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HomeMy WebLinkAboutDSHW-2018-004591 - 0901a0688082616etrr4 Senior Geologist - ( Jtilie Kilgore, President Environmental Manager Div of Waste Management and Radiation Control MAY2_1_2018 WASATCH ENVIRONMENTAL, INC. ENVIRONMENTAL SCIENCE AND ENGINEERING Lt-r-CA- op13 Psi-m-zpto- 00 459 f SAMPLING AND ANALYSIS PLAN IMPLEMENTATION REPORT PARK EAST APARTMENTS 1717 EAST MURRAY-HOLLIDAY ROAD MILLCREEK, UTAH PROJECT NO. 2276-001A PREPARED FOR: MR. SCOTT T. ANDERSON UTAH DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WASTE MANAGEMENT AND RADIATION CONTROL 195 NORTH 1950 WEST, 2ND FLOOR P.O. BOX 144880 SALT LAKE CITY, UTAH 84114-4880 PREPARED BY: WASATCH ENVIRONMENTAL, INC. 2410 WEST CALIFORNIA AVE SALT LAKE CITY, UTAH 84104 PHONE: 801-972-8400 FAX: 801-972-8459 MAY 9, 2018 2410 WEST CALIFORNIA AVENUE SALT LAKE CITY, UTAH 84104 PHONE (801) 972-8400 FAX (801) 972-8459 wei@wasatch-environmental com www. wasatch-environmentatcom Sampling and Analysis Plan Implementation Report Park East Apartments TABLE OF CONTENTS Section Page No. 1. INTRODUCTION 2 2. BACKGROUND 2 3. OBJECTIVE 3 4. SITE INVESTIGATION ACTIVITIES 3 5. METHODOLOGY 3 Indoor Air Sampling 3 Sub-Slab Soil Vapor Sampling 4 6. RESULTS 4 7. DISCUSSION 5 FIGURES Figure 1 — Sample Location Map TABLES Table 1 — Indoor Air Analytical Results Table 2 — Sub Slab Vapor Analytical Results Table 3 — Groundwater Analytical Results Table 4 — Soil Gas Analytical Results APPENDICES Appendix A — Indoor Air Sample Analytical Report Appendix B — Sub Slab Vapor Analytical Report Appendix C — U.S. EPA Memorandum on Removal of the trans-1,2-dichloroethylene Provisional Peer Reviewed Toxicity Value Wasatch Environmental, inc. Page 1 Sampling and Analysis Plan Implementation Report Park East Apartments SAMPLING AND ANALYSIS PLAN IMPLEMENTATION REPORT PARK EAST APARTMENTS 1717 EAST MURRAY HOLLADAY ROAD MILLCREEK, UTAH 1. INTRODUCTION Wasatch Environmental, Inc., (Wasatch) has completed investigation activities at the Park East Apartments. The investigation activities were described in a Sampling and Analysis Plan (SAP), dated March 30, 2018, which was submitted to and approved by the Utah Division of Waste Management and Radiation Control (DWMRC) on April 19, 2018. The scope of work included the collection of five 24-hour indoor air samples and the collection of four sub slab soil vapor samples. 2. BACKGROUND In the Fall of 2017, a lender had a Phase I Environmental Site Assessment completed for the subject property, which identified the presence of a former dry-cleaning facility on the east adjoining property. The lender requested that K & H Development, LLC, the owners of the Park East Apartments, conduct a Limited Site Investigation to investigate if impacts from the former dry cleaner are present on the Park East Property. Wasatch conducted a limited subsurface investigation, which included: 1. advancing four soil borings 2. the collection and laboratory analysis of groundwater samples, and 3. the installation, sampling, and laboratory analysis of six soil gas samples. The results of the investigation were summarized in a Soil Gas and Groundwater Sampling Report, dated December 13, 2017. The report indicates that a release of volatile organic compounds (VOCs) from the east-adjoining dry-cleaning facility has impacted a portion of the groundwater at the Park East Apartments property. The groundwater analytical results were compared to the U.S. Environmental Protection Agency (EPA) Vapor Intrusion Screening Levels (VISL) for residential properties, which indicated that there was a potential for trichloroethene (TCE) and vinyl chloride to be present in indoor air at a concentration greater that the U.S. EPA Regional Screening Level (RSL) for indoor air. Results of soil gas sampling indicated the presence of dry-cleaning related solvents in the soil gas in the areas sampled. However, all the reported concentrations in samples SV-1, SV-2, and SV-3 (see Figure 1) were either below the laboratory reporting limits, or below U.S. EPA Target Sub-Slab and Exterior Soil Gas Concentrations. All reported concentrations in sample SV-4, collected 45 feet southeast of Building C, were either below the laboratory reporting limits, or below U.S. EPA Target Sub-Slab and Exterior Soil Gas Concentrations with the exception of vinyl chloride, which was detected above the Target Sub-Slab and Exterior Soil Gas Concentration of 5.6 micrograms per cubic meter (ug/m3). Additional soil gas samples SV-5 and SV-6, which were collected adjacent to the east and west of Building C did not contain vinyl chloride or other compounds of concern above the U.S. EPA Target Sub-Slab and Exterior Soil Gas Concentrations. Wasatch provided a copy of the Soil Gas and Groundwater Sampling Investigation report, to DWMRC for review and guidance for the steps necessary to receive site closure. DWMRC's reply to K & H Development, dated December 20, 2017, states the following: "To further evaluate the vapor intrusion risk to residents of the apartments (A, B, and C), the Division recommends Wasatch Environmental submit a work plan for review and approval that Wasatch Environmental, inc. Page 2 Sampling and Analysis Plan Implementation Report Park East Apartments details efforts to conduct indoor air monitoring of the apartment buildings. The data collected will help in determining if there is a VI [vapor intrusion] risk at the property that requires mitigation." The approved SAP described additional data collection activities proposed to evaluate if there is a VI risk at the property. 3. OBJECTIVE The objectives of this investigation were to: • Evaluate the sub-slab soil gas and indoor air for VOCs related to dry-cleaning solvents and their daughter degradation compounds, and • Evaluate the vapor intrusion pathway for Buildings B and C. 4. SITE INVESTIGATION ACTIVITIES The sample locations (Figure 1) are based on advice from the risk assessor, Ms. Paige Walton, who suggested sampling at the north portion of Building B and South portion of Building C after review of the groundwater and soil vapor results from the previous investigation. On March 13, 2018, prior to submittal of the SAP, Wasatch collect a 24-hour indoor air sample from Apartment B-101. Apartment B-101 was a ground level apartment which was never occupied but had tenants ready to occupy the apartment. Prior to written SAP approval, but with verbal approval from DWMRC, on April 9, 2018, Wasatch collected 24-hour indoor air samples at one location in a ground level common hallway in Building B and at two ground level hallway locations in Building C. For quality assurance/quality control, a background sample was also collected from a fourth-floor outside balcony. On April 18, 2018, Wasatch collected a 24-hour indoor air sample from recently vacated ground level Apartment C-106, prior to cleaning and painting in advance of a new tenant. The indoor air sampling methodology is described in Section 5. On April 27, 2018, Wasatch collect four sub slab soil vapor samples. Sample SS-1 was collected in the northern portion of Building B in a utility closet containing HVAC and a water heater for an adjoining apartment, sample SS-2 was collected in the garage located at the northeast corner of Building B, sample SS-3 was collected from a utility closet at the southern portion of Building C, and sample SS-4 was collected in the garage located at the southeast corner of Building C. The sub slab sampling methodology is described in Section 5. 