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Home My WebLink AboutDAQ-2024-0050361 DAQC-125-24 Site ID # 16121-B4 MEMORANDUM TO: STACK TEST FILE – CRUSOE ENERGY SYSTEMS – Duchesne Data Center Power Station THROUGH: Harold Burge, Major Source Compliance Section Manager FROM: Robert Sirrine, Environmental Scientist DATE: February 6, 2024 SUBJECT: Location: One mile Northeast of Upalco, Duchesne County, UT Contact: Ken Parker 720-495-3656, Pinyon ES Kaitlin Meszaros 631-245-0308 Tester: Great Plains Analytical Services (GAS), Macie McClellan 580-225-0403 Source: Two 530 hp Waukesha H24 CEs and one 13,634 kw Titan 130 Turbine FRS Site ID#: UT0000004901300215 Permit #: AO DAQE-AN161210002-23 Dated February 13, 2023 Action Code: Tr Subject: Review of stack test report dated January 5, 2024 On January 8, 2024, the DAQ received a stack test report for emissions testing of the Crusoe Energy Systems – Duchesne Data Center Power Station’s, two 530 hp Waukesha H24 compressor engines and one 13,634 kw Titan 130 Turbine located 1 mile Northeast of Upalco, Duchesne County, UT. Testing was performed December 20-21, 2023, to determine compliance with AO Condition II.B.2.a, and NSPS 40 CFR 60, Subpart JJJJ for NOX, CO, and VOC emissions. The DAQ calculated results are: Source Test Date RM/Pollutant DAQ Result Tester Result Limit CE H24-1 12/20/23 */NOX 0.12 lb/hr 0.12 lb/hr 0.18 lb/hr 0.12 g/BHP-H 0.12 g/BHP-Hr 0.15 g/BHP-Hr */CO 0.02 lb/hr 0.02 lb/hr 0.35 lb/hr 0.02 g/BHP-Hr 0.02 g/BHP-Hr 0.30 g/BHP-Hr */VOC 0.01 lb/hr 0.01 lb/hr 0.02 lb/hr 0.01 g/BHP-Hr 0.006 g/BHP-Hr 0.02 g/BHP-Hr CE H24-2 12/20/23 */NOX 0.01 lb/hr 0.01 lb/hr 0.18 lb/hr 0..01 g/BHP-H 0.01 g/BHP-Hr 0.15 g/BHP-Hr */CO 0.02 lb/hr 0.025 lb/hr 0.35 lb/hr 0.03 g/BHP-Hr 0.025 g/BHP-Hr 0.30 g/BHP-Hr */VOC 0.004 lb/hr 0.004 lb/hr 0.02 lb/hr 0.004 g/BHP-Hr 0.004 g/BHP-Hr 0.02 g/BHP-Hr 2 Source Test Date RM/Pollutant DAQ Result Tester Result Limit Turbine 12/21/23 */NOX 2.44 lb/hr 2.42 lb/hr 13.33 lb/hr 0.09 g/BHP-Hr 0.09 g/BHP-Hr 0.33 g/BHP-Hr */CO 0.06 lb/hr 0.06 lb/hr 8.11 lb/hr 0.002 g/BHP-Hr 0.002 g/BHP-Hr 0.20 g/BHP-Hr */VOC 0.72 lb/hr 0.716 lb/hr 4.65 lb/hr 0.03 g/BHP-Hr 0.028 g/BHP-Hr 0.12 g/BHP-Hr *ASTM D6348-03 DEVIATIONS: No deviations were noted. The one discrepancy is the Turbine lb/hr value for NOX, which is an error in entering the correct final value in the test report since the three values listed in the report yield a final average of 2.44 lb/hr which matches the DAQ calculated value. CONCLUSION: All method stipulated QA/QC requirements appear to have been met as determined by a review of the report and entering the provided data into our Excel spreadsheets. The emissions test report appears to be acceptable. RECOMMENDATION: The two 530 hp Waukesha H24 CEs and one 13,634 kw Titan 130 Turbine should be considered to have been in compliance with the NOx, CO, and VOC applicable emissions limits at the time of testing. HPV: No. ATTACHMENT: Crusoe Energy DDC stack testing report received January 8, 2024. DAQ generated Excel spreadsheets. January 5,2024 Harold Burge Utah Division of Air Quality PO Box 144820 Salt Lake City, Utah 841144820 Subject Crusoe Energy Systems, lnc. Duchesne Data Center Power Station - Stack Test Reports On behalf of Crusoe Energy Systems, !nc. (Crusoe Energy) please find attached the three sack test reports for the engines and turbine tabled below. Below is a able summarizing the tested unis along with their test dates. Titan 130 turbine 12t7v2023 Waukesha H24 compressor engine 1?/20D023 r Waukesha H24 compressor engine 322 I 509 t2t20t2023 Should you have any questions or comments about these reports, please contact Kaitlin Meszaros by email at meszaros@pin)ron-env.com or by phone at 631-245-0308.Thank you for your assisance in this matter. Sincerely, PINYON ENVIRONMENTAL, INC.,UTAH DEPARTMENT OF ETWIRONMENTAL OI.iAUTY {urJ.L-^; $lvfa,f^r.r) Kaitlin A Meszaros Air Quality Specialist Cc: Michael Duplantis, Crusoe Energy Systems, lnc. JAN B ?024 DIVISION OF AIR QUALITY Test Started: 08:55 AM Test Completed: 12:37 PM #As 40 CFR Part 60 Subpart JJJJ Performance Test Report Test Type: lnitia! Test Date: 12fr20n2023 Source: Waukesha H24 Rich Burn (4 Cycle) Serial Number:3221509 Engine Hours:3546.8 Location: Duchesne Data Center Power Station Duchesne County, Utah Prepared on Behalf of: Crusoe Energy Systems, lnc. UTAH DEPARTMENT OF ENVIRONMENTAL OUALITY JAN B ?C24 DIVISION OF AIR QUALITY 303 W.3rd St (s80) 225-0403 Elk City ,OK73644 lndex 1.0 Key Personnel.... ............. 3 2.0 Sampling System..... ....... 3 3.0 Methods Used............ ......................... 3 4.0 Test Summaries.. ............ 5 5.0 Run Summaries.. ............ 6 6.0 Volumetric Flow Rate Data.... ............. 7 7.0 Calculations.............. ...... 8 8.0 Orygen Calibration... ...... 9 9.0 Engine Parameter Data Sheet.. .......... 10 10.0 QA/QC Results........ ........11 11.0 D6348 Annexes...... ........ 12 12.0 Signature Page........ ....... 18 13.0 Appendices.............. ....... 19 14.0 Bottle Certs............ ....".... 20 15.0 Tri Probe Certification via GD-031 ...... 25 16.0 GAS ALT 141_FT|R EPA........ ............26 17.0 Tester Qualifications (resume)... ......... 28 18.0 Raw Data. Tables Table 5.1 (Run Summaries)............. ........... 6 Table 6.1 (Volumetric Flow Rate Data)........... ................ 7 Table 6.2 (Stack Gas Measurements)......... .................... 7 Table 8.1 (Oxygen Calibration).. ................. I Annex Table 1.2.1 (Certified Calibration Bottle Concentrations)......... 12 Annex Table 1.2.2 (Measurement System Capabilities)..................... 12 Annex Table 1.3.1 (Test Specific Talget Analytes)............................. 13 Annex Table 4.1 (Measure System Capabilities) ............ 15 Figures Figure 6.1 (Location of Traverse Points per Method 1).......................7 Annex Figure 1.4.1 (Sampling Train)..... ..... 13 Annex Figure 1.4.2 (Sampling Points)... ...... 14 Annex Figure 1.4.3 (Sampling Port Locations).... ............ 14 Appendices Certified Calibration Bottle Certificates............. ...............20 Tri Probe Certification via GD-031 .............. 25 GAS ALT 141_FT|R EPA............. ............... 27 Tester Qualifications (resume)... ................. 28 Raw Data..... ....... 29 29 3 1.0 Key Personnel GAS Crusoe Energy Systems, lnc. Lucas Ennis Kody Walters 2.0 Sampling System The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet Personal Sampling System with a Zirconium Oxide oxygen sensor. 3.0 Methods Used ASTM D6348.03 This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target analytes (CO, NOX, CH2O, & VOC's) from stationary source etfluent. Because an FTIR analyzer is potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific. The analytes, detection levels, and data quality objectives are expected to change for any particular testing situation. tt is the responsibility of the tester to define the target analytes, the associated detection limits for those analytes in the particular source effluent, and the required data quality objectives for each specific test program. Provisions are included in this test method that require the tester to determine critical sampling system and instrument operational parameters, and for the conduct of QA/QC procedures. Test'ers lollbwing this test method will generate data that will allow an independent observer to verify the valid collection, identification, and quantification of the subject target analytes. EPAMethodl&14 The purpose of the method is to provide guidance for the selection of sampling pods and traverse points at which sampling for air pollutants will be performed pursuant to regulations set forth in this part. EPA Method 2 &2C This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas stream. The average gas velocity in a stack is determined from the gas density and from measurement of the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16 separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated utilizing the formulas seen in section 7.0 ol this report. EPA Method 3A This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions using a continuous instrumental analyzer. Quality assurance and quality control requirements are included to assure that the tester collects data of known quality. Documentation to these specific requirements for equipment, supplies, sample collection and analysis, calculations, and data analysis will be included. GAS 4.0 Test Summary Unit with a serial number of 3221509 which is a Waukesha H24 engine located at Duchesne Data Center Power Station and operated by Crusoe Energy Sy$tems, lnc. was tested for emissions of: Carbon Monoxide, Oxides of Nitrogen, and Volatile Organio Compounds. The test was conducted on 1212012023 by Lucas Ennis with Great Plains Analytical Services, lnc. All quality assurance and quality control tests were within acceptable tolerances. The engine is a natural gas fired Rich Burn (4 Cycle) engine rated at 530 brake horse power (BHP) at 1800 RPM. The engine was operating at 436 BHP and 1559 RPM which is 82.33o/o of maximum engine load during the test. The test HP calculation can be found on page 8. The engine was running at the maximum load available at the test site. Site Verification Photos GAS 4.0 Test Duchesne Dala Center Power Station Fsd67A atfia Run 1 Run 2 RUne Pesi Permlts GO 2,000 0.300 o.022 0.021 0.019 0.02'l Pass co flbs/ht 0.350 0.022 0.020 o.0't7 0.020 Pass co @15o/o Q2 2.56t 2.576 2.288 2.484 CO @15YoOz 2586.839 2576.367 2288.458 2483.888 co 7.666 7.619 6.839 7.374 GO 9.144 9.104 8.088 8.779 CO (molwt) 28.01 NOx hlhr 1.000 u.'t5u o.132 0.121 0.116 0.123 Pass NOx (lbsfl U.'IAU 0.133 o.120 0.103 0.118 Pass NOx @15YoOz 9.3€9.204 8.313 8.955 NOx @15o/o Q2 9347.615 9203.704 8312.872 8954.730 NOx DDmvw)27.700 27.216 24.U1 26.586 NOx (Dpmvd)33.042 32.524 29.381 31.M9 NOx (molwt) 46.01 NMNEHC hp-hr 0.700 0.020 0.007 0.006 0.006 o.006 PASS NMNEHC (Ibsfl 0.020 0.007 0.006 0.005 0.006 Pass NMNEHC (oomvd @15o/o QZ 0.512 0.451 0.440 0.468 NMNEHC (ppbvd) @15YoO2 51 1.935 45't.291 439.888 4fjf . to5 NMNEHC ppmvl,l ippmvd 1.517 1.335 1.315 1.389 NMNEHG 1 .E10 1.595 1.555 1.653 NMNEHC (molw 44.10 GAS 6 5.0 Run Summaries Table 5.1 Run Summaries GAS 6.0 Volumetric Flow Rate Data Table 6.1. Data used for volumetric flow rate (Method 2) Table 6.2. Stack gas pr€ssure r€a Aostd = Velocitv head measured bv the' standard pitot tube, (in.) H2O.' Damore aTrer EacK ruroe.o.50 Within 5% of Last Aostd readino:Yes Flgure 6.1 16 Traverse Points Were UsedStack Diameter (inches)6.OO lnches upstream from disturbance 48.00 lnches downstream lrom disturbance 32.00 Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1 *The exhaust stack dld not present cyclonlc flow condltlons at the sampllng locatlon due to the absence of cyclones, inertial demlsterc, venturl scrubbers, or tangsntlal lnlets. 'Cyclonlc Flow Chock (Pass/Fai!): PASS GAS I 7.0 Calculations Method 2: Determination of Stack Gas Velocitv and Volumetric Flow Rate *Note- Use of this method neqates the need for any fuel related numbers for emissions calculations Ap(avg) - Velocity head of stack gas, mm H2O (in H2O). 3600 = Conversion Factor, sec/hr. A = Cross-sectional area of stack, m2 (ftz) Bws = Water vapor in the gas stream (from ASTM D6348) Cp(std) = Standard pitot tube coefficient; use 0.99 Kp = Velocity equation constant. Md = Molecular weight ot stack gas, dry basis, g/g-mole (lb./lb.-mole). Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb./lb. -mole) Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg) Pstd = Standard absolute pressure, 760 mm Hg (29 92 in. Hg). Qsd = DrJl volumetric stack gas flow rate corrected to standard conditions, dscm/hr. (dscf/hr.). Ts(abs) - Absolute stack temperature, "K ("R). = 460 + Ts lor English units. Tstd = Standard absolute temperature, 293'K (528 "R). Vs - Average stack gas velocity, m/sec (ft./sec). Md = .44(%CO2)+.32(%02)+.28(%N2+%CO)Md = 44( 092)+.s2(0)+ 28( 907+ 001) = 29.475 LB/I-B-MOLE Ms = Md(1-Bws)+ 18.0(Bws)Ms = 29.475(1 - 16168)+.18 0(.16168) = 27.62 LB/LB-MOLE vs = Kp.Cp(std;.VApavg'y'(Ts(abs)/(Ps.Ms))vs = 85 49..99',^/ AZ"^/1tSO+.A7424.56',27 62\) = 96.2 FTISEC Qsd = s600(1 -Bws)Vs.A((Tstd-Ps)/(Ts(abs)-Pstd))Qsd = 3600(1-.162\96.202-.349((528.24.56)/ (1304.67.29.92)) =33672.72 DSCF/HR Q = Qsd/35.315 Q = 33672.72/35 315 = 953.496 DSCM/HR Emission Rates (Examples use CO Run 1) 453.6= Conversion lactor lb. to gram HP= Engines rated Horsepower A = Cross-sectional area of stack, m2 (ftz\. Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min) BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.). 02 = Concentration oi oxygen on a dry basis, percent. BTU/HP-HR. = Brake Specific Fuel Consumption (HHV) ppm= Pans Per Million (CO) ER = Emission rate of (CO) in g/HP-hr. ppm@15% 02= PPM corrected lo 15'/"02 F(d )= yelLrr.s of combustion components per unit of heat Qsd = Dry volumetric stack gas flow rate corrected content, scm/J (scf/million Btu). to standard conditions, dscm/hr. (DSCF/HR.). Q = Stack gas volumetric flow rate, in standard cubic meters Run Time = Run Time in Minutes per hour, dry basis Tpy= Tons per year LB/HR.= Emission rate of (Co) in LB/HR. vs = Average stack gas velocity, m/sec (ft./sec). Mol wr.= Mol weight of co (28.01) ppm @ 15% 02 = PPM-((20.9-15o/"O2)l(2o.9-O2l)ppm @ .15% 02 = 9.144'129.9-15)/(20.9-0'/")) = 2.581 PPM @ 15% 02 g/hp-hr = (PPM-(1.1 64-1 0L3)tQ'(Run Time/60))/BHP/HR (9. 1 44.(1 . 1 64.1 0^-3).953.496"(Run Time/60))/455.8 = .022 G/HP-HR lb/hr = ER-1 /453.6-BHP-HR LB/HR = .022- 1 1453.6- 455 8 = .022 LB/HR TPY = LB/HR. '4.38 TPY = .022.4.38 = .096 TPY HP Provided On Site ppm wet. (1(1-H2O) = ppm dry e 14 = 7.6655-(1(1-.16)) GAS 8.0 Oxygen Calibration 9 8'1 calibration error tost; how do I confirm my analyzer calibration is correct? After the tester has assembled, prepared and calibrated thesampling system and analyzer,.they conduct a 3-point inalyzer calibration error test before the first run and again after any failed system bias test orfailed drift test' They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibiation mode. At each calibration gas level(low, mid, and high) the calibration error must be within +2.0 percent of the c;libration span. 8'2- lnitial system bias and system calibration enor checks. Before sampling begins, it is determined whether the high- level or mid-levelcalibration gas best approximates the emissions and it is used as the upscale ga!. rn;e upscale gas is introJuced at the probe upstream of all sample-conditioning components in system calibration mode. (1) Next' zero gas is introduced as described above. The response must be within 0.5 percent ofthe upscale gas concentration.(2) Low-level gas reading is observed until it has reached a final, stable value and the iesults are ,ecoided. rn-e measuremenl system will beoperated at the normal sampling rate during all system bias checks. (3) 1f the initial system bias specification is not met, corrective action is taken. The applicable calibration error test from Section g.2.3 of EpAMethod 7E is repeated along with the initial system bias _check until acceptable resulis are achieved, after which sampling will begin- The pre-and poslrun system bias must be within t 5.0 percent of the calibration span for the low-level ano upicate calibration gales. 8'3 Post-run system bias check and drift assossment - confirming that each sample colloctsd is valid. Sampling may be performed for multipleruns before performing the poslrun bias or system calibration error chEck provided thistest is passed at the conclusion of the group of runs. A failedfinal test in this case will invalidate all runs subsequent to the last passed test. (1) lf the poslrun system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then anothercalibrationerror test and system bias is passed before repeating the run. (2) After each run' the .low-level and upscale drift is cilculated, using Equation 7E-4 in section .12.5 from EpA Method 7E. lf the poslrun low-and upscale bias checks are passed, but the low-or upscale drift exieecls the specification in section 13.3, the run data are valid, but a 3-pointcalibration error test and a system bias check must be performed and passed prior to additional testing- Table 8.1 Oxygen Calibration Method 7E 3.4 To the extent practicable, the measured emissions should be between 20 to 100 percent of the selected calibration span. This may not be practicable in somecases of low concentration measurements or testing for compliance'with an emission limit when emissions are substantially less than the-limit. EPA Method 3A CIA Worksheet ro (,a3 corice-ntraton I Cerflfled Ger Goncentralon I Cerilfled Gac GrLow.Levot (%) | t id-Levet (%) I Xtgtr_t_eu 0.00%l9.O4y"lzo.to, rncentralon Ittlohl I6-1 I I Ze e.S: Note: that you may I risk sampling for muttiple runs before performing the post-run bias provided you pass this test at the conclusion of the group of (DIRECT) Anallzer Calibration Error (S 2%) Check Certifi6d Concentration Value (%) Direct Calibration esponse (%) Abgolute Difrerence (7o) Analyzer Calibration Enor (%) Zero Gas %0-000/o 0.00%0.00%0.00% Mid-Level cas % ligh-Level Gas % 9.040h 20.70o/o 9.03% 20.51yo 0.00% 0.19o/o 0.02% 0.90% (SYSTEM) Calibration Bias Ghecks (S 5%) and Drift Checks (S 3%)Upscale Gas 9.040/o Zero Offset 0.00% Bias Prc lnitial Value Bias Post lnital ValuesSpan 20.70 Analfzer Calibration Response (%) Zero Gas O.OOyo System Calibrations Response Pre (%) System Bias (7 of Span) Pre SysEm Calibration Response Posl t%) iystem Bias (% of Span) Post Drifl (% of Span) O.O0o/o 0.00o/o 0.000/o 0.00%0.00% Upscale Gas 9.03o/o 9.02o/o 0.05%9.00%0 14o/o 0.00% (SYSTEM) Calibratlon Bia3 Checks (S 5%) and Orifl Chech (S 3%) Avg. Gas Concentration (Run 1)0-Mo/o Effuent Gas (Coas) Run 1 0.040h Avg. Gas Concentration (Run 2)O.OSVo Effluent Gas (Cgas) Run 2 0.05% Avg. Gas Concanlration (Run g)0.05o/o Effluent Gas (Cgas) Run 3 0.0s% EPA Method 3A CIA Worksheet zero Gas 100% Nitrogen Mid-Level Gas 9.040/0 High-Level Gas 20.70% Zero Gas o/o Mid-Level Gas % High-Level Gas % zero Gas % l-;oill Upscale Used upscate car l-mr%-l s.o4% Zero Gas % [-;o% lupscare used Upscate car I ,.o0% I s.o4% GAS a 10 9.0 Engine Parameter Data Sheet Run 1 Run 2 Run 3 Completed Company reergySystems,lnc. Facllltv DucheSne L,ata Uenler Fower urarlon Date '11z2u.t21)23 Site Elevation (ft)5A2t Unlt lD Make wauKesna Model t'124 Serlal Number 3221 509 Technlclan Lucas Ennis TunStafr-nmes 08:55 AM 110:07 AM 11:20 AM 12i37 PM Enolne Hours 3543.8 3544.8 3545.8 3546.6 Run 1 Run 2 Run 3 Averaqe Enqine Speed (RPM)1562.0 1557.0 1ss8.0 1559.0 lntake Manlfold Pressure (Psl)39.2 38.6 35.8 37.9 -[-ntakei/hnlfoldTemp'F 122.O 123.O 122.O 122.3 EnEineLo-afl(BHP)455.E 450.5 402.8 4it6.4 TmEienITemF-F 27.O 34.0 37.O 32.7 Tumldltv%I t.u 59.0 51 .O 62.3 EwFoInt.F 21.O 21.O 21.0 21.O AFR Manufacturer/Type Waukesha \,Yaukesha Waukesha Waukesha Suctlon Pressure 75.8 74.3 63.6 71.2 Discharoe Pressure 381 .6 380.7 374.7 379.O catalvst lYes or N0 Yes catd-ulvstManuf acturer GE GE GE GE +o-f -Catalystlnstalled 2 2 2 2 ilatalvst lnlet Temp oF 1159.0 1153.O 1135.0 1149.0 -atalvst Outlet Temp'F 1117.O 1 1 16.0 1 103.0 1112.0 eatalist Pressure Drop H2o 8.8 9.O 8.7 8.8 GAS 11 10.0 OA/OC Results Zero Response Time 45 System Response Time 45 seconds Nitrogen monoxide NO Nitrogen dioxide NO2 NOx voc Oxygen Average:0.00 Average:0.00 Average:0.00 Average:0.00 Average:0.55 Average:0.00 CTS Bottle Concentration CTS Compound Concentration Avg Tolerance Difference between measured and expected Value:100.00 Value:98.56 2.0O/" 1.44o/o Nitrogen monoxide NO Nitrogen dioxide N02 NOx voc Average:0.00 Average:0.00 Average:0.00 Average:0.00 Average:0.47 Average:0.00 CTS Bottle Concentration CTS Compound Goncentration Avg Tolerance Ditference between measured and expected Value:100.00 Value:97.7O 5.00% 2.30% Equilibration Response Time Spike Reported Spike Expected 45 seconds Value:249.61 Value: 251.00 Gas, lnc. 12 1 1.0 D6348 Annexes 1-8 The test q-uality objectives completed for the emissions test are demonstrated throughout Annexes 1,2, g, 4, 5,6,7 & I as layed out per ASTM D6348-03. All reference methods, pre-test and post test procedures were within acceptable limits. Data generated during the pre-test and post-test procedures ard summarized below in order of the distinctive Annex. Three 60 minute test runs were performed. The final analyte concentrations are the average of each test run. Data was taken at 60 second intervals. Each 60 second measurement was the average of 600 scans. .lppale is used as the surrogate compound for the Annex 5 Spiking Technique due to Propane being the VOC that is most commonly found in the combustion process df natural gas. 'Additionally, the molecu-iar weight of Propane coincides with with molecular weight of VOC's per the EPA. Annex Table 1.2.1 Certified Calibration Bottle Concentrations Bottle Expiration N02 Ethylene sF6 02 (Yol cc517745 7t't3t2026 101.90 9.O4"/o cG1 1 7503 4t15t2031 100.00 GG76460 7t5t2031 20.7O"/o Cylinder # CC142828 Expiration: 12-06-2030 Propane co NO sF6 Bottle Value 251.00 5U1 .4U 252.40 9.73 Analyzer System Response 249.61 492.32 247.10 9.60 Percent Difference O.55"/o 1.E1"/o 2.1O"/o 1.29o/" Annex Table 1.2.2 Measurement System Capabilities GAS Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives Compounds lnfrared Analvsls Pcalar Expected Concentratlon Range Measuremenr System Achlevable Mlnimum Detectable Concentratlons Hequrreq Measurement System Accuracy and Preclslon lor fest Appllcatlon (cm-l) co 2000-2200 0-1200 ppm 0.16267 ppm 4 ppm NO 1875-2138 0-1000 oom 0.4007 oom 2 oom NO2 2700-2950 0-'100 oom 0.4899 oom 2 oom voc 2600-3200 0-100 ppm 1.8520 ppm Total VOC'S 1 ppmperVOC910-1 150 2550-2950 CHzO 2550-2850 0-100 oom 0.7878 oom 1 oom lnterferlng Compounds . CO is analyzed in a separate analysis region than CO2 and H2O coz 926-1 150 0-10h 07"nla Water VaDor 3200-3401 O-22"/o O.ZOYI nla 'VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane. .4 a2 SENSOR PROBE -.,itw-* Er ru ffi GAS Figure Annex 1.4.1 Sampling Train The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges through the FTIR outlet. FLOW MTR.s $VENT STACK GAS 14 Sampling Point Locations in lnches 16.7"/o 'r.336 50o/o 4.000 433"h 6.664 TRLPROBE SAMPLE POINT L AS PERCENIAGE OF SIACK Flgure Annex I Sampllng Polnts !nterior Stack lnches Upstream: 48 lnches Downstream: 32 SAMPLE BY Flgure Annex 1.4.3 Sample Port Locatlon LOCATION DETERMINEO FROM USruRBANCE Taroet Analvte Results (oom) GO o.162/ NU o.400r NO2 o.4E9t Ethvlene o37At ProDane 0.4351 Hexane o.2237 lvde 0.615' horm€a o.7a7t N EA 7T7, 7'7fls REF 7n rTns NEA 717, rMDC*t : 'oorr',s * L'ref Lref REF'r.:;s Lcert calabrataon Tlansler standard ExDected Meaaured Path Lenoth valldated Ethvlene 100 9U.5ti 4.924 Passed An nex T able 1.2.2 ileasurement System Capabilitles GAS Parameter Gas Concentratlon i,leasured % Dlfierence speclflcailon Valldated Spike Direct Propane 251.000 250.512 0-'l9o/"+l'2o/o Pass SF6 9. /3U 9.644 0.88%+l- 2o/o PaSS CO 501.400 494.777 1.32o/o +l'2o/o PaSS NO 252.400 247.832 1.81%+l'2o/o Pass SDIke Run 1 vla the Svstem Source Output SDike Averaqe Dilution Factor Expected 70 Becovery Specilication Propane 0.000 22.200 20.180 11O.O1O"/"70-130% SF6 0.000 o.775 8.036%<1Oo/" Soike Run 2 via the System Source OutDut SDike Averaqe Dilutlon Factor ExDected 70 Recovery SDecillcatlon Propane 0.000 22.351 20.482 109.130%70-130% SF6 0.000 0.787 8.161y"<10h sDlKe Hun 3 vta tne svstGm Source OutDut SDlke Averaoe Dilutlon Factor ExDected o/o Recovery SDecilication Propane 0.000 22.490 20.708 108.610%70-130% SF6 0.000 0.796 8.254o/o <1Oo/" Nolse Equivalent Absorbance (NEA) RMS High 0.000445 RMS Mid 0.001823 RMS Low 0.001065 Lrne Position 020 u t5 010 005 0 00 '\./ 2092 2069 2046 ?fi23 199S X$76 r 953 1930 1907 '1 884 1861 1837 I814. 