DAQ-2024-008061

1
DAQC-472-24
Site ID 10238 (B4)

MEMORANDUM

TO: STACK TEST FILE – PACIFICORP ENERGY – Huntington Power Plant

THROUGH: Harold Burge, Major Source Compliance Section Manager

FROM: Paul Morris, Environmental Scientist

DATE: May 16, 2024

SUBJECT: Location: Huntington Power Plant, Huntington, Carbon County, Utah
Contact: Tom Wiscomb – 801-220-2373
Tester: Montrose Air Quality Resources, LLC
Source: Unit #2
FRS ID#: UT0000004901501001
Permit# Title V permit 1501001005 dated January 22, 2020; revised August 26,
2021
Action Code: 3A
Subject: Review of Stack Test Reports Dated May 1, 2024

On May 13, 2024, the Utah Division of Air Quality (DAQ) received a stack test report for the PacifiCorp
Energy Huntington Power Plant located in Castle Dale, Utah. Testing was performed on April 9, 2024, to
determine compliance with Conditions II.B.3.d, II.B.3.f, and 40 CFR 63, Subpart UUUUU for PM
emissions. The DAQ calculated results are:

Source Test Date RM/Pollutant DAQ Result Test Result Limit

Unit #2 4/9/2024 RM 5/202, PM 0.011 lbs/MMBtu 0.011 lbs/MMBtu 0.030 lbs/MMBtu
49.0 lbs/hr 48.3 lbs/hr 70 lbs/hr

DEVIATIONS: This test was originally scheduled to be performed on March 20, 2024, but was
delayed due to elevator issues.

CONCLUSION: The PacifiCorp Energy Huntington Power Plant stack emissions test report for
PM emissions appears to be acceptable.

RECOMMENDATION: Unit #2 should be considered to have been in compliance with the applicable
PM emission limits at the time of testing.

HPV: No.

ATTACHMENTS: PacifiCorp Energy Huntington Plant revised test report received May 13, 2024,
DAQ generated excel spreadsheets

