DSHW-2024-004976

afat .^al
HEffiffi,#MffiM
June 19, 1998
Rob Powers
Utah Division of Solid and Hazardous Waste
288 North 14ti0 West
P.O. Box 144880
Salt Lake City, Utah 84114
Re: Site lnvestigation
Laundry Supply Company
Salt Lake Gity, lltah
Olympus Work Order# 7585
Dear Mr. Powers:
Olympus Environmental, Inc. (Olympus), on behalf of Laundry Supply Company (LSC), has
initiated a site investigation at LSC's facility located at 3785 West 1987 South in Salt Lake
City, Utah (Facility). The purpose of the investigation is to determine the nature and extent of
subsurface halogenated volatile organic (HVO) compound contiamination at the Facility. This
investigation is being performed in accordance with the Utah Department of Environmental
Quality, Division of Solid and Hazardous Waste (DSHw)-approved Site lnvestigation Plan
(SlP) (JBR EnvironmentalConsultants, lnc., November 10, 1997) and the DSHW May 6, 1998
approval of the April21, 1998 revisions to the SlP. Follonting is an interim report of
investigative activities. Olympus will prepare and submit a more detailed report of the
investigation at its onclusion.
SOIL BORING ADVANCEUENT AND SOIL SAilIPLING
On May 12 and 13, 1998, Olympus and its drilling subcontractor, Layne Christensen Company
(Layne) of Salt Lake City, Utah, advaned three soil borings at the Facility. We advanced the
borings to a depth of approximately 20 feet belw ground surface using a 4.2$inch inside
diameter hollor stem auger. Figure 1 shors the locations of the soil hrings labeled SB-1,
SB-2, and S&3. Layne and Olympus collected soil samples using a split spoon soil sampler at
five'foot intervals during the advancement of the soil borings. Olympus screened the soil
samples for tetrachloroethene using Drager gas detector tubes and logged the samples for soil
classification purposes. Attacfiment A indudes copies of the Soil Boring Logs. Soil cuttings
generated during the boring program were drummed and are presently stored at the Facility
pending disposal anangements.
D:\LSC.T'BS.'DE. &rg-s lR.ds Environmental & Hazardous waste services
Kent, WA Billings, MT Boise, lD Helena, MT Portland, OR Spokane, WA
3109 KendallStreet. Boise, ldaho 83706 o [phone]. Fax [phone]
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u,#'Hl;T,ff,,r or E;;**i,,nrar ouar*y
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HazaUtah Division of Solid and
June 19, 1998
Page 2
rdous Waste
Olympus shipped the soil samples by ovemight courier, using chain of custody protocol, to
Evergreen Analytical, lnc. (Evergreen) of \A/heat Ridge, Colorado. At Olympus' instruction,
Evergreen composited (by weight) the sample set from each boring into one sample for
analyses. ln addition, the laboratory prepared grab samples for analyses, Iabeled SB2-1.5 and
SB&3, from split spoon samples collected immediately above the watertable from S&2 and
SB-3, respectively.
Evergreen analyzed the samples for halogenated HVO compounds using procedures
documented in SW-846 Method 8260. Table 1 presents a summary of the soil sample
analyses. Attachment B includes copies of the laboratory analytical reports, the Sample Chain
of Custody Record, and Olympus'data validation report.
MONTTOR|NG rmELL COMPLETTONS AND GROUND WATER SAI'|PLfNG
Olympus and Layne completed the three soil borings as ground water monitoring wells labeled
MW-1, MW-2, and MW-3 (Figure 1). We completed the wells as approximately 20-foot deep
two-inch diameter PVC wells. Attachment A includes copies of the Monitoring Well Completion
Logs.
On May 14, 1998, Olympus surveyed the monitoring wells for vertical and horizontal control to
a relative Facility benchmark (100 feet) and gauged ground water elevations in the wells. Table
2 presents a summary of the ground water elevation gauging. Olympus prepared a Facility
ground water elevation contour map based upon the May 14, 1998 ground water elevations
(Figure 1). Based upon the data used to compile the map, we calculated a ground water flow
direction at the Facility to the north-northwest with a gradient of 0.02 feet per feet.
ln preparation for ground water sampling, Olympus developed the monitoring wells using an
airlift pump on May 14, 1998. We sampled the wells on May 15, 1998. Prior to sampling, we
purged the wells of three casing water volumes using disposable polyethylene bailerc. The
wells were sampled immediately after purging using the same bailer. For quality assuran@
and quality contro! (OA/OC) purposes, Olympus prepared an equipment blank (EB), a trip
blank (l'B), and a duplicate sample from MW-2 (labeled MW-4). As part of our ground water
monitoring program, Olympus measures pH, electricalconductivity, dissolved oxygen, and
temperature (field pararneters) at each monitoring well. Table 2 includes a summary of the
field parameter measurements.
Olympus shipped the ground water and QA/QC samples by ovemight courier, using chain of
custody protocol, to Evergreen Analytical, lnc. (Evergreen) of Wheat Ridge, Colorado. The
laboratory analyzed the samples for HVO compounds using prccedures documented in SW-
846 Method 8260. Table 3 presents a summary of the ground water sample analyses.
Attachment B indudes copies of the laboratory analytical reports, the Sample Chain of
Custody Record, and Olympus'data validation report.
Olympus drummed all development and purge water generated during the ground water
monitoring event. The water storage drums are presently stored at the Facility pending
disposal anangements.
d:tlsc.7585Beq &1 998 ir.doc
t
HazaUtah Division of Solid and
June 19, 1998
Page 3
rdous Waste
ADDITIONAL ASSESSMENT
ln an effort to befter define the nature and extent of HVO compounds in ground water at the
Facility, Olympus proposes to continue the assessment dorrn-gradient of the release area.
We propose to continue the assessment using soil probes outfifted with ground water sampling
apparatus. EarthProbe of Salt Lake City, Utah willprovide soil-probing services. EarthProbe
willdrive five soil probes at apprcximate locations shown in Figure 1. We willgauge ground
water elevations and calculate ground water flow direction prior to soil probing activities to
confirm the flow direction. The soil probe locations will be moved (if necessary) to better locate
the probes down-gradient of the HVO release area (abandoned tank basin) based on the
calculated ground water flor direction.
At soil probe locations SP:l through SP-S, EarthProbe and Olympus willcollecl ground water
samples at depths of 15, 25 and 35 feet belovv the ground surface. Olympus will deliver the
water samples in appropriate contrainers, using chain of custody protocol, to OnSite Analytical
Services, lnc. (OnSite) of Salt Lake City, Utah for screening analyses. The laboratory wil!
screen the samples for HVO compounds using a proprietary analytical method. One duplicate
sample from the event will be shipped to Evergreen for confirfnation analyses. Evergreen will
analyze the confirmation sample using protocol established in SW-846 Method 8260.
Following sample collection, EarthProbe, willabandon the probe holes by sealing them grout.
EarthProbe will decontaminate all down-hole equipment with a pressure washer.
Decontamination waterwill be contained in drums and stored at the Facility pending disposal
anangements.
SCHEDULE
The above-described soil probing and ground water sampling is scheduled forJune 26, 1998.
LIMITATIONS
Olympus performed the services documented in this report in a manner consistent with
generally accepted principles and practices for the nature of the work completed in the same
or similar localities, at the time the work was performed. No otherwananty, express or implied,
is made.
Opinions contained in this report apply to conditions existing when the services were
performed. All conclusions and recommendations are based on readily available and
reasonably ascertainable information on site conditions at the time of the work and for the laws
in effect at that time. We are not responsible for any changes in environmental standards,
practices, or regulations subsequent to performance of services. This report is not meant to
represent a legal opinion. We do not wanant the accuracy of information supplied by others,
nor the use of segregated portions of this report.
d:Vsc.7585Ueq 6,1 9-98 ir.doc
o
HazaUt.f, Division of Solid and
June 19, 1998
Page 4
rdous Waste
Please feelfree to contact Lucy Jenkins at Parsons Behle & Latimer (LSC legal counsel) at
(801) 532-123y'. or me at the letterhead address, telephone orfacsimile numbers, or via E-mail
at <[e-mail] should you have any questions or comments.
oLYMPUS ETMRONMENTAL, tNC.
ffiltl,u(
Michael Backe, P.G.
Senior Hydrogeologist
cc: Craig Reaveley, LSC
Lucy B. Jenkins, Parsons Behle & Latimer
File
d:Usc.7585Ueq 6-1 9-98 ir.doc
N
1987 SOUTH STREET
o
881/MW-1(mEl
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SP.1
Legend
Soil Borirryruonibring Well Locatbn
(grutnd nater ekndm)
Ground WabrGonbur
(0.25 bot lnbrval)
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TABLEI.SoiI SAMPLING
Parsons Behle Latimer
Laundry Supply Company
Salt Lake City, Utah
o
ANA LYSES
Field lnformation H Volatile Oroanics (SWA46 Method 801
tro
'I.JG(Jr-h
IIv-bot-
o*,
TE(f
otr
G
a5IoAAEtr)AI
=E,,t i-
6ae{r- E,
Grl
rF .=
Hetr{P
-i9
tsirl
'F €=
lu
Hst6TT.gEI,,t *
luoes!.-!. Aegr i=.!E E'I- -l- {g
A
E"I
C"
Ir*Y
lUoa-
A
E,,a
E,'-*Y
UJo]-
ot.E
o--*.o6;Ei{trE"
.II\.4JY Cornments
$oil Sarnpling
SBl -Comp 12-May-98 ND<1 ,3 ND<l .3 ND<l.3 10 ND<l .3 ND<l.3 90,000 78 8J Com SA
ND<1 .1 ND<l.1 I ND<1 .1 i ND<l .1 I ND<l.1 i ND<l.1 67 ND<1 .1 i ND<l .1 iGrab sample 1.5'-3.5'
SB2-Comp 1 ND<6.3 ND<6.3 ND<6.3 46 8J ND<6.3 910,000 170 ND<6.3
i ND<l.3 ND<l .3
i ND<6.4
Notes: tdkg = Microg,ams per kilogram
ND = Not Detected (at Reporting Limit)
- = Not Anatyzed or Reported
J = Analyte detected belotl, Practlcal Quantitation Limit
1,1 -DCA = 1,1-Dichloroethane
1,1 -DCE = 1,l-Dichlordhene
Cis-1,2-DCE = Cis-l,2-Dichloroethene
Trans-l,2-DCE = Trans-l,2-Dichloroethene
PCE = Tetrachloroethene
TCE = Trichloroethene
d:Usc.7585\DEQ +19-98 lR-Table 1 Page 1 of I oEt/7585 6t19/98
o
ERFTABLE?. GROUNDWAT
Parsons Behle Latimer
Laundry Supply Gompany
Salt Lake Ciry, lrtah
IELD PARAilIETERS
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xoto>
-roonr-
CT G orments/Obse rvations
fi,lo1t|toritt-g.well smp$g
MW-l g2frg 1 2.88 89.21
1 3.72 88.87 11.7 7.82 7.87 275.2 275.8 2.2 brurn
MW-2 92.U
Duplicate
1 3.42 88.s2
I 3.41 88.90 14.2 8.02 8.04 2575 ?574 1.8 bronrvn
1 14.2 8.04 8.05 2583 25E5 1.8 Sampb brorvn
Ndes: Elemtions referenc€d to Relative Benc*rmark (100 fee$
oC = Degrees Centigra&
pS/cm = Micro-Siemens (micromhos) per Centimeter
mg/l = Milligrans por Liter
"H20 = lnchm of Water
Temprature, Electriml Conftctivity, and Dissolved Oxygen m€nsured in$itu
- = Not Measured or Recorffi
d:Vsc.7585\LSC Master Tables-Table 2 Page 1 of 1 oEffi585 919/98
TABLE 3. GROUND WATER SAITTPLING ANALYSES
Parsons Behle Latimer
Laundry $upply Company
$alt Lake Gity, Utah
Fleld lnformation iH Volatile O ics {StA/n846 Method Sl
Eo
a-IGu
a-
h
ioitrlrE!r
o i E=E i EE
i-r
I
E"
=Y{
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rF
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U,
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luol-
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-
.-r,rEtrEDrI->.?}ConrnEnts
Ground Water Monitoring lfllell A nalrees
th,r\i:i
-'-'----i
B:MAi-bB l-
-i-i fii ND<1 ND<1 45 28.0 3J s0,000 190 28
II
IVIVV-2 15-Mav-98 i ND<l ND<1 ND<1 I 840 t6 81,000 aga 1J
Duplicate l$May-ffi i ND<l ND<1 ND<1 ND<l0 300 10J 79,000 290 ND<l0 Labeled ir\,V-,4
I
irn /-C-
" " " .isrrii;i;ifi'i "-' NiFl ND<1 ND<1 60J 2{0.0 ND<l0 96,000 350 {0J
Notee: pg/l = Micrqrams per Liter
ND = Not Detected (at Reporting Limit)
- = Not Anafyzed or Reported
J = Analyte detwted belo$, Practbal Qmntitation Limil
1,1 -DCA = 1,l-Dichloroethane
1,1 -DCE = 1,1 -Dichloroethene
Cis-l,2-DCE = Cis-l,2-Dichloroefirene
Tran+I ,?-DCE = Trans.l ,2-Dichloroethene
PCE = TEtrachloroethene
TCE = Trichloroethene
d:Usc.7585\DEQ +19-98 lR-Table 3 Page I of 1 oEU7585 6/19/98
oo
ATTACHMENT A
SOIL BORING AND
MONITORI NG WELL COMPLETION
LOGS
OLYMPUS ENVIRONMENTAL, INC.