0.20 0.1 5 010 $CIs 0.OCI l) 05 Line Position Difference:to Beference I 0.29%0.00% Pass GAS Pass The Gasmet GICCOR (Genzel lnterferometer with Cube Corner Retroreflectors) interferometer is specially designed for maximum opticalthroughput and maximum signal to noise ratio of 7.72 (cm-1) remaining stable with any vibration and temperature changes. lne uasmel ux4uuu rs a low resolulron speqro setting and the detector linearity was tested with gas was performed and validated. 158.5898 148.5898 138.5898 128.5898 1185898 108 5898 98 5898 88.5898 78.5898 68 5898695 687 679 672 neter where the aperture is fixed to a maximum angle an alternate approach. A three point linerarity of the CTS Linea rity 664 656 648 641 633 625 61 8 158.5898 148 5898 1 38.5898 128.5898 118 5898 - 1CI8.$898 98.5898 88.5898 78.5898 68 5898ntn nn1utu vvl '15.2439047 Pass The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex 7.6 POST CTS $rstem Check: u ls Botfle uoncentratlon:100.00 L; I S Samole L;OncenraIon Averaoe: 98.92 Difference between measured and expectecl:1.O9% Tolerance:5.OOo/o Run Data Valldatlon - Automated vs Manual Headlng velEated Commente HUn r l.OTnIS r & Z On UU/NU/rrOpane All within 2O7o PASSEd Demonstrates no rntenerences observed. HUn Z HOrntS't & Z On UU/NU/rrOpane All within 2O7o Passecl Demonstrates no Interlerences observed, HUn 3 l.OTnIS'r & Z On UU/NU/rrOpane All within 2O7o Passed Demonstrates no interferences observed, GAS 18 12.0 Signature Page JoUFile Name: Crusoe Energy Systems, lnc.; Duchesne Data Center Power Station; ;JJJJ We certify thal based on review of test data, knowledge of those individuals directly responsible for conducting this test, we believe the submitted information to be accurate and complete. Company: G.A.S. lnc. Print Name: Lucas Ennis Title: Emissions Specialist Dale:1212012023 Company: Print Name: Signature: Title: Phone Number: Date: Company: Print Name: Title: Signature: G.A.S. lnc. Chris Oppel Director of Stack Testing n/,n/l/.// n(,4 %t-{\ Dale:1212012023 PhoneNumber: 580-225-0403 GAS Appendices GAS Spike (5 Gas) *iH3S Part Number: Cylinder Number: Laboratory: PGVP Number: Gas Code: Airts Spccislty Gu6 Airgs USA LLC r2Z2 S. Wetrtmrth Ave. Chicago, IL 60628 Air8s.@m CERTIFICATE OF ANALYSIS Grade of Product: EPA PROTOCOL STANDARI) E05Nr94E15AC014 cc142828 124 - Chicago (SAP) - lL 812022 CO,CO2,NO,NOX, PPN,BALN Reference Number: 54402601324-1 Cylinder Volume: 147.O CF Cylinder Pressure: 2015 PSIG Valve Ouflet: 660 CertificationDate: DecO6,2022 Dato: C.rtf€tion pdbrm6d in e@rdane wtih 'EPA Treeability PEto@lbr ABBY.nd CGr{fietd ot Gr$N C.llbEdon St ndrdt (M.y 2012}' d@ment 000/R-l 2y53 l , Eing th. as.y p@.ducs lbtcd. AnaMi@l M.hodology docs not Equlrc @mdoo tor .natylic.l hbrtbGn@. Thl6 cyllndtr ha8 . tot l sn8tytiel unodeinty as st ild b.low with a ffifid6n6 lovel of 95%. Th€E aB no dgnl€r( impudth6 silich a{tacl th! us ot this elib.atid mixfuE- All ffiGntratiffs aE on a moL/mola basis unlas othailisa hoied. T}le Esults rrl.t. sry to lhc hcrc t!Ld. Th. r.pd shell nd bG Eprodu6d cxcrpt in full withil appDvel of the laboEtory. Do Trl.d D.t! Avallabls Upon Rsquest PERTANENT NOTES:Mixture contalns nominal 1oppm Sulfur l-bxaiuodde as a tracer component. Actual tested value included within the original Certifi@te of Analysis. Contacl the Airgas laboratory if a reprint is requircd NOTES:Mixture contains nominal 10ppm Sulfur Hexafluoride as a tracer component. Actual tested value included within the original Certificate of Analysis. Contact the Argas laboratory if a reprint is required. SF6 Results: JMR137-9.73[PPME n n rl lln Approved for Release P.g. I of I ANALYTICAL RESII,'LTS Gomponent Requested Actual Protocol TotalRel.ilv.Assay Date3ConcenEaton Concentratlon Uothod Uncartllntv NOX 250.0 PPM 253.0 PPM Gl +/- 1.2% NIST TE€ble 11128DO22,12/0612O22 NITRIC OXIDE 250.0 PPM 252.4 PPM Gl +^ 1.0% NIST TE€able 1112812022, 1AOO|2022 PROPANE 250.0 PPM 251.0 PPM G1 +/- 0.7% NIST TE€ble 11I3ODO22 CARBON MONOXIDE 500.0 PPM 501.4 PPM G1 +/- 0.6% NIST TEeable 1112912022 CARBON DIOXIDE 5.000 % 5.025 % G1 +/- 1.4% NIST TE@able 1112U2022 NITROGEN Balene CAI,IBRATTON STANDARDS TyDe Lot lD Cvllnder No Concantratldr Unceitalnw ErDlBtlon Datg NTRM 200603-31 PRM 12386 GMIS 401423838104 NTRM 200502-13 NTRM 13010109 NTRM 13060423 E80113125 250,3 PPM NITRIC OXIDE/NITROGEN D685025 9,91 PPM NITROGEN DIOXIDE/AIR CC5O559O 4,373 PPM NITROGEN DIOXIDE/NITROGEN 6162697Y 243.3 PPM PROPANE.IAIR KALOO3925 495.4 PPM CARBON MONOXIDE/NITROGEN co113685 7.489 % CARBON D|OXIDE/N|TROGEN +l-0.8% +l-2.O% +l-2.0% +l-0.5% +t- 0.60k +l-O.6% Oct 29, 2026 Feb20,2020 F€b 18, 2023 Mat 17,2027 Jul 03, 2024 May 14,2025 ANALYTICAL EQI,IIPMENT lnstrumenuluako/Modol Analytcal Pdnclpls Le3t llultpolnt C.llbratlon Ni@l€t iS50 AUP2010242 CO-1 SIEMENS ULTMMAT 6E N1J57OO Ni@let lS50 AUP2010242 Ni@let iS50 AUP2010242 Ni@let iS50 AUP2110277 NoY 07,2022 Nov 28,2022 Oec05,2022 Dec 05,2022 Nov 07, 2022 FTIR NDIR FTIR FTIR FTIR GAS Airgas ah A[ Lqude company 9o/o O2|NO2 AlrgrsSFdsftyGaG Airgs USAUa 525 North Industial I&p Rosd T@le, UT84074 Airgu.om CERTIFICATE OF ANIALYSIS Grade of Product: EPA PROTOCOL STANDARD Part Number: Cylinder Number Laboratory: PGVP Number: Gas Code: E03Nt90E15W0003 cc517745 124 - Tooele (SAP) - UT 872023 NO2,02.BALN Date: C.rlilletkh pcrbm.d in .@rd.ne wih 'EPA TE6.bill9 PDb@l br Tdad Data Avallablo Upon Roque3l Approved for Relea3e Reference Number: 153402786436-1 Cylinder Volume: '145.0 CF Cylinder Pressure: 2015 PSIG Valve Outlet: 660 Certification Date: Jul 13,2023 C.lbEdon St$dad8 (M.y 2012)' d@m.nt 600/R.12531, Elng thG a$.y prclduEs listod. AMMi€l M.thodology d6s rct EquiG q.d6 tEr .Mlydel inbrf.En@. Thb crlhdd h.s . tot.l .n.Miel unorblnty .s sbbd bdil wlth e dfidcE lcvel of g5%. Thc6 .E m signflldht lhpu.itl& whlcfi aft c't tha ue ol thl! dllbrdid mlxtiE. All 6ehbaliil6 aE m a molG/moL b.8i6 unh$ othwis. not d. Tho Euh6 rclgte dly to lh. lbm6 i.rtcd. Th. ruport Gh.ll not bc Epoduod .xc.pt ln tull wihoul .ppDv.l ol t!. leboEbry. Do Pr!. I ol I ANALYTICALRESULTS Roqu.stsd Actual Protocol Total Relatvg ConcentEflon Concontra0on ileihod Uncertalntv Componont A.3ay Datsg NITROGENDIOXIDE '100.0PPM 101.9PPM Gt +12.0%NISTTE€eble 0710612023,0711312023 OXYGEN 9.000 % 9.037 o/o Gl +/- 1.0% NIST TE@sbl€ 071612023 NITROGEN Bdan€ CALIBRATIONSTANDARDS Type Lot lD Cyllndsr No Concentraton Uncertalnty ExplEtlon O.i. GMIS 153/,022022601 CC517858 10r.r PPM NTTROGEN DTOXTDENTTROGEN 1.1% PRM 12420 D887373 98.9 PPM NITROGEN DIOXIDE/I,IITROGEN 1.O% NTRM 98051010 SG9161286BAL 12.05% OXYGEN/N|TROGEN 0.7% ft. SRM- ffiRM. Pil. d R& mH ebE l. mtu in tud b he GMIS ud ln he Bsv end not Efr dhe an*d.- Nov 09, 2025 Fob23,2023 Ds 14,2023 ANALYIICAL EQI,IIPMENT Anlly[c.l Prlnclplelnstrum€nutak rtodcl L.st 1{ultlpolnt Clllbrstlon MKS FTIR NO2 018143349 Horiba MPA610 W603MM58 02 FTIR 02 Psmmaon€tic (DIXON) Jun 29,2023 Jun29.2023 GAS Airgas. & Alr Lhuide cmparry Cusbmer Part Number Cy{indar Number Laboratory: Analy3b Date: Lot Numbor kimary Standad Gas Component ReqfGonc ETHYLENE NITROGEN ilot |:GREAT PLAINS ANAL CERTIFIED BY FTIR AppDr,.dfurR.L... etutuSpcddVCrs AirtuUSAUa 12722 g. Watmrth AE. Chiogo, IL6o628 lttof!.@ OFAIIIALYSIS STATTIDARI) ReErcnce Number 54.{i02811378-1 Cy,llndervoluma: '144.0 CF Clllndor Pro$ule: 2015 PSIGVahrsoutot 350 , yseights and/a N.I.S.T. G6 Mbture rcftrcnce materials. RESI.'LTS Gonccntretlon Anaffical Uncoftalnty +l- 1c* P.go I otl Explradon Dft: Airgas. 3n Ar Lqude lmp€rry BIP AiryuMtd Southrcgion Airgs USA LLC 9741 E. S6th SL North l\lsa, OK74u7 AirgE.@m CERTIFICAIE OF BATCH ANALYSIS Grade of Product: BIp-BUfLT IN PURIFIER Part Number: Cylinder Analfzed: Laboratory: Analysis Date: Component Nt BtP300 TWo$867349 106 - Tulse Fast Fi[ (SAp) - OK Feb 10,2016 Reference Number: 29-400672389-1 Cylinder Volume: 304.0 CF Cylinder Pressure: 2O4O pSlG Roquosbd Gertlfled WATER TOTAL HYDROCARBONS CARBON DIOXIDE CARBON MONOXIDE 1 PPM 1 PPM 0.1 PPM 0.5 PPM 0.5 PPM 0.94 PPM 0.058 PPM 0.1 PPM 0.235 PPM 0.235 PPM Permanent Not'3:This cart includes val, Salos Repres€ntative for this infomatbn. C-tfllnders ln B.tch: 4263617Y, TW04671107, TWO+831574, TW0S865966, TWO$867349, TW0$867538, TWO5-867578, TW0S81687, TWOS-881820,TW0S920689, TW0S92o76o, TW05848694, TW05867441,TW058g7265, TW05897512, TW05920678, TW05920686, TW05920695,TW0592078 1, TW05920874 tmpurities vedrred against anaryticar stanaa@ Approved for Release Prg. t ol I GAS *itg"*,$' 21o/o 02 Air88 SIEcisltY GaG Air86 USALrc 525 North Indstrisl IeP Road To@le, tIT 84074 Ar18a.@m CERTIFICATE OF AIYALYSIS Grade of Product: EPAPROTOCOL STAI{DARI) Part Number: Cylinder Number: Laboratory: PGVP Number: Gas Code: E02N179E15A00B1 cc76460 124 -Tooele (SAP) - UT 872023 02.BALN Reference Number: 153402783621'1 Cylinder Volume: 146.0 CF Cylinder Pressure: 2015 PSIG Valve Outlet: 590 Certification Date: Jul 05,2023 ileto p.rlo-.a in e@rd.ne wi$ 'EPA Tra66bility Asray end ot GeooB CalibEton (Msy 2012)'d@mdt EPA ,";il;V;;ilird tto* witr i qttdcne lcwlotgs%' Th@rro ,,i15#ilvo"1,1""f#*1t1,H"""ffi#flIlJ*i?"rJ*t,ff;I,ih'J'EEl;ffi;;#ii"jilil;-"i".ptlnr,rr*n'o,t"pp*arotth'.bo6bry' oo Trlad Daia Av.llable UPon Roquest sllnatum on flle - Approved tor Roleaso Prg. I ot I ANALYIICALRESTJLTS Componont Requosted Concrnttatlon Aciual concentratlon Proiocol Total Rolrtvo ilcttrod Unc.rtalnty t-*"Utt 0710512023OrC/cEN 21.o1.h 20.7O'h CALIBRAMON STAIYDARDS Tvm LotlD CyllnderNo Concenlailon Uncsrttlnty ExPlratlon Dato - ANALYTIOAL EQI,IIPMENT lnstrumonUilake/ilodel Analyucal Pdnclple La3t MultlPolnt Callbratlon GAS SAS Part Number: Laboratory: Analysis Date: LOT Number: SN: CERTIF'ICATE OF ANALYSIS Grade of Product: CERTIFIED STAI\DARD-PROBE Measut€d Flow Measured Flow Measurcd Flow Meu Probe Port A (Vml Port B lvm) Port C (Uml Port Srmpled lDelta oll lDelta o2l lDeha o3l Flow (I.,/m) Great Plalns Analytlcal Servlces 303 w 3d st Elk City, OK 73544 (5801225-0403 Fax: (5801?25-2612 Tri Probe Certification 8L GAS INC. 3t3t2022 A 22A8L Reference 22 Number: Stack Diameter: 8' Target Flow 3Umin Rate: Numberof 3 Points: Product performance verified by direct comparison to calibration standards traceable to N.I.S.T. *The probe listed on this form meets the multipoint traverse requirement of EPA Method 7e, section 8.4 as shown in the accompanying data. Method 7e, section 8.4 states that the multipoint traverse requirement can be satisfied by sampling via "a multi-hole probe desigred to sample at the prescribed points with a flow +/- l0 percent of mean flow rate". ANALYTICAL RESULTS Total Flow (Uml Rul Rm2 2 LPM 4 LPM 0.720 (r.00a) t.4t (7.09A) 0.660 (-r.004) 1.30 (-t.21L) 0.520 (-?.00a) t.24 (_5.82A) *Calibration conducM in accordmce with Emission M€asurement Cenrcr Grideline Dommt - EMC GD-031 31312022 DateApproved for Release Probe size: 8L "ja... rrUa ', ,, |\f!f .:' .i- "',r .-. rt. UNITED $TATHS ENVIRONMENTAL PROTECTION AGTNTY [t[$fiAtlf,H tHlAh\rGl-E PARK l.lC ?771 ] March 15,2021 Mr. Jordan Williamson CEO GAS Inc. 303 W. 3ra Street Elk City, OK73644 Dear Mr- Williamson: We are writing in response to your letter received on September 17, 2020,in which you request the approval of alternative testing procedures. The EPA's Office of Air Quality Planning and Standards (OAQPS) is the delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40 CFR parts 60 and 63 under which your request must be addressed, GAS Inc. is requesting a change to one of the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under 40 CFR part 60, Subpart JJJJ - Standards of Performance for Stationary Spark Ignition Internal Combustion Engines (Subpart JJJJ) and 40 CFR part 63, Subpart ZZZZ - National Emissions Standards for Hazardous Air Pollutants for Perfornance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ). The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR) inskumentation used to conduct this method. Specifically, you are requesting that the procedures of section 8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts JJJJ and ZZZZ, be used in lieu of section A6.4.1of ASTM D6348-03 when conducting testing using ASTM D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. In your request, you state that this alternative linearity check procedure will produce consistent results when utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct the entirety of the ASTM D6348-03 method in its current form using such an instrument. Based on our understanding of FTIR instrument principles and recognition that the requested alternative determination of detector linearity is both technically sound and contained within Method 320,we are approving the requested change. We believe that this alternative is acceptable for use for use in testing all engines subj ect to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63 , Subpart ZZZZ. Also, we will post this letter as ALT-141 on EPA's website (atwww.epa.gov/emc/broadly-applicable-approved-alternative- testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for the purposes of meeting Subparts JJJJ and ZZZZ- If you should have any questions or require further information regarding this approval, please contact David Nash of my staff at 919-541-9425 or email at nash.dave@epa.gov. Sincerely, Digitally signed by STEFFAN JOHNSON cc: STEFFAN roHNsoN rffrHil,' Steffan M. Johnson, Group Leader Measurement Technology Group Sara Ayers, EPA/OECA/OCA{AMPD, (ayres. sara@epa. gov) Melanie King, EPA/OAR/OAQPS/SPPD, (king.melanie@epa.gov) James Leather, EPA Region 6, (leatherjames@epa.gov) David Nash, EPA/OAR/OAQPS/AQAD, (nash.dave@epa.gov) Lucas Ennis GAS 580-225-0403 info@gasinc.us Type of Sources Tested: Stationary lnternal Combustion Engines. 4 Stroke Rich Burn Engines. 2 Stroke & 4 Stroke Lean Burn Engines Stationary Natural Gas Fired Generators Stationary Propane Fired Generators Gas Fired Boilers Types of Analyzers:. Gasmel DX4000 FTIR. Gasmet Portable Sampling Unit with Zirconium Oxide 02 Sensory. Testo 350. Flame lonization Detector Qualilications: Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the following Reference Methods:. EPA Method 1 & 1A - Sampling & Traverse Points. EPA Method 2 &2C - Velocity & Volumetric Flow Rate of a Gas Stream. EPA Method 3A - Oxygen. EPA Method 7E - NOX. EPA Method 10 - Carbon Monoxide. EPA Method 25A- Volatile Organic Compounds. ASTM D6348 - Extractive Fourier Transform lnfrared Spectroscopy Conducts emissions testing on a weekly basis including, but not limited to, the following test types: lnitial Compliance, Biennial Compliance, SemiannualCompliance & Quarterly Compliance. Alltests performed are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 117, PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico, Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York, Kentucky, & Mississippi. . Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State Compliance guidelines, & site-specific safety certifications. GAS eq q oo o @@ 6 NN N qc q OO O qc q oo o NN N oo @ os @ o0 0 ai d d 60 n NN N NO ( l ) \q q Nt s N NN N qq q oo o oo @ ot o qq q oo o oo o do i o i ON N o@ o oo N sl -q oo o qq q oo o o@ @ FNu? q u ? oo o NN N OO O 6$ d @6 € ro Oqq q oo o qq q oo o @@ @ @@ @ eq q oo o qq q o* o o@ @ ON S a? a ? q o@ @ @@ @ @n o aq q rO O oo o oo o oo o qq q oo o @N NN O c? o l ': OO O oo o oo o cq c oo o oo o qq q oo o oo o qq q oo o 0N t FO O ol o ? q oo o oo o oo o cg q oo o oo o oo o qq q oo o oo o oo o eq e oo o oo o oo o oo o do o oo o oo o qc q OO O oo o oo o qe q oo o oo o oo o qq c oo o oo o oo o qq q oo o oo o oo o cq q oo o oo o oo o qg q oo o oo o oo o oo o ci c r d ooOO O qc g OO O oo o oo o oo o do d oo o OO O qc c oo o NO O oo o qq q oo o oo o oo o qq q oo o oo o oo o qq c oo o NO @@o o o o o AA q Q O O -d d 9 q q oo o o o o @{ N oo o @ o N OO O N O O Cq q N N N oo o $ $ + NN N oo @ oo o 6 0 0 oo o @ + N q9 9 + + d oo o o o o ss s oo o o @ N 7\ o O o o o - VO O O N N N o) d c i c i + + + ,- e a \ - N s oo $1 8 3 3 83 3 3 AO VL -6 N t 0 .= o o $ ix $ $ * l - 1 9s : A\ \ N H \ N N lr r o o o o ) c o o At o o o 9 0 0 0 x3 s 8 =8 8 8 VN N N g N N N 7- o 6 f ^ o 5 . 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(/ ) 5 5 5 qI R & R rl o o o V N N N 7o 5 5 NN NNN N OO O oo o gq q oo o oo o Oq P P YY Y Eo o o i= lo o o o8 8 8 (/ ) c i d d Loll o o o U) 9 q q Oo o o fI o o o oo o ! o o o P : : = rO O EE 5 5 oo o o (, / ) o @ o >s n Y @5 5 5 CD & R & FR R R OR A R NN N qq q q q ro o o o @o 6 0 0 FN O { M qq q q c oo o o o qO@OdOdo@olNoq6N\o6oociNodONsiNo\oOqoooodOqoooqo@NqNNoOONci@oOoci q q q q q q q q q q q q q c q q q q q q q q q oo o o oo o o o o o o o o o o o o o o o o Q 6@ O O O @ @ O O O O O O @ @@ O O @ @ @ @ @ { $ o N t o 6 n o $ o o o s 9 $ n @ o $ $ s t r qq q e q q c q q q q q q q q q q q q q q q B O O O O O O O o o O O O O O O o o o o o o o c i _oE E, i o. o Y Fq9l ^ oN^os ovOaNx T+ oo o o o cr c i c r c r d @o o o @ !- - o o o ,- s o o o $r ; ; ; SO O N N SO N O O ot d d d c i OO N N N oo o o o OO O O O ne q q q OO O O O ON r O S 6O O O oq c \ \ \ o,O@ O F O F$ @ O O NO O O O do d d d Ls o o o l/ N o o o ,: o o o o $o @ t s o@ @ ul - o q a ? q o EK E E A 9 oo o o o \ o oN o @ o @F O o O FO O O O ci o c i o o oo o o o oo o o o cq q q q oo o o o q q q q q q q q8 OO O O O O O O A oo o o o o o o : * 6@ 6 O @ @ @ @ U ro s N N s o o H e? c ? n t a e ? q q N oo o o o o @ o e u? - 1 0c '. \ t q 3 N@ N @ O @ @ @ i NN N N N N N N i ! oo o o o o o o o oo o o o o o o o q q q q q q q q q oo o o o o o o o @F O O * O v N ON - @ F O S 0 6 \\ q \ \ \ q q q oo o o o OO O O O cq c e q OO O O O sO S - O NO N @ O u? q q o l q ro N N N @o $ o o +o o @ o \q \ q q OO O r O NO @ O @ F 0 N O F N F N @ O O O F 6 O O O @@ O O N 6 @ O @ t @ N t $ 0 @ O $ r N O { F g C g q q q q q C q q ' : C q q C q' : ' : q q q c oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o oo o o o 9 q q q q q q c q q q q e q q q c q c q q q q q o o o o o o o o o o o o o o o o o o o o oo o O @ F O F @ N @ O r+ @ @ O I O O O O N @ @ @O 6 O O O O F F OO r ) @ O O Oo N O@ O @ O N S u' ) q q q q \ ol - q a a? q o q q q ' : q q u ? a q 9 ol OO T N N N O F O O O F N F O T o o o o o o o o o o oo o o o o o o o o o o N o o o o o o o o o o o o o oo o o o o o o o 9 q q q q q q q q q q cq q qq q q q q q q q q o o o o o o o o o o o o o o o o o o o o o o o OS O O o O T O O O O O O O N O O O O O @ O o O$ O O O N @ n O O O O O $ T O O O O O O F qq q C q ' . qC q q q C q q q q q C q q q c q o o o o o o o o o o o o o o o o o o o d d c i o o o o o o o o o o o o o o o o o o o o o o oQ oo o o oo oo o o o o o o o o o oo o o o Q q c q q q c c q c c q c c q c q q q q q q q c O O O O O O O O OO O O O OO O O O O O O O O o o o o o 6 0 o o o oo o o o o o o o o o o N o o o o $ @ o o o o o o o o o o o o o o o o l o O O @ O O 6 O O O O OO O O O O O O O O O O 9 ci c i o c , d c t d c i o d d d c i d d c , d d c i o d c i c, Or N $ O N O 6 O O @ 6 O @ O O N NO O O N T O N @ O O @ N O O $ @O O N O @ N N @ r @O a @O @ $ N @ O @ @ @ N O O @ O F Nn $ r O N q ci + c i r i r i a i + + + r i r i N a i a i N c i c i r i r i r i r t c , o r O O O O t @ O @ O O N @ N @ $ @ r r O @ @N @ N O O O - O O O O O T @ N O O O O O N N O@ \ q q c q a \ q o q \ q \ q \ 0q c q c q e \ \ @ N @. o o o o o o o o o o o o o o o o o o o d d d o o3OEo& : o3 NEo& :3 u2 TE gt (J E IO o=l NEo&*lOr @- d o -E IEz- d gOT NFZ- a g qooo?NNNooeooNq qO@@ry96Nooqo@@\ Ooo@Ono\NNoqoOo\ qo@ol (' )@odNoogoN@q qOO@o':@nNNooqoo!9- qq c q c q q q q oo o o o o o o o oo o o o o o o o @@ @ @ @ @ @ @ @ oN @ o @ N o o o oo o @ o o o t N NO t r @ O O - O qa l q a ? q . . q q NN * O + n N @ t NN N N N N N N N oo o o o o o o o oo o o o o o o o qq q q q q q q q oo o o o o o o o ON N T N N T N O @O - 9 O v O O @ qq n q a ? \ \ q 9 E n€ ' o ii o E^ ' Eoe OE >q o:*l OE zd ge@> Lt r oA g o9 +> IENOogvt -E@x od OF @ @ @ @O O - O FN S T N ;d d + r i NO N O $ oo o o o oo o o o oo o o o oo o o o SO N O O O N 6 O F N O $ O O N @ O F { I I @F @ N O O @ O ( , - O N O N @ N N F N F = \ g \ a? q \ a? q a q ol \ c 14 q o l q q o @ o o li Q N - A O @ O - O A O O O O N F N 0 - r, N $h @@ @ N O N @ N O @ t + t O @ @ t s @ 6 @ @ @ o o o o o o o o o o o o o oo o o o o o o o a o o o o o o o o o o o o o oo o o o o o o o Y O O O O OO O O O O O O O OO O O OO O O O Y ci c , d o c i c , o d o d d d d d d d d d d o d d o O N N 0 n 6 @ O O@ @ O N Oi N @ 6 6 @ @ Fe r o $ r 0 N N r o t N @ O N 6 @ @ O N o O O ! : N N O O O r F O O t @ N S $ 6 F $ O r @ { O Y N N + oi + r j N ai s N ci N d N N o N @ ai @ @ @ h NN N N N N N N N N N N N N N N N N N N N N 9P o N r S 9 9 o o s - N @ o o b E o e N o r : X F N $ : : : 1 @ O N @ @ N O O ^' . 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O F N r O N O r O' : @ $ $ ' i ' i ' 1 @ O O r N O O @ q \ i : P 6 N r j a j a j - cj d G i P ct + + P & P 6 a t x x N + N - o m ol -t roag *?oi z- d g9o: 2C gt o: o OO N O O 6 @ C l ) N * N t { N O O @ @ F o N S @ ( l ) o O O 0 N6 N O @ O @ O N @ @ @ N ON @ @ O O O N O n @ N O N N N s{ $ $ $ o i + $ * $ t + {s ( $ + s s s 9 s + $ $ $ $ o oi o i o i o i 6 , o i o i o i o i o i o i o t o t o i o i o i o i o i o t o t o i o i o i o t o i o t o t o i oi OO @ O O O O O @ O O r + O @ O N N @ O O ( { @ O @ F O O9 O O @ N N O @ $ $ O 6 @ O $ N N r t N @ @ O n @ O N @ q !q ! q ! q q !q q q q q q q q q q ! q q q q q q I (? !q @ o o 6 0 @ @ @ @ @ @ e @ @ @ I @ a @ @ @ @ @ @ @ @ @ @ a o < i d d I : OO F N O $ 6 @ N @ o O r N O + n @ N @ O O - N+ o @ N ? r r :: r . :: r: :: : : : $ l $ l $ l $ l l ! $ I $ l $ l $ l $ l A q? q ? o o o o g) o o o o o o o o o o o 6 o -o o o o o o o o - - o o d o e oo o o o o o o o o o o o o o o o o o o o o o o o o o o NN N N N N N N N N N N N N N N N N N N N N N N N N N N OO O O O O O O O O O O O O O O O O O O O O O O O O O O NN N N N N N N N N N N N N N N N N N N N N N N N N N N .b o o o o . o . o b b b b b b b b d d b o 5b o o o o NN N N N N N N N N N N N N N N N N N N N N N N N N N N NN N N N N N N N N N N N N N N N N N N N N N N N N N N oEFo6o q q q q q q q q c q q q q q q q g q c q q q q q q q q c q q qc o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o @ @ o @ o @ @ @ @ @ o o o@ o o 6 @ @ @ @ @ @ @ @ @ @ @ 60 6 ( o d E I I s 3 E I H E 8 I I 3 3 E € € € d I I d I 3 I I 3 I I 3 3 o o o o o o oo o o o o oo o o o o o o o o o o o d d o d d ; ; oo o o o o o o o o o o o o o o o o o o o oo o oo q q q o B A I I3 3 3 I I I I I3 3 3 I I 8 I I I I 3 8 I 3 3 3 3 I I 3 E ; o @ @ @ @ @ @ @ @ @6 o 6 @ @ O O 6 O O @ O @ O @ @@ @ @ @ 3 u ON $ a F @ s O O @ @ O N O O O n N @ @ O O O F O t o @ S ! p q q a l a ? o ? o ? 