6 , 3
Paclrl@np
Huntlnfion Powor Plant
6 mlbs vtest of Huntlngton, Utah on Hwy. 31
P.O. Box680
Huntington, Utah 8/1528
May 1,N24
Mr. Bryoe Bird, Director
Utah Department of Environmential Quality
Division of Air Qrallty
195 Norh 1950 West
P.O. Box 1ffi20
Salt Lake Clty, UT 841'1ffi2D
Attn: Rob Lebhman
UTAH DEPARTMENT OF
ENVIRONMENTAL OUAIJTY
i'iq'f 1 3 'ii:2.1
DIVISiON OF AIR QUALITY
Subfect Thrce-Ycar Partlculato llatter (PM) Pcrformance Tectlng and the 2024 Annual pM
Toet Report for the Hunilngton plant Unlt 2.
Dear Mr. Bird:
Pacificorp b submitting the reeults of the three-year Merurry and Air Toxics (MATS) Lor Emitting Electrlc
Generating Unit (LEE) PM performanoe testlng and the 2O21 Annual PM Test nepo-rt tor the Hunlington
Pourcr Plant - Unit 2. The tests urcre conduc'ted on Aprll g, n2\ and met the reciulrcmenb of 40 CFR
Part 63_9ubp!rt UUUUU {ongwith the annual testing forfilterable PM as requheb by the Hunflngton
Pourer Plant Tite V Permlt #1501001005.
The Est results indicate the PM emlsslons for Unit 2 are lees than 50 percent of the O.Og0 lb/mmBtu
MATS emisslons limit which demonstatee Ore unit continues to qualfi for PM LEE stiatus. paclflCorp
r€q.uesF the Lltah Department of Erwlronmentral Quality - Diyislon of Air Quality, accept the results oi tnis
test and grant the Huntington Plent's Unlt 2 MATS LEE etatus for the next three years.
As was address€d in a deviation report letter submitted to your orfiice Apr[ 5,2024,the Unit 2 - Three,
Year LEE PM Performan@ Test, as well as the annual Ti0e V PM Test, ulae originally scheduled to beperformed on March 20,2024 but was delayed due to devator operation issues,.
I am authorlzed to make thls submission on behatf of the orutens and openators for the afrected souroe or
affeded unib forwtrlch the submlsslon is made. I certifi uMer penaltyof the lawthat ! have personally
examined, and am familiar with, the etatemenb and lnformaton submitted in thb document and ib
attachments. Baaed on my inquiry of those indlviduals with prlmary resporslbility for obtalnlng the
lnbrmation, I cer@ that the statements and information are to the Ueet of my kn-owledge and believe
true, a@urate, and complete, I am awarethat thelp are signillcant penaltiesfor submitting false
statEments and Information or omitting requlred statements and lnfonnaton, including fre-posslbllity of
fine or imprisonment.
Sttgtrtld you have any questlons regardlng lhis report, please do not hesitate to call Terry Guthrie, Hunter
and Huntington Plant Erwironmental Manager at 435€E7.[334 or Tom Wbcomb at (eOi) ZZO-Z1T1.
Dl€cbr-
Endcurc:'Souu Tost fupdtfurAE4 CorpllumTcthg - Unft2i
cc TomWMrnb-NTO#oGndoBnr€
Scarld Jedcon - NfO w/o qrohqrc
Rreg tttrcon - Hurillngfun frntdcndqrs
Source Test Report for 2O24 Compliance Testing
Unit 2
PacifiCorp
Huntington Power Plant
Huntington, Utah
Prepared For:
PacifiCorp
t4O7 W North Temple, Suite 210
Salt Lake City, Utah 84116
Prepared By:
Montrose Air Quality Services, LLC
990 West 43rd Avenue
Denver, Colorado 80211
For Submission To:
Utah Division of Air Quality
195 North 1950 West
Salt Lake City, UT 84116
Document Number: GPO43AS-O36878-RT- !57 L
Test Date: April 9, 2024
Submittal Date: May 9, 2024
I,TA}I DEPAHruE}TT OF
orunonuatrt ouAunr
iIAY 1 3 2024
DMISION OF AIR OUAUTY
MIfgN,T+g[H ffiAHTE*loltraoudliCllI.lilrr
Signature:
Name:
0 ro
Review and Certification
All work, calculations, and other activities and tasks performed and presented in this
document were carried out by me or under my direction and supervision. I hereby certify
that, to the best of my knowledge, Montrose operated in conformance with the
requirements of the Montrose Quality Management System and ASTM D7O36-O4 during this
test project.
Date:April29,2024
Title: Project Manager
I have reviewed, technically and editorially, details, calculations, results, conclusions, and
other appropriate written materials contained herein. I hereby certify that, to the best of my
knowledge, the presented material is authentic, accurate, and conforms to the requirements
of the Montrose Quality Management System and ASTM D7O36-04.
Signature:
Name:
April29,2024
QA/QC Specialist
!. a
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G P043AS-036878-RT- 1 57 1 Page 2 of 70
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Table of Contents
Section Paqe
1,0 Introduction.. ............ 5
1.1 Summary of Test Program ............ 5
L.2 Key Personnel ........, ........ 6
2.0 Plant and Sampling Location Descriptions...... ........ B
2.L Process Description, Operation, and Control Equipment..... ...........8
2.2 Flue Gas Sampling Location ......... 8
2.3 Operating Conditions and Process Data. ............,. B
3.0 Sampling and Analytical Procedures ...... 9
3.1 Test Methods..... ......... 9
3.1.1 EPA Method 3A..... ,........9
3.1.2 EPA Methods 5 and 2O2........ ........11
3.2 Process Test Methods..... ........72
4,0 Test Discussion and Results....... .................12
4.1 Field Test Deviations and Exceptions.. ............12
4.2 Presentation of Resu1ts............ .............13
5.0 Internal QA/QC Activities .......13
5.1 QA/QC Audits ..............13
5.2 QA/QC Discussion. ............13
5,3 Quality Statement ,...........13
List of Appendices
A Field Data and Calculations..... .....L4
A.1 Sampling Locations.. .....15
A.2 Pafticulate Matter Results and Data Sheets ......t7
A.2.1 Unit 2............. ......,.18
A.3 Example Calculations..,....... ........24
B Facility Process Data. .................28
B,1 Unit 2.. .....29
C Laboratory Analysis Data .. ......44
C,1 Gravimetric Analyses ........45
D Quality Assurance/Quality Control .....,..50
D.1 Units and Abbreviations..... .......51
D.2 Manual Test Method QA/QC Data....... ...........59
D.3 Instrumental Test Method QA/QC Data....... .,.....,...63
D.4 Accreditation Information/Ceftifications ..........67
GP043AS-036878-RT-1571
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List of Tables
Table 1-2 Summary of Average Compllance Results ........6
Table 1-3 Test Perconnel and Obseruers........... ........,....1
Table 2-1 Sampllng Locatlons........... ............ g
List of Figures
Figure 3-1 EPA Method 3 Sampllng Tratn ........ ...............10
Flgure 3-2 EPA Methods 5 and 202 Sampling Train .........12
Pa r. rf rCtrp
2124 Corrplrairce Test R.etart l-lLlntingt.n F.vuer Plant
| ,, i 1
GP043AS-036878-RT- 1 571 Page 4 of 70
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1.O Introduction
1.1 Summary of Test Program
PacifiCorp contracted Montrose Air Quality Services, LLC (Montrose) to perform a
compliance test program at Huntington Power Plant located near Huntington, Utah. The
tests are conducted to determine compliance with the applicable UDEQ permit.
The specific objectives were to:
. Peform annual Particulate Matter (PM) emissions testing on the exhaust
stack of Unit 2
. Perform diagnostic Condensable Particulate Matter (CPM) emissions testing on
the exhaust stack of Unit 2
. Conduct the test program with a focus on safety.
Montrose performed the tests to measure the emission parameters listed in Table 1-1.
Table 1-1
Summary of Test Program
To simplify this repoft, a list of Units and Abbreviations is included in Appendix D.1.
Throughout this report, chemical nomenclature, acronyms, and repofting units are not
defined. Please refer to the list for specific details.
This report presents the test results and supporting data, descriptions of the testing
procedures, descriptions of the facility and sampling locations, and a summary of the quality
assurance procedures used by Montrose. The average emission test results are summarized
and compared to their respective permit limits in Table 1-2, Detailed results for individual
test runs and all supporting data can be found in the appendices,
The testing was conducted by the Montrose personnel listed in Table 1-3. The tests were
conducted according to the test plan (protocol) that was submitted to and approved by
UDEQ.
aaa, . .- ,-aa
GP043AS-035878-RT-157 1 Page 5 of 70
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Table 1-2
Summary of Average Compliance Results
April 9, 2024
Particulate Matter (PM)
40 CFR Part 63, Subpart UUUUU
Operating Permit 1501001004
I.2 Key Personnel
A list of project pafticipants is included below:
Facility Information
Source Location: PacifiCorp
Huntington Plant
Highway 31 West of Huntington
Huntington, Utah 84528
Project Contact: Tom Wiscomb
Role: Sr. Environmental Advisor
Company: PacifiCorp
Telephone: [phone]
Email : [e-mail]
Agency Information
Regulatory Agency: Utah Department of Air Quality
Agency Contact: Rob Leishman
Telephone: [phone]
Email: [e-mail]
Testing Company Information
Testing Firm: Montrose Air Quality Services, LLC
Contact: Craig Kormylo
Title: District Manager
Telephone: [phone]
Email: [e-mail]
City
Russell Willson
Senior Environmental Analyst
PacifiCorp
(43s) 687-433L
Russel [e-mail]
GP043AS-036878-RT-1s71
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Page 6 of 70
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Test personnel and observers are summarized in Table 1-3.
Table 1-3
Test Personnel and Observers
Craig Kormylo
Project Manager
Qualified Individual (QI)
Trailer operator
Sample train operator
Calculations and report preparation
Test Coordinator
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GP043AS-036878-RT-1571
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Page 7 of 70
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2.O PIant and Sampling Location Descriptions
2.1 Process Description, Operation, and Control
Equipment
Huntington Power Plant comprises two pulverized coal-fired boilers.
2.2 Flue Gas Sampling Location
Information regarding the sampling location is presented in Table 2-1.
Table 2-1
Sampling Locations
Sample location(s) were verified in the field to conform to EPA Method 1. See Appendix A.1
for more information.
2.3 Operating Conditions and Process Data
Emission tests were performed while the source/units and air pollution control devices were
operating at the conditions required by the permit. The unit(s) were tested when operating
normally.
Plant personnel were responsible for establishing the test conditions and collecting all
applicable unit-operating data. The process data that was provided is presented in Appendix
B. Data collected includes the following parameters:
. Unit Load (MW)
. Relevant CEMS Parameters
ta
a/ .
GP043AS-036878-RT- 1 57 1
t 't i
Page 8 of 70
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3.O Sampling and Analytical Procedures
3.1 Test Methods
The test methods for this test program have been presented in Table 1-1. Additional
information regarding specific applications or modifications to standard procedures is
presented below.
3.1.1 EPA Method 3A, Determination of Oxygen and Carbon Dioxide
in Emissions from Stationary Sources (Instrumental Analyzer
Procedure)
EPA Method 3A is an instrumental test method used to measure the concentration of Oz and
COz in stack gas. The effluent gas is continuously or intermittently sampled and conveyed to
analyzers that measure the concentrations of Oz and COz. The performance requirements of
the method must be met to validate data.
Pertinent information regarding the performance of the method is presented below:
. Method Options:
o Single-point sampling is performed if Oz and COz meosurements are for
molecular weight calculations only
. Method Exceptions:
o Samples are collected in a Tedlar bag and analyzed on-site.
The typical sampling system is detailed in Figure 3-1.
a'
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GPO43AS-036878-RT- 1 57 1 Page 9 of 70
FIGURE 3-1
US EPA II|ETHOD 3 (TEDLAR BAG) SAI,IPIING TRAIN
SOUEFTE BULB
Facii'iClr-p
,32,4 6s1r-rpiiarrre Test F.eprrt. Huntrngt.rr f .wer f ianl
GP043AS-036878-RT- 1 57 1 Page 10 of 70
