran ND 1.5 5.0 1 U 2,4-Dinitrotoluene ND 1.5 5.0 1 U Diethylphthalate ND 1.5 5.0 1 U 4-Chlorophenyl phenyl ether ND 1.5 5.0 1 U Fluorene ND 1.5 5 0 1 U 4-Nitroaniline ND 1.5 5.0 1 U 4,6-Dinitro-2-methylphenol ND 7.6 20 1 U N-Nitrosodiphenylamine ND 1.5 5.0 1 U 4-Bromophenyl phenyl ether ND 1.5 5.0 1 U Hexachlorobenzene ND 1.5 5.0 1 U Pentachlorophenol ND 7 5 20 1 U Phenanthrene ND 1.5 5 0 1 U Anthracene ND 1.5 5.0 1 U Carbazole ND 1.5 5.0 1 U Di-n-butylphthalate ND 1.5 5.0 1 U Fluoranthene ND 1.5 5.0 1 U Pyrene ND 1.5 5.0 1 U Butylbenzylphthalate ND 1.5 5.0 1 U Results Continued on Next Page Page 13 of 19 Thu, 05/31/18 3:21 PM ENVREP-V4.8 ANALYTICAL REPORT Workorder: 34-1813735 Client: Utah Department of Health Project Manager: Kevin W. Griffiths Analytical Results Sample ID: MW-24 Lab ID: 1813735005 Matrix: Water Sampling Site: 2125762 Media: 1000 mL Amber Glass Sampling Parameter: NA Collected: 05/15/2018 Received: 05/16/2018 AtialÿšiSIMithiad - SW1270 4 t MT:Waal Preparation: EPA 3510, Sep Funnel SVOA Batch: ENVX/26778 (HBN: 215063) Prepared: 05/18/2018 Weight/Volume Analysis: SW 8270D, Water Batch; ESVO/6416 (HBN: 215718) Analyzed: 05/29/2018 18:44 Instrument ID: 5975-H Percent Solid: NA Report Basis: Wet Initial: 1000 mL Final: 1 mL Analyte Result (ug/L) MDL (ug/L) RL (ug/L) Dilution i Qual 3,3'-Dichlorobenzidine ND 1 6 5.0 1 U Benzo(a)anthracene ND 1.5 5.0 1 U Chrysene ND 1.5 5.0 1 U Bis(2-ethylhexyl)phthalate ND 1.5 5.0 1 U Di-n-octylphthalate ND 1.5 5.0 1 U Benzo(b)fluoranthene ND 1.5 5.0 1 U Benzo(k)fluoranthene ND 1.5 5.0 1 U Benzo(a)pyrene ND 1.5 5.0 1 U Indeno(1,2,3-c,d)pyrene ND 1.5 5.0 1 U Dibenzo(a,h)anthracene ND 1.5 5.0 1 U Benzo(g,h,l)perylene ND 1.5 5.0 1 U '1!ittiališts!,Met1iod SW 8:270 A Preparation: EPA 3510, Sep Funnel SVOA Batch: ENVX/26778 (HBN: 215063) Prepared: 05/18/2018 Weight/Volume Analysis: SW 8270D, Water Batch: ESVO/6416 (HBN: 215718) Analyzed: 05/29/2018 18:44 Instrument ID: 5975-H Percent Solid: NA Report. Basis: Wet Initial: 1000 mL Final: 1 mL Tentatively Identified Compound Retention Result (ug/L) Time Dilution Qual Unknown Organic Acid 39 4.50 1 J Unknown Organic Acid 50 4.53 1 J Ethylbenzene 36 4.92 1 J Mesitylene 20 5.91 1 J 2-Cyclopenten-1-one, 3,4-dimethyl- 85 6.12 1 J Benzene, 1,2,3-trimethyl- 50 6.36 1 J lndane 23 6.50 1 J 2-Cyclopenten-1-one, 3,4,5-trimethyl- 50 6.63 1 J Ethanone, 1-(1-cyclohexen-1-y1)- 92 6.85 1 J Mequinol 22 6.93 1 J Ethanamine, N-cyclohexylidene- 18 6.95 1 J 1H-Indene, 1-methyl- 26 7.34 1 J 3-tert-Buty1-2-pyrazolin-5-one 22 7.69 1 J 7-Methylindan-1-one 67 8.97 1 J 2-Pentanone, 3-(phenylmethylene)- 25 9.11 1 J Benzoic acid, 2,4,5-trimethyl- 19 9.29 1 J 4'42-Methylpropypacetophenone 36 9.50 1 J Unknown 17 9.76 1 J 2,3,5,6-Tetramethylbenzoic acid 26 9.81 1 J Results Continued on Next Page Page 14 of 19 Thu, 05/31/18 3:21 PM ENVREP-V4.8 ANALYTICAL REPORT Workorder: 34-1813735 Client: Utah Department of Health Project Manager: Kevin W. Griffiths Analytical Results Sample ID: MW-24 Lab ID: 1813735005 Matrix: Water Sampling Site: 2125762 Media: 1000 mL Amber Glass Sampling Parameter: NA Collected: 05/15/2018 Received: 05/16/2018 .4t4ialfili;Metbod•- SW;8270 Preparation: EPA 3510, Sep Funnel SVOA Batch: ENVX/26778 (HBN. 215063) Prepared: 05/18/2018 WeightNolume Analysis: SW 8270D, Water Batch: ESVO/6416 (HBN: 215718) Analyzed: 05/29/2018 18:44 Instrument ID: 5975-H Percent Solid: NA Report Basis: Wet Initial: 1000 mL Final: 1 mL ..-, Tentatively Identified Compound Retention Result (ug/L) Time Dilution Qua] 5-Aminoindan 18 10.33 1 J Sample ID: MW-109 Lab ID: 1813735006 Matrix: Water Sampling Site: 2125763 Media: 1000 mL Amber Glass Sampling Parameter: NA Collected: 05/15/2018 Received: 05/16/2018 AnalYareAlethp,d - SIN um Ad veva Preparation: EPA 3510, Sep Funnel SVOA Batch: ENVX/26778 (HBN: 215063) Prepared: 05/18/2018 Weiaht/Volume Analysis: SW 8270D, Water Batch: ESVO/6416 (HBN: 215718) Analyzed: 05/29/2018 19:17 Instrument ID: 5975-H Percent Solid: NA Report Basis: Wet Initial: 1000 mL Final: 1 mL Analyte Result (ug/L) MDL (ug/L) RL (ug/L) Dilution Qual Pyridine ND 1 5 5.0 1 U Phenol ND 1.5 5.0 1 U Bis(2-chloroethyl)ether ND 1 5 5.0 1 U 2-Chlorophenol ND 1.5 5.0 1 U 1,3-Dichlorobenzene ND 1.5 5.0 1 U 1,4-Dichlorobenzene ND 1.5 5.0 1 U Benzyl alcohol ND 1.5 5 0 1 U 1,2-Dichlorobenzene ND 1.5 5.0 1 U 2-Methylphenol ND 1.5 5.0 1 U bis(2-Chloroisopropyl)ether ND 1.5 5.0 1 U 4-Methylphenol ND 1.5 5.0 1 U N-Nitrosodi-n-propyl amine ND 1.5 5.0 1 U