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HomeMy WebLinkAboutDAQ-2024-0045591 DAQC-CI107360001-23 Site ID 10736 (B1) MEMORANDUM TO: FILE – CLEAN HARBORS CLIVE, LLC – Clive Hazardous Waste Transfer Facility THROUGH: Chad Gilgen, Minor Source Compliance Section Manager FROM: Connor Kijowski, Environmental Scientist DATE: November 17, 2023 SUBJECT: FULL COMPLIANCE EVALUATION, Minor, Tooele County INSPECTION DATE: November 9, 2023 SOURCE LOCATION: 3.5 Miles South - East of Exit 49 on I-80 Clive, UT DIRECTIONS: Follow signs for Clean Harbors Clive Facility once you exit I-80. The office is located in the modular trailer on the south side of the security fence. Ring the doorbell by the security gate or call the source contact number on the gate to gain access. SOURCE CONTACTS: Branden Prettyman, Facility Operations Manager 435-884-8573; prettyman.branden@cleanharbors.com OPERATING STATUS: Operating normally at the time of inspection. PROCESS DESCRIPTION: This source is currently used for transfer and storage of materials only. Mixing or treatment does not occur at this site, but adsorbents may be applied during loading processes. The incinerator has not operated for years and is now partially dismantled and unable to operate. Materials to be incinerated are taken to the Aragonite or Grassy Mountain facilities. Some incoming wastes are screened to determine acceptability. Wastes are brought in by rail, trucks, and tankers, and include non-energetic and energetic liquids, non-energetic and energetic solids and soils, containerized solids, and other wastes such as medical wastes. Roll boxes containing wastes are stored in one of the RCRA permitted storage areas. APPLICABLE REGULATIONS: Approval Order (AO) DAQE-AN107360018-22, dated May 13, 2022 NSPS (Part 60) IIII : Standards of Performance for Stationary Compression Ignition Internal Combustion Engines, MACT (Part 63) -ZZZZ: National Emissions Standards for Hazardous Air Pollutants for Stationary Reciprocating Internal Combustion Engines, ) 1 2 SOURCE EVALUATION: Name of Permittee: Permitted Location: Clean Harbors Clive, LLC - Clive Hazardous Waste Transfer Facility PO Box 1339 3.5 Miles South - East of Exit 49 on I-80 Grantsville, UT 84023-1339 Clive, UT SIC Code: 4953: (Refuse Systems) Section I: GENERAL PROVISIONS I.1 All definitions, terms, abbreviations, and references used in this AO conform to those used in the UAC R307 and 40 CFR. Unless noted otherwise, references cited in these AO conditions refer to those rules. [R307-101] I.2 The limits set forth in this AO shall not be exceeded without prior approval. [R307-401] I.3 Modifications to the equipment or processes approved by this AO that could affect the emissions covered by this AO must be reviewed and approved. [R307-401-1] I.4 All records referenced in this AO or in other applicable rules, which are required to be kept by the owner/operator, shall be made available to the Director or Director's representative upon request, and the records shall include the two-year period prior to the date of the request. Unless otherwise specified in this AO or in other applicable state and federal rules, records shall be kept for a minimum of two (2) years. [R307-401-8] I.5 At all times, including periods of startup, shutdown, and malfunction, owners and operators shall, to the extent practicable, maintain and operate any equipment approved