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N @ o o N N o o @ @ @ N d - o r N @ o o o @ N $ @ @ d d c i a i . * X 6 @ N N @ @ @ t N ON O @ O N @ @ N N @ @ $ @ + @ N O @ (t @ Q a a a oo o o o oo o o o o o o o o o o o o o o o o o o o Q Q 8 8 8 8 8 8 8 8 8 8 8 8 8 I 8 8 8 8 8 8 8 8 8 8 8 8 8 I 8 I EE d d d o o o d d d o o d c i c i d d d d d d d d d d d d o c i d d oo b aE 6F N os o o N9 qq q q @e @ O N @ O O 6 o O O @ r O O F @ O S O O n N t @@ @ O O O 6 @ O F O O O O O @ * N N @ t N o @ o - \ \ q q o q q \ o? ! ? a a o? q q q q q \ q q q \ \ q _q6 Er i o. o \ , FEgG ' o gH E Ed s (J E OE>o o:= OE z- d gi @> IE(D ' d e oe TE NOog *E It rE* q) a Q O O OO O O O O O O O @ O o @ o OS O oO $ @O O o o + O N O O O O O rO O O ( ) O O O S OO O O O F O O O O O O - -- ; F N o o o o o o o o o o o o o o o o oo o o o o o o o o o -- o o d d d d o o d d d d d d d o o o d d o d d d d d d d d c i d d ci c i O O O O OO O O O O O O O O O O O OO O O O O O O O O O OO O O o o o o o o o o o o o o o o o o o o o o o o o o o o o - -- O O q q q q q q q q c q q q q q q q q q q q q q q q c q c Q a q qg O O o o o o o o o o o o O O o o o o o Oo o o O O o O o o o o o o!OE .i O Yo .ET= NEoR i u2TE g.i (J E !o o oF NE .r O vd*lOF a6 . o -l IFZ- d ool NF Z- d ool It rOAga? 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(9 lo (9 O N O A Q q) @ q) tO o r I O O O O O N S O $N i -@ N o N @ o o o o @ N @o o 6 N o o @ o o o@ e o t o n (b N t - = ! a a 1 a (| q q a a a n n n a a a u? s a a a a a s t $ v s $ o a L $ o o o o o o o o o o o o o o o i oi o i o o o o o o o i o i o i o i oi o f oi o t E t r E P N g q 3: R S 3 I 3 3 P 3 8 I e 3 3 E I s 3 3 3 E 3 l No rt i; o @ @ @ @ @@ @ @ @ @ @ @ @ @ N N @ @ @ @ @ @ @ @ @ @ @ @ O ; (Y ) ;; d d d c i d @ @ d d d d d @ @ @ @ @ d d @ @ d d @ d c i d d d 9 a ? u; ; ; i - = ; = ; ; = g g m$ o @ N @ o F N o s o @ N @ o o F N o s o @ N @ o o - N o v R , 9 A * $ s o o o o o o 6 6 n 0 O O o O O o o O O O I a : T : I P Y ' d d o d o d 5 d d o d c i d d d ; ; ; ; ; ; ; ; ; ; ; ; - ; ; r< $t I q2 g ) ! l q ) ! r ) 0 0 0 oo o oo o o o o o o o o o o o o o o o o c L. qI q I q T C] q] N N N N N N N N N N N N N N N N N N N N N N N N N f oo o o o e a a o o o o e a e o o o o o o o o o A a e a e o E J N N N N N N N N N N N N N N N N N NI N N N N N N N N N N N N tr RF F R R R R R F R R R R R R R R R R R R R R R R R R R R R N N N N I N N - N N N N oN N N N o N N N N - N N N N N N N qq q c q q q q q q q c q q q q q q q q q q q q q q q q q oo o o o o o o o o o o o o o o o o o o o o o o o o o o o @@ @ @ @ @ o o @ o o o 6 0 0 @ @ @ @ @ @ @ @ o o @ o o o oo @ n o @ @ o $ o N O N S s + o o o ( o t o $ 0 $ o e o qq q q q q q q q q q q q q q q q q q q q c g q q q c q q oo o o o o o o o o o o o o o o o o o o o o o o o o o o o OO O O O O O O O O O O O O O O O O O O O O O O O O O O O d d d d o o c , c i c i d d d d d d o d d o d o o c i c t c i o c i d d oo o o o o o o o o o o o o o o o o o o o o o o o o o o o @@ @ @ @ @ 6 0 @ @ o 6 @ @ @ @ @ @ @ @ @ @ @ @ 6 0 @ @ @ @6 O @ N O @ N O O O n N O N 6 N O 6 @ @ O @ r N O r N N @O N o @ @ @ 6 0 N @ N @ 6 0 N S N n @ @ O @ $ 0 6 0 N N d ri r i d d d d r i N @ N r j N d ri r i ci c i d d N @ @ @ @ @ @ NN N N N N N N N N N N N N N N N N N N N N N N N N N N N Qa a a Q o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o qq c q q e q q q q q q q q q q q q c q q q q q q q q q q oo o o o o o o o o o o o o o o o o o o o o o o o o o o o OO F @ O F r N 6 O @ + N @ N O O O $ O O O N O $ N N $@ O O N O O @ @ n O t N r O O O @ O O N @ N O O S F O O q \ q o q \ q q a \ \ a? o q u ? ot q q q q q q o q \ \ \ \ q q \ o? FN r@ O O @ O O * O F { @ $ N N O F O n O O F N O N N O O O @O N @ @ O n r O o r @ O n n r O O O 6 O 0 O N N t 0 @ N q' : q C q' : . -: ' : ' : q q q q q ' : ' : q q q q q q - C q q C q oo o o o o o o o o o o o o o o o o o o o o o o o o o o o aa a a o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o ci d d d d o d c t d d d d d d d d d d d d c i c i c i c i d d d d d Qn = N O N { * @ o N 9 @ N S $ O @ O N N O N o T O O N O O$ O O @ @ @ O O O O @ t N 6 @ n o O F N @ O O r @ O O O On @ N @ F O N O O O O F g O @ O t t F 0 F O @ @ O @ O O d d ; ; ; - Gi N ; ; o o d ; d d N ; ci ; d - d d - ; ; N ; o o o o o o o o o o o o oo o o o o o o o o o o o o o o o -- a a o o o o o o o o o o o o o o o o o o o o o o o o o o o u ) qq q q q q q q q q q q q q q q c g9 g q q c q q q c q a = oo o o o o o o o o o o o o o o o o o o o o o o o o o o o \ o OO 0 T O O O O O @ O O O O O $ O O O $ O O O O O O O F O aa A N n O O O O F O O O O O O O O O O O O O O O O O F O cq q q c q c q q q q q q q q q q q q q q q q q c q q c q oo o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o 88 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 oo o o o o o o o o o o o o o o o o o o o o o o o o o o o OO O O O O O O O O O O O O O O O O O O O O O O O O O O O aa a a Q o o o o o o o o o o o o o o o o o o o - o - o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o d d d c i c i d d d o d o c i d d c i o d d d d d d d o o d o d ci tt o N 0 0 0 0 0 r N o 6 @ n @ @ o o o N N $ N N N t to N O @ @ N $ @ T N O O O N O n < - - O O O - - O N O o \ a o? a ? a ? c ? 9 \ \ q q n c\ s l s l , : , : s i n l n l , : q q q q q c, . + ON N N N N N N N N N N N N N N N N N N N N N N T N N N N (] N N Q 6 O o O @ O @ $ @ N O O O O @ N N o @ o + N o F @ 6$ 6 N N O O 6 6 @ F O O @ N t0 O $ N @ @ O O gF O O N SN N T N N N N @ N N @ O @ N @ N N O N @ @ N @ N N N N N d d d o c i c i d d d c i d o o o o o o d d c i d d d d d d d o o @@ @ N $ 6 @ S N O 0 F O m O O O O N 6 O T N O N T N G O $ N N O O r N o N O g r O O t O n N O $ N O o !O * O @ 9 q I q' : q q a q' : c q a \ 0q e \ 0C 9 n q e A o? q o C o ] ' : q ' . OO o F 6 6 F @ N O @ @ N o v o @ O N N O N 0 $ O @ r O O s@ N N N 6 0 N 6 N O 9 0 @ 0 0 N N t O * O + 6 N @ N N N oo o o o o o o o o o o o o o o o o o o o o o o o o o o o oa o o o o o o o o o o o o o o o o o o o o o o o o o o - oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o d c i d d d o o d d d d d d d d o o d o o o c i c i o d d d o$ o o o @ to o o o t @O O @ N O N N N N @ F @ O N @ @ N O @ O @ n a a c? o ? q q n t a? o ? a q a ? a a a 1 a I o? o t o? Or co6oIOdO6qOoqo .E sE €" E E OE OE >o o:; OEza g .eLt r t. / ) ' d gog {>?ENOog rE IE@: () do3 6Eo& : o!T' Nt r oR : ,t ?t g -?OE Id g *? NE ov B *eOE Ad g -? IEza g oe NF Z- d o ol It roag *?oi z- d ge ,c g? o>oe g _o6 Er i o_ o Y tsgo^Ol o x\ oN^os (- ) vOa NS Tv oEi= ood OF O N N N N O O O N T @ N o O O F $ n N O O n O O N T NO N O N N N N O O N D F O N O F O 0 @ @ N N O @ O O N N q a r y u? q q q u ? Q \ q \ q 1 q \ a \ u? q a q q n r? (? ' : ' : q .S \ N R R & R R & R K N R N K N K K R R E H R N R R R R R E E o 6 o N N s I l ! o N @ o a a a r a @ @ o s s @ @ o @ @ @ s QO - S N F >< X O N O 6 O @ $ O O $ ON O - N N @ @ N h vo N N @ N O y y o @ o @ o o N @ 6 o o r o @ o + 6 - @ o N (O d - 6 + 6 @ P P ri N d N ci d + + * <i + 6 \ o c r j d d @ ; N oy$ N o o O - O F O N $ N N N N @ O $ r @ N O O r O t r o t -t O - - N O o N o @ O O @ N o$ @ N @ @ N @ O N @ $ O $ 6 o =u ? a n n n a a n a n a n n n a 9 a a a a a a n a n n n n s L@ O O O O O O O O O O O O O O O O O O O O O O O O O O O O 'E F @ o @ r O N N O N * O o e Q o @ @ @ n N N @ N o r o O =N 6 @ 9 o o * N @ @ N o @ $ o t 6 < o o t N o o o { + o o rJ N O O @ @ @ @ @ O @ @ @ @ @ @ @ @ O @ @ @ @ @ @ @ @ @ @ @ Cr : , + c j d c j d @ o d d d d d d @ @ @ o c , c i @ c i d 6 d c j d c j d d ; $r $r $ t $ l $ t $ 1 s r l ] n g? g ? g ? q ? g ? q t q ? q 2 9 a a n n n n n 9 n s a (f ) oo o o o o o o o o o o o o o o o o o o o o o o o o o o o I- q] N N N N N N N N N N N N N N N N N N N N N N N N N N N N OO O O O O O O O O O O O O O O O O O O O O O O O O O O O JN N N N N N N N N N N N N N N N N N NN N N ( N N N N N N II R R R R R R R R R R R R R R R R R R R R R R R R R R R R R N N N N N N N N N N N N N N N N N N N N N N N N N N Ri i i N oOOooOqoocOaqo@o (\ Io9 c; :=Oo a 9. ! (g H ff t ON oo o o o o o o o o o o o o o o o o o o o o o o o o d d d o o o d c i o d o c i o c i c i c i o o o o o c i d c i o o oo o o o o o o € o o 6 @ o 6 @ o @ o o o @ @ o @ o oo o o o o n @ o t { t $ 6 0 t o $ o s n @ o o $ N qq q q q q q q q q q q q q q q q q q q q q q c q q oo o o o o o o o o o o o o o o o o o o o o o o o o qq c c q q c q c c q q c q q c q c q q q q q q q q oo o o o o o o o o o o o o o o o o o o o o o o o o OO O c l ) N N N N N N N N N N N N N N N N N N N N N N @@ @ @ @ o o @ o 6 @ @ o @ o o o @ o @ @ o @ @ @ @ @O @ N N N O F O O @ 6 O N 6 O r N @ N F t N O O N q q u ? a a q n q n sl o ? e ? a ? a l a a ol q n a? a 9 a a? q ": OO O O qo@Oqoqof)6oNNq@oNdNotsOaoootNN1ooqoooqoooqoOOod0-o\oo@o?NooeciNqu?@o@NqoO0q (f , : ol< R 'a R oR N @oRE 3EP8 5q cj os3NR OF xi t@8R oi oi No6N6 .A q =@OoO t =< oNoNoNN gqoo @€x$ YO oc j ^oYC I 9c ,u8 *6a5e$ Y+ \d '! Nooooqqoooo NN09 q oo NOqqooOO oooqoos8 ': o l oO88 doO+ oooodaoo88 dooOooOOdc , -o60 N( ,N6 i FO@\ ci o PI oEo8 -FNEo& :*l TE g -e (- ) E !o g oF NEoR : .EOFO- a g -e IEz' d g o? NF Z- d g _o6 Er i () . o Y Ftro^ Oa o 6; a € EP €OE OE>o o:= OF za g .B IL E A- d goc t>IENOog r9 IEEe -$ O F $ @ O @ O @ O @ o F N O o O @ O O N -N O @ t N O O O $ O O O F N 6 $ o N o OO O O ' 1 Y AA A A $ O @ @ @ @ @ @ @ O O @ N @ O @ @ @ O N N N NN N N N N N N N N N N N N N N N N N N N N oo o o o o o o o o o o o o o o o o o o o o o o o o OO O O O O O O O O O O O O O O O O O O O O O O O O qg q c c q q q q q q q c q c q c c q q q q q q q q oo o o o o o o o o o o o o o o o o o o o o o o o o N* O +o N NO @ O* o O O o O O O F S O O o N O o N N o O $ @ NO $ O V F T O 6 O N O O N O N O F O @ $ O e ) @@ @ N @ O @ O @ N @ O N N O N @ t @ N @ N O o d c j i - oi ; - - ; ; ; - - ; - - - ; ; - ; ; O O O O O @ @ O @ @ (O @ 6 O o N F O O @ N + O V @ @ OO O O 6 e ) O @ O @ o O O @ @ F { O O O @ N O O O t q q q q ' : ' : q ' : q q q q ' : q q ' : q C' : q q ' : ' : q q q oo o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o cq q q q q q q q q q q q q q q q q q q q q q q q c oo o o o o o o o o o o o o o o o o o o o o o o o o oo O O O O N - n N O $ @ N V O O T @ N O O N o OO O O O O @ @ N @ N @ N F O O O O N F O N @ N @ 6 q q q q q c ? ry q q C. q q q q q a ? q q \ q c ? q t q '. OO O O O T N T O F T O O F O F T N N O - O -O O O O O O O O O O O O O O O O O O O O O o O O O o oo o o o o o o o o o o o o o o o o o o o o o o o (l ) ce c q q q q q q q q q q q q q q e q q q q q g c q - oo o o o o o o o o o o o o o o o o o o o o o o o o \(, oo o o o o o o o o o o o o o o o o o o 6 0 @ o o o OO O O O O N O O T T N O O O O O O O O N O O O O O oo o o o o o o o o o o o o o o o o o o o o o o o o d d d d d d d d d d d d d d d d d d d d d d o c i d d oo o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o qq q q q q c q q q q c q q q q e c q q q q q q q q oo o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o TO N N O O O O O O O O O O O O O O O O O O O O O O o! s? a ? q q q q q I q q q q q c I e q q c q q e q q c NN O T O O O O O O O O O O O O O O O O O O O O O O NO { + r $ @ F O O N N O O O @ @ O O O < r O @ N @ @@ N N O @ @ O O N O O N $ - N O O N + N $ r O r N @@ O O F O T O O O @ o $ @ @ * O - N O r O O o N s ; ; ; - d - ( ai r j N o j N s i N o j o j N N N Aj ai r j c j c j c i Aj OO O O T O T N O O @ @ O O @ N D O O $ r N @ r O N OO O O O @ @ o @ @ O 6 @ @ O @ F O @ O F O $ O g q c c q \ \ \ \ \ \ \ q \ \ q \ oq q q \ \ \ \ 0q \ OO O O O O O O O O O O O O O O O O O O O O O O O O N O O O O O o F O 6 6 O O 0 N n @ r (' ) o. + O xx = x N F @ @ N N 6 O N O O N r 6 O r t r O @ @ r 55 b 5 o q o ] as l qo q q \ o l q c ! ' : \ r | q s l qq \ \ N t ': ;A ^ ; r s o 6 o F F t o o o @ o N @ @ o N @ @ N @ o@ N @ N @ @ @ O @ N O $ @ $ @ N N N $ 6 0 oo o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o d c i d d d d c i d d d c i c i d c i c i c i d d c i d d c i c i d d d OO @ N N O o @ O N + O O @ O n @ O @ N O - XX X X - O O O $ O O N N O O @ @ O N N @ n O O N N '^ 6 O N o @ O N @ O @ + O O O r N r) $ 6 N 6 oo o o dd d d = 6 @ @ @ @ @ @ @ 6 0 @ t s @ @ @ @ @ n N N N L. N N N N N N N N N N N N N N N N N N N N N N E o o o o s S P l l , N o @ @ o P $ N - o - P o o N oN o O O O O @ = ): : l O N r O n : x @ @ O @ O X{ : : . , $ O O N v o o o o N vj -i - N @ @ @ o q{ o N t o o \: { @ N N (O d d d o c j : = & o, @ @ d c j = ri r i o i E j o ft : P d a i + N oPO O O O { N O @ O O O @ O O @ N N @ F N T O O t O N OO O O O F O $ @ N N 6 @ @ N @ O O O @ O + O 0 @ N $$ $ $ t $ * { s $ $ * t t * $ t $ s { YY Y Y Y LO O O O @ O O O O O O O O O O O O O O O O O O O O O 'F o o o @ F o $ o e N o e e o o o @ o N o N ' -= - = = : o o o N N 0 0 t @ @ @ @ o @ $ N N o $ @ LJ A ^ A > < n O O n @ @ @ @ @ @ @ @ @ @ @ @ @ @ @ O @ @ (o 5 ; ; 5 P I I P I P I I I I I I I I P P I P P 9 9 I fD N @ o o r N O s a @ N @ o o r N o s a @ N @ o o F N .O O O O O O O O O O O O O N N N ' - - - Ai A i o i A i A i \ Ai A i l Ai \ Ai N oi o i ( ( Ai \ Ai oi o i oi CD O O O O O O O O O O O O O O O O O O (' O O O M O O O LN N N N N N N N N N N N N N N N N N N N N N N N N N OO O O O O O O O O O O O O O O O O O O O O O O O O JN N N N N N N N N N N N N N N N N N N N N N N N N N II O O O O OO O O O O O O O O O O O OO O O O O O O O NN N N N N N N N N N N N N N N N N N N N N N N N N N, N N N N N N- , N N N N N N N N N N N N N N N N N N N ol IEOAg *eOF 2- d ge o>ze ge ,\ c vo g N^os (J vOa NN Ie oEi=ooo gq g c q oo o o o @o o o @ oo o o o qq q c c oo o o o qq q q q q q OO O O O O O o@ @ @ @ @ @ NN F N N N N qq q c q q q oo o o o o o qq c oo o oo @ FO O qq q oo o OO O NN N 66 0 qq q oo o o@ o OO O ': q a ? oo o oi o i oi NN N oo o @- @ nq q @@ N @@ @ q q c q qc q oo o o o o o @@ @ @ o o @ e? a p p bg o 99 9 q i 5 5 q OO O o c ; c i o _o 6 Er i o. o y FEg: : ' k\o c-3 ff . 8 E^ ' E ,. r E OE>q o:"l OEzi g?@> LE rr ' ) ' d gog IENOog sE -t r@x od : oF OEo& : o! NEo& :; +E -q g_e OE IO goF NEoR : *lOF O- d g_e IEzd . gRE Z- d q qq q c q oo o o o NN N N N @@ @ @ @ o@ o o o \- : c ! a ? q OO O O O qq q q q q q oo o o o o o NN N N N N N o@ @ @ @ @ @ NO O O < N O 1a ? q ' : u ? 9 a ? FN O O O O O no o 6 6 0 0 NN N N N N N @T O D O N a\ \ q ' : \ q {6 @ N N N @ $s $ $ 9 $ t NN N N N N N OO F @ N O O (r o + t $ o N qq q q q q q oo o o o o o FN @ N O OO O F N O N ': q q q u ? ' : q NN O N N O N q g q c th q PA P Q d ; d ; o s s s s gs s NN N { = o o c? q a a? 5i 5 q ;; O P 9 N o S5 o -: - . 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A =E = E = <o OO O O O oo o o o OO O O O cr c r c i d c i Nr N @ O O N oo o o N t o Or @ N O O dd d o d d o oo o o o o o oo o o o o o oo o o o o o ci o d o o c r c i ts O O r @ O N NN O O O O q9 0 l o l q r y q oo o o o OO O O O qc q c q oo o o o OO F O O NO N O N tr 0 O -- ; c i ; @o N @ o NO * @ u? q \ \ o q OO O O O oo o o o qq q c c oo o o o oo o o o oo o o o qg g q g oo o o o oo o o o oo o o o qq q q c oo o o o NO O 6 0 N O 6F $ + m F o $N N O F N O +d @ N N N d $t + t $ + + NN N N N N N -N @ N @ @ N NN + @ N 6 N \1 q q o ? q q oN O @ O t @ @o o o o o o $t $ s $ $ t NO N N O O N ot n @ 0 N $ (o @ @ @ @ @ @ ++ s $ $ + + o8 8 8 8 8 o) c c q e c LO O O O O :]O- P B x 8 8 5q 5 q q '( / , d 9 d ? ? oFg g B E ? 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A OX K H (L R R R NN N oo o oo o qq e oo o *@qq q oo o !' ) o o o Fq t g ? g ? ol l l P O O O (, N 9 . ! N OK K H no b o NN N }S S $N N O O 6 O @@ @ o n 6 0 9$ $ t r F O oi o i o i o t c t d d Ef ; E H m s = ;; ; ; a i _ { ? :: ( f ) R R 3 \ g, 9 I 5 NN N N , < L N : oo o o ' I o o \9 . ! \ N 2 ( / , N RR R R tr dR RR R R MR NN N N N ooOr c, c i c i oo o OO O cq q oo o OO O oo o qq q OO O oo o oo o qc q oo o OO O oo o qq q oo o oN o oo o qq q oo o oo o oo o qq q oo o NO O 6r N \o ? q @@ o oo o ON O o@ o ON O dd o -t r o ? + N O@ O N O F N .q q C C q c l FO O r r o s@ o @ @ t N FN O O O N N @o O 6 @ F N oi o i o i N N d o i rN O 9 t s @ O ON O O N F O o? 0 q q q q q q oo o o o oo o 6 o qq q c c oo o o o @O O O r o OO O T O t O qa ' : q n q ' : oN o o o o o oo o o o o o oo o o o o o qq q q c q q oo o o o o o OO N so o qu ? q oo o OO O O O oo o o o qq q q q oo o o o oo o oo o oo o ci d d oo o oo o oo o ci o c i RS Ie oEtr@oo U'o <. (\ lOCJ@I4-, a9 q oo o oo 6Eq E oo o oo o oi d o i NN N ao 6 a o NO O oo ! t ct c i d EE E oo oEE E oo o oN @ 6@ + +6 6 dc i c i EE E oo oEg E oo oEE E oo o EE E oo oEE E oo oEE E ct c i ci EE E oo o oo o 88 8 oo o {o N rl s O o3 N ;; ; @o N 66 @ N( O F EE E dc i dEE E oo oEE E oo o oo o 88 8 ci o oEg E 9c i 9 oo o !t ! i tt Ss s oo o NN N oo o NN N oo oss s EE . O hxvo *f i E EE g oeOE>8:*lOE zd A .a II Eu, d _ A oe +EBE !t a iEEE9EEE fEsE :il uI ?E a dE -a g$? 8- E : *l8E g n, e -Ezd - A BEgTEoE : SEz* :eeg 8E a *-8E 40 CFR Part 60 Subpail JJJJ Performance Test Report Test Type: lnitial Test Date: 1U2M2O23 Source: Waukesha H24 Rich Burn (4 Cycle) Serial Number:1663358 Engine Hours:3600.2 Location: Duchesne Data Genter Power Station Duchesne County, Utah Prepared on Behalf of: Grusoe Energy Systems, !nc. #As ureH oTPIRTIUENT oF uvt noru ut= ttIAL-aUAL!ry 303 W. 3rd St (580) 22s-0403 Elk City , OK73644 lndex 1.0 Key Personnel.... ............. 3 2.0 Sampling System..... ....... 3 3.0 Methods Used............ ......................... 3 4.0 Test Summaries.. ............ 5 5.0 Run Summaries.. .......,,,,, 6 6.0 Volumetric Flow Rate Data.... ............. 7 7.0 Calculations.............. ...... I 8.0 Orygen Calibration... ...... I 9.0 Engine Parameter Data Sheet.. .......... 10 10.0 QA/QC Results........ ........ 11 11.0 D6348 Annexes...... ."...... 12 12.0 Signature Page........ ....... 18 13.0 Appendices.............. ....... 19 14.0 Bottle Certs............ ......... 20 1s.0 GAS ALT 141_FTrR EPA......... ...........25 16.0 Tester Qualifications (resume)... ......... 27 17 0 Raw Data . i;i;; .......... 28 Table 5.1 (Run Summaries)............. ........... 6 Table 6.1 (Volumetric Flow Rate Data)............ ............... 7 Table 6.2 (Stack Gas Measurements)......... ....................7 Table 8.1 (Oxygen Calibration).. ................. I Annex Table 1.2.1 (Certified Calibration Bottle Concentrations)......... 12 Annex Table 1.2.2 (Measurement System Capabilities)..................... 12 Annex Table 1 .3. 1 (Test Specific Target Analytes)............................. 1 3 Annex Table 4.1 (Measure System Capabilities) ............ 15 Figures Figure 6.1 (Location of Traverse Points per Method 1)....................... 7 Annex Figure 1.4.1 (Sampling Train)..... ..... 13 Annex Figure 1.4.2 (Sampling Points)... ...... 14 Annex Figure 1.4.3 (Sampling Port Locations).... ............ 14 Appendices Certified Calibration Boftle Certificates............. ...............20 GAS ALT 141_FT|R EPA............. ............... 27 Tester Qualifications (resume)... ................. 27 Raw Data.... ........ 28 1.0 Key Personnel GAS, !nc. Crusoe Energy Systems, lnc. Lucas Ennis Kody Walters 2.0 Sampling System The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet Personal Sampling System with a Zirconium Oxide oxygen sensor. 3.0 Methods Used ASTM D6348-03 This extractive FTIR based field test method is used to quantity gas phase concentrations of multiple target analytes (CO, NOX, CH2O, & VOC's)from stationary source etfluent. Because an FTIR analyzer is potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific. The analytes, detection levels, and data quality objectives are expected to change for any particular testing situation. lt is the responsibility of the tester to define the target analytes, the associated detection limits for those analytes in the particular source effluent, and the required data quality objectives for each specific test program. Provisions are included in this test method that require the tester to determine critical sampling system and instrument operational parameters, and for the conduct of QA/QC procedures. Testers following this test method will generate data that will allow an independent observer to verify the valid collection, identification, and quantification of the subject target analytes. EPA Method 1 & 1A The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at which sampling for air pollutants will be performed pursuant to regulations set forth in this part. EPA Method2 &2C This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas stream. The average gas velocity in a stack is determined from the gas density and from measurement of the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16 separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated utilizing the formulas seen in section 7.0 of this report. EPA Method 3A This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions using a continuous instrumental analyzer. Quality assurance and quality control requirements are included to assure that the tester collects data of known quality. Documentation to these specific requirements for equipment, supplies, sample collection and analysis, calculations, and data analysis will be included. Gas, lnc. 4.0 Test Summary Unit with a serial number of 1663358 which is a Waukesha H24 engine located at Duchesne Data Center Power Station and operated by Crusoe Energy Systems, lnc. was tested for emissions of: Carbon Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 1212012023 by Lucas Ennis with Great Plains Analytical Services, lnc. All quality assurance and quality control tests were within acceptable tolerances. The engine is a natural gas fired Rich Burn (4 Cycle)engine rated at 530 brake horse power (BHP)at 1800 RPM. The engine was operating at 440 BHP and 1552 RPM which is 83.00% of maximum engine load during the test. The test HP calculation can be found on page 8. The engine was running at the maximum load available at the test site. This test will satisfy the testing requirements for 40 CFR Part 60 Subpart JJJJ. Site Verification Photos Gas, lnc. 4.0 Test Gas, lnc. 6 5.0 Run Summaries Table 5.1 Run Summaries Gas, lnc. 6.0 Volumetric Flow Rate Data Table 6.1. Data used for volumetric flow rate (Method 2) 7 Pltot Tube Coefllclent CD(stdl= .99 sracx otamerer = b nches or:.5 Ieet. or:.2 Square Feel H20 o/od 16.24 16.39 16.31 16.31 co2 o/od 9.25 9.34 9.3U 9.30 02 o/od 0.53 0.45 o.37 0.45 GO ppmd 18.05 14.27 '17.54 16.62 Molecular Weiqht Stack Gas dry basis I mole 29.50 29.51 29.50 29.5't Molecular Weiqht Stack Gas wet basis (Ms q/o mole 27.63 27.63 27.63 27.63 Stack Static Pressure 'H20 0.62 0.52 o.47 0.54 Stack Static Pressure "Hq 0.05 0.04 0.03 0.04 Atmospheric Pressure at Location (Pbar MBAR 828.63 828.03 828.72 828.46 Atmospheric Pressure at Location (Pbar "Ho 24.47 24.46 24.48 24.47 Absolute Stack Pressure (Ps ,Hq 24.52 24.s0 24.s'.l,24.5'.1 Stack Temperature Deq G 441.11 442.78 438.89 440.93 Stack Temperature Deq F 826.00 829.00 822.00 825.67 Stack Temoerature Deo R 1285.67 1288.67 1281.67 1285.34 Stack Gas Velocity rusec 91.57 84.57 79.82 85.45 Stack Flow Rate Q cfs 17.98 't6.61 15.67 16.78 Stack Gas Wet Volmetric Flow Rate scf/hr 21783.37 20053.34 19042.81 20325.68 Stack Gas Dry Volumetric Flow Rate scf/hr 18245.21 16766.20 15937.50 17009.78 Emissions Samolino Points lnches Sinole Point Samolino Used 6 inches and Under 3 uamDle afler EacK ruroe.o.46 Within 5% of Last Aostd readinq:YES measured with a standard tube use for Volumetric Flow Rate Flgure 6.1 16 Traverse Points Were Used Table 6.2. Stack gas pressure rea Aostd = Velocitv head measured bv the' standard pitot tube, (in.) H2O.' stack L,rameter (tnchesl 6.OO lnches upstream lrom disturbance 48.00 lnches downstream from disturbance 32.00 Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 'The exhaust stack dld not prEsent cyclonlc flow condltlons at the sampllng locauon due to the absence of cyclones, lnertla! deml3te,!, venturl scrubbei!, or tangentlal lnlets. 