DSHW-2010-036886 - 0901a068801bdbf7

DEPARTMENT OF THE ARMY
us ARMY CHEMICAL MATERIALS AGENCY
TOOELE CHEMICAL AGENT DISPOSAL FACILITY
11620 STARK ROAD
STOCKTON, UTAH 84071
REPLY TO
ATTENTION OF: JUL 1 4 2010
RECEIVED
JUL 1 li 2010
DEPARTMENTOF ENVIRONMENTAL QUALITY
Tooele Chemical Agent Disposal Facility PM0520-10
SUBJECT: Transmittal of the Relative Accuracy Test Audit Report (RATA) for the Metal Parts
Fumace (MPF) Continuous Emissions Monitoring System (CEMS), EPA ID: UT 5210090002
Mr. Scott Anderson, Director
Utah Department of Environmental Quality
Division of Solid and Hazardous Waste
P.O Box 144880
195 North 1950 West
Salt Lake City, Utah 84114-4880
Dear Mr. Anderson:
uir3Cil OOOOOO
HAND DELIVERED
JUL 1 ^ 2010
UTAH DIVISION OF
SOLID & HAZARDOUS WASTE
Please find enclosed one copy of the RATA report for the MPF CEMS annual certification.
These tests were conducted at the TOCDF facility May 14 - May 21, 2010. The results
demonstrate that these CEMS performed to the established specifications.
If you have any questions regarding this issue, please contact Ms. Sheila R. Vance at (435)
833-7577 or Mr. Trace Salmon at [phone].
Sincerely,
Elizabetn A. Lowes
EG&G Defense Materials, Inc.
•CERTIFICATION STATEMENT
Thaddeus A. Qfyba, Jr.
TOCDF Site Project Manager
•CERTIFICATION STATEMENT
Enclosure
* I CERTIFY' UNDER PENALTY OF LAW THAT THIS DOCUMENT AND ALL ATTACHMENTS WERE PREPARED UNDER MY DIRECTION OR SUPERVISION IN
ACCORDANCE WITH A SYSTEM DESIGNED TO ASSURE THAT QUALIFIED PERSONNEL PROPERLY GATHER AND EVALUATE THE INFORMATION SUBMITTED.
BASED ON MY INQUIRY OF THE PERSON OR PERSONS WHO MANAGE THE SYSTEM, OR THOSE PERSONS DIRECTLY RESPONSIBLE FOR GATHERING THE
INFORMATION, THE INFORMATION SUBMITTED IS, TO THE BEST OF MY KNOWLEDGE AND BELIEF, TRUE. ACCURATE AND COMPLETE. 1 AM AWARE THAT
THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF FINE AND IMPRISONMENT FOR KNOWING
VIOLATIONS.
SCANNABLE
MATERIALS
associated with
this document have
been sent to be
processed
TOOELE CHEMICAL AGENT DISPOSAL FACILITY
(TOCDF)
Performance Specification Test (PST) Results
for the
MPF CO and O2CEMS
EG&G Defense Materials, INC.
July 2010
HAND DELIVERED
JUL 1 4 2010
UTAH DIVISION OF
SOLID & HAZARDOUS WASTE
DEPARTMENT OF THE ARMY
us ARMY CHEMICAL MATERIALS AGENCY
TOOELE CHEMICAL AGENT DISPOSAL FACILITY
11620 STARK ROAD
STOCKTON, UTAH 84071
REPLY TO
ATTENTJON OF JUL 1 4 2010
RECEIVED
JUL 1 k 2010
DEPARTMENT OF ENVIRONMENTAL QUALITY
Tooele Chemical Agent Disposal Facility PM0520-10
SUBJECT Transmittal of the Relative Accuracy Test Audit Report (RATA) for the Metal Parts
Furnace (MPF) Continuous Emissions Monitoring System (CEMS), EPA ID UT 5210090002
Mr Scott Anderson, Director
Utah Department of Environmental Quality
Division of Solid and Hazardous Waste
P O Box 144880
195 North 1950 West
Salt Lake City, Utah 84114-4880
Dear Mr Anderson
HAND DELIVERED
JUL 1 ^ 2010
UTAH DIVISION OF
SOLID & HAZARDOUS WASTE
Please find enclosed one copy of the RATA report for the MPF CEMS annual certification
These tests were conducted at the TOCDF facility May 14 - May 21, 2010 The results
demonstrate that these CEMS performed to the established specifications
If you have any questions regarding this issue, please contact Ms Sheila R Vance at (435)
833-7577 or Mr Trace Salmon at [phone]
Sincerely,
ElizabetnA Lowes
EG«&G Defense Materials, Inc
•CERTIFICATION STATEMENT
Thaddeus A ^yoa, Jr
TOCDF Site Project Manager
•CERTIFICATION STATEMENT
Enclosure
I CERTIFY UNDER PENALTY OF LAW THAT THIS DOCUMENT AND ALL ATTACHMENTS WERE PREPARED UNDER MY DIRECTION OR SUPERVISION IN
ACCORDANCE WITH A SYSTEM DESIGNED TO ASSURE THAT QUALIFIED PERSONNEL PROPERLY GATHER AND EVALUATE THE INFORMATION SUBMITTED
BASED ON MY INQUIRY OF THE PERSON OR PERSONS WHO MANAGE THE SYSTEM OR THOSE PERSONS DIRECTLY RESPONSIBLE FOR GATHERING THE
INFORMATION THE INFORMATION SUBMITTED IS TO THE BEST OF MY KNOWLEDGE AND BELIEF TRUE ACCURATE AND COMPLETE I AM AWARE THAT
THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION INCLUDING THE POSSIBILITY OF FINE AND IMPRISONMENT FOR KNOWING
VIOLATIONS
HAND DELIVERED
Performance Specification Test Resuits ^ ^ ^^^^
for the MPF CEMS UTAH DIVISION OF
SOLID & HAZARDOUS WASTE
Tooeie Cliemicai Agent Disposal Facility ^010,03f=>^^
Stoclcton, Utah
Prepared for
EG&G Defense Materials Inc
11600 Stark Road
Stockton, UT 84071
Prepared by
URS Corporation
9400 Amberglen Blvd
P O Box 201088
Austin, Texas 78720-1088
July 2010
Table of Contents
Page
10 Introduction 1-1
2 0 Summary of Results 2-1
21 Calibration Dnft 2-2
2 2 Absolute Calibration Audit 2-5
2 3 Response Time 2-6
2 4 Relative Accuracy 2-7
3 0 Quality Assurance 3-1
APPENDIX A - Calibration Dnft Data Sheets
APPENDIX B - Absolute Calibration Audit and Response Time Data Sheets
APPENDIX C - Relative Accuracy Spreadsheet and Reference Method Data
APPENDIX D - Reference Method Calibration Results
APPENDIX E - MPF CEMS Relative Accuracy Data
APPENDIX F - MPF RATA Fuel Flow Data
APPENDIX G - TOCDF EPA Protocol 1 Gas Certifications
APPENDIX H - Reference Method EPA Protocol 1 Gas Certifications
APPENDIX I - Reference Method CEMs Interference Test
2010 MPF CEMS PST 11 TOCDF 40942240 06
List of Tables
Page
1-1 General Facility and Testing Information 1-2
1-2 CEMS Identification 1-2
2-1 Annual PST Requirements and Acceptance Cntena 2-1
2-2 14-Arr-384/API-164 CO CEMS Calibration Dnft Test Results 2-3
2-3 14-AIT-082/65855 O2 CEMS Calibration Dnft Test Results 2-4
2-4 Absolute Calibration Audit Gas Concentrations 2-5
2-5 Absolute Calibration Audit Test Results 2-5
2-6 Response Time Test Results 2-6
2-7 MPF RM Sampling Location Stratification Check Results 2-10
2-8 14-AIT-384/API-164 CO CEMS Relative Accuracy Test Results 2-10
2-9 14-AIT-082/65855 O2 CEMS Relative Accuracy Test Results 2-11
2010 MPF CEMS PST ill TOCDF 40942240 06
1.0 Introduction
The Tooele Chemical Agent Disposal Facility (TOCDF) operates the Metal Parts Fumace
(MPF) location, which is equipped with redundant carbon monoxide (CO) and oxygen (O2)
continuous emissions monitonng systems (CEMS) In accordance with the Resource
Conservation and Recovery Act (RCRA) permit and the Utah Air Regulation R307-170 under
which the TOCDF facility operates, each MPF CEMS must undergo annual Performance
Specification Testing (PST) This report presents the PST results for the MPF CO and O2
CEMS The general information regarding the testing at this facility is summarized m Table 1-1
The PST acceptance cntena are shown in Table 2-1
The PST of the MPF CO and O2 CEMS was completed in May of 2010 The CEMS
were audited according to the procedures detailed in 40 CFR 60, Appendix B, Performance
Specification 4B, "Specifications and Test Procedures for Carbon Monoxide and Oxygen
Continuous Monitoring Systems in Stationary Sources" (PS 4B), 40 CFR 266, Appendix DC,
Section 2, "Performance Specifications for Continuous Emission Monitoring Systems" 40 CFR
63 Subpart EEE, "National Emission Standards for Hazardous Air Pollutants from Hazardous
Waste Combustors" and EG&G QA/QC document EG 037, "Continuous Emission Monitoring
System Certification Test Protocol " The CEMS met all the PST cntena outlined in the above-
cited references Section 2 presents a detailed summary of these test results Supporting
documentation is located in the appendices
The analyzer identification numbers and serial numbers for the monitors are presented
below in Table 1-2 The CO analyzers are Teledyne Advanced Pollution Instmmentation (API)
Model 300 EM gas correlation CO analyzers The CO analyzers are designed using a single
sample cell equipped with an individual detector system for each of two measurement ranges (0-
200 ppmv and 0-5,000 ppmv) Except for the relative accuracy testing, each range of each CO
analyzer was treated as a separate monitor for the purposes of this testing The O2 analyzers are
Servomex PM 1158 analyzers The data for the CEMS is recorded by the TOCDF Process Data
Acquisition and Recording System (PDARS) Data pnntouts from these monitors documenting
the CEMS performance are presented in Appendix E of this report
2010 MPF CEMS PST 1-1 TOCDF 40942240 06
Table 1-1 Tooele Chemical Agent Disposal Facility
MPF CEMS Performance Specification Testing
General Facility and Testing Information
Facility Name Tooele Chemical Agent Disposal Facility
Contact Person Karl Scott
Telephone Number 435-833-7861
Facility Address EG&G Defense Materials, Inc
11600 Stark Road
Stockton, UT 84071
Facibty Manager Gary McCloskey
Types of Process Sampled MPF Exhaust Gas
Person Responsible for Conducdng Test Michael Fuchs
Telephone Number 512-454^797
Company Name URS Corporadon
Address 9400 Amberglen Boulevard
Ausnn, Texas 78729
Person(s) Conducting Tests Adam Blank
Crawford D Cumn
Test Methods Performed EPA Method 3A and EPA Method 10 Test Methods Performed
CEMS Cahbranon Dnft (performed by EG&G)
Test Methods Performed
CEMS Absolute Calibration Audit
(performed by EG&G)
Test Methods Performed
CEMS Response Time (performed by EG&G)
Date(s) of Testmg May 14 through May 21, 2010
Table 1-2 Tooele Chemical Agent Disposal Facility
MPF CEMS Performance Specification Testing
CEMS Identification
Location Analyzer Type CEMS Range Analyzer
Identiflcation No Serial No
MPF Carbon Monoxide 0-200 ppmv Span 14-AIT-384 API-164 MPF Carbon Monoxide 0-5,000 ppmv Span 14-Arr-384 API-164
MPF Oxygen 0-25% Span 14-AIT-082 65855
2010 MPF CEMS PST 1-2 TOCDF 40942240 06
2.0 Summary of Results
Detailed PST results are presented in this section Section 2 1 provides a summary of the
calibration drift (CD) tests A summary of the absolute calibration audit (ACA) tests are
presented in Section 2 2 Results from the response time (RT) tests are provided in Section 2 3,
and Section 2 4 details the results from the relative accuracy (RA) tests
The ACA, RT, and RA testing is required to occur during the seven-day CD testing
period All test results were within the acceptance cntena as stated m 40 CFR 60, Appendix B,
Performance Specification 4B, "Specifications and Test Procedures for Carbon Monoxide and
Oxygen Continuous Monitoring Systems in Stationary Sources," and EG&G QA/QC document
EG 037, "Continuous Emission Monitoring System Certification Test Protocol" These cntena
are shown below m Table 2-1
Table 2-1 Tooele Chemical Agent Disposal Facility
MPF CEMS Performance Specification Testmg
Annual PST Requirements and Acceptance Criteria
CO Monitors O2 Monitors
Parameters Low Range
(0-200 ppmv)
High Range
(0-5,000 ppmv) Range (0-25%)
Calibration Drift
(7 out of 7 days)
< 3% full scale
(6 ppmv)
< 3% full scale
(150 ppmv) <0 5%
Absolute
Calibration Audit
< 5% full scale
(10 ppmv)
< 5% full scale
(250 ppmv) <0 5%
Response Time < 2 minutes < 2 minutes < 2 minutes
Relative Accuracy
(RA)
The greater of 10% of the Reference
Method (RM) or 5 ppmv CO corrected to
7%02
1 0% O2
2010 MPF CEMS PST 2-1 TOCDF 40942240 06
2 1 Calibration Drift
Tables 2-2 and 2-3 present the results of the CD tests performed by EG&G personnel
from May 14 through May 21, 2010 No analyzer adjustments were made between 24-hour
calibration readings The calibration dnft values are reported m these tables as both the absolute
values and the relative percentages of span of the mean differences between the CEMS response
and the reference gas value All tests produced acceptable results Copies of all CEMS daily
calibration responses are presented in Appendix A
2010 MPF CEMS PST 2-2 TOCDF 40942240 06
Table 2-2 Tooele Chemical Agent Disposal Facility
MPF CEMS Performance Specification Testing
14-AIT-384/API-164 CO CEMS
Calibration Dnft Test Results
14-AIT-384/API-164
Date Cal Gas
(ppmv)
CEMS
Response
(ppmv)
Dnft
(ppmv)
Dnft
(%
Span)
Zero
5/14/2010 0 00 0 0 00
5/15/2010 0 00 0 0 00
5/16/2010 0 00 0 0 00
5/17/2010 0 00 0 0 00
5/18/2010 0 00 0 0 00
5/19/2010 0 00 0 0 00
5/20/2010 0 00 0 0 00
5/21/2010 0 00 0 0 00
Span Low Range (0-200 ppmv)
5/14/2010 155 155 0 0 00
5/15/2010 155 154 1 0 50
5/16/2010 155 155 0 0 00
5/17/2010 155 155 0 0 00
5/18/2010 155 155 0 0 00
5/19/2010 153 153 0 0 00
5/20/2010 153 151 2 1 00
5/21/2010 153 152 1 0 50
Span Hig h Range (0-5000 ppmv)
5/14/2010 3760 3760 0 0 00
5/15/2010 3760 3762 2 0 04
5/16/2010 3760 3743 17 0 34
5/17/2010 3760 3760 0 0 00
5/18/2010 3760 3762 2 0 04
5/19/2010 3780 3772 8 0 16
5/20/2010 3780 3774 6 0 12
5/21/2010 3780 3774 6 0 12
2010 MPF CEMS PST 2-3 TOCDF 40942240 06
Table 2-3 Tooele Chemical Agent Disposal Facility
MPF CEMS Performance Specification Testing
14-AIT-082/65855 O2 CEMS
Calibration Drift Test Results
14-AIT-082/65855
Date
Oxygen
Range 0-25%
Date Cal Gas
(%)
CEMS
Response
(%)
Dnft
(%)
Zero
5/14/2010 0 00 0 00
5/15/2010 0 00 0 00
5/16/2010 0 00 0 00
5/17/2010 0 00 0 00
5/18/2010 0 00 0 00
5/19/2010 0 00 0 00
5/20/2010 0 00 0 00
5/21/2010 0 00 0 00
Span
5/14/2010 20 9 20 9 0
5/15/2010 20 9 20 9 0
5/16/2010 20 9 20 9 0
5/17/2010 20 9 20 9 0
5/18/2010 20 9 20 9 0
5/19/2010 20 9 20 9 0
5/20/2010 20 9 20 9 0
5/21/2010 20 9 20 9 0
2010 MPF CEMS PST 2-4 TOCDF 40942240 06
2 2 Absolute Calibration Audit
Absolute calibration audit (ACA) tests for the MPF CEMS were performed by EG&G
personnel on May 18, 2010 The ACA tests were performed by challenging the CEMS with
three concentrations of EPA Protocol 1 audit gases Table 2-4 presents the specified ranges for
each of the audit gases Table 2-5 presents the results from the ACA testing The values
reported m this table are the average absolute values of the mean differences between the CEMS
response and the reference gas value ACA data sheets and audit gas Protocol 1 certification
sheets are presented m Appendix B and Appendix G, respectively
Table 2-4 Tooele Chemical Agent Disposal Facility
MPF CEMS Performance Specification Testing
Absolute Calibration Audit Gas Concentrations
Monitors CO Low CO High O2
Audit Gas Range One 0-40 ppmv 0-600 ppmv 0-2%
Audit Gas Range Two 60-80 ppmv 1,500-2,000 ppmv 8-10%
Audit Gas Range Three 140-160 ppmv 3,500-4,000 ppmv 14-16%
Table 2-5 Tooele Chemical Agent Disposal Facility
MPF CEMS Performance Specification Testing
Absolute Calibration Audit Test Results
Absolute Calibration Audit Test" Acceptance
Criterion'' MPF CEMS Serial No Date Time Zero Audit
Gas
Mid Audit
Gas
High Audit
Gas
Acceptance
Criterion''
Carbon Monoxide Analyzer
Low range 14-AIT-384 API-164 5/18/2010 14 09 0 00 1 97 0 83 < 10 ppmv
High range 14-AIT-384 API-164 5/18/2010 14 30 0 87 12 53 14 30 < 250 ppmv
Oxygen Analyzer
14-AIT-082 65855 5/18/2010 13 51 0 00 0 05 0 05 <0 5%
"The absolute calibration audit test values are reported as the average absolute mean difference between the CEMS response and
the reference gas value
"Tlie acceptance cntena for carbon monoxide analyzers is less than or equal to 5% of span The span of the analyzers low range
IS 200 ppmv and the span of their high range is 5 000 ppmv
2010 MPF CEMS PST 2-5 TOCDF 40942240 06
2 3 Response Time
The response times (RT) for the MPF CO and O2 CEMS were determined by EG&G
personnel on May 19, 2010 RT test results are presented in Table 2-6 All measured response
times for the MPF CO and O2 CEMS were below the 2-nunute acceptance cnterion Response
time data sheets and hardcopies of the CEMS responses can be found in Appendix B
Table 2-6 Tooele Chemical Agent Disposal Facility
MPF CEMS Performance Specification Testing
Response Time Test Results
MPF CEMS Serial No Date Start/Stop
Mean Response Times
System
Response
Time"
(min sec)
MPF CEMS Serial No Date Start/Stop Upscale Zero
to Duct
(mm sec)
Downscale
High to
Duct
(mm sec)
System
Response
Time"
(min sec)
Carbon Monoxide Analyzers
Low range 14-AIT-384 API-164 5/19/2010 15 11-1518 1 07 1 09 1 09
High range 14-AIT-384 API-164 5/19/2010 15 21-15 30 1 24 1 25 1 25
Oxygen Analyzers
14-AIT-082 65855 5/19/2010 15 02-15 09 0 58 0 53 0 58
'The acceptance cntena for all analyzers is less than or equal to 2 minutes
2010 MPF CEMS PST 2-6 TOCDF 40942240 06
2 4 Relative Accuracy
Relative accuracy (RA) testing was performed by URS personnel on May 19, 2010 RA
testing compares the plant CEMS measurement of CO (corrected to 7% oxygen) and O2 to the
Reference Method (RM) measured using EPA Method 10 for CO and EPA Method 3A for O2
For each run, sample gas was collected over 21-imnute test penods Three traverse points across
the MPF duct were selected according to the procedure outlined in 40 CFR 60, Appendix B,
Performance Specification 2, Section 8 13 2, and sample gas was extracted at each point for
seven minutes dunng the test period A data sheet showing the sample points is included in
Appendix C In addition, a stratification check was conducted at these sample points in
accordance with EPA Method 7E Data from the stratification check are presented in Table 2-7
Oxygen was used as the flue gas constituent for the determination of stratification due to its
presence m the duct at a consistendy detectable level The flue gas at the MPF sampling location
was demonstrated to be unstratified/mimmally stratified Data documenting the stratification
check are included m Appendix C
URS Corporation used a TECO Model 48C CO analyzer to measure the CO
concentration according to EPA Method 10 This analyzer is a gas filter correlation (GFC)
analyzer The analyzer measures CO by comparing infrared absorption of a reference
concentration to the absorption of the sample The TECO Model 48C CO measurements are not
affected by carbon dioxide For this reason, the CO2 interference trap was not incorporated into
the extraction system The exclusion of the CO2 interference trap eliminates the need to conect
sample concentration, improving the accuracy of the analyses Oxygen was measured using a
Servomex Senes 1400 O2 analyzer This analyzer measures O2 on the basis of its paramagnetic
properties These analyzers have been interference tested in accordance with the procedures of
EPA Method 7E The interference response data is presented in Appendix I
The analyzer's electronic output signals were converted to a digital format and stored by
URS Corporation's computenzed data acquisition system The system translated this digital
signal into the proper units of measurement (ppmv CO, % O2) and stored them on a hard disk
The system stored the data as ten-second averages
The analyzers were calibrated prior to initiating testing using appropriately certified
standards as specified by EPA Methods 10 and 3A A system response time test was performed
and documented The total system, which included the probe, sample line, sample pump, and
condenser, was incorporated into the system response Copies of the system response time data
2010 MPF CEMS PST 2^7 TOCDF 40942240 06
are included in Appendix D In addition, system audit tests, as defined in EG&G QA/QC
document EG 033, "CEMS Certification Quality Assurance Program," were performed
throughout the RATA These vanous checks ensured that the system remained withm the
tolerance level defined by the above EPA methods Documentation of the system audits are
included in Appendix C A sampling system calibration bias correction was apphed to all RM
O2 and CO data measured during each test run by using equation EPA Method 7E-5
C =(C -C )x
gas ^ avg ^o'
Where
Cgas = effluent gas concentration, dry basis, ppmv
Cavg = average gas concentration indicated by analyzer, dry basis, ppmv
Cm = average of initial and final system calibration bias check responses for the
upscale calibration gas, ppmv
Cma = actual concentration of the upscale calibration gas, ppmv
Co = average of initial and final system calibration bias check responses for the
zero calibration gas, ppmv
The arithmetic differences between the URS reference method (RM) results for the
analyte gas concentrations and the plant CEMS results for the analyte gas concentrations are
presented in Tables 2-8 and 2-9 Carbon monoxide results for both the RM and the MPF CEMS
were conected to 7% oxygen before calculating anthmetic differences The absolute average
difference, standard deviation (Sd) and confidence coefficient (CC) of the arithmetic differences
were calculated using the equations described in 40 CFR 60, Appendix B, Performance
Specification 2, Section 12 At least nine runs must be used to deternune average difference and
standard deviation Ten runs were performed dunng the May 19, 2010 RA testing
2010 MPF CEMS PST 2-8 TOCDF 40942240 06
The confidence coefficient (CC) was calculated according to the following equation
cc=to 975^-7^
Vn
Where
to 975 = 97 5% Student-1 vanable (2 306 for mne runs), and
n = number of tests used (must be > 9)
Relative accuracy for the MPF CO CEMS was calculated in ppmv CO according to 40
CFR 60, Appendix B, Performance Specification 4A, Section 13 2, by adding together the
absolute value of the average difference between the RM and MPF CEMS and the confidence
coefficient applicable to nine test runs The results for the absolute average difference, standard
deviation, and the confidence coefficient were not rounded before the calculation of relative
accuracy Relative accuracy for the MPF O2 CEMS was calculated in % O2 according to 40 CFR
60, Appendix B, Performance Specification 3, Section 12 0, and was equivalent to the absolute
average difference between the RM and MPF CEMS for ten test runs Hardcopies from the RM
data acquisition system along with hardcopies of the relative accuracy calculation spreadsheet
can be found in Appendix C Hardcopies of the TOCDF CEMS data are presented m Appendix
E
2010 MPF CEMS PST 2-9 TOCDF 40942240 06
Table 2-7 Tooele Chemical Agent Disposal Facility
MPF RM Sampling Location
Stratification Check Results
Traverse Points
Markmg
Location
(inches from wall)
Samphng
Duration
(mmutes)
O2 Concentration
(%)
% DifTerence
from Mean
1 4 45 7 11 85 0 73
2 13 38 7 11 75 0 15
3 22 30 7 11 69 058
Mean Concentration of All Traverse Points 11 76 -- 1
Table 2-8 Tooele Chemical Agent Disposal Facility
MPF CEMS Performance Specification Testing
14-AIT-384/API-164 CO CEMS
Relative Accuracy Test Results
Run Number Date Run Time
Reference
Method (RM)
CEMS
(ppmv CO,
corrected to
7% O2)
TOCDF CEMS
14.AIT-384/
API-164
(ppmv CO,
corrected to
7% O2)
Arithmetic
Difference
(ppmv CO)
1 5/19/2010 736-757 1 08 20 -0 92
2 5/19/2010 804-825 1 25 20 -0 75
3 5/19/2010 830-851 1 45 20 -0 55
4 5/19/2010 857-918 1 45 1 0 0 45
5 5/19/2010 924-945 1 22 00 1 22
6 5/19/2010 951-1012 1 24 00 1 24
7 5/19/2010 1019-1040 1 03 00 1 03
8 5/19/2010 1047-1108 1 26 1 0 0 26
9 5/19/2010 1140-1201 1 50 20 -0 50
10 5/19/2010 1208-1229 1 39 20 -0 61
Runs 1-10 Absolute Average Difference 0 09
Runs 1-10 Standard Deviation 0 86
Runs 1-10 Confidence Coefficient (CC) 0 61
Runs 1-10 Relative Accuracy (ppmv CO) 0 70
2010 MPF CEMS PST 2-10 TOCDF 40942240 06
Table 2-9 Tooele Chemical Agent Disposal Facility
MPF CEMS Performance Specification Testing
14-AIT-082/65855 O2CEMS
Relative Accuracy Test Results
Run Number
i
Date Run Time
Reference
Method (RM)
CEMS
(% O2)
TOCDF CEMS
14-AIT-082/
65855
(% O2)
Anthmetic
Difference
(% O2)
-0 50
Run Number
i 5/19/2010 736-757 11 50 12 0
Anthmetic
Difference
(% O2)
-0 50
2 5/19/2010 804-825 11 86 11 8 0 06
3 5/19/2010 830-851 12 02 11 9 0 12
4 5/19/2010 857-918 12 09 12 0 0 09
5 5/19/2010 924-945 12 23 12 2 0 03
6 5/19/2010 951-1012 12 24 12 2 0 04
7 5/19/2010 1019-1040 12 21 12 2 001
8 5/19/2010 1047-1108 12 20 12 1 0 10
9 5/19/2010 1140-1201 11 89 119 -0 01
10 5/19/2010 1208-1229 11 77 11 8 0 03
Runs 1-10 Absolute Average Dil^erence 001
Runs 1-10 Standard Deviation 0 18
Runs 1-10 Relative Accuracy (% O2) 001 1
2010 MPF CEMS PST 2-11 TOCDF 40942240 06
3 0 Quality Assurance
To ensure accurate and defensible results, stnct quality assurance and control measures
were followed All testing was performed following standard EPA protocol as outlined in 40
CFR, Part 60, Appendix A All PST testing was performed while the plant was operating under
normal conditions For the MPF testing, the incinerator must be operating at 50% full heat input
m btu/min, or 50% fuel flow in cfm of natural gas Acceptable levels of fuel flow were
maintained throughout the testing Hardcopies of incinerator fuel flow data are included m
Appendix F All test cntena were thoroughly documented and checked for completeness EPA
Protocol 1 gas certification documentation for cylinders used dunng the RA testing is included m
Appendix H
The CO and O2 monitors used by URS Corporation were operated and calibrated in
accordance with the EPA Methods 10 and 3A except that the CO2 interference trap was not used
The gas filter correlation monitor used for CO determination uses the charactenstic absorption of
infrared light by CO to measure its relative concentration This is a highly specific method for
determining CO and is virtually free of interference from compounds such as water or carbon
dioxide System bias checks were performed before and after each test mn to ensure that the
measuring systems remained withm their performance specifications All method performance
specifications were met Calibration results are documented m Appendix D
2010 MPF CEMS PST 3-1 TOCDF 40942240 06
APPENDIX A
Calibration Drift Data Sheets
CEMS CALIBRATION DRIFT TEST RECORD
Operator Signature ^. Pg_L
FM-PRPMO001 79 R3C0 THIS IS A RECORD
CEMS CALIBRATION DRIFT TEST RECORD
I Source MPF Date 5/14/10
Monitor CO Location North PAS House/ Rack 105
Serial Number API-164 Span 0 Zoo *-\
Day Date TEme Cylinder
Number
Calibration
Value
Monitor
Response Difference % of Span
0 JlH lo
• - #
O o
1 O 0 o
2 5 IV 10 o o O
2
i 3 o 6 A
ro
/
L
o
4 0 0 <)
u
0 V
N 5 5 l*t fo d « o O
6 5 Z-a 1* 0 0 o o
7 o 0
0 5MM Ic /^IT-0 o
1
—f—'
1 5
2 J5S"
>
IB 3 5 0 Id iss-
•o
S 4 c) O
5 5-/^ to
6 ;sr/ Z
7 to Cjt 14741 I
0 I'^ii^'. 0 O
1 770V .04
2 072! i743 n .34
Le
v
e
l
3 0 0 £
X 4 $700 z oH
5 5*H-|o .10
6 6^-20 lo .a
7 ?77*/ (/ ...
Operator Signature, Pg_L
FM-PRPMO001-79 R3C0 THIS IS A RECORD
GEMS CALIBRATIO
14-MA'
MARY REPORT
OXYGEN
14-AIT-082
MPF AFTERBLOWER
Rack 105
This report or the data herein MUST be screened by the Monitoring Branch before being released from TOCDF control
65855
Time Settlne ReJDonse Tareet DIff
13-0211 Zero Dnft 0 0 0
13-0243 Zero Dnft 0 0 0
13-0313 Zero Set 0 0 0
1305 43 SoanDnft 202 209 -7
CARBON MONOXIDE
14-A1T-384 API-164
Time Settine Response Tareet m
13.-0601 Zero Drift 0 0 0
13-07.27 ZeroDiiR 0 0 0
130747 Zero Dnft 0 0 0
1307 55 Zero Dnft 0 0 0
130819 Zero Set 0 0 0
131325 SoiuiRlDnft 140 155 15
131349 SoanRfSet 155 155 0
131949 SDaiiR2 Drift 3750 3760 10
132011 SoanmSet 3775 3760 15
Comment
£>x. "viAt O eA<-T><UPT
Purpose View CEMS dally calibration drift data by rack number - 02 Is bi 96 and CO and NOx Is in PPM
Difference (Diff) Is the Response minus the Target
MPF Fuel Flow
Cal Dnfl Day 0
Minimum Req'd 84483scfm
14-May-1013 01 00 137 143204
14-May-10 13 0130 138 143934
14-May-10 13 02 00 140 146124
14-May-10 13 02 30 137 143100
14-May-10 13 03 00 138 143621
14-May-101303 30 138 143830
14-May-10 13 04 00 139 144560
14-May-10 13 04 30 138 143413
14-May-10 13 0500 138 143934
14-May-1013 05 30 138 143934
14-May-10 13 06 00 137 143308
14-May-1013 06 30 137 143100
14-May-10 13 07 00 137 142891
14-May-1013 07 30 137 143204
14-May-10 13 08 00 138 143934
14-May-10 13 08 30 139 144664
14-May-1013 09 00 138 144038
14-May 1013 09 30 137 142891
14-May-10 13 10 00 138 143413
14 May-10 13 10 30 138 144038
14-May-101311 00 138 143934
14-May-1013ll 30 139 145290
14-May-10 13 12 00 137 142682
14-May-10 13 12 30 136 141639
14-May-10 13 13 00 137 142995
14-May-1013 13 30 137 142891
14-May-10 13 14 00 136 142057
14-May-101314 30 137 142370
14-May-101316 00 137 142995
14-May-10 13 15 30 142 148419
14 May-10 13 16 00 149 155511
14-May-101316 30 175 182212
14-May-101317 00 192 200047
14-May-10 13 17 30 181 188366
14-May-101318 00 136 141848
14-May-101318 30 111 115356
14-May-101319 00 106 110037
14-May-101319 30 104 108263
14-May-1013 20 00 100 104404
14 May-10 13 20 30 98 101693
14-May-1013 21 00 97 100962
14-May-10 13 21 30 98 102631
C bs/h i
L ^« it
^^^^^^
0 143204
0 143934
0 146124
0 143100
0 143621
0 143830
0 144560
0 143413
0 143934
0 143934
0 143308
0 143100
0 142891
0 143204
0 143934
0 144664
0 144038
0 142891
0 143413
0 144038
0 143934
0 145290
0 142682
0 141639
0 142995
0 142891
0 142057
0 142370
0 142995
0 148419
0 155511
0 182212
0 200047
0 188366
0 141848
0 115356
0 110037
0 108263
0 104404
0 101693
0 100962
0 102631
TOCDF PDARS Data
5/14/2010
OEMS CALIBRATIO
15-MA
N^l MMARY REPORT
0
OXYGEN
14-AlT 082
MPF AFTERBLOWER
Rack 105
This report or the data herein MUST be screened by the Monitonng Branch before being released from TOCDF control
6S855
Time Settine ResDonse Tareet Diff
0729-.02 Zero Drift 1 0 1
073026 Soan Drift 21 2a9 1
CARBON MONOXIDE
14 AIT 384 API-164
Time SetUne Ressonse Tareet DiQ
0731:08 Zero Drift 0 0 0
073414 SnanRl Drift 155 155 0
073612 Soan R2 Dnft 3775 3760 15
Comment
Purpose View CEMS daily calibration drift data by rack number - 02 is in % and CO and NOx is in PPM
Difference (Diff) Is the Response minus the Target
MPF Fuel Flow
Cal Dr/ft Day 1
Minimum Req'd 84483scfm
15-May-10 07 28 00 157 163334
15-May-10 07 28 30 157 163230
15-May-10 0729 00 157 163230
15-May>10 07 29 30 157 163230
15 May-10 07 30 00 157 164168
15-May-10 07 30 30 158 164585
15-May-10 07 31 00 158 164481
15-May-10 07 31 30 157 163230
15-May-10 07 32 00 167 163855
15-May-10 07 32 30 157 163855
15-May 10 07 33 00 157 163855
15-May-1007 33 30 155 161769
15-May-10 07 34 00 157 163647
15-May-10 07 34 30 157 163542
15-May-10 07 35 00 157 163751
15-May-10 07 35 30 156 163125
15-May-10 07 36 00 155 161978
15-May 10 07 36 30 157 163647
15-May-10 07 37 00 156 163125
15-May-10 07 37 30 157 163847
Agen Fvii Agent Qeecl
@tn/tnn
lb.* ^
. BTJ /ai i:
^85Q0m£i))S
Total BTu
Va^e*
0 163334
0 163230
0 163230
0 163230
0 164168
0 164585
0 164481
0 163230
0 163855
0 163855
0 163855
0 161769
0 163647
0 163542
0 163751
0 163125
0 161978
0 163647
0 163125
0 163647
TOCDF PDARS Data
5/15/2010
CEMS CALIBRATIO
16-MA^
M MARY REPORT
TGDDF MPF AFTERBLOWER
Rack 105
OXYGEN
"This report or the data herein MUST be screened by the Monitoring Branch before being released from TOCDF control"
14-AIT 082 65855
Time Settlns ResDonse Tareet Diff
0714 42 Zero Dnft 0 0 0
071610 Soan Drift 209 209 0
CARBON MONOXIDE
14-AIT-384 API-164
Time Settine ResDonse Tareet Ditr
07 16 02 Zero Dnft 0 0 0
0718.02 Soan RI Drift 155 155 0
0719-42 Soan R2 Drift 3750 3760 10
Comment
CO
Purpose View CEMS daily calibration drift data by rack number - 02 is in % and CO and NOx is m PPM
Difference (Diff) is the Response minus the Target
MPF Fuel Flow
Cal Dnft Day 2
Minimum Req'd 84463scfm
fSTowinsucnaGoS
q(Sluu=ilQH(Awu(;la ^^^^^
16-May-10 0713 00 152 158953
16-May-100713 30 150 156554
16-May-100714 00 152 158536
16-May-10 07 14 30 152 158640
16-May-10 07 15 00 152 158327
16-May-10 071S30 152 158536
16-May-10 0716 00 150 156346
16-May-10 0716 30 151 157076
16-May-10 0717 00 150 156867
16-May-10 0717 30 152 158536
16-May-10 0718 00 150 155929
16-May-10 07 18 30 151 157076
164Xay-10 071900 150 156763
16-May-10071930 150 156450
16-May-10 07 2000 151 157180
16-May-10 07 20 30 152 158849
Agen FeecT
^ bs^ir*
t
A^bnuFped Fe«d V
j& l&s/^n igssoOBT-uflb ^^^^
0 158953
0 156554
0 158536
0 158640
0 158327
0 158536
0 156346
0 157076
0 156867
0 158536
0 155929
0 157076
0 156763
0 156450
0 157180
0 158849
TOCDF PDARS Data
5/16/2010
CEMS CALIBRATION,
17-MA^
N^yvi MARY REPORT
TGDDF
OXYGEN
14-AIT 082
MPF AFTERBLOWER
Rack 105
This report or the data herein MUST be screened by the Monitoring Branch before being released from TOCDF control"
65855
Time Settine ResDonse Tareet Diff
07 5144 Zero Dnft 0 0 0
075338 SoanDnft 209 209 0
CARBON MONOXIDE
14-AIT-384 APM64
Time Settine Resoonse Tareet Difl
075412 Zero Drift 0 0 0
07S6J6 SnanRl Drift 156 155 1
07 5932 Soan R2 Drift 3775 3760 15
Comment
Purpose View CEMS daily calibration drift data by rack number 02 is in % and CO and NOx is in PPM
Difference (Diff) is the Response minus the Target
11
MPF Fuel Row
Cal Dnft Day 3
Minimum Req'd 84483scfm
17-May-10 0750 00 151 157180
17-May-100760 30 150 156137
17-May-10 07 51 00 152 158015
17-*lay-10 075130 149 155616
17-May-10 07 52 00 152 158640
17-May-10 07 52 30 150 156867
17-Alay-IO 07 53 00 151 157284
17 May-10 07 53 30 151 157806
17 May-10 07 54 00 151 157284
17-May-10 07 54 30 150 156346
17-May 1007 55 00 152 158327
17-May-1007 55 30 151 157702
17-May-100756 00 151 157180
17-May-10 07S6 30 149 155303
17-May-10 07 57 00 150 156137
17-May-10 07 57 30 150 156137
17-May-10 07 58 00 149 155824
17 May-10 07 58 30 150 155929
17-May-1O07 59 D0 151 156972
17-May 10 07 59 30 152 158119
17-May-10 08 00 00 153 159058
17-May-10 08 00 30 153 159683
0 157180
0 156137
0 156015
0 155616
0 158640
0 156867
0 157284
0 157806
0 157284
0 156346
0 158327
0 157702
0 167180
0 155303
0 156137
0 156137
0 155824
0 155929
0 166972
0 158119
0 159058
0 159683
TOCDF PDARS Data
5/17/2010
HiS8B
CEMS CALIBRATIO
18-MA^
N^|M MARY REPORT
MPF AFTERBLOWER
Rack 105
OXYGEN
14-Arr-082
This report or the data herein, MUST be screened by the Momtoring Branch before bebig released from TOCDF control
6S8SS
Time Setline ResDoose Tareet Difl
0703.32 Zero Dnft 0 0 0
07-04.46 SoanDnft 209 209 0
1342.16 Zero Drift 0 0 0'
1344.30 Zero Dnft 89 0 89
134544 Zero Dnft 15 0 15
134700 Zero Drift 9 0 9
134S06 Zero Drift 1 0 1
1349-12 Zero Drift IS 0 15
13J0-26 Zero Dnft 1 0 1
13 5146 Zero Dnft 9 0 9
135300 Zero Drift 15 0 15 J
14 38 54 Zero Drift 208 0 208
14 39 18 Zero Drift 209 0 209
144048 Zero Drift 2 0 2
CARBON MONOXIDE
14-A1T-384 API-164
Time Settine Resoonse Tareet Difl
070412 Zero Dnft 0 0 0
07 09 DO SnanRl Dnft 157 155 2
071112 Soan RZ Drift 3775 3760 15
13 57 26 Zero Dnft 0 0 0
13 58J0 Zero Dnft 68 0 68
14 0032 Zero Dnft 154 0 154
140154 Zero Drift 69 0 69
14 03 30 Zero Dnft 0 0 0
14.0518 Zero Dnft 154 0 154
14.-0715 Zero Drift 0 0 0
14 09^)4 Zero Dnft 67 0 67
141048 Zero Dnft 155 0 155
1414-04 Zero Drift 0 0 0
14.1614 Zero Drift 1750 0 1750
1418.-00 Zero Drift 3750 0 3750
1419-J8 Zero Dnft 1775 0 1775
Comment
Oifrerenc* (Diff) is the Response minus the Target
13
MPF Fuel Flow
Cal Dnft Day 4
Minimum Req'd 84483scfm
BvenLOafL
.^FoJa^Fuinflit ji/ Total novt
* ai043BTU;cf
18-May-10 0702 00 158 164690
18-MBy-10 0702 30 156 163021
18-May-10 07 03-00 157 164064
18-May-1007 03 30 154 160831
18^ay-10 0704 00 156 162604
18-May-10 07 04 30 154 161039
18-May-10 07 05 00 155 161769
1&^ay-10 070530 157 163751
18-May-10 07 0600 157 163230
18-May-100706 30 155 161665
18-May-1007 07 00 155 161561
18-May-1007 07 30 154 160309
18-May-10 07 0800 154 160622
18-May-10 07 08 30 154 160935
18-May-10 07 09 00 154 160831
18-May-10 07 09 30 154 160205
18-May-10 0710 00 153 159266
18-May-10 0710 30 152 158327
18-May-10 0711 00 154 160413
18-May-10 0711 30 154 160726
18-May-10 07 12 00 153 159892
18-May-10 0712 30 153 159892
^^^^^^^
Agpf)^^^
Ag^n ^
^^^^^
0 164690
0 163021
0 164064
0 160831
0 162604
0 161039
0 161769
0 163751
0 163230
0 161665
0 161561
0 160300
0 160622
0 180935
0 160831
0 160205
0 159266
0 158327
0 160413
0 160726
0 159892
0 159892
TOCDF PDARS Data
5/18/2010
CEMS CALIBRATIO
19-MA^
N^l MMARY REPORT
OXYGEN
14-Arr 082
MPF AFTERBLOWER
Rack 105
This report or the data herein MUST be screened by the Monitoring Branch before being released from TOCDF control"
65855
Time Settine Resoonse Tareet Diff
0722.46 Zero Dnft 0 0 °\ 072542 SoanDnft 209 2a9 o) 15 03 34 Zero Drift 0 0 o" 15-0432 Zero Drift 208 0 208
15-0458 Zero Dnft 209 0 209
15-05.52 Zero Dnft 1 0 1
15-0612 Zero Dnft 0 0 0
issn-m Zero Drift 209 0 209
150726 Zero Drift 21 0 21
15-08-20 Zero Dnft 3 0 3
1509-.04 Zero Dnft 0 0 0
1510D2 Zero Dnft 20.8 0 2a8
1510-.20 Zero Dnft 21 0 21
151116 Zero Dnft 1 0 1
CARBON MONOXIDE
14-AIT-384 API-164
Time Settme Resoonse Tareet Diff
07^324 Zero Dnft 0 0 0
0727 24 SoanRl Dnft 154 153 1
0730-24 Soan R2 Drift 3775 3780 5
151202 Zero Dnft 0 0 0-
1512.52 Zero Dnft 152 0 152
151312 Zero Drift 152 0 152
1514.18 Zero Dnft 4 0 4
151440 Zero Dnft 0 0 0
151552 Zero Dnft 149 0 149
151610 Zero Drift 151 0 151
151716 Zero Dnft 3 0 3
151734 Zero Dnft 0 0 0
151854 Zero Dnft 151 0 151
15 19-10 Zero Dnft 152 0 152
15 20-.22 Zero Dnft 2 0 2
15 2152 Zero Dnft 0 0 0'
Comment
CAt_ -D^kvr 1>AY t>
Ox a.T.