Hexachloroethane ND 1.5 5.0 1 U Nitrobenzene ND 1.5 5.0 1 U lsophorone ND 1.5 5.0 1 U 2-Nitrophenol ND 1.5 5.0 1 U 2,4-Dimethylphenol ND 1.7 5.0 1 U Benzoic acid ND 15 20 1 U Bis(2-Chloroethoxy)methane ND 1.5 5.0 1 U 2,4-Dichlorophenol ND 1.5 5.0 1 U 1,2,4-Trichlorobenzene ND 1.5 5.0 1 U Naphthalene 2.4 1.5 5.0 1 J 4-Chloroaniline ND 1 5 5.0 1 U Hexachlorobutadiene ND 1.8 5.0 1 U Results Continued on Next Page Page 15 of 19 Thu, 05/31/18 3:21 PM ENVREP-V4.8 ANALYTICAL REPORT Workorder: 34-1813735 Client: Utah Department of Health Project Manager: Kevin W. Griffiths Analytical Results Sample ID: MW-109 Lab ID: 1813735006 Matrix: Water Sampling Site: 2125763 Collected: 05/15/2018 Media: 1000 mL Amber Glass Received: 05/16/2018 Sampling Parameter: NA rAtia1y'siiiNfetho WO • ..tvw2s, -'4LYMSEtaZr Preparation: EPA 3510, Sep Funnel SVOA Batch: ENVX/26778 (HBN: 215063) Prepared: 05/18/2018 Weight/Volume Analysis: SW 8270D, Water Batch: ESVO/6416 (HBN: 215718) Analyzed: 05/29/2018 19:17 Instrument ID: 5975-H Percent Solid: NA Report Basis: Wet Initial: 1000 mL Final: 1 mL lAnalyte Result (ug/L) MDL (ug/L) RL Dilution Qual 4-Chloro-3-methylphenol ND 1.5 5.0 1 U 2-Methylnaphthalene ND 1.5 5.0 1 U Hexachlorocyclopentadiene ND 1.7 5.0 1 U 2,4,6-Trichlorophenol ND 1.5 5.0 1 U 2,4,5-Trichlorophenol ND 1.5 5 0 1 U 2-Chloronaphthalene ND 1.5 5.0 1 U 2-Nitroaniline ND 1.5 5.0 1 U Dimethylphthalate ND 1.5 5.0 1 U 2,6-Dinitrotoluene ND 1.5 5.0 1 U Acenaphthylene ND 1.5 5.0 1 U 3-Nitroaniline ND 1.5 5 0 1 U Acenaphthene ND 1.5 5.0 1 U 2,4-Dinitrophenol ND 11 20 1 U 4-Nitrophenol ND 7.5 20 1 U Dibenzofuran ND 1.5 5.0 1 U 2,4-Dinitrotoluene ND 1 5 5.0 1 U Diethylphthalate ND 1.5 5.0 1 U 4-Chlorophenyl phenyl ether ND 1.5 5.0 1 U Fluorene ND 1.5 5.0 1 U 4-Nitroaniline ND 1.5 5.0 1 U 4,6-Dinitro-2-methylphenol ND 7.6 20 1 U N-Nitrosodiphenylamine ND 1.5 5.0 1 U 4-Bromophenyl phenyl ether ND 1.5 5.0 1 U Hexachlorobenzene ND 1.5 5.0 1 U Pentachlorophenol ND 7.5 20 1 U Phenanthrene ND 1.5 5.0 1 U Anthracene ND 1.5 5.0 1 U Carbazole ND 1.5 5.0 1 U Di-n-butylphthalate ND 1.5 5.0 1 U Fluoranthene ND 1.5 5.0 1 U Pyrene ND 1.5 5.0 1 U Butylbenzylphthalate ND 1.5 5.0 1 U 3,3'-Dichlorobenzidine ND 1.6 5.0 1 U Benzo(a)anthracene ND 1.5 5.0 1 U Chrysene ND 1.5 5.0 1 U Results Continued on Next Page Page 16 of 19 Thu, 05/31/18 3:21 PM ENVREP-V4.8 ANALYTICAL REPORT Workorder: 34-1813735 Client: Utah Department of Health Project Manager: Kevin W. Griffiths Analytical Results Sample ID: MW-109 Lab ID: 1813735006 Matrix: Water Sampling Site: 2125763 Media: 1000 mL Amber Glass Sampling Parameter: NA Collected: 05/15/2018 Received: 05/16/2018 AfiarMithOd•- SW,8270 Preparation: EPA 3510, Sep Funnel SVOA Batch: ENVX/26778 (HBN: 215063) Prepared: 05/18/2018 weight/Volume Analysis: SW 8270D, Water Batch: ESVO/6416 (HBN: 215718) Analyzed: 05/29/2018 19:17 Instrument ID: 5975-H Percent Solid: NA Report Basis: Wet Initial: 1000 mL Final: 1 mL 'Analyte Result (ug/L) MDL (ug/L' RL (ug/L) Dilution Qual Bis(2-ethylhexyl)phthalate ND 1.5 5.0 1 U Di-n-octylphthalate ND 1.5 5.0 1 U Benzo(b)fluoranthene ND 1.5 5.0 1 U Benzo(k)fluoranthene ND 1.5 5.0 1 U Benzo(a)pyrene ND 1.5 5.0 1 U Indeno(1,2,3-c,d)pyrene ND 1.5 5.0 1 U Dibenzo(a,h)anthracene ND 1.5 5.0 1 U Benzo(g,h,i)perylene ND 1.5 5.0 1 u Aiiiiiiiioeitiii,a,:w.,:8170 Preparation: EPA 3510, Sep Funnel SVOA Batch: ENVX/26778 (HBN: 215063) Prepared: 05/18/2018 WeiohtNolume Analysis: SW 8270D, Water Batch: ESVO/6416 (HBN: 215718) Analyzed: 05/29/2018 19:17 Instrument ID: 5975-H Percent Solid: NA Report Basis: Wet initial: 1000 mL Final: 1 mL Tentatively identified Compound Retention Result (ug/L) Time Dilution Qual 1,2-Ethanediol, monoacetate 4.4 4.72 1 J Ethanone, 1-(1-cyclohexen-1-yI)- 5.9 6.83 1 J 3-Hexene-2,5-dione 4.2 6.92 1 J Comments Workorder: 1813735 8260 Comments: Sample 1813735002 (MW-24) was analyzed solely at dilution to bring the analytes of interest within the linear range and to preserve instrument integrity. Quality Control: SW 8260 - (HBN: 214983) 8260 QC Comments: The percent difference (or percent drift for a regression fit) for target compounds in the CVS standard must generally be less than 20% relative to the average response from the initial calibration curve. The analyte acetone did not meet this criteria and results for this compound should be considered estimates. Quality Control: SW 8270 - (HBN: 215718) The initial calibration did not pass method criteria for 3-nitroaniline, 