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HomeMy WebLinkAboutDSHW-2018-004113 - 0901a06880813c52Sincerely, /-814L9— L. Chase Forte Senior Remediation Proj ect Manager Georgia-Pacific LLC Georgia-Pacific Georgia-Pacific LLC 133 Peachtree Street NE (30303-1847) P.O. Box 105605 Atlanta, Georgia 30348-5605 (404) 652-6874 (404) 654-4701 fax April 13, 2018 Helge Gabert Utah Department of Environmental Quality Division of Waste Management and Radiation Control 195 North 1950 West Salt Lake City, UT 84116 Subject: GP Gypsum 2017 Groundwater Monitoring Report Georgia-Pacific Fomier Gypsum Manufacturing Facility 200 South State Street (Utah Highway 24) Sigurd, UT Dear. Mr. Gab ert: Div of Waste Managerrent and Radiation Conttoi IvIAY - 8 2018 "171-1W -20/?-00t)15 Please find enclosed the 2017 Groundwater Monitoring Report for activities conducted last year at the Georgia-Pacific Former Gypsum Manufacturing Facility in Sigurd, UT. The monitoring activities were conducted in October of 2017 in accordance with the approved path forward outlined in the Groundwater Quality Evaluation Update and Source-Area Investigation/Excavation Completion Report completed by Tetra Tech, and as discussed in a meeting between Tetra Tech and Georgia-Pacific on June 1, 2017. The work was performed by Tetra Tech on behalf of Georgia-Pacific. We look forward to discussing with you the 2017 monitoring results and Georgia-Pacific's path forward for the site. If you have any questions regarding the final report or our future plans for the site, please feel free to call me at (404) 539-3509 to discuss. Attachments: 2017 Groundwater Monitoring Report CC: Mike Egan, Tetra Tech Greg Council, Tetra Tech Div of Waste Management and Radiation Control MAY - 8 2O18 MAW-200-004-1 /3 20 I 7 Groundwater Monitoring Report Georgia-Pacific Former Gypsum Manufacturing Facility Sigurd, Utah April 13, 2018 TETRA TECH 4750 West 2100 South, Suite 400, Salt Lake Oty, UT 84120 Tel 801364.1064 Fax 801.364.2021 www.tatratech.corn 2017 Groundwater Monitoring Report Georgia-Pacific Former Gypsum Manufacturing Facility REVISION HISTORY Vers Date Description ion 1 January 5, 2018 DRAFT 2 February 2, 2018 DRAFT Revision 3 February 26, 2018 DRAFT Final 4 April 13, 2018 Final April 13, 2018 TETRA TECH ii III 2017 Groundwater Monitoring Report Georgia-Pacific Former Gypsum Manufacturing Facility III TABLE OF CONTENTS I 1 introduction 1 1.1 Description of Work 1 1.2 I Site Background 2 1.3 Physical Setting and Site Geology 3 1.4 Site Hydrogeology 3 1.5 Contaminant Sources. 3 I 1.6 Potential Exposure Pathways 4 2 Groundwater Sampling and Analysis 5 2.1 Methodology 6 I 2.2 Results 5 2.3 Statistical Evaluation 6 2.4 Conclusions 7 I 3 Proposed Path Forward a 3.1 Monitored Natural Attenuation of Diesel-Related Groundwater Impacts 8 3.2 Institutional Control 8 I 4 References 9 111 II III Il 111 i II Il II 111 April 13, 2018 TETRA TECH i 2017 Gra.ndwater Monitoring Report Georgia-Pacific Former Gypsum Manufactunng Facility FIGURES Figure 1. Site Location Map Figure 2. GP Gypsum Facility Site Layout APPENDICES Appendix A. Analytical Laboratory Report Appendix B. Historical Measured Groundwater Concentrations Appendix C. Theil-Sen Trend Analyses Appendix D. Predictive Theil-Sen Trend Analysis for Naphthalene at MW-7 April 13, 2018 TETRA TECH iv 2017 Grouldwater Monitoring Report Georgia-Pacific Former Gypsum Manufacturing Facility ACRONYMS AND ABBREVIATIONS AST aboveground storage tank bgs below ground surface BTEX benzene, toluene, ethylbenzene, and xylenes °C degrees celsius COPC constituent of potential concern DERR Department of Environmental Response and Remediation DWMRC Division of Waste Management & Radiation Control EPA United States Environmental Protection Agency GP Georgia-Pacific GWQS Ground Water Quality Standards HASP health and safety plan LNAPL light non-aqueous phase liquid mg/L milligrams per liter mV millivolts NTU nephelometric turbidity unit SL Screening Level UDEQ Utah Department of Environmental Quality pg/I microgram per liter tiS/cm micro Siemens per centimeter UST underground storage tank VOC volatile organic compound April 13, 2018 TETRA TECH 2017 Grandwater Monitoring Report Georgia-Pacific Former Gypsum Manufactunng Facility 1 INTRODUCTION This report summarizes the results of the groundwater samphng conducted on October 26, 2017 by Tetra Tech, Inc. (Tetra Tech) at the former Georgia-Pacific (GP) Gypsum manufacturing facility located at 200 South State Street in Sigurd, Utah (Site). Figure 1 presents the location of the Site and Figure 2 presents a general layout of the facility. A hydraulic fluid leak occurred within the former manufacturing building in 2005-2006 due to the failure of the hydraulic-lift oil containment sump (Figure 2). Tetra Tech conducted a Phase I subsurface investigation in June 2011 and a Phase II in December 2012, which identified petroleum hydrocarbon impacts exceeding Utah Initial Screening Levels (ISLs) near the hydraulic-oil release location and northeast of that location. Some of the impacts are likely related to past releases of diesel fuel. The Site is identified by the Utah Department of Environmental Quality (UDEQ), Division of Environmental Response and Remediation (DERR) as Facility 2000058. Two state-identified petroleum hydrocarbon releases are associated with this site, with Release IDs HPR and MTX. Release HPR was opened in 1992 during the removal of petroleum storage tanks (USTs) from the property and was dosed on November 1, 1996 with no further action required, following remediation of excavated soil. The hydraulic fluid release is Release MTX. This release was opened on May 17, 2011. The site is currently being regulated by the UDEQ Division of Waste management & Radiation Control (DWMRC). Following source investigation and removal activities in 2017, and demonstration that environmental exposure risks are not significant, GP and UDEQ agreed on a path forward for the site including additional monitoring for regulated volatile organic compounds (VOCs) and trend analyses using the VOC data (Tetra Tech 2017). These activities are documented in this report. 1.1 Description of Work The 2017 groundwater monitoring approach induded the following tasks: 1. Task 1 — Field Preparation & Health and Safety Plan (HASP) Update: a. Prepare for monitoring event by arranging for supplies, coordinating access, and reviewing/updating HASP. 2. Task 2 — Groundwater Monitoring & Bail-Down Test: a. Measure water levels at all accessible monitoring twits and collect samples at the following wells: MW-4, MW 5, MW-6, MW-7, MW-9, MW-12, MW-13, MW-14, MW-15, and MW 17. b. Conduct laboratory analyses for site-specific volatile organic carbons (benzene, toluene, ethylbenzene, xylenes, and naphthalene) by EPA Method 8260, using Test America Laboratory. c. Perform bail-down test on the groundwater well (MW-18) installed in the backfilled hydraulic sump excavation to confirm non-recoverability of light non-aqueous phase liquid (LNAPL). 3. Task 3 — Reporting: a. Prepare a groundwater monitoring report including the lab report, figures, and sampling logs, including a statistical evaluation of the groundwater sampling results following the 2009 EPA Unified Guidance found in Chapter 21.3. April 13, 2018 TETRA TECH 1 2017 Groundwater Monitoring Report Georgia-Pacific Former Gypsum Manufacturing Facility 1.2 Site Background The gypsum facility was reportedly constructed in 1947 (Natresco & Associates 2006). The gypsum processing plant (mill) and wallboard manufacturing ceased operations in 2008. All structures associated with the facility were demolished in 2017. Future use of the Site is being evaluated by GP. Five underground storage tanks (USTs) and two above-ground storage tanks (ASTs) (Figure 2) were removed from the Site between 1988 and 1992. Petroleum impacted soils discovered during UST removals were reported to the State and the petroleum hydrocarbon release was assigned DERR Release Code HPR. The impacted soils were land-farmed on- Site within a 200-foot by 150-foot constructed pad on top of the former gypsum recycle board storage area, located southeast of the mill building. A liner was installed and a berm was built around the pad. Soil was placed in the cell and spread to a thickness of approximately 2.5 feet. The soils were treated with a bioremediation additive, fertilizer was added, and the soils were tilled periodically. DERR issued a no further action letter dated November 1, 1996, and Release HPR was closed. Following a 2005-2006 release of hydraulic oil at the site a limited subsurface assessment was performed (Natresco & Associates 2006). Five borings were advanced; three located within the lift pit and two located approximately 50 and 200 feet from the lift pit. Hydraulic oil was observed in the soil column above groundwater within the three borings advanced in the lift pit. In one of those borings, phase-separated oil was observed at the water table. A hydrocarbon odor was reported in the boring located approximately 50 feet northwest of the rift pit, but no hydrocarbon odor was identified in the boring located approximately 200 feet northwest of the lift pit. Subsequently, a site history review, regulatory review, and site visit was performed (AMEC 2010). Tetra Tech performed a Phase I subsurface investigation in May 2011, which included advancing twenty-two (22) soil borings to depths of between 20 and 35 feet below ground surface (bgs), installation of five groundwater monitoring wells, collection of soil and groundwater samples, and laboratory analyses for presence of petroleum hydrocarbon and related constituents (Tetra Tech 2011). A survey of the Site was also conducted to accurately map borings and monitoring wells relative to existing facility structures and property boundaries. DERR Release Code MTX was assigned for this site based on the initial report of petroleum impacts discussed in the Phase I report The release was opened on May 17, 2011, although the hydraulic oil leak had previously been verbally reported as a suspected release to UDEQ on July 27, 2006. Tetra Tech performed a Phase II subsurface inveštigation in December 2012, which included advancing twenty-one (21) soil borings to depths ranging from 25 to 50 feet bgs, installation of ten (10) groundwater monitoring wells, collection of groundwater and soil samples, and laboratory analysis for presence of petroleum hydrocarbons and other constituents (Tetra Tech 2013). A survey was also included in the Phase II investigation to accurately map new borings and monitoring wells relative to existing facility structures and property boundaries and to accurately determine groundwater levels. Tetra Tech also conducted four additional rounds of groundwater sampling: two in 2014 (Tetra Tech 2015), one in 2015 (Tetra Tech 2016), and one in 2016 (Tetra Tech 2017). In coordination with site demolition activities, a source-area investigation and removal at the hydraulic-oil release location was performed in accordance with a UDEQ-approved work plan (Tetra Tech 2017). Excavation at the hydraulic lift pit was conducted on March 6, 2017. During April 13, 2018 TETRA TECH 2 2017 Grouldwater Monitoring Report Georgia-Pacific Former Gypsum Manufacturing Facility backfill, an observation well was installed in the excavation for potential confirmation that any residual LNAPL was not recoverable. 