5. METHODOLOGY Indoor Air Sampling Wasatch placed 6-liter Summa canisters with a 24-hour flow restrictor attached to each sampling canister at an inlet height of approximately 2 feet. The initial vacuum reading was checked and recorded, and the samples were collected for approximately 24 hours. The following day, the final vacuum reading was checked and recorded, the sample canisters closed, the flow restrictor removed, and a brass cap tightened to the inlet of the sample canister. Canisters were labeled with the appropriate sample location, as well as initial and final vacuum readings. The canisters were hand delivered under chain-of-custody protocol to ALS Laboratories, a Utah-certified laboratory, Salt Lake City, Utah, for the analysis of the following VOCs of concern using U.S. EPA Method TO-15 selective ion monitoring (SIM): Wasatch Environmental, inc. Page 3 Sampling and Analysis Plan Implementation Report Park East Apartments • Tetrachloroethene (PCE) • Trichloroethene (TCE) • trans-1,2-Dichloroethene • cis-1,2-Dichloroethene • 1,1-Dichloroethene • Vinyl Chloride Sub-Slab Soil Vapor Sampling To collect sub-slab soil vapor samples, Wasatch drilled a %-inch hole through the concrete slab at each sample location using a percussion hammer drill. A soil vapor pin with a silicon sleeve was inserted into the hole and allowed to set up for approximately 30 minutes. A sample manifold with a flow restrictor was attached to a laboratory supplied 1-liter Summa canister and the initial vacuum in the canister recorded. Wasatch personnel attached the Summa canister to the vapor pin using new Teflon tubing. The vacuum gauge on the flow restrictor was monitored, with decreasing vacuum pressure indicating that soil gas was being collected into the sample canister. Samples were collected for approximately 10 minutes. The sample canister was closed, and a brass cap tightened to the inlet of the sample canister. During sample collection, an isopropyl alcohol swab was placed near the canister to evaluate for leaks. At the conclusion of sampling, the vapor pins were removed, and the holes filled and finished with concrete. The sub-slab soil vapor samples were submitted under chain-of-custody to ESC Laboratory, Mt. Juliet, Tennessee, for VOC analysis using EPA Method TO-15. The samples were analyzed for the contaminants of concern: PCE, TCE, cis-1,2-dichloroethene, trans-1,2-dichloroethene, 1,1- dichloroethene, and vinyl chloride. 6. RESULTS The analytical results of indoor air sampling are summarized in Table 1. For comparison, the U.S. EPA RSLs for indoor residential air are also shown. As shown on Table 1 the sample results did not exhibit any constituents above the laboratory reporting limits or the U.S. EPA Regional Screening Levels (RSLs) for indoor residential air except for trans-1,2-dichloroethene, which was reported at concentrations between 7.0 micrograms per cubic meter (ug/m3) and 74 ug/m3. The background sample contained trans-1,2-dichloroethene at a concentration of 0.71 ug/m3. There is no U.S. EPA RSL established for trans-1,2-dichloroethene. Copies of the indoor air analytical laboratory report is presented in Appendix A. The analytical results of the sub slab vapor sampling are summarized in Table 2. For comparison the U.S. EPA Target Sub Slab and Exterior Soil Gas Concentrations are shown. The U.S. EPA Target Sub Slab and Exterior Soil Gas Concentrations include a sub slab attenuation factor of approximately 0.33. As shown on Table 2 the sample results did not exhibit any constituents above the laboratory reporting limits for TCE, cis 1,2-dichloroethene, or 1,1-dichloroethene. PCE was reported above laboratory reporting limits in both garage locations (SS-2 and SS-4) but at concentrations well below the U.S. EPA Target Sub Slab and Exterior Soil Gas Concentration for PCE of 360 ug/m3. Vinyl chloride was identified in one sub slag sample SS-3 at a concentration of 3.65 ug/m3, which is below the U.S. EPA Target Sub Slab and Exterior Soil Gas Concentration for vinyl chloride of 5.6 ug/m3. Trans-1,2-dichloroethene was identified in all of the sub slab sample results at concentrations ranging from 6.64 ug/m3 to 474 ug/m3. There is no U.S. EPA RSL or U.S. EPA Target Sub Slab and Exterior Soil Gas Concentration established for trans-1,2-dichloroethene. A copy of the sub slab analytical laboratory report is presented in Appendix B. Wasatch Environmental, Inc. Page 4 Sampling and Analysis Plan Implementation Report Park East Apartments 7. DISCUSSION Based on the groundwater analytical results from the December 2017 sampling investigation (Table 3), the conservative VISL lookup values predicted a potential for vapor intrusion of TCE and vinyl chloride. Based on the soil vapor sample collected at SV-4, the U.S. EPA Target Sub Slab and Exterior Soil Gas Concentration lookup values predicted a vapor intrusion potential for vinyl chloride. Neither TCE nor vinyl chloride were identified above laboratory reporting limits in the indoor air samples. PCE and vinyl chloride were identified in sub slab vapor samples, however the concentrations were below the established U.S. EPA Target Sub Slab and Exterior Soil Gas Concentrations for PCE and vinyl chloride. Because the identified concentration of PCE and vinyl chloride are low compared to the target concentrations, cumulative exposure from PCE and vinyl chloride would not result in excess risk. No PCE was identified above laboratory reporting limit in the indoor air samples. Trans-1,2-dichloroethene was identified in every indoor air sample and sub slab vapor sample, including the background air sample collected from an outside fourth floor balcony. As previously discussed, there is not an established U.S. EPA RSL or U.S. EPA Target Sub Slab and Exterior Soil Gas Concentration established for trans-1,2-dichloroethene. A memorandum from the U. S. EPA director of Superfund Health Risk Technical Support Center, dated June 17, 