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HomeMy WebLinkAboutDRC-2011-007636 - 0901a0688029173bn fl [njjjH^k Denison Mines (USA) Corp. 1050 17th Street, Suite 950 Denver, CO 80265 USA INES '^^^ '• 628-7798 Fax:303 389-4125 www.deniisonmfnes.com Sent VIA Federal Express November 28, 2011 Mr. Rusty Lundberg Co-Executive Secretary Utah Water Quality Board Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144820 Salt Lake City, UT 84114-4820 Re: Transmittal of 3rd Quarter 2011 Routine Chloroform Monitoring Report UDEQ Docket No. UGQ-20-01- White Mesa Uranium Mill Dear Mr, Lundberg: Enclosed are two copies of the White Mesa Uranium Mill Chloroform Monitoring Report for the 3rd Quarter of 2011 as required by the Notice of Violation and Groundwater Corrective Action Order, UDEQ Docket No. UGQ-20-01 as well as two CDs each containing a word searchable _ electronic copy of the report. If you should have any questions regarding this report please contact me. D^sjDN IVIiNES (USA) CORP. Jo Ann Tischler Director, Compliance and Permitting CC: Ron F. Hochstein David C. Frydenlund Harold R. Roberts David E.Turk Kathy Weinel Central Files OENISOJ)~~ MINES Sent VIA Federal Express November 28,2011 Mr. Rusty Lundberg Co-Executive Secretary Utah Water Quality Board Utah Department of Environmental Quality 195 North 1950 West P.O. Box 144820 Salt Lake City, UT 84114-4820 Denison Mines (USA) Corp. 1050 17th Street, Suite 950 . Denver, CO 80265 USA Tel: 303628-7798 Fax: 303389-4125 www.denisonmines.com Re: Transmittal of 3rd Quarter 2011 Routine Chloroform Monitoring Report UDEQ Docket No. UGQ-20-01-White Mesa Uranium Mill Dear Mr. Lundberg: Enclosed are two copies of the White Mesa Uranium Mill Chloroform Monitoring Report for the 3rd Quarter of 2011 as required by the Notice of Violation and Groundwater Corrective Action Order, UDEQ Docket No. UGQ-20-01 as well as two CDs each containing a word searchable electronic copy of the report. If you should have any questions regarding this report please contact me. ( D S\ NINES (USA) CORP. ~V'--'" Jo Ann Tischler Director, Compliance and Permitting CC: Ron F. Hochstein David C. Frydenlund Harold R. Roberts David E. Turk Kathy Weinel Central Files White Mesa Uranium Mill Chloroform Monitoring Report State of Utah Notice of Violation and Groundwater Corrective Action Order UDEQ Docket No. UGQ-20-01 3rd Quarter (July through September) 2011 Prepared by: Denison Mines (USA) Corp. 1050 17th Street, Suite 950 Denver CO 80265 November 28, 2011 TABLE OF CONTENTS 1.0 INTRODUCTION ................................................................................................. 1 2.0 CHLOROFORM MONITORING ...................................................................... 1 2.1 Samples and Measurements Taken During the Quarter ..................................... 1 2.1.1 Chloroform Monitoring .............................................................................. 1 2.1.2 Parameters Analyzed .................................................................................. 2 2.1.3 Groundwater Head Monitoring ................................................................... 2 2.2 Sampling Methodology and Equipment and Decontamination Procedures ....... 3 2.2.1 Well Purging and Depth to Groundwater ................................................... 3 2.2.2 Sample Collection ....................................................................................... 4 2.3 Field Data ............................................................................................................ 5 2.4 Depth to Groundwater Data and Water Table Contour Map .............................. 5 2.5 Laboratory Results .............................................................................................. 5 2.5.1 Copy of Laboratory Results ........................................................................ 5 2.5.2 Regulatory Framework ............................................................................... 5 3.0 QUALITY ASSURANCE AND DATA VALIDATION ................................... 5 3.1 Field QC Samples ............................................................................................... 6 3.2 Adherence to Mill Sampling SOPs ..................................................................... 6 3.3 Analyte Completeness Review ........................................................................... 7 3.4 Data Validation ................................................................................................... 7 3.4.1 Field Data QAlQC Evaluation .................................................................... 7 3.4.2 Holding Time Evaluation ............................................................................ 8 3.4.3 Receipt Temperature Evaluation ................................................................. 8 3.4.4 Analytical Method Checklist ...................................................................... 9 3.4.5 Reporting Limit Evaluation ........................................................................ 9 3.4.6 Trip Blank Evaluation ................................................................................. 9 3.4.7 QAlQC Evaluation for Sample Duplicates ................................................. 9 3.4.8 Rinsate Sample Check ................................................................................ 9 3.4.9 Other Laboratory QAlQC ......................................................................... 11 4.0 INTERPRETATION OF DATA ....................................................................... 12 4.1 Interpretation of Groundwater Levels, Gradients and Flow Directions ........... 12 4.1.1 Current Site Groundwater Contour Map ................................................... 12 4.1.2 Comparison of Current Groundwater Contour Maps to Groundwater Contour Maps for Previous Quarter......................................................... 13 4.1.3 Hydrograpbs .............................................................................................. 14 4.1.4 Depth to Groundwater Measured and Groundwater Elevation ................. 14 4.1.5 Evaluation of the Effectiveness of Hydraulic Capture ............................ 14 4.2 Review of Analytical Results ............................................................................ 15 4.2.1 Current Chloroform Isoconcentration Map .............................................. 15 4.2.2 Chloroform Concentration Trend Data and Graphs .................................. 15 4.2.3 Interpretation of Analytical Data .............................................................. 15 5.0 LONG TERM PUMP TEST AT MW-4, MW-26, TW4-19, TW4-20, AND TW 4-4 OPERATIONS REPORT ..................................................................... 17 5.1 Introduction ....................................................................................................... 17 5.2 Pump Test Data Collection ............................................................................... 17 5.3 Water Level Measurements .............................................................................. 18 1 N:IRequircd RcportslChloroform Quarterly Monitoring Reportl2011 Q312011_Q3Chloroform_Rcporucxl.doc 5.4 Pumping Rates and Volumes ............................................................................ 18 5.4.1 MW-4 ........................................................................................................ 18 5.4.2 TW4-19 ..................................................................................................... 18 5.4.3 MW-26 ...................................................................................................... 19 5.4.4 TW4-20 ..................................................................................................... 19 5.4.5 TW4-4 ....................................................................................................... 19 5.5 Mass Removed .................................................................................................. 19 5.6 Inspections ........................................................................................................ 19 5.7 Conditions That May Affect Water Levels in Piezometers .............................. 20 6.0 CORRECTIVE ACTION REPORT ................................................................. 20 6.1 Rinsate Blank Sample Chloroform Levels ............................................................. 20 6.2 Assessment of Previous Quarter's Corrective Actions .......................................... 21 7.0 CONCLUSIONS AND RECOMMENDATIONS ............................................ 21 8.0 ELECTRONIC DATA FILES AND FORMAT .............................................. 23 9.0 SIGNATURE AND CERTIFICATION ........................................................... 24 LIST OF TABLES Table 1 Summary of Well Sampling for the Period Table 2 Mass of Chloroform Removed Per Well Per Quarter ii N:IRequired ReportslChloroform Quarterly Monitoring RepOltl2011 Q312011_Q3Chloroform_ReporuexLdoc INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Order of Sampling and Field Data Worksheets Tab C Weekly and Monthly Depth to Water Data Tab D Kriged Current Quarter Groundwater Contour Map, Capture Zone Map, Capture Zone Details Map, and Depth to Water Data Table Tab E Kriged Previous Quarter Groundwater Contour Map Tab F Hydrographs of Groundwater Elevations Over Time for Chloroform Monitoring Wells Tab G Depths to Groundwater and Elevations Over Time for Monitoring Wells Tab H Laboratory Analytical Reports Tab I Quality Assurance and Data Validation Tables 1-1 Field Data QAJQC Evaluation 1-2 Holding Time Evaluation 1-3 Receipt Temperature Check 1-4 Analytical Method Check 1-5 Reporting Limit Evaluation 1-6 Trip Blank Evaluation 1-7 QAJQC Evaluation for Sample Duplicates 1-8 QC Control Limits for Analyses and Blanks 1-9 Rinsate Evaluation Tab J Kriged Current Quarter Chloroform Isoconcentration Map Tab K Analyte Concentration Data Over Time Tab L Chloroform Concentration Trend Graphs Tab M CSV Transmittal Letter Tab N Disinfection byproducts -Trihalomethanes 111 N:IRcquired ReponslChloroform Quarterly Monitoring Reponl2011 Q312011_Q3ChlorofornU~ep()rucxl.doc 1.0 INTRODUCTION The presence of chloroform was initially identified in groundwater at the White Mesa Mill (the "Mill") as a result of split sampling performed in May 1999. The discovery resulted in the issuance of State of Utah Notice of Violation ("NOV") and Groundwater Corrective Action Order ("CAO") State of Utah Department of Environmental Quality ("UDEQ") Docket No. UGQ-20-01, which required that Denison Mines (USA) Corp. ("DUSA") submit a Contamination Investigation Plan and Report pursuant to the provisions ofUAC R317-6-6.15(D). The frequency of chloroform sampling, which was initially performed on a monthly basis, was modified on November 8, 2003. Since that time all chloroform contaminant investigation wells have been sampled on a quarterly basis. This is the Quarterly Chloroform Monitoring Report for the third quarter of 2011 as required under the NOV and CAO. This Report also includes the Operations Report for the Long Term Pump Test at MW-4, TW4-19, MW-26 (previously referred to as TW4- 15), TW4-20, and TW4-4 for the quarter. 2.0 CHLOROFORM MONITORING 2.1 Samples and Measurements Taken During the Quarter A map showing the location of all groundwater monitoring wells, piezometers, existing wells, temporary chloroform contaminant investigation wells and temporary nitrate investigation wells is attached under Tab A. Chloroform samples and measurements taken during this reporting period (July through September), are discussed in the remainder of this section. 2.1.1 Chloroform Monitoring Quarterly sampling for chloroform monitoring parameters is currently required in the following wells: TW4-1 TW4-2 TW4-3 TW4-4 TW4-5 TW4-6 TW4-7 TW4-8 TW4-9 TW4-10 TW4-11 TW4-12 TW4-13 TW4-14 TW4-16 TW4-18 TW4-19 TW4-20 1 N:IRcquired RcportslChloroform Quarterly Monitoring Reportl2011 Q312011_Q3ChlorofornU~cporuext.doc TW4-21 TW4-22 TW4-23 TW4-24 TW4-25 MW-4 MW-26 (formerly TW4-15) MW-32 (formerly TW4-17) TW4-26 Table 1 provides an overview of all wells sampled during the cunent period, along with the date samples were collected from each well, and the date(s) which analytical data were received from the contract laboratory. Table 1 also identifies equipment rinsate samples collected, as well as sample numbers associated with the deionized field blank (DIFB) and any required duplicates. As indicated in Table 1, chloroform monitoring was performed in all of the required chloroform monitoring wells. 2.1.2 Parameters Analyzed Wells sampled during this reporting period were analyzed for the following constituents: • Chloroform • Chloromethane • Carbon tetrachloride • Methylene chloride • Chloride • Nitrate plus Nitrite as Nitrogen Use of analytical methods is consistent with the requirements of the Chloroform Investigation Monitoring Quality Assurance Program (the "Chloroform QAP") attached as Appendix A to the White Mesa Uranium Mill Groundwater Monitoring Quality Assurance Plan ("QAP"). 2.1.3 Groundwater Head Monitoring Depth to groundwater was measured in the following wells and/or piezometers, pursuant to Part 1.E.3 of the Groundwater Discharge Permit (the "GWDP"): • The quarterly groundwater compliance monitoring wells. • Existing monitoring well MW -4 and all of the temporary chloroform investigation wells. • Piezometers -P-l, P-2, P-3, P-4 and P-5. • MW-20 and MW-22. • Nitrate monitoring wells. • In addition to the above, depth to water measurements are routinely observed in conjunction with sampling events for all wells sampled during quarterly and accelerated efforts, regardless of the sampling purpose. In addition, weekly and m0nthly depth to groundwater measurements were taken in MW- 4, MW-26, TW4-19, TW4-20, and TW4-4, as part of the long term pumping test for MW-4. 2 N:IRcquircd RcportslChloro[orm Quarterly Monitoring Rcportl2011 Q312011_Q3Chloro[ornU~cporucxl.doc 2.2 Sampling Methodology and Equipment and Decontamination Procedures DUSA completed, and transmitted to UDEQ on May 25, 2006, a revised QAP for sampling under the Mill's GWDP. While the water sampling conducted for chloroform investigation purposes has conformed to the general principles set out in the QAP, some of the requirements in the QAP were not fully implemented prior to UDEQ's approval, for reasons set out in correspondence to UDEQ dated December 8, 2006. Subsequent to the delivery of the December 8, 2006 letter, DUSA discussed the issues brought forward in the letter with UDEQ and has received correspondence from UDEQ about those issues. In response to UDEQ's letter and subsequent discussions with UDEQ, DUSA has incorporated changes in chloroform Quality Assurance ("QA") procedures in the form of the Chloroform QAP, which is a separate Appendix A to the QAP. The Chloroform QAP describes the differing needs of the chloroform investigation program, and is an attachment to the GWDP QAP where QA requirements for the chloroform investigation are addressed. On June 20, 2009 the Chloroform QAP was modified to require that the quarterly chloroform reports include additional items specific to DUSA's ongoing pump testing and chloroform capture efforts. The sampling methodology, equipment and decontamination procedures that were performed for the chloroform contaminant investigation, as summarized below, are consistent with the QAP and the Chloroform QAP. 2.2.1 Well Purging and Depth to Groundwater A list of the wells in order of increasing chloroform contamination is generated quarterly. The order for purging is thus established. The list is included with the Field Data Worksheets under Tab B. Mill personnel stmt purging with all of the non-detect wells and then move to the more contaminated wells in order of chloroform contamination. Before leaving the Mill office, the portable pump and hose are rinsed with DI water. A rinsate blank sample is collected at the beginning of each day prior to the first use of the pump. Mill personnel then proceed to the first well which is the well with the lowest concentration of chloroform based on the previous quarter's sampling results. Well depth measurements are taken and the two casing volumes are calculated for those wells which do not have a dedicated pump (measurements are made using the same instrument used for the monitoring wells under the Mill's GWDP). If the well has a dedicated pump, it is pumped on a set schedule per the remediation plan and is considered sufficiently evacuated to immediately collect a sample; however, if a pumping well has been out of service for 48 hours or more, DUSA will follow the purging requirements outlined in Section 6.2.7(d)(v) of the QAP. The dedicated pump is used to collect parameters and to collect the samples as described below. If the well does not have a dedicated pump, a Grundfos pump (9 -10 gpm pump) is then lowered to the screened interval in the well and purging is started. The purge rate is established for the well by using a calibrated 5 gallon bucket. The purging of the well is completed per Section 6.2.5 of the QAP. In wells where the portable pump is used, a disposable bailer is used to collect the samples the day following purging activities. After each use, the portable pump is decontaminated prior to reuse at the next sample location. This purging process is 3 N:IRequired ReportslChlorofol'ln Quarterly Monitoring Reportl20 II Q3120 ll_Q3Chloroform_Reporuext.doc repeated at each well location moving from least contaminated to the most contaminated well. All wells are capped and secured prior to leaving the sampling location. Wells with dedicated pumps are sampled when the pump is in the pumping mode. If the pump is not pumping at the time of sampling, it is manually switched on by the Mill Personnel. The well is pumped for approximately 5 to 10 minutes prior to the collection of the field parameters. Per the approved QAP, one set of parameters is collected. Samples are collected following the measurement of one set of field parameters. The pump is turned off and allowed to resume its timed schedule. 2.2.2 Sample Collection Samples are collected as described above. In all cases, on days when samples will be collected, a cooler with ice is prepared. The trip blank is also gathered at that time (the trip blank for these events is provided by the Analytical Laboratory). Once Mill Personnel arrive at the well sites, labels are filled out for the various samples to be collected. All personnel involved with the collection of water and samples are then outfitted with rubber gloves. Chloroform investigation samples are collected by means of disposable bailers. Mill personnel use a disposable bailer to sample each well that does not have a dedicated pump. The bailer is attached to a reel of approximately 150 feet of nylon rope and then lowered into the well. After coming into contact with the water, the bailer is allowed to sink into the water in order to fill. Once full, the bailer is reeled up out of the well and the sample bottles are filled as follows: • Volatile Organic Compound ("VOC") samples are collected first. This sample consists of three 40 ml vials provided by the Analytical Laboratory. The VOC sample is not filtered and is preserved with HCI; • A sample for nitrate/nitrite is then collected. This sample consists of one 250 ml. bottle which is provided by the Analytical Laboratory. The nitrate/nitrite sample is also not filtered and is preserved with H2S04; • A sample for chloride is then collected. This sample consists of one 500 ml. bottle which is provided by the Analytical Laboratory. The chloride sample is also not filtered and is not chemically preserved. After the samples have been collected for a particular well, the bailer is disposed of and the samples are placed into the cooler that contains ice. The well is then recapped and Mill personnel proceed to the next well. 4 N:IRequired ReportslChloroform Quarterly Monitoring Reportl20 II Q3120 I I_Q3Chloroform_Reporu exLdoc 2.3 Field Data Attached under Tab B are copies of all Field Data Worksheets that were completed during the quarter for the chloroform contaminant investigation monitoring wells identified in paragraph 2.1.1 above, and Table 1. 2.4 Depth to Groundwater Data and Water Table Contour Map Attached under Tab C are copies of the Depth to Water Sheets for the weekly monitoring of MW-4, MW-26, TW4-19, TW4-20, and TW4-4, as well as the monthly depth to groundwater data for chloroform contaminant investigation wells measured during the quarter that are not included in Tab D. Depth to groundwater measurements which were utilized for groundwater contours are included on the Quarterly Depth to Water Worksheet at Tab D of this report, along with the kriged groundwater contour map for the current quarter generated from this data. A copy of the kriged groundwater contour map generated from the second quarter 2011 data is provided under Tab E. 2.5 Laboratory Results 2.5.1 Copy of Laboratory Results All analytical results were provided by Energy Laboratories ("EL"). Table 1 lists the dates when analytical results were reported to the QA Manager for each well or other sample. Results from analysis of samples collected for the third quarter chloroform contaminant investigation are provided under Tab H of this Report. Also included under Tab Hare the results of analyses for duplicate samples, the DIFB, and rinsate samples for this sampling effort, as identified in Table 1, as well as results for trip blank analyses required by the Chloroform QAP. 2.5.2 Regulatory Framework As discussed in Section 1.0, above, the NOV and requirements of the CAO triggered a series of actions on DUSA's part. In addition to the monitoring program, DUSA has equipped five wells with pumps to recover impacted groundwater, and has initiated recovery of chloroform from the perched zone. Sections 4 and 5, below, interpret the groundwater level and flow information, contaminant analytical results, and pump test data to assess effectiveness of DUSA's chloroform capture program. 3.0 QUALITY ASSURANCE AND DATA VALIDATION The QA Manager performed a QAlQuality Control ("QC") review to confirm compliance of the monitoring program with requirements of the QAP. As required in the QAP, data QA includes preparation and analysis of QC samples in the field, review of field procedures, an analyte completeness review, and QC review of laboratory methods and 5 N:IRequircd RcportslChloroform Quarterly Monitoring Rcportl2011 Q312011_Q3Chloroform_Rcpol'u ext.doc data. Identification of field QC samples collected and analyzed is provided in Section 3.1. Discussion of adherence to Mill sampling Standard Operating Procedures ("SOPs") is provided in Section 3.2. Analytical completeness review results are provided in Section 3.3. The steps and tests applied to check laboratory data QNQC are discussed in Sections 3.4.4 through 3.4.9 below. The analytical laboratory has provided summary reports of the analytical quality QNQC measurements necessary to maintain conformance with National Environmental Laboratory Accreditation Conference ("NELAC") certification and reporting protocol. The Analytical Laboratory QNQC Summary Reports, including copies of the Mill's Chain of Custody and Analytical Request Record forms for each set of Analytical Results, follow the analytical results under Tab H. Results of review of the laboratory QNQC information are provided under Tab I and are discussed in Section 3.4, below. 3.1 Field QC Samples The following QC samples were generated by Mill personnel and submitted to the analytical laboratory in order to assess the quality of data resulting from the field sampling program. Field QC samples for the chloroform investigation program consist of one field duplicate sample for each 20 samples, a trip blank for each shipped cooler which contains VOCs, one DIFB and rinsate samples. During this quarter, two duplicate samples were collected as indicated in Table 1. The duplicates were sent blind to the analytical laboratory and analyzed for the same parameters as the chloroform wells. One trip blank was provided by Energy Laboratories and returned with the quarterly chloroform monitoring samples. Three rinsate blank samples were collected as indicated on Table 1. Rinsate samples were labeled with the name of the subsequently purged well with a terminal letter "R" added (e.g. TW 4-7R). The results of these analyses are included with the routine analyses under Tab H. In addition, one DIFB, while not required by the Chloroform QAP, were collected and analyzed for the same constituents as the well samples and rinsate blank samples. 3.2 Adherence to Mill Sampling SOPs On a review of adherence by Mill personnel to the existing sampling SOPs, the QA Manager observed that QNQC requirements established in the QAP and Chloroform QAP were being adhered to and that the SOPs were implemented, except as described below. 6 N:IRequired ReponslChloroform Quarterly Monitoring Reportl2011 Q312011_Q3Chloroform_RcporUexl.doc One site procedure requiring clarification was noted during the QA Manager's review of the field data. As previously stated, a list of the wells in order of increasing chloroform contamination (based on the previous quarter's data) is generated quarterly prior to the next quarter's sampling to determine the order for purging prior to sampling. Consistent with the approved QAP, each quarterly event begins with purging of the wells from the least affected to the most affected based on the previous quarter's data. Although purging follows this order, the sampling order may deviate slightly from the generated list. This practice does not affect the samples for these reasons: any wells sampled in slightly different order had either dedicated pumps or were sampled via a disposable bailer. This practice does not affect the quality or usability of the data as there is no cross- contamination resulting from sampling order. DUSA intends to propose an amendment to clarify this practice in the next revision of the QAP. 3.3 Analyte Completeness Review All analyses required by the GWDP for chloroform monitoring for the period were performed. 3.4 Data Validation The QAP and GWDP identify the data validation steps and data QC checks required for the chloroform monitoring program. Consistent with these requirements, the QA Manager performed the following evaluations: a field data QNQC evaluation, a holding time check, a receipt temperature check, an analytical method check, a reporting limit evaluation, a trip blank check, a QNQC evaluation of sample duplicates, a QC Control Limit check for analyses and blanks including the DIFB and a rinsate sample check. Each evaluation is discussed in the following sections. Data check tables indicating the results of each test are provided under Tab 1. 3.4.1 Field Data QA/QC Evaluation The QA Manager performs a review of all field recorded parameters to assess their adherence with QAP requirements. The assessment involved review of two sources of information: the Field Data Sheets and the Quarterly Depth to Water summary sheet. Review of the Field Data Sheets addresses well purging volumes and stability of five parameters: conductance, pH, temperature, redox potential, and turbidity. Review of the Depth to Water data confirms that all depth measurements used for development of groundwater contour maps were conducted within a five-day period as indicated by the measurement dates in the summary sheet under Tab D. The results of this quarter's review of field data are provided under Tab I. Based upon this review, all non-pumping wells conformed to the QAP requirement to evacuate two well casing volumes before sampling except TW4-2, TW4-3, TW4-6, TW4-7, TW4-10, TW4-11, TW4-13, TW4-14, and TW4-26. All of these wells were pumped to dryness before two casing volumes were evacuated and as such the requirement to purge two casing volumes does not apply. In each case, representative samples of formation water were collected after the wells were allowed to recover. 7 N:IRequircd RcpOrlslChloroform Quarlerly Monitoring Repootl2011 Q312011_Q3Chloroform_Rcporuexl.doc During review of the field data sheets, it was observed that sampling personnel consistently recorded depth to water to the nearest 0.01 foot. All field parameters for all wells were within the required Relative Percent Difference ("RPD") (other than the wells that were pumped to dryness and the wells which are continually pumped, for which this requirement does not apply), except as follows. The review of the field sheets for compliance with QAP requirements resulted in the observations noted below. The requirements in Section 6.2.7 of the QAP specifically state that field parameters must have stabilized to within 10% over at last 2 consecutive measurements. During the third quarter 2011 sampling event, all field parameters were stabilized within 10%. The QAP states that turbidity should be less than 5 Nephelometric Turbidity Units ("NTU") prior to sampling unless the well is characterized by water that has a higher turbidity. Sixteen turbidity measurements exceeded the QAP's 5 NTU goal. Of the sixteen wells, seven wells were pumped to dryness. The QAP does not require that turbidity measurements be less than 5 NTU prior to sampling. As such, the noted observations regarding turbidity measurements less than 5 NTU below are included for information purposes only. DUSA's letter to DRC of March 26, 2010 discusses further why turbidity does not appear to be an appropriate parameter for assessing well stabilization. In response to DRC's subsequent correspondence dated June 1, 2010 and June 24, 2010, DUSA has completed a monitoring well redevelopment program. The redevelopment report was submitted to DRC on September 30, 2011. Redevelopment results will be discussed with DRC in an effort to come to a consensus regarding turbidity considerations for the chloroform wells at the Mill site. 3.4.2 Holding Time Evaluation QAP Table 1 identifies the method holding times for each suite of parameters. Sample holding time checks are provided in Tab I. All samples were received and analyzed within the required holding time. 3.4.3 Receipt Temperature Evaluation Chain of Custody sheets were reviewed to confirm compliance with the QAP requirement which specifies that samples be received at 6°C or lower. Sample temperatures checks are provided in Tab I. All samples were received within the required temperature limit. 8 N:IRequired ReponslChlorofOlw Quarterly Monitoring Reponl2011 Q312011_Q3Chlorofoml_Reporuext.doc 3.4.4 Analytical Method Checklist All analytical methods reported by the laboratory were checked against the required methods enumerated in the Chloroform QAP. Analytical method checks are provided in Tab 1. All methods were consistent with the requirements of the Chloroform QAP. 3.4.5 Reporting Limit Evaluation All analytical method reporting limits reported by the laboratory were checked against the reporting limits enumerated in the Chloroform QAP. Reporting Limit Checks are provided under Tab 1. All analytes were measured and reported to the required reporting limits, except 21 sets of sample results had the reporting limit raised for at least one analyte due to matrix interference and/or sample dilution. In all cases the reported value for the analyte was higher than the increased detection limit. 3.4.6 Trip Blank Evaluation All trip blank results were reviewed to identify any VOC contamination resulting from transport of the samples. Trip blank checks are provided in Tab 1. All trip blank results were less than the reporting limit for all VOC analytes. 3.4.7 QAlQC Evaluation for Sample Duplicates Section 9.1.4 a) of the QAP states that RPDs will be calculated for the comparison of duplicate and original field samples. The QAP acceptance limits for RPDs between the duplicate and original field sample is less than or equal to 20% unless the measured results (described as activities in the QAP) are less than 5 times the required detection limit. This standard is based on the EPA Contract Laboratory Program National Functional Guidelines for Inorganic Data Review, February 1994, 9240.1-05-01 as cited in the QAP. The RPDs are calculated for all duplicate pairs for all analytes regardless of whether or not the reported concentrations are greater than 5 times the required detection limits; however, data will be considered noncompliant only when the results are greater than 5 times the reported detection limit and the RPD is greater than 20%. The additional duplicate information is provided for information purposes. All analytical results for the sample/duplicate pairs were within the 20% RPD acceptance limits. Results of the RPD test are provided in Tab 1. 3.4.8 Rinsate Sample Check Rinsate blank sample checks are provided in Tab 1. Chloroform A review of the analytical results reported for rinsate blank samples indicated that one of the rinsate blank samples contained chloroform. A DIFB was analyzed and was repOlted as nondetect. A comparison of the rinsate blank sample concentration levels to the QAP requirements -that rinsate sample concentrations be one order of magnitude lower than 9 N:IRequired RcpOrlslChloroform Quarlerly Monitoring Rcportl2011 Q312011_Q3Chloro[orm_Rcporuexl.doc that of the actual well -indicated that the rinsate blank sample with a detection of chloroform met this criterion. This criterion however, is irrelevant and inappropriate for the rinsate blank sample data collected during the chloroform sampling because rinsate blank samples are collected from the decontaminated portable pump used for well purging, and the pump is not used for sample collection. As stated in Section 2.2.1, wells that do not have a dedicated pump are purged using a portable pump. In wells where the portable pump is used for purging, a disposable bailer is used to collect the samples the day following purging activities. Chloroform has been present in the rinsate blanks in previous quarters. Based on the investigation into the source of chloroform, DUSA believes that the potential source for the chloroform present in the rinsate blanks has been identified. It is known from EPA studies that chloroform is frequently a byproduct of the chlorination process in potable water supplies. Based on the EPA documentation, DUSA believes the chloroform contamination in the DI water is most likely the result of chlorination of the intake water used for the DI system. Multiple sources cite the creation of chloroform as a byproduct of chlorination. The following two sources have been attached, EPA -Basic Information about Disinfection Byproducts in Drinking Water: Total Trihalomethanes, Haloacetic Acids, Bromate and Chlorite; and Water Research Net -Disinfection By-Products Trihalomethanes, in Tab N to this report. The chloroform is most likely the result of the chlorination of the potable water at the Mill which is subsequently fed to the DI system. The water is free of chloroform prior to chlorination, as it is tested by the Utah Department of Health, Division of Epidemiology and Laboratory Services on a routine basis. The chlorine added reacts with the naturally occurring organic and inorganic materials in the water. As discussed in the Second Quarter 2011 Chloroform report submitted on September 1, 2011, the low level chloroform contamination in the rinsate blank is due to the addition of a second 55-gallon rinse with DI water added to the rinsate process to minimize nitrate contamination in the nitrate and chloroform sampling programs. The addition of this step eliminated nitrate contamination, but "stressed" the DI system due to increase in volume of water required for the second rinse. The DI system is designed to remove the chloroform. However, due to the stress on the system resulting from the large volume of DI water processed through the system during the chloroform sampling events to accommodate a second rinse, breakthrough appears to occur towards the end of the sampling event. The one rinsate sample with chloroform contamination from the third quarter 2011 was the last rinsate sample taken for this sampling event. This sample was collected from water produced at the end of a DI filter run when the system was "stressed", which caused the low level detection in the rinsate blank. Removal of chloroform and other organics is accomplished by the "activated carbon" portion of the DI system. The performance of this portion of the Dr system is directly proportional to the volume of water treated and, due to the large volumes of water treated in a short time, the system becomes "stressed" and performance decreases resulting in chloroform "breakthrou gh". 10 N:IRequu'cd ReportslChloroform Quarterly Monitoring Reportl2011 Q312011_Q3Chloroform_Rcporucxl.doc Corrective actions for this issue are described in Section 6.1. 3.4.9 Other Laboratory QAlQC Section 9.2 of the QAP requires that the laboratory's QAJQC Manager check the following items in developing data reports: (1) sample preparation information is correct and complete, (2) analysis information is correct and complete, (3) appropriate analytical laboratory procedures are followed, (4) analytical results are correct and complete, (5) QC samples are within established control limits, (6) blanks are within QC limits, (7) special sample preparation and analytical requirements have been met, and (8) documentation is complete. In addition to other laboratory checks described above, DUSA's QA Manager rechecks QC samples and blanks (items (5) and (6)) to confirm that the percent recovery for spikes and the relative percent difference for spike duplicates are within the method-specified acceptance limits, or that the case narrative sufficiently explains any deviation from these limits. Results of this quantitative check are provided in Tab I. All lab QAJQC results met these specified acceptance limits except as noted below. The QAP Section 8.1.2 requires that an MSIMSD (referred to as Duplicate Spike [Matrix spike] in the QAP) pair be analyzed with each analytical batch. The QAP does not specify acceptance limits for the MSIMSD pair, and the QAP does not specify that the MS/MSD pair be prepared on DUSA samples only. Acceptance limits for MSIMSDs are set by the laboratories. The review of the information provided by the laboratories in the data packages verified that the QAP requirement to analyze an MS/MSD pair with each analytical batch was met. While the QAP does not require it, the recoveries were reviewed for compliance with the laboratory established acceptance limits. The QAP does not require this level of review, and the results of this review are provided for information only. The information from the Laboratory QAJQC Summary Reports indicates that the MSIMSDs recoveries and the associated RPDs for all quarterly chloroform samples are within acceptable laboratory limits for all regulated compounds except as indicated in Tab I. The recoveries, which are outside of the laboratory established acceptance limits, do not affect the quality or usability of the data because the recoveries outside of the acceptance limits are indicative of matrix interference. Furthermore, the nitrate sample with MSIMSD recoveries outside of the laboratory established limit is not a Denison sample and as such are not applicable to the Mill samples. The QAP requirement to analyze a MSIMSD pair with each analytical batch was met and as such the data are compliant with the QAP. The QAP specifies that surrogate compounds shall be employed for all organic analyses, but the QAP does not specify acceptance limits for surrogate recoveries. The analytical data associated with the routine quarterly sampling met the requirement specified in the QAP. The information from the Laboratory QAJQC Summary Reports indicates that the surrogate recoveries for all quarterly chloroform samples were within acceptable 11 N:IRequired RcportslChloroform Quarterly Monitoring Repoltl2011 Q31201l_Q3Chloroform_Reporuext.doc laboratory limits for all surrogate compounds except as indicated in Tab I. Seventeen surrogate recoveries were above the laboratory established acceptance limits or had a high recovery, indicating a high bias to the individual sample results. A high bias means that reported results will be higher than the actual results. There is no effect on the quality or usability of the data because there are multiple surrogates added to each sample and all other surrogates were within limits. Furthermore, there are no QAP requirements for surrogate recoveries. The information from the Laboratory QAlQC Summary Reports indicates that all LCS recoveries were within acceptable laboratory limits for all LCS compounds. 4.0 INTERPRETATION OF DATA 4.1 Interpretation of Groundwater Levels, Gradients and Flow Directions. 4.1.1 Current Site Groundwater Contour Map As stated above, a listing of groundwater level readings for the current quarter (shown as depth to groundwater in feet) is included under Tab D. The data from this tab has been interpreted (kriged) and plotted in a water table contour map, provided under the same tab. Also included under Tab D is a groundwater contour map of the Mill site and a more detailed map of a portion of the Mill site where the chloroform pumping wells are located, in each case with hand-drawn stream tubes, depicting hydraulic capture from the pumping. The water level contour maps indicate that perched water flow at the site ranges from generally southwesterly in the western portion of the site to generally southerly in the eastern portion of the site. Perched water mounding associated with the wildlife ponds locally changes the flow patterns. For example, northeast of the Mill site, mounding associated with wildlife ponds results in locally northerly flow near MW-19. Flow directions are also locally influenced by pumping at MW-4, MW-26, TW4-4, TW4-19, and TW4-20. Significant cones of depression have formed in the vicinity of all pumping wells except TW4-4, which began pumping in the first quarter of 2010. Although pumping at TW4-4 has depressed the water table in the vicinity of TW4-4, the well has apparently not been pumped long enough to have affected water levels at adjacent wells sufficiently for a well-defined cone of depression to be evident. Changes in water levels at wells immediately south of TW4-4 resulting from TW4-4 pumping are likely muted because TW4-4 is located at a transition from relatively high to relatively low permeability conditions south (downgradient) of TW4-4. The permeability of the perched zone at TW4-6 and TW4-26 is approximately two orders of magnitude lower than at TW4-4. Any draw down of water levels at wells immediately south of TW4-4 resulting from TW4-4 pumping is also difficult to determine because of a general, long- term increase in water levels in this area. Water levels at TW 4-4 and TW 4-6 increased by nearly 2.7 and 2.9 feet, respectively, between the fourth quarter of 2007 and the fourth quarter of 2009 (just prior to TW4-4 pumping) at rates of approximately 1.2 feet/year and 12 N:IRcquired RcportslChloroform Quarterly Monitoring Rcportl2011 Q312011_Q3Chlorofonn_Rcporu cxl.doc 1.3 feet/year, respectively. However, the increase in water level at TW4-6 has been reduced since the start of pumping at TW4-4 (first quarter of 2010) to approximately 0.3 feet/year suggesting that TW 4-6 is within the hydraulic influence of TW 4-4. The lack of a well-defined cone of depression at TW4-4 is also influenced by the persistent, apparently anomalously low water level at non-pumping well TW4-14, located east of TW4-4 and TW4-6. For the current quarter, the water level at TW4-14 is approximately 13 feet lower than the water level at TW4-6 and approximately 15 feet lower than TW 4-4 even though TW 4-4 is pumping. The low water level at TW 4-14 is considered anomalous because it appears to be downgradient of all three wells TW 4-4, TW4-6, and TW4-26, yet there is no chloroform at TW4-14. Chloroform has apparently migrated from TW4-4 to TW4-6 and from TW4-6 to TW4-26 which suggests that TW4- 26 is actually downgradient of TW 4-6, and TW 4-6 is actually downgradient of TW 4-4, regardless of the flow direction implied by the low water level at TW4-14. The water level at TW4-26 (5537.6 feet amsl) is, however, lower than water levels at adjacent wells TW4-6 (5538.3 feet amsl), and TW4-23 (5541.9 feet amsl) 4.1.2 Comparison of Current Groundwater Contour Maps to Groundwater Contour Maps for Previous Quarter The groundwater contour maps for the Mill site for the second quarter of 2011, as submitted with the Chloroform Monitoring Report for the second quarter of 2011, are attached under Tab E. A comparison of the water table contour maps for the third quarter of 2011 to the water table contour maps for the previous quarter (second quarter of 2011) indicates similar patterns of draw down related to pumping of MW-4, MW-26, TW4-4, TW4-19 and TW4- 20. Water levels and water level contours for the site have not changed significantly since the last quarter, except for a few locations. As discussed in Section 4.1.1, pumping at TW4-4, which began in the first quarter of 2010, has depressed the water table near TW 4-4, but does not yet appear to have affected water levels at adjacent wells sufficiently for a well-defined cone of depression to be evident. Reported increases in water levels of 6 feet occurred in new well MW-37 and of approximately 14 feet occurred in pumping well MW-26. Reported decreases in water levels of approximately 7 feet occurred in well TW4-3, of approximately 6 feet occurred in pumping well MW-4, and of approximately 28 feet occurred in pumping well TW4-20. The water level changes at the remaining pumping wells (TW 4-4 and TW 4-19) were less than 5 feet. Water level fluctuations at pumping wells MW-4, MW-26, TW4-4, TW4-19, and TW4- 20 are due in part to fluctuations in pumping conditions just prior to and at the time the measurements are taken. The largest decrease (increase in draw down) of approximately 28 feet occurred in well TW4-20 and the largest increase (decrease in drawdown), of approximately 14 feet, occurred in well MW-26. The reported water level increase of 6 feet at new well MW-37 during the current quarter is likely due to recovery after development during the previous quarter. The reported decrease in water level of 13 N:IRequircd ReportslChloroform Quarterly Monitoring Reportl2011 Q312011_Q3Chloroform_Reporuexl.doc approximately 7 feet at TW4-3 yields a water level that is similar to historic values suggesting the previous reading (second quarter, 2011 reading) was erroneous. 4.1.3 Hydrographs Attached under Tab Fare hydrographs showing groundwater elevation in each chloroform contaminant investigation monitor well over time. 4.1.4 Depth to Groundwater Measured and Groundwater Elevation Attached under Tab G are tables showing depth to groundwater measured and groundwater elevation over time for each of the wells listed in Section 2.1.1 above. 4.1.5 Evaluation of the Effectiveness of Hydraulic Capture Perched water containing chloroform has been removed from the subsurface by pumping MW-4, MW-26, TW4-4, TW4-19, and TW4-20. The primary purpose of the pumping is to reduce total chloroform mass in the perched zone as rapidly as is practical. Pumping wells upgradient of TW 4-4 were chosen for pumping because 1) they are located in areas of the perched zone having relatively high permeability and saturated thickness, and 2) high concentrations of chloroform were detected at these locations. The relatively high transmissivity of the perched zone in the vicinity of these pumping wells results in the wells having a relatively high productivity. The combination of relatively high productivity and high chloroform concentrations allows a high rate of chloroform mass removal. TW4-4 is located in a down gradient area having relatively high chloroform concentrations but relatively small saturated thickness, and at a transition from relatively high to relatively low permeability conditions downgradient of TW4-4. As with the other pumping wells, pumping TW 4-4 helps to reduce the rate of chloroform migration in downgradient portions of the plume. The impact of pumping is indicated by the water level contour maps attached under Tabs D and E. Cones of depression have developed in the vicinity of MW-4, MW-26, TW4- 19, and TW4-20 which continue to remove significant quantities of chloroform from the perched zone. The water level contour maps indicate that effective capture of water containing high chloroform concentrations in the vicinity of these pumping wells is occurring. Overall, the combined capture of MW-4, MW-26, TW4-19, and TW4-20 has not changed significantly since the last quarter. As noted in Section 4.1.2, decreases in water levels (increases in drawdown) of approximately 6 feet occurred at MW-4 and of approximately 28 feet occurred at TW4-20, and an increase in water level (decrease in drawdown) of approximately 14 feet occurred at MW-26. The increase in drawdown at TW4-20 has increased the apparent capture zone of this well relative to other nearby pumping wells. (The capture zone associated with TW4-20 last quarter was not distinguishable from the larger capture zones of MW -26 and TW 4-19.) As discussed in Section 4.1.1, TW4-4 has apparently not been pumped long enough for a well-defined capture zone to become evident, and the draw down associated with TW 4-4 is likely less apparent due to the low water level at TW4-14. 14 N:IRequircd ReporlslChloroform Quarterly Monitoring RepOltl201 1 Q312011_Q3ChlorofornU~eporuexl.doc Chloroform concentrations exceeding 70 !-lg/L have occurred in the past at some locations downgradient of pumping wells (for example, at TW 4-6, located immediately south of TW4-4), where the lower permeability and relatively small saturated thickness of the perched zone significantly limits the rate at which chloroform mass can be removed by pumping. By removing mass and reducing hydraulic gradients, thereby reducing the rate of down gradient chloroform migration, and allowing natural attenuation to be more effective, pumping at the productive, up gradient locations has a beneficial effect on this downgradient chloroform. Pumping at TW 4-4 was implemented during the first quarter of 2010 to improve capture in this downgradient area to the extent allowable by the lower productivity conditions presumed to exist in this area. The beneficial effect of pumping TW 4-4 is demonstrated by the decrease in chloroform concentrations at TW4-6 from 1000 !-lg/L to 16 !-lg/L, and at TW4-26 from 13 !-lg/L to 2.8 !-lg/L since pumping began at TW4-4. Concentrations at these wells have decreased substantially even though they do not unambiguously appear to be within the hydraulic capture of TW 4-4. As discussed in Section 4.1.1, however, the decrease in the long-term rate of water level rise at TW 4-6 since pumping began at TW 4-4 does suggest that TW 4-6 is within the hydraulic influence of TW4-4. Regardless of whether TW4-6 can be demonstrated to be within hydraulic capture of TW4-4, pumping TW4-4 acts to cut off the source of chloroform to TW4-6 and TW4-26 by the mechanisms discussed above. 