'Cyclonlc Flow Check (Pass/Fall): PASS Gas, lnc. 7.0 Method 2: Determination of Stack Gas Velocitv and Volumetric Flow Rate *Note- Use of this method neqates the need for any fuel related numbers for emissions calculations Ap(avg) = Velocity head ol stack gas, mm H2O (in. H2O). 3600 = Conversion Factor, sec/hr. A = Cross-sectional area of stack, n2 (ll2). Bws = Water vapor in the gas stream (from ASTM D6348) Cp(std) = Standard pitot tube coefiicient; use 0.99 Kp = Velocity equation constant. Md = Molecular weight ol stack gas, dry basis, g/g-mole (lb./lb.-rnole). Ms = Molecular weight of stack gas, wet basis, g/g-mole (lb.flb. -mole). Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg) Pstd = Standard absolute pressure, 760 mm Hg (29.92 in. Hg). Qsd = DU volumetric stack gas flow rate corrected to standard conditions, dscm/hr. (dscf/hr.). Ts(abs) - Absolute stack temperature, oK ("R). = 460 + Ts for English units. Tstd = Standard absolute temperature, 293"K (528'R). Vs = Average stack gas velocity, m/sec (ft./sec). Md = ./t4(.093)+.32(.006)+.28(.899+.002) = 29.5O2 LB/I-B-MOLE lyls = Md(1-Bws)+18.o(Bws)Ms = 29.502(1 -.16243)+.18.0(.16243) = 27.634 LB/LB-MOLE vs = 85.+9'.99-y'62'{(zgs.6zt(24.s2'2z.694ll = 91 .57 FTlsEc Qsd = 3600(1 -Bws)Vs'A(frstd'Ps)/fis(abs)'Pstd))Osd = 3600(1-.162)91.s6s'.196(s28'24.s211 1128s.67'29.921) = 1824s.21 DSCF/HR Q = Qsd135.315 Q = 18245.2OG135.315 = 516.il2 DSCM/HR Emission Rates (Examoles use CO Run 1 453.6= Conversion factor lb. to gram HP= fnglngs rated Horsepower A = Cross-sectional area of stack, m2 (ftz). Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min) BHP/HR. = Brake work ol the engine, horsepower-hour (HP-HR.). 02 = Concentration ol orygen on a dry basis, percent. BTU/HP-HR. = Brake Specilic Fuel Consumption (HHV) ppm- Parts Per Million (CO) ER = Emission rate ol (CO) in g/HP-hr. ppm@15% 02= PPM corrected lo 15%02 F(d )= Volumes ol combustion components per unit of heat Qsd = Dry volumetric stack gas flow rate corrected content, scm/J (scf/million Btu). to standard conditions, dscm/hr. (DSCF/HR.). Q = Stack gas volumetric flow rate, in standard cubic meters Run Time = Run Time in Minutes per hour, dry basis Tpy= Tons peryear LB/HR.= Emission rate of (co) in LB/HR. vs = Average stack gas velocity, m/sec (ft./sec). Molwt.= MolWeight ol CO (28.01) ppm @ 15% 02 = PPM'((20.9-15VoO2)t(20.9-O2l)ppm @ 15% 02 = 21 .549'(20.9-15)(20.9-,6%)) = 6.209 PPM @ 1 5% 02 g/hphr = (PPM'(1 . 1 64'1 043)'Q.(Run Time/60))rBHP/H R (21.549'(1.164-10^-3f51 6.il2-(Run Time/60))t429.3 =.03 c/HP-HR LB/HR = .03'1/453.6'429.3 = .029 LB/HRlb/hr = ER'1 /453.6'BHP-HR TPY = .029'4.38 = .127 TPY ppm wet - (1(1-H2O) = ppm dry 21.55 = 18.049'(1(1-.16)) Gas, lnc. 8.0 Oxygen Calibration 9 8.1 Calibration error test; how do I confirm my analyzor calibration is corroc{? After the tester has assembled, prepared and calibrated the sampling system and analyzet, they conduct a 3-point analyzer calibration error test before the first run and again after any failed system bias test or failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level (low, mid, and high) the calibration error must be within + 2.0 percent of the calibration span. 8.2 lnitial systom bias and systsm calibration orror chocks. Before sampling begins, it is determined whether the high- level or mid-level calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample- condltioning components in system calibration mode. (1) Next, zero gas is introduced as described above. The response must be within 0.5 percent ofthe upscale gas concentration. (2) LowJevel gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be operated at the normal sampling rate during all system bias checks. (3) lf the initial system bias specification is not met, corrective action is taken. The applicable calibration enor test from Section 8.2.3 of EPA Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre- and post-run system bias must be within t 5.0 percent of the calibration span for the low-level and upscale calibration gases. 8.3 Post-run system bias chsck and drift asssssment - confirming that each sample collected is valid. Sampling may be performed for multiple runs before performing the post-run bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed final test in this case will invalidate all runs subsequent to the last passed test. (1) lf the post-run system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration enor test and system bias is passed before repeating the run. (2) After each run, the low-level and upscale drift is calculated, using Equation 7E-4 in Section 12.5 from EPA Method 7E. lf the post-run low- and upscale bias checks are passed, but the low-or upscale drift exceeds the specification in Section 13.3, the run data are valid, but a 3-point calibration error test and a system bias check must be performed and passed prior to additional testing. Table 8.1 Oxygen Calibration Method 7E 3.4 To the extent practicable, the measured emissions should be between 20 to 100 percent of the selected calibration span. This may not be practicable in some cases of low concentration measurements or testing for compliance with an emission limit when emissions are substantially less than the limit. EPA Method 3A CliA Worksheet Certlfied Gac Concentr.lon I Ceilmod Ger Concentrelon I Cortlfbd Ga. Co Low.Level (%) I ltlld.Level (%) | Hlgh.Levo flOO'/ (DIRECT) Analy.er Callbrallon Error (3 2olo) Llnoaritv Check ncentralon 7E 8.5: Note: that you may risk sampling for multiple runs before performing the poslrun bias provided you pass this test at the conclusion of the group of runs Certfied Concentralion Value (%) Dircct Calibration Response (%) Absolute Difrerence (o/o) Analfzer Calibration Enor(%) Zero Gas %0.00% 0.00%0.00% 0.00% Mid-Level Gas % High-Level Gas % 9.04o/o 20.700h 9.03% 20.510/" 0.00% 0.190/o o.o2% 0.90% (SYSTEM) Calibration Bias Checks (S 5%) and Drift Ghecks (S 3%)Upscale Gas 9.Mo/o Zero Offset 0.00% Bias Pre lnitlal Value Bias Post lnilal ValuesSpan 20.70 Analyzer Calibration RespoNe (%) Zero Gas 0.00% Systcm Calibralions Rasponse Pre (%l iystom Bias (9( of Span) Pre Syst6m Calibration Response Pcst (ohl Systam Elias (% of Span) Post Dffi(%of Span) 0.00%0.000/"0.000/.0.00% 0.00% Upscale Gas 9.03o/o 9.02Yo 0.0s%9.02o/o 0.06%0.00% (SYSTEM) Calibration Bias Checks (S 5%) and Driff Check (S 3%) Avg. Gas Concentration (Run 1)0.84% Effluent Gas (Coas) Run 1 0.il% Avg. Gas Concentration (Run 2)0.il6h Effluent Gas (Cgas) Run 2 o.*% Avg. Gas Concentsation (Run 3)0.45o/o Efflueni Gas (Cga8) Run 3 o.450/" EPA Method 3A Cl,A Worksheet Zero Gas 100o/o Nikogen Mid-Level Gas 9.04o/o High-Level Gas 20.7004 Zero Gas o/o Mid-Level Gas % High-Level Gas % zero Gas % ]-o%-l upscare used upscate Cat I g.ozy" | 9.04o/o zero Gas y" f];iill upscar€ us€d Upscate Cal I g.oz* | 9.O4yo Gas, lnc. 10 9.0 Engine Parameter Data Sheet Run 1 Run 2 Run 3 Completed Company Grusoe Enerqy Systems, lnc. Faclllty lJuche8ne Data Center Power Station Date 12t20t2023 SIte Elevatlon (ft)5844 Unlt lD Make Waukesha Model t124 Serial Number 16633s8 Technlclan Lucas Ennis Run Start Tlmes 01:31 PM 02:46 PM 03:58 PM 05:28 PM Enolne Hours 3591.2 3598.2 3599.2 sejuu.z Englne Parameter Data Run 1 Hun 2 RUN 3 Averaqe EnElne Spe6d (RPM)r 552.O 1550.O 1554.O 1552.0 htake Manllold Pressure (Dsl)37.9 36.6 3E.E 38.4 lntal(e Manllold TemO "F 12.7 t:z.J.1 tzz.z 86.O ENEINE LOAd (EHP}429.3 44C.2 +45.2 439.9 Amblent Temp "F 40.0 41 .O 40.o 40.3 Humldlw%46.0 44.O 47.O 45.7 DEW POINT "F 21.O 21.O 21.O 21.O AFR Manufacturer/Type Waukesha Waukesha waul(esha waul(esha sucilon Pressure 73.2 75.3 14.9 t4.5 Dlscharqe Pressure 3U'l 379.2 379.1 380.0 catalvst (Yes or N0 Yes cataNst Manulacturer GE GE GE GE # oI Catary$ hstalled 2 2 2 2 Catalyst lnlet Temp'F 1126.0 1125.0 1125.0 1125.3 Catalyst Outlet Temp oF 1078.0 1080.0 1078.0 1078.7 Catalyst Pressure Drop H2O 6.0 6.1 6.1 6.1 Gas, lnc. 11 10.0 OA/OC Results Time Spike Reported Spike Expected Value:249.61 Value: 251.00 System Zero Response Time System Response Time 45 seconds Nitrogen monoxide NO Nitrogen dioxide N02 NOx voc Average:0.00 Average:0.00 Average:0.00 Average:0.55 Average:0.00 CTS Compound Concentration Avg Tolerance Ditference between measured and expected Value:100.00 Value:98.56 2.O00/o 1.44o/o Nitrogen monoxide NO Nitrogen dioxide N02 NOx voc Oxygen Average:0.00 Average:0.00 Average:0.00 Average:0.00 Average:0.47 Average:0.00 CTS Bottle Concentration CTS Compound Concentration Avg Tolerance Ditference between measured and expected Value:100.00 Value:97.7O 5.00% 2.30o/o Gas, lnc. 11.0 D6348 Annexes 1-8 The test quality objectives completed for the emissir 4, 5, 6, 7 & I as layed out per ASTM D6348-03. All were within acceptable limits. Data generated durin summarized below in order of the distinctive Annex. s test are demonstrated throughout Annexes 1,2,3, rference methods, pre-test and post test procedures the pre-test and post-test procedures are analyte concentrations are the average of each test second measurement was the average of 600 scans. rex 5 Spiking Technique due to Propane being the rcess of natural gas. Additionally, the molecular of VOC's per the EPA. Three 60 minute test runs were performed. The fi run. Data was taken at 60 second intervals. Each Propane is used as the surrogate compound for the VOC that is most commonly f-ound in the combustior weight of Propane coincides with with molecular we Annex Table 1.2.1 Certlfied Bottle Concentrations Annex fable 1.2.2 System Capabllltles I I I 9"' I t I , lnc. 13 1. Annex Table 1.3.1 Test Specific Target Analytes and Data Quality Objectives Compounds Infrared Analysls Reglon (cm-l) Erpected Concentratlon Range Measuremenr System Achlevable Mlnlmum Detectable Concentratlons Hequrreq Measurement System Accuracy and Preclslon for fest Annllcatlon CO 2000-2200 0-1200 oDm 0.16267 Dom 4 oDm NO 1875-2138 0-'1000 oom 0.4007 oDm 2 DDm N02 2700-2950 0-100 oom 0.4899 oom 2 oom voc 2600-3200 0-100 ppm 1.8520 ppm Total VOC'S 1 ppmperVOC910-1 150 2550-2950 cH20 2550-2850 0-100 DDm 0./6/6 DDm 1 DDm lnterferlng Compounds * CO is analyzed in a separate analysis region than CO2 and H2O co2 926-1 150 O-1Oo/o o,/o nla Water Vapor 3200-3401 O'22o/o O.zOYo nla * VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane. .4 {-HtF_ Figure Annex 1.4.1 Sampling Train The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A heated sample line (sixty feet in length) is attached to the inlet of analyzer system and the source effluent discharges through the FTIR outlet. 1 ffi GAS STACK Gas, lnc. 14 Central Sampling Point Location in lnches TRI.PROBE SAMPLE POINT L AS PERCENTAGE OF STACK SAMPLE BY DISI Flgurc Annex 1.4.3 Sample Port Locatlon Sampllng Points LOCATION DETERMINED FROM USruRBANCE Flgure Annex lnterior Stack lnches Upstream: 48 lnches Downstream: 32 NEA#,' * nerfi.s: MDC#1 : *'n&" * cr?-rLrar RE F rr' L""tt 7'717,5 calDrafl on Tranaler Standard ExDected ueasuled Path Lenqth Yaladated tsthvlene r(x)98.56 4.924 Passed Annex Table 1.2.2 Measurement System Capabllltles Gas, lnc. Parameter Gas Concentratlon ifeasur6d 70 Dffierenee specatrcatIon vdtdated Spike Direct Propane 25't.000 ztu.51z o.19"h +l- 2"h HASS SF6 9.730 Y.b44 O.EE%+l- 2"h Pass co 501.400 4Y4.t 1.32"/o +l- 2o/o PaSs NO 252.400 z4t.E32 1.81"/o +l- zYo PaSs SDike Run 1 vla tho Svstem Source Output splke AveraEe Dilution Factor Expectecl 70 ReCOvery specification Propane 0.025 z1 19.977 109.010%7O'13O"/o SF6 0.000 o.767 7.953"/o 11Oo/o Splle Run 2 vla the System Source Output spil(e Average Dilution Factor Expected 70 ReCOvery Specilication Propane o.o00 22.564 f 20.055 112.51O4/o 70-130% SF6 0.000 v.t t1 7.995Vo 11U"/o sDlKe Hun 3 vla the svstem Source Output spil(e Average Dillrtlon Factor Expected 70 ReCOvery specllicailon Propane 0.000 z1 tY4 19.578 1.32OYo 70-130y" SF6 0.000 u. /55 7.8O8"/o 11Oo/o Noise Equivalent Absorbance (NEA) RMS High 0.000445 RMS Mid 0.00',1823 RMS Low 0.001065 Line Position 20$2 2069 :046 2023 1999',]976 1953 1930'X807 18S4 1861 1837 181{ pass Gas, lnc. n 1( 010 nntr 005 n 1n c00 005 @ o.oo% Pass The Gasmet GICCOR (Genzel lnterferometer with Cube Corner Retroreflectors) interferometer is specially designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining stable with any vibration and temperature changes. a low resolution spectrometer where the aperture is fixed to a maximum angle setting and the detector linearity was tested with an alternate approach. A three point linerarity of the CTS gas was performed and validated. Linearity 1 58 5898 148 5898 1 38 5898 128 5898 1 18 5898 108 5898 oa <Qoa 88.5898 78.5898 68 5898695 687 158.5898 148.5898 138 5898 128 5898 1 18.5898 108 5898 98 5898 88.5898 78 5898 68 5898610 602679 672 664 656 648 64.1 633 625 618 1s.2439047 The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex 7.6 POST GTS Ststem Ghecl(: u I ti E oTlte uoncenlraton.100.oo u ru lramDre uoncemralton Averaqe:99.O1 umerence between measured and exoected:.UU-/o I Oterance:5.OO7o BUn Uata Yalloaflon - Automated v3 tanual Roadlno valldated Gomrnonts Run 1 Points 1 & 2 on CO/NO/Prooane Allwithin 20%Passed uemonstrates no rntenerences oDserved, Run 2 Points 1 & 2 on CONO/Prooane All wlthln 2O7o Passed L'emonstrates no rntenerences observed Run 3 Points 1 & 2 on CO/NO/ProDane Allwithin 20%Passed Demonstrates no interferences observed, Gas, lnc. 18 12.0 Slgnature Page Job/Flle Name: Crusoe Energy Systems, lnc.; -#e,ffi+$ &v :.8E * We certify that based on review of test data, kno conducting this test, we believe the submitted inl psne Data Center Power Station; ;JJJJ \ {^-'qk;h ra nf lhnea inr{ivir{rralc diraatlv racnnncihla fnr rdilon to be accurate and comilete. Company: G.A.S. lnc. Print Name: Chris Oppel Title: Director of Stack Testing Signature: uq^< PhoneNumber: 580-22$'0403 Dale:12120f2O23 Company: G.A.S. lnc. Print Name: Lucas Ennis Title: Emissions Specialist Dale:1212012023 Gompany: Print Name: Signature: Tifle: Phone Number: Date: lnc. Appendices Gas, lnc. Spike (5 Gas) Airgas. AirtaSpeddtycuB Airgs USA LI-C 1222 S, Wentworth Ave. Chic{8o, IL 60628 AirgB.@m Part Number: Cylinder Number: Laboratory: PGVP Number: Gas Code: CERTIFICATE OF ANALYSIS Grade of Product: EPA PROTOCOL STANDARI) 805N194E15AC014 Reference Number: *402601324-1 CC142828 Cylinder Volume'. 147 .O CF 124 - Chicr.go (SAP) - lL Cylinder Pressure: 2015 PSIG812022 Valve Outlet: 660 CO,CO2,NO,NOX,PPN,BALN Certification Date: Oec06,2022 Date: Cdlifi@tir pstorhcd in .@rdane with 'EPA TEeability Preb@l turAssy .nd Clrlifatio of GasM CslibrafM Slend.rds (Msy 2012) d@ment EPA 600/R-12/531, 6ing th. .$.y peeduEs listld. Anelytiel M.hodology dG mt EquiE ffiir hr amtytiel inbrbB@. Thb cylinda has e total ssMhd une.taint s steH bebw wih a ffifidanB lewl of 95%- ThcE eE no sigdfer( impurilie6 $!ki 6f*'t thc u* of lhb calibdion mituE. Al 66batids eE oh a molcJmole ba5b unle$ othwise noted. The Gults Elat6 ory io the itere Ectcd. Thr ropon shalt nd bc EpEdu@d erept hr full wi0ujt 6pplMl of the laboEtory. Oo Trlad Data Avallable Upon Request PERMAT{ENT NOTES:Mixture contains nominal 10ppm Sulfur tlexafiuoride as a tracer component Aciual tested value included within the original Certificate of Analysis. Contact the Airgas laboratory if a reprint is required NOTES:Mixture contains nominal 10ppm Sulfur Hexafluoride as a tracer component. Aciual tested value included within the original Certificate of Analysis. Contacl the Argas laboratory if a reprint is required. SF6 Results: JMR137-9.73[PPMn r r n n rl n I FN Approved for Releare Pr!. I ot I Compononl ANALYNCALRESII'LTS Requestod Ac'tual Protocol Total Relatlve Concentra0on Conc.ntrrtlon Method Uncert lnty A$.y Dates NOX 250.0PPM 253.0PPM Gl +/-1.2%NISTTE€able 1112U20?2,121O81202. N|TRIC OXIDE 250.0 PPM 252.4PPM Gl +/- 1.0% N|ST TEffible 11t2812022,1?i06t2022 PROPANE 250.0 PPM 251.0 PPM G1 +^ 0.7% NIST TEeabb 1'113U2022 CARBON MONOXIDE 500.0 PPM 501.4 PPM Gl +/- 0.6% NIST TBffibte 11129/2022 CARBON DIOXIDE 5.m0 % 5.025% c'l +/- 1.4% NIST TEeable 11t2U2022 NITROGEN Bdane CALIBRAIIONSTANDARDSType Lot lD Cyllndor No Concentratldr Unc€i.lnty ErDlratlon Dato EB0113125 250.3 PPM NtIRtC OXTDE/NtTROct D685025 9,9lPPMNITROGENDIOXIDE/AIR +/- 0.8% +l- 2.oor'" +l-2.0% +/- 0.5% +/- 0.6% +/- 0.6% tu 29, 2026 Feb20,2020 Feb 18,2023 Mar 17,2027 Jlt03,2024 May 14,2025 NTRM 200503-31 PRM 12386 GMIS 401423838104 CC505590 4.373 ppM NTTROGEN O|OX|DSNITROGEN NTRM 200602-13 NTRM 13010109 NTRM 13060423 6162697Y 243.3 PPM PROPANE/AIR KALOO3925 495.4 PPM CARBON MONOXIDE/NITROGEN cot't3685 7.489 % CARmN DIOX|DE/N|TROGEN The SRM. NrRM. PRM. d RGM notsd ebove 16 onlv in r6f6r6n6 to lh. GMIS md ln the s$v.nd hot Bd dh ANALYTICALEQUIPMENTlnstrumonutake,Uodol Analytbrl PdnclDlo Lr3t ilultDolnt Callbr.tlon Ni@let lS50 AUP2010242 CO-1 SIEMENS ULTFAMAT6E N1J57OO Ni@lei iS50 AUP2010242 Ni@let iS50 AUP2010242 Ni@let iS50 AUP2110277 NN07,2022 NoY 28,2022 Dec.05,2022 D@05,20?2. NN O7 2022 FTIR NDIR FTIR FTIR FTIR Gas, lnc. Airuas. d Ar Lqurd€ cmpany 9% O2INO2 AirtuSpccidtyGu6 Ail8a USA Ua 525 North Induskial Inp Road T@le, UT84074 Ahza.@m CERTIFICATE OF ANALYSTS Grade of Product: EPA PROTOCOL STANDARI) Part Number: Cy,linder Number: Laboratory: PGVP Number: Gas Code: E03N|90E15W0003 cc517745 124 - Tooele (SAP) - UT 872023 NO2,02,BALN Reference Numb€r: 153.402786436-1 Cylinder Volume: 145.0 CF Cylinder Pressure: 2015 PSIG Valve Outlet 660 CertificationDate: Jul13,2023 trEL./molc b.dr mLs odlwiec mtad. Tha cuh6 roleta illy io tha lbm Hcd. Th. Epod 3hall Td.d Drt Avrll.ble Upon Roque3t Approved for Rslearo h tull withdit +plwl of th. l.boEtory. Do Prg! I ol I Cst'fi€tdr pdturrud an .@rdan@ wilh 'EPA TE€.bility PDb@l br Assy.nd C€rtifetid of G.ffi C.lioctih Sf.nd{d8 (M.y 2012)' d@mnt EPA 6{XrlR-12/531. Eing the .sy pl@duE8 listld. Amlyth.l M.hodology dG not Equh! mdon tu eBlyli:.|inbrftGr. Thb cylindd has a tdc .nstfi6l un€ti.inty s. st bd b.k , wlth . ffilldcne l.wl of 95%. Th.E .E rc Bilrnifont impuitior wfiiirr alt c{ tho us of thb cdib..lhn mixtuE. Al m@ffiida .E m a Not t 8. Thb 1(x)i.c. 0.7 ANALYTICAL REST,'LTS Raquested Acfual Protocol Totrl Rola0ve Conc.nt.flon Concontreflon U.thod Uncortdnw Comporenl Arsay Datos NITROGENDIOXIDE 100.0PPM 10'|.9PPM Gl +/-2.0%NlSTTEeable O7l06,lm23,O7l1WO23 OXYGEN 9.000 % 9.037 oh Gl +/- 1.0% NIST TB€able 07106112023 NITROGEN Balane CALIBRATIONSTANDARDS Typc Lot lD Cyllndcr No Concont luon Uncort lnty Erplratlon Dat D887373 SG9,I61286BAL 12.05%OXYGENNITROGEN TIESRU.NTRM.PRM.dRGMmtd.bosl.onlvlnr.tffi6blh€GMISuodlnlh6*vanddMdolth. Nov 09, 2025 Frb 23, 2023 Occ 14,2023 GM|S 153/,02022601 CC517858 PRM 12420 NTRM 98051010 10,I.1 PPM NITROGEN DIOXIDE/NITROGEN 98.9 PPM NITROGEN DIOXIDE/NITROGEN 1.1% 1.0% o.7% lnatrumonutak modd ANALYIICAL EQTIIPMENT Analttc.l PrlnclDls L!3t tultlpolnt Callbrltlon FTIR 02 PaEmaqnctic (DXON) Jun23,2023 Jun29,m23 MKS FT|R NO2 018143349 Horibs MPA€10 W603MM58 02 Gas, lnc. Airgas. eArtj(iido drprry CERfIFICA OFAIYALYSIS Grade of PRIMARYSTAIVDARI) etrIlrrepcalvOrrcl AiTfUUSAIL rrra g.WattmfthAE. Ctiafo, lL5o6a8 fftsgtm Rafarcnce Number WO281137U1 Cllindervolume: 14/..0 CF CyllnderPr€ssurs: 2015PS|GVahooude* 350 +l-1L P.go t ort Cu3bmor Part Numbel: Cy,linder Numbel: Laborabry: Anailols Date: Lot Numbel: ETHITENE NITROGEN GREAT PI.AINS AMLYTICAL x02Nr99P1sACVH8 ccfi7503 12a - Chlcago (SAP) - lL tug 15,2023 5/-40,2811378.',| E:elradon Dtr: 100.0 PPM Balenca 15,2081 Primary Standard @s Minres are traceaHe b . wdghts and/fr i{.LS.T. G6 Mbtur€ r€ftren@ maElrials, ANAL RESI[[IS Component Req Gonc Goncentratlon Analytca! Unccrtalnty ilort3GREAT PI-AINS AIIIALYTICAL, CERTIFIEO BY FflR alff.luriltl. Appronrd ior Roloao BIP CERTIFICATts OT AATCH Gradc of Produttr BIP-BUILT Prt t*rno.. Hl BPilI! Ctln(brA.rlrao 1U(FB?3.0L-ilnrr MsO -T'.r$ Frnhf {gAPl - OK Arur*. Orr: fa to.4fi6 AI{ALYSIs IN PURINEN, ndrlallurfir CrfnaYffrncCr'r* Prr.rr.v&rQlr* Airms ze"r{mrrt$lslocF !0,m PSl6 eco Ccrprt A}IALYTTCAL R,ESULTS i.ir.edprrlt CruL.l Cciotiloar riltRijlcftt cxrBelt WAYEA rol^L r{rDmt^n&)0iscln66,o*,* L:ln0(rlU(.iaOIDG tt rltP r.. 9t m $ o.ia pPttr o (|!c pPtl o.r PPil 0.2t5 FPn 0 a6 pFtl lt.Irre tCf; nr{ t|ll i.r{rui6 vflr|| *!(rr ort r0ir. il{h ri Lyl irynarrtatryi d ha .r.ra. orrr Frt}. C6iltd $ lrq6r Sft Rlrfrfr*vr b ihe a{rs{r$d qlt-tr'taalr aZ3tot,'r. flr,oaaTltOr, n\S*'{Jrt?4, f}tt$*|dUei lt6irrfar Tv.q}rirltrr irt0tl.,3lt fwl6{artl$l llt|s{Sld.l0 tl$rsst,.rt ?#rt lt0?fii nm6r,niot. tt60tr.ar l}r#)rl3r tt(no?!rt. tw9osr]f,I{' ?lr$$:Ijaa0, tltti&oter, Tr$llcf.,ll7.ri Wlo5rJoq7r t 'f,.rd.- vrdid rfr* rCfr** ntrndrOf pqebh le illt, n, $+a rrd,t rclFr AF!l.{tcrfdllit ,.a.rIr'.agri,'I}l { I PFt'lr I PFtl< (ItFPU r tr6 PrPll <. 