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3.L.2 EPA Methods 5 and 2O2
Determination of Particulate Matter from Stationary Sources and Dry
Impinger Method for Determining Condensable Particulate Emissions from
Stationary Sources
EPA Methods 5 and 202 are manual, isokinetic methods used to measure FPM and CPM
emissions. The methods are performed in conjunction with EPA Methods 1 through 4. The
stack gas is sampled through a nozzle, probe, heated filter, unheated CPM filter, condenser,
and impinger train. FPM is collected from the probe and heater filter. CPM is collected from
the unheated CPM filter and the impinger train. The samples are analyzed gravimetrically.
The sum of FPM and CPM represents TPM. The FPM, CPM, and TPM results are reported in
emission concentration and emission rate units.
Pertinent information regarding the performance of the method is presented below:
o Condensed water is measured gravimetrically
o The post-test nitrogen purge is performed by passing nitrogen through the
train under pressure
o To simplify shipping arrangements to remote locations, stainless steel
probe liners and nozzles are used. After each run, the nozzle and probe
liner are brushed and washed a total of six times with reagent-grade
acetone to assure complete recovery of all particulate matter. The brush is
given a final rinse with acetone and the nozzle and probe liner are given a
final rinse with acetone and all rinsate is collected into the appropriate
sample container
The typical sampling system is detailed in Figure 3-2.
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G P043AS-036878-RT- 1 57 1 Page 11 of 70
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Figure 3-2
EPA Methods 5 and 2O2 Sampling Train
3.2 Process Test Methods
The test plan did not require that process samples be collected during this test program;
therefore, no process sample data are presented in this test repoft.
4.O Test Discussion and Results
4,L Field Test Deviations and Exceptions
No field deviations or exceptions from the test plan or test methods were identified by the
Project Manager.
a / - .-aa I rr - .
GP043AS-036878-RT-1s71
IHERMOCOUPLES
FILIER
HOTDEFI THEFIMOCdJPLE
IFILIER HOLDER
THERMOCOUPLE
THERMOCOUPI.f
NOTZLE---+
WPE'S'
PITOT
er'pfy @tcdt d/NtO
100 mr|.l,o
hodn.drnotlp) 20O
tndiltdlrctip)Slllca Gel(ndttd/NtP)*'ti,V."
MANOMETER +
BY-PASS VALVE(rhr.{D{ VACUUM GAJGE
MAI{OMETER +
Page t2 of 70
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4.2 Presentation of Results
The average results are compared to the permit limits in Table 1-2, Emissions are repofted
in units consistent with those in the applicable regulations. Additional information is included
in the appendices as presented in the Table of Contents.
5.0 Internal QA/QC Activities
5.1 QA/QC Audits
The meter box and sampling trains used during sampling performed within the requirements
of their respective methods. All post-test leak checks, minimum metered volumes, minimum
sample durations, and percent isokinetics met the applicable QA/QC criteria, except where
noted in Section 5.2.
EPA Method 5 analytical QA/QC results are included in the laboratory report. The method
QA/QC criteria were met, except if noted in Section 5.2. An EPA Method 5 reagent blank
was analyzed. The maximum allowable amount that can be subtracted is 0.001o/o of the
weight of the acetone used. The blank did not exceed the maximum residue allowed, except
where noted in Section 5.2.
EPA Method 202 analytical QA/QC results are included in the laboratory report. The method
QA/QC criteria were met, except where noted in Section 5.2. An EPA Method 202 Field Train
Recovery Blank (FTRB) was performed for each source category. The maximum allowable
amount that can be subtracted is 0.002 g (2.0 mg).
5.2 QA/QC Discussion
All QA/QC criteria were met during this test program.
5.3 Quality Statement
Montrose is qualified to conduct this test program and has established a quality
management system that led to accreditation with ASTM Standard D7036-04 (Standard
Practice for Competence of Air Emission Testing Bodies). Montrose participates in annual
functional assessments for conformance with D7036-04 which are conducted by the
American Association for Laboratory Accreditation (A2LA). All testing performed by Montrose
is supervised on site by at least one Qualified Individual (QI) as defined in D7036-04
Section 8.3.2. Data quality objectives for estimating measurement uncertainty within the
documented limits in the test methods are met by using approved test protocols for each
project as defined in D7036-04 Sections 7.2.t and 12.10, Additional quality assurance
information is included in the report appendices. The content of this report is modeled after
the EPA Emission Measurement Center Guideline Document (GD-043),
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GP043AS-036878-RT-1571 Page 13 of 70
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Appendix A
Field Data and Calculations
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GP043AS-036878-RT-157 1 Page 14 of 70
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Appendix A.1
Sampling Locations
,
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GP043AS-036878-RT-1571 Page 15 of 70
Pacificorp Huntington Power Plant sampling Locations
Unit
Diameter (D)
t2
323.3" 322,7"
Upstream Dlstance (A) >22O' >220'
Downstream Dlstance (B) >266' >266'
Semplc Polnt Dldanccr ttom Steck Wal!
Traverse Point 1
Traverse Polnt 2
L4.t' L4.L"47.3" 47.3"
Tlaverse Point 3 95.7' 95.5"
Pafticulate Matter Sampling Points
++
Stack Cross Section (A-A)
f a r ii'rCarp
213,1 Crnrpirance fest R.eprrt. llLrrrtinqir:'r Prw.r Planl
G P043A5-036878-RT- 1 57 1 Page 16 of 70
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Appendix A.2
Pafticulate Matter Results and Data Sheets
GP043AS-036878-RT- 1 57 1 Page 17 ofTO
Appendix A.2.1
Unit 2
Pior{35878
P.dfcorp
Huntlnlm Unlt2
al9l20a
o
EPA Mdhod 2 DEb
Run #
SEn Tlm.
Sbp fh.
s.mpleIIh. (61n.)
2
t3:08
15:18
120
2
372.7
23.74
{.3
0.84
0.768
113_9
322.1
23.74
{.3
0.84
o,7429
114.8
s67.970 367.970
-0.r2 432
30.24 30.24
24.79 24.73
23.42 23-42
573.9 574.4
50.9 52.0
56,088.492 56,93d869
7,101,475 1,115,581
I
9:32
L2t27
120
/av\ ry,lUN I H:Us-I
3
15:4O
18:19
120
Dr
P.
q
T,
q
a
SEcl Di.mrter(inches)
Barom€t.ic Presure ("H8)
Stack Static Pressure ("Hro)
Pitd Tube coefiiciert {unitless)
Av8. Velocity Head ofStack Gas V("Hro)
Stack Gas Tempeft ture ('F)
calolado.s
Stack Area (ftr)
Stack Stati. Pressure ('H8)
SEckGai MolecularWeisht, drybasis (lb/lb-mole)
sbclGas Molecularweight, w.t basls (lb/lb-mol.)
Ab3olute stack Pressure ("Hg)
Absolute Stack GasTeoperature {'R )
Shck G& Velnitv (ft/*c)
StackGas DryVolumetric Flow kte (dscf/hrl
stack cas Dryvolumetdc Flow Rate (ds.f/min)
Vk volumeofwaterftndensed (mL)
vh Volume of stack Gas crlled€d ldcfl
Y M€ter Calibration Factor(unitless)
AH Pressure Dlfferentlal Acrossorifice ("Hro)
T. Temperatureatcas Meter('F)
caldlatlona
Pd Absolute Pressure atG.s Meter ("H8)
T. Absolute Temp€rature at Gas Meter('R)
Vq"q volume ofwater Condensed (sc,
Vaor Smple Gas Volumc (d$0
B*, * Obsetred Stack Gas Moisture Content (%/100)
B*., Saturated Moinure Content (%/1m)
Ss Moinurc Content Us.d {961100)
322.7 tXr.l
2?.74 23.7
-4.3 .4.3
0.84 0.84
0.7641 0.n17
114.3 111
567 ,970 ffi.970
-0.32 {.32
30.21 30.23
28.75 B.7s
23.42 21.42
5?4.3 571
50.7 5t2
6s,645,78O 6,224,U7
1,094,095 1103,71'
31
5.7
12.3
215.9
94.597
0.9970
1.5
52.3
23.86
322.3
10.15
75.99
0.118
o.!24
0.118
2
6.5
t2.1
253.4
106.058
0.9970
2.0
54.7
23.89
528.7
11.93
u.27
0.124
o.127
o.124
6.8
12.1
736.2
103.4r2
0.9970
1.9
71.4
23.88
531,8
11.12
81.58
0.120
0.125
0.120
6.7
D.3
23S,2
101.S2
0.9!t70
,-8
68
2t-41
527.6
11,07
80.65
0.ul
0.126
O.DL
D" iloale diameter (")
Cl Mass ofPM colled€d on fiher (m8)
C2 Massof PM collected in rinse (mg)
W. Ma$ofacdon.blank(mg)
EPA Mdhod 201 D.r.
0.240
3.8
18.3
0.4
I
0.2s2
5.2
14.3
0,5
2
0.252
4.7
2X.2
0.4
3
o.2il8
+6
,7,9
0.4
Avcratc
lnpuB
Masa oflnor8ania Condensible PM (mg)
Mass ofoBanic condensible PM (mg)
Total CPM Ma3s (mg)
Mass oftrain bl.nk (mg)
Total cPM M.,s le$ Blank (mg)
Eml$ior C.lcul.fons
F. Fuel F-Factor ($f/mmBtu)
A cross-sedional area ofnozle (ft!)
I lsokinetic variation (%)
m. Tdal Filter.ble PM ma$ le$ blank {mg)
q Fllterable Paniculate concentration (gr&$0
q FilteEblePati.ulateconcentratlon(lb/dJcfl
Eru, FilteEble Padiculate mass emision Ete (lb/hr)
BoilerLoad (MW)
Filterabl€ Paniculate ma$ emision Ete (lb/Mw-hr)
F. Filte6ble Patiaulate mass emisslon rate (lb/mmBtu)
87ilh.sht Filtenble Paniculate mass emiaslon 6te (tons/yeer)
C. CondenslbleParticulateconcentratlon(gr/dscJ)
c, CondensiblePadculateconcentratlon(lb/dsco
Erm. Condensible Padiculate mass emission raE (lb/hr)
F. Condenslble Particulate mass emlssion Ete (lb/mmgtu)
87@h6lr Condensible Padiculate mass emirsion 6te (tons/year)
Total Padlculate concentntion (grldscfl
Total Pafticulate concentration (lb/dsc0
Total Paniculate massemission rate (lb/hr)
Boiler Load (MWl
Total Particulat€ mass emission rate (lb/Mw-hr)
Tot.l Particulate mass emission rate (lb/mmBtu)
Total Padaulate massemisslon 6te (tons/year)
4.2
6.1
2.0
4.1
1840
3.14E-U
104.0
2t.1
0.m
6.30E{7
41.5
473
0.09
0.009
182.2
0.m1
1.19E-07
7.9
0.m2
34.4
0.m5
7.8E47
49.5
473
0.10
0.011
216.7
5.2
2.0
7.2
2.O
5.2
1840
3.45E-04
103.3
19.0
0.003
4.97E47
33.3
475
0.07
0.m7
145.7
0.001
1.35E{7
9,1
0.002
39.9
0.m4
5.33E{7
42.4
475
0.09
0.009
18S.5
4,3 4.6
2.1 2,0
6.4 5.6
2.O 2.O
11 4.5
1840 r&X'
3.46E{4 3.35Es
102.1 103.1
2s.s t2.L
0-m5 0.m4
6.88E{7 6.05C.O7
45.2 10.0
468 472
0.10 0.G
0.010 0.009
197.9 115.3
0.001 0.m1
1.19E{7 1.25E 07
7.4 &3
0.002 0,002
14.1 36.2
0.006 o.ms
8.078{7 1.r0a'0,
53.0 al.3
468 472
0.11 0.10
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G P043AS-036878-RT- 1 57 1 Page 19 of 70
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GP043AS-036878-RT-157 1
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GP043AS-036878-RT- 1 5 71 Page 23 of 70
Appendix A.3
Example Calculations
PROJ-036878Pacincorp /0v r rll t1l\ I KS] ) t
Huntington Unit 2
Run fll Sample Calculations
EPA Method 5: Determination of Particulat€ Matter Emissions (40 CFR Part 60, Appendix A-11
Varlable Value )effnitlon Unlt of Measurement
D.322.7 itack Diameter inches
A s67.97 :ross-Sedional Area of the Stack ft'
o -4.30 itack Static Pressure in. H20
-0.32 ;tack Static Pressure in. Hg
%co1 t2.3 :oncentration of Carbon Dioxide Dry Volume Percent (%vd)
%oz 6.7 :oncentration of Oxy8en Dry Volume Percent (%vd)
Md 30.24 Dry Molecular weight of the stack 6as (defaultl lb/lb-mole
Po",73.14 Barometric Pressure in. Hg
AH 1,60 Pressure Differential across orifi ce in. H20
23.86 qbsolute Pressure at Gas Meter in.Hg
tm 62 Temperature at Gas Meter
T-522 Absolute Temperature at Gas Meter
K1 0.c/706 Conversion Factor ft'/mL
215.9 Volume of Water Condensed e
10.16 y'olume of Water Condensed scf
&7-1.64 onstant 'R/in.Hg
0.9970 uleter Calibration Factor Unitless
94.597 /olume of Stack Gas collected dcf
75.994 ;ample Gas Volume dscf
B*.0.118 itack Gas Moisture Content .A/7O0
28.79 \ctual Molecular Weight of the Stack Gas lb/lb-mole
P 23.42 \bsolute stack Pressure in. Hg
T 113.9 Werage Stack Temperature "F
s74 Verage Absolute Stack Temperature "R
KP 85.49 :onversion Factor (ft/sec) x v(((lb/lb-moleXin.Hs))/(('RXin.H,o)))
c"0.84 ,itot Coefficient Dimensionless
AvgVAp 0.768 \verage Square Root of Velocity Head Readings in. H70
s0.87 werage Stack Gas Velocity ft/sec
T,,a 528 ;tandard Absolute Temperature "R
P*o 29.92 itandard Absolute Pressure in. H8
a 66,088,492 )ry Volumetric Flow Rate Corrected to Standard Conditions dscf/h r
D"o.24 'lozzle Diameter inches
3.14E-04 lross-Sectional Area of the Nozzle ft'
m.25.80 'otal PM and CPM Mass m8
c,7.44E-O7 )articulate Concentration lb/dsct