4.2 Review of Analytical Results 4.2.1 Current Chloroform Isoconcentration Map Included under Tab J of this Report is a current chloroform isoconcentration map for the Mill site. 4.2.2 Chloroform Concentration Trend Data and Graphs Attached under Tab K is a table summarizing values for all required parameters, chloride, nitrate/nitrite, carbon tetrachloride, chloroform, chloromethane, and methylene chloride, for each well over time. Attached under Tab L are graphs showing chloroform concentration trends in each monitor well over time. 4.2.3 Interpretation of Analytical Data Comparing the analytical results to those of the previous quarter, as summarized in the table included under Tab K, the following observations can be made: Chloroform concentrations have increased by more than 20% in the following wells compared to last quarter: MW-26, TW4-6, TW4-21, TW4-22, and TW4-24; Chloroform concentrations have decreased by more than 20% in the following wells compared to last quarter: TW4-1O, TW4-16, and TW4-19; 15 N:IRequired ReportslChloroform Quarterly Monitoring Reportl2011 Q312011_Q3Chloroform_ReporucxLdoc Chloroform concentrations have remained within 20% in the following wells compared to last quarter: MW-4, TW4-1, TW4-2, TW4-4, TW4-5, TW4-7, TW4-11, TW4-18, TW4-20, and TW4-26; and MW-32, TW4-3, TW4-8, TW4-9, TW4-12, TW4-13, TW4-14, TW4-23, and TW4-25 remained non-detect. As indicated, chloroform concentrations at many of the wells with detected chloroform were within 20% of the values reported for the wells during the previous quarter, suggesting that variations are within the range typical for sampling and analytical error. Wells MW-26, TW4-6, TW4-10, TW4-16, TW4-19, TW4-21, TW4-22, and TW4-24 had changes in concentration greater than 20%. Of the latter, MW-26 and TW4-19 are pumping wells. TW4-6 is located adjacent to pumping well TW4-4; TW4-1O and TW4- 16 are located adjacent to pumping well MW-26; TW4-21 is located adjacent to pumping well TW4-19; and TW4-22 is located adjacent to pumping well TW4-20. Fluctuations in concentrations at pumping wells and wells adjacent to pumping wells likely result in pari from changes in pumping. Although the change in concentration at TW4-24 was greater than 20%, the increase from 1.1 to 1.7 [!g/L is likely due to analytical error because the concentrations are close to the detection limit. Pumping well TW4-20 had the highest detected chloroform concentration. Since the last quarter, the chloroform concentration in TW4-20 decreased from 8,100 [!glL to 6,800 ""giL, the concentration in adjacent pumping well TW4-19 decreased substantially from 4,000 ""gIL to 970 ""giL, the concentration in nearby well TW4-21 increased from 290 to 460 ""giL, and the concentration in nearby well TW4-22 increased from 210 [!glL to 450 ""gIL. Wells TW4-23 and TW4-25 remained non-detect for chloroform. TW4-24, located west of TW4-22, and TW4-25, located north of TW4-21, bound the chloroform plume to the west and north. The chloroform concentration in TW4-16, located immediately downgradient of the chloroform plume, decreased from 16 ""gIL to 9.2 ""gIL. Slight expansion and contraction of the chloroform plume boundaries in response to changes in up gradient pumping are expected to impact the concentrations at TW4-16. In addition, the southernmost boundary of the plume remains between TW 4-4 and TW 4-6 (located just north of southernmost temporary well TW4-26). The chloroform concentration in TW4-6 increased from 9.6 [!g/L to 16 ""gIL. Although the concentration increased, TW 4-6 remains outside the chloroform plume boundary. Concentrations at TW4-6 have been on a generally downward trend since initiation of pumping of TW4-4 in the first quarter of 2010, and have decreased from 1000 ""giL to 16 ""gIL since that time. TW4-6, installed in the second quarter of 2000, was the most downgradient temporary perched well prior to installation of temporary well TW4-23 in 2007 and temporary well TW4-26 in the second quarter of 2010. TW4-6 remained outside the chloroform plume between the second quarter of 2000 and the fourth quarter of 2008. TW4-6 likely remained outside the chloroform plume during this time due to a combination of 1) slow rates of downgradient chloroform migration in this area due to low permeability conditions and the effects of upgradient chloroform removal by 16 N:IRcquired ReporlslChloro[orm Quarterly Monitoring Reporll2011 Q312011_Q3Chloro[orm_Reporu ext.doc pumping, and 2) natural attenuation. Because TW4-6 is again outside the plume boundary, TW4-6 and TW4-23 bound the chloroform plume to the south. The slow rate of chloroform migration in the vicinity of TW4-6 is demonstrated by comparing the rate of increase in chloroform at this well to the rate of increase in the nearest up gradient well TW 4-4. Concentrations at TW 4-4 increased from non-detect to more than 2,200 !!gIL within only 2 quarters whereas 16 quarters were required for concentrations in TW4-6 to increase from non-detect to only 81 !!gIL. This behavior is consistent with hydraulic tests performed at TW4-4, TW4-6, and TW4-26 during the third quarter of 2010 that indicate a nearly two order of magnitude decrease in permeability downgradient of TW 4-4. Chloroform migration rates in the vicinity of recently installed well TW4-26 are also expected to be relatively low due to upgradient pumping and low permeability conditions. 5.0 LONG TERM PUMP TEST AT MW-4, MW-26, TW4-19, TW4-20, AND TW4-4 OPERATIONS REPORT 5.1 Introduction As a part of the investigation of chloroform contamination at the Mill site, DUSA has been conducting a Long Term Pump Test on MW-4, TW4-19, MW-26, and TW4-20, and, since January 31, 2010, TW4-4. The purpose of the test is to serve as an interim action that will remove a significant amount of chloroform-contaminated water while gathering additional data on hydraulic properties in the area of investigation. The following information documents the operational activities during the quarter. 5.2 Pump Test Data Collection The long term pump test for MW-4 was started on April 14, 2003, followed by the start of pumping from TW4-19 on April 30, 2003, from MW-26 on August 8, 2003, from TW4-20 on August 4, 2005, and from TW4-4 on January 31, 2010. Personnel from Hydro Geo Chem, Inc. were on site to conduct the first phase of the pump test and collect the initial two days of monitoring data for MW-4. DUSA personnel have gathered subsequent water level and pumping data. Analyses of hydraulic parameters and discussions of perched zone hydrogeology near MW-4 has been provided by Hydro Geo Chern in a separate report, dated November 12, 2001, and in the May 26,2004 Final Report on the Long Term Pumping Test. Data collected during the quarter included the following: • Measurement of water levels at MW-4, TW4-19, MW-26, and TW4-20 and, commencing regularly on March 1,2010, TW4-4, on a weekly basis, and at selected temporary wells and permanent monitoring wells on a monthly basis. • Measurement of pumping history, including: 17 N:\Rcquired RcportslChloroform Quarterly Monitoring Rcportl2011 Q312011_Q3Chlol'Oform_Reporuexl.doc pumping rates total pumped volume Operational and non-operational periods. • Periodic sampling of pumped water for chloroform and nitrate/nitrite analysis and other constituents. 5.3 Water Level Measurements Beginning August 16, 2003, the frequency of water level measurements from MW-4, MW-26, and TW4-19 was reduced to weekly. From commencement of pumping TW4- 20, and regularly after March 1, 2010 for TW4-4, water levels in these wells have been measured weekly. Depth to groundwater in all other chloroform contaminant investigation wells is monitored monthly. Copies of the weekly Depth to Water monitoring sheets for MW-4, MW-26, TW4-19, TW4-20 and TW4-4 and the monthly Depth to Water monitoring sheets for all of the chloroform contaminant investigation wells are included under Tab C. Monthly depth to water measurements for September are recorded in the Field Data Worksheets included under Tab D. 5.4 Pumping Rates and Volumes Table 2 summarizes the recovered mass of chloroform by well per quarter and historically since the inception of the chloroform recovery program for the five currently- active pumping wells. 5.4.1 MW-4 Approximately 85,327 gallons of water were pumped from MW-4 during the quarter. The average pumping rate from MW-4, when the pump was pumping, was approximately 4.2 gpm throughout the quarter. The well is not pumping continuously, but is on a delay device. The well purges for a set amount of time and then shuts off to allow the well to recharge. Water from MW -4 was transferred to the Cell 1 evaporation pond through a pipeline installed specifically for that purpose. 5.4.2 TW 4-19 Approximately 141,542 gallons of water were pumped from TW4-19 during the quarter. The average pumping rate from TW4-19, when the pump was pumping, was approximately 13.9 gpm throughout the quarter. The pump in this well is operating on a delay. It pumps for approximately one and a half minutes and then is off for two to three minutes. Water from TW4-19 was directly transferred to the Cell 1 evaporation pond through a pipeline installed specifically for that purpose. It was noted by Field Personnel on September 29, 2011 that the flow meter in TW4-19 was damaged during routine maintenence. The flow meter was replaced on September 29, 2011 within 24 hours. Field Personnel collected measurements the following week as scheduled. 18 N:IRequired ReportslChloroform Quarterly Monitoring Reportl2011 Q312011_Q3Chloroform_Reporucxt.doc 5.4.3 MW-26 Approximately 65,618 gallons of water were pumped from MW-26 during the quarter. The average flow rate from MW-26, when the pump was pumping, was approximately 6.3 gpm throughout the quarter. The well is not pumping continuously, but is on a delay device. The well now purges for a set amount of time and then shuts off to allow the well to recharge. The water is directly transferred to the Cell 1 evaporation pond through a pipeline installed specifically for that purpose. 5.4.4 TW 4-20 Approximately 72,311 gallons of water were pumped from TW4-20 during the quarter. The average flow rate from TW4-20, when the pump was pumping, was approximately 9.6 gpm throughout the quarter. The well is not purging continuously but is on a delay device. The well pump is set on a water elevation device. When the water reaches a set point, the pump turns on until the water level drops to another set point. The water is directly transferred to the Cell 1 evaporation pond through a pipeline installed specifically for that purpose. 5.4.5 TW4-4 Approximately 97,535 gallons were pumped from TW4-4 during the quarter. The average flow rate, when the pump was pumping, was 9.9 gpm. The well is not pumping continuously, but is set on a water elevation device. When the water reaches a set point, the pump turns on until the water level drops to another set point. The water is directly transferred to the Cell 1 evaporation pond through a pipeline installed specifically for that purpose. 5.5 Mass Removed Chloroform removal was estimated as of the first quarter 2007. Since that estimation the mass removed by well for each quarter has been compiled in Table 2 below, indicating that a total of 580.6 pounds of chloroform have been removed to date. 5.6 Inspections Denison has submitted an Operations and Maintenance Plan, Chloroform Pumping System, White Mesa Mill, Blanding, Utah, Revision 2.1 to UDEQ for approval on October 25, 2010. Upon approval of that plan, the Mill will commence documenting its required inspections of the operational status of the chloroform pumping wells on an inspection form. An example of the form as well as completed reports for the quarter will be included in future Chloroform reports upon approval by UDEQ. At the time of the publication of this report approval of the Operations and Maintenance Plan, Chloroform Pumping System, White Mesa Mill, Blanding, Utah, Revision 2.1 had not been received. Operational problems in the pumping wells are summarized above. 19 N:IRcquired RcportslChloroform Quarterly Monitoring Reportl2011 Q312011_Q3Chloroform_Reporuext.doc 5.7 Conditions That May Affect Water Levels in Piezometers Water was added to the upper and lower wildlife diversion ponds during the quarter. The middle wildlife pond had no water added and is dry at this time. 6.0 CORRECTIVE ACTION REPORT Necessary corrective actions identified during the current monitoring period are described below. 6.1 Rinsate Blank Sample Chloroform Levels Identification and Definition of the Problem Rinsate Chloroform Levels Chloroform has been present in the rinsate blanks in previous quarters and was addressed through a change in the decontamination procedures and rinsate blank frequency suggested by UDEQ personnel. To address the nitrate contamination in the nitrate and chloroform sampling programs, an additional rinse with 55-gallons of Dr water has been added to the decontamination process. The added 55-gallons of Dr water per decontamination of the portable pump has caused chloroform to reappear in the rinsate blanks. DUSA believes that the potential source for the chloroform present in the rinsate blanks appears to be related to the increasing volume of Dr water used in the rinsate process due to the second 55-gallon rinse with Dr water. The chloroform present in the rinsate blanks is most likely present in the Dr water and is not the result of inadequate decontamination of the purging pump. The chloroform contamination in the Dr water is most likely the result of chlorination of the intake water used for the Dr system. Assignment of Responsibility for Investigation of the Problem The problem is currently under investigation by the QA Manager. Investigation and Determination of Cause of the Problem Rinsate Blank Sample Chloroform Levels As discussed above, chloroform is most likely entering the rinsate blanks from the chlorination of the potable water supply used as a feed to the Dr system. The Dr system is showing signs of breakthrough at times of high usage. To address the issue, the QA manager is working with mill staff evaluating the best approach to implement upgrades to the Dr system to ensure its ability to support the high volume of Dr water needed for the rinsate process. 20 N:IRequired RcporlslChlorofonn Quarlerly Moniloring RcpOltl2011 Q312011_Q3Chloroform_RcporuexLdoc Determination of a Corrective Action to Eliminate the Problem Rinsate Blank Sample Chloroform Levels The chloroform contamination in the DI water is most likely the result of chlorination of the intake water used for the DI system. Based on low level detections this quarter, the additional of a second DI rinse in the process is "stressing" the system and causing chloroform contamination. By upgrading the system, it will be able to support the high volume of DI water being pumped through the system. Assigning and Accepting Responsibility for Implementing the Corrective Action Rinsate Blank Sample Chloroform Levels It will be the joint responsibility of the Director, Compliance and Permitting, and the Mill's sampling staff to implement the changes and to assess the data to determine if it has corrected the problems. Implementing the Corrective Action and Evaluating Effectiveness Rinsate Blank Sample Chloroform Levels Chloroform sources will be removed after the DI system is upgraded to support the high volume of DI water in the system during the rinsate process. Analysis of the DI system by DUSA is underway to determine the best design for the system upgrades. Data collected after the completion of the system upgrades will determine if any fUlther action is necessary to eliminate rinsate contamination. Verifying That the Corrective Action Has Eliminated the Problem Verification that chloroform contamination has been eliminated will occur upon completion of the system upgrades and receipt of at least the two quarters of data. If chloroform contamination persists then additional sources will be researched and the investigation will continue. 6.2 Assessment of Previous Quarter's Corrective Actions The second quarter 2011 report identified corrective actions for chloroform contamination in the rinsate blank samples. Chloroform contamination was present in the third quarter 2011 sampling event, confirming the source of the issue being the DI system's inability to support the volume of DI water necessary for the rinsate process. Evaluation and implementation of system upgrades are underway and will eliminate the chloroform contamination once the upgrades are complete. 7.0 CONCLUSIONS AND RECOMMENDATIONS The water level contour maps for the third quarter, 2011 indicate that effective capture of water containing high chloroform concentrations is occurring in the vicinity of pumping wells MW-4, MW-26, TW4-19, and TW4-20. TW4-4 has apparently not been pumped long enough for a well-defined capture zone to become evident. Furthermore, the capture 21 N:IRequircd ReportslChloroform Quarterly Monitoring Reportl2011 Q312011_Q3Chloroform_Reporuext.doc zone associated with TW 4-4 may be less apparent because of the low water level at adjacent well TW4-14. However, the decrease in chloroform concentrations at TW4-6 (located down gradient of TW4-4)since the fourth quarter of 2009 is likely related to TW 4-4 pumping. Third quarter, 2011 chloroform concentrations at many of the wells with detected chloroform were within 20% of the values reported during the previous qmuter, suggesting that variations are within the range typical for sampling and analytical error. Changes in concentration greater than 20% occurred in wells MW-26, TW4-6, TW4-1O, TW4-16, TW4-19, TW4-21, TW4-22, and TW4-24; the concentration in well TW4-24 increased slightly from 1.1 !!g/L to 1.7 !!g/L. Of the wells showing changes in concentration greater than 20%, MW-26, and TW4-19 are pumping wells. TW4-6 is located adjacent to pumping well TW4-4; TW4-1O and TW4-16 are located adjacent to pumping well MW-26; TW4-21 is located adjacent to pumping well TW4-19; and TW4-22 is located adjacent to pumping well TW4-20. Although the change in concentration at TW4-24 was greater than 20%, the increase from 1.1 to 1.7 !!glL is likely due to analytical error because the concentrations are close to the detection limit. Fluctuations in concentrations at pumping wells and wells adjacent to pumping wells likely result in part from changes in pumping. Between the current and previous quarters, the concentration in TW4-26, which is the most down gradient temporary well, decreased slightly from 2.9 !!glL to 2.8 !!glL. The highest chloroform concentration (6,800 !!glL) was detected at pumping well TW4- 20. Between the current and previous quarters, the chloroform concentration in TW4-20 decreased from 8,100 !!g/L to 6,800 !!glL, the concentration in adjacent pumping well TW4-19 decreased from 4,000 !!glL to 970 !!g/L, the concentration in nearby well TW4- 21 increased from 290 to 460 !!glL, and the concentration in nearby well TW4-22 increased from 210 !!glL to 450 !!glL Fluctuations in concentrations in these wells are likely related to their location near the suspected former office leach field source area in addition to variations in pumping in TW4-20 and nearby wells. Regardless of these measured fluctuations in chloroform concentrations, sampling of temporary wells TW 4- 24 (located west of TW4-22) and TW4-25 (located north of TW4-21), indicates these wells remain outside the chloroform plume and thus bound the plume to the west and north. Chloroform was not detected at TW4-25, and was detected at a concentration of 1.7 !!g/L at TW4-24. The chloroform concentration at well TW4-6 increased from 9.6 !!glL to 16 !!glL. This well has been outside the chloroform plume boundary since the fourth quarter of 2010. In the past, TW 4-6 has been both within and outside the plume. From the first quarter of 2009 through the fourth quarter of 2010, TW4-6 was within the plume. Prior to that time, between the time of installation in the second quarter of 2000 and the fourth quarter of 2008, TW 4-6 was outside the plume. Although fluctuations in concentrations have occurred, this well likely remained outside the plume between installation in 2000 and the fourth quarter of 2008 due to a combination of 1) slow rates of downgradient chloroform migration in this area due to low permeability conditions and the effects of upgradient chloroform removal by pumping, and 2) natural attenuation. The decreases in 22 N:IRequircd ReportslChloro[orm Quarterly Monitoring Rcportl20 II Q3120 Il_Q3Chloro[oml_RcporuexLdoc concentrations at TW 4-6 since the fourth quarter of 2009 are likely the result of up gradient pumping, in particular pumping at adjacent well TW4-4 (which commenced in the first quarter of 2010). Chloroform remained non-detect at downgradient temporary well TW4-23. TW4-23 and TW4-6 (with a chloroform concentration of 16 !!glL) bound the chloroform plume to the south. Continued pumping of MW-4, MW-26, TW4-19, and TW4-20 is recommended. Pumping these wells, regardless of any short term fluctuations in concentrations detected at the wells (such as at TW4-20), helps to reduce downgradient chloroform migration by removing chloroform mass and reducing average hydraulic gradients, thereby allowing natural attenuation to be more effective. Continued pumping at TW 4-4 is also recommended to improve capture of chloroform to the extent practical in the southern portion of the plume where low permeability conditions exist. The general decrease in chloroform concentrations at TW4-6 from 1000 !!glL to 16 !!glL since the first quarter of 2010 is likely related to pumping at TW4-4. The decrease in the long-term rate of water level rise at TW4-6 since TW4-4 pumping began, which suggests that TW4-6 is within the hydraulic influence of TW4-4, is consistent with the decrease in chloroform concentrations at TW 4-6. 8.0 ELECTRONIC DATA FILES AND FORMAT DUSA has provided to the Executive Secretary an electronic copy of all laboratory results for groundwater quality monitoring conducted under the chloroform contaminant investigation during the quarter, in Comma Separated Values (CSV) format. A copy of the transmittal e-mail is included under Tab M. 23 N:IRcquircd RcportslChloroform Quarterly Monitoring RcpOltl20 II Q3120 II_Q3ChlorofomU~cporuexl.doc 9.0 SIGNATURE AND CERTIFICATION This document was prepared by Denison Mines (USA) Corp. on November 28,2011. DENISON MINES (USA) CORP. Vice President, Regulatory Affairs and Counsel 24 N:IRcquircd RcportslChloroform Quarterly Monitoring Rcportl2011 Q312011_Q3Chloroforn'-'~eporuex(.doc Certification: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and nt fo nowing violations. Vice Presid nt, Regulatory Affairs and Counsel Denison Mines (USA) Corp. 25 N:IReqllired ReportslChlorororm Quarterly Monitoring Reportl20 II Q3120 II_Q3Chlorororm_Rcporucxt.doc Tables Table 1: Summary of Well Sampling for the Period , :~/I'~' 'i,' O,);!'..", . 'I" "t Y ". "! ,(. ,;,'1, .'. ., ';" , , 'D'att~ of IJal)(Rtj)~rt.'! ' .,. ,j " t· Sampl~ Date ' "'it t1I . ;,. ': ,i· Well . I' ", MW-4 8117/2011 9/61201 1 TW4-1 8118/2011 9/612011 TW4-2 8117/2011 9/612011 TW4-3 811612011 9/612011 TW4-3R 811512011 9/6/2011 TW4-4 811712011 9/612011 TW4-5 811712011 9/612011 TW4-6 81171201 1 9/612011 TW4-7 8118/2011 9/612011 TW4-7R 811712011 9/6/2011 TW4-8 8116/2011 9/612011 TW4-9 811612011 9/612011 TW4-10 811712011 9/6/2011 TW4-11 811712011 9/612011 TW4-12 811612011 9/6/2011 TW4-13 8/16/2011 9/612011 TW4-14 8/16/2011 9/612011 TW4-15 (MW-26) #N/A 9/612011 TW4-16 8/17/2011 9/612011 MW-32 811612011 9/612011 TW4-18 811712011 9/612011 TW4-19 811712011 9/612011 TW4-20 8/17/2011 9/612011 TW4-21 8/1712011 9/612011 TW4-22 8/17/2011 9/6/2011 TW4-23 8116/2011 9/612011 TW4-24 8/17/2011 9/612011 TW4-24R 8116/2011 9/612011 TW4-25 8116/2011 9/612011 TW4-26 811712011 9/6/2011 TW4-60 811712011 9/612011 TW4-65 811612011 9/6/2011 TW4-70 8117/2011 9/612011 All sample locations were sampled for Chloroform, Carbon Tetrachloride, Chloromethane, Methylene ChlOlide, Chloride and Nitrogen "R" following a well number deisgnates a tinsate sample collected prior to purging of the well of that number. TW4-60 is a DI Field Blank, TW4-65 is a duplicate of TW4-23, and TW4-70 is a duplicate ofTW4-l6, Highlighted wells are continuously pumped, Table 2 Chloroform Mass Removal Per Well Per Quarter I ::f~:." . " " 'I iik, ,~\: " l'W4.:15 (MW.26) TW4·19 TW4·20 ' TW4·4, ,. ,"" I, " II ,. J\:lW ~ll (lb,s:j; I.'e ", ~i,\(lbs\.) ,Ji' ' . ,(Ibs.), .' ". . I, (~bs.) I Quarter 'f otalS"(lbs.), I:JI¥\ I!, .," Quar~~r ' ,'" . if ,'\' )t'" ,"JIbs.) .,'Ct, ' tl I) 'I ' /£ ' I .j........ , Q12007 36.8 12.9 150.2 87.0 NA 286.9 Q22007 1.4 0.1 0.0 2.5 NA 4.0 Q32007 2.2 0.8 2.9 3.1 NA 9.0 Q42007 1.7 1.0 3.1 4.8 NA 10.6 Q12008 1.7 0.4 4.6 7.2 NA 13.8 Q22008 1.3 0.5 3.2 9.9 NA 14.8 Q32008 1.2 0.3 15.9 9.3 NA 26.8 Q42008 1.3 0.3 20.7 0.4 NA 22.7 Q12009 1.7 0.4 4.3 3.6 NA 10.0 Q22009 6.8 0.2 3.7 2.8 NA 13.5 Q32009 1.5 0.4 11.1 5.5 NA 18.5 Q42009 4.8 0.6 17.8 26.1 NA 49.4 Q12010 0.9 0.4 2.7 0.4 NA 4.5 Q22010 1.5 1.0 6.8 5.9 1.4 16.5 Q32010 1.3 1.2 2.0 4.9 1.3 10.6 Q42010 1.1 0.5 7.7 7.4 1.2 17.9 Q12011 l.1 0.2 12.9 9.6 1.1 24.9 Q22011 1.2 0.8 5.3 4.6 1.1 13.1 Q32011 1.2 1.0 4.7 4.9 1.4 13.2 Well Totals (pounds) 70.6 23.0 279.5 199.9 7.6 580.6 INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Order of Sampling and Field Data Worksheets Tab C Weekly and Monthly Depth to Water Data Tab D Kriged Current Quarter Groundwater Contour Map, Capture Zone Map, Capture Zone Details Map, and Depth to Water Data Tab E Kriged Previous Quarter Groundwater Contour Map Tab F Hydrographs of Groundwater Elevations Over Time for Chloroform Monitoring Wells Tab G Depths to Groundwater and Elevations Over Time for Chloroform Monitoring Wells Tab H Laboratory Analytical Reports Tab I Quality Assurance and Data Validation Tables 1-1 Field Data QAlQC Evaluation 1-2 Holding Time Evaluation 1-3 Receipt Temperature Check 1-4 Analytical Method Check 1-5 Reporting Limit Evaluation 1-6 Trip Blank Evaluation 1-7 QAlQC Evaluation for Sample Duplicates 1-8 QC Control Limits for Analyses and Blanks 1-9 Rinsate Check Tab J Kriged Current Quarter Chloroform Isoconcentration Map Tab K Analyte Concentration Data Over Time Tab L Chloroform Concentration Trend Graphs Tab M CSV Transmittal Letter Tab N Disinfection byproducts -Trihalomethanes Tab A Site Plan and Perched Well Locations White Mesa Site ..?-:;::::- 9 7 I!.lf III II II II ~I II I II II II II II II il II I 32 ~ MVv-21 II ,I \1 \\ ~ PROPERTY BOUNDARY II {( II II II II II II II 'I MW-01 • MW-18 • ~S ~ ~ TWN-18 TWN-7 ~ TWN-3 ~ TWN-S ~ TWN-8 ~ TWN-1S ~ TWN-10 ~ TWN-9 PIEZ-1 ., MW-19 • ., ~ ~ TWN-11 TWN-12 ~ ~ TWN-14 d -...;;:: M~27 /rWpJ) Tb~-4 MW-D2 • Mw-bs -¢-, MW-2 CELL NO.1 CELL NO.2 MW~ h MW~3 __ Mll\f-34 M.\t!'- -¢--¢--~ ."-t----M MW-37 MW-03 • MW-17 • 33 PIEZ-3 ., lOTW4-1IbTW4-11 OTW4-13 TW4-7~~-8 M -32 OTW4-1 • OTW4-40TW4_14 TW4-23 OTW4-S ° PIEZ-4 ., PI EZ-S ., OTW4-2S h~'::::=--=--6 7 --==--.=-.==:-' /,~7 /' T378 T38S ~ MW-20 ~ . ~ I ., \ j ~\ ~ i11'~ ~~.~~~~ ~~ 4~~~~~~4_~~~~~~~~~~~7! "'--=- N 1 L...:.--. _ ! MW-22 • II // // o MW-20 • TW4-19 SCALE IN FEET EXPLANATION perched monitoring well o temporary perched monitoring well PIEZ-1 ~ TWN-1 <> MW-34 -9- MW-36 ~ perched piezometer temporary perched nitrate monitoring well perched monitoring well installed August/September, 2010 perched monitoring well installed April, 2011 3000 wildlife pond HYDRO GEO CHEM, INC. APPROVED SJS // // // // // // // // SITE PLAN AND PERCHED WELL LOCATIONS WHITE MESA SITE DATE REFERENCE H:/718000/nov11/welloc11.srf ~ ~ o ~ ~ \. (}, \ FIGURE A-1 • > ., TabB Order of Sampling and Field Data Worksheets , \---o Order of Contamination for 3rd Qua~ter 2011 Chloroform Purging Event Previous Quarter CfilorofOi.·m--- Well Sampletirtle Levels Rinsate date/time TW4 .. 3 TW4-1~ "J)-. TW4;;;13 TW4-14 MW-32 TW4-23 TW4-25 TW4-8 TW4-9 TW4-24 $1 • .,/11 TW4-26 TW4-5 TW4-6 TW4-16 TW4.:.18 --TW4-22 . TW4-1O TW4-21 TW4-H TW4-7 gjlriJI TW4-1 r,/16/11 Oit:lS oW.!> 0(;,'\5 Df-55 67 OS 072.1 01'35 07'-15 o1Sb OM] 0b3.b Of,,'-i7 :SR ND ~/IS/Ii' D(;."iS ND ND ND ND 'f.,!IUII lASS ND ND ND ND .2.'1 R 1.1 S/ib!1l D6.I..\O 2.9 9 9.6 16 26 210 280 290 930 7 iZ 1200 2S/jtIJ 1o 015~q 1200 MW4 ~1i1/il I?Oli 1700 TW4-4 lS/i11il 1':'>15 1700 TW4-15 :6(1"71 II 1&50 1800 TW4-2 I£/I~/'I Ob~7 3000 TW4-19 gil?/ /I jl.\OO 4000 TW4-20 "ih7! II \21..\0 8100 TW4-60 _D_.I_. B_la_n_k __ ..... /!,.u.1..L.11u.)..:..Jl!t.....-1I..t30 TW4-65 Duplicate -~------------TW 4-70 Duplicate tf,,/ l1111 010:::' Comments: lie- Water level Well Depth 141 101.5 102.5 93 130.6 Bladder pump 114 134.8 125 120 112.5 86 120 97.5 142 137.5 Cont. Pumping 113.5 111 121 100 120 110 124 Cont. Pumping 112 Cont. Pumping 122.5 Cont. Pumping 120 125 Cont. Pumping 106 Cont. Pumping Name: Date: -------------------------- Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) OE~~~ONI).4~-1 WHITE A~~~~~~:~~ MILL MINES ~ FIELD DATA WORKSHEET FOR GROUND WATER Attachment 1 ~ See instruction Description of Sampling Event: I '3 rIA Q '-"6..d~(' G h I of I) 'to( fVI ;;l.O II Location (well name):L-1 --'-M_w_-_Ll _________ --' Sampler Name and initials: I 1""o.n 'I u Rol1;J~/'fH Date and Time for Purginm g) 11/~OII and Sampling (if different) ;vIA '--~~-----~ Well Purging Equip Used:@]pump o@ bailer Sampling Event I Q~fM"+~r~ c..hlo<o1~(M I pH Buffer 7.0 7.0 Specific ConductanceL,..I_Q..l..Q..;...1.L.-__ ---lIIJ.MHOS/ cm Depth to Water Before purgind '7 \.O~ Conductance (avg) Well Pump (if other than Bennet) Prevo Well Sampled in Sampling Event L-1 _""r_W_L.\_-_,_S ____ .....I pH Buffer 4.0 L\.D Well Depth(O.Olft): Casing Volume (V) pH of Water (avg) 4" well:~ __ O_---1I(.653h) 3" Well:. 14.YY . (.367h) 6 .57 Well Water Temp. (avg) I IS.1~ Redox Potential (Eh) 1L.....-::J..,.;.;;.13"--_-' Turbidity ...... 1 _0 __ --' Weather Condo Ext'l Amb. Temp. DC (prior sampling event)1 30~ Time I )3oL{ I Gal. Purged I I Time I I Gal. Purged I I Conductance I :l.Ob(;, I pH I b.S7 I Conductance I I pH I I Temp.oC I J5 .9g I Temp.oC I I Redox Potential Eh (m V) I 2.13 I Redox Potential Eh (mV) I I Turbidity (NTU) I 0 I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Grouridwater 1 of2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged L-1 __ o ___ ...J Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = .... 1 _C_} ._, __ ---' gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= 1 0 1 Number of casing volumes evacuated (if other than two) D If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~L-_jV_J_A ______ ----, Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y N VOCs D D 3x40 mI D ~ HCL ~ D Nutrients 1]1 D 100mI D ~ H2SO4 &1 D Heavy Metals D D 250mI D D HN03 D D All Other Non Radiologics D D 250mI D D No Preserv. D D,. Gross Alpha D D 1,000 mI D D HN03 D D Other (specify) Ll D Sample volume D rn D aI G h \o('i~e. If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction A'((l\)e~ 0\"\ ';)i1-G Cl.J ,~S. --rl.nl'let' tN'IQ. &~(f;f\ P"'GSt'fI-t-+or' sa.Y'1jl);~ -e\)~Y1t. 1-l>oK ae.pth to ~o-.+e(, S~t'I\?\~.5' \NU~ l:O \lec.t.eJ. o.t l305. ~G\1e'( \}Jcc, CJe.CA{. I3t>)< is ~ll eJ' M iu: I L-e..ft-s it~ 0..-1-13D7 L-_______ --IIDo not touch this cell (SheetName) White Mesa Mill Fipld Data Worksheetfor Groundwater " 2 of2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 OENISONIlJJ WHITE MESA URANIUM MILL Attachment 1 ~ See instruction MINES FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: ! '3 r til G "'-0,"'\=(.(" z:: h I oc 0='\":' (M 20 \ I Location (well name):L-! _T_W_L_\ _-_, ________ ---1 Sampler Name and initials: 11"';. n n~"'" ~ £) 11.'0\ o.~/T If Date and Time for PurgingJ it) J i 7 ~ 0 ) ) and Sampling (if different) I ~/ 18/:1.-01 \ Well Purging Equip Used: [][] pump or@] bailer Well Pump (if other than Bennet) Prevo Well Sampled in Sampling Event l-rv-J L\_I pH Buffer 7.0 7.0 pH Buffer 4.0 L\.o Specific Conductancel..-! -----'4.....;.~_4 __ ---I!f-tMHOS/ cm Well Depth(O.Olft): 110·00 Depth to Water Before PurgingJ f>l.\. L\ b Casing Volume (V) 4" well:1 ~9.77 1(·653h) 3" Well: () (.367h) '--__ --J Conductance (avg) '-!_2....;...':1..;....Lj...;.;;g~ ____ --J pH of Water (avg) 6.05 Well Water Temp. (avg) ! 1S.2..L Redox Potential (Eh) !I..-~_g_q __ --, Turbidity 1..-1 g_o~-----,_--, Weather Condo Ext'l Amb. Temp. O( (prior sampling event)1 !:I...!..j fI Time ! Oq~ I Gal. Purged I ED I Time I OQ5b I Gal. Purged I bQ I Conductance I ~S) I pH I 6.Cf1 I Conductance IoU.. Y-b I pH Ib'oS I Temp.oC I is ·'3" 1 Temp.oC 1 [5·2:4 1 Redox Potential Eh (mV) 1 :51 \ 1 Redox Potential Eh (m V) I '3:& 7 1 Turbidity (NTU) 1 L.\O I 1 Turbidity (NTU) 1400 I Time 1 ()~.5 7 1 Gal. Purged 1 11 1 Time 1 DqSg 1 Gal. Purged I " ff 1 Conductance I ~qg 1 pH 1 G·05 1 Conductance 1.2.2.47 1 pH 1 b.b3 1 Temp.oC 1 \5.::5 1 Temp.oC 1 1~·2.0 1 Redox Potential Eh (mV) I 3~1 1 Redox Potential Eh (mV) 1 :3 71 1 Turbidity (NTU) 1 y\!) 1 Turbidity (NTU) I Cll7 1 White Mesa Mill Field Data Worksheet for Groundwater" 1 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged ..... 1 ....!::f>:....t::f!~ __ ---I Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = ..... 1 _'_I __ ----l gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= 1 S.!..ll 1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy LablL.....;.,;v_/_~=--______ ......I Sample Taken Sample Vol (indicate Filtered Preservati ve Preservative Type of Sample if other than as Type Added y N specified below) y N Y N VOCs ~ 0 3x40 mI 0 ~ HCL ~ 0 Nutrients III 0 lOOmI 0 ~ H2SO4 I)g 0 Heavy Metals 0 0 250 mI 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml D · 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 mI 0 0 HN03 0 0 Other (specify) 5!1 0 Sample volume 0 @ 0 ~ c::-h \ 0,', c\ ( If preservative is used, specify Type and Quantity of Preservati ve: Comment ~ See instruction A'(r;\lC::~ on si+~ o.:r OqL..\b.--ro.t'\f\d c...n~ G-o.«;f\ pa.s<=I'\t--to pv.r~'C -rwUj~I . f\J.<~t be~o.l'\ "J O'\5D. r W"~a \>.)<u for " +ot .. 1 C>f '6 I"li n",tes. v,) .. -h, W"S J.,A~ \,..)11-~ ~otr\(. ~;rt~ .?C'A/f)(:,I-c~. ?\A(~r €Y1Jeck ~-t bC!S.8'. D-cpt-h 1-D water \.0<0 \Ol.l~. Le·r\-SIte., etY i003. Arr;-Jed .. 01\ ~JT~&<..} Of,LJI. ~""<:r,.,,,4 o-CA.rr,il p,...e~",(a 1-0 (,.DlleG+ ~Mplc~. D1!pth to v.x...+er WtA~ bY.LJ! $oq~1p}t!> we('~ b",:I~&l Ai-Of.'1J. L08-$1+<' 1iI.-t Qb5D '--_______ -'IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 20n Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 ~ See instruction FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: Sampler Name and initials: fi4.t1I1U j.OJo 11 ,()~ Location (well name):trL.._W_Y_-_:l.. _________ ---' Date and Time for PurgingJL....:::g~J..;..17;..:/....::;~.;;:..O_I_' ____ -J and Sampling (if different) "6/lg/:;'OJ J Well Purging Equip Used:OOpump o@ bailer Well Pump (if other than Bennet) Sampling Event I GI\UA r1ed.i c:.h lo .... o-torrVl Prevo Well Sampled in Sampling Event L..I_TW __ \..._I-_I _____ --' pH Buffer 7.0 7.0 pH Buffer 4.0 LI.O Specific Conductance'-l_q.o...:~'_q ___ ___JIf-tMHOS/ cm Well Depth(O.Olft): I l~O.oo Depth to Water Before Purgingj b 7 .1...\ ~ 4" well:l .3y,;z.Q 1(·653h) 3" Well: 0 (.367h) 1....-___ --' Casing Volume (V) Conductance (avg) pH of Water (avg) Well Water Temp. (avg) \b.~O Redox Potential (Eh) I t..j 03 Turbidity 1I--:-ll:....;;D __ --, Weather Condo Ext'l Amb. Temp. O( (prior sampling event)1 :l.,o Time I IO'3g I Gal. Purged I ]7 I Time I I Gal. Purged I I Conductance 1 30bg I pH I b.'-\D I Conductance I I pHI I Temp. DC I 1C:.~o I Temp. DC I I Redox Potential Eh (m V) I LJQ3 I Redox Potential Eh (mV) I I Turbidity (NTU) I " D I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pHI I Conductance I I pHI I Temp. DC I I Temp. DC I I Redox Potential Eh (m V) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater .. 1 of2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1 '-_7_7 ___ ----' Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = ,-I _'_' __ ---' gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= 1 ~.;(3 1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated 77 Name of Certified Analytical Laboratory if Other Than Energy Lab~L...~_'/4"'::"-______ -J Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y VOCs ~ 0 3x40 rnl 0 ~ HCL ~ Nutrients tB 0 100rnl 0 ~ H2SO4 ~ Heavy Metals 0 0 250 rnl 0 0 HN03 0 All Other Non Radiologies 0 0 250 rnl 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 rnl 0 0 HN03 0 Other (specify) Ttl 0 Sample volume 0 ~ 0 G h \ bf' -I J e:-If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction A(ri\le~ on site tA1-10.2.7. I~nner ~ntA 6-Mr~n ?re.seJ\f-+0 ?1..4~<" T~I...I-"<'. 'P"'I"~(.. bCj~1\ ~t Pv,.r~c\ v:>e\\ ro(" r;... -Yo+~l of 7 (f)il'lv--res . P\J,.(~~{~ well ch~l. \.)o..+ct' Wc..~ <A:rtJ· ?v.r~<. e.n~eA f..1 1038. L~++ SI'1-! ~+ loL13· /'rr(:"J-e.~on s,,-\-,; CA.1-obSD. ~~I1-C"" ~ntif &",(ri" ?rc.s.<..Y\t k ~ollt:(,i-.f,t..rVlpl~.>. Pcp1-~ to 'v0o-.1-C( IN~ b 7.5:2,. SV-.W)p\e.) ~e('e.. k~'ecl Q\.t-ObS 7. Le.~.$ ;-rc li\.t 07 DO '--________ ..... IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 1031 N 0 0 0 0 0 C!l 2 of Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) E~i~~~~ l ~'IELD DA~:~~::;~~~~f~R~~D WATER Attachment 1 ~ See instruction Description of Sampling Event: 13ril Q",().("1-c:r G)')o('ofO()'V"' Location (well name): ..... I '_\J_1......:..1 _-::::::.3'--________ ---' Sampler Name and initials: I-r;:nne(" H6Jl,·d4.!1)rH Date and Time for PurgingJ ~/'51;J..O J I Well Purging Equip Used: IT!] pump or@] bailer Sampling Event 1 Q \kIM ta ~ G ~ 10 (of'r>. fV\ pH Buffer 7.0 7.0 Specific Conductance ..... 1 _'I..:....qwq'--__ .....JI ""MHOS/ cm Depth to Water Before PurgingJ '-\ q .':)2) Conductance (avg) 1431 and Sampling (if different) 1 8; J (;'/.20 J I Well Pump (if other than Bennet) Prevo Well Sampled in Sampling Event I Tw Y -3 R pH Buffer 4.0 LJ.O Well Depth(O.Olft): 1 \l.j1.00 Casing Volume (V) pH of Water (avg) 4" well:I .54 .zy 1(·653h) 3" Well: ..... , --"'0 __ --'. (.367h) Well Water Temp. (avg) 1 \5.1 Y Redox Potential (Eh) ..... 1 _l..);....LI'-"\_---' Turbidity ..... 1 ~_J. ...;;.,5_----l Weather Condo Ext" Amb. Temp. DC (prior sampling event)1 11i> Time l o~oC\ I Gal. Purged I q4 I Time I I Gal. Purged I I Conductance 1 1~31 I pH 16.'-\7 I Conductance I 1 pH I I Temp.oC IIS.19 1 Temp.oC I I Redox Potential Eh (mV) 1 ggl 1 Redox Potential Eh (mV) I I Turbidity (NTU) 1 :;l.1·S 1 Turbidity (NTU) I I Time I 1 Gal. Purged 1 I Time I I Gal. Purged I I Conductance I 1 pH I I Conductance 1 I pH I I Temp.oC I I Temp.oC 1 I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) 1 I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1L...-...l4wq ___ ----I Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 10-1 _'....:....1 __ ---' gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= 1 IO.gg 1 Number of casing volumes evacuated (if other than two) I I.bS If well evacuated to dryness, number of gallons evacuated 141 Name of Certified Analytical Laboratory if Other Than Energy Lab~L......:.;..J~:I...L..'AL-_____ ----I Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as Added y N specified below) Y N Type y N VOCs rn 0 3x40 ml 0 ~ HCL ~ 0 Nutrients ~ 0 100ml 0 ~ H2SO4 91 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologies 0 [] 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) r:iI 0 Sample volume 0 [3' 0 [] ;, L-hlo(,'a t If preservative is used, specify Type and Quantity of Preservati ve: See instruction Comment L-.-________ -IIDo not touch this cell (SheetName) White Mesa Mill HiM Data Workshp.p.t for Groundwater .' 2 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) r:~iS;E~Ij~ 11 FIELD DA~~~F§l~~~~~~R~~~D WATER Attachment 1 ~ See instruction Description of Sampling Event: 13 riK Gv.o-rl-e(" Go\-! 101"0+01"1"1 ;tOil Location (well name):L...1 T_W---=~~-...;:3:;.-R.~ ________ --I Sampler Name and initials: l~nf)G(" Holl;J~~.l-rH Date and Time for Purgin~,-,g",J--,t;;:;...usJ 2=-0_11 ____ --' and Sampling (if different) AliA ~~~-~------' Well Purging Equip Used:@Jpump o@ bailer pH Buffer 7.0 7 .0 Specific Conductance .... 1 _'i...:..q..:...~-,--__ --,If.lMHOS/ cm Depth to Water Before Purgin~L._O=---_----I Conductance (avg) 3 .4 '----~-------' Well Pump (if other than Bennet) Prevo Well Sampled in Sampling Event .... I _~_:/,_;tt ______ ---, pH Buffer 4.0 4 .0 Well Depth(O.Olft): IL-D ____ ...J Casing Volume (V) pH of Water (avg) 4" well:ll--o~_--I1 (.653h) 3" Well:. 0 .(.367h) 7.o} Well Water Temp. (avg) \G\.) ~ Redox Potential (Eh) ...... 1 ....;;;..3=o-"'X_---' TurbiditYL.1 ..;;..0 __ ---' Weather Condo Ext'l Amb. Temp. DC (prior sampling event)1 )7() Time 1 b6'-l3 I Gal. Purged I I ~ 0 I Time 1 I Gal. Purged I I Conductance 1 3.C1 I pHI 7 .01 I Conductance I I pH I I Temp.oC 1\9 .1:t I Temp.oC I I Redox Potential Eh (m V) I ~;Sg I Redox Potential Eh (mV) I I Turbidity (NTU) I Q I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pHI I Conductance I I pH I I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet"for Groundwater 1 of2 MiII-Groundwater Discharge Permit Date: 03/22/2010 Rev, 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged .... 1 ....,:2.:.;:.0_0-'--__ ---' Pumping Rate Calculation Flow Rate (Q), in gpm, S/60 = 1,--,-1:.....1 __ --' gallon(s) Time to evacuate two casing volumes (2V) T = 2V/Q = 1 () 1 Number of casing volumes evacuated (if other than two )1 .... _0 __ -----' If well evacuated to dryness, number of gallons evacuated 0 L--___ ...J Name of Certified Analytical Laboratory if Other Than Energy Lab!L..--.::;.D _______ ....J Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) Y N Type y VOCs ~ 0 3x40 ml 0 0 HCL ~ Nutrients ~ 0 100ml o .'. rn H2SO4 ~ Heavy Metals 0 0 250ml 0 0 HN03 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv, 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) ~ 0 Sample volume 0 Gi 0 L.h\or-; ~e If preservative is used, specify Type and Quantity of Preservati ve: Comment ~ See instruction Arr;ued on .si+~ G\t O~O. ,""rn1a o..,,~ 6-Gl;rl'f\ fr-c:s.en-t-+or ,<nSCI.+e. 'R:,,~£\h be~~17 -0:..+ Ob~. ?1,A,..~'Ca S,O Cn..ll ons of A";" wo,,+e., bQ G-,,)IoyU J.oo.f' wc..hr, /.Jo {y"JlonJ or DI LU~+~r. R;I'\So..+<: Gflaea (""~ So..YV)plc:: GoJlec.+eJ. ~J-O~L..).s. L-e~T ~;h .. ",1 oli5> L--_______ ----lIDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 t:] 2 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan {QAP} OENISOJ)J~ [;-.-~-ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 ~ See instruction MINES FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 3("iA C;h~o.l'"ter Ch\oro+~(1"'\ ;2.01\ Location (well name):L..1 T_W_L.\_-~-'--________ -' Sampler Name and initials: 1-rt.\/II1u· Ai> 1I,'J~JTlf Date and Time for PurgingjL..~_I_I_I_I_:A_o_I_J ____ --I and Sampling (if different) .IV/A L..-_______ ~ Well Purging Equip Used:I'tJ Ipump o@ bailer Well Pump (if other than Bennet) Sampling Event IQu.CA.,k 8 c.\-'lo("o::to(W) I fJlW_L/ Prevo Well Sampled in Sampling Event 1-..-_______ ---1 pH Buffer 7.0 pH Buffer 4.0 Specific ConductanceL.1 ---.:..~q_~ ___ ----II f-tMHOS/ ern Well Depth(O.Olft): 1 11.2. .00 Depth to Water Before Purginm 6'1. 9 I 4" well:1 2 7.L18 1(·653h) 3" Well: <' (.367h) L...-___ --I Casing Volume (V) Conductance (avg) 2..1...\'17 pH of Water (avg) Well Water Temp. (avg) 1 17.'31 Redox Potential (Eh) 1 ~$b Turbidity .... 1 _0 __ ----..11 Weather Condo Ext 'j Amb. Temp. O( (prior sampling event)l '30' Time 1 lJ1q 1 Gal. Purged 1 1 Time 1 1 Gal. Purged 1 1 Conductance 1 ~:l9:Z 1 pH 1 6.32 1 Conductance 1 1 pH 1 1 Temp. DC I 17-31 I Temp. DC I I Redox Potential Eh (m V) I :256 I Redox Potential Eh (mV) I I Turbidity (NTU) I 0 I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pH I I Temp. DC I I Temp. DC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged L..I __ O ___ ----' Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1-1 _8_"_0 __ --' gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= 1 0 1 Number of casing volumes evacuated (if other than two) o If well evacuated to dryness, number of gallons evacuated o Name of Certified Analytical Laboratory if Other Than Energy LablL.._N_IIt ______ ----' Sample Taken Sample Vol (indieate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y VOCs ~ D 3x40 ml D [29 HCL IZI Nutrients rn D 100ml D ~ H2SO4 ~ Heavy Metals D D 250ml D D HN03 D All Other Non Radiologies D D 250ml D D No Preserv. D Gross Alpha D D 1,000 rn1 D P HN03 D Other (specify) m D Sample volume D ~ El Ch\c>r;~~ If preservative is used, specify Type and Quantity of Preservati ve: See instruction Comment ihr;"e.ck on si+c:.. 0..1 1308 . -r;;nl'l~T M~ G-c;..fri'l f'r'e'scn+ ~(" SQmpJ.~ e.venf. }oo~ ~t:f+h +0 \.Uqicr} SctW}PJc.) we('( (.ol)ec.~~ ~+ J55, wo..+cr WCAS c...leo.r . le.f\-~i1-~ Cl\T-1318 '--________ ....IIDo not touch this cell (SheetName) White Mesa M.ill Field Data "Worksheet for Groundwater N D D D D D ~ 20f 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 r:-NISON~, ~--~-~ f~.~~E~~ FIELD DATA WORKSHEET FOR GROUND WATER WHITE MESA URANIUM MILL Attachment 1 ~ See instruction Description of Sampling Event: 13 r 3\ Q\ACA.('+~r Ch lorl>~6('M Q.o II Sampler Name and initials: lj;rlYle,(' HoJhJ~/JJ} .. Location (well name):1 'VJt..\-5 ~~--~----------------~ Date and Time for Purgin~ ~ II G./:J..CJ) I and Sampling (if different) .... 1 :::..g/:.....;1..:..7~/_l}.._D,..;....II ______ --1 Well Purging Equip Used: 00 pump or@] bailer pH Buffer 7.0 Specific Conductance .... I --!.~...:..q ...... 1 ______ --1If!MHOS/ cm Depth to Water Before Purginm 2b. DS 1 Conductance (avg) I L.14 Well Pump (if other than Bennet) 1 6-,...v.ndJ'o.s Prevo Well Sampled in Sampling Event I J1A .. )i1 .... ~ pH Buffer 4.0 1...).0 Well Depth(O.Olft): 1;2,.0. dc) Casing Volume (V) pH of Water (avg) 4" well:I ' Y 1.. 75 1(·653h) 3" Well: ...... _0 __ --'. (.367h) Well Water Temp. (avg) 1 15.:l?.. Redox Potential (Eh) L-I 3;;;;..g;;;;..7 __ --1 TurbiditYL-1 .....,;;15;;..,.9...!..-_--1 Weather Condo Ext'l Amb. Temp. O( (prior sampling event) I '1 /) Time 10335 I Gal. Purged I f,,, I Time I Og3~ I Gal. Purged I "1 '"1 I Conductance I 1:b?.L} I pH I C; .;2.1 I Conductance I lb)g I pH I (;.,,1'3 I Temp. DC I IS.;l..~ I Temp. DC I lS.~ I Redox Potential Eh (mV) I 3QIO I Redox Potential Eh (m V) 1 38~ I Turbidity (NTU) I 15~.1 I Turbidity (NTU) 1 1~~ .. o I Time I O&yo I Gal. Purged I ~& I Time l og41 I Gal. Purged 111 I Conductance 1 161~ I pH 110.<23 I Conductance I )1.;0:3 I pH It.R) I Temp. DC I '5.~ I Temp. DC I lS.~ I Redox Potential Eh (mV) I :!>33 I Redox Potential Eh (m V) 132> I I Turbidity (NTU) I I~o.1 I Turbidity (NTU) I 1 Co'3·1 I White Mesa Mill "Field Data Worksheet for Groundwatei ,. 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged L..I _94..:....L.. ___ ---I Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1-1 _..:....!..l) __ --I gallon(s) Time to evacuate two casing volumes (2V) T = 2V /Q = 1 I. 54 1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~L.....;..jtI_/ __ ~=--_____ ---J Sample Taken Sample Vol (indicate Filtered Preservati ve Preservative Type of Sample if other than as Added y N specified below) Y N Type y N VOCs []. 0 3x40 rnl 0 [£ HCL ~ 0 Nutrients [) 0 100 rnl 0 [] H2SO4 ~ 0 Heavy Metals 0 0 250 rnl 0 0 HN03 0 0 All Other Non Radiologies 0 0 250ml 0 0 No Preserv. 0 [] Gross Alpha 0 0 1,000 rnl 0 0 RN03 0 0 Other (specify) CiI 0 Sample volume 0 I:S 0 6) Ch\o(';c\(. If preservative is used, specify Type and Quantity of Preserv ati ve: Comment ~ See instruction A(li\l~6." ()(I.s\t~ 0..1-03:;"7. -r;...nnec q()~ &~(("fl pt"~ent +0 'F"'f'j<-"""fWy .... s. P\A(,~~ btJ~n g..1- og3;2.. fv..(~-e;o. \).)dl-tor 0\ )-oto.l ~ "t l'Vl itllAte.S, ~t\+er stlA.rte~ O\A.to-.. M;/ku.. wb.;+c. huI+- cleMe'q. ?\Ar~c.. ~l1de~ c?.t 08111. D<p+-~ 10 Wodc.r ~fhr p\A~~ ~o..~ 5(,..YI.'-J Lf!-tt .5lfe 0.-1-O&'~ Arr;'Jd, on ~I+C. 01.+ ObllO. I~"n<.r CA"tA. c;.."I(r :" ? rc~"Cn} +1> <:o)Jed-.s1A;vJp)-e~. O~ p+h 17> W&l."hr S&\Mpk.s vJ~(~ bG\;l<~ O\t ObY.5. Le+-t ..sih·~-:t Ob.50. L...-________ ..... IDo not touch this cell (SheetName) White Mesa Mill Field Data Workshe'et for Groundwater 2 6f2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 5ENISOJ)~~ WHITE MESA URANIUM MILL Attachment 1 ~ See instruction MINES FIELD DATA WORKSHEET FOR GROUND WATER , . .' --..-... Description of Sampling Event: 1 '3 rb\ Q \.lo..da to: h I or D'f'D( fI') ;;;2.0 II Location (well name): ..... -r_W_'-l_-_.b _________ ----' Sampler Name and initials: I-ro.nner HO II,GJI~ITII Date and Time for Purgin~ ...... ~:;..;./_I_~..:.../;;.._C_)I ____ ......J and Sampling (if different) 1 &1)7/ /).() I} Well Purging Equip Used: I][J pump or@] bailer Well Pump (if other than Bennet) 1 GrlAl'lc.l:fOs Sampling Event 1 Qv.(.t.rh.r1.!:! G), 'o("~orlV"\ Prevo Well Sampled in Sampling Event ..... 1_T_W_I1_-_S ____ ---' pH Buffer 7.0 1.0 Specific Conductance ..... I.....:9_q....;..~ ___ __'I!-lMHOS/ cm Depth to Water Before Purgingj 70.3'1 Conductance (avg) LJ 173 '--~~~ ____ ......J pH Buffer 4.0 t4.D Well Depth(O.Olft): ...... 1 q.:.....'_. ~_O __ ----' Casing Volume (V) pH of Water (avg) 4" well:l 17 .73 1(·653h) 3 " Well:...... _D __ ----'J367h) Well Water Temp. (avg) IS. b~ Redox Potential (Eh) 1-1 ..::3~(;;.;..~ __ ....J Turbidity I ...... Y..;...:2_0 __ ......J Weather Condo Ext'l Amb . Temp. DC (prior sampling event)1 :;;lOo Time 1 0'12.'1 I Gal. Purged I :l.7 I Time I I Gal. Purged I I Conductance I L\l]t> I pHI b-l..b I Conductance I I pHI I Temp.oC 1 15·62> I Temp.oC I I Redox Potential Eh (m V) I Jb~ I Redox Potential Eh (mV) I I Turbidity (NTU) I \..l~o I Turbidity (NTU) I ) Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp.oC I I Temp.oC I I Redox Potential Eh (m V) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet forGroundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged I ;;).7 . ..5 Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = L...I _ll!.....-_----I gallon(s) Time to evacuate two casing volumes (2V) T = 2V/Q = I 3.2.2. I Number of casing volumes evacuated (if other than two) I ).55 If well evacuated to dryness, number of gallons evacuated 1 ~/.5 Name of Certified Analytical Laboratory if Other Than Energy LablL-.tJ._'IA'--______ --' Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as Added y N specified below) y N Type y N VOCs ~ 0 3x40 ml [j M HCL , -f1 0 Nutrients ID 0 lOOml 0 ~ H2SO4 ~ 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) IN 0 Sample volume 0 15 0 ~ L:'-' \O(,J e If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction '--________ ...JIDo not touch this cell (SheetName) White Mesa Mill .' Field Data Worksheet for Groundwater 2 of 2 PROPERTY BOUNDARY \\ \\ \\ // // // // // // /1 'I /, II /1 --.::::-- MW-01 • ~5 ~ TWN-7 MW-18 • ~ TWN-18 ~ TWN-3 ~ TWN-6 ~ TWN-8 ~ TWN-15 ~ TWN-10 ~ TWN-9 PIEZ-1 " MW-19 • PIEZ-2 " ~ TWN-11 ~ TWN-14 L (e ./ ---11 ~ -,I I-r( ~ \1 // 1\ // ~ //.-~=~- N o SCALE IN FEET EXPLANATION MW-20 • perched monitoring well TW4-19 0 temporary perched monitoring well PIEZ-1 perched piezometer I;l ·TWN-1 temporary perched nitrate ~ monitoring well MW-34 perched monitoring well installed -¢-August/September, 2010 MW-36 ~ perched monitoring well I _II_-l I\ ..... "'il ?()11 CELL NO.1 MW-2 TW4-25 MILL §ITE~ '=~==;; TWN-o 4-21 N-4 ., PIEZ-3 " MW-02 • ~===:F===JIl======-~O~TTi:WJ,4t._2~2~ OTW4-5 MW-B5 -¢-, MW-~ MW~3 -¢-- MW-03 • MW-20 • 3000 ., CELL NO.2 wildlife pond HYDRO GEO CHEM, INC. MW-17 • 33 APPROVED SJS M -26 TW4_1!PTW4-9 • 0 OTW4-3 OTW4-12 OTW4-1IbTW4_11 OTW4-13 TW4-7~~i.8 OTW4-1 OTW4-40TW4_14 TW4-23 OTW4-6 o OTW4-26 PIEZ-4 " .7 / .7 1£------=-..