2014, discussing the derivation of an initial reference concentration for trans-1,2-dichloroethylene (also known as trans-1,2-dichloroethene) suggests that later studies refute the initial derived chronic reference dose as no adverse health impacts were observed at exposure concentrations 20-fold higher. The later studies were the justification in removing a toxicity value for trans-1,2-dichloroethene. A copy of the memorandum is attached in Appendix C. There are no acceptable surrogate chemicals to assess inhalation toxicity for trans-1,2-dichloroethene (or cis- 1,2-dichloroethene) but these compounds are not believed to be toxic via inhalation. Based on the results of indoor air and sub slab vapor sampling, we found no concentrations of indoor vapors above established U.S. EPA guidance which would require mitigation. Trans-1,2-dichloroethene, which was the only chemical identified above laboratory reporting limits in the indoor air samples, appears low and well below concentrations of concern. It is Wasatch's opinion based on available data that the groundwater impacts on the property do not present a potential for vapor intrusion impact to residents at the Park East Apartments. Wasatch Environmental, inc. Page 5 tl iska [44.---- maiftaa '.1101 • +' . 111417 mil Mil II 11111 sr. asw gm Former Location of Dry Cleanqr, eta O Sub-Slab Sample Location *Indoor Air Sample Location 0 Boring Location LI Sub-Surface Soil Gas Sample Location Sample Location Map Figure 1 PARK EAST APARTMENTS WE12276-001A 404,WASATCH .VMONNItliTatt The use or reuse of this information is restricted to the referenced document unless otherwise authorized. Wasatch Environmental Copyright 2006 Table 1 indoor Air Results Park East Apartments 1709 E. Murray Holladay Road Millcreek, Utah (all concentrations are expressed in micrograms per cubic meter htg/m31) Sampling Location Te tr a c hl o r oe the n e ( PCE ) CD C C) .0 t'D 2 o .c o •r: 1- cis - 1, 2- Di c hl o r o e the n e tr a ns - 1, 2- Di c hlo r o e the ne 1, 1- Di c hl o ro ethe n e Vin y l c hl o rid e Apart-B 101 <0.34 <0.27 <0.20 74 <0.20 <0.13 Building B Common Area <0.34 <0.27 <0.20 7.0 <0.20 <0.13 Building C North <0.34 <0.27 <0.20 26 <0.20 <0.13 Apart C 106 <0.34 <0.27 <0.20 42 <0.20 <0.13 Building C South <0.34 <0.27 <0.20 33 <0.20 <0.13 Background Sample <0.34 <0.27 <0.20 0.71 <0.20 <0.13 U.S. EPA Regional Screening Levels for Residential indoor Air 11 0.48 NE NE 210 0.17 NOTES: < = concentration was below the laboratory reporting limit NE = not established Table 2 Sub Slab Vapor Analytical Results Park East Apartments 1709 E. Murray Holladay Road Millcreek, Utah (all concentrations are expressed in micrograms per cubic meter hig/m31) Sampling Location Te tr a chl o r o e the n e ( PCE ) Tr ic hlo r o e the n e cis 1 , 2- Di c hl o r o ethe n e tr a ns - 1, 2- Di c hl o ro e the n e 1, 1- Di c hl o ro e the ne Vi n y l c hl o r id e SS-1 <2.72 <2.14 <1.59 6.34 <2.14 <1.59 SS-2 4.37 <2.14 <1.59 48.5 <2.14 <1.59 SS-3 <2.72 <2.14 <1.59 81.6 <2.14 3.65 SS-4 9.04 <2.14 <1.59 474 <2.14 <1.59 U.S. EPA Target Sub-Slab and Exterior Soil Gas Concentration 360 16 NE NE 7,000 5.6 NOTES: < = concentration was below the laboratory reporting limit NE = not established Table 3 Groundwater Analytical Results Park East Apartments 1709 E. Murray Holladay Road Millcreek, Utah all concentrations are expressed in micrograms per liter (pg/L) Sampling Location Sampling Date Te tr a c hlo ro e the n e ( PC E ) Tr ic hl o r o e the n e cis - 1, 2- Dic hl o ro e the ne tr a n s - 1, 2- Di c hlo ro e the ne 1, 1- Di c hl o r o e the n e Vin y l C h l o rid e GP-1 GW 11/29/2017 <0.262 0.390 0.520 <0.828 <0.263 <0.265 GP-2 GW 11/29/2017 1 9.05 99.8 2.67 <0.263 0.860 GP-3 GW 11/29/2017 1.3 9.50 62.9 2.37 <0.263 1.23 GP-4 GW 11/29/2017 2.48 9.72 54.0 2.12 <0.263 0.9 VISL Target Groundwater Concentrations-Residential 15 1.2 NE NE 200 0.15 U.S. EPA Maximum Contaminant Level 5 5 70 100 7 2 NOTES: < = concentration was below the method detection limit BOLD = Results reported above U.S. EPA MCL Table 4 Soil Gas Analytical Results Park East Apartments 1709 E. Murray Holladay Road Millcreek, Utah (all concentrations are expressed in micrograms per cubic meter [p.g/m3]) Sampling Location Te tr a c hl o ro e the n e ( PC E ) Tr ic hlo r oe the n e cis 1 , 2- Di c hl o r o e the n e tr a ns - 1, 2- Di c hlo ro e the ne 1, 1- Di c hl o r o e the n e Vi n y l c hl o rid e SV-1 3.14 <2.14 <1.59 <1.59 <1.59 <1.02 SV-2 2.88 <2.14 <1.59 <1.59 <1.59 <1.02 SV-3 13.2 <2.14 <1.59 <1.59 <1.59 <1.02 SV-4 <2.72 <2.14 38.6 5.43 <1.59 15.3 SV-5 11.9 <2.14 3.14 <1.59 <1.59 1.16 SV-6 6.77 <2.14 <1.59 <1.59 <1.59 <1.02 U.S. EPA Regional Screening Levels for Residential indoor Air 11 0.48 NE NE 210 0.17 U.S. EPA Target Sub-Slab and Exterior Soil Gas Concentration 360 16 NE NE 7,000 5.6 NOTES: < = concentration was below the laboratory reporting limit NE = not established ANALYTICAL REPORT Report Date: March 21, 2018 Chris Nolan Wasatch Environmental, Inc. 2410 West California Ave Salt Lake City, UT 84104 Phone: (801) 972-8400 E-mail: cn@wasatch-environmental.com Workorder: Project ID: Purchase Order: Project Manager -de‘iiie?bd 03/14/18 34-1807463 ÎlelD `Lab I APT B101 1807463001 *Ct'Poce. 03/13/18 K + H Development 031318 K + H Development Jessica Helland ;Saiitling Si e 7;..v K + H Development ADDRESS 960 West LeVoy Drive, Salt Lake City, Utah, 841 23 USA I PHONE +1 801 266 7700 I FAX +1 801 268 9992 ALS GROUP USA, CORP. An ALS Limited Company www.alsglobaLcom RIGHT soLuTions I T I Page 1 of 3 Wed, 03/21/18 12:55 PM ENVREP-V4.8 ANALYTICAL REPORT Workorder: 34-1807463 Client: Wasatch Environmental, Inc. Project Manager: Jessica Helland Analytical Results Sample ID: APT B101 Lab ID: 1807463001 Matrix. Air Sampling Site: K + H Development Media: Summa 6 Liter Canister Sampling Parameter. NA Collected: 03/13/2018 Received: 03/14/2018 Analysis Method - EPA TO-1 5 SIM Preparation: Mit Applicable r Analysis: EPA TO-15 SIM, Air Batch: IVOA/3919 (HBN: 210828) Analyzed: 03/20/2018 16:45 Instrument ID: 5975-L Percent Solid: NA Report Basis: Wet '-, ' - 'Y' i- AnaiytP :',-,, ... ..10:0-.(ppl?) • ... -,-h , .. e ResUlt .' ughpl) • RL (ppb) ., " ;_tiaiiution„. 4 . . > E.: Vinyl chloride ND <0.13 0 050 1 1,1-Dichloroethene ND <0.20 0.050 1 cis-1,2-Dichloroethene ND <0.20 0 050 1 Trichloroethene ND <0.27 0 050 1 Tetrachloroethene ND <0.34 0.050 1 Analysis MOW - EPA TO-15 SIM Preparation: Not Applicable Analysis: EPA TO-15 SIM, Air Batch: IVOA/3919 (HBN: 210828) Analyzed: 03/20/2018 17:30 . Instrument ID: 5975-L Perceni Solid: NA Report Basis: Wet ;., .., . 