DSHW-2018-005075 - 0901a0688083be83

-.441
UTAH DEPARTMENT OF HEALTH
Final
Results
Diu or W~,=,
and
0 LI
-V-A-I-W-200-05)75
Report To:
Deborah Ng
Division of Waste Management & Radiation Control (
DWMRC)
PO BOX 144880
Salt Lake City, UT 84114
Bill To:
Division of Waste Management & Radiation Control
195 North 1950 West
Salt Lake City, UT 84114
Project ID: C2018-02008
Deborah Ng,
Your sample(s) submitted to Utah Public Health Laboratory (UPHL) on Wednesday, May 16, 2018 were
assigned the UPHL Project ID C2018-02008. Enclosed are the analytical results pertaining to that Project ID.
Herein are the results relating only to the sample(s) received and tested for the project C2018-02008. All
associated analyses were performed following the UPHL Quality Assurance Plan. This report and its contents
have been reviewed and approved by the appropriate Laboratory Staff and Supervisor(s). This report shall not
be reproduced, except in full, without the written permission of UPHL.
If you have any questions regarding your results, please contact UPHL at [phone] and reference the
Project ID C2018-02008.
Reviewed by: Kyle Ashby
Reviewed on: 6/1/2018
ADDRESS: 4431 South 2700 West, Taylorsville, UT 84129 PHONE. [phone] FAX: [phone]
Itah Pt ihlirt 1-laalth I Ahnratnry - r.hpmictry
Z_UT_ProjectChemistryAnalyticalspt Page 1 of 4 Fri, Jun 1, 2018 10:35 am
Project
Summary
Report To:
Deborah Ng (DWMRC_00)
Division of Waste Management & Radiation Control (
DWMRC)
PO BOX 144880
Salt Lake City, UT 84114
Phone: [phone]
Fax: [phone]
E-mail: [e-mail]
Bill To:
Division of Waste Management & Radiation Control
195 North 1950 West
Salt Lake City, UT 84114
Phone: [phone]
Fax: [phone]
Project ID: C2018-02008
Project Notes:
This project contains samples that were analyzed at a different laboratory. Please see the attached report for more information
from that laboatory regarding your sample.
Sample # Date Collected Date Received Facility Sampling Point Site Description
2125762 05/15/18 05/16/18 N/A N/A MW-24
2125768 05/15/18 05/16/18 N/A N/A MW-24
Z_UT_ProjectChemistryAnalytical rpt Page 2 of 4 Fri, Jun 1, 2018 10:35 am
744 IT
UTAH DEPARTMENT OF HEALTH
Analytical
Report
Project ID: C2018-02008
SRL MRL Result Dil Fac Analyte Qualifier MDL
Analysis Method - Pass Through EPA 8270 SVOCS
Sample Notes:
1 CONTAINER HAS HEADSPACE, SAMPLER MENTIONED THERE WERE AIR
BUBBLES AT COLLECTION SITE.
Analysis Method - Pass Through EPA 8260 VOCs
Z_UT_ProjectChemistryAnalytical.rpt Page 3 of 4 Fri, Jun 1, 2018 10.35 am
Analyte Result Dil Fac Qualifier MDL MRL SRL
Pass Through Laboratory ALS Environmental Laboratory
Facility: N/A
Sampling Point: N/A
Site Description: MW-24
Date Collected
Collected By:
COC Initiated:
Condition of Seal:
5/15/2018 4:30:00PM
ZHU, HAO
Yes
Not Present
Sample ID: 2125768
Text ID: PV018-0002
Matrix: Water
Bottle Type:
SDWIS Type: Private Investigative
Date Collected 5/15/2018 4:30:00PM
Collected By: ZHU, HAO
COC Initiated: Yes
Condition of Seal: Not Present
Facility: N/A
Sampling Point: N/A
Site Description: MW-24
Sample ID: 2125762
Text ID: PSV18-0002
Matrix: Water
Bottle Type:
SDWIS Type: Private Investigative
Pass Through Laboratory ALS Environmental Laboratory
zit!, Report Project ID: C2018-02008
116- Notes UTAH DEPARTMENT OF HEALTH
Report Comments
This report contains only the results for analyses requested and tested.
Unless otherwise noted:
- Samples were received in acceptable condition.
- Samples have not been blank corrected.
- All Quality Control Samples processed yielded acceptable results.
Report Symbol Definitions
MDL - Method Detection Limit, a statistically estimated concentration for instrument/method/matrix
sensitivity.
MRL - Method Reporting Limit, the minimum concentration that can be reported as a quantitated value.
SRL - Sample Reporting Limit, the minimum concentration that can be reported as a quantitated value
taking into account limitations inherent in the sample matrix.
ND - Not Detected, tested result was not detected above MDL or MRL.
< - Less than, tested result is less than the numerical value.
Please take our customer satisfaction survey at https://www.surveymonkey.com/r/environmentalchemistry
Z_UT_ProjectChemistryAnalytical.rpt Page 4 of 4 Fri, Jun 1, 2018 10:35 am
Project Name
Pennzoil Refinery
1
.7
Cost Code
>14 t't A- C- call Sheila
Phone No.
801-536-0249 Person to Address Report / Questions To:
Zhu, Hao
email:[e-mail] [e-mail]
Phone No.
[phone]
Zip:
84114
Matrix Time (Mil)
ST:
UT
City:
Salt Lake City
Mailing Address:
UDEQ/WMRC, 195 North 1950 West, 2nd Floor, SLC, UT 84114-4880
05-15-18
water
kola%
a
Use this space for comments:
1- 8 2.(e tip_S 64-eiSe Sars4•10 key- marl:C-1 .sv•.".0.1 etecv
Section
CAS
Sampler Name & Initials (PRINT):
Zhu, Hao
Field ID or Location
M
ontrlik
Date Sampled
ops
3 '01AAN
r3001
water 21,3e
t-Lts
# of Containers
IA*
12
El
82
6
0
:

V
OCs

C
LAB Sample
Number
LAB USE ONLY MAY 16 '16 14:58
Tamper
Seal Intact
(Y or N)
Comments (Temp.,Leaks, etc.)
a
1-3
•IfeNt.
cJ
a
a a
a
EJ
a
a
11 111011111111filli 2125761 - PSV18 -00018 . -
1111111111011111111111112125762 PSV18-000213
2125763 —1-1 PS1/111 -0003C
" 11111111111111111111 2125766 — PV018 -0001D
2125768 11 pvn1R-110112D
2125769 PV018-0003D
LJ
a
a
cf--- es 1te .
Relinquished By:
- Print Name »: l-la T'io cur
Date _c---A6/)<YS
Time
/cf = 4C,
Received By: Invoice / Airbill #
Print Name »: Date Time
elinquished By:
Print Name »:
Date Time Received By: Invoice / Airbill #
Print Name ».
C4-1 Date
ri • 05-Ve-ee me /YY(ta Invoice /Arbil # 'Relinquished By:
Print Name »:
Date Time Received By LAB: - - Print Name »: Date Time
LEGAL CHAIN OF CUSTODY RECORD VI-53(9".°2481'
State of Utah
Unified State Laboratories:
Public Health Bureau of
Chemical and Environmental
Services
Telephone: [phone]
FAX: [phone]
cJ
a
Relinquish d
Relinq ish&51 By:
Relinquished By:
•
Unified State Laboratories: Public Health
Bureau of Chemical and Environmental Services
4431 S 2700 W Taylorsville, UT 84129
801-965-2400 Fax [phone]
httos://health.utah.gov/lab/chem lab
Glip5 t`'4 CHAIN OF CUSTODY
S01136
CI Hand Delivered
0 Shipped Samples
Cooler Returned
System/Agency Name: System/Agency Number: Cost/Project Code: Received Date and Time:
REQUESTED TESTS
city, state, zip: Taylorsville, Utah, 84129
Submitted By: K.D. Ashby
Address: 4431 S 2700 W
REPORTING/CONTACT BILLING (list if different)
Attn: Kyle Ashby Special Code:
Attn: Tiffany Shields
Address: 4431 S 2700 W
Phone: [phone] city, state, zip. Taylorsville, Utah 8412
Fax: [phone] Phone: [phone]
Email: kdashbvOutah.gov
COLLECTION POINT DESCRIPTION
MW-11
MW-24
MW-109
MW-11
MW-24
MW-109
Collectors initials
Fax:
Email: tshieldsOutah.Clov
05/15/18
05/15/18
05/15/18
05/15/18
05/15/18
05/15/18
‘.onection Date
(mm/ddivvl
Collection
Time (24 hr)
15:15
16:30
17:30
15:15
16:30
17:30
9
COMMENTS
X X

EP
A

82
60
:

VO
C
s

EP
A

8
2
70
:

S
V
O
Cs

Date and Time: .054 r
Date and Time:
Date and Time:
R d bV
wed by:
Received by:
Re
c
e
ip
t t
e
m
p
er
a
tu
re

po
o
l:
3
0
0
E1
0

i`
Sample Receipt Conditions
No
El Documentation complete
O Proper containers and in-date
O Containers intact
O Within holding time
O Coolant
O Temperature within-range
O Acceptable pH 0 N/A
El Custody Seals Intact
LAB NUMBER
2125766
2125768
2125769
2125761
2125762
2125763

c
o
: c_zi
Date and Time:
Date and Time:
CLIENT-RELATED INFORMATION
No 0 Client Notified? YES
Date: ALS Project Manager Returned to Sample Receipt by.
PnntedName sigma=
Response Required Within 24 Hours
0 Missing Cooler
El Cooler Conditions 0 Missing Paperwork 0 Missing/Incorrect Bottle
Labels
Missing Samples/Bottles 0 Broken/Leaking Samples
0 Incorrect Bottle Type
Cooler Temperatures Out of Range
0 Incorrect Preservation 0 pH Criteria Not Met
0 Residual Chlorine Present
0 Head Space in Bottles
0 Insufficient Sample
Volume
O Chain of Custody
Problems 0 Other
BRIEFLY DESCRIBE THE PROBLEM AND THE ACTION TAKEN:
a; Katylp Otd, titefej
PROJECT MANAGEMENT
PROJECT MANAGER COMMENTS:
ALS-SALT LAKE CITY-RELATED INFORMATION REPORT CRIR
COOLER OR CONTArR INFORMATION CHECKLIST (Fill In or Circle)
Client Name: vi.)\-- , Project/Task/Site: i ii035.