=-.7 ---- # PIEZ-5 " T378 T38S MW-22 • II ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ SITE PLAN AND PERCHED WELL LOCATIONS WHITE MESA SITE DATE REFERENCE H :/718000/nov11 Iwelloc11 .srf ( o ., FIGURE A-- Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 ~~N:~NI)~~ L MINES FIELD DATA WORKSHEET FOR GROUND WATER WHITE MESA URANIUM MILL Attachment 1 ~ See instruction Description of Sampling Event: 1 ?/o.. Qv,(Arh.r Gl1loroforM .20 II Location (well name):L-I,_Ul_L1_-_7 _________ ---I Sampler Name and initials: 1 ~l!l)e.-He II ,(Ja.~/T d Date and Time for PurgingJ ..... 8_I_J_7_1_.::2._0_'_1 ___ ---' Well Purging Equip Used: [![]pump o@ bailer Sampling Event 1G>v..Q.r+~("h1 d\\o('o"toc"1'n pH Buffer 7.0 7.0 Specific ConductanceL..I_Q_9_9...L.-__ ----'1 [.tMHOS/ cm Depth to Water Before Purginm b 7, b:S Conductance (avg) and Sampling (if different) 1 lS/lg /~OJ J Well Pump (if other than Bennet) l6-rv.ndfoS Prevo Well Sampled in Sampling Event l-rw (..{ -7 R, pH Buffer 4.0 q.O Well Depth(O.Olft): 1 1;2.0. DO Casing Volume (V) pH of Water (avg) 4" well:1 3'1.18 1(.653h) 3" Well: ..... , _O __ --',(.367h) C;.'67 Well Water Temp. (avg) 1 IS·2iS Redox Potential (Eh) 1-1.2_6_7 __ -1 Turbidity 1 17. 9 Weather Condo Ext'l Amb. Temp. °C (prior sampling event)1 ~I· Time 109QI 1 Gal. Purged 1 11 f C· 1 Time 1 1 Gal. Purged 1 1 Conductance 1 1 b'i b 1 pH 1 c, . .s1f 1 Conductance 1 1 pH 1 1 Temp. DC I p;.;Xg I Temp. DC I I Redox Potential Eh (mV) I ?-.bJ I Redox Potential Eh (mV) I I Turbidity (NTU) I 17.Q I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pH I I Temp. DC I I Temp. DC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field bata Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged ..... 1 ----'-7....;;;;:3'--__ ---' Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = ...... 1 _'_1 __ ---' gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= 1 10 .2 ' 1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated 73 Name of Certified Analytical Laboratory if Other Than Energy Lab~L..tJ_/_A _______ ....I Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as Added y N specified below) y N Type y VOCs [gf 0 3x40 rnl 0 ~ HCL 'g] Nutrients ~ 0 100rnl 0 ~ H2SO4 '[] Heavy Metals 0 0 250 rnl 0 0 HN03 0 All Other Non Radiologics 0 0 250 rnl 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 rnl 0 0 HN03 0 Other (specify) ~ 0 Sample volume 0 ~ 0 , .. L h \or-;Je If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction Arri\lea 0(\ ,Sit<~} DZSSb.-r;.nner Mtk G-I)((it'l prc~ef1+-+0 plM".j<:: jWLl-7, ?\A~C!. b't)Afl 0.1- biSSGf. ?~(~c:~ well .\0(' 6... +ot~\ of " M;t)v..tLS ~t1tA 1-15 :S~cond.s. t\.,r~;~~ well Jt'V\ I. ~ lJ.:tc(' \"J~ \'Y10S~ c.\~o.( ~ Pv..('~~ ~rtde~ o-t O~ Of,. L. -e+-t $ n ( 0.. t c~ I D. \j Ar("\\Je~ on ~ji~ A.t Ob3-!. -r;;:n"cr ~flJ.. b--~((; r. p,..e~er1} +c> coiled sc.J'YlfJes-Dep+h +~ V-)p..-tu Lo\)o..s. ~8'·YS . .s~lY1plc,) were:, Goll~G+Ctl G\.}-Ob3b. LefT-~/~+(, "".if-Ob:sf5 L..-_______ ---IIDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for'Groundwater N 0 0 0 0 0 ~ 2 of2 Mill· Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 I~ENI50~l)j j l iJ!..NES FIELD DATA WORKSHEET FOR GROUND WATER WHITE MESA URANIUM MILL Attachment 1 ~ See instruction Description of Sampling Event: 1 '3 .. 0; Q V\()..rh.(' L. \·d 0 ro;::-O(yY'\ 2,.0 \ \ Location (well name):L..1 I-'-W_4-=--.....;I_R ________ ---I Sampler Name and initials: I=rMI'\~(, HolluJ\~/,t-t Date and Time for PurgingjL.._~_1_17_/_::z._0_J ' ____ .....1 and Sampling (if different) L...-_N._y_A-______ ....I Well Purging Equip Used: [!!]pump or@] bailer Sampling Event 1 Q'v\().(+-erh\ Lh lorofo('W) pH Buffer 7.0 Specific Conductance 1-1 _q_1'--'l ___ ---I1 I-tMHOS/ cm Depth to Water Before Purgingj'I-_D __ ---' Conductance (avg) 2..g Well Pump (if other than Bennet) I -r~'1-( J Prevo Well Sampled in Sampling Event '-________ ....1 pH Buffer 4.0 q.O Well Depth(O.Olft): L-I _0 ____ -' Casing Volume (V) pH of Water (avg) 4" Well:~(.653h) 3" Well:~(.367h) Well Water Temp. (avg) 1,;2..5. L\'1 . Redox Potential (Eh)1 '3,~~ TurbiditYL-1 _0 __ ----1 Weather Condo Ext'l Amb. Temp. DC (prior sampling event)1 ~I 0 Time 1 OS t1S I Gal. Purged I I 8' () I Time I I Gal. Purged I I Conductance I ~.6. I pH I 7.~D I Conductance I I pH I I Temp.oC I :;2.5. LJ q I Temp.oC I I Redox Potential Eh (mV) I 3~ I Redox Potential Eh (m V) I I Turbidity (NTU) I Q I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pHI I Conductance I I pHI I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 . Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged L..I_;L._O_O ___ --I Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = L-I __ 11 __ --' gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= I N/A I Number of casing volumes evacuated (if other than two) D If well evacuated to dryness, number of gallons evacuated b Name of Certified Analytical Laboratory if Other Than Energy LabIL.._~_~A'"""'----______ ---' Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as Added y N specified below) y N Type y VOCs rn 0 3x40 ml 0 09 HCL ~ Nutrients rn 0 100ml .D C!9 H2SO4 ~ Heavy Metals 0 0 250ml 0 0 HN03 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. D · Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) ,~ 0 Sample volume 0 ~ , 0 G h lor~a-c If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction Arr'I'Je~ 01"1 s..;te &\.1' ct.;).!:" """",""'Cf'" o..n"'-6-~('r:" rres.e.I1t--to, 6()~t:.\-t<::. Kin's4..te be;)!)." o,.f- o ~'30, 'f\"l" ~~~ f,O G-~lIoYls of fh.; J. lN~t-u-; SO &(l.llon.s of ~oo. P (.Jo,.1-Cf') \00 {,-O\llotJ.s of DT W!A..1-er . R; .,..so . .t~ en t\eJ. "'} b8SO, s,I?\I'flP le,S \Nef"e. (c> ll<c.+ed. ,J 0 g'11 -Left-si-te.~} Ogs:S '---________ --'IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 " ~ 2 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) [OENIS~Ni)~~ ATTACHMENT 1 Attachment 1 ~ See instruction WHITE MESA URANIUM MILL MINES FIELD DATA WORKSHEET FOR GROUND WATER b ._. Description of Sampling Event: 13" '" Q\Ao..rte.r Gh lorJorr>1 .:to II Location (well name): .... 1 'i-,--w_l._\_~ _8 _________ --' Sampler Name . and initials: r-I-r;--:(),:-n-n-e.-r~:nrto-;J'-J ,-jJ'-~-/T-:--R=-------' Date and Time for Purginm ~/l-5/.;2.0J I and Sampling (if different) 1 .... :::;,CJ/:-I:...::'L.;!2..=-D ..... JI ____ --' Well Purging Equip Used:rn=!pump o@ bailer Well Pump (if other than Bennet) l6-r U\lJ ({-P()..S Sampling Event 1 Q\k~l'h(" 1~ Co ~ I o rotor M Prevo Well Sampled in Sampling Event IL-I_W_y_--1S _____ --' pH Buffer 7.0 7 .0 pH Buffer 4.0 Y.O Specific Conductance IL-----L~~q '"'--__ -11 ""MHOS/ cm Well Depth(O.Olft): 1 125.00 Depth to Water Before Purgingj fob. b I 4" well:I 38.1;2. 1(.653h) 3" Well: D (.367h) '---------' Casing Volume (V) Conductance (avg) pH of Water (avg) Well Water Temp. (avg) 15 .07 Redox Potential (Eh)IL.....;....)Y_' __ -I Turbidity 1 ,Q.C1 . )~ Weather Condo Ext'l Amb. Temp. O( (prior sampling event)1 ~1° Time I 13Y3 I Gal. Purged I 5:> I Time I )3yQ I Gal. Purged I 66 I Conductance 133&5 I pH I b.YS I Conductance 1:33Ja I pH 1 6 .l.d.5 I Temp.oC I )5:.11 I Temp.oC I IS.o 7 I Redox Potential Eh (mV) I P15 I Redox Potential Eh (mV) 11Y:1: I Turbidity (NTU) I ;,.tZ.1 I Turbidity (NTU) 1 ~1.;> I Time 1!)t{5 I Gal. Purged I 77 I Time 113cH) I Gal. Purged I &F I Conductance 133gj I pHI G.% I Conductance I 3.:5~ 1 I pH I t::.cp I Temp.oC 115.oQ I Temp.oC 115.Ob I Redox Potential Eh (m V) I )1:11 I Redox Potential Eh (mV) I Itto I Turbidity (NTU) I .2..Q .l I Turbidity (NTU) 13lJ.O I White Mesa Mill .. Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged .... 1 ~g.>::::g ___ ----, Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = ...... 1 _1 ........ 1 __ ---' gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= 1 b.'t3 1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labf .... _M----:.'IA""--_____ ----' Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as Added y N specified below) y N Type y VOCs ~ D 3x40 rnl D ~ HCL l'B Nutrients B D 100 rnl D L1I H2SO4 [2 Heavy Metals D D 250 rnl D D HN03 D All Other Non Radiologics D D 250 rnl D D No Preserv. D Gross Alpha D D 1,000 rnl D D HN03 D Other (specify) Il" D Sample volume D B D L\, \ or·\~(. If preservative is used, specify Type and Quantity of Preservati ve: Comment ~ See instruction A(r "\Je~ on sit~ 0.1 1333. J:11T'lt:( b-rl'" &o.rr Or) ?('esc:nt +0 f\J\(je -r\A)L.:J-~. r V\( ~ be!l~~ "'\ 13%.? "":3eA I»eli -tor ... +ohl of g l"lin",+<.S. ?~, <-enJe~ "t )'34~ ~~+C( ~ l'V10~J!j deo.r throujhov,t +he p\A(~e. D~p+h t6 ~o..~r' o..~( Dv.r~-l ~4~ I). ~3. Lt:+t ~I i-!.. CA.t Y35Q., } -J 'R~o." Po.\(VI1::1' on si+<... to c.oll~(.t .so.T'lpks. Depth 1-0 l.)c(t-cr lJCtj f,7.JD SlXrY\f'\G~ wer(, b.~1t'J. ~f>d-Lolkctc:A (;\1" 11..\.50. '--_______ ----'IDo not touch this cell (SheetName) White Mesa Mill ~i"lrl n~t~ wnrksheet for Groundwater N D D D D D ~ -2 of 2" Mill -Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) Date: 03/22/2010 Rev. 6 Attachment 1 ~ See instruction Location (well name):IL.. _'"T_\N_y_-q~ ________ -J Sampler Name and initials: 1'jlA.nn~(' Ao/J,'J't!;/-rH Date and Time for Purgingjl-g_J_IS_I :2_0 _11 ____ --' and Sampling (if different) $!Ib/:;"O\ I '-=~~-----~ Well Purging Equip Used: [J!]pump o@ bailer Well Pump (if other than Bennet) I Grv.nll(c,,S Sampling Event p",o.r+ed~ c.h lo("of~( YI1 Prevo Well Sampled in Sampling Event 11....,_I,..)_'-1_-_g ____ --' pH Buffer 7.0 /.0 pH Buffer 4.0 g.o Specific ConductanceL...1 '}_~--,i'---__ ----II/-tMHOS/ cm Well Depth(O.Olft): Depth to Water Before Purgind S3. tto Casing Volume (V) 4" well:1 Lt3.1G 1(·653h) 3" Well: 0 (.367h) L....-__ --' Conductance (avg) pH of Water (avg) Well Water Temp. (avg) I 15,3Lf Redox Potential (Eh)IL...:h_g_1 _--' TurbidityI 1;2..Y .55 Weather Condo Time IIY33 I Gal. Purged I 77 Conductance 1 ~47L\ I pH I i: .?-;!.,. Temp.oC 1 \5·~ I Redox Potential Eh (mV) I :;L!:Ii I I Turbidity (NTU) I ~1.5 I Time 11t.135 I Gal. Purged I 1(1 Conductance I ~L..\ l' I pH I C) .;r:z: Temp.oC I \5 .'3"3 I Redox Potential Eh (mV) 12.77 I Turbidity (NTU) I tH.,} I White Mesa Mill Field Data Worksheet for Grounowater I I I I Ext'l Amb. Temp. O( (prior sampling event)1 3 0 6 Time I....I'_Lj3_Y~_...J Gal. Purged IL.:~~~~_----I Conductance 1L...:2_q_7_4_----' pH I b.~~ Temp.oC I IS .~ Redox Potential Eh (mV) 1'-2 .;.....6.....;9 __ ...... Turbidity (NTU) Time I /c13' Conductance l!Zq 78' Temp.oC 115.31 1 ).;2L1 . J I Gal. Purged ..... 1/ ...... 1 d"--_--' pH Ib.!W\ Redox Potential Eh (mV) 1....12_7..::::3~_--I Turbidity (NTU) I l~7.0 1 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1...1 -I.lJ~()~ ___ ...J Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = IL..--.....:..l.!...l __ --' gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= 1 7.f54 1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~L..:M,--,-,'//t-,--______ ----, Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as Type Added y N specified below) y N y N VOCs ~ 0 3x40 ml 0 qI HCL 1$ 0 Nutrients I'll 0 100ml 0 01 H2SO4 lSI 0 Heavy Metals 0 0 250ml 0 0 RN03 0 ,0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 RN03 0 0 Other (specify) 11J 0 Sample volume 0 ~ 0 6J G\'\o~,A( If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction A1"("i~'C:o. on s."tc 01.1-'~. T"rlncr' D.IltA ~ii1((:1"\ fr~5efrr+O pu.r\)< TW!_~. Pur c b~'I.1l 0..+ lLj~~. '?\),r~(~ \pod \ +0(, /1... +oh.J c.f )0 M,1)IA+t'~. \V6.:h:r hc..~ "-j:+}!c ~ . .s~6Jar t~ it. ?LAr~e el'\d(a '" r 143'. O-ep1-h 10 (At<:r 11-.~~1 f>"'ej"C \»C\~ -7). ~5. Let} S;+e iA.t 14YL/. 'Rj/l"r\ Pl1\1~er pre~Cf)} to colle.ct-SQYl'Iple$. p~pt~ +0 Wetter vJ4~ 5~.~. ~(1,Mp\e~ \,)<rc' l::n;, i 1('~ <At J Y.?.1. L...-________ ....... IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheetlor Groundwater .' 2 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 I :E~:~J)iil ,.>\).l~~IN~S ~_J FIELD DATA WORKSHEET FOR GROUND WATER WHITE MESA URANIUM MILL Attachment 1 ~~ See instruction Description of Sampling Event: 13r d\ Q\Ao..rfe r ch loro-forM ~ 0 II Location (well name ):1-1 _'T_W_Ll_-_IO ______ ---'-__ ----I Sampler Name and initials: I I~nrlu ~o'\:JfA.:1/'-1i Date and Time for PurgingjL..:~::;..;....I _1 (,.....:./...:~_\_I ____ -..I and Sampling (if different) 1L...;~;::;.:./....:..I7...:...;/.;...;;:;..._D_I;..:..I ___ ----1 Well Purging Equip Used: [IDpump o@ bailer Well Pump (if other than Bennet) I -rWL\-;;u. Prevo Well Sampled in Sampling Event 1-________ --' pH Buffer 7.0 1L.....-7_._D ___ ....J pH Buffer 4.0 Lto Specific Conductance .... 1 q_~_·~"'--___ -'lftMHOS/ cm Well Depth(O.Olft): ..... 1 \_'_"_0_0 __ --' Depth to Water Before Purging/ E.b ,0 \ . 4" well:1 ~.9() 1(·653h) 3" Well: 0 (.367h) '--------' Casing Volume (V) Conductance (avg) 7)D.~ pH of Water (avg) '.15 Well Water Temp. (avg) 1 16·\·(5 Redox Potential (Eh) 1 .... 3_I..'_<X __ --' Turbidity ..... 1 _)3_Zl __ --' Weather Condo Ext'l Amb. Temp. °C (prior sampling event}IJ..'1 D Time I llY) I Gal. Purged I I::,f} I Time I I Gal. Purged I CC · I c"b Conductance 111O.q I pH I ". \5 I Conductance I I pHI I Temp.oC I ((;.Y3 I Temp.oC I I Redox Potential Eh (m V) I 3 cIl I Redox Potential Eh (mV) I I Turbidity (NTU) I 1'3.b I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (m V) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill , Field Data Worksheet for Grouridwater 1 of 2" Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged .... 1 ---.;;;<;;....,, ___ ---1 Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = ,--I _,_, __ ---' gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= 1 (,.s? 1 Number of casing volumes evacuated (if other than two) 1 \.S3 If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labl .... N.-'v:...;A...:..-______ .......I Sample Taken Sample Vol (indicate Filtered Preservati ve Preservative Type of Sample if other than as Type Added y N specified below) y N y VOCs 1tl 0 3x40 ml 0 ~ HCL lSI Nutrients fl] 0 100ml 0 rll H2SO4 ~ Heavy Metals 0 0 250ml 0 0 HN03 0 All Other Non Radiologics 0 0 250ml 0 0 NoPreserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) rfl 0 Sample volume 0 ~ [] Ch \De; ~e. If preservative is used, specify Type and Quantity of Preservative: ~ See instruction Comment A«';\leo.. on !.i-te. ~.1-'~L -r;."fJe.f" M\d.. G-a...rr:{1 f>f'ese tlt h pv..r~e J'W~~I{), Pv.'{'~c:. bejo.n ~+ '~~7. ?lJ\r~e~ \Nell +or a... +o-k,1 of G:. 'Mi(l""t~~. fv.r~~~ Well <kfj '. l.A)o.-ter W~~ c.le.o... ~ 1'\,f,r~e. -e"h4 0-.'" 1~Y.3. Ld+ ~A<. A.~ U l.\S. A(fi\lt~ on ~i-tc: 0-+ 0131£. "'-;'l1ll~(~f\t.I.. (ru..r(;,., preHI"l+ +0 ,,+Hd~J (olla1-.s{'(fI1pJ('~ . .Dept~ 1-0 \Nctto'" W"~ 5'-.3.5 Sl.Il"\p\t'..) wert c.oll-ec:tc& pJ 01'15. L~-F'} .s;r(' ,,+ 07Y1. L..-.. ________ -JIDo not touch this cell (SheetName) White Mesa Mill Field'Data Worksheet for Groundwater N 0 0 0 0 0 1&1 2 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 1::.soJ)---.n1 L~INES _~ FIELD DATA WORKSHEET FOR GROUND WATER WHITE MESA URANIUM MILL Attachment 1 ~ See instruction Description of Sampling Event: ::, r3: Q",,,,-,..t<,.. Gh Ie:) re:)\i)rrv1 .20 1\ Location (well name) :L-I-r-.:...-w-=---y.:....-_l_l ________ ---I Sampler Name and initials: I"-;nner Ho 11/'J~/-r}t Date and Time for Purging/J.-_g_1_1 b_/._.9-._0_1_' ___ -----' Well Purging Equip Used: [!!]pump or@] bailer pH Buffer 7.0 7.0 Specific Conductancel ..... _Q ..... 49...L...-__ -JIt-tMHOS/ cm Depth to Water Before Purgin~ 57.55 Conductance (avg) lb~J and Sampling (if different) gj 17 /;;.. 0 1\ Well Pump (if other than Bennet) I Cr-rV"-n,,{F'o.S Prevo Well Sampled in Sampling Event I ,W LJ -~I pH Buffer 4.0 Well Depth(O.Olft): I \00.00 Casing Volume (V) pH of Water (avg) 4" well:1 :;2.7:1 J 1(·653h) 3" Well:L-. .....;~~_---I. (.367h) b .37 Well Water Temp. (avg) I 15 .~l..{ Redox Potential (Eh) ..... 13=o::;..Q-'--_--' Turbidity ..... 1 .....;;lg;..;,..;,....1 _---' Weather Condo Ext'l Amb. Temp. O( (prior sampling event)L-13_I_o_...J Time 1 1L\~ I Gal. Purged I 77 I Time I I Gal. Purged I I Conductance I I f/-\l I pH I ro .37 I Conductance I I pH 16' I Temp.oC I \S.',29 I Temp.oC I I Redox Potential Eh (mV) I ~S4 I Redox Potential Eh (mV) I I Turbidity (NTU) I )2$.\ I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pH I I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1-1 _7~7.L....-___ -' Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1..-1 -..:...11:.....-_----' gallon(s) Time to evacuate two casing volumes (2V) T = 2V /Q = 1 5. 03 1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated .... 1 ...:..7 ...... 7"-_---' Name of Certified Analytical Laboratory if Other Than Energy Labl'-_Al_'/_A"--_____ ---' Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y VOCs ~ 0 3x40 mI 0 r:i HCL IE Nutrients ~ 0 100mI 0 [] H2SO4 I]- Heavy Metals 0 0 250 mI 0 0 HN03 0 All Other Non Radiologics 0 -0 250 mI 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 mI 0 0 HN03 I, 0 Other (specify) Qf 0 Sample volume 0 ~ 0 If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction Arr;\le~ on ~;h 0-+ 141~. """I'II1e.r "n~ G-Q.r";n pre.scfl~ +ll pv.\""~~ TWLj-)J. Pv.'~r: bej<:ln ~t lY2..1. P\A.('5etA ",,(:\1 J'c:.r ~ .f-o·h..l of' 7 t>'1ir1v...+es . wo..+a WG\...S cleo.r -f-hrot.tjho\A.J.- t-h~ ?v.r~<. Pur~tc.l ~ell J.rj I. P",r~-e ended G\t !Y2X. It'ft ,s,+! 0..-1-}Y33. A(("·\)·d.ol\ Si1-t:. "'+ o~o.~l...-r(AM-e.~o-(\A 6-"o.r6f1 ?('.e~e.(lt +0 c.oll..e.d-~~rV)ple~. ):::>ept~ to \.UC\.t<<' \NQ..::, Sg .7;(. So.t'1pk~ V-l~(c 60\.le~ At-o go;. \...e.-R-.s;h 0..-)--08'ID '--_______ ---lIDo not touch this cell (SheetName) White Mesa Mill Field D;i'ta Worksheet for Groundwater N 0 0 0 0 0 r:8 2 of; Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 1:~~~jll L.iJtNES . FIELD DATA WORKSHEET FOR GROUND WATER WHITE MESA URANIUM MILL Attachment 1 ~ See instruction Description of Sampling Event: 13 ra Q",o..("h( CJ\)orc)Of~(r¥l .:2,01/ Location (well name) : ... 1 _T_\t.l_'-l_-..:....12.. ________ ----' Sampler Name and initials: l -r;,n'flG .... ~c')I1;Ad In! Date and Time for Purgingj'-'~::;..:/_I.;....5_J_~_O_I_J ___ ----' and Sampling (if different) I &/1,(,/..2.01) Well Purging Equip Used: [![jpump or@] bailer Well Pump (if other than Bennet) Prevo Well Sampled in Sampling Event 1Io-..1_W_L1_-_.J ____ ----' pH Buffer 7.0 pH Buffer 4.0 L).O Specific ConductanceL.-1 4..L.Q....;.,4..l.....-__ ----'I/-tMHOS/ cm Well Depth(O.Olft): Ilbl-5 D Depth to Water Before Purgingj 34.7() Casing Volume (V) 4" well:1 QO.55 1(·653h) 3" Well: c> (.367h) '---------' Conductance (avg) 1L--,q..::.~=B_.~_C> ____ ---, pH of Water (avg) b./l Well Water Temp. (avg) I ILI.K() Redox Potential (Eh)L.-1 L\~lql--_......I Turbidity I y .07 Weather Condo Ext') Amb. Temp. O( (prior sampling eventll 14 b Time 1090.? I Gal. Purged I 5S I Time 1 090) I Gal. Purged I bb I Conductance I q~·o I pH I fo.70 I Conductance I 42>$·7 I pH I {;,.72 I Temp. DC I 1'i .3 () I Temp. DC 114 ·z1 I Redox Potential Eh (m V) I L'30 I Redox Potential Eh (mV) I :l~A. I Turbidity (NTU) I q.l'5 I Turbidity (NTU) 1 1..1 .0 1 Time I o1oy I Gal. Purged I 72 I Time I D9{)5 I Gal. Purged 11ft I Conductance I 93q.J I pHI b ·n I Conductance I '137.25 I pH I b.73 I Temp. DC 11Y .ZO I Temp. DC I 'Iq ·31 I Redox Potential Eh (mV) I c\lq I Redox Potential Eh (mV) I 91D I Turbidity (NTU) I eLl I Turbidity (NTU) I ~!~ I White Mesa Mill Field Data Worksheet for Grou'ndwater 1 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged ..... 1 ...... g ..... f<..<.....-___ ..... gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1'----'11'---_----' Time to evacuate two casing volumes (2V) T=2V/Q= 17.33 1 Number of casing volumes evacuated (if other than two) ,-,I..v.-,'I.~A;;I..-_---' If well evacuated to dryness, number of gallons evacuated L.;..I ,N._:1,...;..ft~_---, Name of Certified Analytical Laboratory if Other Than Energy LablL.....:.."v-l.i....l./...:..\ ______ --I Sample Taken Sample Vol (indicate Filtered Preservati ve Type of Sample if other than as y N specified below) y N Type VOCs ~ 0 3x40 rnl 0 ~ HCL Nutrients _\til 0 100 rnl D ~ H2SO4 Heavy Metals 0 0 250 rnl 0 0 HN03 All Other Non Radiologics 0 0 250 rnl 0 0 No Preserv. Gross Alpha 0 0 1,000 rnl 0 0 HN03 Other (specify) ~ 0 Sample volume 0 m Preservative Added y N "Kl 0 1tI 0 0 0 , 0 D 0 0 0 ~ Ghlo("'J~e If preservative is used, specify Type and Quantity of Preservati ve: Comment ~ See instruction A((;\leJ on s;tc o:J Ogs3.~t'll1u· (}..(1rA (;-M(;n preSt:rrY+b plA~e IWI..J-l~. ?v.r~G be~4n 0..+ 0857 P",,~e~ '" ell k-,,+or.1 '* 8 ",' "",tes, 1il .. +.C \')", G \e"~ +},'D~O'" t-+h. F'''S'' 1" .... ,':'f en~.~ .. :r o~ () s. Del" t~ -l-o \,:> '" 1-<-C .. J).G( F.W"~ e "''''' '1 Z. 71 L J)-$ ;r t-,,1" "9/0. R:j1i\1\ H,..\m-((" prl!~C(l+-1-~ <:.ollt'c,-\-5e:.mp)cS. Pcy+-l-1 -to \.0o..1-c:r lI)4S 3Q .2.0 . .s"""y>\-c> ~c:n .. b",;\clk (}.r'ltA cD\kc.rcd. t'-1-13LJ~ '--_______ ---IIDo not touch this cell (SheetName) White Mesa Mill . Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 ~ENISOt!)~~ WHITE MESA URANIUM MILL Attachment 1 ~ See instruction MINES FIELD DATA WORKSHEET FOR GROUND WATER ...........--.- Description of Sampling Event: 13 fJl Q"'CAr+Gr C.h lor O-tO('M .2..0 I J Location (well name): ..... 1 T...:...-w_L..:....I ---=-1.J&...--________ ---I Sampler Name and initials: 1~Y1Ylu Qo I J/J't1/n~ Date and Time for PurgingJ'-'~ ... /_'}=~..:.../_:A._O.....;.lJ ____ __' and Sampling (if different) ...... 1 g=/;....:}.....;.'''''-)_~_D....;..' _, ___ ----' Well Purging Equip Used:@]pump or@] bailer Sampling Event 1 Q"'CArh.(').::1 (..hlorbforf"'l pH Buffer 7.0 7.0 Specific ConductanceI-I _4 ..... 1....,~ ___ ~h.tMHOS/ cm Depth to Water Before Purginm '1 b .3' Conductance (avg) Ib33 L...-~~~ ____ ~ Well Pump (if other than Bennet) 1 &rW1d+o,S Prevo Well Sampled in Sampling Event ..... 1 -r_w_L.\_-_J_~ ____ ......J pH Buffer 4.0 LI. 0 Well Depth(O.Olft): 1 101 . .50 Casing Volume (V) pH of Water (avg) 4" well:/ ~b. b'1 /(.653h) 3" Well:l-. _D~_~.(.367h) 7057 Well Water Temp. (avg) 1:S.~~ Redox Potential (Eh)1 t..j2D Turbidity ...... 1 ~...:.-.J-,r __ --, Weather Condo Ext'l Amb. Temp. O( (prior sampling event)1 ~C>& Time 1 OQSLj -I Gal. Purged 1 ,-\ '1 . I Time I IY"l5.:5 Gal. Purged ...... 1 ;5_>'5 __ ---' 09.5.,5 1:b35 .55 Conductance 1 1 pH 1 ro .57 I pH ,-I __ ---' Conductance Temp.oC I 15,;;2.4 I Temp.oC Redox Potential Eh (m V) I LU~ I Redox Potential Eh (mV) 1-1 ___ __' Turbidity (NTU) I ~.9 I Turbidity (NTU) I J Time I 0':\5(;, -I Gal. Purged I 6'5 ~ I Time Gal. Purged .... 1 ___ __' Conductance I I pHI I Conductance pHI-I ___ -I Temp.oC I I Temp.oC Redox Potential Eh (m V) I I Redox Potential Eh (mV) 1...1 ___ ---1 Turbidity (NTU) I I Turbidity (NTU) White Mesa Mill Field Data Worksheet for Groundwater ·1 of, Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged ..... I_b....;;' ___ -' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = ..... 1 _, \'---_----' Time to evacuate two casing volumes (2V) T=2V/Q= I 6.0 I Number of casing volumes evacuated (if other than two) I I.bb If well evacuated to dryness, number of gallons evacuated bl Name of Certified Analytical Laboratory if Other Than Energy Lab~ ..... _tV_/_/} ______ ....... Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as Added y N specified below) y N Type y N VOCs I:l-0 3x40 ml 0 Ij. HCL SI 0 Nutrients CB 0 100ml 0 ~ H2SO4 ~ 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) BI 0 Sample volume 0 tlI 0 Cj ch \o{";ae If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction '--_______ -'IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Groundwater Monitoring Quality Assurance plan (QAP) Sampler Name Date: 03/22/2010 Rev. 6 Attachment 1 L"~ See instruction Location (well name):1-1 T_w_L.\_~_l _~ ________ ----, and initials: lr:r:;:nMr f} 0 I LJ",~ /nt Date and Time for PurgingJl-_g..:..../..;;...1.5....:,/_9-_0_1_1 ___ ---' Well Purging Equip Used:~pump or@] bailer Sampling Event IQv'.o..c'+u8 GhlofO}O(rr) pH Buffer 7.0 Specific ConductanceL-1 q_~..:....1 ___ ---'I!lMHOS/ cm Depth to Water Before Purgin~ K1-30 Conductance (avg) 0, , and Sampling (if different) 1L-&~/:....:I.(,;L...7:J.......:.....o..:....)J ___ ----' Well Pump (if other than Bennet) IGTIAr'l(}\~oS Prevo Well Sampled in Sampling Event 11--n_W_L:_\_-_I~ ____ ---' pH Buffer 4.0 Lj.O Well Depth(O.Olft): I ~3. 00 Casing Volume (V) pH of Water (avg) 4" well:1 3.J~ 1(·653h) 3" Well:L-. _O __ -J.(.367h) Well Water Temp. (avg) ':l...S.~ Redox Potential (Eh) I 3gb TurbiditYL-1 ..:..;)....=;0 __ --1 Weather Condo Ext'l Amb. Temp. DC (prior sampling event)1 ~I b Time I )()t; J I Gal. Purged I S.S I Time I I Gal. Purged I I Conductance I 0.1 I pH Is.en I Conductance I I pH I I Temp.oC 1 t95:~b I Temp.oC I I Redox Potential Eh (mV) I 5ZlO I Redox Potential Eh (m V) I I Turbidity (NTU) I l.O I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pH I I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data"Worksheet for Groundwater . 1 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged L..I ....:5~ . .s=--__ ---I gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = IL---'-=-I __ ---I Time to evacuate two casing volumes (2V) T=2V/Q= I .b7C:, I Number of casing volumes evacuated (if other than two) II.Y1 If well evacuated to dryness, number of gallons evacuated .5_5 Name of Certified Analytical Laboratory if Other Than Energy Lab~L.._~_1....:..A-,--_____ ----, Sample Taken Sample Vol (indicate Filtered Preservative Type of Sample if other than as y N specified below) y N Type VOCs 129 0 3x40 mI 0 ~ HCL Nutrients .~ 0 100mI 0 ~ H2SO4 Heavy Metals 0 0 250 mI 0 0 HN03 Preservative Added y N '[I 0 1tJ 0 0 0 All Other Non Radiologies 0 0 250 mI 0 0 No Preserv. 0 D . Gross Alpha [J D 1,000 mI 0 0 HN03 0 Other (specify) lEI 0 Sample volume 0 lEI 0 ch 10(';~L If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction Arri-Jeo.. 0(1 .site "'1 \O:3b. ~/'1"~"" ~1"Id. &Mf:" pre~crrt-+o P'-'("~e.. l~\.l ~ 14. Y"'(je b~~yAn 0..+ JOL.JJ l' W'~-e~ well -rOI v.. ·b+t..\ ~ 3D ~<:('c71Ch P -,. "ell 1 r-J.) 0 -v..r~eo. V'-' O\~. 1 v.r~t:. enat't\ I>,:t lOt.{ I. Wah, ~ ~J.C:G\r +hro~~ovJ-?u.r~e. Left sa·" ",t 10 LI.S . 'R~I1.r'\ ?v..\rv\~(, ?1~Se.(\+ tD c.oned-5~/'l'1FJe.~. 1:J~pt~ 1-0 w~+e( W6.S 27.~;(. SIAt¥'\p\e~ we((' bt\;\<J. (}.(\rA (...o\led-.!:J.. 0..1--P103. L--_______ ----lIDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 0 1f;J 2 of2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 '-:::,-~50J)n ~INES ~ FIELD DATA WORKSHEET FOR GROUND WATER WHITE MESA URANIUM MILL Attachment 1 ~ See instruction Descripti'; ~f ~~~pling Event: 13(/11 Q\Aarftl" c..h \o(o:tof'm 0...011 Location (well name ): ..... 1 __ ""\\J.l....:......;._'4....;.....--..:;l5~ ______ ----I Sampler Name and initials: 1-r411nt.1" 110 II; J~ ;J"H Date and Time for Purginm 'if 17/a..oll and Sampling (if different) ..... 1 N.;.....:....'IA-'--_____ --' Well Purging Equip Used: [!!]pump o@ bailer Sampling Event 1 Q",&\(t-er8 c.h lor o+o( M 1 pH Buffer 7.0 Specific Conductance ..... 1 ---'4 ...... j ...:..1 ___ .... II-tMHOS/ cm Depth to Water Before Purginm 7 b, I J Conductance (avg) Well Pump (if other than Bennet) 1 C.O(l+ifhAOIAS Prevo Well Sampled in Sampling Event IIWl.J -:;;"0 pH Buffer 4.0 Well Depth(O.Olft): 1 12-0.50 Casing Volume (V) pH of Water (avg) 4" well:1 3 0 .2.4 1(.653h) 3" Well:L-. _b;;;......-._-J. (.367h) Well Water Temp. (avg) 1 1 '·"'1 Redox Potential (Eh) .... 1 _~_5_~_---, Turbidity 1 .... _0 __ ---' Weather Condo Ext'l Amb. Temp. O( (prior sampling event)1 '30" Time I l~l.\q I Gal. Purged I I Time I I Gal. Purged I I Conductance I ~~D7 I pH I C::, .~'1 I Conductance I I pH I I Temp.oC I I~·X~ I Temp.oC I I Redox Potential Eh (mV) I {)57 I Redox Potential Eh (m V) I I Turbidity (NTU) I () I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pHI I Conductance I I pHI I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged .... 1_0 ____ ....... gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1-1 .::::;..5.;.:.'3:.......-_----1 Time to evacuate two casing volumes (2V) T=2V/Q= 1 0 1 Number of casing volumes evacuated (if other than two) o If well evacuated to dryness, number of gallons evacuated D Name of Certified Analytical Laboratory if Other Than Energy LabIL..._pJ-...:...'/4..:....-_____ ~ Sample Taken Sample Vol (indicate Filtered Preservative Type of Sample if other than as y N specified below) y N Type VOCs ~ 0 3x40 mI 0 lB HCL Nutrients 1B t1 lOOmI [j ~ H2SO4 Heavy Metals 0 0 250mI 0 0 HN03 All Other Non Radiologics 0 0 250mI 0 0 No Preserv. Gross Alpha 0 0 1,000 mI 0 0 HN03 Other (specify) m 0 Sample volume 0 ~ Date: 03/22/2010 Rev. 6 Preservative Added y N lSI 0 "EI 0 0 LI 0 0 0 0 0 2J Ch \O'·lae. If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction Aff';-.jr:.~ 01'\ S~+e.. 0--+ };l..YY. lo..Mer a.r1~ G-C4.rr;n f("d~n+ -h,(" ~ClMp1j e.venf. 100v,, oepth +0 ~1-cr lMd-.s~W\pl~s ~(~ cDlled~ot ~+ J.;2..50. LUli\.1-c:r WC0;. C't:::&\(, L-e-t} s.; r~ {i:..11~SS . L-________ ..... IDo not touch this cell (SheetName) White Mesa Mill. Field Data Worksheet for Groundwater . 2 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 I~E~'SON"Ji L MINES ~ FIELD DATA WORKSHEET FOR GROUNDWATER WHITE MESA URANIUM MILL Attachment 1 ~ See instruction Description of Sampling Event: I '3,.a Q",c..c-tu Gh lcr()t)rl"1 !Loll Location (well name):L..I_,_w_'-'_-_,_4. ________ -' Sampler Name and initials: 15 ~nn<.r 'flol\:ao..::1)-rA- Date and Time for PurgingJ1-~_/_I_{"_/ !2_D......;I1 ____ --1 and Sampling (if different) I Sj 111~o II Well Purging Equip Used:@]pump o@ bailer Well Pump (if other than Bennet) I &rlAntHO.s. Sampling Event l'?l Quc.,.hrl~ Gk \o("o+orm I Prevo Well Sampled in Sampling Event L..11'_·_W_'i_-_b ____ -' pH Buffer 7.0 7_0 Specific ConductanceL-1 .....;.q...;..~1.!--___ ....II!J.MHOS/ cm Depth to Water Before Purgingj ~. gS Conductance (avg) pH Buffer 4.0 y.o Well Depth(O.Olft): l 1LtQ.O() Casing Volume (V) pH of Water (avg) 4" well:1 S\, (,g 1(·653h) 3" W ell:L-_ _0-'---_----'_ (.367h) Well Water Temp. (avg) I \l...j. 8~ Redox Potential (Eh)'-I.!4...;...b_I __ --' Turb idity 1'----'t.J .... LI'---_--' Weather Condo Ext'l Amb. Temp. O( (prior sampling event)1 ').30 Time 11C 13 I Gal. Purged I ,,'\ I Time I 101"1 I Gal. Purged I lJO I Conductance I '3~9k I pH I {,.;2.1 I Conductance 1 3b6 1 I pH 1(,.;)..$ I Temp.oC I lq ·$~ I Temp.oC 1)4 ·8'> I Redox Potential Eh (mV) I 'r)..7g I Redox Potential Eh (m V) I .?.7~ I Turbidity (NTU) I ~S.b I Turbidity (NTU) I Yl./.l I Time I lD\S I Gal. Purged I 12.1 I Time 1101"" I Gal. Purged I 1 :32 I Conductance I ~.(.D5 I pH I ".~ I Conductance I 'Jft>l I pH I f>5J' I Temp.oC I IQ.go I Temp.oC I ) Y .]~ I Redox Potential Eh (mV) I ').."bd.. I Redox Potential Eh (mV) I ~51 I Turbidity (NTU) I LPlD I Turbidity (NTU) 11.];6.1 I White Mesa Mill Field Data Worksheet for Groundwater ." 1 of2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 11-1_3..;:2""'"---__ ---' Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = ,--I _1_' __ -' gallon(s) Time to evacuate two casing volumes (2V) T = 2V /Q = 1 g .3'i 1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy LablL-tJ_/A _______ .....J Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as Added y N specified below) y N Type y N VOCs ~ 0 3x40 ml 0 ~ HCL 19 .,. 0 Nutrients rB 0 100 ml 0 ~ H2SO4 EI 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) ltl 0 Sample volume 0 ~ 0 m L.h )of'i d.e If preservative is used, specify Type and Quantity of Preservative: See instruction Comment L...-________ ....JIDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) :-EN-IS~J)-~"~~ ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 ~ See instruction MINES FIELD DATA WORKSHEET FOR GROUND WATER <-----..:.,...--..,.. Description of Sampling Event: 3 r-d' Q",{).rtcr' c..J'" lorofo rM !to II Location (well name): .... 1 _N_W_-_3_d.. _________ ---' Sampler Name and initials: 1 ~"'lt'r }"}o 11IJa.j /111 Date and Time for Purgingj fS / I b 7 ~o \ I and Sampling (if different) '/\//1\ '---------~ Well Purging Equip Used: [![] pump o@ bailer Well Pump (if other than Bennet) 1 L.. Q_)_~_O ____ --, Sampling Event IQv.,a.Aerl~ Gh \orbto()N' l-nV '-l-;l.4 R Prevo Well Sampled in Sampling Event L.. _______ --....I pH Buffer 7.0 7 .0 pH Buffer 4.0 1...\.0 Specific ConductanceL..I..:..~_9~ ____ ...J"lMHOS/ cm Well Depth(O.Olft): 1,-\3_~_._b_O __ --, Depth to Water Before PurgingJ -, b . 0 ~ Casing Volume (V) 4" well:1 3b, gb 1(·653h) 3" Well: 0 (.367h) 1.-__ ----1 Conductance (avg) pH of Water (avg) 5,'11 . Well Water Temp. (avg) 1 2...0:11...{ Redox Potential (Eh) .... 1 2._09 __ --' Turbidity IL.......:;:O"-_---' Weather Condo Time I\~So Conductance 1 'J:> b )5 Temp.oC Gal. Purged 1 7 S . "lS pH 1 $.q1 Redox Potential Eh (mV) 1 Q....'01... Turbidity (NTU) () Time 1 120Sd.. Gal. Purged 11 b :3>Z Conductance 1 ,)lSg 5 pH 1 (,.00 Temp.oC 1 Q...6.7'» Redox Potential Eh (mV) 1 ~IO Turbidity (NTU) o White Mesa Mill Field Data Worksheet for Grej'undwater Ext'l Amb. Temp. O( (prior sampling event)I '7 0 . 1 Time 1 t? .. 51 1 Gal. Purged 116 .J-6 1 Conductance 1 35~:S 1 pH 1 S.,,~ 1 Temp.oC 1 M.7D 1 Redox Potential Eh (mV) 1 ~I 0 1 Turbidity (NTU) I () J Time 1 1;:2.53 1 Gal. Purged 1 76. (, () 1 Conductance 1 3k~() 1 pH 1 b .OO 1 Temp.oC 1 ~.c).51 1 Redox Potential Eh (mV) 1:;"'07 1 Turbidity (NTU) 1 () 1 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1 77.03 Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 11.-"_2._17 __ ----1 gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= 1 33G!.gO 1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy LablL..;;V._v...:.;"'--______ --' Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as Added y N specified below) Y N Type y VOCs !1;1 0 3x40 ml 0 f)j] HCL ~ Nutrients $I 0 lOOml 0 I). H2SO4 00 Heavy Metals 0 0 250 ml 0 0 .. HN03 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) ;·lhl 0 Sample volume 0 r.a D C h \ori at If preservative is used, specify Type and Quantity of Preservati ve: Comment ~ See instruction Arr;\ld, on .s;+t: a..t Ob5.(.. ~ntla o,YlJ G-Q,rr;Yl rre..se.n+ .for r\\r~'( o-ntA ,Stimp1;"j cV~f)f . P"'I'~tt b~~IJ,T\ 0-+ 070D. r\A.(,~<c\ we.l\ ~(' ~ +0-\-&0.\ o~ 3SS M;fl""te-S" l.Uo..+cr lU~ I"t\O~~'0 L1C:tAr' +~ro",----,\~oVvt-~G. pur~<, ?\Ar~c d1(;!eA 0."", So,M?}C~ wer<. Lolled-edt (I-..r-1.2.52). D-cpfh}-o V-Jo..,-t~ wt\,~ ~ 1./1. I.-~.t}-S;-1-c. Pi;}-130 I. '--________ -'IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 '0 2 of 2 Mill· Groundwater Discharge Permit Date: 03/22/2010 Rev, 6 Groundwater Monitoring Quality Assurance Plan (QAP) ~O.-~~IS;;~rj~ i WHITE ~!~~~~~I~~ MILL MINES FIELD DATA WORKSHEET FOR GROUND WATER .... ~------- Attachment 1 ~ See instruction Description of Sampling Event: I '3 r6' G \)..C(,-t e.r Gh 10"-0 +0 '{' M :J.-o II Location (well name):IL-'_W_I...\~-..:..I&~ ________ --I Sampler Name and initials: tEllllCr l}o I )iJA~JTI-t Date and Time for Purgind 8,/ 16/;t 0 I) and Sampling (if different) 1-1 ..::.~,,--J_n....:./_a._O_I_1 ___ ----' Well Purging Equip Used: []I] pump o@ bailer Sampling Event IQ\A~rkd.., Co)., lo(o~o("'" pH Buffer 7.0 1 .0 Specific ConductanceI-I -,,~...;..q'l-,--___ ..... If.tMHOS/ cm Depth to Water Before Purginm S b . bO Conductance (avg) Well Pump (if other than Bennet) 16-1"I.Andtos Prevo Well Sampled in Sampling Event L-I ~ __ L.\_-_I_' ____ ---l pH Buffer 4.0 4,0 Well Depth(O.Olft): I 137, SO Casing Volume (V) pH of Water (avg) 4" well:1 S2l.36 1(·653h) 3" Well:L-. ---=.0 __ .....1. (.367h) Well Water Temp. (avg) l IS . b~ Redox Potential (Eh) I L..\?-j Turbidity ..... 1 ~_~...;....{, __ ....... Weather Condo Ext'l Amb. Temp. DC (prior sampling eventll J.5° Time 1110.3 1 Gal. Purged 1 ~g 1 Time 1110'-) 1 Gal. Purged 1 q9 1 Conductance 1 ~()ll 1 pH 15."lD 1 Conductance 1 ~o73 1 pH 15.81 1 Temp.oC I )5,lq I Temp.oC I \'S.73 I Redox Potential Eh (mV) I ~~I I Redox Potential Eh (mV) I '138 I Turbidity (NTU) I ?~O I Turbidity (NTU) 12'13 1 Time I \lOS I Gal. Purged II 10 I Time 1110b I Gal. Purged I );l:j I Conductance I :;),.D.5~ I pH 15.'10 I Conductance I Q...o37 I pH Is.G)! I Temp.oC I )S. bO I Temp.oC I \5152> I Redox Potential Eh (mV) I L\~\ I Redox Potential Eh (mV) I ~J~ I Turbidity (NTU) I :30D I Turbidity (NTU) I ~~ I White Mesa Mill Field Data WorKsheet for Groundwater "1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1-1 .......;;\~;;....!..1 ___ ..... Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1-.1 -..:..:..11 __ --' gallon(s) Time to evacuate two casing volumes (2V) T = 2V /Q = 1 ~. bO 1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~ ..... ....;.#_-,I.~ ______ ----, Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as Added y N specified below) Y N Type y VOCs EJ 0 3x40 ml 0 C)l HCL ~ Nutrients ql 0 100mI 0 ijI H2SO4 IZi Heavy Metals 0 0 250ml 0 0 HN03 0 All Other Non Radiologics 0 0 250 mI 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) 54 · 0 Sample volume 0 ~ 0 C h\o('; c\c If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction A('c<-JecA lin ~I't~ ~-t 1050. '""I4..nnt:1'" MJ. G-Glrr;V\ pre.sent' -+'0< ?\Ar~e. p",(~e. b~Gln ~t lOSS Pv..(~ec}.. U)ell to( c;... -tohl of 1\ 1\-1:f\lAte.5. IJJ6.·-ftr h(i,,~ ~ brown <.olor -ro :+-. 'Pv..(~e4 '<:P"et7 cnd<:d \ If..~ naC:" De~ +0 wo..-tu o-..f.ta fW~e \,!)c;..~ S7.3S.. L~.r+ 5 11<:. 0.1-1'310 Arr"i\le~ on site 1\.1-0717. JlllnllC'r to.f\cA &CJ.('(':'1 prd-c-Yl.}--h coll~d -SCll"'lplt'..). DeptI-. +v w~+((" \.Jf.0 !:.b.b9. S"'rvlf>16 \t.)((~ bO\:)cA (AT-07.:z.1 . L<f't-~i+~ ~-t-07:;1.5. L-________ ...JIDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 D · q 0 0 ~ 2 of 2 Mill -Groundwater Discha rge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 EiEN"~ONI)~~-~.-· WHITE MESA URANIUM MILL Attachment 1 l:& See instruction MINES FIELD DATA WORKSHEET FOR GROUND WATER , ~ ..... - Description of Sampling Event: 13 f h; Q",(A(tcr-c:.hlorOfo(P'1 ~Ol' Location (well name ): .... I'_\JJ_"1_-_'4"'--________ ---1 Sampler Name and initials: I --r;l1fler Rol],a~~/""1J Date and Time for Purgingj g)) 71 ::LOI I and Sampling (if different) ;VIA ~-------~ Well Purging Equip Used:OOpump or@] bailer pH Buffer 7.0 7·0 Specific ConductanceL...1 q.l...,;~:.....!1 ___ --IIfA.MHOS/ cm Depth to Water Before PurgingJ 6 \ . 05 Conductance (avg) Well Pump (if other than Bennet) I -rWL)-'Y Prevo Well Sampled in Sampling Event 1....-_______ ---1 pH Buffer 4.0 11 ·D Well Depth(O.Olft): 1 1~5_00 Casing Volume (V) pH of Water (avg) 4" well:1 Y \. -zs 1(·653h) 3" Well:L.... _o __ --I.(.367h) Well Water Temp. (avg) I lb. '3.2-Redox Potential (Eh) I ..... ~--,-t.t_g_---, TurbiditY ..... 1 _0 __ ---' Weather Condo Time I l~S~ I Gal. Purged I Conductance I ?-734 I pHI 6·;;;z...~ Temp. DC I lb. '3::r: 1 Redox Potential Eh (mV) 1 ;tQg 1 Turbidity (NTU) 1 0 1 Time 1 1 Gal. Purged 1 Conductance 1 1 pH 1 Temp. DC 1 1 Redox Potential Eh (mV) 1 1 Turbidity (NTU) 1 1 White Mesa Mill .. Field Data Worksheet for Groundwater I I 1 1 Ext" Amb. Temp. O( (prior sampling eventll 3J 6 Time Gal. Purged L...I ___ -I Conductance pH 1'--__ --' Temp. DC Redox Potential Eh (m V) .... 1 ___ --I Turbidity (NTU) I I Time Gal. Purged .... 1 ___ --I Conductance pHL....I ___ --I Temp. DC Redox Potential Eh (mV) IL--__ ----I Turbidity (NTU) 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1 I-_6 ____ ---' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = 1 14.0 T=2V/Q= 1 c 1 Number of casing volumes evacuated (if other than two) 1-1 _0 ___ --' If well evacuated to dryness, number of gallons evacuated 1-1 _0 ___ --' Name of Certified Analytical Laboratory if Other Than Energy Lab~L.._#_/ A ______ ----I Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y VOCs 19 , 0 3x40 ml 0 m HCL EJ ' Nutrients ~ 0 .100ml 0 ~ H2SO4 ~ Heavy Metals ,0 0 250ml 0 0 HN03 0 ,. All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 Other (specify) "E 0 Sample volume 0 ~ 0 L. hlor',ac.. If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction Arr;\Jed. ell s,··h: 6..1-1353. 16..Mer 6..nJ &(A,(f:fl pr~seflt +0(" ~a..Il1F);~ e\Jent. +OD~ dey>th +D \.0~tcr (AnA c.o)lectca .so.~'Plc:'S ",,-t-1'-100, wC\.Tc, WCU cl~(". L.c+t s Jc. A1-140 LJ . L--________ ....IIDo not touch this cell (SheetName) White Mesa Mill Field Data Workstieet for Groundwater N 0 0 0 0 0 ~ 2'of.2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 1::.soJ)U ~INES ~j FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampii~g Event: 1 ~ (dj Q\N.'-.('+eo. cJ:; I orD+--;'r I'V) !:(o II WHITE MESA URANIUM MILL Attachment 1 ~ See instruction Location (well name): .... 1 T_\N_~.;....-_:2_0 ________ --J Sampler Name and initials: 1 ==r';Y1l1er fiD/ /.Jl4)lflj)~ Date and Time for Purging/ «/17/:J...D)) and Sampling (if different) Well Purging Equip Used:~pump o@ bailer Well Pump (if other than Bennet) IGon1/l7l.ADV\~ Sampling Event IQv..Cl.r-h::('11 CJ1)Drat~(f1'\ Prevo Well Sampled in Sampling Event I 'T'WL\ -;2. pH Buffer 7.0 /.0 pH Buffer 4.0 q-o Specific ConductanceI-I _~_q_q ___ ....JII-lMHOS/ cm Well Depth(O.Olft): 1 ) Db.CO Depth to Water Before Purging/ bg.L} } Conductance (avg) Well Water Temp. (avg) I Ib·~7 Weather Condo Time /1;2.3'1 1 Gal. Purged 1 Conductance 1 3C.Lj:;,l.. 1 pH 1 Temp.oC I 1(,:;2.7 1 Redox Potential Eh (m V) 1 ~$$ () 1 Turbidity (NTU) 1 D 1 Time 1 1 Gal. Purged 1 Conductance 1 1 pH 1 Temp.oC 1 1 Redox Potential Eh (mV) 1 1 Turbidity (NTU) 1 1 White Mesa Mill Casing Volume (V) pH of Water (avg) 4" well:1 ~Y.5y 1(·653h) 3" Well:l-. _0 __ ....J. (.367h) ~·81 Redox Potential (Eh) 1 .!2..go Turbidity 1-1 _0 __ ----' Ext'l Amb. Temp. O( (prior sampling event)1 '30· 1 Time Gal. Purged 1-1 ___ ....J 5·ZI 1 Conductance pH L-I __ ----I Temp.oC Redox Potential Eh (m V) 11--__ ---' Turbidity (NTU) 1 1 1 Time Gal. Purged 1'-___ --' 1 Conductance pH 11--__ ----1 Temp.oC Redox Potential Eh (mV) 1-1 ___ --I Turbidity (NTU) 1 Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1 ..... __ 0 ___ --' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = I -10 T=2V/Q= 1 0 1 Number of casing volumes evacuated (if other than two) o If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy LablL.-.M_V4-=--______ ....J Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y N VOCs ~ 0 3x40 ml 0 rn HCL 19 0 Nutrients lE ' 0 100ml 0 1ZJ H2SO4 ~ 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 tJ · Other (specify) ~ 0 Sample volume 0 lEI 0 ill c::. h \or ~ J~ If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction A((i.Jt:J.. on .sit~~'} 1~3. -ro.l1n-cf" Mil &--<A((,i" prt:scn1' +or SdI""" plJ -e..Jcnt. +ooK Dep1"-'-' -to wGl.1-~r o.nO-.sG\.T'1 pic;. wert:.. colled·cd ~+ 12.\.10 # l.0~+~i Wli.S C }~o.( . L-e.-t1-s;t <, 60.+ 1:2. Y3 '--________ --'IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 .- Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ~OENISOn~'~ ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 ~ See instruction MINES FIELD DATA WORKSHEET FOR GROUND WATER .... _t . '_ Description of Sampling Event: ';iDl Gv-arfu Chloro+ofM ;;ZOOil Location (well name):l iW\..I-;J,,) ~--~------------------~ Sampler Name and initials: l 4"o..t1 t1c.r Uol/.·J~JTIl Date and Time for PurgingJ,-_g_J_lb_I._~_O_I _1 ___ ----' and Sampling (if different) I r.tJ 1'1/;2.01 \ Well Purging Equip Used: ~pump o@ bailer Well Pump (if other than Bennet) Prey. Well Sampled in Sampling Event L..I T_W_Y_-_IO ______ ----J pH Buffer 7.0 7.0 pH Buffer 4.0 q.o Specific ConductanceL-1 _q_C\9 ___ ----'I""MHOS/ cm Well Depth(O.Olft): I l~I.OO Depth to Water Before PurgingJ SL\ .7Y 4" well:I43.::2.C:, 1(·653h) 3" Well: 0 (.367h) L....-. __ ---I Casing Volume (V) Conductance (avg) pH of Water (avg) I Well Water Temp. (avg) I 1 ~ .1{) Redox Potential (Eh) IL-§_O __ --' TurbiditYL-1 -=5=.( ..... )_--' Weather Condo Ext'l Amb. Temp. O( (prior sampling event)I 30b Time 113'i-b 1 Gal. Purged 1 "''' 1 Time 1)3'17 1 Gal. Purged 1 77 1 Conductance 1 3~b~ 1 pH 1 (·Q7 1 Conductance 134 /) 1 pH 1 b.LJ9 1 Temp. DC I IC · 7]" 1 Temp. DC 11G·7QO 1 Redox Potential Eh (m V) 1 3b9 1 Redox Potential Eh (mV) 1 '3S 6 1 Turbidity (NTU) 1 ~.\ 1 Turbidity (NTU) 15.0 J Time 11'3 q is 1 Gal. Purged 1 ~~ 1 Time 113qq 1 Gal. Purged 1 1r 1 Conductance 1 '1,'179 1 pH 16·9g 1 Conductance 1 39sR 1 pH 1 b.Y$' 1 Temp. DC 116.(>7 1 Temp. DC 1 1". :bS 1 Redox Potential Eh (m V) 1 343 1 Redox Potential Eh (mV) 1 3LJb 1 Turbidity (NTU) 1 ~.Q 1 Turbidity (NTU) 1 5 Q 1 VVhite Mesa Mill 'Field'Data Worksheet for Groundw'ater 1 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1'--4 ..... 4..J.--___ --' Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1.-1 _11 __ -, gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= 1 7.8'-1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~,-_;.J_/_A ______ ---, Sample Taken Sample Vol (indicate Filtered Preservati ve Preservative Type of Sample if other than as Added y N specified below) y N Type y VOCs D§ 0 3x40 rnl til I2J. HCL ~ Nutrients rn 0 . 100 rnl 0 121 H2SO4 ~ Heavy Metals 0 0 250 rnl 0 0 HN03 0 All Other Non Radiologies 0 0 250 rnl 0 0 No Preserv. 0 Gross Alpha 0 0 1,000rnl 0 0 HN03 0 Other (specify) rlJ 0 Sample volume 0 ~ 0 Ch\oc,~-( If preservative is used, specify Type and Quantity of Preservati ve: Comment ~ See instruction A{r·I\J(.~ on s;tc <'1.1 13~. ';::nl1~r 0..(10-(,..I).(,..;n pre.sc:n.t +0 pv.f'~e. IWLJ-;U. Pl..\~e. bt)o..l1 a..t }3~ O. 'P1.\(~e.a \N<:.1I ~, 0... 1-ot'" \ ot ~ Mi n lAte.s . w~+a 1.0c:t.$ cl.ea.(" th,..o~'h()"'t-p\;\rje. P~(5-!. e."d~.c\ "'-1 13Ll ~\ D~p1-'" h \,)l\..·h~:(' we,...) '-1.1.3 L~+~ 51+< ~+ l'3:JY. Aff,-.)ea. 0(\ ~\i-~ ()...t 01.50. '''''I1.e.r tIVI~ 6-r>.rri(l pr~~eni-+0 '-oiled S"MF)~~' De.p-\-h 1-0 \N(}..h( w(A~ SI..\·c:,O >~fY\pl~~ We.re. b(h~l-lt\ 111.+ D'155 . Lef.}-,S,'+c... ",t 0751:$ L-... ________ .....IIDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 [j 2of2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 OENI~:J)~ ~l WHITE MESA URANIUM MILL Attachment 1 ~ See instruction . MINES . FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 1 3("~ QuC\r+er CJ'llor-o-to('fI"'I :l.OI} Location (well name):L-I_I_VJ_y_-_;l.;t ________ ---J Sampler Name and initials: I i'"~nnu no}].J~/TH Date and Time for Purging/L-g.:::..J_l_~_J :;._0_11 ____ ---' and Sampling (if different) 1 ~J II I J;LD 1/ Well Purging Equip Used: [][]pump or@] bailer Well Pump (if other than Bennet) 1 &t"l.AfI J+b..s Sampling Event 1 Qv.o.l"'+crb cJ, lorC5Qrrv) Prevo Well Sampled in Sampling Event 1L....-,_W_L\_-_18 ____ ---J pH Buffer 7.0 ..... 1 _1_.0 ___ ---' Specific Conductance L-I q_9_4-=--__ ---'1 fA,MHOS/ cm Depth to Water Before PurgingJ 51..\.0 D Conductance (avg) ..... I -"'.s=~"-=o........; ____ ---' pH Buffer 4.0 L\.O Well Depth(O.Olft): 1 \ )3. 50 Casing Volume (V) pH of Water (avg) 4" well:/38.6.5 /(.653h) 3" Well:L-. _o __ .....1.(.367h) b.3D Well Water Temp. (avg) 1 1 Co .S~ Redox Potential (Eh) 1 2, 'n TurbiditYL-1 q...:..-__ ....... Weather Condo Ext'l Amb. Temp. O( (prior sampling event)1 :lO8° Time 1 ,~C>\ I Gal. Purged I SS I Time p;2.0~ I Gal. Purged I bb I Conductance I SYL\~ I pH I b .'3:;1.. I Conductance I ~X>.\ I pH I ~.30 I Temp.oC I lb.gC;; I Temp.oC I n;·6S I Redox Potential Eh (mV) I q 1'1 I Redox Potential Eh (mV) I qOO?: I Turbidity (NTU) I q,l I Turbidity (NTU) 1'1,0 I Time I l~03 I Gal. Purged I 77 I Time I );tog I Gal. Purged I g6 I Conductance 151 g;,z.. I pHI ".')0 I Conductance l E:I b3 I pH I ~.~7 I Temp.oC 11(0;.59 I Temp.oC I t b. ""5 I Redox Potential Eh (mV) I .391 I Redox Potential Eh(mV) I 3;G,? I Turbidity (NTU) I 9.1 I Turbidity (NTU) I 9·) I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 . Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged L-I ...lc$S'-=-___ --I Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 11--_1_' __ ----I gallon(s) Time to evacuate two casing volumes (2V) T = 2V/Q = 1 7.0.{, 1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy LablL-_.M._'I_A _______ --' Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y N VOCs "Ill D 3x40 ml D Il!J HCL !J D Nutrients ~ D 100ml D ~ H2SO4 ~ D Heavy Metals D D 250ml D D HN03 D D All Other Non Radiologics D D 250ml D D No Preserv. D D Gross Alpha D D 1,000 ml D D HN03 D D Other (specify) rn D Sample volume D W D ~ Ch' ori d< If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction Afr-;\leo.. 0(\ 5,ih c..1-\ 15~. lAI'ln<.(' iAntA CrOl.(r-:", ?rc.s-en-t to P"''j~ 1\)..)"1-Z2.. Pu.~~~ bejM 0..+ 1)5,. P\>..("~-e~ ~c'l ~O( fA. +0+,,1 of' 8 M;nLA-t~. \A)o..1-u w~ clear thrl)~~o\},.1--tht' ru..'(1-e., . Pv..'(~t:. ~(\c\-e.~ (.>J '~04 . O~?-rh 1-0 'W¢..-1-« ~+t~( P"'~ e Wo.~ "''-'13. L ~·H" sitt: b.1"' 1;;2.0 Arr,IJ!cJ.., Dn Sli-~ ~t 072'1 . IA-Me( "'-11A. &r;.(r:f\ p .... -e.~el'\.}--..for ~"'f"'I pl:~ -e~"t. i~ept~ +0 w",t-("r wt S3.q~ . .s"'fVlp1e!:. w~c-~ b,..:l~~ ~1-073's. L~~ s,l+c.. "'+ 0737 '--_______ -----'IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 -OE~~s~J)J~l. MINES ~ FIELD DATA WORKSHEET FOR GROUND WATER WHITE MESA URANIUM MILL Attachment 1 ~ See instruction Description of Sampling Event: 13 rli Q\Aa.rfc(' c);lol'"o+oryV\ ;L()II Location (well name):L-1 _T_W_L...:.\ _-_:;l,_3 ________ --' Sampler Name and initials: tT~nnu Holl;l~..:1ln.j- Date and Time for Purginm g 11.5 7 ~o J 1 and Sampling (if different) 1 ..... [S"""/-+) ..... 6<-=.h=--D;..:..1/ ___ ---' Well Purging Equip Used:~pump o@ bailer Well Pump (if other than Bennet) Sampling Event IQv.(i.(+uG C.~\O("Of()(M Prevo Well Sampled in Sampling Event [ Iv...> L\ -)L.( pH Buffer 7.0 7.D pH Buffer 4.0 Specific ConductanceL-1 -J4L...;Q.-;.1 ___ ...... I!!MHOS/ cm Well Depth(O.Olft): L-II_lq_._D_D __ --I Depth to Water Before Purgingj GS . q 0 4" well:1 3 \.7;3 1(·653h) 3" Well: C> (.367h) '--------' Casing Volume (V) Conductance (avg) 11-..:3 ...:.7-=.'1 .... 9 _____ __' pH of Water (avg) L-I "'-S--=.g;....;~'___ ____ __' Well Water Temp. (avg) 1 lY.lS4 Redox Potential (Eh)IL-....;..\q...:...q..:.....-_ ...... TurbiditYL-1 (%);t ___ --I Weather Condo Ext'l Amb. Temp. °C (prior sampling event)l~b b Time 1 \~11 I Gal. Purged I qy I Time I l~l~ I Gal. Purged 1.55 I Conductance I 3"11i3 I pH 15.$'1 I Conductance I :37~3 I pH Is.qo I Temp. DC 11l1·Q7 1 Temp. DC 114 ·10 1 Redox Potential Eh (mV) 1 2-,0d-. 1 Redox Potential Eh (mV) 1200 1 Turbidity (NTU) l ~lb.1 1 Turbidity (NTU) I ;;;;'0_0 I Time 1 1~1~ 1 Gal. Purged 1 b~ 1 Time 11d.-IY 1 Gal. Purged 1 77 1 Conductance 1 :379 q 1 pH 1.5 .qi5 1 Conductance 1 3RIL 1 pH 1 S·~2 1 Temp. DC 1 Itt .~:5 1 Temp. DC 1 J9.SQ 1 Redox Potential Eh (mV) 1 19~ 1 Redox Potential Eh (mV) 1 197 1 Turbidity (NTU) l,Xlq .1 1 Turbidity (NTU) 1.;>.30-1 1 White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1-1 .....,;7....:7:.....-___ ....J Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = L-I _,_\ __ --' gallon(s) Time to evacuate two casing volumes (2V) T = 2V/Q = 1 E>.77 1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy LablL...-;v_II'+ _______ ....J Sample Taken Sample Vol (indicate Filtered Preservati ve Preservative Type of Sample if other than as Type Added y N specified below) y N y VOCs III 0 3x40 ml 0 rB . HCL ~ Nutrients tl 0 100ml 0 rpJ H2SO4 ~ Heavy Metals 0 0 250ml 0 0 HN03 0 All Other Non Radiologics 0 0 250ml 0 0 No Preserv. 0 Gross Alpha 0 0 1,000 ml '0 0 HN03 0 Other (specify) rn 0 Sample volume 0 KI 0 Ch\o(;~( If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction A((';\Je~ on ~;tc.. lA.\ l:lO.;z . ~t1f\-t'''' 0\Y1b\ &0.((;/'1 ?(e..se.rrt--+0 J~e--)wL I .... .:l.3. Pv.~e b~h lA~ J2.07 , P\A.(')e~ lN~J\ foc tA. +o}AI of' Seuen WJ;nV\+~~. ?",r£\~ ended ttt 'J:2.14. "0CA..-t-a I.J.J(;U J.' + 'th b <J I( ~ WI "\ rO\J:lr') c.olor. \::kp.J-h 1'1> \"JiA-1 <:r' '-c-~ 71, g~. /..