under this AO, including associated air pollution control equipment, in a manner consistent with good air pollution control practice for minimizing emissions. Determination of whether acceptable operating and maintenance procedures are being used will be based on information available to the Director which may include, but is not limited to, monitoring results, opacity observations, review of operating and maintenance procedures, and inspection of the source. All maintenance performed on equipment authorized by this AO shall be recorded. [R307-401-4] I.6 The owner/operator shall comply with UAC R307-107. General Requirements: Breakdowns. [R307-107] I.7 The owner/operator shall comply with UAC R307-150 Series. Emission Inventories. [R307-150] Status: In Compliance. Each condition from Section I was reviewed and determined to be in compliance. The source is not currently required to submit an Emission Inventory. Section II: SPECIAL PROVISIONS II.A The approved installations shall consist of the following equipment: II.A.1 Clive Hazardous Waste Transfer Facility II.A.2 One (1) Carbon Adsorption System Consists of two (2) units to achieve a 95% removal efficiency II.A.3 One (1) Bulb Recycling Unit Lamp Recycler Controls: Two (2) Baghouses (in parallel) Activated Carbon Filter System 3 Shatter Shield Processor Controls: One (1) Baghouse Activated Carbon Filter II.A.4 One (1) 234 hp Emergency Engine Water Pump Engine Fuel: Diesel Fuel NSPS Subpart IIII MACT Subpart ZZZZ II.A.5 One (1) 341 hp Emergency Engine Water Pump Engine Fuel: Diesel Fuel MACT Subpart ZZZZ II.A.6 One (1) 10,000-gallon Storage Tank Contents: Diesel Fuel II.A.7 Two (2) 500-gallon Storage Tanks Contents: Diesel Fuel II.A.8 One (1) 1,000-gallon Storage Tank Contents: Diesel Fuel Status: In Compliance. No unpermitted equipment was observed during the inspection. Additional Information: II.A.3: The bulb recycling unit was unable to be viewed as it was operating and requires a respirator for entry. II.A.4: The diesel fuel fire pump engine was replaced with a fully electric engine in January 2023. II.A.7: One 500-gallon storage tank was removed in concurrence with the diesel engine replacement. II.B Requirements and Limitations II.B.1 Source-wide Requirements II.B.1.a The owner/operator shall not transfer more than 13,000,000 gallons of liquid waste per rolling 12-month period. [R307-401-8] II.B.1.a.1 The owner/operator shall: A. Determine amount of liquid waste transferred with customer receipts or billing records B. Record amount of liquid waste transferred on a daily basis C. Use the transfer data to calculate a new rolling 12-month total by the 20th day of each month using data from the previous 12 months. [R307-401-8] Status: In Compliance. The source transferred 202,471 gallons of liquid waste for the rolling 12-month period ending in October 2023. Values are calculated according to this condition. Refer to the attachments for more details. 