4-nitroaniline, and carbazole. The CCV did not pass method criteria for 2,4-dimethylphenol, 4-chloroaniline, 3-nitroaniline, 2,4-dinitrophenol, and 4-nitroaniline. Any results for these compounds should be treated as semi-quantitative. The LCSD was outside of percent recovery QC limits for 3-nitroaniline and 2,4-dinitrophenol. RPD was outside of QC limits for 6 compounds. Report Authorization (/S/ is an electronic signature that complies with 21 CFR Part 11) Method Analyst Peer Remiew SW 8260 /S/ Christopher Q. Coleman /S/ Thomas J. Masoian 05/18/2018 11:21 05/22/2018 08:33 Page 17 of 19 Thu, 05/31/18 3:21 PM ENVREP-V4.8 ANALYTICAL REPORT Workorder: 34-1813735 Client: Utah Department of Health Project Manager: Kevin W. Griffiths Report Authorization (/S/ is an electronic signature that complies with 21 CFR Part 11) -3Kt: Peer Review /S/ Thomas J. Masoian 05/31/2018 11:37 05/31/2018 14:57 AnaiyAt /S/ David Teynor Laboratory Contact Information ALS Environmental 960 W Levoy Drive Salt Lake City, Utah 84123 Phone: (801) 266-7700 Email: alslt.lab@ALSGlobal.com Web: www.alsslc.com General Lab Comments The results provided in this report relate only to the items tested. Samples were received in acceptable condition unless otherwise noted. Samples have not been blank corrected unless otherwise noted. This test report shall not be reproduced, except in full, without written approval of ALS. ALS provides professional analytical services for all samples submitted. ALS is not in a position to interpret the data and assumes no responsibility for the quality of the samples submitted. All quality control samples processed with the samples in this report yielded acceptable results unless otherwise noted. ALS is accredited for specific fields of testing (scopes) in the following testing sectors. The quality system implemented at ALS conforms to accreditation requirements and is applied to all analytical testing performed by ALS. The following table lists testing sector, accreditation body, accreditation number and website. Please contact these accrediting bodies or your ALS project manager for the current scope of accreditation that applies to your analytical testing. Testing Sector Accreditation Body Certificate Website Number Environmental PJLA (DoD ELAP) Utah (TNI) Nevada Oklahoma Iowa Page 18 of 19 Thu, 05/31/18 3:21 PM ENVREP-V4.8 ANALYTICAL REPORT Workorder: 34-1813735 Client: Utah Department of Health Project Manager: Kevin W. Griffiths Result Symbol Definitions MDL = Method Detection Limit, a statistical estimate of method/media/instrument sensitivity. RL = Reporting Limit, a verified value of method/media/instrument sensitivity. CRDL = Contract Required Detection Limit Reg. Limit = Regulatory Limit. ND = Not Detected, testing result not detected above the MDL or RL. < This testing result is less than the numerical value. "* No result could be reported, see sample comments for details. Qualifier Symbol Definitions U = Qualifier indicates that the analyte was not detected above the MDL. J = Qualifier Indicates that the analyte value is between the MDL and the RL. It is also used to indicate an estimated value for tentatively identified compounds in mass spectrometry where a 1:1 response is assumed. B = Qualifier indicates that the analyte was detected in the blank. E = Qualifier indicates that the analyte result exceeds calibration range. P = Qualifier indicates that the RPD between the two columns is greater than 40%. Page 19 of 19 Thu, 05/31/18 3.21 PM ENVREP-V4.8 AL L.,0 Analysis Information Quality Control Sample Batch Report Workorder: 1813735 Limits: Historical/Performance Preparation: EPA 3510, Sep Funnel SVOA Analysis: SW 8270 Basis: ALS Laboratory Group Batch: ENVX/26778 (HBN: 215063) Batch: ESVO/6416 (HBN: 215718) Prepared By: Christopher Webb Analyzed By: David Teynor ialAnk Wt47F,T.E..27:42fairAttv, 7%7T.R7 MB: 601571 Analyzed: 05/29/2018 15:28 Units: ug/L -Analyte Result MDL RC Pyridine ND 1.5 5.00 Phenol ND 1.5 5.00 Bis(2-chloroethyl)ether ND 1.5 5.00 2-Chlorophenol ND 1.5 5.00 1,3-Dichlorobenzene ND 1.5 5 00 1,4-Dichlorobenzene ND 1.5 5.00 Benzyl alcohol ND 1.5 5.00 1,2-Dichlorobenzene ND 1.5 5.00 2-Methylphenol ND 1.5 5.00 bis(2-Chloroisopropyl)ether ND 1.5 5.00 4-Methylphenol ND 1.5 5.00 N-Nitrosodi-n-propyl amine ND 1.5 5.00 Hexachloroethane ND 1.5 5 00 Nitrobenzene ND 1.5 5.00 lsophorone ND 1.5 5.00 2-Nitrophenol ND 1.5 5.00 2,4-Dimethylphenol ND 1.7 5.00 Benzoic acid ND 15 20.0 Bis(2-Chloroethoxy)methane