SO't BOR'IUG tOG
Sheet 1 of 1
Client: Parsons Behle & Latimer
Site Name: Laundry Supply Co.
Location: Salt Lake City, UT
Boring No.: SB-1
$urface Elevation: 92.52
Gontracton Layne Christensen
Driller: James Crowley
Method: 4,25" HSA
Rig: Mobile 8-61
Drillins Start Finish
Time 10:10 1 1:10
Date 1 1-May-98 11-May-98
Loggsd By: Mike Backe
Sampler: Split $poon Size: 3 x24 inches Gompletion
lnformation:Depth
(feetl
Blow
Count
$ample
(inch)
Description of
$arnple Material
Observations
Flush Grade
0.0
1.0
2.0
3,0
4.0
SP: Sand/silt, some grave (<112"1; Dull brcwn, dry,
poor grading, fine grained, very soft, non plastic.
ML: SilUsand; Greenish brcwn, wet, poor grading
fine grained, very soft, non plastic.
Cement
Seal
I./
2" PVC
Riser
$ilica $and
Pack
,,J,
2'PVC
Screen
End Cap
5.0 1 24 CL: Glay; Gray with reddish brown staining, moist,
poor grading, fine grained, firm, high plasticity.
Drager tube <2 PPM
Sampled @ 10:50
5.5
6.0
6.5
2
3
3
ML: SilUclay, trace sand; Greenish browo, wet, poor
grading, fine grained, very soft, high plasticity.
7.0
8.0
9.0
10.0
10.5
11.0
4
2
3
24 SP: $and; Reddish brown, wet, poor grained, fine
grained, soft, non plastic.
Drager tube <2 PPM
Sampled @ 10:50
11.5
3 CL: Clay; Greenish gray, poor grading, fine grained,
firm, high plasticity.
12.0
13.0
14.0
Heaving sand
15.0
r 5.5
3
4
24 CL: Clay; Gray; wet, fine grained, poor grading, firm,
high plasticity.
Drager tube >300 PPM
Sampled @ 11:20
16.0 7 SP: sand; Gray, wet, fine grained, poor gradiog, firm,
non plastic.
'16.5 7 CL: Clay-sarne as above.
17.0
19.0
19.0
Bit slipped ahead of
auger pulled and redrilled
20.0 1 15 SP: $and, few gravel (<1 14"). fine grained, poor
grading, very soft, non plastic.
Drager tube >300 PPM
Sampled @ 14:05
20.5
21 .O
1
1
CL: Clay, trace gravel (<1 14"); BlacUgroy, wet, poor
grading, poor grading, fine grained, firm, high
plasticity.
21 .5 10 CL: Clay; BlacUgray, wet, poor grading, poor
grading, fine grained, firm, high plasticity.
Boring terminated @ 20.5'.
Completed as ground water monitoring well MW-1 .
$ee Monitoring Well Construction Log for details.
Water added to control
heaving sand
d:Usc.7585\LSC Log+SB-l BL $oil classifications by ASTM D 2488-84 oEffis8s 6/19ne8
OLYMPUS ENVIRONMENTAL, INC,
MONITORING WELL CO'US TRUCTION LOG
Parson$ Behle Latimer
Laundry Supply Company
Salt Lake Clty, Utah
Monitoring Well lD: l{W:I
We[ $pecificatigns
L-l Setdown: 0'43 feet
L-z Riser: ---mfeet
L-g Screenimfeet
L-4 Bottom Cap-*-T:Af feet
L-5 Well Depth: -, 20.06. feet
L6 Boring Depth: , 20,.4? feet
d:Usc.7585\LSC Logs-MW-l CL
Cornpletion Date: 1,2,-*l?y-98
Pfotective Houping Wilh t oghing Wgterprqof Wqfl 9apDiameter: 0.70 feet
Total Length: ----T66- feet
-
$tickup: . -q.q6 feet
Material: Steel
SUrfA,qe Sppl .Wjth Arynulqfj$pqgB D.rain
Type of Seal: Concrete/Sand Drain
Upper Concrete Thickness: 1.0 feet
Sand Drain Thickness:1.0 feet
Lower Concrete Thickness: 0.8 feet
Riser Pioe
-----.---+-Diarneter:
Materiat:ffi4oPVc
BackfiU:
Spal
2 inch
tsentonite PelletsType of Seal:
Thickness:
Distance Above $creen:
0.3 feet---75feet
Screefr
Diameter:
Slot Size:
Material:
Filter Pack:
2 inch
0.010 inchffic
10-20 Silica Sand
Depth to Bottom of
Filter Pack 20.5 feet
Botpholg,,$eal
Type of Seal:
Thickness:
Borehole Diameter:
Native Material
Ele,yFtions
Top of Housing: , 9?.98 feet
Top of Casing: 92,09 feet
Surface 92.52 feet
, q.0 feet
I inches
oEffi585 6/19fl98
OLYMPUS ENVIRONMENTAL, INC.
SO't BORING LOG
Sheet 1 of 1
Client: Parsons Behle & Latimer
Site Name: Laundry Supply Co.
Location: Salt Lake City, UT
Boring No.: SB-2
$urface Elevation: 92.59
Contractor: Layne Christensen
Driller: James Crowley
Method: 4.25" HSA
Rig: Mobile 8-61
Drilling Start Finish
Time 9:15 10:45
Date 13-May-98 13-May-98
Logged By: Mike Backe
Sampler: Split $poon Size:3 x 24 inches Completion
lnforrnation:Depth
(fectl
BI ow
Gount
Sample
(inchl
Description of
Sample Material
Observations
Flush Grade
0.0
1.0
SP: Sand/silt, some gravel (<112:'); Dull brown, dry,
poor grading, fine grained, very soft, non plastic.
Cement
Seal
,7
1.5
2.0
2,5
3.5
23
35
2A
16
12 SP: Sand/silt, trace gravel (114); Brown, dryn poor
grading, fine grained, very soft, non plastic.
Stratification: None.
Drager tube 15 PPM
sampled @ 9:30
4.0
5.0
6.0
2" PVC
Riser
Silica Sand
Pack
'/2- PVC
Screen
End Cap
7.0
7.5
8.5
9.5
3
5
4
5
15 SP: Sand, mostly gravel (<1/8'); Dull brown, wet,
poor grading, fine grained, very soft, non plastic.
Stratification: None.
Drager tube 30 PPM
sampled @ 9:55
10.0
11.0
12.0
12.5
1
2
24 CL: Clay/sand; Dull gray, moist, poor grading, fine
grained, firm, moderate plasticity.
Drager tube 200 PPM
sampled @ 10:10
13,0
13.5
4
5
CL: Clay; Dull reddish brown with gray layers; moist,
poor grading, fine grained, firm, high plasticity.
14.0
15.0
16.0
17.0
17.5
5
7
16 SP: Sand; Dull grayish brown, wet, poor grading, fine
grained, very soft, non plastic.
Drager tube >300 PPM
Strong solvent odor
Drager tube >300 PPM
Sampled @ 10:30
18.0
19.5
I
7
CL: CIay; Dull grayish brown, wet, poor grading, fine
grained, firm, high plasticity.
19.0
20.0
Heaving sands
Boring terminated @ 20.0'.
Completed as ground water monitoring well M1ru-2.
See Monitoring Well Construction Log for details.
Water added to control
heaving sand
d:Usc.7585\LSC Logs-SB-2 BL Soil classifications by ASTM D 2488-84 oEr/7585 6/19/98
OLYM PUS ENVIRONfrIIENTAL, I NC.
MONITOR,,YG WELI CO'VSTRUCTION LOG
Parcons Behle Latimer
Laundry Supply Company
Salt Lake Gity, Utah
Monitoring Well lD: MW-z
Well SpepificAt!,onS
L-1 Setdown: 0.25 feet
L-ZRiser: mfeet
L-3 $creen:ffifeet
L-4 Bottom Cap--fdf feet
L-5 Well Depth: ,, 1,9.38 feet
L-6 Boring Depth: 2Q,Q0 feet
d:Usc.7585\LSC Logs-ltlW -2 CL
Completion Date : J.3-May-9.8
Prptectivq,hlgupinq Wlth toclting Wgtgrprqp,f Well QapDiameter: 0,70 feet
Total Length: -766- feet
$tickup' lll6I-reet
Material: Steel
$Uffqpe Sqfll With,Annu,lff $pace Prpin
Tyre of Seal: Concrete/Sand Drain
Upper Concrete Thickness: 1.0 feet
Sand Drain Thickness:1.0 feet
Lower Concrete Thickness: 0.8 feet
Ri$er Pioe
Diameter:
Material:
Backfill:Bentonite Chips
Seal
Type of Seal:
Thickness:
Distance Above Screen:
Bentonite Pellets
, ,. l inch
Schedule 40 PVC
1.3 feet
l--E.feet
Sqrqqn
Diameter:
Slot Size:
Material:
Filter Pack:
2 inch
0.010 inchffi
10-20 Silica Sand
Depth to Bottom of
Filter Pack: 19.6 feet
Borehole Seal
Type of Seal:
Thickness:
Borehole Diameter:
Native Material
0.4 feet
I inches
Elevations
Top of Housing: ,92.61,
Top of Casing: , 9?.34
Surface 92.59
feet
feet
feet
oEt/7585 6/19t98
. OLYMPUS ENWRONMENTAL, INC,
SO't BOR"UG tOG
Sheet 1 of 1
Glient: Paruons Behle & Latirner
Site Narne: Laundry Supply Co.
Location: Salt Lake City, UT
Boring No.: SB-3
$urface Elevation: 92.22
Gontractor: Layne Christensen
Driller: Jarnes Crowley
Method: 4.25n HSA
Rig: Mobile B€1
Drillins $tart Finish
Timel 12:23 15:35
Date 13-May-98 13-May-g8
Logged By: Mike Backe
$ampler: Split Spoon $ize: 3 x 24 inches Gompletion
lnformation:Depth
ffeetl
Blow
Gount
$ample
(inchl
Description of
$amplo Material
Observations
Flush Grade
0.0
1.0
$P: $and/silt, some gravel (<1 l2"l; Dull brown, dry,
poor grading, fine grained, very soft, non plastic.