4 II.B.1.b The owner/operator shall use a carbon adsorption system to control emissions from the transfer of liquid waste from rail cars to trucks. [R307-401-8] Status: In Compliance. A carbon adsorption system is used and was viewed during the inspection. II.B.1.c The owner/operator shall maintain and operate the carbon adsorption system according to the manufacturer's instructions or recommendations. [R307-401-8] Status: In Compliance. The carbon adsorption system is maintained and operated according to the manufacturer's recommendations. II.B.1.d The owner/operator shall transfer liquid waste on site by the use of submerged loading. [R307-401-8] Status: In Compliance. Submerged loading is utilized to transfer liquid waste. II.B.1.e Unless otherwise specified in this AO, the owner/operator shall not allow visible emissions from any stationary point or fugitive emission source on site to exceed 10% opacity. [R307-401-8] II.B.1.e.1 Unless otherwise specified in this AO, opacity observations of emissions shall be conducted according to 40 CFR 60, Appendix A, Method 9. [R307-201-3] Status: In Compliance. No visible emissions were observed from any stationary point or fugitive source. Refer to the VEO Form in the attachments. II.B.2 Bulb Recycling System Requirements II.B.2.a The owner/operator shall use two baghouses in parallel and an activated carbon filter system to control emissions from the Lamp Recycler. [R307-401-8] Status: In Compliance. The source indicated that two baghouses are used in parallel along with an activated carbon filter system. The baghouse gauges could not be safely viewed as the Bulb Recycling Unit was operating and requires a respirator for entry. Records provided by the onsite personnel indicate the process is closely monitored and procedures are followed according to this AO. II.B.2.b The owner/operator shall use a baghouse and an activated carbon filter to control emissions from the Shatter Shield Processor. [R307-401-8] Status: In Compliance. The source indicated that a baghouse and an activated carbon filter system are used to control emissions from the Shatter Shield Processor. The baghouse gauges could not be safely viewed as the Bulb Recycling Unit was operating and requires a respirator for entry. Records provided by the onsite personnel indicate the process is closely monitored and procedures are followed according to this AO. II.B.2.c The owner/operator shall maintain and replace each activated carbon filter according to the manufacturer's instructions or recommendations. [R307-401-8] Status: In Compliance. The source indicated that each carbon filter is maintained and replaced according to manufacturer recommendations. II.B.2.d The owner/operator shall install a manometer or magnehelic pressure gauge to measure the static pressure drop across each baghouse in the bulb recycling system. [R307-401-8] II.B.2.d.1 The pressure gauge shall be located such that an inspector/operator can safely read the indicator at any time. [R307-401-8] 5 II.B.2.d.2 The pressure gauge shall measure the pressure drop in 1-inch water column increments or less. [R307-401-8] Status: In Compliance. The source confirmed that a pressure gauge is located on each baghouse and measurements are recorded daily. The Bulb Recycling Unit was operating and the gauges could not be safely viewed without a respirator. The onsite personnel provided records of the previous months' daily pressure drop readings and all values were within the specified range of 2 and 9 inches of water column. II.B.2.e The owner/operator shall maintain the static pressure drop across each bulb recycling system baghouse during operation between 2 and 9 inches of water column. [R307-401-8] II.B.2.e.1 The owner/operator shall record the pressure drop at least once per operating day. [R307-401-8] II.B.2.e.2 