ND 1.5 5.00 2,4-Dichlorophenol ND 1.5 5.00 1,2,4-Trichlorobenzene ND 1.5 5 00 Naphthalene ND 1.5 5.00 4-Chloroaniline ND 1.5 5.00 Hexachlorobutadiene ND 1.8 5.00 4-Chloro-3-methylphenol ND 1.5 5 00 2-Methylnaphthalene ND 1.5 5.00 Hexachlorocyclopentadiene ND 1.7 5.00 2,4,6-Trichlorophenol ND 1.5 5.00 2,4,5-Trichlorophenol ND 1.5 5.00 2-Chloronaphthalene ND 1 5 5.00 2-Nitroaniline ND 1.5 5.00 Dimethylphthalate ND 1.5 5.00 2,6-Dinitrotoluene ND 1.5 5.00 Acenaphthylene ND 1.5 5.00 3-Nitroaniline ND 1.5 5.00 Acenaphthene ND 1.5 5.00 2,4-Dinitrophenol ND 11 20.0 Page 1 of 11 Thursday, May 31, 2018 QCS V4.4 Quality Control Sample Batch Report lAnalysis rT.T.ormation •*"V Workorder: 1813735 Limits: Historical/Performance Preparation: EPA 3510, Sep Funnel SVOA Analysis: SW 8270 Basis: ALS Laboratory Group Batch: ENVX/26778 (HBN: 215063) Batch: ESVO/6416 (HBN• 215718) Prepared By: Christopher Webb Analyzed By: David Teynor rifank kw2r4t/M-14 Matti& i?.21NAlaipif MB: 601571 Analyzed: 05/29/2018 15:28 Units: ug/L AnaIyte Result IVIDL RI: 4-Nitrophenol ND 7.5 20 0 Dibenzofuran ND 1.5 5 00 2,4-Dinitrotoluene ND 1.5 5 00 Diethylphthalate ND 1.5 5.00 4-Chlorophenyl phenyl ether ND 1.5 5.00 Fluorene ND 1.5 5.00 4-Nitroaniline ND 1.5 5.00 4,6-Dinitro-2-methylphenol ND 7.6 20.0 N-Nitrosodiphenylamine ND 1 5 5.00 4-Bromophenyl phenyl ether ND 1.5 5.00 Hexachlorobenzene ND 1.5 5.00 Pentachlorophenol ND 7 5 20.0 Phenanthrene ND 1.5 5.00 Anthracene ND 1.5 5.00 Carbazole ND 1.5 5 00 Di-n-butylphthalate ND 1.5 5.00 Fluoranthene ND 1.5 5.00 Pyrene ND 1.5 5.00 Butylbenzylphthalate ND 1.5 5.00 3,3'-Dichlorobenzidine ND 1.6 5.00 Benzo(a)anthracene ND 1 5 5.00 Chrysene ND 1.5 5 00 Bis(2-ethylhexyl)phthalate ND 1.5 5.00 Di-n-octylphthalate ND 1.5 5 00 Benzo(b)fluoranthene ND 1.5 5 00 Benzo(k)fluoranthene ND 1.5 5.00 Benzo(a)pyrene ND 1.5 5.00 Indeno(1,2,3-c,d)pyrene ND 1.5 5.00 Dibenzo(a,h)anthracene ND 1.5 5.00 Benzo(g,h,i)perylene ND 1.5 5.00 Lai;otatory Control Sample - LaporatorY ConyorSeiripie b-upi*e P KTAU1 LCS: 601572 Analyzed: 05/29/2018 16:01 Dilution: 1 Units: ug/L LCSD: 601573 Analyzed: 05/29/2018 16:35 Dilution: 1 Units: ug/L ill • Analyte Result Target % Rec QC Limits Result % Rec RPD QC Limits Pyridine 15.9 40.0 39.7 1.9 100.0 14.9 37.2 6 52 0.0 40.0 Page 2 of 11 Thursday, May 31, 2018 QCS V4.4 Quality Control Sample Batch Report lAnalysis information Workorder: 1813735 Limits: Historical/Performance Preparation: EPA 3510, Sep Funnel SVOA Analysis: SW 8270 Basis: ALS Laboratory Group Batch: ENVX/26778 (HBN: 215063) Batch: ESVO/6416 (HBN: 215718) Prepared By: Christopher Webb Analyzed By: David Teynor boratory,„4ntrol Sirrip0 - LaiJor$96, Ddilicate, 7,*0-!•-a.417.1hA LCS: 601572 Analyzed: 05/29/2018 16:01 Dilution: 1 Units: ug/L LCSD: 601573 Analyzed: 05/29/2018 16:35 Dilution: 1 Units: ug/L - Analyte Result Target % Rec QC Limits Result % Rec RPD QC Limits 1 Phenol 11.5 40.0 28.7 8.4 100.0 12 3 30 7 6.70 0.0 20.0 Bis(2-chloroethyl)ether 24.5 40 0 61 3 15 3 109.6 27.0 67.5 9.61 0.0 20.0 2-Chlorophenol 28.8 40.0 72.0 14.5 102.2 30.8 77 0 6.67 0.0 20.0 1,3-Dichlorobenzene 25.6 40.0 64.1 0.0 102.1 25 3 63 2 1.48 0.0 20.0 1,4-Dichlorobenzene 24.2 40.0 60.5 0.0 102.6 24.2 60.6 0.135 0.0 20.0 Benzyl alcohol 26.3 40.0 65.8 22.3 116.5 28 4 71.1 7.76 0 0 40.0 1,2-Dichlorobenzene 25.2 40.0 63.0 2.6 106.4 25.5 63.8 1.31 0.0 20.0 2-Methylphenol 24.1 40.0 60.2 26.8 100.0 26.0 65.0 7.76 0.0 20.0 bis(2-Chloroisopropyl)ether 26.6 40.0 66.5 20.5 113 3 29.0 72.5 8.67 0.0 40.0 N-Nitrosodi-n-propyl amine 25.7 40.0 64.2 30.9 118.2 27.7 69.3 7.65 0.0 20.0 Hexachloroethane 19.9 40.0 49.8 7.5 100 0 18.9 47.2 5.48 0.0 20.0 Nitrobenzene 23.0 40.0 57.4 24.3 101.8 29.5 73.8 * 25.0 0.0 20.0 lsophorone 24.7 40.0 61.8 21.5 117 6 31.9 79.8 * 25.5 0.0 20.0 2-Nitrophenol 23.9 40.0 59.9 30.9 100.0 36.0 90.1 * 40.3 0.0 20.0 2,4-Dimethylphenol 19.5 40.0 48.8 3.0 102.3 22.3 55.8 13.4 0.0 20.0 Benzoic acid 14.1 40.0 35.3 0 0 100.0 15.9 39.7 11.7 0.0 40.0 Bis(2-Chloroethoxy)methane 28.8 40.0 72.1 33.7 100.8 31.7 79.2 9.34 0.0 20.0 2,4-Dichlorophenol 29.1 40.0 72.9 36.7 114.3 37.0 92 6 23.8 0.0 40.0 1,2,4-Trichlorobenzene 25.6 40.0 64.0 10.8 110.4 30.8 77.0 18.5 0.0 20.0 Naphthalene 25.7 40 0 64 4 22.0 112.9 28.7 71.7 10.8 0.0 20.0 4-Chloroaniline 13.2 40.0 32.9 0.0 160.6 13.7 34.4 4.43 0.0 40 0 Hexachlorobutadiene 19.0 40.0 47.6 10.0 100.0 23.6 59.1 21.6 0.0 40.0 4-Chloro-3-methylphenol 30.4 40.0 75.9 36.1 108.4 35.8 89.6 16.4 0.0 20.0 2-Methylnaphthalene 25.5 