~Jt-slfe-tA..)-1::2./0/., 'R~"'I'\ PGI.'rY)c(' on ~itc. to c.oI1e& 5~yv\p)eS. Dcpf!l +D \,)Q:ter-w~ 65.3'. ~(/'M pk~ ~ef~ bG\:\-eq o.n~ (o)lec.t~J t'i~ 131.5. L-.. _______ --->IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater N 0 0 0 0 0 ,; lSI 2 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 l~:,som~l UINES :::J FIELD DATA WORKSHEET FOR GROUND WATER WHITE MESA URANIUM MILL Attachment 1 ~ See instruction Description of Sampling Event: 13 0 :)\ Q",o.f+Gf" Gh I orof'orrn ~o II Location (well name):L-1 _J_W_Y_-_2._L_I ________ ----I Sampler Name and initials: l-ro..nner l-lo) /,'CX"'-!:/IJ'H- Date and Time for Purgingj1-8~/:.....;.)....;..b:....;/~:.....;.O_ll ____ ___I Well Purging Equip Used: 1m pump or@] bailer Sampling Event IQ"""ri--uk1 c.h\O(o.fofM pH Buffer 7.0 L-1_7_._0 ___ ....J Specific Conductancei-I ....;4_q....;~ ___ ....... If.tMHOS/ cm Depth to Water Before Purgin~ S b . L\ ~ Conductance (avg) and Sampling (if different) 1 fS / /1 } ~O, I Well Pump (if other than Bennet) 1 &nM10\+OS Prev. Well Sampled in Sampling Event l-rw y .. .;2. Y R pH Buffer 4.0 '1.0 Well Depth(O.Olft): 1 \ 1~ . .50 Casing Volume (V) pH of Water (avg) 4" well:13b. ('.3 1(.653h) 3" Well: 0 (.367h) L.....-~_----I Well Water Temp. (avg) 1 J lL q~ Redox Potential (Eh) L-I ~....;.....O..;...I _----I TurbiditYL-1 _0..;......._----1 Weather Condo Ext'l Amb. Temp. O( (prior sampling eventll 11° Time 101 17 I Gal. Purged I bb I Time I071g I Gal. Purged I 77 I Conductance I GlbOc{ I pH I C;·~ I Conductance I qb6\ I pHl b .~ I Temp. DC 11S.DO I Temp. DC 1'4.91 I Redox Potential Eh (m V) I qlD I Redox Potential Eh (mV) I Qo3 I Turbidity (NTU) I 0 I Turbidity (NTU) I 0 I Time 10/\9 I Gal. Purged I lSg I Time I 07~6 I Gal. Purged I 44 I Conductance 1 9h~O I pHI (;.23 I Conductance 19b89 I pH IG.X3 I Temp. DC I 1s.00 I Temp. DC I IS.LiZ) I Redox Potential Eh (m V) I 3~7 I Redox Potential Eh (mV) I 3'iC I Turbidity (NTU) I 0 I Turbidity (NTU) I 0 I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged .... 1 _Gl....;,Cj ......... __ ---' Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1...-1 _'=--1 __ --' gallon(s) Time to evacuate two casing volumes (2V) T = 2V/Q = 1 ~"(;O 1 (;.bb Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab~,---;.J_/_A ______ -l Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as Added y N specified below) y N Type y N VOCs -m . 0 3x40 ml 0 ~ HCL ~ 0 Nutrients !pi 0 100 ml 0 ~ H2SO4 '29 -D Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologies 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) fiJ 0 Sample volume 0 ~ 0 ~ C h \ ()("', ~( If preservati ve is used, specify Type and Quantity of Preservative: Comment ~ See instruction A,,;'\l~~ On ~;+~ o...t 070f:,. \o.M-e.r o.ntA &o.r('\n prG,S<.nt +0 f\J\('~'C TwLj -~~. ?'A~<" b~~(l 0.1' 0711 PV\r~-e.~ ~)I .tor 0.... ·toi-o.) of '\ tyl;Y1lA tes.. VJCA.tcr ~tr..rtG~ {)o.. 'iHle m:J!j bV\+ GJ-e.o..('~. f' V\.r~~ el'lckt>., (/J 07 ".,t). L-eft ~~Te ~t 07:1.:5 , Pep'" +1:) \).),,~.r w",s, 11.L)O A('(';~e~ On s;1e ,,} O~)q . }(;"I'II\< .... p..ntk G-Mr;" p(,G~e.Y\+-1-0 c,~ \I-e.c.t-~Af'lpl~5>. D ~p1-~ -to wcrh:r \NQ-.. Sc",Sb . ~"",""pl~!:. W~("c-bo.;)-(,a 0.1-o hAS. Let} ~It~ 0..1-OG,;;J..7 '---_______ ---'IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill · Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 1:~~~~~Ni)]ll l~.~ .. M~E~ FIELD DATA WORKSHEET FOR GROUND WATER WHITE MESA URANIUM MILL Attachment 1 ~ See instruction Description ; Sampling Event: 13f"b' Qv.,,(".h:( Ghlorof'ocTVI 2.0\1 Location (well name) : .... 1 ----'T'-w_y-'--~ ..;;;).._Y...l,....!..JR"--______ ---' Sampler Name and initials: fGnt1~'" Ho lJ;J"'~/nt Date and Time for Purginm ~ /1.6 I;;, 0 I , and Sampling (if different) .... 1 ::.,..N.,.;..'I.:....:.A ______ ---I Well Purging Equip Used:@]pump or@] bailer pH Buffer 7.0 7.0 Specific Conductance .... 1 _q...!.q..:...~.:.....-__ --II/!MHOS/ cm Depth to Water Before Purging/~_() __ ---' Conductance (avg) Well Pump (if other than Bennet) 1 b(\AI'uHoS Prevo Well Sampled in Sampling Event 1 .... '_W_4_-_~ _____ ____' pH Buffer 4.0 l4.D Well Depth(O.Olft): .... 1 _0 ___ --1 Casing Volume (V) pH of Water (avg) 4" well:~_o __ -fI(.653h) 3" Well:. 0 . (.367h) 5,\s Well Water Temp. (avg) 1~·1S Redox Potential (Eh)1 366 TurbiditYL...1 _O __ ....J Weather Condo Ext" Amb. Temp. °C (prior sampling event)1 15° Time 1 0('38 I Gal. Purged I ) 2S 0 I Time I I Gal. Purged I I Conductance I J.g I pHl s.IS I Conductance I I pH I I Temp.oC 1d$,75 I Temp.oC I I Redox Potential Eh (mV) I '3 kg I Redox Potential Eh (mV) I I Turbidity (NTU) I Q I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pH I I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White MesaMili Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1-1 ---=~...;.D,;,...O~ __ ....I Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = L-I --!..l' Il.-_-----I gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= 1 0 I Number of casing volumes evacuated (if other than two) 1-1 ",,;u:::"""" __ ...J If well evacuated to dryness, number of gallons evacuated () '----_ ..... Name of Certified Analytical Laboratory if Other Than Energy Lab!I-#;.......<...I..:....ft'--______ ....I Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) Y N Type y N VOCs lSI 0 3x40 ml 0 ISJ HCL §g 0 Nutrients E2I 0 100ml 0 [)-H2SO4 rn 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 250 rnl 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 rnl 0 0 HN03 0 0 Other (specify) I Sample volume .~ 0 0 rn 0 00 Ch\o,ia( If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction A-rr;\le.d on ~;+e ",t 0"15. )~I'\r'\cr o.n~ ('-fA{rir) ?u>ef\t -to rerfotl'Y\ '(';t)..$G\-t-e. R,'n5"'+c b~JGlI) o,t Ob~. t\.\I""l?e~ SD (""l1orls of Ac:a \0c...tu1 SO &",I/OY/.5 o.f .sD~? w"'·h .. ,.... "nd }DO ~c..l/on~ of DJ. Qo-.+c:.r. Ri(l"so...1-G cnde~ c..fl~ .s6i.f'V)ple~ lNerc (.olJ~GtcJ ~t' Of-YO. Lc-f+ Sift £\1-O'{'lJ3. '-________ ..... IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) OENISONI)J ~ ATTACHMENT 1 Attachment 1 WHITE MESA URANIUM MILL ~ See instruction MINES FIELD DATA WORKSHEET FOR GROUND WATER Description oi ;~mpling Event: 13i" (J\ Q\JI.",r+c:r CO h lOt"o{bfM ~ol\ Location (well name): ...... 1 T_W_l.._I _-_;l.S _________ ---I Sampler Name and initials: 11"nnu 'Ao)},J41r7TlJ Date and Time for PurgingJ g / \ ~ / J)...D II and Sampling (if different) &/]'/.:2.611 ~~------~ Well Purging Equip Used: 00 pump or@] bailer pH Buffer 7.0 7.0 Specific ConductanceL-I---'4....;.99-'--__ ---'I~MHOS/ cm Depth to Water Before PurgingJ~J3t 1./ 0 55. Y.(, Conductance (avg) 3125 Well Pump (if other than Bennet) lG-flAndfo.s Prevo Well Sampled in Sampling Event I -rWLJ '-cX3 pH Buffer 4.0 q.o Well Depth(O.Olft): 1 }3y.~a Casing Volume (V) pH of Water (avg) 4" well:1 1l5 .:X,7 . 1(.653h) 51. gO 3" Well: ....... _O __ ......1.(.367h) Well Water Temp. (avg) 1 1.5.35 Redox Potential (Eh) I,-~_L\_b""","--_""" Turbidity I ~ l-.:J Weather Condo Time 1 1300 I Gal. Purged I 77 Conductance I )If)..Y I pH I ~.b'd... Temp. DC I 1'5.";)1 I Redox Potential Eh (mV) I ~~C:. I < Turbidity (NTU) I :20. I I Time I I~O;l.". I Gal. Purged I 49 Conductance I 31?-,5 I pH I 6 .(;'). Temp. DC I 15 .~q I Redox Potential Eh (mV) I ~'Y'i I Turbidity (NTU) I ;2.?. .1 I White Mesa Mill Field Data Worksheet for Groundwater I I I I Ext'l Amb. Temp. °C (prior sampling event)1 :;J.,Jo Time Gal. Purged L-I Z_g __ ----' Conductance pH I b.b' Temp. DC Redox Potential Eh (mV) I 35t.1 Turbidity (NTU) Time I I~03 Conductance I 3)~J I~J·u I Gal. Purged ...... 11_'_0 __ ---' pHI b.'1 Temp. DC I 15 .3~ Redox Potential Eh (mV) L-13"""o~7:--_......I Turbidity (NTU) 1X4 ·6 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged L..I ....;,J..;...10 ____ .... Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1L----..:.11 __ ----J gallon(s) Time to evacuate two casing volumes (2V) T = 2V /Q = I zL:r.~ -I q . L\ 1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Lab!L.._,v,_'/_A ______ --' Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y N VOCs llJ 0 3x40 rnl 0 19 HCL KI 0 Nutrients fi] 0 100 rnl 0 tJ ' H2SO4 r9 0 Heavy Metals 0 0 250 rnl 0 0 HN03 0 0 All Other Non Radiologies 0 0 250 rnl 0 0 No Preserv. D. 0 Gross Alpha 0 0 1,000 rnl 0 0 HN03 0 0 Other (specify) 1:8 0 Sample volume 0 ~ 0. ill C\'lor; J( If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction '--_______ --IIDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater . 2 of 2 Mill -Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan (QAP) Date: 03/22/2010 Rev. 6 Attachment 1 L~ See instruction Location (well name ):L..I _1_1.,.)_4.:..--_2_" ________ ---' Sampler Name and initials: Date and Time for Purgingj g / I{;' ):;"0 I J and Sampling (if different) lL..::g::..:.J_l1--:....;Ig..~O_1\ ___ ____I Well Purging Equip Used:~pump or@] bailer Well Pump (if other than Bennet) 1 &rv.n ~.f()~ Sampling Event IQ"'CA.(te.r \~ C h I Qro1Onv) ! 'TwLl -2L \ Prevo Well Sampled in Sampling Event 1....-_______ ---' pH Buffer 7.0 1'---'-7 ...;...0 ___ ---' pH Buffer 4.0 y,o Specific Conductance ..... 1 q...;..4 ..... 4 ___ --->1 !!MHOS/ cm Well Depth(O.Olft): 1 .8".00 Depth to Water Before Purginm b'-\,O.3 4" well:! J t1.34 !(.653h) 3" Well: 0 (.367h) 1....---=-_----1 Casing Volume (V) Conductance (avg) pH of Water (avg) 1-1 __ 3_, 3~3 __ ~_.....J Well Water Temp. (avg) 1 )S.f,Z> Redox Potential (Eh) 1 q l\3 Turbidity ..... 1 _:;J.._,_l _---..I Weather Condo Ext'J Amb. Temp. DC (prior sampling event)1 ISO Time 1 O"15~ 1 Gal. Purged 1 '" 1 Time 1 1 Gal. Purged 1 1 Conductance 1 f,5~~ 1 pH 1'3.83 1 Conductance 1 1 pH 1 1 Temp.oC I l5.SJ$ I Temp.oC I I Redox Potential Eh (mV) I '1'-\':> I Redox Potential Eh (mV) I I Turbidity (NTU) I 2. \ I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pHI I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged I If:>..50 Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = 1.-1 ----'.1_1 __ --' gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= I ~.b6 I Number of casing volumes evacuated (if other than two) I LlS If well evacuated to dryness, number of gallons evacuated 1 1f),f,() Name of Certified Analytical Laboratory if Other Than Energy Labl .... _.tI,_'/~ _______ -' Sample Taken Sample Vol (indicate Filtered Preservati ve Preservative Type of Sample if other than as Added y N specified below) Y N Type y N VOCs ~ 0 3x40 ml 0 ~ HCL &I 0 Nutrients D1 0 100ml 0 rn H2SO4 ~ 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologies 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 0 HN03 0 0 Other (specify) ~ 0 Sample volume 0 Ci§ 0 D§ chIO'l'd( If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction L-_______ ---IIDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 ~~::~j)~~ WHITE MESA URANIUM MILL Attachment 1 ~ See instruction MINES FIELD DATA WORKSHEET FOR GROUND WATER Description of Sampling Event: 1 '::/'" a"",o.rt~(" C'hlorl):f'orM ;toll Location (well name): .... 1 _,'-w_I4'--....;:b;....O ________ -' Sampler Name . and initials: I'''''-;=-''' n-n-e-:(';-;~t+o"""I;-\ ,""ia-:-IA. .... ~-:/i'z::;:o't:Ff~----, Date and Time for Purging/ .... ..;:..g ..:..../l~1'-!..1=-~..:....()....;.II ____ ....J Well Purging Equip Used:OOpump o@ bailer Sampling Event 1 QIl\o.f'fe(~ z: h I orof'o(1Y) pH Buffer 7.0 7 .0 Specific Conductance lL....-q_11 ___ --'1 t-tMHOS/ cm Depth to Water Before Purging/ .... _() __ -, Conductance (avg) and Sampling (if different) Well Pump (if other than Bennet) I '}w4--iT Prevo Well Sampled in Sampling Event L..-_______ ----' pH Buffer 4.0 q .o Well Depth(O.Olft): D Casing Volume (V) pH of Water (avg) 4" W ell:~..,.D.----_-;1 (. 653h) 3" Well:. 0 . (.367h) 7. \ I Well Water Temp. (avg) 1.2.4.SLl Redox Potential (Eh) 1 '2.(;,7 Turbidity .... I _O __ ....J Weather Condo Ext'l Amb. Temp. °C (prior sampl ing event)1 CX5D Time 11 4~9 I Gal. Purged I I Time I I Gal. Purged I I Conductance 1 2,<=\ I pHI (.11 I Conductance I I pHI I Temp. DC I £[(\,54 I Temp. DC I I Redox Potential Eh (mV) !2;{,7 I Redox Potential Eh (m V) I I Turbidity (NTU) I 0 I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pH I I Temp. DC I I Temp. DC I I Redox Potential Eh (m V) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1'---_0 ___ ---' gallon(s) Pumping Rate Calculation Flow Rate (Q), in gpm. Time to evacuate two casing volumes (2V) S/60 = 1 0 T=2V/Q= 1 25 1 Number of casing volumes evacuated (if other than two) o If well evacuated to dryness, number of gallons evacuated o Name of Certified Analytical Laboratory if Other Than Energy Lab~,---,/J._V:_rt ______ ---, Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y N VOCs ~ 0 3x40 rnl 0 ~ HCL ~ 0 Nutrients Ttl 0 100 rnl 0 ~ H2SO4 ~ 0 Heavy Metals 0 0 250 rnl 0 0 HN03 0 0 All Other Non Radiologics 0 0 " 250 rnl 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 rnl 0 0 HN03 0 0 Other (specify) ~ 0 Sample volume '0 ~ 0 ,ll Ch\or-idc. If preservative is used, specify Type and Quantity of Preservati ve: Comment ~ See instruction Ac(';\Je.J.. )() }cJ:, ad 14;2.S, ~nl"l-C'r ~nJ. G-c:.rr:1'] fres~n+---tD L:01\cct-'" TDD~ \ Sc:1--eX' ?()(o.rv1 eta.s tNll1 c.Dlle'-+~J. ..$GtMr1es 5-..+ 1'-130. Le~ W cA} )q-SL\. Dr '---_______ ---'IDo not touch this cell (SheetName) White Mesa Mill Field Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) OENISONI)~~ l·----------------~-------ATTACHMENT 1 WHITE MESA URANIUM MILL Attachment 1 ~ See instruction MINES FIELD DATA WORKSHEET FOR GROUND WATER _~_~_,.;f", Description of Sampling Event: I '3" 1\ d\J.wter ell )0(0 f'oflY) =:lOll Sampler Name Location (well name):L-1 _I...:.....-W_Y....:...--...;:b_S ________ --I and initials: I :J3.hY) er 8(1)J,. J11 ITI'; Date and Time for Purgingj '6 /1 sJ ~D J I and Sampling (if different) ~ I /(,/20 IJ Well Purging Equip Used: [1[]pump or@] bailer Well Pump (if other than Bennet) I &-rlAt\~tc0 Sampling Event I Q"'(A.(h:.(\~ Ghlo,..o+o('", Prevo Well Sampled in Sampling Event I TW1.\ -I L/ pH Buffer 7.0 Specific ConductanceI-I --,-9_~~..:....-__ --,I~MHOS/ cm Depth to Water Before Purging] 6S. t.\ 0 Conductance (avg) pH Buffer 4.0 1..\.0 Well Depth(O.Olft): \jY. DO Casing Volume (V) pH of Water (avg) 4" well:1 ~ 1. 7'.:> 1(·653h) 3" Well:I-. __ D _----I. (.367h) Well Water Temp. (avg) I ,,;.(4 Redox Potential (Eh) I 194 Turbidity I :;.2?... Weather Condo Ext'l Amb . Temp. O( (prior sampling event)1 :;....r:/' Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pH I I Temp.oC I I Temp.oC I I Redox Potential Eh (m V) I I Redox Potential Eh (mY) I I Turbidity (NTU) I I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pH I I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mY) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet-for Groundwater 1 'of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged ..... 1 _7 .......... 1'--__ ..... Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = ...... 1 --->.1_1 __ ---' gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= 1 5.77 1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy Labl ......... tI_I.:../l,'--______ --' Sample Taken Sample Vol (indicate Filtered Preservative Preservative Type of Sample if other than as Added y N specified below) y N Type y N VOCs 51 0 3x40 ml D C)I HCL ~ 0 Nutrients [J 0 100ml 0 51 H2SO4 III 0 Heavy Metals 0 0 250 ml 0 0 HN03 0 0 All Other Non Radiologics 0 0 ·250 ml 0 0 No Preserv. 0 0 Gross Alpha 0 0 1,000 ml 0 Q HN03 0 0 Other (specify) L5J 0 Sample volume 0 ~ 0 ~ c h \Of\Je If preservative is used, specify Type and Quantity of Preservative: Comment ~ See instruction '--________ ..... IDo not touch this cell (SheetName) White Mesa Mill J'ield Data Worksheet for Groundwater 2 of 2 Mill -Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) ATTACHMENT 1 ~~15~J:)~~ LMINES. FIELD DATA WORKSHEET FOR GROUND WATER WHITE MESA URANIUM MILL Attachment 1 ~ See instruction Description of Sampling Event: 13("JI Q",o.r:te(, c.hlorb+O(fI'I ;2..01\ Location (well name): ..... 1 _T_w_Y_-_7_D ________ ----' Sampler Name and initials: I~nfle(' H () 11, J~/,..}J Date and Time for Purgin~1_~-'/:...../_b_I_~_Jl ____ _' and Sampling (if different) «/ J7/:::z..0 I } Well Purging Equip Used: [!D pump or@] bailer Well Pump (if other than Bennet) 1 {f(\IIr'! {ffD~ Sampling Event 1 Qv...~('+e-d.~ L,}-, loro+o(rV) Prevo Well Sampled in Sampling Event I -r-v-lY--' pH Buffer 7.0 1-1 _1_,.....;;(J'---_----' pH Buffer 4.0 ~.O Specific Conductance ..... I.....j4_Q_Q ___ ---JI""MHOS/ cm Well Depth(O.Olft): \Li;2..00 Depth to Water Before Purgingj b~. k5 Casing Volume (V) 4" well:1 S \. b~ 1(·653h) 3" Well: C _ (.367h) '-------' Conductance (avg) 1 pH of Water (avg) Well Water Temp. (avg) 11L\· f(;L Redox Potential (Eh) ..... 1 '-_b 7 __ _, Turbidity 11-'-1....:.-4 __ --, Weather Condo Ext'l Amb. Temp. DC (prior sampling event)1 ;l-3° Time 1 I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pH I I Temp.oC I I Temp.oC I I Redox Potential Eh (mV) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I Time I I Gal. Purged I I Time I I Gal. Purged I I Conductance I I pH I I Conductance I I pH I I Temp.oC I I Temp.oC I I Redox Potential Eh (m V) I I Redox Potential Eh (mV) I I Turbidity (NTU) I I Turbidity (NTU) I I White Mesa Mill Field Data Worksheet for Groundwater 1 of 2 Mill-Groundwater Discharge Permit Date: 03/22/2010 Rev. 6 Groundwater Monitoring Quality Assurance Plan (QAP) Volume of Water Purged 1 I '3~ Pumping Rate Calculation Flow Rate (Q), in gpm. S/60 = ..... 1 _1_1 __ .--I gallon(s) Time to evacuate two casing volumes (2V) T=2V/Q= 1 Ci.31 1 Number of casing volumes evacuated (if other than two) If well evacuated to dryness, number of gallons evacuated Name of Certified Analytical Laboratory if Other Than Energy LablL..;tI:...:....;../fo~ ______ --1 Sample Taken Sample Vol (indicate Filtered Preservative Preservati ve Type of Sample if other than as Added y N specified below) y N Type y N VOCs 1$J 0 3x40 ml 0 129 HCL fj 0 Nutrients IB 0 100 ml 0 ~ H2SO4 f9 0 Heavy Metals 0 0 250ml 0 0 HN03 0 0 All Other Non Radiologies 0 0 250ml 0 0 No Preserv. 0 0 Gross Alpha ·0 0 1,000 ml 0 0 HN03 0 0 Other (specify) [£] 0 Sample volume 0 ~ 0 ~ L-h lor; J( If preservati ve is used, specify Type and Quantity of Preservative: Comment ~ See instruction '--________ ..... IDo not touch this cell (SheetName) White Mesa Mill ~ield Dafa Worksheet for Groundwater 2 of 2 TabC Weekly and Monthly Depth to Water Data Depth to Water Ime WII e D th ep' c t ommen s Jell g MW-4 7 1:zo Flow I.{.t bPA Meter 51'l!1'd..<6 ,5S' ., Jo ~S MW-26 75, ,'/ Flow l -'-.2-tIN I'· Meter 5~5 7J·S<i ID/'1 TW4-19 '3.~(, Flow 1;)..1/ 1?(J,4 . Meter //:; tt6Lf 75.21 /n 1/1) TW4-20 ~I1A A.~"J iii r Flow 10 6P;t1 o , 't~.2 I Meter ~(j 7 hSg.9 h jD~5 TW4-4 b'J.5l Flow g .--'i 6 P fo1 Meter 431,165.1 Water: 66t.J (, ~ ~ o ... Depth to Water o Date i-I( -c70 It Time Well DeDth Comments ID ~7 MW-4 7 /) 7r. Flow 1./ G, f i't Meter I}z!Jb1l5., h 10 ",0 MW~26 /7.0 1 Flow G.f MM Meter b31 66 1 <i"_ /oSo TW4-19 6 1.45 Flow I/. l.j 6f' /1 Meter · /70' S 't~, JL.J I/)'" n TW4-20 b3.1 ~ Flow q .. z. C9f>,A1 Meter .i?525 8t:J.,,~ o .. Ilo~D TW4-4 70 .,/3 Flow I O.~ ~Pft/ Meter '11 ~7 ~5 . b Water: bO'tO"i O .. --" I L~) C) Depth to Water Date 71ft ! ~o \I Name ~onif Me I I.'. Ime WII e D th eD' c t ommen s 'Oc..:~, MW-4 "1J.05 Flow ~~ G-P.at\ Meter .s~15 7~.~O 0';1$ MW-26 '11.'" Flow ~.o ""PM Meter G, ~ ~"b.E'i l'i ~ TW4-1 9 13.&.1.5 Flow I '1.~ 6-PM. Meter /7 ( &5 '1 8 .~t.f o "X1. TW4-20 '8.bl Flow 10.\of &opM Q Meter :tSKOX1.~1..( oC:,~~ TW4-4 ~f5Ji3 Flow J l.~ (,.p~ Meter ~%:l.q ,.' . Water: ~l bOlg ~ , it; ~ ~."II """\'11' -:\ '-C> Co ('.0 o Depth to Water Date 7/xsl:Jl>11 T" Ime WII e D th eD' c t ommen s 0"11 MW-4 71.:lD Flow Lt. L{ ("PPl Meter 5381S'1.b8 b 'l ~ MW-26 43·1 ~ Flow b.c:t c,.P M Meter '342.'LO I 06Lf5 TW4-19 Sg.30 Flow 1729,"1'14.'10 Meter 1'1..3 6_P A 0'"011\ TW4-20 73.ctS Flow IO.!t c,.PM o Meter 2~ 31 <II. 4"1 O~\ TW4-4 b8.tt5 Flow 10 .f< (rf>~ Meter ~S'1115 .5 Water: f,)'7q~o o C) o o Date ct /1 120 t ( Time Well }O '5 A MW-4 IO .1h MW-26 121~ TW4-19 iD 2 ?--TW4-20 10 ~7 TW4-4 Water: Depth to Water DeDth Comments 70~ 7l Flow L.-\ /, (., (J #\ Meter .s ~g 6'1 . Y ~ 7/,15 Flow h,;S 6P~ Meter 7gf)()3o!;, 7 7 ·7.15 Flow l~.q ~PM Meter \ 7 L{ \ I~ \ . q ::2 \ \ h s .06 Flow 10 Sa £P~ Meter .2696/ Z q'-l . 6 1.g7 Flow 13 '0. (;) !';Pj1J\ Mete r L.J6 ;2.3 15J f ) S t§3Lf;)S 7 Depth to Water Date SJ tJ2-Dl( ~ , Name be. era'l\ -e I vVler Time Well DeDth Comments ILJDl MW-4 7q no Flow Li .3 cPA Meter 5 512LiY AS 141\ MW-26 7 1.IIJ Flow 6.6 Meter g'LJ26Q 71 I L-{ Jt; TW4-19 61 v 2C1 Flow ~_/Yt>:2-b~ Meter ~ ..:">. -T_..I~,.-r).. ~ -:A J L1JA TW4-20 h i ~5 Flow 6L&'C; ID~3 ~f)/l C) -Meter 'J-7 ~ ~5Y _ 3'-i IYOY TW4-4 7o~ 12--Flow q,< GP~ Meter Y70~7 7 'l Water: A ~q3>3 o ~ o () Date 55 //5/)jj 1/ I J ~ Time Well IS!/ MW-4 IS-a L/ MW-2 6 I,~JO TW4-19 /iJ.5:2 TW4-20 () g:~() ~ Vitia II )5.20 TW4-4 Water: Depth to Water Name XI ,WfI1E(i, DeDth omments b 7, Os Flow 'l '7 I,PfV\ Meter 6383h2,. r tf(, %/ Flow 6, g &rJfVl Meter '61'~ 7¥'. ~ 51. 1 .. 5 Flow I If .. ;2 (""11111 Meter I?i 'ihh;l. .. It I I ilarl4 'l.t? fJ, IkrINL Flow!J,uA-hlc .)f tt J a-~ ff'j It f5! ()# / 2:7. c,~ \ Meter 2 f; /()t, -:f-" S- 19-/J~/?~/1 ) Lff/6lfl!. ~ ,? ) It /2(}t/ 'l}' c<;l Flow jj, ij?;M Meter tfl1rfJ6, 'I ;; L/5&51 I () Date r/2Ut( , Depth to Water ... ~ame . 6vt';tAy .&.~(t.- Time Well Depth Comments JJ~2 MW-4 7t~1 Flow 3.1 6 r~ Meter 5,~o.s6.hJ r 2CJ~ MW-2 6 b Cf. -,s, Flow 6. > 6 P.,v\ Meter QY8'3tJ'"-:S~ 1')15 TW4-19 ~J1..qD Flow 14.0 C;P".v\ Meter t::z2Sh 13 . 7' ULtc. TW4-20 '=J 2.4 0 Flow 'to q GP/"\ o Meter Ui54 £/. qy \l ~-l TW4-4 ,(q ~l Flow iO. l ~f".v\ -Meter l.f BY." I I tJ Water: 6 l1 'l IYO () o o o Date g/).q / tl Time Well lL.l/')( MW-4 \357 MW-26 1 3.2~ TW4-19 1.353 TW4-20 111 C> L.\ TW4-4 Water: Dep th to Water Name ~r:V\-e tt4<\e..v- Depth Comments 7 £.52-Flow y .:> 6 P~ Meter S 7 J 7 .... 2J ~ :st 7 1 ~ /~ Flow b ,g" GP,N<. Meter \0£23 ]15 l..--12 ~·2. 80 Flow '~ ... I AP'p\ Meter 17874()L{ q;Z 6 (.60 Flow 10.5 hPA Meter :2 92 1~'. 3S 8't..L ~£1 Flow t . h i9PJVl- Meter !--1q:z ~q 5-:2S 66J~;20 . o Depth to Water Date al i 1J.01 f Name :Unocr H.ll,;J~, fn",.n ft.',.", T-W II Ime e D th ep' C t ommen s osS! MW-4 7 r b Flow 2.5 ~PM Meter ~15~&.fi 010~ MW-26 "K.5' Flow !..~ G.PI"1 Meter f 0., O~i . ~ 0·130 TW4-19 61. 2?-Flow Il-/. ~ 6P~ Meter I X'D 270D 0111 TW4-20 g 10, Flow 10 .0 {rPM o --Meter :t~<f!2a7_0' 0&58 TW4-4 78 .!>'1 Flow g .0 ("'PM Meter _.;o~.7 ., Water: 6b q_L1 ~O o o Depth to Water Date q -! ?. -2-0 II Name 6 4 ("'(':.A-ftA-lMe,C TO Ime WII e o th ep' c t ommen s I~I MW-4 71 Lq Flow 4 .5 bPM Meter .5 ~J?Y 1. 3 7 IDSS MW-26 72.4 0 Flow 7. 6 6 1' ..f/\ Meter J1 0 !i L9~~ 10'25 TW4-19 1-10.S '1 Flow 1 L1 5 G f.;V\ Meter J g'loO IO.SF II7L;n TW4-20 AI.gD Flow 9 . 6 (-,/J ~ o Meter 3 D 3 .2 ;;2.Q.Sq I2.D4 TW4-4 7 1,5 0 Flow II. () 6 PA Meter ~o 73 qc,. '1 1 Water: A 7~LJ 1O o Date .9... , q" r f Depth to Water Name {)o..,,; "'-fl l v0-v Ime WII e D th eD! c t ommen s 1.2. L5 MW-4 71 .3 0 Flow ~ b.~ &'PM Meter 5~ IS 30. 0 4 t2.o ~ MW-26 b't .go Flow (,3 rrPM Meter 11 b3 ;tb.;l..R ()qLfO TW4-19 5cr.;.::~ Flow \4,6 AP8 Meter IK2 1 LJ 3 5_ \0 v.:tc> 1..\ TW4-20 1S,~~ Flow /0 .' C-PI'1 o Mete r 10 Z1;2. '-f .].h \.lJil JaoIO', TW4-4 7 5 ·15 Flow 10·7 &P M \2~o Meter .51Y Q gg .7 Water: £8136'7 o C) Depth to Water Date _ q. ~ 6· ! [ N /' /} l -~ ame Up:cr-j.c.. ~ vv\.eJ ') r A. .... ~ }-k.u :. Time Well nl--.LI. .leal" Comments 120Ll MW-4 ,I r3 Flow _3 t') GP~ Meter .5 q .$;'2 20.<'h J 202 MW-26 J:7 Cf'-l FloW Ah ~-V~ Meter 1 ~1 7 8'tt L-\ \ 192c.. TW4-19 60.IS Flow ILLS Meter ~1 ~3.3f?l? q l ~O(') TW4-20 7g.~c; Flow to.2 liP/i1 Meter "3, ILlI!, S J t'J S? .-I ZIO TW4-4 7c>. L{""3: Flow 10 .0 Meter 5 2':J...t; / h. tt I / Water: h ~3-Yil J; G~ d. +I()~ ~ Mt..+e..r 01"-t\..Jt..l~ICl.F.oI\.~\ i""e..,.).; Wtl.,.S -J'l\e.te..r \,Jfi..} c..~~ be.l.CW 5<:'" i +-LJA...,S tke.-\I\.c$e... ()tf\. ".~~-1l ~ OqOO. 19 ,64 o o 0 ~ 1( lb . J Date ~-r, -s; ,;2(/// Time Well f\l~ ~ MW-4 ()17q MW-26 ~/~/n TW4-19 (\ '1 2 () TW4-20 11J11./£., TW4-4 W ater: 3tO?l-/1 2&' 'I ~fvO Dep th to Wate r Name 1?r dlr ,& DeDth Comments 70. ":;2 Flow 5"~ t &/Jff\. Meter h () 1./ "7rll# ;], 60~ & (., Flow 7,·L t,lfYl Meter 12'11'11. ~ 1/- to. 17 Flow It!. if L-1'lh1 / Jtt~1 L~ t4J (' Meter "72S 7 ,[c() \ () ~ J ('II.(n l lIN Ig~55011,,'1'¥ ~ ~ C/.7f Flow LO. 2 0~rVl Meter :~/'1qll1r1 J.- ~ g~ 15' Flow 1 II ltPtv1. Meter 6' :2ilL1~1 /'~xt g9 CI, () t.Z--0 C3-{; 7 tI q'lll, 'f5 .st';~$ TabD Kriged Current Quarter Groundwater Contour Map, Details Map, and Depth to Water Summary Static Quarterly Depth to Water NAME: Tanner Holliday, Garrin Palmer DATE: 9/20/2011 TIME WELL level TIME WELL Static Level TIME WELL 829 MW-l 64.64 1213 MW-4 71.19 844 PIEZ-l 1246 MW-2 109.74 1209 TW4-1 64.45 840 PIEZ-2 1256 MW-3 83.33 1215 TW4-2 67.26 1156 PIEZ-3 1257 MW-3A 85.45 1204 TW4-3 49.53 1230 PIEZ-4 1322 MW-5 106.15 1220 TW4-4 73.01 1234 PIEZ-5 1326 MW-11 88.65 1200 TW4-5 56.08 1319 MW-12 108.40 1223 TW4-6 70.41 1210 TWN-l 1330 MW-14 103.72 1211 TW4-7 67.61 1400 TWN-2 1333 MW-15 106.35 1207 TW4-8 66.77 1214 TWN-3 1252 MW-17 75.51 1202 TW4-9 54.07 1152 TWN-4 836 MW-18 70.25 1158 TW4-10 56.00 830 TWN-5 842 MW-19 51.84 1217 TW4-11 57.59 824 TWN-6 951 MW-20 87.29 1240 TW4-12 39.91 832 TWN-7 944 MW-22 67.20 1242 TW4-13 46.31 822 TWN-8 1251 MW-23 114.26 1245 TW4-14 87.32 847 TWN-9 1226 MW-24 114.45 1156 TW4-15 73.99 818 TWN-l0 1340 MW-25 74.56 1326 TW4-16 62.50 812 TWN-11 1156 MW-26 73.99 1328 TW4-17 76.05 810 TWN-12 1221 MW-27 51.11 1207 TW4-18 56.57 848 TWN-13 1235 MW-28 76.88 1405 TW4-19 63.55 851 TWN-14 1242 MW-29 102.22 1154 TW4-20 81.03 816 TWN-15 1239 MW-30 76.35 1204 TW4-21 54.55 856 TWN-16 1333 MW-31 68.75 1152 TW4-22 53.94 855 TWN-17 1328 MW-32 76.05 1224 TW4-23 65.47 1148 TWN-18 1302 MW-33 dry 1150 TW4-24 55.64 807 TWN-19 1304 MW-34 107.80 1202 TW4-25 46.83 1255 MW-35 112.20 1227 TW4-26 64.09 1258 MW-36 110.30 1308 MW-37 109.24 Comments: Static Level 61.74 17.79 40.96 48.42 43.21 50.77 16.90 32.10 39.05 69.67 74.59 88.80 61.66 63.41 81.06 69.57 31.80 46.29 62.80 92.12 47.96 34.15 57.80 52.19 TIME 737 740 815 750 747 744 800 803 806 733 755 730 718 715 707 710 725 WELL Static Level DR-l ABANDON DR-2 ABANDON DR-3 MW-36 DR-4 MW-37 DR-5 83.23 DR-6 94.41 DR-7 92.15 DR-8 51.11 DR-9 86.63 DR-l0 78.00 DR-11 98.34 DR-12 87.19 DR-13 70.12 DR-14 76.49 DR-15 93.01 DR-16 ABANDON DR-17 64.85 DR-18 ABANDON DR-19 63.35 DR-20 55.91 DR-21 101.65 DR-22 DRY DR-23 70.78 DR-24 43.88 DR-25 ABANDON PROPERTY BOUNDARY \\ \\ \\ MW·01 .5583 MW-18 .5587 ~5586 TWN-10 TWN-11 TWN.12/ T ~561~ ~56~6/ '6'07,(;) ~558 TWN-14 ~5584 TWN-9 PIEZ-1i----.....L-l- ~5594 f' L "-/ "-I \ ( PI~ 11 J ~ o MW-22 .5450 TW4-1 0 5554 PIEZ-l . " 5594 ·TWN-4 ~ 5603 MW-34 -¢-5492 MW-36 ~5493 MW·02 .5503 ~5~ N-4 / ./ MW.B5 -¢-r 94 MW.36 CELL NO. 48 $6: $93 N SCALE IN FEET EXPLANATION perched monitoring well showing elevation in feet amsl temporary perched monitoring well showing elevation in feet amsl perched piezometer showing elevation in feet amsl temporary perched nitrate monitoring well showing elevation in feet amsl perched monitoring well installed August/September, 2010 showing elevation in feet amsl perched monitoring well installed April, 2011 showing elevation in feet amsl MW-03 .5471 3000 ;? ;? j¥.:::::::===== ___ -----552 \ ~ ij/ -=--=. -::::. -=--=--=--=--=--=--=-- --=--=--=--=--=- "-~-,:::::.-~ $<16'0 HYDRO GEO CHEM, INC. MW.22 ~ II .5450 "" // // // // // // // // // // NOTE: MW-4, MW-26, TW4-4, TW4-19 and TW4-20 are pumping wells KRIGED 3rd QUARTER, 2011 WATER LEVELS WHITE MESA SITE APPROVED DATE REFERENCE FIGURE SJS H:/718000/nov11 /wI0911.srf D-l . ,', N MW-02 8 5503 PROPERTY BOUNDARY MW-03 8 5471 MW-20 8 5453 \\ \\ \\ MW-01 8 5583 MW-18 8 5587 TWN-11 TWN-12/ T ~561~ ~56T6/ ~o1-ru ~5586 TWN-10 ~5584 TWN-9 PIEZ-1~---_.l.-!­ .. 5594 1 ij" -=--=--:::::.. -=--=--=--=--=--=--=-. -=~.-=-4 L:-v"Sf6'O ~! ___ ~~~~§iIii ___ ! o 3000 MW-22 .5450 TW4-1 0 5554 PIEZ-1 '" 5594 TwN-4 ~5603 SCALE IN FEET EXPLANATION perched monitoring well showing elevation in feet amsl temporary perched monitoring well showing elevation in feet amsl perched piezometer showing elevation in feet amsl temporary perched nitrate monitoring well showing elevation in feet amsl perched monitoring well installed August/September, 2010 showing elevation in feet amsl """ " " ,'," estimated capture zone " " ,'," boundary stream tubes I I I , resulting from pumping HYDRO GEO CHEM, INC. MW-22 "" II 85450 '" // // // // // // // // // // NOTE: MW-4, MW-26, TW4-4, TW4-19 and TW4-20 are pumping wells KRIGED 3rd QUARTER, 2011 WATER LEVELS AND ESTIMATED CAPTURE ZONES WHITE MESA SITE APPROVED DATE REFERENCE FIGURE ( MW-34 -<r 5492 MW-36 ~5493 perched monitoring well installed April, 2011 showing elevation in feet amsl SJS H:/718000/nov11/wI0911cz2.srf 0-2 7 EXPLANATION " ,--,----" " " ", estimated capture zone " " ,',' boundary stream tubes I I I I resulting from pumping <> TWN-1 temporary perched nitrate monitoring . 5597 well showing elevation in feet amsl o TW4-1 temporary perched monitoring well 5554 showing elevation in feet amsl • MW-32 perched monitoring well showing 5549 elevation in feet amsl N t T ! ! o 150 300 SCALE IN FEET NOTE: MW-4, MW-26, TW4-4, TW4-19, and TW4-20 are pumping wells HYDRO GEO CHEM, INC . SJS KRIGED 3rd QUARTER, 2011 WATER LEVELS AND ESTIMATED CAPTURE ZONES WHITE MESA SITE (detail map) REFERENCE H:/718000/nov11/wI0911 cz.srf FIGURE 0-3 TabE Kriged Previous Quarter Groundwater Contour Map PROPERTY BOUNDARY \\ \\ \\ II II II II II II II '/ MW-01 eND MW-18 eND ~~ <>NS TWN-15 <>NS TWN-10 <>NS TWN-11 <>NS TWN-14 <>NS TWN-9 <>NS TWN-6 PIEZ-1 <INS <>NS MW-19 TWN-8 eND <>NS TWN-12 f' <>NS II <>NS TWN-18 TWN-7 II <>NS /L « TWN-3 PIEZ-2 ( ~ <INS o MW-4 .1700 TW4-1 0 1200 PIEZ-1 Q NS .TWN-4 . ~ NS MW-34 -9-ND MW-36 ~ NS N SCALE IN FEET EXPLANATION perched monitoring well showing concentration in uG/1 temporary perched monitoring well showing concentration in uG/1 MW-2 MW-02 eND MW-03 e ND MW-20 eND 3000 perched piezometer (not sampled) temporary perched nitrate monitoring well (not sampled) perched monitoring well installed August/September, 2010 showing concentration in uG/1 perched monitoring well installed April, 2011 (not sampled) MWoffo .w ONS r-~ cf M1tt2~TE <>N PIEZ-3 CELL NO.1 TWN-<INS 0 CELL NO.2 MW-17 e ND 33 ND 0 00 m g-14 4-6 o TW4-23 TW~326 PIEZ-4 <INS # PIEZ-5 <INS T37S T38S II ~~ ~~=====4============l "'--===- HYDRO GEO CHEM, INC. MW-22 eNS II // // // // // // // // // ~ // ~ NOTE: MW-4, MW-26, TW4-4, TW4-19 and TW4-20 are pumping wells KRIGED 2nd QUARTER, 2011 CHLOROFORM (uG/L) WHITE MESA SITE APPROVED DATE REFERENCE FIGURE SJS H:/718000/aug11 /chI0611.srf E-1 . ,', TabF Hydrographs of Groundwater Elevations Over Time for Chloroform Monitoring Wells Depth Below Measuring Point (ft.) 0 09/25179 02/06/81 06/21182 11103/83 03/17/85 07/30/86 12/12/87 04/25/89 ~ 09/07/90 ~ ~ 01120192 ~ f""I" ~ 06103/93 ~ ~ 10/16/94 ~ ~ ;. 02128/96 0 < ~ 07/12197 ~ ~ .... 11124/98 = ~ -.. 04/07/00 ~ r:' 08/20101 -= ~ 01102103 '-" 05/16104 09/28/05 02/10107 06/24/08 11106109 03/21111 08/02/12 12/15113 Depth Below Measuring Point (ft.) VI VI VI 0 11108/99 04/06/00 09/03/00 01131/01 06/30/01 11127/01 04/26/02 09/23/02 02/20/03 t-3 07/20/03 ~ "'" 12/17/03 I ~ 05/15/04 ~ '""" 10/12/04 ~ '"'l 03/11105 ~ ~ ~ 08/08/05 '""" =- 01105/06 0 -< 06/04/06 ~ '"'l t-3 11101106 .... !3 03/31107 ~ -- 08/28/07 ~ r::J" -01125/08 !3 ~ 06/23/08 '-" 11120/08 04/19/09 09/16/09 02/13/10 07/13/10 12/10/10 05/09/11 10/06/11 03/04/12 08/01112 Depth Below Measuring Point (ft.) VI 0 11108/99 04/06/00 09/03/00 01131101 06/30101 11127/01 04/26/02 09/23102 02/20103 l-3 07/20103 ~ .a;. 12117/03 I N 05/15/04 ~ f""I" 10112/04 ('D "1 03/11105 ~ ('D "0 08/08/05 :;. 01105106 0 ~ 06/04/06 ('D "1 l-3 11101106 ..... 9 03/31107 ('D --08/28/07 ? 0--01125108 9 "0 06/23/08 '-' 11120108 04119/09 09/16/09 02/13110 07/13/10 12/10/10 05/09/11 10106111 03/04112 08/01112 Depth Below Measuring Point (ft.) .j::.. 0 11/29/99 04/27100 09124/00 02/21101 07/21101 12118/01 05117/02 10114102 03113/03 ~ 08/10103 ~ ~ 01107104 I ~ 06105/04 ~ ..... 11102104 ~ "1 04/01105 ~ ~ ~ 08/29/05 ~ 01126106 0 -< 06125/06 ~ "1 ~ 11/22/06 .... a 04/21107 ~ -- 09118/07 ? r::::r -02115/08 a ~ 07114/08 '-..-' 12111108 05110109 10107/09 03/06/10 08/03110 12/31110 05/30111 10127111 03125112 08/22112 Depth Below Measuring Point (ft.) Vl 0 05/25/00 09102/00 12111100 03/21101 06/29101 10107101 01115/02 04/25/02 08/03102 11111102 02119/03 05/30103 09107/03 t-3 12116103 ~ ~ 03/25/04 I ~ 07/03/04 ~ 10111104 f""Io. 01119105 t'D ~ 04129105 ~ 08/07/05 t'D "'Cl f""Io. 11115105 =-02/23/06 0 06/03/06 -< t'D 09111106 ~ t-3 12/20106 ..... 9 03/30107 t'D 07/08/07 ,-., ~ 10116/07 r::r 01124/08 -9 05/03/08 "'Cl '-" 08111108 11119108 02/27/09 06/07/09 09115109 12/24/09 04/03110 07112110 10/20110 01128111 05/08/11 08116111 11124/11 03/03112 06/11112 Depth Below Measuring Point (ft.) U\ 0 01102/00 04111100 07/20100 10/28/00 02/05/01 05116101 08/24/01 12/02/01 03112102 06/20102 09/28/02 01106103 04116/03 ~ 07/25/03 ~ 11102103 ~ I 02110104 Ul 05/20104 ~ 08/28/04 """ ~ 12/06/04 ~ 03/16/05 ~ ~ 06/24/05 "0 """ 10102/05 =- 01110/06 0 < 04120106 ~ ~ 07/29106 ~ .... 11/06/06 :3 02114107 ~ ~ 05/25/07 ~ 09/02/07 r: -12/11107 :3 03120108 "0 "-' 06/28/08 10106/08 01114/09 04124/09 08/02/09 11110/09 02118110 05/29/10 09/06110 12/15/10 03/25111 07/03/11 10111111 01119112 04/28112 ., 00 VI , ~. 4 ~ 00 o Depth Below Measuring Point (ft.) t \ ~ ~ -J o l..---- ~ 0\ o ----- VI VI ~ VI o - OS/25/00 09/02/00 12111100 03/21101 06/29/01 10107101 01115/02 04/25/02 08/03/02 11111102 02/19/03 05/30103 09/07/03 12116103 03/25/04 07/03/04 10111104 01119/05 04/29/05 08/07/05 11115105 02/23/06 06/03/06 09111106 12/20106 03/30107 07/08/07 10/16/07 01124108 05/03/08 08111108 11119/08 02/27/09 06/07/09 09115109 12/24/09 04/03/10 07112110 10/20110 01/28111 05/08/11 08116111 11124/11 03/03112 06/11112 ~ ~ ,&;;;.. I 0"1 ~ ""'" ~ '"'l ~ ~ "0 ""'" =-0 -< ~ '"'l ~ 1-/. S ~ --? 0--S "0 '-' Depth Below Measuring Point (ft.) VI 0 11/29199 03/08/00 06116/00 09/24/00 01/02/01 04/12/01 07/21101 10129101 02/06/02 05117102 08/25102 12/03/02 03113103 ~ 06/21103 ~ 09/29103 .&;;;.. 01107/04 I ......:J 04116/04 ~ 07/25104 ~ 11102104 ('D "'1 02110105 ~ 05/21/05 ('D "0 08/29105 ~ =-12/07/05 0 03117106 ~ ('D 06/25106 "'1 10/03106 ~ .... 01111107 9 ('D 04/21107 -.. 07/30107 ? 11107107 r::J" -02115108 9 "0 OS/25108 '-" 09102/08 12/11108 03/21109 06/29109 10107109 01115110 04/25/10 08/03110 11111110 02/19/11 05/30111 09107111 12/16/11 03/25/12 07/03112 Depth Below Measuring Point (ft.) 0\ 0 11129/99 03/08/00 06116/00 09/24/00 01102101 04112/01 07/21101 10129/01 02/06/02 05117102 08/25/02 12/03/02 03113103 1-3 06/21103 ~ 09129/03 ,&;;.. 01107/04 I 00 04116/04 ~ 07125/04 ..... 11102/04 ~ "1 02110/05 ~ 05121105 ~ ~ 08/29/05 ;. 12/07/05 0 03117106 < ~ 06/25/06 "1 10/03/06 1-3 ... 01111107 9 ~ 04121107 -.. 07/30/07 ? 11107107 ~ -02115/08 9 ~ 05/25/08 '-' 09/02/08 12111108 03121/09 06/29/09 10/07/09 01115110 04/25110 08/03/10 11111110 02119111 05/30111 09/07111 12116111 03/25112 07/03112 Depth Below Measuring Point (ft.) -..l 0\ 0\ 0\ 0\ 0\ Vl Vl Vl Vl Vl 0 00 0\ +>-N 0 00 0\ +>-N 0 12120/99 03129/00 07/07/00 10/15/00 01123101 05/03/01 08/11101 11119101 02127/02 06/07/02 09115102 12124/02 04/03/03 ~ 07112103 ~ 10/20103 ~ 01128104 I \0 05/07/04 ~ 08115104 f""I" 11123/04 ~ "1 03/03/05 ~ 06111105 ~ "0 09119/05 f""I" =-12128/05 0 04/07/06 ~ ~ 07116106 "1 10124/06 ~ .... 02/01107 9 ~ 05112/07 --08/20107 ? 11128/07 0" -03/07/08 9 "0 06115108 '-" 09/23/08 01101109 04111109 07/20109 10/28/09 02/05110 05116110 08/24110 12/02110 03112111 06120111 09/28111 01106112 04115112 07124112 Depth Below Measuring Point (ft.) VI VI VI VI VI VI VI \0 00 -..] 0\ VI .j::>. (,;) 01103/02 04113/02 07/22/02 10/30102 02/07/03 05118103 08/26/03 12/04/03 03113104 06/21104 09/29/04 ~ 01107/05 ~ .I:;. 04117/05 I ~ 07/26/05 ~ 11103/05 ~ f"'Ioo 02/11106 ('I> "'1 05/22/06 0 ('I> 08/30106 "t:! 12/08/06 e- O 03/18/07 -< ('I> 06/26/07 "'1 10104/07 ~ .... = 01112108 ('I> -.. 04/21108 ? 07/30108 0--11107/08 = "t:! 02/15/09 '-' 05/26/09 09/03/09 12/12/09 03/22/10 06/30110 10108/10 01116111 04/26/11 08/04/11 11112111 02/20/12 05/30/12 Depth Below Measuring Point (ft.) 00 -J -J 0\ 0\ Vl Vl 0 Vl 0 Vl 0 Vl 0 01103/02 04/13/02 07/22/02 10/30/02 02/07/03 05/18/03 08/26/03 12/04/03 03/13/04 06/21104 09/29/04 ~ 01107/05 ~ .&;;.. 04/17/05 I ~ 07/26/05 ~ ~ 11103/05 f""I" 02/11106 t'e ""t OS/22/06 ~ t'e 08/30/06 "0 12/08/06 ;. 0 03/18/07 ~ t'e 06/26/07 ""t ~ 10104/07 .... 9 01112108 t'e --04/21108 ? 07/30/08 r:r -11107/08 9 "0 02/15/09 '"-' OS/26/09 09/03/09 12/12109 03/22/10 06/30/10 10/08/10 01/16/11 04/26/11 08/04/11 11112/11 02/20/12 --05/30/12 Depth Below Measuring Point (ft.) VJ .j::. 08/23/02 12/01/02 03111/03 06/19103 09/27/03 01/05104 04/14/04 07/23/04 10131/04 02/08/05 1-3 05119105 ~ 08127/05 .a;. I I--' 12/05/05 N ~ 03115106 f""Io. 06/23/06 ~ "'1 10101/06 0 ~ 01/09107 "'0 f""Io. =-04119107 0 -< 07128/07 ~ "'1 11/05/07 1-3 ... 02113108 :3 ~ 05/23/08 ,-... ~ 08/31/08 0--12/09108 :3 "'0 03/19109 '-' 06/27/09 10105/09 01/13110 04/23110 08/01110 11/09110 02117111 05/28111 09105111 12114111 l.....-__ -'--_--l.. __ --'L..-_..J __ --I-.__ _ __ -l.-_--l.._---I_. 03/23112 Depth Below Measuring Point (ft.) ....... 0 \0 00 --.l 0\ VI .j::. 0 0 0 0 0 0 0 08/23/02 12/01/02 03/11/03 06/19/03 09/27/03 01/0S/04 04/14/04 07/23/04 10/31/04 02/08/0S ~ OS/19/0S ~ "'" 08/27/0S I ~ (.H 12/0S/0S ~ 03/1S/06 ~ ('tI 06/23/06 "'1 10/01/06 ~ ('tI "0 01/09/07 ~ =- 04/19/07 0 -< 07/28/07 ('tI "'1 11/0S/07 ~ .... 02/13/08 9 ('tI --OS/23/08 ? 08/31/08 "a" -12/09/08 9 "0 '-' 03/19/09 06/27/09 10/0S/09 01/13/10 04/23/10 08/01/10 11/09/10 02/1 7/11 OS/28/11 09/0S/11 12/14/11 03/23/12 Depth Below Measuring Point (ft.) 00 0\ 08/23/02 12/01102 03/11103 06/19/03 09127/03 01105/04 04/14/04 07/23/04 10131104 02/08/05 1-3 05/19105 ~ 08/27/05 ~ I I--" 12/05/05 ~ ~ 03115106 ~ 06/23/06 ~ "1 10101/06 ~ ~ 01109107 "'0 ~ =-04119/07 0 < 07/28/07 ~ "1 11105107 1-3 .... 02113/08 a ~ 05/23/08 --? 08/31108 r::::r -12/09/08 a "'0 03119109 '-' 06/27/09 10105/09 01/13110 04/23/10 08/01110 11109110 02/17111 05/28/11 09/05111 12114111 03/23112 ....... 8 1.0 o Depth Below Measuring Point (ft.) 00 o 0\ o VI 0 .j::.. 0 08/23/02 12/01102 03111103 06119/03 09127/03 01/05/04 04114104 07/23/04 10131104 02/08/05 ~ 05119105 ~ I 08/27/05 N 0'\ 12/05/05 ~ 03115/06 """" ~ 06123/06 "1 ~ 10101106 ~ "C """" 01109/07 =- 04/19/07 0 -< ~ 07128107 "1 11105/07 ~ ... 9 02113/08 ~ -.. 05123/08 ~ 08/31/08 0'" - 12/09/08 9 "C '-' 03119109 06/27/09 10105/09 01113110 04123110 08/01/10 11109110 02117/11 05128111 09/05111 12114111 -03123112 Depth Below Measuring Point (ft.) 00 -..l -..l 0\ 0\ VI VI 0 VI 0 VI 0 VI 0 L-,---_ .. 08/23/02 I 12/01102 03111/03 06/19103 09/27/03 01l0S/04 04114/04 07/23/04 10/31104 02/08/0S ~ OSI1910S ~ 08/27/oS ,&;:.. I ~ 12/0S/OS 0\ ~ 0311S/06 '""" 06/23/06 ~ '"1 10101106 ~ ~ 01109107 "Q '""" =-04/19107 0 < 07/28/07 ~ '"1 11/0S/07 ~ ~. 02113/08 9 ~ 05/23/08 ---? 08/31108 0" -12/09108 9 "Q 03119/09 '-' 06/27/09 1010S/09 01113110 04123110 08/01110 11/09110 02117111 OS/28/11 09105111 12114111 -------_. 03/23/12 Depth Below Measuring Point (ft.) -..) -..) 0\ V\ 08/23/02 12/01/02 03/11/03 06/19/03 09/27/03 01/05/04 04/14/04 07/23/04 10131104 02/08/05 ~ 05/19105 ~ 08/27/05 I ~ 12/05/05 N ~ 03/15/06 ~ 06/23/06 ~ "1 10101/06 ~ ~ 01/09107 "0 ~ =-04/19107 0 -< 07/28/07 ~ "1 11/05/07 ~ .... 02/13/08 = ~ 05/23/08 --? 08/31/08 0--12/09108 = "0 03/19109 '--' 06127/09 10105/09 01/13110 04/23/10 08/01/10 11109/10 02/17/11 OS/28/11 09105/11 12/14/11 03/23/12 Depth Below Measuring Point (ft.) 0 08/23/02 12/01102 03/11/03 06/19103 09/27/03 01105104 04/14/04 07123104 10/31104 02/08/05 1-3 05/19105 ~ 08/27/05 .&;. I ~ 12/05/05 QO ~ 03/15106 ""'" 06/23/06 ('tI --S 10101106 ~ ('tI 01109/07 ~ ""'" =-04/19/07 0 < 07128/07 ('tI --S 11105/07 1-3 .... 02113/08 9 ('tI 05/23/08 ~ ? 08/31108 r:;" -12/09/08 9 ~ 03/19109 '-" 06/27/09 10105/09 01/13/10 04/23110 08/01110 11109110 02/17111 05/28/11 09/05/11 12/14/11 03/23/12 Depth Below Measuring Point (ft.) -J::.. 0 08/23/02 12/01/02 03111103 06119/03 09/27/03 01105104 04114/04 07/23/04 10/31104 02/08/05 1-3 05/19/05 ~ ~ 08/27/05 I ~ 'I.e 12/05/05 ~ 03115106 f""I" ('t 06/23/06 ""1 10101106 ~ ('t "0 01109/07 f""I" =- 04/19/07 0 -< 07/28/07 ('t ""1 11105107 1-3 ... 02113/08 a ('t -.. 05/23/08 ?? 08/31108 0- 12/09/08 !3 "0 '-' 03/19/09 06/27109 10105/09 01113/10 04/23110 08/01110 1110911 0 02117111 OS/28/11 09/05/11 12/14111 03/23112 Depth Below Measuring Point (ft.) ...... 0 1.0 00 -....l 0-U) ~ 0 0 0 0 0 0 0 07/29/05 09/17/05 11106105 12/26/05 02/14/06 04/05/06 05/25/06 07/14106 09/02/06 10/22/06 12/11106 01130107 03121107 ~ 05/10107 ~ 06/29/07 ~ 08/18107 I N 10/07/07 ~ 11126/07 ~ 01115/08 @"+ 03/05/08 ('D "1 04/24/08 0 06/13108 ('D ~ 08/02/08 @"+ =-09/21108 0 11110108 -< ('D 12/30108 "1 02118109 ~ ... 04/09/09 9 05/29/09 ('D ---07118109 ? 09/06/09 0--10/26/09 9 12115109 ~ '-" 02/03/10 03/25110 05114110 07/03/10 08/22/10 10/11/10 11130110 01119/11 03/10/11 04/29111 06118111 08/07111 09/26111 11/15111 01104112 02/23112 Depth Below Measuring Point (ft.) VI tv 07/29/05 09/17/05 11/06105 12/26/05 02/14106 04/05/06 OS/25106 07/14/06 09/02/06 10/22106 12/11/06 01130107 03/21107 05/10107 1-3 06/29/07 ~ 08/18107 ~ I 10107/07 N """"" 11/26/07 ~ 01/15108 ~ 03/05/08 ~ ""'i 04/24/08 ~ 06/13/08 ~ ~ 08/02/08 ~ =-09/21108 0 11/10108 -< 12/30108 ~ ""'i 02/18109 1-3 .... 04/09/09 9 05/29/09 ~ --07/18/09 ? 09/06/09 "a" 10/26109 -9 12/15/09 ~ ---02/03/10 03125/10 05/14/10 07/03/10 08/22/10 10/11/10 11130/10 01/19/11 03/10/11 04/29/11 06/18/11 08/07/11 09/26/11 11115/11 01104/12 02/23/12 Depth Below Measuring Point (ft.) VI 00 VI 00 L r---1\ ~ ~ VI 0\ ~ ~ VI VI VI VI ~ '" [> , ~ 07/29/05 09117105 11106/05 12/26/05 02114/06 04/05/06 OS/25106 07114/06 09/02/06 10/22/06 12111/06 01130107 03/21107 05110107 ~ 06/29/07 ~ 08118107 ~ I 10107/07 N N 11126107 ~ 01115/08 ""'" 03/05/08 ~ ""1 04/24/08 ~ 06/13108 ~ "'C 08/02/08 ""'" =-09/21/08 0 11110108 -< 12130108 ~ ""1 02/18/09 ~ ... 04/09/09 9 05/29/09 ~ -.. 07/18/09 ? 09/06/09 "a" 10/26/09 -9 12/15/09 "'C '-" 02/03110 03125/10 05114110 07/03110 08/22/10 10111110 11130110 01119111 03110111 04/29111 06118/11 I~ 08/07111 09/26/11 11115/11 01/04/12 02/23/12 Depth Below Measuring Point (ft.) 0\ 0\ 0\ 0\ 0\ 0\ 0\ 0\ 0\ \0 \0 00 00 -..) -..) 0\ 0\ VI 09/13/07 11102/07 12/22/07 02/10108 03/31108 OS/20108 07/09/08 08/28108 10/17108 ~ 12106/08 ~ ~ 01125109 I N ~ 03/16/09 ~ 05/05/09 ..... t'tI "1 06/24/09 0 t'tI 08/1 3/09 "C ..... =-10102/09 0 -< 11/21109 t'tI "1 01110/10 ~ .... 9 03/01/10 t'tI -.. 04/20/10 ? 0- 06/09/10 -9 07/29/10 "C "-" 09/17/10 11106/10 12/26/10 02/14/11 04/05/11 05/25/11 07/14111 09/02/11 10/22/11 12/11111 Depth Below Measuring Point (ft.) VI VI 0 09/13/07 11102107 12122/07 02110108 03/31108 05/20108 07/09/08 08/28/08 10117108 1-3 12/06/08 ~ ,&;;;.. 01125109 I N ,&;;;.. 03116/09 ~ 05/05/09 f""I" ~ "1 06/24/09 ~ ~ 08113109 "0 f""I" =-10102/09 0 -< 11121109 ~ "1 01110110 1-3 .... S 03/01110 ~ ,,-., 04120110 ~ r:::J" 06/09110 -S 07129110 "0 '-" 09117110 11106110 12126110 02114111 04/05111 05/25111 07114111 09/02111 10122111 12111111 Depth Below Measuring Point (ft.) VI o ~ • / < I, • • ~ VJ o N o ....... o 0 09/13/07 11102/07 12/22/07 02/10108 03/31108 05/20108 07/09/08 08/28/08 10/17/08 ~ 12/06/08 ~ ~ 01125109 I N VI 03/16/09 ~ 05/05/09 f"'I" t'D ""'i 06/24109 ~ t'D 08113/09 "0 f"'I" =-10102/09 0 -< 11121109 t'D ""'i 01/10110 ~ .... 9 03/01110 t'D --04/20110 ? r::r 06/09110 -9 07/29/10 "0 '-" 09/17110 11/06110 12/26110 02/14111 04/05111 OS/25111 07114111 09/02111 10122/11 12111111 ----Q.; = -.c ~ '-' ~ = .... ~ ;.. ~ ;;. 0 .d ... Q.; ~ ~ ;.. ~ ... ~ \0 N I ~ ~ ~ 111£ZIZ1 111171160 11190/90 1119Z1ZO 01181111 01101180 01lZO/~0 o o ."t \0 ~ ~ ~ ~ ~ r-. ~ ~ 0 0 0 0 0 ~ ~ ~ \0 ~ ."t ."t ."t ."t ."t \0 \0 \0 \0 \0 ClJ) lU!Od iJupnSB;:WoJ: MOPS: qldga o 00 ~ TabG Depths to Groundwater and Elevations Over Time for Chloroform Monitoring Wells Water Levels and Data over Time White Mesa Mill-Well MW4 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,620.77 5,622.33 1.56 123.6 5,527.63 09/25/79 94.70 93.14 5,527.63 10/10/79 94.70 93.14 5,528.43 01/10/80 93.90 92.34 5,529.93 03/20/80 92.40 90.84 5,528.03 06/17/80 94.30 92.74 5,528.03 09/15/80 94.30 92.74 5,527.93 10/08/80 94.40 92.84 5,527.93 02/12/81 94.40 92.84 5,525.93 09/01184 96.40 94.84 5,528.33 12/01/84 94.00 92.44 5,528.13 02/01/85 94.20 92.64 5,528.33 06/01/85 94.00 92.44 5,528.93 09/01/85 93.40 91.84 5,528.93 10/01/85 93.40 91.84 5,528.93 11101/85 93.40 91.84 5,528.83 12/01/85 93.50 91.94 5,512.33 03/01/86 110.00 108.44 5,528.91 06/19/86 93.42 91.86 5,528.83 09/01186 93.50 91.94 5,529.16 12/01/86 93.17 91.61 5,526.66 02/20/87 95.67 94.11 5,529.16 04/28/87 93.17 91.61 5,529.08 08/14/87 93.25 91.69 5,529.00 11/20/87 93.33 91.77 5,528.75 01126/88 93.58 92.02 5,528.91 06/01/88 93.42 91.86 5,528.25 08/23/88 94.08 92.52 5,529.00 11/02/88 93.33 91.77 5,528.33 03/09/89 94.00 92.44 5,529.10 06/21/89 93.23 91.67 5,529.06 09/01/89 93.27 91.71 5,529.21 11/15/89 93.12 91.56 5,529.22 02/16/90 93.11 91.55 5,529.43 05/08/90 92.90 91.34 5,529.40 08/07/90 92.93 91.37 5,529.53 11/13/90 92.80 91.24 5,529.86 02/27/91 92.47 90.91 5,529.91 OS/21/91 92.42 90.86 5,529.77 08/27/91 92.56 91.00 5,529.79 12/03/91 92.54 90.98 5,530.13 03/17/92 92.20 90.64 5,529.85 06/11/92 92.48 90.92 5,529.90 09/13/92 92.43 90.87 Water Levels and Data over Time White Mesa Mill -Well MW 4 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,620.77 5,622.33 1.56 123.6 5,529.92 12/09/92 92.41 90.85 5,530.25 03/24/93 92.08 90.52 5,530.20 06/08/93 92.13 90.57 5,530.19 09/22/93 92.14 90.58 5,529.75 12/14/93 92.58 91.02 5,530.98 03/24/94 91.35 89.79 5,531.35 06/15/94 90.98 89.42 5,531.62 08/18/94 90.71 89.15 5,532.58 12/13/94 89.75 88.19 5,533.42 03/16/95 88.91 87.35 5,534.70 06127/95 87.63 86.07 5,535.44 09/20/95 86.89 85.33 5,537.16 12/11/95 85.17 83.61 5,538.37 03/28/96 83.96 82.40 5,539.10 06/07/96 83.23 81.67 5,539.13 09/16/96 83.20 81.64 5,542.29 03120/97 80.04 78.48 5,551.58 04/07/99 70.75 69.19 5,552.08 05/11/99 70.25 68.69 5,552.83 07/06/99 69.50 67.94 5,553.47 09/28/99 68.86 67.30 5,554.63 01/03/00 67.70 66.14 5,555.13 04/04/00 67.20 65.64 5,555.73 05/02/00 66.60 65.04 5,556.03 05111100 66.30 64.74 5,555.73 05/15/00 66.60 65.04 5,555.98 05125/00 66.35 64.79 5,556.05 06/09/00 66.28 64.72 5,556.18 06/16/00 66.15 64.59 5,556.05 06/26/00 66.28 64.72 5,556.15 07/06/00 66.18 64.62 5,556.18 07/13/00 66.15 64.59 5,556.17 07118/00 66.16 64.60 5,556.26 07/25/00 66.07 64.51 5,556.35 08/02/00 65.98 64.42 5,556.38 08/09/00 65.95 64.39 5,556.39 08115/00 65 .94 64.38 5,556.57 08/31/00 65.76 64.20 5,556.68 09/08/00 65.65 64.09 5,556.73 09113/00 65.60 64.04 5,556.82 09120/00 65.51 63.95 5,556.84 09129100 65.49 63.93 5,556.81 10/05/00 65.52 63.96 Water Levels and Data over Time White Mesa Mill -Well MW 4 Total or Measuriug Measured Total Water Land Poiut Depth to Depth to Total Elevation Surface Elevation Leugth Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,620.77 5,622.33 1.56 123.6 5,556.89 10/12/00 65.44 63.88 5,556.98 10/19/00 65.35 63.79 5,557.01 10/23/00 65.32 63.76 5,557.14 11/09/00 65.19 63.63 5,557.17 11114/00 65.16 63.60 5,556.95 11121/00 65.38 63.82 5,557.08 11130100 65.25 63.69 5,557.55 12/07/00 64.78 63.22 5,557.66 01114/01 64.67 63.11 5,557.78 02/09/01 64.55 62.99 5,558.28 03/29/01 64.05 62.49 5,558.23 04/30101 64.10 62.54 5,558.31 05/31101 64.02 62.46 5,558.49 06/22/01 63.84 62.28 5,558.66 07110101 63.67 62.11 5,559.01 08/20101 63.32 61.76 5,559.24 09/19/01 63.09 61.53 5,559.26 10/02/01 63.07 61.51 5,559.27 11108/01 63.06 61.50 5,559.77 12/03/01 62.56 61.00 5,559.78 01103/02 62.55 60.99 5,559.96 02/06/02 62.37 60.81 5,560.16 03/26/02 62.17 60.61 5,560.28 04/09/02 62.05 60.49 5,560.76 OS/23/02 61.57 60.01 5,560.58 06/05/02 61.75 60.19 5,560.43 07/08/02 61.90 60.34 5,560.44 08/23/02 61.89 60.33 5,560.71 09/11102 61.62 60.06 5,560.89 10/23/02 61.44 59.88 5,557.86 11/22/02 64.47 62.91 5,561.10 12/03/02 61.23 59.67 5,561.39 01/09/03 60.94 59.38 5,561.41 02112/03 60.92 59.36 5,561.93 03/26/03 60.40 58.84 5,561.85 04/02/03 60.48 58.92 5,536.62 05/01103 85.71 84.15 5,528.56 06/09/03 93.77 92.21 5,535.28 07/07/03 87.05 85.49 5,534.44 08/04/03 87.89 86.33 5,537.10 09/11/03 85.23 83.67 5,539.96 10102/03 82.37 80.81 5,535.91 11107/03 86.42 84.86 Water Levels and Data over Time White Mesa Mill -Well MW 4 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,620.77 5,622.33 1.56 123.6 5,550.70 12/03/03 71.63 70.07 5,557.58 01115/04 64.75 63.19 5,558.80 02110104 63.53 . 