The owner/operator shall maintain records of the pressure drop readings. [R307-401-8] Status: In Compliance. The source confirmed that a pressure gauge is located on each baghouse and measurements are recorded daily. The Bulb Recycling Unit was operating and the gauges could not be safely viewed without a respirator. The onsite personnel provided records of the previous months' daily pressure drop readings and all values were within the specified range of 2 and 9 inches of water column. Refer to the attachments for the recorded pressure drop values. II.B.3 Emergency Engine Requirements II.B.3.a The owner/operator shall install a 234 hp emergency engine that is certified to meet a NMHC+NOx emission rate of 3.0 g/hp-hr or less. [R307-401-8] II.B.3.a.1 To demonstrate compliance with the emission rate, the owner/operator shall keep a record of the manufacturer's certification of the emission rate. The record shall be kept for the life of the equipment. [R307-401-8] Status: Not Applicable. The 234 hp emergency engine (II.A.4) was replaced with an all-electric unit and no longer requires an emission rate certification. II.B.3.b The owner/operator shall not operate each emergency engine on site for more than 100 hours per rolling 12-month period during non-emergency situations. There is no time limit on the use of the engines during emergencies. [R307-401-8, 40 CFR 63 Subpart ZZZZ] II.B.3.b.1 To determine compliance with a rolling 12-month total, the owner/operator shall calculate a new 12-month total by the 20th day of each month using data from the previous 12 months. Records documenting the operation of each emergency engine shall be kept in a log and shall include the following: A. The date the emergency engine was used B. The duration of operation in hours C. The reason for the emergency engine usage. [40 CFR 60 Subpart ZZZZ, R307-401-8] II.B.3.b.2 To determine the duration of operation, the owner/operator shall install a non-resettable hour meter for each emergency engine. [R307-401-8, 40 CFR 63 Subpart ZZZZ] Status: In Compliance. A non-resettable hour meter was observed on the emergency diesel engine (II.A.5). The engine operated for 10.1 hour for non-emergency usage for the rolling 12-month period ending in October 2023. A usage log is maintained digitally and contains the date, duration, and reason for engine usage. Refer to the usage log in the attachments. 6 II.B.3.c The owner/operator shall not allow visible emissions from the emergency engines on site to exceed 20% opacity. [R307-401-8] Status: In Compliance. The emergency engine was not operating at the time of inspection and no visible emissions were observed. II.B.3.d The owner/operator shall only use diesel fuel (e.g. fuel oil #1, #2, or diesel fuel oil additives) as fuel in each emergency engine. [R307-401-8] II.B.3.d.1 The owner/operator shall only combust diesel fuel that meets the definition of ultra-low sulfur diesel (ULSD), which has a sulfur content of 15 ppm or less. [R307-401-8] II.B.3.d.2 To demonstrate compliance with the ULSD fuel requirement, the owner/operator shall maintain records of diesel fuel purchase invoices or obtain certification of sulfur content from the diesel fuel supplier. The diesel fuel purchase invoices shall indicate that the diesel fuel meets the ULSD requirements. [R307-401-8] Status: In Compliance. Only ultra-low sulfur diesel is used as fuel