40.0 63.7 25.5 118.8 32 7 81.7 * 24.9 0.0 20.0 Hexachlorocyclopentadiene 20.3 40.0 50.8 7.0 100.0 18.0 45.1 12.0 0 0 40 0 2,4,6-Trichlorophenol 36.6 40.0 91.4 33.8 121.1 34.4 85.9 6.19 0.0 20.0 2,4,5-Trichlorophenol 35.7 40.0 89.2 37.4 118 9 33.6 84.0 5.99 0.0 20.0 2-Chloronaphthalene 31.6 40.0 79.0 31.2 114.4 29.2 73.1 7.84 0 0 20.0 2-Nitroaniline 28.8 40.0 72.0 37.0 120 1 25.9 64.7 10.6 0.0 40.0 Dimethylphthalate 34 9 40 0 87.2 46.8 116.9 32.1 80.2 8.35 0.0 30.0 2,6-Dinitrotoluene 36 1 40.0 90.3 49.5 118.5 31.8 79.4 12.8 0.0 20.0 Acenaphthylene 31.0 40.0 77.6 41.2 111.0 30.0 75.1 3.32 0.0 20 0 3-Nitroaniline 19.8 40.0 49.4 29.1 143.9 11.2 * 28.1 * 55.0 0.0 40.0 Acenaphthene 29.1 40.0 72.7 41.0 113.9 32.7 81.7 11.6 0.0 20.0 2,4-Dinitrophenol 49.0 40.0 122 0.0 127.2 52.7 * 132 7.32 0.0 20.0 4-Nitrophenol 12.7 40.0 31.6 0.0 100.0 8.75 21.9 36.5 0.0 40.0 Dibenzofuran 33.6 40.0 84.1 41.6 117.6 32.7 81 7 2 80 0.0 20 0 Page 3 of 11 Thursday, May 31, 2018 QCS V4.4 Quality Control Sample Batch Report !Analysis InformaVon Workorder: 1813735 Limits: Historical/Performance Preparation: EPA 3510, Sep Funnel SVOA Analysis: SW 8270 Basis: ALS Laboratory Group Batch: ENVX/26778 (HBN: 215063) Batch: ESVO/6416 (HBN: 215718) Prepared By: Christopher Webb Analyzed By: David Teynor Laboratory Cony?) Sample - Laboratory Control Sample Dnplicate LCS: 601572 Analyzed: 05/29/2018 16:01 Dilution: 1 Units: ug/L LCSD: 601573 Analyzed: 05/29/2018 16:35 Dilution: 1 Units: ug/L "Analyto Result Target % Rec QC Limits Result % Rec RPD QC Limits 2,4-Dinitrotoluene 36.9 40.0 92.2 48 9 124.7 31.0 77.6 17.2 0.0 20.0 Diethylphthalate 33.4 40.0 83.5 49.5 118.5 33.1 82.6 1.08 0.0 30.0 4-Chlorophenyl phenyl ether 38.0 40.0 95.1 44.2 118.9 36.3 90.6 4.80 0.0 20.0 Fluorene 31 7 40.0 79.2 46.5 118.6 33.1 82.8 4.45 0.0 20.0 4-Nitroaniline 21.0 40.0 52.4 4.9 164.0 20 0 50.1 4.56 0.0 40.0 4,6-Dinitro-2-methylphenol 41 5 40.0 104 24.2 128 7 36.4 91.0 13.2 0.0 40.0 4-Bromophenyl phenyl ether 38.5 40 0 96.3 42.9 119.9 36 5 91.1 5.54 0.0 20.0 Hexachlorobenzene 37.7 40 0 94.3 42.4 122.4 35 2 87.9 6.98 0.0 20.0 Pentachlorophenol 39.1 40.0 97.8 29 0 135.3 31.2 77.9 * 22.7 0.0 20.0 Phenanthrene 30.7 40.0 76 8 45 7 119.7 32.7 81.8 6.21 0.0 20.0 Anthracene 32.3 40.0 80.9 45 7 120.6 37.5 93 6 14.6 0.0 20.0 Carbazole 44.1 40 0 110 11.7 156.9 35.2 88.0 22.3 0.0 40.0 Di-n-butylphthalate 30 3 40.0 75.9 47.0 127 8 28.9 72.2 4.94 0.0 30.0 Fluoranthene 34.3 40.0 85.8 40.6 133.2 32.8 82 0 4.54 0.0 20.0 Pyrene 34 6 40.0 86.4 47.5 121.4 37.1 92.7 7.03 0.0 20.0 Butylbenzylphthalate 29.1 40.0 72.7 48.6 120 8 31.1 77.8 6.78 0.0 30.0 3,3'-Dichlorobenzidine 28.5 40 0 71.3 7.2 155.3 30 8 77.1 7.75 0.0 40.0 Benzo(a)anthracene 32.8 40.0 81 9 49.8 117.3 35 3 88.3 7.51 0.0 20.0 Chrysene 33.0 40.0 82.5 50.1 123 6 35.2 87.9 6 38 0 0 20.0 Bis(2-ethylhexyl)phthalate 28.9 40.0 72.2 50.6 125.2 31.0 77.6 7.23 0.0 30.0 Di-n-octylphthalate 31.8 40.0 79.5 47.6 121.1 30.6 76.6 3.64 0.0 30.0 Benzo(b)fluoranthene 36.7 40.0 91 6 49.0 113.1 35.5 88.8 3.19 0.0 20.0 Benzo(k)fluoranthene 34.4 40.0 86.0 51.7 117.4 34.0 85.1 1.06 0.0 20.0 Benzo(a)pyrene 28.3 40.0 70.7 49.0 114.4 32.8 82.1 14 9 0.0 20.0 Indeno(1,2,3-c,d)pyrene 39.2 40.0 98.0 40.3 124.4 37.9 94 8 3.31 0.0 20.0 Dibenzo(a,h)anthracene 37 2 40.0 93.0 44.5 124 3 36.1 90.3 2.91 0.0 20.0 Benzo(g,h,i)perylene 39 6 40.0 98.9 42.1 124.5 38.2 95 5 3.56 0.0 20.0 ,Aurrogate kicpyoe s , CA(%.1.!,'44.# .'. • 7 Surrogate 2-Fluorophenol Phenol-d5 Nitrobenzene-d5 QC Limits 0.0 121.0 0.0 145.0 22.0 130.3 Units ug/L ug/L ug/L Lab ID Result Target % Recovery Result Target % Recovery Result Target % Recovery 601571-MB 22.0 50.0 43.9 14.1 50.0 28.2 32.6 50.0 65.3 601572-LCS 22.3 50.0 44.6 14.5 50.0 28.9 26.8 50.0 53.7 601573-LCSD 24 7 50.0 49.3 14.9 50.0 29 7 33.6 50.0 67 1 1813795001 5.16 50.0 10 3 5.07 50.0 10.1 5.91 50.0 * 11 8 Page 4 of 11 Thursday, May 31, 2018 QCS V4.4 Quality Control Sample Batch Report fAnalysis Information Workorder: 1813735 Limits: Historical/Performance Preparation: EPA 3510, Sep Funnel SVOA Analysis: SW 8270 Basis: ALS Laboratory Group Batch: ENVX/26778 (HBN: 215063) Batch: ESVO/6416 (HBN: 215718) Prepared By: Christopher Webb Analyzed By: David Teynor '$uriogate kecoerfes lt. ..., ,C•it A- . , ,,,,_,774iiiWili7114-71,' 3 ' 74 t -?