Date/Time of Receipt: M 1-7tfr1q ((019'i Number of Coolers Received: 1
Condition of Coolers: (AC efUnacceptable Temperature Control: Present/Ne'c,
Cooler Custody Seals: Present/
1ntact/Bront Location Temp Taken: Control/B een S • les
Container Custody Seals: Present/ ...
t/Broke Are all temperatures within Yes/NoeP
Ice Present: /NA project specific guidelines?
elted/NA VOA Headspace Present? YepNA
pH Check Metals es/No/NA Total Phenolics Yes/No/NA NO3/NO2 Yes/No/NA Performed: Cyanide Yes/No/NA TPH— 418.1 Yes/No/NA Oil & Grease Yes/No/NA
Sulfide Yes/No/NA COD Yes/No/NA Total Phosphorous Yes/No/NA
Ammonia Yes/No/NA TEN Yes/No/NA Gross A.% Gamma Spec Yes/No/NA
Cooler Cooler Cooler Received
1
DCL Cooler No. Temp,
fp °C
Received pa, Cooler No. Temp,
°C
Received DCL Cooler No. Temp.
°C C18 6-4-)-- 4 C18 7 C18
2 C18 °C 5 C18 °C 8 C18 °C
3 C18 — oc 6 C18 °C 9 C18 °C ( — /
Taken By: MAIWZ(-4 --/ 440 Oc 110qt
\-.
Signal= PrIntedNune Date
CRIR.dec Revised 01/01/2018
ANALYTICAL REPORT
Report Date: May 31 , 2018 _..:...,___;_ _______ _
Kyle Ashby
Unified State Laboratories
Bureau of Chemical and Env Ser
4431 S 2700 W
Salt Lake City, UT 84119-8600
Client Sample ID Lab ID
MW-11 1813735001
MW-24 1813735002
MW-109 1813735003
MW-11 1813735004
MW-24 1813735005
MW-109 1813735006
Collect Date ·
05/15/18
05/15/18
05/15/18
05/15/18
05/15/18
05/15/18
Phone: [phone]
E-mail: kdashby@utah .gov
Workorder: I 34-1813735 I
Project ID: Utah Dept of Health
Purchase Order: NA
Project Manager Kevin W. Griffiths
Receive Date Sampling Site
05/16/18 2125766
05/16/18 2125768
05/16/18 2125769
05/16/18 2125761
05/16/18 2125762
05/16/18 2125763
ADDRESS 960 West LeVoy Drive, Salt Lake City, Utah, 84123 USA PHONE + 1 801 266 7700 FAX + 1 801 268 9992
ALS GROUP USA, CORP. An ALS Limited Company
Enulronmental J.11 WWW.alsglobal.(Offi
AIOHT SOLUTIOns RIGHT PARTnE:A
Page 1 of 19 Thu, 05/31/18 3:21 PM ENVREP-V4.8
Analytical Results
Sample ID: MW-11
Lab ID: 1813735001
Matrix: Water
Ana11a1a llethod . swuee
Preparation: Not Applicable
Analyte
Dichlorodifluoromethane
Chloromethane
Vinyl chloride
Bromomethane
Chloroethane
Dichlorofluoromethane
Trichlorofluoromethane
Ethyl ether
1 , 1-Dichloroethene
Freon 113
Acetone
lodomethane
Carbon disulfide
Methyl Acetate
Allyl chloride
Methylene chloride
trans-1,2-Dichloroethene
Methyl-I-butyl ether
cis-1 ,2-Dichloroethene
1, 1-Dichloroethane
2,2-Dichloropropane
2-Butanone
Ethyl acetate
Bromochloromethane
Tetrahydrofuran
Chloroform
1, 1, 1-Trichloroethane
Cyclohexane
1 , 1-Dichloropropene
1,2-Dichloroethane
Carbon tetrachloride
Benzene
Trichloroethane
Methylcyclohexane
1,2-Dichloropropane
Results Continued on Next Page
Page 2 of 19
ANALYTICAL REPORT
Result (ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
9.6
ND
ND
ND
21
ND
3.0
ND
Workorder: I 34-1813735 I
Client: Utah Department of Health
Project Manager: Kevin W. Griffiths
Sampling Site: 2125766 Collected: 05/15/2018
Media: 40 ml Amber Glass VOA Received: 05/16/2018
Sampling Parameter: NA
Analysis: SW 8260C, Water Instrument ID: 5975-J
Batch: EV0/7139 (HBN: 214983) Percent Solid: NA
Analyzed: 05/17/2018 13:45 Report Basis: Wet
MDL (ug/L) RL (ug/L) DIiution Qual
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
1.5 5.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
1.5 5.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
1.6 5.0 1 u
1.5 5.0 1 u
0.30 1.0 1 u
2.1 5.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1
0.30 1.0 1 u
0.30 1.0 1
0.30 1.0 1 u
Thu, 05/31/18 3:21 PM ENVREP-V4.8
Analytical Results
Sample ID: MW-1 1
Lab ID: 1813735001
Matrix: Water
Analvllls Method -SW 8260
Preparation: Not Applicable
Analyte
Dibromomethane
Bromodichloromethane
cis-1,3-Dichloropropene
4-Methyl-2-pentanone
trans-1 ,3-Dichloropropene
Ethyl methacrylate
1, 1,2-Trichloroethane
2-Hexanone
1,2-Dibromoethane
Toluene
1,3-Dichloropropane
; ,. Dibromochloromethane
Bromoform
Tetrachloroethene
1-Chlorohexane
Chlorobenzene
1, 1, 1,2-Tetrachloroethane
Ethyl benzene
m,p-Xylene
a-Xylene
Styrene
lsopropylbenzene
1, 1,2,2-Tetrachloroethane
Bromobenzene
1,2,3-Trichloropropane
trans-1,4-Dichloro-2-butene
Pentachloroethane
n-Propylbenzene
1,3,5-Trimethylbenzene
2-Chlorotoluene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
p-lsopropyltoluene
Results Continued on Next Page
Page 3 of 19
ANALYTICAL REPORT
Result (ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.9
ND
1.9
ND
0.74
ND
ND
ND
ND
ND
0.41
ND
ND
ND
ND
ND
ND
ND
Workorder: I 34-1813735 I
Client: Utah Department of Health
Project Manager: Kevin W. Griffiths
Sampling Site: 2125766 Collected: 05/15/2018
Media: 40 ml Amber Glass VOA Received: 05/16/2018
Sampling Parameter: NA
Analysis: SW 8260C, Water Instrument ID: 5975-J
Batch: EV0/7139 (HBN: 214983) Percent Solid: NA
Analyzed: 05/17/2018 13:45 Report Basis: Wet
MDL (ug/L) RL (ug/L) Dilution Qual
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
1.5 5.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
1.5 5.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1
0.30 2.0 1 u
0.30 1.0 1
0.30 1.0 1 u
0.30 1.0 1 J
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
1.5 5.0 1 u
0.30 1.0 1 u
0.30 1.0 1 J
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
Thu, 05/31/18 3:21 PM ENVREP-V4.8
Analytical Results
Sample ID: MW-11
lab ID: 1813735001
Matrix: Water
Anahala llethod • 8W UIO
Preparation: Not Applicable
Analyte
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Sample ID: MW-24
lab ID: 1813735002
Matrix: Water
Analvala Method • 8W 8280
Preparation: Not Applicable
Analyte
1,2-Dichloroethane
Benzene
!Analla .. .8Vf1121m
Preparation: Not Applicable
Analyte
Dichlorodifluoromethane
Chloromethane
Vinyl chloride
Bromomethane
Chloroethane
Dichlorofluoromethane
Trichlorofluoromethane
Ethyl ether
1, 1-Dichloroethene
Freon 113
Acetone
Results Continued on Next Page
Page 4 of 19
ANALYTICAL REPORT
Result (ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
Result (ug/L)
480
1200
Result (ug/L)
ND
ND
ND
ND
3.2
ND
ND
2.6
ND
ND
ND
Workorder: I 34-1813735 I
Client: Utah Department of Health
Project Manager: Kevin W. Griffiths
Sampling Site: 2125766 Collected: 05/15/2018
Media: 40 ml Amber Glass VOA Received: 05/16/2018
Sampling Parameter: NA
Analysis: SW 8260C, Water Instrument ID: 5975-J
Batch: EV0/7139 (HBN: 214983) Percent Solid: NA
Analvzed: 05/17/2018 13:45 ReDort Basis: Wet
MDL (ug/L) RL (ug/L) DIiution Quai
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
1.5 5.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.36 1.0 1 u
0.30 1.0 1 u
Sampling Site: 2125768 Collected: 05/15/2018
Media: 40 ml Amber Glass VOA Received: 05/16/2018
Sampling Parameter: NA
Analysis: SW 8260C, Water Instrument ID: 5975-J
Batch: EV0/7139 (HBN: 214983) Percent Solid: NA
Analvzed: 05/17/2018 14:18 ReDort Basis: Wet
MDL (ug/L) RL (ug/L) Dilution Quai
6.0 20 20
6.0 20 20
Analysis: SW 8260C, Water Instrument ID: 5975-J
Batch: EV0/7139 (HBN: 214983) Percent Solid: NA
Analyzed: 05/17/2018 14:34 Report Basis: Wet
MDL (ug/L) RL (ug/L) Dilution Qual
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2
0.60 2.0 2 u
0.60 2.0 2 u
3.0 10 2 u
Thu, 05/31/18 3:21 PM ENVREP-V4.8
Analytical Results
Sample ID: MW-24
Lab ID: 1813735002
Matrix: Water
Anahals Method· SW 8280
Preparation: Not Applicable
Analyte
lodomethane
Carbon disulfide
Methyl Acetate
Allyl chloride
Methylene chloride
trans-1,2-Dichloroethene
Methyl-t-butyl ether
cis-1 ,2-Dichloroethene
1, 1-Dichloroethane
2,2-Dichloropropane
2-Butanone
Ethyl acetate
Bromochloromethane
Tetrahydrofuran
Chloroform
1, 1, 1-Trichloroethane
Cyclohexane
1 , 1-Dichloropropene
Carbon tetrachloride
Trichloroethene
Methylcyclohexane
1,2-Dichloropropane
Dibromomethane
Bromodichloromethane
cis-1 ,3-Dichloropropene
4-Methyl-2-pentanone
trans-1 ,3-Dichloropropene
Ethyl methacrylate
1, 1,2-Trichloroethane
2-Hexanone
1,2-Dibromoethane
Toluene
1,3-Dichloropropane
Dibromochloromethane
Bromoform
Results Continued on Next Page
Page 5 of 19
ANALYTICAL REPORT
Result (ug/L)
ND
ND
ND
ND
ND
ND
4.5
ND
ND
ND
ND
ND
ND
ND
ND
ND
90
ND
ND
ND
47
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
11
ND
ND
ND
Workorder: I 34-1813735 I
Client: Utah Department of Health
Project Manager: Kevin W. Griffiths
Sampling Site: 2125768 Collected: 05/15/2018
Media: 40 ml Amber Glass VOA Received: 05/16/2018
Sampling Parameter: NA
Analysis: SW 8260C, Water Instrument ID: 5975-J