difference (DIH) is the Response minus the Target
15
MPF Fuel Flow
Cal Dnft Day 5
Minimum Req'd 84483scfm
^^^^
TotalJ^Umace
I^RciwCc^)
* Total Ftok^'
19-May-10 07 20 00 117 122448
19-May-10 0720 30 120 125369
19-Alay-10 0721 00 122 126725
IWWay-10 07.21 30 122 127559
19-May-1007 22 00 128 132983
19-May-10 07 22 30 132 137989
19-May-10 07 23 00 140 146811
19-May-10 07 23 30 147 153530
19-May-10 07 24-00 155 161561
19-May-10 0724 30 157 163230
19-May-10 07 2500 157 164064
19-May-10 07 25 30 156 162917
19-May-10 07 26 00 155 161248
19-May-10 07 26 30 156 162604
19-May-10 07 27 00 164 171365
19-May-1007 2730 171 178770
19^May-10 07 28 00 170 177519
19-May-10 07 28 30 171 177936
19-May-10 07 29 00 172 179813
19-May-10 07 29 30 171 178040
19-May-10 07 30 00 171 178457
19-May-10 07 30 30 168 175015
19^ay-10 07 31 00 167 173972
19-May-10 07 31 30 166 173451
^^^^ ^^^^^
0 122448
0 125369
0 126725
0 127559
0 132983
0 137989
0 145811
0 153530
0 161561
0 163230
0 164064
0 162917
0 161248
0 162604
0 171365
0 178770
0 177519
0 177936
0 179813
0 178040
0 178457
0 175015
0 173972
0 173451
TOCDF PDARS Data
5/19/2010
1B81B
CEMS CALIBRATION,
20-MA
N^U/I MARY REPORT
OXYGEN
14-AIT-082
MPF AFTERBLOWER
Rack 105
This report or the data herein MUST be screened t>y the Monitoring Branch before being released from TOCDF control"
65855
Time Setttes Resoonse Tareet Dtff
0744.57 Zero Drift 0 0 0
0746 27 Snan Drift 209 209 0
CARBON MONOXIDE
14-AIT-384 API-164
Time Setline Resoonse Tareet DUf
074523 Zero Drift 0 0 0
074831 SoanRl Dnft 152 153 1
07 50-35 Soan R2 Drift 3775 3780 5
Comment
i/i, CA«- TVUMM- Tjrvt W
to CM- T)MPT "OM U
Purpose View CEMS daily calibration drift data by racl( numl>er - 02 is ui % and CO and NOx is in PPM
|DHference (Diff) Is the Response minus the Target"
17
MPF Fuel Flow
Cal Dnft Day 6
Minimum Req'd 84483scfm
^^^^^^^^^
20-May-10 07 43 00 156 162708
20-May-10 0743 30 165 172199
20-May-10 0744 00 187 195250
2CU«ay-10 07 44 30 209 218404
2(^ay-10 074500 213 221846
20^ay-10 074530 192 200047
20-May-10 0746 00 159 165420
2aMay-10 0746 30 139 145186
20-May.10 0747 00 139 144977
2^May-10 07-47 30 145 151444
20^ay-10 0748 00 143 149253
2O-May-10 0748 30 138 144351
20-May-10 074900 142 148315
20-May-10 0749 30 141 147167
20-May-10 07 50 00 142 148106
20-May-IO 07 50 30 146 151861
20-May-10 07 51 00 143 148836
20 May-10 07 51 30 144 150401
0 162708
0 172199
0 195250
0 218404
0 221846
0 200047
0 165420
0 145186
0 144977
0 151444
0 149253
0 144351
0 148315
0 147167
0 148106
0 151861
0 148836
0 150401
TOCDF PDARS Data
5/20/2010
CEMS CALIBRATIO
21-MA^
I^^UUI MARY REPORT
OXYGEN
14-AIT-082
MPF AFTERBLOWER
Rack 105
This report or the data herebi MUST be screened by the Monitoring Branch before being released from TOCDF control
65855
Time Setline Resoonse Tareet Diir
09 45 40 Zero Dnft 0 0 0
094654 SoanDnft 21 209 1
CARBON MONOXIDE
14-AIT-384 APM64
Time Settine Resoonse Tareet Dill
09 4832 Zero Dnft 0 0 0
09JS\ 46 SoanRl Drift 152 153 1
095512 Span R2 Drift 3775 3780 5
Comment
Purpose View CEMS daily calibration dnft data by rack number - 02 Is in % and CO and NOx is m PPM
Difference (DifQ Is the Response minus the Target
19
MPF Fuel Flow
Cal Drift Day 7
Minimum Req'd 84483sc6n
21-May-10094400 135 141014
21-May-10 0944 30 137 142474
21-May-10094SOO 137 142682
21-May-10 0946 30 137 142787
21-May-100946 00 136 141639
21-May-10 0946 30 137 142682
21-May-10 0947 00 135 141222
21-May-10 09 47 30 137 142578
21-May-10 09 48 00 138 144038
21-May-10 09 48 30 135 140701
21-May-10 09 49 00 137 142787
21-May-10 09 49 30 134 1399^1
21-MBy-10 09 5000 132 137363
21-May-10 09 50 30 131 136320
21-May-1009 51 00 130 135277
21-May-10 09 5130 129 134443
21 May-10 09 52 00 127 132878
21 May-10 09 52 30 125 130166
21-May-10 0953 00 124 129332
21-May-10 09 53 30 126 131314
21-May-10 09 54 00 130 135590
21-May-10 09 54 30 132 137363
21-May-10 09 5500 135 140596
21-May-10 09 55 30 136 141327
21-May-10 09 56 00 140 145707
21-May-10 09 56 30 143 149149
"*' "*'
AS 0 141014
0 142474
0 142682
0 142787
0 141639
0 142682
0 141222
0 142678
0 144038
0 140701
0 142787
0 139971
0 137363
0 136320
0 135277
0 134443
0 132878
0 130166
0 129332
0 J 131314
0 135590
0 137363
0 140596
0 141327
0 145707
0 149149
TOCDF PDARS Data
5/21/2010
APPENDIX B
Absolute Calibration Audit and Response Time Data Sheets
CEMS Rack, MPF 105 Absolute Calibration Audit Worksheet
CEMS Analyzer, AIT-82 Oz
O2 Analyzer S/N 65855
Manufacturer Servomei
Source I D MPF
CEMS Rack Location North PAS House
CEMS Probe Location Between PAS Houses
Date g'lg 10
SERIAL NUMBER EXPIRATION DATE
Low Cylinder rj|A
Mid Cylinder 5-T n
High Cylinder 0 lt>
Required Gas Ranges for O2
Low Mid High
0-2% 8-10% 14-16%
Range 0-25%
RUN
NUMBER
CALIBRATION
VALUE
MONITOR
RESPONSE
DIFFERENCE
RUN
NUMBER
CALIBRATION
VALUE
MONITOR
RESPONSE LOW MID HIGH
1 - Low r> 0 0 0
2-Mid <\ 0 OS"
3 - High is.os-\S.o
OS"
oS'
4-Mid ^ OS-OS ^^^^
5 - Low D 0 0 0.60
6 - High IS-05 ISO ^^^^^
7- Low 0 0 0 ou ^^^^
8-Mid
9 - High JS D
MEAN DIFFERENCE* = 0 0% 0 or
'Mean Difi^rence = Average of the three Difference values (Round to 1 dedmal place)
reviewer
Date
Date
Time
Job Title
FM-PFlPMOOOI-33 R3C0 THIS IS A RECORD
CEMS Rack, MPF 105 Absolute Calibration Audit Worksheet
CEMS Analyzer, AIT-384 CO R-1
CO Analyzer S/N
Manufacturer
Source I D .
API-164
TELEDYNE
MPF
CEMS Rack Locaton North PAS House
CEMS Probe Location Between PAS Houses
Date S'tR'\e)
SERIAL NUMBER EXPIRATION DATE
Zero Cylinder tJZ. N/A
Mid Cylinder tl'fz n
High Cylinder fZ ZS ll-
Required Gas Ranges for CO R1
Zero Mid High
0(N2) 60-80ppm 140-160ppm
Range 0-200
RUN
NUMBER
CALIBRATION
VALUE
MONITOR
RESPONSE
DIFFERENCE
RUN
NUMBER
CALIBRATION
VALUE
MONITOR
RESPONSE ZERO MID HIGH
1 - Zero o Q O 0
2-Mid 01 L
3 - High /sw
4-Mid (it (P
5-Zero 0
6 - High /srs-IT ^»-r
f. J"
7 - Zero o 0 o mm 8-Mid 67 g (ill Zl mm
9 - High /s-r iss-o
MEAN DIFFERENCE = 1 Coo
CALIBRATION ERROR* = 0 00 0^8 %
*CalEnror = MD/200x100
Round to two decimal places
Date
Reviewer Date
Time
Job Title
FM-PRPMO001-34 R3C0 THIS IS A RECORD
CEMS Rack, MPF 105 Absolute Calibration Audit Worksheet
CEMS Analyzer, AIT-384 CO R-2
CO Analyzer S/N
Manufecturer _
Source I D .
API-164
TELEDYNE
MPF
CEMS Rack Location North PAS House
CEMS Probe Location Between PAS Houses
Date ^'18'to
SERIAL NUMBER EXPIRATION DATE
Zero Cylinder N/A
Mid Cylinder // M
High Cylinder •L \'\ IS
Zero Mid High
0(N,) 1500-2000ppm 3500-4000ppm
Range 0-5000
RUN
NUMBER
CALIBRATION
VALUE
MONITOR
RESPONSE
DIFFERENCE
RUN
NUMBER
CALIBRATION
VALUE
MONITOR
RESPONSE ZERO MID HIGH
1 - Zero O 0
2-Mid nsz. ns"i z. It
3 - High 10
4-Mid 15^ .^^^
5 - Zero 1 H
6 High 18
7 - Zero 0 1 z
8-Mid nu\.\
9 High
MEAN DIFFERENCE =
CALIBRATION ERROR* =
o.en 11 Si MEAN DIFFERENCE =
CALIBRATION ERROR* = 0 o-L ^ n
* Cal Error = MD/5000x100
Round to two decimal places
Reviewer
S" ISio
Date
Date
Time
Job Title
FM-PRPMO001 35 R3C0 THIS IS A RECORD
CEMS CALIBRATION
18-MAY-:
MARY REPORT
MPF AFTERBLOWER
Rack 105
OXYGEN
14-AIT-082
Tills report or the data lierein MUST be screened by the Monitoring Branch before being released from TOCDF control
6S8S5
Tune Settine ResDODse Tareet DIfl
07-0332 Zero Dnft 0 0 0
070446 SoanDnft 20 9 209 0 .
13.42 16 Zero Dnft 0 0 0 ^
1344 30 Zero Dnft 89 0 89
13 4544 Zero Dnft 15 0 15
1347 00 Zero Dnft 9 0 9
13 4806 Zero Drift 1 0 1
13 4912 Zero Dnfl 15 0 15
13 SO 26 Zero Dnft 1 0 1
13 5146 Zero Dnft 9 0 9
1353-00 Zero Dnft 15 0 15 1
1438 54 ZeroDnfi 20.8 0 20 8 1
14 39-16 Zero Dnfl 209 0 20 9
1440-08 Zero Dnii 2 0 2
CARBON MONOXIDE
14 AIT 384 API 164
Time Settine Resoonse Tareel Diff
0704 12 Zero Dnft 0 0 Ol
0709K10 SoanRl Drift 157 155 2
071112 Soan R2 Dnft 3775 3760 15
13 57 26 Zero Drift 0 0 0
13 58 50 Zero Dnfl 68 0 68
14 00 32 Zero Drift 154 0 154
14 0154 Zero Drift 69 0 69
14 0330 Zero Dnft 0 0 0
14 05 18 Zero Dnft 154 0 154
14 0716 Zero Dnft 0 0 0
140M4 Zero Dnft 67 0 67
1410-46 Zero Dnft 155 0 155
14 14-04 Zero Dnft 0 0 0
141614 Zero Drift 1750 0 1750
14 18-00 Zero Dnft 3750 0 3750
1419 58 Zero Dnft 1775 0 1775
Commenl
I
This data is from the Response Time or
ACA tests The calculated "Difference"
between the response and target values does
not reflect pass/fail criteria, only that the
data was recorded by PDARS
OA7 «4 c-AC D«.«++
i=iCA
(it
Difference (Diff) Is the Response minus the Target
CEMS CALIBRATION d^MARY REPORT
18-MAY-2010
MPF AFTERBLOWER
Rack 105
Time Settine ResDonse Tareet Diff
142306 Zero Drift 0 0 0
14.24 48 Zero Drift 3775 0 3775
14 28 20 Zero Drift 0 0 0
14J0-10 Zero Drift 1775 0 1775
143Z.24 Zero Dnft 3750 0 3750
14 43 56 Zero Drift 0 0 0
14 4632 Zero Dnft 1 0 1
14 47 42 Zero Dnft 153 0 153
1449 08 Zero Dnft 3 0 3
1450.30 Zero Drift 151 0 151
14 5044 Zero Drift 154 0 154
14 5154 Zero Dnft 3 0 3
14 5212 Zero Dnft 0 0 0
14 S3 32 Zero Dnft 3750 0 3750
14 5346 Zero Drift 3725 0 3725
14 55 18 Zero Dnft 25 0 25
14 sass Zero Dnft 3750 0 3750
14 5844 Zero Drift 25 0 25
150022 Zero Dnft 3750 0 3750
15-0036 Zero Dnft 3725 0 3725
150208 Zero Drift 25 0 25
This data is from the Response Tmie or
ACA tests The calculated "Difference"
between the response and target values does
not reflect pass/fail cntena, only that the
data was recorded by PDARS
Purpose View CEMS daily calibration drift data by racli number 02 is in % and CO and NOx is in PPM
Difference (Dlft) is the Response minus the Target
MPF Fuel Flow
02andCOR1/R2ACA
Minimum Req'd: 84483scfm
r
Ma > iovt. 1 tm;
Aget}i i-eed
@lbs/hr
Age tFeed
@ib /h
Aae
h Uf
@8500BTU/lb Event Date.:^ is: Ma > iovt. 1 tm;
1 t IFIoi^$ Aget}i i-eed
@lbs/hr
Age tFeed
@ib /h
Feed
@ tosl/nn
h Uf
@8500BTU/lb
To|j BTU «, Ulte'S 18-May-1013:41:00 154 160413 0 160413
18-May-1013:41:30 154 160726 0 160726
18-May-10 13:42:00 154 161039 0 161039
18-May-10 13:42:30 155 162082 0 162082
18-May-1013:43:00 154 160622 0 160622
18-May-1013:43:30 154 161039 0 161039
18-May-1013:44:00 154 160518 0 160518
18-May-1013:44:30 154 160622 0 160622
18-May-1013:45:00 151 157597 0 157597
18-May-10 13:45:30 155 161248 0 161248
18-May-1013:46:00 155 161144 0 161144
18-May-1013:46:30 153 159996 0 159996
18-May-1013:47:00 153 159892 0 159892
18-May-1013:47:30 154 160309 0 160309
18-May-10 13:48:00 153 159996 0 159996
18-May-10 13:48:30 154 160205 0 160205
18-May-10 13:49:00 152 158119 0 158119
1S-May-10 13:49:30 149 155511 0 155511
18-May-10 13:50:00 147 153008 0 153008
18-May-10 13:50:30 143 148732 0 148732
18-May-10 13:51:00 140 146333 0 146333
18-May-1013:51:30 136 141327 0 141327
18-May-10 13:52:00 136 142161 0 142161
ie-May-10 13:52:30 135 140492 0 140492
18-May-10 13:53:00 134 139971 0 139971
18-May-10 13:53:30 134 139345 0 139345
118-May-10 13:54:00 132 137989 0 137989
118-May-10 13:54:30 132 137572 0 137672
18-May-10 13:55:00 132 137259 0 137259
18-May-10 13:55:30 132 137885 0 137885
18-May-10 13:56:00 135 140492 0 140492
18-May-1013:56:30 134 139345 0 139345
18-May-10 13:57:00 135 140284 0 140284
18-May-1013:57:30 134 139658 0 139658
18-May-1013:58:00 134 139658 0 139658
18-May-10 13:58:30 134 139449 0 139449
18-May-10 13:59:00 135 140284 0 140284
18-May-10 13:59:30 136 141952 0 141952
18-May-10 14:00:00 136 141848 0 141848
18-May-10 14:00:30 136 141535 0 141535
18-May-10 14:01:00 136 141431 0 141431
18-May-10 14:01:30 136 141744 0 141744
18-May-10 14:02:00 136 142265 0 142265
18-May-10 14:02:30 137 142578 0 142578
18-May-1014:03:00 136 141535 0 141535
18-May-1014:03:30 138 143830 0 143830
18-May-1014:04:00 135 140388 0 140388
18-May-1014.-04:30 137 142891 0 142891
18-May-1014:05:00 138 143621 0 143621
18-May-10 14:05:30 137 142370 0 142370
18-May-10 14:06:00 136 141846 0 141848
18-May-10 14:06:30 136 141639 0 141639
18-May-10 14:07:00 136 141639 0 141639
18-May-10 14:07:30 136 141744 0 141744
18-May-10 14:08:00 138 143517 0 143517
18-May-10 14:08:30 137 143308 0 143308
18-May-1014:09:00 135 140701 0 140701
TOCDF PDARS Data
5/18/2010
8
MPF Fuel Flow
02 and CO R1/R2ACA
Minimum Req'd: 84483sdrn
1
To It low
Ol043BTU/cf
Agent Feed
@ibsAi
A niFeed
Ageni
1 taid u
V 1 c E c iD V No hlo VI ni
1
To It low
Ol043BTU/cf
Agent Feed
@ibsAi
A niFeed Feed
S it^sAr
cSIJ 1 0
S.a KiJb
1 taid u
V 1 c
18-May-10 14:09:30 137 142370 0 142370
18-May-10 14:10:00 138 144351 0 144351
18-May-10 14:10:30 140 145603 0 145603
18-May-10 14:11:00 141 146542 0 146542
18-May-10 14:11:30 140 146124 0 146124
18-May-1014:12:00 134 139241 0 139241
18-May-1014:12:30 131 136633 0 136633
18-May-1014:13:00 . 129 134338 0 134338
18-May-1014:13:30 129 134130 0 134130
18-May-10 14:14:00 134 . 139449 0 139449
18-May-10 14:14:30 136 141639 0 141639
18-May-1014:15:00 139 144768 0 144768
18-May-1014:15:30 141 147376 0 147376
18-May-10 14:16:00 148 154364 0 154364
18-May-10 14:16:30 174 . 181691 0 181691
18-May-10 14:17:00 206 214545 0 214545
18-May-1014:17:30 211 219864 0 219864
18-May-10 14:18.00 212 221325 0 221325
18-May-1014:18:30 213 222472 0 222472
18-May-1014:19:00 212 220699 0 220699
1&-May-1014:19:30 205 213919 0 213919
18-May-10 14:20:00 198 206618 0 206618
18-May-1014:20:30 195 203176 0 203176
18-May-10 14:21:00 194 202655 0 202655
18-May-1014:21:30 190 198587 0 198587
18-May-1014:22:00 185 193372 0 493372
18-May-10 14:22:30 180 187531 0 187531
18-May-10 14:23:00 174 181065 0 181065
18-May-10 14:23:30 163 170113 0 170113
18-May-10 14:24:00 143 149566 0 149566
18-May-10 14:24:30 132 137363 0 137363
18-May-10 14:25:00 129 134651 0 134651
18-May-1014:25:30 124 128811 0 128811
18-May-1014:26:00 120 125264 0 125264
18-May-1014:26:30 118 122970 0 122970
18-May-10 14:27:00 114 118589 0 118589
18-May-10 14:27:30 113 118068 0 118068
18-May-10 14:28:00 112 116816 0 116816
18-May-10 14:28:30 114 119319 0 119319
18-May-10 14:29:00 114 118589 0 118589
18-May-10 14:29:30 115 119736 0 119736
18-Mav-10 14:30:00 117 122240 122240
18-Mav-10 14:30:30 117 122240 122240
18-Mav-10 14:31:00 117 121822 121822
18-Mav-1014:31:30 119 124013 124013
18-Mav-1014:32:00 120 125056 125056
18-May-10 14:32:30 120 124847 124847
18-May-1014:33:00 122 127350 127350
18-May-10 14:33:30 122 127246 127246
TOCDF PDARS Data
5/18/2010
CEMS RESPONSE TIME DETERMINATION
Plant Name TOCDF Date 5/19/10
Furnace MPF Rack# 105 AIT-082 Operator(s)(f7X^^_^
Analyzer Type Serial No Range Clock Time RTi Clock Time RTz Clock Time RT3
02 65855 0-25% Upscale
Response
02 65855 0-25% Downscale
Response
Upscale
Response
Downscale
Response
DEFINITIONS
RT = Response Time in mm ss
Response Time Average (mm ss}
Range o-2S%
Average Upscale .'QS
Average Downscale . 9 S
Range
Average Upg
Average QtJ^nscale
FM-PRPMO001-64 RSCO THIS IS A RECORD
CEMS RESPONSE TIME DETERMINATION
Plant Name TOCDF Date 5/19/10
Furnace MPF Rack# 105 AIT-384 Operator(s)^^'-<''^J
Analyzer Type Serial No Range Clock Time Clock Time RTz Clock Time ^ RT3
CO API-164 0-200ppm Upscale
Response tS'lI
CO API-164 0-200ppm Downscale
Response is-^r
CO API-164 0-500Gppm Upscale
Response
CO API-164 0-5000ppm Downscale
Response \SZ3
DEFINITIONS
RT = Response Time in mm ss
Response Time Average (mm ss)
Range
Average Upscale tl07
Average Downscale !«' O*^
Range
Average Upscale L*. Z.^-
Average Downscale r« Z5
FM-PRPMO001-64 R3C0 THIS IS A RECORD
OXYGEN
14 AIT-08Z
CEMS CALIBRATIO,
19-M m UMMARY REPORT
10
MPF AFTERBLOWER
Rack 105
This report or the data herein MUST be screened by the Monitoring Branch before being released from TOCDF control
658S5
Tunc Settint Resoonse Taraet DifT
07 2246 Zero Dnft 0 0 0
07.25 42 SoanDnft 209 209 0
15-0334 Zero Dnft 0 0 0
1504 32 Zero Dnft 208 0 208
15-04 58 Zero Drift 209 0 209
15-05 52 Zero Dnft 1 0 1
15-06 12 Zero Dnft 0 0 0
1507-08 Zero Drift 209 0 209
1507 26 Zero Drift 21 0 21
IS 08 20 ZeroDnfi 3 0 3
1509 04 Zero Drift 0 0 0
IS 10 02 ZeroDnfi 20.8 0 208
151020 Zero Dnft 21 0 21
IS 1116 Zero Dnft 1 0 1
Comment
This data is from the Response Time or
ACA tests The calculated "Difference"
between the response and target values does
not reflect pass/fail criteria, only that the
data was recorded by PDARS
CARBON MONOXIDE
14 AIT-384 API 164
Time Settme Resoonse Tareet Difl
0723 24 Zero Drift 0 0 0
0727 24 SoanRl Drift 154 153 1
0730 24 Soan R2 Dnft 3775 3780 5
151202 Zero Dnft 0 0 tf
1512 52 Zero Drift 152 0 152
151312 Zero Drift 152 0 152
151418 Zero Drift 4 0 4
1514 40 Zero Dnft 0 0 0
151552 Zero Drift 149 0 149
151610 Zero Dnft 151 Q 151
151716 Zero Dnft 3 0 3
1517 34 Zero Drift 0 0 0
1518 54 Zero Dnft 151 0 151
151910 Zero Drift 152 0 152
15 2022 Zero Dnft 2 0 2
15 2152 Zero Drift 0 0 0
difference (Dtff) Is the Responee minus the TargeT
CEMS CALIBRATIO
19-M A
i^yi MMARY REPORT
0
MPF AFTERBLOWER
Rack 105
Time Settme Resoonse Taraet Dift
152314 Zero Dnft 3725 0 3725
152332 Zero Dnft 3750 0 3750
1524 58 Zero Dnft 25 0 25
15 2516 Zero Drift 0 0 0
15 2638 Zero Drift 3750 0 3750
15 2656 Zero Drift 3750 0 3750
IS 2818 Zero Dnft 25 0 25
IS 28 34 Zero Dnft 0 0 0
15 30 00 Zero Dnft 3775 0 3775
15 30 18 Zero Drift 3775 0 3775
15 Jl 44 Zero Dnft 25 0 25
This data is from the Response Time or
ACA tests The calculated "Difference"
between the response and target values does
not reflect pass/fail criteria, only that the
data was recorded by PDARS
Purpose View CEMS daily calibration dnft daU by rack number - 02 is in % and CO and NOx is in PPM
Difference (Diff) Is the Response minus the Target
13
MPF Fuel Flow
02 CO Resp Time
Minimum Req'd 844S3scfm
19-Mav-1015 0200 136 142161
19-Mav-101502 30 137 142370
19-Mav-101503 00 138 143934
194Aav-10 15 03 30 138 143830
19-Mav-1015 04 00 140 145811
19-Mav-10 15 04 30 141 147480
1»Mav-1015 05 00 146 152278
ig^av-1015 05 30 148 154468
19-Mav-10 15 06 00 150 156033
19-Mav 10 15 06 30 152 158745
19-H/lay 10 15 07 00 154 160726
19-May-10 15 07 30 154 160101
19-Mav-10 15 08 00 154 160518
19-Mav-1015 0830 158 164794
19-Hflay-10 150900 162 169279
19-May-10 15 09 30 159 165733
19-Mav-101510 00 157 163751
19-IWav-1015 1030 153 159370
19-Mav-101511 00 163 170113
19-IWIav-101511 30 186 194311
ig-Mav-10 1512 00 166 173138
19-May-101512 30 127 132357
19-)Vlay-101513 00 122 126933
19-May-101513 30 125 129854
19-Mav-10 15 14 00 119 123700
19-May-101514 30 117 121718
19-IVIav-10151500 112 117025
19-Mav-101515 30 113 117859
19-Mav-101516 00 113 117755
19-Mav-101516 30 113 117338
19-May-10 1517 00 112 116295
19-Mav-10 15 17 30 112 116920
19-May 101518 00 112 117233
19-Mav 101618 30 113 117338
ig-May 101519 00 114 119111
19 Mav-101519 30 116 120675
19-Mav-1015 20 00 116 120884
19-May-101S20 30 119 124013
19^iflav-1015 21 00 121 125682
19-Mav-1015 21 30 122 127142
19-Mav-1015 22 00 124 129332
19-Mav-1015 22 30 125 129854
19-May-10 1523 00 125 130688
19-Mav-1015 23 30 126 131835
19-May 10 15 24 00 126 131001
19-Mav-10 1524 30 126 131731
19-Mav 10 15 2500 127 132461
19-May-1015 25 30 129 134443
19-May 10 15 26 00 129 134234
19 May-1015 26 30 129 134234
19-May 101527 00 127 132044
19 May-1015 27 30 127 132670
19 May 1015 28 00 130 135173
19-May 1015 28 30 129 134547
19 May-1015 29 00 126 131835
19 Mav-10 15 29 30 128 133713
19-Mav 10 15 30 00 129 134651
ig-May-1015 30 30 129 134860
19-May-1015 31 00 129 134234
1^av-1015 31 30 129 134860
19-May 1015 32 00 129 134547
19-May 1015 32 30 129 134756
^^^^
^^^^
^^^^^
^^i5a%
142161
142370
143934
143830
145811
147480
152278
154468
156033
158745
160726
160101
160518
164794
169279
165733
163751
159370
170113
194311
173138
132357
126933
129854
123700
121718
117025
117859
117755
117338
116295
116920
117233
117338
119111
120675
120884
124013
125682
127142
129332
129854
130688
131835
131001
131731
132461
134443
134234
134234
132044
132670
135173
134547
131835
133713
134651
134860
134234
134860
134547
134756
TOCDF PDARS Data
5/19/2010
APPENDIX C
Relative Accuracy Spreadsheet and Reference Method Data
Method 1 - Circular Duct - Determination of Traverse Points
Project Name J^i^jVJP/Off/l-
Project Number ybnytryggg'
Date <li*il IO
Souixre tAfP-tHO^^
Operator
• velocity^afffy ii/j^
• l£gkrttetic Sampling *^f^
Upstream Distance (ft/in)
D Measurement
• Plant Information
Number of Ports to be sampled '
Upstream Distance (ft/in)
D Measurement
• Plant Information
Duct Dtepieter (m) f C
•Measurement
• Plant Information
Dowfnstream Distance (ft/in)
D Measurement
• Plant Information
Total number of Traverse Points (from Figure 2
(veloaty) or 1 (all Isokinetic sampling)) 3
Number of traverse points per port {
Port Depth
Traverse
Point
Percent
of
Diameter
Distance
from Wall ^
(in)
Marking
Location
(in)
1 U T
2
3
4 /
5 /
6 /
7 /
8
9 /
10 /
11 /
12
Traverse
Point
Percent
of
Diameter
Distance
from Wall
(in)
Marking
Location
On)
13 J
14 /
15 /
16
17
18
19
20
21
22
23
24
Prepare a drawling of the source, showing the ports, disturbances, and the distances
^ According to Method 1, for stacks between 12 and 24", no point may be within inch of the
wall For stacks greater than 24", no point may be within 1 inch of the wall
FOS-03A Method 1 Circular Ouct
ReviSipnDate November 2009
Response Time Detenniiiation - EPA Method 7E
Applicable to Performance of EPA Methods 3A, 6C, 7E and 10
Project Name: Ihcc^F- C&^Hk Krf77^/1^>^^%Sow<»i Q**^
Project Number: Vo^Yci,yptp'/ Date: _^j|i3:^/^IgL,_^
t^tion; GH.^ Sk«-£ (Zoe'/.L/) Time ^^rg"
Parameter c o 1
Analyzer Make and 1 ^
Model dair«r«K4^ /
Analyzer Name| ^K*^jL,;>
Analyzer Range
From Zero Upscale Zero Upscale Zero Upscale
To Upscale Zero Upscale Zero Upscale Zero
Start Time (iih mm) hiot. </<r
15 sec /«.«
30 sec 0x1,0
45 sec 96 r
60 sec 59 r
75 sec
90 sec
105 sec
120 sec ?
135 sec
P 150 sec
165 sec
180 sec
195 sec u
Response Time* Co Co lor
Analyzer Response
Time* CO
- ^-Time In seconds to reach 95% of flnal stable value
^ Greater of upscale and downscale response time
1 Cylinder Number Actual Value
Upscale
Upscale
Upscale
Zero 0
FbS-lOS>A TECmOe^onso Twite
Revision Oate October2009
stratification Determination - EPA Method ^E
Applicable to Performance of EPA Methods 3A, 6C, 7E and 10
Parameter
Plant
Source
Operator At?ig>
Analyzer Make and Model
Analyzer Tag
Analyzer S/N
Analyzer Range
System Response Time Co Sek»^
Traverse Pomts
(3 are required) Marking Location Sampling Duration Concentration Vo Difference
from Mean
1 ll. Ss-?
2 O./S'
3 ll Qf>-
4
5
• 6
7
8 •
9
10
11
12 • ,,, 12 —*
Mean Concentration of all Traverse Points
•'^^^5!*«"r "'•i"'*al
Stratification Test Criteria* - Evaluate in Order ^
1 Do the concentrations at each traverse point differ from the mean concentration by no
more than (a) +5 0% of the mean or (b) ±0 5 ppm (whichever is less resb-icbve)'
If YES, use 1
point
Do the concentrations at each traverse point differ from the mean concentrabon by more
than (a) ±5 0% of the mean or (b) ±0 5 ppm (virhichever Is less restnctlve) and by no more
than (a) ±10 0% of the mean or (bj ±10 ppm (wrtiichever is less resbictlve)'
If YES, use 3
points
3 Do the concentrations at each traverse point differ from the mean concentration by more
than (a) ±10 0% of the mean or (b) ±10 ppm (wrhichever Is less restrictive)'
If YES, use 12
points
* According to EPA Method 3A, Section 8 1, the altemabve acceptance cntenon for 3-point sampling is ±0 5% COi or O2, and the criterion for
single-point sampling is ±0 3% CO2 or O2
Notes
FOS-J2 SiratifKotion Test
Revision Date March 2009
Reviewed February 2010
CEMS Operation Log
Project -^jo yw/f O^lli Page ^ of ^
'ProjectNumber \fcAt/^i_VO{>^ Operator /hO&ftiC.
Source A»fp
Time Activity
Analyzer Response Sample
Flow
Rate
Time Activity
Sample
Flow
Rate
Turn on Analyzers'
/ / V. ^
---
r —
H Ob .
O 4
A»ri^,
5. 1^***,
tk
y At <?.^ Orll s O
10 ft a. , ,.f.. f ,
a/3
... /?tu, /
O, ft
Sfoa U.OAO.l<f.i*//l CO, /O, 1r sr. e>
», (S
fflBl$ -
O }') 0 0%
// 0/<5, /«J6/> C(h 10.V U2
pel _—
fil fin
^«-/
Ei.