Cement
Seal
I
2,O
2.5
6
7
ML: SilUday; greenish gray, dry, por grading, fine
grained, firm, moderate plasticity.
Drager tube 150 PPM
Sampled @ 12:4A
3.0 7 CL: Clay; Greenish gray, moist, poor grading, fine
grained, firm, high plasticity.
3.5 I SP: Sand; Greenish gray, wet, fine grained, poor
grading, very sofi, non plastic.
2" PVC
Riser
Silica Sand
Pack
.r'
2" PVC
Screen
End Cap
4.0
5.0
6.0
7.0
8.0
8.5
9.0
9.5
2
3
7
12
24 CL: Clay; Gray, vrret, poor grading, fine grained, firm,
high plasticity.
Stratification: None.
Drager tube 100 PPM
$ample @ 14:50
10.0
11.0
12.0
13.0 2 12 $P: Sand; Gray, wet, poor grading, fine grained,
very sofi, non plastic.
Drager tube >300 PPM
Sample @ 15:05
13.5
14.0
14.5
3
5
7
CL: Clay; Gray, wet, poor grading, fine grained, firm,
high plasticity.
15.0
16.0
17.0
18.0
18.5
19.0
19.5
2
3
5
7
18 CL: CIay; BlacUgroy, wet, poor grading, fine
grained, firm, htgh plasticity.
Stratification: none.
Drager tube 100 PPM
Sample @ 15:35
20.0 Heaving sand
Boring terminated @, 2O.4' .
Completed as ground water monitoring well MW-3.
See Monitoring \Alell Construction Log for details.
Water added to control
heaving sand
d:\tsc.7585\LSC togs'sB€ BL Soil classifications by ASTM D 248&84 oEffi585 6/19e98
OLYMPUS ENVIRONMENTAL, INC.
MONITORING WELL COffS TRUCTION LOG
tlVashington $tate University
Prosser, Washington
Monitoring Ullell lD: !4ULg
Well.$pecifigfltions
L-1 Setdown: 0.10 feet
L-2 Rise r: ---E,ffi'' fget
L-3 Screen:mfeet
L..f, Bottom Cap---ffifeet
L-5 \lVell Depth: . 29,,30 feet
L-6 Boring Depth: , ,29.49 feet
d:\\I1/SU.7855\LSC Logs-MW-S CL
Completion Date: 19:Mfly:98
Prolectiye H,ou*ing With Logkins yvgtqrpfpqf !/Velt Cap
Diameter: 0.70 feet
Total Length:
*--766-
feet
Stickup' llE-feet
Material: Steel
$prfqcq $e$l with.Annular,fipaqe PrAin
Type of Seal: Concrete/Sand Drain
Upper Concrete Thtckness: 1.0 feet
Sand Drain Thickness:1.0 feet
Lower Concrete Thickness: 0.9 feet
Risef.PipeDiameter: 2 inch
Material: Etffi40 PVc
Backfill:
Seal
Type of Seal:
Thickness:
Distance Above $creen:
Bentonite Pellets
0.6 feet--*-m"fggt
9,cteen
Diameter:
$lot Size:
Material:
Filter Pack:
2 inch
,. , ,q.,0,10 inch
Slotted PVC
10-20 Silica Sand
Depth to Bottom of
Filter Pack ,4A.! feet
Bqreholq $eal
Tyre of Seal:
Thickness:
Borehole Diameter:
Native Materisl
., 0,9, fegt
I inches
Elq.vations
Top of Housing: 92.91 feet
Top of Casing: , 92.7lfeet
Surfscts 92.22 feet
oEw855 6/19/S
ATTACHMENT B
LABORATORY
ANALYTICIAL REPORTS
/4.Euergreen,4.,fr. AnalyticalzN\ t,r.-t->
^/ \ Laboratory
May 29, 1998
MIKEBACKE
OLY'I\{PUS E}TVIRONMENTAL, INC .
5409 KENDALL STREET
BOISE, ID 83706
Lab Work Order: 98-1934
Client Project: 7585
Dear Mike Backe:
Enclosed are the analytical results for the samples shown in the Laboratory Work Order
Summary. The enclosed data have been reviewed for quality assurance. If you have any
questions concerning the reported information, please contact Mark Mensilq Quality
Assurance manager.
SAN4PLE DISPOSAL: Except for high level mercury (>260 ppm) samples, EAL will
dispose of all samples one month from the date of this letter. If you want samples
returned, please advise us by mail or fa,r as soon as possible.
RECORDS RETENTION: Effective January l, 1996 we will retain a copy ofthis
project report and supporting data for a period offive years. It has been our experience
that a five year retention period is more than adequate to respond to client inquiries. If
you want the project file sent to you after the five year period, please return a copy of
this letter.
The invoice for this work will U" I-m"a to your Accounts Payable department shortly.
Thank you for using the services ofEvergreen Analytical.
+"
Sincerely,
_.:]\44
V.P. Operations JUN O Z 19gB
Evergreen Analytical, Inc. 4036 Youngfield St. wheat Ridge, co 80033-3862 [phone] FAx [phone]
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Client Semple II)
Lrb Semple ID
Detc Coltected
Drte Received
DetePrcpered
Dete Anetped
Percent Moisfittc
Client Project II)
Lrb Wortr Order
Semple Metrix
Lrb X'iIe ID
Mcthod BhnI(
Efrective Ililution
7585
98-1934
Soil
>\8638::\R
R8052698
1.33
o.,,u,Ilff#:l,t##ffiffi ";(303) 42tr,o2t
Composite of SB-1
98-19344IE
0sltu98
05l14l9t
05126198
05126198
25.75
Method: SW8260A Hazardou3 Subctanee Ust - Voletile Organicr Unitrs:rrdl(g
Analyte cAs #
Acetone
Berzene
Bromodichloromethane
Bromoform
Bromomethane
67$+1
7143-2
75-274
7*2 2
74-93-9
60J
U
U
U
U
13
0.67
1.3
1.3
1.3
130
6.7
a,7
6.7
13
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Carbon disulfide
Carbon tetrachloride
Chloroberzene
Chloroethane
7&93€
7*1ffi
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10&90-7
7ffie3
U
3J
U
U
U
13
1.3
1.3
1.3
1.3
130
6.7
6.7
6.7
13
2-C h I o roethylvi nyl eth er
Chloroform
Chloromethane
Dibromochloromethane
1 , 1-Dichloroethane
110-7ffi
67S6-3
74-87-3
124 48-1
7*3+3
U
U
U
U
U
4.3
0.67
1.3
1.3
1.3
13
6.7
13
6.7
6.7
1 ,2-Dichloroethane
1 , l-Dichloroethene
cis-1, 2-Dichloroethene
trans-l, 2-Dichloroethene
1,Z-Dichloropropane
107-06-2
75-35-4
15&59-2
156€O-S
78-87-5
16
1.3
1.3
1.3
1.3
1.3
6.7
6.7
6.7
6.7
6.7
U
U
U
cis-l, 3-Dichloropropene
trans-l, 3-Dich loro pro pen e
Ethylbenzene
2-Hexanone
Methylene chloride
10061{1-5
10ffi1-02€
1 00-,41-{
591-78€
7549-2
U
U
U
U
U
1.3
1.3
0.67
6.7
1.3
6.7
6.7
6.7
67
6.7
4-Methyl-Z-pentanone
Styrene
1,1,2,z-Tetrach loroethane
Toluene
1,1,1 -Trichloroethane
10&10-1
10042-5
79-3+5
108€&3
71-55€
U
U
U
U
U
6.7
1.3
1.3
0.67
0.67
67
6.7
6.7
6.7
6.7
1,1,z-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
Total Xylene
7900-5
79-01€
108-05-4
7ffi14
1330-20-7
76
U
8J
U
1.3
1.3
6.7
1.3
0.67
6.7
6.7
67
13
6.7
Surrogate Recovery
1,2-Dichloroethan+d4 (SS-1 )
Toluensd8 (SS-2)
4-Bromofl uoroberuene (SS€)
101%
116%
107%
QC LIni33
75 - 110
82 - 125
74 - 115
U - Nd Dciectcd ltthc Reporting Limit (RL)
, - Anslyt! detcc'tcd below Prr.ticrt qtsnititrtion Limit (PQL)
quntitrtion renSc
S - Spikc Rcovcry outsi& acccptd rccovcry limits
I - Coryouna dc&dcd above reguletry limit
Que[trcn:
B-
Analyst
Method Blrnk
5/2998 l2:16:55 PM
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0sl26le8
0s126198
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Client Proiect ID
Lrb Wort Order
Sr-ph Mrtrir
Lrb fitelD
MethodBhnt
Efrective Dilution
75E5
98-1934
Soil
l::V4
M805269E
167.93
Method: SW8200A Hazardour Substance Llrt - Volrtlle Organlcr pdf(g
Analyte cAs #Concentration PQL
Tetrachloroethene 121-1fl.{1 30000 170 840
Surrogrto Recovery
1,2-Dichloroethan+d4 (SS-1 )
ToluenldS (S$2)
4-Bromofl uorobenzene (SS-3)
fi4iffo
103%
98%
QC Lhitr
79 - 115
82 - 113
74 o 12
aurUncn: U - Not Ddcsted sttbc R4orting Limit (RL)
J - Andytc dctccted bclof hrsticd aunititatlm Limit (PQL)
B - Rcpctcd
B - Ansbt
I
S - Spikc Reoovery outsi& rcceptd rcoovery limib
. - Compound drirx/,rd abovc rcgulatory limil
Analyst
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5n998 12:16:51PM
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IDete Andped
Percent Moistlre
sB-2-15
9t-1934{/2A,
05lt3lgE
051t4198
05126198
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Lrb Wort Order
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Leb File ID
Method Blrnt(
Effective Dilution
Method: SW8260A Hazardous Substanee Llst - Volatlle Organlcr pg/l(g
Analyte cAs #Concentration RL PQL
Acetone
Berzene
Bromodichloromethane
Bromoform
Bromomethane
67 64-1
7143-|2
7*274
7*25-2
7ffi3-ig
60J
U
U
U
U
11
0.34
1.1
1.1
1.1
110
5.4
5.4
5.4
11
2€rltanone
Carbon disulfide
Carbon tetrachloride
Chloroberzene
Chloroethane
7&9&3
75--1ffi
56-2$5
10&9G7
7ilO.3
U
U
U
U
U
11
1.1
1.1
1.1
1.1
110
5.4
5.4
5.4
11
2-Ch I oroeth ylvi nyl ether
Chloroform
Chloromethane
Dibromochtoromethane
1 , 1-Dichloroethane
11G75-8
67€&3
74-t^7-3
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75-U-3
U
U
U
U
U
3.5
0.54
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1.1
1.1
11
5.4
11
5.4
5.4
1,2-Dichloroethane
1 , 1-Dichloroethene
cis-1, 2-Dich loroethene
trans-1, 2-Dichloroethene
1 ,2-Dichloropropane
10746-2
7S35-,4
15&5$2
156€0-5
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U
U
U
U
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1.1