-04.:47 Surrogate 2-Fluorophenol Phenol-d5 Nitrobenzene-d5 QC Limits 0.0 121.0 0.0 145.0 22.0 130.3 Units ug/L ug/L ug/L Lab ID Result Target % Recovery Result Target % Recovery Result Target % Recovery 1813735004 18.3 50.0 36.7 12.9 50.0 25.8 27.9 50.0 55.9 1813735005 17.8 50.0 35.6 11.6 50.0 23.1 30.7 50.0 61.3 1813735006 21.0 50.0 42.0 15.1 50.0 30.2 31 5 50.0 63.0 Surrogate 2-Fluorobiphenyl 2,4,6-Tribromophenol Terphenyl-d14 QC Limits 35.1 113.6 12.1 139.9 16.2 143.5 Units ug/L ug/L ug/L Lab ID Result Target % Recovery Result Target % Recovery Result Target % Recovery 601571-MB 39.1 50.0 78.2 45.0 50.0 90.1 45.4 50.0 90.9 601572-LCS 40.6 50.0 81.2 56.9 50.0 114 46.3 50.0 92.7 601573-LCSD 36.2 50.0 72.4 48.4 50.0 96.9 47.5 50.0 95.1 1813795001 8.88 50.0 * 17.8 5.24 50.0 * 10.5 11.5 50.0 23.0 1813735004 37.0 50.0 73.9 63 2 50.0 126 43.3 50.0 86.6 1813735005 35.2 50.0 70.4 59 0 50.0 118 36.5 50.0 73.0 1813735006 29.9 50.0 59.7 49.8 50 0 99.5 40 6 50.0 81.3 rairiiinents ,eA.1044rniZegArzsmtklEccia,vatkvAaogiolgv.-tua ,.7.9otUrvc.,71.4;IRVEffait,..twvi.Ar‘ MAIIM The initial calibration did not pass method criteria for 3-nitroaniline, 4-nitroaniline, and carbazole. The CCV did not pass method criteria for 2,4-dimethylphenol, 4-chloroaniline, 3-nitroaniline, 2,4-dinitrophenol, and 4-nitroaniline. Any results for these compounds should be treated as semi-quantitative. The LCSD was outside of percent recovery QC limits for 3-nitroaniline and 2,4-dinitrophenol RPD was outside of QC limits for 6 compounds. haq itepoit AuTilorization (1st an, electronic signature that cornPris *Etil 21 CR Part lit Analyst Peer Review /S/ David Teynor /S/ Thomas J. Masoian 05/31/2018 11:37 05/31/2018 14:57 *- Analyte above reporting limit or outside of control limits A- Sample result is greater than 4 times the spike added *- Sample and Matrix Duplicate less than 5 times the reporting limit Result is above the calibration range # - The Matrix Spike, Matrix Spike duplicate or Matrix Duplicate is reported for your information only. The sample matrix may be inappropriate for the method selected. RPD - Relative % Difference (Spike / Spike Duplicate) ND - Not Detected (U - Qualifier also flags analyte as not detected) NA - Not Applicable QC results are not adjusted for moisture correction, where applicable Page 5 of 11 Thursday, May 31, 2018 QCS V4.4 s alysis Information Quality Control Sample Batch Report Workorder: 1813735 Limits: Historical/Performance Preparation: NA Analysis: SW 8260 Basis: ALS Laboratory Group Batch: NA Batch: EVO/7139 (HBN: 214983) Prepared By: NA Analyzed By: Christopher Q. Coleman [Blank MB: 601389 Analyzed: 05/17/2018 10:11 Units: ug/L Analyte Result MDL 1 RL Dichlorodifluoromethane ND 0 3 1.00 Chloromethane ND 0.3 1.00 Vinyl chloride ND 0.3 1.00 Bromomethane ND 0.3 1.00 Chloroethane ND 0.3 1.00 Dichlorofluoromethane ND 0 3 1.00 Trichlorofluoromethane ND 0.3 1.00 Ethyl ether ND 0.3 1.00 1,1-Dichloroethene ND 0 3 1 00 Freon 113 ND 0 3 1.00 Acetone ND 1.5 5.00 lodomethane ND 0.3 1.00 Carbon disulfide ND 0.3 1.00 Methyl Acetate ND 1.5 5.00 Ally! chloride ND 0.3 1.00 Methylene chloride ND 0.3 1.00 trans-1,2-Dichloroethene ND 0.3 1.00 Methyl-t-butyl ether ND 0.3 1.00 cis-1,2-Dichloroethene ND 0.3 1.00 1,1-Dichloroethane ND 0.3 1.00 2,2-Dichloropropane ND 0.3 1.00 2-Butanone ND 1.6 5.00 Ethyl acetate ND 1.5 5.00 Bromochloromethane ND 0.3 1.00 Tetrahydrofuran ND 2.1 5.00 Chloroform ND 0 3 1.00 1,1,1-Trichloroethane ND 0 3 1.00 Cyclohexane ND 0.3 1.00 1,1-Dichloropropene ND 0.3 1.00 1,2-Dichloroethane ND 0.3 1 00 Carbon tetrachloride ND 0.3 1 00 Benzene ND 0.3 1 00 Trichloroethene ND 0 3 1 00 Methylcyclohexane ND 0.3 1.00 1,2-Dichloropropane ND 0.3 1.00 Dibromomethane ND 0.3 1.00 Bromodichloromethane ND 0.3 1.00 Page 6 of 11 Thursday, May 31, 2018 QCS V4.4 S Ist naysis Information Quality Control Sample Batch Report Workorder: 1813735 Limits: Historical/Performance Preparation: NA Analysis: SW 8260 Basis: ALS Laboratory Group Batch: NA Batch: EVO/7139 (HBN. 214983) Prepared By: NA Analyzed By: Christopher Q Coleman 'OrPriM*, MB: 601389 Analyzed: 05/17/2018 10:11 Units: ug/L ., Analyte Result MDL RL cis-1,3-Dichloropropene ND 0.3 1.00 4-Methy1-2-pentanone ND 1.5 5.00 trans-1,3-Dichloropropene ND 0.3 1.00 Ethyl methacrylate ND 0.3 1.00 1,1,2-Trichloroethane ND 0.3 1.00 2-Hexanone ND 1.5 5.00 1,2-Dibromoethane ND 0 3 1.00 Toluene ND 0.3 1.00 1,3-Dichloropropane ND 0.3 1.00 Dibromochloromethane ND 0.3 1.00 Bromoform ND 0.3 1.00 Tetrachloroethene ND 0 3 1.00 1-Chlorohexane ND 0.3 1.00 Chlorobenzene ND 0.3 1.00 1,1,1,2-Tetrachloroethane ND 0.3 1.00 Ethylbenzene ND 0.3 1.00 m,p-Xylene ND 0.3 2.00 o-Xylene ND 0.3 1 00 