for the emergency engine. A certificate of analysis provided by the fuel supplier indicated a sulfur content of 4.8 ppm. Refer to the attachments for more details. II.B.4 Storage Tank Requirements II.B.4.a The owner/operator shall load the 10,000-gallon diesel storage tank by the use of submerged loading. [R307-401-8] Status: In Compliance. The 10,000-gallon diesel storage tank is loaded via submerged loading. Section III: APPLICABLE FEDERAL REQUIREMENTS In addition to the requirements of this AO, all applicable provisions of the following federal programs have been found to apply to this installation. This AO in no way releases the owner or operator from any liability for compliance with all other applicable federal, state, and local regulations including UAC R307. NSPS (Part 60) IIII: Standards of Performance for Stationary Compression Ignition Internal Combustion Engines Status: Not Applicable. The emergency engine subject to this subpart has been replaced with an electric engine and is no longer applicable. MACT (Part 63) -ZZZZ: National Emissions Standards for Hazardous Air Pollutants for Stationary Reciprocating Internal Combustion Engines Status: In Compliance. Refer to Section II.B.3 for more details. AREA SOURCE RULES EVALUATION: The following Area Source Rules were evaluated during this inspection: Emission Standards: Sulfur Content of Fuels [R307-203] Status: In Compliance. Refer to Condition II.B.3.d.2 for more details. 7 Emission Standards: Fugitive Emissions and Fugitive Dust [R307-205] Status: In Compliance. No fugitive emissions or dust were observed during the inspection. The site is mostly paved. National Emission Standards for Hazardous Air Pollutants [R307-214] Status: In Compliance. This rule is satisfied by compliance with 40 CFR Part 63 Subpart ZZZZ. Refer to the Federal Requirements Section and Section II.B.3 for more details. EMISSION INVENTORY: The emissions listed below are an estimate of the total potential emissions (PTE) from Clean Harbors Clive, LLC - Clive Hazardous Waste Transfer Facility on the Approval Order (AO) DAQE-AN107360018-22, dated May 13, 2022. PTE are supplied for supplemental purposes only. Criteria Pollutant PTE tons/yr CO2 Equivalent 33.00 Carbon Monoxide 0.19 Nitrogen Oxides 0.89 Particulate Matter - PM10 0.06 Particulate Matter - PM2.5 0.06 Sulfur Dioxide 0.00 Volatile Organic Compounds 1.28 Hazardous Air Pollutant PTE lbs/yr Benzene (Including Benzene From Gasoline) (CAS #71432) 22 Mercury Compounds (CAS #EDF033) 3 Methylene Chloride (Dichloromethane) (CAS #75092) 1098 Trichloroethylene (CAS #79016) 27 Vinyl Chloride (CAS #75014) 11 PREVIOUS ENFORCEMENT ACTIONS: No enforcement actions within the past five years. COMPLIANCE STATUS & RECOMMENDATIONS: In regards to Approval Order (AO) DAQE-AN107360018-22, dated May 13, 2022: In Compliance. The source appears to be well maintained and operated. Records were provided during the inspection and via email. HPV STATUS: Not Applicable. RECOMMENDATION FOR NEXT INSPECTION: Inspect at the regular interval. NSR RECOMMENDATIONS: None at this time. ATTACHMENTS: VEO Form, Bulb Recycling Unit Daily Inspection Logs, Generator Usage Logs, Liquid Waste Transfer Rolling 12- Month, Fuel Certificate of Analysis Year Fire Pump #1 #2 #1 #2 #1 #2 #1 #2 #1 #2 #1 #2 #1 #2 #1 #2 #1 #2 #1 #2 #1 #2 #1 #2 2022 0.4 0.4 3.3 0.4 1.8 0 2.2 0.2 0.4 0.5 0.4 1 0.5 0.6 1.4 0.7 0.8 