0 ' 9F1U Gas, lnc. Airgas an Ar LqurcE compsy 21% 02 Airt8SFcidtycrE Airgs USA Lrc 525 North Indushial I@p Road Tmle, UT 84074 Arrte,@h CERTIFICATE OF AIVALYSIS Grade of Product: EPA PROTOCOL STANDARI) Part Number: Cylinder Number: Laboratory: PGVP Number: Gas Code: E02Nl79E15A00Bl cc76460 124 -loo,ele (SAP) - UT 872023 02,BALN Reference Number 153402783621-1 CylinderVolume: 146.0CF Cylinder Pressure: 2015 PSIG Valve Outlet: 590 Certification Date: Jul 05,2023 Date: Cdlifietkh pstomed in a@dane wilh 'EPA TEeabillty Prcto@l tor Assy.hd Ccitifetiil of G.ss CalibEiim SEnd*ds (Mey 2012)' d@hili EPA 600/R-1 2,/53l , 6ing thc .say pmeduE6 listed. AnaMi€l Mcihodology dcs not EquiE omcliril 6. anatytiel interlbE@. This cylinda has a toial .n.Micel un@rtainty a8 statad bahw wih s diid.n@ lcwl of 95%. ThcE src no sigrlfent impuriti$ wtil5 affed thc u$ ol thb calibdiril mb&c- All 66htids aE d a rElc/mole baab unl.s oth.Nia€ nobd. The Gults Elate mly to thc item tcted. Th. rcport shall nd b€ EpEduccd crept in tullwi0tdjt.ppowl of ihe leboEtory. Do Trlad Data Avallsble Upon Regu.st SldnrftrE nn f,|. Approved for Release Prg. I ot I Component Requested ConcantEtlon ANALYIICAI, RT,SI'LTS Ac-tual Prctocol Concentratlon fofiod Tot l Rolatlvo Uncort lnty Assay Dates oxYGEN 21.OO% 20.70% NITROGEN Balane Gl +/- 1.4% NIST Traeable O7|OSD023 CALTBRATION STAIYDARDSType Lot lD Cyllndor No Concsntatlon Uncortrlnty Expratlon Dato NTRi' 09061434 CC282492 22.53 % OXYGENNTTROGEN 0.4%Mav 13.2025 lnatrumonuuako/todel ANALYTICAL EQI,'IPMENT An.lytcll Pdnclple L.3t tultlpolnt Callbrrtlon Honbs MPA-510 W603MM58 02 02 Psramaon€dc (DIXON)Jun29.2023 Gas, lnc. UNITED STATES ENVIRONMENTAL PHOTTCTION AGENCY 'JESEARCH TRIANGLE PARK, NC 87717 March 15,2021 Mr. Jordan Williamson CEO GAS Inc. 303 W. 3'a Street Elk City, OK73644 Dear Mr. Williamson: We are writing in response to your leffer received on September 17, 2020, in which you request the approval of alternative testing procedures. The EPA's Office of Air Quality Planning and Standards (OAQPS) is the delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40 CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under 40 CFR part 60, Subpart JJJJ - Standards of Performance for Stationary Spark Ignition Internal Combustion Engines (Subpart JJJJ) and 40 CFR part63, Subpart ZZZZ-National Emissions Standards for Hazardous Air Pollutants for Perfornance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ). The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR) instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section 8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts JJJJ and ZZZZ, be used in lieu of section A6.4.1of ASTM D6348-03 when conducting testing using ASTM D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. In your request, you state that this alternative linearity check procedure will produce consistent results when utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct the entirety of the ASTM D6348-03 method in its current form using such an instrument. Based on our understanding of FTIR instrument principles and recognition that the requested alternative determination of detector linearity is both technically sound and contained within Method 320,we are approving the requested change. We believe that this alternative is acceptable for use for use in testing all engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. Also, we will post this letter as ALT-141 on EPA's website (atwww.epa.gov/emc/broadly-applicable-approved-alternative- testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for the purposes of meeting Subparts JJJJ and ZZZZ. lf you should have any questions or require further Nash of my staffat 919-541-9425 or ernail at regarding this approval, please contact David STEFFAN 12*850 {}[',00 Group Leader Technology Group Sara Ayers, EPA/OECA/OCA{AMPD, Melanie King, EPA/OAR/OAQPS/SPPD,melanie@epa.gov) James Leather, EPA Region 6, (leatherj ) David Nash, EPA/OAR/OAQPS/AQAD, ( JOHN Dlgltally slgned by SIEFFAH JOHNSOi'| 202t o3.t5 cc: Lucas Ennis GAS, lnc. 580-225-0403 info@gasinc.us Type of Sources Tested: Stationary lnternal Combustion Engines. 4 Stroke Rich Burn Engines. 2 Stroke & 4 Stroke Lean Burn Engines Stationary Natural Gas Fired Generators Stationary Propane Fired Generators Gas Fired Boilers Types of Analyzers:. Gasmet DX4000 FTIR. Gasmet Portable Sampling Unit with Zirconium Oxide 02 Sensory. Testo 350. Flame lonization Detector Qualifications: Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the following Reference Methods:. EPA Method 1 & 1A - Sampling & Traverse Points. EPA Method 2 &2C - Velocity & Volumetric Flow Rate of a Gas Stream. EPA Method 3A - Oxygen. EPA Method 7E - NOX. EPA Method 10 - Carbon Monoxide. EPA Method 25A- Volatile Organic Compounds. ASTM D6348 - Extractive Fourier Transform lnfrared Spectroscopy Conducts emissions testing on a weekly basis including, but not limited to, the following test types: lnitial Compliance, Biennial Compliance, Semiannual Compliance & Quarterly Compliance. Alltests performed are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ, ZZZZ, 106.512, 1 17, PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico, Oklahoma, Texas, Louisiana (land and off-shore), Arkansas, Ohio, Pennsylvania, West Virginia, New York, Kentucky, & Mississippi. . Quafterly Performance Reviews covering ongoing changes with Federal Regulations, State Compliance guidelines, & site-specific safety certifications. Gas, lnc. qq q oo o 6@ @ NN N 9q q oo o qq q OO O @@ @ cq q oo o @@ @ ge q oo o @@ @ oo o ci oo o@ o q@do+ooNqN@u?NN@aoodocoN9Nooco@oooOd@ro\IooodooodooqoNoNNCJNoIN0o?@@nooood >\ + .c l c? (U D tA . ' N _o6 Er i ' () . o l, FtrgG ' h\o .E s6 ' €S e ' "EOE>o a: ,l oc zd ge@> [t r '. / , 6 - goi +> -ENOog t?@x ot : o!OEo& -FNEo& i u) rE g -e () F IA goF NEo: 8 *eOF (/ ) a g -g IEza g o,NF z- d g *e -Eoag .eoi za gtgs 9E vo g N^os (- ) vOa !! ; < oEl=oGo oo!aooooogoo).g (Eoq) .Y=o= \tN- @rJ ) (r ) (r ) (o@ id-to= -ot,o= ottE=zEoo o.:oEo)oU' EDoEuJc)ooeo c.96U)o]oIoEooo6oocooEofo tr .! P6 trooooJ ollEz=tr f o$ o qq q oo o qq q oo o , ON N o@ @ oe N ol ': q OO O @o o qo ? o l FO O oo o qq u ? oo o NN N qq q o+ o oo o @o o FO O qq q oo o aa a @N NN O a? n ' : oo o oo o OO O ec e oo o oo o oo o qq q oo o oo o oo o oo o dd d oo o oo o qc q oo o +o o NF N q' : s l @@ { @o o cl A l Al oo o oo o ce e oo o aa a oo o dd d oo o oo o ec e oo o -@ O oo N -n a ? FO@$ o oo + ac ? a oo o oo o oo o dd d NO $ @o { u? q a @@ @ oo o o@ N qa ? n oo o o6 0 OF O oo o dd o oo o oo o cq e oo o N@ @ oo o c! a ] ': NO @ @o @ oo o ;c i c i oo o NO O oo o oo o oo o oo o oo o dd o oo o oo o qq q oo o oo o oo o dd o @@ @ qc q oo o qq q oo o NN N @o @ o{ @ 9q a ? oo o o6 6 NN N NO O \o ) q NN N NN N 00 0 qq q oo o oo o F$ o oo @ Ai 6 i d] ocU'o oo o oo o oo o nN 6 FN On\ ( i oo o 66 r ) NN N to 0 Or $ qu ? q $N @ @( o @ cc a oo o oo o oo o od d @O@N 6 ot nn oo o oo o oo o dc , c , NO N o* o qq q oo N o? o ? ol t$ @ +o o o1 a? a? oo o oo o oo o qq q oo o @$ N @o N \o ? q NN N NN N o6 6 60 0 @t N +$ r i oo o o( o N ooNN N -N t aa a o: : : oL oo $ ox x x oo o o vo o o NN N gN N N |t r ) R R R NN N oo o ii O O O o= = = i5 B B b oo o No o o o*N N R 61 5 5 5 XS B B V N N N 2b 6 5 ec e! ag NN N oo o oo o oo o dc i c i oo o oo o qe q oo o Oo @ $ OP P P LY Y Y OO O oo' I : ; ; NN N L. r o o o >g R R R vo o o NN N C\ r & & & NN N oo o oo o cc q oo o oo o oo o qq g oo o oN { FO O qo ? q oo o oo o oo o qq c oo o oo o oo o qc q oo o cq e o{ o@o @ ON $ aa A l @@ @ @@ @ oo o qq q oo o aa a dd c i @N N ooqq q oo o oo o ai $ r oo o @@ @ o@ 6 00 0 oo c i oo o g9 e oo o oo o oo o 9C q oo o N+ N @o @ dd d oo o oo o qc q oo o oo o oo o cq c oo o oo o oo o oo o do c i oo o oo o qq q oo o oo o oo o 9e q oo o oo o oo o cq c oo o oooo o oo o oo o oo o oo o od d oo o oo o cc e oo o oo o oo o q9 c oo o oo o oo o qc 9 oo o oo o oo o oo o c, c i ci oo o oo o qq q oo o oo o oo o qq q oo o oo o oo o qq q oo o oo o oo o qq c oo o oo o oo o qq q oo o oo t N@ O ON N do c i so @ oN o nn a l oo o oo o oo o dd c i G*,Go==ooE=tr oo o oo o oo o do o oo o oo o qq c oo o oo o oo o 9q q oo o oo o NO O oo o dc r c i oo o oo o oo o dc r c i oo o oo o qq q oo o oo o oo o qe 9 oo o oo o qc c oo o o6 6 oo o oo o 6o c j d Oo @ @ L- o o i< N N N LJ O O O A& R R FR R R OR R R NN N EE E E .! c i o c , ogE E E 6+ N N (/ ) Q a a E; ; ; @@ @ o ! ? rt ? Lt OP 9 P Llo o oo8 8 3 LN N N O. H R R N- N aaw qq q q q q q q oo o o o o o o 6@ O @ O @ O @ Fo r o F o o F u? a ? a n ! ' ? n q a ro o o o o o o OO O O O O O O oi o ' 6 i o i o i d o i o i NN N N N N N N @@ @ @ @ 6 0 6 NO @ @ @ @ O 0 +@ @ o n $ n 6 di ;- ; - ; - ; gg q oo o 6@ 6 qq q OO O @@ @ qq q oo o @@ @ os + oo o c, o i oi oo o oi o , ot NN N o@ o o@ N -r l ': oo o qq q OO O @o @ oN 6 oq o ? q O- N oo o oi o i oi NN N o@ @ F@ o \q o q 6n o @@ @ ,^ o o ts i u? slN oo o oo o dd c i o@ o o- S do d oo o oo o oo o dd d oo o qe q OO O oo o OO O qq c oo o oo o qc q oroo o oo o qq q OO O oo o oo o qq q oo o oo o oo o oo o dc i c i oo o OO O qq q oo o oo o OO O oo o dc , c , oo o oo o qq q oo o OO O oo N N6 0 ci d - NO @ NO N o? o q q qq q oo o @o o oo o qq q oo o _o6 E r i (- ) . o Y tsEo^ Oa o o .E sC ' !o EE^ ' EOA OE>o o:"l oc zd ge@> UE@- dgot {> IENOog t? IEE8 9o o o - o o N -a s @ o N @ N @ ft r o i r j N @ N N oo o o o o o o OO O O O O O O cq q c q q q q oo o o o o o o 0O - 0 O O r 0 @r O @ O N @ F u? \ q q \ o g \ q NN F N N - O O +$ $ o o o @ N a. l q ' : o l ': - - oo o o o o o o TO O O O O O O oo o o o o o o ac q q q q q c oo o o o o o o oCU;o t6 O O $ O @ F NO r o O F 6 @ TO O O N O N @ ri 6 d N d A i d + oo o o o o o o oo o o o o o o qq q q q q q q oo o o o o o o oo o o o o o o oo o o o o o o qq c q q q q c oo o o o o o o oo o o o o o o oo o o o o o o cc q q g q q q oo o o o o o o O@ + N r @ @ O oN 6 @ O $ + O qq q n q q n ' . OO F O N6 O N O N T O NN @ O $ $ r N ol o q q q q a ? q a oN N @ @ @ O 6 oo o o o o o o OO O O O O O O At q q q q q q q oo o o o o o o oo @ @ s N NO W : { O O 6 t fl \ \ t ( q q q q @@ @ ; F O O O oo o x o o o N oo o qq q oo o qe q oo o NN N @o @ 60 @ dd c i OO O qc c oo o oo o oo o qq q oo o NO N qa ! ' ? OO O oo o oo o qq q oo o oo o oo o qq q oo o NO O $o o qq q oo o oo o OO O cq q oo o OO O oo o OO O c, d c i oo o oo o qq q oo o qq q oo o oN C l ) oo @ ': u ? 9 NN N 06 0 NN N oN o no t q @@ @ NN N $r @ OF O o@ @ oi o i oi oN o @@ o \\ qNN N NN N qq q oo o oo o oo o oo c i oo o o, o , oi NN N 6@ @ oona u ? OO O qc q oo o oo o oo o aq q oo o o@ o tF @q\ \ oo o oo o oo o oo o dd d aa a c, c , ci oo o aa a cr c r d oo o oo o gq q oo o oo o oo o oo o cr c i o oo o oo o ce q oo o oo o oo o qq q oo o ol IEoaga? ot s 2- d gE o> geo:oe o oo o oo o oo o LO O O o?i B B 8 >q q q ao o o 9S 9 5 LN N N Oo o o a 9 . ! 9 . ! N (g H H K tr ] H H R NN - oo o oo o qq q oo o -N N 60 N c? \ q oo o NN N @r N {oN6 @++ + $@ o *o o cq c oo o oo o oo o qq q oo o oo o oo o qq q OO O oo o OO O qq q oo o oo o oo o qq q oo o @o@o o u? q \ NN N oo o -O O oo o FO N do o OO N NF O @o N dd d oo o oo o ce c oo o eE oEot o! 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Y or eu NO N 6 0 N O N O N NN N N NN O r NN N O ; Q e ) Q O O O O OO O O O O O O c ) O O O O O O O o o o o o o o o o o o o o oo o o o o o o o 6 q q I q q q q c c c q q q q c q q I q e e Q q o o o o o o o o o o o o o o o o o o o o o o c ) SN @ O N @ @ @ 6 r { O @ - O @ N 6 O O O @ o O N @ O * N O N O F N O o N o o I o @ o o a 5 \ \ q u ? \ q q \ q \ q \ oq q \ \ q a q q q qi NN @ @ { O O @ O O N T N N T N @ $ t O r O Nt $ $ @ $ N OO @ O O @ o F O N NN F F O ; a' : ol a ? e l o ? c l A l q q q - 01 , : a l q q , : q q? c? , . q OO o o o O O O O o o O o o O o O O O O O o O .E sE ' ! i i o Er 5oeOE>o o:*l oc zd gq@> IE@Agoa IENO c. ) o +9 @:od NNoiNootsN\N@@diooocioN@niNu?oo@@c,N@E E S F S E '. . O F O @ io g + o s o N -' t r o ^ o o N e 6p E € : 5 E qP c j : 5 = o SP O O N O N O- O O r @ O -. = \ q q u ? u ? oE N O € O O x' E o @ E o N I oe = S P U p (f ) ; ; p p P .f D r N o s @ O. 's s s s v v ovo - o o o o o =N I - \ \ Q N N '^ o - A O O O O gN J N N N N N @ R tr R R R R R NN N N N N oood QN r or OO N * @@ n @ O s OO O O N n O a oO O F N o @ O : @ s O N N t m + $@ o o F O q 1 n 09 c ? '. ( l e? ' : H e' : q q a o? \ oq q N 6 r @ o, l o - N r) t o s $ ;; 6 oi d Ai o @ o @ o o o i c i d Rl r o s s O 6 O * X O o N $ O O F N O s t * O ; : oo o o o o o o o o o o o o o o oo o o o o Q o o o o o o o o o o o o o o - 6 - - - - - -! f cq q q q 9 c q c q q q q c c q c q o o o o e : o o o o o o o o a o o o o o o c i d c , o o o c i o N @ N @ N O O N N @ @ ts O O N N O N N O O -$ l ro o N o o @ o @ o { o N o @ 0 $ N 6 o $ o o s : oF @ O $ O O O O @ O N N O @ @ N @ O t N O Y N a j o j r j d ^l cj N 6 N ; d N N 6j N cj - sj o j o j d o OO F O ^ O O O O t O ^ - s s o !l ! i i ' N o = P 6 6 n E d u . t o * o o o @ 5 5 q q a' : id a o! \ . Ar ", E * E E E E I € E * d c j K 3 3 3 + $ 3 e 3 R p ru r i cj c j c , N o $ o N ro @ o? TE (. ) A g *gOF Z- d ge o> ge o>oe o c,oodooqo oo o o N N o o o o oo o o o o o o o o o 0 6 o o o o N N o o o o o o o o o o o o o o o o o i q q q q' : Q I q q q q C q q e q e Q q a a q9 o o o o o o o o o o o o o o o o o o o c i c , c i o O@ @ O 0 O @ O O @ o - @ 6 O O O N O O F O * 6@ O { @r @ O N O 9 O O F O N - O O O @ - e d + d N c i d d N d Ai d + @ 6 d r i + + d N N * o o o o o o o o o o o o o o o o o o o o o o o o 8 E 8I I 8 g 8 8 8 8 8 g g g E E E E E E Ee oo o o o o o oo o o o o o oo o o o o o o o QO O O O O O O @ O O O O O O O O O O O O O 88 8 8 8 8 8 8 8 8 88 8 8 8 8 8 8 8 8 8 8 8 d d d d d c t c i d d c i o c i c , d d d d d d d d d o a € ) q) o o o o o o o o o o o o o o o o o o o a oo o oo o o o o o oo o o o o o o o o o o o q gq q q q q qq q q q q q cq q q q o o o o o o o o o o o o o o o o o o o e o e o c i d oo N O t O O O O @ O O N N O N @N @ O O N O N r + 0S E) @ Q O N @ F N O @ N O r $ + @ F O @ O @ o ) q A t I q q q q q q \ q \ o? q q o q \ q q c q o ? q TO O T ( ) O F N -@ o o o o N - P s - o o @ N o o N 6 o o P O N S O F O @ N X O @ S $ O O O @ @ F { $ Y 1 + N N N @ O N t N Y O @ O O O O $ O @ O O O .f F: $ + + d ot o i N d I o o t o j N N d ri r d { + o !@ oo o N @ o o o o o o oo o o o o o o o o o N QO O r S OO O N O O O O OO O O O O O O N @ q q q q q q q q - q q I c q q q e e q a Q ol q oo o o o o o oo o o o o o o o o o o o oo o oBOEo& : oi NEo& ; u2 ?t g -lOE !o o sENEo8 .lOF /. / J - d o -E -E1d o oe NF Z- d o oo o o o qq c q e oo o o o OO O r @ oo o @ @ oo o + * @o N o F NO < r = N$ N 6 ^i s l + d P oo o o o rO N O O oq q n q q oo o o o OO @ o O n O S O o @ O O 6 O N @ o r * N t o@ o 6 t o $ @ o N t o@ 6 n 6 0 6 s o @ o d o0 0 0 n 0 6 ( ) 0 0 0 n 6 0 06 c 6 0 0 0 @ a d, o i oi o i o t 6 i 6 i o t o i oi o i o i o i o i o i oi oi ot o i oi o i ot ci Fj . t ( ! q ) N r O o o @ O O O * o o N O F $ F @ @ @ O O O r ON O F r S @ N O @ $ O N N O @ + q q q q' : q q q cq q q q q q o? 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N q 6 @ t O O @ $ N O o + S O @ t t + S + @ @ - O @ N @ 6 F r + 8 8 I I I8 8 8 8 8 8 8 8 I 8 8 8 8 8 8 8 8 8 8 8 8 I 8 t q c e q q q s q s c q q q q I c e I a a e a a q a c q aq o o o o o o o o o o oo o o o o o o o o o o o o o oo o o Qa Q O O O O O O O O O O O OO O O O O O O O O O OO O O aa a o Q o o o o o oo o o o o o oo o o o o o o oo o o q q q q g q c q q c q q q q q q I I q c c Q q a q q q q c o o o o o o oo o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o 8 8 8 8 8 8 I 8 8 8 8 8 8 I 8 8 8 8 8 8 8 8 8 8 8 8 I 8 8 d d o o c i d d d d o o c i d d d d o o o d d o c , o d o c i d o O$ O N@ N ON N F O@ O N O@ O O N O @ O N t O N No O s - (9 - @ O O O N O O r N @ N @ O @ @ n O { @ @ O N O O A I \ q Q q q q q q a \ q q oq q q C' : q' : q \ q n q ry ' : q q o q NF N O F N N N N N N - N N N N Ng O O N F o P @ O @ N O t @ o N F O @ = = O - n o e @ r @ @ o @ N O )X O N 6 s N O O F N N F O X 1 H o O r t N -N O@ O O F@ @ Yt @@ O @ $ { @ r O @ N ' f iN OO @ N N O d rj d N d d cj N d @ 6 + + d d r + cj d + : : N i d d d + <t oo o o o o o o o o o o o o o o o o o o o o o o o o o o @ Q a o o o o o o o o o o o o o o o -o - - o o o o 6 6 6 ; qc q s c q q e q q q q q q c Q a a a a e q q q Q e a q 9 o o o o o o o o o o o d d o o o o o o o d d o o c i d o c i o o3 6Eoi NEo& ,t TE g -lOE !o o {} NEoR *EOF A- d a -l -EZ- d ool NF zd o odNoaN6ooqo@\i\Nod c@NoqaNqnNqoonlo q@N@oqoqNooqooO\N@Rl o q@N@qo9NooconoqNolo q@Noou?NNoOqo0\Nod q@N@@@d6dooqooo':eo qq@@ NN@@ N@qq@@ \nNOooOOqqoo@o FN\9@N o@A1 0l oo q6N@U' ?6Nooqo@oqNoci OdN@oaNqooqooNoqoct coN@q@aNoOo@oqoci qc q q q q q q q q q q q q c c @o o @ o @ @ o @ o o @ @ @ o o NN N N N N N N N N N N N N N N oo @ o @ @ @ o o @ @ @ @ @ @ o @O T O O T O N @ r @ O O { N N \\ \ \ q q q q n u ? q u ? a q a a QS O 6 N O @ @ N N N O N N N O q A l ' : - a? q u ? a q q 02 o l I q a q NN N N N N N O N O @ O N N T N oo o o o o o o o o o o o o o o oa o o o o o o o o o o o o o o qq c q q q q q q q q q q q q q OO O O O O O O O O O O O O O O 0@ @ O @ O @ N 0 O F O O O O 0 tO O F + N @ N O O O O N @ N @ @ q \ q o q q \ q oq o q q o q q o g \ \ \ Or @ 6 @ O O N N T N @ N N r O NN F O O F O $ N N @ o @ $ N O q n ol R l o l A l o l ' : ' : -, : a, : ^i , : , : oo o o o o o o o o o o o o o o OS O N O N N N N N T S O @ S O 6 $ O - @ O @ N N - o O @ O O O @ O : . O 6 r $ o o 6 $ N o o o O : : N 6 N N o 5 N o N s F @ @ a ? il i q q q \ q \ \ ' : c q N e q Ej a \ q q , . D9 rj ; qr d @ N o ; o @ o o N o r N @ o o @ o J o @ t @ N ; k ' i o$ N o o o N x l Nd ) o o o N N N N O O - \ NO t O O x = *loag E E E E E E E 3 E E E E E E E E E E E E E E E E E E E EE o o o o o o o o o d o c i c i o o o c i o o o o o o o o d o c i o N 6r t N O @ OO $ $ O S @ @ N N N OO O @ N @ $ N Oo i @S O O N O N N T t s N O N @ + N @ - n O @ O O < O O - 6 4 a? q ' : ' : al s l u ? a q a q st o t q u ? q a q \ \ ct , : - a o o o 6 e N N N N N N N o N a @ o N N s N N o s N o o N N q ol r i ci o = P n I o * I P @ o F o o I o o o o o F 6' ^ @ o 6 t o o E SB S P X R S S H E S E ; S E E E E E E e E + P $ E E E E : P @ X o P o $ ej d d d ; N d d d d c i I I o P P N P o d t s NI o- Z- n vqe o> ge RE vo g OO N O O O 0 O F O { O N O n N r @ $ O O O O - O O F O Io t r - N o @ @ N N @ N @ @ N N O N @ @ N N C ) O @ N @ @ E 5 u? u ? q u? a u? (| q s ? u ? (| u2 u ' ) u ? (2 u? u ? 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N dJ dr bb o o b o d o a o o o o o o o o o o a o o o a o o < b o NN N N N N N N N N N N N N N N N N N N N N N N N N N N NN N N N N N N N N N & N N N N N N N N N N N & N N N N oEFooo N^os (J v8s q q q q q c qq qq q q q q q q q q q q q q q q q q q q q q q e o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o Q a @ o o @ o @ @ @ @ o @ @ @ @ @ oo @ o @ @ o o 6 6 0 0 @ @ @ o @ - @@ @ F OO $ @r O O O O O @ ( r ) N F OO N N N r O$ O o6 @ = q a a r y a q a \ a q q q c a ol 02 0 l a q \ e? o ? \ q q q a a q n 5v O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O C i d oo o o o o o o o o o o o o o oo o o o o o oo o o C C qq S S tr i t r i d ci c i d d d d c i c t c i d o d o d d o d c i ai ai d d d c i d d @ c i o od : : N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N I { X ? @ @ @ @ @ @ @ 6 @ 6 6 6 6 @ @ @ @ @ @ @ 6 @ @ @ @ @ @ O O @ ; d a d h P @ @ @ o s @ D o o @ o N e a N o N F @ e N r o @ o o s N! ? e -1 y F o - r @ @ - @ o o 6 o o o s o @ N o * o @ N o ' : a sl o? s E R 3 ri + rt oj s : i l r i o i N Aj A j a i o l r j A j A j N Aj rj Aj ; \ d d r i r i s j N ; ; NO O O O O O O O O O O O O O O O O O O O O O O O O O O O O I O O O O O O O OO O O O O O O O O O O O O O O O O O O O O S d At q q q q q q q q q q q q q q q q q q q g g g c q q c q q e qq o o o o o oo o o o o o o o o o o o o o o oo o o o o oo o o o N @6 6 O N O0 FO N O O O N rN @ @ + O @ - r N @+ S - Oa N + @ 6 O @ r @{ N N o F N @ O nN N S N N @ O N O N $ O N @ { - t F 6 O N N @ N N N @ @ N @ r N N @ @ N O @ O @ @ @ N S @ @( o t - d - - - - - - ; ; ; - ; - - - ; - ; - ; - - - - - - ; ; ; ; -J O O O $ S O FN o* O $ OO N $O N $ O n O rO N O @ o @ @ L N $ F6 O O r @@ O { O $ @@ O @ @ r O @ N O O r S OO o o O + @ d d d d d o o o d c i c i d d d d d d d d d o o o o d o o c , d o cr d N N O o o O O o o o o o o o o o o o o o o O O o o O o o o o i . 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NEoo q l u2 rE o -l (J E !o o r3NEo& : *lOF @- d o -l IEza qol NF Z- d o oloag -eOE z- d voe ,c gt RE vo g c{ ^ O+ - ovO= NS Iv oEi= qq q e c q q q q q c q c c q g 9 g g g q g q q q q q c c oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o 6 6 @ @ @ O O @ O @ O O O O O O 6 0 0 0 0 0 @ @ O cO 6 @ @o @ @ t o N o o N o o $ o o o o o o o o o o o o o o @ @ os O O @ $ O O N @ o O O - 9 N F O O O @ F $ @ O O T N O d d o o c i d d d d d o c j d d o d o d d ci o d c j o d d - d cj 9q c q q q q q q q c q c c q q q q q q q q q g q q q q c @ @ @ 6 @ @ O @ 6 @ @ @ @ @ O @ O O O O ) O O O O O o) O O O NN N N N N N N N N N N N N N N N N N N N N N N N N N N N o@ o @ o @ @ @ @ o o @ @ o @ @ o @ o @ o o o @ @ @ o o o NA ( 9 @ \ t O @ N O @ O @ O N F O O T * t O * O o O @ N @ O a u? a ? ry o? a? q q q q o l o ? c ? q q 9 a a a a? 0 1 u ? a o? u? 6 l q q q OO O q) @ O O r @ $ O O @ 06 $ N O r @ o o @ O N $ O O N F + O q a \ oq \ o? q o? q ol q \ c? \ ol \ o? a q a oq e ol oq , : o q q \, : $N N O @ O N N O N N N O N N N N N O N N O O N M S * QO O O O O O O O O O O O O O O O O O O O O O O O O O O O ao Q a Q o o o o o o o o o o o o o o o o o o o o o o o o 9e c q q q g q q q q q q q q q q c q q c e q q c q q c q oo o o o o o o o o o o o o o o o o o o o o o o o o o o o N@ r @ O $ @ 6 N N O @ O O - o 6 O o o n N O O O O @ + O NT N F O N O T T O O @ 0 $ O O @ O @ O O O O O + N O $ 6 q q q \ q q q q \ q u? \ \ \ \ \ q q q \ q q? \ q \ q' : st sl OO N O A O S N N O O o ) O @ @ O S O O N 6 @ F N F O O N @ O @ L- (9 O m O O N @ r o) N N O O N @ o O O f ) m m N N t N O OT O O F N N T F O O T N F O N F O O O O o d d o d ci d d c i c i d d d d d d d d d c i c i d d d o c i c t d d oo o o o o o o o o o o o o o o o o o o o o o o o o o o o <) a o o o o o o o o o o o o o o o o o o o o o o o o o o o qq c q c c q e q q q q q q q q q q q q q q q q q 9 q q e oo o o o o o o o o o o o o o o o o o o o o o o o o o o o ocU'o =O @ O O @ r 6 @ N O O O { N S O t N N O @ r @ O @ N N $ oN t s o o N O o o @ N $ N 6 0 0 t o o $ o { { @ o o N o N O- O @ O O O @ O F @ S O n O O + F O O O O F @ O @ t + r i + s d ri r i d N d ri d + @ ci + d 6 ci d + d r i + d + N d + oo o o o o o o o o o o o o o o o o o o o o o o o o o o o aa o o o o o o o o o o o o o o o o o o o o o o o o o o o qq q q q q c q c 9 q Q q q c q c q q q q q q q c c c Q a oo o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o QO O O O O O O O O O O O O O O O O O O O O O O O ( ) O O O oo o o o o o o o o o o o o o o o o o o o o o o o o o o o d d o o c i c i d d d d d d o c i o o ci d o d d o d c , d d d d d oo o o o o o o o o o o o o o o o o o o o o o o o o o o o EE 8 8 8 B 8 8 E 8 E E E E 8 E E E E 8 E E 8 E E 8 E E E oo o o o o o o o o o o o o o o o o o o o o o o o o o o o q) N A N O N F n (r ) 6 O n O - N O N @ r O O O O @ 6 @ o O 6 OO O O t T N O @ N n $ O @ N O O @ r O O @ 6 6 O F O O O N N n 6 O N O N N r N O N N @ O O o r N @ O @ O O F F C) O o Ai R i N N o i N \ i s i d ci ri ei o i N ai d ol N N R i o i A i c i ri c i r i d ci o@ F o x F o o e N v @ o o { * @ o S o r o = n N O o o tO 9 6 N n = O O O O 6 O O @ N @ O r )' < @ @ (O :- O O o) r) c s @ N F N o '. $ N @ r I N O O F @ r O Y O $ @ -. 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' : q q q q q q q oo o o o o o o o o o o o o o o o o o o o o o o o OO O { r O N N o * 6 r ) O @ O N O O O O @ - O O O OO F @ O @ t O @ N O S O $ O r O n $ O O O O O O O O O O O 6 O F @ r O O € @ o r r O @ O o N N !+ @ d o c j ct r j 6j oi c i ; oi N i R i o j s l r i d d ej cj e j - Aj N ej rj o@ $ o o o N o = o N o N o @ o o l @ $ * o F @ o \ O 0 s @ @ H O N F O O O O N X N @ H i O N N O q q a q q o q @ N Y o o o o N @ N - Y o o : r N o 6 N N o o s o aj d : d d $ e $ + d o j = N rj P il N ( N OO T O O O O o O O O o O O O O O O O O @ O O O O OO $ O O O O O N O O O O O O O O O O O F O O O O c e q q q q q q c q q q q q c c q q e q o t q q q q oo o o o o o o o o o o o o o o o o o o o o o o o LN O N O N O - F @ @ 6 0 o @ O @ - O * ^ @ @ S O l; 6 (, N $ N N , ) , N @ N r N N N O - O 6 X i ; O O O P Fi q q q Y q q H q e ? q q u ? e ? a' : q' : ' : : &i q \ q Yj @ @ O F t r ^ @ W @ S O O - O - S 0 - ; 9 O O O: N F O N o N X O ON S $ O O N N , ' ^ : ; O O O oo o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o d d d d d o o o d o o o o o d o c i c i c i c i o d d d d NN \! qoo9Aqq NrNOOOooOO dc i {Foao' : .: 6&$ aOxo5q cj o98 , ;O l : _t odCr i o-38 o6oi ot P5 l: CO Yc , NOsa ONoNoNN "l IEoa q *lOF z- d oi o> o^l vq q OO SO @ N T O O N O N O @ N O m @ O 6 0 - @ N == O @ * F ( N O N F @ N T N F N N O N O O N O O O N OO r t N o t O r O O $ O N @ N @ o O N N O O R R , E d d d d ^i - + N + Aj 6 j r j A j r j o; o i o i o i N A j + d oj s i sj s@ t r o ^ @ o s N o s o ^ o N *6 = X X O O o : = 6 X o r Y l .i a i o 8 8 a I 8 8 8 R I ii : I 8 8 ii 6 E { = 3 u 8 ( ic p 5 I (o cj c , ! o d d d Aj 3 5 - ci d o R R S P ei N 6 cj R 3 N \o NN YO < N @ $ N N O @ O @ N O r @ O @ O O F O 6 @ N N OO SO @ t N o $ @ @ N o N O N N F O O O O N @ N N O O ry e? = q \ al q q q q q q q q q q q q q q q? q !q q !q q q r2 oo Lo o o o o o o o o o o o o o o o o o o o o o o o o oo E e s N e F @ @ r @ @ 9 N N @ o o v N @ @ o 0 N OO -= ix ; Or * O t r Cq N O o r @S O $ F N N 9O @ @ O F o L- , ; i ) ; N O O O O O @ O O O O O @ @ O O O @ O @ 6 O O ri r i Gt X : @ @ @ @ @ @ G j @ @ @ c i @ d d c i d @ d c i d d c i ci N@ m@ o o F N O s o @ N @ o o r N m $ o @ N @ o o F N f) ( r ) . $t n 6 6 O 6 O o 0 0 O O O O O O O O O ( ) O F \' r 6 d dd 6 6 d 6 6 6 6 d d 6 N N N N N N N N N N N N N (I ) ( Y ) vO O O o O O ( T O O O O O O O O O O O O O O O O O O O O :N N LN N N N N N N N N N N N N N N N N N N N N N N N N -= o o o o o o o o o o o o o o o o o o o o o o o o o o o sN N J N N N N N N N N N N N N N N N N N N N N qg S g e S ! 