1.3 Physical Setting and Site Geology The Site is situated on the foothills of the Sevier Plateau at an approximate elevation of 5,200 feet above sea level. Before the first quarter of 2017, when site demolition was completed, the facility included an approximately 100,000 square-foot building for gypsum processing and wallboard manufacturing, employee change rooms, and a separate office. A gypsum recycle pile is located east of the mill building. The Site is located within the Colorado Plateau physiographic province on the east side of the Sevier River valley, with surface geology mapped as Quaternary alluvium and colluvirin sediments. Immediately east of the facility are outcrops of late Oligocene to middle Miocene volcanic rocks consisting of ash flow tuffs. Further east and adjacent to the volcanic ash flow tuffs are middle Jurassic mudstones. Based on the Phase I and Phase 11 subsurface investigations conducted by Tetra Tech, subsurface soils generally consist of an upper sandy silt in the eastern half of the Site and an upper silty/gravelly sand fill in the western half of the Site underlain by interbedded and alternating beds of silty sand, sandy silt , and gravelly sand. The northern end of the Site consists of overbank deposits of clayey silt with interbedded silty gravel. The Sevier River is located approximately 400 feet north of the northern Site boundary. The Sevier River flows from west to east at this location and flows toward the north-northeast regionally. The current land use adjacent to the Site is Highway 24 and residential property to the west, commercial property to the north, and undeveloped land to the south and east 1.4 Site Hydrogeol ogy Groundwater flow at the Site is generally toward the north. Groundwater has typically been encountered in coarser grained deposits: well sorted sand and silty gravel. Groundwater below the mill and manufacturing plant was encountered approximately 22 to 26 feet bgs during the 2017 groundwater monitoring events. West of the manufacturing plant, groundwater was encountered approximately 22 to 30 feet bgs. North of the manufacturing plant, groundwater was encountered approximately 12 to 20 feet bgs. The natural discharge point for Site groundwater is the Sevier River. 1.5 Contaminant Sources Potential contaminant sources that have been identified at the Site include: (1) hydraulic oil impacted soil, including adsorbed and ptiase-separated fractions, surrounding the hydraulic lift in the main manufacturing building; and (2) former 10,000 gallon ASTs located east of the main manufacturing building that have been removed. The hydraulic oil release resulted from leaks in the subsurface concrete hydraulic lift sump that acted as a reservoir for oil from the hydraulic lift cylinders. The hydraulic lift was a component of the wallboard manufacturing system. The original hydraulic lift system at the facility was repaired in 2005 and this repair included removing and repacking the hydraulic cylinders. From September 2005 through July 2006, the GP staff documented a loss of approximately 1,800 gallons of hydraulic fluid. At that time, the old lift equipment was removed, the sump was cleaned, and a new lift, pump, and oil tank were installed. In 2017, soil in this area was excavated (Tetra Tech 2017). April 13, 2018 TETRA TECH 3 2017 Groundwater Monitoring Report Georgia-Pacific Former Gypsum Manufacturing Facility The 10,000 gallon ASTs east of the mill building were a probable contaminant source prior to their removal in approximately 1989. The soils in this area have been remediated to remove residual source material. The potential residual impacts from the former 10,000 gallon ASTs were discovered during the Phase l investigation conducted by Tetra Tech in 2011. The investigation identified petroleum hydrocarbon impacts with a pattern consistent with diesel fuel east of the mill building and extending north of the crusher building. 1.6 Potential Exposure Pathways Potential transport mechanisms include downward vertical migration of phase-separated hydraulic oil or leached dissolved fraction hydraulic oil or diesel to groundwater with subsequent lateral migration as dissolved and phase-separated product within or just above shallow groundwater. Based on previous laboratory results indicating very low to non-detected VOCs, contaminant transport by volatilization and either atmospheric dispersion or enclosed space accumulation is expected to be minor at points of potential exposure. Based on data collected to date, no transport mechanisms are believed to have brought contaminants into contact with surface media away from source areas (including surface soils, surface water, or stream sediments). April 13, 2018 TETRA TECH 4 2017 Grouridwater Monitoring Report Georgia-Pacific Former Gypsum Manufactunng Facility 2 GROUNDWATER SAMPLING AND ANALYSIS An additional round of groundwater samples was collected in October 2017 and analyzed for Site VOCs. This section describes the methodology, results, and conclusions of that sampling event 2.1 Methodology All sampling conducted during the 2017 groundwater monitoring event was conducted in accordance with the approved Sampling and Analysis Plan and Quality Assurance and Control Plan (Tetra Tech 2012) and for the wells and parameters identified in the latest Groundwater Quality Evaluation (Tetra Tech 2017). The site specific health and safety plan (HASP) was reviewed by field personnel. Unfiltered groundwater samples were collected from nine groundwater monitoring wells on October 26, 2017: MW-4, MW 5, MW-6, MW-7, MW-9, MW-12, MW-13, MW-15, and MW-17. Field parameter measurements collected included pH, temperature, specific conductance, dissolved oxygen, oxidation reduction potential, turbidity and depth to water. Tetra Tech attempted to locate monitoring well MW-14, but the well appeared to have been covered and/or damaged during Site activities. MW-17 is a deeper well with a 5-foot-long screened section 45 to 50 feet bgs. The remaining wells have longer (10 to 20 ft) screens across or near the water table (screen tops and bottoms range from 10 to 35 feet bgs). All down-hole sampling and monitoring equipment was decontaminated prior to use at each sampling location. Decontamination consisted of a Liquinox solution wash followed by a triple rinse with deionized water. All field parameter monitoring equipment was field calibrated prior to performing measurements. Each well was purged of three borehole volumes of water or until groundwater parameters stabilized. The groundwater surface was allowed to recover to near pre-purging conditions prior to sample collection. Sample collection was conducted utilizing a bladder pump. When LNAPL was present in a well (MW-12), groundwater samples were collected from below the LNAPL. Groundwater samples were shipped with chain-of-custody documentation to TestAmerica Laboratories, inc. in Nashville, Tennessee for analyses of Site-specific VOCs by EPA Method 8260B. The Site-specific VOCs indude benzene, toluene, ethylbenzene, and xylenes (BTEX) plus naphthalene. These constituents are often found in petroleum releases. Tetra Tech attempted to conduct a bail-down test on MW-18 installed in the backfilled hydraulic sump excavation to confirm-non-Tcoverability of LNAPL, but the well was dry when measured on October 26, 2017. 2.2 Results Groundwater field parameters collected during the 2017 monitoring event are presented in Table 1. Groundwater analytical laboratory results from the 2017 monitoring event are presented in Table 2. The full laboratory report is provided in Appendix A. Appendix B provides results from past groundwater sampling. At MW-12, which is near the hydraulic oil release, phase-separated oil was detected at an approximate thickness of 1.42 feet. This is consistent with past observations of LNAPL in this 1-inch diameter well. Based on prior analyses (Tetra Tech 2017), the LNAPL in the vicinity of this well is not recoverable and the LNAPL is not a significant source of regulated constituents. April 13, 2018 TETRA TECH 5 2017 Groundwater Monitonng Report Georgia-Pacific Former Gypsum Manufacturing Facility A hydrocarbon odor was noted at MW-7, although no discemable free product was measured in the well. Table 1. October 2017 Groundwater Field Parameters Monitoring Well ID Top of Casing Elevation Depth to Water (ft bgs) Temp (T) „H r SC (pS/cm) DO (mg/L) oRF, (mV) Turbidity (NTU) MW-4 5233 89 17 80 13 79 7.00 3 63 2.32 38 0 59 8 MW-5 5227.54 12 60 10 38 7 02 2 07 0.00 -175.0 33.1 MW-6 5242 26 24.69 17.15 7.67 0 72 4.52 6 0 627.0 MW-7 5235 71 20 09 16 27 7.63 1 59 0 00 -199 0 523 0 MW-9 5239 10 22 21 20 56 7.27 1.52 0 11 -105.0 294.0 MW-12 5241.92 25.90 16 60 7.77 0 65 1.25 -153 0 444.0 MW-13 5240 39 23 16 17.59 7 51 1 37 0 00 198 0 236 0 MW-15 5229 62 14 87 11.31 7.16 1.76 0 37 185 0 0 4 MW-17 5239 37 23 40 18.89 8.03 0 84 2.57 49 0 26.4 *C degrees Celsius; pS/cm micro Siemens/centmeter; mg/L: milligrams per liter; mV millivolts; NTU. nephelometric tsbidity unit Table 2. October 2017 Groundwater Sampling Results Monitoring Well ID Benzene (p cll.) Toluene (pg/L) Ethylbenzene (pg/L) Xyienes, Total (pg/L) Naphthalene (141-) GWQS: 2.2 GWQS: 1000 GWQS: 530 GWQS: 10000 GWQS: - MW-4 ND ND ND ND ND MW-5 ND ND ND ND ND MW-6 ND ND ND ND ND MW-7 ND ND 0.504 J ND 4.41 J MW-9 ND ND ND ND 1.01 J MW-12 ND ND ND ND ND MW-13 0.584 J ND 1.99 ND 1.02 J MW-15 ND ND ND ND ND MW-17 ND ND ND ND ND pg/L micrograms per liter; ND: non-detect; GWQS Utah Grcund Water Quality Standards (R317-6-2, Utah Administrative Code) J Estimated; detected below practical quantitation level No VOCs were detected at levels above the Utah Ground Water Quality Standards (GWQSs; R317-6-2, Utah Administrative Code). Low concentrations - below the practical quantitation limit- of benzene, ethylbenzene, and naphthalene were detected at MW-7, MW-9, and MW-13. Additionally, MW-13 (near the presumed former diesel source) had a measured ethylbenzene concentration of 1.99 pg/L. At MW-12 near the hYdraulic oil release, there were no detections of benzene, toluene, ethylbenzene, xylenes, or naphthalene. 