1.1
1.1
1.1
1.1
5.4
5.4
5.4
5.4
5.4
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trans-l, 3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
10061-01-5
10061 42$
1 00-41 -4
591-78€
7il9-2
U
U
U
U
U
1.1
1.1
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5.4
1.1
5.4
5.4
5.4
54
5.4
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Styrene
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1,1,z,z-Tetrach lo roethan e
Toluene
1 08-1 0-1
100-42-5
127_1U
793+5
108-8E=a
57
U
U
U
U
5.4
1.1
1.1
1.1
0.54
54
5.4
5.4
5.4
5.4
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1,1,z:Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
71-55€
79-00-5
79-01€
108-05-,4
7ffi14
U
U
U
U
U
0.54
1.1
1.1
5.4
1.1
5.4
5.4
5.4
il
11
Total Xylene 1330-20-7 0.54 5.4
Surrogite Recovery
1,2-Dichloroethane-d4 (SS-1 )
Toluen+dS (S$2)
4-B ro mofl u oroberzen e (SS-3)
10/-%
111%
98%
QC Lfnits
75 - 110
82 - 125
74 - 115
U - Not Deicded atthc R€porting Ljmit (Rt)
J - Andytc dcicclcd bclow Practic.l auaititEtion Limit (PQL)
S - Spikc Rccovery outside sccqdd r€covery limits
t - Coryouna dcncdcd above rcgulatory timit
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98-1934{38
05113198
051t4198
05126198
05126198
2l.E
Client Semple IID
Lrb Semple IID
Dete Collected
Detc Rcceived
Ilete Prepered
Dete Anrlped
Percent Moisture
Client Prujet ID : 7585
Lrb lVort Order : 9&1934
Sempte Mrtrix : Soil
Lrb File ID : >V8640::V3
Mcthod Btrnl( : R8052698
Efrective Dilution : 6.33
Method: SW8200A Hazardour Substenee Ust - Voletlle Organicr pdKs
Analyte cAs #Concentration RL PQL
Acetone
Berzene
Bromodichloromethane
Bromoform
Bromomethane
67$*1
714&|2
7s274
7*2*2
74-83-9
100 J
U
U
U
U
63
3.2
6.3
6.3
6.3
630
32
32
32
63
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Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodhane
7&93-3
7*15{
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7ilG3
U
U
U
20J
U
63
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6.3
6.3
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630
32
32
32
63
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Chloroform
Chloromethane
Dibromochloromethane
1 , 1-Dichloroethane
11&7ffi
67€613
7#7-3
12U*1
7*3*g
63
32
63
32
32
U
U
U
U
U
20
3.2
6.3
6.3
6.3
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1 ,1-Dichloroethene
cis-1, 2-Dich loroethene
trans-l, 2-Dichloroethene
1,2-Dichloropropane
10746-2
75-3S4
15&s9-2
1566G5
7ffi7-5
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6
8J
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U
6.3
6.3
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6.3
6.3
32
32
32
32
32
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tra ns-1, 3-Dichloro pro pene
Ethylbenzene
2-Hexanone
Methylene chloride
10061{1-5
10061-02€
1 00-41-4
591-78€
7ffi9-2
U
U
U
U
U
6.3
6.3
3.2
32
6.3
32
32
32
320
32
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Styrene
1,1,2,z-Tetrach I o ro eth a n e
Toluene
1 , 1 , 1-Trichtoroethane
10&10-1
10042-5
7$.34-5
10&88-3
71-5s5
U
U
U
U
U
32
6.3
6.3
3,2
3.2
320
32
32
32
32
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Trichloroethene
Vinyl acetate
Vinyl chloride
Total Xylene
7$.0&5
79-01€
108-05-,{
7fi14
133G20-7
170
6.3
6.3
32
6.3
3.2
32
32
320
63
32
U
U
U
Surrogate Recovery
1,2-Dichloroethan+d4 (SS-1 )
ToluenldS (SS-2)
4-Bromofl uoroberzene (SS-3)
92%
133% S X
92%
QC Lirftr
75 - 110
g2 - 125
74 - 115
Q,ueU[cn: U - Not Dcteded sttbc Reporting Limit (RL)
J - And),b &tec'tcd below PrsstiC aunititrtion Limit (PQL)
E - Rcported
Sprkc Rccovery outsi& rcceptcd rcoovcry limits
CompouA dcioctcd abovc rcgulrttry limit
Poc rurrogdo rtsovry &€ to nrrdrix iderfereoce. ScG
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Lrb grmple ID
Drtc Collected
Dete Received
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Clicnt Project ID : 7585
Lrb Work Order : 9t-1934
Semple Metrir : Soil
Leb X'ile IID : >L6939::V4
Method BhnI( : MB052698
Efrective Dilution : 3212.99
Method: SW8260A Hazardous Substanee Ust - Volatile Organlcr TdKg
Tetrachloroethene 127-18-,4 81 0000 16000
Sunogsto Recovery
1,2-Dichloroethane-d4 (S$1 )
Toluene-d8 (SS-2)
4-Bromofl uoro berzene (SS-3)
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4036 Youngfield St, TYheet Ridge CO
(303) 42sfl2r
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80033
Ctient Semple ID
Lrb Semple II)
Drte Coltected
Detc Rcceived
DetePrepered
Drtc Anetped
PercentMoisfurc
SB-3-2
9t-1934{4A
05113198
05lt4l9E
0512619E
0512619E
21.56
Client Pmject ID : 7585
L,rb lYor{r Order : 98-1934
Semple Metrix : Soil
Lrb X'itc IID : >\8637::V3
Method Btrnl( : R8052698
Efrective Dilution z L.Tl
Method: SW8260A Hazardoua Substance Ust - Voletile Organicr Unitr:rcrKg
Analyte PQL
Acetone
Berzene
Bromodichloromethane
Bromoform
Bromomethane
67$+1
714&|2
7*274
7*25-|2
74-83-g
40J
U
U
U
U
13
0.64
1.3
1.3
1.3
130
4,4
6.4
6.4
13
2-Butanone
Carbon dlsulfide
Carbon tetrachloride
Chloroberzene
Chloroethane
7&93-3
7*1m
5&2&5
10&9G7
7ilH
U
U
U
U
U
13
1.3
1.3
1.3
1.3
130
6.4
6.4
6.4
13
2€h I o roethylvi ny I eth er
Chloroform
Chloromethane
Dibromochloromethane
1 , 1-Dichloroethane
11G7ffi
67€&3
7+87-3
124-4,8.1
7**3
U
U
U
U
U
4.1
0.64
1.3
1.3
1.3
13
6.4
13
6.4
6.4
1,2-Dichloroethane
1,l-Dichloroethene
cis-l,2-Dichloroethene
trans-l,2-Dichloroethene
1 ,2-Dichloropropane
107 06 2
7s|}5-,4,
156-59-2
156€G5
7847-5
U
U
4J
U
U
1.3
1.3
1.3
1.3
1.3
6.4
6.4
6.4
6.4
6.4
cis-1, 3-Dichloropropene
trans-l, 3-Dichloro propene
Ethylbenzene
2-Hocanone
Methylene chloride
10061-01€
1006142$
1 00-,{1-4
591-786
7ffi9-2
U
U
U
U
U
1.3
1.3
0.44
6.4
1.3
6.4
6.4
6.4
64
6.4
4-Methyl-Z-pentanone
Styrene
1,1,z,z{etrachl oroetha n e
Toluene
1 ,1 , 1-Trichloroethane
10&1&1
l ggr-41-$
79-34-5
10&8&3
-71-sffi
U
U
U
1J
U
6.4
1.3
1.3
0.64
0.64
64
6.4
6.4
6.4
6.4
1,1,z-Trich loroetha n e
Trichloroethene
Vinyl acetate
Vinyl chloride
Total Xylene
7$0G5
79-01€
108{5-,4
7il1-,4
1330-20-7
U
7.7
U
U
U
1.3
1.3
6.4
1.3
0.64
6.4
6.4
64
13
6.4
Surrogsb Recovery
1,2-Dichloroethan+d4 (SS-1 )
Toluene-d8 (SS-2)
+Bromofl uorobenzene (SS-3)
%%
107%
83%
QC Linitr
75 - 110
82 - 125
74 - 115
Queilf,crr: U - Not Dctcdcd etthc R4ortiry Limit (Rt)
J - Analytc detcdcd bclgw Prutic.l qnnititrtisn r imit (PQL)
S - Spikc Rmvcry oilsi& rcccptcd rGcov€ry limitl
. - Coqqrna de&ctcd above regulEttry limit
X- Not Applicebla
5n&98 12:26:01PM
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[!rrant flrrtnLrt fiInstrirmEnt le:ID:
fi:7f, nA1 T i. rrre
F{INT5]
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Llpertstor II-}:lli rant fime :
In jecteLi at:
I(IHPBI-t5?rt 1,2:47
PBlJ526 .l?:'1 Fl
Evergreen Anatytical, Inc.
4036 Youngfietd SA, TYheet Ridge CO
(303) 42ffi02t
o
80033
Client Sample II)
Lrb Srmpte II)
Dete Collected
IDrtc Rsceived
Dete Prepared
Ilete Analped
Percent Moisfirre
sB-3-2
9E-193 444A;
05/13/98
05lt4l98
0s126198
05126198
2L.56
Client Project II)
Lrb \f,ort Order
Semple Metrir
Lrb File ID
Method Btenl(
Efrective IDilution
7585
98-1934
Soil
0::V4
M8052698
158.17
Method: SWE260A Hazerdout Substanee Llst - Voletlle Organlcr pg/t(g
Analyte cAs #Concentratlon RL PQL
Tetrachloroethene 1ZT_1U 7200 160 790
Surrogrtc Recovery
1,2-Dichloroethane-d4 (SS-1 )
ToluenldS (SS-2)
4-Bromofl uoroberzene (SS€)
99%
99%
97%
QC Unlts
79 - 115
82 - 113
74 o 122
aurnAcn: U - Not DetcCcd stthc RcPoding Limit (RL)
J- Aoalytc MdbcloyrPractical amititeti,on Limit (PQL)
vc quaditetioonngc
S - Spftc Rccovcry outri& scccptd rocov€ry limits
' - Coryound dr/,,od,dabovrc rcgplEtory limit-'*::K
sn&s,t2:t6:s7P.Analyst
iat€d Mcthod Blrnk
P 4EgI
l'{L.5F{liir [rF -t
PF BffF-t
T0TBL I trl.t t:HREtii?T0EiRt:tli
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Data file: >l f,74tl ::U4
I.lame: ?B-'LF-=,c+-ll 4Fl H. l.
11 isc: 5HHr" D[=1 4,
t rt F i le : tlt_t"128 : : llTTitle: It-: rTl r rn[: APF[-r.tnlH
| .ast tla t rLirat inn : ?HlJFl-4 l.P :
[lner*ator II-]: t{. I11
[1i ran t T i me : 9,$ l]5:?6 ,l t :2nInjn*ted at: PE[5?6 71:t-l f,
Qr-rant flutprrt fiInstrument
tl :{EF;1tl tl Lll
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o
4036
Evergreen Anatytical, Inc.