49.5 ,M Mass Emission Rate pounds per hour
F 1840 rFactor frcm EPA Method 1q scf/mmBtu
Erb/mmBN 0.011 )M Mass Emission Rate pounds per million Btu
276.7 )M Mass Emission Rate tons per year
K5 0.0945 :onstant (in.Hg. min) / ('R.sec)
e 120 iample Time minutes
104.0%sokinetic variation
G P043AS-036878-RT- 1 57 1 Page 25 of 70
PROJ{36!18
PecifiCorp
Huntluton uhlt 2
Run 11$mpL C.ldl.tloils
EPA Mcthod 5: Dlt.mlnsdon of P.dlcul8tc Mrtts Eml$lom (ilo CFR Psn 60, App.ndlx A-t)
A= n(O/24)!
n1322.il241^7
= 567,97 ft^2
Pf PlLe.a
= 4,31t3.6
= {.32tn Ht
M3 = (0,rt4 x %co2) + (0.32 x %or) + 0.28(100-%cor-%or)
= (0.44 x 12.3) + (0.32 x 5.7) + 0.28(100 - L2.l -6.71
= 30.24|bllb-molc
P.= Pu+(AH/13'5)
= 72.74 + (L.6113.61
= 2t.t6 In. HS
T.= 460+t
r 450 + 52.3
= 5:12 R
Vrqo4r K1xV6
= 0.04706 x 215.9
r 10,163cf (Eq.4-1)
V.tatt=&xYxVmxPm
T.
' 17.64x0.997x94.597x23.86
. 75.99 dscl
B*=
(8q.4-31
Vr<.o + Vuu)
10.15
10:16 + 75,99
= o.llt (t /lml {Eq.+4)
M,= Mdx(1-L)+(18.0x B"E)
, (0.rt4 x 12.3) + (0.32 x 6.7) r 0.28(100 - 12.3 _ 6.7) x (1 - 0.118) + (18.0 x 0.1181
= 28.79|bllb-mol.
Pr= Pb + Pt
. 23.74 + (-0.32)
r 23.42 ln. Ht
Ttu)= 45O+Ts
. 460 + 113:9
=574*
(Eq.2-6)
d\fi lf9Nl"\slll
G P043AS-036878-RT- 1 5 7 1 Page 26 of 70
PRoJ-035t78
P.clftcorp
HundnGlon Unlt 2
Run [1 S.mplc Calqll.tbns
EPA Mcthod 5: D.t.rmlnaalon of Por$culat. M.tter Emlsslors ({O crn P.n 60, AppcndkA-l)
G-
v. = (, xc, xAvgrlAp x \ (P, x M,)
. 85.49 x 0.84 x 0.768 x
= 50.9fVscc
q= 3600 x (1-B*)x (V,)x (A) x fr* x PJ
(T4*1 x Pr,.1
= 3500 x (1 - 0.118) x (s0.87) x (s67.97) x (528 x 23.42)
(574x29.92l.
= 56,088,,192 dscf/ht (Eq. 2{)
A = r(D,/24)'l
nls.24/241^2
= 3.14E4tft42
(m&/s) (g/lb) (v.rdr)
= 25.8
(1000) (4s3.s92) (75.994)
= 7.tI8C{7lbldrcf
EnA*= C'xQ
= 7.tl8E-07 x 56088492
. 49,5 lb/hr
(23.42 x 28.79)
(Ec.2-7)
q=
Etvmm=C,xF.x100
(Cor%vd)
7.IBE-O7x1840x1O0
(12.3)
= 0.0t1lb/mmltu
qqr. x (Hrs/yr)
(lbs/ton)
49.47 x8,76a
2000
= 215.7 tons/y.al
l= K5xTa.raxVaarxl(X)
P4a5s1 x V! x An x I x (1-B*)
= O-09rt5 r S74 r 75-994 x 1OO
23.42 x 50.87x 3.1EOt x 120 x (1- 0.118)
= 10t1,0 16
(Eq. s-4
Eq/r.
GP043AS-036878-RT- 1 57 1 Page 27 af 70
t ro
Appendix B
Facility Process Data
ta
-l,.0 t .: . .ra ar .r .
GP043AS-036878-RT- 157 1 Page 28 of 70
o rl
Appendix B.1
Unit 2
tl
a / . .- a .r - .
GP043AS-036878-RT-1571 Page 29 of 70
Source
Paramet€r
(Unit)
UtOgl24 00:32
Average Data - Run 1
Plant: HUNTINGTON PLANT
lnterval: 1 Minute
Type: Block
Report Period: 0410912024 09:32 Through O4lO9l2O24 12:21
Time Online Criteria: 1 minute(s)
108.18
UNIT2
BARPRESS
(NHG)
co2
(PCr)
OPACITY
(PCr)
liIKIEMP
(DEGF)
UNITLOAD
(MW)
23.747 0.8
Uloglz4 09:33 1 1.0
Ungn4 09:34 23.74A 11.1 107.83 171
O4lOSn4 09:35 23.714 107.69
or,lognl 09:36 23.744 11.1 0.6 107 .75 172
04l0glz4 00:37 23.74 107_3s
0r,l0glz4 09:38 23.713 11.2 0.5 106.96 .168
04l0glz4 0€:39 23.742
Ulogtz4 09:40 23.711 '11.2 107.22 .185
or,/0€,l24 G):.tl 23.741 11.2 0.5 107.U
Ul0gl24 09:12 23.74',1 11.2
o!,Dgn4 09:43 23.740 't 1.1 1 10.1 I 486
O4ngnl 09:4.{23.74',1 110.28
04l0gn4 09:45 23.740 't1 _2 I 1 0.26 &7
O4l0gl24 00:46 23.7&'t10.24
Ul09l24 09:47 23.739 11.2 110.?3 469
Ungnl oe:/l8 23.738 11.2 '110.28 47'.|
c4.l0glz4 09:49 23.734 11.2 0.5 1 10.19
o4/ognl 09:50 23.738 11.2 10s.90
0,4l(]€,l24 09:51 11.3 0.5
Ul09l21 09:52 23.739 11.1 82
04,Dgl21 Og:53 11.4
Ul09l24 09:54 11.1 1 1 0.00
Ungn4 09:55
04l0sl24 09:56 11.1 0.5 1 10.50 173
o4ngnl 09:57 110.60
04l0gn4 09:58 110.61
04,l0€,n4 09:59
utogt24
Ul09n4 10:01 23.737
04l0gl24 10:02 23.7U 11.2 107.7A
04,109124 '10:03 11.3 0.5 107.17
Ulogtz4 10:04 23.738 1',t.1 0.5 107.10 478
Oqognl i0:05 23.737 11.4 ,07.19
OqOSnl 10:06 23.7W 11.1 0.5 107.65
0410€,121 10:07 23.735 11.4
UloSl24 10:08 23.735 't1.1 0.5 107.64 478
23.738
E = Exceedance
! = lnvalid
M = Maintenance
Report Generated: 04/ 29 / 24 t4:12
GP043AS-036878-RT- 1 571
C = Calibration
S = Substituted
T = Out Of C.ontrol
11.4 107.57
Page 30 of 70
04t09l24 '10:10
Average Data - Run 1
P|ant: HUNTINGTON PLANT
lnterval: 1 Minute
Type: Block
Report Period: 0410912024 09:32 Through 0410912024 12:21
Time Online Criteria: 1 minute(s)
23.739 11.4 0.5 107.51
o4l09n4 10:11 23.739 0.511 .3 107.31 466
04t09t24 10..12 11 .3 o.5 '1o7.25
04t09t24 10:13 23.739 0.511.3 107.54 465
04t09t24 10:14 11.3 o.5 '107.90
04109n4 10:15 23.739 4720.51 1.3 '109.13
04to9t24 1 1.3 0.5
o4togl24 'lO:17 23.738 0.611.4 110.17
04n9l24 l0:18 23.737 1 1.3 4820.5 1 10.54
o4l09l24 '10:19 23.737 1 1.3 0.5 111.01
o4to9t24 ?3.736 1 1.3 0.5 111.12 479
ut09124 10i21 23.736 11.2 1 1 1.19
04t09t24 1O:22 23.735 4730.511.2 1 1 1.10
04,t09l24 10:23 23.735 0.511.1 111.28
ut09t24 1Oi24 23.7U 1 1.0 0.5 r 1 r.55 467
04l09t24 23.733 1 1.0 111.57
ut09t24 10:26 23.732 11.0 0.5 1 l 1.38 468
utogt24 23.732 't 1.0 111.28
ollost24 1O:28 23.732 1 1.0 4720.5 1 11.15
ut09t24 23.732 11.0 I 1 1.10
o4to9t24 23.731 fi_0 11 't .09
04togl24 4770.510:31 23.732 1'l .0 11'!. 15
Ml09t24 23.731 11.1 111.21
o4t09t24 10:33 23.730 11 .0 4750.6 111.37
o4t09l24 23.729 11 .0 111.43
o4lost24 '10:35 23.729 1'l .0 4720.5 I I 0.83
Mtogl24 23.724 11 .0
04t09t24 10:37 23.729 11 .0 4700.5 t08.64
04t09t24 23.724 11 .0
o4to9t24 10:39 23.728 'I 1.0 4710.5 107.79
o4tost24 23_727 0.6 107.63 470
ul0st24 10:41 23.726 0.511.2 107.70 469
04to9l24 23.725 1'1.2 0.5 't07.67 470
04l09t24 10:43 23.725 0.511.2 't07.66
o4lo9t24 23.725 tl.3 107.55
ut09t24 '10:45 23.724 11.3 0.5 t07.'19 480
utw24 23.723 1'1.4 107.O2 482
04t09t24 10:47 23.723 0.51't.4 t07.03 483
uta9l24 10:48 23.723 11.4 107.12
utogt24 10:49 23.723 1 1.5 0.5 107.27
0/.t09l24 10:50 25.723 0.511.4 109.75 474
Page 31 of 70
F = Untt gfllne
E = Exceedance
I = Invalid
M = Maintenance
Report Generated: 04/29124 74:12
GP043AS-036878-RT- 1 57 1
C = Calibration
S = Substituted
T = Out Of Control
Average Data - Run 1
Plant: HUNTINGTON PLANT
lnterval: 1 Minute
Type: Block
Report Period : 041 09 I 2024 09: 32 Th rou gh O4l O9 I 2024 12:21
Time Online Criteria: 1 minute(s)
04tosl24 23.722 11.4 0.5 110.55 469
04t09t24 10:52 23.721 11.4 0.5 '110.50
o4tost24 23.721 I 1.3 4660.5 110_51
ul09t24 '10:54 23.720 't 1.3 0.5 1 10.56 468
04t09l24 10:55 23.719 t 1.3 0.5 110.40 471
ut0sn4 10:56 23.719 11 .3 0.5 110.26
04togt24 10:57 23.718 11.3 0.5 110.32 477
ut09t24 23.71a 11.3 4780.5 '110.35
ut09t24 10:59 23.718 1',1.4 0.5 1 10.43
04to9t24 1 1:00 23.716 11.4 0.5 '110.47 479
ul09t24 'I 1:01 23.716 '11.4 0.6 110.59 477
o4togt24 11:02 23.716 11.4 110.67 476
o4to9t24 1 l:03 11.4 0.5 1'10.55
ul09t24 11:04 23.715 110.41 476
0/,t09t24 23.714 4750.5
04to9t24 1 l:06 23.715 0.5 110.73
04t09t24 11:08 23.715 11.4 1 '10.91 471
o4t09t24 11 :09 23.715 11.3 0.5 I 1 1.01 469
o4t09t24 1'l:10 23.714 t't .3 0.5 110.93
utogt24 11:11 23.714 11 .3 110.99 467
04109t24 11:12 23.714 11.2 0.5 1't 0.97
o4l09t24 1 1:13 23.714 'l 1.3 109.27 469
ut09t24 25.713 1 1.3 0.5 108.55
o4lo9t24 1 1:15 23.7',t2 1 1.3 0.5 1 08.1 I 473
ut09t24 23.7't3 1 1.3 0.5 'to7.97 473
04t09124 1'l:17 23.712 11.4 0.5 107.U 473
ut09t24 23.714 11.4 0.5 107.62 475
ut09t24 1 1:19 23.713 11.4 0.5 107.64 477
04togt24 11..20 23.713 'I 1.5 0_5 107.57 480
041o9t24 '11:21 23.7'14 'I 1.5
04t09t24 11:22 23.713 1 1.5 o.5 'to7.73 482
04t09t?4 11i23 23.7'14 t1.5 0.5 107.50 481
o4lo9t24 11:24 23.713 t1.5 107_so 478
ut09t24 11:25 23.7',t4 1'1.4 0.5 107.35
04togt24 11:26 23.714 11.4 0.5 '1o7.77
utogt24 11:27 23.715 11.4 0.5
ul09t24 't1..28 23.71s 11.4 468
utogt24 11:29
04l09t24 23.715 1 1.3 110.80 469
uto9t24 11 :31 23.7',t5 1'1.3 0.5 ,111.18 470
F = Untt urflne
E = Exceedance
I = lnvalid
M = Maintenance
Report Generate d: 04/ 29 I 24 74:tZ
G P043AS -036878 -RT- 1 57 1
C = Calibration
S = Substituted
T = Out Of Control
Page 32 of 70
o4t09lit4 11:32
Average Data - Run 1
PIant: HUNTINGTON PLANT
lnterval: 'l Minute
Type: Block
Report Period: Mlogl2024 09:32 Through 0410912024 12:21
Time Online Criteria: 1 minute(s)
1't.3 fi1.350.5
utosru 1 l:33 23.715 11.3 0.5 111.12 472
ut0sn1 1 1:34 23.7't6 '| 1.3 0.5 110.92
utosru 1 1:35 23.718 11.3 0.5 't10.80 175
Mngnl 11:36 2?.715 11.3 0.5 110.8t1 476
04l0E,n1 11:37 23.715 11.3 111.01 177
u/ogn1 11:38 23,715 11.3 0.5 111.13 477
utosnl 'l l:39 23.716 1 I 1.15 475
uDsn4 11:40 23.715 11.3 0.5 11 t.09 174
0/.togl24 11..4'.1 23.715 111.20
utauzl 11:42 23.715 11.3 0.5 11 1.36 472
ut09t21 '11:4:t 23.715 11.3 111.23
o4togt24 l1:44 23.7'.tA 'I 1.3 0.5 1 1 1.13 471
olto9t21 l1:45 23.716 t, _3 I 10.96
04t09t21 11:46 23.718 11 .3 0.5 1 10.15 173
u$gn4 11:47 23.717 11 .3 0.5 109.39
04,l08,t24 11:48 23.717 11.3 1710.5 108.64
0,,tosn.-11:49 23.714 11 .3 0.5 108.36 472
oqosnl I 1:50 23.714 11.3 4710.5 108.30
04,logtit4 l1:51 23.714 11.3 0.5 1@.42 470
utosn4 11:52 23.716 11.3 0.5 108.70 460
04ngn1 1l:53 23.714 '| 1.3 0.5
urcsn4 l1:54 23.719 4710.5I 1.3 108.65
uMnl '| l:55 fi.3 0.5
wpsn4 11:56 23.718 0.5I 1.3 107.98 4n
0/,tof)n1 '11:57 23.717 11.3
0/,t0{,,n4 1 1:58 23.717 0.511.4 't07.69 480
o4,tost24.l1:59 23.717 11.1 0.5
0,,t0p,t24 12:00 23.718 9.2 I 4810.5 107.78
ut09l24 12:O1 23.718 7.9 I 479
o4tosl2l 12:02 23.719 11.3 I 4770.5 1fi.11
od,togl24 12:03 23.718 111.41 474
utogt24 12:U 23.718 11.2 I 4710.5 111.33
0/,lo9l24 12:05 t l t.38
0d,,t0€,t24 12:06 23.718 0.511.2 111.50 467
uDgn4 12:O7 23.714 't1.2 0.5 1'.t1.57
utost24 12:08 23.717 0.511.2 1'11.55 468
04,1osn4.11.2 0.5 t'i t -64 468
0/,,t0f)t24 12i10 23.717 0.511.2 111.71 /169
uMnl 12:11 23.718 11.2 4720.5 111.8
utost24 12112 23.718 0.511.2 111.11 178
Page 33 of 70
F = UNIE (,IIIINE
E = Exceedance
I = lnvalid
M = Maintenance
Report Generate d: O4l 29 | 24 L4:L2
GP043AS-036878- RT- 1 5 7 1
G = Calibration
S = Substituted
T = Out Of Control
Ul0gl24 '12:13 23.718
Average Data - Run 1
P|ant: HUNTINGTON PLANT
lnterval: 1 Minute
Type: Block
Report Period : Ul 09 I 2024 09: 32 Th rou gh 041 09 12024 12:21
Time Online Criteria: 1 minute(s)
1 1.3 0.5 111.04
04,l0glz4 12:14 1 1.3 '11't.o2
Ulogl24 12:15 23.717 11.4 1 10.94
O4l09n4 1?i16 11.4 l l 1.00
O4l09lZ4 12i17 23.718 11.4
O4l0gl24 12:18 11.4 110.O8
uto9l24 12:19 23.718 11.1 0.5 109.23 473
oqogn4 12..20 1 1.3 109.16
O4logl24 12i21 11.3
A\rerage
Minimum
Maximum
Summation
lncluded Data
9^i6ta
Total number of
nal. P^i6tq
23.725
23.712
23.747
4,O33.278
1 1.3
1 1.0
11.5
1,848.8
0.5
0.5
0.6
86.1
C = Calibration
S = Substituted
T = Out Of Control
109.55
106.96
111.71
18,623.42
473
463
47
80,442
't70
170
,l64
170
170
170
170
170
170
170
F = Unit Offline
E = Exceedance
I = lnvalid
M = Maintenance
Report Generated: 04/29/24 74:L2
GP043AS-036878-RT- 1 571 Page 34 of 70
Average Data - Run 2
P|ant: HUNTINGTON PLANT
lnterval: 1 Minute
Type: Block
Report Period: 041091202413:08 Through 0410912024 15:18
Time Online Criteria: 1 minute(s)
Source
Parameter
(Unit)
o4,l0gl24 13:08 23.709
UNIT2
t'AKI'KE55
(lNHG)
ugz
(PCr)
UI'AUI I Y
(PCr)
STKTEMP
(DEGF)
UNITLOAT)
(tlvv)
't1 111.88
O4,,togllll 13:09 23.710 0.511.2 't12.21 408
O4lW24 13:10 23.710 0.511.2 112.22
04..109124 13:11 23.7'.tO 0.511.2 112.O9 473
04,l0€,n4 13:12 23.711 11.2 112.'19
04t08,124 13:13 23.710 11.3 0.5 112.35 la1
04l0{,n1 13:14 23.708 11.3 0.5 112.43 442
Urcgn4 13:15 23.704 I 1.3 0.5 112.76 42
04,Ngl24 13:16 23.70e 11.3 0.5 112.U
04l0glz4 13i17 23.7@ 1 1.3 '112.U 479
oI,l0€,121 '13:18 23.709 1 1.3 0.5 113.O2 474
04l0€,n4 13:19 23.7@ I 1.3 113.20 172
Uloglz4 13:20 23.7@ 11.3 4700.5 113.37
04to9l21 13:.21 11.2 l'13./+5 469
04109124 13:22 23.709 0.5't1.2 113.42 .168
utosDl 13..23 23_704 11.2 t'13.55
O4l09l?4 13:24 23.707 11.2 0.5 't 13_73
04l@,n4 13:25 23_708 1'1.2 4720.5 1 13.48
Ulognl 13:20 23.708 11.2 115.24
UlOSn4 13:27 23.7@ 11.2 0.5 I 13.34 476
Ulognl 13:28 23.704 11.2 1 13.3/t
0d,l0gn4 13:29 23.707 11.3 0.5 t 1 3.06 479
o1,l0,,n1 13:30 23.704 't't.3 113.26 477
04,l0gl24 13:31 23.708 1 1.3 0.5 '113.25 175
04l0p,121 13:32 23.707 113.O7
Ul0gl24 13:33 23.707 '11.2 0.5 113.32 471
O4ls,,121 l3:3/t 23.707 11.2 113.70 470
04t@,121 13:35 23.708 0.511.1 1't 3.57 472
Ungnl 13:38 23.707 '1 t.l '| 13.30