2.3 Statistical Evaluation In accordance with discussions between UDEQ and GP on June 1, 2017, measured VOC concentrations from 2012 through 2017 were used to perform statistical analyses. These Theil-Sen trend analyses were performed in accordance with Section 21.3.2 of the EPA Unified Guidance using the "R" (R Core Team, 2012) script provided by EPA (Appendix C of EPA, 2009). Appendix C presents the results of the analyses. All VOC concentration trends that can be generated (i.e. there are enough detections) show a declining concentration trend (Appendix C). The upper 95th percentile ("P95") concentrations of benzene were compared to the EPA Maximum Contaminant Level (MCL). Naphthalene April 13, 2018 TETRA TECH 6 2017 Grouldwater Monitoring Report Georgia-Pacific Former Gypsum Manufacturing Facility P96 concentrations were compared to the EPA residential tapwater non-cancer screening level (SL) with a Target Hazard Index of 1 (6.1 pg/L). The P95 concentrations of ethylbenzene were compared to EPA Ingestion Screening Levels corresponding to Total Risk (TR) values of 1E-05 and 1E-06. The October measured concentrations for all constituents of potential concern (COPCs) were below their respective benchmarks (i.e. MCL, non-cancer SL, or 1E-05 TR ingestion SL). The October 2017 P95 concentrations for five of the six analyzed trends were also below the regulatory standards; only naphthalene at MW-7 had a P95 above the non-cancer SL. However, the last two samples from MW-7 (collected in 2016 and 2017) both had naphthalene concentrations below this screening level. Additionally, a predictive analysis of MW-7 naphthalene concentrations indicates that even if future concentrations are equal to the most recent sample concentration (4.41 pg/L), the P95 concentration will not drop below the non- cancer SL after numerous sampling events (see Appendix D). 2.4 Conclusions Based on results from the October 2017 groundwater monitoring event and past investigations at the Site: • Groundwater flow is toward the north and the Sevier River. • Groundwater impacts are limited to the shallow aquifer near the water table. • Phase-separated oil has been observed in a well near and downgradient of the hydraulic-oil release (MW-12); the oil is not practically recoverable from the well. • All VOC concentrations were below regulatory standards and risk-based screening levels in October 2017. • Accounting for uncertainty in the VOC trend analysis, only naphthalene at MW-7 has an upper-bound (P95) potential level above the non-cancer SL; however, the last two samples collected at that monitoring well had naphthalene concentrations below the non-cancer SL. Additionally, a predictive analysis indicates that even after numerous sampling events with the same concentrations of naphthalene that are currently present, the P95 concentration would not drop below the non-cancer SL. April 13, 2016 TETRA TECH 7 2017 Groundwater Monitoring Report Georgia-Pacific Former Gypsum Manufacturing Facdity 3 PROPOSED PATH FORWARD Based on measured groundwater quatity, estimates of future plume behavior, and an assessment of potential human health risks conducted previously by Tetra Tech (2016, 2017), active remedialion to address groundwater impacts is not warranted. Avoidance of future exposure risks can be assured through appropriate land use restrictions. 3.1 Monitored Natural Attenuation of Diesel-Related Groundwater Impacts Based on sampling results from the October 2017 sampling event, it is recommended that groundwater sampling cease at the Site. All VOC concentrations measured from the October 2017 sampling event were below regulatory standards and risk-based screening levels. Additionally, the statistical evaluation conducted on results from the October 2017 event indicated that only naphthalene at MW-7 has an upper-bound (P95) potential level above the non-cancer SL, and that the last two samples collected at MW-7 resulted in naphthalene concentrations below the non-cancer SL. A predictive analysis conducted as part of this report shows that even with numerous additional sampling events that result with naphthalene concentrations below the non-cancer SL at MW-7, the P95 concentrations will not drop below the non-cancer SL. Because it will take numerous additional sampling events to show with 95% confidence that the nonparametric Theil-Sen trend line is less than the non-cancer SL for naphthalene at MW-7, Tetra Tech proposes that sampling be discontinued at the Site and that the naphthalene concentration at MW-7 be considered below the appropriate threshold for VOCs. 3.2 Institutional Control Future use of Site groundwater as a drinking-water source should be prohibited. This can be accomplished with a restrictive covenant that becomes part of the property deed records. 4 April 13, 2018 TETRA TECH 8 2017 Grouidwater Monitoring Report Georgia-Pacific Former Gypsum Manufacturing Facility 4 REFERENCES AMEC Earth & Environmental, Inc., 2010. Site Visit Memorandum. October 4. EPA, 2009. Statistical Analysis of Groundwater Monitoring Data at RCRA Facilities—Unified Guidance. EPA Publication 530/R-09-007. March. Natresco & Associates, 2006. Soil Investigation, Hydraulic Fluid Leak. Prepared for Georgia Pacific Gypsum. Report Dated September 20, 2006. R Core Team, 2012. R: A language and environment for statistical computing. R Foundation for Statistical Computing, Vienna, Austria. ISBN 3-900051-07-0 (URL: http://www.R- projectorga Tetra Tech, 2011. Subsurface Investigation Petroleum Hydrocarbon Release. Prepared for Georgia-Pacific LLC. Report Dated September 16, 2011. 287 pp. Tetra Tech, 2012. Sampling and Analysis Plan and Quality Assurance and Control Plan. Prepared for Georgia-Pacific LLC. Report Dated October 25, 2012. Tetra Tech, 2013. Phase II Subsurface Investigation, Petroleum Hydrocarbon Release, GP Gypsum Manufacturing Facility. Technical report prepared for Georgia-Pacific LLC, August 13. Tetra Tech, 2015. GP Gypsum 2014 Groundwater Monitoring Report. Technical report submitted to David Wheeler, Utah DEQ. April 14. Tetra Tech, 2017. Groundwater Quality Evaluation Update and Source-Area Investigation/Excavation Completion Report Version 2. 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FIGURE 1 SITE LOCATION MAP SEVIER RIVER US GYPSUM PROPERTY ALMA CORD PROPERTY 9.000 OR 5.000 GALLON DIESEL UST MUNICIPAL WATER SUPPLY LINE _,„0- FUEL STATION 0" CHECK IN STATION MW5 MW15-/fr (2) 1,000 GALLON GASOLINE UST -joy-COMPANY OFFICE 1 MW4 POSSIBLE FORMER 5.000 GALLON UST EXIS11NG GAS LINE 500 GALLON GASOLINE UST M W12 MW1 (2) 10,000 GALLON DIESEL AST .0-}--APPROXIMATE LOCATION OF CLOSED LANDFARM 9,000 GALLON FUEL OIL °--0IL STORAGE EAST QUARTER CORNER OF SECTION 1 T.23 S., R.2 W., LEGEND SECTION UNE QUARTER SECTION UNE G-P GYPSUM PROPERTY BOUNDARY EXISTNG STRUCTURES FORMER STRUCTURES UNDERGROUND GAS UNE QUARTER SECTION CORNER AS NOTED MONITORMG WELL UNDERGROUND WATER UNE (APPROXIMATE LOCATION) C-D SCALE IN FEET ISISEE!!!! 0 200 TAKEN FROM JONES AND DEMILLE ENGINEERING, INC PROJECT 1106-095, DATED 12-10-12 MODIFIED BY TETRA TECH, JANUARY 2013 FEBRUARY 2018 FIGURE 2 GP GYPSUM FACILITY SITE LAYOUT GP GYPSUM, INC. 2017 Gromdwater Monitonng Report Georgia-Pacific Former Gypsum Manufactunng Facility APPENDIX A. ANALYTICAL LABORATORY REPORT 1 April 13, 2018 TETRA TECH TestAmerica THE LEADER IN ENVIRONMENTAL TESTING ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Nashville 2960 Foster Creighton Drive Nashville, TN 37204 Tel: (615)726-0177 TestAmerica Job ID: 490-139683-1 Client Project/Site: Sigurd, UT For: Tetra Tech GEO 1165 Sanctuary Parkway Suite 270 Alpharetta, Georgia 30009 Attn: Dr. Scott Simpson 4.-44 Authorized for re/ease by: 11/1/2017 3:21 :34 PM Ken Hayes, Project Manager II (615)301-5035 ken. hayes@testame rica inc. com lieview your project Tesultsihrough Have a Question. Ask The Ex ert The test results in this report meet all 2003 NELAC and 2009 TM requirements for accredited parameters, exceptions are noted in this repoit. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronical4r signed and authorized by the signatory. Electmnic signature is intended to be the legally binding equwalent of a traditionally handwntten signature. Milt us at: www.testamericainc.com Results relate only to the items tested and the sample(s) as received by the laboratory. Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd. UT Table of Contents Cover Page 1 Table of Contents 2 Sample Summary 3 Case Narrative 4 Definitions 5 Client Sample Results 6 QC Sample Results 17 QC Association 19 Chronicle 20 Method Summary 22 Certification Summary 23 Chain of Custody 24 Receipt Checklists 26 Ei TestAm erica Nashville Page 2 of 26 11/1/2017 Sample Summary Client: Tetra Tech GEO Project/Site: Sigurd, UT TestAmerica Job ID: 490-139683-1 Lab Sample ID Client Sample ID Matrix Collected Received 490-139683-1 MW4 Wa ter 10/26/17 11:00 10/28/17 09:55 490-139683-2 MW-5 Wa ter 10/26/17 0a55 10/28/17 09:56 490-139683-3 MW-6 Wa ter 10/26/17 1825 10/28/17 09:55 490-139683-4 MW-7 Wa ter 10/26/17 13:40 10/28/17 0955 490-139683-5 MW-9 Wa ter 10/26/17 15:15 10/28/17 09:55 490-139683-6 MW-12 Wa ter 10/26/17 17:55 10/28/17 09:55 490-139683-7 MW-13 Wa ter 10/26/17 17:05 10/28/17 0a55 490-139683-8 MW-15 Wa ter 10/26/17 0850 10/28/17 09:55 490-139683-9 MW-17 Wa ter 10/26/17 16:05 10/28/17 09:55 490-139683-10 Du p-1 Wa ter 10/26/17 1Z 00 10/28/17 oa55 490-139683-11 Tnp Blank Wa ter 10/26/17 00:01 10/28)17 0955 ,t q TestAmenca Nashville Page 3 of 26 11/1/2017 Case Narrative Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd, UT Job ID: 490-139683-1 Laboratory: TestAmerica Nashville Narrative Job Narrative 490-139683-1 Comments No additional comments. Receipt The samples were received on 10/28/2017 9:55 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 4.3° C. GCIMS VOA No analytical or quality issues were noted, other than those described in the Defnitions/Glossary page. VOA Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. TestAmerica Nashville Page 4 of 26 11/1/2017 Definitions/Glossary Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd, UT Qualifiers GC/MS VOA Qualifier Qualifier Description Indicates the analyte was analyzed for but not detected. Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. a Listed under the '13" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CNF Contains No Free Liquid DER Duplicate Error Ratio (normalved absolute dfference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between taro points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity EquivalentQuotient (Dioxin) TestAmerica Nashville Page 5 of 26 11/1/2017 Client Sample Results Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd, UT Client Sample ID: MW-4 Lab Sample ID: 490-139683-1 Date Collected: 10/26/17 11:00 Matrix: Water Date Received: 10/28/17 09:55 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil FaG Benzene 0.200 U 1.00 0200 ug 10/31/17 12:45 1 Ethylbenzene 0.190 U 1.00 0.190 ug/L 10/31/17 1245 1 Naphthalene 0.210 U 5.00 0.210 ug/L 10/31/17 1245 1 Toluene 0.170 U 1.00 0.170 ug/L 10/31/17 1245 1 Xylen es, Total 0.580 U 100 0.580 ug/L 10/31/17 1245 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Coil Ric 1,2-Dichloroethane-d4 (Sun) 101 70 - 130 10/31/17 1245 1 4-Bromofluorobenzene (Sun) 96 70 - 130 10/31/17 12:45 1 Dobromofluoromethane (Sun) 104 70 - 130 10/31/17 1245 1 Toluene-d8 (Sun) 94 70 - 130 10/31/17 1245 1 _ 4 TestAmerica Nashville Page 6 of 26 11/1/2017 Client Sample Results Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd, UT Client Sample ID: MVV-5 Lab Sample ID: 490-139683-2 Date Collected: 10/26/17 09:55 Matrix: Water Date Received: 10/28/17 09:55 - Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Benzene 0.200 U 1.00 0.200 ug/L 10/31/17 13:12 1 Ethylbenzene 0.190 U 1.00 0.190 ug/L 10/31/17 13:12 1 Naphthalene 0.210 U 5.00 0.210 ug/L 10/31/17 13:12 1 Toluene 0.170 U 1.00 0.170 ug/L 10/31/17 13:12 1 Xylenes, Total 0.580 U 3.00 0.580 ug/L 10/31/17 13:12 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloreethane-d4 (Sun) 101 70 - 130 10/31/17 13:12 1 4-Bromotluorobenzene (Sum) 108 70 - 130 10/31/17 1312 1 abromoikioromethane (Sun) 103 70 - 130 10/31/17 13:12 1 Toluene-d8 (Surd 98 70- 130 10/31/17 1312 1 _ TestAmerica Nashville Page 7 of 26 11/1/2017 Client Sample Results Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd, UT Client Sample ID: MVV-6 Lab Sample ID: 490-139683-3 Date Collected: 10/26/17 18:25 Matrix: Water Date Received: 10/28/17 09:55 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Dil Fac Benzene 0.200 U 1.00 0200 ug/L 10/31/17 13:38 1 Ethylbenzene 0.190 U 1.00 0.190 ug/L 10/31/17 13:38 1 Naphthalene 0210 U 5.00 0210 ug/L 10/31/17 13:38 1 Toluene 0.170 U 1.00 0.170 ug/L 10/31/17 13:38 1 Xylenes, Total 0.580 U 3.00 0.580 ug/L 10/31/17 13:38 1 Surrogate %Recovety Qualifier Limits Prepared Analyzed Dll Fac 1,2-Dichloroethane-d4 (Sun) 101 70- 130 10/31/17 13:38 1 4-Brotnofluorobenzene (Sun) 98 70 -130 10/31/17 1138 1 Dibrotnoftuoromethane (Sun) 105 70 - 130 10/31/17 13:38 1 Toluene-d8 (Sun) 102 70 - 130 10/31/17 13:38 1 4 TestAmerica Nashville Page 8 of 26 11/1/2017 Client Sample Results Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd, UT Client Sample ID: PAW-7 Lab Sample ID: 490-139683-4 Date Collected: 10/26/17 13:40 Matrix: Water Date Received: 10/28/17 09:55 - Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL PADL Unit D Prepared Analyzed Oil Fac Benzene 0.200 U 1.00 0.200 ug/L 10/31/17 14:57 1 Ethylbenzene 0.504 J 1.00 0.190 ug/L 10/31/17 14:57 1 Naphthalene 4.41 J 5.00 0.210 ug/L 10/31/17 14:57 1 Toluene 0.170 U 1.00 0.170 ug/L 10/31/17 14:57 1 Xylenes. Total 0.580 U 3.00 0.580 ug/L 10/31/17 14:57 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Pac 1,2-Dichlomethane-d4 (Sun) 100 70 - 130 10/31117 14:57 1 4-13romofluorobenzene (Sun) 101 70 - 130 10/31/17 14:57 1 Dobromoffuoromethane (Sun-) 103 70 - 130 10/31/17 14:57 1 Toluene-d8 (Sun) 101 70 - 130 10/31/17 14:57 1 _ TestAmerica Nashville Page 9 of 26 11/1/2017 Client Sample Results Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd, UT Client Sample ID: MVV-9 Lab Sample ID: 490-139683-5 Date Collected: 10/26/17 15:15 Matrix: Water Date Received: 10/28/17 09:55 - Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Dil Fac Benzene 0200 U 1.00 0.200 ug/L 10/31/17 15:24 1 Ethylbenzene 0.190 U 1.00 0.190 ug/L 10/31/17 15:24 1 Naphthalene 1.01 J 5.00 0.210 ug/L 10/31/17 15:24 1 Toluene 0.170 U 1.00 0.170 ug/L 10/31/17 15:24 1 Xylenes, Total 0.580 U 3.00 0.580 ug/L 10/31/17 15:24 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Sun) 101 70 - 130 10/31/17 15:24 1 4-Bromoiluorobenzene (Sun) 96 70 - 130 1 OP31/17 15:24 1 Dibromofkloromethane (Sun) 104 70 - 130 10/31/17 15:24 1 Toluene-d8 (Sun) se 70 - 130 10/31/17 15:24 1 _ TestAmerica Nashville Page 10 of 26 11/1/2017 Client Sample Results Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd, UT Client Sample ID: MVV-12 Lab Sample ID: 490-139683-6 Date Collected: 10/26/17 17:55 Matrix: Water Date Received: 10/28/17 09:55 - Method: 82608 - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL PADL Unit D Prepared Analyzed 011 Fac Benzene 0200 U 1.00 0.200 ug/L 10/31/17 15:50 1 Ethylbenzene 0.190 U 1.00 0.190 ug/L 10/31/17 15:50 1 Naphthalene 0.210 U 5.00 0.210 ug/L 10/31/17 15:50 1 Toluene 0.170 U 1.00 0.170 ug/L 10/31/17 15:50 1 Xylenes. Total 0.580 U 3.00 0.580 ug/L 10/31/17 15:50 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dtchloroethane-d4 (Sun) 98 70-130 10/31/17 15:50 1 4-Bmmofluorobenzene (Surr) 105 70-130 10/31/17 15:50 1 DibnDmofkioromethane (Sun) 104 70-130 10/31/17 15:50 1 Toluene-d8 (Sun) 95 70-130 10/31/17 15:50 1 _ TestAmerica Nashville Page 11 of 26 11/1/2017 Client Sample Results Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd, UT Client Sample ID: NIW-13 Lab Sample ID: 490-139683-7 Date Collected: 10/26/17 17:05 Matrix: Water Date Received: 10/28/17 09:55 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DO Fac Benzene 0.584 J 1.00 0.200 ug/L 10/31/17 16:16 1 Ethylbenzene 1.99 1.00 0.190 ug/L 10/31/17 16:16 1 Naphthalene 1.02 J 5.00 0210 ug/L 10/31/17 16:16 1 Toluene 0.170 U 1.00 0.170 ug/L 10/31/17 16:16 1 Xylenes, Total 0.580 U 3.00 0.580 ug/L 10/31/17 16:16 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Oil Ric "I ,2-Dichloroethane-d4 (Sun, 92 70 - 130 10t31/17 16:16 1 4-Bromofluorobenzene (Surd 105 70 - 130 10/31/17 16:16 1 Dibromofluoromethane (Sum) 102 70 - 130 10/31/17 16:16 1 Toluene-d8 (Surr) 100 70 - 130 10/31/17 16:16 1 4 TestAmerica Nashville Page 12 of 26 11/1/2017 Client Sample Results Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd, UT Client Sample ID: MW-15 Lab Sample ID: 490-139683-8 Date Collected: 10/26/17 08:50 Matrix: Water Date Received: 10/28/17 09:55 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MIX Unit 0 Prepared Analyzed Dil Fac Benzene 0.200 U 1.00 0.200 ug/L 10/31/17 14:05 1 Ethylbenzene 0.190 U 1.00 0.190 ug/L 10/31/17 14:05 1 Naphthalene 0.210 U 5.00 0210 ug/L 10/31/17 14:05 1 Toluene 0.170 U 1.00 0.170 ug/L 10/31/17 14:05 1 Xylen es, Total 0.580 U 3.00 0.580 ug/L 10/31/17 14:05 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1 ,2-achloroethane-d4 (Surr) 103 70 -130 1001/17 14:05 1 4-Baynciluorobenzene (Sur?) 97 70 - 130 10/31/17 14:05 1 abromofluoromethane (Surr) 105 70 - 130 10/31/17 14:05 1 Toluene-d8 (Sum) 101 70 -130 10/31/17 14:05 1 _ TestAmerica Nashville Page 13 of 26 11/1/2017 Client Sample Results Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd, UT Client Sample ID: MW-17 Lab Sample ID: 490-139683-9 Date Collected: 10/26/17 16:05 Matrix: Water Date Received: 10/28/17 09:55 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Dil Pas Benzene 0200 U 1.00 0200 ug/L 10/31/17 14:31 1 Ethylbenzene 0.190 U 1.00 0.190 ug/L 10/31/17 14:31 1 Naphthalene 0.210 U 5.00 0210 ug/L 10/31/17 14:31 1 Toluene 0.170 U 1.00 0.170 ug/L 10/31/17 14:31 1 Xylen es, Total 0380 U 3.00 0.580 ug/L 10/31/17 14:31 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Sun) 103 70 -130 10/31/1 7 14:31 1 443romolluorobenzene (Sun) 98 70 -130 10/31/17 14:31 1 Dtbromofluommethane (Sun) 105 70 - 130 10/31/17 14:31 1 Toluene-d8 (Sun) 101 70 - 130 10/31/17 14:31 1 _ TestAmerica Nashville Page 14 of 26 11/1/2017 Client Sample Results Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd, UT Client Sample ID: Dup-1 Lab Sample ID: 490-139683-10 Date Collected: 10/26/17 12:00 Matrix: Water Date Received: 10/28/17 09:55 — Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit 0 Prepared Analyzed Dil PIK Benzene 0.200 U 1.00 0.200 ug/L 10/31/17 16:42 1 Ethylbenzene 0.190 U 1.00 0.190 ug/L 10/31/17 16:42 1 Naphthalene 0.210 U 5.00 0210 ug/L 10/31/17 16:42 1 Toluene 0.170 U 1.00 0.170 ug/L 10/31/17 16:42 1 Xylen es, Total 0.580 U 3.00 0.580 ug/L 10/31/17 16:42 1 6 Surrogate %Recovery Qualifier Limits 1,2-Dichloroethane-d4 (Sun) 97 70 - 130 4-Bromofluonabenzene (Sun) 98 70 -130 Dibromofluoromefhane (Sun) 103 70 - 130 Toluene-d8 (Sun) 102 70 - 130 _ Prepared Analyzed Di! Fac 10/31117 16:42 10/31117 16:42 10131/17 16:42 1 10131117 16:42 1 TestAmerica Nashville Page 15 of 26 11/1/2017 Client Sample Results Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd, UT Client Sample ID: Trip Blank Lab Sample ID: 490-139683-11 Date Collected: 10/26/17 00:01 Matrix: Water Date Received: 10/28/17 09:55 — Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL AWL Unit D Prepared Analyzed Dil Fac Benzene 0200 U 1.00 0200 ug/L 10/31/17 12:19 1 Ethylbenzene 0.190 U 1.00 0.190 ug/L 10/31/17 1219 1 Naphthalene 0210 U 5.00 0.210 ug/L 10/31/17 1219 1 Toluene 0.170 U 1.00 0.170 ug/L 10/31/17 1219 1 Xylenes. Total 0.580 U 3.00 0.580 ug/L 10/31/17 1219 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1 ,2-Dichloroethane-d4 (Sun) 100 70 -130 10/31/17 1219 1 4-Bromofluorobenzene (Sun) 99 70-130 10/31/17 12:19 1 Dibrornoffuorornethane (Sun) 103 70 - 130 10/31/17 1219 1 Toluene-dB (Sun) 102 70 - 130 10/31/17 1219 1 _ TestAmerica Nashville Page 16 of 26 11/1/2017 QC Sample Results Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd, UT Method: 8260B - Volatile Organic Compounds (GC/MS) _ Lab Sample ID: MB 490-472175/6 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 472175 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Benzene 0.200 U 1.00 0.200 ug/L 10/31/17 11:46 1 Ethylbenzene 0.190 U 1.00 0.190 ug/L 10/31/17 11:46 1 Naphthalene 0.210 U 5.00 0.210 ug/L 10/31/17 11:46 1 Toluene 0.170 U 1.00 0.170 ug/L 10/31/17 11:46 1 Xylenes, Total 0380 U 3.00 0.580 ug/L 10/31/17 11:46 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1 ,2-Dschloroethane-d4 (Sun) 102 70 - 130 10/31/17 11:46 1 4-Bromofluorobenzene (Sun) 97 70- 130 10131/17 11:46 1 abromofluoromethane (Sun) 105 70 -130 10/31/17 11:46 1 Toluene-d8 (Sun.) 103 70- 130 10/31/17 11:46 1 - - Lab Sample ID: LCS 490-472175/3 Matrix: Water Analysis Batch: 472175 Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Benzene 50.0 52.82 ug/L 106 70 -130 Ethylbenzene 50.0 53.12 ug/L 106 70 -130 Naphthalene 50.0 53.49 ug/L 107 54 -150 Toluene 50.0 49.92 ug/L 100 70 - 130 Xylenes, Total 150 155.8 ug/L 104 70 - 132 LCS LCS Surrogate %Recovery Qualifier Limits 1,2-Dichloroethane-d4 (Surr) 107 70 -130 4-Bromoftuorobenzene (Sun) 96 70 -130 Dibromofiuoromethane (Sun) 103 70 _130 Toluene-d8 (Sun) 95 70 -130 - - Lab Sample ID: LCSD 490-472175/4 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 472175 4 Spike LCSD LCSD . %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Benzene 50.0 51.29 ug/L 103 70 - 130 3 12 Ethylbenzene 50.0 52.52 ug/L 105 70 - 130 1 12 Naphthalene 50.0 49.59 ug/L 99 54 - 150 8 15 Toluene 50.0 50.14 ug/L 100 70 - 130 0 13 Xylenes, Total 150 159.3 ug/L 106 70 - 132 2 11 LCSO LCSD Surrogate %Recovery Qualifier Limits 1 ,2-Dtchloroethane-d4 (Sun) 106 70 -130 4-Bromofluorobenzene (Sun-) 96 70 _130 Dibromoftuoromethane (Sun) 103 70 -130 Toktene-d8 (Sun) 97 70-130 _ TestAmerica Nashville Page 17 of 26 11/1/2017 QC Sample Results Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd, UT Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 490-139683-1 MS Matrix: Water Analysis Batch: 472175 Sample Sample Analyte Result Qualifier Spike Added MS MS Result Qualifier Unit Client Sample ID: MW-4 Prep Type: Total/NA %Rec. D %Rec Limits Benzene 0.200 U Ethylbenzene 0.193 U Naphthalene 0.210 U Toluene 0.170 U Xylenes, Total 0.580 U 50.0 50.0 50.0 50.0 150 55.25 55.55 46.77 53.43 166.9 ug/L ug/L ug/L ug/L ug/L 110 55- 147 111 65 - 139 94 32 - 150 107 64 - 136 111 69-132 MS MS Surrogate %Recovery Qudifier Limits 1,2-Dichlomethane-d4 (Sun) 102 70 -130 4-Bromofluorobenzene (Sun) 101 70-130 Dtbromotluoromethane (Sun) 103 70 - 130 Toluene-dB (Sun) 97 70-130 Lab Sample ID: 490-139683-1 MSD Client Sample ID: MW-4 Matrix: Water Prep Type: Total/NA Analysis Batch: 472175 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Benzene 0.200 U 50.0 55.87 