Youngfield St, lVheet Ridge CO
(303) 4q5-6021
r0033
Client Srmple IID
Lrb Semple ID
Dete Collected
Detc Received
Drte Prepered
Drtc Anetped
Percent Moisture
Composite of SB-3
98-193445D
05/r3198
05lr4l9E
0st26198
0s126198
26.15
Client Project II)
Lrb lVork Order
Semple Mrtrix
Lrb FiIe IID
Method Btrnk
Effective Dilution
7585
9t-1934
Soil
9::V3
R8052698
6.U
Method: SW8200A Hazardous Substance Ust - Volgtllc Organlct Unltl:pCKs
Analyte cAs #Concentratlon RL PQL
Acetone
Berzene
Bromodichloromethane
Bromoform
Bromomethane
67 64-1
714&|2
7*274
7*2*2
74-83-g
200 J
U
U
U
U
64
3.2
6.4
4.4
6.4
640
32
32
32
64
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chloroberzene
Chloroethane
78-93-3
7*1ffi
56-23-5
108-9&7
7il0-3
U
10J
U
U
U
64
6.4
6.4
6.4
6.4
640
32
32
32
64
2€h lo roethylvi nyl ether
Chloroform
Chloromethane
Dibromochloromethane
1 , 1-Dichloroethane
110-7ffi
67€&3
74-87-3
12Hb1
75-34-3
64
32
64
32
32
U
U
U
U
U
21
3.2
6.4
6.4
6.4
1 ,2-Dichloroethane
1 , 1-Dichloroethene
cis-l,2-Dichloroethene
trans- 1, 2-Dich loroeth ene
1,2-Dichloropropane
107-06-i2
75-35-,4
15&59-2
1ffiGs
78€7-5
U
35
30J
U
U
6.4
6.4
6.4
6.4
6.4
32
32
32
32
32
cis-l, 3-Dichtoropropene
trans-l, 3-Dichtoro propene
Ethylberuzene
2-Ho<anone
Methylene chloride
10061{1-5
10061 {/2€/
10G41-4
591-78€
7*09-2
32
32
32
320
32
U
U
U
U
U
6.4
6.4
3.2
32
6.4
4-Methyl-2-pentanone
Styrene
1,1,z,z-Tetrach lo roetha n e
Toluene
1,1,1 -Trich loroethane
108-1&1
100-412-5
793+5
10&8&3
71-5F6
U
U
U
U
U
32
6.4
6.4
3.2
3.2
320
32
32
32
32
1,1,2-Trich loroetha ne
Trichloroethene
Vinyl acetate
Vinyl chloride
79-00-5
79-01€
108-05-4
7il1-{
1330.20.7
330
6.4
6.4
32
6.4
3.2
32
32
320
64
32
U
U
Total X
Surrogats Recovery
1,2-Dichloroethane.d4 (SS-1 )
ToluenldS (SS-2)
4-Bromofl uoroberzen e (SS-3)
103%
109%
102%
QC Linitr
75 - 110
82 - 125
74 - 115
U - Not Dctcstcd dtb€ Rcporting Iimit (RL)
J- Arlal,,tc dctcdcd below Prrsticrl Annititrtim l,imit (PQL)
grrrlitrtimnngg
S - Spikc Reoovcry outsi& Eccqtrd rccoycry limits
t - Coryqoa deiccted above reguldmy limit
Queltfrcn:
B-
Analyst
Mctbod Blrak
X - Not Applic$le.
5/2&98 12:16:59 PM
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lloeraton III: KIHtJuant Trme : FB05!rt 1.]:4FInjected at: FBu52e l3:tU
o
40x
Evergreen Anatyticel, Inc.
Yungfield St, TYhert Ridge CO
(303) 4255$/r
O
8m33
Client Sample ID
Lrb Semple IID
Dete Coltected
Ilete Received
I)ete Prepered
Dete Anelped
Percent Moisfure
Composirc of SB-3
98-1934{5D
05/13/98
05lL4l98
05126l9t
05126198
26.15
Client Project ID
Lrb lVort Order
Semple Metrir
Lrb File IID
M€thod Btrnk
Effective Dilution
75E5
9t-1934
Soil
>L6941::V4
M8052698
169.26
Method: SW826OA Hazerdour Substanee LId - Voletllc Organlcr pdKs
Analyte cAs #Goncentratlon PQL
Tetrachloroethene 121-1${1 65000 170 850
Surrog.to Recovery
1,2-Dichloroethan+d4 (S$1 )
Toluen+d8 (SS-2)
4 Bromofluoroberzene (SS-3)
103%
103%
99%
QC Lhtitr
79 - 115
82 - 113
74 - 12
(lueHfrcrr: U - Not Detccted at the R4orting Limit (RL)
J - An lytc dctcdcd bclowlncticd Qnnititetion Limit (PQL)
S - Spikc Rcoovery outsi& accqtrdrecovery limits
' - Coryouod dr/rdrdabove rcgulstfiy limil
B-
Analyst
Mcthod Blsnk
5/2998 I2:16:58 PM
TCITEL IOI.I CHRTIIiflTIIBRHTi
1
-1
rr r.} ra ,'r a.r It= E, 3., rL, tE tL, t
Il
rlrar..1r-r=r= Ir:} E, ?.f ?, q',a, t
I
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rf
c-
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re
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9!I
Itfi
Data f ile: >l e94L=:Lr4f.lanre: ?B-'I?}4-05fi
1"1 isc: SHHI--'l-)F=L
[.!uant flrrtFLrt fiJe:l4:l- [nstriln]ent ltl:4. Ll LI EF;1UUUt
tJ['lHs HfT'HUt't
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: '{none}t?ir6uHt l- r rne
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E : I t.I TTI F T]FJ AFF'F I.{II I Xlla I rBrat ron : Plill5 14'15 :
l-lne rE t o r' I Il:
I-li rant Time :
In jected nt:
Everyreen Andyticll, Inc"
4036 Youngfield St, Wheet Ridge CO
(303) 475402r
Method Bhnk Report
a
80033
Lrb Semple ID 3
Date Prepared 3
I)ete Anetfzed 3
R8052698
05126198
05126198
Client Proiect IID :
I,eb Work Order:
Lrb FiIe IID :
Efrective Dilution :
7585
98-1934
>\X8635::V3
I
Method: SWE200A voA 8260 pg/Kg
Analyte GAS #Goncentration RL PQL
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
67a64.1
7143-|2
7*274
7*2*2
74-83-9
U
U
U
U
U
10
0.5
1
1
1
100
5
5
5
10
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chloroberzene
Chloroethane
7&93-3
7*1il)
5e2$5
10&9G7
7il0-3
U
U
U
U
U
10
1
1
1
1
100
5
5
5
10
24hloroethyMnylether
Chloroform
Chloromethane
Dibromochloromethane
1 , 1-Dichloroethane
110-7ffi
67663
7ffi7-3
12HU1
7**3
U
U
U
U
U
3.2
0.5
1
1
1
10
5
10
5
5
1,2-Dichloroethane
1 ,l-Dichloroethene
cis-1, 2-Dich loroethen e
trans.1, 2-Dich loroethene
1 ,2-Dichloropropane
10746-2
7S35-4
156-59-2
156€0-5
78€7-5
15
15
15
15
15
U
U
U
U
U
cis-l, 3-Dichloropro pene
trans-l, 3-Dich loropropene
Ethylbenzene
2-Hexanone
Methylene chloride
10061{1-5
10061{25
1 00-,{1-4
591-78€
7ffi9-2
5
5
5
50
5
U
U
U
U
U
1
1
0.5
5
1
4-Methyl-2-gentanone
Styrene
Tetrachloroethene
1,1,2,2-Tdrachloroethane
Toluene
10&1G1
1ggr.{l-5
127-18.4
79134-5
108-88-3
U
U
U
U
U
5
1
1
1
0.5
50
5
5
5
5
1 ,1 , 1-Trichloroethane
1,1,2:f rich I oroetha ne
Trichloroethene
Vinyl acetate
Vinyl chloride
71-sffi
79-0()-5
79{1€
108-05-4
7ffi14
U
U
U
U
U
0.5
1
1
5
1
5
5
5
50
10
Total Xylene 133G20-7 0.5
Surrogate Recovery
1,2-Dichloroethane-d4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl uoro benzen e (SS-3)
106%
104%
102%
QC Lirtitr
75 - 110
82 - 125
74 - 115
aurnmn U-Nd Detcctcddth ReportingLimit (RL)
, - Anrlytc drirdrdbelow Prr.ticd Annititatim Limit (PQL)
S - Spikc Rccovery outside acceptd rccovery limits
B-
5/2&9E l2:l l:59 PM
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OLYIIJIPUS ENVIRONTI/I ENTAL, INC.
ANALYTICAL DATA VALIDATION FORM
ClienUProje
Work Order#:7s8-<Laboratory:
Olympus' Sample ldentification Numbers : 5tq - t 4 O A - t -tt SA - Ht.fA 4 -eoi
-d -l{-J- /-3 -l'?-l 5'- 3-J
-3-8 h 3-/3
EPA Analytical Methoa.S/) g,*06-'I @, t
Data Completeness
-318.cl ,
b Sgao
Results received out of
Are completeness results acceptable? MN):
q5 -Q
pecte( =/rt o/o._gx@
Comments:
Defensibility
Chain-of-Custody form present and signe d?(Y lN):
Samples stored and/or shipped cool? MN):
Preservative present in sample containers? (Y/N):
Are d efen si bility parameters acceptablg! ff/N) :
Comments:
Holding Time
Were samples extracted within acceptable holding times? (Y/N) , n J/
Were samples analyzed within acceptable holding times? (Y/N) d ,l
Are holding time parameters acceptable? MN):
Comments:
Page 1 12t15t97
Equipment and Trip Blank Analyses
Appropriate number of equipment blanks submitted? (Y/N): lfle
Appropriate number of trip blanks submitted? MN): {/t
Are results above method detection limits? (Y/N): [/n
lf yes, provide concentrations detected and concentrations of those compounds in
sample data if present:
Method Blanks
Are results above method detection limits? MN): Y)D
lf yes, provide concentrations detected and concentrations of those compounds in
sampte data if present:
Surrogate Recoveries
Are re@veries within acceptable
lf no, list results outside of limits.
percent recovery control limits? CflN)
Are duplicate RPDswithin acceptable limits? UlNf ,4-P- -=46,17, b1o 24**
lVlatrix Spike and Spike Duplicate Recoveries
Are recoveries within acceptable percent recovery control limits? (Y/N) 9,
= / l{,Jrl =/o5,= Qo.4 V"
= 83a,L7,3 /34
-t4. V q
lf no, list results outside of limits: Atcd.., . I 3,7?o t(Pb .( - ' -,Jo , J'Attao^r,r.. 2oo,o7o
RPa l,ru'* =.tt r t)uly'- 0 'to*, = 4o'1r" Rh 4 ' ' =.lo
Page 2 letlstsT
lfno, listresultsoutsideoflimits. /,t =--',a7o ^ t/"''L=5f4, (' ')
'J=3o , J- C = .fr,S 7o Rft)
Laboratory Duplicates
Are RPDs for laboratory duplicates within acceptable ranges? (Y/N):
lf no, list results outside of ranges.
t{/n
Field Duplicates
Calculate and list RPDs for field duplicates. /(/A
Do the RPDs appear appropriate?
OA/QC Discussion
Page 3 12115t97
,/\Euergreen,4.,/|. Analytical
A";;;,ratory
May 27,1998
MIKEBACKE
OLY},{PUS E}I\IRONMENTAL, INC.
54A9 KENDALL STREET
BOISE, ID 83706
Lab Work Order: 98-1985
Client Project:7585
Dear Mke Backe:
Enclosed are the analytical results for the samples shown in the Laboratory Work Order
Summary. The enclosed data have been reviewed for quality assurance. Ifyou have any
questions concerning the reported information, please contact Mark Mensik, Quality
Assurance manager.
SAMPLE DISPOSAL: Except for high level mercury Q26O ppm) samples, EAL will
dispose of all samples one month from the date of this letter. If you want samples
returned, please advise us by mail or far as soon as possible.
RECORDS RETENTION: Effective fanuary l, 1996 we will retain a copy of this
project report and supporting data for a period offive years. It has been our experience
that a five year retention period is more than adequate to respond to client inquiries. If
you want the project file sent to you after the five year period, please return a copy of
this letter.
The invoice for this work will be mailed to your Accounts Payable department shortly.
Thank you for using the services of Evergreen Analytical.
Sincerely,
Carl Smits
V.P. Operations
Evergreen Analytical, Inc. 4036 Youngfield St. Wheat Ridge, CO 80033-3862 (303]1425-6027 FAX [phone]
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Evergreen Analytical, Inc.