04,l08,n4 13:37 23.708 0.511.1 1'12.68 478
o/,nglz4 13:38 23.707 11.0 't 11.36
04ls)121 i3:39 23.708 0.511.1 1 10.55 481
O4,l0gl24 13:40 23.7M 0.511.1 109.98 $1
UlW24 13:41 23.707 11.2 0.5 109.74 479
0/,tost24 13..12 23.707 11-2 0.5 109.52
Ulogl24 13:rl'!}23.707 11.3 0.5 109..t5 475
04l0gl24 13:11
utoetz4 F J'if' r ctfrti,,.*!1o1 0.511.3 1@.81 473
Page 35 of 70
E = Exceedance
| = lnvalid
M = Maintenance
Report Generated:. 04129 124 t4ttl
GP043AS-035878-RT- 1 571
C = Calibration
S = Substituted
T = Out Of Control
o4to9t24 13:46 23.708
Average Data - Run 2
Plant: HUNTINGTON PLANT
lnterval: 1 Minute
Type: Block
Report Period: 041091202413:08 Through 0410912024 15:18
Time Online Criteria: 1 minute(s)
11.2 0.5 109.63
04t09t24 '|.3:47 23.707 11.2 0.5 471
04t09t24 13:48 23.707 'l 1.3 0.5 108.88 470
o4to9l24 '13:49 23.706 11.3 470
04togt24 13:50 'l 1.3 0.5 108.73
04togl24 13:51 23.706 11.4
11.1
108.85
109.1 104t09t2423.705
04t09124 13:53 23.704 11.4
Mt09l24 1 23.705
0/.t09t24 13:55 23.705
ut09t24 1 3:56 111.62
04t09t24 13:57 23.703 1 1.3 0.5 't 1 't _83
04l09t24 '13:58 23.703 1 1.3 0.5 't12.14 483
04t0st24 l3:59 23.703 11 .3
utosl24 14:00 23.703 11.3 0.4 112.03
ut09t24 23.703 11.3 112.10 477
04l09t24 14:02 23.703 't 1.3 473
468
0.4 112.48
04l09n4 23.702 t'1.3
utost24 14i04 23.701 1 t.3 0.4 112.32 466
o4to9t24 23.7W 11 .3 o.4 112.36
04t09t24 '14:06 23.700 1 1.3
04tost24 14:07 23.699 1 1.3 0.5 11?.O7
04t09n4 14:08 11.3 0.5 .l
1 1.69 476
o4to9t24 14:09 23.699 0.5 109.36
utogl24 14:1O 11.4 0_5 4U
04t09t24 't4..11 23.700 't 1.5 0.5 108.85 483
04t09t24 14:12 23.69S 't 1.5 108.73 481
utost24 14:13 23.699 11 .5 0.5
04t09t24 14:14 23.699 11.5 109.12 473
0/,t09t24 14:15 23.698 11.4 0.5 109.24 469
ut09t24 14:16 23.698
04l09t?4 14117 1'1.4 0.5 468
o4to9t24 23.697 11.4 0.5 108.80
04109t24 14'.15 23.697 11.4 0.5 473
474-utogt24 14:20 11.4
04l09t24 14:21 23.698 11.4 0.5 108.32 475
o4to9t24 23.699 l't.4 0.5 108.5'l 475
o4lo9t24 '14:23 23.700 1't.4 0.5 108.47 474
utogl24 'l.4:24 23.70o 11.4
11.4
110.60 474
Page 36 of 70
04t09t24 14'.25 23.70',1 11.4 0.5
o4t09t24 '14:26 23.700
F = Untt urltne
E = Exceedance
I = lnvalid
M = Maintenance
Report Generate d: 04 / 29 / 24 7a:73
GP043AS-036878-RT-157 1
C = Calibration
S = Substituted
T = Out Of Control
04togl24 14:27 23.700
Average Data - Run 2
Plant: HUNTINGTON PIANT
lnterval: 1 Minute
Type: Block
Report Period: 041091202413:08 Through 0410912024 15:18
Time Online Criteria: 1 minute(s)
1'1.4 0.5 111.22 475
oq09n4 fi'.24 23.701 4760.511.4 't11.20
04t09t24 14'.29 23.701 1't.4 4780_5 111.20
04t09t24 14:30 23.701 0.511.4 111.U 479
04109t24 14:31 23.701 0.5't1.4 1',11.37
Mto9t21 23_703 11.5 111.47 480
o4t09t24 14:33 23.702 11 .5 0.5 't 1 't.60
04t09t24 23.701 1'1.4 111.77 477
04t09t24 14:35 23.701 0.511.4 1 11.90
ut09t24 23.70.2 11.4 1 1 1.80 475
04t09t24 0.511.4l4:37 23.702 111.47
04.t09t24 23.703 11_1 't12.14 473
o4t09t24 14:39 23.70'.1 0.511.4 112.22
ut09t24 14:40 23.701 11 .3 1't2.10 472
o4l09t24 14'.41 23.700 0.5t1.3 1 11.53 472
04t09n4 14'.42 23.701 1't.3
04t09t24 14:43 23.701 0.5t 1.3 '109.45 474
o4109124 14:44 23.701 11.4 474
04t09l24 14:45 23.701 11.4 4750.5 109.06
utogl24 14:46 23.700 11.4 0.5 108.74
o4to9t24 14:47 23.700 0.511.4 108.75
04t09t24 14:48 23.699 11 .5 0.5 108.79 479
04to9l24 't4'.49 23.7@ 0.511 .5 108.54
04lo9t24 0.511 .5 '108.44 479
0/,t09124 l4:51 23.701 0.41 1.5
04lo9t24 'l 1.5 108.45 476
o4109t24 14:53 23.700 0.511.5 475
o4tost24 23.701 4720.51',t.4 108.52
o4t09124 0.511.414:55 23.701 104.72
o4lost24 '14:56 23.702 0.4l't.4 10s.24 470
ut09l24 14'.57 23.701 o.411.4 110.47
o4t09n4 23.700 11.4 4720.5 't11.27
04t09t24 14:59 23.701 0.511.4 111.27
04l09n4 23.700 0.511.4 111.24 479
04l09t24 15:01 23.701 0.411.4 111.29
04t09t24 23.70'l 11.4 111.42 480
ut09t24 15:03 23.700 4780.411.4 't't1.49
04to9t24 23.700 11.4 11 1.3'l 476
o4to9t24 15:05 23.701 0.5't1.4 11 1.31
o4to9l24 23.7N 11.4 1't 1.53
o4to9t24 15:07 23.700 0.511.4 I 1 1.64 471
Page 37 of 70
F = Unit offlane
E = Exceedance
I = lnvalid
M = Maintenance
Report Generated: O4l 29 /2a M:73
GP043AS-036878-RT- 1 57 1
C = Galibration
S = Substituted
T = Out Of Contro!
O4t09l?4 15:08 23.699
Average Data - Run 2
P|ant: HUNTINGTON PLANT
lnterval: 1 Minute
Type: Block
Report Period : 041 09 I 2024 1 3: 08 Th rou gh Ml 09 12024 1 5: 1 8
Time Online Criteria: 1 minute(s)
1 1.3 0.5
Ul09l24 15:09 23.699 1 t.3 0.5 11 1.63 473
04l0gl24 '15:10 23.699 't1.3 0.5 11 1.68 175
Uloglz4 t5:11 23.698 11.4 0.5 111.83 479
Ul09l24 15:12 23.699 1'1.4 0.5
0{,l09n4 15:13 23.7OO 11.4 0.5 11 1.59 481
Ulogl24 15:14 23.7@ '11.4 111.73 480
UlO9l24 15:15 23.699 11.4 1 10.93
O4l09n4 15:16 23.701 11.1 110.00 473
Ul09n4 15i17 23.701 109.30
04109124 15:18 23.702
Avorage 23.703
Minimum 23.697
Maximum 23.711
Summation 3,105.100
lncluded Data 131
P^inte
Total numberof 131
nete l,^i^1.
F = Unit Offline
E = Exceedance
I = lnvalid
M = Maintenance
Report Generated: 04/ 29 / 24 L4:73
GP043AS-036878-RT- 1571
63.8 14,il4.49
11 .3
1 1.0
11.5
1,485.0
'l 11.03
108.32
113.73
475
466
4U
62,218
0.5
0.4
0.5
13',1
131
13'l
131
131
131
131
131
C = Calibration
S = Substituted
T = Out Of Control
Page 38 of 70
Average Data - Run 3
Plant: HUNTINGTON PI-ANT
lnterval: 1 Minute
Type: Block
Report Period: O4lOgl2O24 1 5:40 Through 0410912024 18:19
Time Online Criteria: 1 minute(s)
Sorrce
Parameder
(Unit)
An@,24 15:.10 23.696 11.4 0.5 1 1'l .81
UNIT2
BARPRESS
ONHG)
co2
(PCT)
OPAC]TY
(PCT)
STKTEMP
(DEGF)
uNll L9AU
(lufw)
04l0gl24 15:41 111.98 473
0d,l0€,121 15:42 23.698 11.3 0.5 112.15 471
0/,ngl24 15:43 23.6S9 112.10 470
UlW24 15:44 23.698 11.3 0.5 112.14 170
G{,l09l24 15:t+5 23.698 '1 1.3 112.17 473
04,109124 15:/+6 23.698 '| 1.3 0.5 112.07 475
04l0gn4 15:17 23.698 t1.3 111.97 474
0(,l0q,n4 15:48 23.698 0.5r 1.3 1 11 .84 480
U$gnl 15:49 23.699 1',t.4 0.5 11',t.57
O1l0gl21 15:50 23.699 11.4 4790.5 't 10.53
o4,D9n1 15:51 23.698 11.4 0.5 109.58
O1l0gl21 15:52 '11.1 0.5 109.43 472
0410E,124 15:53 23.696 11.1 0.5 109.38
O1l0gl21 15:54 11.4 0.5 109.40 /169
UlNl21 15:55 23.696 4710.511.4 109.54
O4l0gl24 15:56 11.4 109.42 173
UlOSl24 15:57 23.695 11.4 0.5
UlOSnl 15:58 11.4 109.16 480
UlOSn4 15:59 23.694 11.4 0.5 't 09.14
o4,l0,,,n1 16:00 23.094 9.4 I 0.5 108.97 4A1
0{,nU24 16:01 23.696 8.0 I o.5
o4,l0gn4 16:02 23.695 '11.5 I 0.5 108.88 476
O{,l0gl24 l8:o3 'to9.t8
0/.,10€,124 10:01 23.693 11.3 I 0.5 110.31 469
OltOSl2l 16:05 111.63 447
0d.,l09/21 16:06 23.694 0.511.3 1'.tz.27 .+66
0/,l0gl24 16:07 0.5t1.3 fi2.14
Ul09l24 16:08 23.693 0.511.2 112.37 470
04l0gl24 16:00 23.693 112.080.511.3
Ut09l24 16:10 23.694 0.511.3 111.86 480
O/..l0glill 16:11 23.693 0.511.4 't 1't _93
Ul09l24 1A:12 23.694 0.411.4 112.t5 484
04.,10€,124 16:13 23.695 0.511.4 112.06 142
0r,t0€,124 16:14 23.497 4790.511.5 112.03
Mlognl 16:15 23.097 0.51',1.1 112.13 475
UlW21 16:16 23.897 11.4 112.9
04,lOSn4 16:17 23.691E=llril ftf,tlira 0.511.1 112.*468
Page 39 of 70
E = Exceedance
I = lnvalid
M = Maintenance
Report Generated: 041 29 / 24 L4:L3
GP043AS-036878-RT- 1 57 1
C = Calibration
S = Substituted
T = Out Of Contrcl
ut09l24 l6:18
Average Data - Run 3
Plant: HUNTINGTON PLANT
lnterval: 1 Minute
Type: Block
Report Peri od : O4l 09 I 2024 1 5: 40 Th rou gh 04 I 09 I 2024 1 8: 1 I
Time Online Criteria: 1 minute(s)
'11.3 0.5 112.67 468
o4t09t24 16:19 112.47
o4to9t24 16:21 11.3 0.5
04t09t24 16:22 0.5I 1.3 '110.49 452
04l09t24 16:23 23.696 't 1.3 0.5 109.69 441
04t09t24 16i24 11.4 0.5 109.46 477
ut09t24 16:25 23.697 11.4 0.5 109.14
04togt24 '16:26 23.698 11.4 109.19 471
04t09t24 16:27 23.699 't1.4 0.5 109.26 469
o4t09n4 16:28 23.700 11.4 r09.33 468
ut09l24 16:29 23.700 1'l.3 0.5 109.26 470
o4to9t24 16:30 23.700 '11.3 0.5 108.96 172
04109t24 16:31 11.4 0.5 108.81 473
04tost24 16:32 23.70',1 11.1 0.5 108.66
04to9t24 16:33 23.702 11.4
04t09l24 16:34 23.702
04to9t24 16:36
ul09t24 16:38 23.703 1'1.4 0.4 'l'l't.00 471
ut09t24 23.704 11.4 't 1 1.69
04t09t24 16:40 23.704 1 1.3 0.4 11 1.81 470
04109t24 16:41 23.705 1 1.3 0.4 111.75 470
ul09l24 16:42 23.705 11.3 0.4 111.67 472
o4to9l24 23.705 11.3 0.4
04t09t24 16:44 23.706 1 1.3 0.4 111.52 473
0/,t09t24 2?.706 1 1.3 111.32 474
04109t24 16:46 23.707 11.3 0.5 1 1 1_O9 475
o4to9t24 23.707 0.4 111.15 476
ut09l24 '16:48 23.707 11.4
ut09t24 23.708 't1.4 0.4
04t09t24 '16:50 23.708 1 1.5 't11.25 4U
o4lo9t24 23.708 1 1.5 111.24
o4t09124 16i52 23.710 11 .5 0.5 111.27 479
04t09t24 23.710 11.4 111.47 476
04.t09t24 16:54 23.709 't1.4 0.5 1't't.79 474
o4to9t24 23.7'10 11.4 't 11.96 473
ut09t24 t6:56 23.710 11.3 0.4 't11.94 474
o4to9t24 23.7'tO 11.3 0.5 111.75
04.t09t24 16:58 23.709 0.5 1 11.69 47611.3
Page 40 of 70
F = Untt grltne
E = Exceedance
! = lnvalid
M = Maintenance
Report Generate& 04/29/2a U:73
GP043AS-036878-RT- 1 57 1
C = Galibration
S = Substituted
T = Out Of Control
o4t09l24 l6:59 23.710
Average Data - Run 3
Plant: HUNTINGTON PLANT
lnterval: 1 Minute
Type: Block
Report Period: 0410912024 15:40 Through 0410912024 18:19
Time Online Criteria: 1 minute(s)
1 1.3 0.5 1 I 1.89
o/,togt24 23.710 1 1.3 1 1 1.96 474
ul09t24 l7:01 23.709 1 't.3 0.4 1 I 1.95
04t09l24 23.709 11.3 1 l 1.83 474
04.t09t24 l7:03 23.709 0.411.3 11 1.81
04t09t24 17:04 23.709 11 .3 11.42 473
ut09t24 '17:05 23.709 0.5t'l .3 111.94 472
04to9t24 17:06 23.705 r1.3 0.4 1',t2.O5
04t09124 17:O7 23.7'.1O 11.3 o.4 I 10.18 473
04t09t24 1 7:08 23.709 1 1.3
ut09l24 17:09 23.708 0.51 1.3 109.23 474
ut09t24 17:10 23.707 11.3 108.99
utogt24 17:11 23.707 0.41 1.3 108.73
04tost24 11.4 108.40 475
04t09124 17:13 23.704 0.411.4 108.50
o4t09t24 l't.4 108.7r 480
utosl24 17:15 23.706 0.411.5 't08.48 481
04t09t24 11.5 108.10 480
ul09t24 17 i17 23.706 0.4'l 1.5 107.98 478
04to9t24 17:18 1 1.5 108.05 475
0/,l09t24 17i19 23.705 0.4'l 1.5 108.32 472
0/.togt24 11.4 108.60 472
Mtogt24 17:21 23.705 o.41',t.4
Ml09t24 471109.8111.3
04t09124 17:23 23.7U 0.411 .3 110.77
04t09t24 1'1.3 1 11 "05 469
04t09n4 17:25 23.7U 0.511.3 I 10.95
Mlogt24 23.702 4810.511.4 '110.87
ut09t24 17i27 23.702 0.511.4 1 10_66
o4to9t24 23.703 0.51 1.5 '1 t0.54 488
un9l24 17:29 23.705 0.51 1.5 'l l0.65
o4l09t24 23.7U 0.51 1.5 1 10.84 483
04t09124 17:31 23.705 1 1.5 0.5 1'l 1.01
04togt24 17:32 23.703 1 l 1.43 475
o4losl24 17:33 23.704 4720.511.4 111.64
0/,t09t24 '17:34 23.705 11.4 r 1 1.65 471
04t09t24 4710.411.3'17:35 23.705 111.74
ut09t24 17:36 23.7U 1'l .3 111.41 474
04t0st24 17:37 23.705 11 .3 475o.4 11't.77
o4./09n4 17:38 23.707 11.3 I t'l .64
utogl24 0.417:39 23.707 1'1.3 111.37 477
Page 41 of 70
F = Unit Offline
E = Exceedance
! = lnvalid
M = Maintenance
Report Generated: 04/ 29 I 24 74:13
GP043AS-036878- RT- 1 57 1
C = Calibration
S = Substituted
T = Out Of Control
04togt24 't7..40 23.704
Average Data - Run 3
P|ant: HUNTINGTON PLANT
lnterval: 1 Minute
Type: Block
Report Peri od: 041 Og I 2024 1 5: 40 Th rou gh 041 09 I 2024 1 8: 1 9
Time Online Criteria: 1 minute(s)
11.4 0.4 111.26
04t09t24 17'.41 23.706 47311.4 0.4 't11.4'l
ut09t24 17:42 23.706 o.411.4
04t09t24 17:43 23.705 11.4 0.4 11 1.58 472
o4l09t24 17:44 23.706 11.3 o.4 1 l 1.68 471
04t09124 23.706 I 1.3 111.74
o4t09t24 17:46 23.705 11.3 4720.5 11'1.71
o4t09t24 17:47 23.706 11.3 o.4 111.64 472
04t09t24 17:48 23.707 11 .3 0.4 111.43 473
o4n9t24 25.706 11.4 0.4 1't 1.15
ut09t24 '17:50 23.707 11.4 o.4 109.00 477
$4tost24 17:51 23.709 '11.4 0.4 108.72 478
o4n9t24 23.709 1 l.5 108.63 476
04to9124 17:53 23.710 fi.5 0.4 473
o/,togt24 17..54 23.710 1 1.5 t08.35
o4t09t24 17:55 11.4
o4lo9l24 17:56 23.710 11.4 0.4 108.52
04,t09t24 17i57 23.710 11.4 461
o4lo9l24 17'.58 23.709 11.3
ut09t24
04t09t24 18:00 23.710 1'1.1 107.40 4U
o4t09124 23.710 1't .5 107.01
ul09t24 18:02 23.709 1 1.5 0.4 107.08
o4lo9t24 23.707 1 1.5 107.59
04t09t24 18:04 23.709 1't.4 0.4 107.91
o4t09124 23.711
ut09124 18:06
04t09l24 18:07 23.7',tO 11.2 0.5 111.26
04t09t24 18:08 23.7'tO 'tl.2
o4t0,9,t24 18:09 23.710 11.2 0.4 111.22 409
utogt24 18:'10 23.711 11.2 11 1 .30 412