ug/L 112 55 - 147 1 22 Ethylbenzene 0.193 U 50.0 55.81 ug/L 112 65-139 0 18 Naphthalene 0210 U 50.0 47.76 ug/L 96 32 - 150 2 40 Toluene 0.170 U 50.0 56.80 ug/L 114 64 -136 6 18 Xylenes, Total 0.580 U 150 172.3 ug/L 115 69-132 3 17 MSD MSD Surrogate %Recovery Qualifier Limits 1,2-Dochloroethane-d4 (Sun) 103 70 - 130 4-Bromofluorobenzene (Star) 98 70 -130 Dibromoiluoromethane (Surr) 102 70 _130 Toluene-d8 (Surd 103 70-130 TestAmerica Nashville Page 18 of 26 11/1/2017 QC Association Summary Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd, UT GC/MS VOA Analysis Batch: 472175 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 490-139683-1 MW-4 Total/NA Water 82608 490-139683-2 MW-5 Total/NA Water 82608 490-139683-3 MW-6 Total/NA Water 8260B 490-1396834 MW-7 TotaVNA Water 8260B 490-139683-5 MW-9 Total/NA Water 8260B 490-139683-6 MW-12 Total/NA Water 8260B 490-139683-7 MW-13 Total/NA Water 8260B 490-139683-8 MW-15 Total/NA Water 8260B 490-139683-9 MW-17 Total/NA Water 8260B 490-139683-10 Dup-1 Total/NA Water 8260B 490-139683-11 Trip Bank Total/NA Water 8260B MB 490-472175/6 Method Blank Total/NA Water 8260B LCS 490-472175/3 Lab Control Sample Total/NA Water 8260B LCSD 490472175/4 Lab Control Sample Dup Total/NA Water 82608 490-139683-1 MS MW-4 Total/NA Water 82608 490-139683-1 MSD MW4 Total/NA Water 8260B _ TestAmerica Nashville Page 19 of 26 11/1/2017 Lab Chronicle Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd, UT Client Sample ID: MW-4 Lab Sample ID: 490-139683-1 Date Collected: 10/26/17 11:00 Matrix: Water Date Received: 10/28/17 09:55 - Batch Batch Dil initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab _ Total/NA Analysis 8260B 1 10 mL 10 mL 472175 10/31/17 12:45 RP TAL NSH Client Sample ID: MW-5 Lab Sample ID: 490-139683-2 Date Collected: 10/26/17 09:55 Matrix: Water Date Received: 10/28/17 09:55 - Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab _ Total/NA Analysis 8260B 1 10 mL 10 mL 472175 10/31/17 13:12 RP TAL NSH Client Sample ID: MW-6 Lab Sample ID: 490-139683-3 Date Collected: 10/26/17 18:25 Matrix: Water Date Received: 10/28/17 09:55 Batch Batch Dil initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab _ Total/NA Analysis 8260B 1 10 mL 10 mL 472175 10/31/17 13:38 RP TAL NSH Client Sample ID: MW-7 Lab Sample ID: 490-139683-4 Date Collected: 10/26/17 13:40 Matrix: Water Date Received: 10/28/17 09:55 - Batch Batch Dil initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab _ TotaVNA Analysis 6260B 1 10 mL 10 mL 472175 10/31/17 14:57 RP TAL NSH Client Sample ID: MW-9 Lab Sample ID: 490-139683-5 Date Collected: 10/26/17 15:15 Matrix: Water Date Received: 10/28/17 09:55 - Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab _ Total/NA Analysis 8260e Client Sample ID: MW-12 Date Collected: 10/26/17 17:55 Date Received: 10/28/17 09:55 1 10 mL 10 mL 472175 10/31/17 15:24 RP TAL NSH 4 Lab Sample ID: 490-139683-6 Matrix: Water Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 6260B 1 10 mL 10 mL 472175 10/31/17 15:50 RP TAL NSH - TestAmerica Nashville Page 20 of 26 11/1/2017 Client Sample ID: MW-13 Date Collected: 10/26/17 17:05 Date Received: 10/28/17 09:55 Lab Sample ID: 490-139683-7 Matrix: Water Client Sample ID: MW-15 Date Collected: 10/26/17 08:50 Date Received: 10/28/17 09:55 Lab Sample ID: 490-139683-8 Matrix: Water Client Sample ID: MW-17 Date Collected: 10/26/17 16:05 Date Received: 10/28/17 09:55 Lab Sample ID: 490-139683-9 Matrix: Water Client Sample ID: Dup-1 Date Collected: 10/26/17 12:00 Date Received: 10/28/17 09:55 Lab Sample ID: 490-139683-10 Matrix: Water Total/NA Analysis 8260B 1 10 mL 10 mL 472175 10/31/17 14:05 RP TAL NSH Batch Batch Di l initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 60e 1 10 mL 10 mL 472175 10/31/17 16:42 RP TAL NSH Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 10 mL 10 mL 472175 10/31/17 16:16 RP TAL NSH Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis eaoB 1 10 mL 10 mL 472175 10/31/17 14:31 RP TAL NSH Lab Chronicle Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd, UT Client Sample ID: Trip Blank Lab Sample ID: 490-139683-11 Date Collected: 10/26/17 00:01 Matrix: Water Date Received: 10/28/17 09:55 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab TotaVNA Analysis 8260B 1 10 mL 10 mL 472175 10/31/17 12:19 RP TAL NSH Laboratory References: TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Dnve, Nashville, TN 37204, TEL (615)726-0177 TestAmerica Nashville Page 21 of 26 11/1/2017 Method Summary Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd, UT Method Method Description Protocol Laboratory 8260B Volatile Organic Compounds (GC/MS) SW846 TAL NSH Protocol References: 5W846 = 'Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Ecition, November 1986 And lts Updates. Laboratory References: TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177 TestAmerica Nashville Page 22 of 26 11/1/2017 Accreditation/Certification Summary Client: Tetra Tech GEO TestAmerica Job ID: 490-139683-1 Project/Site: Sigurd, UT Laboratory: TestAmerica Nashville The accredita tons/certifications listed below are applicable to this report [Authority Program EPA Region Identification Number Expiration Date Utah NELAP a TN00032 07-31-18 • TestAmerica Nashville Page 23 of 26 11/1/2017 (ffgrh10...NA YES...NO.. TestAmerica THE LEADER IN ENVIRONMENTAL TESTING Nashville, TN COOLER RECEIrr FORM _ 490 139683 Chen of Custody - - - - Cooler Received/Opened On 10128/2017 42/..18_5_5_ Tithe Samples Removed From Cooler t Time Samples Placed in Storage (2 Hour Window) 1. Tracking*? 1:1,24, (last 4 digits, FedEx) Courier. FedEx IR Gun ID Ramer pH Strip Lot ...•4(4— Chlorine Ship L 2. Ternperature of rep. sample or temp blank when opened: Lt3 _Degrees Celsius 3. if *ern #2 temperature fit 0°C or less, was the representative sample or temp blank frozen? YES Nale 4. Were custody seals on outside of cooler'? If yes, how many and where: 5. Were the seals intact, signed, and dated correctly? Were custody papers Inside cooler'? j codify that I canned the cooler and anewergl tiuesV_ons 14)Jitt1kh 7. Were custody seals on containers: 6.9 erk:43.1.rci intact Were these signed and dated correctly? (Oklk V.NO 8. Packing marl used? Itile";—"Jra) Plastic bag Peanuts Vermiculite Foam insert Paper Other None 9. Cooling process: Ice-peck ice (direct contact) Dry los Other Sione 10. Did all containers arrive In good condition (unbroken)? 11. Wet)e all container labels complete (#, date, signed, pros., etc)? 12. Did all container labels and tags agree with custody papers? 13a. Were VOA vials received? b. Was there any observable headspace present In any VOA Vial? Offl..NO... NA .651.140...NA 41'74(17 • fig Larger than this. 14. Was there a Trip Blank In this cooler? YES. A If muttiple coolers, sequence # I certify thg) unloggled tile cooler Inct ansvertd auestlons 7-14 (Intel) -4f4- 15a. On pres'd bottles, cid pii test strips suggest preservation reached the correct pH level? YES...NO6P (roe- 61..NO...NA ...NO...NA b. Dki the bottliklabels Indcate that the correct preservatives were used 16. Was residual chlorine present? I certify that! checked tor chlorine and pH as Per SOP and answered tteesgone.15-46 (049 17. Were custody Papers Properly filled out (Ink, signed, etc)? 18. Did you sign the custody papers in the appropriate (dace? 19. Wore correct containers used for the analysis requested? 20. Was sufficient amount of sample sent in each contalner? I certify Mat I entered this protect into LIMB and answered questions 17-20 (iella) i certify that I attached a rebel with the unique likis number to each container lintel) 21. Were there Non-Conformanco Issues at logIn?c73,10 Was a NCR* generated? BIS Broken in shipment Cooler Receipt Form.don LF-1 End of Form Revbied W2'3/17 Page 24 of 26 11/1/2017' MI NM =I MN =I MEN MN INN NM NM MN NMI NM I= 111•11 =II NM TestAmerica Nashville 290C Foster Orephmn Drive NashivItis TN 37204 Phone (615) 72e-3177 Fax ela 726-3404 Chain of Custody Record TesiAmerica r 04 tyy.10.1...NV .t Client information Sampler. cb, /...jr, 4.61b Pta Hayes, Hen Carer Tra:RiA Iwo WC lin' 490-74594-227681 Page Page 1 012 C,Ilent acne= Dr. Scutt Simpson . . eZli--3‘04/ ..106, 4 -Mat keitheyes testamencamc.ccm Compeer, Tema Tech GEO Analysts Requested Joh* Aarsta '.165 SarctUary Parkway Sik.e 270 ow Date Reeeested , . * r i5' 1 a • IS 6 2 e op . .. , ' ... . . ' 3 , 1: 15 S I.• Preveread(te Code& A -1-0L M - Hwile B As01- N - Nene C . >en Acwiate 0 -AsNa02 0 - VAC Acld P - I...4204E F - &WON 0 - NeM03 F •14eCH R - Na2S203 5 . Arrhim. 9 --rno4 1-1 Ascerbie ?ad - TSP Delecareelrate 1-1c* U -Acatme J - Ca odatur V- MCM K -EDTA VI pH 4.6 . -EDA z -carer 'Neely) other NV: Alpharetta' TAT Requested (dem: ,5-74^417114. A 0 'TAFT' State Zigr GA 0009 3 Phu.: 770-619-9650(Te ) .'" * Purchase Order ReauesMci Email' scott simpson@tetratech.com WO 5 WOO= MAW StgLIMI, ,JT .rupv.lit e900 7790 Sea. atom 'Veda! Matra? none/Note! .. 2.1=4.e ntificatinn Sample Date Sample Ti me Sample i matrix TyPe ; (C.vornp..1 a...Z:71 G=grabs) • 111.11m., C - 'PeeseMitate Cade,. A 'A ---.—. . ........a /11‘ Irlf — 4/. if:12/7 //CV di of i Water • Al 14/ —5 /0/207 6145 61w w" j LoG: 490 Arl Vii— 41 /0 12-a7 //91-6- Gui Water r‘, 139683 Al /14/ — 7 /0/21,17 I3Yo cio Wate X ,k,/,,, /5, nv Water XJ i XS" ._• INate r 3 M Pt/ — 0 104a7 00.5 610 , Wate^ All/1/ —PC * /6/7-0)? ObA Li tAi Water Xj /VI 1A/— /7 ,/04/7 4,04. CiW Water Alz447 /2610 CAW • water 1 1 Water .4 Possibie Hazard Identification 7.7 — F-1 Aron-Harem' Mamma,* =I Ain brdant Pokon B C:3 Unlmcht.1 Radloicomal Sample Disposal (A fee may be assessed ff samples are retsined longer than 1 month) LJ a Renim To Can! LDJsposal Sy Lab Archii,e Fr Months Deliverable Requested* 1, II, III, IV. Other (speciy) Special Instuctione/QC Recurements• Empty Kit lie inquishec by: Date. Tme: roc of akiereset ReLnqr.iteltd I DateiTrie , ,C ) / 1 erfu: 0 27 Received .. me P.efriquermd by: ,C Date'll ne. Corr b• Reireeirlee by ,IDEtmlime leoace^y I_ Received br /, 4Balrie. I Caepany Gtrateldy Seas lntect [kelp* Seal WI' Ayes A NO l 0.e.terTentperauire(s; 'Card 00-Ar lenarks: 0'3 Vcr 061042016 Login Sample Receipt Checklist Client: Tetra Tech GEO Job Number: 490-139683-1 Login Number: 139683 List Source: TestAmerica Nashville List Number: 1 Creator: Huskey, Adam Question Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey True meter. The cooler's custody seal, if present, is intact True Sample custody seals, if present, are intact. N/A The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample contahers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is False Headspace larger than 1/4". <6mm (1/4"). Multiphasic samples are not present True Samples do not require splitting or com positing. True Residual Chlorine Checked. N/A TestAmerica Nashville Page 26 of 26 11/1/2017 2017 Grouldwater Monitonng Report Georgia-Pacific Former Gypsum Manufacturing Facility APPENDIX B. HISTORICAL MEASURED GROUNDWATER CONCENTRATIONS April 13, 2018 TETRA TECH 1 Table 3 Groundwater Sam piing Results Parameter TPH - Oil & Grease TPH (GC/FID) High Fraction 8260B Detections