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(n d d ff db o d o - 6 . o o o o b . . b b d d b b o o o o NN N N N N N N N N N N N N N N N N N N N N N N N N N -N NN N N N N N NN N N N N N N N N N N N N N N N N N^os () J!! :F av oEi:o6o eq q q c oo o o o 66 @ O O oo o o o oo o o o ci c i c i d d 9q q q q oo o o o NN N N N @o o o @ @N @ N N q' : a ? a ? a oo o o o qq q q q g oo o o o o @o @ @ o @ N- cq c q 9 q oo o o o o oo o o o qc c q c oo o o o oo o o o oo o o o qq q q q oo o o o @- N O @ +@ $ @ N O- 6 t * cr c r d d c ; qq e q q q oo o o o o NN N N N N oo @ o o o F@ N t s 6 O NN @ O oi o i a t N o i d oo 6 0 0 0 NN N N N N or $ o r N \a q \ ' : o l 6@ @ @ N N $$ $ $ $ $ NN N N N N @N O @ @ { OO T N O T u? q q q q q o, o o o) o o @o o o o N n9 F O @ N oo o o $ 6 si s i s i 6i si si NO @ c? - q -N N cc q oo o @@ @ rN N ': q s l oo o to @ o6 N a? q ' : oo o cc e oo o o@ 6 q q e q e gg q oo o o o Q Q o @o o o @ o o @ $ \ q E qg g E oo o o o d d o qq q c c E t g RR R R R P i R R @@ @ @ @ s i d 6 3 G ff E q Fi l 3 _ J* 3 5 [ 5 ph E 8 cj N N j o j . ; ; c i oo o o o o o o oo o o o o o o oo o o o o o o ci c i c i d c i c i c i o @o O N $ O - O 6@ @ O $ ( D ; N N@ @ N O r O @ 6 -- - ; ; - - o s: $ 3 3 P 8 8 FN N N O dd d c i d < r d d oo o o o o t o oo o o o o a o oo o o o o o o oc t c i d d o o o oo o N t L . 6 o FN 0 N 6 o ) O O o@ r n o ( o o o dd c i N s * s c i OO O O O N - O oo o o o o o o oo o o o 9 q o dc i c i c r c i o o d OO O O O i N O oo o o o o e o oo o o o 9 Q o oo o c j d < i d d oo o o o o a o oo o o o o o o oo o o o o o o ci d d d c i o o c i : N@ O @ O o o O Or @ N S O O O @@ $ @ N \ r : o ri c i c i r i d N N c i oN o o t F 6 0 @@ o o o o + N @o t - o \ q s dc t N d @ @ @ N OO O O O @ ( I O oo o o o N N o oo o o o q o o ci c , d d d oc i d _o 6 Er i o. o \ , FEgc >o \ xvo6d 6 ! ii ! 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NEo& *Eot r (, - d o_l It rza ool NF Z- d a ol IEoa o -EOE z- d q^l ,c oi o>oE o NOc9 c oo o oo o oi o i ot NN N oo o qq q oo o NN N @o @ oo @ a? q q @@ @ @@ @ ': a ? q oN o oo o oo o oo o qq q oo o o6 0 @o o ': ': e? oo o oo o oo o cq q oo o oo o oo o cq q oo o oo o oo o oo o oo o OO O oo o qc q oo o oo o oo o q9 q oo o oo o oo o qq q oo o oo o OF O {N O oo o o@ o oi ; ; @N O OF O ': o ? c oN o oo o oo o oo o qq q oo o aa a oo o do d oo o oo o cq c oo o oo o oo o oo o oo o oo o oo o qq c oo o oo o oo o qc c oo o oo o oo o cc c oo o oo o qq q oo o dtrao $o o o o $o o o o oo o o o do c i c i d oo o o o $o o o o o, l g q q c oo o o o oo o @ o FO O O O $O O r N dd c i od OF O O O ON O O O c9 q c c oo o o o oo o o o oo o o o cc q q q oo o o o oo o o o oo o o o aa Q o o oo o o o o6 0 0 6 66 N r N \u ? q q ' : oo o o o NO 0 0 n o oN o @ $ N oo @ t o N ;; - c j - - oo @ { a o r@ O $ O N o? q \ q o ? q rN F N OF O 6 6 $ NO N O t t qq o ? q q 0 1 oo o o o oo o o o ce q q q oo o o o oo o o o oo o o o oo o o o do d c i c i oo o o o o oo o o o o eq c c c e oo o o o o NO O N N @ FO @ @ O O a? o g a ? \ q q oo o o o o tt 6 $ 6 6 NN N N N N ot { c o F O rN O @ @s o o o { ri d r i c i d $ *F N O o @ OO O N - O ': ( I q a c ? q oo o o o o oo o o o o oo o o o o qq q q q c oo o o o o on o N N 6 NO @ N O N a? a ? c \ o l a ? a] $@ N N O O Or N @ F O aq a ? q a o l oN o o o o oo o o o o oo o o o o qq q q q q oo o o o o o@ N o @ o oc ) ( r ) ( . ) o N qc ? q \ ' : A I o@ @ @ N N $s $ 9 t t NN N N N N @+ O r @ N 66 N O N O aa l n q e q o6 6 0 6 { oo o o o o ) ts s * t { OO O @ r O @N O 6 0 0 qq q q \ \ t* $ * $ t oN o A | N Q F o o N o - @ 35 3 i i S E B 5 8 8 8 E 8 Y f f f r f t N8 f l s q, \ \ N R f t & Ol f r O: > > '6 : > r S : S .r { o o o + , o o o + , o o o o c ) o th N N N ar r N t: ! g! 0l l q g ! N N N N 6R R R 6 R R R 6 R R R R R R 11 00 o no bb n - d 5 o o o - NN N _ N N N _ N N N N N N NF F FN F N N N N N N oo o oo o qe c oo o n@ o N@ 6 @o o ci c i ci oo o oo o cq q oo o oo o oo o qq c oo o oo o oo o cq q oo o oo o oo o qq c oo o oo o oo o oo o oo c i NF O NS N @o o ci o t ot oo o aa a qq q oo o oo o o N @o \\ q q \ oo o o o oo o o o cc 9 e q oo o o o oo o oo o qc a oo o N@ @ @o oo N dd - oo o oo o qq q oo o oo o oo o oo o dd c i aa a a a oo o o o dd d d d @o @ @ o @ N 3 6 e S E 8{ 8 No i o i + ; @ l l q oo o $ t ; : : : o P P P P P 8 8 P xx x x x o 6 x ci d d o c i o o c i E 3 [ P S EN 8 $t N o N 9 - o oi N o ; N o i o c ) d 6r a n t 6 d o@ $ @ @ + < x @o 6 6 6 q 9 X NN N @ F ; i -; s l N F o OO S O N F 6 O OO O N F O 6 O o@ @ @ @ o N o oi o i o i o i o i a i o i o N 5 g P 5 o n o o; d d b i r i 6 O o F E E E = EE o, 3 I: P I P e9 I & NN N N N , < - L N : oo o o o t r O o NN N N ( f g , q R& & & E tr 6 8 o- o - o - o - o - m R st E ! ! s u s ! NN N N T N oo o o o OO O O O oo o o o cr c , d d d o8 8 8 8 8 ct c q c c e LO O O O O :, AO O O EO A A o o 95 5 C q -. r r ? d d ? ? oFE E E A E hN N N N N o RR R R R LN N N N N IT r R R R R R NN N N N N^os () vRS Iv oEl= qq c oo o (D @ O oo o oo o do c , qc c o) o o NN N @C O E O oN o tt r i 6 oc , c i EE E oo o 88 8 oo o do c t o6 6 (o ( o t - ct c i ci dcao oo o oo o oo o od c i oN o oo o oo o oc i d @o o oo 6 oo o ci o o 88 8 oo o ct d d oo oEE E oo o OF N !t \ r @ \o l c oo o no N o6 0 \\ o ? oo o oo o oo o oc i d oo o oo o oo o dd o oo o 88 8 ci o d oo o 88 8 ci c t d EE E oo oEE E oo o EE E oo oEE E d9 e oo o g? g ? e l' - N N oo o NN N oo o NN N oo o NN N NN N _e iE o cqF xvo7 .^ Eg E i" t e o? OE>E t;OE z' d a a;LE (/ , A . got +> tEog :e--EE:el 6Eo&9; 8E ; u2 ?E -o g dE -a gsg NEoo o : a. , I 8E g .g IEZ- d a RE Z- d a fE l oa l el^t sE l za _ l ol ee l ol 8e l ql -: l 8r l 8s l -" 1 EI Test Started: 08:51 AM Test Completed: 01:20 PM #As State Gompliance Test Performance Test Report Test Type: lnitia! Test Date: 1?fi21n023 Source: Titan 130 Lean Burn (4 Cycle) Serial Number: KGl4856 Engine Hours:3538 Location: Duchesne Data Center Power Station Duchesne County, Utah Prepared on Behalf of: Crusoe Energy Systems, lnc. - ^r,l'llt o r pn n iturE rtTbF- E_NyiEq N I,IEIIAIS uA!= irv JAN - I 2A24 DIVISION OF AIR QUALIry 303 W. 3rd St (s80) 225-0403 Elk City ,OK73644 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 16.0 17.0 18.0 Raw Data.... Table 6.2 (Stack Gas Raw Data... Key Personne|......................... Sampling System........ Methods Used...............-...... Test Summaries................... Run Summaries....................... Volumetic Flow Rate Data...... Calculations Orygen Calibration... Engine Parameter Data Sheet. QA/OC Results........ D6348 Annexes...... Signature Page............ Appendices. Botile Certs. Tri Probe Certification via GAS ALT 14l-FTIR EPA........ Tester Qualifications Table 5.1 (Run Summaries)............. Table 6.1 (Volumetric Flor Rate Table 8.1 (Oxygen Calibration)..... Annex Table 1.2.1 (Ceriified Bottle Concentrations)......... Annex Table 1.2.2 (Measurement Capabilities) Annex Table 1.3.1 (Test Specilic T Analytes)..... Annex Table 4.1 (Measure System Figure 6.1 (Location of Traverse per Method 1 )....................... Annex Figure 1.4.1 (Sampling Annex Figure 1.4.2 (Sampling Annex Figure 1.4.3 (Sampling Port Certified Calibration Bottle Tri Prcbe Certification via GD-031... GAS ALT 141 FTIR EPA............... Tester Qualifications (resume)......... 2 1.0 Key Personnel GAS Crusoe Energy Systems, lnc. Lucas Ennis Kody Walters 2,0 Sampling System The sampling system used consisted of a Stainless steel probe, heated Teflon line, gas conditioning system, and a Gasmet model DX4000 FTIR analyzer. The gas conditioning system used was a Gasmet Persona! Sampling System with a Zirconium Oxide orygen sensor. 3.0 Methods Used ASTM D6348-03 This extractive FTIR based field test method is used to quantify gas phase concentrations of multiple target analytes (CO, NOX, CH2O, & VOC's)from stationary source etfluent. Because an FTIR analyzer is potentially capable of analyzing hundreds of compounds, this test method is not analyte or source specific. The analytes, detection levels, and data quality objectives are expected to change for any particular testing situation. lt is the responsibility of the tester to define the target analytes, the associated detection limits for those analytes in the particular source etfluent, and the required data quality objectives for each specific test program. Provisions are included in this test method that require the tester to determine critical sampling system and instrument operational parameters, and for the conduct of QA/QC procedures. Testers following this test method will generate data that will allow an independent observer to verify the valid collection, identilication, and quantification of the subject target analytes. EPAMethodl&1A The purpose of the method is to provide guidance for the selection of sampling ports and traverse points at which sampling for air pollutants will be performed pursuant to regulations set forth in this part. EPA Method 2 &2C This method is applicable for the determination of the average velocity and the volumetric flow rate of a gas stream. The average gas velocity in a stack is determined from the gas density and from measurement of the average velocity head with a standard pitot tube. Velocity readings are taken from each stack at 16 separate traverse points (Table 6.1) and used to determine the engines mass emissions rate, calculated utilizing the formulas seen in section 7.0 ol this report. EPA Method 3A This is a procedure for measuring oxygen (O2) and carbon dioxide (CO2) in stationary source emissions using a continuous instrumental analyzer. Quality assurance and quality control requirements are included to assure that the tester collects data of known quality. Documentation to these specific requirements for equipment, supplies, sample collection and analysis, calculations, and data analysis will be included. GAS 4.0 Test Summary Unit with a serial number of KG14856 which is a Titan 130 engine located at Duchesne Data Center Power Station and operated by Crusoe Energy Systems, lnc. was tested for emissions of: Carbon Monoxide, Oxides of Nitrogen, and Volatile Organic Compounds. The test was conducted on 1212112023 by Lucas Ennis with Great Plains Analytical Services, lnc. All quality assurance and quality control tests were within acceptable tolerances. The engine is a natura! gas fired Lean Burn (4 Cycle) engine rated at 13,364 Kilowatts (KW) at N/A RPM. The engine was operating at 11,816.59 BHP and RPM which is 86.67% of maximum engine load during the test. The test HP calculation can be found on Table 7.0. The engine was running at the maximum load available at the test site. Site Verification Photos 3 GAS 4.0 Test GAS 5 5.0 Run Summaries Table 5.1 Run Summaries GAS Pltot Tube Coefilclent Cp(std)= .99 srecx olameret = bu ncheS 0r:leet. or:19.63 square Feel H20 o/od 5.64 5.52 5.s3 5.56 co?"/od 2.93 2.84 2.84 2.87 02 o/od 14.39 14.53 14.55 't4.49 GO ppmd 0.03 0.47 0.00 o.17 Molecular Weioht Stack Gas dry basis (Md)q/q mole 29.O4 29.04 29.O4 29.04 Molecular Weiqht Stack Gas wet basis (Ms)o/o mole 28.42 28.43 28.43 28.42 Stack Static Pressure (Po)"H20 4.O4 3.89 2.93 3.62 Stack Static Pressure (Po),HO 0.30 o.29 o.22 o.27 AtmosDheric Pressure at Location (Pbar)MBAR 834.77 835.00 834.05 834.61 Atmosoheric Pressure at Location (Pbar)'Ho 24.66 24.66 24.63 24.65 Absolute Stack Pressure (Ps)"Ho 24.95 24.95 24.85 24.92 Stack Temperature Deq G 496.67 497.22 495.56 496.48 Stack Temperature Deq F 926.00 927.OO 924.OO 925.67 Stack Temperature Deq R 1385.67 1386.67 1383.67 1385.34 Stack Gas Velocitv fusec 237.g'.233.49 202.89 225.32 Stack Flow Rate Q cls 4671.43 4584.49 3983.66 u24.O9 Stack Gas Wet Volmetric Flow Rate sc?hr 5344280.7 s240139.3 4545227.O1 5055284.77 Stack Gas Dry Volumetric Flow Rate scflhr 5043050.4 4950883.6 4293739.60 4774050.86 tmlsstons samDltno Potnls - 3 Dolnl lono ltne samDltno DroD€lnches First Samolino Point aken @ 16.7o/o ol Stack Diameter 10.02 Second SamDlino Point Taken @ SOyo ot Stac Diameter 30 Third SamDlino Point Taken @ 8{1.3% of Stacl Diameter 49.98 6.0 Volumetric Flow Rate 6.1. Data used for volumetrac flow rate (Method 2) Table 6.2. Stack gas pressure measured with a standard tube use for Volumetrlc Flow Rate Aostd = Velocitv head measured bv the' standard pitot tube, (in.) H2o.' Flgure 6.1 16 Traverse Points Were UsedStack Diameter (inches)60.00 lnches upstream lrom disturbance 12.OO lnches downstream lrom disturbance 35.00 Pitot readings are taken for Method 2 calculations using measuring points outlined in Method 1 rThe exhaust stack dld not present cyclonlc flow condltlons at the sampllng locatlon duo to the absence of cyclones, Inertlal demlstetr, yenturl scrubberu, or tangentlal lnlets. 6Data Table GAS 7.0 Calculations Method 2: Determination of Stack Gas Velocitv and Volumetric Flow Rate *Note- Use of this method neoates the need for anv fuel related numbers for emissions calculations Ap(avg) = Velocity head of stack gas, mm H2O (in. H2O). 3600 = Conversion Factor, sec/hr. A = Cross-sectional area of stack, m2 (ft2). Bws = Water vapor in the gas stream (from ASTM D6348) Cp(std) = Standard pitot tube coetficient; use 0.99 Kp = Velocity equation constant. Md = Molecular weight of stack gas, dry basis, g/g-mole (lb./b.-mole). Ms = Molecular weight ol stack gas, wet basis, g/g-mole (lb./lb. -mole). Ps = Absolute stack pressure (Pbar+ Pg), mm Hg (in Hg) Pstd = Standard absolute pressure,760 mm Hg (29.92 in. Hg). Q5d = Dry volumetric stack gas flow rate conected to standard conditions, dscm/hr. (dsct/hr.). Ts(abs) - Absolute stack temperature, oK ('R). = 460 + Ts for English units. Tstd = Standard absolute temperature, 293'K (528 "R). Vs = Average stack gas velocity, m/sec (ft./sec). Md = .44(.029)+.32(.153)+.28(.81 8+0) = 29.044 LB/LB-MOLEMd = .M(/"CO2I+.32(/"O2)+.28(%N2+%CO) Ms - Md(l-Bws)+1 8.0(Bws)Ms = 29.044(1 -.056it7)+. 1 8.0( .O5637) = 28.421 LB/LB-MOLE vs = 8s.+9'.99-y'+.04-y'(1 gas.67(24.9s-zl.4z1ll = 237.91 FTlsEc Qsd = 3600(1 -Bws)Vs-A(fistd'Ps)(Ts(abs)'Pstd)) Q = 5043050.403/35.31 5 = 142801 .937 DSCM/HR Emission Rates (Examples use CO Run I 453.6= Conversion lactor lb. to gram HP= Engines rated Horsepower A = Cross-sectional area of stack, m2 (ll2l. Mfg.= Manufacturer Exhaust flow rate at 100% (ft3/min) BHP/HR. = Brake work of the engine, horsepower-hour (HP-HR.). 02 = Concentration of oxygen on a dry basis, percent. BTU/HP-HR. = Brake Specilic Fuel Consumption (HHV) ppm= Parts Per Million (CO) ER = Emission rate ol (CO) in g/HP-hr. ppm@15% 02= PPM corrected lo 15o/oO2 F(d )= Velurnss ol combustion components per unit of heat Qsd = DU volumetric stack gas llow rate corrected content, scm/J (scf/million Btu). to standard conditions, dscm/hr. (DSCF/HR.). Q = Stack gas volumetric flow rate, in standard cubic meters Run Time = Run Time in Minutes per hour, dry basis Tpy= Tons peryear LB/HR.= Emission rate ol (Co) in LB/HR. vs = Average stack gas velocity, m/sec (ft./sec). Molwt.= MolWeight ol CO (28.01) ppm @ 15% 02 = PPM'((20 .9-151oO2)l(2O.9-O2)l ppm @ 15% 02 =.03'(20.9-'t5)l(20.9-15.3yo)) = .032 PPM @ 15% 02 g/hphr = (PPM'(1.1 64'1oa3)-Q',(Run Time/60))rBHP/HR (.03'(1 . 1 64.1 0^-3)-1 42801 .937t(Run Time/60))/1 1 81 6.59 = 0 G/HP-HR LB/HR = 0'1/453.6'1 1816.59 = .011 LB/HR TPY = .01 1'4.38 = .048 TPY ppm wet'(1(1-H2O) = ppm dry .03 = .0285.(1(1-.06)) GAS E.0 oxygen calibration 8 8.1 Calibration error test; how do I confirm my analyzsr calibration is correc{? After the tester has assembled, prepared and calibrated the sampling system and analyzet, they conduct a 3-point analyzet calibration error test before the first run and again afier any failed system bias test or failed drift test. They then introduce the low-, mid-, and high-level calibration gases sequentially in direct calibration mode. At each calibration gas level (low, mid, and high) the calibration error must be within I 2.0 percent of the calibration span. 8.2 lnitial system bias and systsm calibration orror chocks. Before sampling begins, it is determined whether the high- level or mid-level calibration gas best approximates the emissions and it is used as the upscale gas. The upscale gas is introduced at the probe upstream of all sample- conditioning components in system calibration mode. (1) Next, zero gas is introduced as described above, The response must be within 0.5 percent ofthe upscale gas concentration. (2) Low-level gas reading is observed until it has reached a final, stable value and the results are recorded. The measurement system will be operated at the normal sampling rate during all system bias checks. (3) lf the initial system bias specification is not met, conective action is taken. The applicable calibration error test from Section 8.2.3 of EPA Method 7E is repeated along with the initial system bias check until acceptable results are achieved, after which sampling will begin. The pre- and postrun system bias must be within I 5.0 percent of the calibration span for the low-level and upscale calibration gases. 8.3 Post-run systsm bias check and drift asssssment - confirming that each sample collected is valid. Sampling may be performed for multiple runs before performing the poslrun bias or system calibration error check provided this test is passed at the conclusion of the group of runs. A failed final test in this case will invalidate all runs subsequent to the last passed test. (1) lf the postrun system bias check is not passed, then the run is invalid. The problem is then diagnosed and fixed, then another calibration error test and system bias is passed before repeating the run. (2) After each run, the low-level and upscale drift is calculated, using Equation 7E-4 in Section '12.5 from EPA Method 7E. lf the post-run low- and upscale bias checks are passed, but the low-or upscale drift exceeds the speciflcation in Section '13.3, the run data are valid, but a 3-point calibration error test and a system bias check must be performed and passed prior to additional testing. Table 8.1 Oxygen Calibration Method 7E3.4To the extent practicable, the measured emissions should be between 20 to 100 percent of the selected calibration span. This may not be practicable in some cases of low concentration measurements or testing for compliance with an emission limit when emissions are substantially less than the limit. EPA Method 3A CIA Worksheet Certified Gas Concantralon I Ceriifiod Gas Concordralon I Cortmed Ga! Co Low-Level (%) | mld-Loyel (%) | High-Levo oro./ (DIRECT) Anallzer Callbratlon Error (S 2olo) Chock ncont.aion 7E 8.5: Note: that you may risk sampling for multiple runs before performing the post-run bias provided you pass this test at the conclusion of the group of runs Certified Concenlration Value (%) Direct Calibration R$ponse (%) Absolute Difference ( Analyzer Calibration Enor (o/o) Zero Gas o/o 0.00% 0.00% 0.00% 0.00% Mid-Level Gas % High-Level Gas % 9.04% 20.70o/o 9.02o/o 20.680/0 0.01o/o O.O2o/o 0.07% 0.08% (SYSTEM) Galibration Bias Checks (S 5%) and Driff Checks (S 3%)Upscale Gas 9.04o/o Zero Offset 0.00% Bias Pre lnilial Value Bias Post lnital Values Span 20.70 Analyzer Calibration Response (%) Zero Gas 0.00% Svstem Calibrations R€sponse Pre (olrl lFtem Biss (91 of Span) Pre System Calibralion Response Posl (1/.', iystem Bias (% of Span) Post Drift (% of Span) 0.000/o 0.00%O.O0!o 0.00o/o 0.00% Upscale Gas 9.02o/o 9.01%0.080/"9.00%0.11o/o 0.00% (SYSTEill) Calibration Bias Checks (S 5%) and Drifi Checks (S 3%) Avs. Gas Concentration (Run I 15.25% Effiuent Gas (Coas) Run 1 15.31o/o Avg. Gas Concentration (Run 2)15.38%Effiuent Gas (Cgas) Run 2 15.44o/o Avg. Gas Concentration (Run 3)15.40o/o Efiluent Gas (C,gas) Run 3 15.460/o EPA Method 3A CIA Worksheet Zero Gas 100% Nitrogen Mid-Level Gas 9.O40 High-Level Gas 20.7OYo Zero Gas o/o Mid-Level Gas % High-Level Gas % zero cas 7" [G;fl upscate used upscale cat t ,!o% I s.o4% GAS 9 9.0 Engine Parameter Data Sheet AS ,4nalylicul $erra'ces. Inc Run 1 Run 2 Run 3 Completed Company Grusoe Enerov Svstems. lnc. Faclllty lJucheBne Data conter Power station Date 1'4Z1|ZUZ$ SIte Elevatlon (ft)5474 Unlt lD Make Tltan Model 130 Serlal Number KG14E56 Technlclan Lucas Ennis Run Start Tlmes 06:51 AM IO:44 AM 11:5E AM 01 :20 PM Enqlne Hours 3535 3536 3537 3538 GAS 10 10.0 OA/QC Results Equilibration Response Time Spike Reported Spike Expected Value:248.78 Value: 251.00 system zero Hesponse !rme System Response Time 45 SeCOnOS 45 seconds Nitrogen monoxide NO Nitrogen dioxide NO2 NOx voc Orygen Average:0.00 Average:0.00 Average:0.00 Average:0.01 Average:0.00 alue:100.00 CTS Compound Concentration Avg Tolerance Ditference between measured and expected Value:99.32 2.OO/" 0.68% Nitrogen monoxide NO Nitrogen dioxide NO2 NOx voc Orygen Average:0.00 Average:0.00 Average:0.00 Average:0.00 Average:0.13 Average:0.00 Mechanical Response Time CTS Bottle Concentration CTS Compound Concentration Avg Tolerance Ditference between measured and expected Value:100.00 Value:97.4O 5.00% 2.60o/" Gas, lnc. 11 11.0 D6348 Annexes 1-8 The test quality objectives completed for the emissiqns test are demonstrated throughout Annexes 1,2,3, 4, 5, 6, 7 & 8 as layed out per ASTM D6348-03. Allfeference methods, pre-test and post test procedures were within acceptable limits. Data generated durin! the pre-test and post-test procedures ard summarized below in order of the distinctive Annex.' Three 60 minute test runs were performed. The finaf analyte concentrations are the average of each test run. Data was taken at 60 second intervals. Each 6Q second measurement was the average of 600 scans. Pppale is used as the surrogate compound for the lAnnex 5 Spiking Technique due to Propane being the VOC that is most commonly found in the combustiorf process of natural gas. Additionally, the molecu-iar weight of Propane coincide's with with molecular welBht of VOC's per the-EPA. i Annex Table 1.2.1 Cefilfled Bottle Concentratlons Annex Table 1.2.2 System Capabilities GAS Annex Table 1.3.1 Test Specilic Target Analytes and Data Quality Objectives Compounds lntrared Analysls Reglon (cm-l) Expected Concentratlon Range luleasuremenr System Achlevable Mlnlmum Detectable Concentratlons l.lequrreq Measurement System Accuracy and Preclslon lor fest Appllcatlon CO 2000-2200 0-1200 ppm 0.16267 ppm 4 ppm NO 1 875-21 38 0-1000 ppm 0.4007 ppm 2 ppm NO2 2700-2950 0-'100 ppm 0.4899 ppm zppm voc 2600-3200 0-100 ppm 1.8520 ppm Tota VOC'S I ppmperVOC910-1 150 2550-2950 CH20 2550-2850 0-1OO ppm 0.7878 ppm 1 ppm lnterferlng Compounds * CO is analyzed in a separate analysis region than CO2 and H2O coz 926-1 150 O-1O"/o o"h nla Water Vapor 3200-3401 O-22"/o O.2O"/o nla * VOCs compiled of Acetaldehyde, Ethylene, Hexane, and Propane. T1 FLOW MTR. VENT Figure Annex 1.4.1 Sampling Train The testing instrumentation is housed in an enclosed vehicle which is located approximately 45 feet from the source. A heated sample line (sixty feet in length) is attached to the inlet of analfzer system and the source effluent discharges through the FTIR outlet. l ffi GAS STACK 13 Sampling Point Locations ln lnches 16.7o/o 10. 