04to9t24 '18:11 23.711 11.2 416
o4to9t24 18:13 23.712 11.2
o4to9t24 23.711 11.2
utogt24 18:15 23.711 111.37
04109t24 l8:16 23.712 11.2
o4to9t24 23.710 11.2 111.A4
04t09t24 18:18 23.710 11.2
ut09t24 23.710 11.'l 1 11.81
Page 42 of 70
F = Unit Offline
E = Exceedance
I = lnvalid
M = Maintenance
Report Generated: 041 29 / 24 t4:73
GP043AS-036878-RT-1571
C = Calibration
S = Substituted
T = Out Of Control
Average Data - Run 3
Plant: HUNTINGTON PLANT
lnterval: 1 Minute
Type: Block
Report Period: 0410512024 15:40 Through 0410912024 18:19
Time Online Criteria: 1 minute(s)
Average 23.7u
Minimm 23.693
Madmum 23.712
Summatlon 3,792.589
F = Unit Offline
E = Exceedance
I = lnvalid
M = Maintenance
Report Generated: O4129124 t4:73
GP043AS-036878- RT-1 5 7 1
71.9 17,687.66
,11.4
11 .1
11.5
1,7*9.3
0.4
0.4
0.5
110.55
107.01
112.67
.{08
379
488
74,883
lncluded Data 160 154 160 160 '160
P^i6tc
Total numberof 160 160 160 160 180
nal. P^ihla
C = Calibration
S = Substituted
T = Out Of Control
Page 43 of 70
a ro
Appendix C
Laboratory Analysis Data
GP043AS-036878-RT- 1 571 Page 44 of 70
',1 la
,
i r.i I
Appendix C.1
Gravimetric Analyses
Page 45 of 70
ryh |l?,N l"+,9)!
Project Code:
EPA Method5l2O2 Gravimetric Analysis Report
PROJ-036878
Date Finalized:4126/2024
Analyst:G. Marston/T. Wojtach
Analytica! Narrative
Filters were dessicated and tared to a constant weight in the MAQS laboratory prior to sampling. Following testing,
the filters were dessicated for at least 24 hours, then weighed to a constant weight (10.5 mg). The acetone rinses
were measured to the nearest milliliter, transferred to tared aluminum weighing dishes, taken to dryness under a
fume hood, dessicated for at least 24 hours, then weighed to a constant weight (t0.5 mg). Each result above
represents total filterable particulate matter for each test run (acetone rinse + filter catch), with no blank correction
performed unless otherwise indicated.
Teflon CPM filters were extracted in a sonicator three times with water and three times with hexane. The extraction
water was added to the back-half impinger contents and extracted with hexane three times in a separatory funnel.
The inorganic fraction was transferred to a tared Teflon baggie, baked at 105C until 10 mL remained, taken to dryness
under a fume hood, dessicated for at least 24 hours, then weighed to a constant weight (t0.5 mg). The organic
fraction was combined with the acetone and hexane field rinses, measured to the nearest milliliter, transferred to a
tared aluminum weighing dish, taken to dryness under a fume hood, dessicated for at least 24 hours, then weighed
to a constant weight (t0.5 mg). No blank correction was performed unless otherwise indicated.
lnstrumentation
All measurements were taken using a Torbal Model AGCN200 Analytical Balance under laboratory conditions. The
instrument is auto-calibrated and challanged with three N|ST-traceable reference weights daily.
Detection Limit / Sensitivity
All measurements are recorded to 0.00019 (0,1mg).
Notes
No deviations from the analytical procedures from EPA Method 5 were noted. All samples were received in good
condition. After analysis, all samples are archived for a period of one year.
Attachments
Gravimetric Analysis Logs
Sample Chain of Custody
laboratory Results Summary
Sample !D Filterable Particulate Mafter (mel
Unit 2, Run #1 21.7
Unit 2. Run #2 19.0
Unit 2, Run #3 25.5
Sample !D Condensable Particulate Matter (mcl
Unit 2, Run f1 4,L
Unit 2, Run #2 5.2
Unit 2, Run #3 4.4
rBlank corrections were performed in accordance with EPA Method 5.
CPM value includes a field blank correction.
GP043AS-036878-RT- 1 57 1 Page 46 of 70
,a \ M\lh, l tl}lsh EpAMethod 5GravimetricAnalysis Log
Proiect Code:PROJ-036878
Unit lD:Unit 2
Front-Half Particulate Matter Filter Catch
Run #l
Filter# 1943
Final Filter Weight fi1 (g)
Final Filter Weight f2 (gl
Filter Tare Weight #1 (g)
Filter Tare Weight #2 (g)
Filter Catch (gl
Front-Half Partaculate Matter Acetone Rinse Catch
Run f2
L979
Run #3 Elank
2000 1993
Date Weisht (8) Date Weight (g) Date Weight (g) Date Weight (8)
4lL7 /24 0.3780 4lLtl24 0.3807 4/17124 0.3788 4h7/24 0.3753
4118/24 o3744 4/18/24 0.3811 4lL8/24 0.3790 4/18124 o.3758
L0/s/23 o.3744 LL/9/24 0.3756 LtlL0l23 0.3742 Lt/70/23 0.3753
o.3744 LtlLO/24 0.3758 tut3/23 o.3742 tLlt3/231 0.37s5
0.0038 0.00s2 0.fl)47 0.0001
Run fl
Rinse Volume (mL) 70.3
Rinse Mass (g) 55.2
Tin f 8399
Run #2
9t.7
72.O
8392
Run #3
85.6
67.2
8352
Blank
120.0
94.2
8397
Final Dish Weight #1 (g)
Final Dish Weight S2 (g)
Dish Tare Weight (g)
Dish Tare Weight (g)
Total Rinse Catch (g)
Acetone Blank Correction
Date weight (g)Date Date Weight (g)Date weisht (s)
4122124 6.4903 4/22/24 6.3457 4/22/24 6.3196 4/22124 | 5.430s
4/23/24 6.4904 4/23/24 6.34s2 4123/24 5.3192 4/23124 6.4303
6.47t9 2lsl24 6.3312 118124 5.2983 2lsl24 6.4296
216/24 6.4722 216124 5.3312 t/23/24 6.2980 216/24 | 6.4300
0.0183 0.0143 0.0212 0.0006
EPA Method 5 672.5: Acetone Blonk Concentrotion
m-0.6
V"". (Eq.5-4) (1r0X?85)= 6.37E-06 mSlmC
Where:
C o = Acetone blank residue concentrotion (mS/mS)
fr o = Moss of residue of ocetone ofier evoporotion (mg)
V o = Volume of ocetone blonk (nL)
p o = Density of ocetone (785 mg/mL)
EPA Method 5 672.7: Acetone Wosh Blonk
W" = C"V"rp" Eq. 5-S)
Where:
W o = Weight ol residue in ocetone wosh (mg)
C o = Acetone blonk residue concentrotion (mS/nS)
V ,n = Volume of ocetone wosh (mL)
p o = Density of ocetone (785 mg/mL)
Moximum Allowoble Blonk lma)
Run #7: (6.37E-06)(70.3)(78s) = 0.4 mg 0.6
Run #2: (6.37E-06)(91.7)(785) = 0.5 m9 0.7
Run #3: (6.37E-06)(85.6)(785) = 0.4 mg 0.7
Total Particulate Catch
Run #1
Filter Catch (g) 0.0038
+ Rinse Catch (g) 0.0183
-Acetone Blank (g) 0.0004
Run fr2
0.00s2
0.0143
0.0005
Run #3
0.0047
0.02t2
0.0004
Total PM (g! O.O2L7
GP043AS-035878-RT-157 1 Page 47 of 70
trth MYry
',TH)!EPA Method2O2 Gravimetric Analysis Log
Project Code:PROJ-036878
Unit lD:Unit 2
Back-Half Organic Particulate Matter Catch
Run fil
8354
Run #2
8355
Run #3
8356
Blank
8357Tin #
FinalWeight #1 (g)
FinalWeight #2 (gf
Tare Weight fr1 (g!
Tare Weight f2 (g)
Organic CPM Catch (g)
Back-Half lnorganic Particulate Matter Catch
Date Date weight (g) Date weight (g) Date Weight (g)
4/22/24 6.37t9 4122124 5.4056 4122/24 6.3564 4122124 6.3044
4123/24 6.37L7 4123/24 6.4055 4123/24 6.3552 4123124 6.3044
tl8/24 6.3700 Ll8/24 5.4033 u8/24 6.3542 7/8124 6.3019
U23124 6.3697 Ll23/24 6.4038 tl23/24 5.3541 u23/24 6.3020
0.0019 0.0020 0.0021 0.0024
Run #1
Teflon Baggie * L867
Run f2
1858
Run #3
1858
Blank
1853
Final Weight fl (g)
Final Weight #2 (g)
Tare Weight f1 (g)
Tare Weight #2 (g)
lnorganic CPM Catch (g)
Condensable Particulate Catch
Date weight (8) Date weight (g) Date weiSht (g) Date weight (g)
4124124 3.9977 4124/24 3.9311 4/2s124 3.8951 4l2sl24 3.9833
4l2sl24 3.9978 4/2s/24 3.931s 4/26124 3.8947 4126/24 3.9830
216124 3.9936 216124 3.9262 216/24 3.8908 216124 3.982
2/7/24 3.993s 217124 3.9260 217124 3.8904 217/24 3.9816
0.0042 0.00s2 0.0043 0.0014
Organic CPM Catch (g)
+ lnorganic CPM Catch (g)
- CPM Blank (g!
Run f1
0.0019
0.0042
0.0020
Run #2
0.0020
0.0052
0.0020
Run fi3
0.0021
0.0043
0.0020
TotalcPM (g)0.0041 0.0052 0.0044
GP043AS-036878-RT-1571 Page 48 of 70
MONTROSE
,ir[-F" -, :l i;XI. IT" 5:li'fi:^I5
Laboratory Chain of Custody Record
oseeT 6
?o-$uor
)vnat"rZ
C. Korvn
Sample lD / Run #
Date 4// 7/2
GP043AS-036878-RT-157 I Page 49 of 70
t 1l
Appendix D
Quality Assurance/Quality Control
Page 50 of 70GP043AS-036878-RT-1 57 1
I ro
Appendix D.1
Units and Abbreviations
GP043AS-036878-RT-1 57 1 Page 51 of 70
6O AT?N,I+P,T.H
UNITS AND ABBREVIATIONS
@Xo/o 02 corrected to X% orygen (corrected for dilution air)
lCCl absolute value of the confidence coefficient
ldl absolute value of the mean differencesoC degrees CelsiusoF degrees FahrenheitoR degrees Rankine
" HzO inches of water column
13.6 specific gravity of mercury
AH pressure drop across orifice meter, inches H2O
AP velocity head of stack gas, inches H2O
e total sampling time, minutespS microgram
9" density of acetone, mg/ml
Pw density of water, 0.9982 g/ml or 0.002201 lb/ml
acfm actual cubic feet of gas per minute at stack conditionsAn cross-sectional area of nozzle, ft'
As cross-sectional area of stack, square feet (ft')
Btu British thermal unit
B*" proportion by volume of water vapor in gas stream
C" particulate matter concentration in stack gas, gr/acf
Cn s average unadjusted gas concentration, ppmv
Coi, measured concentration of calibration gas, ppmv
cf or ft3 cubic feetcfrn cubic feet per minute
Cc"" average gas concentration adjusted for bias, ppmv
CM average of initial and final system bias check responses from upscale calibration gas, ppmv
cm or m3 cubic meters
Cun actual concentration of the upscale calibration gas, ppmvCo average of initial and final system bias check responses from lowievel calibration gas, ppmvCp pitot tube coefficient
Cs particulate matter concentration in stack gas, gr/dscf
CS calibration span, % or ppmv
Cs measured concentration of calibration gas, ppmv
Cv manufactured certified concentration of calibration gas, ppmv
D drift assessment, % of spandcf dry cubic feetdcm dry cubic meters
Dn diameter of nozzle, inches
Ds diameter of stack, inches
dscf dry standard cubic feetdscfrn dry standard cubic feet per minutedscm dry standard cubic meters
Fd F-factor, dscf/MMBtu of heat input
fom feet per minutefps feet per secondft feet
# square feet
gram
gallonsgr grains (7000 grains per pound)gr/dscf grains per dry standard cubic feet
hour
s
gal
GP043AS-036878-RT- 1 57 1 Page 52 of 70
60 l*?.NI+gLE
UNITS AND ABBREVIATIONS
I percent of isokinetic sampling
in inch
k kilo or thousand (metric units, multiply by 103)
K kelvin (temperature)
Ks conversion factor 0.0154 gr/mg
& conversion factor 0.002668 ((in. HgXft'))/((mlX"R))
kg kilogram
l$ pitot tube constant (85.49 fUsec)
kwscfh thousand wet standard cubic feet per hour
I liters
lb/hr pounds per hour
lb/MMBtu pounds per million Btu
lpm liters per minute
m meter or milli
M thousand (English units) or mega (million, metric units)
m3 cubic meters
ma mass of residue of acetone after evaporation, mg
Md molecular weight of stack gas; dry basis, lb/lb-mole
meq milliequivalent
mg milligram
Mg megagram (106 grams)
min minute
ml or mL milliliter
mm millimeter
MM million (English units)
MMBtu/hr million Btu per hour
mn total amount of particulate matter collected, mg
mol mole
mol. wt. or MW molecularweight
Ms molecular weight of stack gas; wet basis, lb/lb-mole
MW molecular weight or megawatt
n number of data points
ng nanogram
nm nanometer
Po", barometric pressure, inches Hg
pg picogram
Ps stack static pressure, inches H2O
Pm barometric pressure of dry gas meter, inches Hg
ppb parts per billionppbv parts per billion, by volumeppbvd parts per billion by volume, dry basisppm parts per millionppmv parts per million, by volumeppmvd parts per million by volume, dry basis
ppm\ ff parts per million by volume, wet basis
Ps absolute stack gas pressure, inches Hg
psi pounds per square inchpsia pounds per square inch absolutepsig pounds per square inch gauge
Psto standard absolute pressure, 29.92 inches Hg
Q" volumetric flow rate, actual conditions, acftn
Qs volumetric flow rate, standard conditions, scftn
Qsto volumetric flow rate, dry standard conditions, dscfrn
R ideal gas constant 21.85 ((in. Hg) (ft3)y(("R) (lbmole))
GP043AS-036878-RT- 1571 Page 53 of 70
6(\ l*?N,I+gp.H
UNITS AND ABBREVIATIONS
SBn,,"r post-run system bias check, % of span
SBi pre-run system bias check, % ofspan
scf standard cubic feetscfh standard cubic feet per hourscftn standard cubic feet per minutescm standard cubic metersscmh standard cubic meters per hoursec second
sf, sq. ft., or ft2 square feetstd standardt metric ton (1000 kg)
T o.szs t-value
Ta absolute average ambient temperature, oR (+459.67 for English)