0 }(, S.o
lOnl
O.VL 0 Z.9 o.lS
/»» ^/
7 16
6 li
10 it
U Tt-M
' Turn On Analyzers" is to document sufficient warm up time
If applicable, 'yesterday" Is an acceptable entry FOS OlA CEMS Operation
Reyision Date September 2009
CEMS Operation Log
Project :iO\0 ^^X-Page 1 of ^
ProjectNumber ^5(>\^lMd.oS Operator >\DB|0^
Source ^WPP-Date $ \^l\o
Time Activity
Analyzer Response Sample
Flow
Rate
Time Activity
Sample
Flow
Rate
Tarn on Anders' ------
0 1-7 0 »"J % 0
IV0/. Ol./ CO,
a r 1 /-l L /
o.n
Til
1017-
1 loos
Mn.i CO
you
ion o.tl OIL
—•— ' *• , ^
.4t lo2i
lOHO
L=
/dV3 J. 72.
0 to 0 U
—• 1" •F ^
o lg o.o<?
0 11. 0
1 a I
(7)4 r 0
/ZoV
Sir-
F' >• ' ''
^ .-2-O o4
U ^.'^..M. ——
x^*^
' "Turn On Analyzers' s to docunwnt suffiaent warm up time
If applicable, 'yesterday* Is an acceptable entry FDS-OIA CEMS Operation
Revision Date Septemlxr 2009
Project Z.f "> (y\Pf:rUin/\ Page "J of 3
Project Number l^«><)Sl.'l^Wd 05" Operator
Source fV\Pf"-pf^^ •3'4f«-+
Calibration Gases
Component(s) Concentration(s) Cylinder ID
CO
CO
Jo /« >
Indicate multi-component standards appropriately
Instrument Identification
Anaiyte Manufac
turer*
Model
Number Soiai Nnmber Instrument Name
CO
I wo
—-—^
Method Performance Checks
Activity Method Criterion InWais
Span Sdecbon
3A,6Q7E,
10 Efflissfocis ti^iw^jr^O%|^ of calBjtabon span
Span Sdecbon
25A Span 1 5-2.5 times'the emission ImH; if no emittion
limS; span t.5-2 5 times expectad level -—
CaBbrabon Gas
Selection
3^ 6C, 7E,
10
Protocol gas, callbiation span, 40-60% of cattiration
span, and <2a<ft of caObtabon span (or zero gas) DC CaBbrabon Gas
Selection 25A Protocol gas 25-35%, 45-55% and 80-90% of «pai^ zero grade air
Calibration Encr
3A, 6C; 76,
10
Span gas withm :fe2% of caBbration span PL
Calibration Encr
3A, 6C; 76,
10 Mid-range gas within d:2% of CBlil)ratIon span
Calibration Encr
3A, 6C; 76,
10 Zero gas withm ±2% of calibration span Calibration Encr
2SA
Low-range gas withh 54it of ceitlfled value — Calibration Encr
2SA Mid-range gas within 5% of certffled value
Calibration Encr
2SA
Span gas wiINn 5% of certified value —
Converter Oiedc 7E 290% converter efficiency
System Bias
Check
3A, 60,7E,
10
Selected gas wttNn ±5% of calibtabon to measured
value during calibration enor System Bias
Check 25A Not Applicable —
Response Time 3A, 6C, 7E,
10,25A
No cntena, evaluated to determine duratton at sample
points Oc
Sample Flow
Rate
3A,6C;7E,
10
Stable sample flow rate vnthin 10% of foKv rate
established dunng system response bme dtedc and
bias check 0^
3 Point
Stratification
Check*'
3A, 6Q 7E,
10
± 5% of mean at each point - single point
± 5-10% of mean at each point - 3 points
> 10% Of mean at each pomt 12 pomts
DC-
Post Test
CalibtatiDn Dnft
Che*
3A,6q,7E,
10
Selected gas reading within ±3% of callbiation span of
pre-tEst readng Dt.
Post Test
CalibtatiDn Dnft
Che*
3A,6q,7E,
10 Zero gas within ±3% of caBbration span of pre-test
reading Post Test
CalibtatiDn Dnft
Che*
25A
Selected gas readbtg wltHn ±3% of span of pre-test
readng
Post Test
CalibtatiDn Dnft
Che*
25A
Zem qis within ±3% of span of previous reading —
^ The strabftcatian check Is not required for stacks or ducts <A Inchai in dlametar
Hourly Drift Check (M25A only)
Selected gas reading vnthin
i;3% of span of Initial reading
Zero gas within ±3% of span
of mifaal reading
Hourl Hour 2 Hour 3 Hour 4 Hour 5 Hour 6
Okay (initiate)
^ Code T - Thenno, W - Western, C - California, S - Servomex, O -Omega FDS-OIBCEMS OpTotion
RaviSlanDala Septenier 20O9
CEMs Samphng System Audit Log
Project ^<,,o (^Pf MT4 Page / of ^
ProjectNumber Y6t*/«.2VA^ Operator Av^jpC
Source /f7/^ . Ouf fe t Date Sli^lfa
vehicle ID \A^04^\%tJ<
Heated Une ID 1 HC-^
Sample Pump ID 1 OhWA) ^
ChiilerlD Cua.L.y
Time
Heated UneTenn pCF) Sample Pump Temp {"^F) Chiller Temp
(T)
Sample Flow
(Ipm) Time Section 1 Section 2 Section 3 Pump 1 Pump 2 Chiller Temp
(T)
Sample Flow
(Ipm) Time Section 1 Section 2 Section 3 Head 1 Head 2 Head 1 Head 2
Chiller Temp
(T)
Sample Flow
(Ipm)
2cr 7cr 5". o
U$ in'). 720 — — CO
uc m -
—
/^"^
Comments-
FDS-n PS CEMS System Audit
Revision Date February 2009
2010 MPF RATA
Relative Accuracy Results
5/19/2010 TIME
URS TCEMS
O2
%
CO
PPIVIV
CO
PPMV
O2 Corr
STACK ANALYZERS
14-Ait-082
O2
{%)
Use
of
Run'
14-Ait 384
CO
PPMV
Use
of
Run'
ARITHMETIC DIFFERENCE
O2
(%)
Use
of
Run'
CO
PPMV
O2 Corr
Use
of
Run'
Run 1
Run 2
Run 3
Run 4
Run 5
Run 6
Run 7
Run 8
Run 9
Run 10
736-757
804-825
830-851
857-918
924-945
951-1012
1019-1040
1047-1108
1140-1201
1208-1229
11 50
11 86
12 02
12 09
12 23
12 24
12 21
12 20
11 89
11 77
0 73
0 81
0 93
0 92
0 76
0 77
0 64
0 79
0 97
0 91
1 08
1 25
1 45
1 45
1 22
1 24
1 03
1 26
1 50
1 39
12 0
11 8
11 9
120
122
122
122
12 1
11 9
11 8
20
20
2 0
1 0
00
0 0
0 0
1 0
2 0
20
-0 50
0 06
0 12
0 09
0 03
0 04
0 01
0 10
-0 01
-0 03
0 92
-0 75
-0 55
0 45
1 22
1 24
1 03
0 26
-0 50
-0 61
Average 12 001 1 287 Number of Runs Used in Calculation
Average Difference
Standard Deviation
t-Value
Confidence Coeffient
Permit Limit
Relative Accuracy (Absolute Average Difference
Relative Accuracy (Absolute Average Difference + Absolute CC]
Relative Accuracy (% of Reference Method]
Relative Accuracy (% of Permit Liipit)
10
-0 01
0 18
2 262
0 13
NA
0 01
0 14
1 15
NA
10
0 09
0 86
2 262
0 61
100
0 09
0 70
54 36
0 70
An X in this column denotes a run which is not used in calculation of relative accuracy
10
2010 MPF RATA
URS TCEMS
Bias Corrected Concentrations
Uncorrected Concentrations
O2 CO
19-May-10 Time (%) (ppmv)
Run 1 , 736-757 - ^-11 42 155,,'
Run 2 '• - 8P4-825>'-' 11 76. :% 168 '•^
Run 3 : ; 5 830-851 - ' 11 91 -• ' M 77
Run 4 - ' "857-918" .... - * 11 99-' 1 73 \ -,-
Run 5 .. ' •924-945 \ ^ '-12 13 -159
Run 6 - 951-1012'"'., •^1- ,,^1213 ' ^ i 63 •
Run 7 ' . '1019-1040 ' 1213 . -• ••i52' l'
Run 8 104741108 -t ', %i212; ' '"'. -1 63 ' .
Run 9 "''I140r1201 'Vl182' -•. ..1 74-:,^
Run 10 ''1208.-1229 ., . 11-70'il
Corrected O2 Cone
02 Eq 7E-5 Factors Bias Corrected
5/19/2010 Time (%) Co Cma/(Cm-Co) Concentration
Run 1 736-757 11 42 0 17 1 02 11 50
Run 2 804-825 11 76 0 18 1 02 11 86
Run 3 830-851 11 91 0 19 1 03 12 02
Run 4 857-918 11 99 0 20 1 02 12 09
Run 5 924-945 12 13 0 21 1 03 12 23
Run 6 951-1012 12 13 0 21 1 03 12 24
Run 7 1019-1040 12 13 0 18 1 02 12 21
Run 8 1047-1108 12 12 0 17 1 02 12 20
Run 9 1140-1201 11 82 0 17 1 02 11 89
Run 10 1208-1229 11 70 0 16 1 02 11 77
Corrected CO Cone
CO Eq 7E-5 Factors Bias Corrected
5/19/2010 Time (ppm) Co Cma/(Cm-Co) Concentration
Run 1 736-757 1 55 0 83 1 03 0 73
Run 2 804-825 1 68 0 89 1 02 0 81
Run 3 830-851 1 77 0 87 1 02 0 93
Run 4 857-918 1 73 0 83 1 02 0 92
Run 5 924-945 1 59 0 85 1 02 0 76
Run 6 951-1012 1 63 0 87 1 02 0 77
Run 7 1019-1040 1 52 0 89 1 02 0 64
Run 8 1047-1108 1 63 0 85 1 02 0 79
Run 9 1140-1201 1 74 0 78 1 02 0 97
Run 10 1208-1229 1 73 084 1 02 0 91
11
2010 MPF RATA
URS TCEMS Raw Data
12 hourtlmt 02(/) CO (ppm)
Calibnttion Error
5/19/2010 6 55 10 0 13 0 027
5/19/2010 6 55 20 0 135 0 027
5/19/2010 6 65 30 0 133 0 027
5/19/2010 6 56 40 0126 -0 027
2:eroN2 013 •0 03
5/19/2010 6 55 50 14 709 0 072
5/19/2010 6 56 00 21 665 0 027
5/19/2010 6 6610 21 84 0 327
5/19/2010 6 56 20 21846 0 518
5/19/2010 6 56 30 21 856 0 626
5/19/2010 6 56 40 21 653 0 728
5/19/2010 6 56 50 21 856 0 626
5/19/2010 6 57 00 21 66 0 527
5/19/2010 6 57 10 21 86 0 626
6il19/2010 6 57 20 21 861 0 027
5/19/20106 57 30 21 923 0 126
21 9%02/19 5AC02 21 8> •0 26
5/19/2010 6 57 40 11 11 0 023
5/19/2010 6 57 50 10 996 0 072
5/19/2010 6 58 00 11 0 072
5/19/2010 6 58 10 11 005 0 177
5/19/20106 58 20 11 008 0 276
5/19/2010 6 58 30 11 008 0 276
5/19/2010 6 58 40 10 988 0 276
5/19/2010 6 58 50 11 006 0 276
110% 02/9 64V C02 11 00 0 28
5/19/2010 6 59 00 10 857 0 276
S/19/20106 59 10 0 282 2 369
5/19/2010 6 59 20 0133 16 267
5/19/2010 6 59 30 0 131 47 843
5/19/2010 6 59 40 0 14 76 81
5/19/20106 69 50 0125 94 285
5/19/2010 7 00 00 0123 99 877
5/19/2010 7 0010 0 125 99 877
5/19/2010 7 00 20 0125 99 877
5/19/2010 7 00 30 0113 97 677
5/19/2010 7 00 40 0 111 97 081
5/19/2010 7 00 50 0114 97 276
5/19/2010 7 01 00 0109 97 677
5/19/2010 7 01 10 0 111 97 581
5/19/2010 7 01 20 0 111 97 378
5/19/2010 7 01 30 0106 97 378
6/19/2010 7 01 40 0 091 97 474
5/19/2010 7 01 60 0 319 97 779
97 8 ppm CO 017 97 54
5/19/2010 7 02 00 0 109 91 389
5/19/2010 7 02 10 0 103 76 004
5/19/2010 7 02 20 0 109 59 925
5/19/2010 7 02 30 0106 50 136
5/19/2010 7 02 40 0114 46 844
5/19/2010 7 02 50 0 116 46 536
5/19/2010 7 03 00 0 114 46 136
5/19/2010 7 03 10 0 116 45 832
5/19/2010 7 03 20 0123 46 134
5/19/2010 7 03 30 0 114 46 332
5/19/2010 7 03 40 0 088 46 136
5/19/2010 7 03 50 0 156 46 035
471 ppm CO 012 4617
5/19/2010 7 04 00 11 79 45 634
5/19/2010 7 04 10 12 376 36 249
5/19/2010 7 04 20 12 43 24 053
5/19/2010 7 04 30 12 472 11 567
5/19/2010 7 04 40 12 27 4 67
5/19/2010 7 04 50 12 081 2 068
5/19/2010 7 05 00 11 911 1 493
6/19/2010 7 05 10 11 604 1 37
5/19/2010 7 05 20 11 02 1 373
5/19/2010 7 05 30 10 217 1 373
5/19/2010 7 05 40 9 447 1 271
5/19/2010 7 05 60 8 922 1 271
5/19/2010 7 06 00 8 66 1 271
5/19/2010 7 06 10 8 537 1 37
5/19/2010 7 06 20 8 529 1 271
5/19/2010 7 06 30 8 578 1 271
5/19/2010 7 06 40 8 609 1 271
6/19/2010 7 06 50 8 641 1 274
6/19/2010 7 07 00 8 653 1 274
5/19/2010 7 07 10 8 65 1 271
5/19/2010 7 07 20 8 633 1 373
5/19/2010 7 07 30 8 66 1 274
5/19/2010 7 07 40 8 73 1 274
5/19/2010 7 07 50 8 806 1 373
5/19/2010 7 08 00 8 918 1 271
5/19/2010 7 08 10 9 002 1 274
5/19/2010 7 08 20 9 051 1 274
5/19/2010 7 08 30 9 13 1 373
5/19/2010 7 08 40 9 249 1 373
5/19/2010 7 06 50 9 313 1 373
5/19/2010 7 09 00 9 377 1 274
5/19/2010 7 09 10 9 439 1 274
5/19/2010 7 09 20 9 506 1 373
Page 1 of 24
12 2010 MPF RATA
URS TCEMS Raw Data
Calibration Bias
12 hour time 02(%) CO (ppm)
5/19/2010 7 09 30 9 596 1 373
5/19/2010 7 09 40 9 667 1 373
5/19/2010 7 09 50 9 704 1 386
5/19/2010 7 10 00 9 674 1373
5/19/2010 7 10 10 9 657 1 373
5/19/2010 7 10 20 9 761 1373
5/19/2010 7 10 30 9818 1 274
5/19/2010 7 10 40 9 843 1274
5/19/2010 7 10 50 9 85 1271
5/19/20107 11 00 9 815 1 373
5/19/2010 7 11 10 9 82 1 373
5/19/2010 711 20 9 877 1271
5/19/2010 711 30 9 875 1 373
5/19/2010 711 40 9 905 1 373
5/19/2010 7 11 50 9 93 1 373
5/19/2010 712 00 10011 1 373
5/19/2010 712 10 10 083 1 373
5/19/2010 7 12 20 10 058 1 37
5/19/2010 7 12 30 9 801 1 472
5/19/2010 7 12 40 9 351 1 472
5/19/2010 7 12 50 8 975 1 373
5/19/2010 7 13 00 8 913 1 472
6/19/2010 7 13 10 9 017 1 472
5/19/2010 7 13 20 8 954 1 571
5/19/2010 7 13 30 8 638 1 571
5/19/2010 713 40 8 227 1 571
5/19/2010 7 13 50 7 857 1 571
5/19/2010 7 14 00 7 638 1 571
5/19/2010 7 1410 7 648 1 571
5/19/2010 714 20 7 617 1 672
5/19/2010 7 14 30 7 468 1 672
5/19/2010 7 14 40 7 377 1672
5/19/2010 7 14 50 7 391 1 672
5/19/2010 7 15 00 7 443 1 672
5/19/2010 7 15 10 7 659 1672
6/19/2010 7 15 20 8 077 1 672
5/19/2010 7 15 30 8 596 1 672
5/19/2010 7 15 40 9 148 1 672
5/19/2010 7 15 50 9 632 1 672
5/19/2010 7 16 00 10 004 1 571
5/19/2010 716 10 10 325 1 672
5/19/2010716 20 10 583 1 672
5/19/2010 7 16 30 10 793 1 672
5/19/20107 1640 10 899 1 672
5/19/2010 7 16 50 10 926 1 667
5/19/2010 7 17 00 10 956 1 672
5/19/2010 7 17 10 10 949 1 672
5/19/2010 7 17 20 10 627 1 672
5/19/2010 7 17 30 10 681 1 672
5/19/2010 7 17 40 10 624 1 672
5/19/2010 7 17 50 10 562 1 672
5/19/2010 7 18 00 10419 1 672
5/19/2010 7 18 10 10 296 1 672
5/19/2010 7 18 20 10 239 1 771
S/19/2010 7 16 20 10 169 1 672
5/19/2010 7 16 40 10 174 1 672
5/19/2010 7 18 50 10 162 1 672
5/19/2010 7 19 00 10 145 1 672
5/19/2010 7 19 10 10 271 1 672
5/19/2010 7 19 20 10 528 1 679
5/19/2010 7 19 30 10 795 1 672
5/19/2010 7 19 40 11 013 1 687
5/19/2010 7 19 50 11 159 1 672
6/19/2010 7 20 00 11 28 1 672
5/19/2010 7 2010 11 349 1 672
6/19/2010 7 20 20 11 396 1 672
5/19/2010720 30 11 429 1 672
5/19/2010 720 40 11 461 1 672
5/19/2010 7 20 50 11 522 1 675
5/19/2010 7 21 00 11 577 1 576
5/19/2010 7 21 10 11 624 1 576
5/19/2010 7 21 20 11 651 1 571
5/19/2010 721 30 11 683 1 675
5/19/2010 7 21 40 11 743 1 576
5/19/2010 7 21 50 11 812 1 571
6/19/2010 7 22 00 418 1 675
5/19/2010 7 22 10 3 992 4 772
5/19/2010 7 22 20 11 315 12 769
5/19/2010 7 22 30 12 932 18 865
5/19/2010 7 22 40 6 688 18266
5/19/2010 7 22 50 2 402 23 958
5/19/2010 7 23 00 0465 36 448
5/19/2010 7 2310 0 18 42 742
5/19/2010 7 23 20 0182 44 941
5/19/2010 7 23 30 0 173 45 142
5/19/2010 7 23 40 0 165 45 742
5/19/2010 7 23 50 0153 46 237
6/19/2010 7 24 00 0 146 46 437
5/19/2010 7 24 10 0 173 46 536
5/19/2010 7 24 20 0 161 46 737
5/19/2010 7 24 30 7 975 46 635
Page 2 of 24
13
2010 MPF RATA
URS TCEMS Raw Data
471 ppm CO
12 hour time 02(%) CO (ppm)
2 77 46 64
5/19/2010 7 24 40 10 644 43 64
5/19/2010 7 24 50 10 901 32 553
5/19/20107 25 00 10 917 17 661
5/19/2010 7 2510 10 932 7 668
5/19/20107 2520 10 924 2 872
5/19/2010 7 25 30 10 948 1 175
5/19/2010 7 25 40 10 936 0 675
>2 10 94 157
5/19/2010 7 25 50 10 37 0 576
5/19/2010 7 26 00 4 677 0 675
5/19/2010 7 2610 3 356 0 774
5/19/2010 7 26 20 2 209 0 974
5/19/2010 7 26 30 2 078 0 974
5/19/2010 7 26 40 2 075 1 064
5/19/2010 7 26 50 1 949 0 965
5/19/2010 7 27 00 1 738 0 965
5/19/2010 7 27 10 1 756 0 866
5/19/2010 7 27 20 0 606 0 866
5/19/2010 7 27 30 0 165 0 866
5/19/2010 7 27 40 0 153 0 965
5/19/2010 7 27 50 0178 0 866
5/19/2010 7 28 00 0172 0 767
5/19/2010 7 28 10 0156 0 767
017 0 80
5/19/2010 7 28 20 5 16 0 764
5/19/2010 7 28 30 10 694 0 767
5/19/2010 7 28 40 10 773 0 866
5/19/2010 7 28 50 10 771 1 064
5/19/2010 7 29 00 10 786 1 466
5/19/2010 7 2910 10 818 2 563
5/19/2010 7 29 20 10 854 4 563
5/19/2010 7 29 30 10 859 6 459
5/19/2010 7 29 40 10 675 7 557
5/19/2010 7 29 50 10 874 8 067
5/19/2010 7 30 00 10 855 7 958
6/19/2010 7 3010 10 849 7 649
5/19/2010 7 30 20 10 664 7 58
5/19/2010 7 30 30 10 865 7 752
5/19/2010 7 30 40 10 855 7 951
5/19/2010 7 30 50 10 82 7 951
5/19/2010 7 31 00 10 766 7 951
5/19/2010 7 31 10 10 832 8 153
5/19/2010 7 31 20 10 875 7 653
5/19/2010 7 31 30 10 901 6 154
5/19/2010 7 31 40 10 954 4 056
5/19/2010 7 31 50 10 961 2 458
5/19/2010 7 32 00 11 043 1 655
5/19/2010 7 32 10 11 063 1 457
5/19/2010 7 32 20 11 07 1 457
5/19/2010 7 32 30 11 065 1 556
5/19/2010 7 32 40 11 092 1 556
5/19/2010 7 32 50 11 117 1 457
5/19/2010 7 33 00 11 132 1 457
5/19/2010 7 33 10 11 179 1 454
5/19/2010 7 33 20 11 204 1 457
5/19/2010 7 33 30 11 204 1 556
5/19/2010 7 33 40 11 209 1 553
5/19/2010 7 33 50 11 174 1 556
5/19/2010 7 34 00 11 11 1 558
5/19/2010 7 34 10 11 084 1 454
5/19/2010 7 34 20 11 08 1 454
5/19/2010 7 34 30 11 097 1 556
5/19/2010 7 34 40 11 152 1 553
5/19/2010 7 34 50 11 228 1 556
5/19/2010 7 35 00 11 285 1 595
5/19/2010 7 3510 11 332 1 556
5/19/2010 7 35 20 11 372 1 553
5/19/2010 7 35 30 11 369 1 556
5/19/2010 7 35 40 11 334 1 556
5/19/2010 7 35 50 11 295 1 556
5/19/2010 7 36 00 11 238 1 553
5/19/2010 7 36 10 11 204 1 454
6/19/2010 7 36 20 11 211 1 454
5/19/2010 7 36 30 11 179 1 553
5/19/2010 7 36 40 11 142 1 553
5/19/2010 7 36 50 11 132 1 457
5/19/2010 7 37 00 11 152 1 457
5/19/2010 7 37 10 11 174 1 556
5/19/2010 7 37 20 11 171 1 454
5/19/2010 7 37 30 11 188 1 454
5/19/2010 7 37 40 11 255 1 556
5/19(2010 7 37 50 11 295 1 661
5/19/2010 7 36 00 11 305 1 556
5/19/2010 7 38 10 11 293 1 556
5/19/2010 7 38 20 11 297 1 556
5/19/2010 7 38 30 11 303 1 553
5/19/2010 7 38 40 11 349 1 556
5/19/2010 7 38 60 11 361 1 556
5/19/2010 7 39 00 11 344 1 553
5/19/2010 7 3910 11 319 1 553
Page 3 of 24
14
2010 MPF RATA
URS TCEMS Raw Data
12 hour time 02(/) CO (ppm)
5/19/2010 7 39 20 11 334 1 663
5/19/2010 7 39 30 11 335 1 553
5/19/2010 7 39 40 11 332 1 454
5/19/2010 7 39 50 11 324 1 454
5/19/2010 7 40 00 11283 1 454
5/19/2010 7 4010 11 277 1 454
5/19/2010 7 40 20 11263 1 451
5/19/2010 7 40 30 11 262 1 454
5/19/2010 7 4040 11 293 1 454
5/19/2010 7 40 50 11 292 1 563
5/19/2010 7 41 00 11 295 1 553
5/19/2010 7 41 10 11 305 1 553
5/19/2010 7 41 20 11 334 1 553
5/19/2010 7 41 30 11 359 1 454
5/19/2010 7 41 40 11 409 1 352
5/19/2010 7 41 50 11 443 1454
5/19/2010 7 42 00 11 463 1 454
5/19/2010 7 42 10 11 496 1 653
5/19/2010 7 42 20 11542 1 553
5/19/2010 7 42 30 11 575 1 454
5/19/2010 7 42 40 11 58 1 454
5/19/2010 7 42 50 11 556 1 553
5/19/2010 7 43 00 11 557 1 454
5/19/2010 7 43 10 11 542 1 561
5/19/2010 7 43 20 11 528 1 561
5/19/2010 7 43 30 11 528 1 561
5/19/2010 7 43 40 11 495 1 561
5/19/2010 7 43 50 11 443 1 561
5/19/2010 7 44 00 11 392 1 561
5/19/2010 7 44 10 11 345 1 466
5/19/2010 7 44 20 11 334 1 462
5/19/2010 7 44 30 11 317 1 462
5(19/2010 7 44 40 11 3 1 462
5/19/2010 7 44 50 11 277 1 462
5/19/2010 7 45 00 11293 1 462
5/19/2010 7 45 10 11 31 1 561
5/19/2010 7 45 20 11 308 1 462
5/19/2010 7 45 30 11 295 1 462
5/19/2010 7 45 40 11 305 1 462
5/19/2010 7 45 50 11 325 1 462
5/19/2010 7 46 00 11 307 1 462
5/19/2010 7 46 10 11 317 1 561
5/19/2010 7 46 20 11 337 1 561
5/19/2010 7 46 30 11 361 1 592
5/19/2010 7 46 40 11 411 1 561
5/19/2010 7 46 50 11 399 1 561
5/19/2010 7 47 00 11 387 1 561
5/19/2010 7 47 10 11 362 1 561
5/19/2010747 20 11 308 1 561
5/18/2010 7 47 30 11 243 1 565
5/19/2010 7 47 40 11 189 1 565
5/19/2010 7 47 50 11 179 1 561
5/19/2010 7 46 00 11 176 1 661
5/19/2010 7 4810 It 157 1 561
5/19/2010 7 46 20 11 087 1 561
5/19/2010 7 46 30 11 042 1 565
5/19/2010 7 48 40 11062 1 565
5/19/2010 7 48 50 11 068 1 592
5/19/2010749 00 11 063 1 664
5/19/2010 7 49 10 11 07 1 561
5/19/2010 7 49 20 11 048 1 565
S/19O010 7 49 30 11 058 1 565
6/19/2010 7 49 40 11 095 1 565
6/19/2010 7 49 50 11 164 1 561
5/19/2010 7 50 00 11 211 1 561
5/19/2010 7 50 10 11 265 1 561
5/19/2010 7 50 20 11 324 1 66
5/19/2010 7 50 30 11 401 1 565
5(19/2010 7 50 40 11 449 1 565
5/19/2010 7 50 50 11 475 1 565
5/19/2010 7 51 00 11 517 1 664
5/19/2010 7 51 10 11 547 1 583
5/19/2010 7 51 20 It 542 1 565
5/19/2010 7 51 30 11 533 1 565
5/19/2010 7 51 40 11 53 1 565
5/19/2010 7 51 50 11 55 1 565
5/19/2010 7 52 00 11 592 1 664
5/10/2010 7 52 10 11 627 1 565
5/19/2010 7 52 20 11 654 1 565
5/19/2010 7 52 30 11 681 1 565
5/19/2010 7 52 40 11 71 1 565
5/19/2010 7 52 50 11 76 1 565
5/19/2010 7 53 00 11 773 1 664
5/19/2010 7 53 10 11 787 1 664
5/19/2010 7 53 20 11 795 1 565
5/19/2010763 30 11 605 1 664
5/19/2010 7 53 40 11 822 1 66
5/19/2010 7 63 50 11 81 1 66
5/19/2010 7 54 00 It 794 1 66
5/19/2010 7 64 10 11 765 1 561
5/19/2010 7 54 20 11 794 1 561
5/19/2010 7 54 30 11 799 1 565
Page 4 of 24
15
2010 MPF RATA
URS TCEMS Raw Data
Calibration Bias
47 1 ppm CO
12 hour tlm« 02 (y) CO (ppm)
5/19/2010 7 54 40 11 79 1 561
5/19/2010 7 54 50 11758 1565
5/19/2010 7 55 00 11 713 1 561
5/19/2010 7 55 10 11 69 1 66
5/19/2010 7 55 20 11 673 1 66
5/10/2010 7 55 30 11676 1 565
5/19/2010 7 5540 11 718 1 561
5/19/2010 7 55 60 11 745 1 561
5/19/2010 7 56 00 11 784 1 675
5/19/2010 7 56 10 11 782 1 561
5/19/2010 7 56 20 11 776 1565
5/19/2010 7 56 30 11 792 1 565
5/19/2010 7 66 40 11 805 1 561
5/19/2010 7 56 50 11 772 1 561
1142 1 55
5/19/2010 7 57 00 11 683 1 561
5/19/2010 7 5710 11 661 1 66
5/19/2010 7 57 20 11 632 1 66
5/19/2010 7 57 30 11 627 1 565
5/19/2010 7 57 40 1 499 1 561
5/19/2010 7 57 50 0 252 306
5/10/2010 7 58 00 021 10 567
5/19/2010 7 58 10 0 193 24 847
5/19/2010 7 56 20 0182 37 643
5/19/2010 7 58 30 0 185 44 432
5/19/2010 7 58 40 0 185 46 431
5/19/2010 7 58 50 0 162 46 635
5/19/2010 7 59 00 0 172 46 73
5/19/2010 7 59 10 0 166 46 833
5/19/2010 7 59 20 0 166 46 734
5/19/2010 7 59 30 2 723 46 734
1 02 46 77
5/19/2010 7 59 40 10713 46 035
5/19/2010 7 59 50 10 887 36141
5/19/2010 6 00 00 10917 23 352
5/19/2010 8 00 10 10 917 11 057
5/19/2010 8 00 20 10 921 4 262
5/19/2010 8 00 30 10 927 1 565
5/19/2010 8 00 40 10 927 0 764
5/19/2010 8 00 60 10 948 0 665
)2 10 93 1 00
5/19/2010 8 01 00 6 795 0 664
5/19/2010 8 01 10 1 795 0 665
5/19/2010 8 01 20 1 607 0 764
5/19/2010 6 01 30 1 626 0 663
5/19/2010 8 01 40 0 939 0 863
6/19/2010 8 01 50 0 198 0 863
6/19/2010 8 02 00 0 185 0 863
5/19/2010 8 02 10 0175 0 863
5/19/2010 8 02 20 0177 0 863
5/19/2010 8 02 30 0 175 0 863
OK oas
5/19/2010 8 02 40 0 17 0 863
5/19/2010 8 02 50 2 563 0 87
6/19/2010 6 03 00 11 109 0 863
5/19/2010 6 03 10 11 597 0 962
5/19/2010 8 03 20 11 651 1 061
5/19/2010 8 03 30 11 688 1 362
5/19/2010 8 03 40 11 715 1 561
5/19/2010 8 03 50 11 683 1 66
5/19/2010 8 04 00 11 698 1 66
5/19/2010 8 04 10 11 718 1 664
5/19/2010 8 04 20 11 718 1 66
5/19/2010 8 04 30 11 726 1 66
5/19/2010 8 04 40 11 708 1 655
5/19/2010 8 04 50 11 681 1 66
5/19/2010 6 05 00 11 673 1 561
5/19/2010 8 05 10 11 663 1 561
5/19/2010 8 05 20 11 679 1 561
5/19/2010 8 06 30 11 69 1 565
5/19/2010 8 05 40 11 723 1 654
5/19/2010 8 05 50 11 708 1 66
5/19/2010 8 06 00 11 695 1 565
5/19/2010 8 0610 11 664 1 565
5/19/2010806 20 11 644 1 565
6/19/2010 8 06 30 11 654 1 664
5/19/2010 8 06 40 11 681 1 664
5/19/2010 8 06 50 11 678 1 664
5/19/2010 8 07 00 11 676 1 664
5/19/2010 8 07 10 11 691 1 664
5/19/2010 6 07 20 11 72 1 565
5/19/2010 6 07 30 11 755 1 565
5/19/2010 8 07 40 11 789 1 565
5/19/2010 6 07 50 11 822 1 565
5/19/2010 8 08 00 11 822 1 664
6/19/201080610 11 814 1 565
5/19/2010 8 06 20 11 832 1 565
6/19/2010 8 08 30 11 807 1 664
6/19/2010 8 08 40 11 752 1 664
5/19/2010 8 08 50 11 607 1 565
Page 5 of 24
16
2010 MPF RATA
URS TCEMS Raw Data
12 hourtinw 02(/) CO (ppm)
5/19/2010 8 09 00 11 569 1 565
5/19/2010 8 09 10 11 627 1 565
5/19/2010 609 20 11 666 1 665
5/19/2010 8 09 30 11663 1664
5/19/2010 8 09 40 11673 1 568
S/1ft/2010 8 0950 11646 1 466
5/19/2010 8 10 00 11 661 1 565
5/19/2010 8 10 10 11 671 1 664
5/19/2010 8 10 20 11 658 1 664
5/19/2010 8 10 30 11 653 1 664
5/19/2010 810 40 11 632 1 664
5/19/2010 8 10 50 11 572 1 763
5/19/2010 8 11 00 11 486 1 766
5/19/2010 8 11 10 11 423 1 766
5/19/2010 811 20 11 382 1 766
5/19/2010 8 11 30 11 366 1 766
5/10/2010 6 11 40 11 364 1 766
5/19/2010 8 11 50 11 389 1 664
5/19/2010 8 12 00 11 414 1 667
5/19/2010 8 12 10 11 428 1 664
5/19/2010 8 12 20 11 429 1 664
5/19/2010 8 12 30 11 456 1667
5/19/2010 812 40 11 522 1763
5/19/2010 8 12 50 11 617 1 664
5/19/2010 8 13 00 11 676 1 766
5/19/2010 8 13 10 11 721 1 766
5/19/2010 8 13 20 11 762 1 664
5/19/2010 8 13 30 11 782 1 664
5/19/2010 8 13 40 11 812 1 661
5/19/2010 8 13 50 11 847 1 664
5/19/2010 8 14 00 11 879 1 664
5/19/2010 814 10 11 899 1 565
5/19/2010 8 14 20 11 879 1 66
5/19/2010 8 14 30 11 869 1 565
5/19/2010 8 14 40 11 869 1 566
6/19/2010 8 14 60 11 906 1 664
5/19/2010 8 15 00 11 908 1 66
5/19/2010 8 15 10 11 913 1 664
5/19/2010 8 15 20 It 926 1664
5/19/2010 8 15 30 11 913 1 664
5/19/2010 8 15 40 11 901 1 66
5/19/2010 8 15 50 11 866 1 664
5/19/2010 8 16 00 11 847 1 664
5/19/2010 8 16 10 11 866 1 763
5/19/2010 8 16 20 11 906 1 664
5/19/2010 8 16 30 11 943 1 664
5/19/2010 8 16 40 11 963 1 664
5/19/2010 6 16 50 11 965 1 763
5/19/2010 8 17 00 11 938 1 763
5/19/2010 6 17 10 11 921 1 763
5/19/2010 8 17 20 11 888 1 763
5/19/2010 8 17 30 11 654 1 763
5/19/2010 8 17 40 11 831 1 763
5/19/2010 8 17 50 11 804 1 664
5/19/2010 8 18 00 11 765 1 664
5/19/2010 8 18 10 11 723 1 763
5/19/2010 8 18 20 11 731 1 763
5/19/2010 8 18 30 11 698 1 763
5/19/2010 8 16 40 11 703 1 763
5/19/2010 8 18 50 11 706 1 763
5/19/2010 8 19 00 11 728 1 763
5/19/2010 8 19 10 11 747 1 763
5/19/2010 8 19 20 11 802 1 783
5/19/2010 8 19 30 11 844 1 756
5/19/2010 8 19 40 11 847 1 756
5/19/2010 8 19 50 11 836 1 756
5/19/2010 8 20 00 11 856 1652
5/19/2010 6 20 10 11 901 1 756
5/19/2010 8 20 20 11 893 1 756
5/19/2010 8 20 30 11 871 1 756
5/19/2010 8 20 40 11 862 1 756
5/19/2010 8 20 50 11 837 1 756
5/19/2010 6 21 00 11 847 1 756
5/19/2010 8 21 10 11 847 1 756
5/19/2010 8 21 20 11 866 1 756
5/19/2010 8 21 30 11 864 1 652
5/19/2010 8 21 40 11 881 1 652
5/19/2010 8 21 50 11 909 1 756
5/19/2010 8 22 00 11 953 1 756
5/19/2010 8 22 10 11 953 1 756
5/19/2010 8 22 20 11 933 1 751
5/19/2010 8 22 30 11 924 1 756
5/19/2010 8 22 40 11 906 1 766
5/19/2010 8 22 50 11 886 1 751
5/19/2010 8 23 00 11 663 1 756
5/19/2010 8 23 10 11 859 1 756
5/19/2010 8 23 20 11 874 1 756
5/19/2010 8 23 30 11 886 1 756
5/19/2010 6 23 40 11 866 1 756
5/19/2010 8 23 50 11 854 1 751
5/19/2010 8 24 00 11 836 1 774
5/19/2010 8 24 10 11 844 1 751
Page 6 of 24
17 2010 MPF RATA
URS TCEMS Raw Data
Caiibrataon Bias
47 1 ppm CO
12 hour time 02(%) CO (ppm)
5/19/2010 8 24 20 11 893 1 751
5/19/2010 8 24 30 11 923 1 756
5/19/2010 8 24 40 11 931 1 756
5/19/2010 8 24 50 11 872 1 751
11 76 16«
5/19/2010 8 25 00 11 82 1 751
5/19/2010 8 25 10 11 832 1 751
5/19/2010 6 25 20 11 656 1 751
5/19/2010 8 25 30 0 772 1 751
5/19/2010 8 25 40 0 255 3 849
5/19/2010 8 25 50 0 22 12 349
5/19/2010 8 26 00 0 208 26 934
5/19/2010 8 26 10 0185 39 031
5/19/2010 8 26 20 0 182 44 825
5/19/2010 8 26 30 0182 46 42
5/19/2010 8 26 40 0 163 46 718
5/19/2010 8 26 50 0166 46 821
5/19/2010 8 27 00 0173 47 019
5/19/2010 8 27 10 0151 47 016
5/19/2010 8 27 20 0 474 47 019
0 27 47 02
5/19/2010 8 27 30 10 436 46 92
5/19/2010 8 27 40 10 862 41 225
5/19/2010 8 27 50 10 904 27 635
5/19/2010 8 28 00 10 904 13 944
5/19/2010 8 2810 10911 5 647
5/19/2010 8 28 20 10912 2 05
5/19/2010 6 28 30 10 921 0 954
)2 10 91 2 88
5/19/2010 6 26 40 2 181 0 756
5/19/2010 8 26 50 0 306 0 653
6/19/2010 8 29 00 0 222 0 752
5/19/2010 8 29 10 0 208 0 851
5/19/2010 8 29 20 0 187 0 954
6/19/2010 8 29 30 0 168 0 95
019 0 92
5/19/2010 8 29 40 4 433 0 95
5/19/2010 8 29 50 11 631 0 848
5/19/2010 8 30 00 11 904 1 049
5/19/2010 8 30 10 11 689 1 247
5/19/2010 8 30 20 11 894 1 649
5/19/2010 6 30 30 11 904 1 748
5/19/2010 8 30 40 11 928 1 748
5/19/2010 8 30 50 11 933 1 748
5/19/2010 8 31 00 11 977 1 847
5/19/2010 8 31 10 11 968 1 946
5/19/2010 8 31 20 11 982 1 847
5/19/2010 8 31 30 11 982 1 748
5/19/2010 8 31 40 11 963 1 847
5/19/2010 8 31 50 11 945 1 647
6/19/2010 8 32 00 11 898 1 647
5/19/2010 8 32 10 11 844 1 748
5/19/2010 8 32 20 11 8 1 748
5/19/2010 8 32 30 11 766 1 748
5/19/2010 8 32 40 11 76 1 748
5/19/2010 8 32 50 11 799 1 748
5/19/2010 8 33 00 11 802 1 847
5/19/2010 8 33 10 11 817 1 748
5/19/2010 8 33 20 11 832 1 748
5/19/2010 8 33 30 11 834 1 748
5/19/2010 8 33 40 11 852 1 748
5/19/2010 8 33 50 11 891 1 85
5/19/2010 8 34 00 11 899 1 85
5/19/2010 6 34 10 11 911 1 85
5/19/2010 6 34 20 11 918 1 751
5/19/2010 8 34 30 11 924 1 751
5/19/2010 8 34 40 11 94 1 751
5/19/2010 8 34 50 11 973 1 85
5/19/2010 8 35 00 11 998 1 85
5/19/2010 8 35 10 12 015 1 85
5/19/2010 8 35 20 12 02 1 85
5/19/2010 8 35 30 12 007 1 751
5/19/2010 8 35 40 11 982 1 751
5/19/2010 8 35 50 11 945 1 751
5/19/2010 8 36 00 11 893 1 748
5/19/2010 8 36 10 11 857 1 85