50o/o 30. 83.3% 49. Inches Upstream: 12 lnches Downstream: 35 TRI.PROBE SAMPLE POINT AS PERCENTAGE OF $IACK D Flgure Annex 1.4.3 Sample Port Locatlon Flgure Annex 1 Sampllng Polnts SAMPLE LOCATION DETERMINEO BY OIST FROM USruRBANCE Taroet Analvte Results (oom) GO o.162r NO o.400t NO2 o.4E9t Ethvlene o3742 Prooane o.rtit51 Hexane o.223i Acetaldehvde o.8l5i Formaldehvde o.7a7t NEA fit rtrls REF TN :rTn s M DCt*t : *'n'#" * crqrLrcr REF r';s Lceu Galibreton Transtbl standald ExDected MeaSured Path Lenqth va!ldated Ethvlena 100 99.32 4.906 Pas{ied Annex Table 1,2.2 lieasurement System Capabilltles GAS Parameter Ges Gonoentratbn Ueasured 70 Dlflerence SDeclllcatlon valldated Spike Direct Propane 251 .000 251.609 O.24o/"+l- 2o/"Pass SI-6 9.t$U 9.726 O.O4"/"+l- 2o/"Pass co 501 .400 492.662 - 14"/o +l- 2o/"Pass NO 252.400 249.Uztj 1.34o/o +l- 20/.Pass Splke Run 1 vla the System Source Output Splke Averaqe Dllr,.rtlon Factor Expected 70 Recoverv Speciflcation Propane 0.000 20.183 20.156 100.140/.7O-13O/" SF6 0.000 0.781 8.030%11O"/o DplKe l{Un Z Vra Ino uyalem source output Spike Averaqe Dllutlon Factor ExDected 70 Recoverv Speciflcatlon Propane o.ooo 19.510 20.632 94.560%7O'13Q"/o SF6 0.000 0.799 8.215o/o <10/" liprrg Hun 5 vra me uyalem Source Output Splke Averaoe Dllutlon Factor Erpected I o/o Recovery speclflcatlon Propane U.UUU 18.991 19.603 96.880%7O-13Oo/o SF6 0.000 0.760 7.8'14/"<10"h Noise Equivalent Absorbance (NEA) RMS High 0.000486 RMS Mid 0.000283 RMS Low 0.000316 Line Position 015 0.10 0.05 ,,:_.:.. ,l-_. 6 66 ;l -:::',.:-_l'.--- -:\ _f \\,/ 0.20 015 0.10 005 000 -0 05 -0.05 2092 2069 2046 2023 19S9 1976 1953 1930 1907 1884 1861 1837 1814 @ o.oo% pass pass GAS The Gasmet GICCOR (Genzel lnterferometer with Cube Corner Retroreflectors) interferometer is specially designed for maximum optical throughput and maximum signal to noise ratio of 7.72 (cm-1) remaining stable with any vibration and temperature changes. The Gasmet DX4000 is a low resolution spectrometer where the aperture is fixe, setting and the detector linearity was tested with an alternate approach. A three point linerarity of thie CTS a gas was performed and validated. Linearity 164 7422 154 7422 t44 t 4tl 134.7422 124 7422 114 7422 104 7422 94 7422 84.7422 74 7422 695 687 679 672 664 656 648 641 633 625 6'18 610 164 7422 154.7422 144^7422 lJ+ /+tz 124 7422 114 7422 104 7422 94 7422 84 7422 74 7422 but 15.4326919 Pass The analytical accuracy of the quantification algorithm is satisfied via the results from Annex 5 per Annex 7.6 POST CTS W3tsm Checr: u ls Eonle uoncentraton:100.oo u I s samote uoncenralron Averaoe:100.69 Difference between measured and expected:0.68% toterance:5.OO% Fun Drta Valldrflon - Automctod vr Manual Rsadlno Yaldatod commentt HUn I HOtnIS 1 & Z On UU/NU/HrOOane All wlthln 2O7o Passed Demonstrates no interterences observed. HUn Z HOtnIS I & Z On UU/NU/HrODane All within 2O7o Passed Demonstrates no lnterterences observed. F{Un 5 rOlnIS r & Z On UU/NU/rrOpane All within 2oolo Passed Demonstrates no interlerences observed. GAS 17 12.0 Signature Page Job/File Name: Crusoe Energy Systems, lnc.; Duchesne Data Center Power Station; ; State Compliance Test II We certify that based on review of test data, knowledge of those individuals directly responsible for conducting this test, we believe the submitted information to be accurate and complete- Company: G.A.S. lnc. Print Name: Lucas Ennis Title: Emissions Specialist Dale:1212112023 Company: G.A.S. lnc. Print Name: Chris Oppel Title: Director of Stack Testing Signature: /,[ C 0?fl"///\ PhoneNumber: 580-225-0403 Dale:1212112023 Company: Print Name: Signature: Title: Phone Number: Date: GAS Appendices GAS Spike (5 Gas) Airgas. an Arr Lqude company AittaSpcddtyGsH Airgs USA LI-C 12722 S. Wstwortb Are. Chiago, IL 60628 Aillu.@m CERIIFICATE OF ANALYSIS Grade of Product: EPA PROTOCOL STANDARI) Part Number Cylinder Number Laboratory: PGVP Number Gas Code: E05Nt94E15AC014 ccl42828 124 - Chicago (SAP) - lL 812022 CO,CO2,NO,NOX,PPN,BALN Referencs Number il4O26O1324-1 Cylinder Volume:. 147.O CF CylinderPressure: 2015PS|G Valve Ouflet: 660 CertificationDate: Dec06,2022 mola/ftolG basb Mbs othwi6. notld. Thr 6ut6 rcletc dly to th. it m3 t-rt.d. Th. Epo.t dr.ll nd bc Eproduc.d o@.pt ih tul wilhdjt EpplMl ol fir l.boEbry. D,o Tdad Data Avallable Upon Requeit PERIANENT NOTES:Mixture contains nominal 1oppm Sulfur Hexaf,uodde as a tracer componenL Aciual tested value included within the original Certifcate of Analysis. oontacl the Airgas laboratory if a reprint is requiI€d NOTES:Mixture contains nominal loppm Sulfur Hexafluoride as a tracer component. Actual testsd value includ€d within the original Certificab of Analysis. Contact the Atgas laboratory if a repdnt is Equired. SF6 Resulb: JMR137-9.73PPMi E E r-t n n Il r nn SldhrluE 6n il. Approved for Releele Plg.1oll Cdt'fietbnp..bm.din.6rdsh6wiih'EPATBe.bilityPrcto@llo.A6sysndCcrtfelidofc.$ffiC5llbr.lirSbdgds(Msy2012) ddmstEPA 600/R-12531, Ging thc asy proc€duEs listcd. AneMlel MGthodology doG not cqJlE @.dd br .Blylical inb.lbEM. Thb crlindd has a totel eaMiEl un6rtahty aa atatad bclo, with a dIHGE Lwl of g5%. ThaB aro no 6igrient impuddcs rfildr .llLsl lhc u$ ol thb elib.etio mlxtrc. All dqMiils aE m a Nd lJ6. Thl.tm i. O7 ANALYIICAL RESIT'LTS Componelrt Requerted Actual Protocol TotalRslatlve Assay Dats3Concentretlon Concentratlon Ueftod Uncort lnty NOX 250.0 PPM 253.0 PPM G1 +/- 1.2% NIST TE@bh 1'lli28l2l22, 1AOG|202. NITRIC OXIDE 250.0 PPM 252.4 PPM Gl +/- 'l .0% NIST TE€abl€ 1112812022, 1A0612022. PROPANE 250.0 PPM 251.0 PPM Gl +/- 0.7% NIST TBeeble 1113il2022 CARBON MONOXIDE 500.0PPM sol.4PPM G1 +/-0.6%NISTTE@ble 11Ds12022 CARBON DIOXIDE 5.000 % 5.025% cl +/- 1.4% NIST Ttuabl€ 1112812022 NITROGEN Bdane CALTBRATIONSTANDARDS TyDo Lot lD Cyllnder No Concontratlolr Uncert lnty ExDlratlon D.to EB0113125 250.3 PPM NtlRtC OXTDE/NTIROGEN D685025 9,9,I PPM NITROGEN DIOXIDSAIR GMIS 401423838104 CC505590 4.373 PPM NTTROGEN DTOX|DE/NTTROGEN NTRM 2fl)60331 PRM 12386 +/- 0.8% +l- 2.0o/" +l- 2.Oo/" +l- O.sP/o +/- 0.6% +/- 0.6% OcrZi,2,.26 Feb20,2O2O Feb 18,2023 Msr 17,2027 Jul 03,2024 May 14,2025 NTRtil 2m602-13 NTRII 13010109 NTRM 13060423 6162697Y 243.3 PPM PROPANE/AIR KALOO3925 49s.4PPMCARBONMONOXIDE/NITROGEN cc4'13685 7.489 % CARBON DTOXTOE/NTTROGEN tlE SRM. NTRM. PRM. d RGM ffid.bow lr dlv lh r.t hnd io fr . GMls ld h h. sv and d En dtu.r ANALYTICALEQUIPMENTlnstrumenutrk.ruodel An.lyflC.l Prlnclds L.3t tultpolnt Callbrruon Nl@bt lS50 AUP2010242 CO.1 SIEMENS ULTMMAT 6E N1J57OO Ni@let iS50 AUP2010242 Nl@let lS50 AUP2010242 Ni@bt iS50 4UP2110277 Nw07,2022 Nw28,2022 ])€c,05,2022 D€c05,2022 Nw07,2O2. FTIR NDIR FTIR FTIR FTIR GAS Airgas. il Ar Uquid€ cmpary 9o/o O2|NO2 Alrgl!spcdrltyctg Airg8 USALrc 525 North Indusuial Iep Rqd T@le,UT84074 Airtu@m CERTIFICAIE OF ANALYSIS Grade of Product: EPA PROTOCOL STA\IDARI) Part Number: Cylindor Numbsr: Laboratory: PGVP Number: Gas Code: E03Nt90E15W0003 cc517745 124 -'roD,eb (SAP) - UT 872023 NO2.02.BALN Refer€nce Number: 153.402786436-1 Cylinder Volume: 145.0 CF Cylinder Pressure: 2015 PSIG Valve Outlel 660 Certification Date: Jul 13,2023 Cdn€ton pdiomld in .@d.n6 with 'EPA TE6.t llty Prc(o@l lbr Asy.nd Ccrdidtd of G.-@ C.lb..iff Stsdrd. (M.y m12I d@'Mt EPA 000/R-12631,uCigth..s.ypl@du6lh.d.An bdelM.,lhodologydGndEqdE@m(doilb..mlyd€lkrbdbEE.Thbcrfindth.!.totcil.lyti4lun6d.hy...t ird bdil rilh . @ffrn6 lrvll of 95%. Th.E .E m.lgnlllent lmpurit . wfihar.lt d th. us dlhb cCb..toi mbdrE. All dqtciona.E on . ildc6rybt tld um Thh b.ld, bG 6p.odE d .rc.pt 0.7 .pplMl of th! leDffiuy. ANALYTICALRESTJLTS Req@.ted Actu.l Protocol Tot l Reldvo Conc.ntr.Uon Conccntnuon U.ffrod Uncert lnty A3s.yD.biCompon€nt NITROGENDIOXIDE 100.0PPM 101.9PPM G1 +^2.0%NISTTEHtI€ o7106,fm23,071132023 OXYGEN 9.000 % 9.037 % Gi +/- 1.0% NlSTTffible O7I06,DO23 NITROGEN Bebne CALIBRATIONSTANDARDS TyDa LotlD CyllndcrNo ConcenElton Uncortrlnty ExDlrrtlon D.!a Nry 09, 2025 F6b23,2023 D*14,2023 GMIS PRM NTRM 1sw202@1 12120 98051010 CC5l7858,IO1.1PPMNITROGENDIOXIDE/NITROGEN D887373 98.9 PPM NITROGEN DIOXIDFJNITROGEN SG9161286BAL 12.05%OXYGEIVNTTROGEN 1.1% 1.0% o.704 ln3trumenut.kdtodcl ANALYTICAL EQT,IIPMENT Anrhrtdl PilnclDl.Lert llultloolni Cellbreilon FTIR 02 PaEmenolb aDXON) Jun 29,2023 Jun29.2023 MKS FT|R NO2 0't8143349 Horlbe MPA-5iO W8O3MM58 02 Tdad Dlt Avllhble Upon Requs3t Approvod for Releare P.g. I ot I GAS Alruas. e AF tiqulo wDdry elrluSpcdrlryOea AtugUUSAIIC unz S.Watwo[ttAc Cbt6ge, IL60618 At!!r.@ OFAIYALYSE PRIMARY STAI{DARI) RefaronceNumbd: 54-4(,?81137'}1Crlndervolur€: 141-OG Cyllnder Prcosum: 2015 PSlc Vahro Outlo* 350 Pror I ol I Crrsbmec Part Nwnb€r: Cyllnder Number Laboratory: Anaurb Dab: Lot Number Grade of GRE{T PLNNS ANALYTIO{I x02Nr99P1sACVH8 ccfi7503 12a - Chioago (SAP) - lL AtS 15,2023 w:t281137&.1 Epln0on Deta:t5,203t Prlmary Sbndad G.6 MbGrcs arctEoeable b f. uteighE and/r N.IS.T, G6 llbltrc rcftrenoe maE lals. RESI,'LIS Componcnt Rcq Gonc Gonccntrdon Analy{cal Unccttalfi16) ETHYLENE 100.0 PPM BaLnc. +l- 1Vt iloil[:GREAT PLAINS A]IALYTICAL. CERf,IFIED BY mR .lr.trmdil. AppotrdiorRobu AI\IAI Ailgas. e Ar Liquid€ Mparry BIP rtufu MtdSouthEliotr AirgsUSALLC 974r E.55th St- North ftbs, Ox74rr7 Airta.@a CERTIFICATE OF BATCH AIYALYSIS Part Number: Cylinder Analyzed: Laboratory: Analysis Date: Grade Nt BtP300 TWo$867349 106 - Tulsa Fast Fill (SAP) - OK F€b 10,2016 of Product: BIP-BUILT IN PT RIFIER Referenca Number: 29.400672389-1 Cylindor Volume: 304.0 CF Cy'inder Pressure: 2O40 PSIG Valve Ou0et 580 Compononl ANALYTICAL RESI.'LTS Requelt d Purlty Certlflod Concentratlon NITROGEN OXYGEN WATER TOTAL HYDROCARBONS CARBON DIOXIDE CARBON MONOXIDE 99.999 % 1 PPM 1 PPM 0.1 PPM 0.5 PPM 0.5 PPM 99.999 % 0.94 PPM 0.058 PPM 0.1 PPM 0.235 PPM 0.235 PPM Pa]meneirt llotaa:This cort lndud€s \€lues from the nfrll' sH€ and is not ropres€ntative of the 'us€' side pudty. Contacrt an Airgas Sales Representative br thls infomatbn. C}lndorr In B.tch: 42861ry, TW04671107, TW0$831574, TW0$865966, TW0$867349, TW0+867538, TW05-867578, Tw0il8r687, TW05-881820, TW0$920689, TW0$920760, TW05848694, TW0586744't, TW05897265, TW05897512, TW05920678, TW05920686, TUm5920695, TW05920781, TW05920874 lmpuritiss v6rifi6d against anaMical stBndards tracoeble to NIST by weight and/or analysis. Approvcd for Rclearo P.g. 'l ot I GAS Airgas. aArLiquir:k cmpsy 21% 02 AiryuSpcsidtycrg AirysUSALrc 525 North Indutrisl fmp Rod T@le, uT84074 Airt8.@m CERTIFICAIE OF AI\IALYSIS Grade of Product: EPA PROTOCOL STANDARD Parl Number Cylinder Number Laboratory: PGVP Number: Gas Code: E02Nr79E15A00B1 cc76460 124 -Tooele (SAP) - UT 872023 02,BALN Refer€nce Number: 1534027 8362'l -'l Cylinder Volume: 146.0 CF Cylinder Pressure: 2015 PSIG Valve Outlet 590 Certification Date: Jul 05,2023 Date:2031 Cqffetbo p{tomrd in .@rd.ne wlth 'EPA TE@eblllty PDio@l br Alsy.nd C..tlletio of G..rs C.lbi.tim Slndrdr (M.y 2012)' d@mdn 6m/R-1 Z53l , Blng thG r$y prEduG. lisi.d. AnaMi€l M.lhodology l@3 not EqulE mrioi ftr .mtyt6l lnbdbE6. Thb crhdd h.s e tot l s.ldal unori.inty.. tt t d b.lo, wlth e ffilldc@ lGwl.of 95%. ThoE.rc no sigrtf€nt impu,id.. rtrkfi eli.oi th. u! ol thh cCb..tbo mlr(irE. Al o6t tioo. .E d s rEb/md6 b.ds unhs o(h.illaa rctad. Tha cult6 Elgte sly b lhc hrm3 taatrd. Th. Epod $.! d b. EFoduc.d cxc.pl h full wlthdrt .ppEEl ot lh. l.hoEbry. Oo Td.d Date Avallable Upon Roquo3l Sldh.hrn ah fl. Approved lor Relea:e Prg. I ot I Component Requolled ConcantEtlon ANALYUCALRESULTS Ac.tual Protocol ConmnlBdon t.lhod Totll Rolatlvo Uncarlrlnty Assay Datsr oxYGEN 21.00% 20.70% NITROGEN Balam G1 +/- 1.4% NIST Tr66aHe O1lOSnO23 CAIIBRAIION STAIYDARDS Typo LotlD Cyllndorilo Concontadon Uncertllnty Explrltlon Dlt NTRM 09061434 C,c282492 22.s3%OXYGENNTIROGEN O.4%M8v 13,2025 lnstrumenutaks/todsl ANNLYTICAL EQT,IIPMENT An.hrdc.l PrlnclDl.La3t ilultlDolnt C.llbnllon Horiba MPA-510 W603MM58 02 02 PaBmaondc (DIXON)Jln?9,2023 GAS @es Great Plains Analytical Services so3 w 3d st Elk City, OK73644 (580) 2 2 5-0403 Fax (580)225 -26L2 CERTIFICATE OF ANALYSIS Grade of Product: CERTIFIED STAI\DARD-PROBE Part Number: 60L Reference P1 Number: Laboratory: GAS INC. Stack Diameter: 60' Analysis Date: 312712023 Target Flow 3Umin Raie: LOT Number: A Number of 3SN: P1A 60L Points: Product performance verified by direct comparison to calibration standards traceable to N.I.S.T. *The probe listed on this form meets the multipoint traverse requirement of EPA Method 7e, section 8.4 as shown in the accompanying data. Method 7e, section 8.4 states that the multipoint traverse requirement can be safisfied by samplingvia"amulti-hole probe designed to sample at the prescribed points with a flow +/- l0 percent of mean flow rate". ANALYTICAL RESULTS Run fr Total Flow Measured Flow Measured Flow Measured Flow Mean Probe (Uml Port A (t/ml Port B (Uml Port C (Um) Port Sampled (Delta qll (Delta q2l (Delta q3l Flow (L/m) Run I 2LPM Run2 4LPM 0.690 0.550 0.580 0.640 (7.814) (1.564) (-e.384) 1.39 t.3l 1.23 1.31(6.ll^) (0.004) (-6.lra) *Calibration conducted in accordance with Emission Measurement Center Guideline Document - EMC GD-031 Notes: 312712023 Approved for Release Date in /..j a"', tNZJ, -\*'4t t ntr'tt " UilITED STATES ENVIRONMENTAL PROTHCTION AGENCY RESEARCH TRIANGLI PAHK. NC T7711 March 15,2021 ' ; ; i i ,i r,;i. ;, ;,1, i' r ;)i ,il,ilJll,ir , ,rral .,!t {r1l Mr. Jordan Williamson CEO GAS Inc. 303 W. 3'a Street Elk City, OK73644 Dear Mr. Williamson: We are writing in response to your leffer received on September 17, 2020,in which you request the approval of alternative testing procedures. The EPA's Office of Air Quality Planning and Standards (OAQPS) is the delegated authority for consideration of major alternatives to test methods and procedures as set forth in 40 CFR parts 60 and 63 under which your request must be addressed. GAS Inc. is requesting a change to one of the test methods, ASTM D6348-03, used for conducting performance tests to determine compliance under 40 CFR part 60, Subpart JJJJ - Standards of Performance for Stationary Spark Ignition Internal Combustion Engines (Subpart JJJJ) and 40 CFR part63, Subpart ZZZZ - National Emissions Standards for Hazardous Air Pollutants for Performance for Stationary Reciprocating Internal Combustion Engines (Subpart ZZZZ). The change being requested will be used to check detector linearity of the Fourier Transform Infrared (FTIR) instrumentation used to conduct this method. Specifically, you are requesting that the procedures of section 8.3.3 of Method 320 (40 CFR part 60, Appendix A), another FTIR-based method allowed under Subparts JJJJ and ZZZZ, be used in lieu of section A6.4.1of ASTM D6348-03 when conducting testing using ASTM D6348-03 under 40 CFR part 60, Subpart JJJJ and 40 CFR part 63, Subpart ZZZZ. In your request, you state that this alternative linearity check procedure will produce consistent results when utilizing either Method 320 or ASTM D6348-03. Additionally, some FTIR instrumentation does not allow for reducing the size of the aperture in the instrument and, thus, it would not be feasible to properly conduct the entirety of the ASTM D6348-03 method in its current form using such an instrument. Based on our understanding of FTIR instrument principles and recognition that the requested alternative determination of detector linearity is both technically sound and contained within Method 320, we are approving the requested change. We believe that this alternative is acceptable for use for use in testing all engines subject to 40 CFR part 60 Subpart JJJJ and 40 CFR part63, Subpart ZZZZ. Also, we will post this letter as ALT-l4l on EPA's website (atwww.epa.gov/emc/broadly-applicable-approved-alternative- testmethods) to announce that our approval of this alternative test method is broadly applicable to engines for the purposes of meeting Subparts JJJJ and ZZZZ. If you should have any questions or require firther information regarding this approval, please contact David Nash ofmy staffat 919-541-9425 or email atnash.dave@epa.gov. STEFFAN Dlgltelfi rlgned by AN JOHHSOf{ 202t.03.15JOHNS cc: t2f$50 -{t4'0s SteffanM. Johnson, Group Leader Measurement Technolory Group Sara Ayers, EPA/OECA/OC/I\dAMPD, (ayres.sara@epa.gov) Melanie King, EPA/OAR/OAQPS/SPPD, fting.melanie@epa.gov) James Leather, EPA Region 6, (leatherjames@epa.gov) David Nash, EPA/OAR/OAQPS/AQAD, (nash.dave@epa.gov) Sincerely, Lucas Ennis GAS 580-225-0403 info@gasinc.us Type of Sources Tested: Stationary Internal Combustion Engines. 4 Stroke Rich Burn Engines. 2 Stroke & 4 Stroke Lean Burn Engines Stationary Natural Gas Fired Generators Stationary Propane Fired Generators Gas Fired Boilers Types ol Analyzers:. Gasmet DX4000 FTIR. Gasmet Portable Sampling Unit with Zirconium Oxide 02 Sensory. Testo 350. Flame lonization Detector Qualifications: Trained, studied, and fully demonstrates compliance for emissions testing via data collection outlined in the following Reference Methods:. EPA Method 1 & 1A - Sampling & Traverse Points. EPA Method 2 &2C - Velocity & Volumetric Flow Rate of a Gas Stream. EPA Method 3A - Oxygen. EPA Method 7E - NOX. EPA Method 10 - Carbon Monoxide. EPA Method 254- Volatile Organic Compounds. ASTM D6348 - Extractive Fourier Transform lnfrared Spectroscopy Conducts emissions testing on a weekly basis including, but not limited to, the following test types: lnitial Compliance, BiennialCompliance, SemiannualCompliance & Quarterly Compliance. Alltest-s performed are in accordance to any and all Federal & State requirements as applicable (i.e. JJJJ,ZZZZ, 106.512, 117, PEA, etc.). Performed testing in Colorado, Utah, Wyoming, North Dakota, Montana, Kansas, New Mexico, Oklahoma, Texas, I ouisiana (land and off-shore), Alkansas, Ohio, Pennsylvania, West Virginia, New York, Kentucky, & Mississippi. . Quarterly Performance Reviews covering ongoing changes with Federal Regulations, State Compliance guidelines, & site-specific safety certifications. GAS oo o :: : @@ @ NN N cc q oo o oo o $t t o( r q ) oo o 00 * @o o ri + a t :6 0 6 .N N N :N O N :n u? e :@ o o :N N N :- o N :N (f J N :N N N '6 t ot oi c) N o oo iF No i o i U)o oo o oo o gq c oo o @{ N oou? \ q 60 6 NN N oo o (o o Fo o , 6r + NF O NO ( l ) na s l oo o r@ O FO N ci c i d Or O F@ O aa ? a ? oo o oo o qq c oo o on@@ @ FO O oi o i ; OO N o qq q .@ o s Fr ) O NO O i+ d oo o oo o oo o ci c i ci NO N FO N au ? c @o o NN N oN o oN @ .o o + ci o i si oo o +t $@t o oo o @@ N *t $aa y o o x () d c i = oL .- N O O oo o lJ d t . b t i d oo o o vo o o NN N II . 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It roa g -gOE Z- d oeo:ze gto: oE g 8ERs -v oEi:gGo oocaoooooEoofL= cotr o(o @rr )@sf (,Y i6 .Y.E= .: . iot,o= oltEz(E 't roo os6Eo,oooocIJ JIoPo c.96U'o]o(LoEooooo(,coocofo troo troa!oo oltE3z=tr= oo o oo o oo o dd c t oN o oo o 9q q oo o oo o : o o o oo o o o o oo o o o o oo o o o o no o o o o ot + r o o o 61 0 O O O dd c i d d d oo o 6 0 0 oo o o o o oo o o o o dc i c i d o d oo @ o o t oo N { o o oo o o o o .o o o : o o o NN N ^ o@ o x x x qe ? e ? t s E E oo o ^ ; ; 66 6 v :o o o : ,@ o o .o o o @ o :O O O : iF O C) oo d c i c r o iO O O I :O O O :o o o : :o o t s rq q q : ': ' : ' : :O O O : 'o O o 'o o o i ,o o o oo o o o o .q q q : q q q oo o : o o o oo o oo o cq e oo o Nr ) O FO Oqq e oo o oo o oo o qq q oo o oo o qc c oo o oo o NO O qq q oo o oo o oo o qq e oo o oo o o* o oo o ci c i d oo o oo o cg q oo o oo N FO O ci c i ci oo o oN 6 NN c, c i ci oo o oo o qc c oo o (r+,Go==oot=Eaw qc q q q q q c oo o o o o o o @o @ o 6 0 @ o oo N 6 0 0 0 @ N( , O O N ( r ) O O ++ + + $ + + + oo o o o o o o ++ { $ + s r + 19 O O O O ( r C ) O o@ o o o @ o 6 NO O O @ @ @ O Os s s v s v s ci c i d o c i c i o d Po - n o o - @ '? o t N @ t N $ PN r i s + + s $ oo o o o o o o QO O O O O O O oo o o o o o o dc i c r c i d c i c i c i C) O @ O N N F O NN F N O c ) O N o@ N @ ( o @ o @ ci d o c i c r o d d ON N O T N N O NN O F qq q q e q c c oo o o o o o o QO O O O O C ) O aa Q o o o o o qc c q q q q c oo o o o o o o aa o o o o o o oo o o o o o o cq q q q q q q oo o o o o o o R8 8 8 8 8 8 8 t^ oo o o o o o o - - z od c i c t d c i c i c r < f . o sa o o o o o o oo o o o o o o qg q q 9 q q 9 oo o o o o o o oo o o o o o o oa o o o o o o cq q 9 q q c 9 oo o o o o o o aa o o o o o o QO O O O O O O oo o o o o o o ci c i d o c i d d d so N $ o t s N o o@ n o @ o s N O$ N F O O O O ^j - - - - - c r c i QO O O O O O O oo o o o o o o cc q q c q q q oo o o o o o o qq q oo o oo o cq e oo o @6 N NN N ce q oo o cq q oo o 6@ @ OF N ol c q oo o qc q oo o @@ @ eq q oo o 60 0 @@ o oo o oo o LO O O o6: b b >c q c u) o o o 9€ E E @o @ O' o o o EH H H dr i = = .N N N _o 6 Er i . o. o \ , FcgG ' >\ xvo E nE ' 3 ii o E^ ' Eo? 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OO O t s - N OO O o N T c9 e q q q o o o : ,t o o : OO O F N N OO O $ F O oo o o i N N i oo o ce c oo o oo o +$ s oo o 66 @ o6 0 qo ? 9 {$ n @@ @ :o o o io o o iO O O . :d ci c, 9P P :o o o :d d o oo o oo o oo o oo o oo @ oo o cc q oo o NO O oN o ni o i - oo o ++ r o6 @ @N O dc i d oo o qq c oo o oo o oo o cq q oo o oo o oo o oo o ci c i ci o$ s qq q oo o oo o oo o qc c oo o oo o oo o oo o ci o o OF O oN o qc q oo o oo o oo o q9 c oo o or ) N @o o q? q o q @o @ NN N @$ o tr ) N @ NN 6 oo o (' \ i $ eq q oo o oo o oo o qq q oo o o{ * o@ o ol R / Al oo o :O O O oo o ON N :c i o ci :N O $ ir ) 0 N :o o o :c i d d i oo { oo @ qc 9 oo o FN O tc ) a ) o@ @ il i N s i oo o NO @ qa u ? oo o oo o eq g oo o @N O rN N aJ q oo o O- o oo o oo o dc i c i oo o oo o qq q oo o NN O , o@ o N+ O NN N oo o oo o oo o qc 9 oo o oo s o@ o 1a ? a oo o o@ t s @N N 9g c oo o ot 6 o@ @ ci c i d oo o oo o oo o oc i d oo o oo o oo o oo c , 98 i l f i Eo o o i='. 8 H 5 I (/ ) - - , j E OO o ! - 6- F fr E E E E E, O ^c L .I - 6 6 d f / , -O O o r t =d c i d d SE E E E EE E E H .9 c j ? 9 E a O( o @ s i ,* ; E ; A SH H E S z ss s a oo o oe 9 9 Eo o o i= lo o o o8 8 8 (r , c, d ci E8. s I 8 (, q c e (l ) o o o tr ' N $ o !o o o :H - o c i c, = ws @ EE E E oo o o Cl r o , o o >e 9 - (f ) I I I U) R R R FR R R oi i i NN N N( ) oo o qq q oo o oo o oo + oo o oo c i oo N oo o ec q oo o oo o oo o oo o dd o oo o oo o qq 9 oo o oo o oo o oo o od o . oo o : oo o : oo o : do d : l OF N : NO O a a? a ? a ? : oo o . 