1, - A „Result (ppb) , Result-, cug/nV- RL (ppb) 2.:4Pilution „ _ . ua -. trans-1,2-Dichloroethene 19 74 0 50 10 E Report Authorization (/S/ is an electronic signature that complies with 21 CFR Part 11) Method Analyst Peer Review EPA TO-15 SIM /S/ Lisa M. Reid 03/21/2018 11:51 /S/ Thomas J. Masoian 03/21/2018 12:52 Laboratory Contact Information ALS Environmental Phone: (801) 266-7700 960 W Levoy Drive Email. alslt.lab@ALSGlobal.com Salt Lake City, Utah 84123 Web: www.alsslc.com Page 2 of 3 Wed, 03/21/18 12.55 PM ENVREP-V4.8 ANALYTICAL REPORT Workorder: 34-1807463 Client: Wasatch Environmental, Inc. Project Manager: Jessica HeIland General Lab Comments The results provided in this report relate only to the items tested. Samples were received in acceptable condition unless otherwise noted. Samples have not been blank corrected unless otherwise noted. This test report shall not be reproduced, except in full, without written approval of ALS. ALS provides professional analytical services for all samples submitted ALS is not in a position to interpret the data and assumes no responsibility for the quality of the samples submitted. All quality control samples processed with the samples in this report yielded acceptable results unless otherwise noted. ALS is accredited for specific fields of testing (scopes) in the following testing sectors. The quality system implemented at ALS conforms to accreditation requirements and is applied to all analytical testing performed by ALS. The following table lists testing sector, accreditation body, accreditation number and website. Please contact these accrediting bodies or your ALS project manager for the current scope of accreditation that applies to your analytical testing. Testing Sector Accreditation Body Certificate Website Number Environmental PJLA (DoD ELAP) Utah (TNI) Nevada Oklahoma Iowa Result Symbol Definitions MDL = Method Detection Limit, a statistical estimate of method/media/instrument sensitivity. RL = Reporting Limit, a verified value of method/media/instrument sensitivity. CRDL = Contract Required Detection Limit Reg Limit = Regulatory Limit. ND = Not Detected, testing result not detected above the MDL or RL. < This testing result is less than the numerical value. ** No result could be reported, see sample comments for details. Qualifier Symbol Definitions U = Qualifier indicates that the analyte was not detected above the MDL. J = Qualifier Indicates that the analyte value is between the MDL and the RL. It is also used to indicate an estimated value for tentatively identified compounds in mass spectrometry where a 1 1 response is assumed. B = Qualifier indicates that the analyte was detected in the blank E = Qualifier indicates that the analyte result exceeds calibration range. P = Qualifier indicates that the RPD between the two columns is greater than 40%. Page 3 of 3 Wed, 03/21/18 12.55 PM ENVREP-V4.8 ANALYTICAL REPORT Report Date: April 17, 2018 Chris Nolan Wasatch Environmental, Inc. 2410 West California Ave Salt Lake City, UT 84104 Phone: (801) 972-8400 E-mail: cn@wasatch-environmental.com Workorder: 34-1810211 Project ID: Indoor Air Sampling Purchase Order: Indoor Sampling Project Manager Jessica Helland • i'.4iiAlfia'ae ID 'MY ID ÌÌtDaté eceivéDai Špíing ife Building 6-Common 1810211001 NA 04/11/18 Indoor Sampling Building C-South 1810211002 NA 04/11/18 Indoor Sampling Building C-North 1810211003 NA 04/11/18 Indoor Sampling Background 1810211004 NA 04/11/18 Indoor Sampling ADDRESS 960 West LeVoy Drive, Salt Lake City, Utah, 841 23 USA PHONE +1 801 266 7700 FAX +1 801 268 9992 ALS GROUP USA, CORP. An ALS Limited Company www.alsglobalcom RIOHT SOLUTICHIS Page 1 of 5 Tue, 04/17/18 2.55 PM ENVREP-V4.8 ANALYTICAL REPORT Workorder: 34-1810211 Client: Wasatch Environmental, Inc. Project Manager: Jessica Helland Analytical Results Sample ID: Building B-Common Lab ID: 1810211001 Matrix: Air Sampling Site: Indoor Sampling Media. Summa 6 Liter Canister Sampling Parameter. NA Received: 04/11/2018 AnalysisiMeIhrtd - EPA TO-15 SIM Preparation: Not Applicable • AnalySia: EPA TO-15 SIM, Air Batch: IV0A/3956 (HBN: 212799) Analyzed: 04/12/2018 15:12 Instrument ID: 5975-L Percent Solid: NA Report Basis: Wet -t• ,.: Analyte ,_ ':f suit (pp.13)-,,, 1R.6$174 s', ;‘, 6i61m3 "RL2ipph - 'Oilution: .: ' .: 74„ „upt. , '‘ - • :2 Vinyl chloride ND <0.13 0 050 1 1,1-Dichloroethene ND <0 20 0.050 1 cis-1,2-Dichloroethene ND <0 20 0.050 1 Tnchloroethene ND <0.27 0 050 1 Tetrachloroethene ND <0.34 0 050 1 APalysiS Method - EPA TO,15 SIM Preparation: Not Applicable Analysis: EPA TO-15 SIM, Air Batch: IV0N3956 (HBN: 212799) Analyzed: 04/13/2018 13:30 Instrument ID: 5975-L Percent Sad: NA Report Basis: Wet -v- t 2.- Alla! ' „ ' ...... -. :tac,•;•Reult (pph) ,!„ -.: „ ReSult . ‘, , „ (pg/tn3) ' '..)3.1_ (ppb)',›, Pilutiok„.•; . ' - ',;F'• up! "" 4 •;! trans-1,2-Dichloroethene 1.8 7.0 0.50 10 Sample ID: Building C-South Lab ID: 1810211002 Matrix: Air Sampling Site: Indoor Sampling Media: Summa 6 Liter Canister Sampling Parameter: NA Received: 04/11/2018 AnalieiS-Method , EPA TO-15 SIM w....-• Thele Preparation; Not Applicable Analysis: EPA TO-15 SIM, Air Batch: IVOA/3956 (1-IBN: 212799) Analyzed: 04/12/2018 16:01 Instrument ID: 5975-L Percent Solid: NA Report Basis: Wet . ,; .1,_ , , • 4`""-" ' ---'- . Appl e , _ .,,=•.,.,,, • — ,? esutt (ppb) Rettilt e • •-,. ; 4 (P0,11113) y., 4;:ftl- (ppb) •, ,Pilptiop,,,, . ,6.. . _ •ipz • ' uW,, i:,. Vinyl chloride ND <0.13 0.050 1 1,1-Dichloroethene ND <0.20 0.050 1 cis-1,2-Dichloroethene ND <0 20 0.050 1 Trichloroethene ND <0.27 0.050 1 Tetrachloroethene ND <0.34 0.050 1 Analysis MethAd - EPA TO-15 SIM Preparation: Not Applicable • Analysis: EPA TO-15 SIM, Air Batch: IVOA/3956 (HBN: 212799) Analyzed: 04/13/2018 14:17 Instrument ID: 5975-L Percent Solid: NA Report Basis: Wet — • . lq 4PaNte ' , ii At.). ,-,,,, Etw4(0104) '‘ .