61.97 5,560.08 03128/04 62.25 60.69 5,560.55 04112/04 61.78 60.22 5,561.06 05/13/04 61.27 59.71 5,561.48 06118/04 60.85 59.29 5,561.86 07/28/04 60.47 58.91 5,529.17 08 /30104 93.16 91.60 5,536.55 09116/04 85 .78 84.22 5,529.00 10111104 93.33 91.77 5,541.55 11/16/04 80.78 79.22 5,541.12 12122/04 81.21 79.65 5,540.59 01118/05 81.74 80.18 5,542.85 02/28/05 79.48 77.92 5,537.91 03115/05 84.42 82.86 5,548.67 04/26/05 73.66 72.10 5,549.53 05124/05 72.80 71.24 5,544.36 06/30105 77.97 76.41 5,545.16 07129/05 77.17 75.61 5,544.67 09/12/05 77.66 76.10 5,541.28 09/27/05 81.05 79.49 5,536.96 12/07/05 85.37 83.81 5,546.49 03/08/06 75.84 74.28 5,546.15 06113/06 76.18 74.62 5,545.15 07/18/06 77.18 75.62 5,545.91 11117/06 76.42 74.86 5,545.90 02127/07 76.43 · 74.87 5,548.16 05/02/07 74.17 72.61 5,547.20 08/13/07 75.13 73.57 5,547.20 10110107 75.13 73.57 5,547.79 03/26/08 74.54 72.98 5,545.09 06125/08 77.24 75.68 5,550.36 08126/08 71.97 70.41 5,550.39 10/14/08 71.94 70.38 5,542.25 03/03 /09 80.08 78.52 5,542.25 06/24/09 80.08 78.52 5,550.19 09110109 72.14 70.58 5,550.94 12/11109 71.39 69.83 5,546.08 03/11110 76.25 74.69 5,550.98 05111110 71.35 69.79 5,548.33 09129/10 74.00 72.44 5,551.01 12/21110 71.32 69 .76 Water Levels and Data over Time White Mesa Mill -Well MW 4 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,620.77 5,622.33 1.56 123.6 5,547.00 02128/11 75.33 73.77 5,557.54 06/21111 64.79 63.23 5,551.14 09/20/11 71.19 69.63 Water Levels and Data over Time White Mesa Mill -Well TW 4-1 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well z 5,620.77 5,618.58 1.02 111.04 5,537.23 11108/99 81.35 80.33 5,537.38 11109/99 81.20 80.18 5,537.48 01102/00 81.10 80.08 5,537.48 01110/00 81.10 80.08 5,537.23 01117/00 81.35 80.33 5,537.28 01124/00 81.30 80.28 5,537.28 02/01100 81.30 80.28 5,537.18 02/07/00 81.40 80.38 5,537.48 02/14/00 81.10 80.08 5,537.48 02123/00 81.10 80.08 5,537.58 03/01/00 81.00 79.98 5,537.68 03/08/00 80.90 79.88 5,537.98 03/15/00 80.60 79.58 5,537.68 03120/00 80.90 79.88 5,537.68 03129/00 80.90 79.88 5,537.43 04/04/00 81.15 80.13 5,537.18 04/13/00 81.40 80.38 5,537.48 04121/00 81.10 80.08 5,537.68 04128/00 80.90 79.88 5,537.58 05/01100 81.00 79.98 5,537.88 05/11100 80.70 79.68 5,537.58 05/15/00 81.00 79.98 5,537.88 OS/25/00 80.70 79.68 5,537.88 06/09/00 80.70 79.68 5,537.90 06/16/00 80.68 79.66 5,537.88 06126/00 80.70 79.68 5,538.10 07/06/00 80.48 79.46 5,538.04 07/13/00 80.54 79.52 5,538.16 07/18/00 80.42 79.40 5,538.42 07127/00 80.16 79.14 5,538.56 08/02/00 80.02 79.00 5,538.68 08/09/00 79.90 78.88 5,538.66 08/15/00 79.92 78.90 5,538.33 08/31100 80.25 79.23 5,539.18 09/01100 79.40 78.38 5,539.12 09/08/00 79.46 78.44 5,539.34 09/13/00 79.24 78.22 5,539.50 09/20/00 79.08 78.06 5,539.69 10/05/00 78.89 77.87 5,540.33 11109/00 78.25 77.23 5,540.74 12/06/00 77.84 76.82 5,542.39 01/14/01 76.19 75.17 5,543.69 02/02/01 74.89 73.87 Water Levels and Data over Time White Mesa Mill -Well TW 4-1 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well z 5,620.77 5,618.58 1.02 111.04 5,544.96 03/29/01 73.62 72.60 5,545.45 04/30/01 73.13 72.1 1 5,545.89 05/31101 72.69 71.67 5,546.19 06121101 72.39 71.37 5,546.50 07/10/01 72.08 71.06 5,547.18 08/20/01 71.40 70.38 5,547.59 09/19/01 70.99 69.97 5,547.84 10/02/01 70.74 69.72 5,548.12 11108/01 70.46 69.44 5,548.65 12/03/01 69.93 68.91 5,548.87 01103/02 69.71 68.69 5,549.37 02/06/02 69.21 68.19 5,550.00 03126/02 68.58 67 .56 5,550.22 04/09/02 68.36 67.34 5,550.81 OS/23/02 67.77 66.75 5,550.79 06/05/02 67.79 66.77 5,551.08 07/08/02 67.50 66.48 5,551.54 08/23/02 67.04 66.02 5,551.79 09/11102 66.79 65.77 5,552.19 10/23/02 66.39 65.37 5,552.27 11122/02 66.3 1 65.29 5,552.48 12/03/02 66.10 65.08 5,552.74 01/09/03 65 .84 64.82 5,552.92 02/12/03 65.66 64.64 5,553.40 03126/03 65.18 64.16 5,553.48 04/02/03 65.10 64.08 5,552.32 05/01103 66.26 65.24 5,550.53 06/09/03 68.05 67.03 5,550.09 07/07/03 68.49 67.47 5,549.64 08/04/03 68.94 67.92 5,549.31 09/11103 69.27 68.25 5,549.58 10/02/03 69.00 67.98 5,549.50 11107/03 69.08 68.06 5,550.07 12/03/03 68.51 67.49 5,551.86 01/15/04 66.72 65.70 5,552.57 02/10/04 66.01 64.99 5,553.63 03/28/04 64.95 63.93 5,554.04 04/12/04 64.54 63.52 5,554.60 05/13/04 63.98 62.96 5,556.28 06/18/04 62.30 61.28 5,556.61 07128/04 61.97 60.95 5,554.21 08/30/04 64.37 63.35 5,553.49 09/16/04 65.09 64.07 Water Levels and Data over Time White Mesa Mill -Well TW 4-1 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well z 5,620.77 5,618.58 1.02 111.04 5,552.53 10111104 66.05 65.03 5,552.42 11116/04 66.16 65.14 5,552.46 12/22/04 66.12 65.10 5,552.07 01118/05 66.51 65.49 5,552.21 02128/05 66.37 65.35 5,552.26 03/15/05 66.32 65.30 5,552.30 04/26/05 66.28 65.26 5,552.25 05/24/05 66.33 65.31 5,552.22 06/30105 66.36 65.34 5,552.15 07129/05 66.43 65.41 5,552.47 09112/05 66.11 65 .09 5,552.50 12/07/05 66.08 65 .06 5,552.96 03/08/06 65.62 64.60 5,553.23 06/14/06 65.35 64.33 5,557.20 07118/06 61.38 60.36 5,553.32 11/07/06 65.26 64.24 5,554.35 02/27/07 64.23 63.21 5,554.07 05/02/07 64.51 63.49 5,554.07 08/14/07 64.51 63.49 5,553.88 10/10/07 64.70 63.68 5,555.73 03/26/08 62.85 61.83 5,556.60 06/24/08 61.98 60.96 5,556.83 08126/08 61.75 60.73 5,556.87 10/14/08 61.71 60.69 5,556.90 03/10/09 61.68 60.66 5,556.91 06/24/09 61.67 60.65 5,556.61 09110109 61.97 60.95 5,556.78 12/11109 61.8 60.78 5,556.75 03/11110 61 .83 60.81 5,556.19 05/11110 62.39 61.37 5,555.26 09/29110 63.32 62.30 5,554.66 12121110 63.92 62.90 5,554.74 02128111 63.84 62.82 5,554.57 06/21111 64.01 62.99 5,554.l3 09120111 64.45 63.43 Water Levels and Data over Time White Mesa Mill -Well TW 4-2 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,623.10 5,624.72 1.62 121.125 5,548.57 11108/99 76.15 74.53 5,548.57 11109/99 76.15 74.53 5,548.32 01102/00 76.40 74.78 5,548.52 01110/00 76.20 74.58 5,548.32 01117/00 76.40 74.78 5,548.72 01124/00 76.00 74.38 5,548.62 02/01100 76.10 74.48 5,548.62 02/07/00 76.10 74.48 5,549.02 02/14/00 75.70 74.08 5,549.12 02/23/00 75.60 73.98 5,549.22 03/01/00 75.50 73.88 5,549.32 03/08/00 75.40 73.78 5,549.22 03/15/00 75.50 73.88 5,549.92 03/20/00 74.80 73.18 5,549.72 03/29/00 75.00 73.38 5,549.42 04/04/00 75.30 73.68 5,549.52 04/13/00 75.20 73.58 5,549.72 04/21100 75.00 73.38 5,549.82 04/28/00 74.90 73.28 5,549.82 05/01100 74.90 73.28 5,550.12 05111100 74.60 72.98 5,549.82 05/15/00 74.90 73.28 5,550.12 OS/25/00 74.60 72.98 5,550.12 06/09/00 74.60 72.98 5,550.22 06/16/00 74.50 72.88 5,550.07 06/26/00 74.65 73.03 5,550.17 07/06/00 74.55 72.93 5,550.17 07/13/00 74.55 72.93 5,550.18 07/18/00 74.54 72.92 5,550.33 07/27/00 74.39 72.77 5,550.38 08/02/00 74.34 72.72 5,550.40 08/09/00 74.32 72.70 5,550.42 08/15/00 74.30 72.68 5,550.54 08/31/00 74.18 72.56 5,550.87 09/08/00 73.85 72.23 5,550.97 09/13/00 73.75 72.13 5,551.04 09/20/00 73.68 72.06 5,545.83 10/05/00 78.89 77.27 5,546.47 11109/00 78.25 76.63 5,546.88 12/06/00 77.84 76.22 5,552.18 01126/01 72.54 70.92 5,552.20 02/02/01 72.52 70.90 5,551.10 03/29/01 73.62 72.00 Water Levels and Data over Time White Mesa Mill-Well TW4-2 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,623 .10 5,624.72 1.62 121.125 5,551.59 04/30101 73.13 71.51 5,552.03 05/31/01 72.69 71.07 5,552.33 06/21/01 72.39 70.77 5,552.64 07110101 72.08 70.46 5,553.32 08/20101 71.40 69.78 5,553.73 09/19/01 70.99 69.37 5,553.98 10/02/01 70.74 69.12 5,554.14 11/08/01 70.58 68.96 5,554.79 12/03/01 69.93 68.31 5,554.74 01/03/02 69.98 68.36 5,554.91 02/06/02 69.81 68 .19 5,555.15 03/26/02 69.57 67.95 5,555.39 04/09/02 69.33 67 .71 5,555.73 OS/23/02 68.99 67 .37 5,555.79 06/05102 68.93 67.31 5,555.91 07/08/02 68.81 67.19 5,556.04 08/23/02 68.68 67.06 5,556.25 09/11102 68.47 66.85 5,556.72 10/23/02 68.00 66.38 5,556.42 11/22/02 68.30 66.68 5,557.01 12/03/02 67.71 66.09 5,557.20 01/09/03 67.52 65.90 5,557.35 02/12/03 67.37 65.75 5,557.83 03/26/03 66.89 65.27 5,557.87 04/02/03 66.85 65.23 5,553.71 05/01103 71.01 69.39 5,548.98 06/09/03 75.74 74.12 5,548.14 07/07/03 76.58 74.96 5,547.75 08/04/03 76.97 75.35 5,547.22 09/11103 77.50 75.88 5,547.68 10102/03 77.04 75.42 5,547.52 11107/03 77.20 75.58 5,548.29 12/03/03 76.43 74.81 5,554.00 01115104 70.72 69.10 5,555.46 02110104 69.26 67.64 5,556.90 03/28/04 67.82 66.20 5,557.49 04112/04 67.23 65.61 5,558.07 05/13/04 66.65 65.03 5,558.19 06/18/04 66.53 64.91 5,559.00 07/28/04 65.72 64.10 5,554.26 08/30104 70.46 68.84 5,551.97 09/16/04 72.75 71.13 5,549.65 10/11/04 75.07 73.45 Water Levels and Data over Time White Mesa Mill-Well TW4-2 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,623.10 5,624.72 1.62 121.125 5,549.89 11116/04 74.83 73.21 5,550.37 12/22/04 74.35 72.73 5,549.95 01118/05 74.77 · 73.15 5,550.09 02/28/05 74.63 73.01 5,550.13 03115/05 74.59 72.97 5,550.18 04/26/05 74.54 72.92 5,550.32 OS/24/05 74.40 72.78 5,550.21 06/30/05 74.51 72.89 5,550.11 07/29/05 74.61 72.99 5,550.33 09112/05 74.39 72.77 5,550.29 12/07/05 74.43 72.81 5,551.30 03/08/06 73.42 71.80 5,551.42 06/14/06 73.3 71.68 5,550.52 07118/06 74.20 72.58 5550.52 11107/06 74.20 72.58 5552.89 02/27/07 71.83 70.21 5,552.06 05/02/07 72.66 71.04 5,552.02 08114/07 72.7 71.08 5,552.20 10110/07 72.52 70.90 5,554.58 03/26/08 70.14 68.52 5,555.23 06/24/08 69.49 67.87 5,555.29 08/26/08 69.43 67.81 5,555.43 10/14/08 69.29 67.67 5,555.73 03/10/09 68.99 67.37 5,556.25 06/24/09 68.47 66.85 5,555.94 09/10/09 68.78 67.l6 5,556.53 12/11109 68.19 66.57 5,557.87 03/11110 66.85 65 .23 5,557.63 05/11110 67.09 65.47 5,557.24 09/29110 67.48 65.86 5,557.00 12/21110 67.72 66.l0 5,557.61 02/28111 67.11 65.49 5,557.58 06/21111 67.14 65.52 5,557.46 09/20111 67.26 65.64 Water Levels and Data over Time White Mesa Mill -Well TW 4-3 Total or Measuring Measured Total Water Land Point Depth to Depth to Elevation Surface Elevation Length Of Date Of Water Water (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Total Depth Of Well 5,63l.21 5,632.23 l.02 141 5,565.78 11/29/99 66.45 65.43 5,566.93 01/02/00 65.30 64.28 5,567.03 01/10/00 65.20 64.18 5,566.83 01117/00 65.40 64.38 5,567.13 01124/00 65.10 64.08 5,567.33 02/01/00 64.90 63.88 5,567.13 02/07/00 65.10 64.08 5,567.43 02114/00 64.80 63.78 5,567.63 02/23/00 64.60 63.58 5,567.73 03/01/00 64.50 63.48 5,567.83 03/08/00 64.40 63.38 5,567.70 03/15/00 64.53 63.51 5,568.03 03/20/00 64.20 63.18 5,567.93 03/29/00 64.30 63.28 5,567.63 04/04/00 64.60 63.58 5,567.83 04/13/00 64.40 63.38 5,568.03 04/21/00 64.20 63.18 5,568.23 04/28/00 64.00 62.98 5,568.13 05/01/00 64.10 63.08 5,568.53 05/11/00 63.70 62.68 5,568.23 05/15/00 64.00 62.98 5,568.53 OS/25/00 63.70 62.68 5,568.61 06/09/00 63.62 62.60 5,568.69 06116/00 63.54 62.52 5,568.45 06/26/00 63.78 62.76 5,568.61 07/06/00 63.62 62.60 5,568.61 07/06/00 63 .62 62.60 5,568.49 07/13/00 63 .74 62.72 5,568.55 07118/00 63.68 62.66 5,568.65 07/27/00 63.58 62.56 5,568.73 08/02/00 63.50 62.48 5,568.77 08/09/00 63.46 62.44 5,568.76 08116/00 63.47 62.45 5,568.95 08/31/00 63.28 62.26 5,568.49 09/08/00 63.74 62.72 5,568.67 09/13/00 63.56 62.54 5,568.96 09/20/00 63.27 62.25 5,568.93 10/05/00 63.3 62.28 5,569.34 11/09/00 62.89 6l.87 5,568.79 12/06/00 63.44 62.42 5,569.11 01/03/01 63.12 62.10 5,569.75 02/09/01 62.48 61.46 5,570.34 03/28/01 6l.89 60.87 Water Levels and Data over Time White Mesa Mill -Well TW 4-3 Total or Measuring Measured Total Water Land Point Depth to Depth to Elevation Surface Elevation Length Of Date Of Water Water (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Total Depth Of Well 5,631.21 5,632.23 1.02 141 5,570.61 04/30/01 61.62 60.60 5,570.70 05/31101 61 .53 60.51 5,570.88 06/21101 61.35 60.33 5,571.02 07/10/01 61.21 60.19 5,571.70 08/20/01 60.53 59.51 5,572.12 09/19/01 60.11 59.09 5,572.08 10/02/01 60.15 59.13 5,572.78 11108/01 59.45 58.43 5,573 .27 12/03/01 58.96 57.94 5,573.47 01/03/02 58.76 57.74 5,573.93 02/06/02 58.30 57.28 5,574.75 03/26/02 57.48 56.46 5,574.26 04/09/02 57.97 56.95 5,575.39 OS/23/02 56.84 55.82 5,574.84 06/05/02 57.39 56.37 5,575.33 07/08/02 56.90 55.88 5,575.79 08/23/02 56.44 55.42 5,576.08 09/11102 56.15 55.13 5,576.30 10/23/02 55.93 54.91 5,576.35 11122/02 55.88 54.86 5,576.54 12/03/02 55.69 54.67 5,576.96 01/09/03 55.27 54.25 5,577.11 02/12/03 55.12 54.10 5,577.61 03/26/03 54.62 53.60 5,572.80 04/02/03 59.43 58.41 5,577.89 05/01103 54.34 53.32 5,577.91 06/09/03 54.32 53.30 5,577.53 07/07/03 54.70 53.68 5,577.50 08/04/03 54.73 53.71 5,577.71 09/11103 54.52 53 .50 5,577.31 10/02/03 54.92 53 .90 5,577.33 11107/03 54.90 53 .88 5,577.34 12/03/03 54.89 53 .87 5,578.24 01115/04 53.99 52.97 5,578.38 02/10/04 53.85 52.83 5,578.69 03/28/04 53 .54 52.52 5,579.15 04/12/04 53.08 52.06 5,579.47 05/13/04 52.76 51.74 5,579.53 06/18/04 52.70 51.68 5,580.17 07/28/04 52.06 51.04 5,580.20 08/30/04 52.03 51.01 5,580.26 09/16/04 51.97 50.95 5,580.12 10/11104 52.11 51.09 Water Levels and Data over Time White Mesa Mill -Well TW 4-3 Total or Measuring Measured Total Water Land Point Depth to Depth to Elevation Surface Elevation Length Of Date Of Water Water (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Total Depth Of Well 5,631.21 5,632.23 1.02 141 5,579.93 11/16/04 52.30 51.28 5,580.07 12122/04 52.16 51.14 5,579.80 01/18/05 52.43 51.41 5,580.35 02128/05 51.88 50.86 5,580.57 03/15/05 51.66 50.64 5,580.86 04126/05 51.37 50.35 5,581.20 05124/05 51.03 50.01 5,581.51 06/30/05 50.72 49.70 5,581.55 07/29/05 50.68 49.66 5,581.68 09/12/05 50.55 49.53 5,581.83 12/07/05 50.4 49.38 5,564.92 03/08/06 67.31 66.29 5,582.73 06/13/06 49.50 48.48 5,582.33 07/18/06 49.90 48 .88 5,582.75 11/07/06 49.48 48.46 5583.35 02/27/07 48.88 47.86 5,559.57 05/02/07 72.66 71.64 5,583.29 08/14/07 48.94 47.92 5,583.49 10/10/07 48.74 47.72 5,584.95 03/26/08 47.28 46.26 5,584.59 06/24/08 47.64 46.62 5,584.55 08126/08 47.68 46.66 5,584.03 10/14/08 48 .2 47.18 5,583.64 03/03/09 48.59 47.57 5,587.34 06124/09 44.89 43.87 5,582.90 09/10/09 49.33 48.31 5,583.27 12/11/09 48 .96 47.94 5,583.63 03/11/10 48.6 47.58 5,583.82 05/11/10 48.41 47.39 5,583.51 09/29/10 48.72 47.70 5,582.86 12121/10 49.37 48.35 5,582.60 02128/11 49.63 48.61 5,590.00 06121/11 42.23 41.21 5,582.70 09/20/11 49.53 48.51 Water Levels and Data over Time White Mesa Mill -Well TW 4-4 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,612.301 5,613.485 1.184 114.5 5,512.145 05125/00 101.34 100.16 5,518.985 06/09/00 94.50 93.32 5,512.145 06/16/00 101.34 100.16 5,517.465 06126/00 96.02 94.84 5,520.145 07/06/00 93.34 92.16 5,521.435 07/13/00 92.05 90.87 5,522.005 07/18/00 91.48 90.30 5,522.945 07/27/00 90.54 89.36 5,523.485 08/02/00 90.00 88.82 5,523.845 08/09/00 89.64 88.46 5,523.885 08/15/00 89.60 88.42 5,524.555 09/01100 88.93 87.75 5,513.235 09/08/00 100.25 99.07 5,516.665 09/13/00 96.82 95.64 5,519.085 09120/00 94.40 93.22 5,522.165 10/05/00 91.32 90.14 5,524.665 11109/00 88.82 87.64 5,518.545 12/06/00 94.94 93.76 5,527.695 01103/01 85.79 84.61 5,529.085 02/09/01 84.40 83.22 5,529.535 03/27/01 83.95 82.77 5,530.235 04/30/01 83.25 82.07 5,530.265 05/31101 83.22 82.04 5,534.405 06122/01 79.08 77.90 5,533.145 07/10/01 80.34 79.16 5,534.035 08120/01 79.45 78.27 5,534.465 09/19/01 79.02 77.84 5,533.285 10/02/01 80.20 79.02 5,533.865 11108/01 79.62 78.44 5,534.275 12/03/01 79.21 78.03 5,534.715 01103/02 78.77 77.59 5,535.435 02/06/02 78.05 76.87 5,536.445 03/26/02 77.04 75.86 5,536.405 04/09/02 77.08 75.90 5,537.335 OS/23/02 76.15 74.97 5,537.325 06/05/02 76.16 74.98 5,537.975 07/08/02 75.51 74.33 5,538.825 08123/02 74.66 73.48 5,539.275 09/11102 74.21 73.03 5,539.765 10/23/02 73.72 72.54 5,540.205 11122/02 73.28 72.10 5,540.295 12/03/02 73.19 72.01 5,540.795 01109/03 72.69 71.51 Water Levels and Data over Time White Mesa Mill -Well TW 4-4 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,612.301 5,613.485 1.184 114.5 5,540.985 02112/03 72.50 71.32 5,541.675 03126/03 71.81 70.63 5,541.765 04/02/03 71.72 70.54 5,541.885 05/01103 71.60 70.42 5,542.025 06/09/03 71.46 70.28 5,541.925 07/07/03 71.56 70.38 5,541.885 08/04/03 71.60 70.42 5,541.825 09/11103 71.66 70.48 5,541.885 10/02/03 71.60 70.42 5,541.995 11107/03 71.49 70.31 5,542.005 12/03/03 71.48 70.30 5,542.555 01115/04 70.93 69.75 5,542.705 02/10/04 70.78 69.60 5,543.225 03128/04 70.26 69.08 5,543.555 04/12/04 69.93 68.75 5,543.865 05/13/04 69.62 68.44 5,543.915 06/18/04 69.57 68.39 5,544.655 07128/04 68.83 67.65 5,544.795 08/30/04 68.69 67.51 5,544.845 09/16/04 68.64 67.46 5,544.705 10/11104 68.78 67.60 5,544.525 11116/04 68.96 67.78 5,544.625 12122/04 68.86 67.68 5,544.305 01118/05 69.18 68.00 5,544.585 02128/05 68.90 67.72 5,544.685 03/15/05 68.80 67.62 5,544.675 04126/05 68.81 67.63 5,544.785 05124/05 68.70 67.52 5,544.795 06/30/05 68.69 67.51 5,544.775 07129/05 68.71 67.53 5,545.005 09112/05 68.48 67.30 5,545.225 12/07/05 68.26 67.08 5,545.735 03/08/06 67.75 66.57 5,545.785 06114/06 67 .70 66.52 5,545.855 07118/06 67.63 66.45 5,545.805 11107/06 67.68 66.50 5546.675 02127/07 66.81 65.63 5,546.535 05/02/07 66.95 65.77 5,547.155 08/15/07 66.33 65.15 5,547.215 10/10/07 66.27 65.09 5,548.305 03126/08 65.18 64.00 5,548.865 06124/08 64.62 63.44 5,549.235 08126/08 64.25 63.07 Water Levels and Data over Time White Mesa Mill -Well TW 4-4 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,612.301 5,613.485 1.184 114.5 5,549.305 10/14/08 64.18 63.00 5,549.725 03/03/09 63.76 62.58 5,549.905 06/24/09 63.58 62.40 5,549.695 09110/09 63.79 62.61 5,549.865 12/11109 63.62 62.44 5,545.60 03/11110 67.89 66.71 5,530.88 05/11110 82.61 81.43 5,545.24 09/29110 68.25 67.07 5,533.66 12/21110 79.83 78.65 5,544.44 02/28/11 69.05 67.87 5,543.73 06/21/11 69.76 68.58 5,540.48 09/20/11 73.01 71.83 Water Levels and Data over Time White Mesa Mill -Well TW 4-5 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Snrface Elevation Length Of Date Of Water Water Depth Of (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,638.75 5,640.70 1.95 121.75 5,579.30 01/02/00 61.40 59.45 5,579.60 01/10/00 61.10 59.15 5,579.35 01/17/00 61.35 59.40 5,579.60 01/24/00 61.10 59.15 5,579.50 02/01/00 61.20 59.25 5,579.50 02/07/00 61.20 59.25 5,579.90 02/14/00 60.80 58.85 5,579.90 02/23/00 60.80 58.85 5,580.20 03/01/00 60.50 58.55 5,580.00 03/08/00 60.70 58.75 5,580.04 03/15/00 60.66 58.71 5,580.70 03/20/00 60.00 58.05 5,580.30 03/29/00 60.40 58.45 5,580.00 04/04/00 60.70 58.75 5,580.20 04/13/00 60.50 58.55 5,580.40 04/21/00 60.30 58.35 5,580.50 04/28/00 60.20 58.25 5,580.50 05/01/00 60.20 58.25 5,580.90 05/11/00 59.80 57.85 5,580.50 05/15/00 60.20 58.25 5,580.75 OS/25/00 59.95 58.00 5,580.80 06/09/00 59.90 57.95 5,580.92 06/16/00 59.78 57.83 5,580.80 06/26/00 59.90 57.95 5,580.90 07/06/00 59.80 57.85 5,581.05 07/13/00 59.65 57.70 5,580.90 07/18/00 59.80 57.85 5,581.05 07/27/00 59.65 57.70 5,581.06 08/02/00 59.64 57.69 5,581.08 08/09/00 59.62 57.67 5,581.07 08/16/00 59.63 57.68 5,581.25 08/31/00 59.45 57.50 5,581.32 09/08/00 59.38 57.43 5,581.34 09/13/00 59.36 57.41 5,581.41 09/20/00 59.29 57.34 5,581.37 10/05/00 59.33 57.38 5,581.66 11/09/00 59.04 57.09 5,581.63 12/06/00 59.07 57.12 5,581.92 01/03/01 58.78 56.83 5,582.20 02/09/01 58.50 56.55 5,582.54 03/28/01 58.16 56.21 5,582.72 04/30/01 57.98 56.03 5,582.72 05/31/01 57.98 56.03 Water Levels and Data over Time White Mesa Mill -Well TW 4-5 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,638.75 5,640.70 1.95 121.75 5,582.81 06/22/01 57.89 55.94 5,582.92 07/10101 57.78 55.83 5,583.17 08/20101 57.53 55.58 5,583.28 09/19101 57.42 55.47 5,583.36 10/02/01 57.34 55.39 5,583.49 11108/01 57.21 55.26 5,583.84 12/03/01 56.86 54.91 5,583.79 01103/02 56.91 54.96 5,583.96 02/06/02 56.74 54.79 5,584.39 03/26/02 56.31 54.36 5,584.12 04/09102 56.58 54.63 5,584.55 OS/23/02 56.15 54.20 5,584.42 06/05/02 56.28 54.33 5,583.65 07/08/02 57.05 55.l0 5,584.90 08/23/02 55.80 53.85 5,585.02 09/11102 55.68 53.73 5,585.20 10/23/02 55.50 53.55 5,585.15 11122/02 55.55 53.60 5,585.42 12/03/02 55.28 53.33 5,585.65 01109/03 55.05 53.10 5,585.65 02/12/03 55.05 53.l0 5,585.92 03/26/03 54.78 52.83 5,586.22 04/02/03 54.48 52.53 5,586.01 05/01103 54.69 52.74 5,584.81 06/09103 55.89 53.94 5,584.34 07/07/03 56.36 54.41 5,584.40 08/04/03 56.30 54.35 5,583.88 09/11/03 56.82 54.87 5,583.57 10102/03 57.13 55.18 5,583.39 11/07/03 57.31 55.36 5,583.97 12/03/03 56.73 54.78 5,585.28 01/15/04 55.42 53.47 5,585.50 02/10/04 55.20 53.25 5,585.87 03/28/04 54.83 52.88 5,586.20 04/12/04 54.50 52.55 5,586.45 05/13/04 54.25 52.30 5,586.50 06/18/04 54.20 52.25 5,587.l3 07/28/04 53.57 51.62 5,586.22 08/30104 54.48 52.53 5,585.69 09/16/04 55.01 53.06 5,585.17 10/11/04 55.53 53.58 5,584.64 11116/04 56.06 54.11 5,584.77 12/22/04 55.93 53.98 Water Levels and Data over Time White Mesa Mill -Well TW 4-5 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,638.75 5,640.70 1.95 121.75 5,584.65 01/18/05 56.05 54.10 5,584.98 02128/05 55.72 53.77 5,585.15 03/15/05 55.55 53.60 5,586.25 04126/05 54.45 52.50 5,586.79 05124/05 53.91 51.96 5,586.52 06/30105 54.18 52.23 5,586.03 07129/05 54.67 52.72 5,586.05 09/12/05 54.65 52.70 5,585.80 12/07/05 54.90 52.95 5,587.06 03/08/06 53.64 51.69 5,585.90 06/13/06 54.80 52.85 5,585.32 07/18/06 55.38 53.43 5,585.35 11107/06 55.35 53.40 5585.81 02127/07 54.89 52.94 5,585.20 05/02/07 55.50 53.55 5,586.66 08114/07 54.04 52.09 5,586.80 10/10/07 53.90 51.95 5,588.48 03126/08 52.22 50.27 5,586.51 06124/08 54.19 52.24 5,586.45 08126/08 54.25 52.30 5,585.40 10/14/08 55.3 53.35 5,584.80 03/03/09 55.9 53.95 5,584.73 06/24/09 55.97 54.02 5,584.36 09/10109 56.34 54.39 5,585.02 12/11109 55.68 53.73 5,585.66 03111110 55.04 53.09 5,584.86 05/11/10 55.84 53.89 5,584.55 09129/10 56.15 54.20 5,584.17 12121110 56.53 54.58 5,583.55 02128/11 57.15 55.20 5,584.72 06/21111 55.98 54.03 5,584.62 09120/11 56.08 54.13 Water Levels and Data over Time White Mesa Mill -Well TW 4-6 Total or Measuring Measured Total Total Water Land Point Depth to Depth to Depth Of Elevation Surface Elevation Length Of Date Of Water Water Well (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) (blw.LSD) 5,607.33 5,608.78 1.450 98.55 5,522.28 OS/25/00 86.50 85.05 5,521.51 06/09/00 87.27 85.82 5,522.35 06/16/00 86.43 84.98 5,522.14 06/26/00 86.64 85.19 5,522.25 07/06/00 86.53 85.08 5,522.13 07/13/00 86.65 85.20 5,522.17 07/18/00 86.61 85.16 5,522.26 07/25/00 86.52 85.07 5,522.31 08/02/00 86.47 85.02 5,522.33 08/09/00 86.45 85.00 5,522.35 08/15/00 86.43 84.98 5,522.40 08/31/00 86.38 84.93 5,522.40 09/08/00 86.38 84.93 5,522.45 09/13/00 86.33 84.88 5,522.53 09/20/00 86.25 84.80 5,522.39 10/05/00 86.39 84.94 5,522.42 11/09/00 86.36 84.91 5,522.29 12/06/00 86.49 85.04 5,522.63 01/03/01 86.15 84.70 5,522.72 02/09/01 86.06 84.61 5,522.90 03/26/01 85.88 84.43 5,522.70 04/30/01 86.08 84.63 5,522.89 05/31/01 85.89 84.44 5,522.88 06/20/01 85.90 84.45 5,522.96 07/10/01 85.82 84.37 5,523.10 08/20/01 85.68 84.23 5,523.23 09/19/01 85.55 84.10 5,523.21 10/02/01 85.57 84.12 5,523.25 11/08/01 85.53 84.08 5,523.46 12/03/01 85.32 83.87 5,523.36 01/03/02 85.42 83.97 5,523.50 02/06/02 85.28 83.83 5,523.94 03/26/02 84.84 83.39 5,523.75 04/09/02 85.03 83.58 5,524.23 OS/23/02 84.55 83.10 5,523.98 06/05/02 84.80 83.35 5,524.31 07/08/02 84.47 83.02 5,524.36 08/23/02 84.42 82.97 5,524.49 09/11/02 84.29 82.84 5,524.71 10/23/02 84.07 82.62 5,524.60 11/22/02 84.18 82.73 5,524.94 12/03/02 83.84 82.39 5,525.10 01/09/03 83.68 82.23 Water Levels and Data over Time White Mesa Mill -Well TW 4-6 Total or Measuring Measured Total Total Water Land Point Depth to Depth to Depth Of Elevation Surface Elevation Length Of Date Of Water Water Well (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) (blw.LSD) 5,607.33 5,608.78 1.450 98.55 5,525.15 02112/03 83.63 82.18 5,525.35 03/26/03 83.43 81.98 5,525.68 04/02/03 83.10 81.65 5,525.74 05/01103 83.04 81.59 5,525.98 06/09103 82.80 81.35 5,526.04 07/07/03 82.74 81.29 5,526.07 08/04/03 82.71 81.26 5,526.42 09/11103 82.36 80.91 5,526.30 10102/03 82.48 81.03 5,526.41 11107/03 82.37 80.92 5,526.46 12/03/03 82.32 80.87 5,526.83 01115/04 81.95 80.50 5,526.81 02110104 81.97 80.52 5,527.14 03/28/04 81.64 80.19 5,527.39 04112/04 81.39 79.94 5,527.64 05/13/04 81.14 79.69 5,527.70 06/18/04 81.08 79.63 5,528.16 07/28/04 80.62 79.17 5,528.30 08/30104 80.48 79.03 5,528.52 09116/04 80.26 78.81 5,528.71 10/11104 80.07 78.62 5,528.74 11116/04 80.04 78.59 5,529.20 12/22/04 79.58 78.13 5,528.92 01/18/05 79.86 78.41 5,529.51 02/28/05 79.27 77.82 5,529.74 03115/05 79.04 77.59 5,529.96 04/26/05 78.82 77.37 5,530.15 OS/24/05 78.63 77.18 5,530.35 06/30105 78.43 76.98 5,530.47 07/29105 78.31 76.86 5,530.95 09/12/05 77.83 76.38 5,531.50 12/07/05 77.28 75.83 5,532.43 03/08/06 76.35 74.90 5,533.49 06/13/06 75.29 73.84 5,532.58 07118/06 76.20 74.75 5,532.88 11/07/06 75.90 74.45 5534.09 02/27/07 74.69 73.24 5,534.04 05/02/07 74.74 73.29 5,534.43 08114/07 74.35 72.90 5,554.54 10/10/07 54.24 52.79 5,535.40 03/26/08 73.38 71.93 5,535.55 06/24/08 73.23 71.78 5,535.90 08/26/08 72.88 71.43 Water Levels and Data over Time White Mesa Mill -Well TW 4-6 Total or Measuring Measured Total Total Water Land Point Depth to Depth to Depth Of Elevation Surface Elevation Length Of Date Of Water Water Well (z) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) (blw.LSD) 5,607.33 5,608.78 1.450 98.55 5,535.87 10114/08 72.91 71.46 5,536.42 03110/09 72.36 70.91 5,536.71 06124/09 72.07 70.62 5,536.83 09/10/09 71.95 70.50 5,537.35 12111109 71.43 69.98 5,537.93 03111110 70.85 69.40 5,538.14 05111/10 70.64 69.19 5,538.03 09129/10 70.75 69.30 5,538.04 12121110 70.74 69.29 5,537.98 02128111 70.8 69.35 5,538.46 06121111 70.32 68.87 5,538.37 09120111 70.41 68.96 Water Levels and Data over Time White Mesa Mill -Well TW 4-7 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Depth Elevation Surface Elevation Length Of Date Of Water Water Of Well (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) (blw.LSD) 5,619.87 5,621.07 1.20 119.8 5,552.37 11129/99 68.70 67 .50 5,553.57 01/02/00 67.50 66.30 5,553.87 01/10/00 67.20 66 .00 5,553.72 01/17/00 67.35 66.15 5,553.97 01/24/00 67.10 65 .90 5,553.87 02/01/00 67.20 66.00 5,553.87 02/07/00 67.20 66.00 5,554.17 021l4/00 66.90 65.70 5,554.27 02123 /00 66.80 65.60 5,554.37 03/01/00 66.70 65.50 5,554.37 03/08/00 66.70 65.50 5,554.27 03/15/00 66.80 65.60 5,554.77 03/20/00 66.30 65.10 5,554.57 03129/00 66.50 65.30 5,554.27 04/04/00 66.80 65.60 5,554.57 04/13/00 66.50 65.30 5,554.77 04/21/00 66.30 65.10 5,554.87 04128/00 66.20 65.00 5,554.87 05/01/00 66.20 65.00 5,555.27 05/11/00 65.80 64.60 5,554.97 05/15/00 66.10 64.90 5,555.27 OS/25/00 65.80 64.60 5,555.33 06/09/00 65 .74 64.54 5,555.45 06/16/00 65.62 64.42 5,555.22 06126/00 65 .85 64.65 5,555.45 07/06/00 65.62 64.42 5,555.40 07/13/00 65.67 64.47 5,555.45 07/18/00 65.62 64.42 5,555.59 07/27/00 65.48 64.28 5,555.65 08/02/00 65.42 64.22 5,555.70 08/09/00 65.37 64.17 5,555.74 08/16/00 65.33 64.13 5,555.96 08/31/00 65.11 63 .91 5,555.87 09/08/00 65.20 64.00 5,555.95 09/13/00 65.12 63 .92 5,556.05 09/20/00 65.02 63 .82 5,556.06 10/05/00 65.01 63 .81 5,556.17 10/12/00 64.90 63.70 5,556.20 10119/00 64.87 63.67 5,556.22 10123/00 64.85 63.65 5,556.36 11/09/00 64.71 63 .51 5,556.42 11114/00 64.65 63.45 5,556.45 11/30/00 64.62 63.42 Water Levels and Data over Time White Mesa Mill -Well TW 4-7 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Depth Elevation Surface Elevation Length Of Date Of Water Water Of Well (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) (blw.LSD) 5,619.87 5,621.07 1.20 119 .8 5,556.15 12/06/00 64.92 63.72 5,556.89 01/14/01 64.18 62.98 5,557.07 02/09101 64.00 62.80 5,557.62 03129101 63.45 62.25 5,557.51 04/30101 63.56 62.36 5,557.77 05 /31/01 63.30 62.10 5,557.84 06/21101 63.23 62.03 5,557.98 07110101 63.09 61.89 5,558.33 08120101 62.74 61.54 5,558.57 09/19101 62.50 61.30 5,558.53 10/02/01 62.54 61.34 5,558.62 11108/01 62.45 61.25 5,559.03 12/03/01 62.04 60.84 5,559.08 01103/02 61.99 60.79 5,559.32 02/06/02 61.75 60.55 5,559.63 03/26/02 61.44 60.24 5,559.55 04/09102 61.52 60.32 5,560.06 05123/02 61.01 59.81 5,559.91 06/05102 61.16 59.96 5,560.09 07/08/02 60.98 59.78 5,560.01 08123/02 61.06 59.86 5,560.23 09/11/02 60.84 59.64 5,560.43 10/23/02 60.64 59.44 5,560.39 11122/02 60.68 59.48 5,560.61 12/03/02 60.46 59.26 5,560.89 01109103 60.18 58.98 5,560.94 02/12/03 60.13 58.93 5,561.28 03126/03 59.79 58.59 5,561.35 04/02/03 59.72 58.52 5,546.20 05101103 74.87 73 .67 5,539.47 06/09/03 81.60 80.40 5,541.87 07/07/03 79.20 78.00 5,542.12 08/04/03 78.95 77.75 5,541.91 09111/03 79.16 77 .96 5,544.62 10102/03 76.45 75.25 5,542.67 11/07/03 78.40 77.20 5,549.96 12/03/03 71.11 69.91 5,557.17 01/15104 63.90 62.70 5,558.65 02/10/04 62.42 61.22 5,559.90 03/28/04 61.17 59.97 5,560.36 04/12/04 60.71 59.51 5,560.87 05/13/04 60.20 59.00 5,560.95 06/18/04 60.12 58.92 Water Levels and Data over Time White Mesa Mill -Well TW 4-7 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Depth Elevation Surface Elevation Length Of Date Of Water Water Of Well (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) (blw.LSD) 5,619.87 5,621.07 1.20 119.8 5,561.64 07/28/04 59.43 58.23 5,543.00 08/30104 78.07 76.87 5,541.91 09/16104 79.16 77.96 5,540.08 10/11104 80.99 79.79 5,546.92 11116/04 74.15 72.95 5,546.97 12/22/04 74.10 72.90 5,546.51 01118/05 74.56 73 .36 5,546.66 02/28/05 74.41 73.21 5,546.81 03/15105 74.26 73.06 5,548.19 04126105 72.88 71.68 5,547.11 05/24/05 . 73 .96 72.76 5,546.98 06/30105 74.09 72.89 5,546.92 07/29105 74.15 72.95 5,547.26 09/12/05 73.81 72.61 5,547.26 12/07/05 73.81 72.61 5,548.86 03/08/06 72.21 71.01 5,548.62 06/13/06 72.45 71.25 5,550.04 07/18/06 71.03 69.83 5,548.32 11107/06 72.75 71.55 5,550.44 02127/07 70.63 69.43 5,549.69 05102/07 71.38 70.18 5,549.97 08/14/07 71.10 69.90 5,550.30 10/10/07 70.77 69.57 5,551.92 03126108 69.15 67.95 5,552.94 06124/08 68.13 66.93 5,552.34 08/26108 68.73 67.53 5,552.61 10/14/08 68.46 67.26 5,552.81 03/10/09 68.26 67.06 5,553.11 06124/09 67.96 66.76 5,552.55 09/10109 68.52 67.32 5,553.06 12/11109 68.01 66.81 5,554.64 03/11110 66.43 65.23 5,554.20 05111110 66.87 65.67 5,553.45 09/29110 67 .62 66.42 5,553.40 12/21/10 67 .67 66.47 5,553.93 02/28111 67 .14 65.94 5,553.67 06/21111 67.4 66.20 5,553.46 09120/11 67.61 66.41 Water Levels and Data over Time White Mesa Mill -Well TW 4-8 Total or Measuring Measured Water Land Point Depth to Total Depth Total Elevation Surface Elevation Length Of Date Of Water to Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,616.80 5,621.40 4.60 126.00 5,546.40 11129/99 75.00 70.40 5,546.20 01/02/00 75.20 70.60 5,546.50 01/10/00 74.90 70.30 5,546.30 01/17/00 75.10 70.50 5,546.60 01/24/00 74.80 70.20 5,546.50 02/01/00 74.90 70.30 5,546.50 02/07/00 74.90 70.30 5,546.90 02/14/00 74.50 69.90 5,546.95 02123/00 74.45 69.85 5,547.05 03/01/00 74.35 69.75 5,547.05 03/08/00 74.35 69.75 5,547.10 03/15/00 74.30 69.70 5,547.50 03/20/00 73.90 69.30 5,547.40 03/29/00 74.00 69.40 5,547.20 04/04/00 74.20 69.60 5,547.40 04/13/00 74.00 69.40 5,547.60 04/21/00 73.80 69.20 5,547.70 04/28/00 73.70 69.10 5,547.70 05/01/00 73.70 69.10 5,548.00 05/11/00 73.40 68.80 5,547.70 05/15/00 73.70 69.10 5,547.90 05125/00 73.50 68.90 5,547.90 06/09/00 73.50 68.90 5,548.00 06/16/00 73.40 68.80 5,547.87 06126/00 73.53 68.93 5,547.95 07/06/00 73.45 68.85 5,547.96 07/13/00 73.44 68.84 5,547.95 07/18/00 73.45 68.85 5,548.11 07127/00 73.29 68.69 5,548.15 08/02/00 73.25 68.65 5,548.17 08/09/00 73.23 68.63 5,548.16 08/15/00 73.24 68.64 5,548.40 08/31/00 73.00 68.40 5,548.50 09/08/00 72.90 68.30 5,548.62 09/13/00 72.78 68.18 5,548.75 09120/00 72.65 68.05 5,548.76 10/05/00 72.64 68.04 5,549.00 11/09/00 72.40 67.80 5,548.85 12/06/00 72.55 67.95 5,549.47 01/03/01 71.93 67.33 5,549.89 02/09/01 71.51 66.91 5,550.37 03/27/01 71.03 66.43 5,550.50 04/30/01 70.90 66.30 Water Levels and Data over Time White Mesa Mill -Well TW 4-8 Total or Measuring Measured Water Land Point Depth to Total Depth Total Elevation Surface Elevation Length Of Date Of Water to Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,616.80 5,621.40 4.60 126.00 5,550.68 05/31/01 70.72 66.12 5,550.68 06/20101 70.72 66.12 5,551.02 07/10101 70.38 65.78 5,551.32 08/20101 70.08 65.48 5,551.49 09/19101 69.91 65.31 5,551.64 10/02/01 69.76 65.16 5,551.81 11/08/01 69.59 64.99 5,552.22 12/03/01 69.18 64.58 5,552.16 01103/02 69.24 64.64 5,552.38 02/06102 69.02 64.42 5,552.85 03/26102 68.55 63.95 5,552.83 04/09102 68.57 63.97 5,553.20 OS/23/02 68.20 63.60 5,553.16 06105/02 68.24 63.64 5,553.32 07 /08/02 68.08 63.48 5,553.49 08 /23/02 67.91 63.31 5,553.69 09/11/02 67.71 63.11 5,554.09 10/23/02 67 .31 62.71 5,554.02 11/22/02 67.38 62.78 5,554.23 12/03/02 67 .17 62.57 5,554.43 01109103 66.97 62.37 5,554.42 02/12/03 66.98 62.38 5,554.71 03126103 66.69 62.09 5,554.83 04/02/03 66.57 61.97 5,552.21 05/01/03 69.19 64.59 5,547.93 06109103 73.47 68.87 5,546.97 07/07/03 74.43 69.83 5,546.58 08/04/03 74.82 70.22 5,546.24 09/11/03 75.16 70.56 5,546.38 10/02/03 75.02 70.42 5,546.40 11107/03 75 .00 70.40 5,546.59 12/03/03 74.81 70.21 5,551.29 01115/04 70.11 65.51 5,552.69 02110104 68.71 64.11 5,554.06 03128/04 67.34 62.74 5,554.52 04/12/04 66.88 62.28 5,555.06 05/13/04 66.34 61.74 5,555.11 06/18/04 66.29 61.69 5,555.88 07/28/04 65.52 60.92 5,552.97 08/30104 68.43 63.83 5,550.65 09116104 70.75 66.15 5,548.40 10/11104 73.00 68.40 5,548.28 11116104 73.12 68.52 Water Levels and Data over Time White Mesa Mill -Well TW 4-8 Total or Measuring Measured Water Land Point Depth to Total Depth Total Elevation Surface Elevation Length Of Date Of Water to Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,616.80 5,621.40 4.60 126.00 5,548.80 12/22/04 72.60 68.00 5,548.43 01118/05 72.97 68.37 5,548.61 02128/05 72.79 68.19 5,548.64 03/15/05 72.76 68.16 5,548.65 04126/05 72.75 68.15 5,548.85 05/24/05 72.55 67.95 5,548.73 06/30105 72.67 68.07 5,548.62 07129/05 72.78 68 .18 5,548.80 09/12/05 72.60 68.00 5,548.71 12/07/05 72.69 68.09 5,549.72 03/08/06 71.68 67 .08 5,549.70 06113/06 71.70 67.10 5,549.70 07/18/06 71.70 67.10 5,549.65 11107/06 71.75 67.15 5,551.11 02/27/07 70.29 65.69 5,550.20 05/02/07 7l.20 66.60 5,550.59 08/14/07 70.81 66.21 5,550.76 10/10/07 70.64 66.04 5,55l.95 03126/08 69.45 64.85 5,552.36 06/24/08 69.04 64.44 5,552.50 08126/08 68.9 64.30 5,552.56 10/14/08 68.84 64.24 5,552.91 03/03/09 68.49 63.89 5,553.27 06124/09 68.13 63.53 5,553.12 09110109 68.28 63.68 5,553.63 12/11109 67.77 63.17 5,554.65 03111110 66.75 62.15 5,554.57 05/11110 66.83 62.23 5,554.34 09/29/10 67.06 62.46 5,554.09 12121/10 67.31 62.71 5,554.50 02128/11 66.9 62.30 5,554.79 06/21111 66.61 62.01 5,554.63 09/20111 66.77 62.17 Water Levels and Data over Time White Mesa Mill -Well TW 4-9 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,636.11 5,637.59 1.48 121.33 5,577.09 12120/99 60.5 59.02 5,577.09 01102/00 60.5 59.02 5,577.29 01/10/00 60.3 58.82 5,577.09 01117/00 60.5 59.02 5,577.39 01124/00 60.2 58.72 5,577.29 02/01100 60.3 58.82 5,577.19 02/07/00 60.4 58.92 5,577.69 02/14/00 59.9 58.42 5,577.69 02/23/00 59.9 58.42 5,577.79 03/01/00 59.8 58.32 5,577.79 03/08/00 59.8 58.32 5,577.89 03/15/00 59.7 58.22 5,568.49 03120/00 69.1 67.62 5,578.14 03129/00 59.45 57.97 5,577.84 04/04/00 59.75 58.27 5,578.04 04/13/00 59.55 58.07 5,578.24 04/21/00 59.35 57.87 5,578.39 04128/00 59.2 57.72 5,578.39 05/01/00 59.2 57.72 5,578.79 05/11/00 58.8 57.32 5,578.39 05/15/00 59.2 57.72 5,578.79 05125/00 58.8 57.32 5,578.81 06/09/00 58.78 57.30 5,578.89 06/16/00 58.7 57.22 5,578.74 06126/00 58.85 57.37 5,578.86 07/06/00 58.73 57.25 5,578.87 07/13/00 58.72 57.24 5,578.84 07/18/00 58.75 57.27 5,579.03 07/27/00 58.56 57.08 5,579.03 08/02/00 58.56 57.08 5,579.05 08/09/00 58.54 57.06 5,579.04 08/15/00 58.55 57.07 5,579.25 08/31/00 58.34 56.86 5,579.35 09/08/00 58.24 56.76 5,579.40 09/13/00 58.19 56.71 5,579.46 09120/00 58.13 56.65 5,579.44 10/05/00 58.15 56.67 5,579.79 11/09/00 57.8 56.32 5,579.73 12/06/00 57.86 56.38 5,580.01 01/03/01 57.58 56.10 5,580.30 02/09/01 57.29 55.81 5,580.66 03/27/01 56.93 55.45 5,580.75 04/30/01 56.84 55.36 Water Levels and Data over Time White Mesa Mill -Well TW 4-9 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,636.11 5,637.59 1.48 121.33 5,581.04 05/31101 56.55 55.07 5,581.12 06121/01 56.47 54.99 5,581.15 07/10/01 56.44 54.96 5,581.51 08120101 56.08 54.60 5,581.70 09/19101 55.89 54.41 5,581.61 10/02/01 55.98 54.50 5,581.83 11108/01 55 .76 54.28 5,582.17 12/03/01 55.42 53 .94 5,582.21 01103/02 55.38 53.90 5,582.57 02/06/02 55.02 53.54 5,583.12 03126/02 54.47 52.99 5,582.77 04/09102 54.82 53.34 5,583.21 05123/02 54.38 52.90 5,582.94 06/05102 54.65 53.17 5,582.71 07/08/02 54.88 53.40 5,583.67 08123/02 53.92 52.44 5,583.82 09/11102 53.77 52.29 5,584.01 10123/02 53.58 52.10 5,583.88 11122/02 53.71 52.23 5,583.81 12/03/02 53.78 52.30 5,584.28 01109103 53.31 51.83 5,584.41 02/12/03 53.18 51.70 5,584.68 03126/03 52.91 51.43 5,584.49 04/02/03 53.10 51.62 5,584.51 05101103 53.08 51.60 5,583.59 06/09/03 54.00 52.52 5,582.96 07/07/03 54.63 . 53.15 5,582.98 08/04/03 54.61 53 .13 5,582.57 09/11103 55.02 53.54 5,582.25 10102/03 55.34 53.86 5,582.09 11107/03 55.50 54.02 5,582.48 12/03/03 55.11 53.63 5,583.69 01115104 53.90 52.42 5,583.89 02/10104 53.70 52.22 5,584.30 03128/04 53.29 51.81 5,584.59 04/12/04 53.00 51.52 5,584.87 05/13/04 52.72 51.24 5,584.96 06/18/04 52.63 51.15 5,585.50 07128/04 52.09 50.61 5,584.81 08/30104 52.78 51.30 5,584.40 09/16/04 53 .19 51.71 5,583.91 10/11104 53 .68 52.20 5,583.39 11116/04 54.20 52.72 Water Levels and Data over Time White Mesa Mill-Well TW4-9 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,636.11 5,637.59 1.48 121.33 5,583.54 12122/04 54.05 52.57 5,583.34 01118/05 54.25 52.77 5,583.66 02128/05 53.93 52.45 5,583.87 03/15105 53.72 52.24 5,584.74 04126/05 52.85 51.37 5,585.26 05124/05 52.33 50.85 5,585.06 06/30105 52.53 51.05 5,584.67 07/29/05 52.92 51.44 5,584.75 09/12/05 52.84 51.36 5,584.51 12/07/05 53.08 51.60 5,585.74 03/08/06 51.85 50.37 5,584.74 06113/06 52.85 51.37 5,584.26 07118/06 53.33 51.85 5,584.21 11107/06 53.38 51.90 5,584.67 02/27/07 52.92 51.44 5,584.06 05102/07 53 .53 52.05 5,585.33 08114/07 52.26 50.78 5,585.42 10110107 52.17 50.69 5,587.01 03126/08 50.58 49.10 5,585.44 06124/08 52.15 50.67 5,585.23 08126/08 52.36 50.88 5,584.42 10114/08 53.17 51.69 5,583.59 03 /03/09 54 52.52 5,583.35 06124/09 54.24 52.76 5,582.91 09/10/09 54.68 53.20 5,583.43 12/11109 54.16 52.68 5,584.00 03111110 53.59 52.11 5,583.27 05111110 54.32 52.84 5,582.92 09/29/10 54.67 53.19 5,583.08 12121110 54.51 53.03 5,582.63 02128/11 54.96 53.48 5,583.62 06121111 53.97 52.49 5,583.52 09120/11 54.07 52.59 Water Levels and Data over Time White Mesa MiII-Well TW4-10 Total or Measuring Measured Water Land Point Depth to Total Depth Total Elevation Surface Elevation Length Of Date Of Water to Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,631.99 5,634.24 2.25 111 5,576.75 01103/02 57.49 55.24 5,576.92 02/06/02 57.32 55 .07 5,577.43 03126/02 56.81 54.56 5,577.22 04/09/02 57.02 54.77 5,577.80 05123/02 56.44 54.19 5,577.47 06/05/02 56.77 54.52 5,577.55 07/08/02 56.69 54.44 5,578.10 08/23/02 56.14 53.89 5,578.24 09/11/02 56.00 53.75 5,578.49 10/23/02 55.75 53 .50 5,578.43 11122/02 55.81 53.56 5,578.43 12/03/02 55.81 53.56 5,578.66 01109/03 55.58 53.3 3 5,578.66 02/12/03 55.58 53.33 5,578.78 03126/03 55.46 53.21 5,578.90 04/02/03 55.34 53.09 5,578.83 05/01103 55.41 53.16 5,578.05 06/09/03 56.19 53.94 5,577.38 07/07/03 56.86 54.61 5,577.15 08/04/03 57.09 54.84 5,576.76 09111103 57.48 55.23 5,576.36 10/02/03 57.88 55.63 5,576.05 11107/03 58.19 55.94 5,576.20 12/03/03 58 .04 55.79 5,577.43 01115/04 56.81 54.56 5,577.81 02110/04 56.43 54.18 5,578.47 03128/04 55.77 53.52 5,578.69 04/12/04 55.55 53.30 5,578.93 05/13/04 55.31 53.06 5,578.99 06/18/04 55.25 53.00 5,579.18 07/28/04 55.06 52.81 5,579.06 08/30/04 55.18 52.93 5,578.78 09116/04 55.46 53.21 5,577.80 10111104 56.44 54.19 5,577.13 11/16/04 57.11 54.86 5,576.96 12/22/04 57.28 55 .03 5,576.63 01118/05 57.61 55.36 5,576.82 02128/05 57.42 55.17 5,576.86 03115/05 57.38 55 .13 5,577.52 04126/05 56.72 54.47 5,578.01 OS/24/05 56.23 53.98 5,578.15 06/30/05 56.09 53.84 5,577.90 07129/05 56.34 54.09 Water Levels and Data over Time White Mesa Mill-Well TW4-10 Total or Measuring Measured Water Land Point Depth to Total Depth Total Elevation Surface Elevation Length Of Date Of Water to Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,631.99 5,634.24 2.25 III 5,578.02 09/12/05 56.22 53.97 5,577.56 12/07/05 56.68 54.43 5,579.69 03/08/06 54.55 52.30 5,578.34 06/13/06 55.90 53.65 5,577.94 07/18/06 56.30 54.05 5,578.01 11/07/06 56.23 53.98 5578.43 02/27/07 55.81 53.56 5,577.84 05/02/07 56.40 54.15 5,578.74 08/14/07 55.50 53.25 5,579.04 10/10107 55.20 52.95 5,580.69 03/26/08 53.55 51.30 5,579.87 06/24/08 54.37 52.12 5,579.47 08/26/08 54.77 52.52 5,578.87 10/14/08 55.37 53.12 5,578.01 03/10109 56.23 53.98 5,577.85 06/24/09 56.39 54.14 5,577.49 09/10109 56.75 54.50 5,577.98 12/11/09 56.26 54.01 5,578.38 03/11/10 55.86 53.61 5,578.16 05/11/10 56.08 53.83 5,577.85 09129/10 56.39 54.14 5,577.28 12/21/10 56.96 54.71 5,577.14 02/28/11 57.1 54.85 5,578.09 06/21/11 56.15 53.90 5,578.24 09120111 56 53.75 Water Levels and Data over Time White Mesa Mill -Well TW 4-11 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,621.92 5,623.62 1.70 100 5,548.32 01103/02 75.30 73.60 5,548.73 02/06/02 74.89 73.19 5,549.03 03/26/02 74.59 72.89 5,548.84 04/09102 74.78 73.08 5,549.30 OS/23/02 74.32 72.62 5,549.01 06/05/02 74.61 72.91 5,549.22 07/08/02 74.40 72.70 5,549.44 08/23/02 74.18 72.48 5,549.57 09/11102 74.05 72.35 5,549.64 10/23/02 73.98 72.28 5,549.58 11122/02 74.04 72.34 5,549.62 12/03/02 74.00 72.30 5,549.85 01109/03 73.77 72.07 5,549.91 02112/03 73.71 72.01 5,550.15 03/26/03 73.47 71.77 5,550.01 04/02/03 73.61 71.91 5,550.31 05/01103 73.31 71.61 5,550.44 06/09103 73.18 71.48 5,550.33 07/07/03 73.29 71.59 5,550.35 08/04/03 73.27 71.57 5,550.44 09111103 73.18 71.48 5,550.47 10102/03 73.15 71.45 5,550.60 11/07/03 73.02 71.32 5,550.60 12/03/03 73.02 71.32 5,550.94 01115/04 72.68 70.98 5,551.00 02110104 72.62 70.92 5,550.34 03/28/04 73.28 71.58 5,551.54 04/12/04 72.08 70.38 5,551.89 05/13/04 71.73 70.03 5,551.94 06118/04 71.68 69.98 5,552.49 07/28/04 71.13 69.43 5,552.74 08/30104 70.88 69.18 5,553.01 09/16/04 70.61 68.91 5,553.11 10111/04 70.51 68.81 5,553.19 11116/04 70.43 68.73 5,553.53 12/22/04 70.09 68.39 5,553.31 01118/05 70.31 68.61 5,553.84 02/28/05 69.78 68.08 5,554.04 03115/05 69.58 67 .88 5,554.23 04/26/05 69.39 67.69 5,553.87 05/24/05 69.75 68.05 5,554.46 06/30105 69.16 67.46 5,554.57 07/29105 69.05 67.35 Water Levels and Data over Time White Mesa Mill -Well TW 4-11 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,621.92 5,623.62 1.70 100 5,553.86 09/12/05 69.76 68.06 5,555.30 12/07/05 68.32 66.62 5,556.20 03/08/06 67.42 65 .72 5,556.48 06114/06 67.14 65.44 5,556.37 07118/06 67.25 65.55 5,556.94 11 /07/06 66.68 64.98 5557.92 02/27/07 65.7 64 5,557 .84 05/02/07 65.78 64.08 5,558.02 08115/07 65.60 63.90 5,557.13 10/10/07 66.49 64.79 5,569.74 03/26/08 53 .88 52.18 5,561.01 06/24/08 62.61 60.91 5,562.07 08/26/08 61 .55 59.85 5,562.47 10/14/08 61.15 59.45 5,563.80 03110109 59.82 58 .12 5,564.27 06/24/09 59.35 57.65 5,564.32 09/10/09 59.3 57.60 5,564.70 12/11109 58.92 57.22 5,565.14 03/11110 58.48 56.78 5,565.61 05111110 58.Q1 56.31 5,565.67 09/29110 57.95 56.25 5,565.62 12/21110 58 56.30 5,565.42 02/28/11 58.2 56.50 5,566.01 06/21111 57.61 55.91 5,566.03 09/20/11 57.59 55.89 Water Levels and Data over Time White Mesa Mill -Well TW 4-12 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,622.38 5,624.23 1.85 101.5 5,580.91 08/23/02 43.32 41.47 5,581.54 09/11102 42.69 40.84 5,581.33 10/23/02 42.90 41.05 5,581.47 11122/02 42.76 40.91 5,581.55 12/03/02 42.68 40.83 5,582.58 01109/03 41.65 39.80 5,582.47 02112/03 41.76 39.91 5,582.71 03/26/03 41.52 39.67 5,582.11 04/02/03 42.12 40.27 5,582.92 05/0ll03 41.31 39.46 5,583.13 06/09/03 41.10 39.25 5,583.21 07/07/03 41.02 39.17 5,583.31 08/04/03 40.92 39.07 5,583.55 09/1l103 40.68 38.83 5,583.72 10/02/03 40.51 38.66 5,583.77 11107/03 40.46 38.61 5,584.01 12/03/03 40.22 38.37 5,584.37 01115/04 39.86 38.01 5,584.39 02/10/04 39.84 37.99 5,584.51 03/28/04 39.72 37.87 5,584.90 04/12/04 39.33 37.48 5,584.88 05/13/04 39.35 37.50 5,584.93 06/18/04 39.30 37.45 5,585.36 07/28/04 38.87 37.02 5,585.38 08/30/04 38.85 37.00 5,585.49 09/16/04 38.74 36.89 5,585.85 1O/1l104 38.38 36.53 5,585.91 11/16/04 38.32 36.47 5,586.35 12/22/04 37.88 36.03 5,586.14 01118/05 38.09 36.24 5,586.56 02/28/05 37.67 35.82 5,586.95 03/15/05 37.28 35.43 5,587.20 04/26/05 37.03 35.18 5,587.35 OS/24/05 36.88 35.03 5,587.58 06/30/05 36.65 34.80 5,587.58 07/29/05 36.65 34.80 5,587.94 09/12/05 36.29 34.44 5,588.43 12/07/05 35.80 33.95 5,588.92 03/08/06 35.31 33.46 5,588.34 06/13/06 35.89 34.04 5,588.33 07/18/06 35.90 34.05 5,584.70 11107/06 39.53 37.68 5588.85 02/27/07 35.38 33.53 Water Levels and Data over Time White Mesa Mill -Well TW 4-12 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,622.38 5,624.23 1.85 101.5 5,588.53 05102/07 35.70 33.85 5,586.49 08/14/07 37.74 35.89 5,586.68 10110107 37.55 35.70 5,587.76 03126/08 36.47 34.62 5,587.59 06124/08 36.64 34.79 5,587.35 08/26/08 36.88 35.03 5,586.84 10/14/08 37.39 35.54 5,586.17 03/03/09 38.06 36.21 5,585.74 06124/09 38.49 36.64 5,585.54 09/10/09 38.69 36.84 5,585.77 12111/09 38.46 36.61 5,585.88 03/11110 38.35 36.50 5,586.35 05111110 37.88 36.03 5,585.68 09129/10 38.55 36.70 5,585.09 12121110 39.14 37.29 5,584.65 02128111 39.58 37.73 5,584.76 06121111 39.47 37.62 5,584.32 09120111 39.91 38.06 Water Levels and Data over Time White Mesa Mill-Well TW4-13 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,618.09 5,619.94 1.85 102.5 5,529.66 08/23/02 90.28 88.43 5,530.66 09111102 89.28 87.43 5,529.10 10/23/02 90.84 88.99 5,530.58 11122/02 89.36 87.51 5,530.61 12/03/02 89.33 87.48 5,529.74 01109/03 90.20 88.35 5,531.03 02/12/03 88.91 87 .06 5,531.82 03/26/03 88.12 86.27 5,524.63 04/02/03 95.31 93.46 5,531.54 05/01103 88.40 86.55 5,538.46 06/09/03 81.48 79.63 5,539.38 07/07/03 80.56 78.71 5,540.72 08/04/03 79.22 77.37 5,541.25 09/11103 78.69 76.84 5,541.34 10102/03 78.60 76.75 5,541.69 11107/03 78.25 76.40 5,541.91 12/03/03 78.03 76.18 5,542.44 01115/04 77.50 75.65 5,542.47 02/10/04 77.47 75.62 5,542.84 03/28/04 77.10 75.25 5,543.08 04/12/04 76.86 75.01 5,543.34 05/13/04 76.60 74.75 5,543.40 06/18/04 76.54 74.69 5,544.06 07/28/04 75.88 74.03 5,544.61 08/30104 75.33 73.48 5,545.23 09/16/04 74.71 72.86 5,546.20 10/11104 73.74 71.89 5,547.43 11116/04 72.51 70.66 5,548.96 12/22/04 70.98 69.13 5,549.02 01118/05 70.92 69.07 5,550.66 02/28/05 69.28 67.43 5,551.26 03/15/05 68.68 66.83 5,552.23 04/26/05 67.71 65.86 5,552.87 OS/24/05 67.07 65.22 5,553.42 06/30105 66.52 64.67 5,554.00 07/29/05 65.94 64.09 5,555.21 09/12/05 64.73 62.88 5,558.13 12/07/05 61.81 59.96 5,562.93 03/08/06 57.01 55.16 5,564.39 06/13/06 55.55 53.70 5,562.09 07/18/06 57.85 56.00 5,565.49 11/07/06 54.45 52.60 5571.08 02/27/07 48.86 47.01 Water Levels and Data over Time White Mesa Mill -Well TW 4-13 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,618.09 5,619.94 1.85 102.5 5,570.63 05/02/07 49.31 47.46 5,565.24 08/14/07 54.7 52.85 5,565.83 10110107 54.11 52.26 5,569.29 03126/08 50.65 48.80 5,570.00 06124/08 49.94 48.09 5,570.41 08/26/08 49.53 47.68 5,570.64 10114/08 49.3 47.45 5,570.43 03/03/09 49.51 47.66 5,570.56 06124/09 49.38 47.53 5,570.42 09110109 49.52 47 .67 5,571.15 12111109 48.79 46.94 5,572.01 03111110 47.93 46.08 5,572.88 05111110 47.06 45 .21 5,573.17 09129110 46.77 44.92 5,573.14 12121110 46.8 44.95 5,573.10 02128111 46.84 44.99 5,573.75 06/21/11 46.19 44 .34 5,573.63 09120111 46.31 44.46 Water Levels and Data over Time White Mesa Mill -Well TW 4-14 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,610.92 5,612.77 1.85 93 5,518.90 08123/02 93.87 92.02 5,519.28 09/11102 93.49 91.64 5,519.95 10123/02 92.82 90.97 5,520.32 11122/02 92.45 90.60 5,520.42 12/03/02 92.35 90.50 5,520.70 01109/03 92.07 90.22 5,520.89 02112/03 91.88 90.03 5,521.12 03/26/03 91.65 89.80 5,521.12 04/02/03 91.65 89.80 5,521.24 05101103 91.53 89.68 5,521.34 06/09/03 91.43 89.58 5,521.36 07/07/03 91.41 89.56 5,521.35 08/04/03 91.42 89.57 5,521.30 09111/03 91.47 89.62 5,521.35 10102/03 91.42 89.57 5,521.36 11107/03 91.41 89.56 5,521.16 12/03/03 91.61 89.76 5,521.29 01115/04 91.48 89.63 5,521.36 02/10/04 91.41 89.56 5,521.46 03/28/04 91.31 89.46 5,521.54 04/12/04 91.23 89.38 5,521.59 05/13/04 91.18 89.33 5,521.69 06/18/04 91.08 89.23 5,521.71 07/28/04 91.06 89.21 5,521.76 08/30104 91.01 89.16 5,521.77 09/16/04 91.00 89.15 5,521.79 10/11104 90.98 89.13 5,521.80 11/16/04 90.97 89.12 5,521.82 12122/04 90.95 89.10 5,521.82 01/18/05 90.95 89.10 5,521.86 02128/05 90.91 89.06 5,521.85 03/15/05 90.92 89.07 5,521.91 04126/05 90.86 89.01 5,521.93 05124/05 90.84 88.99 5,521.94 06/30105 90.83 88.98 5,521.84 07129105 90.93 89.08 5,521.99 09112/05 90.78 88 .93 5,522.04 12/07/05 90.73 88.88 5,522.05 03/08/06 90.72 88 .87 5,522.27 06/13/06 90.50 88.65 5,521.92 07/18/06 90.85 89.00 5,520.17 11107/06 92.60 90.75 5522.24 02127/07 90.53 88.68 Water Levels and Data over Time White Mesa Mill -Well TW 4-14 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,610.92 5,612.77 1.85 93 5,522.47 05/02/07 90.30 88.45 5,520.74 08114/07 92.03 90.18 5,518.13 10110/07 94.64 92.79 5,522.85 03126/08 89.92 88.07 5,522.91 06124/08 89.86 88.01 5,523.01 08126/08 89.76 87.91 5,522.96 10/14/08 89.81 87.96 5,523.20 03/03/09 89.57 87.72 5,523.33 06124/09 89.44 87.59 5,523.47 09/10/09 89.3 87.45 5,523.54 12111/09 89.23 87.38 5,522.98 03111/10 89.79 87.94 5,524.01 05111110 88.76 86.91 5,524.37 09129110 88.40 86.55 5,524.62 12121110 88.15 86.30 5,524.78 02128/11 87.99 86.14 5,525.23 06/21/11 87.54 85.69 5,525.45 09120/11 87.32 85.47 Water Levels and Data over Time White Mesa Mill-Well MW-26 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,624.15 5,625.45 1.30 121.33 5,574.75 08/23/02 50.70 49.40 5,574.97 09/11102 50.48 49.18 5,575.10 10123/02 50~35 49.05 5,574.99 11122/02 50.46 49.16 5,575.28 12/03/02 50.17 48.87 5,575.41 01109/03 50.04 48.74 5,575.43 02112/03 50.02 48.72 5,575.63 03/26/03 49.82 48.52 5,575.91 04/02/03 49.54 48.24 5,575.81 05101103 49.64 48.34 5,572.36 06/09103 53.09 51.79 5,570.70 07/07/03 54.75 53.45 5,570.29 08/04/03 55 .16 53.86 5,560.94 09/11103 64.51 63.21 5,560.63 10102/03 64.82 63.52 5,560.56 11/07/03 64.89 63.59 5,564.77 12/03/03 60.68 59.38 5,570.89 01115104 54.56 53.26 5,572.55 02110104 52.90 51.60 5,574.25 03128/04 51.20 49.90 5,574.77 04/12/04 50.68 49.38 5,575.53 05/13/04 49.92 48.62 5,575.59 06/18/04 49.86 48.56 5,576.82 07/28/04 48.63 47.33 5,527.47 09116/04 97.98 96.68 5,553.97 11116/04 71.48 70.18 5,562.33 12/22/04 63.12 61.82 5,550.00 01118/05 75.45 74.15 5,560.02 04/26/05 65.43 64.13 5,546.11 OS/24/05 79.34 78.04 5,556.71 06/30105 68.74 67.44 5,554.95 07/29105 70.50 69.20 5,555.48 09112/05 69.97 68.67 5,551.09 12/07/05 74.36 73.06 5,552.85 03/08/06 72.60 71.30 5,554.30 06/13/06 71.15 69.85 5,554.87 07118/06 70.58 69.28 5,550.88 11/07/06 74.57 73.27 5558.77 02/27/07 66.68 65.38 5,548.54 05102/07 76.91 75.61 5,551.33 10/10107 74.12 72.82 5,545.56 03/26/08 79.89 78.59 5,545.56 06/25108 79.89 78 .59 Water Levels and Data over Time White Mesa Mill -Well MW -26 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,624.15 5,625.45 1.30 121.33 5,545.82 08/26/08 79.63 78.33 5,545.64 10/14/08 79.81 78.51 5,544.45 03/03/09 81.00 79.70 5,545.32 06/24/09 80.13 78.83 5,544.61 09/10/09 80.84 79.54 5,549.33 12/11109 76.12 74.82 5,543.78 03/11/10 81.67 80.37 5,545.61 05/11/10 79.84 78.54 5,547.43 09/29/10 78.02 76.72 5,544.14 12/21110 81.31 80.01 5,546.77 02/28/11 78.68 77.38 5,537.60 06/21/11 87.85 86.55 5,551.46 09/20/11 73.99 72.69 Water Levels and Data over Time White Mesa Mill-Well TW4-16 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,622.19 5,624.02 1.83 142 5,562.91 08123/02 61.11 59.28 5,563.45 09111102 60.57 58.74 5,563.75 10/23/02 60.27 58.44 5,563.68 11122/02 60.34 58.51 5,563.68 12/03/02 60.34 58.51 5,564.16 01/09/03 59.86 58.03 5,564.25 02/12/03 59.77 57.94 5,564.53 03/26/03 59.49 57.66 5,564.46 04/02/03 59.56 57.73 5,564.79 05/01103 59.23 57.40 5,564.31 06/09/03 59.71 57.88 5,563.29 07/07/03 60.73 58.90 5,562.76 08/04/03 61.26 59.43 5,561.73 09111103 62.29 60.46 5,561.04 10102/03 62.98 61.15 5,560.39 11/07/03 63.63 61.80 5,559.79 12/03/03 64.23 62.40 5,561.02 01115/04 63 61.17 5,561.75 02110104 62.27 60.44 5,562.98 03128/04 61.04 59.21 5,563.29 04/12/04 60.73 58.90 5,564.03 05/13/04 59.99 58.16 5,564.09 06118/04 59.93 58.10 5,565.08 07128/04 58.94 57 .11 5,564.56 08/30104 59.46 57.63 5,563.55 09116/04 60.47 58.64 5,561.79 10/11104 62.23 60.40 5,560.38 11116/04 63.64 61.81 5,559.71 12/22/04 64.31 62.48 5,559.14 01118/05 64.88 63.05 5,558.65 02128/05 65.37 63.54 5,558.54 03115/05 65.48 63.65 5,558.22 04126/05 65.8 63.97 5,558.54 05/24/05 65.48 63.65 5,559.24 06/30105 64.78 62.95 5,559.38 07129/05 64.64 62.81 5,559.23 09/12/05 64.79 62.96 5,557.67 12/07/05 66.35 64.52 5,557.92 03/08/06 66.10 64.27 5,558.47 06/13/06 65.55 63.72 5,558.42 07/18/06 65.60 63.77 5,558.09 11/07/06 65.93 64.10 5557.34 02127/07 66.68 64.85 Water Levels and Data over Time White Mesa Mill-Well TW4-16 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,622.19 5,624.02 1.83 142 5,547.11 05/02/07 76.91 75.08 5,558.52 08/14/07 65.5 63.67 5,559.02 10110107 65.00 63.17 5,561.04 03126/08 62.98 61.15 5,560.06 06124/08 63.96 62.13 5,559.32 08126/08 64.7 62.87 5,558.89 10114/08 65.13 63.30 5,558.40 03/03/09 65.62 63 .79 5,558.32 06124/09 65.7 63.87 5,558.03 09/10/09 65.99 64.16 5,558.81 12111109 65.21 63 .38 5,559.80 03111110 64.22 62.39 5,559.85 05111110 64.17 62.34 5,560.54 09129/10 63.48 61.65 5,558.65 12121110 65.37 63.54 5,559.26 02128/11 64.76 62.93 5,560.48 06121111 63.54 61.71 5,561.52 09120/11 62.5 60.67 Water Levels and Data over Time White Mesa Mill -Well MW -32 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,623.41 5,625.24 1.83 130.6 5,542.17 08/23/02 83.07 81.24 5,542.39 09/11/02 82.85 81.02 5,542.61 10/23/02 82.63 80.80 5,542.49 11122/02 82.75 80.92 5,542.82 12/03/02 82.42 80.59 5,543.03 01/09/03 82.21 80.38 5,543.04 02/12/03 82.20 80.37 5,543.41 03126/03 81.83 80.00 5,543.69 04/02/03 81.55 79.72 5,543.77 05101/03 81.47 79.64 5,544.01 06/09/03 81.23 79.40 5,544.05 07/07/03 81.19 79.36 5,543.99 08/04/03 81.25 79.42 5,544.17 09/11/03 81.07 79.24 5,544.06 10102/03 81.18 79.35 5,544.03 11/07/03 81.21 79.38 5,543.94 12/03/03 81.30 79.47 5,543.98 01/15104 81.26 79.43 5,543.85 02/10104 81.39 79.56 5,544.05 03128/04 81.19 79.36 5,544.33 04/12/04 80.91 79.08 5,544.55 05/13/04 80.69 78.86 5,544.59 06/18/04 80.65 78.82 5,545.08 07/28/04 80.16 78.33 5,545.26 08/30104 79.98 78.15 5,545.48 09/16/04 79.76 