Batch: EV0/7139 (HBN: 214983) Percent Solid: NA
Analvzed: 05/17/2018 14:34 Report Basis: Wet
MDL (ug/L) RL (ug/L) Dilution Qual
0.60 2.0 2 u
0.60 2.0 2 u
3.0 10 2 u
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2 u
3.2 10 2 u
3.0 10 2 u
0.60 2.0 2 u
4.2 10 2 u
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2 u
3.0 10 2 u
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2 u
3.0 10 2 u
0.60 2.0 2 u
0.60 2.0 2
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2 u
Thu, 05/31/18 3:21 PM ENVREP-V4.8
Analytical Results
Sample ID: MW-24
Lab ID: 1813735002
Matrix: Water
Ana•la llelhod • SW 8HO
Preparation: Not Applicable
Analyte
Tetrachloroethene
1-Chlorohexane
Chlorobenzene
1, 1, 1,2-Tetrachloroethane
Ethylbenzene
m,p-Xylene
o-Xylene
Styrene
lsopropylbenzene
1, 1,2,2-Tetrachloroethane
Bromobenzene
1,2,3-Trichloropropane
trans-1,4-Dichloro-2-butene
Pentachloroethane
n-Propylbenzene
1,3,5-Trimethylbenzene
2-Chlorotoluene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
p-lsopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Page 6 of 19
ANALYTICAL REPORT
Result (ug/L)
ND
ND
ND
ND
120
110
4.7
ND
4.5
ND
ND
ND
ND
ND
11
79
ND
ND
ND
100
0.71
0.67
ND
ND
1.4
ND
ND
ND
ND
72
ND
Workorder: j 34-1813735 I
Client: Utah Department of Health
Project Manager: Kevin W. Griffiths
Sampling Site: 2125768 Collected: 05/15/2018
Media: 40 ml Amber Glass VOA Received: 05/16/2018
Sampling Parameter: NA
Analysis: SW 8260C, Water Instrument ID: 5975-J
Batch: EV0/7139 (HBN: 214983) Percent Solid: NA
Analvzed: 05/17/2018 14:34 Report Basis: Wet
MDL (ug/L) RL (ug/L) DIiution Qual
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2
0.60 4.0 2
0.60 2.0 2
0.60 2.0 2 u
0.60 2.0 2
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2 u
3.0 10 2 u
0.60 2.0 2 u
0.60 2.0 2
0.60 2.0 2
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2
0.60 2.0 2 J
0.60 2.0 2 J
0.60 2.0 2 u
0.60 2.0 2 u
0.60 2.0 2 J
0.60 2.0 2 u
3.0 10 2 u
0.60 2.0 2 u
0.60 2.0 2 u
0.72 2.0 2
0.60 2.0 2 u
Thu, 05/31/18 3:21 PM ENVREP-V4.8
Analytical Results
Sample ID: MW-109
Lab ID: 1813735003
Matrix: Water
Analvsls Method -SW 8280
Preparation: Not Applicable
Analyte
Dichlorodifluoromethane
Chloromethane
Vinyl chloride
Bromomethane
Chloroethane
Dichlorofluoromethane
Trichlorofluoromethane
Ethyl ether
1, 1-Dichloroethene
Freon 113
Acetone
lodomethane
Carbon disulfide
Methyl Acetate
Allyl chloride
Methylene chloride
trans-1,2-Dichloroethene
Methyl-I-butyl ether
cis-1 ,2-Dichloroethene
1, 1-Dichloroethane
2,2-Dichloropropane
2-Butanone
Ethyl acetate
Bromochloromethane
Tetrahydrofuran
Chloroform
1, 1, 1-Trichloroethane
Cyclohexane
1 , 1-Dichloropropene
1,2-Dichloroethane
Carbon tetrachloride
Benzene
Trichloroethene
Methylcyclohexane
1,2-Dichloropropane
Results Continued on Next Page
Page 7 of 19
ANALYTICAL REPORT
Result (ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
16
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
17
ND
4.0
ND
ND
ND
Workorder: I 34-1813735 I
Client: Utah Department of Health
Project Manager: Kevin W. Griffiths
Sampling Site: 2125769 Collected: 05/15/2018
Media: 40 ml Amber Glass VOA Received: 05/16/2018
Sampling Parameter: NA
Analysis: SW 8260C, Water Instrument ID: 5975-J
Batch: EV0/7139 (HBN: 214983) Percent Solid: NA
Analvzed: 05/17/2018 14:01 Report Basis: Wet
MDL (ug/L) RL (ug/L) Dilution Qual
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
1.5 5.0 1
0.30 1.0 1 u
0.30 1.0 1 u
1.5 5.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
1.6 5.0 1 u
1.5 5.0 1 u
0.30 1.0 1 u
2.1 5.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1
0.30 1.0 1 u
0.30 1.0 1
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
Thu, 05/31/18 3:21 PM ENVREP-V4.8
Analytical Results
Sample ID: MW-109
Lab ID: 1813735003
Matrix: Water
Analvala llMhod -SW 8280
Preparation: Not Applicable
Analyte
Dibromomethane
Bromodichloromethane
cis-1, 3-Dichloropropene
4-Methyl-2-pentanone
trans-1 ,3-Dichloropropene
Ethyl methacrylate
1, 1,2-Trichloroethane
2-Hexanone
1,2-Dibromoethane
Toluene
1,3-Dichloropropane
Dibromochloromethane
Bromoform
Tetrachloroethene
1-Chlorohexane
Chlorobenzene
1, 1, 1,2-Tetrachloroethane
Ethylbenzene
m,p-Xylene
o-Xylene
Styrene
lsopropylbenzene
1, 1,2,2-Tetrachloroethane
Bromobenzene
1,2,3-Trichloropropane
trans-1,4-Dichloro-2-butene
Pentachloroethane
n-Propylbenzene
1,3,5-Trimethylbenzene
2-Chlorotoluene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
p-lsopropyltoluene
Results Continued on Next Page
Page 8 of 19
ANALYTICAL REPORT
Result (ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3.4
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.5
ND
Workorder: I 34-1813735 I
Client: Utah Department of Health
Project Manager: Kevin W . Griffiths
Sampling Site: 2125769 Collected: 05/15/2018
Media: 40 ml Amber Glass VOA Received: 05/16/2018
Sampling Parameter: NA
Analysis: SW 8260C, Water Instrument ID: 5975-J
Batch: EV0/7139 (HBN: 214983) Percent Solid: NA
Analyzed: 05/17/2018 14:01 Report Basis: Wet
MDL (ug/L) RL (ug/L) DIiution Qual
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
1.5 5.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
1.5 5.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 2.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
1.5 5.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1 u
0.30 1.0 1
0.30 1.0 1 u
Thu, 05/31/18 3:21 PM ENVREP-V4.8
Analytical Results
Sample ID: MW-109
lab ID: 1813735003
Matrix: Water
Analvllls Method • SW 8260
Preparation: Not Applicable
Analyte
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Sample ID: MW-11
lab ID: 1813735004
Matrix: Water
Anal,,.ls Method • SW 8270
Preparation: EPA 3510, Sep Funnel SVOA
Batch: ENVX/26778 (HBN: 215063)
Prepared: 05/18/2018
Analyte
Pyridine
Phenol
Bis(2-chloroethyl)ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ether
4-Methylphenol
N-Nitrosodi-n-propyl amine
Hexachloroethane
Nitrobenzene
lsophorone
2-Nitrophenol
2,4-Dimethylphenol
Results Continued on Next Page
Page 9 of 19
ANALYTICAL REPORT
Workorder: I 34-1813735 I
Client: Utah Department of Health
Project Manager: Kevin W. Griffiths
Sampling Site: 2125769 Collected: 05/15/2018
Media: 40 ml Amber Glass VOA Received: 05/16/2018
Sampling Parameter: NA
Analysis: SW 8260C, Water Instrument ID: 5975-J
Batch: EV0/7139 (HBN: 214983) Percent Solid: NA
Analyzed: 05/17/2018 14:01 Report Basis: Wet
Result (ug/L) MDL (ug/L) RL (ug/L) Dilution Qual
ND 0.30 1.0 1 u
ND 0.30 1.0 1 u
ND 0.30 1.0 1 u
ND 0.30 1.0 1 u
ND 1.5 5.0 1 u
ND 0.30 1.0 1 u
ND 0.30 1.0 1 u
ND 0.36 1.0 1 u
ND 0.30 1.0 1 u
Sampling Site: 2125761 Collected: 05/15/2018
Media: 1000 ml Amber Glass Received: 05/16/2018
Sampling Parameter: NA
Weight/Volume Analysis: SW 82700, Water Instrument ID: 5975-H
Initial: 1000 ml Batch: ESV0/6416 (HBN: 215718) Percent Solid: NA
Final: 1 ml Analyzed: 05/29/2018 18:12 Report Basis: Wet
Result (ug/L) MDL (ug/L) RL (ug/L) Dilution Qual
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.7 5.0 1 u
Thu, 05/31/18 3:21 PM ENVREP-V4.8
Analytical Results
Sample ID: MW-11
Lab ID: 1813735004
Matrix: Water
Analvsls Method -SW 8270
Preparation: EPA 3510, Sep Funnel SVOA
Batch: ENVX/26778 (HBN: 215063)
Prepared: 05/18/2018
Analyte
Benzoic acid
Bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthalene
Hexachlorocyclopentadiene
2 ,4, 6-Trichlorophenol
2 ,4, 5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
2,6-Dinitrotoluene
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl phenyl ether
Fluorene
4-Nitroahiline
4,6-Dinitro-2-methylphenol
N-Nitrosodiphenylamine
4-Bromophenyl phenyl ether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Carbazole
Results Continued on Next Page
Page 10 of 19
ANALYTICAL REPORT
Workorder: I 34-1813735 I
Client: Utah Department of Health
Project Manager: Kevin W. Griffiths
Sampling Site: 2125761 Collected: 05/15/2018
Media: 1000 ml Amber Glass Received: 05/16/2018
Sampling Parameter: NA
WeighW£olyme Analysis: SW 8270D, Water Instrument ID: 5975-H
Initial: 1000 ml Batch: ESV0/6416 (HBN: 215718) Percent Solid: NA
Final: 1 ml Analyzed: 05/29/2018 18:12 Report Basis: Wet
Result (ug/L) MDL (ug/L) RL (ug/L) Dilution Qual
ND 15 20 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.8 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.7 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 11 20 1 u