4036 Yorrngfield St, TYheet Ridge CO
(303) 4zS^6a/l
o
80033
Client Project ID : 7585
Lrb TYork Order : 98-1985
Sempte Mrtrir : Water
Lrb Fite ID : >I5837::Y4
Method Bhnk : RB05199EA
Efrective Dilution: I
Cticnt Semple II)
Lrb Semple ID
IDetc Coltected
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lvf\M-l
98-1985{1A
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0sl19l98
0slL9l98
Method: SW8260A HazardouE Substanee Urt - Volatile Organicr pgfl-
Analyte cAs #Concentration RL PQL
Acetone
Berzene
Bromodichloromethane
Bromoform
Broinomethane
676r1
7143i2
7*274
7*2*2
7+8$9
20J
U
U
U
U
10
0.5
1
1
1
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5
5
5
10
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Carbon disulfide
Carbon tetrachloride
Chloroberzene
Chloroethane
7&93-3
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56-2&5
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7il0-3
U
U
U
1J
U
10
'l
1
1
1
100
5
5
5
10
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Chloroform
Chloromethane
Dibromochloromethane
1 ,1-Dichloroethane
1 10-75-8
67€&3
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7*3+3
U
3J
U
U
U
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1
1
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5
10
5
5
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1 , 1-Dichloroethene
cis-1, 2-Dichloroeth en e
trans-l, 2-Dichloroethene
1 ,2-Dichloropropane
107-06-2
75-35-,4
156-59-2
156€0-5
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28
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1
1
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5
5
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Ethylbenzene
2-Hetcanone
Methylene chloride
10061-01-5
10061{2€
1 00!41r4
591-786
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5
5
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U
U
U
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Styrene
1,1,z,z-Tetrach loroetha ne
Toluene
1, 1, 1 -Trichloroethane
10&10-1
10G42-5
79-34-5
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71-5#
U
U
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5
1
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190
25
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Surrogate Recovery
1,2-Dichloroethan+d4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl uoroberzene (SS-3)
108%
155%
116%
QC Lirftr
82 - 116
89 - 107
87 - 109
SX
SX
U - Not Deneded etthe R.portiog Limit (RL)
J - Anrl,,tc dctcc'tcd bclow Pradic.l annititrtion Limit (PQL)
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Evergreen Analyticel, Inc.
Yumgfield St, Ttrheet Ridge CO
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7585
9t-1985
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>\18621::Y3
RB052298
500
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Tetrachloroethene 127_1U 69000 500 2500
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1,2-Dichloroethane-d4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl u o roberzene (SS-3)
102%
100%
100%
AC Lfrft3
82 - 116
89 - 107
87 - 109
U - Not Dctcctcd etthc Rcporting Limit (Rt)
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E - Reportcd quditrtioonnge
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4036
Evergreen Analyticel, Inc.
Yumglield SL, Whert Ridge CO
(303) 47s4o2r
o
80033
Client Project ID : 7585
Leb TYork Order : 9t-1985
Srmple Mrtrir : Water
Lrb tr.ite IID : >Ij83E::V4
Mcthod Bhnk : RB05199tA
Efiective Dilution : I
Client Semple IID
Leb gemple ID
Dete Collected
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98-198542A;
05lrsle8
05lt6le8
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Analytc CAS #Concentration RL PQL
Acetone
Berzene
Bromodichloromethane
Bromoform
Bromomethane
676r1
7143-|2
7*274
7*2*2
74€&9
U
U
U
U
U
10
0.5
1
1
1
100
5
5
5
10
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
7&9&3
75-1il
5&23-5
10&9G7
7$OG.3
U
U
U
3J
U
10
1
1
1
1
100
5
5
5
10
24 h I o roethylvi ny leth er
Chloroform
Chloromethane
Dibromochloromethane
1 ,1-Dichloroethane
11G7S8
67 66-3
7+87-3
12U8-1
75-34-3
U
U
U
U
U
3.2
1
1
1
1
10
5
10
5
5
1 ,2-Dichloroethane
1 , l-Dichloroethene
cis-l,2-Dichloroethene
tra n s. 1, 2-Dich loroeth ene
1 ,2-Dichloropropane
107{6.-2
7S35-,4
156-59-2
1ffi0-5
7&.87-5
6
340
15
1
1
1
1
1
5
5
5
5
5
cis-1, 3-Dishloropropene
tra ns-l, 3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
10061{1-5
10061{2€
1 00-,41-4
591-78{
7U09-2
5
5
5
50
5
U
U
U
U
U
1
1
0.5
5
1
4-Methyl-Z-pentanone
Styrene
1,1,2,zfetrach lo roetha n e
Toluene
1 , 1 , 1-Trichloroethane
1 08-1 0-1
100.,4,2-5
79-3+5
10&8&3
71-55EGt
50
5
5
5
5
U
U
U
U
U
5
1
1
0.5
0.5
1,1,2-Trich loroeth a ne
Trichloroethene
Vinyl acetate
Vinyl chloride
Total Xylene
79-00-5
7$01€
108-05-4
7fi14
133&20-7
290
U
1J
U
1
1
5
1
0.5
5
5
50
10
5
Surrogate Recovery
1,2-Dichloroethane-d4 (SS-1 )
ToluenldS (SS-2)
4-Bromofl u oroberzen e (SS-3)
87%
159%
113%
QC Lirnit3
82 - 116
89 - 107
87 - 109
SX
SX
U - Not Dcicdcd rtth Rcporting tjmit (RL)
, - Anrl)rtc dctcctod bclow PrE ticrl aunititrtion Limit (PQL)
E - Reportcd fabovc quditdonrange
thc rrf&iatod Mdhod Blank
Spiks Rooovcry oubi& rcccdd rccovcry limitr
Coryound &rrtrdrborrc rqufmy fmit
Poa fuc to mrtrix idcrftncocc. Sec
s-
a_
QurHtrcn:
B-
Analyst
x-
diltnim.
5n5/98 II:15:19AM
o
4036
Evelgreen Anetyticd, Inc.
Yungtield St, Whcrt Ridge CO
(303) 4 S4t2l
o
&n33
Client Srmple II)
Lrb Semple II)
Detc Collected
Drtc Received
Dete Prepered
Drtc Anelped
IvfW-2
98-1985{/2A:
051L5198
05lt6l98
0512u98
05lzu98
Client Project II)
Lrb Work Order
Semple Metrir
Lrb X'ile ID
Method Blenk
Efrective Dilution
7585
98-1985
\[ater
>\18628::V3
RB052298
500
Method: SW8260A Hazardour Substanea UJt - Volatlle Organicr pgrL
Analyte cAs #Concentratlon
Tetrachloroethene 127-1&4 81 000
Surrogetr Ftecovery
1,2-Dichloroethan+d4 (SS-1 )
Toluened8 (SS-2)
4-Bromofl uoroberzene (SS-3)
10/}%
97%
97%
OC Lfrfts
82 - 116
89 - 107
87 - 109
@rUncn: U - Not Dcicctcd atthG RePorting Limit (Rt)
J - Andytc dctccted below Prqcticrl atranititdim Limit (PQL)
E - Reportcd @ qryfitrtlm rlngc
S - Spikr Rccovcry qrEi& rccfld r€coycry limits
I - Coryouod dcnccrcd rbove regulstry limil
B-Mcthod Bhk
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5n5/gS tI:15:18AM
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oLlmPUS ENVIRONMENTAT, lNC. .
€'j Fr:r c/ c=_icr-: =r G'.V FC R.\l . X LS CS!,ifcrra teflGJSIl
Evergreen Analyticel, Inc"
NX Yumgfield St, TYheet Ridge, CO
(303) {254021
o
80033
Client Semple ID
Lrb Semple ID
Dete Co[ected
Drtc Received
Detc Preprred
Detc Anrtyrcd
lvfw-4
9E-19E5{34
05/15/98
05116198
05DA98
0slzu98
Ctient Project IID
Lrb TYort Order
Semple Mrtrir
Lrb f ile II)
Method Bhnt(
Efiective Dilution
75E5
98-1985
\Mater
>V8619::V3
RB052298
10
Hazardous Substanee U3t - Voletllc Organlcr pg/L
An
Acdone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
CAS #
67 64-1
7143-i2
7*274
7*2*2
7€&9
Concentration
U
U
U
U
U
RL
100
5
10
10
10
PQL
1000
50
50
50
100
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chloroberzene
Chloroethane
7&9&3
7*1ffi
5&23-5
10&90-7
7il&3
U
U
U
U
U
100
10
10
10
10
1000
50
50
50
100
24 h I o roethylvi nyl eth er
Chloroform
Chloromethane
Dibromochloromethane
1 , 1-Dichloroethane
11G7ffi
67{&3
74-97-3
124-4,(J-"1
7$3+3
U
U
U
U
U
32
10
10
10
10
100
50
100
50
50
1 ,2-Dichloroethane
1 , 1-Dichloroethene
cis-1, 2-Dich loroethens
tra ns-1, 2-Dich loroeth ene
1 ,2-Dichloropropane
107-06-2
75-35-,4
156-59-2
156€0-5
78-87-5
U
U
390
10J
U
10
10
10
10
10
50
50
50
50
50
cis-l, 3-Dichloropropene
trans-1, 3-Dichloropropene
Ethylberuzene
2-Hexanone
Methylene chloride
10061{1-5
10061-02€
10G41-4
591-78€
7549-2
U
U
U
U
U
10
10
5
50
10
50
50
50
500
50
4-Methyl-Z-pentanone
Styrene
1, 1,z,z-Tetrach I o roeth a n e
Toluene
1 , 1 , 1-Trichloroethane
1 08-1 0-1
100-42-5
79-34-5
108€&3
71-55=6
U
U
U
U
U
50
10
10
5
5
500
50
50
50
50
1,1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
Total Xylene
7900-5
79-01€
108-0s4
7fi14
1330-20-7
zso
10
10
50
10
5
50
50
500
100
50
U
U
U
Surrogate Recovery
1,2-Dichloroethan+d4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl uorobenzene (SS-3)
98%
106%
102%
Qc Lin*ti
82 - 116
89 - 107
87 - 109
aUltrcn U - Nd Dctccted rtthc Repqting Umit (RL)
J - Anrl)rtc Mxrdbclovy-Practicrl Aunititrtim Limit (PQL)
E - Rcportcd
Spib Rmvery outsi& ssetrd rccovery limits
Coryound &rrt,rdeborrc rcguLtory timit
s-
a_
Analyst
x-
5/25/98 II:15:504M
Evergreen Anatyticll, Inc.
4036 Ymnglietd St, Wheet Ridge CO
o
t0033
(303) 4r5qi021
Client Project IID : 7585
Lrb lVork Order : 98-1985
Semple Mrtrir : Water
Lrb X'iIe IID : >\l8529::W
Method Bhnk : R805X298
Efrective Dilution: 500
Client Semple IID
Lrb Semple IID
Detc Cotlected
Drtc Received
Irrts Prepered
Drtc Anelped
'IvfW-4
: 98-198543A
05/15/98
a5n6le8
05nz98
05nae8
Method: SW8260A Hazardous Substance Ust - Volatile Organicr ru/L
Analyte cAs #Concentration RL PQL
Tetrachloroethene 127-1$-.{79000 500 2500
Surrogete Recovery
1,2-Dichloroethane-d4 (SS-l )
Toluenld8 (SS-2)
4-Bromofl uoroberzene (SS-3 )
96%
96%
97%
QC Lhitr
82 - 116
89 - 107
87 - 109
U - Not Detcded atthe Reporting Ijmit (RL)
J- Anrlyc drtoc/rcdbclow Pnctic8l auninrtion Limit (PQL)
loa aboX $rilitdimrsngc
thc rdocirtod Mcnhod Blrnk
S - Spilcc Rcovery oilside scogdd rcoovcry limits
. - CqorrnA dctcdod above reguletry limit
Qudlf,cn:
Analyst 5nSD8 It:15:194M
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GRouND torER sAMpuNG tNFoRilrAnoGRlr
oLWPUS ENVTRONMENTAI, lNC. .
c:' tlra c/ca-fcr-:=r G'.V F C R.tt .X LS
Evergreen Analyticel, Inc.