77.93 5,545.61 10/11/04 79.63 77.80 5,545.46 11/16/04 79.78 77.95 5,545.66 12122/04 79.58 77.75 5,545.33 01/18/05 79.91 78.08 5,545.51 02128/05 79.73 77.90 5,545.57 03/15105 79.67 77.84 5,545.46 04126/05 79.78 77.95 5,545.45 05124/05 79.79 77.96 5,545.33 06/30105 79.91 78.08 5,545.16 07129/05 80.08 78.25 5,545.54 09112/05 79.70 77.87 5,545.77 12/07/05 79.47 77.64 5,546.09 03/08/06 79.15 77.32 5,545.94 06/13/06 79.30 77.47 5,545.94 07/18/06 79.30 77.47 5,546.24 11107/06 79.00 77.17 5546.81 02/27/07 78.43 76.6 Water Levels and Data over Time White Mesa Mill -Well MW -32 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,623.41 5,625.24 1.83 130.6 5546.56 05/02/07 78.68 76.85 5546.81 08/15/07 78.43 76.6 5546.96 10/10107 78.28 76.45 5547.9 03126/08 77.34 75.51 5548.08 06125/08 77.16 75.33 5548.42 08126/08 76.82 74.99 5548.05 10/14/08 77.19 75.36 5548.29 03/03/09 76.95 75.12 5548.09 06/24/09 77.15 75.32 5547.79 09/10/09 77.45 75.62 5548.09 12/11109 77.15 75.32 5,548.50 03/11110 76.74 74.91 5,548.89 05/11110 76.35 74.52 5,548.83 09129/10 76.41 74.58 5,548.97 12121110 76.27 74.44 5,548.68 02128/11 76.56 74.73 5,549.33 06/21111 75.91 74.08 5,549.19 09/20/11 76.05 74.22 Water Levels and Data over Time White Mesa Mill -Well TW 4-18 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,639.13 5,641 .28 2.15 137.5 5,585.13 08/23/02 56.15 54.00 5,585.41 09/11102 55.87 53.72 5,585.47 10123/02 55.81 53.66 5,585.40 11122/02 55.88 53.73 5,585.68 12/03/02 55.60 53.45 5,585.90 01109/03 55.38 53.23 5,590.79 02/12/03 50.49 48.34 5,586.18 03126/03 55.10 52.95 5,586.36 04/02/03 54.92 52.77 5,586.24 05/01103 55.04 52.89 5,584.93 06/09/03 56.35 54.20 5,584.46 07/07/03 56.82 54.67 5,584.55 08/04/03 56.73 54.58 5,584.01 09/11103 57.27 55.12 5,583.67 10/02/03 57.61 55.46 5,583.50 11 /07/03 57.78 55.63 5,584.08 12/03/03 57.20 55 .05 5,585.45 01/15/04 55 .83 53.68 5,585.66 02/10/04 55.62 53.47 5,586.13 03/28/04 55 .15 53.00 5,586.39 04/12/04 54.89 52.74 5,586.66 05/13/04 54.62 52.47 5,586.77 06/18/04 54.51 52.36 5,587.35 07128/04 53 .93 51.78 5,586.34 08/30/04 54.94 52.79 5,585 .85 09/16/04 55.43 53.28 5,585 .22 10/11/04 56.06 53.91 5,584.70 11116/04 56.58 54.43 5,584.81 12122/04 56.47 54.32 5,584.68 01118/05 56.60 54.45 5,585.02 02128/05 56.26 54.11 5,585.25 03/15/05 56.03 53.88 5,586.31 04126/05 54.97 52.82 5,586.97 05124/05 54.31 52.16 5,586.58 06/30/05 54.70 52.55 5,586.10 07129/05 55.18 53 .03 5,586.05 09/12/05 55.23 53 .08 5,585.86 12/07/05 55.42 53.27 5,587.13 03/08/06 54.15 52.00 5,585.93 06/13/06 55.35 53.20 5,585.40 07/18/06 55.88 53 .73 5,585.38 11107/06 55.90 53 .75 5585.83 02127/07 55.45 53 .30 Water Levels and Data over Time White Mesa Mill -Well TW 4-18 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,639.13 5,641.28 2.15 137.5 5585.15 05102/07 56.13 53.98 5586.47 06/24/08 54.81 52.66 5586.3 08/26/08 54.98 52.83 5585.21 10/14/08 56.07 53.92 5584.47 03/03/09 56.81 54.66 5584.35 06124/09 56.93 54.78 5583.88 09/10/09 57.4 55.25 5584.43 12/11/09 56.85 54.70 5,585.26 03/11/10 56.02 53.87 5,584.17 05111/10 57.11 54.96 5,583.61 09/29/10 57.67 55 .52 5,604.29 12121110 36.99 34.84 5,583.56 02/28/11 57.72 55.57 5,584.73 06/21111 56.55 54.40 5,584.71 09120/11 56.57 54.42 Water Levels and Data over Time White Mesa Mill -Well TW 4-19 Total or Measuring Measured Water Land Point Depth to Total Depth Elevation Surface Elevation Length Of Date Of Water to Water Total Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,629.53 5,631.39 1.86 121.33 5,581.88 08/23/02 49.51 47.65 5,582.14 09111102 49.25 47.39 5,582.06 10/23/02 49.33 47.47 5,582.07 11122/02 49.32 47.46 5,582.16 12/03/02 49.23 47.37 5,582.28 01109/03 49.11 47.25 5,582.29 02/21/03 49.10 47.24 5,582.74 03/26/03 48.65 46.79 5,582.82 04/02/03 48.57 46.71 5,548.47 05/01103 82.92 81.06 5,564.76 06/09/03 66.63 64.77 5,562.53 07/07/03 68.86 67.00 5,564.10 08/04/03 67.29 65.43 5,566.01 08/30/04 65.38 63.52 5,555.16 09116/04 76.23 74.37 5,549.80 10111104 81.59 79.73 5,546.04 11/16/04 85.35 83.49 5,547.34 12/22/04 84.05 82.19 5,548.77 01118/05 82.62 80.76 5,551.18 02/28/05 80.21 78.35 5,556.81 03115/05 74.58 72.72 5,562.63 04/26/05 68.76 66.90 5,573.42 OS/24/05 57.97 56.11 5,552.94 07/29/05 78.45 76.59 5,554.00 09/12/05 77.39 75.53 5,555.98 12/07/05 75.41 73.55 5,552.00 03/08/06 79.39 77.53 5,545.74 06/13/06 85.65 83.79 5,544.06 07/18/06 87.33 85.47 5,548.81 11107/06 82.58 80.72 5543.59 02/27/07 87.8 85.94 5544.55 05/02/07 86.84 84.98 5558.97 08/15/07 72.42 70.56 5559.73 10/10/07 71.66 69.8 5569.26 03/26/08 62.13 60.27 5535.47 06/25/08 95.92 94.06 5541.41 08/26/08 89.98 88.12 5558.45 10/14/08 72.94 71.08 5536.9 03/03/09 94.49 92.63 5547.76 06/24/09 83.63 81.77 5561.48 09110/09 69.91 68.05 5548.14 12111/09 83.25 81.39 5,570.58 03111110 60.81 58.95 Water Levels and Data over Time White Mesa Mill -Well TW 4-19 Total or Measuring Measured Water Land Point Depth to Total Depth Elevation Surface Elevation Length Of Date Of Water to Water Total Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,629.53 5,631.39 1.86 121.33 5,561.35 05/11110 70.04 68.18 5,535.26 09/29/10 96.13 94.27 5,568.40 12/21110 62.99 61.13 5,550.36 02/28/11 81.03 79.17 5,570.41 06/21/11 60.98 59.12 5,567.84 09/20111 63.55 61.69 Water Levels and Data over Time White Mesa Mill -Well TW 4-20 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,628.52 5,629.53 1.01 106.0 5,565.70 07/29/05 63.83 62.82 5,546.53 08/30105 83.00 81.99 5,540.29 09112/05 89.24 88.23 5,541.17 12/07/05 88.36 87.35 5,540.33 03/08/06 89.20 88.19 5,530.43 06/13/06 99.10 98.09 5,569.13 07/18/06 60.40 59.39 5,547.95 11107/06 81.58 80.57 5,549.25 02127/07 80.28 79.27 5,550.58 05/02/07 78.95 77.94 5,563.60 08/14/07 65.93 64.92 5,555.85 10/10/07 73.68 72.67 5,569.10 03/26/08 60.43 59.42 5,560.00 06125/08 69.53 68.52 5,539.64 08/26/08 89.89 88.88 5,539.51 10/14/08 90.02 89.01 5,553.00 03/03/09 76.53 75.52 5,534.18 06124/09 95.35 94.34 5,558.39 09/10/09 71.14 70.l3 5,560.99 12/11109 68.54 67.53 5,564.09 03/11110 65.44 64.43 5,564.22 05111110 65.31 64.30 5,560.33 09129/10 69.20 68.19 5,561.35 12/21110 68.18 67.17 5,560.18 02128111 69.35 68.34 5,576.23 06/21111 53 .3 52.29 Water Levels and Data over Time White Mesa MiII-Well TW4-21 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,638.20 5,639.35 1.15 120.92 5,582.98 07129/05 56.37 55.22 5,583.43 08/30105 55 .92 54.77 5,581.87 09112/05 57.48 56.33 5,580.50 12/07/05 58.85 57 .70 5,583.64 03/08/06 55.71 54.56 5,580.55 06113/06 58.80 57.65 5,578.95 07/18/06 60.40 59.25 5,578.47 11107/06 60.88 59.73 5,579.53 02127/07 59.82 58.67 5,578.07 05/02/07 61.28 60.13 5,583.41 08115/07 55.94 54.79 5,583.45 10110107 55.9 54.75 5,586.47 03/26108 52.88 51.73 5,579.16 06124/08 60.19 59.04 5,579.92 08126108 59.43 58.28 5,577.37 10/14/08 61.98 60.83 5,578.00 03110109 61.35 60.20 5,580.14 06124/09 59.21 58.06 5,578.72 09/10/09 60.63 59.48 5,579.99 12111109 59.36 58.21 5,582.81 03111110 56.54 55.39 5,582.23 05111110 57.12 55.97 5,576.60 09/29110 62.75 61.60 5,581.14 12121110 58.21 57.06 5,579.53 02/28/11 59.82 58.67 5,584.17 06121111 55.18 54.03 5,584.80 09120/11 54.55 53.40 Water Levels and Data over Time White Mesa Mill-Well TW4-22 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,627.83 5,629.00 1.17 113.5 5,571.89 07/29/05 57.11 55.94 5,572.20 08/30/05 56.80 55.63 5,572.08 09/12/05 56.92 55.75 5,571.61 12/07/05 57.39 56.22 5,571.85 03/08/06 57.15 55.98 5,571.62 06/13/06 57.38 56.21 5,57 1.42 07118/06 57.58 56.41 5,571.02 11/07/06 57.98 56.81 5571.24 02/27/07 57.76 56.59 5,570.75 06/29/07 58.25 57.08 5,571.82 08114/07 57.18 56.01 5,571.99 10/10/07 57.01 55.84 5,573.05 03/26/08 55.95 54.78 5,573.04 06/24/08 55.96 54.79 5,573.04 08/26/08 55.96 54.79 5,573.02 10114/08 55.98 54.81 5,573.19 03/10/09 55.81 54.64 5,573.32 06/24/09 55.68 54.51 5,573.17 09/10/09 55.83 54.66 5,513.52 12/11/09 55.48 54.31 5,573.88 03/11/10 55.12 53.95 5,574.29 05/11/10 54.71 53.54 5,574.88 09/29/10 54.12 52.95 5,574.44 12/21/10 54.56 53.39 5,574.49 02/28/11 54.51 53.34 5,574.97 06/21111 54.03 52.86 5,575.06 09/20/11 53.94 52.77 Water Levels and Data over Time White Mesa Mill-Well TW4-23 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,605.77 5,607.37 1.60 113.5 5,538.89 09/13/07 68.48 66.88 5,538.80 10/10107 68.57 66.97 5,539.25 11/30107 68.12 66.52 5,539.49 12111/07 67 .88 66.28 5,539.19 01/08/08 68.18 66.58 5,539.44 02118/08 67.93 66.33 5,539.54 03/26/08 67.83 66.23 5,539.71 04/23/08 67 .66 66.06 5539.48 05/30108 67.89 66.29 5,539.53 06/24/08 67.84 66.24 5,539.44 07116/08 67.93 66.33 5,539.68 08/26/08 67.69 66.09 5,541.18 09110108 66.19 64 .59 5,539.57 10/14108 67.8 66.20 5,539.29 11/26/08 68 .08 66.48 5,539.55 12/29/08 67.82 66.22 5,540.15 01/26/09 67.22 65.62 5,539.74 02/24/09 67.63 66.03 5,539.86 03/06/09 67 .51 65.91 5,539.72 04/07/09 67.65 66.05 5,539.84 05/29/09 67.53 65.93 5,540.12 06/30109 67.25 65.65 5,540.12 07/31/09 67.25 65.65 5,540.27 08/31/09 67.1 65.50 5,540.13 09110109 67.24 65.64 5,540.64 12/11/09 66.73 65.13 5,541.15 03/11110 66.22 64.62 5,541.61 05/11110 65.76 64.16 5,541.47 09/29/10 65.90 64.30 5,541.54 12/21 /10 65.83 64.23 5,541.54 02/28111 65.83 64.23 5,541.98 06/21111 65.39 63.79 5,541.90 09/20/11 65.47 63.87 Water Levels and Data over Time White Mesa MiII-Well TW4-24 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,625.70 5,627.83 2.13 113.5 5,570.61 09/13/07 57.22 55.09 5,570.53 10/10107 57.30 55.17 5,571.16 11/30107 56.67 54.54 5,571.30 1211 1/07 56.53 54.40 5,571.03 01/08/08 56.80 54.67 5,571.22 02118/08 56.61 54.48 5,571.43 03/26/08 56.40 54.27 5,571.68 04123/08 56.15 54.02 5571.52 05/30108 56.31 54.18 5,571.34 06124/08 56.49 54.36 5,571.28 07/16/08 56.55 54.42 5,571.34 08126/08 56.49 54.36 5,571.23 09/10/08 56.60 54.47 5,57 1.12 10/14/08 56.71 54.58 5,570.95 11126/08 56.88 54.75 5,570.92 12/29/08 56.91 54.78 5,571.65 01126/09 56.18 54.05 5,571.31 02124/09 56.52 54.39 5,571.37 03/06/09 56.46 54.33 5,571.21 04/07/09 56.62 54.49 5,571.23 05/29/09 56.60 54.47 5,571.42 06/30109 56.41 54.28 5,571.38 07/31109 56.45 54.32 5,571.48 08/31/09 56.35 54.22 5,571.28 09110109 56.55 54.42 5,571.64 1211 1/09 56.19 54.06 5,571.86 03/1 1110 55.97 53.84 5,571.91 05 /11/10 55.92 53.79 5,572.18 09129/10 55.65 53.52 5,571.86 12121110 55 .97 53.84 5,571.78 02128/11 56.05 53.92 5,572.40 06/21111 55.43 53.30 5,572.19 09/20/11 55.64 53.51 Water Levels and Data over Time White Mesa Mill -Well TW 4-25 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,627.83 5,644.91 17.08 134.8 5,601.86 09/13/07 43.05 25.97 5,601.89 10/10/07 43.02 25.94 5,602.57 11/30/07 42.34 25.26 5,602.82 12/11/07 42.09 25.01 5,601.94 01/08/08 42.97 25.89 5,599.13 02/18/08 45.78 28.70 5,597.11 03/26/08 47.80 30.72 5,595.51 04/23/08 49.40 32.32 5594.42 05/30/08 50.49 33.41 5,594.26 06/24/08 50.65 33.57 5,586.67 07/16/08 58.24 41.16 5,594.17 08/26/08 50.74 33.66 5,594.23 09/10/08 50.68 33.60 5,594.12 10/14/08 50.79 33.71 5,594.06 11/26/08 50.85 33.77 5,594.87 12/29/08 50.04 32.96 5,595.89 01/26/09 49.02 31.94 5,596.27 02/24/09 48.64 31.56 5,596.47 03/06/09 48.44 31.36 5,596.74 04/07/09 48.17 31.09 5,597.55 OS/29/09 47.36 30.28 5,598.11 06/30/09 46.8 29.72 5,598.22 07/31/09 46.69 29.61 5,598.52 08/31/09 46.39 29.31 5,598.49 09/10/09 46.42 29.34 5,599.48 12/11/09 45.43 28.35 5,599.75 03/11/10 45.16 28.08 5,599.63 05/11/10 45.28 28.20 5,598.68 09/29/10 46.23 29.15 5,598.66 12/21/10 46.25 29.17 5,598.18 02/28/11 46.73 29.65 5,598.61 06/21/11 46.30 29.22 5,598.08 09/20/11 46.83 29.75 Water Levels and Data over Time White Mesa MiII-Well TW4-26 Total or Measuring Measured Total Water Land Point Depth to Depth to Total Elevation Surface Elevation Length Of Date Of Water Water Depth Of (WL) (LSD) (MP) Riser (L) Monitoring (blw.MP) (blw.LSD) Well 5,599.98 5,601.68 1.70 86 5,536.90 06/14/10 64.78 63.08 5,536.95 09129/10 64.73 63.03 5,537.17 12121110 64.51 62.81 5,537.16 02128/11 64.52 62.82 5,537.57 06121111 64.11 62.41 5,537.59 09120/11 64.09 62.39 TabH Laboratory Analytical Reports EN:RGY LI\B ORATORI ES &I. ,. www.energylab.com fr .r;\ ·H~lenQ, '~rB7H72-P711 • Billings, MT 800-135-44B9 • Casper, WY B88-23~-0515 ~I&\i An,lytIcslExc,lIsnc,Slnc, '952 )~JllMtte, ~Y86&~&B6-7i75 • R.apid City, SO 88H72-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-026 Client Sample ID: MW-4 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 41 4.9 1.1 1700 ND ND 98.0 105 92.0 87.0 D -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/17/11 13:05 DateReceived: 08/19/11 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By 1 A4500-CI B 08/25/11 16 :24 1 wc D 0.5 E353.2 08/22111 15:131 dc 1.0 SW8260B 08/27/1 1 04:281 ilr D 100 SW8260B 08/25/11 18:521 ilr 1.0 SW8260B 08/27/11 04:281 ilr 1.0 SW8260B 08/27/11 04:281 ilr 80-120 SW8260B 08/27/11 04:281 ilr 70-130 SW8260B 08/27/11 04:281 ilr 80-120 SW8260B 08/27/11 04:281 ilr 80-120 SW8260B 08/27/11 04:281 ilr MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 29 of 51 EN:RGY LABORAT ORI ES www.energylab.com An.fytlcal £XCII/snc, Sines '952 Heiena,·MT'817·472~0711 • Billings, MT BOO·735·4489 • Casper, WY 88B~23~-0515 '. 'Gillette, WV 8Ga-68~~7f75 . Rapid City, SO 888-672-1225 • College Station, IX 888-690-2218 ~R"" •• , ,. , . LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-025 Client Sample ID: TW4-1 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 36 6.8 ND 1300 ND ND 98.0 103 90.0 88.0 D -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/18/11 06:47 DateReceived: 08/19/11 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By 1 A4500-CI B 08/25/11 16:21 1 wc D 0.5 E353.2 08/22/11 15:10 1 dc 1.0 SW8260B 08/26/11 03:20 1 jlr D 100 SW8260B 08/25/11 18 :15 1 jlr 1.0 SW8260B 08/26/11 03:20 1 jlr 1.0 SW8260B 08/26/11 03:201 jlr 80-120 SW8260B 08/26/11 03 :20 1 jlr 70-130 SW8260B 08/26/11 03:20 1 jlr 80-120 SW8260B 08/26/11 03 :20 1 jlr 80-120 SW8260B 08/26/11 03 :20 1 jlr MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 28 of 51 EN:RGY LAB ORATORIES www.energylab.com AnB/ytfCIII Excs//sncs Slncs '952 Helena, MT 8~H127071i • Billings, MT 800· 735·4489 . Casper, WY 888·235·0515 ~ . ,,"01~d~, WtQ6l·6,86:717~ • Rapid City, S0888~672·1225 • College Station, TX 888·690·2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: LablD: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-029 Client Sample ID: TW4-2 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 48 6.0 1.6 2400 NO NO 113 114 120 92.0 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/17/11 06:57 DateReceived: 08/19/11 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By 1 A4500-CI B 08/25/11 16 :431 wc o 0.5 E353.2 08/22111 15:301 dc 1.0 SW8260B 08/26/11 17: 13 1 jlr o 100 SW8260B 08/26/11 14:20 1 jlr 1.0 SW8260B 08/26/11 17:131 jlr 1.0 SW8260B 08/26/11 17:13 1 jlr 80-120 SW8260B 08/26/11 17:13 1 jlr 70-130 SW8260B 08/26/11 17:13 1 jlr 80-120 SW8260B 08/26/11 17:131 jlr 80-120 SW8260B 08/26/11 17:13 1 jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 32 of 51 EN:RGY LAB ORATORIES W'MY.energylab.com Analytfcal ExCS/lsnC9 Slnc9 1152 1 -Billings, MT 800-735-4489 -Casper, WY 888-235-0515 • RapidCitYiSD.888~~72-1225 . ColiegeStalian, TX 880-6.0-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: LablD: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C 11080835-004 Client Sample ID: TW4-3 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 23 4.0 ND ND ND ND 113 108 125 91.0 D -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/16/11 14:40 DateReceived: 08/19/11 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By A4500-CI B 08/22/11 12:151 wc D 0.2 E353.2 08/22111 13:501 dc 1.0 SW8260B 08/23/11 17:351 ilr 1.0 SW8260B 08/23/11 17:35 1 ilr 1.0 SW8260B 08/23/11 17:35 1 ilr 1.0 SW8260B 08/23/11 17:351 ilr 80-120 SW8260B 08/23/11 17:351 ilr 70-130 SW8260B 08/23/11 17:351 ilr S 80-120 SW8260B 08/23/11 17:351 ilr 80-120 SW8260B 08/23/11 17:351 ilr MCl -Maximum contaminant level. ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 7 of 51 EN:RGY LAB OIl:Al ORI ES www.energylab.com AnB/ytfcal Excsl/encs Sincs 1952 n'. 'i ,.';!.'He,I~~.a.':Mr'81l-4t2~0711 . Billings, MT 800-735-4489 -Casper, WY 888-235-0515 ~~ ,Jljll~~§;,~U~6::~86-m5, • Rapid City, SO 888~'72-1225 • College Station, IX 888-6~0-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-001 Client Sample ID: TW4-3R Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result NO NO NO NO NO NO 115 104 124 90.0 Units mg/L mg/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC S -Spike recovery outside of advisory limits. Report Date: 09/06/11 Collection Date: 08/15/11 06:45 DateReceived: 08/19/11 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date 1 By A4500-CI B 08/22111 12:061 wc 0.1 E353.2 08/22111 13:431 dc 1.0 SW8260B 08/23/11 21 :38 1 jlr 1.0 SW8260B 08/23/11 21 :381 jlr 1.0 SW8260B 08/23/11 21 :38 1 jlr 1.0 SW8260B 08/23/11 21 :38 1 jlr 80-120 SW8260B 08/23/11 21 :38 1 jlr 70-130 SW8260B 08/23/11 21 :38 1 jlr S 80-120 SW8260B 08/231.11 21 :38 1 jlr 80-120 SW8260B 08/23/11 21 :38 1 jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 4 of 51 EN:RGY LA B OI1ATORI ES www.energylab.com Ma/yt/csl Excsl/,nc; Sinc, '952 ~. i;~' " 'c:~.el~.na:·' .. n ~17-412-07t 1 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 )~:~l1ll.dl' .§~,ite:~ 8667l86-7i75 • Rapi!! City, SD .88B~672-1225 • College Station, lJ( 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-027 Client Sample 10: TW4-4 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 40 6.6 NO 1500 NO NO 100 104 93.0 86.0 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/17/11 13:15 DateReceived: 08/19/11 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date 1 By A4500-CI B 08/25/11 16:271 wc o 0.5 E353.2 08/22/11 15:251 dc 1.0 SW8260B 08/27/11 05:051 jlr o 100 SW8260B 08/27/11 03:521 jlr 1.0 SW8260B 08/27/11 05:051 jlr 1.0 SW8260B 08/27/11 05:051 jlr 80-120 SW8260B 08/27/11 05:05 1 jlr 70-130 SW8260B 08/27/11 05:051 jlr 80-120 SW8260B 08/27/11 05:051 jlr 80-120 SW8260B 08/27/11 05 :05 1 jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 30 of 51 www.energylab.com Ans/ylf/lll/ hell/Inc, Slnc, 1952 EI\ERGY LAB ORATORIES • .' 'Helena, M{S77-412-0711 • Billings, MT BOO-735-44B9 · Casper, WY BB8-235-0515 "i '1 "",.,. '. ..' .. . , .. ~~!t~~!Wy~6.S~JB6·7175 • Rapid City, SDBBB~672-1225 • ColI~ge Station, IX 888-6~0-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-016 Client Sample 10: TW4-5 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: l,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 37 7.5 NO 10 NO NO 100 117 91 ,0 94.0 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/17/11 06:45 DateReceived: 08/19/11 Matrix: Aqueous MCll Qualifier Rl QCl Method Analysis Date 1 By A4500-CI B 08/25/11 14:37 1 wc 0 0.5 E353.2 08/22/11 14:351 dc 1.0 SW8260B 08/25/11 03:23 1 ilr 1.0 SW8260B 08/25/11 03:23/ ilr 1.0 SW8260B 08/25/11 03:23/ ilr 1.0 SW8260B 08/25/11 03:23 / ilr 80-120 SW8260B 08/25/11 03:23 / ilr 70-130 SW8260B 08/25/11 03 :23 / ilr 80-120 SW8260B 08/25/11 03:23/ ilr 80-120 SW8260B 08/25/11 03:23 / ilr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 19 of 51 EN:RGY LABORAT ORIES www.energylab.com Analytical Excal/snc. Sinc.1952 " ' .~,~i~n.~2M(87H12-0711 • Billings, MT 800-735·4489 . Casper, WY 888-23~-0515 . I " • ~~,(!Y 8'SH86-7n5 . Rapid City, sil 88B~672·1225 • College Station, TX 888-6eO-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-017 Client Sample ID: TW4-6 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 39 0.3 NO 16 NO NO 101 113 88.0 88.0 Units mg/L mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier RL 0.1 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 Report Date: 09/06/11 Collection Date: 08/17/11 06:55 DateReceived: 08/19/11 Matrix: Aqueous MCL! QCL Method Analysis Date 1 By A4500-CI B 08/25/11 14 :48 / wc E353.2 08/22111 14 :50 1 dc SW8260B 08/25/11 04:00 1 ilr SW8260B 08/25/11 04:00 1 ilr SW8260B 08/25/11 04:00 1 ilr SW8260B 08/25/11 04:00 / ilr SW8260B 08/25/11 04:00 / ilr SW8260B 08/25/11 04 :00 1 ilr SW8260B 08/25/11 04:00/ ilr SW8260B 08/25/11 04:001 ilr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 20 of 51 E~RGY LABORATORIES www.energylab.com Ana/yffcsl Exc8/11111e8 Sines 1951 ! ·H~je~a, Ml'·877·472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 .,~Q!II~t!Q, Wi 8tQ~686-1175·. Rapi!! City, SO 88B-~72-1225 • College Station, TJ( 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: LablD: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C 11080835-024 Client Sample 10: TW4-7 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 37 4.1 NO 1200 NO NO 98.0 107 91.0 87.0 D -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/18/11 06:36 DateReceived: 08/19/11 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By A4500-CI B 08/25/11 16:191 wc o 0.2 E353.2 08/22111 15:08 1 dc 1.0 SW8260B 08/26/11 02:44 1 jlr o 100 SW8260B 08/25/11 17 :39 1 jlr 1.0 SW8260B 08/26/11 02:441 jlr 1.0 SW8260B 08/26/11 02:441 jlr 80-120 SW8260B 08/26/11 02:441 jlr 70-130 SW8260B 08/26/11 02:44 1 jlr 80-120 SW8260B 08/26/11 02:44 1 jlr 80-120 SW8260B 08/26/11 02:441 jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 27 of 51 EN:RGY L I\B ORAT ORIES www.energylab.com Analytfcal Exell/snc, Sines 1952 Heilina, MT&77·472-0711 • Billings, MT 800·735·4489 . Casper, WV 888·235·0515 ". /" . 'r'" \.~ -.... '; <. Jlll.I~tt~ wy 86Q'f.@86·711~. Rapid City, SD.888~672-1225 • CollegeStalion, 1)( 888·6~O-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-003 Client Sample ID: TW4-7R Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result NO NO NO 2.8 NO NO 114 107 132 90.0 Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC S -Spike recovery outside of advisory limits. Report Date: 09/06/11 Collection Date: 08/17/11 08:49 DateReceived: 08/19/11 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date 1 By A4500-CI B 08/22/11 12:11 1 wc 0.1 E353.2 08/22/11 13 :48 1 dc 1.0 SW8260B 08/23/11 17:00 1 jlr 1.0 SW8260B 08/23/11 17:00 1 jlr 1.0 SW8260B 08/23/11 17:001 jlr 1.0 SW8260B 08/23/11 17:001 jlr 80-120 SW8260B 08/23/11 17:00 1 jlr 70-130 SW8260B 08/23/11 17:00 1 jlr S 80-120 SW8260B 08/23/11 17:00 1 jlr 80-120 SW8260B 08/23/11 17:00 1 jlr MCl - Maximum contaminant level. NO -Not detected at the reporting limit. Page 6 of 51 EN:RGY LA B ORAT ORIES www.energylab.com Ans/ytfr:al Exc.l/.nc, Slncs 1952 . ' . ·Heje.n~, M(877.;472-0711 • Billings, MY 800-735-4489 • Casper, WY 888-235-0515 . '!lfu~DL ]llIlttte; W,i·.86~';'$B·6-7,17~ • Rapi!! Cijy, SO 8b8~672-1225 • College Station, TX 888-6~O-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-011 Client Sample 10: TW4-8 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 46 0.1 NO NO NO NO 114 122 124 89.0 Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC S -Spike recovery outside of advisory limits. Report Date: 09/06/11 Collection Date: 08/16/11 14:50 DateReceived: 08/19/11 Matrix: Aqueous MCll Qualifier Rl QCl Method Analysis Date 1 By A4500-CI B 08/25/11 13:56 1 wc 0.1 E353.2 08/22/11 14:181 dc 1.0 SW8260B 08/24/11 01 :421 jlr 1.0 SW8260B 08/24/11 01 :42 1 jlr 1.0 SW8260B 08/24/11 01 :42 1 jlr 1.0 SW8260B 08/24/11 01:421 jlr 80-120 SW8260B 08/24/11 01 :42 1 jlr 70-130 SW8260B 08/24/11 01 :42 1 jlr S 80-120 SW8260B 08/24/11 01 :42 1 jlr 80-120 SW8260B 08/24/11 01 :421 jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 14 of 51 EN:RGY LAB ORATORIES www.energylab.com AnalytlClI £Xcsl/enc; Sincs 1952 '14 " . '.; ijei~na~ 'MT&17-41.2-o711 • Billings, MT 800-135-4489 . Casper, WY 888-235-0515 ~~'(.~ I'; :~J,I~tt~;:WY s6i~86-711~ • Rapid City, SD888~~72-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 3rd Quarter Chloroform 2011 Lab 10: C11080835-012 Client Sample 10: TW4-9 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 21 4.0 NO NO NO NO 118 129 130 92.0 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/16/11 14:21 DateReceived: 08/19/1 1 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date 1 By A4500-CIB 08/25/11 14:21 1 wc 0 0.2 E353.2 08/22/11 14 :20 1 dc 1.0 SW8260B 08/24/11 02:171 jlr 1.0 SW8260B 08/24/11 02:171 jlr 1.0 SW8260B 08/24/11 02: 171 jlr 1.0 SW8260B 08/24/11 02 :171 jlr 80-120 SW8260B 08/24/11 02:171 jlr 70-130 SW8260B 08/24/11 02: 171 jlr S 80-120 SW8260B 08/24/11 02: 171 jlr 80-120 SW8260B 08/24/11 02:17/ jlr MCl - Maximum contaminant level. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 15 of 51 . EI\ERGY LABORATORIES W'MY.energylab.com Analytical Excsl/snc' Sincs 1952 i • Billings,·Mt 800-735-44B9 · Casper, WY 88B-23~-D515 'SO 8QP~612" 1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-021 Client Sample 10: TW4-10 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 41 1.9 NO 180 NO NO 98.0 104 90.0 86.0 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/17/11 07:45 DateReceived: 08/19/11 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date 1 By A4500-CI B 08/25/1116:13/wc 0.1 E353.2 08/22/11 15 :00 1 dc 1.0 SW8260B 08/26/11 00:54/ jlr 0 10 SW8260B 08/25/11 15:50/ jlr 1,0 SW8260B 08/26/11 00:54/ jlr 1.0 SW8260B 08/26/11 00:54/ jlr 80-120 SW8260B 08/26/11 00:54/ jlr 70-130 SW8260B 08/26/11 00:54/ jlr 80-120 SW8260B 08/26/11 00:541 jlr 80-120 SW8260B 08/26/11 00:54/ jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 24 of 51 , . . Heien~, MTS77-412-0711 • Billings, MT 800-735-4489 . Casper, WY 888·235-0515 ... ·:]"._.1 '. ,(1':.1 -.:. • • • . ' ,'.~.1..:~!I!~n~, WY, 8~~\ .• 86·717~ • Rapid City, SD.888~~72-1225 • College Station, TX 888-6~0-2218 EN:RGY L A B ORAT ORIES www.energylab.com Mafytfcsl £XClI/BneB SineB 1952 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-023 Client Sample 10: TW4-11 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 48 7.1 NO 820 NO NO 100 108 89.0 89.0 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/17/11 08:07 DateReceived: 08/19/11 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By A4500-CI B 08/25/11 16:161 wc o 0.5 E353.2 08/22/11 15 :05 1 dc 1.0 SW8260B 08/26/11 02:071 jlr o 100 SW8260B 08/25/11 17:031 jlr 1.0 SW8260B 08/26/11 02:07 1 jlr 1.0 SW8260B 08/26/11 02:07 1 jlr 80-120 SW8260B 08/26/11 02:071 jlr 70-130 SW8260B 08/26/11 02:071 jlr 80-120 SW8260B 08/26/11 02:07 1 jlr 80-120 SW8260B 08/26/11 02:071 jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 26 of 51 EI\ERGY LI\B ORI\TORIE S www.energylab.com Analytical Excsllsnes Sines Ig52 !.. 1l~1~nJl,'MT8i1-472-0111 -Sillings, MT 800-135-4489 -Casper, WV 888-235-0515 , ... ~ . ..~ .. '-. ,".. ' . -. . ". . '"~GII!ette! ~i 8~.6-6B6-7175 -Rapid City, So 88B-612-1 225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C 11080835-005 Client Sample ID: TW4-12 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 31 6.8 NO NO NO NO 121 119 134 90.0 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/16/11 13:45 DateReceived: 08/19/11 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By A4500-CI B 08/22/11 12:18 1 wc o 0.5 E353.2 08/22/11 13:531 dc 1.0 SW8260B 08/23/11 18:10 1 jlr 1.0 SW8260B 08/23/11 18 :101 jlr 1.0 SW8260B 08/23/11 18:101 jlr 1.0 SW8260B 08/23/11 18:101 jlr S 80-120 SW8260B 08/23/11 18:10 1 jlr 70-130 SW8260B 08/23/11 18:101 jlr S 80-120 SW8260B 08/23/11 18:101 jlr 80-120 SW8260B 08/23/11 18:101 jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 8 of 51 EN:RGY LAB ORAT OR IES www.energylab.com Ans!ytlClI ExeBl/enes Sine, 1952 :~eJe.~~,MrBlH12-0711 • aillings, MT 800·735-4489 . Casper, WY 888-235·0515 _~~",j;ll!e.*, WY'8t&~686.1175 • Rapid City, SD.888~672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C 11080835-006 Client Sample 10: TW4-13 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 60 5.2 ND ND ND ND 117 112 133 90.0 D -RL increased due to sample matrix. Units mg/L mg/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/16/11 13:51 DateReceived: 08/19/11 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By A4500-CI B 08/22111 12 :20 1 wc D 0.5 E353.2 08/22111 13:551 dc 1.0 SW8260B 08/23/11 18:451 jlr 1.0 SW8260B 08/23/11 18 :45 1 jlr 1.0 SW8260B 08/23/11 18:451 jlr 1.0 SW8260B 08/23/11 18:451 jlr 80-120 SW8260B 08/23/11 18:45 1 jlr 70-130 SW8260B 08/23/11 18:45 1 jlr S 80-120 SW8260B 08/23/11 18:451 jlr 80-120 SW8260B 08/23/11 18:451 jlr MCL -Maximum contaminant level. ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 9 of 51 EN:RGY LABORAT ORIES www.energylab.com Analytical £XCIl/sncB Slnc, 1952 ..Helena,M(877-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 ~,~ " :~jll~e;~X:~Gc(Q86-7i7~ • RaplpCity"SD888~G72-1225 • CollegeStation,lX 888-6$0-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C 11080835-007 Client Sample ID: TW4-14 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1 ,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 33 2.6 NO NO NO NO 100 111 96.0 93.0 Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier Rl 0.1 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 Report Date: 09/06/11 Collection Date: 08/16/11 14:03 DateReceived: 08/19/11 Matrix: Aqueous MCL! QCl Method Analysis Date 1 By A4500-CI B 08/22/11 12:231 wc E353.2 08/22111 13:581 dc SW8260B 08/25/11 02 :07 1 jlr SW8260B 08/25/11 02:071 jlr SW8260B 08/25/11 02:07 1 jlr SW8260B 08/25/11 02:071 jlr SW8260B 08/25/11 02:071 jlr SW8260B 08/25/11 02:071 jlr SW8260B 08/25/11 02:071 jlr SW8260B 08/25/11 02:071 jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 10 of 51 EI\ERGY LABORAT ORIES www.energylab.com Analytfcsl [xCII/snC' Sine, '952 ;~ . Heiena;;MT877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 {!: 1'. I' .. ,,,);~. ~ !",;,;·cl , .' . - . . ~JGille~e, WY8Sn,8S-n 75 • Rapid City, SD. 888-672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-028 Client Sample 10: TW4-15 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 58 0.9 ND 720 ND 7.2 112 114 116 92.0 D -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/17/11 12:50 DateReceived: 08/19/11 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By A4500-CI B 08/25/11 16 :28 1 wc 0.1 E353.2 08/22111 15 :28 1 dc 1.0 SW8260B 08/26/11 16:39 1 ilr D 100 SW8260B 08/26/11 13:451 ilr 1.0 SW8260B 08/26/11 16:391 ilr 1.0 SW8260B 08/26/11 16:391 ilr 80-120 SW8260B 08/26/11 16 :39 1 ilr 70-130 SW8260B 08/26/11 16:391 ilr 80-120 SW8260B 08/26/11 16:391 ilr 80-120 SW8260B 08/26/11 16:391 ilr MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 31 of 51 EN:RGY L.AB ORAT ORIES www.energylab.com An,lytIcal ExcIl/encB Since 1952 'Helega, MT 877 -412-0711 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 U~i!qi~Y .6$~J~6-m.5 . Rapid City, SD.88S-672-1225 · College,Station,1X 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-018 Client Sample 10: TW4-16 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 63 1.7 NO 9.2 NO NO 103 118 88.0 86.0 Units mg/L mg/L ug/L ug/L ug/L ug/l %REC %REC %REC %REC Qualifier Rl 0.1 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 Report Date: 09/06/11 Collection Date: 08/17/11 07:05 DateReceived: 08/19/11 Matrix: Aqueous MCL! QCl Method Analysis Date 1 By A4500-CI B 08/25/11 15:14 1 wc E353.2 08/22/11 14:53 1 dc SW8260B 08/25/11 04:38 1 ilr SW8260B 08/25/11 04:38 1 ilr SW8260B 08/25/11 04:38 1 jlr SW8260B 08/25/11 04:38 1 jlr SW8260B 08/25/11 04:38 1 jlr SW8260B 08/25/11 04:38 1 jlr SW8260B 08/25/1 1 04:381 ilr SW8260B 08/25/11 04:38 1 jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 21 of 51 www.energylab.com EN:RGY LAB ORATORIES Analytical £XcIl/enes Sines 1952 • .' ' •. 1. Ifele,na,M(817.472-071i • Billings, MT 800·735·4489 · Casper, WY 888-235-0515 C!~c..'Ii~tG!!I~ne!~~8'J~$~6-7i 75 • Ralli~ City,SD .888~672-1225 • College,Station, 1)( 888-6~0-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C 11080835-008 Client Sample ID: MW-32 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-dS Report Definitions: Rl -Analyte reporting limit, QCl -Quality control limit. Result 33 NO NO NO NO NO 9S.0 12S SS.O 91.0 Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier Rl 0.1 1.0 1.0 1.0 1,0 SO-120 70-130 SO-120 SO-120 Report Date: 09/06/11 Collection Date: 08/16/11 12:55 DateReceived: 08/19/11 Matrix: Aqueous MCll QCl Method Analysis Date 1 By A4500-CI B OS/22/11 12 :26 1 wc E353.2 OS/22111 14:00 1 dc SWS260B OS/25/11 02:451 jlr SWS260B OS/25/11 02:45 1 jlr SWS260B OS/25/11 02:45 1 jlr SWS260B OS/25/11 02:45 1 jlr SWS260B OS/25/11 02:45 1 jlr SWS260B OS/25/11 02:451 jlr SWS260B OS/25/11 02:45 1 jlr SWS260B OS/25/11 02:45 1 jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 11 of 51 EN:RGY LI\BOJ~ATORI ES www.energylab.com An./yIfca/ Exes//lncB SincB 1952 '. .'" '. ,~ej~n~ Mr817·4~2~0711 • Billings,MT 800·735·4489 • Casper, WV 888·235·0515 ~~,t ... ",->Q!I,I~!!i!J·Wy'~QlJ86.71j5 . Rapi~ City, SO 888~672·1225 • College Station, TX 888·6~0-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: LablD: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-019 Client Sample ID: TW4-18 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: RL -Analyte reporting limit. QCL -Quality control limit. Result 23 4.6 NO 29 NO NO 120 129 127 91 .0 o -RL increased due to sample matrix. Units mg/L mg/L ug/L ug/L ug/L ug/L %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/17/11 07:21 DateReceived: 08/19/11 Matrix: Aqueous MCL! Qualifier RL QCl Method Analysis Date 1 By A4500-CI B 08/25/11 15:56 1 wc o 0.5 E353.2 08/22/11 14:55 1 dc 1.0 SW8260B 08/24/11 06:201 jlr 1.0 SW8260B 08/24/11 06:20 1 jlr 1.0 SW8260B 08/24/11 06:20 1 jlr 1.0 SW8260B 08/24/11 06:20 1 jlr 80-120 SW8260B 08/24/11 06:20 1 jlr 70-130 SW8260B 08/24/11 06:201 jlr S 80-120 SW8260B 08/24/11 06:201 jlr 80-120 SW8260B 08/24/11 06:201 jlr MCL -Maximum contaminant level. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. P~ge 22 of 51 EI\ERGY l-AB ORATORIES www.energylab.com An8lytical ExCIl/sncB Sinc. 1952 .. Heleqa, Mt 877-472-0711 • Billings, MT 800-735-4489 · Casper, WY 888-235-0515 ,Giliette:WY'.866~6B6-7175 • Rapid City, SO 888-672-1225 • College Station, 1)( 888-690-2218 .v...... .i1.>:,·.li. ". • ~'., ,'.:.,' . .,' '. . " , ."' • LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C 11080835-030 Client Sample ID: TW4-19 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 148 3.0 2.1 970 ND ND 111 115 119 92.0 D -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/17/11 14:00 DateReceived: 08/19/11 Matrix: Aqueous MCll Qualifier Rl QCl Method Analysis Date 1 By A4500-CI B 08/25/11 16:471 wc D 0.2 E353.2 08/22/11 15 :33 1 dc 1.0 SW8260B 08/26/11 17 :481 jlr D 100 SW8260B 08/26/11 14:55 1 jlr 1.0 SW8260B 08/26/11 17:48 1 jlr 1.0 SW8260B 08/26/11 17:481 jlr 80-120 SW8260B 08/26/11 17:481 jlr 70-130 SW8260B 08/26/11 17:48 1 jlr 80-120 SW8260B 08/26/11 17:48 1 jlr 80-120 SW8260B 08/26/11 17:48 1 jlr MCl -Maximum contaminant level. ND -Not detected at the reporting limit. Page 33 of 51 EN:RGY L.A B ORATORIE S WIWI.energylab.com Analytical Excsllsncs SInes 1952 ·ilel~qa,Mh17·412-0711 • Billings, MT 800·735·4489 . Casper, WY 888-235-0515 ",p' }.~,~~. it'!!iII~tt~,:'wf~'66~~86-7175 • Rapid Clty,S988B~672·1225 • College.Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C 11080835-031 Client Sample 10: TW4-20 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 207 6.5 7.3 6800 NO 3.1 98.0 101 97.0 96.0 o -Rl increased due to sample matrix. Units mg/L mg/L ug/L ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/17/11 12:40 DateReceived: 08/19/11 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By A4500-CI B 08/25/11 16:49 1 wc o 0.5 E353.2 08/22/11 15:351 dc 1.0 SW8260B 08/27/11 18:471 ilr o 1000 SW8260B 08/26/11 15 :29 1 ilr 1.0 SW8260B 08/27/11 18:47 1 ilr 1.0 SW8260B 08/27/11 18:471 ilr 80-120 SW8260B 08/27/11 18:47 1 ilr 70-130 SW8260B 08/27/11 18:471 ilr 80-120 SW8260B 08/27/11 18:47 1 ilr 80-120 SW8260B 08/27/11 18:47 1 ilr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 34 of 51 . EN:RGY LABORATORIES ,( 'tleieqa, MTS1H72-D711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 :1li\l~,\t~"W:Y'86$~&86':;71 75 • Rapid City, so 888~672-'1225 • College Station, 1X 888-690-2218 www.energylab.com Analytfcal Excellsnce Slncs '952 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-022 Client Sample 10: TW4-21 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 287 14 6.3 460 NO NO 103 107 94.0 88.0 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/17/11 07:55 DateReceived: 08/19/11 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date 1 By A4500-CI B 08/25/1116:15 /wc 0 E353.2 08/22/11 15:03 1 de 1.0 SW8260B 08/27/11 05:41 1 jlr 0 10 SW8260B 08/25/11 16:26 1 jlr 1.0 SW8260B 08/27/11 05:41 1 jlr 1.0 SW8260B 08/27/11 05:41 1 jlr 80-120 SW8260B 08/27/11 05:41 1 jlr 70-130 SW8260B 08/27/11 05:41 1 jlr 80-120 SW8260B 08/27/11 05:41 1 jlr 80-120 SW8260B 08/27/11 05:41 1 jlr MCl - Maximum contaminant level. NO -Not detected at the reporting limit. Page 25 of 51 EN:RGY LAB ORATORIES www.energylab.com An./ytIcal £XcII/snell Sines 1952 , . :He!ena, MT 877-412-0711 • Billings, MT 800-135-4489 • Casper, WY 888-235-0515 ""e_~ .:.,GiII,~!t~e,'W.Y 8'Q6~$86-7175 ~ Rapip City, SD.88B~672-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: LablD: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-020 Client Sample ID: TW4-22 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1.2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 120 15 NO 450 NO NO 119 122 125 90.0 o -Rl increased due to sample matrix. Units mg/L mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/17/11 07:35 DateReceived: 08/19/11 Matrix: Aqueous MCll Qualifier Rl QCl Method AnalysiS Date 1 By A4500-CI B 08/25/11 15:571 wc o E353.2 08/22/11 14:58 1 dc 1.0 SW8260B 08/24/11 06:551 jlr o 100 SW8260B 08/25/11 05 :16 1 jlr 1.0 SW8260B 08/24/11 06:551 jlr 1.0 SW8260B 08/24/11 06:55 1 jlr 80-120 SW8260B 08/24/1 1 06:551 jlr 70-130 SW8260B 08/24/11 06:551 jlr S 80-120 SW8260B 08/24/11 06:55 1 jlr 80-120 SW8260B 08/24/11 06:55 1 jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 23 of 51 EN:RGY LI\BORA-( ORIES www.energylab.com An./ytfcs/ [xcII/.ncs Since 1952 ., I ~el(toa, 'MT ·B1l~472-0111 • Billings, MT 800-735-448~ • Casper, WY 888-235-0515 IDJ~_' ,"].!!ie,~~!y:!y 8~$-~86-7f15 • Rapid City, SO .88H72-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C 11080835-009 Client Sample 10: TW4-23 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 41 NO NO NO NO NO 122 117 135 91.0 Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC S -Spike recovery outside of advisory limits. Report Date: 09/06/11 Collection Date: 08/16/11 13: 15 DateReceived: 08/19/11 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By A4500-CI B 08/25/11 13:501 wc 0.1 E353.2 08/22/1114:13 /dc 1.0 SW8260B 08/23/11 20 :29 1 ilr 1.0 SW8260B 08/23/11 20:291 ilr 1.0 SW8260B 08/23/11 20:29 1 ilr 1.0 SW8260B 08/23/11 20:291 ilr S 80-120 SW8260B 08/23/11 20:29 1 ilr 70-130 SW8260B 08/23/11 20:29 1 ilr S 80-120 SW8260B 08/23/11 20:29 1 ilr 80-120 SW8260B 08/23/11 20:29 1 jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 12 of 51 EI\ERGY LABORATORIES www.energylab.com Analytfca' Excsl/enes Sincs /952 '1" Helenl!,MT Q17~412-0711 • Billings, MT 800-735-4489 · Casper, WY 888-235-0515 ~~ .\ I.l';'~'\~, ,'" -.,-;', .. ' ~; ~Bittte,.~Y'e&6-~"86-7175 . Rapid City, 5D.888-672-1225 • College5tation, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-014 Client Sample 10: TW4-24 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-Dichlorobenzene-d4 Surr: Dibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 967 34 ND 1.7 ND ND 121 124 124 92.0 D -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/17/11 06:25 DateReceived: 08/19/11 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date 1 By A4500-CI B 08/25/11 14:31 1 wc D E353.2 08/22/11 14:30 1 dc 1.0 SW8260B 08/24/11 03:261 jlr 1.0 SW8260B 08/24/11 03:26 1 jlr 1.0 SW8260B 08/24/11 03:26 1 jlr 1.0 SW8260B 08/24/11 03:261 jlr S 80-120 SW8260B 08/24/11 03:26 1 jlr 70-130 SW8260B 08/24/1 1 03 :26 1 jlr S 80-120 SW8260B 08/24/11 03:26 1 jlr 80-120 SW8260B 08/24/11 03 :26 1 jlr MCl -Maximum contaminant level. ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 17 of 51 EN:RGY LAB ORATORIES www.energylab.com An.IytfClI Excsl/sncs Sines 1952 Helena, MT 877-472-0111 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 , 9iil~.ttq,;kV)Y 8&.~-&86-7175 • Rapid City, SO 888-&72-1225 • College Station, TX 888-&90-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-002 Client Sample 10: TW4-24R Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result NO NO NO NO NO NO 97.0 100 92.0 88.0 Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier Rl 0.1 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 Report Date: 09/06/11 Collection Date: 08/16/11 06:40 DateReceived: 08/19/11 Matrix: Aqueous MCll QCl Method Analysis Date 1 By A4500-CI B 08/22111 12:09 1 wc E353.2 08/22111 13:451 dc SW8260B 08/25/11 01 :30 1 jlr SW8260B 08/25/11 01 :30 1 jlr SW8260B 08/25/11 01 :30 1 jlr SW8260B 08/25/11 01 :30 1 jlr SW8260B 08/25/11 01 :30 1 jlr SW8260B 08/25/11 01 :30 1 jlr SW8260B 08/25/11 01 :30 1 jlr SW8260B 08/25/11 01 :30 1 jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 5 of 51 EN:RGY LABORI\TORIES www.energylab.com An.lytlcal £XcallBnes Slnes /952 " '\ .. H~!~ri~,Mt 817-472-071 j -Billings, MY 800-135-4489 . Caspar, WY 888-235-0515 ,&C".!ill'~!1e; W(~~~~~8~~ 711~ -. Rapid City,SO 888~672-1225 • Collage Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11 080835-01 0 Client Sample 10: TW4-25 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 276 16 NO NO ND NO 117 117 128 90.0 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/16/11 12:58 DateReceived: 08/19/11 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date 1 By A4500-CI B 08/25/11 13:531 wc 0 E353.2 08/22/11 14:151 dc 1.0 SW8260B 08/24/11 01 :07 / jlr 1.0 SW8260B 08/24/11 01 :07 / jlr 1.0 SW8260B 08/24/11 01 :07 / jlr 1.0 SW8260B 08/24/11 01 :07 1 jlr 80-120 SW8260B 08/24/11 01 :07 1 jlr 70-130 SW8260B 08/24/11 01 :07 / jlr S 80-120 SW8260B 08/24/11 01 :07 1 jlr 80-120 SW8260B 08/24/11 01 :07 / jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 13 of 51 EN:RGY LABORAT ORIES www.energylab.com Analytfca' !xcIl/enc' SinclIlB52 ; IMf';'" ,;~~eie~a;;'Mra1?-472"0711 . Billings, MT 800-735-4489 · Casper, WY 888"23~-D515 .J!m~tteiY,lY 869".686-7175 • Rapid City, SD88P~672-1225 • ColiegeStation, TX 888-6~D-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab 10: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-015 Client Sample 10: TW4-26 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 19 11 NO 2.8 NO NO 120 125 127 91.0 o -Rl increased due to sample matrix. Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Report Date: 09/06/11 Collection Date: 08/17/11 06:35 DateReceived: 08/1 9/11 Matrix: Aqueous MCL! Qualifier RL QCL Method Analysis Date 1 By A4500-CI B 08/25/11 14:34 1 wc 0 E353.2 08/22/11 14 :33 1 dc 1.0 SW8260B 08/24/11 04:01 / jlr 1.0 SW8260B 08/24/11 04:01 1 jlr 1.0 SW8260B 08/24/11 04:01 / jlr 1.0 SW8260B 08/24/11 04:01 1 jlr 80-120 SW8260B 08/24/11 04:01 1 jlr 70-130 SW8260B 08/24/11 04 :01 1 jlr S 80-120 SW8260B 08/24/11 04:01 1 jlr 80-120 SW8260B 08/24/11 04:01 / jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 18 of 51 EI\ERGY L A B ORATORI ES lWIW.energylab.com AnB/ytfcal Excel/ence Since 1952 Heiena,MTQ77-412-0711 • Billings, MT 800-735-4489 · Casper, WY 888-235-0515 .J .M'~~~i ,:WY 86~JB6~ 7175 • Rapi~ City, SO 888~672-1225 • College Station, TX 888-6~O-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-032 Client Sample ID: TW4-60 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 17 NO NO NO NO NO 110 99.0 112 91.0 Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier Rl 0.1 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 Report Date: 09/06/11 Collection Date: 08/17/11 14:30 DateReceived: 08/19/11 Matrix: Aqueous MCL! QCl Method AnalysIs Date 1 By A4500-CI B 08/25/11 16:521 wc E353.2 08/22111 15 :38 1 dc SW8260B 08/26/11 13:11 1 jlr SW8260B 08/26/11 13:11 / jlr SW8260B 08/26/11 13:11/ jlr SW8260B 08/26/11 13:11 / jlr SW8260B 08/26/11 13:11 / jlr SW8260B 08/26/11 13:11 / jlr SW8260B 08/26/11 13:11 / jlr SW8260B 08/26/11 13:11/ jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 35 of 51 EN:RGY LABORATORIES www.energylab.com An.lytfCIII Excsllsncli SInes 1952 II~~'X'.·' -n111 • Billings, MTBOO-735-44B9 • Casper, W'i 888-235-0515 • R~pi~ City, so 888~672-1225 • Collegl),Stat[on, 1)( 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C 11080835-013 Client Sample ID: TW4-65 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 45 NO NO NO NO NO 119 124 130 93.0 Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC S -Spike recovery outside of advisory limits. Report Date: 09/06/11 Collection Date: 08/16/11 13: 15 DateReceived: 08/19/11 Matrix: Aqueous MCL! Qualifier Rl QCl Method Analysis Date 1 By 1 A4500-CI B 08/25/11 14:23 1 wc 0.1 E353.2 08/22/11 14:23 1 dc 1.0 SW8260B 08/24/11 02:521 jlr 1.0 SW8260B 08/24/11 02:521 jlr 1.0 SW8260B 08/24/11 02:521 jlr 1.0 SW8260B 08/24/11 02:52 1 jlr 80-120 SW8260B 08/24/11 02:52 1 jlr 70-130 SW8260B 08/24/11 02:52 1 jlr S 80-120 SW8260B 08/24/11 02:521 jlr 80-120 SW8260B 08/24/11 02:521 jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 16 of 51 EN:RGY LABORATORIES www.energylab.com Ans/yflCIII £Xcsl/sncs Slncs 1952 "\ "<, . "Helena,Mr'81'7-472-0711 . Billings, MT 800-735-4489 . Casper, WY 888-235-0515 l'';!iji ~'.&!!i~~~i·WY ~~&7686.7i 7~ • Rapid City, SD.B88~672-1225 • ColiegeStation, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-033 Client Sample ID: TW4-70 Analyses MAJOR IONS Chloride Nitrogen, Nitrate+Nitrite as N VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result 62 1.7 NO 8.1 NO 1.3 112 102 116 92.0 Units mg/l mg/l ug/l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier RL 0.1 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 Report Date: 09/06/11 Collection Date: 08/17/11 07:05 DateReceived: 08/19/11 Matrix: Aqueous MCL! QCL Method Analysis Date 1 By A4500-CI B 08/25/11 16:56 1 wc E353.2 08/22/11 15:401 dc SW8260B 08/26/11 18:231 jlr SW8260B 08/26/11 18:231 jlr SW8260B 08/26/11 18:231 jlr SW8260B 08/26/11 18:231 jlr SW8260B 08/26/11 18:231 jlr SW8260B 08/26/11 18:231 jlr SW8260B 08/26/11 18:231 jlr SW8260B 08/26/11 18 :23 1 jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 36 of 51 EN:RGY l.ABORAT ORIES www.energylab.com Anslylfcsl £XcII/.nc. Sines '952 ". .'. ',Hei~na, ~i"811-472-07t 1 • Billings, MT 800-135-4489 · Casper, WY 888-235-0515 ~~"" ;.QW!tte; Wy 866~.~86-m5 • Rapid City, SO 8BB~612-1225 • College Station, TX 888-690-2218 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C11080835-034 Client Sample ID: Trip Blank 6092 Analyses VOLATILE ORGANIC COMPOUNDS Carbon tetrachloride Chloroform Chloromethane Methylene chloride Surr: 1,2-0ichlorobenzene-d4 Surr: Oibromofluoromethane Surr: p-Bromofluorobenzene Surr: Toluene-d8 Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result NO NO NO NO 96.0 106 90.0 85.0 Units ug!l ug/l ug/l ug/l %REC %REC %REC %REC Qualifier Rl 1.0 1.0 1.0 1.0 80-120 70-130 80-120 80-120 Report Date: 09/06/11 Collection Date: 08/15/11 DateReceived: 08/19/11 Matrix: Aqueous MCl! QCl Method Analysis Date! By SW8260B 08/27/11 03:161 jlr SW8260B 08/27/11 03:161 jlr SW8260B 08/27/11 03:161 jlr SW8260B 08/27/11 03:161 jlr SW8260B 08/27/11 03 :161 jlr SW8260B 08/27/11 03:161 jlr SW8260B 08/27/11 03 :161 jlr SW8260B 08/27/11 03 :161 jlr MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 37 of 51 EI\ERGY L.AB ORATORIES 1 • Billings, MT 800-135-4489 -Casper, WY 888-235-0515 I City; SD888~672-1225 • College Station, TX 8 www.energylab.com Analytical Excel/BncSS/nCB Ili52 LABORATORY ANALYTICAL REPORT Prepared by Casper, WY Branch Client: Project: Lab ID: Denison Mines USA Corp 3rd Quarter Chloroform 2011 C 11080835-035 Client Sample ID: Temp Blank Analyses PHYSICAL PROPERTIES Temperature Report Definitions: Rl -Analyte reporting limit. QCl -Quality control limit. Result Units 2.8 Qualifier Rl Report Date: 09/06/11 Collection Date: 08/18/11 DateReceived: 08/19/11 Matrix: Aqueous MClI QCl Method Analysis Date 1 By E170.1 08/19/11 09 :20 1 kbh MCl -Maximum contaminant level. NO -Not detected at the reporting limit. Page 38 of 51 ----.::;==-= EI\ERGY LAB ORATORIES www.energylab.~om An,lyt/I:6/ Exc.IIB11csSliIc. /952 ....... -..... -... 1' -Billings. MT 800·735·4489 · Casper. WY 888-235-0515 CitY. SD .888-672"1225 -College Station. TX 888-690-2218 QA/Qe Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Project: 3rd Quarter Chloroform 2011 Analyte Count Result Units Method: A4500-CI B Sample 10: MBLK9-11/08/22 Chloride Sample 10: C11080835-008AMS Chloride Sample 10: C11080835-008AMSO Chloride Sample 10: LCS35-11/08/22 Chloride Method: A4500-CI B Sample 10: MBLK9-110825 Chloride Sample 10: C11080835-009AMS Chloride Sample 10: C11080835-009AMSO Chloride Sample 10: C11080835-028AMS Chloride Sample 10: C11080835-028AMSO Chloride Sample 10: LCS35-110825 Chloride Qualifiers: RL -Analyte reporting limit. Method Blank ND mg/L Sample Matrix Spike 68.3 mg/L Sample Matrix Spike Duplicate 68.3 mg/L Laboratory Control Sample 3560 mg/L Method Blank ND mg/L Sample Matrix Spike 221 mg/L Sample Matrix Spike Duplicate 221 mg/L Sample Matrix Spike 180 mg/L Sample Matrix Spike Duplicate 175 mg/L Laboratory Control Sample 3520 mg/L Report Date: 09/06/11 Work Order: C11080835 RL %REC Low Limit High Limit RPO RPOLimit Qual Batch: 11/08/22-CL-TTR-W Run: TITRATION_110822A 08/22/11 11 :10 0.5 Run: TITRATION_11 0822A 08/22/11 12:30 1.0 100 90 110 Run: TITRATION 110822A 08/22/11 12:32 1.0 100 90 110 0.0 10 Run: TITRATION_11 0822A 08/22/11 12 :35 1.0 100 90 110 Batch: 110825-CL-TTR-W Run: TITRATION_11 0825A 08/25/11 13:44 0.4 Run: TITRATION_11 0825A 08/25/11 15:30 1.0 101 90 110 Run: TITRATION_11 0825A 08/25/11 15:33 1.0 101 90 110 0.0 10 Run: TITRATION_11 0825A 08/25/11 16 :32 1.0 103 90 110 Run: TITRATION_11 0825A 08/25/11 16:34 1.0 99 90 110 2.6 10 Run: TITRATION 110825A 08/25/11 16:39 - 1.0 99 90 110 ND -Not detected at the reporting limit. Page 39 of 51 EN:RGY LABORATORIES www.energylab.~om Anllyt/CII/ Exes//snes Sine. 1952 IIUU··/3~1·44I,1S . Casper,WY 888·235·0515 225 • ColiegeSlalion, TX 888·690·2218 QA/Qe Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Report Date: 09/06/11 Project: 3rd Quarter Chloroform 2011 Work Order: C11080835 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: E353.2 Batch: R149648 Sample 10: MBLK·1 Method Blank Run: TECHNICON_110822A 08/22/11 12:18 Nitrogen, Nitrate+Nitrite as N ND mg/L 0.06 Sample 10: LCS·2 Laboratory Control Sample Run: TECHNICON_11 0822A 08/22/11 12:20 Nitrogen, Nitrate+Nitrite as N 2.49 mg/L 0.10 100 90 110 Sample 10: LFB·3 Laboratory Fortified Blank Run: TECHNICON_11 0822A 08/22/11 12 :23 Nitrogen, Nitrate+Nitrite as N 1.99 mg/L 0.10 102 90 110 Sample 10: C11080813·009EMS Sample Matrix Spike Run: TECHNICON_110822A 08/22/11 12:50 Nitrogen, Nitrate+Nitrite as N 2.03 mg/L 0.10 104 90 110 Sample 10: C11080813·009EMSO Sample Matrix Spike Duplicate Run: TECHNICON_11 0822A 08/22/11 12:53 Nitrogen, Nitrate+Nitrite as N 2.06 mg/L 0.10 105 90 110 1.5 10 Sample 10: C11080821·002FMS Sample Matrix Spike Run: TECHNICON_11 0822A 08/22/11 13:25 Nitrogen, Nitrate+Nitrite as N 2.10 mg/L 0.10 107 90 110 Sample 10: C11080821·002FMSO Sample Matrix Spike Duplicate Run: TECHNICON_11 0822A 08/22/11 13:28 Nitrogen, Nitrate+Nitrite as N 2.18 mg/L 0.10 111 90 110 3.7 10 S Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. S -Spike recovery outside of advisory limits. Page 40 of 51 EI\ERGY LAB ORATORIES www.energylab.com An.lylfc.l be,/I,nc, Sinel 1952 Heiena; Mf 877-412-0111 • Billings, MT 800-135-4489 · Casper, WY 888-235-0515 'l ,.