ND 7.5 20 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 7.6 20 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 7.5 20 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
Thu, 05/31/18 3:21 PM ENVREP-V4.8
Analytical Results
Sample ID: MW-11
Lab ID: 1813735004
Matrix: Water
Anahlllls Method • SW 8270
Preparation: EPA 3510, Sep Funnel SVOA
Batch: ENVX/26778 (HBN: 215063)
Prepared: 05/18/2018
Analyte
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
3,3'-Dichlorobenzidine
Benzo(a)anthracene
Chrysene
Bis(2-ethylhexyl)phthalate
Di-n-octylphthalate
Benzo(b )fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1,2,3-c,d)pyrene
Dibenzo(a,h)anthracene
Benzo(g,h,i)perylene
Analvsls Method -SW 8270
Preparation: EPA 3510, Sep Funnel SVOA
Batch: ENVX/26778 (HBN: 215063)
Prepared: 05/18/2018
Tentatively Identified Compound
Unknown Aromatic Acid
Unknown Aromatic Acid
Unknown Aromatic Acid
Unknown Aromatic Acid
Unknown Aromatic Acid
Benzene, 1-methoxy-4-phenoxy-
1-Hydroxy-4-methyl-2-oxo-1 ,2-
dihydro-3-quinoline
Unknown Aromatic Acid
Unknown Aromatic Acid
Unknown Aromatic Acid
Unknown Aromatic Acid
Unknown Aromatic Acid
Unknown Aromatic Acid
Unknown Aromatic Acid
Unknown Aromatic Acid
Results Continued on Next Page
Page 11 of 19
ANALYTICAL REPORT
Workorder: J 34-1813735 J
Client: Utah Department of Health
Project Manager: Kevin W. Griffiths
Sampling Site: 2125761 Collected: 05/15/2018
Media: 1000 ml Amber Glass Received: 05/16/2018
Sampling Parameter: NA
WeighWol!,!m!l Analysis: SW 8270D, Water Instrument ID: 5975-H
Initial: 1000 ml Batch: ESV0/6416 (HBN: 215718) Percent Solid: NA
Final: 1 ml Analvzed: 05/29/2018 18:12 Report Basis: Wet
Result (ug/L) MDL (ug/L} RL (ug/L} Dilution Qual
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.6 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
WeighWolume Analysis: SW 8270D, Water Instrument ID: 5975-H
Initial: 1000 ml Batch: ESV0/6416 (HBN: 215718) Percent Solid: NA
Final: 1 ml Analyzed: 05/29/2018 18:12 Report Basis: Wet
Retention
Result (ug/L) Time Dilution Qual
12 10.76 1 J
8.7 11.01 1 J
18 11.18 1 J
19 11.24 1 J
30 11.36 1 J
33 11.41 1 J
34 11.44 1 J
18 11.49 1 J
34 11.67 1 J
26 11.75 1 J
20 11.79 1 J
29 11.82 1 J
32 11.85 1 J
5.9 11.90 1 J
7.1 11.98 1 J
Thu, 05/31/18 3:21 PM ENVREP-V4.8
Analytical Results
Sample ID: MW-11
Lab ID: 1813735004
Matrix: Water -. ·-swmo
Preparation: EPA 3510, Sep Funnel SVOA
Batch: ENVX/26778 (HBN: 215063)
Prepared: 05/18/2018
Tentatively Identified Compound
Unknown Aromatic Acid
Unknown Aromatic Acid
Unknown Aromatic Hydrocarbon
Unknown Aromatic Hydrocarbon
Sample ID: MW-24
Lab ID: 1813735005
Matrix: Water
Anahala llethod. sw:m.o
Preparation: EPA 3510, Sep Funnel SVOA
Batch: ENVX/26778 (HSN: 215063)
Prepared: 05/18/2018
Analyte
Pyridine
Phenol
Sis(2-chloroethyl)ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ether
4-Methylphenol
N-Nitrosodi-n-propyl amine
Hexachloroethane
Nitrobenzene
lsophorone
2-Nitrophenol
2,4-Dimethylphenol
Senzoic acid
Bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Results Continued on Next Page
Page 12 of 19
ANALYTICAL REPORT
Workorder: I 34-1813735 I
Client: Utah Department of Health
Project Manager: Kevin W. Griffiths
Sampling Site: 2125761 Collected: 05/15/2018
Media: 1000 ml Amber Glass Received: 05/16/2018
Sampling Parameter: NA
Weight/Volum~ Analysis: SW 8270D, Water Instrument ID: 5975-H
Initial: 1000 ml Batch: ESV0/6416 (HSN: 215718) Percent Solid: NA
Final: 1 ml Analyzed: 05/29/2018 18:12 Report Basis: Wet
Retention
Result (ug/L) Time Dilution Qual
25 12.09 1 J
26 12.14 1 J
6.6 17.35 1 J
5.9 17.57 1 J
Sampling Site: 2125762 Collected: 05/15/2018
Media: 1000 ml Amber Glass Received: 05/16/2018
Sampling Parameter: NA
Weight/Volume Analysis: SW 8270D, Water Instrument ID: 5975-H
Initial: 1000 ml Batch: ESV0/6416 (HSN: 215718) Percent Solid: NA
Final: 1 ml Analvzed: 05/29/201818:44 Report Basis: Wet
Result (ug/L) MDL (ug/L) RL (ug/L) DIiution Qual
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.7 5.0 1 u
ND 15 20 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
Thu, 05/31/18 3:21 PM ENVREP-V4.8
Analytical Results
Sample ID: MW-24
Lab ID: 1813735005
Matrix: Water
Analvsls Method -SW 8270
Preparation: EPA 3510, Sep Funnel SVOA
Batch: ENVX/26778 (HBN: 215063)
Prepared: 05/18/2018
Analyte
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthalene
Hexachlorocyclopentadiene
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
2,6-Dinitrotoluene
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl phenyl ether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
N-Nitrosodiphenylamine
4-Bromophenyl phenyl ether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Carbazole
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
Results Continued on Next Page
Page 13 of 19
ANALYTICAL REPORT
Workorder: I 34-1813735 I
Client: Utah Department of Health
Project Manager: Kevin W. Griffiths
Sampling Site: 2125762 Collected: 05/15/2018
Media: 1000 ml Amber Glass Received: 05/16/2018
Sampling Parameter: NA
W!!ighWolume Analysis: SW 8270D, Water Instrument ID: 5975-H
Initial: 1000 ml Batch: ESV0/6416 (HBN: 215718) Percent Solid: NA
Final: 1 ml Analvzed: 05/29/2018 18:44 Report Basis: Wet
Result (ug/L} MDL (ug/L) RL (ug/L) Dilution Qual
35 1.5 5.0 1
ND 1.5 5.0 1 u
ND 1.8 5.0 1 u
ND 1.5 5.0 1 u
20 1.5 5.0 1
ND 1.7 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 11 20 1 u
ND 7.5 20 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 7.6 20 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 7.5 20 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
Thu, 05/31/18 3:21 PM ENVREP-V4.8
Analytical Results
Sample ID: MW-24
Lab ID: 1813735005
Matrix: Water
Anahale llethod • SW 8270
Preparation: EPA 3510, Sep Funnel SVOA
Batch: ENVX/26778 (HBN: 215063)
Prepared: 05/18/2018
Analyte
3,3'-Dichlorobenzidine
Benzo(a)anthracene
Chrysene
Bis(2-ethylhexyl)phthalate
Di-n-octylphthalate
Benzo(b )fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1,2,3-c,d)pyrene
Dibenzo(a,h)anthracene
Benzo(g, h, i )perylene
Anahale Method. SW 8270
Preparation: EPA 3510, Sep Funnel SVOA
Batch: ENVX/26778 (HBN: 215063)
Prepared: 05/18/2018
Tentatively Identified Compound
Unknown Organic Acid
Unknown Organic Acid
Ethylbenzene
Mesitylene
2-Cyclopenten-1-one, 3,4-dimethyl-
Benzene, 1,2,3-trimethyl-
lndane
2-Cyclopenten-1-one, 3,4,5-trimethyl-
Ethanone, 1-( 1-cyclohexen-1-yl)-
Mequinol
Ethanamine, N-cyclohexylidene-
1 H-lndene, 1-methyl-
3-tert-Butyl-2-pyrazolin-5-one
7-Methylindan-1-one
2-Pentanone, 3-(phenylmethylene )-
Benzoic acid, 2,4,5-trimethyl-
4'-(2-Methylpropyl)acetophenone
Unknown
2,3,5,6-Tetramethylbenzoic acid
Results Continued on Next Page
Page 14 of 19
ANALYTICAL REPORT
Workorder: I 34-1813735 I
Client: Utah Department of Health
Project Manager: Kevin W. Griffiths
Sampling Site: 2125762 Collected: 05/15/2018
Media: 1000 ml Amber Glass Received: 05/16/2018
Sampling Parameter: NA
WgighWQIUm!! Analysis: SW 8270D, Water Instrument ID: 5975-H
Initial: 1000 ml Batch: ESV0/6416 (HBN: 215718) Percent Solid: NA
Final: 1 ml Analvzed: 05/29/2018 18:44 Report Basis: Wet
Result (ug/L) MDL (ug/L) RL (ug/L) Dilution Qual
ND 1.6 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
WeighWolume Analysis: SW 8270D, Water Instrument ID: 5975-H
Initial: 1000 ml Batch: ESV0/6416 (HBN: 215718) Percent Solid: NA
Final: 1 ml Analvzed: 05/29/2018 18:44 Report Basis: Wet
Retention
Result (ug/L) Time Dilution Qual
39 4.50 1 J
50 4.53 1 J
36 4.92 1 J
20 5.91 1 J
85 6.12 1 J
50 6.36 1 J
23 6.50 1 J
·50 6.63 1 J
92 6.85 1 J
22 6.93 1 J
18 6.95 1 J
26 7.34 1 J
22 7.69 1 J
67 8.97 1 J
25 9.11 1 J
19 9.29 1 J
36 9.50 1 J
17 9.76 1 J
26 9.81 1 J
Thu, 05/31/18 3:21 PM ENVREP-V4.8
Analytical Results
Sample ID: MW-24
lab ID: 1813735005
Matrix: Water
Anahals Method • SW 8270
Preparation: EPA 3510, Sep Funnel SVOA
Batch: ENVX/26778 (HBN: 215063)
Prepared: 05/18/2018
Tentatively Identified Compound
5-Aminoindan
Sample ID: MW-109
l ab ID: 1813735006
Matrix: Water
Anahals Method • SW 8270
Preparation: EPA 3510, Sep Funnel SVOA
Batch: ENVX/26778 (HBN: 215063)
Prepared: 05/18/2018
Analyte
Pyridine
Phenol
Bis(2-chloroethyl)ether
2-Chlorophenol
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ether
4-Methylphenol
N-Nitrosodi-n-propyl amine
Hexachloroethane
Nitrobenzene
lsophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic acid
Bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