4A36 Youngfield St, YYheet Ridge, CO
(303) 4rs{r021
o
8m33
Client grmple II)
Lrb Semple II)
Dete Collected
Drte Rcceived
IDetc Prepered
Date Analped
I\d\[-3
98-1985444
05/r5/er
05lt6le8
05lzue8
a5DA98
Client Project II)
Lrb lYor* Order
Semple Mrtrir
Lrb File IID
Method Bhnk
Efrective Dilution
7585
98-1985
Water
0::V3
R8052298
10
Method: SW8260A Hazardous Substanoe LIrt - Volatlle Organlcr pg/L
Analytc CAS #Concentratlon RL PQL
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
67 6 l-1
714&|2
7*274
7*2*2
74-83-g
U
U
U
U
U
100
5
10
10
10
1 000
50
50
50
100
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
7&93-3
7*1il
56-23-5
10&90-7
7il0-3
U
U
U
U
U
100
10
10
10
10
1 000
50
50
50
100
2€hloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
1 ,1-Dichloroethane
11G7S8
67663
74-87-3
124-4,8-1
75-U-3
U
U
U
U
U
32
10
10
10
10
100
50
100
50
50
1 ,2-Dichloroethane
1 , 1-Dichloroethene
cis-l, 2-Dichtoroethene
tra ns-1,2-Dichloroethene
1 ,2-Dichloropropane
107-06.-2
75-35-,4
156-59-2
156€0-5
7g-97-5
U
50J
210
U
U
10
10
10
10
10
50
50
50
50
50
cis-l, 3-Dichloropropene
tra ns-l, 3-Dich loropropene
Ethylbenzene
2-Hexanone
Methylene chloride
10061{1-5
10061 {/2{,
1O(Hl-4
591-786
7ffi9-2
50
50
50
500
50
U
U
U
U
U
10
10
5
50
10
4-Methy)-2-pentanone
Styrene
1,1,z,2-Tetrach loroetha n e
Toluene
1,1,1 -Trichloroetha ne
1 08-1 0-1
14042-5
79-3+5
10&88-3
-71-55€
U
U
U
U
U
50
10
10
5
5
500
50
50
50
50
1,1,2-Trichloroethane 79-0G5 U 10 50
Trichloroethene 79-016 350 10 50
Vinyl acetate 108-05-4 U 50 500
Vinylchloride 75{14 10 J 10 100
Total Xylene J33G?G7 U 5 50
Surrogate Recovery
1,2-Dichloroethane-d4 (SS-1 )
Toluenld8 (SS-2)
4-Bro mofl uoroberzen e (SS-3 )
102%
106%
103%
AC Limits
g2 - 116
89 - 147
87 - 109
U - Nd Dctociod rtth R€porting I"imit (Rt)
J - And)rtc ddcctcd below Prrsticrl aunitfrtU Limit (PQL)
S - Spikc Rmvcry odri& rcccptcd rccovcry limitr
' - CompounA dcbctcd rbow rcgulrtry limil
@rEficn:
X- Nd Applicrblo.
5/25/98 Il:15:Sl AM
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[nenator Ilt: ['(IHQirant Time : FBuS?2 1.]:c+5Injected at: 9ELl 522 l3:2tl
Evergreen Analyticel, Inc.
40fi Youngfield St, TYheet Ridge CO
(303) 4?ffi21
o
tm33
Client Semple IID
Lrb Semple ID
Dete Collected
Detc Received
DetcPrepered
Dete Anelped
IvfW-3
98-198544A
0sltslgE
0slt6l98
05D2/98
0slzu98
Client Pmjet IID
Lrb lYork Order
Semple Mrtrir
Lrb File ID
Mcthod Blrnk
Efrective Dilution
7585
9E-19E5
Water
>\18630::V3
RB052298
500
Method: SW8260A Hazardous Substanee U3t - Volatilc Organicr pg/t
Analyte cAs #Concentration
Tetrachloroethene 127-18-,{2500
Surrogrtc Recovery
1,2-Dichloroethan+d4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl uoro berzene (SS-3)
99%
100%
100%
QC Lhits
82 - 116
89 - 1A7
87 - 109
U - Not Detccted atthe R.porting Limit (RL)
J - Anrl},tc drjrer,trdbelow PracticEl annititetion Limit (PQL)
S - Spikc Rccovcry outsi& rccqtrd rccovcry limits
. - Cqoua dctcstcd ebovc rcguletry limit
Qur[f,cn:
B-
5/25/98 I I:15:51 AM
TNTF{1. I OT.T IHREIiffTD6RFIIi
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148*r*l
_ - -1IHf4|J*\
].BE'**J
_ -1
::::,:
br4 u rrtrl
, - -. -1+aus brfl
_ _1ct,lrt4tfl
-1H
,trlllt-l
r+
I
,ag,
ttt_l
1E LE i4
Data file: >UE63t] ::U}
l-{a me : '.r B - 1.9 B 5 - ll 4tt l,(:l .
11 isc: SfimP rlr=5u[l
i,l i:iLe: tD_824::tlTTitle: In rTl r rr-lh: F\rrrf-{n}}(
I .,e=t l-.a I i.hra t i nn : Ffi lJStf 1. 1.3 :
flperatnr Ill: t{: }H
lf,i rant Time : PBllS?.2 1.n:'L?Inj*r:ted at: PBtt T;2? .1 7255
Ie:
TD:
t-t p f, Ll1 TiL.I I NT
51
Qr-rant flur tFrrt fitnet rirnrent
I'l'l'l'I'l18 EB AE
tJ['lHs Hf -f l it-lnl.ast Qca
,r\,JLt 630: : [!?tJnfi 1.
ftrne: (nnne)'
GRou ND vt}R, sAMpuNG tNFo RlilAnotoRlr
oL'\mPUS ENVIRONMENTAI_ lNC. .
€'-'n":r e/€s_lcr- =r G'.V FC R l.l.XLS
Evergreen Analytical, Inc"
4036 Youngfield St, Wheet Ridge CO
(303) 42S4A2r
o
80033
Client Sempb II)
Lrb Srmple ID
IDete Collected
Detc Received
Drts Prepered
Detc Anrlyzed
E.B.
98-198545A
051t5198
051t6t98
0snae8
05nu98
Client Prclcct II)
Lrb Work Ordcr
Srmple Mrtrir
Lrb File ID
Mcthod Btrnk
Efrective Dilution
7585
9t-lgg5
Water
>\X8518::V3
RB052298
I
Method: SW8260A Hezardous Substanee U3t - Volatile Organicr Units:trg/L
Analyte cAs #Concentration RL PQL
Acdone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
67 6l-1
7143-2
7*274
75-25-2
74-83-9
U
U
U
U
U
10
0.5
1
1
1
100
5
5
5
10
2-Butanon€
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
7g-9&3
75.-1il
56-23-5
10&90-7
75-00-3
U
U
U
U
U
10
1
1
1
1
100
5
5
5
10
2€ h I oroethylvi ny I eth er
Chloroform
Chloromethane
Dibromochloromethane
1 ,1-Dichloroethane
11G7ffi
67€613
74a87-3
12448-1
75-34-3
10
3.2
1
1
1
1
10
5
10
5
5
U
U
U
1,2-Dichloroethane
1 ,l-Dichlorosthene
cis- 1, 2-Dichloroeth ene
trans- 1,2-Dichloroethene
1 ,2-Dichloropropane
107-06-2
7ffis-4
156-59-2
15ffi0-5
7847-5
5
5
5
5
5
1
1
1
1
1
U
U
U
U
U
cis-1, 3-Dichloropropene
trans-1, 3-Dishloropropene
Ethylbenzene
2-Flexanone
Methylene chloride
10061-01-5
10061 42$
100-41-4
591-78€
7fr9-2
5
5
5
50
5
U
U
U
U
U
1
1
0.5
5
1
4-Methyl4-pentanone
Styrene
Tetrachlorodhene
1,1,2,z-Tdrach loroetha n e
Toluene
10&1el
19942-$
127-18-,4
79-34-5
109-gGr
50
5
5
5
5
U
U
U
U
U
5
1
1
1
0.5
1 , 1 , 1-Trichloroethane
1,1,z-Trich loroetha ne
Trichloroethene
Vinyl acetate
Vinyl chloride
71-55€
79-00-5
79-016
108-05-d
7ffi14
U
U
U
U
U
0.5
1
1
5
1
5
5
5
50
10
Total Xylene 1330-2A-7 0.5
Surrogate Recovery
1,2-Dichloroethan+d4 (SS-1 )
Toluen+d8 (SS-2)
4-Bromofl uoroberzen e (SS-3 )
95%
96%
94%
QC Lir*t3
82 - 116
89- fi7
87 - 109
aurUOcn U - Not Dctcctcd dthc Reporting Limit (RL)
J - Andy& ddccted below PEacticrl Qranititetion Limit (PQL)
E-Rcportod s1l{rfa!211u1rir!do1.:p:
S - Spiks Rccovcry outsi& accept€d rccoy€ry limib
r - Coryoud detccilcd above reguldry limil
Analyst
B - Antt)'tc atcd Mcnhod Blank
X - Not Appliceble.
5n5/98 II:15:52AM
TOTSL I OI{ CHE O}iRT O6RF{}I
Fi 1e )tlB61B 35.S-e6B.B EmLr,'18-1!E-6!j
TIIJ
4ErEr 8Ag 1 ? ilFJ 1 6AE
F;
Iw({
I.!,ln
148gA\
_ _ -11;{tcoool
legrr*]
1 1 aoooJ--'-.- - -
J
{ rafimOr'f I.trE UUs,t.Fl
J
eB6B&l
{
BBEEE
I
7ggt3$*{
6aa--j
tttefiioJt.rt.r(. -"J
4aEu*J
+'l ra fi.a - Irf E crqrqr I
l
eEBBB-l
{180tls1
_1W
[-]ata Fi J e : >Ul3('L8 : : U]l.lame: 9E-L?85-li5ff Ki-llisc: SAHP l-)F=l
Irl FrIe: ID_B'J4::lJTTitIE: IN TTI F FDT;i ftPT]ENT}IXLast llal ibrat lEn: 98052't'I]:
llnerator Ill: l(lm
-tl.luant Time : FBll 52? 1.?j:5tlInjected at: P80522 'J?z?ti
tlluant filr tprrt f i Ie:Instrirment Itf:
LB c14 'ze
UUHs mf THnllLast Qcn
oUS& 1-Q : : [!?tJtlA 1.
F{INF
53
8261I fiI l-ime: (fior-re)
*
I
(.'1
Itl
Evergreen Analytical, Inc.