- :3 - Result .. (ug4r0 ;. .. L (ppb) = Outipp ' , , mit , ,, trans-1,2-Dichloroethene 8.3 33 0 50 10 Page 2 of 5 Tue, 04/17/18 255 PM ENVREP-V4 8 ANALYTICAL REPORT Workorder: 34-1810211 Client: Wasatch Environmental, Inc. Project Manager: Jessica Helland Analytical Results Sample ID: Building C-North Lab ID: 1810211003 Matrix: Air Sampling Site. Indoor sampling Media: Summa 6 Liter Canister Sampling Parameter: NA Received: 04/11/2018 Analysis Method - EPA TO-15 SIM la, Preparation: Not Applicable • Analysis: EPA TO-15 SIM, Air Batch: IVOA/3956 (HBN: 212799) Analyzed: 04/12/2018 16:51 • instrument ID: 5975-L • Percent Solid: NA •Report Basis: Wet I. . Anal e ,•,i '‘. , -1142 :1011:.7,11 'Iv ,,, -'.5,4454: V Result • esult,(ppb) k- (ug/M3 RL (01)) Dilytipli• - , - '-:- u.A , Vinyl chloride ND <0.13 0.050 1 1,1-Dichloroethene ND <0.20 0.050 1 cis-1,2-Dichloroethene ND <0.20 0.050 1 Trichloroethene ND <0.27 0.050 1 Tetrachloroethene ND <0.34 0.050 1 Analysis Methp,d - EPA TO-15 SIM •Preparation: Not Applicable , Analysis: EPA TO-15 SIM, Air Batch: IVOA/3956 (HBN. 212799) Analyzed: 04/13/2018 15:03 Instrument ID: 5975-L , Percent Solid: niA RePort Basis: Wet ,Aftalyto - . „,• „ , • . ? . : , "Ik*U4';- " ' '; osult•(ppb) • -,,(uglni , - ,R,L (ppb) 9i1,utiori ,., 1,'' ua t )x. trans-1,2-Dichloroethene 6.6 26 0 50 10 Sample ID: Background Lab ID: 1810211004 Matrix: Air Sampling Site: Indoor Sampling Media: Summa 6 Liter Canister Sampling Parameter: NA Received: 04/11/2018 Analysts Metlipd -EPA TO-15 SIM Preparation: Not Applicable • Analysis: EPA TO-15 SIM, Air Batch: IVOA/3956 (HBN: 212799) Analyzed: 04/12/2018 17:41 Instrument ID: 5975-L Percent Solid: NA Report Bašis: Wet - p - Anal e v. .., •, , ' ." esultIpp4) - '' ' FkO„Oit '' (ug/tn!) , , 12L. (Nib) ',4: Ditutiop .., 0013 Vinyl chloride ND <0.13 0.050 1 1,1-Dichloroethene ND <0.20 0.050 1 trans-1,2-Dichloroethene 0.18 0.71 0.050 1 cis-1,2-Dichloroethene ND <0.20 0.050 1 Trichloroethene ND <0.27 0 050 1 Tetrachloroethene ND <0.34 0.050 1 Report Authorization (lS/ is an electronic signature that complies with 21 CFR Part 11) Method Analffit Peer Review EPA TO-15 SIM /S/ Lisa M. Reid 04/16/2018 15:02 /S/ Benson Boy 04/17/2018 14:48 Page 3 of 5 Tue, 04/17/18 2 55 PM ENVREP-V4 8 ANALYTICAL REPORT Workorder: 34-1810211 Client: Wasatch Environmental, lnc. Project Manager: Jessica Helland Laboratory Contact Information ALS Environmental Phone: (801) 266-7700 960 W Levoy Drive Email alslt lab@ALSGlobal.com Salt Lake City, Utah 84123 Web: www.alsslc.com General Lab Comments The results provided in this report relate only to the items tested. Samples were received in acceptable condition unless otherwise noted Samples have not been blank corrected unless otherwise noted. This test report shall not be reproduced, except in full, without written approval of ALS ALS provides professional analytical services for all samples submitted. ALS is not in a position to interpret the data and assumes no responsibility for the quality of the samples submitted. All quality control samples processed with the samples in this report yielded acceptable results unless otherwise noted ALS is accredited for specific fields of testing (scopes) in the following testing sectors. The quality system implemented at ALS conforms to accreditation requirements and is applied to all analytical testing performed by ALS The following table lists testing sector, accreditation body, accreditation number and website. Please contact these accrediting bodies or your ALS project manager for the current scope of accreditation that applies to your analytical testing. Testing Sector Accreditation Body Certificate Website Number Environmental PJLA (DoD ELAP) Utah (TNI) Nevada Oklahoma Iowa Page 4 of 5 Tue, 04/17/18 2 55 PM ENVREP-V4.8 ANALYTICAL REPORT Workorder: 34-1810211 Client: Wasatch Environmental, inc. Project Manager: Jessica Helland Result Symbol Definitions MDL = Method Detection Limit, a statistical estimate of method/media/instrument sensitivity. RL = Reporting Limit, a verified value of method/media/instrument sensitivity CRDL = Contract Required Detection Limit Reg. Limit = Regulatory Limit. ND = Not Detected, testing result not detected above the MDL or RL < This testing result is less than the numerical value. ** No result could be reported, see sample comments for details. Qualifier Symbol Definitions U = Qualifier indicates that the analyte was not detected above the MDL. J = Qualifier Indicates that the analyte value is between the MDL and the RL. It is also used to indicate an estimated value for tentatively identified compounds in mass spectrometry where a 1 1 response is assumed B = Qualifier indicates that the analyte was detected in the blank E = Qualifier indicates that the analyte result exceeds calibration range. P = Qualifier indicates that the RPD between the two columns is greater than 40%. Page 5 of 5 Tue, 04/17/18 2:55 PM ENVREP-V4 8 ANALYTICAL REPORT Report Date: April 24, 2018 Chris Nolan Wasatch Environmental, Inc. 2410 West California Ave Salt Lake City, UT 84104 Phone: (801) 972-8400 E-mail: cn@wasatch-environmental.com Workorder: Project ID: Purchase Order: Project Manager 34-1810970 Indoor Sampling 041818 2276-001A Jessica Helland 14.0.101.i , 6,cpare Date - 'Šarnpling Apart-C + 106 1810970001 04/18/18 04/18/18 Indoor Sampling ADDRESS 960 West LeVoy Drive, Salt Lake City, Utah, 841 23 USA 1 PHONE +1 801 266 7700 I FAX +1 801 268 9992 ALS GROUP USA, CORP. An ALS Limited Company www.alsglobal.com RIMHT SOLUTIOrIS i . Page 1 of 3 Tue, 04/24/18 1:57 PM ENVREP-V4.8 ANALYTICAL REPORT Workorder: 34-1810970 Client: Wasatch Environmental, Inc. Project Manager: Jessica He!land Analytical Results Sample ID: Apart-C + 106 Lab ID: 1810970001 Matrix: Air Sampling Site: Indoor Sampling Media: Summa 6 Liter Canister Sampling Parameter. Air Volume 6 L Collected: 04/18/2018 Received: 04/18/2018 Analysis Method - EPA TO-15 SIM Preparation: Not Applicable Analysis: EPA TO-15 SIM, Air Batch: IV0A/3967 (HBN: 213420) Analyzed: 04/23/2018 19:50 Instrument ID: 5975-L Percent Solid: NA - Report Basis: Wet Analyte 1,' ,?, P., -.. ' :;f4es,41t (PPP) I '; 1: „ „ I- Result 4 - 4 ugtrtil : (pphri' , g.),Ilutior ''" R SI. e • , ... ual ••• Vinyl chloride ND <0.13 0.050 1 1,1-Dichloroethene ND <0.20 0.050 1 cis-1,2-Dichloroethene ND <0 20 0.050 1 Trichloroethene ND <0.27 0.050 1 Tetrachloroethene ND <0 34 0.050 1 Analysis Methpd - EPA TO-15 SJM Preparation: Not Applicable Analysis: EPA TO-15 SIM, Air Analyzed: 04/24/2018 09:54 - 1 ‘. 3atch: IVOA/3967 (HBN: 213420) Result , : , Instrument ID: 5975-L Percent Solid: NA 'Report Basis: Wet ,i' ‘,ArtOlytq: : ..-.: -A ..... •Rosult (p.0): , r , - .f..- (iig/ir3) 43.1. (ppb) , .Pilutiok ' ! . ? . _ " ual-- trans-1,2-Dichloroethene 10 42 0 50 10 E Comments Workorder: 1810970 Compound flagged with an "E" qualifier is considered to be an estimated value. Report Authorization (/S/ is an electronic signature that complies with 21 CFR Part 11) :Method Analyst Peer Review EPA TO-15 SIM /S/ Benson Boy /S/ Lisa M. Reid 04/24/2018 12 23 04/24/2018 13:39 Laboratory Contact Information ALS Environmental Phone (801) 266-7700 960 W Levoy Drive Email: alslt.lab@ALSGlobal.com Salt Lake City, Utah 84123 Web: www.alsslc.com Page 2 of 3 Tue, 04/24/18 1:57 PM ENVREP-V4.8 ANALYTICAL REPORT Workorder: 34-1810970 Client: Wasatch Environmental, lnc. Project Manager: Jessica He!land General Lab Comments The results provided in this report relate only to the items tested. Samples were received in acceptable condition unless otherwise noted Samples have not been blank corrected unless otherwise noted This test report shall not be reproduced, except in full, without written approval of ALS. ALS