0.5 1.3 0.4 1.1 0.5 0.7 0.4 2023 0.0 2 0 1.2 0.0 0.7 0.0 0.8 0.0 0.9 0.0 0.7 0.0 0.9 0.0 1.0 0.0 0.5 0.0 0.7 0.0 0.3 0.0 0.0 12 Month Rolling Average 13.9 7.2 10.6 8.0 8.8 8.5 6.6 9.1 6.2 9.5 5.8 9.2 5.3 9.5 3.9 9.8 3.1 9.8 1.8 10.1 0.7 9.9 0.0 9.5 Fire Pump #1 Electric- Does Not Emit Emissions Fire Pump #2(Diesel) Date Hours Reason HR METER Date Hours Reason HR METER 1/3/2023 0.1 WEEKLY TEST RUN 9.8 1/10/2023 0.6 WEEKLY TEST RUN 10.5 1/17/2023 0.4 WEEKLY TEST RUN 10.9 1/24/2023 0 WEEKLY TEST RUN 10.9 1/31/2023 0.7 WEEKLY TEST RUN 11.6 2/7/2023 0 WEEKLY TEST RUN 11.6 2/14/2023 0.1 WEEKLY TEST RUN 11.7 2/21/2023 0.3 WEEKLY TEST RUN 12 2/28/2023 0.8 WEEKLY TEST RUN 12.8 3/7/2023 0.2 WEEKLY TEST RUN 13 3/14/2023 0.2 WEEKLY TEST RUN 13.2 3/21/2023 0.1 WEEKLY TEST RUN 13.3 3/28/2023 0.2 WEEKLY TEST RUN 13.5 4/4/2023 0.2 WEEKLY TEST RUN 13.7 4/11/2023 0.2 WEEKLY TEST RUN 13.9 4/18/2023 0.2 WEEKLY TEST RUN 14.1 4/25/2023 0.2 WEEKLY TEST RUN 14.3 5/2/2023 0.1 WEEKLY TEST RUN 14.4 5/9/2023 0.2 WEEKLY TEST RUN 14.6 5/16/2023 0.2 WEEKLY TEST RUN 14.8 5/23/2023 0.2 WEEKLY TEST RUN 15 5/30/2023 0.2 WEEKLY TEST RUN 15.2 6/6/2023 0.4 WEEKLY TEST RUN 15.6 6/13/2023 0 WEEKLY TEST RUN 15.6 6/20/2023 0.1 WEEKLY TEST RUN 15.7 6/27/2023 0.2 WEEKLY TEST RUN 15.9 7/4/2023 0.4 WEEKLY TEST RUN 16.3 7/11/2023 0 WEEKLY TEST RUN 16.3 7/18/2023 0.3 WEEKLY TEST RUN 16.6 7/25/2023 0.2 WEEKLY TEST RUN 16.8 8/1/2023 Off Line WEEKLY TEST RUN Off Line 8/8/2023 0.5 WEEKLY TEST RUN 17.3 8/15/2023 0.2 WEEKLY TEST RUN 17.5 8/22/2023 0.1 WEEKLY TEST RUN 17.6 8/29/2023 0.2 WEEKLY TEST RUN 17.8 9/5/2023 0 WEEKLY TEST RUN 17.8 9/12/2023 0.2 WEEKLY TEST RUN 18 9/19/2023 0.1 WEEKLY TEST RUN 18.1 9/26/2023 0.2 WEEKLY TEST RUN 18.3 10/3/2023 0.1 WEEKLY TEST RUN 18.4 10/10/2023 0 WEEKLY TEST RUN 18.4 10/17/2023 0 WEEKLY TEST RUN 18.4 10/24/2023 0.2 WEEKLY TEST RUN 18.6 10/31/2023 0.4 WEEKLY TEST RUN 19 11/7/2023 0.3 WEEKLY TEST RUN 19.3 DecemberJanuaryFebruaryMarchApril May June July August September October November Year January February March April May June July August September October November December 2022 283984 254274 171250 172137 165753 230458 231104 267207 242324 275689 299540 326088 2023 268319 314451 295626.5291 212210.8374 376562.992 145861 260037 134920 157135 202471 43090 0 2 Month Rolling Averag 2904143 3218594 3088697 3128771 3339580 3254984 3283917 3151630 3066441 2993222 2736773 2410685 Density of Water 8.34 lbs/gallon RAILCAR DATE PROFILE WCC LOADS LBS GALLONS SG 1 2 3 4 5 SKSX117111 6-Nov-23 A22KUN1993AIRB A22K 1 46540 5637 0.99 46540 GATX88856 3-Nov-23 FB1UN1993AIRB FB1 3 82520 9994 0.99 40860 31580 10080 GATX88856 2-Nov-23 FB1UN1993AIRB FB1 1 46200 5596 0.99 46200 TEVX73723 2-Nov-23 CH2618156B-AG A22K 2 63600 7703 0.99 43060 20540 TEVX73723 1-Nov-23 CH2618156B-AG A22K 2 92140 11160 0.99 45120 47020 TEVX5059 1-Nov-23 CH2618156B-AG A22K 1 24780 3001 0.99 24780 TEVX5059 31-Oct-23 CH2618156B-AG A22K 3 119040 14418 0.99 48360 23580 47100 TEVX5050 30-Oct-23 CH2618156B-AG A22K 2 65440 7926 0.99 48000 17440 TEVX5050 27-Oct-23 CH2618156B-AG A22K 2 92840 11244 0.99 45660 47180 TILX197917 27-Oct-23 CH151791B-AG FB1 1 32800 3973 0.99 32800 TILX197917 26-Oct-23 CH151791B-AG FB1 3 130720 15832 0.99 43660 44900 42160 SKSX117131 25-Oct-23 FB1UN1993AIRB FB1 2 84480 10232 0.99 42940 41540 SKSX117131 24-Oct-23 FB1UN1993AIRB FB1 2 87440 10590 0.99 44800 42640 GATX205210 23-Oct-23 