6r O oo t t @@ @ oo o oo o oo o dd o 'o o o io o o 'q q q :o o o :r N N :N N + 'd ci ci 'O N F oo o 'c e q oo o oo o oo o qq q oo o oo o oo o 9e q oo o oo @ FO N oo o ;c i d oo o oo o cc q oo o NN O F@ o oo o ci c i ci @@ O I O N F F @ t 6 O O O N t N o, o o o o $ o o o o c i N NO S F N N N N O O 6 ' ; d N cj d t r O o c j c j aj - d c j c , - - cj EL 88 8 i : 8 3 8 PS S B h R R S oo o - o o o o @ @ ( 9 o m @ @ ci c i o O c i c i c i d - - - ; - - ; o Ng E 58 8 8 S $ E B E B E E S S R 8 3 3 3 tr s r i 3 3 3 3 R @N - O HH k d8 8 8 E8 8 8 B B 8 8 B ct N N _ c q o v o o o o o o o o 6o b l - o o d ( O d d d c j d d o o ss s . = = . ., @ . 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T o. o v Fco^qo o o6 s $ o no q ' : \ q NN O O O oo o o o oo o o o qq q q q oo o o o ON r @ N 6r N { @ qq o ? q q oo o o o @t o N { OO O N N oo o + $ ci d d d d oo o o o o oo o o o o o o o o o o o o eq E + + s $ $ s d d ri d ri r i r i 6 rj d d d ri o rl u : f o o o o o C. ) o (l ) c) (o r) o c) (o o o o o o o o o i t @ o @ @ @ o o o @ o o @ @ @ @ @ @ @ @ @ @ @ i 5 NN o @ @ N sN N @ o N F No N O a N N O o N n a n n n q q a u? q q q q q q q \ \ q q \ qi t o o o o oo o o o o o o o oo o o o o o o o d O@ O { $ N O O N O @ @ O F O N O $ t s @ @ N 9 \ a \ . oq a q q g ' : q o l s l ' : o? q q ' : \ Al q q H *@ @ N O $ 6 6 N n @ 6 6 6 $ + @ @ { + t t d oo o o o o oo o o o o o o o o o o o o o o o oo o o o o oo o o o o o oo o o o o o o o o c e q c c c c 9 q c 9 q c qq q q q q q cq g oo o o o o o o o o o o o o o o o o o o o o o O@ N O O @ @ @ @ $ r @ O O F n r N @ N @ $ O N O (O N O @ @ N 6 O O O O O O r O O O n @ 6 6@ 6 6 6 @ @ n @ N ts @@ N N r @N @ N N @ q ci c i o d d c i d o o ci o ci d d c i d d d d d d d e .E sE ' E. . g E "?OE>o o:. x>OE zd g .e Ig(a 6 . go9 t>IENO (J o *E -t r@:oa co n o N o @ o o o N o o $ N c , n N o o o o @ C7 ) N O 6 O * t t * N O @ N N O N O O O O O F o C q q q C q q q q q q q q q q q q q . . q ' : S oo o o o o oo o o o o o oo o o oo o o o o @o o o o o o o o o o o o o o o o o o o o o o oo o o o o oo o o o o o oo o o o o o o o o qq q q c q 9 q 9 c c e e 9 e q q q q q q q ? oo o o o o oo o o o o o o o o o o o d d d o No o o o o o o o o o o o o o o o o O o O O o oo o o o o o o o o oo o o o o o oo o o o o cq q q q c e q c q e q q q q g g g q q q 0 9 o o o o o o o o o o o o o o d o o o o o d c i o oo o o o o o o o o o o o o o o o o o o o o oo o o o o oo o o o o o o o o o o o o o oo eq q 9 q q q c q q q g q q q g g g q o o o c oo o o o o o o o o o o o o o o o o o o o o o OO O o o O O O O O OO O O O O O O O t O F r o o o o o o o o o o o o o o o o o o o o o o q ) q c q q q q e q q q q q q q q q q g c e q q c o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o Q q e9 c c q qc c c c c c qc q q q o o o o e o o o o o o o o o o o o o o a a a a o o o c i o o o o o o o o o o o o o o o o o o o o o o o e o o o o o o o o o o o o o o o o o o o o o o 9 o o o o o o o o o o o o o o o o o o o o o o a ci o c i o o c i c i c i c , c i c , c i c i d c i d d d d d d d ct O@ F * N @ O @ O N NN O $ O F ON O @ O t ( o ro o O o n N o O o N * 6 N @ - @ o o o ( 9 o o 6 0 00 6 0 @ o6 0 N 6N N N @N N N N9 ci d o d c i d c i d c i c , c i c , d c i c i c , c , c i c i o c i d ci oo N N o o o o o o o o o o o o o o o o o o OO r O O O OO O OO O O O O O O O O O O O O 9e c c 9 c qq q q c c c q cq q q q q q c ? o o o o o o o o o o o o o o o o o o o c i o c r a oiOEo&o3 NEo& ,I -E-o o .i ot r Id a *3 NEoo o -lOE u) 6-o -l -Eza dol NF Z- d g oo o o o oo o o o qq q 9 c oo o o o oo o o o oo o o o oo o o o oc i c i o o oo o o o - - 88 8 8 8 y) oo o o o \ , o oo o o o oo o o o ': q 9 q q oo o o o oo o o o oo o o o eq c e e oo o o o 6N N 6 O NO F { N a? q 9 0 ? \ NN r O { NO @ { @ F6 N N N -c i c i d c , :@ : 'a : .N :t '6 si : :d :i i: i : ]q : :o i :@ a:\oodNaC,aIaoNo\N oo o o o oo o o o qq c c e oo o o o @O N N N (' ) $ ( r ) o o @o o o t ;- - - " - . 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I d J N N N N N N N N N N N N N N N N N N N N N N N N NN N N N N N N N N N N N N N N N N N N N N N N N N N N NN N N N N N N N E N N N N N N N N N N N N & & N N N N N^O: e (J v oEi:o6o cq qq q q oo o o o oo o o o o oo o o o oo o o o o oo o o a a a ci c , d o c i c i o o c i c i c i c t d d c i d 6 0 @ 6 @ o 6 0 0 @ c. 6 6 0 @ @ o o o I B 3 3 3 3 I I 3 I I 8 8 5 3 3 3 3 h B h h ff 6 $ 3 3 3 3 3 3 3 8 h 3 3 3 3 3 3 6 S E f $ + + + + r + + + + + + + $ $ s + + + + * + $ $ + { s < J + J " j = -- : ; qq q q q q oo o o o o oo o o o o o o o o o o oo o o o o P P H H H H H H H H H H H g H H H H H H H H H H H E H H H H H H HE E s E I g $ B R b \ e e E R s B s B B 3I p E E s $ s p B p E& R r, c j d d a i r j o i d c j < $ c j d e j ; C j a i r j c i ai a ; f , j "; " i ; ii . i ; j 3: E E E E E E E E E E E E E E E E E E E E E E E E E E E E E E $E o o o o o o o o o o o o d o o o o d o o o o o o o c i o c i c i d< r c t E I I s s 5 I e 3 ts E p N I il S S E I3 > E s E E U H H E N pF @ o N @N N 66 N N o N r o 6 N N 6 @ N @ N o N r: o o o c i c i d o c i c i c i c i ci d c i d d o c i o d d d d c , o o c i - - J c ; ii ; i Q ! a q, O, F @ F @ O F N N { @ O F O O 6 N () N N O O e ) 6 N @- o q q q € E E q E E E E U U q E E E fi d q 8 S E q S q S PJ E E EE o o o o o o o o o c i c i c i c i o o o o o o d o c i o c i c i d o c i c i d ci d *o o o o o o E E E E 5 E E E E E E E E E E E E E E E E E E E E E E E E E f; E P cj c i cj c j c j c i d c j c t o d c i o c ! c ; - 6 d - - - - - 6 - o c j c ; 3 oc j E E E E E E E E E E E E E E E E E E E E E E E E g E E E E E EE o o o d o c , d c i ci c i c t d o o a o o o o o o d d o c , d d d o d oo E E E E E E E E g E E E E E g E E E E E E E E E E g E E E E gt a, o - - - - - - o o E - 6 6 o o - - E ; 6 ; d o o - - ; ; ; ; E; <o E E E E E E E E E E g E E E E E E E E E E E E E E B H E E E BE o o o c i o c i o o d o c i d c i o a o o o o o c i o o c i c i c , c i c i a a oc , N a a o o o o e ) o o o o o o o o o oo o o o o o o o o o o o c r N R 8 g g E E 8 8 I 8 8 I 8 I 8 8 8 I I I I E B I I I E E E E 8E o o o c i c , d o c i c i d d o c i c , c i c i d o d c i c i c i c , c i d o c i c i d d oo S N - O $ N @ l . - N N @ N 0 N F O N N o ) N N O O 6 O N @ N o F N a q, o o F N $ u) N ts N o N o + o 6 o o 6 t (i (o (i 6 N 6 i (j N 6 + o C i E s n 6 o $ o n o t rO $ o S o ra + o o + < a < - * 6 + < + L a + 6 i t ci c i o c i c i c i d c , ci c i c i c , d o c , c i d o o o d o o c i c i d d ci 6 6 d o @a a a o o o Q o o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o O Oo o 6 6 6 6 6 6 66 6 5 -- - -- 5 t q q q I c c o o o o o o - 6 6 6 6 - - 6 - - 6 - - 6 5 6 6 6 -E o o o c i c , o o c i c i c i d d c i c , c i o c i c i c i c i c , d d c i c i ci c i c i d - <, ci @N o N q o P r E s ol o l s / - ': Rl \ .. - .. ts 6 ;; oN { $ FN N N Rs . - N N g : f - o N o @ N @ v o N '. ' o o o N N N O N N N N ; ci t N oi P; - - - ; - - - ; - - ; - ; - _o6 E , i ' o. o \ , tscgc ' >\ oEn h 5 i i o E^ ' Eol OE>a o:"l OEzd g9@> IEat , 'dgot +> IENd (J o *9 -E@x od : o!OEo& : o3 NEo& : *E rE-o g _e OE IO _o se NEo&*lot r @- d g -? -Fz- d g og NF Z- d gol IEoag *eOF z- d gc o: g ^eEE g N^8sO- i5 (,Etr O F O O O O N O O F O o ) O O O O o N o N - $ o N N N O O N N O (. 0 F @ - rb 6 k r =i D d \ q \ \ oq q q \ q q q q \ \ q q q q q E. ? NF F N F N ro o $ o NO 6 @ o@ @ N 6@ F 6 O @ O o@ o N 6 a? q c ? t q u ? q NFfi ft f t [; H $ $ J H H f; H E H U $ E R R H $ g H 8 ! il H H E$ H ct - - - - - - - - - - - - ; ; - - - - - - ; - ; - - , j , j - - J - oO6N6@ @o oo@t ooq @\ ' T N N N O NO O N @ N N oo @ o o o < o@u? 6N N + no $ o $@ ( o @ -N N a o ) o { @ N o t @ o @ N NN N t ( ' ) 0 O O { O N N O O 6 r@ N N @ O O { N 6 @ N O O @ -; - - - ; - - - i - - - - ; q; N F E E H H S H \ E E F P E F H N H fi g E il H E B 3 H S EB C N ai o i N - - - ; - - nl ^j oi ; oi N oi sj s ; ; - - ai - ; sj - oi ; si N N 'E P o o o o o o o o o o c E H E E E E c E 8 8 8 8 8 E E E E E E E E E E E E E E E E E E Eq lE l R ci o o c j c j d o c i c i o o o c j d d o o d d c j c , d d d d - - o ; oo oE fi H N H H H H fr * H k R H H R H k H ft H H H tr H H H H H H k R* Et ! 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Qq c g q q q q q q q c q q q q q 9 q q q q q q q q q q q ' OO O O O O O O O - O O O O O O O O O O O O O O O o O O O : :@ 6 6 0 0 0 0 @ @ @ o o @ o o @ @ @ @ 6 0 0 0 0 @ @ @ @ @ :: : ,O N O N - $ N N N O $ O + O O N O o N @ N @ @ @ @ O @ O O : :a ? n n u? u ? q q q a u? q u ? q q 1 a q q u ? u ? u ? q u ? a q a u? r i u? : :S * + $ $ $ $ * * * $ $ $ t + t $ $ $ S S * * $ t $ + { + i : r :: ,q c c q I q q q I q q c q q q q q q c I c q q c q c q q q : no o s i $ $ $ $ $ s $ $ $ { t $$ $ $ $ r i { t { { $ s * $ : :O (, (, (r ) c) O c) O O O O O O O O O c) c ) (l ) O O O O O O O O a q) i o@ @ @ @ @ o @ @ @ @ @ 6 6 0 @ o o @ @ @ @ @ @ o @ o o o @O O O @ S F N O O + ( ) O @ N O N O O O $ @ F O o F N O N ,' : ': dl ' : ' : ' : q' : q .' : ' : ' : ' : ' : -' : .: q q C q' : q C' : - q q rO :O.O:@ oo :o ]:o:o:o ::o :N:o + O N O @ F O (D t (, D @ O O N r N O N O N @ O r) $ F O O D \ a s? q a q q o? o ? 01 \ ol o? a ? o i u ? q' : a a q oq o ? oq \ o? ' : q' : OO O O O O O N N O N N O O O O O O N N N N N N N N O N O oo o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o a a a q9 e 9 e c q q q q q q q q q q q q c c c q q q q q q q q oo o o o o o o o o o o o o o o o o o o o o o o o o o o o @r o $ O O 0 * O F N O 6 @ F O @ N @ N o ) @ O @ ( ) O @ N OO N 6 $ @ $ O O N O F O O O O F N @ N O O N T O c 1 O N O N@ @ O 6 N 6 @ N O O O O N N N @ O N @ N N O N N O O N N d d d d c t c i c i c , c , c i d c i o o d o o o o d d c i c , c i c i c i o o d O O O - N O r O O F ) N t O @ N O 6 6 O r + N O F O O 6 F N N- N - N O F O O O C D F O @ F N @ N t s N N @ N N N O N o? a ? a ? a ? a ? c ? o ? o ? a a o? a ol a ol s l a ? o { R l n l q q R I q R l 0 1 r l o l ol oo o o o o o o o o o o o o o o o o o o o o o o o o o o o ooqooo(loNOg?o oc^bg Fc8, a o;i 6E€ (L 9ol OE>o oi ocza o .l Lt r r. / ) ' d q og IENOo. g r€ IE@x (J o- o3OEot o3 NE oo o ,. I ?E o -l (J E !o oSI NEo& .lOFU' A o -l It rza ool NFza ool IEOA o -EOE Z- d o^t ze oi oe o c.c !E N^8e8s IV oEtr oo o o o o o o o o o o o o o o o o o o o o o o o o o o o : oo o o o o o o o o o o o o o o o o o o o o o o o o o o o . :C C C q q I q C q q g q q q q q q C e e C q q C q q q C q , ,o o o o o o o o o o o o o o o o o o o o o o o o o o o o o l: io o o o o o o o o o o o o o o o o o o a a o a a o o o o o : :O o o o o o o o o o o o o o o o o O o o o o O o O o o o o : :o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o d d o o o o o d d c i d d d d c i c i c , c i c i o o ci o o o d d ci : : o o o o o o o o o o o o o o o o o o o o o o o o o o o o e) : : o o o o o o o o o o o o o o o o o o o o o o o o o o o o o u) : q9 e q e e q c e 9 c q q c c e c q q c q q c c q 9 c q q : : OO O O O O O O O O O O O O O O O O o O O O O O o o o o o -o . o o o o o o o o o o o o o o o o o o o o o o o o o o o o o . oo o o o o o o o o o o o o o o o o o o o o o o o o o o o . qq c q c q q q 9 c q c q q q q c c c q c c 9 9 q 9 q q q oo o o o o o o o o o o o o o o o o o o o o o o o o o o o $O N - $ F $ O O F o N @ N F O O O 6 @ N O @ O O @ O @ * N N t @ N O O 0 O O O N O @ O \i N O m C) (l ) F @ N F 6 @ o0 v !+ $ $ $ $ $ $ * $ $ s { t + s $ s t t s $ o o $ (, o ci o o d d d o o d d d c i d c i d c i d c i d d d d d ci c i d d d d oo o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o qq q q q c q q q q 9 q q q c 9 9 c q c q q q q c c c c q oo o o o o o o o o o o o o o o o o o o o o o o o o o o o .O N O O n N r N si \ i O $ N N O O - O { O O C ) { O @ $ r O O - O @ @ @ @ (O O 6 N t N r O( l ) (' ) c) @ O O O { O O O t s @ @ ,a a q c ? 0 2 G l e ? o l c ? 9 c? a a al a o? a ? q q a ? a ? a c" l a c? e ? a a Nl : I -O O @ O O F O @ @ O t O O @ t r N N @ t s @ N @ N O F O O : :r O N O O O $ c1 @ O , N N O \f o) (o ( o O () @ I N N O N r N - N : :' : . n a a a u? a q? o? A a? a ? 1 a? a ': q 1 q ': A 1 r y o! n a a? a i :- oadooocioqo oo o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o d d d d d c t c i c i c i c i o c i d o o d d d c i d @ N O si @ N O N N @ O O O F @ 6 (O O - O n O FO O { O O c ) O N @ N r O 6 t @ O { O * N O \ o) 9' : oq C q o? oq o? q' : \ q q o q q q o? o ) q o) FN T N T N - N N F NO 6 NO O O@ F O oo o o ae o o Nr F N :: i :O : ,@ @ @ O $ @ r O O O t N O * O 6 N O N O N F O F O 6 t :O : l N N o) r) @ O o ) N o (O r @ (O F N { 6 O F @ N O N @ @ C D F @ N :q : t q ': oq I q . a u? u ? o q c ? u ? q q q q q u 2 u ? 9 (| u? a u? a q \ u? q OF N N N N T N i : .- o E o o o o o o o o o o o o o o o o o o o o a o o o o o o o o o -o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o uo o o o o o o o o o o o o o o o o o o o o o o o o o o o o d (O d d d d d d d d c i d d d d c , c i c i c i c i d o d o o o o d c i d d \ . :o O -O N O 0 6 T O O @ O N N N N @ @ N N $ F O @ $ F O O F @ o. = q o q o q q o g a oq o q o q o q q a a q o g e oq q 0 q 0 q 0 q 0 q e oq o q q o q q a O LN N N N N N N N N N N N N N N N N N N N N N N N N N N N N L F L+ @ r O @ N o @ { N @ N @ O O N O O 6 6 F O O N N O O N - AO O 6 O N N n $ S s O O $ N O @ $ O S O n N N O O O S 6 @ c = q u ? q q q u? q q q q u ? q q u ? r | s ? u ? u ? u ? u ? q u ? u ? u ? 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OO O F oo o o oo o @ oo o N qq q c ? oo o o oo o o oo o o oo o o oc i o d oo o o oo o o qq q q oo o o oo o o oo o o oo o o oo o c i oo o o oo o o qg c q oo o o oo o o oo o o qq c q oo o o NO * N oo o o ci c i c i ci !D + $ o o F: : r - - ,\ o o o o \- , oo o o o! ! N ! PS S S S b N N N N :f t N N N g I3 S $ s 8 66 O O O O O sj s j o i s j .\ i oi O FN F O @ @@ N @ l o q u ? u ? u? 33 q oo n 0 6 6 c , ) o E E E B d, 9 I l oo o o r < E o := oo o o ; O o NN N N ' I , l N RR R R lr TR ii i i d) i NN N N N Eail .atLozIct )=o tr5zul Lrl JoT ao aq c oo o oo 6EE E oo o oo o ci a i 6t oo o 66 ! O 6@ < (o r o ( o oo oEE E oo oEE E oo o 6Cl F o FOci c i ct ot l l Nt s N qR ! s l oo oEE E oo oqE E oo o EE E oo o8g E oo oTE E oo oEE g oo oEE E cr d o +( o N mN o oo o d6 \ i ; FN O OE rt r ! t ci c i o EE E oo oTE E cr d c i EE B oo oEE g oo oEE E 9o d NN g ' NN NPP P c) c r o NN N oo o NN NsN s aE .B S l Fhxvo€eE5? 3d o. fEoa A o; EE+E i:EE:el EE :P' BE ^E -EdE rE$i 8EHE TE 2- ^ o. BETE OE , e8; zE ,E8E A HeEs Run NOx ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 33.042 0.04 9.35 0.30 0.00000 0.13291 0.13221 2 32.524 0.05 9.20 0.31 0.00000 0.12012 0.12081 3 29.381 0.05 8.31 0.28 0.00000 0.10313 0.11608 AVG 31.649 0.05 8.95 0.30 0.00000 0.11872 0.12303 Run CO ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 9.144 0.04 2.59 #DIV/0! 0.00000 0.02239 0.02227 2 9.104 0.05 2.58 #DIV/0! 0.00000 0.02047 0.02059 3 8.088 0.05 2.29 #DIV/0! 0.00000 0.01728 0.01945 AVG 8.779 0.05 2.48 #DIV/0! 0.00000 0.0200 0.02077 Run VOC ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 1.81 0.04 0.51 #DIV/0! 0.00000 0.00698 0.00694 2 1.60 0.05 0.45 #DIV/0! 0.00000 0.00565 0.00568 3 1.56 0.05 0.44 #DIV/0! 0.00000 0.00523 0.00589 AVG 1.65 0.05 0.47 #DIV/0! 0.00000 0.0060 0.00617 Run HCOH ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 0.00 #DIV/0! 0.00000 0.0000 0.00000 2 0.00 #DIV/0! 0.00000 0.0000 0.00000 3 0.00 #DIV/0! 0.00000 0.0000 0.00000 AVG #DIV/0! #DIV/0! 0.0000 #DIV/0! 0.00000 0.0000 0.00000 Operating Parameter R1 R2 R3 AVG. Engine Load %86.00 85.00 76.00 82.33 Fuel Feed Rate (SCF/hr):#DIV/0! F-Factor;#DIV/0! Engine HP 456.00 451.00 403.00 436.67 BSFC (BTU/BHP-hr):#DIV/0! Q Stack dscf/hr 33672.72 30915.70 29384.03 31324.15 HHV #DIV/0! Ambient Temperature (F):#DIV/0! Crusoe Energy - Duchesne Data Center; H24 Compressor Engine-1 Stack Test Date 12/20/23, Reviewed by Robert Sirrine on 02/03/24 Test Results NOx Test Parameters Generator #1 Test Results VOC Test Results HCOH Test Results CO Analyte High Recovery +- 10% Gas Value Pre Direct Response % Recovery Pre System Response % Recovery Post System Reponse % Recovery NOx 354.30 0.00 0.00 0.00 NO2 101.9 0.00 0.00 0.00 NO 252.40 247.83 98.19 247.10 97.90 246.65 97.72 CO 501.40 494.78 98.68 492.32 98.19 494.06 98.54 Ethylene (CTS) 100.00 98.56 98.56 97.70 97.70 98.92 98.92 Oxygen 9.04 9.03 99.89 9.02 99.78 9.00 99.56 SF6 9.73 9.64 99.12 9.60 98.71 9.62 98.89 Propane 251.00 250.51 99.81 249.61 99.45 250.29 99.72 Baseline Baseline R1 Baseline R2 Baseline R3 NOx 0.0000 0.0000 0.000 NO2 0.0000 0.0000 0.000 NO 0.0000 0.0000 0.000 CO 0.0000 0.0000 0.000 VOC 0.3500 0.6100 0.610 Oxygen 0.0000 0.0000 0.000 Analyte Cal Gas Value Stack gas measured Stack + Spike measured Spike % Recovery Dilution Factor +=10% Spike Value SF6 run 1 9.73 0.0000 0.78 99.12 0.080 0.78 SF6 run 2 9.73 0.0000 0.79 99.11 0.082 0.79 SF6 run 3 9.73 0.0000 0.80 99.11 0.083 0.80 Propane spike run 1 251.00 0.0000 22.20 110.06 0.080 20.17 Propane spike run 2 251.00 0.0000 22.35 109.11 0.082 20.48 Propane spike run 3 251.00 0.0000 22.49 108.56 0.083 20.72 Analyte CO NO NO2 Form CO2 VOC MDC 0.1627 0.4007 0.4899 0.7878 0.0000 1.8520 Calibration Transfer Standard (CTS) Analyte/Spike %Recovery, Error & Drift System Zero Background Check Pretest Spiked amout should be < 10% of the Certified gas concentration. The DF should be < 0.100 Spiked amout should be +-50% of the Stack analyte gas concentration Sample Spike Recovery (70%-130%) Sample Spike MDC ppmdv Run NOx ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 4.555 0.64 1.33 0.06 0.00000 0.00993 0.01050 2 4.735 0.54 1.37 0.06 0.00000 0.00948 0.00967 3 3.733 0.45 1.08 0.05 0.00000 0.00711 0.00724 AVG 4.341 0.54 1.26 0.06 0.00000 0.00884 0.00914 Run CO ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 21.549 0.64 6.28 #DIV/0! 0.00000 0.02859 0.03023 2 17.065 0.54 4.95 #DIV/0! 0.00000 0.02081 0.02121 3 20.962 0.45 6.05 #DIV/0! 0.00000 0.02430 0.02477 AVG 19.859 0.54 5.76 #DIV/0! 0.00000 0.0246 0.02540 Run VOC ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 2.25 0.64 0.65 #DIV/0! 0.00000 0.00469 0.00496 2 1.96 0.54 0.57 #DIV/0! 0.00000 0.00377 0.00384 3 1.58 0.45 0.46 #DIV/0! 0.00000 0.00288 0.00294 AVG 1.93 0.54 0.56 #DIV/0! 0.00000 0.0038 0.00391 Run HCOH ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 0.00 #DIV/0! 0.00000 0.0000 0.00000 2 0.00 #DIV/0! 0.00000 0.0000 0.00000 3 0.00 #DIV/0! 0.00000 0.0000 0.00000 AVG #DIV/0! #DIV/0! 0.0000 #DIV/0! 0.00000 0.0000 0.00000 Operating Parameter R1 R2 R3 AVG. Engine Load %81.00 84.00 84.00 83.00 Fuel Feed Rate (SCF/hr):#DIV/0! F-Factor;#DIV/0! Engine HP 429.00 445.00 445.00 439.67 BSFC (BTU/BHP-hr):#DIV/0! Q Stack dscf/hr 18245.21 16766.20 15937.50 16982.97 HHV #DIV/0! Ambient Temperature (F):#DIV/0! Crusoe Energy - Duchesne Data Center; H24 Compressor Engine-2 Stack Test Date 12/20/23, Reviewed by Robert Sirrine on 02/05/24 Test Results NOx Test Parameters Generator #1 Test Results VOC Test Results HCOH Test Results CO Analyte High Recovery +- 10% Gas Value Pre Direct Response % Recovery Pre System Response % Recovery Post System Reponse % Recovery NOx 354.30 0.00 0.00 0.00 NO2 101.9 0.00 0.00 0.00 NO 252.40 247.83 98.19 247.10 97.90 246.63 97.71 CO 501.40 494.78 98.68 492.32 98.19 495.03 98.73 Ethylene (CTS) 100.00 98.56 98.56 97.70 97.70 99.01 99.01 Oxygen 9.04 9.03 99.89 9.02 99.78 9.02 99.78 SF6 9.73 9.64 99.12 9.60 98.71 9.61 98.77 Propane 251.00 250.51 99.81 249.61 99.45 249.97 99.59 Baseline Baseline R1 Baseline R2 Baseline R3 NOx 0.0000 0.0000 0.000 NO2 0.0000 0.0000 0.000 NO 0.0000 0.0000 0.000 CO 0.0000 0.0000 0.000 VOC 0.3500 0.5400 0.430 Oxygen 0.0000 0.0000 0.000 Analyte Cal Gas Value Stack gas measured Stack + Spike measured Spike % Recovery Dilution Factor +=10% Spike Value SF6 run 1 9.73 0.0000 0.77 99.12 0.080 0.77 SF6 run 2 9.73 0.0000 0.77 99.11 0.080 0.78 SF6 run 3 9.73 0.0000 0.75 99.12 0.078 0.76 Propane spike run 1 251.00 0.0250 21.78 108.96 0.080 19.96 Propane spike run 2 251.00 0.0000 22.56 112.44 0.080 20.07 Propane spike run 3 251.00 0.0000 21.79 111.20 0.078 19.60 Analyte CO NO NO2 Form CO2 VOC MDC 0.1627 0.4007 0.4899 0.7878 0.0000 1.8520 Calibration Transfer Standard (CTS) Analyte/Spike %Recovery, Error & Drift System Zero Background Check Pretest Spiked amout should be < 10% of the Certified gas concentration. The DF should be < 0.100 Spiked amout should be +-50% of the Stack analyte gas concentration Sample Spike Recovery (70%-130%) Sample Spike MDC ppmdv Run NOx ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 5.149 15.31 5.43 0.01 0.00000 3.10198 0.11907 2 4.264 15.44 4.61 0.01 0.00000 2.52187 0.09680 3 3.337 15.46 3.62 0.01 0.00000 1.71165 0.06570 AVG 4.250 15.40 4.55 0.01 0.00000 2.44516 0.09386 Run CO ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 0.030 15.31 0.03 #DIV/0! 0.00000 0.01100 0.00042 2 0.495 15.44 0.53 #DIV/0! 0.00000 0.17823 0.00684 3 0.000 15.46 0.00 #DIV/0! 0.00000 0.00000 0.00000 AVG 0.175 15.40 0.19 #DIV/0! 0.00000 0.0631 0.00242 Run VOC ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 1.12 15.31 1.18 #DIV/0! 0.00000 0.64615 0.02480 2 1.72 15.44 1.86 #DIV/0! 0.00000 0.97447 0.03741 3 1.11 15.46 1.20 #DIV/0! 0.00000 0.54375 0.02087 AVG 1.31 15.40 1.41 #DIV/0! 0.00000 0.7215 0.02769 Run HCOH ppm %O2 PPM @ 15% O2 PPM @ ISO lb/MMBtu lb/hr g/hp-hr 1 0.00 #DIV/0! 0.00000 0.0000 0.00000 2 0.00 #DIV/0! 0.00000 0.0000 0.00000 3 0.00 #DIV/0! 0.00000 0.0000 0.00000 AVG #DIV/0! #DIV/0! 0.0000 #DIV/0! 0.00000 0.0000 0.00000 Operating Parameter R1 R2 R3 AVG. Engine Load %87.00 87.00 87.00 87.00 Fuel Feed Rate (SCF/hr):#DIV/0! F-Factor;#DIV/0! Engine HP 11816.60 11816.60 11816.60 11816.60 BSFC (BTU/BHP-hr):#DIV/0! Q Stack dscf/hr 5043050.40 4950883.64 4293739.60 4762557.88 HHV #DIV/0! Ambient Temperature (F):#DIV/0! Crusoe Energy - Duchesne Data Center; Titan 130 Turbine Stack Test Date 12/21/23, Reviewed by Robert Sirrine on 02/08/24 Test Results NOx Test Parameters Generator #1 Test Results VOC Test Results HCOH Test Results CO Analyte High Recovery +- 10% Gas Value System Response % Recovery Pre Direct Response % Recovery Post System Reponse % Recovery NOx 354.30 0.00 0.00 0.00 NO2 101.9 0.00 0.00 0.00 NO 252.40 249.03 98.66 246.72 97.75 249.56 98.87 CO 501.40 492.66 98.26 487.31 97.19 491.49 98.02 Ethylene (CTS) 100.00 99.32 99.32 97.40 97.40 100.69 100.69 Oxygen 9.04 9.02 99.78 9.01 99.67 9.00 99.56 SF6 9.73 9.73 99.96 9.62 98.82 9.72 99.89 Propane 251.00 251.61 100.24 248.78 99.12 251.24 100.10 Baseline Baseline R1 Baseline R2 Baseline R3 NOx 0.0200 0.0000 0.000 NO2 0.0200 0.0000 0.000 NO 0.0000 0.0000 0.000 CO 0.0000 0.0000 0.000 VOC 0.2200 1.0800 0.790 Oxygen 0.0000 0.0000 0.000 Analyte Cal Gas Value Stack gas measured Stack + Spike measured Spike % Recovery Dilution Factor +=10% Spike Value SF6 run 1 9.73 0.0000 0.78 99.96 0.080 0.78 SF6 run 2 9.73 0.0000 0.80 99.96 0.082 0.80 SF6 run 3 9.73 0.0000 0.76 99.96 0.078 0.76 Propane spike run 1 251.00 0.0000 20.18 100.14 0.080 20.16 Propane spike run 2 251.00 0.0000 19.51 94.62 0.082 20.62 Propane spike run 3 251.00 0.0000 18.99 96.83 0.078 19.61 Analyte CO NO NO2 Form CO2 VOC MDC 0.1627 0.4007 0.4899 0.7878 0.0000 1.8520 Calibration Transfer Standard (CTS) Analyte/Spike %Recovery, Error & Drift System Zero Background Check Pretest Spiked amout should be < 10% of the Certified gas concentration. The DF should be < 0.100 Spiked amout should be +-50% of the Stack analyte gas concentration Sample Spike Recovery (70%-130%) Sample Spike MDC ppmdv