Units rng/l mg/l me Method 1664A 3510C/ DRO 826013 Client Sample ID Collect Date Value ISL Tier 1 Value ISL Tier 1 Parameter Value MCL ISL Tier 1 GW-MW2 22FT 5/4/2011 NM 10 10 ND 1 10 ND GW-MW3 22FT 5/4/2011 ND 10 10 ND 1 10 ND GW-MW4 20 FT 5/5/2011 NM 10 10 ND 1 10 ND GW-MW5 11 FT 5/5/2011 NM 10 10 0.23 1 10 ND GW-MW6 22 FT 5/5/2011 ND 10 10 1 10 NM GW-51 25 FT 5/3/2011 430 10 10 N M 1 10 n-Butylbenzene 0.027 sec-Butylbenzene 0.057 tert-Butylbenzene 0.1319 Ethylbenzene 0.0024 0.7 0 7 4 l sop ropylbenzen e 0.0059 p-lscpropyltoluene 0036 Naphthalene 0.04 07 o 7 n-Pr opylbenz en e 0014 1,2,4-Trimethyibenzene 0.11 1,2,3-Tri methylb en ze ne 0.039 Xyle nes, Total 0.003 10 10 10 W- G13.2 25 FT 5/3/2011 410 10 10 N M 1 10 Benzene 0.002 0.005 acos 03 n-Butylbenzene 0.11017 Ethylbenzene 0.0(126 0.7 0.7 4 4-Methyt-2-pentanone (MlBK) 0.024 Methyl tert-butyl ether 0.001.2 0.2 az n-Prcpylbenz en e 0.0021 1,2,4-Trimethyl b en ze ne 0.012 1,2,3-Trimethyl b en ze ne 0.0015 13,5-Tri methyl b en ze ne 0.0045 Xylenes, Total 0.017 10 10 10 GW-B3 25 FT 5/3/2011 440 10 10 NM 1 10 n-Butylbenzene 0.0011 sec-Butylbenzene 0.001 Ethylbenzene 0.0028 07 a7 4 1,2,4-Trimethyl b en ze ne 0.0097 12,3-Thmethyl b en ze ne 0.0029 13,5-Trimethyi b en ze ne 0.0033 Xylenes, Total 0.0056 10 10 10 OW-B4 25 FT 5/3/2011 ND 10 10 N M 1 10 ND GW-B5 25 FT 5/3/2011 140 10 10 N M i 10 Ethyl b enzene 0.0014 G7 0.7 4 1,2,4-Tnmethy1b en ze ne 0.0047 1,23-Trimethyib en ze ne 0.0015 1,3,5-Trimethylb en ze ne 0.0017 Xylenes, Total 0.0E03 10 10 10 GW-B625 FT 5/3/2011 ND 10 10 N M 1 10 sec-Butylbenzene 0.001 Xylenes, Total 0.0053 10 10 10 GW-B725 FT 5/3/2011 NM 10 10 32 1 10 Benzene 0.0071 0.005 0.035 03 n-Butylbenzene 0.0059 sec-B utyl b en zene 0.0078 Ethylbenzene 0.043 0.7 0 7 4 l sopropyl b en zene 0.012 p-lsoprcpyltoluene 0.0071 Naphthalene 0.17 0.7 0.7 n-Prcpylbenzene 0.019 1,2,4-Trimethyl b en ze ne 0.19 1,2,3-Trimethylb en ze ne 0.1 1,3,5-Trirnethy1b en ze ne 0.03 Xylenes, Total 0.24 10 10 10 GW-13825 FT 5/4/2011 NM 10 10 ND 1 10 Nro GW-B925 FT 5/4/2011 ND 10 10 NM 1 10 ND GW-B1025 FT 5/4/2011 NM 10 10 ND 1 10 ND GW-B12 22FT 5/4/2011 NM 10 10 ND i 10 ND GW-B13 22FT 5/4/2011 ND 10 10 N M 1 10 ND GW-B1622 FT 5/5/2011 NM 98 10 10 10 10 N M Nrvl 1 1 10 10 n-Butylbenzene 11018 sec-Butylb en zen e 0.022 Ethylbenzene 0.038 0 7 0.7 4 Isopropyl b en zen e 0.016 p-lscpropyltoluene 0.047 Naphthalene 0.32 0.7 07 n-Prcpylbenzene 0.031 1,2,4-Trimethyl b en ze ne 0.3 1,23-Trimethyib en ze ne 0.13 1,3,5-Trimethylb en ze ne 0.12 Xylenes, Total n-Butylbenzene 0.21 0.0037 10 10 10 GW-B18 19 FT 5/5/2011 sec-Butylbenzene 0.012 tert-Butylbenzene 0.01 Ethylb en zene 0.001.4 0.7 0.7 4 lsopropylbenzene 0.001.8 n-Prcpylbenzene 0.0027 GW-DUP02 MW9 B30 08-Dec-12 GW-MW11 MW11 B38 09-Dec-12 GW-DUP03 MW11 B38 09-Dec-12 GW-MW12 MW12 B33 09-Dec-12 3.8 J ND 0.34 J ND 4.14 J 1 ND Diesel No Pattern ND ND ND No Pattern ND 0.78 J 0.78 J Oil 0.4 J I ND 1.8 ND ND ND 3.1 ND ND ND ND ND ND 0.37 J ND ND ND ND ND ND 0.69 J ND ND ND 0.58 J ND 0.58 J 0.86 J Table 5.1 Laboratory Analytical Results - Water (TPH-DRO and VOCs) GP Gypsum Phase!! Site Investigation Sample ID GW-MW2 GW-MW3 GW-MW4 GW-MW6 GW-MW7 GW-MW8 GW-MW9 Monitoring Well ID MW2 MW3 MW4 MW6 MW7 MW8 MW9 Boring ID B11 B10 B17 B21 B25 B28 B30 Sample Date 08-Dec-12 09-Dec-12 08-Dec-12 09-Dec-12 08-Dec-12 08-Dec-12 08-Dec-12 Analyte Units ISLI Tier 1' C10-C20 MG/L No ISL No Tier 1 ND ND ND ND 9.4 0.57 J 9.6 J C20-C28 MG/L No ISL No Tier 1 ND ND ND ND 1.1 ND 1 J Total TPH-DRO2 MG/L 1 10 ND ND ND ND 10.5 0.57 10.6 J Pattern3 No Pattern No Pattern No Pattern No Pattern Diesel No Pattern Diesel EPA RSL - Tapwater MCL BENZENE UG/L 0.39 5 0.31 J ND ND ND ND ND 0.64 J TOLUENE UG/L 860 1000 ND ND 0.31 J ND ND ND ND l ETHYLBENZEN UG/L 1.3 40 0.35 J 0.4 J ND ND 5.8 0.36 J 2.8 l M+P-XYLENE UG/L 1904 No MCL 0.76 J 0.84 J ND ND ND ND ND O-XYLENE UG/L 190 No MCL ND ND ND ND 1.1 ND ND TOTAL XYLENE UG/L 190 10000 0.76 0.84 ND ND 1.1 ND ND NAPHTHALENE UG/L 0.14 No MCL 0.81 J 1.1 ND 0.32 J 26 0.66 J 4.6 Sample ID Monitoring Well ID Boring ID Sample Date Analyte C10-C20 C20-C28 Units MG/L MG/L !SC No ISL No ISL Tier 12 No Tier 1 No Tier 1 GW-MW13 MW13 B35 08-Dec-12 13 2 GW-MW14 MW14 B40 09-Dec-12 ND ND GW-MW16 MW16 B42 17-Dec-12 ND ND GW-DUP04 MW16 B42 17-Dec-12 ND ND GW-MW17 MW17 B43 08-Dec-12 1.7 J 0.21 J GW-B26 NA B26 07-Dec-12 ND ND GW-B27 NA B27 06-Dec-12 ND 0.2 J GW-B34 NA B34 06-Dec-12 9.3 J 4 J GW-B36 NA B36 07-Dec-12 200 J 19 J GW-B37 NA B37 06-Dec-12 77 J 11 J Total TPH-DRO3 MG/L 1 10 /5 ND ND ND j 1.91 J l ND 0.2 13.3 J l 219 J l 88 J Pattern EPA RSL - Tapwater MCL Diesel No Pattern No Pattern No Pattern Diesel No Pattern No Pattern Diesel and Oil Diesel and Oil Diesel BENZENE UG/L 0.39 5 27 ND 0.37 J 0.31 J l 0.43 J l 0.32 J ND l 0.43 J 0.47 J 0.43 J TOLUENE ETHYLBENZENE M+P-XYLENE O-XYLENE TOTAL XYLENEE UG/L UG/L UG/L UG/L UG/L 860 1.3 1904 190 190 1000 40 No MCL No MCL 10000 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.31 J 0.64 J ND 0.36 J ND ND ND 0.36 J ND ND ND ND ND ND 0.32 J ND ND ND ND 0.36 J ND 1.1 1.1 0.43 J 1.53 63 11 140 9.8 149.8 0.34 J 2.3 2.64 NAPHTHALENE UG/L 0.14 No MCL 120 l 0.72 J l ND ND l 3.3 l ND l ND ND l 6.4 l 3.6 Notes: Only groundwater samples with at least one detection are listed 1 - Levels typically used by the DMsion of Response and Remediation (DERR) to evaluate petroleum hydrocarbon releases from underground storage tanks. These values are presented to provide an approximate cleanup goal for reference purposes only. 2 - Sum of C10-C20 and C20-C28 ranges 3 - As reported by ALS Environmental 4 - RSL for m-xylene and p-xylene J - Estimated Value EPA RSL - Environmental Protection Agency Regional Screening Level BOLD -Value exceeds ISL or EPA tapwater RSL -Value exceeds Tier 1 level or EPA MCL IALIC MN NMI I= MI MN =I I= NM NM NM NM in MI MI MOM— NM NM Table 5.2 Laboratory Analytical Results - Water (SVOCs) GP Gypsum Phase II Site Investigation sample ID GW-MW7 GW- MW8 GW -MW9 GW-DUP 02 GW-MW13 GW- MW17 Monitoring Well ID MW7 MW8 MW9 MW9 MW13 MW17 Boring ID B25 B28 B30 B30 B35 B43 Sample Date 08- Dec- 12 08-Dec- 12 08 -Dec-12 08- Dec- 12 08-Dec- 12 08-Dec-12 Analyte Units EPA RSL - Tapwater MCL 1,1'-BIPHENYL UG/L 0.83 No MCL 18 14 J I 21 I 19 29 11 J 2,4-DIMETHYLPHENOL UGIL 270 No MCL ND ND ND ND 3.3 J ND 2-METHYLNAPHTHALENE UG/L 27 No MCL 57 ND 8.1 7.4 r 110 19 J ACENAPHTHENE UG/L 400 No MCL 9 3.3 J 8.9 7.8 8.6 6.1 J ANTHRACENE UG/L 1300 No MCL ND ND 3.3 J ND ND ND BENZALDEHYDE UG/L 1500 No MCL 18 ND ND ND ND ND CARBAZOLE UG/L No RSL No MCL ND ND ND ND 14 ND DIBENZOFURAN UG/L 5.8 No MCL 6.4 ND 5.6 4.8 ND 3.7 J DIETHYL PHTHALATE UG/L 11000 No MCL ND ND ND ND 7.5 ND FLUORENE UG/L 220 No MCL 15 6.3 J 13 12 15 11 J NAPHTHALENE UG/L 0.14 No MCL 29 ND ND ND l 110 ND PHENANTHRENE UG/L No RSL No MCL 20 9.2 J 23 17 17 23 J Notes: Only groundwater samples with at least one detection are listed Only analytes detected in at least one groundwater sample are listed. J - Estimated Value EPA RSL - Environmental Protection Agency Regional Screening Level Primary MCL - National Primary Drinking Water Maximum Contaminant Level BOLD - Value exceeds EPA Tapwater RSL BOLD Notes: J - Estimated Value EPA RSL - Environmental Protection Agency Regional Screening Level Primary MCL - National Primary Drinking Water Maximum Contaminant Level 1 - Chromium RSL is for Chromium III 2 - Chromium MCL is for Total Chromium 3 - National Secondary Drinking Water (NSDW) Standard - Value exceeds MCL - Value exceeds NSDW Standard Table 5.3 Laboratory Analytical Results - Water (Metals) GP Gypsum Phase II Site Investigation Sample ID GW-MW11 GW-DUP03 GW-MW12 GW-MW13 Monitoring Well ID MW11 MW11 MW12 MW13 Boring ID B38 B38 B33 B35 Sample Date 09-Dec-12 09-Dec-12 09-Dec-12 08-Dec-12 Analyte Units MCL ALUMINUM UG/L 50-200J 1200 I 270 ' 190 J 800 ANTIMONY UG/L 6 ND ND ND ND ARSENIC UG/L 10 ND 7 J 14 7.2 J BARIUM UG/L 2000 58 J 27 J 31 J 160 BERYLLIUM UG/L 4 ND ND ND ND CADMIUM UG/L 5 ND ND ND ND CALCIUM UG/L No MCL 110000 100000 32000 340000 CHROMIUM UG/L 1002 ND ND ND 0.81 J COBALT UG/L No MCL ND ND ND ND COPPER UG/L 1300 ND ND ND ND IRON UG/L 300 840 I 240 170 l 8000 LEAD UG/L 15 1.4 J 0.99 J ND ND MAGNESIUM UG/L No MCL 28000 26000 8100 110000 MANGANESE UG/L 504 72 1 44 8.8 J 870 NICKEL UG/L No MCL ND ND ND 2.4 J POTASSIUM UG/L No MCL 4800 J 4100 2800 14000 SELENIUM UG/L 50 ND ND ND ND SILVER UG/L 0.13 ND ND ND ND SODIUM UG/L No MCL 82000 79000 89000 600000 THALLIUM UG/L 2 ND ND ND ND VANADIUM UG/L No MCL 12 12 19 2.6 J ZINC UG/L 50003 ND ND ND 8.2 J MERCURY UG/L 2 ND ND ND ND ITALIC 1 1 1 I I I l i 1 I 1 I 1 I i I i 1 1 Table 2 LaboratOry Analytical Res ullS GP Gypsum GroundWater Monitoring Sample ID GW-MW2 GW- MW2 OAQC #2 MW-2 MW-24 GW-MW5 GVV- MW5 MW-5 MW-5` GW-MW6 GW- MW6 MW-6 MW-64 tvlonitoring Well ID MW2 MW2 MW 2 MW2 MW 2 MWS MW5 MW5 MW5 MW6 MW6 MW6 MW6 Sample Date Ana lyte Units lSLi Tier J.' 8-Dec-12 3 0-May-14 30-May-14 29-Oct-14 29-Oct-14 8-D e c-12 29-May-14 29-Oct-14 29-Oct-14 9-Dec-12 30-May-14 30-Oct-14 300ct-14 C10-C20 rng/L No ISL No Tier 1 ND ND ND ND ND 0 24 1 Q705 ND ND ND C20-C28 rng/L No ISL No Tier 1 ND ND ND ND ND ND Q138 ND ND ND Total TPH-DRO2 mg/L 1 10 ND ND ND ND ND Q24 (1843 ND ND ND Patter ni No Pattern No Pattern No Pattern No Pattern No Pattern No Pattern Diesel N o Pattern No Pattern N o Pattern EPA FS L - VOCS Ta pwater Primary MCL BENZENE pg/L Q39 5 a31 .1 ND ND ND ND ND ND ND ND ND TOLUENE pg/L 860 1C00 ND ND Q31 1 ND ND ND ND ND ND ND ETHYLBENZENE pg/L 13 40 035 1 ND ND ND ND ND ND ND ND ND IV14-P -XYLENE pg/L 190 No ma Q 76 1 ND ND ND ND ND ND O-XYLENE pgfL 190 No ma ND ND ND ND ND ND ND TOTAL XY LEN E S pg/L 190 10000 -- - ND ND ND ND NAPHTHALENE pat Q14 No ma 081 .1 0.761 0.57 J ND ND ND ND 0.32J ND ND SVOCs 2-METHYLNAPHTHALENE 24-DIMETHYLPHENOL NAPHTHALENE ACENAPHTHYLENE ACENAPHTHENE DIBENZOFURAN DIETHYL PHTHALATE FLUORENE PHENANTHRENE AN THRACE NE BIS(2-ETHYLHEXYL)P HTHALATE BENZALDE HYDE µg/L pg/L pg/L pg/L pg/L pg/L pg/L pg/L pg/L pg/L pg/L pg/L 27 36 Q14 No RSL 4C0 5 8 15C0 220 No RSL 180 5 6 190 No ma No ma No ma No ma No ma No Ma No Ma No ma No ma No Ma No MCL No Ma ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND CARBAZOLE CAPROLACTAM PYRENE la-BIPHENYL µg/L pg/L pg,/L pg/L No RSL 990 12 Q83 No Ma No ma No ma No ma ND ND ND ND ND ND ND ND METALS ALUMINUM pg/L 16C00 No Ma 66000 22000 ND ND 19000 ND ND 260000 ND ND ANTIMONY pg/L 6 6 ND 111 ND ND ND ND ND 8 7 I ND ND ARSENIC pet 0 045 10 34 95 13.4 16.8 19 ND 10 2 97 ND ND BARIUM pg/L 380 20 860 3900 307 32 4 470 37 9 39 8 9600 24 1 25 1 BERYLLIUM µg/L 2 5 4 43 1 17 ND ND 1.61 ND ND 16 ND ND CADMIUM pg/L 6 9 5 ND ND ND ND ND ND ND ND ND ND CALCIUM pg/L No RSL No ma 290000 44000 36803 35300 670000 372000 367003 1900000 529C0 51500 CHROMIUM µg/L No RSL 100 100 410 ND ND /4 ND ND 270 ND ND COBALT pat 4 7 No Ma 20 SO ND ND 71 ND ND 110 ND ND COPPER pg/L 620 1300 65 290 ND ND 10 ND ND 300 ND ND RON µg/L 11C00 No Ma 56000 230000 ND ND 18000 963 980 220000 ND ND LEAD µg/L No RSL 15 41 130 ND ND 22 ND ND 140 ND ND MAGNESIUM µg/L No RSL No Ma 48000 190000 9950 993 0 46000 172C0 17700 200000 13903 