5/19/2010 8 36 20 11 854 1 751
5/19/2010 8 36 30 11 832 1 751
5/19/2010 8 36 40 11 822 1 751
5/19/2010 8 36 50 11 849 1 85
5/19/2010 8 37 00 11 889 1 85
5/19/2010 8 37 10 11 924 1 751
5/19/2010 8 37 20 11 926 1 756
5/19/2010 8 37 30 11 901 1 751
5/19/2010 8 37 40 11 846 1 85
5/19/2010 8 37 50 11 787 1 74S
5/19/2010 8 38 00 11 77 1 746
5/19/2010 6 3810 11 787 1 751
5/19/2010 8 36 20 11 641 1 85
5/19/2010 8 38 30 11 919 1 85
Page 7 of 24
18
2010 MPF RATA
URS TCEMS Raw Data
Calibration Bias
12 hour time 02(%) CO (ppm)
5/19/2010 8 38 40 11 985 1 85
5/19/2010 8 38 50 12 1 86
5/19/2010 8 39 00 11 992 1 751
5/19/2010 8 3910 11 967 1 847
5/19/2010 8 39 20 11 966 185
5/19/2010839 30 11 953 1 86
5/19/2010 8 39 40 11 941 1 682
5/19/2010 8 39 50 11 995 1 85
5/19/2010840 00 12 022 1 751
5/19/20108 40 10 12 02 1 751
5/19/2010 8 40 20 11 995 1 751
5/19/2010840 30 11 948 1 761
5/19/2010840 40 11 924 1 751
5/19/2010840 50 11 906 1 751
5/19/2010841 00 11906 1 751
5/19/2010 8 41 10 It 903 1 85
5/19/2010841 20 11 877 1 751
5/19/2010 841 30 11 856 1 748
5/19/2010 8 41 40 11 852 1 751
5/19/2010 8 41 50 11 836 1 748
5/19/2010 8 42 00 11 827 1 85
5/19/2010 8 42 10 11 837 1 85
5/19/2010842 20 11 644 1 647
5/19/2010 8 42 30 11 879 1 751
5/19/2010842 40 11 918 1 649
5/19/2010 8 42 50 11 931 1 751
5/19/2010843 00 11 933 1 85
5/19/2010 8 43 10 11 926 1 751
5/19/2010 8 43 20 11 945 1 751
5/19/2010843 30 11 966 1 751
5/19/2010843 40 11 973 1 751
5/19/2010 8 43 50 11 911 1 751
5/19/2010 8 44 00 11 898 1 751
5/19/2010 8 44 10 11 946 1 85
5/19/2010 6 44 20 11 977 1 855
5/19/2010 6 44 30 11 955 1 65
5/19/2010844 40 11 941 1 748
5/19/2010 8 44 50 11 953 1 751
5/19/2010 8 45 00 11 95 1 751
5/19/2010845 10 11 894 1 751
5/19/2010 6 45 20 11 869 1 85
5/19/2010 6 45 30 11 884 1 85
5/19/2010 8 45 40 11 906 1 751
5/19/2010 8 45 50 11 884 1 751
5/19/2010 8 46 00 11 671 1 751
5/19/2010 8 46 10 11 901 1 748
5/19/2010 6 46 20 11 906 1 751
5/19/2010 8 46 30 11 891 1 751
5/19/2010 8 46 40 11 869 1 751
5/19/2010 6 46 50 11 669 1 85
5/19/2010 6 47 00 11 868 1 85
5/19/2010 8 47 10 11 916 1 751
5/19/2010 8 47 20 11 958 1 751
5/19/2010847 30 12 01 1 751
5/19/2010 8 47 40 12 035 1 85
5/19/2010847 60 12 018 1 85
5/19/2010 8 48 00 11 995 1 85
5/19/2010 8 48 10 11 95 1 751
5/19/2010 8 48 20 11 924 1 649
5/19/2010 8 48 30 11 898 1 751
5/19/2010 8 48 40 11 899 1 751
5/19/2010 8 48 50 11 04 1 748
5/19/2010 8 49 00 11 995 1 756
5/19/2010 8 49 10 12 008 1 751
5/19/2010849 20 11 956 1 751
5/19/2010 8 49 30 11 943 1 751
5/19/2010 8 49 40 11 956 1 85
5/19/2010 8 49 50 11 941 1 751
5/19/2010 8 50 00 11 898 1 748
5/19/2010 8 50 10 11 881 1 751
5/19/2010 6 50 20 11 894 1 751
5/19/2010 8 50 30 11 889 1 751
5/19/2010 6 50 40 11 901 1 751
5/19/2010 6 50 50 11 852 1 751
11 91 1 77
5/19/2010 8 51 00 11 831 1 748
5/19/2010 8 51 10 11 856 1 751
5/19/2010 8 51 20 11 901 1 761
5/19/2010 8 51 30 9 912 1 751
5/19/2010 8 51 40 0 542 4 148
5/19/2010 8 51 50 0 245 13 177
5/19/2010 8 52 00 0 239 27 536
5/19/2010 8 52 10 0 195 39 226
5/19/2010 8 52 20 0 195 44 926
5/19/2010 8 52 30 0185 46 321
5/19/2010 8 52 40 0 178 46 623
5/19/2010 8 52 50 0 178 46 722
5/19/2010 8 53 00 0 18 46 619
5/19/2010 8 5310 0 166 46 92
5/19/2010 8 53 20 017 46 818
5/19/2010 8 53 30 2 369 46 425
Page 8 of 24
19
2010 MPF RATA
URS TCEMS Raw Data
12 hourtinw 02(A) CO (ppm)
471 ppm CO 0 90 46 72
5/10/2010 8 53 40 10 597 40 728
5/19/2010 8 53 50 10 875 26 034
5/19/2010 8 54 00 10 896 13 643
5/19/2010 8 54 10 10 909 5 548
5/19/2010 8 54 20 10 927 2 05
5/19/2010 8 54 30 10 926 0 851
5/19/2010 8 54 40 10 938 0 549
11 OS 02/ 9 64% C02 10 »J 11S
5/19/2010 8 54 50 1 474 0 653
5/19/2010 8 55 00 0 301 0 752
5/19/2010 8 55 10 0 245 0 752
5/19/2010 8 5520 0 208 0 752
5/19/2010 6 55 30 0 202 0 851
5/19/2010 8 55 40 0195 0 851
Z«roN2 0 20 0 82
5/19/2010 8 55 50 7 092 0 992
5/19/2010 8 5600 11 683 0 95
5/19/2010 8 56 10 11 825 1 252
5/19/2010 8 56 20 11 8 1 553
5/19/2010 8 56 30 11 849 1 652
5/19/2010 8 56 40 11 864 1 751
5/19/2010 8 56 50 11 881 1 761
Start Run 4
5/19/2010 8 57 00 11 862 1 751
5/19/2010 8 57 10 11 851 1 751
5/19/2010 8 57 20 11 859 1 847
5/19/2010 8 67 30 11 906 1 751
5/19/2010 8 57 40 11 941 1 751
5/19/2010 8 57 50 11 921 1 85
5/19/2010 6 58 00 11877 1 751
5/19/2010 8.^8 10 11 881 1 786
5/19/2010 8 58 20 11 933 1 751
5/19/2010 8 58 30 11 945 1 751
5/19/2010 8 58 40 11 919 1 748
5/19/2010 8 58 50 11 898 1 748
5/19/2010 8 59 00 11 901 1 748
5/19/2010 8 59 10 11 923 1 85
5/19/2010 6 59 20 11 909 1 847
5/19/2010 8 59 30 11 889 1 748
5/19/2010 8 59 40 11 869 1 748
5/19/2010 8 59 50 11 943 1 748
5/19/2010 9 00 00 11 978 1 85
5/19/2010 9 0010 11 943 1 85
5/19/2010 9 00 20 11 908 1 748
5/19/2010 9 00 30 11 919 1 771
5/19/2010 9 00 40 11 953 1 751
5/19/2010 9 0050 11 936 1 85
5/19/2010 9 01 00 11 904 1 65
5/19/2010 9 01 10 11 904 1 751
5/19/2010 9 01 20 11 923 1 751
5/19/2010 9 01 30 11 951 1 85
5/19/2010 9 01 40 11 982 1 748
5/19/2010 9 01 50 11 977 1 748
5/19/2010 9 02 00 11 965 1 85
5/19/2010 9 02 10 11 965 1 751
5/19/2010 9 02 20 11 96 1 748
5/19/2010 9 02 30 11 948 1 748
5/19/2010 9 02 40 11 941 1 751
5/19/2010 9 02 50 11 901 1 751
5/19/2010 9 03 00 11 898 1 751
5/19/2010 9 03 10 11 918 1 85
5/19/2010 9 03 20 11 958 1 65
5/19/2010 9 03 30 11 985 1 85
5/19/2010 9 03 40 12 018 1 751
5/19/2010 9 03 50 12 047 1 751
5/19/2010 9 04 00 12 062 1 85
5/19/2010 9 04 10 12 03 1 751
5/19/2010 9 04 20 11 963 1 751
5/19/2010 9 04 30 11 911 1 751
5/19/2010 9 04 40 11 899 1 847
5/19/2010 9 04 50 11 699 1 85
5/19/2010 9 05 00 11 911 1 756
5/19/2010 9 0510 11 913 1 855
5/19/2010 9 0520 11 931 1 858
5/19/2010 9 05 30 11 946 1 756
5/19/2010 9 05 40 11 978 1 756
5/19/2010 9 05 60 11 975 1 756
5/19/2010 9 06 00 11 919 1 756
5/19/2010 9 06 10 11 891 1 855
5/19/2010 9 06 20 11 913 1 855
5/19/2010 9 06 30 11 941 1 756
6/19/2010 9 06 40 11 936 1 756
5/19/2010 9 06 50 11 901 1 756
5/19/2010 9 07 00 11 935 1 855
5/19/2010 9 07 10 12 133 1 855
5/19/2010 9 07 20 12 284 1 855
5/19/2010 9 07 30 12 279 1 855
5/19/2010 9 07 40 12218 1 85
5/19/2010 9 07 50 12 139 1 751
5/19/2010 9 08 00 12 052 1 751
5/19/2010 9 08 10 12 027 1 751
Page 9 of 24
20
2010 MPF RATA
URS TCEMS Raw Data
Calibration Bias
47 1 ppm CO
12hourtim* 02(%) CO (ppm)
5/19/2010 9 08 20 12 144 1 652
5/19/2010 9 08 30 12 285 1 652
5/19/2010 9 08 40 12 408 1 652
5/19/2010 9 08 50 12 514 1 652
5/10/20109 09 00 12 549 1756
5/19/2010 9 09 10 12 586 1 652
5/19/2010 9 0920 12603 1652
5/19/2010 9 09 30 12 579 1 751
5/19/2010 9 09 40 12 525 1 652
5/19(2010 9 09 50 12 478 1652
5/19/2010 9 10 00 12 473 1 652
5/19/2010 9 10 10 12 515 1 652
5/19/2010 910 20 12 53 1 652
5/19/2010 9 10 30 12 504 1 652
5/19/2010 9 10 40 12 465 1 652
5/19/2010 910 50 12 43 1652
5/19/2010911 00 12 351 1652
5/19/2010 9 11 10 12 277 1 652
5/19/2010 9 11 20 12 215 1751
5/19/20109 11 30 12 17 1 652
5/19/2010 9 11 40 12 099 1 652
5/19/2010 9 11 50 12 017 1 652
5/19/2010 9 12 00 11 931 1 652
5/19/2010 9 12 10 11 852 1 664
5/19/2010 9 12 20 11 822 1 751
5/19/2010 9 12 30 11 775 1 751
5/19/2010 912 40 11 76 1 748
5/19/2010 9 12 50 11 738 1 649
5/19/2010 9 13 00 11 715 1 645
5/19/2010 913 10 11 718 1 645
5/19/2010 9 13 20 11 728 1 645
5/19/2010 9 13 30 11 715 1 649
5/19/2010 9 13 40 11 674 1 645
5/18/2010 9 13 50 11 684 1645
5/19/2010 9 14 00 11 693 1 645
5/19/2010 9 14 10 11 7 1 645
5/19/2010 9 14 20 11 668 1 744
5/19/2010 9 14 30 11 663 1 746
5/19/2010 9 14 40 11 716 1 748
5/19/2010 9 14 50 11 76 1 645
5/19/2010 9 15 00 11 773 1 645
5/19/2010 9 15 10 11 756 1 645
5/19/2010 9 15 20 11 797 1 645
6/19/2010 9 15 30 11 804 1 549
5/19/2010 9 15 40 11 614 1 645
5/19/2010 9 15 50 11 844 1 649
5/19/2010 9 16 00 11 898 1 649
5/19/2010 9 16 10 11 919 1 649
S(19/2010 9 16 20 11 918 1 549
5/19/2010 9 16 30 11 921 1 55
5/19/2010 9 16 40 11 933 1 655
5/19/2010 9 16 50 11 96 1 649
5/19/2010 9 17 00 11 962 1 748
5/19/2010 9 17 10 11 965 1 649
5/19/2010 9 17 20 11 89 1 649
5/19/2010 9 17 30 11 985 1 649
5/19/2010 9 17 40 11 98 1 748
5/19/2010 9 17 50 11 978 1 649
11 99 1 73
5/19/2010 9 18 00 12 1 649
5/19/2010 9 18 10 12 015 1 649
6/19/2010 9 18 20 11 926 1 649
6/19/2010 9 18 30 0 885 2 545
5/19/2010 9 18 40 0 266 9 042
5/19/2010 9 18 50 0 234 22 738
5/19/2010 9 19 00 0 198 36 231
5/19/2010 9 19 to 0 195 44 124
5/19/2010 9 19 20 0 182 46 722
5/19/2010 9 19 30 0 172 47 019
5/19/2010 9 19 40 0 178 47 118
5/19/2010 9 19 50 0165 47 019
5/19/2010 9 20 00 0 168 46 917
5/19/2010 9 2010 0 168 47 118
5/19/2010 9 20 20 0 257 47 123
0 20 47 05
5/19/2010 9 20 30 10 263 43 922
5/19/2010 9 20 40 10 672 32 428
5/19/2010 9 20 50 10 909 17 64
5/19/2010 9 21 00 10 912 7 646
5/19/2010 9 21 10 10 927 2 949
5/19/2010921 20 10 948 1 148
5/19/2010 9 21 30 10 927 0 749
>2 10 93 1 62
5/19/2010 9 21 40 10 043 0 646
5/19/2010 9 21 50 0 561 0 646
5/19/2010 9 22 00 0 252 0 749
5(19/2010 922 10 0 212 0 752
5/19/2010 9 22 20 0198 0 848
5/19/2010 9 22 30 0182 0 851
5/19/2010 9 22 40 0 185 0 648
019 0 85
Page 10 of 24
21
2010 MPF RATA
URS TCEMS Raw Data
12 hourtinw 02(%) CO (ppm)
5(19/2010 8 22 60 9 857 0 85
5/19/2010 9 23 00 11 914 1 048
5/19/2010! )23 10 11 97 1 247
5/19/2010! 9 23 20 11 982 1451
5/19/2010 923 30 11 998 1 65
5/19/2010 9 23 40 12 012 1 652
5/19/2010 8 23 50 12 01 1 648
5/19/2010 9 24 00 12 1 55
5/19/2010 9 24 10 12 029 1 649
5/10/2010 9 24 20 12 027 1645
5/19/20101 )24 30 12 069 1649
5/19/2010! 9 24 40 12 089 1 649
5/19/20101 9 24 50 12 084 1 546
5/19/2010 9 25 00 12 089 1645
5/19/2010! 9 25 10 12 076 1 748
5/19/2010! 9 25 20 12 066 1 649
6/19/20101 9 25 30 12 086 1 645
5/19/2010! 125 40 12 089 1 649
5/18/2010! 9 25 50 12 092 1 649
5/19/2010! 9 26 00 12 124 1 55
5/19/2010! 9 26 10 12 136 1 55
5/19/2010! 9 26 20 12 106 1645
6/19/2010! 9 26 30 12 101 1 645
5/19/2010 9 26 40 12 096 1 649
5/19/2010 8 26 50 12 094 1 645
5/19/2010! 9 27 00 12 082 1 649
5/19/2010! 9 27 10 12 069 1 645
5/19/2010! 9 27 20 12 05 1 746
5/19/2010! J 27 30 12 037 1 649
5/19/2010! 9 27 40 12 057 1 55
5/19/2010! 127 50 12 104 1 645
5/19/2010! 9 28 00 12 131 1 649
5/19/2010! 9 28 10 12 153 1 649
5/19/2010! 9 26 20 12 158 1 649
5/19/20101 9 28 30 12 17 1 691
5/19/20101 9 28 40 12 165 1 649
5/19/2010! 9 28 50 12 138 1 546
5/19/2010 9 29 00 12 092 1 648
5/19/2010! 9 29 10 12 077 1 649
5/19/2010! 9 29 20 12 092 1 649
5/19/2010! 9 29 30 12 097 1 649
5/19/2010! 9 29 40 12 112 1 649
5/19/2010! 9 29 50 12 116 1 649
5/19/2010! 9 30 00 12 089 1 649
5/19/2010! 9 30 10 12 089 1 649
5/19/2010 1 9 30 20 12 094 1 748
5/19/2010! 9 30 30 12 087 1 652
5/19/2010! 9 30 40 12 089 1 55
5/19/2010! 9 30 50 12 065 1 649
5/19/2010 ! 9 31 00 12 082 1 649
6/19/2010! 9 31 10 12 086 1637
5/19/2010! 9 31 20 12 092 1 637
5/19/2010 9 31 30 12 101 1 637
5/19/2010! 9 31 40 12 119 1 637
6/19/2010 9 31 50 12 128 1 541
5/19/2010! 9 32 00 12 121 1 637
5/19(2010! 9 32 10 12 126 1 538
5/19/2010! 9 32 20 12 124 1 64
5/19/2010! 9 32 30 12 128 1 64
5/19/2010! 9 32 40 12 124 1 637
5/19/2010! 9 32 50 12 109 1 637
5/19/20101 9 33 00 12 092 1 538
5/19/2010! 9 33 10 12 074 1 538
5/19/2010! 9 33 20 12 049 1 583
5/18/2010! 9 33 30 12 076 1 637
5/19/2010! 9 33 40 12 131 1 541
5/19/2010! 9 33 50 12 154 1 538
5/19/2010! 9 34 00 12 149 1 64
5/18/2010! 9 34 10 12 138 1 64
5/19/2010 1 9 34 20 12 156 1 541
5/19/2010! 9 34 30 12 163 1 64
5/19/2010! 9 34 40 12 195 1 64
5/19/2010! 9 34 60 12 183 1 64
5/19/2010 9 35 00 12 178 1 64
5/19/2010! 9 35 10 12159 1 541
5/19/2010! 9 35 20 12 136 1 541
5/18/2010! 9 35 30 12 114 1 541
6/19/2010! 9 35 40 12 123 1 64
5/19/2010! 9 35 50 12131 1 541
5/19/2010! 9 36 00 12 123 1 538
5/18/2010! 9 36 10 12 123 1 638
5/19/2010! 9 36 20 12 104 1 538
5/19/2010! 9 36 30 12 099 1 541
6/19/2010 9 36 40 12 114 1 541
5/18/2010 ( 9 36 50 12 163 1 538
5/19/2010 9 37 00 12 196 1 541
5/19/2010 9 37 10 12212 1 541
5/19/2010! 9 37 20 12 218 1 541
5/19/2010 9 37 30 12 195 1 541
5/19/2010 9 37 40 12 183 1 541
5/19/2010! 9 37 50 12 17 1 541
Page 11 0124
22
2010 MPF RATA
URS TCEMS Raw Data
Calibration Bias
47 1 ppm CO
12 hour time 02 (y) CO (ppm)
5/18/2010 9 38 00 12 166 1 568
5/19/2010 9 38 10 12 148 1 439
5/19/2010 9 3820 12 149 1 541
5/19/2010938 30 12 154 1 536
5/19/2010 9 38 40 12 153 1 541
5/19/2010 9 38 50 12 134 1 541
5/18/2010 9 3900 12 116 1541
5/19/2010 8 3910 12 111 1 541
5/18/2010 8 39 20 12 123 1 541
5/19/2010 0 39 30 12 144 1 541
5/19/2010 9 39 40 12171 1 541
5/19/2010 9 39 50 12 2 1 536
5/19/2010 9 40 00 12 2 1 64
6/19/2010 940 10 12188 1 536
5/19/2010940 20 12178 1 541
5/18/2010 9 40 30 12 149 1 541
5/19/2010 9 40 40 12 173 1 439
5/19/2010 9 40 50 12 165 1 541
5/19/2010 0 41 00 12 141 1 541
5/19/2010 9 41 10 12 141 1 541
5/19/2010 9 41 20 12 163 1 541
5/19/2010 9 41 30 12 159 1 538
5/19/2010 9 41 40 12 086 1 538
5/19/2010 9 41 50 12 05 1 538
5/19/2010 9 42 00 12 047 1 538
5/19/2010 9 42 10 12 077 1 538
5/19/2010 9 42 20 12 131 1 538
5/19/2010 9 42 30 12 168 1 637
5/19/2010 9 42 40 12 2 1 638
5/19/2010 9 42 50 12 227 1 538
5/19/2010 9 43 00 12 245 1 536
5/19/2010 8 43 10 12 235 1 541
5/19/2010 9 43 20 12 21 1 538
5/19(2010943 30 12 198 1 538
5/19/2010 9 43 40 12 205 1 538
5/19/2010 9 43 50 12 193 1 536
5/19/2010 9 44 00 12 18 1 637
5/19/2010 9 44 10 12 168 1 637
5/19/2010 9 44 20 12 165 1 637
5/19/2010 9 44 30 12 131 1 637
5/19/2010 9 44 40 12 106 1 538
5/19/2010 9 44 50 12 097 1 538
1213 1 59
5/19/2010 9 45 00 12 099 1 538
5/19/2010 945 10 12 089 1 538
5/19/2010 8 45 20 11 043 1 637
5/19/2010 9 45 30 0 613 2 74
5/19/2010 9 45 40 0 277 9 534
5/19/2010 945 50 0 249 23 427
5/19/2010 9 46 00 0 202 36 819
5/19/2010846 10 0 185 44 315
5/19/2010 9 46 20 0 188 46 611
5/19/2010 9 46 30 0 187 47 007
5/19/2010 9 46 40 0 187 47 007
5/19/2010 9 46 50 0 182 46 809
5/18/2010 9 47 00 0161 46 809
5/19/2010 9 47 10 0 158 47 012
5/19(2010 8 47 20 0 957 47 108
0 43 46 98
5(19/2010 9 47 30 10 506 43 712
5/19/2010 9 47 40 10 891 32 119
5/19/2010 9 47 50 10 912 17 531
5/18/2010 9 46 00 10 919 7 634
5/19/2010 9 48 10 10 916 2 834
5/19/2010 9 48 20 10 914 1 236
02 10 92 3 93
5/19/2010 943 30 d292 0 836
5/19/2010 8 48 40 0 438 0 737
5/19/2010 9 48 50 0 255 0 737
5/19/2010 9 49 00 0219 0 67
5/19/2010 9 49 10 0193 0 935
0 22 0 85
5/19/2010 9 48 20 0187 0 935
5/19/2010 9 49 30 0 18 0 935
5/19/2010 9 49 40 5 57 0 939
5/19/2010 9 49 50 11 881 1 038
5/19/2010 9 60 00 12 102 1 137
5/19/2010 9 5010 12 091 1 336
5/19/2010 9 50 20 12 107 1 439
5/19/2010 9 50 30 12 106 1 538
5/18/2010 9 50 40 12 153 1 637
5/19/2010 9 50 50 12 195 1 736
5/19/2010 9 51 00 12 195 1 634
5/19/2010 9 51 10 12 203 1 637
5/19/2010 9 51 20 12 198 1 538
5/19/2010 9 51 30 12 144 1 538
5/19/2010 8 61 40 12 118 1 637
5/19/2010 9 51 50 12 067 1 637
5/19/2010 9 52 00 12 032 1 637
5/19/2010 9 52 10 12 06 1637
Page 12 of 24
23 2010 MPF RATA
URS TCEMS Raw Data
12 hour time 02(A) CO (ppm)
5/19/2010 9 52 20 12 066 1637
5/19/2010 9 52 30 12 034 1637
5/19/2010 9 52 40 11 993 1637
5/19/2010 9 52 50 11 968 1 637
5/19/2010 9 53 00 12 02 1 637
5/19/2010 9 53 10 12 078 1637
6/19/2010 9 53 20 12 086 1 634
5/19/2010 9 53 30 12116 1637
5/19/2010 9 53 40 12 186 1 675
5/18/2010 9 53 50 12 235 1637
5/18/2010 9 54 00 12 268 1 637
6/19/2010 9 54 10 12 282 1 637
5/19/2010 9 54 20 12 278 1 534
5/19/2010 9 54 30 12 25 1 536
5/18/2010 9 54 40 12 168 1 S34
5/19/2010 9 54 50 12 116 1 736
5/19/2010 9 55 00 12 078 1637
5/^9/2010 9 55 10 12 088 1 538
5/19/2010 9 55 20 12 077 1 634
5/19/2010 9 55 30 12 072 1 634
5/19/2010 8 55 40 12 065 1 637
5/19/2010 9 55 50 12 042 1 736
5/19/2010 9 56 00 12 045 1 637
5/19/2010 9 56 10 12 067 1 637
5/18/2010 9 56 20 12 082 1 634
5/18/2010 9 58 30 12 108 1 634
5/19/2010 8 56 40 12 119 1 634
5/19/2010 9 56 50 12 134 1 634
5/19/2010 9 57 00 12 165 1 634
5/19/2010 9 57 10 12 165 1 634
5(19/2010 9 57 20 12 178 1 634
5/18/2010 9 57 30 12 208 1 634
5/19/2010 8 57 40 12 222 1 534
6/19/2010 9 57 50 12 22 1 63
5/19/2010 9 58 00 12 233 1 634
5(19/2010 9 58 10 12 205 1 63
5(19/2010 9 58 20 12 191 1 63
5/19/2010 9 56 30 12 185 1 63
5/19/2010 9 56 40 12 138 1 728
5/19/2010 9 58 50 12 101 1 733
6/19/2010 9 59 00 12 086 1 729
5(19/2010 9 59 10 12 089 1 63
5(19/2010 9 59 20 12 111 1 63
5/19/2010 9 59 30 12 121 1 63
5/19/2010 9 59 40 12 082 1 63
5/19/2010 9 59 60 12 064 1 625
5/19/2010 10 00 00 12 081 1 63
5/19/2010 10 00 10 12 084 1 63
5/19/2010 10 00 20 12 092 1 63
5/19/2010 10 00 30 12 096 1 63
5/19/201010 00 40 12 104 1 529
5/19/201010 00 50 12 114 1 63
5/19/201010 01 00 12 165 1 733
5/19/201010 01 10 12 19 1 63
5/19/2010 10 01 20 12 205 1 63
5/19/2010 10 01 30 12 186 1 529
5/18/2010 10 01 40 12 206 1 529
5/19/2010 10 01 50 12 237 1 63
5/19/2010 10 02 00 12 26 1 63
5/19/2010 10 02 10 12 255 1 63
5/19/2010 10 02 20 12 191 1 63
5/19/2010 10 02 30 12 173 1 63
6/19/2010 10 02 40 12 116 1 729
5/19/201010 02 50 12 072 1 728
5/19/2010 10 03 00 12 091 1 63
5/19/2010 10 03 10 12 092 1 63
5/19/201010 03 20 12 055 1 63
6/19/201010 03 30 12 065 1 63
5/19/201010 03 40 12 097 1 63
5/19/201010 03 50 12 128 1 63
5/19/2010 10 04 00 12 112 1 63
5/19/201010 04 10 12 094 1 63
5/19/2010 10 04 20 12 081 1 63
5/19/2010 10 04 30 12 069 1 625
5/19/2010 10 04 40 12 06 1 625
5/19/2010 10 04 50 12 06 1 63
5/19/2010 10 05 00 12 061 1 63
5/19/2010 10 05 10 12 134 1634
5/19/2010 10 05 20 12 186 1 728
6/19/2010 10 05 30 12 21 1 625
5/19/2010 10 05 40 12218 1 625
5/18/2010 10 05 50 12 235 1 625
5/18/2010 10 06 00 12 237 1 63
5/18/2010 10 06 10 12 235 1625
5/18/201010 06 20 12 238 1 63
5/19/2010 10 06 30 12 16 1 724
5/19/201010 06 40 12 094 1 729
5/19/2010 10 06 50 12 079 1 625
5/19/2010 10 07 00 12 072 1 625
5/19/2010 10 07 10 12 084 1 625
5/19/2010 10 07 20 12 086 1 526
5/19/20101007 30 12 091 1 529
Page 13 of 24
24 2010 MPF RATA
URS TCEMS Raw Data
Calibration Bias
47 1 ppm CO
12 hour time 02 (V) CO (ppm)
5/18/2010 10 07 40 12 116 1 625
5/18/201010 07 50 12 146 1 625
5/19/201010 06 00 12 129 1 625
5/19/201010 08 10 12 126 1 63
5/19/201010 08 20 12 107 1 625
5/18/2010 10 08 30 12 102 1 63
5/18/2010 10 08 40 12 081 1 63
5/1912010 10 08 50 12 109 163
5/19/201010 09 00 12 156 163
5/19/20101008 10 12 161 1 63
5/19/201010 09 20 12 17 1 63
5/19/201010 09 30 12 195 1 629
5/19/20101009 40 12 213 1 529
5/19/201010 09 50 12 195 1 566
5/19/20101010 00 12 161 1 529
5/18/2010 10 10 10 12 131 1 529
5/19/2010 10 10 20 12 139 1 63
5/19/201010 10 30 12 136 1 63
5/19/201010 10 40 12 139 1 63
5/19/2010 10 10 50 12 144 1 63
6/18/2010 1011 00 12 121 1 733
5/18/2010 10 11 10 12 134 1 63
5/19/201010 11 20 12104 1 529
5/19/201010 11 30 12 047 1 63
5/18/2010 101140 12 037 1 63
5/18/2010 10 11 50 12 114 1 63
1213 1 63
5/19/20101012 00 12 154 1 63
5/19/2010 10 12 (0 (2 203 1 534
5/19/201010 12 20 12 2 1 63
5/19/201010 12 30 12 195 1 63
5/19/201010 12 40 12 195 1 63
5/19/2010 10 12 50 12 21 1 63
5/19/201010 13 00 12 23 1 634
5/19/201010 13 10 12 233 1 634
5/19/20101013 20 12 212 1 634
5/19/2010 10 13 30 2 025 1 634
5/19/201010 13 40 0 264 5 033
5/19/20101013 50 0 237 15 631
5/19/2010 1014 00 0217 30 417
5/19/2010 10 14 10 0 207 41 312
5/19/2010 10 14 20 0 188 46 81
5/19/201010 14 30 0 19 4671
5/19/201010 14 40 0 187 46 805
5/19/2010 10 14 50 0 178 46 805
5/18/2010 10 15 00 0 175 46 805
5/19(2010 10 15 10 0 163 46 905
5/19/201010 15 20 0 175 47 108
5/19/20(0 10 15 30 0 175 47 207
017 47 07
5/19/2010 10 15 40 9 048 46 703
5/19/2010 10 15 50 10 84 38 81
5/18/2010 10 16 00 10 909 26 316
5/18/201010 16 10 10912 12 322
5/19/201010 16 20 10 832 4 925
5/19/201010 16 30 10 941 1 828
5/19/201010 16 40 10 936 0 927
:o2 10 94 2 66
5/19/2010 10 16 50 1 353 0 725
5/18/2010 10 17 00 0 304 0 725
5/18/2010 10 17 10 0 229 0 824
5/18/2010 10 17 20 0215 0 828
5/19/20101017 30 0 185 0 927
5/19/20101017 40 0 18 0 827
019 0 89
5/19/2010 10 17 50 5 051 0 923
5/19/2010 10 18 00 11 721 0 927
5/18/201010 18 10 11 951 1 026
6/19/201010 18 20 12 01 1 226
5/(9/201010 18 30 12 057 1 427
5/19/2010 1018 40 12 072 1 526
5/19/2010 10 18 50 12 035 1 526
5/19/2010 10 18 00 12 069 1 526
5/18/2010 10 18 10 12 114 1 526
5/19/201010 19 20 12 116 1 625
5/19/2010 10 19 30 12 118 1 625
5/19/2010 10 19 40 12 112 1 625
5/19/2010 10 19 50 12 107 1 526
5/19/2010 10 20 00 12 086 1 526
5/19/201010 20 10 12 089 1 625
5/19/2010 10 20 20 12 089 1 528
5/19/2010 10 20 30 12 096 1 526
6/19/2010 10 20 40 12 099 1 526
5/19/2010 10 20 50 12 116 1 526
5/19/2010 10 21 00 12 146 1 526
5/19/201010 21 10 12 175 1 625
5/19/2010 10 21 20 12 163 1 526
5/19/2010 10 21 30 12 124 1 556
5/18/2010 10 21 40 12 131 1 625
5(19/20(010 2(50 12 138 1625
Page 14 of 24
25
2010 MPF RATA
URS TCEMS Raw Data
12 hour time 02(A) CO (ppm)
5/18/2010 10 22 00 12 154 1 526
5/18/2010 10 22 10 12144 1 526
5/19/2010 10 22 20 12116 1 529
5/19/2010 1022 30 12 124 1 529
5/19/2010 10 22 40 12133 1 529
5/19/201010 22 50 12 133 1 529
5/18/201010 23 00 12106 1 427
5/19/20101023 10 12 072 1 529
5/19/2010 10 23 20 12 106 1 529
5/19/2010 10 23 30 12 138 1 528
5/19/2010 10 23 40 12 146 1 526
5/19/201010 23 50 12 153 1 528
5/19/201010 24 00 12 158 1 529
5/19/2010 10 24 10 12 165 1 526
5/19/2010 10 24 20 12 18 1 529
5/19/2010 10 24 30 12186 1 529
5/18/201010 24 40 12 17 1 529
5/18/2010 10 24 50 12 134 1 529
5/19/2010 10 26 00 12 087 1 526
5/19/2010 10 25 10 12 097 1 526
5/19/2010 10 25 20 12 104 1 529
5/19/201010 25 30 12 133 1 529
5/19/2010 10 25 40 12 156 1 526
5/19/2010 10 25 50 12 178 1 528
5/19/2010 10 26 00 12165 1 568
5/18/2010 10 2610 12158 1 529
5/19/2010 10 26 20 12 138 1 526
5/19/2010 10 26 30 12 131 1 529
5/19/201010 26 40 12 133 1 528
5/19/2010 10 25 50 12 133 1 523
5/19/2010 10 27 00 12 136 1 523
5/18/2010 10 27 10 12 153 1 523
5/19/2010 10 27 20 12 173 1 523
5/19/201010 27 30 12 166 1 523
5/19/2010 10 27 40 12 154 1 519
5/19/2010 10 27 60 12 141 1 519
5/18/2010 10 28 00 12 121 1 519
5/19/2010 10 28 10 12 118 1 42
5/19/201010 28 20 12 121 1 55
5/19/2010 10 28 30 12 136 1 519
5/19/2010 10 28 40 12 153 1 519
5/19/2010 10 28 50 12 165 1 519
5/19/2010 10 29 00 12 17 1 519
5/19/201010 29 10 12 148 1 519
5/19/2010 10 29 20 12 146 1 415
5/19/2010 10 29 30 12 134 1 42
5/19/2010 102940 12 118 1 519
5/19/2010 1029 50 12 091 1 519
5/19/2010 10 30 00 12 107 1 519
5/19/2010 10 30 10 12 136 1 519
5/19/2010 10 30 20 12 18 1 519
5/19/2010 10 30 30 12 173 1 519
5/19/2010 10 30 40 12 143 1 568
5/19/2010 10 30 50 12 164 1 519
5/19/2010 10 31 00 12 146 1 519
5/19/2010 10 31 10 12 139 1 518
5/19/2010 10 31 20 12 099 1 514
5/19/201010 31 30 12 072 1 518
6/19/201010 31 40 12 099 1 519
5/19/201010 31 50 12 131 1 519
5/19/2010 10 32 00 12 148 1 42
5/19/2010 10 32 10 12 144 1 415
5/19/2010 10 32 20 12 156 1 519
5/19/2010 10 32 30 12 158 1 518
5/19/2010 10 32 40 12 168 1 519
5/19/2010 10 32 50 12 165 1 519
5/19/201010 33 00 12 153 1 523
5/19/2010 10 33 10 12 141 1 519
5/19/2010 10 33 20 12 111 1 519
5/19/201010 33 30 12 076 1 519
5/19/2010 10 33 40 12 06 1 519
5/19/2010 10 33 50 12 062 1 519
5/19/2010 10 34 00 12 084 1 519
5/19/2010 10 34 10 12 128 1 415
5/19/2010 10 34 20 12 149 1 519
5/19/2010 10 34 30 12 138 1 519
5/19/2010 10 34 40 12 139 1 519
5/18/2010 10 34 50 12 121 1 614
5/19/2010 10 35 00 12 104 1 519
5/19/2010 10 35 10 12 118 1 519
5/19/2010 10 35 20 12 104 1 519
5/19/201010 35 30 12 128 1 518
5/19/201010 35 40 12 131 1 518
5/19/2010 10 35 60 12 123 1 519
5/19/2010 10 36 00 12 136 1 519
6/19/201010 36 10 12 133 1 519
5/19/201010 36 20 12 118 1 519
5/19/201010 36 30 12 104 1 519
5/19/2010 10 36 40 12 128 1 415
5/19/2010 10 36 50 12 099 1 514
5/19/2010 10 37 00 12 064 1 519
5/19/2010 10 37 10 12 071 1 519
Page 15 of 24
26 2010 MPF RATA
URS TCEMS Raw Data
Calibration Bias
47 1 ppm CO
12 hour time 02 (V) CO (ppm)
5/19/201010 37 20 12 074 1 519
5/19/201010 37 30 12 076 1 519
5/18/J01010 37 40 12 064 1 42
5/18/2010 10 37 60 12 081 1 446
5/19/2010 10 38 00 12 082 1 42
5/19/2010 10 3810 12 072 1 519
5/19/20101038 20 12 096 1618
5/19/2010 10 38 30 12 123 1 616
5/19/2010 10 38 40 12 143 1 514
5/19/2010 10 38 60 12 156 1 514
5/19/2010 1038 00 12 163 1 519
5/19/201010 3910 12143 1 519
5/18/2010 10 39 20 12 133 1 614
5/19/2010 10 39 30 12 131 1 619
5/19/201010 39 40 12 092 1 519
5/18/2010 10 38 50 12 091 1 519
1213 152
5/19/2010 10 40 00 12 087 1 514
5/19/201010 40 10 12 082 1 514
5/18/2010 10 40 20 0 93 1 518
5/18/2010 10 40 30 0 22 4 715
5/19/2010 10 40 40 1)192 15214
5/19/201010 40 50 0185 30 111
5/19/201010 41 00 0 175 41 012
5/19/2010 10 41 10 0186 46 906
5/19/2010 10 41 20 0185 46 802
5/19/201010 41 30 0166 47 004
5/19/201010 41 40 0 17 47 306
5/19/2010 10 41 50 0 18 47 202
5/19/2010 10 42 00 0 182 47 207
5/19/2010 10 42 10 0175 47 207
018 47 21
5/19/201010 42 20 8 747 46 905
5/19/2010 10 42 30 10 814 41 111
5/19/2010 10 42 40 10 841 27 125
5/19/2010 1042 50 10 932 13 616
5/19/201010 43 00 10 954 5 414
5/19/201010 43 10 10 946 2 015
:02 10 94 7 02
5/19/2010 1043 20 9 242 0 917
5/19/2010 10 43 30 3 087 0 717
5/19/201010 43 40 3 035 0 816
6/19/201010 43 50 3 0917
5/19/201010 44 00 1 508 1 019
5/19/2010 1044 10 1 021 1 019
5/19/2010 1044 20 021 1 019
5/19/201010 44 30 0 173 0 92
5/19/2010 10 44 40 0 17 0 923
5/19/201010 44 50 0 16 0 917
5/19/2010 10 46 00 0163 0 816
016 0 89
5/19/2010 10 45 10 1 78 0 92
5/19/201010 45 20 11 424 0 917
5/19/201010 45 30 11 74 1 019
5/19/201010 45 40 11 691 1 217
5/19/2010 10 45 50 11 634 1 415
5/19/2010 10 46 00 11 629 1 518
5/19/2010 10 46 10 11 639 1 618
5/18/2010 10 46 20 11 686 1 717
5/18/2010 10 46 30 11 726 1 717
5/18/2010 10 46 40 11 767 1 618
5/18/2010 10 46 50 11 841 1 618
5/19/2010 10 47 00 11 876 1 618
5/19/2010 10 47 10 11 906 1 613
5/19/2010 10 47 20 11 938 1 63
5/19/2010 10 47 30 11 99 1 618
5/19/201010 47 40 12 032 1 613
5/19/201010 47 50 12 081 1 616
5/19/201010 48 00 12 109 1 618
5/19/2010 10 48 10 12 112 1 618
5/19/2010 10 48 20 12 128 1 721
5/18/2010 10 48 30 12 102 1 618
5/19/2010 10 48 40 12 144 1 717
5/19/2010 10 48 50 12 213 1 717
5/18/2010 10 48 00 12 264 1 714
5/19/2010 10 4910 12 275 1 717
5/19/2010 10 49 20 12 302 1 714
5/19/2010 10 49 30 12 306 1 714
5/19/2010 10 49 40 12 284 1 714
5/19/2010 10 49 50 12 262 1 717
5/19/201010 50 00 12 243 1 717
5/19/201010 5010 12 243 1 618
5/19/2010 10 50 20 12 262 1 717
5/19/2010 10 50 30 12 268 1 613
5/19/2010 10 50 40 12 272 1 618
5/19/2010 10 50 50 12.267 1 613
5/19/2010 10 61 00 12 27 1 717
5/19/2010 10 51 10 12 28 1 717
5/19/2010 10 51 20 12 292 1 717
5/19/2010 10 51 30 12 289 1 613
Page 16 of 24
27 2010 MPF RATA