Styrene ND 0.3 1 00 lsopropylbenzene ND 0.3 1 00 1,1,2,2-Tetrachloroethane ND 0.3 1.00 Bromobenzene ND 0.3 1.00 1,2,3-Trichloropropane ND 0.3 1.00 trans-1,4-Dichloro-2-butene ND 1.5 5.00 Pentachloroethane ND 0.3 1.00 n-Propylbenzene ND 0.3 1.00 1,3,5-Trimethylbenzene ND 0.3 1.00 2-Chlorotoluene ND 0 3 1.00 4-Chlorotoluene ND 0.3 1.00 tert-Butylbenzene ND 0.3 1.00 1,2,4-Trimethylbenzene ND 0.3 1.00 sec-Butylbenzene ND 0.3 1.00 p-lsopropyltoluene ND 0.3 1.00 1,3-Dichlorobenzene ND 0.3 1.00 1,4-Dichlorobenzene ND 0 3 1.00 n-Butylbenzene ND 0.3 1.00 1,2-Dichlorobenzene ND 0 3 1.00 Page 7 of 11 Thursday, May 31, 2018 QCS V4.4 nelfsis Infoi-mation Quality Control Sample Batch Report Workorder: 1813735 Limits: Historical/Performance Preparation: NA Analysis: SW 8260 Basis: ALS Laboratory Group Batch: NA Batch: EVO/7139 (HBN: 214983) Prepared By: NA Analyzed By: Christopher Q. Coleman .1,44$340r.M- 'Blank MB: 601389 Analyzed: 05/17/2018 10:11 Units: ug/L lAnalyte Result MDL Ri.! 1,2-Dibromo-3-Chloropropane ND 1.5 5.00 1,2,4-Trichlorobenzene ND 0.3 1.00 Hexachlorobutadiene ND 0.3 1.00 Naphthalene ND 0.36 1.00 1,2,3-Trichlorobenzene ND 0.3 1.00 stilabc4ratory Contrp) Sam,* LCS: 601390 Analyzed: 05/17/2018 09:22 Dilution: 1 Units: ug/L 7Analyte Result Target % Rec QC Limits Dichlorodifluoromethane 47.0 50.0 94.0 48.9 155 3 Chloromethane 47.7 50.0 95.4 66.8 135.9 Vinyl chloride 49.2 50 0 98.4 66.4 115.8 Bromomethane 52.0 50.0 104 56.3 146.8 Chloroethane 49.8 50 0 99.6 77.3 129.5 Dichlorofluoromethane 52.1 50 0 104 77.5 131.2 Trichlorofluoromethane 47.9 50 0 95.8 76.1 131.0 Ethyl ether 54.1 50.0 108 79.8 129 3 1,1-Dichloroethene 48.3 50.0 96.6 77.6 136 5 Freon 113 53.6 50.0 107 65.8 129.3 Acetone 60.1 50 0 120 41.9 164.4 lodomethane 48 8 50.0 97.6 50.1 154 9 Carbon disulfide 50.3 50.0 101 72.3 127 8 Methyl Acetate 51 2 50.0 102 42 7 147.1 Allyl chloride 51 7 50.0 103 74 5 134.7 Methylene chloride 49.0 50.0 98.0 75 9 127.6 trans-1,2-Dichloroethene 49.4 50.0 98 8 73 5 130.0 Methyl-t-butyl ether 50.7 50.0 101 79.6 127 4 cis-1,2-Dichloroethene 49.2 50.0 98.4 73.5 126 3 1,1-Dichloroethane 49.1 50.0 98.3 73.2 120.9 2,2-Dichloropropane 50 4 50.0 101 66.5 143.6 2-Butanone 59.9 50 0 120 51.1 147.7 Ethyl acetate 59.9 50.0 120 38.8 216.2 Bromochloromethane 47.9 50.0 95 9 73.7 123.9 Tetra hyd rofu ran 47.6 50 0 95.2 69.2 140.7 Chloroform 48.9 50.0 97.9 75 4 124 1 Page 8 of 11 Thursday, May 31, 2018 QCS V4.4 Quality Control Sample Batch Report Wnalysis informalion Workorder: 1813735 Limits: Historical/Performance Preparation: NA Analysis: SW 8260 Basis: ALS Laboratory Group Batch: NA Batch: EVO/7139 (HBN: 214983) Prepared By: NA Analyzed By: Christopher Q. Coleman •EW-,4` LaltOriterpj Snple wimAtitrazz LCS: 601390 Analyzed: 05/17/2018 09:22 Dilution: 1 Units: ug/L l Analyte Result Target % Rec 1 QC Limits 1,1,1-Trichloroethane 48.3 50.0 96.7 75.9 129.4 Cyclohexane 53.7 50.0 107 78.0 134.0 1,1-Dichloropropene 50.3 50.0 101 75.9 123.9 1,2-Dichloroethane 49.9 50.0 99.8 76.9 126.7 Carbon tetrachloride 47.7 50.0 95.4 73.5 136.2 Benzene 49.6 50.0 99.3 79.4 124.0 Trichloroethene 48.1 50.0 96 3 74.5 126.7 Methylcyclohexane 50.6 50.0 101 76.8 127 7 1,2-Dichloropropane 51.1 50.0 102 80.7 122.3 Dibromomethane 48.7 50.0 97.3 75.1 120.5 Bromodichloromethane 49.6 50.0 99.2 77.8 125.4 cis-1,3-Dichloropropene 51.4 50.0 103 80.0 129.2 4-Methy1-2-pentanone 56.8 50 0 114 70.9 133.5 trans-1,3-Dichloropropene 47.7 50.0 95.5 83.0 129.6 Ethyl methacrylate 51.5 50.0 103 77.9 135.8 1,1,2-Trichloroethane 46.9 50 0 93.8 83.3 116.9 2-Hexanone 56.6 50.0 113 56.9 143.8 1,2-Dibromoethane 46.4 50.0 92.8 82.8 120.7 Toluene 46.3 50.0 92.5 86 1 117.8 1,3-Dichloropropane 47 0 50.0 94.0 82.9 119.3 Dibromochloromethane 47.2 50.0 94.4 75.5 136.4 Bromoform 44.3 50.0 88.5 63.1 139 2 Tetrachloroethene 42.4 50.0 84.8 63.2 122.5 1-Chlorohexane 48.8 50.0 97 6 87.4 125 2 Chlorobenzene 45.9 50.0 91.8 86.5 113 3 1,1,1,2-Tetrachloroethane 46.4 50.0 92.8 81.3 130.8 Ethylbenzene 46.9 50.0 93.9 88 4 117.0 m,p-Xylene 94 6 100 94.6 88.4 116.9 o-Xylene 47.4 50.0 94.8 86.5 116 1 Styrene 48.7 50.0 97.5 89 1 121.1 lsopropylbenzene 47.3 50.0 94.6 86.8 118.9 1,1,2,2-Tetrachloroethane 48.9 50.0 97.7 77.8 128.9 Bromobenzene 45.2 50.0 90.3 81.3 119.8 1,2,3-Trichloropropane 47.8 50.0 95.7 76.5 127.9 trans-1,4-Dichloro-2-butene 49.9 50.0 99 9 58.2 139 4 Pentachloroethane 47.1 50.0 94.3 38.6 196.6 n-Propylbenzene 48.1 50.0 96.2 81.3 125.5 Page 9 of 11 Thursday, May 31, 2018 QCS V4.4 Quality Control