provides professional analytical services for all samples submitted. ALS is not in a position to interpret the data and assumes no responsibility for the quality of the samples submitted. All quality control samples processed with the samples in this report yielded acceptable results unless otherwise noted. ALS is accredited for specific fields of testing (scopes) in the following testing sectors. The quality system implemented at ALS conforms to accreditation requirements and is applied to all analytical testing performed by ALS. The following table lists testing sector, accreditation body, accreditation number and website Please contact these accrediting bodies or your ALS project manager for the current scope of accreditation that applies to your analytical testing. Testing Sector Accreditation Body Certificate Website Number Environmental PJLA (DoD ELAP) Utah (TNI) Nevada Oklahoma Iowa Result Symbol Definitions MDL = Method Detection Limit, a statistical estimate of method/media/instrument sensitivity. RL = Reporting Limit, a verified value of method/media/instrument sensitivity. CRDL = Contract Required Detection Limit Reg Limit = Regulatory Limit. ND = Not Detected, testing result not detected above the MDL or RL. < This testing result is less than the numerical value. ** No result could be reported, see sample comments for details. Qualifier Symbol Definitions U = Qualifier indicates that the analyte was not detected above the MDL J = Qualifier Indicates that the analyte value is between the MDL and the RL It is also used to indicate an estimated value for tentatively identified compounds in mass spectrometry where a 1:1 response is assumed. B = Qualifier indicates that the analyte was detected in the blank. E = Qualifier indicates that the analyte result exceeds calibration range. P = Qualifier indicates that the RPD between the two columns is greater than 40%. Page 3 of 3 Tue, 04/24/18 1 57 PM ENVREP-V4 8 , *ESC ANALYTICAL REPORT May 03, 2018 myESC " C. 065 Lebanon Rd, Moiu,rfaluiftet, TN 37122 615-758-5858 800-765.859 www.esciabsciences.com of ' Wasatch Environmental Sample Delivery Group: Samples Received: Project Number: Description: Report To: L989596 04/28/2018 2276-001A Sub Slab Soil Gas Christopher Nolan 2410 West California Avenue Salt Lake City, UT 84104 Entire Report Reviewed By: VI-10 John Hawkins Technical Service Representative Results relate only to the items tested or calibrated and are reported as rounded values This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable. sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures 060302, 060303. and 060304. 1Cp o Sc 8 Al 7 GI 6 Qc 5 Sr 3 SS 4 Cn TABLE OF CONTENTS ONE LAB. NATIONWIDE. 40 Cp: Cover Page 1 Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results 5 1 L989596-01 5 2 L989596-02 6 3 L989596-03 7 4 L989596-04 8 Qc: Quality Control Summary 9 Volatile Organic Compounds (MS) by Method TO-15 9 GI: Glossary of Terms 11 Al: Accreditations & Locations 12 Sc: Sample Chain of Custody 13 ACCOUNT. PROJECT: SDG DATE/TIME. PAGE Wasatch Environmental 2276-001A L989596 05/03/181218 2 of 14 1 Cp 2 Tc 9 SC 8 Al GI 6 Qc 4 Cn 5 Sr SAMPLE SUMMARY ONE LAB NATIONWIDE. 1 L989596-01 Air Collected by Chris Nolan Collected date/time 04/27/18 09.45 Received date/time 04/28/18 0845 Method „ . Volatile Organic Compounds (MS) by Method TO-15 Batch —WG110436/ Dilution Preparation dateltime 04/30/18 22:07 Analysis dateltime 04/30/18 22 07 Analyst MBF— — Collected by Collected date/time Received date/time 2 L989596-02 Air Chris Nolan 04/27/18 09:50 04/28/18 08:45 Method Batch Dilution Preparation date/tIme Analysis date/time Analyst Volatile Organic Compounds (MS) by Method TO-15 WG1104867 2 04/30/18 22.52 04/30/18 22.52 MBF Collected by Collected date/time Received date/time 3 L989596-03 Air Chris Nolan 04/27/18 10'00 04/28/18 08:45 Method Batch Dilution Preparation date/time Analysis date/time Analyst Volatile Organic Compounds (MS) by Method TO-15 WG1104867 04/30/18 23 36 04/30/18 23.36 MBF Collected by Collected date/time Received date/time 4 L989596-04 Air Chris Nolan 04/27/18 10.05 04/28/18 08:45 Method Batch Dilution Preparation date/time Analysis date/time Analyst , Volatile Organic Compounds (MS) by Method TO-15 WG1104867 2 05/01/18 00 21 05/01/18 0.0:21 MBF Volatile Organic Compounds (MS) by Method TO-15 WG1105325 10 05/01/18 19•40 05/01/18 19:40 BG ACCOUNT' PROJECT: SDG* DATE/TIME: PAGE Wasatch Environmental 2276-001A L989596 05/03/18 12 18 3 of 14 3 Ss Cp 2 Tc Sc 8 Al 7 GI 5 Sr 6 Qc CASE NARRATIVE ONE LAB. NATIONWIDE. .410 All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All radiochemical sample results for solids are reported on a dry weight basis with the exception of tritium, carbon-14 and radon, unless wet weight was requested by the client. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, l affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. John Hawkins Technical Service Representative ACCOUNT: PROJECT. SDG. DATE/TIME* PAGE. Wasatch Environmental 2276-001A L989596 05/03/181218 4 of 14 1 SAMPLE RESULTS - 01 Collected date/time: 04/27/18 09:45 L989596 Volatile Organic Compounds (MS) by Method T0-15 ONE LAB NATIONWIDE 41* 'Cp CAS # Mol. Wt. RDL1 RDL2 Result Result Qualifier Dilution Batch Analyte ppbv ug/m3 ppbv ug/m3 2 1,1-Dichloroethene 75-35-4 96.90 0.400 1.59 ND ND WG1104867 Tc cis-1,2-Dichloroethene 156-59-2 96.90 0.400 1 59 ND ND WG1104867 trans-1,2-Dichloroethene 156-60-5 96 90 0 400 1 59 1 60 6.34 WG1104867 3 Ss WG1104867 Tetra chloroethylene 127-18-4 166 0.400 2.72 ND ND Trichloroethylene 79-01-6 131 0 400 2 14 ND ND WG1104867 4 WG1104867 Vinyl chloride 75-01-4 62.50 0 400 1 02 ND ND Cn (S)1,4-Bromofluorobenzene 460-00-4 175 60 0-140 97 3 WG1104867 6 Qc 7 GI 3 Al 9 SC ACCOUNT: PROJECT: SDG. DATE/TIME: PAGE: Wasatch Environmental 2276-001A L989596 05/03/181218 5 of 14 2 SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE. Collected date/time: 04/27/18 09:50 Volatile Organic Compounds (MS) by Method TO-15 L989596 Cp CAS # Mol. Wt. RDL1 RDL2 Result Result Qualifier Dilution Batch Analyte ppbv ug/m3 ppbv ug/m3 2 1,1-Dichloroethene 75-35-4 96.90 0.400 1 59 ND ND 2 WG1104867 Tc cis-1,2-Dichloroethene 156-59-2 96.90 0.400 1 59 ND ND 2 WG1104867 trans-1,2-Dichloroethene 156-60-5 96.90 0 400 1 59 12 2 48 5 2 WG1104867 3 Ss WG1104867 Tetrachloroethylene 127-18-4 166 0.400 2.72 0 643 4.37 2 Trichloroethylene 79-01-6 131 0 400 2 14 ND ND 2 WG1104867 4 WG1104867 Vinyl chloride 75-01-4 62.50 0 400 1 02 ND ND 2 Cn (S)1,4-Bromofluorobenzene 460-00-4 175 60.0-140 98 3 WG1104867 6 Qc 7 GI 3 Al 9 SC ACCOUNT' PROJECT. SDG• DATE/TIME: PAGE Wasatch Environmental 2276-001A L989596 05/03/1812:18 6 of 14 3 SAMPLE RESULTS - 03 ONE LAB. NATIONWDE. Collected