FB1UN1993AIRB FB1 1 32940 3990 0.99 32940 GATX205210 20-Oct-23 FB1UN1993AIRB FB1 3 118960 14408 0.99 42740 35220 41000 UTLX660000 18-Oct-23 A22KUN1993AIRB A22K 1 27900 3379 0.99 27900 UTLX660000 17-Oct-23 A22KUN1993AIRB A22K 1 47120 5707 0.99 47120 GATX1376 17-Oct-23 FB1UN1993AIRB FB1 2 107100 12971 0.99 42240 45780 19080 GATX1376 16-Oct-23 FB1UN1993AIRB FB1 1 41460 5021 0.99 41460 UTLX660000 16-Oct-23 A22KUN1993AIRB A22K 1 46760 5663 0.99 46760 UTLX660000 13-Oct-23 A22KUN1993AIRB A22K 1 47220 5719 0.99 47220 TEVX5007 12-Oct-23 CH2618156B-AG A22K 3 112020 13567 0.99 45460 44760 21800 TEVX5007 11-Oct-23 CH2618156B-AG A22K 1 46380 5617 0.99 46380 TEVX5058 11-Oct-23 CH2618156B-AG A22K 1 18540 2245 0.99 18540 TEVX5058 10-Oct-23 CH2618156B-AG A22K 1 92300 11179 0.99 46760 45540 TEVX5058 9-Oct-23 CH2618156B-AG A22K 1 47260 5724 0.99 47260 CBTX740451 9-Oct-23 A22KUN1993AIRB A22K 2 0 0 0.99 CBTX740451 6-Oct-23 A22KUN1993AIRB A22K 2 88520 10721 0.99 43140 45380 SKSX117136 6-Oct-23 FB1UN1993AIRB FB1 1 18160 2199 0.99 18160 SKSX117136 5-Oct-23 FB1UN1993AIRB FB1 2 81060 9818 0.99 41660 39400 SKSX117136 4-Oct-23 FB1UN1993AIRB FB1 2 85260 10326 0.99 43000 42260 SKSX117134 27-Sep-23 A22KUN1993AIRB A22K 4 178240 21588 0.99 48660 45940 48140 35500 GATX54024 27-Sep-23 FB1UN1993AIRB FB1 2 90160 10920 0.99 44120 36020 10020 GATX54024 26-Sep-23 FB1UN1993AIRB FB1 2 80920 9801 0.99 43100 37820 GATX53942 26-Sep-23 A22KUN1993AIRB A22K 2 84380 10220 0.99 45980 38400 GATX53942 25-Sep-23 A22KUN1993AIRB A22K 2 94080 11395 0.99 48020 46060 UTLX670717 22-Sep-23 FB1UN1993AIRB FB1 4 126200 15285 0.99 36960 40880 40000 8360 UTLX202939 19-Sep-23 A22KUN1993AIRB A22K 1 28060 3398 0.99 28060 UTLX202939 18-Sep-23 A22KUN1993AIRB A22K 3 137620 16668 0.99 45840 46040 45740 GATX57914 14-Sep-23 FB1UN1993AIRB FB1 2 40880 4951 0.99 40360 520 GATX57914 13-Sep-23 FB1UN1993AIRB FB1 2 86020 10418 0.99 43060 42960 SKSX117137 12-Sep-23 DH3UN1993B DH3 1 11620 1407 0.99 11620 SKSX117137 11-Sep-23 DH3UN1993B DH3 4 172860 20936 0.99 41540 45880 42840 42600 UTLX649311 5-Sep-23 A22KUN1993AIRB A22K 4 166360 20149 0.99 46220 45160 44180 30800 SKSX117111 28-Aug-23 A22KUN1993AIRB A22K 2 50880 6162 0.99 47400 3480 SKSX117111 25-Aug-23 A22KUN1993AIRB A22K 3 136540 16537 0.99 47280 41020 48240 GATX205210 25-Aug-23 FB1UN1993AIRB FB1 1 36800 4457 0.99 36800 GATX205210 24-Aug-23 FB1UN1993AIRB FB1 1 42040 5092 0.99 42040 GATX205210 23-Aug-23 FB1UN1993AIRB FB1 2 77700 9411 0.99 37880 39820 GATX63606 22-Aug-23 FB1UN1993AIRB FB1 2 56200 6807 0.99 41500 14700 GATX63606 21-Aug-23 FB1UN1993AIRB FB1 2 86020 10418 0.99 43380 42640 UTLX662555 18-Aug-23 FB1UN1993AIRB FB1 4 151500 18349 0.99 42980 42900 42240 23380 SKSX117115 17-Aug-23 FB1UN1993AIRB FB1 1 40800 4942 0.99 40800 GATX54505 17-Aug-23 A22KUN1993AIRB A22K 2 94700 11470 0.99 48940 45760 SHPX202447 16-Aug-23 A22KUN1993AIRB A22K 1 8820 1068 0.99 8820 SHPX202447 15-Aug-23 A22KUN1993AIRB A22K 3 123760 14989 0.99 41540 41540 40680 SHPX202447 14-Aug-23 A22KUN1993AIRB A22K 1 43280 5242 0.99 43280 GATX54505 11-Aug-23 A22KUN1993AIRB A22K 2 81700 9895 0.99 48000 33700 GATX53919 7-Aug-23 FB1UN1993AIRB FB1 2 83240 10082 0.99 40040 43200 GATX53919 31-Jul-23 FB1UN1993AIRB FB1 2 81980 9929 0.99 41840 40140 TILX197917 28-Jul-23 FB1UN1993AIRB FB1 2 69080 8367 0.99 50460 18620 TILX197917 27-Jul-23 FB1UN1993AIRB FB1 2 106540 12904 0.99 51600 54940 GATX54365 27-Jul-23 FB1UN1993AIRB FB1 