~iI.ie~q,·WV :a66-686~1175 • Rapid City, SD 888-612-1225 • College Station, IX 888-690-2218 QA/Qe Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Report Date: 09/06/11 Project: 3rd Quarter Chloroform 2011 Work Order: C11080835 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R149732 Sample 10: 23-Aug-11_LCS_9 8 Laboratory Control Sample Run : GCMS2_11 0823A 08/23/11 14:41 Carbon tetrachloride 9.0 ug/L 1.0 90 70 130 Chloroform 8.9 ug/L 1.0 89 70 130 Chloromethane 8.9 ug/L 1.0 89 70 130 Methylene chloride 8.9 ug/L 1.0 89 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 96 80 120 Surr: Dibromofluoromethane 1.0 96 70 130 Surr: p-Bromofluorobenzene 1.0 111 80 130 Surr: Toluene-d8 1.0 93 80 120 Sample 10: 23-Aug-11_MBLK_11 8 Method Blank Run: GCMS2_11 0823A 08/23/11 15 :51 Carbon tetrachloride ND ug/L 1.0 Chloroform ND ug/L 1.0 Chloromethane ND ug/L 1.0 Methylene chloride ND ug/L 1.0 Surr: 1,2-Dichlorobenzene-d4 1.0 106 80 120 Surr: Dibromofluoromethane 1.0 95 70 130 Surr: p-Bromofluorobenzene 1.0 120 80 120 Surr: Toluene-d8 1.0 89 80 120 Sample 10: C11080835-001CMS 8 Sample Matrix Spike Run: GCMS2_11 0823A 08/23/11 22:13 Carbon tetrachloride 200 ug/L 10 102 70 130 Chloroform 200 ug/L 10 102 70 130 Chloromethane 180 ug/L 10 91 70 130 Methylene chloride 200 ug/L 10 98 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 92 80 120 Surr: Dibromofluoromethane 1.0 111 70 130 Surr: p-Bromofluorobenzene 1.0 107 80 120 Surr: Toluene-d8 1.0 92 80 120 Sample 10: C11080835-001CMSO 8 Sample Matrix Spike Duplicate Run: GCMS2_11 0823A 08/23/11 22:48 Carbon tetrachloride 190 ug/L 10 97 70 130 5.6 20 Chloroform 200 ug/L 10 98 70 130 4.8 20 Chloromethane 190 ug/L 10 94 70 130 2.6 20 Methylene chloride 190 ug/L 10 96 70 130 2.5 20 Surr: 1,2-Dichlorobenzene-d4 1.0 94 80 120 0.0 10 Surr: Dibromofluoromethane 1.0 105 70 130 0.0 10 Surr: p-Bromofluorobenzene 1.0 106 80 120 0.0 10 Surr: Toluene-d8 1.0 91 80 120 0.0 10 Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. Page 41 of 51 www.energylab.com An.lytful ExCSl/lnCl Sinc1I1952 ,j.:!,,,.. I "' • .' , -', , ' .. • , i;Hel~~~; ~T 871-472-0711 • Billings, MT 800-735-4489 · Casper, WY 888-235-0515 , j f~~e,'wYB66'~$86-~J 75 • Rapid City, SO 888-672-1225 • College Station, TX 888-6~D-221 8 EN:RGY LABORAT ORIES QA/Qe Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Report Date: 09/06/11 Project: 3rd Quarter Chloroform 2011 Work Order: C11080835 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R149789 Sample 10: 082411_LCS_3 8 Laboratory Control Sample Run: SATURNCA_11 0824B 08/24/11 11 :31 Carbon tetrachloride 10 ug/L 1.0 104 70 130 Chloroform 11 ug/L 1.0 106 70 130 Chloromethane 10 ug/L 1.0 101 70 130 Methylene chloride 9.9 ug/L 1.0 99 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 100 80 120 Surr: Dibromofluoromethane 1.0 98 70 130 Surr: p-Bromofluorobenzene 1.0 95 80 130 Surr: Toluene-d8 1.0 86 80 120 Sample 10: 082411_MBLK_5 8 Method Blank Run: SATURNCA_11 0824B 08/24/11 12:45 Carbon tetrachloride NO ug/L 1.0 Chloroform NO ug/L 1.0 Chloromethane NO ug/L 1.0 Methylene chloride NO ug/L 1.0 Surr: 1,2-Dichlorobenzene-d4 1.0 96 80 120 Surr: Dibromofluoromethane 1.0 100 70 130 Surr: p-Bromofluorobenzene 1.0 90 80 120 Surr: Toluene-d8 1.0 88 80 120 Sample 10: C11080571-011GMS 8 Sample Matrix Spike Run: SATURNCA_ 110824B 08/24/11 19 :26 Carbon tetrachloride 230 ug/L 10 116 70 130 Chloroform 230 ug/L 10 116 70 130 Chloromethane 220 ug/L 10 108 70 130 Methylene chloride 230 ug/L 10 114 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 103 80 120 Surr: Dibromofluoromethane 1.0 104 70 130 Surr: p-Bromofluorobenzene 1.0 104 80 120 Surr: Toluene-d8 1.0 95 80 120 Sample 10: C11080571-011GMSO 8 Sample Matrix Spike Duplicate Run : SATURNCA_ 110824B 08/24/11 20:02 Carbon tetrachloride 240 ug/L 10 118 70 130 1.4 20 Chloroform 240 ug/L 10 118 70 130 2.1 20 Chloromethane 230 ug/L 10 113 70 130 4.7 20 Methylene chloride 230 ug/L 10 116 70 130 2.4 20 Surr: 1,2-Dichlorobenzene-d4 1.0 100 80 120 0.0 10 Surr: Dibromofluoromethane 1.0 102 70 130 0.0 10 Surr: p-Bromofluorobenzene 1.0 100 80 120 0.0 10 Surr: Toluene-d8 1.0 92 80 120 0.0 10 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. Page 42 of 51 EN:RGY LAB ORAT ORIES www.energylab.com An,lytlClI £XCll/snC. SIne, 1952 ii" :«~I~"a .. MT &17-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-23$-0515 IU •. .\,', , ,.' . .,' . 11, Jlilletle, Wv q~6:686-717~ • Rapid City, SD,888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Report Date: 09/06/11 Project: 3rd Quarter Chloroform 2011 Work Order: C11080835 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R149846 Sample 10: 082511_LCS_3 8 Laboratory Control Sample Run: SATURNCA_110825B 08/25/11 13:17 Carbon tetrachloride 11 ug/L 1.0 106 70 130 Chloroform 11 ug/L 1.0 112 70 130 Chloromethane 9.0 ug/L 1.0 90 70 130 Methylene chloride 11 ug/L 1.0 112 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 102 80 120 Surr: Dibromofluoromethane 1.0 105 70 130 Surr: p-Bromofluorobenzene 1.0 97 80 130 Surr: Toluene-d8 1.0 91 80 120 Sample 10: 082511_MBLK_5 8 Method Blank Run: SATURNCA_ 110825B 08/25/11 14:32 Carbon tetrachloride ND ug/L 1.0 Chloroform ND ug/L 1.0 Chloromethane ND ug/L 1.0 Methylene chloride ND ug/L 1.0 Surr: 1,2-Dichlorobenzene-d4 1.0 102 80 120 Surr: Dibromofluoromethane 1.0 101 70 130 Surr: p-Bromofluorobenzene 1.0 93 80 120 Surr: Toluene-d8 1.0 90 80 120 Sample 10: C11080813-010JMS 8 Sample Matrix Spike Run: SATURNCA_ 110825B 08/25/11 21 :17 Carbon tetrachloride 240 ug/L 10 121 70 130 Chloroform 250 ug/L 10 127 70 130 Chloromethane 230 ug/L 10 117 70 130 Methylene chloride 240 ug/L 10 121 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 102 80 120 Surr: Dibromofluoromethane 1.0 110 70 130 Surr: p-Bromofluorobenzene 1.0 103 80 120 Surr: Toluene-d8 1.0 91 80 120 Sample 10: C11080813-010JMSO 8 Sample Matrix Spike Duplicate Run : SATURNCA_11 0825B 08/25/11 21 :53 Carbon tetrachloride 250 ug/L 10 123 70 130 2.0 20 Chloroform 250 ug/L 10 124 70 130 2.2 20 Chloromethane 240 ug/L 10 119 70 130 1.7 20 Methylene chloride 250 ug/L 10 124 70 130 2.3 20 Surr: 1,2-Dichlorobenzene-d4 1.0 100 80 120 0.0 10 Surr: Dibromofluoromethane 1.0 110 70 130 0.0 10 Surr: p-Bromofluorobenzene 1.0 100 80 120 0.0 10 Surr: Toluene-d8 1.0 88 80 120 0.0 10 Qualifiers: RL -Analyte reporting limit. ND -Not detected at the reporting limit. Page 43 of 51 EI\ERGY LAB ORAT ORIES wWw.energylab.~om An'~1 Exeel/ene. Sine. 1852 .~ , ;Ilef~na; MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 J;iII~iie,.WY 8&6-686-7175 • Rapid City, 51) 888-672-1225 • College Station, TX 888-690-2218 QA/QC Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Report Date: 09/06/11 Project: 3rd Quarter Chloroform 2011 Work Order: C11080835 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SW8260B Batch: R149885 Sample 10: 26-Aug-11_LCS_3 8 Laboratory Control Sample Run: GCMS2_110826A 08/26/11 11 :27 Carbon tetrachloride 10 ug/L 1.0 103 70 130 Chloroform 10 ug/L 1.0 100 70 130 Chloromethane 9.8 ug/L 1.0 98 70 130 Methylene chloride 11 ug/L 1.0 106 70 130 Surr: 1,2-0ichlorobenzene-d4 1.0 93 80 120 Surr: Oibromofluoromethane 1.0 101 70 130 Surr: p-Bromofluorobenzene 1.0 102 80 130 Surr: Toluene-d8 1.0 92 80 120 Sample 10: 26-Aug-11_MBLK_5 8 Method Blank Run: GCMS2_11 0826A 08/26/11 12:36 Carbon tetrachloride NO ug/L 1.0 Chloroform NO ug/L 1.0 Chloromethane NO ug/L 1.0 Methylene chloride NO ug/L 1.0 Surr: 1,2-0ichlorobenzene-d4 1.0 104 80 120 Surr: Dibromofluoromethane 1.0 94 70 130 Surr: p-Bromofluorobenzene 1.0 109 80 120 Surr: Toluene-d8 1.0 90 80 120 Sample 10: C11080835-028CMS 8 Sample Matrix Spike Run: GCMS2_110826A 08/26/11 18:57 Carbon tetrachloride 1900 ug/L 100 94 70 130 Chloroform 2800 ug/L 100 102 70 130 Chloromethane 1800 ug/L 100 91 70 130 Methylene chloride 2200 ug/L 100 110 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 92 80 120 Surr: Oibromofluoromethane 1.0 111 70 130 Surr: p-Bromofluorobenzene 1.0 96 80 120 Surr: Toluene-d8 1.0 95 80 120 Sample 10: C11080835-028CMSO 8 Sample Matrix Spike Duplicate Run: GCMS2_ 110826A 08/26/11 19:32 Carbon tetrachloride 1700 ug/L 100 84 70 130 11 20 Chloroform 2500 ug/L 100 87 70 130 11 20 Chloromethane 1800 ug/L 100 88 70 130 3.1 20 Methylene chloride 1900 ug/L 100 95 70 130 14 20 Surr: 1,2-Dichlorobenzene-d4 1.0 92 80 120 0.0 10 Surr: Dibromofluoromethane 1.0 98 70 130 0.0 10 Surr: p-Bromofluorobenzene 1.0 94 80 120 0.0 10 Surr: Toluene-d8 1.0 94 80 120 0.0 10 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. Page 44 of 51 EI\ERGY LAB ORATORIE S www.energylab.~om An./ytlclf ExCIl/snC' Sine, IgS2 . ' . .' ,Heiima,.MT 877-472-0711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 ;.1 ,!iiIlMkwv ·~B&768~-7115' .. Rap'ld City, SD.8Q8-672-1225 .. College Station, IX 888-690-2218 QA/Qe Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Report Date: 09/06/11 Project: 3rd Quarter Chloroform 2011 Work Order: C11080835 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimlt Qual Method: SW8260B Batch: R149888 Sample 10: 082611_LCS_ 4 8 Laboratory Control Sample Run: SATURNCA_110826C 08/26/11 12:10 Carbon tetrachloride 9.4 ug/L 1.0 94 70 130 Chloroform 9.0 ug/L 1.0 90 70 130 Chloromethane 8.3 ug/L 1.0 83 70 130 Methylene chloride 8.4 ug/L 1.0 84 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 97 80 120 Surr: Dibromofluoromethane 1.0 94 70 130 Surr: p-Bromofluorobenzene 1.0 98 80 130 Surr: Toluene-d8 1.0 95 80 120 Sample 10: 082611_MBLK_6 8 Method Blank Run: SATURNCA_110826C 08/26/11 13:22 Carbon tetrachloride NO ug/L 1.0 Chloroform NO ug/L 1.0 Chloromethane NO ug/L 1.0 Methylene chloride NO ug/L 1.0 Surr: 1,2-Dichlorobenzene-d4 1.0 99 80 120 Surr: Dibromofluoromethane 1.0 101 70 130 Surr: p-Bromofluorobenzene 1.0 92 80 120 Surr: Toluene-d8 1.0 86 80 120 Sample 10: C11080835-027CMS 8 Sample Matrix Spike Run: SATURNCA_11 0826C 08/27/11 06:18 Carbon tetrachloride 2100 ug/L 100 104 70 130 Chloroform 3700 ug/L 100 112 70 130 Chloromethane 1800 ug/L 100 90 70 130 Methylene chloride 2000 ug/L 100 100 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 96 80 120 Surr: Dibromofluoromethane 1.0 103 70 130 Surr: p-Bromofluorobenzene 1.0 93 80 120 Surr: Toluene-d8 1.0 87 80 120 Sample 10: C11080835-027CMSO 8 Sample Matrix Spike Duplicate Run: SATURNCA_ 110826C 08/27/11 06 :54 Carbon tetrachloride 2000 ug/L 100 102 70 130 2.3 20 Chloroform 3500 ug/L 100 100 70 130 6.5 20 Chloromethane 1700 ug/L 100 85 70 130 5.5 20 Methylene chloride 1900 ug/L 100 94 70 130 7.0 20 Surr: 1,2-Dichlorobenzene-d4 1.0 98 80 120 0.0 10 Surr: Dibromofluoromethane 1.0 102 70 130 0.0 10 Surr: p-Bromofluorobenzene 1.0 93 80 120 0.0 10 Surr: Toluene-d8 1.0 86 80 120 0.0 10 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. Page 45 of 51 EN:RGY LAB ORATORIES www.energylab.com An.lytlllll ExcIl/lnc, Slnel 7152 <.We~a, M,TB77-4i2-Q711 • Billings, MT 800-735-4489 · Casper, WY 888-235-0515 ~~ __ ~1),1ette,iWXJi6-$B6-7115 . Rapid City, SD 888-672-1225 . ColiegeStalion, TX 888-690-2218 QA/Qe Summary Report Prepared by Casper, WY Branch Client: Denison Mines USA Corp Report Date: 09/06/11 Project: 3rd Quarter Chloroform 2011 Work Order: C11080835 Analyte Count Result Units RL %REC Low Limit High Limit RPO RPOLimit Qual Method: SWB260B Batch: R149911 Sample 10: OB2711_LCS_ 4 7 Laboratory Control Sample Run: SATURNCA_11 0827C 08/27/11 13:57 Carbon tetrachloride 11 ug/L 1.0 105 70 130 Chloromethane 8.9 ug/L 1.0 89 70 130 Methylene chloride 9.6 ug/L 1.0 96 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 101 80 120 Surr: Dibromofluoromethane 1.0 98 70 130 Surr: p-Bromofluorobenzene 1.0 101 80 130 Surr: Toluene-d8 1.0 93 80 120 Sample 10: OB2711_MBLK_6 7 Method Blank Run: SATURNCA_11 0827C 08/27/11 15 :09 Carbon tetrachloride NO ug/L 1.0 Chloromethane NO ug/L 1.0 Methylene chloride NO ug/L 1.0 Surr: 1,2-Dichlorobenzene-d4 1.0 98 80 120 Surr: Dibromofluoromethane 1.0 99 70 130 Surr: p-Bromofluorobenzene 1.0 94 80 120 Surr: Toluene-d8 1.0 90 80 120 Sample 10: C110BOB35-031CMS 7 Sample Matrix Spike Run: SATURNCA_ 110827C 08/27/1121:12 Carbon tetrachloride 22000 ug/L 1000 108 70 130 Chloromethane 18000 ug/L 1000 90 70 130 Methylene chloride 20000 ug/L 1000 102 70 130 Surr: 1,2-Dichlorobenzene-d4 1.0 94 80 120 Surr: Dibromofluoromethane 1.0 100 70 130 Surr: p-Bromofluorobenzene 1.0 96 80 120 Surr: Toluene-d8 1.0 89 80 120 Sample 10: C110BOB35-031CMSO 7 Sample Matrix Spike Duplicate Run: SATURNCA_ 110827C 08/27/11 21 :48 Carbon tetrachloride 21000 ug/L 1000 105 70 130 2.3 20 Chloromethane 17000 ug/L 1000 87 70 130 3.6 20 Methylene chloride 19000 ug/L 1000 97 70 130 5.2 20 Surr: 1,2-Dichlorobenzene-d4 1.0 100 80 120 0.0 10 Surr: Dibromofluoromethane 1.0 97 70 130 0.0 10 Surr: p-Bromofluorobenzene 1.0 98 80 120 0.0 10 Surr: T oluene-d8 1.0 90 80 120 0.0 10 Qualifiers: RL -Analyte reporting limit. NO -Not detected at the reporting limit. Page 46 of 51 :Helena, M(877.472-p711 • Billings, MT 800-735-4489 • Casper, WY 888-235-0515 :'. • :' •. j" • .• ~1II~~8, WY'8~67686~m5 · Rapid City, SO.888-672-1225 • College Station, 1X 888-6~0-221 8 www.energylab.com Anllytftml £Xcsl/BllCI Sines 1852 EN:RGY LABOF~Al Or~1 ES Workorder Receipt Checklist Denison Mines USA Corp 111111111111111111111111111111111111111111111111111111I C11080835 Login completed by: Debra Williams Reviewed by: BL2000\kschroeder Reviewed Date: 8/19/2011 Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? ContainerfTemp Blank temperature: Water -VOA vials have zero headspace? Water -pH acceptable upon receipt? Contact and Corrective Action Comments : None Yes 0 Yes 0 Yes D Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 Yes 0 2.8"(; On Ice Yes 0 Yes 0 Date Received: 8/19/2011 Received by: kg Carrier FedEx name: No 0 No 0 No 0 No 0 No 0 NoD No 0 No 0 No 0 No 0 No 0 No 0 Not Present 0 Not Present 0 Not Present 0 No VOA vials submitted 0 Not Applicable 0 Page 47 of 51 Chain of Custody and Analytical Request Record Page-.Lof~ LA BORA TORIES PLEASE PRINT (Provide as much information as possible.) Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPNState Compliance: D .u'I;~C(\ Mh,~ :~tcA Qu.o.rW c. h lo(ot¢rl"'l ;to It State: lAT Yes I)J No 0 Report Mail Address: p Contact Name: PhonefFax: Email: Sampler: (Please Print) o BO)< goq ~nner ij~iI;JAtt ~j Q,n a; I"IJ;.\ \AT ~45\1 R,,\o.t\ Po,J 1'¥Ie.(" \.13~ ('78 .:o.:l..\ Invoice AddresS" Invoice Contact & Phone: Purchase Order: QuotelBottle Order: 'scAM(' ~4mc: Special ReporVFormats: ~ W&iD&i OO[§®QD~IID • Contact ELI prior to ~hlpped by: $: RUSH sample submittal FE-Ext' ° ID ~Otl)= t=' R for charges and Cooler lO(s): ~ ~1Il;gOI ID \.fl 0 ~ scheduling -See (. J.. i'l f~~ ~ ._> 0 >-ro LU I nstruction Page Dow o EDD/EDT(Electronic Data) ~en~~$: o~= ~ 0) ~ :r: "0 Receipt T em p 13' '\'n" DpOTWNVWTP () c: Comments: Format: ~c:(a31.2 ~ ~ U o ~[()I c:: ci « e :1. ~ °C o State: o LEVEL IV "-Qj~ C::"i:: J I-(1l ~a.(1llgo l-e o Other: o NELAC E~(1l ' « :; On Ice: (YN ~ IV·: Q) :s: ::tt t-5 zCic:(I5r0 LU "2 . Custody Sear !il >1 .~ UJ ro On Bottle Y N (f) "0 @N en c: On Cooler <) ctr ~N -:S -H Intact CI) SAMPLE IDENTIFICATION Collection Collection MATRIX a Signature @ N (Name, Location, Interval, etc.) Date TIme Match 1 TWi.\-"3 K ~115lH Ob~ 54\>.) 1-~ 2 -rWl.\ -;2.\i R ~/lb/H "O~O 5~w y. !~ 3 "TW 1.\-7 R ~/l1111 Ogq,( 5-W 'f. i 4 IvJ~-3 is' /l'-/ll 144~ S-w "X 51W4~ \2 ,glIb/it 1~L1:S S .. \J != Y.. ~ 61""w4,.. i3 I K/HJ II l3S1 :5--.,.1 Y.. I~ 7 iwl.{ -14 I VoJlbl It \t10~ .5-itJ .'X ~ I~ BMW -S;t. 8f1b/1l l.1~ 5-'N 'I.. If-~ -, I C5dJ. ~ 9 "Tv.t4 -:l3 K /''''1\ \~15 ~-w 'f. I~ I~ 1°TW4_~ Z/I"/li I.2SfS _5.-w y. It::::!. Custody ~n;~s: bU:\I',llAd fl.fl~i:;~:l \I~C ~ LJ4NX.Siwp~ Received by (print): DatefTime: Signature: Record Relinquished by (print): ,.J DatefTime: Signature: ./" Received by (print): DatefTime: Signature: MUST be Signed RCflIvea oY;ADoralOry: Ualet 'me: qt~ ;:r.a ure: Sample Disposal: Return to Client: Lab Disposal: f, ',:j C.Sf"z "1-)ti!{~ Lf .:;......L.- In certain circumstances. samples submitted to Energy Laboratories. Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information. downloadable fee schedule, forms, and links. "U m co CD .~ o .-' <Jl ....... .. Chain of Custody and Analytical Request Record Page~of --.!:L PLEASE PRINT (Provide as much information as possible.) Company Name: M~f\e.~ Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: De.tlI~C(\ :r~ ~U!>.J1-d"" Chi oratolrYl .:t~ t, State: \.AT Yes ~ No 0 Report Mail Address: Po Bel( 80'1 Contact Name: Phone/Fax: Email: Sampler: (Please Print) B L"na 'I tI G\ v.T gt-!'S\! Rt\A.r\ PaJrnu-11~ b78~1 '1:'.nner Jto}/,d"t' Invoice Address~ Invoice Contact & Phone: Purchase Order: QuotelBottle Order: ~O\t\'\C ..s"m~ Special Report/Formats: ~&[1 W@O® [M@:®QD~@ .. Contact ELI prior to ffdbY: ~ ~ RUSH sample submittal -6t 0 :v ~om= ~ for charges and Cooler 10(5): [g III ;g 01 :v l-l1 0 « R scheduling -See [li~J ._> 0 >-Ci5 W t:. Instruction Page Dow o EDO/EDT(Electronic Data) ~U)U) ro s: r-c: Us en I o~= gj OJ ct "0 Receipt Temp D POTWIWWTP Format: u 0 o.~ 0 c Comments: .... <::U)liill~ :J U ,-"8 o State: o LEVEL IV o ... c -..) ~ e °c ..... Qj oS J::-1:: ca ~~l~~ ~ t: o Other: o NELAC ~ ... On Ice: ~N « :J :J \1).= iii s: ~ 5 za.<::Ig>O 1 W 'E Custody Seal fij >1 W ca On Bottle Y N C/) "0 g: CJ) t: On Cooler m <3 U5 H Intact SAMPLE IDENTIFICATION Collection Collection MATRIX Signature ON (Name, Location, Interval, etc.) Date Time Match 1 TW1.\·. g g/l~1 \I 'L1~O s· 'vJ I~ ~ 2 T w 4 ... Q K/lb/ )( )4.2\ ;-'W 't. ~ 3 TWU.-6~ ~/I"/11 1 ~1~ s.,·~W 'X 1lQ) Iflnn 4 1W4-;1..4 8/111\1 C~ S~W 'f.. ~ 5 Tw4. -:tb ~1I1/11 D~"35 );-\eJ 'I... i'= ~ 5 TWi.\-S Ig/n/II Db"'\b S-w 'I. ~- 7IW~-G, ~/1i/1I Ob~!:> Y;,-w I}( ~ B TWl.l-\b %/1, III 07()S 5-W y.. ~ 9-rWi..\-\15 g/ll/U 07;2.\ b--W y.. ! -l/tXD~~ ~ IOTW~_Xl Ml1/U 01'3'5 5 ... vJ }. ~ Custody Relinquished by (print): Datemme: ~Uftr1J)::.n1l~~ Received by (print): Datemme: Signature: I&V\J\r:.r ~oJl:~14 gllg/..acll li'~O Record Relinquished by (print): ~ Date/Time: Signature: ...-Received by (print): Datemme: Signature: MUST be Signed ~i?;yea Dy ~DOrawry: uatel Ime: 'f: ;)0 :la u~: ~ Sample Disposal: Return to Client: Lab Disposal: i l ; .:»< f··;</-IJ In certain circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certrried laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub·contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. "'U OJ (Q CI> (}1 o o ....., (}1 IIIIiII Chain of Custody and Analytical Request Record Page~of~ PLEASE PRINT (Provide as much information as possible.) Company Name: Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: DenlsO(\ "A',(\~S ?{~ Qv...o..'~(, Ghloro,fciM ~Oll State: ucr Yes Il:l No 0 Report Mail Address: fO Bo'')( gD~ Contact Name: Phone/Fax: Email: Sampler: (Please Print) BIW\J..~1\\ \.C\ )5'1t)l\ "R ~ AA 1',:\.\ 1\"1 ~(" l1~!) b7~ .:z;Q\ ~nner ~cj/;J",*" Invoice Address: Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: S",",,-c.. Sc:...M&e. Special Report/Formats: &[Wl\[1 Yi'@O@ ~@:®@~m@) • Contact ELI prior to ~nipped by: :;: RUSH sample submittal LE-£.o 0 Q; "'0 <f)oC. ~ for charges and Cooler !D(s}: I ~co;gOI Q; ...c'l 0 « R scheduling -See C!·~J ._> 0 >.~ W t:.. Instruction Page Dow D EDD/EOT(Electronic Data) j!lCl,)CI,) ctI:;: C ~<f) r I 0:;:= ~ OJ '0 Receipt Temp D POTWMlWTP a-U e Comments: Format: u<c~I.Q~ C'{ :J U ;)/j '0 .... COI c: « 0 °C D State: o LEVEL IV '-Gi$ ~.~ <J I-m ~ o..ctI.QD l-e o Other: o NELAC ~Iro ' ... On Ice: (!)N « :J :J (I).: (j):;: ~ ~ 5 zo..<Cl~o W 'E Custody Seal E >1 ~ W (tI On Bottle <1~ rn (f) '0 CI,) 0 c:: On Cooler ~ S H Intact ~N 0 CJ) SAMPLE IDENTIFICATION Collection Collection MATRIX Signature G H (Name, Location, Interval, etc.) Date Time Match 1 tWI-\ -lO ~/11111 Oil..\S -S ... W "i. ~ 2 T'Ni..\-2..\ ~/\i/1l CiS!) ~-W '{. I~ 3 _TW~-' \ ~/17/l\ 0307 E,-vJ '!. Itg Iln.n 4-rWL\-'7 g/Ig/Ii Cb3b ~-W Y. ~ 5\'"W!.\_ 1 WIK/\1 0641 ~-vJ 't ."-= ~ 6 MW-'i g/i1JI\ t~05 5-W 'f. ~ 7 \W L.\ -'-\ 3/nl\1 ,~\.5 :!;-w " .~ a -r'W i..\ -\~ g/ll!l \ l~50 £-w Y. ~ -Itrfx(i(l;J ..... 9 TW~-:l. _[/I~/li ObS, -S-w 'i. ao v ~ 1°TWq _1q gIn/ii )/..\00 ~-W y.. <:::o! Custody ~linqUiShed by (print): ~Ofgti;:~~l "3u ~,,"m.~ SitJ';~L, Received by (print): DatefTime: Signature: f~t'\e.r t\d\.J.,,~ Record Relinquished by (print): ....J DatefTime: Signature: '-' Received by (print): DatelTime: Signature: MUST be Signed R,eo;elvea DJ( .. agora ory: ]:latE!! ,me: 1'(~ ~'gnature: k Sample Disposal: Return to Client: Lab Disposal: Jt:5 ~.5x_ '(-i~-I( x.~ In certain Circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sub-contract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. IIlIIII Chain of Custody and Analytical Request Record Pagel of$- PLEASE PRINT (Provide as much information as possible.) Company Name: , M:t\6 Project Name, PWS, Permit, Etc. Sample Origin EPA/State Compliance: D~nl~on 1:rd. Qv .. c~rh:r Chl or~f'()r1t'l G..Ol\ State: Yes ~ No 0 Report Mail Address: PC) Bey.. g'D<\ Contact Name: Phone/Fax: Email: Sampler: (Please Print) f.:> "tC"'(It'\"\. \,\\ 8't45)1 R .... "\~1'l 1/ oJ yYl-er L.t35 bif1 ~l -re::nner ~o 11 ,-J4Y Invoice Address: -Invoice Contact & Phone: Purchase Order: Quote/Bottle Order: . S~fVlt:: 5~mz: Special Report/Formats: &[J:!]8[b W®D@ OO~@l!DI]@lj'~[ID .. Contact ELI prior to Shipped by: 5: Fr.-6x' 0 :u RUSH sample submittal "'0 00 -,= for charges and Cooler 10(s): ~cc;gOI :u ~ R 0 « scheduling -See (lUll .-> 0>.(6 lJ) W C Instruction Page Dow o EOO/EOT(Electronic Data) .c;! CI) CI) (1)?; c Cis tI) T-:c O?;= Kl 0> "0 ReceiptTemp D POTWflNWTP u °0C: ~ C) e Comments: Format: .... <C Cl)lccl :";;:: :I U ? '9 o State: o LEVEL IV ° ~ c: « e °c "-Q)~ t::'~ V I-ro 1l Cl..(1) 00 l-e (jN o Other: o NELAC "-On Ice: E~I'S ' ~ « :I :I Q).= CD ?; l-S zo.«l~o ~ W "E Custody Seal ~ >1 W (1) On Bottle &: (f) "0 CI) C On Cooler d ~ H Intact ~N SAMPLE IDENTIFICATION Collection Collection MATRIX Signature G)N (Name, Location, Interval. etc.) Date Time Match 1 "f vJ 1..\ -;;to g/r111~ \;t4D ~-w ). ~ 2 Tw~-be gIn/a \~\~O S-w '" ~ 3 IW i..\-70 g/l1/11 0705 l;-W X g nnl 4 trio Bto..nk. roof;! 81\~/t\ ~ 5 1 ~ 6 ~ 7 I~ 8 I~ } -/ ( OI-og-3 D 9 I~ 10 I<:::::!J Custody --r;~S:;'b"~\tr:!tl~ 8';'K/:;~~l 1130 :::JaJl :~g:tu1t,~I.;/--A Received by (print): DatelTime: Signature: Record Relinquished by (print):...,J DatefTime: Signatu\'e: J Received by (print): Date/Time: Signature: MUST be Signed r<;JJ'¥ved Dy LaD!'ralOg: Uatel~lme: lIdo %;::e:LL Sample Disposal: Return to Client: LabDi~sal: r.:c. 6·5 ( ~_If~ II - In certain Circumstances, samples submitted to Energy Laboratories, Inc. may be subcontracted to other certified laboratories in order to complete the analysis requested. This serves as notice of this possibility. All sutH:ontract data will be clearly notated on your analytical report. Visit our web site at www.energylab.com for additional information, downloadable fee schedule, forms, and links. www.energylab.com E~RGY LAB ORATORIES An.lytfcsl £XcII/Inc. Slnc. 11i52 '~'~,,,,',; ":,~ei~na,,MT 817-472-0711 • Billings, MT 800-735-4489 . Casper, WY 888-235-0515 :Grll~~e/WY:8l6~$8~·m5 • Rap.id Ci~, SO 888-672-1225 • College,Station, TX 888-690-2218 September 06,2011 Denison Mines USA Corp 6425 S Hwy 191 Blanding, UT 84511 Workorder No.: C11080835 ANAL VTICAL SUMMARY REPORT Quote 10: C2975 -Chloroform Sampling Project Name: 3rd Quarter Chloroform 2011 Energy Laboratories, Inc. Casper WY received the following 35 samples for Denison Mines USA Corp on 8/19/2011 for analysis. Sample 10 Client Sample 10 Collect Date Receive Date Matrix Test C11080835-001 TW4-3R 08/15/11 6:45 08/19/11 Aqueous Chloride Nitrogen, Nitrate + Nitrite SW8260B VOCs, Standard List C 11080835-002 TW4-24R 08/16/11 6:40 08/19/11 Aqueous Same As Above C11080835-003 TW4-7R 08/17/11 8:49 08/19/11 Aqueous Same As Above C11080835-004 TW4-3 08/16/11 14:40 08/19/11 Aqueous Same As Above C11080835-005 TW4-12 08/16/11 13 :45 08/19/11 Aqueous Same As Above C11080835-006 TW4-13 08/16/11 13 :51 08/19/11 Aqueous Same As Above C11080835-007 TW4-14 08/16/11 14:03 08/19/11 Aqueous Same As Above C11080835-008 MW-32 08/16/11 12:55 08/19/11 Aqueous Same As Above C11080835-009 TW4-23 08/16/11 13:15 08/19/11 Aqueous Same As Above C11 080835-01 0 TW4-25 08/16/11 12:58 08/19/11 Aqueous Same As Above C11080835-011 TW4-8 08/16/11 14:50 08/19/11 Aqueous Same As Above C11080835-012 TW4-9 08/16/11 14:21 08/19/11 Aqueous Same As Above C11080835-013 TW4-65 08/16/11 13:15 08/19/11 Aqueous Same As Above C11080835-014 TW4-24 08/17/11 6:25 08/19/11 Aqueous Same As Above C 11 080835-01 5 TW4-26 08/17/11 6:35 08/19/11 Aqueous Same As Above C11080835-016 TW4-5 08/17/11 6:45 08/19/11 Aqueous Same As Above C 11 080835-01 7 TW4-6 08/17/11 6:55 08/19/11 Aqueous Same As Above C 11 080835-01 8 TW4-16 08/17/11 7:05 08/19/11 Aqueous Same As Above C 11 080835-01 9 TW4-18 08/17/117:21 08/19/11 Aqueous Same As Above C11080835-020 TW4-22 08/17/11 7:35 08/19/11 Aqueous Same As Above C11080835-021 TW4-10 08/17/11 7:45 08/19/11 Aqueous Same As Above C11080835-022 TW4-21 08/17/11 7:55 08/19/11 Aqueous Same As Above C11080835-023 TW4-11 08/17/11 8:07 08/19/11 Aqueous Same As Above C11080835-024 TW4-7 08/18/11 6 :36 08/19/11 Aqueous Same As Above C11080835-025 TW4-1 08/18/11 6:47 08/19/11 Aqueous Same As Above C11080835-026 MW-4 08/17/11 13:05 08/19/11 Aqueous Same As Above C11080835-027 TW4-4 08/17/11 13:1508/19/11 Aqueous Same As Above Page 1 of 51 EN:RGY LABORATO,~I ES C11080835-028 C11080835-029 C11080835-030 C11080835-031 C11080835-032 C11080835-033 C11080835-034 C11080835-035 wWw.energylab.com An.lytfcal £XciiI/Inc, Slncs Ig52 . 'L,> tHel~na/Mt8j7-412-0711 • Billings, MT 800-735-4489 . Casper, W'f 888-235-0515 AiIlBtl~;Wt ~8$~\G.86'-7J J~'. Rapid City, SO ,886-672-1225 • College Station, lX 888·6~O-2218 ANALYTICAL SUMMARY REPORT TW4-15 08/17/11 12 :50 08/19/11 Aqueous Same As Above TW4-2 08/17/11 6:57 08/19/11 Aqueous Same As Above TW4-19 08/17/11 14:00 08/19/11 Aqueous Same As Above TW4-20 08/17/11 12:40 08/19/11 Aqueous Same As Above TW4-60 08/17/11 14 :30 08/19/11 Aqueous Same As Above TW4-70 08/17/11 7:05 08/19/11 Aqueous Same As Above Trip Blank 6092 08/15/11 0:00 08/19/11 Aqueous SW8260B VOCs, Standard List Temp Blank 08/18/11 0:00 08/1 9/11 Aqueous Temperature This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601 . Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. All samples are reported on an as received basis unless otherwise indicated. Samples corrected for dry weight indicate units that have -dry appended. If you have any questions regarding these test results, please call. Report Approved By: cS¥~ D LJcJ.~ Reporting Supervisor Digitally signed by Stephanie Waldrop Date: 2011 .09.06 11 :23:35 ·06:00 Page 2 of 51 www.energyJab.com Ans/ytfClI ExCill/lncs SlnCil 1952 'hei~na .. MJB1J.472·0711 • Billings, MT 800·735-4489 · Casper, WY 88~·23~-D515 Gillette WY86S-'686-7fi5 • Raid Ci ,SO 888-672-1225 • Colle e station IX 888-690-2218 CLIENT: Denison Mines USA Corp Project: 3rd Quarter Chloroform 2011 Report Date: 09/06/11 Sample Delivery Group: C11080835 CASE NARRATIVE ORIGINAL SAMPLE SUBMITTAL(S) All original sample submittals have been returned with the data package. SAMPLE TEMPERATURE COMPLIANCE: 4"C (±2"C) Temperature of samples received may not be considered properly preserved by accepted standards. Samples that are hand delivered immediately after collection shall be considered acceptable if there is evidence that the chilling process has begun. GROSS ALPHA ANALYSIS Method 900.0 for gross alpha and gross beta is intended as a drinking water method for low TDS waters. Data provided by this method for non potable waters should be viewed as inconsistent. RADON IN AIR ANALYSIS The desired exposure time is 48 hours (2 days). The time delay in returning the canister to the laboratory for processing should be as short as possible to avoid excessive decay, Maximum recommended delay between end of exposure to beginning of counting should not exceed 8 days. SOIL/SOLID SAMPLES All samples reported on an as received basis unless otherwise indicated. ATRAZINE, SIMAZINE AND PCB ANALYSIS Data for PCBs, Atrazine and Simazine are reported from EPA 525.2. PCB data reported by ELI reflects the results for seven individual Aroclors, When the results for all seven are ND (not detected), the sample meets EPA compliance criteria for PCB monitoring. SUBCONTRACTING ANALYSIS Subcontracting of sample analyses to an outside laboratory may be required. If so, ENERGY LABORATORIES will utilize its branch laboratories or qualified contract laboratories for this service. Any such laboratories will be indicated within the Laboratory Analytical Report. BRANCH LABORATORY LOCATIONS eli-b -Energy Laboratories, Inc. -Billings, MT eli-g -Energy Laboratories, Inc. -Gillette, WY eli-h -Energy Laboratories, Inc. -Helena, MT eli-r -Energy Laboratories, Inc. -Rapid City, SD eli-t -Energy Laboratories, Inc. -College Station, TX CERTIFICATIONS: USEPA: WY00002, Radiochemical WY00937; FL-DOH NELAC: E87641, Radiochemical E871 017; California: 02118CA; Oregon: WY200001; Utah: 3072350515; Virginia: 00057; Washington: C1903 ISO 17025 DISCLAIMER: The results of this Analytical Report relate only to the items submitted for analysis. ENERGY LABORATORIES, INC. -CASPER,WY certifies that certain method selections contained in this report meet requirements as set forth by the above accrediting authorities. Some results requested by the client may not be covered under these certifications. All analysis data to be submitted for regulatory enforcement should be certified in the sample state of origin. Please verify ELI's certification coverage by visiting www.energylab.com ELI appreciates the opportunity to provide you with this analytical service. For additional information and services visit our web page www.energylab.com. Page 3 of 51 Tab I Quality Assurance and Data Validation Tables I-I: Field QA/QC Evaluation 2x Casing Volume 2x Casing Volume Location Volume Pumped Volume Pumped Volume Check Conductivity RPD Continuously MW-4 NA pumped well --2066 NIA TW4-1 59.54 88.00 60 88 OK 2248 2247 0.04 TW4-2 68.58 77.00 69 77 Pumped Dry 3068 NIA TW4-3 119.68 99.00 120 99 Pumped Dry 1937 NIA Continuously TW4-4 NA pumped well --2497 NIA TW4-5 83.50 99.00 84 99 OK 1612 1603 0.56 TW4-6 35.46 27.50 .35 28 Pumped Dry 4178 NIA TW4-7 68.36 73.00 68 73 Pumped Dry 1690 NIA TW4-8 76.24 88.00 76 88 OK 3381 3381 0.00 TW4-9 86.32 110.00 86 110 OK 2479 2478 0.04 TW4-1O 71.80 66.00 72 66 Pumped Dry 710.9 NIA TW4-11 55.42 77.00 , 55 77 Pumped Dry 1691 NIA TW4-12 80.70 88.00 81 88 OK 989.1 987 0.21 TW4-l3 73.38 61.00 73 61 Pumped Dry 1633 N/A TW4-14 7.44 5.50 ·7 6 Pumped Dry 0.1 N/A TW4-15 (MW Continuously 26) NA pumped well --3607 N/A TW4-16 103.36 l32.00 103 132 OK 3600 3601 0.03 TW4-17 73.72 77.03 :74 77 OK 3685 3680 0.14 TW4-18 105.64 121.00 106 121 OK 2058 2037 1.03 Continuously TW4-19 NA pumped well --2789 NIA Continuously TW4-20 NA pumped well .--3642 NIA TW4-21 86.52 99.00 87 99 OK 3479 3488 0.26 TW4-22 77.70 88.00 78 88 OK 5182 5163 0.37 TW4-23 63.46 77.00 63 77 OK 3794 3816 0.58 TW4-24 73.26 99.00 73 99 OK 9680 9684 0.04 TW4-25 103.60 110.00 104 110 OK 3125 3131 0.19 TW4-26 28.68 16.5 29 17 Pumped Dry 6582 NIA Ii -- ---MW 4, TW4 4, TW4 15, TW4 19, and TW4 20 are contmually pumped wells. TW4-2,TW4-3, TW4-6, TW4-7, TW4-1O, TW4-11, TW4-13, TW4-14, and TW4-26 were pumped dry and sampled after recovery. RPD > than 10% pH 6.57 15.25 15.2 6.4 6.47 6.38 6.23 6.23 6.16 6.57 6.46 6.47 6.22 6.22 6.15 6.37 6.71 6.73 6.57 5.97 6.27 6.28 6.28 6 6 5.9 5.91 6.26 5.81 6.48 6.48 6.3 6.31 5.9 5.89 6.23 6.23 6.62 6.61 3.83 RPD Temp RPD Redox Potential RPD Turbi<iity RPD I NIA 15.98 NIA 213 NIA 0.0 NIA 0.33 15.25 15.2 0.33 381 379 0.53 415 I~ 4!!lVi 0.48 NIA 16.2 NIA 403 NIA 110 NIA NIA 15.14 NIA 441 NIA I~ 21.5 .. NIA NIA 17.31 NIA 256 NIA 0 NIA 0.00 15.22 15.22 0.00 383 381 0.52 160.l [~6i3iJ~ , 1.86 NIA 15.68 NIA 363 NIA 420:. NIA NIA 15.28 NIA 267 NIA .. h~.4! ..... NIA 0.15 15.04 15.06 0.13 141 140 0.71 29.1 3'0'1:1 3.05 0.00 15.33 15.39 0.39 277 273 1.45 126.1 1.27 0.71 NIA 16.43 NIA 342 NIA 1I3.~~ NIA NIA 15.34 NIA 359 NIA '1l8.l! , NIA 0.30 14.8 14.81 0.07 414 410 0.97 4.1 4.2 2.41 NIA 15.29 NIA 420 NIA .. '" 19.9 N/A NIA 25.36 NIA 386 NIA 1.00 N/A NIA 16.29 NIA 257 NIA 0.00 NIA 0.00 14.8 14.79 0.07 262 257 1.93 44 46.t 4.66 0.00 20.73 20.81 0.39 210 207 1.44 0 0 0.00 0.17 15.6 15.58 0.l3 421 419 0.48 421 Ill' 4['9 " 0.48 NIA 16.32 N/A 248 N/A 0 N/A NIA 16.27 NIA 280 N/A ,0.00 NIA 0.00 16.67 16.65 0.12 348 340 2.33 5 5 0.00 0.16 16.59 16.63 0.24 391 383 2.07 9.1 9.~ 0.00 0.17 14.85 14.84 0.07 198 197 0.51 224.1 23(U 2.64 0.00 15 15.00 0.00 397 396 0.25 0 0 0.00 0.15 15.34 15.33 0.07 339 337 0.59 22.1 22 0.45 NIA 15.68 NIA 493 NIA 2.1 NIA 1-2: Holding Time Evaluation Sample Holding Collection Lab Analysis Allowed Time Location Constituent Date Date Holding Time Holding Time Check MW-4 Chloroform 8117/2011 8/25/2011 8.00 days 14 days OK MW-4 Chloromethane 8117/2011 8/27/2011 10.00 days 14 days OK MW-4 Methylene chloride 8/17/2011 8/27/2011 10.00 days 14 days OK MW-4 Carbon Tetrachloride 8117/2011 8/27/2011 10.00 days 14 days OK MW-4 Nitrogen 8117/2011 8/22/2011 5.00 days 28 days OK MW-4 Chloride 8/17/2011 8/25/2011 8.00 days 28 days OK TW4-1 Chloroform 8118/2011 8/25/2011 7.00 days 14 days OK TW4-1 Chloromethane 8118/2011 8/26/2011 8.00 days 14 days OK TW4-1 Methylene chloride 8/18/2011 8/26/2011 8.00 days 14 days OK TW4-1 Carbon Tetrachloride 8118/2011 8/26/2011 8.00 days 14 days OK TW4-1 Nitrogen 8118/2011 8/22/2011 4.00 days 28 days OK TW4-1 Chloride 8/18/2011 8/25/2011 7.00 days 28 days OK TW4-2 Chloroform 8117/2011 8/26/2011 9.00 days 14 days OK TW4-2 Chloromethane 8117/2011 8/26/2011 9.00 days 14 days OK TW4-2 Methylene chloride 8117/2011 8/26/2011 9.00 days 14 days OK TW4-2 Carbon Tetrachloride 8/17/2011 8/26/2011 9.00 days 14 days OK TW4-2 Nitrogen 8/17/2011 8/22/2011 5.00 days 28 days OK TW4-2 Chloride 8117/2011 8/25/2011 8.00 days 28 days OK TW4-3 Chloroform 8/16/2011 8/23/2011 7.00 days 14 days OK TW4-3 Chloromethane 8/16/2011 8/23/2011 7.00 days 14 days OK TW4-3 Methylene chloride 8/16/2011 8/23/2011 7.00 days 14 days OK TW4-3 Carbon Tetrachloride 8/16/2011 8/23/2011 7.00 days 14 days OK TW4-3 Nitrogen 8/16/2011 8/22/2011 6.00 days 28 days OK TW4-3 Chloride 8116/2011 8/22/2011 6.00 days 28 days OK TW4-4 Chloroform 8117/2011 8/27/2011 10.00 days 14 days OK TW4-4 Chloromethane 8/17/2011 8/27/2011 10.00 days 14 days OK TW4-4 Methylene chloride 8117/2011 8/27/2011 10.00 days 14 days OK TW4-4 Carbon Tetrachloride 8/17/2011 8/27/2011 10.00 days 14 days OK TW4-4 Nitrogen 8/17/2011 8/22/2011 5.00 days 28 days OK TW4-4 Chloride 8/17/2011 8/25/2011 8.00 days 28 days OK TW4-5 Chloroform 8/17/2011 8/25/2011 8.00 days 14 days OK TW4-5 Chloromethane 8/17/2011 8/25/2011 8.00 days 14 days OK TW4-5 Methylene chloride 8/17/2011 8/25/2011 8.00 days 14 days OK TW4-5 Carbon Tetrachloride 8/17/2011 8/25/2011 8.00 days 14 days OK TW4-5 Nitrogen 8117/2011 8/22/2011 5.00 days 28 days OK TW4-5 Chloride 8/17/2011 8/25/2011 8.00 days 28 days OK TW4-6 Chloroform 8/17/2011 8/25/2011 8.00 days 14 days OK TW4-6 Chloromethane 8117/2011 8/25/2011 8.00 days 14 days OK TW4-6 Methylene chloride 8117/2011 8/25/2011 8.00 days 14 days OK TW4-6 Carbon Tetrachloride 8117/2011 8/25/2011 8.00 days 14 days OK TW4-6 Nitrogen 8117/2011 8/22/2011 5.00 days 28 days OK TW4-6 Chloride 8117/2011 8/25/2011 8.00 days 28 days OK TW4-7 Chloroform 8/18/2011 8/25/2011 7.00 days 14 days OK TW4-7 Chloromethane 8/18/2011 8/26/2011 8.00 days 14 days OK TW4-7 Methylene chloride 8/18/2011 8/26/2011 8.00 days 14 days OK TW4-7 Carbon Tetrachloride 8/18/2011 8/26/2011 8.00 days 14 days OK TW4-7 Nitrogen 8/18/2011 8/22/2011 4.00 days 28 days OK 1-2: Holding Time Evaluation Sample Holding Collection Lab Analysis Allowed Time Location Constituent Date Date Holding Time Holding Time Check TW4-7 Chloride 8/1812011 8/2512011 7.00 days 28 days OK TW4-8 Chloroform 811612011 8/2412011 8.00 days 14 days OK TW4-8 Chloromethane 8/1612011 8/2412011 8.00 days 14 days OK TW4-8 Methylene chloride 8/16/2011 8/24/2011 8.00 days 14 days OK TW4-8 Carbon Tetrachloride 8/1612011 812412011 8.00 days 14 days OK TW4-8 Nitrogen 8/1612011 812212011 6.00 days 28 days OK TW4-8 Chloride 8/1612011 8/25/2011 9.00 days 28 days OK TW4-9 Chloroform 8/1612011 8/2412011 8.00 days 14 days OK TW4-9 Chloromethane 8/1612011 8/2412011 8.00 days 14 days OK TW4-9 Methylene chloride 8/1612011 8/2412011 8.00 days 14 days OK TW4-9 Carbon Tetrachloride 8/1612011 812412011 8.00 days 14 days OK TW4-9 Nitrogen 8/16/2011 812212011 6.00 days 28 days OK TW4-9 Chloride 8/16/2011 812512011 9.00 days 28 days OK TW4-10 Chloroform 8/1712011 8/2512011 8.00 days 14 days OK TW4-10 Chloromethane 8/1712011 8126/2011 9.00 days 14 days OK TW4-10 Methylene chloride 8/17/2011 812612011 9.00 days 14 days OK TW4-10 Carbon Tetrachloride 8/1712011 8/2612011 9.00 days 14 days OK TW4-10 Nitrogen 8117/2011 8/2212011 5.00 days 28 days OK TW4-10 Chloride 811712011 8/2512011 8.00 days 28 days OK TW4-11 Chloroform 8/17/2011 8/2512011 8.00 days 14 days OK TW4-11 Chloromethane 8117/2011 8/2612011 9.00 days 14 days OK TW4-11 Methylene chloride 8117/2011 8/26/2011 9.00 days 14 days OK TW4-11 Carbon Tetrachloride 8117/2011 8/26/2011 9.00 days 14 days OK TW4-11 Nitrogen 8/1712011 8122/2011 5.00 days 28 days OK TW4-11 Chloride 811712011 8125/2011 8.00 days 28 days OK TW4-12 Chloroform 8/1612011 8/2312011 7.00 days 14 days OK TW4-12 Chloromethane 8/1612011 8/2312011 7.00 days 14 days OK TW4-12 Methylene chloride 8/1612011 8/23/2011 7.00 days 14 days OK TW4-12 Carbon Tetrachloride 8/1612011 8/2312011 7.00 days 14 days OK TW4-12 Nitrogen 8/1612011 8/2212011 6.00 days 28 days OK TW4-12 Chloride 8/1612011 812212011 6.00 days 28 days OK TW4-13 Chloroform 8/1612011 812312011 7.00 days 14 days OK TW4-13 Chloromethane 8/16/2011 812312011 7.00 days 14 days OK TW4-13 Methylene chloride -8/16/2011 8/23/2011 7.00 days 14 days OK TW4-13 Carbon Tetrachloride 8/1612011 812312011 7.00 days 14 days OK TW4-13 Nitrogen 8/1612011 8/2212011 6.00 days 28 days OK TW4-13 Chloride 8/1612011 8/2212011 6.00 days 28 days OK TW4-14 Chloroform 8116/2011 812512011 9.00 days 14 days OK TW4-14 Chloromethane 8/1612011 812512011 9.00 da,)'s 14 days OK TW4-14 Methylene chloride 8/1612011 812512011 9.00 days 14 days OK TW4-14 Carbon Tetrachloride 811612011 8/2512011 9.00 days 14 days OK TW4-14 Nitrogen 811612011 8/2212011 6.00 days 28 days OK TW4-14 Chloride 8/16/2011 8/2212011 6.00 days 28 days OK TW4-15 Chloroform 811712011 8/2612011 9.00 days 14 days OK TW4-15 Chloromethane 8/1712011 8/26/2011 9.00 days 14 days OK TW4-15 Methylene chloride 8/1712011 8/2612011 9.00 days 14 days OK TW4-15 Carbon Tetrachloride 8117/2011 8/2612011 9.00 days 14 days OK TW4-15 Nitrogen 8/1712011 812212011 5.00 days 28 days OK 1-2: Holding Time Evaluation Sample Holding Collection Lab Analysis Allowed Time Location Constituent Date Date Holding Time Holding Time Check TW4-15 Chloride 811712011 812512011 8.00 days 28 days OK TW4-16 Chloroform 8117/2011 8/2512011 8.00 days 14 days OK TW4-16 Chloromethane 811712011 8125/2011 8.00 days 14 days OK TW4-16 Methylene chloride 8/1712011 8125/2011 8.00 days 14 days OK TW4-16 Carbon Tetrachloride 811712011 8/25/2011 8.00 days 14 days OK TW4-16 Nitrogen 811712011 8/22/2011 5.00 days 28 days OK TW4-16 Chloride 8117/2011 8125/2011 8.00 days 28 days OK MW-32 Chloroform 8116/2011 8125/2011 9.00 days 14 days OK MW-32 Chloromethane 8116/2011 8125/2011 9.00 days 14 days OK MW-32 Methylene chloride 8116/2011 8125/2011 9.00 days 14 days OK MW-32 Carbon Tetrachloride 8116/2011 8/25/2011 9.00 days 14 days OK MW-32 Nitrogen 8116/2011 8122/2011 6.00 days 28 days OK MW-32 Chloride 8116/2011 8/22/2011 6.00 days 28 days OK TW4-18 Chloroform 811712011 8/24/2011 7.00 days 14 days OK TW4-18 Chloromethane 811712011 8124/2011 7.00 days 14 days OK TW4-18 Methylene chloride 811712011 8124/2011 7.00 days 14 days OK TW4-18 Carbon Tetrachloride 8117/2011 812412011 7.00 days 14 days OK TW4-18 Nitrogen 811712011 812212011 5.00 days 28 days OK TW4-18 Chloride 811712011 8125/2011 8.00 days 28 days OK TW4-19 Chloroform 811712011 812612011 9.00 days 14 days OK TW4-19 Chloromethane 811712011 812612011 9.00 days 14 days OK TW4-19 Methylene chloride 8117/2011 8/2612011 9.00 days 14 days OK TW4-19 Carbon Tetrachloride 8117/2011 8/2612011 9.00 days 14 days OK TW4-19 Nitrogen 8/17/2011 8/22/2011 5.00 days 28 days OK TW4-19 Chloride 8/1712011 8/25/2011 8.00 days 28 days OK TW4-20 Chloroform 811712011 8/2612011 9.00 days 14 days OK TW4-20 Chloromethane 8/17/2011 812712011 10.00 days 14 days OK TW4-20 Methylene chloride 8/1712011 812712011 10.00 days 14 days OK TW4-20 Carbon Tetrachloride 8/17/2011 812712011 10.00 days 14 days OK TW4-20 Nitrogen 8/17/2011 812212011 5.00 days 28 days OK TW4-20 Chloride 8117/2011 8/2512011 8.00 days 28 days OK TW4-21 Chloroform 8117/2011 8/2512011 8.00 days 14 days OK TW4-21 Chloromethane 811712011 8/2712011 10.00 days 14 days OK TW4-21 Methylene chloride 8117/2011 8/2712011 10.00 days 14 days OK TW4-21 Carbon Tetrachloride 811712011 8/2712011 10.00 days 14 days OK TW4-21 Nitrogen 811712011 812212011 5.00 days 28 days OK TW4-21 Chloride 8/17/2011 8/25/2011 8.00 days 28 days OK TW4-22 Chloroform 8/1712011 8/2512011 8.00 days 14 days OK TW4-22 Chloromethane 8/1712011 8/2412011 7.00 days 14 days OK TW4-22 Methylene chloride 8/17/2011 8/2412011 7.00 days 14 days OK TW4-22 Carbon Tetrachloride 811712011 8/2412011 7.00 days 14 days OK TW4-22 Nitrogen 811712011 8/2212011 5.00 days 28 days OK TW4-22 Chloride 8117/2011 812512011 8.00 days 28 days OK TW4-23 Chloroform 8116/2011 8/2312011 7.00 days 14 days OK TW4-23 Chloromethane 811612011 8/2312011 7.00 days 14 days OK TW4-23 Methylene chloride 811612011 8123/2011 7.00 days 14 days OK TW4-23 Carbon Tetrachloride 8116/2011 8/2312011 7.00 days 14 days OK TW4-23 Nitrogen 811612011 8/2212011 6.00 days 28 days OK 1-2: Holding Time Evaluation Sample Holding Collection Lab Analysis Allowed Time Location Constituent Date Date Holding Time Holding Time Check TW4-23 Chloride 8116/2011 8125/2011 9.00 days 28 days OK TW4-24 Chloroform 8117/2011 8/2412011 7.00 days 14 days OK TW4-24 Chloromethane 8117/2011 8/2412011 7.00 days 14 days OK TW4-24 Methylene chloride 8117/2011 8/24/2011 7.00 days 14 days OK TW4-24 Carbon Tetrachloride 8117/2011 8/2412011 7.00 days 14 days OK TW4-24 Nitrogen 811712011 812212011 5.00 days 28 days OK TW4-24 Chloride 8/1712011 8/25/2011 8.00 days 28 days OK TW4-25 Chloroform 8116/2011 8124/2011 8.00 days 14 days OK TW4-25 Chloromethane 8116/2011 8124/2011 8.00 days 14 days OK TW4-25 Methylene chloride 8/16/2011 8/24/2011 8.00 days 14 days OK TW4-25 Carbon Tetrachloride 8116/2011 812412011 8.00 days 14 days OK TW4-25 Nitrogen 8116/2011 8/22/2011 6.00 days 28 days OK TW4-25 Chloride 8116/2011 8/25/2011 9.00 days 28 days OK TW4-26 Chloroform 8/1712011 8/2412011 7.00 days 14 days OK TW4-26 Chloromethane 8/1712011 812412011 7.00 days 14 days OK TW4-26 Methylene chloride 8/17/2011 8/2412011 7.00 days 14 days OK TW4-26 Carbon Tetrachloride 8/17/2011 812412011 7.00 days 14 days OK TW4-26 Nitrogen 8117/2011 8122/2011 5.00 days 28 days OK TW4-26 Chloride 8/17/2011 8125/2011 8.00 days 28 days OK TW4-60 Chloroform 8/1712011 812612011 9.00 days 14 days OK TW4-60 Chloromethane 811712011 812612011 9.00 days 14 days OK TW4-60 Met~ene chloride 811712011 8/26/2011 9.00 days 14 days OK TW4-60 Carbon Tetrachloride 8/17/2011 8126/2011 9.00 days 14 days OK TW4-60 Nitrogen 8/17/2011 8/22/2011 5.00 days 28 days OK TW4-60 Chloride 8/1712011 8/25/2011 8.00 days 28 days OK TW4-65 Chloroform 8/1612011 812412011 8.00 days 14 days OK TW4-65 Chloromethane 8/1612011 812412011 8.00 days 14 days OK TW4-65 Methylene chloride 8/1612011 812412011 8.00 days 14 days OK TW4-65 Carbon Tetrachloride 8/16/2011 812412011 8.00 days 14 days OK TW4-65 Nitrogen 8/1612011 812212011 6.00 days 28 days OK TW4-65 Chloride 8/1612011 8/2512011 9.00 days 28 days OK TW4-70 Chloroform 8/17/2011 8/26/2011 9.00 days 14 days OK TW4-70 Chloromethane 8117/2011 812612011 9.00 days 14 days OK TW4-70 Methylene chloride 8117/2011 8126/2011 9.00 days 14 days OK TW4-70 Carbon Tetrachloride 811712011 8/26/2011 9.00 days 14 days OK TW4-70 Nitrogen 811712011 8/2212011 5.00 days 28 days OK TW4-70 Chloride 811712011 812512011 8.00 days 28 days OK Table 1-3 Recipt Temperature Check Sample Batch Wells in Batch Temperature C11050927 MW-4, TW4-1, TW4-2, TW4-3, TW4-3R, TW4-4, TW4-5, 2.8 °C TW4-6, TW4-7, TW4-7R, TW4-8, TW4-9, TW4-1O, TW4- 11, TW4-12, TW4-13, TW4-14, TW4-15 (MW-26), TW4- 16, MW-32, TW4-18, TW4-19, TW4-20, TW4-21, TW4- 22, TW4-23, TW4-24,TW4-24R, TW4-25, TW4-26, TW4- 60, TW4-65, TW4-70, Trip Blank 1-4 Analytical Method Check Parameter Method Method Used by Lab Carbon Tetrachloride SW8260B SW8260B Chloride A4500-Cl B A4500-Cl B Chloroform SW8260B SW8260B Chloromethane SW8260B SW8260B Methylene chloride SW8260B SW8260B Nitrogen E353.2 E353.2 All parameters were analyzed using the reporting method specificied in the QAP 1-5 Reporting Limit Evaluation Rqd' Lab Reporting Reporting Qualifier Location Constituent Limit Limit Check MW-4 Chloroform 100 ug/L 1.0 ug/L OK MW-4 Chloromethane 1 ug/L 1.0 ug/L OK MW-4 Methylene chloride 1 ug/L 1.0 ug/L OK MW-4 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK MW-4 Nitrogen 0.5 mg/L 0.1 mg/L OK MW-4 Chloride 1 mg/L 1 mg/L OK TW4-1 Chloroform 100 ug/L 1.0 ug/L OK TW4-1 Chloromethane 1 ug/L 1.0 ug/L OK TW4-1 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-1 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-1 Nitrogen 0.5 mg/L 0.1 mg/L OK TW4-1 Chloride 1 mg/L 1 mg/L OK TW4-2 Chloromethane 1 ug/L 1.0 ug/L OK TW4-2 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-2 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-2 Nitrogen 0.5 mg/L 0.1 mg/L OK TW4-2 Chloride 1 mg/L 1 mg/L OK TW4-3 Chloroform 1 ug/L 1.0 ug/L OK TW4-3 Chloromethane 1 ug/L 1.0 ug/L OK TW4-3 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-3 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-3 Nitrogen 0.2 mg/L 0.1 mg/L OK TW4-3 Chloride 1 mg/L 1 mg/L OK TW4-4 Chloroform 100 ug/L 1.0 ug/L OK TW4-4 Chloromethane 1 ug/L 1.0 ug/L OK TW4-4 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-4 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-4 Nitrogen 0.5 mg/L 0.1 mg/L OK TW4-4 Chloride 1 mg/L 1 mg/L OK TW4-5 Chloroform 1 ug/L 1.0 ug/L OK TW4-5 Chloromethane 1 ug/L 1.0 ug/L OK TW4-5 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-5 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-5 Nitrogen 0.5 mg/L 0.1 mg/L OK TW4-5 Chloride 1 mg/L 1 mg/L OK TW4-6 Chloroform 1 ug/L 1.0 ug/L OK TW4-6 Chloromethane 1 ug/L 1.0 ug/L OK TW4-6 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-6 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-6 Nitrogen 0.1 mg/L 0.1 mg/L OK TW4-6 Chloride 1 mg/L 1 mg/L OK TW4-7 Chloroform 100 ug/L 1.0 ug/L OK TW4-7 Chloromethane 1 ug/L 1.0 ug/L OK TW4-7 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-7 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-7 Nitrogen 0.2 mg/L 0.1 mg/L OK TW4-7 Chloride 1 mg/L 1 mg/L OK 1-5 Reporting Limit Evaluation Rqd' Lab Reporting Reporting Qualifier Location Constituent Limit Limit Check TW4-8 Chloroform 1 ug/L 1.0 ug/L OK TW4-8 Chloromethane 1 ug/L 1.0 ug/L OK TW4-8 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-8 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-8 Nitrogen 0.1 mg/L 0.1 mg/L OK TW4-8 Chloride 1 mg/L 1 mg/L OK TW4-9 Chloromethane 1 ug/L 1.0 ug/L OK TW4-9 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-9 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-9 Nitrogen 0.2 mg/L 0.1 mg/L OK TW4-9 Chloride 1 mg/L 1 mg/L OK TW4-1O Chloroform 10 ug/L 1.0 u~/L OK TW4-1O Chloromethane 1 ug/L 1.0 ug/L OK TW4-10 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-1O Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-1O Nitrogen 0.1 mg/L 0.1 m~/L OK TW4-1O Chloride 1 mg/L 1 mg/L OK TW4-11 Chloroform 100 ug/L 1.0 ug/L OK TW4-11 Chloromethane 1 ug/L 1.0 ug/L OK TW4-11 Methylene chloride 1 ug/L 1.0 tJg/L OK TW4-11 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-11 Nitrogen 0.5 mg/L 0.1 mg/L OK TW4-11 Chloride 1 mg/L 1 mg/L OK TW4-12 Chloroform 1 ug/L 1.0 ug/L OK TW4-12 Chloromethane 1 ug/L 1.0 ug/L OK TW4-12 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-12 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-12 Nitrogen 0.5 mg/L 0.1 mg/L OK TW4-12 Chloride 1 mg/L 1 mg/L OK TW4-13 Chloroform 1 ug/L 1.0 ug/L OK TW4-13 Chloromethane 1 ug/L 1.0 u~/L OK TW4-13 Methylene chloride 1 ug/L 1.0 u_~/L OK TW4-13 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-13 Nitrogen 0.5 mg/L 0.1 mg/L OK TW4-13 Chloride 1 mg/L 1 mg/L OK TW4-14 Chloroform 1 ug/L 1.0 u~/L OK TW4-14 Chloromethane 1 ug/L 1.0 ug/L OK TW4-14 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-14 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-14 Nitrogen 0.1 mg/L 0.1 m~/L OK TW4-14 Chloride 1 mg/L 1 mg/L OK TW4-15 Chloroform 100 ug/L 1.0 ug/L OK TW4-15 Chloromethane 1 ug/L 1.0 ug/L OK TW4-15 Methylene chloride 1 ug/L 1.0 tJg/L OK TW4-15 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-15 Nitrogen 0.1 mg/L 0.1 mg/L OK TW4-15 Chloride 1 mg/L 1 mg/L OK TW4-16 Chloroform 1 ug/L 1.0 ug/L OK 1-5 Reporting Limit Evaluation Rqd' Lab Reporting Reporting Qualifier Location Constituent Limit Limit Check TW4-16 Chloromethane 1 ug/L 1.0 ug/L OK TW4-16 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-16 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-16 Nitrogen 0.1 mg/L 0.1 mg/L OK TW4-16 Chloride 1 mg/L 1 mg/L OK MW-32 Chloroform 1 ug/L 1.0 ug/L OK MW-32 Chloromethane 1 ug/L 1.0 ug/L OK MW-32 Methylene chloride 1 ug/L 1.0 ug/L OK MW-32 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK MW-32 Nitrogen 0.1 mg/L 0.1 mg/L OK MW-32 Chloride 1 mg/L 1 mg/L OK TW4-18 Chloroform 1 ug/L 1.0 ug/L OK TW4-18 Chloromethane 1 ug/L 1.0 ug/L OK TW4-18 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-18 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-18 Nitrogen 0.5 mg/L 0.1 mg/L OK TW4-18 Chloride 1 mg/L 1 mg/L OK TW4-19 Chloroform 100 ug/L 1.0 ug/L OK TW4-19 Chloromethane 1 ug/L 1.0 ug/L OK TW4-19 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-19 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-19 Nitrogen 0.2 mg/L 0.1 mg/L OK TW4-19 Chloride 1 mg/L 1 mg/L OK TW4-20 Chloroform 1000 ug/L 1.0 ug/L OK TW4-20 Chloromethane 1 ug/L 1.0 ug/L OK TW4-20 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-20 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-20 Nitrogen 0.5 mg/L 0.1 mg/L OK TW4-20 Chloride 1 mg/L 1 mg/L OK TW4-21 Chloroform 10 ug/L 1.0 ug/L OK TW4-21 Chloromethane 1 ug/L 1.0 ug/L OK TW4-21 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-21 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-21 Nitrogen 1 mg/L 0.1 mg/L OK TW4-21 Chloride 1 mg/L 1 mg/L OK TW4-22 Chloroform 100 ug/L 1.0 ug/L OK TW4-22 Chloromethane 1 ug/L 1.0 ug/L OK TW4-22 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-22 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-22 Nitrogen 1 mg/L 0.1 mg/L OK TW4-22 Chloride 1 mg/L 1 mg/L OK TW4-23 Chloroform 1 ug/L 1.0 ug/L OK TW4-23 Chloromethane 1 ug/L 1.0 ug/L OK TW4-23 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-23 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-23 Nitrogen 0.1 mg/L 0.1 mg/L OK TW4-23 Chloride 1 mg/L 1 mg/L OK TW4-24 Chloroform 1 ug/L 1.0 ug/L OK 1-5 Reporting Limit Evaluation Rqd' Lab Reporting Reporting Qualifier Location Constituent Limit Limit Check TW4-24 Chloromethane 1 ug/L 1.0 ug/L OK TW4-24 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-24 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-24 Nitrogen 1 mg/L 0.1 mg/L OK TW4-24 Chloride 1 mg/L 1 mg/L OK TW4-25 Chloroform 1 ug/L 1.0 ug/L OK TW4-25 Chloromethane 1 ug/L 1.0 ug/L OK TW4-25 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-25 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-25 Nitrogen 1 mg/L 0.1 mg/L OK TW4-25 Chloride 1 mg/L I mg/L OK TW4-26 Chloroform 1 ugIL 1.0 ug/L OK TW4-26 Chloromethane 1 ugIL 1.0 ug/L OK TW4-26 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-26 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-26 Nitrogen 1 mg/L 0.1 mg/L OK TW4-26 Chloride 1 mg/L 1 mg/L OK TW4-60 Chloroform 1 ug/L 1.0 ug/L OK TW4-60 Chloromethane 1 ug/L 1.0 ug/L OK TW4-60 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-60 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-60 Nitrogen 0.1 mg/L 0.1 mg/L OK TW4-60 Chloride 1 mg/L 1 mg/L OK TW4-65 Chloroform 100 ug/L 1.0 ug/L OK TW4-65 Chloromethane 1 ug/L 1.0 ug/L OK TW4-65 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-65 Carbon Tetrachloride 1 ug/L 1.0 ugIL OK TW4-65 Nitrogen 0.1 mg/L 0.1 mg/L OK TW4-65 Chloride 1 mg/L 1 mg/L OK TW4-70 Chloroform 1 ug/L 1.0 ug/L OK TW4-70 Chloromethane 1 ugIL 1.0 ug/L OK TW4-70 Methylene chloride 1 ug/L 1.0 ug/L OK TW4-70 Carbon Tetrachloride 1 ug/L 1.0 ug/L OK TW4-70 Nitrogen 0.1 mg/L 0.1 mg/L OK TW4-70 Chloride 1 mg/L 1 mg/L OK U = Analyte was not detected at the RL D = RL was increased due to sample matrix or required dilution due to the sample concentration. In all 1-6 Trip Blank Evaluation -Lab Report Constituent Result CII080835 Carbon tetrachloride ND ug/L Chloroform ND ug/L Chloromethane ND ug/L Methylene chloride ND ug/L 1-7 QAJQC Evaluation for Sample Duplicates Constituent , TW4-23 TW4-65 %RPD " Chloride (mg/L) 41 45 9 Nitrate + Nitrite (as N) ND ND NC Carbon Tetrachloride ND ND NC Chloroform ND ND NC Chloromethane ND ND NC Dichloromethane (Methylene Chloride) ND ND NC Constituent i" TW4-16 TW4-70 %RPD " Chloride (mg/L) 63 62 1.60 Nitrate + Nitrite (as N) 1.7 1.7 0.00 Carbon Tetrachloride ND ND NC Chloroform 9.2 8.1 12.72 Chloromethane ND ND NC Dichloromethane (Methylene Chloride) ND 1.3 NC 1-8 QC Control Limits for Analysis and Blanks Matrix Spike % Recovery Comparison Lab Report Lab Sample ID Well Cll080835 CII080821-002 NA NA -Not a Denison sample Surrogate % Recovery ., Lab Report Well/Sample Analyte Cll080835 TW4-3 Bromofluorobenezene Cll080835 TW4-3R Bromofluorobenezene Cll080835 TW4-7R Bromofluorobenezene Cll080835 TW4-8 Bromofluorobenezene Cll080835 TW4-9 Bromofluorobenezene Cll080835 TW4-12 Dichlorobenzene-d4 Cll080835 TW4-12 Bromofluorobenezene Cll080835 TW4-13 Bromofluorobenezene Cll080835 TW4-18 Bromofluorobenezene Cll080835 TW4-22 Bromofluorobenezene Cll080835 TW4-23 Dichlorobenzene-d4 Cll080835 TW4-23 Bromofluorobenezene Cll080835 TW4-24 Dichlorobenzene-d4 Cll080835 TW4-24 Bromofluorobenezene Cll080835 TW4-25 Bromofluorobenezene Cll080835 TW4-26 Bromofluorobenezene Cll080835 TW4-65 Bromofluorobenezene Nitrogen 107 111 I ' " "" ,f'i,~';;'~;~~' I ,,:'f'" , , '" ',,',';: " ',' "~" ' Lab "~~, 1"1f . ''''':;',g, ~.' ~ . .;.. ~·i:~ , Q~P:, " ,'~~:", : ~,i' ;;,:"fli: 13;~,pe~~e~:' . Req~!i'r.,ed" Surrogat(!' %l{E'{:'y RE(:-.Raiig~ ~"~Range .. 