URS TCEMS Raw Data
12 hour time 02 (r) CO (ppm)
5/19/201010 51 40 12 299 1 618
5/19/2010 10 51 50 12 295 1 618
6/19/201010 52 00 12 247 1 717
5/19/201010 52 10 12 205 1 613
5/19/2010 10 52 20 12 161 1 613
5/19/201010 52 30 12 139 1 613
5/19/201010 52 40 12134 1 618
5/19/201010 62 50 12 151 1 717
6/19/201010 63 00 12 158 1 613
5/19/201010 53 10 12 158 1613
5/19/2010 10 53 20 12 181 1 613
5/19/201010 53 30 12215 1 613
5/19/2010 10 53 40 12 242 16(3
5/19/201010 53 50 12 235 1 717
5/19/201010 54 00 12 225 1 721
5/19/2010 10 54 10 12 208 1613
5/19/201010 54 20 12 193 1 618
5/19/2010 10 54 30 12 2 1 618
5/19/2010 10 54 40 122 1 613
6/18/201010 54 50 12 201 1 616
5/19/2010 10 55 00 12 193 1 618
5/19/2010 10 55 10 12 2 1 61
5/19/201010 55 20 12 201 1 709
5/19/201010 55 30 12 175 161
5/19/2010 10 55 40 12 168 1 61
5/19/201010 55 50 12 151 1 61
5/19/201010 56 00 12 106 1 61
5/19/201010 5610 12 077 1 613
5/19/201010 56 20 12 082 1 709
5/19/2010 10 56 30 12 079 1 61
5/19/201010 56 40 12 062 1 613
5/19/2010 10 56 50 12 086 1 714
5/19/201010 57 00 12 081 1 709
5/19/2010 10 5710 12 089 1 61
5/19/2010 10 57 20 12 102 1 61
5/19/201010 57 30 12 116 1 613
5/19/2010 10 57 40 12 144 1 614
5/19/2010 10 57 50 12 159 1 613
5/19/201010 58 00 12 141 1 714
5/19/2010 to 58 10 12 109 1 709
6/19/201010 58 20 12 094 1 61
5/19/201010 58 30 12 074 1 61
5/19/2010 10 56 40 12 052 1 613
5/19/2010 10 56 50 12 024 1 61
5/19/201010 69 00 12 025 1 61
5/19/201010 59 10 12 012 1 613
5/19/201010 59 20 11 968 1 613
5/19/201010 58 30 11 966 1 613
5/19/201010 59 40 11 975 1 613
5/19/201010 59 50 12 037 1 613
5/19/2010 11 00 00 12 109 1 61
5/19/201011 00 10 12 195 1 613
5/18/201011 00 20 12 243 1 513
5/19/2010 11 00 30 12 267 1 613
5/19/2010 11 00 40 12 228 1 613
5/19/201011 00 60 12 166 1 61
5/18/201011 01 00 12 076 1 525
5/19/20101101 10 12 022 1 514
5/19/2010 11 01 20 11 975 1 511
5/19/201011 01 30 11 819 1 514
5/19/201011 01 40 11 866 1 514
5/19/201011 01 50 11 849 1 613
5/19/201011 02 00 11 699 1 613
5/19/2010 11 02 10 11 883 1 613
5/19/201011 02 20 12 071 1 613
5/19/201011 02 30 12 107 1 613
5/19/2010 11 02 40 12 136 1 613
5/18/2010 11 02 50 12 149 1 613
5/19/201011 03 00 12 131 1 514
5/18/201011 03 10 12 143 1 613
5/19/2010 11 03 20 12 173 1613
5/19/2010 11 03 30 12 185 1 613
5/18/201011 03 40 12 16 1 613
5/19/201011 03 50 12 128 1 613
5/19/2010 11 04 00 12 128 1 514
5/19/2010 11 04 10 12 123 1 514
5/19/201011 04 20 12 086 1 514
5/19/20101104 30 12 054 1 613
5/19/2010 11 04 40 12 052 1 613
5/19/2010 11 04 50 12 072 1 613
6/19/2010 11 05 00 12 06 1 613
5/19/201011 05 10 12 052 1 514
5/19/2010 11 05 20 12 076 1 514
5/18/201011 05 30 12 092 1 613
5/19/201011 05 40 12 065 1 714
5/19/201011 05 50 11 831 1 744
5/19/201011 06 00 11 857 1 714
5/19(201011 06 10 11 828 1 613
5/19/2010 11 06 20 11 988 1613
5/19/201011 06 30 11 99 1 613
6/18/201011 06 40 11 988 1 613
5/19/201011 06 50 11 885 1 613
Page 17 of 24
28
Calibration Bias
2010 MPF RATA
URS TCEMS Raw Data
12 hourtinw 02(%) CO (ppm)
5/19/201011 07 00 12 003 1 613
5/19/201011 0710 12 02 1 714
5/18/201011 07 20 12 022 1 714
5/18/201011 07 30 12 01 1 717
5/18/201011 07 40 12 1 717
5/19/201011 07 50 11 831 1 717
1212 163
5/19/201011 08 00 11 822 1 816
5/18/201011 0810 11 718 1 816
5/19/201011 08 20 11 663 1 717
5/18/201011 08 30 11 632 1 816
5/18/201011 0840 11 653 1 717
5/19/201011 08 50 11 669 1 717
6/18/201011 09 00 11 691 1 714
5/19/201011 0910 11 731 1 714
5/19/201011 0920 11 799 1 717
5/19/201011 09 30 11 841 1 717
5/19/2010 11 09 40 11 699 1 714
5/19/201011 00 50 11 956 1 613
5/19/2010 11 10 00 11 985 1 717
5/19/201011 10 10 12 008 1 714
5/19/2010 11 1020 12049 1 717
5/18/201011 10 30 12 071 1 763
5/19/2010 11 10 40 12086 1 717
5/19/2010 11 10 50 12 118 1 717
5/19/2010 11 11 00 12 134 1 717
5/19/2010 11 11 10 12143 1 717
5/19/2010 11 11 20 12 153 1 717
5/19/2010 11 11 30 12 144 1 717
5/19/2010 11 11 40 12 166 1 717
5/19/2010 11 11 50 12 148 1 717
5/19/201011 12 00 12 141 1 717
5/19/201011 12 10 12 158 1 717
5/19/2010 11 12 20 12 176 1 717
5/19/2010 11 12 30 12 195 1 717
5/19/201011 12 40 12 218 1 717
5/19/2010 11 12 50 12 183 1 717
5/19/2010 11 13 00 12 168 1 717
5/19/201011 13 10 12 158 1 717
5/19/2010 11 13 20 12 153 1 717
5/19/2010 11 13 30 12 136 1 717
5/19/2010 11 13 40 12 129 1 717
5/19/2010 11 13 50 12 129 1 717
5/19/2010 11 14 00 12 149 1 717
5/18/2010 1114 10 12 171 1717
5/19/2010 11 14 20 12 166 1 721
5/19/2010 11 14 30 12 166 1 618
5/18/2010 11 14 40 12 148 1 613
5/19/2010 11 14 50 12 102 1 717
5/19/2010 11 1500 12072 1 717
5/19/2010 11 15 10 12 042 1 717
5/19/2010 11 15 20 12044 1 717
5/19/2010 11 15 30 12 06 1 717
5/19/2010 11 15 40 12 074 1 717
5/19/2010 11 15 50 12074 1 717
5/19/2010 11 16 00 12045 1 717
5/19/201011 16 10 12008 1 717
5/19/2010 11 16 20 11 977 1 717
5/19/201011 16 30 11 95 1 618
5/19/201011 16 40 11 971 1 717
5/19/201011 16 50 11 861 1 717
5/18/201011 17 00 11 866 1 717
5/19/2010 11 17 10 11 86 1 717
5/18/201011 17 20 11 953 1 717
5/19/2010 11 1730 11 941 1 717
5/19/2010 11 17 40 11 931 1 717
5/19/2010 11 17 50 11 943 1 717
5/19/201011 18 00 11 96 1 717
5/19/201011 18 10 11 936 1 717
5/18/201011 18 20 11 93 1 717
5/18/201011 18 30 11 973 1 816
5/18/201011 1840 12024 1 717
5/18/201011 18 50 12 05 1 714
5/18/201011 18 00 12 069 1 613
5/18/2010 11 18 10 12 008 1 717
5/19/201011 19 20 11 96 1 717
5/19/2010 11 19 30 11 95 1 717
5/19/2010 11 19 40 11 88 1 717
6/19/2010 11 19 50 12 005 1 717
5/19/2010 11 20 00 11 871 1 717
5/19/2010 11 20 10 11 931 1 717
5/19/2010 11 20 20 11 818 1 714
5/18/2010 11 20 30 11 833 1 717
5/19/2010 11 20 40 11 96 1 717
6/19/2010 11 20 50 11 97 1 717
5/19/2010 11 21 00 11 978 1 717
5/19/2010 11 21 10 12 012 1 714
5/19/201011 21 20 12 05 1 613
5/19/2010 11 21 30 12 069 1 744
5/19/2010 11 21 40 12 076 1 717
5/19/2010 11 21 50 12 05 1 717
Page 16 of 24
29
2010 MPF RATA
URS TCEMS Raw Data
12 hour time 02(%) CO (ppm)
5/19/2010 11 22 00 12 007 1 717
5/19/2010 11 22 10 11 073 1 717
5/19/2010 11 22 20 11 978 1 714
5/19/201011 22 30 11 995 1 717
5/19/201011 2240 11 997 1 717
5/19/201011 22 50 12 018 1 717
W19/201011 23 00 12 044 1 717
5/18/201011 23 10 12 057 1 717
5/18/201011 23 20 12 066 1 714
5/18/201011 23 30 12 104 1 717
5/18/201011 23 40 12 094 1 714
5/18/2010 11 23 50 12 054 1 714
5/19/2010 11 24 00 12 017 1 714
5/19/2010 11 24 10 12 003 1 717
5/19/201011 24 20 1201 1 717
5/19/201011 24 30 12 034 1 714
5/19/201011 24 40 12 06 1 717
5/18/201011 24 50 12 076 1 717
5/18/2010 11 25 00 12 062 1 816
5/18/2010 11 25 10 12044 1 816
5/19/2010 11 25 20 12 025 1 714
6/19/2010 11 25 30 12 02 1 717
5/19/201011 25 40 12 039 1 717
5/19/201011 25 50 12 049 1 717
5/19/201011 26 00 12 05 1 714
5/19/201011 26 10 12 069 1 763
5/18/201011 26 20 12 065 1 714
5/19/2010 11 26 30 12 042 1 714
5/19/2010 11 26 40 12 016 1 714
5/19/201011 26 50 11 976 1 714
5/19/2010 11 27 00 11 966 1 714
5/19/2010 11 27 10 11 861 1 613
5/18/201011 27 20 11 951 1 816
5/18/2010 11 27 30 11«56 1714
5/18/2010 11 27 40 11 95 1 714
5/19/2010 11 27 50 11 961 1 714
5/19/2010 11 28 00 11 982 1 818
5/19/2010 11 28 10 11 965 1 616
5/19/201011 28 20 12008 1 816
5/19/201011 28 30 11 993 1 714
5/19/2010 11 28 40 11 983 1 714
5/19/2010 11 28 50 11 963 1 714
5/18/2010 11 29 00 11 953 1 813
5/19/2010 11 2910 11 956 1 714
5/19/2010 11 29 20 11 956 1 714
5/19/2010 11 29 30 11 973 1 813
5/19/2010 11 29 40 11 887 1 714
5/19/2010 11 29 50 11 983 1 714
5/19/2010 11 30 00 11 971 1 813
5/19/201011 3010 11 99 1 808
5/19/2010 11 30 20 12015 1 714
5/19/2010 11 30 30 12 017 1 816
5/19/201011 30 40 12 015 1 813
5/19/2010 11 30 50 1202 1 714
5/19/201011 31 00 12 042 1 714
5/19/201011 31 10 11 97 1 714
5/19/2010 11 31 20 11 901 1 714
5/19/2010 11 31 30 11 889 1 714
5/19/2010 11 31 40 11 919 1 613
5/18/2010 11 31 50 11 921 1 714
5/18/201011 32 00 11 933 1 714
5/19/2010 11 32 10 11 956 1 714
5/18/2010 11 32 20 12 1 714
5/18/2010 11 32 30 11 975 1 714
5/18/201011 32 40 11 923 1 613
5/18/2010 11 32 50 11 906 1 613
5/19/2010 11 33 00 11 936 1 714
5/19/2010 11 33 10 11 988 1 709
5/19/2010 11 33 20 12 012 1 813
5/19/201011 33 30 11 961 1 816
5/19/2010 11 33 40 11 919 1 717
5/19/2010 11 33 50 11 926 1 714
5/19(2010 11 34 00 12 01 1 61
5/19/201011 34 10 12 146 1 613
5/19/2010 11 34 20 12 322 1 714
5/19/2010 11 34 30 12498 1 813
5/19/201011 34 40 12 621 1 717
5/19/201011 34 50 12 653 1 717
5/19/201011 35 00 5 979 1 714
5/19/201011 35 10 0 336 2 114
5/19/201011 35 20 0 208 7 011
5/19/201011 35 30 0 193 19414
5/19/2010 11 35 40 0 183 33 809
5/18/2010 11 35 50 0175 43 006
5/18/2010 11 36 00 0 178 46 504
5/18/2010 11 36 10 0 16 47 207
5/18/2010 11 36 20 0161 47 202
5/18/2O10 11 36 30 0 165 47 202
5/18/201011 36 40 0 156 47202
5/19/201011 36 50 1 14 47 202
471 ppm CO 0 49 47 20
Calibration Bias
Page 19 of 24
30
2010 MPF RATA
URS TCEMS Raw Data
12 hour time 02(%) CO (ppm)
5/19/201011 37 00 10714 46688
5/19/2010 11 37 10 10931 38813
5/19/2010 11 37 20 10 841 23 921
5/19/2010 11 37 30 10841 11 525
5/18/2010 11 37 40 10 951 4 521
110% 02/9 64S C02 10 94 13 32
5/18/2010 11 37 50 9 736 1 622
5/19/201011 38 00 0 371 0 821
5/19/20101138 10 0 207 0 722
5/18/201011 38 20 0192 0 722
5/19/201011 38 30 0 185 0 722
5/19/201011 38 40 018 0 621
5/19/2010 11 38 50 018 0 92
Zero N2 011 0 82
5/19/201011 39 00 6 786 0 92
5/19/201011 3910 11 752 0 92
5/19/2010 11 38 20 11 868 1 122
5/19/2010 11 38 30 11 889 1 325
5/19/2010 11 39 40 11 841 1 618
5/18/2010 11 39 50 11 965 1 82
Start Run 9
5/19/2010 11 40 00 11 95 1 82
5/19/201011 40 10 11 843 1 885
5/19/2010 11 40 20 11 856 1 786
5/19/2010 11 4030 11 975 1 781
5/19/2010 11 40 40 11 995 1 885
5/19/2010 11 40 50 12 008 1 885
5/19/2010 11 41 00 12 01 1 886
5/19/2010 11 41 10 11 982 1 816
5/19/201011 41 20 11 868 1 721
5/19/2010 11 41 30 11 935 1 82
5/19/2010 11 41 40 11 933 1 82
5/19/2010 11 41 50 11 951 1 721
5/19/2010 11 42 00 11 963 1 721
5/19/2010 11 42 10 12 032 1 82
5/19/2010 11 42 20 12 109 1 843
5/19/2010 11 42 30 12 141 1 717
5/19/2010 11 42 40 12 109 1 62
5/19/2010 11 42 50 12 04 1 62
6/19/2010 11 4300 11 986 1 82
5/19/2010 11 43 10 11 978 1 721
5/19/2010 11 4320 12 003 1 721
5/19/2010 11 43 30 11 988 1 82
5/19/2010 11 43 40 11 935 1 805
5/19/2010 11 43 50 11 911 1 605
5/18/2010 11 44 00 11 961 1 801
5/19/201011 44 10 11 875 1 801
5/19/2010 11 44 20 11 963 1 702
5/19/2010 11 44 30 11 933 1 702
5/19/2010 11 44 40 11 966 1 714
5/19/2010 11 44 50 12 008 1 717
5/19/2010 11 45 00 12 008 1 717
5/19/2010 11 45 10 11 97 1 816
5/18/2010 11 45 20 11 938 1 717
5/19/2010 11 45 30 11 943 1 816
5/19/2010 11 45 40 11 853 1 805
5/18/2010 11 45 50 11 966 1 843
5/19/2010 11 46 00 11 861 1 832
5/19/2010 11 46 10 11 904 1 832
5/19/2010 11 46 20 11 824 1 721
5/19/201011 4630 11 742 1 702
5/19/2010 11 46 40 11 653 1 724
5/19/2010 11 4650 11 582 1 709
5/19/2010 11 47 00 11 535 1 706
5/19/2010 11 47 10 11 515 1 618
5/19/2010 11 47 20 11 491 1 637
5/19/2010 11 47 30 11 485 1 724
5/19/2010 11 47 40 11 493 1 702
5/19/2010 11 47 50 11 488 1 675
5/19/2010 11 4800 11 48 1 733
5/19/2010 11 48 10 11 475 1 667
5/19/2010 11 48 20 11 475 1 766
6/19/2010 11 4830 11 502 1 596
5/19/2010 11 48 40 11 542 1 763
5/19/2010 11 48 50 11 582 1 702
5/19/2010 11 4900 11 565 1 568
5/19/2010 11 49 10 11 53 1 702
5/19/2010 11 49 20 11 52 1 736
5/19/2010 11 49 30 11 547 1 662
5/10/2010 11 49 40 11 589 1 751
5/19/2010 11 49 50 11 643 1 744
5/19/2010 11 5000 11 663 1 744
5/19/2010 11 50 10 11 715 1 733
5/19/2010 11 50 20 11 725 1 823
6/19/2010 11 50 30 11 703 1 766
5/19/2010 11 50 40 11 671 1 744
5/19/2010 11 50 50 11 639 1 702
5/19/2010 11 51 00 11 648 1 721
5/18/2010 11 51 10 11 649 1 717
5/19/2010 11 51 20 11 668 1 808
5/18/2010 11 51 30 11 698 1 801
5/19/201011 51 40 11 743 1 721
Page 20 of 24
31
2010 MPF RATA
URS TCEMS Raw Data
Calibration Bias
47 1 ppm CO
12 hour time 02(7) CO (ppm)
5/19/2010 11 51 50 11 76 1 729
5/19/201011 52 00 11 79 1 709
5/19(2010 11 52 10 11 819 1 608
5/19/2010 11 52 20 11 834 1 828
5/19/201011 52 30 11 837 1 813
5/19/2010 11 52 40 11 842 1 832
5/18/201011 52 50 11 849 1 729
5/19/201011 53 00 11 82 1622
5/19/201011 53 10 11 806 1 714
5/19/2010 11 53 20 11 788 1 714
5/19/2010 11 53 30 11 792 1 721
5/19/201011 53 40 11 789 1 828
5/18/2010 11 53 50 11 606 1 724
5/19/2010 11 54 00 11862 1 756
5/19/2010 11 54 10 11 888 1 724
5/18/2010 11 54 20 11 883 1 729
5/18/201011 54 30 11 839 1 729
5/19/2010 11 54 40 11 785 1 607
5/19/2010 11 54 50 11 767 1 706
5/18/201011 55 00 11 752 1 771
5/19/201011 56 10 11 753 1 694
5/19/201011 55 20 11 763 1 709
5/18/2010 11 55 30 11 765 1721
5/190010 11 55 40 11 77 1 649
5/19/201011 55 50 11 773 1 691
5/19/2010 11 56 00 11 772 1 724
5/19/2010 11 56 10 11 767 1 717
5/19(201011 56 20 11 768 1 756
5/19/2010 11 56 30 11 765 1 625
5/19(2010 11 56 40 11 827 1 607
5/19/2010 11 56 50 11 839 1 766
5/19(2010 11 57 00 11 859 1 603
5/19/2010 11 57 10 11 906 1 649
5/18/2010 11 57 20 11 953 1 697
5/19/2010 11 57 30 11 96 1 728
5/19/2010 11 57 40 11 824 1 681
5/19/2010 11 57 50 11 883 1 588
5/19(2010 11 58 00 11 664 1 625
5/19/2010 11 58 10 11 876 1 744
5/19/2010 11 58 20 11 888 1 736
5/19/2010 11 58 30 11 891 1 79
5/19/2010 11 58 40 11 379 1 648
5/19/2010 11 68 50 11 872 1 744
5/19(2010 11 58 00 11 862 1 717
5/19/2010 11 59 10 11 857 1 721
5/19/2010 11 59 20 11 841 1 733
5/19/2010 11 58 30 11 82 1 729
5/19/2010 11 59 40 11 817 1 637
5/19/2010 11 59 50 11 831 1 702
5/19/2010 12 00 00 11 852 1 744
5/19/201012 00 10 11 662 I 721
5/19/201012 00 20 11 862 1 634
5/19/2010 12 00 30 11 868 1 625
5/19/2010 12 00 40 11 883 1 588
5/19/2010 12 00 50 11 888 1 664
11 82 1 74
5/19/2010 12 01 00 11 889 1 618
5/19/2010 12 01 10 11 884 1 729
5/18/201012 01 20 5 147 1 721
5/18/201012 01 30 0 324 1 813
5/19(2010 12 01 40 0215 562
5/19/2010 12 01 50 0 192 16 725
5/19/2010 12 02 00 0 177 31 061
5/19/2010 12 02 10 0 173 41 393
5/19/2010 12 02 20 0168 45 661
5/19/2010 12 02 30 0 156 46 425
5/19/2010 12 02 40 0 166 46 668
5/19/2010 12 02 50 0 161 46 467
5/19/2010 12 03 00 0 151 46 737
5/19/2010 12 03 10 0165 46 839
5/18/2010 12 03 20 7 243 46 661
2 52 46 75
5/19/2010 12 03 30 10 852 45 78
5/19/2010 12 03 40 10 919 36 887
5/19/2010 12 03 50 10 934 21 605
5/18(2010 12 04 00 10 941 99
5/19/2010 12 04 10 10 949 3 846
02 10 94 11 78
5/19/2010 12 04 20 10 397 1 42
5/18/2010 12 04 30 0 373 0 725
5/19/2010 12 04 40 0 208 0 645
5/19/2010 12 04 50 0 192 0 732
5/19/2010 12 05 00 0 135 0 737
5/19/2010 12 05 10 0 172 0 707
5/19/2010 12 05 20 0 16 0 64
5/19/2010 12 05 30 0 151 0 624
5/19/2010 12 05 40 0 151 0 786
5/19/2010 12 05 50 0 15 0 806
5(19/2010 12 06 00 0145 0 836
5/19/2010 12 06 10 0 14 0 836
5/19/2010 12 06 20 0 148 0 828
Page 21 of 24
32
2010 MPF RATA
URS TCEMS Raw Data
12 hour tfme 02(%) CO (ppm)
5/19/2010 12 06 30 0 155 0 791
5/19/2010 12 06 40 0148 0 794
5/19/2010 12 06 50 0151 0 801
5/19/201012 07 00 015 0 794
5/18/201012 07 10 014 0 71
5/10/2010 12 07 20 016 0 722
015 0 74
5/19/2010 12 07 30 1 174 0 782
5/19/201012 07 40 11 288 0 947
5/19/2010 12 07 50 1171 0 942
5/19/201012 08 00 11 745 1 229
5/19/2010 12 08 10 11 74 1424
5/18/201012 08 20 11 736 1 622
5/19/2010 12 08 30 11743 1729
5/19/2010 12 08 40 11 738 1 733
5/18/2010 12 08 50 11 728 1 721
5/19/2010 12 09 00 11 735 1 714
5/19/2010 12 09 10 11 755 1 756
5/19/2010 12 09 20 11 787 1 748
5/19/2010 12 09 30 11 795 1 717
5/19(2010 12 09 40 11 827 1 721
5/19/2010 12 09 50 11 849 1 721
5/19/2010 12 10 00 11 864 1 721
5/19/2010 12 10 10 11 662 1 721
5/19/2010 12 10 20 11 636 1 736
5/19/2010 12 10 30 11 778 1 828
5/19/2010 12 10 40 11 753 1 82
5/19/2010 12 10 50 11 768 1 62
5/18/2010 12 11 00 11 866 1 714
5/19/2010 12 11 10 12 128 1 714
5/18/2010 12 11 20 12 396 1 717
5/18/2010 12 11 30 12713 1 717
5/19/2010 12 11 40 12 98 1 816
5/19/2010 12 11 50 13 13 1 813
5/19/201012 12 00 13 202 1 82
5/19/2010 12 12 10 13 267 1 709
5/19/2010 12 12 20 13 448 1 724
5/19/2010 12 12 30 13 566 1 877
5/19/2010 12 12 40 13618 1 721
5/19/2010 12 12 50 13 647 1 724
5/19/2010 12 13 00 13 668 1 729
5/19/201012 13 10 13 687 1 724
5/19/2010 12 13 20 13 67 1 721
5/19/2010 12 13 30 13 628 1 733
5/19/2010 12 13 40 13611 1 832
5/19/2010 12 13 50 13 696 1 813
5/19/2010 12 14 00 13 583 1 729
5/19/2010 12 14 10 13 558 1 832
5/19/2010 12 14 20 13 529 1 724
5/19/2010 12 14 30 13 477 1 724
5/19/2010 12 14 40 13 386 1 813
5/19/2010 12 14 50 13 299 1 816
5/19/2010 12 15 00 13 182 1 82
5/19/2010 12 15 10 13 096 1 823
5/19/2010 12 15 20 12 974 1 82
5/19/2010 1215 30 12 836 1 816
5/19/2010 12 15 40 12 683 1 724
5/19/2010 12 15 50 12564 1 724
5/19/2010 12 16 00 12 507 1 82
5/19/2010 12 16 10 12 497 1 717
5/19/2010 1216 20 12 509 1 721
5/19/2010 12 16 30 12 515 1 714
5/18/2010 12 16 40 12 534 1 721
5/19/2010 12 16 50 12 549 1 724
5/19/2010 12 17 00 12 572 1 729
5/19/2010 1217 10 12 576 1 729
5/18/2010 12 17 20 12 582 1 706
5/19/2010 12 17 30 12 604 1 733
5/19/2010 12 17 40 12 648 1 729
5/19/2010 12 17 50 12 687 1 717
5/18/2010 12 18 00 12 713 1 733
5/19/2010 12 18 10 12 702 1 721
5/19/2010 12 18 20 12 703 1 724
5/19/201012 18 30 12 663 1 832
5/19/2010 12 18 40 12 674 1 82
5/19/2010 12 18 50 12 466 1 823
5/19/2010 12 19 00 12 433 1 736
5/19/2010 12 19 10 12 363 1 733
5/19/2010 12 18 20 12 349 1 729
5/19/2010 12 19 30 12 347 1 847
5/19/201012 1940 12 379 1 826
5/19/201012 19 50 12 393 1 721
5/19/201012 20 00 12 425 1 828
5/19/201012 20 10 12 488 1 729
5/19/201012 20 20 12 472 1 733
5/19/2010 12 20 30 12 455 1 724
5/19/2010 12 20 40 12 438 1 717
5/19/2010 12 20 50 12416 1 736
5/19/2010 12 21 00 12 408 1 733
5/19/2010 12 21 10 12 406 1 724
Page 22 of 24
33 2010 MPF RATA
URS TCEMS Raw Data
Calibration Bias
47 1 ppm CO
12 hour time 02 (V) CO (ppm)
5/19/2010 12 21 20 12 441 1 736
5/19/2010 12 21 30 12 5 1 643
6/19/2010 12 21 40 12 564 1 835
5/19/2010 12 21 50 12 593 1 729
5/19/2010 12 22 00 12 582 1 637
5/19/201012 22 10 12 537 1 733
5/19/201012 22 20 12 512 1 736
5/19/2010 12 22 30 12 544 1 729
5/19/2010 12 22 40 12 609 1 729
5/19/2010 12 22 50 12 656 163
5/19/201012 23 00 12 696 1 625
5/19/2010 12 23 10 12 695 1 724
5/19/201012 23 20 12 887 1 724
5/10/2010 12 23 30 12712 1 714
5/19/2010 12 23 40 12 782 1 733
5/19/2010 12 23 50 12 705 1 744
5/19/2010 12 24 00 12 488 1 733
5/19/2010 12 24 10 12212 1 733
5/19/2010 12 24 20 11 836 1 736
5/19/2010 12 24 30 11 233 1 733
5/19/2010 12 24 40 10 424 1 623
5/19/2010 12 24 50 9 546 1 733
5/19/2010 12 25 00 8 807 1 735
5/19/2010 12 25 10 8 269 1 736
5/19/201012 25 20 7 661 1 724
5/19/2010 12 25 30 7 674 1 733
5/19/2010 12 25 40 7 507 1 733
6/19/2010 12 25 50 7 394 1 744
5/19/201012 26 00 7 266 1 634
5/19/201012 26 10 7 003 1 649
5/19/2010 12 26 20 6 865 1 729
5/19/2010 12 26 30 6 901 1 634
5(19/2010 12 26 40 7 104 1 641
5/19/2010 12 26 50 7 408 1 541
5/19/2010 12 27 00 7612 1 626
5/19/2010 12 27 10 7 607 1 634
5/19/2010 12 27 20 7 666 1 729
5/19/2010 12 27 30 8 03 1 733
6/19/2010 12 27 40 8 663 1 739
5/19/201012 27 50 9 229 1 744
5/19/2010 12 28 00 9 523 1 733
5/18/2010 12 26 10 9615 1 724
5/19/2010 12 28 20 9 694 1 729
5/19/2010 12 28 30 9 791 1 739
5/19/2010 12 28 40 9684 1 748
5/18/2010 12 28 50 8 425 1 733
11 70 1 73
5/18/2010 12 29 00 9 277 1 63
5/19/2010 12 28 10 9 142 1 625
5/19/2010 12 29 20 7 149 1 739
5/19/2010 12 29 30 0 378 5 524
5/19/2010 12 29 40 0 193 22 414
5/18/2010 12 28 50 0 178 53 921
5/19/2010 12 30 00 0 16 81 048
5/19/2010 12 30 10 0172 95 681
5/19/2010 12 30 20 0161 99 157
5/19/2010 12 30 30 0 16 99 565
5/19/2010 12 30 40 0 16 99 55
5/19/2010 12 30 50 0 143 99 523
5/19/2010 12 31 00 0 158 99 511
5/18/2010 12 31 10 0 156 99 614
5/18/2010 12 31 20 0156 99 968
5/19/2010 12 31 30 0153 99 767
5/19/2010 12 31 40 0 143 99 691
5/19/2010 12 31 50 0 237 99 404
5/19/2010 12 32 00 0 16 90 981
5/19/201012 32 10 0 133 74 284
5/19/2010 12 32 20 014 59 22
5/19/2010 12 32 30 0153 50 502
5/18/2010 12 32 40 0161 47 642
5/19/2010 12 32 50 0143 47 264
5/19/2010 12 33 00 0153 47 076
6/19/2010 12 33 10 0 145 47 024
5/19/2010 12 33 20 0 125 47 16
5/19/2010 12 33 30 0 136 47 217
5/19/2010 12 33 40 0 136 47 21
0 13 47 20
5/19/2010 12 33 50 0 151 47 034
5/19/2010 12 34 00 9 429 45 314
5/19/2010 12 34 10 10 862 35 563
5/19/2010 12 34 20 10 009 20 384
5/19/2010 12 34 30 10 936 9 256
5/19/201012 34 40 10 948 3 591
5/19/2010 12 34 50 10 936 1 31
5/19/2010 12 35 00 10 929 0 722
5/19/2010 12 35 10 10 959 0 645
5/19/201012 35 20 10 959 0 626
02 10 95 OSS
5/19/2010 12 35 30 0 838 0 63
5/19/2010 12 35 40 0 227 0 699
5/19/2010 12 35 50 0 186 0 824
Page 23 of 24
34 2010 MPF RATA
URS TCEMS Raw Data
12 hour time 02(%) CO (ppm)
5/19/201012 36 00 0 182 0 836
5/19/201012 38 10 0 166 0 917
5/19/2010 12 36 20 0173 0 932
5/19/2010 12 36 30 0 16 0 935
5/19/201012 3640 0153 0 935
016 0 93
5/19/2010 12 36 50 8 348 0 912
5/19(201012 37 00 10 12 1 049
5/19/201012 37 10 10 258 1 336
5/19/201012 37 20 10 494 1 613
5/19/2010 12 37 30 10 778 1 729
5/10/201012 37 40 10 978 1 739
5/19/2010 12 37 50 11 099 1 808
5/19/201012 38 00 11 225 1 84
5/19/2010 12 38 10 11 411 1 813
5/19/201012 38 20 11 626 1 843
5/19/201012 38 30 11 723 1 82
5/19/201012 38 40 11 73 1 828
6/19/201012 36 50 11 721 1 823
5/19/201012 39 00 11 745 1 823
5/19/2010 12 39 10 11 768 1 84
5/19/2010 12 39 20 11 773 1 816
5/19/201012 39 30 11 69 1 828
5/19/201012 39 40 11 597 1 714
5/18/201012 39 50 11 51 1 816
5/18/201012 40 00 11 444 1 823
5/19/2010 12 40 10 2 192 1 756
5/19/2010 12 40 20 0 153 1 095
5/19/2010 12 40 30 0 138 1 247
5/19/201012 40 40 0 133 0 932
5/18/201012 40 50 0 123 0 816
5/19/2010 12 41 00 0 125 0 714
5/19/2010 12 41 10 0 133 0 725
5/19/2010 12 41 20 0126 0 767
5/19/2010 12 41 30 0118 0 752
5/19/2010 12 41 40 0 13 0 756
5/18/201012 41 50 1 135 0 717
5/19/2010 12 42 00 0 133 0 737
5/19/2010 12 42 10 0 118 0 717
5/19/2010 12 42 20 0121 0 833
5/19/2010 12 42 30 0 131 0 774
5/19/201012 42 40 0 121 0 707
5/19/201012 42 50 0 114 0 717
5/19/2010 12 43 00 0133 0 71
5/19/201012 43 10 0 118 0 756
6/19/2010 12 43 20 1 947 0 71
5/19/2010 12 43 30 11 092 0714
5/19/2010 12 43 40 11 243 1 Oil
5/19/2010 12 43 50 11 243 1 32
5/19/2010 12 44 00 11 243 1 553
5/19/2010 12 44 10 11 231 1 568
5/19/2010 12 44 20 11 265 1 717
5/19/2010 12 44 30 11 292 1 724
5/19/201012 44 40 11 325 1 721
5/19/201012 44 50 11 325 1 667
5/19/201012 45 00 11 305 1 702
5/19/201012 45 10 11 285 1 721
5/19/2010 12 45 20 11 277 1 717
5/19/2010 12 45 30 11 298 1 759
5/19/2010 12 45 40 11 33 1 706
5/19/2010 12 45 50 11 352 1 675
6/19/2010 12 46 00 11 342 1 63
5/19/2010 12 46 10 11 344 1 714
5/19/2010 12 46 20 11 324 1 739
5/19(2010 12 46 30 11 312 1 687
5/19/2010 12 46 40 11 307 1 756
5/19/2010 12 46 50 11 334 1 709
5/19/2010 12 47 00 11 371 1 739
5/19/201012 47 10 11 381 1 672
5/19/2010 12 47 20 11 402 1 607
5/19/2010 12 47 30 11 438 1 613
Page 24 of 24
Reference
APPENDIX D
Method calibration Results
Project ID MPF RATA
2010 MPF RATA
CO Calibration Data Summary
Date 19 May 10 2% Limit
Instrument Make/Model Thermo 480 Calibration Error Test Results
ID Number Ozzy Certified CEM Absolute Cal Error
Calibration Span Value 97 80 Cylinder ID Value Time Response Difference (% of Span)
Analyzer Range 0-100 zero gas ALM008609 0 00 06 55 -0 03 0 03 0 03%
Units ppm span gas CC 113980 97 80 07 01 97 54 0 26 0 26%
Technician(s) ADB/DG mid-range ALM048820 47 10 07 03 46 17 0 93 0 95%
CEMS Calibration Bias and Drift Tests 5% Limit 1 5% Limit 3% Limit
Gal Error Pre test Post test
GEMS GEMS Bias CEMS Bias Drift
Run No Cylinder Value Response Time Response (% of Span) Time Response (% of Span) (% of Span) Eq 7E 5
Run 1 0 00 0 03 07 28 0 80 0 85% 08 02 0 86 0 91% 0 06% Co= 0 832
47 10 46 17 07 24 46 64 ' 0 48% 07 59 46 77 0 61% 0 13% Cma/(Cm Co) 1 027
Run 2 0 00 0 03 08 02 0 86 0 91% 08 29 0 92 0 97% 0 06% Co= 0 891
47 10 46 17 07 59 46 77 0 61% 08 27 47 02 0 87% 0 26% Cnna/(Cni Co) 1 024
Run 3 0 00 0 03 08 29 0 92 0 97% 08 55 0 82 0 86% 0 10% Co= 0 868
47 10 46 17 08 27 47 02 0 87% 08 53 46 72 0 57% 0 30% Cma/(Cm Co) 1 024
Run 4 0 00 0 03 08 55 0 82 0 86% 09 22 0 85 0 90% 0 03% Co= 0 834
47 10 46 17 08 53 46 72 0 57% 09 20 47 05 0 90% 0 34% Cma/(Cm Co) 1 023
Run 5 0 00 0 03 09 22 0 85 0 90% 09 49 0 85 0 89% 0 00% Co= 0 848
47 10 46 17 09 20 47 05 0 90% 09 47 46 98 0 83% 0 08% Cma/(Cm Co) 1 020
Run 6 0 00 0 03 09 49 0 85 0 89% 10 17 0 89 0 94% 0 05% Co= 0 871
47 10 46 17 09 47 46 98 0 83% 10 15 47 07 0 93% 0 10% Cma/(Cm Co) 1 020
Run 7 0 00 0 03 10 17 0 89 0 94% 10 45 0 89 0 93% 0 01% Co= 0 890
47 10 46 17 10 15 47 07 0 93% 10 42 47 21 1 06% 0 13% Cma/(Cm Co) 1 018
Run 8 0 00 0 03 10 45 0 89 0 93% 11 38 0 82 0 87% 0 07% Co= 0 853
-47 10 46 17 10 42 47 21 1 06% 11 36 47 20 1 06% 0 00% Cma/(Cm Co) 1 016
^ Run9_ 0 00 0 03 11 38 0 82 0 87% 12 07 V 0 74 0 79% 0 08% Co= 0 782
-47 10 46 17 11 36 47 20 1 06% 12 03 46 75 0 59% 0 47% Cma/(Cm Co) 1 020
Run 10_ 0 00 0 03 12 07 0 74 0 79% 12 36 0 93 0 98% 0 20% Co= 0 838
47 10 46 17 12 03 46 75 0 59% 12 33 47 20 1 05% 0 46% Cma/(Cm Co) 1 021
- 201O:MPF RATA
O2 Calibration Data Summary
Date 19-May .. 2% Limit
Instrument Make/Model Servomex , Calibration Error Test Results
ID Number Hendnx-^ Gertified CEM Absolute Cal Error
Calibration Span Value 21 90 Cylinder ID Value Time Response Difference (% of Span)
Analyzer Range 0-25' zero gas A11M008609 ', 0 00 , 06 55-'013 , , 0 13 0 60%
Units % \ span gas i' CCi'78359 . - 21 90 " 06 57 ,^ » 2V88 , 0 02 0 09%
Technician(s) ADB/DC J -mid-range ALii}l009988 • 11 00 06 58 . 'ir oo ,. 0 00 0 00%
CEMS Calibration Bias and Drift Tests 5% Limit 5% Limit 3% Limit
Run No Cylinder Value
Cal Error
CEMS
Response Time
Pre-test
GEMS
Response
Bias
(% of Span)
Post-test
GEMS Bias
Time Response (%
Dnft
of Span)|(% of Span) Eq 7E-5
. Run'1
Run 2
"c,Rurr3
Run 4
Run 5
,Run6
* Run 7
Run 8'
- •^•^ ^ •'
'fPuh 9 .:
^^Run 10
0 00
11 00
0 00
11 00
0 00
11 00
0 00
11 00
0 00
11 00
0 00
11 00
0 00
11 00
0 00
11 00
0 00
11 00
0 00
11 00
0 13
11 00
0 13
11 00
0 13
11 00
0 13
11 00
0 13
11 00
0 13
11 00
0 13
11 00
0 13
11 00
0 13
11 00
0 13
11 00
' ' c ,.•>-
'07 28"
07 25
08 02
08 00
08 29
08 28
08 55
08 54
09 22
09 21
09 49
09 48
10 17
10 16
10 45
10 43
11 38
11 37
12 07
12 04
"0 17 '
icfgii
0 18
10 93
0 19
10 91
0 20
10 93
0 19
10 93
0 22
10 92
0 19
10 94
0 16
10 94
0 18
10 94
0 15
10 94
0 17%
0 30%
0 20%
-0 30%
0 26%
-0 39%
0 32%
-0 32%
0 26%
-0 30%
0 42%
-0 39%
0 28%
0 29%
0 15%
0 26%
0 23%
-0 26%
0 09%
-0 27%
,„08 02.