13903 MANGANESE µg,/L 320 No Ma 1300 6200 ND ND 2100 341 334 7600 ND ND NICKEL pg/L 3 CO No Ma 39 160 ND ND 5 1 ND ND 150 ND ND POTASS UM pg/L No RSL No ma 28000 88000 313 0 3340 31000 22703 23800 89000 3010 3190 SELENIUM µg/L 78 50 ND ND ND ND ND ND ND ND ND ND SILVER µg/L 9 4 No Ma ND ND ND ND ND ND ND ND ND ND SODIUM µg/L No RSL No Ma 12000) 150000 114000 11SOCO 140000 223030 223003 130000 112C00 112000 THALLIUM pg/L (116 2 44 3 8181 ND ND 631 ND ND ND ND ND VANADIUM pet 78 No ma 140 480 26 4 29 8 50 ND ND 470 ND ND ZINC pg/L 47C0 No ma 170 .760 ND ND 52 ND ND 580 AID ND MERCURY µg/L (163 2 ND 0153 ND ND ND ND ND 0.15 .1 ND ND Notes Only analytes detected in at least one well are hsted 1 - Levels typically used by the Division of Response and Remediation (DERR) to evaluate petroleum hydrocarbon releases from underground storage tanks These values are presented to provide an approximate cleanup goal for reference purposes onty 2 - Sum of C10-C20 and C20-C28 ranges 3 -As reported by ALS Environmental 4 - Samples were field filtered. all other samples were unfiltered J - Estimated Value - Result is less than the reporting limit but greater than the method ddection limit (MOL) EPA RSL - Environmental Protection Agency Regional Screening Level BOLD BOLD ITALIC BLUE R-AUG -Value exceeds ISL or EPA tapwater RSL -Value exceeds Tier 1 level or EPA MCL - May 201 4 metals concentrations were anomalously high in general compared to prior and later (Oct 2014) concentrations Therefore. May metals concentrahors are deem ed unrepresentatne of site conditions Table 2 Laboratory Analytical Results GP Gypsum Groundwater Monitoring Sample ID Monitoring Well ID Sample Date Ana lyte Units ISL.' Tier 1' C10-C20 rng/L No ISL No Tier 1 C20-C28 rng/L No ISL No Tier 1 Total 1PH-DRO2 rng/L 1 10 Pattern' EPA R5L- VOCS Ta parater Primary MCL BENZENE pg/L Q39 5 TOLUENE pg/L 860 1000 ETHYLBENZENE pg/L 1 3 40 M-I-P-XYLENE pg/L 190 No ma O-XYLENE pg/L 190 No ma TOTAL XYLEN ES pg/L 190 10000 NAPHTHALENE pg/L 014 No ma SV005', 2-METHYLNAPHTHALENE pg/L 27 No MCI. Z4DIMETHYLPHENOL pg/L 36 No ma NAPHTHALENE pg/L 014 No ma ACENAPHTHYLENE pg/L No RSL No ma ACENAPHTHENE pg/L 403 No MCL DIBENZOFURAN pg/L 5 8 No ma DIETHYL PHTHALATE pg/L 1500 No ma FLUORENE pg/L 220 No ma PHENANTHRENE pg/L No RSL No MCL ANTHRACE NE pg/L 180 No ma 1315(2-ET HYLHEXYL)PHTHALAT E pg/L 5 6 No MCL BENZALDE HYDE pg/L 190 No ma CARBAZOLE pg/L No RSL No ma CAPROLACTAM pg/L 990 No MCL PYRENE pg/L 12 No ma 1,1-BIPHENYL pg/L 083 No ma METAIS ALUMINUM pg/L 16030 No ma ANTIMONY pg/L 6 6 ARSENIC pg/L 0 045 10 BARIUM pg/L 380 2030 BERYLLIUM pg/L 2 5 4 CADMIUM pg,/L 6 9 5 CALCIUM pg,/L No RSL No ma CHROMIUM pg/L No RSL 100 COBALT pg/L 4 7 No MCL COPPER pg/L 620 1300 IRON pg/L 11030 No MCL LEAD pg/L No RSL 15 MAGNESIUM pg/L No RSL No MCL MANGANESE pg,/L 320 No ma NICKEL pg/L 303 No MCL POTASSIUM pgJL No RSL No ma SELENIUM pg/L 78 50 SILVER pg/L 9 4 No ma SODIUM pg/L No RSL No ma THALLIUM µg/L 016 2 VANADIUM pg/L 78 No MCL ZINC pg/L 4703 No MCL MERCURY ;Agit 063 2 GW-MW7 GW-MW7 (0111-7 MW-7' GW-MW8 GW-MW9 GW-DUP02 GW -MW9 ()AOC #1 MW-9 OACtC#1 MW-94 OA QC #1` GW-MW11 GW-DU KB GW -MW11 MW-11 MW-11' MW7 MW7 MW7 MW7 MW8 MW9 MW9 MW 9 MW9 MW9 MW9 MW9 MW9 MW11 MW11 MW11 MW11 MW11 8-Dec-12 29-May-14 30-Oct-14 3 0-Oct-14 8-Dec-12 8-Dec-12 9-Dec-12 29-May-14 29-May-14 29-Oct-14 29-Oct-14 29-Oct-14 29-Oct-14 9-Dec-12 9-Dec-12 30-May-14 29-Oct-14 29-Oct-14 9 4 5 3 49 0 57 1 9 6 3 8 . , 2 6 3 1 . 12 25 8 ND ND ND ND 1 1 0 83 0 305 ND 1 0 34 1 045 J 0 54 J 1 04 1 9 ND ND ND ND 20.5 5.83 3.795 057 10.6 4.14 3.05 3.64 1104 27.7 ND ND ND ND Diesel Diesel Diesel No Pattern Diesel Diesel Diesel Diesel Diesel Diesel No Pattern No Pattern No Pattern NoPattern ND ND ND ND 0.641 0.4.1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0 31 1 ND 5.8 3.9 2.51 036 1 2.8 18 093 1 0 93 1 ND ND ND ND ND ND ND ND ND ND ND ND ND -- - ND ND ND -- 1 1 0 521 ND ND ND ND ND -- - ND ND ND -- 0 52 ND ND -- -- ND ND ND -- -- -- ND 26 22 ND 0.66 .1 4.6 3.1 3.8 4.1 ND ND 0.37 I 0.69 I ND ND 57 6 4 3 13 ND 8 1 7 4 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 5 6 ND ND ND ND ND 9 ND 53 3 3 1 8 9 7 8 ND 8 1 309 13 4 ND ND ND ND 6.4 3 81 ND ND 5 6 4 8 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 15 22 9 17 6 3 13 12 19 10 ND 25 7 ND ND ND ND 20 39 4 17 9 2 23 17 16 8 147 34 4 ND ND ND ND ND 9 6 ND ND 3 3 1 ND 3 11 ND 6 34 ND ND ND ND ND ND ND 11.7 ND ND ND ND ND 11.5 ND ND ND ND ND 18 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 180 ND ND ND ND ND ND ND ND ND ND ND ND 7 39 2 17 ND ND ND ND 18 ND ND 14 21 19 ND ND 32.1 133 ND ND ND ND 26000 ND ND 4600 /.1000 ND ND ND ND 1200 270 280000 1970 588 ND ND ND NO NO ND ND ND ND ND ND 8.71 ND ND 12 ND ND ND NO ND ND ND ND ND 76 90 ND 10.2 1400 467 487 19 0 4 60 60 2 62 5 63 3 61 9 58 1 2713 12000 71 4 33 9 1.8 ND ND NO ND ND ND ND ND ND ND 19 ND fJD ND ND ND ND ND ND ND ND ND ND ND ND 1 ND 130000 27700 26703 /90000 230000 85203 83503 84300 87103 nom) mocoo 30c12000 191000 19COCO 28 ND ND 62 1 12 ND ND ND ND ND ND 290 ND ND 9.5 1 ND ND 150 1.71 ND ND ND ND ND ND 85 ND ND 29 ND ND ND 9.2 i ND ND ND ND ND ND 310 ND ND 22000 ND ND 4 600 9500 1060 113 0 1060 1100 840 240 240000 1310 517 28 ND 6.9 14 ND 1170 ND ND 1 4 .1 0998 140 ND ND 39 X0 21100 21103 67000 73000 48400 48600 49000 50103 28000 26000 220000 47100 47700 620 70 6 663 430 550 820 300 310 327 72 44 6600 302 26 4 161 ND ND .181 8.21 ND ND ND ND ND ND 140 ND ND 17000 3720 3 870 7300 10000 4620 4660 4840 4790 4800 4100 120000 5080 4720 ND ND ND ND ND ND ND ND ND ND ND NO ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 350000 333 OM 333000 220000 220700 273000 276000 274000 284000 82030 79000 110000 96300 97600 ND ND ND NO ND ' ND ND ND ND ND ND ND ND ND 57 ND ND 101 22 ND ND ND ND 12 12 480 ND ND 65 ND ND 151 22 ND ND ND ND ND ND 610 ND ND ND ND ND ND ND ND ND ND ND ND ND 0072 1 ND ND Notes Only analytes detected in at least one well are hsted 1 - Levels typically used by the Division of Response and Remediation (DER R) to evaluate petroleum hydrocarbon releases from underground storage tanks These values are pres ented to provide an approximate cleanup goal f or reference purposes only 2 - Sum of C10-C20 and C20-C28 ranges 3 - As reported by ALS Environmental 4 - Samples were field filtered. all other samples were unfiltered J - Estimated Value - R es utt s less than the reporting limit but greater tha ri the method detection limit (MDL) EPA RSL - Environmental Protection Agency Regional Screening Level BOLD -Value exceeds ISL or EPA tapwater RSL - Value exceeds Tier 1 level or EPA MCL - May 201 4 metab concentrations were anomalously high in general cornpared to prior and later (0 d 2014) concentrations Therefore. May m etals concentrations are deemed unrepresentative of site conditions 80L0 ITALIC LUE 1TAL7C Table 2 Laboratory Analytical Itesult5 GP Gyp5um Groundwater MOnitOring Sample ID Monitoring Well ID Sample Date Ana lyte Units is Tier C10-C20 rrigh No ISL No Tier 1 C20-C28 n1g/L No ISL No Tier 1 Total TPH-DRO' mg/L 1 10 Pattern' EPA RSL- VOCs Ta water Primary MCL BENZENE ugh Q39 5 TOLUENE ug/L 860 1030 ETHYLBENZENE ugh 13 40 -XYLENE ugh 190 No Ma O-XYLENE pg/L 190 No ma TOTAL XYLEN ES pg/L 190 10003 NAPHTHALENE ugh 014 No ma 6VOCs , 2-METHYLNAPHTHALENE pg/L 27 No MCL Z4-DIMETHYLPHENOL pg/L 36 No ma NAPHTHALENE pg/L 0.14 No Ma ACENAPHTHYLENE pg/L No RSL No Ma ACENAPHTHENE pg/L 400 No ma DIBEN ZOFURAN pg/L 5 8 No ma DIETHYL PHTHALATE pg/L 15C0 No Ma FLUORENE pet. 220 No Ma PHENANTHRENE pg/L No RSL No Ma ANTHRACE NE pg/L 180 No ma BIS(2-ETHYLHEXYL(PHTHALATE pg/L 5 6 No Ma BENZALDE HYDE pg/L 190 No ma CARBAZOLE pg,/L No RSL No ma CAP ROLACTAM pg/L 990 No Ma PYRENE pg/L 12 No ma 3., r-BIPHENYL pg/L 083 No ma METALS ALUMINUM pg/L 16030 No ma ANTIMONY pg/L 6 6 ARSENIC pg/L 0 045 10 BARIUM pg/L 380 2030 BERYLLIUM pg/L 2 5 4 CADMIUM pg/L 6 9 5 CALCIUM pg/L No RSL No Ma CHROMIUM pg/L No RSL 100 COBALT pg/L 4 7 No ma COPPER pg/L 620 1300 IRON ug,/L 11030 No Ma LEAD pg/L No RSL 15 MAGNESIUM pg/L No RSL No ma MANGANESE pg/L 320 No Ma NICKEL pg/L 3 CO No ma POTASSIUM pg/L No RSL No ma SELENIUM pie/L 78 50 SILVER pg/L 9 4 No ma SODIUM pg,/L No RSL No ma THALLIUM pg/L 016 2 VANADIUM pg/L 78 No ma ZINC pg/L 4703 No ma MERCURY pg/L 063 2 Notes Only analytes detected in at least one well are listed 1 - Levels typically used by the Drii ision of Response and R emediation (DERR) to evaluate petroleum hydrocarbon releases from underground storage tanks These values are ores ente d to provide an approximate cleanup goal for reference purposes only 2 - Sum of C10-C20 and C20-C28 ranges 3 - As reported by ALS Environmental 4 - Samples we re field filtered, all other samples were untittered J - Estimated Value - Result a less than the reporting limit but greater than the method detection lim d (MOL) EPA RSL - Environmental Protection Agency Regional Screening Level GW-MW12 GW- MW12 MW-12 MW-12` GW-MW13 GW-MW13 MVV-13 MW-13' GW-MW14 GW- MW14 MW-14 MW-14` GW-MW15 GYV -MW15 MW-15 MW-15' MW12 MW12 MW12 MW12 MW13 MW13 MW13 MW13 MW14 MW14 MW14 MW14 MW15 MW15 MW15 MW15 9-Dec-12 30-May-14 30-Oct-14 3 DOct-14 8-D ec-12 29-May-14 28-Oct-14 28-Oct-14 9-De c-12 29-May-14 29-Oct-14 29-Oct-14 Dec-12 29-May-14 28-Oct-14 28-Oct-14 „ ND ND 0 249 13 4 8 4 42 ND ND ND ND ND ND 078 0481 0 139 2 0 94 0 598 ND ND ND ND ND ND 078 0 48 0 388 .15 5.74 53128 ND ND ND ND ND ND Mctor Oil No Pattern Diesel Diesel Diesel Diesel No Pattern N o Pattern No Pattern No Pattern No Pattern No Pattern ND ND ND 27 3.9 6.06 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 63 7 2 32.7 ND ND ND ND ND ND Q581 ND 140 2 3 ND ND ND ND ND ND 9 8 ND ND ND ND ND Q58 ND 149 8 2 3 4 92 ND ND ND ND 0.86 1 ND ND 120 9.4 8.98 0.721 ND ND ND ND ND ND ND ND 110 ND ND ND ND ND ND ND ND ND ND ND 3 3 1 ND ND ND ND ND ND ND ND ND ND ND ND 9.1 9.79 ND ND ND ND ND ND ND ND ND ND 4 3 1 2 55 ND ND ND ND ND ND ND ND ND 8 6 22 12 7 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 7 5 ND ND ND ND ND ND ND ND ND ND ND 15 34 20 1 ND ND ND ND ND ND ND ND ND 17 59 9 47 ND ND ND ND ND ND ND ND ND ND 7 7 ND ND ND ND ND ND ND ND ND 13.7 ND ND ND ND AID 212 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 14 10 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 5 1 ND ND ND ND ND ND ND ND ND ND 29 92 31.7 ND ND ND ND ND ND 190.1 3200 ND ND sco 3 700000 ND ND 750000 ND ND 64000 148 ND ND ND ND ND ND 77 ND ND 25 ND ND ND ND ND 24 9.6 ND 12.4 7.2 420 ND ND 270 16.2 13.9 32 ND ND 31 1 58 1 31 8 33 2 160 106000 240 253 23000 20 20 8 1500 29 5 25 9 ND ND ND ND ND 120 ND ND 43 ND ND 4.3 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 32a)0 38000 33900 33103 340303 11000000 41600 40803 4200000 19703 19030 550G00 6980 71500 ND 4.6 1 ND ND 0 81 1 2000 ND ND 890 ND ND 53 ND ND ND ND ND ND ND 780 ND ND 210 ND ND 18 ND ND ND ND ND ND ND 2400 ND ND 800 ND ND 63 71 9 ND 170 1900 ND ND 8030 2700000 ND ND 630000 ND ND 57000 118 ND ND 6.3 ND ND ND 1300 ND ND 350 ND ND 40 1080 ND 810 9500 8910 8903 110000 1200000 17000 17103 470000 2850 2830 82000 2s800 26400 8 81 ND ND 870 49000 203 202 46000 27 7 25 2 1800 ND