4036 Younglield St, TYheet Ridge CO
(303) 42s4o2r
Method Bhnk Report
o
t0033
Lrb Semple IID :
Detc Prepercd 3
Drte Anrt]"zed 3
RBO5I99EA
05lL9l9t
05/19/98
Clicnt Prciect ID 3
Lrb Wodr Order:
Lrb FiIe IID :
Efrective Dilution :
7585
9t-1985
>158n::V4
I
Msthod: SW8260A voA 8260 pg/t
Analyte cAs #Goncentration RL POL
Acetone
Berzene
Bromodichloromethane
Bromoform
Bromomethane
67611
714&|2
7*274
75-2$i2
74-8&9
U
U
U
U
U
10
0.5
I
1
1
100
5
5
5
10
2€utanone
Carbon disulfide
Carbon tetrachloride
Chloroberzene
Chloroethane
7&93-3
7*15-0
5&23-5
10&90-7
7ilG3
U
U
U
U
U
10
1
1
1
1
100
5
5
5
10
2€h lo roethylvi nyl eth er
Chloroform
Chloromethane
Dibromochloromethane
1 , 1-Dichloroethane
110-7$8
67663
74 g7-3
12UU1
7S34-3
U
U
U
U
U
3.2
1
1
1
1
10
5
10
5
5
1 ,2-Dichloroethane
1 ,1-Dichloroethene
cis-1, 2-Dichloroethene
tra ns- 1, 2-Dich loroeth ene
1,2-Dichloropropane
107{,6-2
7S35-,4
156-59-2
156SG5
7&87-5
U
U
U
U
U
1
1
1
1
1
5
5
5
5
5
cis-l, 3-Dichloropropene
trans-l, 3-Dichloropropen e
Ethylbenzene
2-Hocanone
Methylene chloride
10061-01-5
10061-02€
1 00-41 -4
591-78€
7ffi9-2
5
5
5
50
5
U
U
U
U
U
1
1
0.5
5
1
+Methyl-2-pentanone
Styrene
Tetrachloroethene
1,1,z,z-Tetrach loroeth a n e
Toluene
10&1G1
10H2-5
127-18-,{
79.3+5
10&88-3
50
5
5
5
5
U
U
U
U
U
5
1
1
1
0.5
1 ,1 , 1-Tricfiloroethane
1,1,z-Trich loroeth a n e
Trichloroethene
Vinyl acetate
Vinyl chloride
71-55-6i
79-00-5
79{1S
108-05-4
7ffi14
U
U
U
U
U
0.5
1
1
5
1
5
5
5
50
10
Total Xylene 133G20-7 0.5
Surrogate Recovery
1,2-Dichloroethaned4 (SS-l )
ToluenldS (SS-2)
+Bromofl uoroberzene (SS-3)
105%
105%
101%
GIC Limitr
82 - 116
89 - 107
87 - 109
aueUficn: U - Not Dctodod rttbc Rcporting Umit (RL)
J - Anrl)rtc dctcciled below Practic8l aunifttlon Limil (PQL)
S - Spikc R.eovcry outri& rccqtrd r€covcry limitr
X- Nd Applicabla
Analyst 5n5/9E I I:I5:55 AM
TOTSL IOT.I CHROTiffTOGRBTi
tr i I o 'rl Al1iJ7 ?ii E-2fiA' Ota --b r ;,J.r.bt tJtJtL' bl-.uat-.
4fi4
lml I.l-ala t-\ r
8RE
AH
1 ?AA I 6mF
RB'.ITIC
P4Eft
f,
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56Eo88j
5eB F:A+4
[Esr**1
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4ssrr"]
3f,R AP;;A---!
3eBtrl
eSBBBE
e4Brr*l
A A A^,^.^ 1eUBU'JEFI
16Ess6l
1Fr,1rifiJ
;;;;;
{40EBE
_1w
14 Ib
Data tiJe: >l r'877::U4Hame: REtlSt9?8fi Hl .
P1 isn: llHl t( DF=1
Irl Frte: ID_U?B:;QTTitIE: IN TTI F TNR APFFF{NI}<l.ast llatihratirrn: ?'4n514 1-5:
Quant fhrtput fiInstrirment IelID:
R26LI AI Tinre:F{ I I'{F'r9
"l frs77: : 82* l15l -ft|.I
tJ[-lFls Hf T Hnnl.ast l.lea tnnne)
flneratnr Il-): KIll
Qi rant Time : 9B[51.9 1.8:28Injentecl at: ?s05'II l8:tl 6
o
4036
Evergreen Analytical, Inc"
Yumgfield St, TYheet Ridge CO
(303) {t$^6s21
Method BhnI( Beport
o
80033
Lrb Semple ID 3
DetcPrcpered :
Ilete Anellzed 3
RBo52298
05D2/98
05lLu9E
Client Project IID 3
Lrb lVor{r Order :
Leb FiIe IID :
Efrective Dilution :
75r5
98-1985
>V8615::V3
I
Method: SW8260A voA 8260 pg/L
Analytl CAS * Goncentratlon RL POL
Acdone
Berzcnc
Bromodichloromethane
Bromoform
Bromomethane
67 64-1
714&i2
7*274
7*2t|2
74€3-9
U
U
U
U
U
10
0.5
1
1
1
100
5
5
5
10
2€utanone
Carbon disulfidc
Carbon tetrachloride
Chloroberzene
Chloroethane
7&9H
7*1m
5&23-5
10&90-7
75{}013
U
U
U
U
U
10
1
I
1
1
100
5
5
5
10
2-C h loroethylvi nyl dh er
Chloroform
Chloromethane
Dibromochloromethane
1 , 1-Dichloroethane
110-7ffi
67 66-3
7H7-3
124-4,8.1
7**3
U
U
U
U
U
3.2
1
1
1
1
10
5
10
5
5
1,2-Dichloroethane
1 , 1-Dichloroethene
cis-1, 2-Dichloroethene
tra ns-l, 2-Dich loroeth ene
1,2-Dichloropropane
107{6.-2
7S35-,4
15&59-2
156€0-5
7g-97-5
U
U
U
U
U
1
1
1
1
1
5
5
5
5
5
cis-1, 3-Dichloropropene
tra ns-l, 3-Dich loropro pene
Ethylbenzone
2*lo<anon€
Methylene chloride
10061-01-5
10061{26
1 00-,{1-,{
591-78{
7ffi9_2
5
5
5
50
5
U
U
U
U
U
1
1
0.5
5
1
4-Methyl?-gentanone
Styrene
Tetrachloroethene
1,1,2,2-Tetrach loroetha ne
Toluene
10&1G-1
10G42-5
127-18-,{
7$34-5
108-8H
50
5
5
5
5
U
U
U
U
U
5
1
1
1
0.5
1, 1, 1 -Trichloroethane
1 ,l,2Jrichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
71-55.O
79-0C5
79-01€
108-05-4
7fi14
U
U
U
U
U
0.5
1
1
5
1
5
5
5
50
10
Total Xylene 133&2V7 0.5
Surrogate Recovery
1,2-Dichloroethane-d4 (SS-1 )
Toluen+dg (SS-2)
4 Bromofluorobenzene (SS-3)
98%
99%
100%
QC Limitt
82 o 116
89 - 107
87 - 109
U- Nd Ddodcd etthc Reporting Limit (RL)
, - Anrlytc &r,trrdbelow Prasticrl annititrti,on Umit (PQL)
S - Spikc Rrcovcry outside acccptd rccovery limits
X - Nd Appliceblc.
aurUncn:
5/25/98 II:15:564M
TNTHI. I OTi I]HRflIif,TOGEPIi
tiiIg 'rtJRAlt ?t fi-2AB A. a -'- , . b"-'-'J S.u a'-' l-u'-' a -J emu. R8tl.5e?1A liltiEL!,i BF-tTII
186 Bt3
{ { r?r?l?I.l l, c,
",
4fi4 80F 1?AF: I 6afi PAfiA,,. t,.r t.,,r,,. t,., r.,, l .,r, !, 1.,, t,., t.,.t r.
1. BBBE
A.aa.l
TtulJll
AAAAeiv)ul?J
7BffB
e,aga
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F. F..-. F.
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f'l isc: l1t-'!l F( [-]F=1
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le:ID:^U[i 6]5::Q?t-JllH 1.
Irl Fite: ID_11 ';4::QTTrtJE: II-I FTI F TilR AFP[.F{NIX NIF{T:l.ast tlali.bration: 9Bll 521. 1"]:53 UL-lFt= mf f Hnl-l fi 7 r, tl Al.ast llcat Tirrre: {none}'
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F B rl 5??. 1. 't : ?,7P80527 I 1 : n]
Fuergreen
A^trY:;:r:ry
r-r I 4? -?JUND)
Wl, 1998
MIKE BACKE
OLYMPUS ENVIRONMENTAL, INC.
5409 I(ENDALL STREET
BOISE, ID 83706
Lab Work Order: 98- 198.5
Client Project: 7-585
Dear Mike Backe:
Enclosed are the analyical results for the samples shown in the Laboratory Work Order
Summary. The enclosed data have been reviewed lor quality assurance. If you have any
questions concerning the reported information, please contact i\{ark Mensik, Quality
Assurance mana_qer.
SAMPLE DISPOSAL: Except for high level mercury (>260 pprn) sanrples, EAL will
dispose of all samples one month from the date of this letter. If you want samples
returned, please advise us by mail or fax as soon as possible.
RECORDS RETENTION: Effective January l, 1996 we rvill retain a copy of this
project report and supporting data for a period offive years. It has been our experience
that a five year retention period is more than adequate to respond to client inquiries. If
you want the project file sent to you after the five year period, please return a copy of
this letter. -
The invoice for this work will be mailed to your Accounts Payable department shortly.
Thank you for using the services of Evergreen Analytical.
Sincerely,6m-u WtoffJ
.^!
i' \'
Kr?ubcTu0 €y ,ffiuey
or ,/, 118
NS
\ Carl Smits
fl
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OLYMPUS ENVIRONilIENTAL, INC.
ANALYTICAL DATA VALIDATION FORM
ClienUProject:Reviewer
Work Order #:_r{ 85 Laboratory:
Olympus Sample ldentification Numbers: mr.D-t , tnr! -A, rnd - a , Onf,J-r-[,
5/,5-:'
EpAAnaryticarMethod, St*tg4c zn ,41 t 8a ao/l
Data Completeness
Results received out of expected =/00 o/o.
Are completeness results acceptable? MN):
Comments:
Defensibility
Chain-oFCustody form present and signe d?U lN):
Samples stored and/or shipped cool? (Y/N):
Preservative present in sarnple containers? (Y/N):
Are defensibili$ parErmeters acceptable? (Y/N):
-4'aA)v
Comments:
Holding Time
Were samples extracted within acceptable holding times? (Y/N)
Were samples analyzed within acceptable holding times? (Y/N)
Are holding time parameters acceptable? (Y/N), P
Comments:
Page 1 12t15t97
Equipment and Trip Blank Analyses
Appropriate number of equipment blanks submitted? MN):
Appropriate number of trip blanks submitted? (Y/N):
Are results above method detection limits? (Y/N):
lf yes, provide concentrations detected and concentrations of those compounds in
sample data if present:
Are results above method detection limits? (Y/N): ,4(A-
lf yes, provide concentrations detected and concentrations of those compounds in
sample data if present:
Surrogate Recoveries
Are recoveries within acceptable percent recovery control limits? (t?N) ,.1(.A
lf no, listresultsoutsideof limits. r-tU-t J oo , -alfl(sS-r\ = '<t'?, OO4t'O, fr-tor
4--t .J\'t/6 %
t/t:tw7 *#
Matrix Spike and Spike Duplicate Recoveries
Are recoveries within acceptable percent recovery control limits? (Y/N)
lf no, list results outside of limits.
h,*1 ={t/o,ee
Method Blanks
Are duplicate RPDs within acceptable limits? (Y/N)
lf no, list results outside of limits:
Page 2 12t15/97
Laboratory Duplicates
Are RPDs for laboratory duplicates within acceptable ranges? (Y/N):/,1^
lf no, list results outside of ranges.
Field Duplicates
Calculate and list RPDs for field duplicates. ;J , ; &-a-t*-t t A.,A
Do the RPDs appear appropriate?
OA/QC Discussion
Page 3 12t15/97
ofuft^* :
ra-J
4-
Ao*q58€
J*-ftd €/''/'i't
o
t€l ?,
( sr *z) //!/ n
trF " /07
tt - ro ?
ClienUProject:
Work Order#:
Date Sampled:
Sample lD #:
Formula:
Analyte:
cis. 1, 2- Dicholoroethe
trans- 1,24ich o I o roetl
Tricholorethene
Tetrachloroethene
Laundry Supply Go./Salt Lake City, UT
7585
5/1 5/98
MW-z Mw-4
RPD= (SR-DS Ry((SR+ DSR)/2)*1 00
SR
340
15
290
81 000
DSR
390
10
290
79000
RPD
13.70
40.00..
0.00
2.54
d : [vorkorders\7S8Shaecs 1 598