08 00,
•. p8 29
" 08 28'-,
.'•08 55'
' 08 54'
09 22 .
,^ 0 '9 21_ •
09 49
' 09 48'
\ 'i ' •• •
"10 17'4
;v10 16
018
10 93j
.'0 19
1091
019
10 93
: 0 i22
.;;iO 92
"0'19'-'
1,0 9/t ?
'•;^^10 45>^:-> Jo 16' . ,
.10'43'X' 10 9'4 • ;
»11 ^^\",
..-• "1.1 37 -
"V V f, ;
12 07 f ••
,12 04^?
'"'i - ^
.'1236 '
'12 35'
,' 0 18 , ,
109i.,'-.'
•0 15,
- V ^ i
• '''0-'16 ' j
' .10 95 ^
0 20%
-0 30%
0 26%
-0 39%
0 20 0 32%
10 93'-V -0 32%
0 26%
-0 30%
0 42%
-0 39%
0 28%
-0 29%
0 15%
-0 26%
0 23%
0 26%
0 09%
-0 27%
0 14%
-0 24%
0 03%
-0 01 %
0 05%
-0 09%
0 06%
0 07%
-0 06%
0 02%
0 16%
-0 08%
-0 13%
0 09%
-0 13%
0 04%
0 08%
0 00%
-0 14%
0 01%
0 05%
0 04%
Co=
Cma/(Cm Co)
Co=
Cma/(Cfn Co)
Co=
Cma/(Cm Co)
Co=
Cma/(Cm Co)
Co=
Cma/(Cfti Co)
Co=
Cma/(Cm Co)
Co=
Cma/(Cm Co)
Co=
Cma/(Ctn Co)
Co=
Cma/(Cm Co)
Co=
Cma/(Cni Co)
0 173
1 022
0 182
1 024
0 195
1 025
0195
1 024
0 205
1 026
0 208
1 026
0 179
1 022
0 173
1 021
0 166
1 021
0 156
1 020
APPENDIX E
MPF CEMS Relative Accuracy Data
2
MPF RATA Data
Run 1
0736 - 0757
14-Ait-082 14-Ait-384 14-Ait-384o
02 CO Raw CO Corr
65855 API-164 API-164
5/18/10 7 36 00 12 0 1 2
5/18/10 7 36 30 12 0 1 2
5/18/10 7 37 00 120 1 2
5/18/10 7 37 30 120 1 2
5/18/10 7 38 00 120 1 0
5/18/10 7 38 30 12 1 1 2
5/18/10 7 39 00 12 1 1 2
5/18/10 7 39 30 12 1 1 2
5/18/10 7 40 00 12 1 1 2
5/18/10 7 40 30 12 1 1 2
5/18/10 7 41 00 12 1 1 2
5/18/10 7 41 30 12 1 1 2
5/18/10 7 42 00 120 1 2
5/18/10 7 42 30 120 1 2
5/18/10 7 43 00 12 0 1 2
5/18/10 7 43 30 12 0 1 2
5/18/10 7 44 00 12 1 1 2
5/18/10 7 44 30 12 1 1 2
5/18/10 7 45 00 12 1 1 2
5/18/10 7 45 30 12 1 1 2
5/18/10 7 46 00 12 1 1 2
5/18/10 7 46 30 12 1 1 2
5/18/10 7 47 00 12 0 1 2
5/18/10 7 47 30 12 0 1 2
5/18/10 7 48 00 12 0 1 2
5/18/10 7 48 30 11 8 1 2
5/18/10 7 49 00 11 8 1 2
5/18/10 7 49 30 11 7 1 2
5/18/10 7 50 00 11 6 1 1
5/18/10 7 50 30 11 7 1 2
5/18/10 7 51 00 11 9 1 2
5/18/10 7 51 30 12 0 1 2
5/18/10 7 52 00 12 1 1 2
5/18/10 7 52 30 12 1 1 2
5/18/10 7 53 00 12 1 1 2
5/18/10 7 53 30 12 2 1 2
5/18/10 7 54 00 122 1 2
5/18/10 7 54 30 12 3 1 0
5/18/10 7 55 00 12 3 1 2
5/18/10 7 55 30 12 3 1 2
5/18/10 7 56 00 122 1 2
5/18/10 7 56 30 122 1 2
5/18/10 7 57 00 122 1 2
5/18/10 7 57 30 12 1 1 2
Average 12 0 1 2
TOCDF PDARS Data
5/19/10
MPF RATA Data
Run 2
08 04 - 08 25
14-Ait-082 14-Ait-384 14-Ait-3
O2 CO Raw coc
65855 API-164 API-1
5/19/10 8 04 00 11 8 1 2
5/19/10 8 04 30 11 8 1 2
5/19/10 8 05 00 11 8 1 2
5/19/10 8 05 30 11 7 1 2
5/19/10 8 06 00 11 8 1 2
5/19/10 8 06 30 11 7 1 2
5/19/10 8 07 00 11 7 1 2
5/19/10 8 07 30 11 7 1 2
5/19/10 8 08 00 11 8 1 2
5/19/10 8 08 30 11 9 1 2
5/19/10 8 09 00 11 8 0 0
5/19/10 8 09 30 11 7 1 1
5/19/10 8 10 00 11 7 0 0
5/19/10 8 10 30 11 7 0 0
5/19/10 8 11 00 11 7 1 2
5/19/10 8 11 30 11 5 1 1
5/19/10 8 12 00 11 4 1 1
5/19/10 8 12 30 11 5 0 1
5/19/10 8 13 00 11 5 0 0
5/19/10 8 13 30 11 8 0 0
5/19/10 8 14 00 11 8 1 2
5/19/10 8 14 30 11 9 1 2
5/19/10 8 15 00 11 9 0
5/19/10 8 15 30 12 0 1 2
5/19/10 8 16 00 11 9 2
5/19/10 8 16 30 11 9 1 2
5/19/10 8 17 00 120 1 2
5/19/10 8 17 30 12 0 0
5/19/10 8 18 00 11 9 1 2
5/19/10 8 18 30 11 8 1 2
5/19/10 8 19 00 11 7 1 2
5/19/10 8 19 30 11 8 1 2
5/19/10 8 20 00 11 9 1 2
5/19/10 8 20 30 11 9 1 2
5/19/10 8 21 00 11 9 1 2
5/19/10 8 21 30 11 9 1 2
5/19/10 8 22 00 11 9 1 2
5/19/10 8 22 30 120 1 2
5/19/10 8 23 00 120 1 2
5/19/10 8 23 30 11 9 1 2
5/19/10 8 24 00 11 9 1 2
5/19/10 8 24 30 11 9 1 2
5/19/10 8 25 00 120 1 2
5/19/10 8 25 30 11 9 2
Average 11 8 1 2
TOCDF PDARS Data
5/19/10
MPF RATA Data
Run 3
08 30 - 08 51
14-Ait-082
O2
65855
5/19/10 8 30 00 12 0
5/19/10 8 30 30 12 0
5/19/10 8 31 00 120
5/19/10 8 31 30 120
5/19/10 8 32 00 120
5/19/10 8 32 30 11 9
5/19/10 8 33 00 11 8
5/19/10 8 33 30 11 8
5/19/10 8 34 00 11 9
5/19/10 8 34 30 11 9
5/19/10 8 35 00 120
5/19/10 8 35 30 12 1
5/19/10 8 36 00 12 0
5/19/10 8 36 30 11 9
5/19/10 8 37 00 11 8
5/19/10 8 37 30 11 9
5/19/10 8 38 00 11 9
5/19/10 8 38 30 11 8
5/19/10 8 39 00 120
5/19/10 8 39 30 120
5/19/10 8 40 00 120
5/19/10 8 40 30 12 1
5/19/10 8 41 00 120
5/19/10 8 41 30 11 9
5/19/10 8 42 00 11 9
5/19/10 8 42 30 11 9
5/19/10 8 43 00 11 9
5/19/10 8 43 30 120
5/19/10 8 44 00 120
5/19/10 8 44 30 12 0
5/19/10 8 45 00 120
5/19/10 8 45 30 11 9
5/19/10 8 46 00 11 9
5/19/10 8 46 30 11 9
5/19/10 8 47 00 11 9
5/19/10 8 47 30 11 9
5/19/10 8 48 00 12 1
5/19/10 8 48 30 120
5/19/10 8 49 00 11 9
5/19/10 8 49 30 120
5/19/10 8 50 00 120
5/19/10 8 50 30 11 9
5/19/10 8 51 00 11 9
5/19/10 8 51 30 11 9
Average 11 9
14-Ait-384
CO Raw
API-164
14-Ait-384o
CO Corr
API-164
2
2
0
2
2
2
0
2
0
0
2
2
2
2
0
0
0
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
0
0
0
2
2
2
2
2
2
2
TOCDF PDARS Data
5/19/10
MPF RATA Data
Run 4
08 57-09 18
14-Ait-082
02
65855
14-Ait-384
CO Raw
API-164
14-Ait-384o
CO Corr
API-164
5/19/10 8 57 00 12 0 1 2
5/19/10 8 57 30 11 9 1 2
5/19/10 8 58 00 120 1 2
5/19/10 8 58 30 11 9 1 2
5/19/10 8 59 00 120 1 2
5/19/10 8 59 30 120 1 2
5/19/10 9 00 00 11 9 1 2
5/19/10 9 00 30 120 1 2
5/19/10 9 01 00 120 1 2
5/19/10 9 01 30 11 9 1 2
5/19/10 9 02 00 120 1 2
5/19/10 9 02 30 120 1 2
5/19/10 9 03 00 120 1 2
5/19/10 9 03 30 11 9 1 2
5/19/10 9 04 00 120 1 2
5/19/10 9 04 30 12 1 0 0
5/19/10 9 05 00 11 9 0 Q
5/19/10 9 05 30 11 9 1 2
5/19/10 9 06 00 120 0 0
5/19/10 9 06 30 11 9 0 0
5/19/10 9 07 00 120 0 0
5/19/10 9 07 30 12 0 0 0
5/19/10 9 08 00 12 3 0 0
5/19/10 9 08 30 12 1 0 2
5/19/10 9 09 00 124 0 0
5/19/10 9 09 30 126 0 0
5/19/10 9 10 00 126 0 0
5/19/10 9 10 30 125 0 0
5/19/10 9 11 00 12 5 0 0
5/19/10 9 11 30 124 1 2
5/19/10 9 12 00 122 0 0
5/19/10 9 12 30 11 9 0 0
5/19/10 9 13 00 11 8 0 0
5/19/10 9 13 30 11 7 0 0
5/19/10 9 14 00 11 7 0 0
5/19/10 9 14 30 11 7 0 0
5/19/10 9 15 00 11 7 0 0
5/19/10 9 15 30 11 8 1 2
5/19/10 9 16 00 11 8 0 0
5/19/10 9 16 30 11 9 0 0
5/19/10 9 17 00 12 0 1 2
5/19/10 9 17 30 12 0 1 2
5/19/10 9 18 00 12 0 0 0
5/19/10 9 18 30 12 0 1 2
Average 12 0 0 1
TOCDF PDARS Data
5/19/10
6
MPF RATA Data
Run 5
09 24 - 09 45
14-Ait-082 14-Ait-384 14-Ait-384o
O2 CO Raw CO Corr
65855 API-164 API-164
5/19/10 9 24 00 12 1 0 0
5/19/10 9 24 30 12 1 0 0
5/19/10 9 25 00 12 1 0 0
5/19/10 9 25 30 12 1 0 0
5/19/10 9 26 00 12 2 0 0
5/19/10 9 26 30 12 2 0 0
5/19/10 9 27 00 12 2 0 0
5/19/10 9 27 30 12 1 0 0
5/19/10 9 28 00 12 1 0 0
5/19/10 9 28 30 12 2 0 0
5/19/10 9 29 00 12 2 0 0
5/19/10 9 29 30 12 1 0 0
5/19/10 9 30 00 12 1 0 0
5/19/10 9 30 30 12 1 0 0
5/19/10 9 31 00 12 1 0 0
5/19/10 9 31 30 12 1 0 0
5/19/10 9 32 00 12 2 0 0
5/19/10 9 32 30 12 2 0 0
5/19/10 9 33 00 12 2 0 0
5/19/10 9 33 30 12 1 0 0
5/19/10 9 34 00 12 1 0 2
5/19/10 9 34 30 12 2 0 0
5/19/10 9 35 00 12 2 1 2
5/19/10 9 35 30 12 2 1 2
5/19/10 9 36 00 12 1 0 0
5/19/10 9 36 30 12 1 0 2
5/19/10 9 37 00 12 2 1 2
5/19/10 9 37 30 12 2 0 2
5/19/10 9 38 00 12 3 1 2
5/19/10 9 38 30 12 2 0 2
5/19/10 9 39 00 12 2 0 0
5/19/10 9 39 30 12 1 0 2
5/19/10 9 40 00 12 2 0 0
5/19/10 9 40 30 12 2 0 0
5/19/10 9 41 00 12 2 0 0
5/19/10 9 41 30 12 2 0 0
5/19/10 9 42 00 12 2 0 0
5/19/10 9 42 30 12 1 0 0
5/19/10 9 43 00 12 2 0 0
5/19/10 9 43 30 12 3 0 0
5/19/10 9 44 00 12 2 0 0
5/19/10 9 44 30 12 2 0 0
5/19/10 9 45 00 12 1 0 0
5/19/10 9 45 30 12 1 0 0
Average 12 2 0 0
TOCDF PDARS Data
5/19/10
7
MPF RATA Data
Run 6
09 51 -10 12
14-Ait-082 14-Ait-384 14-Ait-384o
O2 CO Raw CO Corr
65855 API-164 API-164
5/19/10 9 51 00 12 2 0 0
5/19/10 9 51 30 12 3 0 0
5/19/10 9 52 00 12 2 0 0
5/19/10 9 52 30 12 1 0 0
5/19/10 9 53 00 12 1 0 0
5/19/10 9 53 30 12 1 1 2
5/19/10 9 54 00 12 2 0 0
5/19/10 9 54 30 12 3 0 2
5/19/10 9 55 00 12 3 0 0
5/19/10 9 55 30 12 1 0 0
5/19/10 9 56 00 12 1 0 0
5/19/10 9 56 30 12 1 0 0
5/19/10 9 57 00 12 2 0 0
5/19/10 9 57 30 12 2 0 0
5/19/10 9 58 00 12 2 0 0
5/19/10 9 58 30 12 3 0 2
5/19/10 9 59 00 12 2 0 0
5/19/10 9 59 30 12 1 0 0
5/19/10 10 00 00 12 2 0 0
5/19/10 10 00 30 12 1 0 0
5/19/10 10 01 00 12 1 0 0
5/19/10 10 01 30 12 2 0 0
5/19/10 10 02 00 12 2 0 0
5/19/10 10 02 30 12 3 0 0
5/19/10 10 03 00 12 2 0 0
5/19/10 10 03 30 12 1 0 0
5/19/10 10 04 00 12 1 0 0
5/19/10 10 04 30 12 1 0 0
5/19/10 10 05 00 12 1 0 0
5/19/10 10 05 30 12 1 0 0
5/19/10 10 06 00 12 3 0 0
5/19/10 10 06 30 12 3 0 0
5/19/10 10 07 00 12 2 0 0
5/19/10 10 07 30 12 1 0 0
5/19/10 10 08 00 12 2 0 0
5/19/10 10 08 30 12 2 0 0
5/19/10 10 09 00 12 1 0 0
5/19/10 10 09 30 12 2 0 0
5/19/10 10 10 00 12 2 0 0
5/19/10 10 10 30 12 2 0 0
5/19/10 10 11 00 12 2 0 0
5/19/10 10 1130 12 1 0 0
5/19/10 10 12 00 12 1 0 0
5/19/10 10 12 30 12 2 0 0
Average 12 2 0 0
TOCDF PDARS Data
5/19/10
8
MPF RATA Data
Run 7
10 19-1040
14-Ait-082 14-Ait-384 14-Ait-;
O2 CO Raw coc
65855 API-164 API-1
5/19/10 10 19 00 12 1 0 0
5/19/10 10 19 30 12 1 0 0
5/19/10 10 20 00 122 0 0
5/19/10 10 20 30 12 1 0 0
5/19/10 10 21 00 122 0 0
5/19/10 10 21 30 122 0 0
5/19/10 10 22 00 122 0 0
5/19/10 10 22 30 122 0 0
5/19/10 10 23 00 12 1 0 0
5/19/10 10 23 30 12 1 0 0
5/19/10 10 24 00 122 0 0
5/19/10 10 24 30 12 2 0 0
5/19/10 10 25 00 12 2 0 0
5/19/10 10 25 30 12 1 0 0
5/19/10 10 26 00 12 1 0 0
5/19/10 10 26 30 12 2 0 0
5/19/10 10 27 00 122 0 0
5/19/10 10 27 30 12 1 0 0
5/19/10 10 28 00 122 0 0
5/19/10 10 28 30 12 1 0 0
5/19/10 10 29 00 122 0 0
5/19/10 10 29 30 122 1 2
5/19/10 10 30 00 12 1 0 0
5/19/10 10 30 30 12 1 0 0
5/19/10 10 31 00 122 0 0
5/19/10 10 31 30 122 0 0
5/19/10 10 32 00 12 1 0 0
5/19/10 10 32 30 122 0 0
5/19/10 10 33 00 122 0 0
5/19/10 10 33 30 122 0 0
5/19/10 10 34 00 12 1 0 0
5/19/10 10 34 30 12 1 0 0
5/19/10 10 35 00 12 1 0 0
5/19/10 10 35 30 12 1 0 0
5/19/10 10 36 00 122 0 0
5/19/10 10 36 30 122 0 0
5/19/10 10 37 00 12 1 0 0
5/19/10 10 37 30 12 1 0 0
5/19/10 10 38 00 12 1 0 0
5/19/10 10 38 30 12 1 0 0
5/19/10 10 39 00 12 1 0 0
5/19/10 10 39 30 122 0 0
5/19/10 10 40 00 122 0 0
5/19/10 10 40 30 12 1 0 0
Average 122 0 0
TOCDF PDARS Data
5/19/10
MPF RATA Data
Run 8
10 47-11 08
14-Ait-082 14-Ait-384 14-Ait-:
O2 CO Raw coc
65855 API-164 API-1
5/19/10 10 47 00 11 8 1 2
5/19/10 10 47 30 11 9 1 2
5/19/10 10 48 00 12 0 1 2
5/19/10 10 48 30 12 1 1 2
5/19/10 10 49 00 122 1 2
5/19/10 10 49 30 12 3 0 0
5/19/10 10 50 00 124 0 0
5/19/10 10 50 30 12 3 0 0
5/19/10 10 51 00 12 3 0 0
5/19/10 10 51 30 12 3 0 0
5/19/10 10 52 00 12 3 0 0
5/19/10 10 52 30 123 0 0
5/19/10 10 53 00 122 0 0
5/19/10 10 53 30 122 0 0
5/19/10 10 54 00 122 0 0
5/19/10 10 54 30 122 0 0
5/19/10 10 55 00 12 2 0 0
5/19/10 10 55 30 122 0 0
5/19/10 10 56 00 122 0 0
5/19/10 10 56 30 12 1 0 0
5/19/10 10 57 00 12 1 0 0
5/19/10 10 57 30 12 1 0 0
5/19/10 10 58 00 12 1 0 0
5/19/10 10 58 30 122 0 0
5/19/10 10 59 00 12 1 0 0
5/19/10 10 59 30 12 1 0 0
5/19/10 11 00 00 12 0 0 0
5/19/10 11 00 30 12 1 0 0
5/19/10 11 01 00 122 0 0
5/19/10 11 01 30 12 1 0 0
5/19/10 11 02 00 12 0 0 0
5/19/10 11 02 30 11 9 0 0
5/19/10 11 03 00 12 1 0 0
5/19/10 11 03 30 122 0 0
5/19/10 11 04 00 122 1 2
5/19/10 11 04 30 12 1 1 2
5/19/10 11 05 00 12 1 1 2
5/19/10 11 05 30 12 1 1 2
5/19/10 11 06 00 12 1 1 2
5/19/10 11 06 30 11 9 1 2
5/19/10 11 07 00 12 0 1 2
5/19/10 11 07 30 120 0
5/19/10 11 08 00 12 1 1 2
5/19/10 11 08 30 11 9 2
Average 12 1 0 1
TOCDF PDARS Data
5/19/10
10
MPF RATA Data
Run 9
11 40-12 01
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
5/19/10
11 40 00
11 40 30
11 41 00
11 41 30
11 42 00
11 42 30
11 43 00
11 43 30
11 44 00
11 44 30
11 45 00
11 45 30
11 46 00
11 46 30
11 47 00
11 47 30
11 48 00
11 48 30
11 49 00
11 49 30
11 50 00
11 50 30
11 51 00
11 51 30
11 52 00
11 52 30
11 53 00
11 53 30
11 54 00
11 54 30
11 55 00
11 55 30
11 56 00
11 56 30
11 57 00
11 57 30
11 58 00
11 58 30
11 59 00
11 59 30
12 00 00
12 00 30
12 01 00
12 01 30
14-Alt-082
O2
65855
120
12 0
12 0
12 0
120
120
122
12 0
12 0
120
120
12 1
12 0
12 0
11 8
11 6
11
11
11
11
11
11
11
11
11
11 8
11 9
11 9
11 8
11 9
11 9
11 8
11 8
11 8
11 8
11 9
120
11 9
11 9
11 9
11 8
11 9
11 9
11 9
14-Ait-384
CO Raw
API-164
14-Ait-384o
CO Corr
API-164
2
2
2
2
2
2
2
2
2
2
2
2
2
2
0
1
1
0
1
0
0
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
Average 11 9
TOCDF PDARS Data
5/19/10
11
MPF RATA Data
Run 10
12 08- 12 29
14-Ait-082 14-Ait-384 14-Ait-384o
O2 CO Raw CO Corr
65855 API-164 API-164
5/19/10 12 08 00 11 8 1 2
5/19/10 12 08 30 11 9 1 2
5/19/10 12 09 00 11 8 1 2
5/19/10 12 09 30 11 8 1 0
5/19/10 12 10 00 11 9 1 0
5/19/10 12 10 30 11 9 1 2
5/19/10 12 1100 118 1 2
5/19/10 12 1130 119 1 2
5/19/10 12 12 00 12 7 1 2
5/19/10 12 12 30 13 2 1 2
5/19/10 12 13 00 13 6 1 2
5/19/10 12 13 30 13 7 1 2
5/19/10 12 14 00 13 7 1 2
5/19/10 12 14 30 13 7 1 2
5/19/10 12 15 00 13 6 1 2
5/19/10 12 15 30 13 3 1 2
5/19/10 12 16 00 12 9 1 2
5/19/10 12 16 30 12 6 1 2
5/19/10 12 17 00 12 5 1 2
5/19/10 12 17 30 12 6 1 2
5/19/10 12 18 00 12 6 1 2
5/19/10 12 18 30 12 7 1 2
5/19/10 12 19 00 12 7 1 2
5/19/10 12 19 30 12 5 1 2
5/19/10 12 20 00 12 4 1 2
5/19/10 12 20 30 12 5 1 2
5/19/10 12 21 00 12 5 1 2
5/19/10 12 21 30 12 4 1 2
5/19/10 12 22 00 12 5 0 0
5/19/10 12 22 30 12 6 0 0
5/19/10 12 23 00 12 6 1 2
5/19/10 12 23 30 12 7 0 2
5/19/10 12 24 00 12 7 0 2
5/19/10 12 24 30 12 6 1 2
5/19/10 12 25 00 11 5 1 1
5/19/10 12 25 30 9 0 1 1
5/19/10 12 26 00 7 7 1 1
5/19/10 12 26 30 7 3 0 1
5/19/10 12 27 00 6 8 0 0
5/19/10 12 27 30 7 5 0 0
5/19/10 12 28 00 7 9 1 1
5/19/10 12 28 30 9 5 1 1
5/19/10 12 29 00 9 7 1 1
5/19/10 12 29 30 9 3 1 1
Average 118 1 2
TOCDF PDARS Data
5/19/10
APPENDIX F
MPF RATA Fuel Flows
MPF Fuel Flow
MPF RATA
Minimum Req d 84483scfm
1^^^
19-May-10 07 35 00 165 171678
19-May-10 07 35 30 165 171782
19 May 10 07 36 DO 165 172199
19 May 10 07 36 30 163 170322
19 May 10 07 37 00 164 170948
19 May 10 07 37 30 163 169592
19 May-10 07 38 00 162 168757
19 May 10 07 3S 30 163 170218
19 May 10 07 39 00 163 169488
19-May 10 07 39 30 162 166653
19 May-10 07 40 00 162 169175
19 May-10 07 40 30 161 168340
19-May 10 07 41 00 160 167297
19 May 10 07 41 30 157 163855
19 May 10 07 42 00 159 165316
19 May 10 07 42 30 162 168862
19 May 10 07 43 00 164 170635
19 May 10 07 43 30 163 170218
19 May 10 07 44 00 163 170322
19 May 10 07 44 30 162 168757
19 May 10 07 45 00 163 170426
19 May-10 07 45 30 160 167089
19-May 10 07 46 00 160 166984
19 May 10 07 46 30 159 165941
19 May 10 07 47 00 159 165628
19 May 10 07 47 30 155 161665
19 May 10 07 48 00 153 159370
19 May 10 07 48 30 150 156137
19 May 10 07 49 00 145 151652
19 May 10 07 49 30 144 149983
19 May 10 07 50 00 141 146750
19 May 10 07 50 30 141 147480
19 May 10 07 51 00 138 143517
19 May 10 07 51 30 137 142474
19 May 10 07 52 00 135 140909
19 May 10 07 52 30 136 141639
19 May 10 07 53 00 136 141848
19 May 10 07 53 30 136 141848
19 May 10 07 54 00 137 142787
19 May 10 07 54 30 137 142891
19 May 10 07 55 00 137 142370
19 May-10 07 55 30 137 142474
19 May-10 07 56 00 139 144768
19 May 10 07 56 30 138 143934
19 May 10 07 57 00 138 143830
19 May 10 07 57 30 137 142370
19 May 10 07 58 00 137 142995
19 May 10 07 58 30 137 143100
19 May-10 07 59 00 137 142787
19 May-10 07 59 30 138 143517
19 May 10 08 00 00 136 142057
19-May 10 08 00 30 137 143204
19 May 10 08 01 00 137 142474
19 May-10 08 01 30 138 143517
19 May 10 08 02 00 137 142370
19 May 10 08 02 30 136 142265
19 May 10 08 03 00 137 142891
^^^^^^
0 171678
0 171782
0 172199
0 170322
0 170948
0 169592
0 168757
0 170218
0 169488
0 168653
0 169175
0 168340
0 167297
0 163855
0 165316
0 168862
0 170635
0 170218
0 170322
0 168757
0 170426
0 167089
0 166984
0 165941
0 165628
0 161665
0 159370
0 156137
0 151652
0 149983
0 146750
0 147480
0 143517
0 142474
0 140909
0 141639
0 141848
0 141848
0 142787
0 142891
0 142370
0 142474
0 144768
0 143934
0 143830
0 142370
0 142995
0 143100
0 142787
0 143517
0 142057
0 143204
0 142474
0 143517
0 142370
0 142265
0 142891
TOCDF PDARS Data
5/19/2010
MPF Fuel Flow
MPF RATA
Minimum Req d 84483scfm
iTMlmSl^Sr^ilf^
19 May 10 08 03 30 138 144351
19 May 10 08 04 00 137 142474
19-May-10 08 04 30 139 145081
19-May-10 0e05 00 139 144456
19 May 10 08 05 30 139 144560
19 May 10 08 06 00 136 142265
19 May 10 08 06 30 137 142891
19 May-10 08 07 00 136 141535
19 May 10 08 07 30 138 143413
19 May 10 08 08 00 137 142787
19 May 10 08 08 30 139 145081
19 May 10 08 09 00 141 146646
19 May-10 08 09 30 136 141431
19 May 10 08 10 00 130 135903
19 May 10 08 10 30 126 131209
19 May 10 08 11 00 123 128393
19 May 10 08 11 30 120 125577
19 May 10 08 12 00 117 121718
19 May 10 08 12 30 118 123178
19 May 10 08 13 00 116 120571
19 May 10 08 13 30 115 120362
19 May 10 08 14 00 116 121092
19 May-10 08 14 30 115 119841
19 May-10 08 15 00 115 119632
19 May 10 08 15 30 115 119945
19 May 10 08 16 00 118 122553
19 May 10 08 16 30 118 122865
19 May 10 08 17 00 120 125056
19 May 10 08 17 30 119 123804
19 May 10 08 18 00 117 121927
19 May-10 08 18 30 117 121718
19 May 10 08 19 00 117 122448
19 May 10 08 19 30 118 122865
19 May 10 08 20 00 118 122761
19-May 10 08 20 30 116 121197
19 May-10 08 21 00 117 122135
19 May 10 08 21 30 117 122031
19 May 10 08 22 00 117 122344
19 May 10 08 22 30 117 121614
19 May 10 08 23 00 116 120884
19 May 10 08 23 30 118 122761
19 May 10 08 24 00 116 121301
19 May 10 08 24 30 117 122135
19 May 10 08 25 00 118 122970
19 May 10 08 25 30 119 123596
19 May-10 08 26 00 116 120988
19 May 10 08 26 30 116 121301
19 May 10 08 27 00 119 124430
19 May 10 08 27 30 120 124743
19 May 10 08 28 00 118 123074
19 May 10 08 28 30 117 122135
19 May 10 08 29 00 118 122970
19 May 10 08 29 30 117 121718
19 May 10 08 30 00 117 122031
19 May 10 08 30 30 119 124221
19 May-10 08 31 00 119 124221
19 May 10 08 31 30 119 123700
0 144351
0 142474
0 145081
0 144456
0 144560
0 142265
0 142891
0 141535
0 143413
0 142787
0 145081
0 146646
0 141431
0 135903
0 131209
0 128393
0 125577
0 121718
0 123178
0 120571
0 120362
0 121092
0 119841
0 119632
0 119945
0 122553
0 122865
0 125056
0 123804
0 121927
0 121718
0 122448
0 122865
0 122761
0 121197
0 122135
0 122031
0 122344
0 121614
0 120884
0 122761
0 121301
0 122135
0 122970
0 123596
0 120988
0 121301
0 124430
0 124743
0 123074
0 122135
0 122970
0 121718
0 122031
0 124221
0 124221
0 123700
TOCDF PDARS Data
5/19/2010
MPF Fuel Flow
MPF RATA
Minimum Req d 84483scfm
19-May 10 08 32 00 119 123804
19 May 10 08 32 30 117 122240
19 May 10 08 33 00 117 121510
19 May 10 08 33 30 117 121614
19 May 10 08 34 00 117 122135
19 May 10 08 34 30 117 121927
19-May-10 08 35 00 119 123908
19 May 10 08 35 30 118 123491
19 May-10 08 36 00 120 124847
19-May-10 08 36 30 119 124534
19 May 10 08 37 00 117 121614
19 May 10 08 37 30 116 121197
19 May-10 08 38 00 117 122240
19 May 10 08 38 30 117 121822
19-May-10 08 39 00 117 122344
19 May 10 08 39 30 117 121822
19 May 10 08 40 00 119 124326
19 May 10 08 40 30 118 123387
19 May 10 08 41 00 118 123491
19 May-10 08 41 30 119 123700
19 May 10 08 42 00 116 121301
19 May 10 08 42 30 118 123283
19 May 10 08 43 00 116 120779
19 May 10 08 43 30 118 122761
19 May 10 08 44 00 117 122448
19 May 10 08 44 30 118 122970
19 May 10 08 45 00 118 123283
19 May 10 08 45 30 118 122970
19 May 10 08 46 00 117 122344
19 May 10 08 46 30 117 122448
19 May 10 08 47 00 117 122031
19 May 10 08 47 30 117 121718
19 May 10 08 48 00 117 121822
19 May 10 08 48 30 120 124639
19 May 10 08 49 00 119 124117
19 May 10 08 49 30 119 123908
19 May 10 08 50 00 119 124430
19 May 10 08 50 30 116 121301
19 May 10 08 51 00 118 122761
19 May 10 08 51 30 119 124013
19 May 10 08 52 00 119 124534
19 May 10 08 52 30 119 124534
19-May 10 08 53 00 119 124326
19 May-10 08 53 30 119 124534
19 May 10 08 54 00 119 124326
19 May 10 08 54 30 120 124639
19 May 10 08 55 00 118 123491
19 May 10 08 55 30 119 124013
19 May 10 08 56 00 119 124221
19 May 10 08 56 30 120 125264
19 May 10 08 57 00 119 124326
19 May 10 08 57 30 119 124430
19 May 10 08 58 00 120 125160
19 May 10 08 58 30 119 123908
19 May 10 08 59 00 120 125473
19 May 10 08 59 30 120 124951
19 May 10 09 00 00 119 124534
0 123804
0 122240
0 121510
0 121614
0 122135
0 121927
0 123908
0 123491
0 124847
0 124534
0 121614
0 121197
0 122240
0 121822
0 122344
0 121822
0 124326
0 123387
0 123491
0 123700
0 121301
0 123283
0 120779
0 122761
0 122448
0 122970
0 123283
0 122970
0 122344
0 122448
0 122031
0 121718
0 121822
0 124639
0 124117
0 123908
0 124430
0 121301
0 122761
0 124013
0 124534
0 124534
0 124326
0 124534
0 124326
0 124639
0 123491
0 124013
0 124221
0 125264
0 124326
0 124430
0 125160
0 123908
0 125473
0 124951
0 124534
TOCDF PDARS Data
5/19/2010
MPF Fuel Flow
MPF RATA
Minimum Req d 84483scfm
19 May 10 09 00 30 119 123804
19-May 10 09 01 00 119 124534
19 May 10 09 01 30 120 124847
19-May 10 09 02 00 119 124117
19-May 10 09 02 30 120 124639
19 May 10 09 03 00 121 126412
19 May 10 09 03 30 121 126307
19-May-10 09 04 00 121 126307
19 May 10 09 04 30 122 126933
19 May 10 09 05 00 122 126829
19 May 10 09 05 30 119 124117
19 May 10 09 06 00 123 128706
19-May 10 09 06 30 124 129123
19-May 10 09 07 00 124 129645
19 May 10 09 07 30 125 129958
19 May 10 09 08 00 128 133504
19 May 10 09 08 30 133 138928
19-May 10 09 09 00 135 140805
19 May 10 09 09 30 138 144247
19 May 10 09 10 00 145 151235
19 May 10 09 10 30 149 155720
19-May-10 09 11 00 156 162291
19 May 10 09 11 30 157 163855
19 May 10 09 12 00 159 166046
19 May 10 09 12 30 161 168340
19 May 10 09 13 00 162 169279
19 May 10 09 13 30 159 165628
19 May 10 09 14 00 160 166671
19 May 10 09 14 30 159 165420
19 May 10 09 15 00 157 163647
19 May 10 09 15 30 158 164273
19 May 10 09 16 00 156 162499
19 May 10 09 16 30 157 163542
19 May 10 09 17 00 155 161248
19 May-10 09 17 30 153 159996
19 May 10 09 18 00 154 160413
19 May 10 09 18 30 154 160518
19 May 10 09 19 00 154 160101
19 May 10 09 19 30 152 158432
19 May 10 09 20 00 154 160101
19 May 10 09 20 30 153 159162
19 May 10 09 21 00 151 157284
19 May 10 09 21 30 153 159579
19 May 10 09 22 00 152 158432
19 May 10 09 22 30 152 158849
19 May 10 09 23 00 151 157493
19 May 10 09 23 30 152 158015
19 May 10 09 24 00 151 156972
19 May 10 09 24 30 152 158119
19 May 10 09 25 00 151 157910
19 May 10 09 25 30 150 156763
19 May 10 09 26 00 153 159266
19 May 10 09 26 30 151 157806
19 May 10 09 27 00 152 158327
19 May 10 09 27 30 153 159683
19 May 10 09 28 00 153 159162
19 May-10 09 28 30 152 158536
0 123804
0 124534
0 124847
0 124117
0 124639
0 126412
0 126307
0 126307
0 126933
0 126829
0 124117
0 128706
0 129123
0 129645
0 129958
0 133504
0 138928
0 140805
0 144247
0 151235
0 155720
0 162291
0 163855
0 166046
0 168340
0 169279
0 165628
0 166671
0 165420
0 163647
0 164273
0 162499
0 163542
0 161248
0 159996
0 160413
0 160518
0 160101
0 158432
0 160101
0 159162
0 157284
0 159579
0 158432
0 158849
0 157493
0 158015
0 156972
0 158119
0 157910
0 156763
0 159266
0 157806
0 158327
0 159683
0 159162
0 158536
TOCDF PDARS Data
5/19/2010
MPF Fuel Flow
MPF RATA
Minimum Req d 84483scfm
19-May 10 09 29 00 153 159683
19 May 10 09 29 30 153 159475
19 May 10 09 30 00 153 159058
19 May-10 09 30 30 150 156033
18-May-10 09 31 00 152 156849
19 May-10 09 31 30 152 158536
lg-May 10 09 32 00 153 159370
19 May 10 09 32 30 152 158432
19 May 10 09 33 00 152 158432
19-May-10 09 33 30 151 157076
19-May-10 09 34 00 153 159683
19 May-10 09 34 30 153 159370
19 May 10 09 35 00 152 158849
19 May 10 09 35 30 152 158640
19-May 10 09 36 00 152 158849
19 May 10 09 36 30 152 158745
19 May 10 09 37 00 153 159162
19 May 10 09 37 30 153 159788
19 May 10 09 38 00 153 159162
19-May 10 09 38 30 153 159162
19 May 10 09 39 00 152 158015
19 May 10 09 39 30 153 159892
19 May 10 09 40 00 151 157076
19 May 10 09 40 30 150 156450
19 May 10 09 41 00 150 156346
19-May 10 09 41 30 150 156450
19 May 10 09 42 00 151 157597
19 May 10 09 42 30 151 157910
19 May 10 09 43 00 152 158119
19 May 10 09 43 30 153 159266
19 May 10 09 44 00 153 159996
19 May 10 09 44 30 152 158327
19-May 10 09 45 00 153 159058
19-May-10 09 45 30 151 157702
19 May 10 09 46 00 151 157389