T, absolute average dry gas meter temperature, oR (+459.67 for English)
ton ort ton = 2000 pounds
tph ortons/hr tons per hour
tpy ortons/yr tons peryear
Ts absolute average stack gas meter temperature, oR (+459.67 for English)
T*a absolute temperature at standard conditions
V volt
% volume of acetone blank, ml
Vaw volume of acetone used in wash, ml
V" total volume H2O collected in impingers and silica gel, grams
Vm volume of gas sampled through dry gas meter, fto
Vm(std) volume of gas measured by the dry gas meter, corrected to standard conditions, dscfVma stack gas volume sampled, acf
Vn volume collected at stack conditions through nozzle, acf
% average stack gas velocity, feet per second
Vwc(std) volume of water vapor condensed, corrected to standard conditions, scf
Vwi(std) volume of water vapor in gas sampled from impingers, scf
V*.s1.t01 volume of water vapor in gas sampled from silica gel, scf
W" weight of residue in acetone wash, mg
Wirp total weight of impingers, grams
totalweight of silica gel, grams
dry gas meter calibration factor, dimensionless
Wss
Y
GP043AS-036878-RT-1571 Page 54 of 70
64\ lt?,N,T+gp.H
AAS
ACDP
ACE
AD
ADL
AETB
AS
ASTM
BACT
BDL
BHP
BIF
BLS
CC
CD
CE
CEM
CEMS
CERMS
CET
CFR
CGA
CHNOS
CNCG
CO
COC
COMS
CPM
CPMS
CT
CTM
cro
CVAAS
De
DE
Dioxins
DLL
DNCG
ECD
EIT
ELCD
EMPC
EPA
EPRI
ES
ESP
EU
FCCU
FGD
FI
FIA
FID
FPD
FPM
FTIR
FTPB
FTRB
Furans
GC
ACRONYMS
atom ic absorption spectroscopy
air contaminant discharge permit
analyzer calibration error, percent of span
absolute difference
above detection limit
Air Emissions Testing Body
applicable standard (emission limit)
American Society For Testing And Materials
best achievable control technology
below detection limit
brake horsepower
boiler and industrial furnace
black liquor solids
confidence coefficient
calibration drift
calibration error
continuous emissions monitor
continuous emissions monitoring system
continuous emissions rate monitoring system
calibration error test
Code of Federal Regulations
cylinder gas audit
elemental analysis for determination of C, H, N, O, and S content in fuels
concentrated non-condensable gas
catalytic oxidizer
chain of custody
continuous opacity monitoring system
condensible particulate matter
continuous parameter monitoring system
combustion turbine
conditional test method
catalytic thermal oxidizer
cold vapor atomic absorption spectroscopy
equivalent diameter
destruction efficiency
polychlorinated dibenzo-p{ioxins (pcdd's)
detection level limited
dilute non-condensable gas
electron capture detector
Engineer ln Training
electoconductivity detector (hall detector)
estimated maximum possible concentration
US Environmental Protection Agency
Electric Power Research lnstitute
emission standard (applicable limit)
electrostatic precipitator
emission unit
fluid catalytic cracking unit
fl ue gas desulfurization
flame ionization
flame ionization analyzer
flame ionization detector
fl ame photometric detector
fi lterable particulate m atter
Fourier-transform infrared spectroscopy
field train proof blank
field train recovery blank
polychlorinated dibenzofurans (pcdfs)
gas chromatography
GP043AS-036878-RT-157 1 Page 55 of 70
6d ttgtxT+gp.H
ACRONYMS
GC/MS gas chromatography/mass spectroscopyGFMS graphite furnace atomic absorption spectroscopy
GFC gas filter correlation
GHG greenhouse gas
HAP hazardous air pollutant
HC hydrocarbons
HHV higher heating value
HPLC high performance liquid chromatographyHRGC/HRMS high-resolution gas chromatography/high-resolution mass spectroscopyHRSG heatrecoverysteam generator
lC ion chromatography
ICAP inductively-coupled argon plasmography
ICPCR ion chromatography with a post-column reactorICP-MS inductively coupled plasma-mass spectroscopylR infrared radiation
ISO lnternational Standards OrganizationkW kilowatts
LFG landfill gas
LHV lower heating value
LPG liquified petroleum gas
MACT maximum achievable control technologyMDI methylene diphyenyl diisocyanateMDL method detection limitMNOC maximum normal operating conditionsMRL method reporting limitMS mass spectrometryNA not applicable or not availableNCASI National Council For Air And Steam lmprovementNCG non-condensable gases
ND not detectedNDIR nondispersive infraredNESHAP National Emissions Standards For Hazardous Air PollutantsNG natural gas
NIOSH National lnstitute For Occupational Safety And HealthNIST National lnstitute Of Standards And TechnologyNMC non-methane cutterNMOC non-methane organic compoundsNMVOC non-methane volatile organic compoundsNPD nitrogen phosphorus detectorNSPS New Source Performance StandardsOSHA Occupational Safety And Health AdministrationPAH polycyclic aromatic hydrocarlconsPCB polychlorinated biphenylcompoundsPCWP plywood and composite wood products
PE Professional EngineerPFAS per- and polyfluoroalkyl substances (PFAS)
Pl photoionization
PID photoionization detectorPM particulate matter
PMro particulate matter less than 10 microns in aerodynamic diameter
PMz.s particulate matter less than 2.5 microns in aerodynamic diameter
POM polycyclic organic matterPS performance specificationPSD particle size distributionPSEL plant site emission limitsPST performance specification testPTE permanent total enclosurePTM performance test method
GP043AS-036878-RT-157 1 Page 56 of 70
60 l*?NI+gp.H
ACRONYMS
QA/QC quality assurance and quality control
Ql Qualified lndividual
QSTI Qualified Source Testing lndividual
RA relative accuracy
RAA relative accuracy audit
RACT reasonably avaihbb control technologyRATA relative accuracy test audit
RCTO rotary concentrator thermal oxidizerRICE stationary reciprocating internal combustion engine
RM reference method
RTO regenerative thermal oxidizer
SAM sulfuric acid mist
SCD sulfur chemiluminescent detector
SCR selective catalytic reduction system
SD standard deviation
Sem|-VOST semivolatile organic compounds sample train
SRM standard reference material
TAP toxic air pollutant
TBD to be determined
TCA thermal conductivity analyzer
TCD thermal conductivity detector
TGNENMOC total gaseous non-ethane non-methane organic compoundsTGNMOC total gaseous non-methane organic compounds
TGOC total gaseous organic compoundsTHC total hydrocarlcons
TIC tentatively identified compoundTO thermal oxidizerTO toxic organic (as in EPA Method TO-15)TPM total particulate matter
TSP total suspended particulate matterTTE temporary total enclosure
ULSD ultralow sulfur dieselUV ultraviolet radiation range
VE visible emissionsVOC volatile organic compoundsVOST volatile organic sample trainWC water columnWWTP waste watertreatment plant
G P043AS-036878-RT- 1 57 1 Page 57 ot 70
Se
Soz
Sog
SO,
TCDD
TCDF
TGOC
THC
TI
TRS
Zn
Ag
As
Ba
Be
c
Cle
cl02
co
Co
Coz
Cr
Cu
Eto
Hzo
N2
NHs
Ni
NO
Noz
NO"
o2
6/I ltgN,I+gp.H
silver
arsenic
barium
beryllium
carbon
Cd cadmium
CdS cadmium sulfide
CH2O formaldehyde
CH3CHO acetaldehyde
CH3OH methanol
CH, methane
C2H4O ethylene oxide
CzHo ethane
CaH4O acrolein
CaH6O propionaldehyde
CeHs propane
C6H5OH phenol
chlorine
chlorine dioxide
carbon monoxide
cobalt
carbon dioxide
chromium
copper
ethylene oxideEIOH ethyl alcohol (ethanol)
H2 hydrogen
HzOz hydrogen peroxide
HzS hydrogen sulfide
H2SO4 sulfuric acid
HCI hydrogen chlorideHg mercuryIPA isopropyl alcoholMDI methylene diphyenyl diisocyanate
MeCl2 methylene chloride
MEK methyl ethyl ketoneMeOH methanolMn manganese
nitrogen
ammonia
nickel
nitric oxide
nitrogen dioxide
nitrogen oxides
oxygen
P phosphorusPb leadPCDD polychlorinated dibenzo-p{ioxinsPCDF polychlorinated dibenzofurans
antimony
CHEMIGAL NOi'ENCLATURE
selenium
sulfur dioxide
sulfur trioxide
sulfur oxides
tetrachlorodibenzodioxin
tetrach lorod ibenzofuran
total gaseous organic concentration
total hydrocarbons
thallium
total reduced sulfur compounds
zinc
GP043AS-036878-RT-1 571 Page 58 of 70
Appendix D.2
Manual Test Method QA/QC Data
EPA tlethod 5
Meter Box Calibration by Calibrated Critical Orilice,
Leak Check, and Thermocouple Calibration Check
English Meter 8ox Units, English K'Factor
Yd:0.0970
AH@r 1.742
n.b? Bor Otinc. C.llbtrton
flHTff td d rn u{r r[^Mv*s rl*t t b 2. $ F& rh rn llB4 qdv]un tM e
flffitM rn cn4 ffi. ffid. ('. m, Bffi . End.n 6. oH1o9 R)! !(.ngf{mD
F,CF6 f& Y. E.&olh l@E dlE atwds ilrlott cyF dd
Ed&lffiadrMtuMmltFil r,0O2
rdffi.Ntefdd6rlc, rm .ffi rem, 6t cEld.st6 looT!fr d,
ioF dre .&rds,e4s!&lred&@tutmh.e! tr.82
Iatar Bor Vrcuum L.'k Chrck
E&(ffitErt@8tffi.)
2a
malrr 8or Praa.utt Lcah Ch.sl
X.!3r Bor Th.rmocouplo R..dout C.llbr.tioo Chock
lxd-d"L.h&rr9,Htth
IE
zw 239 &!
a
GP043AS-036878-RT- 157 1 Page 50 of 70
EPA Method 5
Meter Box Calibration by Calibrated Critical Orifice: Post-Test,
English Meter Box Units, English K' Factor
,rte:4t15124
DENVER CO
r ^t nrn. l&hult 3l :i
hremeidc onsauE lin. Hol:24.32 tn. Hg
t.6Eiidl c#al Ecuum ll47 in Hd
:urrent Cal. Yd:0.9870
rost-test Yd:0.9894
,ost-test Result:PASS
Meter Box Orifice Calibration
IMPORTANT Forvalid l6t resuh, hetutual Vacuum 3hould b€ 1 to 2 in. Hg gr6abrUan the Th6or6tical Cdical Vacuum shom ebov6
IMPORTANT Th€ Criical Orffice Coeficiont K', musl b6 6nt6red in English unft, {fi)^3'(deg Rf0.5((in.Hg)'(min))
- SAMPLE RATE -
INDCATED VS. ACTUAL
For Calibraton Fador Y, th6 ratio of Ss reading ofthe calibraton m6t€r to th6 dry gas m€t€r,
.c@pbble tderane of individual valuas fom the average is +10.02.
ForOrifce CalabEtion Fador AH@, So orilice diferental pressuro in inch6s ofH20that equates to 0.75 cfrn ofai
at 68 F and 2S.9 inch€s of Hg, accepbble tolerance ofindilidual values from the average is +/{.2
AH Tim€lnfral Net lnld out6t lnlet outet SETEil tnfrat Fhel
o
adjustvaMa tullyopon, fns adjusttully closd, semplo inlet plugged
be 2610 (mtd dialsbbb for 1 minu6)
Meter Box Vacuum Leak Check
T..tv..uum /in H.\1o
0
Nam6
GPq3S-036678-RT-1571
I
i
I
I
TEITIODs CRMCAL OruFrcE CALIBRANO}I
GRIII:AL OEFTCE Ser en: @!
[T,l ' f*F-l
-
l-iifrTffiil .ar
l_J t I r! I r! I lrr. l.LElgr.:L!!$.d Gzro
[Tl ' r--T;-l
-
EEI .'oI I r I rc I tl I lre.rol lrrsrlzro.rl ew
l;l ,|_,-ril _ @@.,,.l_l t I 16 | il | I,Dr.J lzDrulilr.rarlalrr
l;l ,T;-rl.l _ @f@.,..l_l r | il | r. tl4J lrrrr, l?lrrcl..r.!
rnBllcctmtCE,llcxr^lnt'mmC-tObff r*rDd-p.dnc$hmrahlEfr,ri&-hoqtfrrE, y,'a[{rrfr htE eALh(8.er Om!-q*rnF tt'joht .ttHdar.dfr i.
cHffiId. ffi.
.e.ot
at,at
o.rt
o.L
,ofi
?0r!
,ott
7!...
rur
lt-r
Gla
{.tc
ort
GOt
ooa
a.oa
T-;-l l-"., If ro--j f;t-]
AIAI K FrgIOR.l-fi] T-;lf;oo- f ,--1
ort0a o.ltlt t.7tat{a
GIGd
0.?0lt 0ttl2 a.lttE{a
orfla ll or2ro 4.210E{a
lc . cfualslic.oofichrt
lG1fRtta)trtorr.xsxmtn.)l - Enstbh unht
t(tto|tlcx)ultl[(mm Hcxmtn.tt - t.trtcilbll untr
(mTKlrtrUt(mm ttgxmtnJt . t.t to Unttr
0.0t
{.01
{.fi
0.il
fI ' [rg--I-l-l fffiTrr*-] .-'[J ' I tTr.--] lll.lll l-ffiTurril .,o
EiylrmE &fetyco., ha . 706 E Ctr6 Bfid, ouili, t{c 270a .
GP043AS-036878-RT.157 1
elle!..at - w.diuwlyd @1721.
Page 62 of 70
*'*T=l
ir.1 &, s ru
i.t att ru .t.?U
oa 3.t
o.a L att aa.t ,n2
n-,D-t [2 il
d,D-t tu ?Gt ttt
dt D/nt at fr,
tl m/,o.a nt-tf.t
It tut na A'
aa.l ,oa rut ,t,t ,t.t
Appendix D.3
Instrumental Test Method QA/QC Data
PROI-036878
PaclflCorp
Huntlngon Unlt 2
4lel2o24
EPA Method 3A
Calibration Error Check
lnltlal
Gas Concentratlon Value Response
Or Low
E80141006 Mid
E80156888 High
COr Low
E80141006 Mid
E80156888 High
T.dlar BagAnalFls Data
Run #1
Run f2
Run #3
010
LO.47 I 10.5
21.19 I 2t.t
0t0.1
8.925 ! 9.1
t7.82 a L7.8
(,2 Gor
6.7
6.5
6.8
L2.3
t7:4
L2,L
Enor Ol(?
0.0% Y
0.r% Y
0.4Yo Y
0.6% Y
L,O% Y
0.t% Y
GP043AS-036878- RT- 1 5 7 1 Page @ of 70
AiIgas.
an Air Liquide company
Airgas Specialty Gases
Airgas USA LLC
SzS North Industrial loop Road
Tooele, UT 84o74
Airgas.com
Part Number:E03N180E15A0015
Grade of Product: EPA PROTOCOL STAIYDARI)
CERTIFICATE OF AIVALYSIS
Reference Number:
Cylinder Volume:
Cylinder Pressure:
Valve Outlet:
Certification Date:
1 53-402892933-1
150.0 cF
2015 PSrG
590
Nov't4, 2023
CylinderNumber: EB0141006