Results Continued on Next Page
Page15of19
ANALYTICAL REPORT
Workorder: I 34-1813735 I
Client: Utah Department of Health
Project Manager: Kevin W. Griffiths
Sampling Site: 2125762 Collected: 05/15/2018
Media: 1000 ml Amber Glass Received: 05/16/2018
Sampling Parameter: NA
WeighWolum1 Analysis: SW 8270D, Water Instrument ID: 5975-H
Initial: 1000 ml Batch: ESV0/6416 (HBN: 215718) Percent Solid: NA
Final: 1 ml Analvzed: 05/29/2018 18:44 Report Basis: Wet
Retention
Result (ug/L) Time Dilution Qual
18 10.33 1 J
Sampling Site: 2125763 Collected: 05/15/2018
Media: 1000 ml Amber Glass Received: 05/16/2018
Sampling Parameter: NA
WeighWolume Analysis: SW 8270D, Water Instrument ID: 5975-H
Initial: 1000 ml Batch: ESV0/6416 (HBN: 215718) Percent Solid: NA
Final: 1 ml Analyzed: 05/29/2018 19:17 Report Basis: Wet
Result (ug/L) MDL (ug/L) RL (ug/L) Dilution Qual
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.7 5.0 1 u
ND 15 20 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
2.4 1.5 5.0 1 J
ND 1.5 5.0 1 u
ND 1.8 5.0 1 u
Thu, 05/31/18 3:21 PM ENVREP-V4.8
Analytical Results
Sample ID: MW-109
Lab ID: 1813735006
Matrix: Water
Analvala lhlhod • 8W 8270
Preparation: EPA 3510, Sep Funnel SVOA
Batch: ENVX/26778 (HBN: 215063)
Prepared: 05/18/2018
Analyte
4-Chloro-3-methylphenol
2-Methylnaphthalene
Hexachlorocyclopentadiene
2.4,6-Trichlorophenol
2.4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
2,6-Dinitrotoluene
Acenaphthylene
3-Nitroaniline
Acenaphthene
2.4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2.4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl phenyl ether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
N-Nitrosodiphenylamine
4-Bromophenyl phenyl ether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Carbazole
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
3,3'-Dichlorobenzidine
Benzo(a)anthracene
Chrysene
Results Continued on Next Page
Page 16 of 19
ANALYTICAL REPORT
Workorder: I 34-1813735 I
Client: Utah Department of Health
Project Manager: Kevin W. Griffiths
Sampling Site: 2125763 Collected: 05/15/2018
Media: 1000 ml Amber Glass Received: 05/16/2018
Sampling Parameter: NA
Weigh~olum~ Analysis: SW 82700, Water Instrument ID: 5975-H
Initial: 1000 ml Batch: ESV0/6416 (HBN: 215718) Percent Solid: NA
Final: 1 ml Analyzed: 05/29/2018 19:17 Report Basis: Wet
Result (ug/L) MDL (ug/L) RL (ug/L) Dilution Qual
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.7 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 11 20 1 u
ND 7.5 20 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 7.6 20 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 7.5 20 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
ND 1.6 5.0 1 u
ND 1.5 5.0 1 u
ND 1.5 5.0 1 u
Thu, 05/31/18 3:21 PM ENVREP-V4.8
Analytical Results
Sample ID: MW-109
Lab ID: 1813735006
Matrix: Water
Analvllls Method • SW 8270
Preparation: EPA 3510, Sep Funnel SVOA
Batch: ENVX/26778 (HBN: 215063)
Prepared: 05/18/2018
ANALYTICAL REPORT
Workorder: I 34-1813735 I
Client: Utah Department of Health
Project Manager: Kevin W. Griffiths
Sampling Site: 2125763 Collected: 05/15/2018
Media: 1000 ml Amber Glass Received: 05/16/2018
Sampling Parameter: NA
WeighWolume Analysis: SW 82700, Water Instrument ID: 5975-H
Initial: 1000 ml Batch: ESV0/6416 (HBN: 215718) Percent Solid: NA
Final: 1 ml Analvzed: 05/29/2018 19:17 Reoort Basis: Wet
Analyte Result (ug/L) MDL (ug/L) RL (ug/L) Dilution Qual
Bis(2-ethylhexyl}phthalate ND 1.5 5.0 1 u
Di-n-octylphthalate ND 1.5 5.0 1 u
Benzo(b )fluoranthene ND 1.5 5.0 1 u
Benzo(k)fluoranthene ND 1.5 5.0 1 u
Benzo(a)pyrene ND 1.5 5.0 1 u
lndeno(1 ,2,3-c,d)pyrene ND 1.5 5.0 1 u
Dibenzo(a,h)anthracene ND 1.5 5.0 1 u
Benzo(g, h, i)perylene ND 1.5 5.0 1 u
Analvllla Method • SW 8270
Preparation: EPA 3510, Sep Funnel SVOA WeighWolume Analysis: SW 82700, Water Instrument ID: 5975-H
Batch: ENVX/26778 (HBN: 215063) Initial: 1000 ml Batch: ESV0/6416 (HBN: 215718) Percent Solid: NA
Prepared: 05/18/2018 Final: 1 ml .Analyzed: 05/29/2018 19:17 Report Basis: Wet
Retention
Tentatively Identified Compound Result (ug/L) Time Dilution Qual
1,2-Ethanediol, monoacetate 4.4 4.72 1 J
Ethanone, 1-(1-cyclohexen-1-yl)-5.9 6.83 1 J
3-Hexene-2,5-dione 4.2 6.92 1 J
Comments
I Workorder: 1813735
8260 Comments: Sample 1813735002 (MW-24) was analyzed solely at dilution to bring the analytes of interest within the linear
range and to preserve instrument integrity.
Quality Control: SW 8260 -(HBN: 214983)
8260 QC Comments: The percent difference (or percent drift for a regression fit) for target compounds in the CVS standard
must generally be less than 20% relative to the average response from the initial calibration curve. The analyte acetone did not
meet this criteria and results for this compound should be considered estimates.
Quality Control: SW 8270 -(HBN: 215718)
The initial calibration did not pass method criteria for 3-nitroaniline, 4-nitroaniline, and carbazole. The CCV did not pass method
criteria for 2,4-dimethylphenol, 4-chloroaniline, 3-nitroaniline, 2,4-dinitrophenol, and 4-nitroaniline. Any results for these
compounds should be treated as semi-quantitative.
The LCSD was outside of percent recovery QC limits for 3-nitroaniline and 2,4-dinitrophenol. RPD was outside of QC limits for 6
compounds.
Report Authorization (ISi is an electronic signature that complies with 21 CFR Part 11)
Method Analvst
SW 8260
Page 17 of 19
ISi Christopher Q. Coleman
0511812018 11 :21
Thu, 05/31/18 3:21 PM
PeerRevlew
ISi Thomas J. Masoian
0512212018 08:33
ENVREP-V4.8
ANALYTICAL REPORT
Workorder: I 34-1813735 j
Client: Utah Department of Health
Project Manager: Kevin W. Griffiths
Report Authorization (IS/ is an electronic signature that complies with 21 CFR Part 11)
Method Analvat
SW8270
Laboratory Contact Information
ALS Environmental
960 W Levoy Drive
Salt Lake City, Utah 84123
General Lab Comments
/S/ David T eynor
05/31/201811:37
Phone: [phone]
Email: [e-mail]
Web: www.alsslc.com
The results provided in this report relate only to the items tested.
Samples were received in acceptable condition unless otherwise noted.
Samples have not been blank corrected unless otherwise noted.
This test report shall not be reproduced, except in full, without written approval of ALS.
ISi Thomas J. Masoian
05/31/2018 14:57
ALS provides professional analytical services for all samples submitted. ALS is not in a position to interpret the data and
assumes no responsibility for the quality of the samples submitted.
All quality control samples processed with the samples in this report yielded acceptable results unless otherwise noted.
ALS is accredited for specific fields of testing (scopes) in the following testing sectors. The quality system implemented at ALS
conforms to accreditation requirements and is applied to all analytical testing performed by ALS. The following table lists testing
sector, accreditation body, accreditation number and website. Please contact these accrediting bodies or your ALS project
manager for the current scope of accreditation that applies to your analytical testing.
Testing Sector
Environmental
Page 18 of 19
Accreditation Body
PJLA (DoD ELAP)
Utah (TNI)
Nevada
Oklahoma
Iowa
Certificate
Number
Website
Thu, 05/31/18 3:21 PM ENVREP-V4.8
ANALYTICAL REPORT
Workorder: I 34-1813735 I
Client: Utah Department of Health
Project Manager: Kevin W. Griffiths
Result Symbol Definitions
MDL = Method Detection Limit, a statistical estimate of method/media/instrument sensitivity.
RL = Reporting Limit, a verified value of method/media/instrument sensitivity.
CRDL = Contract Required Detection Limit
Reg. Limit= Regulatory Limit.
ND = Not Detected, testing result not detected above the MDL or RL.
< This testing result is less than the numerical value.
** No result could be reported, see sample comments for details.
Qualifier Symbol Definitions
U = Qualifier indicates that the analyte was not detected above the MDL.
J = Qualifier Indicates that the analyte value is between the MDL and the RL. It is also used to indicate an estimated value for
tentatively identified compounds in mass spectrometry where a 1 :1 response is assumed.
B = Qualifier indicates that the analyte was detected in the blank.
E = Qualifier indicates that the analyte result exceeds calibration range.
P = Qualifier indicates that the RPD between the two columns is greater than 40%.