19 May 10 09 46 30 151 157702
19 May 10 09 47 00 153 159683
19 May 10 09 47 30 154 160101
19 May 10 09 48 00 152 158432
19 May 10 09 48 30 150 156137
19 May 10 09 49 00 151 157597
19 May 10 09 49 30 151 157702
19 May 10 09 50 00 152 158119
19 May 10 09 50 30 152 158432
19 May 10 09 51 00 153 159788
19 May 10 09 51 30 154 160309
19 May 10 09 52 00 151 157180
19 May 10 09 52 30 150 156137
19 May 10 09 53 00 152 158536
19 May 10 09 53 30 154 160205
19 May 10 09 54 00 154 160413
19 May 10 09 54 30 153 159892
19 May 10 09 55 00 152 158640
19 May 10 09 55 30 153 159266
19 May-10 09 56 00 151 156972
19 May 10 09 56 30 150 156659
19 May-10 09 57 00 151 157597
_
0 159683
0 159475
0 159058
0 156033
0 158849
0 158536
0 159370
0 158432
0 158432
0 157076
0 159683
0 159370
0 158849
0 158640
0 158849
0 158745
0 159162
0 159788
0 159162
0 159162
0 158015
0 159892
0 157076
0 156450
0 156346
0 156450
0 157597
0 157910
0 158119
0 159266
0 159996
0 158327
0 159058
0 157702
0 157389
0 157702
0 159683
0 160101
0 158432
0 156137
0 157597
0 157702
0 158119
0 158432
0 159788
0 160309
0 157180
0 156137
0 158536
0 160205
0 160413
0 159892
0 158640
0 159266
0 156972
0 156659
0 157597
TOCDF PDARS Data
5/19/2010
MPF Fuel Flow
MPF RATA
Minimum Req d 84483scfm
19-May-10 09 57 30 154 160622
19-May-10 09 56 00 153 159266
19 May-10 09 58 30 153 159996
lg-May-10 09 59 00 154 160101
19 May 10 09 59 30 153 159370
19 May 10 10 00 00 151 157493
19-May-10 10 00 30 150 156867
19-May 10 10 01 00 153 159162
19 May 10 10 01 30 154 160309
19 May 10 10 02 00 154 160101
19 May-10 10 02 30 153 159162
19 May 10 10 03 00 153 159579
19 May 10 10 03 30 153 159370
19-May 10 10 04 00 150 156867
19 May 10 10 04 30 150 156450
19 May 10 10 05 00 151 157284
19-May-10 10 05 30 154 160101
19 May 10 10 06 00 154 160518
19 May 10 10 06 30 153 159475
19-May-10 10 07 00 153 159579
19-May-10 10 07 30 154 160518
19 May 10 10 08 00 154 160205
19 May 10 10 08 30 152 158640
19 May-10 10 09 00 151 157806
19 May 10 10 09 30 154 160726
19 May 10 10 10 00 153 159892
19 May 10 10 10 30 154 160205
19 May 10 10 11 00 151 157389
19 May 10 10 11 30 152 158640
19 May-10 10 12 00 152 158536
19 May 10 10 12 30 151 157389
19 May 10 10 13 00 153 159996
19 May 10 10 13 30 154 160518
19 May 10 10 14 00 153 159475
19 May 10 10 14 30 154 160205
19 May 10 10 15 00 154 160622
19 May 10 10 15 30 152 158223
19 May 10 10 16 00 153 159058
19 May 10 10 16 30 154 160831
19 May 10 10 17 00 154 160101
19 May 10 10 17 30 153 159683
19 May-10 10 18 00 153 159579
19-May-10 10 18 30 153 159788
19 May 10 10 19 00 154 160935
19 May 10 10 19 30 153 159579
19 May 10 10 20 00 152 158953
19 May 10 10 20 30 153 159788
19 May 10 10 21 00 153 159683
19 May 10 10 21 30 154 160101
19 May 10 10 22 00 154 160309
19 May 10 10 22 30 153 159579
19 May 10 10 23 00 152 158849
19 May 10 10 23 30 153 159683
19 May 10 10 24 00 154 160935
19 May 10 10 24 30 152 158849
19 May 10 10 25 00 153 159892
19 May 10 10 25 30 154 160726
_ . . . w
0 160622
0 159266
0 159996
0 160101
0 159370
0 157493
0 156867
0 159162
0 160309
0 160101
0 159162
0 159579
0 159370
0 156867
0 156450
0 157284
0 160101
0 160518
0 159475
0 159579
0 160518
0 160205
0 158640
0 157806
0 160726
0 159892
0 160205
0 157389
0 158640
0 158536
0 157389
0 159996
0 160518
0 159475
0 160205
0 160622
0 158223
0 159058
0 160831
0 160101
0 159683
0 159579
0 159788
0 160935
0 159579
0 158953
0 159788
0 159683
0 160101
0 160309
0 159579
0 158849
0 159683
0 160935
0 158849
0 159892
0 160726
TOCDF PDARS Data
5/19/2010
8
MPF Fuel Flow
MPF RATA
Minimum Req d 84483scfm
^^^^^^^^
^^^^
159370 19 May-10 10 26 00 153 ^ 159370
19-May-10 10 26 30 153 159788
19 May-10 10 27 00 155 161144
19 May-10 10 27 30 153 159996
19 May 10 10 28 00 154 160205
19-May-10 10 28 30 154 160726
19 May-10 10 29 00 153 159788
19 May-10 10 29 30 152 158953
19 May 10 10 30 00 154 161039
19-May 10 10 30 30 154 160935
19 May 10 10 31 00 153 159370
19 May 10 10 31 30 154 160205
19 May-10 10 32 00 155 161456
19 May 10 10 32 30 156 162187
19 May 10 10 33 00 154 160101
19 May-10 10 33 30 154 160101
19 May-10 10 34 00 154 160622
19 May 10 10 34 30 153 159683
19 May 10 10 35 00 153 159266
19 May-10 10 35 30 154 160413
19 May-10 10 36 00 154 160831
19 May 10 10 36 30 154 160935
19 May 10 10 37 00 153 159892
19 May-10 10 37 30 152 158849
19 May-10 10 38 00 153 159788
19 May 10 10 38 30 154 160309
19-May 10 10 39 00 154 160101
19 May-10 10 39 30 153 159683
19 May 10 10 40 00 153 159579
19 May 10 10 40 30 155 161978
19 May 10 10 41 00 153 159996
19 May 10 10 41 30 152 158849
19 May 10 10 42 00 154 160518
19 May 10 10 42 30 153 159996
19 May 10 10 43 00 154 161039
19 May-10 10 43 30 152 158015
19 May-10 10 44 00 150 156763
19 May-10 10 44 30 151 157076
19 May-10 10 45 00 147 153530
19 May 10 10 45 30 145 151652
19 May 10 10 46 00 141 147063
19 May 10 10 46 30 140 145811
19 May 10 10 47 00 136 142057
19 May 10 10 47 30 133 139032
19 May 10 10 48 00 133 138928
19 May 10 10 48 30 134 139866
19 May 10 10 49 00 133 139032
19 May 10 10 49 30 134 139658
19 May 10 10 50 00 131 137050
19 May 10 10 50 30 132 137363
19 May 10 10 51 00 133 139136
19 May 10 10 51 30 133 139136
19 May 10 10 52 00 133 138406
19 May 10 10 52 30 133 138406
19 May-10 10 53 00 134 139449
19 May 10 10 53 30 134 139658
19 May 10 10 54 00 134 139866
0 159370
0 159788
0 161144
0 159996
0 160205
0 160726
0 159788
0 158953
0 161039
0 160935
0 159370
0 160205
0 161456
0 162187
0 160101
0 160101
0 160622
0 159683
0 159266
0 160413
0 160831
0 160935
0 159892
0 158849
0 159788
0 160309
0 160101
0 159683
0 159579
0 161978
0 159996
0 158849
0 160518
0 159996
0 161039
0 158015
0 156763
0 157076
0 153530
0 151652
0 147063
0 145811
0 142057
0 139032
0 138928
0 139866
0 139032
0 139658
0 137050
0 137363
0 139136
0 139136
0 138406
0 138406
0 139449
0 139658
0 139866
TOCDF PDARS Data
5/19/2010
9
MPF Fuel Flow
MPF RATA
Minimum Req d 84483scfm
139553 ig-May 10 10 54 30 134 139553
19-May 10 10 55 00 136 141848
19-May-10 10 55 30 135 141014
19-May 10 10 56 00 136 141535
19-May 10 10 56 30 135 141014
19-May 10 10 57 00 136 1419S2
19 May-10 10 57 30 138 143934
19 May 10 10 58 00 137 142995
19 May-10 10 58 30 137 142995
19-May 10 10 59 00 136 141744
19 May 10 10 59 30 136 142265
19 May 10 11 00 00 138 143830
19-May-10 11 00 30 137 142787
19 May 10 11 01 00 135 140284
19 May 10 11 01 30 135 141014
19 May 10 11 02 00 135 141014
19 May-10 11 02 30 137 142370
19 May 10 11 03 00 136 141848
19 May 10 11 03 30 136 141848
19-May 10 11 04 00 137 143204
19-May 10 11 04 30 136 142057
19 May 10 11 05 00 135 140596
19 May 10 11 05 30 138 144143
19-May 10 11 06 00 139 144664
19 May-10 11 06 30 139 144560
19 May-10 11 07 00 131 136842
19-May 10 11 07 30 127 132565
19 May 10 11 08 00 123 127768
19 May 10 11 08 30 120 124847
19 May-10 11 09 00 119 124534
19-May 10 11 09 30 117 121927
19-May 10 11 10 00 117 122344
19 May 10 11 10 30 116 121197
19-May 10 11 11 00 117 122344
19-May 10 11 11 30 117 121718
19 May-10 11 12 00 116 121405
19 May 10 11 12 30 117 121718
19 May 10 11 13 00 118 122553
19-May 10 11 13 30 119 123700
19-May 10 11 14 00 118 123178
19-May 10 11 14 30 118 123074
19 May 10 11 15 00 121 125682
19 May 10 11 15 30 121 125890
19 May 10 11 16 00 120 124951
19 May-10 11 16 30 121 125682
19 May 10 11 17 00 120 125369
19 May 10 11 17 30 119 123804
19 May 10 11 18 00 121 125682
19-May 10 11 18 30 120 125160
19 May 10 11 19 00 120 125577
19 May-10 11 19 30 120 124951
19-May 10 11 20 00 119 124534
19 May 10 11 20 30 120 125369
19-May 10 11 21 00 121 125890
19 May-10 11 21 30 120 125473
19 May-10 11 22 00 120 124639
19 May 10 11 22 30 119 124534
^^^^ ^^^^
0 139553
0 141848
0 141014
0 141535
0 141014
0 141952
0 143934
0 142995
0 142995
0 141744
0 142265
0 143830
0 142787
0 140284
0 141014
0 141014
0 142370
0 141848
0 141848
0 143204
0 142057
0 140596
0 144143
0 144664
0 144560
0 136842
0 132565
0 127768
0 124847
0 124534
0 121927
0 122344
0 121197
0 122344
0 121718
0 121405
0 121718
0 122553
0 123700
0 123178
0 123074
0 125682
0 125890
0 124951
0 125682
0 125369
0 123804
0 125682
0 125160
0 125577
0 124951
0 124534
0 125369
0 125890
0 125473
0 124639
0 124534
TOCDF PDARS Data
5/19/2010
10
MPF Fuel Flow
MPF RATA
Minimum Req d 84483scfm
19-May-10 11 23 00 121 125890
19 May-10 11 23 30 120 125264
19 May 10 11 24 00 120 124951
19 May 10 11 24 30 120 124639
19-May-10 11 25 00 120 125473
19 May-10 11 25 30 120 124847
19 May 10 11 26 00 120 125577
19 May 10 11 26 30 121 125786
19 May 10 11 27 00 120 125160
19 May-10 11 27 30 121 125786
19-May-10 11 28 00 119 124534
19 May 10 11 28 30 121 126307
19 May 10 11 29 00 121 125682
19 May 10 11 29 30 119 124117
19-May 10 11 30 00 122 127663
19-May-10 11 30 30 122 126933
19 May 10 11 31 00 120 125160
19 May 10 11 31 30 120 124639
19 May 10 11 32 00 118 123491
19-May 10 11 32 30 120 125160
19-May-10 11 33 00 121 125890
19 May 10 11 33 30 124 128915
19 May 10 11 34 00 128 133087
19 May 10 11 34 30 126 131835
19 May 10 11 35 00 126 131731
19-May-10 11 35 30 124 129436
19 May 10 11 36 00 124 129123
19 May 10 11 36 30 124 129541
19 May 10 11 37 00 123 128289
19 May 10 11 37 30 122 127350
19-May 10 11 38 00 121 125890
19 May 10 11 38 30 120 125473
19 May 10 11 39 00 120 124847
19 May 10 11 39 30 120 125369
19 May 10 11 40 00 120 125577
19 May 10 11 40 30 118 122865
19 May 10 11 41 00 117 121927
19 May 10 11 41 30 120 124951
19 May 10 11 42 00 119 124326
19 May 10 11 42 30 120 125369
19 May 10 11 43 00 120 125264
19 May 10 11 43 30 120 125577
19 May 10 11 44 00 120 125369
19 May 10 11 44 30 119 124326
19 May 10 11 45 00 126 131731
19 May 10 11 45 30 128 133400
19 May 10 11 46 00 130 135381
19 May 10 11 46 30 130 135069
19 May-10 11 47 00 130 135069
19 May 10 11 47 30 130 135069
19 May 10 11 48 00 129 134547
19 May 10 11 48 30 127 131940
19 May 10 11 49 00 128 133608
19 May 10 11 49 30 126 131209
19 May 10 11 50 00 126 131627
19 May 10 11 50 30 126 131001
19 May 10 11 51 00 124 129019
0 125890
0 125264
0 124951
0 124639
0 125473
0 124847
0 125577
0 125786
0 125160
0 125786
0 124534
0 126307
0 125682
0 124117
0 127663
0 126933
0 125160
0 124639
0 123491
0 125160
0 125890
0 128915
0 133087
0 131835
0 131731
0 129436
0 129123
0 129541
0 128289
0 127350
0 125890
0 125473
0 124847
0 125369
0 125577
0 122865
0 121927
0 124951
0 124326
0 125369
0 125264
0 125577
0 125369
0 124326
0 131731
0 133400
0 135381
0 135069
0 135069
0 135069
0 134547
0 131940
0 133608
0 131209
0 131627
0 131001
0 129019
TOCDF PDARS Data
5/19/2010
11
MPF Fuel Flow
MPF RATA
Minimum Req d 84483scfm
19 May 10 11 51 30 124 129436
19 May-10 11 52 00 124 129019
19-May-10 11 52 30 123 128498
19 May-10 11 53 00 124 128811
19 May-10 11 53 30 124 129541
19 May-10 11 54 00 124 129541
19 May-10 11 54 30 124 129332
19 May-10 11 55 00 122 127455
19 May 10 11 55 30 124 129541
19 May 10 11 56 00 122 127455
19 May 10 11 56 30 124 128915
19 May 10 11 57 00 123 128602
19 May 10 11 57 30 124 129228
19 May-10 11 58 00 125 129854
19 May 10 11 58 30 125 129854
19 May 10 11 59 00 123 128393
19 May 10 11 59 30 124 129645
19 May 10 12 00 00 124 128915
19 May 10 12 00 30 125 130271
19 May-10 12 01 00 125 129854
19 May 10 12 01 30 124 129228
19 May 10 12 02 00 123 128498
19 May 10 12 02 30 123 128602
19 May-10 12 03 00 124 128915
19 May 10 12 03 30 124 129019
19 May 10 12 04 00 125 129854
19-May-10 12 04 30 124 129228
19 May 10 12 05 00 125 130062
19 May 10 12 05 30 123 128498
19 May 10 12 06 00 124 129332
19 May 10 12 06 30 123 128706
19 May 10 12 07 00 123 128289
19 May 10 12 07 30 124 129332
19 May 10 12 08 00 122 127142
19 May 10 12 08 30 122 127350
19 May 10 12 09 00 122 127663
19 May 10 12 09 30 124 129436
19 May 10 12 10 00 98 102110
19-May 10 12 10 30 99 102840
19 May 10 12 11 00 91 94496
19-May-10 12 11 30 92 95852
19 May 10 12 12 00 93 97208
19 May 10 12 12 30 95 98876
19 May 10 12 13 00 98 102110
19-May 10 12 13 30 106 110975
19 May 10 12 14 00 113 117859
19 May 10 12 14 30 118 123074
19 May 10 12 15 00 118 123178
19 May 10 12 15 30 116 120675
19-May 10 12 16 00 115 119632
19-May 10 12 16 30 112 117025
19 May 10 12 17 00 114 118798
19 May 10 12 17 30 120 124743
19-May 10 12 18 00 119 123596
19 May 10 12 18 30 119 123804
19-May 10 12 19 00 117 121927
19 May 10 12 19 30 117 122240
0 129436
0 129019
0 128498
0 128811
0 129541
0 129541
0 129332
0 127455
0 129541
0 127455
0 128915
0 128602
0 129228
0 129854
0 129854
0 128393
0 129645
0 128915
0 130271
0 129854
0 129228
0 128498
0 128602
0 128915
0 129019
0 129854
0 129228
0 130062
0 128498
0 129332
0 128706
0 128289
0 129332
0 127142
0 127350
0 127663
0 129436
0 102110
0 102840
0 94496
0 95852
0 97208
0 98876
0 102110
0 110975
0 117859
0 123074
0 123178
0 120675
0 119632
0 117025
0 118798
0 124743
0 123596
0 123804
0 121927
0 122240
TOCDF PDARS Data
5/19/2010
12
MPF Fuel Flow
MPF RATA
Minimum Req d 84483scfm
^^^^^^
19-May-10 12 20 00 117 121510
19-May-10 12 20 30 118 123491
19-May-10 12 21 00 121 126099
19-May 10 12 21 30 124 128915
19 May 10 12 22 00 128 133713
19 May 10 12 22 30 132 137676
19 May-10 12 23 00 150 156137
19 May 10 12 23 30 180 188053
19 May 10 12 24 00 187 194832
19 May 10 12 24 30 183 190765
19 May 10 12 25 00 170 177623
19 May 10 12 25 30 136 141952
19 May 10 12 26 00 111 116190
19 May-10 12 26 30 109 114000
19 May-10 12 27 00 107 111392
19 May 10 12 27 30 106 110975
19 May 10 12 28 00 105 109724
19 May 10 12 28 30 102 106386
19 May-10 12 29 00 103 107429
19 May-10 12 29 30 108 112748
19-May-10 12 30 00 110 114939
19 May 10 12 30 30 113 117338
0 121510
0 123491
0 126099
0 128915
0 133713
0 137676
0 156137
0 188053
0 194832
0 190765
0 177623
0 141952
0 116190
0 114000
0 111392
0 110975
0 109724
0 106386
0 107429
0 112748
0 114939
0 117338
TOCDF PDARS Data
5/19/2010
APPENDIX G
TOCDF EPA Protocol 1 Gas Certifications
JPRJUaUK
DocNumber 00000002774
Praxnir
5700 South Alameda Street
Los Angeles CA 90058
Telephone [phone]
Facsimile [phone]
Customer & Order IttfemmUon
EGG Praxair Order Number 06029731-00
CustomerP O Number 01461629
Customer Reference Number WA 344
Fill Dot
Pari Numbir
Lot Ntimbtr
Cflmikr Slyli <* Ouilm
Certified Concentration Cylindir Pnmrr A Votumt
Expiration Date. 5/7/2011
Cylinder Number CC 179188 Analytical Uncertainty
9 05 % OXYGEN ± 1 %
Balance NITROGEN
NOx ppm = N/A NOX Values for Reference Only
EV NI0X9E AS
10SSI2002
AS S90
2000 psi 140 cuf)
Certifcation Information Certification Date 5/7/2008 Term 36 Months Expiration Dale 5/7/2011
This cylinder was certified according to the 1997 EPA Traceability Protocof Document #EPA-600/R-97/121 using Procedure G1
Do Not Use this Standard if Pressure is less than 150 PSIG
Analytical Data
1 Component OXYGEH
Rfiquflsted Concentralion
Certified Cancenlralion
Instrumenl UAAd
Analytical Mslhotf
Last MuU>poinl CaMbralion
(R=Rsfeience Sttmdard Z=Zero Gss. C-Gas Candidate]
9K
905%
SwiEinOiymalSE S/NA12 639
Paramagnekc
4/19/2008
Flr>t Analysis Data
Z 0 R 1001
R loot Z 0
Z Q C 9 05
Date 5/7/2008
UOM
C 9 05 Cone SOS
C 9 05 Cone 9 0S
R loot Cone 9 05
IHe»n Test Assay
Analyzed by
Reference Standard Type GMIS
Ref Std Cylnder# CC 257765
Ref Std Cone: 1001*
Ref Std Traceable lo SRM # vs 265Sa
SRM Sample t» 72 2B B
SRM Cylinder n CUiM()6696
Second Analysis Data
Z 0 R 0 C 0
R 0 Z 0 C 0
Z 0 C 0 R 0
Dale
Cone
Cone
Cone
UOM Mean Test Assay
Certified by
Keesuk Kim
ton contained herain has been prepared at your request by qualified experts within Praxair DistnlMlion Inc While we belnve that the nformalion Is accurate withm the Timits of the anatytical
employMl and a complel^ to the extent of the spectRc ar^aly^es performed we matie no warranty or representalton as to the suitaMity ol the use of the information lor any purpose The
Infonnallon is offered with the understandmg thel any use of the information is al the sole discretion and r'Sk of the uMr In no event shall the babilrty of Praxar Dislritxjtlon Inc. ensing out of the
u3ft of the informabon con tained herein exceed the fee established for providing such informaUoa
IPRJOAIR
Praxair
5700 South Alameda Street
Los Angeles. CA 90058
Telephone [phone]
Facsimile [phone]
^ - fSfMWm^" / MpA mOmCOL GAM
CUSTOMER ESC
COMPONENT
OXWKN QMIS
NISTSRMNO,
V8 SR>)«;2£59
P O NUMBER
CVUNDER NO
SA 3633
CONCENTRATION
15 03 *
R'=REFERB\CE STANDASD Z=ZBRO GAS C^GAS CANDIDATE
1 COMPONENT OxyoPN GMis
ANALYTICAL PRINCIPLE
ffSSl ANALYSIS DATE
ANALVZe|lM*KpiMODEL-S/N Siemens Oxymat 5E s/N A12-839
R is 02 I
^ 0 00
IS 02
Z 0 00
C IS 04
Paramagnetic
C IS 04
C 15 04
R 15 02
MEAN n ' AS3AV Ts CS
LAST CALIBRATION DATE
SECOND ANALYSIS DATE
R C
Z C
C R
06/02/07
con'C
CONC
\\
MEAN TEST ASSAY
Values not vaij,(] below ISO psij
THIS CYLINDER NO cc 9252s
HAS BEEN CERTIFIED ACCORDING TO SECTION
OF TRACEABILITY PROTOCOL NO Rev 9/97
PROCEDURE Gi
EPA-60O/R97/121
CERTIHED CONCENTRATION
OXYGEN 15 05 *
NITROGEN BALANCE
CERTIFIED ACCURACY
CYLI>fDER PRESSURE
CERTIFICATION DATE
EXPIRATION DATE
± 1
2000 PSIG
06/15/07
06/15/10 TERM
" iHoF TRACEABLE
36 M0NTB3
ANALYZED BY CERTIFIED BY
ERIC YOONG
Information contained herern has been prepared at your request by qualified experts within PrSxair Dislnbution Inc While wa believe lhat ttie information is awurate .
analytical methods employed and is complete to the extent of the specific analyses performed we make no warranty or representation as to the suHabi ity of '"^"f! °'JTI. ,. ^ p^^^^,
any particular purpose The mfonnation is offered with the understanding that any use of the information is at the sole discretion and risk of tht user In no event sna y
Distnbution Inc arising out of the use of the mfomiatlon contained herein exceed the fee established for providing such information
DocNumber 00000010246
Praxair
5700 Souih A] ameda Sired
Los Angeles, CA 90058
Telephone [phone]
Facsinmle [phone]
CERTIFICATE OF ANALYSIS / EPA PROTOCOL GAS
Customer & Order Information
EGG Praxair Order Number 08019P99-00
Customer P O tiwnber 02173717
Customer Reference Number WA344
hiiiDuit
fantiHiH'ttr
Ijn Ntimh4T
(yhnltr <t Omiti
Certified Contenlration Lyiintivr Prexnuv it Vahimit
Expiration Date 11/12/2011
Cylinder Number SA 15S58 Analytical Uncertainty
69 8 ppm CARBON MONOXIDE ± 1 %
Balance NITROGEN
EV N1C070ME^S
109630503
AS 350
2000 p» 140curi
NOx ppm = N/A NOX Values for Reference Only
Certifcimon Information Certification Date 11/12/2008 Term 36 Months Expiration Date 11/12/2011
This cylinder was certified according to the 1997 EPA Traceability Protocol document #EPA 600/R 97/121 using Procedure GI
Do Not Use this Standard rf Pressure is less than 150 PSIG
Analytical Data
1 Compontnt CARBON MONOKIDE
Requested Concentreuon
Certiried Conconlration
Instrumenl Used
Analytical Method
Last Mulltpoint Calibration
(R^Relerance Standard Z-Zero Gas, C^Gas Candidate)
70 ppm
e9 8 ;pm
Siemens Uilramat SE S/N
ND«
^O^UI?OOB
'icrerence Standard "Type GMIS
r^ol Std Cylinder* CC 155680
<of std Cone 99ti>|iiii
<el Sid Traceable to SRM # »s. ie7ti
SRI4 Sample # Mi
SRM Cylinder tt FF28593
First Analysis Data Date 11'50008 Second Analysis r^a^a Date
Z 0 P 99 J 0 es 8 Cone 691> 2 0 R 99 8 C 69 8 Cone 69 8
R 99 8 Z 0 C 1)9 8 Cone 69 0 R 99 8 Z 0 C 69 8 Com, 69 6
Z 0 C 69 8 R 99 8 Co-c 69 8 Z 0 C 69 8 R 99 8 Cone 69 8
UOM ppm Mean Tost Assay 59 8 ppm iOM ppm Mean Test Assay 69 8 ppm
Analyzed by Certified by
Peter Ngo Paolo Reyes
y
0
l/l^^pfcn containod herein has been propareu d ycur request bjr c|ualified experts within Praxair Distribulion Inc While we believe that the informalion is acouate within the Nmiis of the analylical
me'hods employed arxJ is complolc to Ihe extent of tf-o specific analyses parformed we make no warf^nly or rep ttantatron as to the surtsbility of the use of Ihu information for any purpose The
IP ormatior is offered with the understanding lhat any Lsn of the irformation IE al Ihe so a dtsi^ etnn arK) risk of ^cr In no event shaft the liability of Praxair Distribution Inc ansing out of the
use of Ihe informalton con tained hercm exceed J fee cstabhshed for providing such information
Making Our Planet More Productive
iPRimm
DocNumber 000004500
Pr»\air
3700 South Alameda Street
Los Angeles CA 90058
Telephone [phone]
facsimile [phone]
CERTIFICATE OF ANALYSIS / EPA PROTOCOL GAS
Customer & Order Information
PRAXAIR WHSE SALT LAKE CITY
PRAXAIR PLANT SALT LAKE CITY
SALT LAKE CITY UT 841210
Praxair Order Number 11923463
Customer P 0 Number 02678893
Customer Reference Number
Certified Concentration
Fill Dan 12/11/2009
Ptirt Numbtr EV NIC01SOME-AS
iMlNlmlxr 109934501
CylaKkr Style iOlllkl AS CGA3S0
CyltntAa-rrexatrv it yitliHnt 2000 psig 140cufL
Expiration Date 12/28/2012 NIST Traceable
Cylinder Number CC 326019 /Analytical Uncertainty
155 ppm CARBON MONOXIDE ±1 %
Balance NITROGEN
Cemfcaiion Information Certification Date 12/28/2009 Tem 36 Months Expiration Date 12/28/2012
This cylinder was certified according to the 1997 EPA Traceability Protocol Document #EPA 600/R 97/121 using Procedure G1
Do Not Use this Standard if Pressure is less than 150 PSIG
Analytical Data (R°Retemnce Standard Z-Zero Gas C^^Ges Candidate}
1 ComponenI CARBON MONOXIDE
Requested Concentration
Certified Concentration
Instalment Used
Analytical Mettiod
Last Multtpoml Calibration
150 ppm
165 ppm
Siemens Ullramat EE S/N A17 729
IVOIR
12/1/2009
Analyzed by
S'lameela Jiffrey
Reference Standard Type GMIS
Ref Std Cylinder* CC 159809
Ret Std Cone 148 8 ppm
Ref Std Traceable to SRM « vs 2636a
SRM Sample # 3-1 45
SRM Cylinder« FF2B593
nrst Anatyls Data i->/ pyirag £et.o Id An&ly&is Data Date 12fi!B/20O9
Z 0 R 148 8 C 1654 Cone 155 Z D R 148 8 C 1554 Cone 155
R 148 8 Z 0 C 1554 Cone 155 R 148 8 Z 0 C 155 2 Cone 155
Z 0 C 1554 R 148 8 Cone 155 Z 0 C 1C5 2 R 148 8 Cone 155
UOM ppm Mean Test Assay 155 ppm UOM ppm Mean Test Assay 155 ppm
Certified by
Imnatjon contained herein has been prepared at your request by quaf/fied experts within PrBxar Djstrliutlon Inc V\Ai(Je we believe that the irtformation is accurate within the limits of the analytical
_ Rhodft employed and is complete to the extent of Ihe specific analyses performed we make no warra ity or representation as lo the suitability of the use of the tnformation for any purpose The
infcmation is offered with the understanding that ar^ use of the mformatron is at the sole discretion and nsk of Ihe user In no event shaft the liability of Praxair Dtstnbution. Inc arising out of the
use of the information con tair>ed herein exceed Ihe fee established for providing such mfomiation
WRAXAIR
DocNumber 000008304
Praxnir
5700 South Alameda Street
Los Angeles CA 90058
Telephone [phone]
Facsimile [phone]
CERTIFICATE OF ANALYSIS / EPA PROTOCOL GAS 1
Customer A Order Information
EG&G DEFENSE MONITORING'M
11600 STARK RD
STOCKTON UT 840710
Praxair Order Number
Customer P 0 Number
Customer Reference Number
12733447
DMB4600103 RE
Certified Concentration
FiUDale
Pun titimbtr
I jot Number
CyllKler Style i Oiillel
Cylinder Preixiirt <( Vulumr
Expiration Date 3/27/2013 NIST Traceable
Cylinder Number CC 74747 Analytical Uncertainty
153 ppm CARBON MONOXIDE ±1 %
Balance NITROGEN
3/11/2010
NIC0150E AS
10S0070CB
AS CGA350
2000 pclg 140 cu ft
Certifcation Informauon Certification Date 3/27/2010 Term 36 Months Expiration Date 3/27/2013
This cylinder was certified according to the 1997 EPA Traceability Protocol Document #EPA 600/R-97/121 using Procedure GI
Do Not Use this Standard if Pressure is less than 150 PSIG
Analytical Data (R=RefBrancB Standard Z=Zero Gas C=Gas Candidate}
1 Component- CARBON MONOXIDE
Requetled Concentration
Certified Concentration.