Laboratory:124 - Tooele (SAP) - UT
PGVP Number: 872023
Gas Code:CO2,02,BALN
Expiration Date: Nov i4,203i
Certification performed in accordance with "EPA Trac€ability Probcol for Assay and Certmcation of Gaseous Calibration Standards (May 2012)" document EPA
600/R-12/531, using the assay procedures listed. Analytical Methodology does not require conection for analytical intederence. This cylinder has a btal analytical
uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mDdure. All concentrations are on a
mole/mole basis unless otheMise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval of the laboratory. Do
Not Use This below'100 osio. i.e- 0.7
Triad Data Available Upon Request
Sionature on file
Approved for Release
G P043AS-036878-RT- 1 57 1
Page 1 of 1
Page 65 of 70
ANALYTICAL RESULTS
Actual ProtocolConcentration Method
TotalRelative
Uncertainty
CARBON DIOXIDE
OXYGEN
NITROGEN
9.000 7o
10.50 o/o
Balance
8.925 o/o
10.47 o/o
G1
G1
+l- 1.0o/o NIST Traceable
+l- 0.8o/o NIST Traceable
11t14t2023
1',U1412023
CALIBRATION STANIDARDS
No Concentration
NTRM
NTRM
1306041 1
98051010
cc413537
SGg161286BAL
7 .489 OA CARBON DIOXIDE/NITROGEN
1 2.05 O/O OXYGEN/N ITROGEN
0.6%
0.7o/o
May'14,2025
Dec 14,2023
ANALYTICAL EQTIIPMENT
Analytical Principle
Horiba VIA-510 SV4MEUTJ CO2
Horiba MPA-510 W603MM58 02
od 17,2023
od 17,2023
AiIgas.
an AirUquide company
Airgas Specialty Gases
Airgas USA LLC
525 North Industrial Ioop Road
Tooele, IIT 84o74
Airgas.com
Part Number:
Cylinder Number:
Laboratory:
PGVP Number:
Gas Code:
Reference Number:
Cylinder Volume:
Cylinder Pressure:
Valve Outlet:
Certification Date:
153-402506334-1
158.0 CF
2015 PS|G
590
4u908,2022
Expiration Date: Auq 08.2030
Certification performed in accordance with 'EPA Traceability Probcol for Assay and Certmcation of Gaseous Calibration Standards (May 2012)" document EPA
600/R-12/531, using the assay procedur* listed. Analytical Methodology does not require conection for analytical interference. This cylinder has a total analytical
uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a
mole/mole basis unless otheMise noted. The results relate only to the items tested. The report shall not be reproduced except in full without approval of the laboratory. Do
Triad Data Available Upon Request
Sionature on file
Approved for Release
GP043AS-036878-RT- 1 57 1
Page I of I
Page 66 of 70
CERTIFICATE OF ANALYSIS
Grade of Product: EPA PROTOCOL STANDARI)
E03Nt61E15A0287
EB01 56888
124 - Tooele (SAP) - UT
872022
co2,02,BALN
Not use this below 100 03io. i.e. 0.
Component Requested
Concentration
ANALYTICAL RESULTSActual ProtocolConcentration Method
TotalRelative
Uncertainty
Assay
Dates
CARBON DIOXIDE
OXYGEN
NITROGEN
18.00 %
21.00 o/o
Balance
17.82 Yo
21.19 o/o
G1
G1
+l- 0.7o/o NIST Traceable
+l- 0.60/o NIST Traceable
08108t2022
o810812022
CALIBRATION STAIVDARDSType Lot ID Cylinder No Concentration Uncertainty Expiration Date
NTRM
NTRM
1 3060802
09061434
cc415397
cc282492
24.04 Oh CARBON DIOXIDE/NITROGEN
22.53 Yo OXYGEN/N ITROGEN
0.6%
0.4o/o
Dec 11 ,2025
Mav 13. 2025
I nstrumenUMakeliiodel
ANALITICAL EQUIPMENT
Analytical Princlple Last Multipoint Calibration
Horiba VIA-510 SV4MEUTJ CO2
Horiba MPA-510 W603MM58 02
CO2 NDIR (Dixon)
02 Paramagnetic (Mason)
Jul 20,2022
Jul 20,2022
Appendix D.4
Accreditation Informatio n I Certifications
STAE Americon Associotion f or Loborotorv Accreditotion
Accredited Air Emission Testing Body
A2LA hos qccrediled
MONTROSE AIR QUALITY SERVICES
ln recognition of the successful completion of lhe joint A2LA ond Stock Testing Accreditotion Council (STAC)
evoluotion process, this loborotory is occredited to perform testing octiviiies in complionce with
ASTM D7036:2004 - Stondord Proctice for Compelence of Air Emission Tesiing Bodies.
Vice President, Accreditotion Services
For the Accrediiolion Council
Cerlificote Number 3925.01
Volid to Februory 28,2026
This aureditatinn program is not included under the A2LA ILAC Mutual Recognitinn Arrangement.
GP043AS-036878-RT-157 I Page 68 of 70
this 27tt'doy of Februory 2024,
CERTIFICATE OF COMPLETION
Craig Kormylo
This document certifies that this individual has passed a comprehensive examination and is now a
Qualified lndividual (Ql) as defined in Section 8.3 of ASTM D7036{4 for the following method(s}:
Source Evaluation Society Group 1: EPA Manual Gas Volume and Flow Measurements and lsokinetic
Pafticulate Sampling Methods
Certifi cate N umber: 043-2020-3
-*r/t--cl DATE oF ISSUE: 12131120
Tate Strickler, VP - Quality Systems
DATE OF
EXPIMTION: 12130125
M$PNTNPJ
GP043AS-036878-RT- r57 r Page 69 of 70
This is the Last Page of This Document
If you have any questions, please contact one of the following
individuals by email or phone.
Name: Craig Kormylo
Title: District Manager
Region: USA - Stack - Great PIains - Operations
Email : [e-mail]
Phone: [phone]
Name: Glen Capra
Title: Vice President
Region: USA - Stack
Email : [e-mail]
Phone: (5L2) 772-6450
UTAH DEPAHTMENT OF
EI.IVIRONMENTAL OUALITY
MAY 1 3 2024
DIVISION OF AIR QUALITV
Source Information
Division of Air Quality
Compliance Demonstration
Source Information
Company Name PacifiCorp Huntington - Unit No. 2
Company Contact:Richard Neilsen
Contact Phone No.435-687-4334
Source Designation:Unit No. 2
Test & Review Dates
Test Date: 4/9/2024
Review Date: 5/16/2024 Tabs Are Shown
Observer:
Reviewer:Paul Morris
Particulate Emission Limits
lbs/MMBtu lbs/hr gr/dscf
70.000
Emission Rates - "Front Half"
lbs/MMBtu lbs/hr gr/dscf
0.0093 40.7770 0.0043
Test Information
Stack_I.D._inches As ft^2 Y Dl H @ Cp Pbar Pq (static)Dn
322.54 567.39 0.9970 1.782 0.84 23.74 -4.3 0.252
Contractor Information
Contracting Company: Montrose Air Quality Services, LLC
Contact: Cheyney Guymon
Phone No.: 801-794-2950
Project No.:
1840
Circular
10100
9780
9860
9190
8710
8710
8710
10540
10640
11950
320
10610
10200
10390
1970
1800
1910
1420
1040
1190
1250
F factor usedF factors for Coal, Oil, and Gas
Anthrocite 2
Lignite
Natural
Propane
Butane
COAL
OIL
GAS
Bituminous 2
Fd Fw Fc
scf/MMBtu scf/MMBtu scf/MMBtu
O2
CO2
lbs/MMBtu
Page 1
Summary
Division of Air Quality
Reference Methods 5 - TSP
Compliance Demonstration of
PacifiCorp Huntington - Unit No. 2
Testing Results Lab Data - grams collected
Test Date 4/9/2024 4/9/2024 4/9/2024 4/9/2024 Lab Data Probe Filter Back
Circular Run 1 Run 2 Run 3 Run 4 Run 1 0.0183 0.0038 0.0041
As ft^2 567.39 567.39 567.39 Run 2 0.0143 0.0052 0.0052
Pbar 23.74 23.74 23.74 Run 3 0.0212 0.0047 0.0044
Pq (static)-4.30 -4.30 -4.30 Run 4
Ps 23.42 23.42 23.42
Avg. Ts F 113.92 114.75 114.25 Front Half Emissions Summary
CO2 - FCO2 12.30 12.40 12.10 Run 1 Run 2 Run 3 Run 4 Avg.
O2 6.70 6.50 6.80 gr./dscf 0.0045 0.0036 0.0049 0.0043
N2+C 81.00 81.10 81.10 lbs/hr 42.3367 34.1390 45.8554 40.7770
Md 30.24 30.24 30.21 lbs/MMBtu 0.009591811 0.00756917 0.010631063 0.0093
Ms 28.79 28.73 28.75
Y 1.00 1.00 1.00
Cp 0.84 0.84 0.84 Total Emissions Summary w/back half condensable
Vm cf 94.60 106.06 103.43 Run 1 Run 2 Run 3 Run 4 Avg.
Vlc 215.90 253.40 236.20 gr./dscf 0.0053 0.0045 0.0057 0.0052
AVG. Tm F 62.33 68.67 71.83 lbs/hr 50.1910 43.2427 53.6455 49.0264
Vm std 75.99 84.28 81.68 lbs/MMBtu 0.011371287 0.009587615 0.012437113 0.0111
Vw std 10.16 11.93 11.12
Bws 0.12 0.12 0.12
S Bws 0.12 0.13 0.13
Avg. Sqrt
Dlp 0.77 0.78 0.76
Vs 50.87 52.00 50.67 F factor used
scfm wet 1247433.08 1273091.27 1241788.07 1840
acfm 1731948.44 1770139.06 1725112.22
Qsd dscfh 66016963.34 66915294.94 65580267.49
# Sample
Points 24.00 24.00 24.00
Dn 0.252 0.252 0.252
An 3.46E-04 3.46E-04 3.46E-04
Start Time 0:00 0:00 0:00
End Time 0:00 0:00 0:00
Total Test
time 120.00 120.00 120.00
Time @ point 10.00 10.00 10.00
80.00
90.00
100.00
110.00
120.00
1 3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43 45 47
%
I
s
o
k
i
n
e
t
i
c
Points
Run 1 PxP Isokinetic
80.00
90.00
100.00
110.00
120.00
1 3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43 45 47
%
I
s
o
k
i
n
e
t
i
c
Sample Points
Run 2 PxP Isokinetic
80.00
90.00
100.00
110.00
120.00
1 3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43 45 47
%
I
s
o
k
i
n
e
t
i
c
Sample Points
Run 3 PxP Isokinetic
O2
CO2
lbs/MMBtu
80.00
90.00
100.00
110.00
120.00
1 3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43 45 47
Sample Points
Run 4 PxP Isokinetic
Page 1
Run 1
PacifiCorp Huntington - Unit No. 2 Flow & Moisture Test Date 4/9/2024
As ft^2 Pbar Pq (static) Ps Avg. Ts F CO2 - FCO2 O2 N2+C Md Ms
567.39 23.74 -4.30 23.42 114 12.30 6.70 81.00 30.24 28.79
Y Cp Vm cf Vlc Avg. Tm F Vm std Vw std Bws S Bws 0.1244
0.9970 0.84 94.597 215.90 62.33 75.987 10.162 0.1180 0.1244 0.999
Avg. Sqrt
Dlp Vs scfm wet acfm Qsd dscfh
# Sample
Points Dn
Total Test
time (minutes)
Time @ point
(minutes)Avg. Dlh
0.768 50.87 1,247,433 1,731,948 6.60E+07 24 0.252 120 10.00 1.591667
FALSE
Point No.Meter (cf) dl "p" dl "h" ts F tm F (in) tm F (out) Imp. Liquid Collected
1 285.190 0.40 1.10 114 57 Wt. (Final) Wt. (Initial) lc
2 292.022 0.67 1.80 112 59 604.20 493.70 110.5
3 300.163 0.71 1.90 115 60 709.50 652.70 56.8
4 308.828 0.45 1.20 114 61 765.50 741.50 24.0
5 315.940 0.68 1.80 115 61 925.90 901.30 24.6
6 324.352 0.72 1.90 113 62 0.0
7 333.005 0.44 1.20 115 62
8 340.070 0.63 1.70 113 64 Isokinetics 94.3
9 348.040 0.67 1.80 113 64 Test Date 4/9/2024
10 356.090 0.53 1.40 114 65 Start Time enter
11 363.642 0.60 1.60 115 66 End Time
12 371.532 0.64 1.70 114 67 Run 1
13 379.787
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
Page 1
Run 2
PacifiCorp Huntington - Unit No. 2 Flow & Moisture Test Date 4/9/2024
As ft^2 Pbar Pq (static) Ps Avg. Ts F CO2 - FCO2 O2 N2+C Md Ms
567.39 23.74 -4.30 23.42 115 12.40 6.50 81.10 30.24 28.73
Y Cp Vm cf Vlc Avg. Tm F Vm std Vw std Bws S Bws 0.1273
0.9970 0.84 106.058 253.40 69 84.279 11.928 0.1240 0.1273 0.999
Avg. Sqrt
Dlp Vs scfm wet acfm Qsd dscfh
# Sample
Points Dn
Total Test
time (minutes)
Time @ point
(minutes)Avg. Dlh
0.783 52.00 1,273,091 1,770,139 6.69E+07 24 0.252 120 10.00 2.00
FALSE
Point No.Meter (cf) dl "p" dl "h" ts F tm F (in) tm F (out) Imp. Liquid Collected
1 382.707 0.52 1.70 115.0 63.0 Wt. (Final) Wt. (Initial) lc
2 390.940 0.65 2.10 113.0 65.0 454.30 346.90 107.4
3 399.942 0.68 2.20 113.0 67.0 710.40 648.20 62.2
4 409.265 0.52 1.60 115.0 68.0 729.20 675.10 54.1
5 417.292 0.66 2.30 116.0 69.0 958.20 928.50 29.7
6 426.355 0.67 2.20 114.0 70.0 0.0
7 435.692 0.49 1.60 116.0 70.0
8 443.695 0.64 2.10 116.0 70.0 Isokinetics 103.2
9 452.740 0.70 2.20 116.0 70.0 Test Date 4/9/2024
10 462.190 0.56 1.80 114.0 71.0 Start Time
11 470.550 0.63 2.00 115.0 70.0 End Time
12 479.430 0.67 2.20 114.0 71.0 Run 2
13 488.765
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
Page 1
Run 3
PacifiCorp Huntington - Unit No. 2 Flow & Moisture Test Date 4/9/2024
As ft^2 Pbar Pq (static) Ps Avg. Ts F CO2 - FCO2 O2 N2+C Md Ms
567.39 23.74 -4.30 23.42 114 12.10 6.80 81.10 30.21 28.75
Y Cp Vm cf Vlc Avg. Tm F Vm std Vw std Bws S Bws 0.1255
0.9970 0.84 103.432 236.20 72 81.675 11.118 0.1198 0.1255 0.999
Avg. Sqrt
Dlp Vs scfm wet acfm Qsd dscfh
# Sample
Points Dn
Total Test
time (minutes)
Time @ point
(minutes)Avg. Dlh
0.764 50.67 1,241,788 1,725,112 6.56E+07 24 0.252 120 10.00 1.89
FALSE
Point No.Meter (cf) dl "p" dl "h" ts F tm F (in) tm F (out) Imp. Liquid Collected
1 490.225 0.50 1.60 115.0 69.0 Wt. (Final) Wt. (Initial) lc
2 498.050 0.61 2.00 113.0 70.0 566.5 489.8 76.7
3 508.805 0.68 2.20 115.0 72.0 708.3 651.2 57.1
4 515.995 0.44 1.40 115.0 69.0 826.8 763.8 63.0
5 523.450 0.53 1.70 115.0 70.0 963.1 923.7 39.4
6 531.352 0.54 1.70 113.0 71.0 0.0
7 539.756 0.56 1.80 115.0 71.0
8 548.240 0.68 2.20 114.0 72.0 Isokinetics 102.1
9 557.470 0.68 2.20 113.0 74.0 Test Date 4/9/2024
10 566.800 0.51 1.60 115.0 74.0 Start Time
11 575.125 0.64 2.10 115.0 75.0 End Time
12 584.250 0.67 2.20 113.0 75.0 Run 3
13 593.657
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