Page 19 of 19 Thu, 05/31/18 3:21 PM ENVREP-V4.8
Analysi!..lnformatlon
Workorder: 1813735
Limits: Historical/Performance
Basis: ALS Laboratory Group
BIMk
MB: 601571
Analyzed: 05/29/2018 15:28
Units: ug/L
Analyte
Pyridine
Phenol
Bis(2-chloroethyl)ether
2-Chlorophenol
1,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Benzyl alcohol
1,2-Dichlorobenzene
2-Methylphenol
bis(2-Chloroisopropyl)ether
4-Methylphenol
N-Nitrosodi-n-propyl amine
Hexachloroethane
Nitrobenzene
lsophorone
2-Nitrophenol
2,4-Dimethylphenol
Benzoic acid
Bis(2-Chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol
2-Methylnaphthalene
Hexachlorocyclopentadiene
2,4, 6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
Dimethylphthalate
2,6-Dinitrotoluene
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenol
Page 1 of 11
Quality Control Sample
Batch Report
Preparation: EPA 3510, Sep Funnel SVOA
Batch: ENVX/26778 (HBN: 215063)
Prepared By: Christopher Webb
Result MDL RL
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.7 5.00
ND 15 20.0
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.8 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.7 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 11 20.0
Thursday, May 31 , 2018
Analysis: SW 8270
Batch: ESV0/6416 (HBN: 215718)
Analyzed By: David Teynor
I
QCSV4.4
Analysis Information
Workorder: 1813735
Limits: Historical/Performance
Basis: ALS Laboratory Group
Blank
MB: 601571
Analyzed: 05/29/2018 15:28
Units: ug/L
Analyte
4-Nitrophenol
Dibenzofuran
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl phenyl ether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
N-Nitrosodiphenylamine
4-Bromophenyl phenyl ether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Carbazole
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
3,3'-Dichlorobenzidine
Benzo(a)anthracene
Chrysene
Bis(2-ethylhexyl)phthalate
Di-n-octylphthalate
Benzo(b )fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenzo(a,h)anthracene
Benzo(g,h,i)perylene
LCS: 601572
Analyzed: 05/29/2018 16:01
Dilution: 1
Units: u /L
Analyte
Pyridine
Page 2 of 11
Quality Control Sample
Batch Report
Preparation: EPA 3510, Sep Funnel SVOA
Batch: ENVX/26778 (HBN: 215063)
Prepared By: Christopher Webb
Result MDL RL
ND 7.5 20.0
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 7.6 20.0
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 7.5 20.0
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.6 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
ND 1.5 5.00
Control~!• lca18
Result Target % Rec QC Limits
15.9 40.0 39.7 1.9 100.0
Analysis: SW 8270
Batch: ESV0/6416 (HBN: 215718)
Analyzed By: David Teynor
LCSD: 601573
Analyzed: 05/29/2018 16:35
Dilution: 1
Units: u /L
Result % Rec RPO QC Limits
14.9 37.2 6.52 0.0 40.0
I
Thursday, May 31, 2018 QCS V4.4
Analysis lnforrna!(on
Workorder: 1813735
Limits: Historical/Performance
Basis: ALS Laboratory Group
Quality Control Sample
Batch Report
Preparation: EPA 3510, Sep Funnel SVOA
Batch: ENVX/26778 (HBN: 215063)
Prepared By: Christopher Webb
Analysis: SW 8270
Batch: ESV0/6416 (HBN: 215718)
Analyzed By: David Teynor
II i ControfSimnle. LaboratofY. ControfBimnle D~lcate I
LCS: 601572 LCSD: 601573
Analyzed: 05/29/2018 16:01 Analyzed: 05/29/2018 16:35
Dilution: 1 Dilution: 1
Units: ua/L Units: ua/L
Analyte Result Target %Rec QC Limits Result %Rec RPD QC Limits
Phenol 11 .5 40.0 28.7 8.4 100.0 12.3 30.7 6.70 0.0 20.0
Bis(2-chloroethyl)ether 24.5 40.0 61 .3 15.3 109.6 27.0 67.5 9.61 0.0 20.0
2-Chlorophenol 28.8 40.0 72.0 14.5 102.2 30.8 77.0 6.67 0.0 20.0
1,3-Dichlorobenzene 25.6 40.0 64.1 0.0 102.1 25.3 63.2 1.48 0.0 20.0
1 ,4-Dichlorobenzene 24.2 40.0 60.5 0.0 102.6 24.2 60.6 0.135 0.0 20.0
Benzyl alcohol 26.3 40.0 65.8 22.3 116.5 28.4 71 .1 7.76 0.0 40.0
1,2-Dichlorobenzene 25.2 40.0 63.0 2.6 106.4 25.5 63.8 1.31 0.0 20.0
2-Methylphenol 24.1 40.0 60.2 26.8 100.0 26.0 65.0 7.76 0.0 20.0
bis(2-Chloroisopropyl)ether 26.6 40.0 66.5 20.5 113.3 29.0 72.5 8.67 0.0 40.0
N-Nitrosodi-n-propyl amine 25.7 40.0 64.2 30.9 118.2 27.7 69.3 7.65 0.0 20.0
Hexachloroethane 19.9 40.0 49.8 7.5 100.0 18.9 47.2 5.48 0.0 20.0
Nitrobenzene 23.0 40.0 57.4 24.3 101.8 29.5 73.8 * 25.0 0.0 20.0
lsophorone 24.7 40.0 61 .8 21.5 117.6 31 .9 79.8 * 25.5 0.0 20.0
2-Nitrophenol 23.9 40.0 59.9 30.9 100.0 36.0 90.1 * 40.3 0.0 20.0
2,4-Dimethylphenol 19.5 40.0 48.8 3.0 102.3 22.3 55.8 13.4 0.0 20.0
Benzoic acid 14.1 40.0 35.3 0.0 100.0 15.9 39.7 11.7 0.0 40.0
Bis(2-Chloroethoxy)methane 28.8 40.0 72.1 33.7 100.8 31 .7 79.2 9.34 0.0 20.0
2,4-Dichlorophenol 29.1 40.0 72.9 36.7 114.3 37.0 92.6 23.8 0.0 40.0
1,2,4-Trichlorobenzene 25.6 40.0 64.0 10.8 110.4 30.8 77.0 18.5 0.0 20.0
Naphthalene 25.7 40.0 64.4 22.0 112.9 28.7 71.7 10.8 0.0 20.0
4-Chloroaniline 13.2 40.0 32.9 0.0 160.6 13.7 34.4 4.43 0.0 40.0
Hexachlorobutadiene 19.0 40.0 47.6 10.0 100.0 23.6 59.1 21 .6 0.0 40.0
4-Chloro-3-methylphenol 30.4 40.0 75.9 36.1 108.4 35.8 89.6 16.4 0.0 20.0
2-Methylnaphthalene 25.5 40.0 63.7 25.5 118.8 32.7 81.7 * 24.9 0.0 20.0
Hexachlorocyclopentadiene 20.3 40.0 50.8 7.0 100.0 18.0 45.1 12.0 0.0 40.0
2,4,6-Trichlorophenol 36.6 40.0 91.4 33.8 121 .1 34.4 85.9 6.19 0.0 20.0
2,4,5-Trichlorophenol 35.7 40.0 89.2 37.4 118.9 33.6 84.0 5.99 0.0 20.0
2-Chloronaphthalene 31 .6 40.0 79.0 31 .2 114.4 29.2 73.1 7.84 0.0 20.0
2-Nitroaniline 28.8 40.0 72.0 37.0 120.1 25.9 64.7 10.6 0.0 40.0
Dimethylphthalate 34.9 40.0 87.2 46.8 116.9 32.1 80.2 8.35 0.0 30 .0
2,6-Dinitrotoluene 36.1 40.0 90.3 49.5 118.5 31 .8 79.4 12.8 0.0 20.0
Acenaphthylene 31.0 40.0 77.6 41.2 111 .0 30.0 75.1 3.32 0.0 20.0
3-Nitroaniline 19.8 40.0 49.4 29.1 143.9 11.2 * 28.1 * 55.0 0.0 40.0
Acenaphthene 29.1 40.0 72.7 41.0 113.9 32.7 81 .7 11.6 0.0 20.0
2,4-Dinitrophenol 49.0 40.0 122 0.0 127.2 52.7 * 132 7.32 0.0 20.0
4-Nitrophenol 12.7 40.0 31 .6 0.0 100.0 8.75 21 .9 36.5 0.0 40.0
Dibenzofuran 33.6 40.0 84.1 41.6 117.6 32.7 81 .7 2.80 0.0 20.0
Page 3 of 11 Thursday, May 31, 2018 QCS V4.4
Analysis Information
Workorder: 1813735
Limits: Historical/Performance
Basis: ALS Laboratory Group
LCS: 601572
Analyzed: 05/29/2018 16:01
Dilution: 1
Units: ug/L
Analyte
2,4-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl phenyl ether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Carbazole
Di-n-butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
3,3'-Dichlorobenzidine
Benzo(a)anthracene
Chrysene
Bis(2-ethylhexyl)phthalate
Di-n-octylphthalate
Benzo(b )fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1,2,3-c,d)pyrene
Dibenzo(a,h)anthracene
Benzo(g ,h, i)perylene
Surm11ate Recoveries
Surrogate 2-Fluorophenol
QC Limits 0.0
Units ug/L
Lab ID Result
601571-MB 22.0
601572-LCS 22.3
601573-LCSD 24.7
1813795001 5.16
Page 4 of 11
Quality Control Sample
Batch Report
Preparation: EPA 3510, Sep Funnel SVOA
Batch: ENVX/26778 (HBN: 215063)
Prepared By: Christopher Webb
Result Target %Rec QC Limits
36.9 40.0 92.2 48.9 124.7
33.4 40.0 83.5 49.5 118.5
38.0 40.0 95.1 44.2 118.9
31.7 40.0 79.2 46.5 118.6
21 .0 40.0 52.4 4.9 164.0
41.5 40.0 104 24.2 128.7
38.5 40.0 96.3 42.9 119.9
37.7 40.0 94.3 42.4 122.4
39.1 40.0 97.8 29.0 135.3
30.7 40.0 76.8 45.7 119.7
32.3 40.0 80.9 45.7 120.6
44.1 40.0 110 11.7 156.9
30 .3 40.0 75.9 47.0 127.8
34.3 40.0 85.8 40.6 133.2
34.6 40.0 86.4 47.5 121.4
29.1 40.0 72.7 48.6 120.8