Instrument Used
Analytical Method
Last Multipoint Calitiration
150 ppm
153 ppm
Siemens Ullramat 5E S/NA12 729
NDIR
3/11/2010
Analyzed by
Shameela Jiffrey
Reference Standard Type GMIS
Ref Std Cylinder # CC 159889
Ret Std Cone 148 B ppm
Ref Std Traceable lo SRM # vs 2636a
SRM Sample # 3-1-45
SRM Cylinder # FP28593
I
hlret Analysis Data Date 3/18/2010 Second Analysis Data Data 37.'201C
Z 0 R 148 8 C 152 6 Cone 153 , Z 0 R 1488 C 152 6 Cone 153
R 148 8 Z 0 C 152 6 Cone 153 R 148 0 Z 0 C 152 6 Cone 153
Z 0 C 152 6 R 148 8 Cone 153 1 Z 0 C 1526 R 148 8 Cone 153
UOM ppm Mean Test Assay 153 ppm ' UOM ppm Mean Test Assay 153 ppm
Certified by ^"^^c^
Nelson Ma
VP
information contained herein has been prepared al your request by qualified experts within Praxair DistFiUition Inc While we t»iieve lhat the information is accurate wilhm the limits of the analytical
methods employed and is compete to the extent of Ihe speciftc analyses performed we make no warranty or represenlalion as to the suitability of (he use of the infbrmafion for any purpose The
information is offered with the understanding that any use of the information is at the sole disa-etton and rtsK of the user In no event shall the fiability of Praxair Distrtoution Inc. ansmg out of the
use of the mtormation con tained herein exceed the fee established for providing such information
miUUUUR he
DocNumber 00000010627
Praxair
5700 South Alameda Street
Los Angeles, CA 90058
Telephone [phone]
Facsinule [phone]
l^RTmmTE OF2&M^$I^/MPA PROTOCOL GAS
Customer A Order It^ormation
EGG Praxair Order Nmnher 08019208 00
Customer P O Number 02173703
Customer Reference Number WA344
Certified Concentration
HIIDale
Part Hmmher
Lot Niimhtr
lytinJet Style i Otillel
CyliiK/er Pressure A Volume
NI CO1750E AS
109830901
AS 350
2000 psi 140 cu (I
Expiration Date 11/19/2011
Cylinder Number SA 15234 Analytical Uncertainty
1752 ppm CARBON MONOXIDE ±1 %
Balance NITROGEN
NOx ppm = N/A NOX Values for Reference Only
Certifcation Information. Certification Date 11/19/2008 Term 36 Months Expiration Date 11/19/2011
This cylinder was certified according to the 1997 EPA Traceability Protocol Document #EPA-600/R-97/l21 using Procedure G1
Do Not Use this Standard if Pressure is less than 150 PSIG
Analytical Data
1 ComponenI l»RBOtl UOHOXlOE
Requested Concentration
Certified Concentration
Instrument Used
Anelytleal Method
Lest Multipoint Calitvation
IR=Reteience Standard Z=Zero Gas C=Ges Candidate}
1752 ppm
Slernens Uttramat 5E S/N At2 729
NDIR
11/15/2008
Reference Standard Type GlillS
Ref Std Cylinder # GG11757
Ref Std Cone 1724 ppm
Ref Std Traceable to SRM H vs 2637a
SRM Sample # 5&E-40
SRM Cylinder* Ff23073
First Analysis Data Date 11/122006
1
Second Analysis Data ufite
Z 0 R 1724 C 1752 Cone 1752 Z. 0 R 1724 C 1752 Cone
R 1724 Z 0 C 1752 Cone 1752 R 1724 Z 0 C 1752 Cone
Z 0 C 1752 R 1724 Cone 1752 ' Z 0 C 1752 R 724 Cone
UOM ppm Mee n Test Assay 1752 ppm j UOM ppm Mean Test Assay
1752
1752
1752
1752 ppm
Analyzed by Certified by
Peter Ngo esuK Kim
' Information contained tierein hao been prepared at your request by quahried experts wittim Praxeir Dislnbution Inc \Miile we believe that ina information is accurate wittin ttie limits of Ilia enetytical
mettiods employed and is complete to the extent of ttie specific analyses performed we make no ^rananty or representation as lo the suilabiljly of the use of the infomiation for any purpose Ttie
Informstion is offered with the understanding thel any use of the nformalion is at the sole discretion and risk of the user In no event shall ttie liebllity of Praxair Oistrbution Inc ansmg out of ttie
use of the infonnalton con tained tierein exceed the fee established for providing such information
Making Our Planet More Productive
WRAXAIR
DocNumber 000006827
Prttxnir
5700 South Alameda Street
Los Angeles CA 90058
Telephone [phone]
racsimilc [phone]
CERTIFICATE OF ANALYSIS / EPA PROTOCOL GAS
Customer & Order Information
PRAXAIR WHSE SALT LAKE CITY
PRAXAIR PLANT SALT LAKE CITY
SALT UKE CITY UT 841210
Praxair Order Number 12409332
Customer P 0 Number 02746737
Customer Reference Number
Certified Concentration
FilllJoie 2/B/2010
Pan Number NI CO37S0E AS
IJH Number 109003901
CyRiitler Style/tOiiilel AS CGA 350
CylinJer PreKnire A Vuhime 200O psiQ 140 cu ft
Expiration Date 2/19/2013 NIST Traceable
Cylinder Number CC 325473 Analytical Uncertainty
3760 ppm CARBON MONOXIDE ±1 %
Balance NITROGEN
Certifcauon Information. Certification Date 2/19/2010 Term 36 Months Expiration Date 2/19/2013
This cylinder was certified according to the 1997 EPA Traceability Protocol Document #EPA 600/R 97/121 using Procedure GI
Do Not Use this Standard if Pressure is less than 150 PSIG
Analytical Data (Ri^Referenca Standard Z-Zero Gas C=Ga$ Candidate)
1 Component CARBON MONOXIDE
Requested Concentretion
Certified Concentration-
Instrument Used
Analytical Mettiod
Last Multipoint Calibration
First Analysis Data
Z 0
R 0 502
Z 0 C
UOM ppm
0 502
0
0 376
3750 ppm
3760 ppm
Siemens Ultramat SE S/N A12 729
NOIR
2/11/2010
C 0 376 Cone
C 0 376 Cone
R 0 502 Cone
Mean Test Assay
5/?oin
3760
3760
3760
3760 ppm
Analysed by
Shameela Jiffrey
Reference Standerd Type
Ref Std Cylinder #
Ret Std Cone
Ref Sid Traceable to SRM #
SRM Sample #
SRM Cylinder»
Second Analysis Data
0 R
0 502 Z
j Z 0 c
I UOM ppm
0 502
0
0 375
GMIS
SA 3516
0 502 •*
vs 263Ba
55 24 C
CLM 00480S
Date 2/iai2010
C 0 376 Cone
C 0 376 Cone
R 0 502 Cone
Mean Test Assay
3760
3760
3760
3760 ppm
Certified by
Nelson Ma
formation contained herein has been prepared at your request by qualified experts withm PrHXair Dtstntjution Inc V\ttile we believe lhat the information ra accurate withm Ihe Imits of ihe analytical
methods employed and is compleis to Ih* extent of Ihe specific analyses performed we make no wan^nty or representation as to the suitability of the use of the information for any purpose The
information ts offered with the understantfing that any use of the information is at the sole discretion and nsk of the user In no event shall the liability of Pra^tair Distribution Inc. arising out of Ihs
use of the information con tained herein exceed the fee established for providing such information
PRAXAIR
DocNumber 000009654
Pmxair
5700 South Alameda Street
Los Angeles CA 90058
Telephone [phone]
facsimile [phone]
CERTIFICATE OF ANALYSIS / EPA PROTOCOL GAS ~]
Customer A Order Iitformation
EG&G DEFENSE MONITORING'M
11600 STARK RD
STOCKTON UT 840710
Praxair Order Number
Customer P O Number
Customer Reference Number
13076551
DMB4600103
Certified Concentration
nil Dole
Pari Number
I at Number
Cyllntter S/yle A Oitlltl
Cytlikter Pressure iS Vohme
Expiration Date 4/30/2013 NIST Traceable
Cylinder Number CC133963 Analytical Uncertainty
3780 ppm CARBON MONOXIDE ± 1 %
Balance NITROGEN
4/15/2010
NICO37S0eAS
108010501
AS CGA 360
ZOOOpsifl 140 cu a.
Certifcation Informauon Certification Date 4/30/2010 Term 35 Months Expiration Date 4/30/2013
This cylinder was certified according to the 1997 EPA Traceability Protocol Document #EPA-600/R 97/121 using Procedure GI
Do Not Use this Standard if Prsssure is less than 150 PSIG
Analytical Data (R=Refeivnce Standard Z=Zero Gas C=Gas Candidate)
1 Component CAI^BON MONOXIDE
Requested Concantralion
Certified Concentration
Instrument Used
Analytical Method
Last Multipoint Calibration
^ Firsi Aildiysis Data
' Z 0 R 0 502
R 0 502 Z 0
I Z 0 C 0 37B
I
UOM ppm
3750 ppm
3780 ppm
Siemens Ultramat SE S/N A12 729
NDIR
4/11/2010
Date
C 0 37s Cone
C 0 378 Cone
R 0 502 Cone
Mean Test Assay
4/21/ljlO
3780
3780
3780
3780 ppm
Analyzed by
Shameela Jiffrey
Reference Stervtard Type
Ref Std Cylinder/*
Ref Std Cone
Ref Std Traceefcle to SRM »
SRM Sample #
SRM Cylinder*
^ Second Anelysia Dat«
1
I Z 0 R 0 602
R 0 502 Z 0
Z 0 C 0 378
UONI ppm
GMIS
SA3518
0502H
vs 2638a
55-24 C
CLM-O0480e
DDto
C 0 378 Cone
C 0 378 Cone
R 0 502 Cone
Mean Test Assay
3780
3780
3780
3780 ppm
Ceitified by
Aruna Nalla
r
•7
lormalion contained herein has t»en prepared at your request by qualified experts within P/axair Oistribulion. Ina While we believe that Ihe inlormation is accurate withn the limits of the analylical
lethods employed and is complete to the extent of the spealic analyses peifomied we make no warranty or representation as to the suitabilily of the use of the informstion for any purpoie The
information is offered with the understandnfl that any use of the information Is at the solo discretion and risli of the user In no event shall the liability of Praxair Distribution Inc ensmg out ol the
use of the information con tained herein exceed the Ice established for providing such information
APPENDIX H
Reference Method EPA Protocol 1 Gas Certifications
r "1
RAl A CLASS
Dual-Analyzed Calibration Standard
AiR LIQUIDE Air Liquide / menca
Specialty Gz^es LLC Scott~
9810 BAY AREA BLVD, PASADENA, TX 77507
CERTIFICATE OF ACCURACY. EPA Protocpl Gas
Phone [phone] Fax [phone]
Customer
URS
ITEM* URS012
Assay laboratory i
PO No URS ^
AIR LIQUIDE AMERICA SPECIALTY GASES LLC Project No 04-i!4924-001
9810 BAY AREA BLVD f
PASADENA, TX, 77507 ^ , I
- ~ ^ . i i
ANALYTICAL INFORMATION -•^ '^ ^
This certification was performed accordiii^'to EPA Traceability Pritocol For Assay & Certiftcation of Gaseous Calibration Standards,
Procedure G 1, September, 199V I
Cylinder Number ALM048820 Certificationipate 07Jul200g Exp Date 07Jul2012
Cylinder Pressure* 1897 PSIG '
ANALYTICAL
COMPONENT CERTIFIED CONCENiqiATION (Moles) ACCURACY** TRACEABILITY
CARBON MONOXIDE 47 1 PPM Direct NIST and NMi
NITROGEN > BALANCE
'" Do not use whien cylbtier pressure is b6\<yN 15p psIg
** Analytical accuracy is ba*ed on the requirements of EPA Protocol Propedure GI, September 1997
REFERENCE STANDAR
TYPE/SRM NO EXPI8&B0JI DATE CYLINDER NUMBER
NTRM 1679 KAL003168
CONCENTRATION
101 0 PPM
COMPONENT
CARBON MONOXIDE
INSTRUMENTATION
iWSTnUMEWT/MODEL/SERIALli'
mR//000929060
ANALYZER READINGS
DATE LAST CALIBRATED
30Jun2009
ANALYTICAL PRINCIPLE
FTIR
(Z = Zero Gas R = Reference Gas T = Test Gas r=Correlation Coefficient)
First Triad Analyse Second Triad Analysis Calibration Curve
CARBON MONOXIDE
Date 2$Jun2009 Rnponw Unit PPM
Z1-0 02528 R1 = 101J193 T1-47 240B5
R2-101 3671 Z2=10 03067 T2» 47 30458
Z3<:<0 0S6S0 T3a47 30815 R3''101 52S4
Avg CofRentntio n 47 07 PPM
Dit* 07Jul2009 RMponn Untt- PPM
21-0 00119 R1-100^636 T1-47 21S7Z
R2-iai 0366 Z2«0 05124 T2 -47 23912
Z3»0 10040 T3-47 24401 R3-101 1317
Avg Concanmtlon 47 19 PPM
Concirnralion-A+Bx + Cx2+Dx3 4- Ex4
r-9 99997E1
Constants A-OOOOOOE+0
B=7 10S75E1 C=3 41000E-4
DcOOOOOOE+0 E-OOOOOOE+0
Special Notes
APPROVED BY
CERTS AND TAGS URS
ITEM* UagOU LOT#^
Ramien JR
Page 1 of 1
AIR LIQUIDE
CERTIFICATE of ANALYSIS
interference-Free Multi-Component EPA Protocol Gases
NOTE Analytical uncertainty and NIST traceability are in compliance with EPA-600/R-97/121
Section 2 2 Procedure G-1
Customer
PO Number
Item Number
Notes
Assay Date
URS CORPORATION
URS013
7-Aug-07
Cyl Number CC113980
Expiration Dale 6 Aug-10
Shipping Order U 26178926
Transfer # 26178926
LOT# LPX225131
Valve CGA350
Cyl Pressure* igoopslg
*Cy1lndar should not bs ussd wlion gas
prsasura Is bslow 190 psIg
Component
Requested
Concentration
Assay
Concentration
Carbon Monoxide 97 S ppm 97 8 ±1 0 ppm
Nitrogen Balance Balance
Reference Standard(s) Employed For Analysis
Std name Std # Cone Units Std Erior Comp Balance Cvl No Exp Date Sample No
GMIS312 GMIS342 99 51 ppm 0 48 CO N2 CC186844 11/14/2008 0
Analysis Information
kiRDonsnt 1 Carbon Monoxido
^miatf tnlormatlon Hret Triad Analysis On: 7/31/2007 Second Triad Analysis Oa e/7/2007
•fnuractmr KVB/Analad Trial 1 Thai 2 Tltel3 Units Trial 1 Trial 2 Trials Units
t^odslMuriber EN3024 Zsro •Oitn 4113 ao* Zero •023 005 001
Seftal Nimtwr 3024 RcterencB 103.07 10242 103.28 Reference 103 71 10X92 103 44
/Uialyf cal Principle FTIR
miosiat &
Candidate 100 SI 10126 100 C9 Candidate 101 74 102 3D 102.14
MPC Ceitirated Result 9740 S7M 6738 tm Restit 07 64 alio 98.02 Bum
MeanResuB: 9758 Mean Result 97 99 ppm
Analyst Signature RonStitt Calculated by M Adnane
MIX Assayed At Air Liquide America 11426 Fairmont Pkwy, La Porte, TX, 77571 Phone [phone] Fax [phone]
— !
AiR LIQUIDE Air LiquidB America SCOtt" Specialty Gases LLC %^ J w n.
9810 BAY AREA BLVD, PASADENA. TX 77507
CERTIFICATE OF ACCURACY- EPA Protocol Gas
RATA CLASS
Dual-Analyzed Calibration Standard
Phone [phone] Fax [phone]
Astav Laboratory
PO No URS
AIR LIQUIDE AMERICA SPECIALTY GASES LLC Project No 04-74926 001
9810 BAY AREA BLVD '
Customer
URS
ITEM* URS019
PASADENA, TX 77507
ANAkYTICAL INFORMATION.
^ -\ —
This certification was performed according to EPA Traceability Protocol
Procedure G-1, September, 1997
Cylinder Number ALM009988 Certlficaton
Cylinder Pressure* *• 2000 PSIG
COMPONENT
CARBON DIOXIDE
OXYGEN
NITROGEN
CERTIPIED CONCENTIATION (Moles)
9 64
010
* Do not use when cylinder pressure Is IMIOW 150 pslg
Analytical accuracy Is based on the requirements of EPA Protocol Procedure GI September 1997
l=or Assay & Certification of Gaseous Calibration Standards,
Date 08JUI2009 Exp Date 08Jul2012
%
BALANCE
ANALYTICAL
ACCURACY** TRACEABILITY
+1- ^% Direct NIST and NMi
+/- 1% Direct NIST and NMi
REFERENCE STANDARD
TYPE/SRM NO EXPIRATION DATE CYLINDER NUMBER
NTRM 1373 ""-02OCT20TZ 'KOOZeOa
NTRM 2350 01Apr20l2 A6S20
INSTRUMENTATION
INSTRUMENT/MODEL/SERIAliy
MTIA/M2O0/171109
SERVOMEX/MODEL 244A/701/716
ANALYZER READINGS
CONCENTRATION
•13 93 %
23 51 %
COMPONENT
CARBON DIOXIDE
OXYGEN
DATE LAST CALIBRATED
18Jun2009
29Jun2009
ANALYTICAL PRINCIPLE
GAS CHROMATOGRAPHY
PARAMAGNETIC
(Z = Zero Gas R= Reference Gas T=Test Gas r = Correlation Coefficient)
First Triad Analysis Second Triad Analysis Calibration Curve
CARBON DIOXIDE
Date 0SJUI2DD9 Rnpciiue UnitJUlEA
21 -0 00000 R1 -1754124 T1 a 737274 0
R2 0 1754208 Z2 -515 0000 72- 738015 0
Z3- 401 0000 T3 = 738013 0 R3-1755614
Avg ConcentrBlfon 9 £39 %
OXYGEN
a*ta 08JulZ009 Responai Unit VOLTS
Zli 0 00000 R1 -o^szeo T1-0 4G410
n2= 0 99340 22 -0 00100 T2- 0 48430
Z3 = 0 00100 T3 -0 464SO R3-0J93SO
Avs Connirtratloa 10^5 %
ConcentraUon ••A + Bx + Cii2+Dx3+ Ex4
leO 9999948
Consiantt A- 0 03C337S2
B= 0000132179 C-
D- E-
Special Notes
APPROVED BY
WD TAGP
f UR^019
D>yiD KELLV
Coneentntlon - A+Bx + Cx2 + D«3 + Elt4
r-0 9999961
Con«tttnts A—0 01708837
B-23 7Z1S1747 C-
D-E=
iPagft-1 nf 1
AIRaLIQUIDE
CERTIFICATE of ANALYSIS
Interference-Free Multi-Component EPA Protocol Gases
NOTE Analytical uncertainty and NIST traceability are in compliance with EPA-600/R-97/121
Section 2 2 Procedure G-1
Customer
P O Number
Item Number
Notes
Assay Date
URS CORPORATION
URS020
29-Jan-09
Cylinder Number CC178359
Expiration Date 29-Jan-12
Shipping Order It 32218928
Transfer #• 32218928
LOT# LPX247285
Vaive CGASgO
Cyl Pressure* 1900psig
Cylinder should not ba UMd whan gas
prvnuro la balow 150 ptig
Component
Requested
Concentration
Assay
Concentration
Carbon Dioxide
Oxygen
19 S %
22 %
19 S ±0 2 %
21 9 ±0 1 %
Nitrogen Balance Balance
Rsferance Stanilard(s) Employed For Analysis
Std name Std# Cone Units Std Error Comp Balance Cyl No Exp Date Sample No
NTRM43 1800 17 87 % 011 C02 N2 K023932 3/1/2009 100104
GMIS421 GMIS421 21 9 % 0 1 02 N2 CC178365 3/27/2011 N A
lysis Information
Componanl T Carbon DIoKlda
y^nolvzer trrformaVon Fli«t Triad Anilnlc Oit 1/27/2009 Second Triad Analysis On.
Manutacttrer KVB/Analect Trial 1 Trtal2 Tnel3 Units Trial 1 Trial 2 Tit 013 Units
Modal Numter EN3024 Zero 0 37 0129 a26 Zero
Serlal Klumber 3024 Reference 17 74 17 84 1(01 Reference
Analytical Princliito. FTIR Candidate 19 39 1990 1940 Candidate
MPCCalbrated-01/22109 Result 19 39 19 S3 19^4 % Result
Mean ResuL 19 4S H Mean ResulC
Component 2 Oitvqen
/^nalvzef Informalton First Triad Analysis On 1/2312009 Second Triad Analysis On.
Manufacturer Servomex Trial 1 Trial 2 Tt1al3 Units Triall Trial 2 Trial 3 Units
Model Numtwr 4G05C Zero 0 04 004 004 Zero
Sertal Numtwr 1101 Reference 21 7S 21 77 2177 Reference
Analylcal Principle Paramag Cenclldate 21 79 21 7« 2179 Candidate
MPC C^Rvated-01123103 Resid 21 ea Z190 2199 Result
Mean Result 21 e9 Mean Result
Analyst signature Warren Pereira Calculated by Warren Pereira
MIX Assayed At Air Liquide America 11426 Fairmont Pkwy, La Porte, TX, 77571 Phone [phone] Fax [phone]
APPENDIX I
Reference Method CEMs Interference Test
MEMORANDUM
To File ^^003
Date 9 Januarv^ed?
From E Youn^erman
Subject CEMS Interference Testing
The attached tables and data sheets present the results of CEMS interference testing
performed in the Austin laboratones in October 2007 Note that the values presented m
the tables may disagree slightly with the values m the hand-wntten data sheets The
values in the tables were taJcen from the actual raw data, found on the local area network
in
Ursausfsl\Data\Projects\Measurements\Quality Management Program\CEMs Interference Testing 2007
Date of Test 11-Oct
Analyzer Type NOx
Manufacturer Thermo
Model Number 42 CHL
Serial Number 76266-382
Calibration Span 100
Without Target Analyte
Interferent Instrument Response (ppm)
Component Concentration
(ppm)
Without
Interferent
With
Interferent
Arithmetic
Difference
NH3 10
-0 1 0 04 0 14 Propane 50 -0 1 0 04 0 14
Hydrogen 50
-0 1 0 04 0 14
Methane 50 -01 0 1 02
HCI 10 -0 1 0 21 0 31
CO 50 -0 1 0 1 02
SOz 20 -0 1 0 1 02
COz 5% -0 1 00 0 09 Oz 6% -0 1 00 0 09
CO2 15% -0 1 -0 1 0 Oz 18%
-0 1 -0 1 0
Sum of Responses ^ 1 14
% of Calibration Span 1 1%
^ Only includes worst case contribution from CO2
With Target Analyte
interferent instrument Response (ppm)
Component Concentration Without With Arithmetic Component (ppm) Interferent Interferent Difference
NH3 10
Propane 50 26 8 26 7 -0 1
Hydrogen 50
Methane 50 26 8 26 7 -01
HCI 10 26 8 26 8 0
CO 50 28 9 28 9 0
SO2 20 28 9 29 3 04
COz 5% 26 79 26 5 -0 3 Oz 6%
26 79 26 5 -0 3
COz 14% 26 5 25 6 -0 9
Oz 17% 26 5 25 6 -0 9
Sum of Responses ^ -07
% of Calibration Span -0 7%
^ Only includes worst case contribution from CO2
Date of Test 11-Oct
Analyzer Type NOx
Manufacturer Teledyne
Model Number 200 EH
Serial Number 395
Calibration Span 100
Without Target Analyte
Interferent Instrument Response (ppm)
Component Concentration
(ppm)
Without
Interferent,
With
Interferent
Anthmetic
Difference
NH3 10
0 78 07 -0 08 Propane 50 0 78 07 -0 08
Hydrogen 50
0 78 07 -0 08
Methane 50 0 78 07 -0 08
HCI 10 0 78 07 -0 08
CO 50 0 78 1 05 0 27
SOz 20 0 78 08 0 02
COz 5% 0 78 1 08 03
Oz 6%
0 78 1 08 03
COz 15% 0 78 1 08 03
Oz 18%
0 78 1 08 03
Sum of Responses ^ 0 35
% of Calibration Span 0 4%
Only includes worst case contribution from COz
With Target Analyte
Interferent Instrument Response (ppm)
Component Concentration Without With Arithmetic Component (ppm) Interferent Interferent Difference
NH3 10
20 7 20 6 -0 1 Propane 50 20 7 20 6 -0 1
Hydrogen 50
Methane 50 20 7 20 65 -0 1
HCI 10 20 7 20 77 01
CO 50 20 7 20 96 03
SOz 20 20 7 20 46 -0 2
COz 15% 20 7 19 77 -0 9
Oz 18%
20 7 19 77 -0 9
COz 14% 20 7 19 43 -1 3
Oz 17%
20 7 19 43 -1 3
Sum of Responses ^ -1 3
% of Calibration Span -1 3%
Only includes worst case contribution from COz
Date of Test 11-Oct
Analyzer Type CO2
Manufacturer Servomex
Model Number 1440
Serial Number 0144OD1/3982
Calibration Span (%) 20
Without Target Analyte
Interferent Instrument Response (ppm)
Component Concentration Without With Anthmetic Component (ppm) Interferent Interferent Difference
NH3 10
Propane 50 -0 09 -0 09 -0 09
Hydrogen 50
Methane 50 -0 09 -0 09 0
HCI 10 -0 09 -0 01 0 08
CO 50 -0 09 -0 09 0
SO2 20 -0 09 -0 08 0 01
N2O 10
NO2 14 -0 09 -0 05 0 04
NO 16
Sum of Responses 0 04
% of Calibration Span 0 2%
With Target Analyte
Interferent Instrument Response (ppm)
Component Concentration Without With Arithmetic Component (ppm) Interferent Interferent Difference
NH3 10
Propane 50 4 88 4 88 0
Hydrogen 50
Methane 50 4 88 4 89 0 01
HCI 10 4 88 4 88 0
CO 50 4 88 4 78 -01
SO2 20 4 88 49 0 02
N2O 10
NO2 14 4 88 4 88 0
NO 16
Sum of Responses -0 07
% of Calibration Span -0 3%
Date of Test 11-Oct
Analyzer Type Oxygen
Manufacturer Servomex
Model Number 1440
Serial Number 0144OD1/3982
Calibration Span (%) 20
Without Tar get Analyte
Interferent Instrument Response (ppm)
Component Concentration
(ppm)
Without
Interferent
With
Interferent
Arithmetic
Difference
NH3 10
0 05 0 06 -0 09 Propane 50 0 05 0 06 -0 09
Hydrogen 50
0 05 0 06 -0 09
Methane 50 0 05 0 03 -0 02
HCI 10 0 05 0 03 -0 02
CO 50 0 05 0 02 -0 03
SO2 20 0 05 0 02 -0 03
N2O 10
0 05 0 04 -0 01 NO2 14 0 05 0 04 -0 01
NO 16
0 05 0 04 -0 01
Sum of Responses -0 2
% of Calibration Span -1 0%
With Target Analyte
Interferent Instrument Response (ppm)
Component Concentration Without With Arithmetic Component (ppm) Interferent Interferent Difference
NH3 10
5 95 Propane 50 5 95 5 93 -0 02
Hydrogen 50
Methane 50 5 95 5 94 -0 01
HCI 10 5 95 5 94 -0 01
CO 50 5 95 5 78 -017
SO2 20 5 95 5 95 0
N2O 10
NO2 14 5 95 5 94 -0 01
NO 16
Sum of Responses -0 22
% of Calibration Span -1 1%
Date of Test 11-Oct
Analyzer Type ^Oz
Manufacturer Ametek
Model Number 721AT
Senal Number 91-721AT2-7866-1
Calibration Span 100
Without Tar get Analyte
Interferent Instrument Response (ppm)
Component Concentration
(ppm)
Without
Interferent
With
Interferent
Arithmetic
Difference
NH3 10
05 08 03 Propane 50 05 08 03
Hydrogen 50
05 08 03
Methane 50 05 04 -01
HCI 10 05 02 -0 3
CO 50 05 -0 2 -0 7
N2O 10
05 -0 2 -08 NOz 14 05 -0 2 -08
NO 16
05 -0 2 -08
COz 5% 05 02 -0 3
Oz 6%
05 02 -0 3
COz 15% 05 -0 2 -0 7 Oz 18% 05 -0 2 -0 7
Sum of Responses ^ -2 4
% of Calibration Span -2 4%
^ Only includes worst case contribution from CO;
With Target Analyte
Interferent Instrument Response (ppm)
Component Concentration Without With Arithmetic Component (ppm) Interferent Interferent Difference
NH3 10
Propane 50 20 3 20 4 0 1
Hydrogen 50
Methane 50 20 3 20 1 -0 2
HCI 10 20 3 20 4 0 1
CO 50 20 3 20 3 00
NzO 10
NOz 14 20 3 20 7 04
NO 16
COz 5% 20 3 199 -0 4 Oz 6% 20 3 199 -0 4
COz 14% 20 3 20 0 -0 3
Oz 17%
20 3 20 0 -0 3
Sum of Responses ^ 00
% of Calibration Span 0 0%
^ Only includes worst case contribution from COz
Date of Test 11-Oct
Analyzer Type ^Oz
Manufacturer Ametek
Model Number 921
Sena! Number AC-921-9467-1
Calibration Span 100
Without Target Analyte
Interferent Instrument Response (ppm)
Component Concentration
(ppm)
Without
Interferent
With
Interferent
Anthmetic
Difference
NH3 10
-0 3 -0 2 01 Propane 50 -0 3 -0 2 01
Hydrogen 50
-0 3 -0 2 01
Methane 50 -0 3 -0 7 -0 4
HCI 10 -0 3 -0 6 -0 3
CO 50 -0 3 -0 8 -0 5
N2O 10
-0 3 -0 7 -0 4 NO2 14 -0 3 -0 7 -0 4
NO 16
-0 3 -0 7 -0 4
COz 5% -0 3 -0 8 -0 5
Oz 6% -0 3 -0 8 -0 5
CO2 15% -0 3 -0 8 -0 5
O2 18%
-0 3 -0 8 -0 5
Sum of Responses ^ -1 8
% of Calibration Span -1 8%
^ Only includes worst case contnbution from COz
With Target Analyte
Interferent Instrument Response (ppm)
Component Concentration Without With Arithmetic Component (ppm) Interferent Interferent Difference
NH3 10
Propane 50 198 198 00
Hydrogen 50
Methane 50 198 196 -0 2
HCI 10 198 198 00
CO 50 198 198 00
N2O 10
NOz 14 198 20 1 03
NO 16
CO2 5% 198 19 5 -0 3 O2 6% 198 19 5 -0 3
CO2 14% 198 195 -0 4 O2 17%
198 195 -0 4
Sum of Responses ^ -0 4
% of Calibration Span -0 4%
Only includes worst case contribution from CO2
Date of Test 12-Oct
Analyzer Type CO
Manufacturer Thermo
Model Number 48C
Serial Number 532714042
Calibration Span 100
Without Target Analyte
Interferent Instrument Response (ppm)
Component Concentration
(ppm)
Without
Interferent
With
Interferent
Arithmetic
Difference
NH3 10
-0 6 -0 4 02 Propane 50 -0 6 -0 4 02
Hydrogen 50
-0 6 -0 4 02
Methane 50 -0 6 -0 6 00
HCI 10 -0 6 -0 4 02
SOz 20 -0 6 -0 6 00
N2O 10
-0 6 -0 7 -0 1 NOz 14 -0 6 -0 7 -0 1
NO 16
-0 6 -0 7 -0 1
CO2 5% -0 6 -1 1 -0 5
O2 6%
-0 6 -1 1 -0 5
CO2 15% -0 6 -1 0 -0 4
Oz 18% -0 6 -1 0 -0 4
Sum of Responses ^ -0 3
% of Calibration Span -0 3%
^ Only includes worst case contribution from COz
With Target Analyte
Interferent Instrument Response (ppm)
Component Concentration
(ppm)
Without
Interferent
With
Interferent
Anthmetic
Difference
NH3 10
49 1 48 8 -0 3 Propane 50 49 1 48 8 -0 3
Hydrogen 50
49 1 48 8 -0 3
Methane 50 491 48 7 -0 3
HCI 10 49 1 49 0 00
SOz 20 491 491 0 1
NzO 10
491 48 8 -0 3 NOz 14 491 48 8 -0 3
NO 16
491 48 8 -0 3
COz 5% 189 185 -0 4
Oz 6% 189 185 -0 4
COz 15% 189 177 -1 2
O2 18%
189 177 -1 2
Sum of Responses ^ -2 0
% of Calibration Span -2 0%
^ Only includes worst case contribution from CO2
10
Date of Test 12-Oct
Analyzer Type CO
Manufacturer Teledyne
Model Number 300 EM
Serial Number 173
Calibration Span 100
Without Target Analyte
Interferent Instrument Response (ppm)
Component Concentration
(ppm)
Without
Interferent
With
Interferent
Anthmetic
Difference
NH3 10
1 2 1 1 -0 1 Propane 50 1 2 1 1 -0 1
Hydrogen 50
1 2 1 1 -0 1
Methane 50 1 2 1 2 01
HCI 10 1 2 09 -0 3
SOz 20 1 2 1 1 -01
NzO 10
1 2 1 2 00 NOz 14 1 2 1 2 00
NO 16
1 2 1 2 00
COz 5% 1 2 1 4 02
Oz 6%
1 2 1 4 02
COz 15% 1 2 1 1 -0 1
Oz 18% 1 2 1 1 -0 1
Sum of Responses ^ 00
% of Calibration Span 0 0%
^ Only includes worst case contribution from COz
With Target Analyte
Interferent Instrument Response (ppm)
Component Concentration
(ppm)
Without
Interferent
With
Interferent
Arithmetic
Difference
NH3 10
50 2 50 1 -0 1 Propane 50 50 2 50 1 -0 1
Hydrogen 50
50 2 50 1 -0 1
Methane 50 50 2 50 3 0 1
HCI 10 50 2 501 -0 1
SOz 20 50 2 50 4 01
NzO 10
50 2 50 3 0 1 NOz 14 50 2 50 3 0 1
NO 16
50 2 50 3 0 1
COz 5% 21 1 21 3 02
Oz 6%
21 1 21 3 02
CO2 15% 21 1 20 9 -0 3
Oz 18%
21 1 20 9 -0 3
Sum of Responses ^ -01
% of Calibration Span -0 1%
^ Only includes worst case contribution from COz
11
Table 7E-3 ^Example Interference Check Gas Concentrations
Potential interferent gas\l\
Concentrations \2\ Sample
conditioning type
Hot wet Dried
C02 5 and 15% 5 and 15%
H20 25% 1%
NO 15 ppmv 15 ppmv
N02 15 ppmv 15 ppmv
N20 10 ppmv 10 ppmv
CO 50 ppmv 50 ppmv
NH3 10 ppmv 10 ppmv
''CH4 50 ppmv 50 ppmv
"S02 20 ppmv 20 ppmv
H2 50 ppmv 50 ppmv
HCI 10 ppmv 10 ppmv
\1\ Any applicable gas may be eliminated or tested at a reduced level
If
the manufacturer has provided reliable means for limiting or
scrubbing
that gas to a specified level
\2\ As Practicable, gas concentrations should be the highest expected
at
test sites
0"^35 ffv^ VIC]
3fc AJOJ /(ol j,p M^O
12
URS CEMS Operation Log
Page \ of )
Project Number ^ J Operator
Source ^-^^ CJPJA^ Tfvci-Date 10-11-01
Time Activity Analyzer Response Time Activity <:09
|^>'2.L) 1(4
-O.o| il.o;3L 003L
-0 \) ^7 05
Qtn -100
^) oO 0 \^ rj,70 I 14
0 00 K m
0 o\ in ni\ n«u*/\ (24«f RL-OO;)L 0 70
1-7 ^v. PxD ^^^^ >nO 0 I on 0.-7^ MS.7/
f
50-L /
0 74-— ^ I? o3o
0 02 0 n QlH \ 11
10 Mll^ 1pJt <:o 0 h 50. /-^
Oo\ *oni La \
0 o\ 0 19
0 01 070 I |o
0 09^
111
a 09 1.4 (
KM
» !>!
n.o| 1 Rl .10'
001 i.a^
^^.^ A 07
-1 =^7
ao"7S 1 1-7
"^S^ NO Mdi <:rrla. D OO \\ ^ —f-
9.'^ 71 lb 1 Is?
-0 MS
V ll f 7T^ •iD /4A 0
i r
\9-13
i 3^ A-5*^
CO /^6rl + ^^f'3 7i1
10 -ilCI
CO
O 6c
1^53 IH'A co^ /^b CO
I^^D „„vw CO
-c <>{ /i le,
I^^S /'Ul/i u
(7 57/^0
/M is:
17^
M<i /ii^ V1C\ 77
4
14
URS CEMS Operation Lo^i^^l^y
Page of ]
ProjectNumber Operator Dr >
Source ^1^5 ^I^C, T/ut^ Date /t)-)
4
Time Activity Analyzer Response
<3Q fltft^ MiJ— ^0 o t5 Oi<i\ -0.71
ro.^7
0 oM -o^ I
oil
ml 0 4^ tQ,'^7 0.7C)
1^ •^0 - o.33i
l^fil^ic;)^/ AO MX)
AM.
EM 5.70 ^ 7C7 -0.^.0
f?;:>
0 0^ 0
5. fog ^.7 I -0 17 ^0 0/
:^7rT Ho.00
0 oq 21 %1
V S3 -0.5.1 0 0^
1^ -0^(0^
53^ O'Oa
Q.o6
<50.00 n 4fo
QQ^ -0.13 90.05?
^O^O^/ IQ \[C[ 6,0^ ~Q.07
7^ CO
-0.0 A
30 ./ '0 faQ
pro's -<^cOl
-<^.c^l OJ
G ID
a0^6^.. gO.Qg
5)^ / »o % V 0 -007 n 7g
17^
;?lo^
/O He I j^L
^0 Gl> MO
-2670 A'O^
V7.^
OS CO
M'^ C^^/ ^$G0 NO
^IG 6c:^;^ <ig Ait,
s,^^V7/ co^
6
4/t
<14 /^«^^
j?Cb.qH/l1v^7