Sample Batch Report tAnaysis informatio Workorder: 1813735 Limits: Historical/Performance Preparation: NA Analysis: SW 8260 Basis: ALS Laboratory Group Batch: NA Batch: EVO/7139 (HBN: 214983) Prepared By: NA Analyzed By: Christopher Q. Coleman Liboratsry Contrcil 6ample LCS: 601390 Analyzed: 05/17/2018 09:22 Dilution: 1 Units: ug/L Analyte Result Target % Rec QC Limits I 1 ,3,5-Trim ethylbenzene 47.3 50.0 94.7 82 9 127.1 2-Chlorotoluene 46.9 50.0 93.8 82.8 121.6 4-Chlorotoluene 45.2 50.0 90.3 83.1 120.9 tert-Butylbenzene 46.6 50.0 93.3 80.5 130.5 1 ,2,4-Trim ethylbenzene 47.9 50.0 95.7 81.7 125.6 sec-Butylbenzene 50.6 50.0 101 84.4 128.9 p-lsopropyltoluene 48 2 50.0 96.4 83.0 126.1 1,3-Dichlorobenzene 45 4 50.0 90.8 82.6 118.3 1,4-Dichlorobenzene 44.9 50.0 89.9 82.0 117.8 n-Butylbenzene 48.8 50.0 97 6 83.8 131.4 1,2-Dichlorobenzene 45 3 50.0 90.6 81.4 119.9 1,2-Dibromo-3-Chloropropane 50.4 50.0 101 56.2 157 5 1,2,4-Trichlorobenzene 43.9 50.0 87.7 70.2 140.4 Hexachlorobutadiene 45.9 50.0 91.8 79.7 129.9 Naphthalene 43.4 50.0 86.7 62.8 150.8 1,2,3-Trichlorobenzene 40.8 50.0 81.7 71.8 138.2 -Matrix Spike - filabix SIce Duplicate ic '4?Ettiir. 4 s'inefIQV ) Sample: 1813516001 Analyzed: 05/17/2018 12:39 Dilution: 1 Units: ug/L MS: 601392 Arialyzed: 05/17/2018 14:50 Dilution: 1 Units: ug/L MSD: 601393 Analyzed: 05/17/2018 15:06 Dilution: 1 Units: ug/L Analyte Result Result Target % Rec QC Limits Result % Rec RPD QC Limits-4 Benzene ND 55.8 50 112 79.4 124.0 51 102 9.01 0.0 20.0 Toluene ND 51.3 50 103 86 1 117.8 46.7 93.4 9.36 0.0 20.0 Ethylbenzene ND 51.4 50 103 88.4 117 0 46 7 93.5 9.5 0.0 20.0 m,p-Xylene ND 103 100 103 88.4 116 9 94 1 94.1 9.22 0.0 20.0 o-Xylene ND 51 4 50 103 86.5 116.1 47.2 94.4 8 61 0.0 20.0 u rrb:g ate AecoyArises ' fii2! . 7.7:77-....., EA,,,ir• Surrogate 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene QC Limits 72.2 123.4 77.5 116.4 78.5 121.6 Units ug/L ug/L ug/L Lab ID Result Target % Recovery Result Target % Recovery Result Target % Recovery 601390-LCS 51.7 50.0 103 48.8 50.0 97.6 51.4 50.0 103 601389-MB 48.3 50.0 96 7 51.5 50.0 103 53.1 50.0 106 1813642004-TRIPB 50.9 50.0 102 50.6 50.0 101 52.7 50.0 105 1813516001 48.8 50.0 97.7 51 0 50.0 102 53.1 50.0 106 Page 10 of 11 Thursday, May 31, 2018 QCS V4.4 Quality Control Sample Batch Report ;Analysis Information Workorder: 1813735 Limits: Historical/Performance Preparation: NA Analysis: SW 8260 Basis: ALS Laboratory Group Batch: NA Batch: EVO/7139 (HBN: 214983) Prepared By: NA Analyzed By: Christopher Q. Coleman l'§u-le-QtMe ReRTIATA9 s '"1"11-a/4164rag.WriginetvitglaPANP4Ott 15'" 't.i.k, S. r3. ,1 Surrogate 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene QC Limits 72.2 123.4 77.5 116.4 78.5 121.6 Units ug/L ug/L ug/L Lab 10 Result Target % Recovery Result Target % Recovery Result Target % Recovery 1813642001 50.0 50.0 99.9 51 0 50.0 102 52.3 50.0 105 1813642002 49.2 50 0 98.4 50.7 50.0 101 52.5 50.0 105 1813642003 49.2 50.0 98.3 50.9 50.0 102 52.6 50.0 105 1813735001 51.8 50.0 104 50.1 50.0 100 53.1 50.0 106 1813735003 51.0 50.0 102 50.5 50.0 101 53.3 50.0 107 1813735002 51.7 50.0 103 50.5 50.0 101 51.8 50.0 104 601392-MS 51.2 50.0 102 48.6 50.0 97.2 51.9 50.0 104 601393-MSD 51.4 50.0 103 48.5 50.0 97.0 51.9 50.0 104 Kinerits vszav& 8260 QC Comments: The percent difference (or percent drift for a regression fit) for target compounds in the CVS standard must generally be less than 20% relative to the average response from the initial calibration curve The analyte acetone did not meet this criteria and results for this compound should be considered estimates. avikePorlAciigation 0/ is an ele,ctiTc,nic sjoature ttiat gomplies OM 21 CFR Part ti Analyst Peer Review /S/ Christopher Q. Coleman /S/ Thomas J. Masoian 05/18/2018 11.21 05/22/2018 08:32 ASTIN fti(mbols An0fil3ktioos * - Analyte above reporting limit or outside of control limits A- Sample result is greater than 4 times the spike added (D- Sample and Matrix Duplicate less than 5 times the reporting limit - Result is above the calibration range # - The Matrix Spike, Matrix Spike duplicate or Matrix Duplicate is reported for your information only. The sample matrix may be inappropriate for the method selected. RPD - Relative % Difference (Spike / Spike Duplicate) ND - Not Detected (U - Qualifier also flags analyte as not detected) NA - Not Applicable QC results are not adjusted for moisture correction, where applicable Page 11 of 11 Thursday, May 31, 2018 QCS V4.4