28.5 40.0 71.3 7.2 155.3
32.8 40.0 81 .9 49.8 117.3
33.0 40.0 82.5 50.1 123.6
28.9 40.0 72.2 50.6 125.2
31.8 40.0 79.5 47.6 121.1
36.7 40.0 91.6 49.0 113.1
34.4 40.0 86.0 51.7 117.4
28.3 40.0 70.7 49.0 114.4
39.2 40.0 98.0 40.3 124.4
37.2 40.0 93.0 44.5 124.3
39.6 40.0 98.9 42.1 124.5
Phenol-d5
I 121 .0 0.0 I 145.0
ug/L
Target % Recovery Result Target
50.0 43.9 14.1 50.0
50.0 44.6 14.5 50.0
50.0 49.3 14.9 50.0
50.0 10.3 5.07 50.0
Thursday, May 31, 2018
Analysis: SW 8270
Batch: ESV0/6416 (HBN: 215718)
Analyzed By: David Teynor
LCSD: 601573
Analyzed: 05/29/2018 16:35
Dilution: 1
Units: ug/L
Result %Rec RPO QC Limits
31 .0 77.6 17.2 0.0 20.0
33.1 82.6 1.08 0.0 30.0
36.3 90.6 4.80 0.0 20.0
33.1 82.8 4.45 0.0 20.0
20.0 50.1 4.56 0.0 40.0
36.4 91.0 13.2 0.0 40.0
36.5 91 .1 5.54 0.0 20.0
35.2 87.9 6.98 0.0 20.0
31.2 77.9 111 22.7 0.0 20.0
32.7 81.8 6.21 0.0 20.0
37.5 93.6 14.6 0.0 20.0
35.2 88.0 22.3 0.0 40.0
28.9 72.2 4.94 0.0 30.0
32.8 82.0 4.54 0.0 20.0
37.1 92.7 7.03 0.0 20.0
31 .1 77.8 6.78 0.0 30.0
30.8 77.1 7.75 0.0 40.0
35.3 88.3 7.51 0.0 20.0
35.2 87.9 6.38 0.0 20.0
31.0 77.6 7.23 0.0 30.0
30.6 76.6 3.64 0.0 30.0
35.5 88.8 3.19 0.0 20.0
34.0 85.1 1.06 0.0 20.0
32.8 82.1 14.9 0.0 20.0
37.9 94.8 3.31 0.0 20.0
36.1 90.3 2.91 0.0 20.0
38.2 95.5 3.56 0.0 20.0
Nitrobenzene-d5
22.0 I 130.3
ug/L
% Recovery Result Target % Recovery
28.2 32.6 50.0 65.3
28.9 26.8 50.0 53.7
29.7 33.6 50.0 67.1
10.1 5.91 50.0 111 11.8
QCS V4.4
~[lalysis lnformcttton
Workorder: 1813735
Limits: Historical/Performance
Basis: ALS Laboratory Group
Surroaate Recoveries
Surroaate 2-Fluorophenol
QC Limits 0.0
Units ug/L
Quality Control Sample
Batch Report
Preparation: EPA 3510, Sep Funnel SVOA
Batch: ENVX/26778 (HBN: 215063)
Prepared By: Christopher Webb
Phenol-d5
I 121 .0 0.0 I 145.0
ug/L
Analysis: SW 8270
Batch: ESV0/6416 (HBN: 215718)
Analyzed By: David Teynor
Nitrobenzene-d5
22.0 I 130.3
UQ/L
Lab ID Result Target % Recovery Result Target % Recovery Result Target % Recovery
1813735004 18.3 50.0 36.7 12.9 50.0 25.8 27.9 50.0 55.9
1813735005 17.8 50.0 35.6 11.6 50.0 23.1 30.7 50.0 61.3
1813735006 21 .0 50.0 42.0 15.1 50.0 30.2 31 .5 50.0 63.0
Surroaate 2-Fluorobiphenyl 2,4,6-Tribromophenol Terphenyl-d14
QC Limits 35.1 I 113.6 12.1 I 139.9 16.2 I 143.5
Units ug/L ug/L ug/L
Lab ID Result Target % Recovery Result Target % Recovery Result Target % Recovery
601571-MB 39.1 50.0 78.2 45.0 50.0 90.1 45.4 50.0
601572-LCS 40.6 50.0 81.2 56.9 50.0 114 46.3 50.0
601573-LCSD 36.2 50.0 72.4 48.4 50.0 96.9 47.5 50.0
1813795001 8.88 50.0 * 17.8 5.24 50.0 * 10.5 11 .5 50.0
1813735004 37.0 50.0 73.9 63.2 50.0 126 43.3 50.0
1813735005 35.2 50.0 70.4 59.0 50.0 118 36.5 50.0
1813735006 29.9 50.0 59.7 49.8 50.0 99.5 40.6 50.0
Co
The initial calibration did not pass method criteria for 3-nitroaniline, 4-nitroaniline, and carbazole. The CCV did not pass method criteria for
2,4-dimethylphenol, 4-chloroaniline, 3-nitroaniline, 2,4-dinitrophenol, and 4-nitroaniline. Any results for these compounds should be treated
as semi-quantitative.
The LCSD was outside of percent recovery QC limits for 3-nitroaniline and 2,4-dinitrophenol. RPO was outside of QC limits for 6
compounds.
Analyst Peer Review
/S/ David Teynor ISi Thomas J. Masoian
05/31/2018 11 :37 05/31/2018 14:57
RPO -Relative% Difference (Spike/ Spike Duplicate)
90.9
92.7
95.1
23.0
86.6
73.0
81.3
* -Analyte above reporting limit or outside of control limits
A-Sample result is greater than 4 times the spike added
•-Sample and Matrix Duplicate less than 5 times the reporting limit
•-Result is above the calibration range
ND -Not Detected (U -Qualifier also flags analyte as not detected)
NA -Not Applicable
# -The Matrix Spike, Matrix Spike duplicate or Matrix Duplicate is
reported for your information only. The sample matrix may be
inappropriate for the method selected.
QC results are not adjusted for moisture correction, where applicable
Page 5 of 11 Thursday, May 31, 2018 QCS V4.4
Analysis Information
Workorder: 1813735
Limits: Historical/Performance
Basis: ALS Laboratory Group
Blank
MB: 601389
Analyzed: 05/17/201810:11
Units: ug/L
Analyte
Dichlorodifluoromethane
Chloromethane
Vinyl chloride
Bromomethane
Chloroethane
Dichlorofluoromethane
Trichlorofluoromethane
Ethyl ether
1, 1-Dichloroethene
Freon 113
Acetone
lodomethane
Carbon disulfide
Methyl Acetate
Allyl chloride
Methylene chloride
trans-1,2-Dichloroethene
Methyl-t-butyl ether
cis-1 ,2-Dichloroethene
1, 1-Dichloroethane
2,2-Dichloropropane
2-Butanone
Ethyl acetate
Bromochloromethane
Tetrahydrofuran
Chloroform
1, 1, 1-Trichloroethane
Cyclohexane
1, 1-Dichloropropene
1,2-Dichloroethane
Carbon tetrachloride
Benzene
Trichloroethene
Methylcyclohexane
1,2-Dichloropropane
Dibromomethane
Bromodichloromethane
Page 6 of 11
Quality Control Sample
Batch Report
Preparation: NA
Batch: NA
Prepared By: NA
Result MDL RL
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 1.5 5.00
ND 0.3 1.00
ND 0.3 1.00
ND 1.5 5.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 1.6 5.00
ND 1.5 5.00
ND 0.3 1.00
ND 2.1 5.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
Thursday, May 31 , 2018
Analysis: SW 8260
Batch: EV0/7139 (HBN: 214983)
Analyzed By: Christopher Q. Coleman
QCS V4.4
Workorder: 1813735
Limits: Historical/Performance
Basis: ALS Laboratory Group
Blank
MB: 601389
Analyzed: 05/17/2018 10:11
Units: ug/L
Analyte
cis-1,3-Dichloropropene
4-Methyl-2-pentanone
trans-1 ,3-Dichloropropene
Ethyl methacrylate
1, 1,2-Trichloroethane
2-Hexanone
1,2-Dibromoethane
Toluene
1,3-Dichloropropane
Dibromochloromethane
Bromoform
Tetrachloroethene
1-Chlorohexane
Chlorobenzene
1, 1, 1,2-Tetrachloroethane
Ethyl benzene
m,p-Xylene
o-Xylene
Styrene
lsopropylbenzene
1, 1,2,2-Tetrachloroethane
Bromobenzene
1,2,3-Trichloropropane
trans-1,4-Dichloro-2-butene
Pentachloroethane
n-Propylbenzene
1,3,5-Trimethylbenzene
2-Chlorotoluene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
p-lsopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
Page 7 of 11
Quality Control Sample
Batch Report
Preparation: NA
Batch: NA
Prepared By: NA
Result MDL RL
ND 0.3 1.00
ND 1.5 5.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 1.5 5.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 2.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 1.5 5.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
ND 0.3 1.00
Thursday, May 31, 2018
Analysis: SW 8260
Batch: EV0/7139 (HBN: 214983)
Analyzed By: Christopher Q. Coleman
QCS V4.4
Analysis Information
Workorder: 1813735
Limits: Historical/Performance
Basis: ALS Laboratory Group
Blank
MB: 601389
Analyzed: 05/17/201810:11
Units: ug/L
Analyte
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
Hexachlorobutadiene
Naphthalene
1,2, 3-Trichlorobenzene
Control ••
LCS: 601390
Analyzed: 05/17/2018 09:22
Dilution: 1
Units: ug/L
Analyte
Dichlorodifluoromethane
Chloromethane
Vinyl chloride
Bromomethane
Chloroethane
Dichlorofluoromethane
Trichlorofluoromethane
Ethyl ether
1 , 1-Dichloroethene
Freon 113
Acetone
lodomethane
Carbon disulfide
Methyl Acetate
Allyl chloride
Methylene chloride
trans-1,2-Dichloroethene
Methyl-I-butyl ether
cis-1 ,2-Dichloroethene
1, 1-Dichloroethane
2,2-Dichloropropane
2-Butanone
Ethyl acetate
Bromochloromethane
Tetrahydrofuran
Chloroform
Page 8 of 11