125 80-120 None 124 80-120 None 132 80-120 None 124 80-120 None 130 80-120 None 121 80-120 None 134 80-120 None 133 80-120 None 127 80-120 None 125 80-120 None 122 80-120 None 135 80-120 None 121 80-120 None 124 80-120 None 128 80-120 None 127 80-120 None 130 80-120 None .REC Rlinge 90-110 RPI) , 3.7 1-9 Rinsate Evaluation Result for Previous Well Previous Well Rinsate Sample Parameter Rinsate Result Sampled Sampled TW4-7R Chloroform 2.8 I ugiL TW4-11 820 I ugiL Previous well sampled is the well that the pump was used to purge prior to the rinsate sample. D = Reporting limit raised due to dilution/sample matrix. ** Only rinsates with detections are listed. TW4-3R and TW4-24R results were ND Rinsate Reporting Qualifier Limit D 1.0ugiL TabJ Kriged Current Quarter Chloroform Isoconcentration Map ~ f' PROPERTY BOUNDARY II II « -...:::-- MW-2 II MW-01 eNS II II II II II ~g II '/ ~NS TWN-7 CELL NO.1 MW-18 eNS ~NS TWN-18 ~NS TWN-3 NO ~NS TWN-15 ~NS ~NS TWN-11 ~NS TWN-14 TWN-10 ~NS ~NS TWN-9 TWN-6 PIEZ-1 "NS ~NS MW-19 TWN-8 eNS PIEZ-2 "NS ~NS Mltt2~ITE N4 f ~N PIEZ-3 TWN-"NS 0 ~NS TWN-12 ( CELL NO.2 o MW-4 .1700 TW4-1 0 1300 PIEZ-1 Q NS TWN-4 ,~ NS MW-35 . -</-ND MW-36 ~ ND MW-03 eNS N MW-20 eNS SCALE IN FEET EXPLANATION perched monitoring well showing concentration in uG/1 temporary perched monitoring well showing concentration in uG/1 perched piezometer (not sampled) temporary perched nitrate monitoring well (not sampled) perched monitoring well installed August/September, 2010 showing concentration in uG/1 perched monitoring well installed April, 2011 showing concentration in uG/L 3000 HYDRO GEO CHEM, INC. MW-17 e NS 33 l'M~1 500 6Wg-14 4-6 NO 0 1 o TW4-23 TW~326 PIEZ4 "NS * PIEZ-5 "NS T37S T38S MW-22 e NS II // // // // // // // // // // NOTE: MW-4, MW-26, TW4-4, TW4-19 and TW4-20 are pumping wells ) > '7 KRIGED 3rd QUARTER, 2011 CHLOROFORM (uG/L) WHITE MESA SITE APPROVED DATE REFERENCE FIGURE SJS H:/718000/nov11/chI0911.srf J-1 TabK Analyte Concentrations Over Time 1~:':~~~~~'!J~~11~~f~~~ ~,~ : "nil! ' , ' lti 1 '~'t '. ~ . ' , I e ' a ' etli . C':lil e IMW . metr:a~llIodde . .: .!l; . . , ':~\l.iI(' ' .. !I;\! ii~~ ~~!~Ug{.l~~~. h:IOlnde ~ " I~ tID )~. "" . -{;c' '" '" _, .-(~U I, iJ;.. r~ ',,,: '.li\ ',' . I~' 28-Sep-99 6200 28-Sep-99 5820 28-Sep-99 6020 15-Mar-00 5520 15-Mar-00 5430 2-Sep-00 5420 9.63 30-Nov-00 6470 9.37 29-Mar-01 4360 8.77 22-Jun-01 6300 9.02 20-Sep-01 5300 9.45 8-Nov-01 5200 8 26-Mar-02 4700 8.19 22-May-02 4300 8.21 12-Sep-02 6000 8.45 24-Nov-02 2500 8.1 28-Mar-03 2000 8.3 30-Apr-03 3300 NA 30-May-03 3400 8.2 23-Jun-03 4300 8.2 30-Jul-03 3600 8.1 29-Aug-03 4100 8.4 12-Sep-03 3500 8.5 15-0ct-03 3800 8.1 8-Nov-03 3800 8 29-Mar-04 NA NA 22-Jun-04 NA NA 17-Sep-04 3300 6.71 17-Nov-04 4300 7.5 16-Mar-05 2900 6.3 25-May-05 3170 NA NA NA 7.1 NA 31-Aug-05 3500 <10 <10 <10 7.0 NA I-Dec-OS 3000 <50 <50 <50 7.0 NA 9-Mar-06 3100 <50 <50 50 6 49 14-Jun-06 3000 <50 <50 50 6 49 20-Jul-06 2820 <50 <50 <50 1.2 48 9-Nov-06 2830 2.1 1.4 <1 6.4 50 28-Feb-07 2300 1.6 <1 <1 6.3 47 27-Jun-07 2000 1.8 <1 <1 7 45 15-Aug-07 2600 1.9 <1 <1 6.2 47 1O-0ct-07 2300 1.7 <1 <1 6.2 45 26-Mar-08 2400 1.7 <1 <1 5.8 42 25-Jun-08 2500 1.6 <1 <1 6.09 42 10-Sep-08 1800 1.8 <1 <1 6.36 35 15-0ct-08 2100 1.7 <1 <1 5.86 45 4-Mar-09 2200 1.5 <1 <1 5.7 37 2000 <1 <1 5.3 43 14-0ec-09 1800 1.6 NO NO 5.8 44 17-Feb-1O 1600 1.2 NO NO 4 45 14-Jun-1O 2100 1.2 NO NO 5.1 41 16-Aug-1O 1900 1.5 NO NO 4.8 38 11-0ct-l0 1500 1.4 NO NO 4.9 41 23-Feb-ll 1700 1.5 NO NO 4.6 40 I-Jun-ll 1700 1.4 NO NO 4.9 35 17-Aug-ll 1700 1.1 NO NO 4.9 41 24-Jun-09 1500 1 <1 <1 37 15-Sep-09 1700 <1 <1 <1 7.3 36 29-Dec-09 1400 <1 <1 <1 6.8 41 3-Mar-1O 1300 <1 <1 <1 7.1 35 15-Jun-1O 1600 1.2 <1 <1 6.8 40 24-Aug-1O 1500 <1 <1 <1 6.8 35 14-0ct-1O 1500 <1 <1 <1 6.6 40 24-Feb-ll 1300 ND ND ND 6.6 41 I-Jun-ll 1200 ND ND ND 7 35 18-Aug-ll 1300 ND ND ND 6.8 36 ~i' 'TW4-' ~hlo .,., ,~>: 'I t ., .IlI'de;,1 C ~etl1:a~e 1:/ eltl' 'd~~~ If",Nltl7<ater lil·fE6IoFld~ , "'~ "~"". "ifloi>1 "j ..da'ibon" .'~ ":H Melh~te"M .;,'.t <'" l ' .• ~, ~-. ' I~' " '~l'!:-e ,rae OFI e. 'Ii " ; ~ :~;~ on e~,.li~ I !t~: IU~ '\",' it~~r~j~ 1~~1i ",~~~~~,,'i "";~·i:tA~·~;tt.'.~ :,j i~i'::ffli' .,~J ,£ ,:,,~~ 1~,,1(lllktI~):; I~~!~~~~.~~l !~.,w.~P.,)~ 1O-Nov-99 2510 2-Sep-00 5220 28-Nov-00 4220 10.7 29-Mar-Ol 3890 10.2 22-Jun-Ol 5500 9.67 20-Sep-Ol 4900 11,4 8-Nov-Ol 5300 10.1 26-Mar-02 5100 9.98 23-May-02 4700 9.78 12-Sep-02 6000 9,44 24-Nov-02 5400 10,4 28-Mar-03 4700 9.5 23-Jun-03 5100 9.6 12-Sep-03 3200 8.6 8-Nov-03 4700 9.7 29-Mar-04 4200 9.14 22-Jun-04 4300 8.22 17-Sep-04 4100 8,4 17-Nov-04 4500 8.6 16-Mar-05 3700 7.7 25-May-05 3750 8.6 31-Aug-05 3900 <10 <10 <10 8 NA I-Dee-05 3500 <50 <50 <50 7.8 NA 9-Mar-06 3800 <50 <50 <50 7.5 56 14-Jun-06 3200 <50 <50 <50 7.1 56 20-Jul-06 4120 <50 <50 <50 7,4 54 8-Nov-06 3420 2.3 <1 <1 7.6 55 28-Peb-07 2900 1.8 <1 <1 7.3 54 27-Jun-07 3000 2.5 <1 <1 7.8 50 15-Aug-07 340 2.2 <1 <1 7.3 49 1O-0ct-07 3200 2.1 <1 <1 6.9 51 26-Mar-08 3300 2.3 <1 <1 6.9 48 25-Jun-08 3100 2.2 <1 <1 7,44 46 10-Sep-08 2800 2,4 <1 <1 7.1 42 15-0ct-08 3200 2,4 <2 <2 7.99 47 ll-Mar-09 3100 2.2 <1 <1 6.5 46 24-Jun-09 2800 2 <1 <1 6,4 44 15-Sep-09 3000 2 <1 <1 6.6 43 29-Dec-09 1600 2 <1 <1 6,4 46 3300 <1 <1 6.7 43 3300 2.5 <1 <1 6.6 43 14-0ct-10 3000 2.1 <1 <1 6.5 41 24-Feb-11 3100 2.4 ND ND 7 46 2-Jun-ll 3000 2.2 ND ND 6.8 42 17-Aug-ll 2400 1.6 ND ND 6 48 ~,::~\,)};:t~: i"~f!l""'Il+~J'_ B iF .. ' 011Om.! iii .' ,Nlbat 10 .. 00 ! i. :,~ ':,;:, I .: I OF. r ~li' II , ~' I iUgll ). II,: .' ,~~ ;~li ,1f ,/), 'i,,' , 28-Jun-99 3S00 7.6 29-Nov-99 702 lS-Mar-OO 834 2-Sep-00 836 1.S6 29-Nov-00 836 1.97 27-Mar-01 347 1.8S 21-Jun-01 390 2.61 20-Sep-Ol 300 3.06 7-Nov-01 170 3.6 26-Mar-02 11 3.87 21-May-02 204 4.34 12-Sep-02 203 4.32 24-Nov-02 102 4.9 28-Mar-03 0 4.6 23-Jun-03 0 4.8 12-Sep-03 0 4.3 8-Nov-03 0 4.8 29-Mar-04 0 4.48 22-Jun-04 0 3.68 17-Sep-04 0 3.88 17-Nov-04 0 4.1 16-Mar-OS 0 3.S 2S-May-OS <1 NA NA NA 3.7 NA 31-Aug-OS <1 <1 6.4 <1 3.S NA I-Dec-OS <1 <1 2.3 <1 3.3 NA 9-Mar-06 <1 <1 2.2 <1 3.3 26 14-Jun-06 <1 <1 <1 <1 3.2 26 20-Jul-06 <1 <1 1.6 <1 2.9 26 8-Nov-06 <1 <1 <1 <1 1.S 23 28-Feb-07 <1 <1 <1 <1 3.1 22 27-Jun-07 <1 <1 <1 <1 3.3 23 IS-Aug-07 <1 <1 <1 <1 3.1 24 10-0ct-07 <1 <1 <1 <1 2.8 27 26-Mar-08 <1 <1 <1 <1 2.8 21 2S-Jun-08 <1 <1 <1 <1 2.8S 19 10-Sep-08 <1 <1 <1 <1 2.66 19 IS-0ct-08 <1 <1 <1 <1 2.63 22 4-Mar-09 <1 <1 <1 <1 2.S 21 24-Jun-09 <1 <1 <1 <1 2.9 20 16-Dec-09 <1 <1 <1 <1 2.5 22 23-Feb-1O <1 <1 <1 <1 2.8 23 8-Jun-10 <1 <1 <1 <1 3 24 lO-Aug-lO <1 <1 <1 <1 3.1 22 5-0ct-1O <1 <1 <1 <1 3.3 26 15-Feb-11 ND ND ND ND 3.5 23 25-May-11 ND ND ND ND 3.7 23 16-Aug-ll ND ND ND ND 4 23 . '.' . FofoF~W; I~I ' • I~ U etliane 1,1< .' ,j ,ra ~. ;~~~~'¥I~'@O~~'~~:~~~:r\~/N:'len~ W~ . Ill , ry . . cl l~lFetIr~chlolll,(I~K~'. . ') t, Chlorn'le. Zi, '1 (m ' I':,. :.r.'~;.h'." ,,~, . '~l,;.\1.~;;'1!'I~il ,~r~tiilIJ)r4P :~:~. ,M'~i' ;'\It,~~" ,,/!(t~~~'1 ;fl\7 ,~;,' ,'Iii Ii" '. 6-Jun-00 0 2-Sep-00 0 28-Nov-00 3,9 28-Mar-01 2260 1.02 20-Jun-01 3100 14,S 20-Sep-01 3200 14 8-Nov-01 2900 14,8 26-Mar-02 3400 IS 22-May-02 3200 13,2 12-Sep-02 4000 13.4 24-Nov-02 3800 12,6 28-Mar-03 3300 13.4 23-Jun-03 3600 12,8 12-Sep-03 2900 12,3 8-Nov-03 3S00 12,3 29-Mar-04 3200 12.2 22-Jun-04 3S00 12,1 17-Sep-04 3100 11,1 17-Nov-04 3600 10,8 16-Mar-OS 3100 11.6 2S-May-OS 2400 NA NA NA 11.3 NA 31-Aug-OS 3200 <10 <10 <10 9,9 NA I-Dee-OS 2800 <SO <SO <SO 10.2 NA 9-Mar-06 2900 <SO <SO <SO 9.S Sl 14-Jun-06 2600 <SO <SO <SO 8.6 48 20-Jul-06 28S0 <SO <SO <SO 9.7 SO 8-Nov-06 2670 1.7 <1 <1 10.1 49 28-Feb-07 2200 1.S <1 <1 9 49 27-Jun-07 2400 1.7 <1 <1 9.4 47 lS-Aug-07 2700 1.S <1 <1 9.S 4S 1O-Oet-07 2S00 1.S <1 <1 9.S 47 26-Mar-08 2800 1.6 <1 <1 9.2 43 2S-Jun-08 2S00 1.S <1 <1 10.8 42 10-Sep-08 2200 1.4 <1 <1 8.83 39 lS-0et-08 2S00 2 <2 <2 10.1 44 4-Mar-09 2200 1.2 <1 <1 10.2 37 24-Jun-09 1800 1.2 <1 <1 8,2 34 lS-Sep-09 2000 1.1 <1 <1 8.4 39 29-Dee-09 9S0 1.1 <1 <1 7,6 41 I~~i~~~'/" ~ ~.m~o~"'~'tl. ~~ty_ ''ifW4 5 -.11,11',((;; ,0fOFnl::r . "IiI • d 100comethane hI· o~ld~ 'I • ~ Ii', ~~ 't!' etrac 01'1 e ti Olu ., 'm' \' I' ., . rf . ,!Ql~ lit, I ,,;~ ,~;\\\:imt(\;~~~~f~lf . g,,~~jfi' I I " I/~~~f~ . 20-Dec-99 29.5 15-Mar-00 49.0 2-Sep-00 124 29-Nov-00 255 28-Mar-Ol 236 20-Jun-Ol 240 20-Sep-Ol 240 7-Nov-Ol 260 26-Mar-02 260 22-May-02 300 12-Sep-02 330 24-Nov-02 260 28-Mar-03 240 23-Jun-03 290 12-Sep-03 200 8-Nov-03 240 29-Mar-04 210 22-Jun-04 200 17-Sep-04 150 17-Nov-04 180 16-Mar-05 120 25-May-05 113 NA NA NA 3.7 NA 31-Aug-05 82.0 <2.5 5.8 <2.5 6 NA I-Dec-05 63.0 <2.5 2.5 <2.5 6 NA 9-Mar-06 66.0 <2.5 3.1 <2.5 6 52 14-Jun-06 51.0 <1 <2.5 <2.5 5.9 51 20-Jul-06 53.7 <1 <1 <1 6.7 54 8-Nov-06 47.1 <1 <1 <1 2.9 55 28-Feb-07 33.0 <1 <1 <1 7.8 57 27-Jun-07 26.0 <1 <1 <1 7 45 15-Aug-07 9.2 <1 <1 <1 7.7 38 10-0ct-07 9.4 <1 <1 <1 8.2 39 26-Mar-08 11.0 <1 <1 <1 7.4 36 25-Jun-08 9.3 <1 <1 <1 8.7 37 10-Sep-08 11.0 <1 <1 <1 7.91 34 15-0ct-08 10.0 <1 <1 <1 9.3 37 4-Mar-09 12.0 <1 <1 <1 7.9 34 24-Jun-09 13.0 <1 <1 <1 7.5 37 15-Sep-09 12.0 <1 <1 <1 8.3 48 13.0 <1 <1 <1 6.8 43 9-Jun-1O 12.0 <1 <1 <1 7.1 28 ll-Aug-lO 12.0 <1 <1 <1 7 38 13-0ct-1O 11.0 <1 <1 <1 7.2 41 22-Feb-ll 10.0 ND ND ND 7 34 26-May-11 9.0 ND ND ND 7.2 35 17-Aug-ll 10.0 ND ND ND 7.5 37 ~~'" ~l "'.1: ~,! ' !I ,,' €~t;I;on I;, ... ;~~~'.. ~~~;"~ '}!',-:;', ~,,, , . y. eth~lene T;W4'~ t!. (8h~:o,f.~l1~ ,~ " Il i,;i&\~~~ethane I ' 'a ,ate 1~:OftlbrJde\~ Tetl1 r,i(le I "I I' ';~1:! 0111 e .' , Ill , ( glD' !) "",iI' !Ij ,~I:~ (\tM"G ,:~~~'~.'j ~,.j~, • ,~, , I~~,'~,,~~ :', U~9;~'i[' , ~~tisIl, "dW~ 6-Jun-00 0 2-Sep-00 0 28-Nov-00 0 ND 26-Mar-Ol 0 0,13 20-Jun-Ol 0 ND 20-Sep-Ol 4 ND 7-Nov-Ol 1 ND 26-Mar-02 0 ND 21-May-02 0 ND 12-Sep-02 0 ND 24-Nov-02 0 ND 28-Mar-03 0 0.1 23-Jun-03 0 ND 12-Sep-03 0 ND 8-Nov-03 0 ND 29-Mar-04 0 ND 22-Jun-04 0 ND 17-Sep-04 0 ND 17-Nov-04 0 ND 16-Mar-05 0 0,2 25-May-05 2.5 NA NA NA 0,4 NA 31-Aug-05 10,0 <1 2.8 <1 0.8 NA I-Dec-05 17.0 <1 1.3 <1 0.9 NA 9-Mar-06 31.0 <1 <1 <1 1.2 31 14-Jun-06 19.0 <1 <1 <1 1 30 20-Ju1-06 11.0 <1 <1 <1 0.6 37 8-Nov-06 42.8 <1 <1 <1 1,4 65 28-Feb-07 46.0 <1 <1 <1 1.5 32 27-Jun-07 11.0 <1 <1 <1 0.6 38 15-Aug-07 18.0 <1 <1 <1 0.7 36 1O-0ct-07 18.0 <1 <1 <1 0.8 38 26-Mar-08 52.0 <1 <1 <1 1.1 33 25-Jun-08 24.0 <1 <1 <1 0.9 35 10-Sep-08 39.0 <1 <1 <1 1.14 35 15-0ct-08 37.0 <1 <1 <1 1.01 33 I1-Mar-09 81.0 <1 <1 <1 2.2 35 24-Jun-09 120 <1 <1 <1 2.7 37 15-Sep-09 280 <1 <1 <1 5.0 37 22-Dec-09 250 <1 <1 <1 6.1 41 25-Feb-1O 1000 <1 <1 <1 1.6 45 lO-Jun-lO 590 <1 <1 <1 2.5 33 12-Aug-1O 630 <1 <1 <1 3.9 31 13-0ct-1O 420 <1 <1 <1 4.3 41 23-Feb-ll 47 ND ND ND 0.7 40 ~!ii';' . tJhlorofol'm !" j' m'eth'ane ." «;Iil ' lor1di: ' e ' 01' ", • ' .1i \, " ~?I , ~ i',,~~~~,: , . ' g~&~! I 29-Nov-99 256 15-Mar-00 616 2-Sep-00 698 29-Nov-00 684 1.99 28-Mar-01 747 2.46 20-Jun-01 1100 2.65 20-Sep-01 1200 3.38 8-Nov-Ol 1100 2.5 26-Mar-02 1500 3.76 23-May-02 1600 3.89 12-Sep-02 1500 3.18 24-Nov-02 2300 4.6 28-Mar-03 1800 4.8 23-Jun-03 5200 7.6 12-Sep-03 3600 7.6 8-Nov-03 4500 7.1 29-Mar-04 2500 4.63 22-Jun-04 2900 4.83 17-Sep-04 3100 5.59 17-Nov-04 3800 6 16-Mar-05 3100 5.2 25-May-05 2700 NA NA NA 5.4 NA 31-Aug-05 3100 <10 <10 <10 5.2 NA I-Dec-05 2500 <50 <50 <50 5.3 NA 9-Mar-06 1900 <50 <50 <50 1 48 14-Jun-06 2200 <50 <50 <50 4.5 47 20-Jul-06 2140 <50 <50 <50 4.7 51 8-Nov-06 2160 1.5 <1 <1 4.6 49 28-Feb-07 1800 1.1 <1 <1 5 47 27-Jun-07 2600 1.5 <1 <1 5.1 45 14-Aug-07 2300 1.4 <1 <1 4.7 44 10-0ct-07 1900 1.2 <1 <1 4.7 45 26-Mar-08 2200 1.3 <1 <1 4.2 43 25-Jun-08 1800 1.3 <1 <1 4.8 43 10-Sep-08 1600 1.4 <1 <1 4.16 35 15-0ct-08 1900 <2 <2 <2 4.01 40 ll-Mar-09 1800 1.2 <1 <1 3.7 35 24-Jun-09 1400 <1 <1 <1 3.8 37 15-Sep-09 1500 1.0 <1 <1 4.1 37 ~"~J:;~r~M~~ W4 ' lor ·d 0 3 'C " , -I II e' . e · , ,~ugll) " ,~ . . ·'.l, !J , gn9 mgtJ~ ·.il "' ., "q~' "~l,." 0/), 1",:\i~/'(\uWI~, -1l®! ,.;~ ~ ')rt1i';J 11\. (lll;gZi~jj. "I ;'),'ir ~,pf'~t?~ 29-Nov-99 0 15-Mar-00 21.8 2-Sep-00 102 29-Nov-00 107 ND 26-Mar-01 116 ND 20-Jun-01 180 ND 20-Sep-01 180 0.35 7-Nov-01 180 ND 26-Mar-02 190 0.62 22-May-02 210 0.77 12-Sep-02 300 ND 24-Nov-02 450 ND 28-Mar-03 320 0.8 23-Jun-03 420 ND 12-Sep-03 66.0 ND 8-Nov-03 21.0 0.1 29-Mar-04 24.0 0.65 22-Jun-04 110 0.52 17-Sep-04 120 ND 17-Noy-04 120 ND 16-Mar-05 10.0 ND 25-May-05 <1 NA NA NA 0.2 NA 31-Aug-05 1.1 <1 1.7 <1 <0.1 NA 30-Noy-05 <1 <1 <1 <1 <0.1 NA 9-Mar-06 1.3 <1 2.1 <1 0.3 39 14-Jun-06 1.0 <1 1.8 <1 <0.1 37 20-Jul-06 <1 <1 <1 <1 0.1 39 8-Noy-06 <1 <1 <1 <1 <0.1 40 28-Feb-07 2.5 <1 <1 <1 0.7 39 27-Jun-07 2.5 <1 <1 <1 0.2 42 15-Aug-07 1.5 <1 <1 <1 <0.1 42 1O-0ct-07 3.5 <1 <1 <1 0.5 43 26-Mar-08 <1 <1 <1 <1 0.1 46 25-Jun-08 <1 <1 <1 <1 <0.05 45 10-Sep-08 <1 <1 <1 <1 <0.05 39 15-0ct-08 <1 <1 <1 <1 <0.05 44 4-Mar-09 <1 <1 <1 <1 <0.1 42 24-Jun-09 <1 <1 <1 <1 <0.1 44 15-Sep-09 <1 <1 <1 <1 <1 44 <1 <1 <1 <0.1 57 9-Jun-1O <1 <1 <1 <1 <0.1 42 ll-Aug-lO <1 <1 <1 <1 <0.1 45 5-0ct-1O <1 <1 <1 <1 <0.1 46 16-Feb-ll ND ND ND ND ND 52 25-May-ll ND ND ND ND 0.1 45 16-Aug-ll ND ND ND ND 0.1 46 ~,~~r:~~~I~~d rlttt~i60~;'.'.>">" lWeifi'-. Im'~~1!4!~ :filii .. .. 0\10:;J~~ '''If iii' 'a IIOmel& Ii' Jj!il~~ .; .' ., e1!r,ae OPl e· ,. "I~ ( " @.~¥j , .. i U ',iii." U ~ m , ~uiffl,)· ';~;"r{ jljj< 1\ Ll!;I,Y;j,~§i'~qgil'~ii',r"Jtl . ~j~.~ '~U " ,~~\;;;, ",''.i "', \\ll";~ 20-Dee-99 4.2 15-Mar-00 1.9 2-Sep-00 14.2 29-Nov-00 39.4 ND 27-Mar-Ol 43.6 ND 20-Jun-Ol 59.0 0.15 20-Sep-Ol 19.0 0.4 7-Nov-Ol 49.0 0.1 26-Mar-02 41.0 0.5 22-May-02 38.0 0.65 12-Sep-02 49.0 0.2 24-Nov-02 51.0 0.6 28-Mar-03 34.0 0.6 23-Jun-03 33.0 0.8 12-Sep-03 32.0 1.1 8-Nov-03 46.0 1.1 29-Mar-04 48.0 0.82 22-Jun-04 48.0 0.75 17-Sep-04 39.0 0.81 17-Nov-04 26.0 1.2 16-Mar-05 3.8 1.3 25-May-05 1.2 NA NA NA 1.3 NA 31 -Aug-05 <1 <1 2.9 <1 1.3 NA I-Dee-05 <1 <1 <1 <1 1.3 NA 9-Mar-06 <1 <1 2.6 <1 1.5 38 14-Jun-06 <1 <1 2.7 <1 1.5 39 20-Jul-06 <1 <1 <1 <1 0.9 41 8-Nov-06 <1 <1 <1 <1 0.7 44 28-Feb-07 <1 <1 <1 <1 0.6 44 27-Jun-07 21 <1 <1 <1 1.3 42 15-Aug-07 9.5 <1 <1 <1 1.8 38 10-0et-07 8.7 <1 <1 <1 2 40 26-Mar-08 1.3 <1 <1 <1 2.1 35 25-Jun-08 1.0 <1 <1 <1 2.3 35 10-Sep-08 <1 <1 <1 <1 2.79 28 15-0et-08 <1 <1 <1 <1 1.99 58 4-Mar-09 <1 <1 <1 <1 2.5 30 24-Jun-09 <1 <1 <1 <1 2.3 30 15-Sep-09 <1 <1 <1 <1 2.5 30 lilt· ' u, '1r~" • '. "';~.ilI\oJl\' ~ ,',' ~~ M.~~~!' ,,; '\<i,' .~C' fP, 1rW4' ~O N C1110 . ,ffi" 'r.r ' '&llll ,it I 'lhrometllane-Pl1ill'G:lk Nittlate:" lClllovide.' ". " , . ~1i,g7,!! I" I • '~ug/.l) '~'~ 1 ~mg4", ~m~1) , ~\'i" ,,-:~i"'fi! ~ ,*', eti,ac om e "" 0 ,v. ''.;~i: ,.ill: fJr~~".if~Ii' " ;,~ k'; .. ,f.t:~~i;" ~!~b: 1~~'",~:tIYi\( U:gtt~!.'I!!, ' :I~~t " ',1~, "~iJ, ;J';, ' -t~1 , ,"ii'" ~'~.illf><I""" '!;II',; ,,.;.1 21-Jan-02 14 26-Mar-02 16 0.14 21-May-02 17 0.11 12-Sep-02 6 ND 24-Nov-02 14 ND 28-Mar-03 29 0.2 23-Jun-03 110 0.4 12-Sep-03 74 0.4 8-Nov-03 75 0.3 29-Mar-04 22 0.1 22-Jun-04 32 ND 17-Sep-04 63 0.46 17-Nov-04 120 0.4 16-Mar-05 140 1.6 25-May-05 62.4 NA NA NA 0.8 NA 31-Aug-05 110 <2.5 6.2 <2.5 1.1 NA 1-Dec-05 300 <2.5 <2.5 <2.5 3.3 NA 9-Mar-06 190 <5 <50 <50 2.4 50 14-Jun-06 300 <5 <50 <50 3.5 54 20-Jul-06 504 <5 <50 <50 6.8 61 8-Nov-06 452 <1 1.6 1 5.7 58 28-Feb-07 500 <1 <1 1 7.6 62 27-Jun-07 350 <1 <1 1 5.1 54 15-Aug-07 660 <1 <1 1 7.3 59 10-0ct-07 470 <1 <1 1 6.7 59 26-Mar-08 620 <1 <1 1 7.3 55 25-Jun-08 720 <1 <1 1 9.91 58 10-Sep-08 680 <1 <1 1 9.23 51 15-0ct-08 1200 <2 <2 2 10.5 61 11-Mar-09 1100 <1 <1 1 11.6 64 24-Jun-09 1200 <1 <1 1 9.8 62 15-Sep-09 910 <1 <1 1 8.1 51 22-Dec-09 300 <1 <1 <1 3.5 51 3-Mar-1O 460 <1 <1 <1 5 49 lO-Jun-lO 220 <1 <1 <1 1.6 42 12-Aug-1O 100 <1 <1 <1 0.8 38 13-0ct-l0 1100 <1 <1 <1 11 52 23-Feb-11 620 ND ND ND 9 62 I-Jun-11 280 ND ND ND 3.3 42 17-Aug-ll 180 ND ND ND 1.9 41 17-Aug-ll 820 ND ND ND 7.1 48 f~ ~;~~ ~,,~~>,),~.~a~6o~]lr'~·'·-~r~e1~11r tff '" , 1'W4 ' j ,p hlollOf ... n\\ "iI1 i 'hi ' "d romelh Dhl I IIf1lr2ijj [l810nl\' . , " . e raG OF) e I .I . . . * , . I €uwH;~~~ , ~~,~ lw~ i'~ugtl9 I '/ ~Ii1~~' g!tl~ rt11 1.;41,,', .'i1l};t :!, .~;}·fJ;: .1,.~'~l" ;", ~u: " ~i~~ i I ,,; . I '" w' . ~u 1, . '!l'\;~~~ij .. . ., fit " ,I 12-Sep-02 2 2,S4 24-Nov-02 0 2.2 28-Mar-03 0 1.9 23-Jun-03 0 1.8 12-Sep-03 0 1.8 9-Nov-03 0 1.6 29-Mar-04 0 1.S8 22-Jun-04 0 1.4 17-Sep-04 0 1.24 17-Nov-04 0 1.S 16-Mar-OS 0 1.4 2S-May-OS <1 NA NA NA 1.6 NA 31-Aug-OS <1 <1 S.8 <1 1.S NA I-Dee-OS <1 <1 1.9 <2 1.4 NA 9-Mar-06 <1 <1 2.6 <1 1.3 19 14-Jun-06 <1 <1 1.4 <1 1.4 16 20-Jul-06 <1 <1 <1 <1 1.4 16 8-Nov-06 <1 <1 <1 <1 1.4 16 28-Feb-07 <1 <1 <1 <1 1.S 16 27-Jun-07 <1 <1 <1 <1 I,S 18 IS-Aug-07 <1 <1 <1 <1 1.4 29 1O-Oet-07 <1 <1 <1 <1 1.4 16 26-Mar-08 <1 <1 <1 <1 1.6 16 2S-Jun-08 <1 <1 <1 <1 2.69 19 10-Sep-08 <1 <1 <1 <1 2.6S 18 IS-0et-08 <1 <1 <1 <1 2.47 22 4-Mar-09 <1 <1 <1 <1 2.4 23 24-Jun-09 <1 <1 <1 <1 3.8 22 IS-Sep-09 <1 <1 <1 <1 S.1 22 16-Dee-09 <1 <1 <I <I 3.6 23 23-Feb-1O <I <1 <1 <1 4 22 8-Jun-1O <I <1 <1 <I 11 29 lO-Aug-lO <I <1 <1 <I 9 3S S-Oet-lO <1 <1 <1 <I 8 31 IS-Feb-II ND ND ND ND 6.S 31 2S-May-l1 ND ND ND ND 7 32 16-Aug-11 ND ND ND ND 6.8 31 1~~~Vlilrfif,'r,,~ ",~~1'~,,~> I~NI~ifelt. ~'. ~ •. , 'W oof. . hi • d '~ (. CliIorom~!;~e "~~~i' Ie €hlomde . , -ac OFl e ' . , • ' . 1:1 m e' If' ", ~ifAif' .', J :W' ~/ • ,~UgtIl :,,~ , il):' . 9 "·I~'1lQm~~ .,,, .. ,11, ,O'!N~ '4f I ~~~. . 1I11 ,'\ ff,.' ,,'r.,Iii;~J~I»;: 12-Sep-02 3 ND 24-Nov-02 0 ND 28-Mar-03 0 0.1 23-Jun-03 7800 14.5 15-Aug-03 7400 16.8 12-Sep-03 2500 2.7 25-Sep-03 2600 2.5 29-0ct-03 3100 3.1 8-Nov-03 3000 2.8 29-Mar-04 NA NA 22-Jun-04 NA NA 17-Sep-04 1400 0.53 17-Nov-04 300 0.2 16-Mar-05 310 0,3 30-Mar-05 230 0.2 25-May-05 442 NA NA NA 0.2 NA 31-Aug-05 960 <5 5.4 <5 0.2 NA I-Dec-05 1000 <50 <50 <50 0.3 NA 9-Mar-06 1100 <50 <50 <50 0.2 52 14-Jun-06 830 <50 <50 <50 0.2 52 20-Jul-06 2170 <50 <50 <50 1.4 65 8-Nov-06 282 <1 <1 2.8 0.3 54 28-Feb-07 570 <1 <1 5.5 0,5 56 27-Jun-07 300 <1 <1 13 0.4 49 15-Aug-07 1400 <1 <1 36 1 57 10-0ct-07 2000 <1 <1 14 0.6 57 26-Mar-08 930 <1 <1 40 0.1 49 25-Jun-08 1300 <1 <1 53 0.56 57 10-Sep-08 630 <1 <1 24 0.24 44 15-0ct-08 1700 <1 <1 100 0.65 64 4-Mar-09 950 <1 <1 51 0.4 49 24-Jun-09 410 <1 <1 12 0.2 48 15-Sep-09 850 <1 <1 30 0.1 46 14-Dec-09 1100 <1 <1 40 2.3 60 17-Feb-1O 780 <1 <1 19 0.2 57 9-Jun-1O 1900 <1 <1 28 1.1 58 16-Aug-1O 2200 <1 <1 21 0.6 49 ll-Oct-lO 970 <1 <1 6.5 0.7 65 23-Feb-11 450 ND ND 3.6 0.5 57 31-May-ll 1800 ND ND 1.3 0.4 88 17-Aug-ll 720 ND ND 7.2 0.9 58 I'~~'_~t ~';'~' r Me~,) y " 'met . <31110 . 1l:W tli3€lllovide H II) lilo ( I'~t" !,u ' ')li!~;\!\V~[\ g , '~~ m ,,'~if";~,,'" "),~~ , ',~, !'iil' ':\ 1~,lif!: ' llU, Ill " ,,.~~ , 12-Sep-02 140 ND 24-Nov-02 200 ND 28-Mar-03 260 ND 23-Jun-03 370 ND 12-Sep-03 350 ND 8-Nov-03 400 ND 29-Mar-04 430 ND 22-Jun-04 530 ND 17-Sep-04 400 ND 17-Nov-04 350 ND 16-Mar-05 240 ND 25-May-05 212 NA NA NA <0.1 NA 31-Aug-05 85 <1 3.2 43 <0.1 NA I-Dec-05 14 <2.5 2.6 5.9 1.4 NA 9-Mar-06 39.0 <1 1.1 21 3 60 14-Jun-06 13.0 <1 2.4 8.9 1.9 55 20-Jul-06 5.2 <1 <1 2.7 2.7 60 8-Nov-06 13.6 <1 <1 9.2 5.6 62 28-Feb-07 8.7 <1 <1 6.5 12.3 79 27-Jun-07 2.6 <1 <1 1.8 9.9 75 15-Aug-07 7.1 <1 <1 5.1 5.4 66 10-0ct-07 1.4 <1 <1 <1 4.4 69 26-Mar-08 11.0 <1 <1 26 ND 52 25-Jun-08 <1 <1 <1 <1 1.46 58 10-Sep-08 10 <1 <1 14 10.5 71 15-0ct-08 3.9 <1 <1 6.6 9.82 89 4-Mar-09 <1 <1 <1 <1 9.6 78 24-Jun-09 <1 <1 <1 <1 8.9 76 15-Sep-09 <1 <1 <1 <1 8.8 79 17-Dec-09 <1 <1 <1 <1 5.2 76 24-Feb-1O <1 <1 <1 <1 4.2 77 9-Jun-1O 2.1 <1 <1 <1 4.7 64 24-Aug-1O 4.3 <1 <1 <1 4.6 72 6-0ct-1O 3.0 <1 <1 <1 3.3 72 22-Feb-11 15.0 ND ND ND 7 86 26-May-ll 16.0 ND ND ND 5 81 17-Aug-ll 9.2 ND ND ND 1.7 63 I~l , ~i~~ '1~1j ,~f'~~n .,''' r ,:,' j\'f ,:"~; rMell\y.i;nef~ ~i'l~t·,' I TIW4 (21110 if t hi "(I hloFome~~ane",' om "(I ;~l 'NI ' ~mo ,-'c' lyi:F e raG 0111 e ~ gf,l,~ 'i~' d~~ e I j ~ ( ~~~ , t " ' , U ! ' ',,' lIn , 'm, ~ I/!'{;:~,j: ";'~'!r t~~,}, ",j";1!!,~;~iQ1Jl!m!~i~~ , .. 'k 1,1t~~",,.,,~1 ::\oA ,~1,~,,~1 .. ~,'n'; ~~~'~'~: .. , 12-Sep-02 440 1.49 24-Nov-02 240 13.3 28-Mar-03 160 13.1 23-Jun-03 110 19 12-Sep-03 68.0 19.9 9-Nov-03 84.0 20.7 29-Mar-04 90.0 14 22-Jun-04 82.0 12.2 17-Sep-04 38.0 14.5 17-Nov-04 51.0 17.3 16-Mar-05 38.0 14.1 25-May-05 29.8 NA NA NA 12.9 NA 31-Aug-05 39 <1 2.8 <1 13.3 NA I-Dec-05 14 <1 1.1 <1 7.3 NA 9-Mar-06 12.0 <1 1.1 <1 5.9 5.9 14-Jun-06 12.0 <1 1.6 <1 4.7 35 20-Jul-06 10.8 <1 2.7 <1 6.1 35 8-Nov-06 139 <1 <1 <1 8.7 34 28-Feb-07 9.2 <1 <1 <1 5.1 30 27-Jun-07 8.0 <1 <1 <1 4.9 28 15-Aug-07 8.9 <1 <1 <1 5 32 10-0ct-07 7.4 <1 <1 <1 4.4 27 26-Mar-08 6.4 <1 <1 <1 0.7 23 25-Jun-08 5.7 <1 <1 <1 4.55 23 10-Sep-08 8.0 <1 <1 <1 4.68 26 15-0ct-08 9.4 <1 <1 <1 5,15 30 4-Mar-09 11.0 <1 <1 <1 5.2 29 24-Jun-09 16.0 <1 <1 <1 6.2 30 15-Sep-09 13.0 <1 <1 <1 5.9 26 22-Dec-09 8.2 <1 <1 <1 5.4 30 24-Feb-1O 69.0 <1 <1 <1 5.1 41 9-Jun-l0 29.0 <1 <1 <1 9 35 12-Aug-1O 29.0 <1 <1 <1 9 37 13-0ct-1O 30.0 <1 <1 <1 10 50 22-Feb-11 39.0 ND ND ND 10 52 26-May-l1 26.0 ND ND ND 9 36 17-Aug-11 29.0 ND ND ND 4.6 23 ll-Oct-lO 1200 1.3 <1 <1 2.7 146 17-Feb-ll 3400 17 ND ND 17 135 7-Jun-ll 4000 8.3 ND ND 12 148 17-Aug-ll 970 2.1 ND ND 3 148 I~U 1 ~'f\ ,,;~,,~, ,:~ I~()~I~~~;~~ i~i. ~ta~bon' " ,roW:';/m, I ':I,' ~ ,"", , 1;)~~etli~leqe~'~1 '~r ~ 1-,,' ~,~;l!t~th.n:., 11~~itp 'Ollioliide I';, lFW4-2Q fJ 1 .. ;Tetra~hlori<Ie\~ , 0h1OlriGe :":~~ I I;i!~mgtl);~ :s,,~;{, flJ' ~ .'~ Ir~~1 ,~U~~, ,:,~ Ii ~ ug(l~ I , 11(c~ "I!'\~u~n~!c'~ lV.' , " 'ilf Z~f~'i ~~'!,WI!((\.rgtIi5):i ~"!i:'il II~~} "' ,k11 :~~k:,'~11 i~~~ " ")ri.i'I' ,i" 25-May-05 39000 NA NA NA 10.1 NA 31-Aug-05 3800 <10 <10 <10 2.9 NA I-Dee-05 19000 <250 <250 <250 1.8 NA 9-Mar-06 9200 <500 <500 <500 3.8 120 14-Jun-06 61000 <500 <500 <500 9.4 235 20-Jul-06 5300 <1000 <1000 <1000 2.9 134 8-Nov-06 11000 7.1 1.9 2.2 3.5 124 28-Feb-07 4400 3.1 <1 1.1 4.2 124 27-Jun-07 1800 2.2 <1 <1 2.3 112 15-Aug-07 5200 3.5 <1 1.8 2.1 117 1O-0et-07 9000 6.8 <1 1.9 5.6 170 26-Mar-08 13000 9 <1 1.5 0.9 132 25-Jun-08 30000 13 <1 1.2 7.96 191 10-Sep-08 21000 15 <1 3.7 4.44 156 15-0et-08 NA NA NA NA 5.51 166 4-Mar-09 8200 5.7 <1 5.2 5.1 164 24-Jun-09 6800 4.9 <2 4.2 2.9 164 15-Sep-09 13000 8.4 <2 4.4 3.3 153 14-Dee-09 15000 14 <1 3 5.3 187 17-Feb-1O 3500 2.7 <1 3.2 2 179 14-Jun-1O 18000 11 <1 3.7 5.6 200 16-Aug-1O 15000 12 <1 2.2 5.3 196 11-0et-1O 24000 20 <1 5.5 4.6 203 23-Feb-l1 31000 27 ND 19 4.4 220 I-Jun-11 8100 10 ND 2.1 4.8 177 17-Aug-11 6800 7.3 ND 3.1 6.5 207 ~,*'.trb~n~·I ·II'·~; M"~~~.~~ , e y: e . ' I ; .,' , M" FoE . 'l t'r. 'hi . d J:Tomet ~(Jhlor,i l(.Q~ldm(;J~: ( " e ~~!M~rI, ~j ~ • 1). ~ \ll , . .' , "H., ~m~~~~ ,I.., '. I." ~~;",.{il ' , ) . j!):.1" ',." , . ' )t~Jl "I' .' " f,YI/ ; -ii'i.~~\'i: I , 25-May-05 192 NA NA NA 14.6 NA 31-Aug-05 78 <5 <5 <5 10.1 NA I-Dec-05 86 <1 1.0 <1 9.6 NA 9-Mar-06 120 <2.5 <2.5 <2.5 8.5 347 14-Juo-06 130 <2.5 <2.5 <2.5 10.2 318 20-Jul-06 106 <2.5 <2.5 <2.5 8.9 357 8-Nov-06 139 2 <1 <1 8.7 296 28-Feb-07 160 1.8 <1 <1 8.7 306 27-Juo-07 300 5.8 <1 <1 8.6 327 15-Aug-07 140 <1 <1 <1 8.6 300 10-0ct-07 120 <1 <1 <1 8.3 288 26-Mar-08 380 7 <1 <1 14.3 331 25-Juo-08 160 1.7 <1 <1 8.81 271 10-Sep-08 120 1.6 <1 <1 7.57 244 15-0ct-08 170 2 <1 <2 8.00 284 I1-Mar-09 180 <1 <1 <1 8.3 279 24-Juo-09 200 <1 <1 <1 8.1 291 15-Sep-09 140 <1 <1 <1 9.2 281 22-Dec-09 160 <1 <1 <1 8.4 256 25-Feb-1D 170 <1 <1 <1 8.4 228 lD-Juo-lD 210 1.2 <1 <1 12 266 12-Aug-1D 390 9.2 <1 <1 14 278 13-0ct-1D 200 1.2 <1 <1 7 210 22-Feb-11 230 1.2 ND ND 9 303 28-Juo-l1 290 4.8 ND ND 12 290 17-Aug-l1 460 6.3 ND ND 14 287 ~~'~j'.M:~' ... "J .... rVhtJi".'''' • ~"i 'f~~~J . " ,'. . ," , , "e ~ ene I;:~~' '~hloFofpFml ", ChlOJ1Ometb '. , . I 'd i l:ll~Nitnlte" ,. I 111 ' lt~~~~~~ '. QIi' e ?, 4t 1j ,l, -~l\~';;: . ,,~ I.~t' ~ '~~I1~IJl\~~i,~1 :~;¥ ~.1 I i ~ f ; , (1 P ~~ , I;': :~i! \ J .T" '. 25-May-05 340 NA NA NA 18.2 NA 31-Aug-05 290 <5 <5 <5 15.7 NA I-Dec-05 320 <5 <5 <5 15.1 NA 9-Mar-06 390 <10 <10 <10 15.3 236 14-Jun-06 280 <10 <10 <10 14.3 221 20-Jul-06 864 <10 <10 <10 14.5 221 8-Nov-06 350 <1 1.6 <1 15.9 236 28-Feb-07 440 <1 <1 <1 20.9 347 27-Jun-07 740 <1 <1 <1 19.3 273 15-Aug-07 530 <1 <1 <1 19.3 259 10-0ct-07 440 <1 <1 <1 18.8 238 26-Mar-08 1400 <1 <1 <1 39.1 519 25-Jun-08 1200 <1 <1 <1 41.9 271 10-Sep-08 6300 1.3 <1 <1 38.7 524 15-0ct-08 630 <2 <2 <2 36.3 539 11-Mar-09 390 <1 <1 <1 20.7 177 24-Jun-09 730 <1 <1 <1 20.6 177 15-Sep-09 2300 <1 <1 <1 40.3 391 29-Dec-09 380 <1 <1 <1 17 .8 175 3-Mar-1O 2200 <1 <1 <1 36.6 427 15-Jun-1O 540 <1 <1 <1 19 134 24-Aug-1O 340 <1 <1 <1 15 130 13-0ct-1O 340 <1 <1 <1 16 134 23-Feb-11 1300 ND ND ND 18 114 1-Jun-ll 210 ND ND ND 17 138 17-Aug-11 450 ND ND ND 15 120 , ~~;~~~'i "':~1 ~ EhI . ,,,niJ.:' . r ethllenfJ ." . ,on ,. ~.. ~I:~rm,. l~ 1 V' ~ • ..• ~ . oForne . a . 1 • f I:~~l I ,~I.Oli~~tf 1:~:;fHl:' ~ ga~ hIOV~~I\'1 . 'i,~;")~' ! '~~llWJ9 ~' I~~~~ ~ , ~~~~ii~ 27-Jun-07 <1 <1 <1 <1 <0.1 47 15-Aug-07 <1 <1 <1 <1 <0.1 46 10-0ct-07 <1 <1 <1 <1 <0.1 43 26-Mar-08 <1 <1 <1 <1 <0.1 41 25-Jun-08 <1 <1 <1 <1 <0.05 41 10-Sep-08 <1 <1 <1 <1 <0.05 35 15-0ct-08 <2 <2 <2 <2 <0.05 51 4-Mar-09 <1 <1 <1 <1 <0.1 41 24-Jun-09 <1 <1 <1 <1 <0.1 43 15-Sep-09 <1 <1 <1 <1 <0.1 43 16-Dec-09 <1 <1 <1 <1 <0.1 37 24-Feb-1O <1 <1 <1 <1 <0.1 45 8-Jun-1O <1 <1 <1 <1 <0.1 40 lO-Aug-lO <1 <1 <1 <1 <0.1 40 5-0ct-1O <1 <1 <1 <1 <0.1 34 16-Feb-ll ND ND ND ND ND 44 25-May-11 ND ND ND ND ND 44 16-Aug-ll ND ND ND ND ND 41 2.2 <1 <1 29 791 1.5 <1 <1 <1 24.7 692 26-Mar-08 1.5 <1 <1 <1 24.4 740 25-Jun-08 1.4 <1 <1 <1 45.3 834 10-Sep-08 2.9 <1 <1 <1 38.4 1180 15-0ct-08 <2 <2 <2 <2 44.6 1130 4-Mar-09 1.4 <1 <1 <1 30.5 1010 24-Jun-09 1.5 <1 <1 <1 30.4 759 15-Sep-09 1.4 <1 <1 <1 30.7 618 17-Dec-09 1.2 <1 <1 <1 28.3 1080 25-Feb-1O 1.3 <1 <1 <1 33.1 896 9-Jun-1O 1.7 <1 <1 <1 30 639 24-Aug-1O 1.8 <1 <1 <1 31 587 6-0ct-1O 1.4 <1 <1 <1 31 522 17-Feb-ll 1.8 ND ND ND 31 1100 26-May-ll 1.1 ND ND ND 35 1110 17-Aug-ll 1.7 ND ND ND 34 967 TabL Chloroform Concentration Trend Graphs (ug/L) o o o I\.) o o o .j:>. o o o -..J o o o CJ1 o o o m o o o w o o o o Sep-99 +-----~----~------+-----~----~~--~~~--~ Dec-99 Mar-OO Jun-OO Sep-OO Dec-OO Mar-01 Jun-01 Sep-01 Dec-01 Mar-02 Jun-02 Sep-02 Dec-02 Mar-03 Jun-03 Sep-03 Dec-03 l __ -+_--t---t-~7 Mar-04 Jun-04 r--t----j~-_!-...~ Sep-04 Dec-04 Mar-05 Jun-05 Sep-05 Dec-05 Mar-06 Jun-06 Sep-06 Dec-06 Mar-O? Jun-O? Sep-O? Dec-O? Mar-08 Jun-08 Sep-08 Dec-08 Mar-09 Jun-09 Sep-09 Dec-09 Mar-10 Jun-10 Sep-10 Dec-10 Mar-11 Jun-11 ~ :E .J::>. I o ~ o ""'" o ....... o ""'" 3 ~ c CD CJ) tn Q) ::::J CU > E 10.. 0 -0 10.. .2 J: () ,.... I o::t 3: I- o ~-/\ON-8 ~ 6o-lnr-9 80-qe.::l-cc 90-l00-0~ 90-fi"eV\l-8c vo-uer-v~ co-des-~ 66-0eO-9 f---+----I---+----+---+----+----+ 86-lnr-vc o o o f'-. o o o <.0 o o o l!) o o o """ o o o C') o o o (\J o o o o TW4-2 Chloroform Values 7000 ~-------------------------------------------------------------------------------------------, 6000 +---------------------------.---------------------------------------------------------------~ 5000 +--------=~~~--_r~--~r_--r_~------------------------------------------------------~ 4000 +---------~~--~r_------------~1_--=-~~--~----~----------------------------------~ -....I a, :::I -3000 +-______ ~~--------------------------------------------~~~--~~~~~~~L-~~~--~ 2000 +------------------------------------------------------------4~------------~HL------------~ Data point represented corresponds 1000 to laboratory results. The value is likely underestimated due to laboratory error not considering the dilution factor of 10. 0 co (j) .,.... C\I oo;;t l!) <D co (j) 0 C\I (j) (j) 9 0 0 0 9 0 ~ .,.... .,.... , (, 6. C :>, .D > , "5 0.. t5 '- Cll Cll ctS ctS Cll ::J 0 0.. -, <t: 0 -, 4= .,;. 0 CJ? -, ~ LL I Z OJ I 6 <D C\I <b .,.... oo;;t ro N ro C\I C\I UI Q) ::l CU > E 10. 0 0 -0 10. .2 J: 0 M I "=t I ~ I- (1/6n) In Q) ::::J as > E 10. 0 -0 10. ..2 .r:. 0 o::t I o::t == I- o ~-AoN-8~ 60-lnr-9 80-Q8.:1-GG 90-PO-O~ so-keLl\l-8G VO-U1:W-V~ GO-d8S-~ 66-880-9 1---+---+--+---+---1----+---+--+----1-86-lnr-vG o o L{) """ o o o """ o o L{) CI) o o o CI) o o L{) C\J o o o C\J o o L{) o o o o o L{) o U) CI> :::l co > E "-0 -0 "-0 .c: 0 Lt) I o::t 3= I- ...------.,...---,-----"T""----,..---'----.,...---,..-----r G ~ -JdV-~ 0~-AON-8 ~ 60-lnr-9 80-q8.::1-GG 90-l00-0 ~ 90-k81/\1-8G VO-UBr-V~ GO-d8S-~ 66-080-9 I-----l----I---+----f----f----I----+ 86-lnr-vG o LO C<) o o C<) o LO C\J o o C\J o LO o o o LO o o I\) o o ~ o o (ug/L) (j) o o co o o o o o -'- I\) o o 07124/98 +I----I-----j-----j-----t----+-----j 12/06/99 04/19/01 09/01/02 + 01/14/04 l \ 05/28/05 " \ ~ \ 10/10106 02/22/08 07/06/09 11/18/10 04/01/12 .L ___ -..I. ____ '"-___ ....i-___ --'---:--__ --', ___ ----' -t :E ,J::Io I en 0 :::r 0' ., 0 -0 ., 3 < Q) I: CD en en G> ::::s ca > E J.. 0 -0 J.. .2 J: 0 ..... I 'I:t == I- O~-I\ON-8~ 60-lnr-9 80-q8::1-GG 90-PO-O~ 90-AB l/IJ-8G VO-UBr-V~ GO-d8S-~ 66-:::>80-9 1------+-----1-----+-----1-----+-----+ 86-lnr-vG o o o (0 o o o L{) o o o '<t o o o C') o o o C\I o o o o tn Q) ::::J C'CS > E ... 0 -0 ... .£! J: () CX) I 'II:t 3: I- . ....,....--,.--:....-..-.,.---.r-----,.--....,---,.....---,..----.-G ~ -JdV-l o ~ -l\oN-8 ~ 60-lnr-9 80-Q8.:l-GG 90-PO-O~ 90-keV\l-8G VO-UBr-V~ GO-d8S-~ 66-:::J80-9 I---+--+---I----I---\----!----I---+--+---+ 86-lnr-vG o o L() o L() "<t o o "<t o L() C') o o C') o L() C\J o o C\J (1/6n) o L() o o o L() o f/) Q) ::s ii > E "-0 -0 "-.Q J: 0 C') I o::t == t- ,...-----,------,----..,.--'--,-----,.------,-----..-c ~ -JdV-~ O~-AON-8 ~ 60-lnr-g 80-q8,:1-CG 9O-PO-O~ so-liell\l-8( 170-uer-17 ~ CO-d8S-~ 66-080-g 1----+----+----I----+----f-----+----1--86-lnr-17c o <.0 o Li) (1/6n) o CI) o C\J o o UJ Q) ::l C'CS > E lo. 0 -0 lo. .2 J: 0 0 ,.... 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CD C\I I 3: ~ o ~-J\ON-8 ~ 60-lnr-9 80-qa.:l-cc 90-l::JO-O~ 90-keV'J-8c 1-----+-----+--------4------1------1-VO-U1:W-V ~ o o L() C\J o o o C\J o o L() o o o o o L() o In Q) :::::I ctI > E "-0 -0 "-0 J: 0 (0 "'"" I o::t ~ I- .----r----~---__,__----r__---_.._---__._ G ~-Jd\f-~ 60-lnr-g 80-qe.:l -GG 9O-PO-O~ SO-ABlI\I-9G VO-UBr-v ~ GO-des-~ I----+-----!-----+----+-----+-----I-~O-Jd\f-6 ~ o o <D o o L() o o '<t o o (I') o o C\J o o o II) Q) ::s C'a > E ... 0 -0 ... ..2 J: 0 (\/ M I ~ :iE .....----r----.,----r---.:...--.---,----,---r----y----. G ~ -JdV-~ 60-lnr-9 80-qa.::l-GG 90-PO-O~ 90-ABV\I-8G L---+--~-+--t--t--I--I-l Go-das-~ I-------i------i----+---+---\----+-----!----t----I-W-JdV-6 ~ co c:i <.0 c:i (\J c:i o U) CI) ::::J C'CS > E ~ o '0 ~ .2 .c o co ,.... I ~ o o If) o If) "'" • o o "'" o If) C') o o C') ~ ~ o If) C\J o o C\J o If) J ~ Ii ~ ~ ~ r---....~ ~ ~ ~ I .. r D. l> o o o If) o o ~ -l\oN-B ~ 60-lnr-g BO-qa.:l-GG 90-PO-O~ so-kell'J-BG vo-uer-v~ Go-das-~ If) Q) ::::J C'O > E ... o '0 ... ..2 J: (,) 0) ,.... I ~ o o o 00 A V o o o I' ~ I-""'" ~ o o o CO o o o L{') +::: ~ I---r-- F: I.. -~ ~ --- ~ < 1-~ ~D ~ 1\ ~ ----- o o o C') o o o C\J o o o o ~-I\ON-B ~ 60-lnr-9 BO-qa::l-GG 90-PO-O~ 90-keV\l-BG VO-UBr-v~ o r------r-----r--~.-_r__--__,_---...,__---r_---__r G ~ -Jd\f-~ O~-AON-8~ 60-lnr-g In Q) ::::I ctI > E 80-qa.:l-GG ... 0 -0 ... .2 J: 0 0 C\I I o::t 3: 9O-loO-O~ I- VO-UBr-v~ 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 I"-<.0 l!) """ C') N (1/6n) 0 Q) ::::s m > E ~ 0 -0 ~ .2 .c () ,.... C\I I o::t 3: I- ,...----.--.-,----.---,-.:....-....,...-.-,----,---,.---,--.---y-G ~ ·Jd\f· ~ O~-AON-B ~ 60-lnr-9 Bo·qa,:l-GG 90-PO-O ~ so-keV\l-BG I----!----I----+----I---I---+---I----+----I-----I-PO-UBr-p ~ o o l!) o l!) ..r o o ..r o l!) C') o o C') o l!) (\J o o (\J o l!) o o o l!) o t/) Q) ::::J co > E ... 0 -0 ... .2 J: (,) N N I ~ == I- ,. o o o I'-- o o o CO o o o L{) o o o "<:t o o o C') (1/6n) l-\ ~I'- [) ..-: L------~ t.-----+:::::::::: t-----II Z, ~N o o o C\J o o o ~ ~ ~ O~-i\ON-8 ~ 60-lnr-g 80-qa:!-cc 90-PO-O~ so-lieV\l-8c vo-uer-v~ o o CI) ::::J CU > E Jo. o -o Jo. .2 J: () ('I) C\I I 'd' 3: I- ('t) C\I I oq- $ r c .- "'C Q) ....... U Q) ....... Q) "'C C Q) Q) .0 ....... 0 C (J) CO ..c E ~ 0 -0 ~ 0 -..c 0 o ~ ~ ~-unr o~-::>eo o ~-des o~-unr o ~ -JBVII 60-::>eo 60-deS 60-unr 60-JBVII 80-::>eo 80-deS 80-unr 80-JBVII Lo-::>eo Lo-des Lo-unr o o o o III Q) ::J !tI > E ... 0 -0 ... ..S! ..s:: U o::t N I o::t 3: I- ,-----.,------r-----..,-------,-----.-------.-------,-l"(:-JdV-1 LI) m __ ~ _______ ~ ______ . _____________ ~ ______ J __ _ LI) N ~ N LI) c:i (1/3n) n-das-p1 n-qa:l-9l 01-uer-ll 60-lnr-9 80-Jaa-81 -80-unr-1 LO-AON-P1 LO-JdV-8l 90-PO-01 o c:i tn Q) ::::J co > E ... o -o ... .2 J: () It) N • o::t 3: .... L() C\I I ~ $ l- e .- -c Q) +-' () Q) +-' Q) -c e Q) Q) ..c +-' 0 e en co ..c E !i.... 0 '+-0 !i.... 0 -..c 0 ~ ~ -unr o~-oeo o ~-des o~-unr o ~ -JBIt\I 60-0eO 60-deS 60-un r 60-JBIt\I 80-0eO 80-deS 80-unr 80-JBIt\I Lo-oeo LO-deS Lo-unr o o o o o (ug/I) Jun-10 Jul-10 Aug-10 Sep-10 Oct-10 Nov-1O -t :E .!::o I N C"I Dec-1O n :T 0" ... 0 -Jan-ll 0 ... 3 < III !: Feb-ll tD III Mar-ll Apr-ll May-ll Jun-ll Jul-ll Aug-ll TabM CSV Transmittal Letter Kathy Weinel From: Sent: To: Cc: Subject: Attachments: Dear Mr. Lundberg, Kathy Weinel Wednesday, October 19, 2011 12:29 PM 'rlundberg@utah.gov' Jo Ann Tischler; David Frydenlund; Jaime Massey Transmittal of CSV Files White Mesa Mill 2011 03 Chloroform Monitoring C11080835.CSV Attached to this e-mail is an electronic copy of laboratory results for chloroform monitoring conducted at the White Mesa Mill during the third quarter of 2011, in Comma Separated Value (CSV) format. Please contact me at 303-389-4134 if you have any questions on this transmittal. Yours Truly Kathy Weinel Denison Mines (USA) Corp. Quality Assurance Manager 1 TabN Disinfection Byproducts -Trihalmethanes '-~.-------------------0----- &m\e-"=-- Basic Information about Regulated Drinking Water Contaminants You are here: Water "Orinking Water" Drinking lI'iater Contaminants -Basic Information about Regulate<! Drinking Water Contaminants" Basic Information aCOlltOisinfeclion Byproducts in Drinking Water: Total Tn'halomeltt.ane5, HaloaceticAcids, Bromate, and Chlorite Basic Information about Disinfection Byproducts in Drinking Water: Total Trihalomethanes, Haloacetic Acids, Bromate, and Chlorite Share To protect drinking walerfrom disease--causing organisms, or pathogens, water suppliers often add a disinfectant. such as chlorine, to drinking water. However, GlSinfection practices can he ccmpffca!ecl because certain microbial pa!l:ogens, suc.~ as Cryptosporidium. are highly resis'.ant to Iladilional disinfection practices. Also, disinfectants themselves can react with naturaJ{y-oc.."tJrring materials In the water to form byprocucts, which may pose heglth risks. A major challell{le fOrwater suppliers is how to control and nrni! the risks from pathogens and alSinfeclion byprcdW.s. It is important to provide protection from pathogens 'liMe simultaneously minimizing health risks to !he popu/alion from disinfection byproducts. For more infcrmaGcn. see fact sheets on Pathogens and Indicators and Disinfectants. • 'J1J118f m.7infhd!oiJ I{vproolld, d'oe..~ EPA (~!lurare. hoVi 2r~ !hpv furmecf and wh?1 ,,!re h!!ir health ,.,{f2fti; in f!rtJL~JlO-'IIf!ter at ~-e:3 above 'hi! maximum ccnrnminanJ /evel? • 'Attlrlt.3t-""-EPN.:l drInHrio w:a!er fOOuintTcnll {er dmfr.fedion hyc~u~ • How willi know if disinfection bvorcducts are in my drinking waler? HoVl will disinfection byproducts be removed &urn mv drinking water? • How do I !earn more aboyt my drinl<jng waler? What disinfection byproducts does EPA regulate, how are they fanned, and what are their health effects in drinking WOlter at levels allove the maximum contaminant level? Disinfection Bypraduct (Chemical Abstract Service Registrl Number) Total Trihalomethanes Bromodichforomelhane (75-27-4) Bromofolm (l5-2$2j Dibromochloromethane (124-48-1) Chloroform (07-68-3j Haloac .. tic acids: Dich/oTOacelic acid (79-4U) Tricl1/oroace!ic acid (78-03-9) Chlorcacetic acid (l9-11-8j 8romoacelic acid(79..fJ8-3) Dibromoace/ic acid (IJ31-64-1j Bromate (1554145-4. Chlorite (7T51l-19-Z) How Is it ronne<i7 T n1tafomethanes occur when nawraily-occurring organic and inorganic materials in the water react wifil the disinfectants, chlorine and chloramine. Haloacetic acids occur when naturaJ~J-C"..curr",g organic and morganic materials in the waler react with tlte disinfectants, chlorine and chloramine. Bromate occurs when bromide in the water reacts wi'" the QlSinfectant. ozone. Health Effects Some people who drink water conlaining lotaillihaiomethanes in excess of !he Mel over many years could experience iiver, kidney, or central nervous system problems and increased risk of cancer. Some people wllo drink water containing haloacelic acids in excess of the MCl over many years may ha.e an increased risk of gelling cancer~ Some peopl .. who drink water containing bromate in excess of file Mel over many years may have an increased risk of getting cancer. Some infants and yOUllg children who drink water containing chlorite in excess of tile MCL could experience n .... rous system .ifeels.. Chlon1e occurs when chlorine dioxide breaks down.. Sirru1ar effects may occur in fetuses of pregnant women '/Vho drink water containing chlorite in excess of me MeL Sollie people may experience anemia. This health effects language is not intended to catalog aU possible ileaJth effects for disinfection byproducts. Rather, it is inlended to inform consumers of some of the pOS!l1Die heallh effed3 associar..d with disinfectiOll byproducts in dIinking water when the rule was ffnaflZed. What are EPA's drinking water regulations for disinrection byproducts? In 1974, Congress passed the Safe Drinking Water Act This Jaw requires EPA to determine the level of contaminants in drinking water at which no adverse health effects are Ilkely 10 occur. These non-enforceable health goals, llased solely on possible health risks and exposure over a lifefime, with an adequate margin of safety. are caUed maximum contaminant level goals (MelG). Contaminants are any physical. chemical, biological or radiological substances or mailer in water. EPA sets MClGs llased on the best available $Oie.nee to prevent potential healll1 problems.. Based on the MelG, EPA sets an enforceable regulation called a maximum contaminant fevet {Mel}. MeLs are set as close [0 the health goals as possible, considering cost. benefits and the abmty of pubfic water systems to detect and remove contaminants using suitable treatmenl tectlnologies. Mels fer disinfection byproducts are set at the foRewing levels: http://water.epa.gov/drink/contaminantsibasicinforrnationldisinfectionbyproducts.cfin 10115/2010 Disinfection Byproduct Total Trihalomethanes Bromodichlorometilane Zero Bromoform Zero DibromochkJrometilane 0.06 mgll ()f 60 pph Chloroform 0.07 mgll or 70 pph Ha!oacetic acids Dichloroacelic acid Zero Trichloroacetic acid 0.02 mg/L or 20 pph Monochloroacetic ·acid 0.07 mgll or 70 ppb Bromoacetic acid Re-aulaled with ihis group but has no MetG Dibromoacetic acid Regulated with tilis group but has no MClG Bromate Zero Chlorite 0.80 mg/L or aeo ppb 0.080 mgll ()f 80 pph (Sum of the coocentralioos of all live frihalomethanes) as an annual average 0.060 mgll or 60 pph (Sum of the concentrations of all live haloace1ic acids) as an annual average 0.010 milJigta'llS per filer (mgll) or 10 parts per binlon (ppb) as an annual average 1.0 mgll or 1 part per million (ppm) MCls are set as close to the health goals as possible, considering cost, benefits and the abilify of public Vlater systems to detect and remove conlaminants using suitable lrea!rnent technologies. States rray set more stringent drinking water MCLGs and MCls for disinfection byproducts than EPA. nle following drinking water regulations apply 10 disinfectaots and disinfection byproducts: Slime ' Dim l\'!e!?!lls "rltl Dlsfnfe¢.f'''' Syc,d.:it:ct& Rule ISla"e t DBPHDecember 16, 1998} The Stage 1 Disinfec!anls and Disinfection Byproducls Rule reduces exposure to disinfection I;yproducts·for cuslomers of community waler systems and norr lransient non·communify systems, including those serving fewer than 10,000 Pflople, that add a disinfectant 10 tile drinking water duP.'lg any part of the Irealment precess. Stage 2 Disinfecrants and Disinfection Byproducts Rule /SIage 2 PBP} (December 15, 2005) Slage 2 PSP rule builds upon "artier rules that addressed disinfeclion byproducts 10 improve your drinking water quailly and provide additional public health protection frcm disinfactlon IP;prcd!Jcts. The Safe Drinking water ... oct requires EPA to periodicaJly review the national primar/ drinking water regulation for each contaminant and revise the regulation, rr appropriate, based on new scientific dala. EPA Vim include the Disinfectants and Disinfection Byproduc'<s rules in a future review cycle. • More information an the Sbc Year R-e:vlew ot Drinkfna W-a:ter Standarr.s How wlll I know if disinfection byproducls are in my drinking water? When routine monitoring ,ndicaies that disinfection byproduct !evels are above the MCl, your water supplier must take steps to reduce lIle amount of disinfection byproductsso that they are below that level. Waler suppliers must nOliff their cuslamers as soon as practical, but no taler than 30 days after the system learns of the violation. Additional actions, suoh as providing alternative drinking water suppHes, may be required to prevent serious risks to public health_ See EPA"s public notification requirements for DubHe water svstems_ How will disinfection byproducts be removed from my drinking water? Water systems tilat use surface water or ground water under the direcl influence of surface water and use conventional fiIlratfon treatment are required to remove specified percentages of organic materials that may raact with disinfectants to form disinfecfion byprcducts, priOT to disinfection. Other CO<ltrol strategies include mcdffication of disinfection practices in a manner that still provides adequale protection against pathogens. How do I learn mont about my drinking water? EPA strongly encourages people to learn more about their drinking water, and to support local efforts to protect the supply of safe dcinkir.g water and upgrade tlte communiP! water system. Your water bm or telephone bOok's government listings are a good slartir.g point for local information, Contact your weter utiliiy_ EPA requires all cammuniiy water systems to prepare and deWier an annual consumer confidence report (CCR) (sometimes called a water quaITty report) for their cuslomers by July 1 of each year. If your water provider is not a community water system, or if you have a private water supply, request a copy from " nearby community water system. The CCR summmjz"'" intonnarfon ffimlrding sOl/S'S used fl.e. rivgm, fakes, reservot!':>, or aqlliferst, dB!el:ted· contaminants. rompliaru;e <lnd edlJCa!io<!al ~n. • Some water suppliers have posted !heir annual reports on EPA's Web Sile. other EPA Web sites • Find an answer or ask a question about drinking water contaminants on EPA's Qlleslion and Answer web site or call EPA's Safe Drinking ,,"Valer HoDine at (800) 426- 4791 EPA's Microbials and Disinfec!!on B'(prodw;!s Web site Stage 2 DisinfectanllOjsinfectjpn Bvoroduc!s Rule Slace 1 OisinfectanliDisinfeciion Byproducts Rule http://water.epa.gov/drink/contaminants/basicinforn;tationldisinfectionbyproducts.cfm 10115/2010 • EPA'" Enyjrofac!s IGR Well stte • OIsinfectioo Byproduct Information • Disinfection Byproduc!J: A Reference Re!IOIlfCe • Dl3infed!jjn BYDroduCl$ Heallb E[eeIs EPA's Guidance Manyal Anern"ljye Q/!!jnfectanls and Oxjdants PDF • EPA's Integrated Risk Information System • EPA I1lS1ory 01 Drinking WaletTrealment PDF • EPA OJjn!!jnq Waler Trea!met1! fact Sheet POf Oth9r Federal Departments and Agencies • Bromate • (&nw" !or Ql!i1!as2 & Prg.ent{on C9/llrol'$ Natlo",,! In5lllu!e Iv< Og;uoational Safe" and f-i ... "Uh InlematioroJI Ch .... njg!! &'Vl"( Card fJ?r S<>dImn 8rrmlo Chlorite • ;'!genco, for Toxic $ubSl2nces lind OIsease Re<?ls!ry ToxFAO~_ Chlarfnt' Qimride and Chforile Agency ~ot Toxic SUGt.lanr.{!!l1fm1 Qi.!'t.~s2 R?c""~N Toxfcoroofl.;.lJ Profile Chthrina tHqxm-eand Chlorite las! updated oo/Aonday. Jur. ... 14. 2CJ10. --0----- http://water.epa.gov/drinklcontaminants/basicinformationldisinfectionbyproducts.cfin 10/15/2010 -&..a. .......... --."..L.IL .... .....,~-....... __ \..a.'&'~."",,1 .LL&. _ .... ..&.&..&.L~Ae r .. _ .. _ ... --------... -----.I - ---_._._. Disinfection By-Products Trihalomethanes .--~ ------------.--------------------_ .. _------------------.-------_._--_._------... -. Trihalomethanes (THM) are a group of four chemicals that are formed along with other disinfection by products when chlorine or other disinfectants used to control microbial contaminants in drinking water react with naturally occurring organic and inorganic matter in water. The trihalomethanes are chloroform, bromodichloromethane, dibromochloromethane, and bromoform. EPA has published the Stage 1 Disinfectants and Disinfection Bvproducts Rule to regulate total trihalomethanes (TTHM) at a maximmn allowable annual average level of 80 parts per billion. The four trihalomethanes (THM's) listed below: Trichloromethane I CHCl3 I (chloroform) I Dibromochloromethane IIcHCIDr2 1 I Bromodichloromethane II CHC1zBr l I TribromoDlethane 16] (bromoform) are all by-products of chlorination. They are Cancer Group B carcinogens (shown to cause cancer in laboratory animals). Trichloromethane (chloroform.) is by far the most conhnon in most water systems. Dibromochloromethane is the most serious cancer risk, (0.6 ~g!l to cause a 10-6 cancer risk increase) followed in order by Bromoform (4 ugIl), and Chloroform (6 ug/l). Current regulations limit the concentration of these 4 chemicals added together (total trihalomethane or TTHM levels) to 100 ug/l. Treatment THM levels tend to increase with pH, temperature, time, and the level of "precursors" present. Precursors are organic material which reacts with chlorine to form THtVI's. One way to decrease TIfM's is to eliminate or reduce chlorination before the filters and to reduce precursors.. There are more http://www.wa.ter-research.netitrihalom.e~anes.htm 10/15/2010 I I I I precursors present before filtration, so we want to reduce or eliminate the time chlorine is in contact with this water. If some oxidation before filtration is required, an alternative disinfectant like potaSsimn permanganate or peroxide could be considered. Note that this may not be an option ifprechlorination is necessary to achieve required CT values. The EPA has indicated that the best available technology for THM control at treatment plants is removal of precursors through "enhanced coagulation". Enhanced coagulation refers to the process 0 f optimizing the filtration process to maximize removal of precursors. Removal is improved by decreasing pH (to levels as low as 4 or 5), increasing the feed rate of co~aulants, and possibly using ferric coagulants instead of alum. For point of use systems at homes, activated carbon filters are the most effective treatment. Reverse osmosis units will also eliminate trihalomethanes. Upcoming Regulations The EPA is considering extensive revisions to the regulations covering disinfection by-products (DBP's). The limit for TIRM's would be lowered to 80 ugJI, and three additional categories ofDBP's . This standard will replace the current standard of a maximum allowable annual average level of 100 parts per billion in December 2001 for large surface water public water systems. The standard will become effective for the first time in December 2003 for small surface water and all ground water systems Halo acetic acids (monobromoacetic acid, dibromoacetic acid, monocbloroacetic acid, dichloroacetic acid, and trichloroacetic acid) are byproducts of chlorination similar to THM's. An MCL for total haloacetic acids of 60 ugll is expected. Excessive levels can cause nervous system and liver effects. Chlorite is to be regulated with an MCL set at 1 mg/l. Excessive levels can cause hemolytic anemia. Bromate, the other newly regulated DBP 1 is a concern only for systems using ozone. An MCL of IO ug/l is expected. Excessive Levels causes gastrointestinal, kidney, and hearing effects. Stage 1 Disinfectants and Disinfection Byproducts Rule More Comprehensive Information on Trihalomethanes University of Florida http://www.agen.ut1.edul'''''Wq/thm/ Canadian Website http://www.watermilLcom.aulchlorine.htm Water Qualitv Help Guides Glossary of Water Temrinology Note: ugll is used as an abbreviation for microgramslliter or parts per billion. Note: THM's are not a major concern for treating groundwater wells with low organic matter content. TH.iYf's fonn through the partial oxidation of organic material, therefore it is a more important concern to http://www.water-research.netltrihalomethanes.htm 1011512010