ND ND ND ND 2 4 1100 ND EID 400 ND ND 32 ND ND 2800 4500 2670 2820 14000 5501200 3 090 3340 240000 3170 3290 25000 4750 4920 ND ND ND ND ND 80 ND ND ND ND ND ND ND ND ND 80 ND ND ND ND ND ND ND ND ND 60 ND ND 89000 100000 104000 104am 600000 440000 345000 346000 210000 188000 188030 320000 321000 33 moo ND ND ND ND ND ND ND ND ND ND ND 51 ND ND 19 24 ND ND 2 61 3300 ND ND 970 24 5 23 8 140 ND ND ND ND ND ND 8 21 4300 ND ND 2700 ND ND 170 ND ND ND NO ND ND ND 0.77 ND ND 0.27 ND ND ND ND ND BOLD BOLD ITALIC BLUE 1TAL1C -Value exceeds ISL or EPA tapwater RSL -Value exceeds Tier 1 level or EPA MCL - May 201 4 metaa concentrations were anom alously high in general compared to prior and later (Oct 2014) concentrations Therefore. May metals concentrations are deem ed unrepresentative 01 site con drt ions Table 2 Laboratory Ana lytital Results GP Gypsum GrOunclWater Monitoring Sample ID Monitoring Well ID Sample Date Ana lyte Units 151.1 Tier C10-C20 rrig/L No ISL No Tier 1 C20-C28 rng/L No ISL No Tier 1 Total TPH-DROi rng/L 1 10 Patterni EPA RSL - VOCs Ta water Primary MC L BENZENE ugh Q39 5 TOLUENE ugh. 860 1COO ETHYLBENZENE ugh 1 3 40 M-i-P-XYLENE ug/L 190 No Ma O-XYLENE ugh 190 No Ma TOTAL XYLEN ES µg/L 190 10000 NAPHTHALENE pg/L 014 No MCI. SVOCS „ 2-METHYLNAPHTHALENE pg/L 27 No ma 2,4-DIMETHYLPHENOL pg/L 36 No ma NAPHTHALENE pg/L 014 No ma ACENAPHTHYLENE pg/L No RSL No ma ACENAPHTHENE µg/L 4o2 No ma DIBENZOFURAN pg/L 5 8 No ma DIETHYL PHTHALATE pg/L 15C0 No Ma FLUORENE pg/I. 220 No ma PHENANTHRENE pet. No RSL No ma ANTHRACE NE pg/L 180 No ma BIS(2-ETHYLHEXYL)PHTHALATE pg/L 5 6 No ma BENZALDEHYDE pg/L 190 No ma CARBAZOLE pg,/L No RSL No Ma CAPROLACTAM pg/L 990 No ma PYRENE pg/L 12 No ma 1,3:-BIPHENYL pg/L 083 No ma METALS ALUMINUM pg/L 16030 No ma ANTIMONY pg/L 6 6 ARSENIC pg/L 0 045 10 BARIUM pg/L 380 2030 BERYLLIUM pg/L 2 5 4 CADMIUM pg/I. 6 9 5 CALCIUM pg/L No RSL No Ma CHROMIUM pg/L No RSL 100 COBALT pg/L 4 7 No Ma COPPER pg/L 620 1300 RON pg/L 11C00 No sna. LEAD pg/L No RSL 15 MAGNESIUM pg/L No RSL No ma MANGANESE pg,/L 320 No ma NICKEL pg/L 303 No ma POTASSIUM pg/L No RSL No ma SELENIUM pet_ 78 50 SILVER pg/L 9 4 No ma SODIUM pg/L No RSL No Ma THALLIUM pg/L 016 '2 VANADIUM pg/L 78 No ma ZINC pg/L 4703 No MCL MERCURY pg/L 063 2 Notes Only analytes detected in at least one well are listed 1 - Levels typically used by the DIV sion of Response and Remediation (DERR) to evaluate petroleum hydrocarbon releases from underground storage tanks These values are presented to provide an approximate cleanup goal for reference pu rpcs es only 2 - Sum of C10-C20 and C20-028 ranges 3 -As reported by ALS Environmental 4 - Samples we re fi eld filtered. all other samples were unfiltered J - Estimated V alue - Result s less than the reporting limrt but greater than the method detection hm it IMDL) EPA RSL - Environmental Protedion Agency Regional Screening Level GW-MW16 GW-DUP04 GW-MW16 MW-16 QAQC 62 MW-16` °AOC #24 GW-MW17 GW-MW17 MW-17 MVV-171 MW16 MW16 MW16 MW16 MW16 MW16 M4V16 MW17 MW17 MW17 MW17 17-Dec-12 17-Dec-12 30-May-14 29-Oct-14 29-Oct-14 29-Oct-14 29-Oct-14 8-Dec-12 29-May-14 29-Oct-14 29-Oct-14 ND ND ND ND ND 1 7 0 54 1 ND ND ND ND ND ND 0211 ND ND ND ND ND ND ND 1.91 054 ND No Pattern No Pattern No Pattern No Pattern No Pattern Diesel No Pattern No Pattern ND 0 311 ND ND ND OA31 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0641 ND ND ND ND ND 0361 ND -- ND ND ND ND ND -- ND ND ND 036 ND ND ND ND ND ND ND 3.3 0.571 ND 19 ND ND ND ND ND ND ND ND ND ND ND 6 1 ND ND 3 71 ND ND ND ND ND 11 ND ND 23 ND ND ND ND ND ND ND 17.9 ND ND ND ND ND ND ND ND ND ND ND ND 11 ND ND 280012011 ND ND 337 ND 12000 ND ND 1101 ND ND ND !VD ND ND ND 1000 ND ND ND ND 19 17 24 110000 27 9 28 363 28 340 19 8 19 5 210 ND ND ND ND 0.981 ND ND NO ND ND ND ND NO ND ND 25000000 59500 61700 66300 64030 46000 13103 13803 3000 ND ND ND ND 22 ND ND 1200 ND ND ND ND 1.11 ND ND .3500 ND ND ND ND 12 ND ND 2900000 122 112 474 ND 8300 ND ND 1700 844 863 ND ND 11 668 ND 2200000 27900 28800 29503 29500 7400 2800 2770 100000 214 219 244 236 250 ND ND 1700 ND ND ND ND 8.4 ND ND 1000000 3680 3650 3880 3790 7900 2980 3140 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 250000 155C00 16C003 163000 164000 210000 229000 236003 NO ND ND - ND ND ND ND ND 6200 ND ND ND ND 51 44 3 44 1 7900 ND ND ND ND 29 ND ND 0,9 ND ND ND ND ND ND ND BOLD BOLD ITALIC SLUE Mt L1C -Value exceeds ISL or EPA tapwater RSL -Value exceeds Tier 1 level or EPA MCL - May 201 4 metals concentrations were anom aloLsly high in general compared to prior and later (Oct 2014) concentrations Therefore. May metals concentrations are deem ed unrepresentatkre of site con drt ions MW-5 MW-6 MW-7 Analyte MW-4 Petroleum Hydrocarbons by 00150 (pgfL) MW-9 MW-12 MW-13 MW-14 MW-15 MW-17 DUP-1 (MW-17) 0 2 U 0 19 U 0 17 U 0 58 U 0 2 U 2.02 0 17 U 0 58 U 2.44 11.3 0.375 J 8.39 0 2 U 0 19 U 0 17 U 0 58 U 0 2 U 0 19 U 0 17 U 0 58 U 0 2 U 0 19 U 0.17 J 0 58 U 0.396 J 0.367 J 0.229 J 2.04 J 0 2 U 0 19 U 0.175 J 0.616 J 0 2 U 0.261 J 0.184 J 0 58 U 0 2 U 0 19 U 0.465 J 0 58 U 0 2 U 0 19 U 0.256 J 0 58 U OD (PcOLI Benzene Ethylbenzene Toluene Xylenes, Total by [WS a 0 21 U 0 319 U 0 21 U 0 21 U 0 319 U 0 21 U 0.306 J B 0 319 U 0 319 U 7_85 B 6.70 6.78 0 21 U 0 319 U 0 21 U 0 21 U 0 319 U 0 21 U 2.37 JB 2.32 2.32 0.236 J B 0 319 U 0 319 U 0.296 J B 0 319 U 0 319 U Naphthalene (8260B) Naphthalene (8270D) Naphthalene (Interpreted) 0 21 U 0 319 U 0 21 U 0 21 U 0 319 U 0 21 U 13_7 8.57 1.01 J 1 98 U 0.7 J 1 9 U 0 345 U 0 276 U 0 302 U 1 98 U 0 328 U 1 9 U 0 345 U 0 276 U 0 302 U 1 98 U 0 328 U 1 9 U 0 345 U 0 276 U 0 302 U 1 98 U 0 328 U 1 9 U 0 345 U 0 276 U 0 302 U 1 98 U 0 328 U 1 9 U 0 345 U 0 276 U 0 302 U 1 98 U 0 328 U 1 9 U 0 345 U 0 276 U 0 302 U 1 98 U 0 328 U 1 9 U 0 345 U 0 276 U 0 302 U 1 98 U 0 328 U 1 9 U 0 345 U 13.4 2.52 1 98 U 2.19 23.7 0 345 U 0 276 U 0 302 U 1 98 U 0 328 U 1 9 U 0 345 U 14_9 0 302 U 2.01 J 5.8 IOU 2-Methylnaphlhalene Acenaphthene Acenaphthylene Acetophenone Ant racene Biphenyl 82.9 J 54.5 J 137 J 40% J 136 64.1 J 200 32% J 78.8 J 276 355 78% J 3030 242 3270 7% 6350 507 6860 7% 1020 14000 15000 93% 4180 293 4470 7% 43 1 U 43 1 U 86 2 U 43 1 U 43 1 U 86 2 U 43 1 U 43 1 U 86 2 U 43 1 U 43 1 U 86 2 U C10-C20 C20-C28 TPH C10-C28 TPH %C20+ • . 700 (1100 Carbazole 2 41 U 2 41 U 2 41 U 2 41 U 2 41 U 2 41 U 6.09 J 2 41 U 2 41 U 2 41 U 2 41 U Dibenzofuran 2 5 U 2 5 U 2 5 U 4.98 J 6_17 J 2 5 U 6.91 J 2 5 U 2 5 U 2 5 U 2 5 U Fluorene 0 276 U 0 276 U 0 276 U 12.3 20.4 0 276 U 18 0 276 U 0 276 U 0 276 U 0 276 U NMI --- MIN MI IM --1•11 INN -MEM MO MN Table 1. December 2015 Groundwater Sampling Results Phenantrene 0 362 U 0 362 U 0 362 U 9.07 9.01 0 362 U 5.31 0 362 U 0 362 U 0 362 U 0 362 U Pyrene 0 302 U 0 302 U 0 302 U 0 302 U 1.95 0 302 U 0.954 J 0 302 U 0 302 U 0 302 U 0 302 U Notes U Not detected; method detection limit provided J Estimated; detected below practical quantitation level B Analyte was detected in associated Method Blank sample 20160114 SigurdGWQxlm Remits Table 1. November 2016 Groundwater Sampling Results, GP Sigurd Analyte 1, MW-2 MW-4 "Alt, MW-5 MW-6 C10-C20 C20-C28 TPH: C10-C28 TPH: %C20+ 0.0843 U 0.0843 U 0.169 U 0.191 0.12 0.311 39% 0.0843 U 0.084 3 U 0.169 U Benzene 0.2 U 0.2 U 0.2 U Ethylbenzene 0.19 U 0.19 U 0.19 U Toluene 0.17 U 0.17 U 0.17 U Xylenes, Total 0.58 U 0.58 U 0.58 U Naphthalene (8260B) 0.21 U 0.21 U 0.21 U Naphthalene (8270D) 0.343 U 0.343 U 0.343 U Naphthalene (interpreted ) 0.21 U 0.21 U 0.21 U 2-Methylnaphthalene 0.37 U 0.37 U 0.37 U Acenaphthene 0.296 U 0296 U 0.296 U Acena phthylene 0.324 U 0.324 U 0.324 U Acetophenone 1.57 U 1.57 U 1.57 U Anthracene 0.352 U 0.352 U 0.352 U Biphenyl 1.11 U 2.08 J 1.11 U Caprolactam 1.48 U 1.48 U 1.48 U Carbazole 0.833 U 0.833 U 0.833 U Dibenzofuran 1.2 U 1.2 U 1.2 U Fluorene 0.296 U 0.296 U 0.296 U Phenanthrene 0.389 U 0.389 U 0.389 U Pyrene 0.324 U 0.324 U 0.324 U Nitrate as N) 0 51 1.75 irtVATAV,40,kr,;•,,,„1.,,fivp, Iron 0.05 U 1.35 Notes: DUP 1 (MW-6) v MW-7 l KW, ;it 4 'qur MW-9 MW-11 MW-12 MW-13 MW-14 MW-15 MW-17 4rdt.1e.,/, 0.0843 U 0.0843 U 0.169 U 1.64 0.16 1.80 92.7 7.64 100.34 2.28 U 14.8 17.08 22.1 1.36 23.46 0.0843 U 0.0843 U 0.169 U 0.0843 U 0.223 0.31 0.0843 U 0.0843 U 0.169 U 9% 8% 87% 6% 73% 0.2 U 0.2 U 0.2 U 0.45 J 1.07 0.2 U 0.2 U 0.2 U 0.19 U 1.4 0.608 J 0.19 U 4.15 0.19 U 0.19 U 0.19 U 0.17 U 0.17 U 0.17 U 0.17 U 0.17 U 0.17 U 0.17 U 0.17 U 0.58 U 0.58 U 0.58 U 2.32 J 1.51 J 0.58 U 0.58 U 0.58 U 0.21 U 4.68 J 0.374 J 0.21 U 1.29 J 0.21 U 0.21 U 0.21 U 0.343 U 1.79 J 9.25 U 9.25 U 9.25 U 0.343 U 0.343 U 0.343 U 0.21 U 4.68 J 0.374 J 021 U 1.29 J 0.21 0.21 U 0.21 U 0.37 U 2.34 10 U 10 U 10 U 0.37 U 0.37 U 0.37 U 0.296 U 4.08 77.3 8 U 8 U 0.296 U 0.296 U 0.296 U 0.324 U 0.324 U 8.75 U 8.75 U 8.75 U 0.324 U 0.324 U 0.324 U 1.57 U 1.57 U 42.5 U 42.5 U 42.5 U 1.57 U 1.57 U 1.57 U 0.352 U 0.352 U 9.5 U 9.5 U 9.5 U 0.352 U 0.352 U 0.352 U 1.11 U 1.11 U 53.8 J 30 U 30 U 1.11 U 1.11 U 1.11 U 1.48 U 152 40 U 40 U 40 U 1.6 J 1.48 U 1.48 U 0.833 U 0.833 U 22.5 U 22.5 U 22.5 U 0.833 U 0.833 U 0.833 U 1.2 U 2.62 J 32.5 1J 32.5 U 32.5 U 1.2 U 1.2 U 1.2 U 0.296 U 6.49 127 8 U 8 U 0.296 U 0.296 U 0.296 U 0.389 U 4.56 173 10.5 U 10.5 U 0.389 U 0.389 U 0.389 U 0.324 U 0.324 U 20.4 „I 8.75 U 8.75 U 0.324 U 0.324 U 0.324 U r,r,* 86.1 U: Not detected; method detection limit provided. J: Estimated; detected below practical quantitation level 20170309 Sig urd GWQ xlsx Results 2017 Groundwater Monitoring Report Georgia-Pacific Forrner Gypsum Manufacturing Facility APPENDIX C. THEIL-SEN TREND ANALYSES April 13, 2018 TETRA TECH 30 • 25 NAPHTHALENE at MW-13 120 • Data 100 Theil-Sen Trend P95 Trend I! 80 ret Noncanoer SL (THI=1) 0 • 1/1/12 12/31/12 12/31/13 12/31/14 1/1/16 12/31/16 12/31/17 Date ETHYLBENZENE at MW-13 70 • • Data 60 Theil-Sen Trend —P95 Trend 50 EPA Ingestion SL (TR=1E-05) cs 40 No. EPA Ingestion SL (TR=1E-06) 10 • 1/1/12 12/31/12 12/31/13 12/31/14 1/1/16 12/31/16 12/31/17 Date 60 .1= a) 0 40 20 BENZENE at MW-13 10 o 0 0 1/1/12 12/31/12 12/31/13 12/31/14 1/1/16 12/31/16 12/31/17 Date 414•4 • • Data Theil-Sen Trend —P95 Trend MCL MB-- MI —111INION NM MI NM MON111 Mil MI WM En NM MN • 0 1/1/12 12/31/12 12/31/13 12/31/14 1/1/16 12/31/16 12/31/17 Date 18 15 2 3. 12 0 0 1/1/12 12/31/12 12/31/13 12/31/14 1/1/16 12/31/16 12/31/17 Date NAPHTHALENE at MW-9 7 6 .10,..... -_,......,... • 0 12/31/12 12/31/13 12/31/14 1/1/16 12/31/16 12/31/17 Date • Data Theil-S en Trend P95 Trend Noncancer SL (THI=1) 3 NAPHTHALENE at MW-7 • Data Theil-S en Trend ---- P95 Trend —Noncancer SL (THI=1). • 30 • ETHYLBENZENE at MW-7 • Data Theil-Sen Trend —P95 Trend EPA Ingestion SL (TR=1E-05) EPA Ingestion SL (TR=1E-06) IIINI MINN— MN NM NM —01115— MTh ME INN MIN INNI 2017 Groundwater Monitoring Report Georgia-Pacific Former Gypsum Manufacturing Facility APPENDIX D. PREDICTIVE THEIL-SEN TREND ANALYSIS FOR NAPHTHALENE AT MW-7 April 13, 2018 TETRA TECH II I I I I I I I IN-- NM V I I I 1 --SION 11=-111111 =I I I I IN 1 I I I I N NAPHMALENE at MW-7 • Data • —Theil-Sen Trend - — P95 Trend — hloncencer SL (TH 1st) • Hypothetical samples 5 • o • 11112 111116 111/20 Date