Quality Control Sample
Batch Report
Preparation: NA
Batch: NA
Prepared By: NA
Result MDL
ND 1.5
ND 0.3
ND 0.3
ND 0.36
ND 0.3
Result Target
47.0 50.0
47.7 50.0
49.2 50.0
52.0 50.0
49.8 50.0
52.1 50.0
47.9 50.0
54.1 50.0
48.3 50.0
53.6 50.0
60.1 50.0
48.8 50.0
50.3 50.0
51.2 50.0
51 .7 50.0
49.0 50.0
49.4 50.0
50.7 50.0
49.2 50.0
49.1 50.0
50.4 50.0
59.9 50.0
59.9 50.0
47.9 50.0
47.6 50.0
48.9 50.0
RL
5.00
1.00
1.00
1.00
1.00
%Rec QC Limits
94.0 48.9 155.3
95.4 66.8 135.9
98.4 66.4 115.8
104 56.3 146.8
99.6 77.3 129.5
104 77.5 131.2
95.8 76.1 131.0
108 79.8 129.3
96.6 77.6 136.5
107 65.8 129.3
120 41 .9 164.4
97.6 50.1 154.9
101 72.3 127.8
102 42.7 147.1
103 74.5 134.7
98.0 75.9 127.6
98.8 73.5 130.0
101 79.6 127.4
98.4 73.5 126.3
98.3 73.2 120.9
101 66.5 143.6
120 51 .1 147.7
120 38.8 216.2
95.9 73.7 123.9
95.2 69.2 140.7
97.9 75.4 124.1
Thursday, May 31 , 2018
Analysis: SW 8260
Batch: EV0/7139 (HBN: 214983)
Analyzed By: Christopher Q. Coleman
QCS V4.4
~Is Info atlon
Workorder: 1813735
Limits: Historical/Performance
Basis: ALS Laboratory Group
II .L .Control ~
LCS: 601390
Analyzed: 05/17/2018 09:22
Dilution: 1
Units: uo/L
Analyte
1, 1, 1-Trichloroethane
Cyclohexane
1, 1-Dichloropropene
1,2-Dichloroethane
Carbon tetrachloride
Benzene
Trichloroethene
Methylcyclohexane
1,2-Dichloropropane
Dibromomethane
Bromodichloromethane
cis-1 ,3-Dichloropropene
4-Methyl-2-pentanone
trans-1,3-Dichloropropene
Ethyl methacrylate
1, 1,2-Trichloroethane
2-Hexanone
1,2-Dibromoethane
Toluene
1,3-Dichloropropane
Dibromochloromethane
Bromoform
Tetrachloroethene
1-Chlorohexane
Chlorobenzene
1, 1, 1,2-Tetrachloroethane
Ethylbenzene
m,p-Xylene
o-Xylene
Styrene
lsopropylbenzene
1, 1,2,2-Tetrachloroethane
Bromobenzene
1,2,3-Trichloropropane
trans-1,4-Dichloro-2-butene
Pentachloroethane
n-Propylbenzene
Page 9 of 11
Quality Control Sample
Batch Report
Preparation: NA
Batch: NA
Prepared By: NA
Result Target
48.3 50.0
53.7 50.0
50.3 50.0
49.9 50.0
47.7 50.0
49.6 50.0
48.1 50.0
50.6 50.0
51 .1 50.0
48.7 50.0
49.6 50.0
51 .4 50.0
56.8 50.0
47.7 50.0
51 .5 50.0
46.9 50.0
56.6 50.0
46.4 50.0
46.3 50.0
47.0 50.0
47.2 50.0
44.3 50.0
42.4 50.0
48.8 50.0
45.9 50.0
46.4 50.0
46.9 50.0
94.6 100
47.4 50.0
48.7 50.0
47.3 50.0
48.9 50.0
45.2 50.0
47.8 50.0
49.9 50.0
47.1 50.0
48.1 50.0
%Rec QC Limits
96.7 75.9 129.4
107 78.0 134.0
101 75.9 123.9
99.8 76.9 126.7
95.4 73.5 136.2
99.3 79.4 124.0
96.3 74.5 126.7
101 76.8 127.7
102 80.7 122.3
97.3 75.1 120.5
99.2 77.8 125.4
103 80.0 129.2
114 70.9 133.5
95.5 83.0 129.6
103 77.9 135.8
93.8 83.3 116.9
113 56.9 143.8
92.8 82.8 120.7
92.5 86.1 117.8
94.0 82.9 119.3
94.4 75.5 136.4
88.5 63.1 139.2
84.8 63.2 122.5
97.6 87.4 125.2
91 .8 86.5 113.3
92.8 81.3 130.8
93.9 88.4 117.0
94.6 88.4 116.9
94.8 86.5 116.1
97.5 89.1 121.1
94.6 86.8 118.9
97.7 77.8 128.9
90.3 81 .3 119.8
95.7 76.5 127.9
99.9 58.2 139.4
94.3 38.6 196.6
96.2 81 .3 125.5
Thursday, May 31 , 2018
Analysis: SW 8260
Batch: EV0/7139 (HBN: 214983)
Analyzed By: Christopher Q. Coleman
I
QCS V4.4
Analysis Information
Workorder: 1813735
Limits: Historical/Performance
Basis: ALS Laboratory Group
Control Sam le
LCS: 601390
Analyzed: 05/17/2018 09:22
Dilution: 1
Units: ua/L
Analyte
1,3,5-Trimethylbenzene
2-Chlorotoluene
4-Chlorotoluene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
p-lsopropyltoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
n-Butylbenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2,4-Trichlorobenzene
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Matrix SP-!ke • Matrix SDlke ~lcate
Sample: 1813516001
Analyzed: 05/17/2018 12:39
Dilution: 1
Units: ua/L
Analyte
Benzene
Toluene
Ethylbenzene
m,p-Xylene
o-Xylene
Surrnnata Recoveries
Quality Control Sample
Batch Report
Preparation: NA
Batch: NA
Prepared By: NA
Result Target
47.3 50.0
46.9 50.0
45.2 50.0
46.6 50.0
47.9 50.0
50.6 50.0
48.2 50.0
45.4 50.0
44.9 50.0
48.8 50.0
45.3 50.0
50.4 50.0
43.9 50.0
45.9 50.0
43.4 50.0
40.8 50.0
%Rec
94.7
93.8
90.3
93.3
95.7
101
96.4
90.8
89.9
97.6
90.6
101
87.7
91 .8
86.7
81 .7
MS: 601392
QC Limits
82.9 127.1
82.8 121 .6
83.1 120.9
80.5 130.5
81 .7 125.6
84.4 128.9
83.0 126.1
82.6 118.3
82.0 117.8
83.8 131.4
81.4 119.9
56.2 157.5
70.2 140.4
79.7 129.9
62.8 150.8
71 .8 138.2
Analyzed: 05/17/2018 14:50
Dilution: 1
Units: ua/L
Analysis: SW 8260
Batch: EV0/7139 (HBN: 214983)
Analyzed By: Christopher Q. Coleman
MSD: 601393
Analyzed: 05/17/2018 15:06
Dilution: 1
Units: ua/L
Result Result Target %Rec QC Limits Result % Rec RPD QC Limits
ND 55.8 50 112 79.4 124.0 51 102 9.01 0.0 20.0
ND 51 .3 50 103 86.1 117.8 46.7 93.4 9.36 0.0 20.0
ND 51.4 50 103 88.4 117.0 46.7 93.5 9.5 0.0 20.0
ND 103 100 103 88.4 116.9 94.1 94.1 9.22 0.0 20.0
ND 51.4 50 103 86.5 116.1 47.2 94.4 8.61 0.0 20.0
.
Surrogate 1,2-Dichloroethane-d4 Toluene-dB 4-Bromofluorobenzene
QC Limits 72.2 I 123.4 77.5 I 115.4 78.5 I 121.6
Units ug/L ug/L ug/L
Lab ID Result Target % Recovery Result Target o/o Recovery Result Target % Recovery
601390-LCS 51 .7 50.0 103 48.8 50.0 97.6 51.4 50.0 103
601389-MB 48.3 50.0 96.7 51 .5 50.0 103 53.1 50.0 106
1813642004-TRIPB 50.9 50.0 102 50.6 50.0 101 52.7 50.0 105
1813516001 48.8 50.0 97.7 51 .0 50.0 102 53.1 50.0 106
Page 10 of 11 Thursday, May 31 , 2018 QCS V4.4
Analysis lnform~tion
VVorkorder: 1813735
Limits: Historical/Performance
Basis: ALS Laboratory Group
Sunoaa11a Recoverlea
Quality Control Sample
Batch Report
Preparation: NA
Batch: NA
Prepared By: NA
Surroaate 1,2-Dichloroethane-d4 Toluene-dB
QC Limits 72.2 I 123.4 77.5 I 116.4
Units ug/L ug/L
Analysis: SW 8260
Batch: EV0/7139 (HBN: 214983)
Analyzed By: Christopher Q. Coleman
4-Bromofluorobenzene
78.5 I 121 .6
ug/L
Lab ID Result Target % Recovery Result Target % Recovery Result Target % Recovery
1813642001 50.0 50.0 99.9 51.0 50.0 102 52.3 50.0 105
1813642002 49.2 50.0 98.4 50.7 50.0 101 52.5 50.0 105
1813642003 49.2 50.0 98.3 50.9 50.0 102 52.6 50.0 105
1813735001 51.8 50.0 104 50.1 50.0 100 53.1 50.0 106
1813735003 51.0 50.0 102 50.5 50.0 101 53.3 50.0 107
1813735002 51 .7 50.0 103 50.5 50.0 101 51 .8 50.0 104
601392-MS 51 .2 50.0 102 48.6 50.0 97.2 51.9 50.0 104
601393-MSD 51.4 50.0 103 48.5 50.0 97.0 51 .9 50.0 104
8260 QC Comments: The percent difference (or percent drift for a regression fit) for target compounds in the CVS standard must generally
be less than 20% relative to the average response from the initial calibration curve. The analyte acetone did not meet this criteria and
results for this compound should be considered estimates.
Analyst
/S/ Christopher Q. Coleman
05/18/201811:21
S bola and Definitions
a C
Peer Review
ISi Thomas J. Masoian
05/22/2018 08:32
* -Analyte above reporting limit or outside of control limits
A-Sample result is greater than 4 times the spike added
•-Sample and Matrix Duplicate less than 5 times the reporting limit
•-Result is above the calibration range
# -The Matrix Spike, Matrix Spike duplicate or Matrix Duplicate is
reported for your information only. The sample matrix may be
inappropriate for the method selected.
) _______ _
RPD -Relative% Difference (Spike/ Spike Duplicate)
ND -Not Detected (U -Qualifier also flags analyte as not detected)
NA -Not Applicable
QC results are not adjusted for moisture correction, where applicable
Page 11 of 11 Thursday, May 31, 2018 QCS V4.4