date/time: 04/27/18 10.00 Volatile Organic Compounds (MS) by Method TO-15 L989596 1 Cp CAS # Mol. Wt. RDL1 RDL2 Result Result Qualifier Dilution Batch Analyte ppbv ug/m3 ppbv ug/m3 2 1,1-Dichloroethene 75-35-4 96 90 0 400 1.59 ND ND 2 WG1104867 Tc cis-1,2-Dichloroethene 156-59-2 96.90 0 400 1.59 ND ND 2. WG1104867 trans-1,2-Dichloroethene 156-60-5 96 90 0 400 1 59 20 6 81 6 2 WG1104867 3 SS W61104867 Tetrachloroethylene 127-18-4 166 0 400 2 72 ND ND 2 Trichloroethylene 79-01-6 131 0.400 2 14 ND ND 2 WG1104867 4 WG1104867 Vinyl chloride 75-01-4 62.50 0 400 1 02 1.43 3.65 2 Cn (S)44-Bromofluorobenzene 460-00-4 175 60.0-140 95.5 WG1104867 6 Oc 7 GI a Al Sc ACCOUNT: PROJECT: SDG• DATE/TIME: PAGE* Wasatch Environmental 2276-001A L989596 05/03/181218 7 of 14 4 Cn 3 Ss 1 Cp 2 Tc 9 Sc Al 6 Qc 7GI 4 SAMPLE RESULTS - 04 Collected date/time: 04/27/18 1005 L989596 Volatile Organic Compounds (MS) by Method TO-15 ONE LAB. NATIONWIDE CAS # Mol. Wt. RDL1 RDL2 Result Result Qualifier Dilution Batch Analyte ppbv ,up_rn..3._ _p_phv ug/m3 1,1-Dichloroethene 75-35-4 96.90 0 400 159 ND ND 2 WG1104867 as-1,2-Dichloroethene 156-59-2 96.90 0.400 1 59 ND ND 2 WG1104867 trans-1,2-Dichloroethene 156-60-5 96.90 2.00 7 93 120 474 10 WG1105325 Tetrachloroethylene 127-18-4 166 0 400 2.72 1.33 9.04 2 WG1104867 Trichloroethylene 79-01-6 131 0 400 2 14 ND ND 2 WG1104867 Vinyl chloride 75-01-4 62.50 0 400 1 02 ND ND 2 WG1104867 (S)Z4-Bromofluorobenzene 460-00-4 175 60.0-140 96.8 WG1104867 (S)Z4-Bromofluorobenzene 460-00-4 175 60.0-140 95 9 WG1105325 SA ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE. Wasatch Environmental 2276-001A L989596 05/03/181218 8 of 14 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3306021-1 04/30/18 08'2 5 • (LCSD) R3306021-2 Spike Amount LCS Result 04/30/18 09.10 LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ppbv ppbv ._.. .... ppbv % % % % , .........,.._ _ % „, ,_,..... ... , _ —3-.75 Vinyl chloride 3 94 4.00 105 107 70 0-130 1 60 25 1,1-Dichloroethene 3.75 3 97 3.95 106 105 70.0-130 0.411 25 trans-1,2-Dichloroethene 3.75 3.93 3 91 105 104 70.0-130 0.630 25 cis-1,2-Dichloroethene 3 75 4.00 3.97 107 106 70.0-130 0.959 25 Tnchloroethylene 3 75 3.94 3.91 105 104 70.0-130 0.692 25 Tetrachloroethylene 3.75 4 06 4 03 108 107 70.0-130 0.807 25 (S)1,4-Bromofluombenzene 99 8 100 60 0-140 9 SC 7 GI Al WG1104867 Volatile Organic Compounds (MS) by Method TO-15 Method Blank (MB) QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. L989596-01,02,03,04 JO 'Cp (MB) R3306021-3 04/30/18 09.57 MB Result MB Qualifier MB MDL MB RDL 2 Analyte _ ppbv ppbv ppbv Tc 1,1-Dichloroethene cis-1,2-Dichloroethene 0.0389 0.200 3 SS trans-1,2-Dichloroethene 0.0464 0.200 Tetrachloroethylene 0.0497 0.200 4 Trichloroethylene 0.0545 0 200 Cn Vinyl chloride 0.0457 0 200 (S)1,4-Bromofluorobenzene 97 3 60 0-140 5 Sr ACCOUNT. PROJECT: SDG: DATE/TIME: PAGE: Wasatch Environmental 2276-001A L989596 05/03/181218 9 of 14 5 Sr 4 Cn 3 SS Cp 2 Tc 9 SC 7 GI Al WG1105325 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE Ilk VolatHe Organic Compounds (MS) by Method TO-15 1989596-04 (MB) R3306297-1 05/01/18 09:50 MB Resu(t MB Qualifier MB MDL MB RDL Analyte ppbv ppbv ppbv trans-1,2-Dichloroethene U 0.0464 0 200 (S)1,4-Bromofluorobenzene .92.2 60 0-140 (LCS) R3306297-2 05/01/18 11.53 • (LCSD) R3306297-3 05/01/18 1237 Spike Amount LCS Result LCSD Result LCS Rec. Ana lyte ppbv ppbv ppbv trans-1,2-Dichloroethene 3 75 3.70 3.98 98.7 (S)1,4-Bromaluorobenzene 99 5 LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits % % % % — 106 —70.6-130-- 7 37 25 101 60.0-140 Method Blank (MB) Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) ACCOUNT: PROJECT. SDG. DATE/TIME: PAGE: Wasatch Environmental 2276-001A L989596 05/03/1812:18 10 of 14 6 Qc 5 Sr 4 Cn 3 Ss 2 Tc 9 SC Cp 7 GI 8 Al GLOSSARY OF TERMS ONE LAB. NATIONWIDE. AO Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative Abbreviations and Definitions MDL ND RDL Rec. RPD SDG (S) Analyte Dilution Limits Qualifier Result Case Narrative (Cn) Quality Control Summary (Qc) Sample Chain of Custody (Sc) Sample Results (Sr) Sample Summary (Ss) Qualifier Method Detection Limit. Not detected at the Reporting Limit (or MDL where applicable). Reported Detection Limit. Recovery. Relative Percent Difference Sample Delivery Group. Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate, used to evaluate analytical efficiency by measuring recovery Surrogates are not expected to be detected in all environmental media. Not detected at the Reporting Limit (or MDL where applicable). The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges This column provides a letter and/or number designation that corresponds to additional information concerning the result reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample If there was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. A brief discussion about the included sample results, including a discussion of any non-conformances to protocol observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report This section of the report includes the results of the laboratory quality control analyses required by procedure or analytical methods to assist in evaluating the validity of the results reported for your samples These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis This section of your report will provide the results of all testing performed on your samples. These results are provided by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Description The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG. ACCOUNT. PROJECT: SDG, DATE/TIME: PAGE Wasatch Environmental 2276-001A L989596 05/03/18 12 18 11 of 14 Cp 2 Tc 3 Ss 4 Cn 5 Sr 6 Qc 7 GI 9 SC ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE ilk ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus The model is conducive to accelerated productivity, decreasing turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. *Not all certifications held by the laboratory are applicable to the results reported in the attached report *Accreditation is only applicable to the test methods specified on each scope of accreditation held by ESC Lab Sciences. State Accreditations Alabama 40660 _ A laska 17-026 Arizona AZ0612 Arkansas 88-0469 California 2932 Colorado TN00003 _ Connecticut PH-0197 Florida _ E87487 Georgia_ NELAP Georgia _923 Idaho TN00003 „ _ Illinois 200008 _ Indiana C-TN-01 _— Iowa 364 Kansas E-10277 Kentucky i 6 90010 _ Kentucky 2 16 Louisiana A130792 Louisiana LA180010., Maine TN0002 Maryland 324 Massachusetts M-TN003 _ Michigan 9958 Minnesota 047-999-395 Mississippu TN00003 Missouri 340 Montana CERT0086 Nebraska Nevada „.., New Hampshire New Jersey-NELAP New Mexico . „ New York „ North Carolina North Carolina North Carolina North Dakota OhiotVAP Oklahoma 91:99911_ Pen nsylvanla Rhode Island South Carolina - „ South Dakota Tennessee 4 Texas Texas 5 Utah Vermont _ Virginia Washington West V!rginia Wisconsin Wyoming NE-OS-15-05 TN-03-2002-34 2975 TN002 n/a. 11742_ EnV3-75 DW21704 41 R-140 ..