1 40520 4908 0.99 40520 GATX54365 26-Jul-23 FB1UN1993AIRB FB1 3 120460 14590 0.99 39440 41200 39820 SKSX117117 25-Jul-23 FB1UN1993AIRB FB1 1 16800 2035 0.99 16800 SKSX117117 24-Jul-23 FB1UN1993AIRB FB1 2 80640 9767 0.99 40540 40100 SKSX117117 20-Jul-23 FB1UN1993AIRB FB1 2 78180 9469 0.99 39520 38660 UTLX41235 20-Jul-23 A22KUN1993AIRB A22K 2 51140 6194 0.99 39500 11640 UTLX41235 19-Jul-23 A22KUN1993AIRB A22K 3 136920 16583 0.99 45980 45260 45680 SKSX117134 17-Jul-23 FB1UN1993AIRB FB1 1 23880 2892 0.99 23880 SKSX117134 14-Jul-23 FB1UN1993AIRB FB1 3 116040 14054 0.99 38000 40120 37920 GATX53995 14-Jul-23 A22KUN1993AIRB A22K 1 42820 5186 0.99 42820 GATX53995 13-Jul-23 A22KUN1993AIRB A22K 3 141120 17092 0.99 45120 46580 49420 GATX89309 12-Jul-23 FB1UN1993AIRB FB1 4 150820 18267 0.99 38780 38400 39700 33940 GATX53932 11-Jul-23 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017687270FLE 017687117FLE 013571163FLE 013571163FLE 013571143FLE 013571143FLE 017687371FLE 017687147FLE 017687147FLE 017687337FLE 017687337FLE 017687337FLE 017687117FLE 017687456FLE 017687456FLE 017687456FLE 012704401FLE 012704401FLE 017687147FLE 013571176FLE 017687198FLE 017687198FLE 017687198FLE 017687166FLE 017687166FLE 012704338FLE 008572315SKS 008572315SKS 017687562FLE 017687562FLE 013571176FLE 017687533FLE 017687511FLE 017687511FLE 017687580FLE 017687580FLE 012704338FLE 017687508FLE 017687533FLE 017687533FLE 017901105FLE 017901105FLE SKSX117124 3-Jan-23 A22KUN1993AIRB A22K 3 123980 15016 0.99 47420 48360 28200017684727FLE HF Sinclair Parco Refining LLC ⦁Laboratory Services⦁Sinclair, WY Certificate of Analysis, Pioneer Pipeline #2 ULSD Diesel Fuel Transferor:HF Sinclair Parco Refining LLC 100 E. Lincoln Highway ⦁ PO Box 277Sinclair, WY 82334EPA Company ID: 5053, Facility ID: 23521 Transferee:ConocoPhillipsPioneer Pipeline600 N. Dairy Ashford RoadHouston, TX 77079-1175EPA Company ID: 4528, Facility ID: 82245 Sample Date: 11/7/2023 Tester(s): Chris Kiley, Hilarie Arellano Tank Number: Tank 532 Sampler: M. Wagy LIMS ID: 770257 EPA Batch Number: 5053-23521-23-500323 Tender: Available BBLS: Approved By: Date: 11/7/2023 Hilarie Arellano #2 Diesel 15ppm w/w Sulfur Motor Vehicle Diesel Fuel. 15 ppm sulfur (maximum) Undyed Ultra-Low Sulfur Diesel Fuel. For use in all diesel vehicles and engines. Lubricity/conductivity additives may need to be added at the terminal in order for the fuel to meet ASTM D975 requirements. SPECIFICATIONSTestMETHODRESULT MINIMUM MAXIMUM Gravity, API @ 60°F ASTM D4052 37.9 30.0 Flash Point (PMCC), °F ASTM D93 143.0 135.0 Haze @ 50°F ASTM D4176, Proc. 2 1 2 Bright & Clear ASTM D4176 Pass PASS Color ASTM D1500 0.5 2.5 Ash, wt%ASTM D482 <0.001 0.010 Distillation @ 760mmHg, °F ASTM D86 IBP 329.8 REPORT 10 vol.% Recovered 386.1 REPORT 50 vol.% Recovered 475.3 REPORT 90 vol.% Recovered 596.2 540.0 640.0 FBP 647.0 698.0 % Total Recovered 99.6 REPORT % Residue 1.3 REPORT BS&W, vol%ASTM D2709 0.025 0.050 Sulfur, ppm ASTM D7039 4.8 10.0 Copper Strip Corrosion, 3hr @ 122°F ASTM D130 1a 1b CR, Ramsbottom, wt%ASTM D524 0.05 0.35 Thermal Stability, Y Filter ASTM D6468 99.7 82.0 Cetane Index, 4V ASTM D4737, Proc. A 47.2 40.0 Cetane Index, 2V ASTM D976 47.1 40.0 Cloud Point, °F ASTM D5773 -3.0 6.0 Pour Point, °F ASTM D5949 -30 -15 Conductivity, pS/m @ T, °C ASTM D2624 3 @ 18.5 10 Viscosity @ 104°F, cSt ASTM D445 2.155 1.9 3.4 NACE Rust Test, Rating TM0172-2001 A B+