—.„ CL0069 9915 TN200002 68-0269 -L-A0 0035.6 84004 n/a 2006 T104704245-17-14 LAB0152 TN00003 VT2006 460132 C847 233 9980939910 - AAA Third Party Federal Accreditations A2LA7 ISO 17025. 1461 01 AIHA-LAP,LLC EMLAP 100789 A2LA - ISO 17025 5 1461 02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 FPA7Creito TN00003 1 Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable Our Locations ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. ESC Lab Sciences performs all testing at our central laboratory. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE. Wasatch Environmental 2276-001A L989596 05/03/18 12.18 12 of 14 ....r....---:-•-•-t Company .NAmef Address: Wasatch Environmental SaR Lalce City, UT 84104 2410 West California Ave, kiting Intormation; WASATCHUT AM Chain of Distal / ... b. ' -e, ... . - ) C- A • , • , c,rar•PMFOO ' 12°"trtietutoc,ov"srat P4 El fhom.m456-sess tfq....; 600467•51b9' xV.. . rax 615-7S8-565.4 121.: Report to; (ft-hz Nch-r---1 Email To: c...A.) 0 k"......4 3perc i4 - eivilirl-Dia2"""1"141.--Cer,• . %Z) 1/4-) L. "*.h: s: - , . Profect • DeScription: S./ 13 ,51... ix a S e.-17.4'...- 6 AS City/State Collected: 5,0 L.1- I.,„".i 4, -4- LI-C(4H , .,,..-,. Phone. 801- 972-8400 Client-Project I( Lab Project it .,.., i ..-. ...„, ' ,:. , ., .. 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L 1.!....t:•. • . f,•••=•!'es. ...tc •%:. ..• ..1.• t ... 4,:,..• • • .: '• .z.. ....s • • M ORANDUM DATE June 17, 2014 SUBJECT: Removal of the trans-1,2-Dichloroethylene (CAS1N 156-60-5) Provisional Peer-Reviewed Toxicity Value (PPRTV) aw:ssment from the Electronic Library FROM: Scott Wessel kamper Director, aiperfund Health Rsk Technical Support Inter (STS EPA/ ORD NCEA TO: Michele Elurgess (0S/VER=TI) Lynn Rowers (NCEA) Teresa thannon (NCEA) The Rle It was brought to the attention of the STMthat there is an inconsistency in the condusions regarding the derivation of a reference concentration (Rq for trans-1,2-Dichloroethylene (DM between the 2006 PPM assessment and the 2010 IRSassessment (http://www.epa.gov/iritoxreviews/0418tr.pdf) for this chemical. The 2006 PPRIVaqcPssment derived a chronic p-RCof 0.06 mg/ m3 based on pulmonary and liver effects observed in the prindpal study by Freundt et al. (1977). No subchronic p-RCwas derived. The 2010 IRSassessment found Freundt et al. (1977), a study by the National Toxicology Program (NIP, 2002), and an unpublished study by DuPont (1998) to be insuffident to support derivation of an RCvalue for trans-1,2-DCE Thus, there appears to be a fundamental difference in how the prindpal study and critical effect(s) used to derive the chronic p- RC in the 2006 PFRIV assessment were evaluated compared to what was more recently done by IRS It is important to note that there are some differences in the respective decision-making processes for developing FPRTV and IRSassessments spedfically with the IRSProgram having a more extensive review process (e.g., agency and interagency review steps, a public comment period, etc.) than that utilized for developing PFRTV assessments. Fbrtinent information from the 2010 lIRISToxicological Review on trans-1,2-DCEthat outlines why the Freundt et al. (1977) study was discounted and no RCvalue was derived is excerpted and italicized below: "The finding of lung effects in the Freundt et al. (1977) study is difficult to interpret as t his study is the only report of lung pathology in animals exposed to trans-1,2-DM a small number of animals were examined, several of the controls also developed this effed, and the upper respiratory tract was not examined for pathology." "For each of the exposure durations, t here was no statistically significant difference between the controls and the exposed groups with resped to the inddence of liver effects (fat accumulation). In general, however, the inddence and severity of fat accumulation increased with increasing exposure duration. Although Freundt et al. (1977) reported histopathologic changes in the liver of rats, the DuPont (1998) study did not corroborate the Freundt et al. (1977) study findings. DuFbnt (1998) reported relatively small increases in relative and absolute liver weight (1-8%) and no gross or microscopic changes of the liver attributable to trans-1,2-DCE at an exposure concentration 20-fold higher than that 1 used in the Freundt et al. (1977) study. NTP (2002a) similarly found no histopathologic changes in the liver when trans-1,2-DCEwas administered for 90 days by the oral route at dietary conœntrations as high as 50,000 ppm. In light of the results of DuPont (1998) and NIP (2002a), it is difficult to explain the liver findings in the single-exposure conœntrat ion study by Freundt et al. (1977). Gven the limitations of the Freundt et al. (1977) study (i.e., small sample size, use of only one exposure concentration, and observation of fatty aocumulat ion in the liver lobules and Kupffer cells in control animals at some exposure durations) and lack of corroboration from other studies, the Freundt et al. (1977) study was not used as the basis for derMng an HCfor trans-1,2-DCE" "In summary, the available inhalation data from DuPont (1998) and Freundt et al. (1977) were considered insufficient to support reference value derivation and, therefore, an RiCfor trans-1,2-DCEwas not derived." arrent practice by the PFR1V Rogram states that once an IR1Sassessrnent becomes available for any given chemical, the PPRTV assessment for that chemical is removed from the PPRTV elect ronic library. Thus, based on this practice and the rationale outlined above, it is recommended that the conclusions presented in the InSassessment for trans-1,2-DCE be prewntly adhered to, and the trans- 1,2-DCEFFRN acecssment has been removed from the electronic library. Any additional questions regarding trans-1,2-DCE should be directed to the IRS Hotl ine at (202) 566-1676 or htt p://www.epa.govi i ri cont act_hot I i ne. ht m. References: Freundt, KJ, GP. Uebaldt and E Ueberwirth. '1977. Toxidty studies on trans-1,2-dichloroethylene. Toxicology. 7: 141-153. NTP (2002). NIP technical report on the toxidty studies of trans-1,2-dichloroethylene (CASNo. 156-60- 5) administered in microcapsules in feed to P3/14/N rats and Bann mice. FUblic Health rvice, U.S Department of Health and Human rviœs; NTP1R55. Available from the National Institute of Environmental Health Sciences, Research Triangle Park, NC and online at http://ntp.niehs.nih.gov/nto/htdocsIST rots/tox055.pdf 2